Environmental Protection Agency § 180.629

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Environmental Protection Agency Pt. 180

Rulemaking, and the information sub- 180.9 Substantive amendments to petitions. mitted as part of the comments, the 180.29 Establishment, modification, and rev- Administrator’s response to comments ocation of tolerance on initiative of Ad- and the documents or information re- ministrator. 180.30 Judicial review. lied on by the Administrator in issuing 180.31 Temporary tolerances. the regulation or order. 180.32 Procedure for modifying and revoking (5) All other documents or informa- tolerances or exemptions from toler- tion submitted to the docket for the ances. rulemaking in question under parts 177 180.33 Fees. or part 180 of this chapter. 180.34 Tests on the amount of residue re- (6) The Notice of Hearing published maining. 180.35 Tests for potentiation. under § 179.20. 180.40 Tolerances for crop groups. (7) All notices of participation filed 180.41 Crop group tables. under § 179.42. (8) Any FEDERAL REGISTER notice Subpart C—Specific Tolerances issued under this part that pertains to the proceeding. 180.101 Specific tolerances; general provisions. (9) All submissions filed under 180.103 Captan; tolerances for residues. § 179.80. 180.106 Diuron; tolerances for residues. (10) Any document of which official 180.107 Triflumezopyrim; tolerance for resi- notice was taken under § 179.95. dues. (b) The record of the administrative 180.108 Acephate; tolerances for residues. proceeding is closed: 180.109 Fenpicoxamid; Tolerances for resi- (1) With respect to the taking of evi- dues. dence, when specified by the presiding 180.111 Malathion; tolerances for residues. 180.114 Ferbam; tolerances for residues. officer. 180.116 Ziram; tolerances for residues. (2) With respect to pleadings, at the 180.117 S-Ethyl dipropylthiocarbamate; tol- time specified in § 179.98(a) for the fil- erances for residues. ing of briefs. 180.123 Inorganic bromide residues resulting (c) The presiding officer may reopen from fumigation with methyl bromide; the record to receive further evidence tolerances for residues. at any time before the filing of the ini- 180.123a Inorganic bromide residues in pea- tial decision. nut hay and peanut hulls; statement of policy. [55 FR 50293, Dec. 5, 1990, as amended at 70 180.124 Methyl bromide; tolerances for resi- FR 33360, June 8, 2005] dues. 180.127 Piperonyl butoxide; tolerances for residues. PART 180—TOLERANCES AND EX- 180.128 Pyrethrins; tolerances for residues. EMPTIONS FOR PESTICIDE CHEM- 180.129 o-Phenylphenol and its sodium salt; ICAL RESIDUES IN FOOD tolerances for residues. 180.130 Hydrogen Cyanide; tolerances for Subpart A—Definitions and Interpretative residues. 180.132 Thiram; tolerances for residues. Regulations 180.142 2,4-D; tolerances for residues. Sec. 180.145 Fluorine compounds; tolerances for 180.1 Definitions and interpretations. residues. 180.3 Tolerances for related pesticide chemi- 180.151 Ethylene oxide; tolerances for resi- cals. dues. 180.4 Exceptions. 180.153 Diazinon; tolerances for residues. 180.5 Zero tolerances. 180.155 1-Naphthaleneacetic acid; tolerances 180.6 Pesticide tolerances regarding milk, for residues. eggs, meat, and/or poultry; statement of 180.163 Dicofol; tolerances for residues. policy. 180.169 Carbaryl; tolerances for residues. 180.172 Dodine; tolerances for residues. Subpart B—Procedural Regulations 180.175 Maleic hydrazide; tolerances for residues. 180.7 Petitions proposing tolerances or ex- 180.176 Mancozeb; tolerances for residues. emptions for pesticide residues in or on 180.178 Ethoxyquin; tolerances for residues. raw agricultural commodities or proc- 180.181 Chlorpropham; tolerances for resi- essed foods. dues. 180.8 Withdrawal of petitions without preju- 180.182 Endosulfan; tolerances for residues. dice. 180.183 Disulfoton; tolerances for residues.

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180.184 Linuron; tolerances for residues. 180.292 Picloram; tolerances for residues. 180.185 DCPA; tolerances for residues. 180.293 Endothall; tolerances for residues. 180.189 Coumaphos; tolerances for residues. 180.297 N-1-Naphthyl phthalamic acid; toler- 180.190 Diphenylamine; tolerances for resi- ances for residues. dues. 180.298 Methidathion; tolerances for resi- 180.191 Folpet; tolerances for residues. dues. 180.198 Trichlorfon; tolerances for residues. 180.299 Dicrotophos; tolerances for residues. 180.200 Dicloran; tolerances for residues. 180.300 Ethephon; tolerances for residues. 180.202 p-Chlorophenoxyacetic acid; toler- 180.301 Carboxin; tolerances for residues. ances for residues. 180.303 Oxamyl; tolerances for residues. 180.204 Dimethoate; tolerances for residues. 180.304 Oryzalin; tolerances for residues. 180.205 Paraquat; tolerances for residues. 180.314 Triallate; tolerances for residues. 180.206 Phorate; tolerances for residues. 180.316 Pyrazon; tolerances for residues. 180.207 Trifluralin; tolerances for residues. 180.317 Propyzamide; tolerances for resi- 180.208 Benfluralin; tolerances for residues. dues. 180.209 Terbacil; tolerances for residues. 180.318 4-(2-Methyl-4-chlorophenoxy) bu- 180.210 Bromacil; tolerances for residues. tyric acid; tolerance for residues. 180.211 Propachlor; tolerances for residues. 180.319 Interim tolerances. 180.212 S-Ethyl cyclohexylethylthiocarba- 180.324 Bromoxynil; tolerances for residues. mate; tolerances for residues. 180.328 Napropamide; tolerances for resi- 180.213 Simazine; tolerances for residues. dues. 180.215 Naled; tolerances for residues. 180.330 S-(2-(Ethylsulfinyl)ethyl) O,O-di- 180.217 Metiram; tolerances for residues. methyl phosphorothioate; tolerances for 180.220 Atrazine; tolerances for residues. residues. 180.222 Prometryn; tolerances for residues. 180.331 4-(2,4-Dichlorophenoxy) butyric acid; 180.225 Phosphine; tolerances for residues. tolerances for residues. 180.226 Diquat; tolerances for residues. 180.332 Metribuzin; tolerances for residues. 180.227 Dicamba; tolerances for residues. 180.337 Oxytetracycline; tolerances for resi- 180.229 Fluometuron; tolerances for residues. dues. 180.231 Dichlobenil; tolerances for residues. 180.339 MCPA; tolerances for residues. 180.235 Dichlorvos; tolerances for residues. 180.341 2,4-Dinitro-6-octylphenyl crotonate 180.236 Triphenyltin hydroxide; tolerances and 2,6-dinitro-4-octylphenyl crotonate; for residues. tolerances for residues. 180.241 Bensulide; tolerances for residues. 180.342 Chlorpyrifos; tolerances for residues. 180.242 Thiabendazole; tolerances for resi- 180.345 Ethofumesate; tolerances for residues. dues. 180.243 Propazine; tolerances for residues. 180.349 Fenamiphos; tolerances for residues. 180.245 Streptomycin; tolerances for resi- 180.350 Nitrapyrin; tolerances for residues. dues. 180.352 Terbufos; tolerances for residues. 180.249 Alachlor; tolerances for residues. 180.353 Desmedipham; tolerances for resi- 180.252 Tetrachlorvinphos; tolerances for dues. residues. 180.355 Bentazon; tolerances for residues. 180.253 Methomyl; tolerances for residues. 180.356 Norflurazon; tolerances for residues. 180.254 Carbofuran; tolerances for residues. 180.360 Asulam; tolerance for residues. 180.258 Ametryn; tolerances for residues. 180.361 Pendimethalin; tolerances for resi- 180.259 Propargite; tolerances for residues. dues. 180.261 Phosmet; tolerances for residues. 180.362 Fenbutatin-oxide; tolerances for res- 180.262 Ethoprop; tolerances for residues. idues. 180.269 Aldicarb; tolerances for residues. 180.364 Glyphosate; tolerances for residues. 180.272 Tribuphos; tolerances for residues. 180.367 n-Octyl bicycloheptenedicarbox- 180.274 Propanil; tolerances for residues. imide; tolerances for residues. 180.275 Chlorothalonil; tolerances for resi- 180.368 Metolachlor; tolerances for residues. dues. 180.370 5-Ethoxy-3-(trichloromethyl)-1, 2, 4- 180.276 Formetanate hydrochloride; toler- thiadiazole; tolerances for residues. ances for residues. 180.371 Thiophanate-methyl; tolerances for 180.278 Phenmedipham; tolerances for resi- residues. dues. 180.372 2,6-Dimethyl-4-tridecylmorpholine; 180.284 Zinc phosphide; tolerances for resi- tolerances for residues. dues. 180.373 [Reserved] 180.287 Amitraz; tolerances for residues. 180.377 Diflubenzuron; tolerances for resi- 180.288 2-(Thiocyanomethylthio) dues. benzothiazole; tolerances for residues. 180.378 Permethrin; tolerances for residues. 180.289 Methanearsonic acid; tolerances for 180.380 Vinclozolin; tolerances for residues. residues. 180.381 Oxyfluorfen; tolerances for residues. 180.291 Pentachloronitrobenzene; tolerance 180.383 Sodium salt of acifluorfen; toler- for residues. ances for residues.

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180.384 Mepiquat (N,N-dimethylpiperidin- 180.441 Quizalofop ethyl; tolerances for resi- ium); tolerances for residues. dues. 180.385 Diclofop-methyl; tolerances for resi- 180.442 Bifenthrin; tolerances for residues. dues. 180.443 Myclobutanil; tolerances for resi- 180.388–180.389 [Reserved] dues. 180.390 Tebuthiuron; tolerances for residues. 180.444 Sulfur dioxide; tolerances for resi- 180.395 Hydramethylnon; tolerances for residues. dues. 180.445 Bensulfuron methyl; tolerances for 180.396 Hexazinone; tolerances for residues. residues. 180.399 Iprodione; tolerances for residues. 180.446 Clofentezine; tolerances for residues. 180.401 Thiobencarb; tolerances for residues. 180.447 Imazethapyr; tolerances for residues. 180.403 Thidiazuron; tolerances for residues. 180.448 Hexythiazox; tolerance for residues. 180.404 Profenofos; tolerances for residues. 180.449 Avermectin B1 and its delta-8,9-iso- 180.405 Chlorsulfuron; tolerances for resi- mer; tolerances for residues. dues. 180.450 Beta-(4-Chlorophenoxy)-alpha-(1,1- 180.407 Thiodicarb; tolerances for residues. dimethylethyl)-1H-1,2,4-triazole-1-eth- 180.408 Metalaxyl; tolerances for residues. anol; tolerances for residues. 180.409 Pirimiphos-methyl; tolerances for 180.451 Tribenuron methyl; tolerances for residues. residues. 180.410 Triadimefon; tolerances for residues. 180.452 Primisulfuron-methyl; tolerances for 180.411 Fluazifop-P-butyl; tolerances for res- residues. idues. 180.454 Nicosulfuron; tolerances for resi- 180.412 Sethoxydim; tolerances for residues. dues. 180.413 Imazalil; tolerances for residues. 180.455 Procymidone; tolerances for resi- 180.414 Cyromazine; tolerances for residues. dues. 180.415 Aluminum tris (O-ethylphospho- 180.457 Bitertanol; tolerances for residues. nate); tolerances for residues. 180.458 Clethodim; tolerances for residues. 180.416 Ethalfluralin; tolerances for resi- 180.459 Triasulfuron; tolerances for residues. dues. 180.460 Benoxacor; tolerances for residues. 180.417 Triclopyr; tolerances for residues. 180.461 Cadusafos; tolerances for residues. 180.418 Cypermethrin and isomers alpha- 180.462 Pyridate; tolerances for residues. cypermethrin and zeta-cypermethrin; 180.463 Quinclorac; tolerances for residues. tolerances for residues. 180.464 Dimethenamid; tolerances for resi- 180.419 Chlorpyrifos-methyl; tolerances for dues. residues. 180.465 4-(Dichloroacetyl)-1-oxa-4- 180.420 Fluridone; tolerances for residues. azaspiro[4.5]decane. 180.421 Fenarimol; tolerances for residues. 180.466 Fenpropathrin; tolerances for resi- 180.425 Clomazone; tolerances for residues. dues. 180.426 2-[4,5-Dihydro-4-methyl-4-(1- 180.467 Carbon disulfide; tolerances for resi- methylethyl)-5-oxo-1H-imidazol-2-yl]-3- dues. quinoline carboxylic acid; tolerance for 180.468 Flumetsulam; tolerances for resi- residues. dues. 180.427 Tau-Fluvalinate; tolerances for resi- 180.469 Dichlormid; tolerances for residues. dues. 180.470 Acetochlor; tolerances for residues. 180.428 Metsulfuron methyl; tolerances for 180.471 Furilazole; tolerances for residues. residues. 180.472 Imidacloprid; tolerances for resi- 180.429 Chlorimuron ethyl; tolerances for dues. residues. 180.473 Glufosinate ammonium; tolerances 180.430 Fenoxaprop-ethyl; tolerances for res- for residues. idues. 180.474 Tebuconazole; tolerances for resi- 180.431 Clopyralid; tolerances for residues. dues. 180.432 Lactofen; tolerances for residues. 180.475 Difenoconazole; tolerances for resi- 180.433 Fomesafen; tolerances for residues. dues. 180.434 Propiconazole; tolerances for resi- 180.476 Triflumizole; tolerances for residues. dues. 180.477 Flumiclorac pentyl; tolerances for 180.435 Deltamethrin; tolerances for resi- residues. dues. 180.478 Rimsulfuron; tolerances for residues. 180.436 Cyfluthrin and the isomer beta- 180.479 Halosulfuron-methyl; tolerances for cyfluthrin; tolerances for residues. residues. 180.437 Imazamethabenz-methyl; tolerances 180.480 Fenbuconazole; tolerances for resi- for residues. dues. 180.438 Lambda-cyhalothrin and an isomer 180.481 Prosulfuron; tolerances for residues. gamma-cyhalothrin; tolerances for resi- 180.482 Tebufenozide; tolerances for residues. dues. 180.439 Thifensulfuron methyl; tolerances 180.484 Flutolanil; tolerances for residues. for residues. 180.485 Cyproconazole; tolerances for resi- 180.440 Tefluthrin; tolerances for residues. dues.

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180.486 Chlorethoxyfos; tolerances for resi- 180.537 Isoxaflutole; tolerances for residues. dues. 180.539 d-Limonene; tolerances for residues. 180.487 Pyrithiobac sodium; tolerances for 180.540 Fenitrothion; tolerances for resi- residues. dues. 180.490 Imazapic; tolerances for residues. 180.543 Diclosulam; tolerances for residues. 180.491 Propylene oxide; tolerances for resi- 180.544 Methoxyfenozide; tolerances for residues. dues. 180.492 Triflusulfuron-methyl; tolerances 180.545 Prallethrin; tolerances for residues. for residues. 180.546 Mefenoxam; tolerances for residues. 180.493 Dimethomorph; tolerances for resi- 180.547 Prohexadione calcium; tolerances dues. for residues. 180.494 Pyridaben; tolerance for residues. 180.549 Diflufenzopyr; tolerances for resi- 180.495 Spinosad; tolerances for residues. dues. 180.498 Sulfentrazone; tolerances for resi- 180.551 Fluthiacet-methyl; tolerances for dues. residues. 180.499 Propamocarb; tolerances for resi- 180.552 Sulfosulfuron; tolerances for residues. dues. 180.500 Imazapyr; tolerances for residues. 180.553 Fenhexamid; tolerances for residues. 180.501 Hydroprene; tolerances for residues. 180.554 Kresoxim-methyl; tolerances for res- 180.502 Aminoethoxyvinylglycine hydro- idues. chloride (aviglycine HCl); tolerances for 180.555 Trifloxystrobin; tolerances for resi- residues. dues. 180.503 Cymoxanil, tolerance for residues. 180.556 Pymetrozine; tolerances for resi- 180.504 [Reserved] dues. 180.505 Emamectin; tolerances for residues. 180.557 Tetraconazole; tolerances for resi- 180.506 Cyclanilide; tolerances for residues. dues. 180.507 Azoxystrobin; tolerances for resi- 180.559 Clodinafop-propargyl; tolerances for dues. residues. 180.509 Mefenpyr-diethyl; tolerance for resi- 180.560 Cloquintocet-mexyl; tolerances for dues. residues. 180.510 Pyriproxyfen; tolerances for resi- 180.561 Acibenzolar-S-methyl; tolerances for dues. residues. 180.511 Buprofezin; tolerances for residues. 180.562 Flucarbazone-sodium; tolerances for 180.512 [Reserved] residues. 180.513 Chlorfenapyr; tolerances for resi- 180.563 Ethametsulfuron-methyl; tolerances dues. for residues. 180.514 Cloransulam-methyl; tolerances for 180.564 Indoxacarb; tolerances for residues. residues. 180.565 Thiamethoxam; tolerances for resi- 180.515 Carfentrazone-ethyl; tolerances for dues. residues. 180.566 Fenpyroximate; tolerances for resi- 180.516 Fludioxonil; tolerances for residues. dues. 180.517 Fipronil; tolerances for residues. 180.567 Zoxamide; tolerances for residues. 180.518 Pyrimethanil; tolerances for resi- 180.568 Flumioxazin; tolerances for residues. dues. 180.569 Forchlorfenuron; tolerances for resi- 180.519 Bromide ion and residual bromine; dues. tolerances for residues. 180.570 Isoxadifen-ethyl; tolerances for resi- 180.521 Fumigants for grain-mill machinery; dues. tolerances for residues. 180.571 Mesotrione; tolerances for residues. 180.522 Fumigants for processed grains used 180.572 Bifenazate; tolerance for residues. in production of fermented malt bev- 180.573 Tepraloxydim; tolerances for resi- erage; tolerances for residues. dues. 180.523 Metaldehyde; tolerances for resi- 180.574 Fluazinam; tolerances for residues. dues. 180.575 Sulfuryl fluoride; tolerances for resi- 180.525 Resmethrin; tolerances for residues. dues. 180.526 Synthetic isoparaffinic petroleum 180.576 Cyhalofop-butyl; tolerances for resi- hydrocarbons; tolerances for residues. dues. 180.527 Flufenacet, N-(4-fluorophenyl)-N-(1- 180.577 Bispyribac-sodium; tolerances for methylethyl)-2-[[5-(trifluoromethyl)-1, 3, residues. 4-thiadiazol-2-yl] oxy]acetamide and its 180.578 Acetamiprid; tolerances for residues. metabolites containing the 4-fluoro-N- 180.579 Fenamidone; tolerances for residues. methylethyl benzenamine tolerances for 180.580 Iodosulfuron-Methyl-Sodium; toler- residues. ances for residues. 180.532 Cyprodinil; tolerances for residues. 180.581 Iprovalicarb; tolerances for residues. 180.533 Esfenvalerate; tolerances for resi- 180.582 Pyraclostrobin; tolerances for residues. dues. 180.535 Fluroxypyr 1-methylheptyl ester; 180.583 Triticonazole; tolerances for resi- tolerances for residues. dues.

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180.584 Tolylfluanid; tolerances for residues. 180.631 Pyrasulfotole; tolerances for resi- 180.585 Pyraflufen-ethyl; tolerances for residues. dues. 180.632 Fenazaquin; Tolerances for residues. 180.586 Clothianidin; tolerances for residues. 180.633 Florasulam; tolerances for residues. 180.587 Famoxadone; tolerance for residues. 180.634 Tembotrione; tolerances for resi- 180.588 Quinoxyfen; tolerances for residues. dues. 180.589 Boscalid; tolerances for residues. 180.635 Spinetoram; tolerances for residues. 180.590 2, 6-Diisopropylnaphthalene (2, 6- 180.636 1,3-dichloropropene; tolerances for DIPN); tolerances for residues. residues. 180.591 Trifloxysulfuron; tolerances for resi- 180.637 Mandipropamid; tolerances for residues. dues. 180.592 Butafenacil; tolerances for residues. 180.638 Pyroxsulam; tolerances for residues. 180.593 Etoxazole; tolerances for residues. 180.639 Flubendiamide; tolerances for resi- 180.594 Thiacloprid; tolerances for residues. dues. 180.595 Flufenpyr-ethyl; tolerances for resi- 180.640 Pyridalyl; tolerances for residues. dues. 180.641 Spirotetramat; tolerances for resi- 180.596 Fosthiazate; tolerances for residues. dues. 180.597 Mesosulfuron-methyl; tolerances for 180.643 Uniconazole; tolerances for residues. residues. 180.644 Cyprosulfamide; tolerances for resi- 180.598 Novaluron; tolerances for residues. dues. 180.599 Acequinocyl; tolerances for residues. 180.645 Thiencarbazone-methyl; tolerances 180.600 Propoxycarbazone; tolerances for for residues. 180.646 Ipconazole; tolerances for residues. residues 180.647 d-Phenothrin; tolerances for resi- 180.601 Cyazofamid; tolerances for residues. dues. 180.602 Spiroxamine; tolerances for residues. 180.648 Meptyldinocap; tolerances for resi- 180.603 Dinotefuran; tolerances for residues. dues. 180.604 Mepanipyrim; tolerances for resi- 180.649 Saflufenacil; tolerances for residues. dues. 180.650 Isoxaben; tolerances for residues. 180.605 Penoxsulam; tolerances for residues. 180.651 Imazosulfuron; tolerances for resi- 180.607 Spiromesifen; tolerances for residues. dues. 180.652 Ethiprole; tolerances for residues. 180.608 Spirodiclofen; tolerances for resi- 180.653 Indaziflam; tolerances for residues. dues. 180.654 Isopyrazam; tolerances for residues. 180.609 Fluoxastrobin; tolerances for resi- 180.655 Flazasulfuron; tolerances for residues. dues. 180.610 Aminopyralid; tolerances for resi- 180.656 Amisulbrom; tolerances for residues. dues. 180.657 Metaflumizone; tolerances for resi- 180.611 Pinoxaden; tolerances for residues. dues. 180.612 Topramezone; tolerances for resi- 180.658 Penthiopyrad; tolerances for residues. dues. 180.613 Flonicamid; tolerances for residues. 180.659 Pyroxasulfone; tolerances for resi- 180.614 Kasugamycin; tolerances for residues. dues. 180.660 Pyriofenone; tolerances for residues. 180.615 Amicarbazone; tolerances for resi- 180.661 Fluopyram; tolerances for residues. dues. 180.662 Trinexapac-ethyl; tolerances for res- 180.616 Fenpropimorph; tolerances for resi- idues. dues. 180.663 Ametoctradin; tolerances for resi- 180.617 Metconazole; tolerances for residues. dues. 180.618 Benthiavalicarb-isopropyl; tolerance 180.664 Penflufen; tolerances for residues. for residues. 180.665 Sedaxane; tolerances for residues. 180.619 Epoxiconazole; tolerances for resi- 180.666 Fluxapyroxad; tolerances for residues. dues. 180.620 Etofenprox; tolerances for residues. 180.667 Cyflufenamid, tolerance for residues. 180.621 Dithianon; tolerances for residues. 180.668 Sulfoxaflor; tolerances for residues. 180.622 Ethaboxam; tolerances for residues. 180.669 Picoxystrobin; tolerances for resi- 180.623 Flufenoxuron; tolerances for residues. dues. 180.671 Fenpyrazamine; tolerances for resi- 180.624 Metrafenone; tolerances for residues. dues. 180.625 Orthosulfamuron; tolerances for res- 180.672 Cyantraniliprole; tolerances for resi- idues. dues. 180.626 Prothioconazole; tolerances for resi- 180.673 Triforine; tolerances for residues. dues. 180.674 Proquinazid; tolerances for residues. 180.627 Fluopicolide; tolerances for residues. 180.675 Tolfenpyrad; tolerances for residues. 180.628 Chlorantraniliprole; tolerances for 180.676 Fenpropidin; tolerances for residues. residues. 180.677 Cyflumetofen; tolerances for resi- 180.629 Flutriafol; tolerances for residues. dues.

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180.678 Tricyclazole; tolerances for residues. 180.950 Tolerance exemptions for minimal 180.679 Flupyradifurone; tolerances for resi- risk active and inert ingredients. dues. 180.960 Polymers; exemptions from the re- 180.680 Fluensulfone; tolerances for resi- quirement of a tolerance. dues. 180.1011 Viable spores of the microorganism 180.681 Isofetamid; tolerances for residues. Bacillus thuringiensis Berliner; exemption 180.682 Bicyclopyrone; tolerances for resi- from the requirement of a tolerance. dues. 180.1016 Ethylene; exemption from the re- 180.684 Benalaxyl-M; tolerances for residues. quirement of a tolerance. 180.685 Oxathiapiprolin; tolerances for resi- 180.1017 Diatomaceous earth; exemption dues. from the requirement of a tolerance. 180.686 Benzovindiflupyr; tolerances for res- 180.1019 Sulfuric acid; exemption from the idues. requirement of a tolerance. 180.687 Teflubenzuron; tolerances for resi- 180.1020 Sodium chlorate; exemption from dues. the requirement of a tolerance. 180.688 Diethofencarb; tolerance for residue. 180.1021 Copper; exemption from the re- 180.689 Aminocyclopyrachlor; tolerances for quirement of a tolerance. residues. 180.1022 Iodine-detergent complex; exemp- 180.690 Mandestrobin; tolerances for resi- tion from the requirement of a tolerance. dues. 180.1023 Propanoic acid; exemptions from 180.691 Halauxifen-methyl; tolerances for the requirement of a tolerance. residues. 180.1025 Xylene; exemption from the re- 180.692 Tioxazafen; tolerances for residues. quirement of a tolerance. 180.693 Benzobicyclon; tolerances for resi- 180.1027 Nuclear polyhedrosis virus of dues. Heliothis zea; exemption from the re- 180.694 Cyclaniliprole; tolerances for resi- quirement of a tolerance. dues. 180.1033 Methoprene; exemption from the re- 180.696 Tolpyralate; tolerances for residues. quirement of a tolerance. 180.697 Flutianil; tolerances for residues. 180.1037 Polybutenes; exemption from the 180.698 Chlormequat chloride; tolerances for requirement of a tolerance. residues. 180.1040 Ethylene glycol; exemption from 180.699 Pydiflumetofen; tolerances for resi- the requirement of a tolerance. dues. 180.1041 Nosema locustae; exemption from 180.700 Afidopyropen; Tolerances for resi- the requirement of a tolerance. dues. 180.1043 Gossyplure; exemption from the re- 180.701 Pyrifluquinazon; tolerances for resi- quirement of a tolerance. dues. 180.1049 Carbon dioxide; exemption from the 180.702 Bixafen; tolerances for residues. requirement of a tolerance. 180.703 6-benzyladenine; tolerances for resi- 180.1050 Nitrogen; exemption from the re- dues. quirements of a tolerance. 180.704 Sulfometuron-methyl; tolerances for 180.1052 2,2,5-trimethyl-3-dichloroacetyl-1,3- residues. oxazolidine; exemption from the require- 180.705 Mefentrifluconazole; tolerances for ment of a tolerance. residues. 180.1054 Calcium hypochlorite; exemptions 180.706 Valifenalate; tolerances for residues. from the requirement of a tolerance. 180.708 Isotianil; tolerances for residues. 180.1056 Boiled linseed oil; exemption from requirement of tolerance. Subpart D—Exemptions From Tolerances 180.1057 Phytophthora palmivora; exemption from requirement of tolerance. 180.900 Exemptions from the requirement of 180.1058 Sodium diacetate; exemption from a tolerance. the requirement of a tolerance. 180.905 Pesticide chemicals; exemptions 180.1064 Tomato pinworm insect pheromone; from the requirement of a tolerance. exemption from the requirement of a tol- 180.910 Inert ingredients used pre- and post- erance. harvest; exemptions from the require- 180.1065 2-Amino-4,5-dihydro-6-methyl-4- ment of a tolerance. propyl-s-triazolo(1,5-alpha)pyrimidin-5- 180.920 Inert ingredients used pre-harvest; one; exemption from the requirement of exemptions from the requirement of a a tolerance. tolerance. 180.1067 Methyl eugenol and malathion com- 180.930 Inert ingredients applied to animals; bination; exemption from the require- exemptions from the requirement of a ment of a tolerance. tolerance. 180.1068 C12-C18 fatty acid potassium salts; 180.940 Tolerance exemptions for active and exemption from the requirement of a tol- inert ingredients for use in antimicrobial erance. formulations (Food-contact surface sani- 180.1069 (Z)-11-Hexadecenal; exemption from tizing solutions). the requirement of a tolerance.

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180.1070 Sodium chlorite; exemption from 180.1114 Pseudomonas fluorescens A506, the requirement of a tolerance. Pseudomonas fluorescens 1629RS, and 180.1071 Peanuts, Tree Nuts, Milk, Soy- Pseudomonas syringae 742RS; exemptions beans, Eggs, Fish, Crustacea, and Wheat; from the requirement of a tolerance. exemption from the requirement of a tol- 180.1118 Spodoptera exigua nuclear poly- erance. hedrosis virus; exemption from the re- 180.1072 Poly-D-glucosamine (chitosan); ex- quirement of a tolerance. emption from the requirement of a toler- 180.1119 Azadirachtin; exemption from the ance. requirement of a tolerance. 180.1073 Isomate-M; exemption from the re- 180.1120 Streptomyces sp. strain K61; exemp- quirement of a tolerance. tion from the requirement of a tolerance. 180.1074 F.D.&C. Blue No. 1; exemption from 180.1121 Boric acid and its salts, borax (so- the requirement of a tolerance. dium borate decahydrate), disodium 180.1075 Colletotrichum gloeosporioides f. sp. octaborate tetrahydrate, boric oxide aeschynomene; exemption from the re- (boric anhydride), sodium borate and so- quirement of a tolerance. dium metaborate; exemptions from the 180.1076 Viable spores of the microorganism requirement of a tolerance. Bacillus popilliae; exemption from the re- 180.1122 Inert ingredients of semiochemical quirement of a tolerance. dispensers; exemptions from the require- 180.1080 Plant volatiles and pheromone; ex- ment of a tolerance. emptions from the requirement of a tol- 180.1124 Arthropod pheromones; exemption erance. from the requirement of a tolerance. 180.1083 Dimethyl sulfoxide; exemption 180.1126 Codlure, (E,E)-8,10-Dodecadien-1-ol; from the requirement of a tolerance. exemption from the requirement of a tol- 180.1084 Monocarbamide dihydrogen sulfate; erance. exemption from the requirement of a tol- 180.1127 Biochemical pesticide plant floral erance. volatile attractant compounds: cinna- 180.1086 3,7,11-Trimethyl-1,6,10-dodecatriene- maldehyde, cinnamyl alcohol, 4-methoxy 1-ol and 3,7,11-trimethyl-2,6,10- cinnamaldehyde, 3-phenyl propanol, 4- dodecatriene-3-ol; exemption from the re- methoxy phenethyl alcohol, indole, and quirement of a tolerance. 1,2,4-trimethoxybenzene; exemptions 180.1087 Sesame stalks; exemption from the from the requirement of a tolerance. requirement of a tolerance. 180.1128 Bacillus amyloliquefaciens MBI600; 180.1089 Poly-N-acetyl-D-glucosamine; ex- exemption from the requirement of a tol- emption from the requirement of a toler- erance. ance. 180.1090 Lactic acid; exemption from the re- 180.1130 N-(n-octyl)-2-pyrrolidone and N-(n- quirement of a tolerance. dodecyl)-2-pyrrolidone; exemptions from 180.1091 Aluminum isopropoxide and alu- the requirement of a tolerance. minum secondary butoxide; exemption 180.1135 Pasteuria penetrans; exemption from from the requirement of a tolerance. the requirement of a tolerance. 180.1092 Menthol; exemption from the re- 180.1139 Sodium 5-nitroguaiacolate; exemp- quirement of a tolerance. tion from the requirement of a tolerance. 180.1095 Chlorine gas; exemptions from the 180.1140 Sodium o-nitrophenolate; exemp- requirement of a tolerance. tion from the requirement of a tolerance. 180.1097 GBM-ROPE; exemption from the re- 180.1141 Sodium p-nitrophenolate; exemp- quirement of a tolerance. tion from the requirement of a tolerance. 180.1098 Gibberellins [Gibberellic Acids (GA3 180.1142 1,4-Dimethylnaphthalene; exemp- and GA4 + GA7), and Sodium or Potas- tion from the requirement of a tolerance. sium Gibberellate]; exemption from the 180.1143 Methyl anthranilate; exemption requirement of a tolerance. from the requirement of a tolerance. 180.1100 Gliocladium virens isolate GL-21; ex- 180.1145 Pseudomonas syringae; exemption emption from the requirement of a toler- from the requirement of a tolerance. ance. 180.1146 Beauveria bassiana Strain GHA; ex- 180.1101 Parasitic (parasitoid) and predatory emption from the requirement of a toler- insects; exemption from the requirement ance. of a tolerance. 180.1148 Occlusion Bodies of the Granulosis 180.1102 Trichoderma harzianum KRL-AG2 Virus of Cydia pomenella; tolerance ex- (ATCC #20847) strain T–22; exemption emption. from requirement of a tolerance. 180.1149 Inclusion bodies of the multi-nu- 180.1103 Isomate-C; exemption from the re- clear polyhedrosis virus of Anagrapha quirement of a tolerance. falcifera; exemption from the require- 180.1110 3-Carbamyl-2,4,5-trichlorobenzoic ment of a tolerance. acid; exemption from the requirement of 180.1150 6-Benzyladenine; exemption from a tolerance. the requirement of a tolerance. 180.1111 Bacillus subtilis GB03; exemption 180.1153 Lepidopteran pheromones; exemp- from the requirement of a tolerance. tion from the requirement of a tolerance.

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180.1156 Cinnamaldehyde; exemption from 180.1205 Beauveria bassiana ATCC #74040; ex- the requirement of a tolerance. emption from the requirements of a tol- 180.1157 Cytokinins; exemption from the re- erance. quirement of a tolerance. 180.1206 Aspergillus flavus AF36; exemption 180.1158 Auxins; exemption from the re- from the requirement of a tolerance. quirement of a tolerance. 180.1207 N-acyl sarcosines and sodium N- 180.1159 Pelargonic acid; exemption from acyl sarcosinates; exemption from the re- the requirement of tolerances. quirement of a tolerance. 180.1160 Jojoba oil; exemption from the re- 180.1209 Bacillus subtilis strain QST 713 and quirement of a tolerance. strain QST 713 variant soil; exemption 180.1161 Clarified hydrophobic extract of from the requirement of a tolerance. neem oil; exemption from the require- 180.1210 Phosphorous acid; exemption from ment of a tolerance. the requirement of a tolerance. 180.1212 Pseudomonas chlororaphis Strain 63– 180.1162 Acrylate polymers and copolymers; 28; exemption from the requirement of a exemption from the requirement of a tol- tolerance. erance. 180.1213 Coniothyrium minitans strain CON/ 180.1163 Killed Myrothecium verrucaria; ex- M/91–08; exemption from the requirement emption from the requirement of a toler- of a tolerance. ance. 180.1218 Indian Meal Moth Granulosis Virus; 180.1165 Capsaicin; exemption from the re- exemption from the requirement of a tol- quirement of a tolerance. erance. 180.1167 Allyl isothiocyanate as a compo- 180.1219 Foramsulfuron; exemption from the nent of food grade oil of mustard; exemp- requirement of a tolerance. tion from the requirement of a tolerance. 180.1220 1-Methylcyclopropene; exemption 180.1176 Sodium bicarbonate; exemption from the requirement of a tolerance. from the requirement of a tolerance. 180.1222 Sucrose octanoate esters; exemp- 180.1177 Potassium bicarbonate; exemption tion from the requirement of a tolerance. from the requirement of a tolerance. 180.1223 Imazamox; exemption from the re- 180.1178 Formic acid; exemption from the quirement of a tolerance. requirement of a tolerance. 180.1224 Bacillus pumilus GB34; exemption 180.1179 Plant extract derived from Opuntia from the requirement of a tolerance. lindheimeri, Quercus falcata, Rhus 180.1225 Decanoic acid; exemption from the aromatica, and Rhizophoria mangle; ex- requirement of a tolerance. emption from the requirement of a toler- 180.1226 Bacillus pumilus strain QST2808; ance. temporary exemption from the require- 180.1180 Kaolin; exemption from the requirement of a tolerance. ment of a tolerance. 180.1228 Diallyl sulfides; exemption from the 180.1181 Bacillus cereus strain BPO1; exemp- requirement of a tolerance. tion from the requirement of a tolerance. 180.1230 Ferrous sulfate; exemption from 180.1187 L-glutamic acid; exemption from the requirement of a tolerance. the requirement of a tolerance. 180.1231 Lime; exemption from the require- 180.1188 Gamma aminobutyric acid; exemp- ment of a tolerance. tion from the requirement of a tolerance. 180.1232 Lime-sulfur; exemption from the re- 180.1189 Methyl salicylate; exemption from quirement of a tolerance. the requirement of a tolerance. 180.1233 Potassium sorbate; exemption from the requirement of a tolerance. 180.1191 Ferric phosphate; exemption from 180.1234 Sodium carbonate; exemption from the requirement of a tolerance. the requirement of a tolerance. 180.1193 Potassium dihydrogen phosphate; 180.1235 Sodium hypochlorite; exemption exemption from the requirement of a tol- from the requirement of a tolerance. erance. 180.1236 Sulfur; exemption from the require- 180.1195 Titanium dioxide. ment of a tolerance. 180.1196 Peroxyacetic acid; exemption from 180.1237 Sodium metasilicate; exemption the requirement of a tolerance. from the requirement of a tolerance. 180.1197 Hydrogen peroxide; exemption from 180.1240 Thymol; exemption from the re- the requirement of a tolerance. quirement of a tolerance. 180.1198 Gliocladium catenulatum strain 180.1243 Bacillus subtilis var. amylolique- J1446; exemption from the requirement of faciens strain FZB24; exemption from the a tolerance. requirement of a tolerance. 180.1199 Lysophosphatidylethanolamine 180.1244 Ammonium bicarbonate; exemption (LPE); exemption from the requirement from the requirement of a tolerance. of a tolerance. 180.1245 Rhamnolipid biosurfactant; exemp- 180.1202 Bacillus sphaericus; exemption from tion from the requirement of a tolerance. the requirement of a tolerance. 180.1246 Yeast Extract Hydrolysate from 180.1204 Harpin protein; exemption from the Saccharomyces cerevisiae: exemption from requirement of a tolerance. the requirement of a tolerance.

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180.1248 Exemption of citronellol from the 180.1280 Poly(hexamethylenebiguanide) hy- requirement of a tolerance. drochloride (PHMB); exemption from the 180.1250 C8, C10, and C12 fatty acid mono- requirement of a tolerance. esters of glycerol and propylene glycol; 180.1281 S-Abscisic Acid, (S)-5-(1-hydroxy- exemption from the requirement of a tol- 2,6,6-trimethyl-4-oxo-1-cyclohex-2-enyl)- erance. 3-methyl-penta-(2Z,4E)-dienoic Acid; ex- 180.1251 Geraniol; exemption from the re- emption from the requirement of a toler- quirement of a tolerance. ance. 180.1253 Streptomyces lydicus WYEC 108; ex- 180.1282 Bacillus firmus I-1582; exemption emption from the requirement of a toler- from the requirement of a tolerance. ance. 180.1283 (Z)-7,8-epoxy-2-methyloctadecane 180.1254 Aspergillus flavus NRRL 21882; ex- (Disparlure); exemption from the re- emption from the requirement of a toler- quirement of a tolerance. ance. 180.1284 Ammonium salts of higher fatty 180.1255 Bacillus pumilus strain QST 2808; ex- acids (C8-C18 saturated; C8-C12 unsatu- emption from the requirement of a toler- rated); exemption from the requirement ance. of a tolerance. 180.1257 Purpureocillium lilacinum strain 180.1285 Polyoxin D zinc salt; exemption 251; exemption from the requirement of a from the requirement of a tolerance. tolerance. 180.1287 Extract of Chenopodium ambrosioides 180.1258 Acetic acid; exemption from the re- near ambrosioides; exemption from the requirement of a tolerance. quirement of a tolerance. 180.1259 Reynoutria sachalinensis extract; ex- 180.1288 Tristyrylphenol ethoxylates; exemption from the requirement of a toler- emption from the requirement of a tolerance. ance. 180.1260 Muscodor albus QST 20799 and the 180.1289 Candida oleophila Strain O; exemp- volatiles produced on rehydration; ex- tion from the requirement of a tolerance. emption from the requirement of a toler- 180.1290 Pasteuria usgae; exemption from the ance. requirement of a tolerance. 180.1261 Xanthomonas campestris pv. 180.1291 Cold pressed neem oil; exemption vesicatoria and Pseudomonas syringae pv. from the requirement of a tolerance. tomato specific Bacteriophages. 180.1292 Ulocladium oudemansii (U3 Strain); exemption from the requirement of a tol- 180.1262 Sorbitol octanoate; exemption from erance. the requirement of a tolerance. 180.1293 Trichoderma gamsii strain ICC 080; 180.1263 Tetrahydrofurfuryl alcohol; exemp- exemption from the requirement of a tol- tion from the requirement of a tolerance. erance. 180.1267 Pantoea agglomerans strain C9–1; ex- 180.1294 Trichoderma asperellum strain ICC emption from the requirement of a toler- 012; exemption from the requirement of a ance. tolerance. 180.1268 Potassium silicate; exemption from 180.1295 Laminarin; exemption from the re- the requirement of a tolerance. quirement of a tolerance. 180.1269 Bacillus mycoides isolate J; exemp- 180.1296 Terpene Constituents a-terpinene, tion from the requirement of a tolerance. d-limonene and p-cymene, of the Extract 180.1270 Isophorone; exemption from the re- of Chenopodium ambrosioides near quirement of a tolerance. ambrosioides as Synthetically Manufac- 180.1271 Eucalyptus oil; exemption from the tured; exemption from the requirement requirement of a tolerance. of a tolerance. 180.1272 Pantoea agglomerans strain E325; ex- 180.1297 Homobrassinolide; exemption from emption from the requirement of a toler- the requirement of a tolerance. ance. 180.1298 Trichoderma hamatum isolate 382; 180.1273 Beauveria bassiana HF23; exemp- exemption from the requirement of a tol- tion from the requirement of a tolerance. erance. 180.1274 Tris (2-ethylhexyl) phosphate; ex- 180.1299 Prohydrojasmon; exemption from emption from the requirement of a toler- the requirement of a tolerance. ance. 180.1300 Potassium hypochlorite; exemption 180.1275 Pythium oligandrum DV 74; exemp- from the requirement of a tolerance. tion from the requirement of a tolerance. 180.1301 Escherichia coli O157:H7 specific 180.1276 Tobacco mild green mosaic bacteriophages; temporary exemption tobamovirus strain U2; exemption from from the requirement of a tolerance. the requirement of a tolerance. 180.1302 Sodium Ferric Ethylenediamine- 180.1277 Dibasic esters; exemption from the tetraacetate (EDTA); exemption from requirement of a tolerance. the requirement of a tolerance. 180.1278 Quillaja saponaria extract 180.1303 Metarhizium anisopliae strain F52; (saponins); exemption from the require- exemption from the requirement of a tol- ment of a tolerance. erance.

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180.1304 Pseudomonas fluorescens strain 180.1327 Tetraacetylethylenediamine CL145A; exemption from the requirement (TAED) and its metabolite of a tolerance. Diacetylethylenediamine (DAED); ex- 180.1305 Chromobacterium subtsugae strain emption from the requirement of a toler- PRAA4–1T; exemption from the require- ance. ment of a tolerance. 180.1328 Beauveria bassiana strain ANT–03; 180.1306 Isaria fumosorosea (formerly exemption from the requirement of a tol- Paecilomyces fumosoroseus) Apopka erance. strain 97; exemption from the require- 180.1329 Bacillus subtilis strain IAB/BS03, ment of a tolerance. exemption from the requirement of a tol- 180.1307 Bacteriophage of Clavibacter erance. michiganensis subspecies michiganensis; 180.1330 1-Octanol; exemption from the re- exemption from the requirement of a tol- quirement of a tolerance. erance. 180.1331 Trichoderma asperelloides strain 180.1308 Bacillus amyloliquefaciens strain JM41R; exemption from the requirement D747; exemption from the requirement of of a tolerance. a tolerance. 180.1332 Lavandulyl senecioate; exemption 180.1309 Bacillus subtilis strain CX–9060; ex- from the requirement of a tolerance. emption from the requirement of a toler- 180.1333 Potassium Salts of Hops Beta acids; ance. exemption from the requirement of a tol- 180.1310 Trichoderma virens strain G–41; ex- erance. emption from the requirement of a toler- 180.1334 Choline Chloride; exemption from ance. the requirement of a tolerance. 180.1311 Pasteuria nishizawae—Pn1; exemp- 180.1335 Isaria fumosorosea strain FE 9901; tion from the requirement of a tolerance. exemption from the requirement of a tol- 180.1312 Aureobasidium pullulans strains erance. DSM 14940 and DSM 14941; exemption 180.1336 Bacillus amyloliquefaciens strain from the requirement of a tolerance. PTA–4838; exemption from the require- 180.1313 Bacillus pumilus strain GHA 180; ex- ment of a tolerance. emption from the requirement of a toler- 180.1337 Citrus tristeza virus expressing ance. spinach defensin proteins 2, 7, and 8; ex- 180.1314 Killed, nonviable Streptomyces emption from the requirement of a toler- acidiscabies strain RL–110T; exemption ance. from the requirement of a tolerance. 180.1338 Aspergillus flavus strains TC16F, 180.1315 Natamycin; exemption from the re- TC35C, TC38B, and TC46G; temporary ex- quirement of a tolerance. emptions from the requirement of a tol- 180.1316 Pasteuria spp. (Rotylenchulus erance. reniformis nematode)—Pr3; exemption 180.1339 Spodoptera frugiperda multiple from the requirement of a tolerance. nucleopolyhedrovirus strain 3AP2; ex- 180.1317 Pesticide chemicals; exemption emption from the requirement of a toler- from the requirements of a tolerance. ance. 180.1318 3-decen-2-one; exemption from the 180.1340 Muscodor albus strain SA–13 and requirement of a tolerance. the volatiles produced on rehydration; 180.1319 Banda de Lupinus albus doce exemption from the requirement of a tol- (BLAD); exemption from the requirement erance. of a tolerance. 180.1341 Pseudomonas chlororaphis strain 180.1320 Methyl jasmonate; exemption from AFS009; exemption from the requirement the requirement of a tolerance. of a tolerance. 180.1321 Complex Polymeric Polyhydroxy 180.1344 Cyclaniliprole; exemption from the Acids; exemption from the requirement requirement of a tolerance. of a tolerance. 180.1345 1-Triacontanol; exemption from the 180.1322 Bacillus pumilus strain BU F–33; ex- requirement of a tolerance. emption from the requirement of a toler- 180.1346 1,3-Dibromo-5,5- ance. Dimethylhydantoin; exemption from the 180.1323 Ethyl-2E,4Z-decadienoate (Pear requirement of a tolerance. Ester); exemption from the requirement 180.1347 Bacillus amyloliquefaciens strain of a tolerance. F727; exemption from the requirement of 180.1324 GS-omega/kappa-Hxtx-Hv1a; ex- a tolerance. emption from the requirement of a toler- 180.1348 Bacillus subtilis strain BU1814; ex- ance. emption from the requirement of a toler- 180.1325 Heat-killed Burkholderia spp. strain ance. A396 cells and spent fermentation media 180.1350 Bacillus licheniformis strain exemption from the requirement of a tol- FMCH001; exemption from the require- erance. ment of a tolerance. 180.1326 Pseudomonas fluorescens strain D7; 180.1351 Bacillus subtilis strain FMCH002; ex- exemption from the requirement of a tol- emption from the requirement of a toler- erance. ance.

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180.1352 Methyl-alpha-D-mannopyranoside 180.1375 Methyl mercaptan; exemption from (Alpha methyl mannoside); exemption the requirement of a tolerance. from the requirement of a tolerance. 180.1376 Ea peptide 91398; exemption from 180.1353 Lipochitooligosaccharide (LCO) the requirement of a tolerance. SP104; exemption from the requirement of a tolerance. Subpart E—Pesticide Chemicals Not Re- 180.1354 Flutianil; exemption from the requiring a Tolerance or an Exemption quirement of a tolerance. From a Tolerance 180.1355 Duddingtonia flagrans strain IAH 1297; exemption from the requirement of 180.2000 Scope. a tolerance. 180.2003 Definitions. 180.1356 Extract of Swinglea glutinosa; ex- 180.2010 [Reserved] emption from the requirement of a toler- 180.2020 Non-food determinations. ance. AUTHORITY: 21 U.S.C. 321(q), 346a and 371. 180.1357 Cerevisane (cell walls of Saccharo- myces cerevisiae strain LAS117); exemp- SOURCE: 36 FR 22540, Nov. 25, 1971, unless tion from the requirement of a tolerance. otherwise noted. 180.1358 Metschnikowia fructicola strain NRRL EDITORIAL NOTE: Nomenclature changes to Y–27328; exemption from the requirement part 180 appear at 62 FR 66023, Dec. 17, 1997. of a tolerance. 180.1359 Bacteriophage active against GLOSSARY Erwinia amylovora; exemption from the re- NOTE: The items in this glossary were com- quirement of a tolerance. piled as an aid to the users of the Code of 180.1360 Bacteriophage active against Federal Regulations. Inclusion or exclusion Xanthomonas citri subsp. citri; exemption from this glossary has no legal significance. from the requirement of a tolerance. APPLI = APPLICATION 180.1361 Pepino mosaic virus, strain CH2, iso- C-I MET = CHOLINESTERASE-INHIBITING late 1906; exemption from the require- METABOLITES ment of a tolerance. CARB = CARBAMATES 180.1362 Beauveria bassiana strain PPRI 5339; EPWRR = EDIBLE PORTION WITH RIND exemption from the requirement of a tol- REMOVED erance. EXC = EXCEPT 180.1363 Bacillus amyloliquefaciens strain I (IN PPM COLUMN) = INTERIM TOLER- ENV503; exemption from the requirement ANCE of a tolerance. INC = INCLUDING 180.1364 Chlorate; exemption from the re- K = CWHR = KERNEL PLUS COB WITH quirement of a tolerance. HUSK REMOVED 180.1365 Bacteriophage active against Xylella MBYP = MEAT BYPRODUCTS fastidiosa; exemption from the require- MIN = MINIMUM ment of a tolerance. N (IN PPM COLUMN) = NEGLIGIBLE RESI- 180.1366 24-Epibrassinolide; exemption from DUES the requirement of a tolerance. NMT = NOT MORE THAN 180.1367 Bacillus amyloliquefaciens subspecies NON-PER BAG/PKGD RAC = NON-PERISH- plantarum strain FZB42; exemption from ABLE PACKAGED OR BAGGED RAW AG- the requirement of a tolerance. RICULTURAL COMMODITY 180.1368 Clonostachys rosea strain CR–7; ex- PPM = PART(S) PER MILLION emption from the requirement of a toler- POST-H = POSTHARVEST APPLICATION ance. PRE-H = PREHARVEST APPLICATION 180.1369 Autographa californica multiple PRE-S = PRESLAUGHTER APPLICATION nucleopolyhedrovirus strain FV#11; ex- PRODS = PRODUCTS rollert emption from the requirement of a toler- T (IN PPM COLUMN) = TEMPORARY TOL- ance. ERANCE 180.1370 Lipochitoolgiosaccharide (LCO) [41 FR 4537, Jan. 30, 1976] MOR116; exemption from the requirement of a tolerance. 180.1371 Florpyrauxifen-benzyl; exemption Subpart A—Definitions and from the requirement of a tolerance. Interpretative Regulations 180.1372 Sodium lauryl sulfate; exemption from the requirement of a tolerance. § 180.1 Definitions and interpretations. 180.1373 Chrysodeixis includens (a) Administrator, without qualifica- nucleopolyhedrovirus isolate #460; ex- tion, means the Administrator of the emption from the requirement of a tolerance. Environmental Protection Agency. 180.1374 Autographa californica multiple (b) Agency, without qualification, nucleopolyhedrovirus strain R3; exemp- means the Environmental Protection tion from the requirement of a tolerance. Agency.

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(c) FFDCA means the Federal Food, modity in conformity with a tolerance Drug, and Cosmetic Act, as amended, under this section; 21 U.S.C. 301–392. (2) The pesticide chemical residue (d) Raw agricultural commodities in- has been removed to the extent pos- clude, among other things, fresh fruits, sible in good manufacturing practice; whether or not they have been washed and and colored or otherwise treated in (3) The concentration of the pesticide their unpeeled natural form; vegetables chemical residue in the processed food in their raw or natural state, whether is not greater than the tolerance pre- or not they have been stripped of their outer leaves, waxed, prepared into scribed for the pesticide chemical res- fresh green salads, etc.; grains, nuts, idue on the raw agricultural com- eggs, raw milk, meats, and similar ag- modity. ricultural produce. It does not include (f) For the purpose of computing fees foods that have been processed, fab- as required by § 180.33, each group of re- ricated, or manufactured by cooking, lated crops listed in § 180.34(e) and each freezing, dehydrating, or milling. crop group or subgroup listed in § 180.41 (e) Where a raw agricultural com- is counted as a single raw agricultural modity bearing a pesticide chemical commodity in a petition or request for residue that has been exempted from tolerances or exemption from the re- the requirement of a tolerance, or quirement of a tolerance. which is within a tolerance permitted (g) Tolerances and exemptions estab- under FFDCA section 408, is used in lished for pesticide chemicals in or on preparing a processed food, the proc- the general category of raw agricul- essed food will not be considered unsafe tural commodities listed in column A within the meaning of FFDCA sections apply to the corresponding specific raw 402 and 408(a), despite the lack of a tolerance or exemption for the pesticide agricultural commodities listed in col- chemical residue in the processed food, umn B. However, a tolerance or exemp- if: tion for a specific commodity in col- (1) The pesticide chemical has been umn B does not apply to the general used in or on the raw agricultural com- category in column A.

A B

Alfalfa Medicago sativa L. Subsp. sativa, (alfalfa, lucerne); Onobrychis viciifolia Scop. (sainfoin, holy clover, esparcet); and Lotus corniculatus L. (trefoil); and varieties and/or hybrids of these.

Banana Banana, plantain.

Bean Cicer arietinum (chickpea, garbanzo bean); Lupinus spp. (including sweet lupine, white sweet lupine, white lupine, and grain lupine). Phaseolus spp. (including kidney bean, lima bean, mung bean, navy bean, pinto bean, snap bean, and waxbean; Vicia faba (broad bean, fava bean); Vigna spp. (including asparagus bean, blackeyed pea and cowpea).

Bean, dry All beans above in dry form only.

Bean, succulent All beans above in succulent form only.

Blackberry Rubus eubatus (including bingleberry, black satin berry, boysenberry Cherokee blackberry, Chesterberry, Cheyenne blackberry, coryberry, darrowberry, dewberry, Dirksen thornless berry, Himalayaberry, hullberry, Lavacaberry, lowberry, Lucretiaberry, mammoth blackberry, marionberry, nectarberry, olallieberry, Oregon evergreen berry, phenomenalberry, rangerberry, ravenberry, rossberry, Shawnee blackberry, and varieties and/or hybrids of these).

Broccoli Broccoli, Chinese broccoli (gai lon, white flowering broccoli).

Cabbage Cabbage, Chinese cabbage (tight-heading varieties only).

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A B

Caneberry Rubus spp. (including blackberry); Rubus caesius (youngberry); Rubus loganbaccus (loganberry); Rubus idaeus (red and black raspberry); cultivars, varieties, and/or hybrids of these.

Celery Celery, Florence fennel (sweet anise, sweet fennel, finochio) (fresh leaves and stalks only).

Cherry Cherry, sweet, and cherry, tart.

Endive Endive, escarole.

Fern, edible, fiddlehead Fern, edible, fiddlehead including: Black lady fern, Deparia japonica (Thunb.) M. Kato; Bracken fern, Pteridium aquilinum (L.) Kuhn; Broad buckler fern, Dryopteris dilatata (Hoffm.) A. Gray; Cinnamon fern, Osmundastrum cinnamomeum (L.) C. Presl; Lady fern, Athyrium filix-femina (L.) Roth ex Mert.; Leather fern, Acrostichum aureum L.; Mother fern, Diplazium proliferum (Lam.) Thouars; Ostrich fern, Matteuccia struthiopteris (L.) Tod.; Vegetable fern, Diplazium esculentum (Retz.) Sw.; Zenmai fern, Osmuda japonica Thunb.

Fruit, citrus Grapefruit, lemon, lime, orange, tangelo, tangerine, citrus citron, kumquat, and hybrids of these.

Garlic Garlic, great headed; garlic, and serpent garlic.

Guava Guava (Psidium guajava L.); Guava, cattley (Psidium cattleyanum Sabine); Guava, Para (Psidium acutangulum DC.); Guava, purple strawberry (Psidium cattleyanum Sabine var. cattleyanum); Guava, strawberry (Psidium cattleyanum Sabine var. littorale (Raddi) Fosberg); Guava, yellow strawberry (Psidium cattleyanum Sabine var. cattleyanum forma lucidum O. Deg.)

Lettuce Lettuce, head; and lettuce, leaf

Lettuce, head Lettuce, head; crisphead varieties only

Lettuce, leaf Lettuce, leaf; cos (romaine), butterhead varieties

Marjoram Origanum spp. (includes sweet or annual marjoram, wild marjoram or oregano, and pot marjoram).

Melon Muskmelon, including hybrids and/or varieties of Cucumis melo (including true cantaloupe, cantaloupe, casaba, Santa Claus melon, crenshaw melon, honeydew melon, honey balls, Persian melon, golden pershaw melon, mango melon, pineapple melon, snake melon); and watermelon, including hybrids and/or varieties of (Citrullus spp.).

Muskmelon Cucumis melo (includes true cantaloupe, cantaloupe, casaba, Santa Claus melon, crenshaw melon, honeydew melon, honey balls, Per- sian melon, golden pershaw melon, mango melon, pineapple melon, snake melon, and other varieties and/or hybrids of these.)

Onion Bulb onion; green onion; and garlic.

Onion, bulb Bulb onion; garlic; great headed garlic; serpent garlic; Chinese onion; pearl onion; potato onion; and shallot, bulb.

Onion, green Green onion; lady’s leek; leek; wild leek; Beltsville bunching onion; fresh onion; tree onion, tops; Welsh onion; and shallot, fresh leaves.

Palm hearts Palm hearts, various species, including: African fan palm, Borassus aethiopum Mart.; Cabbage palm, Euterpe oleracea Mart.; Cabbage palmetto, Sabal palmetto (Walter) Schult. & Schult. f.; Coconut, Cocos nucifera L.; Palmyra palm, Borassus flabellifera L.; Peach Palm, Bactris gasipaes Kunth; Royal palm, Roystonea oleracea (Jacq.) O.F. Cook; Salak palm, Salacca zalacca (Gaertn.) Voss; Saw palmetto, Serenoa repens (W. Bartram) Small; Wine palm, Raphia spp.

Peach Peach, nectarine

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A B

Pea Cajanus cajan (includes pigeon pea); Cicer spp. (includes chickpea and garbanzo bean); Lens culinaris (lentil); Pisum spp. (includes dwarf pea, garden pea, green pea, English pea, field pea, and edible pod pea). [Note: A variety of pesticide tolerances have been previously established for pea and/or bean. Chickpea/garbanzo bean is now classified in both the bean and the pea categories. For garbanzo bean/chickpea only, the highest established pea or bean tolerance will apply to pesticide residues found in this commodity.]

Pea, dry All peas in dry form only.

Pea, succulent All peas in succulent form only.

Pepper All varieties of pepper including pimento and bell, hot, and sweet pepper.

Radish, oriental, roots Raphanus sativus var. longipinnatus (roots and tops), including Chi- nese or Japanese radish (both white and red), winter radish, daikon, lobok, lo pak, and other cultivars and/or hybrids of these.

Radish, oriental, tops) Raphanus sativus var. longipinnatus (roots and tops), including Chi- nese or Japanese radish (both white and red), winter radish, daikon, lobok, lo pak, and other cultivars and/or hybrids of these.

Rapeseed Brassica napus, B. campestris, and Crambe abyssinica (oilseed-producing varieties only which include canola and crambe.)

Raspberry Rubus spp. (including bababerry; black raspberry; blackcap; caneberry; framboise; frambueso; himbeere; keriberry; mayberry; red raspberry; thimbleberry; tulameen; yellow raspberry; and cultivars, varieties, and/or hybrids of these).

Sorghum, grain, grain Sorghum spp. [sorghum, grain, sudangrass (seed crop), and hybrids of these grown for its seed].

Sorghum, forage, stover Sorghum spp. [sorghum, forage; sorghum, stover; sudangrass, and hybrids of these grown for forage and/or stover.

Squash Pumpkin, summer squash, and winter squash.

Sugar apple Annona squamosa L. and its hybrid atemoya (Annona cherimola Mill X A. squamosa L.) Also includes true custard apple (Annona reticulata L.).

Squash, summer Fruits of the gourd (Cucurbitaceae) family that are consumed when immature, 100% of the fruit is edible either cooked or raw, once picked it cannot be stored, has a soft rind which is easily penetrated, and if seeds were harvested they would not germinate; e.g., Cucurbita pepo (i.e., crookneck squash, straightneck squash, scallop squash, and vegetable marrow); Lagenaria spp. (i.e., spaghetti squash, hyotan, cucuzza); Luffa spp. (i.e., hechima, Chinese okra); Momordica spp. (i.e., bitter melon, balsam pear, balsam apple, Chi- nese cucumber); Sechium edule (chayote); and other cultivars and/or hybrids of these.

Sweet potato Sweet potato, yam.

Tangerine Tangerine (mandarin or mandarin orange); clementine; Mediterranean mandarin; satsuma mandarin; tangelo; tangor; cultivars, varieties, and/or hybrids of these.

Tomato Tomato, tomatillo.

Turnip tops or turnip greens Broccoli raab (raab, raab salad), hanover salad, turnip tops (turnip greens).

Wheat Wheat, triticale.

(h) Unless otherwise specified in this ticide chemicals, the raw agricultural paragraph or in tolerance regulations commodity or processed food to be ex- prescribed in this part for specific pes- amined for pesticide residues, shall

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consist of the whole raw agricultural erance, the processed food to be exam- commodity or processed food. ined for residues shall be the whole (1) The raw agricultural commodity processed commodity on an ‘‘as is’’ bananas, when examined for pesticide basis. residues, shall not include any crown (i) The term pesticide chemical shall tissue or stalk. have the meaning specified in FFDCA (2) Shell shall be removed and dis- section 201(q)(1), as amended, except as carded from nuts before examination provided in § 180.4. for pesticide residues. (j) The term negligible residue means (3) Caps (hulls) shall be removed and any amount of a pesticide chemical re- discarded from strawberries before ex- maining in or on a raw agricultural amination for pesticide residues. commodity or group of raw agricul- (4) Stems shall be removed and dis- tural commodities that would result in carded from melons before examination a daily intake regarded as for pesticide residues. toxicologically insignificant on the (5) Roots, stems, and outer sheaths basis of scientific judgment of ade- (or husks) shall be removed and dis- quate safety data. Ordinarily this will carded from garlic bulbs and dry bulb add to the diet an amount which will onions, and only the garlic cloves and be less than 1/2,000th of the amount onion bulbs shall be examined for pes- that has been demonstrated to have no ticide residues. effect from feeding studies on the most (6) Where a tolerance is established sensitive animal species tested. Such on a root vegetable including tops and/ toxicity studies shall usually include or with tops, and the tops and the roots at least 90-day feeding studies in two are marketed together, they shall be species of mammals. analyzed separately and neither the (k) The term nonperishable raw agri- pesticide residue on the roots nor the cultural commodity means any raw agri- pesticide residue on the tops shall ex- cultural commodity not subject to ceed the tolerance level, except that in rapid decay or deterioration that would the case of carrots, parsnips, and ruta- render it unfit for consumption. Exam- bagas, the tops shall be removed and ples are cocoa beans, coffee beans, discarded before analyzing roots for field-dried beans, field-dried peas, pesticide residues. grains, and nuts. Not included are eggs, (7) The crowns (leaves at the top of milk, meat, poultry, fresh fruits, and the fruit) shall be removed and dis- vegetables such as onions, parsnips, po- carded from pineapples before examina- tatoes, and carrots. tion for pesticide residues. (l) The term tolerance with regional (8) The term lima beans means the registration means any tolerance which beans and the pod. is established for pesticide residues re- (9) The term peanuts means the pea- sulting from the use of the pesticide nut meat after removal of the hulls. pursuant to a regional registration. (10) For processed foods consisting Such a tolerance is supported by res- primarily of one ingredient and sold in idue data from specific growing regions a form requiring further preparation for a raw agricultural commodity. Indi- prior to consumption (e.g., fruit juice vidual tolerances with regional reg- concentrates, dehydrated vegetables, istration are designated in separate and powdered potatoes), the processed subsections in 40 CFR 180.101 through food to be examined for residues shall 180.999, as appropriate. Additional res- be the whole processed commodity idue data which are representative of after compensating for or reconsti- the proposed use area are required to tuting to the commodity’s normal expand the geographical area of usage moisture content, unless a tolerance of a pesticide on a raw agricultural for the concentrated or dehydrated commodity having an established ‘‘tol- food form is included in this part. If erance with regional registration.’’ there exists a tolerance for a specific Persons seeking geographically broad- pesticide on the processed food in its er registration of a crop having a ‘‘tol- concentrated or dehydrated food form, erance with regional registration’’ for the purpose of determining whether should contact the appropriate EPA the food is in compliance with that tol- product manager concerning additional

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residue data required to expand the use soil treatment is 300 parts per million area. (40 CFR 180.199), the overall inorganic (m) The term pesticide chemical res- bromide tolerance for asparagus grown idue shall have the meaning specified on methyl bromide-treated soil and in FFDCA section 201(q)(2), as amend- also fumigated with methyl bromide ed, except as provided in § 180.4. after harvest is 300 parts per million. (n) The term food commodity means: (2) Where tolerances are established (1) Any raw agricultural commodity in terms of inorganic bromide residues (food or feed) as defined in section only from use of organic bromide fumi- 201(r) of the Federal Food, Drug, and gants on raw agricutural commodities, Cosmetic Act (FFDCA); and such tolerances are sufficient to pro- (2) Any processed food or feed as detect the public health, and no addi- fined in section 201(gg) of the FFDCA. tional concurrent tolerances for the or- [36 FR 22540, Nov. 25, 1971] ganic pesticide chemicals from such use are necessary. This conclusion is EDITORIAL NOTE: For FEDERAL REGISTER ci- based on evidence of the dissipation of tations affecting § 180.1, see the List of CFR Sections Affected, which appears in the the organic pesticide or its conversion Finding Aids section of the printed volume to inorganic bromide residues in the and at www.govinfo.gov. food when ready to eat. (d)(1) Where tolerances are estab- § 180.3 Tolerances for related pesticide lished for both calcium cyanide and hy- chemicals. drogen cyanide on the same raw agri- (a) Pesticide chemicals that cause re- cultural commodity, the total amount lated pharmacological effects will be of such pesticides shall not yield more regarded, in the absence of evidence to residue than that permitted by the the contrary, as having an additive del- larger of the two tolerances, calculated eterious action. (For example, many as hydrogen cyanide. pesticide chemicals within each of the (2) Where tolerances are established following groups have related pharma- for residues of both O,O-diethyl S-[2- cological effects: Chlorinated organic (ethylthio)ethyl] phosphorodithioate pesticides, arsenic-containing chemi- and demeton (a mixture of O,O-diethyl cals, metallic dithiocarbamates, cho- O-(and S-) [2-(ethylthio)ethyl] linesterase-inhibiting pesticides.) phosphorothioates) on the same raw (b) Tolerances established for such agricultural commodity, the total related pesticide chemicals may limit amount of such pesticides shall not the amount of a common component yield more residue than that permitted (such as As2O3) that may be present, or by the larger of the two tolerances, cal- may limit the amount of biological ac- culated as demeton. tivity (such as cholinesterase inhibi- (3) Where tolerances are established tion) that may be present, or may limit for both terpene polychlorinates the total amount of related pesticide (chlorinated mixture of camphene, pi- chemicals (such as chlorinated organic nene, and related terpenes, containing pesticides) that may be present. 65–66 percent chlorine) and toxaphene (c)(1) Where tolerances for inorganic (chlorinated camphene containing 67–69 bromide in or on the same raw agricul- percent chlorine) on the same raw agri- tural commodity are set in two or cultural commodities, the total more sections in this part (example: amount of such pesticides shall not §§ 180.123 and 180.199), the overall quan- yield more residue than that permitted tity of inorganic bromide to be toler- by the larger of the two tolerances, cal- ated from use of the same pesticide in culated as a chlorinated terpene of mo- different modes of application or from lecular weight 396.6 containing 67 per- two or more pesticide chemicals for cent chlorine. which tolerances are established is the (4) Where a tolerance is established highest of the separate applicable tol- for more than one pesticide containing erances. For example, where the bro- arsenic found in, or on a raw agricul- mide tolerance on asparagus from tural commodity, the total amount of methyl bromide commodity fumigation such pesticide shall not exceed the is 100 parts per million (40 CFR 180.123) highest established tolerance cal- and on asparagus from methyl bromide culated as As2O3. 460

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(5) Where tolerances are established (10) Where a tolerance is established for more than one member of the class for triclopyr, chloropyrifos, and of dithiocarbamates listed in para- chlorpyrifos-methyl having the com- graph (e)(3) of this section on the same mon metabolite 3,5,6-trichloro-2- raw agricultural commodity, the total pyridinol on the same raw agricultural residue of such pesticides shall not ex- commodity, the total amount of such ceed that permitted by the highest tol- residues shall not exceed the highest erance established for any one member established tolerance for any of the of the class, calculated both as zinc pesticides having the metabolites. ethylenebisdithiocarbamate and car- (11) Where tolerances are established bon disulfide. The tolerance based on for more than one pesticide having the zinc ethylenebisdithiocarbamate shall metabolite 3,5,6-trichloro-2-pyridinol first be multiplied by 0.6 to convert it found in or on the raw agricultural to the equivalent carbon disulfide tol- commodity, the total amount of such erance, and then the carbon disulfide residues shall not exceed the highest tolerance levels will be compared to de- established tolerance for a pesticide termine the highest tolerance level per having this metabolite. raw agricultural commodity. (12) Where tolerances are established (6) Where tolerances are established for residues of methomyl, resulting for residues of both S,S,S-tributyl from the use of thiodicarb and/or phosphorotrithioate and tributyl methomyl on the same raw agricul- phosphorotrithioite in or on the same tural commodity, the total amount of raw agricultural commodity, the total methomyl shall not yield more residue amount of such pesticides shall not than that permitted by the higher of yield more residue than that permitted the two tolerances. by the higher of the two tolerances, (e) Except as noted in paragraphs calculated as S,S,S-tributyl (e)(1) and (2) of this section, where resi- phosphorotrithioate. dues from two or more chemicals in the same class are present in or on a raw (7) Where tolerances are established agricultural commodity the tolerance for residues of O,S-dimethyl for the total of such residues shall be phosphoramidothioate, resulting from the same as that for the chemical hav- the use of acephate ( -dimethyl O,S ing the lowest numerical tolerance in acetylphos-phoramidothioate) and/or this class, unless a higher tolerance O,S - dimethylphosphoramidothioate level is specifically provided for the on the same agricultural commodity, combined residues by a regulation in the total amount of O,S-dimethyl- this part. phosphoramidothioate shall not yield (1) Where residues from two or more more residue than that permitted by chemicals in the same class are present the higher of the two tolerances. in or on a raw agricultural commodity (8) Where a tolerance is established and there are available methods that for more than one pesticide having the permit quantitative determination of metabolites 1-(3,4-dichlorophenyl)-3- each residue, the quantity of combined methylurea (DCPMU) and 3,4- residues that are within the tolerance dichlorophenylurea (DCPU) found in or may be determined as follows: on a raw agricultural commodity, the (i) Determine the quantity of each total amount of such residues shall not residue present. exceed the highest established toler- (ii) Divide the quantity of each res- ance for a pesticide having these me- idue by the tolerance that would apply tabolites. if it occurred alone, and multiply by (9) Where a tolerance is established 100 to determine the percentage of the for more than one pesticide having as permitted amount of residue present. metabolites compounds containing the (iii) Add the percentages so obtained benzimidazole moiety found in or on a for all residues present. raw agricultural commodity, the total (iv) The sum of the percentages shall amount of such residues shall not ex- not exceed 100 percent. ceed the highest established tolerance (2) Where residues from two or more for a pesticide having these metabo- chemicals in the same class are present lites. in or on a raw agricultural commodity

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and there are available methods that Chlorbenside (p-chlorobenzyl p-chlorophenyl permit quantitative determinations of sulfide). one or more, but not all, of the resi- Chlordane. ′ dues, the amounts of such residues as Chlorobenzilate (ethyl 4,4 - dichlorobenzilate). may be determinable shall be deducted p-Chlorophenoxyacetic acid. from the total amount of residues p-Chlorophenyl-2,4,5-trichlorophenyl sulfide. present and the remainder shall have 2,4-D (2,4-dichlorophenoxyacetic acid). the same tolerance as that for the DDD (TDE). chemical having the lowest numerical DDT. tolerance in that class. The quantity of 1,1-Dichloro-2,2-bis(p-ethylphenyl) ethane. combined residues that are within the 2,6-Dichloro-4-nitroaniline. 2,4-Dichlorophenyl p-nitrophenyl ether. tolerance may be determined as fol- Dieldrin. lows: Dodecachlorooctahydro-1,3,4-metheno-2H- (i) Determine the quantity of each cyclobuta[cd]pentalene. determinable residue present. Endosulfan (6,7,8,9,10,10-hexachloro-1,5,5a, (ii) Deduct the amounts of such resi- 6,9,9a-hexahydro-6,9-methano-2,4,3- dues from the total amount of residues benzodioxathiepin-3-oxide). present and consider the remainder to Endosulfan sulfate (6,7,8,9,10,10-hexachloro- have the same tolerance as that for the 1,5,5a,6,9,9a-hexahydro-6,9-methano-2,4,3- benzodioxathiepin-3,3-dioxide). chemical having the lowest numerical Heptachlor (1,4,5,6,7,8,8-heptachlor-3a,4,7, 7a- tolerance in that class. tetrahydro-4,7-methanoindene). (iii) Divide the quantity of each de- Heptachlor epoxide (1,4,5,6,7,8,8-heptachloro- terminable residue by the tolerance 2,3-epoxy-2,3,3a,4,7,7a-hexahydro-4,7- that would apply if it occurred alone methanoindene). and the quantity of the remaining res- Hexachlorophene (2,2′-methylenebis(3,4,6- idue by the tolerance for the chemical trichlorophenol) and its monosodium salt. ′ having the lowest numerical tolerance Isopropyl 4,4 -dichlorobenzilate. Lindane. in that class and multiply by 100 to de- Methoxychlor. termine the percentage of the per- Ovex (p-chlorophenyl p- mitted amount of residue present. chlorobenzenesulfonate). (iv) Add the percentages so obtained Sesone (sodium 2,4-dichlorophenoxyethyl for all residues present. sulfate, SES). (v) The sum of the percentages shall Sodium 2,4-dichlorophenoxyacetate. not exceed 100 percent. Sodium trichloroacetate. (3) The following pesticides are mem- Sulphenone (p-chlorophenyl phenyl sulfone). Terpene polychlorinates (chlorinated mix- bers of the class of dithiocarbamates: ture of camphene, pinene, and related A mixture of 5.2 parts by weight of ammoni- terpenes 65-66 percent chlorine). ates of [ethylenebis (dithiocarbamato)] 2,3,5,6-Tetrachloronitrobenzene. zinc with 1 part by weight ethylenebis Tetradifon (2,4,5,4′-tetrachlorodiphenyl [dithiocarbamic acid] bimolecular and sulfone). trimolecular cyclic anhydrosulfides and Toxaphene (chlorinated camphene). disulfides. Trichlorobenzoic acid. 2-Chloroallyl diethyldithiocarbamate. Trichlorobenzyl chloride. Coordination product of zinc ion and maneb (5) The following are members of the containing 20 percent manganese, 2.5 percent zinc, and 77.5 percent class of cholinesterase-inhibiting pes- ethylenebisdithiocarbamate. ticides: Ferbam. Acephate (O,S-dimethyl acetyl- Maneb. phosphoramidothioate) and its cholin- Manganous dimethyldithiocarbamate. esterase-inhibiting metabolite O,S-di- Sodium dimethyldithiocarbamate. methyl phosphoramidothioate. Thiram. Aldicarb (2-methyl-2-(methylthio) Zineb. propionaldehyde O- Ziram. (methylcarbamoyl)oxime) and its (4) The following are members of the chlorinesterase-inhibiting metabolites 2- class of chlorinated organic pesticides: methyl-2-(methylsulfinyl)propionaldehyde O-(methycarbamoyl) oxime and 2-methyl- Aldrin. 2-(methylsulfonyl)propionaldehyde O- BHC (benzene hexachloride). (methylcarbamoyl)oxime. 1,1-Bis(p-chlorophenyl)-2,2,2- 4-tert-Butyl-2-chlorophenyl methyl methyl trichloroethanol. phosphoramidate.

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S-[(tert-Butylthio)methyl] O,O-diethyl O,O-Dimethyl O-p-(dimethylsulfamoyl) phosphorodithioate and its cholinesterase- phenyl phosphate. inhibiting metabolites. O,O-Dimethyl O-p-(dimethylsulfamoyl) Carbaryl (1-naphthyl N-methylcarbamate). phenyl phosphorothioate. Carbofuran (2,3,-dihydro-2,2-dimethyl-7- 3,5-Dimethyl-4-(methylthio) phenyl benzofuranyl-N-methylcarbamate). methylcarbamate. Carbofuran metabolite (2,3-dihydro-2,2-di- O,O-Dimethyl S-[4-oxo-1,2,3-benzotriazin-3- methyl-3-hydroxy-7-benofuranyl N- (4H)-ylmethyl] phosphorodithioate. methylcarbamate). Dimethyl phosphate of 3-hydroxy-N,N-di- Carbophenothion (S-[(p-chlorophenyl) methyl-cis-crotonamide. thiolmethyl] O,O-diethyl Dimethyl phosphate of 3-hydroxy-N-methyl- phosphorodithioate) and its cholinesterase- cis-crotonamide. inhibiting metabolites. Dimethyl phosphate of a-methylbenzyl 3-hy- Chlorpyrifos (O,O-diethyl O-(3,5,6-trichloro- droxy-cis-crotonate. 2-pyridyl)phosphorothioate). O,O-Dimethyl 2,2,2-trichloro-1-hydroxyethyl Chlorpyrifos-methyl (O,O-dimethyl-O-(3,5,6- phosphonate. trichloro-2-pyridyl) phosphorothioate. O,O-Dimethyl phosphorodithioate, S-ester 2-Chloro-1-(2,4,5-trichlorophenyl)vinyl di- with 4-(mercaptomethyl)-2-methozy-D2- methyl phosphate. 1,3,4-thiadiazolin-5-one. 2-Chloro-1-(2,4-dichlorophenyl) vinyl diethyl Dioxathion (2,3-p-dioxanedithiol S,S-bis (O,O- phosphate. diethylphosphorodithioate)) containing ap- Coumaphos (O,O-diethyl O-3-chloro-4-meth- proximately 70 percent cis and trans iso- yl-2-oxo-2H-1-benzopyran-7-yl phosran-7-yl mers and approximately 30 percent related phosphate). compounds. Coumaphos oxygen analog (O,O-diethyl O-3- EPN. chloro-4-methyl-2-oxo-2H-1- Ethephon ((2- - chloroethyl) phosphonic benzopyphorothioate). acid). Dialifor (S-(2-chloro-1-phthalimidoethyl) Ethion. -diethyl phosphorodithioate). O,O Ethion oxygen analog (S- Dialifor oxygen analog (S-(2-chloro-1- [[(diethoxyphosphinothioyl)thio] methyl] phthalimidoethyl) O,O-diethyl O,O-diethyl phosphorothioate). phosphorothioate). O- Ethyl O-[4-(methylthio) phenyl] S-propyl Demeton (a mixture of O,O-diethyl O-(and S) phosphorodithioate and its cholinesterase- [2-ethylthio)ethyl] phosphorothioates). inhibiting metabolites. Ethiolate (S-ethyl diethylthiocarbamate). -Ethyl -dipropylphosphorodithioate. 2,2-Dichlorovinyl dimethyl phosphate. O S,S O,O-Diethyl S-[2-(ethylthio)ethyl] Ethyl 3-methyl-4-(methylthio)phenyl (1- phosphorodithioate and its cholinesterase- methylethyl) phosphoramidate and its cho- inhibiting metabolites. linesterase-inhibiting metabolites. O,O-Diethyl O-(2-diethylamino-6-methyl-4- O-Ethyl S-phenyl ethylphosphonodithioate. pyrimidinyl) phosphorothioate and its oxy- O-Ethyl S-phenyl ethylphosphonothiolate. gen analog diethyl 2-diethylamino-6-meth- m-(1-Ethylpropyl)phenyl methylcarbamate. yl-4-pyrimidinyl phosphate. S-[2-Ethylsulfinyl)ethyl] O,O-dimethyl O,O-Diethyl O-(2-isoprophyl-4-methyl-6- phosphorothioate and its cholinesterase-in- pyrimidinyl) phosphorothioate. hibiting metabolites, (primarily S-[2- O,O-Diethyl O-[p-(methylsulfinyl)phenyl] (ethyl-sulfonyl)ethyl] O,O-dimethyl phosphorothioate and its cholinesterase-in- phosphorothioate). hibiting metabolites. Fenthion (O,O-dimethyl O-[3-methyl-4- Diethyl 2-pyrazinyl phosphate. (methylthio)phenyl]phosphorothioate and O,O-Diethyl O-2-pyrazinyl phosphorothioate. its cholinesterase-inhibiting metabolites. S-(O,O-Diisopropyl phosphorodithioate) of N- Malathion. (2-mercaptoethyl) benzenesulfonamide N-(Mercaptomethyl)phthalimide S-(O,O-di- S-(O,O-Diisopropyl phosphorodithioate) of N- methyl phosphorodithioate). (2-mercaptoethyl) benzenesulfonamide N-(Mercaptomethyl)phthalimide S-(O,O-di- 2-(Dimethylamino)-5.6-dimethyl-4- methyl phosphorothioate). pyrimidinyl dimethylcarbamate and its Methomyl (S-methyl N- metabolites 5,6-dimethyl-2- [(methylcarbamoyl)oxy]thioacetimidate). (formylmethylamino)-4-pyrimidinyl 1-Methoxycarbonyl-1-propen-2-yl dimethyl dimethylcarbamate and 5,6-dimethyl-2- phosphate and its beta isomer. (methylamino)-4-pyrimidinyl m-(1-Methylbutyl)phenyl methylcarbamate. dimethylcarbamate (both calculated as Methyl parathion. parent). Naled (1,2-dibromo-2,2-dichloroethyl di- Dimethoate (O,O-dimethyl S-(N-methyl- methyl phosphate). carbamoylmethyl) phosphorodithioate). Oxamyl (methyl N′,N′-dimethyl-N- Dimethoate oxygen analog (O,O-dimethyl S- [(methylcarbamoyl)oxy]-1- (N-methylcarbamoylmethyl) thiooxamimidate) phosphorothioate). Parathion.

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Phorate (O,O-diethyl S-(ethylthio)methyl § 180.5 Zero tolerances. phosphorodithioate) and its cholinesterase- inhibiting metabolites. A zero tolerance means that no Phosalone (S-(6-chloro-3-mercaptomethyl)-2- amount of the pesticide chemical may benzoxazolinone) O,O-diethyl remain on the raw agricultural com- phosphorodithioate). modity when it is offered for shipment. Phosphamidon (2-chloro-2-diethylcarbamoyl- A zero tolerance for a pesticide chem- 1-methylvinyl dimethyl phosphate) includ- ical in or on a raw agricultural com- ing all of its related cholinesterase-inhib- modity may be established because, iting compounds. Pirimiphos-methyl O-[2-diethylamino-6- among other reasons: methyl-pyrimidinyl) O,O-dimethyl (a) A safe level of the pesticide chem- phosphorothioate ical in the diet of two different species Ronnel. of warm-blooded animals has not been Schradan (octamethylpyrophosphoramide). reliably determined. Tetraethyl pyrophosphate. (b) The chemical is carcinogenic to O,O,O′,O′-Tetramethyl O,O′-sulfinyldi-p- or has other alarming physiological ef- phenylene phosphorothioate. fects upon one or more of the species of ′ ′ ′ O,O,O ,O -Tetramethyl O,O -thiodi-p-phen- the test animals used, when fed in the ylene phosphorothioate. Tributyl phosphorotritlioite. diet of such animals. S,S,S-Tributyl phosphorothrithioate. (c) The pesticide chemical is toxic, 3,4,5-Trimethylphenyl methylcarbamate and but is normally used at times when, or its isomer 2,3,5-trimethylphenyl in such manner that, fruit, vegetables, methylcarbamate. or other raw agricultural commodities (6) The following pesticides are mem- will not bear or contain it. bers of the class of dinitrophenols: (d) All residue of the pesticide chemical is normally removed through good 2,4-Dinitro-6-octylphenyl crotonate and 2,6- agricultural practice such as washing dinitro-4-octylphenyl crotonate, mixture or brushing or through weathering or of. other changes in the chemical itself, 4,6-Dinitro-o-cresol and its sodium salt. Dinoseb (2-sec-butyl-4,6-dinitrophenol) and prior to introduction of the raw agri- its alkanolamine, ammonium, and sodium cultural commodity into interstate salts. commerce. [41 FR 8969, Mar. 2, 1976] § 180.6 Pesticide tolerances regarding EDITORIAL NOTE: For FEDERAL REGISTER ci- milk, eggs, meat, and/or poultry; tations affecting § 180.3, see the List of CFR statement of policy. Sections Affected, which appears in the (a) When establishing tolerances for Finding Aids section of the printed volume pesticide residues in or on raw agricul- and at www.govinfo.gov. tural commodities, consideration is al- § 180.4 Exceptions. ways given to possible residues of those pesticide chemicals or their conversion The substances listed in this section products entering the diet of man are excepted from the definitions of through the ingestion of milk, eggs, ‘‘pesticide chemical’’ and ‘‘pesticide meat, and/or poultry produced by ani- chemical residue’’ under FFDCA sec- mals fed agricultural products bearing tion 201(q)(3) and are therefore exempt such pesticide residues. In each in- from regulation under FFDCA section stance an evaluation of all available 402(a)(2)(B) and 408. These substances data will result in a conclusion either: are subject to regulation by the Food (1) That finite residues will actually and Drug Administration as food addi- be incurred in these foods from feed use tives under FFDCA section 409. of the raw agricultural commodity in- (a) Inert ingredients in food pack- cluding its byproducts; or aging treated with a pesticide, when (2) That it is not possible to establish such inert ingredients are the compo- with certainty whether finite residues nents of the food packaging material will be incurred, but there is a reason- (e.g. paper and paperboard, coatings, able expectation of finite residues; or adhesives, and polymers). (3) That it is not possible to establish (b) [Reserved] with certainty whether finite residues [63 FR 10720, Mar. 4, 1998, as amended at 73 will be incurred, but there is no reason- FR 54976, Sept. 24, 2008] able expectation of finite residues.

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(b) When the data show that finite of the pesticide residue and of the un- residues will actually be incurred in likelihood of such residue exceeding milk, eggs, meat, and/or poultry, a tol- the tolerance. The analytical methods erance will be established on the raw to be used for enforcement purposes agricultural commodity used as feed will be those set forth in the ‘‘Pesticide provided that tolerances can be estab- Analytical Manual’’ (see § 180.101(c)). lished at the same time, on the basis of The sensitivities of these methods are the toxicological and other data avail- expressed in that manual. able, for the finite residues incurred in milk, eggs, meat, and/or poultry. When Subpart B—Procedural it is not possible to determine with certainty whether finite residues will be Regulations incurred in milk, eggs, meat, and/or § 180.7 Petitions proposing tolerances poultry but there is a reasonable expec- or exemptions for pesticide resi- tation of finite residues in light of data dues in or on raw agricultural com- reflecting exaggerated pesticides levels modities or processed foods. in feeding studies, a tolerance will be (a) Petitions to be filed with the established on the raw agricultural Agency under the provisions of FFDCA commodity provided that appropriate section 408(d) shall be submitted in du- tolerances can be established at the plicate. If any part of the material sub- same time, on the basis of the toxi- mitted is in a foreign language, it shall cological and other data available, for the finite residues likely to be incurred be accompanied by an accurate and in these foods through the feed use of complete English translation. The peti- the raw agricultural commodity or its tion shall be accompanied by an ad- byproducts. When it is not possible to vance deposit for fees described in determine with certainty whether fi- § 180.33. The petition shall state the pe- nite residues will be incurred in milk, titioner’s mail address to which notice eggs, meat, and/or poultry but there is of objection under FFDCA section no reasonable expectation of finite res- 408(g)(2) may be sent. The petition idues in light of data such as those re- must be signed by the petitioner or by flecting exaggerated pesticide levels in his attorney or agent, or (if a corpora- feeding studies and those elucidating tion) by an authorized official. the biochemistry of the pesticide (b) Petitions shall include the fol- chemical in the animal, a tolerance lowing information: may be established on the raw agricul- (1) An informative summary of the tural commodity without the necessity petition and of the data, information, of a tolerance on food products derived and arguments submitted or cited in from the animal. support of the petition. Both a paper (c) The principles outlined in para- and electronic copy of the summary graphs (a) and (b) of this section will should be submitted. The electronic also be followed with respect to toler- copy should be formatted according to ances for residues which will actually the Office of Pesticide Programs’ cur- be incurred or are reasonably to be ex- rent standard for electronic data sub- pected in milk, eggs, meat, and/or poul- mission as specified at http:// try by the use of pesticides directly on www.epa.gov/pesticides/regulating/reg- the animal or administered purposely istering/submissions/index.htm. in the feed or drinking water. (2) A statement that the petitioner (d) Tolerances contemplated by para- agrees that such summary or any in- graphs (a) and (b) of this section will in formation it contains may be published addition to toxicological consider- as a part of the notice of filing of the ations be conditioned on the avail- petition to be published under FFDCA ability of a practicable analytical section 408(d)(3) and as a part of a pro- method to determine the pesticide res- posed or final regulation issued under idue; that is, the method must be sen- FFDCA section 408. sitive and reliable at the tolerance (3) The name, chemical identity, and level or in special cases at a higher composition of the pesticide chemical level where such level is deemed satis- residue and of the pesticide chemical factory and safe in light of the toxicity that produces the residue.

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(4) Data showing the recommended (15) Such other data and information amount, frequency, method, and time as the Administrator requires by regu- of application of the pesticide chem- lation to support the petition. ical. (16) Reasonable grounds in support of (5) Full reports of tests and inves- the petition. tigations made with respect to the (c) The data specified under para- safety of the pesticide chemical, in- graphs (b)(1) through (b)(16) of this sec- cluding full information as to the tion should be on separate sheets or methods and controls used in con- sets of sheets, suitably identified. If ducting those tests and investigations. such data have already been submitted (6) Full reports of tests and inves- with an earlier application, the present tigations made with respect to the na- petition may incorporate it by ref- ture and amount of the pesticide chem- erence to the earlier one. ical residue that is likely to remain in (d) Except as noted in paragraph (e) or on the food, including a description of this section, a petition shall not be of the analytical methods used. (See accepted for filing if any of the data § 180.34 for further information about prescribed by FFDCA section 408(d) are residue tests.) lacking or are not set forth so as to be (7) Proposed tolerances for the pes- readily understood. The availability to ticide chemical residue if tolerances the public of information provided to, are proposed. or otherwise obtained by, the Agency (8) Practicable methods for removing under this part shall be governed by any amount of the residue that would part 2 of this chapter. The Adminis- exceed any proposed tolerance. trator shall make the full text of the (9) A practical method for detecting summary referenced in paragraph (b)(1) and measuring the levels of the pes- of this section available to the public ticide chemical residue in or on the in the public docket at http:// food, or for exemptions, a statement www.regulations.gov no later than pub- why such a method is not needed. lication in the FEDERAL REGISTER of (10) If the petition relates to a toler- the notice of the petition filing. ance for a processed food, reports of in- (e) The Administrator shall notify vestigations conducted using the proc- the petitioner within 15 days after its essing method(s) used to produce that receipt of acceptance or nonacceptance food. of a petition, and if not accepted the (11) Such information as the Admin- reasons therefor. If petitioner desires, istrator may require to make the de- the petitioner may supplement a defi- termination under FFDCA section cient petition after notification as to 408(b)(2)(C). deficiencies. If the petitioner does not (12) Such information as the Admin- wish to supplement or explain the peti- istrator may require on whether the tion and requests in writing that it be pesticide chemical may have an effect filed as submitted, the petition shall be in humans that is similar to an effect filed and the petitioner so notified. produced by a naturally occurring es- (f) A notice of the filing of a petition trogen or other endocrine effects. for a pesticide chemical residue toler- (13) Information regarding exposure ance that the Administrator deter- to the pesticide chemical residue due mines has met the requirements of to any tolerance or exemption already paragraph (b) of this section shall be granted for such residue. published in the FEDERAL REGISTER by (14) Information concerning any max- the Administrator within 30 days after imum residue level established by the such determination. The notice shall Codex Alimentarius Commission for state the name of the pesticide chem- the pesticide chemical residue ad- ical residue and the commodities for dressed in the petition. If a Codex max- which a tolerance is sought and an- imum residue level has been estab- nounce the availability of a description lished for the pesticide chemical res- of the analytical methods available to idue and the petitioner does not pro- the Administrator for the detection pose that this level be adopted, a state- and measurement of the pesticide ment explaining the reasons for this chemical residue with respect to which departure from the Codex level. the petition is filed or shall set forth

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the petitioner’s statement of why such petitioner. This may be due to the fact a method is not needed. The notice that the data are not sufficiently clear shall explicitly reference the specific or complete. In such cases, the peti- docket identification number in the tioner may withdraw the petition pend- public docket at http:// ing its clarification or the obtaining of www.regulations.gov where the full text additional data. This withdrawal may of the summary required in paragraph be without prejudice to a future filing. (b) of this section is located, and refer A deposit for fees as specified in § 180.33 interested parties to this document for shall accompany the resubmission of further information on the petition. the petition. The full text of the summary may be omitted from the notice. [70 FR 33361, June 8, 2005] (g) The Administrator may request a § 180.9 Substantive amendments to pe- sample of the pesticide chemical at any titions. time while a petition is under consideration. The Administrator shall specify After a petition has been filed, the in its request for a sample of the pes- petitioner may submit additional in- ticide chemical, a quantity which it formation or data in support thereof, deems adequate to permit tests of ana- but in such cases the petition will be lytical methods used to determine resi- given a new filing date. dues of the pesticide chemical and of [70 FR 33361, June 8, 2005] methods proposed by the petitioner for removing any residues of the chemical § 180.29 Establishment, modification, that exceed the tolerance proposed. and revocation of tolerance on ini- (h) The Administrator shall deter- tiative of Administrator. mine, in accordance with the Act, (a) Upon the Administrator’s own ini- whether to issue an order that estab- tiative, the Administrator may pro- lishes, modifies, or revokes a tolerance pose, under FFDCA section 408(e), the regulation (whether or not in accord issuance of a regulation establishing a with the action proposed by the peti- tolerance for a pesticide chemical or tioner), whether to publish a proposed exempting it from the necessity of a tolerance regulation and request public tolerance, or a regulation modifying or comment thereon under § 180.29, or revoking an existing tolerance or ex- whether to deny the petition. The Ad- emption. ministrator shall publish in the FED- (b) The Administrator shall provide a ERAL REGISTER such order or proposed period of not less than 60 days for per- regulation. After receiving comments sons to comment on the proposed regu- on any proposed regulation, the Ad- lation, except that a shorter period for ministrator may issue an order that es- comment may be provided if the Ad- tablishes, modifies, or revokes a toler- ministrator for good cause finds that it ance regulation. An order published would be in the public interest to do so under this section shall describe briefly and states the reasons for the finding how to submit objections and requests in the notice of proposed rulemaking. for a hearing under part 178 of this (c) After reviewing any timely com- chapter. A regulation issued under this ments received, the Administrator may section shall be effective on the date of by order establish, modify, or revoke a publication in the FEDERAL REGISTER tolerance regulation, which order and unless otherwise provided in the regu- regulation shall be published in the lation. FEDERAL REGISTER. An order published under this section shall state that per- [70 FR 33360, June 8, 2005, as amended at 73 sons may submit objections and re- FR 75600, Dec. 12, 2008] quests for a hearing in the manner de- § 180.8 Withdrawal of petitions with- scribed in part 178 of this chapter. out prejudice. (d) Any final regulation issued under In some cases the Administrator will this section shall be effective on the notify the petitioner that the petition, date of publication in the FEDERAL while technically complete, is inad- REGISTER unless otherwise provided in equate to justify the establishment of a the regulation. tolerance or the tolerance requested by [70 FR 33361, June 8, 2005]

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§ 180.30 Judicial review. (b) Any issue as to which review is or was obtainable under paragraph (a) of (a) Under FFDCA section 408(h), judi- this section shall not be the subject of cial review is available in the United judicial review under any other provi- States Courts of Appeal as to the fol- sion of law. In part, this means that, lowing actions: for the Agency actions subject to the (1) Regulations establishing general objection procedure in FFDCA section procedures and requirements under 408(g)(2), judicial review is not avail- FFDCA section 408(e)(1)(C). able unless an adversely affected party (2) Orders issued under FFDCA sec- exhausts these objection procedures, tion 408(f)(1)(C) requiring the submis- and any petition procedures prelimi- sion of data. nary thereto. (3) Orders issued under FFDCA section 408(g)(2)(C) ruling on objections to [70 FR 33362, June 8, 2005] establishment, modification, or revoca- § 180.31 Temporary tolerances. tion of a tolerance or exemption under FFDCA section 408(d)(4), or any regula- (a) A temporary tolerance (or exemption that is the subject of such an tion from a tolerance) established order. The underlying action here is under the authority of FFDCA section Agency disposition of a petition seek- 408(r) shall be deemed to be a tolerance ing the establishment, modification, or (or exemption from the requirement of revocation of a tolerance or exemption. a tolerance) for the purposes of FFDCA section 408(a)(1) or (a)(2) and for the (4) Orders issued under FFDCA sec- purposes of § 180.30. tion 408(g)(2)(C) ruling on objections to (b) A request for a temporary toler- the denial of a petition under FFDCA ance or a temporary exemption from a section 408(d)(4). tolerance by a person who has obtained (5) Orders issued under FFDCA sec- or is seeking an experimental permit tion 408(g)(2)(C) ruling on objections to for a pesticide chemical under the Fed- the establishment, modification, sus- eral Insecticide, Fungicide, and pension, or revocation of a tolerance or Rodenticide Act shall be accompanied exemption under FFDCA section by such data as are available on sub- 408(e)(1)(A) or (e)(1)(B). The underlying jects outlined in § 180.7(b) and an ad- action here is the establishment, modi- vance deposit to cover fees as provided fication, suspension, or revocation of a in § 180.33. tolerance or exemption upon the initia- (c) To obtain a temporary tolerance, tive of EPA including EPA actions pur- a requestor must comply with the peti- suant to FFDCA sections tion procedures specified in FFDCA 408(b)(2)(B)(v), 408(b)(2)(E)(ii), section 408(d) and § 180.7 except as pro- 408(d)(4)(C)(ii), 408(l)(4), and 408(q)(1). vided in this section. (6) Orders issued under FFDCA sec- (d) A temporary tolerance or exemption 408(g)(2)(C) ruling on objections to tion from a tolerance may be issued for the revocation or modification of a tol- a period designed to allow the orderly erance or exemption under FFDCA sec- marketing of the raw agricultural com- tion 408(f)(2) for noncompliance with modities produced while testing a pes- requirements for the submission of ticide chemical under an experimental data. permit issued under authority of the (7) Orders issued under FFDCA sec- Federal Insecticide, Fungicide, and tion 408(g)(2)(C) ruling on objections to Rodenticide Act if the Administrator rules issued under FFDCA sections concludes that the safety standard in 408(n)(3) and 408(d) or (e) regarding de- FFDCA section 408(b)(2) or (c), as appli- terminations pertaining to State au- cable, is met. Subject to the require- thority to establish regulatory limits ments of FFDCA section 408(e), a tem- on pesticide chemical residues. porary tolerance or exemption from a (8) Orders issued under FFDCA sec- tolerance may be revoked if the experi- tion 408(g)(2)(C) ruling on objections to mental permit is revoked, or may be orders issued under FFDCA section revoked at any time if it develops that 408(n)(5)(C) authorizing States to estab- the application for a temporary toler- lish regulatory limits not identical to ance contains a misstatement of a ma- certain tolerances or exemptions. terial fact or that new scientific data

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or experience with the pesticide chem- ported by data if available) showing ical indicates that it does not meet the that new uses for the pesticide chem- safety standard in FFDCA section ical have been developed or old uses 408(b)(2) or (c), as applicable. abandoned, that new data are available (e) Conditions under which a tem- as to toxicity of the chemical, or that porary tolerance is established shall in- experience with the application of the clude: tolerance or exemption from tolerance (1) A limitation on the amount of the may justify its modification or revoca- chemical to be used on the designated tion. Evidence that a person has reg- crops permitted under the experi- istered or has submitted an application mental permit. for the registration of a pesticide under (2) A limitation for the use of the the Federal Insecticide, Fungicide, and chemical on the designated crops to Rodenticide Act will be regarded as bona fide experimental use by qualified evidence that the person has a substan- persons as indicated in the experi- tial interest in a tolerance or exemp- mental permit. tion from the requirement of a toler- (3) A requirement that the person or ance for a pesticide chemical that con- firm which obtains the experimental sists in whole or in part of the pes- permit for which the temporary toler- ticide. New data should be furnished in ance is established will immediately the form specified in § 180.7(b) for sub- inform the Environmental Protection mitting petitions, as applicable. Agency of any reports on findings from (c) The procedures for completing ac- the experimental use that have a bear- tion on an Administrator initiated pro- ing on safety. posal or a petition shall be those speci- (4) A requirement that the person or fied in §§ 180.29 and 180.7, as applicable. firm which obtained the experimental permit for which the temporary toler- [70 FR 33362, June 8, 2005] ance is established will keep records of production, distribution, and perform- § 180.33 Fees. ance for a period of 2 years and, on re- (a) Each petition for the establish- quest, at any reasonable time, make ment of a new tolerance or a tolerance these records available to any author- higher than already established, shall ized officer or employee of the Environ- be accompanied by a fee of $80,950, plus mental Protection Agency. $2,025 for each raw agricultural com- [70 FR 33362, June 8, 2005] modity more than nine on which the establishment of a tolerance is re- § 180.32 Procedure for modifying and quested, except as provided in para- revoking tolerances or exemptions graphs (b), (d), and (h) of this section. from tolerances. (b) Each petition for the establish- (a) The Administrator on his/her own ment of a tolerance at a lower numer- initiative may propose the issuance of ical level or levels than a tolerance al- a regulation modifying or revoking a ready established for the same pes- tolerance for a pesticide chemical res- ticide chemical, or for the establish- idue on raw agricultural commodities ment of a tolerance on additional raw or processed foods or modifying or re- agricultural commodities at the same voking an exemption from tolerance numerical level as a tolerance already for such residue. established for the same pesticide (b) Any person may file with the Ad- chemical, shall be accompanied by a ministrator a petition proposing the fee of $18,500 plus $1,225 for each raw issuance of a regulation modifying or agricultural commodity on which a tol- revoking a tolerance or exemption erance is requested. from a tolerance for a pesticide chem- (c) Each petition for an exemption ical residue. The petition shall furnish from the requirement of a tolerance or reasonable grounds for the action repeal of an exemption shall be accom- sought. Reasonable grounds shall in- panied by a fee of $14,925. clude an explanation showing wherein (d) Each petition or request for a the person has a substantial interest in temporary tolerance or a temporary such tolerance or exemption from tol- exemption from the requirement of a erance and an assertion of facts (sup- tolerance shall be accompanied by a fee

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of $32,325 except as provided in para- (k) No fee under this section will be graph (e) of this section. A petition or imposed on the Interregional Research request to renew or extend such tem- Project Number 4 (IR-4 Program). porary tolerance or temporary exemp- (l) The Administrator may waive or tion shall be accompanied by a fee of refund part or all of any fee imposed by $4,600. this section if the Administrator deter- (e) A petition or request for a tem- mines in his or her sole discretion that porary tolerance for a pesticide chem- such a waiver or refund will promote ical which has a tolerance for other the public interest or that payment of uses at the same numerical level or a the fee would work an unreasonable higher numerical level shall be accom- hardship on the person on whom the panied by a fee of $16,075, plus $1,225 for fee is imposed. A request for waiver or each raw agricultural commodity on refund of a fee shall be submitted to which the temporary tolerance is the Office of Pesticide Programs’ Docu- sought. ment Processing Desk at the appro- (f) Each petition for revocation of a priate address as set forth in 40 CFR tolerance shall be accompanied by a fee 150.17(a) or (b). A fee of $2,025 shall ac- of $10,125. Such fee is not required company every request for a waiver or when, in connection with the change refund, as specified in paragraph (m) of sought under this paragraph, a petition this section, except that the fee under is filed for the establishment of new this paragraph shall not be imposed on tolerances to take the place of those any person who has no financial inter- sought to be revoked and a fee is paid est in any action requested by such as required by paragraph (a) of this sec- person under paragraphs (a) through (j) tion. of this section. The fee for requesting a (g) If a petition or a request is not ac- waiver or refund shall be refunded if cepted for processing because it is the request is granted. technically incomplete, the fee, less (m) All deposits and fees required by $2,025 for handling and initial review, the regulations in this part shall be shall be returned. If a petition is with- paid by money order, bank draft, or drawn by the petitioner after initial certified check drawn to the order of processing, but before significant Agen- the Environmental Protection Agency. cy scientific review has begun, the fee, All deposits and fees shall be forwarded less $2,025 for handling and initial re- to the Environmental Protection Agen- view, shall be returned. If an unaccept- cy, Headquarters Accounting Oper- able or withdrawn petition is resub- ations Branch, Office of Pesticide Pro- mitted, it shall be accompanied by the grams (Tolerance Fees), P.O. Box fee that would be required if it were 360277M, Pittsburgh, PA 15251. The pay- being submitted for the first time. ments should be specifically labeled (h) Each petition for a crop group tol- ‘‘Tolerance Petition Fees’’ and should erance, regardless of the number of raw be accompanied only by a copy of the agricultural commodities involved, letter or petition requesting the toler- shall be accompanied by a fee equal to ance. The actual letter or petition, the fee required by the analogous cat- along with supporting data, shall be egory for a single tolerance that is not forwarded within 30 days of payment to a crop group tolerance, i.e., paragraphs the Office of Pesticide Programs’ Docu- (a) through (f) of this section, without ment Processing Desk at the appro- a charge for each commodity where priate address as set forth in 40 CFR that would otherwise apply. 150.17(a) or (b). A petition will not be (i) Objections under section 408(d)(5) accepted for processing until the re- of the Act shall be accompanied by a quired fees have been submitted. A pe- filing fee of $4,050. tition for which a waiver of fees has (j) The person who files a petition for been requested will not be accepted for judicial review of an order under sec- processing until the fee has been tion 408(h) of the Act shall pay the waived or, if the waiver has been de- costs of preparing the record on which nied, the proper fee is submitted after the order is based unless the person has notice of denial. A request for waiver no financial interest in the petition for or refund will not be accepted after sci- judicial review. entific review has begun on a petition.

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(n) This fee schedule will be changed commodity in the group, considered annually by the same percentage as the separately. percent change in the Federal General (e) Each of the following groups of Schedule (GS) pay scale. In addition, crops lists raw agricultural commod- processing costs and fees will periodi- ities that are considered to be related cally be reviewed and changes will be for the purpose of paragraph (d) of this made to the schedule as necessary. section. Commodities not listed in this When automatic adjustments are made paragraph are not considered to be re- based on the GS pay scale, the new fee lated for the purpose of paragraph (d) schedule will be published in the FED- of this section. ERAL REGISTER as a final rule to be- (1) Apples, crabapples, pears, quinces. come effective 30 days or more after (2) Avocados, papayas. publication, as specified in the rule. (3) Blackberries, boysenberries, When changes are made based on peri- dewberries, loganberries, raspberries. odic reviews, the changes will be sub- (4) Blueberries, currants, goose- ject to public comment. berries, huckleberries. (o) No fee required by this section (5) Cherries, plums, prunes. shall be levied during the period begin- (6) Oranges, citrus citron, grapefruit, ning on October 1, 2003, and ending Sep- kumquats, lemons, limes, tangelos, tember 30, 2008. tangerines. [68 FR 24371, May 7, 2003, as amended at 69 (7) Mangoes, persimmons. FR 12544, Mar. 17, 2004; 70 FR 33363, June 8, (8) Peaches, apricots, nectarines. 2005; 71 FR 35547, June 21, 2006] (9) Beans, peas, soybeans (each in dry form). § 180.34 Tests on the amount of res- (10) Beans, peas, soybeans (each in idue remaining. succulent form). (a) Data in a petition on the amount (11) Broccoli, brussels sprouts, cauli- of residue remaining in or on a raw ag- flower, kohlrabi. ricultural commodity should establish (12) Cantaloups, honeydew melons, the residue that may remain when the muskmelons, pumpkins, watermelons, pesticide chemical is applied according winter squash. to directions registered under the Fed- (13) Carrots, garden beets, sugar eral Insecticide, Fungicide, and beets, horseradish, parsnips, radishes, Rodenticide Act, or according to direc- rutabagas, salsify roots, turnips. tions contained in an application for (14) Celery, fennel. registration. These data should estab- (15) Cucumbers, summer squash. lish the residues that may remain (16) Lettuce, endive (escarole), Chi- under conditions most likely to result nese cabbage, salsify tops. in high residues on the commodity. (17) Onions, garlic, leeks, shallots (b) The petition should establish the (green, or in dry bulb form). reliability of the residue data reported (18) Potatoes, Jerusalem-artichokes, in it. Sufficient information should be sweetpotatoes, yams. submitted about the analytical method (19) Spinach, beet tops, collards, dan- to permit competent analysts to apply delion, kale, mustard greens, parsley, it successfully. Swiss chard, turnip tops, watercress. (c) If the pesticide chemical is ab- (20) Tomatoes, eggplants, peppers, pi- sorbed into a living plant or animal mentos. when applied (is systemic), residue (21) Pecans, almonds, brazil nuts, data may be needed on each plant or bush nuts, butternuts, chestnuts, fil- animal on which a tolerance or exemp- berts, hazelnuts, hickory nuts, wal- tion is requested. nuts. (d) If the pesticide chemical is not (22) Field corn, popcorn, sweet corn absorbed into the living plant or ani- (each in grain form). mal when applied (is not systemic), it (23) Milo, sorghum (each in grain may be possible to make a reliable es- form). timate of the residues to be expected (24) Wheat, barley, oats, rice, rye on each commodity in a group of re- (each in grain form). lated commodities on the basis of less (25) Alfalfa, Bermuda grass, blue- data than would be required for each grass, brome grass, clovers, cowpea

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hay, fescue, lespedeza, lupines, orchard resentative commodities for a specific grass, peanut hay, peavine hay, rye group or subgroup of related commod- grass, soybean hay, sudan grass, tim- ities, a tolerance may be established othy, and vetch. for all commodities in the associated (26) Corn forage, sorghum forage. group or subgroup. Tolerances may be (27) Sugarcane, cane sorghum. established for a crop group or, alter- [36 FR 22540, Nov. 25, 1971, as amended at 39 natively, tolerances may be established FR 28286, Aug. 6, 1974; 39 FR 28977, Aug. 13, for one or more of the subgroups of a 1974; 40 FR 6972, Feb. 18, 1975; 45 FR 82928, crop group. Dec. 17, 1980; 48 FR 29860, June 29, 1983; 60 FR (d) The representative crops are 26635, May 17, 1995; 73 FR 75600, Dec. 12, 2008] given as an indication of the minimum residue chemistry data base acceptable § 180.35 Tests for potentiation. to the Agency for the purposes of es- Experiments have shown that certain tablishing a group tolerance. The cholinesterase-inhibiting pesticides Agency may, at its discretion, allow when fed together to test animals are group tolerances when data on suitable more toxic than the sum of their indi- substitutes for the representative crops vidual toxicities when fed separately. are available (e.g., limes instead of One substance potentiates the toxicity lemons). of the other. Important toxicological (e) Since a group tolerance reflects interactions also have been observed maximum residues likely to occur on between pesticides and other sub- all individual crops within a group, the stances. Wherever there is reason to proposed or registered patterns of use believe that a pesticide chemical for for all crops in the group or subgroup which a tolerance is proposed may must be similar before a group toler- interact with other pesticide chemicals ance is established. The pattern of use or other substances to which man is ex- consists of the amount of pesticide ap- posed, it may be necessary to require plied, the number of times applied, the special experimental data regarding timing of the first application, the in- potentiation capacities to evaluate the terval between applications, and the safety of the proposed tolerance. This interval between the last application necessarily will be determined on a and harvest. The pattern of use will case-by-case basis. also include the type of application; for § 180.40 Tolerances for crop groups. example, soil or foliar application, or application by ground or aerial equip- (a) Group or subgroup tolerances may ment. Additionally, since a group tol- be established as a result of: erance reflects maximum residues like- (1) A petition from a person who has ly to occur on all individual foods with- submitted an application for the reg- in a group, food processing practices istration of a pesticide under the Fed- must be similar for all crops in the eral Insecticide, Fungicide, and Rodenticide Act. group or subgroup if the processing (2) On the initiative of the Adminis- practice has the potential to result in trator. residues in a processed commodity at a (3) A petition by an interested per- higher concentration than the raw ag- son. ricultural commodity. (b) The tables in § 180.41 are to be (f)(1) General. EPA will not establish used in conjunction with this section a crop group for a pesticide unless all for the establishment of crop group tol- tolerances made necessary by the pres- erances. Each table in § 180.41 lists a ence of pesticide residues in the crop group of raw agricultural commodities group commodities have been issued or that are considered to be related for are being issued simultaneously with the purposes of this section. Refer also the crop group tolerance. For purposes to § 180.1(g) for a listing of commodities of paragraph (f)(1): for which established tolerances may (i) Necessary tolerances for residues be applied to certain other related and resulting from crop group tolerances similar commodities. include: (c) When there is an established or (A) Tolerances for processed food, in- proposed tolerance for all of the rep- cluding processed animal feed, to the

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extent needed under FFDCA section unless indicated otherwise in §§ 180.40 408(a)(2). and 180.41, representative commodities (B) Tolerances for raw commodities for such crop groups are selected tak- not covered by the crop group toler- ing into consideration whether their ance that are derivative of commod- use as animal feed will result in resi- ities in the group. dues in or on meat, milk, and/or eggs (C) Tolerances for meat, milk, or egg at a level representative of the residues products that may contain residues as that would result from use of the other a result of livestock’s consumption of commodities or byproducts in the crop animal feed containing pesticide resi- group as an animal feed. dues to the extent needed under (4) Data. Processing data on rep- § 180.6(b). resentative crops are required prior to (ii) Notwithstanding the foregoing, a establishment of a group tolerance if tolerance is not considered necessary the processing of the representative for processed food, derivative raw com- commodity has the potential to result modities, or meat, milk, and eggs if the in residues in a processed commodity precursor raw commodities are grown at a higher concentration than in the solely for sale as raw commodities and representative commodity. Residue are completely segregated from com- data are required on raw commodities modities grown for the purpose of pro- derived from the crops in the crop ducing processed foods, derivative raw group tolerance but not directly cov- commodities, and commodities, or ered by the tolerance. Animal feeding fractions thereof, that are used as ani- studies with a representative crop are mal feed. required if the representative crop is (2) Processed commodity and related used as a significant animal feed. raw commodity crop group tolerances. (g) If maximum residues (tolerances) EPA may establish crop group toler- for the representative crops vary by ances for processed commodities or more than a factor of 5 from the max- fractions of commodities (e.g., bran imum value observed for any crop in and flour from the Cereal Grains the group, a group or subgroup toler- Group), including processed fractions ance will ordinarily not be established. used as animal feed (e.g., pomace from In this case individual crop tolerances, the Pome Fruit Group), produced from rather than group tolerances, will nor- crops in the crop groups in § 180.41. EPA mally be established. may establish crop group tolerances for (h) Alternatively, a commodity with raw commodities or fractions of com- a residue level significantly higher or modities, including fractions used as lower than the other commodities in a animal feed, derived from commodities group may be excluded from the group covered by the crop groups in § 180.41 tolerance (e.g., cereal grains, except (e.g., aspirated grain dust associated corn). In this case an individual toler- with the Cereal Grains Group). Crop ance at the appropriate level for the group tolerances on processed foods unique commodity would be estab- and derivative raw commodities may lished, if necessary. The alternative ap- be based on data on representative proach of excluding a commodity with commodities for associated crop group. a significantly higher or lower residue Paragraphs (c), (d), (e), (g), and (h) of level will not be used to establish a tol- § 180.40 apply to group tolerances au- erance for a commodity subgroup. Most thorized by paragraph (f)(2). subgroups have only two representa- (3) Representative crops. Unless indi- tive commodities; to exclude one such cated otherwise in §§ 180.40 and 180.41, commodity and its related residue data the processed food and feed forms of would likely provide insufficient res- the representative crops for a crop idue information to support the re- group are considered to be representa- mainder of the subgroup. Residue data tive of the processed food and feed from crops additional to those rep- forms and any derivative raw commod- resentative crops in a grouping may be ities not covered by the crop group, required for systemic pesticides. that are produced from any of the raw (i) The commodities included in the agricultural commodities covered by groups will be updated periodically ei- the crop group tolerance. Additionally, ther at the initiative of the Agency or

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at the request of an interested party. panion law, the Federal Insecticide, Persons interested in updating this sec- Fungicide, and Rodenticide Act. The tion should contact the Registration Registration Division of the Office of Division of the Office of Pesticide Pro- Pesticide Programs should be con- grams. tacted concerning procedures for reg- (j) When EPA amends a crop group in istration of new uses of a pesticide. a manner that expands or contracts the [60 FR 26635, May 17, 1995, as amended at 70 commodities that are covered by the FR 33363, June 8, 2005; 72 FR 69155, Dec. 7, group, EPA will initially retain the 2007; 75 FR 56014, Sept. 15, 2010; 81 FR 26476, pre-existing as well as the revised crop May 3, 2016] group in the CFR. The revised crop group will have the same number as § 180.41 Crop group tables. the pre-existing crop group; however, (a) The tables in this section are to the revised crop group number will be be used in conjunction with § 180.40 to followed by a hyphen and the final two establish crop group tolerances. digits of the year in which it was estab- (b) Commodities not listed are not lished (e.g., if Crop Group 1 is amended considered as included in the groups for in 2007, the revised group will be des- the purposes of paragraph (b), and indi- ignated as Crop Group 1-07). If the pre- vidual tolerances must be established. existing crop group had crop sub- Miscellaneous commodities inten- groups, these subgroups will be num- tionally not included in any group in- bered in a similar fashion in the re- clude globe artichoke, hops, peanut, vised crop group. The name of the re- and water chestnut. vised crop group will not be changed (c) Each group is identified by a from the pre-existing crop group unless group name and consists of a list of the revision so changes the composi- representative commodities followed tion of the crop group that the pre-ex- by a list of all commodity members for isting name is no longer accurate. Once the group. If the group includes sub- a revised crop group is established, groups, each subgroup lists the sub- EPA will no longer establish tolerances group name, the representative com- under the pre-existing crop group. At modity or commodities, and the mem- appropriate times, EPA will amend tol- ber commodities for the subgroup. Sub- erances for crop groups that have been groups, which are a subset of their as- superseded by revised crop groups to sociated crop group, are established for conform the pre-existing crop group to some but not all crops groups. the revised crop group. Once all of the (1) Crop Group 1: Root and Tuber tolerances for the pre-existing crop Vegetables Group. group have been updated, the pre-exist- (i) Representative commodities. Carrot, ing crop group will be removed from potato, radish, and sugar beet. the CFR. (ii) Table. The following table 1 lists (k) Establishment of a tolerance does all the commodities included in Crop not substitute for the additional need Group 1 and identifies the related crop to register the pesticide under a com- subgroups.

TABLE 1—CROP GROUP 1: ROOT AND TUBER VEGETABLES

Related crop Commodities subgroups

Arracacha (Arracacia xanthorrhiza) ...... 1C, 1D Arrowroot (Maranta arundinacea) ...... 1C, 1D Artichoke, Chinese (Stachys affinis) ...... 1C, 1D Artichoke, Jerusalem (Helianthus tuberosus) ...... 1C, 1D Beet, garden (Beta vulgaris) ...... 1A, 1B Beet, sugar (Beta vulgaris) ...... 1A Burdock, edible (Arctium lappa) ...... 1A, 1B Canna, edible (Queensland arrowroot) (Canna indica) ...... 1C, 1D Carrot (Daucus carota) ...... 1A, 1B Cassava, bitter and sweet (Manihot esculenta) ...... 1C, 1D Celeriac (celery root) (Apium graveolens var. rapaceum) ...... 1A, 1B Chayote (root) (Sechium edule) ...... 1C, 1D Chervil, turnip-rooted (Chaerophyllum bulbosum)...... 1A, 1B Chicory (Cichorium intybus) ...... 1A, 1B

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TABLE 1—CROP GROUP 1: ROOT AND TUBER VEGETABLES—Continued

Related crop Commodities subgroups

Chufa (Cyperus esculentus) ...... 1C, 1D Dasheen (taro) (Colocasia esculenta) ...... 1C, 1D Ginger (Zingiber officinale) ...... 1C, 1D Ginseng (Panax quinquefolius) ...... 1A, 1B Horseradish (Armoracia rusticana) ...... 1A, 1B Leren (Calathea allouia) ...... 1C, 1D Parsley, turnip-rooted (Petroselinum crispum var. tuberosum) ...... 1A, 1B Parsnip (Pastinaca sativa) ...... 1A, 1B Potato (Solanum tuberosum) ...... 1C Radish (Raphanus sativus) ...... 1A, 1B Radish, oriental (daikon) (Raphanus sativus subvar. longipinnatus) ...... 1A, 1B Rutabaga (Brassica campestris var. napobrassica) ...... 1A, 1B Salsify (oyster plant) (Tragopogon porrifolius)...... 1A, 1B Salsify, black (Scorzonera hispanica) ...... 1A, 1B Salsify, Spanish (Scolymus hispanicus) ...... 1A, 1B Skirret (Sium sisarum) ...... 1A, 1B Sweet potato (Ipomoea batatas) ...... 1C, 1D Tanier (cocoyam) (Xanthosoma sagittifolium) ...... 1C, 1D Turmeric (Curcuma longa) ...... 1C, 1D Turnip (Brassica rapa var. rapa) ...... 1A, 1B Yam bean (jicama, manoic pea) (Pachyrhizus spp.) ...... 1C, 1D Yam, true (Dioscorea spp.) ...... 1C, 1D

(iii) Table. The following table 2 iden- commodity(ies) for each subgroup, and tifies the crop subgroups for Crop lists all the commodities included in Group 1, specifies the representative each subgroup.

TABLE 2—CROP GROUP 1 SUBGROUP LISTING

Representative commodities Commodities

Crop Subgroup 1A. Root vegetables subgroup. Carrot, radish, and sugar beet...... Beet, garden; beet, sugar; burdock, edible; carrot; celeriac; chervil, turnip-rooted; chicory; ginseng; horseradish; parsley, turnip-rooted; parsnip; radish; radish, oriental; rutabaga; salsify; salsify, black; salsify, Spanish; skirret; turnip. Crop Subgroup 1B. Root vegetables (except sugar beet) subgroup. Carrot and radish...... Beet, garden; burdock, edible; carrot; celeriac; chervil, turnip-rooted; chicory; ginseng; horseradish; parsley, turnip-rooted; parsnip; radish; radish, oriental; rutabaga; salsify; salsify, black; salsify, Spanish; skirret; turnip. Crop Subgroup 1C. Tuberous and corm vegetables subgroup. Potato...... Arracacha; arrowroot; artichoke, Chinese; artichoke, Jerusalem; canna, edible; cassava, bitter and sweet; chayote (root); chufa; dasheen; ginger; leren; potato; sweet potato; tanier; turmeric; yam bean; yam, true. Crop Subgroup 1D. Tuberous and corm vegetables (except potato) subgroup. Sweet potato...... Arracacha; arrowroot; artichoke, Chinese; artichoke, Jerusalem; canna, edible; cassava, bitter and sweet; chayote (root); chufa; dasheen; ginger; leren; sweet potato; tanier; turmeric; yam bean; yam, true.

(2) Crop Group 2. Leaves of Root and CROP GROUP 2: LEAVES OF ROOT AND TUBER Tuber Vegetables (Human Food or Ani- VEGETABLES (HUMAN FOOD OR ANIMAL mal Feed) Group (Human Food or Ani- FEED) GROUP—COMMODITIES mal Feed) Group. Beet, garden (Beta vulgaris) (i) Representative commodities. Turnip Beet, sugar (Beta vulgaris) and garden beet or sugar beet. Burdock, edible (Arctium lappa) (ii) Commodities. The following is a Carrot (Daucus carota) list of all the commodities included in Cassava, bitter and sweet (Manihot esculenta) Crop Group 2: Celeriac (celery root) (Apium graveolens var. rapaceum)

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Chervil, turnip-rooted (Chaerophyllum (ii) Commodities. The following is a bulbosum) list of all the commodities in Crop Chicory (Cichorium intybus) Group 3. Dasheen (taro) (Colocasia esculenta) Parsnip (Pastinaca sativa) CROP GROUP 3: BULB VEGETABLE (Allium SPP.) Radish (Raphanus sativus) GROUP—COMMODITIES Radish, oriental (daikon) (Raphanus sativus Garlic, bulb (Allium sativum) subvar. longipinnatus) Garlic, great headed, (elephant) (Allium ampeloprasum var. Rutabaga (Brassica campestris var. ampeloprasum) Leek (Allium ampeloprasum, A. porrum, A. tricoccum) napobrassica) Onion, dry bulb and green (Allium cepa, A. fistulosum) Salsify, black (Scorzonera hispanica) Onion, Welsh, (Allium fistulosum) Sweet potato (Ipomoea batatas) Shallot (Allium cepa var. cepa) Tanier (cocoyam) (Xanthosoma sagittifolium) (4) Crop Group 3-07. Bulb Vegetable Turnip (Brassica rapa var. rapa) Group. Yam, true (Dioscorea spp.) (i) Representative Commodities. Onion, (3) Crop Group 3. Bulb Vegetables bulb and onion, green. (Allium spp.) Group. (ii) Table. The following Table 1 lists (i) Representative commodities. Onion, all the commodities listed in Crop green; and onion, dry bulb. Group 3-07 and identifies the related crop subgroups.

TABLE 1—CROP GROUP 3-07: BULB VEGETABLE GROUP

Commodities Related crop subgroups

Chive, fresh leaves (Allium schoenoprasum L.) ...... 3-07B Chive, Chinese, fresh leaves (Allium tuberosum Rottler ex Spreng) ...... 3-07B Daylily, bulb (Hemerocallis fulva (L.) L. var. fulva) ...... 3-07A Elegans hosta (Hosta Sieboldiana (Hook.) Engl) ...... 3-07B Fritillaria, bulb (Fritillaria L. fritillary) ...... 3-07A Fritillaria, leaves (Fritillaria L. fritillary) ...... 3-07B Garlic, bulb (Allium sativum L. var. sativum) (A. sativum Common Garlic Group) ...... 3-07A Garlic, great headed, bulb (Allium ampeloprasum L. var. ampeloprasum) (A. ampeloprasum Great Headed Garlic Group) ...... 3-07A Garlic, Serpent, bulb (Allium sativum var. ophioscorodon or A. sativum Ophioscorodon Group) ...... 3-07A Kurrat (Allium kurrat Schweinf. Ex. K. Krause or A. ampeloprasum Kurrat Group) ...... 3-07B Lady’s leek (Allium cernuum Roth) ...... 3-07B Leek Allium porrum L. (syn: A. ampeloprasum L. var. porrum (L.) J. Gay) (A.ampeloprasum Leek Group) ...... 3-07B Leek, wild (Allium tricoccum Aiton) ...... 3-07B Lily, bulb (Lilium spp. (Lilium Leichtlinii var. maximowiczii, Lilium lancifolium)) ...... 3-07A Onion, Beltsville bunching (Allium x proliferum (Moench) Schrad.) (syn: Allium fistulosum L. x A. cepa L.) ...... 3-07B Onion, bulb (Allium cepa L. var. cepa) (A. cepa Common Onion Group) ...... 3-07A Onion, Chinese, bulb (Allium chinense G. Don.) (syn: A. bakeri Regel) ...... 3-07A Onion, fresh (Allium fistulosum L. var. caespitosum Makino) ...... 3-07B Onion, green (Allium cepa L. var. cepa) (A. cepa Common Onion Group) ...... 3-07B Onion, macrostem (Allium macrostemom Bunge) ...... 3-07B Onion, pearl (Allium porrum var. sectivum or A. ampeloprasum Pearl Onion Group) ...... 3-07A Onion, potato, bulb (Allium cepa L. var. aggregatum G. Don.) (A. cepa Aggregatum Group) ...... 3-07A Onion, tree, tops (Allium x proliferum (Moench) Schrad. ex Willd.) (syn: A. cepa var. proliferum (Moench) Regel; A. cepa L. var. bulbiferum L.H. Bailey; A. cepa L. var. viviparum (Metz.) Alef.) ...... 3-07B Onion, Welsh, tops (Allium fistulosum L.) ...... 3-07B Shallot, bulb (Allium cepa var. aggregatum G. Don.) ...... 3-07A Shallot, fresh leaves (Allium cepa var. aggregatum G. Don.) ...... 3-07B Cultivars, varieties, and/or hybrids of these......

(iii) Table. The following Table 2 commodities for each subgroup and identifies the crop subgroups for Crop lists all the commodities included in Group 3-07, specifies the representative each subgroup.

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TABLE 2—CROP GROUP 3-07: SUBGROUP LISTING

Representative commodities Commodities

Crop subgroup 3-07A. Onion, bulb, sub- Daylily, bulb; fritillaria, bulb; garlic, bulb; garlic, great-headed, bulb; garlic, serpent, group. bulb; lily, bulb; onion, bulb; onion, Chinese, bulb; onion, pearl; onion, potato, Onion, bulb...... bulb; shallot, bulb; cultivars, varieties, and/or hybrids of these. Crop subgroup 3-07B. Onion, green, sub- Chive, fresh leaves; chive, Chinese, fresh leaves; elegans hosta; fritillaria, leaves; group. kurrat; lady’s leek; leek; leek, wild; Onion, Beltsville bunching; onion, fresh; Onion, green...... onion, green; onion, macrostem; onion, tree, tops; onion, Welsh, tops; shallot, fresh leaves; cultivars, varieties, and/or hybrids of these.

(5) Crop Group 4. Leafy Vegetables (ii) Table. The following table 1 lists (Except Brassica Vegetables) Group. all the commodities included in Crop (i) Representative commodities. Celery, Group 4 and identifies the related crop head lettuce, leaf lettuce, and spinach subgroups. (Spinacia oleracea).

TABLE 1—CROP GROUP 4: LEAFY VEGETABLES (EXCEPT BRASSICA VEGETABLES) GROUP

Related crop Commodities subgroups

Amaranth (leafy amaranth, Chinese spinach, tampala) (Amaranthus spp.) ...... 4A Arugula (Roquette) (Eruca sativa) ...... 4A Cardoon (Cynara cardunculus) ...... 4B Celery (Apium graveolens var. dulce) ...... 4B Celery, Chinese (Apium graveolens var. secalinum) ...... 4B Celtuce (Lactuca sativa var. angustana) ...... 4B Chervil (Anthriscus cerefolium) ...... 4A Chrysanthemum, edible-leaved (Chrysanthemum coronarium var. coronarium) ...... 4A Chrysanthemum, garland (Chrysanthemum coronarium var. spatiosum) ...... 4A Corn salad (Valerianella locusta) ...... 4A Cress, garden (Lepidium sativum) ...... 4A Cress, upland (yellow rocket, winter cress) (Barbarea vulgaris) ...... 4A Dandelion (Taraxacum officinale) ...... 4A Dock (sorrel) (Rumex spp.) ...... 4A Endive (escarole) (Cichorium endivia) ...... 4A Fennel, Florence (finochio) (Foeniculum vulgare Azoricum Group) ...... 4B Lettuce, head and leaf (Lactuca sativa) ...... 4A Orach (Atriplex hortensis) ...... 4A Parsley (Petroselinum crispum) ...... 4A Purslane, garden (Portulaca oleracea) ...... 4A Purslane, winter (Montia perfoliata) ...... 4A Radicchio (red chicory) (Cichorium intybus) ...... 4A Rhubarb (Rheum rhabarbarum) ...... 4B Spinach (Spinacia oleracea) ...... 4A Spinach, New Zealand (Tetragonia tetragonioides, T. expansa) ...... 4A Spinach, vine (Malabar spinach, Indian spinach) (Basella alba) ...... 4A Swiss chard (Beta vulgaris var. cicla) ...... 4B

(iii) Table. The following table 2 iden- commodities for each subgroup, and tifies the crop subgroups for Crop lists all the commodities included in Group 4, specifies the representative each subgroup.

TABLE 2—CROP GROUP 4 SUBGROUP LISTING

Representative commodities Commodities

Crop Subgroup 4A. Leafy greens subgroup. Head lettuce and leaf lettuce, and spinach Amaranth; arugula; chervil; chrysanthemum, edible-leaved; chrysanthemum, (Spinacia oleracea). garland; corn salad; cress, garden; cress, upland; dandelion; dock; endive; lettuce; orach; parsley; purslane, garden; purslane, winter; radicchio (red chicory); spinach; spinach, New Zealand; spinach, vine. Crop Subgroup 4B. Leaf petioles subgroup. Celery...... Cardoon; celery; celery, Chinese; celtuce; fennel, Florence; rhubarb; Swiss chard.

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(6) Crop Group 4–16. Leafy Vegetable (ii) Commodities. The following Table Group. 1 lists all commodities included in Crop (i) Representative commodities. Head Group 4–16. lettuce, leaf lettuce, mustard greens, and spinach.

TABLE 1—CROP GROUP 4–16: LEAFY VEGETABLE GROUP

Related crop sub- Commodities groups

Amaranth, Chinese (Amaranthus tricolor L.) ...... 4–16A Amaranth, leafy (Amaranthus spp.) ...... 4–16A Arugula (Eruca sativa Mill.) ...... 4–16B Aster, Indian (Kalimeris indica (L.) Sch. Bip.) ...... 4–16A Blackjack (Bidens pilosa L.) ...... 4–16A Broccoli, Chinese (Brassica oleracea var. alboglabra (L.H. Bailey) Musil) ...... 4–16B Broccoli raab (Brassica ruvo L.H. Bailey) ...... 4–16B Cabbage, abyssinian (Brassica carinata A. Braun) ...... 4–16B Cabbage, Chinese, bok choy (Brassica rapa subsp. chinensis (L.) Hanelt) ...... 4–16B Cabbage, seakale (Brassica oleracea L. var. costata DC.) ...... 4–16B Cat’s whiskers (Cleome gynandra L.) ...... 4–16A Cham-chwi (Doellingeria scabra (Thunb.) Nees) ...... 4–16A Cham-na-mul (Pimpinella calycina Maxim) ...... 4–16A Chervil, fresh leaves (Anthriscus cerefolium (L.) Hoffm.) ...... 4–16A Chipilin (Crotalaria longirostrata Hook & Arn) ...... 4–16A Chrysanthemum, garland (Glebionis coronaria (L.) Cass. ex Spach. Glebionis spp.) ...... 4–16A Cilantro, fresh leaves (Coriandrum sativum L.) ...... 4–16A Collards (Brassica oleracea L. var. viridis L.) ...... 4–16B Corn salad (Valerianella spp.) ...... 4–16A Cosmos (Cosmos caudatus Kunth) ...... 4–16A Cress, garden (Lepidium sativum L.) ...... 4–16B Cress, upland (Barbarea vulgaris W.T. Aiton) ...... 4–16B Dandelion, leaves (Taraxacum officinale F.H. Wigg. Aggr.) ...... 4–16A Dang-gwi, leaves (Angelica gigas Nakai) ...... 4–16A Dillweed (Anethum graveolens L.) ...... 4–16A Dock (Rumex patientia L.) ...... 4–16A Dol-nam-mul (Sedum sarmentosum Bunge) ...... 4–16A Ebolo (Crassocephalum crepidioides (Benth.) S. Moore) ...... 4–16A Endive (Cichorium endivia L.) ...... 4–16A Escarole (Cichorium endivia L.) ...... 4–16A Fameflower (Talinum fruticosum (L.) Juss.) ...... 4–16A Feather cockscomb (Glinus oppositifolius (L.) Aug. DC.) ...... 4–16A Good King Henry (Chenopodium bonus-henricus L.) ...... 4–16A Hanover salad (Brassica napus var. pabularia (DC.) Rchb.) ...... 4–16B Huauzontle (Chenopodium berlandieri Moq.) ...... 4–16A Jute, leaves (Corchorus spp.) ...... 4–16A Kale (Brassica oleracea L. var. Sabellica L.) ...... 4–16B Lettuce, bitter (Launaea cornuta (Hochst. ex Oliv. & Hiern) C. Jeffrey) ...... 4–16A Lettuce, head (Lactuca sativa L.; including Lactuca sativa var. capitata L.) ...... 4–16A Lettuce, leaf (Lactuca sativa L.; including Lactuca sativa var. longifolia Lam.; Lactuca sativa var. crispa L.) .. 4–16A Maca, leaves (Lepidium meyenii Walp.) ...... 4–16B Mizuna (Brassica rapa L. subsp. nipposinica (L.H. Bailey) Hanelt) ...... 4–16B Mustard greens (Brassica juncea subsp., including Brassica juncea (L.) Czern. subsp. integrifolia (H. West) Thell., Brassica juncea (L.) Czern. var. tsatsai (T.L. Mao) Gladis) ...... 4–16B Orach (Atriplex hortensis L.) ...... 4–16A Parsley, fresh leaves (Petroselinum crispum (Mill.) Fuss; Petroselinum crispum var. neapolitanum Danert) ... 4–16A Plantain, buckthorn (Plantago lanceolata L.) ...... 4–16A Primrose, English (Primula vulgaris Huds.) ...... 4–16A Purslane, garden (Portulaca oleracea L.) ...... 4–16A Purslane, winter (Claytonia perfoliata Donn ex Willd.) ...... 4–16A Radicchio (Cichorium intybus L.) ...... 4–16A Radish, leaves (Raphanus sativus L. var sativus, including Raphanus sativus L. var. mougri H. W. J. Helm (Raphanus sativus L. var. oleiformis Pers) ...... 4–16B Rape greens (Brassica napus L. var. napus, including Brassica rapa subsp. trilocularis (Roxb.) Hanelt; Brassica rapa subsp. dichotoma (Roxb.) Hanelt; Brassica rapa subsp. oleifera Met) ...... 4–16B Rocket, wild (Diplotaxis tenuifolia (L.) DC.) ...... 4–16B Shepherd’s purse (Capsella bursa-pastoris (L.) Medik) ...... 4–16B Spinach (Spinacia oleracea L.) ...... 4–16A Spinach, Malabar (Basella alba L.) ...... 4–16A Spinach, New Zealand (Tetragonia tetragonioides (Pall.) Kuntze) ...... 4–16A Spinach, tanier (Xanthosoma brasiliense (Desf.) Engl.) ...... 4–16A Swiss chard (Beta vulgaris L. ssp. vulgaris) ...... 4–16A Turnip greens (Brassica rapa L. ssp. rapa) ...... 4–16B Violet, Chinese, leaves (Asystasia gangetica (L.) T. Anderson) ...... 4–16A

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TABLE 1—CROP GROUP 4–16: LEAFY VEGETABLE GROUP—Continued

Related crop sub- Commodities groups

Watercress (Nasturtium officinale W.T. Aiton) ...... 4–16B Cultivars, varieties, and hybrids of these commodities.

(iii) Crop subgroups. The following resentative commodities for each sub- Table 2 identifies the crop subgroups group, and lists all the commodities in- for Crop Group 4–16, specifies the rep- cluded in each subgroup.

TABLE 2—CROP GROUP 4–16: SUBGROUP LISTING

Representative commodities Commodities

Crop Subgroup 4–16A. Leafy greens subgroup

Head lettuce, leaf lettuce, and spinach ...... Amaranth, Chinese; amaranth, leafy; aster, Indian; blackjack; cat’s whiskers; cham-chwi; cham-na-mul; chervil, fresh leaves; chipilin; chrysanthemum, garland; cilantro, fresh leaves; corn salad; cosmos; dandelion, leaves; dang-gwi, leaves; dillweed; dock; dol-nam-mul; ebolo; endive; escarole; fameflower; feather cockscomb; Good King Henry; huauzontle; jute, leaves; lettuce, bitter; lettuce, head; lettuce, leaf; orach; parsley, fresh leaves; plantain, buckhorn; primrose, English; purslane, garden; purslane, winter; radicchio; spinach; spinach, Malabar; spinach, New Zealand; spinach, tanier; Swiss chard; violet, Chinese, leaves; cultivars, varieties, and hybrids of these commodities.

Crop Subgroup 4–16B. Brassica leafy greens subgroup

Mustard greens ...... Arugula; broccoli, Chinese; broccoli raab; cabbage, abyssinian; cabbage, Chinese, bok choy; cabbage, seakale; collards; cress, garden; cress, upland; hanover salad; kale; maca, leaves; mizuna; mustard greens; radish, leaves; rape greens; rocket, wild; shepherd’s purse; turnip greens; watercress; cultivars, varieties, and hybrids of these commodities.

(7) Crop Group 5. Brassica (Cole) Leafy (ii) Table. The following table 1 lists Vegetables Group. all the commodities included in Crop (i) Representative commodities. Broc- Group 5 and identifies the related crop coli or cauliflower; cabbage; and mus- subgroups. tard greens.

TABLE 1—CROP GROUP 5: Brassica (COLE) LEAFY VEGETABLES

Related crop Commodities subgroups

Broccoli (Brassica oleracea var. botrytis) ...... 5A Broccoli, Chinese (gai lon) (Brassica alboglabra) ...... 5A Broccoli raab (rapini) (Brassica campestris) ...... 5B Brussels sprouts (Brassica oleracea var. gemmifera) ...... 5A Cabbage (Brassica oleracea) ...... 5A Cabbage, Chinese (bok choy) (Brassica chinensis) ...... 5B Cabbage, Chinese (napa) (Brassica pekinensis) ...... 5A Cabbage, Chinese mustard (gai choy) (Brassica campestris) ...... 5A Cauliflower (Brassica oleracea var. botrytis) ...... 5A Cavalo broccolo (Brassica oleracea var. botrytis) ...... 5A Collards (Brassica oleracea var. acephala) ...... 5B Kale (Brassica oleracea var. acephala) ...... 5B Kohlrabi (Brassica oleracea var. gongylodes) ...... 5A Mizuna (Brassica rapa Japonica Group) ...... 5B Mustard greens (Brassica juncea) ...... 5B Mustard spinach (Brassica rapa Perviridis Group) ...... 5B Rape greens (Brassica napus) ...... 5B

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(iii) Table. The following table 2 iden- commodity(ies) for each subgroup, and tifies the crop subgroups for Crop lists all the commodities included in Group 5, specifies the representative each subgroup.

TABLE 2—CROP GROUP 5 SUBGROUP LISTING

Representative commodities Commodities

Crop Subgroup 5A. Head and stem Brassica subgroup Broccoli or cauliflower; and cabbage ...... Broccoli; broccoli, Chinese; brussels sprouts; cabbage; cabbage, Chinese (napa); cabbage, Chinese mustard; cauliflower; cavalo broccolo; kohlrabi Crop Subgroup 5B. Leafy Brassica greens subgroup. Mustard greens ...... Broccoli raab; cabbage, Chinese (bok choy); collards; kale; mizuna; mustard greens; mustard spinach; rape greens

(8) Crop Group 5–16. Brassica Head and LIST 1—CROP GROUP 5–16: BRASSICA HEAD Stem Vegetable Group. AND STEM VEGETABLE GROUP—Continued (i) Representative commodities. Broc- Commodities coli or cauliflower and cabbage. (ii) Commodities. The following List 1 Cauliflower (Brassica oleracea L. var. capitata L) contains all commodities included in Cultivars, varieties, and hybrids of these commodities. Crop Group 5–16. (9) Crop Group 6. Legume Vegetables (Succulent or Dried) Group. LIST 1—CROP GROUP 5–16: BRASSICA HEAD (i) Representative commodities. Bean AND STEM VEGETABLE GROUP (Phaseolus spp.; one succulent cultivar Commodities and one dried cultivar); pea (Pisum spp.; one succulent cultivar and one dried Broccoli (Brassica oleracea L. var. italica Plenck) cultivar); and soybean. Brussels sprouts (Brassica oleracea L. var. gemmifera (ii) Table. The following table 1 lists (DC.) Zenker) Cabbage (Brassica oleracea L. var. capitata L.) all the commodities included in Crop Cabbage, Chinese, napa (Brassica rapa L. subsp. Group 6 and identifies the related crop pekinensis (Lour.) Hanelt) subgroups.

TABLE 1—CROP GROUP 6: LEGUME VEGETABLES (SUCCULENT OR DRIED)

Related crop Commodities subgroups

Bean (Lupinus spp.) (includes grain lupin, sweet lupin, white lupin, and white sweet lupin) ...... 6C Bean (Phaseolus spp.) (includes field bean, kidney bean, lima bean, navy bean, pinto bean, runner bean, snap bean, tepary bean, wax bean) ...... 6A, 6B, 6C Bean (Vigna spp.) (includes adzuki bean, asparagus bean, blackeyed pea, catjang, Chinese longbean, cowpea, Crowder pea, moth bean, mung bean, rice bean, southern pea, urd bean, yardlong bean) ...... 6A, 6B, 6C Broad bean (fava bean) (Vicia faba) ...... 6B, 6C Chickpea (garbanzo bean) (Cicer arietinum) ...... 6C Guar (Cyamopsis tetragonoloba) ...... 6C Jackbean (Canavalia ensiformis) ...... 6A Lablab bean (hyacinth bean) (Lablab purpureus) ...... 6C Lentil (Lens esculenta) ...... 6C Pea (Pisum spp.) (includes dwarf pea, edible-pod pea, En glish pea, field pea, garden pea, green pea, snow pea, sugar snap pea) ...... 6A, 6B, 6C Pigeon pea (Cajanus cajan) ...... 6A, 6B, 6C Soybean (Glycine max) ...... N/A Soybean (immature seed) (Glycine max) ...... 6A Sword bean (Canavalia gladiata) ...... 6A

(iii) Table. The following table 2 iden- commodities for each subgroup, and tifies the crop subgroups for Crop lists all the commodities included in Group 6, specifies the representative each subgroup.

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TABLE 2—CROP GROUP 6 SUBGROUP LISTING

Representative commodities Commodities

Crop Subgroup 6A. Edible-podded legume vegetables subgroup. Any one succulent cultivar of edible-podded Bean (Phaseolus spp.) (includes runner bean, snap bean, wax bean); bean bean (Phaseolus spp.) and any one suc- (Vigna spp.) (includes asparagus bean, Chinese longbean, moth bean, culent cultivar of edible-podded pea (Pisum yardlong bean); jackbean; pea (Pisum spp.) (includes dwarf pea, edible-pod spp.).. pea, snow pea, sugar snap pea); pigeon pea; soybean (immature seed); sword bean. Crop Subgroup 6B. Succulent shelled pea and bean subgroup. Any succulent shelled cultivar of bean Bean (Phaseolus spp.) (includes lima bean (green)); broad bean (succulent); (Phaseolus spp.) and garden pea (Pisum bean (Vigna spp.) (includes blackeyed pea, cowpea, southern pea); pea spp.).. (Pisum spp.) (includes English pea, garden pea, green pea); pigeon pea. Crop Subgroup 6C. Dried shelled pea and bean (except soybean) subgroup Any one dried cultivar of bean (Phaseolus Dried cultivars of bean (Lupinus spp.) (includes grain lupin, sweet lupin, white spp.); and any one dried cultivar of pea lupin, and white sweet lupin); (Phaseolus spp.) (includes field bean, kidney (Pisum spp.). bean, lima bean (dry), navy bean, pinto bean; tepary bean; bean (Vigna spp.) (includes adzuki bean, blackeyed pea, catjang, cowpea, Crowder pea, moth bean, mung bean, rice bean, southern pea, urd bean); broad bean (dry); chickpea; guar; lablab bean; lentil; pea (Pisum spp.) (includes field pea); pigeon pea.

(10) Crop Group 7. Foliage of Legume (ii) Table. The following table 1 lists Vegetables Group. the commodities included in Crop (i) Representative commodities. Any Group 7. cultivar of bean (Phaseolus spp.), field pea (Pisum spp.), and soybean.

TABLE 1—CROP GROUP 7: FOLIAGE OF LEGUME VEGETABLES GROUP

Representative commodities Commodities

Any cultivar of bean (Phaseolus spp.) and field Plant parts of any legume vegetable included in the legume vegetables that will pea (Pisum spp.), and soybean (Glycine be used as animal feed. max).

(iii) Table. The following table 2 iden- modities for the subgroup, and lists all tifies the crop subgroup for Crop Group the commodities included in the sub- 7 and specifies the representative com- group.

TABLE 2—CROP GROUP 7 SUBGROUP LISTING

Representative commodities Commodities

Crop Subgroup 7A. Foliage of legume vegetables (except soybeans) subgroup Any cultivar of bean (Phaseolus spp.), and Plant parts of any legume vegetable (except soybeans) included in the legume field pea (Pisum spp.). vegetables group that will be used as animal feed.

(11) Crop Group 8. Fruiting Vegetables CROP GROUP 8: FRUITING VEGETABLES Group. (EXCEPT CUCURBITS)—COMMODITIES (i) Representative commodities. To- Eggplant (Solanum melongena) mato, bell pepper, and one cultivar of Groundcherry (Physalis spp.) non-bell pepper. Pepino (Solanum muricatum) (ii) Commodities. The following is a Pepper (Capsicum spp.) (includes bell pepper, list of all the commodities included in chili pepper, cooking pepper, pimento, Crop Group 8: sweet pepper) Tomatillo (Physalis ixocarpa) Tomato (Lycopersicon esculentum)

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(12) Crop Group 8–10. Fruiting Vege- small tomato; bell pepper and one table Group. cultivar of small nonbell pepper. (i) Representative commodities. To- (ii) Commodities. The following is a mato, standard size, and one cultivar of list of all commodities included in the Crop group 8–10.

TABLE 1—CROP GROUP 8–10: FRUITING VEGETABLE GROUP

Related crop sub- Commodities groups

African eggplant, Solanum macrocarpon L ...... 8–10B, 8–10C Bush tomato, Solanum centrale J.M. Black ...... 8–10A Cocona, Solanum sessiliflorum Dunal ...... 8–10A Currant tomato, Lycopersicon pimpinellifolium L ...... 8–10A Eggplant, Solanum melongena L ...... 8–10B, 8–10C Garden huckleberry, Solanum scabrum Mill ...... 8–10A Goji berry, Lycium barbarum L ...... 8–10A Groundcherry, Physalis alkekengi L., P. grisea (Waterf.) M. Martinez, P. peruviana L., P. pubescens L .. 8–10A Martynia, Proboscidea louisianica (Mill.) Thell ...... 8–10B, 8–10C Naranjilla, Solanum quitoense Lam ...... 8–10A Okra, Abelmoschus esculentus (L.) Moench ...... 8–10B, 8–10C Pea eggplant, Solanum torvum Sw...... 8–10B, 8–10C Pepino, Solanum muricatum Aiton ...... 8–10B, 8–10C Pepper, bell, Capsicum annuum L. var. annuum, Capsicum spp ...... 8–10B Pepper, nonbell, Capsicum chinese Jacq., C. annuum L. var. annuum, C. frutescens L., C. baccatum L., 8–10B, 8–10C C. pubescens Ruiz & Pav., Capsicum spp. Roselle, Hibiscus sabdariffa L ...... 8–10B, 8–10C Scarlet eggplant, Solanum aethiopicum L ...... 8–10B, 8–10C Sunberry, Solanum retroflexum Dunal ...... 8–10A Tomatillo, Physalis philadelphica Lam ...... 8–10A Tomato, Solanum lycopersicum L., Solanum lycopersicum L. var. lycopersicum ...... 8–10A Tree tomato, Solanum betaceum Cav ...... 8–10A Cultivars, varieties and/or hybrids of these ......

(iii) Table. The following Table 2 commodities for each subgroup and identifies the crop subgroups for Crop lists all the commodities included in Group 8–10, specifies the representative each subgroup.

TABLE 2—CROP GROUP 8–10. SUBGROUP LISTING

Representative commodities Commodities

Crop subgroup 8–10A. Tomato subgroup Tomato, standard size, and one cultivar of small tomato ...... Bush tomato; cocona; currant tomato; garden huckleberry; goji berry; groundcherry; naranjilla; sunberry; tomatillo; tomato; tree tomato; cultivars, varieties, and/or hybrids of these. Crop subgroup 8–10B. Pepper/Eggplant subgroup Bell pepper and one cultivar of small nonbell pepper ...... African eggplant; bell pepper; eggplant; Martynia; nonbell pepper; okra; pea eggplant; pepino; roselle; scarlet eggplant; cultivars, varieties, and/or hybrids of these. Crop subgroup 8–10C. Nonbell pepper/Eggplant subgroup One cultivar of small nonbell pepper or one cultivar of small African eggplant; eggplant; martynia; nonbell pepper; okra; pea eggplant. eggplant; pepino; roselle; scarlet eggplant; cultivars, varieties, and/or hybrids of these.

(13) Crop Group 9. Cucurbit Vegeta- (ii) Table. The following table 1 lists bles Group. all the commodities included in Crop (i) Representative commodities. Cucum- Group 9 and identifies the related sub- ber, muskmelon, and summer squash. groups.

TABLE 1—CROP GROUP 9: CUCURBIT VEGETABLES

Related crop Commodities subgroups

Chayote (fruit) (Sechium edule) ...... 9B

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TABLE 1—CROP GROUP 9: CUCURBIT VEGETABLES—Continued

Related crop Commodities subgroups

Chinese waxgourd (Chinese preserving melon) (Benincasa hispida) ...... 9B Citron melon (Citrullus lanatus var. citroides) ...... 9A Cucumber (Cucumis sativus) ...... 9B Gherkin (Cucumis anguria) ...... 9B Gourd, edible (Lagenaria spp.) (includes hyotan, cucuzza); (Luffa acutangula, L. cylindrica) (includes hechima, Chinese okra) ...... 9B Momordica spp. (includes balsam apple, balsam pear, bitter melon, Chinese cucumber) ...... 9B Muskmelon (hybrids and/or cultivars of Cucumis melo) (includes true cantaloupe, cantaloupe, casaba, crenshaw melon, golden pershaw melon, honeydew melon, honey balls, mango melon, Persian melon, pineapple melon, Santa Claus melon, and snake melon) ...... 9A Pumpkin (Cucurbita spp.) ...... 9B Squash, summer (Cucurbita pepo var. melopepo) (includes crookneck squash, scallop squash, straightneck squash, vegetable marrow, zucchini) ...... 9B Squash, winter (Cucurbita maxima; C. moschata) (includes butternut squash, calabaza, hubbard squash); (C. mixta; C. pepo) (includes acorn squash, spaghetti squash) ...... 9B Watermelon (includes hybrids and/or varieties of Citrullus lanatus) ...... 9A

(iii) Table. The following table 2 iden- commodities for each subgroup, and tifies the crop subgroups for Crop lists all the commodities included in Group 9, specifies the representative each subgroup.

TABLE 2—CROP GROUP 9 SUBGROUP LISTING

Representative commodities Commodities

Crop Subgroup 9A. Melon subgroup Cantaloupes ...... Citron melon; muskmelon; watermelon Crop Subgroup 9B. Squash/cucumber subgroup One cultivar of summer squash and cucumber. Chayote (fruit); Chinese waxgourd; cucumber; gherkin; gourd, edible; Momordica spp.; pumpkin; squash, summer; squash, winter.

(14) Crop Group 10. Citrus Fruit Kumquat (Fortunella spp.) Group. Lemon (Citrus jambhiri, Citrus limon) (i) Representative commodities. Sweet Lime (Citrus aurantiifolia) Mandarin (tangerine) (Citrus reticulata) orange; lemon and grapefruit. Orange, sour (Citrus aurantium) (ii) Commodities. The following is a Orange, sweet (Citrus sinensis) list of all the commodities in Crop Pummelo (Citrus grandis, Citrus maxima) Group 10: Satsuma mandarin (Citrus unshiu)

CROP GROUP 10: CITRUS FRUITS (CITRUS SPP., (15) Crop Group 10–10. Citrus Fruit FORTUNELLA SPP.) GROUP—COMMODITIES Group. (i) Representative commodities. Orange Calamondin (Citrus mitis × Citrofortunella mitis) or Tangerine/Mandarin, Lemon or Citrus citron (Citrus medica) Lime, and Grapefruit. Citrus hybrids (Citrus spp.) (includes (ii) Commodities. The following is a chironja, tangelo, tangor) list of all the commodities in Crop Grapefruit (Citrus paradisi) Group 10–10.

TABLE 1—CROP GROUP 10–10: CITRUS FRUIT GROUP

Related crop sub- Commodities groups

Australian desert lime, Eremocitrus glauca (Lindl.) Swingle ...... 10–10B Australian finger lime, Microcitrus australasica (F. Muell.) Swingle ...... 10–10B Australian round lime, Microcitrus australis (A. Cunn. Ex Mudie) Swingle ...... 10–10B Brown River finger lime, Microcitrus papuana Winters ...... 10–10B Calamondin, Citrofortunella microcarpa (Bunge) Wijnands ...... 10–10A Citron, Citrus medica L ...... 10–10A Citrus hybrids, Citrus spp. Eremocitrus spp., Fortunella spp., Microcitrus spp., and Poncirus spp ...... 10–10A Grapefruit, Citrus paradisi Macfad ...... 10–10C

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TABLE 1—CROP GROUP 10–10: CITRUS FRUIT GROUP—Continued

Related crop sub- Commodities groups

Japanese summer grapefruit, Citrus natsudaidai Hayata ...... 10–10C Kumquat, Fortunella spp ...... 10–10B Lemon, Citrus limon (L.) Burm. f ...... 10–10B Lime, Citrus aurantiifolia (Christm.) Swingle ...... 10–10B Mediterranean mandarin, Citrus deliciosa Ten ...... 10–10A Mount White lime, Microcitrus garrowayae (F.M. Bailey) Swingle ...... 10–10B New Guinea wild lime, Microcitrus warburgiana (F.M. Bailey) Tanaka ...... 10–10B Orange, sour, Citrus aurantium L ...... 10–10A Orange, sweet, Citrus sinensis (L.) Osbeck ...... 10–10A Pummelo, Citrus maxima (Burm.) Merr ...... 10–10C Russell River lime, Microcitrus inodora (F.M. Bailey) Swingle ...... 10–10B Satsuma mandarin, Citrus unshiu Marcow ...... 10–10A Sweet lime, Citrus limetta Risso ...... 10–10B Tachibana orange, Citrus tachibana (Makino) Tanaka ...... 10–10A Tahiti lime, Citrus latifolia (Yu. Tanaka) Tanaka ...... 10–10B Tangelo, Citrus xtangelo J.W. Ingram & H.E. Moore ...... 10–10A, 10–10C Tangerine (Mandarin), Citrus reticulata Blanco ...... 10–10A Tangor, Citrus nobilis Lour ...... 10–10A Trifoliate orange, Poncirus trifoliata (L.) Raf ...... 10–10A Uniq fruit, Citrus aurantium Tangelo group ...... 10–10C Cultivars, varieties and/or hybrids of these.

(iii) Table. The following Table 2 tive commodities for each subgroup identifies the crop subgroups for Crop and lists all the commodities included Group 10–10, specifies the representa- in each subgroup.

TABLE 2—CROP GROUP 10–10: SUBGROUP LISTING

Representative commodities Commodities

Crop Subgroup 10–10A. Orange subgroup Orange or tangerine/mandarin ...... Calamondin; citron; citrus hybrids; mediterranean mandarin; orange, sour; orange, sweet; satsuma mandarin; tachibana orange; tangerine (mandarin); tangelo; tangor; trifoliate orange; cultivars, varieties, and/or hybrids of these. Crop Subgroup 10–10B. Lemon/Lime subgroup Lemon or lime ...... Australian desert lime; Australian finger lime; Australian round lime; brown river finger lime; kumquat; lemon; lime; mount white lime; New Guinea wild lime; Russell River lime; sweet lime; Tahiti lime; cultivars , varieties, and/or hybrids of these. Crop Subgroup 10–10C. Grapefruit subgroup Grapefruit ...... Grapefruit; Japanese summer grapefruit; pummelo; tangelo; uniq fruit; cultivars, varieties, and/or hybrids of these.

(16) Crop Group 11: Pome Fruits Quince (Cydonia oblonga) Group. (17) Crop group 11–10. Pome Fruit (i) Representative commodities. Apple Group. and pear. (i) Representative commodities. Apple (ii) Commodities. The following is a and Pear list of all the commodities included in (ii) Commodities. The following is a Crop Group 11: list of all the commodities in Crop CROP GROUP 11: POME FRUITS GROUP— Group 11–10. COMMODITIES CROP GROUP 11–10: POME FRUIT GROUP— Apple (Malus domestica) COMMODITIES Crabapple (Malus spp.) Loquat (Eriobotrya japonica) Apple, Malus domestica Borkh. Mayhaw (Crataegus aestivalis, C. opaca, and C. Azarole, Crataegus azarolus L. rufula) Crabapple, Malus sylvestris (L.) Mill., M. Pear (Pyrus communis) prunifolia (Willd.) Borkh. Pear, oriental (Pyrus pyrifolia) Loquat, Eriobotrya japonica (Thunb.) Lindl.

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Mayhaw, Crataegus aestivalis (Walter) Torr. & CROP GROUP 12: STONE FRUITS GROUP— A. Gray, C. opaca COMMODITIES Hook. & Arn., and C. rufula Sarg. Medlar, Mespilus germanica L. Apricot (Prunus armeniaca) Pear, Pyrus communis L. Cherry, sweet (Prunus avium), Pear, Asian, Pyrus pyrifolia (Burm. f.) Nakai Cherry, tart (Prunus cerasus) var. culta (Makino) Nakai Nectarine (Prunus persica) Pseudocydonia sinensis (Thouin) C.K. Schneid. Peach (Prunus persica) Quince, Cydonia oblonga Mill. Plum (Prunus domestica, Prunus spp.) Quince, Chinese, Chaenomeles speciosa Plum, Chickasaw (Prunus angustifolia) (Sweet) Nakai, Plum, Damson (Prunus domestica spp. Quince, Japanese, Chaenomeles japonica insititia) (Thunb.) Lindl. ex Spach Tejocote, Crataegus mexicana DC. Plum, Japanese (Prunus salicina) Cultivars, varieties and/or hybrids of these. Plumcot (Prunus. armeniaca × P. domestica) Prune (fresh) (Prunus domestica, Prunus spp.) (18) Crop Group 12. Stone Fruits Group. (19) Crop Group 12–12: Stone Fruit (i) Representative commodities. Sweet Group. cherry or tart cherry; peach; and plum (i) Representative commodities. Sweet or fresh prune (Prunus domestica, cherry or Tart cherry; Peach; and Prunus spp.) Plum or Prune plum. (ii) Commodities. The following is a (ii) Commodities. The following Table list of all the commodities included in 1 is a list of all commodities included Crop Group 12: in Crop Group 12–12.

TABLE 1—CROP GROUP 12–12: STONE FRUIT GROUP

Related crop Commodities subgroup

Apricot (Prunus armeniaca L.) ...... 12–12C Apricot, Japanese (Prunus mume Siebold & Zucc.) ...... 12–12C Capulin (Prunus serotina Ehrh. var. salicifolia (Kunth) Koehne) ...... 12–12A Cherry, black (Prunus serotina Ehrh.) ...... 12–12A Cherry, Nanking (Prunus tomentosa Thunb.) ...... 12–12A Cherry, sweet (Prunus avium (L.) L.) ...... 12–12A Cherry, tart (Prunus cerasus L.) ...... 12–12A Jujube, Chinese (Ziziphus jujuba Mill.) ...... 12–12C Nectarine (Prunuspersica (L.) Batsch var. nucipersica (Suckow) C.K. Schneid) ...... 12–12B Peach (Prunus persica (L.) Batsch var. persica) ...... 12–12B Plum (Prunus domestica L. subsp. domestica) ...... 12–12C Plum, American (Prunus americana Marshall) ...... 12–12C Plum, beach (Prunus maritima Marshall) ...... 12–12C Plum, Canada (Prunus nigra Aiton) ...... 12–12C Plum, cherry (Prunus cerasifera Ehrh.) ...... 12–12C Plum, Chickasaw (Prunus angustifolia Marshall) ...... 12–12C Plum, Damson (Prunus domestica L. subsp. insititia (L.) C.K. Schneid.) ...... 12–12C Plum, Japanese (Prunus salicina Lindl.; P. salicina Lindl. var. salicina) ...... 12–12C Plum, Klamath (Prunus subcordata Benth.) ...... 12–12C Plum, prune (Prunus domestica L. subsp. domestica) ...... 12–12C Plumcot (Prunus hybr.) ...... 12–12C Sloe (Prunus spinosa L.) ...... 12–12C Cultivars, varieties, and/or hybrids of these.

(iii) Crop subgroups. The following resentative commodities for each sub- Table 2 identifies the crop subgroups group, and lists all the commodities in- for Crop Group 12–12, specifies the rep- cluded in each subgroup.

TABLE 2—CROP GROUP 12–12: SUBGROUP LISTING

Representative commodities Commodities

Crop subgroup 12–12A. Cherry subgroup

Cherry, sweet or Cherry, tart .... Capulin; Cherry, black; Cherry, Nanking; Cherry, sweet; Cherry, tart; cultivars, varieties, and/or hybrids of these.

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TABLE 2—CROP GROUP 12–12: SUBGROUP LISTING—Continued

Representative commodities Commodities

Crop subgroup 12–12B. Peach subgroup

Peach ...... Peach; Nectarine; cultivars, varieties, and/or hybrids of these.

Crop subgroup 12–12C. Plum subgroup

Plum or Prune plum ...... Apricot; Apricot, Japanese; Jujube, Chinese; Plum; Plum, American; Plum, beach; Plum, Can- ada; Plum, cherry; Plum, Chickasaw; Plum, Damson; Plum, Japanese; Plum, Klamath; Plumcot; Plum, prune; Sloe; cultivars, varieties, and/or hybrids of these.

(20) Crop Group 13. Berries Group. (ii) Table. The following table 1 lists (i) Representative commodities. Any all the commodities included in Crop one blackberry or any one raspberry; Group 13 and identifies the related sub- and blueberry. groups.

TABLE 1—CROP GROUP 13: BERRIES GROUP

Related crop Commodities subgroups

Blackberry (Rubus eubatus) (including bingleberry, black satin berry, boysenberry, Cherokee blackberry, Chesterberry, Cheyenne blackberry, coryberry, darrowberry, dewberry, Dirksen thornless berry, Himalayaberry, hullberry, Lavacaberry, lowberry, Lucretiaberry, mammoth blackberry, marionberry, nectarberry, olallieberry, Oregon evergreen berry, phenomenalberry, rangeberry, ravenberry, rossberry, Shawnee blackberry, youngberry, and varieties and/or hybrids of these) ...... 13A Blueberry (Vaccinium spp.) ...... 13B Currant (Ribes spp.) ...... 13B Elderberry (Sambucus spp.) ...... 13B Gooseberry (Ribes spp.) ...... 13B Huckleberry (Gaylussacia spp.) ...... 13B Loganberry (Rubus loganobaccus) ...... 13A Raspberry, black and red (Rubus occidentalis, Rubus strigosus, Rubus idaeus) ...... 13A

(iii) Table. The following table 2 iden- commodities for each subgroup, and tifies the crop subgroups for Crop lists all the commodities included in Group 13, specifies the representative each subgroup.

TABLE 2—CROP GROUP 13 SUBGROUPS LISTING

Representative commodities Commodities

Crop Subgroup 13A. Caneberry (blackberry and raspberry) subgroup. Any one blackberry or any one raspberry...... Blackberry; loganberry; red and black raspberry; cultivars and/or hybrids of these. Crop Subgroup 13B. Bushberry subgroup.. Blueberry, highbush...... Blueberry, highbush and lowbush; currant; elderberry; gooseberry; huckleberry.

(21) Crop Group 13-07. Berry and Small berry; grape; fuzzy kiwifruit, and Fruit Crop Group strawberry. (i) Representative commodities. Any (ii) Table. The following Table 1 lists one blackberry or any one raspberry; all the commodities listed in Crop highbush blueberry; elderberry or mul- Group 13-07 and identifies the related crop subgroups.

TABLE 1—CROP GROUP 13-07: BERRY AND SMALL FRUIT CROP GROUP

Commodities Related crop subgroups

Amur river grape (Vitis amurensis Rupr) ...... 13-07D, 13-07E, 13-07F Aronia berry (Aronia spp.) ...... 13-07B Bayberry (Myrica spp.) ...... 13-07C

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TABLE 1—CROP GROUP 13-07: BERRY AND SMALL FRUIT CROP GROUP—Continued

Commodities Related crop subgroups

Bearberry (Arctostaphylos uva-ursi) ...... 13-07G, 13-07H Bilberry (Vaccinium myrtillus L.) ...... 13-07G, 13-07H Blackberry (Rubus spp.) (including Andean blackberry, arctic blackberry, bingleberry, black satin berry, boysenberry, brombeere, California blackberry, Chesterberry, Cherokee blackberry, Chey- enne blackberry, common blackberry, coryberry, darrowberry, dewberry, Dirksen thornless berry, evergreen blackberry, Himalayaberry, hullberry, lavacaberry, loganberry, lowberry, Lucretiaberry, mammoth blackberry, marionberry, mora, mures deronce, nectarberry, Northern dewberry, olallieberry, Oregon evergreen berry, phenomenalberry, rangeberry, ravenberry, rossberry, Shaw- nee blackberry, Southern dewberry, tayberry, youngberry, zarzamora, and cultivars, varieties and/or hybrids of these.) ...... 13-07A Blueberry, highbush (Vaccinium spp.) ...... 13-07B Blueberry, lowbush (Vaccinium angustifolium Aiton) ...... 13-07B Buffalo currant (Ribes aureum Pursh) ...... 13-07B Buffaloberry (Shepherdia argentea (Pursh) Nutt.) ...... 13-07C Che (Cudrania tricuspidata Bur. Ex Lavallee) ...... 13-07C Chilean guava (Myrtus ugni Mol.) ...... 13-07B Chokecherry (Prunus virginiana L.) ...... 13-07C Cloudberry (Rubus chamaemorus L.) ...... 13-07G, 13-07H Cranberry (Vaccinium macrocarpon Aiton) ...... 13-07G, 13-07H Currant, black (Ribes nigrum L.) ...... 13-07B Currant, red (Ribes rubrum L.) ...... 13-07B Elderberry (Sambucus spp.) ...... 13-07B, 13-07C European barberry (Berberis vulgaris L.) ...... 13-07B Gooseberry (Ribes spp.) ...... 13-07B, 13-07D, 13- 07E, 13-07F Grape (Vitis spp.) ...... 13-07D, 13-07F Highbush cranberry (Viburnum opulus L. var. Americanum Aiton) ...... 13-07B Honeysuckle, edible (Lonicera caerula L. var. emphyllocalyx Nakai, Lonicera caerula L var . edulis Turcz. ex herder) ...... 13-07B Huckleberry (Gaylussacia spp.) ...... 13-07B Jostaberry (Ribes x nidigrolaria Rud. Bauer and A. Bauer) ...... 13-07B Juneberry (Saskatoon berry) (Amelanchier spp.) ...... 13-07B, 13-07C Kiwifruit, fuzzy (Actinidia deliciosa A. Chev.) (C.F. Liang and A.R. Fergusons, Actinida chinensis Planch.) ...... 13-07D, 13-07E Kiwifruit, hardy (Actinidia arguta (Siebold and Zucc.) Planch. ex Miq) ...... 13-07D, 13-07E, 13-07F Lingonberry (Vaccinium vitis-idaea L.) ...... 13-07B, 13-07G 13-07H Maypop (Passiflora incarnata L.) ...... 13-07E, 13-07F Mountain pepper berries (Tasmannia lanceolata)(Poir.) A.C.Sm...... 13-07C Mulberry (Morus spp.) ...... 13-07C Muntries (Kunzea pomifera F. Muell.) ...... 13-07G, 13-07H Native currant (Acrotriche depressa R. BR.) ...... 13-07B Partridgeberry (Mitchella repens L.) ...... 13-07G, 13-07H Phalsa (Grewia subinaequalis DC.) ...... 13-07C Pincherry (Prunus pensylvanica L.f.) ...... 13-07C Raspberry, black and red (Rubus spp.) ...... 13-07A Riberry (Syzygium luehmannii) ...... 13-07C Salal (Gaultheria shallon Pursh.) ...... 13-07B, 13-07C Schisandra berry (Schisandra chinensis (Turcz.) Baill.) ...... 13-07D, 13-07E, 13-07F Sea buckthorn (Hippophae rhamnoides L.) ...... 13-07B Serviceberry (Sorbus spp.) ...... 13-07C Strawberry (Fragaria x ananassa Duchesne) ...... 13-07G Wild raspberry (Rubus muelleri Lefevre ex P.J. Mull) ...... 13-07A Cultivars, varieties, and/or hybrids of these......

(iii) Table. The following Table 2 tive commodities for each subgroup identifies the crop subgroups for Crop and lists all the commodities included Group 13-07, specifies the representa- in each subgroup.

TABLE 2—CROP GROUP 13-07: SUBGROUP LISTING

Representative commodities Commodities

Crop Subgroup 13-07A. Caneberry subgroup Any one blackberry or any one rasp- Blackberry; loganberry; raspberry, red and black; wild raspberry; cultivars, vari- berry.. eties, and/or hybrids of these. Crop Subgroup 13-07B. Bushberry subgroup.

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TABLE 2—CROP GROUP 13-07: SUBGROUP LISTING—Continued

Representative commodities Commodities

Blueberry, highbush...... Aronia berry; blueberry, highbush; blueberry, lowbush; buffalo currant; Chilean guava; currant, black; currant, red; elderberry; European, barberry; gooseberry; cranberry, highbush; honeysuckle, edible; huckleberry; jostaberry; Juneberry; lingonberry; native currant; salal; sea buckthorn; cultivars, varieties, and/or hybrids of these. Crop Subgroup 13-07C. Large shrub/tree berry subgroup. Elderberry or mulberry...... Bayberry; buffaloberry; che; chokecherry; elderberry; Juneberry; mountain pepper berries; mulberry; phalsa; pincherry; riberry; salal; serviceberry; cultivars, varieties, and/or hybrids of these. Crop Subgroup 13-07D. Small fruit vine climbing subgroup. Grape and fuzzy kiwifruit...... Amur river grape; gooseberry; grape; kiwifruit, fuzzy; kiwifruit, hardy; Maypop; schisandra berry; cultivars, varieties, and /or hybrids of these. Crop Subgroup 13-07E. Small fruit vine climbing subgroup, except grape. Fuzzy kiwifruit...... Amur river grape; gooseberry; kiwifruit, fuzzy; kiwifruit, hardy; Maypop; schisandra berry; cultivars, varieties, and/or hybrids of these. Crop Subgroup 13-07F. Small fruit vine climbing subgroup except fuzzy kiwifruit. Grape...... Amur river grape; gooseberry; grape; kiwifruit, hardy; Maypop; schisandra berry; cultivars varieties, and/or hybrids of these. Crop Subgroup 13-07G. Low growing berry subgroup. Strawberry...... Bearberry; bilberry; blueberry, lowbush; cloudberry; cranberry; lingonberry; muntries; partridgeberry; strawberry; cultivars, varieties, and/or hybrids of these. Crop Subgroup 13-07H. Low growing berry subgroup, except strawberry. Cranberry ...... Bearberry; bilberry; blueberry, lowbush; cloudberry; cranberry; lingonberry; muntries; partridgeberry; cultivars, varieties, and/or cultivars of these.

(22) Crop Group 14. Tree Nuts Group. CROP GROUP 14–12: TREE NUT GROUP (i) Representative commodities. Almond African nut-tree (Ricinodendron heudelotii and pecan. (Baill.) Heckel) (ii) Commodities. The following is a Almond (Prunus dulcis (Mill.) D.A. Webb) list of all the commodities included in Beechnut (Fagus grandifolia Ehrh.; F. Crop Group 14: sylvatica L.) Brazil nut (Bertholletia excelsa Humb. & CROP GROUP 14: TREE NUTS—COMMODITIES Bonpl.) Brazilian pine (Araucaria angustifolia Almond (Prunus dulcis) (Bertol.) Kuntze) Beech nut (Fagus spp.) Bunya (Araucaria bidwillii Hook.) Brazil nut (Bertholletia excelsa) Bur oak (Quercus macrocarpa Michx.) Butternut (Juglans cinerea) Butternut (Juglans cinerea L.) Cashew (Anacardium occidentale) Cajou nut (Anacardium giganteum Hance ex Chestnut (Castanea spp.) Engl.) Chinquapin (Castanea pumila) Candlenut (Aleurites moluccanus (L.) Willd.) Cashew (Anacardium occidentale L.) Filbert (hazelnut) (Corylus spp.) Chestnut (Castanea crenata Siebold & Zucc.; Hickory nut (Carya spp.) C. dentata (Marshall) Borkh.; C. mollissima Macadamia nut (bush nut) (Macadamia spp.) Blume; C. sativa Mill.) Pecan (Carya illinoensis) Chinquapin (Castaneapumila (L.) Mill.) Walnut, black and English (Persian) (Juglans Coconut (Cocos nucifera L.) spp.) Coquito nut (Jubaea chilensis (Molina) Baill.) Dika nut (Irvingia gabonensis (Aubry- (23) Crop Group 14–12. Tree Nut Group. Lecomte ex O’Rorke) Baill.) (i) Representative commodities. Almond Ginkgo (Ginkgo biloba L.) and Pecan. Guiana chestnut (Pachira aquatica Aubl.) (ii) Commodities. The following is a Hazelnut (Filbert) (Corylus americana Mar- list of all commodities included in Crop shall; C. avellana L.; C. californica (A. DC.) Group 14–12. Rose; C. chinensis Franch.) Heartnut (Juglans ailantifolia Carrie`re var. cordiformis (Makino) Rehder)

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Hickory nut (Carya cathayensis Sarg.; C. (i) Representative commodities. Corn, glabra (Mill.) Sweet; C. laciniosa (F. Michx.) wheat, and any other cereal grain crop. W. P. C. Barton; C. myristiciformis (F. (ii) Commodities. The commodities in- Michx.) Elliott; C. ovata (Mill.) K. Koch; C. cluded in Crop Group 16 are: Forage, tomentosa (Lam.) Nutt.) Japanese horse-chestnut (Aesculus turbinate fodder, stover, and straw of all com- Blume) modities included in the group cereal Macadamia nut (Macadamia integrifolia Maid- grains group. EPA may establish sepa- en & Betche; M. tetraphylla L.A.S. John- rate group tolerances on forage, fodder, son) hay, stover, or straw, if data on the Mongongo nut (Schinziophyton rautanenii representative commodities indicate (Schinz) Radcl.-Sm.) differences in the levels of residues on Monkey-pot (Lecythis pisonis Cambess.) Monkey puzzle nut (Araucaria araucana forage, fodder, stover, or straw. (Molina) K. Koch) (26) Crop Group 17. Grass Forage, Fod- Okari nut (Terminalia kaernbachii Warb.) der, and Hay Group. Pachira nut (Pachira insignis (Sw.) Savigny) (i) Representative commodities. Ber- Peach palm nut (Bactris gasipaes Kunth var. muda grass; bluegrass; and bromegrass gasipaes) or fescue. Pecan (Carya illinoinensis (Wangenh.) K. Koch) (ii) Commodities. The commodities in- Pequi (Caryocar brasiliense Cambess.; C. cluded in Crop Group 17 are: Forage, villosum (Aubl.) Pers; C. nuciferum L.) fodder, stover, and hay of any grass, Pili nut (Canarium ovatum Engl.; C. vulgare Gramineae/Poaceae family (either green Leenh.) or cured) except sugarcane and those Pine nut (Pinus edulis Engelm.; P. koraiensis included in the cereal grains group, Siebold & Zucc.; P. sibirica Du Tour; P. that will be fed to or grazed by live- pumila (Pall.) Regel; P. gerardiana Wall. ex D. Don; P. monophylla Torr. & Fre´m.; P. stock, all pasture and range grasses quadrifolia Parl. ex Sudw.; P. pinea L.) and grasses grown for hay or silage. Pistachio (Pistacia vera L.) EPA may establish separate group tol- Sapucaia nut (Lecythis zabucaja Aubl.) erances on forage, fodder, stover, or Tropical almond (Terminalia catappa L.) hay, if data on the representative com- Walnut, black (Juglans nigra L.; J. hindsii modities indicate differences in the Jeps. ex R. E. Sm.; J. microcarpa Berland.) levels of residues on forage, fodder, sto- Walnut, English (Juglans regia L.) ver, or hay. Yellowhorn (Xanthoceras sorbifolium Bunge) Cultivars, varieties, and/or hybrids of these (27) Crop Group 18. Nongrass Animal (24) Crop Group 15. Cereal Grains Feeds (Forage, Fodder, Straw, and Group. Hay) Group. (i) Representative commodities. Corn (i) Representative commodities. Alfalfa (fresh sweet corn and dried field corn), and clover (Trifolium spp.) rice, sorghum, and wheat. (ii) Commodities. EPA may establish (ii) Commodities. The following is a separate group tolerances on forage, list of all the commodities included in fodder, straw, or hay, if data on the Crop Group 15: representative commodities indicate differences in the levels of residues on CROP GROUP 15: CEREAL GRAINS— forage, fodder, straw, or hay. The fol- COMMODITIES lowing is a list of all the commodities Barley (Hordeum spp.) included in Crop Group 18: Buckwheat (Fagopyrum esculentum) Corn (Zea mays) CROP GROUP 18: NONGRASS ANIMAL FEEDS Millet, pearl (Pennisetum glaucum) (FORAGE, FODDER, STRAW, AND HAY) Millet, proso (Panicum milliaceum) GROUP—COMMODITIES Oats (Avena spp.) Alfalfa (Medicago sativa subsp. sativa) Popcorn (Zea mays var. everta) Bean, velvet (Mucuna pruriens var. utilis) Rice (Oryza sativa) Clover (Trifolium spp., Melilotus spp.) Rye (Secale cereale) Kudzu (Pueraria lobata) Sorghum (milo) (Sorghum spp.) Lespedeza (Lespedeza spp.) Teosinte (Euchlaena mexicana) Triticale (Triticum-Secale hybrids) Lupin (Lupinus spp.) Wheat (Triticum spp.) Sainfoin (Onobrychis viciifolia); Wild rice (Zizania aquatica) Trefoil (Lotus spp.) Vetch (Vicia spp.) (25) Crop Group 16. Forage, Fodder Vetch, crown (Coronilla varia) and Straw of Cereal Grains Group. Vetch, milk (Astragalus spp).

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(28) Crop Group 19. Herbs and Spices TABLE 1—CROP GROUP 19: HERBS AND SPICES Group. GROUP—Continued (i) Representative commodities. Basil Related (fresh and dried); black pepper; chive; crop and celery seed or dill seed. Commodities sub- (ii) Table. The following table 1 lists groups all the commodities included in Crop Fennel, Florence (seed) (Foeniculum vulgare Group 19 and identifies the related sub- Azoricum Group) ...... 19B groups. Fenugreek (Trigonella foenumgraecum) ...... 19B Grains of paradise (Aframomum melegueta) ...... 19B Horehound (Marrubium vulgare) ...... 19A TABLE 1—CROP GROUP 19: HERBS AND SPICES Hyssop (Hyssopus officinalis) ...... 19A GROUP Juniper berry (Juniperus communis) ...... 19B Lavender (Lavandula officinalis) ...... 19A Related Lemongrass (Cymbopogon citratus) ...... 19A crop Lovage (leaf) (Levisticum officinale) ...... 19A Commodities subgroups Lovage (seed) (Levisticum officinale) ...... 19B Mace (Myristica fragrans) ...... 19B Allspice (Pimenta dioica) ...... 19B Marigold (Calendula officinalis) ...... 19A Angelica (Angelica archangelica) ...... 19A Marjoram (Origanum spp.) (includes sweet or an- Anise (anise seed) (Pimpinella anisum) ...... 19B nual marjoram, wild marjoram or oregano, and Anise, star (Illicium verum) ...... 19B pot marjoram) ...... 19A Annatto (seed) ...... 19B Mustard (seed) (Brassica juncea, B. hirta, B. nigra) 19B Balm (lemon balm) (Melissa officinalis) ...... 19A Nasturtium (Tropaeolum majus) ...... 19A Basil (Ocimum basilicum) ...... 19A Nutmeg (Myristica fragrans) ...... 19B Borage (Borago officinalis) ...... 19A Parsley (dried) (Petroselinum crispum) ...... 19A Burnet (Sanguisorba minor) ...... 19A Pennyroyal (Mentha pulegium) ...... 19A Camomile (Anthemis nobilis) ...... 19A Pepper, black (Piper nigrum) ...... 19B Caper buds (Capparis spinosa) ...... 19B Pepper, white ...... 19B Caraway (Carum carvi) ...... 19B Poppy (seed) (Papaver somniferum) ...... 19B Caraway, black (Nigella sativa) ...... 19B Cardamom (Elettaria cardamomum) ...... 19B Rosemary (Rosemarinus officinalis) ...... 19A Cassia bark (Cinnamomum aromaticum) ...... 19B Rue (Ruta graveolens) ...... 19A Cassia buds (Cinnamomum aromaticum) ...... 19B Saffron (Crocus sativus) ...... 19B Catnip (Nepeta cataria) ...... 19A Sage (Salvia officinalis) ...... 19A Celery seed (Apicum graveolens) ...... 19B Savory, summer and winter (Satureja spp.) ...... 19A Chervil (dried) (Anthriscus cerefolium) ...... 19A Sweet bay (bay leaf) (Laurus nobilis) ...... 19A Chive (Allium schoenoprasum) ...... 19A Tansy (Tanacetum vulgare) ...... 19A Chive, Chinese (Allium tuberosum) ...... 19A Tarragon (Artemisia dracunculus) ...... 19A Cinnamon (Cinnamomum verum) ...... 19B Thyme (Thymus spp.) ...... 19A Clary (Salvia sclarea) ...... 19A Vanilla (Vanilla planifolia) ...... 19B Clove buds (Eugenia caryophyllata) ...... 19B Wintergreen (Gaultheria procumbens) ...... 19A Coriander (cilantro or Chinese parsley) (leaf) Woodruff (Galium odorata) ...... 19A (Coriandrum sativum) ...... 19A Wormwood (Artemisia absinthium) ...... 19A Coriander (cilantro) (seed) (Coriandrum sativum) ... 19B Costmary (Chrysanthemum balsamita) ...... 19A (iii) Table. The following table 2 iden- Culantro (leaf) (Eryngium foetidum) ...... 19A Culantro (seed) (Eryngium foetidum) ...... 19B tifies the crop subgroups for Crop Cumin (Cuminum cyminum) ...... 19B Group 19, specifies the representative Curry (leaf) (Murraya koenigii) ...... 19A commodities for each subgroup, and Dill (dillweed) (Anethum graveolens) ...... 19A Dill (seed) (Anethum graveolens) ...... 19B lists all the commodities included in Fennel (common) (Foeniculum vulgare) ...... 19B each subgroup.

TABLE 2—CROP GROUP 19 SUBGROUPS

Representative commodities Commodities

Crop Subgroup 19A. Herb subgroup. Basil (fresh and dried) and chive...... Angelica; balm; basil; borage; burnet; camomile; catnip; chervil (dried); chive; chive, Chinese, clary; coriander (leaf); costmary; culantro (leaf); curry (leaf); dillweed; horehound; hyssop; lavender; lemongrass; lovage (leaf); marigold; marjoram (Origanum spp.); nasturtium; parsley (dried); pennyroyal; rosemary; rue; sage; savory, summer and winter; sweet bay; tansy; tarragon; thyme; wintergreen; woodruff; and wormwood. Crop Subgroup 19B. Spice subgroup. Black pepper; and celery seed or dill seed...... Allspice; anise (seed); anise, star; annatto (seed); caper (buds); caraway; caraway, black; cardamom; cassia (buds); celery (seed); cinnamon; clove (buds); coriander (seed); culantro (seed); cumin; dill (seed); fennel, common; fennel, Florence (seed); fenugreek; grains of paradise; juniper (berry); lovage (seed); mace; mustard (seed); nutmeg; pepper, black; pepper, white; poppy (seed); saffron; and vanilla.

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(29) Crop Group 20. Oilseed Group. (ii) Table. The following Table 1 lists (i) Representative commodities. all the commodities listed in Crop Rapeseed (canola varieties only); sun- Group 20 and identifies the related crop flower, seed and cottonseed. subgroups and includes cultivars and/or varieties of these commodities.

TABLE 1—CROP GROUP 20: OILSEED GROUP

Related crop Commodities subgroups

Borage, Borago officinalis L ...... 20A Calendula, Calendula officinalis L ...... 20B Castor oil plant, Ricinus communis L ...... 20B Chinese tallowtree, Triadica sebifera (L.) Small ...... 20B Cottonseed, Gossypium hirsutum L. Gossypium spp ...... 20C Crambe, Crambe hispanica L.; C. abyssinica Hochst. ex R.E. Fr ...... 20A Cuphea, Cuphea hyssopifolia Kunth ...... 20A Echium, Echium plantagineum L ...... 20A Euphorbia, Euphorbia esula L ...... 20B Evening primrose, Oenothera biennis L ...... 20B Flax seed, Linum usitatissimum L ...... 20A Gold of pleasure, Camelina sativa (L.) Crantz ...... 20A Hare’s ear mustard, Conringia orientalis (L.) Dumort ...... 20A Jojoba, Simmondsia chinensis (Link) C.K. Schneid ...... 20B Lesquerella, Lesquerella recurvata (Engelm. ex A. Gray) S. Watson ...... 20A Lunaria, Lunaria annua L ...... 20A Meadowfoam, Limnanthes alba Hartw. ex Benth ...... 20A Milkweed, Asclepias spp ...... 20A Mustard seed, Brassica hirta Moench, Sinapis alba L. subsp. Alba...... 20A Niger seed, Guizotia abyssinica (L.f.) Cass ...... 20B Oil radish, Raphanus sativus L. var. oleiformis Pers ...... 20A Poppy seed, Papaver somniferum L. subsp. Somniferum ...... 20A Rapeseed, Brassica spp.; B. napus L ...... 20A Rose hip, Rosa rubiginosa L ...... 20B Safflower, Carthamus tinctorious L ...... 20B Sesame, Sesamum indicum L., S. radiatum Schumach. & honn ...... 20A Stokes aster, Stokesia laevis (Hill) Greene ...... 20B Sunflower, Helianthus annuus L ...... 20B Sweet rocket, Hesperis matronalis L ...... 20A Tallowwood, Ximenia americana L ...... 20B Tea oil plant, Camellia oleifera C. Abel ...... 20B Vernonia, Vernonia galamensis (Cass.) Less ...... 20B Cultivars, varieties, and/or hybrids of these.

(iii) Table. The following Table 2 commodities for each subgroup and identifies the crop subgroups for Crop lists all the commodities included in Group 20, specifies the representative each subgroup.

TABLE 2—CROP GROUP 20: SUBGROUP LISTING

Representative commodities Commodities

Crop subgroup 20A. Rapeseed subgroup Rapeseed, canola varieties only ...... Borage; crambe; cuphea; echium; flax seed; gold of pleasure; hare’s ear mustard; lesquerella; lunaria; meadowfoam; milkweed; mustard seed; oil radish; poppy seed; rapeseed; sesame; sweet rocket cultivars, varieties, and/or hybrids of these. Crop subgroup 20B. Sunflower subgroup Sunflower, seed...... Calendula; castor oil plant; chinese tallowtree; euphorbia; evening primrose; jojoba; niger seed; rose hip; safflower; stokes aster; sunflower; tallowwood; tea oil plant; vernonia; cultivars, varieties, and/or hybrids of these. Crop subgroup 20C. Cottonseed subgroup Cottonseed ...... Cottonseed; cultivars, varieties, and/or hybrids of these.

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(30) Crop Group 21. Edible fungi CROP GROUP 21—EDIBLE FUNGI GROUP— Group. COMMODITIES (i) Representative commodities. White Blewitt (Lepista nuda) button mushroom and any one oyster Bunashimeji (Hypsizygus marrmoreus) Chinese mushroom (Volvariella volvacea) (Bull.) Singer mushroom or any Shiitake mushroom. Enoki (Flammulina velutipes) (Curt.) Singer (ii) Table. The following is a list of all Hime-Matsutake (Agaricus blazei) Murill Hirmeola (Auricularia auricular) the commodities in Crop Group 21. Maitake (Grifola frondosa) There are no related subgroups. Morel (Morchella spp.) Nameko (Pholiota nameko) Net Bearing (Dictyophora) Oyster mushroom (Pleurotus spp.) Pom Pom (Hericium erinaceus) Reishi mushroom (Ganoderma lucidum (Leyss. Fr.) Karst.) Rodman’s agaricus (Agaricus bitorquis) (Quel.) Saccardo Shiitake mushroom (Lentinula edodes (Berk.) Pegl.) Shimeji (Tricholoma conglobatum) Stropharia (Stropharia spp.) Truffle (Tuber spp.) White button mushroom (Agaricus bisporous (Lange) Imbach) White Jelly Fungi (Tremella fuciformis) (31) Crop Group 22. Stalk, Stem and Leaf Petiole Vegetable Group. (i) Representative commodities. Aspar- agus and celery. (ii) Commodities. The following Table 1 lists all commodities included in Crop Group 22.

TABLE 1—CROP GROUP 22: STALK, STEM AND LEAF PETIOLE VEGETABLE GROUP

Related crop Commodities subgroups

Agave (Agave spp.) ...... 22A Aloe vera (Aloe vera (L.) Burm.f.) ...... 22A Asparagus (Asparagus officinalis L.) ...... 22A Bamboo, shoots (Arundinaria spp.; Bambusa spp., Chimonobambusa spp.; Dendrocalamus spp., Fargesia spp.; Gigantochloa spp., Nastus elatus; Phyllostachys spp.; Thyrsostachys spp.) ...... 22A Cardoon (Cynara cardunculus L.) ...... 22B Celery (Apium graveolens var. dulce (Mill.) Pers.) ...... 22B Celery, Chinese (Apium graveolens L. var. secalinum (Alef.) Mansf.) ...... 22B Celtuce (Lactuca sativa var. angustana L.H. Bailey) ...... 22A Fennel, Florence, fresh leaves and stalk (Foeniculum vulgare subsp. vulgare var. azoricum (Mill.) Thell.) ...... 22A Fern, edible, fiddlehead ...... 22A Fuki (Petasites japonicus (Siebold & Zucc.) Maxim.) ...... 22B Kale, sea (Crambe maritima L.) ...... 22A Kohlrabi (Brassica oleracea L. var gongylodes L.) ...... 22A Palm hearts (various species) ...... 22A Prickly pear, pads (Opuntia ficus-indica (L.) Mill., Opuntia spp.) ...... 22A Prickly pear, Texas, pads (Opuntia engelmannii Salm-Dyck ex Engelm. var. lindheimeri (Engelm.) B.D. Parfitt & Pinkav) ...... 22A Rhubarb (Rheum x rhabarbarum L.) ...... 22B Udo (Aralia cordata Thunb. ) ...... 22B Zuiki (Colocasia gigantea (Blume) Hook. f.) ...... 22B Cultivars, varieties, and hybrids of these commodities.

(iii) Crop subgroups. The following resentative commodities for each sub- Table 2 identifies the crop subgroups group, and lists all the commodities in- for Crop Group 22, specifies the rep- cluded in each subgroup.

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TABLE 2—CROP GROUP 22: SUBGROUP LISTING

Representative commodities Commodities

Crop Subgroup 22A. Stalk and stem vegetable subgroup

Asparagus ...... Agave; aloe vera; asparagus; bamboo, shoots; celtuce; fennel, florence, fresh leaves and stalk; fern, edible, fiddlehead; kale, sea; kohlrabi; palm hearts; prickly pear, pads; prickly pear, Texas, pads; cultivars, varieties, and hybrids of these commodities.

Crop Subgroup 22B. Leaf petiole vegetable subgroup

Celery ...... Cardoon; celery; celery, Chinese; fuki; rhubarb; udo; zuiki; cultivars, varieties, and hybrids of these commodities.

(32) Crop Group 23. Tropical and Sub- (ii) Commodities. The following Table tropical Fruit, Edible Peel Group. 1 lists all commodities included in Crop (i) Representative commodities. Date, Group 23. fig, guava, and olive.

TABLE 1—CROP GROUP 23: TROPICAL AND SUBTROPICAL FRUIT, EDIBLE PEEL GROUP

Related crop Commodities subgroups

Ac¸aı´ (Euterpe oleracea Mart.) ...... 23C Acerola (Malpighia emarginata DC.) ...... 23A Achachairu´ (Garcinia gardneriana (Planch. & Triana) Zappi) ...... 23B African plum (Vitex doniana Sweet) ...... 23A Agritos (Berberis trifoliolata Moric.) ...... 23A Almondette (Buchanania lanzan Spreng.) ...... 23A Ambarella (Spondias dulcis Sol. ex Parkinson) ...... 23B Apak palm (Brahea dulcis (Kunth) Mart.) ...... 23C Appleberry (Billardiera scandens Sm.) ...... 23A Araza´ (Eugenia stipitata McVaugh) ...... 23B Arbutus berry (Arbutus unedo L.) ...... 23A Babaco (Vasconcellea x heilbornii (V.M. Badillo) V.M. Badillo) ...... 23B Bacaba palm (Oenocarpus bacaba Mart.) ...... 23C Bacaba-de-leque (Oenocarpus distichus Mart.) ...... 23C Bayberry, red (Morella rubra Lour.) ...... 23A Bignay (Antidesma bunius (L.) Spreng.) ...... 23A Bilimbi (Averrhoa bilimbi L.) ...... 23B Borojo´ (Borojoa patinoi Cuatrec.) ...... 23B Breadnut (Brosimum alicastrum Sw.) ...... 23A Cabeluda (Plinia glomerata (O. Berg) Amshoff) ...... 23A Cajou, fruit (Anacardium giganteum Hance ex Engl.) ...... 23B Cambuca´ (Marlierea edulis Nied.) ...... 23B Carandas-plum (Carissa edulis Vahl) ...... 23A Carob (Ceratonia siliqua L.) ...... 23B Cashew apple (Anacardium occidentale L.) ...... 23B Ceylon iron wood (Manilkara hexandra (Roxb.) Dubard) ...... 23A Ceylon olive (Elaeocarpus serratus L.) ...... 23A Cherry-of-the-Rio-Grande (Eugenia aggregata (Vell.) Kiaersk.) ...... 23A Chinese olive, black (Canarium tramdenum C.D. Dai & Yakovlev) ...... 23A Chinese olive, white (Canarium album (Lour.) Raeusch.) ...... 23A Chirauli-nut (Buchanania latifolia Roxb.) ...... 23A Ciruela verde (Bunchosia armeniaca (Cav.) DC.) ...... 23B Cocoplum (Chrysobalanus icaco L.) ...... 23A Date (Phoenix dactylifera L.) ...... 23C Davidson’s plum (Davidsonia pruriens F. Muell.) ...... 23B Desert-date (Balanites aegyptiacus (L.) Delile) ...... 23A Doum palm coconut (Hyphaene thebaica (L.) Mart.) ...... 23C False sandalwood (Ximenia americana L.) ...... 23A Feijoa (Acca sellowiana (O. Berg) Burret) ...... 23B Fig (Ficus carica L.) ...... 23B Fragrant manjack (Cordia dichotoma G. Forst.) ...... 23A Gooseberry, abyssinian (Dovyalis abyssinica (A. Rich.) Warb.) ...... 23A Gooseberry, Ceylon (Dovyalis hebecarpa (Gardner) Warb.) ...... 23A Gooseberry, Indian (Phyllanthus emblica L.) ...... 23B Gooseberry, otaheite (Phyllanthus acidus (L.) Skeels) ...... 23A Governor’s plum (Flacourtia indica (Burm. F.) Merr.) ...... 23A Grumichama (Eugenia brasiliensis Lam) ...... 23A

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TABLE 1—CROP GROUP 23: TROPICAL AND SUBTROPICAL FRUIT, EDIBLE PEEL GROUP—Continued

Related crop Commodities subgroups

Guabiroba (Campomanesia xanthocarpa O. Berg) ...... 23A Guava (Psidium guajava L.) ...... 23B Guava berry (Myrciaria floribunda (H. West ex Willd.) O. Berg) ...... 23A Guava, Brazilian (Psidium guineense Sw.) ...... 23A Guava, cattley (Psidium cattleyanum Sabine) ...... 23B Guava, Costa Rican (Psidium friedrichsthalianum (O. Berg) Nied.) ...... 23A Guava, Para (Psidium acutangulum DC.) ...... 23B Guava, purple strawberry (Psidium cattleyanum Sabine var. cattleyanum) ...... 23B Guava, strawberry (Psidium cattleyanum Sabine var. littorale (Raddi) Fosberg) ...... 23B Guava, yellow strawberry (Psidium cattleyanum Sabine var. cattleyanum forma lucidum O. Deg.) ...... 23B Guayabillo (Psidium sartorianum (O. Berg) Nied.) ...... 23A Illawarra plum (Podocarpus elatus R. Br. Ex Endl.) ...... 23A Imbe´ (Garcinia livingstonei T. Anderson) ...... 23B Imbu (Spondias tuberosa Arruda ex Kost.) ...... 23B Indian-plum (Flacourtia jangomas (Lour.). basionym) ...... 23A Jaboticaba (Myrciaria cauliflora (Mart.) O. Berg) ...... 23B Jamaica-cherry (Muntingia calabura L.) ...... 23A Jambolan (Syzygium cumini (L.) Skeels) ...... 23A Jelly palm (Butia capitata (Mart.) Becc.) ...... 23C Jujube, Indian (Ziziphus mauritiana Lam.) ...... 23B Kaffir-plum (Harpephyllum caffrum Bernh. Ex C. Krauss) ...... 23A Kakadu plum (Terminalia latipes Benth. subsp. psilocarpa Pedley) ...... 23A Kapundung (Baccaurea racemosa (Reinw.) Mull. Arg.) ...... 23A Karanda (Carissa carandas L.) ...... 23A Kwai muk (Artocarpus hypargyreus Hance ex Benth.) ...... 23B Lemon aspen (Acronychia acidula F. Muell) ...... 23A Mangaba (Hancornia speciosa Gomes) ...... 23B Marian plum (Bouea macrophylla Griff.) ...... 23B Mombin, malayan (Spondias pinnata (J. Koenig ex L. f.) Kurz) ...... 23B Mombin, purple (Spondias purpurea L.) ...... 23B Mombin, yellow (Spondias mombin L.) ...... 23A Monkeyfruit (Artocarpus lacucha Buch. Ham.) ...... 23B Monos plum (Pseudanamomis umbellulifera (Kunth) Kausel) ...... 23A Mountain cherry (Bunchosia cornifolia Kunth) ...... 23A Nance (Byrsonima crassifolia (L.) Kunth) ...... 23B Natal plum (Carissa macrocarpa (Eckl.) A. DC.) ...... 23B Noni (Morinda citrifolia L.) ...... 23B Olive (Olea europaea L. subsp. europaea) ...... 23A Papaya, mountain (Vasconcellea pubescens A. DC.) ...... 23B Pataua´ (Oenocarpus bataua Mart.) ...... 23C Peach palm, fruit (Bactris gasipaes Kunth var. gasipaes) ...... 23C Persimmon, black (Diospyros texana Scheele) ...... 23A Persimmon, Japanese (Diospyros kaki Thunb.) ...... 23B Pitomba (Eugenia luschnathiana Klotzsch ex O. Berg) ...... 23A Plum-of-Martinique (Flacourtia inermis Roxb.) ...... 23A Pomerac (Syzygium malaccense (L.) Merr. & L.M. Perry) ...... 23B Rambai (Baccaurea motleyana (Mull. Arg.) Mull. Arg.) ...... 23B Rose apple (Syzygium jambos (L.) Alston) ...... 23B Rukam (Flacourtia rukam Zoll. & Moritizi) ...... 23A Rumberry (Myrciaria dubia (Kunth) McVaugh Myrtaceae) ...... 23A Sea grape (Coccoloba uvifera (L.) L.) ...... 23A Sentul (Sandoricum koetjape (Burm. F.) Merr.) ...... 23B Sete-capotes (Campomanesia guazumifolia (Cambess.) O. Berg) ...... 23A Silver aspen (Acronychia wilcoxian (F. Muell.) T.G. Hartley) ...... 23A Starfruit (Averrhoa carambola L.) ...... 23B Surinam cherry (Eugenia uniflora L.) ...... 23B Tamarind (Tamarindus indica L.) ...... 23B Uvalha (Eugenia pyriformis Cambess ) ...... 23B Water apple (Syzygium aqueum (Burm. F.) Alston) ...... 23A Water pear (Syzygium guineense (Willd.) DC) ...... 23A Water berry (Syzygium cordatum Hochst. Ex C. Krauss) ...... 23A Wax jambu (Syzygium samarangense (Blume) Merr. & L.M. Perry) ...... 23A Cultivars, varieties, and hybrids of these commodities.

(iii) Table. The following Table 2 commodities for each subgroup, and identifies the crop subgroups for Crop lists all the commodities included in Group 23, specifies the representative each subgroup.

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TABLE 2—CROP GROUP 23: SUBGROUP LISTING

Representative commodities Commodities

Crop Subgroup 23A. Tropical and Subtropical, Small fruit, edible peel subgroup

Olive ...... Acerola; African plum; agritos; almondette; appleberry; arbutus berry; bayberry, red; bignay; breadnut; cabeluda; carandas-plum; Ceylon iron wood; Ceylon olive; cherry-of-the-Rio-Grande; Chinese olive, black; Chinese olive, white; chirauli-nut; cocoplum; desert-date; false sandalwood; fragant manjack; gooseberry, abyssinian; gooseberry, Ceylon; gooseberry, otaheite; governor’s plum; grumichama; guabiroba; guava berry; guava, Brazilian; guava, Costa Rican; guayabillo; illawarra plum; Indian-plum; Jamaica-cherry; jambolan; kaffir-plum; kakadu plum; kapundung; karanda; lemon aspen; mombin, yellow; monos plum; mountain cherry; olive; persimmon, black; pitomba; plum-of-Martinique; rukam; rumberry; sea grape; sete-capotes; silver aspen; water apple; water pear; water berry; wax jambu; cultivars, varieties, and hybrids of these commodities.

Crop Subgroup 23B. Tropical and Subtropical, Medium to large fruit, edible peel subgroup

Fig and guava ...... Achachairu´; ambarella; araza´; babaco; bilimbi; borojo´; cajou, fruit; cambuca´; carob; cashew apple; ciruela verde; davidson’s plum; feijoa; fig; gooseberry, Indian; guava; guava, cattley; guava, Para; guava, purple strawberry; guava, strawberry; guava, yellow strawberry; imbe´; imbu; jaboticaba; jujube, Indian; kwai muk; mangaba; Marian plum; mombin, Malayan; mombin, purple; monkeyfruit; nance; natal plum; noni; papaya, mountain; persimmon, Japanese; pomerac; rambai; rose apple; sentul; starfruit; Surinam cherry; tamarind; uvalha; cultivars, varieties, and hybrids of these commodities.

Crop Subgroup 23C. Tropical and Subtropical, Palm fruit, edible peel subgroup

Date ...... Ac¸aı´; apak palm; bacaba palm; bacaba-de-leque; date; doum palm coconut; jelly palm; pataua´; peach palm, fruit; cultivars, varieties, and hybrids of these commodities.

(33) Crop Group 24. Tropical and Sub- lychee, passionfruit, pineapple, and tropical Fruit, Inedible Peel Group. prickly pear, fruit. (i) Representative commodities. (ii) Commodities. The following Table Atemoya or sugar apple, avocado, ba- 1 lists all commodities included in Crop nana or pomegranate, dragon fruit, Group 24.

TABLE 1—CROP GROUP 24: TROPICAL AND SUBTROPICAL FRUIT, INEDIBLE PEEL GROUP

Related crop Commodities subgroups

Abiu (Pouteria caimito (Ruiz & Pav.) Radlk) ...... 24B Aisen (Boscia senegalensis (Pers.) Lam.) ...... 24A Akee apple (Blighia sapida K.D. Koenig) ...... 24B Atemoya (Annona cherimola Mill. X A. squamosa L.) ...... 24C Avocado (Persea americana Mill.) ...... 24B Avocado, Guatemalan (Persea americana Mill. var. guatemalensis) ...... 24B Avocado, Mexican (Persea americana Mill. var. drymifolia (Schltdl. & Cham.) S.F. Blak) ...... 24B Avocado, West Indian (Persea americana var. americana) ...... 24B Bacury (Platonia insignis Mart.) ...... 24B Bael fruit (Aegle marmelos (L.) Correˆa) ...... 24A Banana (Musa spp.) ...... 24B Banana, dwarf (Musa hybrids; Musa acuminata Colla) ...... 24B Binjai (Mangifera caesia Jack) ...... 24B Biriba (Annona mucosa Jacq.) ...... 24C Breadfruit (Artocarpus altilis (Parkinson) Fosberg) ...... 24C Burmese grape (Baccaurea ramiflora Lour.) ...... 24A Canistel (Pouteria campechiana (Kunth) Baehni) ...... 24B Cat’s-eyes (Dimocarpus longan Lour. subsp. malesianus Leenh.) ...... 24A Champedak (Artocarpus integer (Thunb.) Merr.) ...... 24C Cherimoya (Annona cherimola Mill.) ...... 24C Cupuacu´ (Theobroma grandiflorum (Willd. Ex Spreng.) K. Schum.) ...... 24B Custard apple (Annona reticulata L.) ...... 24C Dragon fruit (Hylocereus undatus (Haw.) Britton & Rose) ...... 24D Durian (Durio zibethinus L.) ...... 24C

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TABLE 1—CROP GROUP 24: TROPICAL AND SUBTROPICAL FRUIT, INEDIBLE PEEL GROUP—Continued

Related crop Commodities subgroups

Elephant-apple (Limonia acidissima L.) ...... 24C Etambe (Mangifera zeylanica (Blume) Hook. F.) ...... 24B Granadilla (Passiflora ligularis Juss.) ...... 24E Granadilla, giant (Passiflora quadrangularis L.) ...... 24E Ilama (Annona macroprophyllata Donn. Sm.) ...... 24C Inga´ (Inga vera Willd. subsp. affinis (DC.) T.D. Penn.) ...... 24A Jackfruit (Artocarpus heterophyllus Lam.) ...... 24C Jatoba´ (Hymenaea courbaril L.) ...... 24B Karuka (Pandanus julianettii Martelli) ...... 24C Kei apple (Dovyalis caffra (Hook. F. & Harv.) Warb.) ...... 24B Langsat (Lansium domesticum Correˆa) ...... 24B Lanjut (Mangifera lagenifera Griff.) ...... 24B Longan (Dimocarpus longan Lour.) ...... 24A Lucuma (Pouteria lucuma (Ruiz & Pav.) Kuntze) ...... 24B Lychee (Litchi chinensis Sonn.) ...... 24A Mabolo (Diospyros blancoi A. DC.) ...... 24B Madras-thorn (Pithecellobium dulce (Roxb.) Benth.) ...... 24A Mammy-apple (Mammea americana L.) ...... 24C Manduro (Balanites maughamii Sprague) ...... 24A Mango (Mangifera indica L.) ...... 24B Mango, horse (Mangifera foetida Lour.) ...... 24B Mango, Saipan (Mangifera odorata Griff.) ...... 24B Mangosteen (Garcinia mangostana L. ) ...... 24B Marang (Artocarpus odoratissimus Blanco) ...... 24C Marmaladebox (Genipa americana L.) ...... 24C Matisia (Matisia cordata Humb. & Bonpl.) ...... 24A Mesquite (Prosopis juliflora (Sw.) DC.) ...... 24A Mongongo, fruit (Schinziophyton rautanenii (Schinz) Radcl.-Sm) ...... 24A Monkey-bread-tree (Adansonia digitata L.) ...... 24C Monstera (Monstera deliciosa Liebm.) ...... 24E Nicobar-breadfruit (Pandanus leram Jones ex Fontana) ...... 24C Paho (Mangifera altissima Blanco) ...... 24B Pandanus (Pandanus utilis Bory) ...... 24C Papaya (Carica papaya L.) ...... 24B Passionflower, winged-stem (Passiflora alata Curtis) ...... 24E Passionfruit (Passiflora edulis Sims) ...... 24E Passionfruit, banana (Passiflora tripartita var. mollissima (Kunth) Holm-Niels. & P. Jorg.) ...... 24E Passionfruit, purple (Passiflora edulis Sims forma edulis) ...... 24E Passionfruit, yellow (Passiflora edulis Sims forma flavicarpa O. Deg.) ...... 24E Pawpaw, common (Asimina triloba (L.) Dunal) ...... 24B Pawpaw, small-flower (Asimina parviflora (Michx.) Dunal) ...... 24A Pelipisan (Mangifera casturi Kosterm.) ...... 24B Pequi (Caryocar brasiliense Cambess) ...... 24B Pequia (Caryocar villosum (Aubl.) Pers.) ...... 24B Persimmon, American (Diospyros virginiana L.) ...... 24B Pineapple (Ananas comosus (L.) Merr.) ...... 24C Pitahaya (Hylocereus polyrhizus (F.A.C. Weber) Britton & Rose) ...... 24D Pitaya (Hylocereus sp. including H. megalanthus (H. ocamponis and H. polychizus) ...... 24D Pitaya, amarilla (Hylocereus triangularis Britton & Rose) ...... 24D Pitaya, roja (Hylocereus ocamponis (Salm-Dyck) Britton & Rose) ...... 24D Pitaya, yellow (Hylocereus megalanthus (K. Schum. ex Vaupel) Ralf Bauer) ...... 24D Plantain (Musa paradisiaca L.) ...... 24B Pomegranate (Punica granatum L.) ...... 24B Poshte (Annona liebmanniana Baill.) ...... 24B Prickly pear, fruit (Opuntia ficus-indica (L.) Mill.) ...... 24D Prickly pear, Texas, fruit (Opuntia engelmannii Salm-Dyck ex Engelm. var. lindheimeri (Engelm.) B.D. Parfitt & Pinkav) ...... 24D Pulasan (Nephelium ramboutan-ake (Labill.) Leenh.) ...... 24C Quandong (Santalum acuminatum (R. Br.) DC.) ...... 24B Rambutan (Nephelium lappaceum L.) ...... 24C Saguaro (Carnegiea gigantea (Engelm.) Britton & Rose) ...... 24D Sapodilla (Manilkara zapota (L.) P. Royen) ...... 24C Sapote, black (Diospyros digyna Jacq.) ...... 24B Sapote, green (Pouteria viridis (Pittier) Cronquist) ...... 24B Sapote, mamey (Pouteria sapota (Jacq.) H.E. Moore & Stearn) ...... 24C Sapote, white (Casimiroa edulis La Llave & Lex) ...... 24B Sataw (Parkia speciosa Hassk.) ...... 24B Satinleaf (Chrysophyllum oliviforme L.) ...... 24A Screw-pine (Pandanus tectorius Parkinson) ...... 24B Sierra Leone-tamarind (Dialium guineense Willd.) ...... 24A Soncoya (Annona purpurea Moc. & Sesse´ ex Dunal) ...... 24C

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TABLE 1—CROP GROUP 24: TROPICAL AND SUBTROPICAL FRUIT, INEDIBLE PEEL GROUP—Continued

Related crop Commodities subgroups

Soursop (Annona muricata L.) ...... 24C Spanish lime (Melicoccus bijugatus Jacq.) ...... 24A Star apple (Chrysophyllum cainito L.) ...... 24B Sugar apple (Annona squamosa L.) ...... 24C Sun sapote (Licania platypus (Hemsl.) Fritsch) ...... 24C Tamarind-of-the-Indies (Vangueria madagascariensis J.F. Gmel.) ...... 24B Velvet tamarind (Dialium indum L.) ...... 24A Wampi (Clausena lansium (Lour.) Skeels) ...... 24A White star apple (Chrysophyllum albidum G. Don) ...... 24A Wild loquat (Uapaca kirkiana Mu¨ll. Arg.) ...... 24B Cultivars, varieties, and hybrids of these commodities.

(iii) Table. The following Table 2 commodities for each subgroup, and identifies the crop subgroups for Crop lists all the commodities included in Group 24, specifies the representative each subgroup.

TABLE 2—CROP GROUP 24: SUBGROUP LISTING

Representative commodities Commodities

Crop Subgroup 24A. Tropical and Subtropical, Small fruit, inedible peel subgroup

Lychee ...... Aisen; bael fruit; Burmese grape; cat’s-eyes; inga´; longan; lychee; madras-thorn; manduro; matisia; mesquite; mongongo, fruit; pawpaw, small-flower; satinleaf; Sierra Leone-tamarind; Spanish lime; velvet tamarind; wampi; white star apple; cultivars, varieties, and hybrids of these commodities.

Crop Subgroup 24B. Tropical and Subtropical, Medium to large fruit, smooth, inedible peel subgroup

Avocado, plus pomegranate or banana ...... Abiu; akee apple; avocado; avocado, Guatemalan; avocado, Mexican; avocado, West Indian; bacury; banana; banana, dwarf; binjai; canistel; cupuacu´; etambe; jatoba´; kei apple; langsat; lanjut; lucuma; mabolo; mango; mango, horse; mango, Saipan; mangosteen; paho; papaya; pawpaw, common; pelipisan; pequi; pequia; persimmon, American; plantain; pomegranate; poshte; quandong; sapote, black; sapote, green; sapote, white; sataw; screw-pine; star apple; tamarind-of-the-Indies; wild loquat; cultivars, varieties, and hybrids of these commodities.

Crop Subgroup 24C. Tropical and Subtropical, Medium to large fruit, rough or hairy, inedible peel subgroup

Pineapple, plus atemoya or sugar apple ...... Atemoya; biriba; breadfruit; champedak; cherimoya; custard apple; durian; elephant-apple; ilama; jackfruit; karuka; mammy-apple; marang; marmaladebox; monkey-bread tree; nicobar-breadfruit; pandanus; pineapple; pulasan; rambutan; sapodilla; sapote, mamey; soncoya; soursop; sugar apple; sun sapote; cultivars, varieties, and hybrids of these commodities.

Crop Subgroup 24D. Tropical and Subtropical, Cactus, inedible peel subgroup

Dragon fruit and Prickly pear fruit ...... Dragon fruit; pitahaya; pitaya; pitaya, amarilla; pitaya, roja; pitaya, yellow; prickly pear, fruit; prickly pear, Texas, fruit; saguaro; cultivars, varieties, and hybrids of these commodities.

Crop Subgroup 24E. Tropical and Subtropical, Vine, inedible peel subgroup

Passionfruit ...... Granadilla; granadilla, giant; monstera; passionflower, winged-stem; passionfruit; passionfruit, banana; passionfruit, purple; passionfruit, yellow; cultivars, varieties, and hybrids of these commodities.

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[60 FR 26635, May 17, 1995, as amended at 72 Parts per FR 69156, 69157, Dec. 7, 2007; 73 FR 52, Jan. 2, Commodity million 2008; 75 FR 76289, Dec. 8, 2010; 77 FR 50620, Aug. 22, 2012; 81 FR 26477, May 3, 2016] Blueberry ...... 20 .0 Caneberry, subgroup 13A ...... 25.0 Cherry, sweet ...... 50 .0 Subpart C—Specific Tolerances Cherry, tart ...... 50.0 Cotton, undelinted seed ...... 0 .05 Dill, seed ...... 0 .05 EDITORIAL NOTE: Nomenclature changes to Flax, seed ...... 0 .05 subpart C of part 180 appear at 67 FR 41803, Grape ...... 25 .0 June 19, 2002; 67 FR 42393, June 21, 2002; 68 FR Grain, cereal, forage, fodder and straw, group 39430, July 1, 2003; 71 FR 74804, Dec. 13, 2006; 16 ...... 0 .05 Grain, cereal, group 15 ...... 0.05 72 FR 53137, Sept. 18, 2007; 72 FR 61536, Oct. Grass, forage ...... 0 .05 31, 2007; 73 FR 60155, Oct. 10, 2008; 75 FR 56014, Grass, hay ...... 0 .05 Sept. 15, 2010; and 76 FR 34885, June 15, 2011. Nectarine ...... 25 .0 Okra ...... 0.05 § 180.101 Specific tolerances; general Peach ...... 15 .0 provisions. Peanut ...... 0 .05 Peanut, hay ...... 0.05 (a) The tolerances established for Pear ...... 25 .0 pesticide chemicals in this subpart C Plum, prune, fresh ...... 10.0 apply to residues resulting from their Rapeseed, forage ...... 0 .05 Rapeseed, seed ...... 0 .05 application prior to harvest or slaugh- Safflower, seed ...... 0 .05 ter, unless otherwise stated. Toler- Sesame, seed ...... 0 .05 ances are expressed in terms of parts Strawberry ...... 20.0 Sunflower, seed ...... 0.05 by weight of the pesticide chemical per Vegetable, brassica leafy, group 5 ...... 0 .05 one million parts by weight of the raw Vegetable, bulb, group 3 ...... 0 .05 agricultural commodity. Vegetable, cucurbit, group 9 ...... 0.05 (b) The poisonous and deleterious Vegetable, foliage of legume, group 7 ...... 0 .05 Vegetable, fruiting, group 8 ...... 0.05 substances for which tolerances are es- Vegetable, leafy, except brassica, group 4 ...... 0 .05 tablished by the regulations in this Vegetable, leaves of root and tuber, group 2 ..... 0 .05 subpart C are named by their common Vegetable, legume, group 6 ...... 0 .05 names wherever practicable, otherwise Vegetable, root and tuber, group 1 ...... 0 .05 by their chemical names. (2) Tolerances are established for the (c) The analytical methods to be used combined residues of the fungicide, for determining whether pesticide resi- captan (N-trichloromethylthio-4- dues, including negligible residues, in cyclohexene-1,2-dicarboximide) and its or on raw agricultural commodities are metabolite 1,2,3,6- in compliance with the tolerances es- tetrahydrophthalimide (THPI), meas- tablished in this part 180 are identified ured at THPI, in or on the following among the methods contained or ref- commodities: erenced in the Food and Drug Adminis- tration’s ‘‘Pesticide Analytical Man- Commodity Parts per ual’’ which is available from the Food million and Drug Administration, Department Cattle, fat ...... 0.15 of Health, Education, and Welfare, 200 Cattle, meat ...... 0 .20 C Street SW., Washington, DC 20204. Cattle, meat byproducts ...... 0.30 Goat, fat ...... 0 .15 Goat, meat ...... 0.20 § 180.103 Captan; tolerances for resi- Goat, meat byproducts ...... 0 .30 dues. Hog, fat ...... 0 .15 (a)(1) General. Tolerances are estab- Hog, meat ...... 0 .20 Hog, meat byproducts ...... 0 .30 lished for residues of the fungicide, Horse, fat ...... 0 .15 captan (N-trichloromethylthio-4- Horse, meat ...... 0 .20 cyclohexene-1,2-dicarboximide) in or on Horse, meat byproducts ...... 0 .30 Milk ...... 0.10 the following commodities: Sheep, fat ...... 0 .15 Sheep, meat ...... 0.20 Parts per Sheep, meat byproducts ...... 0 .30 Commodity million

Almond ...... 0.25 (b) Section 18 emergency exemptions. Almond, hulls ...... 75 .0 [Reserved] Animal feed, nongrass, group 18 ...... 0 .05 Apple ...... 25.0 (c) Tolerances with regional registra- Apricot ...... 10 .0 tions. [Reserved]

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(d) Indirect or inadvertent residues. Commodity Parts per [Reserved] million [72 FR 52016, Sept. 12, 2007] Wheat, grain ...... 0 .5 Wheat, hay ...... 2 § 180.106 Diuron; tolerances for resi- Wheat, straw ...... 1 .5 dues. (b) Section 18 emergency exemptions. (a) General. Tolerances are estab- [Reserved] lished for the combined residues of the herbicide diuron, 3-(3,4- (c) Tolerances with regional registra- dichlorophenyl)-1,1-dimethylurea and tions. Tolerances with a regional reg- its metabolites convertible to 3,4- istration as defined in § 180.1(l) are es- dichloroaniline in or on food commod- tablished for the combined residues of ities, as follows: the herbicide diuron (3-(3,4- dichlorophenyl)-1,1-dimethylurea and Commodity Parts per its metabolites convertible to 3,4- million dichloroaniline) in or on the raw agri- Alfalfa, forage ...... 3.0 cultural commodities: Alfalfa, hay ...... 2.0 Apple ...... 0.1 Commodity Parts per Artichoke, globe ...... 1 million Asparagus ...... 7 Banana ...... 0.1 Barley, bran ...... 0 .7 Berry group 13 ...... 0 .1 Barley, grain ...... 0 .2 Cattle, fat ...... 1 Barley, hay ...... 2 Cattle, meat ...... 1 Barley, straw ...... 1 .5 Cattle, meat byproducts ...... 1 Cactus ...... 0 .05 Citrus, oil ...... 3.0 Corn, field, grain ...... 0 .1 Clover, forage ...... 0.1 Corn, pop, grain ...... 0.1 Clover, hay ...... 1.0 Cotton, undelinted seed ...... 0 .2 Oat, forage ...... 2 Fish – freshwater finfish, farm raised ...... 2 .0 Oat, grain ...... 0 .1 Fruit, citrus, group 10, except lemon ...... 0 .05 Oat, hay ...... 2 Goat, fat ...... 1 Oat, straw ...... 1.5 Goat, meat ...... 1 Trefoil, forage ...... 0 .1 Goat, meat byproducts ...... 1 Trefoil, hay ...... 1 .5 Grain, aspirated fractions ...... 5 .0 Vetch, forage ...... 0 .1 Grape ...... 0 .05 Vetch, hay ...... 1 .5 Grass, forage, except bermudagrass ...... 2 Grass, hay, except bermudagrass ...... 2 Hazelnut ...... 0 .1 (d) Indirect or inadvertent residues. Hog, fat ...... 1 [Reserved] Hog, meat ...... 1 Hog, meat byproducts ...... 1 [63 FR 2164, Jan. 14, 1998, as amended at 63 Horse, fat ...... 1 FR 57072, Oct. 26, 1998; 64 FR 41305, July 30, Horse, meat ...... 1 Horse, meat byproducts ...... 1 1999; 66 FR 28671, May 24, 2001; 67 FR 46883, Lemon ...... 0.5 July 17, 2002; 69 FR 71717, Dec. 10, 2004; 72 FR Nut, macadamia ...... 0.05 32540, June 13, 2007; 72 FR 35666, June 29, 2007; Olive ...... 1 73 FR 54958, Sept. 24, 2008; 76 FR 34885, June Papaya ...... 0 .5 15, 2011] Peach ...... 0 .1 Pear ...... 1 Pea, field, seed ...... 0 .1 § 180.107 Triflumezopyrim; tolerance Pea, field, vines ...... 2 for residues. Pea, field, hay ...... 2 (a) General. Tolerances are estab- Pecan ...... 0 .05 Peppermint, tops ...... 1 .5 lished for residues of the insecticide Pineapple ...... 0.1 triflumezopyrim, including its metabo- Pineapple, process residue ...... 0 .4 lites and degradates, in or on the fol- Sheep, fat ...... 1 Sheep, meat ...... 1 lowing food commodities in the table Sheep, meat byproducts ...... 1 below. Compliance with the tolerance Sorghum, grain, forage ...... 2 levels specified below is to be deter- Sorghum, grain, grain ...... 0 .5 mined by measuring only Sorghum, grain, stover ...... 2 Spearmint, tops ...... 1 .5 triflumezopyrim (2,4-dioxo-1-(5- Sugarcane, cane ...... 0.2 pyrimidinylmethyl)-3-[3- Sugarcane, molasses ...... 0 .7 (trifluoromethyl)phenyl]-2H-pyrido[1,2- Walnut ...... 0 .05 Wheat, bran ...... 0.7 a] pyrimidinium inner salt) in or on Wheat, forage ...... 2 the commodity.

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Parts per 1 Parts per Commodity million Commodity million

Rice, grain * ...... 0 .40 Soybean, seed ...... 1 .0 Rice, hulls * ...... 1 .0 1 Where there is a direct use of methamidophos on the * There are no U.S. registrations for the use of commodity, residues of methamidophos resulting from triflumezopyrim on these commodities. methamidophos application are regulated under 40 CFR 180.315. (b) Section 18 emergency exemptions. (2) A tolerance of 0.02 ppm is estab- [Reserved] lished for residues of acephate, O,S-di- (c) Tolerances with regional registra- methyl acetyl phosphoramidothioate, tions. [Reserved] including its metabolites and (d) Indirect or inadvertent residues. degradates other than methamidophos, [Reserved] in or on all food items (other than [82 FR 48005, Oct. 16, 2017] those already covered by a higher tolerance as a result of use on growing § 180.108 Acephate; tolerances for resi- crops) in food handling establishments dues. where food and food products are held, (a) General. (1) Tolerances are estab- processed, prepared and served, includ- lished for residues of acephate, O,S-di- ing food service, manufacturing and methyl acetyl phosphoramidothioate, processing establishments, such as res- including its metabolites and taurants, cafeterias, supermarkets, degradates other than methamidophos, bakeries, breweries, dairies, meat in or on the commodities in the fol- slaughtering and packing plants, and lowing table. Compliance with the tol- canneries, where application of erance levels specified in this para- acephate shall be limited solely to spot graph is to be determined by measuring and/or crack and crevice treatment (a only acephate, O,S-dimethyl acetyl coarse, low-pressure spray shall be used phosphoramidothioate, in or on the to avoid atomization or splashing of commodity. the spray for spot treatments; equipment capable of delivering a pin- Parts per Commodity 1 stream of insecticide shall be used for million crack and crevice treatments). Spray Bean, dry, seed ...... 3 .0 concentration shall be limited to a Brussels sprouts ...... 3 .0 maximum of 1.0 percent active ingre- Cattle, fat ...... 0.1 dient. Contamination of food or food- Cattle, meat ...... 0 .1 contact surfaces shall be avoided. Com- Cattle, meat byproducts ...... 0.1 Cauliflower ...... 2 .0 pliance with the tolerance levels speci- Celery ...... 10 fied in this paragraph is to be deter- Cotton, hulls ...... 1 .0 mined by measuring only acephate, Cotton, meal ...... 1 .0 O,S-dimethyl acetyl Cotton, undelinted seed ...... 0 .5 Cranberry ...... 0 .5 phosphoramidothioate, in or on the Egg ...... 0 .1 commodity. Goat, fat ...... 0 .1 (3) Tolerances are established for res- Goat, meat ...... 0.1 idues of methamidophos, O,S-dimethyl Goat, meat byproducts ...... 0 .1 phosphoramidothioate, including its Hog, fat ...... 0 .1 Hog, meat ...... 0 .1 metabolites and degradates, in or on Hog, meat byproducts ...... 0 .1 the commodities in the following table Horse, fat ...... 0 .1 as a result of the application of Horse, meat ...... 0 .1 acephate. Compliance with the toler- Horse, meat byproducts ...... 0 .1 Lettuce, head ...... 10 ance levels specified in this paragraph Milk ...... 0.1 is to be determined by measuring only Peanut ...... 0 .2 methamidophos, O,S-dimethyl Pepper ...... 4 .0 phosphoramidothioate, in or on the Peppermint, tops ...... 27 Poultry, fat ...... 0.1 commodity. Poultry, meat ...... 0 .1 Parts per Poultry, meat byproducts ...... 0.1 Commodity million Sheep, fat ...... 0 .1 Sheep, meat ...... 0.1 Bean, dry, seed ...... 1 Sheep, meat byproducts ...... 0 .1 Brussels sprouts ...... 0 .5 Spearmint, tops ...... 27 Cauliflower ...... 0 .5

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Parts per Parts per Commodity million Commodity million

Celery ...... 1 Rye, grain* ...... 0 .60 Cranberry ...... 0 .1 *There are no U.S. registrations for use of fenpicoxamid on Lettuce, head ...... 1 this commodity. Pepper ...... 1 Peppermint, tops ...... 1 (b) Section 18 emergency exemptions. Spearmint, tops ...... 1 [Reserved] (c) Tolerances with regional registra- (b) Section 18 emergency exemptions. tions. [Reserved] [Reserved] (d) Indirect or inadvertent residues. (c) Tolerances with regional registra- [Reserved] tions. A tolerance with a regional registration is established for residues of [82 FR 48000, Oct. 16, 2017] acephate, O,S-dimethyl acetyl § 180.111 Malathion; tolerances for res- phosphoramidothioate, including its idues. metabolites and degradates other than (a) General. (1) Tolerances are estab- methamidophos, in or on the com- lished for residues of the insecticide modity in the following table. Compli- malathion (O,O-dimethyl ance with the tolerance level specified dithiophosphate of diethyl in this paragraph is to be determined mercaptosuccinate) in or on the fol- by measuring only acephate, O,S-di- lowing food commodities: methyl acetyl phosphoramidothioate, in or on the commodity. Parts per Commodity million

1 Parts per Commodity million Alfalfa, forage ...... 135 Alfalfa, hay ...... 135 Nut, macadamia ...... 0.05 Almond, hulls ...... 50 Almond, postharvest ...... 8 1 Where there is a direct use of methamidophos on the Apple ...... 8 commodity, residues of methamidophos resulting from Apricot ...... 8 methamidophos application are regulated under 40 CFR 180.315. Asparagus ...... 8 Avocado ...... 8 (d) Indirect or inadvertent residues. Barley, grain, postharvest ...... 8 Bean, dry, seed ...... 8 [Reserved] Bean, succulent ...... 8 [63 FR 13542, Mar. 20, 1998, as amended at 67 Beet, garden, roots ...... 8 Beet, garden, tops ...... 8 FR 49615, July 31, 2002; 73 FR 5108, Jan. 29, Beet, sugar, roots ...... 1 2008; 75 FR 60237, Sept. 29, 2010; 81 FR 34905, Beet, sugar, tops ...... 8 June 1, 2016] Blackberry ...... 8 Blueberry ...... 8 § 180.109 Fenpicoxamid; Tolerances for Boysenberry ...... 8 residues. Carrot, roots ...... 8 Chayote, fruit ...... 8 (a) General. Tolerances are estab- Chayote, roots ...... 8 lished for residues of fenpicoxamid in- Cherry ...... 8 Chestnut ...... 1 cluding its metabolites and degradates, Clover, forage ...... 135 in or on the commodities in the table Clover, hay ...... 135 below. Compliance with the tolerance Corn, field, forage ...... 8 Corn, field, grain, postharvest ...... 8 levels for fenpicoxamid is to be deter- Corn, pop, grain, postharvest ...... 8 mined by measuring only fenpicoxamid Corn, sweet, forage ...... 8 ([[4-methoxy-2-[[[(3S,7R,8R,9S)-9-meth- Corn, sweet, kernel plus cob with husks re- yl-8-(2-methyl-1-oxopropoxy)-2,6-dioxo- moved ...... 2 Cowpea, forage ...... 135 7-(phenylmethyl)-1,5-dioxonan-3- Cowpea, hay ...... 135 yl]amino]carbonyl]-3- Cranberry ...... 8 pyridinyl]oxy]methyl 2- Cucumber ...... 8 Currant ...... 8 methylpropanoate) in or on the com- Date, dried fruit ...... 8 modity. Dewberry ...... 8 Eggplant ...... 8 Fig ...... 8 Commodity Parts per million Flax, seed ...... 0 .1 Garlic, bulb ...... 8 Banana* ...... 0 .15 Gooseberry ...... 8 Wheat, grain* ...... 0 .60 Grape ...... 8

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Parts per Parts per Commodity million Commodity million

Grapefruit ...... 8 Walnut ...... 8 Guava ...... 8 Wheat, grain, postharvest ...... 8 Hazelnut ...... 1 Hop, dried cones ...... 1 (2) Tolerances are established for the Horseradish ...... 8 Kumquat ...... 8 combined residues of the insecticide Leek ...... 8 malathion (O,O-dimethyl Lemon ...... 8 dithiophosphate of diethyl Lentil, seed ...... 8 Lespedeza, hay ...... 135 mercaptosuccinate) and its metabolite, Lime ...... 8 malaoxon (O,O-dimethyl thiophosphate Loganberry ...... 8 of diethyl mercaptosuccinate), in or on Lupin, seed ...... 8 Mango ...... 8 the following food commodities: Melon ...... 8 Mushroom ...... 8 Commodity Parts per Nectarine ...... 8 million Nut, macadamia ...... 1 Barley, straw ...... 50 Oat, grain, postharvest ...... 8 Corn, field, stover ...... 30 .0 Okra ...... 8 Onion, bulb ...... 8 Cotton, undelinted seed ...... 20 .0 Onion, green ...... 8 Grass, forage ...... 200 Orange ...... 8 Grass, hay ...... 270 Papaya ...... 1 Oat, forage ...... 4 .0 Parsnip ...... 8 Oat, straw ...... 50 Passionfruit ...... 8 Rye, forage ...... 4 .0 Pea ...... 8 Rye, straw ...... 50 Pea, field, hay ...... 8 Watercress ...... 0 .2 Pea, field, vines ...... 8 Wheat, forage ...... 4 .0 Peach ...... 8 Wheat, straw ...... 50 Peanut, hay ...... 135 Peanut, postharvest ...... 8 (3) Tolerances are established for res- Pear ...... 8 idues of the insecticide malathion Pecan ...... 8 Pepper ...... 8 (O,O-dimethyl dithiophosphate of Peppermint, tops ...... 8 diethyl mercaptosuccinate), in or on Pineapple ...... 8 the following food commodities: Plum ...... 8 Plum, prune ...... 8 Parts per Potato ...... 8 Commodity million Pumpkin ...... 8 Quince ...... 8 Cattle, fat ...... 4 Radish ...... 8 Cattle, meat1 ...... 4 Raspberry ...... 8 Cattle, meat byproducts1 ...... 4 Rice, grain, postharvest ...... 8 Egg ...... 0 .1 Rice, wild ...... 8 Goat, fat ...... 4 Rutabaga ...... 8 Goat, meat1 ...... 4 Rye, grain, postharvest ...... 8 Goat, meat byproducts1 ...... 4 Safflower, seed ...... 0 .2 Hog, fat ...... 4 Salsify, roots ...... 8 Hog, meat1 ...... 4 Salsify, tops ...... 8 Hog, meat byproducts1 ...... 4 Shallot, bulb ...... 8 Horse, fat ...... 4 Sorghum, grain, forage ...... 8 Horse, meat1 ...... 4 Sorghum, grain, grain, postharvest ...... 8 Horse, meat byproducts1 ...... 4 Soybean, forage ...... 135 Milk, fat ...... 0 .5 Soybean, hay ...... 135 Poultry, fat ...... 4 Soybean, seed ...... 8 Poultry, meat1 ...... 4 Soybean, vegetable, succulent ...... 8 Poultry, meat byproducts1 ...... 4 Spearmint, tops ...... 8 Sheep, fat ...... 4 Squash, summer ...... 8 Sheep, meat1 ...... 4 Squash, winter ...... 8 Sheep, meat byproducts1 ...... 4 Strawberry ...... 8 Sunflower, seed, postharvest ...... 8 1 The tolerance level shall not be exceeded in any cut of Sweet potato, roots ...... 1 meat or in any meat byproducts from cattle, goat, hog, horse, Tangerine ...... 8 poultry, or sheep. Tomato ...... 8 (4) Malathion may be safely used in Trefoil, forage ...... 135 Trefoil, hay ...... 135 accordance with the following condi- Turnip, greens ...... 8 tions: Turnip, roots ...... 8 (i) It is incorporated into paper trays Vegetable, brassica, leafy, group 5 ...... 8 Vegetable, leafy, except brassica, group 4 ...... 8 in amounts not exceeding 100 milli- Vetch, hay ...... 135 grams per square foot.

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(ii) Treated paper trays are intended § 180.114 Ferbam; tolerances for resi- for use only in the drying of grape (rai- dues. sins). (a) General. Tolerances are estab- (iii) Total residues of malathion re- lished for residues of the fungicide sulting from drying of grape on treated ferbam (ferric trays and from application to grape be- dimethyldithiocarbamate), calculated fore harvest shall not exceed 12 parts as carbon disulfide, in or on the fol- per million on processed ready-to-eat lowing food commodities: raisins. (5) Residues of malathion in saf- Expiration/ Commodity Parts per Revocation flower, refined oil from application to million Date the growing safflower plant shall not Apple ...... 4.0 1 None exceed 0.6 parts per million. Bean ...... 7.0 1 10/27/07 (6) Malathion may be safely used for Cabbage ...... 7.0 1 10/27/07 the control of insects during the drying Cherry ...... 4.0 1 None Cranberry ...... 4.0 1 None of grape (raisins) in compliance with Fruit, citrus, group 10 ...... 4.0 1 None paragraph (a)(4) of this section by in- Grape ...... 4.0 1 None corporation into paper trays in Lettuce ...... 7.0 1 10/27/07 Nectarine ...... 4.0 1 None amounts not exceeding 100 milligrams Peach ...... 4.0 1 None per square foot. Pear ...... 4.0 1 None (7) Malathion (O,O-dimethyl Raspberry ...... 7.0 1 10/27/07 dithiophosphate of diethyl 1Some of these tolerances were established on the basis of mercaptosuccinate) may be safely used data acquired at the public hearings held in 1950 (formerly § 180.101) and the remainder were established on the basis in feed in accordance with the fol- of pesticide petitions presented under the procedure specified lowing conditions. in the amendment to the Federal Food, Drug, and Cosmetic Act by Pub. L. 518, 83d Congress (68 Stat. 511) (i) A tolerance of 50 parts per million is established for residues of malathion (b) Section 18 emergency exemptions. in citrus, dried pulp for cattle feed, [Reserved] when present as the result of the appli- (c) Tolerances with regional registra- cation of the pesticide to bagged citrus tions. Tolerances with regional reg- pulp during storage. Whether or not istrations, as defined in § 180.1(l), are tolerances for residues of malathion on established for residues of the fun- the fresh fruit have been established gicide ferbam (ferric under section 408 of the Act, the total dimethyldithiocarbamate), calculated residue of malathion in the citrus, as carbon disulfide, in or on the fol- dried pulp shall not exceed 50 parts per lowing food commodities: million. Parts per (ii) A tolerance of 10 parts per million Commodity million is established for malathion in non- Mango ...... 4.0 1 medicated cattle feed concentrate 1 This tolerance was established on the basis of data ac- blocks resulting from its application as quired at the public hearings held in 1950 (formerly § 180.101) a pesticide to paper used in packaging and the remainder was established on the basis of pesticide petitions presented under the procedure specified in the the nonmedicated cattle feed con- amendment to the Federal Food, Drug, and Cosmetic Act by centrate blocks. Pub. L. 518, 83d Congress (68 Stat. 511) (b) Section 18 emergency exemptions. (d) Indirect or inadvertent residues. [Reserved] [Reserved] (c) Tolerances with regional registrations. [Reserved] [63 FR 57072, Oct. 26, 1998, as amended at 72 (d) Indirect or inadvertent residues. FR 53453, Sept. 19, 2007] [Reserved] § 180.116 Ziram; tolerances for resi- [43 FR 22974, May 30, 1978, as amended at 43 dues. FR 45584, Oct. 3, 1978; 44 FR 38844, July 3, (a) General. Tolerances are estab- 1979; 45 FR 76145, Nov. 18, 1980; 47 FR 42738, lished for residues of the fungicide Sept. 29, 1982; 47 FR 55226, Dec. 8, 1982; 52 FR ziram (zinc dimethyldithiocarbamate), 45183, Nov. 25, 1987; 62 FR 66023, 66025, Dec. 17, 1997; 65 FR 33694, May 24, 2000; 72 FR 35665, including its metabolites and June 29, 2007; 73 FR 54959, Sept. 24, 2008; 74 FR degradates, in or on the commodities 47455, Sept. 16, 2009; 75 FR 60238, Sept. 29, in the table below as a result of the ap- 2010] plication of ziram. Compliance with

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the tolerance levels specified below is Commodity Parts per to be determined by measuring total million dithiocarbamates, determined as CS2, Alfalfa, forage ...... 0.2 evolved during acid digestion and ex- Alfalfa, hay ...... 0.6 pressed as zinc Almond ...... 0.08 Almond, hulls ...... 0 .08 ethylenebisdithiocarbamate. Bean, dry, seed ...... 0 .08 Bean, succulent ...... 0 .08 Commodity Parts per Beet, garden, tops ...... 0 .5 million Beet, sugar, molasses ...... 0 .4 Beet, sugar, tops ...... 0.5 1 Almond ...... 0 .10 Clover, forage ...... 0.1 1 Apple ...... 7 .0 Clover, hay ...... 0.1 Apricot ...... 1 7 .0 Corn, field, forage ...... 0 .08 Blueberry ...... 1 7 .0 Corn, field, grain ...... 0 .08 Cherry, sweet ...... 1 7 .0 Corn, field, stover ...... 0 .08 Cherry, tart ...... 1 7 .0 Corn, pop, grain ...... 0.08 Grape ...... 7 .0 Corn, pop, stover ...... 0.08 Hazelnut ...... 0 .10 Corn, sweet, forage ...... 0 .08 Huckleberry ...... 7 .0 Corn, sweet, kernel plus cob with husks re- Peach ...... 7 .0 moved ...... 0 .08 Pear ...... 1 7 .0 Corn, sweet, stover ...... 0 .08 Pecan ...... 0 .10 Cotton, gin byproducts ...... 0 .20 Quince ...... 1 7 .0 Cotton, undelinted seed ...... 0 .08 Strawberry ...... 7 .0 Fruit, citrus, group 10 ...... 0 .1 Tomato ...... 1 7 .0 Grass, forage ...... 0 .60 Grass, hay ...... 0 .50 1 Some of these tolerances were established on the basis of Lespedeza, forage ...... 0 .1 data acquired at the public hearings held in 1950 (formerly § 180.101) and the remainder were established on the basis Lespedeza, hay ...... 0.1 of pesticide petitions presented under the procedure specified Pea, succulent ...... 0 .08 in the amendment to the Federal Food, Drug, and Cosmetic Safflower, seed ...... 0 .08 Act by Public Law 518, 83d Congress (68 Stat. 511). Sunflower, seed ...... 0.08 Tomato ...... 0.08 (b) Section 18 emergency exemptions. Trefoil, forage ...... 0 .1 [Reserved] Trefoil, hay ...... 0 .1 (c) Tolerances with regional registra- Vegetable, root ...... 0 .1 tions. [Reserved] Walnut ...... 0 .08 (d) Indirect or inadvertent residues. (b) Section 18 emergency exemptions. [Reserved] [Reserved] [68 FR 39437, July 1, 2003, as amended at 71 (c) Tolerances with regional registra- FR 54432, Sept. 15, 2006; 73 FR 54959, Sept. 24, tions. [Reserved] 2008; 77 FR 59123, Sept. 26, 2012; 82 FR 57860, (d) Indirect or inadvertent residues. Dec. 8, 2017] [Reserved] § 180.117 S-Ethyl [75 FR 60239, Sept. 29, 2010, as amended at 82 dipropylthiocarbamate; tolerances FR 42952, Sept. 13, 2017] for residues. § 180.123 Inorganic bromide residues (a) General. Tolerances are estab- resulting from fumigation with lished for residues of the herbicide S- methyl bromide; tolerances for resi- ethyl dipropylthiocarbamate, including dues. its metabolites and degradates, in or (a) General. (1) Tolerances are estab- on the commodities in the following lished for residues of inorganic bro- table. Compliance with the tolerance mides (calculated as Br) in or on the levels specified in this paragraph is to following food commodities which have be determined by measuring only the been fumigated with the antimicrobial sum of S-ethyl dipropylthiocarbamate, agent and insecticide methyl bromide S-ethyl (2- after harvest (with the exception of hydroxypropyl)propylcarbamothioate, strawberry): S-(2-hydroxyethyl)dipropylcarbamothioate, and S- Parts per Expiration/ ethyl (3- Commodity million Revocation Date hydroxypropyl)propylcarbamothioate, calculated as the stoichiometric equiv- Alfalfa, hay, postharvest ...... 50.0 10/31/11 alent of S-ethyl Almond, postharvest ...... 200.0 None Apple, postharvest ...... 5.0 None dipropylthiocarbamate, in or on the Apricot, postharvest ...... 20.0 None commodity. Artichoke, jerusalem, postharvest ... 30.0 None

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Expiration/ Expiration/ Commodity Parts per Revocation Commodity Parts per Revocation million Date million Date

Asparagus, postharvest ...... 100.0 None Rutabaga, tops, postharvest ...... 30.0 None Avocado, postharvest ...... 75.0 None Rye, grain, postharvest ...... 50.0 None Barley, grain, postharvest ...... 50.0 None Salsify, roots, postharvest ...... 30.0 None Bean, lima, postharvest ...... 50.0 None Sorghum, grain, grain, postharvest 50.0 None Bean, postharvest ...... 50.0 None Soybean, postharvest ...... 200.0 None Bean, snap, succulent, postharvest 50.0 None Bean, succulent, postharvest ...... 50.0 None Squash, summer, postharvest ...... 30.0 None Beet, garden, roots, postharvest ..... 30.0 None Squash, winter, postharvest ...... 20.0 None Beet, sugar, roots, postharvest ...... 30.0 None Squash, zucchini, postharvest ...... 20.0 None Blueberry, postharvest ...... 20.0 None Strawberry, postharvest ...... 60.0 None Butternut, postharvest ...... 200.0 None Sweet potato, postharvest ...... 75.0 None Cabbage, postharvest ...... 50.0 None Tangerine, postharvest ...... 30.0 None Cacao bean, roasted bean, Timothy, hay, postharvest ...... 50.0 10/19/10 postharvest ...... 50.0 None Tomato, postharvest ...... 20.0 None Cantaloupe, postharvest ...... 20.0 None Turnip, roots, postharvest ...... 30.0 None Carrot, roots, postharvest ...... 30.0 None Walnut, postharvest ...... 200.0 None Cashew, postharvest ...... 200.0 None Cherry, sweet, postharvest ...... 20.0 None Watermelon, postharvest ...... 20.0 None Cherry, tart, postharvest ...... 20 None Wheat ...... 50.0 None Chestnut, postharvest ...... 200.0 None Cippolini, bulb, postharvest ...... 50.0 None (2) Inorganic bromide may be present Citron, citrus, postharvest ...... 30.0 None as a residue in certain processed food Coconut, copra, postharvest ...... 100.0 None Coffee, bean, green, postharvest .... 75.0 None in accordance with the following condi- Corn, field, grain, postharvest ...... 50.0 None tions: Corn, pop, postharvest ...... 240.0 None (i) When inorganic bromide residues Corn, sweet, kernel plus cob with husks removed, postharvest ...... 50.0 None are present as a result of fumigation of Cotton, undelinted seed, the processed food with methyl bro- postharvest ...... 200.0 10/31/11 mide or from such fumigation in addi- Cucumber, postharvest ...... 30.0 None Cumin, seed, postharvest ...... 100.0 None tion to the authorized use of methyl Eggplant, postharvest ...... 20.0 None bromide on the source raw agricultural Garlic, postharvest ...... 50.0 None commodity, as provided for in this Ginger, postharvest ...... 100.0 None part, the total residues of inorganic Grape, postharvest ...... 20.0 None Grapefruit, postharvest ...... 30.0 None bromides (calculated as Br) shall not Hazelnut, postharvest ...... 200.0 None exceed the following levels: Horseradish, postharvest ...... 30.0 None (A) 400 parts per million in or on egg, Kumquat, postharvest ...... 30.0 None Lemon, postharvest ...... 30.0 None dried and herb, processed and spice. Lime, postharvest ...... 30.0 None (B) 325 parts per million in or on Melon, honeydew, postharvest ...... 20.0 None cheese, parmesan and cheese, roquefort Muskmelon, postharvest ...... 20.0 None Nectarine, postharvest ...... 20.0 None cheese. Nut, brazil, postharvest ...... 200.0 None (C) 250 parts per million in or on to- Nut, hickory, postharvest ...... 200.0 None mato, concentrated products and fig, Nut, macadamia, postharvest ...... 200.0 None Oat, postharvest ...... 50.0 None dried fruit. Okra, postharvest ...... 30.0 None (D) 125 parts per million in or on Onion, bulb, postharvest ...... 20.0 None processed food other than those listed Onion, green, postharvest ...... 20.0 None above. Orange, postharvest ...... 30.0 None Parsnip, roots, postharvest ...... 30.0 None (ii) When inorganic bromide residues Peach, postharvest ...... 20.0 None are present in malt beverage, fer- Peanut, postharvest ...... 200.0 None mented in accordance with 21 CFR Pear, postharvest ...... 5.0 None Pea, blackeyed, postharvest ...... 50.0 None 172.730(a)(2), the amount shall not ex- Pea, postharvest ...... 50.0 None ceed 25 parts per million (calculated as Pecan, postharvest ...... 200.0 None Br). Pepper, postharvest ...... 30.0 None Pimento, postharvest ...... 30.0 None (iii) Where tolerances are established Pineapple, postharvest ...... 20.0 None on both the raw agricultural commod- Pistachio, postharvest ...... 200.0 None ities and processed food made there- Plum, postharvest ...... 20.0 None from, the total residues of inorganic Pomegranate, postharvest ...... 100.0 None Potato, postharvest ...... 75.0 None bromides in or on the processed food Pumpkin, postharvest ...... 20.0 None shall not be greater than those des- Quince, postharvest ...... 5.0 None ignated in paragraph (a)(2) of this sec- Radish, postharvest ...... 30.0 None Rice, grain, postharvest ...... 50.0 None tion, unless a higher level is estab- Rutabaga, roots, postharvest ...... 30.0 None lished elsewhere in this part.

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(3) Tolerances are established for res- taining residues of inorganic bromides idues of inorganic bromides (calculated from the use of methyl bromide are un- as Br) as follows: suitable as an ingredient in the feed of (i) 400 parts per million for residues meat and dairy animals and should not in or on dog food, resulting from fumi- be represented, sold, or used for that gation with methyl bromide. purpose. (ii) 125 parts per million for residues [58 FR 65555, Dec. 15, 1993] in or on processed commodities for animal feedstuffs from barley, corn, grain § 180.124 Methyl bromide; tolerances sorghum, oat, rice, rye and wheat, re- for residues. sulting directly from fumigation with (a) General. A tolerance is established methyl bromide or from carryover and for residues of the fumigant methyl concentration of residues of inorganic bromide, including metabolites and bromides from fumigation of the grains degradates, in or on the commodity in with methyl bromide. the table below. Compliance with the (b) Section 18 emergency exemptions. tolerance level specified below is to be [Reserved] determined by measuring only methyl (c) Tolerances with regional registra- bromide. tions. A tolerance with regional registration, as defined in § 180.1(l), is es- Commodity Parts per tablished for residues of inorganic bro- million mides (calculated as Br) in or on the Cotton, undelinted seed ...... 150 following food commodity grown in soil fumigated with methyl bromide. (b) Section 18 emergency exemptions. Time-limited tolerances as listed in Parts per the following table are established for Commodity million residues of the fumigant methyl bro- Ginger, postharvest ...... 100 mide, including its metabolites and degradates, in or on the specified agri- (d) Indirect or inadvertent residues. cultural commodities, resulting from [Reserved] use of the pesticide pursuant to FIFRA [71 FR 74812, Dec. 13, 2006, as amended at 75 section 18 emergency exemptions. Com- FR 60239, Sept. 29, 2010] pliance with the tolerance levels specified below is to be determined by meas- § 180.123a Inorganic bromide residues uring only methyl bromide. These tol- in peanut hay and peanut hulls; erances expire and are revoked on the statement of policy. date indicated in the table. (a) Investigations by the Food and Parts per Expiration Drug Administration show that peanut Commodity million date hay and peanut shells have been used as feed for meat and dairy animals. Avocado ...... 5.0 12/31/20 Banana ...... 5.0 12/31/20 While many growers now harvest pea- Cactus ...... 3.0 12/31/20 nuts with combines and leave the hay Coconut, copra ...... 8.0 12/31/20 on the ground to be incorporated into Coffee, green bean ...... 150 12/31/20 Cola ...... 150 12/31/20 the soil, some growers follow the prac- Cucurbit, seed ...... 150 12/31/20 tice of curing peanuts on the vines in a Fig ...... 10 12/31/20 stack and save the hay for animal feed. Fruit, berry and small fruit, group 13–07 ...... 5.0 12/31/20 Peanut shells or hulls have been used Fruit, stone, group 12–12 ...... 5.0 12/31/20 to a minor extent as roughage for cat- Herb and spice, group 19 ...... 35 12/31/20 tle feed. It has been established that Hibiscus, seed ...... 150 12/31/20 Ivy gourd ...... 5.0 12/31/20 the feeding to cattle of peanut hay and Kaffir lime, leaves ...... 0.50 12/31/20 peanut hulls containing residues of in- Kenaf, seed ...... 150 12/31/20 organic bromides will contribute con- Longan ...... 5.0 12/31/20 siderable residues of inorganic bro- Lychee ...... 5.0 12/31/20 Oilseed group 20 ...... 150 12/31/20 mides to the meat and milk. Peppermint, tops ...... 35 12/31/20 (b) There are no tolerances for inor- Pointed gourd ...... 5.0 12/31/20 ganic bromides in meat and milk to Pomegranate ...... 5.0 12/31/20 Rambutan ...... 5.0 12/31/20 cover residues from use of such peanut Spanish lime ...... 5.0 12/31/20 hulls as animal feed. Peanut hulls con- Spearmint, tops ...... 35 12/31/20

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Parts per Expiration Parts per Commodity million date Commodity million

Stalk, stem and leaf petiole vege- Hog, meat ...... 0 .1 table group 22 ...... 0.50 12/31/20 Hog, meat byproducts ...... 0 .1 Tropical and subtropical fruits, edi- Horse, fat ...... 0 .1 ble peel, group 23 ...... 10 12/31/20 Horse, meat ...... 0 .1 Tropical and subtropical fruits, ined- Horse, meat byproducts ...... 0 .1 ible peel, group 24 ...... 5.0 12/31/20 Loganberry, postharvest ...... 8 Vegetable, bulb, group 3–07 ...... 2.0 12/31/20 Mango, postharvest ...... 8 Vegetable, cucurbit, group 9 ...... 5.0 12/31/20 Milk, fat ...... 0 .25 Vegetable, foliage of legume, group Muskmelon, postharvest ...... 8 7 ...... 0.50 12/31/20 Oat, postharvest ...... 8 Vegetable, fruiting, group 8–10 ...... 7.0 12/31/20 Orange, postharvest ...... 8 Vegetable, Head and Stem Bras- Peach, postharvest ...... 8 sica, group 5–16 ...... 1.0 12/31/20 Peanut, postharvest ...... 8 Vegetable, leafy, group 4–16 ...... 0.50 12/31/20 Pea, postharvest ...... 8 Vegetable, leaves of root and tuber, Pear, postharvest ...... 8 group 2 ...... 0.50 12/31/20 Vegetable, legume, group 6 ...... 3.0 12/31/20 Pineapple, postharvest ...... 8 Vegetable, root and tuber, group 1 3.0 12/31/20 Plum, prune, fresh, postharvest ...... 8 Potato, postharvest ...... 0 .25 Poultry, fat ...... 3 (c) Tolerances with regional registra- Poultry, meat ...... 3 tions. [Reserved] Poultry, meat byproducts ...... 3 (d) Indirect or inadvertent residues. Raspberry, postharvest ...... 8 [Reserved] Rice, postharvest ...... 20 Rye, postharvest ...... 20 [77 FR 35298, June 13, 2012, as amended at 83 Sheep, fat ...... 0 .1 FR 8763, Mar. 1, 2018] Sheep, meat ...... 0.1 Sheep, meat byproducts ...... 0 .1 Sorghum, grain, postharvest ...... 8 § 180.127 Piperonyl butoxide; toler- Sweet potato, postharvest ...... 0 .25 ances for residues. Tomato, postharvest ...... 8 (a) General. (1) Tolerances for resi- Walnut, postharvest ...... 8 dues of the insecticide piperonyl Wheat, postharvest ...... 20 butoxide [(butyl carbityl)(6-propyl (2) Piperonyl butoxide may be safely piperonyl)ether] are established in or used in accordance with the following on the following food commodities: prescribed conditions: (i) It is used or intended for use in Commodity Parts per million combination with pyrethrins for con- Almond, postharvest ...... 8 trol of insects: Apple, postharvest ...... 8 (A) In cereal grain mills and in stor- Barley, postharvest ...... 20 age areas for milled cereal grain prod- Bean, postharvest ...... 8 Birdseed, mixtures, postharvest ...... 20 ucts, whereby the amount of piperonyl Blackberry, postharvest ...... 8 butoxide is at least equal to but not Blueberry, postharvest ...... 8 more than 10 times the amount of Boysenberry, postharvest ...... 8 pyrethrins in the formulation. Buckwheat, grain, postharvest ...... 20 Cattle, fat ...... 0.1 (B) On the outer ply of multiwall Cattle, meat ...... 0 .1 paper bags of 50 pounds or more capac- Cattle, meat byproducts ...... 0.1 ity in amounts not exceeding 60 milli- Cherry, sweet, postharvest ...... 8 Cherry, tart, postharvest ...... 8 grams per square foot, whereby the Cacoa bean, roasted bean, postharvest ...... 8 amount of piperonyl butoxide is equal Coconut, copra, postharvest ...... 8 to 10 times the amount of pyrethrins in Corn, field, grain, postharvest ...... 20 Corn, pop, postharvest ...... 20 the formulation. Such treated bags are Cotton, undelinted seed, postharvest ...... 8 to be used only for food, dried. Crabapple, postharvest ...... 8 (C) On cotton bags of 50 pounds or Currant, postharvest ...... 8 Dewberry, postharvest ...... 8 more capacity in amounts not exceed- Egg ...... 1 ing 55 milligrams per square foot of Fig, postharvest ...... 8 cloth, whereby the amount of piperonyl Flax, seed, postharvest ...... 8 butoxide is equal to 10 times the Goat, fat ...... 0 .1 Goat, meat ...... 0.1 amount of pyrethrins in the formula- Goat, meat byproducts ...... 0 .1 tion. Such treated bags are constructed Gooseberry, postharvest ...... 8 with waxed paper liners and are to be Grape, postharvest ...... 8 Guava, postharvest ...... 8 used only for food, dried that contain 4 Hog, fat ...... 0 .1 percent fat or less.

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(D) In two-ply bags consisting of cel- (3) Piperonyl butoxide may be safely lophane/polyolefin sheets bound to- used in accordance with the following gether by an adhesive layer when it is prescribed conditions: incorporated in the adhesive. The (i) It is used or intended for use in treated sheets shall contain not more combination with pyrethrins for con- than 50 milligrams of piperonyl trol of insects: butoxide per square foot (538 milli- (A) On the outer ply of multiwall grams per square meter). Such treated paper bags of 50 pounds or more capac- bags are to be used only for packaging ity in amounts not exceeding 60 milli- plum, prune, dried; grape, raisin; and grams per square foot. other fruit, dried and are to have a (B) On cotton bags of 50 pounds or maximum ratio of 3.12 milligrams of more capacity in amounts not exceed- piperonyl butoxide per ounce of fruit ing 55 milligrams per square foot of (0.10 milligram of piperonyl butoxide cloth. Such treated bags are con- per gram of product). structed with waxed paper liners and (E) In food processing and food stor- are to be used only for feed, dried that age areas: Provided, That the food is contain 4 percent fat or less. removed or covered prior to such use. (ii) It is used in combination with pyrethrins, whereby the amount of (ii) It is used or intended for use in piperonyl butoxide is equal to 10 times combination with pyrethrins and N- the amount of pyrethrins in the formu- octylbicycloheptene dicarboximide for lation. Such treated bags are to be used insect control in accordance with 21 only for feed, dried. CFR 178.3730. (iii) A tolerance of 10 parts per mil- (iii) A tolerance of 10 parts per million is established for residues of lion is established for residues of piperonyl butoxide when present as the piperonyl butoxide in or on: result of migration: (A) Grain, cereal, milled fractions (A) In or on feed, dried from its use when present therein as a result of its on the outer ply of multiwall paper use in cereal grain mills and in storage bags of 50 pounds or more capacity. areas for milled cereal grain products. (B) In or on feed, dried that contain (B) Food, dried when present as a re- 4 percent fat, or less, from its use on sult of migration from its use on the cotton bags of 50 pounds or more capac- outer ply of multiwall paper bags of 50 ity constructed with waxed paper lin- pounds or more capacity. ers. (C) Food treated in accordance with (iv) To assure safe use of the pes- 21 CFR 178.3730. ticide, its label and labeling shall con- (D) Food, dried that contain 4 perform to that registered with the U.S. cent fat, or less, when present as a re- Environmental Protection Agency. sult of migration from its use on the (v) Where tolerances are established cloth of cotton bags of 50 pounds or on both the raw agricultural commod- more capacity constructed with waxed ities and food, processed made there- paper liners. from, the total residues of piperonyl (E) Food treated in accordance with butoxide in or on the processed food paragraph (a)(2)(i)(D) and (E) of this shall not be greater than that per- section. mitted by the larger of the two toler- (iv) To assure safe use of the pes- ances. ticide, its label and labeling shall con- (b) Section 18 emergency exemptions. form to that registered with the U.S. [Reserved] Environmental Protection Agency, and (c) Tolerances with regional registra- it shall be used in accordance with tions. [Reserved] such label and labeling. (d) Indirect or inadvertent residues. (v) Where tolerances are established [Reserved] on both raw agricultural commodities [71 FR 74813, Dec. 13, 2006] and processed food made therefrom, the total residues of piperonyl butoxide in § 180.128 Pyrethrins; tolerances for or on the processed food shall not be residues. greater than that permitted by the (a) General. (1) Tolerances for resi- larger of the two tolerances. dues of the insecticide pyrethrins ((1S)-

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2-methyl-4-oxo-3-(2Z)-2,4- Commodity Parts per pentadienylcyclopenten-1-yl (1R,3R)- million 2,2-dimethyl-3-(2-methyl-1-pro- Hog, meat ...... 0 .05 penyl)cyclopropanecarboxylate (pyre- Hog, meat byproducts ...... 0 .05 thrin 1), (1S)-2-methyl-4-oxo-3-(2Z)-2,4- Horse, fat ...... 1 .0 pentadienyl-2-cyclopenten-1-yl (1R,3R)- Horse, meat ...... 0 .05 3-[(1E)-3-methoxy-2-methyl-3-oxo-1-pro- Horse, meat byproducts ...... 0 .05 penyl]-2,2-dimethylcyclopropane- Loganberry, postharvest ...... 1 .0 Mango, postharvest ...... 1 .0 carboxylate (pyrethrin 2), (1S)-3-(2Z)-2- Milk, fat (reflecting negligible residues in milk) ... 0 .05 butenyl-2-methyl-4-oxo-2-cyclopenten- Muskmelon, postharvest ...... 1.0 1-yl (1R,3R)-2,2-dimethyl-3-(2-methyl-1- Oat, grain, postharvest ...... 1 .0 propenyl)cyclopropanecarboxylate Orange, postharvest ...... 1.0 (cinerin 1), (1S)-3-(2Z)-2-butenyl-2- Pea, dry, seed, postharvest ...... 1 .0 methyl-4-oxo-2-cyclopenten-1-yl Peach, postharvest ...... 1.0 Peanut, postharvest ...... 1 .0 (1R,3R)-3-[(1E)-3-methoxy-2-methyl-3- Pear, postharvest ...... 1.0 oxo-1-propenyl]-2,2- Pineapple, postharvest ...... 1 .0 dimethylcyclopropanecarboxylate Plum, prune, fresh, postharvest ...... 1 .0 (cinerin 2), (1S)-2-methyl-4-oxo-3-(2Z)-2- Potato, postharvest ...... 0 .05 pentenyl-2-cyclopenten-1-yl (1R, 3R)- Raspberry, postharvest ...... 1.0 Rice, grain, postharvest ...... 3 .0 2,2-dimethyl-3-(2-methyl-1-pro- Rye, grain, postharvest ...... 3 .0 penyl)cyclopropanecarboxylate Sheep, fat ...... 1 .0 (jasmolin 1), and (1S)-2-methyl-4-oxo-3- Sheep, meat ...... 0.05 (2Z)-pentenyl-2-cyclopenten-1-yl Sheep, meat byproducts ...... 0 .05 (1R,3R)-3-[(1E)-3-methoxy-2-methyl-3- Sorghum, grain, grain, postharvest ...... 1.0 oxo-1-propenyl]-2,2- Sweet potato, postharvest ...... 0 .05 Tomato, postharvest ...... 1 .0 dimethylcyclopropanecarboxylate Walnut, postharvest ...... 1.0 (jasmolin 2)), the insecticidally active Wheat, grain, postharvest ...... 3 .0 principles of Chrysanthemum cinerariaefolium, which are measured (2) A tolerance of 1.0 ppm is estab- as cumulative residues of pyrethrin 1, lished for residues of the insecticide cinerin 1, and jasmolin 1 are not to ex- pyrethrins in or on milled fractions de- ceed the following: rived from grain, cereal when present as a result of its use in cereal grain Parts per Commodity million mills and in storage areas for milled cereal grain products. Almond, postharvest ...... 1 .0 Apple, postharvest ...... 1 .0 (3) A tolerance of 1.0 ppm is estab- Barley, grain, postharvest ...... 3 .0 lished for residues of the insecticide Bean, succulent, postharvest ...... 1.0 pyrethrins in or on all food items in Birdseed, mixtures, postharvest ...... 3 .0 Blackberry, postharvest ...... 1 .0 food handling establishments where Blueberry, postharvest ...... 1 .0 food and food products are held, proc- Boysenberry, postharvest ...... 1 .0 essed, prepared and/or served. Food Buckwheat, grain, postharvest ...... 3 .0 must be removed or covered prior to Cacao bean, roasted bean, postharvest ...... 1.0 Cattle, fat ...... 1.0 use. Cattle, meat ...... 0 .05 (4) Where tolerances are established Cattle, meat byproducts ...... 0.05 on both the raw agricultural commod- Cherry, sweet, postharvest ...... 1 .0 Cherry, tart, postharvest ...... 1 .0 ities and processed foods made there- Coconut, copra, postharvest ...... 1 .0 from, the total residues of pyrethrins Corn, field, grain, postharvest ...... 3 .0 in or on the processed food shall not be Corn, pop, grain, postharvest ...... 3 .0 Cotton, undelinted seed, postharvest ...... 1.0 greater than that permitted by the Crabapple, postharvest ...... 1 .0 larger of the two tolerances. Currant, postharvest ...... 1 .0 (b) Section 18 emergency exemptions. Dewberry, postharvest ...... 1 .0 [Reserved] Fig, postharvest ...... 1 .0 Flax, seed, postharvest ...... 1 .0 (c) Tolerances with regional registra- Goat, fat ...... 1 .0 tions. [Reserved] Goat, meat ...... 0.05 Goat, meat byproducts ...... 0 .05 (d) Indirect or inadvertent residues. Gooseberry, postharvest ...... 1 .0 [Reserved] Grape, postharvest ...... 1 .0 Guava, postharvest ...... 1 .0 [71 FR 74814, Dec. 13, 2006, as amended at 73 Hog, fat ...... 1 .0 FR 5108, Jan. 29, 2008]

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§ 180.129 o-Phenylphenol and its so- graph is to be determined by measuring dium salt; tolerances for residues. only thiram.

(a) General. Tolerances are estab- Parts lished for combined residues of the fun- Commodity per million gicide o-phenylphenol and sodium o- Avocado 1 ...... 15 phenylphenate, each expressed as o- phenylphenol, from postharvest appli- 1 No U.S. registrations as of September 23, 2009. cation of either in or on the following (2) Tolerances are established for res- food commodities: idues of the fungicide thiram, tetramethyl thiuram disulfide, includ- Parts per Commodity million ing its metabolites and degradates, in or on the commodities in the table in Apple ...... 25 this paragraph. Compliance with the Cantaloupe (NMT 10 ppm in edible portion) ...... 125 Carrot, roots ...... 20 tolerance levels specified in this para- Cherry ...... 5 graph is to be determined by measuring Citrus fruits ...... 10 only those thiram residues convertible Cucumber ...... 10 Lemon ...... 10 to and expressed in terms of the Nectarine ...... 5 degradate carbon disulfide, in or on the Orange ...... 10 commodity. Pepper, bell ...... 10 Peach ...... 20 Parts Pear ...... 25 .0 Commodity per million Pineapple ...... 10 Plum, prune, fresh ...... 20 Apple ...... 5 Sweet potato, roots ...... 15 Banana 1 ...... 2.0 Tomato ...... 10 Peach ...... 7 .0 Strawberry ...... 13 (b) Section 18 emergency exemptions. 1 There are no U.S. registrations as of September 23, 2009. [Reserved] (c) Tolerances with regional registra- (b) Section 18 emergency exemptions. tions. [Reserved] [Reserved] (d) Indirect or inadvertent residues. (c) Tolerances with regional registra- [Reserved] tions. [Reserved] (d) Indirect or inadvertent residues. [73 FR 54960, Sept. 24, 2008] [Reserved] § 180.130 Hydrogen Cyanide; toler- [67 FR 49615, July 31, 2002, as amended at 74 ances for residues. FR 48391, Sept. 23, 2009; 79 FR 8301, Feb. 12, (a) General. A tolerance for residues 2014; 79 FR 18822, Apr. 4, 2014; 80 FR 16306, Mar. 27, 2015; 80 FR 35252, June 19, 2015; 80 FR of the insecticide hydrogen cyanide 72597, Nov. 20, 2015] from postharvest fumigation as a result of application of sodium cyanide is § 180.142 2,4-D; tolerances for residues. established as follows: 50 parts per mil- (a) General. Tolerances are estab- lion in or on Fruit, citrus. lished for residues of the herbicide, (b) Section 18 emergency exemptions. plant regulator, and fungicide 2,4-D, in- [Reserved] cluding its metabolites and degradates, (c) Tolerances with regional registra- in or on the commodities in the table tions. [Reserved] below. Compliance with the tolerance (d) Indirect or inadvertent residues. levels is to be determined by meas- [Reserved] uring residues of 2,4-D (2,4- [64 FR 39077, July 21, 1999] dichlorophenoxyacetic acid), both free and conjugated, determined as the § 180.132 Thiram; tolerances for resi- acid, in or on the following commod- dues. ities: (a) General. (1) A tolerances for residues of the fungicide thiram Commodity Parts per million (tetramethyl thiuram disulfide), including its metabolites and degradates, Almond hulls ...... 0 .1 in or on the commodities in the table Asparagus ...... 5.0 Barley, bran ...... 4 .0 in this paragraph. Compliance with the Barley, grain ...... 2 .0 tolerance level specified in this para- Barley, straw ...... 50

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Parts per Parts per Commodity million Commodity million

Berry, group 13 ...... 0 .2 Wheat, grain ...... 2 .0 Cattle, fat ...... 0.3 Wheat, straw ...... 50 Cattle, kidney ...... 4 .0 Cattle, meat ...... 0 .3 Cattle, meat byproducts, except kidney ...... 0.3 (b) Section 18 emergency exemptions. Corn, field, forage ...... 6 .0 [Reserved] Corn, field, grain ...... 0 .05 (c) Tolerances with regional registra- Corn, field, stover ...... 50 Corn, pop, grain ...... 0.05 tions. Tolerances with regional reg- Corn, pop, stover ...... 50 istration, as defined in § 180.1(l), are es- Corn, sweet, forage ...... 6 .0 Corn, sweet, kernel plus cob with husks re- tablished for residues of the herbicide, moved ...... 0 .05 plant regulator, and fungicide 2,4-D, in- Corn, sweet, stover ...... 50 cluding its metabolites and degradates, Cotton, gin byproducts ...... 1 .5 Cotton, undelinted seed ...... 0 .08 in or on the commodities in the table Cranberry ...... 0 .5 below. Compliance with the tolerance Fish ...... 0 .1 levels is to be determined by meas- Fruit, citrus, group 10 ...... 3 .0 Fruit, pome, group 11 ...... 0.05 uring residues of 2,4-D (2,4- Fruit, stone, group 12 ...... 0 .05 dichlorophenoxyacetic acid), both free Goat, fat ...... 0 .3 and conjugated, determined as the Goat, kidney ...... 4 .0 Goat, meat ...... 0.3 acid, in or on the follow commodities: Goat, meat byproducts, except kidney ...... 0 .3 Grain, aspirated fractions ...... 40 Commodity Parts per Grape ...... 0 .05 million Grass, forage ...... 360 Grass, hay ...... 300 Rice, wild, grain ...... 0.05 Hop, dried cones ...... 0 .2 Horse, fat ...... 0 .3 (d) Indirect or inadvertent residues. Horse, kidney ...... 4 .0 Horse, meat ...... 0 .3 Tolerances are established for indirect Horse, meat byproducts, except kidney ...... 0 .3 or inadvertent residues of the herbi- Millet, forage ...... 25 cide, plant regulator, and fungicide 2,4- Millet, grain ...... 2 .0 Millet, straw ...... 50 D, including its metabolites and Milk ...... 0.05 degradates, in or on the commodities Nut, tree, group 14 ...... 0 .2 in the table below. Compliance with Oat, forage ...... 25 Oat, grain ...... 2 .0 the tolerances levels is to be deter- Oat, straw ...... 50 mined by measuring residues of 2,4-D Pistachio ...... 0.05 (2,4-dichlorophenoxyacetic acid), both Potato ...... 0 .4 Rice, grain ...... 0 .5 free and conjugated, determined as the Rice, hulls ...... 2 .0 acid, in or on the following commod- Rye, bran ...... 4 .0 ities: Rye, forage ...... 25 Rye, grain ...... 2.0 Rye, straw ...... 50 Parts per Commodity million Sheep, fat ...... 0 .3 Sheep, kidney ...... 4.0 Animal feed, nongrass, group 18 ...... 0 .2 Sheep, meat ...... 0.3 Sheep, meat byproducts, except kidney ...... 0 .3 Avocado ...... 0 .05 Shellfish ...... 1 .0 Dill, seed ...... 0 .05 Sorghum, grain, forage ...... 0.2 Okra ...... 0.05 Sorghum, grain, grain ...... 0 .2 Vegetable, brassica leafy, group 5 ...... 0 .4 Sorghum, grain, stover ...... 0 .2 Vegetable, bulb, group 3 ...... 0 .05 Soybean, forage ...... 0 .02 Vegetable, cucurbit, group 9 ...... 0.05 Soybean, hay ...... 2 .0 Vegetable, foliage of legume, group 7 ...... 0 .2 Soybean, seed ...... 0 .02 Vegetable, fruiting, group 8 ...... 0.05 Strawberry ...... 0 .05 Vegetable, leafy, except brassica, group 4 ...... 0 .4 Sugarcane, cane ...... 0.05 Sugarcane, molasses ...... 0 .2 Vegetable, legume, group 6 ...... 0 .05 Teff, bran ...... 4.0 Teff, forage ...... 25.0 Teff, grain ...... 2 .0 [72 FR 52017, Sept. 12, 2007, as amended at 73 Teff, straw ...... 50 .0 FR 53737, Sept. 17, 2008; 74 FR 48411, Sept. 23, Vegetable, leaves of root and tuber, group 2 ..... 0 .1 2009; 76 FR 55817, Sept. 9, 2011; 80 FR 72597, Vegetable, root and tuber, except potato, group Nov. 20, 2015; 82 FR 9529, Feb. 7, 2017] 1 ...... 0 .1 Wheat, bran ...... 4.0 Wheat, forage ...... 25

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§ 180.145 Fluorine compounds; toler- Commodity Parts per ances for residues. million (a) General. (1) Tolerances are estab- Fruit, dried, except grape, raisin, postharvest ..... 3 .0 lished for combined residues of the in- Ginger, postharvest ...... 70 Grain, aspirated fractions, postharvest ...... 55 .0 secticidal fluorine compounds cryolite Grape, raisin, postharvest ...... 7 .0 and synthetic cryolite (sodium alu- Hog, meat ...... 20 minum fluoride) in or on the following Herbs and spices group 19, postharvest ...... 70 Milk, powdered ...... 5 .0 agricultural commodities: Millet, grain, postharvest ...... 40.0 Nut, pine, postharvest ...... 20 Commodity Parts per Nut, tree, Group 14, postharvest ...... 10 .0 million Oat, flour, postharvest ...... 75 .0 Oat, grain, postharvest ...... 25 .0 Apricot ...... 7 Oat, groats/rolled oats ...... 75 .0 Blackberry ...... 7 Peanut, postharvest ...... 15 Blueberry ...... 7 Pistachio, postharvest ...... 10 .0 Boysenberry ...... 7 Rice, bran, postharvest ...... 31 .0 Broccoli ...... 7 Rice, flour, postharvest ...... 45 Brussels sprouts ...... 7 Rice, grain, postharvest ...... 12.0 Cabbage ...... 7 Rice, hulls, postharvest ...... 35.0 Cauliflower ...... 7 Rice, polished rice, postharvest ...... 25.0 Collards ...... 7 Rice, wild, grain, postharvest ...... 25 .0 Cranberry ...... 7 Sorghum, grain, postharvest ...... 40.0 Cucumber ...... 7 Triticale, grain, postharvest ...... 40.0 Dewberry ...... 7 Vegetable, legume, group 6, postharvest ...... 70 Eggplant ...... 7 Wheat, bran, postharvest ...... 40 .0 Fruit, citrus ...... 7 Wheat, flour, postharvest ...... 125 .0 Grape ...... 7 Wheat, germ, postharvest ...... 130 .0 Kale ...... 7 Wheat, grain, postharvest ...... 40.0 Kohlrabi ...... 7 Wheat, milled byproducts, postharvest ...... 130.0 Lettuce, head ...... 7 Wheat, shorts, postharvest ...... 40.0 Lettuce, leaf ...... 7 Loganberry ...... 7 (b) Section 18 emergency exemptions. Melon ...... 7 Nectarine ...... 7 [Reserved] Peach ...... 7 (c) Tolerances with regional registra- Pepper ...... 7 tions. Tolerances with regional reg- Plum, prune, fresh ...... 7 istration, as defined by § 180.1(l), are es- Pumpkin ...... 7 Raspberry ...... 7 tablished for the combined residues of Squash, summer ...... 7 the insecticidal fluorine compounds, Squash, winter ...... 7 cryolite and synthetic cryolite (sodium Strawberry ...... 7 Tomato ...... 7 aluminum fluoride), in or on the fol- Youngberry ...... 7 lowing raw agricultural commodities:

Parts per (2) Tolerances are established for res- Commodity million idues of fluoride in or on the following commodities from the postharvest fu- Kiwifruit ...... 15 migation with sulfuryl fluoride for the control of insects: (d) Indirect or inadvertent residues. [Reserved] Parts per Commodity million [71 FR 74815, Dec. 13, 2006, as amended at 76 FR 34885, June 15, 2011] All processed food commodities not otherwise listed ...... 70 § 180.151 Ethylene oxide; tolerances Barley, bran, postharvest ...... 45 .0 for residues. Barley, flour, postharvest ...... 45.0 Barley, grain, postharvest ...... 15 .0 (a) General. (1) Tolerances are estab- Barley, pearled barley, postharvest ...... 45.0 lished for residues of the antimicrobial Cattle, meat, dried ...... 40 Cheese ...... 5 .0 agent and insecticide ethylene oxide, Cacao bean, roasted bean, postharvest ...... 20 when used as a postharvest fumigant in Coconut, postharvest ...... 40 or on the following food commodities: Coffee, bean, green, postharvest ...... 15 Corn, field, flour, postharvest ...... 35 .0 Parts per Corn, field, grain, postharvest ...... 10.0 Commodity million Corn, field, grits, postharvest ...... 10.0 Corn, field, meal, postharvest ...... 30 .0 Herb and spice, group 19, dried, except basil .... 7 Corn, pop, grain, postharvest ...... 10 .0 Licorice, roots ...... 7 Cotton, undelinted seed, postharvest ...... 70 Peppermint, tops, dried ...... 7 Egg, dried ...... 900 Sesame, seed ...... 7

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Parts per Parts per Commodity million Commodity million

Spearmint, tops, dried ...... 7 Mushroom ...... 0.75 2 Vegetable, dried ...... 7 Nectarine ...... 0.20 Walnut ...... 50 Onion, bulb ...... 0.75 Onion, green ...... 0.75 (2) Tolerances are established for res- Pea, succulent ...... 0.50 Peach ...... 0.20 idues of the ethylene oxide reaction Pear ...... 0.50 product, 2-chloroethanol, commonly Pineapple ...... 0.50 referred to as ethylene chlorohydrin, Plum, prune, fresh ...... 0.20 Radish ...... 0.50 when ethylene oxide is used as a Rutabaga ...... 0.75 postharvest fumigant in or on food Spinach ...... 0.70 commodities as follows: Strawberry ...... 0.50 Tomato ...... 0.75 Vegetable, brassica, leafy, group 5 ...... 0.70 Parts per Commodity million Watercress ...... 0.05 1There are no domestic registrations for kiwifruit as of Herb and spice, group 19, dried, except basil .... 940 March 6, 2002. Licorice, roots ...... 940 2The expiration/revocation date for this tolerance is 9/10/ Peppermint, tops, dried ...... 940 2010. Sesame, seed ...... 940 Spearmint, tops, dried ...... 940 (b) Section 18 emergency exemptions. Vegetable, dried ...... 940 [Reserved] (c) Tolerances with regional registra- (b) Section 18 emergency exemptions. tions. Tolerances with regional reg- [Reserved] istration, as defined in § 180.1(l), are es- (c) Tolerances with regional registra- tablished for residues of the insecticide tions. [Reserved] diazinon, O, O-diethyl O-[6-methyl-2-(1- (d) Indirect or inadvertent residues. methylethyl)-4-pyrimidinyl]- [Reserved] phosphorothioate (CAS No. 333–41–5), in [65 FR 33695, May 24, 2000, as amended at 74 or on the following food commodities: FR 46696, Sept. 11, 2009] Parts per Commodity million § 180.153 Diazinon; tolerances for residues. Almond ...... 0.50 Banana ...... 0.20 (a) General. Tolerances are estab- Celery ...... 0 .70 lished for residues of the insecticide Cucumber ...... 0 .75 diazinon, O,O-diethyl O-[6-methyl-2-(1- Parsley, leaves ...... 0.75 Parsnip ...... 0.50 methylethyl)-4- Pepper ...... 0 .5 pyrimidinyl]phosphorothioate (CAS Potato ...... 0 .10 No. 333–41–5), in or on the following Squash, summer ...... 0 .50 Squash, winter ...... 0 .75 food commodities: Sweet potato, roots ...... 0 .10 Swiss chard ...... 0.70 Parts per Turnip, roots ...... 0 .50 Commodity million Turnip, tops ...... 0.75 Almond, hulls ...... 3.0 Apple ...... 0.50 (d) Indirect or inadvertent residues. Apricot ...... 0.20 [Reserved] Bean, lima ...... 0.50 Bean, snap, succulent ...... 0.50 [47 FR 42738, Sept. 29, 1982] Beet, garden, roots ...... 0.75 Beet, garden, tops ...... 0.70 EDITORIAL NOTE: For FEDERAL REGISTER ci- Blueberry ...... 0.50 tations affecting § 180.153, see the List of CFR Caneberry subgroup 13-07A ...... 0.75 Sections Affected, which appears in the Carrot, roots ...... 0.75 Finding Aids section of the printed volume Cattle, fat ...... 0.50 Cherry, sweet ...... 0.20 and at www.govinfo.gov. Cherry, tart ...... 0.20 Cranberry ...... 0.50 § 180.155 1-Naphthaleneacetic acid; tol- Endive ...... 0.70 erances for residues. Fig ...... 0.50 Ginseng ...... 0.75 (a) General. Tolerances are estab- Grape ...... 0.75 2 lished for the residues of 1- Hazelnut ...... 0.50 naphthaleneacetic acid, including its Kiwifruit 1 ...... 0.75 Lettuce ...... 0.70 metabolites and degradates in or on Melon ...... 0.75 the commodities in the following table.

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Compliance with the tolerance levels Parts per Expiration/ specified is to be determined by meas- Commodity revocation million date uring only 1-naphthaleneacetic acid and its conjugates, calculated as the Fruit, stone, group 12 ...... 5.0 10/31/16 Stoichiometric equivalent of 1- Grape ...... 5.0 10/31/16 Grape, raisin ...... 20.0 10/31/16 naphthaleneacetic acid, in or on the Hazelnut ...... 0.1 10/31/16 commodity. Hop, dried cones ...... 65.0 10/31/16 Nut, hickory ...... 0.1 10/31/16 Parts per Nut, macadamia ...... 0.1 10/31/16 Commodity million Pecan ...... 0.1 10/31/16 Peppermint, oil ...... 30.0 10/31/16 Avocado ...... 0 .05 Peppermint, tops ...... 25.0 10/31/16 Cherry, sweet ...... 0 .1 Spearmint, oil ...... 30.0 10/31/16 Fruit, pome, group 11–10 ...... 0 .15 Spearmint, tops ...... 25.0 10/31/16 Mango ...... 0.05 Strawberry ...... 10.0 10/31/16 Olive ...... 0 .7 Tea, dried ...... 50.0 None Orange ...... 0 .1 Tea, plucked leaves ...... 30.0 None Pineapple1 ...... 0 .05 Vegetable, cucurbit, group 9 ...... 2.0 10/31/16 Pomegranate ...... 0 .05 Vegetable, fruiting, group 8 ...... 2.0 10/31/16 Potato ...... 0 .01 Walnut ...... 0.1 10/31/16 Rambutan ...... 2 .0 Sapote, mamey ...... 0 .05 (2) Tolerances are established for res- Tangerine ...... 0 .1 idues of the insecticide dicofol, includ- 1 There are no U.S. registrations since 1988. ing its metabolites and degradates, in (b) Section 18 emergency exemptions. or on the commodities in the table in [Reserved] this paragraph. Compliance with the (c) Tolerances with regional registra- tolerance levels specified in this para- tions. [Reserved] graph is to be determined by measuring (d) Indirect or inadvertent residues. only the sum of p,p-dicofol, 4-chloro-a- [Reserved] (4-chlorophenyl)-a- (trichloromethyl)benzenemethanol, its [78 FR 30218, May 22, 2013, as amended at 80 FR 77260, Dec. 14, 2015] isomer o,p-dicofol, 2-chloro-a-(4- chlorophenyl)-a- § 180.163 Dicofol; tolerances for resi- (trichloromethyl)benzenemethanol, dues. and its metabolites 4-chloro-a-(4- (a) General. (1) Tolerances are estab- chlorophenyl)-a- lished for residues of the insecticide (dichloromethyl)benzenemethanol and dicofol, including its metabolites and 2-chloro-a-(4-chlorophenyl)-a- degradates, in or on the commodities (dichloromethyl)benzenemethanol, cal- in the table in this paragraph. Compli- culated as the stoichiometric equiva- ance with the tolerance levels specified lent of p,p-dicofol, 4-chloro-a-(4- in this paragraph is to be determined chlorophenyl)-a- by measuring only dicofol as the sum (trichloromethyl)benzenemethanol, in of its p,p-dicofol and o,p-dicofol iso- or on the commodity. mers: 4-chloro-a-(4-chlorophenyl)-a- Parts per Expiration/ (trichloromethyl)benzenemethanol and Commodity million Revocation 2-chloro-a-(4-chlorophenyl)-a- Date (trichloromethyl)benzenemethanol, in Cattle, fat ...... 50.0 10/31/16 or on the commodity. Cattle, liver ...... 5.0 10/31/16 Cattle, meat ...... 3.0 10/31/16 Expiration/ Cattle, meat byproducts, except Parts per liver ...... 3.0 10/31/16 Commodity million revocation date Egg ...... 0.05 10/31/16 Goat, fat ...... 50.0 10/31/16 Apple, wet pomace ...... 38.0 10/31/16 Goat, liver ...... 5.0 10/31/16 Bean, dry, seed ...... 0.5 10/31/16 Goat, meat ...... 3.0 10/31/16 Bean, succulent ...... 3.0 10/31/16 Goat, meat byproducts, except liver 3.0 10/31/16 Butternut ...... 0.1 10/31/16 Hog, fat ...... 50.0 10/31/16 Caneberry subgroup 13A ...... 5.0 10/31/16 Hog, liver ...... 5.0 10/31/16 Chestnut ...... 0.1 10/31/16 Hog, meat ...... 3.0 10/31/16 Citrus, dried pulp ...... 12.0 10/31/16 Hog, meat byproducts, except liver 3.0 10/31/16 Citrus oil ...... 200.0 10/31/16 Horse, fat ...... 50.0 10/31/16 Cotton, refined oil ...... 0.5 10/31/16 Horse, liver ...... 5.0 10/31/16 Cotton, undelinted seed ...... 0.1 10/31/16 Horse, meat ...... 3.0 10/31/16 Fruit, citrus, group 10 ...... 6.0 10/31/16 Horse, meat byproducts, except Fruit, pome, group 11 ...... 10.0 10/31/16 liver ...... 3.0 10/31/16

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Expiration/ Expiration/ Commodity Parts per Revocation Commodity Parts per revocation million Date million date

Milk, fat (reflecting 0.75 ppm in Grape ...... 10 None whole milk) ...... 22.0 10/31/16 Grape, raisin ...... 12 None Poultry, fat ...... 0.1 10/31/16 Grass, forage ...... 100 None Poultry, meat ...... 0.1 10/31/16 Grass, hay ...... 15 None Poultry, meat byproducts ...... 0.1 10/31/16 Leaf petiole subgroup 4B ...... 3.0 None Sheep, fat ...... 50.0 10/31/16 Lettuce ...... 10 None Sheep, liver ...... 5.0 10/31/16 Millet, proso, grain ...... 1.0 None Sheep, meat ...... 3.0 10/31/16 Sheep, meat byproducts, except Millet, proso, straw ...... 20 None liver ...... 3.0 10/31/16 Nut, tree group 14, except walnut ... 0.1 None Okra ...... 4.0 None Olive ...... 10 None (b) Section 18 emergency exemptions. Oyster ...... 0.25 None [Reserved] Parsley, leaves ...... 22 None (c) Tolerances with regional registra- Pea and bean, dried shelled, except tions. [Reserved] soybean, subgroup 6C ...... 1.0 None (d) Indirect or inadvertent residues. Peanut ...... 0.05 None Peanut, hay ...... 20 None [Reserved] Pineapple ...... 2.0 None [63 FR 34826, June 26, 1998, as amended at 72 Pistachio ...... 0.1 None FR 35665, June 29, 2007; 72 FR 41928, Aug. 1, Rice, grain ...... 15 None 2007; 77 FR 59124, Sept. 26, 2012] Rice, hulls ...... 30 None Sorghum grain, forage ...... 30 None Sorghum grain, grain ...... 10 None § 180.169 Carbaryl; tolerances for resi- Sorghum grain, stover ...... 30 None dues. Soybean, forage ...... 15 None (a) General. (1) Tolerances are estab- Soybean, hay ...... 15 None lished for residues of the insecticide Soybean, seed ...... 0.5 None Spinach ...... 22 None carbaryl, 1-naphthyl N- Strawberry ...... 4.0 None methylcarbamate per se, in or on the Sunflower, seed ...... 0.5 None following food commodities: Sweet potato, roots ...... 0.2 None Trefoil, forage ...... 15 None Trefoil, hay ...... 25 None Parts per Expiration/ Commodity million revocation Vegetable, brassica, leafy, group 5, date except cabbage ...... 10 None Vegetable, cucurbit, group 9 ...... 3.0 None Alfalfa, forage ...... 50 None Alfalfa, hay ...... 75 None Vegetable, foliage of legume, sub- Almond, hulls ...... 50 None group 7A, except soybean ...... 60 None Apple, wet pomace ...... 15 None Vegetable, fruiting, group 8 ...... 5.0 None Asparagus ...... 15 None Vegetable, leaves of root and tuber, Banana ...... 5.0 None group 2, except sugar beet tops 75 None Beet, sugar, roots ...... 0.5 None Vegetable, legume, edible podded, Beet, sugar, tops ...... 25 None subgroup 6A ...... 10 None Bushberry subgroup 13-07B ...... 3.0 None Vegetable, root and tuber, group 1, Cabbage ...... 21 None except sugar beet and sweet po- Cactus, fruit ...... 5.0 None tato ...... 2.0 None Cactus, pads ...... 12 None Walnut ...... 1.0 None Caneberry subgroup 13-07A ...... 12.0 None Wheat, forage ...... 30 None Citrus, oil ...... 20 None Wheat, grain ...... 1.0 None Clover, forage ...... 50 None Wheat, hay ...... 30 None Clover, hay ...... 70 None Wheat, straw ...... 20 None Corn, field, forage ...... 30 None Corn, field, grain ...... 0.02 None Corn, field, stover ...... 20 None (2) Tolerances are established for res- Corn, pop, grain ...... 0.02 None idues of the insecticide carbaryl, 1- Corn, pop, stover ...... 20 None naphthyl N-methylcarbamate, includ- Corn, sweet, forage ...... 185 None ing its metabolites: 1-naphthol Corn, sweet, kernel plus cob with husks removed ...... 0.1 None (naphthyl-sulfate); 5,6- Corn, sweet, stover ...... 215 None dihydrodihydroxycarbaryl; and 5,6- Cotton, undelinted seed ...... 5.0 10/31/09 dihydrodihydroxy naphthol, calculated Cranberry ...... 3.0 None Dandelion, leaves ...... 22 None as 1-naphthyl N-methylcarbamate and Endive ...... 10 None the free and conjugated residues of Flax, seed ...... 0.5 None carbaryl: 5,6-dihydro-5,6-dihydroxy Fruit, citrus, group 10 ...... 10 None carbaryl and 5-methoxy-6-hydroxy Fruit, pome, group 11 ...... 12 None Fruit, stone, group 12 ...... 10 None carbaryl, in or on the following food Grain, aspirated fractions ...... 70 None commodities:

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Expiration/ Parts per Commodity Parts per revocation Commodity million million date Nuts, tree, crop group 14 ...... 0.3 Cattle, fat ...... 0.5 None Peanut ...... 0.013 Cattle, meat ...... 1.0 None Pear ...... 5.0 Cattle, meat byproducts ...... 3.0 None Strawberry ...... 5.0 Egg ...... 0.5 10/31/09 Goat, fat ...... 0.5 None Goat, meat ...... 1.0 None (b) Section 18 emergency exemptions. Goat, meat byproducts ...... 3.0 None [Reserved] Hog, fat ...... 0.5 None (c) Tolerances with regional registra- Hog, meat ...... 1.0 None tions. [Reserved] Hog, meat byproducts ...... 3.0 None Horse, fat ...... 0.5 None (d) Indirect or inadvertent residues. Horse, meat ...... 1.0 None [Reserved] Horse, meat byproducts ...... 3.0 None Milk ...... 1.0 None [72 FR 52017, Sept. 12, 2007, as amended at 73 Poultry, fat ...... 5.0 10/31/09 FR 45634, Aug. 6, 2008; 77 FR 72237, Dec. 5, Poultry, meat ...... 5.0 10/31/09 2012] Sheep, fat ...... 0.5 None Sheep, meat ...... 1.0 None § 180.175 Maleic hydrazide; tolerances Sheep, meat byproducts ...... 3.0 None for residues. (b) Section 18 emergency exemptions. (a) General. (1) Tolerances for resi- [Reserved] dues of the herbicide and plant regu- (c) Tolerances with regional registra- lator maleic hydrazide (1,2-dihydro-3,6- tions. Tolerances with regional reg- pyridazinedione) are established in or istrations, as defined in § 180.1(l), are on the following raw agricultural com- established for residues of the insecti- modities: cide carbaryl, 1-naphthyl N- Parts per methylcarbamate per se, in or on the Commodity million following food commodities: Onion, bulb ...... 15.0 Parts per Potato ...... 50.0 Commodity million (2) A food additive known as maleic Dillweed, fresh leaves ...... 0 .2 hydrazide (1,2-dihydro-3,6- (d) Indirect or inadvertent residues. pyridazinedione) may be present in po- [Reserved] tato, chips when used in accordance with the following conditions: [65 FR 33695, May 24, 2000, as amended at 66 (i) The food additive is present as a FR 38955, July 26, 2001; 67 FR 49615, July 31, result of the application of a pesticide 2002; 70 FR 44492, Aug. 3, 2005; 73 FR 52611, formulation containing maleic hydra- Sept. 10, 2008; 74 FR 10490, Mar. 11, 2009; 80 FR 72597, Nov. 20, 2015] zide to the growing potato plant in accordance with directions registered by § 180.172 Dodine; tolerances for resi- the U.S. Environmental Protection dues. Agency. (a) General. Tolerances are estab- (ii) The label of the pesticide formu- lished for residues of the fungicide lation containing the food additive dodine, including its metabolites and conforms to labeling registered by the degradates, in or on the commodities U.S. Environmental Protection Agen- listed in the table below. Compliance cy. with the tolerance levels specified in (iii) The food additive is present in an the table is to be determined by meas- amount not to exceed 160 parts per mil- uring only dodine, N-dodecylguanidine lion by weight of the finished food. acetate; in or on the following com- (b) Section 18 emergency exemptions. modities. [Reserved] (c) Tolerances with regional registra- Commodity Parts per tions. [Reserved] million (d) Indirect or inadvertent residues. Almond, hull ...... 30.0 [Reserved] Apple ...... 5.0 Apple, wet pomace ...... 15.0 [62 FR 64293, Dec. 5, 1997, as amended at 64 Banana ...... 0.50 FR 11792, Mar. 10, 1999; 67 FR 35048, May 17, Fruit, stone, crop group 12 ...... 5.0 2002]

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§ 180.176 Mancozeb; tolerances for res- Commodity Parts idues. per million (a) General. Tolerances are estab- Papaya ...... 9 lished for residues of mancozeb (a co- Peanut ...... 0 .1 ordination product of zinc ion and Peanut, hay ...... 65 Pear ...... 0 .6 maneb (manganese Pepper ...... 12 ethylenebisdithiocarbamate)), includ- Potato ...... 0 .2 ing its metabolites and degradates, in Poultry, kidney ...... 0 .5 or on the commodities in the following Poultry, liver ...... 0 .5 table. Compliance with the tolerance Quince ...... 0 .6 levels specified in this paragraph is to Rice, grain ...... 0 .06 be determined by measuring only those Rye, bran ...... 2 Rye, flour ...... 1 .2 mancozeb residues convertible to and Rye, grain ...... 1 expressed in terms of the degradate Rye, straw ...... 25 carbon disulfide. Sapodilla ...... 15 .0 Sapote, mamey ...... 15 .0 Parts Sapote, white ...... 15 .0 Commodity per million Sheep, kidney ...... 0.5 Almond ...... 0.1 Sheep, liver ...... 0.5 Almond, hulls ...... 4 Sorghum, grain, forage ...... 0.15 Apple ...... 0.6 Sorghum, grain, grain ...... 0 .25 Asparagus ...... 0.1 Sorghum, grain, stover ...... 0 .15 Atemoya ...... 3 .0 Star apple ...... 15 .0 Banana ...... 2 Sugar apple ...... 3 .0 Barley, bran ...... 2 Tangerine 1 ...... 10 Barley, flour ...... 1 .2 Barley, grain ...... 1 Tomato ...... 2.5 Barley, hay ...... 30 Vegetable, cucurbit, group 9 ...... 2.0 Barley, pearled barley ...... 20 Walnut ...... 0 .70 Barley, straw ...... 25 Wheat, bran ...... 2 Beet, sugar, dried pulp ...... 3 .0 Wheat, flour ...... 1 .2 Beet, sugar, roots ...... 1 .2 Wheat, germ ...... 20 Beet, sugar, tops ...... 60 Wheat, grain ...... 1 Broccoli ...... 7 Wheat, hay ...... 30 Cabbage ...... 9 Canistel ...... 15 .0 Wheat, middlings ...... 20 Cattle, kidney ...... 0 .5 Wheat, shorts ...... 2 Cattle, liver ...... 0 .5 Wheat, straw ...... 25 Cherimoya ...... 3 .0 1 Corn, field, forage ...... 40 There are no U.S. registrations for use of mancozeb on tangerine. Corn, field, grain ...... 0 .06 Corn, field, stover ...... 15 (b) Section 18 emergency exemptions. Corn, pop, grain ...... 0.1 Corn, pop, stover ...... 40 [Reserved] Corn, sweet, forage ...... 70 (c) Tolerances with regional registra- Corn, sweet, kernel plus cob with husks removed ...... 0 .1 tions. A tolerance with regional reg- Corn, sweet, stover ...... 40 istrations, as defined in § 180.1(l), is es- Cotton, undelinted seed ...... 0 .5 tablished for residues of the fungicide Crabapple ...... 0 .6 Cranberry ...... 5 mancozeb, (a coordination product of Custard apple ...... 3 .0 zinc ion and maneb (manganese Fennel ...... 2.5 ethylenebisdithiocarbamate)), includ- Flax, seed ...... 0 .15 Ginseng ...... 1 .2 ing its metabolites and degradates, in Goat, kidney ...... 0 .5 or on the commodity in the following Goat, liver ...... 0.5 table in this paragraph. Compliance Grape ...... 1 .5 Hog, kidney ...... 0.5 with the tolerance levels specified in Hog, liver ...... 0 .5 this paragraph is to be determined by Horse, kidney ...... 0 .5 measuring only those mancozeb resi- Horse, liver ...... 0 .5 Lettuce, head ...... 3.5 dues convertible to and expressed in Lettuce, leaf ...... 18 terms of the degradate carbon disul- Mango ...... 15.0 fide. Oat, flour ...... 1 .2 Oat, grain ...... 1 Parts per Oat, groats/rolled oats ...... 20 Commodity million Oat, hay ...... 30 Oat, straw ...... 25 Carrot, roots ...... 1 Onion, bulb ...... 1 .5

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(d) Indirect or inadvertent residues. Commodity Parts per [Reserved] million [65 FR 33708, May 24, 2000, as amended at 65 Goat, meat byproducts except kidney ...... 0 .06 FR 49924, Aug. 16, 2000; 66 FR 64773, Dec. 14, Hog, fat ...... 0 .20 Hog, kidney ...... 0.30 2001; 68 FR 2247, Jan. 16, 2003; 69 FR 29458, Hog, meat ...... 0 .06 May 24, 2004; 71 FR 76199, Dec. 20, 2006; 74 FR Hog, meat byproducts except kidney ...... 0 .06 46372, Sept. 9, 2009; 75 FR 770, Jan. 6, 2010; 75 Horse, fat ...... 0 .20 FR 50913, Aug. 18, 2010; 76 FR 18915, Apr. 6, Horse, kidney ...... 0 .30 2011; 78 FR 44455, July 24, 2013; 79 FR 27501, Horse, meat ...... 0 .06 May 14, 2014; 80 FR 72597, Nov. 20, 2015] Horse, meat byproducts except kidney ...... 0.06 Milk ...... 0.30 Sheep, fat ...... 0 .20 § 180.178 Ethoxyquin; tolerances for Sheep, kidney ...... 0.30 residues. Sheep, meat ...... 0.06 (a) General. A tolerance is established Sheep, meat byproducts except kidney ...... 0 .06 for residues of the plant regulator (b) Section 18 emergency exemptions. ethoxyquin (1,2-dihydro-6-ethoxy-2,2,4- [Reserved] trimethylquinoline) from preharvest or (c) Tolerances with regional registra- postharvest use in or on the following tions. [Reserved] commodity: (d) Indirect or inadvertent residues. Parts per [Reserved] Commodity million [43 FR 52487, Nov. 13, 1978, as amended at 63 Pear ...... 3 FR 57073, Oct. 26, 1998; 72 FR 37653, July 11, 2007] (b) Section 18 emergency exemptions. [Reserved] § 180.182 Endosulfan; tolerances for (c) Tolerances with regional registra- residues. tions. [Reserved] (a)(1) General. Tolerances are estab- (d) Indirect or inadvertent residues. lished for residues of the insecticide [Reserved] endosulfan, including its metabolites and degradates, in or on the commod- [63 FR 57073, Oct. 26, 1998] ities in the table in this paragraph. § 180.181 Chlorpropham; tolerances for Compliance with the tolerance levels residues. specified in this paragraph is to be de- (a) General. (1) Tolerances are estab- termined by measuring only the sum of lished for residues of the plant regu- endosulfan, 6,7,8,9,10,10-hexachloro- lator and herbicide chlorpropham (iso- 1,5,5a,6,9,9a-hexahydro-6,9-methano- propyl m-chlorocarbanilate (CIPC) in 2,4,3-benzodioxathiepin 3-oxide (alpha or on the following food commodities: and beta isomers), and its metabolite endosulfan sulfate, 6,7,8,9,10,10- Commodity Parts per hexachloro-1,5,5a,6,9,9a-hexahydro-6,9- million methano-2,4,3-benzodioxathiepin-3,3-di- Potato ...... 30 oxide, calculated as the stoichiometric Potato, wet peel ...... 40 equivalent of endosulfan, in or on the commodity. (2) Tolerances are established for the combined residues of the plant regu- Expiration/ Commodity Parts per revocation lator and herbicide chlorpropham (iso- million date propyl m-chlorocarbanilate (CIPC) and its metabolite 4-hydroxychlorpropham- Almond ...... 0.3 7/31/12 Almond, hulls ...... 1.0 7/31/12 O-sulfonic acid (4-HSA) in or on the fol- Apricot ...... 2.0 7/31/12 lowing food commodities: Bean ...... 2.0 7/31/12 Broccoli ...... 3.0 7/31/12 Parts per Brussels sprouts ...... 2.0 7/31/12 Commodity million Cabbage ...... 4.0 7/31/12 Cantaloupe ...... 1.0 7/31/12 Cattle, fat ...... 0.20 Carrot, roots ...... 0.2 7/31/12 Cattle, kidney ...... 0 .30 Cattle, fat ...... 13.0 7/31/16 Cattle, meat ...... 0 .06 Cattle, liver ...... 5.0 7/31/16 Cattle, meat byproducts except kidney ...... 0 .06 Cattle, meat ...... 2.0 7/31/16 Goat, fat ...... 0 .20 Cattle, meat byproducts, except Goat, kidney ...... 0 .30 liver ...... 1.0 7/31/16 Goat, meat ...... 0.06 Cauliflower ...... 2.0 7/31/12

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Expiration/ Expiration/ Commodity Parts per revocation Commodity Parts per revocation million date million date

Celery ...... 8.0 7/31/12 Pear ...... 2.0 7/31/13 Cherry, sweet ...... 2.0 7/31/12 Pineapple ...... 1.0 7/31/16 Cherry, tart ...... 2.0 7/31/12 Pineapple, process residue ...... 20.0 7/31/16 Collards ...... 2.0 7/31/12 Plum ...... 2.0 7/31/12 Cotton, gin byproducts ...... 30.0 7/31/12 Plum, prune ...... 2.0 7/31/12 Cotton, undelinted seed ...... 1.0 7/31/12 Sheep, fat ...... 13.0 7/31/16 Cucumber ...... 1.0 7/31/12 Eggplant ...... 1.0 7/31/12 Sheep, liver ...... 5.0 7/31/16 Goat, fat ...... 13.0 7/31/16 Sheep, meat ...... 2.0 7/31/16 Goat, liver ...... 5.0 7/31/16 Sheep, meat byproducts, except Goat, meat ...... 2.0 7/31/16 liver ...... 1.0 7/31/16 Goat, meat byproducts, except liver 1.0 7/31/16 Squash, summer ...... 1.0 7/31/12 Hazelnut ...... 0.2 7/31/12 Strawberry ...... 2.0 7/31/16 Hog, fat ...... 13.0 7/31/16 Sweet potato, roots ...... 0.15 7/31/12 Hog, liver ...... 5.0 7/31/16 Walnut ...... 0.2 7/31/12 Hog, meat ...... 2.0 7/31/16 Watermelon ...... 1.0 7/31/12 Hog, meat byproducts, except liver 1.0 7/31/16 Horse, fat ...... 13.0 7/31/16 Horse, liver ...... 5.0 7/31/16 (2) A tolerance is established for the Horse, meat ...... 2.0 7/31/16 combined residues of the insecticide Horse, meat byproducts, except endosulfan, 6,7,8,9,10,10-hexachloro- liver ...... 1.0 7/31/16 Kale ...... 2.0 7/31/12 1,5,5a,6,9,9a-hexahydro-6,9-methano-2, Lettuce, head ...... 11.0 7/31/12 4,3-benzodioxathiepin-3-oxide (alpha Lettuce, leaf ...... 6.0 7/31/12 and beta isomers), and its metabolite Milk, fat ...... 2.0 7/31/16 Muskmelon ...... 1.0 7/31/12 endosulfan sulfate, 6,7,8,9,10,10- Mustard greens ...... 2.0 7/31/12 hexachloro-1,5,5a,6,9,9a-hexahydro-6,9- Mustard, seed ...... 0.2 7/31/12 methano-2, 4,3-benzodioxathiepin-3,3- Nectarine ...... 2.0 7/31/12 Nut, macadamia ...... 0.2 7/31/12 dioxide in or on the commodity in the Peach ...... 2.0 7/31/12 following table:

Expiration/ Commodity Parts per million revocation date

Tea, dried ...... 24 (reflecting less than 0.1 ppm in beverage tea) resulting from application of the insecticide 7/31/16 to growing tea.

(b) Section 18 emergency exemptions. Parts per Expiration/ [Reserved] Commodity revocation million date (c) Tolerances with regional registrations. (1) Tolerances with regional reg- Apple ...... 1.0 12/31/14 Apple, wet pomace ...... 5.0 12/31/14 istration, as defined in § 180.1(l), are es- Blueberry ...... 0.3 12/31/14 tablished for residues of the insecticide Corn, sweet, forage ...... 12.0 12/31/14 endosulfan, including its metabolites Corn, sweet, kernel plus cob with husks removed ...... 0.2 12/31/14 and degradates, in or on the commod- Corn, sweet, stover ...... 14.0 12/31/14 ities in the table in this paragraph, Pepper ...... 2.0 12/31/14 when endosulfan is used in the state of Potato ...... 0.2 12/31/14 Pumpkin ...... 1.0 12/31/14 Florida. Compliance with the tolerance Squash, winter ...... 1.0 12/31/14 levels specified in this paragraph is to Tomato ...... 1.0 12/31/14 be determined by measuring only the sum of endosulfan, 6,7,8,9,10,10- (2) Tolerances with regional registra- hexachloro-1,5,5a,6,9,9a-hexahydro-6,9- tions. Tolerances with regional reg- methano-2,4,3-benzodioxathiepin 3- istration, as defined in § 180.1(l), are es- oxide (alpha and beta isomers), and its tablished for residues of the insecticide metabolite endosulfan sulfate, endosulfan, including its metabolites 6,7,8,9,10,10-hexachloro-1,5,5a,6,9,9a- and degradates, in or on the commod- hexahydro-6,9-methano-2,4,3- ities in the table in this paragraph, benzodioxathiepin-3,3-dioxide, cal- when endosulfan is used in the United culated as the stoichiometric equiva- States (except Florida). Compliance lent of endosulfan, in or on the com- with the tolerance levels specified in modity. this paragraph is to be determined by

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measuring only the sum of endosulfan, stoichiometric equivalent of 6,7,8,9,10,10-hexachloro-1,5,5a,6,9,9a- disulfoton, in or on the commodity. hexahydro-6,9-methano-2,4,3- Expiration/ benzodioxathiepin 3-oxide (alpha and Commodity Parts per Revocation beta isomers), and its metabolite million Date endosulfan sulfate, 6,7,8,9,10,10- hexachloro-1,5,5a,6,9,9a-hexahydro-6,9- Bean, lima ...... 0.75 12/31/13 Bean, snap, succulent ...... 0.75 12/31/13 methano-2,4,3-benzodioxathiepin-3,3-di- Broccoli ...... 0.75 12/31/13 oxide, calculated as the stoichiometric Brussels sprouts ...... 0.75 12/31/13 equivalent of endosulfan, in or on the Cabbage ...... 0.75 12/31/13 commodity. Cauliflower ...... 0.75 12/31/13 Coffee, green bean ...... 0.2 6/30/14 Parts per Expiration/ Cotton, undelinted seed ...... 0.75 12/31/13 Commodity revocation Lettuce, head ...... 0.75 12/31/14 million date Lettuce, leaf ...... 2 12/31/14 Apple ...... 1.0 7/31/15 Apple, wet pomace ...... 5.0 7/31/15 (b) Section 18 emergency exemptions. Blueberry ...... 0.3 7/31/15 [Reserved] Corn, sweet, forage ...... 12.0 7/31/15 (c) Tolerances with regional registra- Corn, sweet, kernel plus cob with husks removed ...... 0.2 7/31/15 tions. A tolerance with regional reg- Corn, sweet, stover ...... 14.0 7/31/15 istration is established for residues of Pepper ...... 2.0 7/31/15 the insecticide disulfoton, O,O-diethyl Potato ...... 0.2 7/31/15 S-(2-(ethylthio)ethyl) Pumpkin ...... 1.0 7/31/15 phosphorodithioate, including its me- Squash, winter ...... 1.0 7/31/15 Tomato ...... 1.0 7/31/15 tabolites and degradates, in or on the commodity in the following table. (d) Indirect or inadvertent residues. Compliance with the tolerance levels [Reserved] specified in this paragraph is to be determined by measuring only the sum of [65 FR 33696, May 24, 2000, as amended at 71 disulfoton, O,O-diethyl S-(2- FR 54433, Sept. 15, 2006; 76 FR 56653, Sept. 14, (ethylthio)ethyl) phosphorodithioate, 2011; 78 FR 8409, Feb. 6, 2013] and its metabolites demeton-S, O,O- § 180.183 Disulfoton; tolerances for res- diethyl S-(2-(ethylthio)ethyl) idues. phosphorothioate; disulfoton sulfoxide, O,O-diethyl S-(2-(ethylsulfinyl)ethyl) (a) General. Tolerances are estab- phosphorodithioate; disulfoton oxygen lished for residues of the insecticide analog sulfoxide, O,O-diethyl S-(2- disulfoton, O,O-diethyl S-(2- (ethylsulfinyl)ethyl) phosphorothioate, (ethylthio)ethyl) phosphorodithioate, disulfoton sulfone, O,O-diethyl S-(2- including its metabolites and (ethylsulfonyl)ethyl) degradates, in or on the commodities phosphorodithioate; and disulfoton ox- in the following table. Compliance with ygen analog sulfone, O,O-diethyl S-(2- the tolerance levels specified in this (ethylsulfonyl)ethyl) paragraph is to be determined by meas- phosphorothioate; calculated as the uring only the sum of disulfoton, O,O- stoichiometric equivalent of diethyl S-(2-(ethylthio)ethyl) disulfoton, in or on the commodity. phosphorodithioate, and its metabolites demeton-S, O,O-diethyl S-(2- Parts per Expiration/ (ethylthio)ethyl) phosphorothioate; Commodity million Revocation disulfoton sulfoxide, O,O-diethyl S-(2- Date (ethylsulfinyl)ethyl) Asparagus ...... 0.1 12/31/13 phosphorodithioate; disulfoton oxygen analog sulfoxide, O,O-diethyl S-(2- (d) Indirect or inadvertent residues. (ethylsulfinyl)ethyl) phosphorothioate, [Reserved] disulfoton sulfone, O,O-diethyl S-(2- (ethylsulfonyl)ethyl) [63 FR 2165, Jan. 14, 1998, as amended at 63 FR 57073, Oct. 26, 1998; 66 FR 38955, July 26, phosphorodithioate; and disulfoton ox- 2001; 67 FR 41806, June 19, 2002; 67 FR 49615, ygen analog sulfone, O,O-diethyl S-(2- July 31, 2002; 70 FR 44492, Aug. 3, 2005; 73 FR (ethylsulfonyl)ethyl) 54960, Sept. 24, 2008; 74 FR 46697, Sept. 11, phosphorothioate; calculated as the 2009; 75 FR 60240, Sept. 29, 2010]

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§ 180.185 DCPA; tolerances for resi- Commodity Parts per dues. million (a) General. Tolerances for the com- Bean, snap, succulent ...... 2 .0 bined residues of the herbicide di- Celeriac ...... 2.0 Chicory, roots ...... 2 .0 methyl tetrachloroterephthalate Chicory, tops ...... 5 .0 (DCPA) and its metabolites Chive ...... 5 .0 monomethyltetrachloroterephthalate Coriander, leaves ...... 5 .0 Corn, field, forage ...... 0 .4 (MTP) and tetrachloroterephthalic Corn, field, grain ...... 0 .05 acid (TCP) (calculated as dimethyl Corn, field, stover ...... 0 .4 tetrachloroterephthalate) are estab- Corn, pop, forage ...... 0 .4 Corn, pop, grain ...... 0.05 lished in or on the following food com- Corn, pop, stover ...... 0.4 modities: Corn, sweet, forage ...... 0 .4 Corn, sweet, kernel plus cob with husks re- Commodity Parts per moved ...... 0 .05 million Corn, sweet, stover ...... 0 .4 Cotton, undelinted seed ...... 0 .2 Cantaloupe ...... 1 .0 Cucumber ...... 1 .0 Garlic ...... 1 .0 Dill ...... 5 .0 Ginseng ...... 2 .0 Eggplant ...... 1.0 Horseradish ...... 2.0 Lettuce ...... 2.0 Muskmelon ...... 1 .0 Marjoram ...... 5 .0 Onion, bulb ...... 1 .0 Parsley, dried leaves ...... 20.0 Onion, green ...... 1 .0 Parsley, leaves ...... 5.0 Strawberry ...... 2 .0 Pea, blackeyed, seed ...... 2 .0 Tomato ...... 1.0 Pepper ...... 2 .0 Vegetable, brassica, leafy, group 5 ...... 5.0 Pimento ...... 2 .0 Watermelon ...... 1.0 Potato ...... 2 .0 Radicchio ...... 5.0 (b) Section 18 emergency exemptions. Radish, oriental, roots ...... 2 .0 [Reserved] Radish, oriental, tops ...... 2 .0 Rutabaga ...... 2 .0 (c) Tolerances with regional registra- Soybean ...... 2.0 tions. Tolerances with regional reg- Squash, summer ...... 1 .0 istration, as defined in § 180.1(l), are es- Squash, winter ...... 1 .0 Sweet potato ...... 2.0 tablished for the combined inadvertent Turnip, roots ...... 2 .0 residues of the herbicide dimethyl Turnip, tops ...... 5.0 tetrachloroterephthalate (DCPA) and Yam, true, tuber ...... 2.0 its metabolites monomethyl tetrachloroterephthalate acid (MTP) [72 FR 52018, Sept. 12, 2007, as amended at 73 and terachlorophthalic acid (TCP) (cal- FR 53737, Sept. 17, 2008; 73 FR 80302, Dec. 31, culated as DCPA) in or on the fol- 2008; 74 FR 14744, Apr. 1, 2009] lowing food commodities: § 180.189 Coumaphos; tolerances for Parts per residues. Commodity million (a) General. Tolerances for residues of Radish, roots ...... 2 .0 the insecticide coumaphos (O,O-diethyl Radish, tops ...... 15 .0 O-3-chloro-4-methyl-2-oxo-2H-1- benzopyran-7-yl phosphorothioate and (d) Indirect or inadvertent residues. its oxygen analog (O,O-diethyl O-3- Tolerances are established for the com- chloro-4-methyl-2-oxo-2H-1- bined indirect or inadvertent residues benzopyran-7-yl phosphate) in or on of the herbicide dimethyl food commodities as follows: tetrachloroterephthalate (DCPA) and its metabolites monomethyl Commodity Parts per tetrachloroterephthalate acid (MTP) million and terachlorophthalic acid (TCP) (cal- Cattle, fat ...... 1.0 culated as DCPA) in or on the fol- Cattle, meat ...... 1.0 lowing food commodities: Cattle, meat byproducts ...... 1.0 Goat, fat ...... 1.0 Parts per Goat, meat ...... 1.0 Commodity million Goat, meat byproducts ...... 1.0 Hog, fat ...... 1.0 Basil, dried leaves ...... 20.0 Hog, meat ...... 1.0 Basil, fresh leaves ...... 5 .0 Hog, meat byproducts ...... 1.0 Bean, dry ...... 2.0 Honey ...... 0.15 Bean, mung, seed ...... 2 .0 Honeycomb ...... 45.0

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Commodity Parts per § 180.191 Folpet; tolerances for resi- million dues. Horse, fat ...... 1.0 (a) General. Tolerances are estab- Horse, meat ...... 1.0 lished for the fungicide folpet (N- Horse, meat byproducts ...... 1.0 (trichloromethylthio)phthalimide) in Milk, fat ( = n in whole milk) ...... 0.5 Sheep, fat ...... 1.0 or on raw agricultural commodities as Sheep, meat ...... 1.0 follows: Sheep, meat byproducts ...... 1.0 Parts per Commodity million (b) Section 18 emergency exemptions. [Reserved] Apple 1 ...... 5.0 Cranberry 1 ...... 15.0 (c) Tolerances with regional registra- Cucumber 1 ...... 2.0 tions. [Reserved] Grape 1 ...... 50.0 Grape, raisin 1 ...... 80.0 (d) Indirect or inadvertent residues. Hop, dried cones ...... 120.0 [Reserved] Lettuce 1 ...... 50.0 Melon 1 ...... 3.0 [64 FR 39077, July 21, 1999, as amended at 65 Onion,bulb 1 ...... 2.0 FR 49936, Aug. 16, 2000; 67 FR 46883, July 17, Strawberry 1 ...... 5.0 2002; 69 FR 29458, May 24, 2004; 72 FR 28876, Tomato 1 ...... 25.0 May 23, 2007] 1 No U.S. registrations.

§ 180.190 Diphenylamine; tolerances (b) Section 18 emergency exemptions. for residues. [Reserved] (c) Tolerances with regional registra- (a) General. Tolerances for residues of tions. Tolerances with regional reg- the plant regulator diphenylamine are istrations as defined in § 180.1(l) are es- established in or on the following com- tablished for the fungicide folpet (N- modities: (trichloromethylthio)phthalimide) in or on the following raw agricultural Parts per Commodity million commodity:

Apple, wet pomace ...... 30.0 Commodity Parts per Apple from preharvest or postharvest use, includ- million ing use of impregnated wraps ...... 10.0 Avocado ...... 25.0 Cattle, fat ...... 0.01 Cattle, liver ...... 0.1 Cattle, meat byproducts, except liver ...... 0.01 (d) Indirect or inadvertent residues. Cattle, meat ...... 0.01 [Reserved] Goat, fat ...... 0.01 [61 FR 37222, July 17, 1996, as amended at 68 Goat, liver ...... 0.1 FR 10388, Mar. 5, 2003; 69 FR 52192, Aug. 25, Goat, meat byproducts, except liver ...... 0.01 2004; 72 FR 41928, Aug. 1, 2007] Goat, meat ...... 0.01 Horse, fat ...... 0.01 Horse, liver ...... 0.1 § 180.198 Trichlorfon; tolerances for Horse, meat byproducts, except liver ...... 0.01 residues. Horse, meat ...... 0.01 (a) General. Tolerances are estab- Milk ...... 0.01 lished for residues of the insecticide Pear (post harvest) ...... 5.0 trichlorfon (dimethyl (2,2,2-trichloro-1- Sheep, fat ...... 0.01 Sheep, liver ...... 0.1 hydroxyethyl) phosphonate) in or on Sheep, meat byproducts, except liver ...... 0.01 the following food commodities: Sheep, meat ...... 0.01 Parts per Commodity million (b) Section 18 emergency exemptions. [Reserved] Cattle, fat 1 ...... 0.5 Cattle, meat 1 ...... 0.2 (c) Tolerances with regional registra- Cattle, meat byproducts 1 ...... 0.1 tions. [Reserved] 1 There are no U.S. registrations for cattle commodities as (d) Indirect or inadvertent residues. of June 24, 1999. [Reserved] (b) Section 18 emergency exemptions. [64 FR 25848, May 13, 1999, as amended at 66 [Reserved] FR 63198, Dec. 5, 2001; 72 FR 16283, Apr. 4, (c) Tolerances with regional registra- 2007; 76 FR 34885, June 15, 2011] tions. [Reserved]

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(d) Indirect or inadvertent residues. (c) Tolerances with regional registra- [Reserved] tions. [Reserved] (d) Indirect or inadvertent residues. [72 FR 54578, Sept. 26, 2007] [Reserved] § 180.200 Dicloran; tolerances for resi- [68 FR 39439, July 1, 2003, as amended at 71 dues. FR 56398, Sept. 27, 2006] (a) General. Tolerances are established for residues of the fungicide § 180.204 Dimethoate; tolerances for residues. dicloran, including its metabolites and degradates, in or on the commodities (a) General. Tolerances are estab- in the table in this paragraph. Compli- lished for total residues of the insecti- ance with the tolerance levels specified cide dimethoate (O,O-dimethyl S-(N- in this paragraph is to be determined methylcarbamoylmethyl) by measuring only dicloran, 2,6- phosphorodithioate) including its oxy- dichloro-4-nitroaniline, in or on the gen analog (O,O-dimethyl S-(N- commodity. methylcarbamoylmethyl) phosphorothioate) in or on the fol- Expiration/ lowing food commodities: Commodity Parts per revocation million date Parts per Commodity million Apricot ...... 20 None Bean, snap, succulent ...... 20 None Alfalfa, forage ...... 2.0 Carrot, roots ...... 10 11/2/11 Alfalfa, hay ...... 2.0 Celery ...... 15 None Bean, dry, seed ...... 2.0 Cherry, sweet ...... 20 None Bean, lima ...... 2.0 Cucumber ...... 5 None Bean, snap, succulent ...... 2.0 Endive ...... 10 None Blueberry 1 ...... 1.0 Garlic ...... 5 None Broccoli ...... 2.0 Grape ...... 10 None Cattle, meat byproducts ...... 0.02 Lettuce ...... 10 None Cauliflower ...... 2.0 Nectarine ...... 20 None Celery ...... 2.0 Onion ...... 10 None Citrus, dried pulp ...... 5.0 Peach ...... 20 None Corn, field, forage ...... 1.0 Corn, field, grain ...... 0.1 Plum, prune, fresh ...... 15 None Corn, field, stover ...... 1.0 Potato ...... 0.25 12/31/14 Corn, pop, grain ...... 0.1 Rhubarb ...... 10 None Corn, pop, stover ...... 1.0 Sweet potato, roots ...... 10 None Corn, sweet, forage ...... 1.0 Tomato ...... 5 None Cotton, undelinted seed ...... 0.1 Egg ...... 0.02 (b) Section 18 emergency exemptions. Endive ...... 2.0 [Reserved] Goat, meat byproducts ...... 0.02 Grapefruit ...... 2.0 (c) Tolerances with regional registra- Hog, meat byproducts ...... 0.02 tions. [Reserved] Horse, meat byproducts ...... 0.02 (d) Indirect or inadvertent residues. Kale ...... 2.0 Lemon ...... 2.0 [Reserved] Lettuce, leaf ...... 2.0 Melon ...... 1.0 [77 FR 40815, July 11, 2012] Milk ...... 0.002 Mustard greens ...... 2.0 § 180.202 p-Chlorophenoxyacetic acid; Orange ...... 2.0 tolerances for residues. Pea ...... 2.0 Pear ...... 2.0 (a) General. A tolerance is established Pecan ...... 0.1 for the combined residues of the plant Pepper ...... 2.0 regulator p-chlorophenoxyacetic acid Potato ...... 0.2 Poultry, meat byproducts ...... 0.02 and its metabolite p-chlorophenol to Safflower, seed ...... 0.1 inhibit embryonic root development in Sheep, meat byproducts ...... 0.02 or on the following food commodity: Sorghum, grain, forage ...... 0.1 Sorghum, grain, grain ...... 0.1 Parts per Sorghum, grain, stover ...... 0.1 Commodity million Soybean, forage ...... 2.0 Soybean, hay ...... 2.0 Bean, mung, sprouts ...... 0.2 Soybean, seed ...... 0.05 Swiss chard ...... 2.0 Tangerine ...... 2.0 (b) Section 18 emergency exemptions. Tomato ...... 2.0 [Reserved] Turnip, roots ...... 0.2

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Parts per Parts per Commodity million Commodity million

Turnip, tops ...... 2.0 Cattle, meat ...... 0.05 Wheat, forage ...... 2.0 Cattle, meat byproducts, except kidney ...... 0.05 Wheat, grain ...... 0.04 Cherimoya ...... 0.05 Wheat, hay ...... 2.0 Coffee, bean, green ...... 0.05 Wheat, straw ...... 2.0 Corn, field, forage ...... 3.0 Corn, field, grain ...... 0.1 1 There are U.S. registrations as of August 16, 1996. Corn, field, stover ...... 10.0 (b) Section 18 emergency exemptions. Corn, pop, grain ...... 0.1 Corn, pop, stover ...... 10.0 [Reserved] Corn, sweet, kernel plus cob with husks removed 0.05 (c) Tolerances with regional registra- Cotton, gin byproducts ...... 110.0 tions. Tolerances with regional reg- Cotton, undelinted seed ...... 3.5 istration, as defined in § 180.1(l), are es- Cowpea, forage ...... 0.1 Cowpea, hay ...... 0.4 tablished for total residues of Cranberry ...... 0.05 dimethoate including its oxygen analog Custard apple ...... 0.05 in or on the following food commod- Egg ...... 0.01 Endive ...... 0.05 ities: Feijoa ...... 0.05 Fig ...... 0.05 Commodity Parts per Fruit, citrus, group 10 ...... 0.05 million Fruit, pome, group 11 ...... 0.05 Fruit, stone, group 12 ...... 0.05 Asparagus ...... 0.15 Goat, fat ...... 0.05 Brussels sprouts ...... 5.0 Goat, kidney ...... 0.5 Cherry, sweet ...... 2.0 Goat, meat ...... 0.05 Cherry, tart ...... 2.0 Goat, meat byproducts, except kidney ...... 0.05 Grain, aspirated fractions ...... 65.0 (d) Indirect or inadvertent residues. Grape ...... 0.05 [Reserved] Grass, forage ...... 90.0 Grass, hay ...... 40.0 [65 FR 33697, May 24, 2000, as amended at 69 Guar, seed ...... 0.5 FR 6567, Feb. 11, 2004; 73 FR 53737, Sept. 17, Guava ...... 0.05 2008] Hog, fat ...... 0.05 Hog, kidney ...... 0.5 Hog, meat ...... 0.05 § 180.205 Paraquat; tolerances for resi- Hog, meat byproducts, except kidney ...... 0.05 dues. Hop, dried cones ...... 0.5 (a) General. Tolerances are estab- Horse, fat ...... 0.05 Horse, kidney ...... 0.5 lished for residues of the desiccant, de- Horse, meat ...... 0.05 foliant, and herbicide paraquat (1,1′-di- Horse, meat byproducts, except kidney ...... 0.05 methyl-4,4′-bipyridinium-ion) derived Ilama ...... 0.05 Jaboticaba ...... 0.05 from application of either the Kiwifruit ...... 0.05 bis(methyl sulfate) or the dichloride Lentil, seed ...... 0.3 salt (both calculated as the cation) in Lettuce ...... 0.05 or on the following food commodities: Longan ...... 0.05 Lychee ...... 0.05 Mango ...... 0.05 Parts per Commodity million Milk ...... 0.01 Nut, tree, group 14 ...... 0.05 Acerola ...... 0.05 Okra ...... 0.05 Almond, hulls ...... 0.5 Olive ...... 0.05 Animal feed, nongrass, group 18, forage ...... 75.0 Onion, bulb ...... 0.1 Animal feed, nongrass, group 18, hay ...... 210.0 Onion, green ...... 0.05 Artichoke, globe ...... 0.05 Papaya ...... 0.05 Asparagus ...... 0.5 Passionfruit ...... 0.2 Atemoya ...... 0.05 Pawpaw ...... 0.05 Avocado ...... 0.05 Pea and bean, dried shelled, except soybean, Banana ...... 0.05 subgroup 6C, except guar bean ...... 0.3 Barley, grain ...... 0.05 Pea and bean, succulent shelled, subgroup 6B ... 0.05 Barley, hay ...... 3.5 Pea, field, hay ...... 0.8 Barley, straw ...... 1.0 Pea, field, vines ...... 0.2 Beet, sugar, roots ...... 0.5 Peanut ...... 0.05 Beet, sugar, tops ...... 0.05 Peanut, hay ...... 0.5 Berry group 13 ...... 0.05 Peppermint, tops ...... 0.5 Biriba ...... 0.05 Persimmon ...... 0.05 Cacao bean, bean ...... 0.05 Pineapple ...... 0.05 Canistel ...... 0.05 Pineapple, process residue ...... 0.25 Carrot, roots ...... 0.05 Pistachio ...... 0.05 Cattle, fat ...... 0.05 Pomegranate ...... 0.05 Cattle, kidney ...... 0.5 Pulasan ...... 0.05

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Parts per Sections Affected, which appears in the Commodity million Finding Aids section of the printed volume and at www.govinfo.gov. Rambutan ...... 0.05 Rhubarb ...... 0.05 Rice, grain ...... 0.05 § 180.206 Phorate; tolerances for resi- Safflower, seed ...... 0.05 dues. Sapodilla ...... 0.05 Sapote, black ...... 0.05 (a) General. Tolerances are estab- Sapote, mamey ...... 0.05 lished for the combined residues of the Sapote, white ...... 0.05 insecticide phorate (O,O-diethyl S Sheep, fat ...... 0.05 (ethylthio) meth- Sheep, kidney ...... 0.5 Sheep, meat ...... 0.05 yl]phosphorodithioate), phorate sulf- Sheep, meat byproducts, except kidney ...... 0.05 oxide, phorate sulfone, phorate oxygen Sorghum, forage, forage ...... 0.1 analog, phorate oxygen analog sulf- Sorghum, grain, forage ...... 0.1 Sorghum, grain, grain ...... 0.05 oxide, and phorate oxygen analog Soursop ...... 0.05 sulfone in or on the following food Soybean, forage ...... 0.4 commodities: Soybean, hay ...... 10.0 Soybean, hulls ...... 4.5 Parts per Soybean, seed ...... 0.7 Commodity million Spanish lime ...... 0.05 Spearmint, tops ...... 0.5 Bean, dry, seed ...... 0.05 Star apple ...... 0.05 Bean, succulent ...... 0.05 Starfruit ...... 0.05 Beet, sugar, roots ...... 0.3 Strawberry ...... 0.25 Beet, sugar, tops ...... 3.0 Sugar apple ...... 0.05 Coffee, green bean 1 ...... 0.02 Sugarcane, cane ...... 0.5 Corn, field, forage ...... 0.5 Sugarcane, molasses ...... 3.0 Corn, field, grain ...... 0.05 Sunflower, seed ...... 2.0 Corn, sweet, forage ...... 0.5 Turnip, greens ...... 0.05 Corn, sweet, kernel plus cob with husks removed 0.05 Turnip, roots ...... 0.05 Cotton, undelinted seed ...... 0.05 Vegetable, brassica, leafy, group 5 ...... 0.05 Hop, dried cones ...... 2.0 Vegetable, cucurbit, group 9 ...... 0.05 Peanut ...... 0.1 Vegetable, fruiting, group 8 ...... 0.05 Potato ...... 0.2 Vegetable, legume, edible podded, subgroup 6A 0.05 Sorghum, grain, grain ...... 0.05 Vegetable, tuberous and corm, subgroup 1C ...... 0.50 Sorghum, grain, stover ...... 0.1 Wax jambu ...... 0.05 Soybean, seed ...... 0.05 Wheat, forage ...... 0.5 Wheat, grain ...... 1.1 Sugarcane, cane ...... 0.05 Wheat, hay ...... 3.5 Wheat, forage ...... 1.5 Wheat, straw ...... 50.0 Wheat, grain ...... 0.05 Wheat, hay ...... 1.5 Wheat, straw ...... 0.05 (b) Section 18 emergency exemptions. 1 There are no U.S. registrations as of September 1, 1993 [Reserved] for the use of phorate on the growing crop, coffee. (c) Tolerances with regional registrations. Tolerances with regional reg- (b) Section 18 emergency exemptions. istration as defined in § 180.1(l), are es- [Reserved] tablished for residues of the pesticide (c) Tolerances with regional registra- paraquat (1,1′-dimethyl-4,4′ tions. [Reserved] bipyridinium ion) derived from applica- (d) Indirect or inadvertent residues. tion of either the bis(methyl sulfate) or [Reserved] the dichloride salt (both calculated as [58 FR 62038, Nov. 24, 1993, as amended at 63 the cation) in or on the following food FR 2165, Jan. 14, 1998; 63 FR 57074, Oct. 26, commodities: 1998; 66 FR 50833, Oct. 5, 2001; 67 FR 49616, July 31, 2002; 71 FR 74816, Dec. 13, 2006; 73 FR Parts per 53738, Sept. 17, 2008] Commodity million

Pea, pigeon, seed ...... 0.05 § 180.207 Trifluralin; tolerances for Taro, corm ...... 0.1 residues. Tyfon ...... 0.05 (a) General. Tolerances are estab- (d) Indirect or inadvertent residues. lished for residues of trifluralin, in- [Reserved] cluding its metabolites and degradates, in or on the commodities in the table [46 FR 51614, Oct. 21, 1981] below. Compliance with the tolerance EDITORIAL NOTE: For FEDERAL REGISTER ci- levels specified below is to be deter- tations affecting § 180.205, see the List of CFR mined by measuring only trifluralin

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(2,6-dinitro-N,N-dipropyl-4- benfluralin, N-butyl-N-ethyl-aaa- (trifluoromethyl)benzenamine). trifluoro-2,6-dinitro-p-toluidine, in or on the following food commodities: Parts per Commodity million Parts per Commodity million Alfalfa, forage ...... 3.0 Alfalfa, hay ...... 2.0 Almond, hulls ...... 0.05 Alfalfa, forage ...... 0.05 Asparagus ...... 0.05 Alfalfa, hay ...... 0.05 Barley, grain ...... 0.05 Clover, forage ...... 0.05 Barley, hay ...... 0.05 Clover, hay ...... 0.05 Barley, straw ...... 0.05 Lettuce ...... 0.05 Bean, mung, sprouts ...... 2.0 Trefoil, forage ...... 0.05 Carrot, roots ...... 1.0 Trefoil, hay ...... 0.05 Celery ...... 0.05 Corn, field, forage ...... 0.05 Corn, field, grain ...... 0.05 (b) Section 18 emergency exemptions. Corn, field, stover ...... 0.05 [Reserved] Cotton, gin byproducts ...... 0.05 Endive ...... 0.05 (c) Tolerances with regional registra- Fruit, citrus, group 10 ...... 0.05 tions. [Reserved] Fruit, stone, group 12 ...... 0.05 (d) Indirect or inadvertent residues. Grape ...... 0.05 Hop, dried cones ...... 0.05 [Reserved] Nut, tree, group 14 ...... 0.05 Oilseed, crop group 20 ...... 0.05 [68 FR 39439, July 1, 2003, as amended at 73 Okra ...... 0.05 FR 52613, Sept. 10, 2008] Peanut ...... 0.05 Peanut, hay ...... 0.05 § 180.209 Terbacil; tolerances for resi- Peppermint, oil ...... 2.0 dues. Peppermint, tops ...... 0.05 Rosemary, dried leaves ...... 0.10 (a) General. Tolerances are estab- Rosemary, fresh leaves ...... 0.10 Rosemary, oil ...... 3.0 lished for combined residues of the her- Sorghum, grain, forage ...... 0.05 bicide terbacil, (3-tert-butyl-5-chloro-6- Sorghum, grain, grain ...... 0.05 methyluracil) and its metabolites [3- Sorghum, grain, stover ...... 0.05 tert-butyl-5-chloro-6- Spearmint, oil ...... 2.0 Spearmint, tops ...... 0.05 hydroxymethyluracil], [6-chloro-2,3- Sugarcane, cane ...... 0.05 dihydro-7-hydroxymethyl 3,3-dimethyl- Vegetable, brassica, leafy group 5 ...... 0.05 5H-oxazolo(3,2-a) pyrimidin-5-one], and Vegetable, bulb, group 3 ...... 0.05 Vegetable, cucurbit, group 9 ...... 0.05 [6-chloro-2,3-dihydro-3,3,7-trimethyl- Vegetable, foliage of legume, group 7 ...... 0.05 5H-oxazolo(3,2-a) pyrimidin-5-one], cal- Vegetable, fruiting, group 8 ...... 0.05 culated as terbacil, in or on the fol- Vegetable, leaves of root and tuber, group 2 ...... 0.05 Vegetable, legume, group 6 ...... 0.05 lowing raw agricultural commodities: Vegetable, root and tuber, group 1, except carrot 0.05 Wheat, grain ...... 0.05 Commodity Parts per Wheat, straw ...... 0.05 million

Alfalfa, forage ...... 1.0 (b) Section 18 emergency exemptions. Alfalfa, hay ...... 2.0 [Reserved] Apple ...... 0.3 (c) Tolerances with regional registra- Asparagus ...... 0.4 tions. [Reserved] Blueberry ...... 0 .2 (d) Indirect or inadvertent residues. Caneberry subgroup 13A ...... 0 .2 [Reserved] Peach ...... 0 .2 Peppermint, tops ...... 2 .0 [45 FR 42619, June 25, 1980, as amended at 45 Spearmint, tops ...... 2 .0 FR 56346, Aug. 25, 1980; 45 FR 86493, Dec. 31, Strawberry ...... 0 .1 1980; 46 FR 37250, July 20, 1981; 47 FR 13524, Sugarcane, cane ...... 0.4 Mar. 31, 1982; 47 FR 20309, May 12, 1982; 63 FR Watermelon ...... 1.0 57074, Oct. 26, 1998; 64 FR 39082, July 21, 1999; 70 FR 21643, Apr. 27, 2005; 71 FR 54433, Sept. (b) Section 18 emergency exemptions. 15, 2006; 78 FR 46274, July 31, 2013; 84 FR 4351, [Reserved] Feb. 15, 2019] (c) Tolerances with regional registrations. [Reserved] § 180.208 Benfluralin; tolerances for residues. (d) Indirect or inadvertent residues. [Reserved] (a) General. Tolerances are established for residues of the herbicide [71 FR 30818, May 31, 2006]

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§ 180.210 Bromacil; tolerances for resi- (c) Tolerances with regional registra- dues. tions. [Reserved] (a) General. Tolerances are estab- (d) Indirect or inadvertent residues. lished for residues of the herbicide [Reserved] bromacil (5-bromo-3-sec-butyl-6- [47 FR 25959, June 16, 1982, as amended at 47 methyluracil) in or on the following FR 28381, June 30, 1982; 47 FR 28626, July 1, food commodities: 1982; 47 FR 46701, Oct. 20, 1982; 63 FR 57074, Oct. 26, 1998; 72 FR 53454, Sept. 19, 2007] Commodity Parts per million § 180.212 S-Ethyl cyclohexylethylthio- Fruit, citrus ...... 0.1 carbamate; tolerances for residues. Pineapple ...... 0.1 (a) General. Tolerances are established for residues of the herbicide S- (b) Section 18 emergency exemptions. ethyl cyclohexylethylthiocarbamate in [Reserved] or on the following food commodities: (c) Tolerances with regional registrations. [Reserved] Commodity Parts per (d) Indirect or inadvertent residues. million [Reserved] Beet, garden, roots ...... 0.05(N) Beet, garden, tops ...... 0.05(N) [68 FR 39439, July 1, 2003] Beet, sugar, roots ...... 0.05(N) Beet, sugar, tops ...... 0.05(N) § 180.211 Propachlor; tolerances for Spinach ...... 0.05(N) residues. (b) Section 18 emergency exemptions. (a) General. Tolerances are estab- [Reserved] lished for the combined residues of the (c) Tolerances with regional registra- herbicide propachlor (2-chloro-N- tions. [Reserved] isopropylacetanilide) and its metabo- (d) Indirect or inadvertent residues. lites containing the N-isopropylaniline [Reserved] moiety, calculated as 2-chloro-N- isopropylacetanilide, in or on the fol- [68 FR 39439, July 1, 2003] lowing raw agricultural commodities: § 180.213 Simazine; tolerances for resi- Parts per dues. Commodity million (a) General. Tolerances are estab- Cattle, fat ...... 0.05 lished for the combined residues of the Cattle, kidney ...... 0.2 herbicide simazine (2-chloro-4,6- Cattle, meat ...... 0.02 Cattle, meat byproducts, except kidney ...... 0.05 bis(ethylamino)-s-triazine) and its two Corn, field, forage ...... 3.0 chlorinated degradates (2-amino-4- Corn, field, grain ...... 0.2 chloro-6-ethylamino-s-triazine and 2,4- Corn, field, stover ...... 1.0 diamino-6-chloro-s-triazine), the total Corn, sweet, forage ...... 3.0 Goat, fat ...... 0.05 residue to be measured in or on the fol- Goat, kidney ...... 0.2 lowing food commodities: Goat, meat ...... 0.02 Goat, meat byproducts, except kidney ...... 0.05 Parts per Hog, fat ...... 0.02 Commodity million Hog, meat ...... 0.02 Hog, meat byproducts ...... 0.02 Almond ...... 0.25 Horse, fat ...... 0.05 Almond, hulls ...... 0.25 Horse, kidney ...... 0.2 Apple ...... 0.20 Horse, meat ...... 0.02 Avocado ...... 0.20 Horse, meat byproducts, except kidney ...... 0.05 Blackberry ...... 0.20 Milk ...... 0.02 Blueberry ...... 0.20 Sheep, fat ...... 0.05 Cattle, meat ...... 0.03 Sheep, kidney ...... 0.2 Cattle, meat byproducts ...... 0.03 Sheep, meat ...... 0.02 Cherry ...... 0.25 Sheep, meat byproducts, except kidney ...... 0.05 Corn, field, forage ...... 0.20 Sorghum, forage, forage ...... 8.0 Corn, field, grain ...... 0.20 Sorghum, grain, forage ...... 8.0 Corn, field, stover ...... 0.25 Sorghum, grain, grain ...... 0.25 Corn, pop, grain ...... 0.20 Sorghum, grain, stover ...... 12.0 Corn, pop, stover ...... 0.25 Corn, sweet, forage ...... 0.20 Corn, sweet, kernel plus cob with husks removed 0.25 (b) Section 18 emergency exemptions. Corn, sweet, stover ...... 0.25 [Reserved] Cranberry ...... 0.25

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Parts per Parts per Commodity million Commodity million

Currant ...... 0.25 Eggplant ...... 0.5 Egg ...... 0.03 Grape ...... 0.5 Goat, meat ...... 0.03 Grapefruit ...... 3 Goat, meat byproducts ...... 0.03 Grass, forage ...... 10 Grape ...... 0.20 Hop, dried cones ...... 0.5 Grapefruit ...... 0.25 Kale ...... 3 Hazelnut ...... 0.20 Horse, meat ...... 0.03 Legume, forage ...... 10 Horse, meat byproducts ...... 0.03 Lemon ...... 3 Lemon ...... 0.25 Melon ...... 0.5 Loganberry ...... 0.20 Orange, sweet ...... 3 Milk ...... 0.03 Peach ...... 0.5 Nut, macadamia ...... 0.25 Pea, succulent ...... 0.5 Olive ...... 0.20 Pepper ...... 0.5 Orange ...... 0.25 Pumpkin ...... 0.5 Peach ...... 0.20 Safflower, seed ...... 0.5 Pear ...... 0.25 Spinach ...... 3 Pecan ...... 0.20 Squash, summer ...... 0.5 Plum ...... 0.20 Squash, winter ...... 0.5 Raspberry ...... 0.20 Sheep, meat ...... 0.03 Strawberry ...... 1 Sheep, meat byproducts ...... 0.03 Swiss chard ...... 3 Strawberry ...... 0.25 Tangerine ...... 3 Walnut ...... 0.2 Tomato ...... 0.5 Turnip, greens ...... 3 (b) Section 18 emergency exemptions. Walnut ...... 0.5 [Reserved] (c) Tolerances with regional registra- (2) A tolerance of 0.5 part per million tions. [Reserved] is established for the pesticide naled in (d) Indirect or inadvertent residues. or on all raw agricultural commodities, [Reserved] except those otherwise listed in this section, from use of the pesticide for [63 FR 2165, Jan. 14, 1998, as amended at 63 area pest (mosquito and fly) control. FR 57074, Oct. 26, 1998; 72 FR 35665, June 29, (b) Section 18 emergency exemptions. 2007; 72 FR 53454, Sept. 19, 2007] [Reserved] § 180.215 Naled; tolerances for resi- (c) Tolerances with regional registra- dues. tions. [Reserved] (a) General. (1) Tolerances are estab- (d) Indirect or inadvertent residues. lished for residues of the insecticide [Reserved] naled (1,2-dibromo-2,2-dichloro-ethyl [42 FR 46304, Sept. 15, 1977, as amended at 54 dimethyl phosphate) and its conversion FR 20125, May 10, 1989; 63 FR 57074, Oct. 26, product 2,2-dichlorovinyl dimethyl 1998; 66 FR 50833, Oct. 5, 2001; 77 FR 59124, phosphate, expressed as naled, result- Sept. 26, 2012] ing from the application of the pesticide to growing crops or from direct § 180.217 Metiram; tolerances for residues. application to livestock and poultry, in or on the following raw agricultural (a) General. Tolerances are estab- commodities: lished for residues of a metiram (a mixture of 5.2 parts by weight of ammoni- Parts per ates of [ethylenebis (dithiocarbamato)] Commodity million zinc with 1 part by weight ethylenebis Almond, hulls ...... 0.5 [dithiocarbamic acid] bimolecular and Almond ...... 0.5 trimolecular cyclic anhydrosulfides Bean, dry, seed ...... 0.5 Bean, succulent ...... 0.5 and disulfides), including its metabo- Beet, sugar, roots ...... 0.5 lites and degradates, in or on the com- Beet, sugar, tops ...... 0.5 modities in the following table. Com- Broccoli ...... 1 Brussels sprouts ...... 1 pliance with the tolerance levels speci- Cabbage ...... 1 fied in this paragraph is to be deter- Cauliflower ...... 1 mined by measuring only those Celery ...... 3 metiram residues convertible to and Collards ...... 3 Cotton, undelinted seed ...... 0.5 expressed in terms of the degradate Cucumber ...... 0.5 carbon disulfide.

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Parts per Parts per Commodity million Commodity million

Apple ...... 0.5 Wheat, straw ...... 0.50 Apple, pomace, wet ...... 2 Banana 1 ...... 3 (b) Section 18 emergency exemptions. Grape, wine 1 ...... 5 Potato ...... 0.2 [Reserved] (c) Tolerances with regional registra- 1 There are no U.S. registrations on bananas and grape, wine as of April 29, 2011. tions. [Reserved] (d) Indirect or inadvertent residues. (b) Section 18 emergency exemptions. Tolerances are established for indirect [Reserved] or inadvertant residues of atrazine, 2- (c) Tolerances with regional registra- chloro-4-ethylamino-6-isopropylamino- tions. [Reserved] s-triazine, in or on the following raw (d) Indirect or inadvertent residues. agricultural commodity when present [Reserved] therein as a result of application of [63 FR 57074, Oct. 26, 1998, as amended at 76 atrazine to the growing crops in para- FR 23891, Apr. 29, 2011] graph (a) of this section:

§ 180.220 Atrazine; tolerances for resi- Commodity Parts per dues. million (a) General. Tolerances are estab- Vegetable, leafy, except brassica, group 4 ...... 0.25 lished for the combined residues of the herbicide atrazine (2-chloro-4- [43 FR 29121, July 6, 1978, as amended at 44 ethylamino-6-isopropylamino-s-tri- FR 67116, Nov. 23, 1979; 47 FR 3771, Jan. 27, azine) and its chlorinated metabolites 1982; 47 FR 8012, Feb. 24, 1982; 63 FR 57075, 2-amino-4-chloro-6-isopropylamino-s- Oct. 26, 1998; 67 FR 46893, July 17, 2002; 69 FR triazine, 2-amino-4-chloro-6- 6567, Feb. 11, 2004; 72 FR 35666, June 29, 2007; ethylamino-s-triazine, and 2,4-diamino- 72 FR 53454, Sept. 19, 2007; 73 FR 37852, July 2, 2008; 76 FR 56654, Sept. 14, 2011] 6-chloro-s-triazine, in or on the following food commodities: § 180.222 Prometryn; tolerances for residues. Parts per Commodity million (a) General. Tolerances are estab- Cattle, fat ...... 0.02 lished for residues of the herbicide Cattle, meat ...... 0.02 prometryn, including its metabolites Cattle, meat byproducts ...... 0.02 and degradates, in or on the commod- Corn, field, forage ...... 1.5 ities in the following table. Compliance Corn, field, grain ...... 0.20 Corn, field, stover ...... 0.5 with the tolerance levels specified in Corn, pop, forage ...... 1.5 the following table is to be determined Corn, pop, grain ...... 0.20 by measuring only prometryn, 2,4- Corn, pop, stover ...... 0.5 Corn, sweet, forage ...... 15 bis(isopropylamino)-6-methylthio-s-tri- Corn, sweet, kernel plus cob with husks removed 0.20 azine, in or on the following raw agri- Corn, sweet, stover ...... 2.0 cultural commodities: Goat, fat ...... 0.02 Goat, meat ...... 0.02 Parts per Goat, meat byproducts ...... 0.02 Commodity million Grass, forage ...... 4.0 Grass, hay ...... 4.0 Bean, snap, succulent ...... 0.05 Guava ...... 0.05 Carrot, roots ...... 0.45 Horse, fat ...... 0.02 Celeriac, roots ...... 0.05 Horse, meat ...... 0.02 Celeriac, tops ...... 0.20 Horse, meat byproducts ...... 0.02 Celtuce ...... 0.50 Milk ...... 0.02 Cilantro, leaves ...... 3.5 Nut, macadamia ...... 0.20 Coriander, dried leaves ...... 9.0 Sheep, fat ...... 0.02 Cotton, gin byproducts ...... 1.0 Sheep, meat ...... 0.02 Cottonseed subgroup 20C ...... 0.25 Sheep, meat byproducts ...... 0.02 Dill, oil ...... 1.3 Sorghum, forage, forage ...... 0.25 Dillweed, dried leaves ...... 1.1 Sorghum, grain, forage ...... 0.25 Dillweed, fresh leaves ...... 0.30 Sorghum, grain, grain ...... 0.20 Fennel, Florence, fresh leaves and stalk ...... 0.50 Sorghum, grain, stover ...... 0.50 Leaf petiole vegetable subgroup 22B ...... 0.50 Sugarcane, cane ...... 0.20 Okra ...... 0.05 Wheat, forage ...... 1.5 Parsley, dried leaves ...... 1.5 Wheat, grain ...... 0.10 Parsley, leaves ...... 0.60 Wheat, hay ...... 5.0 Pea, pigeon, seed ...... 0.25

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Parts per Parts per Commodity million Commodity million

Sesame, seed ...... 0.05 Banana ...... 0.01 Swiss chard ...... 0.50 Barley, grain ...... 0.1 Cabbage, Chinese, bok choy ...... 0.01 (b) Section 18 emergency exemptions. Cabbage, Chinese, napa ...... 0.01 [Reserved] Cacao bean, dried bean ...... 0.1 Cashew ...... 0.1 (c) Tolerances with regional exemptions. Citron, citrus ...... 0.01 [Reserved] Coffee, bean, green ...... 0.1 (d) Indirect or inadvertent residues. Corn, field, grain ...... 0.1 Tolerances are established for indirect Corn, pop, grain ...... 0.1 Cotton, undelinted seed ...... 0.1 or inadvertent residues of the herbicide Date, dried fruit ...... 0.1 prometryn, including its metabolites Dill, seed ...... 0.01 and degradates, in or on the commod- Eggplant ...... 0.01 ities in the following table. Compliance Endive ...... 0.01 Grapefruit ...... 0.01 with the tolerance levels specified in Hazelnut ...... 0.1 the following table is to be determined Kumquat ...... 0.01 by measuring only prometryn, 2,4- Lemon ...... 0.01 bis(isopropylamino)-6-methylthio-s-tri- Lettuce ...... 0.01 Lime ...... 0.01 azine, in or on the following raw agri- Mango ...... 0.01 cultural commodities. Millet, grain ...... 0.1 Mushroom ...... 0.01 Commodity Parts per Nut, brazil ...... 0.1 million Oat, grain ...... 0.1 Okra ...... 0.01 Barley, forage ...... 0.3 Orange, sweet ...... 0.01 Barley, hay ...... 1.0 Papaya ...... 0.01 Barley, straw ...... 0.3 Peanut ...... 0.1 Oat, forage ...... 0.3 Pecan ...... 0.1 Oat, hay ...... 1.0 Oat, straw ...... 0.3 Pepper ...... 0.01 Rye, forage ...... 0.3 Persimmon ...... 0.01 Rye, hay ...... 1.0 Pistachio ...... 0.1 Rye, straw ...... 0.3 Rice, grain ...... 0.1 Triticale, forage ...... 0.3 Rye, grain ...... 0.1 Triticale, hay ...... 1.0 Safflower, seed ...... 0.1 Triticale, straw ...... 0.3 Salsify, tops ...... 0.01 Wheat, forage ...... 0.3 Sesame, seed ...... 0.1 Wheat, hay ...... 1.0 Sorghum, grain ...... 0.1 Wheat, straw ...... 0.3 Soybean, seed ...... 0.1 Sunflower, seed ...... 0.1 Sweet potato, roots ...... 0.01 [43 FR 29121, July 6, 1978, as amended at 45 Tangelo ...... 0.01 FR 51782, Aug. 5, 1980; 54 FR 6918, Feb. 15, Tangerine ...... 0.01 1989; 60 FR 20434, Apr. 26, 1995; 63 FR 17692, Tomato ...... 0.01 Apr. 10, 1998; 63 FR 57075, Oct. 26, 1998; 64 FR Vegetable, legume, group 6, except soybean .... 0.01 39082, July 21, 1999; 74 FR 47456, Sept. 16, 2009; Walnut ...... 0.1 74 FR 67108, Dec. 18, 2009; 76 FR 34885, June Wheat, grain ...... 0.1 15, 2011; 78 FR 55640, Sept. 11, 2013; 82 FR 57144, Dec. 4, 2017] (2) Tolerances are established for residues of the fumigant in or on all RACs § 180.225 Phosphine; tolerances for resulting from preharvest treatment of residues. pest burrows in agricultural and non- (a) General. (1) Tolerances are estab- crop land areas. lished for residues of phosphine in or Parts per on the following raw agricultural com- Commodity million modities (RACs) resulting from post- All raw agricultural commodities resulting from harvest fumigation for the control of preharvest treatment of pest burrows ...... 0.01 insects with phosphine gas or phosphide compounds that produce (3) Residues resulting from fumiga- phosphine gas. tion of processed food:

Commodity Parts per Parts per million Commodity million

Almond ...... 0.1 Processed food ...... 0 .01 Avocado ...... 0.01

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(4) Residues resulting from fumigation Commodity Parts per of animal feed: million Horse, meat ...... 0.05 Parts per Commodity million Horse, meat byproducts ...... 0.05 Milk ...... 0.02 Animal feed ...... 0.1 Potato ...... 0.1 Poultry, fat ...... 0.05 (5) To assure safe use of this pes- Poultry, meat ...... 0.05 Poultry, meat byproducts ...... 0.05 ticide, it must be used in compliance Sheep, fat ...... 0.05 with the labeling conforming to that Sheep, meat ...... 0.05 registered by the U.S. Environmental Sheep, meat byproducts ...... 0.05 Protection Agency (EPA) under FIFRA. Labeling shall bear a restric- (2)(i) Tolerances are established for tion to aerate the finished food/feed for residues of the herbicide diquat (6,7 48 hours before it is offered to the con- dihydrodipyrido(1,2-a:2’1’- sumer, unless EPA specifically deter- c)pyrazinediium) (calculated as the mines that a different time period is cation) derived from the application of appropriate. Where appropriate, a the dibromide salt to ponds, lakes, res- warning shall state that under no con- ervoirs, marshes, drainage ditches, ca- dition should any formulation con- nals, streams, and rivers which are taining aluminum or magnesium slow-moving or quiescent in programs phosphide be used so that it will come of the Corp of Engineers or other Fed- in contact with any processed food, ex- eral or State public agencies and to cept processed brewer’s rice, malt, and ponds, lakes and drainage ditches only corn grits stored in breweries for use in where there is little or no outflow of the manufacture of beer. water and which are totally under the (b) Section 18 emergency exemptions. control of the user, in or on the fol- [Reserved] lowing food commodities: (c) Tolerances with regional registra- Parts per tions. [Reserved] Commodity million (d) Indirect or inadvertant residues. [Reserved] Avocado ...... 0.2 Berry group 13 ...... 0.05 [64 FR 72950, Dec. 29, 1999, as amended at 71 Cotton, undelinted seed ...... 0.2 FR 74816, Dec. 13, 2006; 72 FR 41929, Aug. 1, Cranberry ...... 0.05 2007; 74 FR 46372, Sept. 9, 2009] Fish ...... 2.0 Fruit, citrus, group 10 ...... 0.05 Fruit, pome, group 11 ...... 0.02 § 180.226 Diquat; tolerances for resi- Fruit, stone, group 12 ...... 0.02 dues. Grain, cereal, forage, fodder and straw, group 16 0.02 (a) General. (1) Tolerances are estab- Grain, cereal, group 15 ...... 0.02 Grape ...... 0.05 lished for residues of the plant growth Grass, forage, fodder and hay, group 17 ...... 0.2 regulator and herbicide diquat, (6,7- Hop, dried cones ...... 0.2 dihydrodipyrido (1,2-a:2′1′- Nut, tree, group 14 ...... 0.02 Shellfish ...... 20.0 c)pyrazinediium) derived from applica- Strawberry ...... 0.05 tion of the dibromide salt and cal- Sugarcane, cane ...... 0.2 culated as the cation in or on the fol- Vegetable, brassica, leafy, group 5 ...... 0.05 lowing food commodities: Vegetable, cucurbit, group 9 ...... 0.02 Vegetable, foliage of legume, group 7 ...... 0.2 Parts per Vegetable, fruiting, group 8 ...... 0.05 Commodity million Vegetable, leafy, except brassica, group 4 ...... 0.05 Vegetable, root and tuber, group 1 ...... 0.02 Alfalfa, seed ...... 3.0 Vegetable, seed and pod ...... 0.05 Cattle, fat ...... 0.05 Cattle, meat ...... 0.05 (ii) Where tolerances are established Cattle, meat byproducts ...... 0.05 Canola, meal ...... 6.0 at higher levels from other uses of Canola, seed ...... 2.0 diquat on the subject crops, the higher Egg ...... 0.05 tolerances applies also to residues of Goat, fat ...... 0.05 Goat, meat ...... 0.05 the aquatic uses cited in this para- Goat, meat byproducts ...... 0.05 graph. Hog, fat ...... 0.05 (3) Tolerances are established for the Hog, meat ...... 0.05 Hog, meat byproducts ...... 0.05 plant growth regulator diquat (6,7 Horse, fat ...... 0.05 dihydrodipyrido(1,2-a:2’1’-

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c)pyrazinediium) derived from applica- Commodity Parts per tion of the dibromide salt and cal- million culated as the cation in or on the fol- Rye, forage ...... 90.0 lowing food commodites: Rye, grain ...... 2.0 Rye, straw ...... 30.0 Parts per Sorghum, grain, forage ...... 3.0 Commodity million Sorghum, grain, grain ...... 4.0 Sorghum, grain, stover ...... 10.0 Banana1 ...... 0.05 Sugarcane, cane ...... 0.3 Coffee, bean, green1 ...... 0.05 Sugarcane, molasses ...... 5.0 Soybean, hulls ...... 0.6 Teff, forage ...... 90.0

1 Teff, grain ...... 6.0 There are no U.S. registrations as of May 26, 2010. Teff, hay ...... 40.0 (4) A tolerance of 0.5 part per million Teff, straw ...... 30.0 Wheat, forage ...... 90.0 is established for residues of diquat in Wheat, grain ...... 2.0 potato, granules/flakes and potato, Wheat, hay ...... 40.0 chips. Wheat, straw ...... 30.0 (b) Section 18 emergency exemptions. [Reserved] (2) Tolerances are established for res- (c) Tolerances with regional registra- idues of the herbicide dicamba, 3,6- tions. [Reserved] dichloro-o-anisic acid, including its (d) Indirect or inadvertent residues. metabolites and degradates, in or on [Reserved] the commodities in the table below. Compliance with the tolerance levels is [65 FR 33709, May 24, 2000, as amended at 72 to be determined by measuring only FR 41929, Aug. 1, 2007; 75 FR 29441, May 26, the residues of dicamba (3,6-dichloro-o- 2010; 75 FR 60241, Sept. 29, 2010] anisic acid) and its metabolite, 3,6- § 180.227 Dicamba; tolerances for resi- dichloro-2-hydroxybenzoic acid, cal- dues. culated as the stoichiometric equivalent of dicamba, in or on the following (a) General. (1) Tolerances are estab- commodities: lished for the residues of the herbicide dicamba (3,6-dichloro-o-anisic acid), in- Commodity Parts per cluding its metabolites and degradates, million in or on the commodities in the table Asparagus ...... 4.0 below. Compliance with the tolerance Cattle, fat ...... 0.3 levels is to be determined by meas- Cattle, kidney ...... 25.0 Cattle, meat ...... 0.25 uring only the sum of the residues of Cattle, meat byproducts, except kidney ...... 3.0 dicamba (3,6-dichloro-o-anisic acid) and Goat, fat ...... 0.3 its metabolite, 3,6-dichloro-5-hydroxy- Goat, kidney ...... 25.0 Goat, meat ...... 0.25 o-anisic acid, calculated as the stoi- Goat, meat byproducts, except kidney ...... 3.0 chiometric equivalent of dicamba, in or Hog, fat ...... 0.3 on the following commodities: Hog, kidney ...... 25.0 Hog, meat ...... 0.25 Hog, meat byproducts, except kidney ...... 3.0 Parts per Commodity million Horse, fat ...... 0.3 Horse, kidney ...... 25.0 Barley, grain ...... 6.0 Horse, meat ...... 0.25 Barley, hay ...... 2.0 Horse, meat byproducts, except kidney ...... 3.0 Barley, straw ...... 15.0 Milk ...... 0.2 Corn, field, forage ...... 3.0 Sheep, fat ...... 0.3 Corn, field, grain ...... 0.1 Sheep, kidney ...... 25.0 Corn, field, stover ...... 3.0 Sheep, meat ...... 0.25 Corn, pop, grain ...... 0.1 Sheep, meat byproducts, except kidney ...... 3.0 Corn, pop, stover ...... 3.0 Corn, sweet, forage ...... 0.50 (3) Tolerances are established for res- Corn, sweet, kernel plus cob with husks removed 0.04 idues of the herbicide dicamba, 3,6- Corn, sweet, stover ...... 0.50 Grass, forage, fodder and hay, group 17, forage 125.0 dichloro-o-anisic acid, including its Grass, forage, fodder and hay, group 17, hay ...... 200.0 metabolites and degradates, in or on Millet, proso, forage ...... 90.0 the commodities in the table below. Millet, proso, grain ...... 2.0 Millet, proso, hay ...... 40.0 Compliance with the tolerance levels is Millet, proso, straw ...... 30.0 to be determined by measuring only Oat, forage ...... 90.0 the residues of dicamba, 3,6-dichloro-o- Oat, grain ...... 2.0 Oat, hay ...... 40.0 anisic acid, and its metabolites, 3,6- Oat, straw ...... 30.0 dichloro-5-hydroxy-o-anisic acid, and

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3,6-dichloro-2-hydroxybenzoic acid, cal- Commodity Parts per culated as the stoichiometric equiva- million lent of dicamba, in or on the following Milk ...... 0.02 commodities: Poultry, fat ...... 0.1 Poultry, meat ...... 0 .1 Parts per Poultry, meat byproducts ...... 0.1 Commodity million Sheep, meat byproducts ...... 0 .1

Cotton, gin byproducts ...... 70 Cotton, undelinted seed ...... 3.0 (b) Section 18 emergency exemptions. Grain, aspirated fractions ...... 1000 [Reserved] Soybean, forage ...... 60 (c) Tolerances with regional registra- Soybean, hay ...... 100 tions. [Reserved] Soybean, hulls ...... 30.0 Soybean, seed ...... 10.0 (d) Indirect or inadvertent residues. Tolerances are established for the com- (b) Section 18 emergency exemptions. bined residues of the herbicide [Reserved] fluometuron, N, N-dimethyl-N’-[3- (c) Tolerances with regional registra- (trifluoromethyl)phenyl]urea, and its tions. [Reserved] metabolite, trifluoromethylaniline (d) Indirect or inadvertent residues. (TFMA) determined as TFMA, in or on [Reserved] the following food commodities.

[65 FR 33709, May 24, 2000, as amended at 72 Parts per FR 35665, June 29, 2007; 73 FR 17918, Apr. 2, Commodity million 2008; 73 FR 54960, Sept. 24, 2008; 75 FR 60241, Sept. 29, 2010; 76 FR 55806, Sept. 9, 2011; 81 FR Grain, cereal, forage, fodder, and straw group 16, 88634, Dec. 8, 2016] forage ...... 3.0 Grain, cereal, forage, fodder, and straw, group 16, stover ...... 6.0 § 180.229 Fluometuron; tolerances for Grain, cereal, group 15 ...... 0.5 residues. Peanut ...... 0.1 Peanut, hay ...... 4.0 (a) General. (1) Tolerances are estab- Peanut, meal ...... 0.2 lished for the combined residues of the Soybean, forage ...... 3.0 herbicide fluometuron, N, N-dimethyl- Soybean, hay ...... 3.0 Soybean, seed ...... 2.0 N’-[3-(trifluoromethyl)phenyl]urea, and Rice, hulls ...... 1.0 its metabolite, trifluoromethylaniline Wheat, milled byproducts ...... 1.0 (TFMA) determined as TFMA, in or on the following food commodities: [73 FR 52613, Sept. 10, 2008] Parts per Commodity million § 180.231 Dichlobenil; tolerances for residues. Cotton, gin byproducts ...... 3.5 Cotton, undelinted seed ...... 1.0 (a) General. Tolerances are established for the combined residues of the (2) Tolerances are established for the herbicide dichlobenil (2,6- combined residues of the herbicide dichlorobenzonitrile) and its metabo- fluometuron, N,N-dimethyl-N’-[3- lite 2,6-dichlorobenzamide in or on the (trifluoromethyl)phenyl]urea, and its following raw agricultural commod- metabolites determined as TFMA and ities: the hydroxylated metabolites: CGA- Parts per 236431, 1-(4-hydroxy-3- Commodity million trifluoromethylphenyl)urea; CGA- 236432, 1-methyl-3-(4-hydroxy-3- Apple ...... 0.5 Bushberry subgroup 13–07B ...... 0.15 trifluoromethylphenyl)urea; and CGA- Caneberry subgroup 13–07A ...... 0.10 13211, 1,1-dimethyl-3-(4-hydroxy-3- Cranberry ...... 0.1 trifluoromethylphenyl)urea, in or on Fruit, stone, group 12 ...... 0.15 Grape ...... 0.15 the following food commodities: Hazelnut ...... 0.1 Pear ...... 0.5 Parts per Rhubarb ...... 0.06 Commodity million

Cattle, meat byproducts ...... 0.1 (b) Section 18 emergency exemptions. Egg ...... 0 .1 [Reserved] Goat, meat byproducts ...... 0 .1 Hog, meat byproducts ...... 0 .1 (c) Tolerances with regional registra- Horse, meat byproducts ...... 0 .1 tion. [Reserved]

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(d) Indirect or inadvertent residues. (c) Tolerances with regional registra- [Reserved] tions. [Reserved] (d) Indirect or inadvertent residues. [36 FR 22540, Nov. 25, 1971, as amended at 63 FR 57075, Oct. 26, 1998; 66 FR 63198, Dec. 5, [Reserved] 2001; 73 FR 50570, Aug. 27, 2008] [47 FR 55223, Dec. 8, 1982, as amended at 55 FR 26440, June 28, 1990; 56 FR 29183, June 26, § 180.235 Dichlorvos; tolerances for 1991; 63 FR 57075, Oct. 26, 1998; 65 FR 33697, residues. May 24, 2000; 74 FR 46373, Sept. 9, 2009; 77 FR (a) General. (1) Tolerances for resi- 59125, Sept. 26, 2012] dues of the insecticide 2,2-dichlorovinyl dimethyl phosphate are established as § 180.236 Triphenyltin hydroxide; tolerances for residues. follows: (a) General. Tolerances are estab- Parts per lished for the combined residues of the Commodity million fungicide triphenyltin hydroxide Cattle, fat ...... 0.02(N) (TPTH) and its monophenyltin (MPTH) Cattle, meat ...... 0.02(N) and diphenyltin (DPTH) hydroxide and Cattle, meat byproducts ...... 0.02(N) Egg ...... 0.05(N) oxide metabolites, expressed in terms Goat, fat ...... 0.02(N) of parent TPTH, in or on the following Goat, meat ...... 0.02(N) raw agricultural commodities: Goat, meat byproducts ...... 0.02(N) Horse, fat ...... 0.02(N) Parts per Horse, meat ...... 0.02(N) Commodity million Horse, meat byproducts ...... 0.02(N) Milk ...... 0.02(N) Beet, sugar, roots ...... 0.05 Mushroom (residues expressed as naled) ...... 0.5 Beet, sugar, tops ...... 10.0 Poultry, fat ...... 0.05(N) Cattle, fat ...... 0.2 Poultry, meat ...... 0.05(N) Cattle, kidney ...... 2.0 Poultry, meat byproducts ...... 0.05(N) Cattle, liver ...... 4.0 Raw agricultural commodities, nonperishable, Cattle, meat ...... 0.5 bulk stored regardless of fat content, Goat, fat ...... 0.2 postharvest ...... 0.5 Goat, kidney ...... 2.0 Raw agricultural commodities nonperishable, Goat, liver ...... 4.0 packaged or bagged, containing 6 percent fat Goat, meat ...... 0.5 or less, postharvest ...... 0.5 Hog, fat ...... 0.3 Raw agricultural commodities, nonperishable, Hog, meat ...... 0.06 packaged or bagged, containing more than 6 Hog, meat byproducts ...... 0.3 percent fat, postharvest ...... 2 Horse, fat ...... 0.2 Sheep, fat ...... 0.02(N) Horse, kidney ...... 2.0 Sheep, meat ...... 0.02(N) Horse, liver ...... 4.0 Sheep, meat byproducts ...... 0.02(N) Horse, meat ...... 0.5 Milk ...... 0.06 (2) The tolerance of 0.1 part per mil- Pecan ...... 0.05 Potato ...... 0.05 lion prescribed by 21 CFR 556.180 for Sheep, fat ...... 0.2 negligible residues of 2,2-dichlorovinyl Sheep, kidney ...... 2.0 dimethyl phosphate in hog, fat; hog, Sheep, liver ...... 4.0 meat; hog, meat byproducts; and hog, Sheep, meat ...... 0.5 skin covers both its use as an anthel- mintic in swine feed and as an insecti- (b) Section 18 emergency exemptions. cide applied directly to swine. [Reserved] (3) Dichlorvos may be present as a (c) Tolerances with regional registra- residue from application as an insecti- tions. [Reserved] cide on packaged or bagged nonperish- (d) Indirect or inadvertent residues. able processed food (see: 21 CFR [Reserved] 170.3(j)) in an amount in such food not [72 FR 41929, Aug. 1, 2007] in excess of 0.5 part per million (ppm). To assure safe use of the insecticide, § 180.241 Bensulide; tolerances for res- its label and labeling shall conform to idues. the label and labeling registered by the (a) General. Tolerances are estab- U.S. Environmental Protection Agen- lished for the residues of S-(O,O- cy, and the usage employed shall con- diisopropyl phosphorodithioate) of N- form with such label or labeling. (2-mercaptoethyl) benzenesulfonamide (b) Section 18 emergency exemptions. including its oxygen analog S-(O,O- [Reserved] diisopropyl phosphorothioate) of N-(2-

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mercaptoethyl) benzenesulfonamide in Commodity Parts per or on the following food commodities: million Citrus, oil ...... 15.0 Parts per Commodity million Corn, field, forage ...... 0.01 Corn, field, grain ...... 0.01 Onion, bulb ...... 0.10 Corn, field, stover ...... 0.01 Vegetable, brassica, leafy group 5 ...... 0.15 Corn, pop, forage ...... 0.01 Vegetable, cucurbits group 9 ...... 0.15 Corn, pop, grain ...... 0.01 Vegetable, fruiting group 8 ...... 0.10 Corn, pop, stover ...... 0.01 Vegetable, leafy except brassica group 4 ...... 0.15 Corn, sweet, forage ...... 0.01 Corn, sweet, kernels plus cop with husks removed ...... 0.01 (b) Section 18 emergency exemptions. Corn, sweet, stover ...... 0.01 [Reserved] Fruit, citrus, group 10, postharvest ...... 10.0 (c) Tolerances with regional registra- Fruit, pome, group 11, postharvest ...... 5.0 Mango ...... 10.0 tions. Tolerances with regional reg- Mushroom ...... 40.0 istration, as defined in § 180.1(l), are es- Oats, forage ...... 0.30 tablished for the residues of S-(O,O- Oats, grain ...... 0.05 Oats, hay ...... 0.30 diisopropyl phosphorodithioate) of N- Oats, straw ...... 0.30 (2-mercaptoethyl) benzenesulfonamide Onion, bulb, subgroup 3–07A ...... 0.02 including its oxygen analog S-(O,O- Papaya, postharvest ...... 5.0 Potato, postharvest ...... 10.0 diisopropyl phosphorothioate) of N-(2- Radish, tops ...... 0.02 mercaptoethyl) benzenesulfonamide in Rye, forage ...... 0.30 or on the following food commodities: Rye, grain ...... 0.05 Rye, straw ...... 0.30 2 Parts per Soybean ...... 0.1 Commodity million Spinach ...... 0.02 Strawberry 1 ...... 5.0 Carrot, roots ...... 0.10 Sweet potato (postharvest to sweet potato intended only for use as seed) ...... 0.05 Triticale, forage ...... 0.30 (d) Indirect or inadvertent residues. Triticale, grain ...... 0.05 [Reserved] Triticale, hay ...... 0.30 Triticale, straw ...... 0.30 [68 FR 39440, July 1, 2003, as amended at 73 Vegetable, cucurbit, group 9 ...... 0.02 FR 53738, Sept. 17, 2008] Vegetable, foliage of legume, group 7 ...... 0.20 Vegetable, legume, group 6 ...... 0.02 § 180.242 Thiabendazole; tolerances for Vegetable, root (except sugarbeet), subgroup 1B 0.02 Wheat, forage ...... 0.30 residues. Wheat, grain ...... 0.05 (a) General. (1) Tolerances are estab- Wheat, hay ...... 0.30 lished for residues of thiabendazole, in- Wheat, straw ...... 0.30 cluding its metabolites and degradates, 1There are no U.S. registrations on the indicated commodity. in or on the commodities in the table 2 This tolerance expires on March 21, 2017. below. Compliance with the tolerance (2) Tolerances are established for res- levels specified below is to be deter- idues of thiabendazole, including its mined by measuring only the sum of metabolites and degradates, in or on thiabendazole (2-(4- the commodities in the table below. thiazolyl)benzimidazole) and its me- Compliance with the tolerance levels tabolite benzimidazole (free and con- specified below is to be determined by jugated), calculated as the stoichio- measuring only the sum of metric equivalent of thiabendazole, in thiabendazole (2-(4- or on the commodity. thiazolyl)benzimidazole) and its metabolites 5-hydroxythiabendazole (free Commodity Parts per million and conjugated) and benzimidazole Alfalfa, forage ...... 0.02 (free and conjugated), calculated as the Alfalfa, hay ...... 0.02 stoichiometric equivalent of Apple, wet pomace ...... 12.0 thiabendazole, in or on the commodity. Avocado 1 ...... 10.0 Banana, postharvest ...... 3.0 Commodity Parts per Barley, grain ...... 0.05 million Barley, hay ...... 0.30 Barley, straw ...... 0.30 Cattle, meat ...... 0.1 Bean, dry, seed 2 ...... 0.1 Cattle, meat byproducts ...... 0.4 Brassica, head and stem, subgroup 5A ...... 0.02 Goat, meat byproducts ...... 0.4 Cantaloupe 1 ...... 15.0 Hog, meat byproducts ...... 0.3 Carrot, roots, postharvest ...... 10.0 Horse, meat byproducts ...... 0.4

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Parts per Parts per Commodity million Commodity million

Milk ...... 0.1 Sorghum, grain, forage ...... 0.25 Sheep, meat byproducts ...... 0.4 Sorghum, grain, grain ...... 0.25 Sorghum, grain, stover ...... 0.25 (b) Section 18 emergency exemptions. Time-limited tolerances specified in (b) Section 18 emergency exemptions. table 3 to this paragraph (b) are estab- [Reserved] lished for residues of the thiabendazole, (c) Tolerances with regional registra- including its metabolites and tions. [Reserved] degradates, in or on the specified agri- (d) Indirect or inadvertent residues. cultural commodities, resulting from use of the pesticide pursuant to FIFRA [Reserved] section 18 emergency exemptions. Com- [75 FR 60242, Sept. 29, 2010] pliance with the tolerance levels specified in table 3 to this paragraph (b) is § 180.245 Streptomycin; tolerances for to be determined by measuring only residues. the sum of thiabendazole (2-(4- (a) General. (1) Tolerances are estab- thiazolyl)benzimidazole) and its me- lished for residues of the fungicide tabolite benzimidazole (free and con- streptomycin in or on food commod- jugated), calculated as the stoichio- ities as follows: metric equivalent of thiabendazole. The tolerances expire on the date spec- Parts per ified in table 3 to this paragraph (b). Commodity million

Bean, dry, seed ...... 0.5 Parts per Expiration/ Commodity million revocation Bean, succulent ...... 0.5 date Fruit, pome, group 11 ...... 0.25 Sweet potato ...... 10 12/31/22 (2) Tolerances are established for res- (c) Tolerances with regional exemptions. idues of the fungicide streptomycin [Reserved] from treatment of seedling plants be- (d) Indirect or inadvertent residues. fore transplanting in or on the fol- [Reserved] lowing food commodities: [42 FR 32783, June 28, 1977] Commodity Parts per EDITORIAL NOTE: For FEDERAL REGISTER ci- million tations affecting § 180.242, see the List of CFR Celery ...... 0.25 Sections Affected, which appears in the Pepper ...... 0.25 Finding Aids section of the printed volume Tomato ...... 0.25 and at www.govinfo.gov.

§ 180.243 Propazine; tolerances for res- (3) Tolerances are established for residues. idues of the fungicide streptomycin (a) General. Tolerances are estab- from treatment of seed pieces in or on lished for residues of the herbicide the following food commodity: propazine, 2-chloro-4,6- Parts per bis(isopropylamino)-s-triazine, includ- Commodity million ing its metabolites and degradates, in or on the commodities in the following Potato ...... 0.25 table. Compliance with the tolerance levels specified in this paragraph is to (b) Section 18 emergency exemptions. be determined by measuring only the Time-limited tolerances are estab- sum of propazine, 2-chloro-4,6- lished for residues of streptomycin, in bis(isopropylamino)-s-triazine, and its or on the agricultural commodities, as two chlorinated degradates, 2-amino-4- specified in the following table, result- chloro-6-isopropylamino-s-triazine and ing from use of the pesticide pursuant 2,4-diamino-6-chloro-s-triazine, cal- to FIFRA section 18 emergency exemp- culated as the stoichiometric equiva- tions. Compliance with the tolerance lent of propazine, in or on the com- levels listed in the following table is to modity. be determined by measuring the levels

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of streptomycin only, in or on the com- Commodity Parts per modities listed in the table. The toler- million ances expire on the dates specified in Poultry, meat ...... 0.02 the table. Sheep, fat ...... 0.02 Sheep, meat byproducts ...... 0.02 Parts per Expiration Sheep, meat ...... 0.02 Commodity million date Sorghum grain, forage ...... 2.0 Sorghum, grain, grain ...... 0.1 Fruit, citrus, group 10–10 ...... 2.0 12/31/22 Sorghum, grain, stover ...... 1.0 Fruit, citrus, group 10–10, dried Soybeans, seed ...... 1.0 pulp ...... 6.0 12/31/22 Sunflower, meal ...... 3.4 Grapefruit ...... 0.15 12/31/18 Sunflower, seed ...... 2.5 Grapefruit, dried pulp ...... 0.40 12/31/18 (b) Section 18 emergency exemptions. (c) Tolerances with regional registra- [Reserved] tions. [Reserved] (c) Tolerances with regional registra- (d) Indirect or inadvertent residues. tions. [Reserved] [Reserved] (d) Indirect or inadvertent residues. [68 FR 39440, July 1, 2003, as amended at 73 Tolerances are established for indirect FR 54960, Sept. 24, 2008; 78 FR 29055, May 17, or inadvertent residues of alachlor (2- 2013; 80 FR 78145, Dec. 16, 2015; 82 FR 13764, chloro-2′,6′-diethyl-N- Mar. 15, 2017; 85 FR 5578, Jan. 31, 2020] (methoxymethyl)acetanilide) and its metabolites which can be converted to § 180.249 Alachlor; tolerances for resi- 2,6-diethylaniline (DEA) or 2-ethyl-6-(1- dues. hydroxyethyl)aniline (1-HEEA) upon (a) General. Tolerances are estab- basic hydrolysis, calculated as lished for combined residues of alachlor, in or on the following raw ag- alachlor (2-chloro-2′,6″-diethyl-N- ricultural commodities when present (methoxymethyl)acetanilide) and its therein as a result of the application of metabolites which can be converted to alachlor to the growing crops in para- 2,6-diethylaniline (DEA) or 2-ethyl-6-(1- graph (a) of this section: hydroxyethyl)aniline (1-HEEA) upon Parts per basic hydrolysis, calculated as alachlor Commodity million in or on the following raw agricultural commodities. Animal feed, nongrass, group 18, forage ...... 1.4 Animal feed, nongrass, group 18, hay ...... 1.2 Grain, cereal, forage, and straw, group 16 except Parts per Commodity million corn, sorghum, rice, straw ...... 0.8 Grain, cereal, forage, fodder and straw, group 16 Beans, dry ...... 0.1 except corn, sorghum, rice, forage ...... 0.6 Beans, succulent lima ...... 0.1 Grain, cereal, forage, fodder, and straw, group 16 Cattle, fat ...... 0.02 except for corn, sorghum, rice, hay ...... 0.8 Cattle, meat byproducts ...... 0.02 Grain, cereal, group 15 except corn, sorghum, Cattle, meat ...... 0.02 rice ...... 0.05 Corn, field, forage ...... 2.0 Corn, field, grain ...... 0.2 [72 FR 54584, Sept. 26, 2007] Corn, field, pop ...... 0.2 Corn, field, stover ...... 2.0 Corn, pop, stover ...... 2.0 § 180.252 Tetrachlorvinphos; toler- Corn, sweet (K + CWHR) ...... 0.05 ances for residues. Corn, sweet, stover ...... 2.0 Cotton, gin byproducts ...... 0.7 (a) General. Tolerances are estab- Cotton, undelinted seed ...... 0.03 lished for the combined residues of the Cowpea, forage ...... 5.0 insecticide tetrachlorvinphos [(Z)-2- Cowpea, hay ...... 5.0 chloro-1-(2,4,5-trichlorophenyl) vinyl Egg ...... 0.02 Goat, fat ...... 0.02 dimethyl phosphate], including its me- Goat, meat byproducts ...... 0.02 tabolites, 1-(2,4,5-trichlorophenyl)-eth- Goat, meat ...... 0.02 anol (free and conjugated forms), 2,4,5- Hog, fat ...... 0.02 Hog meat byproducts ...... 0.02 trichloroacetophenone, and 1-(2,4,5- Hog, meat ...... 0.02 trichlorophenyl)-ethanediol, in or on Horse, fat ...... 0.02 the following commodities: Horse, meat byproducts ...... 0.02 Horse, meat ...... 0.02 Parts per Milk ...... 0.02 Commodity million Peanut ...... 0.5 Poultry, fat ...... 0.02 Cattle, fat (of which no more than 0.1 ppm is Poultry, meat byproducts ...... 0.02 tetrachlorvinphos per se) ...... 0.2

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Parts per Expiration/ Commodity million Commodity Parts per revocation million date Cattle, kidney (of which no more than 0.05 ppm is tetrachlorvinphos per se) ...... 1.0 Bean, succulent ...... 2 None Cattle, liver (of which no more than 0.05 ppm is Beet, garden, tops ...... 6 None tetrachlorvinphos per se) ...... 0.5 Bermudagrass, forage ...... 10 None Cattle, meat (of which no more than 2.0 ppm is Bermudagrass, hay ...... 40 None tetrachlorvinphos per se) ...... 2.0 Blueberry ...... 6 None Cattle, meat byproducts, except kidney and liver 1.0 Broccoli ...... 3 None Egg (of which no more than 0.05 ppm is Brussels sprouts ...... 2 None tetrachlorvinphos per se) ...... 0.2 Cabbage ...... 5 None Hog, fat (of which no more than 0.1 ppm is Cabbage, Chinese, bok choy ...... 5 None tetrachlorvinphos per se) ...... 0.2 Cabbage, Chinese, napa ...... 5 None Hog, kidney (of which no more than 0.05 ppm is Cauliflower ...... 2 None tetrachlorvinphos per se) ...... 1.0 Celery ...... 3 None Hog, liver (of which no more than 0.05 ppm is Collards ...... 6 None tetrachlorvinphos per se) ...... 0.5 Corn, field, forage ...... 10 None Hog, meat (of which no more than 2.0 ppm is Corn, field, grain ...... 0.1 None tetrachlorvinphos per se) ...... 2.0 Corn, field, stover ...... 10 None Hog, meat byproducts, except kidney and liver .... 1.0 Corn, pop, grain ...... 0.1 None Milk, fat (reflecting negligible residues in whole Corn, pop, stover ...... 10 None milk and of which no more than 0.05 ppm is Corn, sweet, forage ...... 10 None tetrachlorvinphos per se) ...... 0.05 Corn, sweet, kernel plus cob with Poultry, fat (of which no more than 7.0 ppm is husks removed ...... 0.1 None tetrachlorvinphos per se) ...... 7.0 Corn, sweet, stover ...... 10 None Poultry, liver (of which no more than 0.05 ppm is Cotton, undelinted seed ...... 0.1 None tetrachlorvinphos per se) ...... 2.0 Dandelion, leaves ...... 6 None Poultry, meat (of which no more than 3.0 ppm is Endive ...... 5 None tetrachlorvinphos per se) ...... 3.0 Grape ...... 5 12/31/16 Poultry, meat byproducts, except liver ...... 2.0 Grapefruit ...... 2 None Hop, dried cones 1 ...... 12 None (b) Section 18 emergency exemptions. Kale ...... 6 None [Reserved] Lemon ...... 2 None Lentil, seed ...... 0.1 None (c) Tolerances with regional registra- Lettuce ...... 5 None tions. [Reserved] Mustard greens ...... 6 None (d) Indirect or inadvertent residues. Nectarine ...... 5 None Oat, forage ...... 10 None [Reserved] Oat, grain ...... 1 None [76 FR 57659, Sept. 16, 2011, as amended at 78 Oat, hay ...... 10 None FR 15882, Mar. 13, 2013; 78 FR 53684, Aug. 30, Oat, straw ...... 10 None Onion, dry bulb ...... 0.2 None 2013] Onion, green ...... 3 None Orange ...... 2 None § 180.253 Methomyl; tolerances for res- Parsley, leaves ...... 6 None idues. Pea ...... 5 None Pea, field, vines ...... 10 None (a) General. Tolerances are estab- Peach ...... 5 None lished for residues of the insecticide Peanut ...... 0.1 None methomyl, including its metabolites Pecan ...... 0.1 None Pepper, bell ...... 2 None and degradates, in or on the commod- Pepper, nonbell ...... 2 None ities in the table in this paragraph. Peppermint, tops ...... 2 None Compliance with the tolerance levels Pomegranate ...... 0.2 None specified in this paragraph is to be de- Rye, forage ...... 10 None Rye, grain ...... 1 None termined by measuring only Rye, straw ...... 10 None methomyl, methyl N-methylamino Sorghum, grain, forage ...... 1 None carbonyloxyethanimidothioate, in or Sorghum, grain, grain ...... 0.2 None Soybean, forage ...... 10 None on the commodity. Soybean, seed ...... 0.2 None Spearmint, tops ...... 2 None Expiration/ Spinach ...... 6 None Commodity Parts per revocation million date Swiss chard ...... 6 None Tangerine ...... 2 None Alfalfa, forage ...... 10 None Tomato ...... 1 None Alfalfa, hay ...... 10 None Turnip, greens ...... 6 None Apple ...... 1 None Vegetable, brassica, leafy, group 5 6.0 None Asparagus ...... 2 None Vegetable, cucurbit, group 9 ...... 0.2 None Avocado ...... 2 None Vegetable, fruiting, group 8 ...... 0.2 None Barley, grain ...... 1 None Vegetables, leafy 2 ...... 0.2 None Barley, hay ...... 10 None Vegetable, root and tuber, group 1 0.2 None Barley, straw ...... 10 None Wheat, forage ...... 10 None Bean, dry, seed ...... 0.1 None Wheat, grain ...... 1 None Bean, forage ...... 10 None Wheat, hay ...... 10 None

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Expiration/ Parts per Commodity Parts per revocation Commodity million million date Rice, grain 1 ...... 0.2 Wheat, straw ...... 10 None Sugarcane, cane 1 ...... 0.1 1 There are no U.S. registrations for use of methomyl on 1 There are no U.S. registrations for use of carbofuran on hop, dried cone, as of February 14, 1990. these commodities. 2 Except for Beet (tops), broccoli, Brussels sprouts, cabbage, cabbage, Chinese, cauliflower, celery, collards, dan- (b) Section 18 emergency exemptions. delions, endive (escarole), kale, lettuce, mustard greens, parsley, spinach, Swiss chard, turnip, greens (tops), and [Reserved] watercress. (c) Tolerances with regional registra- (b) Section 18 emergency exemptions. tions. [Reserved] [Reserved] (d) Indirect or inadvertent residues. (c) Tolerances with regional registra- [Reserved] tions. A tolerance with regional reg- [39 FR 20597, June 12, 1974] istration, as defined in § 180.1(l), is established for residues of the insecticide EDITORIAL NOTE: For FEDERAL REGISTER ci- methomyl, including its metabolites tations affecting § 180.254, see the List of CFR and degradates, in or on the com- Sections Affected, which appears in the modity in the table in this paragraph. Finding Aids section of the printed volume and at www.govinfo.gov. Compliance with the tolerance level specified in this paragraph is to be de- § 180.258 Ametryn; tolerances for resi- termined by measuring only dues. methomyl, methyl N-[ (a) General. Tolerances are estab- [(methylamino)carbonyl] lished for residues of the desiccant and oxy]ethanimidothioate, in or on the herbicide (2-ethylamino)-4- commodity. (isopropylamino)-6-(methylthio)-s-tri- Parts azine in or on the following raw agri- Commodity per mil- cultural commodities: lion

Pear ...... 4 Expiration/ Commodity Parts per Revocation million Date (d) Indirect or inadvertent residues. [Reserved] Banana ...... 0.25 6/16/10 Corn, field, forage ...... 0.1 None [65 FR 33697, May 24, 2000, as amended at 72 Corn, field, grain ...... 0.05 None FR 35666, June 29, 2007; 74 FR 46373, Sept. 9, Corn, field, stover ...... 0.05 None 2009; 75 FR 60242, Sept. 29, 2010; 76 FR 34885, Corn, pop, grain ...... 0.05 None June 15, 2011; 77 FR 59125, Sept. 26, 2012; 80 FR Corn, pop, stover ...... 0.05 None Corn, sweet, forage ...... 0.5 6/16/10 72598, Nov. 20, 2015] Corn, sweet, kernel plus cob with husks removed ...... 0.25 6/16/10 § 180.254 Carbofuran; tolerances for Corn, sweet, stover ...... 0.5 6/16/10 residues. Pineapple ...... 0.05 None (a) General. Tolerances are estab- Sugarcane, cane ...... 0.05 None lished for the combined residues of the (b) Section 18 emergency exemptions. insecticide carbofuran (2,3-dihydro-2,2- [Reserved] dimethyl-7-benzofuranyl-N- (c) Tolerances with regional registra- methylcarbamate), its carbamate me- tions. [Reserved] tabolite-2,3-dihydro-2,2-dimethyl-3-hy- (d) Indirect or inadvertent residues. droxy-7-benzofuranyl-N- [Reserved] methylcarbamate, and its phenolic metabolites 2,3-dihydro-2,2-dimethyl-7- [43 FR 29121, July 6, 1978, as amended at 48 benzofuranol, 2,3-dihydro-2,2-dimethyl- FR 13175, Mar. 30, 1983; 48 FR 21132, May 11, 3,-oxo-7-benzofuranol and 2,3-dihydro- 1983; 52 FR 33237, Sept. 2, 1987; 63 FR 57075, 2,2-dimethyl-3,7-benzofurandiol in or on Oct. 26, 1998; 73 FR 54961, Sept. 24, 2008; 74 FR 47456, Sept. 16, 2009] the following raw agricultural commodities: § 180.259 Propargite; tolerances for residues. Commodity Parts per million (a) General. Tolerances are estab- Banana 1 ...... 0.1 lished for residues of the pesticide Coffee, bean, green 1 ...... 0.1 propargite (2-(p-tert-butylphenoxy)

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cyclohexyl 2-propynyl sulfite) in or on § 180.261 Phosmet; tolerances for resi- the following food commodities. dues.

Parts per (a) General. Tolerances are estab- Commodity million lished for residues of the insecticide phosmet, N-(mercaptomethyl) phthal- Almond ...... 0.1 Almond, hulls ...... 55.0 imide S-(O,O-dimethyl Bean, dry, seed ...... 0.2 phosphorodithioate), including its me- Cattle, fat ...... 0.1 tabolites and degradates, in or on the Cattle, meat ...... 0.1 Cattle, meat byproducts ...... 0.1 commodities in the following table. Citrus, oil ...... 30.0 Compliance with the tolerance levels Corn, field, forage ...... 10.0 specified in this paragraph is to be de- Corn, field, grain ...... 0.1 Corn, field, stover ...... 10.0 termined by measuring only the sum of Corn, pop, grain ...... 0.1 phosmet, N-(mercaptomethyl) phthal- Corn, pop, stover ...... 10.0 imide S-(O,O-dimethyl Corn, sweet, forage ...... 10.0 phosphorodithioate), and its oxygen Corn, sweet, stover ...... 10.0 Cotton, undelinted seed ...... 0.1 analog, N-(mercaptomethyl) phthal- Egg ...... 0.1 imide S-(O,O-dimethyl Goat, fat ...... 0.1 phosphorothioate, calculated as the Goat, meat ...... 0.1 Goat, meat byproducts ...... 0.1 stoichiometric equivalent of phosmet, Grain, aspirated fractions ...... 0.4 in or on the commodity. Grape ...... 10.0 Grapefruit ...... 5.0 Commodity Parts per Hog, fat ...... 0.1 million Hog, meat ...... 0.1 Hog, meat byproducts ...... 0.1 Alfalfa, forage ...... 20 Hop, dried cones ...... 100.0 Alfalfa, hay ...... 40 Horse, fat ...... 0.1 Almond, hulls ...... 10 Horse, meat ...... 0.1 Apple ...... 10 Horse, meat byproducts ...... 0.1 Apricot ...... 5 Lemon ...... 5.0 Blueberry ...... 10 Milk, fat (0.08 ppm in milk) ...... 2.0 Cattle, fat ...... 0.2 Nectarine ...... 4.0 Cattle, meat ...... 0.1 Orange ...... 10.0 Cattle, meat byproducts ...... 0.1 Peanut ...... 0.1 Cherry ...... 10 Peppermint, tops ...... 50.0 Cranberry ...... 10 Poultry, fat ...... 0.1 Fruit, citrus, group 10 ...... 5 Potato ...... 0.1 Goat, fat ...... 0.1 Sheep, fat ...... 0.1 Goat, meat ...... 0.1 Sheep, meat ...... 0.1 Goat, meat byproducts ...... 0.1 Sheep, meat byproducts ...... 0.1 Grape ...... 10 Sorghum, grain, forage ...... 10.0 Hog, fat ...... 0.2 Sorghum, grain, grain ...... 5.0 Hog, meat ...... 0.04 Sorghum, grain, stover ...... 10.0 Hog, meat byproducts ...... 0.04 Spearmint, tops ...... 50.0 Horse, fat ...... 0.1 Tea, dried ...... 10.0 Horse, meat ...... 0.1 Horse, meat byproducts ...... 0.1 Walnut ...... 0.1 Kiwifruit ...... 25 Milk ...... 0.1 (b) Section 18 emergency exemptions. Nectarine ...... 5 [Reserved] Nut, tree, group 14 ...... 0.1 Pea, dry, seed ...... 0.5 (c) Tolerances with regional registra- Pea, field, hay ...... 20 tions. Tolerances with regional reg- Pea, field, vines ...... 10 istration, as defined in § 180.1(l), are es- Pea, succulent ...... 1 tablished for residues of propargite in Peach ...... 10 Pear ...... 10 or on the following raw agricultural Plum, prune, fresh ...... 5 commodities: Potato ...... 0.1 Sheep, fat ...... 0.1 Parts per Sheep, meat ...... 0.1 Commodity million Sheep, meat byproducts ...... 0.1 Sweet potato, roots ...... 12 Corn, sweet, kernel plus cob with husks removed 0.1 (b) Section 18 emergency exemptions. (d) Indirect or inadvertent residues. [Reserved] [Reserved] (c) Tolerances with regional registra- [65 FR 33710, May 24, 2000, as amended at 72 tions. Tolerances with regional reg- FR 41930, Aug. 1, 2007; 73 FR 54961, Sept. 24, istration are established for residues of 2008; 76 FR 34885, June 15, 2011] the insecticide phosmet, N-

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(mercaptomethyl) phthalimide S-(O,O- Commodity Parts per dimethyl phosphorodithioate), includ- million ing its metabolites and degradates, in Sugarcane, cane ...... 0.02 or on the commodities in the following Sweet potato, roots ...... 0.02 table. Compliance with the tolerance 1 There are no U.S. registrations as of July 23, 2009, except levels specified in this paragraph is to for existing stocks bearing old labeling whose sale, distribution, and use is allowed, provided it is consistent with the be determined by measuring only the terms of the cancellation order of July 9, 2009; i.e., the EPA sum of phosmet, N-(mercaptomethyl) will allow the technical registrant to continue to sell and dis- tribute existing stocks of the amended registered product phthalimide S-(O,O-dimethyl bearing old labeling for use on pineapple for 18 months (until phosphorodithioate), and its oxygen January 9, 2011) and persons other than the registrant may continue to sell and/or use existing stocks of product bearing analog, N-(mercaptomethyl) phthal- the old labeling until such stocks are exhausted, provided that imide S-(O,O-dimethyl such use is consistent with the terms of the previously approved labeling on, or that accompanied, the modified phosphorothioate, calculated as the product. stoichiometric equivalent of phosmet, in or on the commodity. (b) Section 18 emergency exemptions. [Reserved] Commodity Parts per (c) Tolerances with regional registra- million tions. [Reserved] Crabapple ...... 20 (d) Indirect or inadvertent residues. Pistachio ...... 0.1 [Reserved] (d) Indirect or inadvertent residues. [47 FR 53004, Nov. 24, 1982, as amended at 48 [Reserved] FR 51485, Nov. 9, 1983; 52 FR 33237, Sept. 2, 1987; 53 FR 30053, Aug. 10, 1988; 63 FR 57075, [43 FR 46538, Oct. 10, 1978, as amended at 45 Oct. 26, 1998; 64 FR 39078, July 21, 1999; 66 FR FR 8981, Feb. 11, 1980; 48 FR 37213, Aug. 17, 38955, July 26, 2001; 67 FR 49616, July 31, 2002; 1983; 52 FR 48539, Dec. 23, 1987; 53 FR 657, Jan. 73 FR 53731, Sept. 17, 2008; 73 FR 54961, Sept. 11, 1988; 53 FR 39090, Oct. 5, 1988; 63 FR 57075, 24, 2008; 74 FR 46373, Sept. 9, 2009; 75 FR 60242, Oct. 26, 1998; 67 FR 49616, July 31, 2002; 74 FR Sept. 29, 2010] 46698, Sept. 11, 2009; 75 FR 60242, Sept. 29, 2010] § 180.269 Aldicarb; tolerances for residues. § 180.262 Ethoprop; tolerances for residues. (a) General. Tolerances are established for combined residues of the in- (a) General. Tolerances are estab- secticide and nematocide aldicarb (2- lished for residues of the nematocide methyl-2-(methylthio)propionaldehyde and insecticide ethoprop, O-ethyl S,S- O-(methylcarbamoyl) oxime and its dipropyl phosphorodithioate, including cholinesterase-inhibiting metabolites its metabolites and degradates, in or 2-methyl 2-(methylsulfinyl) on the commodities in the following propionaldehyde O-(methylcarbamoyl) table. Compliance with the tolerance oxime and 2-methyl-2-(methylsulfonyl) levels specified in this paragraph is to propionaldehyde O-(methylcarbamoyl) be determined by measuring only oxime in or on the following food com- ethoprop, O-ethyl S,S-dipropyl modities: phosphorodithioate, in or on the commodity. Parts per Commodity million Parts per Commodity million Bean, dry, seed ...... 0.1 Beet, sugar, roots ...... 0.05 Banana ...... 0.02 Beet, sugar, tops ...... 1 Bean, lima ...... 0.02 Citrus, dried pulp ...... 0.6 Bean, snap, succulent ...... 0.02 Coffee, bean, green ...... 0.1 Cabbage ...... 0.02 Cotton, undelinted seed ...... 0.1 Corn, field, forage ...... 0.02 Cotton, hulls ...... 0.3 Corn, field, grain ...... 0.02 Grapefruit ...... 0.3 Corn, field, stover ...... 0.02 Lemon ...... 0.3 Corn, sweet, forage ...... 0.02 Lime ...... 0.3 Corn, sweet, kernel plus cob with husks removed 0.02 Orange, sweet ...... 0.3 Corn, sweet, stover ...... 0.02 Peanut ...... 0.05 Cucumber ...... 0.02 Pecan ...... 0.5 Hop, dried cones ...... 0.02 Potato ...... 1 Peppermint, tops ...... 0.02 Soybean ...... 0.02 1 Pineapple ...... 0.02 Sugarcane, cane ...... 0.02 Potato ...... 0.02 Sweet potato, roots ...... 0.1 Spearmint, tops ...... 0.02

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(b) Section 18 emergency exemptions. Commodity Parts per [Reserved] million (c) Tolerances with regional registra- Crayfish ...... 0.05 tions. [Reserved] Egg ...... 0.30 (d) Indirect or inadvertent residues. Goat, fat ...... 0.10 Goat, meat ...... 0.05 [Reserved] Goat, meat byproducts ...... 1.0 [65 FR 33710, May 24, 2000, as amended at 69 Hog, fat ...... 0.10 Hog, meat ...... 0.05 FR 6567, Feb. 11, 2004; 73 FR 54961, Sept. 24, Hog, meat byproducts ...... 1.0 2008; 81 FR 34905, June 1, 2016] Horse, fat ...... 0.10 Horse, meat ...... 0.05 § 180.272 Tribuphos; tolerances for res- Horse, meat byproducts ...... 1.0 idues. Milk ...... 0.05 Poultry, fat ...... 0.05 (a) General. Tolerances are estab- Poultry, meat ...... 0.10 lished for residues of the defoliant Poultry, meat byproducts ...... 0.50 Rice, bran ...... 40 tribuphos (S,S,S-tributyl Rice, grain ...... 10 phosphorotrithioate) in or on food com- Rice, hulls ...... 30 modities as follows: Sheep, fat ...... 0.10 Sheep, meat ...... 0.05 Parts per Sheep, meat byproducts ...... 1.0 Commodity million (b) Section 18 emergency exemptions. Cattle, fat ...... 0.15 Cattle, meat ...... 0.02 [Reserved] Cattle, meat byproducts ...... 0.02 (c) Tolerances with regional registra- Cotton, gin byproducts ...... 40.0 tions. [Reserved] Cotton, undelinted seed ...... 4.0 Goat, fat ...... 0.15 (d) Indirect or inadvertent residues. Goat, meat ...... 0.02 [Reserved] Goat, meat byproducts ...... 0.02 Hog, fat ...... 0.15 [63 FR 34827, June 26, 1998, as amended at 72 Hog, meat ...... 0.02 FR 28888, May 23, 2007; 80 FR 72598, Nov. 20, Hog, meat byproducts ...... 0.02 2015] Horse, fat ...... 0.15 Horse, meat ...... 0.02 Horse, meat byproducts ...... 0.02 § 180.275 Chlorothalonil; tolerances for Milk ...... 0.01 residues. Sheep, fat ...... 0.15 Sheep, meat ...... 0.02 (a) General. (1) Tolerances are estab- Sheep, meat byproducts ...... 0.02 lished for the fungicide chlorothalonil (tetrachloroisophthalonitrile) and its (b) Section 18 emergency exemptions. metabolite 4-hydroxy-2,5,6- [Reserved] trichloroisophthalonitrile in or on the (c) Tolerances with regional registra- following food commodities. tions. [Reserved] Parts per (d) Indirect or inadvertent residues. Commodity million [Reserved] Almond ...... 0.05 [65 FR 33698, May 24, 2000, as amended at 67 Almond, hulls ...... 1.0 FR 49616, July 31, 2002; 72 FR 53460, Sept. 19, Apricot ...... 0.5 2007] Asparagus ...... 0.1 Banana (NMT 0.05 ppm in edible pulp) ...... 0.5 Bean, dry, seed ...... 0.1 § 180.274 Propanil; tolerances for resi- Bean, snap, succulent ...... 5 dues. Blueberry ...... 1.0 (a) General. Tolerances are estab- Brassica, head and stem, subgroup 5A ...... 5.0 Carrot, roots ...... 1 lished for the combined residues of the Celery ...... 15 herbicide propanil (3′, 4′- Cherry, sweet ...... 0.5 dichloropropionanilide) and its me- Cherry, tart ...... 0.5 Cocoa bean, dried bean ...... 0.05 tabolites convertible to 3, 4- Coffee, bean, green ...... 0.20 dichloroaniline (3, 4-DCA) in or on the Corn, sweet, kernel plus cob with husks removed 1 following food commodities: Cranberry ...... 5.0 Ginseng ...... 4.0 Parts per Horseradish ...... 4.0 Commodity million Lentil ...... 0.10 Lychee ...... 15 Cattle, fat ...... 0.10 Mango ...... 1.0 Cattle, meat ...... 0.05 Mushroom ...... 1.0 Cattle, meat byproducts ...... 1.0 Nectarine ...... 0.5

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(d) Indirect or inadvertent residues. Commodity Parts per million [Reserved] Okra ...... 6.0 [42 FR 56114, Oct. 21, 1977] Onion, bulb ...... 0.5 Onion, green ...... 5 EDITORIAL NOTE: For FEDERAL REGISTER ci- Papaya ...... 15 tations affecting § 180.275, see the List of CFR Parsnip, roots ...... 1 Sections Affected, which appears in the Passionfruit ...... 3 Finding Aids section of the printed volume Pea, edible podded ...... 5 and at www.govinfo.gov. Peach ...... 0.5 Peanut ...... 0.3 Pistachio ...... 0.2 § 180.276 Formetanate hydrochloride; Plum ...... 0.2 tolerances for residues. Plum, prune ...... 0.2 (a) General. Tolerances are estab- Potato ...... 0.1 Rhubarb ...... 4.0 lished for residues of the insecticide Soybean ...... 0.2 formetanate hydrochloride, including Starfruit ...... 3.0 its metabolites and degradates, in or Tomato ...... 5 on the commodities in the table in this Vegetable, cucurbit, group 9 ...... 5.0 Vegetable, fruiting, group 8, except tomato ...... 6.0 paragraph. Compliance with the toler- Yam, true ...... 0.10 ance levels specified in this paragraph is to be determined by measuring only (2) Tolerances are established for the formetanate hydrochloride, N,N-di- metabolite 4-hydroxy-2,5,6- methyl-N’-[3-[(methylamino)carbonyl] trichloroisophthalonitrile in or on the oxy]phenyl]methanimidamide hydro- following food commodities. chloride, in or on the commodity.

Commodity Parts per Expiration/ million Commodity Parts per revocation million date Cattle, fat ...... 0.1 Cattle, kidney ...... 0.5 Apple ...... 0.50 12/31/13 Cattle, meat byproducts, except kidney ...... 0.05 Apple, wet pomace ...... 1.5 12/31/13 Cattle, meat ...... 0.03 Grapefruit ...... 1.5 None Goat, fat ...... 0.1 Lemon ...... 0.60 None Goat, kidney ...... 0.5 Lime ...... 0.03 None Goat, meat byproducts, except kidney ...... 0.05 Nectarine ...... 0.40 None Orange ...... 1.5 None Goat, meat ...... 0.03 Peach ...... 0.40 12/31/13 Hog, fat ...... 0.1 Pear ...... 0.50 12/31/13 Hog, kidney ...... 0.5 Tangelo ...... 0.03 None Hog, meat byproducts, except kidney ...... 0.05 Tangerine ...... 0.03 None Hog, meat ...... 0.03 Horse, fat ...... 0.1 Horse, kidney ...... 0.5 (b) Section 18 emergency exemptions. Horse, meat byproducts, except kidney ...... 0.05 [Reserved] Horse, meat ...... 0.03 (c) Tolerances with regional registra- Milk ...... 0.1 Sheep, fat ...... 0.1 tions. [Reserved] Sheep, kidney ...... 0.5 (d) Indirect or inadvertent residues. Sheep, meat byproducts, except kidney ...... 0.05 [Reserved] Sheep, meat ...... 0.03 [77 FR 40815, July 11, 2012] (b) Section 18 emergency exemptions. [Reserved] § 180.278 Phenmedipham; tolerances (c) Tolerances with regional registra- for residues. tions. Tolerances with regional reg- (a) General. Tolerances are estab- istration, as defined in § 180.1(l), are es- lished for the combined residues of the tablished for the combined residues of herbicide phenmedipham (3- chlorothalonil and its metabolite in or methoxycarbonylaminophenyl-3′- on the following raw agricultural com- methylcarbanilate) in or on the fol- modities: lowing food commodities:

Parts per Commodity Parts per Commodity million million

Hazelnut ...... 0.1 Beet, garden, roots ...... 0.2 Peppermint, tops ...... 2 Beet, garden, tops ...... 0.2 Persimmon ...... 1.5 Beet, sugar, dried pulp ...... 0.5 Spearmint, tops ...... 2 Beet, sugar, molasses ...... 0.2 Beet, sugar, roots ...... 0.1

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(d) Indirect or inadvertent residues. Commodity Parts per million [Reserved] Beet, sugar, tops ...... 0.1 [63 FR 45182, Aug. 25, 1998, as amended at 63 Spinach ...... 4.0 FR 67799, Dec. 9, 1998; 64 FR 40772, July 28, 1999; 64 FR 61791, Nov. 15, 1999; 65 FR 8874, (b) Section 18 emergency exemptions. Feb. 23, 2000; 65 FR 49941, Aug. 16, 2000; 65 FR [Reserved] 62634, Oct. 19, 2000; 66 FR 64773, Dec. 14, 2001; (c) Tolerances with regional registra- 68 FR 2247, Jan. 16, 2003; 68 FR 56195, Sept. 30, tions. [Reserved] 2003; 70 FR 7046, Feb. 10, 2005; 74 FR 46373, Sept. 9, 2009; 76 FR 34885, June 15, 2011] (d) Indirect or inadvertent residues. [Reserved] § 180.287 Amitraz; tolerances for residues. [72 FR 28888, May 23, 2007] (a) General. Tolerances are estab- § 180.284 Zinc phosphide; tolerances lished for residues of the insecticide for residues. amitraz (N’-[2,4-dimethylphenyl]-N- (a) General. Tolerances are estab- [[(2,4-dimethylphenyl)imino]methyl]]- lished for residues of the phosphine re- N-methylmethanimidamide), including its metabolites and degradates, in or sulting from the use of the rodenticide on the commodities in the following zinc phosphide in or on the raw agricul- table. Compliance with the tolerance tural commodities as follows: levels specified is to be determined by Parts per measuring amitraz residues convertible Commodity million to 2,4-dimethylaniline, expressed as the stoichiometric equivalent of amitraz, Alfalfa, forage ...... 0.2 Alfalfa, hay ...... 0.2 in or on the following raw agricultural Barley, grain ...... 0.05 commodities: Barley, hay ...... 0.2 Barley, straw ...... 0.2 Parts per Commodity million Bean, dry, seed ...... 0.05 Beet, sugar, roots ...... 0.05 Cattle, fat ...... 0.1 Beet, sugar, tops ...... 0.2 Cattle, meat ...... 0.02 Grape ...... 0.01 Cattle, meat byproducts ...... 0.2 Grass, rangeland, forage ...... 0.1 Hog, fat ...... 0.1 Grass, rangeland, hay ...... 0.1 Hog, kidney ...... 0.1 Potato ...... 0.05 Hog, liver ...... 0.1 Sugarcane, cane ...... 0.01 Hog, meat ...... 0.05 Hog, meat byproducts ...... 0.3 Timothy, hay ...... 0.5 Honey ...... 0.2 Timothy, forage ...... 0.5 Honeycomb ...... 9 Wheat, forage ...... 0.05 Milk ...... 0.03 Wheat, grain ...... 0.05 Milk, fat ...... 0.2 Wheat, hay ...... 0.05 Wheat, straw ...... 0.05 (b) Section 18 emergency exemptions. [Reserved] (b) Section 18 emergency exemptions. (c) Tolerances with regional registra- [Reserved] tions. [Reserved] (c) Tolerances with regional registra- (d) Indirect or inadvertent residues. tions. Tolerances with regional reg- [Reserved] istration, as defined in § 180.1(l), are established for residues of phosphine re- [44 FR 70145, Dec. 6, 1979, as amended at 51 sulting from the use of the rodenticide FR 16846, May 7, 1986; 52 FR 5767, Feb. 26, 1987; 57 FR 53568, Nov. 12, 1992; 58 FR 14316, zinc phosphide in or on the following Mar. 17, 1993; 60 FR 12704, Mar. 8, 1995; 67 FR raw agricultural commodities as fol- 49616, July 31, 2002; 72 FR 53454, Sept. 19, 2007; lows: 74 FR 47456, Sept. 16, 2009; 78 FR 17133, Mar. 20, 2013; 80 FR 72598, Nov. 20, 2015] Commodity Parts per million § 180.288 2-(Thiocyanomethyl- thio)benzothiazole; tolerances for Artichoke, globe ...... 0.01 Beet, sugar, roots ...... 0.04 residues. Beet, sugar, tops ...... 0.02 (a) General. Tolerances are established for residues of the fungicide 2-

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(thiocyanomethylthio)benzothiazole in (c) Tolerances with regional registra- or on the following food commodities: tions. [Reserved] (d) Indirect or inadvertent residues. Parts per Commodity million [Reserved] [63 FR 34828, June 26, 1998, as amended at 77 Barley, grain ...... 0.1(N) Barley, straw ...... 0.1(N) FR 59126, Sept. 26, 2012] Beet, sugar, roots ...... 0.1(N) Beet, sugar, tops ...... 0.1(N) § 180.291 Pentachloronitrobenzene; tol- Corn, field, forage ...... 0.1(N) erance for residues. Corn, field, grain ...... 0.1 Corn, field, stover ...... 0.1 (a) General. Tolerances are estab- Corn, pop, grain ...... 0.1 lished for the combined residues of the Corn, pop, stover ...... 0.1 fungicide pentachloronitrobenzene Cotton, forage ...... 0.1(N) (PCNB) and its metabolites Cotton, undelinted seed ...... 0.1(N) Oat, forage ...... 0.1(N) pentachloroaniline (PCA), and Oat, grain ...... 0.1(N) pentachlorothioanisole (PCTA), in or Oat, hay ...... 0.1(N) on the following food commodities: Oat, straw ...... 0.1(N) Rice, grain ...... 0.1(N) Commodity Parts per Safflower, seed ...... 0.1(N) million Sorghum, grain, forage ...... 0.1(N) Sorghum, grain, grain ...... 0.1(N) Bean ...... 0.1 Sorghum, grain, stover ...... 0.1(N) Brassica, head and stem, subgroup 5A ...... 0.1 Wheat, forage ...... 0.1(N) Cotton, undelinted seed ...... 0.1 Wheat, grain ...... 0.1(N) Garlic, bulb ...... 0.1 Wheat, hay ...... 0.1(N) Peanut ...... 1.0 Wheat, straw ...... 0.1(N) Potato ...... 0.1 Soybean, forage ...... 0.02 Soybean, hay ...... 0.02 (b) Section 18 emergency exemptions. Soybean, seed ...... 0.02 [Reserved] Vegetable, fruiting, group 8 ...... 0.1 (c) Tolerances with regional registrations. [Reserved] (b) Section 18 emergency exemptions. (d) Indirect or inadvertent residues. [Reserved] [Reserved] (c) Tolerances with regional registrations. Tolerances with regional reg- [68 FR 39440, July 1, 2003, as amended at 74 istrations, as defined in § 180.1(l), are FR 46374, Sept. 9, 2009; 80 FR 72598, Nov. 20, established for the combined residues 2015] of the fungicide § 180.289 Methanearsonic acid; toler- pentachloronitrobenzene (PCNB) and ances for residues. its metabolites pentachloroaniline (PCA), and pentachlorothioanisole (a) General. Tolerances are estab- (PCTA), in or on the following food lished for residues of the herbicide commodities: methanearsonic acid, including its metabolites and degradates, in or on the Commodity Parts per commodities in the table in this para- million graph. Compliance with the tolerance Collards ...... 0.2 levels specified in this paragraph is to Kale ...... 0.2 be determined by measuring only Mustard, greens ...... 0.2 methanearsonic acid, from application (d) Indirect or inadvertent residues. of the disodium and monosodium salts [Reserved] of methanearsonic acid, calculated as the stoichiometric equivalent of As2O3, [74 FR 47456, Sept. 16, 2009] in or on the commodity. § 180.292 Picloram; tolerances for resi- Expiration/ dues. Commodity Parts per Revocation million Date (a) General. Tolerances are established for residues of the herbicide Cotton, undelinted seed ...... 0.7 None Cotton, hulls ...... 0.9 None picloram, 4-amino-3,5,6- Fruit, citrus ...... 0.35 12/31/12 trichloropicolinic acid, including its metabolites and degradates, in or on (b) Section 18 emergency exemptions. the commodities in the following table [Reserved] from its application in the acid form or

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in the form of its salts. Compliance dicarboxylic acid) and its mono-methyl with the tolerance levels specified in ester. this paragraph is to be determined by Parts per measuring only picloram, 4-amino- Commodity million 3,5,6-trichloropicolinic acid, in or on the commodity. Apple ...... 0.05 Apple, wet pomace ...... 0.15 Parts per Cotton, undelinted seed ...... 0.1 Commodity million Fish ...... 0.1 Hop, dried cones ...... 0.1 Barley, grain ...... 0.5 Potato ...... 0.1 Barley, pearled barley ...... 3.0 Rice, grain ...... 0.05 Barley, straw ...... 1.0 Cattle, fat ...... 0.4 (2) An interim tolerance of 0.2 parts Cattle, meat ...... 0.4 Cattle, meat byproducts ...... 15 per million is established for residues Egg ...... 0.05 of the herbicide endothall (7 - Goat, fat ...... 0.4 oxabicyclo[2.2.1] heptane-2,3- Goat, meat ...... 0.4 Goat, meat byproducts ...... 15 dicarboxylic acid) in water, potable Grain, aspirated fractions ...... 4.0 from use of its potassium, sodium, di- Grass, forage ...... 400 N, N-dimethylalkylamine, and mono-N- Grass, hay ...... 225 Hog, fat ...... 0.05 N,-dimethylalkylamine salts as Hog, meat ...... 0.05 algicides or herbicides to control Hog, meat byproducts ...... 0.05 aquatic plants in canals, lakes, ponds, Horse, fat ...... 0.4 Horse, meat ...... 0.4 and other potential sources of water, Horse, meat byproducts ...... 15 potable. Milk ...... 0.25 (b) Section 18 emergency exemptions. Oat, forage ...... 1.0 Oat, grain ...... 0.5 [Reserved] Oat, groats/rolled oats ...... 3.0 (c) Tolerances with regional registra- Oat, straw ...... 1.0 tions. [Reserved] Poultry, fat ...... 0.05 (d) Indirect or inadvertent residues. Poultry, meat ...... 0.05 Poultry, meat byproducts ...... 0.05 Tolerances are established for the indi- Sheep, fat ...... 0.4 rect or inadvertent combined residues Sheep, meat ...... 0.4 of the herbicide, endothall (7 - Sheep, meat byproducts ...... 15 Wheat, bran ...... 3.0 oxabicyclo[2.2.1] heptane-2,3- Wheat, forage ...... 1.0 dicarboxylic acid) in potable water Wheat, germ ...... 3.0 from use of its potassium, sodium, di- Wheat, grain ...... 0.5 Wheat, middlings ...... 3.0 N, N -dimethylalkylamine, and mono- Wheat, shorts ...... 3.0 N-N, -dimethylalkylamine salts as Wheat, straw ...... 1.0 algicides or herbicides to control aquatic plants in canals, lakes, ponds, (b) Section 18 emergency exemptions. and other potable water sources that [Reserved] may lead to endothall residues in or on (c) Tolerances with regional registra- the following commodities: tions. [Reserved] (d) Indirect or inadvertent residues. Commodity Parts per [Reserved] million [41 FR 19221, May 11, 1976, as amended at 47 Almond, hulls ...... 15.0 Animal feed, nongrass, group 18, forage ...... 4.0 FR 53005, Nov. 24, 1982; 64 FR 425, Jan. 5, 1999; Animal feed, nongrass, group 18, hay ...... 10 64 FR 39082, July 21, 1999; 72 FR 41930, Aug. 1, Apple, wet pomace ...... 0.15 2007; 75 FR 60243, Sept. 29, 2010] Beet, sugar, molasses ...... 1.5 Brassica, head and stem subgroup 5A ...... 0.1 § 180.293 Endothall; tolerances for res- Brassica, leafy, subgroup 5B ...... 2.0 idues. Bushberry subgroup 13-07B ...... 0.6 Caneberry subgroup 13-07A ...... 0.6 (a) General. (1) Tolerances are estab- Cattle, fat ...... 0.05 lished for the residues of endothall, in- Cattle, kidney ...... 0.05 Cattle, kidney 1 ...... 0.20 cluding its metabolites and degradates, Cattle, liver 1 ...... 0.10 in or on the commodities in the table, Cattle, liver ...... 0.05 below. Compliance with the tolerance Cattle, meat ...... 0.05 levels specified, below, is to be deter- Corn, field, grain ...... 0.07 Corn, pop, grain ...... 0.07 mined by measuring only endothall (7- Corn, sweet, kernel plus cob with husks removed 0.3 oxabicylco [2.2.1] heptanes-2,3- Citrus, dried pulp ...... 0.1

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Commodity Parts per § 180.297 N-1-Naphthyl phthalamic million acid; tolerances for residues. Egg ...... 0.05 (a) General. Tolerances are estab- Feed commodities not otherwise listed ...... 10.0 lished for residues of the herbicide N-1- Food commodities not otherwise listed ...... 5.0 naphthyl phthalamic acid from appli- Fruit, citrus group 10 ...... 0.05 Fruit, pome, group 11 ...... 0.05 cation of its sodium salt in or on the Fruit, stone, group 12 ...... 0.3 following raw agricultural commod- Goat, fat ...... 0.05 ities: Goat, kidney 1 ...... 0.15 Goat, kidney ...... 0.05 Commodity Parts per Goat, liver ...... 0.05 million Goat, meat ...... 0.05 Grain, aspirated fractions ...... 35.0 Cantaloupe ...... 0.1(N) Cucumber ...... 0.1(N) Grain cereal, forage, fodder and straw, group 16 10.0 Muskmelon ...... 0.1(N) Grain, cereal, group 15, except corn ...... 4.0 Watermelon ...... 0.1(N) Grape ...... 1.0 Grape, raisin ...... 5.0 Grass, forage, fodder, and hay group 17, forage 3.5 (b) Section 18 emergency exemptions. Grass, forage, fodder, and hay group 17, hay ...... 18.0 [Reserved] Herb and spice, group 19 ...... 5.0 (c) Tolerances with regional registra- Hog, fat ...... 0.05 tions. [Reserved] Hog, kidney 1 ...... 0.10 (d) Indirect or inadvertent residues. Hog, kidney ...... 0.05 Hog, liver ...... 0.05 [Reserved] Hog, meat ...... 0.05 [45 FR 32306, May 16, 1980, as amended at 63 1 Milk ...... 0.03 FR 57075, Oct. 26, 1998] Milk ...... 0.01 Nut, tree, group 14 ...... 0.05 Okra ...... 0.05 § 180.298 Methidathion; tolerances for Pea and bean, dried shelled, subgroup 6C ...... 0.2 residues. Pea and bean, succulent shelled, subgroup 6B ... 2.0 (a) General. Tolerances are estab- Peppermint, tops ...... 5.0 lished for residues of the insecticide Pistachio ...... 0.05 Poultry, fat ...... 0.05 methidathion, including its metabo- Poultry, liver ...... 0.05 lites and degradates, in or on the com- Poultry, meat ...... 0.05 modities in the table in this paragraph. Poultry, meat byproducts 1 ...... 0.20 Compliance with the tolerance levels Poultry, meat byproducts ...... 0.05 specified in this paragraph is to be de- Rice, hulls ...... 8.0 Sheep, fat ...... 0.05 termined by measuring only Sheep, kidney 1 ...... 0.15 methidathion, S-[(5-methoxy-2-oxo- Sheep, kidney ...... 0.05 1,3,4-thiadiazol-3(2H)-yl)methyl] O,O- Sheep, liver ...... 0.05 dimethyl phosphorodithioate, in or on Sheep, meat ...... 0.05 the commodity. Soybean, hulls ...... 0.5 Soybean, seed ...... 0.2 Expiration/ Spearmint, tops ...... 5.0 Parts per Commodity million revocation Tomato, paste ...... 0.1 date Tomato, puree ...... 0.1 Vegetable, bulb, group 3-07 ...... 0.5 Almond, hulls ...... 6.0 12/31/16 Vegetable, cucurbit, group 9 ...... 1.5 Artichoke, globe ...... 0.05 12/31/16 Vegetable, foliage of legume, group 7 ...... 4.0 Citrus, oil ...... 420.0 12/31/16 Cotton, undelinted seed ...... 0.2 12/31/16 Vegetable, fruiting, group 8 ...... 0.05 Fruit, citrus, group 10, except tan- Vegetable, leafy, except brassica, group 4 ...... 2.0 gerine ...... 4.0 12/31/16 Vegetable, leaves of root and tuber, group 2 ...... 3.0 Fruit, pome, group 11 ...... 0.05 12/31/16 Vegetable, legume, edible, podded, subgroup 6A 2.0 Fruit, stone, group 12 ...... 0.05 12/31/16 Vegetable, root and tuber, group 1 ...... 1.0 Mango ...... 0.05 12/31/16 Wheat, milled byproducts ...... 5.0 Nut, tree, group 14 ...... 0.05 12/31/16 Olive ...... 0.05 12/31/16 1This tolerance expires on May 22, 2017. Safflower, seed ...... 0.5 12/31/16 Sorghum, forage, forage ...... 2.0 12/31/16 [41 FR 23717, June 11, 1976, as amended at 51 Sorghum, grain, forage ...... 2.0 12/31/16 FR 4498, Feb. 5, 1986; 62 FR 49931, Sept. 24, Sorghum, grain, grain ...... 0.2 12/31/16 1997; 63 FR 42249, Aug. 7, 1998; 67 FR 35048, Sorghum, grain, stover ...... 2.0 12/31/16 May 17, 2002; 71 FR 47106, Aug. 16, 2006; 71 FR Sunflower, seed ...... 0.5 12/31/16 74816, Dec. 13, 2006; 72 FR 52018, Sept. 12, 2007; Tangerine ...... 6.0 12/31/16 74 FR 67097, Dec. 18, 2009; 78 FR 76566, Dec. 18, 2013; 80 FR 72598, Nov. 20, 2015; 81 FR 83169, (b) Section 18 emergency exemptions. Nov. 21, 2016] [Reserved]

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(c) Tolerances with regional registra- phonic acid] in or on food commodities tions. Tolerances with regional reg- as follows: istration, as defined in § 180.1(l), are es- Parts per tablished for residues of the insecticide Commodity million methidathion, including its metabolites and degradates, in or on the com- Apple ...... 5.0 modities in the table in this paragraph. Apple, juice ...... 10.0 Barley, bran ...... 5.0 Compliance with the tolerance levels Barley, grain ...... 2.0 specified in this paragraph is to be de- Barley, straw ...... 10.0 termined by measuring only Blackberry ...... 30.0 methidathion, S-[(5-methoxy-2-oxo- Blueberry ...... 20.0 1,3,4-thiadiazol-3(2H)-yl)methyl] O,O- Cantaloupe ...... 2.0 Cattle, fat ...... 0.02 dimethyl phosphorodithioate, in or on Cattle, kidney ...... 1.0 the commodity. Cattle, meat ...... 0.02 Cattle, meat byproducts, except kidney ...... 0.2 Expiration/ Cherry ...... 10.0 Commodity Parts per revocation million date Coffee, bean, green ...... 0.5 Cotton, gin byproducts ...... 180.0 Kiwifruit ...... 0.1 12/31/16 Cotton, undelinted seed ...... 6.0 Longan ...... 0.1 12/31/16 Egg ...... 0.002 Starfruit ...... 0.1 12/31/16 Goat, fat ...... 0.02 Sugar apple ...... 0.2 12/31/16 Goat, kidney ...... 1.0 Goat, meat ...... 0.02 Goat, meat byproducts, except kidney ...... 0.2 (d) Indirect or inadvertent residues. Grape ...... 2.0 [Reserved] Grape, raisin ...... 12.0 Hazelnut ...... 0.80 [43 FR 44845, Sept. 29, 1978] Hog, fat ...... 0.02 EDITORIAL NOTE: For FEDERAL REGISTER ci- Hog, kidney ...... 1.0 tations affecting § 180.298, see the List of CFR Hog, meat ...... 0.02 Sections Affected, which appears in the Hog, meat byproducts, except kidney ...... 0.2 Finding Aids section of the printed volume Horse, fat ...... 0.02 Horse, kidney ...... 1.0 and at www.govinfo.gov. Horse, meat ...... 0.02 Horse, meat byproducts, except kidney ...... 0.2 § 180.299 Dicrotophos; tolerances for Milk ...... 0.01 residues. Nut, macadamia ...... 0.5 (a) General. Tolerances are estab- Pepper ...... 30.0 Pineapple ...... 2.0 lished for residues of the insecticide Poultry, fat ...... 0.02 dicrotophos, dimethyl phosphate of 3- Poultry, liver ...... 0.05 hydroxy-N,N-dimethyl-cis- Poultry, meat ...... 0.01 crotonamide, in or on the following Poultry, meat byproducts, except liver ...... 0.01 food commodities: Sheep, fat ...... 0.02 Sheep, kidney ...... 1.0 Sheep, meat ...... 0.02 Parts per Commodity million Sheep, meat byproducts, except kidney ...... 0.2 Sugarcane, molasses ...... 1.5 Cotton, gin byproducts ...... 2.0 Tomato ...... 2.0 Cotton, undelinted seed ...... 0.2 Walnut ...... 0.5 Wheat, bran ...... 5.0 Wheat, germ ...... 5.0 (b) Section 18 emergency exemptions. Wheat, grain ...... 2.0 [Reserved] Wheat, middlings ...... 5.0 (c) Tolerances with regional registra- Wheat, shorts ...... 5.0 tions. [Reserved] Wheat, straw ...... 10.0 (d) Indirect or inadvertent residues. [Reserved] (b) Section 18 emergency exemptions. [Reserved] [73 FR 52613, Sept. 10, 2008] (c) Tolerances with regional registrations. A tolerance with regional reg- § 180.300 Ethephon; tolerances for resi- istration, as defined in § 180.1(m), of 0.1 dues. part per million is established for resi- (a) General. Tolerances are estab- dues of the plant regulator ethephon lished for residues of the plant regu- [(2-chloroethyl)phosphonic acid] in or lator ethephon [(2-chloroethyl) phos- on the food commodity sugarcane.

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(d) Indirect or inadvertent residues. (d) Indirect or inadvertent residues. [Reserved] [Reserved] [65 FR 33710, May 24, 2000, as amended at 72 [47 FR 55222, Dec. 8, 1982, as amended at 50 FR 53455, Sept. 19, 2007; 75 FR 56015, Sept. 15, FR 81, Jan. 2, 1985; 62 FR 4915, Feb. 3, 1997; 63 2010; 80 FR 72598, Nov. 20, 2015] FR 4586, Jan. 30, 1998; 64 FR 11801, Mar. 10, 1999; 66 FR 9773, Feb. 12, 2001; 66 FR 64773, § 180.301 Carboxin; tolerances for resi- Dec. 14, 2001; 67 FR 40218, June 12, 2002; 67 FR dues. 72853, Dec. 9, 2002; 71 FR 56383, Sept. 27, 2006; (a) General. Tolerances are estab- 80 FR 72598, Nov. 20, 2015] lished for the combined residues of the § 180.303 Oxamyl; tolerances for resi- fungicide carboxin (5,6-dihydro-2-meth- dues. yl-1,4-oxathiin-3-carboxanilide) and its (a) General. Tolerances are estab- metabolites determined as aniline and lished for the combined residues of the expressed as parent compound, in or on insecticide oxamyl, methyl N,N-di- food commodities as follows: methyl-N-[(methylcarbamoyl)-oxy]-1- thiooxamimidate, and its oxime me- Commodity Parts per million tabolite methyl N,N-dimethyl-N-hy- Barley, grain ...... 0.2 droxy-1-thiooxamimidate calculated as Barley, straw ...... 0.2 oxamyl in or on the following food Bean, dry, seed ...... 0.2 commodities: Bean, succulent ...... 0.2 Canola, seed ...... 0.03 Parts per Cattle, fat ...... 0.05 Commodity million Cattle, meat byproducts ...... 0.1 Cattle, meat ...... 0.05 Apple ...... 2 Corn, field, forage ...... 0.2 Banana ...... 0.3 Corn, field, grain ...... 0.2 Cantaloupe ...... 2.0 Corn, field, stover ...... 0.2 Carrot ...... 0.1 Corn, pop, grain ...... 0.2 Celery ...... 10.0 Corn, pop, stover ...... 0.2 Cotton, undelinted seed ...... 0.2 Corn, sweet, forage ...... 0.2 Cucumber ...... 2.0 Corn, sweet, kernel plus cob with husks removed 0.2 Eggplant ...... 2.0 Corn, sweet, stover ...... 0.2 Fruit, citrus, group 10 ...... 3 Cotton, undelinted seed ...... 0.2 Garlic, bulb ...... 0.2 Egg ...... 0.05 Melon, honeydew ...... 2.0 Goat, fat ...... 0.05 Onion, bulb ...... 0.2 Goat, meat byproducts ...... 0.1 Peanut ...... 0.05 Goat, meat ...... 0.05 Peanut, hay ...... 2.0 Hog, fat ...... 0.05 Pear ...... 2.0 Hog, meat byproducts ...... 0.1 Peppermint, tops ...... 10.0 Hog, meat ...... 0.05 Pepper, bell ...... 2.0 Horse, fat ...... 0.05 Pepper, nonbell ...... 5.0 Horse, meat byproducts ...... 0.1 Pineapple ...... 1 Horse, meat ...... 0.05 Pineapple, process residue ...... 2.0 Milk ...... 0.05 Pumpkin ...... 2.0 Oat, forage ...... 0.5 Spearmint, tops ...... 10.0 Oat, grain ...... 0.2 Squash, summer ...... 2.0 Oat, straw ...... 0.2 Squash, winter ...... 2.0 Onion, bulb ...... 0.2 Tomato ...... 2 Peanut ...... 0.2 Vegetable, tuberous and corm, subgroup 1C ...... 0.1 Peanut, hay ...... 0.2 Watermelon ...... 2.0 Poultry, fat ...... 0.1 Poultry, meat byproducts ...... 0.1 (b) Section 18 emergency exemptions. Poultry, meat ...... 0.1 Rice, grain ...... 0.2 [Reserved] Safflower, seed ...... 0.2 (c) Tolerances with regional registra- Sheep, fat ...... 0.05 tions. [Reserved] Sheep, meat byproducts ...... 0.1 Sheep, meat ...... 0.05 (d) Indirect or inadvertent residues. Soybean, seed ...... 0.2 [Reserved] Wheat, forage ...... 0.5 Wheat, grain ...... 0.2 [73 FR 54961, Sept. 24, 2008, as amended at Wheat, straw ...... 0.2 72598, Nov. 20, 2015]

(b) Section 18 emergency exemptions. § 180.304 Oryzalin; tolerances for resi- [Reserved] dues. (c) Tolerances with regional registra- (a) General. Tolerances are estab- tions. [Reserved] lished for residues of the herbicide

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oryzalin, 3,5-dinitro-N4,N4- diisopropylthiocarbamate) and its me- dipropylsulfanilamide, in or on the fol- tabolite 2, 3, 3-trichloroprop-2- lowing raw agricultural commodities: enesulfonic acid (TCPSA) in or on the following food commodities: Parts per Commodity million Parts per Commodity million Almond, hulls ...... 0.05 Avocado ...... 0.05 Barley, grain ...... 0.05 Berry group 13 ...... 0.05 Barley, hay ...... 1.0 Cranberry ...... 0.05 Barley, straw ...... 0.3 Fig ...... 0.05 Beet, sugar, dried pulp ...... 0.2 Fruit, citrus, group 10 ...... 0.05 Beet, sugar, roots ...... 0.1 Fruit, pome, group 11 ...... 0.05 Beet, sugar, tops ...... 0.5 Fruit, stone, group 12 ...... 0.05 Pea, dry ...... 0.2 Grape ...... 0.05 Kiwifruit ...... 0.05 Pea, field, hay ...... 1.0 Nut, tree, group 14 ...... 0.05 Pea, field, vines ...... 0.5 Olive ...... 0.05 Pea, succulent ...... 0.2 Pistachio ...... 0.05 Wheat, forage ...... 0.5 Pomegranate ...... 0.05 Wheat, grain ...... 0.05 Strawberry ...... 0.05 Wheat, hay ...... 1.0 Wheat, straw ...... 1.0 (b) Section 18 emergency exemptions. [Reserved] (d) Indirect or inadvertent residues. (c) Tolerances with regional registra- [Reserved] tions. Tolerances with regional reg- [72 FR 28888, May 23, 2007, as amended at 73 istration, as defined in § 180.1(l), are es- FR 5109, Jan. 29, 2008; 73 FR 53738, Sept. 17, tablished for residues of oryzalin, 3,5- 2008; 74 FR 29963, June 24, 2009] dinitro-N4,N4-dipropylsulfanilamide, in or on the following raw agricultural § 180.316 Pyrazon; tolerances for resi- commodities: dues. (a) General. Tolerances are estab- Parts per lished for combined residues of the her- Commodity million bicide pyrazon (5-amino-4-chloro-2- Guava ...... 0.05 phenyl-3(2H)-pyridazinone) and its me- Papaya ...... 0.05 tabolites (calculated as pyrazon) in or on the following food commodities: (d) Indirect or inadvertent residues. [Reserved] Parts per Commodity million [71 FR 54434, Sept. 15, 2006, as amended at 76 FR 34885, June 15, 2011] Beet, garden, roots ...... 0.9 Beet, garden, tops ...... 7.0 § 180.314 Triallate; tolerances for resi- Beet, sugar, molasses ...... 1.5 dues. Beet, sugar, roots ...... 0.2 Beet, sugar, tops ...... 3.0 (a) General. Tolerances are estab- Cattle, fat ...... 0.10 lished for residues of triallate, S-2,3,4- Cattle, liver ...... 0.15 Cattle, meat ...... 0.10 trichloroallyl Cattle, meat byproducts, except liver ...... 0.10 diisopropylthiocarbamate and its me- Goat, fat ...... 0.10 tabolite 2,3,3-trichloroprop-2- Goat, liver ...... 0.15 enesulfonic acid (TCPSA) in or on the Goat, meat ...... 0.10 Goat, meat byproducts, except liver ...... 0.10 following food commodity: Horse, fat ...... 0.10 Horse, liver ...... 0.15 Parts per Commodity million Horse, meat ...... 0.10 Horse, meat byproducts, except liver ...... 0.10 Bermudagrass, hay ...... 0.3 Milk ...... 0.02 Sheep, fat ...... 0.10 Sheep, liver ...... 0.15 (b) Section 18 emergency exemptions. Sheep, meat ...... 0.10 [Reserved] Sheep, meat byproducts, except liver ...... 0.10 (c) Tolerances with regional registrations. Tolerances with a regional reg- (b) Section 18 emergency exemptions. istration, as defined in 180.1(l),are es- [Reserved] tablished for residues of the herbicide (c) Tolerances with regional registra- (S-2, 3, 4-trichloroallyl tions. [Reserved]

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(d) Indirect or inadvertent residues. Commodity Parts per Tolerances are established for com- million bined residues of the herbicide pyrazon, Horse, kidney ...... 0.4 5-amino-4-chloro-2-phenyl-3(2H)- Horse, liver ...... 0.4 pyridazinone, and its metabolites (cal- Horse, meat ...... 0.02 culated as pyrazon), in or on the fol- Horse, meat byproducts, except kidney and liver 0.02 Lettuce, head ...... 1.0 lowing food commodities: Lettuce, leaf ...... 1.0 Milk ...... 0.02 Parts per Commodity million Pear ...... 0.1 Poultry, fat ...... 0.02 Corn, field, forage ...... 0.5 Poultry, liver ...... 0.2 Corn, field, stover ...... 0.5 Poultry, meat ...... 0.02 Soybean, forage ...... 0.5 Poultry, meat byproducts, except liver ...... 0.02 Soybean, hay ...... 0.5 Radicchio ...... 2.0 Wheat, forage ...... 0.3 Raspberry ...... 0.05 Wheat, hay ...... 0.2 Sheep, fat ...... 0.2 Wheat, straw ...... 0.1 Sheep, kidney ...... 0.4 Sheep, liver ...... 0.4 [68 FR 39441, July 1, 2003, as amended at 73 Sheep, meat ...... 0.02 Sheep, meat byproducts, except kidney and liver 0.02 FR 52614, Sept. 10, 2008]

§ 180.317 Propyzamide; tolerances for (b) Section 18 emergency exemptions. residues. The time-limited tolerance specified in the table in this paragraph (b) is estab- (a) General. Tolerances are established for residues of the herbicide lished for residues of the herbicide propyzamide, including its metabolites propyzamide, including its metabolites and degradates, in or on the specified and degradates, in or on the commod- agricultural commodity in the table in ities in the table in this paragraph. this paragraph (b), resulting from use Compliance with the tolerance levels of the pesticide pursuant to FIFRA sec- specified in this paragraph is to be de- tion 18 emergency exemptions. Compli- termined by measuring only those ance with the tolerance level specified propyzamide residues convertible to in the table in this paragraph (b) is to methyl 3,5-dichlorobenzoate, expressed be determined by measuring only those as the stoichiometric equivalent of propyzamide residues convertible to propyzamide, 3,5-dichloro-N-(1,1-dimethyl 3,5-dichlorobenzoate, expressed methyl-2-propynyl)benzamide, in or on as the stoichiometric equivalent of the commodity. propyzamide, 3,5-dichloro-N-(1,1-di- Parts per methyl-2-propynyl)benzamide in or on Commodity million the commodity. The time-limited tol- Alfalfa, seed ...... 10.0 erance expires on the date specified in Animal feed, nongrass, group 18 ...... 10.0 the table in this paragraph (b). Apple ...... 0.1 Artichoke, globe ...... 0.01 Parts per Expiration/ Blackberry ...... 0.05 Commodity million revocation Blueberry ...... 0.05 date Boysenberry ...... 0.05 Cattle, fat ...... 0.2 Cranberry ...... 1 December Cattle, kidney ...... 0.4 31, 2022 Cattle, liver ...... 0.4 Cattle, meat ...... 0.02 (c) Tolerances with regional registra- Cattle, meat byproducts, except kidney and liver 0.02 Egg ...... 0.02 tions. Tolerances with regional reg- Endive ...... 1.0 istration, as defined in § 180.1(l), are es- Fruit, stone, group 12 ...... 0.1 tablished for residues of the herbicide Goat, fat ...... 0.2 propyzamide, including its metabolites Goat, kidney ...... 0.4 Goat, liver ...... 0.4 and degradates, in or on the commod- Goat, meat ...... 0.02 ities in the table in this paragraph. Goat, meat byproducts, except kidney and liver ... 0.02 Compliance with the tolerance levels Grape ...... 0.1 Hog, fat ...... 0.2 specified in this paragraph is to be de- Hog, kidney ...... 0.4 termined by measuring only those Hog, liver ...... 0.4 propyzamide residues convertible to Hog, meat ...... 0.02 Hog, meat byproducts, except kidney and liver .... 0.02 methyl 3,5-dichlorobenzoate, expressed Horse, fat ...... 0.2 as the stoichiometric equivalent of

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propyzamide, 3,5-dichloro-N-(1,1-dichlorophenoxy) butyric acid in or on methyl-2-propynyl)benzamide, in or on the following food commodity: the commodity. Commodity Parts per Parts per million Commodity million Pea ...... 0.1(N) Pea, field, seed ...... 0.05 Rhubarb ...... 0.1 (2) Tolerances are established for the combined residues, free and con- (d) Indirect or inadvertent residues. jugated, of the herbicide MCPB, 4-(4- Tolerances are established for indirect or inadvertent residues of the herbicide chloro-2-methylphenoxy)butanoic acid, propyzamide, including its metabolites and its metabolite MCPA, (4-chloro-2- and degradates, in or on the commod- methylphenoxy)acetic acid, in or on ities in the table in this paragraph. the following food commodities: Compliance with the tolerance levels Parts per specified in this paragraph is to be de- Commodity million termined by measuring only those Peppermint, tops ...... 0.20 propyzamide residues convertible to Spearmint, tops ...... 0.20 methyl 3,5-dichlorobenzoate, expressed as the stoichiometric equivalent of (b) Section 18 emergency exemptions. propyzamide, 3,5-dichloro-N-(1,1-di- [Reserved] methyl-2-propynyl)benzamide, in or on (c) Tolerances with regional registra- the commodity. tions. [Reserved] (d) Indirect or inadvertent residues. Commodity Parts per million [Reserved] Grain, cereal, forage, group 16 ...... 0.6 [68 FR 39441, July 1, 2003, as amended at 73 Grain, cereal, hay, group 16 ...... 0.2 Grain, cereal, straw, group 16 ...... 0.3 FR 66785, Nov. 12, 2008] § 180.319 Interim tolerances. [72 FR 52018, Sept. 12, 2007, as amended at 76 FR 23493, Apr. 27, 2011; 81 FR 1531, Jan. 13, (a) General. While petitions for toler- 2016; 84 FR 60943, Nov. 12, 2019] ances for negligible residues are pending and until action is completed on § 180.318 4-(2-Methyl-4-chlorophenoxy) these petitions, interim tolerances are butyric acid; tolerance for residues. established for residues of the listed (a) General. (1) A tolerance is estab- pesticide chemicals in or on the fol- lished for the herbicide 4-(2-methyl-4- lowing raw agricultural commodities:

Raw Expiration/ Substances Uses Tolerance in parts per million agricultural revocation commodity date

Endothall (7-oxabicyclo- Herbicide ...... 0.2 ...... Beet, sugar ...... None (2,2,1)heptane 2,3-dicarboxylic acid. Methyl parathion ...... Herbicide ...... 0.5 ...... Rye ...... 12/31/13

(b) Section 18 emergency exemptions. § 180.324 Bromoxynil; tolerances for [Reserved] residues. (c) Tolerances with regional registra- (a) General. (1) Tolerances are estab- tions. [Reserved] lished for residues of the herbicide (d) Indirect or inadvertent residues. bromoxynil, including its metabolites [Reserved] and degradates, in or on the commod- [77 FR 59126, Sept. 26, 2012, as amended at 79 ities in the table below. Compliance FR 27502, May 14, 2014] with the tolerance levels is to be determined by measuring only bromoxynil, 3,5-dibromo-4-hydroxybenzonitrile, resulting from application of its octanoic

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and/or heptanoic acid ester, in or on Commodity Parts per the commodities. million Poultry, meat byproducts ...... 0.3 Parts per Commodity million Poultry, meat ...... 0.05 Sheep, fat ...... 1 Alfalfa, forage ...... 0.1 Sheep, meat byproducts ...... 3.5 Alfalfa, hay ...... 0.5 Sheep, meat ...... 0.5 Barley, grain ...... 0.05 Barley, hay ...... 9.0 Barley, straw ...... 4.0 (b) Section 18 emergency exemptions. Corn, field, forage ...... 0.3 [Reserved] Corn, field, grain ...... 0.05 Corn, field, stover ...... 0.2 (c) Tolerances with regional registra- Corn, pop, grain ...... 0.05 tions. [Reserved] Corn, pop, stover ...... 0.2 (d) Indirect or inadvertent residues. Flax, seed ...... 0.1 Garlic ...... 0.1 [Reserved] Grain, aspirated fractions ...... 1.2 Grass, forage ...... 18 [62 FR 33023, June 18, 1997, as amended at 63 Grass, hay ...... 5.0 FR 26480, May 13, 1998; 66 FR 47402, Sept. 12, Oat, forage ...... 0.3 2001; 70 FR 7046, Feb. 10, 2005; 72 FR 35666, Oat, grain ...... 0.05 June 29, 2007; 72 FR 41930, Aug. 1, 2007; 76 FR Oat, hay ...... 9.0 Oat, straw ...... 4.0 31491, June 1, 2011] Onion, bulb ...... 0.1 Peppermint, hay ...... 0.1 § 180.328 Napropamide; tolerances for Rye, forage ...... 1.0 residues. Rye, grain ...... 0.05 Rye, straw ...... 2.0 (a) General. Tolerances are estab- Sorghum, grain, forage ...... 0.8 lished for residues of the herbicide Sorghum, grain, grain ...... 0.2 Sorghum, grain, stover ...... 0.2 napropamide, N,N-diethyl-2-(1- Spearmint, hay ...... 0.1 napthalenyloxy) propionamide, in or on Wheat, forage ...... 1.0 the following food commodities: Wheat, grain ...... 0.05 Wheat, hay ...... 4.0 Wheat, straw ...... 2.0 Expiration/ Commodity Parts per revocation million date (2) Tolerances are established for residues of the herbicide bromoxynil, 3,5- Almond, hulls ...... 0.1 None dibromo-4-hydroxybenzonitrile, includ- Asparagus ...... 0.1 None Basil ...... 0.1 None ing its metabolites and degradates, in Berry group 13 ...... 0.1 None or on the commodities in the table Coffee, green bean ...... 0.1 None below. Compliance with the tolerance Cranberry ...... 0.1 None levels is to be determined by meas- Grape ...... 0.1 None uring only bromoxynil and its metabo- Kiwifruit ...... 0.1 None lite, 3,5-dibromo-4-hydroxybenzoic acid Marjoram ...... 0.1 None (DBHA), resulting from application of Nut, tree, group 14 ...... 0.1 None Peppermint, tops ...... 0.1 None its octanoic and/or heptanoic acid Persimmon ...... 0.1 None ester, in or on the commodities. Rhubarb ...... 0.1 None Rosemary ...... 0.1 None Parts per Savory, summer ...... 0.1 None Commodity million Savory, winter ...... 0.1 None Cattle, fat ...... 1 Spearmint, tops ...... 0.1 None Cattle, meat byproducts ...... 3.5 Strawberry ...... 0.1 None Cattle, meat ...... 0.5 Sweet potato, roots ...... 0.1 None Cotton, gin byproducts ...... 7.0 Vegetable, brassica, leafy, group 5 0.1 None Cotton, hulls ...... 5.0 Vegetable, fruiting, group 8 ...... 0.1 None Cotton, undelinted seed ...... 1.5 Egg ...... 0.05 Goat, fat ...... 1 (b) Section 18 emergency exemptions. Goat, meat byproducts ...... 3.5 [Reserved] Goat, meat ...... 0.5 Hog, fat ...... 1 (c) Tolerances with regional registra- Hog, meat byproducts ...... 3.5 tions. [Reserved] Hog, meat ...... 0.5 (d) Indirect or inadvertent residues. Horse, fat ...... 1 Horse, meat byproducts ...... 3.5 [Reserved] Horse, meat ...... 0.5 Milk ...... 0.4 [73 FR 52614, Sept. 10, 2008, as amended at 76 Poultry, fat ...... 0.05 FR 34885, June 15, 2011]

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§ 180.330 S-(2-(Ethylsulfinyl)ethyl) O,O- Commodity Parts per dimethyl phosphorothioate; toler- million ances for residues. Hog, meat byproducts ...... 0.01 (a) General. (1) Tolerances are estab- Horse, fat ...... 0.01 Horse, meat ...... 0.01 lished for the combined residues of the Horse, meat byproducts ...... 0.01 insecticide oxydemeton-methyl (S-(2- Milk ...... 0.01 (ethylsulfinyl)ethyl) O,O-dimethyl Poultry, fat ...... 0.01 Poultry, meat ...... 0.01 phosphorothioate) and its metabolite Poultry, meat byproducts ...... 0.01 oxydemeton-methyl sulfone in or on Sheep, fat ...... 0.01 the following food commodities: Sheep, meat ...... 0.01 Sheep, meat byproducts ...... 0.01 Commodity Parts per million (b) Section 18 emergency exemptions. Alfalfa, forage ...... 5.0 [Reserved] Alfalfa, hay ...... 11.0 (c) Tolerances with regional registra- Bean, lima ...... 0.2 tions. Tolerances with regional reg- Beet, sugar, roots ...... 0.3 Beet, sugar, tops ...... 0.5 istrations, as defined in § 180.1(l), are Broccoli ...... 1.0 established for the combined residues Brussels sprouts ...... 1.0 of the insecticide oxydemeton-methyl Cabbage ...... 2.0 (S-(2-(ethylsulfinyl)-ethyl) O,O-di- Cauliflower ...... 1.0 Clover, forage ...... 5.0 methyl phosphorothioate) and its me- Clover, hay ...... 10.0 tabolite oxydemeton-methyl sulfone in Corn, sweet, forage ...... 1.0 or on the following food commodities: Corn, sweet, kernel plus cob with husks removed 0.5 Corn, sweet, stover ...... 3.0 Parts per Cotton, undelinted seed ...... 0.02 Commodity million Cucumber ...... 1.0 Eggplant ...... 1.0 Broccoli raab ...... 2.0 Grapefruit ...... 1.0 Hazelnut ...... 0.05 Lemon ...... 1.0 (d) Indirect or inadvertent residues. Lettuce, head ...... 2.0 [Reserved] Melon ...... 0.2 Onion, bulb ...... 0.05 [72 FR 54578, Sept. 26, 2007] Orange ...... 1.0 Pepper ...... 0.75 § 180.331 4-(2,4-Dichlorophenoxy) bu- Peppermint, tops ...... 12.5 tyric acid; tolerances for residues. Pumpkin ...... 0.2 Safflower, seed ...... 1.0 (a) General. Tolerances are estab- Sorghum, forage, forage ...... 2.0 lished for residues of the herbicide 4- Sorghum, grain, forage ...... 2.0 (2,4-dichlorophenoxy) butyric acid (2,4- Sorghum, grain, grain ...... 0.75 Spearmint, tops ...... 12.5 DB), both free and conjugated, deter- Squash, summer ...... 1.0 mined as the acid, in or on food com- Squash, winter ...... 0.3 modities, as follows: Strawberry ...... 2.0 Walnut ...... 0.05 Parts per Commodity million (2) Tolerances are established for the Alfalfa, forage ...... 0.7 combined residues of the insecticide Alfalfa, hay ...... 2.0 oxydemeton-methyl (S-(2- Cattle, meat byproducts ...... 0.05 (ethylsulfinyl)ethyl) O,O-dimethyl Clover, forage ...... 0.2 phosphorothioate) and its cholin- Clover, hay ...... 0.2 Goat, meat byproducts ...... 0.05 esterase-inhibiting metabolites in or Hog, meat byproducts ...... 0.05 on the following food commodities: Horse, meat byproducts ...... 0.05 Peanut ...... 0.2 Peppermint, tops ...... 0.2 Commodity Parts per million Sheep, meat byproducts ...... 0.05 Soybean, forage ...... 0.7 Cattle, fat ...... 0.01 Soybean, hay ...... 2.0 Cattle, meat ...... 0.01 Soybean, seed ...... 0.5 Cattle, meat byproducts ...... 0.01 Spearmint, tops ...... 0.2 Egg ...... 0.01 Trefoil, forage ...... 0.7 Goat, fat ...... 0.01 Trefoil, hay ...... 2.0 Goat, meat ...... 0.01 Goat, meat byproducts ...... 0.01 Hog, fat ...... 0.01 (b) Section 18 emergency exemptions. Hog, meat ...... 0.01 [Reserved]

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(c) Tolerances with regional registra- Commodity Parts per tions. [Reserved] million (d) Indirect or inadvertent residues. Wheat, bran ...... 3.0 [Reserved] Wheat, forage ...... 2.0 Wheat, germ ...... 3.0 [73 FR 54961, Sept. 24, 2008, as amended at 74 Wheat, grain ...... 0.75 FR 46374, Sept. 9, 2009] Wheat, hay ...... 7.0 Wheat, middlings ...... 3.0 Wheat, shorts ...... 3.0 § 180.332 Metribuzin; tolerances for Wheat, straw ...... 1.0 residues. (a) General. Tolerances are estab- (b) Section 18 emergency exemptions. lished for combined residues of the her- [Reserved] bicide metribuzin (4-amino-6-(1,1- (c) Tolerances with regional registra- dimethyl- ethyl)-3-(methylthio)-;1,2,4- tions. [Reserved] triazin-5(4H)-one) and its triazinone (d) Indirect or inadvertent residues. metabolites in or on food commodities: [Reserved]

Parts per [42 FR 62913, Dec. 14, 1977, as amended at 43 Commodity million FR 41396, Sept. 18, 1978; 44 FR 26744, May 7, 1979; 44 FR 45387, Aug. 2, 1979; 52 FR 23654, Alfalfa, forage ...... 2.0 June 24, 1987; 55 FR 26440, June 28, 1990; 62 FR Alfalfa, hay ...... 7.0 Asparagus ...... 0.1 66024, 66025, Dec. 17, 1997; 65 FR 33698, May 24, Barley, grain ...... 0.75 2000; 66 FR 63198, Dec. 5, 2001; 67 FR 49617, Barley, hay ...... 7.0 July 31, 2002] Barley, pearled barley ...... 3.0 Barley, straw ...... 1.0 § 180.337 Oxytetracycline; tolerances Carrot, roots ...... 0.3 for residues. Cattle, fat ...... 0.7 Cattle, meat ...... 0.7 (a) General. Tolerances are estab- Cattle, meat byproducts ...... 0.7 lished for residues of the fungicide/ Corn, field, forage ...... 0.1 Corn, field, grain ...... 0.05 bactericide oxytetracycline, including Corn, field, stover ...... 0.1 its metabolites and degradates, in or Corn, pop, grain ...... 0.05 on the commodities in the table in this Corn, sweet, forage ...... 0.1 Corn, sweet, kernel plus cob with husks removed 0.05 paragraph. Compliance with the toler- Corn, sweet, stover ...... 0.1 ance levels specified in this paragraph Egg ...... 0.01 is to be determined by measuring only Goat, fat ...... 0.7 Goat, meat ...... 0.7 oxytetracycline, Goat, meat byproducts ...... 0.7 (4S,4aR,5S,5aR,6S,12aS)-4- Grass, forage ...... 2.0 (dimethylamino)-1,4,4a,5,5a,6,11,12a- Grass, hay ...... 7.0 octahydro-3,5,6,10,12,12a-hexahydroxy- Hog, fat ...... 0.7 Hog, meat ...... 0.7 6-methyl-1,11-dioxo-2- Hog, meat byproducts ...... 0.7 naphthacenecarboxamide, in or on the Horse, fat ...... 0.7 commodity. Horse, meat ...... 0.7 Horse, meat byproducts ...... 0.7 Parts per Lentil ...... 0.05 Commodity million Milk ...... 0.05 Pea, dry, seed ...... 0.05 Apple ...... 0.35 Pea, field, hay ...... 4.0 Fruit, citrus, group 10-10 ...... 0.01 Pea, field, vines ...... 0.5 Peach ...... 0.35 Pea, succulent ...... 0.1 Pear ...... 0.35 Potato ...... 0.6 Potato, chips ...... 3.0 Potato, processed potato waste ...... 3.0 (b) Section 18 emergency exemptions. Poultry, fat ...... 0.7 Time-limited tolerances specified in Poultry, meat ...... 0.7 the following table are established for Poultry, meat byproducts ...... 0.7 Sainfoin, forage ...... 2.0 residues of the fungicide/bactericide Sainfoin, hay ...... 7.0 oxytetracycline, including its metabo- Sheep, fat ...... 0.7 lites and degradates, in or on the com- Sheep, meat ...... 0.7 modities in the table in this paragraph. Sheep, meat byproducts ...... 0.7 Soybean, seed ...... 0.3 Compliance with the tolerance levels Soybean, forage ...... 4.0 specified in this paragraph is to be de- Soybean, hay ...... 4.0 termined by measuring only oxytetra- Sugarcane, cane ...... 0.1 Sugarcane, molasses ...... 2.0 cycline, (4S,4aR,5S,5aR,6S,12aS)-4- Tomato ...... 0.1 (dimethylamino)-1,4,4a,5,5a,6,11,12a-

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octahydro-3,5,6,10,12,12a-hexahydroxy- Commodity Parts per 6-methyl-1,11-dioxo-2- million naphthacenecarboxamide, in or on the Wheat, straw ...... 25 specified agricultural commodities, resulting from use of the pesticide pursu- (2) Tolerances are established for res- ant to FIFRA section 18 emergency ex- idues of the herbicide MCPA ((4-chloro- emptions. The tolerances expire on the 2-methylphenoxy)acetic acid) resulting dates specified in the table. from the direct application of MCPA or its sodium or dimethylamine salts, or Expiration/ Parts per its 2-ethylhexyl ester in or on the fol- Commodity million revocation date lowing food commodities: Fruit, citrus, group 10–10 ...... 0.40 12/31/19 Parts per Commodity million (c) Tolerances with regional registrations. [Reserved] Cattle, fat ...... 0.1 (d) Indirect or inadvertent residues. Cattle, meat ...... 0.1 Cattle, meat byproducts ...... 0.1 [Reserved] Goat, fat ...... 0.1 [76 FR 23493, Apr. 27, 2011, as amended at 82 Goat, meat ...... 0.1 FR 13251, Mar. 10, 2017; 83 FR 62493, Dec. 4, Goat, meat byproducts ...... 0.1 2018] Hog, fat ...... 0.1 Hog, meat ...... 0.1 Hog, meat byproducts ...... 0.1 § 180.339 MCPA; tolerances for resi- Horse, fat ...... 0.1 dues. Horse, meat ...... 0.1 (a) General. (1) Tolerances are estab- Horse, meat byproducts ...... 0.1 lished for residues of the herbicide Milk ...... 0.1 Sheep, fat ...... 0.1 MCPA ((4-chloro-2- Sheep meat ...... 0.1 methylphenoxy)acetic acid), both free Sheep meat byproducts ...... 0.1 and conjugated, resulting from the direct application of MCPA or its sodium (b) Section 18 emergency exemptions. or dimethylamine salts, or its 2- [Reserved] ethylhexyl ester in or on the following (c) Tolerances with regional registra- food commodities: tions. [Reserved] (d) Indirect or inadvertent residues. Parts per Commodity million [Reserved]

Alfalfa, forage ...... 0.5 [72 FR 28888, May 23, 2007, as amended at 73 Alfalfa, hay ...... 2.0 FR 5109, Jan. 29, 2008] Barley, grain ...... 1.0 Barley, hay ...... 40 § 180.341 2,4-Dinitro-6-octylphenyl cro- Barley, straw ...... 25 Clover, forage ...... 0.5 tonate and 2,6-dinitro-4-octylphenyl Clover, hay ...... 2.0 crotonate; tolerances for residues. Flax, seed ...... 0.1 Grain, aspirated fractions ...... 3.0 (a) General. Tolerances are estab- Grass, forage ...... 300 lished for combined negligible residues Grass, hay ...... 20 of a fungicide and insecticide that is a Lespedeza, forage ...... 0.5 mixture of 2,4-dinitro-6-octylphenyl Lespedeza, hay ...... 2.0 Oat, forage ...... 20 crotonate and 2,6-dinitro-4-octylphenyl Oat, grain ...... 1.0 crotonate in or on raw agricultural Oat, hay ...... 115 commodities as follows: Oat, straw ...... 25 Pea, dry ...... 0.1 Pea, field, hay ...... 0.1 Parts per Commodity million Pea, succulent ...... 0.1 Pea, field, vines ...... 0.1 Apple 1 ...... 0.1 Rye, forage ...... 20 Grape 1 ...... 0.1 Rye, grain ...... 1.0 Rye, straw ...... 25 1 There are no U.S. registrations on apple and grape as of Trefoil, forage ...... 0.5 October 24, 2002. Trefoil, hay ...... 2.0 Vetch, forage ...... 0.5 (b) Section 18 emergency exemptions. Vetch, hay ...... 2.0 [Reserved] Wheat, forage ...... 20 Wheat, grain ...... 1.0 (c) Tolerances with regional registra- Wheat, hay ...... 115 tions. [Reserved]

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(d) Indirect or inadvertent residues. Commodity Parts per [Reserved] million [40 FR 29715, July 15, 1975, as amended at 63 Poultry, fat ...... 0.1 FR 57076, Oct. 26, 1998; 69 FR 43924, July 23, Poultry, meat ...... 0.1 Poultry, meat byproducts ...... 0.1 2004] Pumpkin ...... 0.05 Radish ...... 2.0 § 180.342 Chlorpyrifos; tolerances for Rutabaga ...... 0.5 residues. Sheep, fat ...... 0.2 Sheep, meat ...... 0.05 (a) General. (1) Tolerances are estab- Sheep, meat byproducts ...... 0.05 lished for residues of the pesticide Spearmint, tops ...... 0.8 Spearmint, oil ...... 8.0 chlorpyrifos per se (O,O-diethyl-O- Sorghum, grain, forage ...... 0.5 (3,5,6-trichloro-2-pyridyl) Sorghum, grain, grain ...... 0.5 phosphorothioate) in or on the fol- Sorghum, grain, stover ...... 2.0 Soybean, seed ...... 0.3 lowing food commodities: Strawberry ...... 0.2 Sunflower, seed ...... 0.1 Parts per Sweet potato, roots ...... 0.05 Commodity million Turnip, roots ...... 1.0 Turnip, tops ...... 0.3 Alfalfa, forage ...... 3.0 Vegetable, brassica, leafy, group 5 ...... 1.0 Alfalfa, hay ...... 13 Vegetable, legume, group 6. except soybean ...... 0.05 Almond ...... 0.2 Walnut ...... 0.2 Almond, hulls ...... 12 Wheat, forage ...... 3.0 Apple ...... 0.01 Wheat, grain ...... 0.5 Apple, wet pomace ...... 0.02 Wheat, straw ...... 6.0 Banana ...... 0.1 Beet, sugar, dried pulp ...... 5.0 Beet, sugar, molasses ...... 15 (2) Chlorpyrifos [O,O-diethyl O-(3,5,6- Beet, sugar, roots ...... 1.0 trichloro-2-pyridyl) phosphorothioate] Beet, sugar, tops ...... 8.0 Cattle, fat ...... 0.3 may be safely used in accordance with Cattle, meat ...... 0.05 the following prescribed conditions. Cattle, meat byproducts ...... 0.05 (i) Application shall be limited solely Cherry, sweet ...... 1.0 to spot and/or crack and crevice treat- Cherry, tart ...... 1.0 Citrus, dried pulp ...... 5.0 ment in food handling establishments Citrus, oil ...... 20 where food and food products are held, Corn, field, forage ...... 8.0 processed, prepared or served. Contami- Corn, field, grain ...... 0.05 Corn, field, refined oil ...... 0.25 nation of food or food contact surfaces Corn, field, stover ...... 8.0 shall be avoided. Food must be re- Corn, sweet, forage ...... 8.0 moved or covered during treatment. Corn, sweet, kernel plus cob with husk removed 0.05 (ii) Spray concentration for spot Corn, sweet, stover ...... 8.0 Cotton, undelinted seed ...... 0.2 treatment shall be limited to a max- Cranberry ...... 1.0 imum of 0.5 percent of the active ingre- Cucumber ...... 0.05 dient by weight. A course, low-pressure Egg ...... 0.01 Fig ...... 0.01 spray shall be used to avoid atomiza- Fruit, citrus, group 10 ...... 1.0 tion or splashing of the spray. Goat, fat ...... 0.2 (iii) Paint-on application for spot Goat, meat ...... 0.05 treatment shall be limited to a max- Goat, meat byproducts ...... 0.05 Hazelnut ...... 0.2 imum of 2 percent of the active ingre- Hog, fat ...... 0.2 dient by weight. Hog, meat ...... 0.05 (iv) Crack and crevice treatment Hog, meat byproducts ...... 0.05 Horse, fat ...... 0.25 shall be limited to a maximum of 2 per- Horse, meat ...... 0.25 cent of the active ingredient by weight. Horse, meat byproducts ...... 0.25 Equipment capable of delivering a pin- Kiwifruit ...... 2.0 stream of insecticide shall be used. Milk, fat (Reflecting 0.01 ppm in whole milk) ...... 0.25 Nectarine ...... 0.05 (v) Application via adhesive strips Onion, bulb ...... 0.5 shall contain a maximum of 10% by Peach ...... 0.05 weight of the controlled-release prod- Peanut ...... 0.2 uct in food-handling establishments Peanut, refined oil ...... 0.2 Pear ...... 0.05 where food and food products are held, Pecan ...... 0.2 processed, prepared, or served. A max- Pepper ...... 1.0 imum of 36 strips (or 5.15 grams of Peppermint, tops ...... 0.8 Peppermint, oil ...... 8.0 chlorpyrifos) is to be used per 100 Plum, prune, fresh ...... 0.05 square feet of floor space. The strips

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are not to be placed in exposed areas Commodity Parts per where direct contact with food, uten- million sils, and food-contact surfaces would be Grape ...... 0.01 likely to occur. (vi) To assure safe use of the insecti- (d) Indirect or inadvertent residues. cide, its label and labeling shall con- [Reserved] form to that registered by the U.S. En- vironmental Protection Agency, and it [65 FR 33711, May 24, 2000, as amended at 67 shall be used in accordance with such FR 49617, July 31, 2002; 71 FR 74817, Dec. 13, 2006; 73 FR 53739, Sept. 17, 2008; 76 FR 56656, label and labeling. Sept. 14, 2011] (3) A tolerance of 0.1 part per million is established for residues of § 180.345 Ethofumesate; tolerances for chlorpyrifos, per se, in or on food com- residues. modities (other than those already cov- (a) General. Tolerance are established ered by a higher tolerance as a result for residues of the herbicide of use on growing crops) in food service ethofumesate, including its metabo- establishments where food and food lites and degradates, in or on the com- products are prepared and served, as a modities in the table below. Compli- result of the application of chlorpyrifos in microencapsulated form. ance with the tolerance levels specified (i) Application of a microencap- below is to be determined by measuring sulated product shall be limited solely only the sum of ethofumesate, 2- to spot and/or crack and crevice treat- ethoxy-2,3-dihydro-3,3-dimethyl-5- ment in food handling establishments benzofuranyl methanesulfonate, and its where food and food products are pre- metabolites 2-hydroxy-2,3-dihydro-3,3- pared and served. All treatments shall dimethyl-5-benzofuranyl be applied in such a manner as to avoid methanesulfonate, and 2,3-dihydro-3,3- contamination of food or food contact dimethyl-2-oxo-5- surfaces. benzofuranylmethanesulfonate, cal- (ii) Spray concentrations shall be culated as the stoichiometric equiva- limited to a maximum of 0.5 percent of lent of ethofumesate, in or on the fol- the active ingredient by weight. lowing food commodities. (iii) For crack and crevice treatment, Parts per equipment capable of delivering a pin Commodity million stream of spray directly into cracks and crevices or capable of applying Beet, garden, roots ...... 0.5 Beet, garden, tops ...... 5.0 small amounts of insecticide into Beet, sugar, molasses ...... 2.0 cracks and crevices shall be used. Beet, sugar, roots ...... 1.5 (iv) For spot treatment, an individual Beet, sugar, tops ...... 4.0 spot shall not exceed 2 square feet. Cattle, fat ...... 0.05 Cattle, meat ...... 0.05 (v) To assure safe use of the insecti- Cattle, meat byproducts ...... 0.05 cide, its label and labeling shall con- Garlic ...... 0.25 form to that registered by the U.S. En- Goat, fat ...... 0.05 vironmental Protection Agency, and it Goat, meat ...... 0.05 shall be used in accordance with such Goat, meat byproducts ...... 0.05 Grass, straw ...... 1.0 label and labeling. Horse, fat ...... 0.05 (b) Section 18 emergency exemptions. Horse, meat ...... 0.05 [Reserved] Horse, meat byproducts ...... 0.05 (c) Tolerances with regional registra- Onion, bulb ...... 0.25 Shallot, bulb ...... 0.25 tions. Tolerances with regional reg- Shallot, fresh leaves ...... 0.25 istration, as defined in 180.1(l), are es- Sheep, fat ...... 0.05 tablished for residues of the pesticide Sheep, meat ...... 0.05 chlorpyrifos per se (O,O-diethyl- O- Sheep, meat byproducts ...... 0.05 (3,5,6-trichloro-2-pyridyl) phosphorothioate) in or on the fol- (b) Section 18 emergency exemptions. lowing food commodities: [Reserved] (c) Tolerances with regional registra- Commodity Parts per tions. Tolerances with a regional reg- million istration, as defined in § 180.1(l) are es- Asparagus ...... 5.0 tablished for residues of the herbicide

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ethofumesate, including its metabo- (b) Section 18 emergency exemptions. lites and degradates, in or on the com- [Reserved] modities in the table below. Compli- (c) Tolerances with regional registra- ance with the tolerance levels specified tions. [Reserved] is to be determined by measuring only (d) Indirect or inadvertent residues. the sum of ethofumesate, 2-ethoxy-2,3- [Reserved] dihydro-3,3-dimethyl-5-benzofuranyl methanesulfonate, and its metabolites [65 FR 33712, May 24, 2000, as amended at 73 2-hydroxy-2,3-dihydro-3,3-dimethyl-5- FR 53739, Sept. 17, 2008; 75 FR 60243, Sept. 29, benzofuranyl methanesulfonate, and 2010] 2,3-dihydro-3,3-dimethyl-2-oxo-5- benzofuranylmethanesulfonate, cal- § 180.350 Nitrapyrin; tolerances for culated as the stoichiometric equiva- residues. lent of ethofumesate, in or on the raw (a) General. Tolerances are estab- agricultural commodities. lished for residues of the nitrification inhibitor nitrapyrin, including its me- Parts per Commodity million tabolites and degradates, in or on the commodities in the table below. Com- Carrot, roots ...... 7.0 pliance with the tolerance levels specified below is to be determined by meas- (d) Indirect or inadvertent residues. uring only the sum of nitrapyrin (2- [Reserved] chloro-6-(trichloromethyl) pyridine) [63 FR 34828, June 26, 1998, as amended at 71 and its 6–CPA metabolite (6-chloro-pic- FR 51516, Aug. 30, 2006; 72 FR 52019, Sept. 12, olinic acid), calculated as the stoichio- 2007; 82 FR 57158, Dec. 4, 2017] metric equivalent of nitrapyrin, in or on the commodity: § 180.349 Fenamiphos; tolerances for residues. Commodity Parts per (a) General. Tolerances are estab- million lished for residues of the nematicide/in- Almond, hulls ...... 0.06 secticide fenamiphos, ethyl 3-methyl-4- Corn, field, forage ...... 1.0 (methylthio)phenyl 1- Corn, field, grain ...... 0.1 (methylethyl)phosphoramidate, includ- Corn, field, milled byproducts ...... 0.2 ing its metabolites and degradates, in Corn, field, stover ...... 1.0 Corn, pop, grain ...... 0.1 or on the commodities in the following Corn, pop, stover ...... 1.0 table. Compliance with the tolerance Corn, sweet, forage ...... 1.0 levels specified in this paragraph is to Corn, sweet, kernel plus cob with husks removed 0.1 be determined by measuring only the Corn, sweet, stover ...... 1.0 sum of fenamiphos, ethyl 3-methyl-4- Fruit, citrus, group 10–10 ...... 0.06 (methylthio)phenyl 1- Fruit, citrus, group 10–10, dried pulp ...... 0.5 (methylethyl)phosphoramidate, and its Fruit, citrus, group 10–10, oil ...... 2 Leaf petiole vegetable subgroup 22B ...... 0.5 cholinesterase inhibiting metabolites Nut, tree, group 14–12 ...... 0.02 ethyl 3-methyl-4- Sorghum, forage, forage ...... 0.5 (methylsulfinyl)phenyl 1- Sorghum, grain, forage ...... 0.5 (methylethyl)phosphoramidate and Sorghum, grain, grain ...... 0.1 ethyl 3-methyl-4- Sorghum, grain, stover ...... 0.5 (methylsulfonyl)phenyl 1- Vegetable, Brassica, head and stem, group 5–16 0.1 Vegetable, bulb, group 3–07 ...... 0.3 (methylethyl)phosphoramidate, cal- Vegetable, leafy, group 4–16 ...... 0.4 culated as the stoichiometric equiva- Wheat, bran ...... 3.0 lent of fenamiphos, in or on the com- Wheat, forage ...... 2.0 modity. Wheat, grain ...... 0.5 Wheat, milled byproducts, except flour ...... 2.0 Parts per Wheat, straw ...... 6.0 Commodity million

Banana1 ...... 0.1 (b) Section 18 emergency exemptions. Grape1 ...... 0.1 [Reserved] Grape, raisin1 ...... 0.3 (c) Tolerances with regional registra- Pineapple1 ...... 0.3 tions. [Reserved] 1 There are no U.S. registrations as of May 31, 2007.

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(d) Indirect or inadvertent residues. on the following raw agricultural com- [Reserved] modities in the table that follows: [46 FR 58315, Dec. 1, 1981, as amended at 47 Commodity Parts per FR 22957, May 26, 1982; 52 FR 33238, Sept. 2, million 1987; 58 FR 32304, June 9, 1993; 63 FR 57076, Oct. 26, 1998; 72 FR 53461, Sept. 19, 2007; 82 FR Beet, garden, roots ...... 0.05 Beet, garden, tops ...... 1.0 56744, Nov. 30, 2017; 84 FR 44712, Aug. 27, 2019] Beet, sugar, roots ...... 0.1 Beet, sugar, tops ...... 5.0 § 180.352 Terbufos; tolerances for resi- Spinach ...... 6.0 dues. (a) General. Tolerances are estab- (b) Section 18 emergency exemptions. lished for the combined residues of the [Reserved] insecticide terbufos (phosphorodithioic (c) Tolerances with regional registra- acid, S-(t-butylthio)methyl O,O-diethyl tions. [Reserved] ester) and its phosphorylated (cholin- (d) Indirect or inadvertent residues. esterase-inhibiting) metabolites [Reserved] (phosphorothioic acid, S-(t- [40 FR 4658, Jan. 31, 1975, as amended at 62 butylthio)methyl O,O-diethyl ester; FR 45747, Aug. 29, 1997; 63 FR 49472, Sept. 16, phosphorothioic acid, S-(t- 1998; 64 FR 46292, Aug. 25, 1999; 65 FR 82293, butylsulfinyl)methyl O,O-diethyl ester; Dec. 28, 2000; 66 FR 64773, Dec. 14, 2001; 68 FR phosphorothioic acid, S-(t- 37764, June 25, 2003; 69 FR 71717, Dec. 10, 2004; 72 FR 53449, Sept. 19, 2007; 73 FR 53740, Sept. butylsulfonyl)methyl O,O-diethyl 17, 2008] ester; phosphorodithioic acid, S-(t- butylsulfinyl)methyl O,O-diethyl ester; § 180.355 Bentazon; tolerances for resi- and phosphorodithioic acid, S-(t- dues. butylsulfonyl)methyl O,O-diethyl (a) General. (1) Tolerances are estab- ester) in or on food commodities: lished for residues of bentazon, includ- Parts per ing its metabolites and degradates, in Commodity million or on the commodities in the table below. Compliance with the tolerance Banana ...... 0.025 Beet, sugar, roots ...... 0.05 levels specified below is to be deter- Beet, sugar, tops ...... 0.1 mined by measuring for only the sum Coffee, green bean 1 ...... 0.05 of bentazon (3-(1-methylethyl)-1H-2,1,3- Corn, field, forage ...... 0.5 benzothiadiazin-4(3H)-one 2,2-dioxide), Corn, field, grain ...... 0.5 Corn, field, stover ...... 0.5 6-hydroxy-3-isopropyl-1H-2,1,3- Corn, pop, grain ...... 0.5 benzothiadiazin-4(3H)-one 2,2-dioxide, Corn, pop, stover ...... 0.5 and 8-hydroxy-3-isopropyl-1H-2,1,3- Corn, sweet, kernel plus cob with husks removed 0.05 benzothiadiazin-4(3H)-one 2,2-dioxide Corn, sweet, forage ...... 0.5 Corn, sweet, stover ...... 0.5 calculated as the stoichiometric equiv- Sorghum, grain, forage ...... 0.5 alent of bentazon. Sorghum, grain, grain ...... 0.05 Sorghum, grain, stover ...... 0.5 Parts per Commodity million 1 There are no U. S. registrations as of August 2, 1995, for the use of terbufos on the growing crop, coffee. Bean, dry, seed ...... 0.05 Bean, succulent ...... 0.5 (b) Section 18 emergency exemptions. Corn, field, forage ...... 3.0 [Reserved] Corn, field, grain ...... 0.05 (c) Tolerances with regional registra- Corn, field, stover ...... 3.0 tions. [Reserved] Corn, pop, grain ...... 0.05 Corn, sweet, kernel plus cob with husks removed 0.05 (d) Indirect or inadvertent residues. Cowpea, forage ...... 10.0 [Reserved] Cowpea, hay ...... 3.0 Flax, seed ...... 1.0 [73 FR 53740, Sept. 17, 2008] Pea, dry, seed ...... 3 Pea, field, hay ...... 8.0 § 180.353 Desmedipham; tolerances for Pea, field, vines ...... 3.0 residues. Pea, succulent ...... 3.0 Peanut ...... 0.05 (a) General. Tolerances are estab- Peanut, hay ...... 3.0 lished for residues of the herbicide Pepper, nonbell ...... 0.05 Peppermint, tops ...... 1.0 desmedipham, (ethyl-m- Rice, grain ...... 0.05 hydroxycarbanilate carbanilate) in or Rice, hulls ...... 0.25

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Commodity Parts per § 180.356 Norflurazon; tolerances for million residues. Sorghum, forage ...... 0.20 (a) General. Tolerances are estab- Sorghum, grain, grain ...... 0.05 lished for the combined residues of the Sorghum, grain, stover ...... 0.05 Soybean, forage ...... 8.0 herbicide norflurazon (4-chloro-5- Soybean, hay ...... 8.0 (methylamino)-2-(alpha, alpha, alpha- Soybean, seed ...... 0.05 trifluoro-m-tolyl)-3-(2H)-pyridazinone) Spearmint, tops ...... 1.0 and its desmethyl metabolite 4-chloro- 5-(amino)-2-alpha, alpha, alpha- (2) Tolerances are established for the trifluoro-m-tolyl)-3(2H)-pyridazinone in combined residues of the herbicide or on the following raw agricultural bentazon (3-isopropyl-1H-2,1,3- commodities: benzothiadiazin-4(3H)-one-2,2-dioxide) and its metabolite 2-amino-N-isopropyl Commodity Parts per benzamide (AIBA) in or on the fol- million lowing food commodities: Alfalfa, forage ...... 3.0 Alfalfa, hay ...... 5.0 Parts per Alfalfa, seed ...... 0.1 Commodity million Almond, hulls ...... 1.0 Almond ...... 0.1 Cattle, fat ...... 0.05 Apple ...... 0.1 Cattle, meat byproducts ...... 0.05 Apricot ...... 0.1 Cattle, meat ...... 0.05 Asparagus ...... 0.05 Egg ...... 0.05 Avocado ...... 0.20 Goat, fat ...... 0.05 Blackberry ...... 0.1 Goat, meat byproducts ...... 0.05 Blueberry ...... 0.2 Cattle, fat ...... 0.1 Goat, meat ...... 0.05 Cattle, liver ...... 0.50 Hog, fat ...... 0.05 Cattle, meat ...... 0.1 Hog, meat byproducts ...... 0.05 Cattle, meat byproducts, except liver ...... 0.1 Hog, meat ...... 0.05 Cherry ...... 0.1 Milk ...... 0.02 Citrus, dried pulp ...... 0.4 Poultry, fat ...... 0.05 Citrus, molasses ...... 1.0 Poultry, meat byproducts ...... 0.05 Cotton, undelinted seed ...... 0.1 Poultry, meat ...... 0.05 Cranberry ...... 0.1 Sheep, fat ...... 0.05 Fruit, citrus ...... 0.2 Sheep, meat byproducts ...... 0.05 Goat, fat ...... 0.1 Sheep, meat ...... 0.05 Goat, liver ...... 0.50 Goat, meat ...... 0.1 Goat, meat byproducts, except liver ...... 0.1 (b) Section 18 emergency exemptions. Grape ...... 0.1 [Reserved] Hazelnut ...... 0.1 (c) Tolerances with regional registra- Hog, fat ...... 0.1 Hog, liver ...... 0.50 tions. Tolerances with regional reg- Hog, meat ...... 0.1 istration as defined in § 180.1(m), are es- Hog, meat byproducts, except liver ...... 0.1 tablished for combined residues of the Hop, dried cones ...... 3.0 herbicide, bentazon (3-isopropyl-1H-2, Hop, vines ...... 1.0 Horse, fat ...... 0.1 1,3-benzothiadiazin-4(3H)-one-2,2-diox- Horse, liver ...... 0.50 ide) and its 6- and 8-hydroxy metabo- Horse, meat ...... 0.1 lites in or on the following food com- Horse, meat byproducts, except liver ...... 0.1 Milk ...... 0.1 modities: Nectarine ...... 0.1 Peach ...... 0.1 Commodity Parts per Peanut ...... 0.05 million Peanut, hay ...... 5.50 Peanut, hay ...... 1.5 Clover, forage ...... 1.0 Pear ...... 0.1 Clover, hay ...... 2.0 Pecan ...... 0.1 Plum, prune, fresh ...... 0.1 (d) Indirect or inadvertent residues. Poultry, fat ...... 0.1 Poultry, meat ...... 0.1 [Reserved] Poultry, meat byproducts ...... 0.1 [42 FR 26979, May 26, 1977] Raspberry ...... 0.2 Sheep, fat ...... 0.1 EDITORIAL NOTE: For FEDERAL REGISTER ci- Sheep, liver ...... 0.50 tations affecting § 180.355, see the List of CFR Sheep, meat ...... 0.1 Sheep, meat byproducts, except liver ...... 0.1 Sections Affected, which appears in the Soybean ...... 0.1 Finding Aids section of the printed volume Soybean, forage ...... 1.0 and at www.govinfo.gov. Soybean, hay ...... 1.0

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ance levels specified in the following Commodity Parts per million table below is to be determined by Walnut ...... 0.1 measuring only the sum of pendimethalin, [N-(1-ethylpropyl)-3,4- (b) Section 18 emergency exemptions. dimethyl-2,6-dinitrobenzenamine] and [Reserved] its metabolite, 4-[(1- (c) Tolerances with regional registra- ethylpropyl)amino]-2-methyl-3,5- tion. [Reserved] dinitrobenzyl alcohol, calculated as the (d) Indirect or inadvertent residues. stoichiometric equivalent of [Reserved] pendimethalin, in or on the commodity. [47 FR 14909, Apr. 7, 1982]

EDITORIAL NOTE: For FEDERAL REGISTER ci- Commodity Parts per tations affecting § 180.356, see the List of CFR million Sections Affected, which appears in the Alfalfa, forage ...... 80 Finding Aids section of the printed volume Alfalfa, hay ...... 150 and at www.govinfo.gov. Alfalfa, seed ...... 0.10 Almond, hulls ...... 6.0 § 180.360 Asulam; tolerance for resi- Apple, wet pomace ...... 0.20 Artichoke, globe ...... 0.1 dues. Asparagus ...... 0.15 (a) General. Tolerances are estab- Beans ...... 0.10 lished for the combined residues of Beans, forage ...... 0.10 Beans, hay ...... 0.10 asulam (methyl sulfanilylcarbamate) Berry, low growing subgroup 13–07G ...... 0.1 and its sulfanilamide containing me- Brassica head and stem, subgroup 5-A ...... 0.1 tabolites in or on the following food Brassica, leafy greens, subgroup 5B ...... 0.20 Bushberry subgroup 13–07B ...... 0.10 commodities: Caneberry subgroup 13–07A ...... 0.10 Carrot ...... 0.5 Parts per Citrus, oil ...... 0.5 Commodity million Corn, field, forage ...... 0.1 Cattle, fat ...... 0.05 Corn, field, grain ...... 0.1 Cattle, meat ...... 0.05 Corn, field, stover ...... 0.1 Cattle, meat byproducts ...... 0.2 Corn, pop, grain ...... 0.1 Goat, fat ...... 0.05 Corn, sweet, forage ...... 0.1 Goat, meat ...... 0.05 Corn, sweet, kernel plus cob with husks removed 0.1 Goat, meat byproducts ...... 0.2 Corn, sweet, stover ...... 0.1 Hog, fat ...... 0.05 Cotton, gin byproducts ...... 3.0 Hog, meat ...... 0.05 Cotton, undelinted seed ...... 0.1 Hog, meat byproducts ...... 0.2 Crayfish ...... 0.05 Horse, fat ...... 0.05 Fruit, citrus, group 10–10 ...... 0.1 Horse, meat ...... 0.05 Fruit, pome, group 11–10 ...... 0.1 Horse, meat byproducts ...... 0.2 Fruit, small vine climbing, except grape, subgroup Milk ...... 0.05 13–07E ...... 0.10 Sheep, fat ...... 0.05 Fruit, stone, group 12–12 ...... 0.1 Sheep, meat ...... 0.05 Grape ...... 0.1 Sheep, meat byproducts ...... 0.2 Grass, forage, fodder, and hay crop group 17, Sugarcane, cane ...... 1.0 forage ...... 1,000 Sugarcane, molasses ...... 30 Grass, forage, fodder, and hay crop group 17, hay ...... 2,000 (b) Section 18 emergency exemptions. Hop, dried cones ...... 0.1 Leaf petiole vegetable subgroup 22B ...... 0.2 [Reserved] Lettuce, leaf ...... 4.0 (c) Tolerances with regional registra- Melon subgroup 9A ...... 0.10 tions. [Reserved] Monarda, fresh leaves ...... 0.2 (d) Indirect or inadvertent residues. Monarda, oil ...... 1 Nut, tree, group 14–12 ...... 0.10 [Reserved] Olive ...... 0.1 [68 FR 39441, July 1, 2003, as amended at 72 Onion, bulb subgroup 3–07A ...... 0.1 Onion, green subgroup 3–07B ...... 0.2 FR 37654, July 11, 2007] Peanut ...... 0.1 Peanut, hay ...... 0.1 § 180.361 Pendimethalin; tolerances for Peas (except field peas) ...... 0.10 residues. Peppermint, oil ...... 1.0 Peppermint, tops ...... 0.2 (a)(1) General. Tolerances are estab- Pomegranate ...... 0.10 lished for residues of the herbicide Potato ...... 0.1 pendimethalin, including its metabo- Rice, grain ...... 0.1 Rosemary, fresh leaves ...... 0.2 lites and degradates, in or on the com- Rosemary, oil ...... 1 modities. Compliance with the toler- Sorghum, forage ...... 0.1

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Parts per Expiration/ Commodity million Commodity Parts per revocation million date Sorghum, grain, grain ...... 0.1 Sorghum, grain, stover ...... 0.1 Bermuda grass, forage ...... 25 12/31/10 Soybean, forage ...... 0.1 Bermuda grass, hay ...... 60 12/31/10 Soybean, hay ...... 0.1 Soybean, seed ...... 0.1 (c) Tolerances with regional registra- Spearmint, oil ...... 1.0 Spearmint, tops ...... 0.2 tions. [Reserved] Sugarcane, cane ...... 0.1 (d) Indirect or inadvertent residues. Sunflower subgroup 20B ...... 0.1 [Reserved] Turnip greens ...... 0.20 Vegetable, fruiting, group 8–10 ...... 0.1 [49 FR 15293, Apr. 18, 1984] Vegetable, soybean, succulent ...... 0.10 Wheat, grain ...... 0.10 EDITORIAL NOTE: For FEDERAL REGISTER ci- Wheat, forage ...... 3.0 tations affecting § 180.361, see the List of CFR Wheat, hay ...... 0.60 Sections Affected, which appears in the Wheat, straw ...... 0.30 Finding Aids section of the printed volume and at www.govinfo.gov. (2) Tolerances are established for residues of the herbicide pendimethalin, § 180.362 Fenbutatin-oxide; tolerances including its metabolites and for residues. degradates, in or on commodities listed (a) General. (1) Tolerances are estab- in the following table. Compliance with lished for residues of the miticide/acar- the tolerance levels is to be determined icide fenbutatin-oxide, including its by measuring only the sum of metabolites and degradates, in or on pendimethalin (N-(1-ethylpropyl)-3,4-di- the plant commodities in the table in methyl-2,6-dinitrobenzenamine)) and this paragraph. Compliance with the its metabolite, 1-(1-ethylpropyl)-5, 6-di- tolerance levels specified in this para- methyl-7-nitro-1H-benzimidazole (me- graph is to be determined by measuring tabolite 6), calculated as the stoichio- only fenbutatin-oxide, hexakis (2-meth- metric equivalent of pendimethalin, in yl-2-phenylpropyl) distannoxane, in or or on the commodity. on the commodity.

Parts Parts per Commodity per Commodity million million Almond, hulls ...... 80.0 Cattle, fat ...... 0.30 Apple ...... 15.0 Cattle, meat ...... 0.10 Apple, wet pomace ...... 100.0 Cattle, meat byproduct ...... 3.0 Cherry, sweet ...... 6.0 Goats, fat ...... 0.30 Cherry, tart ...... 6.0 Goats, meat ...... 0.10 Citrus, dried pulp ...... 100.0 Goats, meat byproduct ...... 3.0 Citrus, oil ...... 140.0 Horse, fat ...... 0.30 Cucumber ...... 4.0 Horse, meat ...... 0.10 Eggplant ...... 6.0 Horse, byproduct ...... 3.0 Fruit, citrus, group 10 ...... 20.0 Milk ...... 0.04 Grape ...... 5.0 Sheep, fat ...... 0.30 Grape, raisin ...... 20.0 Sheep, meat ...... 0.10 Nut, tree, group 14 ...... 0.5 Sheep, meat byproduct ...... 3.0 Papaya ...... 2.0 Peach ...... 10.0 (b) Section 18 emergency exemptions. Pear ...... 15.0 Time-limited tolerances specified in Pistachio ...... 0.5 Plum, prune, fresh ...... 4.0 the following table are established for Plum, prune, dried ...... 20.0 combined residues of the herbicide Strawberry ...... 10.0 pendimethalin, [N-(1-ethylpropyl)-3,4- dimethyl-2,6-dinitrobenzenamine], and (2) Tolerances are established for res- its metabolite 4-[(1- idues of the miticide/acaricide ethylpropyl)amino]-2-methyl-3,5- fenbutatin-oxide, including its metabo- dinitrobenzyl alcohol, in or on the lites and degradates, in or on the ani- specified agricultural commodities, re- mal commodities in the table in this sulting from use of the pesticide pursu- paragraph. Compliance with the toler- ant to FIFRA section 18 emergency ex- ance levels specified in this paragraph emptions. The tolerances expire and is to be determined by measuring only are revoked on the date specified in the the sum of fenbutatin-oxide, hexakis table. (2-methyl-2-phenylpropyl)

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distannoxane, and its organotin me- glyphosate, the isopropylamine salt of tabolites, dihydroxybis(2-methyl-2- glyphosate, the ethanolamine salt of phenylpropyl) stannane and 2-methyl- glyphosate, the dimethylamine salt of 2-phenylpropylstannoic acid, cal- glyphosate, the ammonium salt of culated as the stoichiometric equiva- glyphosate, and the potassium salt of lent of fenbutatin-oxide, in or on the glyphosate. Compliance with the fol- commodity. lowing tolerance levels is to be determined by measuring only glyphosate Parts per Commodity million (N-(phosphonomethyl)glycine).

Cattle, fat ...... 0.5 Commodity Parts per Cattle, meat ...... 0.5 million Cattle, meat byproducts ...... 0.5 Egg ...... 0.1 Acerola ...... 0.2 Goat, fat ...... 0.5 Alfalfa, seed ...... 0.5 Goat, meat ...... 0.5 Almond, hulls ...... 25 Goat, meat byproducts ...... 0.5 Aloe vera ...... 0.5 Hog, fat ...... 0.5 Ambarella ...... 0.2 Hog, meat ...... 0.5 Animal feed, nongrass, group 18 ...... 400 Hog, meat byproducts ...... 0.5 Artichoke, globe ...... 0.2 Horse, fat ...... 0.5 Asparagus ...... 0.5 Horse, meat ...... 0.5 Atemoya ...... 0.2 Horse, meat byproducts ...... 0.5 Avocado ...... 0.2 Milk, fat ...... 0.1 Bamboo, shoots ...... 0.2 Poultry, fat ...... 0.1 Banana ...... 0.2 Poultry, meat ...... 0.1 Barley, bran ...... 30 Poultry, meat byproducts ...... 0.1 Beet, sugar, dried pulp ...... 25 Sheep, fat ...... 0.5 Beet, sugar, roots ...... 10 Sheep, meat ...... 0.5 Beet, sugar, tops ...... 10 Sheep, meat byproducts ...... 0.5 Berry and small fruit, group 13–07 ...... 0.20 Betelnut ...... 1.0 Biriba ...... 0.2 (b) Section 18 emergency exemptions. Blimbe ...... 0.2 [Reserved] Breadfruit ...... 0.2 (c) Tolerances with regional registra- Cacao bean, bean ...... 0.2 Cactus, fruit ...... 0.5 tions. A tolerance with regional reg- Cactus, pads ...... 0.5 istration, as defined in § 180.1(l), is es- Canistel ...... 0.2 tablished for residues of the miticide/ Carrot ...... 5.0 Chaya ...... 1.0 acaricide fenbutatin-oxide, including Cherimoya ...... 0.2 its metabolites and degradates, in or Citrus, dried pulp ...... 1.5 on the plant commodity in the table in Coconut ...... 0.1 Coffee, bean, green ...... 1.0 this paragraph. Compliance with the Corn, pop, grain ...... 0.1 tolerance level specified in this para- Corn, sweet, kernel plus cob with husk removed 3.5 graph is to be determined by measuring Cotton, gin byproducts ...... 210 only fenbutatin-oxide, hexakis (2-meth- Custard apple ...... 0.2 Date, dried fruit ...... 0.2 yl-2-phenylpropyl) distannoxane, in or Dokudami ...... 2.0 on the commodity. Durian ...... 0.2 Epazote ...... 1.3 Feijoa ...... 0.2 Commodity Parts per million Fig ...... 0.2 Fish ...... 0.25 Raspberry ...... 10.0 Fruit, citrus, group 10–10 ...... 0.50 Fruit, pome, group 11–10 ...... 0.20 (d) Indirect or inadvertent residues. Fruit, stone, group 12 ...... 0.2 [Reserved] Galangal, roots ...... 0.2 Ginger, white, flower ...... 0.2 [65 FR 33713, May 24, 2000, as amended at 72 Gourd, buffalo, seed ...... 0.1 FR 41930, Aug. 1, 2007; 73 FR 5109, Jan. 29, Governor’s plum ...... 0.2 Gow kee, leaves ...... 0.2 2008; 76 FR 23494, Apr. 27, 2011] Grain, cereal, forage, fodder and straw, group 16, except field corn, forage and field corn, stover 100 § 180.364 Glyphosate; tolerances for Grain, cereal, group 15 except field corn, pop- residues. corn, rice, sweet corn, and wild rice ...... 30 Grass, forage, fodder and hay, group 17 ...... 300 (a) General. (1) Tolerances are estab- Guava ...... 0.2 lished for residues of glyphosate, in- Herbs subgroup 19A ...... 0.2 cluding its metabolites and degradates, Hop, dried cones ...... 7.0 Ilama ...... 0.2 in or on the commodities listed below Imbe ...... 0.2 resulting from the application of Imbu ...... 0.2

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Parts per Parts per Commodity million Commodity million

Jaboticaba ...... 0.2 Vegetable, leafy, brassica, group 5 ...... 0.2 Jackfruit ...... 0.2 Vegetable, leafy, except brassica, group 4 ...... 0.2 Kava, roots ...... 0.2 Vegetable, leaves of root and tuber, group 2, ex- Kenaf, forage ...... 200 cept sugar beet tops ...... 0.2 Leucaena, forage ...... 200 Vegetable, legume, group 6 except soybean and Longan ...... 0.2 dry pea ...... 5.0 Lychee ...... 0.2 Vegetables, root and tuber, group 1, except car- Mamey apple ...... 0.2 rot, sweet potato, and sugar beet ...... 0.20 Mango ...... 0.2 Wasabi, roots ...... 0.2 Mangosteen ...... 0.2 Water spinach, tops ...... 0.2 Marmaladebox ...... 0.2 Watercress, upland ...... 0.2 Mioga, flower ...... 0.2 Wax jambu ...... 0.2 Noni ...... 0.20 Yacon, tuber ...... 0.2 Nut, pine ...... 1.0 Nut, tree, group 14 ...... 1.0 (2) Tolerances are established for res- Oilseeds, group 20, except canola ...... 40 Okra ...... 0.5 idues of glyphosate, including its me- Olive ...... 0.2 tabolites and degradates, in or on the Oregano, Mexican, leaves ...... 2.0 commodities listed below resulting Palm heart ...... 0.2 Palm heart, leaves ...... 0.2 from the application of glyphosate, the Palm, oil ...... 0.1 isopropylamine salt of glyphosate, the Papaya ...... 0.2 ethanolamine salt of glyphosate, the Papaya, mountain ...... 0.2 dimethylamine salt of glyphosate, the Passionfruit ...... 0.2 Pawpaw ...... 0.2 ammonium salt of glyphosate, and the Pea, dry ...... 8.0 potassium salt of glyphosate. Compli- Peanut ...... 0.1 ance with the following tolerance lev- Peanut, hay ...... 0.5 Pepper leaf, fresh leaves ...... 0.2 els is to be determined by measuring Peppermint, tops ...... 200 only glyphosate (N- Perilla, tops ...... 1.8 (phosphonomethyl)glycine) and its me- Persimmon ...... 0.2 tabolite N-acetyl-glyphosate (N-acetyl- Pineapple ...... 0.1 Pistachio ...... 1.0 N-(phosphonomethyl)glycine; cal- Pomegranate ...... 0.2 culated as the stoichiometric equiva- Pulasan ...... 0.2 lent of glyphosate). Quinoa, grain ...... 5.0 Rambutan ...... 0.2 Parts per Rice, grain ...... 0.1 Commodity Million Rice, wild, grain ...... 0.1 Rose apple ...... 0.2 Canola, seed ...... 20 Sapodilla ...... 0.2 Cattle, meat byproducts ...... 5.0 Sapote, black ...... 0.2 Corn, field, forage ...... 13 Sapote, mamey ...... 0.2 Corn, field, grain ...... 5.0 Sapote, white ...... 0.2 Corn, field, stover ...... 100 Shellfish ...... 3.0 Egg ...... 0.05 Soursop ...... 0.2 Goat, meat byproducts ...... 5.0 Spanish lime ...... 0.2 Grain aspirated fractions ...... 310.0 Spearmint, tops ...... 200 Hog, meat byproducts ...... 5.0 Spice subgroup 19B ...... 7.0 Horse, meat byproducts ...... 5.0 Star apple ...... 0.2 Poultry, meat ...... 0.10 Starfruit ...... 0.2 Poultry, meat byproducts ...... 1.0 Stevia, dried leaves ...... 1.0 Sheep, meat byproducts ...... 5.0 Sugar apple ...... 0.2 Soybean, forage ...... 100.0 Sugarcane, cane ...... 2.0 Soybean, hay ...... 200.0 Sugarcane, molasses ...... 30 Soybean, hulls ...... 120.0 Surinam cherry ...... 0.2 Soybean, seed ...... 20.0 Sweet potato ...... 3.0 Tamarind ...... 0.2 Tea, dried ...... 1.0 (b) Section 18 emergency exemptions. Tea, instant ...... 7.0 [Reserved] Teff, forage ...... 100 (c) Tolerances with regional registra- Teff, grain ...... 5.0 tions. [Reserved] Teff, hay ...... 100 Ti, leaves ...... 0.2 (d) Indirect or inadvertent residues. Ti, roots ...... 0.2 [Reserved] Ugli fruit ...... 0.5 Vegetable, bulb, group 3–07 ...... 0.20 [45 FR 64911, Oct. 1, 1980] Vegetable, cucurbit, group 9 ...... 0.5 Vegetable, foliage of legume, subgroup 7A, ex- EDITORIAL NOTE: For FEDERAL REGISTER ci- cept soybean ...... 0.2 tations affecting § 180.364, see the List of CFR Vegetable, fruiting, group 8–10 (except okra) ...... 0.10 Sections Affected, which appears in the

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Finding Aids section of the printed volume Parts per and at www.govinfo.gov. Commodity million

§ 180.367 n-Octyl bicycloheptenedi- Corn, field, grain ...... 0.10 Corn, field, stover ...... 6.0 carboximide; tolerances for resi- Corn, pop, grain ...... 0.10 dues. Corn, pop, stover ...... 6.0 (a) General. A tolerance of 5 parts per Corn, sweet, forage ...... 6.0 Corn, sweet, kernel plus cob with husks removed 0.10 million is established for residues of Corn, sweet, stover ...... 6.0 the insecticide synergist N-octyl Cotton, gin byproducts ...... 4.0 bicycloheptene dicarboximide, includ- Cotton, undelinted seed ...... 0.10 Dillweed ...... 0.50 ing its metabolites and degradates, in Egg ...... 0.02 or on all food items in food handling Goat, fat ...... 0.02 establishments where food and food Goat, kidney ...... 0.20 Goat, liver ...... 0.05 products are held, processed, prepared Goat, meat ...... 0.02 and/or served, provided that the food is Goat, meat byproducts, except kidney and liver ... 0.04 removed or covered prior to such use, Grass, forage ...... 10 Grass, hay ...... 0.20 except for bagged food in warehouse Horse, fat ...... 0.02 storage which need not be removed or Horse, kidney ...... 0.20 covered prior to applications of formu- Horse, liver ...... 0.05 lations containing N-octyl Horse, meat ...... 0.02 Horse, meat byproducts, except kidney and liver 0.04 bicycloheptene dicarboximide. Compli- Milk ...... 0.02 ance with the tolerance level specified Nut, tree, group 14 ...... 0.10 in this paragraph is to be determined Okra ...... 0.50 Peanut ...... 0.20 by measuring only N-octyl Peanut, hay ...... 20 bicycloheptene dicarboximide, in or on Peanut, meal ...... 0.40 the commodity. Potato ...... 0.20 Poultry, fat ...... 0.02 (b) Section 18 emergency exemptions. Poultry, meat ...... 0.02 [Reserved] Poultry, meat byproducts ...... 0.05 (c) Tolerances with regional registra- Safflower, seed ...... 0.10 tions. [Reserved] Sheep, fat ...... 0.02 Sheep, kidney ...... 0.20 (d) Indirect or inadvertent residues. Sheep, liver ...... 0.05 [Reserved] Sheep, meat ...... 0.02 Sheep, meat byproducts, except kidney and liver 0.04 [65 FR 33713, May 24, 2000, as amended at 75 Sorghum, grain, forage ...... 1.0 FR 60243, Sept. 29, 2010] Sorghum, grain, grain ...... 0.30 Sorghum, grain, stover ...... 4.0 § 180.368 Metolachlor; tolerances for Soybean, forage ...... 5.0 Soybean, hay ...... 8.0 residues. Soybean, seed ...... 0.20 (a) General. (1) Tolerances are estab- Tomato ...... 0.10 lished for the combined residues (free Vegetable, foliage of legume, subgroup 7A, except soybean ...... 15.0 and bound) of the herbicide Vegetable, legume, group 6 ...... 0.30 metolachlor, 2-chloro-N-(2- ethyl-6- methylphenyl)-N-(2-methoxy-1- (2) Tolerances are established for res- methylethyl)acetamide, and its me- idues of S-metolachlor, including its tabolites, determined as the deriva- metabolites and degradates, in or on tives, 2- [(2-ethyl-6- the commodity(s), as defined. Compli- methylphenyl)amino]-1-propanol and 4- ance with the tolerance levels specified (2-ethyl-6-methylphenyl)-2- hydroxy-5- in the following table below is to be demethyl-3-morpholinone, each expressed termined by measuring only the sum of as the parent compound in the fol- free and bound S-metolachlor, S-2- lowing raw agricultural commodities: chloro-N-(2-ethyl-6-methylphenyl)-N- (2-methoxy-1-methylethyl)acetamide, Parts per Commodity million its R-enantiomer, and its metabolites, determined as the derivatives, 2-(2- Almond, hulls ...... 0.30 ethyl-6-methylphenyl)amino-1-pro- Animal feed, nongrass, group 18 ...... 1.0 Cattle, fat ...... 0.02 panol and 4-(2-ethyl-6-methylphenyl)-2- Cattle, kidney ...... 0.20 hydroxy-5-methyl-3-morpholinone, cal- Cattle, liver ...... 0.05 culated as the stoichiometric equiva- Cattle, meat ...... 0.02 Cattle, meat byproducts, except kidney and liver 0.04 lent of S-metolachlor, in or on the Corn, field, forage ...... 6.0 commodity.

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Parts per Parts per Commodity million Commodity million

Beet, sugar, molasses ...... 2.0 Sunflower subgroup 20B ...... 1.0 Beet, sugar, roots ...... 0.5 Swiss chard ...... 0.15 Beet, sugar, tops ...... 15.0 Tomato, paste ...... 0.30 Brassica, leafy greens, subgroup 4–16B ...... 1.8 Vegetable, Brassica, head and stem, group 5–16 0.60 Bushberry subgroup 13-07B ...... 0.15 Vegetable, cucurbit group 9 ...... 0.50 Caneberry subgroup 13-07A ...... 0.10 Carrot, roots ...... 0.40 Vegetable, foliage of legume, except soybean, Cattle, fat ...... 0.02 subgroup 7A ...... 15.0 Cattle, kidney ...... 0.20 Vegetable, fruiting, group 8–10, except tabasco Cattle, liver ...... 0.05 pepper ...... 0.10 Cattle, meat ...... 0.02 Vegetable, leaves of root and tuber, group 2, ex- Cattle, meat byproducts, except kidney and liver 0.04 cept sugar beet ...... 2.0 Cilantro, leaves ...... 8.0 Vegetable, legume, group 6 ...... 0.30 Coriander, seed ...... 0.13 Vegetable, root, except sugar beet, subgroup 1B, Corn, field, forage ...... 40 except carrot ...... 0.30 Corn, field, grain ...... 0.10 Vegetable, tuberous and corm, subgroup 1C ...... 0.20 Corn, field, stover ...... 40 Corn, pop, grain ...... 0.10 Corn, pop, stover ...... 40 (b) Section 18 emergency exemptions. Corn, sweet, forage ...... 40 [Reserved] Corn, sweet, kernel plus cob with husks removed 0.10 Corn, sweet, stover ...... 40 (c) Tolerances with regional registra- Cotton, gin byproducts ...... 4.0 tions. (1) Tolerances with regional reg- Cottonseed subgroup 20C ...... 0.10 istration as defined in 180.1(l) are es- Egg ...... 0.02 Grain, aspirated fractions ...... 0.70 tablished for the combined residues Goat, fat ...... 0.02 (free and bound) of the herbicide Goat, kidney ...... 0.20 metolachlor [2-chloro-N-(2-ethyl-6- Goat, liver ...... 0.05 Goat, meat ...... 0.02 methylphenyl)-N-(2-methoxy-1- Goat, meat byproducts, except kidney and liver ... 0.04 methylethyl)acetamide] and its me- Grass, forage ...... 10.0 tabolites, determined as the deriva- Grass, hay ...... 0.20 Horse, fat ...... 0.02 tives, 2-[2-ethyl-6- Horse, kidney ...... 0.20 methylphenyl)amino]-1-propanol and 4- Horse, liver ...... 0.05 (2-ethyl-6-methylphenyl)-2-hydroxy-5- Horse, meat ...... 0.02 Horse, meat byproducts, except kidney and liver 0.04 methyl-3-morpholinone, each expressed Kohlrabi ...... 0.60 as the parent compound, in or on the Leaf petiole vegetable subgroup 22B ...... 0.10 following raw agricultural commod- Lettuce ...... 1.5 Low growing berry subgroup 13–07G, except ities: cranberry ...... 0.40 Milk ...... 0.02 Commodity Parts per Onion, bulb, subgroup 3-07A ...... 0.10 million Onion, green, subgroup 3-07B ...... 2.0 Peanut ...... 0.20 Pepper, nonbell ...... 0.50 Peanut, hay ...... 20.0 Peanut, meal ...... 0.40 (2) Tolerances with regional registra- Poultry, fat ...... 0.02 tion are established for residues of S- Poultry, meat ...... 0.02 Poultry, meat byproducts ...... 0.05 metolachlor, including its metabolites Safflower, seed ...... 0.10 and degradates, in or on the commod- Sesame, seed ...... 0.13 ities identified in the following table Sheep, fat ...... 0.02 Sheep, kidney ...... 0.20 below. Compliance with the tolerance Sheep, liver ...... 0.05 levels specified in the following table Sheep, meat ...... 0.02 below is to be determined by measuring Sheep, meat byproducts, except kidney and liver 0.04 Sorghum, grain, forage ...... 1.0 only the sum of free and bound S- Sorghum, grain, grain ...... 0.3 metolachlor, S-2-chloro-N-(2-ethyl-6- Sorghum, grain, stover ...... 4.0 methylphenyl)-N-(2-methoxy-1- Sorghum, sweet, stalk ...... 4.0 Soybean, forage ...... 5.0 methylethyl)acetamide, its R- Soybean, hay ...... 8.0 enantiomer, and its metabolites, deter- Soybean, seed ...... 0.20 mined as the derivatives, 2-(2-ethyl-6- Spinach ...... 0.50 Stalk and stem vegetable subgroup 22A, except methylphenyl)amino-1-propanol and 4- kohlrabi ...... 0.10 (2-ethyl-6-methylphenyl)-2-hydroxy-5- Stevia, dried leaves ...... 15 methyl-3-morpholinone, calculated as Sugarcane, cane ...... 0.20 Sugarcane, molasses ...... 1.5 the stoichiometric equivalent of S- Sunflower, meal ...... 1.0 metolachlor, in or on the commodity.

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Parts per Parts per Commodity million Commodity million

Pepper, tabasco ...... 0.50 Animal feed, nongrass, group 18 ...... 1.0 Barley, grain ...... 0.10 Barley, hay ...... 0.50 (d) Indirect or inadvertent residues. (1) Barley, straw ...... 0.50 Tolerances are established for the indi- Buckwheat, grain ...... 0.10 rect or inadvertent combined residues Millet, forage ...... 0.50 Millet, grain ...... 0.10 (free and bound) of the herbicide Millet, hay ...... 0.50 metolachlor, 2-chloro-N-(2-ethyl-6- Millet, straw ...... 0.50 methylphenyl)-N-(2-methoxy-1- Oat, forage ...... 0.50 Oat, grain ...... 0.10 methylethyl)acetamide, and its me- Oat, hay ...... 0.50 tabolites, determined as the deriva- Oat, straw ...... 0.50 tives, 2-[(2-ethyl-6- Rice, grain ...... 0.10 Rye, forage ...... 0.50 methylphenyl)amino]-1-propanol and 4- Rye, grain ...... 0.10 (2-ethyl-6-methylphenyl)-2- hydroxy-5- Rye, straw ...... 0.50 methyl-3-morpholinone, each expressed Wheat, forage ...... 0.50 Wheat, grain ...... 0.10 as the parent compound in the fol- Wheat, hay ...... 0.50 lowing raw agricultural commodities: Wheat, straw ...... 0.50

Parts per Commodity million [73 FR 53740, Sept. 17, 2008, as amended at 74 FR 48412, Sept. 23, 2009; 75 FR 56903, Sept. 17, Animal feed, nongrass, group 18 ...... 1.0 2010; 77 FR 48906, Aug. 15, 2012; 77 FR 59127, Barley, grain ...... 0.10 Sept. 26, 2012; 79 FR 17441, Mar. 28, 2014; 80 FR Barley, hay ...... 0.80 38986, July 8, 2015; 83 FR 12274, Mar. 21, 2018; Barley, straw ...... 0.80 84 FR 8617, Mar. 11, 2019] Buckwheat, grain ...... 0.10 Millet, forage ...... 0.50 § 180.370 5-Ethoxy-3-(trichloromethyl)- Millet, grain ...... 0.10 1,2,4-thiadiazole; tolerances for resi- Millet, hay ...... 0.80 Millet, straw ...... 0.80 dues. Oat, forage ...... 0.50 (a) General. Tolerances are estab- Oat, grain ...... 0.10 lished for residues of the fungicide 5- Oat, hay ...... 0.80 ethoxy-3-(trichloromethyl)-1,2,4- Oat, straw ...... 0.80 Rice, grain ...... 0.10 thiadiazole and its monoacid metabo- Rye, forage ...... 0.50 lite 3-carboxy-5-ethoxy-1,2,4- Rye, grain ...... 0.10 thiadiazole in or on the following raw Rye, straw ...... 0.80 agricultural commodities: Wheat, forage ...... 0.50 Wheat, grain ...... 0.10 Commodity Parts per Wheat, hay ...... 0.80 million Wheat, straw ...... 0.80 Cotton, gin byproducts ...... 0.1 Cotton, undelinted seed ...... 0.1 (2) Tolerances for are established for Tomato ...... 0.15 the indirect or inadvertent residues of S-metolachlor, including its metabo- (b) Section 18 emergency exemptions. lites and degradates, in or on the com- [Reserved] modities identified in the following (c) Tolerances with regional registra- table below. Compliance with the toler- tions. [Reserved] ance levels specified in the following (d) Indirect or inadvertent residues. table below is to be determined by [Reserved] measuring only the sum of free and [47 FR 49845, Nov. 3, 1982, as amended at 48 bound S-metolachlor, S-2-chloro-N-(2- FR 12088, Mar. 23, 1983; 63 FR 57076, Oct. 26, ethyl-6-methylphenyl)-N-(2-methoxy-1- 1998; 72 FR 41931, Aug. 1, 2007; 73 FR 54961, methylethyl)acetamide, its R- Sept. 24, 2008; 81 FR 34905, June 1, 2016] enantiomer, and its metabolites, determined as the derivatives, 2-(2-ethyl-6- § 180.371 Thiophanate-methyl; toler- methylphenyl)amino-1-propanol and 4- ances for residues. (2-ethyl-6-methylphenyl)-2-hydroxy-5- (a) General. Tolerances are estab- methyl-3-morpholinone, calculated as lished for residues of thiophanate- the stoichiometric equivalent of S- methyl, dimethyl ((1,2-phenylene) bis metolachlor, in or on the commodity. (iminocarbonothioyl)) bis(carbamate),

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including its metabolites and metric equivalent of thiophanate- degradates, in or on the commodities methyl, in or on the commodity. in the following table. Compliance with Parts per the tolerance levels specified in this Commodity million paragraph is to be determined by measuring only the sum of thiophanate- Canola, seed ...... 0.1 methyl, dimethyl ((1,2-phenylene) bis (iminocarbonothioyl)) bis(carbamate), (d) Indirect or inadvertent residues. and its metabolite, methyl 2- [Reserved] benzimidazoyl carbamate (MBC), cal- [75 FR 60244, Sept. 29, 2010] culated as the stoichiometric equivalent of thiophanate-methyl, in or on § 180.372 2,6-Dimethyl-4- the commodity. tridecylmorpholine; tolerances for residues. Parts per (a) General. A tolerance is established Commodity million for residues of the fungicide 2,6-di- Almond ...... 0.1 methyl-4-tridecylmorpholine in or on Almond, hulls ...... 0.5 the following food commodity: Apple ...... 2.0 Apricot ...... 15.0 Parts per Banana ...... 2.0 Commodity million Bean, dry, seed ...... 0.2 Bean, snap, succulent ...... 2.0 Banana 1 ...... 1.0 Beet, sugar, roots ...... 0.2 1 There are no U.S. registrations. Cherry, sweet ...... 20.0 Cherry, tart ...... 20.0 (b) Section 18 emergency exemptions. Grain, aspirated fractions ...... 12 [Reserved] Grape ...... 5.0 Onion, bulb ...... 0.5 (c) Tolerances with regional registra- Onion, green ...... 3.0 tions. [Reserved] Peach ...... 3.0 (d) Indirect or inadvertent residues. Peanut ...... 0.1 [Reserved] Peanut, hay ...... 5.0 Pear ...... 3.0 [73 FR 54961, Sept. 24, 2008] Pecan ...... 0.1 Pistachio ...... 0.1 § 180.373 [Reserved] Plum ...... 0.5 Potato ...... 0.1 Soybean, hulls ...... 1.5 § 180.377 Diflubenzuron; tolerances for Soybean, seed ...... 0.2 residues. Strawberry ...... 7.0 (a) General. (1) Tolerances are estab- Vegetable, cucurbit, group 9 ...... 1.0 Wheat, forage ...... 1.1 lished for residues of diflubenzuron, in- Wheat, grain ...... 0.1 cluding its metabolites and degradates, Wheat, hay ...... 0.1 in or on the commodities in the table Wheat, straw ...... 0.1 below. Compliance with the tolerance levels specified below is to be deter- (b) Section 18 emergency exemptions. mined by measuring only diflubenzuron [Reserved] (N-[[(4-chlorophenyl)amino]carbonyl]- (c) Tolerances with regional registra- 2,6-difluorobenzamide). tions. A tolerance with a regional registration is established for residues of Commodity Parts per thiophanate-methyl, dimethyl ((1,2- million phenylene) bis(iminocarbonothioyl)) Artichoke, globe ...... 6.0 bis(carbamate), including its metabo- Cattle, fat ...... 0.05 lites and degradates, in or on the com- Cattle, meat ...... 0.05 Cottonseed subgroup 20C ...... 0.20 modity in the following table. Compli- Egg ...... 0.07 ance with the tolerance level specified Goat, fat ...... 0.05 in this paragraph is to be determined Goat, meat ...... 0.05 Hog, fat ...... 0.05 by measuring only the sum of Hog, meat ...... 0.05 thiophanate-methyl, dimethyl ((1,2- Horse, fat ...... 0.05 phenylene) bis (iminocarbonothioyl)) Horse, meat ...... 0.05 bis(carbamate), and its metabolite, Milk ...... 0.05 Mushroom ...... 0.2 methyl 2-benzimidazoyl carbamate Poultry, fat ...... 0.10 (MBC), calculated as the stoichio- Poultry, meat byproducts ...... 0.08

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with the tolerance levels specified Commodity Parts per million below is to be determined by measuring Poultry, meat ...... 0.05 only the sum of diflubenzuron (N-[[(4- Sheep, fat ...... 0.05 chlorophenyl)amino]carbonyl]-2,6- Sheep, meat ...... 0.05 difluorobenzamide), 4- Soybean ...... 0.05 Soybean, hulls ...... 0.5 chlorophenylyurea and 4-chloroaniline, calculated as the stoichiometric equiv- (2) Tolerances are established for res- alent of diflubenzuron, in or on the idues of the insecticide diflubenzuron commodity. The tolerances are speci- (N-[[(4-chlorophenyl)amino]carbonyl]- fied in the following table, and will ex- 2,6-difluorobenzamide), in or on the pire and are revoked on the dates speci- commodities in the table below. Com- fied. pliance with the tolerance levels speci- Expiration/ fied below is to be determined by meas- Parts per Commodity million revocation uring only the sum of diflubenzuron (N- date [[(4-chlorophenyl)amino]carbonyl]-2,6- Alfalfa, forage ...... 6.0 12/31/17 difluorobenzamide), 4- Alfalfa, hay ...... 6.0 12/31/17 chlorophenylyurea and 4-chloroaniline, Lemon ...... 0.8 12/31/10 calculated as the stoichiometric equiv- (c) Tolerances with regional registra- alent of diflubenzuron, in or on the tions. Tolerances with regional reg- commodity. istration are established for residues of the insecticide diflubenzuron (N-[[(4- Commodity Parts per million chlorophenyl)amino]carbonyl]-2,6- Almond, hulls ...... 6.0 difluorobenzamide), in or on the com- Barley, grain ...... 0.06 modities in the table below. Compli- Barley, hay ...... 3.0 ance with the tolerance levels specified Barley, straw ...... 1.8 Brassica, leafy greens, subgroup 5B ...... 9.0 below is to be determined by measuring Carrot, roots ...... 0.20 only the sum of diflubenzuron (N-[[(4- Cattle, meat byproducts ...... 0.15 chlorophenyl)amino]carbonyl]-2,6- Citrus, oil ...... 32 Fruit, citrus, group 10–10 ...... 3.0 difluorobenzamide), 4- Goat, meat byproducts ...... 0.15 chlorophenylyurea and 4-chloroaniline, Grain, aspirated fractions ...... 11 calculated as the stoichiometric equiv- Grass, forage, fodder, and hay, group 17 ...... 6.0 Hog, meat byproducts ...... 0.15 alent of diflubenzuron, in or on the Horse, meat byproducts ...... 0.15 commodity. Oat, forage ...... 7.0 Oat, grain ...... 0.06 Commodity Parts per Oat, hay ...... 6.0 million Oat, straw ...... 3.5 Peanut ...... 0.10 Alfalfa, forage ...... 6.0 Peanut, hay ...... 55 Alfalfa, hay ...... 20 Peanut, refined oil ...... 0.20 Alfalfa, seed ...... 0.90 Peach subgroup 12–12B ...... 0.50 Pear ...... 0.50 (d) Indirect or inadvertent residues. Pepper/Eggplant subgroup 8–10B ...... 1.0 Plum Subgroup 12–12C ...... 0.50 [Reserved] Nut, tree, group 14–12 ...... 0.20 Rice, grain ...... 0.02 [65 FR 33699, May 24, 2000] Sheep, meat byproducts ...... 0.15 EDITORIAL NOTE: For FEDERAL REGISTER ci- Turnip greens ...... 9.0 tations affecting § 180.377, see the List of CFR Wheat, forage ...... 7.0 Wheat, grain ...... 0.06 Sections Affected, which appears in the Wheat, hay ...... 6.0 Finding Aids section of the printed volume Wheat, straw ...... 3.5 and at www.govinfo.gov.

(b) Section 18 emergency exemptions. § 180.378 Permethrin; tolerances for Time-limited tolerances are estab- residues. lished for residues of the insecticide (a) General. Tolerances are estab- diflubenzuron (N-[[(4- lished for the combined residues of the chlorophenyl)amino]carbonyl]-2,6- insecticide cis- and trans-permethrin difluorobenzamide) and its metabo- isomers [cis-(3-phenoxyphenyl)methyl lites, in connection with use of the pes- 3-(2,2-dichloroethenyl)-2,2- ticide under section 18 emergency ex- dimethylcyclopropane carboxylate] emptions granted by EPA. Compliance and [trans-(3-phenoxyphenyl)methyl 3-

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(2,2-dichloroethenyl)-2,2- istration, as defined in § 180.1(l) are es- dimethylcyclopropane carboxylate] in/ tablished for the combined residues of on the following food commodities: the insecticide cis- and trans- permethrin isomers [cis-(3- Parts per Commodity million phenoxyphenyl)methyl 3-(2,2- dichloroethenyl)-2,2- Alfalfa, forage ...... 20 dimethylcyclopropane carboxylate] Alfalfa, hay ...... 45 Almond ...... 0.05 and [trans-(3-phenoxyphenyl)methyl 3- Almond, hulls ...... 20 (2,2-dichloroethenyl)-2,2- Artichoke, globe ...... 5.0 dimethylcyclopropane carboxylate] in/ Asparagus ...... 2.0 Avocado ...... 1.0 on the following food commodities: Broccoli ...... 2.0 Brussels sprouts ...... 1.0 Commodity Parts per Cabbage ...... 6.0 million Cattle, fat ...... 1.5 Cattle, meat ...... 0.10 Collards ...... 15 Cattle, meat byproducts ...... 0.10 Grass, forage ...... 15 Cauliflower ...... 0.5 Grass, hay ...... 15 Cherry, sweet ...... 4.0 Papaya ...... 1.0 Turnip, tops ...... 10 Cherry, tart ...... 4.0 Turnip, roots ...... 0.20 Corn, field, forage ...... 50 Corn, field, grain ...... 0.05 Corn, field, stover ...... 30 (d) Indirect or inadvertent residues. Corn, pop, grain ...... 0.05 [Reserved] Corn, pop, stover ...... 30 Corn, sweet, forage ...... 50 [72 FR 52019, Sept. 12, 2007] Corn, sweet, kernel plus cob with husks removed 0.10 Corn, sweet, stover ...... 30 § 180.380 Vinclozolin; tolerances for Egg ...... 0.10 Eggplant ...... 0.50 residues. Fruit, pome, group 11 ...... 0.05 (a) General. Tolerances are estab- Garlic, bulb ...... 0.10 Grain, aspirated fractions ...... 0.50 lished for the combined residues of the Goat, fat ...... 1.5 fungicide vinclozolin (3-(3,5- Goat, meat ...... 0.10 dichlorophenyl)-5-ethenyl-5-methyl-2,4- Goat, meat byproducts ...... 0.10 oxazolidinedione) and its metabolites Hazelnut ...... 0.05 Hog, fat ...... 0.05 containing the 3,5-dichloroaniline moi- Hog, meat ...... 0.05 ety in or on the food commodities in Hog, meat byproducts ...... 0.05 the table below. There are no U.S. reg- Horse, fat ...... 1.5 Horse, meat ...... 0.10 istrations for grape (wine) as of July Horse, meat byproducts ...... 0.10 30, 1997. Horseradish ...... 0.50 Kiwifruit ...... 2.0 Parts per Expiration/ Leaf petioles subgroup 4B ...... 5.0 Commodity million Revocation Leafy greens subgroup 4A ...... 20 Date Lettuce, head ...... 20 Milk, fat (reflecting 0.88 ppm in whole milk) ...... 3.0 Bean, succulent ...... 2.0 11/30/05 Mushroom ...... 5.0 Canola, seed ...... 1.0 11/30/08 Onion, bulb ...... 0.10 Cattle, fat ...... 0.05 11/30/08 Peach ...... 1.0 Cattle, meat ...... 0.05 11/30/08 Pepper, bell ...... 0.50 Cattle, meat byproducts ...... 0.05 11/30/08 Pistachio ...... 0.10 Egg ...... 0.05 11/30/08 Potato ...... 0.05 Goat, fat ...... 0.05 11/30/08 Poultry, fat ...... 0.15 Goat, meat ...... 0.05 11/30/08 Poultry, meat ...... 0.05 Goat, meat byproducts ...... 0.05 11/30/08 Poultry, meat byproducts ...... 0.05 Grape, wine ...... 6. 0 None Sheep, fat ...... 1.5 Hog, fat ...... 0.05 11/30/08 Sheep, meat ...... 0.10 Hog, meat ...... 0.05 11/30/08 Sheep, meat byproducts ...... 0.10 Hog, meat byproducts ...... 0.05 11/30/08 Soybean, seed ...... 0.05 Horse, fat ...... 0.05 11/30/08 Spinach ...... 20 Horse, meat ...... 0.05 11/30/08 Tomato ...... 2.0 Horse, meat byproducts ...... 0.05 11/30/08 Vegetable, cucurbit, group 9 ...... 1.5 Lettuce, head ...... 10.0 11/30/05 Walnut ...... 0.05 Lettuce, leaf ...... 10.0 11/30/05 Watercress ...... 5.0 Milk ...... 0.05 11/30/08 Poultry, fat ...... 0.1 11/30/08 Poultry, meat ...... 0.1 11/30/08 (b) Section 18 emergency exemptions. Poultry, meat byproducts ...... 0.1 11/30/08 [Reserved] Sheep, fat ...... 0.05 11/30/08 (c) Tolerances with regional registra- Sheep, meat ...... 0.05 11/30/08 tions. Tolerances with regional reg- Sheep, meat byproducts ...... 0.05 11/30/08

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(b) Section 18 emergency exemptions. Commodity Parts per [Reserved] million (c) Tolerances with regional registra- Horse, meat byproducts ...... 0.01 tions. [Reserved] Horseradish ...... 0.05 (d) Indirect or inadvertent residues. Kiwifruit ...... 0.05 Milk ...... 0.01 [Reserved] Nut, tree, group 14 ...... 0.05 (e) Revoked tolerances subject to the Olive ...... 0.05 channel of trade provisions. The fol- Onion, bulb ...... 0.05 Peppermint, tops ...... 0.05 lowing table lists commodities with Persimmon ...... 0.05 residues of vinclozolin resulting from Pistachio ...... 0.05 lawful use are subject to the channels Pomegranate ...... 0.05 of trade provisions of section 408(l)(5) Poultry, fat ...... 0.2 Poultry, meat ...... 0.01 of the FFDCA: Poultry, meat byproducts ...... 0.01 Sheep, fat ...... 0.01 Commodity Parts per Sheep, meat ...... 0.01 million Sheep, meat byproducts ...... 0.01 Soybean ...... 0.05 Cucumber ...... 1 .0 Spearmint, tops ...... 0.05 Fruit, stone, except plum, prune, fresh ...... 25.0 Pepper, bell ...... 3 .0 Strawberry ...... 10.0 (b) Section 18 emergency exemptions. [Reserved] [62 FR 38474, July 18, 1997, as amended at 63 (c) Tolerances with regional registra- FR 7308, Feb. 13, 1998; 65 FR 44468, July 18, tions. Tolerances with regional reg- 2000; 67 FR 40189, June 12, 2002; 68 FR 56189, istration are established for residues of Sept. 30, 2003; 68 FR 69323, Dec. 12, 2003; 70 FR the herbicide oxyfluorfen [2-chloro-1-(3- 55268, Sept. 21, 2005] ethoxy-4-nitrophenoxy)-4- (trifluoromethyl)benzene] in or on the § 180.381 Oxyfluorfen; tolerances for following food commodities: residues.

(a) General. Tolerances are estab- Commodity Parts per lished for residues of the herbicide million oxyfluorfen [2-chloro-1-(3-ethoxy-4- Blackberry ...... 0.05 nitrophenoxy)-4- Chickpea, seed ...... 0.05 Grass, forage ...... 0.05 (trifluoromethyl)benzene] in or on the Grass, hay ...... 0.05 following food commodities: Grass, seed screenings ...... 0.05 Guava ...... 0.05 Commodity Parts per Papaya ...... 0.05 million Raspberry ...... 0.05 Taro, corm ...... 0.05 Almond, hulls ...... 0.1 Taro, leaves ...... 0.05 Artichoke, globe ...... 0.05 Avocado ...... 0.05 Banana ...... 0.05 (d) Indirect or inadvertent residues. Broccoli ...... 0.05 [Reserved] Cabbage ...... 0.05 Cacao bean, dried bean ...... 0.05 [45 FR 85022, Dec. 24, 1980] Cattle, fat ...... 0.01 Cattle, meat ...... 0.01 EDITORIAL NOTE: For FEDERAL REGISTER ci- Cattle, meat byproducts ...... 0.01 tations affecting § 180.381, see the List of CFR Cauliflower ...... 0.05 Sections Affected, which appears in the Coffee, bean, green ...... 0.05 Finding Aids section of the printed volume Corn, field, grain ...... 0.05 and at www.govinfo.gov. Cotton, undelinted seed ...... 0.05 Date, dried fruit ...... 0.05 Egg ...... 0.03 § 180.383 Sodium salt of acifluorfen; Feijoa ...... 0.05 tolerances for residues. Fig ...... 0.05 Fruit, pome, group 11 ...... 0.05 (a) General. Tolerances are estab- Fruit, stone, group 12 ...... 0.05 lished for combined residues of the her- Goat, fat ...... 0.01 bicide sodium salt of acifluorfen, so- Goat, meat ...... 0.01 dium 5-[2-chloro-4- Goat, meat byproducts ...... 0.01 Grape ...... 0.05 (trifluoromethyl)phenoxy]-2- Hog, fat ...... 0.01 nitrobenzoate, and its metabolites (the Hog, meat ...... 0.01 corresponding acid, methyl ester, and Hog, meat byproducts ...... 0.01 Horse, fat ...... 0.01 amino analogues) in or on the fol- Horse, meat ...... 0.01 lowing raw agricultural commodities:

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and its metabolites, 2-[4-(2,4- Commodity Parts per million dichlorophenoxy)phenoxy]propanoic Peanut ...... 0.1 acid and 2-[4-(2,4-dichloro-5- Rice, grain ...... 0.1 hydroxyphenoxy)phenoxy]propanoic Soybean, seed ...... 0.1 acid, in or on the following raw agri- Strawberry ...... 0.05 cultural commodities:

(b) Section 18 emergency exemptions. Parts per [Reserved] Commodity million (c) Tolerances with regional restric- Barley, grain ...... 0.1 tions. [Reserved] Barley, straw ...... 0.1 (d) Indirect or inadvertent residues. Wheat, grain ...... 0.1 [Reserved] Wheat, straw ...... 0.1

[45 FR 24877, Apr. 11, 1980, as amended at 46 (b) Section 18 emergency exemptions. FR 61272, Dec. 16, 1981; 47 FR 39490, Sept. 8, 1982; 61 FR 30165, June 14, 1996; 62 FR 39974, [Reserved] July 25, 1997; 67 FR 35048, May 17, 2002; 69 FR (c) Tolerances with regional registra- 6567, Feb. 11, 2004; 71 FR 54434, Sept. 15, 2006; tions. [Reserved] 80 FR 72598, Nov. 20, 2015] (d) Indirect or inadvertent residues. [Reserved] § 180.384 Mepiquat (N,N-dimethylpiperidinium); tolerances for residues. [45 FR 23425, Apr. 7, 1980, as amended at 50 FR 20211, May 15, 1985; 51 FR 3599, Jan. 29, (a) General. Tolerances are estab- 1986; 51 FR 19176, May 28, 1986; 63 FR 57077, lished for residues of the plant growth Oct. 26, 1998; 72 FR 41931, Aug. 1, 2007] regulator mepiquat, including its metabolites and degradates, in or on the §§ 180.388–180.389 [Reserved] commodities in the table in this paragraph. Compliance with the tolerance § 180.390 Tebuthiuron; tolerances for levels specified in this paragraph is to residues. be determined by measuring only (a) General. (1) Tolerances are estab- mepiquat, N,N-dimethylpiperidinium, lished for the combined residues of the in or on the commodity. herbicide tebuthiuron (N-(5-(1,1- dimethylethyl)-1,3,4-thiadiazol-2-yl)- Parts Commodity per mil- N,N’-dimethylurea) and its metabolites lion N-(5-(2-hydroxy-1,1-dimethylethyl)- Cattle, meat byproducts ...... 0.1 1,3,4-thiadiazol-2-yl)-N,N’- Cotton, gin byproducts ...... 6.0 dimethylurea, N-(5-(1,1-dimethylethyl)- Cotton, undelinted seed ...... 2.0 1,3,4-thiadiazol-2-yl)-N-methylurea, and Goat, meat byproducts ...... 0.1 Grape ...... 1.0 N-(5-(1,1-dimethylethyl)-1,3,4- Grape, raisin ...... 5.0 thiadiazol-2-yl)-N’-hydroxymethyl-N- Hog, meat byproducts ...... 0.1 methylurea in or on the following raw Horse, meat byproducts ...... 0.1 Sheep, meat byproducts ...... 0.1 agricultural commodities: Parts per (b) Section 18 emergency exemptions. Commodity million [Reserved] (c) Tolerances with regional registra- Grass, forage ...... 10.0 Grass, hay ...... 10.0 tions. [Reserved] (d) Indirect or inadvertent residues. (2) Tolerances are established for the [Reserved] combined residues of the herbicide [67 FR 3118, Jan. 23, 2002, as amended at 80 tebuthiuron (N-(5-(1,1-dimethylethyl)- FR 72598, Nov. 20, 2015] 1,3,4-thiadiazol-2-yl)-N,N’- dimethylurea) and its metabolites N-(5- § 180.385 Diclofop-methyl; tolerances (1,1-dimethylethyl)-1,3,4-thiadiazol-2- for residues. yl)-N-methylurea, N-(5-(1,1- (a) General. Tolerances are estab- dimethylethyl)-1,3,4-thiadiazol-2- lished for the combined residues of the yl)urea, 2-dimethylethyl-5-amino-1,3,4- herbicide diclofop-methyl (methyl 2-[4- thiadiazole, and N-(5-(1,1- (2,4- dimethylethyl)-1,3,4-thiadiazol-2-yl)-N’- dichlorophenoxy)phenoxy]propanoate) hydroxymethyl-N-methylurea in or on

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the following raw agricultural com- Commodity Parts per modities: million Grass, hay ...... 2 .0 Parts per Commodity million Pineapple ...... 0.05 Cattle, fat ...... 1.0 (b) Section 18 emergency exemptions. Cattle, meat ...... 1.0 Cattle, meat byproducts ...... 5.0 [Reserved] Goat, fat ...... 1.0 (c) Tolerances with regional registra- Goat, meat ...... 1.0 tions. [Reserved] Goat, meat byproducts ...... 5.0 Horse, fat ...... 1.0 (d) Indirect or inadvertent residues. Horse, meat ...... 1.0 [Reserved] Horse, meat byproducts ...... 5.0 Sheep, fat ...... 1.0 [45 FR 55198, Aug. 19, 1980, as amended at 63 Sheep, meat ...... 1.0 FR 10543, Mar. 4, 1998; 63 FR 65073, Nov. 25, Sheep, meat byproducts ...... 5.0 1998; 66 FR 28672, May 24, 2001; 68 FR 37764, June 25, 2003; 68 FR 48312, Aug. 13, 2003; 72 FR (3) A tolerance is established for the 41931, Aug. 1, 2007] combined residues of the herbicide tebuthiuron (N-(5-(1,1-dimethylethyl)- § 180.396 Hexazinone; tolerances for 1,3,4-thiadiazol-2-yl)-N,N’- residues. dimethylurea) and its metabolites N-(5- (a) General. (1) Tolerances are estab- (1,1-dimethylethyl)-1,3,4-thiadiazol-2- lished for residues of the herbicide yl)-N-methylurea, N-(5-(2-hydroxy-1,1- hexazinone, 3-cyclohexyl-6- dimethylethyl)-1,3,4-thiadiazol-2-yl)-N- (dimethylamino)-1-methyl-1,3,5-tri- methylurea, N-(5-(1,1-dimethylethyl)- azine-2,4-(1H, 3H)-dione, including its 1,3,4-thiadiazol-2-yl)urea, N-(5-(1,1- metabolites and degradates, in or on dimethylethyl)-1,3,4-thiadiazol-2-yl)-N’- the commodities in the following table. hydroxymethyl-N-methylurea, and N- Compliance with the tolerance levels (5-(2-hydroxy-1,1-dimethylethyl)-1,3,4- specified in this paragraph is to be de- thiadiazol-2-yl)-N’-hydroxymethyl-N- termined by measuring only the sum of methylurea in or on the following raw hexazinone, 3-cyclohexyl-6- agricultural commodities: (dimethylamino)-1-methyl-1,3,5-triazine-2,4-(1H, 3H)-dione, and its plant Parts per Commodity million metabolites: metabolite A, 3-(4- hydroxycyclohexyl)-6- Milk ...... 0.8 (dimethylamino)-1-methyl-1,3,5-triazine-2,4-(1H, 3H)-dione, metabolite B, (b) Section 18 emergency exemptions. 3-cyclohexyl-6-(methylamino)-1-meth- [Reserved] yl-1,3,5-triazine-2,4-(1H, 3H)-dione, me- (c) Tolerances with regional registra- tabolite C, 3-(4-hydroxycyclohexyl)-6- tions. [Reserved] (methylamino)-1-methyl-1,3,5-triazine- (d) Indirect or inadvertent residues. 2,4-(1H, 3H)-dione, metabolite D, 3- [Reserved] cyclohexyl-1-methyl-1,3,5-triazine-2,4,6- [72 FR 53461, Sept. 19, 2007] (1H, 3H, 5H)-trione, and metabolite E, 3-(4-hydroxycyclohexyl)-1-methyl-1,3,5- § 180.395 Hydramethylnon; tolerances triazine-2,4,6-(1H, 3H, 5H)-trione, cal- for residues. culated as the stoichiometric equiva- (a) General. Tolerances are estab- lent of hexazinone, in or on the com- lished for residues of the insecticide modity. tetrahydro-5,5-dimethyl-2(1H)- Parts per pyrimidinone(3-(4- Commodity million (trifluoromethyl)phenyl)-1-(2-(4- (trifluoromethyl)phenyl)ethenyl)-2- Alfalfa, forage ...... 2.0 propenylidene)hydrazone in or on the Alfalfa, hay ...... 4.0 Alfalfa, seed ...... 2.0 following raw agricultural commod- Blueberry ...... 0.6 ities: Grass, forage ...... 250 Grass, hay ...... 230 Commodity Parts per Pineapple ...... 0.6 million Sugarcane, cane ...... 0.6 Sugarcane, molasses ...... 4.0 Grass, forage ...... 2 .0

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(2) Tolerances are established for res- metric equivalent of hexazinone, in or idues of the herbicide hexazinone, 3- on the commodity. cyclohexyl-6-(dimethylamino)-1-meth- Parts per yl-1,3,5-triazine-2,4-(1H, 3H)-dione, in- Commodity million cluding its metabolites and degradates, in or on the commodities in the fol- Milk ...... 11 lowing table. Compliance with the tolerance levels specified in this para- (b) Section 18 emergency exemptions. graph is to be determined by measuring [Reserved] only the sum of hexazinone, 3- (c) Tolerances with regional registra- cyclohexyl-6-(dimethylamino)-1-meth- tions. [Reserved] yl-1,3,5-triazine-2,4-(1H, 3H)-dione, and (d) Indirect or inadvertent residues. its animal tissue metabolites: metabo- [Reserved] lite B, 3-cyclohexyl-6-(methylamino)-1- [65 FR 33713, May 24, 2000, as amended at 71 methyl-1,3,5-triazine-2,4-(1H, 3H)-dione, FR 56399, Sept. 27, 2006; 75 FR 60244, Sept. 29, and metabolite F, 3-cyclohexyl-6- 2010] amino-1-methyl-1,3,5-triazine-2,4-(1H, 3H)-dione, calculated as the stoichio- § 180.399 Iprodione; tolerances for residues. metric equivalent of hexazinone, in or on the commodity. (a) General. (1) Tolerances are established for the combined residues of the Commodity Parts per fungicide iprodione [3-(3,5- million dichlorophenyl)-N-(1-methylethyl)-2,4- Cattle, fat ...... 0.1 dioxo-1-imidazolidinecarboxamide], its Cattle, meat ...... 0.5 isomer 3-(1-methylethyl)-N-(3,5- Cattle, meat byproducts ...... 4.0 dichlorophenyl)-2,4-dioxo-1- Goat, fat ...... 0.1 Goat, meat ...... 0.5 imidazolidinecarboxamide, and its me- Goat, meat byproducts ...... 4.0 tabolite 3-(3,5-dichlorophenyl)-2,4- Hog, fat ...... 0.1 dioxo-1-imidazolidine-carboxamide in Hog, meat ...... 0.5 or on the following food commodities: Hog, meat byproducts ...... 4.0 Horse, fat ...... 0.1 Parts per Horse, meat ...... 0.5 Commodity million Horse, meat byproducts ...... 4.0 Sheep, fat ...... 0.1 Almond, hulls ...... 2.0 Sheep, meat ...... 0.5 Almond ...... 0.3 Sheep, meat byproducts ...... 4.0 Apricot ...... 20.0 Bean, dry, seed ...... 2.0 Bean, forage ...... 90.0 (3) A tolerance is established for resi- Bean, succulent ...... 2.0 dues of the herbicide hexazinone, 3- Blueberry ...... 15.0 cyclohexyl-6-(dimethylamino)-1-meth- Boysenberry ...... 15.0 yl-1,3,5-triazine-2,4-(1H, 3H)-dione, in- Broccoli ...... 25.0 Caneberry subgroup 13A ...... 25.0 cluding its metabolites and degradates, Carrot, roots ...... 5.0 in or on the commodity in the fol- Cherry, sweet, postharvest ...... 20.0 lowing table. Compliance with the tol- Cherry, tart ...... 20.0 Cotton, undelinted seed ...... 0.10 erance level specified in this paragraph Cowpea, hay ...... 90.0 is to be determined by measuring only Currant ...... 15.0 the sum of hexazinone, 3-cyclohexyl-6- Garlic ...... 0.1 Ginseng ...... 2.0 (dimethylamino)-1-methyl-1,3,5-tri- Ginseng, dried root ...... 4.0 azine-2,4-(1H, 3H)-dione, and its me- Grape ...... 60.0 tabolites: metabolite B, 3-cyclohexyl-6- Grape, raisin ...... 300 (methylamino)-1-methyl-1,3,5-triazine- Kiwifruit ...... 10.0 Lettuce ...... 25.0 2,4-(1H, 3H)-dione, metabolite C, 3-(4- Nectarine, postharvest ...... 20.0 hydroxycyclohexyl)-6-(methylamino)-1- Onion, bulb ...... 0.5 methyl-1,3,5-triazine-2,4-(1H, 3H)-dione, Peach, postharvest ...... 20.0 Peanut ...... 0.5 metabolite C-2, 3-(3- Peanut, hay ...... 150.0 hydroxycyclohexyl)-6-(methylamino)-1- Plum, postharvest ...... 20.0 methyl-1,3,5-triazine-2,4-(1H, 3H)-dione, Plum, prune ...... 20.0 and metabolite F, 3-cyclohexyl-6- Potato ...... 0.5 Raspberry ...... 15.0 amino-1-methyl-1,3,5-triazine-2,4-(1H, Rice, bran ...... 30.0 3H)-dione, calculated as the stoichio- Rice, grain ...... 10.0

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dioxo-1-imidazolidinecarboxamide] in Commodity Parts per million or on the following food commodity: Rice, hulls ...... 50.0 Strawberry ...... 15.0 Parts per Commodity million

(2) Tolerances are established for the Mustard greens ...... 15.0 combined residues of iprodione [3-(3,5- dichlorophenyl)-N-(1-methylethyl)-2,4- (d) Indirect or inadvertent residues. dioxo-1-imidazolidinecarboxamide], its [Reserved] isomer [3-(1-methylethyl)-N-(3,5- [48 FR 40385, Sept. 7, 1983] dichlorophenyl)-2,4-dioxo-1- imidazolidinecarboxamide, and its me- EDITORIAL NOTE: For FEDERAL REGISTER ci- tabolites [3-(3,5-dichlorophenyl)-2,4- tations affecting § 180.399, see the List of CFR dioxo-1-imidazolidine-carboxamide] Sections Affected, which appears in the and [N-(3,5-dichloro-4-hydroxyphenyl)- Finding Aids section of the printed volume and at www.govinfo.gov. ureido-carboxamide], all expressed as iprodione equivalents in or on the fol- § 180.401 Thiobencarb; tolerances for lowing food commodities of animal ori- residues. gin: (a) General. Tolerances are established for the combined residues of the Commodity Parts per million herbicide thiobencarb (S-[(4- Cattle, fat ...... 0.5 chlorophenyl)methyl]diethyl- Cattle, kidney ...... 3.0 carbamothioate) and its chlorobenzyl Cattle, liver ...... 3.0 and chlorophenyl moiety-containing Cattle, meat ...... 0.5 Cattle, meat byproducts, except kidney and liver 0.5 metabolites in or on the following raw Egg ...... 1.5 agricultural commodities: Goat, fat ...... 0.5 Goat, kidney ...... 3.0 Part per Goat, liver ...... 3.0 Commodity million Goat, meat ...... 0.5 Goat, meat byproducts, except kidney and liver ... 0.5 Cattle, fat ...... 0.2 Hog, fat ...... 0.5 Cattle, meat byproducts ...... 0.2 Hog, kidney ...... 3.0 Cattle, meat ...... 0.2 Hog, liver ...... 3.0 Egg ...... 0.2 Hog, meat ...... 0.5 Goat, fat ...... 0.2 Hog, meat byproducts, except kidney and liver .... 0.5 Goat, meat byproducts ...... 0.2 Horse, fat ...... 0.5 Goat, meat ...... 0.2 Horse, kidney ...... 3.0 Hog, fat ...... 0.2 Horse, liver ...... 3.0 Hog, meat byproducts ...... 0.2 Horse, meat ...... 0.5 Horse, meat byproducts, except kidney and liver 0.5 Hog, meat ...... 0.2 Milk ...... 0.5 Horse, fat ...... 0.2 Poultry, fat ...... 3.5 Horse, meat byproducts ...... 0.2 Poultry, liver ...... 5.0 Horse, meat ...... 0.2 Poultry, meat ...... 1.0 Milk ...... 0.05 Poultry, meat byproducts, except liver ...... 1.0 Poultry, fat ...... 0.2 Sheep, fat ...... 0.5 Poultry, meat byproducts ...... 0.2 Sheep, kidney ...... 3.0 Poultry, meat ...... 0.2 Sheep, liver ...... 3.0 Rice, grain ...... 0.2 Sheep, meat ...... 0.5 Sheep, fat ...... 0.2 Sheep, meat byproducts, except kidney and liver 0.5 Sheep, meat byproducts ...... 0.2 Sheep, meat ...... 0.2 (b) Section 18 emergency exemptions. [Reserved] (b) Section 18 emergency exemptions. (c) Tolerances with regional registra- [Reserved] tions. Tolerances with regional reg- (c) Tolerances with regional registra- istration, as defined in § 180.1(l), are es- tions. Tolerances with regional reg- tablished for the combined residues of istration, as defined in § 180.1(l), are es- the fungicide iprodione [3-(3,5- tablished for residues of the herbicide dichlorophenyl)-N-(1-methylethyl)-2,4- thiobencarb (S-[(4-chloro- dioxo-1-imidazolidinecarboxamide], its phenyl)methyl]diethylcarbamothioate) isomer [3-(1-methylethyl)-N-(3,5- and its chlorobenzyl and chlorophenyl dichlorophenyl)-2,4-dioxo-1- moiety-containing metabolites in or on imidazolidinecarboxamide], and its me- the following raw agricultural com- tabolite [3-(3,5-dichlorophenyl)-2,4- modities:

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Parts per Parts per Commodity million Commodity million

Celery ...... 0.2 Cattle, meat byproducts ...... 0.05 Endive ...... 0.2 Cotton, gin byproducts ...... 55.0 Lettuce ...... 0.2 Cotton, undelinted seed ...... 2.0 Goat, fat ...... 0.05 (d) Indirect or inadvertent residues. Goat, meat ...... 0.05 Goat, meat byproducts ...... 0.05 [Reserved] Horse, fat ...... 0.05 Horse, meat ...... 0.05 [47 FR 6833, Feb. 17, 1982, as amended at 56 Horse, meat byproducts ...... 0.05 FR 2440, Jan. 23, 1991; 76 FR 34885, June 15, Milk ...... 0.01 2011; 80 FR 72599, Nov. 20, 2015] Sheep, fat ...... 0.05 Sheep, meat ...... 0.05 § 180.403 Thidiazuron; tolerances for Sheep, meat byproducts ...... 0.05 residues. (b) Section 18 emergency exemptions. (a) General. Tolerances are estab- [Reserved] lished for the combined residues of the (c) Tolerances with regional registra- defoliant thidiazuron (N-phenyl-N-1,2,3- tions. [Reserved] thiadiazol-5-ylurea) and its aniline con- (d) Indirect or inadvertent residues. taining metabolites in or on the fol- [Reserved] lowing food commodities: [65 FR 33700, May 24, 2000, as amended at 66 Parts per FR 50833, Oct. 5, 2001; 67 FR 49617, July 31, Commodity million 2002; 72 FR 54579, Sept. 26, 2007] Cattle, fat ...... 0.4 Cattle, meat ...... 0.4 § 180.405 Chlorsulfuron; tolerances for Cattle, meat byproducts ...... 0.4 residues. Cotton, gin byproducts ...... 24.0 Cotton, undelinted seed ...... 0.3 (a) General. (1) Tolerances are estab- Goat, fat ...... 0.4 lished for the combined residues of Goat, meat ...... 0.4 Goat, meat byproducts ...... 0.4 chlorsulfuron (2-chloro-N-[(4-methoxy- Hog, fat ...... 0.4 6-methyl-1,3,5-triazin-2- Hog, meat ...... 0.4 yl)aminocarbonyl]benzenesulfonamide) Hog, meat byproducts ...... 0.4 Horse, fat ...... 0.4 and its metabolite, 2-chloro-5-hydroxy- Horse, meat ...... 0.4 N-[(4-methoxy-6-methyl-1,3,5-triazin-2- Horse, meat byproducts ...... 0.4 yl)aminocarbonyl] benzenesulfonamide Milk ...... 0.05 Sheep, fat ...... 0.4 in or on the following raw agricultural Sheep, meat ...... 0.4 commodities: Sheep, meat byproducts ...... 0.4 Commodity Parts per (b) Section 18 emergency exemptions. million [Reserved] Barley, grain ...... 0.1 (c) Tolerances with regional registra- Barley, straw ...... 0.5 Oat, forage ...... 20.0 tions. [Reserved] Oat, grain ...... 0.1 (d) Indirect or inadvertent residues. Oat, straw ...... 0.5 [Reserved] Wheat, forage ...... 20.0 Wheat, grain ...... 0.1 [65 FR 33700, May 24, 2000, as amended at 72 Wheat, straw ...... 0.5 FR 53462, Sept. 19, 2007] (2) Tolerances are established for res- § 180.404 Profenofos; tolerances for idues of chlorsulfuron (2-chloro-N-[(4- residues. methoxy-6-methyl-1,3,5-triazin-2- (a) General. Tolerances are estab- yl)aminocarbonyl] lished for residues of the insecticide benzenesulfonamide) in or on the fol- profenofos (O-(4-bromo-2- lowing raw agricultural commodities. chlorophenyl)-O-ethyl-S-propyl Parts per phosphorothioate) in or on the fol- Commodity million lowing food commodities: Cattle, fat ...... 0.3 Parts per Cattle, meat ...... 0.3 Commodity million Cattle, meat byproducts ...... 0.3 Goat, fat ...... 0.3 Cattle, fat ...... 0.05 Goat, meat ...... 0.3 Cattle, meat ...... 0.05 Goat, meat byproducts ...... 0.3

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Commodity Parts per § 180.408 Metalaxyl; tolerances for res- million idues. Grass, forage ...... 11.0 (a) General. Tolerances are estab- Grass, hay ...... 19.0 lished for the combined residues of the Hog, fat ...... 0.3 fungicide metalaxyl [N-(2,6- Hog, meat ...... 0.3 Hog, meat byproducts ...... 0.3 dmethylphyenyl)-N-(methoxyacetyl) Horse, fat ...... 0.3 alanine methylester] and its metabo- Horse, meat ...... 0.3 lites containing the 2,6- Horse, meat byproducts ...... 0.3 dimethylaniline moiety, and N-(2-hy- Milk ...... 0.1 droxy methyl-6-methylphenyl)-N- Sheep, fat ...... 0.3 (methoxyacetyl)-alanine methyl ester, Sheep, meat ...... 0.3 each expressed as metalaxyl equiva- Sheep, meat byproducts ...... 0.3 lents, in or on the following food com- (b) Section 18 emergency exemptions. modities: [Reserved] Commodity Parts per (c) Tolerances with regional registra- million tions. [Reserved] Alfalfa, forage ...... 6.0 (d) Indirect or inadvertent residues. Alfalfa, hay ...... 20.0 [Reserved] Almond ...... 0.5 Almond, hulls ...... 10.0 [67 FR 52873, Aug. 14, 2002] Apple ...... 0.2 Apple, wet pomace ...... 0.4 Apricot, dried ...... 4.0 § 180.407 Thiodicarb; tolerances for Asparagus ...... 7.0 residues. Avocado ...... 4.0 Beet, garden, roots ...... 0.1 (a) General. Tolerances are estab- Beet, garden, tops ...... 0.1 lished for the combined residues of the Beet, sugar ...... 0.1 Beet, sugar, molasses ...... 1.0 insecticide thiodicarb (dimethyl N,N′- Beet, sugar, roots ...... 0.5 [thiobis[[(methylimino)carbonyloxy]] Beet, sugar, tops ...... 10.0 bis[ethanimidothioate]) and its me- Blueberry ...... 2.0 Broccoli ...... 2.0 tabolite methomyl (S-methyl N- Brussels sprouts ...... 2.0 [(methylcarbamoyl) Cabbage ...... 1.0 oxy]thioacetimidate) in or on the fol- Cattle, fat ...... 0.4 Cattle, kidney ...... 0.4 lowing food commodities or groups. Cattle, liver ...... 0.4 The time-limited tolerances expire and Cattle, meat ...... 0.05 are revoked on the dates listed in the Cattle, meat byproducts, except kidney and liver 0.05 Cauliflower ...... 1.0 following table: Citrus, oil ...... 7.0 Citrus, dried pulp ...... 7.0 Parts per Expiration/ Clover, forage ...... 1.0 Commodity million revocation Clover, hay ...... 2.5 date Cotton, undelinted seed ...... 0.1 Cranberry ...... 4.0 Broccoli ...... 7.0 None Egg ...... 0.05 Cabbage ...... 7.0 None Fruit, citrus ...... 1.0 Cauliflower ...... 7.0 None Fruit, stone, group 12 ...... 1.0 Corn, sweet, kernel plus cob with Ginseng ...... 3.0 husks removed ...... 2.0 None Goat, fat ...... 0.4 Cotton, undelinted seed ...... 0.4 None Goat, kidney ...... 0.4 Soybean, hulls ...... 0.8 None Goat, liver ...... 0.4 Soybean ...... 0.2 None Goat, meat ...... 0.05 Goat, meat byproducts, except kidney and liver ... 0.05 Vegetable, leafy, except brassica, Grain, cereal, group 15, except barley, oat and group 4 ...... 35 None wheat ...... 0.1 Grain, crop ...... 0.1 (b) Section 18 emergency exemptions. Grape ...... 2.0 [Reserved] Grape, raisin ...... 6.0 Grass, forage ...... 10.0 (c) Tolerances with regional registra- Grass, hay ...... 25.0 tions. [Reserved] Hog, fat ...... 0.4 (d) Indirect or inadvertent residues. Hog, kidney ...... 0.4 Hog, liver ...... 0.4 [Reserved] Hog, meat ...... 0.05 Hog, meat byproducts, except kidney and liver .... 0.05 [62 FR 44595, Aug. 22, 1997, as amended at 75 Hop, dried cones ...... 20 FR 60245, Sept. 29, 2010] Hop, vines ...... 2.0

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metalaxyl, in or on the following raw Commodity Parts per million agricultural commodity: Horse, fat ...... 0.4 Parts per Horse, kidney ...... 0.4 Commodity million Horse, liver ...... 0.4 Horse, meat ...... 0.05 Papaya ...... 0.1 Horse, meat byproducts, except kidney and liver 0.05 Lettuce, head ...... 5.0 Milk ...... 0.02 (d) Indirect or inadvertent tolerances. Mustard greens ...... 5.0 Tolerances are established for indirect Onion, bulb ...... 3.0 or inadvertent residues of metalaxyl in Onion, green ...... 10.0 Peanut ...... 0.2 or on the food commodities when Peanut, hay ...... 20.0 present therein as a result of the appli- Peanut, meal ...... 1.0 cation of metalaxyl to growing crops Peanut, hulls ...... 2.0 Pineapple ...... 0.1 listed in paragraph (a) of this section Pineapple, fodder ...... 0.1 and other non-food crops to read as fol- Pineapple, forage ...... 0.1 lows: Plum, prune, dried ...... 4.0 Potato, chips ...... 4.0 Part per Potato, granules, flakes ...... 4.0 Commodity million Potato, processed potato waste ...... 4.0 Potato, wet peel ...... 4.0 Barley, bran ...... 1.0 Poultry, fat ...... 0.4 Barley, flour ...... 1.0 Poultry, kidney ...... 0.4 Barley, grain ...... 0.2 Poultry, liver ...... 0.4 Barley, pearled barley ...... 1.0 Poultry, meat ...... 0.05 Barley, straw ...... 2.0 Poultry, meat byproducts, except kidney and liver 0.05 Grain, cereal, forage, fodder and straw, group 16, Potato ...... 0.5 except barley, oat, and wheat; forage ...... 1.0 Raspberry ...... 0.5 Grain, cereal, forage, fodder and straw, group 16, Sheep, fat ...... 0.4 except barley, oat, and wheat; stover ...... 1.0 Sheep, kidney ...... 0.4 Grain, cereal, forage, fodder and straw, group 16, Sheep, liver ...... 0.4 except barley, oat, and wheat; straw ...... 1.0 Sheep, meat ...... 0.05 Oat, flour ...... 1.0 Sheep, meat byproducts, except kidney and liver 0.05 Oat, forage ...... 2.0 Soybean, hulls ...... 2.0 Oat, grain ...... 0.2 Soybean, meal ...... 2.0 Oat, groats, rolled oats ...... 1.0 Soybean, seed ...... 1.0 Oat, straw ...... 2.0 Spinach ...... 10.0 Wheat, bran ...... 1.0 Strawberry ...... 10.0 Wheat, flour ...... 1.0 Sunflower, seed ...... 0.1 Wheat, forage ...... 2.0 Sunflower, forage ...... 0.1 Wheat, germ ...... 1.0 Tomato, paste ...... 3.0 Wheat, grain ...... 0.2 Tomato, puree ...... 3.0 Wheat, middlings ...... 1.0 Vegetable, brassica, leafy, group 5, except broc- Wheat, shorts ...... 1.0 coli, cabbage, cauliflower, brussels sprouts, Wheat, straw ...... 2.0 and mustard greens ...... 0.1 Vegetable, cucurbit, group 9 ...... 1.0 Vegetable, foilage of legume, group 7 ...... 8.0 [65 FR 33700, May 24, 2000, as amended at 72 Vegetable, fruiting, group 8 ...... 1.0 FR 35666, June 29, 2007; 74 FR 46374, Sept. 9, Vegetable, leafy, except brassica, group 4, ex- 2009; 75 FR 56015, Sept. 15, 2010] cept spinach ...... 5.0 Vegetable, leaves of root and tuber, group 2 ...... 15.0 Vegetable, legume, cannery waste ...... 5.0 § 180.409 Pirimiphos-methyl; toler- Vegetable, legume, group 6 ...... 0.2 ances for residues. Vegetable, root and tuber, group 1 ...... 0.5 Walnut ...... 0.5 (a) General. Tolerances are established for residues of the insecticide (b) Section 18 emergency exemptions. pirimiphos-methyl (O-(2-diethylamino- [Reserved] 6-methyl-4-pyrimidinyl) O,O-dimethyl (c) Tolerances with regional registra- phosphorothioate) in or on the fol- tions. Tolerances with regional reg- lowing raw agricultural commodities: istration (refer to § 180.1(m)) are estab- Parts per lished for the combined residues of the Commodity million fungicide metalaxyl [N-(2,6- dimethylphenyl)-N-(methoxyacetyl) al- Cattle, fat ...... 0.02 Cattle, meat byproducts ...... 0.02 anine methyl ester] and its metabolites Corn, field, grain ...... 8.0 containing the 2,6-dimethylaniline Corn, pop, grain ...... 8.0 moiety, and N-(2-hydroxy methyl-6- Goat, fat ...... 0.02 Goat, meat byproducts ...... 0.02 methyl)-N-(methoxyacetyl)-alanine Grain, aspirated fractions ...... 20.0 methylester, each expressed as Hog, fat ...... 0.02

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solved isomer of fluazifop, (R)-2-[4-[[5- Commodity Parts per million (trifluoromethyl)-2- Hog, meat byproducts ...... 0.02 pyridinyl]oxy]phenoxy]propanoic acid, Horse, fat ...... 0.02 calculated as the stoichiometric equiv- Horse, meat byproducts ...... 0.02 alent of fluazifop, in or on the com- Poultry, fat ...... 0.02 Sheep, fat ...... 0.02 modity. Sheep, meat byproducts ...... 0.02 Sorghum, grain, grain ...... 8.0 Parts per Commodity million

(b) Section 18 emergency exemptions. Banana ...... 0.01 [Reserved] Beans, dry, seed ...... 50 (c) Tolerances with regional registra- Beet, sugar, dried pulp ...... 1.0 tions. [Reserved] Beet, sugar, molasses ...... 3.5 Beet, sugar, roots ...... 0.25 (d) Indirect or inadvertent residues. Bushberry subgroup 13–07B ...... 0.30 [Reserved] Caneberry subgroup 13–07A ...... 0.08 Carrot, roots ...... 2.0 [65 FR 33714, May 24, 2000, as amended at 67 Cattle, fat ...... 0.05 FR 41807, June 19, 2002; 67 FR 49617, July 31, Cattle, meat ...... 0.05 2002; 70 FR 44492, Aug. 3, 2005; 72 FR 53462, Cattle, meat byproducts ...... 0.05 Sept. 19, 2007] Citrus, dried pulp ...... 0.40 Citrus, juice ...... 0.06 § 180.410 Triadimefon; tolerances for Citrus, oil ...... 30.0 Cotton, gin byproducts ...... 1.5 residues. Cotton, refined oil ...... 1.3 (a) General. Tolerances are estab- Cotton, undelinted seed ...... 1.0 lished for the combined residues of the Egg ...... 0.05 Endive ...... 6.0 fungicide triadimefon, 1-(4- Fruit, citrus, group 10 ...... 0.03 chlorophenoxy)-3,3-dimethyl-1-(1H- Fruit, small vine climbing, except fuzzy kiwifruit, 1,2,4-triazol-1-yl)-2-butanone, and subgroup 13–07F ...... 0.03 triadimenol, -(4-chlorophenoxy)- -(1,1- Fruit, stone ...... 0.05 b a Goat, fat ...... 0.05 dimethylethyl)-1H-1,2,4-triazole-1-eth- Goat, meat ...... 0.05 anol, expressed as triadimefon, in or on Goat, meat byproducts ...... 0.05 the following food commodities: Hog, fat ...... 0.05 Hog, meat ...... 0.05 Expiration/ Hog, meat byproducts ...... 0.05 Parts per Horse, fat ...... 0.05 Commodity million Revocation Date Horse, meat ...... 0.05 Horse, meat byproducts ...... 0.05 Pineapple ...... 2.0 None Lettuce, head ...... 3.0 Lettuce, leaf ...... 5.0 (b) Section 18 emergency exemptions. Milk ...... 0.05 [Reserved] Nut, macadamia ...... 0.1 Onion, bulb, subgroup 3–07A ...... 0.50 (c) Tolerances with regional registra- Onion, green ...... 1.5 tions. [Reserved] Peanut ...... 1.5 (d) Indirect or inadvertent residues. Peanut, meal ...... 2.2 [Reserved] Pecans ...... 0.05 Poultry, fat ...... 0.05 [73 FR 54962, Sept. 24, 2008, as amended at 76 Poultry, meat ...... 0.05 FR 34885, June 15, 2011] Poultry, meat byproducts ...... 0.05 Potato1 ...... 1.0 Potato, chips1 ...... 2.0 § 180.411 Fluazifop-P-butyl; tolerances Potato, granules/flakes1 ...... 4.0 for residues. Rhubarb ...... 0.50 (a) General. Tolerances are estab- Sheep, fat ...... 0.05 Sheep, meat ...... 0.05 lished for residues of the herbicide Sheep, meat byproducts ...... 0.05 fluazifop-P-butyl, including its me- Soybean, seed ...... 2.5 tabolites and degradates, in or on the Strawberry ...... 3.0 following commodities in the table. Vegetable, tuberous and corm, except potato, subgroup 1D ...... 1.5 Compliance with the tolerance levels specified in the table below is to be de- 1 No U.S. registrations. termined by measuring only the sum of (b) Section 18 emergency exemptions. fluazifop-P-butyl, butyl(R)-2-[4-[[5- [Reserved] (trifluoromethyl)-2- (c) Tolerances with regional registra- pyridinyl]oxy]phenoxy]propanoate, and tions. Tolerances with regional reg- the free and conjugated forms of the re- istrations are established for residues

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of the herbicide fluazifop-P-butyl, in- Commodity Parts per cluding its metabolites and degradates, illion in or on the following commodities in Borage, meal ...... 40 the table. Compliance with the toler- Buckwheat, flour ...... 25 ance levels specified in the table below Buckwheat, grain ...... 19 Bushberry subgroup 13–07B ...... 4.0 is to be determined by measuring only Calendula, meal ...... 20 the sum of fluazifop-P-butyl, butyl(R)- Caneberry subgroup 13–07A ...... 5.0 2-[4-[[5-(trifluoromethyl)-2- Canola, meal ...... 40 Castor oil plant, meal ...... 20 pyridinyl]oxy]phenoxy]propanoate, and Cattle, fat ...... 0.2 the free and conjugated forms of the re- Cattle, meat ...... 0.2 solved isomer of fluazifop, (R)-2-[4-[[5- Cattle, meat byproducts ...... 1.0 (trifluoromethyl)-2- Cherry, sweet ...... 0.2 Cherry, tart ...... 0.2 pyridinyl]oxy]phenoxy]propanoic acid, Chinese tallowtree, meal ...... 20 calculated as the stoichiometric equiv- Citrus, dried pulp ...... 1.5 alent of fluazifop, in or on the com- Clover, forage ...... 35 Clover, hay ...... 55 modity. Coriander, leaves ...... 4.0 Corn, field, forage ...... 2.0 Commodity Parts per Corn, field, grain ...... 0.5 million Corn, field, stover ...... 2.5 Corn, sweet, forage ...... 3.0 Asparagus ...... 3.0 Corn, sweet, kernel plus cob with husk removed 0.4 Coffee, bean ...... 0.1 Fescue, forage ...... 4.0 Corn, sweet, stover ...... 3.5 Fescue, hay ...... 15 Cottonseed subgroup 20C ...... 5.0 Pepper, tabasco ...... 1.0 Cowpea, forage ...... 15 Cowpea, hay ...... 50 Crambe, meal ...... 40 (d) Indirect or inadvertent residues. Cuphea, meal ...... 40 [Reserved] Dillweed, fresh leaves ...... 10 Echium, meal ...... 40 [65 FR 33714, May 24, 2000, as amended at 74 Egg ...... 2.0 FR 9372, Mar. 4, 2009; 74 FR 46374, Sept. 9, Euphorbia, meal ...... 20 2009; 74 FR 47457, Sept. 16, 2009; 76 FR 5703, Evening primrose, meal ...... 20 Feb. 2, 2011; 76 FR 59908, Sept. 28, 2011; 80 FR Flax seed, meal ...... 40 46822, Aug. 6, 2015; 82 FR 44942, Sept. 27, 2017] Fruit, citrus, group 10–10 ...... 0.5 Fruit, pome, group 11–10 ...... 0.2 Fruit, small, vine climbing, except fuzzy kiwifruit, § 180.412 Sethoxydim; tolerances for subgroup 13–07F ...... 1.0 residues. Goat, fat ...... 0.2 Goat, meat ...... 0.2 (a) Tolerances are established for the Goat, meat byproducts ...... 1.0 herbicide sethoxydim, including its Gold of pleasure, meal ...... 40 metabolites and degradates, in or on Grape, raisin ...... 2.0 the commodities in the table below. Hare’s ear mustard, meal ...... 40 Hog, fat ...... 0.2 Compliance with the tolerance levels Hog, meat ...... 0.2 specified below is to be determined by Hog, meat byproducts ...... 1.0 measuring only the sum of the herbi- Horse, fat ...... 0.2 Horse, meat ...... 0.2 cide 2-[1-(ethoxyimino)butyl]-5-[2- Horse, meat byproducts ...... 1.0 (ethylthio)propyl]-3-hydroxy-2-cyclo- Jojoba, meal ...... 20 hexen-1-one (CAS Reg. No. 74051–80–2) Juneberry 1 ...... 5.0 and its metabolites containing the 2- Lesquerella, meal ...... 40 Lingonberry 1 ...... 5.0 cyclohexen-1-one moiety, calculated as Lunaria, meal ...... 40 the stoichiometric equivalent of Meadowfoam, meal ...... 40 sethoxydim, in or on the commodity. Milk ...... 0.5 Milkweed, meal ...... 40 Parts per Mustard, meal ...... 40 Commodity illion Nectarine ...... 0.2 Niger seed, meal ...... 20 Alfalfa, forage ...... 40 Nut, tree, group 14 ...... 0.2 Alfalfa, hay ...... 40 Oil radish, meal ...... 40 Almond, hulls ...... 2.0 Pea and bean, dried shelled, except soybean, Apricot ...... 0.2 subgroup 6C ...... 25 Apple, wet pomace ...... 0.8 Pea, field, hay ...... 40 Asparagus ...... 4.0 Pea, field, vines ...... 20 Bean, succulent ...... 15 Pea, succulent ...... 10 Beet, sugar, molasses ...... 10 Peach ...... 0.2 Beet, sugar, tops ...... 3.0 Peanut ...... 25 Berry, low growing, subgroup 13–07H, except Peppermint, tops ...... 30 strawberry ...... 2.5 Pistachio ...... 0.2

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Commodity Parts per § 180.413 Imazalil; tolerances for resi- illion dues. Poppy seed, meal ...... 40 (a) General. (1) Tolerances are estab- Potato granules/flakes ...... 8.0 lished for the combined residues of the Potato waste, processed ...... 8.0 Poultry, fat ...... 0.2 fungicide imazalil, 1-[2-(2,4- Poultry, meat ...... 0.2 dichlorophenyl)-2-(2- Poultry, meat byproducts ...... 2.0 propenyloxy)ethyl]-1H-imidazole, and Radish, tops ...... 4.5 Rapeseed, meal ...... 40 its metabolite, 1-(2,4-dichlorophenyl)-2- Rapeseed subgroup 20A ...... 35 (1H-imidazole-1-yl)-1-ethanol, in or on Rose hip, meal ...... 20 the following food commodities: Safflower, seed ...... 15 Salal 1 ...... 5.0 Parts per Sesame, meal ...... 40 Commodity million Sheep, fat ...... 0.2 Sheep, meat ...... 0.2 Banana ...... 3.0 Sheep, meat byproducts ...... 1.0 Barley, grain ...... 0.1 Soybean, hay ...... 10 Barley, hay ...... 0.5 Soybean, seed ...... 16 Barley, straw ...... 0.5 Spearmint, tops ...... 30 Citrus, dried pulp ...... 25.0 Strawberry ...... 10 Citrus, oil ...... 200.0 Stokes aster, meal ...... 20 Fruit, citrus, postharvest ...... 10.0 Sunflower, meal ...... 20 Wheat, forage ...... 0.5 Sunflower subgroup 20B, except safflower ...... 7.0 Sweet rocket, meal ...... 40 Wheat, grain ...... 0.1 Tallowwood, meal ...... 20 Wheat, hay ...... 0.5 Tea oil plant, meal ...... 20 Wheat, straw ...... 0.5 Turnip, tops ...... 5.0 Vegetable, brassica, leafy, group 5 ...... 5.0 (2) Tolerances are established for the Vegetable, bulb, group 3–07 ...... 1.0 combined residues of the fungicide Vegetable, cucurbit, group 9 ...... 4.0 Vegetable, fruiting, group 8–10 ...... 4.0 imazalil, 1-[2-(2,4-dichlorophenyl)-2-(2- Vegetable, leafy, except brassica, group 4 ...... 4.0 propenyloxy)ethyl]-1H-imidazole, and Vegetable, root and tuber, group 1 ...... 4.0 its metabolites, 3-[2-(2,4- Vernonia, meal ...... 20 dichlorophenyl)-2-(2,3- 1 The individual tolerances for Juneberry, Lingonberry, and dihydroxypropoxy)ethyl]-2,4- Salal expire on December 15, 2015. imidazolidinedione (FK772) and 3-[2- (b) Section 18 emergency exemptions. (2,4-dichlorophenyl)-2-(hydroxy)]-2,4- [Reserved] imidazolidinedione (FK284), in or on (c) Tolerances with regional registra- the following food commodities: tion. Tolerances are established for the herbicide sethoxydim, including its Commodity Parts per metabolites and degradates, in or on million the commodities in the table below. Cattle, fat ...... 0.01 Compliance with the tolerance levels Cattle, meat ...... 0.01 specified below is to be determined by Cattle, meat byproducts ...... 0.2 measuring only the sum of the herbi- Goat, fat ...... 0.01 Goat, meat ...... 0.01 cide 2-[1-(ethoxyimino)butyl]-5-[2- Goat, meat byproducts ...... 0.2 (ethylthio)propyl]-3-hydroxy-2-cyclo- Horse, fat ...... 0.01 hexen-1-one) and its metabolites con- Horse, meat ...... 0.01 taining the 2-cyclohexen-1-one moiety, Horse, meat byproducts ...... 0.2 calculated as the stoichiometric equiv- Milk ...... 0.02 Sheep, fat ...... 0.01 alent of sethoxydim, in or on the com- Sheep, meat ...... 0.01 modity. Sheep, meat byproducts ...... 0.2

Parts per Commodity million (b) Section 18 emergency exemptions. [Reserved] Artichoke, globe ...... 5.0 (c) Tolerances with regional registra- Fescue, forage ...... 7.0 Fescue, hay ...... 4.0 tions. [Reserved] Rhubarb ...... 0.3 (d) Indirect or inadvertent residues. [Reserved] (d) Indirect and inadvertent residues. [Reserved] [65 FR 33715, May 24, 2000, as amended at 67 FR 46893, July 17, 2002; 71 FR 54434, Sept. 15, [80 FR 34077, June 15, 2015] 2006]

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§ 180.414 Cyromazine; tolerances for Commodity Parts per residues. million (a) General. (1) Tolerances are estab- Snow pea, edible podded ...... 0.4 lished for residues of cyromazine, in- Sugar snap pea, edible podded ...... 0.4 Tomato subgroup 8–10A ...... 1 cluding its metabolites and degradates, Vegetable, brassica, head and stem, group 5–16, in or on the commodities in the table except broccoli ...... 35 in this paragraph. Compliance with the Vegetable, cucurbit, group 9 ...... 1.0 tolerance levels specified in this para- Vegetable, tuberous and corm, subgroup 1C ...... 0.8 graph is to be determined by measuring 1There are no U.S. registrations on mango as of May 4, 2000. only cyromazine, N-cyclopropyl-1,3,5- 2 This tolerance expires on April 7, 2020. triazine-2,4,6-triamine. (2) A tolerance of 5.0 parts per mil- Parts per lion is established for residues of the Commodity million insecticide cyromazine, including its Bean, dry, except cowpea ...... 3.0 metabolites and degradates, in or on Bean, lima ...... 1.0 poultry feed when used as a feed addi- Bean, succulent ...... 2.0 tive only in feed for chicken layer hens Brassica, leafy greens, subgroup 4–16B ...... 35 and chicken breeder hens at the rate of Broccoli ...... 1.0 Cattle, fat ...... 0.05 not more than 0.01 pound of Cattle, kidney ...... 0.2 cyromazine per ton of poultry feed for Cattle, meat ...... 0.05 control of flies in manure of treated Cattle, meat byproducts, except kidney ...... 0.05 Celtuce ...... 10 chicken layer hens and chicken breeder Chickpea, edible podded ...... 0.4 hens, provided the feeding of Chickpea, succulent shelled ...... 0.3 cyromazine-treated feed must stop at Dwarf pea, edible podded ...... 0.4 Edible podded pea, edible podded ...... 0.4 least 3 days (72 hours) before slaughter. Egg ...... 0.25 If the feed is formulated by any person English pea, succulent shelled ...... 0.3 other than the end user, the formulator Fennel, Florence, fresh leaves and stalk ...... 10 Garden pea, succulent shelled ...... 0.3 must inform the end user, in writing, Goat, fat ...... 0.05 of the 3-day (72 hours) pre-slaughter in- Goat, kidney ...... 0.2 terval. Compliance with the tolerance Goat, meat ...... 0.05 level specified in this paragraph is to Goat, meat byproducts, except kidney ...... 0.05 Grass-pea, edible podded ...... 0.4 be determined by measuring only Green pea, edible podded ...... 0.4 cyromazine, N-cyclopropyl-1,3,5-tri- Green pea, succulent shelled ...... 0.3 azine-2,4,6-triamine, in or on the com- Hog, fat ...... 0.05 Hog, kidney ...... 0.2 modity. Hog, meat ...... 0.05 (b) Section 18 emergency exemptions. Hog, meat byproducts, except kidney ...... 0.05 [Reserved] Horse, fat ...... 0.05 Horse, kidney ...... 0.2 (c) Tolerances with regional registra- Horse, meat ...... 0.05 tions. [Reserved] Horse, meat byproducts, except kidney ...... 0.05 (d) Indirect or inadvertent residues. Kohlrabi ...... 35 Tolerances are established for indirect Leaf petiole vegetable subgroup 22B ...... 10 Leafy greens subgroup 4–16A ...... 10 or inadvertent residues of the insecti- Lentil, edible podded ...... 0.4 cide cyromazine, including its metabo- Lentil, succulent shelled ...... 0.3 lites and degradates, in or on the com- Mango 1 ...... 0.3 Milk ...... 0.05 modities in the table in this paragraph Mushroom ...... 1.0 when present therein as a result of the Onion, bulb, subgroup 3–07A ...... 0.3 application of cyromazine to growing Onion, green, subgroup 3–07B ...... 3 crops listed in paragraph (a)(1) of this Onion, potato 2 ...... 3.0 Pepper/eggplant subgroup 8–10B ...... 3 section. Compliance with the tolerance Pigeon pea, edible podded ...... 0.4 levels specified in this paragraph is to Pigeon pea, succulent shelled ...... 0.3 be determined by measuring only Poultry, fat (from chicken layer hens and chicken breeder hens only) ...... 0.05 cyromazine, N-cyclopropyl-1,3,5-tri- Poultry, meat (from chicken layer hens and chick- azine-2,4,6-triamine, in or on the com- en breeder hens only) ...... 0.05 modity. Poultry, meat byproducts (from chicken layer hens and chicken breeder hens only) ...... 0.05 Parts per Sheep, fat ...... 0.05 Commodity million Sheep, kidney ...... 0.2 Sheep, meat ...... 0.05 Cotton, undelinted seed ...... 0.1 Sheep, meat byproducts, except kidney ...... 0.05 Corn, sweet, kernel plus cob with husks removed 0.5 Snap pea, edible podded ...... 0.4 Corn, sweet, forage ...... 0.5

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by measuring only aluminum tris (O- Commodity Parts per million ethylphosphonate), in or on the com- Corn, sweet, stover ...... 0.5 modity. Radish, roots ...... 0.5 Radish, tops ...... 0.5 Parts per Commodity million

[65 FR 25860, May 4, 2000, as amended at 67 Asparagus ...... 0.1 FR 72593, Dec. 6, 2002; 68 FR 55269, Sept. 24, Grape ...... 10 2003; 75 FR 22256, Apr. 28, 2010; 76 FR 23494, Apr. 27, 2011; 84 FR 53322, Oct. 7, 2019] (d) Indirect or inadvertent residues. § 180.415 Aluminum tris (O- [Reserved] ethylphosphonate); tolerances for [64 FR 36801, July 8, 1999, as amended at 64 residues. FR 37875, July 14, 1999; 65 FR 50438, Aug. 18, (a) General. Tolerances are estab- 2000; 67 FR 55346, Aug. 29, 2002; 68 FR 11335, lished for residues of the fungicide alu- Mar. 10, 2003; 70 FR 7047, Feb. 10, 2005; 76 FR minum tris (O-ethylphosphonate), in- 23494, Apr. 27, 2011; 80 FR 2320, Jan. 16, 2015; cluding its metabolites and degradates, 83 FR 12265, Mar. 21, 2018] in or on the commodities in the table in this paragraph. Compliance with the § 180.416 Ethalfluralin; tolerances for tolerance levels specified in this para- residues. graph is to be determined by measuring (a) General. Tolerances are estab- only aluminum tris (O- lished for residues of the herbicide ethylphosphonate), in or on the com- ethalfluralin, including its metabolites modity. and degradates, in or on the commod-

Parts per ities in the following table. Compliance Commodity million with the tolerance levels specified in the following table is to be determined Avocado ...... 25 Banana ...... 3.0 by measuring only the residues of Bushberry subgroup 13B ...... 40 ethalfluralin, N-ethyl-N-(2-methyl-2- Caneberry subgroup 13A ...... 0.1 Cranberry ...... 0.5 propenyl)-2,6-dinitro-4- Fruit, citrus, group 10–10 ...... 9.0 (trifluoromethyl)benzenamine. Fruit, pome, group 11 ...... 10 Ginseng ...... 0.1 Parts per Hop, dried cones ...... 45 Commodity million Juneberry ...... 40 Lingonberry ...... 40 Bean, dry, seed ...... 0.05 Nut, macadamia ...... 0.20 Dill, dried leaves ...... 0.05 Onion, bulb ...... 0.5 Dill, fresh leaves ...... 0.05 Onion, green ...... 10.0 Pea, succulent ...... 0.3 Peanut ...... 0.05 Pepper/eggplant, subgroup 8–10B 1 ...... 0.01 Pea, dry, seed ...... 0.05 Pineapple ...... 0.1 Potato ...... 0.05 Salal ...... 40 Rapeseed subgroup 20A ...... 0.05 Strawberry ...... 75 Soybean ...... 0.05 Tomato ...... 3 Sunflower subgroup 20B ...... 0.05 Turnip, greens ...... 40 Turnip, roots ...... 15 Vegetable, cucurbit, group 9 ...... 0.05 Vegetable, brassica, leafy, group 5 ...... 60 Vegetable, cucurbit, group 9 ...... 15 (b) Section 18 emergency exemptions. Vegetable, leafy, except brassica, group 4 ...... 100 [Reserved] (b) Section 18 emergency exemptions. (c) Tolerances with regional registra- [Reserved] tions. [Reserved] (c) Tolerances with regional registra- (d) Indirect or inadvertent residues. tions. Tolerances with regional reg- [Reserved] istration, as defined in § 180.1(l), are es- [49 FR 391, Jan. 4, 1984, as amended at 50 FR tablished for residues of the fungicide 4976, Feb. 5, 1985; 52 FR 11262, Apr. 8, 1987; 62 aluminum tris (O-ethylphosphonate), FR 66014, Dec. 17, 1997; 64 FR 5191, Feb. 3, including its metabolites and 1999; 64 FR 54782, Oct. 8, 1999; 66 FR 37598, degradates, in or on the commodities July 19, 2001; 66 FR 41454, Aug. 8, 2001; 67 FR in the table in this paragraph. Compli- 2342, Jan. 17, 2002; 67 FR 49617, July 31, 2002; ance with the tolerance levels specified 72 FR 68534, Dec. 5, 2007; 78 FR 40020, July 3, in this paragraph is to be determined 2013]

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§ 180.417 Triclopyr; tolerances for resi- residues of the triclopyr (2-[(3,5,6- dues. trichloro-2-pyridinyl)oxy]acetic acid), (a) General. (1) Tolerances are estab- including its metabolites and lished for residues of the herbicide degradates in or on the specified agri- triclopyr, including its metabolites and cultural commodities, resulting from degradates, in or on the commodities use of the pesticide pursuant to FIFRA in the table below resulting from the section 18 emergency exemptions. The application of the butoxyethyl ester of tolerances expire on the date specified triclopyr, triethylamine salt of in the table. triclopyr, or choline salt of triclopyr. Commodity Parts per Expiration Compliance with the tolerance levels million date specified below is to be determined by measuring only triclopyr, 2-[(3,5,6- Sugarcane, cane ...... 40 12/31/20 trichloro-2-pyridinyl)oxy]acetic acid. (c) Tolerances with regional registra- Parts per Commodity million tions. [Reserved] (d) Indirect or inadvertent residues. Egg ...... 0.05 [Reserved] Fish ...... 3.0 Grass, forage ...... 700.0 [50 FR 18486, May 1, 1985, as amended at 55 Grass, hay ...... 200.0 FR 26440, June 28, 1990; 60 FR 4095, Jan. 20, Milk ...... 0.60 Poultry, fat ...... 0.1 1995; 62 FR 46894, Sept. 5, 1997; 63 FR 45406, Poultry, meat ...... 0.1 Aug. 26, 1998; 67 FR 35048, May 17, 2002; 67 FR Poultry, meat byproducts, except kidney ...... 0.1 58725, Sept. 18, 2002; 72 FR 41931, Aug. 1, 2007; Rice, grain ...... 0.3 80 FR 72599, Nov. 20, 2015; 81 FR 9359, Feb. 25, Shellfish ...... 3.5 2016; 82 FR 26603, June 8, 2017]

(2) Tolerances are established for res- § 180.418 Cypermethrin and isomers idues of the herbicide triclopyr, includ- alpha-cypermethrin and zeta- ing its metabolites and degradates, in cypermethrin; tolerances for resi- or on the commodities in the table dues. below resulting from the application of (a) General. (1) Tolerances are estab- the butoxyethyl ester of triclopyr, lished for residues of the insecticide triethylamine salt of triclopyr, or cypermethrin (±)alpha cyano-(3- choline salt of triclopyr. Compliance phenoxyphenyl)methyl(±)cis,trans- with the tolerance levels specified 3(2,2-dichloroethenyl-2,2- below is to be determined by measuring dimethylcyclopropanecarboxylate in or the combined residues of triclopyr, 2- on the following commodities: [(3,5,6-trichloro-2-pyridinyl)oxy]acetic Parts per acid, and its metabolite 3,5,6-trichloro- Commodity million 2-pyridinol (TCP), calculated as the stoichiometric equivalent of triclopyr. Brassica, head and stem, subgroup 5A ...... 2.0 Brassica, leafy greens, subgroup 5B ...... 14.0 Parts per Cattle, fat ...... 1.0 Commodity million Cattle, meat ...... 0.2 Cattle, meat byproducts ...... 0.05 Cattle, fat ...... 0.10 Cotton, gin byproducts ...... 11.0 Cattle, meat ...... 0.10 Cotton, undelinted seed ...... 0.5 Cattle, meat byproducts ...... 0.50 Egg ...... 0.05 Goat, fat ...... 0.10 Goat, fat ...... 1.0 Goat, meat ...... 0.10 Goat, meat ...... 0.2 Goat, meat byproducts ...... 0.50 Goat, meat byproducts ...... 0.05 Hog, fat ...... 0.10 Hog, fat ...... 0.1 Hog, meat ...... 0.10 Hog, meat ...... 0.05 Hog, meat byproducts ...... 0.50 Horse, fat ...... 1.0 Horse, fat ...... 0.10 Horse, meat ...... 0.2 Horse, meat ...... 0.10 Horse, meat byproducts ...... 0.05 Horse, meat byproducts ...... 0.50 Lettuce, head ...... 4.0 Sheep, fat ...... 0.10 Milk, fat (reflecting 0.10 in whole milk) ...... 2.5 Sheep, meat ...... 0.10 Onion, bulb ...... 0.1 Sheep, meat byproducts ...... 0.50 Onion, green ...... 6.0 Pecan ...... 0.05 (b) Section 18 emergency exemptions. Poultry, fat ...... 0.05 Poultry, meat ...... 0.05 Time-limited tolerances specified in Sheep, fat ...... 1.0 the following table are established for Sheep, meat ...... 0.2

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Parts per Parts per Commodity million Commodity million

Sheep, meat byproducts ...... 0.05 Evening primrose, seed ...... 0.2 Flax, seed ...... 0.2 (2) Tolerances are established for res- Food commodities/feed commodities (other than those covered by a higher tolerance as a result idues of zeta-cypermethrin, (S-cyano(3- of use on growing crops) in food/feed handling phenoxyphenyl) methyl (±))(cis-trans 3- establishments ...... 0.05 (2,2-dichloroethenyl)-2,2 Fruit, citrus, group 10 ...... 0.35 Fruit, pome, group 11 ...... 2 dimethylcyclopropanecarboxylate), in- Fruit, stone, group 12 ...... 1 cluding its metabolites and degradates, Goat, fat ...... 1.00 in or on the commodities in the fol- Goat, meat ...... 0.2 Goat, meat byproducts ...... 0.05 lowing table. Compliance with the tol- Gold of pleasure, seed ...... 0.2 erance levels specified in the following Grain, aspirated fractions ...... 10.0 table is to be determined by measuring Grape ...... 2 only total cypermethrin, cyano(3- Grass, forage, fodder, and hay, group 17, forage 10 Grass, forage, fodder and hay, group 17, hay ...... 35 phenoxyphenyl)methyl 3-(2,2- Hare’s-ear mustard, seed ...... 0.2 dichloroethenyl)-2,2- Hog, fat ...... 0.1 dimethylcyclopropane carboxylate, in Hog, meat ...... 0.05 Horse, fat ...... 1.00 or on the commodity. Horse, meat ...... 0.2 Horse, meat byproducts ...... 0.05 Parts per Jojoba, refined oil ...... 0.4 Commodity million Jojoba, seed ...... 0.2 Lesquerella, seed ...... 0.2 Alfalfa, forage ...... 15 Alfalfa, hay ...... 30 Lunaria, seed ...... 0.2 Alfalfa, seed ...... 0.50 Mango ...... 0.70 Almond, hulls ...... 6 Meadowfoam, seed ...... 0.2 Animal feed, nongrass, group 18, forage ...... 8 Milk, fat (reflecting 0.10 in whole milk) ...... 2.50 Animal feed, nongrass, group 18, hay ...... 40 Milkweed, seed ...... 0.2 Artichoke, globe ...... 0.60 Mustard, seed ...... 0.2 Avocado ...... 0.50 Niger seed, refined oil ...... 0.4 Barley, grain ...... 3.0 Niger seed, seed ...... 0.2 Barley, hay ...... 6.0 Nut, tree, group 14 ...... 0.05 Barley, straw ...... 20.0 Oat, grain ...... 3.0 Beet, sugar, roots ...... 0.05 Oat, hay ...... 6.0 Beet, sugar, tops ...... 0.20 Oat, straw ...... 20.0 Berry group 13 ...... 0.8 Oil radish, seed ...... 0.2 Borage, seed ...... 0.2 Okra ...... 0.2 Brassica, head and stem, subgroup 5A ...... 2.00 Onion, bulb ...... 0.10 Brassica, leafy greens, subgroup 5B ...... 14.00 Onion, green ...... 3.00 Buckwheat, grain ...... 3.0 Papaya ...... 0.50 Buckwheat, hay ...... 6.0 Pea and bean, dried shelled, except soybean, Buckwheat, straw ...... 20.0 subgroup 6C ...... 0.05 Cabbage ...... 2.00 Pea and bean, succulent shelled, subgroup 6B ... 0.1 Canistel ...... 0.50 Peanut ...... 0.05 Castor oil plant, refined oil ...... 0.4 Pecan ...... 0.05 Castor oil plant, seed ...... 0.2 Pistachio ...... 0.05 Cattle, fat ...... 1.00 Poppy, seed ...... 0.2 Cattle, meat ...... 0.2 Poultry, fat ...... 0.05 Cattle, meat byproducts ...... 0.05 Poultry, meat ...... 0.05 Chinese tallowtree, refined oil ...... 0.4 Rapeseed ...... 0.2 Chinese tallowtree, seed ...... 0.2 Rice, grain ...... 1.50 Cilantro, leaves ...... 10 Rice, hulls ...... 6.00 Citrus, dried pulp ...... 1.8 Rice, wild, grain ...... 1.5 Citrus, oil ...... 4.0 Rose hip, refined oil ...... 0.4 Corn, field, forage ...... 9.0 Rose hip, seed ...... 0.2 Corn, field, grain ...... 0.05 Rye, grain ...... 3.0 Corn, field, stover ...... 30 Rye, hay ...... 6.0 Corn, pop, grain ...... 0.05 Rye, straw ...... 20.0 Corn, pop, stover ...... 30 Safflower, seed ...... 0.2 Corn, sweet, forage ...... 15.00 Sapodilla ...... 0.50 Corn, sweet, kernel plus cob with husks removed 0.05 Sapote, black ...... 0.50 Corn, sweet, stover ...... 15.00 Sapote, mamey ...... 0.50 Cotton, undelinted seed ...... 0.5 Sesame, seed ...... 0.2 Crambe, seed ...... 0.2 Sheep, fat ...... 1.00 Cuphea, seed ...... 0.2 Sheep, meat ...... 0.2 Echium, seed ...... 0.2 Sheep, meat byproducts ...... 0.05 Egg ...... 0.05 Sorghum, grain, forage ...... 0.1 Euphorbia, refined oil ...... 0.4 Sorghum, grain, grain ...... 0.5 Euphorbia, seed ...... 0.2 Sorghum, grain, stover ...... 5.0 Evening primrose, refined oil ...... 0.4 Soybean, seed ...... 0.05

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Parts per Parts per Commodity million Commodity million

Star apple ...... 0.50 Hog, fat ...... 0.10 Stokes aster, refined oil ...... 0.4 Hog, meat ...... 0.05 Stokes aster, seed ...... 0.2 Horse, fat ...... 1.0 Sugarcane, cane ...... 0.60 Horse, meat ...... 0.20 Sunflower, refined oil ...... 0.5 Horse, meat byproducts ...... 0.05 Sunflower, seed ...... 0.2 Milk, fat, reflecting 0.10 ppm in whole milk ...... 2.5 Sweet rocket, seed ...... 0.2 Nut, tree, group 14–12 ...... 0.05 Tallowwood, refined oil ...... 0.4 Pea and bean, dried shelled, except soybean, Tallowwood, seed ...... 0.2 subgroup 6C ...... 0.05 Tea oil plant, refined oil ...... 0.4 Pea and bean, succulent shelled, subgroup 6B ... 0.10 Tea oil plant, seed ...... 0.2 Poultry, fat ...... 0.05 Turnip, greens ...... 14 Poultry, meat ...... 0.05 Vegetable, cucurbit, group 9 ...... 0.2 Rice, grain ...... 1.5 Vegetable, fruiting, group 8 ...... 0.2 Sheep, fat ...... 1.0 Vegetable, leafy, except brassica, group 4 ...... 10.00 Sheep, meat ...... 0.20 Vegetable, legume, edible podded, subgroup 6A 0.5 Sheep, meat byproducts ...... 0.05 Vegetable, root and tuber, group 1, except sugar Sorghum, grain, grain ...... 0.50 beet ...... 0.1 Soybean, seed ...... 0.05 Vernonia, refined oil ...... 0.4 Vegetable, cucurbit, group 9 ...... 0.20 Vernonia, seed ...... 0.2 Vegetable, fruiting, group 8–10 ...... 0.20 Wheat, forage ...... 3.0 Vegetable, leafy, group 4 ...... 10 Wheat, grain ...... 0.2 Vegetable, legume, edible podded, subgroup 6A 0.50 Wheat, hay ...... 6.0 Vegetable, root and tuber, group 1, except sugar Wheat, straw ...... 7.0 beet ...... 0.10 Wheat, grain ...... 0.20 (3) Tolerances are established for res- 1 This tolerance expires on December 5, 2018. idues of the insecticide, alpha- cypermethrin, (R)-cyano(3- (b) Section 18 emergency exemptions. phenoxyphenyl)methyl (1S,3S)-rel-3- [Reserved] (2,2-dichloroethenyl)-2,2- (c) Tolerances with regional registra- dimethylcyclopropane carboxylate, in- tions. [Reserved] cluding its metabolites and degradates, (d) Indirect or inadvertent residues. in or on the commodities in the table [Reserved] below. Compliance with the tolerance [62 FR 63235, 63243, Nov. 26, 1997, as amended levels specified below is to be deter- at 63 FR 48586, Sept. 11, 1998; 66 FR 47993, mined by measuring only total Sept. 17, 2001; 67 FR 6430, Feb. 12, 2002; 67 FR cypermethrin, cyano(3- 56495, Sept. 4, 2002; 69 FR 71717, Dec. 10, 2004; phenoxyphenyl)methyl 3-(2,2- 71 FR 78382, Dec. 29, 2006; 72 FR 53462, Sept. dichloroethenyl)-2,2- 19, 2007; 72 FR 71801, Dec. 19, 2007; 73 FR 1525, dimethylcyclopropane carboxylate, in Jan. 9, 2008; 77 FR 72984, Dec. 7, 2012; 78 FR or on the commodity. 7275, Feb. 1, 2013; 79 FR 73213, Dec. 10, 2014; 79 FR 77394, Dec. 24, 2014; 80 FR 45438, July 30, Parts per 2015; 80 FR 72599, Nov. 20, 2015; 83 FR 25943, Commodity million June 5, 2018]

Alfalfa, hay ...... 15 § 180.419 Chlorpyrifos-methyl; toler- Beet, sugar, roots ...... 0.05 Beet, sugar, tops ...... 0.20 ances for residues. Brassica, head and stem, subgroup 5A ...... 2.0 (a) General. (1) Tolerances are estab- Cattle, fat ...... 1.0 Cattle, meat ...... 0.20 lished for the combined residues of the Cattle, meat byproducts ...... 0.05 insecticide chlorpyrifos-methyl [O,-O,- Citrus, dried pulp ...... 1.8 dimethyl O-(3,5,6-trichloro-2-pyridyl)] Citrus, oil ...... 4.0 phosphorothioate and its metabolite Corn, field, grain ...... 0.05 Corn, pop, grain ...... 0.05 (3,5,6-trichloro-2-pyridinol) in or on the Corn, sweet, kernel plus cob with husks removed 0.05 following food commodities: Cotton, undelinted seed ...... 0.50 Egg ...... 0.05 Parts per Food commodities/feed commodities (other than Commodity million those covered by a higher tolerance as a results of use on growing crops) in food/feed Barley, grain ...... 6.0 handling establishments ...... 0.05 Cattle, fat ...... 0.5 Fruit, citrus, group 10–10 1 ...... 10 Cattle, meat ...... 0.5 Fruit, citrus, group 10–10 ...... 0.35 Cattle, meat byproducts ...... 0.5 Goat, fat ...... 1.0 Egg ...... 0.1 Goat, meat ...... 0.20 Goat, fat ...... 0.5 Goat, meat byproducts ...... 0.05 Goat, meat ...... 0.5 Hog, fat 1 ...... 1.0 Goat, meat byproducts ...... 0.5

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culated as the stoichiometric equiva- Commodity Parts per million lent of fluridone, in or on the com- Hog, fat ...... 0.5 modity. Hog, meat ...... 0.5 Hog, meat byproducts ...... 0.5 Commodity Parts per Horse, fat ...... 0.5 million Horse, meat ...... 0.5 Horse, meat byproducts ...... 0.5 Crayfish ...... 0.5 Milk, fat (0.05 ppm (N) in whole milk ...... 1.25 Fish ...... 0.5 Oat, grain ...... 6.0 Poultry, fat ...... 0.5 (2) Tolerances are established for res- Poultry, meat ...... 5 idues of the herbicide fluridone, includ- Poultry, meat byproducts ...... 5 Rice, grain ...... 6.0 ing its metabolites and degradates, in Sheep, fat ...... 0.5 or on the commodities in the table in Sheep, meat ...... 0.5 this paragraph. Compliance with the Sheep, meat byproducts ...... 0.5 Sorghum, grain ...... 6.0 tolerance levels specified in this para- Wheat, grain ...... 6.0 graph is to be determined by measuring only fluridone, 1-methyl-3-phenyl-5-(3- (2) Tolerances are established for the (trifluoromethyl)phenyl)-4(1H)- combined residues of the insecticide pyridinone, in or on the commodity. chlorpyrifos-methyl (O,-O- dimethyl-O- (3,5,6-trichloro-2-pyridyl) Parts per Commodity million phosphorothioate and its metabolite (3,5,6-trichloro-2-pyridinol) in or on the Avocado ...... 0 .1 following food commodities when Cattle, fat ...... 0.05 Cattle, kidney ...... 0 .1 present therein as a result of applica- Cattle, liver ...... 0 .1 tion to stored grains: Cattle, meat ...... 0 .05 Cattle, meat byproducts ...... 0.05 Parts per Cotton, gin byproducts ...... 0 .1 Commodity million Cotton, undelinted seed ...... 0 .1 Egg ...... 0 .05 Barley, bran ...... 90 Fruit, stone, group 12–12 ...... 0 .1 Barley, pearled barley ...... 90 Goat, fat ...... 0 .05 Rice, bran ...... 30 Goat, kidney ...... 0 .1 Rice, hulls ...... 30 Goat, liver ...... 0.1 Rice, polished rice ...... 30 Goat, meat ...... 0.05 Sorghum, grain, bran ...... 90 Goat, meat byproducts ...... 0 .05 Wheat, bran ...... 30 Hog, fat ...... 0 .05 Wheat, germ ...... 30 Hog, kidney ...... 0.1 Wheat, middlings ...... 30 Hog, liver ...... 0 .1 Wheat, shorts ...... 30 Hog, meat ...... 0 .05 Hog, meat byproducts ...... 0 .05 (b) Section 18 emergency exemptions. Horse, fat ...... 0 .05 Horse, kidney ...... 0 .1 [Reserved] Horse, liver ...... 0 .1 (c) Tolerances with regional registra- Horse, meat ...... 0 .05 tions. [Reserved] Horse, meat byproducts ...... 0 .05 Milk ...... 0.05 (d) Indirect or inadvertent residues. Pistachio ...... 0.1 [Reserved] Pomegranate ...... 0 .1 Poultry, fat ...... 0.05 [65 FR 33715, May 24, 2000, as amended at 74 Poultry, kidney ...... 0 .01 FR 46374, Sept. 9, 2009] Poultry, liver ...... 0 .01 Poultry, meat ...... 0 .05 § 180.420 Fluridone; tolerances for res- Poultry, meat byproducts ...... 0.05 Sheep, fat ...... 0 .05 idues. Sheep, kidney ...... 0.1 (a) General. (1) Tolerances are estab- Sheep, liver ...... 0.1 lished for residues of the herbicide Sheep, meat ...... 0.05 Sheep, meat byproducts ...... 0 .05 fluridone, including its metabolites Tangerine ...... 0 .1 and degradates, in or on the commodities in the table in this paragraph. (b) Section 18 emergency exemptions. Compliance with the tolerance levels [Reserved] specified in this paragraph is to be de- (c) Tolerances with regional registra- termined by measuring only the sum of tions. [Reserved] fluridone, 1-methyl-3-phenyl-5-(3- (d) Indirect or inadvertent residues. (trifluoromethyl)phenyl)-4(1H)- Tolerances are established for indirect pyridinone, and its bound residues, cal- or inadvertent residues of the herbicide

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fluridone, including its metabolites Parts per Expiration/ and degradates, in or on the irrigated Commodity revocation million date crop commodities and crop groupings in the table in this paragraph, result- Apple, wet pomace ...... 0.3 7/31/16 ing from use of irrigation water con- Banana 1 ...... 0.25 None Cattle, fat ...... 0.01 7/31/16 taining residues of 0.15 parts per mil- Cattle, kidney ...... 0.01 7/31/16 lion following applications of fluridone Cattle, meat ...... 0.01 7/31/16 on or around aquatic sites. Where tol- Cattle, meat byproducts, except kid- erances are established at higher levels ney ...... 0.05 7/31/16 Cherry, sweet ...... 1.0 7/31/16 from other uses of fluridone on the Cherry, tart ...... 1.0 7/31/16 crops in the table in this paragraph, Goat, fat ...... 0.01 7/31/16 the higher tolerance also applies to res- Goat, kidney ...... 0.01 7/31/16 idues in or on the irrigated commodity. Goat, meat ...... 0.01 7/31/16 Goat, meat byproducts, except kid- Compliance with the tolerance levels ney ...... 0.05 7/31/16 specified in this paragraph is to be de- Grape ...... 0.1 7/31/16 termined by measuring only fluridone, Hazelnut ...... 0.02 7/31/16 1-methyl-3-phenyl-5-(3- Hop, dried cones ...... 5.0 7/31/16 Horse, fat ...... 0.01 7/31/16 (trifluoromethyl)phenyl)-4(1H)- Horse, kidney ...... 0.01 7/31/16 pyridinone, in or on the commodity. Horse, meat ...... 0.01 7/31/16 Horse, meat byproducts, except kid- Commodity Parts per ney ...... 0.05 7/31/16 million Pear ...... 0.1 7/31/16 Pecan ...... 0.02 7/31/16 Animal feed, nongrass, group 18 ...... 0.15 Sheep, fat ...... 0.01 7/31/16 Berry, group 13 ...... 0.1 Sheep, kidney ...... 0.01 7/31/16 Cranberry ...... 0.1 Sheep, meat ...... 0.01 7/31/16 Fruit, citrus, group 10 ...... 0.1 Sheep, meat byproducts, except Fruit, pome, group 11 ...... 0.1 kidney ...... 0.05 7/31/16 Grain, cereal, forage, fodder and straw, group 16 0.1 Vegetable, cucurbit, group 9 2 ...... 0.20 None Grain, cereal, group 15 ...... 0.1 Grape ...... 0.1 1 There are no U.S. registrations for bananas as of April 26, Grass, forage ...... 0.15 1995. Hop, dried cones ...... 0.1 2 There are no U.S. registrations for cucurbit vegetable Nut, tree, group 14 ...... 0.1 group 9 as of August 27, 2010. Okra ...... 0.1 Strawberry ...... 0.1 (b) Section 18 emergency exemptions. Vegetable, brassica, leafy, group 5 ...... 0.1 [Reserved] Vegetable, cucurbit, group 9 ...... 0.1 (c) Tolerances with regional registra- Vegetable, fruiting, group 8 ...... 0.1 Vegetable, leafy, except brassica, group 4 ...... 0.1 tions. [Reserved] Vegetable, leaves of root and tuber, group 2 ...... 0.1 (d) Indirect or inadvertent residues. Vegetable, legume, group 6 ...... 0.1 [Reserved] Vegetable, root and tuber, group 1 ...... 0.1 [51 FR 39662, Oct. 30, 1986, as amended at 53 [76 FR 23495, Apr. 27, 2011, as amended at 77 FR 27349, July 20, 1988; 53 FR 44403, Nov. 3, FR 66720, Nov. 7, 2012; 80 FR 18143, Apr. 3, 1988; 54 FR 45734, Oct. 31, 1989; 60 FR 33354, 2015; 81 FR 7987, Feb. 17, 2016; 81 FR 72539, June 28, 1995; 62 FR 49937, Sept. 24, 1997; 62 FR Oct. 20, 2016; 85 FR 29637, May 18, 2020] 61447, Nov. 18, 1997; 67 FR 35048, May 17, 2002; 67 FR 41807, June 19, 2002; 69 FR 6567, Feb. 11, § 180.421 Fenarimol; tolerances for res- 2004; 71 FR 32846, June 7, 2006; 71 FR 54434, idues. Sept. 15, 2006; 74 FR 68173, Dec. 23, 2009; 75 FR 56897, Sept. 17, 2010; 81 FR 34905, June 1, 2016] (a) General. Tolerances are established for residues of fenarimol, includ- § 180.425 Clomazone; tolerances for ing its metabolites and degradates, in residues. or on the commodities in the following (a) General. Tolerances are estab- table. Compliance with the tolerance lished for residues of the herbicide levels specified in the following table is clomazone, including its metabolites to be determined by measuring only and degradates, in or on the commod- fenarimol alpha-(2 chlorophenyl)- ities in the table in this paragraph. alpha-(4-chlorophenyl)-5- Compliance with the tolerance levels pyrimidinemethanol. specified in this paragraph is to be determined by measuring only Parts per Expiration/ Commodity million revocation clomazone, 2-[(2-chlorophenyl)methyl]- date 4,4-dimethyl-3-isoxazolidinone, in or on Apple ...... 0.3 7/31/16 the commodity.

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Commodity Parts per § 180.426 2-[4,5-Dihydro-4-methyl-4-(1- million methylethyl)-5-oxo-1H-imidazol-2- Bean, asparagus, dry seed ...... 0.05 yl]-3-quinoline carboxylic acid; tol- Bean, broad, dry seed ...... 0.05 erance for residues. Bean, broad, succulent seed ...... 0.05 A tolerance is established for resi- Bean, kidney, dry seed ...... 0.05 Bean, lima, dry seed ...... 0.05 dues of the herbicide 2-[4,5-dihydro-4- Bean, lima, succulent seed ...... 0.05 methyl-4-(1-methylethyl)-5-oxo-1H- Bean, mung, dry seed ...... 0.05 imidazol-2-yl]-3-quinoline carboxylic Bean, navy, dry seed ...... 0.05 acid, in or on the raw agricultural com- Bean, pinto, dry seed ...... 0.05 modity soybean at 0.05 part per mil- Bean, snap, succulent ...... 0.05 Bean, wax, succulent seed ...... 0.05 lion. Broccoli, Chinese ...... 0.10 [51 FR 13309, Apr. 2, 1986] Chickpea, dry seed ...... 0.05 Cilantro, dried leaves ...... 0.30 Cilantro, fresh leaves ...... 0.05 § 180.427 Tau-Fluvalinate; tolerances Coriander, seed ...... 0.05 for residues. Cottonseed subgroup 20C ...... 0.05 (a) General. Tolerances are estab- Cowpea, forage ...... 0.05 Cowpea, hay ...... 0.05 lished for residues of the insecticide Cucumber * ...... 0.1 tau-fluvalinate, including its metabo- Dill, dried leaves ...... 0.40 lites and degradates, in or on commod- Dill, fresh leaves ...... 0.08 ities in the table below. Compliance Dill, oil ...... 0.07 Dill, seed ...... 0.05 with the specified tolerance level is to Grain lupin, dry seed ...... 0.05 be determined by measuring only tau- Kohlrabi ...... 0.10 fluvalinate, (cyano-(3- Pea, southern, dry seed ...... 0.05 phenoxyphenyl)methylN-[2-chloro-4- Pea, southern, succulent seed ...... 0.05 (trifluoromethyl)phenyl]-D-valinate), Pea, succulent ...... 0.05 Pepper ...... 0.05 in or on the commodity. Peppermint, tops ...... 0.05 Pumpkin * ...... 0.1 Parts per Commodity million Rapeseed subgroup 20A ...... 0.05 Rhubarb ...... 0.30 Grape, wine 1 ...... 1.0 Rice, grain ...... 0.02 Honey ...... 0.02 Soybean ...... 0.05 Soybean, vegetable, succulent ...... 0.05 1 There is no U.S. registration for use of tau-fluvalinate on Spearmint, tops ...... 0.05 wine grapes. Squash, summer * ...... 0.1 (b) Section 18 emergency exemptions. Squash, winter * ...... 0.1 Stalk and stem vegetable subgroup 22A, except [Reserved] kohlrabi ...... 0.05 (c) Tolerances with regional registra- Sugarcane, cane ...... 0.05 tions. [Reserved] Sweet lupin, dry seed ...... 0.05 Vegetable, Brassica, head and stem, group 5–16 0.10 (d) Indirect and inadvertent residues. Vegetable, cucurbit, group 9 ...... 0.05 [Reserved] Vegetable, tuberous and corm, except potato, subgroup 1D ...... 0.05 [65 FR 33701, May 24, 2000, as amended at 67 White lupin, dry seed ...... 0.05 FR 49617, July 31, 2002; 73 FR 52616, Sept. 10, White sweet lupin, dry seed ...... 0.05 2008; 81 FR 87462, Dec. 5, 2016] * This tolerance expires on June 5, 2019. § 180.428 Metsulfuron methyl; toler- (b) Section 18 emergency exemptions. ances for residues. [Reserved] (a) General. (1) Tolerances are estab- (c) Tolerances with regional registra- lished for the combined residues of the tions. [Reserved] herbicide metsulfuron methyl (methyl (d) Indirect or inadvertent residues. 2-[[[[(4-methoxy-6-methyl-1,3,5- triazin- [Reserved] 2-yl)amino]carbonyl]amino] sulfonyl] [51 FR 9446, Mar. 19, 1986] benzoate) and its metabolite methyl 2- [[[[(4-methoxy-6-methyl-1-,3,5- triazin- EDITORIAL NOTE: For FEDERAL REGISTER citations affecting § 180.425, see the List of CFR 2-yl)amino]carbonyl]amino] sulfonyl]- Sections Affected, which appears in the 4-hydroxybenzoate in or on the fol- Finding Aids section of the printed volume lowing raw material agricultural com- and at www.govinfo.gov. modities:

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termined by measuring only Commodity Parts per million chlorimuron ethyl, ethyl 2-[[[[(4- Barley, grain ...... 0.1 chloro-6-methoxypyrimidin- Barley, hay ...... 20.0 2yl)amino]carbonyl]sulfonyl]benzoate] Barley, straw ...... 0.3 in or on the following commodities: Grass, forage ...... 15.0 Grass, hay ...... 15.0 Parts per Grass, straw ...... 15.0 Commodity million Sorghum, grain, forage ...... 0.2 Sorghum, grain, grain ...... 0.1 Berry, low growing, except strawberry, subgroup Sorghum, grain, stover ...... 0.2 13–07H ...... 0.02 Sugarcane, cane ...... 0.05 Corn, field, forage ...... 0.5 Wheat, forage ...... 5.0 Corn, field, grain ...... 0.01 Wheat, grain ...... 0.1 Corn, field, stover ...... 2.0 Wheat, hay ...... 20.0 Grain, aspirated fractions ...... 3.0 Wheat, straw ...... 0.3 Peanut ...... 0.02 Soybean, forage ...... 0.45 (2) Tolerances are established for res- Soybean, hay ...... 1.8 idues of metsulfuron methyl (methyl- Soybean, seed ...... 0.05 2[[[[(4-methoxy- 6-methyl-1,3,5-triazin- 2- yl)amino]carbonyl]amino] sulfonyl] (b) Section 18 emergency exemptions. benzoate) in or on the following raw [Reserved] agricultural commodities: (c) Tolerances with regional registrations. [Reserved] Commodity Parts per (d) Indirect or inadvertent residues. million [Reserved] Cattle, fat ...... 0.1 Cattle, kidney ...... 0.5 [74 FR 10494, Mar. 11, 2009, as amended at 74 Cattle, meat ...... 0.1 FR 67087, Dec. 18, 2009] Cattle, meat byproducts ...... 0.1 Goat, fat ...... 0.1 § 180.430 Fenoxaprop-ethyl; tolerances Goat, kidney ...... 0.5 for residues. Goat, meat ...... 0.1 Goat, meat byproducts ...... 0.1 (a) General. Tolerances are estab- Hog, fat ...... 0.1 lished for residues of the herbicide Hog, kidney ...... 0.5 Hog, meat ...... 0.1 fenoxaprop-ethyl, including its me- Hog, meat byproducts ...... 0.1 tabolites and degradates, in or on the Horse, fat ...... 0.1 commodities in the table in this para- Horse, kidney ...... 0.5 graph. Compliance with the tolerance Horse, meat ...... 0.1 Horse, meat byproducts ...... 0.1 levels specified in this paragraph is to Milk ...... 0.05 be determined by measuring only the Sheep, fat ...... 0.1 sum of fenoxaprop-ethyl, (±)-ethyl 2-[4- Sheep, kidney ...... 0.5 Sheep, meat ...... 0.1 [(6-chloro-2- Sheep, meat byproducts ...... 0.1 benzoxazolyl)oxy]phenoxy]propanoate, and its metabolites, 2-[4-[(6-chloro-2- (b) Section 18 emergency exemptions. benzoxazolyl)oxy]phenoxy]propanoic [Reserved] acid and 6-chloro-2,3- (c) Tolerances with regional registra- dihydrobenzoxazol-2-one, calculated as tions. [Reserved] the stoichiometric equivalent of (d) Indirect or inadvertent residues. fenoxaprop-ethyl, in or on the com- [Reserved] modity.

[64 FR 70191, Dec. 16, 1999, as amended at 66 Parts per FR 64773, Dec. 14, 2001; 67 FR 51097, Aug. 7, Commodity million 2002] Barley, grain ...... 0.05 § 180.429 Chlorimuron ethyl; toler- Barley, straw ...... 0.1 Cattle, fat ...... 0.05 ances for residues. Cattle, meat byproducts ...... 0.05 (a) General. Tolerances are estab- Cattle, meat ...... 0.05 lished for residues of the herbicide Cotton, undelinted seed ...... 0.05 Goat, fat ...... 0.05 chlorimuron ethyl, including its me- Goat, meat byproducts ...... 0.05 tabolites and degradates, in or on the Goat, meat ...... 0.05 commodities in the table below. Com- Hog, fat ...... 0.05 Hog, meat byproducts ...... 0.05 pliance with the tolerance levels speci- Hog, meat ...... 0.05 fied in the following table is to be de- Horse, fat ...... 0.05

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acid and 6-chloro-2,3- Commodity Parts per million dihydrobenzoxazol-2-one, calculated as Horse, meat byproducts ...... 0.05 the stoichiometric equivalent of Horse, meat ...... 0.05 fenoxaprop-ethyl, in or on the com- Milk ...... 0.02 modity Peanut ...... 0.05 Peanut, hulls ...... 0.05 Parts per Rice, grain ...... 0.05 Commodity million Sheep, fat ...... 0.05 Sheep, meat byproducts ...... 0.05 Grass, hay ...... 0.09 Sheep, meat ...... 0.05 Soybean ...... 0.05 Wheat, grain ...... 0.05 (d) Indirect or inadvertent residues. Wheat, straw ...... 0.50 [Reserved] (b) Section 18 emergency exemptions. [63 FR 1377, Jan. 9, 1998, as amended at 63 FR Time-limited tolerances are estab- 19837, Apr. 22, 1998; 73 FR 33718, June 13, 2008; 75 FR 80346, Dec. 22, 2010; 76 FR 23495, Apr. 27, lished for residues of the herbicide 2011; 78 FR 78748, Dec. 27, 2013; 79 FR 26164, fenoxaprop-ethyl, including its me- May 7, 2014] tabolites and degradates, in or on the commodities in the table in this para- § 180.431 Clopyralid; tolerances for graph in connection with use of residues. fenoxaprop-ethyl under section 18 (a) General. Tolerances are estab- emergency exemptions granted by lished for residues of the herbicide EPA. Compliance with the tolerance clopyralid, including its metabolites levels specified in this paragraph is to and degradates, in or on the commod- be determined by measuring only the ities in the table below from its appli- ± sum of fenoxaprop-ethyl, ( )-ethyl 2-[4- cation in the acid form or in the form [(6-chloro-2- of its salts. Compliance with the toler- benzoxazolyl)oxy]phenoxy]propanoate, ance levels specified below is to be de- and its metabolites, 2-[4-[(6-chloro-2- termined by measuring only clopyralid, benzoxazolyl)oxy]phenoxy]propanoic (3,6-dichloro-2-pyridinecarboxylic acid), acid and 6-chloro-2,3- in or on the following commodities: dihydrobenzoxazol-2-one, calculated as the stoichiometric equivalent of Commodity Parts per fenoxaprop-ethyl, in or on the com- million modity. The tolerances expire and are Barley, bran ...... 12 revoked on the dates specified in the Barley, grain ...... 3.0 table in this paragraph. Barley, hay ...... 9.0 Barley, pearled barley ...... 12 Expiration/ Barley, straw ...... 9.0 Commodity Parts per revocation Beet, garden, roots ...... 4.0 million date Beet, sugar, molasses ...... 10 Beet, sugar, roots ...... 2.0 Grass, forage ...... 0.05 12/31/16 Berry, low growing, subgroup 13–07G ...... 4.0 Grass, hay ...... 0.05 12/31/16 Brassica, leafy greens, subgroup 4–16B ...... 5.0 Broccoli, Chinese ...... 2.0 (c) Tolerances with regional registra- Bushberry subgroup 13-07B ...... 0.50 Canola, meal ...... 6.0 tions. Tolerances with regional reg- Cattle, fat ...... 1.0 istration, as defined in § 180.1(l), are es- Cattle, liver ...... 3.0 tablished for residues of the herbicide Cattle, meat ...... 1.0 Cattle, meat byproducts, except liver ...... 36.0 fenoxaprop-ethyl, including its me- Corn, field, forage ...... 3.0 tabolites and degradates, in or on the Corn, field, grain ...... 1.0 commodities in the table in this para- Corn, field, milled byproducts ...... 1.5 graph when fenoxaprop-ethyl is used in Corn, field, stover ...... 10.0 Corn, pop, grain ...... 1.0 the states of Oregon, Washington, and Corn, pop, stover ...... 10.0 Utah. Compliance with the tolerance Corn, sweet, forage ...... 7.0 levels specified in this paragraph is to Corn, sweet, kernel plus cob with husks removed 1.0 Corn, sweet, stover ...... 10.0 be determined by measuring only the Egg ...... 0.1 sum of fenoxaprop-ethyl, (±)-ethyl 2-[4- Flax, meal ...... 6.0 [(6-chloro-2- Fruit, pome, group 11–10 ...... 0.05 benzoxazolyl)oxy]phenoxy]propanoate, Fruit, stone, group 12–12 ...... 0.50 Goat, fat ...... 1.0 and its metabolites, 2-[4-[(6-chloro-2- Goat, liver ...... 3.0 benzoxazolyl)oxy]phenoxy]propanoic Goat, meat ...... 1.0

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degradates, in or on the commodities Commodity Parts per million in the table in this paragraph. Compli- Goat, meat byproducts, except liver ...... 36.0 ance with the tolerance levels specified Grass, forage ...... 500.0 in this paragraph is to be determined Grass, hay ...... 500.0 Hog, fat ...... 0.2 by measuring only lactofen, 2-ethoxy-1- Hog, meat ...... 0.2 methyl-2-oxoethyl 5-[2-chloro-4- Hog, meat byproducts ...... 0.2 (trifluoromethyl)phenoxy]-2- Hop, dried cones ...... 5.0 Horse, fat ...... 1.0 nitrobenzoate, in or on the commodity. Horse, liver ...... 3.0 Horse, meat ...... 1.0 Commodity Parts per Horse, meat byproducts, except liver ...... 36.0 million Kohlrabi ...... 2.0 Milk ...... 0.2 Beans, snap, succulent, except lima bean ...... 0.01 Oat, forage ...... 9.0 Cotton, gin byproducts ...... 0.02 Oat, grain ...... 3.0 Cotton, undelinted seed ...... 0.01 Oat, groats/rolled oats ...... 12 Peanut ...... 0.01 Oat, straw ...... 9.0 Soybean, seed ...... 0.01 Peppermint, tops ...... 3.0 Plum, prune, dried ...... 1.5 Poultry, fat ...... 0.2 (b) Section 18 emergency exemptions. Poultry, meat ...... 0.2 [Reserved] Poultry, meat byproducts ...... 0.2 Radish, roots ...... 0.30 (c) Tolerances with regional registra- Rapeseed, forage ...... 3.0 tions. Tolerances with regional reg- Rapeseed, meal ...... 6.0 Rapeseed, subgroup 20A, except gold of pleas- istration, as defined in § 180.1(l), are es- ure ...... 3.0 tablished for residues of the herbicide Sheep, fat ...... 1.0 lactofen, including its metabolites and Sheep, liver ...... 3.0 Sheep, meat ...... 1.0 degradates, in or on the commodities Sheep, meat byproducts, except liver ...... 36.0 in the table in this paragraph. Compli- Spearmint, tops ...... 3.0 ance with the tolerance levels specified Spinach ...... 5.0 Stalk and stem vegetable subgroup 22A ...... 1.0 in this paragraph is to be determined Swiss chard ...... 3.0 by measuring only lactofen, 2-ethoxy-1- Teff, forage ...... 9.0 methyl-2-oxoethyl 5-[2-chloro-4- Teff, grain ...... 3.0 Teff, hay ...... 9.0 (trifluoromethyl)phenoxy]-2- Teff, straw ...... 9.0 nitrobenzoate, in or on the commodity. Turnip, roots ...... 1.0 Vegetable, Brassica, head and stem, group 5–16 2.0 Parts per Vegetable, leaves of root and tuber, group 2 ...... 5.0 Commodity million Wheat, bran ...... 12 Wheat, forage ...... 9.0 Okra ...... 0.02 Wheat, germ ...... 12 Vegetables, fruiting, group 08 ...... 0.02 Wheat, grain ...... 3.0 Wheat, middling ...... 12 Wheat, shorts ...... 12 (d) Indirect or inadvertent residues. Wheat, straw ...... 9.0 [Reserved] (b) Section 18 emergency exemptions. [69 FR 57216, Sept. 24, 2004, as amended at 72 [Reserved] FR 33906, June 20, 2007; 76 FR 23496, Apr. 27, (c) Tolerances with regional registra- 2011] tions. [Reserved] (d) Indirect or inadvertent residues. § 180.433 Fomesafen; tolerances for [Reserved] residues. [52 FR 10566, Apr. 2, 1987] (a) General. Tolerances are established for residues of the herbicide EDITORIAL NOTE: For FEDERAL REGISTER ci- fomesafen, including its metabolites tations affecting § 180.431, see the List of CFR Sections Affected, which appears in the and degradates, in or on the following Finding Aids section of the printed volume commodities. Compliance with the tol- and at www.govinfo.gov. erance levels specified in the following table below is to be determined by § 180.432 Lactofen; tolerances for resi- measuring only fomesafen, 5-[2-chloro- dues. 4-(trifluoromethyl)phenoxy]-N- (a) General. Tolerances are estab- (methylsulfonyl)-2-nitrobenzamide, in lished for residues of the herbicide or on the commodity. lactofen, including its metabolites and

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Parts per Parts per Commodity million Commodity million

Berry, low growing, subgroup 13–07G, except Cattle, liver ...... 2.0 cranberry ...... 0.02 Cattle, meat ...... 0.05 Cantaloupe ...... 0.025 Cattle, meat byproducts, except liver and kidney 0.05 Cotton, gin byproducts ...... 0.025 Celtuce ...... 5 Cotton, undelinted seed ...... 0.025 Cilantro, leaves ...... 13 Cucumber ...... 0.025 Citrus, oil ...... 1000 Pepper, bell ...... 0.025 Corn, field, forage ...... 12 Pepper, non-bell ...... 0.025 Corn, field, grain ...... 0.2 Pumpkin ...... 0.025 Corn, field, stover ...... 30 Squash, summer ...... 0.025 Corn, pop, grain ...... 0.2 Squash, winter ...... 0.025 Corn, pop, stover ...... 30 Tomato ...... 0.025 Corn, sweet, forage ...... 6.0 Vegetable, legume, group 6 ...... 0.05 Corn, sweet, kernel plus cob with husks removed 0.1 Vegetable, tuberous and corm, subgroup 1C ...... 0.025 Corn, sweet, stover ...... 30 Watermelon ...... 0.025 Dill, seed ...... 15 Dillweed, dried leaves ...... 80 (b) Section 18 emergency exemptions. Dillweed, fresh leaves ...... 30 Fennel, Florence, fresh leaves and stalk ...... 5 [Reserved] Fruit, citrus, group 10–10 ...... 8.0 (c) Tolerances with regional registra- Fruit, stone, group 12–12, except plum ...... 4.0 tions. [Reserved] Goat, fat ...... 0.05 Goat, kidney ...... 2.0 (d) Indirect or inadvertent residues. Goat, liver ...... 2.0 [Reserved] Goat, meat ...... 0.05 Goat, meat byproducts, except liver and kidney ... 0.05 [71 FR 25951, May 3, 2006, as amended at 72 Grain, aspirated fractions ...... 110 FR 52020, Sept. 12, 2007; 76 FR 12882, Mar. 9, Grass, forage ...... 0.5 2011; 78 FR 65570, Nov. 1, 2013; 80 FR 9391, Feb. Grass, hay ...... 0.5 23, 2015; 83 FR 5316, Feb. 7, 2018] Grass, straw ...... 40 Hog, kidney ...... 0.2 § 180.434 Propiconazole; tolerances for Hog, liver ...... 0.2 Horse, fat ...... 0.05 residues. Horse, kidney ...... 2.0 (a) General. (1) Tolerances are estab- Horse, liver ...... 2.0 lished for residues of propiconazole, in- Horse, meat ...... 0.05 Horse, meat byproducts, except liver and kidney 0.05 cluding its metabolites and degradates, Leaf petiole vegetable subgroup 22B ...... 5 in or on the commodities in the table Low growing berry subgroup 13–07G, except below. Compliance with the tolerance cranberry ...... 1.3 Milk ...... 0.05 levels specified below is to be deter- Mushroom ...... 0.1 mined by measuring only those Nut, tree, group 14–12 ...... 0.10 propiconazole residues convertible to Oat, forage ...... 4.0 2,4-dichlorobenzoic acid (2,4–DCBA), ex- Oat, grain ...... 3.0 Oat, hay ...... 15 pressed as the stoichiometric equiva- Oat, straw ...... 10 lent of propiconazole, in or on the com- Onion, bulb subgroup 3–07A ...... 0.2 modity in the table below: Onion, green, subgroup 3–07B ...... 9.0 Parsley, fresh leaves ...... 13 Parts per Parsley, dried leaves ...... 35 Commodity million Peanut ...... 0.2 Peanut, hay ...... 20 Almond, hulls ...... 7.0 Peppermint, tops ...... 10.0 Avocado ...... 0.2 Pineapple ...... 4.5 Banana ...... 0.2 Pineapple, process residue ...... 7.0 Barley, bran ...... 6.0 Plum ...... 0.60 Barley, grain ...... 3.0 Rapeseed subgroup 20A ...... 0.30 Barley, hay ...... 30 Quinoa, grain ...... 3.0 Barley, straw ...... 20 Radish, tops ...... 0.20 Bean, dry seed ...... 0.40 Rice, bran ...... 15 Bean, snap ...... 0.70 Rice, grain ...... 7.0 Bean, succulent shelled ...... 0.10 Rice, hulls ...... 20 Beet, garden, tops ...... 5.5 Rye, bran ...... 0.6 Beet, sugar, dried pulp ...... 1.0 Rye, forage ...... 9.0 Beet, sugar, molasses ...... 1.5 Rye, grain ...... 0.3 Beet, sugar, roots ...... 0.3 Rye, straw ...... 10 Beet, sugar, tops ...... 10 Sheep, fat ...... 0.05 Brassica, leafy greens, subgroup 4–16B, except Sheep, kidney ...... 2.0 watercress ...... 20 Sheep, liver ...... 2.0 Bushberry, subgroup 13–07B ...... 1.0 Sheep, meat ...... 0.05 Caneberry, subgroup 13–07A ...... 1.0 Sheep, meat byproducts, except liver and kidney 0.05 Cattle, fat ...... 0.05 Sorghum, grain, forage ...... 12 Cattle, kidney ...... 2.0 Sorghum, grain, grain ...... 3.5

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dichlorobenzoic acid and expressed as Commodity Parts per million parent compound, in or on the fol- Sorghum, grain, stover ...... 15 lowing commodities: Soybean, forage ...... 11 Soybean, hay ...... 30 Commodity Parts per Soybean, seed ...... 2.0 million Spearmint, tops ...... 10.0 Sugarcane, cane ...... 0.4 Cranberry ...... 1.0 Swiss chard ...... 5 Rice, wild, grain ...... 0.5 Ti palm, leaves ...... 10 Ti palm, roots ...... 0.30 Tomato ...... 3.0 (d) Indirect or inadvertent residues. Vegetable, foliage of legume, group 7 ...... 30 Tolerances are established for the com- Vegetable, root, except sugar beet, subgroup 1B 0.3 bined residues of the fungicide 1-[[2- Watercress ...... 6.0 Wheat, bran ...... 0.6 (2,4-dichlorophenyl)-4-propyl-1,3- Wheat, forage ...... 15 dioxolan-2-yl] methyl]-1H-1,2,4-triazole Wheat, grain ...... 0.3 and its metabolites determined as 2,4- Wheat, hay ...... 30 Wheat, straw ...... 20 dichlorobenzoic acid and expressed as parent compound in or on the following (2) Tolerances are established for commodities when present therein as a propiconazole, including its metabo- result of application of propiconazole lites and degradates, in or on the com- to growing crops in paragraphs (a) and modities in the table below. Compli- (c) of this section: ance with the tolerance levels specified Parts per below is to be determined by measuring Commodity million only propiconazole, 1-[[2-(2,4- dichlorophenyl)-4-propyl-1,3-dioxolan-2- Alfalfa, forage ...... 0.1 yl]methyl]-1H-1,2,4-triazole, in or on Alfalfa, hay ...... 0.1 the commodity. [71 FR 55306, Sept. 22, 2006, as amended at 72 Commodity Parts per FR 20439, Apr. 25, 2007; 74 FR 12613, Mar. 25, million 2009; 75 FR 80346, Dec. 22, 2010; 76 FR 27268, Tea 1 ...... 4.0 May 11, 2011; 77 FR 38204, June 27, 2012; 77 FR 75044, Dec. 19, 2012; 78 FR 23503, Apr. 19, 2013; 1 There are no United States registrations for use of propiconazole on tea as of December 24, 2015. 78 FR 78748, Dec. 27, 2013; 79 FR 18467, Apr. 2, 2014; 80 FR 72599, Nov. 20, 2015; 80 FR 79718, (b) Section 18 emergency exemptions. Dec. 23, 2015; 80 FR 80275, Dec. 24, 2015; 82 FR Time-limited tolerances are estab- 1210, Jan. 5, 2017; 84 FR 39774, Aug. 12, 2019] lished for residues of propiconazole (1- [[2-(2,4-dichlorophenyl)-4-propyl-1,3- § 180.435 Deltamethrin; tolerances for dioxolan-2-yl] methyl]-1H-1,2,4-triazole) residues. and its metabolites determined as 2,4- (a) General. (1) Tolerances are estab- dichlorobenzoic acid and expressed as lished for residues of deltamethrin, in- parent compound, in connection with cluding its metabolites and degradates, use of the pesticide under section 18 in or on the commodities listed in the emergency exemptions granted by following table. Compliance with the EPA. The tolerances will expire and tolerance levels specified is to be deter- are revoked on the dates specified in mined by measuring only the following table: deltamethrin, (1R,3R)-3-(2,2- dibromovinyl)-2,2- Expiration/ Commodity Parts per revocation dimethylcyclopropanecarboxylic acid million date (S)-alpha-cyano-3-phenoxybenzyl ester, Nectarine ...... 2.0 12/31/13 and its major metabolites, trans- Peach ...... 2.0 12/31/13 deltamethrin, (S)-alpha-cyano-m- phenoxybenzyl(1R,3S)-3-(2,2- (c) Tolerances with regional registra- dibromovinyl)-2,2- tions. A tolerance with regional reg- dimethylcyclopropanecarboxylate, and istration, as defined in § 180.1(l), is es- alpha-R-deltamethrin, (R)-alpha-cyano- tablished for residues of 1-[[2-(2,4- m-phenoxybenzyl-(1R,3R)-3-(2,2- dichlorophenyl)-4-propyl-1,3-dioxolan-2- dibromovinyl)-2,2- yl]methyl]-1H-1,2,4-triazole and its me- dimethylcyclopropanecarboxylate, in tabolites determined as 2,4- or on the commodity.

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higher tolerance as a result of use on Commodity Parts per million growing crops) when deltamethrin is Almond, hulls ...... 2.5 used in food/feed handling establish- Apple, wet pomace ...... 1.0 ments or as a wide-area mosquito Artichoke, globe ...... 0.5 adulticide. Compliance with the toler- Barley, bran ...... 5.0 Cattle, fat ...... 0.05 ance levels specified is to be deter- Cattle, meat ...... 0.02 mined by measuring only Cattle, meat byproducts ...... 0.05 deltamethrin, (1R,3R)-3-(2,2- Citrus, dried pulp * ...... 3.0 Citrus, oil * ...... 50 dibromovinyl)-2,2- Corn, field, forage ...... 0.7 dimethylcyclopropanecarboxylic acid Corn, field, refined oil ...... 2.5 (S)-alpha-cyano-3-phenoxybenzyl ester, Corn, field, stover ...... 5.0 and its major metabolites, trans- Corn, pop, stover ...... 5.0 Corn, sweet, forage ...... 10 deltamethrin, (S)-alpha-cyano-m- Corn, sweet, kernel plus cob with husks removed 0.03 phenoxybenzyl(1R,3S)-3-(2,2- Corn, sweet, stover ...... 15 dibromovinyl)-2,2- Cotton, refined oil ...... 0.2 Cotton, undelinted seed ...... 0.04 dimethylcyclopropanecarboxylate, and Egg ...... 0.02 alpha-R-deltamethrin, (R)-alpha-cyano- Fish—freshwater finfish ...... 0.01 m-phenoxybenzyl-(1R,3R)-3-(2,2- Fish—freshwater finfish, farm raised ...... 0.01 Fish—saltwater finfish, other ...... 0.01 dibromovinyl)-2,2- Fish—saltwater finfish, tuna ...... 0.01 dimethylcyclopropanecarboxylate, in Fruit, pome, Group 11 ...... 0.2 or on the commodity. Goat, fat ...... 0.05 (b) Section 18 emergency exemptions. Goat, meat ...... 0.02 Goat, meat byproducts ...... 0.05 [Reserved] Grain, aspirated fractions ...... 65 (c) Tolerances with regional registra- Grain, cereal, Group 15, except sweet corn ...... 1.0 tions. [Reserved] Hog, fat ...... 0.05 Horse, fat ...... 0.05 (d) Indirect or inadvertent residues. Horse, meat ...... 0.02 [Reserved] Horse, meat byproducts ...... 0.05 Lychee* ...... 0.2 [62 FR 63001, Nov. 26, 1997, as amended at 63 Milk, fat (reflecting 0.02 ppm in whole milk) ...... 0.1 FR 45414, Aug. 26, 1998; 69 FR 62614, Oct. 27, Nut, tree, Group 14 ...... 0.1 2004; 74 FR 46375, Sept. 9, 2009; 76 FR 34885, Onion, bulb ...... 0.1 June 15, 2011; 79 FR 66301, Nov. 7, 2014; 80 FR Onion, green ...... 1.5 16302, Mar. 27, 2015; 82 FR 18580, Apr. 20, 2017] Orange * ...... 0.30 Poultry, fat ...... 0.05 Poultry, meat ...... 0.02 § 180.436 Cyfluthrin and the isomer Poultry, meat byproducts ...... 0.02 beta-cyfluthrin; tolerances for resi- Radish, tops ...... 4.0 dues. Rapeseed ...... 0.2 Rice, hulls ...... 2.5 (a) General. (1) Tolerances are estab- Rye, bran ...... 5.0 lished for residues of the insecticide Sheep, fat ...... 0.05 cyfluthrin (cyano(4-fluoro-3- Sheep, meat ...... 0.02 Sheep, meat byproducts ...... 0.05 phenoxyphenyl)methyl-3-(2,2- Sorghum, grain, forage ...... 0.5 dichloroethenyl)-2,2dimethyl- Sorghum, grain, stover ...... 1.0 cyclopropane-carboxylate; CAS No. Soybean, seed ...... 0.1 68359–37–5) in or on the following raw Soybean, hulls ...... 0.2 Starfruit* ...... 0.2 agricultural commodities: Sunflower, seed ...... 0.1 Tomato ...... 0.2 Commodity Parts per Tomato, paste ...... 1.0 million Tomato, puree ...... 1.0 Alfalfa ...... 5.0 Vegetable, cucurbit, Group 9 ...... 0.2 Alfalfa, forage ...... 5.0 Vegetable, fruiting, Group 8 ...... 0.3 Alfalfa, hay ...... 13 Vegetable, root, except sugar beet, Subgroup IB 0.2 Almond, hulls ...... 0.5 Vegetable, tuberous and corm, Subgroup IC ...... 0.04 Barley, bran ...... 0.5 Wheat, bran ...... 5.0 Barley, grain ...... 0.15 * There are no U.S. registrations for use of deltamethrin on Beet, sugar, dried pulp ...... 1.0 starfruit and lychee. Beet, sugar, roots ...... 0.10 * There are no U.S. registrations. Brassica, head and stem, subgroup 5A ...... 2.5 Brassica, leafy greens, subgroup 5B ...... 7.0 (2) A tolerance of 0.05 ppm is estab- Buckwheat, grain ...... 0.15 lished for residues of the insecticide Carrot, roots ...... 0.20 deltamethrin, including its metabolites Cattle, fat ...... 2.0 Cattle, meat ...... 0.10 and degradates, in or on all food/feed Cattle, meat byproducts ...... 0.10 items (other than those covered by a Citrus, dried pulp ...... 0.3

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Parts per Parts per Commodity million Commodity million

Citrus, oil ...... 0.3 Tomato, wet pomace ...... 5.0 Corn, field, grain ...... 0.05 Triticale, grain ...... 0.15 Corn, pop, grain ...... 0.05 Turnip, greens ...... 7.0 Corn, sweet, kernel plus cob with husks removed 0.05 Vegetable, cucurbit, group 9 ...... 0.1 Cotton, hulls ...... 2.0 Vegetable, fruiting, group 8 ...... 0.5 Cotton, refined oil ...... 2.0 Vegetable, leafy, except brassica, group 4 ...... 6.0 Cotton, undelinted seed ...... 1.0 Egg ...... 0.01 Vegetable, tuberous and corm, subgroup 1C ...... 0.01 Fruit, citrus, group 10 ...... 0.2 Wheat, bran ...... 0.5 Fruit, pome, group 11 ...... 0.5 Wheat, grain ...... 0.15 Fruit, stone, group 12 ...... 0.3 Wheat, shorts ...... 0.5 Goat, fat ...... 2.0 Goat, meat ...... 0.05 (2) A tolerance of 0.05 ppm is estab- Goat, meat byproducts ...... 0.05 Grain, aspirated fractions ...... 150 lished for residues of the insecticide Grain, cereal, forage, fodder and hay, group 16, cyfluthrin (cyano(4-fluoro-3- forage, except rice ...... 25 phenoxyphenyl)methyl-3-(2,2- Grain, cereal, forage, fodder and hay, group 16, hay, except rice ...... 6.0 dichloroethenyl)-2,2- Grain, cereal, forage, fodder and hay, group 16, dimethylcyclopropanecarboxylate; stover, except rice ...... 30 CAS Reg. No. 69359–37–5) in food com- Grain, cereal, forage, fodder and hay, group 16, straw, except rice ...... 7.0 modities exposed to the insecticide Grape ...... 1.0 during treatment of food-handling es- Grape, raisin ...... 3.5 tablishments where food and food prod- Grass, forage, fodder and hay, group 17, forage 12 ucts are held, processed, prepared, or Grass, forage, fodder and hay, group 17, hay ...... 50 Hog, fat ...... 0.5 served. Treatments may be made by Hog, meat ...... 0.01 general surface, spot, and/or crack and Hog, meat byproducts ...... 0.01 crevice applications. Hop, dried cones ...... 20.0 Hop, vines ...... 4.0 (i) General surface treatments shall Horse, fat ...... 2.0 be limited to a maximum of 3.8 grams Horse, meat ...... 0.05 of active ingredient per 1,000 square Horse, meat byproducts ...... 0.05 feet, applying to walls, floors, and ceil- Lettuce, head ...... 2.0 Lettuce, leaf ...... 3.0 ings with a low-pressure system. Cover Milk ...... 0.2 or remove all food processing and/or Milk, fat ...... 5.0 handling equipment during applica- Millet, grain ...... 0.15 Mustard greens ...... 7.0 tion. Do not apply directly to food Nut, tree, group 14 ...... 0.01 products. Reapplications may be made Oat, bran ...... 0.5 at 10-day intervals. Oat, grain ...... 0.15 Pea and bean, dried shelled, except soybean, (ii) Crack and crevice or spot treat- subgroup 6C ...... 0.15 ments shall be limited to a maximum Pea, dry, seed ...... 0.15 of 0.1 percent of the active ingredient Pea, southern, succulent ...... 0.25 weight, applied with a low-pressure Peanut ...... 0.01 Peanut, hay ...... 6.0 system with a pinpoint or variable-pat- Pepper ...... 0.50 tern nozzle. Dust formulation shall be Pistachio ...... 0.01 limited to a maximum of 0.1 percent of Poultry, fat ...... 0.01 Poultry, meat ...... 0.01 the active ingredient by weight, ap- Poultry, meat byproducts ...... 0.01 plied using a hand duster, power dust- Radish, roots ...... 1.0 er, or other equipment capable of ap- Rye, bran ...... 0.5 plying dust insecticide directly into Rye, grain ...... 0.15 Sheep, fat ...... 2.0 voids and cracks and crevices. Dust ap- Sheep, meat ...... 0.05 plications should be made in a manner Sheep, meat byproducts ...... 0.05 to avoid deposits on exposed surfaces Sorghum, grain, grain ...... 3.5 Soybean, forage ...... 8.0 or introducing the material into the Soybean, hay ...... 4.0 air. Cover exposed food or remove food Soybean, seed ...... 0.03 from premises. Do not apply directly to Sugarcane, cane ...... 0.05 food. Reapplications may be made at Sugarcane, molasses ...... 0.20 Sunflower, forage ...... 5.0 10-day intervals. Sunflower, seed ...... 0.02 (iii) To ensure safe use of the insecti- Teosinte, grain ...... 0.05 cide, its label and labeling shall con- Tomato ...... 0.20 Tomato, dry pomace ...... 5.0 form to that registered by the Environ- Tomato, paste ...... 0.5 mental Protection Agency, and it shall

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be used in accordance with such label dimethylcyclopropanecarboxylate and and labeling. (S)-a-cyano-4-fluoro-3-phenoxybenzyl (3) A tolerance of 0.05 part per mil- (1R,3R)-3-(2,2-dichlorovinyl)-2,2- lion is established for residues of the dimethylcyclopropanecarboxylate with insecticide cyfluthrin (cyano(4-fluoro- the enantiomeric pair (R)-a-cyano-4- 3-phenoxyphenyl)methyl-3-(2,2- fluoro-3-phenoxybenzyl (1S,3R)-3-(2,2- dichloroethenyl)-2,2- dichlorovinyl)-2,2- dimethylcyclopropanecarboxylate; dimethylcyclopropanecarboxylate and CAS Reg. No. 68359–37–5) in feed com- (S)-a-cyano-4-fluoro-3-phenoxybenzyl modities exposed to the insecticide (1R,3S)-3-(2,2-dichlorovinyl)-2,2- during treatment of feed-handling es- dimethylcyclopropanecarboxylate], in tablishments where feed and feed prod- or on the following raw agricultural ucts are held, processed, prepared, or commodities: served. Treatments may be made by Parts per general surface, spot, and/or crack and Commodity million crevice applications. (i) General surface tratments shall be Alfalfa ...... 5.0 Alfalfa, forage ...... 5.0 limited to a maximum of 3.8 grams of Alfalfa, hay ...... 13 active ingredient per 1,000 square feet, Almond, hulls ...... 0.5 applying to walls, floors, and ceilings Barley, bran ...... 0.5 Barley, grain ...... 0.15 with a low-pressure system. Cover or Beet, sugar, dried pulp ...... 1.0 remove all feed processing and/or han- Beet, sugar, roots ...... 0.10 dling equipment during application. Do Brassica, head and stem, subgroup 5A ...... 2.5 not apply directly to feed products. Re- Brassica, leafy greens, subgroup 5B ...... 7.0 Buckwheat, grain ...... 0.15 applications may be made at 10-day in- Carrot, roots ...... 0.20 tervals. Cattle, fat ...... 2.0 (ii) Crack and crevice or spot treat- Cattle, meat ...... 0.10 Cattle, meat byproducts ...... 0.10 ments shall be limited to a maximum Citrus, dried pulp ...... 0.3 of 0.1 percent of the active ingredient Citrus, oil ...... 0.3 by weight, applied with a low-pressure Corn, field, grain ...... 0.05 Corn, pop, grain ...... 0.05 system with a pinpoint or variable-pat- Corn, sweet, kernel plus cob with husks removed 0.05 tern nozzle. Dust formulation shall be Cotton, hulls ...... 2.0 limited to a maximum of 0.1 percent of Cotton, refined oil ...... 2.0 Cotton, undelinted seed ...... 1.0 the active ingredient by weight, ap- Egg ...... 0.01 plied using a hand duster, power dust- Fruit, citrus, group 10 ...... 0.2 er, or other equipment capable of ap- Fruit, pome, group 11 ...... 0.5 plying dust insecticide directly into Fruit, stone, group 12 ...... 0.3 Goat, fat ...... 2.0 voids and cracks and crevices. Dust ap- Goat, meat ...... 0.05 plications should be made in a manner Goat, meat byproducts ...... 0.05 to avoid deposits on exposed surfaces Grain, aspirated fractions ...... 150 Grain, cereal, forage, fodder and hay, group 16, or introducing the material into the forage, except rice ...... 25 air. Cover exposed feed or remove feed Grain, cereal, forage, fodder and hay, group 16, from premises. Do not apply directly to hay, except rice ...... 6.0 Grain, cereal, forage, fodder and hay, group 16, feed. Reapplications may be made at stover, except rice ...... 30 10-day intervals. Grain, cereal, forage, fodder and hay, group 16, (iii) To ensure safe use of the insecti- straw, except rice ...... 7.0 cide, its label and labeling shall con- Grape ...... 1.0 Grape, raisin ...... 3.5 form to that registered by EPA, and it Grass, forage, fodder and hay, group 17, forage 12 shall be used in accordance with such Grass, forage, fodder and hay, group 17, hay ...... 50 label and labeling. Hog, fat ...... 0.5 Hog, meat ...... 0.01 (4) Tolerances are established for res- Hog, meat byproducts ...... 0.01 idues of the isomer, beta-cyfluthrin, Hop, dried cones ...... 20.0 cyano(4-fluoro-3- Hop, vines ...... 4.0 Horse, fat ...... 2.0 phenoxyphenyl)methyl-3-(2,2- Horse, meat ...... 0.05 dichloroethenyl)-2,2-dimethyl- Horse, meat byproducts ...... 0.05 cyclopropanecarboxylate [mixture Lettuce, head ...... 2.0 comprising the enantiomeric pair (R)- Lettuce, leaf ...... 3.0 Milk ...... 0.2 a-cyano-4-fluoro-3-phenoxybenzyl Milk, fat ...... 5.0 (1S,3S)-3-(2,2-dichlorovinyl)-2,2- Millet, grain ...... 0.15

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is to be determined by measuring only Commodity Parts per million imazamethabenz-methyl (methyl 2-[4,5- Mustard greens ...... 7.0 dihydro-4-methyl-4-(1-methylethyl)-5- Nut, tree, group 14 ...... 0.01 oxo-1H-imidazol-2-yl]-4- Oat, bran ...... 0.5 methylbenzoate) or (methyl 2-[4,5- Oat, grain ...... 0.15 Pea and bean, dried shelled, except soybean, dihydro-4-methyl-4-(1-methylethyl)-5- subgroup 6C ...... 0.15 oxo-1H-imidazol-2-yl]-5- Pea, dry, seed ...... 0.15 methylbenzoate), as the sum of its Pea, southern, succulent ...... 0.25 Peanut ...... 0.01 para- and meta-isomers in or on the Peanut, hay ...... 6.0 commodity. Pepper ...... 0.50 Pistachio ...... 0.01 Parts per Expiration/ Poultry, fat ...... 0.01 Commodity million revocation Poultry, meat ...... 0.01 date Poultry, meat byproducts ...... 0.01 Barley, grain ...... 0.10 12/31/16 Radish, roots ...... 1.0 Barley, straw ...... 2.00 12/31/16 Rye, bran ...... 0.5 Sunflower, seed ...... 0.10 12/31/16 Rye, grain ...... 0.15 Wheat, grain ...... 0.10 12/31/16 Sheep, fat ...... 2.0 Wheat, straw ...... 2.00 12/31/16 Sheep, meat ...... 0.05 Sheep, meat byproducts ...... 0.05 Sorghum, grain, grain ...... 3.5 (b) Section 18 emergency exemptions. Soybean, forage ...... 8.0 [Reserved] Soybean, hay ...... 4.0 (c) Tolerances with regional registra- Soybean, seed ...... 0.03 Sugarcane, cane ...... 0.05 tions. [Reserved] Sugarcane, molasses ...... 0.20 (d) Indirect or inadvertent residues. Sunflower, forage ...... 5.0 [Reserved] Sunflower, seed ...... 0.02 Teosinte, grain ...... 0.05 [81 FR 34906, June 1, 2016] Tomato ...... 0.20 Tomato, paste ...... 0.5 § 180.438 Lambda-cyhalothrin and an Tomato, pomace ...... 5.0 isomer gamma-cyhalothrin; toler- Triticale, grain ...... 0.15 Turnip, greens ...... 7.0 ances for residues. Vegetable, cucurbit, group 9 ...... 0.1 (a) General. (1) Tolerances are estab- Vegetable, fruiting, group 8 ...... 0.5 lished for the combined residues of the Vegetable, leafy greens, except Brassica, group 4 ...... 6.0 pyrethroid lambda-cyhalothrin, 1:1 Vegetable, tuberous and corm, subgroup 1C ...... 0.01 mixture of (S)-a-cyano-3- Wheat, bran ...... 0.5 phenoxybenzyl-(Z)-(1R,3R)-3-(2-chloro- Wheat, grain ...... 0.15 Wheat, shorts ...... 0.5 3,3,3-trifluoroprop-1-enyl)-2,2- dimethylcyclopropanecarboxylate and (b) Section 18 emergency exemptions. (R)-a-cyano-3-phenoxybenzyl-(Z)- [Reserved] (1S,3S)-3-(2-chloro-3,3,3-trifluoroprop-1- (c) Tolerances with regional registra- enyl)-2,2- tions. [Reserved] dimethylcyclopropanecarboxylate and (d) Indirect or inadvertent residues. its epimer expressed as epimer of lamb- [Reserved] da-cyhalothrin, a 1:1 mixture of (S)-a- cyano-3-phenoxybenzyl-(Z)-(1S,3S)-3-(2- [53 FR 1924, Jan. 25, 1988] chloro-3,3,3-trifluoroprop-1-enyl)-2,2- EDITORIAL NOTE: For FEDERAL REGISTER ci- dimethylcyclopropanecarboxylate and tations affecting § 180.436, see the List of CFR (R)-a-cyano-3-phenoxybenzyl-(Z)- Sections Affected, which appears in the (1R,3R)-3-(2-chloro-3,3,3-trifluoroprop-1- Finding Aids section of the printed volume enyl)-2,2- and at www.govinfo.gov. dimethylcyclopropanecarboxylate, on § 180.437 Imazamethabenz-methyl; tol- plants and livestocks, as indicated in erances for residues. the following table. (a) General. Tolerances are estab- Commodity Parts per lished for residues of the herbicide million imazamethabenz-methyl, including its Alfalfa, forage ...... 5.0 metabolites and degradates, in or on Alfalfa, hay ...... 6.0 the commodities in the table in this Almond, hulls ...... 1.5 Apple, wet pomace ...... 2.50 paragraph. Compliance with the toler- Avocado, imported ...... 0.20 ance levels specified in this paragraph Barley, bran ...... 0.2

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Parts per Parts per Commodity million Commodity million

Barley, grain ...... 0.05 Sunflower, seed ...... 0.2 Barley, hay ...... 2.0 Tomato ...... 0.1 Barley, straw ...... 2.0 Tomato, dry pomace ...... 6.0 Brassica, head and stem, subgroup 5A ...... 0.4 Tomato, wet pomace ...... 6.0 Buckwheat, grain ...... 0.05 Vegetable, cucurbit, group 9 ...... 0.05 Canola, refined oil ...... 2.0 Vegetable, fruiting, group 8 ...... 0.20 Canola, seed ...... 1.0 Vegetable, legume, edible podded, subgroup 6A 0.20 Cattle, fat ...... 3.0 Vegetable, tuberous and corm, subgroup 1C ...... 0.02 Cattle, meat ...... 0.2 Wheat, grain ...... 0.05 Cattle, meat byproducts ...... 0.2 Wheat, forage ...... 2.0 Corn, field, flour ...... 0.15 Wheat, hay ...... 2.0 Corn, field, forage ...... 6.0 Wheat, straw ...... 2.0 Corn, field, grain ...... 0.05 Wheat, bran ...... 0.2 Corn, field, stover ...... 1.0 Corn, pop, grain ...... 0.05 (2) Tolerances 1 are established for Corn, pop, grain, flour ...... 0.05 Corn, pop, stover ...... 1.0 the combined residues of the Corn, sweet, forage ...... 6.0 pyrethroid [gamma-cyhalothrin (the Corn, sweet, stover ...... 1.0 isolated active isomer of lambda- Corn, sweet, kernel plus cob with husks removed 0.05 cyhalothrin) (S)-′-cyano-3- Cotton, undelinted seed ...... 0.05 Egg ...... 0.01 phenoxybenzyl (Z)-(1R,3R)-3-(2-chloro- Fruit, pome, group 11 ...... 0.30 3,3,3-trifluoroprop-1-enyl)-2,2- Fruit, stone, group 12 ...... 0.50 dimethylcyclopropanecarboxylate)) Garlic ...... 0.1 ′ Goat, fat ...... 3.0 and its epimer (R)- -cyano-3- Goat, meat ...... 0.2 phenoxybenzyl (Z)-(1R,3R)-3-(2-chloro- Goat, meat byproducts ...... 0.2 3,3,3-trifluoroprop-1-enyl)-2,2- Grain, aspirated fractions ...... 2.0 dimethylcyclopropanecarboxylate in/ Grass, forage, fodder and hay, group 17 ...... 7.0 Hog, fat ...... 0.2 on the following commodities: Hog, meat ...... 0.01 Hog, meat byproducts ...... 0.02 Commodity Parts per Hop, dried cones ...... 10.0 million Horse, fat ...... 3.0 Alfalfa, forage ...... 5 Horse, meat ...... 0.2 Alfalfa, hay ...... 6 Horse, meat byproducts ...... 0.2 Almond, hulls ...... 1.5 Lettuce, head ...... 2.0 Apple, pomace, wet ...... 2.50 Lettuce, leaf ...... 2.0 Avocado, imported ...... 0.20 Milk, fat (reflecting 0.4 ppm in whole milk) ...... 10.0 Brassica, head and stem, subgroup 5A ...... 0.4 Nut, tree, group 14 ...... 0.05 Canola, seed ...... 0.15 Oat, grain ...... 0.05 Cattle, fat ...... 3 Oat, forage ...... 2.0 Cattle, meat ...... 0.2 Oat, hay ...... 2.0 Cattle, meat byproducts ...... 0.2 Oat, straw ...... 2.0 Corn, field, flour ...... 0.15 Onion, bulb ...... 0.1 Corn, field, forage ...... 6.0 Pea and bean, dried shelled, except soybean, Corn, field, grain ...... 0.05 subgroup 6C ...... 0.10 Corn, field, stover ...... 1.0 Pea and bean, succulent shelled, subgroup 6B ... 0.01 Corn, pop, grain ...... 0.05 Peanut ...... 0.05 Corn, pop, stover ...... 1.0 Peanut, hay ...... 3.0 Corn, sweet, forage ...... 6.0 Pistachio ...... 0.05 Corn, sweet, kernel plus cob with husks removed 0.05 Poultry, fat ...... 0.03 Corn, sweet, stover ...... 1.0 Poultry, meat ...... 0.01 Cotton, undelinted seed ...... 0.05 Poultry, meat byproducts ...... 0.01 Egg ...... 0.01 Rice, grain ...... 1.0 Fruit, pome, group 11 ...... 0.30 Rice, hulls ...... 5.0 Fruit, stone, group 12 ...... 0.50 Rice, wild, grain ...... 1.0 Garlic ...... 0.10 Rye, bran ...... 0.2 Goat, fat ...... 3.0 Rye, grain ...... 0.05 Goat, meat ...... 0.2 Rye, forage ...... 2.0 Goat, meat byproducts ...... 0.2 Rye, straw ...... 2.0 Grain, aspirated fractions ...... 2.0 Sheep, fat ...... 3.0 Hog, fat ...... 3.0 Sheep, meat ...... 0.2 Hog, meat ...... 0.2 Sheep, meat byproducts ...... 0.2 Hog, meat byproducts ...... 0.2 Soybean ...... 0.01 Horse, fat ...... 3.0 Sorghum, grain, grain ...... 0.2 Horse, meat ...... 0.2 Sorghum, grain, forage ...... 0.30 Horse, meat byproducts ...... 0.2 Sorghum, grain, stover ...... 0.50 Lettuce, head ...... 2.0 Sugarcane, cane ...... 0.05 Lettuce, leaf ...... 2.0 Sunflower, forage ...... 0.2 Milk, fat (reflecting 0.20 ppm in whole milk) ...... 5.0 Sunflower, seed, hulls ...... 0.50 Nut, tree, group 14 ...... 0.05 Sunflower, refined oil ...... 0.30 Okra ...... 0.20

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Compliance with the tolerance levels Commodity Parts per million specified in the following table [below] Onion, bulb ...... 0.1 is to be determined by measuring only Pea and bean, dried shelled, except soybean, thifensulfuron methyl (methyl 3-[[[[(4- subgroup 6C ...... 0.10 methoxy-6-methyl-1,3,5-triazin-2- Pea and bean, succulent shelled, subgroup 6B ... 0.01 Peanut ...... 0.05 yl)amino]carbonyl]amino] sulfonyl]-2- Peanut, hay ...... 3.0 thiophenecarboxylate). Pistachio ...... 0.05 Poultry, fat ...... 0.03 Parts per Poultry, meat ...... 0.01 Commodity million Poultry, meat byproducts ...... 0.01 Rice, grain ...... 1.0 Barley, grain ...... 0.05 Rice, hulls ...... 5.0 Barley, hay ...... 0.8 Sheep, fat ...... 3.0 Barley, straw ...... 0.10 Sheep, meat ...... 0.2 Canola, seed ...... 0.02 Sheep, meat byproducts ...... 0.2 Sorghum, grain, forage ...... 0.30 Chicory, roots ...... 0.01 Sorghum, grain, grain ...... 0.20 Chicory, tops ...... 0.01 Sorghum, grain, stover ...... 0.50 Corn, field, forage ...... 0.10 Soybean ...... 0.01 Corn, field, grain ...... 0.05 Sugarcane ...... 0.05 Corn, field, stover ...... 0.10 Sunflower, forage ...... 0.20 Cotton, gin byproducts ...... 0.02 Sunflower, refined oil ...... 0.30 Cotton, undelinted seed ...... 0.02 Sunflower, seed ...... 0.20 Flax, seed ...... 0.02 Sunflower, seed, hulls ...... 0.50 Tomato ...... 0.10 Oat, forage ...... 0.2 Tomato, dry pomace ...... 6.0 Oat, grain ...... 0.05 Tomato, wet pomace ...... 6.0 Oat, hay ...... 0.05 Vegetables, fruiting, group 8 ...... 0.20 Oat, straw ...... 0.10 Vegetable, legume, edible podded, subgroup 6A 0.20 Rice, grain ...... 0.05 Wheat, bran ...... 2.0 Sorghum, grain, forage...... 0.05 Wheat, forage ...... 2.0 Sorghum, grain, grain ...... 0.05 Wheat, grain ...... 0.05 Sorghum, grain, stover ...... 0.05 Wheat, hay ...... 2.0 Soybean ...... 0.10 Wheat, straw ...... 2.0 Wheat, forage ...... 2.5 1 The analytical enforcement methods for lambda- Wheat, grain ...... 0.05 cyhalothrin are applicable for determination of gamma- Wheat, hay ...... 0.7 cyhalothrin residues in plant and animal commodities. Wheat, straw ...... 0.10 (3) A tolerance of 0.01 part per million is established for residues of the (b) Section 18 emergency exemptions. insecticide lamba-cyhalothrin and an [Reserved] isomer gamma-cyhalothrin in or on all (c) Tolerances with regional registra- food commodities (other than those al- tions. Tolerances are established for ready covered by a higher tolerance as residues of thifensulfuron methyl, in- a result of use on growing crops) in cluding its metabolites and degradates, food-handling establishments where in or on the commodities listed in the food products are held, processed, or following table [below]. Compliance prepared. with the tolerance levels specified in (b) Section 18 emergency exemptions. the following table [below] is to be de- [Reserved] termined by measuring only (c) Tolerances with regional registra- thifensulfuron methyl (methyl 3-[[[[(4- tions. [Reserved] methoxy-6-methyl-1,3,5-triazin-2- (d) Indirect or inadvertent residues. yl)amino]carbonyl]amino] sulfonyl]-2- [Reserved] thiophenecarboxylate). [71 FR 74817, Dec. 13, 2006, as amended at 72 Parts per FR 45663, Aug. 15, 2007; 73 FR 39264, July 9, Commodity million 2008; 76 FR 34885, June 15, 2011; 80 FR 72599, Nov. 20, 2015] Safflower, seed ...... 0.05

§ 180.439 Thifensulfuron methyl; toler- (d) Indirect or inadvertent residues. ances for residues. [Reserved] (a) General. Tolerances are estab- [69 FR 55982, Sept. 17, 2004, as amended at 69 lished for residues of thifensulfuron FR 63957, Nov. 3, 2004; 72 FR 13184, Mar. 21, methyl, including its metabolites and 2007; 73 FR 47075, Aug. 13, 2008; 75 FR 19277, degradates, in or on the commodities Apr. 14, 2010; 77 FR 52240, Aug. 29, 2012; 80 FR listed in the following table [below]. 72599, Nov. 20, 2015]

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§ 180.440 Tefluthrin; tolerances for res- Commodity Parts per idues. million (a) General. Tolerances are estab- Cotton, undelinted seed ...... 0.1 lished for the combined residues of the Cowpea, forage ...... 3.0 Cowpea, hay ...... 3.0 insecticide tefluthrin (2,3,5,6 Crambe, meal ...... 2.0 tetrafluroro-4-methylphenyl)methyl-(1 Flax, seed ...... 0.05 alpha, 3 alpha)-(Z)-(±)-3(2-chloro-3,3,3- Gold of pleasure, meal ...... 2.0 Lentil, seed ...... 0.05 trifluoro-1-propenyl)-2,2- Pea, dry ...... 0.25 diemthylcyclopropanecarboxylate) and Pea, field, hay ...... 3.0 its metabolite (Z)-3-(2-chloro-3,3,3- Pea, field, vines ...... 3.0 Pea, succulent ...... 0.3 trifluroro-1-propenyl)-2,2- Peppermint, tops ...... 2.0 dimethylcyclopropanecarboxylic acid Rapeseed, meal ...... 2.0 in or on the following commodities: Rapeseed subgroup 20A, except flax, seed ...... 1.5 Rice, grain ...... 0.05 Parts per Sorghum, grain, aspirated grain fractions ...... 1.0 Commodity million Sorghum, grain, forage ...... 0.20 Sorghum, grain, grain ...... 0.20 Corn, field, forage ...... 0.06 Sorghum, grain, stover ...... 0.30 Corn, field, grain ...... 0.06 Soybean, flour ...... 0.5 Corn, field, stover ...... 0.06 Soybean, hulls ...... 0.02 Corn, pop, grain ...... 0.06 Soybean, meal ...... 0.5 Corn, pop, stover ...... 0.06 Soybean, seed ...... 0.05 Corn, sweet, forage ...... 0.06 Spearmint, tops ...... 2.0 Corn, sweet, kernel plus cob with husks removed 0.06 Sunflower, seed ...... 1.9 Corn, sweet, stover ...... 0.06 Wheat, forage ...... 2.0 Wheat, germ ...... 0.40 (b) Section 18 emergency exemptions. Wheat, grain ...... 0.05 Wheat, hay ...... 2.0 [Reserved] Wheat, milled byproducts ...... 0.40 (c) Tolerances with regional registra- Wheat, straw ...... 0.80 tions. [Reserved] (d) Indirect or inadvertent residues. (2) Tolerances are established for res- [Reserved] idues of the herbicide quizalofop ethyl, including its metabolites and [62 FR 62961, Nov. 26, 1997, as amended at 74 FR 46375, Sept. 9, 2009] degradates, in or on the commodities in the following table. Compliance with § 180.441 Quizalofop ethyl; tolerances the tolerance levels specified in the fol- for residues. lowing table is to be determined by (a) General. (1) Tolerances are estab- measuring only those quizalofop ethyl lished for residues of the herbicide residues convertible to quizalofop (2-[4- quizalofop ethyl, including its metabo- (6-chloroquinoxalin-2-yl- lites and degradates, in or on the com- oxy)phenoxy]propanoic acid), expressed modities in the following table. Com- as quizalofop, in or on the commodity. pliance with the tolerance levels speci- Parts per fied in the following table is to be de- Commodity million termined by measuring only those Cattle, fat ...... 0.05 quizalofop ethyl residues convertible to Cattle, meat ...... 0.02 2-methoxy-6-chloroquinoxaline, ex- Cattle, meat byproducts ...... 0.05 pressed as the stoichiometric equiva- Egg ...... 0.02 Goat, fat ...... 0.05 lent of quizalofop ethyl, in or on the Goat, meat ...... 0.02 commodity. Goat, meat byproducts ...... 0.05 Hog, fat ...... 0.05 Commodity Parts per Hog, meat ...... 0.02 million Hog, meat byproducts ...... 0.05 Horse, fat ...... 0.05 Barley, grain ...... 0.05 Horse, meat ...... 0.02 Barley, hay ...... 0.05 Horse, meat byproducts ...... 0.05 Barley, straw ...... 0.05 Milk ...... 0.01 Bean, dry, seed ...... 0.4 Milk, fat ...... 0.25 Bean, succulent ...... 0.25 Poultry, fat ...... 0.05 Beet, sugar, molasses ...... 0.2 Poultry, meat ...... 0.02 Beet, sugar, roots ...... 0.1 Poultry, meat byproducts ...... 0.05 Beet, sugar, tops ...... 0.5 Sheep, fat ...... 0.05 Corn, field, forage ...... 0.02 Sheep, meat ...... 0.02 Corn, field, grain ...... 0.02 Sheep, meat byproducts ...... 0.05 Corn, field, stover ...... 0.03

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(3) Tolerances are established for res- Commodity Parts per idues of the herbicide quizalofop-P- million ethyl, including its metabolites and Almond, hulls ...... 2.0 degradates, in or on the commodities Artichoke, globe ...... 1.0 in the following table. Compliance with Banana 1 ...... 0.1 Beet, garden, roots ...... 0.45 the tolerance levels specified in the fol- Beet, garden, tops ...... 15 lowing table is to be determined by Brassica, head and stem, subgroup 5A, except measuring quizalofop ethyl and cabbage ...... 0.6 Brassica, leafy greens, subgroup 5B ...... 3.5 quizalofop acid, expressed as the stoi- Bushberry subgroup 13-07B ...... 1.8 chiometric equivalent of quizalofop Cabbage ...... 4.0 ethyl, in or on the commodity. Caneberry subgroup 13A ...... 1.0 Cattle, fat ...... 1.0 Parts per Cattle, meat byproducts ...... 0.10 Commodity million Cattle, meat ...... 0.5 Coriander, dried leaves ...... 25 Fish-shellfish, crustacean ...... 0.04 Coriander, leaves ...... 6.0 Coriander, seed ...... 5.0 Corn, field, forage ...... 3.0 (b) Section 18 emergency exemptions. Corn, field, grain ...... 0.05 [Reserved] Corn, field, stover ...... 5.0 (c) Tolerances with regional registra- Corn, pop, grain ...... 0.05 Corn, pop, stover ...... 5.0 tions. Tolerances with regional reg- Corn, sweet, forage ...... 3.0 istration are established for residues of Corn, sweet, kernel plus cob with husk removed 0.05 the herbicide quizalofop ethyl, includ- Corn, sweet, stover ...... 5.0 Cotton, undelinted seed ...... 0.5 ing its metabolites and degradates, in Eggplant ...... 0.05 or on the commodities in the following Egg ...... 0.05 table. Compliance with the tolerance Fruit, citrus, group 10 ...... 0.05 levels specified in the following table is Goat, fat ...... 1.0 Goat, meat byproducts ...... 0.10 to be determined by measuring only Goat, meat ...... 0.5 those quizalofop ethyl residues con- Grain, aspirated fractions ...... 70 vertible to 2-methoxy-6- Grape ...... 0.2 Groundcherry ...... 0.5 chloroquinoxaline, expressed as the Herb subgroup 19A ...... 0.05 stoichiometric equivalent of quizalofop Hog, fat ...... 1.0 ethyl, in or on the commodity. Hog, meat byproducts ...... 0.10 Hog, meat ...... 0.5 Parts per Hop, dried cones ...... 10.0 Commodity million Horse, fat ...... 1.0 Horse, meat byproducts ...... 0.10 Pineapple ...... 0.1 Horse, meat ...... 0.5 Leafy petioles subgroup 4B ...... 3.0 Lettuce, head ...... 3.0 (d) Indirect or inadvertent residues. Mayhaw ...... 1.4 [Reserved] Milk, fat (reflecting 0.1 ppm in whole milk) ...... 1.0 Nut, tree, group 14 ...... 0.05 [63 FR 32759, June 16, 1998, as amended at 70 Okra ...... 0.50 FR 7870, Feb. 16, 2005; 71 FR 56378, Sept. 27, Pea and bean, dried shelled, expect soybean, 2006; 76 FR 56045, Sept. 15, 2010; 77 FR 23630, subgroup 6C ...... 0.15 Apr. 20, 2012; 80 FR 72599, Nov. 20, 2015; 81 FR Pea and bean, succulent shelled, subgroup 6B ... 0.05 Peanut ...... 0.05 86586, Dec. 1, 2016; 83 FR 7115, Feb. 20, 2018; 83 Pear ...... 0.5 FR 8011, Feb. 23, 2018] Pepino ...... 0.5 Pepper, bell ...... 0.5 § 180.442 Bifenthrin; tolerances for res- Pepper, nonbell ...... 0.5 idues. Pistachio ...... 0.05 Poultry, fat ...... 0.05 (a) General. (1) Tolerances are estab- Poultry, meat byproducts ...... 0.05 lished for residues of the insecticide Poultry, meat ...... 0.05 Radish, tops ...... 4.5 bifenthrin, including its metabolites Rapeseed, seed ...... 0.05 and degradates, in or on the commod- Sheep, fat ...... 1.0 ities in the table below. Compliance Sheep, meat byproducts ...... 0.1 with the tolerance levels specified Sheep, meat ...... 0.5 Soybean, hulls ...... 0.50 below is to be determined by measuring Soybean, refined oil ...... 0.30 only bifenthrin, (2-methyl [1,1′- Soybean, seed ...... 0.2 biphenyl]-3-yl) methyl-3-(2-chloro- Spinach ...... 0.2 Strawberry ...... 3.0 3,3,3,-trifluoro-1-propenyl)-2,2- Tea, dried 1 ...... 30 dimethylcyclopropanecarboxylate. Tomato ...... 0.15

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(b) Section 18 emergency exemptions. Commodity Parts per million Time-limited tolerances specified in Turnip, greens ...... 3.5 the following table are established for Vegetable, cucurbit, group 9 ...... 0.4 residues of the bifenthrin, (2- Vegetable, legume, edible podded, subgroup 6A 0.6 methyl[1,1′-biphenyl]-3-yl)methyl-3-(2- Vegetable, root, subgroup 1B except sugar beet chloro-3,3,3-trifluoro-1-propenyl)-2,2- and garden beet ...... 0.10 Vegetable, tuberous and corm, subgroup 1C ...... 0.05 dimethylcyclopropane-carboxylate) in or on the specified agricultural com- 1 There are no U.S. registrations. modities, resulting from use of the pes- (2) A tolerance of 0.05 ppm is estab- ticide pursuant to FIFRA section 18 lished for residues of the insecticide emergency exemptions. The tolerances bifenthrin, (2-methyl[1,1′-biphenyl]-3- expire on the date specified in the yl)methyl-3-(2-chloro-3,3,3-trifluoro-1- table. propenyl)-2,2-dimethylcyclopropanecarboxylate, as follows: Parts per Expiration Commodity million date (i) In or on all food/feed items (other than those covered by a higher toler- Apple ...... 0.5 12/31/21 ance as a result of use on growing Avocado ...... 0.50 12/31/19 Nectarine ...... 0.5 12/31/21 crops) in food/feed handling establish- Peach ...... 0.5 12/31/21 ments. Pomegranate ...... 0.50 12/31/22 (ii) The insecticide may be present as a residue from application of bifenthrin (c) Tolerances with regional registra- in food handling establishments, in- tions. Tolerances with regional reg- cluding food service, manufacturing istrations are established for residues and processing establishments, such as of the insecticide bifenthrin, including restaurants, cafeterias, supermarkets, its metabolites and degradates, in or bakeries, breweries, dairies, meat on the commodities in the table below. slaughtering and packing plants, and Compliance with the tolerance levels canneries, feed handling establish- specified below is to be determined by ments including feed manufacturing measuring only bifenthrin, (2-methyl and processing establishments, in ac- [1,1′-biphenyl]-3-yl) methyl-3-(2-chloro- cordance with the following prescribed 3,3,3,-trifluoro-1-propenyl)-2,2- conditions: dimethylcyclopropanecarboxylate. (A) Application shall be limited to Parts per general surface and spot and/or crack Commodity million and crevice treatment in food/feed handling establishments where food/feed Grass, forage ...... 4 .0 and food/feed products are held, proc- Grass, hay ...... 15 essed, prepared and served. General surface application may be used only (d) Indirect or inadvertent residues. when the facility is not in operation [Reserved] provided exposed food/feed has been [62 FR 31002, June 6, 1997] covered or removed from the area EDITORIAL NOTE: For FEDERAL REGISTER ci- being treated. Spot and/or crack and tations affecting § 180.442, see the List of CFR crevice application may be used while Sections Affected, which appears in the the facility is in operation provided ex- Finding Aids section of the printed volume posed food/feed is covered or removed and at www.govinfo.gov. from the area being treated prior to application. Spray concentration shall be § 180.443 Myclobutanil; tolerances for limited to a maximum of 0.06 percent residues. active ingredient. Contamination of (a) General. Tolerances are estab- food/feed or food/feed contact surfaces lished for combined residues of the fun- shall be avoided. gicide myclobutanil alpha-butyl-alpha- (B) To assure safe use of the insecti- (4-chlorophenyl)-1H-1,2,4-triazole-1- cide, its label and labeling shall con- propanenitrile and its alcohol metabo- form to that registered with the U.S. lite (alpha-(3-hydroxybutyl)-alpha-(4- Environmental Protection Agency and chlorophenyl)-1H-1,2,4-triazole-1- shall be used in accordance with such propanenitrile (free and bound), in or label and labeling. on the following food commodities:

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(b) Section 18 emergency exemptions. Commodity Parts per million [Reserved] Almond ...... 0.1 (c) Tolerances with regional registra- Almond, hulls ...... 2.0 tions. [Reserved] Apple ...... 0.5 (d) Indirect or inadvertent residues. Apple, dry pomace ...... 5.0 Apple, wet pomace ...... 5.0 Tolerances are established for residues Artichoke, globe ...... 0.90 of the fungicide myclobutanil alpha- Asparagus ...... 0.02 butyl-alpha-(4-chlorophenyl)-1H-1,2,4- Banana, postharvest ...... 4.0 triazole-1-propanenitrile in or on the Bean, snap, succulent ...... 1.0 Caneberry subgroup 13A ...... 2.0 following food commodities: Canistel ...... 3.0 Cattle, fat ...... 0.05 Commodity Parts per Cattle, liver ...... 1.0 million Cattle, meat ...... 0.1 Cattle, meat byproducts, except liver ...... 0.2 Animal feed, nongrass, group 18 ...... 0.03 Cherry, sweet ...... 5.0 Grain, cereal, forage, fodder and straw, group 16 0.03 Cherry, tart ...... 5.0 Grain, cereal, group 15 ...... 0.03 Cilantro, leaves ...... 9.0 Vegetable, brassica, leafy, group 5 ...... 0.03 Cotton, undelinted seed ...... 0.02 Vegetable, foliage of legume, group 7 ...... 0.03 Currant ...... 3.0 Vegetable, fruiting, group 8 ...... 0.03 Egg ...... 0.02 Vegetable, leafy, except brassica, group 4 ...... 0.03 Fruit, stone, except cherry ...... 2.0 Vegetable, leaves of root and tuber, group 2 ...... 0.03 Goat, fat ...... 0.05 Vegetable, legume, group 6 ...... 0.03 Goat, liver ...... 1.0 Vegetable, root and tuber, group 1 ...... 0.03 Goat, meat ...... 0.1 Goat, meat byproducts, except liver ...... 0.2 Gooseberry ...... 2.0 [54 FR 6131, Feb. 8, 1989] Grain, aspirated fractions ...... 35 EDITORIAL NOTE: For FEDERAL REGISTER ci- Grape ...... 1.0 Grape, dried pomace ...... 10.0 tations affecting § 180.443, see the List of CFR Grape, raisin ...... 10.0 Sections Affected, which appears in the Grape, raisin, waste ...... 25.0 Finding Aids section of the printed volume Grape, wet pomace ...... 10.0 and at www.govinfo.gov. Hog, fat ...... 0.05 Hog, liver ...... 1.0 § 180.444 Sulfur dioxide; tolerances for Hog, meat ...... 0.1 Hog, meat byproducts, except liver ...... 0.2 residues. Hop, dried cones ...... 10 (a) General. A tolerance is established Horse, fat ...... 0.05 Horse, liver ...... 1.0 as follows for sulfite residues of the Horse, meat ...... 0.1 fungicide sulfur dioxide (determined as Horse, meat byproducts, except liver ...... 0.2 (SO2)) in or on the following raw agri- Leafy greens, subgroup 4A, except spinach ...... 9.0 cultural commodity(ies): Mango ...... 3.0 Mayhaw ...... 0.70 Parts per Milk ...... 0.2 Commodity million Okra ...... 4.0 Papaya ...... 3.0 Grape, postharvest ...... 10.0 Peppermint, tops ...... 3.0 Plum, prune, dried ...... 8.0 Poultry, fat ...... 0.02 (b) Section 18 emergency exemptions. Poultry, meat ...... 0.02 Time-limited tolerances specified in Poultry, meat byproducts ...... 0.02 the following table are established for Sapodilla ...... 3.0 Sapote, black ...... 3.0 residues of sulfur dioxide, including its Sapote, mamey ...... 3.0 metabolites and degradates in or on Sheep, fat ...... 0.05 the specified agricultural commodities, Sheep, liver ...... 1.0 resulting from use of the pesticide pur- Sheep, meat ...... 0.1 Sheep, meat byproducts, except liver ...... 0.2 suant to FFIFRA section 18 emergency Soybean, forage ...... 3.5 exemptions. Compliance with the toler- Soybean, hay ...... 15 ance levels specified below is to be de- Soybean, refined oil ...... 0.40 Soybean, seed ...... 0.25 termined by measuring only sulfur di- Spearmint, tops ...... 3.0 oxide (SO2). The tolerances expire on Star apple ...... 3.0 the date specified in the table. Strawberry ...... 0.50 Tomato ...... 0.30 Expiration/ Tomato, puree ...... 0.50 Parts per Commodity million revocation Tomato, paste ...... 1.0 date Vegetable, cucurbit, group 9 ...... 0.20 Vegetable, fruiting, group 8, except tomato ...... 4.0 Fig ...... 10 12/31/14

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(c) Tolerances with regional registra- (2) Tolerances are established for res- tions. [Reserved] idues of the insecticide clofentezine, (d) Indirect or inadvertent residues. including its metabolites and [Reserved] degradates, in or on the commodities in the table in this paragraph. Compli- [54 FR 20126, May 10, 1989, as amended at 76 FR 56648, Sept. 14, 2011] ance with the tolerance levels specified in this paragraph is to be determined § 180.445 Bensulfuron methyl; toler- by measuring only the sum of ances for residues. clofentezine, 3,6-bis(2-chlorophenyl)- (a) General. Tolerances are estab- 1,2,4,5-tetrazine, and its metabolite, 3- lished for residues of the herbicide (2-chloro-4-hydroxyphenyl)-6-(2- bensulfuron methyl (methyl-2[[[[[(4,6- chlorophenyl)-1,2,4,5-tetrazine, cal- dimethoxy-pyrimidin-2-yl) amino] car- culated as the stoichiometric equiva- bonyl] amino] sulfonyl] methyl] ben- lent of clofentezine, in or on com- zoate) in or on the following raw agri- modity. cultural commodities: Parts per Commodity million Commodity Parts per million Cattle, fat ...... 0.05 Cattle, liver ...... 0.4 Crayfish ...... 0.05 Cattle, meat ...... 0.05 Rice, grain ...... 0.02 Cattle, meat byproducts, except liver ...... 0.05 Goat, fat ...... 0.05 (b) Section 18 emergency exemptions. Goat, liver ...... 0.4 [Reserved] Goat, meat ...... 0.05 Goat, meat byproducts, except liver ...... 0.05 (c) Tolerances with regional registra- Hog, fat ...... 0.05 tions. [Reserved] Hog, liver ...... 0.4 (d) Indirect or inadvertent residues. Hog, meat ...... 0.05 [Reserved] Hog, meat byproducts, except liver ...... 0.05 Horse, fat ...... 0.05 [63 FR 9435, Feb. 25, 1998, as amended at 80 Horse, liver ...... 0.4 FR 72599, Nov. 20, 2015] Horse, meat ...... 0.05 Horse, meat byproducts, except liver ...... 0.05 Milk ...... 0.01 § 180.446 Clofentezine; tolerances for Sheep, fat ...... 0.05 residues. Sheep, liver ...... 0.4 (a) General. (1) Tolerances are estab- Sheep, meat ...... 0.05 Sheep, meat byproducts, except liver ...... 0.05 lished for residues of the insecticide clofentezine, including its metabolites (b) Section 18 emergency exemptions. and degradates, in or on the commod- [Reserved] ities in the table in this paragraph. (c) Tolerances with regional registra- Compliance with the tolerance levels tions. [Reserved] specified in this paragraph is to be de- (d) Indirect or inadvertent residues. termined by measuring only [Reserved] clofentezine, 3,6-bis(2-chlorophenyl)- 1,2,4,5-tetrazine, in or on the com- [56 FR 15503, Apr. 17, 1991, as amended at 56 modity. FR 22335, May 15, 1991; 59 FR 26947, May 25, 1994; 60 FR 12709, Mar. 8, 1995; 64 FR 19050, Parts per Apr. 19, 1999; 70 FR 11572, Mar. 9, 2005; 74 FR Commodity million 46375, Sept. 9, 2009; 76 FR 23496, Apr. 27, 2011; 81 FR 38609, June 14, 2016; 84 FR 24726, May Almond, hulls ...... 5.0 29, 2019] Almond ...... 0.5 Apple, dry pomace ...... 3.0 Apple, wet pomace ...... 3.0 § 180.447 Imazethapyr; tolerances for Apricot ...... 1.0 residues. Avocado ...... 0.30 Cherry, subgroup 12–12A ...... 1.0 (a) General. (1) Tolerances are estab- Fruit, pome, group 11–10 ...... 0.50 lished for residues of the herbicide Fruit, small, vine climbing, except fuzzy kiwifruit, imazethapyr, 2-[4,5-dihydro-4-methyl-4- Subgroup 13–07F ...... 1.0 (1-methylethyl)-5-oxo- 1H-imidazol-2- Guava ...... 3 Persimmon ...... 0.05 yl]-5-ethyl-3-pyridine carboxylic acid, Papaya ...... 0.30 applied as its acid or ammonium salt, Peach, subgroup 12–12B ...... 1.0 in or on the following raw agricultural Walnut ...... 0.02 commodities:

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chapter, are established for the sum of Commodity Parts per million residues of the herbicide imazethapyr, Canola, seed 1 ...... 0.10 2- [4,5-dihydro-4-methyl-4-(1- Soybean ...... 0.1 methylethyl)-5-oxo-1H-imidazol-2-yl]-5- Vegetable, legume, group 6 ...... 0.1 ethyl- 3-pyridine carboxylic acid, as its 1 There are no U.S. registrations for canola as of March ammonium salt, and its metabolite, 2- 21, 2003. [4,5-dihydro-4-methyl-4-(1- (2) Tolerances are established for the methylethyl)-5-oxo-1H-imidazol-2-yl]-5- sum of the residues of the herbicide (1- hydroxyethyl)-3-pyridine carboxylic imazethapyr, 2-[4,5-dihydro-4-methyl-4- acid, both free and conjugated, applied (1-methylethyl)-5-oxo- 1H-imidazol-2- as its acid or ammonium salt, in or on yl]-5-ethyl-3-pyridine carboxylic acid; the following raw agricultural com- its metabolite CL 288511, 2-[4,5-dihydro- modities: 4-methyl-4-(1-methylethyl)-5-oxo-1H- Parts per imidazol-2-yl]-5-(1-hydroxyethyl)-3-pyr- Commodity million idine carboxylic acid; and its metabolite CL 182704, 5-[1-(beta-D- Endive ...... 0.1 Lettuce, head ...... 0.1 glucopyranosyloxy)ethyl]-2-[4,5- Lettuce, leaf ...... 0.1 dihydro-4-methyl-4-(1-methylethyl)-5- oxo-1H-imidazol-2-yl]-3- (d) Indirect or inadvertent residues. pyridinecarboxylic acid, applied as its [Reserved] acid or ammonium salt, in or on the following commodities: [67 FR 55331, Aug. 29, 2002, as amended at 68 FR 13849, Mar. 21, 2003; 71 FR 6359, Feb. 8, Parts per 2006; 76 FR 34885, June 15, 2011; 80 FR 72599, Commodity million Nov. 20, 2015] Alfalfa, seed ...... 0.15 § 180.448 Hexythiazox; tolerance for Alfalfa, seed screenings ...... 0.15 residues. Animal feed, nongrass, group 18, forage ...... 3.0 Animal feed, nongrass, group 18, hay ...... 5.5 (a) General. Tolerances are estab- Peanut ...... 0.1 lished for residues of hexythiazox, in- Rice, bran ...... 1.2 Rice, grain ...... 0.3 cluding its metabolites and degradates, in or on the commodities in the table (3) A tolerance is established for the below. Compliance with the tolerance sum of residues of the herbicide levels specified below is to be deter- imazethapyr, 2-[4,5-dihydro-4-methyl-4- mined by measuring only hexythiazox (1-methylethyl)-5-oxo- 1H-imidazol-2- and its metabolites containing the (4- yl]-5-ethyl-3-pyridine carboxylic acid, chlorophenyl)-4-methyl-2-oxo-3- and its metabolite CL 288511, 2-[4,5- thiazolidine moiety, calculated as the dihydro-4-methyl-4-(1-methylethyl)-5- stoichiometric equivalent of oxo-1H-imidazol-2-yl]-5-(1-hydroxy- hexythiazox. ethyl)-3-pyridine carboxylic acid, ap- Parts per plied as its acid or ammonium salt, in Commodity million or on the following commodities: Almond, hulls ...... 10 Parts per Apple, wet pomace ...... 0.40 Commodity million Beet, sugar, dried pulp ...... 0.30 Beet, sugar, root ...... 0.15 Cattle, meat byproducts ...... 0.10 Berry, low growing, subgroup 13–07G ...... 6 Corn, field, forage ...... 0.1 Caneberry subgroup 13–07A ...... 1 Corn, field, grain ...... 0.1 Cattle, fat ...... 0.05 Corn, field, stover ...... 0.1 Cattle, meat byproducts ...... 0.5 Crayfish ...... 0.15 Citrus, oil ...... 25 Goat, meat byproducts ...... 0.10 Corn, field, forage ...... 3.0 Hog, meat byproducts ...... 0.10 Corn, field, grain ...... 0.02 Horse, meat byproducts ...... 0.10 Corn, field, stover ...... 7.0 Sheep, meat byproducts ...... 0.10 Cotton, gin byproducts ...... 15 Cotton, undelinted seed ...... 0.4 Date, dried fruit ...... 1.0 (b) Section 18 emergency exemptions. Egg ...... 0.05 [Reserved] Fruit, pome, group 11–10 ...... 0.4 (c) Tolerances with regional registra- Fruit, small, vine climbing, subgroup 13–07F, except fuzzy kiwifruit ...... 1 tions. Tolerances with regional reg- Fruit, stone, group 12 ...... 1.0 istration, as defined in § 180.1(l) of this Goat, fat ...... 0.05

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Parts per EDITORIAL NOTE: For FEDERAL REGISTER ci- Commodity million tations affecting § 180.448, see the List of CFR Sections Affected, which appears in the Goat, meat byproducts ...... 0.5 Finding Aids section of the printed volume Grain, aspirated fractions ...... 5 Hog, fat ...... 0.02 and at www.govinfo.gov. Hog, meat byproducts ...... 0.05 Hop, dried cones ...... 20 § 180.449 Avermectin B1 and its delta- Horse, fat ...... 0.05 8,9-isomer; tolerances for residues. Horse, meat byproducts ...... 0.5 Milk ...... 0.05 (a) General. Tolerances are estab- Nut, tree, group 14 ...... 0.30 lished for residues of abamectin, in- Pepper/eggplant subgroup 8–10B ...... 1.5 cluding its metabolites and degradates, Peppermint, tops ...... 2.0 Pistachio ...... 0.30 in or on the commodities in the fol- Plum, prune, dried ...... 1.3 lowing table. Compliance with the tol- Poultry, fat ...... 0.05 erance levels specified in the following Poultry, meat byproducts ...... 0.05 Sheep, fat ...... 0.05 table is to be determined by measuring Sheep, meat byproducts ...... 0.5 only avermectin B1 a mixture of Spearmint, tops ...... 2.0 avermectins containing greater than or Tomato ...... 0.50 equal to 80% avermectin B1 a (5-O- demethyl avermectin A1) and less than (b) Section 18 emergency exemptions. or equal to 20% avermectin B1b (5- - [Reserved] O (c) Tolerances with regional registra- demethyl-25-de(1-methylpropyl)-25-(1- tions. Tolerances with regional reg- methylethyl) avermectin A1) and its istrations as defined by § 180.1(l), are es- delta-8,9-isomer in or on the following tablished for residues of hexythiazox, commodities: including its metabolites and OMMODITY degradates, in or on the commodities in the table below. Compliance with Commodity Parts per the tolerance levels specified below is million to be determined by measuring only Acerola ...... 0.015 hexythiazox and its metabolites con- Almond, hulls ...... 0.10 Apple, wet pomace ...... 0.10 taining the (4-chlorophenyl)-4-methyl- Arugula ...... 0.1 2-oxo-3-thiazolidine moiety, calculated Avocado ...... 0.020 as the stoichiometric equivalent of Banana 1 ...... 0.006 hexythiazox. Bean ...... 0.015 Berry, low growing, subgroup 13–07G ...... 0.05 Black sapote ...... 0.40 Parts per Commodity million Caneberry subgroup 13–07A ...... 0.20 Canistel ...... 0.40 Alfalfa, forage (EPA Regions 7–11 only) ...... 20 Carrot, roots ...... 0.03 Alfalfa, hay (EPA Regions 7–11 only) ...... 60 Cattle, fat ...... 0.05 Bean, dried, seed (EPA Regions 7–12 only) ...... 0.4 Cattle, meat ...... 0.02 Bean, succulent (EPA Regions 7–12 only) ...... 0.3 Cattle, meat byproducts ...... 0.09 Bermuda grass, forage (EPA Regions 9–10 only) 40 Celeriac, roots ...... 0.05 Bermuda grass, hay (EPA Regions 9–10 only) .... 70 Celeriac, tops ...... 0.05 Corn, field, forage ...... 6.0 Celtuce ...... 0.1 Corn, field, grain ...... 0.02 Chive, dried leaves ...... 0.02 Corn, field, stover ...... 2.5 Chive, fresh leaves ...... 0.01 Corn, sweet, forage (EPA Regions 7–12 only) ..... 4.0 Citrus, dried pulp ...... 0.10 Corn, sweet, kernel plus cob with husks removed Citrus, oil ...... 0.10 (EPA Regions 7–12 only) ...... 0.1 Corn, sweet, forage ...... 0.20 Fruit, citrus group 10–10 (CA, AZ, TX only) ...... 0.6 Corn, sweet, kernel plus cob with husk removed 0.01 Potato ...... 0.02 Corn, sweet, stover ...... 0.50 Sorghum, grain, forage (EPA Regions 6–8 only) 5 Cotton, gin byproducts ...... 1.0 Sorghum, grain, grain (EPA Regions 6–8 only) .... 3 Cotton, undelinted seed ...... 0.02 Sorghum, grain, stover (EPA Regions 6–8 only) .. 6 Feijoa ...... 0.015 Timothy, forage (EPA Regions 9–11 only) ...... 40 Fennel, Florence, fresh leaves and stalk ...... 0.1 Timothy, hay (EPA Regions 9–11 only) ...... 40 Food products in food handling establishments Wheat, forage (EPA Regions 9–12 only) ...... 6.0 (other than those already covered by higher Wheat, grain (EPA Regions 9–12 only) ...... 0.02 tolerances as a result of use on growing crops, Wheat, hay (EPA Regions 9–12 only) ...... 30 and other than those already covered by toler- Wheat, straw (EPA Regions 9–12 only) ...... 8.0 ances on milk, meat, and meat byproducts) ..... 0.01 Fruit, citrus, group 10–10 ...... 0.02 Fruit, pome, group 11–10 ...... 0.02 (d) Indirect or inadvertent residues. Fruit, small vine climbing, except fuzzy kiwifruit, [Reserved] subgroup 13–07F ...... 0.02 Fruit, stone, group 12–12 ...... 0.09 [54 FR 17948, Apr. 26, 1989] Garden cress ...... 0.1

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OMMODITY—Continued Finding Aids section of the printed volume and at www.govinfo.gov. Commodity Parts per million § 180.450 Beta-(4-Chlorophenoxy)- Goat, fat ...... 0.03 alpha-(1,1-dimethylethyl)-1H-1,2,4- Goat, meat ...... 0.02 triazole-1-ethanol; tolerances for Goat, meat byproducts ...... 0.04 residues. Grain, aspirated grain fractions ...... 0.40 Guava ...... 0.015 (a) General. Tolerances are estab- Herb subgroup 19A, except chive ...... 0.030 lished for the combined residues of the Hog, fat ...... 0.01 fungicide b-(4-chlorophenoxy)-a-(1,1- Hog, meat ...... 0.02 dimethylethyl)-1H-1,2,4-triazole-1-eth- Hog, meat byproducts ...... 0.02 Hop, dried cones ...... 0.20 anol (triadimenol) and its butanediol Horse, fat ...... 0.03 metabolite, 4-(4-chlorophenoxy)-2,2-di- Horse, meat ...... 0.02 methyl-4-(1H-1,2,4-triazol-l-yl)-1,3- Horse, meat byproducts ...... 0.04 Jaboticaba ...... 0.015 butanediol, calculated as triadimenol, Leaf petiole vegetable subgroup 22B ...... 0.1 in or on the following commodities: Leafy greens subgroup 4–16A ...... 0.1 Longan ...... 0.01 Parts per Expiration/ Mamey sapote ...... 0.40 Commodity million Revocation Milk ...... 0.015 Date Nut, tree, group 14–12 ...... 0.01 1 Onion, bulb, subgroup 3–07A ...... 0.01 Banana ...... 0.2 None Onion, green, subgroup 3–07B ...... 0.08 Barley, grain ...... 0.05 None Barley, straw ...... 0.2 None Papaya ...... 0.40 Corn, field, forage ...... 0.05 None Passionfruit ...... 0.015 Corn, field, grain ...... 0.05 None Peppermint, tops ...... 0.010 Corn, field, stover ...... 0.05 None Pineapple ...... 0.015 Corn, pop, grain ...... 0.05 None Plum, prune, dried ...... 0.025 Corn, pop, stover ...... 0.05 None Poultry, meat ...... 0.02 Corn, sweet, forage ...... 0.05 None Poultry, meat byproducts ...... 0.02 Corn, sweet, kernel plus cob with Pulasan ...... 0.01 husks removed ...... 0.05 None Rambutan ...... 0.01 Corn, sweet, stover ...... 0.05 None Sapodilla ...... 0.40 Cotton, undelinted seed ...... 0.02 None Sheep, fat ...... 0.03 Oat, forage ...... 2.5 None Sheep, meat ...... 0.02 Oat, grain ...... 0.05 None Sheep, meat byproducts ...... 0.04 Oat, straw ...... 0.2 None Soybean, forage ...... 0.30 Rye, forage ...... 2.5 None Soybean, hay ...... 1.0 Rye, grain ...... 0.05 None Soybean, seed ...... 0.01 Rye, straw ...... 0.1 None Spanish lime ...... 0.01 Wheat, forage ...... 2.5 None Spearmint, tops ...... 0.010 Wheat, grain ...... 0.05 None Star apple ...... 0.40 Wheat, straw ...... 0.2 None Starfruit ...... 0.015 Tea, dried 1 ...... 1.0 1 There are no U.S. registrations for banana (whole) as of Tropical and subtropical, small fruit, inedible peel, September 22, 1993. subgroup 24A ...... 0.01 Upland cress ...... 0.1 (b) Section 18 emergency exemptions. Vegetable, cucurbit, group 9 ...... 0.005 [Reserved] Vegetable, fruiting, group 8–10 ...... 0.07 (c) Tolerances with regional registra- Vegetable, legume, dried shelled, except soy- tions. [Reserved] bean, subgroup 6C ...... 0.01 Vegetable, legume, edible podded, subgroup 6A 0.08 (d) Indirect or inadvertent residues. Vegetable, legume, succulent shelled, subgroup [Reserved] 6B ...... 0.08 Vegetable, tuberous and corm, subgroup 01C ..... 0.01 [73 FR 54962, Sept. 24, 2008, as amended at 74 Wax jambu ...... 0.015 FR 47457, Sept. 16, 2009; 76 FR 34885, June 15, 2011] 1 There are no U.S. registrations for use of abamectin on banana or tea. § 180.451 Tribenuron methyl; toler- (b) Section 18 emergency exemptions. ances for residues. [Reserved] (a) General. Tolerances are estab- (c) Tolerances with regional registra- lished for residues of the herbicide tions. [Reserved] tribenuron methyl and its metabolites (d) Indirect or inadvertent residues. and degradates in or on the commod- [Reserved] ities in the following table. Compliance [62 FR 44095, Aug. 19, 1997] with the tolerance levels specified EDITORIAL NOTE: For FEDERAL REGISTER ci- below is to be determined by measuring tations affecting § 180.449, see the List of CFR only tribenuron methyl, methyl-2- Sections Affected, which appears in the [[[[N-(4-methoxy-6-methyl-1,3,5-triazin-

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2-yl) methylamino] carbonyl] amino] pyrimidin-2-yl]-1-(2- sulfonyl] benzoate, in or on the fol- methoxycarbonylphenylsulfonyl) urea) lowing commodities: in or on the following raw agricultural commodities. Parts per Commodity million Parts per Commodity million Barley, grain ...... 0.05 Barley, hay ...... 0.4 Cattle, fat ...... 0.10 Barley, straw ...... 0.10 Cattle, meat ...... 0.10 Canola, seed ...... 0.02 Cattle, meat byproducts ...... 0.10 Corn, field, forage ...... 0.15 Corn, field, forage ...... 0.10 Corn, field, grain ...... 0.01 Corn, field, grain ...... 0.02 Corn, field, stover ...... 1.1 Corn, field, stover ...... 0.10 Cotton, gin byproducts ...... 0.02 Corn, pop, grain ...... 0.02 Cotton, undelinted seed ...... 0.02 Corn, pop, stover ...... 0.10 Flax, seed ...... 0.02 Egg ...... 0.10 Grain, aspirated fractions ...... 1.5 Goat, fat ...... 0.10 Oat, forage ...... 0.05 Goat, meat ...... 0.10 Oat, grain ...... 0.05 Goat, meat byproducts ...... 0.10 Oat, hay ...... 0.05 Hog, fat ...... 0.10 Oat, straw ...... 0.10 Hog, meat ...... 0.10 Rice, grain ...... 0.05 Sorghum, grain, forage ...... 0.05 Hog, meat byproducts ...... 0.10 Sorghum, grain, grain ...... 0.05 Horse, fat ...... 0.10 Sorghum, grain, stover ...... 0.05 Horse, meat ...... 0.10 Soybean, forage ...... 0.07 Horse, meat byproducts ...... 0.10 Soybean, hay ...... 0.35 Milk ...... 0.02 Soybean, hulls ...... 0.04 Poultry, fat ...... 0.10 Soybean, seed ...... 0.01 Poultry, meat ...... 0.10 Sunflower, seed ...... 0.05 Poultry, meat byproducts ...... 0.10 Wheat, forage ...... 0.3 Sheep, fat ...... 0.10 Wheat, grain ...... 0.05 Sheep, meat ...... 0.10 Wheat, hay ...... 0.5 Sheep, meat byproducts ...... 0.10 Wheat, straw ...... 0.10 (b) Section 18 emergency exemptions. (b) Section 18 emergency exemptions. [Reserved] [Reserved] (c) Tolerances with regional registra- (c) Tolerances with regional registrations. [Reserved] tions. Tolerances with regional reg- (d) Indirect or inadvertent residues. istration, as defined in § 180.1(l) are es- [Reserved] tablished for residues of the herbicide [55 FR 21548, May 25, 1990, as amended at 62 tribenuron methyl (methyl-2-[[[[N-(4- FR 66020, Dec. 17, 1997; 63 FR 66458, Dec. 2, methoxy-6-methyl-1,3,5-triazin-2-yl) 1998; 67 FR 35049, May 17, 2002; 74 FR 46375, methylamino] car- Sept. 9, 2009; 74 FR 46699, Sept. 11, 2009; 77 FR bonyl]amino]sulfonyl] benzoate) in or 59128, Sept. 26, 2012] on the following raw agricultural commodities: § 180.454 Nicosulfuron; tolerances for residues. Parts per Commodity million (a) General. Tolerances are established for residues of the herbicide Grass, forage, fodder and hay, group 17, except nicosulfuron, including its metabolites bermudagrass; forage ...... 0.10 Grass, forage, fodder and hay, group 17, except and degradates, in or on the commod- bermudagrass; hay ...... 0.10 ities in the following table. Compliance with the tolerance levels specified in (d) Indirect or inadvertent residues. the following table is to be determined [Reserved] by measuring only nicosulfuron, 2- [69 FR 56718, Sept. 22, 2004, as amended at 72 [[[[(4,6-dimethoxy-2- FR 11789, Mar. 14, 2007; 73 FR 47065, Aug. 13, pyrimidinyl)amino]car- 2008; 74 FR 67128, Dec. 18, 2009; 76 FR 34885, bonyl]amino]sulfonyl]-N,N-dimethyl-3- June 15, 2011; 80 FR 72599, Nov. 20, 2015] pyridinecarboxamide.

§ 180.452 Primisulfuron-methyl; toler- Commodity Parts per ances for residues. million (a) General. Tolerances are estab- Cattle, fat ...... 0.01 Cattle, meat ...... 0.01 lished for residues of primisulfuron- Cattle, meat byproducts ...... 0.05 methyl (3-[4,6-bis-(difluoromethoxy)- Corn, field, forage ...... 0.1

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(b) Section 18 emergency exemptions. Commodity Parts per million [Reserved] Corn, field, grain ...... 0.1 (c) Tolerances with regional registra- Corn, field, stover ...... 0.1 tions. [Reserved] Corn, pop, grain ...... 0.1 (d) Indirect or inadvertent residues. Corn, pop, stover ...... 0.1 [Reserved] Corn, sweet, forage ...... 0.1 Corn, sweet, kernel plus cob with husks removed 0.1 [74 FR 47457, Sept. 16, 2009] Corn, sweet, stover ...... 0.1 Goat, fat ...... 0.01 § 180.458 Clethodim; tolerances for res- Goat, meat ...... 0.01 idues. Goat, meat byproducts ...... 0.05 Grass, forage ...... 9.0 (a) General. Tolerances are estab- Grass, hay ...... 25.0 lished for residues of the herbicide Horse, fat ...... 0.01 clethodim, including its metabolites Horse, meat ...... 0.01 Horse, meat byproducts ...... 0.05 and degradates, in or on the commod- Milk ...... 0.01 ities in the table in this paragraph. Sheep, fat ...... 0.01 Compliance with the tolerance levels Sheep, meat ...... 0.01 specified in this paragraph is to be de- Sheep, meat byproducts ...... 0.05 Sorghum, grain, forage ...... 0.3 termined by measuring only the sum of Sorghum, grain, grain ...... 0.8 clethodim, 2-[(1E)-1-[[[(2E)-3-chloro-2- Sorghum, grain, stover ...... 0.05 propenyl]oxy]imino]propyl]-5-[2- (ethylthio)propyl]-3-hydroxy-2-cyclo- (b) Section 18 emergency exemptions. hexen-1-one, and its metabolites con- [Reserved] taining the 5-(2- (c) Tolerances with regional registra- ethylthiopropyl)cyclohexene-3-one and tions. [Reserved] 5-(2-ethylthiopropyl)-5- (d) Indirect or inadvertent residues. hydroxycyclohexene-3-one moieties [Reserved] and their sulphoxides and sulphones, [75 FR 17578, Apr. 7, 2010, as amended at 80 calculated as the stoichiometric equiv- FR 68265, Nov. 4, 2015] alent of clethodim, in or on the commodity. § 180.455 Procymidone; tolerances for Parts per residues. Commodity million A tolerance is established for the res- Alfalfa, forage ...... 6.0 idues of the fungicide procymidone, N- Alfalfa, hay ...... 10 (3,5-dichlorophenyl)-1,2- Almond, hulls ...... 0.20 dimethylcyclopropane-1,2 Artichoke, globe ...... 1.2 Berry, low growing, subgroup 13–07G, except dicarboximide, in or on the following cranberry ...... 3.0 raw agricultural commodity: Beet, sugar, molasses ...... 1.0 Beet, sugar, roots ...... 0.20 Beet, sugar, tops ...... 1.0 Commodity Parts per million Brassica, leafy, greens, subgroup 4–16B ...... 3.0 Bushberry subgroup 13–07B ...... 0.20 Grape, wine ...... 5.0 Caneberry subgroup 13–07A ...... 0.30 Canola, meal ...... 1.0 Cattle, fat ...... 0.2 [59 FR 42514, Aug. 18, 1994] Cattle, meat ...... 0.2 Cattle, meat byproducts ...... 0.2 § 180.457 Bitertanol; tolerances for res- Clover, forage ...... 10.0 idues. Clover, hay ...... 20.0 Corn, field, forage ...... 0.2 (a) General. A tolerance is established Corn, field, grain ...... 0.2 for the residues of the fungicide Corn, field, stover ...... 0.2 bitertanol, -([1,1′-biphenyl]-4-yloxy)- - Cotton, meal ...... 2.0 b a Cottonseed subgroup 20C ...... 1.0 (1,1-dimethylethyl)-1H-1,2,4-triazole-1- Cranberry ...... 0.50 ethanol, in or on the following raw ag- Egg ...... 0.2 ricultural commodity: Flax, meal ...... 1.0 Flax, seed ...... 0.6 Fruit, pome, group 11–10 ...... 0.20 Parts per Commodity million Fruit, stone, group 12–12 ...... 0.20 Goat, fat ...... 0.2 Banana 1 ...... 0.5 Goat, meat ...... 0.2 Goat, meat byproducts ...... 0.2 1 There are no U.S. registrations as of April 1, 1992. Herb subgroup 19A ...... 12.0

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Parts per Parts per Commodity million Commodity million

Hog, fat ...... 0.2 Barley, straw ...... 2.0 Hog, meat ...... 0.2 Cattle, fat ...... 0.1 Hog, meat byproducts ...... 0.2 Cattle, kidney ...... 0.5 Hop, dried cones ...... 0.5 Cattle, meat byproducts, except kidney ...... 0.1 Horse, fat ...... 0.2 Horse, meat ...... 0.2 Cattle, meat ...... 0.1 Horse, meat byproducts ...... 0.2 Goat, fat ...... 0.1 Kohlrabi 1 ...... 3.0 Goat, kidney ...... 0.5 Leaf petiole vegetable subgroup 22B ...... 0.60 Goat, meat byproducts, except kidney ...... 0.1 Leafy greens subgroup 4–16A ...... 2.0 Goat, meat ...... 0.1 Melon subgroup 9A ...... 2.0 Grass, forage ...... 7.0 Milk ...... 0.05 Grass, hay ...... 2.0 Nut, tree, group 14–12 ...... 0.20 Okra ...... 1.5 Hog, fat ...... 0.1 Onion, bulb, subgroup 3–07A ...... 0.50 Hog, kidney ...... 0.5 Onion, green, subgroup 3–07B ...... 2.0 Hog, meat byproducts ...... 0.1 Peanut ...... 3.0 Hog, meat ...... 0.1 Peanut, hay ...... 3.0 Horse, fat ...... 0.1 Peanut, meal ...... 5.0 Horse, kidney ...... 0.5 Peppermint, tops ...... 5.0 Horse, meat byproducts, except kidney ...... 0.1 Potato, granules/flakes ...... 2.0 Poultry, fat ...... 0.2 Horse, meat ...... 0.1 Poultry, meat ...... 0.2 Milk ...... 0.02 Poultry, meat byproducts ...... 0.2 Sheep, fat ...... 0.1 Radish, tops ...... 0.70 Sheep, kidney ...... 0.5 Rapeseed subgroup 20A, except flax seed ...... 0.50 Sheep, meat byproducts, except kidney ...... 0.1 Safflower, meal ...... 10.0 Sheep, meat ...... 0.1 Sheep, fat ...... 0.2 Wheat, forage ...... 5.0 Sheep, meat ...... 0.2 Wheat, grain ...... 0.02 Sheep, meat byproducts ...... 0.2 Soybean ...... 10.0 Wheat, straw ...... 2.0 Spearmint, tops ...... 5.0 Squash/cucumber subgroup 9B ...... 0.50 (b) Section 18 emergency exemptions. Stalk and stem vegetable subgroup 22A ...... 1.7 [Reserved] Stevia, dried leaves ...... 12 Sunflower, meal ...... 10.0 (c) Tolerances with regional registra- Sunflower subgroup 20B ...... 5.0 tions. [Reserved] Vegetable, brassica, head and stem, group 5–16 3.0 Vegetable, fruiting, group 8–10, except okra ...... 1.0 (d) Indirect or inadvertent residues. Vegetable, legume, group 6, except soybean ...... 3.5 [Reserved] Vegetable, root, except sugar beet, subgroup 1B 1.0 Vegetable, tuberous and corm, subgroup 1C ...... 1.0 [60 FR 36731, July 18, 1995, as amended at 63 FR 44152, Aug. 18, 1998; 63 FR 66449, Dec. 2, 1 This tolerance expires on October 12, 2018. 1998] (b) Section 18 emergency exemptions. [Reserved] § 180.460 Benoxacor; tolerances for (c) Tolerances with regional registra- residues. tions. [Reserved] (a) General. Tolerances are estab- (d) Indirect or inadvertent residues. lished for residues of the inert ingre- [Reserved] dient (safener) benoxacor (4- [76 FR 23496, Apr. 27, 2011, as amended at 77 (dichloroacetyl)-3,4-dihydro-3-methyl- FR 59128, Sept. 26, 2012; 81 FR 27342, May 6, 2H-1, 4-benzoxazine) at 0.01 parts per 2016; 83 FR 15753, Apr. 12, 2018] million (ppm) when used in pesticide formulations containing metolachlor § 180.459 Triasulfuron; tolerances for or S-metolachlor in or on raw agricul- residues. tural commodities for which tolerances (a) General. Tolerances are estab- have been established for metolachlor lished for residues of the herbicide or S-metolachlor. triasulfuron [3-(6-methoxy-4-methyl- (b) Section 18 energency exemptions. 1,3,5-triazin-2-yl)-1-(2-(2- [Reserved] chloroethoxy)phenylsulfonyl)urea] in (c) Tolerances with regional registra- or on the following raw agricultural tions. [Reserved] commodities: (d) Indirect or inadvertent residues. Parts per [Reserved] Commodity million [63 FR 7305, Feb. 13, 1998, as amended at 70 Barley, grain ...... 0.02 FR 21631, Apr. 27, 2005]

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§ 180.461 Cadusafos; tolerances for res- § 180.463 Quinclorac; tolerances for idues. residues. A tolerance is established for the res- (a)(1) General. Tolerances are estab- idues of the nematicide/insecticide lished for residues of the herbicide cadusafos, O-ethyl S,S-di-sec-butyl quinclorac, including its metabolites phosphorodithioate, in or on the fol- and degradates, in or on the commod- lowing raw agricultural commodity: ities in the table in this paragraph. Compliance with the tolerance levels Parts per Commodity million specified in this paragraph is to be determined by measuring only Banana ...... 0.01 quinclorac, 3,7-dichloro-8- quinolinecarboxylic acid, in or on the There are no U.S. registrations as of commodity. May 10, 1994, for the nematicide/ insecticid cadusafos. Parts per Commodity million [59 FR 39467, Aug. 3, 1994] Asparagus ...... 0.08 § 180.462 Pyridate; tolerances for resi- Bushberry, subgroup 13–07B ...... 0.08 Caneberry subgroup 13–07A ...... 0.08 dues. Barley, grain ...... 2.0 (a) General. Tolerances are estab- Berry, low growing, except strawberry, subgroup lished for residues of the herbicide 13–07H ...... 1.5 Cattle, fat ...... 0.7 pyridate, including its metabolites and Cattle, meat byproducts ...... 1.5 degradates, in or on the commodities Cattle, meat ...... 0.05 in the table in this paragraph. Compli- Egg ...... 0.05 Goat, fat ...... 0.7 ance with the tolerance levels specified Goat, meat byproducts ...... 1.5 in this paragraph is to be determined Goat, meat ...... 0.05 by measuring only the sum of pyridate, Grain, aspirated fractions ...... 1200 Grass, forage ...... 150 O-(6-chloro-3-phenyl-4-pyridazinyl)-S- Grass, hay ...... 130 octyl-carbonothioate, and its metabo- Hog, fat ...... 0.7 lites, 6-chloro-3-phenyl-pyridazine-4-ol Hog, meat byproducts ...... 1.5 and conjugates of 6-chloro-3-phenyl-py- Hog, meat ...... 0.05 Horse, fat ...... 0.7 ridazine-4-ol, calculated as the stoi- Horse, meat byproducts ...... 1.5 chiometric equivalent of pyridate, in Horse, meat ...... 0.05 or on the commodity. Milk ...... 0.05 Poultry, fat ...... 0.05 Poultry, meat byproducts ...... 0.1 Parts per Commodity million Poultry, meat ...... 0.05 Rhubarb ...... 0.5 Brassica, head and stem, subgroup 5A ...... 0.03 Rice, bran ...... 15.0 Cabbage ...... 0.03 Rice, grain ...... 5.0 Chickpea, seed ...... 0.1 Sheep, fat ...... 0.7 Collards ...... 0.03 Sheep, meat byproducts ...... 1.5 Corn, field, forage ...... 0.03 Sheep, meat ...... 0.05 Corn, field, grain ...... 0.03 Sorghum, grain, forage ...... 3.0 Corn, field, stover ...... 0.03 Sorghum, grain, grain ...... 6.0 Corn, pop, grain ...... 0.03 Sorghum, grain, stover ...... 1.0 Corn, pop, stover ...... 0.03 Wheat, forage ...... 1.0 Peanut ...... 0.03 Wheat, germ ...... 0.75 Peppermint, tops ...... 0.20 Wheat, grain ...... 0.5 Spearmint, tops ...... 0.20 Wheat, hay ...... 0.5 Wheat, straw ...... 0.1 (b) Section 18 emergency exemptions. [Reserved] (2) Tolerances are established for res- (c) Tolerances with regional registra- idues of the herbicide quinclorac, in- tions. [Reserved] cluding its metabolites and degradates, (d) Indirect or inadvertent residues. in or on the commodity in the fol- [Reserved] lowing table. Compliance with the tolerance levels specified in this para- [57 FR 54303, Nov. 18, 1992, as amended at 62 graph is to be determined by measuring FR 44558, Aug. 22, 1997; 63 FR 53844, Oct. 7, 1998; 64 FR 46298, Aug. 25, 1999; 65 FR 25652, only quinclorac, 3,7-dichloro-8- May 3, 2000; 67 FR 35049, May 17, 2002; 72 FR quinolinecarboxylic acid, and its meth- 35665, June 29, 2007; 74 FR 46376, Sept. 9, 2009; yl ester, methyl-3,7-dichloro-8- 76 FR 23496, Apr. 27, 2011] quinolinecarboxylate, calculated as the

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stoichiometric equivalent of Commodity Parts per quinclorac, in or on the commodity. million Corn, field, stover ...... 0.01 Parts per Commodity million Corn, pop, forage ...... 0.01 Corn, pop, grain ...... 0.01 Rapeseed, subgroup 20A 1 ...... 1.5 Corn, pop, stover ...... 0.01 1 There are no U.S. Registrations. Corn, sweet, forage ...... 0.01 Corn, sweet, kernel plus cob with husks removed 0.01 (b) Section 18 emergency exemptions. Corn, sweet, stover ...... 0.01 Time-limited tolerances are estab- Cotton, gin byproducts ...... 1.5 lished for residues of the herbicide Cottonseed subgroup 20C ...... 0.01 quinclorac, including its metabolites Garlic ...... 0.01 and degradates, in or on the com- Grass, forage ...... 0.15 Grass, hay ...... 2.5 modity in the table in this paragraph. Grass, seed screenings ...... 0.01 Compliance with the tolerance level Grass, straw ...... 0.01 specified in this paragraph is to be de- Hop, dried cones ...... 0.05 termined by measuring only Horseradish ...... 0.01 quinclorac, 3,7-dichloro-8- Leek ...... 0.01 quinolinecarboxylic acid, in or on the Onion, bulb ...... 0.01 Onion, green ...... 0.01 commodity. The tolerance expires and Onion, Welsh ...... 0.01 is revoked on the date specified in the Peanut ...... 0.01 table in this paragraph. Peanut, hay ...... 0.01 Radish, roots ...... 0.01 Expiration/ Radish, tops ...... 0.01 Commodity Parts per revocation million date Rutabaga, roots ...... 0.01 Rutabaga, tops ...... 0.1 Cranberry ...... 15.0 12/31/12 Shallot, bulb ...... 0.01 Shallot, fresh leaves ...... 0.01 (c) Tolerances with regional registra- Sorghum, grain, forage ...... 0.01 tions. [Reserved] Sorghum, grain, grain ...... 0.01 (d) Indirect or inadvertent residues. Sorghum, grain, stover ...... 0.01 Soybean, seed ...... 0.01 [Reserved] Turnip, greens ...... 0.1 [57 FR 47996, Oct. 21, 1992, as amended at 64 Turnip, roots ...... 0.01 FR 6548, 6549, Feb. 10, 1999; 64 FR 14632, Mar. Turnip, tops ...... 0.1 26, 1999; 65 FR 33701, May 24, 2000; 67 FR 35049, Vegetable, tuberous and corm, subgroup 1C ...... 0.01 May 17, 2002; 72 FR 55073, Sept. 28, 2007; 74 FR 51490, Oct. 7, 2009; 74 FR 67090, Dec. 18, 2009; (b) Section 18 emergency exemptions. 76 FR 23497, Apr. 27, 2011; 77 FR 75566, Dec. 21, [Reserved] 2012; 78 FR 71528, Nov. 29, 2013; 80 FR 72599, (c) Tolerances with regional registra- Nov. 20, 2015; 82 FR 57149, Dec. 4, 2017] tions. Tolerances with regional registration are established for residues of § 180.464 Dimethenamid; tolerances for dimethenamid, 1 (R,S)-2-chloro-N-[(1- residues. methyl-2-methoxy) ethyl]-N-(2,4- (a) General. Tolerances are estab- dimethylthien-3-yl)-acetamide) in or lished for residues of the herbicide on the following raw agricultural com- dimethenamid, 1(R,S)-2-chloro-N-[(1- modities: methyl-2-methoxy)ethyl]-N-(2,4- dimethylthien-3-yl)-acetamide, applied Commodity Parts per as either the 90:10 or 50:50 S:R isomers, million in or on the following food commod- Pumpkin ...... 0.01 ities: Squash, winter ...... 0.01

Parts per Commodity million (d) Indirect or inadvertent residues. [Reserved] Bean, dry, seed ...... 0.01 Beet, garden, roots ...... 0.01 [65 FR 51551, Aug. 24, 2000, as amended at 67 Beet, garden, tops ...... 0.01 FR 46884, July 17, 2002; 69 FR 29459, May 24, Beet, sugar, dried pulp ...... 0.01 2004; 69 FR 57207, Sept. 24, 2004; 70 FR 24712, Beet, sugar, molasses ...... 0.01 May 11, 2005; 71 FR 25942, May 3, 2006; 71 FR Beet, sugar, roots ...... 0.01 Beet, sugar, tops ...... 0.01 49354, Aug. 23, 2006; 72 FR 44388, Aug. 8, 2007; Corn, field, forage ...... 0.01 72 FR 73630, Dec. 28, 2007; 80 FR 9215, Feb. 20, Corn, field, grain ...... 0.01 2015]

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§ 180.465 4-(Dichloroacetyl)-1-oxa-4- Commodity Parts per azaspiro[4.5]decane. million (a) General. Tolerances are estab- Cotton, undelinted seed ...... 1.0 lished for the residues of 4- Custard apple ...... 1.5 Egg ...... 0.05 (dichloroacetyl)-1-oxa-4- Feijoa ...... 3.0 azaspiro[4.5]decane, (CAS No. 71526–07– Fruit, citrus, group 10–10 ...... 2.0 3) when used as an inert ingredient Fruit, pome, group 11–10 ...... 5.0 (safener) in or on the following raw ag- Fruit, small vine climbing, except fuzzy kiwifruit, subgroup 13–07F ...... 5.0 ricultural commodities: Fruit, stone, crop group 12, except cherry ...... 1.4 Goat, fat ...... 1.0 Parts per Commodity 1 Goat, meat byproducts ...... 0.1 million Goat, meat ...... 0.1 Grape, raisin ...... 10.0 Corn, field, forage ...... 0.005 Guava ...... 3.0 Corn, field, grain ...... 0.005 Corn, field, stover ...... 0.005 Hog, fat ...... 1.0 Corn, pop, grain ...... 0.005 Hog, meat byproducts ...... 0.1 Corn, pop, stover ...... 0.005 Hog, meat ...... 0.1 Horse, fat ...... 1.0 1There are no U.S. registered products containing 4- Horse, meat byproducts ...... 0.1 (dichloroacetyl)-1-oxa-4-azaspiro[4.5]decane as of June 17, Horse, meat ...... 0.1 2002. Ilama ...... 1.5 (b) Section 18 emergency exemptions. Jaboticaba ...... 3.0 Longan ...... 7.0 [Reserved] Lychee ...... 7.0 (c) Tolerances with regional registra- Mango ...... 1.0 tions. [Reserved] Melon subgroup 9A ...... 0.5 (d) Indirect or inadvertent residues. Milk, fat (reflecting 0.08 ppm in whole milk) ...... 2.0 Nut, tree, crop group 14 ...... 0.10 [Reserved] Olive ...... 5.0 [68 FR 4392, Jan. 29, 2003] Papaya ...... 1.0 Passionfruit ...... 3.0 Pea, succulent ...... 0.02 § 180.466 Fenpropathrin; tolerances for Peanut, hay ...... 20.0 residues. Peanut ...... 0.01 (a) General. Tolerances are estab- Pistachio ...... 0.10 Poultry, fat ...... 0.05 lished for residues of fenpropathrin, in- Poultry, meat byproducts ...... 0.05 cluding its metabolites and degradates, Poultry, meat ...... 0.05 in or on the commodities in the fol- Pulasan ...... 7.0 lowing table. Compliance with the tol- Rambutan ...... 7.0 Sapodilla ...... 1.0 erance levels specified below is to be Sapote, black ...... 1.0 determined by measuring only Sapote, mamey ...... 1.0 fenpropathrin (alpha-cyano-3-phenoxy- Sheep, fat ...... 1.0 Sheep, meat byproducts ...... 0.1 benzyl 2,2,3,3 Sheep, meat ...... 0.1 tetramethylcyclopropanecarboxylate). Soursop ...... 1.5 Spanish lime ...... 7.0 Commodity Parts per Squash/Cucumber subgroup 9B ...... 0.5 million Star apple ...... 1.0 Starfruit ...... 3.0 Acerola ...... 3.0 Sugar apple ...... 1.5 Almond, hulls ...... 4.5 Tea, dried 1 ...... 2.0 Atemoya ...... 1.5 Vegetable, fruiting, group 8–10 ...... 1.0 Avocado ...... 1.0 Wax jambu ...... 3.0 Barley, grain ...... 0.04 Barley, hay ...... 3.0 1 There are no U.S. registrations as of November 28, 2012, Barley, straw ...... 2.0 for the use of fenpropathrin on tea, dried. Berry, low growing, subgroup 13–07G ...... 2.0 Biriba ...... 1.5 (b) Section 18 emergency exemptions. Brassica, head and stem, subgroup 5A ...... 3.0 Time-limited tolerances specified in Bushberry subgroup 13–07B ...... 3.0 Caneberry subgroup 13-07A ...... 12 Table 2 to this paragraph (b) are estab- Canistel ...... 1.0 lished for residues of fenpropathrin, Cattle, fat ...... 1.0 (alpha-cyano-3-phenoxy-benzyl 2,2,3,3 Cattle, meat byproducts ...... 0.1 tetramethylcyclopropane carboxylate) Cattle, meat ...... 0.1 Cherimoya ...... 1.5 in or on the specified agricultural com- Cherry, sweet ...... 5.0 modities, resulting from use of the pes- Cherry, tart ...... 5.0 ticide pursuant to FIFRA section 18 Citrus, dried pulp ...... 4.0 Citrus, oil ...... 75 emergency exemptions. The tolerance Cotton, refined oil ...... 3.0 expires on the date specified in Table 2.

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TABLE 2 TO PARAGRAPH (b) Parts per Commodity million Parts per Expiration Commodity million date Corn, field, grain ...... 0 .05 Corn, field, stover ...... 0 .05 Kiwifruit, fuzzy ...... 5 12/31/2022 Soybean, seed ...... 0 .05

(c) Tolerances with regional registra- (b) Section 18 emergency exemptions. tions. [Reserved] [Reserved] (d) Indirect or inadvertent residues. (c) Tolerances with regional registra- [Reserved] tions. [Reserved] [62 FR 63034, Nov. 26, 1997, as amended at 63 (d) Indirect or inadvertent residues. FR 48116, Sept. 9, 1998; 64 FR 3009, Jan. 20, [Reserved] 1999; 65 FR 11242, Mar. 2, 2000; 65 FR 24397, Apr. 26, 2000; 65 FR 48620, Aug. 9, 2000; 66 FR [76 FR 23497, Apr. 27, 2011] 64774, Dec. 14, 2001; 67 FR 35049, May 17, 2002; 70 FR 38789, July 6, 2005; 70 FR 55747, Sept. 23, § 180.469 Dichlormid; tolerances for 2005; 74 FR 12606, Mar. 25, 2009; 77 FR 70908, residues. Nov. 28, 2012; 78 FR 69569, Nov. 20, 2013; 84 FR 70434, Dec. 23, 2019] (a) General. (1) Tolerances are established for residues of dichlormid, in- § 180.467 Carbon disulfide; tolerances cluding its metabolites and degradates, for residues. when used as an inert ingredient (her- Tolerances are established for the bicide safener) in pesticide formula- nematicide, insecticide, and fungicide tions, in or on the commodities in the carbon disulfide, from the application following table. Compliance with the of sodium tetrathiocarbonate, in or on tolerances is to be determined by meas- the following raw agricultural com- uring only dichlormid (2,2-dichloro- modities: N,N-di-2-propenylacetamide). Parts per Commodity million Parts per Commodity million Almond ...... 0.1 Corn, field, forage ...... 0.05 Almond, hulls ...... 0.1 Grape ...... 0.1 Corn, field, grain ...... 0.05 Grapefruit ...... 0.1 Corn, field, stover ...... 0.05 Lemon ...... 0.1 Corn, pop, grain ...... 0.05 Orange, sweet ...... 0.1 Corn, pop, stover ...... 0.05 Peach ...... 0.1 Corn, sweet, forage ...... 0.05 Plum, prune, fresh ...... 0.1 Corn, sweet, kernel plus cob with husks removed 0.05 Corn, sweet, stover ...... 0.05 [58 FR 33771, June 21, 1993, as amended at 62 FR 26949, May 16, 1997] (2) Tolerances are established for residues of dichlormid, including its me- § 180.468 Flumetsulam; tolerances for tabolites and degradates, at 0.05 parts residues. per million (ppm) when used as an inert (a) General. Tolerances are estab- ingredient (herbicide safener) in pes- lished for residues of the herbicide ticide formulations containing flumetsulam, including its metabolites metolachlor or S-metolachlor in or on and degradates, in or on the commod- raw agricultural commodities for ities in the table in this paragraph. which tolerances have been established Compliance with the tolerance levels for metolachlor or S-metolachlor. specified in this paragraph is to be de- Compliance with the tolerances is to be termined by measuring only determined by measuring only flumetsulam, N-(2,6-difluorophenyl)-5- dichlormid (2,2-dichloro-N,N-di-2- methyl-(1,2,4)-triazolo-(1,5a)-pyrimi- propenylacetamide). dine-2-sulfonamide, in or on the commodity. (b) Section 18 emergency exemptions. [Reserved] Commodity Parts per (c) Tolerances with regional registra- million tions. [Reserved] Bean, dry, seed ...... 0 .05 Corn, field, forage ...... 0 .05

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(d) Indirect or inadvertent residues. Commodity Parts per [Reserved] million [65 FR 16149, Mar. 27, 2000, as amended at 67 Sheep, kidney ...... 0.03 FR 51105, Aug. 7, 2002; 69 FR 58290, Sept. 30, Sheep, meat ...... 0.02 Sheep, meat byproducts, except kidney ...... 0.02 2004; 70 FR 76699, Dec. 28, 2005; 74 FR 37623, Sorghum, grain, forage ...... 1.6 July 29, 2009; 76 FR 16310, Mar. 23, 2011; 81 FR Sorghum, grain, grain ...... 0.05 69406, Oct. 6, 2016] Sorghum, grain, stover ...... 1.7 Soybean, meal ...... 1.2 § 180.470 Acetochlor; tolerances for Soybean, seed ...... 1.0 residues. (b) Section 18 emergency exemptions. (a) General. Tolerances are estab- [Reserved] lished for residues of acetochlor, in- (c) Tolerances with regional registra- cluding its metabolites and degradates, tions. [Reserved] in or on the commodities in the table (d) Indirect or inadvertent residues. below. Compliance with the tolerance Tolerances are established for indirect levels specified below is to be deter- or inadvertent residues of acetochlor, mined by measuring only acetochlor, 2- including its metabolites and chloro-2’-methyl-6-ethyl-N- degradates, in or on the raw agricul- ethoxymethylacetanilide, and its me- tural commodities in the table to this tabolites containing the ethyl methyl paragraph when present therein as a aniline (EMA) moiety and the hydroxy- result of application of acetochlor to ethyl methyl aniline (HEMA) moiety. the growing crops in the table to para- Both parent and the named metabo- graph (a) of this section. Compliance lites shall be determined as ethyl with the tolerance levels specified methyl aniline (EMA) and hydroxy- below is to be determined by measuring ethyl methyl aniline (HEMA), and cal- only acetochlor, 2-chloro-2’-methyl-6- culated as the stoichiometric equiva- ethyl-N-ethoxymethylacetanilide, and lents of acetochlor, in or on the fol- its metabolites containing the ethyl lowing commodities: methyl aniline (EMA) moiety and the Parts per hydroxyethyl methyl aniline (HEMA) Commodity million moiety. Both parent and the named Alfalfa, forage ...... 8.0 metabolites shall be determined as Alfalfa, hay ...... 20 ethyl methyl aniline (EMA) and hy- Beet, sugar, dried pulp ...... 0.50 droxyethyl methyl aniline (HEMA), Beet, sugar, molasses ...... 0.80 Beet, sugar, roots ...... 0.30 and calculated as the stoichiometric Beet, sugar, tops ...... 0.70 equivalents of acetochlor, in or on the Cattle, fat ...... 0.02 following commodities. Cattle, kidney ...... 0.03 Cattle, meat ...... 0.02 Parts per Cattle, meat byproducts, except kidney ...... 0.02 Commodity million Corn, field, forage ...... 4.5 Corn, field, grain ...... 0.05 Animal feed, nongrass, group 18, except alfalfa, Corn, field, stover ...... 2.5 forage ...... 1.3 Corn, pop, grain ...... 0.05 Animal feed, nongrass, group 18, except alfalfa, Corn, pop, stover ...... 2.5 hay ...... 3.5 Corn, sweet, forage ...... 1.5 Grain, cereal, forage, fodder and straw, group 16, Corn, sweet, kernels plus cob with husks re- except corn, grain sorghum, rice and wheat, moved ...... 0.05 forage ...... 0.5 Corn, sweet, stover ...... 1.0 Grain, cereal, forage, fodder and straw, group 16, Cotton, gin byproducts ...... 4.0 except corn, grain sorghum, rice and wheat, Cotton, undelinted seed ...... 0.6 hay ...... 2.0 Goat, fat ...... 0.02 Grain, cereal, forage, fodder and straw, group 16, Goat, kidney ...... 0.03 except corn, grain sorghum, rice and wheat, Goat, meat ...... 0.02 stover ...... 0.1 Goat, meat byproducts, except kidney ...... 0.02 Grain, cereal, forage, fodder and straw, group 16, Hog, kidney ...... 0.02 except corn, grain sorghum, and wheat, straw 0.3 Horse, fat ...... 0.02 Grain, cereal, group 15, except corn, grain sor- Horse, kidney ...... 0.03 ghum, and wheat, grain ...... 0.05 Horse, meat ...... 0.02 Pea and bean, dried shelled, except soybean, Horse, meat byproducts, except kidney ...... 0.02 subgroup 6C ...... 0.05 Milk ...... 0.02 Potato ...... 0.05 Peanut ...... 0.20 Soybean, forage ...... 0.7 Peanut, hay ...... 7.0 Soybean, hay ...... 1.0 Peanut, meal ...... 0.25 Sunflower, seed ...... 0.05 Sheep, fat ...... 0.02 Wheat, forage ...... 0.5

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imidazolidinimine) and its metabolites Commodity Parts per million containing the 6-chloropyridinyl moi- Wheat, grain ...... 0.02 ety, calculated as the stoichiometric Wheat, hay ...... 2.0 equivalent of imidacloprid, in or on the Wheat, straw ...... 0.1 following commodities:

[72 FR 27468, May 16, 2007, as amended at 74 Parts per Commodity million FR 29969, June 24, 2009; 74 FR 47450, Sept. 16, 2009; 78 FR 13268, Feb. 27, 2013; 79 FR 3517, Acerola ...... 1.0 Jan. 22, 2014; 83 FR 29028, June 22, 2018] Almond, hulls ...... 4.0 Apple ...... 0.5 § 180.471 Furilazole; tolerances for res- Apple, wet pomace ...... 3.0 Artichoke, globe ...... 2.5 idues. Aspirated grain fractions ...... 240 (a) General. Tolerances are estab- Atemoya ...... 0.30 Avocado ...... 1.0 lished for residues of furilazole, includ- Banana ...... 0.50 ing its metabolites and degradates, Beet, sugar, molasses ...... 0.30 when used as an inert ingredient Beet, sugar, roots ...... 0.05 (safener) in pesticide formulations ap- Beet, sugar, tops ...... 0.50 Biriba ...... 0.30 plied to the following raw agricultural Blueberry ...... 3.5 commodities. Compliance with the tol- Borage, seed ...... 0.05 erance levels specified in the table in Caneberry, subgroup 13-A ...... 2.5 Canistel ...... 1.0 this paragraph (a) is to be determined Canola, seed ...... 0.05 by measuring only furilazole, 3- Cattle, fat ...... 0.30 dichloroacetyl-5-(2-furanyl)-2, 2- Cattle, meat ...... 0.30 Cattle, meat byproducts ...... 0.30 dimethyloxazolidine (CAS Reg. No. Cherimoya ...... 0.30 121776–33–8) in or on the commodity. Citrus, dried pulp ...... 5.0 Coffee, bean, green ...... 0.80 Commodity Parts per Cotton, gin byproducts ...... 4.0 million Cotton, meal ...... 8.0 Cotton, undelinted seed ...... 6.0 Corn, field, forage ...... 0.01 Crambe, seed ...... 0.05 Corn, field, grain ...... 0.01 Cranberry ...... 0.05 Corn, field, stover ...... 0.01 Currant ...... 3.5 Corn, pop, grain ...... 0.01 Custard apple ...... 0.30 Corn, pop, stover ...... 0.01 Egg ...... 0.02 Corn, sweet, forage ...... 0.01 Elderberry ...... 3.5 Corn, sweet, kernel plus cob with husks removed 0.01 Feijoa ...... 1.0 Corn, sweet, stover ...... 0.01 Fish ...... 0.05 Sorghum, forage ...... 0.01 Fish-shellfish, mollusc ...... 0.05 Sorghum, grain ...... 0.01 Flax, seed ...... 0.05 Sorghum, stover ...... 0.01 Fruit, citrus, group 10 ...... 0.70 Fruit, pome, group 11 ...... 0.6 (b) Section 18 emergency exemptions. Fruit, stone, group 12 ...... 3.0 [Reserved] Goat, fat ...... 0.30 Goat, meat ...... 0.30 (c) Tolerances with regional registra- Goat, meat byproducts ...... 0.30 tions. [Reserved] Gooseberry ...... 3.5 (d) Indirect or inadvertent residues. Grain, cereal, forage, fodder and straw, group 16, [Reserved] forage, except rice ...... 7.0 Grain, cereal, forage, fodder and straw, group 16, [65 FR 8867, Feb. 23, 2000, as amended at 67 hay, except rice ...... 6.0 FR 15735, Apr. 3, 2002; 72 FR 57492, Oct. 10, Grain, cereal, forage, fodder and straw, group 16, 2007; 84 FR 52774, Oct. 3, 2019] stover, except rice ...... 0.30 Grain, cereal, forage, fodder and straw, group 16, straw, except rice ...... 3.0 § 180.472 Imidacloprid; tolerances for Grain, cereal, group 15, except rice ...... 0.05 residues. Grape ...... 1.0 Grape, juice ...... 1.5 (a) General. Tolerances are estab- Grape, raisin ...... 1.5 lished for residues of the insecticide Guava ...... 1.0 imidacloprid, including its metabolites Herbs subgroup 19A, dried herbs ...... 48 and degradates, in or on the commod- Herbs subgroup 19-A, fresh herbs ...... 8.0 Hog, fat ...... 0.30 ities in the table below. Compliance Hog, meat ...... 0.30 with the tolerance levels specified Hog, meat byproducts ...... 0.30 below is to be determined by measuring Hop, dried cones ...... 6.0 Horse, fat ...... 0.30 only the sum of imidacloprid (1-[6- Horse, meat ...... 0.30 chloro-3-pyridinyl) methyl]-N-nitro-2- Horse, meat byproducts ...... 0.30

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(b) Section 18 emergency exemptions. Commodity Parts per million Time-limited tolerances are estab- Huckleberry ...... 3.5 lished for residues of the insecticide Ilama ...... 0.30 imidacloprid, including its metabolites Jaboticaba ...... 1.0 Juneberry ...... 3.5 and degradates in connection with use Kava, leaves ...... 4.0 of the pesticide under a Section 18 Kava, roots ...... 0.40 emergency exemption granted by EPA. Leaf petioles subgroup 4B ...... 6.0 Leafy greens subgroup 4A ...... 3.5 Compliance with the tolerance levels Lettuce, head ...... 3.5 specified below is to be determined by Lettuce, leaf ...... 3.5 measuring only the sum of Lingonberry ...... 3.5 Longan ...... 3.0 imidacloprid (1-[6-chloro-3- Lychee ...... 3.0 pyridinyl)methyl]-N-nitro-2- Mango ...... 1.0 imidazolidinimine) and its metabolites Milk ...... 0.10 Mustard, black, seed ...... 0.05 containing the 6-chloropyridinyl moi- Mustard, field, seed ...... 0.05 ety, calculated as the stoichiometric Mustard, Indian, seed ...... 0.05 Mustard, rapeseed, seed ...... 0.05 equivalent of imidacloprid. These tol- Mustard, seed ...... 0.05 erances will expire and are revoked on Nut, tree, group 14 ...... 0.05 the dates specified in the following Okra ...... 1.0 Onion, dry bulbs, subgroup 3-07A ...... 0.15 table: Onion, green, subgroup 3-07B ...... 2.5 Papaya ...... 1.0 Parts per Expiration/ Passionfruit ...... 1.0 Commodity million revocation Peanut ...... 0.45 date Peanut, hay ...... 35 Peanut, meal ...... 0.75 Sugarcane, cane ...... 6.0 12/31/18 Pecan ...... 0.05 Sugarcane, molasses ...... 50 12/31/18 Persimmon ...... 3.0 Pistachio ...... 0.05 (c) Tolerances with regional registra- Pomegranate ...... 0.90 Potato, chip ...... 0.40 tions. [Reserved] Potato, processed potato waste ...... 0.90 (d) Indirect or inadvertent residues. Poultry, fat ...... 0.05 Tolerances are established for indirect Poultry, meat ...... 0.05 Poultry, meat byproducts ...... 0.05 or inadvertent residues of the insecti- Pulasan ...... 3.0 cide imidacloprid, including its me- Rambutan ...... 3.0 Rapeseed, seed ...... 0.05 tabolites and degradates, in or on the Raspberry, wild ...... 2.5 commodities in the table below. Com- Safflower, seed ...... 0.05 pliance with the tolerance levels speci- Salal ...... 3.5 Sapodilla ...... 1.0 fied below is to be determined by meas- Sapote, black ...... 1.0 uring only the sum of imidacloprid (1- Sapote, mamey ...... 1.0 [6-chloro-3-pyridinyl) methyl]-N-nitro- Sheep, fat ...... 0.30 Sheep, meat ...... 0.30 2-imidazolidinimine) and its metabo- Sheep, meat byproducts ...... 0.30 lites containing the 6-chloropyridinyl Soursop ...... 0.30 moiety, calculated as the stoichio- Soybean, forage ...... 8.0 Soybean, hay ...... 35 metric equivalent of imidacloprid, in Soybean, meal ...... 4.0 or on the following commodities, when Soybean, seed ...... 3.5 Spanish lime ...... 3.0 present therein as a result of the appli- Star apple ...... 1.0 cation of the pesticide to growing crops Starfruit ...... 1.0 listed in this section and other non- Strawberry ...... 0.50 Sugar apple ...... 0.30 food crops as follows: Sunflower, seed ...... 0.05 Tomato, paste ...... 6.0 Commodity Parts per Tomato, puree ...... 3.0 million Vegetable, brassica leafy, group 5 ...... 3.5 Vegetable, cucurbit, group 9 ...... 0.5 Rice, grain ...... 0 .05 Vegetable, fruiting, group 8 ...... 1.0 Vegetable, foliage of legume, group 7 ...... 2 .5 Vegetable, leaves of root and tuber, group 2 ...... 4.0 Vegetable, legume, group 6 ...... 0 .3 Vegetable, legume, group 6, except soybean ...... 4.0 Vegetable, root and tuber, group 1, except sugar beet ...... 0.40 [75 FR 22251, Apr. 28, 2010, as amended at 78 Watercress ...... 3.5 FR 33743, June 5, 2013; 80 FR 78145, Dec. 16, Watercress, upland ...... 3.5 2015] Wax jambu ...... 1.0

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§ 180.473 Glufosinate ammonium; tol- Commodity Parts per erances for residues. million (a) General. Tolerances are estab- Poultry, fat ...... 0.15 lished for residues of the herbicide Poultry, meat ...... 0.15 Poultry, meat byproducts ...... 0.60 glufosinate ammonium, including its Rice, grain ...... 1.0 metabolites and degradates, in or on Rice, hull ...... 2.0 the commodities in the table below. Salal ...... 0.10 Sheep, fat ...... 0.40 Compliance with the tolerance levels Sheep, meat ...... 0.15 specified below is to be determined by Sheep, meat byproducts ...... 6.0 measuring the sum of glufosinate am- Soybean ...... 2.0 Soybean, hulls ...... 10 monium, butanoic acid, 2-amino-4- (hydroxymethylphosphinyl) (b) Section 18 emergency exemptions. monoammonium salt, and its metabo- [Reserved] lites, 2-(acetylamino)-4- (c) Tolerances with regional restric- (hydroxymethyl phosphinyl)butanoic tions. [Reserved] acid, and 3- (d) Indirect or inadvertent residues. (hydroxymethylphosphinyl)propanoic Tolerances are established for indirect acid, expressed as 2-amino-4- or inadvertent residues of glufosinate (hydroxymethylphosphinyl)butanoic ammonium, including its metabolites acid equivalents: and degradates, in or on the commod- Parts per ities in the table below, as a result of Commodity million the application of glufosinate ammonium to crops listed in paragraph (a) of Almond, hulls ...... 0.50 Apple ...... 0.05 this section. Compliance with the tol- Banana ...... 0.30 erance levels specified below is to be Banana, pulp ...... 0.20 determined by measuring the sum of Beet, sugar, molasses ...... 5.0 Beet, sugar, roots ...... 0.9 glufosinate ammonium, butanoic acid, Beet, sugar, tops (leaves) ...... 1.5 2-amino-4-(hydroxymethylphosphinyl) Bushberry subgroup 13B ...... 0.15 monoammonium salt, and its metabo- Canola, meal ...... 1.1 lite, 3-(hydroxymethylphosphinyl) pro- Canola, seed ...... 0.40 Cattle, fat ...... 0.40 panoic acid, expressed as 2-amino-4- Cattle, meat ...... 0.15 (hydroxymethylphosphinyl)butanoic Cattle, meat byproducts ...... 6.0 acid equivalents. Corn, field forage ...... 4.0 Corn, field, grain ...... 0.20 Parts per Corn, field, stover ...... 6.0 Commodity million Corn, sweet, forage ...... 1.5 Corn, sweet, kernels plus cob with husks re- Barley, hay ...... 0.40 moved ...... 0.30 Barley, straw ...... 0.40 Corn, sweet, stover ...... 6.0 Buckwheat, fodder ...... 0.40 Cotton, gin byproducts ...... 15 Buckwheat, forage ...... 0.40 Cotton, undelinted seed ...... 4.0 Oat, forage ...... 0.40 Egg ...... 0.15 Oat, hay ...... 0.40 Fruit, citrus, group 10–10 ...... 0.15 Oat, straw ...... 0.40 Fruit, pome, group 11–10 ...... 0.25 Rye, forage ...... 0.40 Fruit, stone, group 12–12 ...... 0.30 Rye, straw ...... 0.40 Goat, fat ...... 0.40 Teosinte ...... 0.40 Goat, meat ...... 0.15 Triticale ...... 0.40 Goat, meat byproducts ...... 6.0 Wheat, forage ...... 0.40 Grain aspirated fractions ...... 25 Wheat, hay ...... 0.40 Grape ...... 0.05 Wheat, straw ...... 0.40 Hog, fat ...... 0.40 Hog, meat ...... 0.15 Hog, meat byproducts ...... 6.0 [68 FR 55849, Sept. 29, 2003, as amended at 71 Horse, fat ...... 0.40 FR 25945, May 3, 2006; 72 FR 72625, Dec. 21, Horse, meat ...... 0.15 2007; 76 FR 23497, Apr. 27, 2011; 77 FR 59113, Horse, meat byproducts ...... 6.0 Sept. 26, 2012; 80 FR 72599, Nov. 20, 2015; 84 FR Juneberry ...... 0.10 21708, May 15, 2019] Lingonberry ...... 0.10 Milk ...... 0.15 Nut, tree, group 14–12 ...... 0.50 § 180.474 Tebuconazole; tolerances for Olive ...... 0.50 residues. Pistachio ...... 0.10 (a) General. (1) Tolerances are estab- Potato ...... 0.80 Potato, chips ...... 1.6 lished for residues of tebuconazole, Potato granules/flakes ...... 2.0 alpha-[2-(4-chlorophenyl)ethyl]-alpha-

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(1,1-dimethylethyl)-1H-1,2,4-triazole-1- Commodity Parts per ethanol, including its metabolites and million degradates, in or on the commodities Vegetable, fruiting, group 8–10 ...... 1.3 in the table below. Compliance with Watercress ...... 9 the tolerance levels specified below is Wheat, forage ...... 3.0 Wheat, germ ...... 0.20 to be determined by measuring only Wheat, grain ...... 0.15 tebuconazole [a-[2-(4-chlorophenyl) Wheat, hay ...... 7.0 ethyl]-a-(1,1-dimethylethyl)-1H-1,2,4- Wheat, shorts ...... 0.20 triazole-1-ethanol], in or on the com- Wheat, straw ...... 1.5 modity. 1There are no U.S. registrations. (2) Tolerances are established for res- Parts per Commodity million idues of the fungicide tebuconazole, including its metabolites and degradates, Almond, hulls ...... 6.0 Apple, wet pomace ...... 0.1 in or on the commodities in the fol- Asparagus ...... 0.05 lowing table. Compliance with the tol- Banana ...... 0.05 erance levels specified in the following Barley, grain ...... 0.3 table is to be determined by measuring Barley, hay ...... 7.0 Barley, straw ...... 3.5 only the sum of tebuconazole (alpha-[2- Bean, dry seed ...... 0.1 (4-chlorophenyl)ethyl]-alpha-(1,1- Bean, succulent ...... 0.1 dimethylethyl)-1H-1,2,4-triazole-1-eth- Beet, garden, roots ...... 0.70 Beet, garden, tops ...... 7.0 anol) and its diol metabolite (1-(4- Brassica, leafy greens, subgroup 4–16B, except chlorophenyl)-4,4-dimethyl-3-(1H -1,2,4- watercress ...... 2.5 triazole-1-yl-methyl)-pentane-3,5-diol), Cherry, sweet, pre- and post-harvest ...... 5.0 Cherry, tart, pre- and post-harvest ...... 5.0 calculated as the stoichiometric equiv- Coffee, green bean 1 ...... 0.15 alent of tebuconzole, in or on the com- Coffee, roasted bean 1 ...... 0.3 modity. Corn, field, forage ...... 4.0 Corn, field, grain ...... 0.05 Parts per Corn, field, stover ...... 3.5 Commodity million Corn, pop, grain ...... 0.05 Corn, pop, stover ...... 3.5 Cattle, meat byproducts ...... 0.2 Corn, sweet, forage ...... 7.0 Goat, meat byproducts ...... 0 .2 Corn, sweet, kernel plus cob with husks removed 0.5 Horse, meat byproducts ...... 0 .2 Corn, sweet, stover ...... 6.0 Milk ...... 0.1 Cotton, gin byproducts ...... 25.0 Sheep, meat byproducts ...... 0 .2 Cottonseed, subgroup 20C ...... 2 Fruit, pome, group 11–10 ...... 1 Fruit, small, vine climbing, except fuzzy kiwifruit, (b) Section 18 emergency exemptions. subgroup 13–07F ...... 6 [Reserved] Ginseng, dried 1 ...... 0.40 (c) Tolerances with regional registra- Ginseng, fresh 1 ...... 0.15 tions. Tolerances are established for Grain, aspirated fractions ...... 16.0 Grass, forage ...... 8.0 residues of the fungicide tebuconazole, Grass, hay ...... 25.0 including its metabolites and Grass, seed screenings ...... 55.0 degradates, in or on the commodities Grass, straw ...... 30.0 Hop, dried cones ...... 35.0 in the following table. Compliance with Mango, postharvest ...... 0.15 the tolerance levels specified below is Nut, tree, group 14–12 ...... 0.05 to be determined by measuring only Oat, forage ...... 0.10 Oat, grain ...... 0.15 tebuconazole, alpha-[2-(4- Oat, hay ...... 0.10 chlorophenyl)ethyl]-alpha-(1,1- Oat, straw ...... 0.10 dimethylethyl)-1H-1,2,4-triazole-1-eth- Onion, bulb, subgroup 3-07A ...... 0.2 anol, in or on the commodity. Onion, green, subgroup 3-07B ...... 1.3 Orange 1 ...... 1.0 1 Parts per Orange, oil ...... 10 Commodity million Peach subgroup 12–12B ...... 2 Peanut ...... 0.1 Turnip, roots ...... 0.5 Plum subgroup 12–12C ...... 1 Turnip, tops ...... 7.0 Soybean, forage ...... 25 Soybean, hay ...... 50 Soybean, seed ...... 0.08 (d) Indirect or inadvertent residues. Sunflower, subgroup 20B ...... 0.1 [Reserved] Tropical and subtropical, small fruit, inedible peel, subgroup 24A ...... 1.6 [59 FR 39464, Aug. 3, 1994] Sunflower, meal ...... 0.2 Sunflower, refined oil ...... 0.2 EDITORIAL NOTE: For FEDERAL REGISTER ci- Vegetable, cucurbit, group 9 ...... 0.4 tations affecting § 180.474, see the List of CFR

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Sections Affected, which appears in the Parts per Finding Aids section of the printed volume Commodity million and at www.govinfo.gov. Rye, grain ...... 0.01 Rye, straw ...... 0.05 § 180.475 Difenoconazole; tolerances Soybean, hulls ...... 0.20 for residues. Soybean, seed ...... 0.15 (a) General. (1) Tolerances are estab- Tea, dried 1 ...... 15 lished for residues of difenoconazole, Vegetable, Brassica, head and stem, group 5–16 2.0 Vegetable, cucurbit, group 9 ...... 0.70 including its metabolites and Vegetable, fruiting, group 8–10 ...... 0.60 degradates, in or on the commodities Vegetable, leaves of root and tuber, group 2 ...... 8 in the following table. Compliance with Vegetable, root, subgroup 1A, except ginseng ..... 0.6 the tolerance levels specified below is Vegetable, tuberous and corm, subgroup 1C ...... 4.0 to be determined by measuring only Wax jambu 1 ...... 1.5 Wheat, forage ...... 0.1 difenoconazole, 1-[2-[2-chloro-4-(4- Wheat, grain ...... 0.1 chlorophenoxy)phenyl]-4-methyl-1,3- Wheat, hay ...... 0.05 dioxolan-2-ylmethyl]-1H-1,2,4-triazole, Wheat, straw ...... 0.1 in or on the following raw agricultural 1 There are no U.S. registrations for these commodities. commodities: 2 This tolerance expires on August 14, 2020.

Parts per (2) Tolerances are established for res- Commodity million idues of difenoconazole, including its metabolites and degradates, in the Almond, hulls ...... 7.0 Apple, wet pomace ...... 25 commodities in the table below. Com- Artichoke, globe ...... 1.5 pliance with the tolerance levels speci- Aspirated grain fractions ...... 95 fied below is to be determined by meas- Banana1 ...... 0.2 Barley, grain ...... 0.1 uring the sum of difenoconazole, 1-[2- Barley, hay ...... 0.05 [2-chloro-4-(4-chlorophenoxy)phenyl]-4- Barley, straw ...... 0.05 methyl-1,3-dioxolan-2-ylmethyl]-1H- Beet, sugar, dried pulp ...... 1.9 Berry, low growing, subgroup 13–07G, except 1,2,4-triazole, and its metabolite, CGA– cranberry ...... 2.5 205375, 1-[2-chloro-4-(4-chloro- Brassica, leafy greens, subgroup 4–16B ...... 35 phenoxy)phenyl]-2-[1,2,4]triazol-1-yl- Bushberry subgroup 13–07B ...... 4.0 ethanol, calculated as the stoichio- Citrus, dried pulp ...... 2.0 Citrus, oil ...... 25 metric equivalent of difenoconazole, in Corn, sweet, forage ...... 0.01 the following commodities: Corn, sweet, kernel plus cob with husks removed 0.01 Corn, sweet, stover ...... 0.01 Parts per Cotton, gin byproducts ...... 15 Commodity million Cottonseed subgroup 20C ...... 0.40 Cranberry ...... 0.60 Cattle, fat ...... 0.10 Dragonfruit1 ...... 1.5 Cattle, liver ...... 0.7 Fruit, citrus, group 10–10 ...... 0.60 Cattle, meat ...... 0.05 Fruit, pome, group 11–10 ...... 5.0 Cattle, meat byproduct (except liver) ...... 0.10 Fruit, small, vine climbing, except fuzzy kiwifruit, Egg ...... 0.02 subgroup 13–07F ...... 3.0 Goat, fat ...... 0.10 Fruit, stone, group 12–12 ...... 2.5 Goat, liver ...... 0.7 Ginseng 2 ...... 1.0 Ginseng ...... 0.8 Goat, meat ...... 0.05 Grape, raisin ...... 6.0 Goat, meat byproduct (except liver) ...... 0.10 Guava ...... 3.0 Hog, fat ...... 0.10 Kohlrabi ...... 2.0 Hog, liver ...... 0.40 Mango 1 ...... 0.07 Hog, meat ...... 0.05 Nut, tree, group 14–12 ...... 0.03 Hog, meat byproduct (except liver) ...... 0.10 Oat, forage ...... 0.15 Horse, fat ...... 0.10 Oat, grain ...... 0.01 Horse, liver ...... 0.7 Oat, hay ...... 0.05 Horse, meat ...... 0.05 Oat, straw ...... 0.05 Horse, meat byproduct (except liver) ...... 0.10 Onion, bulb, subgroup 3-07A ...... 0.20 Milk ...... 0.02 Onion, green, subgroup 3-07B ...... 6.0 Sheep, fat ...... 0.10 Papaya ...... 0.60 Sheep, liver ...... 0.7 Pea and bean, dried shelled, except soybean, Sheep, meat ...... 0.05 subgroup 6C ...... 0.20 Sheep, meat byproduct (except liver) ...... 0.10 Pea, field, hay ...... 40 Pea, field, vines ...... 10 Potato, wet peel ...... 7.3 (b) Section 18 emergency exemptions. Rapeseed subgroup 20A ...... 0.10 [Reserved] Rice, grain ...... 7.0 Rice, wild, grain ...... 7.0 (c) Tolerances with regional registra- Rye, forage ...... 0.15 tions. [Reserved]

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(d) Indirect or inadvertent residues. (trifluoromethyl)phenyl)imino)-2- [Reserved] propoxyethyl)-1 H -imidazole, the metabolite 4-chloro-2-hydroxy-6- [64 FR 36254, July 6, 1999] trifluoromethylaniline sulfate, and EDITORIAL NOTE: For FEDERAL REGISTER ci- other metabolites containing the 4- tations affecting § 180.475, see the List of CFR chloro-2-trifluoromethylaniline moi- Sections Affected, which appears in the ety, calculated as the parent com- Finding Aids section of the printed volume and at www.govinfo.gov. pound. Parts § 180.476 Triflumizole; tolerances for Commodity per mil- residues. lion

(a) General. (1) Tolerances are estab- Cattle, fat ...... 0.10 lished for residues of the fungicide Cattle, meat byproducts ...... 0.20 triflumizole, including its metabolites Goat, fat ...... 0.10 Goat, meat byproducts ...... 0.20 and degradates, in or on the commod- Horse, fat ...... 0.10 ities listed in the table below. Compli- Horse, meat byproducts ...... 0.20 ance with the tolerance levels specified Sheep, fat ...... 0.10 below is to be determined by measuring Sheep, meat byproducts ...... 0.20 only the parent compound triflumizole, 1-(1-((4-chloro-2- (b) Section 18 emergency exemptions. (trifluoromethyl)phenyl)imino)-2- [Reserved] propoxyethyl)-1 H -imidazole, and its (c) Tolerances with regional registra- metabolites containing the 4-chloro-2- tions. [Reserved] trifluoromethylaniline moiety, cal- (d) Indirect or inadvertent residues. culated as stoichiometric equivalent of [Reserved] the parent compound. [65 FR 33702, May 24, 2000, as amended at 67 FR 40228, June 12, 2002; 67 FR 54587, Aug. 23, Parts 2002; 70 FR 7047, Feb. 10, 2005; 70 FR 17915, Commodity per million Apr. 8, 2005; 71 FR 13279, Mar. 15, 2006; 71 FR 49358, Aug. 23, 2006; 74 FR 26543, June 3, 2009; Berry, low growing, subgroup 13–07G, except 74 FR 46376, Sept. 9, 2009; 76 FR 34885, June 15, cranberry ...... 2.0 2011; 79 FR 12408, Mar. 5, 2014; 80 FR 72599, Brassica, head and stem, subgroup 5A ...... 8.0 Nov. 20, 2015] Brassica, leafy greens, subgroup 5B ...... 40 Canistel ...... 2.5 Cherry, sweet ...... 1.5 § 180.477 Flumiclorac pentyl; toler- Cherry, tart ...... 1.5 ances for residues. Cilantro, leaves ...... 35 Fruit, pome, group 11–10 ...... 0.50 (a) General. Tolerances are estab- Fruit, small, vine climbing, except fuzzy kiwifruit, lished for residues of the herbicide subgroup 13–07F ...... 2.5 flumiclorac pentyl, including its me- Hazelnut ...... 0.05 Hop, dried cones ...... 50 tabolites and degradates, in or on the Leafy greens subgroup 4A, except spinach ...... 35 commodities in the table in this para- Mango ...... 2.5 graph. Compliance with the tolerance Papaya ...... 2.5 levels specified in this paragraph is to Pineapple ...... 4.0 Sapodilla ...... 2.5 be determined by measuring only Sapote, black ...... 2.5 flumiclorac pentyl, pentyl(2-chloro-4- Sapote, mamey ...... 2.5 fluoro-5-(1,3,4,5,6,7-hexahydro-1,3-dioxo- Star apple ...... 2.5 Swiss chard ...... 18 2H-isoindol-2-yl)phenoxy)acetate, in or Tomato ...... 1.5 on the commodity. Turnip, greens ...... 40 Vegetable, cucurbit, group 9 ...... 0.5 Parts per Commodity million (2) Tolerances are established for res- Corn, field, forage ...... 0.01 idues of the fungicide triflumizole, in- Corn, field, grain ...... 0.01 cluding its metabolites and degradates, Corn, field, stover ...... 0.01 in or on the commodities of animal ori- Cotton, gin byproducts ...... 3.0 Cotton, undelinted seed ...... 0.2 gin listed in the table below. Compli- Soybean, hulls ...... 0.02 ance with the tolerance levels specified Soybean, seed ...... 0.01 below is to be determined by measuring only the parent compound triflumizole, (b) Section 18 emergency exemptions. 1-(1-((4-chloro-2- [Reserved]

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(c) Tolerances with regional registra- pyrimidinyl)amino] carbonyl]-3- tions. [Reserved] (ethylsulfonyl)-2-pyridinesulfonamide. (d) Indirect or inadvertent residues. [Reserved] Parts per Commodity million [65 FR 33702, May 24, 2000, as amended at 71 FR 11533, Mar. 8, 2006; 76 FR 23497, Apr. 27, Fescue, forage ...... 0.01 Fescue, hay ...... 0.01 2011] Ryegrass, perennial, forage ...... 0.01 Ryegrass, perennial, hay ...... 0.01 § 180.478 Rimsulfuron; tolerances for residues. (d) Indirect or inadvertent residues. (a) General. Tolerances are estab- [Reserved] lished for residues of the herbicide rimsulfuron, including its metabolites [63 FR 16696, Apr. 6, 1998, as amended at 72 and degradates, in or on the commod- FR 41913, Aug. 1, 2007; 74 FR 67137, Dec. 18, ities in the following table. Compliance 2009; 77 FR 3625, Jan. 25, 2012; 77 FR 46306, Aug. 3, 2012; 80 FR 66805, Oct. 30, 2015; 83 FR with the tolerance levels specified in 5947, Feb. 12, 2018] the following table is to be determined by measuring only rimsulfuron, N- § 180.479 Halosulfuron-methyl; toler- [[(4,6-dimethoxy-2-pyrimidinyl)amino] ances for residues. carbonyl]-3-(ethylsulfonyl)-2- (a) General. (1) Tolerances are estab- pyridinesulfonamide. lished for residues of the herbicide halosulfuron-methyl, methyl 5-[(4,6- Commodity Parts per million dimethoxy-2-pyrimidiny)amino] Almond, hulls ...... 0.09 carbonylaminosulfonyl]-3-chloro-1- Berry, low growing, except strawberry, subgroup methyl-1H-pyrazole-4-carboxylate, in- 13–07H ...... 0.02 cluding its metabolites and degradates, Bushberry, subgroup 13–07B ...... 0.01 Caneberry, subgroup 13–07A ...... 0.01 in or on the commodities in the fol- Chicory, roots ...... 0.01 lowing table. Compliance with the tol- Chicory, tops ...... 0.01 erance levels specified in the following Corn, field, forage ...... 0.4 Corn, field, grain ...... 0.1 table is to be determined by measuring Corn, field, stover ...... 2.5 only those halosulfuron-methyl resi- Fruit, citrus, group 10–10 ...... 0.01 dues containing the 3- Fruit, pome, group 11–10 ...... 0.01 Fruit, small, vine climbing, except fuzzy kiwifruit, chlorosulfonamide (3-CSA) moiety, ex- subgroup 13–07F ...... 0.01 pressed as the stoichiometric equiva- Fruit, stone, group 12–12 ...... 0.01 lent of halosulfuron-methyl, in or on Grain, aspirated fractions ...... 4.5 the commodity. Nut, tree, group 14–12 ...... 0.01 Potato 1 ...... 0.1 Sorghum, grain, forage ...... 0.01 Commodity Parts per Sorghum, grain, grain ...... 0.01 million Sorghum, grain, stover ...... 0.01 Soybean, forage ...... 0.25 Cattle, fat ...... 0.05 Soybean, hay ...... 1.2 Cattle, meat ...... 0.05 Soybean, hulls ...... 0.04 Cattle, meat byproducts ...... 1.0 Soybean, seed ...... 0.01 Goat, fat ...... 0.05 Tomato ...... 0.05 Goat, meat ...... 0.05 Vegetable, tuberous and corm, subgroup 1C ...... 0.10 Goat, meat byproducts ...... 1.0 Hog, meat byproducts ...... 0.1 1 This tolerance expires on August 12, 2018. Horse, fat ...... 0.05 (b) Section 18 emergency exemptions. Horse, meat ...... 0.05 [Reserved] Horse, meat byproducts ...... 1.0 (c) Tolerances with regional registra- Milk ...... 0.05 Sheep, fat ...... 0.05 tions. Tolerances with regional reg- Sheep, meat ...... 0.05 istrations, as defined in § 180.1(1), are Sheep, meat byproducts ...... 1.0 established for residues of the herbicide rimsulfuron, including its metabo- (2) Tolerances are established for res- lites and degradates, in or on the com- idues of the herbicide halosulfuron- modities in the following table. Com- methyl, methyl 5-[(4,6-dimethoxy-2- pliance with the tolerance levels spe- pyrimidiny)amino] cific in the following table is to be de- carbonylaminosulfonyl]-3-chloro-1- termined by measuring only methyl-1H-pyrazole-4-carboxylate, in- rimsulfuron, N-[[(4,6-dimethoxy-2- cluding its metabolites and degradates,

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in or on the commodities in the fol- Commodity Parts per lowing table. Compliance with the tol- million erance levels specified in the following Fruit, small vine climbing, except fuzzy kiwifruit, table is to be determined by measuring subgroup 13–07F ...... 0 .05 only halosulfuron-methyl. (d) Indirect or inadvertent residues. Parts per [Reserved] Commodity million [64 FR 25448, May 12, 1999, as amended at 65 Alfalfa, forage ...... 1.0 FR 58433, Sept. 29, 2000; 66 FR 66340, Dec. 26, Alfalfa, hay ...... 2.0 2001; 66 FR 66786, Dec. 27, 2001; 67 FR 45649, Almond, hulls ...... 0.2 July 10, 2002; 67 FR 59192, Sept. 20, 2002; 70 FR Artichoke ...... 0.05 51622, Aug. 31, 2005; 72 FR 8927, Feb. 28, 2007; Asparagus ...... 0.8 Bean, dry, seed ...... 0.05 74 FR 48401, Sept. 23, 2009; 75 FR 46853, Aug. Bushberry, subgroup 13-07B ...... 0.05 4, 2010; 76 FR 34886, June 15, 2011; 77 FR 71561, Caneberry subgroup 13–07A ...... 0.05 Dec. 3, 2012; 78 FR 53051, Aug. 28, 2013; 80 FR Corn, field, forage ...... 0.2 55773, Sept. 17, 2015; 80 FR 72599, Nov. 20, 2015] Corn, field, grain ...... 0.05 Corn, field, stover ...... 0.8 § 180.480 Fenbuconazole; tolerances Corn, pop, grain ...... 0.05 for residues. Corn, pop, stover ...... 0.8 Corn, sweet, forage ...... 0.2 (a) Tolerances are established for res- Corn, sweet, kernel plus cob with husks removed 0.05 idues of the fungicide fenbuconazole, Corn, sweet, stover ...... 0.8 including its metabolites and Cotton, gin byproducts ...... 0.05 degradates, in or on the commodities Cotton, undelinted seed ...... 0.05 in the table below. Compliance with Fruit, pome, group 11–10 ...... 0.05 Grass, forage, fodder, and hay, group 17, forage 20 the tolerance levels specified below is Grass, forage, fodder, and hay, group 17, hay ..... 0.5 to be determined by measuring only Melon subgroup 9A ...... 0.1 the sum of fenbuconazole, alpha-[2-(4- Millet, proso, forage ...... 10 chlorophenyl)-ethyl]-alpha-phenyl-3- Millet, proso, grain ...... 0.01 (1H-1,2,4-triazole)-1-propanenitrile, and Millet, proso, hay ...... 0.01 Millet, proso, straw ...... 0.01 its metabolites RH-9129, cis-5-(4- Nut, tree, group 14 ...... 0.05 chlorophenyl)-dihydro-3-phenyl-3-(1H- Okra ...... 0.05 1,2,4-triazole-1-ylmethyl)-2-3 H- Pea and bean, succulent shelled, subgroup 6 ...... 0.05 furanone, and RH-9130, trans-5-(4- Pea and bean, succulent shelled, subgroup 6B ... 0.05 chlorophenyl)-dihydro-3-phenyl-3-(1H- Pistachio ...... 0.05 Rhubarb ...... 0.05 1,2,4-triazole-1-ylmethyl)-2-3 H- Rice, grain ...... 0.05 furanone, calculated as the stoichio- Sorghum, grain, forage ...... 0.05 metric equivalent of fenbuconazole, in Sorghum, grain, grain ...... 0.05 or on the following agricultural com- Sorghum, grain, stover ...... 0.1 Soybean, seed ...... 0.05 modities. Squash/Cucumber subgroup 9B ...... 0.5 Parts per Sugarcane, cane ...... 0.05 Commodity million Vegetable, fruiting, group 8 ...... 0.05 Vegetable, tuberous and corm, subgroup 1C ...... 0.05 Almond ...... 0.05 Almond, hulls ...... 1.0 (b) Section 18 emergency exemptions. Apple ...... 0.4 Apple, wet pomace ...... 1.0 [Reserved] Banana ...... 0.3 (c) Tolerances with regional registra- Beet, sugar, dried pulp ...... 1.0 tions. Tolerances with regional reg- Beet, sugar, molasses ...... 0.4 Beet, sugar, roots ...... 0.3 istrations are established for residues Beet, sugar, tops ...... 9.0 of the herbicide halosulfuron-methyl, Bushberry subgroup 13B ...... 0.3 methyl 5-[(4,6-dimethoxy-2- Cattle, meat byproducts ...... 0.05 Citrus, dried pulp ...... 5.0 pyrimidiny)amino] Citrus, oil ...... 40.0 carbonylaminosulfonyl]-3-chloro-1- Cranberry ...... 0.5 methyl-1H-pyrazole-4-carboxylate, in- Fruit, citrus, group 10 ...... 1.0 cluding its metabolites and degradates, Fruit, stone, group 12 ...... 1.0 Goat, meat byproducts ...... 0.05 in or on the commodities in the fol- Grain, aspirated fractions ...... 6.0 lowing table. Compliance with the tol- Grape 1 ...... 1.0 erance levels specified in the following Horse, meat byproducts ...... 0.05 Peanut ...... 0.1 table is to be determined by measuring Pecan ...... 0.05 only halosulfuron-methyl. Pepper ...... 1.0

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Commodity Parts per § 180.482 Tebufenozide; tolerances for million residues. Sheep, meat byproducts ...... 0.05 (a) General. (1) Tolerances are estab- Tea, dried 2 ...... 30 lished for residues of the insecticide Tea, instant 2 ...... 30 tebufenozide, including its metabolites Wheat, forage ...... 4.0 Wheat, grain ...... 0.1 and degradates, in or on the commod- Wheat, hay ...... 8.0 ities in the table in this paragraph. Wheat, straw ...... 8.0 Compliance with the tolerance levels specified in this paragraph is to be de- 1 There are no United States registrations for grape as of August 2006. termined by measuring only 2 There are no U.S. registrations for use of fenbuconazole tebufenozide, 3,5-dimethylbenzoic acid on tea. 1-(1,1-dimethylethyl)-2-(4- (b) Section 18 emergency exemptions. ethylbenzoyl)hydrazide, in or on the [Reserved] commodity. (c) Tolerances with regional registra- Parts per tions. [Reserved] Commodity million (d) Indirect or inadvertent residues. Almond, hulls ...... 30 [Reserved] Apple, dry pomace ...... 3.0 Apple, wet pomace ...... 3.0 [60 FR 11032, Mar. 1, 1995] Bushberrry subgroup 13–07B ...... 3.0 Brassica, head and stem, subgroup 5A ...... 5.0 EDITORIAL NOTE: For FEDERAL REGISTER ci- Brassica, leafy greens, subgroup 5B ...... 10.0 tations affecting § 180.480, see the List of CFR Canola, refined oil ...... 4.0 Sections Affected, which appears in the Canola, seed ...... 2.0 Finding Aids section of the printed volume Caneberry subgroup 13–07A ...... 3.0 and at www.govinfo.gov. Citrus, oil ...... 15.0 Cotton ...... 1.5 Cotton, gin byproducts ...... 30 § 180.481 Prosulfuron; tolerances for Cranberry ...... 1.0 residues. Fruit, citrus, group 10–10 ...... 2.0 Fruit, pome 1 ...... 1.5 (a) General. Tolerances are estab- Fruit, pome, group 11–10 ...... 1.0 lished for residues of prosulfuron, in- Grape ...... 3.0 cluding its metabolites and degradates, Kiwifruit 2 ...... 0.5 Leaf petioles subgroup 4B ...... 2.0 in or on the commodities in the table Leafy greens subgroup 4A ...... 10.0 below. Compliance with the tolerance Nut, tree, group 14–12 ...... 0.1 levels specified below is to be deter- Peppermint, tops ...... 10.0 Spearmint, tops ...... 10.0 mined by measuring only prosulfuron Sugarcane, cane ...... 1.0 (N-[[(4-methoxy-6-methyl-1,3,5-triazin- Sugarcane, molasses ...... 3.0 2-yl)amino]carbonyl]-2-(3,3,3- Turnip, greens ...... 9.0 Turnip, roots ...... 0.3 trifluoropropyl)benzenesulfonamide) in Vegetable, fruiting, group 8–10 ...... 1.0 or on the commodity. Vegetable, tuberous and corm, except potato, subgroup 1D ...... 0.015 Parts per Commodity 1 This tolerance expires on May 16, 2018. million 2 There are no U.S. registrations on kiwifruit. Grain, cereal, forage, fodder, and straw, group (2) Tolerances are established for res- 16, forage ...... 0.10 idues of the insecticide tebufenozide, Grain, cereal, forage, fodder, and straw, group 16, hay ...... 0.20 including its metabolites and Grain, cereal, forage, fodder, and straw, group degradates, in or on the commodities 16, stover ...... 0.01 in the table in this paragraph. Compli- Grain, cereal, forage, fodder, and straw, group ance with the tolerance levels specified 16, straw ...... 0.02 in this paragraph is to be determined Grain, cereal, group 15 ...... 0.01 by measuring only the sum of (b) Section 18 emergency exemptions. tebufenozide, 3,5-dimethylbenzoic acid [Reserved] 1-(1,1-dimethylethyl)-2-(4- ethylbenzoyl)hydrazide, and its me- (c) Tolerances with regional registra- tabolites, 3,5-dimethylbenzoic acid 1- tion. [Reserved] (1,1-dimethylethyl)-2-((4- (d) Indirect or inadvertent residues. carboxymethyl)benzoyl)hydrazide, 3- [Reserved] hydroxymethyl-5-methylbenzoic acid 1- [74 FR 67118, Dec. 18, 2009, as amended at 82 (1,1-dimethylethyl)-2-(4- FR 31475, July 7, 2017] ethylbenzoyl)hydrazide, stearic acid

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conjugate of 3-hydroxymethyl-5- EDITORIAL NOTE: For FEDERAL REGISTER ci- methylbenzoic acid 1-(1,1- tations affecting § 180.482, see the List of CFR dimethylethyl)-2-(4- Sections Affected, which appears in the ethylbenzoyl)hydrazide, and 3- Finding Aids section of the printed volume and at www.govinfo.gov. hydroxymethyl-5-methylbenzoic acid 1- (1,1-dimethylethyl)-2-(4-(1-hydroxy- § 180.484 Flutolanil; tolerances for res- ethyl)benzoyl)hydrazide, calculated as idues. the stoichiometric equivalent of (a) General. Tolerances are estab- tebufenozide, in or on the commodity. lished for residues of flutolanil, N-(3-(1- methylethoxy) phenyl)-2- Commodity Parts per million (trifluoromethyl)benzamide, including Cattle, fat ...... 0.1 its metabolites and degradates, in or Cattle, meat ...... 0.08 on the commodities in the table below. Cattle, meat byproducts ...... 0.08 Compliance with the tolerance levels Goat, fat ...... 0.1 Goat, meat ...... 0.08 specified below is to be determined by Goat, meat byproducts ...... 0.08 measuring only flutolanil and its me- Hog, fat ...... 0.1 tabolites converted to 2- Hog, meat ...... 0.08 Hog, meat byproducts ...... 0.08 (trifluoromethyl) benzoic acid and cal- Horse, fat ...... 0.1 culated as flutolanil, in or on the fol- Horse, meat ...... 0.08 lowing commodities: Horse, meat byproducts ...... 0.08 Milk ...... 0.04 Parts per Sheep, fat ...... 0.1 Commodity million Sheep, meat ...... 0.08 Sheep, meat byproducts ...... 0.08 Cattle, fat ...... 0.10 Cattle, kidney ...... 1.00 (b) Section 18 emergency exemptions. Cattle, liver ...... 2.00 [Reserved] Cattle, meat byproducts ...... 0.05 Cattle, meat ...... 0.05 (c) Tolerances with regional registra- Cotton, gin byproducts ...... 0.20 tions. [Reserved] Cotton, undelinted seed ...... 0.20 (d) Indirect or inadvertent residues. Egg ...... 0.05 Tolerances are established for indirect Goat, fat ...... 0.10 Goat, kidney ...... 1.00 or inadvertent residues of the insecti- Goat, liver ...... 2.00 cide tebufenozide, including its me- Goat, meat byproducts ...... 0.05 tabolites and degradates, in or on the Goat, meat ...... 0.05 Hog, fat ...... 0.10 commodities in the table in this para- Hog, kidney ...... 1.00 graph when present therein as a result Hog, liver ...... 2.00 of the application of tebufenozide to Hog, meat byproducts ...... 0.05 growing crops listed in the table to Hog, meat ...... 0.05 Horse, fat ...... 0.10 paragraph (a)(1) of this section. Com- Horse, kidney ...... 1.00 pliance with the tolerance levels speci- Horse, liver ...... 2.00 fied in this paragraph is to be deter- Horse, meat byproducts ...... 0.05 Horse, meat ...... 0.05 mined by measuring only the sum of Milk ...... 0.05 tebufenozide, 3,5-dimethylbenzoic acid Peanut ...... 0.5 1-(1,1-dimethylethyl)-2-(4- Peanut, hay ...... 15.0 ethylbenzoyl)hydrazide, and its me- Peanut, meal ...... 1.0 Potato ...... 0.20 tabolite, 3,5-dimethylbenzoic acid 1- Potato, wet peel ...... 0.30 (1,1-dimethylethyl)-2-(4-(1-hydroxy- Poultry, fat ...... 0.05 ethyl)benzoyl)hydrazide, calculated as Poultry, meat ...... 0.05 Poultry, meat byproducts ...... 0.05 the stoichiometric equivalent of Rice, bran ...... 10.0 tebufenozide, in or on the commodity. Rice, grain ...... 7.0 Rice, hulls ...... 25.0 Commodity Parts per Sheep, fat ...... 0.10 million Sheep, kidney ...... 1.00 Sheep, liver ...... 2.00 Animal feed, nongrass, group 18 ...... 1 .0 Sheep, meat ...... 0.05 Grain, cereal, forage, fodder and straw, group Sheep, meat byproducts ...... 0.05 16 ...... 1 .0 Soybean, forage ...... 8.0 Grass, forage, fodder and hay, group 17 ...... 1 .0 Soybean, hay ...... 2.5 Vegetable, foliage of legume, group 7 ...... 0 .20 Soybean, seed ...... 0.20 Turnip, greens ...... 0.1 [60 FR 29347, May 31, 1995] Vegetable, brassica, leafy, group 5 ...... 0.1

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(b) Section 18 emergency exemptions. Commodity Parts per [Reserved] million (c) Tolerances with regional registra- Horse, meat byproducts (except liver) ...... 0.01 tions. [Reserved] Peanut ...... 0.01 (d) Indirect or inadvertent residues. Peanut, hay ...... 6.0 Sheep, fat ...... 0.01 Tolerances are established for the indi- Sheep, meat byproducts (except liver) ...... 0.01 rect or inadvertent residues of Soybean, forage ...... 1.0 flutolanil, N-(3-(1- Soybean, hay ...... 3.0 Soybean, oil ...... 0.10 methylethoxy)phenyl)-2- Soybean, seed ...... 0.05 (trifluoromethyl)benzamide, including Wheat, forage ...... 0.80 its metabolites and degradates, in or Wheat, grain ...... 0.05 Wheat, grain, milled byproducts ...... 0.10 on the commodities in the table below. Wheat, hay ...... 1.3 Compliance with the tolerance levels Wheat, straw ...... 0.90 specified below is to be determined by 1There are no U.S. registrations as of February 15, 2008 for measuring only flutolanil and its me- use on coffee bean. tabolites converted to 2- (2) A tolerance is established for the (trifluoromethyl) benzoic acid and cal- combined residues of the free and con- culated as flutolanil, in or on the fol- jugated forms of the fungicide lowing commodities. cyproconazole, including its metabo- Parts per lites and degradates, in or on the com- Commodity million modity in the table below. Compliance with the tolerance level specified below Wheat, bran ...... 0.20 Wheat, forage ...... 2.5 is to be determined by measuring only Wheat, grain ...... 0.05 the sum of cyproconazole (a-(4- Wheat, hay ...... 1.2 chlorophenyl)-a-(1-cyclopropylethyl)- Wheat, straw ...... 0.20 1H-1,2,4-triazole-1-ethanol) and its metabolite d-(4-chlorophenyl)-b,d- [60 FR 42458, Aug. 16, 1995, as amended at 61 dihydroxy-g-methyl-1H-1,2,4-triazole-1- FR 33044, June 26, 1996; 63 FR 42256, 42257, hexenoic acid, calculated as the stoi- Aug. 7, 1998; 66 FR 10825, Feb. 20, 2001; 71 FR 74818, Dec. 13, 2006; 72 FR 35665, June 29, 2007; chiometric equivalent of 73 FR 33017, June 11, 2008; 75 FR 17570, Apr. 7, cyproconazole, in or on the following 2010; 75 FR 80350, Dec. 22, 2010; 80 FR 72599, commodity: Nov. 20, 2015] Parts per Commodity million § 180.485 Cyproconazole; tolerances for residues. Milk ...... 0.02 (a) General. (1) Tolerances are established for residues of the free and con- (3) Tolerances are established for the jugated forms of the fungicide combined residues of the free and con- cyproconazole, including its metabo- jugated forms of the fungicide lites and degradates, in or on the com- cyproconazole, including its metabo- modities in the table below. Compli- lites and degradates, in or on the com- ance with the proposed tolerance levels modities in the table below. Compli- specified below is to be determined by ance with the tolerance level specified below is to be determined by measuring measuring only cyproconazole (a-(4- only the sum of cyproconazole ( -(4- chlorophenyl)-a-(1-cyclopropylethyl)- a 1H-1,2,4-triazole-1-ethanol) in or on the chlorophenyl)-a-(1-cyclopropylethyl)- following commodities: 1H-1,2,4-triazole-1-ethanol) and its metabolite 2-(4-chlorophenyl)-3- Commodity Parts per cyclopropyl-1-[1,2,4]triazol-1-yl-butane- million 2,3-diol, calculated as the stoichio- Aspirated grain fractions ...... 2.5 metric equivalent of cyproconazole, in Cattle, fat ...... 0.01 or on the following commodities: Cattle, meat byproducts (except liver) ...... 0.01 Coffee bean, green (Imported) 1 ...... 0.1 Parts per Corn, field, forage ...... 0.60 Commodity million Corn, field, grain ...... 0.01 Corn, field, stover ...... 1.2 Cattle, liver ...... 0.50 Goat, fat ...... 0.01 Goat, liver ...... 0.50 Goat, meat byproducts (except liver) ...... 0.01 Hog, liver ...... 0.01 Horse, fat ...... 0.01 Horse, liver ...... 0.50

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Parts per Parts per Commodity million Commodity million

Sheep, liver ...... 0.50 Cotton, undelinted seed ...... 0.02

(b) Section 18 emergency exemptions. (b) Section 18 emergency exemptions. [Reserved] [Reserved] (c) Tolerances with regional registra- (c) Tolerances with regional registrations. [Reserved] tions. [Reserved] (d) Indirect or inadvertent residues. (d) Indirect or inadvertent residues. [Reserved] [Reserved] [63 FR 53835, Oct. 7, 1998, as amended at 71 FR [62 FR 54783, Oct. 22, 1997, as amended at 64 71058, Dec. 8, 2006; 73 FR 27760, May 14, 2008; FR 56469, Oct. 20, 1999; 67 FR 72110, Dec. 4, 78 FR 37473, June 21, 2013] 2002]

§ 180.486 Chlorethoxyfos; tolerances § 180.490 Imazapic; tolerances for resi- for residues. dues. (a) General. Tolerances are estab- (a) General. (1) Tolerances are established for residues of the insecticide lished for residues of the herbicide chlorethoxyfos, including its metabo- imazapic, including its metabolites and lites and degradates, in or on the com- degradates, in or on the commodities modities in the table in this paragraph. listed in the following table. Compli- Compliance with the tolerance levels ance with the tolerance levels specified specified in this paragraph is to be de- is to be determined by measuring the termined by measuring only sum of imazapic (2-[4,5-dihydro-4-meth- chlorethoxyfos, O,O-diethyl O-(1,2,2,2- yl-4-(1-methylethyl)-5-oxo-1H-imidazol- tetrachloroethyl) phosphorothioate, in 2-yl]-5-methyl-3-pyridinecarboxylic acid) and its metabolites (±)-2-[4,5- or on the commodity. dihydro-4-methyl-4-(1-methylethyl)-5- oxo-1H-imidazol-2-yl]-5- Commodity Parts per million hydroxymethyl-3-pyridinecarboxylic ± Corn, field, forage ...... 0.01 acid and ( )-2-[4,5-dihydro-4-methyl-4- Corn, field, grain ...... 0.01 (1-methylethyl)-5-oxo-1H-imidazol-2- Corn, field, stover ...... 0.01 yl]-5-(b-D-glucopyranosyloxy)methyl-3- Corn, pop, grain ...... 0.01 pyridinecarboxylic acid, calculated as Corn, pop, stover ...... 0.01 Corn, sweet, forage ...... 0.01 the stoichiometric equivalent of Corn, sweet, kernel plus cob with husks removed 0.01 imazapic. Corn, sweet, stover ...... 0.01 Commodity Parts per (b) Section 18 emergency exemptions. million [Reserved] Grass, forage ...... 15 (c) Tolerances with regional registra- Grass, hay ...... 30 Peanut ...... 0.1 tions. [Reserved] Soybean, seed 1 ...... 0.40 (d) Indirect or inadvertent residues. Sugarcane, cane 2 ...... 0.03 [Reserved] 1 There are no US registrations as of April 4, 2014. 2 There are no U.S. registrations as of June 4, 2014. [76 FR 23498, Apr. 27, 2011] (2) Tolerances are established for res- § 180.487 Pyrithiobac sodium; toler- idues of the herbicide imazapic, includ- ances for residues. ing its metabolites and degradates, in (a) General. Tolerances are estab- or on the commodities listed in the fol- lished for residues of the herbicide, lowing table. Compliance with the tol- pyrithiobac sodium, (sodium 2-chloro- erance levels specified is to be deter- 6-[(4,6-dimethoxypyrimidin-2- mined by measuring the sum of yl)thio]benzoate), resulting from the imazapic (2-[4,5-dihydro-4-methyl-4-(1- application of the pesticide chemical in methylethyl)-5-oxo-1H-imidazol-2-yl]-5- or on the following foods/feeds: methyl-3-pyridinecarboxylic acid) and its metabolite (±)-2-[4,5-dihydro-4- Commodity Parts per methyl-4-(1-methylethyl)-5-oxo-1H- million imidazol-2-yl]-5-hydroxymethyl-3- Cotton, gin byproducts ...... 0.15 pyridinecarboxylic acid, calculated as

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the stoichiometric equivalent of commodities in the table in this para- imazapic. graph. Compliance with the tolerance levels specified in this paragraph is to Parts per Commodity million be determined by measuring only the sum of propylene chlorohydrin (1- Cattle, fat ...... 0.10 chloro-2-propanol), and its isomer 2- Cattle, kidney ...... 1.0 Cattle, meat byproducts, except kidney ...... 0.1 chloro-1-propanol, calculated as the Cattle, meat ...... 0.1 stoichiometric equivalent of propylene Goat, fat ...... 0.1 chlorohydrin (1-chloro-2-propanol), Goat, kidney ...... 1.0 Goat, meat byproducts, except kidney ...... 0.1 that results from the use of propylene Goat, meat ...... 0.1 oxide as a postharvest fumigant, in or Horse, fat ...... 0.1 on the commodity. Horse, kidney ...... 1.0 Horse, meat byproducts, except kidney ...... 0.1 Horse, meat ...... 0.1 OMMODITY Milk ...... 0.1 Sheep, fat ...... 0.1 Parts per Commodity million Sheep, kidney ...... 1.0 Sheep, meat byproducts, except kidney ...... 0.1 Basil, dried leaves ...... 6000 Sheep, meat ...... 0.1 Cacao bean, cocoa powder ...... 20.0 Cacao bean, dried bean ...... 20.0 (b) Section 18 emergency exemptions. Fig ...... 3.0 [Reserved] Garlic, dried ...... 6000 Grape, raisin ...... 4.0 (c) Tolerances with regional registra- Herbs and spices, group 19, dried, except basil .. 1500 tions. [Reserved] Nut, pine ...... 10.0 (d) Indirect or inadvertent residues. Nut, tree, group 14 ...... 10.0 Nutmeat, processed, except peanuts ...... 10.0 [Reserved] Onion, dried ...... 6000 [64 FR 54224, Oct. 6, 1999, as amended at 66 FR Pistachio ...... 10.0 Plum, prune, dried ...... 2.0 64774, Dec. 14, 2001; 66 FR 66332, Dec. 26, 2001; 78 FR 49932, Aug. 16, 2013; 79 FR 18818, Apr. 4, 2014; 79 FR 32170, June 4, 2014] (b) Section 18 emergency exemptions. [Reserved] § 180.491 Propylene oxide; tolerances (c) Tolerances with regional registra- for residues. tions. [Reserved] (a) General. (1) Tolerances are estab- (d) Indirect or inadvertent residues. lished for residues of the fumigant pro- [Reserved] pylene oxide, including its metabolites [65 FR 33702, May 24, 2000, as amended at 68 and degradates, in or on the commod- FR 39430, July 1, 2003; 72 FR 49651, Aug. 29, ities in the table in this paragraph. 2007; 73 FR 54963, Sept. 24, 2008; 76 FR 38037, Compliance with the tolerance levels June 29, 2011; 77 FR 28495, May 15, 2012] specified in this paragraph is to be determined by measuring only propylene § 180.492 Triflusulfuron-methyl; tolerances for residues. oxide, when used as a postharvest fumigant, in or on the commodity. (a) General. Tolerances are established for residues of triflusulfuron- Commodity Parts per methyl, including its metabolites and million degradates, in or on the commodities Cacao bean, cocoa powder ...... 200 listed in the table below. Compliance Cacao bean, dried bean ...... 200 with the tolerance levels specified Fig ...... 3.0 Garlic, dried ...... 300 below is to be determined by measuring Grape, raisin ...... 1.0 only triflusulfuron-methyl (methyl 2- Herbs and spices, group 19, dried ...... 300 [[[[[4-(dimethylamino)-6-(2,2,2- Nut, pine ...... 300 Nut, tree, group 14 ...... 300 trifluoroethoxy)-1,3,5-triazin-2- Nutmeat, processed, except peanuts ...... 300 yl]amino]carbonyl]amino]sulfonyl]-3- Onion, dried ...... 300 methylbenzoate) in or on the following Pistachio ...... 300 commodities: Plum, prune, dried ...... 2.0 Parts per (2) Tolerances are established for res- Commodity million idues of the reaction product, pro- Beet, garden, roots ...... 0.01 pylene chlorohydrin, including its me- Beet, garden, tops ...... 0.02 tabolites and degradates, in or on the Beet, sugar, roots ...... 0.05

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to be determined by measuring only Commodity Parts per million dimethomorph in or on the commodity. Beet, sugar, tops ...... 0.05 Chicory, roots ...... 0.05 Parts per Commodity million

(b) Section 18 emergency exemptions. Bean, lima, succulent ...... 0.60 [Reserved] (c) Tolerances with regional registra- (d) Indirect or inadvertent residues. tions. [Reserved] Tolerances are established for the indi- (d) Indirect or inadvertent residues. rect or inadvertent residues of the fun- [Reserved] gicide dimethomorph, 4-[3-(4- [67 FR 40196, June 12, 2002, as amended at 76 chlorophenyl)-3-(3,4-dimethoxyphenyl)- FR 22625, Apr. 22, 2011] 1-oxo-2-propen-1-yl]morpholine, including its metabolites and degradates, in § 180.493 Dimethomorph; tolerances or on the commodities in the following for residues. table. Compliance with the tolerance (a) General. Tolerances are estab- levels specified in the following table is lished for residues of the fungicide to be determined by measuring only dimethomorph, 4-[3-(4-chlorophenyl)-3- dimethomorph in or on the commodity. (3,4-dimethoxyphenyl)-1-oxo-2-propen- 1-yl]morpholine, including its metabo- Commodity Parts per lites and degradates, in or on the com- million modities in the following table. Com- Wheat, forage ...... 0.15 pliance with the tolerance levels speci- Wheat, hay ...... 0.15 fied in the following table is to be de- Wheat, straw ...... 0.4 termined by measuring only dimethomorph in or on the commod- [62 FR 26416, May 14, 1997] ities. EDITORIAL NOTE: For FEDERAL REGISTER citations affecting § 180.493, see the List of CFR Commodity Parts per million Sections Affected, which appears in the Finding Aids section of the printed volume Brassica, head and stem, subgroup 5A ...... 6.0 Brassica, leafy greens, subgroup 5B ...... 30.0 and at www.govinfo.gov. Ginseng ...... 0.90 Grape ...... 3.0 § 180.494 Pyridaben; tolerance for resi- Grape, raisin ...... 7.0 dues. Hop, dried cones ...... 60 Onion, bulb, subgroup 3–07A ...... 0.6 (a) General. Tolerances are estab- Onion, green, subgroup 3–07B ...... 15.0 lished for residues of the insecticide Papaya 1 ...... 1.5 Potato ...... 0.05 pyridaben, including its metabolites Potato, wet peel ...... 0.20 and degradates, in or on the commod- Strawberry ...... 0.90 ities as indicated in the following Taro, corm ...... 0.5 Taro, leaves ...... 6.0 table. Compliance with the tolerance Turnip, greens ...... 20.0 levels specified below for plant com- Vegetable, cucurbit, group 9 ...... 0.5 modities is to be determined by meas- Vegetable, fruiting, group 8 ...... 1.5 Vegetable, leafy (except Brassica) group 4 ...... 30.0 uring the insecticide pyridaben [2-tert- 1 There are no U.S. registrations as of January 20, 2015. butyl-5-(4-tert-butylbenzylthio)-4- chloropyridazin-3(2H)-one] on the plant (b) Section 18 emergency exemptions. commodity. Compliance with the toler- [Reserved] ance levels specified below for animal (c) Tolerances with regional registra- commodities is to be determined by tions. Tolerances with regional reg- measuring the insecticide pyridaben istrations are established for residues and its metabolites, [2-tert-butyl-5-(4- of the fungicide dimethomorph, 4-[3-(4- (1-carboxy-1-methylethy 1) benzylthio)- chlorophenyl)-3-(3,4-dimethoxyphenyl)- 1-oxo-2-propen-1-yl]morpholine, includ- 4-chloropyridazin-3 (2H)one] and [2- ing its metabolites and degradates, in tert-butyl-5-[4(-1, l-dimethyl-2-hy- or on the commodities in the following droxyethyl)benzylthio-4- table. Compliance with the tolerance chloropyridazin-3(2H)one] on the ani- levels specified in the following table is mal commodity.

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Commodity Parts per § 180.495 Spinosad; tolerances for resi- million dues. Almond, hulls ...... 4.0 (a) General. Tolerances are estab- Apple, wet pomace ...... 0.75 lished for residues of the insecticide Berry, low growing, subgroup 13–07G, except cranberry ...... 2.5 spinosad, including its metabolites and Canistel ...... 0.10 degradates, in or on the commodities Cattle, fat ...... 0.05 in the table below. Compliance with Cattle, meat ...... 0.05 the tolerance levels specified below is Cattle, meat byproducts ...... 0.05 Citrus, dried pulp ...... 1.5 to be determined by measuring only Citrus, oil ...... 10.0 the sum of spinosyn A (Factor A: CAS Cucumber ...... 0.50 #131929–60–7; Fruit, citrus group 10–10 ...... 0.9 Fruit, pome group 11–10 ...... 0.75 (2R,3aS,5aR,5bS,9S,13S,14R,16aS,16bR)-2- Fruit, small, vine climbing, except fuzzy kiwifruit, [(6-deoxy-2,3,4-tri-O-methyl-a-L- subgroup 13–07F ...... 2.0 mannopyranosyl)oxy]-13-[[(2R,5S,6R)-5- Fruit, stone, group 12–12 ...... 3.0 (dimethylamino)tetrahydro-6-methyl- Goat, fat ...... 0.05 Goat, meat ...... 0.05 2H-pyran-2-yl]oxy]-9-ethyl- Goat, meat byproducts ...... 0.05 2,3,3a,5a,5b,6,9,10,11,12,13,14,16a,16b- Hog, fat ...... 0.05 tetradecahydro-14-methyl-1H-as- Hog, meat ...... 0.05 indaceno[3,2-d]oxacyclododecin-7,15- Hog, meat byproducts ...... 0.05 Hop, dried cones ...... 10.0 dione); and Spinosyn D (Factor D; CAS Horse, fat ...... 0.05 #131929–63–0) or Horse, meat ...... 0.05 (2S,3aR,5aS,5bS,9S,13S,14R,16aS,16bS)-2- Horse, meat byproducts ...... 0.05 [(6-deoxy-2,3,4-tri-O-methyl- -L- Mango ...... 0.10 a Milk ...... 0.01 mannopyranosyl)oxy]-13-[[(2R,5S,6R)-5- Nut, tree, group 14–12 ...... 0.05 (dimethylamino)tetrahydro-6-methyl- Papaya ...... 0.10 2H-pyran-2-yl]oxy]-9-ethyl- Sapodilla ...... 0.10 Sapote, black ...... 0.10 2,3,3a,5a,5b,6,9,10,11,12,13,14,16a,16b- Sapote, mamey ...... 0.10 tetradecahydro-4,14-dimethyl-1H-as- Sheep, fat ...... 0.05 indaceno[3,2-d]oxacyclododecin-7,15- Sheep, meat ...... 0.05 dione), calculated as the stoichio- Sheep, meat byproducts ...... 0.05 Star apple ...... 0.10 metric equivalent of spinosad. Tomato ...... 0.15 Parts per Commodity million (b) Section 18 emergency exemptions. [Reserved] Acerola ...... 1.5 (c) Tolerances with regional registra- Alfalfa, seed ...... 0.15 Alfalfa, seed screenings ...... 2.0 tions. Tolerances with regional reg- Almond, hulls ...... 19 istration, as defined in § 180.1(m) are es- Amaranth, grain, grain ...... 1.0 tablished for residues of the insecticide Amaranth, grain, stover ...... 10 Animal feed, nongrass, group, 18 ...... 0.02 pyridaben, including its metabolites Animal feed, nongrass, group, 18, forage ...... 35.0 and degradates, in or on the commod- Animal feed, nongrass, group, 18, hay ...... 30.0 ities in the table below. Compliance Apple, dry pomace ...... 0.5 Apple, wet pomace ...... 0.5 with the tolerance levels specified Artichoke, globe ...... 0.3 below is to be determined by measuring Asparagus ...... 0.2 the insecticide pyridaben [2-tert-butyl- Atemoya ...... 0.3 5-(4-tert-butylbenzylthio)-4- Avocado ...... 0.3 Banana ...... 0.25 chloropyridazin-3(2H)-one] on the fol- Beet, sugar, molasses ...... 0.75 lowing plant commodity. Berry, low growing, subgroup 13–07G, except cranberry ...... 0.90 Parts per Biriba ...... 0.3 Commodity million Brassica, head and stem, subgroup 5A ...... 2.0 Brassica, leafy greens, subgroup 5B ...... 10.0 Cranberry ...... 0.5 Bushberry subgroup 13–07B ...... 0.40 Caneberry subgroup 13–07A ...... 1.0 (d) Indirect or inadvertent residues. Canistel ...... 0.3 Cattle, fat ...... 50 [Reserved] Cattle, liver ...... 10 [65 FR 43712, July 14, 2000, as amended at 66 Cattle, meat ...... 2.0 Cattle, meat byproducts, except liver ...... 5.0 FR 33199, June 21, 2001; 70 FR 55769, Sept. 23, Cherimoya ...... 0.3 2005; 76 FR 56015, Sept. 15, 2010; 81 FR 70979, Citrus, oil ...... 3.0 Oct. 14, 2016] Citrus, dried pulp ...... 0.5

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Parts per Parts per Commodity million Commodity million

Coffee, green bean ...... 0.04 Sapote, mamey ...... 0.3 Corn, sweet, kernel plus cob with husks removed 0.02 Sapote, white ...... 0.3 Cotton, gin byproducts ...... 1.5 Sheep, fat ...... 50 Cottonseed subgroup 20C ...... 0.02 Sheep, liver ...... 10 Cranberry ...... 0.01 Sheep, meat ...... 2.0 Custard apple ...... 0.3 Sheep, meat byproducts, except liver ...... 5.0 Date ...... 0.10 Soursop ...... 0.3 Egg ...... 0.30 Feijoa ...... 05 Soybean ...... 0.02 Fig ...... 0.10 Spanish lime ...... 0.3 Fish ...... 4.0 Spearmint, tops ...... 3.5 Fish-shellfish, crustacean ...... 4.0 Spice, subgroup 19B, except black pepper ...... 1.7 Fish-shellfish, mollusc ...... 4.0 Star apple ...... 0.3 Food commodities ...... 0.02 Starfruit ...... 0.3 Fruit, citrus, group 10–10 ...... 0.30 Sugar apple ...... 0.3 Fruit, pome, group 11–10 ...... 0.20 Tea, dried 1 ...... 2 Fruit, small, vine climbing, subgroup13–07F, ex- Tea, instant 1 ...... 2 cept fuzzy kiwifruit ...... 0.50 Ti, leaves ...... 10.0 Fruit, stone 12–12 ...... 0.20 Vegetable, cucurbit, group 9 ...... 0.3 Goat, fat ...... 50 Vegetable, foliage of legume, group 7 ...... 8.0 Goat, liver ...... 10 Goat, meat ...... 2.0 Vegetable, fruiting, group 8–10 ...... 0.40 Goat, meat byproducts, except liver ...... 5.0 Vegetable, leafy, except brassica, group 4 ...... 8.0 Grain, aspirated fractions ...... 200 Vegetable, leaves of root and tuber, group 2 ...... 10.0 Grain, cereal, group 15 ...... 1.5 Vegetable, legume, edible podded, subgroup 6A 0.30 Grain, cereal, group 16, forage, except rice ...... 2.5 Vegetable, root and tuber, group 1 ...... 0.10 Grain, cereal, group 16, hay, except rice ...... 10.0 Watercress ...... 8.0 Grain, cereal, group, 16, stover, except rice ...... 10.0 Wax jambu ...... 0.3 Grain, cereal, group, 16, straw, except rice ...... 1.0 1 Grape, raisin ...... 1.0 There are no U.S. registrations for use on tea. Grass, forage, fodder and hay, group 17, forage 10.0 (b) Section 18 emergency exemptions. Grass, forage, fodder and hay, group 17, hay ...... 5.0 Guava ...... 0.3 [Reserved] Herb subgroup 19A, dried ...... 22 (c) Tolerances with regional registra- Herb subgroup 19A, fresh ...... 3.0 tions. [Reserved] Hog, fat ...... 5.0 Hog, meat ...... 0.50 (d) Indirect or inadvertant residues. Hog, meat byproducts ...... 2.0 [Reserved] Hop, dried cones ...... 22 Horse, fat ...... 50 [72 FR 68540, Dec. 5, 2007, as amended at 74 Horse, liver ...... 10 FR 46376, Sept. 9, 2009; 74 FR 48408, Sept. 23, Horse, meat ...... 2.0 2009; 75 FR 60327, Sept. 30, 2010; 80 FR 72599, Horse, meat byproducts, except liver ...... 5.0 Nov. 20, 2015; 80 FR 80672, Dec. 28, 2015; 84 FR Ilama ...... 0.3 Jaboticaba ...... 0.3 49201, Sept. 19, 2019] Longan ...... 0.3 Lychee ...... 0.3 § 180.498 Sulfentrazone; tolerances for Mango ...... 0.3 residues. Milk ...... 7.0 Milk, fat ...... 85 (a)(1) General. Tolerances are estab- Nut, tree, group 14–12 ...... 0.10 lished for the combined residues of the Onion, bulb, subgroup 3–07A ...... 0.10 free and conjugated forms of Onion, green, subgroup 3–07B ...... 4.0 Papaya ...... 0.3 sulfentrazone, including its metabo- Passionfruit ...... 0.3 lites and degradates, in or on the com- Pea and bean, dried shelled, except soybean, modities in the table below. Compli- subgroup 6C ...... 0.02 ance with the tolerance levels specified Pea and bean, succulent shelled, subgroup 6B ... 0.02 Peanut ...... 0.02 below is to be determined by measuring Peanut, hay ...... 11.0 only the sum of sulfentrazone (N-[2,4- Peppermint, tops ...... 3.5 dichloro-5-[4-(difluoromethyl)-4,5- Pineapple ...... 0.02 Pineapple, process residue ...... 0.08 dihydro-3-methyl-5-oxo-1H-1,2,4-triazol- Pomegranate ...... 0.30 1-yl]phenyl]methanesulfonamide) and Poultry, fat ...... 1.3 its metabolite HMS (N-(2,4-dichloro-5- Poultry, meat ...... 0.10 (4-(difluoromethyl)-4,5-dihydro-3- Poultry, meat byproducts ...... 0.20 Pulasan ...... 0.3 hydroxymethyl-5-oxo-1H-1,2,4-triazol-1- Quinoa, grain ...... 0.02 yl)phenyl)methanesulfonamide, cal- Rambutan ...... 0.3 culated as the stoichiometric equiva- Rice, hulls ...... 4.0 Sapodilla ...... 0.3 lent of sulfentrazone in or on the fol- Sapote, black ...... 0.3 lowing commodities.

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(c) Tolerances with regional registra- Commodity Parts per million tions. Tolerances with regional reg- Soybean, seed ...... 0.05 istration are established for the combined residues of the free and con- (2) Tolerances are established for the jugated forms of sulfentrazone, includ- combined residues of the free and con- ing its metabolites and degradates, in jugated forms of sulfentrazone, includ- or on the commodities in the table ing its metabolites and degradates, in below. Compliance with the tolerance or on the commodities in the table levels specified below is to be deter- below. Compliance with the tolerance mined by measuring only the sum of levels specified below is to be deter- sulfentrazone (N-[2,4-dichloro-5-[4- mined by measuring only the sum of (difluoromethyl)-4,5-dihydro-3-methyl- sulfentrazone (N-[2,4-dichloro-5-[4- 5-oxo-1H-1,2,4-triazol-1- (difluoromethyl)-4,5-dihydro-3-methyl- yl]phenyl]methanesulfonamide) and its 5-oxo-1H-1,2,4-triazol-1- metabolites HMS (N-(2,4-dichloro-5-(4- yl]phenyl]methanesulfonamide) and its (difluoromethyl)-4,5-dihydro-3- metabolites HMS (N-(2,4-dichloro-5-(4- hydroxymethyl-5-oxo-1H-1,2,4-triazol-1- (difluoromethyl)-4,5-dihydro-3- yl)phenyl)methanesulfonamide) and hydroxymethyl-5-oxo-1H-1,2,4-triazol-1- DMS (N-(2,4-dichloro-5-(4- yl)phenyl)methanesulfonamide) and (difluoromethyl)-4,5-dihydro-5-oxo-1H- DMS (N-(2,4-dichloro-5-(4- 1,2,4-triazol-1- (difluoromethyl)-4,5-dihydro-5-oxo-1H- yl)phenyl)methanesulfonamide, cal- 1,2,4-triazol-1- culated as the stoichiometric equiva- yl)phenyl)methanesulfonamide, cal- lent of sulfentrazone in or on the fol- culated as the stoichiometric equiva- lowing commodities. lent of sulfentrazone in or on the fol- Parts per lowing commodities. Commodity million

Parts per Bean, lima, succulent ...... 0.15 Commodity million Cowpea, succulent ...... 0.15 Wheat, forage ...... 0.50 Apple ...... 0.15 Wheat, grain ...... 0.15 Berry and small fruit, group 13–07 ...... 0.15 Wheat, hay ...... 0.30 Brassica, leafy greens, subgroup 4–16B ...... 0.60 Wheat, straw ...... 1.5 Chia, seed ...... 0.15 Corn, field, forage ...... 0.20 (d) Indirect or inadvertent residues. Corn, field, grain ...... 0.15 Tolerances are established for inad- Corn, field, stover ...... 0.30 Flax ...... 0.15 vertent and indirect combined residues Fruit, citrus, group 10–10 ...... 0.15 of the free and conjugated forms of Horseradish ...... 0.20 sulfentrazone, including its metabo- Melon, subgroup 9A ...... 0.15 lites and degradates, in or on the com- Nut, tree, group 14–12 ...... 0.15 Pea and bean, dried shelled, except soybean, modities in the table below. Compli- subgroup 6C ...... 0.15 ance with the tolerance levels specified Pea, succulent ...... 0.15 below is to be determined by measuring Peanut ...... 0.20 only the sum of sulfentrazone (N-[2,4- Peanut, meal ...... 0.40 Peppermint, tops ...... 0.30 dichloro-5-[4-(difluoromethyl)-4,5- Rhubarb ...... 0.15 dihydro-3-methyl-5-oxo-1H-1,2,4-triazol- Spearmint, tops ...... 0.30 1-yl]phenyl]methanesulfonamide) and Stalk and stem vegetable subgroup 22A ...... 0.15 its metabolites HMS (N-(2,4-dichloro-5- Sugarcane, cane ...... 0.15 Sugarcane, molasses ...... 0.20 (4-(difluoromethyl)-4,5-dihydro-3- Sunflower subgroup 20B ...... 0.20 hydroxymethyl-5-oxo-1H-1,2,4-triazol-1- Teff, forage ...... 0.50 yl)phenyl)methanesulfonamide) and Teff, grain ...... 0.15 DMS (N-(2,4-dichloro-5-(4- Teff, hay ...... 0.30 Teff, straw ...... 1.5 (difluoromethyl)-4,5-dihydro-5-oxo-1H- Turnip, roots ...... 0.15 1,2,4-triazol-1- Vegetable, Brassica, head and stem, group 5–16 0.20 yl)phenyl)methanesulfonamide, cal- Vegetable, fruiting, group 8–10 ...... 0.15 Vegetable, soybean, succulent ...... 0.15 culated as the stoichiometric equiva- Vegetable, tuberous and corm, subgroup 1C ...... 0.15 lent of sulfentrazone in or on the following commodities when present (b) Section 18 emergency exemptions. therein as a result of the application of [Reserved] sulfentrazone to growing crops.

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Parts per Parts per Commodity million Commodity million

Grain, cereal (excluding sweet corn), Hulls ...... 0.30 Bean, lima, succulent ...... 2 .0 Grain, cereal, forage, fodder and straw, group 16, except sweet corn; forage ...... 0.2 (d) Indirect or inadvertent residues. Grain, cereal, forage, fodder and straw, group 16, except sweet corn; hay ...... 0.2 [Reserved] Grain, cereal, forage, fodder and straw, group 16, except sweet corn; stover ...... 0.1 [62 FR 15620, Apr. 2, 1997, as amended at 62 Grain, cereal, forage, fodder and straw, group 16, FR 26966, May 16, 1997; 63 FR 32136, June 12, except sweet corn; straw ...... 0.6 1998; 64 FR 16843, Apr. 7, 1999; 65 FR 58399, Grain, cereal, group 15, except sweet corn ...... 0.1 Sept. 29, 2000; 66 FR 37598, July 19, 2001; 66 FR Grain, cereal, group 15, except sweet corn; bran 0.15 48585, Sept. 21, 2001; 67 FR 35049, May 17, 2002; 69 FR 47022, Aug. 4, 2004; 70 FR 7047, Feb. 10, [62 FR 10708, Mar. 10, 1997] 2005; 78 FR 33736, June 5, 2013; 82 FR 9523, Feb. 7, 2017; 84 FR 66620, Dec. 5, 2019] EDITORIAL NOTE: For FEDERAL REGISTER citations affecting § 180.498, see the List of CFR § 180.500 Imazapyr; tolerances for resi- Sections Affected, which appears in the dues. Finding Aids section of the printed volume and at www.govinfo.gov. (a) General. Tolerances are established for residues of the herbicide, § 180.499 Propamocarb; tolerances for imazapyr, including its metabolites residues. and degradates, in or on the commod- (a) General. Tolerances are estab- ities in the following table. Compliance lished for the residues of propamocarb, with the tolerance levels specified in including its metabolites and the following table is to be determined degradates, in or on the commodities by measuring only the residues of specified in table 1 to this paragraph imazapyr [2-[4,5-dihydro-4-methyl-4-(1- (a) resulting from the application of methylethyl)-5-oxo-1H-imidazol-2-yl]-3- the hydrochloride salt of propamocarb. pyridinecarboxylic acid]. Compliance with the tolerance levels Parts per in table 1 to this paragraph (a) is to be Commodity million determined by measuring only Cattle, fat ...... 0.05 propamocarb (propyl N-[3- Cattle, kidney ...... 0.20 (dimethylamino)propyl]carbamate): Cattle, meat ...... 0.05 Cattle, meat byproducts, except kidney ...... 0.05 TABLE 1 TO PARAGRAPH (a) Corn, field, forage ...... 0.05 Corn, field, grain ...... 0.05 Parts per Corn, field, stover ...... 0.05 Commodity million Fish ...... 1.0 Goat, fat ...... 0.05 Guava ...... 0.05 Goat, kidney ...... 0.20 Leafy greens subgroup 4–16A ...... 150 Goat, meat ...... 0.05 Starfruit ...... 0.05 Goats, meat byproducts, except kidney ...... 0.05 Tomato, paste ...... 5.0 Grass, forage ...... 100 Vegetable, cucurbit, group 9 ...... 1.5 Grass, hay ...... 30 Vegetable, fruiting, group 8–10 ...... 4 Horse, fat ...... 0.05 Vegetable, tuberous and corm, subgroup 1C ...... 0.3 Horse, kidney ...... 0.20 Horse, meat ...... 0.05 (b) Section 18 emergency exemptions. Horse, meat byproducts, except kidney ...... 0.05 Lentil 1 ...... 0.2 [Reserved] Milk ...... 0.01 (c) Tolerance with regional registra- Rapeseed subgroup 20A 1 ...... 0.05 tions. Tolerances with regional reg- Sheep, fat ...... 0.05 istrations are established for the resi- Sheep, kidney ...... 0.20 Sheep, meat ...... 0.05 dues of propamocarb, including its me- Sheep, meat byproducts, except kidney ...... 0.05 tabolites and degradates, in or on the Shellfish ...... 0.10 commodities specified in the following Soybean, meal 1 ...... 4.5 Soybean, seed 1 ...... 4.0 table resulting from the application of Sunflower subgroup 20B 1 ...... 0.05 the hydrochloride salt of propamocarb. Compliance with the following toler- 1 There are no U.S. Registrations. ance levels is to be determined by (b) Section 18 emergency exemptions. measuring only propamocarb (propyl [Reserved] N-[3- (c) Tolerances with regional registra- (dimethylamino)propyl]carbamate): tions. [Reserved]

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(d) Indirect or inadvertent residues. chloride (aviglycine HCl) in or on the [Reserved] following food commodities:

[68 FR 55484, Sept. 26, 2003, as amended at 78 Parts per FR 66653, Nov. 6, 2013; 79 FR 19487, Apr. 9, Commodity million 2014] Apple ...... 0.08 § 180.501 Hydroprene; tolerances for Fruit, stone, group 12, except cherry ...... 0.170 residues. Pear ...... 0.08 (a) General. A tolerance of 0.2 part per million is established for residues of (b) Section 18 emergency exemptions. hydroprene [(S)-(Ethyl (2E,4E,7S)- [Reserved] 3,7,11-trimrthyl-2,4-dodecadienoate)], (c) Tolerances with regional registra- (CAS Reg. No. 65733–18–8) on food com- tions. [Reserved] modities in food-handling establish- (d) Indirect or inadvertent residues. ments in accordance with the following [Reserved] prescribed conditions: [62 FR 24838, May 7, 1997, as amended at 64 (1) Application shall be limited to FR 31129, June 10, 1999; 66 FR 36481, 36484, spot, crack and crevice, perimeter and July 12, 2001; 69 FR 7606, Feb. 18, 2004] ultra low volume (ULV) fogging treatment in food storage or food-handling § 180.503 Cymoxanil, tolerance for resi- establishments, including warehouses, dues. food service, manufacturing, and processing establishments such as res- (a) General. Tolerances are estab- taurants, cafeterias, supermarkets, lished for residues of the fungicide, bakeries, breweries, dairies, meat cymoxanil, 2-cyano -N- slaughtering and packing plants, and [(ethylamino)carbonyl]-2- canneries where food and food products (methoxyimino) acetamide, in or on are held, processed, and served: Pro- the following food commodities: vided that the food is removed or cov- Parts per ered prior to such use, and food-proc- Commodity million essing surfaces are covered during treatment or thoroughly cleaned before Caneberry, subgroup 13A-07 ...... 4.0 using, or in the case of point-source de- Cilantro, leaves ...... 19 vice treatments, devices must not Hop, dried cones ...... 7.0 Leafy greens, subgroup 4A ...... 19 come into direct contact with food Leaf petioles, subgroup 4B ...... 6.0 preparation surfaces and must be in a Lychee 1 ...... 1.0 minimum distance of 3 feet from ex- Onion, bulb, subgroup 3-07A ...... 0.05 posed foods. Onion, green, subgroup 3-07B ...... 1.1 (2) To assure safe use of the insect Potato ...... 0.05 growth regulator, the label and label- Vegetable, cucurbit, group 9 ...... 0.05 ing shall conform to that registered by Vegetable, fruiting, group 8 ...... 0.2 the U.S. Environmental Protection 1 There is no U.S. registration for lychee. Agency, and it shall be used in accord- (b) Section 18 emergency exemptions. ance with such label and labeling. [Reserved] (b) Section 18 emergency exemptions. (c) Tolerances with a regional registra- [Reserved] Tolerances with a regional reg- (c) Tolerances with regional registration. tions. [Reserved] istration as defined in § 180.1(l) are es- (d) Indirect or inadvertent residues. tablished for the residues of the fun- [Reserved] gicide cymoxanil, 2-cyano -N- [(ethylamino)carbonyl]-2- [62 FR 61647, Nov. 19, 1997, as amended at 71 (methoxyimino) acetamide) in or on FR 74818, Dec. 13, 2006] the raw agricultural commodities: § 180.502 Aminoethoxyvinylglycine hy- Parts per drochloride (aviglycine HCl); toler- Commodity million ances for residues. (a) General. Tolerances are estab- Grape ...... 0.10 lished for residues of aminoethoxyvinylglycine hydro-

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(d) Indirect or inadvertent residues. and degradates, in or on the commod- [Reserved] ities in the following table. Compliance with the tolerance levels specified in [62 FR 26411, May 14, 1997, as amended at 62 FR 39956, July 25, 1997; 63 FR 24949, May 6, the following table is to be determined 1998; 63 FR 66464, Dec. 2, 1998; 64 FR 6539, Feb. by measuring only the sum of 10, 1999; 64 FR 47689, Sept. 1, 1999; 66 FR 37598, emamectin (MAB1a + MAB1b isomers) July 19, 2001; 67 FR 35049, May 17, 2002; 68 FR and the associated 8,9-Z isomers (8,9- 41936, July 16, 2003; 70 FR 7047, Feb. 10, 2005; ZB1a and 8,9-ZB1b). 72 FR 37646, July 11, 2007; 73 FR 58885, Oct. 8, 2008; 76 FR 34885, June 15, 2011] Parts per Commodity million

§ 180.504 [Reserved] Cattle, fat ...... 0.010 Cattle, liver ...... 0.050 § 180.505 Emamectin; tolerances for Cattle, meat ...... 0.003 residues. Cattle, meat byproducts, except liver ...... 0.020 Goat, fat ...... 0.010 (a) General. (1) Tolerances are estab- Goat, liver ...... 0.050 lished for emamectin, including its me- Goat, meat ...... 0.003 Goat, meat byproducts, except liver ...... 0.020 tabolites and degradates, in or on the Hog, fat ...... 0.003 commodities in the table below. Com- Hog, liver ...... 0.020 pliance with the tolerance levels speci- Hog, meat ...... 0.002 fied below is to be determined by meas- Hog, meat byproducts (except liver) ...... 0.005 Horse, fat ...... 0.010 uring only the sum of emamectin (a Horse, liver ...... 0.050 mixture of a minimum of 90% 4′-epi- Horse, meat ...... 0.003 Horse, meat byproducts, except liver ...... 0.020 methylamino-4′-deoxyavermectin B1a ′ Milk ...... 0.003 and maximum of 10% 4 -epi- Sheep, fat ...... 0.010 methylamino-4′-deoxyavermectin B1b) Sheep, liver ...... 0.050 and its metabolites 8,9-isomer of the Sheep, meat ...... 0.003 Sheep, meat byproducts, except liver ...... 0.020 B1a and B1b component of the parent ′ ′ (8,9-ZMA), or 4 -deoxy-4 -epi-amino- (b) Section 18 emergency exemptions. avermectin B1a and 4’-deoxy-4′-epi- ′ ′ [Reserved] amino-avermectin B1b; 4 -deoxy-4 -epi- (c) Tolerances with regional registra- amino avermectin B1a (AB1a); 4′-deoxy- ′ tions. [Reserved] 4 -epi-(N-formyl-N-methyl)amino- (d) Indirect and inadvertant residues. ′ ′ avermectin (MFB1a); and 4 -deoxy-4 - [Reserved] epi-(N-formyl)amino-avermectin B1a (FAB1a), calculated as the stoichio- [71 FR 18649, Apr. 12, 2006, as amended at 74 metric equivalent of emamectin. FR 2873, Jan. 16, 2009; 78 FR 18511, Mar. 27, 2013; 78 FR 49939, Aug. 16, 2013; 84 FR 44725, Parts per Aug. 27, 2019] Commodity million § 180.506 Cyclanilide; tolerances for Almond, hulls ...... 0.20 Apple, wet pomace ...... 0.075 residues. Artichoke, globe ...... 0.05 (a) General. Tolerances are estab- Brassica, leafy greens, subgroup 4–16B ...... 0.2 Celtuce ...... 0.1 lished for residues of the plant growth Cherry subgroup 12–12A ...... 0.09 regulator, cyclanilide, [1-(2,4- Cotton, gin byproducts ...... 0.050 dichlorophenylaminocarbonyl)- Cotton, undelinted seed ...... 0.025 cyclopropane carboxylic acid] deter- Fennel, florence, fresh leaves and stalk ...... 0.1 Fruit, pome, group 11–10 ...... 0.02 mined as 2,4-dichloroaniline (cal- Grape, wine 1 ...... 0.03 culated as cyclanilide) in or on the fol- Herb subgroup 19A ...... 0.4 lowing food commodities and processed Kohlrabi ...... 0.05 Leaf petiole vegetable subgroup 22B ...... 0.1 feed: Leafy greens subgroup 4–16A ...... 1 Nut, tree, group 14–12 ...... 0.02 Commodity Parts Per Tomato, paste ...... 0.150 Million Vegetable, brassica, head and stem, group 5–16 0.05 Vegetable, cucurbit, group 9 ...... 0.02 Cattle, fat ...... 0.10 Vegetable, fruiting, group 8–10 ...... 0.02 Cattle, meat ...... 0.02 Cattle, meat byproducts, except kidney ...... 0.2 1 There are no U.S. registrations for use of emamectin on Cattle, kidney ...... 2.0 grape, wine. Cotton, undelinted seed ...... 0.60 Cotton, gin byproducts ...... 25.0 (2) Tolerances are established for Goat, fat ...... 0.10 emamectin, including its metabolites Goat, meat ...... 0.02

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Parts Per Parts per Commodity Million Commodity million

Goat, meat byproducts, except kidney ...... 0.20 Brassica, leafy greens, subgroup 5B ...... 25 Goat, kidney ...... 2.0 Bushberry subgroup 13–07B ...... 5.0 Horse, fat ...... 0.10 Caneberry subgroup 13–07A ...... 5.0 Horse, meat ...... 0.02 Canistel ...... 2.0 Horse, meat byproducts, except kidney ...... 0.20 Cherimoya ...... 2.0 Horse, kidney ...... 2.0 Cilantro, leaves ...... 30.0 Hog, fat ...... 0.10 Citrus, dried pulp ...... 20.0 Hog, meat ...... 0.02 Citrus, oil ...... 40.0 Hog, meat byproducts, except kidney ...... 0.20 Coffee, green bean 1 ...... 0.03 Hog, kidney ...... 2.0 Corn, field, forage ...... 12.0 Milk ...... 0.04 Corn, field, grain ...... 0.05 Sheep, fat ...... 0.10 Corn, field, refined oil ...... 0.3 Sheep, meat ...... 0.20 Corn, field, stover ...... 25.0 Sheep, meat byproducts, except kidney ...... 0.20 Corn, pop, grain ...... 0.05 Sheep, kidney ...... 2.0 Corn, pop, stover ...... 25.0 Corn, sweet, forage ...... 12.0 Corn, sweet, kernel plus cob with husks removed 0.05 (b) Section 18 emergency exemptions. Corn, sweet, stover ...... 25.0 [Reserved] Cotton, gin byproducts ...... 45 (c) Tolerances with regional registra- Cottonseed subgroup 20C ...... 0.7 tions. [Reserved] Cranberry ...... 0.50 Custard apple ...... 2.0 (d) Indirect or inadvertent residues. Dragon fruit ...... 2.0 [Reserved] Feijoa ...... 2.0 Fruit, citrus, group 10–10 ...... 15.0 [62 FR 28355, May 23, 1997; 62 FR 34182, June Fruit, small vine climbing, except fuzzy kiwifruit, 25, 1997] subgroup 13–07F ...... 2.0 Fruit, stone, group 12–12 ...... 2.0 § 180.507 Azoxystrobin; tolerances for Ginseng 1 ...... 0.5 residues. Grain, aspirated fractions ...... 420 Grass, forage ...... 15 (a) General. (1) Tolerances are estab- Grass, hay ...... 20 lished for residues of the fungicide, Guava ...... 2.0 Herb Subgroup 19A, dried leaves ...... 260 azoxystrobin, including its metabolites Herb Subgroup 19A, fresh leaves ...... 50 and degradates, in or on the commod- Hop, dried cones ...... 20.0 ities in the following table. Compliance Ilama ...... 2.0 Jaboticaba ...... 2.0 with the tolerance levels specified in Jackfruit ...... 2.0 the table is to be determined by meas- Longan ...... 2.0 uring only the sum of azoxystrobin, Loquat ...... 2.0 [methyl(E)-2-(2-(6-(2-cyanophenoxy) Lychee ...... 2.0 Mango ...... 2.0 pyrimidin-4-yloxy)phenyl)-3- Nut, tree, group 14–12, except pistachio ...... 0.02 methoxyacrylate], and the Z-isomer of Oats, forage ...... 5.0 azoxystrobin [methyl(Z)-2-(2-(6-(2- Oats, grain ...... 1.5 Oats, hay ...... 10.0 cyanophenoxy)pyrimidin-4- Oats, straw ...... 3.0 yloxy)phenyl)-3 methoxyacrylate] in or Onion, bulb, subgroup 3–07A ...... 1.0 on the commodity. Onion, green, subgroup 3–07B ...... 7.5 Papaya ...... 2.0 Parts per Passionfruit ...... 2.0 Commodity million Pawpaw ...... 2.0 Pea and bean, dried shelled, except soybean, Acerola ...... 2.0 subgroup 6C ...... 0.5 Almond, hulls ...... 4.0 Pea and bean, succulent shelled, subgroup 6B ... 0.5 Animal feed, nongrass, group 18, forage ...... 45 Peanut ...... 0.2 Animal feed, nongrass, group 18, hay ...... 120 Peanut, hay ...... 15.0 Artichoke, globe ...... 4.0 Peanut, refined oil ...... 0.6 Asparagus ...... 0.04 Pear, Asian 1 ...... 0.07 Atemoya ...... 2.0 Pepper/eggplant subgroup 8–10B ...... 3.0 Avocado ...... 2.0 Peppermint, tops ...... 30 Banana ...... * Persimmon ...... 2.0 Barley, bran ...... 6.0 Pistachio ...... 0.50 Barley, forage ...... 25 Pulasan ...... 2.0 Barley, grain ...... 3.0 Quinoa, grain ...... 3.0 Barley, hay ...... 10.0 Rambutan ...... 2.0 Barley, straw ...... 15.0 Rapeseed subgroup 20A ...... 1.0 Beet, sugar, roots ...... 5.0 Rice, grain ...... 5.0 Berry, low growing, subgroup 13–07G, except Rice, hulls ...... 20 cranberry ...... 10.0 Rice, wild, grain ...... 5.0 Biriba ...... 2.0 Rye, forage ...... 7.0 Brassica, head and stem, subgroup 5A ...... 3.0 Rye, grain ...... 0.2

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Parts per Parts per Commodity million Commodity million

Rye, straw ...... 1.5 Hog, meat byproducts ...... 0.010 Sapodilla ...... 2.0 Horse, fat ...... 0.03 Sapote, black ...... 2.0 Horse, meat ...... 0.01 Sapote, mamey ...... 2.0 Horse, meat byproducts ...... 0.07 Sapote, white ...... 2.0 Milk...... 0.006 Sorghum, grain, forage ...... 25 Sheep, fat ...... 0.03 Sorghum, grain, grain ...... 11 Sheep, meat ...... 0.01 Sorghum, grain, stover ...... 40 Sheep, meat byproducts ...... 0.07 Soursop ...... 2.0 Soybean, hay ...... 55.0 (b) Section 18 emergency exemptions. Soybean, hulls ...... 1.0 Soybean, seed ...... 0.5 [Reserved] Spanish lime ...... 2.0 (c) Tolerances with regional registra- Spearmint, tops ...... 30 tion. [Reserved] Spice Subgroup 19B, except black pepper ...... 38 Star apple ...... 2.0 (d) Indirect or inadvertent residues. Starfruit ...... 2.0 [Reserved] Sugar apple ...... 2.0 Sugarcane, cane ...... 0.2 [62 FR 32235, June 13, 1997] Sunflower subgroup 20B ...... 0.5 EDITORIAL NOTE: For FEDERAL REGISTER ci- Tamarind ...... 2.0 Tea, dried 1 ...... 20.0 tations affecting § 180.507, see the List of CFR Ti, leaves ...... 50.0 Sections Affected, which appears in the Ti, roots ...... 0.5 Finding Aids section of the printed volume Tomato, paste ...... 0.6 and at www.govinfo.gov. Tomato subgroup 8–10A ...... 0.2 Turnip, greens ...... 25 § 180.509 Mefenpyr-diethyl; tolerance Vegetable, cucurbit, group 9 ...... 0.3 Vegetable, foliage of legume, group 7 ...... 30.0 for residues. Vegetable, leafy, except brassica, group 4 ...... 30.0 (a) General. Tolerances are estab- Vegetable, leaves of root and tuber, group 2 ...... 50.0 Vegetable, legume, edible podded, subgroup 6A, lished for residues of the safener, except soybean ...... 3.0 mefenpyr-diethyl, including its me- Vegetable, root, except sugar beet, subgroup 1B 1.0 tabolites and degradates, when applied Vegetable, tuberous and corm, subgroup 1C ...... 8.0 Wasabi, dry ...... 260 at a rate no greater than 0.053 pound Wasabi, fresh ...... 50 safener per acre per growing season in Watercress ...... 3.0 or on the commodities in the table Wax jambu ...... 2.0 below. Compliance with the tolerance Wheat, forage ...... 15.0 Wheat, grain ...... 0.2 levels specified below is to be deter- Wheat, hay ...... 30.0 mined by measuring only the sum of Wheat, straw ...... 10.0 mefenpyr-diethyl (1-(2,4- * 2.0 (of which not more than 0.1 is contained in the pulp) dichlorophenyl)-4,5-dihydro-5-methyl- 1 There are no United States registrations for use of azoxystrobin on coffee, green bean; ginseng; pear, Asian and 1H-pyrazole-3,5-dicarboxylic acid, tea, dried. diethyl ester) and its 2,4- (2) Tolerances are established for res- dichlorophenyl-pyrazoline metabolites, idues of the fungicide, azoxystrobin, in- calculated as the stoichiometric equiv- cluding its metabolites and degradates, alent of mefenpyr-diethyl, in or on the in or on the commodities in the fol- commodity. lowing table. Compliance with the tol- Parts per erance levels specified in the table is to Commodity million be determined by measuring only Barley, grain ...... 0.05 azoxystrobin, [methyl(E)-2-(2-(6-(2- Barley, hay ...... 0.2 cyanophenoxy) pyrimidin-4- Barley, straw ...... 0.5 yloxy)phenyl)-3-methoxyacrylate] in or Cattle, meat byproducts ...... 0.1 Goat, meat byproducts ...... 0.1 on the commodity. Grass, forage ...... 1.6 Grass, hay ...... 0.2 Commodity Parts per Hog, meat byproducts ...... 0.1 million Horse, meat byproducts ...... 0.1 Sheep, meat byproducts ...... 0.1 Cattle, fat ...... 0.03 Sorghum, grain, forage ...... 0.4 Cattle, meat ...... 0.01 Sorghum, grain, grain ...... 0.04 Cattle, meat byproducts ...... 0.07 Sorghum, grain, stover ...... 0.2 Goat, fat ...... 0.03 Wheat, forage ...... 0.2 Goat, meat ...... 0.01 Wheat, grain ...... 0.05 Goat, meat byproducts ...... 0.07 Wheat, hay ...... 0.2 Hog, fat ...... 0.010 Wheat, straw ...... 0.5 Hog, meat ...... 0.01

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(b) Section 18 emergency exemptions. Commodity Parts per [Reserved] million (c) Tolerances with regional registra- Biriba ...... 0.20 tions. [Reserved] Brassica, head and stem, subgroup 5A ...... 0.70 (d) Indirect or inadvertent residues. Brassica, leafy greens, subgroup 5B ...... 2.0 Bushberry subgroup 13–07B ...... 1.0 Tolerances are established for the indi- Cacao bean, dried ...... 0.02 rect or inadvertent residues of Caneberry subgroup 13–07A ...... 1.0 mefenpyr-diethyl, including its me- Canistel ...... 1.0 Canola, seed ...... 0.20 tabolites and degradates, when applied Cherimoya ...... 0.20 at a rate no greater than 0.053 pound Citrus, oil ...... 20 safener per acre per growing season in Citrus, dried pulp ...... 2.0 or on the commodities identified in the Coffee, instant ...... 0.10 Coffee, green bean ...... 0.02 table below. Compliance with the toler- Cotton, gin byproducts ...... 2.0 ance levels specified below is to be de- Cotton, undelinted seed ...... 0.05 termined by measuring only the sum of Custard apple ...... 0.20 Date ...... 0.30 mefenpyr-diethyl (1-(2,4- Feijoa ...... 0.10 dichlorophenyl)-4,5-dihydro-5-methyl- Fig ...... 0.30 1H-pyrazole-3,5-dicarboxylic acid, Fig, dried fruit ...... 1.0 Fruit, citrus, group 10–10 ...... 0.50 diethyl ester) and its 2,4- Fruit, pome, group 11–10 ...... 0.20 dichlorophenyl-pyrazoline metabolites, Fruit, small, vine climbing, except grape, sub- calculated as the stoichiometric equiv- group 13–07E ...... 0.35 alent of mefenpyr-diethyl, in or on the Fruit, stone, group 12 ...... 1.0 Grain, cereal, group 15 ...... 1.1 commodity. Grain, cereal, forage, fodder and straw, group 16 1.1 Grape ...... 2.5 Commodity Parts per Grass, forage, fodder, and hay, group 17, forage 0.70 million Grass, forage, fodder, and hay, group 17, hay ..... 1.1 Guava ...... 0.10 Canola, seed ...... 0.02 Herb subgroup 19A ...... 100 Soybean, forage ...... 0.1 Ilama ...... 0.20 Soybean, hay ...... 0.1 Jaboticaba ...... 0.10 Soybean, seed ...... 0.02 Lychee ...... 0.30 Mango ...... 1.0 [73 FR 74977, Dec. 10, 2008, as amended at 76 Nut, tree, group 14 ...... 0.02 FR 23903, Apr. 29, 2011] Olive ...... 1.0 Olive, oil ...... 2.0 Papaya ...... 1.0 § 180.510 Pyriproxyfen; tolerances for Passionfruit ...... 0.10 residues. Pawpaw ...... 1.0 Peanut ...... 0.20 (a) General. (1) Tolerances are estab- Pineapple ...... 0.30 lished for residues of pyriproxyfen, in- Pineapple, process residue ...... 1.1 cluding its metabolites and degradates, Pistachio ...... 0.02 in or on the commodities in the fol- Pomegranate ...... 0.20 Potato, chips ...... 0.75 lowing table. Compliance with the tol- Potato, granules/flakes ...... 0.75 erance levels specified is determined by Potato, wet peel ...... 0.75 measuring only pyriproxyfen, 2-[1- Pulasan ...... 0.30 Rambutan ...... 0.30 methyl-2-(4-phenoxyphenoxy) Rice, hulls ...... 5.5 ethoxy]pyridine, in or on the com- Safflower, seed ...... 0.20 modity. Sapodilla ...... 1.0 Sapote, black ...... 1.0 Parts per Sapote, mamey ...... 1.0 Commodity million Sapote, white ...... 0.30 Sesame, seed ...... 0.02 Acerola ...... 0.10 Soursop ...... 0.20 Almond, hulls ...... 2.0 Spanish lime ...... 0.30 Animal feed, nongrass, group 18, forage ...... 0.70 Star apple ...... 1.0 Animal feed, nongrass, group 18, hay ...... 1.1 Starfruit ...... 0.10 Animal feed, nongrass, group 18, seed ...... 2.0 Strawberry ...... 0.30 Apple, wet pomace ...... 0.8 Sugar apple ...... 0.20 Artichoke, globe ...... 2.0 Sugarcane ...... 1.1 Asparagus ...... 2.0 Tea ...... 15 Atemoya ...... 0.20 Vegetable, bulb, group 3–07 ...... 0.70 Avocado ...... 1.0 Vegetable, cucurbit, group 9 ...... 0.10 Banana ...... 0.20 Vegetable, foliage of legume, group 7 ...... 2.0 Beet, sugar, dried pulp ...... 3.0 Vegetable, fruiting, group 8–10 ...... 0.80 Berry, low growing, except strawberry, subgroup Vegetable, leafy, except Brassica, group 4 ...... 3.0 13–07H ...... 1.0 Vegetable, leaves of root and tuber, group 2 ...... 2.0

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mined by measuring only the Commodity Parts per million buprofezin, 2-[(1,1- Vegetable, legume, group 6 ...... 0.20 dimethylethyl)imino]tetrahydro-3(1- Vegetable, root and tuber, group 1 ...... 0.15 methylethyl)-5-phenyl-4H-1,3,5- Walnut ...... 0.02 thiadiazin-4-one, in the commodity. Watercress ...... 2.0 Wax jambu ...... 0.10 Parts per Commodity million (2) A tolerance of 0.10 parts per million is established for all food commod- Almond, hulls ...... 2.0 Apricot 3 ...... 9.0 ities as a result of the proposed use of Atemoya ...... 0.30 NYLAR in food handling establish- Avocado ...... 0.30 ments where food and food products are Banana ...... 0.20 Bean, snap, succulent ...... 0.02 held, prepared, processed or served. Ap- Bean, succulent ...... 0.02 plication is limited to space, general Berry, low growing, subgroup 13-07G ...... 2.5 surface, spot, and/or crack and crevice Birida ...... 0.30 treatment in food handling establish- Brassica, leafy greens, subgroup 4–16B ...... 60 Canistel ...... 0.90 ments where food and food products are Cattle, fat ...... 0.05 held, processed, prepared and served. Cattle, kidney ...... 0.05 Space and general surface application Cattle, liver ...... 0.05 Cattle, meat ...... 0.05 may be used only when the facility is Cattle, meat byproducts ...... 0.05 not in operation provided exposed food Celtuce ...... 35 is covered or removed from the area Cherimoya ...... 0.30 being treated prior to application. Citrus, dried pulp ...... 7.5 Citrus, oil ...... 80 Spot, and/or crack and crevice treat- Coffee, green bean ...... 0.35 ment may be used while the facility is Cotton, gin byproducts ...... 20.0 in operation provided exposed food is Cottonseed subgroup 20C ...... 0.35 Custard apple ...... 0.30 covered or removed from the area Feijoa ...... 0.30 being treated prior to application. Fennel, Florence, fresh leaves and stalk ...... 35 Food contact surfaces should be thor- Fig ...... 0.7 oughly washed with an effective clean- Fruit, citrus, group 10–10 ...... 4 Fruit, pome, group 11–10, except pear and pear, ing compound and rinced with potable Asian ...... 3.0 water after use of the product. To as- Fruit, small, vine climbing, except fuzzy kiwifruit, sure safe use of this additive, its label subgroup 13–07F ...... 1 Fruit, stone, group 12–12, except nectarine and and labeling shall conform to that reg- peach ...... 2 istered with the U.S. Environmental Goat, fat ...... 0.05 Protection Agency, and shall be used in Goat, kidney ...... 0.05 accordance with such label and label- Goat, liver ...... 0.05 Goat, meat ...... 0.05 ing. Goat, meat byproducts ...... 0.05 (b) Section 18 emergency exemptions. Grape 3 ...... 2.5 [Reserved] Grape, raisin ...... 2 (c) Tolerances with regional registra- Guava ...... 0.3 Hog, fat ...... 0.05 tions. [Reserved] Hog, kidney ...... 0.05 (d) Indirect or inadvertent residues. Hog, liver ...... 0.05 [Reserved] Hog, meat ...... 0.05 Hog, meat byproducts ...... 0.05 [64 FR 10233, Mar. 3, 1999] Horse, fat ...... 0.05 Horse, kidney ...... 0.05 EDITORIAL NOTE: For FEDERAL REGISTER ci- Horse, liver ...... 0.05 tations affecting § 180.510, see the List of CFR Horse, meat ...... 0.05 Sections Affected, which appears in the Horse, meat byproducts ...... 0.05 Finding Aids section of the printed volume Ilama ...... 0.30 and at www.govinfo.gov. Jaboticaba ...... 0.30 Kohlrabi ...... 12 Leaf petiole vegetable subgroup 22B ...... 35 § 180.511 Buprofezin; tolerances for Leafy greens subgroup 4–16A ...... 35 residues. Mango ...... 0.90 (a) General. Tolerances are estab- Milk ...... 0.01 Nut, tree, group 14–12 ...... 0.05 lished for residues of buprofezin, in- Papaya ...... 0.90 cluding its metabolites and degradates Passionfruit ...... 0.30 in or on the commodities in the table Peach ...... 9.0 Pear ...... 6.0 below. Compliance with the tolerance Pear, Asian ...... 6.0 levels specified below is to be deter- Persimmon ...... 1.9

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Parts per Parts per Commodity million Commodity million

Pomegranate ...... 1.9 Vegetable, fruiting, group 8–10 ...... 2 Pulasan ...... 0.30 1 Rambutan ...... 0.30 There are no U.S. registrations for Tea, dried as of Janu- ary 26, 2018. Rice, grain 1 ...... 1.5 Sapodilla ...... 0.90 (2) A tolerance of 0.01 parts per mil- Sapote, black ...... 0.90 lion is established for residues of Sapote, mamey ...... 0.90 Sheep, fat ...... 0.05 chlorfenapyr in or on all food commod- Sheep, kidney ...... 0.05 ities (other than those covered by a Sheep, liver ...... 0.05 higher tolerance as a result of use on Sheep, meat ...... 0.05 Sheep, meat byproducts ...... 0.05 growing crops) in food/feed handling Soursop ...... 0.30 areas where food/feed products are pre- Star apple ...... 0.90 pared, held, processed, or served and in Starfruit ...... 0.30 accordance with the following pre- Sugar apple ...... 0.30 Tea2 ...... 20 scribed conditions: Tropical and subtropical, small fruit, edible peel, (i) Application shall be no greater subgroup 23A ...... 5 than a 0.5% active ingredient solution Tropical and subtropical, small fruit, inedible peel, subgroup 24A ...... 0.3 for spot crack and crevice use in food/ Vegetable, Brassica, head and stem, group 5–16 12 feed handling establishments, where Vegetable, cucurbit, group 9 ...... 0.50 food and food products are held, proc- Vegetable, fruiting, group 8–10 ...... 2.0 essed, prepared and/or served. 1 There are no U.S. registrations as of July 10, 2017 for use (ii) Application may only be under- on rice. 2 There are no U.S. registrations at this time. taken when the facility is not in oper- 3 This tolerance expires on March 2, 2020. ation, and provided exposed food has (b) Section 18 emergency exemption. been covered, or removed from the area [Reserved] being treated prior to application. (c) Tolerances with regional registra- (iii) Food contact surfaces and equip- tions. [Reserved] ment should be throughly washed with (d) Indirect or inadvertent residues. an effective cleaning compound, and [Reserved] rinsed with potable water after each use of the product. [62 FR 40741, July 30, 1997] (iv) Contamination of food or food EDITORIAL NOTE: For FEDERAL REGISTER ci- contact surfaces shall be avoided. Ap- tations affecting § 180.511, see the List of CFR plication excludes any direct applica- Sections Affected, which appears in the tion to any food, food packaging, or Finding Aids section of the printed volume any food contact surfaces. and at www.govinfo.gov. (v) To assure safe use, the label and § 180.512 [Reserved] labeling shall conform to that registered by the U.S. Environmental Pro- § 180.513 Chlorfenapyr; tolerances for tection Agency, and it shall be used in residues. accordance with such label and label- (a) General. (1) Tolerances are estab- ing. lished for residues of chlorfenapyr, in- (b) Section 18 emergency exemptions. cluding its metabolites and degradates, [Reserved] in or on the commodities in the table (c) Tolerances with regional registra- below. Compliance with the tolerance tions. [Reserved] levels specified below is to be deter- (d) Indirect or inadvertent residues. mined by measuring only chlorfenapyr, [Reserved] 4-bromo-2-(4-chlorophenyl)-1- [68 FR 55527, Sept. 26, 2003, as amended at 70 (ethoxymethyl)-5-(trifluoromethyl)-1H- FR 3654, Jan. 26, 2005; 83 FR 3610, Jan. 26, pyrrole-3-carbonitrile, in or on the 2018; 85 FR 8472, Feb. 14, 2020] commodity. § 180.514 Cloransulam-methyl; toler- Parts per ances for residues. Commodity million (a) General. Tolerances are estab- Basil, fresh leaves ...... 80 lished for residues of the herbicide, Chive, fresh leaves ...... 20 Cucumber ...... 0.5 cloransulam-methyl, N-(2- Tea, dried 1 ...... 70 carboxymethyl-6-chlorophenyl)-5-

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ethoxy-7-fluoro-(1,2,4)-triazolo[1,5c]-py- Commodity Parts per rimidine-2-sulfonamide, plus its acid, million cloransulam, calculated as parent ester Cattle, meat ...... 0.10 in or on the following raw agricultural Cattle, meat byproducts ...... 0.10 commodities: Cherimoya ...... 0.10 Coffee, bean, green ...... 0.10 Parts per Cotton, gin byproducts ...... 10 Commodity million Cottonseed subgroup 20C ...... 0.20 Custard apple ...... 0.10 Soybean, forage ...... 0.1 Date, dried fruit ...... 0.10 Soybean, hay ...... 0.2 Feijoa ...... 0.10 Soybean, seed ...... 0.02 Fig ...... 0.10 Fish ...... 0.30 Fruit, citrus, group 10–10 ...... 0.10 (b) Section 18 emergency exemptions. Fruit, pome, group 11–10 ...... 0.10 [Reserved] Fruit, small vine climbing, subgroup 13–07F, ex- (c) Tolerances with regional registra- cept Fuzzy kiwifruit ...... 0.10 tions. [Reserved] Fruit, stone, group 12–12 ...... 0.10 Goat, fat ...... 0.10 (d) Indirect or inadvertent residues. Goat, meat ...... 0.10 [Reserved] Goat, meat byproducts ...... 0.10 Grain, aspirated grain fractions ...... 1.8 [62 FR 49163, Sept. 19, 1997] Grain, cereal, group 15 (except rice grain and sorghum grain) ...... 0.10 § 180.515 Carfentrazone-ethyl; toler- Grain, cereal, group 16, forage ...... 1.0 ances for residues. Grain, cereal, group 16, hay ...... 0.30 Grain, cereal, group 16, stover ...... 0.80 (a) General. Tolerances are estab- Grain, cereal, group 16, straw ...... 3.0 lished for residues of the herbicide Grass, forage ...... 5.0 carfentrazone-ethyl, including its me- Grass, hay ...... 8.0 Guava ...... 0.10 tabolites and degradates, in or on the Herbs and spices group 19 ...... 2.0 commodities listed in the following Hog, fat ...... 0.10 table. Compliance with the following Hog, meat ...... 0.10 Hog, meat byproducts ...... 0.10 tolerance levels is to be determined by Hop, dried cones ...... 0.10 measuring only the sum of Horse, fat ...... 0.10 carfentrazone-ethyl (ethyl-alpha-2- Horse, meat ...... 0.10 dichloro-5-[-4-(difluoromethyl)-4,5- Horse, meat byproducts ...... 0.10 Horseradish ...... 0.10 dihydro-3-methyl-5-oxo-1H -1,2,4- Ilama ...... 0.10 triazol-1-yl]-4- Jaboticaba ...... 0.10 fluorobenzenepropanoate) and its me- Kava, roots ...... 0.10 Kiwifruit ...... 0.10 tabolite carfentrazone-chloropropionic Longan ...... 0.10 acid (alpha, 2-dichloro-5-[-4- Lychee ...... 0.10 difluoromethyl)-4,5-dihydro-3-methyl-5- Mango ...... 0.10 oxo-1H-1,2,4-triazol-1-yl]-4- Milk ...... 0.05 Noni ...... 0.10 fluorobenzenepropanoic acid), cal- Nut, tree, group 14–12 ...... 0.10 culated as the stoichiometric equiva- Olive ...... 0.10 lent of carfentrazone-ethyl, in or on Palm heart ...... 0.10 Palm heart, leaves ...... 0.10 the following commodities: Papaya ...... 0.10 Passionfruit ...... 0.10 Parts per Pawpaw ...... 0.10 Commodity million Peanut ...... 0.10 Acerola ...... 0.10 Peanut, hay ...... 0.10 Almond, hulls ...... 0.20 Peppermint, tops ...... 0.10 Animal feed, nongrass, crop group 18, forage ..... 2.0 Persimmon ...... 0.10 Animal feed, nongrass, crop group 18, hay ...... 5.0 Pomegranate ...... 0.10 Animal feed, nongrass, crop group 18, seed ...... 15.0 Poultry, meat byproducts ...... 0.10 Artichoke, globe ...... 0.10 Psyllium, seed ...... 0.10 Asparagus ...... 0.10 Pulasan ...... 0.10 Atemoya ...... 0.10 Quinoa, grain ...... 0.10 Avocado ...... 0.10 Rambutan ...... 0.10 Banana ...... 0.10 Rapeseed, forage ...... 0.10 Berry, low growing, subgroup 13–07G ...... 0.10 Rapeseed subgroup 20A ...... 0.10 Birida ...... 0.10 Rice, grain ...... 1.3 Bushberry subgroup 13–07B ...... 0.10 Sapodilla ...... 0.10 Cacao bean, bean ...... 0.10 Sapote, black ...... 0.10 Cactus ...... 0.10 Sapote, mamey ...... 0.10 Caneberry subgroup 13–07A ...... 0.10 Sheep, fat ...... 0.10 Canistel ...... 0.10 Sheep, meat ...... 0.10 Cattle, fat ...... 0.10 Sheep, meat byproducts ...... 0.10

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Parts per Parts per Commodity million Commodity million

Shellfish ...... 0.30 Atemoya ...... 20 Sorghum, grain ...... 0.25 Avocado ...... 5.0 Soursop ...... 0.10 Bean, dry ...... 0.4 Soybean, seed ...... 0.10 Bean, succulent ...... 0.4 Spanish lime ...... 0.10 Beet, sugar, roots ...... 4.0 Spearmint, tops ...... 0.10 Berry, low growing, subgroup 13–07G, except Star apple ...... 0.10 cranberry ...... 3.0 Starfruit ...... 0.10 Biriba ...... 20 Stevia ...... 0.10 Brassica, head and stem, subgroup 5A ...... 2.0 Strawberrypear ...... 0.10 Brassica, leafy greens, subgroup 5B ...... 10 Sugar apple ...... 0.10 Bushberry subgroup 13–07B ...... 2.0 Sugarcane ...... 0.15 Caneberry subgroup 13–07A ...... 5.0 Sunflower, subgroup 20B ...... 0.10 Canistel ...... 5.0 Tea, dried ...... 0.10 Carrots ...... 7.0 Teff, forage ...... 1.0 Cherimoya ...... 20 Teff, grain ...... 0.25 Citrus, oil ...... 500 Teff, hay ...... 0.30 Cotton, gin byproducts ...... 0.05 Teff, straw ...... 3.0 Cotton, undelinted seed ...... 0.05 Ti, leaves ...... 0.10 Custard apple ...... 20 Ti, roots ...... 0.10 Dragon fruit ...... 1.0 Vanilla ...... 0.10 Feijoa ...... 5.0 Vegetable, brassica, leafy, group 5 ...... 0.10 Flax, seed ...... 0.05 Vegetable, bulb, group 3–07 ...... 0.10 Fruit, citrus, group 10–10 ...... 10 Vegetable, cucurbit, group 9 ...... 0.10 Fruit, pome, group 11–10 ...... 5.0 Vegetable, foliage of legume, except soybean, Fruit, small vine climbing, except fuzzy kiwifruit, subgroup 7A ...... 0.10 subgroup 13–07F ...... 2.0 Vegetable, fruiting, group 8–10 ...... 0.10 Fruit, stone, group 12–12 ...... 5.0 Vegetable, leafy, except brassica, group 4 ...... 0.10 Ginseng ...... 4.0 Vegetable, leaves of root and tuber, group 2 ...... 0.10 Grain, cereal, group 15 ...... 0.02 Vegetable, legume, group 6 ...... 0.10 Grain, cereal, forage, fodder, and straw, group 16 0.01 Vegetable, root and tuber, group 1 ...... 0.10 Grass, forage, fodder and hay, group 17 ...... 0.01 Wasaba, roots ...... 0.10 Guava ...... 5.0 Wax jambu ...... 0.10 Herb subgroup 19A, dried leaves ...... 65 1 Effective Date to be removed: May 18, 2016. Herb subgroup 19A, fresh leaves ...... 10 Ilama ...... 20 (b) Section 18 emergency exemptions. Jaboticaba ...... 5.0 [Reserved] Kiwifruit, fuzzy ...... 20 Leaf petioles subgroup 4B ...... 15 (c) Tolerances with regional registra- Leafy greens subgroup 4A ...... 30 tions. [Reserved] Longan ...... 20 (d) Indirect or inadvertent residues. Lychee ...... 20 [Reserved] Mango ...... 5.0 Melon subgroup 9A ...... 0.03 [63 FR 52180, Sept. 30, 1998] Onion, bulb, subgroup 3–07A ...... 0.50 Onion, green, subgroup 3–07B ...... 7.0 EDITORIAL NOTE: For FEDERAL REGISTER ci- Papaya ...... 5.0 tations affecting § 180.515, see the List of CFR Passionfruit ...... 5.0 Sections Affected, which appears in the Peanut ...... 0.01 Finding Aids section of the printed volume Peanut, hay ...... 0.01 and at www.govinfo.gov. Pineapple ...... 20 Pistachio ...... 0.10 Pomegranate ...... 5.0 § 180.516 Fludioxonil; tolerances for Pulasan ...... 20 residues. Rambutan ...... 20 Rapeseed, forage ...... 0.01 (a) General. (1) Tolerances are estab- Rapeseed subgroup 20A, except flax seed ...... 0.01 lished for residues of the fungicide Safflower, seed ...... 0.01 fludioxonil, including its metabolites Sapodilla ...... 5.0 and degradates, in or on the commod- Sapote, black ...... 5.0 Sapote, mamey ...... 5.0 ities in the following table. Compliance Soursop ...... 20 with the tolerance levels specified in Spanish lime ...... 20 the following table is to be determined Spice subgroup 19B ...... 0.02 Star apple ...... 5.0 by measuring only fludioxonil, 4-(2,2- Starfruit ...... 5.0 difluoro-1,3-benzodioxol-4-yl)-1-H- Sugar apple ...... 20 pyrrole-3-carbonitrile). Sunflower, seed ...... 0.01 Tomato ...... 5.0 Parts per Turnip, greens ...... 10 Commodity million Vegetable, cucurbit, group 9 ...... 0.45 Vegetable, foliage of legume, group 7 ...... 0.01 Acerola ...... 5.0 Vegetable, fruiting, group 8–10, except tomato .... 0.50 Animal feed, nongrass, group 18 ...... 0.01 Vegetable, leaves of root and tuber, group 2 ...... 30

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[(trifluoromethyl) sulfonyl]-1H-pyr- Commodity Parts per million azole-3-carbonitrile and 5-amino-1-[2,6- Vegetable, legume, group 6 ...... 0.01 dichloro-4-(trifluoromethyl) phenyl]-4- Vegetable, root, except sugar beet, subgroup 1B 0.75 [(trifluoromethyl)thio]-1H-pyrazole-3- Vegetable, tuberous and corm, subgroup 1C ...... 6.0 carbonitrile and its photodegradate 5- Watercress ...... 7.0 Wax jambu ...... 5.0 amino-1-(2,6-dichloro-4- Yam, true, tuber ...... 8.0 (trifluoromethyl)phenyl]-4-[(1R,S)- (trifluoromethyl)]-1H-pyrazole-3- (2) Tolerances are established for res- carbonitrile in or on the following idues of the fungicide fludioxonil, in- items at the levels specified: cluding its metabolites and degradates, Parts per in or on the commodities in the fol- Commodity million lowing table. Compliance with the tolerance levels specified in the following Cattle, fat ...... 0.40 Cattle, liver ...... 0.10 table is to be determined by measuring Cattle, meat ...... 0.04 only the sum of fludioxonil, 4-(2,2- Cattle, meat byproducts, except liver ...... 0.04 difluoro-1,3-benzodioxol-4-yl)-1-H- Corn, field, grain ...... 0.02 Corn, field, stover ...... 0.30 pyrrole-3-carbonitrile), and its metabo- Corn, field, forage ...... 0.15 lites converted to 2,2-difluoro-l,3- Egg ...... 0.03 benzodioxole-4-carboxylic acid, cal- Goat, fat ...... 0.40 Goat, liver ...... 0.10 culated as the stoichiometric equiva- Goat, meat ...... 0.04 lent of fludioxonil. Goat, meat byproducts, except liver ...... 0.04 Hog, fat ...... 0.04 Hog, liver ...... 0.02 Commodity Parts per million Hog, meat ...... 0.01 Hog, meat byproducts, except liver ...... 0.01 Cattle, fat ...... 0.05 Horse, fat ...... 0.40 Cattle, meat ...... 0.01 Horse, liver ...... 0.10 Cattle, meat byproducts ...... 0.05 Horse, meat ...... 0.04 Goat, fat ...... 0.05 Horse, meat byproducts, except liver ...... 0.04 Goat, meat ...... 0.01 Milk, fat (reflecting 0.05 ppm in whole milk) ...... 1.50 Goat, meat byproducts ...... 0.05 Potato ...... 0.03 Horse, fat ...... 0.05 Potato, wet peel ...... 0.10 Horse, meat ...... 0.01 Poultry, fat ...... 0.05 Horse, meat byproducts ...... 0.05 Poultry, meat ...... 0.02 Milk ...... 0.01 Poultry, meat byproducts ...... 0.02 Sheep, fat ...... 0.05 Rice, grain ...... 0.04 Sheep, meat ...... 0.01 Sheep, fat ...... 0.40 Sheep, meat byproducts ...... 0.05 Sheep, liver ...... 0.10 Sheep, meat ...... 0.04 (b) Section 18 emergency exemptions. Sheep, meat byproducts, except liver ...... 0.04 [Reserved] (b) Section 18 emergency exemptions.. (c) Tolerances with regional registra- Time-limited tolerances are estab- tions. [Reserved] lished for combined residues of the in- (d) Indirect or inadvertent residues. secticide, fipronil, 5-amino-1-(2,6- [Reserved] dichloro-4-(trifluoromethyl) phenyl)-4- [62 FR 56082, Oct. 29, 1997] ((1,R,S)-trifluoromethyl)sulfinyl)-1-H- EDITORIAL NOTE: For FEDERAL REGISTER ci- pyrazole-3-carbonitrile and its 2 me- tations affecting § 180.516, see the List of CFR tabolites MB45950 (5-amino-1-(2,6- Sections Affected, which appears in the dichloro-4-(trifluoromethyl)phenyl)-4- Finding Aids section of the printed volume [(trifluoromethyl)thio]-1H-pyrazole-3- and at www.govinfo.gov. carbonitrile) and MB46136 (5-amino-1- (2,6-dichloro-4- § 180.517 Fipronil; tolerances for resi- (trifluoromethyl)phenyl)-4- dues. [(trifluoromethyl)sulfonyl]-1H-pyr- (a) General. Therefore, tolerances are azole-3-carbonitrile) and its established for combined residues of photodegradate MB46513 (5-amino-1- the insecticide fipronil (5-amino-1-[2,6- (2,6-dichloro-4- dichloro-4-(trifluoromethyl)phenyl]-4- (trifluoromethyl)phenyl]-4-[(1R,S)- [(1R,S)-(trifluoromethyl)sulfinyl]-1H- (trifluoromethyl)]-1H-pyrazole-3- pyrazole-3-carbonitrile) and its me- carbonitrile), in connection with use of tabolites 5-amino-1-[2,6-dichloro-4- the pesticide under Section 18 emer- (trifluoromethyl)phenyl]-4- gency exemptions granted by EPA. The

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tolerances expire and are revoked on Commodity Parts per the dates specified in the table for this million paragraph. Grape, raisin ...... 8.0 Onion, bulb, subgroup 3–07A ...... 0.2 Expiration/ Onion, green, subgroup 3–07B ...... 3.0 Commodity Parts per revocation million date Pistachio ...... 0.20 Pomegranate ...... 5.0 Rutabaga ...... 1.0 12/31/16 Tomato subgroup 8–10A ...... 0.50 Turnip ...... 1.0 12/31/16 Vegetable, tuberous and corm, subgroup 1C ...... 0.05

(c) Tolerances with regional registra- (2) Tolerances are established for res- tions. [Reserved] idues of the fungicide pyrimethanil, in- (d) Indirect or inadvertent residues. cluding its metabolites and degradates, Tolerances are established for com- in or on the commodities in the fol- bined indirect or inadvertent residues lowing table. Compliance with the tol- of the insecticide fipronil and its me- erance levels specified in the following tabolites and photodegradate in or on table is to be determined by measuring food commodities when present therein only the sum of pyrimethanil and its as a result of the application of fipronil metabolite 4-[4,6-dimethyl-2- to growing crops listed in paragraphs pyrimidinyl)amino]phenol, calculated (a) and (b) of this section and other as the stoichiometric equivalent of nonfood crops to read as follows: pyrimethanil.

Commodity Parts per Parts per million Commodity million

Wheat, forage ...... 0.02 Cattle, fat ...... 0.01 Wheat, grain ...... 0.005 Cattle, kidney ...... 2.5 Wheat, hay ...... 0.03 Cattle, meat ...... 0.01 Wheat, straw ...... 0.03 Cattle, meat byproducts, except kidney ...... 0.01 Goat, fat ...... 0.01 [62 FR 62979, Nov. 26, 1997, as amended at 63 Goat, kidney ...... 2.5 FR 38495, July 17, 1998; 72 FR 46913, Aug. 22, Goat, meat ...... 0.01 2007; 74 FR 46377, Sept. 9, 2009; 75 FR 80346, Goat, meat byproducts, except kidney ...... 0.01 Dec. 22, 2010; 78 FR 78748, Dec. 27, 2013; 80 FR Horse, fat ...... 0.01 72599, Nov. 20, 2015] Horse, kidney ...... 2.5 Horse, meat ...... 0.01 Horse, meat byproducts, except kidney ...... 0.01 § 180.518 Pyrimethanil; tolerances for Sheep, fat ...... 0.01 residues. Sheep, kidney ...... 2.5 (a) General. (1) Tolerances are estab- Sheep, meat ...... 0.01 lished for residues of the fungicide Sheep, meat byproducts, except kidney ...... 0.01 pyrimethanil, including its metabolites (3) Tolerances are established for res- and degradates, in or on the commod- idues of the fungicide pyrimethanil, in- ities in the following table Compliance cluding its metabolites and degradates, with the tolerance levels specified in in or on the commodities in the fol- the following table is to be determined lowing table. Compliance with the tol- by measuring only pyrimethanil (4,6-di- erance levels specified in the following methyl-N-phenyl-2-pyrimidinamine). table is to be determined by measuring only the sum of pyrimethanil and its Commodity Parts per million metabolite 4,6-dimethyl-2- Almond ...... 0.20 (phenylamino)-5-pyrimidinol, cal- Almond, hulls ...... 12 culated as the stoichiometric equiva- Apple, wet pomace ...... 40 lent of pyrimethanil. Banana ...... 0.10 Berry, low growing, subgroup 13–07G ...... 3.0 Parts per Bushberry subgroup 13–07B ...... 8.0 Commodity million Caneberry subgroup 13–07A ...... 15 Citrus, oil ...... 150 Milk ...... 0.05 Cucumber ...... 1.5 Fruit, citrus, group 10–10 ...... 10 Fruit, pome, group 11–10 ...... 15 (b) Section 18 emergency exemptions. Fruit, small, vine climbing, subgroup 13–07F, ex- [Reserved] cept fuzzy kiwifruit ...... 5.0 Fruit, stone, group 12–12 ...... 10 (c) Tolerances with regional registra- Ginseng ...... 1.5 tions. [Reserved]

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(d) Indirect or inadvertent residues. istered by the U.S. Environmental Pro- [Reserved] tection Agency. (3) Residues of inorganic bromides [62 FR 63669, Dec. 2, 1997, as amended at 69 FR 52443, Aug. 26, 2004; 73 FR 64251, Oct. 29, (calculated as Br) in milled fractions 2008; 74 FR 32448, July 8, 2009; 77 FR 45503, derived from cereal grain from all fu- Aug. 1, 2012; 80 FR 7975, Feb. 13, 2015; 80 FR migation sources, including fumigation 63691, Oct. 21, 2015] of grain-mill machinery, shall not exceed 125 parts per million. § 180.519 Bromide ion and residual (b) Section 18 emergency exemptions. bromine; tolerances for residues. [Reserved] (a) General. The food additives, bro- (c) Tolerances with regional registra- mide ion and residual bromine, may be tions. [Reserved] present in water, potable in accordance (d) Indirect or inadvertent residues. with the following conditions: [Reserved] (1) The food additives are present as a result of treating water aboard ships [40 FR 14156, Mar. 28, 1975. Redesignated at 41 with a polybrominated ion-exchange FR 26568, June 28, 1976, as amended at 49 FR 44459, Nov. 7, 1984. Further redesignated at 53 resin (as a source of bromine) under the FR 24667, June 29, 1988, as amended at 54 FR supervision of trained personnel. 6130, Feb. 8, 1989. Further redesignated and (2) Residual bromine levels are con- amended at 63 FR 34319, June 24, 1998] trolled to not exceed 1.0 part per million (ppm) in the final treated water. § 180.522 Fumigants for processed Control is effected using calibrated re- grains used in production of fer- circulating or proportioning bromine mented malt beverage; tolerances feeder equipment and periodic checks for residues. of residual bromine using a bromine (a) General. Fumigants for processed test kit. To assure safe use of the addi- grain may be safely used, in accordance tives, the label and labeling of the dis- with the following conditions. infectant formulation containing the (1) Methyl bromide. Total residues of food additives shall conform to the inorganic bromides (calculated as Br) label and labeling registered by the from the use of this fumigant shall not U.S. Environmental Protection Agen- exceed 125 parts per milion. cy. (2) Methyl bromide is used to fumi- (3) No tolerance is established for gate corn grits and cracked rice in the bromide ion levels. production of fermented malt beverage. (b) Section 18 emergency exemptions. (3) To assure safe use of the fumi- [Reserved] gant, its label and labeling shall con- (c) Tolerances with regional registra- form to the label and labeling reg- tions. [Reserved] istered by the U.S. Environmental Pro- (d) Indirect or inadvertent residues. tection Agency, and the usage em- [Reserved] ployed should conform with such label or labeling. [41 FR 17893, Apr. 29, 1976. Redesignated at 41 FR 26568, June 28, 1976, and at 53 FR 24667, (4) The total residue of inorganic bro- June 29, 1988. Redesignated and amended at mides in fermented malt beverage, re- 63 FR 34319, June 24, 1998; 71 FR 74818, Dec. sulting from the use of corn grits and 13, 2006] cracked rice fumigated with the fumigant described in paragraph (a)(2) of § 180.521 Fumigants for grain-mill ma- this section plus additional residues of chinery; tolerances for residues. inorganic bromides that may be (a) General. Fumigants may be safely present from uses in accordance with used in or on grain-mill machinery in other regulations in this chapter pro- accordance with the following pre- mulgated under section 408 and/or 409 scribed conditions: of the Act, does not exceed 25 parts per (1) The fumigants consist of methyl million bromide (calculated as Br). bromide. (b) Section 18 emergency exemptions. (2) To assure safe use of the fumi- [Reserved] gant, its label and labeling shall con- (c) Tolerances with regional registra- form to the label and labeling reg- tions. [Reserved]

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(d) Indirect or inadvertent residues. Commodity Parts per [Reserved] million [71 FR 74818, Dec. 13, 2006] Beet, garden, leaves ...... 0.08 Beet, garden, roots ...... 0.05 Clover, forage ...... 0.60 § 180.523 Metaldehyde; tolerances for Clover, hay ...... 0.60 residues. Hop, dried cones ...... 0.10 Rutabaga, roots ...... 0.05 (a) General. Tolerances are estab- Soybean, seed ...... 0.05 lished for residues of the molluscicide Turnip greens ...... 0.08 metaldehyde, including its metabolites Turnip, roots ...... 0.05 and degradates, in or on the commod- Wheat, forage ...... 0.05 Wheat, grain ...... 0.05 ities listed in the following table. Com- Wheat, hay ...... 0.05 pliance with the specified tolerance Wheat, straw ...... 0.05 levels is to be determined by measuring only metaldehyde, 2,4,6,8- (d) Indirect or inadvertent residues. tetramethyl-1,3,5,7-tetroxocane, in or [Reserved] on the commodity. [73 FR 54963, Sept. 24, 2008, as amended at 78 FR 70869, Nov. 27, 2013; 80 FR 11588, Mar. 4, Parts per Commodity million 2015; 81 FR 71638, Oct. 18, 2016]

Artichoke, globe ...... 0.07 § 180.525 Resmethrin; tolerances for Berry, low growing, subgroup 13–07G ...... 6.25 residues. Bushberry subgroup 13–07B ...... 0.15 Cactus ...... 0.07 (a) General. Tolerances are estab- Caneberry subgroup 13–07A ...... 0.15 lished for residues of the insecticide Corn, field, forage ...... 0.30 resmethrin [5-(phenylmethyl)-3- Corn, field, grain ...... 0.05 furanyl] methyl 2,2-dimethyl-3-(2- Corn, field, stover ...... 0.10 Corn, sweet, forage ...... 0.30 methyl-1-propenyl) Corn, sweet, kernel plus cob with husks removed 0.05 cyclopropanecarboxylate in or on food Corn, sweet, stover ...... 0.10 commodities at 3.0 ppm resulting from Fruit, citrus, group 10–10 ...... 0.26 use of the insecticide in food handling Ginseng ...... 0.05 and storage areas as a space concentra- Grass, forage ...... 2.0 Grass, hay ...... 2.0 tion for spot/or crack and crevice treat- Leaf petioles subgroup 4B ...... 0.50 ment and shall be limited to a max- Lettuce ...... 1.73 imum of 3.00 percent of the active in- Pea and bean, succulent shelled, subgroup 6B ... 0.20 gredient by weight, and as a space Peppermint, oil ...... 12 Peppermint, tops ...... 4.0 treatment shall be limited to a max- Spearmint, oil ...... 12 imum of 0.5 fluid ounce of 3.0 percent Spearmint, tops ...... 4.0 active ingredient by weight per 1000 Taro, corm ...... 0.15 cubic feet of space provided that the Taro, leaves ...... 1.0 Tomato subgroup 8–10A ...... 0.24 food is removed or covered prior to Vegetable, brassica, leafy, group 5 ...... 2.5 such use. To assure safe use of the ad- Vegetable, foliage of legume, except soybean, ditive, its label and labeling shall con- subgroup 7A ...... 1.5 form to that registered with the U.S. Vegetable, legume, edible podded subgroup 6A .. 0.80 Environmental Protection Agency, and Watercress ...... 3.2 shall be used in accordance with such (b) Section 18 emergency exemptions. label and labeling. [Reserved] (b) Section 18 emergency exemptions. (c) Tolerances with regional registra- [Reserved] tions. Tolerances with a regional reg- (c) Tolerances with regional registra- istration as defined in § 180.1(l) are es- tions. [Reserved] tablished for residues of the (d) Indirect or inadvertent residues. molluscicide metaldehyde, including [Reserved] its metabolites and degradates, in or [71 FR 74819, Dec. 13, 2006] on the following commodities. Compli- ance with the specified tolerance level § 180.526 Synthetic isoparaffinic petro- is to be determined by measuring only leum hydrocarbons; tolerances for metaldehyde, 2,4,6,8-tetramethyl- residues. 1,3,5,7-tetroxocane, in or on the com- (a) General. Synthetic isoparaffinic modity. petroleum hydrocarbons complying

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with 21 CFR 172.882 (a) and (b) may be (c) Tolerances with regional registra- safely used as a component of insecti- tions. Tolerances are established for cide formulations for use on animal combined residues of flufenacet, N-(4- feed in an amount no greater than rea- fluorophenyl)-N-(1-methylethyl)-2-[[5- sonably required to accomplish its in- (trifluoromethyl)-1, 3, 4-thiadiazol-2-yl] tended effect as an adjuvant in the in- oxy]acetamide, and its metabolites secticide formulation and shall not be containing the 4-fluoro-N-methylethyl intended to accomplish any effect in benzenamine moiety, with regional animal feed. It is used or intended for registration. use as a component of insecticide formulations used in compliance with reg- Commodity Parts per ulations issued in 40 CFR part 180 and million in this part. Grass, forage ...... 7.0 (b) Section 18 emergency exemptions. Grass, hay ...... 0.4 [Reserved] (c) Tolerances with regional registra- (d) Indirect or inadvertent residues. tions. [Reserved] Tolerances are established for indirect (d) Indirect or inadvertent residues. or inadvertent residues of the herbicide [Reserved] flufenacet, N-(4-fluorophenyl)-N-(1- [40 FR 14161, Mar. 28, 1975, as amended at 50 methylethyl)-2-[[5-(trifluoromethyl)- FR 2959, Jan. 23, 1985, and amended at 53 FR 1,3,4-thiadiazol-2-yl]oxy]acetamide and 24668, 24669, June 29, 1988. Redesignated and its metabolites containing the 4-fluoro- amended at 63 FR 34319, June 24, 1998] N-methylethyl benzenamine moiety in or on the following raw agricultural § 180.527 Flufenacet, N-(4- fluorophenyl)-N-(1-methylethyl)-2- commodities when present therein as a [[5-(trifluoromethyl)-1, 3, 4- result of application of flufenacet to thiadiazol-2-yl] oxy]acetamide and the growing crops in paragraph (a) of its metabolites containing the 4- this section. fluoro-N-methylethyl benzenamine tolerances for residues. Parts per Commodity million (a) General. Tolerances are established for the combined residues of the Alfalfa, forage ...... 0.1 herbicide flufenacet, N-(4- Alfalfa, hay ...... 0.1 fluorophenyl)-N-(1-methylethyl)-2-[[5- Alfalfa, seed ...... 0.1 (trifluoromethyl)-1, 3, 4-thiadiazol-2-yl] Clover, forage ...... 0.1 Clover, hay ...... 0.1 oxy]acetamide and its metabolites con- Grain, cereal, group 15, except rice ...... 0.1 taining the 4-fluoro-N-methylethyl Grain, cereal, forage, fodder, and straw, group benzenamine moiety in or on the fol- 16, except rice ...... 0.1 lowing commodities. Grass, forage, fodder, and hay, group 17 ...... 0.1

Parts per Commodity million [63 FR 26473, May 13, 1998, as amended at 63 FR 50791, Sept. 23, 1998; 64 FR 42846, Aug. 6, Cattle, kidney ...... 0.05 1999; 65 FR 64366, Oct. 27, 2000; 68 FR 2247, Corn, field, forage ...... 0.4 Jan. 16, 2003; 68 FR 37759, June 25, 2003; 70 FR Corn, field, grain ...... 0.05 Corn, field, stover ...... 0.4 37696, June 30, 2005; 71 FR 76200, Dec. 20, 2006; Corn, sweet, forage ...... 0.45 72 FR 26310, May 9, 2007] Corn, sweet, kernel plus cob with husks removed 0.05 Corn, sweet, stover ...... 0.30 § 180.532 Cyprodinil; tolerances for Goat, kidney ...... 0.05 residues. Hog, kidney ...... 0.05 Horse, kidney ...... 0.05 (a) General. (1) Tolerances are estab- Sheep, kidney ...... 0.05 lished for residues of the fungicide Soybean, seed ...... 0.1 Wheat, bran ...... 0.80 cyprodinil, including its metabolites Wheat, forage ...... 6.0 and degradates, in or on the commod- Wheat, grain ...... 0.60 ities in the table below. Compliance Wheat, hay ...... 1.2 Wheat, straw ...... 0.35 with the tolerance levels specified below is to be determined by measuring (b) Section 18 emergency exemptions. only cyprodinil 4-cyclopropyl-6-meth- [Reserved] yl-N-phenyl-2-pyrimidinamine.

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measuring only the sum of cyprodinil Commodity Parts per million 4-cyclopropyl-6-methyl-N-phenyl-2- Acerola ...... 1.5 pyrimidinamine and free and con- Almond ...... 0.02 jugated CGA–304075 4-(4-cyclopropyl-6- Almond, hulls ...... 8.0 methyl-pyrimidin-2-ylamino)-phenol, Apple, wet pomace ...... 4.6 Artichoke, globe ...... 4.0 calculated as the stoichiometric equiv- Avocado ...... 1.2 alent of cyprodinil. Bean, dry ...... 0.6 Bean, succulent ...... 0.6 Commodity Parts per Berry, low growing, subgroup 13–07G, except million cranberry ...... 5.0 Brassica, head and stem, subgroup 5A ...... 1.0 Cattle, meat byproducts ...... 0.02 Brassica, leafy greens, subgroup 5B ...... 10.0 Goat, meat byproducts ...... 0.02 Bushberry subgroup 13–07B ...... 3.0 Horse, meat byproducts ...... 0.02 Caneberry subgroup 13–07A ...... 10 Sheep, meat byproducts ...... 0.02 Canistel ...... 1.2 Canola, seed 1 ...... 0.03 (b) Section 18 emergency exemptions. Citrus, dried pulp ...... 8.0 Citrus, oil ...... 60 [Reserved] Dragon fruit ...... 2.0 (c) Tolerances with regional registra- Feijoa ...... 1.5 tions. [Reserved] Fruit, pome, group 11–10 ...... 1.7 (d) Indirect or inadvertent residues. Fruit, small vine climbing, except fuzzy kiwifruit, subgroup 13–07F ...... 3.0 [Reserved] Fruit, stone, group 12–12 ...... 2.0 Grape, raisin ...... 5.0 [63 FR 17706, Apr. 10, 1998] Guava ...... 1.5 EDITORIAL NOTE: For FEDERAL REGISTER ci- Herb subgroup 19A, dried, except parsley ...... 15.0 tations affecting § 180.532, see the List of CFR Herb subgroup 19A, fresh, except parsley ...... 3.0 Jaboticaba ...... 1.5 Sections Affected, which appears in the Kiwifruit ...... 1.8 Finding Aids section of the printed volume Leaf petioles subgroup 4B ...... 30 and at www.govinfo.gov. Leafy greens subgroup 4A ...... 50 Lemon ...... 0.60 § 180.533 Esfenvalerate; tolerances for Lime ...... 0.60 residues. Longan ...... 2.0 Lychee ...... 2.0 (a) General. (1) Tolerances are estab- Mango ...... 1.2 lished for the combined residues of the Nut, tree, group 14–12; except almond and pistachio ...... 0.04 insecticide esfenvalerate, (S)-cyano(3- Onion, bulb, subgroup 3–07A ...... 0.6 phenoxyphenyl)methyl-(S)-4-chloro-a- Onion, green, subgroup 3–07B ...... 4.0 (1-methylethyl)benzeneacetate, its Papaya ...... 1.2 Parsley, dried leaves ...... 170 non-racemic isomer, (R)-cyano(3- Parsley, leaves ...... 35 phenoxyphenyl)methyl-(R)-4-chloro-a- Passionfruit ...... 1.5 (1-methylethyl)benzeneacetate and its Pistachio ...... 0.10 diastereomers (S)-cyano(3- Pomegranate ...... 10 Potato, wet peel ...... 0.03 phenoxyphenyl)methyl-(R)-4-chloro-a- Pulasan ...... 2.0 (1-methylethyl)benzeneacetate and (R)- Rambutan ...... 2.0 cyano(3-phenoxyphenyl)methyl-(S)-4- Sapodilla ...... 1.2 Sapote, black ...... 1.2 chloro-a-(1- Sapote, mamey ...... 1.2 methylethyl)benzeneacetate, in or on Spanish lime ...... 2.0 food commodities as follows: Star apple ...... 1.2 Starfruit ...... 1.5 Parts per Turnip, greens ...... 10.0 Commodity million Vegetable, cucurbit, group 9 ...... 0.70 Vegetable, fruiting, group 8–10 ...... 1.5 Almond ...... 0.2 Vegetable, leaves of root and tuber, group 2 ...... 10 Almond, hulls ...... 5.0 Vegetable, root, except sugarbeet, subgroup 1B 0.75 Apple ...... 1.0 Vegetable, tuberous and corm, subgroup 1C ...... 0.01 Artichoke, globe ...... 1.0 Watercress ...... 20 Bean, dry, seed ...... 0.25 Wax jambu ...... 1.5 Bean, snap, succulent ...... 1.0 Beet, sugar, roots ...... 0.05 1 Import only. Beet, sugar, tops ...... 5.0 (2) Tolerances are established for res- Blueberry ...... 1.0 Broccoli ...... 1.0 idues of the fungicide cyprodinil, in- Cabbage, except Chinese cabbage ...... 3.0 cluding its metabolites and degradates, Caneberry subgroup 13A ...... 1.0 in the commodities in the table below. Cantaloupe ...... 0.5 Carrot, roots ...... 0.5 Compliance with the tolerance levels Cattle, fat ...... 1.5 specified below is to be determined by Cattle, meat ...... 1.5

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covered by a higher tolerance as a re- Commodity Parts per million sult of use on growing crops) is estab- Cattle, meat byproducts ...... 1.5 lished for the combined residues of the Cauliflower ...... 0.5 insecticide esfenvalerate, (S)-cyano(3- Collards ...... 3.0 phenoxyphenyl)methyl-(S)-4-chloro-a- Corn, field, forage ...... 15.0 Corn, field, grain ...... 0.02 (1-methylethyl)benzeneacetate, its Corn, field, stover ...... 15.0 non-racemic isomer, (R)-cyano(3- Corn, pop, grain ...... 0.02 phenoxyphenyl)methyl-(R)-4-chloro-a- Corn, pop, stover ...... 15.0 (1-methylethyl)benzeneacetate and its Corn, sweet, forage ...... 15.0 Corn, sweet, kernel plus cob with husks removed 0.1 diastereomers (S)-cyano(3- Corn, sweet, stover ...... 15.0 phenoxyphenyl)methyl-(R)-4-chloro-a- Cotton, undelinted seed ...... 0.2 (1-methylethyl)benzeneacetate and (R)- Cucumber ...... 0.5 Egg ...... 0.03 cyano(3-phenoxyphenyl)methyl-(S)-4- Eggplant ...... 0.5 chloro-a-(1- Elderberry ...... 1.0 methylethyl)benzeneacetate as a result Fruit, stone, group 12 ...... 3.0 of the use of esfenvalerate in food-han- Goat, fat ...... 1.5 Goat, meat ...... 1.5 dling establishments. Goat, meat byproducts ...... 1.5 (b) Section 18 emergency exemptions. Gooseberry ...... 1.0 [Reserved] Hazelnut ...... 0.2 Hog, fat ...... 1.5 (c) Tolerances with regional registra- Hog, meat ...... 1.5 tions. Tolerances with regional reg- Hog, meat byproducts ...... 1.5 istration are established for the com- Horse, fat ...... 1.5 bined residues of the insecticide Horse, meat ...... 1.5 Horse, meat byproducts ...... 1.5 esfenvalerate, (S)-cyano(3- Kiwifruit ...... 0.5 phenoxyphenyl)methyl-(S)-4-chloro-a- Lentil, seed ...... 0.25 (1-methylethyl)benzeneacetate, its Melon, honeydew ...... 0.5 Milk ...... 0.3 non-racemic isomer, (R)-cyano(3- Milk, fat ...... 7.0 phenoxyphenyl)methyl-(R)-4-chloro-a- Muskmelon ...... 0.5 (1-methylethyl)benzeneacetate and its Mustard greens ...... 5.0 diastereomers (S)-cyano(3- Okra ...... 0.5 Pea, dry, seed ...... 0.25 phenoxyphenyl)methyl-(R)-4-chloro-a- Pea, succulent ...... 0.5 (1-methylethyl)benzeneacetate and (R)- Peanut ...... 0.02 cyano(3-phenoxyphenyl)methyl-(S)-4- Pear ...... 1.0 Pecan ...... 0.2 chloro-a-(1- Pepper ...... 0.5 methylethyl)benzeneacetate, in or on Potato ...... 0.02 food commodities as follows: Poultry, fat ...... 0.3 Poultry, liver ...... 0.03 Parts per Poultry, meat ...... 0.03 Commodity million Poultry, meat byproducts, except liver ...... 0.3 Pumpkin ...... 0.5 Cabbage, chinese, bok choy ...... 1.0 Radish, roots ...... 0.3 Kohlrabi ...... 2.0 Radish, tops ...... 3.0 Lettuce, head ...... 5.0 Sheep, fat ...... 1.5 Sheep, meat ...... 1.5 (d) Indirect or inadvertent residues. Sheep, meat byproducts ...... 1.5 [Reserved] Sorghum, grain, forage ...... 10.0 Sorghum, grain, grain ...... 5.0 [63 FR 23401, Apr. 29, 1998, as amended at 63 Sorghum, grain, stover ...... 10.0 FR 48615, Sept. 11, 1998; 74 FR 46699, Sept. 11, Soybean, hulls ...... 0.5 Soybean, seed ...... 0.05 2009] Squash, summer ...... 0.5 Squash, winter ...... 0.5 § 180.535 Fluroxypyr 1-methylheptyl Sugarcane, cane ...... 1.0 ester; tolerances for residues. Sunflower, seed ...... 0.5 Sweet potato, roots ...... 0.05 (a) General. Tolerances are estab- Tomato ...... 0.5 lished for combined residues of Turnip, greens ...... 7.0 fluroxypyr 1-methylheptyl ester [1- Turnip, roots ...... 0.5 Walnut ...... 0.2 methylheptyl ((4-amino-3,5-dichloro-6- Watermelon ...... 0.5 fluoro-2-pyridinyl)oxy)acetate] and its metabolite fluroxypyr [((4-amino-3,5- (2) A tolerance of 0.05 ppm on raw ag- dichloro-6-fluoro-2-pyridinyl)oxy)acetic ricultural food commodities (other acid] in or on the following raw agri- than those food commodities already cultural commodities. Compliance with

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the established tolerance levels is de- (b) Section 18 emergency exemptions. termined by measuring only the sum of [Reserved] fluroxypyr 1-methylheptyl ester [1- (c) Tolerances with regional registra- methylheptyl ((4-amino-3, 5-dichloro-6- tions. [Reserved] fluoro-2-pyridinyl)oxy)acetate] and its (d) Indirect or inadvertent residues. metabolite fluroxypyr [((4-amino-3,5- [Reserved] dichloro-6-fluoro-2-pyridinyl)oxy)acetic [63 FR 52169, Sept. 30, 1998, as amended at 64 acid] calculated as the stoichiometric FR 22799, Apr. 28, 1999; 66 FR 37598, July 19, equivalent of fluroxypyr. 2001; 66 FR 47971, Sept. 17, 2001; 67 FR 46884, July 17, 2002; 67 FR 60146, Sept. 25, 2002; 68 FR Parts per 75438, Dec. 31, 2003; 69 FR 2074, Jan. 14, 2004; Commodity million 70 FR 3649, Jan. 26, 2005; 70 FR 7047, Feb. 10, Barley, grain ...... 0.5 2005; 71 FR 76204, Dec. 20, 2006; 72 FR 73635, Barley, hay ...... 12.0 Dec. 28, 2007; 78 FR 3333, Jan. 16, 2013; 83 FR Barley, hay ...... 20.0 29706, June 26, 2018] Barley, straw ...... 12.0 Cattle, fat ...... 0.1 § 180.537 Isoxaflutole; tolerances for Cattle, kidney ...... 1.5 residues. Cattle, meat ...... 0.1 Cattle, meat byproducts ...... 0.1 (a) General. Tolerances are estab- Corn, field, forage ...... 1.0 lished for residues of the herbicide, Corn, field, grain ...... 0.02 isoxaflutole, including its metabolites Corn, field, stover ...... 0.5 Corn, sweet, forage ...... 1.0 and degradates, in or on the commod- Corn, sweet, kernel plus cob with husks removed 0.02 ities in the table below. Compliance Corn, sweet, stover ...... 2.0 with the tolerance levels specified Fruit, pome, group 11 ...... 0.02 Garlic, bulb ...... 0.03 below is to be determined by measuring Goat, fat ...... 0.1 only the sum of isoxaflutole ((5- Goat, kidney ...... 1.5 cyclopropyl-4-isoxazolyl) [2- Goat, meat ...... 0.1 (methylsulfonyl)-4- Goat, meat byproducts ...... 0.1 Grain, aspirated fractions ...... 0.6 (trifluoromethyl)phenyl] methanone) Grass, forage ...... 120 and its metabolite 1-(2-methylsulfonyl- Grass, hay ...... 160 4-trifluoromethylphenyl)-2-cyano-3- Hog, fat ...... 0.1 cyclopropyl propan-1,3-dione (RPA Hog, kidney ...... 1.5 Hog, meat ...... 0.1 202248), calculated as the stoichio- Hog, meat byproducts ...... 0.1 metric equivalent of isoxaflutole, in or Horse, fat ...... 0.1 on the commodity: Horse, kidney ...... 1.5 Horse, meat ...... 0.1 Parts per Horse, meat byproducts ...... 0.1 Commodity million Milk ...... 0.3 Millet, forage ...... 12.0 Corn, field, forage ...... 0.04 Millet, grain ...... 0.5 Corn, field, grain ...... 0.02 Millet, hay ...... 20.0 Corn, field, stover ...... 0.02 Millet, proso, straw ...... 12.0 Grain, aspirated fractions ...... 0.30 Oat, forage ...... 12.0 Soybean, seed ...... 0.05 Oat, grain ...... 0.5 Oat, hay ...... 20.0 (b) Section 18 emergency exemptions. Oat, straw ...... 12.0 [Reserved] Onion, bulb ...... 0.03 Rice, bran ...... 3.0 (c) Tolerances with regional registra- Rice, grain ...... 1.5 tions. [Reserved] Shallot, bulb ...... 0.03 (d) Indirect or inadvertent residues. Sheep, fat ...... 0.1 [Reserved] Sheep, kidney ...... 1.5 Sheep, meat ...... 0.1 [63 FR 50784, Sept. 23, 1998, as amended at 73 Sheep, meat byproducts ...... 0.1 FR 75608, Dec. 12, 2008; 76 FR 76314, Dec. 7, Sorghum, grain, forage ...... 2.0 2011] Sorghum, grain, grain ...... 0.02 Sorghum, grain, stover ...... 4.0 Teff, forage ...... 12 § 180.539 d-Limonene; tolerances for Teff, grain ...... 0.50 residues. Teff, hay ...... 20 (a) General. (1) The insecticide d-lim- Teff, straw ...... 12 Wheat, forage ...... 12.0 onene may be safely used in insect-re- Wheat, grain ...... 0.5 pellent tablecloths and in insect-repel- Wheat, hay ...... 20.0 lent strips used in food- or feed-han- Wheat, straw ...... 12.0 dling establishments.

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(2) To assure safe use of the insect re- (d) Indirect or inadvertent residues. pellent, its label and labeling shall con- [Reserved] form to that registered by the U.S. En- [65 FR 12134, Mar. 8, 2000] vironmental Protection Agency, and it shall be used in accordance with such § 180.544 Methoxyfenozide; tolerances label and labeling. for residues. (b) Section 18 emergency exemptions. (a) General. (1) Tolerances are estab- [Reserved] lished for residues of the insecticide (c) Tolerances with regional registra- methoxyfenozide, including its metabo- tions. [Reserved] lites and degradates, in or on the com- (d) Indirect or inadvertent residues. modities listed in the following table. [Reserved] Compliance with the tolerance levels [65 FR 33715, May 24, 2000, as amended at 70 specified in the following table is to be FR 55268, Sept. 21, 2005] determined by measuring only methoxyfenozide (3-methoxy-2- § 180.540 Fenitrothion; tolerances for methylbenzoic acid 2-(3,5- residues. dimethylbenzoyl)-2-(1,1-dimethylethyl) hydrazide) in or on the commodity. (a) General. Tolerances are established for residues of the insecticide Commodity Parts per fenitrothion, O,O-dimethyl O-(4-nitro- million m-tolyl) phosphorothioate, from the Acerola ...... 0.4 postharvest application of the insecti- Almond, hulls ...... 25 cide to stored wheat in Australia, in or Animal feed, nongrass, group 18, forage ...... 50.0 Animal feed, nongrass, group 18, hay ...... 150.0 on the following food commodity: Apple, wet pomace ...... 7.0 Artichoke, globe ...... 3.0 Commodity Parts per Atemoya ...... 0.60 million Avocado ...... 0.6 Beet, sugar, roots ...... 0.50 1 Wheat, gluten ...... 3.0 Berry, low growing, subgroup 13–07G, except 1 There are no U.S. registrations on food commodities since cranberry ...... 2.0 1987. Biriba ...... 0.60 Brassica, head and stem, subgroup 5A ...... 7.0 (b) Section 18 emergency exemptions. Brassica, leafy greens, subgroup 5B ...... 30 [Reserved] Bushberry subgroup 13-07B ...... 3.0 Caneberry subgroup 13–07A ...... 6.0 (c) Tolerances with regional registra- Canistel ...... 0.6 tions. [Reserved] Cattle, fat ...... 0.50 Cattle, meat ...... 0.02 (d) Indirect or inadvertent residues. Cherimoya ...... 0.60 [Reserved] Chive, fresh leaves ...... 30 Citrus, oil ...... 100 [73 FR 54963, Sept. 24, 2008] Corn, field, forage ...... 15 Corn, field, grain ...... 0.05 § 180.543 Diclosulam; tolerances for Corn, field, refined oil ...... 0.20 Corn, field, stover ...... 125 residues. Corn, pop, grain ...... 0.05 (a) General. Tolerances are estab- Corn, pop, stover ...... 125 Corn, sweet, forage ...... 30 lished for residues of the herbicide Corn, sweet, kernel plus cob with husks removed 0.05 diclosulam [N-(2,6-dichlorophenyl)-5- Corn, sweet, stover ...... 60 ethoxy-7-fluoro[1,2,4] triazolo[1,5- Cotton, gin byproducts ...... 35 Cotton, undelinted seed ...... 2.0 c]pyrimidine-2-sulfonamide] in or on Cranberry ...... 0.5 the following raw agricultural com- Custard apple ...... 0.60 modities as follows: Date ...... 8.0 Feijoa ...... 0.4 Parts per Fruit, citrus, group 10–10 ...... 3.0 Commodity million Fruit, pome, group 11–10 ...... 2.0 Fruit, small, vine climbing, except fuzzy kiwifruit, Peanut ...... 0.020 subgroup 13–07F ...... 1.0 Soybean, seed ...... 0.020 Fruit, stone, group 12–12, except plum, prune, fresh ...... 3.0 Goat, fat ...... 0.50 (b) Section 18 emergency exemptions. Goat, meat ...... 0.02 [Reserved] Grain, aspirated grain fractions ...... 120 Grape, raisin ...... 1.5 (c) Tolerances with regional registra- Grass, forage, fodder and hay, group 17, forage 18.0 tions. [Reserved] Grass, forage, fodder and hay, group 17, hay ...... 30.0

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(2) Tolerances are established for res- Commodity Parts per million idues of the insecticide Guava ...... 0.4 methoxyfenozide, including its metabo- Herb subgroup 19A, except chive, fresh leaves ... 400 lites and degradates, in or on the com- Hog, fat ...... 0.1 modities in the following table. Com- Hog, meat ...... 0.02 Horse, fat ...... 0.50 pliance with the tolerance levels speci- Horse, meat ...... 0.02 fied in the following table is to be de- Ilama ...... 0.60 termined by measuring only the sum of Jaboticaba ...... 0.4 Leaf petioles subgroup 4B ...... 25 methoxyfenozide [3-methoxy-2- Leafy greens subgroup 4A ...... 30 methylbenzoic acid 2-(3,5- Longan ...... 2.0 dimethylbenzoyl)-2-(1,1-dimethylethyl) Lychee ...... 2.0 Mango ...... 0.6 hydrazide] and its glucuronide metabo- Milk ...... 0.10 lite (b-D-Glucopyranuronic acid, 3-[[2- Nut, tree, group 14–12 ...... 0.10 (1,1-dimethylethyl)-2-(3,5- Onion, green, subgroup 3–07B, except chive, fresh leaves ...... 5.0 dimethylbenzoyl)-hydrazino]carbonyl]- Papaya ...... 0.6 2-methylphenyl-), calculated as the Passionfruit ...... 0.4 stoichiometric equivalent of Pea and bean, dried shelled, except soybean, subgroup 6C, except pea, blackeyed, seed and methoxyfenozide. pea, southern, seed ...... 0.50 Pea and bean, succulent shelled, subgroup 6B ... 0.2 Parts per Commodity million Pea, blackeyed, seed ...... 4.0 Pea, southern, seed ...... 4.0 Cattle, liver ...... 0.40 Peanut ...... 0.02 Cattle, meat byproducts, except liver ...... 0.10 Peanut, hay ...... 55.0 Egg ...... 0.02 Peanut, oil ...... 0.04 Goat, liver ...... 0.40 Peppermint, tops ...... 7.0 Goat, meat byproducts, except liver ...... 0.10 Pineapple ...... 0.70 Hog, liver ...... 0.1 Plum, prune, fresh ...... 0.30 Hog, meat byproducts, except liver ...... 0.02 Pomegranate ...... 0.6 Horse, liver ...... 0.40 Poultry, fat ...... 0.02 Poultry, meat ...... 0.02 Horse, meat byproducts, except liver ...... 0.10 Pulasan ...... 2.0 Poultry, liver ...... 0.10 Rambutan ...... 2.0 Poultry, meat byproducts, except liver ...... 0.02 Sapodilla ...... 0.6 Sheep, liver ...... 0.40 Sapote, black ...... 0.6 Sheep, meat byproducts, except liver ...... 0.10 Sapote, mamey ...... 0.6 Sheep, fat ...... 0.50 (b) Section 18 emergency exemptions. Sheep, meat ...... 0.02 Time-limited tolerances are estab- Sorghum, grain, forage ...... 15 Sorghum, grain, grain ...... 6.0 lished for residues of the insecticide Sorghum, grain, stover ...... 20 methoxyfenozide, including its metabo- Sorghum, sweet, forage ...... 15 lites and degradates in or on the com- Sorghum, sweet, grain ...... 6.0 Sorghum, sweet, stalk ...... 15 modities listed in table 3 to this para- Sorghum, sweet, stover ...... 20 graph (b), resulting from use of the pes- Soursop ...... 0.60 ticide under a Section 18 emergency ex- Soybean, aspirated grain fractions ...... 160 Soybean, forage ...... 30 emption granted by EPA. Compliance Soybean, hay ...... 80 with the tolerance levels specified in Soybean, hulls ...... 2.0 table 3 to this paragraph (b) is to be de- Soybean, seed ...... 1.0 Spanish lime ...... 2.0 termined by measuring only Spearmint, tops ...... 7.0 methoxyfenozide (3-methoxy-2- Star apple ...... 0.6 methylbenzoic acid 2-(3,5- Starfruit ...... 0.4 Sugar apple ...... 0.60 dimethylbenzoyl)-2-(1,1-dimethylethyl) Tea, dried 1 ...... 20 hydrazide) in or on the commodity. Tea, instant 1 ...... 20 Turnip, greens ...... 30 Parts per Expiration/ Vegetable, cucurbit, group 9 ...... 0.3 Commodity million revocation Vegetable, foliage of legume, except soybean, date subgroup 7A ...... 35 Vegetable, fruiting, group 8–10 ...... 2.0 Rice, bran ...... 4.0 12/31/22 Vegetable, leaves of root and tuber, group 2 ...... 30 Rice, grain ...... 0.50 12/31/22 Vegetable, legume, edible podded, subgroup 6A 1.5 Vegetable, root, except sugar beet, Subgroup 1B 0.90 (c) Tolerances with regional registra- Vegetable, tuberous and corm, except potato, tions. [Reserved] subgroup 1D ...... 0.02 Wax jambu ...... 0.4 (d) Indirect or inadvertent tolerances. (1) Tolerances are established for the 1 There are no U.S. registrations as of March 12, 2019 for use on tea. indirect or inadvertent residues of the

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insecticide methoxyfenozide, including EDITORIAL NOTE: For FEDERAL REGISTER ci- its metabolites and degradates, in or tations affecting § 180.544, see the List of CFR on the raw agricultural commodities in Sections Affected, which appears in the the following table, when present Finding Aids section of the printed volume and at www.govinfo.gov. therein as a result of the application of methoxyfenozide to growing crops as § 180.545 Prallethrin; tolerances for listed in paragraph (a) of this section. residues. Compliance with the tolerance levels (a) General. Tolerances are estab- specified in the following table is to be lished for residues of the insecticide determined by measuring only prallethrin, including its metabolites methoxyfenozide [3-methoxy-2- and degradates, in or on all raw agri- methylbenzoic acid 2-(3,5- cultural commodities and processed dimethylbenzoyl)-2-(1,1-dimethylethyl) food from use of prallethrin in food hydrazide]. handling establishments where food and food products are held, processed, Commodity Parts per million prepared and/or served, or as a wide- Onion, bulb, subgroup 3–07A ...... 0.10 area mosquito adulticide at 1.0 part per Potato ...... 0.02 million (ppm). Compliance with the tolerance level specified is to be deter- (2) Tolerances are established for the mined by measuring only prallethrin, indirect or inadvertent residues of the 2-methyl-4-oxo-3-(2-propyn-1-yl)-2- insecticide methoxyfenozide, including cyclopenten-1-yl-2,2-dimethyl-3-(2- its metabolites and degradates, in or methyl-1-propen-1- on the raw agricultural commodities in yl)cyclopropanecarboxylate. the following table, when present (b) Section 18 emergency exemptions. therein as a result of the application of [Reserved] methoxyfenozide to growing crops as (c) Tolerances with regional registra- listed in paragraph (a) of this section. tions. [Reserved] Compliance with the tolerance levels (d) Indirect or inadvertent residues. specified in the following table is to be [Reserved] determined by measuring only the sum of methoxyfenozide [3-methoxy-2- [79 FR 64330, Oct. 29, 2014] methylbenzoic acid, 2-(3,5- § 180.546 Mefenoxam; tolerances for dimethylbenzoyl)-2-(1,1-dimethylethyl) residues. hydrazide] and the following metabo- (a) General. Tolerances are estab- lites (all calculated as the stoichio- lished for residues of mefenoxam, in- metric equivalent of methoxyfenozide): cluding its metabolites and degradates, free phenol of methoxyfenozide [3,5- in or on the commodities in the table dimethylbenzoic acid N-tert-butyl-N′- below. Compliance with the tolerance (3-hydroxy-2-methylbenzoyl) hydra- levels specified below is to be deter- zide], the glucose conjugate of the phe- mined by measuring only metalaxyl nol [3,5-dimethyl benzoic acid N-tert- (methyl N-(2,6-dimethylphenyl)-N- butyl-N′-[3 (b-D-glucopyranosyloxy)-2- (methoxyacetyl)-DL-alaninate). methylbenzoyl]-hydrazide] and the malonylglycosyl conjugate of the phe- Commodity Parts per nol [3,5-dimethyl benzoic acid N-tert- million ′ butyl-N -[3 (b-D-6-malonyl- Artichoke, globe ...... 0.05 glucopyranosyl-1-oxy)-2- Atemoya ...... 0.20 methylbenzoyl]-hydrazide]. Bean, snap, succulent ...... 0.20 Bushberry subgroup 13–07B ...... 2.0 Parts per Cacao, dried bean ...... 0.20 Commodity million Caneberry subgroup 13–07A ...... 0.70 Canistel ...... 0.40 Animal feed, nongrass, group 18, straw ...... 8.0 Custard apple ...... 0.20 Grain, cereal, forage, fodder and straw group 16, Fruit, small, vine climbing, except grape, sub- except corn ...... 6.0 group 13–07E ...... 0.10 Rapeseed subgroup 20A ...... 1.0 Herbs, dried ...... 55 Spice subgroup 19B ...... 4.5 Herbs, fresh ...... 8.0 Sunflower subgroup 20B ...... 1.0 Mango ...... 0.40 Onion, bulb, subgroup 3–07A ...... 3.0 Onion, green, subgroup 3–07B ...... 10 [67 FR 59203, Sept. 20, 2002] Papaya ...... 0.40

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istration are established for residues of Commodity Parts per million the plant growth regulator, Rapeseed subgroup 20A ...... 0.05 prohexadione calcium, including its Sapodilla ...... 0.40 metabolites and degradates, in or on Sapote, black ...... 0.40 the commodities in table 2 in this para- Sapote, mamey ...... 0.40 Spinach ...... 10 graph (c). Compliance with the toler- Star apple ...... 0.40 ance levels specified in table 2 in this Starfruit ...... 0.20 paragraph (c) is to be determined by Sugar apple ...... 0.20 Wasabi, stem ...... 3.0 measuring only prohexadione calcium Wasabi, tops ...... 6.0 (calcium 3-oxido-5-oxo-4- propionylcyclohex-3-enecarboxylate) in (b) Section 18 emergency exemptions. or on the following commodities. [Reserved] (c) Tolerances with regional registra- TABLE 2 TO PARAGRAPH (c) tions. [Reserved] Parts per (d) Indirect or inadvertant residues. Commodity million [Reserved] Alfalfa, forage ...... 0.1 [65 FR 57556, Sept. 25, 2000, as amended at 66 Alfalfa, hay ...... 0.1 FR 48003, Sept. 17, 2001; 67 FR 35050, May 17, Corn, field, forage ...... 0.1 2002; 76 FR 4548, Jan. 26, 2011; 81 FR 26727, Corn, field, grain ...... 0.1 May 4, 2016; 83 FR 65546, Dec. 21, 2018] Corn, field, stover ...... 0.1

§ 180.547 Prohexadione calcium; toler- (d) Indirect or inadvertent residues. ances for residues. [Reserved] (a) General. Tolerances are established for residues of the growth regu- [65 FR 25660, May 3, 2000, as amended at 66 FR 29712, June 1, 2001; 76 FR 71464, Nov. 18, lator, prohexadione calcium, including 2011; 80 FR 38980, July 8, 2015; 85 FR 8461, Feb. its metabolites and degradates, in or 14, 2020] on the commodities in the table below. Compliance with the tolerance levels § 180.549 Diflufenzopyr; tolerances for specified below is to be determined by residues. measuring only prohexadione calcium (a) General. Tolerances are estab- (calcium 3-oxido-5-oxo-4- lished for combined residues of propionylcyclohex-3-enecarboxylate)’’ diflufenzopyr, 2-(1-[([3,5- in or on the following commodities. difluorophenylamino] car- Parts per bonyl)hydrazono]ethyl)-3- Commodity million pyridinecarboxylic acid, and its me- Cattle, kidney ...... 0.10 tabolites convertible to 8- Cattle, meat byproducts, except kidney ...... 0.05 methylpyrido[2,3-d]pyridazin-5(6H)-one, Cherry, sweet ...... 0.40 expressed as diflufenzopyr, in or on the Fruit, pome, group 11 ...... 3.0 following raw agricultural commod- Goat, kidney ...... 0.10 Goat, meat byproducts, except kidney ...... 0.05 ities: Grass, forage 1 ...... 0.10 1 Grass, hay ...... 0.10 Commodity Parts per Grass, seed screenings 1 ...... 3.5 million Grass, straw 1 ...... 1.2 Hog, kidney ...... 0.10 Corn, field, forage ...... 0.05 Hog, meat byproducts, except kidney ...... 0.05 Corn, field, grain ...... 0.05 Horse, kidney ...... 0.10 Corn, field, stover ...... 0.05 Horse, meat byproducts, except kidney ...... 0.05 Corn, pop, grain ...... 0.05 Peanut ...... 1.0 Corn, pop, stover ...... 0.05 Peanut, hay ...... 0.60 Corn, sweet, forage ...... 0.05 Sheep, kidney ...... 0.10 Corn, sweet, kernel plus cob with husks removed 0.05 Sheep, meat byproducts, except kidney ...... 0.05 Strawberry ...... 0.30 Corn, sweet, stover ...... 0.05 Watercress ...... 4.0 Grass, forage ...... 22.0 Grass, hay ...... 7.0 1Registration is limited to grass grown for seed. (b) Section 18 emergency exemptions. (b) Section 18 emergency exemptions. [Reserved] [Reserved] (c) Tolerances with regional registra- (c) Tolerances with regional registrations. Tolerances with regional reg- tions. [Reserved]

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(d) Indirect or inadvertent residues. dimethoxypyrimidin-2-yl)-3-[(2- [Reserved] ethanesulfonyl-imidazo[1,2-a]pyridine- 3-yl) sulfonyl]urea and its metabolites [64 FR 4308, Jan. 28, 1999, as amended at 67 FR 55338, Aug. 29, 2002; 76 FR 34886, June 15, converted to 2-(ethylsulfonyl)- 2011] imidazo[1,2-a]pyridine and calculated as sulfosulfuron in or on the raw agri- § 180.551 Fluthiacet-methyl; tolerances cultural commodities. for residues. Parts per (a) General. (1) A tolerance is estab- Commodity million lished for residues of the herbicide, fluthiacet-methyl, acetic acid [[2- Cattle, fat ...... 0.02 Cattle, meat ...... 0.01 chloro-4-fluoro-5-[(tetrahydro-3-oxo- Cattle, meat byproducts ...... 0.3 1H,3H-[1,3,4]thiadiazolo[3,4-a]pyridazin- Goat, fat ...... 0.02 1-ylidene)amino]phenyl]thio]-methyl Goat, meat ...... 0.01 Goat, meat byproducts ...... 0.3 ester, in or on the food commodity: Grass, forage, fodder and hay, group 17, forage 14 Grass, forage, fodder and hay, group 17, hay ...... 25 Commodity Parts per Hog, fat ...... 0.005 million Hog, meat ...... 0.005 Hog, meat byproducts ...... 0.05 Corn, field, forage ...... 0.050 Horse, fat ...... 0.02 Corn, field, grain ...... 0.010 Corn, field, stover ...... 0.050 Horse, meat ...... 0.01 Corn, pop, grain ...... 0.010 Horse, meat byproducts ...... 0.3 Corn, pop, stover ...... 0.050 Milk ...... 0.02 Corn, sweet, forage ...... 0.050 Sheep, fat ...... 0.02 Corn, sweet, kernel plus cob with husks removed 0.010 Sheep, meat ...... 0.01 Corn, sweet, stover ...... 0.050 Sheep, meat byproducts ...... 0.3 Soybean, seed ...... 0.01 Wheat, forage ...... 4.0 Wheat, grain ...... 0.02 Wheat, hay ...... 0.3 (2) A tolerance is established for the Wheat, straw ...... 0.1 combined residues of the herbicide fluthiacet-methyland its acid metabo- (b) Section 18 emergency exemptions. lite: acetic acid, [[2-chloro-4-fluoro-5- [Reserved] [tetrahydro-3-oxo-1H,3H- (c) Tolerances with regional registra- [1,3,4]thiadiazolo[3,4-a]pyridazin-1- tions. [Reserved] ylidene)amino]phenyl]thio]-methyl (d) Indirect or inadvertent residues. ester, and its acid metabolite, acetic [Reserved] acid, [[2-chloro-4-fluoro-5-[(tetrahydro- 3-oxo-1H,3H-[1,3,4]thiadiazolo[3,4- [64 FR 27192, May 19, 1999, as amended at 70 FR 69464, Nov. 16, 2005; 72 FR 54574, Sept. 26, a]pyridazin-1- 2007] ylidene)amino]phenyl]thio]- , in or on the following food commodities: § 180.553 Fenhexamid; tolerances for residues. Parts per Commodity million (a) General. Tolerances are estab- Cotton, gin byproducts ...... 0.20 lished for residues of fenhexamid, in- Cotton, undelinted seed ...... 0.020 cluding its metabolites and degradate, in or on the commodities in the table (b) Section 18 emergency exemptions. in this paragraph (a). Compliance with [Reserved] the tolerance levels specified in this (c) Tolerances with regional registra- paragraph (a) is to be determined by tions. [Reserved] measuring only fenhexamid (N-2,3- (d) Indirect or inadvertent residues. dichloro-4-hydroxyphenyl)-1- [Reserved] methylcyclohexanecarboxamide).

[64 FR 18357, Apr. 14, 1999, as amended at 66 Parts per FR 65850, Dec. 21, 2001; 71 FR 77625, Dec. 27, Commodity million 2006] Almond, hulls ...... 2.0 Almond ...... 0.02 § 180.552 Sulfosulfuron; tolerances for Arugula ...... 30 residues. Asparagus ...... 0.02 (a) General. Tolerances are estab- Berry, low growing, subgroup 13–07G ...... 3 Bushberry subgroup 13–07B ...... 5 lished for residues of the herbicide Caneberry subgroup 13–07A ...... 20 sulfosulfuron, 1–(4,6- Cress, garden ...... 30

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(2) Tolerances are established in or Commodity Parts per million on the following commodities for the Cress, upland ...... 30 residues of the metabolite (E)-2-[2-(2- Cucumber ...... 2.0 methylphenoxy)methyl]-phenyl-2- Fruit, small, vine climbing, except fuzzy kiwifruit, (methoxyimido)acetic acid resulting subgroup 13–07F ...... 4 from the use of the fungicide kresoxim- Fruit, stone, group 12–12, except plum, prune ..... 10 Ginseng ...... 0.3 methyl: Grape, raisin ...... 6.0 Kiwifruit, fuzzy ...... 30 Parts per Commodity million Leafy greens, subgroup 4–16A, except spinach ... 30 Onion, bulb, subgroup 3–07A ...... 2 Cattle, meat byproducts ...... 0.01 Onion, green, subgroup 3–07B ...... 30 Goat, meat byproducts ...... 0.01 Pear ...... 10 Sheep, meat byproducts ...... 0.01 Pepper, nonbell ...... 0.02 Pistachio ...... 0.02 (b) Section 18 emergency exemptions. Plum, prune, dried ...... 2.5 [Reserved] Plum, prune, fresh ...... 1.5 Pomegranate ...... 2.0 (c) Tolerances with regional registra- Vegetable, fruiting, group 8–10, except nonbell tions. [Reserved] pepper ...... 2 (d) Indirect or inadvertent residues. [Reserved] (b) Section 18 emergency exemptions. [Reserved] [64 FR 31136, June 10, 1999, as amended at 71 (c) Tolerances with regional registra- FR 50359, Aug. 25, 2006; 74 FR 46377, Sept. 9, 2009] tions. [Reserved] (d) Indirect or inadvertent residues. § 180.555 Trifloxystrobin; tolerances [Reserved] for residues. [64 FR 28924, May 28, 1999, as amended at 65 (a) General. Tolerances are estab- FR 19849, Apr. 13, 2000; 65 FR 69883, Nov. 21, lished for residues of trifloxystrobin, 2000; 67 FR 19120, Apr. 18, 2002; 68 FR 2247, including its metabolites and Jan. 16, 2003; 68 FR 55519, Sept. 26, 2003; 71 FR degradates, in or on the commodities 15617, Mar. 29, 2006; 71 FR 43664, Aug. 2, 2006; in the table below. Compliance with 73 FR 19154, Apr. 9, 2008; 85 FR 2659, Jan. 16, the tolerance levels specified below is 2020] to be determined by measuring only § 180.554 Kresoxim-methyl; tolerances the sum of trifloxystrobin, for residues. benzeneacetic acid, (E,E)-a- (methoxyimino)-2-[[[[1-[3- (a) General. (1) Tolerances are estab- (trifluoromethyl) phenyl]ethylidene] lished for the combined residues of the amino]oxy]methyl]-, methyl ester, and fungicide kresoxim-methyl (methyl the free form of its acid metabolite (E)-2-[2-(2-methylphenoxy)-meth- CGA–321113, (E,E)-methoxyimino-[2-[1- yl]phenyl-2-(methoxyimido)acetate) (3-trifluoromethyl-phenyl)- and its metabolites as follows: (E)-2-[2- ethylideneaminooxymethyl]- (2-methylphenoxy)methyl]-phenyl-2- phenyl]acetic acid, calculated as the (methoxyimido)acetic acid; (E)-2-[2-(2- stoichiometric equivalent of hydroxymethylphenoxy)methyl]- trifloxystrobin, in or on the com- phenyl-2-(methoxyimido)acetic acid modity. (free and glucose conjugated); and (E)- 2-[2-(4-hydroxy-2-methylphenoxy)- Commodity Parts per methyl]phenyl-2-(methoxyimido)acetic million acid (free and glucose conjugated) in or Alfalfa, forage ...... 0.01 on the following commodities: Alfalfa, hay ...... 0.01 Almond, hulls ...... 9.0 Parts per Apple, wet pomace ...... 5.0 Commodity million Artichoke, globe ...... 1.0 Asparagus ...... 0.07 Apple, dry pomace ...... 1.0 Banana 1 ...... 0.10 Apple, wet pomace ...... 1.0 Barley, grain ...... 0.05 Fruit, pome ...... 0.5 Barley, hay ...... 0.3 Grape ...... 1.0 Barley, straw ...... 5.0 Grape, raisin ...... 1.5 Beet, sugar, dried pulp ...... 0.4 Pecan ...... 0.15 Beet, sugar, molasses ...... 0.2 Vegetable, cucurbit, group 9 ...... 0.40 Beet, sugar, roots ...... 0.1 Beet, sugar, tops ...... 4.0

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Parts per Parts per Commodity million Commodity million

Berry, low growing subgroup 13–07G ...... 1.5 Sheep, meat byproducts ...... 0.1 Brassica, head and stem, subgroup 5A ...... 2.0 Soybean, forage ...... 10.0 Brassica, leafy greens, subgroup 5B ...... 30 Soybean, hay ...... 25.0 Canistel ...... 0.7 Soybean, seed ...... 0.08 Cattle, fat ...... 0.1 Star apple ...... 0.7 Cattle, meat ...... 0.1 Tea, dried 3 ...... 5 Cattle, meat byproducts ...... 0.1 Tea, instant 3 ...... 5 Citrus, dried pulp ...... 1.0 Vegetable, cucurbit, group 9 ...... 0.50 Citrus, oil ...... 38 Vegetable, fruiting ...... 0.5 Coffee, green bean 2 ...... 0.02 Vegetable, root, except sugar beet, subgroup 1B 0.1 Corn, field, forage ...... 8.0 Vegetable, tuberous and corm, subgroup 1C ...... 0.04 Corn, field, grain ...... 0.05 Wheat, bran ...... 0.15 Corn, field, stover ...... 7 Wheat, forage ...... 0.3 Corn, field, refined oil ...... 0.1 Wheat, grain ...... 0.05 Corn, pop, grain ...... 0.05 Wheat, hay ...... 0.2 Corn, pop, stover ...... 7 Wheat, straw ...... 5.0 Corn, sweet, cannery waste ...... 0.6 Corn, sweet, forage ...... 7.0 1 There are no U.S. registrations as of September 27, 1999 Corn, sweet, kernel plus cob with husks removed 0.04 for use on banana. 2 There are no U.S. registrations as of January 18, 2012 for Corn, sweet, stover ...... 4.0 use on coffee, green bean. Cotton, gin byproducts ...... 3.0 3 There are no U.S. registrations as of June 24, 2019, for Cottonseed subgroup 20C ...... 0.50 use on tea. Dill, seed ...... 30 Egg ...... 0.04 (b) Section 18 emergency exemptions. Flax, seed ...... 0.40 [Reserved] Fruit, citrus, group 10 ...... 0.6 (c) Tolerances with regional registra- Fruit, pome ...... 0.5 Fruit, small vine climbing, except fuzzy kiwifruit, tions. [Reserved] subgroup 13–07F ...... 2.0 (d) Indirect or inadvertent residues. Fruit, stone, group 12 ...... 2 [Reserved] Goat, fat ...... 0.1 Goat, meat ...... 0.1 [64 FR 51907, Sept. 27, 1999] Goat, meat byproducts ...... 0.1 Grain, aspirated fractions ...... 10 EDITORIAL NOTE: For FEDERAL REGISTER ci- Grape, raisin ...... 5.0 tations affecting § 180.555, see the List of CFR Grass, forage ...... 12 Sections Affected, which appears in the Grass, hay ...... 17 Finding Aids section of the printed volume Herbs, subgroup 19A ...... 200 and at www.govinfo.gov. Hog, fat ...... 0.05 Hog, meat ...... 0.05 Hog, meat byproducts ...... 0.05 § 180.556 Pymetrozine; tolerances for Hop, dried cones ...... 11.0 residues. Horse, fat ...... 0.1 Horse, meat ...... 0.1 (a) General. Tolerances are estab- Horse, meat byproducts ...... 0.1 lished for residues of the insecticide Leaf petioles subgroup 4B ...... 9.0 pymetrozine 1,2,4-triazin-3(2H)-one,4,5- Leafy greens, subgroup 4A ...... 30 dihydro-6-methyl-4-[(3- Mango ...... 0.7 Milk ...... 0.02 pyridinylmethylene) amino] in or on Nut, tree, group 14 ...... 0.04 the following raw agricultural com- Oat, forage ...... 0.3 modities. The tolerance level for each Oat, grain ...... 0.05 Oat, hay ...... 0.3 commodity is expressed in terms of the Oat, straw ...... 5.0 parent insecticide only, which serves as Papaya ...... 0.7 an indicator of the use of pymetrozine Pea, field, hay ...... 15 on these raw agricultural commodities. Pea, field, vines ...... 4 Pea and bean, dried shelled, except soybean, subgroup 6C ...... 0.06 Parts per Commodity million Peanut, hay ...... 4.0 Peanut ...... 0.05 Asparagus ...... 0.04 Pistachio ...... 0.04 Brassica, head and stem, subgroup 5A ...... 0.5 Poultry, fat ...... 0.04 Brassica, leafy greens, subgroup 5B ...... 0.25 Poultry, meat ...... 0.04 Cotton, gin byproducts ...... 2.0 Poultry, meat byproducts ...... 0.04 Cotton, undelinted seed ...... 0.3 Radish, tops ...... 10 Hop, dried cones ...... 6.0 Rice, grain ...... 3.5 Pecan ...... 0.02 Rice, hulls ...... 8 Turnip, greens ...... 0.25 Sapodilla ...... 0.7 Vegetable, fruiting, group 8 ...... 0.2 Sapote, black ...... 0.7 Vegetable, cucurbit, group 9 ...... 0.1 Sapote, mamey ...... 0.7 Vegetable, leafy, execpt brassica, group 4 ...... 0.6 Sheep, fat ...... 0.1 Vegetable, tuberous and corm, subgroup 1C ...... 0.02 Sheep, meat ...... 0.1

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(b) Section 18 emergency exemptions. Commodity Parts per [Reserved] million (c) Tolerances with regional registra- Sheep, meat ...... 0.02 tions. [Reserved] Sheep, meat byproducts (except liver) ...... 0.15 (d) Indirect or inadvertent residues. Small fruit vine climbing, except fuzzy kiwifruit, [Reserved] subgroup 13–07F ...... 0.20 Soybean, refined oil ...... 0.80 [65 FR 48634, Aug. 9, 2000, as amended at 66 Soybean, seed ...... 0.15 FR 14846, Mar. 14, 2001; 66 FR 66794, Dec. 27, Vegetable, cucurbit, group 9 ...... 0.15 2001; 70 FR 7047, Feb. 10, 2005; 70 FR 43298, Vegetable, foliage of legume (except soybeans) July 27, 2005] subgroup 7A ...... 8.0 Vegetable, fruiting, group 8–10 ...... 0.30 § 180.557 Tetraconazole; tolerances for Wheat, bran ...... 0.15 Wheat, flour ...... 0.08 residues. Wheat, germ ...... 0.50 (a) General. Tolerances are estab- Wheat, grain ...... 0.05 lished for residues of tetraconazole, including its metabolites and degradates, (b) Section 18 emergency exemptions. in or on the commodities listed below. [Reserved] Compliance with the following toler- (c) Tolerances with regional registra- ance levels is to be determined by tions. [Reserved] measuring only tetraconazole (1-[2-(2,4- (d) Indirect or inadvertent residues. dichlorophenyl)-3-(1,1,2,2- [Reserved] tetrafluoroethoxy)propyl]-1H-1,2,4-tri- [70 FR 20830, Apr. 22, 2005, as amended at 70 azole), in or on the following commod- FR 31359, June 1, 2005; 72 FR 18134, Apr. 11, ities. 2007; 73 FR 67406, Nov. 14, 2008; 76 FR 53648, Aug. 29, 2011; 82 FR 2905, Jan. 10, 2017; 83 FR Parts per Commodity million 16206, Apr. 16, 2018] Barley, bran ...... 1.0 § 180.559 Clodinafop-propargyl; toler- Barley, flour ...... 0.50 ances for residues. Barley, grain ...... 0.30 Beet sugar, dried pulp ...... 0.20 (a) General. Tolerances are estab- Beet sugar, molasses ...... 0.25 Beet sugar, root ...... 0.15 lished for clodinafop-propargyl, includ- Cattle, fat ...... 0.15 ing its metabolites and degradates, in Cattle, liver ...... 1.50 or on the commodities in the following Cattle, meat ...... 0.02 table. Compliance with the tolerance Cattle, meat byproducts (except liver) ...... 0.15 Corn, field, grain ...... 0.01 levels specified in the following table is Corn, pop, grain ...... 0.01 to be determined by measuring only Eggs ...... 0.02 clodinafop-propargyl [(2R)-2-[4-[(5- Goat, fat ...... 0.15 Goat, liver ...... 1.50 chloro-3-fluoro-2- Goat, meat ...... 0.02 pyridinyl)oxy]phenoxy]propanoic acid, Goat, meat byproducts (except liver) ...... 0.15 2-propynyl ester] and its metabolite Grain, aspirated fractions ...... 4.0 Grain, cereal, forage, fodder, and straw, group 16 7.0 clodinafop [(2R)-2-[4-[(5-chloro-3-fluoro- Hog, fat ...... 0.01 2- pyridinyl)oxy]phenoxy]propanoic Hog, liver ...... 0.05 acid]. Hog, meat ...... 0.01 Hog, meat byproducts (except liver) ...... 0.01 Parts per Horse, fat ...... 0.15 Commodity million Horse, liver ...... 1.50 Horse, meat ...... 0.02 Wheat, forage ...... 0.1 Horse, meat byproducts (except liver) ...... 0.15 Wheat, grain ...... 0.02 Low growing berry subgroup 13–07G, except Wheat, hay ...... 0.1 cranberry ...... 0.25 Milk ...... 0.06 Wheat, straw ...... 0.5 Milk, fat ...... 0.75 Pea and bean, dried shelled (except soybean) (b) Section 18 emergency exemptions. subgroup 6C ...... 0.09 [Reserved] Peanut ...... 0.03 Peanut, oil ...... 0.10 (c) Tolerances with regional registra- Pecan ...... 0.04 tions. [Reserved] Poultry, fat ...... 0.05 (d) Indirect or inadvertent residues. Poultry, meat ...... 0.01 Poultry meat byproducts ...... 0.05 [Reserved] Rapeseed subgroup 20A ...... 0.90 Sheep, fat ...... 0.15 [65 FR 38774, June 22, 2000, as amended at 77 Sheep, liver ...... 1.50 FR 72226, Dec. 5, 2012]

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§ 180.560 Cloquintocet-mexyl; toler- in or on the commodities in the table ances for residues. below. Compliance with the tolerance (a) General. Tolerances are estab- levels specified below is to be deter- lished for residues of the inert ingre- mined by measuring only those dient cloquintocet-mexyl, including its acibenzolar-S-methyl residues convert- metabolites and degradates, in or on ible to benzo(1,2,3)thiadiazole-7-car- the commodities in the following table boxylic acid (CGA–210007), expressed as when used as a safener in pesticide for- the stoichiometric equivalent of mulations containing the active ingre- acibenzolar-S-methyl, in or on the fol- dients clodinafop-propargyl (wheat lowing raw agricultural commodities. only), dicamba (wheat only), Parts per flucarbazone-sodium (wheat only), Commodity million halauxifen-methyl (wheat or barley), pinoxaden (wheat or barley), Banana 1 ...... 0.1 pyroxsulam (wheat or teff), florasulam Berry, low growing, subgroup 13–07G ...... 0.15 (teff), or fluroxypyr 1-methylheptyl Fruit, citrus, group 10–10 ...... 0.02 ester (teff). Compliance with the toler- Fruit, pome, group 11–10 ...... 0.03 Onion, bulb, subgroup 3–07A ...... 0.1 ance levels specified is to be deter- Spinach ...... 1.0 mined by measuring the combined resi- Tomato, paste ...... 3.0 dues of cloquintocet-mexyl, (acetic Vegetable, brassica, leafy, group 5 ...... 1.0 acid [(5-chloro-8-quinolinyl)oxy]-, 1- Vegetable, cucurbit, group 9 ...... 2.0 methylhexyl ester; CAS Reg. No. 99607– Vegetable, fruiting, group 8 ...... 1.0 70–2) and its acid metabolite (5-chloro- Vegetable, leafy, group 4 ...... 0.25 8-quinolinoxyacetic acid), expressed as 1 There are no United States registrations for banana. cloquintocet-mexyl, in or on the fol- (2) Tolerances are established for res- lowing commodities: idues of acibenzolar- S -methyl, benzo(1,2,3)thiadiazole-7-carbothioic Commodity Parts per million acid- S -methyl ester, including its me- Barley, grain ...... 0.1 tabolites and degradates, in or on the Barley, hay ...... 0.1 commodities in the table below. Com- Barley, straw ...... 0.1 pliance with the tolerance levels speci- Teff, forage 1 ...... 0.2 Teff, grain 1 ...... 0.1 fied below is to be determined by meas- Teff, hay 1 ...... 0.5 uring only those acibenzolar- S -methyl Teff, straw 1 ...... 0.1 residues convertible to Wheat, forage ...... 0.2 Wheat, grain ...... 0.1 benzo(1,2,3)thiadiazole-7-carboxylic Wheat, hay ...... 0.5 acid (CGA–210007), expressed as the Wheat, straw ...... 0.1 Stoichiometric equivalent of 1 There are no U.S. registrations for use on this commodity acibenzolar- S -methyl, in or on the fol- as of March 22, 2017. lowing raw agricultural commodities. (b) Section 18 emergency exemptions. [Reserved] Expiration/ Commodity Parts per revocation (c) Tolerances with regional registra- million date tions. [Reserved] (d) Indirect or inadvertent residues. Apple ...... 0.05 12/31/15 [Reserved] Grapefruit ...... 0.05 12/31/15 Pear ...... 0.05 12/31/15 [65 FR 38764, June 22, 2000, as amended at 70 FR 74688, Dec. 16, 2005; 73 FR 11820, Mar. 5, (b) Section 18 emergency exemptions. 2008; 75 FR 16020, Mar. 31, 2010; 76 FR 38035, [Reserved] June 29, 2011; 81 FR 50634, Aug. 2, 2016; 82 FR 14623, Mar. 22, 2017; 83 FR 45843, Sept. 11, 2018] (c) Tolerances with regional registrations. [Reserved] § 180.561 Acibenzolar-S-methyl; toler- (d) Indirect or inadvertent residues. ances for residues. [Reserved] (a) General. (1) Tolerances are estab- [65 FR 50446, Aug. 18, 2000, as amended at 70 lished for residues of acibenzolar-S- FR 7861, Feb. 16, 2005; 71 FR 76200, Dec. 20, methyl, benzo(1,2,3)thiadiazole-7- 2006; 74 FR 24710, May 26, 2009; 76 FR 34886, carbothioic acid-S-methyl ester, in- June 15, 2011; 77 FR 21676, Apr. 11, 2012; 77 FR cluding its metabolites and degradates, 30406, May 23, 2012; 80 FR 58620, Sept. 30, 2015]

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§ 180.562 Flucarbazone-sodium; toler- (b) Section 18 emergency exemptions. ances for residues. [Reserved] (a) General. Tolerances are estab- (c) Tolerances with regional registra- lished for combined residues of the her- tions. [Reserved] bicide flucarbazone-sodium, 4,5- (d) Indirect of inadvertent residues. dihydro-3-methoxy-4-methyl-5-oxo-N- [Reserved] [[2(trifluoromethoxy)phenyl] sulfonyl]- [65 FR 57972, Sept. 27, 2000, as amended at 66 1H-1,2,4-triazole 1-carboxamide, sodium FR 18207, Apr. 6, 2001; 67 FR 35050, May 17, salt) and its N-desmethyl metabolite; 2002] and its metabolites converted to 2- (trifluoromethoxy)benzene sulfonamide § 180.564 Indoxacarb; tolerances for residues. and calculated as flucarbazone-sodium in or on the following food commod- (a) General. (1) Tolerances are estab- ities: lished for residues of indoxacarb, including its metabolites and degradates, Commodity Parts per in or on the commodities in the table million below. Compliance with the tolerance Cattle, liver ...... 1.50 levels specified below is to be deter- Cattle, meat ...... 0.01 mined by measuring only indoxacarb, Cattle, meat byproducts, except liver ...... 0.01 (S)-methyl 7-chloro-2,5-dihydro-2-[[(me- Goat, liver ...... 1.50 Goat, meat ...... 0.01 thoxycarbonyl)[4- Goat, meat byproducts, except liver ...... 0.01 (trifluoromethoxy)phenyl] Hog, liver ...... 1.50 amino]carbonyl]indeno[1,2-e] Hog, meat ...... 0.01 [1,3,4][oxadiazine-4a(3H)-carboxylate, Hog, meat byproducts, except liver ...... 0.01 and its R-enantiomer, (R)-methyl 7- Horse, liver ...... 1.50 Horse, meat ...... 0.01 chloro-2,5-dihydro-2-[[(methoxycar- Horse, meat byproducts, except liver ...... 0.01 bonyl)[4- Milk ...... 0.005 (trifluoromethoxy)phenyl]amino]car- Sheep, liver ...... 1.50 bonyl]indeno[1,2-e][1,3,4][oxadiazine- Sheep, meat ...... 0.01 Sheep, meat byproducts, except liver ...... 0.01 4a(3H)-carboxylate. Wheat, forage ...... 0.30 Wheat, grain ...... 0.01 Parts per Commodity million Wheat, hay ...... 0.10 Wheat, straw ...... 0.05 Apple, wet pomace ...... 3.0 Alfalfa, forage ...... 10 (b) Section 18 emergency exemptions. Alfalfa, hay ...... 50 Bean, dry, seed ...... 0.2 [Reserved] Bean, succulent ...... 0.9 (c) Tolerances with regional registra- Beet, garden, roots ...... 0.30 tions. [Reserved] Beet, garden, tops ...... 6.0 Berry, low growing, except strawberry, subgroup (d) Indirect or inadvertant residues. 13–07H ...... 1 [Reserved] Bushberry subgroup 13–07B ...... 1.5 Cattle, fat ...... 1.5 [70 FR 67915, Nov. 9, 2005, as amended at 71 Cattle, meat ...... 0.05 FR 76931, Dec. 22, 2006] Cattle, meat byproducts ...... 0.03 Corn, field, forage ...... 6.0 Corn, field, grain ...... 0.02 § 180.563 Ethametsulfuron-methyl; tol- Corn, field, stover ...... 15 erances for residues. Corn, pop, grain ...... 0.02 (a) General. A tolerance is established Corn, pop, stover ...... 15 Corn, sweet, forage ...... 10 for residues of ethametsulfuron methyl Corn, sweet, kernel plus cob with husk removed 0.02 (methyl 2- ((((4-ethoxy-6- Corn, sweet, stover ...... 15 (methylamino)-1,3,5- triazin-2-yl) Cotton, gin byproducts ...... 15 Cotton, undelinted seed ...... 2.0 amino) carbonyl) amino) sulfonyl) ben- Cowpea, forage ...... 50 zoate) in or on the following raw agri- Cowpea, hay ...... 100 cultural commodities. Fruit, pome, except pear, group 11 ...... 1.0 Fruit, small vine climbing, except fuzzy kiwifruit, Parts per subgroup 13–07F ...... 2 Commodity million Fruit, stone, group 12 ...... 0.90 Goat, fat ...... 1.5 Canola, seed ...... 0.02 Goat, meat ...... 0.05 Crambe, seed ...... 0.02 Goat, meat byproducts ...... 0.03 Rapeseed, seed ...... 0.02 Grain, aspirated fractions ...... 45 Grape, raisin ...... 5.0

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2-carboxylate; and IN–KB687, methyl Commodity Parts per million [4- Hog, fat ...... 1.5 (trifluoromethoxy)phenyl]carbamate, Hog, meat ...... 0.05 calculated as the stoichiometric equiv- Hog, meat byproducts ...... 0.03 Horse, fat ...... 1.5 alent of indoxacarb in the commodity. Horse, meat ...... 0.05 Horse, meat byproducts ...... 0.03 Commodity Parts per Milk ...... 0.15 million Milk, fat ...... 4.0 Okra ...... 0.50 Egg ...... 0.20 Pea, southern, seed ...... 0.10 Poultry, fat ...... 0.20 Peanut ...... 0.01 Poultry, meat ...... 0.06 Peanut, hay ...... 40 Poultry, meat byproducts ...... 0.06 Pear ...... 0.20 Pear, oriental ...... 0.20 Peppermint, tops ...... 11 (b) Section 18 emergency exemptions. Sheep, fat ...... 1.5 Time-limited tolerances specified in Sheep, meat ...... 0.05 the following table are established for Sheep, meat byproducts ...... 0.03 Soybean, hulls ...... 4.0 residues of the indoxacarb, including Soybean, seed ...... 0.80 its metabolites and degradates, in or Spearmint, tops ...... 11 on the specified agricultural commod- Turnip, greens ...... 12 Vegetable, Brassica, leafy, group 5 ...... 12 ities in the table below, resulting from Vegetable, cucurbit, group 9 ...... 0.60 use of the pesticide pursuant to FIFRA Vegetable, fruiting, group 8 ...... 0.50 section 18 emergency exemptions. Com- Vegetable, leafy, except Brassica, group 4 ...... 14 Vegetable, tuberous and corm, subgroup 1-C ...... 0.01 pliance with the tolerance levels specified in the table below is to be deter- (2) Tolerances are established for res- mined by measuring only indoxacarb, idues of indoxacarb, including its me- (S)-methyl 7-chloro-2,5-dihydro-2-[[(metabolites and degradates, in or on the thoxycarbonyl)[4- commodities in the table below. Com- (trifluoromethoxy)phenyl] pliance with the tolerance levels speci- amino]carbonyl]indeno[1,2-e] fied below is to be determined by meas- [1,3,4][oxadiazine-4a(3H)-carboxylate, uring only the sum of indoxacarb, (S)- and its R-enantiomer, (R)-methyl 7- methyl-7-chloro-2,5-dihydro-2-[[(me- chloro-2,5-dihydro-2-[[(methoxycar- thoxycarbonyl)[4-(trifluoromethoxy)- bonyl)[4-(trifluoromethoxy)phenyl] phenyl]amino]carbonyl]indeno[1,2e] amino]carbonyl]indeno[1,2-e] [1,3,4]oxadiazine-4a(3H)-carboxylate, its [1,3,4][oxadiazine-4a(3H)-carboxylate. R-enantiomer, (R)-methyl 7-chloro-2,5- The tolerances expire on the dates dihydro-2-[[(methoxycarbonyl)[4- specified in the table. (trifluoromethoxy) phenyl]amino]carbonyl]indeno [1,2-e] [1,3,4] oxadiazine-4a(3H)-carboxylate, and the metabolites: IN–JT333, methyl Commodity Parts per Expiration 7-chloro-2,5-dihydro-2-[[[4- million date (trifluoromethoxy)phenyl]- Grass, forage ...... 10 12/31/2022 amino]carbonyl]indeno[1,2- Grass, hay ...... 50 12/31/2022 e][1,3,4]oxadiazine-4a(3H)-carboxylate; IN–KT319, (E)-methyl 5-chloro-2,3,- (c) Tolerances with regional registra- dihydro-2-hydroxy-1-[[[(methoxycar- tions. [Reserved] bonyl)[4- (d) Indirect or inadvertent residues. (trifluoromethoxy)phenyl]amino]-car- [Reserved] bonyl]hydrazono]-1H-indene-2- carboxylate; IN–JU873, methyl 5- [65 FR 58424, Sept. 29, 2000, as amended at 67 chloro-2,3-dihydro-2-hydroxy-1-[[[[4- FR 41807, June 19, 2002; 67 FR 47309, July 18, (triflurormethoxy)- 2002; 67 FR 58730, Sept. 18, 2002; 68 FR 25830, May 14, 2003; 68 FR 27746, May 21, 2003; 69 FR phenyl]amino]carbonyl]hydrazono]-1H- 28842, May 19, 2004; 69 FR 29459, May 24, 2004; indene-2-carboxylate; IN–KG433, meth- 69 FR 32282, June 9, 2004; 72 FR 37641, July 11, yl 5-chloro-2,3,-dihydro-2-hydroxy-1- 2007; 74 FR 33165, July 10, 2009; 77 FR 8749, [[[(methoxycarbonyl)[4- Feb. 15, 2012; 78 FR 78738, Dec. 27, 2013; 82 FR (trifluoromethoxy)phenyl] 57866, Dec. 8, 2017; 84 FR 32094, July 5, 2019; 85 amino]carbonyl]-hydrazono]-1H-indene- FR 31389, May 26, 2020]

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§ 180.565 Thiamethoxam; tolerances Commodity Parts per for residues. million (a) General. Tolerances are estab- Goat, meat byproducts ...... 0.04 lished for residues of the insecticide Grain, aspirated fractions ...... 2.0 Grain, cereal, group 15, except barley ...... 0.02 thiamethoxam, including its metabo- Grape, raisin ...... 0.30 lites and degradates, in or on the fol- Hog, meat ...... 0.02 lowing commodities. Compliance with Hog, meat byproducts ...... 0.02 Hop, dried cones ...... 0.10 the tolerance levels specified below is Horse, meat ...... 0.02 to be determined by measuring only Horse, meat byproducts ...... 0.04 thiamethoxam 3-[(2-chloro-5- Mango ...... 0.40 Milk ...... 0.02 thiazolyl)methyl]tetrahydro-5-methyl- Millet, pearl, forage ...... 0.02 N-nitro-4H-1,3,5-oxadiazin-4-imine and Millet, pearl, stover ...... 0.02 its metabolite CGA–322704 N-[(2-chloro- Millet, proso, forage ...... 0.02 thiazol-5-yl)methyl]-N′-methyl-N″- Millet, proso, stover ...... 0.02 Millet, proso, straw ...... 0.02 nitro-guanidine, calculated as the stoi- Mustard, seed ...... 0.02 chiometric equivalent of Nut, tree, group 14 ...... 0.02 thiamethoxam, in or on the following Oat, forage ...... 0.50 Oat, hay ...... 0.02 commodities: Oat, straw ...... 0.02 Onion, dry bulb ...... 0.03 Parts per Papaya ...... 0.40 Commodity million Peanut ...... 0.05 Alfalfa, forage ...... 0.05 Peanut, hay ...... 0.25 Alfalfa, hay ...... 0.12 Peanut, meal ...... 0.15 Almond, hulls ...... 1.2 Peppermint, tops ...... 1.5 Artichoke, globe ...... 0.45 Pistachio ...... 0.02 Avocado ...... 0.40 Potato ...... 0.25 Banana 1 ...... 0.03 Radish, tops ...... 0.80 Barley, grain ...... 0.4 Rapeseed, seed ...... 0.02 Barley, hay ...... 0.40 Rye, forage ...... 0.50 Barley, straw ...... 0.40 Rye, straw ...... 0.02 Bean, succulent ...... 0.02 Safflower, seed ...... 0.02 Berry, low growing, subgroup 13–07G, except Sapodilla ...... 0.40 cranberry ...... 0.30 Sapote, black ...... 0.40 Borage, seed ...... 0.02 Sapote, mamey ...... 0.40 Brassica, head and stem, subgroup 5–A ...... 4.5 Sheep, meat ...... 0.02 Brassica, leafy greens, subgroup 5–B ...... 3.0 Sheep, meat byproducts ...... 0.04 Buckwheat, forage ...... 0.50 Sorghum, forage ...... 0.02 Buckwheat, hay ...... 0.02 Sorghum, grain, stover ...... 0.02 Buckwheat, straw ...... 0.02 Soybean, hulls ...... 0.08 Bushberry subgroup 13–07B, except lingonberry Spearmint, tops ...... 1.5 and blueberry, lowbush ...... 0.20 Star apple ...... 0.40 Caneberry subgroup 13–07A ...... 0.35 Sunflower ...... 0.02 Canistel ...... 0.40 Tea, dried 1 ...... 20 Canola, seed ...... 0.02 Tomato, paste ...... 0.80 Cattle, meat ...... 0.02 Vegetable, cucurbit, group 9 ...... 0.2 Cattle, meat byproducts ...... 0.04 Vegetable, fruiting, group 8 ...... 0.25 Citrus, dried pulp ...... 0.60 Vegetable, leafy, except brassica, group 4 ...... 4.0 Coffee, green, bean 1 ...... 0.20 Vegetable, legume, group 6 ...... 0.02 Corn, field, forage ...... 0.10 Vegetable, root, subgroup 1A ...... 0.05 Corn, field, stover ...... 0.05 Vegetable, tuberous and corm, except potato, Corn, pop, forage ...... 0.10 subgroup 1D ...... 0.02 Corn, pop, stover ...... 0.05 Wheat, forage ...... 0.50 Corn, sweet, forage ...... 0.10 Wheat, hay ...... 0.02 Corn, sweet, kernel plus cob with husks removed 0.02 Wheat, straw ...... 0.02 Corn, sweet, stover ...... 0.05 1 Cotton, gin byproducts ...... 1.5 There are no U.S. registrations for these commodities as of February 15, 2017. Cotton, undelinted seed ...... 0.10 Crambe, seed ...... 0.02 (b) Section 18 emergency exemptions. Cranberry ...... 0.02 Flax, seed ...... 0.02 Time-limited tolerances specified in Food commodities and feed commodities (other the table are established for residues of than those covered by a higher tolerance as a the insecticide thiamethoxam, includ- result of use on growing crops) in food/feed ing its metabolites and degradates. handling establishments ...... 0.02 Fruit, citrus, group 10 ...... 0.40 Compliance with the tolerance levels Fruit, pome, group 11 ...... 0.2 specified below is to be determined by Fruit, small, vine climbing, subgroup 13–07F, ex- measuring only thiamethoxam 3-[(2- cept fuzzy kiwifruit ...... 0.20 Fruit, stone, group 12 ...... 0.5 chloro-5-thiazolyl)methyl]tetrahydro- Goat, meat ...... 0.02 5-methyl-N-nitro-4H–1,3,5-oxadiazin-4-

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imine and its metabolite CGA–322704 N- TABLE 1 OF PARAGRAPH (a)(1)—Continued [(2-chloro-thiazol-5-yl)methyl]-N′- ″ Parts per methyl-N -nitro-guanidine, calculated Commodity million as the stoichiometric equivalent of thiamethoxam, in or on the specified Corn, field, forage ...... 2.0 agricultural commodities, resulting Corn, field, grain ...... 0.02 Corn, field, refined oil ...... 0.05 from use of the pesticide pursuant to Corn, field, stover ...... 7.0 FFIFRA section 18 emergency exemp- Corn, pop, forage ...... 2.0 tions. The tolerances expire on the Corn, pop, grain ...... 0.02 date specified in the table. Corn, pop, stover ...... 7.0 Cotton, gin byproducts ...... 10 Cottonseed subgroup 20C ...... 0.1 Commodity Parts per Expiration million date Cowpea, succulent shelled ...... 0.4 Crowder pea, succulent shelled ...... 0.4 Rice, grain ...... 6 12/31/2024 Fruit, citrus, group 10–10 ...... 1.0 Rice, straw ...... 2 12/31/2024 Fruit, pome, group 11–10 ...... 0.30 Fruit, small, vine climbing, except fuzzy kiwifruit, (c) Tolerances with regional registra- subgroup 13–07F ...... 1.0 tions. [Reserved] Fruit, stone, group 12–12 ...... 2.0 (d) Indirect or inadvertent residues. Goa bean, pods, succulent shelled ...... 0.4 [Reserved] Grain, aspirated fractions ...... 0.40 Hop, dried cones ...... 10 [65 FR 79762, Dec. 20, 2000] Lablab bean, succulent shelled ...... 0.4 Leaf petiole vegetable subgroup 22B ...... 4 EDITORIAL NOTE: For FEDERAL REGISTER ci- Lima bean, succulent shelled ...... 0.4 tations affecting § 180.565, see the List of CFR Melon subgroup 9A ...... 0.10 Sections Affected, which appears in the Nut, tree, group 14–12 ...... 0.1 Finding Aids section of the printed volume Peanut ...... 0.04 and at www.govinfo.gov. Peanut, hay ...... 30 Peppermint, tops ...... 7.0 § 180.566 Fenpyroximate; tolerances Sapodilla ...... 0.15 for residues. Sapote, mamey ...... 0.15 Southern pea, succulent shelled ...... 0.4 (a) General. (1) Tolerances are estab- Soybean, edible, succulent shelled ...... 0.4 lished for residues of the insecticide Spearmint, tops ...... 7.0 fenpyroximate, including its metabo- Squash/cucumber subgroup 9B ...... 0.4 lites and degradates, in or on the com- Succulent bean, succulent shelled ...... 0.4 modities in the table below. Compli- Tea, dried 1 ...... 20 Tropical and subtropical, medium to large fruit, ance with the tolerance levels specified smooth, inedible peel subgroup 24B, except in the table is to be determined by banana ...... 0.6 measuring only the sum of Vegetable, fruiting, group 8–10 ...... 0.20 fenpyroximate, (E)-1,1-dimethylethyl 4- Vegetable, tuberous and corm, subgroup 1C ..... 0.10 [[[[(1,3-dimethyl-5-phenoxy-1H-pyrazol- Velvet bean, succulent shelled ...... 0.4 4-yl)methylene]amino]oxy]methyl]ben- 1 There are no U.S. Registrations. zoate and its Z-isomer, (Z)-1,1- (2) Tolerances are established for res- dimethylethyl 4-[[[[(1,3-dimethyl-5- idues of the insecticide fenpyroximate, phenoxy-1H-pyrazol-4-yl)methylene] including its metabolites and amino]oxy]methyl]benzoate, calculated degradates, in or on the commodities as the stoichiometric equivalent of in the table below. Compliance with fenpyroximate. the tolerance levels specified in the table is to be determined by measuring TABLE 1 OF PARAGRAPH (a)(1) only the sum of fenpyroximate, (E)-1,1- dimethylethyl 4-[[[[(1,3-dimethyl-5- Commodity Parts per million phenoxy-1H-pyrazol-4-yl)methylene] Almond, hulls ...... 3.0 amino]oxy]methyl]benzoate and its Banana ...... 1 metabolites (E)-4-[(1,3-dimethyl-5- Bean, snap, succulent ...... 0.40 phenoxypyrazol-4-yl)-methylene Berry, low growing, subgroup 13–07G ...... 1.0 Blackeyed pea, succulent shelled ...... 0.4 aminooxymethyl]benzoic acid and (E)- Broad bean, succulent shelled ...... 0.4 1,1-dimethylethyl-2-hydroxyethyl 4- Bushberry subgroup 13–07B ...... 3 [[[[(1,3-dimethyl-5-phenoxy-1H-pyrazol- Caneberry subgroup 13–07A ...... 3 4-yl)methylene]amino]oxy]methyl]ben- Chickpea, succulent shelled ...... 0.4 Citrus, dried pulp ...... 4.0 zoate, calculated as the stoichiometric Citrus, oil ...... 15 equivalent of fenpyroximate.

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TABLE 2 OF PARAGRAPH (a)(2) § 180.567 Zoxamide; tolerances for residues. Parts per Commodity million (a) General. (1) Tolerances are established for residues of zoxamide includ- Cattle, fat ...... 0.1 Cattle, meat ...... 0.03 ing metabolites and degradates, in or Cattle, meat byproducts, except kidney and liver 0.03 on the commodities in the table below. Goat, fat ...... 0.1 Compliance with the tolerance levels Goat, meat ...... 0.03 specified below is to be determined by Goat, meat byproducts, except kidney and liver 0.03 measuring only zoxamide (3,5-dichloro- Horse, fat ...... 0.1 Horse, meat ...... 0.03 N-(3-chloro-1-ethyl-1-methyl-2- Horse, meat byproducts, except kidney and liver 0.03 oxopropyl)-4-methylbenzamide). Milk ...... 0.015 Sheep, fat ...... 0.1 Commodity Parts per Sheep, meat ...... 0.03 million Sheep, meat byproducts, except kidney and Banana 1 ...... 0.20 liver ...... 0.03 Fruit, small vine climbing, except fuzzy kiwifruit, subgroup 13–07F ...... 5.0 (3) Tolerances are established for res- Grape, raisin ...... 15.0 idues of the insecticide fenpyroximate, Pepper/Eggplant Subgroup 8–10B ...... 1.0 including its metabolites and Tomato subgroup 8–10A ...... 2.0 degradates, in or on the commodities Vegetable, cucurbit, group 9 ...... 1.0 in the table below. Compliance with 1 There are no U.S. registrations allowing use of zoxamide the tolerance levels specified in the on banana as of February 9, 2018. table is to be determined by measuring (2) Tolerances are established for res- only the sum of fenpyroximate, (E)-1,1- idues of zoxamide including metabo- dimethylethyl 4-[[[[(1,3-dimethyl-5- lites and degradates, in or on the com- phenoxy-1H-pyrazol-4-yl)methylene] modities in the table below. Compli- amino]oxy]methyl]benzoate and its ance with the tolerance levels specified metabolite (E)-4-[(1,3-dimethyl-5- below is to be determined by measuring phenoxypyrazol-4-yl)-methylene only the sum of zoxamide (3,5-dichloro- aminooxymethyl]benzoic acid, cal- N-(3-chloro-1-ethyl-1-methyl-2- culated as the stoichiometric equiva- oxopropyl)-4-methylbenzamide) and its lent of fenpyroximate. metabolites 3,5-dichloro-1,4- benzenedicarboxylic acid (RH–1455 and TABLE 3 OF PARAGRAPH (a)(3) RH–141455) and 3,5-dichloro-4- hydroxymethylbenzoic acid (RH–1452 Parts per Commodity million and RH–141452) calculated as the stoichiometric equivalent of zoxamide. Cattle, kidney ...... 0.5 Cattle, liver ...... 0.7 Parts per Goat, kidney ...... 0.5 Commodity million Goat, liver ...... 0.7 Horse, kidney ...... 0.5 Ginseng ...... 0.30 Horse, liver ...... 0.7 Onion, bulb, subgroup 3–07A ...... 0.7 Sheep, kidney ...... 0.5 Potato, granules/flakes ...... 0.30 Sheep, liver ...... 0.7 Potato, wet peel ...... 0.10 Vegetable, tuberous and corm, subgroup 1C ...... 0.06 (b) Section 18 emergency exemptions. [Reserved] (b) Section 18 emergency exemptions. (c) Tolerances with regional registra- [Reserved] tions. [Reserved] (c) Tolerances with regional registra- (d) Indirect or inadvertent residues. tions. [Reserved] [Reserved] (d) Indirect or inadvertent residues. [Reserved] [66 FR 18568, Apr. 10, 2001, as amended at 69 FR 32464, June 10, 2004; 71 FR 49368, Aug. 23, [66 FR 18733, Apr. 11, 2001, as amended at 66 2006; 72 FR 26321, May 9, 2007; 74 FR 37617, FR 49118, Sept. 26, 2001; 69 FR 16805, Mar. 31, July 29, 2009; 74 FR 63079, Dec. 2, 2009; 75 FR 2004; 71 FR 31104, June 1, 2006; 71 FR 76200, 80346, Dec. 22, 2010; 77 FR 73951, Dec. 12, 2012; Dec. 20, 2006; 75 FR 770, Jan. 6, 2010; 79 FR 78 FR 36097, June 17, 2013; 82 FR 34875, July 41915, July 18, 2014; 81 FR 12015, Mar. 8, 2016; 27, 2017; 84 FR 66625, Dec. 5, 2019; 85 FR 36758, 83 FR 5719, Feb. 9, 2018; 84 FR 12524, Apr. 2, June 18, 2020] 2019]

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§ 180.568 Flumioxazin; tolerances for dihydro-3-oxo-4-(2-propynyl)-2H-1,4- residues. benzoxazin-6-yl]-4,5,6,7-tetrahydro-1H- (a) General. Tolerances are estab- isoindole-1,3(2H)-dione, including its lished for residues of flumioxazin, 2-[7- metabolites and degradates, in or on fluoro-3,4-dihydro-3-oxo-4-(2-propynyl)- the commodities in the table below. 2H-1,4-benzoxazin-6-yl]-4,5,6,7- Compliance with the tolerance levels tetrahydro-1H-isoindole-1,3(2H)-dione, specified below is to be determined by including its metabolites and measuring only flumioxazin. degradates, in or on the commodities Parts per in the table below. Compliance with Commodity million the tolerance levels specified below is Clover, forage ...... 0.02 to be determined by measuring only Clover, hay ...... 0.15 flumioxazin. Grass, forage ...... 0.40 Grass, hay ...... 0.05 Commodity Parts per million (d) Indirect or inadvertent residues. Alfalfa, forage ...... 3.0 [Reserved] Alfalfa, hay ...... 8.0 Almond, hulls ...... 0.70 [81 FR 91851, Dec. 19, 2016, as amended at 83 Artichoke, globe ...... 0.02 FR 50288, Oct. 5, 2018] Asparagus ...... 0.02 Berry, low growing, subgroup 13–07G ...... 0.07 § 180.569 Forchlorfenuron; tolerances Bushberry subgroup 13–07B ...... 0.02 for residues. Caneberry, subgroup 13–07A ...... 0.50 Citrus, group 10–10 ...... 0.02 (a) General. (1) Tolerances are estab- Citrus, oil ...... 0.1 lished for residues of forchlorfenuron, Corn, field, forage ...... 0.02 including its metabolites and Corn, field, grain ...... 0.02 Corn, field, stover ...... 0.02 degradates, in or on the commodities Cotton, gin byproducts ...... 0.60 in the table below. Compliance with Cotton, undelinted seed ...... 0.02 the tolerance levels specified below is Fish, freshwater ...... 1.5 Fruit, pome, group 11–10 ...... 0.02 to be determined by measuring only Fruit, small vine climbing, except for fuzzy forchlorfenuron (N-(2-chloro-4- kiwifruit, subgroup 13–07F ...... 0.02 pyridinyl)-N-phenylurea). Fruit, stone, group 12–12 ...... 0.02 Grain, aspirated fractions ...... 100 Parts per Hop, dried cones ...... 0.05 Commodity million Leaf petioles subgroup 4B ...... 0.02 Nut, tree, group 14–12 ...... 0.02 Almond ...... 0.01 Olive ...... 0.02 Almond, hulls ...... 0.15 Onion, bulb subgroup 3–07A ...... 0.02 Bushberry subgroup 13–07B ...... 0.01 Pea and bean, dried shelled, except soybean, Cherry, sweet ...... 0.01 subgroup 6C ...... 0.07 Fig ...... 0.01 Peanut ...... 0.02 Grape ...... 0.03 Peppermint, tops ...... 0.04 Grape, raisin ...... 0.06 Pomegranate ...... 0.02 Kiwifruit ...... 0.04 Prickly pear, fruit ...... 0.07 Pear ...... 0.01 Prickly pear, pads ...... 0.06 Pistachio ...... 0.01 Rapeseed subgroup 20A ...... 0.40 Plum, prune, fresh ...... 0.01 Soybean forage ...... 0.03 Soybean hay ...... 0.02 (2) Temporary tolerances are estab- Soybean, seed ...... 0.02 Spearmint, tops ...... 0.04 lished for residues of forchlorfenuron, Sugarcane, cane ...... 0.20 including its metabolites and Sunflower subgroup 20B ...... 0.50 degradates, in or on the commodities Vegetable, brassica, head and stem, group 5–16 0.02 Vegetable, cucurbit, group 9 ...... 0.03 in the table below. Compliance with Vegetable, fruiting, group 8–10 ...... 0.02 the tolerance levels specified below is Vegetable, tuberous and corm, subgroup 1C ...... 0.02 to be determined by measuring on Wheat, forage ...... 0.02 Wheat, grain ...... 0.40 forchlorfenuron (N-(2-chloro-4- Wheat, hay ...... 0.02 pyridinyl)-N′-phenylurea). Wheat, straw ...... 6.0 Parts per Expiration/ Commodity revocation (b) Section 18 emergency exemptions. million date [Reserved] (c) Tolerances with regional registra- Almond ...... 0.01 12/31/15 Almond, hulls ...... 0.15 12/31/15 tions. Tolerances are established for Cherry, sweet ...... 0.01 12/31/15 residues of flumioxazin, 2-[7-fluoro-3,4- Fig ...... 0.01 12/31/15

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(d) Indirect or inadvertent residues. Parts per Expiration/ Commodity revocation [Reserved] million date [66 FR 33187, June 21, 2001, as amended at 66 Pear ...... 0.01 12/31/15 Pistachio ...... 0.01 12/31/15 FR 40141, Aug. 2, 2001; 67 FR 12878, Mar. 20, Plum, prune, fresh ...... 0.01 12/31/15 2002; 69 FR 29890, May 26, 2004; 72 FR 63997, Nov. 14, 2007; 80 FR 72599, Nov. 20, 2016] (b) Section 18 emergency exemptions. [Reserved] § 180.571 Mesotrione; tolerances for (c) Tolerances with regional restric- residues. tions. [Reserved] (a) General. Tolerances are estab- (d) Indirect or inadvertent residues. lished for residues of the herbicide [Reserved] mesotrione, including its metabolites [66 FR 22936, May 7, 2001, as amended at 69 and degradates, in or on the commod- FR 48805, Aug. 11, 2004; 69 FR 58322, Sept. 30, ities in the table below. Compliance 2004; 73 FR 47846, Aug. 15, 2008; 78 FR 46283, with the tolerance levels specified July 31, 2013; 79 FR 18471, Apr. 2, 2014] below is to be determined by measuring only mesotrione, 2-[4-(methylsulfonyl)- § 180.570 Isoxadifen-ethyl; tolerances 2-nitrobenzoyl]-1,3-cyclohexanedione, for residues. in or on the following raw agricultural (a) General. (1) Tolerances are estab- commodities: lished for residues of isoxadifen-ethyl (ethyl 5,5-diphenyl-2-isoxazoline-3- Parts per Commodity million carboxylate, (CAS No. 163520–33–0), and its metabolite: 4,5-dihydro-5,5-di- Almond, hulls ...... 0.02 phenyl-3-isoxazolecarboxylic acid, Asparagus ...... 0.01 when used as an inert ingredient Berry, group 13 ...... 0.01 Corn, field, forage ...... 0.01 (safener) in or on the following raw ag- Corn, field, grain ...... 0.01 ricultural commodities: Corn, field, stover ...... 0.01 Corn, pop, grain ...... 0.01 Commodity Parts per Corn, pop, stover ...... 0.01 million Corn, sweet, forage ...... 0.5 Corn, sweet, kernel plus cob with husks removed 0.01 Corn, field, forage ...... 0.20 Corn, sweet, stover ...... 1.5 Corn, field, grain ...... 0.08 Corn, field, stover ...... 0.40 Cranberry ...... 0.02 Corn, oil ...... 0.50 Flax, seed ...... 0.01 Corn, pop, grain ...... 0.04 Fruit, citrus, group 10–10 ...... 0.01 Corn, pop, stover ...... 0.25 Fruit, pome, group 11–10 ...... 0.01 Corn, sweet, forage ...... 0.30 Fruit, stone, group 12–12 ...... 0.01 Corn, sweet, kernel plus cob with husk removed 0.04 Grass, forage ...... 0.01 Corn, sweet, stover ...... 0.45 Grass, hay ...... 0.01 Grass, seed screenings ...... 0.10 (2) Tolerances are established for the Grass, straw ...... 0.10 residues of isoxadifen-ethyl (3- Lingonberry ...... 0.01 Millet, forage ...... 0.01 isoxazolecarboxylic acid, 4,5-dihydro- Millet, grain ...... 0.01 5,5-diphenyl-, ethyl ester (CAS No. Millet, hay ...... 0.02 164520–33–0)), and its metabolites 4,5- Millet, straw ...... 0.02 dihydro-5,5-diphenyl-3- Nut, tree, group 14–12 ...... 0.01 Oat, forage ...... 0.01 isoxazolecarboxylic acid and b-hy- Oat, grain ...... 0.01 droxy-b-benzenepropanenitrile when Oat, hay ...... 0.01 used as an inert ingredient (safener) in Oat, straw ...... 0.01 or on the following raw agricultural Okra ...... 0.01 commodities: Rhubarb ...... 0.01 Sorghum, grain, forage ...... 0.01 Sorghum, grain, grain ...... 0.01 Parts per Commodity million Sorghum, grain, stover ...... 0.01 Sorghum, sweet ...... 0.01 Rice, grain ...... 0 .10 Soybean, seed ...... 0.01 Rice, hulls ...... 0 .50 Sugarcane, cane ...... 0.01

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(d) Indirect or inadvertent residues. Commodity Parts per [Reserved] million [66 FR 33195, June 21, 2001, as amended at 67 Passionfruit ...... 0.90 FR 45656, July 10, 2002; 68 FR 273, Jan. 3, 2003; Pea and bean, succulent shelled, subgroup 6B ... 0.70 Peppermint, tops ...... 25 69 FR 58310, Sept. 30, 2004; 70 FR 14551, Mar. Pistachio ...... 0.20 23, 2005; 72 FR 71802, Dec. 19, 2007; 73 FR 1512, Plum ...... 0.20 Jan. 9, 2008; 73 FR 9226, Feb. 20, 2008; 74 FR Pulasan ...... 5.0 67123, Dec. 18, 2009; 76 FR 34886, June 15, 2011; Rambutan ...... 5.0 80 FR 30630, May 29, 2015] Sapodilla ...... 7.0 Sapote, mamey ...... 7.0 Sheep, fat ...... 0.10 § 180.572 Bifenazate; tolerance for resi- Soursop ...... 1.6 dues. Soybean, succulent shelled ...... 0.70 Spanish lime ...... 5.0 (a) General. (1) Tolerances are estab- Spearmint, tops ...... 25 lished for residues of bifenazate (1- Star apple ...... 7.0 methylethyl 2-(4-methoxy[1,1′- Starfruit ...... 0.90 Strawberry ...... 1.5 biphenyl]-3-yl)hydrazinecarboxylate) Sugar apple ...... 1.6 including its metabolites and Vegetable, cucurbit, group 9 ...... 0.75 degradates, in or on the commodities Vegetable, fruiting, group 8–10 ...... 4.0 Vegetable, legume, edible-podded, subgroup 6A 6.0 listed in the following table. Compli- Vegetable, tuberous and corm, subgroup 1C ...... 0.10 ance with the tolerance levels specified Wax jambu ...... 0.90 are to be determined by measuring only the sum of bifenazate and its me- (2) Tolerances are established for res- tabolite, diazinecarboxylic acid, 2-(4- idues of bifenazate (1-methylethyl 2-(4- methoxy-[1,1′-biphenyl]-3-yl), 1- methoxy[1,1′-biphenyl]-3-yl) methylethyl ester, (calculated as the hydrazinecarboxylate) including its stoichiometric equivalent of metabolites and degradates, in or on bifenazate) in or on the following food the commodities listed in the following commodities: table. Compliance with the tolerance levels specified are to be determined by Parts per Commodity million measuring only the sum of bifenazate and its metabolites diazinecarboxylic Acerola ...... 0.90 acid, 2-(4-methoxy-[1,1′-biphenyl]-3-yl), Almond, hulls ...... 15 ′ Apple, wet pomace ...... 1.2 1-methylethyl ester; 1,1 -biphenyl, 4-ol; Atemoya ...... 1.6 and 1,1′-biphenyl, 4-oxysulfonic acid Avocado ...... 7.0 (calculated as the stoichiometric Bean, dry seed ...... 0.60 Berry, low-growing subgroup 13–07G ...... 1.5 equivalent of bifenazate) in or on the Biriba ...... 1.6 following food commodities: Black sapote ...... 7.0 Caneberry subgroup 13-07A ...... 5.0 Commodity Parts per Canistel ...... 7.0 million Cattle, fat ...... 0.10 Cherimoya ...... 1.6 Cattle, meat ...... 0.02 Cotton, gin byproducts ...... 35 Cattle, meat byproducts ...... 0.02 Cotton, undelinted seed ...... 0.75 Goat, meat ...... 0.02 Custard apple ...... 1.6 Goat, meat byproducts ...... 0.02 Feijoa ...... 0.90 Hog, meat ...... 0.02 Fruit, pome, group 11–10 ...... 0.7 Hog, meat byproducts ...... 0.02 Fruit, small, vine climbing subgroup 13–07F, ex- Horse, meat ...... 0.02 cept fuzzy kiwifruit ...... 1.0 Horse, meat byproducts ...... 0.02 Fruit, stone, group 12, except plum ...... 2.5 Milk ...... 0.02 Goat, fat ...... 0.10 Sheep, meat ...... 0.02 Grape ...... 0.75 Sheep, meat byproducts ...... 0.02 Grape, raisin ...... 1.2 Guava ...... 0.9 (b) Section 18 emergency exemptions. Herb, subgroup 19A, except chervil and chive ..... 300 [Reserved] Hog, fat ...... 0.10 Hop, dried cones ...... 15 (c) Tolerances with regional registra- Horse, fat ...... 0.10 tions. Tolerances with regional reg- Jaboticaba ...... 0.90 istration, as defined in § 180.1(l), are es- Ilama ...... 1.6 Longan ...... 5.0 tablished for residues of bifenazate (1- Lychee ...... 5.0 methylethyl 2-(4-methoxy[1,1′- Mango ...... 7.0 biphenyl]-3-yl)hydrazinecarboxylate) Nut, tree, group 14 ...... 0.20 Okra ...... 2.0 including its metabolites and Papaya ...... 7.0 degradates, in or on the commodities

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listed in the following table. Compli- the commodities in the table below. ance with the tolerance levels specified Compliance with the tolerance levels are to be determined by measuring specified below is to be determined by only the sum of bifenazate and its me- measuring only the combined residues tabolite, diazinecarboxylic acid, 2-(4- of tepraloxydim (2-[1-[[[(2E)-3-chloro-2- methoxy-[1,1′-biphenyl]-3-yl), 1- propen-1-yl]oxy]imino]propyl]-3-hy- methylethyl ester, (calculated as the droxy-5-(tetrahydro-2H-pyran-4-yl)-2- stoichiometric equivalent of cyclohexen-1-one) and its metabolites bifenazate) in or on the following food convertible to GP (3-(tetrahydropyran- commodities: 4-yl)pentane-1,5-dioic acid), OH–GP (3- hydroxy-3-(tetrahydropyran-4- Parts per Commodity million yl)pentane-1,5-dioic acid), and GL (3-(2- oxotetrahydropyran-4-yl)-1,5-dioic Timothy, forage ...... 200 Timothy, hay ...... 150 acid), calculated as tepraloxydim, in or on the commodities. (d) Indirect or inadvertent residues. Expiration/ [Reserved] Commodity Parts per revocation million date [66 FR 34569, June 29, 2001] Cattle, fat ...... 0.15 12/31/18 EDITORIAL NOTE: For FEDERAL REGISTER ci- Cattle, kidney ...... 0.50 12/31/18 tations affecting § 180.572, see the List of CFR Cattle, meat ...... 0.20 12/31/18 Sections Affected, which appears in the Cattle, meat byproducts, except kid- Finding Aids section of the printed volume ney ...... 0.20 12/31/18 and at www.govinfo.gov. Egg ...... 0.20 12/31/18 Goat, fat ...... 0.15 12/31/18 § 180.573 Tepraloxydim; tolerances for Goat, kidney ...... 0.50 12/31/18 residues. Goat, meat ...... 0.20 12/31/18 Goat, meat byproducts, except kid- (a) General. (1) Tolerances are estab- ney ...... 0.20 12/31/18 lished for residues of tepraloxydim, in- Hog, fat ...... 0.15 12/31/18 cluding its metabolites and degradates, Hog, kidney ...... 0.50 12/31/18 Hog, meat ...... 0.20 12/31/18 in or on the commodities in the table Hog, meat byproducts, except kid- below. Compliance with the tolerance ney ...... 0.20 12/31/18 levels specified below is to be deter- Horse, fat ...... 0.15 12/31/18 mined by measuring only the combined Horse, kidney ...... 0.50 12/31/18 Horse, meat ...... 0.20 12/31/18 residues of tepraloxydim, (2-[1-[[[(2E)-3- Horse, meat byproducts, except kid- chloro-2-propen-1-yl]oxy]imino]propyl]- ney ...... 0.20 12/31/18 3-hydroxy-5-(tetrahydro-2H-pyran-4-yl)- Milk ...... 0.10 12/31/18 2-cyclohexen-1-one) and its metabolites Poultry, fat ...... 0.30 12/31/18 Poultry, liver ...... 1.00 12/31/18 convertible to GP (3-(tetrahydropyran- Poultry, meat ...... 0.20 12/31/18 4-yl)pentane-1,5-dioic acid) and OH–GP Poultry, meat byproducts, except (3-hydroxy-3-(tetrahydropyran-4- liver ...... 0.20 12/31/18 yl)pentane-1,5-dioic acid), calculated as Sheep, fat ...... 0.15 12/31/18 Sheep, kidney ...... 0.50 12/31/18 tepraloxydim, in or on the commod- Sheep, meat ...... 0.20 12/31/18 ities. Sheep, meat byproducts, except kidney ...... 0.20 12/31/18 Expiration/ Commodity Parts per revocation million date (b) Section 18 emergency exemptions. [Reserved] Cotton, undelinted seed ...... 0.2 12/31/18 (c) Tolerances with regional registra- Cotton, gin byproducts ...... 3.0 12/31/18 Flax, seed ...... 0.10 12/31/18 tions. A tolerance with regional reg- Grain, aspirated fraction ...... 1200.0 12/31/18 istration, as defined in § 180.1(l), is es- Pea and bean, dried shelled, except tablished for residues of tepraloxydim, soybean, subgroup 6C 1 ...... 0.10 12/31/18 Soybean, seed ...... 6.0 12/31/18 including its metabolites and Soybean, hulls ...... 8.0 12/31/18 degradates, in or on the commodities Sunflower subgroup 20B 1 ...... 0.20 12/31/18 in the table below. Compliance with 1 There are no U.S. registrations for commodities in this the tolerance levels specified below is subgroup. to be determined by measuring only (2) Tolerances are established for res- the combined residues of tepraloxydim idues of tepraloxydim, including its (2-[1-[[[(2E)-3-chloro-2-propen-1- metabolites and degradates, in or on yl]oxy]imino]propyl]-3-hydroxy-5-

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(tetrahydro-2H-pyran-4-yl)-2-cyclo- tabolites and degradates, in or on the hexen-1-one) and its metabolites con- commodities in the table below. Com- vertible to GP (3-(tetrahydropyran-4- pliance with the tolerance levels speci- yl)pentane-1,5-dioic acid) and OH–GP fied below is to be determined by meas- (3-hydroxy-3-(tetrahydropyran-4- uring only fluazinam and its metabo- yl)pentane-1,5-dioic acid), calculated as lite AMGT (3-[[4-amino-3-[[3-chloro-5- tepraloxydim, in or on the commod- (trifluoromethyl)-2-pyridinyl]amino]-2- ities. nitro-6-(trifluoromethyl) phenyl]thio]- 2-(beta-D-glucopyranosyloxy) propionic Expiration/ Commodity Parts per revocation acid). million date Commodity Parts per Canola, seed ...... 0.50 12/31/18 million Grape, wine 1 ...... 3.0 (d) Indirect or inadvertent residues. [Reserved] 1 No US registration as of March 15, 2002. [66 FR 40150, Aug. 2, 2001, as amended at 72 (3) Tolerances are established for res- FR 54588, Sept. 26, 2007; 76 FR 34885, June 15, idues of fluazinam (3-chloro-N-[3- 2011; 76 FR 82152, Dec. 30, 2011; 81 FR 34906, chloro-2,6-dinitro-4- June 1, 2016] (trifluoromethyl)phenyl]-5- (trifluoromethyl)-2-pyridinamine), in- § 180.574 Fluazinam; tolerances for cluding its metabolites and degradates, residues. in or on the commodities in the table (a) General. (1) Tolerances are estab- below. Compliance with the tolerance lished for residues of fluazinam (3- levels specified below is to be deter- chloro-N-[3-chloro-2,6-dinitro-4- mined by measuring only fluazinam, (trifluoromethyl)phenyl]-5- AMPA (2-(6-amino-3-chloro-a,a,a- (trifluoromethyl)-2-pyridinamine), in- trifluoro-2-nitro-p-toluidino)-3-chloro- cluding its metabolites and degradates, 5-(trifluoromethyl) pyridine), DAPA (3- in or on the commodities in the table chloro-2-(2,6-diamino-3-chloro-a,a,a.- below. Compliance with the tolerance trifluoro-p-toluidino)-5- levels specified below is to be deter- (trifluoromethyl)pyridine), and their mined by measuring only fluazinam. sulfamate conjugates.

Parts per Commodity Parts per Commodity million million

Apple ...... 2.0 Cattle, fat ...... 0.05 Apple, wet pomace ...... 5.0 Cattle, meat byproducts ...... 0.05 Bushberry subgroup 13-07B ...... 7.0 Goat, fat ...... 0.05 Cabbage ...... 3.0 Goat, meat byproducts ...... 0.05 Carrot, roots ...... 0.70 Horse, fat ...... 0.05 Ginseng ...... 4.5 Horse, meat byproducts ...... 0.05 Lettuce, head ...... 0.02 Sheep, fat ...... 0.05 Lettuce, leaf ...... 2.0 Sheep, meat byproducts ...... 0.05 Mayhaw ...... 2.0 Onion, bulb, subgroup 3-07A ...... 0.20 (b) Section 18 emergency exemptions. Pea and bean, dried shelled, except soybean, subgroup 6C, except pea ...... 0.02 [Reserved] Pea and bean, succulent shelled, subgroup 6B, (c) Tolerances with regional registra- except pea ...... 0.04 tions. [Reserved] Peanut ...... 0.02 (d) Indirect or inadvertent residues. Pepper/eggplant subgroup 8–10B ...... 0.09 Soybean, seed ...... 0.01 [Reserved] Soybean, hulls ...... 0.05 [66 FR 46738, Sept. 7, 2001, as amended at 67 Tea, dried 1 ...... 6.0 Turnip, greens ...... 0.01 FR 19130, Apr. 18, 2002; 72 FR 60260, Oct. 24, Vegetable, Brassica leafy, group 5, except cab- 2007; 75 FR 26667, May 12, 2010; 76 FR 3029, bage ...... 0.01 Jan. 19, 2011; 77 FR 66729, Nov. 7, 2012; 81 FR Vegetable, cucurbit, group 9 ...... 0.07 20550, Apr. 8, 2016; 81 FR 34283, May 31, 2016; Vegetable, legume, edible-podded, subgroup 6A, 82 FR 21948, May 11, 2017] except pea ...... 0.10 Vegetable, tuberous and corm, subgroup 1C ...... 0.02 § 180.575 Sulfuryl fluoride; tolerances 1 There is no U.S. registration as of January 19, 2017. for residues. (2) Tolerances are established for res- (a)(1) General. Tolerances are estab- idues of fluazinam, including its me- lished for residues of sulfuryl fluoride

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in or on the following commodities § 180.576 Cyhalofop-butyl; tolerances from the postharvest fumigation with for residues. sulfuryl fluoride for the control of in- (a) General. Tolerances are estab- sects: lished for residues of cyhalofop-butyl, including its metabolites and Commodity Parts per million degradates, in or on the commodities All processed food commodities not otherwise listed in the table below. Compliance listed ...... 2.0 with the tolerance levels specified Barley, bran, postharvest ...... 0.05 below is to be determined by measuring Barley, flour, postharvest ...... 0.05 Barley, grain, postharvest ...... 0.1 cyhalofop butyl [R-( + )-n-butyl-2-(4(4- Barley, pearled barley, postharvest ...... 0.05 cyano-2-fluorophenoxy)- Cacao bean, roasted bean, postharvest ...... 0.2 phenoxy)propionate], cyhalofop acid Cattle, meat, dried ...... 0.01 [R-( + )-2-(4(4-cyano-2-fluorophenoxy)- Cheese ...... 2.0 Coconut, postharvest ...... 1.0 phenoxy)propionic acid], and the di- Coffee, bean, roasted bean, postharvest ...... 1.0 acid metabolite [(2R)-4-(4-(1- Corn, field, flour, postharvest ...... 0.01 carboxyethoxy)phenoxy)-3- Corn, field, grain, postharvest ...... 0.05 fluorobenzoic acid]. Corn, field, grits, postharvest ...... 15.0 Corn, field, meal, postharvest ...... 0.01 Parts per Corn, pop, grain, postharvest ...... 0.05 Commodity million Cotton, undelinted seed, postharvest ...... 0.5 Egg, dried ...... 1.0 Rice, grain ...... 0.40 Fruit, dried, postharvest ...... 0.05 Wild rice, grain ...... 0.40 Ginger, postharvest ...... 0.5 Grain, aspirated fractions, postharvest ...... 0.05 Herbs and spices group 19, postharvest ...... 0.5 (b) Section 18 emergency exemptions. Hog, meat ...... 0.02 [Reserved] Milk, powdered ...... 2.0 (c) Tolerances with regional registra- Millet, grain, postharvest ...... 0.1 Nut, pine, postharvest ...... 0.2 tions. [Reserved] Nut, tree, Group 14, postharvest ...... 3.0 (d) Indirect or inadvertent residues. Oat, flour, postharvest ...... 0.05 [Reserved] Oat, grain, postharvest ...... 0.1 Oat, groats/rolled oats, postharvest ...... 0.1 [67 FR 43256, June 27, 2002, as amended at 74 Peanut, postharvest ...... 0.5 FR 15880, Apr. 8, 2009; 76 FR 82157, Dec. 30, Pistachio, postharvest ...... 3.0 2011] Rice, bran, postharvest ...... 0.01 Rice, flour, postharvest ...... 0.05 Rice, grain, postharvest ...... 0.04 § 180.577 Bispyribac-sodium; toler- Rice, hulls, postharvest ...... 0.1 ances for residues. Rice, polished rice, postharvest ...... 0.01 (a) General. Tolerances are estab- Rice, wild, grain, postharvest ...... 0.05 Sorghum, grain, grain, postharvest ...... 0.1 lished for residues of the herbicide Triticale, grain, postharvest ...... 0.1 bispyribac-sodium, including its me- Vegetable, legume, group 6, postharvest ...... 0.5 tabolites and degradates, in or on the Wheat, bran, postharvest ...... 0.05 Wheat, flour, postharvest ...... 0.05 commodity listed below. Compliance Wheat, germ, postharvest ...... 0.02 with the tolerance level specified below Wheat, grain, postharvest ...... 0.1 is to be determined by measuring only Wheat, milled byproducts, postharvest ...... 0.05 bispyribac-sodium, (2,6-bis[(4,6- Wheat, shorts, postharvest ...... 0.05 dimethoxy-2-pyrimidinyl)oxy]benzoic (2) To assure safe use of this pesticide acid, sodium salt), in or on the fol- commodities treated with sulfuryl flu- lowing raw agricultural commodities: oride must be aerated for at least 24 Parts per hours prior to entering commerce. Commodity million (b) Section 18 emergency exemptions. [Reserved] Fish, freshwater ...... 0.01 Rice, grain ...... 0.02 (c) Tolerances with regional registration. [Reserved] (b) Section 18 emergency exemptions. (d) Indirect or inadvertant residues. [Reserved] [Reserved] (c) Tolerances with regional registra- [67 FR 5740, Feb. 7, 2002, as amended at 69 FR tions. [Reserved] 3257, Jan. 23, 2004; 70 FR 40908, July 15, 2005]

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(d) Indirect or inadvertent residues. N′-cyano-N-methylethanimidamide, in- [Reserved] cluding its metabolites and degradates, in or on the commodities in the table [66 FR 48097, Sept. 18, 2001, as amended at 76 FR 5716, Feb. 2, 2011; 80 FR 72599, Nov. 20, below as a result of the application of 2015] acetamiprid. Compliance with the tolerance levels specified below is to be § 180.578 Acetamiprid; tolerances for determined by measuring acetamiprid residues. and (1E)-N-[(6-chloro-3- (a) General. (1) Tolerances are estab- pyridinyl)methyl]-N′-cyano-N- lished for residues of the insecticide ethanimidamide in or on the following acetamiprid (1E)-N-[(6-chloro-3- commodities. pyridinyl)methyl]-N’-cyano-N- Parts per methylethanimidamide, including its Commodity million metabolites and degradates, in or on the commodities in the table below as Cattle, fat ...... 0.20 Cattle, meat ...... 0.30 a result of the application of Cattle, meat byproducts ...... 0.70 acetamiprid. Compliance with the tol- Egg ...... 0.010 erance levels specified below is to be Goat, fat ...... 0.20 determined by measuring only Goat, meat ...... 0.30 Goat, meat byproducts ...... 0.70 acetamiprid in or on the following Hog, fat ...... 0.10 commodities. Hog, meat ...... 0.10 Hog, meat byproducts ...... 0.20 Commodity Parts per Horse, fat ...... 0.20 million Horse, meat ...... 0.30 Horse, meat byproducts ...... 0.70 Almond, hulls ...... 5.0 Milk ...... 0.30 Asparagus ...... 0.80 Berry, low growing subgroups 13–07G ...... 0.60 Poultry, fat ...... 0.010 Brassica, leafy greens, subgroup 4–16B ...... 15 Poultry, liver ...... 0.050 Bushberry subgroup 13–07B ...... 1.6 Poultry, meat ...... 0.010 Caneberry subgroup 13–07A ...... 1.6 Sheep, fat ...... 0.20 Celtuce ...... 3 Sheep, meat ...... 0.30 Citrus, dried pulp ...... 1.20 Sheep, meat byproducts ...... 0.70 Corn, sweet, forage ...... 15 Corn, sweet, kernel plus cob with husks removed 0.01 (3) A tolerances of 0.01 ppm is estab- Corn, sweet, stover ...... 30 Cotton, gin byproducts ...... 20.0 lished for residues of the insecticide Cottonseed subgroup 20C ...... 0.7 acetamiprid, including its metabolites Fennel, florence, fresh leaves and stalk ...... 3 and degradates, in or on all food/feed Fruit, citrus, group 10–10 ...... 1.0 Fruit, pome, group 11–10 ...... 1.0 items (other than those covered by a Fruit, small, vine climbing, except fuzzy kiwifruit, higher tolerance in paragraph (a)(1) or subgroup 13-07F ...... 0.35 (a)(2) of this section as a result of the Fruit, stone, group 12–12 ...... 1.5 Grain, aspirated fractions ...... 5.0 use on growing crops) as a result of the Kohlrabi ...... 1.2 application of acetamiprid in food/feed Leaf petiole vegetable subgroup 22B ...... 3 handling establishments. Compliance Leafy greens subgroup 4–16A ...... 3 Nut, tree, group 14–12 ...... 0.1 with the 0.01 ppm tolerance level is to Onion, bulb, subgroup 3–07A ...... 0.02 be determined by measuring only Onion, green, subgroup 3–07B ...... 4.5 acetamiprid (1E)-N-[(6-chloro-3- Pea and bean, succulent shelled, subgroup 6B ... 0.40 ′ Rapeseed subgroup 20A ...... 0.01 pyridinyl)methyl]-N -cyano-N- Soybean, hulls ...... 0.04 methylethanimidamide in or on the Soybean, seed ...... 0.03 commodities. Tea, dried1 ...... 50.0 Tomato, paste ...... 0.40 (b) Section 18 emergency exemptions. Tropical and subtropical, medium to large fruit, Time-limited tolerances specified in smooth, inedible peel, subgroup 24B ...... 0.5 the following table are established for Vegetable, brassica, head and stem, group 5–16 1.2 residues of the acetamiprid, (1E)-N-[(6- Vegetable, cucurbit, group 9 ...... 0.50 Vegetable, fruiting, group 8–10 ...... 0.20 chloro-3-pyridinyl)methyl]-N’-cyano-N- Vegetable, legume, edible podded, subgroup 6A 0.60 methylethanimidamide, in or on the Vegetable, tuberous and corm, group 1 ...... 0.01 specified agricultural commodities, re- 1There are no U.S. registrations as of February 10, 2010, sulting from use of the pesticide pursu- for the use of acetamiprid on dried tea. ant to FIFRA section 18 emergency ex- (2) Tolerances are established for res- emptions. Compliance with the toler- idues of the insecticide acetamiprid ance levels specified below is to be de- (1E)-N-[(6-chloro-3-pyridinyl)methyl]- termined by measuring only

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acetamiprid. The tolerances expire on Commodity Parts per the date specified in the table. million Kohlrabi ...... 5.0 Parts per Expiration Commodity million date Leaf petiole vegetable subgroup 22B ...... 60 Leafy vegetable group 4–16 ...... 60 Sugarcane, cane ...... 45 12/31/19 Okra ...... 3.5 Sugarcane, molasses ...... 600 12/31/19 Onion, bulb, subgroup 3–07A ...... 0.20 Onion, green, subgroup 3–07B ...... 1.5 (c) Tolerances with regional registra- Pepper, nonbell ...... 3.5 tions. Tolerances with regional reg- Sunflower ...... 0.02 istrations are established for residues Tomato, paste ...... 2.2 of the insecticide acetamiprid (1E)-N- Tomato, puree ...... 2.0 [(6-chloro-3-pyridinyl)methyl]-N′- Turnip, greens ...... 55 Vegetable, Brassica, head and stem, group 5–16 5.0 cyano-N-methylethanimidamide, in- Vegetable, cucurbit, group 9 ...... 0.15 cluding its metabolites and degradates, Vegetable, fruiting, group 8, except nonbell pep- in or on the commodities in the table per ...... 1.0 below as a result of the application of Vegetable, root, except sugar beet, subgroup 1B, acetamiprid. Compliance with the tol- except radish ...... 0.15 erance levels specified below is to be Vegetable, tuberous and corm, subgroup 1C ...... 0.02 determined by measuring only (2) Tolerances are established for res- acetamiprid in or on the following idues of the fungicide fenamidone, in- commodities. cluding its metabolites and degradates,

Commodity Parts per in or on the following commodities. million Compliance with the tolerance levels is Clover, forage ...... 0.30 to be determined by measuring Clover, hay ...... 2.0 fenamidone (4H-Imidazol-4-one, 3,5- dihydro-5-methyl-2-(methylthio)-5- (d) Indirect or inadvertent residues. phenyl-3 (phenylamino)-,(S)-), and its [Reserved] metabolite RPA 717879 (2,4- [67 FR 14659, Mar. 27, 2002, as amended at 68 imidazolidinedione, 5-methyl-5-phenyl), FR 52352, Sept. 3, 2003; 70 FR 19293, Apr. 13, in or on the commodities: 2005; 72 FR 67262, Nov. 28, 2007; 73 FR 2811, Jan. 16, 2008; 75 FR 6582, Feb. 10, 2010; 77 FR Parts per 18716, Mar. 28, 2012; 77 FR 43529, July 25, 2012; Commodity million 78 FR 36676, June 19, 2013; 80 FR 68778, Nov. 6, 2015; 82 FR 17151, Apr. 10, 2017; 85 FR 8441, Cattle, fat ...... 0.10 Feb. 14, 2020] Cattle, meat ...... 0.10 Cattle, meat byproducts ...... 0.10 § 180.579 Fenamidone; tolerances for Goat, fat ...... 0.10 residues. Goat, meat ...... 0.10 Goat, meat byproducts ...... 0.10 (a) General. (1) Tolerances are estab- Milk ...... 0.02 lished for residues of the fungicide, Sheep, fat ...... 0.10 fenamidone, including its metabolites Sheep, meat ...... 0.10 and degradates, in or on the following Sheep, meat byproducts ...... 0.10 commodities. Compliance with the tolerance levels is to be determined by (b) Section 18 emergency exemptions. measuring only fenamidone (4H- [Reserved] Imidazol-4-one, 3,5-dihydro-5-methyl-2- (c) Tolerances with regional registra- (methylthio)-5-phenyl-3 (phenylamino)- tions. A tolerance with regional reg- ,(S)-), in or on the commodities: istration as defined in § 180.1(l) is established for residues of the fungicide Parts per Commodity million fenamidone, including its metabolites and degradates, in or on the following Basil, dried leaves ...... 200 Basil, fresh leaves ...... 30 commodities. Compliance with the tol- Bean, succulent, except cowpea ...... 0.80 erance levels is to be determined by Celtuce ...... 60 measuring only fenamidone (4H- Cilantro, fresh leaves ...... 60 Cotton, gin byproducts ...... 0.02 Imidazol-4-one, 3,5-dihydro-5-methyl-2- Cottonseed subgroup 20C ...... 0.02 (methylthio)-5-phenyl-3 (phenylam- Fennel, Florence, fresh leaves and stalk ...... 60 ino)-,(S)-), in or on the commodity: Ginseng ...... 0.80

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(c) Tolerances with regional registra- Commodity Parts per million tions. [Reserved] Grape1 ...... 1.0 (d) Indirect or inadvertent residues. [Reserved] 1 Applicable to grapes grown East of the Rocky Mountains. [67 FR 57532, Sept. 11, 2002, as amended at 74 (d) Indirect or inadvertent residues. FR 23644, May 20, 2009] Tolerances are established for residues of the fungicide fenamidone, including § 180.581 Iprovalicarb; tolerances for its metabolites and degradates, in or residues. on the following commodities. Compli- (a) General. Tolerances are estab- ance with the tolerance levels is to be lished for residues of iprovalicarb, [2- determined by measuring fenamidone methyl-1[[[(1S)-(4-methylphenyl) ethyl] (4H-Imidazol-4-one, 3,5-dihydro-5-meth- amino]carbonyl] propyl]carbamic acid yl-2-(methylthio)-5-phenyl-3 methylethylester, in or on the fol- (phenylamino)-,(S)-), and its metabo- lowing commodities. lite RPA 717879 (2,4-imidazolidinedione, 5-methyl-5-phenyl), in or on the fol- Commodity Parts per lowing commodities when present million therein as a result of application of Grape 1 ...... 2.0 fenamidone to the crops in paragraph Tomato 1 ...... 1.0 (a)(1). 1There is no U.S. registration as of September 1, 2005.

Parts per (b) Section 18 emergency exemptions. Commodity million [Reserved] Grain, cereal, group 15, except rice ...... 0.1 (c) Tolerances with regional registra- Grain, cereal, forage, fodder and straw, group 16, tions. [Reserved] except rice ...... 0.5 (d) Indirect or inadvertent residues. Soybean, forage ...... 0.15 [Reserved] Soybean, hay ...... 0.25 Soybean, seed ...... 0.02 [67 FR 54359, Aug. 22, 2002, as amended at 70 Strawberry ...... 0.02 FR 55281, Sept. 21, 2005]

[67 FR 60976, Sept. 27, 2002, as amended at 69 § 180.582 Pyraclostrobin; tolerances FR 58066, Sept. 29, 2004; 71 FR 55293, Sept. 22, for residues. 2006; 72 FR 60272, Oct. 24, 2007; 74 FR 34257, (a) General. (1) Tolerances are estab- July 15, 2009; 76 FR 34885, June 15, 2011; 76 FR lished for residues of the fungicide 70895, Nov. 16, 2011; 77 FR 32401, June 1, 2012; pyradostrobin, including its metabo- 79 FR 13882, Mar. 12, 2014; 82 FR 35114, July lites and degradates, in or on the com- 28, 2017] modities in the table below. Compli- § 180.580 Iodosulfuron-Methyl-Sodium; ance with the tolerance levels specified tolerances for residues. below is to be determined by measuring only the sum of pyraclostrobin (car- (a) General. Tolerances are estab- bamic acid, [2-[[[ 1-(4-chlorophenyl)-1H- lished for residues of the herbicide pyrazol-3-yl]oxy] meth- Iodosulfuron-Methyl-Sodium (methyl 4- yl]phenyl]methoxy-, methyl ester) and iodo-2-[3-(4-methoxy-6-methyl-1,3,5 its desmethoxy metabolite (methyl-N- triazin-2-yl)ureidosulfonyl]benzoate, so- [[[1-(4-chlorophenyl)-1H-pyrazol-3- dium salt) in or on the following com- yl]oxy]methyl] phenylcarbamate), cal- modities: culated as the stoichiometric equiva- Parts per lent of pyraclostrobin, in or on the Commodity million commodity.

Corn, field, forage ...... 0.05 Parts per Corn, field, grain ...... 0.03 Commodity million Corn, field, stover ...... 0.05 Wheat, forage ...... 0.10 Alfalfa, forage ...... 10 Wheat, grain ...... 0.02 Alfalfa, hay ...... 30 Wheat, hay ...... 0.05 Almond, hulls ...... 7.0 Wheat, straw ...... 0.05 Apple, wet pomace ...... 8.0 Artichoke, globe ...... 3.0 Avocado ...... 0.6 (b) Section 18 emergency exemptions. Banana ...... 0.04 [Reserved] Barley, grain ...... 1.4

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Parts per Parts per Commodity million Commodity million

Barley, hay ...... 25 Soybean, seed ...... 0.04 Barley, straw ...... 6.0 Spearmint, tops ...... 8.0 Bean, succulent shelled ...... 0.5 Star apple ...... 0.6 Beet, sugar, dried pulp ...... 1.0 Sugarcane, cane ...... 0.20 Beet, sugar, roots ...... 0.2 Vegetable, Brassica, head and stem, group 5–16 5.0 Beet, sugar, tops ...... 8.0 Vegetable, bulb, group 3–07 ...... 0.9 Berry, low growing, subgroup 13–07G, except Vegetable, cucurbit, group 9 ...... 0.5 cranberry ...... 1.2 Vegetable, foliage of legume, except soybean, Brassica, leafy greens, subgroup 4–16B, except subgroup 7A ...... 25.0 watercress ...... 16 Vegetable, fruiting, group 8–10 ...... 1.4 Bushberry subgroup 13–07B ...... 4.0 Vegetable, leaves of root and tuber, group 2, ex- Caneberry subgroup 13–07A ...... 4.0 cept sugar beet ...... 16.0 Canistel ...... 0.6 Vegetable, legume, edible podded, subgroup 6A 0.5 Celtuce ...... 29 Vegetable, root, except sugar beet, subgroup 1B 0.4 Citrus, dried pulp ...... 12.5 Vegetable, tuberous and corm, subgroup 1C ...... 0.04 Citrus, oil ...... 9.0 Vegetables, foliage of legume, group 7 ...... 25 Coffee, green bean ...... 1 0.3 Wheat, grain ...... 0.02 Corn, field, forage ...... 5.0 Wheat, hay ...... 6.0 Corn, field, grain ...... 0.1 Wheat, straw ...... 8.5 Corn, field, refined oil ...... 0.2 Corn, field, stover ...... 17.0 Corn, pop, grain ...... 0.1 (2) Tolerances are established for Corn, pop, stover ...... 17.0 combined residues of the fungicide Corn, sweet, forage ...... 5.0 Corn, sweet, kernel plus cob with husks removed 0.04 pyraclostrobin carbamic acid, [2-[[[1-(4- Corn, sweet, stover ...... 23.0 chlorophenyl)-1H-pyrazol-3- Cotton, gin byproducts ...... 30 yl]oxy]methyl]phenyl]methoxy-, meth- Dill, seed ...... 40 yl ester and its metabolites convertible Endive, belgium ...... 4.0 Fennel, Florence ...... 29 to 1-(4-chlorophenyl)-1H-pyrazol-3-ol Fruit, citrus, group 10–10 ...... 2.0 and 1-(4-chloro-2-hydroxyphenyl)-1H- Fruit, pome, group 11–10 ...... 1.5 pyrazol-3-ol, expressed as parent com- Fruit, small vine climbing, except fuzzy kiwifruit, subgroup 13–07F ...... 2.0 pound, in or on the following raw agri- Fruit, stone, group 12–12 ...... 2.5 cultural commodities. Grain, aspirated fractions ...... 2.5 Grape, raisin ...... 7.0 Commodity Parts per Grass, forage ...... 10 million Grass, hay ...... 4.5 Grass, seed screenings ...... 27 Cattle, fat ...... 0.1 Grass, straw ...... 14 Cattle, liver ...... 1.5 Herb subgroup 19A ...... 40 Cattle, meat ...... 0.1 Hop, dried cones ...... 23.0 Cattle, meat byproducts, except liver ...... 0.2 Kohlrabi ...... 5.0 Goat, fat ...... 0.1 Leaf petiole vegetable, subgroup 22B ...... 29 Goat, liver ...... 1.5 Leafy greens, subgroup 4–16A ...... 40 Goat, meat ...... 0.1 Mango ...... 0.6 Goat, meat byproducts, except liver ...... 0.2 Nut, tree, group 14–12, except pistachio ...... 0.04 Hog, fat ...... 0.1 Oat, grain ...... 1.2 Hog, liver ...... 1.5 Oat, hay ...... 18 Hog, meat ...... 0.1 Oat, straw ...... 15 Hog, meat byproducts, except liver ...... 0.2 Oilseed group 20 ...... 0.45 Horse, fat ...... 0.1 Papaya ...... 0.6 Horse, liver ...... 0.1 Pea, succulent ...... 0.2 Horse, meat ...... 0.1 Pea and bean, dried shelled, except soybean, Horse, meat byproducts, except liver ...... 0.2 subgroup 6C ...... 0.5 Milk ...... 0.1 Peanut ...... 0.05 Poultry, eggs ...... 0.10 Peanut, refined oil ...... 0.1 Poultry, fat ...... 0.10 Peppermint, tops ...... 8.0 Poultry, meat ...... 0.10 Persimmon ...... 3.0 Poultry, meat byproducts ...... 0.10 Pistachio ...... 0.7 Sheep, fat ...... 0.1 Radish, tops ...... 16 Sheep, liver ...... 1.5 Rye, grain ...... 0.04 Sheep, meat ...... 0.1 Rye, straw ...... 0.5 Sheep, meat byproducts, except liver ...... 0.2 Sapodilla ...... 0.6 Sapote, black ...... 0.6 (b) Section 18 emergency exemptions. A Sapote, mamey ...... 0.6 Sorghum, grain, forage ...... 5.0 time-limited tolerance is established Sorghum, grain, grain ...... 0.60 for combined residues of the fungicide Sorghum, grain, stover ...... 0.80 pyraclostrobin, (carbamic acid, [2-[[[1- Soybean, forage ...... 11 Soybean, hay ...... 14 (4-chlorophenyl)-1H-pyrazol-3- Soybean, hulls ...... 0.06 yl]oxy]methyl] phenyl]methoxy-,

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methyl ester) and its desmethoxy me- dichloro-N-[(dimethylamino)-sulfonyl]- tabolite (methyl-N-[[[1-(4- 1-fluoro-N-(4- chlorophenyl) pyrazol-3-yl]oxy]o- methylphenyl)methanesulfenamide in tolyl]carbamate) in connection with or on the following commodities. use of the pesticide under section 18 Parts per emergency exemptions granted by Commodity million EPA. The time-limited tolerance will expire and is revoked on the date speci- Apple 1 ...... 5.0 Grape 1 ...... 11 fied in the following table. Hop, dried cones 1 ...... 30 Tomato 1 ...... 2.0 Expiration/ Commodity Parts per revocation 1 No U.S. registration as of August 31, 2002. million date (b) Section 18 emergency exemptions. Endive, belgium ...... 11.0 12/31/13 [Reserved] (c) Tolerances with regional registra- (c) Tolerances with regional registrations. [Reserved] tions. [Reserved] (d) Indirect or inadvertent residues. (d) Indirect or inadvertent residues. [Reserved] [Reserved] [67 FR 60141, Sept. 25, 2002] [67 FR 60901, Sept. 27, 2002, as amended at 69 FR 63100, Oct. 29, 2004; 71 FR 17021, Apr. 5, § 180.585 Pyraflufen-ethyl; tolerances 2006; 72 FR 54569, Sept. 26, 2007; 73 FR 15431, for residues. Mar. 24, 2008; 73 FR 21842, Apr. 23, 2008; 73 FR 44167, July 30, 2008; 74 FR 11499, Mar. 18, 2009; (a) General. Tolerances are estab- 74 FR 51496, Oct. 7, 2009; 75 FR 770, Jan. 6, lished for residues of the herbicide, 2010; 75 FR 42329, July 21, 2010; 75 FR 80346, pyraflufen-ethyl, including its metabo- Dec. 22, 2010; 76 FR 81396, Dec. 28, 2011; 78 FR lites and degradates, in the commod- 53046, Aug. 28, 2013; 80 FR 19238, Apr. 10, 2015; ities in the table below. Compliance 83 FR 51862, Oct. 15, 2018] with the plant commodity tolerance levels specified in the table is to be de- § 180.583 Triticonazole; tolerances for termined by measuring only the sum of residues. the parent pyraflufen-ethyl, ethyl 2-[2- (a) General. Tolerances are estab- chloro-5-(4-chloro-5-difluoromethoxy)- lished for residues of the fungicide 1-methyl-1H-pyrazol-3-yl]-4- triticonazole, (1RS)-(E)-5-[(4- fluorophenoxy] acetate, and its acid chlorophenyl)methylene]-2,2-dimethyl- metabolite, E–1, 2-chloro-5-(4-chloro-5- 1-(1H-1,2,4-triazol-1- difluoromethoxy-1-methyl-1H-pyrazol- ylmethyl)cyclopentanol, from the 3-yl)-4-fluorophenoxyacetic acid, cal- treatment of seed prior to planting in culated as the stoichiometric equiva- or on raw agricultural commodities as lent of pyraflufen-ethyl in or on the follows: commodity. Compliance with the livestock commodity tolerance levels spec- Parts per Commodity million ified in the table is to be determined by measuring only the sum of the parent Grain, cereal, forage, fodder and straw, group 16, pyraflufen-ethyl, ethyl 2-[2-chloro-5-(4- except rice ...... 0.10 Grain, cereal, group 15, except rice ...... 0.01 chloro-5-difluoromethoxy)-1-methyl- 1H-pyrazol-3-yl]-4-fluorophenoxy] ace- (b) Section 18 emergency exemptions. tate and its acid metabolites: E–1, 2- [Reserved] chloro-5-(4-chloro-5-difluoromethoxy-1- (c) Tolerances with regional registra- methyl-1H-pyrazol-3-yl)-4- tions. [Reserved] fluorophenoxyacetic acid, and E–9, 2- (d) Indirect or inadvertent residues. chloro-5-(4-chloro-5-difluoromethoxy- [Reserved] 1H-pyrazol-3-yl)-4-fluorophenoxyacetic acid, both calculated as the stoichio- [67 FR 60959, Sept. 27, 2002, as amended at 75 metric equivalent of pyraflufen-ethyl FR 4288, Jan. 27, 2010] in or on the commodity.

§ 180.584 Tolylfluanid; tolerances for Parts per residues. Commodity million

(a) General. Tolerances are estab- Almond, hulls ...... 0.02 lished for residues of tolylfluanid, 1,1- Cattle, fat ...... 0.03

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Parts per Parts per Commodity million Commodity million

Cattle, meat ...... 0.03 Almond, hulls ...... 1.5 Cattle, meat byproducts ...... 0.03 Beet, sugar, dried pulp ...... 0.03 Corn, field, forage ...... 0.01 Beet, sugar, molasses ...... 0.05 Corn, field, grain ...... 0.01 Beet, sugar, roots ...... 0.02 Corn, field, stover ...... 0.01 Berry, low-growing, subgroup 13-07H, except Cotton, gin byproducts ...... 1.5 strawberry ...... 0.01 Cottonseed subgroup 20C ...... 0.04 Canola, seed ...... 0.01 Fruit, pome, group 11–10 ...... 0.01 Cotton, gin byproducts ...... 4.5 Fruit, small, vine climbing, except fuzzy kiwifruit, Cotton, undelinted seed ...... 0.20 subgroup. Fig ...... 0.05 Fruit, pome ...... 1.0 Fruit, stone, group 12–12 ...... 0.01 Grain, cereal, forage, fodder and straw, group 16, Goat, fat ...... 0.03 except rice, forage ...... 0.35 Goat, meat ...... 0.03 Grain, cereal, forage, fodder and straw, group 16, Goat, meat byproducts ...... 0.03 except rice, hay ...... 0.07 Grass, forage, group 17 ...... 1.0 Grain, cereal, forage, fodder and straw, group 16, Grass, hay, group 17 ...... 1.4 except rice, stover ...... 0.1 Hop, dried cones ...... 0.02 Grain, cereal, forage, fodder and straw, group 16, Horse, fat ...... 0.03 except rice, straw ...... 0.05 Horse, meat ...... 0.03 Grain, cereal, group 15, except rice ...... 0.01 Horse, meat byproducts ...... 0.03 Grape ...... 0.60 Milk ...... 0.03 Milk ...... 0.01 Nut, tree, group 14–12 ...... 0.01 Mustard, seed ...... 0.01 Peanut ...... 0.01 Nut, tree, group 14 ...... 0.01 Peanut, hay ...... 0.07 Peach ...... 0.80 Pomegranate ...... 0.01 Pepper ...... 0.80 1 Sheep, fat ...... 0.03 Persimmon ...... 0.5 Pomegranate ...... 0.20 Sheep, meat ...... 0.03 Potato, chips ...... 0.6 Sheep, meat byproducts ...... 0.03 Potato, granules/flakes ...... 1.5 Soybean, forage ...... 0.05 Rice, grain ...... 0.01 Soybean, hay ...... 0.10 Soybean, seed ...... 0.02 Soybean, seed ...... 0.01 Tea, dried 1 ...... 70 Tropical and subtropical, small fruit, edible peel, Vegetable, brassica, leafy, group 5 ...... 1.9 subgroup 23A ...... 0.01 Vegetable, bulb, group 3-07 ...... 0.45 Vegetable, tuberous and corm, subgroup 1C ...... 0.02 Vegetable, cucurbit, group 9 ...... 0.06 Wheat, forage ...... 0.02 Vegetable, fruiting, group 8, except pepper ...... 0.20 Wheat, grain ...... 0.01 Vegetable, leafy, except brassica, group 4 ...... 3.0 Wheat, hay ...... 0.01 Vegetable, root, except sugar beet, subgroup 1B 0.8 Wheat, straw ...... 0.01 Vegetable, tuberous and corm, subgroup 1C ...... 0.3 1 No U.S. registrations. (b) Section 18 emergency exemptions. [Reserved] (2) Time-limited tolerances are estab- (c) Tolerances with regional registra- lished for residues of the insecticide tions. [Reserved] clothianidin, including its metabolites (d) Indirect or inadvertent residues. and degradates. Compliance with the [Reserved] tolerance levels specified below is to be determined by measuring only [68 FR 23055, Apr. 30, 2003, as amended at 68 clothianidin, (E)-1-(2-chloro-1,3-thiazol- FR 27739, May 21, 2003; 69 FR 26312, May 12, 5-ylmethyl)-3-methyl-2-nitroguanidine, 2004; 73 FR 51743, Sept. 5, 2008; 76 FR 31484, June 11, 2011; 77 FR 75861, Dec. 26, 2012; 78 FR in or on the following raw agricultural 13263, Feb. 27, 2013; 84 FR 48076, Sept. 12, 2019] commodity: Expiration/ § 180.586 Clothianidin; tolerances for Commodity Parts per revocation residues. million date

(a) General. (1) Tolerances are estab- Rice, seed ...... 0.01 6/23/12 lished for residues of the insecticide clothianidin, including its metabolites (b) Section 18 emergency exemptions. A and degradates. Compliance with the time-limited tolerance specified in the tolerance levels specified below is to be following table is established for resi- determined by measuring only dues of clothianidin, (E)-N-[(2-chloro-5- clothianidin, (E)-N-[(2-Chloro-5- thiazolyl)methyl]-N’-methyl-N’’- thiazolyl)methyl]-N′ -methyl-N″ nitroguanidine, in or on the specified -nitroguanidine, in or on the following agricultural commodity, resulting raw agricultural commodities: from use of the pesticide pursuant to

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FIFRA section 18 emergency exemp- Commodity Parts per tions. This tolerance expires on the million date specified in the table. Milk, fat (reflecting negligible residues in whole milk) ...... 0.06 Parts per Expiration/ Onion, bulb, subgroup 3–07A ...... 0.45 Commodity million revocation Onion, green, subgroup 3–07B ...... 40 date Potato ...... 0.02 Sheep, fat ...... 0.02 Fruit, citrus, group 10–10 ...... 0.07 12/31/20 Sheep, liver ...... 0.05 Rice, grain ...... 0.5 12/31/24 Spinach ...... 50 Tomato ...... 1.0 (c) Tolerances with regional registra- Vegetable, cucurbit, group 9 ...... 0.30 Vegetable, fruiting, group 8, except tomato ...... 4.0 tions. [Reserved] Vegetable, leafy, except Brassica, group 4, ex- (d) Indirect and inadvertant residues. cept spinach ...... 25 Tolerances are established for the indi- 1 There are no U.S. registrations as of May 15, 2003. rect or inadvertent residues of the insecticide clothianidin, including its (b) Section 18 emergency exemptions. metabolites and degradates. Compli- [Reserved] ance with the tolerance levels specified (c) Tolerances with a regional registra- below is to be determined by measuring tions. Tolerances with a regional reg- only clothianidin, (E)-1-(2-chloro-1,3- istration as defined in § 180.1(l) are es- thiazol-5-ylmethyl)-3-methyl-2- tablished for the residues of the fun- nitroguanidine, in or on the following gicide famoxadone, 3-anilino-5-methyl- raw agricultural commodities when 5-(4-phenoxyphenyl)-1,3-oxazolidine-2,4- present therein as a result of the appli- dione) in or on the raw agricultural cation of clothianidin to crops listed in commodities: paragraph (a) of this section: Parts per Commodity million Commodity Parts per million Grape ...... 2.5

Animal feed, nongrass, group 18 ...... 0.02 Grass, forage, fodder and hay, group 17 ...... 0.02 (d) Indirect or inadvertant residues. Soybean, forage ...... 0.02 [Reserved] Soybean, hay ...... 0.02 [68 FR 39471, July 2, 2003, as amended at 72 FR 28881, May 23, 2007; 74 FR 9364, Mar. 4, [74 FR 65028, Dec. 9, 2009, as amended at 76 2009; 76 FR 34885, June 15, 2011] FR 7718, Feb. 11, 2011; 76 FR 25246, May 4, 2011; 76 FR 34886, June 15, 2011; 77 FR 52252, § 180.588 Quinoxyfen; tolerances for Aug. 29, 2012; 78 FR 19136, Mar. 29, 2013; 80 FR residues. 10007, Feb. 25, 2015; 82 FR 57151, Dec. 4, 2017; (a) General. Tolerances are estab- 84 FR 53336, Oct. 7, 2019; 84 FR 64777, Nov. 25, 2019] lished for residues of the fungicide quinoxyfen, including its metabolites § 180.587 Famoxadone; tolerance for and degradates, in or on the commod- residues. ities in the following table. Compliance (a) General. Tolerances are estab- with the tolerance levels specified in lished for residues of the fungicide the following table is to be determined famoxadone (3-anilino-5-methyl-5-(4- by measuring only quinoxyfen (5,7- phenoxyphenyl)-1,3-oxazolidine-2,4- dichloro-4-(4-fluorophenoxy)quinoline). dione) in or on the following commod- Parts per ities: Commodity million

Parts per Artichoke, globe ...... 1.4 Commodity million Berry, low growing, subgroup 13–07G ...... 1.0 Fruit, small vine climbing, except fuzzy kiwifruit, Caneberry subgroup 13–07A ...... 10 subgroup 13–07F ...... 2.0 Cattle, fat ...... 0.02 Fruit, stone, group 12 ...... 0.70 Cattle, liver ...... 0.05 Hop, dried cones ...... 3.0 Cilantro, leaves ...... 25 Gourd, edible ...... 0.20 Lettuce, head ...... 7.0 Goat, fat ...... 0.02 Lettuce, leaf ...... 19 Goat, liver ...... 0.05 Melon, subgroup 9A ...... 0.08 Grape, raisin 1 ...... 4.0 Pumpkin ...... 0.20 Hop, dried cone ...... 80 Squash, winter ...... 0.20 Horse, fat ...... 0.02 Vegetable, fruiting, group 8–10 ...... 1.7 Horse, liver ...... 0.05

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(b) Section 18 emergency exemptions. Commodity Parts per [Reserved] million (c) Tolerances with regional registra- Peanut ...... 0.05 tions. [Reserved] Peanut, meal ...... 0.15 (d) Indirect or inadvertent residues. Peanut, refined oil ...... 0.15 Peppermint, tops ...... 30.0 [Reserved] Persimmon ...... 8.0 [68 FR 55858, Sept. 29, 2003, as amended at 70 Sapodilla ...... 1.5 Sapote, black ...... 1.5 FR 4032, Jan. 28, 2005; 71 FR 50354, Aug. 25, Sapote, mamey ...... 1.5 2006; 74 FR 14743, Apr. 1, 2009; 78 FR 57280, Soybean, hulls ...... 0.2 Sept. 18, 2013] Soybean, seed ...... 0.1 Soybean, vegetable ...... 2.0 § 180.589 Boscalid; tolerances for resi- Spearmint, tops ...... 30.0 dues. Star apple ...... 1.5 Vegetable, Brassica, head and stem, group 5–16 6.0 (a) General. (1) Tolerances are estab- Vegetable, bulb, group 3–07 ...... 5.0 lished for residues of the fungicide Vegetable, cucurbit, group 9 ...... 3.0 Vegetable, fruiting, group 8–10 ...... 3.0 boscalid, including its metabolites and Vegetable, legume, edible podded subgroup 6A .. 5.0 degradates, in or on the commodities Vegetable, root, except sugar beet, subgroup 1B 2.0 listed below. Compliance with the tol- Vegetable, tuberous and corm, subgroup 1C ...... 0.05 erance levels specified below is to be 1No US registrations as of September 16, 2009. determined by measuring only (2) Tolerances are established for res- boscalid, 3-pyridinecarboxamide, 2- idues of the fungicide boscalid, includ- chloro-N-(4′-chloro[1,1′-biphenyl]-2-yl), ing its metabolites and degradates, in in or on the following raw agricultural or on the commodities listed below. commodities: Compliance with the tolerance levels specified below is to be determined by Commodity Parts per million measuring only the sum of boscalid, 3- Alfalfa, forage ...... 30.0 pyridinecarboxamide, 2-chloro-N-(4′- Alfalfa, hay ...... 65.0 chloro[1,1′-biphenyl]-2-yl), and metabo- Almond, hulls ...... 17 lites 2-chloro-N-(4’-chloro-5-hydroxy- Apple, wet pomace ...... 10 Artichoke, globe ...... 6.0 biphenyl-2-yl) nicotinamide and glucu- Avocado ...... 1.5 ronic acid conjugate of 2-chloro-N-(4′- Banana, import 1 ...... 0.40 chloro-5-hydroxy-biphenyl-2-yl) nico- Berry, low growing, subgroup 13–07G, except cranberry ...... 4.5 tinamide, calculated as the stoichio- Brassica, leafy greens, subgroup 4–16B, except metric equivalent of boscalid in or on watercress ...... 60 the following food commodities: Bushberry subgroup 13–07B ...... 13.0 Caneberry subgroup 13–07A ...... 10.0 Parts per Canistel ...... 1.5 Commodity million Canola, refined oil ...... 5.0 Celtuce ...... 45 Cattle, fat ...... 0.30 Citrus, dried pulp ...... 4.5 Cattle, meat ...... 0.10 Citrus, oil ...... 85.0 Cattle, meat byproducts ...... 0.35 1 Coffee, green bean, import ...... 0.05 Egg ...... 0.02 Cotton, gin byproducts ...... 55.0 Goat, fat ...... 0.30 Dill, seed ...... 100 Goat, meat ...... 0.10 Endive, Belgium ...... 6.0 Goat, meat byproducts ...... 0.35 Fennel, Florence ...... 45 Hog, fat ...... 0.20 Fruit, citrus, group 10–10 ...... 2.0 Hog, meat ...... 0.05 Fruit, pome, group 11–10 ...... 3.0 Hog, meat byproducts ...... 0.10 Fruit, small vine climbing, except fuzzy kiwifruit, Horse, fat ...... 0.30 subgroup 13–07F ...... 5.0 Horse, meat ...... 0.10 Fruit, stone, group 12–12 ...... 3.5 Horse, meat byproducts ...... 0.35 Grain, aspirated fractions ...... 3.0 Milk ...... 0.10 Grape, raisin ...... 8.5 Poultry, fat ...... 0.20 Herb subgroup 19A ...... 150 Poultry, meat ...... 0.05 Hop, dried cones ...... 35 Poultry, meat byproducts ...... 0.20 Kohlrabi ...... 6.0 Sheep, fat ...... 0.30 Leaf petiole vegetable subgroup 22B ...... 45 Sheep, meat ...... 0.10 Leafy greens subgroup 4–16A ...... 70 Sheep, meat byproducts ...... 0.35 Mango ...... 1.5 Nut, tree, group 14–12 ...... 0.70 Oilseed group 20 ...... 3.5 (b) Section 18 emergency exemptions. Papaya ...... 1.5 Time-limited tolerances are estab- Pea and bean, dried shelled, except soybean, subgroup 6C ...... 2.5 lished for residues of the fungicide Pea and bean, succulent shelled, subgroup 6B ... 0.60 boscalid, including its metabolites and

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degradates, in connection with use of [68 FR 44651, July 30, 2003, as amended at 69 the pesticide under section 18 emer- FR 19774, Apr. 14, 2004; 70 FR 55293, Sept. 21, gency exemptions granted by EPA. 2005; 71 FR 6364, Feb. 8, 2006; 71 FR 25961, May 3, 2006; 71 FR 76190, Dec. 20, 2006; 73 FR 16558, Compliance with the tolerance level Mar. 28, 2008; 74 FR 47445, Sept. 16, 2009; 75 FR specified below is to be determined by 770, Jan. 6, 2010; 75 FR 29907, May 28, 2010; 75 measuring only boscalid, 3- FR 80346, Dec. 22, 2010; 78 FR 67048, Nov. 8, pyridinecarboxamide, 2-chloro-N-(4′- 2013; 80 FR 14014, Mar. 18, 2015; 82 FR 56739, chloro[1,1′-biphenyl]-2-yl). This toler- Nov. 30, 2017; 83 FR 52996, Oct. 19, 2018] ance will expire and is revoked on the § 180.590 2, 6-Diisopropylnaphthalene date specified in the following table: (2, 6-DIPN); tolerances for residues. (a) General. Tolerances are estab- Parts per Expiration/ Commodity revocation lished for residues of the growth inhib- million date itor 2,6-DIPN, including its metabolites Endive, Belgian ...... 16 12/31/13 and degradates, in or on the commodities in the following table. Compliance (c) Tolerances with regional registra- with the tolerance levels specified in tion. [Reserved] the following table is to be determined (d) Indirect or inadvertent residues. by measuring only 2,6- Tolerances are established for the indi- Diisopropylnaphthalene. rect or inadvertent residues of the fun- Parts per gicide boscalid, including its metabo- Commodity million lites and degradates, in or on the com- Cattle, fat ...... 0.2 modities listed below. Compliance with Cattle, meat ...... 0.02 the tolerance levels specified below is Cattle, meat byproducts, except fat ...... 0.02 Goat, fat ...... 0.2 to be determined by measuring only Goat, meat ...... 0.02 boscalid, 3-pyridinecarboxamide, 2- Goat, meat byproducts, except fat ...... 0.02 chloro-N-(4′-chloro[1,1′-biphenyl]-2-yl), Horse, fat ...... 0.2 Horse, meat ...... 0.02 in or on the following commodities: Horse, meat byproducts, except fat ...... 0.02 Milk, fat ...... 0.02 Commodity Parts per Potato, granules/flakes ...... 5.5 million Potato, wet peel ...... 6.0 Potato, whole ...... 2.0 Animal feed, nongrass, group 18, forage, except Sheep, fat ...... 0.2 alfalfa ...... 1.0 Sheep, meat ...... 0.02 Animal feed, nongrass, group 18, hay, except al- Sheep, meat byproducts, except fat ...... 0.02 falfa ...... 2.0 Animal feed, nongrass, group 18, seed ...... 0.05 (b) Section 18 emergency exemptions. Beet, sugar, roots ...... 0.1 [Reserved] Grain, cereal, forage, fodder and straw, group 16, forage ...... 2.0 (c) Tolerances with regional registra- Grain, cereal, forage, fodder and straw, group 16, tions. [Reserved] stover ...... 1.5 (d) Indirect or inadvertent residues. Grain, cereal, forage, fodder and straw, group 16, [Reserved] straw ...... 3.0 Grain, cereal, group 15 ...... 0.20 [71 FR 52011, Sept. 1, 2006, as amended at 74 Grass, forage, fodder, and hay, group 17, forage 2.0 FR 66579, Dec. 16, 2009; 77 FR 32406, June 1, Grass, forage, fodder, and hay, group 17, hay ..... 8.0 2012] Grass, forage, fodder, and hay, group 17, seed screenings ...... 0.20 § 180.591 Trifloxysulfuron; tolerances Grass, forage, fodder, and hay, group 17, straw .. 0.30 for residues. Rice, hulls ...... 0.50 Vegetable, foliage of legume, group 7, forage ...... 1.5 (a) General. Tolerances are estab- Vegetable, foliage of legume, group 7, hay ...... 2.0 lished for residues of the herbicide Vegetable, foliage of legume, group 7, vines ...... 0.05 trifloxysulfuron, N-[[(4,6-dimethoxy-2- Vegetable, leafy, except brassica, group 4, ex- pyrimidinyl)amino]carbonyl]-3-(2,2,2- cept celery, lettuce and spinach ...... 1.0 trifluoroethoxy)-2-pyridinesulfonamide Vegetable, leaves of root and tuber, group 2 ...... 0.1 in or on the following raw agricultural commodities.

Parts per Commodity million

Almond ...... 0.02

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(d) Indirect and inadvertant residues. Commodity Parts per million [Reserved] Almond, hulls ...... 0.01 [68 FR 54827, Sept. 19, 2003] Fruit, citrus, Group 10 ...... 0.03 Cotton, undelinted seed ...... 0.05 Cotton, gin byproducts ...... 1.0 § 180.593 Etoxazole; tolerances for resi- Sugarcane ...... 0.01 dues. Tomato ...... 0.01 (a) General. Tolerances are established for residues of etoxazole, includ- (b) Section 18 emergency exemptions. ing its metabolites and degradates, in [Reserved] or on the commodities in the table (c) Tolerances with regional registra- below. Compliance with the tolerance tions. [Reserved] levels specified below is to be deter- (d) Indirect or inadvertent residues. mined by measuring only etoxazole (2- [Reserved] (2,6-difluorophenyl)-4-[4-(1,1- [68 FR 54386, Sept. 17, 2003] dimethylethyl)-2-ethoxyphenyl]-4,5- dihydrooxazole) in or on the com- § 180.592 Butafenacil; tolerances for modity. residues. Parts per (a) General. (1) Tolerances are estab- Commodity million lished for residues of the herbicide Almond, hulls ...... 2.0 butafenacil, (1,1-dimethyl-2-oxo-2-(2- Apple, wet pomace ...... 0.50 propenyloxy)ethyl 2-chloro-5-[3,6- Avocado ...... 0.20 dihydro-3-methyl-2,6-dioxo-4- Beet, sugar, leaves ...... 1 Beet, sugar, roots ...... 0.02 (trifluoromethyl)-1(2H)-pyrimidinyl] Berry, low growing, subgroup 13–07G ...... 0.50 benzoate) in or on the following raw Caneberry subgroup 13–07A ...... 1.5 agricultural commodities: Canistel ...... 0.20 Cattle, fat ...... 0.02 Parts per Cattle, liver ...... 0.01 Commodity million Cherry subgroup 12–12A ...... 1.0 Corn, field, forage ...... 0.80 Cotton, gin byproducts ...... 10 Corn, field, grain ...... 0.01 Cotton, undelinted seed ...... 0.50 Corn, field, refined oil ...... 0.03 Corn, field, stover ...... 4.0 Corn, pop, grain ...... 0.01 (2) Tolerances are established for res- Corn, pop, stover ...... 4.0 idues of the herbicide butafenacil, (1,1- Corn, sweet, forage ...... 1.5 dimethyl-2-oxo-2-(2-propenyloxy)ethyl Corn, sweet, kernel plus cob with husks removed 0.01 Corn, sweet, stover ...... 5.0 2-chloro-5-[3,6-dihydro-3-methyl-2,6- Cotton, gin byproducts ...... 1.0 dioxo-4-(trifluoromethyl)-1(2H)- Cottonseed subgroup 20C ...... 0.05 pyrimidinyl] benzoate) and its metabo- Fruit, pome, group 11–10 ...... 0.20 lite CGA-293731 (1-carboxy-1- Fruit, small vine climbing, except fuzzy kiwifruit, subgroup 13–07F ...... 0.50 methylethyl 2-chloro-5-[3,6-dihydro-3- Goat, fat ...... 0.02 methyl-2,6-dioxo-4-(trifluoromethyl)- Goat, liver ...... 0.01 1(2H)-pyrimidinyl] benzoate), in or on Grape, raisin ...... 1.5 Hop, dried cones ...... 7.0 the following livestock commodities: Horse, fat ...... 0.02 Horse, liver ...... 0.01 Parts per Mango ...... 0.20 Commodity million Melon subgroup 9A ...... 0.20 Cattle, kidney ...... 0.05 Milk, fat ...... 0.01 Nut, tree group 14–12 ...... 0.01 Cattle, liver ...... 0.50 Orange 2 ...... 0.10 Goat, kidney ...... 0.05 Orange, oil 2 ...... 1.0 Goat, liver ...... 0.50 Papaya ...... 0.20 Hog, kidney ...... 0.05 Peach subgroup 12–12B ...... 1.0 Hog, liver ...... 0.50 Pepper/eggplant subgroup 8–10B ...... 0.20 Horse, kidney ...... 0.05 Peppermint, oil ...... 20 Horse, liver ...... 0.50 Peppermint, tops ...... 10 Sheep, kidney ...... 0.05 Plum, prune, dried ...... 0.30 Sheep, liver ...... 0.50 Plum subgroup 12–12C ...... 0.15 Sapodilla ...... 0.20 (b) Section 18 emergency exemptions. Sapote, black ...... 0.20 [Reserved] Sapote, mamey ...... 0.20 Sheep, fat ...... 0.02 (c) Tolerances with regional registra- Sheep, liver ...... 0.01 tions. [Reserved] Soybean, seed ...... 0.02

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Parts per Parts per Commodity million Commodity million

Spearmint, oil ...... 20 Peach subgroup 12–12C 1 ...... 0.05 Spearmint, tops ...... 10 Pepper 1 ...... 1.0 Squash/cucumber subgroup 9B ...... 0.02 Sheep, fat 1 ...... 0.020 Star apple ...... 0.20 Sheep, kidney 1 ...... 0.050 Tangerine 1 ...... 0.10 Sheep, liver 1 ...... 0.15 Tea, dried * ...... 15 Sheep, meat 1 ...... 0.030 Tomato ...... 0.20 Sheep, meat byproducts 1 ...... 0.050 1 There are no U.S. registrations for use of etoxazole on 1 There are no U.S. registrations for the commodity since tangerines as of September 26, 2003. August 6, 2014. * There are currently no U.S. registrations for tea as of April 13, 2011. 2 There are no U.S. registrations for orange and orange, oil (b) Section 18 emergency exemptions. as of December 2, 2015. [Reserved] (b) Section 18 emergency exemptions. (c) Tolerances with regional registra- [Reserved] tions. [Reserved] (c) Tolerances with regional registra- (d) Indirect or inadvertent residues. tions. [Reserved] [Reserved] (d) Indirect and inadvertant residues. [68 FR 55512, Sept. 26, 2003, as amended at 78 [Reserved] FR 8416, Feb. 6, 2013; 81 FR 34907, June 1, 2016] [68 FR 55493, Sept. 26, 2003, as amended at 70 FR 41625, July 20, 2005; 72 FR 72963, Dec. 26, § 180.595 Flufenpyr-ethyl; tolerances 2007; 74 FR 25160, May 27, 2009; 76 FR 20542, for residues. Apr. 13, 2011; 77 FR 3621, Jan. 25, 2012; 80 FR (a) General. (1) Tolerances are estab- 75430, Dec. 2, 2015; 81 FR 49169, July 27, 2016; lished for residues of the herbicide, 83 FR 51867, Oct. 15, 2018; 84 FR 66630, Dec. 5, flufenpyr-ethyl; acetic acid, [2-chloro- 2019] 4-fluoro-5-[5-methyl-6-oxo-4- § 180.594 Thiacloprid; tolerances for (trifluoromethyl)-1-(6H)-pyridazinyl]- residues. phenoxy]-ethyl ester], in or on the following commodities: (a) General. Tolerances are established for residues of the insecticide Commodity Parts per thiacloprid, including its metabolites million and degradates in or on the commod- Corn, field, grain ...... 0.01 ities in the following table. Compliance Soybean, seed ...... 0.01 with the tolerance levels specified in Sugarcane, cane ...... 0.01 the following table is to be determined by measuring only thiacloprid ([3-[(6- (2) Tolerances are established for res- chloro-3-pyridinyl)methyl]-2- idues of the herbicide flufenpyr-ethyl; thiazolidinylidene] cyanamide) in or on acetic acid, [2-chloro-4-fluoro-5-[5- the commodity. methyl-6-oxo-4-(trifluoromethyl)-1- (6H)-pyridazinyl]-phenoxy]-ethyl Commodity Parts per ester], and its metabolite, S-3153 acid- million 4-OH; [2-chloro-4-hydroxy-5-[5-methyl- Apple, wet pomace 1 ...... 0.60 6- oxo-4-(trifluoromethyl)-1-(6H)- Cattle, fat 1 ...... 0.020 pyridazinyl]-phenoxy]-acetic acid, free Cattle, kidney 1 ...... 0.050 Cattle, liver 1 ...... 0.15 and conjugated, in or on the following Cattle, meat 1 ...... 0.030 commodities: Cattle, meat byproducts 1 ...... 0.050 Cherry subgroup 12–12A 1 ...... 0.5 Commodity Parts per Cotton, gin byproducts 1 ...... 11.0 million Cotton, undelinted seed 1 ...... 0.020 Fruit, pome, group 11 1 ...... 0.30 Corn, field, forage ...... 0.05 Goat, fat 1 ...... 0.020 Corn, field, stover ...... 0.05 Goat, kidney 1 ...... 0.050 Goat, liver 1 ...... 0.15 (b) Section 18 emergency exemptions. Goat, meat 1 ...... 0.030 Goat, meat byproducts 1 ...... 0.050 [Reserved] Horse, fat 1 ...... 0.020 (c) Tolerances with regional registra- Horse, kidney 1 ...... 0.050 tions. [Reserved] Horse, liver 1 ...... 0.15 Horse, meat 1 ...... 0.030 (d) Indirect or inadvertent residues. Horse, meat byproducts 1 ...... 0.050 [Reserved] Milk 1 ...... 0.030 Peach subgroup 12–12B 1 ...... 0.5 [68 FR 54842, Sept. 19, 2003]

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§ 180.596 Fosthiazate; tolerances for (d) Indirect or inadvertent residues. residues. [Reserved] (a) General. A tolerance is established [69 FR 18263, Apr. 7, 2004] for residues of the insecticide fosthiazate, including its metabolites § 180.598 Novaluron; tolerances for and degradates, in or on the com- residues. modity in the table in this paragraph. (a) General. Tolerances are estab- Compliance with the tolerance level lished for residues of the insecticide specified in this paragraph is to be de- novaluron, including its metabolites termined by measuring only the sum of and degradates, in or on the following fosthiazate, O-ethyl S-(1- commodities. Compliance with the tol- methylpropyl)(2-oxo-3- erance levels specified in the following thiazolidinyl)phosphonothioate, and its table is to be determined by measuring metabolite, O-ethyl S-(1- only novaluron, (N-[[[3-chloro-4-[1,1,2- methylpropyl)(2- trifluoro-2- (methylsulfonyl)ethyl) (trifluoromethoxy)ethoxy]phenyl] phosphoramidothioate, calculated as amino]carbonyl]-2,6- the stoichiometric equivalent of difluorobenzamide), in or on the fol- fosthiazate, in or on the commodity. lowing raw agricultural commodities:

Commodity Parts per Parts per million Commodity million

Tomato ...... 0.02 Apple, wet pomace ...... 8.0 Avocado ...... 0.60 (b) Section 18 emergency exemptions. Bean, dry, seed ...... 0.30 Bean, succulent ...... 0.70 [Reserved] Berry, low growing, subgroup 13-07G, except (c) Tolerances with regional registra- lowbush blueberry ...... 0.45 tions. [Reserved] Brassica, head and stem, subgroup 5A ...... 0.50 Brassica, leafy greens, subgroup 5B ...... 25 (d) Indirect or inadvertent residues. Bushberry subgroup 13-07B ...... 7.0 [Reserved] Carrot ...... 0.05 Cattle, fat ...... 11 [69 FR 18275, Apr. 7, 2004, as amended at 76 Cattle, kidney ...... 1.0 FR 23498, Apr. 27, 2011] Cattle, liver ...... 1.0 Cattle, meat ...... 0.60 Cattle, meat byproducts, except kidney and liver 11 § 180.597 Mesosulfuron-methyl; toler- Cherry subgroup 12–12A ...... 8.0 ances for residues. Corn, sweet, forage ...... 16 (a) General. Tolerances are estab- Corn, sweet, kernel plus cob with husks removed 0.05 Corn, sweet, stover ...... 50 lished for residues of the herbicide Cotton, gin byproducts ...... 30 mesosulfuron-methyl, (methyl 2- Cotton, undelinted seed ...... 0.60 [[[[(4,6-dimethoxy-2-pyrimidinyl) Egg ...... 1.5 Food commodities and feed commodities (other amino]carbonyl]amino]sulfonyl] -4- than those covered by a higher tolerance as a [[(methylsulfonyl)amino] meth- result of use on growing crops) in food and yl]benzoate]) in or on the following raw feed handling establishments ...... 0.01 agricultural commodities: Fruit, pome, group 11–10 ...... 3.0 Goat, fat ...... 11 Goat, kidney ...... 1.0 Parts per Goat, liver ...... 1.0 Commodity million Goat, meat ...... 0.60 Cattle, meat byproducts ...... 0.01 Goat, meat byproducts, except kidney and liver ... 11 Goat, meat byproducts ...... 0 .01 Grain, aspirated fractions ...... 25 Grain, aspirated fractions ...... 0 .60 Hog, fat ...... 1.5 Hog, kidney ...... 0.10 Horse, meat byproducts ...... 0 .01 Hog, liver ...... 0.10 Sheep, meat byproducts ...... 0 .01 Hog, meat ...... 0.07 Wheat, forage ...... 0 .60 Hog, meat byproducts, except kidney and liver .... 1.5 Wheat, germ ...... 0 .10 Horse, fat ...... 11 Wheat, grain ...... 0 .03 Horse, kidney ...... 1.0 Wheat, hay ...... 0 .06 Horse, liver ...... 1.0 Wheat, straw ...... 0 .30 Horse, meat ...... 0.60 Horse, meat byproducts, except kidney and liver 11 (b) Section 18 emergency exemptions. Milk ...... 1.0 [Reserved] Milk, fat ...... 20 Peach subgroup 12–12B ...... 1.9 (c) Tolerances with regional registra- Peanut ...... 0.01 tions. [Reserved] Plum, prune, dried ...... 3.0

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Parts per Parts per Commodity million Commodity million

Plum subgroup 12–12C ...... 1.9 Cattle, fat ...... 0.02 Poultry, fat ...... 7.0 Cattle, meat byproducts ...... 0.02 Poultry, kidney ...... 0.80 Cherry, subgroup 12–12A ...... 1.0 Poultry, liver ...... 0.80 Citrus, oil ...... 30 Poultry, meat ...... 0.40 Cowpea, forage ...... 6.0 Poultry, meat byproducts, except kidney and liver 7.0 Cowpea, hay ...... 18 Sheep, fat ...... 11 Fruit, citrus, group 10–10 ...... 0.35 Sheep, kidney ...... 1.0 Fruit, pome, group 11–10 ...... 0.40 Sheep, liver ...... 1.0 Fruit, small vine climbing, except fuzzy kiwifruit, Sheep, meat ...... 0.60 subgroup 13–07F ...... 1.6 Sheep, meat byproducts, except kidney and liver 11 Goat, fat ...... 0.02 Sorghum, grain, forage ...... 6.0 Goat, meat byproducts ...... 0.02 Sorghum, grain, grain ...... 3.0 Guava ...... 0.90 Sorghum, grain, stover ...... 40 Hop, dried cones ...... 15 Soybean, seed ...... 0.07 Horse, fat ...... 0.02 Sugarcane, cane ...... 0.50 Horse, meat byproducts ...... 0.02 Swiss chard ...... 12 Nut, tree, group 14–12 ...... 0.02 Turnip, greens ...... 25 Sheep, fat ...... 0.02 Vegetable, cucurbit, group 9 ...... 0.20 Sheep, meat byproducts ...... 0.02 Vegetable, fruiting, group 8–10 ...... 1.0 Soybean, vegetable, succulent ...... 0.25 Vegetable, tuberous and corm, subgroup 1C ...... 0.05 Tea, plucked leaves 1 ...... 40 Tropical and subtropical, small fruit, inedible peel, subgroup 24A ...... 2.0 (b) Section 18 emergency exemptions. Vegetable, cucurbit, group 9 ...... 0.30 [Reserved] Vegetable, fruiting, group 8–10 ...... 0.70 (c) Tolerances with regional registra- 1 There are no U.S. registrations as of January 18, 2017 for tions. [Reserved] use on tea. (d) Indirect or inadvertant residues. (b) Section 18 emergency exemptions. [Reserved] [Reserved] [69 FR 31021, June 2, 2004, as amended at 71 (c) Tolerances with regional registra- FR 17014, Apr. 5, 2006; 71 FR 61911, Oct. 20, tions. [Reserved] 2006; 73 FR 74982, Dec. 10, 2008; 74 FR 637, Jan. (d) Indirect or inadvertent residues. 7, 2009; 74 FR 20891, May 6, 2009; 74 FR 65033, [Reserved] Dec. 9, 2009; 75 FR 4278, Jan. 27, 2010; 75 FR 29447, May 26, 2010; 76 FR 55814, Sept. 9, 2011; [69 FR 43533, July 21, 2004, as amended at 73 78 FR 40033, July 3, 2013; 80 FR 43335, July 22, FR 17910, Apr. 2, 2008; 75 FR 70148, Nov. 17, 2015] 2010; 77 FR 25909, May 2, 2012; 81 FR 21756, Apr. 13, 2016; 82 FR 5414, Jan. 18, 2017; 83 FR § 180.599 Acequinocyl; tolerances for 26373, June 7, 2018; 85 FR 29340, May 15, 2020] residues. § 180.600 Propoxycarbazone; toler- (a) General. Tolerances are estab- ances for residues. lished for residues of acequinocyl, in- (a) General. (1) Tolerances are estab- cluding its metabolites and degradates, lished for combined residues of the her- in or on the commodities in the table bicide propoxycarbazone methyl 2- below. Compliance with the tolerance [[[(4,5-dihydro-4-methyl-5-oxo-3- levels specified below is to be deter- propoxy-1H-1,2,4-triazol-1- mined by measuring only the sum of yl)carbonyl]amino]sulfonyl]benzoate acequinocyl [2-(acetyloxy)-3-dodecyl- and its metabolite methyl 2-[[[(4,5- 1,4-naphthalenedione] and its metabo- dihydro-3-(2-hydroxypropoxy)-4-meth- lite, 2-dodecyl-3-hydroxy-1,4- yl-5-oxo-1H-1,2,4-triazol-1-yl)carbonyl] naphthoquinone, calculated as the stoi- amino]sulfonyl]benzoate in/on the fol- chiometric equivalent of acequinocyl, lowing raw agricultural commodities: in or on the commodity. Parts per Parts per Commodity million Commodity million Grass, forage ...... 20 Almond, hulls ...... 2.0 Grass, hay ...... 25 Apple, wet pomace ...... 1.0 Wheat, forage ...... 17 Avocado ...... 0.50 Wheat, grain ...... 0.02 Bean, dry, seed ...... 0.15 Wheat, hay ...... 0.15 Bean, edible podded ...... 0.25 Wheat, straw ...... 0.05 Bean, succulent shelled ...... 0.30 Berry, low growing, subgroup 13–07G ...... 0.50 Bushberry subgroup 13–07B ...... 3 (2) Tolerances are established for res- Caneberry subgroup 13–07A ...... 4.0 idues of the herbicide

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propoxycarbazone methyl 2-[[[(4,5- (c) Tolerances with regional registra- dihydro-4-methyl-5-oxo-3-propoxy-1H- tions. Tolerances with regional reg- 1,2,4-triazol-1-yl)carbonyl] istrations are established for residues amino]sulfonyl]benzoate in/on the fol- of the fungicide cyazofamid, including lowing raw agricultural commodities: its metabolites and degradates, in or on the commodities in the following Parts per Commodity million table. Compliance with the tolerance levels specified in the following table is Cattle, meat ...... 0.05 Cattle, meat byproducts ...... 0.3 to be determined by measuring only Goat, meat ...... 0.05 the sum of 4-chloro-2-cyano-N,N-di- Goat, meat byproducts ...... 0.3 methyl-5-(4-methylphenyl)-1H-imid- Horse, meat ...... 0.05 Horse, meat byproducts ...... 0.3 azole-1-sulfonamide and its metabolite, Milk ...... 0.03 4-chloro-5-(4-methylphenyl)-1H-imid- Sheep, meat ...... 0.05 azole-2-carbonitrile, calculated as the Sheep, meat byproducts ...... 0.3 stoichiometric equivalent of (b) Section 18 emergency exemptions. cyazofamid, in or on the following [Reserved] commodities: (c) Tolerances with regional registra- Parts per tions. [Reserved] Commodity million (d) Indirect or inadvertent residues. [Reserved] Grape ...... 1.5 [69 FR 40781, July 7, 2004, as amended at 71 (d) Indirect or inadvertent residues. FR 52487, Sept. 6, 2006; 74 FR 9377, Mar. 4, [Reserved] 2009] [69 FR 58299, Sept. 30, 2004, as amended at 73 § 180.601 Cyazofamid; tolerances for FR 21839, Apr. 23, 2008; 74 FR 32453, July 8, residues. 2009; 75 FR 40751, July 14, 2010; 77 FR 4252, (a) General. Tolerances are estab- Jan. 27, 2012; 77 FR 59119, Sept. 26, 2012; 81 FR lished for residues of the fungicide 5605, Feb. 3, 2016; 85 FR 15391, Mar. 18, 2020] cyazofamid, including its metabolites and degradates, in or on the commod- § 180.602 Spiroxamine; tolerances for ities in the following table. Compliance residues. with the tolerance levels specified in (a) General. Tolerances are estab- the following table is to be determined lished for residues of the fungicide by measuring only the sum of 4-chloro- spiroxamine, including its metabolites 2-cyano-N,N-dimethyl-5-(4- and degradates, in or on the commod- methylphenyl)-1H-imidazole-1-sul- ities in the table below. Compliance fonamide and its metabolite, 4-chloro- with the tolerance levels specified in 5-(4-methylphenyl)-1H-imidazole-2- the following table is to be determined carbonitrile, calculated as the stoichio- by measuring only spiroxamine, [(8- metric equivalent of cyazofamid, in or (1,1-dimethylethyl)-N-ethyl-N-propyl- on the following commodities: 1,4-dioxaspiro[4,5]decane-2- Parts per methanamine) in or on the commod- Commodity million ities.

Bean, succulent ...... 0.5 Parts per Bean, succulent shelled ...... 0.08 Commodity million Brassica, leafy greens, subgroup 4–16B ...... 15 Bulb vegetables, group3–07 ...... 2.0 Artichoke, globe, import 1 ...... 0.7 Carrot, roots ...... 0.09 Asparagus 1 ...... 0.05 Ginseng ...... 0.3 Banana (import) ...... 3.0 Herb subgroup 19A ...... 90 Hop dried cones ...... 10.0 Grape (import) ...... 1.0 Kohlrabi ...... 1.5 Vegetable, fruiting , crop group 8 1 ...... 1.2 Leafy greens subgroup 4–16A ...... 10 1 No U.S. registration as of December 1, 2010. Vegetable, brassica, head and stem, group 5–16 1.5 Vegetable, cucurbit, group 9 ...... 0.10 (b) Section 18 emergency exemptions. Vegetable, fruiting, group 8–10 ...... 0.9 Vegetable, tuberous and corm, subgroup 1C ...... 0.02 [Reserved] (c) Tolerances with regional registra- (b) [Reserved] tions. [Reserved]

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(d) Indirect or inadvertent residues. ((tetrahydro-3- [Reserved] furanyl)methyl)guanidine in or on the commodities listed in the table below: [69 FR 42570, July 16, 2004, as amended at 75 FR 74640, Dec. 1, 2010; 80 FR 72599, Nov. 20, Parts per 2015] Commodity million § 180.603 Dinotefuran; tolerances for Cattle, fat ...... 0.05 Cattle, meat ...... 0.05 residues. Cattle, meat byproducts ...... 0.05 (a) General. (1) Tolerances are estab- Egg ...... 0.01 Goat, fat ...... 0.05 lished for residues of dinotefuran, (RS)- Goat, meat ...... 0.05 1-methyl-2-nitro-3-((tetrahydro-3- Goat, meat byproducts ...... 0.05 furanyl)methyl)guanidine, including Hog, fat ...... 0.05 its metabolites and degradates, in or Hog, meat ...... 0.05 Hog, meat byproducts ...... 0.05 on the commodities listed in the fol- Horse, fat ...... 0.05 lowing table. Compliance with the tol- Horse, meat ...... 0.05 erance levels specified below is to be Horse, meat byproducts ...... 0.05 Milk ...... 0.05 determined by measuring only the sum Poultry, meat byproducts ...... 0.01 of dinotefuran and its metabolites DN, Sheep, fat ...... 0.05 1-methyl-3-(tetrahydro-3- Sheep, meat ...... 0.05 furylmethyl)guanidine, and UF, 1- Sheep, meat byproducts ...... 0.05 methyl-3-(tetrahydro-3- (3) A tolerance of 0.01 parts per mil- furylmethyl)urea, calculated as the lion is established for residues of the stoichiometric equivalent of insecticide dinotefuran, (RS)-1-methyl- dinotefuran, in or on the commodities 2-nitro-3-((tetrahydro-3- listed in the table below: furanyl)methyl)guanidine, including Parts per its metabolites and degradates, in or Commodity million on all food and/or feed commodities Berry, low growing, except strawberry, subgroup (other than those covered by a higher 13–07H ...... 0.2 tolerance as a result of use on growing Brassica, head and stem, subgroup 5A ...... 1.4 crops or inadvertent residues) when Brassica, leafy greens, subgroup 5B ...... 15.0 residues result from application of Cotton, undelinted seed ...... 0.4 Cotton, gin byproducts ...... 8.0 dinotefuran in food and/or feed han- Fruit, small vine climbing, except fuzzy kiwifruit, dling establishments where food and/or subgroup 13–07F ...... 0.9 feed products are held, stored, proc- Grape, raisin ...... 2.5 Onion, bulb, subgroup 3–07A ...... 0.15 essed, prepared, or served. Compliance Onion, green, subgroup 3–07B ...... 5.0 with the tolerance level is to be deter- Peach ...... 1.0 mined by measuring only dinotefuran. Persimmon 1 ...... 2 Potato, chips ...... 0.1 (b) Section 18 emergency exemptions. Potato, granules/flakes ...... 0.15 Time-limited tolerances are estab- Rice, grain ...... 9.0 lished for residues of dinotefuran, (RS)- Tea, dried2 ...... 50 1-methyl-2-nitro-3-((tetrahydro-3- Tomato, paste ...... 1.0 Turnip, greens ...... 15.0 furanyl)methyl)guanidine, including Vegetable, fruiting, group 8 ...... 0.7 its metabolites and degradates, in or Vegetable, cucurbit, group 9 ...... 0.5 on the commodities in the table below Vegetable, leafy, except Brassica, group 4 ...... 5.0 Vegetable, tuberous and corm, subgroup 1C ...... 0.05 resulting from use of the pesticide pur- Watercress ...... 8.0 suant to FIFRA section 18 emergency 1 There are no U.S. registrations for use of dinotefuran on exemptions. Compliance with the toler- this commodity ance levels specified below is to be de- 2 There are no U.S. registrations for tea. termined by measuring only the sum of (2) Tolerances are established for res- dinotefuran and its metabolites DN, 1- idues of dinotefuran, (RS)-1-methyl-2- methyl-3-(tetrahydro-3- nitro-3-((tetrahydro-3- furylmethyl)guanidine, and UF, 1- furanyl)methyl)guanidine, including methyl-3-(tetrahydro-3- its metabolites and degradates, in or furylmethyl)urea, calculated as the on the commodities listed in the fol- stoichiometric equivalent of lowing table. Compliance with the tol- dinotefuran, in or on the commodities erance levels specified below is to be listed in the table below. The toler- determined by measuring only the sum ances expire and are revoked on the of dinotefuran, (RS)-1-methyl-2-nitro-3- dates specified in the table.

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pyrimidin-2-yl)-6-(trifluoromethyl) Parts per Expiration/ Commodity revocation benzenesulfonamide, in or on the com- million date modity. Fruit, pome, Group 11 ...... 2.0 12/31/21 Fruit, stone, Group 12 ...... 2.0 12/31/21 Commodity Parts per Kiwifruit, fuzzy ...... 0.9 12/31/2022 million

Almond, hulls ...... 0.01 (c) Tolerances with regional registra- Artichoke, globe ...... 0.01 tions. [Reserved] Fish ...... 0.01 (d) Indirect or inadvertent residues. Fish, shellfish, crustacean ...... 0.01 Fish, shellfish, mollusc ...... 0.02 [Reserved] Fruit, pome, group 11–10 ...... 0.01 [70 FR 14546, Mar. 23, 2005, as amended at 74 Fruit, small, vine climbing, subgroup 13–07F, except fuzzy kiwifruit ...... 0.01 FR 12601, Mar. 25, 2009; 74 FR 67104, Dec. 18, Fruit, stone, group 12–12 ...... 0.01 2009; 75 FR 770, Jan. 6, 2010; 77 FR 56138, Sept. Nut, tree, group 14–12 ...... 0.01 12, 2012; 77 FR 67285, Nov. 9, 2012; 77 FR 70913, Olive ...... 0.01 Nov. 28, 2012; 78 FR 21272, Apr. 10, 2013; 78 FR Pomegranate ...... 0.01 24683, Apr. 26, 2013; 79 FR 3512, Jan. 22, 2014; Rice, grain ...... 0.02 80 FR 78145, Dec. 16, 2015; 83 FR 62732, Dec. 6, 2018; 84 FR 49479, Sept. 20, 2019; 84 FR 59936, (b) Section 18 emergency exemptions. Nov. 7, 2019] [Reserved] (c) Tolerances with regional registra- § 180.604 Mepanipyrim; tolerances for tions. [Reserved] residues. (d) Indirect or inadvertent residues. (a) General. [Reserved] [Reserved] (b) Section 18 emergency exemptions. [69 FR 57197, Sept. 24, 2004, as amended at 72 [Reserved] FR 40763, July 25, 2007; 74 FR 18648, Apr. 24, (c) Tolerances with regional registra- 2009; 80 FR 72599, Nov. 20, 2015; 81 FR 10776, tions. [Reserved] Mar. 2, 2016; 85 FR 13552, Mar. 9, 2020] (d) Indirect of inadvertent residues. [Reserved] § 180.607 Spiromesifen; tolerances for (e) Revoked tolerances subject to the residues. channel of trade provisions. [Reserved] (a) General. (1) Tolerances are estab- (f) Import tolerances. Tolerances are lished for residues of the insecticide/ established for the combined residues miticide spiromesifen, including its of mepanipyrim, 4-methyl-N-phenyl-6- metabolites and degradates, in or on (1-propynyl)-2-pyrimidinamine, and its the commodities listed below. Compli- metabolite, 4-methyl-N-phenyl-6-(2- ance with the tolerance levels specified hydroxypropylk)-2-pyrimidinamine, below is to be determined by measuring both free and conjugated in or on the only the sum of spiromesifen [2-oxo-3- following commodities: (2,4,6-trimethylphenyl)-1- oxaspiro[4.4]non-3-en-4-yl 3,3- Parts per Commodity million dimethylbutanoate] and 4-hydroxy-3- (2,4,6-trimethylphenyl)-1- Grape ...... 1.5 Grape, raisin ...... 3.0 oxaspiro[4.4]non-3-en-2-one, calculated Strawberry ...... 1.5 as the stoichiometric equivalent of Tomato ...... 0.5 spiromesifen, in or on the following primary crop commodities: [68 FR 60827, Oct. 13, 2004] Parts per Commodity million § 180.605 Penoxsulam; tolerances for residues. Bean, dry ...... 0.02 Bean, edible podded ...... 0.80 (a) General. Tolerances are estab- Bean, succulent ...... 0.10 lished for residues of penoxsulam, in- Berry and small fruit, low growing berry, sub- cluding its metabolites and degradates, group 13-07G ...... 2.0 in or on the commodities listed in the Brassica, head and stem, subgroup 5A ...... 2.0 Brassica, leafy greens, subgroup 5B ...... 12 table below. Compliance with the toler- Coffee, green bean 1 ...... 0.20 ance levels specified below is to be de- Corn, field, forage ...... 5.0 termined by measuring only Corn, field, grain ...... 0.02 Corn, field, stover ...... 8.0 penoxsulam 2-(2,2-difluoroethoxy)-N- Corn, pop, grain ...... 0.02 (5,8-dimethoxy[1,2,4]triazolo[1,5-c] Corn, pop, stover ...... 4.0

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determined by measuring only the sum Commodity Parts per million of spiromesifen [2-oxo-3-(2,4,6- Corn, sweet, forage ...... 17 trimethylphenyl)-1-oxaspiro[4.4]non-3- Corn, sweet, kernel plus cob with husks removed 0.02 en-4-yl 3,3-dimethylbutanoate] and 4- Corn, sweet, stover ...... 12 hydroxy-3-(2,4,6-trimethylphenyl)-1- Cotton, gin byproducts ...... 15 Cotton, undelinted seed ...... 0.50 oxaspiro[4.4]non-3-en-2-one, calculated Cowpea, forage ...... 30 as the stoichiometric equivalent of Cowpea, hay ...... 86 spiromesifen, in or on the specified ag- Leaf petiole subgroup 4B ...... 6.0 Leafy greens subgroup 4A ...... 12 ricultural commodities, resulting from Pea, dry, seed ...... 0.20 use of the pesticide pursuant to FIFRA Peppermint, tops ...... 45 section 18 emergency exemptions. The Spearmint, tops ...... 45 Tea, dry ...... 40 tolerances expire and are revoked on Tomato, paste ...... 0.80 the date specified in the table. Vegetable, cucurbit, group 9 ...... 0.10 Vegetable, fruiting, group 8 ...... 0.45 Expiration/ Vegetable, tuberous and corm, subgroup 1C ...... 0.02 Commodity Parts per revocation million date 1 This use has not been registered in the United States as of August 28, 2018. Soybean, forage ...... 30 12/31/14 (2) Tolerances are established for res- Soybean, hay ...... 86 12/31/14 idues of the insecticide/miticide Soybean, seed ...... 0.02 12/31/14 spiromesifen, including its metabolites and degradates, in or on the commod- (c) Tolerances with regional registra- ities listed below. Compliance with the tions. [Reserved] tolerance levels specified below is to be (d) Indirect or inadvertent residues. determined by measuring only the sum Tolerances are established for the inad- of spiromesifen [2-oxo-3-(2,4,6- vertent or indirect residues of the in- trimethylphenyl)-1-oxaspiro[4.4]non-3- secticide/miticide spiromesifen, includ- en-4-yl 3,3-dimethylbutanoate] and its ing its metabolites and degradates, in metabolites containing the 4-hydroxy- or on the commodities listed below. 3-(2,4,6-trimethylphenyl)-1- Compliance with the tolerance levels oxaspiro[4.4]non-3-en-2-one and 4-hy- specified below is to be determined by droxy-3-[4-(hydroxymethyl)-2,6- measuring only the sum of dimethylphenyl]-1-oxaspiro[4.4]non-3- spiromesifen [2-oxo-3-(2,4,6- en-2-one moieties, calculated as the trimethylphenyl)-1-oxaspiro[4.4]non-3- stoichiometric equivalent of en-4-yl 3,3-dimethylbutanoate], 4-hy- spiromesifen, in the following livestock droxy-3-(2,4,6-trimethylphenyl)-1- commodities: oxaspiro[4.4]non-3-en-2-one, and its metabolites containing the 4-hydroxy-3-[4- Commodity Parts per (hydroxymethyl)-2,6-dimethylphenyl]- million 1-oxaspiro[4.4]non-3-en-2-one moiety, Cattle, fat ...... 0.10 calculated as the stoichiometric equiv- Cattle, meat ...... 0.02 alent of spiromesifen, in the following Cattle, meat byproducts ...... 0.20 Goat, fat ...... 0.10 rotational crop commodities: Goat, meat ...... 0.02 Goat, meat byproducts ...... 0.20 Commodity Parts per Horse, fat ...... 0.10 million Horse, meat ...... 0.02 Horse, meat byproducts ...... 0.20 Alfalfa, forage ...... 1.5 Milk ...... 0.01 Alfalfa, hay ...... 3.0 Milk, fat ...... 0.25 Barley, grain ...... 0.03 Sheep, fat ...... 0.10 Barley, hay ...... 0.25 Sheep, meat ...... 0.02 Barley, straw ...... 0.15 Sheep, meat byproducts ...... 0.20 Beet, sugar, roots ...... 0.03 Beet, sugar, tops ...... 0.20 (b) Section 18 emergency exemptions. Oat, forage ...... 0.20 Time-limited tolerances specified in Oat, grain ...... 0.03 the following table are established for Oat, hay ...... 0.25 Oat, straw ...... 0.25 residues of the insecticide/miticide Vegetable, bulb, group 3-07 ...... 0.09 spiromesifen, including its metabolites Wheat, forage ...... 0.20 and degradates, in or on the commod- Wheat, grain ...... 0.03 ities listed below. Compliance with the Wheat, hay ...... 0.15 tolerance levels specified below is to be Wheat, straw ...... 0.25

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[70 FR 43283, July 27, 2005, as amended at 72 Parts per FR 3079, Jan. 24, 2007; 73 FR 13140, Mar. 12, Commodity million 2008; 73 FR 52606, Sept. 10, 2008; 74 FR 8492, Feb. 25, 2009; 74 FR 15886, Apr. 8, 2009; 75 FR Horse, fat ...... 0.02 Horse, meat byproducts ...... 0.1 5526, Feb. 3, 2010; 75 FR 53586, Sept. 1, 2010; 76 Horse, meat ...... 0.02 FR 81396, Dec. 28, 2011; 78 FR 3337, Jan. 16, Milk ...... 0.01 2013; 83 FR 45849, Sept. 11, 2018] Milk, fat ...... 0.03 Sheep, fat ...... 0.02 § 180.608 Spirodiclofen; tolerances for Sheep. meat byproducts ...... 0.1 residues. Sheep. meat ...... 0.02 (a) General. (1) Tolerances are estab- (b) Section 18 emergency exemptions. lished for residues of spirodiclofen, in- [Reserved] cluding its metabolites and degradates, (c) Tolerances with regional registra- in or on the commodities listed below. tions. [Reserved] Compliance with the following toler- (d) Indirect or inadvertent residues. ance levels is to be determined by [Reserved] measuring only spirodiclofen (3-(2,4- dichlorophenyl)-2-oxo-1- [70 FR 40211, July 13, 2005, as amended at 73 FR 25539, May 7, 2008; 75 FR 24434, May 5, oxaspiro[4.5]dec-3-en-4-yl 2,2- 2010; 77 FR 73939, Dec. 12, 2012; 79 FR 33464, dimethylbutanoate). June 11, 2014]

Parts per Commodity million § 180.609 Fluoxastrobin; tolerances for residues. Almond, hulls ...... 20.0 Apple, wet pomace ...... 2.4 (a) General. (1) Tolerances are estab- Avocado ...... 1.0 lished for residues of fluoxastrobin, in- Black sapote ...... 1.0 cluding its metabolites and degradates, Canistel ...... 1.0 in or on the commodities in the table Citrus, juice ...... 0.60 Citrus, oil ...... 35 below. Compliance with the tolerance Fruit, citrus, group 10 ...... 0.50 levels specified below is to be deter- Fruit, pome, group 11 ...... 0.80 mined by measuring only Fruit, stone, group 12 ...... 1.0 Grape ...... 2.0 fluoxastrobin, (1E)-[2-[[6-(2- Grape, raisin ...... 6.0 chlorophenoxy)-5-fluoro-4- Hop, dried cones ...... 30 pyrimidinyl]oxy]phenyl](5,6-dihydro- Mamey sapote ...... 1.0 Mango ...... 1.0 1,4,2-dioxazin-3-yl)methanone O- Nut, tree, group 14 ...... 0.10 methyloxime and its Z isomer, (1Z)-[2- Papaya ...... 1.0 [[6-(2-chlorophenoxy)-5-fluoro-4- Pistachio ...... 0.10 pyrimidinyl]oxy]phenyl](5,6-dihydro- Sapodilla ...... 1.0 Star apple ...... 1.0 1,4,2-dioxazin-3-yl)methanone O- methyloxime, calculated as the stoi- (2) Tolerances are established for res- chiometric equivalent of fluoxastrobin. idues of spirodiclofen, including its me- Parts per tabolites and degradates, in or on the Commodity million commodities listed below. Compliance with the following tolerance levels is Avocado ...... 1.0 Barley, grain ...... 0.40 to be determined by measuring only Barley, hay ...... 15 spirodiclofen (3-(2,4-dichlorophenyl)-2- Barley, straw ...... 15 oxo-1-oxaspiro[4.5]dec-3-en-4-yl 2,2- Berry, low growing, subgroup 13-07G ...... 1.9 Corn, field, forage ...... 3.0 dimethylbutanoate) and its metabolite Corn, field, grain ...... 0.02 3-(2,4-dichlorophenyl)-4-hydroxy-1- Corn, field, stover ...... 4.5 oxaspiro[4,5] dec-3-en-2-one, calculated Corn, sweet, forage ...... 13 Corn, sweet, kernel plus cob with husks removed 0.01 as the stoichiometric equivalent of Corn, sweet, stover ...... 10 spirodiclofen. Cotton, gin byproducts ...... 0.01 Cotton, undelinted seed ...... 0.01 Parts per Grain, aspirated grain fractions ...... 60 Commodity million Leaf petioles subgroup 4B ...... 4.0 Melon subgroup 9A ...... 1.5 Cattle, fat ...... 0.02 Pea and bean, dried shelled, except soybean, Cattle, meat byproducts ...... 0.10 subgroup 6C ...... 0.20 Cattle, meat ...... 0.02 Peanut ...... 0.02 Goat, fat ...... 0.02 Peanut, hay ...... 20.0 Goat, meat byproducts ...... 0.1 Peanut, refined oil ...... 0.06 Goat, meat ...... 0.02 Rapeseed, subgroup 20A ...... 0.70

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lites and degradates, in or on the com- Commodity Parts per million modities in the table below, when Rice, grain ...... 4.0 present therein as a result of the appli- Sorghum, grain, forage ...... 5.0 cation of fluoxastrobin to the growing Sorghum, grain, grain ...... 1.5 crops listed in paragraph (a)(1) of this Sorghum, grain, stover ...... 5.0 Soybean, forage ...... 9.0 section. Compliance with the tolerance Soybean, hay ...... 1.2 levels specified below is to be deter- Soybean, hulls ...... 0.20 mined by measuring only Soybean, seed ...... 0.05 Squash/cucumber subgroup 9B ...... 0.50 fluoxastrobin, (1E)-[2-[[6-(2- Tomato, paste ...... 1.5 chlorophenoxy)-5-fluoro-4- Vegetable, fruiting, group 8 ...... 1.0 pyrimidinyl]oxy]phenyl](5,6-dihydro- Vegetable, tuberous and corm, subgroup 1C ...... 0.010 Wheat, forage ...... 7.0 1,4,2-dioxazin-3-yl)methanone O- Wheat, grain ...... 0.15 methyloxime and its Z isomer, (1Z)-[2- Wheat, hay ...... 17 [[6-(2-chlorophenoxy)-5-fluoro-4- Wheat, straw ...... 11 pyrimidinyl]oxy]phenyl](5,6-dihydro- (2) Tolerances are established for res- 1,4,2-dioxazin-3-yl)methanone O- idues of fluoxastrobin, including its methyloxime, calculated as the stoi- metabolites and degradates, in or on chiometric equivalent of fluoxastrobin. the commodities in the table below. Parts per Compliance with the tolerance levels Commodity million specified below is to be determined by Alfalfa, forage ...... 0.050 measuring only fluoxastrobin, (1E)-[2- Alfalfa, hay ...... 0.10 [[6-(2-chlorophenoxy)-5-fluoro-4- Cotton, gin byproducts ...... 0.020 pyrimidinyl]oxy]phenyl](5,6-dihydro- Grain, cereal, forage, fodder, and straw, group 1,4,2-dioxazin-3-yl)methanone O- 16, except corn ...... 0.10 Grass, forage ...... 0.10 methyloxime, its Z isomer, (1Z)-[2-[[6- Grass, hay ...... 0.50 (2-chlorophenoxy)-5-fluoro-4- Vegetable, foliage of legume, group 7 ...... 0.050 pyrimidinyl]oxy]phenyl](5,6-dihydro- 1,4,2-dioxazin-3-yl)methanone O- [74 FR 67113, Dec. 18, 2009, as amended at 75 methyloxime, and its phenoxy- FR 60333, Sept. 30, 2010; 76 FR 50898, Aug. 17, hydroxypyrimidine, 6-(2- 2011; 77 FR 26471, May 4, 2012; 77 FR 64915, chlorophenoxy)-5-fluoro-4-pyrimidinol, Oct. 24, 2012; 79 FR 20105, Apr. 11, 2014; 79 FR calculated as the stoichiometric equiv- 59119, Oct. 1, 2014; 82 FR 45735, Oct. 2, 2017; 84 alent of fluoxastrobin. FR 38143, Aug. 6, 2019]

Parts per § 180.610 Aminopyralid; tolerances for Commodity million residues. Cattle, fat ...... 0.10 (a) General. (1) Tolerances are estab- Cattle, meat ...... 0.05 lished for residues of the herbicide Cattle, meat byproducts ...... 0.20 Goat, fat ...... 0.10 aminopyralid, 4-amino-3,6-dichloro-2- Goat, meat ...... 0.05 pyridinecarboxylic acid, including its Goat, meat byproducts ...... 0.20 metabolites and degradates, in or on Hog, fat ...... 0.03 Hog, meat byproducts ...... 0.06 the commodities in the table below. Horse, fat ...... 0.10 Compliance with the tolerance levels Horse, meat ...... 0.05 specified below is to be determined by Horse, meat byproducts ...... 0.20 measuring only free and conjugated Milk ...... 0.03 Milk, fat ...... 0.75 aminopyralid. Poultry, liver ...... 0.06 Sheep, fat ...... 0.10 Commodity Parts per Sheep, meat ...... 0.05 million Sheep, meat byproducts ...... 0.20 Corn, field, forage ...... 0.30 Corn, field, grain ...... 0.20 (b) Section 18 emergency exemptions. Corn, field, stover ...... 0.20 [Reserved] Grain, aspirated fractions ...... 0.2 (c) Tolerances with regional registra- Grass, forage ...... 25 tions. [Reserved] Grass, hay ...... 50 Wheat, bran ...... 0.1 (d) Indirect or inadvertent residues. Wheat, forage ...... 2.0 Tolerances are established for the indi- Wheat, grain ...... 0.04 rect or inadvertent residues of Wheat, hay ...... 4.0 fluoxastrobin, including its metabo- Wheat, straw ...... 0.25

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(2) Tolerances are established for res- Commodity Parts per idues of the herbicide aminopyralid, 4- million amino-3,6-dichloro-2- Barley, straw ...... 1.0 pyridinecarboxylic acid, including its Egg ...... 0.06 metabolites and degradates, in or on Poultry, fat ...... 0.06 Poultry, meat ...... 0.06 the commodities in the table below. Poultry, meat byproducts ...... 0.06 Compliance with the tolerance levels Wheat, bran ...... 3.0 specified below is to be determined by Wheat, forage ...... 3.5 Wheat, grain ...... 1.3 measuring only aminopyralid. Wheat, hay ...... 2.0 Wheat, straw ...... 1.5 Parts per Commodity million (2) For the combined residues of Cattle, fat ...... 0.02 pinoxaden, 8-(2,6-diethyl-4- Cattle, kidney ...... 0.3 Cattle, meat ...... 0.02 methylphenyl)-1,2,4,5-tetrahydro-7-oxo- Cattle, meat byproducts, except kidney ...... 0.02 7H-pyrazolo[1,2-d][1,4,5] oxadiazepin-9- Goat, fat ...... 0.02 yl 2,2-dimethylpropanoate), and its me- Goat, kidney ...... 0.3 Goat, meat ...... 0.02 tabolites M2, 8-(2,6-diethyl-4-methyl- Goat, meat byproducts, except kidney ...... 0.02 phenyl)-tetrahydro-pyrazolo[1,2- Horse, fat ...... 0.02 d][1,4,5]oxadiazepine-7,9-dione, and free Horse, kidney ...... 0.3 and conjugated forms of M4, 8-(2,6- Horse, meat ...... 0.02 Horse, meat byproducts, except kidney ...... 0.02 diethyl-4-hydroxymethyl-phenyl)- Milk ...... 0.03 tetrahydro-pyrazolo[1,2-d][1,4,5] Sheep, fat ...... 0.02 oxadiazepine-7,9-dione, calculated as Sheep, kidney ...... 0.3 Sheep, meat ...... 0.02 pinoxaden, in/on the following com- Sheep, meat byproducts, except kidney ...... 0.02 modities:

(b) Section 18 emergency exemptions. Commodity Parts per [Reserved] million (c) Tolerances with regional registra- Cattle, fat ...... 0.04 tions. [Reserved] Cattle, meat ...... 0.04 Cattle, meat byproducts ...... 0.04 (d) Indirect or inadvertent residues. Milk ...... 0.02 [Reserved] [70 FR 46428, Aug. 10, 2005, as amended at 75 (b) Section 18 emergency exemptions. FR 17584, Apr. 7, 2010] [Reserved] (c) Tolerances with regional registra- § 180.611 Pinoxaden; tolerances for tions. [Reserved] residues. (d) Indirect or inadvertent residues. (a) General. (1) Tolerances are estab- [Reserved] lished for the combined residues of [70 FR 43322, July 27, 2005] pinoxaden (8-(2,6-diethyl-4- methylphenyl)-1,2,4,5-tetrahydro-7-oxo- § 180.612 Topramezone; tolerances for 7H-pyrazolo[1,2-d][1,4,5] oxadiazepin-9- residues. yl 2,2-dimethylpropanoate), and its me- (a) General. Tolerances are estab- tabolites 8-(2,6-diethyl-4-methyl- lished for residues of the herbicide phenyl)-tetrahydro-pyrazolo[1,2- topramezone, including its metabolites d][1,4,5]oxadiazepine-7,9-dione (M2), and and degradates, in or on the following free and conjugated forms of 8-(2,6- commodities. Compliance with the fol- diethyl-4-hydroxymethyl-phenyl)- lowing tolerance levels is to be deter- tetrahydro-pyrazolo[1,2-d][1,4,5] mined by measuring only topramezone oxadiazepine-7,9-dione (M4), and 4-(7,9- ([3-(4,5-dihydro-3-isoxazolyl)-2-methyl- dioxo-hexahydro-pyrazolo[1,2-d] 4-(methylsulfonyl)phenyl](5-hydroxy-1- [1,4,5]oxadiazepin-8-yl)-3,5-diethyl-ben- methyl-1H-pyrazol-4-yl)methanone) in zoic acid (M6), calculated as pinoxaden, or on the following commodities: in/on the following commodities: Commodity Parts per Parts per million Commodity million Cattle, meat byproducts ...... 0.80 Barley, bran ...... 1.6 Corn, field, forage ...... 0.05 Barley, grain ...... 0.9 Corn, field, grain ...... 0.01 Barley, hay ...... 1.5 Corn, field, stover ...... 0.05

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Parts per Parts per Commodity million Commodity million

Corn, pop, grain ...... 0.01 Hop, dried cones ...... 20.0 Corn, pop, stover ...... 0.05 Kohlrabi ...... 1.5 Corn, sweet, forage ...... 0.05 Leaf petiole vegetable subgroup 22B ...... 4.0 Corn, sweet, kernel plus cob with husks removed 0.01 Leafy greens subgroup 4–16A, except spinach .... 8 Corn, sweet, stover ...... 0.05 Nut, tree, group 14–12 except pistachio ...... 0.15 Fish-freshwater finfish ...... 0.05 Pea and bean, dried shelled, except soybean, Fish-saltwater finfish ...... 0.05 subgroup 6C ...... 3.0 Fish-shellfish, crustacean ...... 0.05 Pea and bean, succulent shelled, subgroup 6B ... 7.0 Fish-shellfish, mollusk ...... 0.05 Pepper/Eggplant, subgroup 8–10B ...... 3.0 Goat, meat byproducts ...... 0.80 Peppermint, tops ...... 7.0 Hog, meat byproducts ...... 0.40 Pistachio ...... 0.60 Horse, meat byproducts ...... 0.80 Potato, granules/flakes ...... 0.40 Poultry, meat byproducts ...... 0.02 Radish, tops ...... 20 Sheep, meat byproducts ...... 0.80 Rapeseed subgroup 20A ...... 1.5 Sugarcane, cane ...... 0.01 Spearmint, tops ...... 7.0 Spinach ...... 9.0 (b) Section 18 emergency exemptions. Sunflower subgroup 20B ...... 0.70 Tea 1 ...... 40 [Reserved] Tomato, paste ...... 2.0 (c) Tolerances with regional registra- Tomato, puree ...... 0.50 tions. [Reserved] Tomato subgroup 8–10A ...... 0.4 Vegetable, brassica, head and stem, group 5–16 1.5 (d) Indirect or inadvertent residues. Vegetable, cucurbit, group 9 ...... 1.5 [Reserved] Vegetable, legume, edible podded, subgroup 6A 4.0 Vegetable, root, except sugar beet, subgroup 1B 0.60 [78 FR 48074, Aug. 7, 2013, as amended at 82 Vegetable, tuberous and corm, subgroup 1C ...... 0.20 FR 35120, July 28, 2017] 1 There are no U.S. registrations for tea as of May 11, 2017. § 180.613 Flonicamid; tolerances for residues. (2) Tolerances are established for the (a) General. (1) Tolerances are estab- residues of the insecticide flonicamid, lished for the residues of the insecti- including its metabolites and cide flonicamid, including its metabo- degradates, in or on the commodities lites and degradates, in or on the com- in the table below. Compliance with modities in the table below. Compli- the tolerance levels specified below is ance with the tolerance levels specified to be determined by measuring only below is to be determined by measuring the sum of flonicamid, N- only the sum of flonicamid, N- (cyanomethyl)-4-(trifluoromethyl)-3- (cyanomethyl)-4-(trifluoromethyl)-3- pyridinecarboxamide, and its metabo- pyridinecarboxamide, and its metabolites, TFNA (4- lites, TFNA (4- trifluoromethylnicotinic acid), and trifluoromethylnicotinic acid), TFNA– TFNA–AM (4- AM (4-trifluoromethylnicotinamide), trifluoromethylnicotinamide), cal- and TFNG, N-(4- culated as the Stoichiometric equiva- trifluoromethylnicotinoyl)glycine, cal- lent of flonicamid, in or on the fol- culated as the stoichiometric equiva- lowing commodities. lent of flonicamid, in or on the fol- Parts per lowing commodities. Commodity million

Parts per Cattle, fat ...... 0.03 Commodity million Cattle, meat ...... 0.08 Cattle, meat byproducts ...... 0.08 Alfalfa, forage ...... 10.0 Egg ...... 0.04 Alfalfa, hay ...... 1.0 Goat, fat ...... 0.03 Alfalfa, seed ...... 1.5 Goat, meat ...... 0.08 Almond, hulls ...... 9.0 Goat, meat byproducts ...... 0.08 Berry, low growing, subgroup 13–07G ...... 1.5 Hog, fat ...... 0.03 Brassica, leafy greens, subgroup 4–16B, except Hog, meat ...... 0.03 radish, tops ...... 16 Hog, meat byproducts ...... 0.03 Celtuce ...... 4.0 Horse, fat ...... 0.03 Cotton, gin byproducts ...... 6.0 Horse, meat ...... 0.08 Cotton, hulls ...... 2.0 Horse, meat byproducts ...... 0.08 Cotton, meal ...... 1.0 Milk ...... 0.05 Cottonseed subgroup 20C ...... 0.60 Poultry, fat ...... 0.03 Florence fennel ...... 4.0 Poultry, meat ...... 0.03 Fruit, citrus, group 10–10 ...... 1.5 Poultry, meat byproducts ...... 0.03 Fruit, pome, group 11–10 ...... 0.20 Sheep, fat ...... 0.03 Fruit, stone, group 12–12 ...... 0.60 Sheep, meat ...... 0.08

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(d) Indirect or inadvertent residues. Commodity Parts per million [Reserved] Sheep, meat byproducts ...... 0.08 [70 FR 51614, Aug. 31, 2005, as amended at 71 FR 15608, Mar. 29, 2006; 73 FR 17923, Apr. 2, (b) Section 18 emergency exemptions. 2008; 77 FR 67776, Nov. 14, 2012; 78 FR 75266, Time-limited tolerances specified in Dec. 11, 2013; 81 FR 52352, Aug. 8, 2016; 82 FR the following table are established for 21945, May 11, 2017; 82 FR 31471, July 7, 2017; residues of the flonicamid, N- 83 FR 3615, Jan. 26, 2018; 83 FR 34780, July 23, (cyanomethyl)-4-(trifluoromethyl)-3- 2018; 84 FR 13808, Apr. 8, 2019; 85 FR 31986, May 28, 2020] pyridinecarboxamide) and its metabolites, TFNA (4- § 180.614 Kasugamycin; tolerances for trifluoromethylnicotinic acid), TFNA- residues. AM (4-trifluoromethylnicotinamide), (a) General. Tolerances are estab- and TFNG (N-(4- lished for residues of kasugamycin, in- trifluoromethylnicotinoyl)glycine), cluding its metabolites and degradates, calculated as the stoichiometric equiv- in or on the commodities listed in the alent of flonicamid, in or on the speci- following table. Compliance with the fied agricultural commodities, result- tolerance levels specified is to be deter- ing from use of the pesticide pursuant mined by measuring only kasugamycin to FFIFRA section 18 emergency ex- (3-O-[2-amino-4-[(carboxyimino-meth- emptions. The tolerances expire on the yl)amino]-2,3,4,6-tetradeoxy-a-D- date specified in the table. arabino-hexopyranosyl]-D-chiro-ino- sitol) in or on the commodity. Parts per Expiration Commodity million date Parts per Commodity million Prickly pear, fruit ...... 1.5 12/31/20 Prickly pear, pads ...... 1.5 12/31/20 Cherry subgroup 12–12A ...... 0.60 Fruit, pome, group 11–10 ...... 0.20 (c) Tolerances with regional registra- Vegetable, fruiting, group 8 1 ...... 0.04 tions. Tolerances with regional reg- Walnut ...... 0.04 istration, as defined by § 180.1(1), are es- 1 There is no U.S. registration as of September 1, 2005. tablished for the residues of the insec- (b) Section 18 emergency exemptions. ticide flonicamid, including its me- [Reserved] tabolites and degradates, in or on the (c) Tolerances with regional registra- commodities in the table below. Com- tions. [Reserved] pliance with the tolerance levels speci- (d) Indirect or inadvertent residues. fied below is to be determined by meas- [Reserved] uring only the sum of flonicamid, N- (cyanomethyl)-4-(trifluoromethyl)-3- [79 FR 51497, Aug. 29, 2014, as amended at 83 pyridinecarboxamide, and its metabo- FR 9446, Mar. 6, 2018] lites, TFNA (4- § 180.615 Amicarbazone; tolerances for trifluoromethylnicotinic acid), TFNA– residues. AM (4-trifluoromethylnicotinamide), and TFNG (N-(4- (a) General. Tolerances are estab- trifluoromethylnicotinoyl)glycine), lished for combined residues of the herbicide, amicarbazone [4-amino-4, 5- calculated as the stoichiometric equiv- dihydro- N-(1,1-dimethylethyl)-3-(1- alent of flonicamid, in or on the fol- methylethyl)-5-oxo-1H-1,2,4-triazole-1- lowing commodities: carboxamide] and its metabolites DA Parts per amicarbazone [N-(1,1-dimethylethyl)- Commodity million 4,5-dihydro-3-(1-methylethyl)-5-oxo-1H- 1,2,4-triazole-1-carboxamide] and iPr-2- Clover, forage ...... 0.90 Clover, hay ...... 5.0 OH DA amicarbazone [N-(1,1- dimethylethyl)-4,5-dihydro-3-(1-hydroxy-1-methylethyl)-5-oxo-1H-1,2,4-triazole-1-carboxamide], calculated as parent equivalents, in or on the following commodities:

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Parts per Parts per Commodity million Commodity million

Cattle, fat ...... 0.01 Wheat, shorts ...... 0.15 Cattle, liver ...... 1.0 Wheat, straw ...... 0.50 Cattle, meat ...... 0.01 Cattle, meat byproducts, except liver ...... 0.10 Corn, field, forage ...... 0.80 [70 FR 55760, Sept. 23, 2005, as amended at 74 Corn, field, grain ...... 0.05 FR 46377, Sept. 9, 2009] Corn, field, stover ...... 1.0 Goat, fat ...... 0.01 § 180.616 Fenpropimorph; tolerances Goat, liver ...... 1.0 Goat, meat ...... 0.01 for residues. Goat, meat byproducts, except liver ...... 0.10 Tolerances are established for the Hog, fat ...... 0.01 Hog, liver ...... 0.10 residues of the fungicide Hog, meat ...... 0.01 fenpropimorph (rel-(2R,6S)-4-[3-[4-(1,1- Hog, meat byproducts, except liver ...... 0.01 dimethylethyl)phenyl]-2- Horse, fat ...... 0.01 Horse, liver ...... 1.0 methylpropyl]-2,6-dimethylmorpholine) Horse, meat ...... 0.01 in or on the following commodity: Horse, meat byproducts, except liver ...... 0.10 Milk ...... 0.01 Commodity Parts per Sheep, fat ...... 0.01 million Sheep, liver ...... 1.0 Sheep, meat ...... 0.01 Banana* ...... 2.0 Sheep, meat byproducts, except liver ...... 0.10 *No U.S. registration as of February 10, 2006. Poultry, liver ...... 0.10 (b) Section 18 emergency exemptions. (b) Section 18 emergency exemptions. [Reserved] [Reserved] (c) Tolerances with regional registra- (c) Tolerances with regional registrations. [Reserved] tions. [Reserved] (d) Indirect or inadvertent residues. (d) Indirect or inadvertent residues. [Reserved] Tolerances are established for the indi- [71 FR 15612, Mar. 29, 2006] rect or inadvertent residues of amicarbazone [4-amino-4, 5-dihydro-N- § 180.617 Metconazole; tolerances for (1,1-dimethylethyl)-3-(1-methylethyl)-5- residues. oxo-1H-1,2,4-triazole-1-carboxamide] (a) General. Tolerances are estab- and its metabolites DA amicarbazone lished for residues of metconazole, in- [N-(1,1-dimethylethyl)-4,5-dihydro-3-(1- cluding its metabolites and degradates, methylethyl)-5-oxo-1H-1,2,4-triazole-1- in or on the commodities in the fol- carboxamide] and iPr-2-OH DA lowing table. Compliance with the tol- amicarbazone [N-(1,1-dimethylethyl)- erance levels specified below is to be 4,5-dihydro-3-(1-hydroxy-1- determined by measuring only methylethyl)-5-oxo-1H-1,2,4-triazole-1- metconazole [5-[(4- carboxamide], calculated as parent chlorophenyl)methyl]-2,2-dimethyl-1- equivalents, in or on the following (1H-1,2,4-triazol-1- commodities when present therein as a ylmethyl)cyclopentanol] as the sum of result of application of amicarbazone its cis- and trans-isomers in or on the to the growing crops in paragraph (a) following commodities: of this section: Parts per Parts per Commodity million Commodity million Almond, hulls ...... 4.0 Alfalfa, forage ...... 0.05 Banana 1 ...... 0.1 Alfalfa, hay ...... 0.10 Barley, grain ...... 2.5 Cotton, gin byproducts ...... 0.30 Barley, hay ...... 7.0 Cotton, undelinted seed ...... 0.07 Barley, straw ...... 7.0 Soybean, forage ...... 1.50 Beet, sugar, dried pulp ...... 0.70 Soybean, hay ...... 5.0 Beet, sugar, molasses ...... 0.08 Soybean, seed ...... 0.80 Beet, sugar, roots ...... 0.07 Wheat, bran ...... 0.15 Bushberry subgroup 13–07B ...... 0.40 Wheat, flour ...... 0.15 Cattle, meat byproducts ...... 0.04 Wheat, forage ...... 0.50 Corn, field, forage ...... 3.0 Wheat, germ ...... 0.15 Corn, field, grain ...... 0.02 Wheat, grain ...... 0.10 Corn, field, stover ...... 30 Wheat, hay ...... 1.0 Corn, pop, grain ...... 0.02 Wheat, middlings, ...... 0.15 Corn, pop, stover ...... 30

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Parts per Parts per Commodity million Commodity million

Corn, sweet, forage ...... 3.0 Grape, imported ...... 0.25 Corn, sweet, kernel plus cob with husks removed 0.01 Grape, raisin ...... 1.0 Corn, sweet, stover ...... 30.0 Tomato ...... 0.45 Cotton, gin byproducts ...... 8.0 Note: There are no U.S. registrations as of July 30, 2006. Cotton, undelinted seed ...... 0.25 Egg ...... 0.04 (b) Section 18 emergency exemptions. Fruit, stone, group 12–12 ...... 0.2 [Reserved] Goat, meat byproducts ...... 0.04 (c) Tolerances with regional registra- Grain, aspirated grain fractions ...... 7.0 tions. [Reserved] Horse, meat byproducts ...... 0.04 Nut, tree, group 14–12 ...... 0.04 (d) Indirect of inadvertent residues. Oat, grain ...... 1.0 [Reserved] Oat, hay ...... 17 [71 FR 52003, Sept. 1, 2006] Oat, straw ...... 6.0 Pea and bean, dried shelled, except soybean, subgroup 6C ...... 0.15 § 180.619 Epoxiconazole; tolerances for Peanut ...... 0.04 residues. Peanut, refined oil ...... 0.05 (a) General. Tolerances are estab- Rapeseed subgroup 20A ...... 0.08 lished for the residues of the fungicide Rye, grain ...... 0.25 Rye, straw ...... 14 epoxiconazole [(rel-1-[[(2R,3S)-3-(2- Sheep, meat byproducts ...... 0.04 chlorophenyl)-2-(4- Soybean, forage ...... 3.0 fluorophenyl)oxiranyl]methyl]-1H-1,2,4- Soybean, hay ...... 6.0 triazole]) in or on the following com- Soybean, hulls ...... 0.08 modities: Soybean, seed ...... 0.05 Sugarcane, cane ...... 0.06 Parts per Sunflower subgroup 20B ...... 0.7 Commodity million Vegetable, tuberous and corn, subgroup 1C ...... 0.04 Wheat, grain ...... 0.15 Banana * ...... 0 .5 Wheat, hay ...... 16 Coffee * ...... 0 .05 Wheat, milled byproducts ...... 0.20 * No U.S. Registration as of August 4, 2006 Wheat, straw ...... 18 (b) Section 18 emergency exemptions. 1 No U.S. registration as of August 30, 2006. [Reserved] (b) Section 18 emergency exemptions. (c) Tolerances with regional Registra- [Reserved] tions. [Reserved] (c) Tolerances with regional registra- (d) Indirect or inadvertent residues. tions. [Reserved] [Reserved] (d) Indirect or inadvertent residues. [71 FR 53989, Sept. 13, 2006] [Reserved] [71 FR 56388, Sept. 27, 2006, as amended at 71 § 180.620 Etofenprox; tolerances for FR 76196, Dec. 20, 2006; 73 FR 22828, Apr. 28, residues. 2008; 74 FR 21266, May 7, 2009; 76 FR 50904, (a) General. A tolerance is established Aug. 17, 2011; 76 FR 81396, Dec. 28, 2011; 77 FR for residues of the insecticide 26456, May 4, 2012; 77 FR 66723, Nov. 7, 2012; 79 etofenprox, including its metabolites FR 12411, Mar. 5, 2014; 80 FR 30625. May 29, and degradates, in or on the com- 2015] modity in the table in this paragraph. § 180.618 Benthiavalicarb-isopropyl; Compliance with the tolerance level tolerance for residues. specified in this paragraph is to be determined by measuring only (a) General. Tolerances are estab- etofenprox, 2-(4-ethoxyphenyl)-2- lished for the combined residues of methylpropyl 3-phenoxybenzyl ether, benthiavalicarb-isopropyl, in or on the commodity. isopropyl[(S)-1-[[[(1R)-1-(6-fluoro-2- benzothiazolyl)ethyl]amino] carbonyl]- Commodity Parts per 2-methylpropyl]carbamate and million isopropyl[(S)-1-[[[(1S)-1-(6-fluoro-2- Cattle, fat ...... 10.0 benzothiazolyl)ethyl]amino] carbonyl]- Cattle, meat ...... 0.40 2-methylpropyl]carbamate, in or on the Cattle, meat byproducts ...... 10.0 Egg ...... 0.40 following raw agricultural commod- All food commodities (including feed commodities: ities) not otherwise listed in this subsection ...... 5.0

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ance levels specified below is to be de- Commodity Parts per million termined by measuring only Goat, fat ...... 10.0 ethaboxam (N-(cyano-2-thienylmethyl)- Goat, meat ...... 0.40 4-ethyl-2-(ethylamino)-5- Goat, meat byproducts ...... 10.0 thiazolecarboxamide) in or on the com- Hog, fat ...... 4.0 Hog, meat ...... 0.20 modity. Hog, meat byproducts ...... 4.0 Horse, fat ...... 10.0 Commodity Parts per Horse, meat ...... 0.40 million Horse, meat byproducts ...... 10.0 Milk ...... 0.60 Ginseng ...... 0.10 1 Poultry, fat ...... 1.0 Grape ...... 6.0 Poultry, meat ...... 0.01 Pepper/eggplant subgroup 8–10B ...... 0.90 Poultry, meat byproducts ...... 1.0 Vegetable, cucurbit, group 9 ...... 0.30 Rice, grain ...... 0.01 Vegetable, tuberous and corm, subgroup 1C ...... 0.01 Sheep, fat ...... 10.0 1 There is no U.S. registration as of September 27, 2006. Sheep, meat ...... 0.40 Sheep, meat byproducts ...... 10.0 (b) Section 18 emergency exemptions. [Reserved] (b) Section 18 emergency exemptions. (c) Tolerances with regional registra- [Reserved] tions. [Reserved] (c) Tolerances with regional registra- (d) Indirect or inadvertent residues. tions. [Reserved] [Reserved] (d) Indirect or inadvertent residues. [Reserved] [71 FR 56392, Sept. 27, 2006, as amended at 82 FR 36090, Aug. 3, 2017] [76 FR 23498, Apr. 27, 2011, as amended at 78 FR 70877, Nov. 27, 2013] § 180.623 Flufenoxuron; tolerances for residues. § 180.621 Dithianon; tolerances for residues. (a) General. Tolerances are established for residues of the insecticide, (a) General. Tolerances are estab- flufenoxuron, 1-[4-(2-chloro-a,a,a- lished for residues of dithianon, includ- trifluoro-p-tolyloxy)-2-fluorophenyl]-3- ing its metabolites and degradates, in (2,6-difluorobenzoyl)urea, in or on the or on the commodities in the table following food commodities. below. Compliance with the tolerance levels specified below is to be deter- Commodity Parts per mined by measuring only dithianon, 5, million 10-dihydro-5,10-dioxonaphtho(2,3-b)-1,4- Apple 1 ...... 0.50 dithiin-2,3-dicarbonitrile. Cattle, fat 1 ...... 4.5 Cattle, meat 1 ...... 0.10 Parts per Cattle, meat byproducts 1 ...... 0.50 Commodity million Goat, fat 1 ...... 4.5 Goat, meat 1 ...... 0.10 Fruit, pome, group 111 ...... 5 Goat, meat byproducts 1 ...... 0.50 Grape 2 ...... 3 Grape 1 ...... 0.70 Hop, dried cones1 ...... 100 Grape, raisin 1 ...... 2.0 1 1 Horse, fat ...... 4.5 No U.S. registration as of September 5, 2006. 1 2No U.S. registration as of January 29, 2010. Horse, meat ...... 0.10 Horse, meat byproducts 1 ...... 0.50 (b) Section 18 emergency exemptions. Milk ...... 0.20 [Reserved] Milk, fat 1 ...... 4.0 Orange 1 ...... 0.30 (c) Tolerances with regional registra- Orange, oil 1 ...... 60 tions. [Reserved] Pear 1 ...... 0.50 (d) Indirect or inadvertent residues. Sheep, fat 1 ...... 4.5 Sheep, meat 1 ...... 0.10 [Reserved] Sheep, meat byproducts 1 ...... 0.50 [75 FR 5522, Feb. 3, 2010] 1There are no U.S. registrations as of September 30, 2006. § 180.622 Ethaboxam; tolerances for (b) Section 18 emergency exemptions. residues. [Reserved] (c) Tolerances with regional restric- (a) General. Tolerances are estab- [Reserved] lished for residues of ethaboxam, in- tions. (d) cluding its metabolites and degradates, Indirect or inadvertent residues. in or on the commodities listed in the [Reserved] table below. Compliance with the toler- [71 FR 57436, Sept. 29, 2006]

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§ 180.624 Metrafenone; tolerances for § 180.626 Prothioconazole; tolerances residues. for residues. (a) General. Tolerances are estab- (a) General. (1) Tolerances are established for residues of the fungicide lished for residues of prothioconazole, metrafenone, including its metabolites 2-[2-(1-chlorocylcopropyl)-3-(2- and degradates, in or on the commod- chlorophenyl)-2-hydroxypropyl]-1,2- ities in the table below. Compliance dihydro-3H-1,2,4-triazole-3-thion, in- with the tolerance levels specified in cluding its metabolites and degradates, the following table is to be determined in or on the commodities in the table by measuring only metrafenone (3- below. Compliance with the tolerance bromo-6-methoxy-2- levels specified below is to be deter- methylphenyl)(2,3,4-trimethoxy-6- mined by measuring only methylphenyl)methanone in or on the prothioconazole and its metabolite following commodities: prothioconazole-desthio, or a-(1- chlorocyclopropyl)-a-[(2- Parts per chlorophenyl)methyl]-1H-1,2,4-triazole- Commodity million 1-ethanol, calculated as parent in or on Apricot ...... 0.70 the commodity. Cherry subgroup 12–12A ...... 2.0 Fruit, pome, group 11–10 ...... 1.5 Commodity Parts per Fruit, small, vine climbing, except fuzzy kiwifruit, million subgroup 13–07F ...... 4.5 Grape, raisin ...... 17 Alfalfa, forage ...... 0.02 Hop, dried cones ...... 70 Alfalfa, hay ...... 0.02 Beet, sugar, roots ...... 0.25 Peach subgroup 12–12B ...... 0.70 Berry, low growing, except strawberry, subgroup Vegetable, cucurbit, group 9 ...... 0.50 13–07H ...... 0.20 Vegetable, fruiting, group 8–10 ...... 0.90 Bushberry, subgroup 13–07B ...... 2.0 White button mushroom ...... 0.50 Corn, sweet kernel plus cob with husks removed 0.04 Cotton, gin byproducts ...... 4.0 (b) Section 18 emergency exemption. Cottonseed subgroup 20C ...... 0.4 Grain, aspirated grain fractions ...... 11 [Reserved] Grain, cereal, forage, fodder and straw, group 16, (c) Tolerances with regional registra- except sorghum, and rice; forage ...... 8.0 tions. [Reserved] Grain, cereal, forage, fodder and straw, group 16, except sorghum, and rice; hay ...... 7.0 (d) Indirect or inadvertent residues. Grain, cereal, forage, fodder and straw, group 16, [Reserved] except sorghum, and rice; stover ...... 10 Grain, cereal, forage, fodder and straw, group 16, [71 FR 54917, Sept. 20, 2006, as amended at 75 except sorghum, straw ...... 5.0 FR 75393, Dec. 3, 2010; 79 FR 63053, Oct. 22, Grain, cereal, group 15, except sweet corn and 2014; 84 FR 12520, Apr. 2, 2019] sorghum ...... 0.35 Pea and bean, dried shelled, except soybean, subgroup 6C ...... 0.9 § 180.625 Orthosulfamuron; tolerances Peanut ...... 0.02 for residues. Potato ...... 0.02 (a) General. Tolerances are estab- Rapeseed subgroup 20A ...... 0.15 Rice, hulls ...... 0.90 lished for residues of orthosulfamuron Soybean, forage ...... 4.5 1-(4,6-dimethoxypyrimidin-2-yl)-3-[2- Soybean, hay ...... 17 (dimethylcarbamoyl)- Soybean, seed ...... 0.15 Sunflower subgroup 20B 1 ...... 0.2 phenylsulfamoyl] urea) per se in or on Vegetable, cucurbit, crop group 9 ...... 0.30 the following commodities: 1 There are no U.S. registrations allowing use of prothioconazole on the commodities in the Sunflower sub- Parts per group 20B as of August 16, 2017. Commodity million (2) Tolerances are established for res- Rice, grain ...... 0.05 idues of prothioconazole, 2-[2-(1- chlorocylcopropyl)-3-(2-chlorophenyl)- (b) Section 18 emergency exemptions. 2-hydroxypropyl]-1,2-dihydro-3H-1,2,4- [Reserved] triazole-3-thion, including its metabo- (c) Tolerances with regional registra- lites and degradates, in or on the com- tions. [Reserved] modities in the table below. Compli- (d) Indirect and inadvertant residues. ance with the tolerance levels specified [Reserved] below is to be determined by measuring [72 FR 8931, Feb. 28, 2007, as amended at 80 only prothioconazole and its metabo- FR 72599, Nov. 20, 2015] lites prothioconazole-desthio, or a-(1- 698

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chlorocyclopropyl)- -[(2- a Commodity Parts per chlorophenyl)methyl]-1H-1,2,4-triazole- million 1-ethanol, and conjugates that can be Brassica, head and stem, subgroup 5A ...... 5.0 converted to these two compounds by Citrus, dried pulp ...... 0.03 acid hydrolysis, calculated as parent in Citrus, oil ...... 1.0 Fruit, citrus, crop group 10–10 ...... 0.01 or on the commodity. Fruit, small, vine climbing, except fuzzy kiwifruit, subgroup 13–07F ...... 2.0 Parts per Grape, raisin ...... 6.0 Commodity million Hop, dried cones ...... 15 Cattle, fat ...... 0.1 Potato, granules/flakes ...... 0.15 Cattle, meat ...... 0.02 Potato, processed potato waste ...... 0.2 Cattle, meat byproducts ...... 0.2 Vegetable, brassica (cole) leafy subgroup 5B ...... 18 Goat, fat ...... 0.1 Vegetable, bulb, crop group 3–07 ...... 7.0 Goat, meat ...... 0.02 Vegetable, cucurbit, group 9 ...... 0.50 Goat, meat byproducts ...... 0.2 Vegetable, fruiting, crop group 8–10 ...... 1.6 Hog, meat byproducts ...... 0.05 Vegetable, leafy, except brassica, group 4 ...... 25 Horse, fat ...... 0.1 Vegetable, leaves of root and tuber, group 2 ...... 15.0 Horse, meat ...... 0.02 Vegetable root, subgroup 1A ...... 0.15 Horse, meat byproducts ...... 0.2 Vegetable, tuberous and corm, subgroup 1C ...... 0.09 Milk ...... 0.02 Poultry liver ...... 0.02 (b) Section 18 emergency exemptions. Sheep, fat ...... 0.1 Sheep, meat ...... 0.02 [Reserved] Sheep, meat byproducts ...... 0.2 (c) Tolerances with regional registrations. [Reserved] (b) Section 18 emergency exemptions. (d) Indirect or inadvertent residues. [Reserved] Tolerances are established for residues (c) Tolerances with regional registra- of the fungicide fluopicolide [2,6- tions. [Reserved] dichloro-N-[[3-chloro-5- (d) Indirect or inadvertent residues. (trifluoromethyl)-2- [Reserved] pyridinyl]methyl]benzamide], includ- [72 FR 11783, Mar. 14, 2007, as amended at 73 ing its metabolites and degradates, in FR 14719, Mar. 19, 2008; 74 FR 14749, Apr. 1, or on the commodities in the table in 2009; 74 FR 46699, Sept. 11, 2009; 75 FR 29914, this paragraph. Compliance with the May 28, 2010; 76 FR 61592, Oct. 5, 2011; 78 FR tolerance levels specified below is to be 67052, Nov. 8, 2013; 81 FR 78923, Nov. 10, 2016; determined by measuring only 82 FR 38846, Aug. 16, 2017; 83 FR 52991, Oct. 19, fluopicolide [2,6-dichloro-N-[[3-chloro-5- 2018] (trifluoromethyl)-2- § 180.627 Fluopicolide; tolerances for pyridinyl]methyl]benzamide] in or on residues. the commodity. (a) General. Tolerances are estab- Commodity Parts per lished for residues of the fungicide million fluopicolide [2,6-dichloro-N-[[3-chloro-5- Corn, field, forage ...... 0.08 (trifluoromethyl)-2- Corn, field, grain ...... 0.01 pyridinyl]methyl]benzamide], includ- Corn, field, stover ...... 0.20 Wheat, aspirated grain fractions ...... 0.07 ing its metabolites and degradates, in Wheat, forage ...... 0.20 or on the commodities in the table in Wheat, grain ...... 0.02 this paragraph. Compliance with the Wheat, hay ...... 0.50 tolerance levels specified below is to be Wheat, milled byproducts ...... 0.07 Wheat, straw ...... 0.50 determined by measuring only fluopicolide [2,6-dichloro-N-[[3-chloro-5- (trifluoromethyl)-2- [72 FR 14447, Mar. 28, 2007, as amended at 73 pyridinyl]methyl]benzamide] in or on FR 5455, Jan. 30, 2008; 73 FR 30498, May 28, 2008; 76 FR 22054, Apr. 20, 2011; 79 FR 12401, the commodity. Mar. 5, 2014; 79 FR 45693, Aug. 6, 2014; 81 FR 65924, Sept. 26, 2016; 83 FR 9712, Mar. 7, 2018] Parts per Commodity million § 180.628 Chlorantraniliprole; toler- Basil, dried, leaves ...... 200 ances for residues. Basil, fresh leaves ...... 40 Bean, moth, succulent ...... 0.90 (a) General. Tolerances are estab- Bean, runner, succulent ...... 0.90 lished for residues of the insecticide Bean, snap, succulent ...... 0.90 Bean, wax, succulent ...... 0.90 chlorantraniliprole, including its me- Bean, yardlong, succulent ...... 0.90 tabolites and degradates, in or on the

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commodities in the table below. Com- Commodity Parts per pliance with the tolerance levels speci- million fied below is to be determined by meas- Hog, meat byproducts ...... 0.05 uring only chlorantraniliprole, 3- Hop, dried cones 1 ...... 90 bromo-N-[4-chloro-2-methyl-6-[(methyl Hop, dried cones ...... 40 Horse, fat ...... 0.5 amino)carbonyl]phenyl]-1-(3-chloro-2- Horse, meat ...... 0.1 pyridinyl)-1H-pyrazole-5-carboxamide. Horse, meat byproducts ...... 0.5 Ilama ...... 4.0 Parts per Jaboticaba ...... 2.0 Commodity million Longan ...... 4.0 Lychee ...... 2.0 Acerola ...... 2.0 Mango ...... 4.0 Alfalfa, seed ...... 7.0 Milk ...... 0.1 Almond, hulls ...... 5.0 Nut, tree, group 14 1 ...... 0.04 Animal feed, nongrass, group 18, forage ...... 25 Nut, tree, group 14–12 ...... 0.02 Animal feed, nongrass, group 18, hay ...... 90 Olive ...... 4.0 Apple, wet pomace ...... 2.5 Olive, oil ...... 40 Artichoke, globe 1 ...... 4.0 Onion, bulb, subgroup 3–07A ...... 0.30 Artichoke, globe ...... 2.0 Onion, green, subgroup 3–07B ...... 3.0 Asparagus ...... 13 Palm, oil 2 ...... 1.5 Atemoya ...... 4.0 Papaya ...... 4.0 Avocado ...... 4.0 Passionfruit ...... 4.0 Banana ...... 4.0 Peanut ...... 0.06 Beet, sugar, molasses ...... 9.0 Peanut, hay ...... 90 Berry, large shrub/tree, subgroup 13–07C ...... 2.5 Peppermint, tops ...... 9.0 Berry, low growing, subgroup 13–07G ...... 1.0 Persimmon ...... 4.0 Biriba ...... 4.0 Pineapple ...... 1.5 Brassica, head and stem, subgroup 5A ...... 4.0 Pineapple, process residue ...... 3.0 Brassica, leafy greens, subgroup 5B ...... 11 Pistachio 1 ...... 0.04 Bushberry, subgroup 13–07B ...... 2.5 Pomegranate ...... 4.0 Cacao bean ...... 0.08 Poultry, fat ...... 0.2 Cacao bean, chocolate ...... 1.5 Poultry, meat ...... 0.05 Cacao bean, cocoa powder ...... 1.5 Poultry, meat byproducts ...... 0.2 Cacao bean, roasted bean ...... 0.8 Pulasan ...... 4.0 Cactus ...... 13 Quinoa, forage ...... 40 Canistel ...... 4.0 Quinoa, grain ...... 6.0 Cattle, fat ...... 0.5 Quinoa, hay ...... 40 Cattle, meat ...... 0.1 Quinoa, straw ...... 40 Cattle, meat byproducts ...... 0.5 Rambutan ...... 4.0 Cherimoya ...... 4.0 Rapeseed subgroup 20A ...... 2.0 Citrus, dried pulp ...... 14 Rice, grain ...... 0.15 Coffee, green bean ...... 0.4 Rice, hulls ...... 0.4 Coffee, instant ...... 2.0 Sapodilla ...... 4.0 Corn, field, grain ...... 0.04 Sapote, black ...... 4.0 Corn, field, milled byproducts ...... 0.1 Sapote, mamey ...... 4.0 Corn, pop, grain ...... 0.04 Sapote, white ...... 4.0 Sheep, fat ...... 0.5 Corn, sweet, kernel plus cobs with husk removed 0.02 Sheep, meat ...... 0.1 Cotton, gin byproduct ...... 30 Sheep meat byproducts ...... 0.5 Cotton, hulls ...... 0.40 Soursop ...... 4.0 Cottonseed subgroup 20C ...... 0.3 Spanish lime ...... 4.0 Crayfish ...... 8.0 Spearmint, tops ...... 9.0 Custard apple ...... 4.0 Spice, subgroup 19B ...... 90 Egg ...... 1.0 Star apple ...... 4.0 Feijoa ...... 4.0 Starfruit ...... 4.0 Fig ...... 4.0 Sugar apple ...... 4.0 Fruit, caneberry, subgroup 13–07A ...... 1.8 Sugarcane, cane ...... 14 Fruit, citrus, group 10–10 ...... 1.4 Sugarcane, molasses ...... 420 Fruit, pome, group 11–10 ...... 1.2 Sunflower subgroup 20B ...... 2.0 Fruit, small vine climbing, subgroup 13–07F ...... 2.5 Tea, dried ...... 50.0 Fruit, stone, group 12–12 ...... 2.5 Teff, forage ...... 40 Fruit, stone, group 12–12, except cherry, chicka- Teff, grain ...... 6.0 1 saw plum, and damson plum ...... 4.0 Teff, hay ...... 40 Goat, fat ...... 0.5 Teff, straw ...... 40 Goat, meat ...... 0.1 Ti, leaves ...... 13.0 Goat, meat byproducts ...... 0.5 Ti, root ...... 0.3 Grain, aspirated grain fractions ...... 640 Vegetable, cucurbit, group 9 ...... 0.5 Grain, cereal, except rice and corn, group 15 ...... 6.0 Vegetable, foliage of legume, group 7 ...... 90 Grain, cereal, forage, fodder and straw, group 16 40 Vegetable, fruiting, group 8–10 ...... 1.4 Grape, raisin ...... 5.0 Vegetable, leafy, except brassica, group 4 ...... 13 Grass forage, fodder and hay, group 17 ...... 90 Vegetable, leaves of root and tuber, group 2 ...... 40.0 Guava ...... 4.0 Vegetable, legume, group 6 ...... 2.0 Herb subgroup 19A, dried leaves ...... 90 Vegetable, root and tuber, group 1 ...... 0.30 Herb subgroup 19A, fresh leaves ...... 25 Wax jambu ...... 4.0 Hog, fat ...... 0.05 Hog, meat ...... 0.02 1 This tolerance expires on December 14, 2016.

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2 There are no U.S. registrations for use of Parts per chlorantraniliprole on this commodity. Commodity million

(b) Section 18 emergency exemptions. Egg ...... 0.02 [Reserved] Fruit, pome, group 11–09 ...... 0.40 (c) Tolerances with regional registra- Fruit, stone, group 12–10 ...... 1.5 tions. [Reserved] Goat, fat ...... 0.2 (d) Indirect or inadvertent residues. Goat, liver ...... 1.5 [Reserved] Goat, meat byproducts, except liver ...... 0.08 Goat, muscle ...... 0.05 [75 FR 5532, Feb. 3, 2010, as amended at 75 FR Grain, aspirated fractions ...... 6.0 17566, Apr. 7, 2010; 76 FR 44821, July 27, 2011; Grape ...... 1.5 76 FR 59909, Sept. 28, 2011; 77 FR 60315, Oct. 3, Grape, raisin ...... 2.4 2012; 77 FR 75561, Dec. 21, 2012; 78 FR 57285, Guiana chestnut ...... 0.02 Sept. 18, 2013; 79 FR 7401, Feb. 7, 2014; 81 FR Hazelnut ...... 0.02 38604, June 14, 2016; 81 FR 61619, Sept. 7, 2016; Heartnut ...... 0.02 84 FR 53326, Oct. 7, 2019] Hickory nut ...... 0.02 Hog, fat ...... 0.01 § 180.629 Flutriafol; tolerances for resi- Hog, meat byproducts ...... 0.05 dues. Hog, muscle ...... 0.01 Hop, dried cones ...... 20 (a) General. Tolerances are estab- Horse, fat ...... 0.2 lished for the residues of flutriafol, Horse, liver ...... 1.5 [(±)-a-(2-fluorophenyl)-a-(4- Horse, meat byproducts, except liver ...... 0.08 fluorophenyl)-1H-1,2,4-triazole-1-eth- Horse, muscle ...... 0.05 anol], including its metabolites and Japanese horse-chestnut ...... 0.02 degradates in or on the following com- Lettuce, head ...... 1.5 Macadamia nut ...... 0.02 modities. Compliance with the fol- Milk ...... 0.02 lowing tolerances is to be determined Mongongo nut ...... 0.02 by measuring flutriafol only. Monkey-pot ...... 0.02 Pachira nut ...... 0.02 Commodity Parts per Peanut ...... 0.09 million Peanut, hay ...... 15 African tree nut ...... 0.02 Pecan ...... 0.02 Alfalfa, forage ...... 20 Poultry, fat ...... 0.02 Alfalfa, hay ...... 70 Poultry, meat byproducts ...... 0.02 Almond ...... 0.60 Radicchio ...... 1.5 Almond, hull ...... 15 Sapucaia nut ...... 0.02 1 Banana ...... 0.30 Sheep, fat ...... 0.2 Barley, grain ...... 1.5 Sheep, liver ...... 1.5 Barley, hay ...... 7 Barley, straw ...... 8 Sheep, meat byproducts, except liver ...... 0.08 Beet sugar ...... 0.08 Sheep, muscle ...... 0.05 Brassica, head and stem (subgroup 5A) ...... 1.5 Sorghum, grain, forage ...... 2.0 Brassica, leafy greens (subgroup 5B) ...... 7.0 Sorghum, grain, grain ...... 1.5 Brazil nut ...... 0.02 Sorghum, grain, stover ...... 6.0 Bur oak ...... 0.02 Soybean, seed ...... 0.35 Butternut ...... 0.02 Strawberry ...... 1.5 Cajou ...... 0.02 Tomato, paste ...... 1.5 Cashew ...... 0.02 Vegetable, cucurbit, group 9 ...... 0.30 Castanha-do-maranhao ...... 0.02 Cattle, fat ...... 0.2 Vegetable, fruiting, group 8–10 ...... 1.0 Cattle, liver ...... 1.5 Vegetable, leafy, except Brassica, crop group 4, Cattle, meat byproducts, except liver ...... 0.08 except head lettuce and radicchio ...... 10 Cattle, muscle ...... 0.05 Walnut, black ...... 0.02 Coconut ...... 0.02 Walnut, English ...... 0.02 Coffee, green, bean 1 ...... 0.15 Wheat, bran ...... 0.30 Coffee, instant 1 ...... 0.30 Wheat, forage ...... 30 Coquito nut ...... 0.02 Wheat, germ ...... 0.25 Corn, field, forage ...... 5.0 Wheat, grain ...... 0.15 Corn, field, grain ...... 0.01 Wheat, hay ...... 15 Corn, field, refined oil ...... 0.02 Corn, field, stover ...... 15 Wheat, straw ...... 9.0 Corn, pop ...... 0.01 1 There are no U.S. registrations as of October 22, 2013. Corn, pop, stover ...... 15 Corn, sweet, forage ...... 9 (b) Section 18 emergency exemptions. Corn, sweet, kernel plus cob with husk removed 0.03 Corn, sweet, stover ...... 8 [Reserved] Cotton, gin byproducts ...... 6.0 (c) Tolerances with regional registra- Cotton, undelinted seed ...... 0.50 tions [Reserved] Dika nut ...... 0.02

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(d) Indirect or inadvertent residues. Commodity Parts per Tolerances are established for the indi- million rect or inadvertent residues of the fun- Eggs ...... 0.02 gicide flutriafol, including its metabo- Goat, fat ...... 0.03 lites and degradates, in or on the com- Goat, liver ...... 3.0 Goat, meat ...... 0.02 modities in the table 2 to this para- Goat, meat byproducts, except liver ...... 0.70 graph (d) when present therein as a re- Grass, forage ...... 25 sult of the application of flutriafol to Grass, hay ...... 3.5 the growing crops listed in the table to Hog, fat ...... 0.02 Hog, liver ...... 0.30 paragraph (a) of this section. Compli- Hog, meat ...... 0.02 ance with the following tolerance lev- Hog, meat byproducts, except liver ...... 0.05 els specified in table 2 to this para- Horse, fat ...... 0.03 Horse, liver ...... 3.0 graph (d) is to be determined by meas- Horse, meat ...... 0.02 uring only flutriafol ((±)-a-(2- Horse, meat byproducts, except liver ...... 0.70 fluorophenyl)-a-(4-fluorophenyl)-1H- Milk ...... 0.03 Oat, forage ...... 0.10 1,2,4-triazole-1-ethanol) in or on the fol- Oat, grain ...... 0.08 lowing commodities: Oat, hay ...... 0.50 Oat, straw ...... 0.20 TABLE 2 TO PARAGRAPH (d) Poultry, fat ...... 0.02 Poultry, meat ...... 0.02 Parts per Poultry, meat byproducts ...... 0.20 Commodity million Rye, forage ...... 0.20 Rye, grain ...... 0.02 Rice, grain ...... 0.5 Rye, straw ...... 0.20 Sheep, fat ...... 0.03 Sheep, liver ...... 3.0 [75 FR 26673, May 12, 2010, as amended at 76 Sheep, meat ...... 0.02 FR 69647, Nov. 9, 2011; 77 FR 47301, Aug. 8, Sheep, meat byproducts, except liver ...... 0.70 2012; 77 FR 48901, Aug. 15, 2012; 78 FR 75262, Sorghum, grain, forage ...... 1.5 Dec. 11, 2013; 79 FR 32673, June 6, 2014; 80 FR Sorghum, grain, grain ...... 0.70 5951, Feb. 4, 2015; 80 FR 71952, Nov. 18, 2015; 85 Sorghum, grain, stover ...... 0.80 Wheat, forage ...... 0.20 FR 8467, Feb. 14, 2020] Wheat, grain ...... 0.02 Wheat, hay ...... 0.80 § 180.631 Pyrasulfotole; tolerances for Wheat, straw ...... 0.20 residues. (a) General. Tolerances are estab- (b) Section 18 emergency exemptions. lished for residues of the herbicide [Reserved] pyrasulfotole, including its metabo- (c) Tolerances with regional registra- lites and degradates, in or on the com- tions. [Reserved] modities in the table below. Compli- (d) Indirect or inadvertent residues. ance with the tolerance levels specified [Reserved] below is to be determined by measuring [72 FR 45649, Aug. 15, 2007, as amended at 76 only the sum of pyrasulfotole ((5-hy- FR 23898, Apr. 29, 2011] droxy-1,3-dimethyl-1H-pyrazol-4-yl)[2- (methylsulfonyl)-4- § 180.632 Fenazaquin; Tolerances for (trifluoromethyl)phenyl]methanone) residues. and its desmethyl metabolite (5-hy- (a) General. Tolerances are estab- droxy-3-methyl-1H-pyrazol-4-yl)[2- lished for residues of the insecticide (methylsulfonyl)-4- fenazaquin, including its metabolites (trifluoromethyl)phenyl]methanone), and degradates, in or on the commod- calculated as the stoichiometric equiv- ities in the table below. Compliance alent of pyrasulfotole, in or on the with the tolerance levels specified commodities: below is to be determined by measuring only fenazaquin, or 4-[2-[4-(1,1- Parts per Commodity million dimethylethyl)phenyl]- ethoxy]quinazoline. Aspirated grain fractions ...... 0.40 Barley, grain ...... 0.02 Parts per Barley, hay ...... 0.30 Commodity million Barley, straw ...... 0.20 Cattle, fat ...... 0.03 Almond, hulls ...... 4 Cattle, liver ...... 3.0 Avocado ...... 0.15 Cattle, meat ...... 0.02 Berry, low growing, subgroup 13–07G ...... 2 Cattle, meat byproducts, except liver ...... 0.70 Bushberry, subgroup 13–07B ...... 0.8

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Parts per Parts per Commodity million Commodity million

Caneberry, subgroup 13–07A ...... 0.7 Wheat, grain ...... 0.01 Fruit, Citrus, Group 10 except Grapefruit 2 ...... 0.5 Wheat, hay ...... 0.05 Fruit, citrus, group 10–10 ...... 0.4 Wheat, straw ...... 0.05 Fruit, citrus, group 10–10, oil ...... 20 Fruit, pome, group 11–10 ...... 0.6 (b) Section 18 emergency exemptions. Fruit, small vine climbing, except fuzzy kiwifruit, subgroup 13–07F ...... 0.7 [Reserved] Fruit, stone, group 12–12 ...... 2 (c) Tolerances with regional registra- Grape, raisin ...... 0.8 tions. [Reserved] Hop, dried cones ...... 30 Nuts, Tree, Group 14–12 ...... 0.02 (d) Indirect or inadvertent residues. Pea and bean, dried shelled, except soybean, [Reserved] subgroup 6C ...... 0.3 Pea and bean, succulent shelled, subgroup 6B ... 0.03 [72 FR 55077, Sept. 28, 2007, as amended at 83 Peppermint, fresh leaves ...... 10 FR 35147, July 25, 2018] Pineapple 1 ...... 0.2 Spearmint, fresh leaves ...... 10 § 180.634 Tembotrione; tolerances for Tea, dried 1 ...... 9 Vegetable, cucurbit, group 9 ...... 0.3 residues. Vegetable, fruiting, group 8–10 ...... 0.3 (a) General. (1) Tolerances are estab- Vegetable, legume, edible podded, subgroup 6A 0.4 lished for residues of the herbicide 1 There are no U.S. registrations as of May 25, 2017 for use tembotrione, including its metabolites on pineapple and tea. 2 This tolerance expires on October 11, 2019. and degradates, in or on the commodities listed in the table to this para- (b) Section is emergency exempotions. graph. Compliance with the tolerance [Reserved] levels specified below is to be deter- (c) Tolerances with regional registra- mined by measuring only the sum of tion. [Reserved] tembotrione, 2-[2-chloro-4- (d) Indirect or inadvertent residues. (methylsulfonyl)-3-[(2,2,2- [Reserved] trifluoroethoxy)methyl]benzoyl]-1,3- [72 FR 44393, Aug. 8, 2007, as amended at 80 cyclohexanedione and its metabolite, 2- FR 25958, May 6, 2015; 82 FR 24071, May 25, [2-chloro-4-(methylsulfonyl)-3-[(2,2,2- 2017; 84 FR 14622, Apr. 11, 2019] trifluoroethoxy) methyl]benzoyl]-4,6- dihydroxy-1,3-cyclohexanedione, cal- § 180.633 Florasulam; tolerances for residues. culated as the stoichiometric equivalent of tembotrione, in or on the fol- (a) General. Tolerances are estab- lowing commodities. lished for residues of the herbicide florasulam, including its metabolites Commodity Parts per and degradates, in or on the commod- million ities below. Compliance with the toler- Cattle, liver ...... 0.40 ance levels specified below is to be de- Cattle, meat byproducts, except liver ...... 0.07 Corn, field, forage ...... 0.60 termined by measuring only Corn, field, grain ...... 0.02 florasulam, N-(2, 6-difluorophenyl)-8- Corn, field, stover ...... 0.45 fluoro-5-methoxy (1, 2, 4) triazole (1, 5- Corn, pop, grain ...... 0.02 c)pyrimidine-2-sulfonamide, in or on Corn, pop, stover ...... 0.35 Corn, sweet, forage ...... 0.35 the commodities. Corn, sweet, stover ...... 0.60 Goat, liver ...... 0.40 Commodity Parts per Goat, meat byproducts, except liver ...... 0.07 million Horse, liver ...... 0.40 Horse, meat byproducts, except liver ...... 0.07 Barley, grain ...... 0.01 Poultry, liver ...... 0.07 Barley, hay ...... 0.05 Sheep, liver ...... 0.40 Barley, straw ...... 0.05 Sheep, meat byproducts, except liver ...... 0.07 Oat, forage ...... 0.05 Oat, grain ...... 0.01 Oat, hay ...... 0.05 (2) Tolerances are established for res- Oat, straw ...... 0.05 idues of the herbicide tembotrione, in- Rye, forage ...... 0.05 cluding its metabolites and degradates, Rye, grain ...... 0.01 Rye, straw ...... 0.05 in or on the commodities listed in the Teff, forage ...... 0.05 table to this paragraph. Compliance Teff, grain ...... 0.01 with the tolerance levels specified Teff, hay ...... 0.05 Teff, straw ...... 0.05 below is to be determined by measuring Wheat, forage ...... 0.05 only tembotrione, 2-[2-chloro-4-

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(methylsulfonyl)-3-[(2,2,2- L-mannopyranosyl)oxy]-9-ethyl-14- trifluoroethoxy)methyl]benzoyl]-1,3- methyl-7,15-dioxo-2,3,3a,4,5,5a,5b,6,7, cyclohexanedione in or on the fol- 9,10,11,12,13,14,15,16a,16b-octadecahydro- lowing commodities. 1H-as-indaceno[3,2d]oxacyclododecin- 13-yl]oxy)-2-methyltetrahydro-2H- Parts per Commodity million pyran-3-yl(methyl)formamide, calculated as the stoichiometric equiva- Corn, sweet, kernel plus cob with husks removed 0.01 lent of spinetoram.

(b) Section 18 emergency exemptions. Commodity Parts per [Reserved] million (c) Tolerances with regional registra- Acerola ...... 0.30 tions. [Reserved] Almond, hulls ...... 19 (d) Indirect or inadvertent residues. Amaranth grain, grain ...... 1.0 Apple, wet pomace ...... 0.50 [Reserved] Artichoke, globe ...... 0.30 Asparagus ...... 0.04 [72 FR 55085, Sept. 28, 2007, as amended at 74 Atemoya ...... 0.30 FR 47894, Sept. 18, 2009] Avocado ...... 0.30 Banana ...... 0.25 § 180.635 Spinetoram; tolerances for Beet, sugar, molasses ...... 0.75 residues. Berry, low growing, subgroup 13–07G, except cranberry ...... 0.90 (a) General. Tolerances are estab- Biriba ...... 0.30 lished for residues of the insecticide Brassica, head and stem, subgroup 5A ...... 2.0 Brassica, leafy greens, subgroup 5B ...... 10 spinetoram, including its metabolites Bushberry subgroup 13–07B ...... 0.50 and degradates, in or on the commod- Caneberry subgroup 13–07A ...... 0.80 ities in the table below. Compliance Canistel ...... 0.30 with the tolerance levels specified Cattle, fat ...... 5.5 Cattle, liver ...... 0.85 below is to be determined by measuring Cattle, meat ...... 0.20 only the sum of XDE–175–J: 1-H-as- Cattle, meat byproducts (except liver) ...... 0.60 indaceno[3,2-d]oxacyclododecin-7,15- Cherimoya ...... 0.30 Citrus, dried pulp ...... 0.50 dione,2-[(6deoxy-3-O-ethyl-2,4-di-O- Citrus, oil ...... 3.0 methyl-a-L-mannopyranosyl)oxy]-13- Coffee, green bean ...... 0.04 [[(2R,5S,6R)-5(dimethylamino) Corn, sweet, kernel plus cob with husks removed 0.04 tetrahydro-6-methyl-2H-pyran-2- Cotton, gin byproducts ...... 1.5 Cottonseed subgroup 20C ...... 0.04 yl]oxy]-9-ethyl-2,3,3a,4,5,5a,5b,6,9, Cranberry ...... 0.04 10,11,12,13,14,16a,16b-hexadecahydro-14- Custard apple ...... 0.30 methyl- Date ...... 0.10 Egg ...... 0.04 ,(2R,3aR,5aR,5bS,9S,13S,14R,16aS,16bR); Feijoa ...... 0.30 XDE–175–L: 1H-as-indaceno[3,2- Fig ...... 0.10 d]oxacyclododecin-7,15-dione,2- Fruit, citrus, group 10–10 ...... 0.30 [(6deoxy-3-O-ethyl-2,4-di-O-methyl- -L- Fruit, pome, group 11–10 ...... 0.20 a Fruit, small, vine climbing, subgroup 13–07F, ex- mannopyranosyl)oxy]-13-[[(2R,5S,6R)- cept fuzzy kiwifruit ...... 0.50 5(dimethylamino)tetrahydro-6-methyl- Fruit, stone 12–12 ...... 0.30 2H-pyran-2-yl]oxy]-9-ethyl- Goat, fat ...... 5.5 Goat, liver ...... 0.85 2,3,3a,5a,5b,6,9,10,11,12,13,14,16a,16b- Goat, meat ...... 0.20 tetradecahydro-4,14-dimethyl- Goat, meat byproducts (except liver) ...... 0.60 ,(2S,3aR,5aS,5bS,9S,13S,14R,16aS,16bS); Grain, aspirated fractions ...... 20 ND–J: Grain, cereal, group 15, except rice, sorghum, pearl millet and proso millet ...... 0.04 (2R,3aR,5aR,5bS,9S,13S,14R,16aS,16bR)-9- Grain, cereal, group 16, forage ...... 3.5 ethyl-14-methyl-13[[(2S,5S,6R)-6-meth- Grain, cereal, group 16, hay ...... 10 yl-5-(methylamino)tetrahydro-2H- Grain, cereal, group 16, stover ...... 10 Grain, cereal, straw, group 16, except rice ...... 1.0 pyran-2-yl]oxy]-7,15- Grape, raisin ...... 0.70 dioxo2,3,3a,4,5,5a,5b,6,7,9,10,11,12,13, Guava ...... 0.30 14,15,16a,16b-octadecahydro-1H-as- Herb, dried, subgroup 19A ...... 22 indaceno[3,2d]oxacyclododecin-2-yl-6- Herb, fresh, subgroup 19A ...... 3.0 Hog, fat ...... 0.40 deoxy-3-O-ethyl-2,4-di-O-methyl-a-L- Hog, meat ...... 0.04 mannopyranoside; and NF–J: Hog, meat byproducts ...... 0.04 (2R,3S,6S)-6- Hop, dried cones ...... 22 Horse, fat ...... 5.5 ([(2R,3aR,5aR,5bS,9S,13S,14R,16aS,16bR)- Horse, liver ...... 0.85 2-[(6-deoxy-3-O-ethyl-2,4-di-O-methyl-a- Horse, meat ...... 0.20 704

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(d) Indirect and invertent residues. [Re- Commodity Parts per million served] Horse, meat byproducts (except liver) ...... 0.60 [72 FR 57499, Oct. 10, 2007, as amended at 73 Ilama ...... 0.30 FR 14714, Mar. 19, 2008; 74 FR 40759, Aug. 13, Jaboticaba ...... 0.30 2009; 80 FR 80282, Dec. 24, 2015; 83 FR 38981, Longan ...... 0.30 Aug. 8, 2018] Lychee ...... 0.30 Mango ...... 0.30 § 180.636 1,3-dichloropropene; toler- Milk ...... 0.30 ances for residues. Milk, fat ...... 7.5 Millet, pearl, grain ...... 1.0 (a) General. Tolerances are estab- Millet, proso, grain ...... 1.0 lished for the combined residues of the Nut, tree, group 14–12 ...... 0.10 fungicide cis- and trans-1,3- Onion, bulb, subgroup 3–07A ...... 0.10 dichloropropene and its metabolites Onion, green, subgroup 3–07B ...... 2.0 Papaya ...... 0.30 cis- and trans-3-chloroacrylic acid, and Passionfruit ...... 0.30 cis- and trans-3-chloroallyl alcohol in or Pea and bean, dried shelled, except soybean, on the following commodities. subgroup 6C ...... 0.04 Pea and bean, succulent shelled, subgroup 6B ... 0.04 Commodity Parts per Peanut ...... 0.04 million Peanut, hay ...... 11 Grape ...... 0.018 Peppermint, tops ...... 3.5 Pineapple ...... 0.04 Pineapple, processed residue ...... 0.15 (b) Section 18 emergency exemptions. Pomegranate ...... 0.30 [Reserved] Poultry, fat ...... 0.10 (c) Tolerances with regional registra- Poultry, meat ...... 0.04 tions. [Reserved] Poultry, meat byproducts ...... 0.04 (d) Indirect or inadvertent residues. Pulasan ...... 0.30 [Reserved] Quinoa, grain ...... 0.04 Rambutan ...... 0.30 [73 FR 8218, Feb. 13, 2008] Sapodilla ...... 0.30 Sapote, black ...... 0.30 § 180.637 Mandipropamid; tolerances Sapote, mamey ...... 0.30 for residues. Sapote, white ...... 0.30 Sheep, fat ...... 5.5 (a) General. Tolerances are estab- Sheep, liver ...... 0.85 lished for residues of mandipropamid, Sheep, meat ...... 0.20 including its metabolites and Sheep, meat products (except liver) ...... 0.60 degradates, in or on the commodities Sorghum, grain, grain ...... 1.0 listed in the table below. Compliance Soursop ...... 0.30 Soybean, seed ...... 0.04 with the tolerance levels specified Spanish lime ...... 0.30 below is to be determined by measuring Spearmint, tops ...... 3.5 only mandipropamid (4-chloro-N-[2-[3- Spice, subgroup 19B, except black pepper ...... 1.7 methoxy-4-(2-propynyloxy) Star apple ...... 0.30 phenyl]ethyl]-a-(2-propynyloxy) Star fruit ...... 0.30 Sugar apple ...... 0.30 benzeneacetamide) in or on the com- Tea, dried 1 ...... 70 modity. Tea, instant 1 ...... 70 Ti, leaves ...... 10 Parts per Commodity million Vegetable, cucurbit, group 9 ...... 0.30 Vegetable, foliage of legume, group 7 ...... 8.0 Asparagus bean, edible podded ...... 0.90 Vegetable, fruiting, group 8–10 ...... 0.40 Basil, dried leaves ...... 200 Vegetable, leafy, except Brassica, group 4 ...... 8.0 Basil, fresh leaves ...... 30 Vegetable, leaves of root and tuber, group 2 ...... 10 Bean (Phaseolus spp.), edible podded ...... 0.90 Vegetable, legume, edible podded, subgroup 6A 0.30 Bean (Vigna spp.), edible podded ...... 0.90 1 Vegetable, root and tuber, group 1 ...... 0.10 Cacao, dried bean ...... 0.06 Watercress ...... 8.0 Catjang bean, edible podded ...... 0.90 Celtuce ...... 20 Wax jambu ...... 0.30 Chinese longbean, edible podded ...... 0.90 1 There are no U.S. registrations as of August 8, 2018 for Citrus, dried pulp ...... 0.70 use on tea. Citrus, oil ...... 15 Cowpea, edible podded ...... 0.90 (b) Section 18 emergency exemptions. Fennel, Florence, fresh leaves and stalk ...... 20 [Reserved] French bean, edible podded ...... 0.90 Fruit, citrus, group 10–10 ...... 0.50 (c) Tolerances with regional registra- Fruit, small vine climbing, except fuzzy kiwifruit, tion. [Reserved] subgroup 13–07F ...... 1.4

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Parts per Parts per Commodity million Commodity million

Garden bean, edible podded ...... 0.90 Velvet bean, edible podded ...... 0.90 Ginseng ...... 0.30 Wax bean, edible podded ...... 0.90 Goa bean, edible podded ...... 0.90 Winged pea, edible podded ...... 0.90 Grape, raisin ...... 3.0 Yardlong bean, edible podded ...... 0.90 Green bean, edible podded ...... 0.90 Guar bean, edible podded ...... 0.90 1 There are no U.S. registrations allowing use of Hop, dried cones ...... 50 mandipropamid on cacao as of October 28, 2019. Jackbean, edible podded ...... 0.90 (b) Section 18 emergency exemptions. Kidney bean, edible podded ...... 0.90 Kohlrabi ...... 3.0 Time-limited tolerances are estab- Lablab bean, edible podded ...... 0.90 lished for residues of mandipropamid, Leaf petiole vegetable subgroup 22B ...... 20 including its metabolites and Moth bean, edible podded ...... 0.90 degradates, in or on the commodities Mung bean, edible podded ...... 0.90 Navy bean, edible podded ...... 0.90 listed in the table below resulting from Onion, bulb, subgroup 3–07A ...... 0.05 use of the pesticide pursuant to Onion, green, subgroup 3–07B ...... 4.0 FFIFRA section 18 emergency exemp- Potato, wet peel ...... 0.15 Rice bean, edible podded ...... 0.90 tions. Compliance with the tolerance Scarlet runner bean, edible podded ...... 0.90 levels specified below is to be deter- Snap bean, edible podded ...... 0.90 mined by measuring only Sword bean, edible podded ...... 0.90 mandipropamid (4-chloro-N-[2-[3- Urd bean, edible podded ...... 0.90 Vegetable, Brassica, head and stem, group 5–16 3.0 methoxy-4-(2-propynyloxy) Vegetable, cucurbit, group 9 ...... 0.6 phenyl]ethyl]-a-(2-propynyloxy) Vegetable, fruiting, group 8–10 ...... 1.0 benzeneacetamide) in or on the com- Vegetable, leafy, group 4–16 ...... 25 Vegetable soybean, edible podded ...... 0.90 modity. The tolerances expire on the Vegetable, tuberous and corm, subgroup 1C ...... 0.09 date specified in the table.

Parts per Expiration/revocation Commodity million date

Basil, dried ...... 240 12/31/15

(c) Tolerances with regional registra- Commodity Parts per tions. [Reserved] million (d) Indirect or inadvertent tolerances. Teff, grain ...... 0.01 [Reserved] Teff, hay ...... 0.01 Teff, straw ...... 0.03 [73 FR 2816, Jan. 16, 2008, as amended at 74 Wheat, forage ...... 0.06 FR 33169, July 10, 2009; 76 FR 55804, Sept. 9, Wheat, grain ...... 0.01 2011; 77 FR 74119, Dec. 13, 2012; 78 FR 76992, Wheat, hay ...... 0.01 Dec. 20, 2013; 81 FR 17088, Mar. 28, 2016; 84 FR Wheat, straw ...... 0.03 10700, Mar. 22, 2019; 84 FR 57621, Oct. 28, 2019] (b) Section 18 emergency exemptions. § 180.638 Pyroxsulam; tolerances for [Reserved] residues. (c) Tolerances with regional registrations. [Reserved] (a) General. Tolerances are estab- (d) lished for residues of pyroxsulam, in- Indirect or inadvertent residues. [Reserved] cluding its metabolites and degradates, in or on the commodities listed in the [73 FR 10402, Feb. 27, 2008, as amended at 82 table below. Compliance with the toler- FR 30990, July 5, 2017; 83 FR 31895, July 10, ance levels specified below is to be de- 2018] termined by measuring only pyroxsulam, N-(5,7-dimethoxy[l, 2,4] § 180.639 Flubendiamide; tolerances for residues. triazolo[l, 5-a]pyrimidin-2-yl)-2- methoxy-4-(trifluoromethyl)-3- (a) General. (1) Tolerances are estab- pyridinesulfonamide, in or on the com- lished for residues of flubendiamide, in- modity. cluding its metabolites and degradates, in or on the commodities in the table Commodity Parts per below. Compliance with the tolerance million levels specified in the table is to be de- Teff, forage ...... 0.06 termined by measuring only

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flubendiamide N2-[1, 1-dimethyl-2- Commodity Parts per (methylsulfonyl)ethyl]-3-iodo-N1-[2- million methyl-4- [1,2,2,2-tetrafluoro-1- Horse, fat ...... 0.70 (trifluoromethyl)ethyl]phenyl]-1,2- Horse, meat ...... 0.08 benzenedicarboxamide, in or on the fol- Horse, meat byproducts ...... 0.60 Milk ...... 0.15 lowing commodities: Milk, fat ...... 1.0 Pea and bean, dried shelled, except soybean, Commodity Parts per subgroup 6C ...... 0.60 million Pea and bean, succulent shelled, subgroup 6B ... 0.05 Peanut, hay ...... 60 Almond, hulls ...... 9.0 Peanut, meal ...... 0.03 Apple, wet pomace ...... 5.0 Peanut, nutmeat ...... 0.02 Corn, field, forage ...... 8.0 Corn, field, grain ...... 0.03 Peanut, refined oil ...... 0.03 Corn, field, stover ...... 15 Pistachio ...... 0.06 Corn, pop, grain ...... 0.02 Poultry, fat ...... 3.0 Corn, pop, stover ...... 15 Poultry, liver ...... 0.60 Corn, sweet, forage ...... 9.0 Poultry, meat ...... 0.10 1 Corn, sweet, kernel plus cob with husks removed 0.01 Rice, grain ...... 0.50 Corn, sweet, stover ...... 25 Safflower, seed ...... 5.0 Cotton gin byproducts ...... 60 Sheep, fat ...... 0.70 Cotton, undelinted seed ...... 0.90 Sheep, meat ...... 0.08 Fruit, pome, group 11 ...... 1.5 Sheep, meat byproducts ...... 0.60 Fruit, stone, group 12 ...... 1.6 Sorghum, grain, forage ...... 12 Grape ...... 1.4 Sorghum, grain, grain ...... 5.0 Nut, tree, group 14 ...... 0.06 Sorghum, grain, stover ...... 14 Okra ...... 0.30 Soybean, forage ...... 18 Tea 1 ...... 50 Soybean, hay ...... 60 Vegetable, cucurbit, group 9 ...... 0.20 Soybean, hulls ...... 0.80 Vegetable, fruiting, group 8 ...... 0.60 Soybean, seed ...... 0.25 Vegetable, leafy, except Brassica, group 4 ...... 11 Sugarcane, cane ...... 0.30 Sunflower, seed ...... 5.0 1 There are no U.S. registrations as of July 5, 2017, for use Turnip, greens ...... 25 of flubendiamide on tea. Vegetable, foliage of legume, except soybean, subgroup 7A ...... 35 (2) Tolerances are established for res- Vegetable, legume, edible podded, subgroup 6A 0.50 idues of flubendiamide, including its metabolites and degradates, in or on 1 There are no U.S. registrations for rice, grain. the commodities in the table below. (b) Section 18 emergency exemptions. Compliance with the tolerance levels [Reserved] specified in the table is to be deter- (c) Tolerances with regional registra- mined by measuring only tions. [Reserved] flubendiamide N2-[1,1-dimethyl-2- (d) Indirect or inadvertent residues. (methylsulfonyl)ethyl]-3-iodo-N1-[2- Tolerances are established for residues methyl-4-[1,2,2,2-tetrafluoro-1- of flubendiamide, including its metabo- (trifluoromethyl)ethyl]phenyl]-1,2- lites and degradates, in or on the com- benzenedicarboxamide, in or on the fol- modities in the table below. Compli- lowing commodities: ance with the tolerance levels specified in the table is to be determined by Parts per Commodity million measuring only flubendiamide N2-[1, 1- dimethyl-2-(methylsulfonyl)ethyl]-3- Alfalfa, forage ...... 25 iodo-N1-[2-methyl-4- [1,2,2,2- Alfalfa, hay ...... 65 Artichoke, globe ...... 1.6 tetrafluoro-1-(trifluoromethyl)ethyl] Berry, low growing, subgroup 13–07G, except phenyl]-1, 2-benzenedicarboxamide, in cranberry ...... 1.5 or on the following commodities: Brassica, head and stem, subgroup 5A ...... 3.0 Brassica, leafy greens, subgroup 5B ...... 25 Parts per Cattle, fat ...... 0.70 Commodity million Cattle, meat ...... 0.08 Cattle, meat byproducts ...... 0.60 Barley, hay ...... 0.04 Egg ...... 0.40 Barley, straw ...... 0.07 Fruit, small fruit vine climbing except fuzzy Buckwheat ...... 0.07 kiwifruit, subgroup 13–07F ...... 1.4 Clover, forage ...... 0.15 Goat, fat ...... 0.70 Clover, hay ...... 0.04 Goat, meat ...... 0.08 Grass, forage ...... 0.15 Goat, meat byproducts ...... 0.60 Grass, hay ...... 0.04 Grain, aspirated grain fractions ...... 153 Millet, pearl, forage ...... 0.15 Hog, fat ...... 0.15 Millet, pearl, hay ...... 0.04 Hog, meat ...... 0.03 Millet, proso, forage ...... 0.15 Hog, meat byproducts ...... 0.15 Millet, proso, hay ...... 0.04

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1-azaspiro[4.5]decane-2,4-dione, cis-3- Commodity Parts per million (2,5-dimethylphenyl)-8-methoxy-2-oxo- Millet, proso, straw ...... 0.07 1-azaspiro[4.5]dec-3-en-4-yl beta-D-glu- Oats, forage ...... 0.15 copyranoside, and cis-3-(2,5- Oats, hay ...... 0.04 dimethylphenyl)-4-hydroxy-8-methoxy- Oats, straw ...... 0.07 Rye, forage ...... 0.15 1-azaspiro[4.5]decan-2-one, calculated Rye, straw ...... 0.07 as the stoichiometric equivalent of Teosinte, forage ...... 0.15 spirotetramat, in or on the following Teosinte, hay ...... 0.04 Teosinte, straw ...... 0.07 commodities. Triticale, forage ...... 0.15 Triticale, hay ...... 0.04 Parts per Commodity million Triticale, straw ...... 0.07 Wheat, forage ...... 0.15 Acerola ...... 2.5 Wheat, hay ...... 0.03 Almond, hulls ...... 9.0 Wheat, straw ...... 0.03 Artichoke, globe ...... 1.5 Asparagus 1 ...... 0.10 [76 FR 16307, Mar. 23, 2011, as amended at 76 Aspirated grain fractions ...... 10.0 Avocado ...... 0.60 FR 55273, Sept. 7, 2011; 77 FR 73945, Dec. 12, Beet, sugar, molasses ...... 0.30 2012; 82 FR 30982, July 5, 2017] Beet, sugar, roots ...... 0.15 Berry, low growing, except strawberry, subgroup § 180.640 Pyridalyl; tolerances for resi- 13–07H ...... 0.30 dues. Black sapote ...... 0.60 Brassica, head and stem, subgroup 5A ...... 2.5 (a) General. Tolerances are estab- Brassica, leafy, subgroup 5B ...... 8.0 lished for residues of pyridalyl, pyri- Bushberry subgroup 13–07B ...... 3.0 Canistel ...... 0.60 dine,2-[3-[2,6-dichloro-4-[(3,3-dichloro-2- Carrot, roots ...... 0.15 propenyl)oxy]phenoxy]propoxy]-5- Citrus, oil ...... 6.0 (trifluoromethyl, in or on the following Coffee, green bean ...... 0.20 raw agricultural commodities:) Coffee, instant ...... 0.50 Corn, sweet, kernel plus cob with husks removed 1.5 Cotton gin byproducts1 ...... 10.0 Parts per 1 Commodity million Cotton, undelinted seed ...... 0.30 Feijoa ...... 2.5 Brassica, head and stem, subgroup 5A ...... 3.5 Fruit, citrus, group 10–10 ...... 0.60 Mustard greens ...... 30 Fruit, pome, group 11–10 ...... 0.70 Turnip greens ...... 30 Fruit, stone, group 12–12 ...... 4.5 Vegetable, fruiting, group 8 ...... 1.0 Grape, raisin ...... 3.0 Vegetables, leafy, except Brassica, group 4 ...... 20 Guava ...... 2.5 Hop, dried cones ...... 10.0 Jaboticaba ...... 2.5 (b) Section 18 emergency exemptions. Longan ...... 13.0 [Reserved] Lychee ...... 13.0 (c) Tolerances with regional registra- Mamey sapote ...... 0.60 Mango ...... 0.60 tions. [Reserved] Nut, tree, group 14–12 ...... 0.25 (d) Indirect or inadvertent residues. Papaya ...... 0.40 [Reserved] Passionfruit ...... 2.5 Persimmon ...... 2.5 [73 FR 25533, May 7, 2008] Pineapple ...... 0.30 Pistachio ...... 0.25 § 180.641 Spirotetramat; tolerances for Pomegranate ...... 0.50 Potato, flakes ...... 1.6 residues. Pulasan ...... 13.0 (a) General. (1) Tolerances are estab- Rambutan ...... 13.0 lished for residues of the insecticide Sapodilla ...... 0.60 Small fruit vine climbing subgroup, except fuzzy spirotetramat, including its metabo- kiwifruit, subgroup 13–07F ...... 1.3 lites and degradates, in or on the com- Soybean forage ...... 8.0 modities in the table below. Compli- Soybean hay ...... 16.0 Soybean seed ...... 5.0 ance with the tolerance levels specified Spanish lime ...... 13 below is to be determined by measuring Star apple ...... 0.60 only the sum of spirotetramat (cis-3- Starfruit ...... 2.5 (2,5-dimethlyphenyl)-8-methoxy-2-oxo- Strawberry1 ...... 0.40 Taro, leaves ...... 9.0 1-azaspiro[4.5]dec-3-en-4-yl-ethyl car- Vegetable, bulb, group 3–07 ...... 0.80 bonate) and its metabolites cis-3-(2,5- Vegetable, cucurbit, group 9 ...... 0.30 dimethylphenyl)-4-hydroxy-8-methoxy- Vegetable, foliage of legume, except soybean, subgroup 07A ...... 7.0 1-azaspiro[4.5]dec-3-en-2-one, cis-3-(2,5- Vegetable, fruiting, group 8–10 ...... 2.5 dimethylphenyl)-3-hydroxy-8-methoxy- Vegetable, leafy, except brassica, group 4 ...... 9.0

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(2,5-dimethylphenyl)-8-methoxy-2-oxo- Commodity Parts per million 1-azaspiro[4.5]dec-3-en-4-yl beta-D-glu- Vegetable, legume, group 06, except soybean .... 2.5 copyranoside, and cis-3-(2,5- Vegetable, tuberous and corm, subgroup 1C ...... 0.60 dimethylphenyl)-4-hydroxy-8-methoxy- Watercress ...... 2.0 1-azaspiro[4.5]decan-2-one, calculated Wax jambu ...... 2.5 White sapote ...... 0.60 as the stoichiometric equivalent of spirotetramat, in or on the following 1 There are no U.S. registrations for these commodities. commodities. (2) Tolerances are also established for Parts per residues of the insecticide Commodity million spirotetramat, including its metabolites and degradates, in or on the com- Banana ...... 4.0 modities in the table below. Compli- ance with the tolerance levels specified (d) Indirect or inadvertant residues. below is to be determined by measuring [Reserved] only the sum of spirotetramat (cis-3- [73 FR 39256, July 9, 2008, as amended at 76 (2,5-dimethlyphenyl)-8-methoxy-2-oxo- FR 28681, May 18, 2011; 77 FR 8746, Feb. 15, 1-azaspiro[4.5]dec-3-en-4-yl-ethyl car- 2012; 77 FR 75859, Dec. 26, 2012; 78 FR 28512, bonate]) and its metabolite cis-3-(2,5- May 15, 2013; 78 FR 66651, Nov. 6, 2013; 81 FR dimethylphenyl)-4-hydroxy-8-methoxy- 73347, Oct. 25, 2016; 82 FR 27149, June 14, 2017] 1-azaspiro[4.5]dec-3-en-2-one, calculated § 180.643 Uniconazole; tolerances for as the stoichiometric equivalent of residues. spirotetramat, in or on the following (a) General. Tolerances are estab- commodities: lished for residues of the fungicide/ plant growth regulator uniconazole-P, Commodity Parts per million (E)-(S)-1-(4-chlorophenyl)-4,4-dimethyl- Cattle, fat ...... 0.02 2-(1H-1,2,4-triazol-1-yl)pent-1-en-3-ol, Cattle, meat ...... 0.02 its R-enantiomer and its Z-isomer in or Cattle, meat byproducts ...... 0.20 on the following raw agricultural com- Eggs ...... 0.02 Goat, fat ...... 0.02 modities: Goat, meat ...... 0.02 Goat, meat byproducts ...... 0.20 Parts per Commodity million Hog, meat byproducts ...... 0.02 Horse, fat ...... 0.02 Vegetable, fruiting, group 8 ...... 0.01 Horse, meat ...... 0.02 Horse, meat byproducts ...... 0.20 Milk ...... 0.01 (b) Section 18 emergency exemptions. Poultry, meat byproducts ...... 0.02 [Reserved] Sheep, fat ...... 0.02 (c) Tolerances with regional registra- Sheep, meat ...... 0.02 Sheep, meat byproducts ...... 0.20 tions. [Reserved] (d) Indirect or inadvertant residues. (b) Section 18 emergency exemptions. [Reserved] [Reserved] [73 FR 51736, Sept. 5, 2008] (c) Tolerances with regional registrations. Tolerances with regional reg- § 180.644 Cyprosulfamide; tolerances istrations are established for residues for residues. of the insecticide spirotetramat, in- (a) General. (1) Tolerances are estab- cluding its metabolites and degradates, lished for residues of the herbicide in or on the commodities in the table safener cyprosulfamide, N-[[4- below. Compliance with the tolerance [(cyclopropylamino)carbonyl] levels specified below is to be deter- phenyl]sulfonyl]-2-methoxybenzamide, mined by measuring only the sum of in or on the following raw agricultural spirotetramat (cis-3-(2,5- commodities: dimethlyphenyl)-8-methoxy-2-oxo-1- azaspiro[4.5]dec-3-en-4-yl-ethyl car- Commodity Parts per bonate) and its metabolites cis-3-(2,5- million dimethylphenyl)-4-hydroxy-8-methoxy- Corn, field, forage ...... 0.20 1-azaspiro[4.5]dec-3-en-2-one, cis-3-(2,5- Corn, field, grain ...... 0.01 Corn, field, stover ...... 0.20 dimethylphenyl)-3-hydroxy-8-methoxy- Corn, pop, grain ...... 0.01 1-azaspiro[4.5]decane-2,4-dione, cis-3- Corn, pop, stover ...... 0.20

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(2) Tolerances are established for res- Commodity Parts per million idues of thiencarbazone-methyl, in- Corn, sweet, forage ...... 0.40 cluding its metabolites and degradates, Corn, sweet, kernel plus cob with husks removed 0.01 in or on the commodities in the table Corn, sweet, stover ...... 0.35 below. Compliance with the tolerance levels specified below is to be deter- (2) Tolerances are established for res- mined by measuring only the sum of idues of the herbicide safener thiencarbazone-methyl [methyl 4- cyprosulfamide, N-[[4-[(cyclopropyl [[[(4,5-dihydro-3-methoxy-4-methyl-5- amino)carbonyl] phenyl]sulfonyl]-2- oxo-1H-1,2,4-triazol-1-yl)-car- methoxybenzamide, and its metabolite bonyl]amino]sulfonyl]-5-methyl-3- 4-(aminosulfonyl)-N- thiophenecarboxylate] and its metabo- cyclopropylbenzamide, calculated as lite BYH 18636–MMT [5-methoxy-4- cyprosulfamide, in or on the following methyl-2,4-dihydro-3H-1,2,4-triazol-3- raw agricultural commodities: one], calculated as the stoichiometric equivalent of thiencarbazone-methyl, Parts per Commodity million in or on the following food commodities of animal origin: Cattle, meat byproducts ...... 0.02 Goat, meat byproducts ...... 0.02 Parts per Horse, meat byproducts ...... 0.02 Commodity million Sheep, meat byproducts ...... 0.02 Cattle, meat ...... 0.02 Cattle, meat byproducts ...... 0.02 (b) Section 18 emergency exemptions. Goat, meat ...... 0.02 [Reserved] Goat, meat byproducts ...... 0.02 (c) Tolerances with regional registra- Horse, meat ...... 0.02 Horse, meat byproducts ...... 0.02 tions. [Reserved] Milk ...... 0.02 (d) Indirect or inadvertant residues. Sheep, meat ...... 0.02 [Reserved] Sheep, meat byproducts ...... 0.02 [73 FR 60974, Oct. 15, 2008] (b) Section 18 emergency exemptions. [Reserved] § 180.645 Thiencarbazone-methyl; tol- (c) Tolerances with regional registra- erances for residues. tions. [Reserved] (a)(1) General. Tolerances are estab- (d) Indirect or inadvertent residues. lished for residues of the Tolerances are established for residues thiencarbazone-methyl, including its of thiencarbazone-methyl, including its metabolites and degradates, in or on metabolites and degradates, in or on the commodities in the table below. the commodities in the table below. Compliance with the tolerance levels Compliance with the tolerance levels specified below is to be determined by specified below is to be determined by measuring only only thiencarbazone- measuring only the sum of methyl [methyl 4-[[[(4,5-dihydro-3- thiencarbazone-methyl [methyl 4- methoxy-4-methyl-5-oxo-1H-1,2,4- [[[(4,5-dihydro-3-methoxy-4-methyl-5- triazol-1-yl)-carbonyl]amino]sulfonyl]- oxo-1H-1,2,4-triazol-1-yl)-car- 5-methyl-3-thiophenecarboxylate] in or bonyl]amino]sulfonyl]-5-methyl-3- on the following food and feed com- thiophenecarboxylate] and its metabo- modities. lite BYH 18636–MMT-glucoside [2- hexopyranosyl-5-methoxy-4-methyl-2,4- Parts per Commodity million dihydro-3H-1,2,4-triazol-3-one], calculated as the stoichiometric equiva- Corn, field, forage ...... 0.04 Corn, field, grain ...... 0.01 lent of thiencarbazone-methyl, in or on Corn, field, stover ...... 0.02 the following food commodities: Corn, pop, grain ...... 0.01 Corn, pop, stover ...... 0.01 Commodity Parts per Corn, sweet, forage ...... 0.05 million Corn, sweet, kernel plus cob with husks removed 0.01 Corn, sweet, stover ...... 0.05 Soybean, forage ...... 0.04 Wheat, forage ...... 0.15 Soybean, hay ...... 0.15 Wheat, grain ...... 0.01 Wheat, hay ...... 0.01 [73 FR 60968, Oct. 15, 2008, as amended at 83 Wheat, straw ...... 0.01 FR 29033, June 25, 2018]

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§ 180.646 Ipconazole; tolerances for Commodity Parts Per residues. Million (a) General. Tolerances are estab- Grape ...... 0.20 lished for residues of ipconazole, including its metabolites and degradates, (b) Section 18 emergency exemptions. in or on the commodities listed in the [Reserved] table below. Compliance with the toler- (c) Tolerances with regional registra- ance levels specified below is to be de- tions. [Reserved] termined by measuring only ipconazole (d) Indirect or inadvertent residues. (2-[(4-chlorophenyl)methyl]-5-(1- [Reserved] methylethyl)-1-(1H-1,2,4-triazol-1- [74 FR 48396, Sept. 23, 2009] ylmethyl)cyclopentanol) in or on the commodity. § 180.649 Saflufenacil; tolerances for residues. Parts per Commodity million (a) General. (1) Tolerances are established for residues of saflufenacil, in- Cotton, gin byproducts ...... 0.01 cluding its metabolites and degradates, Cotton, undelinted seed ...... 0.01 Grain, cereal, forage, fodder and straw, group 16, in or on the commodities in the table except rice ...... 0.01 below. Compliance with the tolerance Grain, cereal group 15, except rice ...... 0.01 levels specified below is to be deter- Peanut ...... 0.01 mined by measuring only the sum of Soybean, forage ...... 0.01 Vegetable, legume, group 6 ...... 0.01 saflufenacil, 2-chloro-5-[3,6-dihydro-3- methyl-2,6-dioxo-4-(trifluoromethyl)- (b) Section 18 emergency exemptions. 1(2H)-pyrimidinyl]-4-fluoro-N-[[meth- [Reserved] yl(1-methylethyl)amino] (c) Tolerances with regional registra- sulfonyl]benzamide, and its metabo- tions. [Reserved] lites N-[2-chloro-5-(2,6-dioxo-4- (d) Indirect or inadvertent residues. (trifluoromethyl)-3,6-dihydro-1(2H)- [Reserved] pyrimidinyl)-4-fluorobenzoyl]-N′- isopropylsulfamide and N-[4-chloro-2- [73 FR 69559, Nov. 19, 2008, as amended at 79 fluoro-5-({[(isopropylamino) FR 15240, Mar. 19, 2014] sulfonyl]amino}carbonyl)phenyl]urea, calculated as the stoichiometric equiv- § 180.647 d-Phenothrin; tolerances for residues. alent of saflufenacil, in or on the commodities. (a) General. A tolerance of 0.01 parts per million is established for residues Commodity Parts per of the insecticide d-phenothrin in or on million all food/feed crops following wide-area Alfalfa, forage ...... 0.08 mosquito adulticide applications. Alfalfa, hay ...... 0.10 (b) Section 18 emergency exemptions. Almond, hulls ...... 0.10 Banana 1 ...... 0.03 [Reserved] Barley, bran ...... 1.5 (c) Tolerances with regional registra- Barley, grain ...... 1.0 tions. [Reserved] Barley, straw ...... 15 Coffee, green bean 1 ...... 0.03 (d) Indirect or inadvertent residues. Cotton, gin byproducts ...... 0.45 [Reserved] Cottonseed subgroup 20C ...... 0.20 Fruit, citrus, group 10 ...... 0.03 [74 FR 32443, July 8, 2009] Fruit, pome, group 11 ...... 0.03 Fruit, stone, group 12 ...... 0.03 § 180.648 Meptyldinocap; tolerances Grain, aspirated grain fractions ...... 50 for residues. Grain, cereal, forage, fodder and straw group 16 (except barley and wheat straw) ...... 0.10 (a) General. Tolerances are estab- Grain, cereal, group 15 (except barley and wheat lished for the combined residues of the grain) ...... 0.03 Grape ...... 0.03 fungicide meptyldinocap, 2-(1- Grass, forage ...... 15 methylheptyl)-4,6-dinitrophenyl (2E)-2- Grass, hay ...... 20 butenoate and 2,4-DNOP, 2,4-dinitro-6- Grass, seed screenings ...... 0.15 (1-methylheptyl)phenol expressed as Grass, straw ...... 0.15 Mango 1 ...... 0.03 meptyldinocap in or on the following Nut, tree, group 14 ...... 0.03 commodities: Olive ...... 0.03

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(d) Indirect or inadvertent residues. Commodity Parts per million [Reserved] Pea and bean, dried shelled, except soybean, [74 FR 46689, Sept. 11, 2009, as amended at 76 subgroup 6C ...... 0.30 FR 27261, May 11, 2011; 76 FR 76309, Dec. 7, Pea and bean, succulent shelled, subgroup 6B ... 0.03 2011; 79 FR 9866, Feb. 21, 2014; 79 FR 52219, Pea, hay ...... 17 Sept. 3, 2014; 80 FR 22420, Apr. 22, 2015; 80 FR Pistachio ...... 0.03 Pomegranate ...... 0.03 73667, Nov. 25, 2015] Rapeseed subgroup 20A ...... 0.45 Soybean, hulls ...... 0.50 § 180.650 Isoxaben; tolerances for resi- Soybean, seed ...... 0.10 dues. Sugarcane, cane 2 ...... 0.05 (a) General. Tolerances are estab- Sugarcane, molasses 2 ...... 0.08 Sunflower subgroup 20B ...... 1.0 lished for residues of the herbicide Vegetable, foliage of legume, group 7 (except isoxaben, including its metabolites and pea, hay) ...... 0.10 degradates, in or on the commodities Vegetable, legume, edible podded, subgroup 6A 0.03 in the table below. Compliance with Wheat, grain ...... 0.60 the tolerance levels specified below is Wheat, straw ...... 6.0 to be determined by measuring only 1 No U.S. registration as of December 7, 2011. isoxaben, N-[3-(1-ethyl-1- 2 No U.S. registration as of February 21, 2014. methylpropyl)-5-isoxazolyl]-2, 6- (2) Tolerances are established for res- dimethoxybenzamide, in or on the com- idues of saflufenacil, including its me- modity. tabolites and degradates, in or on the Parts per commodities in the table below. Com- Commodity million pliance with the tolerance levels specified below is to be determined by meas- Almond, hulls ...... 0.40 Apple ...... 0.01 uring only saflufenacil, 2-chloro-5-[3,6- Bushberry subgroup 13–07B ...... 0.01 dihydro-3-methyl-2,6-dioxo-4- Caneberry subgroup 13–07A ...... 0.01 (trifluoromethyl)-1(2H)-pyrimidinyl]-4- Fruit, small, vine climbing, except fuzzy kiwifruit, fluoro-N-[[methyl(1- subgroup 13–07F ...... 0.01 Hop, dried cones ...... 0.01 methylethyl)amino] Nut, tree, group 14–12 ...... 0.02 sulfonyl]benzamide, in or on the commodities. (b) Section 18 emergency exemptions. [Reserved] Parts per Commodity million (c) Tolerances with regional registrations. [Reserved] Cattle, fat ...... 0.04 (d) Indirect or inadvertent residues. Cattle, liver ...... 50 [Reserved] Cattle, meat ...... 0.02 Cattle, meat byproducts, except liver ...... 0.30 [75 FR 69360, Nov. 12, 2010, as amended at 83 Fish-freshwater finfish ...... 0.01 FR 5312, Feb. 7, 2018; 85 FR 29344, May 15, Fish-shellfish, crustacean ...... 0.01 2020] Goat, fat ...... 0.04 Goat, liver ...... 50 § 180.651 Imazosulfuron; tolerances for Goat, meat ...... 0.02 Goat, meat byproducts, except liver ...... 0.30 residues. Hog, fat ...... 0.01 (a) General. Tolerances are estab- Hog, liver ...... 2.0 lished for residues of the herbicide Hog, meat ...... 0.01 Hog, meat byproducts, except liver ...... 0.02 imazosulfuron, including its metabo- Horse, fat ...... 0.04 lites and degradates, in or on the fol- Horse, liver ...... 50 lowing commodities. Compliance with Horse, meat ...... 0.02 the tolerance levels specified in the fol- Horse, meat byproducts, except liver ...... 0.30 lowing table below is to be determined Milk ...... 0.01 Sheep, fat ...... 0.04 by measuring only imazosulfuron, 2- Sheep, liver ...... 50 chloro-N-[[(4,6-dimethoxy-2- Sheep, meat ...... 0.02 pyrimidinyl)amino]carbonyl]imidazo- Sheep, meat byproducts, except liver ...... 0.30 [1,2-a]pyridine-3-sulfonamide, in or on the commodity. (b) Section 18 emergency exemptions. [Reserved] Commodity Parts per (c) Tolerances with regional registra- million tions. [Reserved] Melon subgroup 9A ...... 0.02

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6-[(1R)-1-fluoroethyl]-1,3,5-triazine-2,4- Commodity Parts per million diamine, calculated as the stoichio- Pepper, bell ...... 0.02 metric equivalent of indaziflam, in or Pepper, non-bell ...... 0.02 on the commodity. Rice, grain ...... 0.02 Tomato ...... 0.02 Vegetable, tuberous and corm, subgroup 1C ...... 0.02 TABLE 1 TO PARAGRAPH (a)(1)

Parts per (b) Section 18 emergency exemptions. Commodity million [Reserved] (c) Tolerances with regional registra- Almond, hulls ...... 0.15 tions. [Reserved] Bushberry subgroup 13–07B ...... 0.01 (d) Indirect or inadvertent residues. Caneberry subgroup 13–07A ...... 0.01 Coffee, green bean ...... 0.01 [Reserved] Fruit, citrus, group 10–10 ...... 0.01 [75 FR 81884, Dec. 29, 2010, as amended at 78 Fruit, pome, group 11–10 ...... 0.01 FR 44444, July 24, 2013] Fruit, small, vine climbing, except fuzzy kiwifruit, subgroup 13–07F ...... 0.01 § 180.652 Ethiprole; tolerances for resi- Fruit, stone, group 12–12 ...... 0.01 Fruit, tropical and subtropical, edible peel, group dues. 23 ...... 0.01 (a) General. Tolerances are estab- Fruit, tropical and subtropical, inedible peel, lished for residues of ethiprole, includ- group 24 ...... 0.01 ing its metabolites and degradates, in Grass, forage, fodder and hay, group 17, forage 30 Grass, forage, fodder and hay, group 17, hay .... 10 or on the commodities in the table Hop, dried cones ...... 0.06 below. Compliance with the tolerance Nut, tree, group 14–12 ...... 0.01 levels specified below is to be deter- Palm, oil 1 ...... 0.03 mined by measuring only ethiprole, 5- Sugarcane, cane ...... 0.01 amino-1-[2,6-dichloro-4- 1 No U.S. Registrations as of 12/02/2013. (trifluoromethyl)phenyl]-4- (ethylsulfinyl)-1H-pyrazole-3- (2) Tolerances are established for res- carbonitrile. idues of the herbicide indaziflam, N- [(1R,2S)-2,3-dihydro-2,6-dimethyl-1H- Commodity Parts per inden-1-yl]-6-(1-fluoroethyl)-1,3,5-tri- million azine-2,4-diamine, including its me- Coffee, green bean 1 ...... 0.1 tabolites and degradates, in or on the Rice, grain 1 ...... 1.7 commodities in the following table. 1 Tea, dried ...... 30 Compliance with the tolerance levels 1 There are no U.S. registrations for this commodity as of specified in the following table is to be June 28, 2019. determined by measuring only (b) Section 18 emergency exemptions. indaziflam in or on the commodity. [Reserved] (c) Tolerances with regional registra- TABLE 2 TO PARAGRAPH (a)(2) tions. [Reserved] (d) Indirect or inadvertent residues. Commodity Parts per [Reserved] million [76 FR 18921, Apr. 6, 2011, as amended at 84 Cattle, fat ...... 0.07 FR 30939, June 28, 2019] Cattle, meat ...... 0.01 Cattle, meat byproducts ...... 0.2 § 180.653 Indaziflam; tolerances for Goat, fat ...... 0.07 residues. Goat, meat ...... 0.01 Goat, meat byproducts ...... 0.2 (a) General. (1) Tolerances are estab- Horse, fat ...... 0.07 lished for residues of the herbicide Horse, meat ...... 0.01 indaziflam, N-[(1R,2S)-2,3-dihydro-2,6- Horse, meat byproducts ...... 0.2 dimethyl-1H-inden-1-yl]-6-(1- Milk ...... 0.01 Milk, fat ...... 0.25 fluoroethyl)-1,3,5-triazine-2,4-diamine, Sheep, fat ...... 0.07 including its metabolites and Sheep, meat ...... 0.01 degradates, in or on the commodities Sheep, meat byproducts ...... 0.2 in the following table. Compliance with the tolerance levels specified in the fol- (b) [Reserved] lowing table is to be determined by (c) Tolerances with regional registra- measuring only indaziflam and FDAT, tions. [Reserved]

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(d) Indirect or inadvertent residues. mined by measuring only flazasulfuron [Reserved] (N-[[(4,6-dimethoxy-2-pyrimidinyl) amino]carbonyl]-3-(trifluoromethyl)-2- [76 FR 18905, Apr. 6, 2011, as amended at 79 FR 4630, Jan. 29, 2014; 82 FR 30987, July 5, pyridinesulfonamide). 2017; 83 FR 8002, Feb. 23, 2018; 84 FR 54516, Parts per Oct. 10, 2019; 85 FR 37762, June 24, 2020] Commodity million § 180.654 Isopyrazam; tolerances for Almond, hulls ...... 0.01 residues. Fruit, citrus, group 10–10 ...... 0.01 Grape ...... 0.01 (a) General. Tolerances are estab- Nut, tree, group 14–12 ...... 0.01 lished for residues of the fungicide Olive ...... 0.01 Sugarcane ...... 0.01 isopyrazam, including its metabolites and degradates, in or on the commod- (b) Section 18 emergency exemptions. ities listed in the following table. Com- [Reserved] pliance with the tolerance levels speci- (c) Tolerances with regional registra- fied in the following table is to be de- tions. [Reserved] termined by measuring only (d) Indirect or inadvertent residues. isopyrazam (3-(difluoromethyl)-1-meth- [Reserved] yl-N-[1,2,3,4-tetrahydro-9-(1- methylethyl)-1,4-methano-naphthalen- [77 FR 10968, Feb. 24, 2012, as amended at 79 5-yl]-1H-pyrazole-4-carboxamide), as FR 52989, Sept. 5, 2014; 82 FR 24066, May 25, 2017] the sum of its syn-isomer (3- (difluoromethyl)-1-methyl-N-[(1RS, § 180.656 Amisulbrom; tolerances for 4SR, 9RS)-1,2,3,4-tetrahydro-9-(1- residues. methylethyl)-1,4-methanonaphthalen- (a) General. Tolerances are estab- 5-yl]-1H-pyrazole-4-carboxamide) and lished for residues of the fungicide anti-isomer (3-(difluoromethyl)-1-meth- amisulbrom, including its metabolites yl-N-[(1RS, 4SR, 9SR)-1,2,3,4- and degradates, in or on the commod- tetrahydro-9-(1-methylethyl)-1,4- ities listed below. Compliance with the methano-naphthalen-5-yl]-1H-pyrazole- tolerance levels is to be determined by 4-carboxamide) in or on the com- measuring only amisulbrom, 3-[(3- modity. bromo-6-fluoro-2-methyl-1H-indole-1- Parts per yl) sulfonyl]-N, N-dimethyl-1H-1, 2, 4- Commodity million triazole-1-sulfonamide]. Apple1 ...... 0.70 1 Parts per Banana1 ...... 0.05 Commodity million Peanut1 ...... 0.01 Pepper, bell 1 ...... 0.50 Grape ...... 0.40 Tomato 1 ...... 0.50 Grape, raisin ...... 1.0 Vegetable, cucurbit, subgroup 9A 1 ...... 0.30 Tomato ...... 0.50 Tomato, paste ...... 1.2 1 There are no U.S. registrations for use of isopyrazam on these commodities. 1 There is no U.S. registration for use of amisulbrom on grape or tomato. (b) Section 18 emergency exemptions. [Reserved] (b) Section 18 emergency exemptions. (c) Tolerances with regional registra- [Reserved] tions. [Reserved] (c) Tolerances with regional registra- (d) Indirect or inadvertent residues. tions. [Reserved] [Reserved] (d) Indirect or inadvertent residues. [Reserved] [76 FR 61596, Oct. 5, 2011, as amended at 78 FR 78745, Dec. 27, 2013; 82 FR 24075, May 25, 2017] [76 FR 59914, Sept. 28, 2011]

§ 180.655 Flazasulfuron; tolerances for § 180.657 Metaflumizone; tolerances residues. for residues. (a) General. Tolerances are estab- (a) General. Tolerances are established for residues of flazasulfuron, in- lished for residues of the insecticide cluding its metabolites and degradates, metaflumizone, including its metabo- in or on the commodities in the table lites and degradates, in or on the com- below. Compliance with the tolerance modities listed in the following table. levels specified below is to be deter- Compliance with the tolerance levels

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specified in the following table is to be Commodity Parts per determined by measuring only the sum million of metaflumizone (E and Z isomers; 2- Bushberry subgroup 13–07B ...... 6 [2-(4-cyanophenyl)-1-[3- Caneberry subgroup 13–07A ...... 10 (trifluoromethyl) phenyl]ethylidene]- Celtuce ...... 30 Corn, field, forage ...... 40 N-[4-(trifluoromethoxy)phenyl] Corn, field, grain ...... 0.01 hydrazinecarboxamide) and its metabo- Corn, field, refined oil ...... 0.05 lite 4-{2-oxo-2-[3-(trifluoromethyl) Corn, field, stover ...... 15 } Corn, pop, grain ...... 0.01 phenyl]ethyl -benzonitrile, calculated Corn, sweet, kernel plus cob with husks removed 0.01 as the stoichiometric equivalent of Cotton, gin byproducts ...... 15 metaflumizone, in or on the following Fennel, Florence, fresh leaves and stalk ...... 30 commodities: Fruit, pome, group 11–10 ...... 0.50 Fruit, stone, group 12–12 ...... 4 Grain, aspirated fractions ...... 30 Parts per Commodity million Kohlrabi ...... 5 Leaf petiole vegetable subgroup 22B ...... 30 Almond, hulls ...... 0.04 Leafy greens subgroup 4–16A ...... 30 Eggplant 1 ...... 1.5 Millet, spp...... 0.80 Fruit, citrus, group 10–10 ...... 0.04 Nut, tree, group 14 1 ...... 0.06 Fruit, pome, group 11–10 ...... 0.04 Nut, tree, group 14–12 ...... 0.05 Fruit, stone, group 12–12 ...... 0.04 Oat, forage ...... 40 Grape ...... 0.04 Oat, grain ...... 0.15 Nut, tree, group 14–12 ...... 0.04 Oat, hay ...... 80 Pepper 1 ...... 1.5 Oat, straw ...... 1.0 Tomato 1 ...... 0.60 Oilseed group 20 ...... 1.5 Tomato, paste 1 ...... 1.2 Pea and bean, dried shelled, except soybean, subgroup 6C ...... 0.40 1 There are no U.S. registrations as of April 4, 2014. Peanut ...... 0.04 (b) Section 18 emergency exemptions. Peanut, hay ...... 30 Peanut, refined oil ...... 0.06 [Reserved] Pistachio 1 ...... 0.06 (c) Tolerances with regional registra- Potato, processed potato waste ...... 0.20 tions. [Reserved] Rye, forage ...... 40 (d) Indirect or inadvertent residues. Rye, grain ...... 0.15 Rye, straw ...... 1.0 [Reserved] Sorghum, forage ...... 40 [77 FR 10386, Feb. 22, 2012, as amended at 79 Sorghum, grain, grain ...... 0.80 Sorghum, stover ...... 15 FR 18810, Apr. 4, 2014; 80 FR 66800, Oct. 30, Soybean, seed ...... 0.40 2015] Teosinte, grain ...... 0.15 Tomato, paste ...... 3.5 § 180.658 Penthiopyrad; tolerances for Triticale, forage ...... 40 residues. Triticale, grain ...... 0.15 Triticale, hay ...... 80 (a) General. (1) Tolerances are estab- Triticale, straw ...... 1.0 lished for residues of penthiopyrad, in- Vegetable, brassica, head and stem, group 5–16 5 cluding its metabolites and degradates, Vegetable, bulb, group 3–07 ...... 3.0 Vegetable, cucurbit, group 9 ...... 0.60 in or on the commodities in the table Vegetable, foliage of legume, group 7, hay ...... 200 below. Compliance with the tolerance Vegetable, foliage of legume, group 7, vines/for- levels specified below is to be deter- age ...... 50 Vegetable, fruiting, group 8–10 ...... 3.0 mined by measuring only penthiopyrad Vegetable, leaves of root and tuber, group 2 ...... 50 (N-[2-(1,3-dimethylbutyl)-3-thienyl]-1- Vegetable, legume, edible podded, subgroup 6A 4.0 methyl-3-(trifluoromethyl)-1H-pyr- Vegetable, legume, succulent shelled, subgroup azole-4-carboxamide). 6B ...... 0.40 Vegetable, root, subgroup 1B, except sugar beet 3.0 Vegetable, tuber and corm, subgroup 1C ...... 0.06 Parts per Commodity million Wheat, forage ...... 40 Wheat, grain ...... 0.15 Alfalfa, forage ...... 7.0 Wheat, hay ...... 80 Alfalfa, hay ...... 20 Wheat, milled byproducts ...... 0.30 Almond, hulls ...... 6.0 Wheat, straw ...... 1.0 Apple, wet pomace ...... 1.5 1 This tolerance expires on December 6, 2019. Barley, grain ...... 0.15 Barley, hay ...... 80 (2) Tolerances are established for res- Barley, milled byproducts ...... 0.90 Barley, straw ...... 1.0 idues of penthiopyrad, including its Beet, sugar, dried pulp ...... 1.5 metabolites and degradates, in or on Beet, sugar, roots ...... 0.5 the commodities in the table below. Berry, low growing, subgroup 13–07G ...... 3.0 Brassica, leafy greens, subgroup 4–16B ...... 50 Compliance with the tolerance levels Buckwheat, grain ...... 0.15 specified below is to be determined by

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measuring only the sum of (2) Tolerances are established for res- penthiopyrad (N-[2-(1,3-dimethylbutyl)- idues of the herbicide pyroxasulfone, 3-thienyl]-1-methyl-3- including its metabolites and (trifluoromethyl)-1H-pyrazole-4- degradates, in or on the commodities carboxamide) and its metabolite (1- in the table below. Compliance with methyl-3-trifluoromethyl-1H-pyrazole- the tolerance levels specified below is 4-carboxamide), calculated as the stoi- to be determined by measuring only chiometric equivalent of penthiopyrad, the sum of pyroxasulfone, 3-[[[5- in or on the commodity. (difluoromethoxy)-1-methyl-3- (trifluoromethyl)-1H-pyrazol-4- Parts per Commodity million yl]methyl]sulfonyl]-4,5-dihydro-5,5- dimethylisoxazole, and its metabolites, Cattle, fat ...... 0.03 5-(difluoromethoxy)-1-methyl-3- Cattle, meat ...... 0.03 (trifluoromethyl)-1H-pyrazol-4- Cattle, meat byproducts ...... 0.09 Goat, fat ...... 0.03 yl]methanesulfonic acid (M–1); 5- Goat, meat ...... 0.03 (difluoromethoxy)-1-methyl-3- Goat, meat byproducts ...... 0.09 (trifluoromethyl)-1H-pyrazol-4-car- Horse, fat ...... 0.03 Horse, meat ...... 0.03 boxylic acid (M-3); and [5- Horse, meat byproducts ...... 0.09 (difluoromethoxy)-3-(trifluoromethyl)- Milk ...... 0.02 1H-pyrazol-4-yl]methanesulfonic acid Sheep, fat ...... 0.03 (M-25), calculated as the stoichiometric Sheep, meat ...... 0.03 Sheep, meat byproducts ...... 0.09 equivalent of pyroxasulfone, in or on the commodity. (b) Section 18 emergency exemptions. Parts per [Reserved] Commodity million (c) Tolerances with regional registrations. [Reserved] Corn, field, forage ...... 0.09 Corn, field, stover ...... 0.15 (d) Indirect or inadvertent residues. Corn, pop, stover ...... 0.15 [Reserved] Corn, sweet, forage ...... 0.10 Corn, sweet, stover ...... 0.15 [77 FR 14297, Mar. 9, 2012, as amended at 84 Cotton, gin byproducts ...... 0.20 FR 26359, June 6, 2019] Soybean, forage ...... 1.0 Soybean, hay ...... 2.0 § 180.659 Pyroxasulfone; tolerances for Wheat, forage ...... 6.0 residues. Wheat, hay ...... 1.0 (a) General. (1) Tolerances are estab- Wheat, straw ...... 0.60 lished for residues of the herbicide (3) Tolerances are established for res- pyroxasulfone, including its metabo- idues of the herbicide pyroxasulfone, lites and degradates, in or on the com- including its metabolites and modities in the table below. Compli- degradates, in or on the commodities ance with the tolerance levels specified in the table below. Compliance with below is to be determined by measuring the tolerance levels specified below is only the sum of pyroxasulfone, 3-[[[5- to be determined by measuring only (difluoromethoxy)-1-methyl-3- the sum of pyroxasulfone, 3-[[[5- (trifluoromethyl)-1H-pyrazol-4- (difluoromethoxy)-1-methyl-3- yl]methyl]sulfonyl]-4,5-dihydro-5,5- (trifluoromethyl)-1H-pyrazol-4- dimethylisoxazole, and its metabolite, yl]methyl]sulfonyl]-4,5-dihydro-5,5- 5-(difluoromethoxy)-1-methyl-3- dimethylisoxazole, and its metabolites, (trifluoromethyl)-1H-pyrazol-4-car- 5-(difluoromethoxy)-1-methyl-3- boxylic acid (M-3), calculated as the (trifluoromethyl)-1H-pyrazol-4-car- stoichiometric equivalent of boxylic acid (M–3); [5- pyroxasulfone, in or on the commodity. (difluoromethoxy)-3-(trifluoromethyl)- Parts per 1H-pyrazol-4-yl]methanesulfonic acid Commodity million (M–25); and 3-[1-carboxy-2-(5,5-dimethyl-4,5-dihydroisoxazol-3- Corn, field, grain ...... 0.02 Corn, pop, grain ...... 0.015 ylthio)ethylamino]-3-oxopropanoic acid Corn, sweet, kernel plus cob with husks removed 0.015 (M–28), calculated as the stoichio- Cottonseed, subgroup 20C ...... 0.04 metric equivalent of pyroxasulfone, in Wheat, grain ...... 0.03 or on the commodity.

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Parts per Parts per Commodity million Commodity million

Soybean, seed ...... 0.06 Leaf petiole vegetable subgroup 22B ...... 0.80 Pea and bean, dried shelled, except soybean, (4) Tolerances are established for res- subgroup 6C ...... 0.15 Peanut ...... 0.30 idues of the herbicide pyroxasulfone, Peanut, hay ...... 4.0 including its metabolites and Peanut, meal ...... 0.40 degradates, in or on the commodities Potato, granules/flakes ...... 0.20 in the following table. Compliance with Peppermint, fresh leaves ...... 0.20 the tolerance levels specified in the fol- Peppermint, oil ...... 0.70 Soybean, vegetable, succulent shelled ...... 0.40 lowing table is to be determined by Spearmint, fresh leaves ...... 0.20 measuring only the sum of Spearmint, oil ...... 0.70 pyroxasulfone [3-[[[5- Sunflower subgroup 20B ...... 0.30 (difluoromethoxy)-1-methyl-3- Vegetable, bulb, group 3–07 ...... 0.15 Vegetable, foliage of legume, except soybean, (trifluoromethyl)-1H-pyrazol-4- subgroup 7A ...... 3.0 yl]methyl]sulfonyl]-4,5-dihydro-5,5- Vegetable, soybean, edible podded ...... 0.40 dimethylisoxazole] and its metabolites Vegetable, tuberous and corm, subgroup 1C ...... 0.08 [5-(difluoromethoxy)-1-methyl-3- (trifluoromethyl)-1H-pyrazol-4- (b) Section 18 emergency exemptions. yl]methanesulfonic acid (M–1) and 5- [Reserved] (difluoromethoxy)-1-methyl-3- (c) Tolerance with regional registra- (trifluoromethyl)-1H-pyrazol-4-car- tions. Tolerances are established for boxylic acid (M–3), calculated as the residues of the herbicide stoichiometric equivalent of pyroxasulfone, including its metabo- pyroxasulfone, in or on the commodity. lites and degradates, in or on the commodities in the table below. Compli- Parts per ance with the tolerance levels specified Commodity million below is to be determined by measuring Milk ...... 0.003 only the sum of pyroxasulfone (3-[(5- difluoromethoxy-1-methyl-3- (5) Tolerances are established for res- (trifluoromethyl)pyrazol-4- idues of the herbicide pyroxasulfone, ylmethylsulfonyl]-4,5-dihydro-5,5-di- including its metabolites and methyl-1,2-oxazole), and its metabo- degradates, in or on the commodities lites, M–1 (5-difluoromethoxy-1-methyl- in the table below. Compliance with 3-trifluoromethyl-1H-pyrazol-4- the tolerance levels specified below is yl)methanesulfonic acid), M–3 (5- to be determined by measuring only difluoromethoxy-1-methyl-3- the sum of pyroxasulfone (3-[(5- trifluoromethyl-1H-pyrazol-4-car- difluoromethoxy-1-methyl-3- boxylic acid), M–25 (5-difluoromethoxy- (trifluoromethyl)pyrazol-4- 3-trifluoromethyl-1H-pyrazol-4- ylmethylsulfonyl]-4,5-dihydro-5,5-di- yl)methanesulfonic acid) and M–28 (3- methyl-1,2-oxazole), and its metabo- [1-carboxy-2-(5,5-dimethyl-4,5- lites, M-1 (5-difluoromethoxy-1-methyl- dihydroisoxazol-3-ylthio)ethylamino]- 3-trifluoromethyl-1H-pyrazol-4-yl) 3-oxopropanoic acid) calculated as the methanesulfonic acid), M-3 (5- stoichiometric equivalent of difluoromethoxy-1-methyl-3- pyroxasulfone, in or on the commodity. trifluoromethyl-1H-pyrazol-4-carboxylic acid), M-25 (5-difluoromethoxy- Parts per 3-trifluoromethyl-1H-pyrazol-4- Commodity million yl)methanesulfonic acid) and M-28 (3- [1-carboxy-2-(5,5-dimethyl-4,5- Grass, forage ...... 0.50 dihydroisoxazol-3-ylthio)ethylamino]- Grass, hay ...... 1.0 3-oxopropanoic acid) calculated as the stoichiometric equivalent of (d) Indirect or inadvertent residues. pyroxasulfone, in or on the following [Reserved] commodities: [77 FR 12213, Feb. 29, 2012, as amended at 78 FR 13257, Feb. 27, 2013; 78 FR 46279, July 31, Parts per Commodity million 2013; 79 FR 34633, June 18, 2014; 82 FR 18235, Apr. 18, 2017; 83 FR 22859, May 17, 2018; 83 FR Flax, seed ...... 0.07 54264, Oct. 29, 2018]

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§ 180.660 Pyriofenone; tolerances for Commodity Parts per residues. million (a) General. Tolerances are estab- Citrus, oil ...... 8.0 lished for residues of the fungicide Corn, field, grain ...... 0.02 Corn, pop, grain ...... 0.02 pyriofenone, including its metabolites Corn, sweet, kernel plus cob with husks removed 0.01 and degradates, in or on the following Cotton, gin byproducts ...... 30 commodities listed in the table. Com- Cottonseed subgroup 20C ...... 0.80 Cranberry 1 ...... 2 pliance with the tolerance levels speci- Dill, seed ...... 70 fied in the table is to be determined by Fruit, citrus, group 10–10 ...... 1.0 measuring only pyriofenone, (5-chloro- Fruit, pome, group 11–10 ...... 0.80 Fruit, small vine climbing, except fuzzy kiwifruit, 2-methoxy-4-methyl-3-pyridinyl)(2,3,4- subgroup 13–07F ...... 2.0 trimethoxy-6-methylphenyl) Grain, aspirated grain fractions ...... 50 methanone, in or on the following com- Grain, cereal, forage, fodder and straw, group 16 20 Grain, cereal, group 15, except corn and rice ...... 4.0 modities: Grape, raisin ...... 3.0 Herb subgroup 19A ...... 40 Commodity Parts per Hop, dried cones ...... 60 million Leafy greens subgroup 4A ...... 40 Leafy petioles subgroup 4B ...... 20 Berry, low growing, subgroup 13–07G (except Lentil, dry seed 1 ...... 0.7 cranberry) ...... 0.50 Melon subgroup 9A ...... 1.0 Bushberry subgroup 13–07B ...... 1.5 Nut, tree, group 14–12 ...... 0.05 Caneberry subgroup 13–07A ...... 0.90 Onion, bulb, subgroup 3–07A ...... 0.40 Fruit, small vine climbing subgroup 13–07D ...... 1.5 Onion, green, subgroup 3–07B ...... 15 Vegetables, cucurbit, crop group 9 ...... 0.30 Pea, dry seed 1 ...... 0.7 Vegetable, fruiting, group 8–10 ...... 0.3 Pea and bean, succulent shelled, subgroup 6B ... 0.20 Peach subgroup 12–12B ...... 1.0 (b) Section 18 emergency exemptions. Peanut ...... 0.20 [Reserved] Pepper/eggplant subgroup 8–10B ...... 4.0 Plum subgroup 12–12C ...... 0.50 (c) Tolerances with regional registra- Potato, wet peel ...... 0.30 tions. [Reserved] Rapeseed subgroup 20A ...... 5.0 (d) Indirect or inadvertent residues. Soybean, seed ...... 0.30 [Reserved] Squash/cucumber subgroup 9B ...... 0.60 Sunflower subgroup 20B ...... 0.70 [77 FR 13506, Mar. 7, 2012, as amended at 82 Tomato subgroup 8–10A ...... 1.0 FR 18240, Apr. 18, 2017; 84 FR 24987, May 30, Vegetable, leaves of root and tuber, group 2 ...... 30 Vegetable, legume, edible podded, subgroup 6A 4.0 2019] Vegetable, root, except sugar beet, subgroup 1B 0.30 Vegetable, tuberous and corm, subgroup 1C ...... 0.10

§ 180.661 Fluopyram; tolerances for 1 residues. There are no U.S. registrations. (a) General. (1) Tolerances are estab- (2) Tolerances are established for res- lished for residues of the fungicide idues of the fungicide fluopyram, N-[2- Fluopyram, N-[2-[3-chloro-5- [3-chloro-5-(trifluoromethyl)-2- (trifluoromethyl)-2-pyridinyl]ethyl]-2- pyridinyl]ethyl]-2- (trifluoromethyl)benzamide, including (trifluoromethyl)benzamide, including its metabolites and degradates in or on its metabolites and degradates. Com- the commodities in the table below. pliance with the tolerance levels speci- Compliance with the tolerance levels fied in the table below is to be deter- specified in the table is to be determined by measuring only the sum of mined by measuring only fluopyram in fluopyram and its metabolite, 2- or on the commodity. (trifluoromethyl)benzamide, calculated as the stoichiometric equivalent of Parts per fluopyram, in or on the commodity. Commodity million Parts per Almond, hulls ...... 10 Commodity million Artichoke, globe ...... 4.0 Banana 1 ...... 1.0 Cattle, fat ...... 0.70 Bean, dry ...... 0.70 Cattle, meat ...... 0.80 Beet, sugar ...... 0.10 Cattle, meat byproducts ...... 7.5 Berry, low growing, except cranberry, subgroup Egg ...... 0.08 13–07G ...... 2.0 Goat, fat ...... 0.70 Brassica, head and stem, subgroup 5A ...... 4.0 Goat, meat ...... 0.80 Brassica, leafy greens, subgroup 5B ...... 50 Goat, meat byproducts ...... 7.5 Bushberry subgroup 13–07B ...... 7.0 Hog, fat ...... 0.20 Caneberry subgroup 13–07A ...... 5.0 Hog, meat ...... 0.02 Cherry subgroup 12–12A ...... 2.0 Hog, meat byproducts ...... 0.20

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its metabolites and degradates, in or Commodity Parts per million on the commodities in the table below. Horse, fat ...... 0.70 Compliance with the tolerance levels Horse, meat ...... 0.80 specified below is to be determined by Horse, meat byproducts ...... 7.5 measuring both trinexapac-ethyl, ethyl Milk ...... 0.40 Poultry, fat ...... 0.04 4-(cyclopropylhydroxymethylene)-3,5- Poultry, meat ...... 0.04 dioxocyclohexanecarboxylate and the Poultry, meat byproducts ...... 0.20 associated metabolite, trinexpac, 4- Sheep, fat ...... 0.70 Sheep, meat ...... 0.80 (cyclopropylhydroxymethylene)-3,5- Sheep, meat byproducts ...... 7.5 dioxocyclohexanecarboxylic acid, calculated as the stoichiometric equiva- (b) Section 18 emergency exemptions. lent of trinexapac-ethyl, in or on the [Reserved] commodity. (c) Tolerances with regional registrations. Tolerances with regional reg- Parts per Commodity million istration, as defined in § 180.1(1), are established for indirect or inadvertent Barley, bran ...... 2.5 residues of fungicide fluopyram, N-[2- Barley, grain ...... 2.0 [3-chloro-5-(trifluoromethyl)-2- Barley, hay ...... 0.8 pyridinyl]ethyl]-2- Barley, straw ...... 0.4 Cattle, fat ...... 0.02 (trifluoromethyl)benzamide, including Cattle, meat ...... 0.02 its metabolites and degradates, in or Cattle, meat byproducts ...... 0.04 on the commodities in the table below. Goat, fat ...... 0.02 Compliance with the tolerance levels Goat, meat ...... 0.02 specified in the table is to be deter- Goat, meat byproducts ...... 0.04 mined by measuring only fluopyram in Grass, forage ...... 1.5 or on the commodity. Grass, hay ...... 4.0 Grass, seed screenings ...... 40.0 Grass, straw ...... 10.0 Parts per Commodity million Hog, fat ...... 0.02 Hog, meat ...... 0.02 Sugarcane, cane ...... 0.08 Hog, meat by-products ...... 0.03 Horse, fat ...... 0.02 (d) Indirect or inadvertent residues. It Horse, meat ...... 0.02 is recommended that tolerances be es- Horse, meat byproducts ...... 0.04 tablished for indirect or inadvertent Oat, forage ...... 1.0 residues of fungicide fluopyram, N-[2- Oat, grain ...... 4.0 Oat, hay ...... 1.5 [3-chloro-5-(trifluoromethyl)-2- Oat, straw ...... 0.9 pyridinyl]ethyl]-2- Poppy, seed imported 1 ...... 8 (trifluoromethyl)benzamide, including Rice, bran ...... 1.5 its metabolites and degradates, in or Rice, grain ...... 0.4 on the commodities in the table below. Rice, straw ...... 0.07 Compliance with the tolerance levels Rice, wild, grain ...... 0.4 Rye, bran ...... 6.0 specified in the table is to be deter- Rye, grain ...... 4.0 mined by measuring only fluopyram in Rye, hay ...... 1.5 or on the commodity. Rye, straw ...... 0.9 Sheep, fat ...... 0.02 Commodity Parts per Sheep, meat ...... 0.02 million Sheep, meat byproducts ...... 0.04 Sugarcane, cane ...... 0.8 Alfalfa, forage ...... 0.45 Alfalfa, hay ...... 1.1 Sugarcane, molasses ...... 2.5 Soybean, seed ...... 0.10 Wheat, bran ...... 6.0 Wheat, forage ...... 1.0 Wheat, grain ...... 4.0 [81 FR 12023, Mar. 8, 2016, as amended at 84 Wheat, hay ...... 1.5 FR 31213, July 1, 2019] Wheat, middlings ...... 10.5 Wheat, straw ...... 0.9 § 180.662 Trinexapac-ethyl; tolerances for residues. (b) Section 18 emergency exemptions. (a) General. Tolerances are estab- [Reserved] lished for residues of the plant growth (c) Tolerances with regional registra- inhibitor, trinexapac-ethyl, including tions. [Reserved]

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(d) Indirect or inadvertent residues. Commodity Parts per [Reserved] million [77 FR 12745, Mar. 2, 2012, as amended at 77 Alfalfa, hay ...... 0.01 FR 60919, Oct. 3, 2012; 80 FR 28848, May 20, Beet, sugar, roots ...... 0.01 ppm 2015; 83 FR 11422, Mar. 15, 2018] Beet, sugar, tops ...... 0.01 ppm Cotton, gin by-products ...... 0.01 Grain cereal, forage, fodder and straw, group 16 0.01 § 180.663 Ametoctradin; tolerances for Grain, cereal, group 15 ...... 0.01 residues. Oilseed, group 20 ...... 0.01 (a) General. Tolerances are estab- Vegetable, bulb, group 3–07 ...... 0.01 ppm lished for residues of the fungicide Vegetable, foliage of legume, group 7 ...... 0.01 ametoctradin, including its metabo- Vegetable, legume, group 6 ...... 0.01 Vegetable, tuberous and corm subgroup 1C ...... 0.01 lites and degradates, in or on the commodities in the following table. Com- (b) Section 18 emergency exemptions. pliance with the tolerance levels speci- [Reserved] fied in the following table is to be de- (c) Tolerances with regional registra- termined by measuring only tions. [Reserved] ametoctradin (5-ethyl-6- (d) Indirect or inadvertent residues. octyl[1,2,4]triazolo[1,5-a]pyrimidin-7- [Reserved] amine). [77 FR 28281, May 14, 2012, as amended at 81 Parts per FR 72007, Oct. 19, 2016] Commodity million

Brassica, head and stem, subgroup 5A ...... 9.0 § 180.665 Sedaxane; tolerances for resi- Brassica, leafy greens, subgroup 5B ...... 50 dues. Grape ...... 4.0 Grape, raisin ...... 8.0 (a) General. Tolerances are estab- Hop, dried cones ...... 100 lished for residues of the fungicide Onion, bulb, subgroup 3–07A ...... 1.5 sedaxane, including its metabolites and Onion, green, subgroup 3–07B ...... 20.0 Spinach ...... 50.0 degradates, in or on the commodities Vegetable, cucurbit, group 9 ...... 3.0 in the following table. Compliance with Vegetable, fruiting, group 8–10 ...... 1.5 the tolerance levels specified in the fol- Vegetable, leafy, except Brassica, group 4, except spinach ...... 40.0 lowing table is to be determined by Vegetable, tuberous and corm, subgroup 1C ...... 0.05 measuring only sedaxane, N-[2-[1,1′- bicyclopropyl]-2-ylphenyl]-3- (b) Section 18 emergency exemptions. (difluoromethyl)-1-methyl-1H-pyrazole- [Reserved] 4-carboxamide, as the sum of its cis- (c) Tolerances with regional registra- and trans-isomers in or on the com- tions. [Reserved] modity. (d) Indirect or inadvertent residues. [Reserved] Parts per Commodity million [77 FR 21734, May 9, 2012, as amended at 82 FR 34877, July 27, 2017] Beet, sugar, roots ...... 0.01 Canola, seed ...... 0.01 Cotton, gin byproducts ...... 0.01 § 180.664 Penflufen; tolerances for resi- Cotton, undelinted seed ...... 0.01 dues. Grain, cereal, forage, fodder and straw, group 16 0.10 (a) General. Tolerances are estab- Grain, cereal, group 15 ...... 0.01 Peanut ...... 0.01 lished for residues of the fungicide Peanut, hay ...... 0.08 penflufen, including its metabolites Potato ...... 0.02 and degradates, in or on the following Potato, wet peel ...... 0.075 commodities listed in the table. Com- Rapeseed, subgroup 20A ...... 0.01 pliance with the tolerance levels speci- Soybean, forage ...... 0.05 Soybean, hay ...... 0.04 fied in the table is to be determined by Soybean, seed ...... 0.01 measuring only penflufen N-[2-(1,3- Vegetable, foliage of legume, except soybean, dimethylbutyl)phenyl]-5-fluoro-1,3-di- subgroup 7A ...... 0.01 methyl-1H-pyrazole-4-carboxamide, in Vegetable, legume, group 6 ...... 0.01 or on the following commodities. (b) Section 18 emergency exemptions. Commodity Parts per [Reserved] million (c) Tolerances with regional registra- Alfalfa, forage ...... 0.01 tions. [Reserved]

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(d) Indirect inadvertent residues. [Re- Commodity Parts per served] million [77 FR 36924, June 20, 2012, as amended at 78 Milk, fat ...... 0.15 FR 33748, June 5, 2013; 78 FR 60719, Oct. 2, Non-grass animal feed, group 18 ...... 30 Nut, tree, group 14–12 ...... 0.06 2013; 80 FR 43329, July 22, 2015; 82 FR 57871, Oilseeds, group 20 (except cottonseed) ...... 0.9 Dec. 8, 2017; 84 FR 44707, Aug. 27, 2019] Papaya 1 ...... 0.6 Pea and bean, dried shelled except soybean, § 180.666 Fluxapyroxad; tolerances for subgroup 6C ...... 0.4 residues. Pea and bean, succulent shelled, subgroup 6B ... 0.5 Peanut ...... 0.01 (a) General. Tolerances are estab- Peanut, refined oil ...... 0.02 lished for residues of the fungicide Plum, prune, dried ...... 3.0 Potato, wet peel ...... 0.1 fluxapyroxad, including its metabolites Poultry, fat ...... 0.01 and degradates, in or on the commod- Poultry, meat ...... 0.01 ities listed in the table below. Compli- Poultry, meat byproduct ...... 0.01 Rice, bran ...... 4.5 ance with the tolerance levels specified Rice, bran ...... 8.5 below is to be determined by measuring Rice, grain ...... 5.0 only fluxapyroxad, 3-(difluoromethyl)- Rice, hulls ...... 8.0 ′ ′ ′ ′ Rice, hulls ...... 15.0 1-methyl-N-(3 ,4 ,5 -trifluoro[1,1 - Sheep, fat ...... 0.06 biphenyl]-2-yl)-1H-pyrazole-4- Sheep, meat ...... 0.01 carboxamide in or on the commodity. Sheep, meat byproduct ...... 0.04 Soybean, hulls ...... 0.3 Parts per Soybean, seed ...... 0.15 Commodity million Sugarcane, cane ...... 3.0 Vegetable, brassica leafy, group 5 ...... 4.0 Almond, hulls ...... 4.0 Vegetable, bulb, group 3–07 ...... 1.5 Apple, wet pomace ...... 2.0 Vegetable, cucurbit, group 9 ...... 0.50 Banana 1 ...... 3.0 Vegetable, foliage of legume, group 7 ...... 30 Beet, sugar ...... 0.1 Vegetables, fruiting, group 8 ...... 0.7 Beet, sugar, dried pulp ...... 0.1 Vegetable, leafy, except brassica, group 4 ...... 30 Beet, sugar, tops ...... 7.0 Vegetable, legume, edible podded, subgroup 6A 2.0 Berry, low growing, subgroup 13–07G ...... 4.0 Vegetable, root, except sugarbeet, subgroup 1B 0.90 Bushberry, subgroup 13–07B ...... 7.0 Vegetable, tuberous and corm, subgroup 1C ...... 0.02 Caneberry, subgroup 13–07A ...... 5.0 Wheat, bran ...... 0.6 Cattle, fat ...... 0.06 Wheat, grain ...... 0.3 Cattle, meat ...... 0.01 1 There are no U.S. registrations for this commodity as of Cattle, meat byproduct ...... 0.04 November 8, 2016. Citrus, dried pulp ...... 3.0 Citrus, oil ...... 40 (b) Section 18 emergency exemptions. Coffee, green bean 1 ...... 0.2 [Reserved] Corn, field, grain ...... 0.01 Corn, oil ...... 0.03 (c) Tolerances with regional registra- Corn, pop, grain ...... 0.01 tions. [Reserved] Corn, sweet, kernels plus cobs with husks re- (d) Indirect or inadvertent residues. moved ...... 0.15 Tolerances are established for the com- Cotton, gin byproducts ...... 20 Cotton, undelinted seed ...... 0.30 bined indirect or inadvertent residues Egg ...... 0.01 of the fungicide fluxapyroxad, includ- Fish-freshwater finfish ...... 0.01 ing its metabolites and degradates, in Fish-shellfish, crustacean ...... 0.01 Fruit, citrus, group 10–10 ...... 1.0 or on the commodities listed in the Fruit, pome, group 11 ...... 0.8 table below. Compliance with the toler- Fruit, small, vine climbing, except fuzzy kiwifruit, ance levels specified below is to be de- subgroup 13–07F ...... 2.0 Fruit, stone, group 12–12 ...... 3.0 termined by measuring only Goat, fat ...... 0.06 fluxapyroxad, 3-(difluoromethyl)-1- Goat, meat ...... 0.01 methyl-N-(3′,4′,5′-trifluoro[1,1′- Goat, meat byproduct ...... 0.04 biphenyl]-2-yl)-1H-pyrazole-4- Grain, aspirated fractions ...... 20.0 Grain, cereal, forage, fodder and straw, group 16 20 carboxamide in or on the commodity. Grain, cereal, group 15, (except corn, field, grain; except corn, pop, grain; except corn, kernels Commodity Parts per plus cobs with husks removed; except rice; ex- million cept wheat ...... 3.0 Grape, raisin ...... 5.7 Peppermint, tops ...... 0 .01 Spearmint, tops ...... 0 .01 Grass, forage, fodder and hay, group 17 ...... 40 Hog, meat byproducts ...... 0.01 Horse, fat ...... 0.06 [77 FR 28275, May 14, 2012, as amended at 77 Horse, meat ...... 0.01 Horse, meat byproduct ...... 0.04 FR 46307, Aug. 3, 2012; 79 FR 10677, Feb. 26, Mango 1 ...... 0.7 2014; 80 FR 45078, July 29, 2015; 81 FR 27025, Milk ...... 0.01 May 5, 2016; 81 FR 78511, Nov. 8, 2016]

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§ 180.667 Cyflufenamid, tolerance for Commodity Parts per residues. million (a) General. Tolerances are estab- Barley, straw ...... 2.0 lished for residues of the fungicide Bean, dry seed ...... 0.20 Bean, succulent ...... 4.0 cyflufenamid, including its metabolites Beet, sugar, dried pulp ...... 0.07 and degradates, in or on the commod- Beet, sugar, molasses ...... 0.25 ities in the table below. Compliance Berry, low growing, subgroup 13–7G ...... 0.70 Brassica, leafy greens, subgroup 4–16B, except with the tolerance levels specified watercress ...... 2 below is to be determined by measuring Bushberry subgroup 13–07B ...... 2 only cyflufenamid, [N(Z)]-N- Cacao, dried bean ...... 0.05 Caneberry subgroup 13–07A ...... 1.5 [[(cyclopropylmethoxy)amino][2,3- Cattle, fat ...... 0.2 difluoro-6- Cattle, meat ...... 0.4 (trifluoromethyl)phenyl]methylene] Cattle, meat byproducts ...... 0.8 benzeneacetamide. Cauliflower ...... 0.08 Celtuce ...... 2 Citrus, dried pulp ...... 3.6 Parts per Commodity million Corn, field, forage ...... 0.5 Corn, field, grain ...... 0.015 Apple, wet pomace ...... 0.10 Corn, field, stover ...... 0.8 Berry, low growing, subgroup 13–07G, except Corn, pop, grain ...... 0.015 cranberry ...... 0.20 Corn, pop, stover ...... 0.8 Cherry subgroup 12–12A ...... 0.60 Corn, sweet, forage ...... 0.6 Fruit, pome, group 11 ...... 0.06 Corn, sweet, kernel plus cob with husks removed 0.01 Fruit, small vine climbing, except fuzzy kiwifruit, Corn, sweet, stover ...... 0.7 subgroup 13–07F ...... 0.15 Cotton, gin byproducts ...... 6.0 Grape, raisin ...... 0.30 Cotton, hulls ...... 0.35 Hop, dried cones ...... 5.0 Cottonseed subgroup 20C ...... 0.20 Vegetable, cucurbit, group 9 ...... 0.10 Cress, garden 1 ...... 6 Vegetable, fruiting, group 8–10 ...... 0.20 Cress, upland 1 ...... 6 Egg ...... 0.06 (b) Section 18 emergency exemptions. Fennel, Florence, fresh leaves and stalk ...... 2 Fruit, citrus, group 10–10 ...... 0.70 [Reserved] Fruit, pome, group 11–10 ...... 0.50 (c) Tolerances with regional registra- Fruit, small, vine climbing, subgroup 13–07F, ex- tions. [Reserved] cept fuzzy kiwi fruit ...... 2.0 Fruit, stone, group 12–12 ...... 3 (d) Indirect or inadvertent residues. Goat, fat ...... 0.2 [Reserved] Goat, meat ...... 0.4 Goat, meat byproducts ...... 0.8 [77 FR 38210, June 27, 2012, as amended at 83 Grain, aspirated fractions ...... 20.0 FR 5717, Feb. 9, 2018] Grape, raisin ...... 6.0* Hog, fat ...... 0.03 § 180.668 Sulfoxaflor; tolerances for Hog, meat ...... 0.3 residues. Hog, meat byproducts ...... 0.6 Horse, fat ...... 0.2 (a) General. Tolerances are estab- Horse, meat ...... 0.4 lished for residues of the insecticide Horse, meat byproducts ...... 0.8 sulfoxaflor, including its metabolites Kohlrabi ...... 2 Leaf petiole vegetable subgroup 22B ...... 2 and degradates, in or on the commod- Leafy greens subgroup 4–16A ...... 6 ities in the table. Compliance with the Milk ...... 0.3 tolerance levels specified is to be deter- Millet, proso, forage ...... 0.4 Millet, pearl, forage ...... 0.4 mined by measuring only sulfoxaflor Millet, proso, grain ...... 0.3 (N-[methyloxido[1-[6-(trifluoromethyl)- Millet, pearl, grain ...... 0.3 3-pyridinyl]ethyl]-g4- Nut, tree, group 14–12 ...... 0.015 sulfanylidene]cyanamide). Oat, grain ...... 0.4 Oat, hay ...... 1 Oat, straw ...... 2 Parts per Commodity million Onion, bulb, subgroup 3–07A ...... 0.01 Onion, green, subgroup 3–07B ...... 0.70 Alfalfa, forage ...... 7 Pineapple ...... 0.1 Alfalfa, hay ...... 20 Poultry, fat ...... 0.02 Alfalfa, seed ...... 40 Poultry, meat ...... 0.1 Alfalfa, silage ...... 9 Poultry, meat byproducts ...... 0.3 Almond, hulls ...... 6.0 Rapeseed, meal ...... 0.50 Artichoke, globe ...... 0.7 Rapeseed subgroup 20A ...... 0.40 Arugula 1 ...... 6 Rice, grain ...... 5 Asparagus ...... 0.01 Rice, hulls ...... 15 Avocado ...... 0.15 Rye, forage ...... 1 Barley, grain ...... 0.40 Rye, grain ...... 0.08 Barley, hay ...... 1.0 Rye, hay ...... 1.5

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(d) Indirect or inadvertent residues. Commodity Parts per million [Reserved] Rye, straw ...... 2 [77 FR 59565, Sept. 28, 2012, as amended at 78 Sheep, fat ...... 0.2 FR 38227, June 26, 2013; 80 FR 4515, Jan. 28, Sheep, meat ...... 0.4 2015; 82 FR 57151, Dec. 4, 2017; 84 FR 35553, Sheep, meat byproducts ...... 0.8 July 24, 2019; 84 FR 57343, Oct. 25, 2019] Sorghum, grain, forage ...... 0.4 Sorghum, grain, grain ...... 0.3 § 180.669 Picoxystrobin; tolerances for Sorghum, grain, stover ...... 1 residues. Soybean, seed ...... 0.20 Sunflower subgroup 20B ...... 0.3 (a) General. Tolerances are estab- Teff, forage ...... 1 lished for residues of the fungicide Teff, grain ...... 0.08 picoxystrobin, including its metabo- Teff, hay ...... 1.5 lites and degradates, in or on the com- Teff, straw ...... 2 modities listed below. Compliance with Teosinte, grain ...... 0.015 Tomato, paste ...... 2.60 the tolerance levels specified below is Tomato, puree ...... 1.20 to be determined by measuring only Triticale, forage ...... 1 picoxystrobin, methyl (aE)-a- Triticale, grain ...... 0.08 (methoxymethylene)-2-[[[6- Triticale, hay ...... 1.5 (trifluoromethyl)-2- Triticale, straw ...... 2 pyridinyl]oxy]methyl]benzeneacetate. Vegetable, brassica, head and stem, group 5–16, except cauliflower ...... 2 Parts per Vegetable, cucurbit, group 9 ...... 0.40 Commodity million Vegetable, fruiting, group 8–10 ...... 0.70 Vegetable, leaves of root and tuber, group 2 ...... 3.0 Alfalfa, forage ...... 4.0 Vegetable, legume, foliage, group 7 ...... 3.0 Alfalfa, hay ...... 5.0 Alfalfa, seed ...... 9.0 Vegetable, root and tuber, group 1 ...... 0.05 Almond, hulls ...... 7.0 Watercress ...... 6.0 Barley, bran ...... 0.5 Wheat, forage ...... 1.0 Barley, grain ...... 0.3 Wheat, grain ...... 0.08 Beet, sugar, dried pulp ...... 1.5 Wheat, hay ...... 1.5 Bluegrass, forage ...... 30 Wheat, straw ...... 2.0 Bluegrass, hay ...... 60 Bromegrass, forage ...... 30 1 This tolerance expires on January 24, 2020. Bromegrass, hay ...... 60 Cattle, fat ...... 0.01 (b) Section 18 emergency exemptions. Cattle, meat ...... 0.01 Time-limited tolerances specified in Cattle, meat byproducts ...... 0.01 Corn, field, refined oil ...... 0.07 the following table are established for Cotton, gin byproducts ...... 20 residues of sulfoxaflor (N- Cottonseed subgroup 20C ...... 2.0 [methyloxido[1-[6-(trifluoromethyl)-3- Eggs ...... 0.01 Fescue, forage ...... 30 λ4 pyridinyl]ethyl]- - Fescue, hay ...... 60 sulfanylidene]cyanamide), including its Goat, fat ...... 0.01 metabolites and degradates, in or on Goat, meat ...... 0.01 Goat, meat byproducts ...... 0.01 the specified agricultural commodities, Grain, aspirated grain fractions ...... 10 resulting from use of the pesticide pur- Grain, cereal, forage, fodder, and straw, group suant to FIFRA section 18 emergency 16, forage ...... 15 Grain, cereal, forage, fodder, and straw, group exemptions. Compliance with the toler- 16, hay ...... 5 ance levels specified in the following Grain, cereal, forage, fodder, and straw, group 16, stover ...... 10 table is to be determined by measuring Grain, cereal, forage, fodder, and straw, group only sulfoxaflor in or on the com- 16, straw ...... 2 modity. The tolerances expire on the Grain, cereal, group 15, except rice and barley ... 0.04 Hog, fat ...... 0.01 date specified in the table. Hog, meat ...... 0.01 Hog, meat byproducts ...... 0.01 Parts per Expiration/ Horse, fat ...... 0.01 Commodity revocation Horse, meat ...... 0.01 million date Horse, meat byproducts ...... 0.01 Leaf petiole vegetable subgroup 22B ...... 20 Sorghum, forage ...... 0.4 12/31/20 Lettuce, head ...... 4.0 Sorghum, grain ...... 0.3 12/31/20 Milk ...... 0.01 Sorghum, stover ...... 0.9 12/31/20 Nut, tree, group 14–12 ...... 0.08 Onion, bulb, subgroup 3–07A ...... 0.50 (c) Tolerances with regional registra- Onion, green, subgroup 3–07B ...... 10 Orchardgrass, forage ...... 30 tions. [Reserved] Orchardgrass, hay ...... 60

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Parts per Parts per Commodity million Commodity million

Pea and bean, dried shelled, except soybean, Fruit, small vine climbing, except fuzzy kiwifruit, subgroup 6C ...... 0.06 subgroup 13–07F ...... 3 Pea and bean, succulent shelled, subgroup 6B ... 0.90 Ginseng ...... 0.7 Peanut ...... 0.05 Grape, juice ...... 4 Peanut, hay ...... 30 Lettuce, head ...... 1.5 Potato, wet peel ...... 0.10 Lettuce, leaf ...... 2 Poultry, fat ...... 0.01 Pistachio ...... 0.02 Poultry, meat ...... 0.01 Poultry, meat byproducts ...... 0.01 (b) Section 18 emergency exemptions. Rapeseed subgroup 20A ...... 0.08 [Reserved] Ryegrass, forage ...... 30 Ryegrass, hay ...... 60 (c) Tolerances with regional registra- Sheep, fat ...... 0.01 tions. [Reserved] Sheep, meat ...... 0.01 (d) Indirect or inadvertent residues. Sheep, meat byproducts ...... 0.01 Soybean, forage ...... 1 [Reserved] Soybean, hay ...... 3 [78 FR 14465, Mar. 6, 2013] Soybean, hulls ...... 0.2 Soybean, seed ...... 0.05 Sunflower subgroup 20B ...... 2.0 § 180.672 Cyantraniliprole; tolerances Switchgrass, forage ...... 30 for residues. Switchgrass, hay ...... 60 (a) General. Tolerances are estab- Vegetable, brassica, head and stem, group 5–16 2.0 Vegetable, cucurbit, group 9 ...... 0.30 lished for the combined residues of the Vegetable, foliage of legume, except soybean, insecticide cyantraniliprole, 3-bromo-1- subgroup 7A ...... 40 (3-chloro-2-pyridinyl)-N-[4-cyano-2- Vegetable, fruiting, group 8–10 ...... 0.70 methyl-6-[((methylamino)car- Vegetable, leafy, group 4–16, except lettuce, head ...... 30 bonyl]phenyl]-1H-pyrazole-5- Vegetable, leaves of root and tuber, group 2 ...... 30 carboxamide, including its metabolites Vegetable, legume, edible podded, subgroup 6A 2.0 and degradates, in or on commodities Vegetable, root, subgroup 1A ...... 0.50 Vegetable, tuberous and corm, subgroup 1C ...... 0.03 in the following table. Compliance with Wheat, bran ...... 0.06 the tolerance levels specified in the fol- Wheat, germ ...... 0.09 lowing table is to be determined by measuring only cyantraniliprole in or (b) Section 18 emergency exemptions. on the commodity. [Reserved] (c) Tolerances with regional registra- Commodity Parts per tions. [Reserved] million (d) Indirect or inadvertent residues. Almond, hulls ...... 8.0 [Reserved] Artichoke, globe 1 ...... 0.10 Berry, low growing, except strawberry, subgroup [77 FR 72231, Dec. 5, 2012, as amended at 83 13–07H, except blueberry, lowbush and FR 39610, Aug. 10, 2018] lingonberry ...... 0.08 Brassica, leafy greens, subgroup 4–16B ...... 30 Bushberry, subgroup 13–07B ...... 4.0 § 180.671 Fenpyrazamine; tolerances Caneberry subgroup 13–07A ...... 4.0 for residues. Cattle, fat ...... 0.10 (a) General. Tolerances are estab- Cattle, meat ...... 0.10 Cattle, meat byproducts ...... 0.40 lished for residues of the fungicide Celtuce ...... 20 fenpyrazamine, in or on the following Cherry, subgroup 12–12A ...... 6.0 commodities. Compliance with the tol- Citrus, oil ...... 2.4 Coffee, green bean ...... 0.05 erance levels specified in the following Corn, field, grain ...... 0.01 table is to be determined by measuring Corn, pop, grain ...... 0.01 only fenpyrazamine S-allyl 5-amino-2- Corn, sweet, kernel plus cob with husks removed 0.01 Cotton, gin byproducts ...... 10 isopropyl-4-(2-methylphenyl)-3-oxo-2,3- Fennel, Florence, fresh leaves and stalk ...... 20 dihydropyrazole-1-carbothioate, in or Fruit, citrus, group 10–10 ...... 0.70 on the following commodities: Fruit, pome, group 11–10 ...... 1.5 Goat, fat ...... 0.10 Parts per Goat, meat ...... 0.10 Commodity million Goat, meat byproducts ...... 0.40 Grain, aspirated grain fractions ...... 200 Almond ...... 0.02 Grape, wine 1 ...... 2.0 Almond, hulls ...... 1.5 Horse, fat ...... 0.10 Berry, low growing, subgroup 13–07G ...... 3 Horse, meat ...... 0.10 Bushberry subgroup 13–07B ...... 5 Horse, meat byproducts ...... 0.40 Caneberry subgroup 13–07A ...... 5 Kohlrabi ...... 3.0

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Parts per [79 FR 6833, Feb. 5, 2014, as amended at 82 FR Commodity million 14629, Mar. 22, 2017; 83 FR 56267, Nov. 13, 2018; 85 FR 8457, Feb. 14, 2020] Leaf petiole vegetable subgroup 22B ...... 20 Leafy greens subgroup 4–16A ...... 20 Milk ...... 0.20 § 180.673 Triforine; tolerances for resi- Nut, tree, group 14–12 ...... 0.04 dues. Oilseed group 20 ...... 1.5 Olive 1 ...... 1.5 (a) General. Tolerances are estab- Olive, oil 1 ...... 2.0 lished for residues of triforine, includ- Onion, bulb, subgroup 3–07A ...... 0.04 ing its metabolites and degradates. Onion, green, subgroup 3–07B ...... 8.0 Peach, subgroup 12–12B ...... 1.5 Compliance with the tolerance levels Peanut ...... 0.01 specified in the following table is to be Peanut hay ...... 3.0 determined by measuring only triforine Plum, subgroup 12–12C ...... 0.50 ′ Pomegranate 1 ...... 0.01 (N,N -[1,2-piperazinediylbis(2,2,2- Rice, grain ...... 0.02 trichloroehylidene)]bis[formamide]), in Rice, hulls ...... 0.05 or on the following commodities. Rice, straw ...... 0.015 Sheep, fat ...... 0.10 Parts per Sheep, meat ...... 0.10 Commodity million Sheep, meat byproducts ...... 0.40 Soybean, forage ...... 15 Blueberry 1 ...... 1.0 Soybean, hay ...... 50 Tomato 1 ...... 0.5 Soybean, hulls ...... 1.0 Soybean, seed ...... 0.40 1 There are no U.S. registrations for blueberry and tomato. Strawberry ...... 1.5 Tea 1 ...... 30 (b) Section 18 emergency exemptions. Vegetable, Brassica, head and stem, group 5–16 3.0 [Reserved] Vegetable, cucurbit, group 9 ...... 0.70 Vegetable, foliage of legume, except soybean, (c) Tolerances with regional registra- group 7A ...... 40 tions. [Reserved] Vegetable, fruiting, group 8–10 ...... 2.0 (d) Indirect or inadvertent residues. Vegetable, leaves of root and tuber, group 2 ...... 40 Vegetable, legume, dried shelled, except soy- [Reserved] bean, subgroup 6C ...... 1.0 Vegetable, legume, edible podded, subgroup 6A 2.0 [78 FR 32151, May 29, 2013. Redesignated at 78 Vegetable, legume, succulent shelled, subgroup FR 36677, June 19, 2013] 6B ...... 0.20 Vegetable, root, except sugar beet, subgroup 1B 0.40 § 180.674 Proquinazid; tolerances for Vegetable, tuberous and corm, subgroup 1C ...... 0.15 residues. 1 There are no U.S. registrations for these commodities. (a) General. Tolerances are estab- (b) Section 18 emergency exemptions. lished for residues of the fungicide, [Reserved] proquinazid, including its metabolites (c) Tolerances with regional registra- and degradates, in or on the commod- tions. [Reserved] ities listed in the following table. Com- (d) Indirect or inadvertant residues. pliance with the tolerance levels speci- Tolerances are established for indirect fied in the following table is to be de- or inadvertant tolerances for residues termined by measuring only of cyantraniliprole, 3-bromo-1-(3- proquinazid, [6-Iodo-2-propoxy-3- chloro-2-pyridinyl)-N-[4-cyano-2-meth- propyl-3H-quinazolin-4-one), in or on yl-6-[((methylamino)carbonyl]phenyl]- the following commodities: 1H-pyrazole-5-carboxamide, including its metabolites and degradates, in or Commodity Parts per on commodities in the following table. million Compliance with the tolerance levels Grape 1 ...... 0.50 specified in the following table is to be Grape, raisin 1 ...... 1.0 determined by measuring only 1 No U.S. registrations for Proquinazid. cyantraniliprole in or on the commodity. (b) Section 18 emergency exemptions. [Reserved] Parts per (c) Tolerances with regional registra- Commodity million tions. [Reserved] Animal feed, nongrass, group 18 ...... 0.20 (d) Indirect or inadvertent residues. Beet, sugar, roots ...... 0.02 Grain, cereal, forage, fodder and straw, group 16 0.50 [Reserved] Grass forage, fodder and hay, group 17 ...... 0.50 [79 FR 18815, Apr. 4, 2014]

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§ 180.675 Tolfenpyrad; tolerances for methyl]phenoxy]-benzoic acid, cal- residues. culated as the stoichiometric equiva- (a) General. (1) Tolerances are estab- lent of tolfenpyrad. lished for residues of the insecticide Parts per tolfenpyrad, including its metabolites Commodity million and degradates, in or on the commodities in the table below. Compliance Cattle, fat ...... 0.01 Cattle, meat ...... 0.01 with the tolerance levels specified Cattle, meat byproducts ...... 0.35 below is to be determined by measuring Goat, fat ...... 0.01 only tolfenpyrad (4-chloro-3-ethyl-1- Goat, meat ...... 0.01 methyl-N-[[4-(4- Goat, meat byproducts ...... 0.35 Horse, fat ...... 0.01 methylphenoxy)phenyl]methyl]-1H- Horse, meat ...... 0.01 pyrazole-5-carboxamide) in or on the Horse, meat byproducts ...... 0.35 commodity. Milk ...... 0.03 Sheep, fat ...... 0.01 Commodity Parts per Sheep, meat ...... 0.01 million Sheep, meat byproducts ...... 0.35 Almond hulls ...... 6.0 Apple, wet pomace ...... 3.0 (b) Section 18 emergency exemptions. Avocado ...... 1.5 [Reserved] Berry, low growing, subgroup 13–07G, except (c) Tolerances with regional registra- cranberry and lowbush blueberry ...... 3.0 Brassica, leafy greens, subgroup 4–16B ...... 40 tion. [Reserved] Bushberry, subgroup 13–07B ...... 7.0 (d) Indirect or inadvertent residues. Caneberry, subgroup 13–07A ...... 7.0 Celtuce ...... 30 [Reserved] 1 Citrus, dried pulp ...... 8.0 [79 FR 1605, Jan. 9, 2014, as amended at 81 FR Citrus, dried pulp ...... 4.0 Citrus, oil 1 ...... 70.0 68944, Oct. 5, 2016; 82 FR 46934, Oct. 10, 2017; 83 Citrus, oil ...... 30 FR 29023, June 22, 2018; 83 FR 65550, Dec. 21, Cotton, gin byproducts ...... 15.0 2018] Cottonseed, subgroup 20C ...... 0.70 Fennel, Florence, fresh leaves and stalk ...... 30 § 180.676 Fenpropidin; tolerances for Fruit, citrus, group 10–10 1 ...... 1.5 Fruit, citrus, group 10–10 ...... 0.80 residues. Fruit, pome, group 11–10 ...... 1.0 (a) General. Tolerances are estab- Fruit, small, vine climbing, except fuzzy kiwifruit, subgroup 13–07F ...... 2.0 lished for the residues of fenpropidin, Fruit, stone, group 12–12 ...... 2.0 including its metabolites and Grape, raisin ...... 6.0 degradates, in or on the commodities Leaf petiole vegetable subgroup 22B ...... 30 Leafy greens, subgroup 4–16A ...... 30 in the table below. Compliance with Nuts, tree, group 14–12 ...... 0.05 the tolerance levels specified below is Onion, bulb, subgroup 3–07A ...... 0.09 to be determined by measuring only Onion, green, subgroup 3–07B ...... 10 Persimmon ...... 2.0 fenpropidin (1-[3-[4-(1,1- Plum, prune ...... 3.0 dimethylethyl)phenyl]-2- Pomegranate ...... 2.0 methylpropyl]piperidine). Tea ...... 30.0 Vegetable, Brassica, head and stem, group 5–16 5.0 Parts per Vegetable, cucurbit, group 9 ...... 0.70 Commodity million Vegetable, fruiting, group 8–10 ...... 1.5 Vegetable, tuberous and corm, subgroup 1C ...... 0.01 Banana 1 ...... 10 1 This tolerance expires on December 24, 2018. 1 There are no U.S. registrations as of December 13, 2013. (2) Tolerances are established for res- (b) Section 18 tolerance. [Reserved] idues of the insecticide tolfenpyrad, in- (c) Tolerances with regional registra- cluding its metabolites and degradates, tions. [Reserved] in or on the commodities in the fol- (d) Indirect or inadvertent residues. lowing table. Compliance with the tol- [Reserved] erance levels specified below is to be determined by measuring only the sum [79 FR 8096, Feb. 11, 2014] of tolfenpyrad, 4-chloro-3-ethyl-1-methyl-N-[[4-(4- § 180.677 Cyflumetofen; tolerances for methylphenoxy)phenyl]methyl]-1H- residues. pyrazole-5-carboxamide, and its me- (a) General. Tolerances are estab- tabolite 4-[4-[(4-chloro-3-ethyl-1- lished for residues of the insecticide methylpyrazol-5-yl)carbonylamino- cyflumetofen, including its metabolites

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and degradates, in or on the commod- (d) Indirect or inadvertent residues. ities in the table below. Compliance [Reserved] with the tolerance levels for [79 FR 33468, June 11, 2014] cyflumetofen is to be determined by measuring only cyflumetofen, 2- § 180.679 Flupyradifurone; tolerances methoxyethyl a-cyano-a-[4-(1,1- for residues. dimethylethyl)phenyl]-b-oxo-2- (a) General. Tolerances are estab- (trifluoromethyl)benzenepropanoate, in lished for residues of the insecticide or on the commodity. flupyradifurone, including its metabo- Parts per lites and degradates, in or on the com- Commodity million modities in the following table. Com- Almond, hulls ...... 4.0 pliance with the tolerance levels speci- Cherry subgroup 12–12A ...... 1.5 fied in the following table is to be de- Citrus, oil ...... 16 termined by measuring only Coffee, green bean 2 ...... 0.08 flupyradifurone, 4-[[(6-chloro-3- Cucumber ...... 0.3 Fruit, citrus, group 10–10 ...... 0.30 pyridinyl)methyl](2,2- Fruit, pome, group 11–10 ...... 0.30 difluoroethyl)amino]- 2(5H)-furanone. Grape ...... 0.60 Nut, tree, group 14–12 ...... 0.01 Parts per Peach subgroup 12–12B ...... 0.4 Commodity million Pepper/eggplant subgroup 8–10B ...... 2 Plum subgroup 12–12C ...... 0.3 Alfalfa, forage ...... 9.0 Strawberry ...... 0.6 Alfalfa, hay ...... 20 Tea, dried 1 ...... 40 Almond, hulls ...... 15 Tomato subgroup 8–10A ...... 0.7 Bean, succulent ...... 0.20 Berry, low growing, except cranberry subgroup 1 There are no U.S. registrations for this commodity as of 13–07G ...... 1.5 May 8, 2019. 2 There are no U.S. registrations for these commodities as Brassica, head and stem subgroup 5A ...... 6.0 of November 25, 2019. Brassica, leafy greens subgroup 5B ...... 40 Bushberry, except cranberry subgroup 13–07B ... 4.0 (b) Section 18 emergency exemptions. Cactus, fruit ...... 0.30 [Reserved] Cactus, pads ...... 0.70 Caneberry subgroup 13–07A ...... 5.0 (c) Tolerances with regional registra- Cattle, fat ...... 0.20 tions. [Reserved] Cattle, meat ...... 0.30 (d) Indirect or inadvertent residues. Cattle, meat byproducts ...... 1.0 [Reserved] Cilantro, fresh leaves ...... 30 Coffee, green bean 1 ...... 1.5 [79 FR 29108, May 21, 2014, as amended at 84 Corn, field, grain ...... 0.05 Corn, pop, grain ...... 0.05 FR 20042, May 8, 2019; 84 FR 64779, Nov. 25, Corn, sweet, kernels plus cobs with husks re- 2019; 85 FR 39494, July 1, 2020] moved ...... 0.05 Cotton, gin byproducts ...... 40 § 180.678 Tricyclazole; tolerances for Cottonseed, subgroup 20C ...... 0.80 residues. Egg ...... 0.01 Fruit, citrus, dried pulp ...... 10 (a) General. (1) Tolerances are estab- Fruit, citrus, group 10–10 ...... 3.0 lished for residues of the fungicide Fruit, pome, group 11–10 ...... 0.70 tricyclazole, including its metabolites Fruit, small vine climbing, except fuzzy kiwifruit, subgroup 13–07F ...... 3.0 and degradates, in or on the commod- Fruit, stone, group 12–12 ...... 1.5 ities in the table below. Compliance Goat, fat ...... 0.20 with the tolerance levels specified Goat, meat ...... 0.30 Goat, meat byproducts ...... 1.0 below is to be determined by measuring Grain, aspirated grain fractions ...... 40 only tricyclazole (5-methyl-1,2,4- Grain, cereal, forage, fodder and straw, group 16 30 triazolo[3,4-b ]benzothiazole). Grain, cereal, group 15, except rice and corn ...... 3.0 Grape, raisin ...... 5.0 Parts Hog, fat ...... 0.01 Commodity per mil- Hog, meat ...... 0.01 lion Hog, meat byproducts ...... 0.04 Hops, dried cones ...... 10 Rice, grain 1 ...... 3.0 Horse, fat ...... 0.20 1 There are no U.S. Registrations on Rice as of June 11, Horse, meat ...... 0.30 2014. Horse, meat byproducts ...... 1.0 Kava, fresh leaves ...... 40 (b) Section 18 emergency exemptions. Kava, roots ...... 0.90 [Reserved] Leaf petioles, subgroup 4B ...... 9.0 Leafy greens, subgroup 4A ...... 30 (c) Tolerances with regional registra- Milk ...... 0.15 tions. [Reserved] Nut, tree, group 14–12 ...... 0.02

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pyridinyl)methyl](2,2- Commodity Parts per million difluoroethyl)amino]- 2(5H)-furanone. Onion, bulb, subgroup 3–07A ...... 0.09 Parts per Onion, green, subgroup 3–07B ...... 3.0 Commodity million Pea and bean, dried, shelled except soybean, subgroup 6C ...... 3.0 Clover, forage ...... 20 Pea, succulent ...... 2.0 Clover, hay ...... 30 Peanut ...... 0.04 Peanut, hay ...... 20 (d) Indirect or inadvertent residues. Pitaya ...... 0.30 Quinoa, grain ...... 3.0 [Reserved] Sheep, fat ...... 0.20 Sheep, meat ...... 0.30 [80 FR 3487, Jan. 23, 2015, as amended at 81 Sheep, meat byproducts ...... 1.0 FR 65557, Sept. 23, 2016; 82 FR 13256, Mar. 10, Soybean, seed ...... 1.5 2017; 85 FR 5578, Jan. 31, 2020] Taro leaves ...... 30 Tropical and subtropical, medium to large fruit, § 180.680 Fluensulfone; tolerances for smooth, inedible peel subgroup 24B ...... 0.60 residues. Turnip greens ...... 40 Vegetable, cucurbit, group 9 ...... 0.40 (a) General. Tolerances are estab- Vegetable, foliage of legume, group 7 ...... 30 lished for residues of the nematicide Vegetable, fruiting, group 8–10 ...... 1.5 fluensulfone, including its metabolites Vegetable, legume, edible podded, subgroup 6A 3.0 Vegetable, root, except sugar beet, subgroup 1B 0.90 and degradates, in or on the commod- Vegetable, tuberous and corm, subgroup 1C ...... 0.05 ities in the table 1 to § 180.680. Compli- 1 No U.S. registration. ance with the tolerance levels specified in the following table below is to be de- (b) Section 18 emergency exemptions. termined by measuring only the sum of Time-limited tolerances are estab- fluensulfone, 5-chloro-2-[(3,4,4- lished for residues of flupyradifurone, trifluoro-3-buten-1-yl)sulfonyl]thiazole including its metabolites and and its metabolite, 3,4,4-trifluoro-but-3- degradates in or on the specified com- ene-1-sulfonic acid, calculated as the modities listed in table 2 to this para- stoichiometric equivalent of graph (b), resulting from use of the pes- fluensulfone, in or on the commodity. ticide under section 18 emergency exemptions granted by EPA. The time- TABLE 1 TO § 180.680 limited tolerances expire and are re- Parts per voked on the date specified in table 2 Commodity million to this paragraph (b). Compliance with the tolerance levels specified in table 2 Almond, hulls ...... 5 Berry, low growing, subgroup 13–07G ...... 0.5 to this paragraph (b) is to be deter- Brassica, head and stem, subgroup 5A ...... 1.5 mined by measuring only Brassica, leafy greens, subgroup 5B ...... 20 flupyradifurone, 4-[[(6-chloro-3- Fruit, citrus, group 10–10 ...... 0.3 Fruit, citrus, group 10–10, dried pulp ...... 0.9 pyridinyl)methyl](2,2- Fruit, citrus, group 10–10, oil ...... 15 difluoroethyl)amino]-2(5H)-furanone in Fruit, pome, group 11–10 ...... 0.4 or on the commodity. Fruit, small, vine climbing, subgroup 13–07D ...... 0.8 Fruit, stone, group 12–12 ...... 0.15 Grape, raisin ...... 1.5 TABLE 2 TO PARAGRAPH (b) Nut, tree, group 14–12 ...... 0.02 Potato, chips ...... 2 Parts per Expiration/ Potato, granules/flakes ...... 2 Commodity million revocation Sugarcane, cane ...... 0.06 date Sugarcane, molasses ...... 0.3 Tomato, paste ...... 1.5 Sorghum, syrup ...... 90.0 12/31/22 Vegetables, cucurbits, group 9 ...... 0.7 Sweet sorghum, forage ...... 30.0 12/31/22 Vegetables, fruiting, group 8–10 ...... 0.7 Vegetables, leafy, except Brassica, group 4 ...... 4 (c) Tolerances with regional restric- Vegetables, leaves of root and tuber, group 2, tions. Tolerances are established for except sugar beet ...... 50 Vegetables, root, except sugar beet, subgroup 1B 4 residues of the insecticide Vegetables, tuberous and corm, subgroup 1C ..... 0.8 flupyradifurone, including its metabolites and degradates, in or on the com- (b) Section 18 emergency exemptions. modities in the following table. Com- [Reserved] pliance with the tolerance levels speci- (c) Tolerances with regional registra- fied in the following table is to be de- tions. [Reserved] termined by measuring only (d) Indirect or inadvertent residues. flupyradifurone, 4-[[(6-chloro-3- Tolerances are established for residues

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of the nematicide fluensulfone, includ- Commodity Parts per ing its metabolites and degradates, in million or on the commodities in table 2 to Fruit, small vine climbing, except fuzzy kiwifruit, § 180.680. Compliance with the tolerance subgroup 13–07F ...... 3.0 levels specified in the following table Fruit, small vine climbing, except grape, subgroup 13–07E ...... 10.0 below is to be determined by measuring Grape, raisin ...... 5.0 only the sum of fluensulfone, 5-chloro- Lettuce, head ...... 5.0 2-[(3,4,4-trifluoro-3-buten-1- Lettuce, leaf ...... 7.0 Mustard, seed, oil ...... 0.03 yl)sulfonyl]thiazole and its metabolite, Pea and bean, dried shelled, except soybean, 3,4,4-trifluoro-but-3-ene-1-sulfonic acid, subgroup 6C ...... 0.040 calculated as the stoichiometric equiv- Pea and bean, succulent shelled, subgroup 6B ... 0.030 Peach subgroup 12–12B ...... 3.0 alent of fluensulfone, in or on the com- Plum, Prune, Dried ...... 1.50 modity. Plum subgroup 12–12C ...... 0.80 Rapeseed subgroup 20A ...... 0.015 TABLE 2 TO § 180.680 Sesame, oil ...... 0.03 Vegetable, legume, edible podded, subgroup 6A 1.50 Commodity Parts per million (b) Section 18 emergency exemptions. Barley, bran ...... 0.15 [Reserved] Barley, grain ...... 0.1 (c) Tolerances with regional registra- Barley, hay ...... 15 tions. [Reserved] Barley, straw ...... 6 Buckwheat, grain ...... 0.1 (d) Indirect or inadvertent residues. Grain, cereal, forage, fodder and straw, group 16 3 [Reserved] Grain, cereal, group 15 ...... 0.05 Oat, forage ...... 6 [80 FR 45443, July 30, 2015, as amended at 81 Oat, grain ...... 0.1 FR 70974, Oct. 14, 2016; 82 FR 27154, June 14, Oat, hay ...... 15 2017] Oat, straw ...... 6 Wheat, bran ...... 0.15 § 180.682 Bicyclopyrone; tolerances for Wheat, forage ...... 6 Wheat, germ ...... 0.1 residues. Wheat, grain ...... 0.1 (a) General. (1) Tolerances are estab- Wheat, hay ...... 15 Wheat, milled byproducts ...... 0.15 lished for residues of the herbicide Wheat, straw ...... 6 bicyclopyrone (4-hydroxy-3-[[2-[(2- methoxyethoxy)methyl]-6- [84 FR 24047, May 24, 2019] (trifluoromethyl)-3- pyridinyl]carbonyl]bicyclo[3.2.1]oct-3- § 180.681 Isofetamid; tolerances for en-2-one), including its metabolites and residues. degradates, in or on the commodities (a) General. Tolerances are estab- in the table below. Compliance with lished for residues of the fungicide the tolerance levels specified below is isofetamid, including its metabolites to be determined by measuring only and degradates, in or on the commod- the sum of the common moieties ities in the table below. Compliance SYN503780 (2-[(2- with the tolerance levels specified methoxyethoxy)methyl]-6- below is to be determined by measuring (trifluoromethyl)-3-pyridinecarboxylic only isofetamid, N-[1,1-dimethyl-2-[2- acid) and CSCD686480 (2-[(2- methyl-4-(1-methylethoxy)phenyl]-2- hydroxyethoxy)methyl]-6- oxoethyl]-3-methyl-2- (trifluoromethyl)-3-pyridinecarboxylic thiophenecarboxamide, in or on the fol- acid), calculated as the stoichiometric lowing commodities: equivalent of bicyclopyrone, in or on the commodities. Commodity Parts per million Parts per Commodity million Almond ...... 0.01 Almond, hulls ...... 0.01 Barley, bran ...... 0.15 Apple, wet pomace ...... 2.0 Barley, grain ...... 0.07 Berry, low growing, subgroup 13–07G ...... 4.0 Barley, hay ...... 0.30 Bushberry subgroup 13–07B ...... 5.0 Barley, straw ...... 0.40 Caneberry subgroup 13–07A ...... 4.0 Cattle, meat byproducts ...... 2.0 Canola, refined oil ...... 0.03 Corn, field, forage ...... 0.30 Cherry subgroup 12–12A ...... 4.0 Corn, field, grain ...... 0.02 Flax, seed, oil ...... 0.03 Corn, field, stover ...... 0.40 Fruit, pome, group 11–10 ...... 0.60 Corn, pop, grain ...... 0.02

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difluorophenyl)-4,5-dihydro-3- Commodity Parts per million isoxazolyl]-2-thiazolyl]-1-piperidinyl]-2- Corn, pop, stover ...... 0.40 [5-methyl-3-(trifluoromethyl)-1H- Corn, sweet, forage ...... 0.40 pyrazol-1-yl]-ethanone, in or on the Corn, sweet, kernel plus cob with husks removed 0.03 commodity. Corn, sweet, stover ...... 0.70 Goat, meat byproducts ...... 2.0 Parts per Grain, aspirated fractions ...... 0.30 Commodity million Hog, meat byproducts ...... 0.40 Horse, meat byproducts ...... 2.0 Basil, dried leaves ...... 80 Sheep, meat byproducts ...... 2.0 Basil, fresh leaves ...... 10 Sugarcane, cane 1 ...... 0.02 Wheat, bran ...... 0.07 Brassica leafy greens subgroup 4–16B ...... 10 Wheat, forage ...... 0.40 Cacao bean, dried bean ...... 0 .15 Wheat, grain ...... 0.04 Caneberry subgroup 13–07A ...... 0.50 Wheat, hay ...... 0.80 Citrus, dried pulp ...... 0 .09 Wheat, straw ...... 0.50 Citrus, oil ...... 2.0 Fruit, citrus, group 10–10 ...... 0 .06 1 There are no U.S. Registration on Sugarcane as of March 13, 2015. Ginseng ...... 0 .15 Grape 1 ...... 0 .70 (2) [Reserved] Leafy greens subgroup 4–16A ...... 15 (b) [Reserved] Onion, bulb, subgroup 3–07A ...... 0 .04 Onion, green, subgroup 3–07B ...... 2 .0 [80 FR 22654, Apr. 23, 2015, as amended at 81 Pea, edible-podded ...... 1 .0 FR 86965, Dec. 2, 2016] Pea, succulent shelled ...... 0 .05 Potato, wet peel ...... 0 .07 § 180.684 Benalaxyl-M; tolerances for Soybean, seed ...... 0 .01 residues. Stalk and stem vegetable subgroup 22A ...... 2 .0 Sunflower, seed ...... 0.01 (a) General. Tolerances are estab- Tomato, dried ...... 3 .0 lished for residues of the fungicide Vegetable, Brassica head and stem, group 5– benalaxyl-M, including its metabolites 16 ...... 1 .5 and degradates, in or on the commod- Vegetable, cucurbit, group 9 ...... 0.20 Vegetable, fruiting, group 8–10 ...... 0 .50 ities in the table below. Compliance Vegetable, tuberous and corm, subgroup 1C ... 0.04 with the tolerance levels specified 1 There is no associated U.S. registration as of September below is to be determined by measuring 4, 2015. only benalaxyl [methyl N-(2,6- dimethylphenyl)-N-(phenylacetyl)-DL- (b) Section 18 emergency exemptions. alaninate] in or on the commodity. [Reserved] (c) Tolerances with regional registra- Parts per tions. [Reserved] Commodity million (d) Indirect or inadvertent residues. Grape 1 ...... 3 .0 Tolerances are established for residues Tomato 1 ...... 0.20 of the fungicide oxathiapiprolin, in- 1 There is no U.S. registration for use on this commodity as cluding its metabolites and degradates, of July 30, 2015. in or on the commodities in the table (b) Section 18 emergency exemptions. below. Compliance with the tolerance [Reserved] levels specified below is to be deter- (c) Tolerances with regional registra- mined by measuring only tions. [Reserved] oxathiapiprolin, 1-[4-[4-[5-(2,6- (d) Indirect or inadvertent residues. difluorophenyl)-4,5-dihydro-3- [Reserved] isoxazolyl]-2-thiazolyl]-1-piperidinyl]-2- [5-methyl-3-(trifluoromethyl)-1H- [80 FR 45448, July 30, 2015] pyrazol-1-yl]-ethanone, in or on the § 180.685 Oxathiapiprolin; tolerances commodity. for residues. Parts per (a) General. Tolerances are estab- Commodity million lished for residues of the fungicide All other food commodities/feed commodities oxathiapiprolin, including its metabo- (other than those covered by a tolerance as a lites and degradates, in or on the com- result of use on growing crops) ...... 0.10 modities in the table below. Compli- ance with the tolerance levels specified [80 FR 53473, Sept. 4, 2015, as amended at 81 below is to be determined by measuring FR 87467, Dec. 5, 2016; 82 FR 44945, Sept. 27, only oxathiapiprolin, 1-[4-[4-[5-(2,6- 2017]

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§ 180.686 Benzovindiflupyr; tolerances Commodity Parts per for residues. million (a) General. Tolerances are estab- Pea, field, hay ...... 7.0 lished for residues of the fungicide Pea, field, vine ...... 1 .5 Peanut ...... 0 .01 benzovindiflupyr, including its metabo- Peanut, hay ...... 15.0 lites and degradates, in or on the com- Potato, processed potato waste ...... 0 .10 modities in the table below. Compli- Rapeseed, subgroup 20A ...... 0.15 Rye, grain ...... 0.1 ance with the tolerance levels specified Rye, hay ...... 15 .0 below is to be determined by measuring Rye, straw ...... 15 .0 only benzovindiflupyr (N-[9- Ryegrass, forage ...... 0 .15 Ryegrass, hay ...... 7 .0 (dichloromethylene)-1,2,3,4-tetrahydro- Ryegrass, straw ...... 6 .0 1,4-methanonaphthalen-5-yl]-3- Sheep, fat ...... 0 .02 (difluoromethyl)-1-methyl-1H-pyrazole- Sheep, liver ...... 0.06 4-carboxamide) in or on the com- Sheep, meat ...... 0.01 Sheep meat byproducts, except liver ...... 0 .01 modity. Soybean, forage ...... 15 .0 Soybean, hay ...... 50 .0 Commodity Parts per Soybean, hulls ...... 0 .20 million Soybean, seed ...... 0 .07 Sugarcane, cane ...... 0.30 Barley, grain ...... 1 .5 Tomato, dried ...... 4 .0 Barley, hay ...... 15 .0 Vegetable, cucurbit, group 9 ...... 0.30 Barley, straw ...... 15 .0 Vegetable, fruiting, group 8–10 ...... 1 .5 Bluegrass, forage ...... 0.15 Vegetable, tuberous and corm, subgroup 1C ... 0.02 Bluegrass, hay ...... 7 .0 Wheat, forage ...... 4 .0 Bluegrass, straw ...... 6 .0 Wheat, grain ...... 0 .10 Bromegrass, forage ...... 0 .15 Wheat, hay ...... 15 .0 Bromegrass, hay ...... 7 .0 Wheat, straw ...... 15 .0 Bromegrass, straw ...... 6 .0 Cattle, fat ...... 0.02 Cattle, liver ...... 0 .06 (b) Section 18 emergency exemptions. Cattle, meat ...... 0 .01 [Reserved] Cattle, meat byproducts, except liver ...... 0 .01 (c) Tolerances with regional registra- Coffee, green bean1 ...... 0 .09 Corn, field, forage ...... 3 .0 tions. [Reserved] Corn, field, grain ...... 0 .02 (d) Indirect or inadvertent residues. Corn, field, stover ...... 15 .0 [Reserved] Corn, pop, grain ...... 0.02 Corn, pop, stover ...... 15.0 [80 FR 59633, Oct. 2, 2015, as amended at 82 FR Corn, sweet, forage ...... 4 .0 52674, Nov. 14, 2017; 83 FR 29038, June 22, 2018] Corn, sweet, kernel plus cob with husks removed ...... 0 .01 Corn, sweet, stover ...... 5 .0 § 180.687 Teflubenzuron; tolerances for Cottonseed, subgroup 20C ...... 0 .15 residues. Cotton, gin byproducts ...... 3 .0 (a) General. (1) Tolerances are estab- Fescue, forage ...... 0.15 Fescue, hay ...... 7.0 lished for residues of the insecticide Fescue, straw ...... 6 .0 teflubenzuron, including its metabo- Fruit, pome, group 11–10 ...... 0 .20 lites and degradates, in or on the com- Fruit, small vine climbing, except fuzzy kiwifruit, subgroup 13–07F ...... 1.0 modities in the table below. Compli- Goat, fat ...... 0 .02 ance with the tolerance levels specified Goat, liver ...... 0.06 below is to be determined by measuring Goat, meat ...... 0.01 Goat, meat byproducts, except liver ...... 0 .01 only teflubenzuron (N-[[(3,5-dichloro- Grain, aspirated fractions ...... 15.0 2,4-difluorophenyl)amino]carbonyl]-2,6- Grape, raisin ...... 3 .0 difluorobenzamide). Horse, fat ...... 0 .02 Horse, liver ...... 0 .06 Parts per Horse, meat ...... 0 .01 Commodity million Horse, meat byproducts, except liver ...... 0 .01 Milk ...... 0.01 Apple 1 ...... 1.0 Milk, fat ...... 0 .02 Broccoli 1 ...... 0 .20 Oat, grain ...... 1 .5 Cauliflower 1 ...... 0 .01 Oat, hay ...... 15.0 Citrus, oil 1 ...... 100 Oat, straw ...... 15.0 Coffee, bean, green 1 ...... 0 .60 Onion, bulb, subgroup 3–07A ...... 0 .02 Corn, field, grain 1 ...... 0 .01 Onion, green, subgroup 3–07B ...... 0 .40 Corn, field, refined oil 1 ...... 0 .02 Orchardgrass, forage ...... 0 .15 Lemon 1 ...... 0.80 Orchardgrass, hay ...... 7 .0 Mango 1 ...... 1.5 Orchardgrass, straw ...... 6 .0 Melon, subgroup 9A 1 ...... 0 .30 Pea and bean, dried shelled, except soybean, Orange 1 ...... 0 .60 subgroup 6C ...... 0 .20 Papaya 1 ...... 0 .50

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the stoichiometric equivalent of Commodity Parts per million aminocyclopyrachlor. Pineapple 1 ...... 0.80 1 Parts per Soybean, seed ...... 0 .05 Commodity million Soybean, hulls 1 ...... 0 .15 Sugarcane, cane 1 ...... 0.01 Cattle, fat 1 ...... 0.05 Sunflower, seed 1 ...... 0.30 Cattle, meat 1 ...... 0 .01 Tomato 1 ...... 1.5 Cattle, meat byproducts 1 ...... 0.30 Goat, fat 1 ...... 0 .05 1 There are no U.S. registrations as of October 30, 2015. Goat, meat 1 ...... 0.01 (b) Section 18 emergency exemptions. Goat, meat byproducts 1 ...... 0 .30 Horse, fat 1 ...... 0 .05 [Reserved] Horse, meat 1 ...... 0 .01 (c) Tolerances with regional registra- Horse, meat byproducts 1 ...... 0 .30 tions. [Reserved] Milk 1 ...... 0.01 Sheep, fat 1 ...... 0 .05 (d) Indirect or inadvertent residues. Sheep, meat 1 ...... 0.01 [Reserved] Sheep, meat byproducts 1 ...... 0 .30 [80 FR 66809, Oct. 30, 2015] 1 There are no U.S. registrations as of August 11, 2016. (b) Section 18 emergency exemptions. § 180.688 Diethofencarb; tolerance for [Reserved] residue. (c) Tolerances with regional registra- (a) General. (1) Tolerances are estab- tions. [Reserved] lished for residues of the fungicide (d) Indirect or inadvertent residues. diethofencarb, including its metabo- [Reserved] lites and degradates, in or on the commodities in the table below. Compli- [81 FR 53018, Aug. 11, 2016] ance with the tolerance levels specified § 180.690 Mandestrobin; tolerances for below is to be determined by measuring residues. only diethofencarb (1-methylethyl N- (a) General. Tolerances are estab- (3,4-diethoxyphenyl)carbamate). lished for residues of mandestrobin, including its metabolites and degradates, Commodity Parts per million in or on the commodities in the table Banana * ...... 0 .10 below. Compliance with the tolerance levels specified below is to be deter- * There is no U.S. registration for use on this commodity as of November 4, 2015. mined by measuring only mandestrobin, 2-[(2,5- (b) Section 18 emergency exemptions. dimethylphenoxy)methyl]-a-methoxy- [Reserved] N-methylbenzeneacetamide. (c) Tolerances with regional registrations. [Reserved] Commodity Parts per (d) Indirect or inadvertent residues [Re- million served] Berry, low growing, subgroup 13–07G, except cranberry ...... 3.0 [80 FR 68261, Nov. 4, 2015] Fruit, small vine climbing, except fuzzy kiwifruit, subgroup 13–07F ...... 5.0 § 180.689 Aminocyclopyrachlor; toler- Grape, raisin ...... 7 .0 ances for residues. (a) General. Tolerances are estab- (b) Section 18 emergency exemptions. lished for residues of the herbicide [Reserved] aminocyclopyrachlor, including its me- (c) Tolerances with regional registra- tabolites and degradates, in or on the tions. [Reserved] commodities in the table below. Com- (d) Indirect or inadvertent tolerances. pliance with the tolerance levels speci- [Reserved] fied below is to be determined by meas- [81 FR 70043, Oct. 11, 2016] uring only the sum of aminocyclopyrachlor, 6-amino-5- § 180.691 Halauxifen-methyl; toler- chloro-2-cyclopropyl-4- ances for residues. pyrimidinecarboxylic acid, and (a) General. Tolerances are estab- aminocyclopyrachlor methyl ester, lished for residues of the herbicide, methyl 6-amino-5-chloro-2-cyclopropyl- halauxifen-methyl, including its me- 4-pyrimidinecarboxylate, calculated as tabolites and degradates, in or on the

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commodities in the table below. Com- § 180.693 Benzobicyclon; tolerances for pliance with the tolerance levels speci- residues. fied below is to be determined by meas- (a) General. [Reserved] uring only halauxifen-methyl (methyl (b) Section 18 emergency exemptions. (4-amino-3-chloro-6-(4-chloro-2-fluoro-3- [Reserved] methoxyphenyl)-2-pyridine (c) Tolerances with regional registra- carboxylate). tions. Tolerances with regional registration, as defined in § 180.1(l), are es- Parts per Commodity million tablished for residues of the herbicide benzobicyclon, including its metabo- Barley, grain ...... 0 .01 lites and degradates, in or on the com- Barley, hay ...... 0 .01 modity in the table below. Compliance Barley, straw ...... 0 .01 with the tolerance levels specified Wheat, forage ...... 0 .50 Wheat, grain ...... 0 .01 below is to be determined by measuring Wheat, hay ...... 0 .03 only benzobicyclon, 3-[2-chloro-4- Wheat, straw ...... 0 .015 (methylsulfonyl)benzoyl]-4- (phenylthio)bicyclo-[3.2.1]oct-3-en-2- (b) Section 18 emergency exemptions. one), in or on the following raw agri- [Reserved] cultural commodities: (c) Tolerances with regional registra- Parts per tions. [Reserved] Commodity million (d) Indirect or inadvertent residues. Rice, grain ...... 0 .01 [Reserved] [81 FR 53025, Aug. 11, 2016] (d) Indirect or inadvertent residues. [Reserved] § 180.692 Tioxazafen; tolerances for [82 FR 19001, Apr. 25, 2017] residues. (a) General. Tolerances are estab- § 180.694 Cyclaniliprole; tolerances for lished for residues of tioxazafen, in- residues. cluding its metabolites and degradates, (a) General. Tolerances are estab- in or on the commodities in the table lished for residues of the insecticide below. Compliance with the tolerance cyclaniliprole, including its metabo- levels specified below is to be deter- lites and degradates, in or on the com- mined by measuring the combined resi- modities in the table below. Compli- dues of tioxazafen [3-phenyl-5-(2- ance with the tolerance levels specified thienyl)-1,2,4-oxadiazole] and below is to be determined by measuring benzamidine, expressed as tioxazafen in only cyclaniliprole, 3-bromo-N-[2- or on the commodity. bromo-4-chloro-6-[[(1- cyclopropylethyl)amino]car- Commodity Parts bonyl]phenyl]-1-(3-chloro-2-pyridinyl)- per million 1H-pyrazole-5-carboxamide, in or on Corn, field, forage ...... 0 .02 the commodity. Corn, field, grain ...... 0 .02 Corn, field, stover ...... 0 .02 Parts Commodity per million Cotton, gin by-products ...... 0 .02 Cotton, undelinted seed ...... 0 .02 Almond, hulls ...... 6 .0 Soybean, forage ...... 0 .15 Apple, wet pomace ...... 0 .50 Soybean, hay ...... 0 .30 Berry, low growing, subgroup 13–07G ...... 0 .4 Soybean, meal ...... 0.05 Bushberry subgroup 13–07B ...... 1 .5 Caneberry subgroup 13–07A ...... 0.8 Soybean, seed ...... 0 .04 Cattle, fat ...... 0.015 Cattle, meat ...... 0 .01 (b) Section 18 emergency exemptions. Cattle, meat byproducts ...... 0.015 [Reserved] Fruit, citrus, group 10–10, oil ...... 30 Fruit, pome, group 11–10 ...... 0 .30 (c) Tolerances with regional registra- Fruit, small vine climbing, except fuzzy tions. [Reserved] kiwifruit, subgroup 13–07F ...... 0.80 Fruit, small, vine climbing, except grape, sub- (d) Indirect or inadvertent residues. group 13–07E ...... 1 [Reserved] Fruit, stone, group 12–12 ...... 1 .0 Goat, fat ...... 0 .015 [82 FR 20283, May 1, 2017] Goat, meat ...... 0.01

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(d) Indirect or inadvertent residues. Commodity Parts per million [Reserved] Goat, meat byproducts ...... 0 .015 [82 FR 34882, July 27, 2017] Grapefruit subgroup 10–10C ...... 0 .2 Horse, fat ...... 0 .015 § 180.697 Flutianil; tolerances for resi- Horse, meat ...... 0 .01 dues. Horse, meat byproducts ...... 0 .015 Lemon/lime subgroup 10–10B ...... 0.3 (a) General. Tolerances are estab- Milk ...... 0.015 lished for the combined residues of the Nut, tree, group 14–12 ...... 0 .03 fungicide flutianil, including its me- Orange subgroup 10–10A ...... 0.4 tabolites and degradates in or on food Potato, wet peel ...... 0 .06 Sheep, fat ...... 0 .015 commodities in Table 1 to this para- Sheep, meat ...... 0.01 graph (a). Compliance with the toler- Sheep, meat byproducts ...... 0 .015 ance levels specified in Table 1 is to be Tea, dried 1 ...... 50 determined by measuring only Vegetable, Brassica, head and stem, group 5– flutianil, (2Z)-2-[2-fluoro-5- 16 ...... 1 .0 Vegetable, cucurbit, group 9 ...... 0.15 (trifluoromethyl)phenyl]sulfanyl-2-[3- Vegetable, fruiting, group 8–10 ...... 0 .20 (2-methoxyphenyl)thiazolidin-2- Vegetable, leafy, group 4–16 ...... 15 ylidene]acetonitrile in or on the fol- Vegetable, tuberous and corm, subgroup 1C ... 0.01 lowing commodities: 1 There are no U.S. registrations for tea. TABLE 1 TO PARAGRAPH (a) (b) Section 18 emergency exemptions. [Reserved] Parts per Commodity million (c) Tolerances with regional registrations. [Reserved] Apple ...... 0.15 Apple, wet pomace ...... 0.30 (d) Indirect or inadvertent residues. Berry, low growing, subgroup 13–07G ...... 0.5 [Reserved] Cherry subgroup 12–12A ...... 0.4 Fruit, small, vine climbing, except fuzzy kiwifruit, [82 FR 36094, Aug. 3, 2017, as amended at 84 subgroup 13–07F ...... 0.7 FR 50763, Sept. 26, 2019] Hop, dried cones ...... 2 Melon subgroup 9A ...... 0.07 § 180.696 Tolpyralate; tolerances for Squash/cucumber subgroup 9B ...... 0.2 residues. (b) Section 18 emergency exemptions. (a) General. Tolerances are estab- [Reserved] lished for residues of tolpyralate, in- (c) Tolerances with regional registra- cluding its metabolites and degradates, tions. [Reserved] in or on the commodities in the table (d) Indirect or inadvertent residues. below. Compliance with the tolerance [Reserved] levels specified below is to be deter- [83 FR 12268, Mar. 21, 2018, as amended at 84 mined by measuring only tolpyralate, FR 70026, Dec. 20, 2019] 1-[[1-ethyl-4-[3-(2-methoxyethoxy)-2- methyl-4-(methylsulfonyl)benzoyl]-1H- § 180.698 Chlormequat chloride; toler- pyrazol-5-yl]oxy]ethyl methyl car- ances for residues. bonate, in or on the commodity. (a) General. Tolerances are estab- Parts per lished for the residues of the plant reg- Commodity million ulator chlormequat chloride, including its metabolites and degradates in or on Corn, field, forage ...... 0 .01 food commodities in the table below. Corn, field, grain ...... 0 .01 Corn, field, stover ...... 0 .01 Compliance with the tolerance levels Corn, pop, grain ...... 0.01 specified below is to be determined by Corn, pop, stover ...... 0.01 measuring only chlormequat chloride Corn, sweet, forage ...... 0 .01 [(2-chloroethyl) trimethylammonium Corn, sweet, kernel plus cob with husks removed ...... 0 .01 chloride in or on the following com- Corn, sweet, stover ...... 0 .01 modities:

Parts per (b) Section 18 emergency exemptions. Commodity million [Reserved] Barley, grain 1 ...... 2 .0 (c) Tolerances with regional registra- Cattle, meat byproduct 1 ...... 0.50 tions. [Reserved] Cattle, meat 1 ...... 0 .20

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Parts per Parts per Commodity million Commodity million

Egg 1 ...... 0 .10 Cottonseed subgroup 20C ...... 0 .4 Goat, meat byproduct 1 ...... 0 .50 Fruit, citrus, group 10–10 ...... 1 Goat, meat 1 ...... 0.20 Fruit, citrus, group 10–10, oil ...... 30 Hog, meat byproduct 1 ...... 0 .50 Fruit, pome, group 11–10 ...... 0 .2 Hog, meat 1 ...... 0 .20 Fruit, small vine climbing, except fuzzy Milk 1 ...... 0.50 kiwifruit, subgroup 13–07F ...... 1.5 Oat, grain 2 ...... 40 Goat, fat ...... 0 .03 Poultry, meat byproduct 1 ...... 0.10 Goat, meat ...... 0.01 Poultry, meat 1 ...... 0 .04 Goat, meat byproducts ...... 0 .03 Sheep, meat byproduct 1 ...... 0 .50 Grain, aspirated fractions ...... 100 Sheep, meat 1 ...... 0.20 Grape, raisin ...... 2 .0 1 Wheat, grain ...... 3 .0 Horse, fat ...... 0 .03 1 There are no U.S. registrations for this commodity as of Horse, meat ...... 0 .01 April 25, 2018. Horse, meat byproducts ...... 0 .03 2 There are no U.S. registrations for this commodity. Leaf petiole vegetable subgroup 22B ...... 15 Leafy greens subgroup 4–16A ...... 40 (b) Section 18 emergency exemptions. Milk ...... 0.03 [Reserved] Nut, tree, group 14–12 ...... 0 .07 (c) Tolerances with regional registra- Oat, forage ...... 10 tions. [Reserved] Oat, grain ...... 3 .0 Oat, hay ...... 40 (d) Indirect or inadvertent residues. Oat, straw ...... 20 [Reserved] Onion, bulb, subgroup 3–07A ...... 0 .2 Onion, green, subgroup 3–07B ...... 2 [83 FR 17929, Apr. 25, 2018, as amended at 85 Pea and bean, succulent shelled, subgroup 6B 0 .1 FR 31386, May 26, 2020] Pea, field, forage ...... 6.0 Pea, field, hay ...... 40 § 180.699 Pydiflumetofen; tolerances Peach subgroup 12–12B ...... 1 for residues. Peanut ...... 0 .02 Peanut, hay ...... 30 (a) General. Tolerances are estab- Peanut, refined oil ...... 0.05 lished for residues of pydiflumetofen, Peas and bean, dried shelled, except soybean, subgroup 6C ...... 0 .40 including its metabolites and Plum, prune, dried ...... 1 degradates, in or on the commodities Plum subgroup 12–12C ...... 0 .6 in the table below. Compliance with Potato, processed potato waste ...... 0 .03 the tolerance levels specified below is Potato, wet peel ...... 0 .03 Quinoa, grain ...... 4 .0 to be determined by measuring only Rapeseed subgroup 20A ...... 0 .90 pydiflumetofen (3-(difluoromethyl)-N- Rye, grain ...... 0.30 methoxy-1-methyl-N-[1-methyl-2-(2,4,6- Rye, hay ...... 50 Rye, straw ...... 30 trichlorophenyl)ethyl]-1H-pyrazole-4- Sheep, fat ...... 0 .03 carboxamide) in or on the commodity: Sheep, meat ...... 0.01 Sheep, meat byproducts ...... 0 .03 Commodity Parts per Sorghum, grain, forage ...... 1.5 million Sorghum, grain, grain ...... 3 Sorghum, grain, stover ...... 10 Almond, hulls ...... 9 Soybean, seed ...... 0 .40 Apple, wet pomace ...... 1 Sunflower subgroup 20B ...... 0.5 Barley, grain ...... 4 .0 Tomato, dried ...... 3 .0 Barley, hay ...... 30 Vegetable, Brassica, head and stem, group 5– Barley, straw ...... 30 16 ...... 3 Berry, low growing, subgroup 13–07G ...... 1 Vegetable, cucurbit, group 9 ...... 0.50 Brassica, leafy greens, subgroup 4–16B ...... 50 Vegetable, fruiting, group 8–10 ...... 0 .60 Bushberry subgroup 13–07B ...... 5 Vegetable, leaves of root and tuber, group 2 ... 10 Cattle, fat ...... 0.03 Vegetable, legume, edible podded, subgroup Cattle, meat ...... 0 .01 6A ...... 1 Cattle, meat byproducts ...... 0.03 Vegetable, root, subgroup 1A ...... 0 .5 Cherry subgroup 12–12A ...... 2 Vegetable, tuberous and corm subgroup 1C .... 0 .015 Corn, field, flour ...... 0 .02 Wheat, forage ...... 15 Corn, field, forage ...... 6 .0 Corn, field, grain ...... 0 .015 Wheat, germ ...... 0 .40 Corn, field, milled byproducts ...... 0 .06 Wheat, grain ...... 0 .30 Corn, field, stover ...... 15 Wheat, hay ...... 50 Corn, pop, forage ...... 6 .0 Wheat, milled byproducts ...... 2 .0 Corn, pop, grain ...... 0.015 Wheat, straw ...... 30 Corn, pop, stover ...... 10 Corn, sweet, forage ...... 5 .0 (b) Section 18 emergency exemptions. Corn, sweet, kernel plus cob with husks re- [Reserved] moved ...... 0 .01 Corn, sweet, stover ...... 9 .0 (c) Tolerances with regional registra- Cotton, gin byproducts ...... 7 tions. [Reserved]

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(d) Indirect or inadvertent residues. tyl-3,4-dihydro-3-[(3- [Reserved] pyridinylmethyl)amino]-6-[1,2,2,2- tetrafluoro-1-(trifluoromethyl)ethyl]- [83 FR 24044, May 24, 2018, as amended at 84 FR 39767, Aug. 12, 2019] 2(1H)-quinazolinone) and its metabolite IV–01 (3-[(pyridin-3-ylmethyl)amino]-6- § 180.700 Afidopyropen; tolerances for [1,2,2,2-tetrafluoro-1- residues. (trifluoromethyl)ethyl]-3,4-dihydro-1H- (a) General. Tolerances are estab- quinazolin-2-one), calculated as the lished for residues of afidopyropen, in- stoichiometric equivalent of cluding its metabolites and degradates, pyrifluquinazon. in or on the commodities in the table Commodity Parts per below. Compliance with the tolerance million levels specified below is to be deter- Almond, hulls ...... 0 .60 mined by measuring only afidopyropen, Cherry subgroup 12–12A ...... 0 .30 [(3S,4R,4aR,6S,6aS,12R,12aS,12bS)-3- Citrus, dried pulp ...... 2 .0 [(cyclopropylcarbonyl)oxy]- Citrus, oil ...... 30 Cotton, gin byproducts ...... 6 .0 1,3,4,4a,5,6,6a,12,12a,12b-decahydro-6,12- Cotton, undelinted seed ...... 0 .30 dihydroxy-4,6a,12b-trimethyl-11-oxo-9- Fruit, citrus, group 10–10 ...... 0 .70 (3-pyridinyl)-2H,11H-naphtho[2,1- Fruit, pome, group 11–10 ...... 0 .07 b]pyrano[3,4-e]pyran-4-yl]methyl Fruit, small vine climbing, except fuzzy kiwifruit, subgroup 13–07F ...... 0.30 cyclopropanecarboxylate, in or on the Leaf petiole vegetable, subgroup 22B ...... 1 .5 following food commodities: Peach subgroup 12–12B ...... 0.04 Plum subgroup 12–12C ...... 0 .02 Parts per Nut, tree, group 14–12 ...... 0 .02 Commodity million Tea, dried1 ...... 20 Vegetable, brassica, head and stem, group 5– Almond, hulls ...... 0 .15 16 ...... 0 .60 Apple, wet pomace ...... 0 .05 Vegetable, cucurbit, group 9 ...... 0.07 Brassica, head and stem, group 5–16 ...... 0.50 Vegetable, fruiting, group 8–10 ...... 0 .30 Brassica, leafy greens, subgroup 4–16B ...... 5 .0 Vegetable, leafy, group 4–16 ...... 5 .0 Citrus, oil ...... 0.40 Vegetable, tuberous and corm, subgroup 1C ... 0.02 Cotton, gin byproducts ...... 2 .0 Cotton, undelinted seed ...... 0 .08 1 There are no U.S. registrations as of November 26, 2018 Fruit, citrus, group 10–10 ...... 0 .15 for use on tea. Fruit, pome, group 11–10 ...... 0 .02 (2) Tolerances are established for res- Fruit, stone, group 12–12 ...... 0 .03 Grain, aspirated fractions ...... 0 .15 idues of the insecticide Leafy Greens, subgroup 4–16A ...... 2.0 pyrifluquinazon, including its metabo- Leaf petiole vegetable subgroup 22B ...... 3 .0 lites and degradates, in or on the com- Nut, tree, group 14–12 ...... 0 .01 Soybean, seed ...... 0 .01 modities in the table below. Compli- Tomato, dried ...... 0 .50 ance with the tolerance levels specified Vegetable, cucurbit, group 9 ...... 0.70 below is to be determined by measuring Vegetable, fruiting, group 8–10 ...... 0 .20 Vegetable, tuberous and corm, subgroup 1C ... 0.01 only the sum of pyrifluquinazon (1-acetyl-3,4-dihydro-3-[(3- (b) Section 18 emergency exemptions. pyridinylmethyl)amino]-6-[1,2,2,2- [Reserved] tetrafluoro-1-(trifluoromethyl)ethyl]- (c) Tolerances with regional registra- 2(1H)-quinazolinone) and the free and tions. [Reserved] conjugated forms of its metabolites IV– (d) Indirect or inadvertent residues. 01 (3-[(pyridin-3-ylmethyl)amino]-6- [Reserved] [1,2,2,2-tetrafluoro-1- (trifluoromethyl)ethyl]-3,4-dihydro-1H- [83 FR 46401, Sept. 13, 2018] quinazolin-2-one) and IV–203 (6-[1,2,2,2- § 180.701 Pyrifluquinazon; tolerances tetrafluoro-1-trifluoromethyl)ethyl]- for residues. 1H-quinazolin-2,4-dione), calculated as the stoichiometric equivalent of (a) (1) Tolerances are estab- General. pyrifluquinazon. lished for residues of the insecticide pyrifluquinazon, including its metabo- Parts per Commodity lites and degradates, in or on the com- million modities in the table below. Compli- Cattle, liver ...... 0 .04 ance with the tolerance levels specified Goat, liver ...... 0.04 below is to be determined by measuring Horse, liver ...... 0 .04 only the sum of pyrifluquinazon (1-ace- Sheep, liver ...... 0.04

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(b) Section 18 emergency exemptions. Commodity Parts per [Reserved] million (c) Tolerances with regional registra- Goat, muscle ...... 0 .08 tions. [Reserved] Horse, fat ...... 0 .08 (d) Indirect or inadvertent residues. Horse, meat byproducts ...... 0 .40 Horse, muscle ...... 0.08 [Reserved] Milk ...... 0.04 [83 FR 60371, Nov. 26, 2018] Sheep, fat ...... 0 .08 Sheep, meat byproducts ...... 0 .40 Sheep, muscle ...... 0 .08 § 180.702 Bixafen; tolerances for residues. (b) Section 18 emergency exemptions. (a) General. (1) Tolerances are estab- [Reserved] lished for residues of the fungicide (c) Tolerances with regional registra- bixafen, including its metabolites and tions. [Reserved] degradates, in or on the commodities (d) Indirect or inadvertent residues. in the table below. Compliance with [Reserved] the tolerance levels specified below is to be determined by measuring only [83 FR 62485, Dec. 4, 2018] bixafen, N-(3,4-dichloro-5- § 180.703 6-benzyladenine; tolerances fluorobiphenyl-2-yl)-3- for residues. (difluoromethyl)-1-methylpyrazole-4- carboxamide, in or on the commodity. (a) General. Tolerances are established for residues of the plant growth Commodity Parts per regulator, 6-benzyladenine in or on the million commodities listed in the table below. Beet, sugar, dried pulp ...... 1 .0 Compliance with the tolerance levels Grain, aspirated grain fractions ...... 80 specified in this paragraph is to be de- Grain, cereal, forage, fodder, and straw, group termined by measuring only 6- 16, except rice ...... 20 Grain, cereal, group 15, except rice and grain benzyladenine in or on the commodity. sorghum ...... 0 .40 Peanut ...... 0 .01 Commodity Parts per Peanut, hay ...... 8.0 million Radish, tops ...... 3 .0 Avocado ...... 0 .02 Sorghum, grain, grain ...... 3 .0 Cucumber ...... 0 .01 Soybean, hulls ...... 0 .15 Melon ...... 0 .01 Soybean, seed ...... 0 .04 Pepper ...... 0 .01 Vegetable, root, subgroup 1A ...... 0 .30 Squash ...... 0 .01 Vegetable, tuberous and corm, subgroup 1C ... 0.01 Tomato ...... 0.01

(2) Tolerances are established for res- (b) Section 18 emergency exemptions. idues of the fungicide bixafen, includ- [Reserved] ing its metabolites and degradates, in (c) Tolerances with regional registra- or on the commodities in the table tions. [Reserved] below. Compliance with the tolerance (d) Indirect or inadvertent residues. levels specified below is to be deter- [Reserved] mined by measuring only the sum of bixafen, N-(3,4-dichloro-5- [83 FR 64030, Dec. 13, 2018] fluorobiphenyl-2-yl)-3- (difluoromethyl)-1-methylpyrazole-4- § 180.704 Sulfometuron-methyl; tolerances for residues. carboxamide, and its desmethyl metabolite, N-(3′,4′-dichloro-5-fluoro[1,1′- (a) General. (1) Tolerances are estab- biphenyl]-2-yl)-3-(difluoromethyl)-1H- lished for residues of the herbicide pyrazole-4-carboxamide, calculated as sulfometuron-methyl, including its me- the stoichiometric equivalent of tabolites and degradates, in or on the bixafen, in or on the commodity. commodity in the table below. Compli- ance with the tolerance levels specified Parts per below is to be determined by measuring Commodity million only sulfometuron-methyl, (methyl 2- Cattle, fat ...... 0.08 [[[[(4,6-dimethyl-2-pyrimidinyl)amino] Cattle, meat byproducts ...... 0.40 carbonyl]amino]sulfonyl]benzoate), in Cattle, muscle ...... 0 .08 Goat, fat ...... 0 .08 or on the following raw agricultural Goat, meat byproducts ...... 0 .40 commodities:

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Parts per Parts per Commodity million Commodity million

Sugarcane, cane 1 ...... 0.1 Horse, fat ...... 0.2

1 Horse, meat ...... 0.03 There are no U.S. Registrations on Sugarcane as of Sep- Horse, meat byproducts ...... 0.3 tember 24, 2018. Lemon/lime subgroup 10–10B ...... 1 (b) Section 18 emergency exemptions. Lentil, dry, seed ...... 2 Milk ...... 0.03 [Reserved] Milk, fat ...... 0.8 (c) Tolerances with regional registra- Nut, tree, group 14–12 ...... 0.06 tions. [Reserved] Orange subgroup 10–10A ...... 0.6 Peach subgroup 12–12B ...... 1.5 (d) Indirect or inadvertent residues. Peanut ...... 0.01 [Reserved] Peanut, hay ...... 30 Plum prune, dried ...... 4 [84 FR 11420, Mar. 27, 2019] Plum subgroup 12–12C ...... 2 Poultry, fat ...... 0.015 § 180.705 Mefentrifluconazole; toler- Poultry, meat ...... 0.01 ances for residues. Poultry, meat byproducts ...... 0.01 Rapeseed subgroup 20A ...... 1 (a) General. Tolerances are estab- Sheep, fat ...... 0.2 lished for residues of Sheep, meat ...... 0.03 Sheep, meat byproducts ...... 0.3 mefentrifluconazole, including its me- Soybean, seed ...... 0.4 tabolites and degradates, in or on the Vegetable, foliage of legume, group 7 ...... 20 commodities in the table below. Com- Vegetable, legume, group 6, except lentil and soybean seed ...... 0.15 pliance with the tolerance levels speci- Vegetable, tuberous and corm, subgroup 1C ..... 0.04 fied below is to be determined by meas- Wheat, grain ...... 0.3 uring only mefentrifluconazole, a-[4-(4- chlorophenoxy)-2- (b)–(d) [Reserved] (trifluoromethyl)phenyl]-a-methyl-1H- [84 FR 30945, June 28, 2019] 1,2,4-triazole-1-ethanol, in or on the commodity. § 180.706 Valifenalate; tolerances for residues. Parts per Commodity million (a)(1) Tolerances are established for residues of the fungicide valifenalate, Almond, hulls ...... 4 Beet, sugar, dried pulp ...... 2 including its metabolites and Beet, sugar, leaves ...... 9 degradates, in or on the following com- Beet, sugar, roots ...... 0.6 modities. Compliance with the toler- Cattle, fat ...... 0.2 Cattle, meat ...... 0.03 ance levels is to be determined by Cattle, meat byproducts ...... 0.3 measuring only valifenalate (methyl N- Cherry subgroup 12–12A ...... 4 (isopropoxycarbonyl)-L-valyl-(3RS)-3- Corn, field, grain ...... 0.01 Corn, milled byproducts ...... 0.03 (4-chlorophenyl)-b-alainate), in or on Corn, pop, grain ...... 0.01 the following commodities. Corn, sweet, kernel plus cob with husks removed ...... 0.03 Parts per Egg ...... 0.01 Commodity million Fruit, citrus, group 10–10, dried pulp ...... 2 Fruit, citrus, group 10–10, oil ...... 15 Celery ...... 5 Fruit, pome, group 11–10 ...... 1.5 Grape 1 ...... 5 Fruit, small, vine climbing, except fuzzy kiwifruit, Grape, raisin 1 ...... 6 subgroup 13–07F ...... 1.5 Vegetable, bulb, group 3–07 ...... 0.6 Goat, fat ...... 0.2 Vegetable, cucurbit, group 9 ...... 0.3 Goat, meat ...... 0.03 Vegetable, fruiting, group 8–10 ...... 1 Goat, meat byproducts ...... 0.3 1 Grain, aspirated grain fractions ...... 6 As of July 1, 2019, valifenalate is not registered in the United States for use on this commodity. Grain, cereal, forage, fodder, and straw, group 16, forage ...... 6 (2) Tolerances are established for res- Grain, cereal, forage, fodder, and straw, group 16, hay ...... 15 idues of the fungicide valifenalate, in- Grain, cereal, forage, fodder, and straw, group cluding its metabolites and degradates, 16, stover ...... 9 in or on the following commodities. Grain, cereal, forage, fodder, and straw, group Compliance with the tolerance levels is 16, straw ...... 30 Grain, cereal, group 15, except wheat and corn 4 to be determined by measuring only Grape, raisin ...... 4 the sum of valifenalate, methyl N- Grapefruit subgroup 10–10C ...... 0.5 (isopropoxycarbonyl)-L-valyl-(3RS)-3- Hog, fat ...... 0.015 Hog, meat ...... 0.01 (4-chlorophenyl)-b-alainate and Hog, meat byproducts ...... 0.03 valifenalate acid, 3-(4-chlorophenyl)-3-

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[[N-(isopropoxycarbonyl)-L-valyl]- total quantity of the pesticide chem- amino] propionic acid calculated as the ical in or on all raw agricultural com- stoichiometric equivalent of modities for which it is useful under valifenalate, in or on the following conditions of use currently prevailing commodities. or proposed will involve no hazard to Parts per the public health. Commodity million [69 FR 23117, Apr. 28, 2004] Potato ...... 0.04 Potato, granules/flakes ...... 0.09 § 180.905 Pesticide chemicals; exemptions from the requirement of a tol- (b) Section 18 emergency exemptions. erance. [Reserved] (c) Tolerances with regional registra- (a) When applied to growing crops, in tions. [Reserved] accordance with good agricultural (d) Indirect or inadvertent residues. practice, the following pesticide chemi- [Reserved] cals are exempt from the requirement of a tolerance: [84 FR 31218, July 1, 2019] (1) Petroleum oils. § 180.708 Isotianil; tolerances for resi- (2) Piperonyl butoxide. dues. (3) Pyrethrins. (a) General. Tolerances are estab- (4) Sabadilla. lished for residues of isotianil, includ- (b) When applied to growing crops, in ing its metabolites and degradates, in accordance with good agricultural or on the commodities in the table practice, the pesticides rotenone or below. Compliance with the tolerance derris or cube roots are exempt from level specified in the table in this para- the requirement of a tolerance. There graph (a) is to be determined by meas- are no U.S. registrations for use of ro- uring only isotianil (3,4-dichloro-N-(2- tenone, derris, or cube roots on food cyanophenyl)-5- commodities as of March 23, 2011. isothiazolecarboxamide) in or on the (c) These pesticides are not exempted commodity. from the requirement of a tolerance when applied to a crop at the time of or Commodity Parts per million after harvest.

1 Banana ...... 0.02 [77 FR 59128, Sept. 26, 2012] 1 There are no U.S. registrations for bananas as of Novem- ber 1, 2019. § 180.910 Inert ingredients used pre- (b) [Reserved] and post-harvest; exemptions from the requirement of a tolerance. [84 FR 58627, Nov. 1, 2019] Residues of the following materials Subpart D—Exemptions From are exempted from the requirement of Tolerances a tolerance when used in accordance with good agricultural practice as inert § 180.900 Exemptions from the require- (or occasionally active) ingredients in ment of a tolerance. pesticide formulations applied to grow- An exemption from a tolerance shall ing crops or to raw agricultural com- be granted when it appears that the modities after harvest:

TABLE 1 TO 180.910

Inert ingredients Limits Uses

Acetic acid ...... Catalyst Acetic anhydride ...... Solvent, cosolvent Acetone ...... Do.

Alcohols, C2–33, manuf. of, by-products from, ...... Solvent overheads (CAS Reg. No. 876065–86–0). Alkanoic and alkenoic acids, mono- and diesters of ...... Emulsifiers a-hydro-w-hydroxypoly (oxyethylene) with molecular weight (in amu) range of 200 to 6,000.

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TABLE 1 TO 180.910—Continued

Inert ingredients Limits Uses

Alkyl (C8-C24) benzenesulfonic acid and its ammo- ...... Surfactants, related adjuvants of surfactants nium, calcium, magnesium, potassium, sodium, and zinc salts.

C10-C18-Alkyl dimethyl amine oxides (CAS Reg. 15% by weight in pesticide Surfactant Nos. 1643–20–5, 2571–88–2, 2605–79–0, 3332– formulation. 27–2, 61788–90–7, 68955–55–5, 70592–80–2, 7128–91–8, 85408–48–6, and 85408–49–7).

a-alkyl(C6- C15)-w-hydroxypoly(oxyethylene)sulfate, Not to exceed 30% of for- Surfactants, related adjuvants of surfactants. and its ammonium, calcium, magnesium, potas- mulation. sium, sodium, and zinc salts, poly(oxyethylene) content averages 2–4 moles (CAS Reg. Nos.: 3088–31–1, 3694–74–4, 9004–82–4, 9004–84– 6, 9021–91–4, 9086–52–6, 13150–00–0, 15826– 16–1, 25446–78–0, 26183–44–8, 27140–00–7, 27731–62–0, 32612–48–9, 34431–25–9, 35015– 74–8, 50602–06–7, 52286–18–7, 52286–19–8, 54116–08–4, 55901–67–2, 61702–79–2, 61894– 66–4, 62755–21–9, 63428–85–3, 63428–86–4, 63428–87–5, 65086–57–9, 65086–79–5, 65104– 74–7, 65122–38–5, 67674–66–2, 67762–19–0, 67762–21–4, 67845–82–3, 67845–83–4, 67923– 90–4, 68037–05–8, 68037–06–9, 68171–41–5, 68424–50–0, 68511–39–7, 68585–34–2, 68610– 66–2, 68611–29–0, 68611–55–2, 68649–53–6, 68890–88–0, 68891–29–2, 68891–30–5, 68891– 38–3, 69011–37–6, 73665–22–2, 75422–21–8, 78330–16–2, 78330–17–3, 78330–25–3, 78330– 26–4, 78330–27–5, 78330–28–6, 78330–29–7, 78330–30–0, 96130–61–9, 106597–03–9, 110392–50–2, 119432–41–6, 125301–88–4, 125301–89–5, 125301–92–0, 125736–54–1, 157707–85–2, 160104–51–8, 160901–27–9, 160901–28–0, 160901–29–1, 160901–30–4, 161025–28–1, 161074–79–9, 162063–19–6, 219756–63–5).

a-alkyl (C12-C15)-w-hydroxypoly (oxypropylene) Not more than 20% of pes- Surfactant poly (oxyethylene) copolymers (where the poly ticide formulations. (oxypropylene) content is 3–60 moles and the poly (oxyethylene) content is 5–80 moles).

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TABLE 1 TO 180.910—Continued

Inert ingredients Limits Uses

a-Alkyl-w-hydroxypoly (oxypropylene) and/or poly ...... Surfactants, related adjuvants of surfactants (oxyethylene) polymers where the alkyl chain contains a minimum of six carbons (CAS Reg. Nos.: 9002–92–0; 9004–95–9; 9004–98–2; 9005–00–9; 9035–85–2; 9038–29–3; 9038–43– 1; 9040–05–5; 9043–30–5; 9087–53–0; 25190– 05–0; 24938–91–8; 25231–21–4; 251553–55–6; 26183–52–8; 26468–86–0; 26636–39–5; 27252– 75–1; 27306–79–2; 31726–34–8; 34398–01–1; 34398–05–5; 37251–67–5; 37311–00–5; 37311– 01–6; 37311–02–7; 37311–04–9; 39587–22–9; 50861–66–0; 52232–09–4; 52292–17–8; 52609– 19–5; 57679–21–7; 59112–62–8; 60828–78–6; 61702–78–1; 61723–78–2; 61725–89–1; 61791– 13–7; 61791–20–6; 61791–28–4; 61804–34–0; 61827–42–7; 61827–84–7; 62648–50–4; 63303– 01–5; 63658–45–7; 63793–60–2; 64366–70–7; 64415–24–3; 64415–25–4; 64425–86–1; 65104– 72–5; 65150–81–4; 66455–14–9: 66455–15–0; 67254–71–1; 67763–08–0; 68002–96–0; 68002– 97–1; 68131–39–5; 68131–40–8; 68154–96–1; 68154–97–2; 68154–98–3; 68155–01–1; 68213– 23–0; 68213–24–1; 68238–81–3; 68238–82–4; 68409–58–5; 68409–59–6; 68439–30–5; 68439– 45–2; 68439–46–3; 68439–48–5; 68439–49–6; 68439–50–9; 68439–51–0; 68439–53–2; 68439– 54–3; 68458–88–8; 68526–94–3; 68526–95–4; 68551–12–2; 68551–13–3; 68551–14–4; 68603– 20–3; 68603–25–8; 68920–66–1; 68920–69–4; 68937–66–6; 68951–67–7; 68954–94–9; 68987– 81–5; 68991–48–0; 69011–36–5; 69013–18–9; 69013–19–0; 69227–20–9; 69227–21–0; 69227– 22–1; 69364–63–2; 70750–27–5; 70879–83–3; 70955–07–6; 71011–10–4; 71060–57–6; 71243– 46–4; 72066–65–0; 72108–90–8; 72484–69–6; 72854–13–8; 72905–87–4; 73018–31–2; 73049– 34–0; 74432–13–6; 74499–34–6; 78330–19–5; 78330–20–8; 78330–21–9; 78330–23–1; 79771– 03–2; 84133–50–6; 85422–93–1; 97043–91–9; 97953–22–5; 102782–43–4; 103331–86–8; 103657–84–7; 103657–85–8; 103818–93–5; 103819–03–0; 106232–83–1; 111905–54–5; 116810–31–2; 116810–32–3; 116810–33–4; 120313–48–6; 120944–68–5; 121617–09–2; 126646–02–4; 126950–62–7; 127036–24–2; 139626–71–4; 152231–44–2; 154518–36–2; 157627–86–6; 157627–88–8; 157707–41–0; 157707–43–2; 159653–49–3; 160875–66–1; 160901–20–2; 160901–09–7; 160901–19–9; 161025–21–4; 161025–22–5; 166736–08–9; 169107–21–5; 172588–43–1; 176022–76–7; 196823–11–7; 287935–46–0; 288260–45–7; 303176–75–2; 954108–36–2; 2222805–23–2).

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TABLE 1 TO 180.910—Continued

Inert ingredients Limits Uses

a-alkyl (minimum C6 linear, branched, saturated Not to exceed 30% of for- Surfactants, related adjuvants of surfactants. and/or unsaturated)-w-hydroxypolyoxyethylene mulation. polymer with or without polyoxypropylene, mixture of di- and monohydrogen phosphate esters and the corresponding ammonium, calcium, magnesium, monoethanolamine, potassium, sodium, and zinc salts of the phosphate esters; minimum oxyethylene content is 2 moles; minimum oxypropylene content is 0 moles (CAS Reg. Nos.: 9004–80–2, 9046–01–9, 26982–05– 8, 31800–89–2, 37280–82–3, 37281–86–0, 39341–09–8, 39341–65–6, 39464–66–9, 39464– 69–2, 42612–52–2, 50643–20–4, 50668–50–3, 51325–10–1, 51884–64–1, 52019–36–0, 57486– 09–6, 58206–38–5, 58318–92–6, 58857–49–1, 59112–71–9, 60267–55–2, 61837–79–4, 62362– 49–6, 62482–61–5, 63747–86–4, 63887–54–7, 63887–55–8, 66020–37–9, 66272–25–1, 66281– 20–7, 67711–84–6, 67786–06–5, 67989–06–4, 68070–99–5, 68071–17–0, 68071–35–2, 68071– 37–4, 68130–44–9, 68130–45–0, 68130–46–1, 68130–47–2, 68186–29–8, 68186–34–5, 68186– 36–7, 68186–37–8, 68238–84–6, 68311–02–4, 68311–04–6, 68332–75–2, 68389–72–0, 68400– 75–9, 68413–78–5, 68425–73–0, 68425–75–2, 68439–39–4, 68458–48–0, 68511–15–9, 68511– 36–4, 68511–37–5, 68551–05–3, 68585–15–9, 68585–16–0, 68585–17–1, 68585–36–4, 68585– 39–7, 68603–24–7, 68607–14–7, 68610–64–0, 68610–65–1, 68649–29–6, 68649–30–9, 68650– 84–0, 68815–11–2, 68855–46–9, 68856–03–1, 68890–90–4, 68890–91–5, 68891–12–3, 68891– 13–4, 68891–26–9, 68908–64–5, 68909–65–9, 68909–67–1, 68909–69–3, 68921–24–4, 68921– 60–8, 68954–87–0, 68954–88–1, 68954–92–7, 68987–35–9, 69029–43–2, 69980–69–4, 70247– 99–3, 70248–14–5, 70844–96–1, 70903–63–8, 71965–23–6, 71965–24–7, 72480–27–4, 72623– 67–7, 72623–68–8, 72828–56–9, 72828–57–0, 73018–34–5, 73038–25–2, 73050–08–5, 73050– 09–6, 73361–29–2, 73378–71–9, 73378–72–0, 73559–42–9, 73559–43–0, 73559–44–1, 73559– 45–2, 74499–76–6, 76930–25–1, 78041–18–6, 78330–22–0, 78330–24–2, 82465–25–6, 84843– 37–8, 91254–26–1, 93925–54–3, 95014–34–9, 96416–89–6, 99924–51–3, 103170–31–6, 103170–32–7, 106233–09–4, 106233–10–7, 108818–88–8, 110392–49–9, 111798–26–6, 111905–50–1, 116671–23–9, 117584–36–8, 119415–05–3, 120913–45–3, 121158–61–0, 121158–63–2, 123339–53–7, 125139–13–1, 125301–86–2, 125301–87–3, 126646–03–5, 129208–04–4, 129870–77–5, 129870–80–0, 130354–37–9, 136504–88–6, 143372–50–3, 143372–51–4, 144336–75–4, 146815–57–8, 151688–56–1, 154518–39–5, 154518–40–8, 155240–11–2, 159704–69–5, 160498–49–7, 160611–24–5, 171543–66–1, 172027–16–6, 172274–69–0, 176707–42–9, 181963–82–6, 188741–55–1, 191940–53–1, 210493–60–0, 210993–53–6, 246159–55–7, 251298–11–0, 261627–68–3, 290348–69–5, 290348–70–8, 317833–96–8, 340681–28–9 , 422563–19–7, 422563–26–6, 522613–09–8, 717140–06–2, 717140–09–5, 717827–29–7, 762245–80–7, 762245–81–8, 866538–89–8, 866538–90–1, 873662–29–4, 913068–96–9, 936100–29–7, 936100–30–0, 1072943–56–6, 1087209–87–7, 1174313–54–2, 1187742–89–7, 1187743–35–6, 1205632–03–6, 1233235–49–8, 1451002–50–8, 1456802–88–2, 1456802–89–3, 1456803–12–5).

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TABLE 1 TO 180.910—Continued

Inert ingredients Limits Uses

N-alkyl (C8-C18) primary amines and their acetate Concentration in formu- Surfactants, related adjuvants of surfactants salts where the alkyl group is linear and may be lated end-use products saturated and/or unsaturated (CAS Reg. Nos. not to exceed 10% by 61790–57–6, 61790–58–7, 61790–59–8, 61790– weight in herbicide prod- 60–1, 61788–46–3, 61790–33–8, 68155–38–4). ucts, 4% by weight in insecticide products, and 4% by weight in fungicide products. Alkyl (C8-C18) sulfate and its ammonium, calcium, ...... Surfactants. isopropylamine, magnesium, potassium, sodium, and zinc salts. Aluminum hydroxide ...... Diluent, carrier Aluminum oxide ...... Diluent Aluminum stearate ...... Surfactant Amides, C5-C9, N-[3-(dimethylamino) propyl] (CAS ...... Surfactant Reg. No. 1044764–00–2). Amides, C6-C12, N-[3-(dimethylamino) propyl] (CAS ...... Surfactant Reg. No. 1044764–06–8). Ammonium bicarbonate ...... Surfactant, suspending agent, dispersing agent Ammonium carbamate...... Synergist in aluminum phosphide formulations Ammonium chloride ...... Intensifier when used with ammonium nitrate as a dessicant or defoliant. Fire suppressant in aluminum phosphide and magnesium phosphide formulations Ammonium hydroxide ...... Solvent, cosolvent, neutralizer, solubilizing agent Ammonium persulfate (CAS Reg.No. 7727–54–0) 0.05% ...... Preservative Ammonium salts of fatty acids (C8-C18 saturated) ...... Surfactant (CAS Reg. No. 5972–76–9, 63718–65–0, 16530–70–4, 32582–95–9, 2437–23–2, 191799– 95–8, 16530–71–5, 93917–76–1, 5297–93–8, 94266–36–1, 1002–89–7). Ammonium stearate ...... Surfactant Ammonium sulfate ...... Solid diluent, carrier Ammonium thiosulfate ...... Intensifier when used with ammonium nitrate as desiccant or defoliant Amyl acetate ...... Solvent, cosolvent, attractant Ascorbyl palmitate ...... Preservative Attapulgite-type clay ...... Solid diluent, carrier, thickener Bacillus simplex strain BU288 ...... Emulsifier Bacillus thuringiensis fermentation solids and/or ...... Diluent, carrier solubles. Bentonite ...... Solid diluent, carrier Benzoic acid ...... Preservative for formulation Bicyclo[3.1.1]hept–2–ene, 2,6,6–trimethyl–, ...... Surfactants, related adjuvants of surfactants homopolymer (Alpha-pinene, homopolymer)(CAS Reg. No. 25766–18–1). Bicyclo[3.1.1]heptane, 6,6–dimethyl–2–methylene–, ...... Surfactants, related adjuvants of surfactants homopolymer (Beta-pinene, homopolymer) (CAS Reg. No. 25719–60–2). Bicyclo[3.1.1]hept–2–ene, 2,6,6–trimethyl–, poly- ...... Surfactants, related adjuvants of surfactants mer with 6,6–dimethyl–2–methylenebicyclo [3.1.1] heptane (Copolymer of alpha- and beta- pinene) (CAS Reg. No. 31393–98–3). 2-Bromo-2-nitro-1,3-propanediol (CAS Reg. No. 0.04% or less by weight of In-can preservative 52–51–7). the total pesticide formulation. Butane ...... Propellant Butanedioic acid, 2-sulfo-, C-C9-11-isoalkyl esters, Not to exceed 10% by Surfactant C10-rich, disodium salts (CAS Reg. No. weight in pesticide for- 815583–91–6). mulation for agricultural use. n-Butanol (CAS Reg. No. 71–36–3) ...... Solvent, cosolvent n-Butyl benzoate (CAS Reg. No.136–60–7) ...... Solvent di-n-Butyl adipate (CAS Reg. No. 105–99–7) ...... Not to exceed 25% by Plasticizer in pesticide formulations for varroa weight of pesticide for- mite control around bee hives mulation. n-Butyl-3-hydroxybutyrate (CAS Reg. No. 53605– ...... Solvent 94–0). Butylated hydroxyanisole ...... Antioxidant

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TABLE 1 TO 180.910—Continued

Inert ingredients Limits Uses

Butylated hydroxytoluene ...... Do. Calcareous shale ...... Solid diluent carrier Calcite ...... Do. Calcium carbonate ...... Do. Calcium chloride ...... Stabilizer Calcium phosphate ...... Solid diluent, carrier Calcium hydroxide ...... Do. Calcium hypochlorite ...... Sanitizing and bleaching agent Calcium lactate pentahydrate (CAS Reg. No...... Nutrient, stabilizer 5743–47–5). Calcium oxide ...... Solid diluent, carrier Calcium salt of partially dimerized rosin, con- ...... Coating agent forming to 21 CFR 172.210. Calcium silicate ...... Solid diluent, carrier Calcium stearate ...... Do. Carbon Dioxide (CAS Reg. No. 124–38–9) ...... None ...... Propellant Carrageenan, conforming to 21 CFR 172.620 ...... Minimum molecular weight Thickener (in amu): 100,000. Cetyl alcohol (CAS Reg. No. 36653–82–4) ...... Not more than 5.0% of Evaporation retardant pesticide formulation. Charcoal, activated ...... Meets specifications in the Carrier Food Chemical Codex. Coconut shells ...... Solid diluent and carrier Cod liver oil ...... Solvent, cosolvent Croscarmellose sodium (CAS Reg. No. 74811–65– ...... Disintegrant, solid diluent, carrier, and thick- 7). ener n-Decyl alcohol (CAS Reg. No. 112–30–1) ...... Solvent or co-solvent Dialkyl (C8-C18) dimethyl ammonium chloride ...... Not more than 0.2% in sili- Flocculating agent in the manufacture of silica, hydrated silica. ca, hydrated silica for use as a solid diluent, carrier Diatomite (diatomaceous earth) ...... Solid diluent carrier Diethylaminoethanol, ethoxylated, propoxylated, re- ...... Surfactant action products with fatty acid dimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173188–75–4). Diethylaminoethanol, ethoxylated, propoxylated, re- ...... Surfactant action products with fatty acid trimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173188–83–4). Diethylaminoethanol, ethoxylated, reaction product ...... Surfactant with fatty acid dimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173188–72–1). Diethylaminoethanol, ethoxylated, reaction prod- ...... Surfactant ucts with fatty acid trimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173188–81–2). Diethylene glycol abietate ...... Surfactants, related adjuvants of surfactants 1,1-Difluoroethane (CAS Reg. No. 75–37–6) ...... In pesticide formulations Aerosol propellant used for insect control in food- and feed-handling establishments and animals; in bird repellent pesticide formulations. 1,2-Dihydro-6-ethoxy-2,2,4-trimethylquinolene ...... Not more than 0.02% of Antioxidant pesticide formulation. Diisopropanolamine (CAS Reg. No. 110–97–4) ...... Not to exceed 10% by Neutralizer or stabilizer weight of pesticide formulation. Diisopropyl adipate (CAS Reg. No. 6938–94–9) .... 40% in mosquito control Solvent, co-solvent formulations. Dimethyl adipate (CAS no. 627–93–0) ...... None ...... Solvent/co-solvent Dimethylaminoethanol, ethoxylated, propoxylated, ...... Surfactant reaction products with fatty acid dimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173188–42–5). Dimethylaminoethanol, ethoxylated, propoxylated, ...... Surfactant reaction products with fatty acid trimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173188–67–4).

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Inert ingredients Limits Uses

Dimethylaminoethanol, ethoxylated, reaction prod- ...... Surfactant ucts with fatty acid dimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173188–38–9). Dimethylaminoethanol, ethoxylated, reaction prod- ...... Surfactant ucts with fatty acid trimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173188–49–2). N,N-Dimethyl 9-decenamide (CAS Reg. No. Not to exceed 20% by Surfactant, solvent 1356964–77–6). weight of pesticide formulation. N,N-Dimethyldodecanamide (CAS Reg. No. 3007– Not to exceed 20% by Surfactant, solvent 53–2). weight of pesticide formulation. Dimethyl ether (methane, oxybis-) (CAS Reg. No...... Propellant 115–10–6). Dimethyl glutarate (CAS no. 1119–40–0) ...... None ...... Solvent/co-solvent 3,6-Dimethyl-4-octyn-3,6-diol ...... Not more than 2.5% of Surfactants, related adjuvants of surfactants pesticide formulation. Dimethyl succinate (CAS no. 106–65–0) ...... None ...... Solvent/co-solvent N,N-Dimethyltetradecanamide (CAS Reg. No. Not to exceed 20% by Surfactant, solvent 3015–65–4). weight of pesticide formulation. Di-n-butyl carbonate (CAS Reg. No. 542–52–9) ...... Solvent Dipropylene glycol ...... Solvent, cosolvent Disodium phosphate ...... Anticaking agent, conditioning agent Disodium zinc ethylenediaminetetraacetate ...... Sequestrant dihydride. Distillates, (Fishcher-Tropsch), heavy, C18-C50, ...... Solvent, diluent and/or dust suppressant branched, cyclic and linear (CAS Reg. No. 848301–69–9). Distillates (petroleum), solvent-dewaxed heavy par- ...... Carrier affinic (CAS Reg. No. 64742–65–0). Dolomite ...... Solid diluent, carrier Epoxidized linseed oil ...... Surfactants, related adjuvants of surfactants Epoxidized soybean oil ...... Do. Ethanesulfonic acid, 2-hydroxy- (CAS Reg. No...... Chelator, sequestrant, or conditioning agent 107–36–8). Ethanesulfonic acid, 2-hydroxy-, ammonium salts ...... Do. (CAS Reg. No. 57267–78–4). Ethanesulfonic acid, 2-hydroxy-, calcium salts ...... Do. (CAS Reg. No. 10550–47–7). Ethanesulfonic acid, 2-hydroxy-, magnesium salts ...... Do. (CAS Reg. No. 17345–56–1). Ethanesulfonic acid, 2-hydroxy-, potassium salts ...... Do. (CAS Reg. No. 1561–99–5). Ethanesulfonic acid, 2-hydroxy-, sodium salts (CAS ...... Do. Reg. No. 1562–00–1). Ethanesulfonic acid, 2-hydroxy-, zinc salts (CAS ...... Do. Reg. No. 129756–32–7). Ethyl acetate ...... Solvent, cosolvent Ethyl alcohol ...... Do. Ethyl esters of fatty acids derived from edible fats ...... Solvent, cosolvent and oils. Ethyl maltol (CAS Reg. No.4940–11–8) ...... Not more than 0.2 % of Odor masking agent the pesticide formulation. Ethylene glycol (CAS Reg. No. 107–21–1) ...... Without limitation ...... Encapsulating agent for pesticides being applied post-harvest as residual, and crack and crevice sprays in and around food and nonfood areas of residential and nonresi- dential structures, including food handling establishments Ethylene oxide adducts of 2,4,7,9-tetramethyl-5- ...... Surfactants, related adjuvants of surfactants decynediol, the ethylene oxide content averages 3.5, 10 or 30 moles (CAS Reg. No. 9014–85–1). Ethylenebis(oxyethylene) bis[3-(5-tert-butyl-4-hy- 1% by weight ...... Stabilizer droxy-m-tolyl) propionate] (CAS Reg. No. 36443–68–2). (S,S)-Ethylenediamine disuccinic acid trisodium ...... Sequestrant or chelating agent salt (CAS Reg. No. 178949–82–1). Ethylenediaminetetraacetic acid ...... 3% of pesticide formulation Sequestrant Ethylenediaminetetraacetic acid, tetrasodium salt .. 5% of pesticide formulation Sequestrant

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TABLE 1 TO 180.910—Continued

Inert ingredients Limits Uses

2–Ethyl-1-hexanol (CAS Reg. No. 104–76–7) ...... Not more than 10% of pes- Solvent, adjuvant of surfactants ticide. Fatty acids, conforming to 21 CFR 172.860 ...... Binder, defoaming agent, lubricant FD&C Blue No. 1 ...... Not more than 0.2% of Dye pesticide formulation. FD&C Red No. 40 (CAS Reg. No. 25956–17–6) Not to exceed 0.002% by Dye, coloring agent conforming to 21 CFR 74.340. weight of pesticide formulation. Ferric Citrate (CAS Reg. No. 2338–05–8) ...... Stabilizer Ferric sulfate ...... Solid diluent, carrier Formic Acid (CAS Reg. No. 64–18–6) ...... 25% ...... adjuvant, pH buffering agent, pH adjuster Fulvic acid (CAS Reg. No. 479–66–3) ...... Carrier Furcelleran ...... Thickener

D-Glucitol, 1-deoxy-1-(methyl-amino)-, N-C8-10 acyl Not more than 40% by Surfactant derivatives (CAS Reg. No. 1591782–62–5). weight in pesticide formulation. D-glucitol, 1,4:3,6-dianhydro-2,5-di-O-methyl- (CAS ...... solvent, co-solvent, viscosity modifier, and Reg. No. 5306–85–4); D-glucitol, 1,4:3,6- adjuvant dianhydro-2,5-di-O-ethyl- (CAS Reg. No. 30915– 81–2); D-glucitol, 1,4:3,6-dianhydro-2,5-di-O- propyl) (CAS Reg. No.107644–13–3); D-glucitol, 1,4:3,6-dianhydro-2,5-bis-O-(1-methylethyl)-,(isopropyl diether) (CAS Reg. No. 103594–41–8); D- glucitol, 1,4:3,6-dianhydro-2,5-di-O-butyl- (CAS Reg. No. 103594–42–9); D-glucitol, 1,4:3,6- dianhydro-2,5-di-O-(1-methylpropyl)-, (CAS Reg. No. not assigned); and D-glucitol, 1,4:3,6- dianhydro-2,5-di-O-(2-methylpropyl)-, (CAS Reg. No. not assigned).

D-glucopyranose, oligomeric, C10–16-alkyl ...... Surfactant glycosides (CAS Reg. No. 110615–47–9). D-glucopyranose, oligomeric, 6-(dihydrogen cit- ...... Surfactant rates), C8–20 branched and linear alkyl glycosides, sodium salts (CAS Reg. No. 1079993–97–7). D-glucopyranose, oligomeric, 6-(hydrogen ...... Surfactant sulfosuccinates), C8–20 branched and linear alkyl glycosides, sodium salts (CAS Reg. No. 1079993–92–2).

D-glucopyranose, oligomeric, lactates, C8–20 ...... Surfactant branched and linear alkyl glycosides (CAS Reg. No. 1079993–94–4). D-glucurono-6-deoxy-L-manno-D-glucan, acetate, ...... Stabilizer/suspension agent. calcium magnesium potassium sodium salt (diutan gum) (CAS Reg. No. 595585–15–2). Glycerides, edible fats and oils derived from plants ...... Emulsifier, dispersing agent and animals, reaction products with sucrose (CAS Reg. Nos. 100403–38–1, 100403–41–6, 100403–39–2, 100403–40–5). Glycerol mono-, di-, and triacetate ...... Solvent, cosolvent Glyceryl monostearate ...... Emulsifier Granite ...... Do. Graphite ...... Solid diluent, carrier Gum arabic (acacia) ...... Surfactant, suspending agent, dispersing agent Gypsum ...... Solid diluent, carrier Hexamethylenetetramine ...... For use in citrus washing Preservative solutions only at not more than 1%. 3-hexen-1-ol, (3Z)- (CAS Reg. No. 928-96-1) ...... Not more than 0.4% of the Odorant, alerting agent pesticide formulation. n-Hexyl alcohol (CAS Reg. No. 111–27–3) ...... Solvent, cosolvent

C9 rich aromatic hydrocarbons (CAS Reg. No...... Solvent 64742–95–6).

C10–11 rich aromatic hydrocarbons (CAS Reg. No...... Solvent 64742–94–5).

C11–12 rich aromatic hydrocarbons (CAS Reg. No...... Solvent 64742–94–5). Hydrochloric acid ...... Solvent, neutralizer

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Inert ingredients Limits Uses

Hydroxyethylmorpholine, ethoxylated, ...... Surfactant propoxylated, reaction products with fatty acid dimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173189– 06–4). Hydroxyethylmorpholine, ethoxylated, ...... Surfactant propoxylated, reaction products with fatty acid trimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173189– 17–7). Hydroxyethylmorpholine, ethoxylated, reaction ...... Surfactant products with fatty acid dimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173189–00–8). Hydroxyethylmorpholine, ethoxylated, reaction ...... Surfactant products with fatty acid trimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173189–09–7). Hydroxyethylpiperidine, ethoxylated, propoxylated, ...... Surfactant reaction products with fatty acid dimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173189–22–4. Hydroxyethylpiperidine, ethoxylated, propoxylated, ...... Surfactant reaction products with fatty acid trimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173189–28–0). Hydroxyethylpiperidine, ethoxylated, reaction prod- ...... Surfactant ucts with fatty acid dimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173189–20–2). Hydroxyethylpiperidine, ethoxylated, reaction prod- ...... Surfactant ucts with fatty acid trimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173189–25–7). Hydroxyethylidine diphosphonic acid (HEDP) (CAS For use in antimicrobial Stabilizer, chelator Reg. No. 2809–21–4). pesticide formulations at not more than 1 percent. Iron oxide ...... Solid diluent, carrier Iron oxide yellow (CAS Reg. No. 20344–49–4) ...... Not to exceed 0.15% by Colorant in pesticide formulations for varroa weight of pesticide for- mite control around bee hives mulation. Isoamyl acetate (CAS Reg. No. 123–92–2) ...... Buffering agent Isobutane (CAS Reg. No. 75–28–5) ...... None ...... Propellant Isobutyl Acetate (CAS Reg. No. 110–19–0) ...... Solvent Isobutyl isobutyrate (CAS Reg. No. 97–85–8) ...... None ...... Solvent Isobutyric Acid (CAS Reg. No. 79–31–2) ...... Solvent Isopropyl-3-hydroxybutyrate (CAS Reg. No...... Solvent 54074–94–1). Isopropyl myristate (CAS Reg. No. 110–27–0) ...... Solvent Kaolinite-type clay ...... Solid diluent, carrier Lactic acid ...... Solvent Lactic acid, 2-ethylhexyl ester (CAS Reg. No...... Solvent 6283–86–9). Lactic acid, 2-ethylhexyl ester, (2S)- (CAS Reg...... Solvent No. 186817–80–1). Lactic acid, n-propyl ester, (S); (CAS Reg. No...... Solvent 53651–69–7). Lauryl alcohol ...... Surfactant Lignin (CAS Reg. No. 9005–53–2) ...... Surfactant, related adjuvants of surfactants Lignin, alkali (CAS Reg. No. 8068–05–1) ...... Do. Lignin, alkali, oxidized, sodium salt (CAS Reg. No...... Do. 68201–23–0). Lignin alkali reaction products with disodium sulfite ...... Do. and formaldehyde (CAS Reg. No. 105859–97–0). Lignin alkali reaction products with formaldehyde ...... Do. and sodium bisulfite (CAS Reg. No. 68512–35– 6). Lignosulfonic acid (CAS Reg. No. 8062–15–5) ...... Do. Lignosulfonic acid, ammonium calcium salt (CAS ...... Do. Reg. No. 12710–04–2). Lignosulfonic acid, ammonium magnesium salt ...... Do. (CAS Reg. No. 123175–37–1).

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TABLE 1 TO 180.910—Continued

Inert ingredients Limits Uses

Lignosulfonic acid, ammonium salt (CAS Reg. No...... Do. 8061–53–8). Lignosulfonic acid, ammonium sodium salt (CAS ...... Do. Reg. No. 166798–73–8). Lignosulfonic acid, calcium magnesium salt (CAS ...... Do. Reg. No. 55598–86–2). Lignosulfonic acid, calcium salt (CAS Reg. No...... Do. 8061–52–7). Lignosulfonic acid, calcium sodium salt (CAS Reg...... Do. No. 37325–33–0). Lignosulfonic acid, ethoxylated, sodium salt (CAS ...... Do. Reg. No. 68611–14–3). Lignosulfonic acid, magnesium salt (CAS Reg. No...... Do. 8061–54–9). Lignosulfonic acid, potassium salt (CAS Reg. No...... Do. 37314–65–1). Lignosulfonic acid, sodium salt (CAS Reg. No...... Do. 8061–51–6). Lignosulfonic acid, sodium salt, oxidized (CAS ...... Do. Reg. No. 68855–41–4). Lignosulfonic acid, sodium salt, polymer with form- ...... Do. aldehyde and phenol (CAS Reg. No. 37207–89– 9). Lignosulfonic acid, sodium salt, sulfomethylated ...... Do. (CAS Reg. No. 68512–34–5). Lignosulfonic acid, zinc salt (CAS Reg. No. 57866– ...... Do. 49–6). d-Limonene (CAS Reg. No. 5989–27–5) ...... Solvent, fragrance Magnesium carbonate ...... Anticaking agent, conditioning agent Magnesium chloride ...... Safener Magnesium lime ...... Solid diluent, carrier Magnesium oxide ...... Do. Magnesium silicate ...... Do. Magnesium stearate ...... Surfactant Magnesium sulfate ...... Solid diluent, carrier, safener Methyl alcohol ...... Solvent Methyl n-amyl ketone (CAS Reg. No. 110–43–0) ...... Solvent, cosolvent Methyl 5-(dimethylamino)-2-methyl-5- ...... Solvent oxopentanoate (1174627–68–9). Methyl esters of fatty acids derived from edible fats ...... Solvent, cosolvent and oils. Methyl esters of higher fatty acids conforming to ...... Antidusting agent, surfactant 21 CFR 573.640. Methyl isobutyl ketone ...... Solvent 2-methyl-2,4-pentanediol (CAS Reg. No. 107–41– Without limitation ...... Growing crops and food animals 5). Methyl isobutyrate (CAS Reg. No. 547–63–7) ...... None ...... Solvent 2-methyl-1,3-propanediol (CAS Reg. No. 2163–42– ...... Solvent, surfactant 0). Methylated silicones ...... Antifoaming agent Mono-, di-, and trimethylnaphthalenesulfonic acids ...... Surfactants, related adjuvants of surfactants and naphthalenesulfonic acids formaldehyde condensates, ammonium, sodium and potassium salts (CAS Reg. Nos. 9008–63–3, 9069–80–1, 9084–06–4, 36290–04–7, 91078–68–1, 141959– 43–5, 68425–94–5, 67828–14–2). Mica ...... Solid diluent, carrier Mineral oil, U.S.P., or conforming to 21 CFR ...... Diluent, carrier, and solvent 172.878 or 178.3620(a) (CAS Reg. No. 8012– 95–1). Monoammonium phosphate ...... No more than 3.75% by Postharvest fumigation in formulation with weight in formulation. aluminum phosphide Monoethanolamine (CAS Reg. No. 141–43–5) ...... Not to exceed 3.35% by Solvent weight in pesticide formulation.

Mono- and diglycerides of C 8-C18 fatty acids ...... Surfactants, related adjuvants of surfactants Montmorillonite-type clay ...... Solid diluent, carrier

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Inert ingredients Limits Uses

Nonyl, decyl, and undecyl glycoside mixture with a ...... Surfactant. mixture of nonyl, decyl, and undecyl oligosaccharides and related reaction products (primarily decanol and undecanol) produced as an aqueous-based liquid (50 to 65% solids) from the reaction of primary alcohols (containing 15 to 20% secondary alcohol isomers) in a ratio of 20% C9, 40% C10, and 40% C11 with carbo- hydrates (average glucose to alkyl chain ratio 1.3 to 1.8). a-(p-Nonylphenol)-w-hydroxypoly(oxyethylene) mix- Not to exceed 7% of pes- Surfactants, related adjuvants of surfactants ture of dihydrogen phosphate and ticide formulation. monohydrogen phosphate esters and the corresponding ammonium, calcium, magnesium, potassium, sodium, and zinc salts of the phosphate esters; the nonyl group is a propylene trimer isomer and the poly(oxyethylene) content averages 4–14 or 30 moles (CAS Reg. Nos. 51811–79–1, 59139–23–0, 67922–57–0, 68412– 53–3, 68553–97–9, 68954–84–7, 99821–14–4, 152143–22–1, 51609–41–7, 37340–60–6, 106151–63–7, 68584–47–4, 52503–15–8, 68458–49–1). a-(p-Nonylphenyl)-w-hydroxypoly(oxyethylene) pro- ...... Surfactants, related adjuvants of surfactants duced by the condensation of 1 mole of nonylphenol (nonyl group is a propylene trimer isomer) with an average of 4-14 or 30-90 moles of ethylene oxide; if a blend of products is used, the average number of moles of ethylene oxide reacted to produce any product that is a component of the blend shall be in the range of 4-14 or 30-90. a-(p-Nonylphenol)-w-hydroxypoly(oxyethylene) sul- Not to exceed 7% of pes- Surfactants, related adjuvants of surfactants fate, ammonium, calcium, magnesium, potas- ticide formulation. sium, sodium, and zinc salts the nonyl group is propylene trimer isomer and the poly(oxyethylene) content averages 4 moles (CAS Reg. Nos. 9014–90–8, 9051–57–4, 9081– 17–8, 68649–55–8, 68891–33–8. 1-Octanal (CAS Reg. No. 124–13–0) ...... Not more than 0.2% of the Odor masking agent pesticide formulation. n-Octyl alcohol (CAS Reg. No. 111–87–5) ...... Solvent or co-solvent Octyl and decyl glucosides mixture with a mixture ...... Surfactants, related adjuvants of surfactants of octyl and decyloligosaccharides and related reaction products (primarily n- decanol) produced as an aqueous-based liquid (68-72% solids) from the reaction of straight chain alcohols (C8(45%), C10 (55%)) with anhydrous glucose. Oleic acid ...... Diluent Oleic acid diester of a-hydro-w-hydroxypoly (oxy- ...... Surfactants, related adjuvants of surfactants ethylene); the poly(oxyethylene) having average molecular weight (in amu) 400. a-Oleoyl-w-hydroxypoly(oxyethylene), average mo- ...... Emulsifier lecular weight (in amu) of 600. Oleyl alcohol (CAS Reg. No. 143–28–2 ...... 15% ...... Cosolvent Oxalic acid ...... No more oxalic acid should Calcium chelating hard water inhibitor be used than is necessary to chelate calcium and in no case should more than 2 lb oxalic acid per acre be used. Palmitic acid ...... Diluent Pentaerythritol ester of maleic anhydride modified ...... Plasticizer wood rosin. Pentaerythritol tetrakis (3-(3,5-di-tert-butyl-4- Not to exceed 5% by Antioxidant, stabilizer hydroxyphenyl)propionate) (CAS Reg. No. 6683– weight of the pesticide 19–8). formulation. Petrolatum, conforming to 21 CFR 172.880 ...... Coating agent Petroleum hydrocarbons, light odorless conforming ...... Solvent, diluent. to 21 CFR 172.884.

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TABLE 1 TO 180.910—Continued

Inert ingredients Limits Uses

Petroleum hydrocarbons, synthetic isoparaffinic, ...... Do. conforming to 21 CFR 172.882. Petroleum naphtha, conforming to 21 CFR ...... Component of coating agent 172.250(d). Petroleum wax, conforming to 21 CFR 172.886(d) ...... Coating agent 2-Phenoxyethanol (CAS Reg. No. 122–99–6) ...... 0.2% by weight in pes- Solvent or co-solvent ticide formulation. Phenylethyl acetate (CAS Reg. No. 103–45–7) ...... Not to exceed 0.015% in Solvent pesticide formulation. Phosphoric acid ...... Buffer Polyethylene, conforming to 21 CFR 177.1520(c) ...... Binder, carrier, and coating agent Polyethylene glycol[a-hydro-w- ...... Surfactants, related adjuvants of surfactants hydroxypoly(oxyethylene)]; mean molecular weight (in amu) 194 to 9,500 conforms to 21 CFR 178.3750. Polyethyleneimine (CAS Reg. No. 9002–98–6) ...... Minimum number average Emulsifier, surfactant, adjuvant, dispersant molecular weight 1,300 and/or coating amu. Polyglycerol esters of fatty acids conforming to 21 ...... Surfactants, related adjuvants of surfactants CFR 172.854. Polyglyceryl phthalate ester of coconut oil fatty None ...... Surfactants, related adjuvants of surfactants acids, including fatty acid coco polymers with glyceryl and phthalic anhydride (CAS No. 67746–02–5) and coconut oil polymer with glyceryl and phthalic anhydride (CAS No. 66070– 87–9). Poly(oxy-1,2-ethanediyl), a-(carboxymethyl)-w- ...... Surfactant (nonylphenoxy) produced by the condensation of 1 mole of nonylphenol (nonyl group is a propylene trimer isomer) with an average of 4-14 or 30-90 moles of ethylene oxide. The molecular weight (in amu) ranges are 454-894 and 1598- 4238. Poly(oxy-1,2-ethanediyl), a-(1-oxoalkyl)-w-methoxy- Not to exceed 25% by Stabilizer, solubilizing agent , where the alkyl chain contains a minimum of 6 weight in pesticide for- and a maximum of 18 carbons and the oxy- mulation. ethylene content is 3–13 moles (CAS Reg. No. 53100–65–5, 194289–64–0, 34398–00–0, 9006– 27–3, 32761–35–6, 53467–81–5, 518299–31–5, and 34397–99–4). Poly(oxy-1,2-ethanediyl), a-[tris(1- For use in post-harvest ap- Surfactants phenylethyl)phenyl]-w-hydroxy-, (CAS Reg. No. plications; not to exceed 99734–09–5). 15% by weight in pesticide formulations. Poly(oxy-1,2-ethanediyl), a-(3-carboxy-1- Not to exceed 10% by Surfactant oxosulfopropyl)-w-hydroxy-, C10-12-alkyl ethers, weight of pesticide for- disodium salts, the poly(oxyethylene) content mulation. averages 5–15 moles (CAS Reg. No. 68954– 91–6). Poly(oxy-1,2-ethanediyl), a-(3-carboxy-1- Not to exceed 10% by Surfactant oxosulfopropyl)-w-hydroxy-, C10-16-alkyl ethers, weight of pesticide for- disodium salts, the poly(oxyethylene) content mulation. averages 5–15 moles (CAS Reg, No. 68815– 56–5). Poly(oxy-1,2-ethanediyl), a-(3-carboxy-1- Not to exceed 10% by Surfactant oxosulfopropyl)-w-hydroxy-, C12-14-alkyl ethers, weight of pesticide for- disodium salts, the poly(oxyethylene) content mulation. averages 5–15 moles (CAS Reg. No. 1024612– 24–5). Poly(oxy-1,2-ethanediyl), a-(3-carboxy-1- Not to exceed 10% by Surfactant oxosulfopropyl)-w-(isotridecyloxy)-, sodium salt weight of pesticide for- (1:2), the poly(oxyethylene) content averages 5– mulation. 15 moles (CAS Reg. No. 1013906–64–3). Polyoxyethylene (20) sorbitan monostearate ...... Surfactants, related adjuvants of surfactants [Poly[oxy(methyl-1,2-ethanediyl)], a-[2-bis(2-hy- Not to exceed 15% in the Surfactant droxyethyl)amino]propyl]-w-hydroxy,-ether with formulated product; only a-hydro-w-hydroxypoly(oxy-1,2-ethanediyl) (1:2), for use with glyphosate. mono-C12–16 alkyl ethers, (CAS Reg. No. 176022–82–5). Polysorbate 65, conforming to 21 CFR 172.838 ...... Emulsifier Potassium aluminum silicate ...... Solid diluent, carrier Potassium benzoate (Cas No. 582–25–2) ...... None ...... Preservative

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TABLE 1 TO 180.910—Continued

Inert ingredients Limits Uses

Potassium hydroxide ...... Neutralizer Potassium phosphate ...... Buffer Potassium sulfate ...... Solid diluent Propanamide, 2-hydroxy-N, N-dimethyl- (CAS Reg. Not to exceed 50% by Solvent/co-solvent No. 35123–06–9). weight in pesticide formulation. Propane ...... Propellant 1,3-Propanediol (CAS Reg. No. 504–63–2) ...... Solvent, co-solvent, diluent, or freeze-point depressant Propanoic acid, 2-methyl-, monoester with 2,2,4- ...... Solvent, co-solvent trimethyl-1,3-pentanediol (CAS Reg. No. 25265– 77–4). 2-Propanol, 1,1′,1″-nitrilotris- (CAS No. 122–20–3) Without limitation ...... Neutralizer n-Propanol ...... Solvent, cosolvent 2-Propenoic acid, 2-methyl-, polymer with ethyl 2- ...... Encapsulating agent, dispensers, resins, fi- propenoate and methyl 2-methyl-2-propenoate, bers and beads ammonium salt (CAS Registration No. 55989– 05–4), minimum number average molecular weight (in amu), 18,900.. Propyl gallate ...... Antioxidant Propyl p-hydroxybenzoate ...... Preservative for formulations Propylene glycol ...... Solvent, cosolvent Propylene glycol alginate (as defined in 21 CFR ...... Defoaming agent 172.858). Propylene glycol monomethyl ether (CAS No. 107– none ...... solvent 98–2). Pyrophyllite ...... Solid diluent, carrier Rhizobium inoculants (e.g. Sinorhizobium, ...... All leguminous food commodities Bradyrhizobium & Rhizobium). Rosin, partially dimerized (as defined in 21 CFR ...... Surfactants, related adjuvants of surfactants 172.615). Rosin, partially hydrogenated (as defined in 21 ...... Do. CFR 172.615). Rosin, wood ...... Do. Salicylaldehyde (CAS Reg. No. 90–02–8) ...... Not to exceed 14% by Penetration aid weight of pesticide formulation. Salts of fatty acids, conforming to 21 CFR 172.863 ...... Binder, emulsifier, anticaking agent Sand ...... Solid diluent, carrier Shellac, bleached; refined, food grade, arsenic and ...... Coating agent rosin-free. Silver nitrate (Cas Reg. No. 7761–88–8) ...... For use on potatoes as Stabilizer post-harvest treatment to control sprouting at no more than 0.06% by weight in pesticide formulations. Soapstone ...... Solid diluent Sodium acid pyrophosphate ...... Surfactant, suspending agent, dispersing agent, buffer Sodium alkyl naphthalenesulfonates (CAS Reg. Limited to no more than Surfactants, related adjuvants of surfactants Nos. 68909–83–1, 68909–84–2, 68909–82–0, 30% by weight in pes- 27213–90–7, 26264–58–4, 27178–87–6, ticide end-use products. 111163–74–7, 908356–16–1, 25417–20–3, 25638–17–9, 145578–88–7, 1322–93–6, 1323– 19–9, 7403–47–6, 68442–09–1, 127646–44–0, 908356–18–3). Sodium aluminum silicate ...... Solid diluent, carrier Sodium dioctylsulfosuccinate ...... Surfactants, related adjuvants of surfactants Sodium 1,4-dihexyl sulfosuccinate (CAS Reg. No...... Surfactants, related adjuvants of surfactants 3006–15–3). Sodium 1,4-diisobutyl sulfosuccinate (CAS Reg...... Surfactants, related adjuvants of surfactants No. 127–39–9). Sodium 1,4-dipentyl sulfosuccinate (CAS Reg. No...... Surfactants, related adjuvants of surfactants 922–80–5). Sodium Formate (CAS Reg. No. 141–53–7) ...... adjuvant, pH buffering agent Sodium DL-lactate (CAS Reg. No. 72–17–3) ...... Surfactant Sodium hexametaphosphate...... Surfactant, emulsifier, wetting agent, suspending agent, dispersing agent, buffer Sodium hydroxide ...... Neutralizer Sodium L-lactate (CAS Reg. No. 867–56–1) ...... Surfactant

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TABLE 1 TO 180.910—Continued

Inert ingredients Limits Uses

Sodium metasilicate ...... Surfactants, emulsifiers, wetting agents, dispersing agents, buffer Sodium monoalkyl and dialkyl (C6-C16) phenoxy Not to exceed 20% in pes- Surfactants, related adjuvants of surfactants benzenedisulfonates and related acids (CAS ticide formulations. Reg. Nos. 147732–59–0, 147732–60–3, 169662–22–0, 70191–75–2, 36445–71–3, 39354–74–0, 70146–13–3, 119345–03–8, 149119–20–0, 149119–19–7, 119345–04–9, 28519–02–0, 25167–32–2, 30260–73–2, 65143– 89–7, 70191–76–3). Sodium a-olefinsulfonate (sodium C14-C16) (Olefin ...... Surfactants, related adjuvants of surfactants sulfonate). SodiumN-oleoyl- N-methyl taurine (CAS Reg. No...... Surfactants, related adjuvants of surfactants 137–20–2). Sodium and potassium salts of N-alkyl (C8–C18)- Concentration in formu- Surfactants, related adjuvants of surfactants beta-iminodipropionic acid where the C8–C18 is lated end-use products linear and may be saturated and/or unsaturated not to exceed 30% by (CAS Reg. Nos. 110676–19–2, 3655–00–3, weight in pesticide for- 61791–56–8, 14960–06–6, 26256–79–1, 90170– mulations. 43–7, 91696–17–2, 97862–48–1). Sodium salt of sulfated oleic acid ...... Surfactants, related adjuvants of surfactants Sodium silicate ...... Surfactant, emulsifier, wetting agent, stabilizer, inhibitor Sodium starch glycolate (CAS Reg. No. 9063–38– Granular and tableted Disintegrant 1). products only; not to exceed 8% of the formulated product. Sodium sulfate ...... Solid diluent, carrier Sodium tripolyphosphate ...... Buffer, surfactant, suspending agent, dispersing agent, anticaking agent, conditioning agent Sorbic acid (CAS Reg. No. 110–44–1) ...... Preservative for formulations Sorbitan fatty acid esters (fatty acids limited to C12, ...... Surfactants, related adjuvants or surfactants. C14, C16, and C18 containing minor amounts of associated fatty acids) and their derivatives; the poly(oxyethylene) content averages 5-20 moles. Soybean flour ...... Expires May 24, 2005...... Surfactant Soybean oil-derived fatty acids ...... Solvent, cosolvent Stearic acid ...... Diluent a-Stearoyl-w-hydroxypoly(oxyethylene), average ...... Emulsifier molecular weight (in amu) of 600. a-Stearoyl-w-hydroxypoly(oxyethylene); the ...... Surfactants, related adjuvants of surfactants poly(oxyethylene) content averages either 8, 9, or 40 moles; if a blend of products is used, the average number of moles ethylene oxide reacted to produce any product that is a component of the blend shall be either 8, 9, or 40. Sucrose octaacetate ...... Adhesive Sulfite liquors and cooking liquors, spent, oxidized ...... Surfactant, related adjuvants of surfactants (CAS Reg. No. 68514–09–0). Sulfuric acid (CAS Reg. No.7664–93–9) ...... Not to exceed 10% of the pH Control agent pesticide formulation; non-aerosol formulations only. Sweet orange peel tincture (CAS Reg. No. 8028– Not to exceed 10% Surfactant, fragrance, related adjuvants of 48–6). (weight/weight) in pes- surfactants ticide formulation. Synthetic paraffin and its succinic derivatives con- ...... Carrier, binder, and carrying agent forming to 21 CFR 172.275. Synthetic petroleum wax, conforming to 21 CFR ...... Binder, carrier, and coating agent 172.888. Talc ...... Solid diluent, carriers Tall oil; fatty acids not less than 58%, rosin acids ...... Surfactants, related adjuvants of surfactants not more than 44%, unsaponifiables not more than 8%. Tall oil fatty acids (CAS Reg. No. 61790–12–3) ...... Solvent/carrier Tartrazine ...... Dye Terpenes and terpenoids, turpentine oil, alpha-pi- ...... Surfactants, related adjuvants of surfactants nene fraction, polymd. (CAS Reg. No. 70750– 57–1). 1,1,1,2-Tetrafluoroethane, (CAS Reg. No. 811–97– ...... Aerosol propellant 2).

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TABLE 1 TO 180.910—Continued

Inert ingredients Limits Uses

Trans-1,3,3,3-tetrafluoroprop-1-ene (CAS Reg. No...... Propellant 29118–24–9). Tetrahydrofurfuryl alcohol (THFA) (CAS Reg. No Expires February 9, 2008 Solvent/cosolvent 97–99–4). N,N,N′,N″,-tetrakis-(2-hydroxypropyl) ethylene- Concentration in formu- Stabilizer for formulation. diamine (CAS Reg. No. 102–60–3). lated end-use products not to exceed 20% by weight in pesticide formulations. a-[p-(1,1,3,3-tetramethylbutyl)phenyl]-w- Not to exceed 7% of pes- Surfactants related adjuvants of surfactants hydroxypoly(oxyethylene) produced by the con- ticide formulation. densation of 1 mole of p-(1,1,3,3- tetramethylbutyl)phenol with a range of 1–14 or 30–70 moles of ethylene oxide: If a blend of products is used, the average range number of moles of ethylene oxide reacted to produce any product that is a component of the blend shall be in the range of 1–14 or 30–70 (CAS Reg. Nos. 9036–19–5, 9002–93–1). 2,4,7,9-Tetramethyl-5-decyn-4, 7-diol ...... Not more than 2.5% of Surfactants, related adjuvants of surfactants pesticide formulation. Tetrasodium pyrophosphate ...... Anticaking agent, conditioning agent Thiosulfuric acid, disodium salt, anhydrous. (CAS ...... Dechlorinator, reducing agent Reg. No 7772–98–7). Thiosulfuric acid, disodium salt, pentahydrate...... Do. (CAS Reg. No. 10102–17–7). d-Alpha tocopherol (CAS Reg. No. 9–02–9 ...... None ...... Safener d-Alpha tocopheryl acetate (CAS Reg. No. 58–95– None ...... Do. 7). dl-Alpha tocopherol (CAS Reg. No.10191–41–0) ... None ...... Do. dl-Alpha tocopheryl acetate (CAS Reg. No. 7695– None ...... Do. 91–2). Tricalcium phosphate ...... Surfactant, suspending agent, dispersing agent, anticaking agent, conditioning agent Trisodium phosphate ...... Surfactant, emulsifier, wetting agent Vermiculite ...... Solid diluent, carrier. Vitamin E (CAS Reg. No. 1406–18–4) ...... None ...... Safener Walnut shells ...... Leaching inhibitor, binder for water-dispers- ible aggregates, sticker and suspension stabilizer Waxes and waxy substances, rice bran, oxidized ...... Flow aid, surface protectant, film-forming (CAS Reg. No. 1883583–80–9). agent, carrier, coating agent, or adjuvant Wintergreen oil ...... Attractant Wood flour ...... Derived from wood free of Solid diluent and carrier chemical preservatives. Xanthan gum-modified, produced by the reaction Not more than 0.5% of Surfactant of xanthan gum and glyoxal (maximum 0.3% by pesticide formulation. weight). Xylene meeting the specifications listed in 21 CFR In pesticide formulations Solvent, cosolvent 172.884(b)(4). for grain storage only. Zeolite (hydrated alkali aluminum silicate) ...... Solid diluent, carrier Zinc oxide (CAS Reg. No. 1314–13–2) ...... Not more than 15% by Coating agent, stabilizer weight in pesticide formulations when used as stabilizer. Zinc sulfate (basic and monohydrate) ...... Do. Zinc sulfate (basic and monohydrate) ...... Solid diluent, carrier

[69 FR 23117, Apr. 28, 2004]

EDITORIAL NOTE: For FEDERAL REGISTER citations affecting § 180.910, see the List of CFR Sections Affected, which appears in the Finding Aids section of the printed volume and at www.govinfo.gov.

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§ 180.920 Inert ingredients used pre- when used in accordance with good ag- harvest; exemptions from the re- ricultural practice as inert (or occa- quirement of a tolerance. sionally active) ingredients in pesticide The following materials are exempt- formulations applied to growing crops ed from the requirement of a tolerance only:

Inert ingredients Limits Uses

Acetophenone ...... Attractant Adenosine (CAS Reg. No. 58–61–7) ...... Maximum of 0.5% of formu- Synergist lation. Alder bark ...... Seed germination stimulator

Alkyl (C12-C16) dimethyl ammonio acetate (CAS 20% by weight in pesticide Surfactant Reg. Nos. 683–10–3, 2601–33–4 and 693– formulation. 33–4.

a-Alkyl (minimum C6 linear, branched, saturated Not to exceed 30% of pes- Surfactants, related adjuvants of surfactants and/or unsaturated)-w-hydroxypolyoxyethylene ticide formulation. polymer with or without polyoxypropylene, mixture of di- and monohydrogen phosphate esters and the corresponding ammonium, calcium, magnesium, monoethanolamine, potassium, sodium, and zinc salts of the phosphate esters; minimum oxyethylene content is 2 moles; minimum oxypropylene content is 0 moles (CAS Reg. Nos. 9046–01–9, 37280– 82–3, 39464–66–9, 42612–52–2, 50643–20– 4, 52019–36–0, 58318–92–6, 60267–55–2, 61837–79–4, 67711–84–6, 68070–99–5, 68071–35–2, 68071–17–0, 68130–47–2, 68186–37–8, 68186–36–7, 68311–02–4, 68425–73–0, 68458–48–0, 68511–37–5, 68610–65–1, 68585–36–4, 68649–29–6, 68815–11–2, 68908–64–5, 68891–13–4, 73038–25–2, 78330–24–2, 108818–88–8, 154518–39–5, 317833–96–8, 873662–29–4, 936100–29–7, 936100–30–0).

N-alkyl(C8-C18) dimethylamidopropylamines Not to exceed 20% by Surfactants, related adjuvants of surfactants where the alkyl group is linear and may be weight in herbicide formu- saturated and/or unsaturated (CAS Reg. Nos. lations. 109–28–4, 3179–80–4, 7651–02–7, 22890– 10–4, 22890–11–5, 39669–97–1, 45267–19– 4, 68140–01–2, 1147459–12–8, 146987–98– 6).

N-alkyl (C8-C18) primary amines and their ace- Concentration in formulated Surfactants, related adjuvants of surfactants tate salts where the alkyl group is linear and end-use products not to may be saturated and/or unsaturated (CAS exceed 10% by weight in Reg. Nos. 61790–57–6, 61790–58–7, 61790– herbicide products, 4% 59–8, 61790–60–1, 61788–46–3, 61790–33– by weight in insecticide 8, 68155–38–4). products, and 4% by weight in fungicide products. N,N-Bis-a-ethyl-w-hydroxypoly(oxy-1,2- Not to exceed 25% in herbi- Surfactants, related adjuvants of surfactants ethanediyl) C8–C18 saturated and unsatu- cide formulations and rated alkylamines; the poly(oxy-1,2-ethanediyl) 10% in insecticide and content is 2–60 moles (CAS Reg. Nos. fungicide formulations. 10213–78–2, 25307–17–9, 26635–92–7, 26635–93–8, 288259–52–9, 58253–49–9, 61790–82–7, 61791–14–8, 61791–24–0, 61791–26–2, 61791–31–9, 61791–44–4, 68155–33–9, 68155–39–5, 68155–40– 8,70955–14–5, 73246–96–5, 1266162–49–5). N,N–Bis-a-ethyl-w-hydroxypoly(oxy-1,2- Not to exceed 25% in herbi- Surfactants, related adjuvants of surfactants ethanediyl/oxy(methyl-1,2-ethanediyl) C8-C18 cide formulations and saturated and unsaturated alkylamines; the 10% in insecticide and poly(oxy-1,2-ethanediyl/oxy(methyl-1,2- fungicide formulations. ethanediyl) content is 2–60 moles (CAS Reg. Nos. 68213–26–3, 68153–97–9, 75601–76–2). Aluminum sulfate ...... Safener adjuvant Ammonium acetate (CAS No. 631–61–8) ...... 15% ...... Buffering Agent. Ammonium chloride (CAS Reg. No. 12125–02– ...... Carrier/nutrient 9). Ammonium formate (CAS Reg. No. 540–69–2) ...... Complexing or fixing agent Ammonium nitrate (CAS Reg. No. 6484–52–2) ...... Adjuvant/ intensifier for herbicides

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Inert ingredients Limits Uses

Ammonium polyphosphate (CAS Reg. No...... Sequestrant, buffer, or surfactant 68333–79–9). Quaternary ammonium compounds, Not to exceed 1.0% by Suspending or structuring agent benzylbis(hydrogenated tallow alkyl)methyl, weight of pesticide formu- bis(hydrogenated tallow alkyl)di- lation. methylammonium salts with saponite (CAS Reg. No. 1588523–05–0). Quaternary ammonium compounds, Not to exceed 2.0% by Suspending or structuring agent benzylbis(hydrogenated tallow alkyl)methyl, weight of pesticide formu- bis(hydrogenated tallow alkyl)di- lation, asbestos free and methylammonium salts with sepiolite (CAS containing less than 1% Reg. No. 1574487–61–8). crystalline silica. Barium sulfate ...... Carrier 1,4-Benzenedicarboxylic acid, dimethyl ester, For use in honeybee hive Component of controlled release agent polymer with 1,4-butanediol, adipic acid, and miticide formulations. hexamethylene diisocyanate, minimum number average molecular weight (in amu) 30,000 (CAS Reg. No. 55231–08–8). 1,2-Benzisothiazolin-3-one ...... Not more than 0.1% of for- Preservative/stabilizer mulation. Not more than 0.02 lb to be applied per acre. Benzyl acetate (CAS Reg. No. 140–11–4) ...... Solvent Beta Cyclodextrin, Methyl Ethers (CAS Reg. No. 40% by weight ...... Stabilizer and solvent 128446–36–6). Boric acid ...... Sequestrant Buffalo gourd root powder (Cucurbita No more than 2.5 lbs/acre/ Gustatory stimulant foetidissima root powder); or, Zucchini juice season (3.4 gm/acre/sea- (Cucurbita pepo juice) or Hawkesbury melon son of Cucurbitacin). Citrullus lanatus.. Butyl stearate ...... Defoamer g-Butyrolactone ...... Solvent C.I. Pigment Blue #15 (CAS Reg. No. 147–14– For seed treament use only Dye, coloring agent 8; containing no more than 50 ppm poly- chlorinated biphenyls (PCBs)). C.I. Pigment Green #7 (CAS Reg. No. 1328– For seed treatment use Dye, coloring agent 53–6; containing no more than 50 ppm poly- only. chlorinated biphenyls (PCBs)). C.I. Pigment Red #112 (CAS Reg. No. 6535– Seed treatment use only. Coloring agent 46–2). Limited to 10% w/w of pesticide formulation. C.I. Pigment Violet #23 (CAS Reg. No. 6358– For seed treatment use Dye, coloring agent 30–1; containing no more than 20 ppb of poly- only. chlorinated dibenzo-p-dioxins and/or poly- chlorinated dibenzofurans). C.I. Pigment Yellow 1 (CAS Reg. No. 2512–29– Not to exceed 10% (weight/ Colorant 0). weight) in pesticide formulation. Calcium formate (CAS Reg. No. 544–17–2) ...... Carrier Calcium gluconate (CAS Reg. No. 299–28–5) ...... Sequestrant Camphor (CAS Reg. No. 76–22–2) ...... Not more than 5% weight to Deodorant, melting point adjustment weight (w/w) of pesticide formulations. Carbon Black (CAS Reg. No. 1333–86–4) ...... For seed treatment use Colorant only. Carbonic acid, dipotassium salt (CAS Reg. No...... Buffering agent 584–08–7). Carbonic acid, dipotassium salt, trihydrate (CAS ...... Buffering agent Reg. No. 18662–52–7). Carboxymethyl guar gum sodium salt (CAS Without limitation ...... Thicker/drift reduction agent Reg. No. 39346–76–4). Carboxymethyl-hydroxypropyl guar (CAS Reg. Without limitation ...... Thicker/drift reduction agent No. 68130–15–4). Carous chloride ...... 10 ppm in formulation ...... Tagging agent Carrageenan, conforming to 21 CFR 172.260 .... Not more than 0.15% of Thickener and stabilizer for pesticide formula- pesticide formulation. tions applied to seeds before planting Chlorobenzene ...... Contains not more than 1% Solvent, cosolvent impurities. Not for use after edible parts of plant begin to form. Do not graze livestock in treated areas within 48 hours after application.

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Inert ingredients Limits Uses

5-Chloro-2-methyl-4-isothiazolin-3-one (in com- Not more than 0.0022% Preservative bination with 2-methyl-4-isothiazolin-3-one). (22.5 ppm) in the formulation; 0.00022% (or 2.25 ppm) in the final solution applied to growing crops. Choline chloride (CAS Reg. No. 67–48–1) ...... As a solvent Choline hydroxide (CAS Reg No. 123–41–1) ..... Without limitation ...... Neutralizer Cis-isomer of 1-(3-chloroallyl)-3,5,7-triaza-1- Maximum of 0.14% by Preservative azoniaadamantane chloride (CAS Reg. No. weight of formulation. 51229–78–8). Coco alkyl dimethyl amines (CAS Reg. No. Not to exceed 0.5% in pes- Emulsifier 61788–93–0). ticide formulation. Copper naphthenate ...... Not more than 2.5% of for- Mercaptan scavenger in technical pesticide mulation; application limited to before edible por- tions of plants begin to form. Cumene sulfonic acid and its ammonium, cal- ...... Surfactant, related adjuvant of surfactant cium, magnesium, potassium, sodium and zinc salts (CAS Reg. Nos. 15763–76–5, 16066–35–6, 164524–02–1, 28085–69–0, 28348–53–0, 28631–63–2, 32073–22–6, 37475–88–0, 37953–05–2, and 90959–88–9). Cyclohexane ...... Solvent, cosolvent Cyclohexanone ...... Do. Cysteine (CAS Reg. No. 52–90–4) ...... Maximum of 0.5% of formu- Synergist lation. D&C Green No. 6 ...... Dye D&C Red No. 17, technical grade ...... Dye D&C Red No. 33 (CAS Reg. No. 3567–66–6); ...... Dye meeting the specifications listed in 21 CFR 74.1333. D&C Violet No. 2, technical grade ...... Not more than 0.005% of Dye pesticide formulation. Decanamide, N,N-dimethyl (CAS Reg. No...... Emulsifier, solvent, cosolvent 14433–76–2). Diammonium phosphate (CAS Reg. No. 7783– ...... Buffer, surfactant 28–0). dibenzylidene sorbitol (32647–67–9) ...... Thinning agent Diethanolamine ...... Stabilizer, inhibitor for formulations used before crop emerges from soil

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Inert ingredients Limits Uses

Dimethylaminopropylamine, isopropylamine, eth- ...... Surfactants, related adjuvants of surfactants. anolamine, and triethanolamine salts of alkyl (C8-C24) benzenesulfonic acid (CAS Reg. Nos. 3088–30–0, 12068–12–1, 26264–05–1, 26836–07–7, 27323–41–7, 55470–69–4, 58089–99–9, 61886–59–7, 61931–76–8, 67924–05–4, 68110–32–7, 68259–35–8, 68411–31–4, 68442–72–8, 68567–69–1, 68584–24–7, 68584–25–8, 68648–81–7, 68648–96–4, 68649–00–3, 68815–30–5, 68815–35–0, 68910–32–7, 68953–93–5, 68953–98–0, 70528–84–6, 72391–21–0, 84961–74–0, 85480–55–3, 85480–56–4, 85995–82–0, 90194–42–6, 90194–53–9, 90194–54–0, 90194–55–1, 90218–09–0, 90218–11–4, 90218–35–2, 96687–54–6, 99924–49–9, 121617–08–1, 157966–96–6, 193562–36–6, 319926–68–6, 877677–48–0, 1093628–27–3). 3,6-Dimethyl-4-octyn-3,6-diol ...... In pesticide formulations, Surfactants, related adjuvants of surfactants for soil prior to planting or to plants before edible parts form. Dimethyl sulfoxide ...... Solvent or cosolvent for formulations used before crop emerges from soil or prior to formation of edible parts of food plants Dimethyl sulfoxide (CAS No. 67–68–5) ...... For pesticide formulations Solvent or co-solvent used before crop emerges from soil or prior to formation of edible parts of food plants; for pesticide formulations used after crop emerges but before harvest, provided that the potential for increased residues of the formulation’s active ingredient(s) in or on food commodities has been assessed. Dipotassium hydrogen phosphate ...... Buffering agent Dipropylene glycol monomethyl ether ...... Stabilizer Douglas-fir bark, ground ...... Solid diluent, carrier Dysprosium chloride ...... 10 ppm in formulation ...... Tagging agent 1,2-ethanediamine,N,N,N″, N″-tetramethyl-, poly- For use in pesticide formu- Adjuvant or water conditioner mer with 1,1′-oxybis[2-chloroethane] (CAS lations applied to cotton Reg. No. 31075–24–8). or wheat only. (S,S)–Ethylenediaminedisuccinic acid (CAS ...... Sequestrant or chelating agent Reg. No. 20846–91–7). Ethylene glycol ...... Antifreeze, deactivator for all pesticides used before crop emerges from soil and in herbicides before or after crop emerges Ethylene glycol (CAS Reg. No. 107–21–1) ...... Without limitation ...... Pesticide inert ingredient as a solvent, stabilizer and/or antifreeze. Ethylene glycol monobutyl ether ...... 2-Ethylhexanol ...... Cosolvent, defoamer, solvent for all pesticides used before crop emerges from soil and in herbicides before or after crop emerges Europic chloride ...... 10 ppm in formulation ...... Tagging agent FD&C Blue No. 1 (CAS Reg. No. 3844–45–9) ... For seed treatment use Dye, coloring agent only. FD&C Blue No. 1, methyl-polyethylene glycol For seed treatment use Dye, coloring agent derivative (CAS Reg. No. 9079–34–9). only; Number average molecular weight (in amu) is greater than 1,000; Not to exceed 5% of the formulated pesticide product. FD&C Blue No. 1, polyethylene glycol derivative For seed treatment use Dye, coloring agent (CAS Reg. No. 9079–33–8). only; Number average molecular weight (in amu) is greater than 1,000; Not to exceed 5% of the formulated pesticide product.

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Inert ingredients Limits Uses

FD&C Red No. 40 (CAS Reg. No. 25956–17–6) For seed treatment use Dye, coloring agent only. Not to exceed 2% by weight of the pesticide formulation. Ferric chloride ...... Not greater than 2% of suspending, dispersing agent, pesticide formulation Fluoroapatite ...... Solid diluent, carrier Folic acid (CAS Reg. No. 59–30–3) ...... Maximum of 0.5% of formu- Synergist lation. Gluconic acid (and sodium salt) ...... Sequestrant l-Glutamic acid (C5 H9 NO4´ CAS Reg. No. 56– Seet treatment use only ..... Plant nutrient 86–0). [alpha]-D-glucopyranoside, 2-ethylhexyl 6-O- ...... Surfactant [alpha]-D glucopyranosyl- (CAS Reg. No. 330980–61–5). [alpha]-D-glucopyranoside, 2-ethylhexyl (CAS ...... Surfactant Reg. No. 125590–73–0). Glutamine (CAS Reg. No. 56–85–9) ...... Maximum of 0.5% of formu- Synergist lation. Glycerol—propylene oxide polymer (CAS Reg...... Component in water-soluble film No. 25791–96–2). Glyceryl triacetate ...... Stabilizer Glyceryl tris-12-hydroxystearate ...... Flow control agent Glycine betaine (CAS Reg. No. 107–43–7) ...... Plant nutrient Graphite ...... Treatment aid for seeds Guar hydroxypropyltrimethylammonium chloride ...... Thickener/drift reduction agent (CAS Reg. No. 71329–50–5). Hexamethylenetetramine ...... Stabilizer for carriers in solid pesticide formulations 2-(2′-hydroxy-3′,5′-di-tert-amylphenyl) Maximum concentration of Ultraviolet (UV) stabilizer benzotriazole (CAS Reg. No. 25973–55–1). 0.6% in insecticide formulations applied to adzuki beans, canola, chickpeas, cotton, faba beans, field peas, lentils, linola, linseed, lucerne, lupins, mung beans, navy beans, pigeon peas, safflower, sunflower, and vetch. 2-Hydroxy-4-n-octoxybenzophenone (CAS Reg. Not more than 0.2 pt of Light stabilizer No. 1843–05–6). pesticide formulation. Hydroxypropyl guar gum ...... Thickener 2-Hydroxypropyl starch (CAS Reg. No. 9049– ...... Adjuvant 76–7). Isobornyl acetate ...... Solvent Isobutyl alcohol ...... Do. Isobutylene-butene copolymers ...... For soil application only ...... Binder Isooctadecanol ...... Not more than 2% of pes- Defoaming agent ticide formulation. Konjac glucomannan (CAS Reg. No. 37220–17– Not to exceed 1.0% by Thickener 0). weight in pesticide formulation. Lanthanum chloride ...... 10 ppm in formulation ...... Tagging agent. Magnesium nitrate (in combination with 2-meth- None ...... Preservation yl-4-isothiazolin-3-one and 5-chloro-2-methyl- 4-isothiazolin-3-one). Maleic acid ...... For pesticide formulations Stabilizer applied to apples with a minimum preharvest interval of 21 days. Maleic anhydride (CAS Reg. No. 108–31–6) ...... Not to exceed 3.5% in pes- Stabilizer ticide formulations; or for pesticide formulations applied to apples with a minimum preharvest interval of 21 days. Manganese carbonate ...... Plant nutrient D-mannose (CAS Reg. No. 3458–28–4) ...... Sequestrant, binder, filler Mesityl oxide ...... Not for use after edible Solvent, cosolvent parts of plant begin to form. Do not graze livestock in treated areas within 48 hours after application.

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Inert ingredients Limits Uses

Methionine (CAS Reg. No. 59–51–8) ...... Maximum of 0.5% of formu- Synergist lation. Methyl alcohol ...... Do. Methyl ethyl ketone ...... Surfactant Methyl p- hydroxybenzoate ...... Preservative for formulations Methyl isobutyl ketone ...... Solvent, cosolvent 2-Methyl-4-isothiazolin-3-one (in combination Not more than 0.0022% Preservative with 5-chloro-2-methyl-4-isothiazolin-3-one). (22.5 ppm) in the formulation; 0.00022% (or 2.25 ppm) in the final solution applied to growing crops. Mono-, di-, and trimethylnapthalenesulfonic ...... Surfactants, related adjuvants of surfactants acids and napthalenesulfonic acids formaldehyde condensates, ammonium and sodium salts (CAS Reg. Nos. 9008–63–3, 9069–80–1, 9084–06–4, 36290–04–7, 91078–68–1, 141959–43–5, 68425–94–5). Methyl oleate ...... Surfactant 2-Methyl-2,4-pentanediol ...... Solvent for formulations used before crop emerges from soil Methyl poly(oxyethylene)C8–C18 alkylammonium Concentration in formulated Surfactants, related adjuvants of surfactants chlorides where the poly(oxyethylene) content end use products not to is n = 2–15 and where C8–C18 alkyl is linear exceed 10% by weight in and may be saturated or unsaturated (CAS herbicide products and Reg. Nos. 3010–24–0, 18448–65–2, 70750– 5% by weight in all other 47–9, 22340–01–8, 67784–77–4, 64755–05– pesticide products. 1, 61791–10–4, 28724–32–5, 28880–55–9, 68187–69–9, 68607–27–2, 60687–90–3. N-Methylpyrrolidone (CAS Reg. No. 872-504) ...... Solvent, cosolvent Mixed phytosterols (consisting of campesterol, ...... Surfactant sitosterol and stigmasterol, with minor amounts of associated plant sterols) derived from edible vegetable oils. Mono- and bis-(1H, 1H, 2H, 2H-perfluoroalkyl) Not more than 0.5% of pes- Surfactant, related adjvants of surfactants phosphates where the alkyl group is even ticide formulation. Expires numbered and in the C6-C12 range. February 9, 2008. Mono- and dialkyl (C8-C18) methylated ammo- ...... Surfactants, related adjuvants of surfactants nium chloride compounds, where the alkyl group(s) (C8-C18) are derived from coconut, cottonseed, soya, tallow, or hogfat fatty acids. Morpholine 4-C6-12 Acyl Derivatives (CAS Reg...... As a solvent No. 887947–29–7). Nicotinamide (CAS Reg. No. 98–92–0) ...... Not to exceed 0.5% by Synergist, corrosion inhibitor weight of pesticide formulation as synergist; not to exceed 5% by weight of pesticide formulation as corrosion inhibitor. a-(p-Nonylphenyl)-w-hydroxypoly(oxyethylene); ...... Surfactant produced by the condensation of 1 mole of nonylphenol (nonyl group is a propylene trimer isomer) with an average of 4-14 or 30- 100 moles of ethylene oxide; if a blend of products is used, the average number of moles of ethylene oxide reacted to produce any product that is a component of the blend shall be in the range 4-14 or 30-100. Octanamide, N,N-dimethyl (CAS Reg. No...... Emulsifier, solvent, cosolvent 1118–92–9). a-Oleoyl-w-(oleoyloxy) poly(oxyethylene) derived ...... Component of defoamers from a-hydro-w-hydroxypoly(oxyethylene) (molecular weight 600 amu). Oxo-decyl acetate (CAS reg. No. 108419–33–6) ...... Solvent Oxo-heptyl acetate (CAS Reg. No. 90438–79–2) ...... Solvent Oxo-hexyl acetate (CAS Reg. No. 88230–35–7) ...... Solvent Oxo-nonyl acetate (CAS Reg. No. 108419–34– ...... Solvent 7). Oxo-octyl acetate (CAS Reg. No. 108419–32–5) ...... Solvent Oxo-tridecyl acetate (CAS Reg. No. 108419– ...... Solvent 35–8). Phenol ...... Solvent, cosolvent Phenol, 2-(2H-benzotriazol-2-yl)-6-dodecyl-4- Not more than 10% by UV stabilizer. methyl-, (CAS Reg. No. 23328–53–2). weight of pesticide formulations.

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Inert ingredients Limits Uses

Phenolsulfonic acid—formaldehyde—urea con- Applied to growing plants Dispersant surfactant densate and its sodium salt. only. (Phthalocyaninato (2)) copper; (C.I. pigment When used as a colorant in Coloring agent, pigment blue No. 15). low-density plastic films. Pigment red 48 ...... For seed treatment use Dye only. a-Pinene ...... Not more than 2% of formu- Stabilizer lation by weight. Poly(oxy-1,2-ethanediyl), a-isotridecyl-w- At a maximum of 10% in Surfactant methoxy (CAS Reg. No. 345642–79–7). formulation. Poly(oxy-1,2-ethanediyl), a-(3-carboxy-1- Not to exceed 0.125% for Surfactant. oxosulfopropyl)-w-hydroxy-, (C10–C12)-alkyl seed treatment use only. ethers, disodium salts, polyoxylene content averages 4–5 moles (CAS Reg. No. 68815– 56–5). Poly(oxy-1,2-ethanediyl), a-(3-carboxy-1- Not to exceed 0.125% for Surfactant oxosulfopropyl)-w-hydroxy-, (C10–C16)-alkyl seed treatment use only. ethers, disodium salts, polyoxyethylene content averages 5 moles (CAS Reg. No. 68954– 91–6). Poly(oxyethylene) adducts of mixed phytosterols ...... Surfactant, related adjuvants (such sterols to consist of campesterol, stigmasterol and sitosterol with minor amounts of associated plant sterols) derived from edible vegetable oils; polyoxyethylene content averaging 5-26 moles. Polyoxyethylene polyoxypropylene mono(di-sec- Limited to herbicide formu- Surfactants, related adjuvants of surfactants butylphenyl) ether (CAS Reg. No. 69029–39– lations only, and to no 6). more than 30% by weight in herbicide formulations intended for application to turf. Poly(oxyethylene) (5) sorbitan monooleate ...... Surfactants, related adjuvants of surfactants Polysorbate 60, conforming to 21 CFR 172.836 ...... Surfactant Potassium dihydrogen phosphate ...... Buffering agent 2-Propanamine, compound with a-phosphono-w- Not more than 15% in the Surfactant butoxypoly (oxy-1,2-ethanediyl) (2:1) (CAS formulated product. Reg. No. 431040–31–2). 2-Propanamine, compounds with polyethylene Not more than 15% in the Surfactant glycol dihydrogen phosphate C8–10- alkyl ether formulated product. (2:1) (CAS Reg. No. 431062–72–5). 1,2-Propanediol, 3-[3-[1, 3, 3, 3-tetramethyl-1- Not to exceed 5% by Antifoaming agent [(trimethylsilyl)oxy]-1-disiloxyanyl] propoxy]- weight of pesticide formu- (CAS Reg. No. 70280–68–1). lation. Propylene glycol monomethyl ether ...... Solvent Pyridoxine (CAS Reg. No. 65–23–6) ...... Maximum of 0.5% of formu- Synergist lation. 2-Pyrrolidinone, 1-butyl- (CAS Reg. No. 3470– Not to exceed 30% by Solvent/cosolvent 98–2). weight of pesticide formulation. Rosin, dark wood (as defined in 21 CFR ...... Surfactants, related adjuvants of surfactants 178.3870(a)(1)(v)). Rosin, gum ...... Do. Rosin, tall oil ...... Do. Scandium chloride ...... 10 ppm in formulation ...... Tagging agent Sodium bisulfate (CAS Reg. No. 7681–38–1) ...... Acidifying/buffering agent Sodium 1,4-dicyclohexyl sulfosuccinate ...... Surfactants, related adjuvants of surfactants Sodium 1,4-dihexyl sulfosuccinate (CAS Reg...... Surfactants, related adjuvants of surfactants No. 3006–15–3). Sodium dihydrogen phosphate (CAS Reg. No...... Buffering agent 7558–80–7) conforming to 21 CFR 182.6778. Sodium 1,4-diisobutyl sulfosuccinate (CAS Reg...... Surfactants, related adjuvants of surfactants No. 127–39–9). Sodium 1,4-dipentyl sulfosuccinate (CAS Reg...... Surfactants, related adjuvants of surfactants No. 922–80–5). Sodium metaborate ...... Sequestrant Sodium molybdate ...... Plant nutrient Sodium nitrate ...... Solid diluent Sodium nitrite ...... Not more than 3% of pes- Stabilizer, inhibitor. ticide formulation. Sodium o-phenylphenate ...... Not more than 0.1% of pes- Preservative for formulation ticide formulation. Sodium salt of the insoluble fraction of rosin ...... Surfactants, related adjuvants of surfactants

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Inert ingredients Limits Uses

Sodium salts of N-alkyl (C8-C18)-beta- Concentration in formulated Surfactants, related adjuvants of surfactants iminodipropionic acid where the C8-C18 is lin- end-use products not to ear and may be saturated and/or unsaturated exceed 30% by weight in (CAS Reg. Nos. 3655-00-3, 61791-56-8, pesticide formulations. 14960-06-6, 26256-79-1, 90170-43-7, 91696- 17-2, 97862-48-1). Sodium tetraborate ...... Not more than 2% of pes- Buffering agent; corrosion inhibitor ticide formulation. Sulfonic acids, C13-17-sec-alkane, sodium salts Not to exceed 40% by Surfactant (CAS Reg. No. 85711–69–9). weight in non-residential use pesticide formulation only. Sulfonic acids, C14-17-sec-alkane, sodium salts Not to exceed 40% by Surfactant (CAS Reg. No. 97489–15–1). weight in non-residential pesticide formulation only. Tallowamine, ethoxylated, mixture of dihydrogen Not to exceed 20% of pes- Surfactants, related adjuvants of surfactants phosphate and monohydrogen phosphate ticide formulation. esters and the corresponding ammonium, calcium, potassium, and sodium salts of the phosphate esters, where the poly(oxyethylene) content averages 2–20 moles (CAS Reg. No. 68308–48–5). Tannin ...... Dispersing agent Tertiary butylhydroquinone ...... Antioxidant 1-Tetradecanamine, N,N-dimethyl-, N-oxide ...... Component in water-soluble film (CAS Reg. No. 3332–27–2). Tetraethylene glycol (CAS Reg. No. 112–60–7) ...... Solvent N,N,N′,N″-Tetrakis-(2-hydroxypropyl) ethylene- Concentration in formulated Stabilizer for formulations diamine (CAS Reg. No. 102–60–3). end-use products not to exceed 20% by weight in pesticide formulations. 2,4,7,9-Tetramethyl-5-decyne 4,7-diol ...... In pesticide formulations, Surfactants, related adjuvants of surfactants for application to soil prior to planting or to plants before edible parts form. Tetrapotassium pyrophosphate (CAS Reg. No. Not to exceed 10% of for- Sequestrant, anticaking agent, conditioning 7320–345). mulation. agent Tin oxide (CAS Reg. No. 18282–10–5) ...... Not to exceed 40% by Colorant weight for use in seed treatment pesticide formulations only. Titanium dioxide (CAS Reg. No. 13463–67–7) ...... Pigment, colorant, carrier Toluenesulfonic acid and its ammonium, cal- ...... Solvent, cosolvent cium, magnesium, potassium, sodium, and zinc salts. Triethanolamine ...... Stabilizer, inhibitor for formulations used before crop emerges from soil Triethanolamine (CAS Reg. No. 102–71–6) ...... Stabilizer, inhibitor Triethylene glycol ...... Deactivator Triethyl phosphate ...... Stabilizer for formulations used before crop emerges from soil Trimethylolpropane (CAS Reg. No. 77–99–6) .... Not to exceed 15% by Component in water-soluble film weight of the film. a-[2,4,6-Tris[1-(phenyl)ethyl]phenyl]-w-hydroxy Not more than 15% of the Surfactant. poly(oxyethylene), the poly(oxyethylene) con- formulation. tent averages 4-150 moles). a-[2,4,6-Tris[1-(phenyl)ethyl]phenyl]-w-hydroxy Not more than 15% of the Do. poly(oxyethylene); mixture of monohydrogen formulation. and dihydrogen phosphate esters and the corresponding ammonium, calcium, magnesium, potassium, sodium, and zinc salts, the poly(oxyethylene) content averages 4-150 moles). a-[2,4,6-Tris[1-(phenyl)ethyl]phenyl]-w-hydroxy Not more than 15% of the Do. poly(oxyethylene) sulfate, and the cor- pesticide formulation. responding ammonium, calcium, magnesium, potassium, sodium, and zinc salts, the poly(oxyethylene) content averages 4-150 moles. Tryptophan (CAS Reg. No. 73–22–3) ...... Maximum of 0.5% of formu- Synergist lation. Valeric acid, normal ...... Not more than 2% in pes- Stenching agent or odorant ticide formulations. Xylene ...... Solvent, cosolvent

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Inert ingredients Limits Uses

Xylenesulfonic acid its ammonium calcium, mag- ...... Surfactants, related adjuvants of surfactants nesium, potassium, sodium, and zinc salts. Yucca extract from Yucca schidigera ...... Wetting agent Ytterbium chloride ...... 10 ppm in formulation ...... Tagging agent Yttrium chloride ...... 10 ppm in formulation ...... Tagging agent Zinc orthophosphate ...... Plant nutrient and safener Zinc stearate, conforming to 21 CFR 182.5994 ...... Flow control agent and 582.5994.

[69 FR 23124, Apr. 28, 2004]

EDITORIAL NOTE: For FEDERAL REGISTER citations affecting § 180.920, see the List of CFR Sections Affected, which appears in the Finding Aids section of the printed volume and at www.govinfo.gov.

§ 180.930 Inert ingredients applied to when used in accordance with good ag- animals; exemptions from the re- ricultural practice as inert (or occa- quirement of a tolerance. sionally active) ingredients in pesticide The following materials are exempt- formulations applied to animals: ed from the requirement of a tolerance

Inert ingredients Limits Uses

Acetic acid (CAS Reg. No. 64–19–7) ...... Not more than 0.5% of Catalyst pesticide formulation. Acetic anhydride ...... Solvent, cosolvent, stabilizer Acetone (Cas Reg. No. 67–64–1) ...... Solvent or cosolvent

Alcohols, C2–33, manuf. of, by-products from, ...... Solvent overheads (CAS Reg. No. 876065–86–0). Alkanoic and alkenoic acids, mono- and diesters of ...... Emulsifiers a-hydro-w-hydroxypoly(oxyethylene) with molecular weight (in amu) range of 200 to 6,000.

Alkyl (C8-C24) benzenesulfonic acid and its ammo- ...... Surfactants, emulsifier, related adjuvants of nium, calcium, magnesium, potassium, sodium, surfactants and zinc salts.

Alkyl (C12-C16) dimethyl ammonio acetate (CAS 20% by weight in pesticide Surfactant Reg. Nos. 683–10–3, 2601–33–4 and 693–33–4. formulation.

a-alkyl(C6- C15)-w-hydroxypoly(oxyethylene)sulfate, Not to exceed 30% of for- Surfactants, related adjuvants of surfactants. and its ammonium, calcium, magnesium, potas- mulation. sium, sodium, and zinc salts, poly(oxyethylene) content averages 2–4 moles (CAS Reg. Nos.: 3088–31–1, 3694–74–4, 9004–82–4, 9004–84– 6, 9021–91–4, 9086–52–6, 13150–00–0, 15826– 16–1, 25446–78–0, 26183–44–8, 27140–00–7, 27731–61–9, 27731–61–9, 27731–62–0, 32612– 48–9, 34431–25–9, 35015–74–8, 50602–06–7, 52286–18–7, 52286–19–8, 54116–08–4, 55901– 67–2, 61702–79–2, 61894–66–4, 62755–21–9, 63428–85–3, 63428–86–4, 63428–87–5, 65086– 57–9, 65086–79–5, 65104–74–7, 65122–38–5, 67674–66–2, 67762–19–0, 67762–21–4, 67845– 82–3, 67845–83–4, 67923–90–4, 68037–05–8, 68037–06–9, 68171–41–5, 68424–50–0, 68511– 39–7, 68585–34–2, 68610–66–2, 68611–29–0, 68611–55–2, 68649–53–6, 68890–88–0, 68891– 29–2, 68891–30–5, 68891–38–3, 69011–37–6, 73665–22–2, 75422–21–8, 78330–16–2, 78330– 17–3, 78330–25–3, 78330–26–4, 78330–27–5, 78330–28–6, 78330–29–7, 78330–30–0, 96130– 61–9, 106597–03–9, 110392–50–2, 119432–41– 6, 125301–88–4, 125301–89–5, 125301–92–0, 125736–54–1, 157707–85–2, 160104–51–8, 160901–27–9, 160901–28–0, 160901–29–1, 160901–30–4, 161025–28–1, 161074–79–9, 162063–19–6, 219756–63–5).

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Inert ingredients Limits Uses

a-alkyl (C12-C15)-w-hydroxypoly Not to exceed 20% of pes- Surfactant (oxypropylene)poly (oxyethylene)copolymers ticide formulations. (where the poly(oxypropylene) content is 3-60 moles and the poly(oxyethylene) content is 5-80 moles), the resulting ethoxylated propoxylated (C12-C15) alcohols having a minimum molecular weight (in amu) of 1,500, CAS Reg. No. 68551– 13–3. a-Alkyl-w-hydroxypoly (oxypropylene) and/or poly ...... Surfactants, related adjuvants of surfactants (oxyethylene) polymers where the alkyl chain contains a minimum of six carbons (CAS Reg. Nos.: 9002–92–0; 9004–95–9; 9004–98–2; 9005–00–9; 9035–85–2; 9038–29–3; 9038–43– 1; 9040–05–5; 9043–30–5; 9087–53–0; 25190– 05–0; 24938–91–8; 25231–21–4; 251553–55–6; 26183–52–8; 26468–86–0; 26636–39–5; 27252– 75–1; 27306–79–2; 31726–34–8; 34398–01–1; 34398–05–5; 37251–67–5; 37311–00–5; 37311– 01–6; 37311–02–7; 37311–04–9; 39587–22–9; 50861–66–0; 52232–09–4; 52292–17–8; 52609– 19–5; 57679–21–7; 59112–62–8; 60828–78–6; 61702–78–1; 61723–78–2; 61725–89–1; 61791– 13–7; 61791–20–6; 61791–28–4; 61804–34–0; 61827–42–7; 61827–84–7; 62648–50–4; 63303– 01–5; 63658–45–7; 63793–60–2; 64366–70–7; 64415–24–3; 64415–25–4; 64425–86–1; 65104– 72–5; 65150–81–4; 66455–14–9: 66455–15–0; 67254–71–1; 67763–08–0; 68002–96–0; 68002– 97–1; 68131–39–5; 68131–40–8; 68154–96–1; 68154–97–2; 68154–98–3; 68155–01–1; 68213– 23–0; 68213–24–1; 68238–81–3; 68238–82–4; 68409–58–5; 68409–59–6; 68439–30–5; 68439– 45–2; 68439–46–3; 68439–48–5; 68439–49–6; 68439–50–9; 68439–51–0; 68439–53–2; 68439– 54–3; 68458–88–8; 68526–94–3; 68526–95–4; 68551–12–2; 68551–13–3; 68551–14–4; 68603– 20–3; 68603–25–8; 68920–66–1; 68920–69–4; 68937–66–6; 68951–67–7; 68954–94–9; 68987– 81–5; 68991–48–0; 69011–36–5; 69013–18–9; 69013–19–0; 69227–20–9; 69227–21–0; 69227– 22–1; 69364–63–2; 70750–27–5; 70879–83–3; 70955–07–6; 71011–10–4; 71060–57–6; 71243– 46–4; 72066–65–0; 72108–90–8; 72484–69–6; 72854–13–8; 72905–87–4; 73018–31–2; 73049– 34–0; 74432–13–6; 74499–34–6; 78330–19–5; 78330–20–8; 78330–21–9; 78330–23–1; 79771– 03–2; 84133–50–6; 85422–93–1; 97043–91–9; 97953–22–5; 102782–43–4; 103331–86–8; 103657–84–7; 103657–85–8; 103818–93–5; 103819–03–0; 106232–83–1; 111905–54–5; 116810–31–2; 116810–32–3; 116810–33–4; 120313–48–6; 120944–68–5; 121617–09–2; 126646–02–4; 126950–62–7; 127036–24–2; 139626–71–4; 152231–44–2; 154518–36–2; 157627–86–6; 157627–88–8; 157707–41–0; 157707–43–2; 159653–49–3; 160875–66–1; 160901–20–2; 160901–09–7; 160901–19–9; 161025–21–4; 161025–22–5; 166736–08–9; 169107–21–5; 172588–43–1; 176022–76–7; 196823–11–7; 287935–46–0; 288260–45–7; 303176–75–2; 954108–36–2; 2222805–23–2).

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Inert ingredients Limits Uses

a-alkyl (minimum C6 linear, branched, saturated Not to exceed 30% of for- Surfactants, related adjuvants of surfactants. and/or unsaturated)-w-hydroxypolyoxyethylene mulation. polymer with or without polyoxypropylene, mixture of di- and monohydrogen phosphate esters and the corresponding ammonium, calcium, magnesium, monoethanolamine, potassium, sodium, and zinc salts of the phosphate esters; minimum oxyethylene content is 2 moles; minimum oxypropylene content is 0 moles, (CAS Reg. Nos.: 9004–80–2, 9046–01–9, 26982–05– 8, 31800–89–2, 37280–82–3, 37281–86–0, 39341–09–8, 39341–65–6, 39464–66–9, 39464– 69–2, 42612–52–2, 50643–20–4, 50668–50–3, 51325–10–1, 51884–64–1, 52019–36–0, 52019– 38–2, 52019–38–2, 57486–09–6, 58206–38–5, 58318–92–6, 58857–49–1, 59112–71–9, 60267– 55–2, 61837–79–4, 62362–49–6, 62482–61–5, 63747–86–4, 63887–54–7, 63887–55–8, 66020– 37–9, 66272–25–1, 66281–20–7, 67711–84–6, 67786–06–5, 67989–06–4, 68070–99–5, 68071– 17–0, 68071–35–2, 68071–37–4, 68130–44–9, 68130–45–0, 68130–46–1, 68130–47–2, 68186– 29–8, 68186–34–5, 68186–36–7, 68186–37–8, 68238–84–6, 68311–02–4, 68311–04–6, 68332– 75–2, 68389–72–0, 68400–75–9, 68413–78–5, 68425–73–0, 68425–75–2, 68439–39–4, 68458– 48–0, 68511–15–9, 68511–36–4, 68511–37–5, 68551–05–3, 68585–15–9, 68585–16–0, 68585– 17–1, 68585–36–4, 68585–39–7, 68603–24–7, 68607–14–7, 68610–64–0, 68610–65–1, 68649– 29–6, 68649–30–9, 68650–84–0, 68815–11–2, 68855–46–9, 68856–03–1, 68890–90–4, 68890– 91–5, 68891–12–3, 68891–13–4, 68891–26–9, 68908–64–5, 68909–65–9, 68909–67–1, 68909– 69–3, 68921–24–4, 68921–60–8, 68954–87–0, 68954–88–1, 68954–92–7, 68987–35–9, 69029– 43–2, 69980–69–4, 70247–99–3, 70248–14–5, 70844–96–1, 70903–63–8, 71965–23–6, 71965– 24–7, 72480–27–4, 72623–67–7, 72623–68–8, 72828–56–9, 72828–57–0, 73018–34–5, 73038– 25–2, 73050–08–5, 73050–09–6, 73361–29–2, 73378–71–9, 73378–72–0, 73559–42–9, 73559– 43–0, 73559–44–1, 73559–45–2, 74499–76–6, 76930–25–1, 78041–18–6, 78330–22–0, 78330– 24–2, 82465–25–6, 84843–37–8, 91254–26–1, 93925–54–3, 95014–34–9, 96416–89–6, 99924– 51–3, 103170–31–6, 103170–32–7, 106233–09– 4, 106233–10–7, 108818–88–8, 110392–49–9, 111798–26–6, 111905–50–1, 116671–23–9, 117584–36–8, 119415–05–3, 120913–45–3, 121158–61–0, 121158–63–2, 123339–53–7, 125139–13–1, 125301–86–2, 125301–87–3, 126646–03–5, 129208–04–4, 129870–77–5, 129870–80–0, 130354–37–9, 136504–88–6, 143372–50–3, 143372–51–4, 144336–75–4, 146815–57–8, 151688–56–1, 154518–39–5, 154518–40–8, 155240–11–2, 159704–69–5, 160498–49–7, 160611–24–5, 171543–66–1, 172027–16–6, 172274–69–0, 176707–42–9, 181963–82–6, 188741–55–1, 191940–53–1, 210493–60–0, 210993–53–6, 246159–55–7, 251298–11–0, 261627–68–3, 290348–69–5, 290348–70–8, 317833–96–8, 340681–28–9, 422563–19–7, 422563–26–6, 522613–09–8, 717140–06–2, 717140–09–5, 717827–29–7, 762245–80–7, 762245–81–8, 866538–89–8, 866538–90–1, 873662–29–4, 913068–96–9, 936100–29–7, 936100–30–0, 1072943–56–6, 1087209–87–7, 1174313–54–2, 1187742–89–7, 1187743–35–6, 1205632–03–6, 1233235–49–8, 1451002–50–8, 1456802–88–2, 1456802–89–3, 1456803–12–5).

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Inert ingredients Limits Uses

Alkyl (C8-C18) sulfate and its ammonium, calcium, ...... Surfactant magnesium, potassium, sodium, and zinc salts. N,N-Bis-a-ethyl-w-hydroxypoly(oxy-1,2-ethanediyl) Not to exceed 25% in her- Surfactants, related adjuvants of surfactants C8–C18 saturated and unsaturated alkylamines; bicide formulations and the poly(oxy-1,2-ethanediyl) content is 2–60 10% in insecticide and moles (CAS Reg. Nos. 10213–78–2, 25307–17– fungicide formulations. 9, 26635–92–7, 26635–93–8, 288259–52–9, 58253–49–9, 61790–82–7, 61791–14–8, 61791– 24–0, 61791–26–2, 61791–31–9, 61791–44–4, 68155–33–9, 68155–39–5, 68155–40–8,70955– 14–5, 73246–96–5, 1266162–49–5). N,N-Bis-a-ethyl-w-hydroxypoly(oxy-1,2-ethanediyl/ Not to exceed 25% in her- Surfactants, related adjuvants of surfactants oxy(methyl-1,2-ethanediyl) C8-C18 saturated and bicide formulations and unsaturated alkylamines; the poly(oxy-1,2- 10% in insecticide and ethanediyl/oxy(methyl-1,2-ethanediyl) content is fungicide formulations. 2–60 moles (CAS Reg. Nos. 68213–26–3, 68153–97–9, 75601–76–2). Ascorbyl palmitate ...... Preservative Attapulgite-type clay ...... Solid diluent, carrier Barium sulfate (CAS Reg. No. 7727–43–7) ...... Carrier, density control agent Benzoic acid ...... Preservative for formulations 2-Bromo-2-nitro-1,3-propanediol (CAS Reg. No. 0.04% or less by weight of In-can preservative 52–51–7). the total pesticide formulation. Butane ...... Propellant n-Butanol (CAS Reg. No. 71–36–3) ...... Solvent for blended emulsifiers n-Butyl benzoate (CAS RN 136–60–7) ...... Solvent n-Butyl-3-hydroxybutyrate (CAS Reg. No. 53605– ...... Solvent 94–0). Butylated hydroxyanisole ...... Antioxidant Butylated hydroxytoluene ...... Do. Calcium carbonate ...... Solid diluent, carrier Calcium chloride ...... Stabilizer Calcium silicate, hydrated calcium silicate ...... Anticaking agent, solid diluent, carrier

C9 rich aromatic hydrocarbons (CAS Reg. No...... Solvent 64742–95–6).

C10–11 rich aromatic hydrocarbons (CAS Reg. No...... Solvent 64742–94–5).

C11–12 rich aromatic hydrocarbons (CAS Reg. No...... Solvent 64742–94–5). Calcium stearate (CAS Reg. No. 1592–23–0) ...... Stabilizer, component of plastic animal tag Calcium sulfate ...... Solid diluent, carrier Carbon black (CAS Reg. No. 1333–86–4) ...... Colorant/pigment in animal tag Carbon Dioxide (CAS Reg. No. 124–38–9) ...... None ...... Propellant Carrageenan, conforming to 21 CFR 172.620 ...... Minimum molecular weight Thickener (in amu): 100,000. Cumene sulfonic acid and its ammonium, calcium, ...... Surfactant, related adjuvant of surfactant magnesium, potassium, sodium and zinc salts (CAS Reg. Nos. 15763–76–5, 16066–35–6, 164524–02–1, 28085–69–0, 28348–53–0, 28631–63–2, 32073–22–6, 37475–88–0, 37953– 05–2, and 90959–88–9). Cyclohexanone ...... Solvent, cosolvent D&C Green No. 6 ...... Dye, coloring agent D&C Red No. 17 ...... Do. D&C Violet No. 2 ...... Do.

Dialkyl (C8-C18) dimethylammonium chloride ...... Not more than 0.2% in sili- Flocculating agent in the manufacture of silica ca hydrated silica. hydrated silica for use as a solid diluent, carrier Diatomite (diatomaceous earth) ...... Solid diluent, carrier

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Inert ingredients Limits Uses

Diethanolamine salts of alkyl (C8-C24) Not to exceed 7% of pes- Surfactants, related adjuvants of surfactants. benzenesulfonic acid (CAS Reg. Nos. 26545– ticide formulation. 53–9, 67815–95–6, 67889–94–5, 67889–95–6, 68259–34–7, 68478–47–7, 68567–68–0, 68815– 34–9, 68815–37–2, 68891–02–1, 68953–97–9, 84989–15–1, 85338–09–6, 90194–39–1, 90194– 40–4, 90218–08–9). Diethylaminoethanol, ethoxylated, propoxylated, re- ...... Surfactant action products with fatty acid dimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173188–75–4). Diethylaminoethanol, ethoxylated, propoxylated, re- ...... Surfactant action products with fatty acid trimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173188–83–4). Diethylaminoethanol, ethoxylated, reaction prod- ...... Surfactant ucts with acid trimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173188–81–2). Diethylaminoethanol, ethoxylated, reaction product ...... Surfactant with fatty acid dimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173188–72–1). Diethylphthalate ...... Solvent, cosolvent 1,1-Difluoroethane (CAS Reg. No. 75–37–6) ...... In pesticide formulations Aerosol propellant used for insect control in food- and feed-handling establishments and animals; in bird repellent pesticide formulations. Dimethyl ether (CAS Reg. No. 115–10–6) ...... Propellant Dimethylaminoethanol, ethoxylated, propoxylated, ...... Surfactant reaction products with fatty acid dimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173188–42–5). Dimethylaminoethanol, ethoxylated, propoxylated ...... Surfactant reaction products with fatty acid trimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173188–67–4). Dimethylaminoethanol, ethoxylated, reaction prod- ...... Surfactant ucts with fatty acid trimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173188–38–9). Dimethylaminoethanol, ethoxylated, reaction prod- ...... Surfactant ucts with fatty acid trimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173188–49–2). Dimethylaminopropylamine, isopropylamine, etha- ...... Surfactants, related adjuvants of surfactants. nolamine, and triethanolamine salts of alkyl (C8- C24) benzenesulfonic acid (CAS Reg. Nos. 3088–30–0, 12068–12–1, 26264–05–1, 26836– 07–7, 27323–41–7, 55470–69–4, 58089–99–9, 61886–59–7, 61931–76–8, 67924–05–4, 68110– 32–7, 68259–35–8, 68411–31–4, 68442–72–8, 68567–69–1, 68584–24–7, 68584–25–8, 68648– 81–7, 68648–96–4, 68649–00–3, 68815–30–5, 68815–35–0, 68910–32–7 68953–93–5, 68953–98–0, 70528–84–6, 72391– 21–0, 84961–74–0, 85480–55–3, 85480–56–4, 85995–82–0, 90194–42–6, 90194–53–9, 90194– 54–0, 90194–55–1, 90218–09–0, 90218–11–4, 90218–35–2, 96687–54–6, 99924–49–9, 121617–08–1, 157966–96–6, 193562–36–6, 319926–68–6, 877677–48–0, 1093628–27–3).. 3,6-Dimethyl-4-octyne-3,6-diol ...... Not more than 2.5% of Surfactants, related adjuvants of surfactants pesticide formulation. Dimethylpolysiloxane (CAS Reg. No. 9016–00–6) ...... Defoaming agent Di-n-butyl carbonate (CAS Reg. No. 542–52–9) ...... Solvent Dipropylene glycol monomethyl ether ...... Surfactants, related adjuvants of surfactants Distillates (petroleum), solvent-dewaxed heavy par- ...... Carrier affinic (CAS Reg. No. 64742–65–0). Epoxidized soybean oil (CAS Reg. No. 8013–07– ...... Stabilizer, plasticizer, component animal tag 8).

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Inert ingredients Limits Uses

Ethanesulfonic acid, 2-hydroxy- (CAS Reg. No...... Chelator, sequestrant, or conditioning agent. 107–36–8). Ethanesulfonic acid, 2-hydroxy-, ammonium salts ...... Do. (CAS Reg. No. 57267–78–4). Ethanesulfonic acid, 2-hydroxy-, calcium salts ...... Do. (CAS Reg. No. 10550–47–7). Ethanesulfonic acid, 2-hydroxy-, magnesium salts ...... Do. (CAS Reg. No. 17345–56–1). Ethanesulfonic acid, 2-hydroxy-, potassium salts ...... Do. (CAS Reg. No. 1561–99–5). Ethanesulfonic acid, 2-hydroxy-, sodium salts (CAS ...... Do. Reg. No. 1562–00–1). Ethanesulfonic acid, 2-hydroxy-, zinc salts (CAS ...... Do. Reg. No. 129756–32–7). Ethyl alcohol ...... Solvent, cosolvent Ethyl maltol (CAS Reg. No.4940–11–8) ...... Not more than 0.2 % of Odor masking agent the pesticide formulation. Ethylene oxide adducts of 2,4,7,9-tetramethyl-5- ...... Surfactants, related adjuvants of surfactants decynediol, the ethylene oxide content averages 3.5, 10 or 30 moles (CAS Reg. No. 9014–85–1). 2-Ethyl-1-hexanol (CAS Reg. No. 104–76–7) ...... Not more than 10% of pes- Solvent, adjuvant of surfactants ticide. FD&C Blue No. 1 ...... Dye, coloring agent FD&C Yellow No. 6 Aluminum Lake (CAS Reg. Not more than 2% by Pigment in animal tag and similar slow-re- No. 15790–07–5). weight of pesticide for- lease devices mulation. Formic Acid (CAS Reg. No. 64–18–6) ...... 25% ...... pH adjuster. D-glucitol, 1,4:3,6-dianhydro-2,5-di-O-methyl-(CAS ...... solvent, co-solvent, viscosity modifier, and Reg. No. 5306–85–4); D-glucitol, 1,4:3,6- adjuvant dianhydro-2,5-di-O-ethyl- (CAS Reg. No. 30915– 81–2); D-glucitol, 1,4:3,6-dianhydro-2,5-di-O- propyl) (CAS Reg. No.107644–13–3); D-glucitol, 1,4:3,6-dianhydro-2,5-bis-O-(1-methylethyl)-,(isopropyl diether) (CAS Reg. No. 103594–41–8); D- glucitol, 1,4:3,6-dianhydro-2,5-di-O-butyl- (CAS Reg. No. 103594–42–9); D-glucitol, 1,4:3,6- dianhydro-2,5-di-O-(1-methylpropyl)-, (CAS Reg. No. not assigned); and D-glucitol, 1,4:3,6- dianhydro-2,5-di-O-(2-methylpropyl)-, (CAS Reg. No. not assigned). D-glucopyranose, oligomeric, C10–16-alkyl ...... Surfactant glycosides (CAS Reg. No. 110615–47–9). Glycerol monooleate ...... Surfactants, related adjuvants of surfactants Glyceryl monostearate ...... Emulsifier Glyceryl tris-12-hydroxystearate ...... Flow control agent Graphite ...... Solid diluent, carrier n-Hexyl alcohol (CAS Reg. No. 111–27–3) ...... Solvent, cosolvent Hydroxyethylmorpholine, ethoxylated, ...... Surfactant propoxylated, reaction products with fatty acid dimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173189– 06–4). Hydroxyethylmorpholine, ethoxylated, ...... Surfactant propoxylated, reaction products with fatty acid trimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173188– 67–4). Hydroxyethylmorpholine, ethoxylated, reaction ...... Surfactant products with fatty acid dimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173189–00–8). Hydroxyethylmorpholine, ethoxylated, reaction ...... Surfactant products with fatty acid trimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173189–09–7). Hydroxyethylpiperidine, ethoxylated, propoxylated, ...... Surfactant reaction products with fatty acid dimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173189–22–4). Hydroxyethylpiperidine, ethoxylated, propoxylated, ...... Surfactant reaction products with fatty acid trimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173189–28–0).

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Inert ingredients Limits Uses

Hydroxyethylpiperidine, ethoxylated, reaction prod- ...... Surfactant ucts with fatty acid dimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173189–20–2). Hydroxyethylpiperidine, ethoxylated, reaction prod- ...... Surfactant ucts with fatty acid trimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173189–25–7). 2-(2′-Hydroxy-5′-methylphenyl)benzotriazole (CAS Not more than 0.5% by Ultraviolet light absorber/stabilizer in animal Reg. No. 2440–22–4). weight of pesticide for- tag and similar slow-release devices mulation. Iron oxide (CAS Reg. No. 1309–37–1) ...... Colorant in pesticide formulations for animal tags Isobutane (CAS Reg. No. 75–28–5) ...... None ...... Propellant Isopropyl-3-hydroxybutyrate (CAS Reg. No...... Solvent 54074–94–1). Isopropyl myristate, CAS Reg. No. 110–27–0 ...... Solvent Kaolinite-type clay ...... Solid diluent, carrier Kerosene, U.S.P. reagent ...... Solvent, cosolvent Lactic acid ...... Solvent Lactic acid, 2-ethylhexyl ester (CAS Reg. No...... Solvent 6283–86–9). Lactic acid, 2-ethylhexyl ester, (2S)- (CAS Reg...... Solvent No. 186817–80–1). Lactic acid, n-propyl ester, (S); (CAS Reg. No...... Solvent 53651–69–7). Lignin (CAS Reg. No. 9005–53–2) ...... Surfactant, related adjuvants of surfactants Lignin, alkali (CAS Reg. No. 8068–05–1) ...... Do. Lignin, alkali, oxidized, sodium salt (CAS Reg. No...... Do. 68201–23–0). Lignin alkali reaction products with disodium sulfite ...... Do. and formaldehyde (CAS Reg. No. 105859–97–0). Lignin alkali reaction products with formaldehyde ...... Do. and sodium bisulfite (CAS Reg. No. 68512–35– 6). Lignosulfonic acid (CAS Reg. No. 8062–15–5) ...... Do. Lignosulfonic acid, ammonium calcium salt (CAS ...... Do. Reg. No. 12710–04–2). Lignosulfonic acid, ammonium magnesium salt ...... Do. (CAS Reg. No. 123175–37–1). Lignosulfonic acid, ammonium salt (CAS Reg. No...... Do. 8061–53–8). Lignosulfonic acid, ammonium sodium salt (CAS ...... Do. Reg. No. 166798–73–8). Lignosulfonic acid, calcium magnesium salt (CAS ...... Do. Reg. No. 55598–86–2). Lignosulfonic acid, calcium salt (CAS Reg. No...... Do. 8061–52–7). Lignosulfonic acid, calcium sodium salt (CAS Reg...... Do. No. 37325–33–0). Lignosulfonic acid, ethoxylated, sodium salt (CAS ...... Do. Reg. No. 68611–14–3). Lignosulfonic acid, magnesium salt (CAS Reg. No...... Do. 8061–54–9). Lignosulfonic acid, potassium salt (CAS Reg. No...... Do. 37314–65–1). Lignosulfonic acid, sodium salt (CAS Reg. No...... Do. 8061–51–6). Lignosulfonic acid, sodium salt, oxidized (CAS ...... Do. Reg. No. 68855–41–4). Lignosulfonic acid, sodium salt, polymer with form- ...... Do. aldehyde and phenol (CAS Reg. No. 37207–89– 9). Lignosulfonic acid, sodium salt, sulfomethylated ...... Do. (CAS Reg. No. 68512–34–5). Lignosulfonic acid, zinc salt (CAS Reg. No. 57866– ...... Do. 49–6). d-Limonene (CAS Reg. No. 5989–27–5) ...... Solvent, fragrance Magnesium carbonate ...... Solid diluent, carrier Magnesium silicate, hydrated magnesium silicate ...... Do. Methane sulfonic acid (CAS Reg. No. 75–75–2) .... Not to exceed 3.0% by Acidifying agent weight in pesticide formulation. Methyl alcohol ...... Solvent, cosolvent

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Inert ingredients Limits Uses

Methyl n-amyl ketone (CAS Reg. No. 110–43–0) ...... Solvent, cosolvent Methyl esters of higher fatty acids conforming to ...... Antidusting agent 21 CFR 573.640. Methyl-p-hydroxybenzoate (Methyl paraben) ...... Meets specifications of Preservative Food Chemicals Codex; not to exceed 0.1% in formulations. Methyl isobutyl ketone ...... Solvent, cosolvent 2-methyl-2,4-pentanediol (CAS Reg. No.–107–41– Without limitation ...... Growing crops and food animals 5). 2-methyl-1,3-propanediol (CAS Reg. No. 2163–42– ...... Solvent, surfactant 0). Mineral oil, U.S.P., or conforming to 21 CFR ...... Solvent, diluent 172.878 or 178.3620(a), (b). Montmorillonite-type clay ...... Solid diluent, carrier Nonyl, decyl, and undecyl glycoside mixture with a ...... Surfactant mixture of nonyl, decyl, and undecyl oligosaccharides and related reaction products (primarily decanol and undecanol) produced as an aqueous-based liquid (50 to 65% solids) from the reaction of primary alcohols (containing 15 to 20% secondary alcohol isomers) in a ratio of 20% C9, 40% C10, and 40% C11 with carbo- hydrates (average glucose to alkyl chain ratio 1.3 to 1.8). a-(p-Nonylphenol)-w-hydroxypoly(oxyethylene) mix- Not to exceed 7% of pes- Surfactants, related adjuvants of surfactants ture of dihydrogen phosphate and ticide formulation. monohydrogen phosphate esters and the corresponding ammonium, calcium, magnesium, potassium, sodium, and zinc salts of the phosphate esters; the nonyl group is a propylene trimer isomer and the poly(oxyethylene) content averages 4–14 or 30 moles (CAS Reg. Nos. 51811–79–1, 59139–23–0, 67922–57–0, 68412– 53–3, 68553–97–9, 68954–84–7, 99821–14–4, 152143–22–1, 51609–41–7, 37340–60–6, 106151–63–7, 68584–47–4, 52503–15–8, 68458–49–1). a-(p-Nonylphenol)-w-hydroxypoly(oxyethylene) sul- Not to exceed 7% of pes- Surfactants, related adjuvants of surfactants fate, ammonium, calcium, magnesium, potas- ticide formulation. sium, sodium, and zinc salts the nonyl group is propylene trimer isomer and the poly(oxyethylene) content averages 4 moles (CAS Reg. Nos. 9014–90–8, 9051–57–4, 9081– 17–8, 68649–55–8, 68891–33–8. a-(p-Nonylphenyl)-w-hydroxypoly(oxyethylene) pro- ...... Surfactants, emulsifier, related adjuvants of duced by the condensation of 1 mole of surfactants. nonylphenol (nonyl group is a propylene trimer isomer) with an average of 4-15 or 30-90 moles of ethylene oxide; if a blend of products is used, the average number of moles of ethylene oxide reacted to produce any product that is a component of the blend shall be in the range of 4-15 or 30-90 moles. Octadecyl 3,5-di-tert-butyl-4-hydroxyhydro Not more than 0.5% by Thermal stabilizer/antioxidant in animal tag cinnamate (CAS Reg. No. 2082–79–3). weight of pesticide for- and similar slow-release devices mulation. 1-Octanal (CAS Reg. No. 124–13–0) ...... Not more than 0.2% of the Odor masking agent pesticide formulation. Octyl and decyl glucosides mixture with a mixture ...... Thermal stabilizer/antioxidant in animal tag of octyl and decyl oligosaccharides and related and similar slow-release devices reaction products (primarily n-decanol) produced as an aqueous-based liquid (68-72% solids) from the reaction of straight chain alcohols (C8(45%), C10) with anhydrous glucose. Octyl epoxytallate (CAS Reg. No. 61788–72–5) ...... Plasticizer, component animal tag Oleic acid, conforming to 21 CFR 172.862 (CAS ...... Defoaming agent Reg. No. 112–80–1). a-Oleoyl-w-hydroxypoly(oxyethylene), average mo- ...... Emulsifier lecular weight (in amu) of 600. a-Oleoyl-w-(oleyloxy)poly(oxyethylene) derived ...... Emulsifier, defoaming agent from a-hydro-w-hydroxypoly(oxyethylene), molecular weight (in amu) 600.

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Inert ingredients Limits Uses

Pentaerythritol tetrakis (3-(3,5-di-tert-butyl-4- Not to exceed 3% by Antioxidant, stabilizer. hydroxyphenyl)propionate) (CAS Reg. No. 6683– weight of the pesticide 19–8). formulation. Petroleum hydrocarbons, light, odorless, con- ...... Solvent, diluent forming to 21 CFR 172.884 or 178.3650. Petroleum hydrocarbons, synthetic isoparaffinic, ...... Do. conforming to 21 CFR 172.882 or 178.3530. Phenol ...... Solvent, cosolvent a-Pinene ...... Not more than 2% of for- Stabilizer mulation by weight. Polyethylene (CAS Reg. No. 9002–88–4) con- ...... Component of plastic slow release tag forming to 21 CFR 172.615. Polyethylene glycol [a-hydro-w- ...... Surfactants, related adjuvants of surfactants hydroxypoly(oxyethylene)]; mean molecular weight (in amu) 194 to 9,500 conforms to 21 CFR 178.3750. Poly(oxy-1,2-ethanediyl), a-(3-(1,3,3,3-tetramethyl- ...... Surfactant 1-((trimethylsilyl) oxy) disiloxanyl) propyl)-w- hydroxy- (CAS Reg. No. 67674–67–3). Potassium benzoate (Cas No. 582–25–2) ...... None ...... Preservative Potassium hydroxide ...... Meeting Food Chemicals, Neutralizer Codex specifications. Propanamide, 2-hydroxy-N, N-dimethyl- (CAS Reg. Not to exceed 50% by Solvent/co-solvent No. 35123–06–9). weight in pesticide formulation. Propane ...... Propellant 1,2,3-Propanetriol, homopolymer ...... Emulsifier diisooctadecanoate (CAS Reg. No. 63705–03–3). n-Propanol ...... Solvent, for blended emulsifiers 2-Propenoic acid, 2-methyl-, polymer with ethyl 2- ...... Encapsulating agent,dispensers, resins, fibers propenoate and methyl 2-methyl-2-propenoate, and beads ammonium salt (CAS Registration No. 55989– 05–4), minimum number average molecular weight (in amu), 18,900.. Propylene glycol ...... Solvent, cosolvent Propylene glycol monomethyl ether ...... Deactivator, emmolient Propyl gallate ...... Antioxidant Propyl p-hydroxybenzoate (Propyl paraben) ...... Meets specifications of Preservative Food Chemicals Codex; not to exceed 0.1% in formulations. Pyrophylite ...... Solid diluent, carrier Silica, hydrated silica ...... Anticaking agent, solid diluent, carrier Silica aerogel (finely powdered microcellular silica ...... Component of antifoaming agent foam having a minimum silica content of 89.5%). Soapstone ...... Solid diluent Sodium alkyl naphthalenesulfonates (CAS Reg. Limited to no more than Surfactants, related adjuvants of surfactants Nos. 68909–83–1, 68909–84–2, 68909–82–0, 30% by weight in pes- 27213–90–7, 26264–58–4, 27178–87–6, ticide end-use products. 111163–74–7, 908356–16–1, 25417–20–3, 25638–17–9, 145578–88–7, 1322–93–6, 1323– 19–9, 7403–47–6, 68442–09–1, 127646–44–0, 908356–18–3). Sodium 1,4-dihexyl sulfosuccinate (CAS Reg. No...... Surfactants, related adjuvants of surfactants 3006–15–3). Sodium 1,4-diisobutyl sulfosuccinate (CAS Reg...... Surfactants, related adjuvants of surfactants No. 127–39–9). Sodium dioctylsulfosuccinate ...... Surfactants, related adjuvants of surfactants Sodium 1,4-dipentyl sulfosuccinate (CAS Reg. No...... Surfactants, related adjuvants of surfactants 922–80–5). Sodium hydroxide ...... Neutralizer Sodium monoalkyl and dialkyl (C6-C16) phenoxy Not to exceed 20% in pes- Surfactants, related adjuvants of surfactants benzenedisulfonates and related acids (CAS ticide formulations. Reg. Nos. 147732–59–0, 147732–60–3, 169662–22–0, 70191–75–2, 36445–71–3, 39354–74–0, 70146–13–3, 119345–03–8, 149119–20–0, 149119–19–7, 119345–04–9, 28519–02–0, 25167–32–2, 30260–73–2, 65143– 89–7, 70191–76–3). Sodium N-oleoyl-N-methyl taurine (CAS Reg. No...... Surfactants, related adjuvants of surfactants 137–20–2).

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Inert ingredients Limits Uses

Sodium and potassium salts of N-alkyl (C8–C18)- Concentration in formu- Surfactants, related adjuvants of surfactants beta-iminodipropionic acid where the C8–C18 is lated end-use products linear and may be saturated and/or unsaturated not to exceed 30% by (CAS Reg. Nos. 110676–19–2, 3655–00–3, weight in pesticide for- 61791–56–8, 14960–06–6, 26256–79–1, 90170– mulations. 43–7, 91696–17–2, 97862–48–1). Sodium starch glycolate (CAS Reg. No. 9063–38– Granular and tableted Disintegrant 1). products only; not to exceed 8% of the formulated product. Sodium sulfate ...... Solid diluent, carrier Sorbitan fatty acid esters (fatty acids limited to C12, ...... Buffering agent; corrosion inhibition C14, C16, and C18 containing minor amounts of associated fatty acids) and poly(oxyethylene) derivatives of sorbitan fatty acid esters; the poly(oxyethylene) content averages 16-20 moles. Sorbitol ...... Antidusting agent. Stearic acid (CAS Reg. No. 57–11–4) ...... Lubricant, component animal tag a-Stearoyl-w-hydroxypoly(oxyethylene), average ...... Emulsifier molecular weight (in amu) of 600. a-Stearoyl-w-hydroxypoly(oxyethylene); the ...... Surfactants; related adjuvants of surfactants poly(oxyethylene) content averages 8, 9, or 40 moles; if a blend of products is used, the average number of moles of ethylene oxide reacted to produce any product that is a component of the blend shall be 8, 9, or 40. Sulfite liquors and cooking liquors, spent, oxidized ...... Surfactant, related adjuvants of surfactants (CAS Reg. No. 68514–09–0). Sulfur (CAS Reg. No. 7704–34–9) ...... Stabilizer Talc ...... Do. Tall oil; fatty acids not less than 58%, rosin acids ...... Surfactants, related adjuvants of surfactants not more than 44%, unsaponifiables not more than 8%. Tall oil fatty acids (CAS Reg. No. 61790–12–3) ...... Solvent/carrier Tartrazine ...... Dye, coloring agent N,N,N′,N″,-tetrakis-(2-hydroxypropyl) ethylene- Concentration in formu- Stabilizer for formulation. diamine (CAS Reg. No. 102–60–3). lated end-use products not to exceed 20% by weight in pesticide formulations. Trans-1,3,3,3-tetrafluoroprop-1-ene (CAS Reg. No...... Propellant. 29118–24–9). 2,4,7,9-Tetramethyl-5-decyne-4.7-diol ...... Not more than 2.5% of Surfactants, related adjuvants of surfactants pesticide formulation. Titanium dioxide (CAS Reg. No. 13463–67–7) ...... Pigment/colorant in pesticide formulations for animal tag Toluenesulfonic acid and its ammonium, calcium, ...... Do. magnesium, potassium, sodium, and zinc salts. Triacetin (glyceryl triacetate) ...... Solvent, cosolvent Trisodium phosphate ...... Precipitant, buffer, filler Waxes and waxy substances, rice bran, oxidized ...... Flow aid, surface protectant, film-forming (CAS Reg. No. 1883583–80–9). agent, carrier, coating agent, or adjuvant Xylene ...... Solvent, cosolvent Xylenesulfonic acid and its ammonium, calcium, ...... Surfactants, related adjuvants of surfactants magnesium, potassium, sodium, and zinc salts. Zinc oxide ...... Solid diluent, carrier Zinc stearate, conforming to 21 CFR 182.5994 and ...... Water repellant, dessicant, and coating agent. 582.5994. Zinc stearate (CAS Reg. No. 557–05–1) ...... Water repellant, desiccant, and coating agent; stabilizer, component of plastic animal tag Zinc sulfate (basic and monohydrate) ...... Water repellant, dessicant, and coating agent

[69 FR 23130, Apr. 28, 2004]

EDITORIAL NOTE: For FEDERAL REGISTER citations affecting § 180.930, see the List of CFR Sections Affected, which appears in the Finding Aids section of the printed volume and at www.govinfo.gov.

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§ 180.940 Tolerance exemptions for ac- semi-permanent or permanent food- tive and inert ingredients for use in contact surface (other than being ap- antimicrobial formulations (Food- plied on food packaging) with adequate contact surface sanitizing solu- draining before contact with food. tions). (a) The following chemical sub- Residues of the following chemical stances when used as ingredients in an substances are exempted from the re- antimicrobial pesticide formulation quirement of a tolerance when used in may be applied to: Food-contact sur- accordance with good manufacturing faces in public eating places, dairy- practice as ingredients in an anti- processing equipment, and food-proc- microbial pesticide formulation, provided that the substance is applied on a essing equipment and utensils.

Pesticide Chemical CAS Reg. No. Limits

Acetic acid ...... 64–19–7 ...... When ready for use, the end-use concentration is not to exceed 100 ppm Alkylbenzene sulfonates (branched and linear) of chain 27176–87–0 ...... When ready for use, the end-use concentration is not lengths C10-C16, including benzenesulfonic acid, dodecyl 25155–30–0 to exceed 700 ppm and benzenesulfonic acid, dodecyl-, sodium salt. Allyl cylcohexylpropionate ...... 2705–87–5 ...... When ready for use, the end-use concentration is not to exceed 100 ppm

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Pesticide Chemical CAS Reg. No. Limits

a-Alkyl-w-hydroxypoly (oxypropylene) and/or poly (oxy- 9002–92–0; 9004–95–9; 9004– None ethylene) polymers where the alkyl chain contains a min- 98–2; 9005–00–9; 9035–85– imum of six carbons. 2; 9038–29–3; 9038–43–1; 9040–05–5; 9043–30–5; 9087–53–0; 25190–05–0; 24938–91–8; 25231–21–4; 251553–55–6; 26183–52–8; 26468–86–0; 26636–39–5; 27252–75–1; 27306–79–2; 31726–34–8; 34398–01–1; 34398–05–5; 37251–67–5; 37311–00–5; 37311–01–6; 37311–02–7; 37311–04–9; 39587–22–9; 50861–66–0; 52232–09–4; 52292–17–8; 52609–19–5; 57679–21–7; 59112–62–8; 60828–78–6; 61702–78–1; 61723–78–2; 61725–89–1; 61791–13–7; 61791–20–6; 61791–28–4; 61804–34–0; 61827–42–7; 61827–84–7; 62648–50–4; 63303–01–5; 63658–45–7; 63793–60–2; 64366–70–7; 64415–24–3; 64415–25–4; 64425–86–1; 65104–72–5; 65150–81–4; 66455–14–9: 66455–15–0; 67254–71–1; 67763–08–0; 68002–96–0; 68002–97–1; 68131–39–5; 68131–40–8; 68154–96–1; 68154–97–2; 68154–98–3; 68155–01–1; 68213–23–0; 68213–24–1; 68238–81–3; 68238–82–4; 68409–58–5; 68409–59–6; 68439–30–5; 68439–45–2; 68439–46–3; 68439–48–5; 68439–49–6; 68439–50–9; 68439–51–0; 68439–53–2; 68439–54–3; 68458–88–8; 68526–94–3; 68526–95–4; 68551–12–2; 68551–13–3; 68551–14–4; 68603–20–3; 68603–25–8; 68920–66–1; 68920–69–4; 68937–66–6; 68951–67–7; 68954–94–9; 68987–81–5; 68991–48–0; 69011–36–5; 69013–18–9; 69013–19–0; 69227–20–9; 69227–21–0; 69227–22–1; 69364–63–2; 70750–27–5; 70879–83–3; 70955–07–6; 71011–10–4; 71060–57–6; 71243–46–4; 72066–65–0; 72108–90–8; 72484–69–6; 72854–13–8; 72905–87–4; 73018–31–2; 73049–34–0; 74432–13–6; 74499–34–6; 78330–19–5; 78330–20–8; 78330–21–9; 78330–23–1; 79771–03–2; 84133–50–6; 85422–93–1; 97043–91–9; 97953–22–5; 102782–43–4; 103331–86–8; 103657–84–7; 103657–85–8; 103818–93–5; 103819–03–0; 106232–83–1; 111905–54–5; 116810–31–2; 116810–32–3; 116810–33–4; 120313–48–6; 120944–68–5; 121617–09–2; 126646–02–4; 126950–62–7; 127036–24–2; 139626–71–4; 152231–44–2; 154518–36–2; 157627–86–6; 157627–88–8; 157707–41–0; 157707–43–2; 159653–49–3; 160875–66–1; 160901–20–2; 160901–09–7; 160901–19–9; 161025–21–4; 161025–22–5; 166736–08–9; 169107–21–5; 172588–43–1; 176022–76–7; 196823–11–7; 287935–46–0; 288260–45–7; 303176–75–2; 954108–36–2; 2222805–23–2. Aluminum sulfate 10043–01–3 ...... When ready for use, the end-use concentration is not to exceed 50 ppm

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Pesticide Chemical CAS Reg. No. Limits

2-propen-1-aminium, N,N-dimethyl-N-propenyl-, chloride, 26062–79–3 ...... When ready for use, the end-use concentration is not homopolymer to exceed 0.6% Ammonium chloride 12125–02–9 When ready for use, the end-use concentration is not to exceed 48 ppm Amylopectin, acid-hydrolyzed, 1-oxtenylbutanedioate 113894–85–2 None Amylopectin, hydrogen 1-octadecenylbutanedioate 125109–81–1 None Aspartic acid, N-(1,2-dicarboxyethyl)-, tetrasodium salt ...... 144538–83–0 ...... When ready for use, the end-use concentration is not to exceed 5000 ppm Butryic acid ...... 107–92–6 ...... When ready for use, the end-use concentration is not to exceed 100 ppm Butyl alcohol ...... 71–36–3 ...... When ready for use, the end-use concentration is not to exceed 100 ppm n-Butyl benzoate ...... 136–60–7 ...... When ready for use, the end-use concentration is not to exceed 15,000 ppm n-Butyl-3-hydroxybutyrate ...... 53605–94–0 ...... Solvent Citral ...... 5392–40–5 ...... When ready for use, the end-use concentration is not to exceed 100 ppm Citronellol ...... 106–22–9 ...... When ready for use, the end-use concentration is not to exceed 100 ppm Citronellyl acetate ...... 150–84–5 ...... When ready for use, the end-use concentration is not to exceed 100 ppm Copper sulfate pentahydrate 7758–99–8 When ready for use, the end-use concentration is not to exceed 80 ppm b-Damascone, (Z)- ...... 23726–92–3 ...... When ready for use, the end-use concentration is not to exceed 100 ppm Decanal ...... 112–31–2 ...... When ready for use, the end-use concentration is not to exceed 100 ppm Decanoic acid ...... 334–48–5 ...... When ready for use, the end-use concentration is not to exceed 100 ppm 1-Decanol ...... 112–30–1 ...... When ready for use, the end-use concentration is not to exceed 100 ppm (E)-4-Decenal ...... 65405–70–1 ...... When ready for use, the end-use concentration is not to exceed 100 ppm D-Glucopyranose, oligomeric, decyl octyl glycosides 68515–73–1 None 1,3-dibromo-5,5-dimethylhydantoin ...... 77–48–5 ...... None 2,6-Dimethyl-5-heptanal ...... 106–72–9 ...... When ready for use, the end-use concentration is not to exceed 100 ppm Di-n-butyl carbonate 542–52–9 ...... When ready for use, the end-use concentration is not to exceed 15,000 ppm 2-Dodecanol, (2E)- ...... 20407–84–5 ...... When ready for use, the end-use concentration is not to exceed 100 ppm Ethanol 64–17–5 None Ethyl 2-methylbutyrate ...... 452–79–1 ...... When ready for use, the end-use concentration is not to exceed 100 ppm Ethylenediaminetetraacetic acid (EDTA), tetrasodium salt 64–02–8 None FD&C Green No. 3 CAS Reg. No. 2353–45–9 None FD&C Red No. 40 25956–17–6 ...... When ready for use, the end-use concentration is not to exceed 20 ppm. FD&C Yellow No. 5 1934–21–0 When ready for use, the end-use concentration is not to exceed 1000 ppm (E)-Geraniol ...... 106–24–1 ...... When ready for use, the end-use concentration is not to exceed 100 ppm (E)-Geraniol acetate ...... 105–87–3 ...... When ready for use, the end-use concentration is not to exceed 100 ppm C1-C4 linear and branched chain alkyl d-glucitol dianhydro 5306–85–4; 30915–81–2; When ready for use, the end-use concentration is not alkyl ethers cluster. 107644–13–3; 103594–41–8; to exceed 500 ppm. 103594–42–9. D-glucitol, 1,4:3,6-dianhydro-2,5-di-O-(1-methylpropyl)-, ...... None. D-glucitol, 1,4:3,6-dianhydro-2,5-di-O-(2-methylpropyl)-, (CAS None. Reg. No. not assigned). D-glucurono-6-deoxy-L-manno-D-glucan, acetate, calcium (CAS No. 595585–15–2) ...... None magnesium potassium sodium salt (diutan gum). Heptanal ...... 111–71–7 ...... When ready for use, the end-use concentration is not to exceed 100 ppm Heptanoic acid ...... 111–14–8 ...... When ready for use, the end-use concentration is not to exceed 100 ppm Heptyl alcohol ...... 111–70–6 ...... When ready for use, the end-use concentration is not to exceed 100 ppm Hexanal ...... 66–25–1 ...... When ready for use, the end-use concentration is not to exceed 100 ppm Hexanoic acid ...... 142–62–1 ...... When ready for use, the end-use concentration is not to exceed 100 ppm n-Hexanol ...... 111–27–3 ...... When ready for use, the end-use concentration is not to exceed 100 ppm (Z)-3-Hexenol ...... 928–96–1 ...... When ready for use, the end-use concentration is not to exceed 100 ppm (Z)-3-Hexenol acetate ...... 3681–71–8 ...... When ready for use, the end-use concentration is not to exceed 100 ppm Hexyl acetate ...... 142–92–7 ...... When ready for use, the end-use concentration is not to exceed 100 ppm Hydrogen peroxide 7722–84–1 When ready for use, the end-use concentration is not to exceed 91 ppm Hypochlorous acid, sodium salt 7681–52–9 When ready for use, the end-use concentration of all hypochlorous acid chemicals in the solution is not to exceed 200 ppm determined as total available chlorine

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Pesticide Chemical CAS Reg. No. Limits

Iodine 7553–56–2 When ready for use, the total end-use concentration of all iodide-producing chemicals in the solution is not to exceed 25 ppm of titratable iodine Isopropyl-3-hydroxybutyrate ...... 54074–94–1 ...... Solvent Lactic acid ...... 50–21–5 ...... When ready for use, the end-use concentration is not to exceed 10,000 ppm in antimicrobial formulations applied to food-contact surfaces in public eating places Lauric acid ...... 143–07–7 ...... When ready for use, the end-use concentration is not to exceed 100 ppm Lauric aldehyde ...... 112–54–9 ...... When ready for use, the end-use concentration is not to exceed 100 ppm Lauryl alcohol ...... 112–53–8 ...... When ready for use, the end-use concentration is not to exceed 100 ppm d-Limonene ...... 5989–27–5 ...... When ready for use, the end-use concentration is not to exceed 100 ppm Lipase, triacylglycerol 9001–62–1 When ready for use, the end-use concentration is not to exceed 500 ppm Magnesium oxide 1309–48–4 None Methane sulfonic acid 75–75–2 When ready for use, the end use concentration is not to exceed 5,000 ppm Methylene blue 61–73–4 When ready for use, the end-use concentration is not to exceed 0.4 ppm Methyl-a-ionone ...... 127–42–4 ...... When ready for use, the end-use concentration is not to exceed 100 ppm 3-Methyl-2-butenyl acetate ...... 1191–16–8 ...... When ready for use, the end-use concentration is not to exceed 100 ppm 2-Methylundecanal ...... 110–41–8 ...... When ready for use, the end-use concentration is not to exceed 100 ppm 2-Methyl-1,3-propanediol 2163–42–0 None Myristaldehyde ...... 124–25–4 ...... When ready for use, the end-use concentration is not to exceed 100 ppm Myristic acid ...... 544–63–8 ...... When ready for use, the end-use concentration is not to exceed 100 ppm Neryl acetate ...... 141–12–8 ...... When ready for use, the end-use concentration is not to exceed 100 ppm Nitric acid 7697–37–2 When ready for use, the end-use concentration is not to exceed 1,000 ppm Nonanal ...... 124–19–6 ...... When ready for use, the end-use concentration is not to exceed 100 ppm Nonanoic acid ...... 112–05–0 ...... When ready for use, the end-use concentration is not to exceed 100 ppm Nonyl alcohol ...... 143–08–8 ...... When ready for use, the end-use concentration is not to exceed 100 ppm a-(p-Nonylphenyl)-w-hydroxypoly (oxyethylene) average None None poly(oxyethylene) content 11 moles) Octadecanoic acid, calcium salt 1592–23–0 None 9-Octadecenoic acid (9Z)-, sulfonated, oxidized 1315321–93–7 ...... When ready for use, the end-use concentration is not to exceed 250 ppm. 9-Octadecenoic acid (9Z)-, sulfonated, oxidized, potassium 1315321–94–8 ...... When ready for use, the end-use concentration is not salts to exceed 250 ppm. 9-Octadecenoic acid (9Z)-, sulfonated, oxidized, sodium salts 1315321–95–9 ...... When ready for use, the end-use concentration is not to exceed 250 ppm. Octanal ...... 124–13–0 ...... When ready for use, the end-use concentration is not to exceed 100 ppm 1-Octanesulfonic acid, sodium salt 5324–84–5 When ready for use, the end-use concentration is not to exceed 46 ppm Octanoic acid 124–07–2 When ready for use, the end-use concentration is not to exceed 52 ppm Octanoic acid ...... 124–07–2 ...... When ready for use, the end-use concentration is not to exceed 100 ppm 1-Octanol ...... 111–87–5 ...... When ready for use, the end-use concentration is not to exceed 100 ppm Oxirane, methyl-, polymer with oxirane, minimum molecular 9003–11–6 None weight (in amu), 1900 Palmitic acid ...... 57–10–3 ...... When ready for use, the end-use concentration is not to exceed 100 ppm Peroxyacetic acid 79–21–0 When ready for use, the end-use concentration is not to exceed 58 ppm Peroxyoctanoic acid 33734–57–5 When ready for use, the end-use concentration is not to exceed 52 ppm Phosphonic acid, (1-hydroxyethylidene)bis- 2809–21–4 When ready for use, the end-use concentration is not to exceed 14 ppm Phosphoric acid, trisodium salt 7601–54–9 When ready for use, the end-use concentration is not to exceed 5916 ppm Potassium bromide 7758–02–3 When ready for use, the end-use concentration is not to exceed 46 ppm total available halogen Potassium iodide 7681–11–0 When ready for use, the total end-use concentration of all iodide-producing chemicals in the solution is not to exceed 25 ppm of titratable iodine 1,3-Propanediol 504–63–2 None Propionic acid ...... 79–09–4 ...... When ready for use, the end-use concentration is not to exceed 100 ppm Propylene glycol 57–55–6 None Quaternary ammonium compounds, alkyl (C12-C18) 8001–54–5 When ready for use, the end-use concentration of all benzyldimethyl, chlorides quaternary chemicals in the solution is not to exceed 200 ppm of active quaternary compound

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Pesticide Chemical CAS Reg. No. Limits

Quaternary ammonium compounds: n-alkyl (C12-18) dimethyl 68424–85–1 When ready for use, the end-use concentration of all benzyl ammonium chloride quaternary chemicals in solution is not to exceed 400 ppm of active quaternary compound Quaternary Ammonium Compounds: n-alkyl (C 12-14) dimethyl 85409–23–0 When ready for use, the end-use concentration of all ethylbenzyl ammonium chloride, average molecular weight quaternary chemicals in solution is not to exceed (in amu), 377 to 384 400 ppm of active quaternary compound. Quaternary ammonium compounds n-alkyl (C12-C18) dimethyl None When ready for use, the end-use concentration of all ethylbenzyl ammonium chloride average molecular weight quaternary chemicals in the solution is not to exceed (in amu) 384 200 ppm of active quaternary compound Quaternary ammonium compounds, Di-n-Alkyl (C8-10) dimethyl None When ready for use, the end-use concentration of ammonium chloride, average molecular weight (in amu) 332 these specific in quaternary ammonium compounds to 361 is not to exceed 240 ppm of active quaternary ammonium compound; the end-use concentration of all quaternary chemicals in the solution is not to exceed 400 ppm of active quaternary compound Quaternary ammonium compounds, didecyl dimethyl ammo- 148788–55–0/148812–654–1 When ready for use, the end-use concentration of nium carbonate/didecyl dimethyl ammonium bicarbonate these specific ammonium compounds is not to exceed 400 ppm of active quaternary ammonium compound Silver ions resulting from the use of electrolytically-generated 14701–21–4 When ready for use, the end-use concentration of sil- silver ions stabilized in citric acid as silver dihydrogen cit- ver ions is not to exceed 50 ppm of active silver rate (does not include metallic silver) Sodium bisulfate 7681–38–1 When ready for use, the end-use concentration is not to exceed 2,000 ppm. Sorbitan, mono-9-octadecenoate, poly(oxy-1,2-ethanediyl) 9005–65–6 None derivs., (Z)- Stearic acid...... 57–11–4 ...... When ready for use, the end-use concentration is not to exceed 100 ppm Sulfuric acid ...... 7664–93–9 ...... Food-contact surfaces in public eating places, dairy- processing equipment, and food-processing equipment and utensils in antimicrobial formulations. Not to exceed 600 ppm. Sulfuric acid monododecyl ester, sodium salt (sodium lauryl 151–21–3 When ready for use, the end-use concentration is not sulfate) to exceed 350 ppm Tall oil fatty acid (CAS Reg. No. 61790–12–3) ...... Solvent/carrier Trans-1,3,3,3-tetrafluoroprop-1-ene ...... 29118–24–9 ...... None 1,3,5-Triazine-2,4,6(1H,3H,5H)-trione, 1,3-dichloro-, sodium 2893–78–9 When ready for use, the end-use concentration of all salt di- or trichloroisocyanuric acid chemicals in the solution is not to exceed 100 ppm determined as total available chlorine 2-Tridecanal ...... 7774–82–5 ...... When ready for use, the end-use concentration is not to exceed 100 ppm 3,5,5-Trimethylhexanal ...... 5435–64–3 ...... When ready for use, the end-use concentration is not to exceed 100 ppm Undecanal ...... 112–44–7 ...... When ready for use, the end-use concentration is not to exceed 100 ppm Undecyl alcohol ...... 112–42–5 ...... When ready for use, the end-use concentration is not to exceed 100 ppm Valeraldehyde ...... 110–62–3 ...... When ready for use, the end-use concentration is not to exceed 100 ppm Valeric acid ...... 109–52–4 ...... When ready for use, the end-use concentration is not to exceed 100 ppm Waxes and waxy substances, rice bran, oxidized ...... 1883583–80–9 ...... None Xylenesulfonic acid, sodium salt 1300–72–7 When ready for use, the end-use concentration is not to exceed 500 ppm

(b) The following chemical sub- may be applied to: Dairy processing stances when used as ingredients in an equipment, and food-processing equip- antimicrobial pesticide formulation ment and utensils.

Pesticide Chemical CAS Reg. No. Limits

Acetic acid 64–19–7 When ready for use, the end-use concentration is not to exceed 1200 ppm Acetic acid, chloro-, sodium salt, reaction products 68608–66–2 When ready for use, the end-use concentra- with 4,5-dihydro-2-undecyl-1H-imidazole-1-eth- tion is not to exceed 42 ppm chloroacetic anol and sodium hydroxide acid Butanedioic acid, octenyl- 28805–58–5 When ready for use, the end-use concentration is not to exceed 156 ppm Butoxy monoether of mixed (ethylene-propylene) None None polyalkylene glycol, minimum average molecular weight (in amu), 2400 Calcium chloride 10043–52–4 When ready for use, the end-use concentration is not to exceed 17 ppm n-Carboxylic acids (C6-C12), consisting of a mixture None When ready for use, the end-use concentra- of not less than 56% octanoic acid and not less tion is not to exceed 39 ppm than 40% decanoic acid Decanoic acid 334–48–5 When ready for use, the end-use concentration is not to exceed 90 ppm

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Pesticide Chemical CAS Reg. No. Limits

Ethanesulfonic acid, 2-[cyclohexyl (1- 132–43–4 When ready for use, the end-use concentra- oxohexadecyl) amino]-, sodium salt tion is not to exceed 237 ppm Ethylenediaminetetraacetic acid (EDTA), disodium 139–33–3 When ready for use, the end-use concentra- salt tion is not to exceed 1400 ppm FD&C Yellow No. 5 (Tartrazine) (conforming to 21 1934–21–0 None CFR 74.705) C1-C4 linear and branched chain alkyl d-glucitol 5306–85–4; 30915–81–2; When ready for use, the end-use concentra- dianhydro alkyl ethers cluster. 107644–13–3; 103594– tion is not to exceed 1,000 ppm. 41–8; 103594–42–9. D-glucitol, 1,4:3,6-dianhydro-2,5-di-O-(1- None. methylpropyl)-,. D-glucitol, 1,4:3,6-dianhydro-2,5-di-O-(2- None. methylpropyl)-, (CAS Reg. No. not assigned). D-Gluconic acid, monosodium salt 527–07–1 When ready for use, the end-use concentration is not to exceed 760 ppm Hydriodic acid 10034–85–2 When ready for use, the total end-use concentration of all iodide-producing chemicals is not to exceed 25 ppm of titratable iodine Hydrogen peroxide 7722–84–1 When ready for use, the end-use concentration is not to exceed 465 ppm Hypochlorous acid 7790–92–3 When ready for use, the end-use concentration of all hypochlorous acid chemicals in the solution is not to exceed 200 ppm determined as total available chlorine Iodine 7553–56–2 When ready for use, the total end-use concentration of all iodide-producing chemicals in the solution is not to exceed 25 ppm of titratable iodine Lactic acid 50–21–5 When ready for use, the end-use concentration is not to exceed 138 ppm Nonanoic acid 112–05–0 When ready for use, the end-use concentration is not to exceed 90 ppm 1-Octanamine, N,N-dimethyl- 7378–99–6 When ready for use, the end-use concentration is not to exceed 113 ppm 1,2-Octanedisulfonic acid 113669–58–2 When ready for use, the end-use concentration is not to exceed 102 ppm 1-Octanesulfonic acid 3944–72–7 When ready for use, the end-use concentration is not to exceed 172 ppm 1-Octanesulfonic acid, sodium salt 5324–84–5 When ready for use, the end-use concentration is not to exceed 297 ppm 1-Octanesulfonic acid, 2-sulfino- 113652–56–5 When ready for use, the end-use concentration is not to exceed 102 ppm Octanoic acid 124–07–2 When ready for use, the end-use concentration is not to exceed 176 ppm Oxychloro species (including chlorine dioxide) gen- None When ready for use, the end-use concentra- erated by acidification of an aqueous solution of tion is not to exceed 200 ppm of chlorine sodium chlorite dioxide as determined by the method titled, Iodometric Method for the Determination of Available Chlorine Dioxide (50-250 ppm available chlorine dioxide) Peroxyacetic acid 79–21–0 When ready for use, the end-use concentration is not to exceed 315 ppm Peroxyoctanoic acid 33734–57–5 When ready for use, the end-use concentration is not to exceed 122 ppm Phosphonic acid, (1-hydroxyethylidene)bis- 2809–21–4 When ready for use, the end-use concentration is not to exceed 34 ppm Phosphoric acid 7664–38–2 None Phosphoric acid, monosodium salt 7558–80–7 When ready for use, the end-use concentration is not to exceed 350 ppm Potassium iodide 7681–11–0 When ready for use, the total end-use concentration of all iodide-producing chemicals in the solution is not to exceed 25 ppm of titratable iodine Propanoic acid 79–09–4 When ready for use, the end-use concentration is not to exceed 297 ppm 2,6-Pyridinedicarboxylic acid 499–83–2 When ready for use, the end-use concentration is not to exceed 1.2 ppm Sulfuric acid monododecyl ester, sodium salt (so- 151–21–3 When ready for use, the end-use concentra- dium lauryl sulfate) tion is not to exceed 350 ppm

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(c) The following chemical sub- may be applied to: Food-processing stances when used as ingredients in an equipment and utensils. antimicrobial pesticide formulation

Pesticide Chemical CAS Reg. No. Limits

Acetic acid 64–19–7 When ready for use, the end-use concentration is not to exceed 1,200 ppm Acetic acid, chloro-, sodium salt, reaction products 68608–66–2 When ready for use, the end-use concentra- with 4,5-dihydro-2-undecyl-1H-imidazole-1-eth- tion is not to exceed 42 ppm chloroacetic anol and sodium hydroxide acid Ammonium chloride 12125–02–9 When ready for use, the end-use concentration is not to exceed 48 ppm [1,1′-Biphenyl]-2-ol 90–43–7 When ready for use, the end-use concentration is not to exceed 400 ppm Boric acid, sodium salt 7775–19–1 None Butanedioic acid, octenyl- 28805–58–5 When ready for use, the end-use concentration is not to exceed 156 ppm Butanedioic acid, sulfo-, 1,4-dioctyl ester, sodium 1639–66–3 None salt Butoxy monoether of mixed (ethylene-propylene) None None polyalkylene glycol, cloudpoint of 90 - 100oC in 0.5 aqueous solution, average molecular weight (in amu), 3300 Butoxy monoether of mixed (ethylene-propylene) None None polyalkylene glycol, minimum average molecular weight (in amu), 2400 Calcium chloride 10043–52–4 When ready for use, the end-use concentration is not to exceed 17 ppm n-Carboxylic acids (C6-C12), consisting of a mixture None When ready for use, the end-use concentra- of not less than 56% octanoic acid and not less tion is not to exceed 39 ppm than 40% decanoic acid 3-Cyclohexene-1-methanol,a,a,4-trimethyl- 98–55–5 None 1-Decanaminium, N-decyl-N, N-dimethyl-, chloride 7173–51–5 When ready for use, the end-use concentration is not to exceed 200 ppm of active quaternary compound Decanoic acid 3347–48–5 When ready for use, the end-use concentration is not to exceed 234 ppm Ethanesulfonic acid, 2-[cyclohexyl (1- 132–43–4 When ready for use, the end-use concentra- oxohexadecyl) amino]-, sodium salt tion is not to exceed 237 ppm Ethanol 64–17–5 None Ethanol, 2 butoxy- 111–76–2 None Ethanol, 2-(2-ethoxyethoxy)- 111–90–0 None Ethylenediaminetetraacetic acid (EDTA), disodium 139–33–3 When ready for use, the end-use concentra- salt tion is not to exceed 1400 ppm Ethylenediaminetetraacetic acid (EDTA), 64–02–8 None tetrasodium salt Fatty acids, coco, potassium salts 61789–30–8 None Fatty acids, tall-oil, sulfonated, sodium salts 68309–27–3 When ready for use, the end-use concentration is not to exceed 66 ppm FD&C Yellow No. 5 (Tartrazine) (conforming to 21 1934–21–0 None CFR 74.705) D-Gluconic acid, monosodium salt 527–07–1 When ready for use, the end-use concentration is not to exceed 760 ppm Hydriodic acid 10034–85–2 When ready for use, the total end-use concentration of all iodide-producing chemicals in the solution is not to exceed 25 ppm of titratable iodine Hydrogen peroxide 7722–84–1 When ready for use, the end-use concentration is not to exceed 1100 ppm Hypochlorous acid 7790–92–3 When ready for use, the end-use concentration of all hypochlorous acid chemicals in the solution is not to exceed 200 ppm determined as total available chlorine Hypochlorous acid, calcium salt 7778–54–3 When ready for use, the end-use concentration of all hypochlorous acid chemicals in the solution is not to exceed 200 ppm determined as total available chlorine Hypochlorous acid, lithium salt 13840–33–0 When ready for use, the end-use concentration of all hypochlorous acid chemicals in the solution is not to exceed 200 ppm determined as total available chlorine and 30 ppm lithium

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Pesticide Chemical CAS Reg. No. Limits

Hypochlorous acid, potassium salt 7778–66–7 When ready for use, the end-use concentration of all hypochlorous acid chemicals in the solution is not to exceed 200 ppm determined as total available chlorine Hypochlorous acid, sodium salt 7681–52–9 When ready for use, the end-use concentration of all hypochlorous acid chemicals in the solution is not to exceed 200 ppm determined as total available chlorine Iodine 7553–56–2 When ready for use, the total end-use concentration of all iodide-producing chemicals in the solution is not to exceed 25 ppm of titratable iodine Magnesium oxide 1309–48–4 None Methylene blue 61–73–4 When ready for use, the end-use concentration is not to exceed 0.4 ppm Neodecanoic acid 26896–20–8 When ready for use, the end-use concentration is not to exceed 174 ppm Nonanoic acid 112–05–0 When ready for use, the end-use concentration is not to exceed 90 ppm a-(p-Nonylphenyl)-w-hydroxypoly (oxyethylene) None None maximum average molecular weight (in amu), 748 a-(p-Nonylphenol)-w-hydroxypoly (oxyethylene) av- None None erage poly(oxyethylene) content 11 moles a-(p-Nonylphenyl)-w-hydroxypoly (oxyethylene) None None produced by the condensation of 1 mole p- nonylphenol with 9 to 12 moles ethylene oxide a-(p-Nonylphenyl)-w-hydroxypoly (oxyethylene), 9 None None to 13 moles ethylene oxide Octadecanoic acid, calcium salt 1592–23–0 None 9-Octadecenoic acid (9Z)-, sulfonated 68988–76–1 When ready for use, the end-use concentration is not to exceed 312 ppm 9-Octadecenoic acid (9Z)-sulfonated, sodium salts 68443–05–0 When ready for use, the end-use concentration is not to exceed 200 ppm 1-Octanamine, N,N-dimethyl- 7378–99–6 When ready for use, the end-use concentration is not to exceed 113 ppm 1,2-Octanedisulfonic acid 113669–58–2 When ready for use, the end-use concentration is not to exceed 102 ppm 1-Octanesulfonic acid 3944–72–7 When ready for use, the end-use concentration is not to exceed 172 ppm 1-Octanesulfonic acid, sodium salt 5324–84–5 When ready for use, the end-use concentration is not to exceed 312 ppm 1-Octanesulfonic acid, 2-sulfino- 113652–56–5 When ready for use, the end-use concentration is not to exceed 102 ppm Octanoic acid 124–07–2 When ready for use, the end-use concentration is not to exceed 234 ppm Oxirane, methyl-, polymer with oxirane, minimum 9003–11–6 None molecular weight (in amu), 1900 Oxirane, methyl-, polymer with oxirane, block, av- 106392–12–5 None erage molecular weight (in amu), 1900 Oxirane, methyl-, polymer with oxirane, block, min- None None imum average molecular weight (in amu), 2000 Oxirane, methyl-, polymer with oxirane, block, 27 None None to 31 moles of polyoxypropylene, average molecular weight (in amu) 2000 Oxychloro species (predominantly chlorite, chlorate None When ready for use, the end-use concentra- and chlorine dioxide in an equilibrium mixture) tion is not to exceed 200 ppm of chlorine generated either (i) by directly metering a con- dioxide as determined by the method titled, centrated chlorine dioxide solution prepared just ‘‘Iodometric Method for the Determination prior to use, into potable water, or (ii) by acidifi- of Available Chlorine Dioxide (50-250 ppm cation of an aqueous alkaline solution of available chlorine dioxide)’’ oxychloro species (predominately chlorite and chlorate) followed by dilution with potable water Oxychloro species (including chlorine dioxide) gen- None When ready for use, the end-use concentra- erated by acidification of an aqueous solution of tion is not to exceed 200 ppm of chlorine sodium chlorite dioxide as determined by the method titled, ‘‘Iodometric Method for the Determination of Available Chlorine Dioxide (50-250 ppm available chlorine dioxide)’’ 2,4-Pentanediol, 2-methyl- 107–41–5 None Peroxyacetic acid 79–21–0 When ready for use, the end-use concentration is not to exceed 315 ppm Peroxyoctanoic acid 33734–57–5 When ready for use, the end-use concentration is not to exceed 122 ppm

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Pesticide Chemical CAS Reg. No. Limits

Phenol, 4-chloro-2-(phenylmethyl)- 120–32–1 When ready for use, the end-use concentration is not to exceed 320 ppm Phenol, 4-(1,1-dimethylpropyl)- 80–46–6 When ready for use, the end-use concentration is not to exceed 80 ppm Phosphonic acid, (1-hydroxyethylidene)bis- 2809–21–4 When ready for use, the end-use concentration is not to exceed 34 ppm Phosphoric acid 7664–38–2 None Phosphoric acid, monosodium salt 7558–80–7 When ready for use, the end-use concentration is not to exceed 350 ppm Phosphoric acid, trisodium salt 7601–54–9 When ready for use, the end-use concentration is not to exceed 5916 ppm Poly(oxy-1,2-ethanediyl), a-[(1,1,3,3- None None tetramethylbutyl) phenyl]-w-hydroxy-, produced with one mole of the phenol and 4 to 14 moles ethylene oxide Potassium bromide 7758–02–3 When ready for use, the end-use concentration of all bromide-producing chemicals in the solution is not to exceed 200 ppm total available halogen Potassium iodide 7681–11–0 When ready for use, the total end-use concentration of all iodide-producing chemicals in the solution is not to exceed 25 ppm of titratable iodine Propanoic acid 79–09–4 When ready for use, the end-use concentration is not to exceed 297 ppm 2,6-Pyridinedicarboxylic acid 499–83–2 When ready for use, the end-use concentration is not to exceed 1.2 ppm

Quaternary ammonium compounds, alkyl (C12-C18) 8001–54–5 When ready for use, the end-use concentra- benzyldimethyl, chlorides tion of this specific quaternary compound is not to exceed 200 ppm within the end-use total concentration that is not to exceed 400 ppm active quaternary compound

Quaternary ammonium compounds, n-alkyl (C12- None When ready for use, the end-use concentra- C14) dimethyl ethylbenzyl ammonium chloride, tion of this specific quaternary compound is average molecular weight (in amu), 377 to 384 not to exceed 200 ppm within the end-use total concentration that is not to exceed 400 ppm active quaternary compound

Quaternary ammonium compounds, n-alkyl (C12- None When ready for use, the end-use concentra- C18) dimethyl ethylbenzyl ammonium chloride tion of this specific quaternary compound is average molecular weight (in amu) 384 not to exceed 200 ppm within the end-use total concentration that is not to exceed 400 ppm active quaternary compound

Quaternary ammonium compounds, di-n-Alkyl (C8- None When ready for use, the end-use concentra- C10) dimethyl ammonium chloride, average mo- tion of this specific quaternary compound is lecular weight (in amu), 332 to 361 not to exceed 240 ppm within the end-use total concentration that is not to exceed 400 ppm active quaternary compound

Sodium-a-alkyl(C12-C15)-w-hydroxypoly (oxy- None None ethylene) sulfate with the poly(oxyethylene) content averaging one mole Sodium bromide 7647–15–6 When ready for use, the end-use concentration of all bromide-producing chemicals in the solution is not to exceed 200 ppm total available halogen Sodium iodide 7681–82–5 When ready for use, the total end-use concentration of all iodide-producing chemicals in the solution is not to exceed 25 ppm of titratable iodine Sulfuric acid monododecyl ester, sodium salt (so- 151–21–3 None dium lauryl sulfate) 1,3,5-Triazine-2,4,6(1H,3H,5H)-trione, 1,3-dichloro- 2782–57–2 When ready for use, the end-use concentration of all di- or trichloroisocyanuric acid chemicals in the solution is not to exceed 100 ppm determined as total available chlorine 1,3,5-Triazine-2,4,6(1H,3H,5H)-trione, 1,3-dichloro-, 2244–21–5 When ready for use, the end-use concentra- potassium salt tion of all di- or trichloroisocyanuric acid chemicals in the solution is not to exceed 100 ppm determined as total available chlorine

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Pesticide Chemical CAS Reg. No. Limits

1,3,5-Triazine-2,4,6(1H,3H,5H)-trione, 1,3-dichloro-, 2893–78–9 When ready for use, the end-use concentra- sodium salt tion of all di- or trichloroisocyanuric acid chemicals in the solution is not to exceed 100 ppm determined as total available chlorine 1,3,5-Triazine-2,4,6(1H,3H,5H)-trione, 1,3,5- 87–90–1 When ready for use, the end-use concentra- trichloro- tion of all di- or trichloroisocyanuric acid chemicals in the solution is not to exceed 100 ppm determined as total available chlorine 1,3,5-Triazine, N,N′,N″-trichloro-2,4,6-triamino- 7673–09–8 When ready for use, the end-use concentration of all di- or trichloroisocyanuric acid chemicals in the solution is not to exceed 200 ppm determined as total available chlorine

[69 FR 23136, Apr. 28, 2004]

EDITORIAL NOTE: For FEDERAL REGISTER citations affecting § 180.940, see the List of CFR Sections Affected, which appears in the Finding Aids section of the printed volume and at www.govinfo.gov.

§ 180.950 Tolerance exemptions for (ii) Both the raw and processed forms minimal risk active and inert ingre- of peanuts, tree nuts, milk, soybeans, dients. eggs, fish, crustacea, and wheat. Unless specifically excluded, residues (iii) Alcoholic beverages. resulting from the use of the following (iv) Dietary supplements. substances as either an inert or an ac- (b) Animal feed items. Animal feed tive ingredient in a pesticide chemical items means meat meal and all items formulation, including antimicrobial derived from field crops that are fed to pesticide chemicals, are exempted from livestock excluding both the raw and the requirement of a tolerance under processed forms of peanuts, tree nuts, FFDCA section 408, if such use is in ac- milk, soybeans, eggs, fish, crustacea, cordance with good agricultural or and wheat. Meat meal is an animal feed manufacturing practices. composed of dried animal fat and pro- (a) Commonly consumed food commod- tein that has been sterilized. Other ities. Commonly consumed food com- than meat meal, the term animal feed modities means foods that are com- item does not extend to any item de- monly consumed for their nutrient signed to be fed to animals that con- properties. The term commonly contains, to any extent, components of sumed food commodities shall only animals. Included within the term ani- apply to food commodities (whether a mal feed items are: raw agricultural commodity or a proc- (1) The hulls and shells of the com- essed commodity) in the form the commodities specified in paragraph modity is sold or distributed to the (a)(2)(ii) of this section, and cocoa public for consumption. bean. (1) Included within the term com- (2) Bird feed such as canary seed. monly consumed food commodities are: (3) Any feed component of a medi- (i) Sugars such as sucrose, lactose, cated feed meeting the definition of an dextrose and fructose, and invert sugar animal feed item. and syrup. (c) Edible fats and oils. Edible fats and (ii) Spices such as cinnamon, cloves, oils means all edible (food or feed) fats and red pepper. and oils, derived from either plants or (iii) Herbs such as basil, anise, or animals, whether or not commonly fenugreek. consumed, including products derived (2) Excluded from the term com- from hydrogenating (food or feed) oils, monly consumed food commodities are: or liquefying (food or feed) fats. (i) Any food commodity that is adul- (1) Included within the term edible terated under 21 U.S.C. 342. fats and oils are oils (such as soybean

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oil) that are derived from the commod- Chemical CAS No. ities specified in paragraph (a)(2)(ii) of Citric acid, dipotassium salt ...... 3609–96–9 this section when such oils are highly Citric acid, disodium salt ...... 144–33–2 refined via a solvent extraction proce- Citric acid, monohydrate ...... 5949–29–1 dure. Citric acid, monopotassium salt ...... 866–83–1 (2) Excluded from the term edible Citric acid, monosodium salt ...... 18996–35–5 Citric acid, potassium salt ...... 7778–49–6 fats and oils are plant oils used in the Citric acid, triethyl ester ...... 77–93–0 pesticide chemical formulation specifi- Citric acid, tripotassium salt ...... 866–84–2 cally to impart their characteristic Citric acid, tripotassium salt, monohydrate ...... 6100–05–6 Citric acid, sodium salt ...... 994–36–5 fragrance and/or flavoring. Citric acid, trisodium salt ...... 68–04–2 (d) [Reserved] Citric acid, trisodium salt, dihydrate ...... 6132–04–3 (e) Specific chemical substances. Resi- Citric acid, trisodium salt, pentahydrate ...... 6858–44–2 dues resulting from the use of the fol- Coffee grounds ...... 68916–18–7 Dextrins ...... 9004–53–9 lowing substances as either an inert or 1,3-Dioxolan-2-one, 4-methyl-(propylene car- an active ingredient in a pesticide bonate) ...... 108–32–7 chemical formulation, including anti- Fumaric acid ...... 110–17–8 Gamma-cyclodextrin ...... 17465–86–0 microbial pesticide chemicals, are ex- Gellan gum ...... 71010–52–1 empted from the requirement of a tol- D-Glucitol (sorbitol) ...... 50–70–4 erance under FFDCA section 408, if Glycerol (glycerin) (1,2,3-propanetriol) ...... 56–81–5 such use is in accordance with good ag- Guar gum ...... 9000–30–0 Humic acid ...... 1413–93–6 ricultural or manufacturing practices. Humic acid, potassium salt ...... 68514–28–3 Humic acid, sodium salt ...... 68131–04–4 Chemical CAS No. Lactic acid, n-butyl ester ...... 138–22–7 Lactic acid, n-butyl ester, (S) ...... 34451–19–9 Acetic acid, sodium salt ...... 127–09–3 Lactic acid, ethyl ester ...... 97–64–3 Alpha-cyclodextrin ...... 10016–20–3 Lactic acid, ethyl ester,(S) ...... 687–47–8 Amylopectin, acid-hydrolyzed, 1- Lanolin ...... 8006–54–0 octenylbutanedioate ...... 113894–85– Lecithins ...... 8002–43–5 2 Lecithins, soya ...... 8030–76–0 Amylopectin, hydrogen 1- Licorice Extract ...... 68916–91–6 octadecenylbutanedioate ...... 125109–81– Maltodextrin ...... 9050–36–6 1 Paper ...... None Animal glue ...... None Potassium chloride ...... 7447–40–7 Ascorbic acid (vitamin C) ...... 50–81–7 2-Propanol (isopropyl alcohol) ...... 67–63–0 Beeswax ...... 8012–89–3 Red cabbage color, expressed from edible red Benzoic acid, sodium salt ...... 532–32–1 cabbage heads via a pressing process using Beta-cyclodextrin ...... 7585–39–9 only acidified water ...... None Carbonic acid, monopotassium salt ...... 298–14–6 Silica, amorphous, fumed (crystalline free) ...... 112945–52– Carbonic acid, monosodium salt (sodium bicar- 5 bonate) ...... 144–55–8 Silica, amorphous, precipitated and gel ...... 7699–41–4 Carnauba wax ...... 8015–86–9 Silica gel ...... 63231–67–4 Carob gum (locust bean gum) ...... 9000–40–2 Silica gel, precipitated, crystalline-free ...... 112926–00– Castor oil ...... 8001–79–4 8 Castor oil, hydrogenated ...... 8001–78–3 Silica, hydrate ...... 10279–57–9 Cellulose ...... 9004–34–6 Silica, vitreous ...... 60676–86–0 Cellulose acetate ...... 9004–35–7 Soap (The water soluble sodium or potassium Cellulose, carboxy methyl ether, sodium salt ... 9004–32–4 salts of fatty acids produced by either the Cellulose, 2-hydroxyethyl ether ...... 9004–62–0 saponification of fats and oils, or the neutral- Cellulose, 2-hydroxypropyl ether ...... 9004–64–2 ization of fatty acid) ...... None Cellulose, 2-hydroxypropyl methyl ether ...... 9004–65–3 Sorbic acid, potassium salt ...... 24634–61–5 Cellulose, methyl ether ...... 9004–67–5 Soapbark (Quillaja saponin) ...... 1393–03–9 Cellulose, mixture with cellulose carboxymethyl Sodium alginate ...... 9005–38–3 ether, sodium salt ...... 51395–75–6 Sodium chloride ...... 7647–14–5 Cellulose, pulp ...... 65996–61–4 Syrups, hydrolyzed starch, hydrogenated ...... 68425–17–2 Cellulose, regenerated ...... 68442–85–3 Ultramarine blue (C.I. Pigment Blue 29) ...... 57455–37–5 Citric acid ...... 77–92–9 Urea ...... 57–13–6 Citric acid, 2-(acetyloxy)-, tributyl ester ...... 77–90–7 Vanillin ...... 121–33–5 Citric acid, calcium salt ...... 7693–13–2 Xanthan gum ...... 11138–66–2 Citric acid, calcium salt (2:3) ...... 813–94–5

[67 FR 36537, May 24, 2002]

EDITORIAL NOTE: For FEDERAL REGISTER citations affecting § 180.950, see the List of CFR Sections Affected, which appears in the Finding Aids section of the printed volume and at www.govinfo.gov.

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§ 180.960 Polymers; exemptions from dient in a pesticide chemical formula- the requirement of a tolerance. tion, including antimicrobial pesticide Residues resulting from the use of chemical formulations, are exempted the following substances, that meet the from the requirement of a tolerance definition of a polymer and the criteria under FFDCA section 408, if such use is specified for defining a low-risk poly- in accordance with good agricultural or mer in 40 CFR 723.250, as an inert ingre- manufacturing practices.

Polymer CAS No.

Acetic acid ethenyl ester, polymer with ethane, ethenyltriethoxysilane and so- 913187–38–9 dium ethenesulfonate (1:1); minimum number average molecular weight (in amu), 16,200

Acetic acid ethenyl ester, polymer with ethene and ethenol, minimum number 26221–27–2 average molecular weight (in amu), 20,000

Acetic acid ethenyl ester, polymer with ethenol and (a)-2-propenyl-(w)- 137091–12–4 hydroxypoly (oxy-1,2-ethanediyl) minimum number average molecular weight (in amu), 15,000

Acetic acid ethenyl ester, polymer with 1-ethenyl-2-pyrrolidinone 25086–89–9

Acetic acid ethenyl ester, polymer with oxirane, minimum number average mo- 25820–49–9 lecular weight (in amu), 17,000

Acetic acid ethenyl ester, polymer with sodium 2-methyl-2-[(1-oxo-2-propen-1- 924892–37–5 yl)amino]-1-propanesulfonate (1:1), hydrolyzed, minimum number average molecular weight (in amu), 61,000

Acrylamide-Sodium Acrylamidomethylpropanesulfonate Copolymer, minimum 38193–60–1 number average molecular weight (amu), 1,000,000 daltons.

Acrylic acid-benzyl methacrylate-1-propanesulfonic acid, 2-methyl-2-[(1-oxo-2- 1152297–42–1 propenyl)amino]-, monosodium salt, minimum number average molecular weight (in amu), 1500

Acrylic acid-butyl acrylate-styrene copolymer, minimum number average molec- 25586–20–3 ular weight (in amu), 5,200

Acrylic acid, polymerized, and its ethyl and methyl esters None

Acrylic acid-sodium acrylate-sodium-2-methylpropanesulfonate copolymer, min- 97953–25–8 imum average molecular weight (in amu), 4,500

Acrylic acid-stearyl methacrylate copolymer, minimum number average molec- 27756–15–6 ular weight (in amu), 2,500

Acrylic acid, styrene, a-methyl styrene copolymer, ammonium salt, minimum 89678–90–0 number average molecular weight (in amu), 1,250

Acrylic acid terpolymer, partial sodium salt, minimum number average molec- 151006–66–5 ular weight (in amu), 2,400

Acrylic polymers composed of one or more of the following monomers: Acrylic None acid, butyl acrylate, butyl methacrylate, carboxyethyl acrylate, ethyl acrylate, ethyl methacrylate, hydroxybutyl acrylate, hydroxybutyl methacrylate, hydroxyethyl acrylate, hydroxyethyl methacrylate, hydroxypropyl acrylate, hydroxypropyl methacrylate, isobutyl methacrylate, lauryl methacrylate, methacrylic acid, methyl acrylate, lauryl acrylate, methyl methacrylate and stearyl methacrylate; with none and/or one or more of the following monomers: Ac- rylamide, diethyl maleate, dioctyl maleate, maleic acid, maleic anhydride, monoethyl maleate, monooctyl maleate, N-methyl acrylamide, N,N-dimethyl acrylamide, N-octylacrylamide, and acrylamidopropyl methyl sulfonic acid; and their corresponding ammonium, isopropylamine, monoethanolamine, potassium, sodium triethylamine, and/or triethanolamine salts; the resulting polymer having a minimum number average molecular weight (in amu), 1,200. Acrylonitrile-butadiene copolymer conforming to 21 CFR 180.22, minimum aver- 9003–18–3 age molecular weight (in amu), 1,000

Acrylonitrile-styrene-hydroxypropyl methacrylate copolymer, minimum number None average molecular weight (in amu), 447,000

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Polymer CAS No.

≤a-Alkyl-w-hydroxypoly (oxypropylene) and/or poly (oxyethylene) polymers 9002–92–0; 9004–95–9; 9004–98–2; 9005– where the alkyl chain contains a minimum of six carbons and a minimum 00–9; 9035–85–2; 9038–29–3; 9038–43–1; number average molecular weight (in amu) 1,100 9040–05–5; 9043–30–5; 9087–53–0; 25190–05–0; 24938–91–8; 25231–21–4; 251553–55–6; 26183–52–8; 26468–86–0; 26636–39–5; 27252–75–1; 27306–79–2; 31726–34–8; 34398–01–1; 34398–05–5; 37251–67–5; 37311–00–5; 37311–01–6; 37311–02–7; 37311–04–9; 39587–22–9; 50861–66–0; 52232–09–4; 52292–17–8; 52609–19–5; 57679–21–7; 59112–62–8; 60828–78–6; 61702–78–1; 61723–78–2; 61725–89–1; 61791–13–7; 61791–20–6; 61791–28–4; 61804–34–0; 61827–42–7; 61827–84–7; 62648–50–4; 63303–01–5; 63658–45–7; 63793–60–2; 64366–70–7; 64415–24–3; 64415–25–4; 64425–86–1; 65104–72–5; 65150–81–4; 66455–14–9: 66455–15–0; 67254–71–1; 67763–08–0; 68002–96–0; 68002–97–1; 68131–39–5; 68131–40–8; 68154–96–1; 68154–97–2; 68154–98–3; 68155–01–1; 68213–23–0; 68213–24–1; 68238–81–3; 68238–82–4; 68409–58–5; 68409–59–6; 68439–30–5; 68439–45–2; 68439–46–3; 68439–48–5; 68439–49–6; 68439–50–9; 68439–51–0; 68439–53–2; 68439–54–3; 68458–88–8; 68526–94–3; 68526–95–4; 68551–12–2; 68551–13–3; 68551–14–4; 68603–20–3; 68603–25–8; 68920–66–1; 68920–69–4; 68937–66–6; 68951–67–7; 68954–94–9; 68987–81–5; 68991–48–0; 69011–36–5; 69013–18–9; 69013–19–0; 69227–20–9; 69227–21–0; 69227–22–1; 69364–63–2; 70750–27–5; 70879–83–3; 70955–07–6; 71011–10–4; 71060–57–6; 71243–46–4; 72066–65–0; 72108–90–8; 72484–69–6; 72854–13–8; 72905–87–4; 73018–31–2; 73049–34–0; 74432–13–6; 74499–34–6; 78330–19–5; 78330–20–8; 78330–21–9; 78330–23–1; 79771–03–2; 84133–50–6; 85422–93–1; 97043–91–9; 97953–22–5; 102782–43–4; 103331–86–8; 103657–84–7; 103657–85–8; 103818–93–5; 103819–03–0; 106232–83–1; 111905–54–5; 116810–31–2; 116810–32–3; 116810–33–4; 120313–48–6; 120944–68–5; 121617–09–2; 126646–02–4; 126950–62–7; 127036–24–2; 139626–71–4; 152231–44–2; 154518–36–2; 157627–86–6; 157627–88–8; 157707–41–0; 157707–43–2; 159653–49–3; 160875–66–1; 160901–20–2; 160901–09–7; 160901–19–9; 161025–21–4; 161025–22–5; 166736–08–9; 169107–21–5; 172588–43–1; 176022–76–7; 196823–11–7; 287935–46–0; 288260–45–7; 303176–75–2; 954108–36–2; 2222805–23–2

Amines, coco alkyl, ethoxylated, compounds with acrylic acid-Bu acrylate- 1186094–73–4 methylstyrene-styrene polymer, ammonium salts; minimum number average molecular weight (in amu), 2700

2H-Azepin-2-one, 1-ethenylhexahydro-, homopolymer 25189–83–7

1,3 Benzene dicarboxylic acid, 5-sulfo-, 1,3-dimethyl ester, sodium salt, poly- 212842–88–1 mer with 1,3-benzene dicarboxylic acid, 1,4-benzene dicarboxylic acid, dimethyl 1,4-benzene dicarboxylate and 1,2-ethanediol, minimum number average molecular weight (in amu), 2,580

3,5-Bis(6-isocyanatohexyl)-2H-1,3,5-oxadiazine-2,4,6-(3H,5H)-trione, polymer 87823–33–4 with diethylenetriamine, minimum number average molecular weight (in amu), 1,000,000

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Polymer CAS No.

Polymer of one or more diglycidyl ethers of bisphenol A, resorcinol, glycerol, None cyclohexanedimethanol, neopentyl glycol, and polyethylene glycol with one or more of the following: Polyoxypropylene diamine, polyoxypropylene triamine, N-aminoethyl-piperazine, trimethyl-1,6-hexanediamine isophorone diamine, N,N-dimethyl-1,3-diaminopropane, nadic methyl anhydride, 1,2-cyclohexane- dicarboxylic anhydride and 1,2,3,6-tetrahydrophthalic anhydride, minimum number average molecular weight (in amu), 400,000

Butadiene-styrene copolymer None

Butanedioic acid, 2-methylene-, homopolymer, sodium salt, minimum number 26099–89–8 average molecular weight (in amu), 3936

Butanedioic acid, 2-methylene-, polymer with 1,3-butadiene, ethenylbenzene 36089–06–2 and 2-hydroxyethyl 2-propenoate, minimum number average molecular weight (in amu), 10,000

Butanedioic acid, 2-methylene-, polymer with 2,5-furandione, sodium and am- 556055–76–6 monium salts, hydrogen peroxide-initiated, minimum number average molec- 701908–99–8 ular weight (in amu), 2,500–3,000

Butanedioic acid, 2-methylene-, telomer with sodium phosphinate (1:1), acidi- 1663489–14–2 fied, potassium salt minimum number average molecular weight (in amu), 3800

1,4-Butanediol-methylenebis(4-phenylisocyanate)-poly(tetramethylene glycol) 9018–04–6 copolymer, minimum molecular weight (in amu) 158,000

Butene, homopolymer 9003–29–6

2-butenedioic acid (2Z)-, monobutyl ester, polymer with methoxyethene, sodium 205193–99–3 salt, minimum number average molecular weight (in amu), 18,200

2-Butenedioic acid (Z)-, polymer with ethenol and ethenyl acetate, sodium salt, 139871–83–3 minimum number average molecular weight (in amu), 75,000

Butyl acrylate-vinyl acetate-acrylic acid copolymer, minimum number average 65405–40–5 molecular weight (in amu), 18,000

Carbonic acid, diethyl ester, polymer with a-hydro-w-hydroxypoly[oxy(methyl- 1147260–65–8 1,2-ethanediyl)] ether with 2-ethyl-2-(hydroxymethyl)-1,3-propanediol (3:1), ester with a-[[[[5-(carboxyamino)-1,3,3- trimethylcyclohexyl]methyl]amino]carbonyl]-w-methoxypoly(oxy-1,2- ethanediyl), minimum number average molecular weight (in amu), 1,900

Castor oil, ethoxylated, dioleate, minimum number average molecular weight (in 110531–96–9 amu), 1260.

Castor oil, ethoxylated, oleate, minimum number average molecular weight (in 220037–02–5 amu), 1,600

Castor oil, polymer with adipic acid, linoleic acid, oleic acid and ricinoleic acid, 1357486–09–9 minimum number average molecular weight (in amu), 3,500

Castor oil, polyoxyethylated; the poly(oxyethylene) content averages 5–54 None moles

Cellulose carboxymethyl ether, potassium salt, minimum number average mo- 54848–04–3 lecular weight 9587 Daltons

Chlorinated polyethylene 64754–90–1

Cross-linked nylon-type polymer formed by the reaction of a mixture of None sebacoyl chloride and polymethylene polyphenylisocycanate with a mixture of ethylenediamine and diethylenetriamine

Cross-linked polyurea-type encapsulating polymer None

D-Glucitol, polymer with decanedioic acid, docosanoate, minimum number av- 943440–33–3 erage molecular weight (in amu) 1,100

D-Glucitol, polymer with decanedioic acid, docosanoate, minimum number av- 1681043–28–6 erage molecular weight (in amu) 1,100

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Polymer CAS No.

D-Glucitol, polymer with decanedioic acid, octadecanoate, minimum number av- 68562–93–6 erage molecular weight (in amu) 1,100

D-Glucitol, polymer with decanedioic acid and 1,3-propanediol, minimum num- 1681043–31–1 ber average molecular weight (in amu) 1,100

D-Glucitol, polymer with decanedioic acid and 1,3-propanediol, octadecanoate, 1681043–33–3 minimum number average molecular weight (in amu) 1,100

Dimethylpolysiloxane minimum number average molecular weight (in amu), 63148–62–9 6,800

Dimethyl silicone polymer with silica, minimum number average molecular 67762–90–7 weight (in amu), 1,100,000

a-(o,p-Dinonylphenyl)-w-hydroxypoly(oxyethylene) produced by condensation of 9014–93–1 1 mole of dinonylphenol (nonyl group is a propylene trimer isomer) with an average of 140-160 moles of ethylene oxide

Docosyl methacrylate-acrylic acid copolymer, or docosyl methacrylate-octadecyl None methacrylate-acrylic acid copolymer, minimum number average molecular weight (in amu), 3,000

1,12-Dodecanediol dimethacrylate polymer, minimum molecular weight (in None amu), 100,000

a-(p-Dodecylphenyl)-w-hydroxypoly(oxyethylene) produced by the condensation 9014–92–0 of 1 mole of dodecylphenol (dodecyl group is a propylene tetramer isomer) 26401–47–8 with an average of 30-70 moles of ethylene oxide

1,2-Ethanediamine, N1-(2-aminoethyl)-, polymer with 2,4-diisocyanato-1- 35297–61–1 methylbenzene, minimum number average molecular weight (in amu), one million

1, 2-Ethanediamine, polymer with methyl oxirane and oxirane, minimum num- 26316–40–5 ber average molecular weight (in amu), 1,100

Ethylene glycol dimethyacrylate-lauryl methacrylate copolymer, minimum mo- None lecular weight (in amu), 100,000

Ethylene glycol dimethacrylate polymer, minimum molecular weight (in amu), None 100,000

Fatty acids, montan-wax, ethoxylated, minimum number average molecular 68476–04–0 weight (in amu), 1800

Fatty acids, C18-unsatd., dimers, polymers with docosanoic acid and sorbitol, 1685270–83–0 minimum number average molecular weight (in amu) 1,100

Fatty acids, C18-unsatd., dimers, polymers with docosenoic acid and sorbitol, 1685271–02–6 minimum number average molecular weight (in amu) 1,100

Fatty acids, C18-unsatd., dimers, polymers with docosenoic acid, 1,3- 1685271–04–8 propanediol and sorbitol, minimum number average molecular weight (in amu) 1,100

Fatty acids, C18-unsatd., dimers, polymers with docosanoic acid, 1,3- 1685270–84–1 propanediol and stearic acid, minimum number average molecular weight (in amu) 1,100

Fatty acids, C18-unsatd., dimers, polymers with 1,3-propanediol, sorbitol and 1685271–01–5 stearic acid

Fatty acids, C18-unsatd., dimers, polymers with sorbitol and stearic acid, min- 1685270–99–8 imum number average molecular weight (in amu) 1,100

Fatty acids, C18-unsatd., dimers, polymers with ethylenediamine and stearyl al- 363162–42–9 cohol, minimum number average molecular weight (in amu) 1,400

Fatty acids, C18-unsatd., dimers, hydrogenated, polymers with ethylenediamine, 678991–29–2 neopentyl glycol and stearyl alcohol, minimum number average molecular weight (in amu) 1,400

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Polymer CAS No.

Fatty acids, C18-unsatd., dimers, hydrogenated, polymers with ethylenediamine 951153–32–5 and stearyl alcohol, minimum number average molecular weight (in amu) 1,400

Fatty acids, C18-unsatd., dimers, polymers with 1-docosanol and ethylene- 1699751–19–3 diamine, minimum number average molecular weight (in amu) 1,400

Fatty acids, C18-unsatd., dimers, polymers with cetyl alcohol, neopentyl glycol 1699751–23–9 and trimethylenediamine, minimum number average molecular weight (in amu) 1,400

Fatty acids, C18-unsatd., dimers, polymers with hexamethylenediamine and ste- 1699751–24–0 aryl alcohol, minimum number average molecular weight (in amu) 1,400

Fatty acids, C18-unsatd., dimers, hydrogenated, polymers with cetyl alcohol and 1699751–25–1 ethylenediamine, minimum number average molecular weight (in amu) 1,400

Fatty acids, C18-unsatd., dimers, hydrogenated, polymers with neopentyl glycol, 1699751–28–4 stearyl alcohol and trimethylenediamine, minimum number average molecular weight (in amu) 1,400

Fatty acids, C18-unsatd., dimers, polymers with 1-docosanol and 1699751–29–5 trimethylenediamine, minimum number average molecular weight (in amu) 1,400

Fatty acids, C18-unsatd., dimers, polymers with 1-docosanol, 1699751–31–9 hexamethylenediamine and neopentyl glycol, minimum number average molecular weight (in amu) 1,400

Fatty acids, C18-unsatd., dimers, polymers with docosanoic acid, 1,3- 1685271–04–8 propanediol and sorbitol, minimum number average molecular weight (in amu) 1,400

Fatty acids, rape-oil, triesters with polyethylene glycol ether with glycerol (3:1); 688045–21–8 minimum number average molecular weight (in amu), 1800. Fatty acids, tall-oil, ethoxylated propoxylated, minimum number average molec- 67784–86–5 ular weight (in amu), 2,009

Formaldehyde, polymer with a-[bis(1-phenylethyl)phenyl]-w-hydroxypoly(oxy- 157291–93–5 1,2-ethanediyl), number average molecular weight (in amu), 1,803

Formaldehyde, polymer with 1,3-benzenediol, ethers with polyethylene glycol 1998118–32–3 mono-Me ether, minimum number average molecular weight (in amu) 1,000,000. Formaldehyde, polymer with 1,3-benzenediol, 2-methyloxirane and oxirane, 1998118–31–2 ethers with polyethylene glycol mono-Me ether, minimum number average molecular weight (in amu) 1,000,000. Formaldehyde, polymer with 2-methyloxirane and 4-nonylphenol, minimum 37523–33–4 number average molecular weight (in amu), 4,000

Formaldehyde, reaction products with melamine, minimum number average 94645–56–4 molecular weight (in amu), 10000

Formaldehyde, reaction products with melamine and methanol, minimum num- 94645–53–1 ber average molecular weight (in amu), 10000

Fumaric acid-isophthalic acid-styrene-ethylene/propylene glycol copolymer, min- None imum average molecular weight (in amu), 1 × 1018

2,5-Furandione, polymer with ethenylbenzene, hydrolyzed, 3- 1062609–13–5 (dimethylamino)propyl imide, imide with polyethylene-polypropylene glycol 2- aminopropyl me ether, 2,2′-(1,2-diazenediyl)bis[2-methylbutanenitrile]-initiated, minimum number average molecular weight (in amu), 5,816

2,5-Furandione, polymer with ethenylbenzene, reaction products with poly- 162568–32–3 ethylene-polypropylene glycol 2-aminopropyl Me ether; minimum number average molecular weight (in amu), 14,000

2,5-Furandione, polymer with methoxyethene, butyl ethyl ester, sodium salt, 1471342–08–1 minimum number average molecular weight (in amu), 18,200

Hexadecyl acrylate-acrylic acid copolymer, hexadecyl acrylate-butyl acrylate- None acrylic acid copolymer, or hexadecyl acrylate-dodecyl acrylate-acrylic acid copolymer, minimum number average molecular weight (in amu), 3,000

787

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Polymer CAS No.

Hexamethyl disilizane, reaction product with silica, minimum number average 68909–20–6 molecular weight (in amu), 645,000

1,6-Hexanediol dimethyacrylate polymer, minimum molecular weight (in amu), None 100,000

a-Hydro-w-hydroxy-poly(oxyethylene) C8 alkyl ether citrates, poly(oxyethylene) 330977–00–9 content is 4–12 moles, minimum number average molecular weight (in amu) 1,300

a-Hydro-w-hydroxy-poly(oxyethylene) C10–C16-alkyl ether citrates, 330985–58–5 poly(oxyethylene) content is 4–12 moles, minimum number average molecular weight (in amu) 1,100

a-Hydro-w-hydroxy-poly(oxyethylene) C16–C18-alkyl ether citrates, 330985–61–0 poly(oxyethylene) content is 4–12 moles, minimum number average molecular weight (in amu) 1,300

a-Hydro-w-hydroxypoly(oxyethylene), minimum number average molecular 25322–68–3 weight (in amu), 17,000

a-Hydro-w-hydroxypoly(oxyethylene)poly (oxypropylene) poly(oxyethylene) None block copolymer; the minimum poly(oxypropylene) content is 27 moles and the minimum molecular weight (in amu) is 1,900

a-Hydro-w-hydroxypoly(oxypropylene); minimum molecular weight (in amu) None 2,000

12-Hydroxystearic acid-polyethylene glycol copolymer, minimum number aver- 70142–34–6 age molecular weight (in amu), 3,690

Isodecyl alcohol ethoxylated (2–8 moles) polymer with chloromethyl oxirane, None minimum number average molecular weight (in amu) 2,500

Lauryl methacrylate-1,6-hexanediol dimethacrylate copolymer, minimum molec- None ular weight (in amu), 100,000

Lignosulfonic acid, calcium, comp. with 1,6 hexanediamine polymer with guani- 1905409–74–6 dine hydrochloride (1:1), minimum number average molecular weight (in amu); 4,500 daltons

Maleic acid-butadiene copolymer None

Maleic acid monobutyl ester-vinyl methyl ether copolymer, minimum average 25119–68–0 molecular weight (in amu), 52,000

Maleic acid monoethyl ester-vinyl methyl ether copolymer, minimum average 25087–06–3 molecular weight (in amu), 46,000

Maleic acid monoisopropyl ester-vinyl methyl ether copolymer, minimum aver- 31307–95–6 age molecular weight (in amu), 49,000

Maleic anhydride-diisobutylene copolymer, sodium salt, minimum number aver- 37199–81–8 age molecular weight (in amu) 5,0007–18,000

Maleic anhydride-methylstyrene copolymer sodium salt, minimum number aver- 60092–15–1 age molecular weight (in amu), 15,000

Maleic anhydride-methyl vinyl ether, copolymer, average molecular weight (in None amu), 250,000

Maltodextrin-vinyl pyrrolidinone copolymer, minimum number average molecular 1323833–56–2 weight (in amu), 21,000

Methacrylic acid-methyl methacrylate-polyethylene glycol methyl ether meth- 100934–04–1 acrylate copolymer, minimum number averge molecular weight (in amu), 3,700

Methacrylic acid-methyl methacrylate-polyethylene glycol monomethyl ether 111740–36–4 methacrylate graft copolymer, minimum number average molecular weight (in amu), 1,800

Methacrylic copolymer, minimum number average molecular weight (in amu), 63150–03–8 15,000

788

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Polymer CAS No.

Methyl methacrylate-methacrylic acid-monomethoxypolyethylene glycol meth- 119724–54–8 acrylate copolymer,) minimum number average molecular weight (in amu), 2,730

Methyl methacrylate-2-sulfoethyl methacrylate-dimethylaminoethylmethacrylate- None glycidyl methacrylate-styrene-2-ethylhexyl acrylate graft copolymer, minimum average molecular weight (in amu), 9,600

2-methyl-2-[(1-oxo-2-propenyl)amino]-1-propanesulfonic acid monosodium salt 2115702–24–2 polymer with 2-propenoic acid, 2-methyl-, C12-16 alkyl esters, minimum number average molecular weight (in amu), 10,000

Methyl vinyl ether-maleic acid copolymer), minimum number average molecular 25153–40–6 weight (in amu), 75,000

Methyl vinyl ether-maleic acid copolymer, calcium sodium salt, minimum num- 62386–95–2 ber average molecular weight (in amu), 900,000

Monophosphate ester of the block copolymer a-hydro-w- None hydroxypoly(oxyethylene) poly(oxypropylene) poly(oxyethylene); the poly(oxypropylene) content averages 37–41 moles, average molecular weight (in amu), 8,000

a-(p-Nonylphenyl)-w-hydroxypoly(oxyethylene) mixture of dihydrogen phosphate None and monohydrogen phosphate esters and the corresponding ammonium, calcium, magnesium, monoethanolamine, potassium, sodium, and zinc salts of the phosphate esters; the nonyl group is a propylene trimer isomer and the poly(oxyethylene) content averages 30 moles

a-(p-Nonylphenyl)-w-hydroxypoly(oxyethylene) sulfate, and its ammonium, cal- None cium, magnesium, monoethanolamine, potassium, sodium, and zinc salts; the nonyl group is a propylene trimer isomer and the poly(oxyethylene) content averages 30-90 moles of ethylene oxide

a-(p-Nonylphenyl-w-hydroxypoly(oxypropylene) block polymer with None poly(oxyethylene); polyoxypropylene content of 10–60 moles; polyoxyethylene content of 10–80 moles; molecular weight (in amu), 1,200– 7,100.

a-(r-Nonylphenyl)poly(oxypropylene) block polymer with poly(oxyethylene); poly 37251–69–7 oxyethylene content 30 to 90 moles; minimum number average molecular weight (in amu), 1,889

Octadecanoic acid, 12-hydroxy-, homopolymer, ester with a, a’, a’’-1,2,3- 1939051–18–9 propanetriyltris[w-hydroxypoly(oxy-1,2-ethanediyl)], minimum number average molecular weight (in amu), 5,000

Octadecanoic acid, 12-Hydroxy-, Homopolymer Ester with 2-Methylloxirane 1373125–59–7 Polymer with Oxirane monobutyl Ether, minimum number average molecular weight (in amu), 4,500

Octadecanoic acid, 12-hydroxy-, homopolymer, octadecanoate minimum num- 58128–22–6) ber average molecular weight (in amu), 1,370

a-cis-9-Octadecenyl-w-hydroxypoly(oxyethylene); the octadecenyl group is de- None rived from oleyl alcohol and the poly(oxyethylene) content averages 20 moles

Octadecyl acrylate-acrylic acid copolymer, octadecyl acrylate-dodecyl acrylate- None acrylic acid copolymer, octadecyl methacrylate-butyl acrylate-acrylic acid copolymer, octadecyl methacrylate-hexyl acrylate-acrylic acid copolymer, octadecyl methacrylate-dodecyl acrylate-acrylic acid copolymer, or octadecyl methacrylate-dodecyl methacrylate-acrylic acid copolymer, minimum number average molecular weight (in amu) 3,000

Oleic acid diester of a-hydro-w-hydroxypoly(oxyethylene); the None poly(oxyethylene), average molecular weight (in amu), 2,300

2-oxepanone, homopolymer, minimum number average molecular weight (in 24980–41–4 amu) 52,000

Oxirane, decyl-, reaction products with polyethylene-polypropylene glycol ether 903890–89–1 with trimethylolpropane (3:1)

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Polymer CAS No.

Oxirane, hexadecyl-, reaction products with polyethylene-polypropylene glycol 893427–80–0 ether with trimethylolpropane (3:1)

Oxirane, 2-methyl-, polymer with oxirane, dimethyl ether, minimum number av- 61419–46–3 erage molecular weight (in amu), 2,800

Oxirane, methyl-, polymer with oxirane, ether with 2-ethyl-2-(hydroxymethyl)- 903890–90–4 1,3-propanediol (3:1), reaction products with tetradecyloxirane

Oxirane, methyl-, polymer with oxirane, mono[2-(2-butoxyethoxy) ethyl] ether, 85637–75–8 minimum number average molecular weight (in amu), 2,500

Oxirane, methyl-, polymer with Oxirane, Monobutyl Ether 9038–95–3

Oxirane, 2-methyl-, polymer with oxirane, mono[2-[2-(2-methoxymethylethoxy) CAS Reg. No. 2112825–11–1. methylethoxy]methylether] ether, minimum number average molecular weight (in amu), 1400 daltons. Oxirane, 2-methyl-, polymer with oxirane, minimum number average molecular 9003–11–6 weight (in amu), 1,100

Oxirane, 2-methyl-, polymer with oxirane, mono [2-[2-(2- 926031–36–9 butoxymethylethoxy)methylethoxy]methylethyl] ether, minimum number average molecular weight (in amu), 3,000

Oxirane, 2-methyl, polymer with oxirane, hydrogen sulfate, ammonium salt; av- 57608–14–7 erage molecular weight (in amu), 1800

Oxirane, 2-methyl, polymer with oxirane, hydrogen sulfate, potassium salt; av- 1838191–48–2 erage molecular weight (in amu), 2100

Oxirane, phenyl, polymer with oxirane, monooctyl ether, minimum average mo- 83653–00–3 lecular weight (in amu) 1,200

Polyamide polymer derived from sebacic acid, vegetable oil acids with or with- None out dimerization, terephthalic acid and/or ethylenediamine

Polyethylene glycol-polyisobutenyl anhydride-tall oil fatty acid copolymer, min- 68650–28–2 imum number average molecular weight (in amu), 2,960

Polyethylene, oxidized, minimum number average molecular weight (in amu), None 1,200

Polyglycerol polyricinoleate; minimum number average molecular weight (in 29894–35–7 amu), 2,500

Polymers produced by the reaction of either 1,6-hexanediisocyanate; 2,4,4- 1161844–26–3, 1161844–30–9, 1161844–43– trimethyl-1,6-hexanediisocyanate; 5-isocyanato-1-(isocyanatomethyl)- 4, 1161844–51–4, 1161844–53–6, 693252– fxsp0;1,3,3-trimethyIcyclohexane (isophoronediisocyanate); 4,4′-methylene- 31–2, 162993–60–4, 630102–86–2 bis-1,1′-cyclohexanediisocyanate; 4,4′-methylene-bis-1,1′ benzyldiisocyanate; or 1,3-bis-(2-isocyanatopropan-2-yl)benzene with polyethylene glycol and end-capped with one or a mixture of more than one of octanol, decanol, dodecanol, tetradecanol, hexadecanol, octadecanol, and octadec-9-enol or polyethyleneglycol ethers of octanol, decanol, dodecanol, tetradecanol, hexadecanol, octadecanol, and octadec-9-enol, minimum number average molecular weight (in amu), 20,000

Polymethylene polyphenylisocyanate, polymer with ethylene diamine, None diethylene triamine and sebacoyl chloride, cross-linked; minimum number average molecular weight (in amu), 100,000

Polyoxyalkylated glycerol fatty acid esters; the mono-, di-, or triglyceride mix- 61791–23–9, 68201–46–7, 68440–49–3, tures of C8 through C22, primarily C8 through C18 saturated and unsaturated, 68458–88–8, 68606–12–2, 68648–38–4, fatty acids containing up to 15% water by weight reacted with a minimum of 70377–91–2, 70914–02–2, 72245–12–6, three moles of either ethylene oxide or propylene oxide; the resulting poly- 72698–41–3, 180254–52–8, 248273–72–5, oxyalkylated glycerol ester polymer minimum number average molecular 308063–50–5, 952722–33–7 weight (in amu), 1,500

790

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Polymer CAS No.

Polyoxyalkylated sorbitan fatty acid esters with C6 through C22 aliphatic 81776–11–6, 87090–31–1, 88895–72–1, alkanoic and/or alkenoic fatty acids, branched or linear, the resulting 103171–31–9, 161026–53–5, 1472644–80– polyoxyalkylene sorbitan esters minimum number average molecular weight 6, 1472644–81–7, 1472644–84–0, (in amu), 1,300 1472644–85–1, 1472644–87–3, 1472644– 88–4, 1472654–83–3, 1472655–32–5, 1472661–05–4, 1472661–17–8, 1472663– 59–4, 1472663–64–1, 1472663–66–3, 1472663–92–5, 1472668–03–3

Polyoxyalkylated trimethylopropanes with 20 to 80 moles of ethylene and/or 25765–36–0; 29860–47–7; 37339–03–0; propylene oxide, fatty acid esters with C8 through C22 aliphatic alkanoic and/ 52624–57–4; 58090–24–7; 63964–38–5; or alkenoic fatty acids, branched or linear; minimum number average molec- 72939–62–9; 74521–14–5; 75300–70–8; ular weight (in amu), 3,000 75300–90–2; 84271–03–4; 84271–04–5; 86850–92–2; 107120–02–5; 133331–01–8; 137587–60–1; 149797–40–0; 149797–41–1; 150695–97–9; 152130–24–0; 163349–94–8; 163349–95–9; 163349–96–0; 163349–97–1; 163349–98–2; 165467–70–9; 183619–46–7; 183619–50–3; 185260–01–9; 202606–04–0; 210420–84–1; 233660–70–3; 263011–96–7; 283602–94–8; 701980–40–7; 872038–58–9; 875709–44–7; 875709–45–8; 875709–46–9; 875709–47–0; 879898–63–2; 910038–01–6; 1190748–04–9; 1225384–02–0; 1428944– 41–5; 1446498–15–2.

Poly(oxy-1,2-ethanediyl), a-hydro-w-hydroxy-, polymer with 1, 1′-methylene-bis- 39444–87–6 [4-isocyanatocyclohexane], minimum number average molecular weight (in amu), 1800

Polyoxyethylated primary amine (C14–C18); the fatty amine is derived from an None animal source and contains 3% water; the poly(oxyethylene) content averages 20 moles

Polyoxyethylated sorbitol fatty acid esters; the polyoxyethylated sorbitol solution None containing 15% water is reacted with fatty acids limited to C12, C14, C16, and C18, containing minor amounts of associated fatty acids; the poly(oxyethylene) content averages 30 moles.

Polyoxyethylated sorbitol fatty acid esters; the sorbitol solution containing up to None 15% water is reacted with 20–50 moles of ethylene oxide and aliphatic alkanoic and/or alkenoic fatty acids C8 through C22 with minor amounts of associated fatty acids; the resulting polyoxyethylene sorbitol ester having a minimum molecular weight (in amu), 1,300

Poly(oxyethylene/oxypropylene) monoalkyl (C6–C10) ether sodium fumarate 102900–02–7 adduct, minimum number average molecular weight (in amu), 1,900

Poly[oxy(methyl-1,2-ethanediyl)], a-[(9Z)-1-oxo-9-octadecen-1-yl]-w-[[(9Z)-1-oxo- 26571–49–3 9-octadecen-1yl]oxy]-, minimum number average molecular weight (in amu) 2,300

Polyoxymethylene copolymer, minimum number average molecular weight (in None amu), 15,000

Poly(oxypropylene) block polymer with poly(oxyethylene), molecular weight (in None amu), 1,800–16,000

Poly(phenylhexylurea), cross-linked, minimum average molecular weight (in None amu), 36,000

Polypropylene 9003–07–0

Polystyrene, minimum number average molecular weight (in amu), 50,000 9003–53–6

Polytetrafluoroethylene 9002–84–0

Polyvinyl acetate, copolymer with maleic anhydride, partially hydrolyzed, so- None dium salt, minimum number average molecular weight (in amu), 53,000

Polyvinyl acetate, minimum molecular weight (in amu), 2,000 None

Polyvinyl acetate—polyvinyl alcohol copolymer, minimum number average mo- 25213–24–5 lecular weight (in amu), 50,000

791

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Polymer CAS No.

Polyvinyl acetate—polyvinyl alcohol copolymer, minimum number average mo- 25213–24–5 lecular weight (in amu), 14,000

Polyvinyl alcohol 9002–89–5

Polyvinyl chloride None

Polyvinyl chloride, minimum number average molecular weight (in amu), 29,000 9002–86–2

Polyvinylpyrrolidone butylated polymer, minimum number average molecular 26160–96–3 weight (in amu), 9,500

Poly(vinylpyrrolidone), minimum number average molecular weight (in amu), 9003–39–8 4,000

Poly(vinylpyrrolidone-1-eicosene), minimum average molecular weight (in amu), 28211–18–9 3,000

Poly(vinylpyrrolidone-1-hexadecene), minimum average molecular weight (in 63231–81–2 amu), 4,700

Propanesulfonic acid, 2-methyl-2-[(1-oxo-2-propen-1-y1)amino]-, homopolymer, 55141–01–0 sodium salt, minimum number average molecular weight (in amu) 14,000.

1-propanesulfonic acid, 2-methyl-2-[(1-oxo-2-propenyl)amino]-, monosodium 107568–12–7 salt, polymer with ethenol and ethenyl acetate, minimum number average molecular weight (in amu) 50,000

1-Propanesulfonic acid, 2-methyl-2-[(1-oxo-2-propen-1-y1)amino]-, sodium salt 35641–59–9 (1:1), homopolymer, minimum number average molecular weight (in amu) 14,000.

2-Propene-1-sulfonic acid sodium salt, polymer with ethenol and ethenyl ace- None tate, number average molecular weight (in amu) 6,000–12,000

2-Propenoic acid, butyl ester, polymer with 1,6-diisocyanatohexane, N- 1469998–09–1 (hydroxymethyl)-2-methyl-2-propenamide and 2-propenenitrile, minimum number average molecular weight (in amu), 100,000

2-Propenoic acid, butyl ester, polymer with ethenyl acetate and sodium 66573–43–1 ethenesulfonate, minimum number average molecular weight (in amu), 20,500

2-propenoic acid, butyl ester, polymer with ethenylbenzene, methyl 2-methyl-2- 27306–39–4 propenoate and 2-propenoic acid (in amu), 1900.

2-Propenoic acid, butyl ester, polymer with ethyl 2-propenoate and N- 33438–19–6 (hydroxymethyl)-2-propenamide, minimum number average molecular weight (in amu), 30,000

2-Propenoic acid, 2-ethylhexyl ester, polymer with ethenylbenzene 14,000 dal- 25153–46–2 tons

2-Propenoic acid, 2-ethylhexyl ester, polymer with ethenylbenzene and 2- 68240–06–2 methylpropyl 2-methyl-2-propenoate, minimum number average molecular weight (in amu), 18,000

2-propenoic acid, homopolymer, ester with a-[2,4,6-tris(1-phenylethyl)phenyl]-w- 1477613–46–9 hydroxypoly(oxy-1,2-ethanediyl), compd. with 2,2′,2″-nitrilotris[ethanol]), minimum number average molecular weight (in amu), 10,000. 2-Propenoic acid, 2-hydroxyethyl ester, polymer with a-[4-(ethenyloxy)butyl]-w- 1007234–89–0 hydroxypoly (oxy-1,2-ethanediyl), minimum number average molecular weight (in amu), 17,000

[2-propenoic acid, 2-methyl-, C12-16-alkyl esters, telomers with 1- 950207–35–9 dodecanethiol, polyethylene-polypropylene glycol ether with propylene glycol monomethacrylate (1:1), and styrene 2,2’-(1,2-diazenediyl)bis[2- methylbutanenitrile]-initiated, minimum number average molecular weight (in amu), 4,000

2-propenoic acid, 2-methyl-, dodecyl ester, polymer with 1-ethenyl-2- 193743–10–1 pyrrolidinone and a-(2-methyl-1-oxo-2-propen-1-yl)-w-methoxypoly(oxy-1,2- ethanediyl), minimum number average molecular weight (in amu), 20,600

792

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Polymer CAS No.

2-Propenoic acid, methyl ester, polymer with ethene and 2,5-furandione, min- 88450–35–5 imum number average molecular weight (in amu), 10,500

2-Propenoic acid, methyl ester, polymer with ethenyl acetate, hydrolyzed, so- 886993–11–9 dium salts

2-Propenoic acid, 2-methyl-, 2-ethylhexyl ester, telomer with 1-dodecanethiol, 1283712–50–4 ethenylbenzene and 2-methyloxirane polymer with oxirane monoether with 1,2-propanediol mono(2-methyl-2-propenoate), hydrogen 2-sulfobutanedioate, sodium salt, 2, 2′-(1,2-diazenediyl)bis[2-methylpropanenitrile]-initiated, minimum number average molecular weight (in amu), 1,200

2-Propenoic acid, 2-methyl-, 2-methylpropyl ester, homopolymer, minimum 9011–15–8 number average molecular weight (in amu), 55,000

2-Propenoic acid, 2-methyl-, 2-oxiranylmethyl ester, polymer with butyl 2- 58499–26–6 propenoate, ethenylbenzene and 2-ethylhexyl 2-propenoate, minimum number average molecular weight (in amu), 3,600.

2-propenoic acid, 2-methyl-, 2-oxiranylmethyl ester, polymer with ethene, eth- 518057–54–0 enyl acetate, ethenyltrimethoxysilane and sodium ethenesulfonate (1:1), minimum number average molecular weight (in amu), 20,000.

2-Propenoic acid, 2-methyl-, phenylmethyl ester, polymer with 2-propenoic acid, 1574486–33–1 peroxydisulfuric acid ([(HO)S(O)2]2O2) sodium salt (1:2)-initiated, compounds with diethanolamine, minimum number average molecular weight (in amu), 2,000

2-Propenoic acid, 2-methyl-, phenylmethyl ester, polymer with 2-propenoic acid CASRN 1246766–57–3 and sodium 2-methyl-2-[(1-oxo-2-propen-1-yl)amino]-1-propanesulfonate (1:1), peroxydisulfuric acid ([HO)S(O)2]202) sodium salt (1:2)-initiated minimum number average molecular weight >1,000 Daltons; maximum number average molecular weight 10,000 Daltons

2-Propenoic acid, 2-methyl-, polymer with butyl 2-methyl-2-propenoate, butyl 2- 481053–27–4 propenoate, N-(1,1-dimethyl-3-oxobutyl)-2-propenamide, ethenylbenzene, 2- ethylhexyl 2-propenoate and methyl 2-methyl-2-propenoate, minimum number average molecular weight (in amu), 7,300

2-Propenoic acid, 2-methyl-, polymer with butyl 2-propenoate and 25036–16–2 ethenylbenzene, minimum number average molecular weight (in amu), 17,000

2-Propenoic acid, 2-Methyl-, Polymer with Butyl 2-Propenoate, Methyl 2-Methyl- 153163–36–1 2-Propenoate, Methyl 2-Propenoate and 2-Propenoic Acid, graft, Compound with 2-Amino-2-Methyl-1-Propanol

2-Propenoic Acid, 2-Methyl-, Polymer with Ethenylbenzene, 2-Ethylhexyl 2- 146753–99–3 Propenoate, 2-Hydroxyethyl 2-Propenoate, N-(Hydroxymethyl) -2-Methyl-2- Propenamide and Methyl 2-Methyl-2-Propenoate, Ammonium Salt

2-Propenoic acid, 2-methyl-, polymers with Bu acrylate, Et acrylate, Me meth- 890051–63–5 acrylate and polyethylene glycol methacrylate C16-18-alkyl ethers, minimum number average molecular weight (in amu), 13,000

2-propenoic acid, 2-methyl-, polymers with tert-Bu acrylate, Me methacrylate, 1515872–09–9 polyethylene glycol methacrylate C16-C18-alkyl ethers and vinylpyrrolidone, tert-Bu 2-ethylhexaneperoxoate-initiated, compounds with 2-amino-2-methyl- 1-propanol, minimum number average molecular weight (in amu), 2,600. 2-Propenoic acid, 2-methyl-, telomer with 2-ethylhexyl 2-propenoate, 2-propanol 1260001–65–7 and sodium 2-methyl-2-[(1-oxo-2-propen-1-yl) amino]-1-propanesulfonate (1:1), sodium salt, minimum number average molecular weight (in amu): 2,900

2-Propenoic acid, monoester with 1,2-propanediol, polymer with a-[4- 955015–23–3 (ethenyloxy) butyl]-w-hydroxypoly (oxy-1,2-ethanediyl) and 2,5-furandione, minimum number average molecular weight (in amu), 25,000

2-propenoic acid polymer, with 1,3-butadiene and ethenylbenzene, minimum 25085–39–6 number average molecular weight (in amu), 9400

2-Propenoic acid, polymer with butyl 2-propenoate, ethenylbenzene and (1- 360564–31–4 methylethenyl) benzene, ammonium salt, minimum number average molecular weight (in amu), 2,300

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Polymer CAS No.

2-Propenoic acid, polymer with ethenyl acetate, ethenylbenzene, 2-ethylhexyl 85075–52–1 2-propenoate and ethyl 2-propenoate, minimum number average molecular weight (50,149 Daltons)

2-Propenoic acid, polymer with ethenylbenzene and (1-methylethenyl)benzene, 52831–04–6 minimum number average molecular weight (in amu), 2,000

2-Propenoic acid, polymer with ethenylbenzene and (1-methylethenyl) benzene, 129811–24–1 sodium salt, minimum number average molecular weight (in amu), 2,800

2-Propenoic acid, polymer with a-[4-(ethenyloxy) butyl]-w-hydroxypoly (oxy-1,2- 251479–97–7 ethanediyl) and 2,5-furandione, sodium salt, minimum number average molecular weight (in amu), 25,000

2-Propenoic acid, polymer with a-[4-(ethenyloxy) butyl]-w-hydroxypoly (oxy-1,2- 518026–64–7 ethanediyl) and 1,2-propanediol mono-2-propenoate, potassium sodium salt, minimum number average molecular weight (in amu), 16,000

2-Propenoic acid, polymer with a-[4-(ethenyloxy) butyl]-w-hydroxypoly (oxy-1, 2- 250591–84–5 ethanediyl), sodium salt, minimum number average molecular weight (in amu), 24,000

2-Propenoic acid, polymer with 2-propenamide, sodium salt, minimum number 25085–02–3 average molecular weight (in amu), 18,000

2-Propenoic acid, sodium salt, polymer with 2-propenamide, minimum number 25987–30–8 average molecular weight (in amu), 18,000

2-Propenoic, 2-methyl-, polymers with ethyl acrylate and polyethylene glycol 888969–14–0 methylacrylate C18-22 alkyl ethers

2-Pyrrolidone, 1-ethenyl-, polymer with ethenol, minimum number average mo- 26008–54–8 lecular weight (in amu), 23,000

Silane, dichloromethyl- reaction product with silica minimum number average 68611–44–9 molecular weight (in amu), 3,340,000

Silane, trimethoxy[3-(oxiranylmethoxy)propyl]-, hydrolysis products with silica, 68584–82–7 minimum number average molecular weight (in amu), 640,000

Silicic acid, sodium salt, reaction products with chlorotrimethylsilane and iso- None propyl alcohol, reaction with poly(oxypropylene)-poly(oxyethylene) glycol, minimum number average molecular weight (in amu), 75,000

Sodium polyflavinoidsulfonate, consisting chiefly of the copolymer of catechin None and leucocyanidin

Soybean oil, ethoxylated; the poly(oxyethylene) content averages 10 moles or 61791–23–9 greater

Starch, oxidized, polymers with Bu acrylate, tert-Bu acrylate and styrene, min- 204142–80–3 imum number average molecular weight (in amu), 10,000

Stearyl methacrylate-1,6-hexanediol dimethacrylate copolymer, minimum mo- None lecular weight (in amu), 100,000

Styrene, copolymers with acrylic acid and/or methacrylic acid, with none and/or None one or more of the following monomers: Acrylamidopropyl methyl sulfonic acid, methallyl sulfonic acid, 3-sulfopropyl acrylate, 3-sulfopropyl methacrylate, hydroxypropyl methacrylate, hydroxypropyl acrylate, hydroxyethyl methacrylate, hydroxyethyl acrylate, and/or lauryl methacrylate; and its sodium, potassium, ammonium, monoethanolamine, and triethanolamine salts; the resulting polymer having a minimum number average molecular weight (in amu), 1200

Styrene-ethylene-propylene block copolymer, minimum number average molec- 108388–87–0 ular weight (in amu), 125,000

Styrene, 2-ethylhexyl acrylate, butyl acrylate copolymer, minimum number aver- 30795–23–4 age molecular weight (in amu), 4,200

Styrene-2-ethylhexyl acrylate-glycidyl methacrylate-2-acrylamido-2- None methylpropanesulfonic acid graft copolymer, minimum number average molecular weight (in amu), 12,500

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Polymer CAS No.

Styrene-maleic anhydride copolymer None

Styrene-maleic anhydride copolymer, ester derivative None

Tall oil, polymer with polyethylene glycol and succinic anhydride 1398573–80–2 monopolyisobutylene derivs., minimum number average molecular weight (in amu), 1,200

Tamarind seed gum, 2-hydroxypropyl ether polymer, minimum number average 68551–04–2 molecular weight (in amu), 10,000

Tetradecyl acrylate-acrylic acid copolymer, minimum number average molecular None weight (in amu), 3,000

Tetraethoxysilane, polymer with hexamethyldisiloxane, minimum number aver- 104133–09–7 age molecular weight (in amu), 2,500

Tetraethoxysilane, polymer with hexamethyldisiloxane, minimum number aver- 104133–09–7 age molecular weight (in amu), 6,500

a-[p-(1,1,3,3-Tetramethylbutyl)phenyl]-w-hydroxypoly(oxyethylene) produced by 9036–19–5 the condensation of 1 mole of p-(1,1,3,3-tetramethylbutyl)phenol with a range 9002–93–1 of 30-70 moles of ethylene oxide

a-[p-(1,1,3,3-Tetramethylbutyl)phenyl] poly(oxypropylene) block polymer with None poly(oxyethylene); the poly(oxypropylene) content averages 25 moles, the poly(oxyethylene) content averages 40 moles, the molecular weight (in amu) averages 3,400

1,3,5-triazine-2,4,6-triamine, polymer with formaldehyde, methylated, minimum 68002–20–0 number average molecular weight (in amu), 10000

1,3,5-triazine-2,4,6-triamine, polymer with formaldehyde, minimum number av- 9003–08–1 erage molecular weight (in amu), 10000

a-[2,4,6-Tris[1-(phenyl)ethyl]phenyl]-w-hydroxy poly(oxyethylene) None poly(oxypropylene) copolymer, the poly(oxypropylene) content averages 2–8 moles, the poly(oxyethylene) content averages 16–30moles, average molecular weight (in amu), 1,500

Alpha-[2,4,6-Tris[1-(phenyl)ethyl]phenyl]-Omega-hydroxy poly(oxyethylene) 70880–56–7 poly(oxypropylene) copolymer, the poly(oxypropylene) content averages 2–8 moles, the poly(oxyethylene) content averages 16–60 moles. Minimum number-average molecular weight (in amu) of 1,500

Urea-formaldehyde copolymer, minimum average molecular weight (in amu), 9011–05–6 30,000

Vinyl acetate-allyl acetate-monomethyl maleate copolymer, minimum average None molecular weight (in amu), 20,000

Vinyl acetate-ethylene copolymer, minimum number average molecular weight 24937–78–8 (in amu), 69,000

Vinyl acetate polymer with none and/or one or more of the following monomers: None Ethylene, propylene, N-methyl acrylamide, acrylamide, monoethyl maleate, diethyl maleate, monooctyl maleate, dioctyl maleate, maleic anhydride, maleic acid, octyl acrylate, butyl acrylate, ethyl acrylate, methyl acrylate, acrylic acid, octyl methacrylate, butyl methacrylate, ethyl methacrylate, methyl methacrylate, methacrylic acid, carboxyethyl acrylate, and diallyl phthalate; and their corresponding sodium, potassium, ammonium, isopropylamine, triethylamine, monoethanolamine and/or triethanolamine salts; the resulting polymer having a minimum number average molecular weight (in amu), 1,200

Vinyl acetate-vinyl alcohol-alkyl lactone copolymer, minimum number average None molecular weight (in amu), 40,000; minimum viscosity of 18 centipoise

Vinyl alcohol-disodium itaconate copolymer, minimum average molecular None weight (in amu), 50,290

Vinyl alcohol-vinyl acetate copolymer, benzaldehyde-o-sodium sulfonate con- None densate, minimum number average molecular weight (in amu), 20,000

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Polymer CAS No.

Vinyl alcohol-vinyl acetate-monomethyl maleate, sodium salt-maleic acid, diso- None dium salt-g-butyrolactone acetic acid, sodium salt copolymer, minimum number average molecular weight (in amu), 20,000

Vinyl chloride-vinyl acetate copolymers None

Vinyl pyrrolidone-acrylic acid copolymer, minimum number average molecular 28062–44–4 weight (in amu), 6,000

Vinyl pyrrolidone-dimethylaminoethylmethacrylate copolymer, minimum number 30581–59–0 average molecular weight (in amu), 20,000

Vinyl pyrrolidone-styrene copolymer 25086–29–7

[67 FR 36528, May 24, 2002]

EDITORIAL NOTE: For FEDERAL REGISTER citations affecting § 180.960, see the List of CFR Sections Affected, which appears in the Finding Aids section of the printed volume and at www.govinfo.gov.

§ 180.1011 Viable spores of the micro- satisfied either by determining that organism Bacillus thuringiensis each master seed lot brought into pro- Berliner; exemption from the reduction is a Bacillus thuringiensis strain quirement of a tolerance. which does not produce b-exotoxin (a) For the purposes of this section under standard manufacturing condi- the microbial insecticide for which ex- tions or by periodically determining emption from the requirement of a tol- that b-exotoxin synthesized during erance is being established shall have spore production is eliminated by the the following specifications: subsequent spore-harvesting procedure. (1) The microorganism shall be an au- (b) Exemption from the requirement thentic strain of Bacillus thuringiensis of a tolerance is established for resi- Berliner conforming to the morpho- dues of the microbial insecticide Bacil- logical and biochemical characteristics lus thuringiensis Berliner, as specified of Bacillus thuringiensis as described in in paragraph (a) of this section, in or Bergey’s Manual of Determinative Bac- on honey and honeycomb and all other teriology, Eighth Edition. raw agricultural commodities when it (2) Spore preparations of Bacillus is applied either to growing crops, or thuringiensis Berliner shall be produced when it is applied after harvest in ac- by pure culture fermentation proce- cordance with good agricultural prac- dures with adequate control measures tices. during production to detect any changes from the characteristics of the [36 FR 22540, Nov. 25, 1971, as amended at 38 parent strain or contamination by FR 19045, July 17, 1973; 42 FR 28540, June 3, other microorganisms. 1977; 45 FR 43721, June 30, 1980; 45 FR 56347, Aug. 25, 1980; 74 FR 26533, June 3, 2009] (3) Each lot of spore preparation, prior to the addition of other mate- § 180.1016 Ethylene; exemption from rials, shall be tested by subcutaneous the requirement of a tolerance. injection of at least 1 million spores into each of five laboratory test mice Ethylene is exempted from the re- weighing 17 grams to 23 grams. Such quirement of a tolerance for residues test shall show no evidence of infection when: or injury in the test animals when ob- (a) For all food commodities, it is served for 7 days following injection. used as a plant regulator on plants, (4) Spore preparations shall be free of seeds, or cuttings and on all food com- the Bacillus thuringiensis b-exotoxin modities after harvest and when ap- when tested with the fly larvae tox- plied in accordance with good agricul- icity test (‘‘Microbial Control of In- tural practices. sects and Mites,’’ R.P.M. Bond et al., p. (b) Injected into the soil to cause pre- 280 ff., 1971). This specification can be mature germination of witchweed in

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bean (lima and string), cabbage, canta- byproducts; egg; milk; fish, shellfish, loupe, collard, corn, cotton, cucumber, and irrigated crops when it results eggplant, okra, onion, pasture grass, from the use of sulfuric acid as an inert pea (field and sweet), peanut, pepper, ingredient in a pesticide product used potato, sweet potato, sorghum, soy- in irrigation conveyance systems and bean, squash, tomato, turnip, and wa- lakes, ponds, reservoirs, or bodies of termelon fields as part of the U.S. De- water in which fish or shellfish are cul- partment of Agriculture witchweed tivated. The sulfuric acid is not to ex- control program. ceed 10% of the pesticide formulation [39 FR 33315, Sept. 17, 1974, as amended at 40 (non-aerosol formulations only). FR 19477, May 5, 1975; 64 FR 31505, June 11, [69 FR 40787, July 7, 2004, as amended at 74 1999] FR 26533, June 3, 2009]

§ 180.1017 Diatomaceous earth; exemp- § 180.1020 Sodium chlorate; exemption tion from the requirement of a tol- from the requirement of a toler- erance. ance. (a) Diatomaceous earth is exempted Sodium chlorate is exempted from from the requirement of a tolerance for the requirement of a tolerance for resi- residues when used in accordance with dues when used as a defoliant or des- good agricultural practice in pesticide formulations applied to growing crops, iccant in accordance with good agricul- to food commodities after harvest, and tural practice on the following crops: to animals. Bean, dry, seed (b) Diatomaceous earth may be safely Corn, field, forage used in accordance with the following Corn, field, grain conditions. Application shall be lim- Corn, field, stover ited solely to spot and/or crack and Corn, pop, grain crevice treatments in food or feed proc- Corn, pop, stover essing and food or feed storage areas in Corn, sweet, forage accordane with the precribed condi- Corn, sweet, stover tions: Cotton, undelinted seed (1) It is used or intended for use for Flax, seed control of insects in food or feed proc- Grain, aspirated fractions essing and food or feed storage areas: Guar, seed Pea, southern Provided, That the food or feed is re- Pepper, nonbell moved or covered prior to such use. Potato (2) To assure safe use of the insecti- Rice, grain cide, its label and labeling shall con- Rice, straw form to that registered by the U.S. En- Safflower, seed vironmental Protection Agency, and it Sorghum, forage, forage shall be used in accordance with such Sorghum, grain, forage label and labeling. Sorghum, grain, grain Sorghum, grain, stover [65 FR 33716, May 24, 2000] Soybean, forage § 180.1019 Sulfuric acid; exemption Soybean, hay from the requirement of a toler- Soybean, seed ance. Sunflower, seed Wheat, grain (a) Residues of sulfuric acid are exempted from the requirement of a tol- [74 FR 47457, Sept. 16, 2009] erance when used in accordance with good agricultural practice when used § 180.1021 Copper; exemption from the as a herbicide in the production of gar- requirement of a tolerance. lic and onions, and as a potato vine (a) Copper is exempted from the re- dessicant in the production of potatoes. quirement of a tolerance in cattle, (b) Residues of sulfuric acid are ex- meat; goat, meat; hog, meat; horse, empted from the requirement of a tol- meat; sheep, meat; milk, poultry, fat; erance in cattle, meat; goat, meat; hog, poultry, meat; poultry, meat byprod- meat; horse, meat; sheep, meat; poul- ucts; egg, fish, shellfish, and irrigated try, fat; poultry, meat; poultry, meat, crops when it results from the use of:

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(1) Copper sulfate as an algicide or § 180.1022 Iodine-detergent complex; herbicide in irrigation conveyance sys- exemption from the requirement of tems and lakes, ponds, reservoirs, or a tolerance. bodies of water in which fish or shell- The aqueous solution of hydriodic fish are cultivated. acid and elemental iodine, including (2) Basic copper carbonate (mala- one or both of the surfactants (a) chite) as an algicide or herbicide in im- polyoxypropylene-polyoxyethylene gly- pounded and stagnant bodies of water col nomionic block polymers (min- (3) Copper triethanolamine and cop- imum average molecular weight 1,900) per monoethanolamine as an algicide and (b) a-(p- nonylphenyl)-omega- or herbicide in fish hatcheries, lakes, hydroxypoly (oxyethylene) having a ponds, and reservoirs maximum average molecular weight of (4) Cuprous oxide bearing antifouling 748 and in which the nonyl group is a coatings for control of algae or other propylene trimer isomer, is exempted coatings for control of algae or other from the requirement of a tolerance for organisms on submerged concrete or residues in egg, and poultry, fat; poul- other (irrigation) structures. try, meat; poultry, meat byproducts (5) Copper oxide embedded in polymer when used as a sanitizer in poultry emitter heads used in irrigation sys- drinking water. tems for root incursion prevention. (b) The following copper compounds [74 FR 26534, June 3, 2009] are exempt from the requirement of a tolerance when applied (primarily) as a § 180.1023 Propanoic acid; exemptions fungicide to growing crops using good from the requirement of a toler- agricultural practices: ance. (a) Postharvest application of pro- Copper compounds CAS Reg. No. panoic acid or a mixture of methylene Basic copper carbonate (mala- bispropionate and oxy(bismethylene) chite) ...... 1184–64–1 bisproprionate when used as a fun- Copper ammonia complex ...... 16828–95–8 Copper ethylenediamine complex 13426–91–0 gicide is exempted from the require- Copper hydroxide ...... 20427–59–2 ment of a tolerance for residues in or Copper octanoate ...... 20543–04–8 on the following raw agricultural com- Copper oxychloride ...... 1332–65–6 Copper oxychloride sulfate ...... 8012–69–9 modities: Alfalfa, forage; alfalfa, hay; Copper salts of fatty and rosin alfalfa, seed; barley, grain; acids ...... 9007–39–0 Bermudagrass, forage; Bermudagrass, Copper sulfate basic ...... 1344–73–6 hay; bluegrass, forage; bluegrass, hay; Copper sulfate pentahydrate ...... 7758–99–8 Cuprous oxide ...... 1317–19–1 bromegrass, forage; bromegrass, hay; clover, forage; clover, hay; corn, field, (c) Copper sulfate pentahydrate (CAS grain; corn, pop, grain; cowpea, hay; Reg. No. 7758–99–8) is exempt from the fescue, forage; fescue, hay; lespedeza, requirement of a tolerance when ap- forage; lespedeza, hay; lupin; oat, plied as a fungicide to growing crops or grain; orchardgrass, forage; to raw agricultural commodities after orchardgrass, hay; peanut, hay; pea, harvest, and as a bactericide/fungicide field, hay; ryegrass, Italian, hay; sor- in or on meat, fat and meat by-prod- ghum, grain, grain; soybean, hay; ucts of cattle, sheep, hogs, goats, sudangrass, forage; sudangrass, hay; horses and poultry, milk and eggs when timothy, forage; timothy, hay; vetch, applied as a bactericide/fungicide to forage; vetch, hay; and wheat, grain. animal premises and bedding. (b) Propanoic acid is exempt from the (d) Copper (II) hydroxide (CAS Reg. requirement of a tolerance for residues No. 20427–59–2) is exempt from the re- in or on cattle, meat; cattle, meat by- quirement of a tolerance when applied products; goat, meat; goat, meat by- to growing crops or to raw agricultural products; hog, meat; hog meat byprod- commodities as an inert ingredient (for ucts; horse, meat; horse, meat byprod- pH control) in pesticide products. ucts; sheep, meat; sheep meat byprod- [65 FR 68912, Nov. 15, 2000, as amended at 69 ucts; and, poultry, fat; poultry meat; FR 4069, Jan. 28, 2004; 71 FR 46110, Aug. 11, poultry meat byproducts; milk, and 2006; 74 FR 26534, June 3, 2009; 74 FR 47457, egg when applied as a bactericide/fun- Sept. 16, 2009; 80 FR 37551, July 1, 2015] gicide to livestock drinking water,

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poultry litter, and storage areas for si- (b) Each lot of active ingredient of lage and grain. the viral insecticide shall have the fol- (c) Preharvest and postharvest appli- lowing specifications: cation of propanoic acid (CAS Reg. No. (1) The level of extraneous bacterial 79–09–4), propanioc acid, calcium salt contamination of the final (CAS Reg. No. 4075–81–4), and propanioc unformulated viral insecticide should sodium salt (CAS Reg. No. 137–40–6) are not exceed 107 colonies per gram as de- exempted from the requirement of a termined by an aerobic plate on tolerance on all crops when used as ei- trypticase soy agar. ther an active or inert ingredient in ac- (2) Human pathogens, e.g., Sal- cordance with good agricultural practice in pesticide formulations applied monella, Shigella, or Vibrio, must be to growing crops, to raw agricultural absent. commodities before and after harvest (3) Safety to mice as determined by and to animals. an intraperitoneal injection study must be demonstrated. [69 FR 47025, Aug. 4, 2004, as amended at 74 FR 26534, June 3, 2009] (4) Identity of the viral product, as determined by the most sensitive and § 180.1025 Xylene; exemption from the standardized analytical technique, e.g., requirement of a tolerance. restriction endonuclease and/or SDS- Xylene is exempted from the require- PAGE analysis, must be demonstrated. ment of a tolerance when used as an (c) Exemptions from the requirement aquatic herbicide applied to irrigation of a tolerance are established for the conveyance systems in accordance with residues of the microbial insecticide the following conditions: Heliothis zea NPV, as specified in para- (a) It is to be used only in programs graphs (a) and (b) of this section, in or of the Bureau of Reclamation, U.S. De- on all agricultural commodities. partment of Interior, and cooperating water user organizations. [60 FR 42460, Aug. 16, 1995, as amended at 74 (b) It is to be applied as an emulsion FR 26534, June 3, 2009] at an initial concentration not to exceed 750 parts per million. § 180.1033 Methoprene; exemption from the requirement of a toler- (c) It is not to be applied when there ance. is any likelihood that the irrigation water will be used as a source of raw Methoprene is exempt from the re- water for a potable water system or quirement of a tolerance in or on all where return flows of such treated irri- food commodities when used to control gation water into receiving rivers and insect larvae. streams would contain residues of xy- [68 FR 34829, June 11, 2003] lene in excess of 10 parts per million. (d) Xylene to be used as an aquatic § 180.1037 Polybutenes; exemption herbicide shall meet the requirement from the requirement of a toler- limiting the presence of a polynuclear ance. aromatic hydrocarbons as listed in 21 CFR 172.250. (a) Polybutenes are exempt from the requirement of a tolerance for residues [38 FR 16352, June 22, 1973, as amended at 50 in or on the raw agricultural com- FR 2980, Jan. 3, 1985] modity cotton, undelinted seed when § 180.1027 Nuclear polyhedrosis virus used as a sticker agent for formula- of Heliothis zea; exemption from tions of the attractant gossyplure (1:1 the requirement of a tolerance. mixture of (Z,Z)- and (Z,E)-7,11- (a) For the purposes of this section, hexadecadien-1-ol acetate) to disrupt the viral insecticide must be produced the mating of the pink bollworm. with an unaltered and unadulterated (b) Polybutenes are exempt from the inoculum of the single-embedded requirement of a tolerance for residues Heliothis zea nuclear polyhedrosis virus in or on the raw agricultural com- (HzSNPV). The identity of the seed modity artichoke when used as a stick- virus must be assured by periodic er agent in multi-layered laminted checks. controlled-release dispensers of (Z)-11-

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hexaadecenal to disrupt the mating of § 180.1052 2,2,5-trimethyl-3-dichloro- the artichoke plume moth. acetyl-1,3-oxazolidine; exemption from the requirement of a toler- [74 FR 26534, June 3, 2009] ance. § 180.1040 Ethylene glycol; exemption 2,2,5-trimethyl-3-dichloroacetyl-1,3- from the requirement of a toler- oxazolidine is exempted from the re- ance. quirement of a tolerance when used as an inert ingredient in formulations of Ethylene glycol as a component of the herbicides S-ethyl pesticide formulations is exempt from dipropylthiocarbamate, S-propyl the requirement of a tolerance when dipropylthiocarbamate, and S-ethyl used in foliar applications to peanut diisobutylthiocarbamate applied to plants. corn fields before the corn plants emerge from the soil with a maximum [43 FR 41393, Sept. 18, 1978] of 0.5 pound of the inert ingredient per § 180.1041 Nosema locustae; exemption acre. from the requirement of a toler- [45 FR 51201, Aug. 1, 1980] ance. § 180.1054 Calcium hypochlorite; ex- The insecticide Nosema locustae is exemptions from the requirement of a empted from the requirement of a tol- tolerance. erance for residues in or on all raw ag- (a) Calcium hypochlorite is exempted ricultural commodities. from the requirement of a tolerance [47 FR 21537, May 19, 1982] when used preharvest or postharvest in solution on all raw agricultural com- § 180.1043 Gossyplure; exemption from modities. the requirement of a tolerance. (b) Calcium hypochlorite is exempted The pheromone gossyplure, a 1:1 mix- from the requirement of a tolerance in or on grape when used as a fumigant ture of (Z,Z)- and (Z,E)-7,11- postharvest by means of a chlorine hexadecadien-1-ol acetate) is exempt generator pad. from the requirement of a tolerance in or on the raw agricultural commodity [59 FR 59165, Nov. 16, 1994, as amended at 74 cotton, undelinted seed when applied to FR 26534, June 3, 2009] cotton from capillary fibers. § 180.1056 Boiled linseed oil; exemp- [74 FR 26534, June 3, 2009] tion from requirement of tolerance. Boiled linseed oil (containing no § 180.1049 Carbon dioxide; exemption more than 0.33 percent manganese from the requirement of a toler- naphthenate and no more than 0.33 per- ance. cent cobalt naphthenate) is exempt The insecticide carbon dioxide is ex- from the requirement of a tolerance empted from the requirement of a tol- when used as a coating agent for S- erance when used after harvest in ethyl hexahydro-1H-azepine-1- modified atmospheres for stored insect carbothioate. No more than 15 percent control on food commodities. of the pesticide formulation may consist of ‘‘boiled linseed oil.’’ This exemp- [65 FR 33716, May 24, 2000] tion is limited to use on rice before edible parts form. § 180.1050 Nitrogen; exemption from the requirements of a tolerance. [46 FR 33270, June 29, 1981] The insecticide nitrogen is exempted § 180.1057 Phytophthora palmivora; from the requirements of a tolerance exemption from requirement of tol- when used after harvest in modified erance. atmospheres for stored product insect Phytophthora palmivora is exempted control on all food commodities. from the requirement of a tolerance in or on the raw agricultural commodity [65 FR 33716, May 24, 2000] fruit, citrus. [74 FR 26534, June 3, 2009]

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§ 180.1058 Sodium diacetate; exemp- § 180.1067 Methyl eugenol and mala- tion from the requirement of a tol- thion combination; exemption from erance. the requirement of a tolerance. Sodium diacetate, when used The insect attractant methyl eugenol postharvest as a fungicide, is exempt and the insecticide malathion are ex- from the requirement of a tolerance for empt from the requirement of toler- residues in or on alfalfa, hay; ances on all raw agricultural commod- Bermudagrass, hay; bluegrass, hay; ities when used in combination in Ori- bromegrass, hay; clover,hay; corm, ental fruit fly eradication programs field, grain; corn, pop, grain; oat, grain; under the authority of the U.S. Depart- orchardgrass, hay; sorghum, grain, ment of Agriculture, in accordance grain; sudangrass, hay; ryegrass, with the following directions and speci- Italian, hay; timothy, hay. fications: (a) The combination shall be at the [74 FR 26534, June 3, 2009] ratio of three parts methyl eugenol to § 180.1064 Tomato pinworm insect one part technical malathion (3:1). pheromone; exemption from the re- (b) This combination is to be impreg- quirement of a tolerance. nated on a carrier (cigarette filter tips An exemption from the requirement (cellulose acetate); cotton strings; fi- of a tolerance is established for com- berboard squares) or mixed with a jel bined residues of both components of cleared under 40 CFR 180.920 or 180.950. the tomato pinworm insect pheromone (c) The maximum actual dosage per (E)-4-tridecen-1-yl acetate and (Z)-4- application per acre shall be 28.35 tridecen-1-yl acetate in or on all raw grams (one ounce avoirdupois) methyl agricultural commodities (preharvest) eugenol and 9.45 grams (one-third (0.33) in accordance with the following pre- ounce avoirdupois) technical mala- scribed conditions: thion. (a) Application shall be limited sole- [47 FR 9002, Mar. 3, 1982, as amended at 69 FR ly to point source dispensers or point 23142, Apr. 28, 2004] source chopped fibers containing the tomato pinworm insect pheromone. § 180.1068 C12-C18 fatty acid potassium (b) Cumulative yearly application salts; exemption from the require- cannot exceed 200 grams of tomato ment of a tolerance. pinworm pheromone per acre. C12-C18 fatty acids (saturated and unsaturated) potassium salts are exempt- [58 FR 34376, June 25, 1993] ed from the requirement of a tolerance § 180.1065 2-Amino-4,5-dihydro-6-meth- for residues in or on all raw agricul- yl-4-propyl-s-triazolo(1,5- tural commodities when used in ac- alpha)pyrimidin-5-one; exemption cordance with good agricultural prac- from the requirement of a toler- tice. ance. [60 FR 34871, July 5, 1995] The inert ingredient, 2-amino-4,5- dihydro-6-methyl-4-propyl-s- § 180.1069 (Z)-11-Hexadecenal; exemp- triazolo(1,5-alpha)pyrimidin-5-one is tion from the requirement of a tol- exempted from the requirement of a erance. tolerance when used as an emetic at An exemption from the requirement not more than 0.3 percent in formula- of a tolerance is established for resi- tions of paraquat dichloride. Further dues of the biological insecticide restrictions on this exemption are that (pheromone) (Z)-11-hexadecenal when this ingredient may not be advertised used as a sex attractant on artichoke as an emetic and the paraquat product plants to control the artichoke plume may not be promoted in any way be- moth. cause of the inclusion of this inert ingredient. [47 FR 14906, Apr. 7, 1982] [70 FR 46431, Aug. 10, 2005]

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§ 180.1070 Sodium chlorite; exemption vestable food commodities are present from the requirement of a toler- (usually pre-bloom). ance. (12) Application as part of an animal Sodium chlorite is exempted from feed-through product. the requirement of a tolerance for resi- (13) Applications as gel and solid dues when used in accordance with (non-liquid/non-spray) crack and crev- good agricultural practice as a seed- ice treatments that place the gel or soak treatment in the growing of the bait directly into or on top of the raw agricultural commodities vege- cracks and crevices via a mechanism table, brassica, leafy, group 5 and rad- such as a syringe. ish, roots and radish, tops. (14) Applications to the same crop [74 FR 26534, June 3, 2009] from which the food commodity is derived, whether the plant fraction(s) in- § 180.1071 Peanuts, Tree Nuts, Milk, tended for harvest are present or not, Soybeans, Eggs, Fish, Crustacea, e.g., applications of peanut meal when and Wheat; exemption from the re- applied to peanut plants. quirement of a tolerance. (b) Specific chemical substances. Resi- (a) General. Residues resulting from dues resulting from the use of the fol- the following uses of the food com- lowing substances as either an inert or modity forms of peanuts, tree nuts, an active ingredient in a pesticide for- milk, soybeans, eggs (including putres- mulation are exempted from the re- cent eggs), fish, crustacea, and wheat quirement of a tolerance under FFDCA are exempted from the requirement of section 408, if such use is in accordance a tolerance in or on all food commod- with good agricultural practices and ities under FFDCA section 408 (when such use is included in paragraph (a): used as either an inert or an active ingredient in a pesticide formulation), if Chemical Substance CAS No. such use is in accordance with good ag- Caseins ...... 9000–71–9 ricultural practices: Caseins, ammonium complexes ...... 9005–42–9 (1) Use in pesticide products intended Caseins, hydrolyzates ...... 65072–00–6 to treat seeds. Caseins, potassium complexes ...... 68131–54–4 (2) Use in nursery and greenhouse op- Caseins, sodium complexes ...... 9005–46–3 erations, as defined in 40 CFR 170.3, which includes seeding, potting and [70 FR 1360, Jan. 7, 2005] transplanting activities. (3) Pre-plant and at-transplant appli- § 180.1072 Poly-D-glucosamine cations. (chitosan); exemption from the re- (4) Incorporation into seedling and quirement of a tolerance. planting beds. (a) An exemption from the require- (5) Applications to cuttings and bare ment of a tolerance is established for roots. residues of the biological plant growth (6) Applications to the field that regulator poly-D-glucosamine when occur after the harvested crop has been used as a seed treatment in or on bar- removed. ley, beans, oats, peas, rice, and wheat. (7) Soil-directed applications around (b) An exemption from the require- and adjacent to all plants. ment of a tolerance is established for (8) Applications to rangelands, which residues of the biological plant growth is land, mostly grasslands, whose regulator poly-D-glucosamine when plants can provide food (i.e., forage) for used as a pesticide in the production grazing or browsing animals. any raw agricultural commodity. (9) Use in chemigation and irrigation systems (via flood, drip, or furrow ap- [60 FR 19524, Apr. 19, 1995] plication with no overhead spray applications). § 180.1073 Isomate-M; exemption from (10) Application as part of a dry fer- the requirement of a tolerance. tilizer on which an active ingredient is The oriental fruit moth pheromone impregnated. (Isomate-M) (Z-8-dodecen-l-yl acetate, (11) Aerial and ground applications E-8-dodecen-l-yl acetate, Z-8-dodecen-l- that occur when no above-ground har- ol) is exempt from the requirement of a

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tolerance in or on all the raw agricul- (3) Each lot of spore preparation, tural commodities (food and feed) in- prior to the addition of other mate- cluding, peach; quince; nectarine; and rials, shall be tested by subcutaneous nut, macadamia when used in orchards injection of at least 1 million spores with encapsulated polyethylene tubing into each of five laboratory test mice to control oriental fruit moth. weighing 17 grams to 23 grams. Such test shall show no evidence of infection [74 FR 26534, June 3, 2009] of injury in the test animals when ob- § 180.1074 F.D.&C. Blue No. 1; exemp- served for 7 days following injection. tion from the requirement of a tol- (b) Exemption from the requirement erance. of a tolerance is established for resi- F.D.&C. Blue No. 1 is exempted from dues of the microbial insecticide Bacil- the requirement of a tolerance when lus popilliae, as specified in paragraph used as an aquatic plant control agent. (a) of this section in or on grass, pasture, forage and grass, rangeland, for- [47 FR 25963, June 16, 1982] age when it is applied to growing crops in accordance with good agricultural § 180.1075 Colletotrichum gloeosporioides f. sp. aeschynomene; practices. exemption from the requirement of [47 FR 38535, Sept. 1, 1982, as amended at 74 a tolerance. FR 26535, June 3, 2009] An exemption from the requirement of a tolerance is established for resi- § 180.1080 Plant volatiles and dues of the mycoherbicide pheromone; exemptions from the Colletotrichum gloeosporioides f. sp. requirement of a tolerance. aeschynomene in or on the following An exemption from the requirement raw agricultural commodities: of a tolerance is established for residues of the plant volatiles cyclic COMMODITY decadiene, cyclic decene, cyclic Aspirated grain fractions pentadecatriene, and decatriene and Rice, grain the pheromone Z-2-isopropenyl-1- Soybean, forage methylcyclobutaneethanol; Z-3,3-di- Soybean, hay methyl-D1,b-cyclohexaneethanol; Z-3,3- Soybean, seed dimethyl-D1,a-cyclohexaneethanal; E- [47 FR 25742, June 15, 1982, as amended at 74 3,3-dimethyl-D1,a-cyclohexaneethanal FR 26534, June 3, 2009] combination when applied to cotton in hollow synthetic fibers. § 180.1076 Viable spores of the microorganism Bacillus popilliae; exemp- [48 FR 28442, June 22, 1983] tion from the requirement of a tolerance. § 180.1083 Dimethyl sulfoxide; exemp- (a) For the purposes of this section tion from the requirement of a tol- the microbial insecticide for which ex- erance. emption from the requirement of a tol- Dimethyl sulfoxide (DMSO) [CAS erance is being established shall have Registry Number 67–68–5] is exempted the following specifications: from the requirement of a tolerance (1) The microorganism shall be an au- when used as an inert solvent or cosol- thentic strain of Bacillus popilliae con- vent in formulations with the following forming to the morphological and bio- pesticides when used in accordance chemical characteristics of Bacillus with good agricultural practices in or popilliae as described in Bergey’s Man- on the following raw agricultural com- ual of Determinative Bacteriology, modities: Eighth Edition. (a) Carbaryl (1-naphthyl methyl-car- (2) Spore preparations of Bacillus bamate) popilliae shall be produced by an extraction process from diseased Japa- Pea, dry, seed Pea, succulent nese beetles, and may contain a small percentage of the naturally occurring (b) O-O-Diethyl O-(2-isopropyl-6- milky disease bacterium Bacillus methyl-4-pyrimidinyl) lentimorbus. phosphorothioate

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Pea, dry, seed poly-N-acetyl-D-glucosamine on a vari- Pea, succulent ety of agricultural crops. [48 FR 54819, Dec. 7, 1983, as amended at 74 [53 FR 10249, Mar. 30, 1988] FR 26535, June 3, 2009]

§ 180.1084 Monocarbamide dihydrogen § 180.1090 Lactic acid; exemption from sulfate; exemption from the require- the requirement of a tolerance. ment of a tolerance. Lactic acid (2-hydroxypropanoic Monocarbamide dihydrogen sulfate is acid) is exempted from the requirement exempted from the requirement of a of a tolerance when used as a plant tolerance when used as a herbicide or growth regulator in or on all raw agri- desiccant in or on all raw agricultural cultural commodities. commodities. [53 FR 15286, May 4, 1988] [53 FR 12152, Apr. 13, 1988] § 180.1091 Aluminum isopropoxide and § 180.1086 3,7,11-Trimethyl-1,6,10- aluminum secondary butoxide; ex- dodecatriene-1-ol and 3,7,11- emption from the requirement of a trimethyl-2,6,10-dodecatriene-3-ol; tolerance. exemption from the requirement of Aluminum isopropoxide (CAS Reg. a tolerance. No. 555–31–7) and aluminum secondary The insect pheromone containing the butoxide (CAS Reg. No. 2269–22–9) are active ingredients 3,7,11-trimethyl- exempted from the requirement of a 1,6,10-dodecatriene-1-ol and 3,7,11- tolerance when used in accordance trimethyl-2,6,10-dodecatriene-3-ol is ex- with good agricultural practices as sta- empted from the requirement of a tol- bilizers in formulations of the insecti- erance in or on all raw agricultural cide amitraz [N′-(2,4-dimethylphenyl)- commodities. N-[[(2,4-dimethylphenyl)imino]-N- [52 FR 12165, Apr. 15, 1987; 52 FR 29014, Aug. methylmethanimidamide] applied to 5, 1987] growing crops or animals. [53 FR 34509, Sept. 7, 1988; 53 FR 36696, Sept. § 180.1087 Sesame stalks; exemption 21, 1988] from the requirement of a tolerance. § 180.1092 Menthol; exemption from An exemption from the requirement the requirement of a tolerance. of a tolerance is established for resi- An exemption from the requirement dues of the biorational nematicide ses- of a tolerance is established for resi- ame stalk in or on the following raw dues of the pesticidal chemical men- agricultural commodities: Almond; al- thol in or on honey and honeycomb mond, hulls; cotton, undelinted seed; when used in accordance with good ag- cotton, gin byproducts; soybean, seed; ricultural practice in over-wintering soybean, forage; soybean, hay; aspi- bee hives. rated grain fractions; potato; beet, sugar, roots; beet, sugar, tops; tomato; [74 FR 26535, June 3, 2009] pepper, bell; squash; strawberry; eggplant; cucumber; carrot, roots; radish, § 180.1095 Chlorine gas; exemptions roots; radish, top; turnip, roots; turnip, from the requirement of a tolerance. tops; onion; pea, dry; pea, succulent; melon; grape; walnut; orange; grape- Chlorine gas is exempted from the re- fruit; mulberry; peach; apple; apricot; quirement of a tolerance when used blackberry; loganberry; pecan; cherry; preharvest or postharvest in solution plum, and cranberry. on all raw agricultural commodities. [74 FR 26535, June 3, 2009] [56 FR 21309, May 8, 1991]

§ 180.1089 Poly-N-acetyl-D-glu- § 180.1097 GBM-ROPE; exemption from cosamine; exemption from the re- the requirement of a tolerance. quirement of tolerance. The grape berry moth pheromone An exemption from the requirement (GBM-ROPE) containing the active in- of a tolerance is established for resi- gredients (Z)-9-dedecenyl acetate and dues of the biochemical nematicide (Z)-11-tetradecenyl acetate is exempt

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from the requirement of a tolerance in Anisopteromalus, Choetospila, or on the raw agricultural commodity Lariophagus, Dibrachys, Habrocytus, grape when used in orchards with en- Pteromalus, Pteromalidae; capsulated polyethylene tubing to con- Cephalonomia, Holepyris, Laelius, trol grape berry moth. Bethylidae; and of Hemiptera in the [74 FR 26535, June 3, 2009] genera Xylocoris, Lyctocoris, and Dufouriellus, Anthocoridae. Whole in- § 180.1098 Gibberellins [Gibberellic sects, fragments, parts, and other resi- Acids (GA3 and GA4 + GA7), and So- dues of these parasites and predators dium or Potassium Gibberellate]; exemption from the requirement of remain subject to 21 U.S.C. 342(a)(3). a tolerance. [57 FR 14646, Apr. 22, 1992] An exemption from the requirement of a tolerance is established for resi- § 180.1102 Trichoderma harzianum dues of gibberellins [gibberellic acids KRL-AG2 (ATCC #20847) strain T– (GA3 and GA4 + GA7), and sodium or 22; exemption from requirement of potassium gibberellate] in or on all a tolerance. food commodities when used as plant An exemption from the requirement regulators on plants, seeds, or cuttings of a tolerance is established for resi- and on all food commodities after har- dues of the biofungicide Trichoderma vest in accordance with good agricul- harzianum KRL-AG2 (ATCC #20847); tural practices. also known as strain T-22 when applied [64 FR 31505, June 11, 1999] in/or on all food commodities.

§ 180.1100 Gliocladium virens isolate [64 FR 16860, Apr. 7, 1999] GL-21; exemption from the requirement of a tolerance. § 180.1103 Isomate-C; exemption from the requirement of a tolerance. An exemption from the requirement of a tolerance is established for resi- The codling moth pheromone dues of the biofungicide Gliocladium (Isomate-C) E,E-8,10-dodecenyl alcohol, virens GL-21 in or on all raw agricul- dodecanol, tetradecanol is exempt from tural commodities when used either as the requirements of a tolerance in or a fungicide for inoculation of plant on all raw agricultural commodities growth media in greenhouses or on ter- when formulated in polyethylene restrial food crops grown outdoors in pheromone dispensers for use in or- accordance with good agricultural chards with encapsulated polyethylene practices. tubing to control codling moth. [60 FR 48659, Sept. 20, 1995; 60 FR 52248, Oct. [74 FR 26535, June 3, 2009] 5, 1995]

§ 180.1101 Parasitic (parasitoid) and § 180.1110 3-Carbamyl-2,4,5-trichloro- predatory insects; exemption from benzoic acid; exemption from the the requirement of a tolerance. requirement of a tolerance. Parasitic (parasitoid) and predatory An exemption from the requirement insects are exempted from the require- of a tolerance is established for the res- ment of a tolerance for residues when idues of 3-carbamyl-2,4,5- they are used in accordance with good trichlorobenzoic acid in or on all raw agricultural and pest control practices agricultural commodities which occur to control insect pests of stored raw from the direct application of whole grains such as corn, small chlorothalonil to crops in § 180.275 (a) grains, rice, soybeans, peanuts, and and (b) and/or as an inadvertent residue other legumes either bulk or resulting from the soil metabolism of warehoused in bags. For the purposes chlorothalonil when applied to crops in of this rule, the parasites (parasitoids) § 180.275 (a) and (b), and subsequent up- and predators are considered to be spe- take by rotated crops when used ac- cies of Hymenoptera in the genera cording to approved agricultural prac- Trichogramma, Trichogrammatidae; tices. Bracon, Braconidae; Venturia, Mesostenus, Ichneumonidae; [57 FR 24552, June 10, 1992]

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§ 180.1111 Bacillus subtilis GB03; ex- used as a fungicide for the treatment of emption from the requirement of a seeds, cuttings, transplants, and plants tolerance. of agricultural crops in accordance The biofungicide Bacillus subtilis GB03 with good agricultural practices. is exempted from the requirement of a [58 FR 21403, Apr. 21, 1993] tolerance in or on all raw agricultural commodities when used in accordance § 180.1121 Boric acid and its salts, with good agricultural practices. borax (sodium borate decahydrate), disodium octaborate tetrahydrate, [73 FR 50556, Aug. 27, 2008] boric oxide (boric anhydride), sodium borate and sodium metabo- § 180.1114 Pseudomonas fluorescens rate; exemptions from the require- A506, Pseudomonas fluorescens ment of a tolerance. 1629RS, and Pseudomonas syringae 742RS; exemptions from the re- An exemption from the requirement quirement of a tolerance. of a tolerance is established for resi- The biological pesticides dues of the pesticidal chemical boric Pseudomonas fluorescens A506, acid and its salts, borax (sodium borate Pseudomonas fluorescens 1629RS, and decahydrate), disodium octaborate tet- Pseudomonas syringae 742RS are ex- rahydrate, boric oxide (boric anhy- empted from the requirement of a tol- dride), sodium borate and sodium met- erance in or on all raw agricultural aborate, in or on raw agricultural com- commodities when applied as a frost modities when used as an active ingre- protection agent or biological control dient in insecticides, herbicides, or fun- agent to growing agricultural crops in gicides preharvest or postharvest in ac- accordance with good agricultural cordance with good agricultural prac- practices. tices. [57 FR 42700, Sept. 16, 1992] [58 FR 44283, Aug. 20, 1993]

§ 180.1118 Spodoptera exigua nuclear § 180.1122 Inert ingredients of polyhedrosis virus; exemption from semiochemical dispensers; exemp- the requirement of a tolerance. tions from the requirement of a tolerance. An exemption from the requirement (a) All inert ingredients of of a tolerance is established for the mi- semiochemical dispenser products for- crobial pest control agent Spodoptera mulated with, and/or contained in, dis- exigua nuclear polyhedrosis virus when pensers made of polymeric matrix ma- used as a pesticide control agent on all terials (including the monomers, plas- raw agricultural commodities. ticizers, dispersing agents, anti- [58 FR 25784, Apr. 28, 1993] oxidants, UV protectants, stabilizers, and other inert ingredients) are ex- § 180.1119 Azadirachtin; exemption empted from the requirement of a tol- from the requirement of a toler- erance when used as carriers in pes- ance. ticide formulations for application to An exemption from the requirement growing crops only. These dispensers of a tolerance is established for the bio- shall conform to the following speci- chemical azadirachtin, which is iso- fications: lated from the berries of the Neem tree (1) Exposure must be limited to inad- (Azadirachta indica), when used as a vertent physical contact only. The de- pesticide at 20 grams or less per acre on sign of the dispenser must be such as to all raw agricultural commodities. preclude any contamination by its [58 FR 8696, Feb. 17, 1993] components of the raw agricultural commodity (RAC) or processed foods/ § 180.1120 Streptomyces sp. strain K61; feeds derived from the commodity by exemption from the requirement of virtue of its proximity to the RAC or a tolerance. as a result of its physical size. The biological pesticide Streptomyces (2) The dispensers must be applied sp. strain K61 is exempted from the re- discretely. This exemption does not quirement of a tolerance in or on all apply to components of semiochemical raw agricultural commodities when formulations applied in a broadcast

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manner either to a crop field plot or to (2) The dispensers must be applied individual plants. discretely, i.e., placed in the field in (b) A semiochemical dispenser is a easily perceived distinct locations in a single enclosed or semi-enclosed unit manner that does not prevent later re- that releases semiochemical(s) into the trieval. This exemption does not apply surrounding atmosphere via volatiliza- to codlure applied in a broadcast man- tion and is applied in a manner to pro- ner either to a crop field plot or to in- vide discrete application of the dividual plants. semiochemical(s) into the environ- (b) A codlure dispenser is a single en- ment. closed or semi-enclosed unit that re- (c) Semiochemicals are chemicals leases codlure into the surrounding at- that are emitted by plants or animals mosphere via volatilization and is ap- and modify the behavior of receiving plied in a manner to provide discrete organisms. These chemicals must be application (i.e., in easily perceived dis- naturally occurring or substantially tinct locations in a manner that does identical to naturally occurring not prevent later retrieval) of the semiochemicals. codlure into the environment. [58 FR 64494, Dec. 8, 1993] [59 FR 9931, Mar. 2, 1994]

§ 180.1124 Arthropod pheromones; ex- § 180.1127 Biochemical pesticide plant emption from the requirement of a floral volatile attractant com- tolerance. pounds: cinnamaldehyde, cinnamyl alcohol, 4-methoxy cinnamaldehyde, Arthropod pheromones, as described 3-phenyl propanol, 4-methoxy in § 152.25(b) of this chapter, when used phenethyl alcohol, indole, and 1,2,4- in retrievably sized polymeric matrix trimethoxybenzene; exemptions dispensers are exempt from the re- from the requirement of a toler- quirement of a tolerance in or on all ance. raw agricultural commodities when ap- Residues of the biochemical pesticide plied to growing crops only at a rate plant floral volatile attractant com- not to exceed 150 grams active ingre- pounds: cinnamaldehyde, cinnamyl al- dient/acre/year in accordance with good cohol, 4-methoxy cinnamaldehyde, 3- agricultural practices. phenyl propanol, 4-methoxy phenethyl alcohol, indole, and 1,2,4- [59 FR 14759, Mar. 30, 1994] trimethoxybenzene are exempt from the requirement of a tolerance in or on § 180.1126 Codlure, (E,E)-8,10- the following raw agricultural com- Dodecadien-1-ol; exemption from the requirement of a tolerance. modities: the following field crops—alfalfa, clover, cotton, dandelion, pea- An exemption from the requirement nuts (including hay), rice, sorghum of a tolerance is established for the in- (milo), soybeans, sunflower, sweet po- sect pheromone codlure, (E,E)-8,10- tatoes, and wheat; the following vege- dodecadien-1-ol, on all raw agricultural table crops—asparagus, beans (includ- commodities in accordance with the ing forage hay), beets, carrots, celery, following prescribed conditions: cole crops (cabbage, broccoli, brussels (a) Application shall be limited sole- sprouts, cauliflower), collards (kale, ly to codlure dispensers that conform mustard greens, turnip greens, kohl- to the following specifications: rabi), corn, fresh (field, sweet, pop, (1) Commodity exposure must be lim- seed), corn fodder and forage, chinese ited to inadvertent physical contact. cabbage, cowpeas, cucurbitis (cucum- The design of the dispenser must be bers, squash, pumpkin), egg plant, en- such as to preclude any exposure of its dive (escarole), horseradish (radish, ru- components to the raw agricultural tabagas, turnip roots), leafy greens commodity (RAC) or processed foods/ (spinach, swiss chard), lettuce (head feeds derived from the commodity due leaf), okra, parsley, parsnip, peas, peas to its proximity to the RAC or as a re- with pods, peppers, potatoes, sugar sult of its physical size. Dispensers beets, tomatoes; the following tree must be of such size and construction fruit, berry and nut crops—almonds, that they are readily recognized post- apples, apricots, berries (blackberry, application. boysenberry, dewberry, loganberry,

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raspberry), blueberry, cherry, citrus in the production of fruits and vegeta- (grapefruit, kumquat, lemon, lime, or- bles in greenhouses. ange, tangelo, and tangerine) cranberry, grapes, melons, (watermelon, [59 FR 66741, Dec. 28, 1994] honeydew, crenshaw, cantaloupe, ca- § 180.1139 Sodium 5-nitroguaiacolate; saba, persian), nectarines, pears, pe- exemption from the requirement of cans, peaches, and strawberry as dis- a tolerance. persed from the end-use product Corn Rootworm Bait ®, a pesticidal bait, in The biochemical sodium 5- accordance with the prescribed condi- nitroguiacolate is exempted from the tions in paragraph (a) of this section. requirement of a tolerance when used (a) Cumulative yearly application as a plant growth regulator in end-use cannot exceed 20 grams of each floral products at a concentration of 0.1% by attractant/acre/application. weight and applied at an application (b) [Reserved] rate of 20 g of a.i. per acre or less per application, in or on all food commod- [59 FR 15857, Apr. 5, 1994] ities. § 180.1128 Bacillus amyloliquefaciens [65 FR 66181, Nov. 3, 2000] MBI600; exemption from the requirement of a tolerance. § 180.1140 Sodium o-nitrophenolate; An exemption from the requirement exemption from the requirement of of a tolerance is established for resi- a tolerance. dues of the biofungicide Bacillus The biochemical sodium o- amyloliquefaciens MBI600 (antecedent nitrophenolate is exempted from the Bacillus subtilis MBI600) in or on all requirement of a tolerance when used food commodities, including residues as a plant growth regulator in end-use resulting from post-harvest uses, when products at a concentration of 0.2% by applied or used in accordance wi weight and applied at an application [80 FR 78143, Dec. 16, 2015] rate of 20 g of a.i. per acre or less per application, in or on all food commod- § 180.1130 N-(n-octyl)-2-pyrrolidone ities. and N-(n-dodecyl)-2-pyrrolidone; exemptions from the requirement of a [65 FR 66181, Nov. 3, 2000] tolerance. § 180.1141 Sodium p-nitrophenolate; (a) N-(n-octyl)-2-pyrrolidone and N- exemption from the requirement of (n-dodecyl)-2-pyrrolidone are exempt a tolerance. from the requirement of a tolerance The biochemical sodium p- when used as solvents in cotton defo- nitrophenolate is exempted from the liant formulations containing thidiazuron and diuron as active ingre- requirement of a tolerance when used dients. as a plant growth regulator in end-use (b) N-(n-octyl)-2-pyrrolidone is ex- product at a concentration of 0.3% by empt from the requirement of a toler- weight and applied at an application ance when used as a solvent in formu- rate of 20 g of a.i. per acre or less per lations containing pyraflufen-ethyl as application, in or on all food commod- an active ingredient at a concentration ities. not to exceed 20% by weight. [65 FR 66181, Nov. 3, 2000] [79 FR 10682, Feb. 26, 2014] § 180.1142 1,4-Dimethylnaphthalene; § 180.1135 Pasteuria penetrans; exemp- exemption from the requirement of tion from the requirement of a tol- a tolerance. erance. An exemption from the requirement The biological nematicide Pasteuria of a tolerance is established for the res- penetrans is exempted from the require- idues of the plant growth regulator, ment of a tolerance in or on all raw ag- 1,4-dimethylnaphthalene (1,4-DMN), ricultural commodities, except roots and tubers, when used as a nematicide

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when applied postharvest to all sprout- falcifera is exempted from the require- ing root, tuber, and bulb crops in ac- ment of a tolerance in or on all raw ag- cordance with good agricultural prac- ricultural commodities when used to tices. control certain lepidopteran pest spe- [77 FR 68697, Nov. 16, 2012] cies.

§ 180.1143 Methyl anthranilate; exemp- [60 FR 37020, July 19, 1995] tion from the requirement of a tolerance. § 180.1150 6-Benzyladenine; exemption from the requirement of a toler- Residues of methyl anthranilate, a ance. biochemical pesticide, are exempt from the requirement of a tolerance in or on The biochemical plant regulator 6- all food commodities, when used in ac- benzyladenine (6–BA) is exempt from cordance with good agricultural prac- the requirement of a tolerance in or on tices. apple and pear when applied at a rate of ≤182 grams of active ingredient per [67 FR 51088, Aug. 7, 2002] acre per season, and in or on pistachio § 180.1145 Pseudomonas syringae; ex- when applied at a rate of ≤60 grams of emption from the requirement of a active ingredient per acre per season. tolerance. [72 FR 13179, Mar. 21, 2007] Pseudomonas syringae is exempted from the requirement of a tolerance on § 180.1153 Lepidopteran pheromones; all raw agricultural commodities when exemption from the requirement of applied postharvest according to good a tolerance. agricultural practices. Lepidopteran pheromones that are [60 FR 12703, Mar. 8, 1995] naturally occurring compounds, or identical or substantially similar syn- § 180.1146 Beauveria bassiana Strain thetic compounds, designated by an GHA; exemption from the requirement of a tolerance. unbranched aliphatic chain (between 9 and 18 carbons) ending in an alcohol, Strain GHA is ex- Beauveria bassiana aldehyde or acetate functional group empted from the requirement of a tol- and containing up to 3 double bonds in erance in or on all raw agricultural the aliphatic backbone, are exempt commodities when applied to growing crops according to good agricultural from the requirement of a tolerance in practices. or on all raw agricultural commodities. This exemption only pertains to those [60 FR 18547, Apr. 12, 1995] situations when the pheromone is: Ap- plied to growing crops at a rate not to § 180.1148 Occlusion Bodies of the Granulosis Virus of Cydia exceed 150 grams active ingredient/ pomenella; tolerance exemption. acre/year in accordance with good agri- An exemption from the requirement cultural practices; and applied as a of a tolerance is established for resi- post-harvest treatment to stored food dues of the microbial pest control commodities at a rate not to exceed 3.5 agent Occlusion Bodies of the grams active ingredient/1,000 ft2/year Granulosis Virus of Cydia pomonella (equivalent to 150 grams active ingre- (codling moth) in or on all raw agricul- dient/acre/year) in accordance with tural commodities. good agricultural practices. [60 FR 42450, Aug. 16, 1995] [71 FR 45399, Aug. 9, 2006]

§ 180.1149 Inclusion bodies of the § 180.1156 Cinnamaldehyde; exemption multi-nuclear polyhedrosis virus of from the requirement of a toler- Anagrapha falcifera; exemption ance. from the requirement of a tolerance. Cinnamaldehyde (3-phenyl-2- The microbial pest control agent in- propenal) is exempted from the re- clusion bodies of the multi-nuclear quirement of a tolerance in or on all polyhedrosis virus of Anagrapha

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food commodities, when used as a fun- (c) An exemption from the require- gicide, insecticide, and algaecide in ac- ment of a tolerance is established for cordance with good agricultual prac- residues of pelargonic acid in or on all tices. raw agricultural commodities and in processed commodities, when such resi- [64 FR 7804, Feb. 17, 1999; 64 FR 14099, Mar. 24, 1999] dues result from the use of pelargonic acid as an antimicrobial treatment in § 180.1157 Cytokinins; exemption from solutions containing a diluted end-use the requirement of a tolerance. concentration of pelargonic acid up to 170 ppm per application on food contact An exemption from the requirement surfaces such as equipment, pipelines, of a tolerance is established for resi- tanks, vats, fillers, evaporators, dues of cytokinins (specifically: aque- pasteurizers and aseptic equipment in ous extract of seaweed meal and restaurants, food service operations, kinetin) in or on all food commodities dairies, breweries, wineries, beverage when used as plant regulators on and food processing plants. plants, seeds, or cuttings and on all food commodities after harvest in ac- [62 FR 28364, May 23, 1997, as amended at 64 cordance with good agricultural prac- FR 31505, June 11, 1999; 68 FR 7935, Feb. 19, tices. 2003] [64 FR 31505, June 11, 1999] § 180.1160 Jojoba oil; exemption from the requirement of a tolerance. § 180.1158 Auxins; exemption from the The insecticide and spray tank adju- requirement of a tolerance. vant jojoba oil is exempted from the An exemption from the requirement requirement of a tolerance in or on all of a tolerance is established for resi- raw agricultural commodities when ap- dues of auxins (specifically: indole-3- plied at the rate of 1.0% or less of the acetic acid and indole-3-butyric acid) final spray in accordance with good ag- in or on all food commodities when ricultural practices, provided the used as plant regulators on plants, jojoba oil does not contain seeds, or cuttings and on all food com- simmondsin, simmondsin-2-ferulate, modities after harvest in accordance and related conjugated organonitriles with good agricultural practices. including demethyl simmondsin and didemethylsimmondsin. [64 FR 31505, June 11, 1999] [61 FR 2121, Jan. 25, 1996] § 180.1159 Pelargonic acid; exemption from the requirement of tolerances. § 180.1161 Clarified hydrophobic ex- (a) An exemption from the require- tract of neem oil; exemption from the requirement of a tolerance. ment of a tolerance is established for residues of pelargonic acid in or on all Clarified hydrophobic extract of food commodities when used as a plant neem oil is exempt from the require- regulator on plants, seeds, or cuttings ment of a tolerance on all food com- and on all food commodities after har- modities when used as a botanical fun- vest in accordance with good agricul- gicide/insecticide/miticide. tural practices. [67 FR 43552, June 28, 2002] (b) Pelargonic acid when used as an herbicide is exempt from the require- § 180.1162 Acrylate polymers and co- ment of a tolerance on all plant food polymers; exemption from the re- commodities provided that: quirement of a tolerance. (1) Applications are not made di- (a) Acrylate polymers and copoly- rectly to the food commodity except mers are exempt from the requirement when used as a harvest aid or desiccant of a tolerance when used as inert ingre- to: any root and tuber vegetable, bulb dients in pesticidal formulations ap- vegetable or cotton. plied to growing, raw agricultural com- (2) When pelargonic acid is used as a modities. This tolerance exemption harvest aid or desiccant, applications covers the acrylate polymers/copoly- must be made no later than 24 hours mers that are intrinsically safe and al- prior to harvest. ready listed in TSCA inventory or will

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meet the polymer tolerance exemption with approved label rates and good ag- from requirements of ricultural practice. premanufacturing notification under 40 [63 FR 39521, July 23, 1998] CFR 723.250. Polymers exempted can be used as dispensers, resins, fibers, and § 180.1167 Allyl isothiocyanate as a beads, as long as the fibers, beads and component of food grade oil of mus- resins particle sizes are greater than 10 tard; exemption from the require- microns and insoluble in water. This ment of a tolerance. exemption pertains to the acrylate The insecticide and repellent Allyl polymers/copolymers used as inert in- isothiocyanate is exempt from the re- gredients for sprayable and dispenser quirement of a tolerance for residues pesticide formulations that are applied when used as a component of food on food crops. Any acrylate polymers/ grade oil of mustard, in or on all raw copolymers used for encapsulating ma- agricultural commodities, when ap- terial must be cleared as an inert in- plied according to approved labeling. gredient when used in pesticide formulation applied on food crops. [61 FR 24894, May 17, 1996] (b) For the purposes of this exemp- § 180.1176 Sodium bicarbonate; exemption, acrylate polymers/copolymers tion from the requirement of a tol- used as inert ingredients in an end-use erance. formulation must meet the definition for a polymer as given in 40 CFR The biochemical pesticide sodium bi- 723.250(b), are not automatically ex- carbonate is exempted from the re- cluded by 40 723.250(d), and meet the quirement of a tolerance in or on all tolerance exemption criteria in 40 CFR raw agricultural commodities when ap- 723.250(e)(1), 40 CFR 723.250 (e)(2) or 40 plied as a fungicide or post-harvest fun- CFR 723.250(e)(3). Therefore, acrylate gicide in accordance with good agricul- polymers and copolymers that are al- tural practices. ready listed in the TSCA inventory or [61 FR 67473, Dec. 23, 1996] will meet the polymer tolerance exemption under 40 CFR 723.250 as § 180.1177 Potassium bicarbonate; ex- amended on March 29, 1995 are covered emption from the requirement of a by this exemption. tolerance. [61 FR 6551, Feb. 21, 1996] The biochemical pesticide potassium bicarbonate is exempted from the re- § 180.1163 Killed Myrothecium quirement of a tolerance in or on all verrucaria; exemption from the re- raw agricultural commodities when ap- quirement of a tolerance. plied as a fungicide or post-harvest fun- Killed Myrothecium verrucaria is ex- gicide in accordance with good agricul- empted from the requirement of a tol- tural practices. erance in or on all raw agricultural [61 FR 67473, Dec. 23, 1996] commodities when applied as a pre- seed or pre- or post-planting soil treat- § 180.1178 Formic acid; exemption ment alone or mixed with water and from the requirement of a toler- the mixed suspension be applied ance. through drip or border irrigation sys- The pesticide formic acid is exempted tems and the indicator mycotoxin lev- from the requirement of a tolerance in els do not exceed 15 ppm. or on honey and honeycomb when used [61 FR 11315, Mar. 20, 1996, as amended at 61 to control tracheal mites and suppress FR 58332, Nov. 14, 1996] varroa mites in bee colonies, and applied in accordance with label use di- § 180.1165 Capsaicin; exemption from rections. the requirement of a tolerance. [74 FR 26535, June 3, 2009] Capsaicin is exempt from the requirement of a tolerance in or on all food commodities when used in accordance

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§ 180.1179 Plant extract derived from § 180.1189 Methyl salicylate; exemption Opuntia lindheimeri, Quercus from the requirement of a toler- falcata, Rhus aromatica, and ance. Rhizophoria mangle; exemption The biochemical pesticide methyl sa- from the requirement of a toler- licylate is exempt from the require- ance. ment of a tolerance for residues in or The biochemical pesticide plant ex- on food or feed when used as an insect tract derived from Opuntia lindheimeri, repellant in food packaging and animal Quercus falcata, Rhus aromatica, and feed packaging at an application rate Rhizophoria mangle is exempted from that does not exceed 0.2 mg of methyl the requirement of a tolerance in or on salicylate per square inch of packaging all raw agricultural commodities when materials. applied as a nematicide/plant regulator [62 FR 61639, Nov. 19, 1997] in accordance with good agricultural practices. § 180.1191 Ferric phosphate; exemption from the requirement of a tol- [62 FR 24842, May 7, 1997] erance. An exemption from the requirement § 180.1180 Kaolin; exemption from the of a tolerance is established for resi- requirement of a tolerance. dues of the biochemical pesticide, fer- Kaolin is exempted from the require- ric phosphate (FePO4, CAS No. 11045– ment of a tolerance for residues when 86–0) in or on all food commodities. used on or in food commodities to aid [62 FR 56105, Oct. 29, 1997] in the control of insects, fungi, and bacteria (food/feed use). § 180.1193 Potassium dihydrogen phos- [81 FR 34907, June 1, 2016] phate; exemption from the requirement of a tolerance. § 180.1181 Bacillus cereus strain BPO1; Potassium dihydrogen phosphate is exemption from the requirement of exempted from the requirement of a a tolerance. tolerance in or on all food commodities An exemption from the requirement when applied as a fungicide in accord- of a tolerance for residues of the Bacil- ance with good agricultural practices. lus cereus strain BPO1 in or on all raw [63 FR 43085, Aug. 12, 1998] agricultural commodities when applied/used in accordance with label di- § 180.1195 Titanium dioxide. rections. (a) Titanium dioxide (CAS Reg. No. 13463–67–7) is exempted from the re- [67 FR 70017, Nov. 20, 2002] quirement of a tolerance for residues in § 180.1187 L-glutamic acid; exemption or on growing crops, when used as an from the requirement of a toler- inert ingredient (UV protectant) in ance. microencapsulated formulations of the insecticide lambda cyhalothrin at no L-glutamic acid is exempt from the more than 3.0% by weight of the formu- requirement of a tolerance on all food lation and as an inert ingredient (UV commodities when used in accordance stabilizer) at no more than 5% in pes- with good agricultural practices. ticide formulations containing the ac- [66 FR 33198, June 21, 2001] tive ingredient napropamide. (b) Residues of titanium dioxide (CAS § 180.1188 Gamma aminobutyric acid; Reg. No. 13463–67–7) in honey are ex- exemption from the requirement of empted from the requirement of a tol- a tolerance. erance, when used as an inert ingre- Gamma aminobutyric acid is exempt dient (colorant) in pesticide formula- from the requirement of a tolerance on tions intended for varroa mite control all food commodities when used in ac- around bee hives at no more than 0.1% cordance with good agricultural prac- by weight in the pesticide formulation. (c) Titanium dioxide (CAS Reg. No. tices. 13463–67–7) is exempted from the re- [66 FR 33198, June 21, 2001] quirement of a tolerance for residues in

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or on growing crops, when used as an hydrogen peroxide per application on inert ingredient (colorant) in foliar ap- growing and postharvest crops. plications at no more than 45% of the [67 FR 41844, June 20, 2002] formulations containing anthraquinone. § 180.1198 Gliocladium catenulatum [82 FR 30997, July 5, 2017, as amended at 83 strain J1446; exemption from the FR 8619, Feb. 28, 2018] requirement of a tolerance. An exemption from the requirement § 180.1196 Peroxyacetic acid; exemp- of a tolerance is established for resi- tion from the requirement of a tol- dues of the microbial pesticide, erance. Gliocladium catenulatum strain J1446 (a) An exemption from the require- when used in or on all food commod- ment of a tolerance is established for ities. residues of peroxyacetic acid in or on all food commodities, when such resi- [63 FR 37288, July 10, 1998] dues result from the use of peroxy- § 180.1199 acetic acid as an antimicrobial treat- Lysophosphatidylethanolamine ment in solutions containing a diluted (LPE); exemption from the require- end use concentration of peroxyacetic ment of a tolerance. acid up to 100 ppm per application on An exemption from the requirement fruits, vegetables, tree nuts, cereal of a tolerance is established for resi- grains, herbs, and spices. dues of the biochemical pesticide (b) An exemption from the require- lysophosphatidylethanolamine in or on ment of a tolerance is established for all food commodities. residues of peroxyacetic acid, in or on all food commodities when used in [67 FR 17636, Apr. 11, 2002] sanitizing solutions containing a diluted end-use concentration of peroxy- § 180.1202 Bacillus sphaericus; exemp- acetic acid up to 500 ppm, and applied tion from the requirement of a tolerance. to tableware, utensils, dishes, pipelines, tanks, vats, fillers, evaporators, An exemption from the requirement pasteurizers, aseptic equipment, milk- of a tolerance is established for resi- ing equipment, and other food proc- dues of the microbial pesticides, Bacil- essing equipment in food handling es- lus sphaericus when used in or on all tablishments including, but not limited food crops. to dairies, dairy barns, restaurants, [63 FR 48597, Sept. 11, 1998] food service operations, breweries, wineries, and beverage and food proc- § 180.1204 Harpin protein; exemption essing plants. from the requirement of a toler- (c) An exemption from the require- ance. ment of a tolerance is established for An exemption from the requirement residues of the biochemical pesticide of a tolerance is established for resi- peroxyacetic acid and its metabolites dues of individual harpin proteins that and degradates, including hydrogen meet specified physiochemical and tox- peroxide and acetic acid, in or on all icological criteria when used as bio- food commodities, when used in ac- chemical pesticides on all food com- cordance with good agricultural prac- modities to enhance plant growth, tices. quality and yield, to improve overall [74 FR 26535, June 3, 2009, as amended at 76 plant health, and to aid in pest man- FR 11969, Mar. 4, 2011] agement. The physiochemical and toxicological criteria identifying harpin § 180.1197 Hydrogen peroxide; exemp- proteins are as follows: tion from the requirement of a tol- (a) Consists of a protein less than 100 erance. kD in size, that is acidic (pI<7.0), gly- An exemption from the requirement cine rich (>10%), and contains no more of a tolerance is established for resi- than one cystine residue. dues of hydrogen peroxide in or on all (b) The source(s) of genetic material food commodities at the rate of ≤1% encoding the protein are bacterial

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plant pathogens not known to be mam- pop, grain; and corn, pop, stover, when malian pathogens. applied/used as an antifungal agent. (c) Elicits the hypersensitive re- (d) Section 18 emergency exemptions. A sponse (HR) which is characterized as time-limited exemption from the re- rapid, localized cell death in plant tis- quirement of a tolerance is established sue after infiltration of harpin into the for residues of Aspergillus flavus AF36, intercellular spaces of plant leaves. in or on dried figs, resulting from use (d) Possesses a common secondary of the pesticide pursuant to a FIFRA structure consisting of a and b units section 18 emergency exemption. This that form an HR domain. time-limited exemption from the re- (e) Is heat stable (retains HR activity quirement of a tolerance for residues of ° when heated to 65 C for 20 minutes). Aspergillus flavus AF36 in or on dried (f) Is readily degraded by a proteinase figs will expire and is revoked on De- representative of environmental condi- cember 31, 2017. tions (no protein fragments >3.5 kD after 15 minutes degradation with (e) An exemption from the require- Subtilisin A). ment of a tolerance is established for (g) Exhibits a rat acute oral toxicity residues of Aspergillus flavus AF36 in or on almond and fig when used in accord- (LD50) of greater than 5,000 mg product/ kg body weight. ance with label directions and good agricultural practices. [69 FR 24996, May 5, 2004] [68 FR 41541, July 14, 2003, as amended at 72 § 180.1205 Beauveria bassiana ATCC FR 28871, May 23, 2007; 72 FR 72965, Dec. 26, #74040; exemption from the require- 2007; 74 FR 26535, 26546, June 3, 2009; 76 FR ments of a tolerance. 16301, Mar. 23, 2011; 77 FR 14291, Mar. 9, 2012; An exemption from the requirement 81 FR 1894, Jan. 14, 2016; 82 FR 14632, Mar. 22, of a tolerance is established for resi- 2017] dues of the insecticide Beauveria § 180.1207 N-acyl sarcosines and so- bassiana (ATCC #74040) in or on all food dium N-acyl sarcosinates; exemp- commodities when applied or used as tion from the requirement of a tol- ground and aerial foliar sprays for use erance. only on terrestrial crops. An exemption from the requirement [64 FR 22796, Apr. 28, 1999] of a tolerance is established for residues of the following substances when § 180.1206 Aspergillus flavus AF36; exemption from the requirement of a used as inert ingredients (surfactants) tolerance. at levels not to exceed 10% in pesticide formulations containing glyphosate: (a) An exemption from the requirement of a tolerance is established for CAS Reg. residues of the microbial pesticide As- Name No. pergillus flavus AF36 in or on cotton, N-acyl sarcosines. gin byproducts; cotton, hulls; cotton, N-cocoyl sarcosine mixture ...... 68411-97-2 meal; cotton, refined oil; cotton, N-lauroyl sarcosine ...... 97-78-9 undelinted seed. N-myristoyl sarcosine ...... 52558-73-3 (b) An exemption from the require- N-oleoyl sarcosine ...... 110-25-8 ment of a tolerance is established for N-stearoyl sarcosine ...... 142-48-3 residues of Aspergillus flavus AF36 in or Sodium N-acyl sarcosinates. N-cocoyl sarcosine sodium salt mixture ...... 61791-59-1 on pistachio when applied as an N-methyl-N-(1-oxo-9-octodecenyl) glycine .... 3624-77-9 antifungal agent and used in accord- N-methyl-N-(1-oxododecyl) glycine ...... 137-16-6 ance with good agricultural practices. N-methyl-N-(1-oxooctadecyl) glycine ...... 5136-55-0 (c) An exemption from the require- N-methyl-N-(1-oxotetradecyl glycine ...... 30364-51-3 ment of a tolerance is established for residues of Aspergillus flavus AF36 in or [64 FR 68046, Dec. 6, 1999] on corn, field, forage; corn, field, grain; corn, field, stover; corn, field, aspirated grain fractions; corn, sweet, kernel plus cob with husk removed; corn, sweet, forage; corn, sweet, stover; corn,

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§ 180.1209 Bacillus subtilis strain QST § 180.1218 Indian Meal Moth 713 and strain QST 713 variant soil; Granulosis Virus; exemption from exemption from the requirement of the requirement of a tolerance. a tolerance. An exemption from the requirement An exemption from the requirement of a tolerance is established for resi- of a tolerance is established for residues of the microbial pesticide Indian dues of the microbial pesticides Bacil- Meal Moth Granulosis Virus when used lus subtilis strain QST 713 and strain in or on all food commodities. QST 713 variant soil when used in or on [68 FR 55875, Sept. 29, 2003] all food commodities. § 180.1219 Foramsulfuron; exemption [77 FR 73937, Dec. 12, 2012] from the requirement of a tolerance. § 180.1210 Phosphorous acid; exemp- The pesticide foramsulfuron is ex- tion from the requirement of a tol- empted from the requirement of a tolerance. erance in corn, field, grain/corn, field, (a) An exemption from the require- forage/ corn, field, stover/corn, pop, ment of a tolerance is established for grain/corn, pop, forage/corn, pop, sto- residues of phosphorous acid and its ver; corn, sweet, forage; corn, sweet, ammonium, sodium and potassium kernel plus cob with husks removed; salts in or on all food commodities corn, sweet, stover when applied as a when used as an agricultural fungicide herbicide in accordance with good agri- and in or on potatoes when applied as cultural practices. a post-harvest treatment at 35,600 ppm [74 FR 26535, June 3, 2009] or less phosphorous acid. (b) An exemption from the require- § 180.1220 1-Methylcyclopropene; ex- ment of a tolerance is established for emption from the requirement of a tolerance. residues of calcium salts of phosphorous acid, including its metabolites An exemption from the requirement and degradates, in or on all food com- of a tolerance is established for resi- modities when used as a fungicide or as dues of the 1-Methylcyclopropene in or a systemic acquired resistance (SAR) on fruits and vegetables when: (a) Used as a post harvest plant inducer. growth regulator, i.e., for the purpose [83 FR 3605, Jan. 26, 2018] of inhibiting the effects of ethylene. (b) Applied or used outdoors for pre- § 180.1212 Pseudomonas chlororaphis harvest treatments. Strain 63–28; exemption from the requirement of a tolerance. [73 FR 19150, Apr. 9, 2008] An exemption from the requirement § 180.1222 Sucrose octanoate esters; of a tolerance is established for resi- exemption from the requirement of dues of the microbial pesticide a tolerance. Pseudomonas chlororaphis Strain 63–28 An exemption from the requirement in or on all food commodities. of a tolerance is established for residues of sucrose octanoate esters [(a-D- [66 FR 53346, Oct. 22, 2001] glucopyranosyl-b-D-fructofuranosyl-octanoate), mono-, di-, and triesters of § 180.1213 Coniothyrium minitans sucrose octanoate] in or on all food strain CON/M/91–08; exemption from the requirement of a toler- commodities when used in accordance ance. with good agricultural practices. An exemption from the requirement [67 FR 60152, Sept. 25, 2002] of a tolerance is established for resi- § 180.1223 Imazamox; exemption from dues of the microbial pesticide the requirement of a tolerance. Coniothyrium minitans strain CON/M/91– ± 08 when used in or on all food commod- The herbicide imazamox, ( ) 2, -[4,5- dihydro-4-methyl-4-(1-methylethyl)-5- ities. oxo-1H-imidazol-2-yl]-5- [66 FR 16874, Mar. 28, 2001] (methoxymethyl)-3-pyridinecarboxylic

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acid, is exempt from the requirement § 180.1228 Diallyl sulfides; exemption of a tolerance on all food commodities from the requirement of a toler- when applied as a herbicide in accordance. ance with good agricultural practices. An exemption from the requirement [68 FR 7433, Feb. 14, 2003] of a tolerance is established for residues of diallyl sulfides when used in/on § 180.1224 Bacillus pumilus GB34; ex- garlic, leeks, onions, and shallots. emption from the requirement of a [68 FR 40808, July 9, 2003] tolerance. An exemption from the requirement § 180.1230 Ferrous sulfate; exemption of a tolerance is established for resi- from the requirement of a toler- dues of the microbial pesticide Bacillus ance. pumilus GB34 when used as a seed treat- An exemption from the requirement ment in or on all food commodities. An of a tolerance is established for resi- exemption is also granted for such residues of ferrous sulfate. dues on treated but unplanted soybean [70 FR 33363, June 8, 2005] seeds. [69 FR 76625, Dec. 22, 2004] § 180.1231 Lime; exemption from the requirement of a tolerance. § 180.1225 Decanoic acid; exemption An exemption from the requirement from the requirement of a toler- of a tolerance is established for resi- ance. dues of lime. An exemption from the requirement [70 FR 33363, June 8, 2005] of a tolerance is established for residues of decanoic acid in or on all raw § 180.1232 Lime-sulfur; exemption from agricultural commodities and in proc- the requirement of a tolerance. essed commodities, when such residues An exemption from the requirement result from the use of decanoic acid as of a tolerance is established for resi- an antimicrobial treatment in solu- dues of lime-sulfur. tions containing a diluted end-use concentration of decanoic acid (up to 170 [70 FR 33363, June 8, 2005] ppm per application) on food contact surfaces such as equipment, pipelines, § 180.1233 Potassium sorbate; exemp- tanks, vats, fillers, evaporators, tion from the requirement of a tolerance. pasteurizers and aseptic equipment in restaurants, food service operations, An exemption from the requirement dairies, breweries, wineries, beverage of a tolerance is established for resi- and food processing plants. dues of potassium sorbate. [68 FR 7939, Feb. 19, 2003; 68 FR 17308, Apr. 9, [70 FR 33363, June 8, 2005] 2003] § 180.1234 Sodium carbonate; exemp- § 180.1226 Bacillus pumilus strain tion from the requirement of a tol- QST2808; temporary exemption erance. from the requirement of a toler- An exemption from the requirement ance. of a tolerance is established for resi- A temporary exemption from the re- dues of sodium carbonate. quirement of a tolerance is established [70 FR 33363, June 8, 2005] for residues of the microbial pesticide Bacillus pumilus strain QST2808 when § 180.1235 Sodium hypochlorite; ex- used in or on all agricultural commod- emption from the requirement of a ities when applied/used in accordance tolerance. with label directions. An exemption from the requirement [68 FR 36480, June 18, 2003] of a tolerance is established for residues of sodium hypochlorite. [70 FR 33363, June 8, 2005]

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§ 180.1236 Sulfur; exemption from the § 180.1243 Bacillus subtilis var. requirement of a tolerance. amyloliquefaciens strain FZB24; exemption from the requirement of a An exemption from the requirement tolerance. of a tolerance is established for residues of sulfur. An exemption from the requirement of a tolerance for residues of the Bacil- [70 FR 33363, June 8, 2005] lus subtilis var. amyloliquefaciens strain FZB24 in or on all agricultural com- § 180.1237 Sodium metasilicate; exemp- modities when applied/used in accord- tion from the requirement of a tol- ance with label directions. erance. [68 FR 44640, July 30, 2003] (a) An exemption from the requirement of a tolerance is established for § 180.1244 Ammonium bicarbonate; ex- residues of sodium metasilicate in or emption from the requirement of a on all food commodities when used in tolerance. accordance with approved label rates An exemption from the requirement and good agricultural practices as a of tolerance is established for residues plant desiccant, so long as the sodium of ammonium bicarbonate used in or metasilicate does not exceed 4% by on all food commodities when used in weight in aqueous solution. accordance with good agricultural (b) An exemption from the require- practices. ment of a tolerance is established for residues of sodium metasilicate in or [69 FR 13745, Mar. 24, 2004] on all food commodities when used in § 180.1245 Rhamnolipid biosurfactant; accordance with approved label rates exemption from the requirement of and good agricultural practices as an a tolerance. insecticide and fungicide, so long as An exemption from the requirement the sodium metasilicate does not ex- of a tolerance is established for resi- ceed 2.41% by weight in aqueous solu- dues of rhamnolipid biosurfactant tion. when used in accordance with good ag- [71 FR 19441, Apr. 14, 2006] ricultural practices as a fungicide in or on all food commodities. § 180.1240 Thymol; exemption from the [69 FR 16800, Mar. 31, 2004] requirement of a tolerance. (a) Time-limited exemptions from § 180.1246 Yeast Extract Hydrolysate the requirement of a tolerance are es- from Saccharomyces cerevisiae: ex- tablished for residues of thymol on emption from the requirement of a tolerance. honey and honeycomb in connection with use of the pesticide under section This regulation establishes an ex- 18 emergency exemptions granted by emption from the requirement of a tol- the EPA. These time-limited exemp- erance for residues of the biochemical tions from the requirement of a toler- pesticide Yeast Extract Hydrolysate ance for residues of thymol will expire from Saccharomyces cerevisiae on all and are revoked on June 30, 2007. food commodities when applied/used (b) An exemption from the require- for the management of plant diseases. ment of a tolerance for residues of the [69 FR 9958, Mar. 3, 2004] thymol (as present in thyme oil) in or on food commodities when applied/used § 180.1248 Exemption of citronellol in/on public eating places, dairy proc- from the requirement of a toler- essing equipment, and/or food proc- ance. essing equipment and utensils. An exemption from the requirement of a tolerance is established for resi- [70 FR 37696, June 30, 2005, as amended at 71 dues of the biochemical pesticide FR 2895, Jan. 18, 2006; 74 FR 12617, Mar. 25, citronellol in or on all food commod- 2009] ities. [69 FR 23146, Apr. 28, 2004]

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§ 180.1250 C8, C10, and C12 fatty acid § 180.1255 Bacillus pumilus strain QST monoesters of glycerol and pro- 2808; exemption from the require- pylene glycol; exemption from the ment of a tolerance. requirement of a tolerance. An exemption from the requirement The C8, C10, and C12 straight-chain of a tolerance is established for resi- fatty acid monoesters of glycerol (glyc- dues of the microbial pesticide Bacillus erol monocaprylate, glycerol pumilus strain QST 2808 when used in or monocaprate, and glycerol on all agricultural commodities when monolaurate) and propylene glycol applied/used in accordance with label (propylene glycol monocaprylate, pro- directions. pylene glycol monocaprate, and pro- [69 FR 63954, Nov. 3, 2004] pylene glycol monolaurate) are exempt from the requirement of a tolerance in § 180.1257 Purpureocillium lilacinum or on all food commodities when used strain 251; exemption from the re- in accordance with approved label rates quirement of a tolerance. and good agricultural practice. An exemption from the requirement of a tolerance is established for resi- [69 FR 34944, June 23, 2004] dues of Purpureocillium lilacinum strain § 180.1251 Geraniol; exemption from 251 in or on all food commodities when the requirement of a tolerance. applied/used in accordance with label directions and good agricultural prac- An exemption from the requirement tices. of a tolerance is established for residues of the biochemical pesticide gera- [84 FR 70022, Dec. 20, 2019] niol in or on all food commodities. § 180.1258 Acetic acid; exemption from [69 FR 23151, Apr. 28, 2004] the requirement of a tolerance. (a) An exemption from the require- § 180.1253 Streptomyces lydicus WYEC ment of a tolerance is established for 108; exemption from the require- residues of the biochemical pesticide ment of a tolerance. acetic acid when used as a preservative An exemption from the requirement on post-harvest agricultural commod- of a tolerance is established for resi- ities intended for animal feed, includ- dues of the microbial pesticide ing Alfalfa, seed; alfalfa, hay; barley, Streptomyces lydicus WYEC 108 when grain; bermudagrass, hay; bluegrass, used in or on all agricultural commod- hay; bromegrass, hay; clover, hay; ities when applied/used in accordance corn, field, grain; corn, pop, grain; with label directions. cowpea, hay; fescue, hay; lespedeza, hay; lupin; oat, grain; orchardgrass, [69 FR 31301, June 3, 2004] hay; peanut, hay; timothy, hay; vetch, hay; and wheat, grain, or commodities § 180.1254 Aspergillus flavus NRRL 21882; exemption from the require- described as grain or hay. ment of a tolerance. (b) An exemption from the requirement of a tolerance is established for (a) An exemption from the require- residues of acetic acid in or on all food ment of a tolerance is established for crops resulting from unintentional residues of Aspergillus flavus NRRL spray and drift to non-target vegeta- 21882 on peanut; peanut, hay; peanut, tion including non-food, food and feed meal; and peanut, refined oil. crops when used as a non-selective con- (b) An exemption from the require- tact herbicide spray. ment of a tolerance is established for residues of Aspergillus flavus NRRL [75 FR 40741, July 14, 2010] 21882 on corn, field, forage; corn, field, § 180.1259 Reynoutria sachalinensis ex- grain; corn, field, stover; corn, field, as- tract; exemption from the require- pirated grain fractions; corn, sweet, ment of a tolerance. kernel plus cob with husk removed; Residues of the biochemical pesticide corn, sweet, forage; corn, sweet, stover; Reynoutria sachalinensis extract, when corn, pop, grain; and corn, pop, stover. derived from the whole plant extract, [75 FR 6576, Feb. 10, 2010] are exempt from the requirement of a

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tolerance in or on all food commod- (e) For use in herbicides with two ap- ities. plications to field corn and popcorn up [70 FR 55277, Sept. 21, 2005] to 36 inches tall (V8 stage). (f) For use in herbicides with two ap- § 180.1260 Muscodor albus QST 20799 plications to canola prior to the early and the volatiles produced on re- bolting stage. hydration; exemption from the re- (g) For use in herbicides with two ap- quirement of a tolerance. plications to soybeans prior to the An exemption from the requirement bloom growth stage. of a tolerance is established on all food/ feed commodities, for residues of [71 FR 45415, Aug. 9, 2006, as amended at 83 Muscodor albus QST 20799, and the FR 53002, Oct. 19, 2018] volatiles produced on its rehydration, when the pesticide is used for all agri- § 180.1267 Pantoea agglomerans strain cultural applications, including seed, C9–1; exemption from the requirement of a tolerance. propagule and post harvest treatments. An exemption from the requirement [70 FR 56576, Sept. 28, 2005] of a tolerance is established for resi- § 180.1261 Xanthomonas campestris pv. dues of Pantoea agglomerans strain C9–1 vesicatoria and Pseudomonas when used on apples and pears. syringae pv. tomato specific Bacteriophages. [71 FR 24596, Apr. 26, 2006] An exemption from the requirement § 180.1268 Potassium silicate; exemp- of a tolerance is established for resi- tion from the requirement of a tol- dues of Xanthomonas campestris pv. erance. vesicatoria and Pseudomonas syringae pv. Potassium silicate is exempt from tomato specific bacteriophages in or on the requirement of a tolerance in or on pepper and tomato. all food commodities so long as the po- [74 FR 26536, June 3, 2009] tassium silicate is not applied at rates exceeding 1% by weight in aqueous so- § 180.1262 Sorbitol octanoate; exemption from the requirement of a tol- lution and when used in accordance erance. with good agricultural practices. An exemption from the requirement [71 FR 34272, June 14, 2006] of a tolerance is established for residues of sorbitol octanoate in or on all § 180.1269 Bacillus mycoides isolate J; food commodities when used in accord- exemption from the requirement of ance with label directions. a tolerance. [71 FR 4518, Jan. 27, 2006] An exemption from the requirement of a tolerance is established for resi- § 180.1263 Tetrahydrofurfuryl alcohol; dues of Bacillus mycoides isolate J in or exemption from the requirement of on all agricultural commodities when a tolerance. used in accordance with label direc- Tetrahydrofurfuryl alcohol (THFA, tions and good agricultural practices. CAS Reg. No. 97–99–4) is exempt from the requirement of a tolerance in or on [81 FR 67922, Oct. 3, 2016] all raw agricultural commodities when § 180.1270 Isophorone; exemption from used in accordance with good agricul- the requirement of a tolerance. tural practices as an inert ingredient applied only: Isophorone (CAS Reg. No. 78–59–1) is (a) For use as a seed treatment. exempt from the requirement of a tol- (b) For applications prior to planting erance when used as an inert ingre- and at the time of planting. dient in pesticide formulations applied (c) For use on cotton. to beets, ginseng, rice, spinach, sugar (d) For use in herbicides with one ap- beets, and Swiss chard. plication to wheat, buckwheat, barley, oats, rye, sorghum, triticale, rice, and [71 FR 45408, Aug. 9, 2006] wild rice prior to the pre-boot stage.

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§ 180.1271 Eucalyptus oil; exemption (d) The applications occur no later from the requirement of a toler- than the pre-boot stage (prior to for- ance. mation of edible grain). An exemption from the requirement [72 FR 5624, Feb. 7, 2007, as amended at 74 FR of tolerance is established for residues 26536, June 3, 2009] of eucalyptus oil in or on honey, honeycomb, and honeycomb with honey § 180.1275 Pythium oligandrum DV 74; when used at 2g or less eucalyptus oil exemption from the requirement of per hive, where the eucalyptus oil con- a tolerance. tains 80% or more eucalyptol. An exemption from the requirement of a tolerance is established on all food/ [71 FR 53979, Sept. 13, 2006] feed commodities for residues of § 180.1272 Pantoea agglomerans strain Pythium oligandrum DV 74 when the E325; exemption from the require- pesticide is used on food crops. ment of a tolerance. [81 FR 34907, June 1, 2016] An exemption from the requirement of a tolerance is established for resi- § 180.1276 Tobacco mild green mosaic dues of Pantoea agglomerans strain E325 tobamovirus strain U2; exemption when used on apples and pears. from the requirement of a tolerance. [71 FR 54933, Sept. 20, 2006] An exemption from the requirement § 180.1273 Beauveria bassiana HF23; of a tolerance is established for resi- exemption from the requirement of dues of Tobacco mild green mosaic a tolerance. tobamovirus strain U2 in or on all commodities of crop groups 17 and 18 when Residues of Beauveria bassiana HF23 applied as a post-emergent herbicide are exempt from the requirement of a and used in accordance with label di- tolerance on all food/feed commodities, rections and good agricultural prac- when the pesticide is used for the tices. treatment of chicken and livestock facilities, including the treatment of [79 FR 75756, Dec. 19, 2014] chicken and livestock manure. § 180.1277 Dibasic esters; exemption [75 FR 10190, Mar. 5, 2010] from the requirement of a tolerance. § 180.1274 Tris (2-ethylhexyl) phosphate; exemption from the require- Dibasic esters (CAS Reg. No. 95481–62– ment of a tolerance. 2) is exempted from the requirement of a tolerance for residues when used as Tris (2-ethylhexyl) phosphate (TEHP, an inert ingredient (solvent and/or CAS Reg. No. 78–42–2) is exempt from anti-freeze) at 10% W/W or less in the requirement of a tolerance for resi- microencapsulated pesticide formula- dues in grain, aspirated fractions; bar- tions with the active ingredient ley, grain, barley, hay, barley, straw; cyfluthrin. wheat, grain; wheat, forage; wheat, hay; wheat, straw when used under the [73 FR 10398, Feb. 27, 2008] following conditions: (a) The use is in accordance with § 180.1278 Quillaja saponaria extract good agricultural practices; (saponins); exemption from the requirement of a tolerance. (b) Tris (2-ethylhexyl) phosphate is used as an inert ingredient in pesticide Residues of the biochemical pesticide formulations with the active ingredi- Quillaja saponaria extract (saponins) ents pinoxaden, clodinafop-propargyl, are exempt from the requirement of a and tralkoxydium; tolerance in or on all food commod- (c) Tris (2-ethylhexyl) phosphate is ities. applied no more than twice per season; [72 FR 41935, Aug. 1, 2007] and

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§ 180.1280 § 180.1284 Ammonium salts of higher Poly(hexamethylenebiguanide) hy- fatty acids (C8-C18 saturated; C8-C12 drochloride (PHMB); exemption unsaturated); exemption from the from the requirement of a toler- requirement of a tolerance. ance. Ammonium salts of C8-C18 saturated Poly(hexamethylenebiguanide) hy- and C8-C12 unsaturated higher fatty drochloride (PHMB)(CAS Reg. No. acids are exempted from the require- 32289–58–0) is exempt from the requirement of a tolerance for residues in or ment of a tolerance for residues of the on all food commodities when used in antimicrobial in or on all food com- accordance with good agricultural modities when the residues are the re- practice. sult of the lawful application of a food [74 FR 47457, Sept. 16, 2009] contact surface sanitizer containing PHMB at 550 parts per million (ppm). § 180.1285 Polyoxin D zinc salt; exemption from the requirement of a tol- [73 FR 1517, Jan. 9, 2008] erance. An exemption from the requirement § 180.1281 S-Abscisic Acid, (S)-5-(1-hydroxy-2,6,6-trimethyl-4-oxo-1- of a tolerance is established for the res- cyclohex-2-enyl)-3-methyl-penta- idues of polyoxin D zinc salt in or on (2Z,4E)-dienoic Acid; exemption all food commodities when applied as a from the requirement of a toler- fungicide and used in accordance with ance. good agricultural practices. An exemption from the requirement [77 FR 56133, Sept. 12, 2012] of a tolerance is established for residues of S-Abscisic Acid in or on all food § 180.1287 Extract of Chenopodium commodities when applied or used ambrosioides near ambrosioides; exemption from the requirement of a preharvest as a plant regulator. tolerance. [75 FR 11744, Mar. 12, 2010] An exemption from the requirement of a tolerance is established for the res- § 180.1282 Bacillus firmus I-1582; ex- idues of Extract of Chenopodium emption from the requirement of a ambrosioides near ambrosioides when tolerance. used as an insecticide/acaricide on all An exemption from the requirement food commodities. of a tolerance is established in/on all [74 FR 634, Jan. 7, 2009] food/feed commodities, for residues of Bacillus firmus I-1582 when used as a soil § 180.1288 Tristyrylphenol ethoxylates; application or seed treatment. exemption from the requirement of a tolerance. [73 FR 25528, May 7, 2008] An exemption from the requirement § 180.1283 (Z)-7,8-epoxy-2- of a tolerance is established for resi- methyloctadecane (Disparlure); ex- dues of poly(oxy-1,2-ethanediyl), a- emption from the requirement of a [2,4,6-tris(1-phenylethyl)phenyl]-w-hy- tolerance. droxy-, (CAS Reg. No. 70559–25–0) and An exemption from the requirement poly(oxy-1,2-ethanediyl), a-[tris(1- of a tolerance is established for resi- phenylethyl)phenyl]-w-hydroxy-, (CAS dues of (Z)-7,8-epoxy-2- Reg. No. 99734–09–5) on citrus crops, group 10, when used as inert ingredi- methyloctadecane on all food and feed ents under the following conditions: crops that occur when it is used to (a) They are applied post-harvest; treat trees, shrubs, and pastures and (b) They are used as inert ingredients such use results in unintentional spray in pesticide formulations with and drift to non-target vegetation in- azoxystrobin and fludioxonil; and cluding non-food, food, and feed crops. (c) They constitute no more than This active ingredient is also known as 10.0% of the formulated pesticide prod- Disparlure. uct. [73 FR 33714, June 13, 2008] [74 FR 12625, Mar. 25, 2009]

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§ 180.1289 Candida oleophila Strain O; § 180.1294 Trichoderma asperellum exemption from the requirement of strain ICC 012; exemption from the a tolerance. requirement of a tolerance. An exemption from the requirement Trichoderma asperellum strain ICC 012 of a tolerance is established for the res- is exempted from the requirement of a idues of the microbial pesticide, tolerance in or on all food and feed Candida oleophila Strain O, on apples commodities when applied pre-harvest and pears when applied/used as a post- and used in accordance with good agri- harvest biofungicide. cultural practices. [74 FR 22464, May 13, 2009] [75 FR 9530, Mar. 3, 2010]

§ 180.1290 Pasteuria usgae; exemption § 180.1295 Laminarin; exemption from from the requirement of a toler- the requirement of a tolerance. ance. An exemption from the requirement An exemption from the requirement of a tolerance is established for resi- of a tolerance is established for residues of laminarin in or on all food com- dues of Pasteuria usgae in or on all food modities when laminarin is applied commodities when applied preharvest preharvest. and used as a nematicide in accordance with good agricultural practices. [75 FR 8256, Feb. 24, 2010]

[75 FR 37737, June 30, 2010] § 180.1296 Terpene Constituents α-terpinene, d-limonene and p-cymene, § 180.1291 Cold pressed neem oil; ex- of the Extract of Chenopodium emption from the requirement of a ambrosioides near ambrosioides as tolerance. Synthetically Manufactured; exemp- Residues of the biochemical pesticide tion from the requirement of a tol- cold pressed neem oil are exempt from erance. the requirement of a tolerance in or on An exemption from the requirement all food commodities. of a tolerance is established for the res- [74 FR 55463, Oct. 28, 2009] idues of the biochemical pesticide Ter- pene Constituents a-terpinene, d-limo- § 180.1292 Ulocladium oudemansii (U3 nene and p-cymene, of the Extract of Strain); exemption from the re- Chenopodium ambrosioides near quirement of a tolerance. ambrosioides as Synthetically Manufac- An exemption from the requirement tured when used as an insecticide/acar- of a tolerance is established in/on all icide in or on all food commodities. food commodities for residues of [75 FR 39455, July 9, 2010] Ulocladium oudemansii (U3 Strain), when applied or used pre-harvest-only, § 180.1297 Homobrassinolide; exemp- excluding applications made post-har- tion from the requirement of a tol- vest or to processed commodities, as a erance. microbial fungicide in accordance with An exemption from the requirement good agricultural practices. of a tolerance is established for the res- [74 FR 55458, Oct. 28, 2009] idues of homobrassinolide in or on all food commodities when applied/used as § 180.1293 Trichoderma gamsii strain a plant growth regulator in accordance ICC 080; exemption from the re- with good agricultural practices. quirement of a tolerance. [75 FR 39459, July 9, 2010] Trichoderma gamsii strain ICC 080 is exempted from the requirement of a § 180.1298 Trichoderma hamatum iso- tolerance in or on all food and feed late 382; exemption from the re- commodities when applied preharvest quirement of a tolerance. and used in accordance with good agri- An exemption from the requirement cultural practices. of a tolerance is established for resi- [75 FR 8507, Feb. 25, 2010] dues of Trichoderma hamatum isolate 382

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in or on all food commodities when ap- § 180.1303 Metarhizium anisopliae plied as a fungicide and used in accord- strain F52; exemption from the re- ance with good agricultural practices. quirement of a tolerance. [75 FR 43076, July 23, 2010] An exemption from the requirement of a tolerance is established for resi- § 180.1299 Prohydrojasmon; exemption dues of Metarhizium anisopliae strain from the requirement of a toler- F52 in or on all food commodities when ance. applied as an insecticide, miticide, or An exemption from the requirement ixodicide and used in accordance with of a tolerance is established for resi- good agricultural practices. dues of the biochemical pesticide [76 FR 26198, May 6, 2011] prohydrojasmon (PDJ), propyl-3-oxo-2- pentylcyclo-pentylacetate, when used § 180.1304 Pseudomonas fluorescens as a plant growth regulator in or on strain CL145A; exemption from the apple and grape pre-harvest, in accord- requirement of a tolerance. ance with label directions and good ag- An exemption from the requirement ricultural practices. of a tolerance is established for residues of Pseudomonas fluorescens strain [78 FR 75257, Dec. 11, 2013] CL145A in or on all food commodities § 180.1300 Potassium hypochlorite; ex- when applied as a molluscicide. emption from the requirement of a [76 FR 52875, Aug. 24, 2011] tolerance. An exemption from the requirement § 180.1305 Chromobacterium of a tolerance is established for resi- subtsugae strain PRAA4–1T; exemp- dues of potassium hypochlorite in or on tion from the requirement of a tolerance. all commodities. An exemption from the requirement [76 FR 11343, Mar. 2, 2011] of a tolerance is established for residues of Chromobacterium subtsugae § 180.1301 Escherichia coli O157:H7 T specific bacteriophages; temporary strain PRAA4–1 in or on all food com- exemption from the requirement of modities when applied as an insecticide a tolerance. or miticide and used in accordance with good agricultural practices. A temporary exemption from the requirement of a tolerance is established [76 FR 55272, Sept. 7, 2011] for residues of lytic bacteriophages that are specific to Escherichia coli § 180.1306 Isaria fumosorosea (for- O157:H7, sequence negative for shiga merly Paecilomyces fumosoroseus) Apopka strain 97; exemption from toxins I and II, and grown on the requirement of a tolerance. atoxigenic host bacteria when used/applied on food contact surfaces in food An exemption from the requirement processing plants in accordance with of a tolerance is established for resi- the terms of Experimental Use Permit dues of Isaria fumosorosea (formerly (EUP) No. 74234–EUP–2. This temporary Paecilomyces fumosoroseus) Apopka exemption expires on April 1, 2013. strain 97 in or on all food commodities when applied as an insecticide or [76 FR 20546, Apr. 13, 2011] miticide and used in accordance with good agricultural practices. § 180.1302 Sodium Ferric Ethylene- diaminetetraacetate (EDTA); ex- [76 FR 59905, Sept. 28, 2011] emption from the requirement of a tolerance. § 180.1307 Bacteriophage of Clavibacter michiganensis sub- An exemption from the requirement species michiganensis; exemption of a tolerance is established for resi- from the requirement of a toler- dues of sodium ferric EDTA in or on all ance. food commodities when applied as a An exemption from the requirement molluscicide and used in accordance of a tolerance is established for resi- with good agricultural practices. dues of lytic bacteriophage of [76 FR 17561, Mar. 30, 2011] Clavibacter michiganensis subspecies

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michiganensis produced in Clavibacter § 180.1312 Aureobasidium pullulans michiganensis subspecies strains DSM 14940 and DSM 14941; michiganensis in or on tomato when exemption from the requirement of applied as a bactericide in accordance a tolerance. with good agricultural practices. An exemption from the requirement of a tolerance is established for resi- [76 FR 66192, Oct. 26, 2011] dues of Aureobasidium pullulans strains DSM 14940 and DSM 14941 in or on all § 180.1308 Bacillus amyloliquefaciens food commodities when used in accord- strain D747; exemption from the re- ance with label directions and good ag- quirement of a tolerance. ricultural practices. An exemption from the requirement of a tolerance is established for resi- [80 FR 73662, Nov. 25, 2015] dues of the microbial pesticide, Bacillus § 180.1313 Bacillus pumilus strain amyloliquefaciens strain D747 in or on GHA 180; exemption from the re- all food commodities when used in ac- quirement of a tolerance. cordance with good agricultural prac- An exemption from the requirement tices. of a tolerance is established for resi- [77 FR 749, Jan. 6, 2012. Redesignated at 77 dues of Bacillus pumilus strain GHA 180 FR 2911, Jan. 20, 2012] in or on all food commodities when used in accordance with good agricul- § 180.1309 Bacillus subtilis strain CX– tural practices. 9060; exemption from the require- [77 FR 19112, Mar. 30, 2012] ment of a tolerance. An exemption from the requirement § 180.1314 Killed, nonviable of a tolerance is established for resi- Streptomyces acidiscabies strain RL–110T; exemption from the re- dues of the microbial pesticide Bacillus quirement of a tolerance. subtilis strain CX–9060, in or on all food An exemption from the requirement commodities, when applied or used in of a tolerance is established for resi- accordance with good agricultural dues of killed, nonviable Streptomyces practices. acidiscabies strain RL–110T in or on all [77 FR 1637, Jan. 11, 2012] food commodities when applied as a pre- or post-emergent herbicide and § 180.1310 Trichoderma virens strain used in accordance with good agricul- G–41; exemption from the require- tural practices. ment of a tolerance. [77 FR 35295, June 13, 2012] An exemption from the requirement of a tolerance is established for resi- § 180.1315 Natamycin; exemption from dues of Trichoderma virens strain G–41, the requirement of a tolerance. in or on all food commodities, when ap- An exemption from the requirement plied as a fungicide and used in accord- of a tolerance is established for the res- ance with good agricultural practices. idues of natamycin in or on mush- rooms, pineapples, citrus, pome, stone [77 FR 4908, Feb. 1, 2012] fruit crop groups, avocado, kiwi, mango, and pomegranates when used in § 180.1311 Pasteuria nishizawae—Pn1; accordance with label directions and exemption from the requirement of a tolerance. good agricultural practices. An exemption from the requirement [81 FR 58410, Aug. 25, 2016] of a tolerance is established for resi- § 180.1316 Pasteuria spp. dues of Pasteuria nishizawae—Pn1 in or (Rotylenchulus reniformis nema- on all food commodities when applied tode)—Pr3; exemption from the re- as a nematicide and used in accordance quirement of a tolerance. with good agricultural practices. An exemption from the requirement [77 FR 8741, Feb. 15, 2012] of a tolerance is established for residues of Pasteuria spp. (Rotylenchulus reniformis nematode)—Pr3 in or on all

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food commodities when applied as a § 180.1321 Complex Polymeric nematicide and used in accordance Polyhydroxy Acids; exemption from with label directions and good agricul- the requirement of a tolerance. tural practices. An exemption from the requirement [77 FR 40276, July 9, 2012] of a tolerance is established for the residues of complex polymeric § 180.1317 Pesticide chemicals; exemp- polyhydroxy acids in or on all food tion from the requirements of a tol- commodities when applied as a plant erance. growth regulator and used in accord- An exemption from the requirement ance with good agricultural practices. of a tolerance is established for resi- [78 FR 46267, July 31, 2013] dues of Didecyl dimethyl ammonium chloride in or on broccoli resulting § 180.1322 Bacillus pumilus strain BU from the use of Didecyl dimethyl am- F–33; exemption from the require- monium chloride as a seed treatment ment of a tolerance. at a treatment concentration of 1200 An exemption from the requirement ppm prior to planting by immersion. of a tolerance is established for resi- [77 FR 47296, Aug. 8, 2012] dues of Bacillus pumilus strain BU F–33 in or on all food commodities when ap- § 180.1318 3-decen-2-one; exemption plied to elicit induced systemic resist- from the requirement of a tolerance in plants and used in accordance ance. with label directions and good agricul- An exemption from the requirement tural practices. of a tolerance is established for resi- [78 FR 35149, June 12, 2013] dues of the biochemical pesticide, 3- decen-2-one, in or on potatoes when ap- § 180.1323 Ethyl-2E,4Z-decadienoate plied as a potato sprout inhibitor and (Pear Ester); exemption from the used in accordance with label direc- requirement of a tolerance. tions and good agricultural practices. An exemption from the requirement [78 FR 11766, Feb. 20, 2013] of a tolerance is established for residues of the biochemical pesticide, § 180.1319 Banda de Lupinus albus ethyl-2E,4Z-decadienoate (pear ester), doce (BLAD); exemption from the in or on all food commodities, when requirement of a tolerance. used in accordance with label direc- An exemption from the requirement tions and good agricultural practices. of a tolerance is established for the res- [78 FR 53054, Aug. 28, 2013] idues of Banda de Lupinus albus doce (BLAD), a naturally occurring § 180.1324 GS-omega/kappa-Hxtx-Hv1a; polypeptide from the catabolism of a exemption from the requirement of seed storage protein (b-conglutin) of a tolerance. sweet lupines (Lupinus albus), in or on An exemption from the requirement all food commodities when applied as a of a tolerance is established for resi- fungicide and used in accordance with label directions and good agricultural dues of the pesticide GS-omega/kappa- practices. Hxtx-Hv1a in or on all food commodities when applied or used in accord- [78 FR 17604, Mar. 22, 2013] ance with label directions and good agricultural practices. § 180.1320 Methyl jasmonate; exemption from the requirement of a tol- [79 FR 10685, Feb. 26, 2014] erance. § 180.1325 Heat-killed Burkholderia An exemption from the requirement spp. strain A396 cells and spent fer- of a tolerance is established for resi- mentation media exemption from dues of methyl jasmonate in or on all the requirement of a tolerance. food commodities when methyl An exemption from the requirement jasmonate is applied pre-harvest. of a tolerance is established for resi- [78 FR 22794, Apr. 17, 2013] dues of heat-killed Burkholderia spp.

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strain A396 cells and spent fermenta- § 180.1330 1-Octanol; exemption from tion media in or on all food commod- the requirement of a tolerance. ities when applied as a biological insec- An exemption from the requirement ticide to agricultural crops and used in of a tolerance is established for resi- accordance with label directions and dues of 1-octanol in or on root and good agricultural practices. tuber vegetables when applied as a [79 FR 15704, Mar. 21, 2014] plant growth regulator in accordance with label directions and good agricul- § 180.1326 Pseudomonas fluorescens tural practices. strain D7; exemption from the requirement of a tolerance. [80 FR 25953, May 6, 2015] An exemption from the requirement § 180.1331 Trichoderma asperelloides of a tolerance is established for resi- strain JM41R; exemption from the dues of Pseudomonas fluorescens strain requirement of a tolerance. D7 in or on all food commodities when An exemption from the requirement used in accordance with label direc- of a tolerance is established for resi- tions and good agricultural practices. dues of Trichoderma asperelloides strain [79 FR 60750, Oct. 8, 2014] JM41R in or on all food commodities when used in accordance with label di- § 180.1327 Tetraacetylethylenediamine rections and good agricultural prac- (TAED) and its metabolite tices. Diacetylethylenediamine (DAED); exemption from the requirement of [80 FR 28203, May 18, 2015] a tolerance. § 180.1332 Lavandulyl senecioate; ex- An exemption from the requirement emption from the requirement of a of a tolerance is established for resi- tolerance. dues of the pesticide, tetraacetylethylenediamine (TAED), An exemption from the requirement and its metabolite of a tolerance is established for resi- diacetylethylenediamine (DAED), in or dues of the arthropod pheromone, on rice and strawberries, when used as lavandulyl senecioate (5-methyl-2-(1- a fungicide and bactericide in accord- methylethenyl)-4-hexenyl 3-methyl-2- ance with label directions and good ag- butonate), in or on all raw agricultural commodities when applied or used in ricultural practices. microbeads/dispensers at a rate not to [79 FR 59121, Oct. 1, 2014] exceed 150 grams active ingredient/ acre/year in accordance with good agri- § 180.1328 Beauveria bassiana strain cultural practices. ANT–03; exemption from the requirement of a tolerance. [80 FR 49171, Aug. 17, 2015] An exemption from the requirement § 180.1333 Potassium Salts of Hops of a tolerance is established for resi- Beta acids; exemption from the re- dues of Beauveria bassiana strain ANT– quirement of a tolerance. 03 in or on all food commodities, when An exemption from the requirement applied as a microbial insecticide and of a tolerance is established for resi- used in accordance with label direc- dues of the biochemical potassium tions and good agricultural practices. salts of hops beta acids in or on honey [79 FR 77396, Dec. 24, 2014] and honeycomb, when used for the control of Varroa mites in accordance with § 180.1329 Bacillus subtilis strain IAB/ label directions and good agricultural BS03, exemption from the require- practices. ment of a tolerance. An exemption from the requirement [80 FR 63683, Oct. 21, 2015] of a tolerance is established for resi- § 180.1334 Choline Chloride; Exemp- dues of Bacillus subtilis strain IAB/BS03 tion from the Requirement of a Tol- in or on all food commodities when erance. used in accordance with label direc- An exemption from the requirement tions and good agricultural practices. of a tolerance is established for resi- [80 FR 9217, Feb. 20, 2015] dues of Choline Chloride in or on all

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food commodities when Choline Chlo- Permit No. 91163–EUP–1. These tem- ride is applied pre-harvest and used in porary exemptions from the require- accordance with label directions and ment of a tolerance expire on June 30, good agricultural practices. 2020. [80 FR 78149, Dec. 16, 2015] [81 FR 63710, Sept. 16, 2016]

§ 180.1335 Isaria fumosorosea strain § 180.1339 Spodoptera frugiperda mul- FE 9901; exemption from the re- tiple nucleopolyhedrovirus strain quirement of a tolerance. 3AP2; exemption from the require- An exemption from the requirement ment of a tolerance. of a tolerance is established for resi- An exemption from the requirement dues of Isaria fumosorosea strain FE of a tolerance is established for resi- 9901 in or on all food commodities when dues of Spodoptera frugiperda multiple used in accordance with label direc- nucleopolyhedrovirus strain 3AP2 in or tions and good agricultural practices. on all food commodities when used in [81 FR 47311, July 21, 2016] accordance with label directions and good agricultural practices. § 180.1336 Bacillus amyloliquefaciens strain PTA–4838; exemption from [81 FR 83706, Nov. 22, 2016] the requirement of a tolerance. An exemption from the requirement § 180.1340 Muscodor albus strain SA– 13 and the volatiles produced on re- of a tolerance is established for resi- hydration; exemption from the re- dues of Bacillus amyloliquefaciens strain quirement of a tolerance. PTA–4838 in or on all food commodities. An exemption from the requirement of a tolerance is established for resi- [81 FR 41222, June 24, 2016] dues of Muscodor albus strain SA–13 and the volatiles produced on rehydration § 180.1337 Citrus tristeza virus expressing spinach defensin proteins in or on all food commodities when 2, 7, and 8; exemption from the re- used in accordance with label direc- quirement of a tolerance. tions and good agricultural practices. A temporary exemption from the re- [81 FR 86581, Dec. 1, 2016] quirement of a tolerance is established for residues of the microbial pesticide § 180.1341 Pseudomonas chlororaphis Citrus tristeza virus expressing spinach strain AFS009; exemption from the defensin proteins 2, 7, and 8 (either requirement of a tolerance. alone or in combinations with each An exemption from the requirement other) in or on the commodities listed of a tolerance is established for resi- in fruit, citrus group 10–10, when used dues of Pseudomonas chlororaphis strain in accordance with the terms of Experi- AFS009 in or on all food commodities mental Use Permit No. 88232–EUP–2. when used in accordance with label di- This temporary exemption from the re- rections and good agricultural prac- quirement of a tolerance expires on Au- tices. gust 31, 2020. [82 FR 35122, July 28, 2017] [81 FR 59502, Aug. 30, 2016]

§ 180.1338 Aspergillus flavus strains § 180.1344 Cyclaniliprole; exemption TC16F, TC35C, TC38B, and TC46G; from the requirement of a toler- temporary exemptions from the re- ance. quirement of a tolerance. An exemption from the requirement Temporary exemptions from the re- of a tolerance is established for indi- quirement of a tolerance are estab- rect and inadvertent residues of the in- lished for residues of Aspergillus flavus secticide cyclaniliprole, including its strains TC16F, TC35C, TC38B, and metabolites and degradates, in or on TC46G in or on the food and feed com- all raw agricultural commodities not modities of corn, field; corn, pop; and listed in paragraph (a) of § 180.694, when corn, sweet when used in accordance residues are present therein as a result with the terms of Experimental Use of subsequent uptake by crops rotated

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into fields where the crops in § 180.694 when used in accordance with label di- (a) were treated with cyclaniliprole. rections and good agricultural prac- [82 FR 36095, Aug. 3, 2017] tices. [83 FR 17498, Apr. 20, 2018] § 180.1345 1-Triacontanol; exemption from the requirement of a tolerance. § 180.1351 Bacillus subtilis strain FMCH002; exemption from the re- Residues of the biochemical pesticide quirement of a tolerance. 1-Triacontanol are exempt from the requirement of a tolerance in or on all An exemption from the requirement food commodities. of a tolerance is established for residues of Bacillus subtilis strain FMCH002 [82 FR 38852, Aug. 16, 2017] in or on all food commodities when used in accordance with label direc- § 180.1346 1,3-Dibromo-5,5- Dimethylhydantoin; exemption tions and good agricultural practices. from the requirement of a toler- [83 FR 17500, Apr. 20, 2018] ance. Residues of 1,3-dibromo-5,5- § 180.1352 Methyl-alpha-D- dimethylhydantoin, including its me- mannopyranoside (Alpha methyl tabolites and degradates, resulting mannoside); exemption from the re- from the use of 1,3-dibromo-5,5- quirement of a tolerance. dimethylhydantoin in antimicrobial Residues of the biochemical pesticide treatment solutions of raw agricultural Methyl-alpha-D-mannopyranoside commodities in treatment facilities are (alpha methyl mannoside) are exempt exempt from the requirement of a tol- from the requirement of a tolerance in erance. or on all raw agricultural commodities. [82 FR 57370, Dec. 5, 2017] [83 FR 7619, Feb. 22, 2018] § 180.1347 Bacillus amyloliquefaciens strain F727; exemption from the re- § 180.1353 Lipochitooligosaccharide quirement of a tolerance. (LCO) SP104; exemption from the An exemption from the requirement requirement of a tolerance. of a tolerance is established for resi- Residues of the biochemical pesticide dues of Bacillus amyloliquefaciens strain Lipochitooligosaccharide (LCO) SP104 F727 in or on all food commodities (which has been used in accordance when used in accordance with label di- with label directions and good agricul- rections and good agricultural prac- tural practices) are exempt from the tices. requirement of a tolerance in or on all [82 FR 49747, Oct. 27, 2017] food commodities.

§ 180.1348 Bacillus subtilis strain [83 FR 9442, Mar. 6, 2018] BU1814; exemption from the requirement of a tolerance. § 180.1354 Flutianil; exemption from the requirement of a tolerance. An exemption from the requirement of a tolerance is established for resi- An exemption from the requirement dues of Bacillus subtilis strain BU1814 in of a tolerance is established for indi- or on all food commodities when used rect and inadvertent residues of the in accordance with label directions and fungicide flutianil, including its me- good agricultural practices. tabolites and degradates, in or on all food commodities not listed in [82 FR 57873, Dec. 8, 2017] § 180.697(a), when residues are present § 180.1350 Bacillus licheniformis strain therein as a result of uptake by crops FMCH001; exemption from the re- rotated into fields containing the crops quirement of a tolerance. in § 180.697(a) that were previously An exemption from the requirement treated with flutianil. of a tolerance is established for resi- [83 FR 12269, Mar. 21, 2018] dues of Bacillus licheniformis strain FMCH001 in or on all food commodities

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§ 180.1355 Duddingtonia flagrans § 180.1359 Bacteriophage active strain IAH 1297; exemption from against Erwinia amylovora; exemp- the requirement of a tolerance. tion from the requirement of a tol- An exemption from the requirement erance. of a tolerance is established for resi- An exemption from the requirement dues of Duddingtonia flagrans strain of a tolerance is established for resi- IAH 1297 in or on all food commodities dues of lytic bacteriophage active when used in accordance with label di- against Erwinia amylovora that are pro- rections and good agricultural prac- duced in Erwinia amylovora in or on tices. apple and pear, when used in accordance with label directions and good ag- [83 FR 19972, May 7, 2018] ricultural practices. § 180.1356 Extract of Swinglea glutinosa; [83 FR 46403, Sept. 13, 2018] exemption from the requirement of a tolerance. § 180.1360 Bacteriophage active Residues of the biochemical pesticide against Xanthomonas citri subsp. Extract of Swinglea glutinosa are ex- citri; exemption from the requirement of a tolerance. empt from the requirement of a tolerance in or on all food commodities An exemption from the requirement when applied pre-harvest in accordance of a tolerance is established for resi- with label directions and good agricul- dues of lytic bacteriophage active tural practices. against Xanthomonas citri subsp. citri that are produced in Xanthomonas citri [83 FR 27713, June 14, 2018] subsp. citri in or on food commodities included in the fruit, citrus groups 10 § 180.1357 Cerevisane (cell walls of Saccharomyces cerevisiae strain and 10–10, when used in accordance LAS117); exemption from the re- with label directions and good agricul- quirement of a tolerance. tural practices. Residues of the biochemical pesticide [83 FR 46405, Sept. 13, 2018] cerevisane (cell walls of Saccharomyces cerevisiae strain LAS117) are exempt § 180.1361 Pepino mosaic virus, strain from the requirement of a tolerance in CH2, isolate 1906; exemption from or on all food commodities, when used the requirement of a tolerance. in accordance with label directions and Residues of Pepino mosaic virus, strain good agricultural practices. CH2, isolate 1906 are exempt from the requirement of a tolerance in or on to- [83 FR 39375, Aug. 9, 2018] mato when this pesticide chemical is § 180.1358 Metschnikowia fructicola used in accordance with label direc- strain NRRL Y–27328; exemption tions and good agricultural practices. from the requirement of a toler- [83 FR 46407, Sept. 13, 2018] ance. Residues of Metschnikowia fructicola § 180.1362 Beauveria bassiana strain strain NRRL Y–27328 are exempt from PPRI 5339; exemption from the re- the requirement of a tolerance in or on quirement of a tolerance. the food commodities included in the Residues of Beauveria bassiana strain following crop groups and subgroups PPRI 5339 are exempt from the require- when this pesticide chemical is used in ment of a tolerance in or on all food accordance with label directions and commodities when this pesticide chem- good agricultural practices: Fruit, ical is used in accordance with label di- stone group 12–12; Fruit, small fruit rections and good agricultural prac- vine climbing, except fuzzy kiwifruit, tices. subgroup 13–07F; and Berry, low grow- [83 FR 47076, Sept. 18, 2018] ing subgroup 13–07G. [83 FR 46117, Sept. 12, 2018]

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§ 180.1363 Bacillus amyloliquefaciens all food commodities when used in ac- strain ENV503; exemption from the cordance with label directions and good requirement of a tolerance. agricultural practices. An exemption from the requirement [84 FR 28237, June 18, 2019] of a tolerance is established for residues of Bacillus amyloliquefaciens strain § 180.1368 Clonostachys rosea strain ENV503 in or on all food commodities CR–7; exemption from the require- when used in accordance with label di- ment of a tolerance. rections and good agricultural practices. An exemption from the requirement of a tolerance is established for resi- [83 FR 58508, Nov. 20, 2018] dues of Clonostachys rosea strain CR–7 § 180.1364 Chlorate; exemption from in or on all food commodities when the requirement of a tolerance. used in accordance with label directions and good agricultural practices. Residues of chlorate in or on tomato and cantaloupe are exempt from the re- [84 FR 40271, Aug. 14, 2019] quirement of a tolerance when resulting from the application of gaseous § 180.1369 Autographa californica mul- chlorine dioxide as a fungicide, tiple nucleopolyhedrovirus strain bactericide, and antimicrobial pes- FV#11; exemption from the require- ticide. ment of a tolerance. [83 FR 66143, Dec. 26, 2018] An exemption from the requirement of a tolerance is established for resi- § 180.1365 Bacteriophage active dues of Autographa californica multiple against Xylella fastidiosa; exemption nucleopolyhedrovirus strain FV#11 in from the requirement of a toler- or on all food commodities when used ance. in accordance with label directions and An exemption from the requirement good agricultural practices. of a tolerance is established for residues of lytic bacteriophage active [84 FR 38562, Aug. 7, 2019] against Xylella fastidiosa in or on all food commodities when the § 180.1370 Lipochitoolgiosaccharide bacteriophage are sequenced and have (LCO) MOR116; exemption from the sequences free of toxins and lysogenic requirement of a tolerance. genes and are used in accordance with Residues of the plant growth regu- label directions and good agricultural lator Lipochitoolgiosaccharide (LCO) practices. MOR116 in or on all food commodities [84 FR 16791, Apr. 23, 2019] are exempt from the requirement of a tolerance, when used in accordance § 180.1366 24-Epibrassinolide; exemp- with label directions and good agricul- tion from the requirement of a tol- tural practices. erance. Residues of the plant growth regu- [84 FR 43705, Aug. 22, 2019] lator 24-epibrassinolide in or on all § 180.1371 Florpyrauxifen-benzyl; ex- food commodities are exempt from the emption from the requirement of a requirement of a tolerance, when used tolerance. in accordance with label directions and good agricultural practices. An exemption from the requirement of a tolerance is established for resi- [84 FR 27968, June 17, 2019] dues of florpyrauxifen-benzyl, includ- § 180.1367 Bacillus amyloliquefaciens ing its metabolites and degradates, in subspecies plantarum strain FZB42; or on all food and feed commodities, exemption from the requirement of when it is applied as an herbicide in ac- a tolerance. cordance with good agricultural prac- An exemption from the requirement tices. of a tolerance is established for resi- [84 FR 50766, Sept. 26, 2019] dues of Bacillus amyloliquefaciens subspecies plantarum strain FZB42 in or on 830

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§ 180.1372 Sodium lauryl sulfate; ex- § 180.1376 Ea peptide 91398; exemption emption from the requirement of a from the requirement of a toler- tolerance. ance. Residues of the fungicide and An exemption from the requirement miticide sodium lauryl sulfate (CAS of a tolerance is established for resi- No. 151–21–3) in or on all food commod- dues of Ea peptide 91398 in or on all ities are exempt from the requirement food commodities when used in accord- of a tolerance, when used in accordance ance with label directions and good ag- with label directions and good agricul- ricultural practices. tural practices. [85 FR 34361, June 4, 2020] [84 FR 52372, Oct. 2, 2019]

§ 180.1373 Chrysodeixis includens Subpart E—Pesticide Chemicals nucleopolyhedrovirus isolate #460; Not Requiring a Tolerance or exemption from the requirement of an Exemption From a Toler- a tolerance. ance Residues of Chrysodeixis includens nucleopolyhedrovirus isolate #460 are exempt from the requirement of a tol- SOURCE: 66 FR 66772, Dec. 27, 2001, unless otherwise noted. erance in or on all food commodities, when used in accordance with label di- § 180.2000 Scope. rections and good agricultural practices. This subpart sets forth the pesticide chemicals for use in agricultural or [85 FR 13548, Mar. 9, 2020] other food-related settings for which § 180.1374 Autographa californica mul- neither a tolerance nor an exemption is tiple nucleopolyhedrovirus strain deemed to be needed by EPA. R3; exemption from the requirement of a tolerance. § 180.2003 Definitions. Residues of Autographa californica (a) Food uses are the uses of a pes- multiple nucleopolyhedrovirus strain ticide chemical that are likely to yield R3 are exempt from the requirement of residues in food or feed crops, meat, a tolerance in or on all food commod- milk, poultry or egg. ities when used in accordance with (b) Non-food uses are those uses that label directions and good agricultural are not likely to yield residues in food practices. or feed crops, meat, milk, poultry or [85 FR 20187, Apr. 10, 2020] egg. [66 FR 66772, Dec. 27, 2001, as amended at 73 § 180.1375 Methyl mercaptan; exemp- FR 60158, Oct. 10, 2008] tion from the requirement of a tolerance. § 180.2010 [Reserved] Residues of methyl mercaptan are exempt from the requirement of a toler- § 180.2020 Non-food determinations. ance in or on all food commodities, The following pesticide chemical uses when methyl mercaptan is used as a do not need a tolerance or exemption gopher repellent in irrigation lines in from the requirement of a tolerance accordance with label directions and based on EPA’s determination that good agricultural practices. they are not likely to result in residues [85 FR 29633, May 18, 2020] in or on food.

Pesticide Chemical CAS Reg. No. Limits Uses

Methyl bromide 74–83–9 When applied as a pre-plant soil fumigant All pre-plant soil uses Potassium 12298–68–9 When applied to growing crops in foreign countries Bananas, grapes, triiodide (KI3) and melons Rhodamine B 81–88–9 Not to exceed 2% by weight of the formulated product and 60 ppm on Dye for seed treat- the treated seed ment

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[66 FR 66772, Dec. 27, 2001, as amended at 70 FR 40201, July 13, 2005; 71 FR 45402, Aug. 9, 2006]

PARTS 181–189 [RESERVED]

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