422 Part 180—Tolerances and Ex- Emptions for Pesticide

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Pt. 180 40 CFR Ch. I (7–1–16 Edition)

at any time before the filing of the ini- 180.124 Methyl bromide; tolerances for resi- tial decision. dues. 180.127 Piperonyl butoxide; tolerances for [55 FR 50293, Dec. 5, 1990, as amended at 70 residues. FR 33360, June 8, 2005] 180.128 Pyrethrins; tolerances for residues. 180.129 o-Phenylphenol and its sodium salt; PART 180—TOLERANCES AND EX- tolerances for residues. 180.130 Hydrogen Cyanide; tolerances for EMPTIONS FOR PESTICIDE CHEM- residues. ICAL RESIDUES IN FOOD 180.132 Thiram; tolerances for residues. 180.142 2,4-D; tolerances for residues. Subpart A—Definitions and Interpretative 180.145 Fluorine compounds; tolerances for Regulations residues. 180.151 Ethylene oxide; tolerances for resi- Sec. dues. 180.1 Definitions and interpretations. 180.153 Diazinon; tolerances for residues. 180.3 Tolerances for related pesticide chemi- 180.154 Azinphos-methyl; tolerances for resi- cals. dues. 180.4 Exceptions. 180.155 1-Naphthaleneacetic acid; tolerances 180.5 Zero tolerances. for residues. 180.6 Pesticide tolerances regarding milk, 180.163 Dicofol; tolerances for residues. eggs, meat, and/or poultry; statement of 180.169 Carbaryl; tolerances for residues. policy. 180.172 Dodine; tolerances for residues. 180.175 Maleic hydrazide; tolerances for resi- Subpart B—Procedural Regulations dues. 180.176 Mancozeb; tolerances for residues. 180.7 Petitions proposing tolerances or ex- 180.178 Ethoxyquin; tolerances for residues. emptions for pesticide residues in or on 180.181 Chlorpropham; tolerances for resi- raw agricultural commodities or proc- dues. essed foods. 180.182 Endosulfan; tolerances for residues. 180.8 Withdrawal of petitions without preju- 180.183 Disulfoton; tolerances for residues. dice. 180.184 Linuron; tolerances for residues. 180.9 Substantive amendments to petitions. 180.185 DCPA; tolerances for residues. 180.29 Establishment, modification, and rev- 180.189 Coumaphos; tolerances for residues. ocation of tolerance on initiative of Ad- 180.190 Diphenylamine; tolerances for resi- ministrator. dues. 180.30 Judicial review. 180.191 Folpet; tolerances for residues. 180.31 Temporary tolerances. 180.198 Trichlorfon; tolerances for residues. 180.32 Procedure for modifying and revoking 180.200 Dicloran; tolerances for residues. tolerances or exemptions from toler- 180.202 p-Chlorophenoxyacetic acid; tolerances. ances for residues. 180.33 Fees. 180.204 Dimethoate; tolerances for residues. 180.34 Tests on the amount of residue re- 180.205 Paraquat; tolerances for residues. maining. 180.35 Tests for potentiation. 180.206 Phorate; tolerances for residues. 180.40 Tolerances for crop groups. 180.207 Trifluralin; tolerances for residues. 180.41 Crop group tables. 180.208 Benfluralin; tolerances for residues. 180.209 Terbacil; tolerances for residues. Subpart C—Specific Tolerances 180.210 Bromacil; tolerances for residues. 180.211 Propachlor; tolerances for residues. 180.101 Specific tolerances; general provi- 180.212 S-Ethyl cyclohexylethylthiocarba- sions. mate; tolerances for residues. 180.103 Captan; tolerances for residues. 180.213 Simazine; tolerances for residues. 180.106 Diuron; tolerances for residues. 180.215 Naled; tolerances for residues. 180.108 Acephate; tolerances for residues. 180.217 Metiram; tolerances for residues. 180.111 Malathion; tolerances for residues. 180.220 Atrazine; tolerances for residues. 180.114 Ferbam; tolerances for residues. 180.222 Prometryn; tolerances for residues. 180.116 Ziram; tolerances for residues. 180.225 Phosphine; tolerances for residues. 180.117 S-Ethyl dipropylthiocarbamate; tol- 180.226 Diquat; tolerances for residues. erances for residues. 180.227 Dicamba; tolerances for residues. 180.121 Methyl parathion; tolerances for res- 180.229 Fluometuron; tolerances for resi- idues. dues. 180.123 Inorganic bromide residues resulting 180.231 Dichlobenil; tolerances for residues. from fumigation with methyl bromide; 180.232 Butylate; tolerances for residues. tolerances for residues. 180.235 Dichlorvos; tolerances for residues. 180.123a Inorganic bromide residues in pea- 180.236 Triphenyltin hydroxide; tolerances nut hay and peanut hulls; statement of for residues. policy. 180.241 Bensulide; tolerances for residues.

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180.242 Thiabendazole; tolerances for resi- 180.339 MCPA; tolerances for residues. dues. 180.341 2,4-Dinitro-6-octylphenyl crotonate 180.243 Propazine; tolerances for residues. and 2,6-dinitro-4-octylphenyl crotonate; 180.245 Streptomycin; tolerances for resi- tolerances for residues. dues. 180.342 Chlorpyrifos; tolerances for residues. 180.249 Alachlor; tolerances for residues. 180.345 Ethofumesate; tolerances for resi- 180.252 Tetrachlorvinphos; tolerances for dues. residues. 180.349 Fenamiphos; tolerances for residues. 180.253 Methomyl; tolerances for residues. 180.350 Nitrapyrin; tolerances for residues. 180.254 Carbofuran; tolerances for residues. 180.352 Terbufos; tolerances for residues. 180.257 Chloroneb; tolerances for residues. 180.353 Desmedipham; tolerances for resi- 180.258 Ametryn; tolerances for residues. dues. 180.259 Propargite; tolerances for residues. 180.355 Bentazon; tolerances for residues. 180.261 Phosmet; tolerances for residues. 180.356 Norflurazon; tolerances for residues. 180.262 Ethoprop; tolerances for residues. 180.360 Asulam; tolerance for residues. 180.263 Phosalone; tolerances for residues. 180.361 Pendimethalin; tolerances for resi- 180.269 Aldicarb; tolerances for residues. dues. 180.272 Tribuphos; tolerances for residues. 180.362 Fenbutatin-oxide; tolerances for res- 180.274 Propanil; tolerances for residues. idues. 180.275 Chlorothalonil; tolerances for resi- 180.364 Glyphosate; tolerances for residues. dues. 180.367 n-Octyl bicycloheptenedicarbox- 180.276 Formetanate hydrochloride; toler- imide; tolerances for residues. ances for residues. 180.368 Metolachlor; tolerances for residues. 180.278 Phenmedipham; tolerances for resi- 180.370 5-Ethoxy-3-(trichloromethyl)-1, 2, 4- dues. thiadiazole; tolerances for residues. 180.284 Zinc phosphide; tolerances for resi- 180.371 Thiophanate-methyl; tolerances for dues. residues. 180.287 Amitraz; tolerances for residues. 180.372 2,6-Dimethyl-4-tridecylmorpholine; 180.288 2-(Thiocyanomethylthio) tolerances for residues. benzothiazole; tolerances for residues. 180.373 [Reserved] 180.289 Methanearsonic acid; tolerances for 180.377 Diflubenzuron; tolerances for resi- residues. dues. 180.291 Pentachloronitrobenzene; tolerance 180.378 Permethrin; tolerances for residues. for residues. 180.380 Vinclozolin; tolerances for residues. 180.292 Picloram; tolerances for residues. 180.381 Oxyfluorfen; tolerances for residues. 180.293 Endothall; tolerances for residues. 180.383 Sodium salt of acifluorfen; toler- 180.297 N-1-Naphthyl phthalamic acid; tolerances for residues. ances for residues. 180.384 Mepiquat (N,N-dimethylpiperidin- 180.298 Methidathion; tolerances for resi- ium); tolerances for residues. dues. 180.385 Diclofop-methyl; tolerances for resi- 180.299 Dicrotophos; tolerances for residues. dues. 180.300 Ethephon; tolerances for residues. 180.388–180.389 [Reserved] 180.301 Carboxin; tolerances for residues. 180.390 Tebuthiuron; tolerances for residues. 180.303 Oxamyl; tolerances for residues. 180.395 Hydramethylnon; tolerances for resi- 180.304 Oryzalin; tolerances for residues. dues. 180.311 Cacodylic acid; tolerances for resi- 180.396 Hexazinone; tolerances for residues. dues. 180.399 Iprodione; tolerances for residues. 180.314 Triallate; tolerances for residues. 180.401 Thiobencarb; tolerances for residues. 180.315 Methamidophos; tolerances for resi- 180.403 Thidiazuron; tolerances for residues. dues. 180.404 Profenofos; tolerances for residues. 180.316 Pyrazon; tolerances for residues. 180.405 Chlorsulfuron; tolerances for resi- 180.317 Propyzamide; tolerances for residues. dues. 180.407 Thiodicarb; tolerances for residues. 180.318 4-(2-Methyl-4-chlorophenoxy) bu- 180.408 Metalaxyl; tolerances for residues. tyric acid; tolerance for residues. 180.409 Pirimiphos-methyl; tolerances for 180.319 Interim tolerances. residues. 180.324 Bromoxynil; tolerances for residues. 180.410 Triadimefon; tolerances for residues. 180.328 Napropamide; tolerances for resi- 180.411 Fluazifop-P-butyl; tolerances for res- dues. idues. 180.330 S-(2-(Ethylsulfinyl)ethyl) O,O-di- 180.412 Sethoxydim; tolerances for residues. methyl phosphorothioate; tolerances for 180.413 Imazalil; tolerances for residues. residues. 180.414 Cyromazine; tolerances for residues. 180.331 4-(2,4-Dichlorophenoxy) butyric acid; 180.415 Aluminum tris (O-ethylphospho- tolerances for residues. nate); tolerances for residues. 180.332 Metribuzin; tolerances for residues. 180.416 Ethalfluralin; tolerances for resi- 180.337 Oxytetracycline; tolerances for residues. dues. 180.417 Triclopyr; tolerances for residues.

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180.418 Cypermethrin and isomers alpha- 180.457 Bitertanol; tolerances for residues. cypermethrin and zeta-cypermethrin; 180.458 Clethodim; tolerances for residues. tolerances for residues. 180.459 Triasulfuron; tolerances for residues. 180.419 Chlorpyrifos-methyl; tolerances for 180.460 Benoxacor; tolerances for residues. residues. 180.461 Cadusafos; tolerances for residues. 180.420 Fluridone; tolerances for residues. 180.462 Pyridate; tolerances for residues. 180.421 Fenarimol; tolerances for residues. 180.463 Quinclorac; tolerances for residues. 180.422 Tralomethrin; tolerances for resi- 180.464 Dimethenamid; tolerances for residues. dues. 180.425 Clomazone; tolerances for residues. 180.465 4-(Dichloroacetyl)-1-oxa-4- 180.426 2-[4,5-Dihydro-4-methyl-4-(1- azaspiro[4.5]decane. methylethyl)-5-oxo-1H-imidazol-2-yl]-3- 180.466 Fenpropathrin; tolerances for resi- quinoline carboxylic acid; tolerance for dues. residues. 180.467 Carbon disulfide; tolerances for resi- 180.427 Tau-Fluvalinate; tolerances for residues. dues. 180.468 Flumetsulam; tolerances for resi- 180.428 Metsulfuron methyl; tolerances for dues. residues. 180.469 Dichlormid; tolerances for residues. 180.429 Chlorimuron ethyl; tolerances for 180.470 Acetochlor; tolerances for residues. residues. 180.471 Furilazole; tolerances for residues. 180.430 Fenoxaprop-ethyl; tolerances for res- 180.472 Imidacloprid; tolerances for resi- idues. dues. 180.431 Clopyralid; tolerances for residues. 180.473 Glufosinate ammonium; tolerances 180.432 Lactofen; tolerances for residues. for residues. 180.433 Fomesafen; tolerances for residues. 180.474 Tebuconazole; tolerances for resi- 180.434 Propiconazole; tolerances for residues. dues. 180.475 Difenoconazole; tolerances for resi- 180.435 Deltamethrin; tolerances for residues. dues. 180.476 Triflumizole; tolerances for residues. 180.436 Cyfluthrin and the isomer beta- 180.477 Flumiclorac pentyl; tolerances for cyfluthrin; tolerances for residues. residues. 180.437 Methyl 2-(4-isopropyl-4-methyl-5- 180.478 Rimsulfuron; tolerances for residues. oxo-2-imidazolin-2-yl)-p-toluate and 180.479 Halosulfuron-methyl; tolerances for methyl 6-(4-isopropyl-4-methyl-5-oxo-2- residues. imidazolin-2-yl)-m-toluate; tolerances for 180.480 Fenbuconazole; tolerances for resi- residues. dues. 180.438 Lambda-cyhalothrin and an isomer 180.481 Prosulfuron; tolerances for residues. gamma-cyhalothrin; tolerances for resi- 180.482 Tebufenozide; tolerances for residues. dues. 180.439 Thifensulfuron methyl; tolerances 180.484 Flutolanil; tolerances for residues. for residues. 180.485 Cyproconazole; tolerances for resi- 180.440 Tefluthrin; tolerances for residues. dues. 180.441 Quizalofop ethyl; tolerances for resi- 180.486 Chlorethoxyfos; tolerances for residues. dues. 180.442 Bifenthrin; tolerances for residues. 180.487 Pyrithiobac sodium; tolerances for 180.443 Myclobutanil; tolerances for resi- residues. dues. 180.490 Imazapic; tolerances for residues. 180.444 Sulfur dioxide; tolerances for resi- 180.491 Propylene oxide; tolerances for residues. dues. 180.445 Bensulfuron methyl; tolerances for 180.492 Triflusulfuron-methyl; tolerances residues. for residues. 180.446 Clofentezine; tolerances for residues. 180.493 Dimethomorph; tolerances for resi- 180.447 Imazethapyr; tolerances for residues. dues. 180.448 Hexythiazox; tolerance for residues. 180.494 Pyridaben; tolerance for residues. 180.449 Avermectin B1 and its delta-8,9-iso- 180.495 Spinosad; tolerances for residues. mer; tolerances for residues. 180.496 Thiazopyr; tolerances for residues. 180.450 Beta-(4-Chlorophenoxy)-alpha-(1,1- 180.497 Clofencet; tolerances for residues. dimethylethyl)-1H-1,2,4-triazole-1-eth- 180.498 Sulfentrazone; tolerances for resi- anol; tolerances for residues. dues. 180.451 Tribenuron methyl; tolerances for 180.499 Propamocarb; tolerances for resi- residues. dues. 180.452 Primisulfuron-methyl; tolerances for 180.500 Imazapyr; tolerances for residues. residues. 180.501 Hydroprene; tolerances for residues. 180.454 Nicosulfuron; tolerances for resi- 180.502 Aminoethoxyvinylglycine hydro- dues. chloride (aviglycine HCl); tolerances for 180.455 Procymidone; tolerances for resi- residues. dues. 180.503 Cymoxanil, tolerance for residues.

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180.504 [Reserved] 180.554 Kresoxim-methyl; tolerances for res- 180.505 Emamectin; tolerances for residues. idues. 180.506 Cyclanilide; tolerances for residues. 180.555 Trifloxystrobin; tolerances for resi- 180.507 Azoxystrobin; tolerances for residues. dues. 180.556 Pymetrozine; tolerances for resi- 180.509 Mefenpyr-diethyl; tolerance for residues. dues. 180.557 Tetraconazole; tolerances for resi- 180.510 Pyriproxyfen; tolerances for residues. dues. 180.559 Clodinafop-propargyl; tolerances for 180.511 Buprofezin; tolerances for residues. residues. 180.512 [Reserved] 180.560 Cloquintocet-mexyl; tolerances for 180.513 Chlorfenapyr; tolerances for resi- residues. dues. 180.561 Acibenzolar-S-methyl; tolerances for 180.514 Cloransulam-methyl; tolerances for residues. residues. 180.562 Flucarbazone-sodium; tolerances for 180.515 Carfentrazone-ethyl; tolerances for residues. residues. 180.563 Ethametsulfuron-methyl; tolerances 180.516 Fludioxonil; tolerances for residues. for residues. 180.517 Fipronil; tolerances for residues. 180.564 Indoxacarb; tolerances for residues. 180.518 Pyrimethanil; tolerances for resi- 180.565 Thiamethoxam; tolerances for residues. dues. 180.519 Bromide ion and residual bromine; 180.566 Fenpyroximate; tolerances for resi- tolerances for residues. dues. 180.521 Fumigants for grain-mill machinery; 180.567 Zoxamide; tolerances for residues. tolerances for residues. 180.568 Flumioxazin; tolerances for residues. 180.522 Fumigants for processed grains used 180.569 Forchlorfenuron; tolerances for resi- in production of fermented malt bev- dues. erage; tolerances for residues. 180.523 Metaldehyde; tolerances for resi- 180.570 Isoxadifen-ethyl; tolerances for residues. dues. 180.525 Resmethrin; tolerances for residues. 180.571 Mesotrione; tolerances for residues. 180.526 Synthetic isoparaffinic petroleum 180.572 Bifenazate; tolerance for residues. hydrocarbons; tolerances for residues. 180.573 Tepraloxydim; tolerances for resi- 180.527 Flufenacet, N-(4-fluorophenyl)-N-(1- dues. methylethyl)-2-[[5-(trifluoromethyl)-1, 3, 180.574 Fluazinam; tolerances for residues. 4-thiadiazol-2-yl] oxy]acetamide and its 180.575 Sulfuryl fluoride; tolerances for resi- metabolites containing the 4-fluoro-N- dues. methylethyl benzenamine tolerances for 180.576 Cyhalofop-butyl; tolerances for resi- residues. dues. 180.530 2,2-Dimethyl-1,3-benzodioxol-4-ol 180.577 Bispyribac-sodium; tolerances for methylcarbamate; tolerances for resi- residues. dues. 180.578 Acetamiprid; tolerances for residues. 180.532 Cyprodinil; tolerances for residues. 180.579 Fenamidone; tolerances for residues. 180.533 Esfenvalerate; tolerances for resi- 180.580 Iodosulfuron-Methyl-Sodium; toler- dues. ances for residues. 180.535 Fluroxypyr 1-methylheptyl ester; 180.581 Iprovalicarb; tolerances for residues. tolerances for residues. 180.582 Pyraclostrobin; tolerances for resi- 180.537 Isoxaflutole; tolerances for residues. dues. 180.539 d-Limonene; tolerances for residues. 180.583 Triticonazole; tolerances for resi- 180.540 Fenitrothion; tolerances for residues. dues. 180.584 Tolylfluanid; tolerances for residues. 180.543 Diclosulam; tolerances for residues. 180.585 Pyraflufen-ethyl; tolerances for resi- 180.544 Methoxyfenozide; tolerances for residues. dues. 180.586 Clothianidin; tolerances for residues. 180.545 Prallethrin; tolerances for residues. 180.587 Famoxadone; tolerance for residues. 180.546 Mefenoxam; tolerances for residues. 180.588 Quinoxyfen; tolerances for residues. 180.547 Prohexadione calcium; tolerances 180.589 Boscalid; tolerances for residues. for residues. 180.590 2, 6-Diisopropylnaphthalene (2, 6- 180.548 Tralkoxydim; tolerances for resi- DIPN); tolerances for residues. dues. 180.591 Trifloxysulfuron; tolerances for resi- 180.549 Diflufenzopyr; tolerances for residues. dues. 180.592 Butafenacil; tolerances for residues. 180.551 Fluthiacet-methyl; tolerances for 180.593 Etoxazole; tolerances for residues. residues. 180.594 Thiacloprid; tolerances for residues. 180.552 Sulfosulfuron; tolerances for resi- 180.595 Flufenpyr-ethyl; tolerances for residues. dues. 180.553 Fenhexamid; tolerances for residues. 180.596 Fosthiazate; tolerances for residues.

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180.597 Mesosulfuron-methyl; tolerances for 180.642 Gentamicin; tolerances for residues. residues. 180.643 Uniconazole; tolerances for residues. 180.598 Novaluron; tolerances for residues. 180.644 Cyprosulfamide; tolerances for resi- 180.599 Acequinocyl; tolerances for residues. dues. 180.600 Propoxycarbazone; tolerances for 180.645 Thiencarbazone-methyl; tolerances residues for residues. 180.601 Cyazofamid; tolerances for residues. 180.646 Ipconazole; tolerances for residues. 180.602 Spiroxamine; tolerances for residues. 180.647 d-Phenothrin; tolerances for resi- 180.603 Dinotefuran; tolerances for residues. dues. 180.604 Mepanipyrim; tolerances for resi- 180.648 Meptyldinocap; tolerances for residues. dues. 180.605 Penoxsulam; tolerances for residues. 180.649 Saflufenacil; tolerances for residues. 180.607 Spiromesifen; tolerances for resi- 180.650 Isoxaben; tolerances for residues. dues. 180.651 Imazosulfuron; tolerances for resi- 180.608 Spirodiclofen; tolerances for residues. dues. 180.652 Ethiprole; tolerances for residues. 180.609 Fluoxastrobin; tolerances for resi- 180.653 Indaziflam; tolerances for residues. dues. 180.654 Isopyrazam; tolerances for residues. 180.610 Aminopyralid; tolerances for resi- 180.655 Flazasulfuron; tolerances for residues. dues. 180.611 Pinoxaden; tolerances for residues. 180.656 Amisulbrom; tolerances for residues. 180.612 Topramezone; tolerances for resi- 180.657 Metaflumizone; tolerances for residues. dues. 180.613 Flonicamid; tolerances for residues. 180.658 Penthiopyrad; tolerances for resi- 180.614 Kasugamycin; tolerances for residues. dues. 180.659 Pyroxasulfone; tolerances for resi- 180.615 Amicarbazone; tolerances for residues. dues. 180.660 Pyriofenone; tolerances for residues. 180.616 Fenpropimorph; tolerances for resi- 180.661 Fluopyram; tolerances for residues. dues. 180.662 Trinexapac-ethyl; tolerances for res- 180.617 Metconazole; tolerances for residues. idues. 180.618 Benthiavalicarb-isopropyl; tolerance 180.663 Ametoctradin; tolerances for resi- for residues. dues. 180.619 Epoxiconazole; tolerances for resi- 180.664 Penflufen; tolerances for residues. dues. 180.665 Sedaxane; tolerances for residues. 180.620 Etofenprox; tolerances for residues. 180.666 Fluxapyroxad; tolerances for resi- 180.621 Dithianon; tolerances for residues. dues. 180.622 Ethaboxam; tolerances for residues. 180.667 Cyflufenamid, tolerance for residues. 180.623 Flufenoxuron; tolerances for resi- 180.668 Sulfoxaflor; tolerances for residues. dues. 180.669 Picoxystrobin; tolerances for resi- 180.624 Metrafenone; tolerances for residues. dues. 180.625 Orthosulfamuron; tolerances for res- 180.671 Fenpyrazamine; tolerances for resi- idues. dues. 180.626 Prothioconazole; tolerances for resi- 180.672 Cyantraniliprole; tolerances for residues. dues. 180.627 Fluopicolide; tolerances for residues. 180.673 Triforine; tolerances for residues. 180.628 Chlorantraniliprole; tolerances for 180.674 Proquinazid; tolerances for residues. residues. 180.675 Tolfenpyrad; tolerances for residues. 180.629 Flutriafol; tolerances for residues. 180.676 Fenpropidin; tolerances for residues. 180.630 Flusilazole; tolerances for residues. 180.677 Cyflumetofen; tolerances for resi- 180.631 Pyrasulfotole; tolerances for residues. dues. 180.678 Tricyclazole; tolerances for residues. 180.632 Fenazaquin; Tolerances for residues. 180.679 Flupyradifurone; tolerances for resi- 180.633 Florasulam; tolerances for residues. dues. 180.634 Tembotrione; tolerances for resi- 180.680 Fluensulfone; tolerances for residues. dues. 180.635 Spinetoram; tolerances for residues. 180.681 Isofetamid; tolerances for residues. 180.636 1,3-dichloropropene; tolerances for 180.682 Bicyclopyrone; tolerances for resi- residues. dues. 180.637 Mandipropamid; tolerances for resi- 180.684 Benalaxyl-M; tolerances for residues. dues. 180.685 Oxathiapiprolin; tolerances for resi- 180.638 Pyroxsulam; tolerances for residues. dues. 180.639 Flubendiamide; tolerances for resi- 180.686 Benzovindiflupyr; tolerances for res- dues. idues. 180.640 Pyridalyl; tolerances for residues. 180.687 Teflubenzuron; tolerances for resi- 180.641 Spirotetramat; tolerances for residues. dues. 180.688 Diethofencarb; tolerance for residue.

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Subpart D—Exemptions From Tolerances 180.1057 Phytophthora palmivora; exemption from requirement of tolerance. 180.900 Exemptions from the requirement of 180.1058 Sodium diacetate; exemption from a tolerance. the requirement of a tolerance. 180.905 Pesticide chemicals; exemptions 180.1064 Tomato pinworm insect pheromone; from the requirement of a tolerance. exemption from the requirement of a tol- 180.910 Inert ingredients used pre- and post- erance. harvest; exemptions from the require- 180.1065 2-Amino-4,5-dihydro-6-methyl-4- ment of a tolerance. propyl-s-triazolo(1,5-alpha)pyrimidin-5- 180.920 Inert ingredients used pre-harvest; one; exemption from the requirement of exemptions from the requirement of a a tolerance. tolerance. 180.1067 Methyl eugenol and malathion com- 180.930 Inert ingredients applied to animals; bination; exemption from the require- exemptions from the requirement of a ment of a tolerance. tolerance. 180.1068 C12-C18 fatty acid potassium salts; 180.940 Tolerance exemptions for active and exemption from the requirement of a tol- inert ingredients for use in antimicrobial erance. formulations (Food-contact surface sani- 180.1069 (Z)-11-Hexadecenal; exemption from tizing solutions). the requirement of a tolerance. 180.950 Tolerance exemptions for minimal 180.1070 Sodium chlorite; exemption from risk active and inert ingredients. the requirement of a tolerance. 180.960 Polymers; exemptions from the re- 180.1071 Peanuts, Tree Nuts, Milk, Soy- quirement of a tolerance. beans, Eggs, Fish, Crustacea, and Wheat; 180.1011 Viable spores of the microorganism exemption from the requirement of a tol- Bacillus thuringiensis Berliner; exemption erance. from the requirement of a tolerance. 180.1072 Poly-D-glucosamine (chitosan); ex- 180.1016 Ethylene; exemption from the re- emption from the requirement of a toler- quirement of a tolerance. ance. 180.1017 Diatomaceous earth; exemption 180.1073 Isomate-M; exemption from the re- from the requirement of a tolerance. quirement of a tolerance. 180.1019 Sulfuric acid; exemption from the 180.1074 F.D.&C. Blue No. 1; exemption from requirement of a tolerance. the requirement of a tolerance. 180.1020 Sodium chlorate; exemption from 180.1075 Colletotrichum gloeosporioides f. sp. the requirement of a tolerance. aeschynomene; exemption from the re- 180.1021 Copper; exemption from the requirement of a tolerance. quirement of a tolerance. 180.1076 Viable spores of the microorganism 180.1022 Iodine-detergent complex; exemp- Bacillus popilliae; exemption from the re- tion from the requirement of a tolerance. quirement of a tolerance. 180.1023 Propanoic acid; exemptions from 180.1080 Plant volatiles and pheromone; ex- the requirement of a tolerance. emptions from the requirement of a tol- 180.1025 Xylene; exemption from the re- erance. quirement of a tolerance. 180.1083 Dimethyl sulfoxide; exemption 180.1027 Nuclear polyhedrosis virus of from the requirement of a tolerance. Heliothis zea; exemption from the re- 180.1084 Monocarbamide dihydrogen sulfate; quirement of a tolerance. exemption from the requirement of a tol- 180.1033 Methoprene; exemption from the re- erance. quirement of a tolerance. 180.1086 3,7,11-Trimethyl-1,6,10-dodecatriene- 180.1037 Polybutenes; exemption from the 1-ol and 3,7,11-trimethyl-2,6,10- requirement of a tolerance. dodecatriene-3-ol; exemption from the re- 180.1040 Ethylene glycol; exemption from quirement of a tolerance. the requirement of a tolerance. 180.1087 Sesame stalks; exemption from the 180.1041 Nosema locustae; exemption from requirement of a tolerance. the requirement of a tolerance. 180.1089 Poly-N-acetyl-D-glucosamine; ex- 180.1043 Gossyplure; exemption from the re- emption from the requirement of a toler- quirement of a tolerance. ance. 180.1049 Carbon dioxide; exemption from the 180.1090 Lactic acid; exemption from the re- requirement of a tolerance. quirement of a tolerance. 180.1050 Nitrogen; exemption from the re- 180.1091 Aluminum isopropoxide and alu- quirements of a tolerance. minum secondary butoxide; exemption 180.1052 2,2,5-trimethyl-3-dichloroacetyl-1,3- from the requirement of a tolerance. oxazolidine; exemption from the require- 180.1092 Menthol; exemption from the re- ment of a tolerance. quirement of a tolerance. 180.1054 Calcium hypochlorite; exemptions 180.1095 Chlorine gas; exemptions from the from the requirement of a tolerance. requirement of a tolerance. 180.1056 Boiled linseed oil; exemption from 180.1097 GBM-ROPE; exemption from the re- requirement of tolerance. quirement of a tolerance.

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180.1098 Gibberellins [Gibberellic Acids (GA3 180.1130 N-(n-octyl)-2-pyrrolidone and N-(n- and GA4 + GA7), and Sodium or Potas- dodecyl)-2-pyrrolidone; exemptions from sium Gibberellate]; exemption from the the requirement of a tolerance. requirement of a tolerance. 180.1131 Ampelomyces quisqualis isolate M10; 180.1100 Gliocladium virens isolate GL-21; ex- exemption from the requirement of a tol- emption from the requirement of a toler- erance. ance. 180.1135 Pasteuria penetrans; exemption from 180.1101 Parasitic (parasitoid) and predatory the requirement of a tolerance. insects; exemption from the requirement 180.1139 Sodium 5-nitroguaiacolate; exemp- of a tolerance. tion from the requirement of a tolerance. 180.1102 Trichoderma harzianum KRL-AG2 180.1140 Sodium o-nitrophenolate; exemp- (ATCC #20847) strain T–22; exemption tion from the requirement of a tolerance. from requirement of a tolerance. 180.1141 Sodium p-nitrophenolate; exemp- 180.1103 Isomate-C; exemption from the re- tion from the requirement of a tolerance. quirement of a tolerance. 180.1142 1,4-Dimethylnaphthalene; exemp- 180.1107 Delta endotoxin of Bacillus tion from the requirement of a tolerance. thuringiensis variety kurstaki encap- 180.1143 Methyl anthranilate; exemption sulated into killed Pseudomonas from the requirement of a tolerance. fluorescens; exemption from the require- 180.1144 Candida oleophila isolate I-182; ex- ment of a tolerance. emption from the requirement of a toler- 180.1108 Delta endotoxin of Bacillus ance. thuringiensis variety San Diego encap- 180.1145 Pseudomonas syringae; exemption sulated into killed Pseudomonas from the requirement of a tolerance. fluorescens; exemption from the require- 180.1146 Beauveria bassiana Strain GHA; ex- ment of a tolerance. emption from the requirement of a toler- 180.1110 3-Carbamyl-2,4,5-trichlorobenzoic ance. acid; exemption from the requirement of 180.1148 Occlusion Bodies of the Granulosis a tolerance. Virus of Cydia pomenella; tolerance ex- 180.1111 Bacillus subtilis GB03; exemption emption. from the requirement of a tolerance. 180.1149 Inclusion bodies of the multi-nu- 180.1113 Lagenidium giganteum; exemption clear polyhedrosis virus of Anagrapha from the requirement of a tolerance. falcifera; exemption from the require- 180.1114 Pseudomonas fluorescens A506, ment of a tolerance. Pseudomonas fluorescens 1629RS, and 180.1150 6-Benzyladenine; exemption from Pseudomonas syringae 742RS; exemptions the requirement of a tolerance. from the requirement of a tolerance. 180.1153 Lepidopteran pheromones; exemp- 180.1118 Spodoptera exigua nuclear poly- tion from the requirement of a tolerance. hedrosis virus; exemption from the re- 180.1154 CryIA(c) and CryIC derived delta- quirement of a tolerance. endotoxins of Bacillus thuringiensis var. 180.1119 Azadirachtin; exemption from the kurstaki encapsulated in killed requirement of a tolerance. Pseudomonas fluorescens, and the expres- 180.1120 Streptomyces sp. strain K61; exemp- sion plasmid and cloning vector genetic tion from the requirement of a tolerance. constructs. 180.1121 Boric acid and its salts, borax (so- 180.1156 Cinnamaldehyde; exemption from dium borate decahydrate), disodium the requirement of a tolerance. octaborate tetrahydrate, boric oxide 180.1157 Cytokinins; exemption from the re- (boric anhydride), sodium borate and so- quirement of a tolerance. dium metaborate; exemptions from the 180.1158 Auxins; exemption from the re- requirement of a tolerance. quirement of a tolerance. 180.1122 Inert ingredients of semiochemical 180.1159 Pelargonic acid; exemption from dispensers; exemptions from the require- the requirement of tolerances. ment of a tolerance. 180.1160 Jojoba oil; exemption from the re- 180.1124 Arthropod pheromones; exemption quirement of a tolerance. from the requirement of a tolerance. 180.1161 Clarified hydrophobic extract of 180.1126 Codlure, (E,E)-8,10-Dodecadien-1-ol; neem oil; exemption from the require- exemption from the requirement of a tol- ment of a tolerance. erance. 180.1162 Acrylate polymers and copolymers; 180.1127 Biochemical pesticide plant floral exemption from the requirement of a tol- volatile attractant compounds: cinna- erance. maldehyde, cinnamyl alcohol, 4-methoxy 180.1163 Killed Myrothecium verrucaria; ex- cinnamaldehyde, 3-phenyl propanol, 4- emption from the requirement of a toler- methoxy phenethyl alcohol, indole, and ance. 1,2,4-trimethoxybenzene; exemptions 180.1165 Capsaicin; exemption from the re- from the requirement of a tolerance. quirement of a tolerance. 180.1128 Bacillus amyloliquefaciens MBI600; 180.1167 Allyl isothiocyanate as a compo- exemption from the requirement of a tol- nent of food grade oil of mustard; exemp- erance. tion from the requirement of a tolerance.

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180.1176 Sodium bicarbonate; exemption 180.1218 Indian Meal Moth Granulosis Virus; from the requirement of a tolerance. exemption from the requirement of a tol- 180.1177 Potassium bicarbonate; exemption erance. from the requirement of a tolerance. 180.1219 Foramsulfuron; exemption from the 180.1178 Formic acid; exemption from the requirement of a tolerance. requirement of a tolerance. 180.1220 1-Methylcyclopropene; exemption 180.1179 Plant extract derived from Opuntia from the requirement of a tolerance. lindheimeri, Quercus falcata, Rhus 180.1221 Pseudozyma flocculosa strain PF-A22 aromatica, and Rhizophoria mangle; ex- UL; exemption from the requirement of a emption from the requirement of a toler- tolerance. ance. 180.1222 Sucrose octanoate esters; exemp- 180.1180 Kaolin; exemption from the require- tion from the requirement of a tolerance. ment of a tolerance. 180.1223 Imazamox; exemption from the re- 180.1181 Bacillus cereus strain BPO1; exemp- quirement of a tolerance. tion from the requirement of a tolerance. 180.1224 Bacillus pumilus GB34; exemption 180.1187 L-glutamic acid; exemption from from the requirement of a tolerance. the requirement of a tolerance. 180.1225 Decanoic acid; exemption from the 180.1188 Gamma aminobutyric acid; exemp- requirement of a tolerance. tion from the requirement of a tolerance. 180.1226 Bacillus pumilus strain QST2808; 180.1189 Methyl salicylate; exemption from temporary exemption from the require- the requirement of a tolerance. ment of a tolerance. 180.1191 Ferric phosphate; exemption from 180.1228 Diallyl sulfides; exemption from the the requirement of a tolerance. requirement of a tolerance. 180.1193 Potassium dihydrogen phosphate; 180.1230 Ferrous sulfate; exemption from exemption from the requirement of a tol- the requirement of a tolerance. 180.1231 Lime; exemption from the require- erance. ment of a tolerance. 180.1195 Titanium dioxide. 180.1232 Lime-sulfur; exemption from the re- 180.1196 Peroxyacetic acid; exemption from quirement of a tolerance. the requirement of a tolerance. 180.1233 Potassium sorbate; exemption from 180.1197 Hydrogen peroxide; exemption from the requirement of a tolerance. the requirement of a tolerance. 180.1234 Sodium carbonate; exemption from 180.1198 Gliocladium catenulatum strain the requirement of a tolerance. J1446; exemption from the requirement of 180.1235 Sodium hypochlorite; exemption a tolerance. from the requirement of a tolerance. 180.1199 Lysophosphatidylethanolamine 180.1236 Sulfur; exemption from the require- (LPE); exemption from the requirement ment of a tolerance. of a tolerance. 180.1237 Sodium metasilicate; exemption 180.1200 Pseudomonas fluorescens strain from the requirement of a tolerance. PRA–25; temporary exemption from the 180.1240 Thymol; exemption from the re- requirement of a tolerance. quirement of a tolerance. 180.1201 Trichoderma harzianum strain T-39; 180.1241 Eucalyptus oil; exemption from the exemption from the requirement of a tol- requirement of a tolerance. erance. 180.1243 Bacillus subtilis var. amylolique- 180.1202 Bacillus sphaericus; exemption from faciens strain FZB24; exemption from the the requirement of a tolerance. requirement of a tolerance. 180.1204 Harpin protein; exemption from the 180.1244 Ammonium bicarbonate; exemption requirement of a tolerance. from the requirement of a tolerance. 180.1205 Beauveria bassiana ATCC #74040; ex- 180.1245 Rhamnolipid biosurfactant; exemp- emption from the requirements of a tol- tion from the requirement of a tolerance. erance. 180.1246 Yeast Extract Hydrolysate from 180.1206 Aspergillus flavus AF36; exemption Saccharomyces cerevisiae: exemption from from the requirement of a tolerance. the requirement of a tolerance. 180.1207 N-acyl sarcosines and sodium N- 180.1248 Exemption of citronellol from the acyl sarcosinates; exemption from the re- requirement of a tolerance. quirement of a tolerance. 180.1250 C8, C10, and C12 fatty acid mono- 180.1209 Bacillus subtilis strain QST 713 and esters of glycerol and propylene glycol; strain QST 713 variant soil; exemption exemption from the requirement of a tol- from the requirement of a tolerance. erance. 180.1210 Phosphorous acid; exemption from 180.1251 Geraniol; exemption from the re- the requirement of a tolerance. quirement of a tolerance. 180.1212 Pseudomonas chlororaphis Strain 63– 180.1253 Streptomyces lydicus WYEC 108; ex- 28; exemption from the requirement of a emption from the requirement of a toler- tolerance. ance. 180.1213 Coniothyrium minitans strain CON/ 180.1254 Aspergillus flavus NRRL 21882; ex- M/91–08; exemption from the requirement emption from the requirement of a toler- of a tolerance. ance.

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180.1255 Bacillus pumilus strain QST 2808; ex- 180.1283 (Z)-7,8-epoxy-2-methyloctadecane emption from the requirement of a toler- (Disparlure); exemption from the re- ance. quirement of a tolerance. 180.1256 Alternaria destruens strain 059; ex- 180.1284 Ammonium salts of higher fatty emption from the requirement of a toler- acids (C8-C18 saturated; C8-C12 unsatu- ance. rated); exemption from the requirement 180.1257 Paecilomyces lilacinus strain 251; ex- of a tolerance. emption from the requirement of a toler- 180.1285 Polyoxin D zinc salt; exemption ance. from the requirement of a tolerance. 180.1258 Acetic acid; exemption from the re- 180.1287 Extract of Chenopodium ambrosioides quirement of a tolerance. near ambrosioides; exemption from the re- 180.1259 Reynoutria sachalinensis extract; ex- quirement of a tolerance. emption from the requirement of a toler- 180.1288 Tristyrylphenol ethoxylates; ex- ance. emption from the requirement of a toler- 180.1260 Muscodor albus QST 20799 and the ance. volatiles produced on rehydration; ex- 180.1289 Candida oleophila Strain O; exemp- emption from the requirement of a toler- tion from the requirement of a tolerance. ance. 180.1290 Pasteuria usgae; exemption from the 180.1261 Xanthomonas campestris pv. requirement of a tolerance. vesicatoria and Pseudomonas syringae pv. 180.1291 Cold pressed neem oil; exemption tomato specific Bacteriophages. from the requirement of a tolerance. 180.1262 Sorbitol octanoate; exemption from 180.1292 Ulocladium oudemansii (U3 Strain); the requirement of a tolerance. exemption from the requirement of a tol- 180.1263 Tetrahydrofurfuryl alcohol; exemp- erance. tion from the requirement of a tolerance. 180.1293 Trichoderma gamsii strain ICC 080; 180.1267 Pantoea agglomerans strain C9–1; ex- exemption from the requirement of a tol- emption from the requirement of a toler- erance. ance. 180.1294 Trichoderma asperellum strain ICC 180.1268 Potassium silicate; exemption from 012; exemption from the requirement of a the requirement of a tolerance. tolerance. 180.1269 Bacillus mycoides isolate J; exemp- 180.1295 Laminarin; exemption from the re- tion from the requirement of a tolerance. quirement of a tolerance. 180.1270 Isophorone; exemption from the requirement of a tolerance. 180.1296 Terpene Constituents a-terpinene, 180.1271 Eucalyptus oil; exemption from the d-limonene and p-cymene, of the Extract requirement of a tolerance. of Chenopodium ambrosioides near 180.1272 Pantoea agglomerans strain E325; ex- ambrosioides as Synthetically Manufac- emption from the requirement of a toler- tured; exemption from the requirement ance. of a tolerance. 180.1273 Beauveria bassiana HF23; exemp- 180.1297 Homobrassinolide; exemption from tion from the requirement of a tolerance. the requirement of a tolerance. 180.1274 Tris (2-ethylhexyl) phosphate; ex- 180.1298 Trichoderma hamatum isolate 382; emption from the requirement of a toler- exemption from the requirement of a tol- ance. erance. 180.1275 Pythium; exception from the re- 180.1299 Prohydrojasmon; exemption from quirement of a tolerance. the requirement of a tolerance. 180.1276 Tobacco mild green mosaic 180.1300 Potassium hypochlorite; exemption tobamovirus strain U2; exemption from from the requirement of a tolerance. the requirement of a tolerance. 180.1301 Escherichia coli O157:H7 specific 180.1277 Dibasic esters; exemption from the bacteriophages; temporary exemption requirement of a tolerance. from the requirement of a tolerance. 180.1278 Quillaja saponaria extract 180.1302 Sodium Ferric Ethylenediamine- (saponins); exemption from the require- tetraacetate (EDTA); exemption from ment of a tolerance. the requirement of a tolerance. 180.1279 Zucchini yellow mosaic virus— 180.1303 Metarhizium anisopliae strain F52; weak strain; exemption from the require- exemption from the requirement of a tol- ment of a tolerance. erance. 180.1280 Poly(hexamethylenebiguanide) hy- 180.1304 Pseudomonas fluorescens strain drochloride (PHMB); exemption from the CL145A; exemption from the requirement requirement of a tolerance. of a tolerance. 180.1281 S-Abscisic Acid, (S)-5-(1-hydroxy- 180.1305 Chromobacterium subtsugae strain 2,6,6-trimethyl-4-oxo-1-cyclohex-2-enyl)- PRAA4–1T; exemption from the require- 3-methyl-penta-(2Z,4E)-dienoic Acid; ex- ment of a tolerance. emption from the requirement of a toler- 180.1306 Isaria fumosorosea (formerly ance. Paecilomyces fumosoroseus) Apopka 180.1282 Bacillus firmus I-1582; exemption strain 97; exemption from the require- from the requirement of a tolerance. ment of a tolerance.

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180.1307 Bacteriophage of Clavibacter 180.1329 Bacillus subtilis strain IAB/BS03, michiganensis subspecies michiganensis; exemption from the requirement of a tol- exemption from the requirement of a tolerance. erance. 180.1330 1-Octanol; exemption from the re- 180.1308 Bacillus amyloliquefaciens strain quirement of a tolerance. D747; exemption from the requirement of 180.1331 Trichoderma asperelloides strain a tolerance. JM41R; exemption from the requirement 180.1309 Bacillus subtilis strain CX–9060; ex- of a tolerance. emption from the requirement of a toler- 180.1332 Lavandulyl senecioate; exemption ance. from the requirement of a tolerance. 180.1310 Trichoderma virens strain G–41; ex- 180.1333 Potassium Salts of Hops Beta acids; emption from the requirement of a toler- exemption from the requirement of a tol- ance. erance. 180.1311 Pasteuria nishizawae—Pn1; exemp- 180.1334 Choline Chloride; exemption from tion from the requirement of a tolerance. the requirement of a tolerance. 180.1312 Aureobasidium pullulans strains 180.1336 Bacillus amyloliquefaciens strain DSM 14940 and DSM 14941; exemption PTA–4838; exemption from the require- from the requirement of a tolerance. ment of a tolerance. 180.1313 Bacillus pumilus strain GHA 180; exemption from the requirement of a toler- Subpart E—Pesticide Chemicals Not Re- ance. quiring a Tolerance or an Exemption 180.1314 Killed, nonviable Streptomyces From a Tolerance acidiscabies strain RL–110T; exemption from the requirement of a tolerance. 180.2000 Scope. 180.1315 Natamycin; exemption from the re- 180.2003 Definitions. quirement of a tolerance. 180.2010 Threshold of regulation determina- 180.1316 Pasteuria spp. (Rotylenchulus tions. reniformis nematode)—Pr3; exemption 180.2020 Non-food determinations. from the requirement of a tolerance. AUTHORITY: 21 U.S.C. 321(q), 346a and 371. 180.1317 Pesticide chemicals; exemption from the requirements of a tolerance. SOURCE: 36 FR 22540, Nov. 25, 1971, unless 180.1318 3-decen-2-one; exemption from the otherwise noted. requirement of a tolerance. EDITORIAL NOTE: Nomenclature changes to 180.1319 Banda de Lupinus albus doce part 180 appear at 62 FR 66023, Dec. 17, 1997. (BLAD); exemption from the requirement of a tolerance. GLOSSARY 180.1320 Methyl jasmonate; exemption from NOTE: The items in this glossary were com- the requirement of a tolerance. piled as an aid to the users of the Code of 180.1321 Complex Polymeric Polyhydroxy Federal Regulations. Inclusion or exclusion Acids; exemption from the requirement from this glossary has no legal significance. of a tolerance. APPLI = APPLICATION 180.1322 Bacillus pumilus strain BU F–33; ex- C-I MET = CHOLINESTERASE-INHIBITING emption from the requirement of a toler- METABOLITES ance. CARB = CARBAMATES 180.1323 Ethyl-2E,4Z-decadienoate (Pear EPWRR = EDIBLE PORTION WITH RIND Ester); exemption from the requirement REMOVED of a tolerance. EXC = EXCEPT 180.1324 GS-omega/kappa-Hxtx-Hv1a; ex- I (IN PPM COLUMN) = INTERIM TOLER- emption from the requirement of a toler- ANCE ance. INC = INCLUDING 180.1325 Heat-killed Burkholderia spp. strain K = CWHR = KERNEL PLUS COB WITH A396 cells and spent fermentation media HUSK REMOVED exemption from the requirement of a tol- MBYP = MEAT BYPRODUCTS erance. MIN = MINIMUM 180.1326 Pseudomonas fluorescens strain D7; N (IN PPM COLUMN) = NEGLIGIBLE RESI- exemption from the requirement of a tol- DUES erance. NMT = NOT MORE THAN 180.1327 Tetraacetylethylenediamine NON-PER BAG/PKGD RAC = NON-PERISH- (TAED) and its metabolite ABLE PACKAGED OR BAGGED RAW AG- Diacetylethylenediamine (DAED); ex- RICULTURAL COMMODITY emption from the requirement of a toler- PPM = PART(S) PER MILLION ance. POST-H = POSTHARVEST APPLICATION 180.1328 Beauveria bassiana strain ANT–03; PRE-H = PREHARVEST APPLICATION exemption from the requirement of a tol- PRE-S = PRESLAUGHTER APPLICATION erance. PRODS = PRODUCTS rollert

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T (IN PPM COLUMN) = TEMPORARY TOL- essed food will not be considered unsafe ERANCE within the meaning of FFDCA sections [41 FR 4537, Jan. 30, 1976] 402 and 408(a), despite the lack of a tolerance or exemption for the pesticide Subpart A—Definitions and chemical residue in the processed food, Interpretative Regulations if: (1) The pesticide chemical has been § 180.1 Definitions and interpretations. used in or on the raw agricultural com- (a) Administrator, without qualifica- modity in conformity with a tolerance tion, means the Administrator of the under this section; Environmental Protection Agency. (2) The pesticide chemical residue (b) Agency, without qualification, has been removed to the extent pos- means the Environmental Protection sible in good manufacturing practice; Agency. and (c) FFDCA means the Federal Food, (3) The concentration of the pesticide Drug, and Cosmetic Act, as amended, chemical residue in the processed food 21 U.S.C. 301–392. is not greater than the tolerance pre- (d) Raw agricultural commodities in- scribed for the pesticide chemical res- clude, among other things, fresh fruits, idue on the raw agricultural com- whether or not they have been washed modity. and colored or otherwise treated in (f) For the purpose of computing fees their unpeeled natural form; vegetables as required by § 180.33, each group of re- in their raw or natural state, whether lated crops listed in § 180.34(e) and each or not they have been stripped of their crop group or subgroup listed in § 180.41 outer leaves, waxed, prepared into is counted as a single raw agricultural fresh green salads, etc.; grains, nuts, commodity in a petition or request for eggs, raw milk, meats, and similar ag- tolerances or exemption from the re- ricultural produce. It does not include quirement of a tolerance. foods that have been processed, fab- (g) Tolerances and exemptions estab- ricated, or manufactured by cooking, lished for pesticide chemicals in or on freezing, dehydrating, or milling. the general category of raw agricul- (e) Where a raw agricultural com- tural commodities listed in column A modity bearing a pesticide chemical apply to the corresponding specific raw residue that has been exempted from agricultural commodities listed in col- the requirement of a tolerance, or umn B. However, a tolerance or exemp- which is within a tolerance permitted tion for a specific commodity in col- under FFDCA section 408, is used in umn B does not apply to the general preparing a processed food, the proc- category in column A.

A B

Alfalfa Medicago sativa L. Subsp. sativa, (alfalfa, lucerne); Onobrychis viciifolia Scop. (sainfoin, holy clover, esparcet); and Lotus corniculatus L. (trefoil); and varieties and/or hybrids of these.

Banana Banana, plantain.

Bean Cicer arietinum (chickpea, garbanzo bean); Lupinus spp. (including sweet lupine, white sweet lupine, white lupine, and grain lupine). Phaseolus spp. (including kidney bean, lima bean, mung bean, navy bean, pinto bean, snap bean, and waxbean; Vicia faba (broad bean, fava bean); Vigna spp. (including asparagus bean, blackeyed pea and cowpea).

Bean, dry All beans above in dry form only.

Bean, succulent All beans above in succulent form only.

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A B

Blackberry Rubus eubatus (including bingleberry, black satin berry, boysenberry Cherokee blackberry, Chesterberry, Cheyenne blackberry, coryberry, darrowberry, dewberry, Dirksen thornless berry, Himalayaberry, hullberry, Lavacaberry, lowberry, Lucretiaberry, mammoth blackberry, marionberry, nectarberry, olallieberry, Oregon evergreen berry, phenomenalberry, rangerberry, ravenberry, rossberry, Shawnee blackberry, and varieties and/or hybrids of these).

Broccoli Broccoli, chinese broccoli (gia lon, white flowering broccoli).

Cabbage Cabbage, Chinese cabbage (tight-heading varieties only).

Caneberry Rubus spp. (including blackberry); Rubus caesius (youngberry); Rubus loganbaccus (loganberry); Rubus idaeus (red and black raspberry); cultivars, varieties, and/or hybrids of these.

Celery Celery, Florence fennel (sweet anise, sweet fennel, finochio) (fresh leaves and stalks only).

Cherry Cherry, sweet, and cherry, tart.

Endive Endive, escarole.

Fruit, citrus Grapefruit, lemon, lime, orange, tangelo, tangerine, citrus citron, kumquat, and hybrids of these.

Garlic Garlic, great headed; garlic, and serpent garlic.

Lettuce Lettuce, head; and lettuce, leaf

Lettuce, head Lettuce, head; crisphead varieties only

Lettuce, leaf Lettuce, leaf; cos (romaine), butterhead varieties

Marjoram Origanum spp. (includes sweet or annual marjoram, wild marjoram or oregano, and pot marjoram).

Melon Muskmelon, including hybrids and/or varieties of Cucumis melo (including true cantaloupe, cantaloupe, casaba, Santa Claus melon, crenshaw melon, honeydew melon, honey balls, Persian melon, golden pershaw melon, mango melon, pineapple melon, snake melon); and watermelon, including hybrids and/or varieties of (Citrullus spp.).

Muskmelon Cucumis melo (includes true cantaloupe, cantaloupe, casaba, Santa Claus melon, crenshaw melon, honeydew melon, honey balls, Per- sian melon, golden pershaw melon, mango melon, pineapple melon, snake melon, and other varieties and/or hybrids of these.)

Onion Bulb onion; green onion; and garlic.

Onion, bulb Bulb onion; garlic; great headed garlic; serpent garlic; Chinese onion; pearl onion; potato onion; and shallot, bulb.

Onion, green Green onion; lady’s leek; leek; wild leek; Beltsville bunching onion; fresh onion; tree onion, tops; Welsh onion; and shallot, fresh leaves.

Peach Peach, nectarine

Pea Cajanus cajan (includes pigeon pea); Cicer spp. (includes chickpea and garbanzo bean); Lens culinaris (lentil); Pisum spp. (includes dwarf pea, garden pea, green pea, English pea, field pea, and edible pod pea). [Note: A variety of pesticide tolerances have been previously established for pea and/or bean. Chickpea/garbanzo bean is now classified in both the bean and the pea categories. For garbanzo bean/chickpea only, the highest established pea or bean tolerance will apply to pesticide residues found in this commodity.]

Pea, dry All peas in dry form only.

Pea, succulent All peas in succulent form only.

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A B

Pepper All varieties of pepper including pimento and bell, hot, and sweet pepper.

Radish, oriental, roots Raphanus sativus var. longipinnatus (roots and tops), including Chi- nese or Japanese radish (both white and red), winter radish, daikon, lobok, lo pak, and other cultivars and/or hybrids of these.

Radish, oriental, tops) Raphanus sativus var. longipinnatus (roots and tops), including Chi- nese or Japanese radish (both white and red), winter radish, daikon, lobok, lo pak, and other cultivars and/or hybrids of these.

Rapeseed Brassica napus, B. campestris, and Crambe abyssinica (oilseed-producing varieties only which include canola and crambe.)

Raspberry Rubus spp. (including bababerry; black raspberry; blackcap; caneberry; framboise; frambueso; himbeere; keriberry; mayberry; red raspberry; thimbleberry; tulameen; yellow raspberry; and cultivars, varieties, and/or hybrids of these).

Sorghum, grain, grain Sorghum spp. [sorghum, grain, sudangrass (seed crop), and hybrids of these grown for its seed].

Sorghum, forage, stover Sorghum spp. [sorghum, forage; sorghum, stover; sudangrass, and hybrids of these grown for forage and/or stover.

Squash Pumpkin, summer squash, and winter squash.

Sugar apple Annona squamosa L. (sugar apple, sweetsop, anon), and its hybrid A. squamosa L. x A. cherimoya M. (atemoya). Also A. reticulata L. (true custard apple).

Squash, summer Fruits of the gourd (Cucurbitaceae) family that are consumed when immature, 100% of the fruit is edible either cooked or raw, once picked it cannot be stored, has a soft rind which is easily penetrated, and if seeds were harvested they would not germinate; e.g., Cucurbita pepo (i.e., crookneck squash, straightneck squash, scallop squash, and vegetable marrow); Lagenaria spp. (i.e., spaghetti squash, hyotan, cucuzza); Luffa spp. (i.e., hechima, Chinese okra); Momordica spp. (i.e., bitter melon, balsam pear, balsam apple, Chi- nese cucumber); Sechium edule (chayote); and other cultivars and/or hybrids of these.

Sweet potato Sweet potato, yam.

Tangerine Tangerine (mandarin or mandarin orange); clementine; Mediterranean mandarin; satsuma mandarin; tangelo; tangor; cultivars, varieties, and/or hybrids of these.

Tomato Tomato, tomatillo.

Turnip tops or turnip greens Broccoli raab (raab, raab salad), hanover salad, turnip tops (turnip greens).

Wheat Wheat, triticale.

(h) Unless otherwise specified in this (2) Shell shall be removed and dis- paragraph or in tolerance regulations carded from nuts before examination prescribed in this part for specific pes- for pesticide residues. ticide chemicals, the raw agricultural (3) Caps (hulls) shall be removed and commodity or processed food to be ex- discarded from strawberries before examined for pesticide residues, shall amination for pesticide residues. consist of the whole raw agricultural (4) Stems shall be removed and dis- commodity or processed food. carded from melons before examination (1) The raw agricultural commodity for pesticide residues. bananas, when examined for pesticide (5) Roots, stems, and outer sheaths residues, shall not include any crown (or husks) shall be removed and dis- tissue or stalk. carded from garlic bulbs and dry bulb onions, and only the garlic cloves and

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onion bulbs shall be examined for pes- that has been demonstrated to have no ticide residues. effect from feeding studies on the most (6) Where a tolerance is established sensitive animal species tested. Such on a root vegetable including tops and/ toxicity studies shall usually include or with tops, and the tops and the roots at least 90-day feeding studies in two are marketed together, they shall be species of mammals. analyzed separately and neither the (k) The term nonperishable raw agri- pesticide residue on the roots nor the cultural commodity means any raw agri- pesticide residue on the tops shall ex- cultural commodity not subject to ceed the tolerance level, except that in rapid decay or deterioration that would the case of carrots, parsnips, and ruta- render it unfit for consumption. Exam- bagas, the tops shall be removed and ples are cocoa beans, coffee beans, discarded before analyzing roots for field-dried beans, field-dried peas, pesticide residues. grains, and nuts. Not included are eggs, (7) The crowns (leaves at the top of milk, meat, poultry, fresh fruits, and the fruit) shall be removed and dis- vegetables such as onions, parsnips, po- carded from pineapples before examina- tatoes, and carrots. tion for pesticide residues. (l) The term tolerance with regional (8) The term lima beans means the registration means any tolerance which beans and the pod. is established for pesticide residues re- (9) The term peanuts means the pea- sulting from the use of the pesticide nut meat after removal of the hulls. pursuant to a regional registration. (10) For processed foods consisting Such a tolerance is supported by res- primarily of one ingredient and sold in idue data from specific growing regions a form requiring further preparation for a raw agricultural commodity. Indi- prior to consumption (e.g., fruit juice vidual tolerances with regional reg- concentrates, dehydrated vegetables, istration are designated in separate and powdered potatoes), the processed subsections in 40 CFR 180.101 through food to be examined for residues shall 180.999, as appropriate. Additional res- be the whole processed commodity idue data which are representative of after compensating for or reconsti- the proposed use area are required to tuting to the commodity’s normal expand the geographical area of usage moisture content, unless a tolerance of a pesticide on a raw agricultural for the concentrated or dehydrated commodity having an established ‘‘tol- food form is included in this part. If erance with regional registration.’’ there exists a tolerance for a specific Persons seeking geographically broad- pesticide on the processed food in its er registration of a crop having a ‘‘tol- concentrated or dehydrated food form, erance with regional registration’’ for the purpose of determining whether should contact the appropriate EPA the food is in compliance with that tol- product manager concerning additional erance, the processed food to be exam- residue data required to expand the use ined for residues shall be the whole area. processed commodity on an ‘‘as is’’ (m) The term pesticide chemical res- basis. idue shall have the meaning specified (i) The term pesticide chemical shall in FFDCA section 201(q)(2), as amend- have the meaning specified in FFDCA ed, except as provided in § 180.4. section 201(q)(1), as amended, except as (n) The term food commodity means: provided in § 180.4. (1) Any raw agricultural commodity (j) The term negligible residue means (food or feed) as defined in section any amount of a pesticide chemical re- 201(r) of the Federal Food, Drug, and maining in or on a raw agricultural Cosmetic Act (FFDCA); and commodity or group of raw agricul- (2) Any processed food or feed as de- tural commodities that would result in fined in section 201(gg) of the FFDCA. a daily intake regarded as [36 FR 22540, Nov. 25, 1971] toxicologically insignificant on the EDITORIAL NOTE: For FEDERAL REGISTER ci- basis of scientific judgment of ade- tations affecting § 180.1, see the List of CFR quate safety data. Ordinarily this will Sections Affected, which appears in the add to the diet an amount which will Finding Aids section of the printed volume be less than 1/2,000th of the amount and at www.fdsys.gov.

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EFFECTIVE DATE NOTE: At 81 FR 26476, May 5, 2016. For the convenience of the user, the 3, 2016, § 180.1 was amended in the table in revised text is set forth as follows: paragraph (g) by revising the entries for ‘‘Broccoli’’ and ‘‘Sugar apple’’ and by adding § 180.1 Definitions and interpretations. the entries ‘‘Fern, edible, fiddlehead’’, ‘‘Guava’’, and ‘‘Palm hearts’’, effective July * * * * * (g) * * *

A B

******* Broccoli ...... Broccoli, Chinese broccoli (gai lon, white flowering broccoli).

******* Fern, edible, fiddlehead ...... Fern, edible, fiddlehead including: Black lady fern, Deparia japonica (Thunb.) M. Kato; Bracken fern, Pteridium aquilinum (L.) Kuhn; Broad buckler fern, Dryopteris dilatata (Hoffm.) A. Gray; Cinnamon fern, Osmundastrum cinnamomeum (L.) C. Presl; Lady fern, Athyrium filix-femina (L.) Roth ex Mert.; Leather fern, Acrostichum aureum L.; Mother fern, Diplazium proliferum (Lam.) Thouars; Ostrich fern, Matteuccia struthiopteris (L.) Tod.; Vegetable fern, Diplazium esculentum (Retz.) Sw.; Zenmai fern, Osmuda japonica Thunb.

******* Guava ...... Guava (Psidium guajava L.); Guava, cattley (Psidium cattleyanum Sabine); Guava, Para (Psidium acutangulum DC.); Guava, purple strawberry (Psidium cattleyanum Sabine var. cattleyanum); Guava, strawberry (Psidium cattleyanum Sabine var. littorale (Raddi) Fosberg); Guava, yellow strawberry (Psidium cattleyanum Sabine var. cattleyanum forma lucidum O. Deg.)

******* Palm hearts ...... Palm hearts, various species, including: African fan palm, Borassus aethiopum Mart.; Cabbage palm, Euterpe oleracea Mart.; Cabbage palmetto, Sabal palmetto (Walter) Schult. & Schult. f.; Coconut, Cocos nucifera L.; Palmyra palm, Borassus flabellifera L.; Peach Palm, Bactris gasipaes Kunth; Royal palm, Roystonea oleracea (Jacq.) O.F. Cook; Salak palm, Salacca zalacca (Gaertn.) Voss; Saw palmetto, Serenoa repens (W. Bartram) Small; Wine palm, Raphia spp.

******* Sugar apple ...... Annona squamosa L. and its hybrid atemoya (Annona cherimola Mill X A. squamosa L.) Also includes true custard apple (Annona reticulata L.).

*******

* * * * * the total amount of related pesticide chemicals (such as chlorinated organic § 180.3 Tolerances for related pesticide pesticides) that may be present. chemicals. (c)(1) Where tolerances for inorganic (a) Pesticide chemicals that cause re- bromide in or on the same raw agricul- lated pharmacological effects will be tural commodity are set in two or regarded, in the absence of evidence to more sections in this part (example: the contrary, as having an additive del- §§ 180.123 and 180.199), the overall quan- eterious action. (For example, many tity of inorganic bromide to be toler- pesticide chemicals within each of the ated from use of the same pesticide in following groups have related pharma- different modes of application or from cological effects: Chlorinated organic two or more pesticide chemicals for pesticides, arsenic-containing chemi- which tolerances are established is the cals, metallic dithiocarbamates, cho- highest of the separate applicable tol- linesterase-inhibiting pesticides.) erances. For example, where the bro- (b) Tolerances established for such mide tolerance on asparagus from related pesticide chemicals may limit methyl bromide commodity fumigation the amount of a common component is 100 parts per million (40 CFR 180.123) (such as As2O3) that may be present, or and on asparagus from methyl bromide may limit the amount of biological ac- soil treatment is 300 parts per million tivity (such as cholinesterase inhibi- (40 CFR 180.199), the overall inorganic tion) that may be present, or may limit bromide tolerance for asparagus grown

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on methyl bromide-treated soil and graph (e)(3) of this section on the same also fumigated with methyl bromide raw agricultural commodity, the total after harvest is 300 parts per million. residue of such pesticides shall not ex- (2) Where tolerances are established ceed that permitted by the highest tol- in terms of inorganic bromide residues erance established for any one member only from use of organic bromide fumi- of the class, calculated both as zinc gants on raw agricutural commodities, ethylenebisdithiocarbamate and car- such tolerances are sufficient to pro- bon disulfide. The tolerance based on tect the public health, and no addi- zinc ethylenebisdithiocarbamate shall tional concurrent tolerances for the or- first be multiplied by 0.6 to convert it ganic pesticide chemicals from such to the equivalent carbon disulfide tol- use are necessary. This conclusion is erance, and then the carbon disulfide based on evidence of the dissipation of tolerance levels will be compared to de- the organic pesticide or its conversion termine the highest tolerance level per to inorganic bromide residues in the raw agricultural commodity. food when ready to eat. (6) Where tolerances are established (d)(1) Where tolerances are estab- for residues of both S,S,S-tributyl lished for both calcium cyanide and hy- phosphorotrithioate and tributyl drogen cyanide on the same raw agri- phosphorotrithioite in or on the same cultural commodity, the total amount raw agricultural commodity, the total of such pesticides shall not yield more amount of such pesticides shall not residue than that permitted by the yield more residue than that permitted larger of the two tolerances, calculated by the higher of the two tolerances, as hydrogen cyanide. calculated as S,S,S-tributyl (2) Where tolerances are established phosphorotrithioate. for residues of both O,O-diethyl S-[2- (7) Where tolerances are established (ethylthio)ethyl] phosphorodithioate for residues of O,S-dimethyl and demeton (a mixture of O,O-diethyl phosphoramidothioate, resulting from O-(and S-) [2-(ethylthio)ethyl] the use of acephate (O,S-dimethyl phosphorothioates) on the same raw acetylphos-phoramidothioate) and/or agricultural commodity, the total O,S - dimethylphosphoramidothioate amount of such pesticides shall not on the same agricultural commodity, yield more residue than that permitted the total amount of O,S-dimethyl- by the larger of the two tolerances, cal- phosphoramidothioate shall not yield culated as demeton. more residue than that permitted by (3) Where tolerances are established the higher of the two tolerances. for both terpene polychlorinates (8) Where a tolerance is established (chlorinated mixture of camphene, pi- for more than one pesticide having the nene, and related terpenes, containing metabolites 1-(3,4-dichlorophenyl)-3- 65–66 percent chlorine) and toxaphene methylurea (DCPMU) and 3,4- (chlorinated camphene containing 67–69 dichlorophenylurea (DCPU) found in or percent chlorine) on the same raw agri- on a raw agricultural commodity, the cultural commodities, the total total amount of such residues shall not amount of such pesticides shall not exceed the highest established toler- yield more residue than that permitted ance for a pesticide having these me- by the larger of the two tolerances, cal- tabolites. culated as a chlorinated terpene of mo- (9) Where a tolerance is established lecular weight 396.6 containing 67 per- for more than one pesticide having as cent chlorine. metabolites compounds containing the (4) Where a tolerance is established benzimidazole moiety found in or on a for more than one pesticide containing raw agricultural commodity, the total arsenic found in, or on a raw agricul- amount of such residues shall not ex- tural commodity, the total amount of ceed the highest established tolerance such pesticide shall not exceed the for a pesticide having these metabo- highest established tolerance cal- lites. culated as As2O3. (10) Where a tolerance is established (5) Where tolerances are established for triclopyr, chloropyrifos, and for more than one member of the class chlorpyrifos-methyl having the com- of dithiocarbamates listed in para- mon metabolite 3,5,6-trichloro-2-

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pyridinol on the same raw agricultural may be determinable shall be deducted commodity, the total amount of such from the total amount of residues residues shall not exceed the highest present and the remainder shall have established tolerance for any of the the same tolerance as that for the pesticides having the metabolites. chemical having the lowest numerical (11) Where tolerances are established tolerance in that class. The quantity of for more than one pesticide having the combined residues that are within the metabolite 3,5,6-trichloro-2-pyridinol tolerance may be determined as fol- found in or on the raw agricultural lows: commodity, the total amount of such (i) Determine the quantity of each residues shall not exceed the highest determinable residue present. established tolerance for a pesticide (ii) Deduct the amounts of such resi- having this metabolite. dues from the total amount of residues (12) Where tolerances are established present and consider the remainder to for residues of methomyl, resulting have the same tolerance as that for the from the use of thiodicarb and/or chemical having the lowest numerical methomyl on the same raw agricul- tolerance in that class. tural commodity, the total amount of (iii) Divide the quantity of each de- methomyl shall not yield more residue terminable residue by the tolerance than that permitted by the higher of that would apply if it occurred alone the two tolerances. and the quantity of the remaining res- (e) Except as noted in paragraphs idue by the tolerance for the chemical (e)(1) and (2) of this section, where resi- having the lowest numerical tolerance dues from two or more chemicals in the in that class and multiply by 100 to de- same class are present in or on a raw termine the percentage of the per- agricultural commodity the tolerance mitted amount of residue present. for the total of such residues shall be (iv) Add the percentages so obtained the same as that for the chemical hav- for all residues present. ing the lowest numerical tolerance in (v) The sum of the percentages shall this class, unless a higher tolerance not exceed 100 percent. level is specifically provided for the (3) The following pesticides are mem- combined residues by a regulation in bers of the class of dithiocarbamates: this part. A mixture of 5.2 parts by weight of ammoni- (1) Where residues from two or more ates of [ethylenebis (dithiocarbamato)] chemicals in the same class are present zinc with 1 part by weight ethylenebis in or on a raw agricultural commodity [dithiocarbamic acid] bimolecular and and there are available methods that trimolecular cyclic anhydrosulfides and permit quantitative determination of disulfides. each residue, the quantity of combined 2-Chloroallyl diethyldithiocarbamate. Coordination product of zinc ion and maneb residues that are within the tolerance containing 20 percent manganese, 2.5 per- may be determined as follows: cent zinc, and 77.5 percent (i) Determine the quantity of each ethylenebisdithiocarbamate. residue present. Ferbam. (ii) Divide the quantity of each res- Maneb. idue by the tolerance that would apply Manganous dimethyldithiocarbamate. if it occurred alone, and multiply by Sodium dimethyldithiocarbamate. Thiram. 100 to determine the percentage of the Zineb. permitted amount of residue present. Ziram. (iii) Add the percentages so obtained for all residues present. (4) The following are members of the (iv) The sum of the percentages shall class of chlorinated organic pesticides: not exceed 100 percent. Aldrin. (2) Where residues from two or more BHC (benzene hexachloride). chemicals in the same class are present 1,1-Bis(p-chlorophenyl)-2,2,2- in or on a raw agricultural commodity trichloroethanol. Chlorbenside (p-chlorobenzyl p-chlorophenyl and there are available methods that sulfide). permit quantitative determinations of Chlordane. one or more, but not all, of the resi- Chlorobenzilate (ethyl 4,4′- dues, the amounts of such residues as dichlorobenzilate).

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p-Chlorophenoxyacetic acid. Carbofuran metabolite (2,3-dihydro-2,2-di- p-Chlorophenyl-2,4,5-trichlorophenyl sulfide. methyl-3-hydroxy-7-benofuranyl N- 2,4-D (2,4-dichlorophenoxyacetic acid). methylcarbamate). DDD (TDE). Carbophenothion (S-[(p-chlorophenyl) DDT. thiolmethyl] O,O-diethyl 1,1-Dichloro-2,2-bis(p-ethylphenyl) ethane. phosphorodithioate) and its cholinesterase- 2,6-Dichloro-4-nitroaniline. inhibiting metabolites. 2,4-Dichlorophenyl p-nitrophenyl ether. Chlorpyrifos (O,O-diethyl O-(3,5,6-trichloro- Dieldrin. 2-pyridyl)phosphorothioate). Dodecachlorooctahydro-1,3,4-metheno-2H- Chlorpyrifos-methyl (O,O-dimethyl-O-(3,5,6- cyclobuta[cd]pentalene. trichloro-2-pyridyl) phosphorothioate. Endosulfan (6,7,8,9,10,10-hexachloro-1,5,5a, 2-Chloro-1-(2,4,5-trichlorophenyl)vinyl di- 6,9,9a-hexahydro-6,9-methano-2,4,3- methyl phosphate. benzodioxathiepin-3-oxide). 2-Chloro-1-(2,4-dichlorophenyl) vinyl diethyl Endosulfan sulfate (6,7,8,9,10,10-hexachloro- phosphate. 1,5,5a,6,9,9a-hexahydro-6,9-methano-2,4,3- Coumaphos (O,O-diethyl O-3-chloro-4-meth- benzodioxathiepin-3,3-dioxide). yl-2-oxo-2H-1-benzopyran-7-yl phosran-7-yl Heptachlor (1,4,5,6,7,8,8-heptachlor-3a,4,7, 7a- phosphate). tetrahydro-4,7-methanoindene). Coumaphos oxygen analog (O,O-diethyl O-3- Heptachlor epoxide (1,4,5,6,7,8,8-heptachloro- chloro-4-methyl-2-oxo-2H-1- 2,3-epoxy-2,3,3a,4,7,7a-hexahydro-4,7- benzopyphorothioate). methanoindene). Dialifor (S-(2-chloro-1-phthalimidoethyl) Hexachlorophene (2,2′-methylenebis(3,4,6- O,O-diethyl phosphorodithioate). trichlorophenol) and its monosodium salt. Dialifor oxygen analog (S-(2-chloro-1- Isopropyl 4,4′-dichlorobenzilate. phthalimidoethyl) O,O-diethyl Lindane. phosphorothioate). Methoxychlor. Demeton (a mixture of O,O-diethyl O-(and S) Ovex (p-chlorophenyl p- [2-ethylthio)ethyl] phosphorothioates). chlorobenzenesulfonate). Ethiolate (S-ethyl diethylthiocarbamate). Sesone (sodium 2,4-dichlorophenoxyethyl 2,2-Dichlorovinyl dimethyl phosphate. sulfate, SES). O,O-Diethyl S-[2-(ethylthio)ethyl] Sodium 2,4-dichlorophenoxyacetate. phosphorodithioate and its cholinesterase- Sodium trichloroacetate. inhibiting metabolites. Sulphenone (p-chlorophenyl phenyl sulfone). O,O-Diethyl O-(2-diethylamino-6-methyl-4- Terpene polychlorinates (chlorinated mix- pyrimidinyl) phosphorothioate and its oxy- ture of camphene, pinene, and related gen analog diethyl 2-diethylamino-6-meth- terpenes 65-66 percent chlorine). yl-4-pyrimidinyl phosphate. 2,3,5,6-Tetrachloronitrobenzene. O,O-Diethyl O-(2-isoprophyl-4-methyl-6- ′ Tetradifon (2,4,5,4 -tetrachlorodiphenyl pyrimidinyl) phosphorothioate. sulfone). O,O-Diethyl O-[p-(methylsulfinyl)phenyl] Toxaphene (chlorinated camphene). phosphorothioate and its cholinesterase-in- Trichlorobenzoic acid. hibiting metabolites. Trichlorobenzyl chloride. Diethyl 2-pyrazinyl phosphate. (5) The following are members of the O,O-Diethyl O-2-pyrazinyl phosphorothioate. class of cholinesterase-inhibiting pes- S-(O,O-Diisopropyl phosphorodithioate) of N- ticides: (2-mercaptoethyl) benzenesulfonamide S-(O,O-Diisopropyl phosphorodithioate) of N- Acephate (O,S-dimethyl acetyl- (2-mercaptoethyl) benzenesulfonamide phosphoramidothioate) and its cholin- 2-(Dimethylamino)-5.6-dimethyl-4- esterase-inhibiting metabolite O,S-di- pyrimidinyl dimethylcarbamate and its methyl phosphoramidothioate. metabolites 5,6-dimethyl-2- Aldicarb (2-methyl-2-(methylthio) (formylmethylamino)-4-pyrimidinyl propionaldehyde O- dimethylcarbamate and 5,6-dimethyl-2- (methylcarbamoyl)oxime) and its (methylamino)-4-pyrimidinyl chlorinesterase-inhibiting metabolites 2- dimethylcarbamate (both calculated as methyl-2-(methylsulfinyl)propionaldehyde parent). O-(methycarbamoyl) oxime and 2-methyl- Dimethoate (O,O-dimethyl S-(N-methyl- 2-(methylsulfonyl)propionaldehyde O- carbamoylmethyl) phosphorodithioate). (methylcarbamoyl)oxime. Dimethoate oxygen analog (O,O-dimethyl S- 4-tert-Butyl-2-chlorophenyl methyl methyl (N-methylcarbamoylmethyl) phosphoramidate. phosphorothioate). S-[(tert-Butylthio)methyl] O,O-diethyl O,O-Dimethyl O-p-(dimethylsulfamoyl) phosphorodithioate and its cholinesterase- phenyl phosphate. inhibiting metabolites. O,O-Dimethyl O-p-(dimethylsulfamoyl) Carbaryl (1-naphthyl N-methylcarbamate). phenyl phosphorothioate. Carbofuran (2,3,-dihydro-2,2-dimethyl-7- 3,5-Dimethyl-4-(methylthio) phenyl benzofuranyl-N-methylcarbamate). methylcarbamate.

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O,O-Dimethyl S-[4-oxo-1,2,3-benzotriazin-3- Phosphamidon (2-chloro-2-diethylcarbamoyl- (4H)-ylmethyl] phosphorodithioate. 1-methylvinyl dimethyl phosphate) includ- Dimethyl phosphate of 3-hydroxy-N,N-di- ing all of its related cholinesterase-inhib- methyl-cis-crotonamide. iting compounds. Dimethyl phosphate of 3-hydroxy-N-methyl- Pirimiphos-methyl O-[2-diethylamino-6- cis-crotonamide. methyl-pyrimidinyl) O,O-dimethyl Dimethyl phosphate of a-methylbenzyl 3-hy- phosphorothioate droxy-cis-crotonate. Ronnel. O,O-Dimethyl 2,2,2-trichloro-1-hydroxyethyl Schradan (octamethylpyrophosphoramide). phosphonate. Tetraethyl pyrophosphate. O,O-Dimethyl phosphorodithioate, S-ester O,O,O′,O′-Tetramethyl O,O′-sulfinyldi-p- with 4-(mercaptomethyl)-2-methozy-D2- phenylene phosphorothioate. 1,3,4-thiadiazolin-5-one. O,O,O′,O′-Tetramethyl O,O′-thiodi-p-phen- Dioxathion (2,3-p-dioxanedithiol S,S-bis (O,O- ylene phosphorothioate. diethylphosphorodithioate)) containing ap- Tributyl phosphorotritlioite. proximately 70 percent cis and trans iso- S,S,S-Tributyl phosphorothrithioate. mers and approximately 30 percent related 3,4,5-Trimethylphenyl methylcarbamate and compounds. its isomer 2,3,5-trimethylphenyl EPN. methylcarbamate. Ethephon ((2- - chloroethyl) phosphonic (6) The following pesticides are mem- acid). bers of the class of dinitrophenols: Ethion. Ethion oxygen analog (S- 2,4-Dinitro-6-octylphenyl crotonate and 2,6- [[(diethoxyphosphinothioyl)thio] methyl] dinitro-4-octylphenyl crotonate, mixture O,O-diethyl phosphorothioate). of. O- Ethyl O-[4-(methylthio) phenyl] S-propyl 4,6-Dinitro-o-cresol and its sodium salt. phosphorodithioate and its cholinesterase- Dinoseb (2-sec-butyl-4,6-dinitrophenol) and inhibiting metabolites. its alkanolamine, ammonium, and sodium O-Ethyl S,S-dipropylphosphorodithioate. salts. Ethyl 3-methyl-4-(methylthio)phenyl (1- [41 FR 8969, Mar. 2, 1976] methylethyl) phosphoramidate and its cholinesterase-inhibiting metabolites. EDITORIAL NOTE: For FEDERAL REGISTER ci- O-Ethyl S-phenyl ethylphosphonodithioate. tations affecting § 180.3, see the List of CFR O-Ethyl S-phenyl ethylphosphonothiolate. Sections Affected, which appears in the m-(1-Ethylpropyl)phenyl methylcarbamate. Finding Aids section of the printed volume and at www.fdsys.gov. S-[2-Ethylsulfinyl)ethyl] O,O-dimethyl phosphorothioate and its cholinesterase-inhibiting metabolites, (primarily S-[2- § 180.4 Exceptions. (ethyl-sulfonyl)ethyl] O,O-dimethyl The substances listed in this section phosphorothioate). are excepted from the definitions of Fenthion (O,O-dimethyl O-[3-methyl-4- ‘‘pesticide chemical’’ and ‘‘pesticide (methylthio)phenyl]phosphorothioate and chemical residue’’ under FFDCA sec- its cholinesterase-inhibiting metabolites. tion 201(q)(3) and are therefore exempt Malathion. from regulation under FFDCA section N-(Mercaptomethyl)phthalimide S-(O,O-dimethyl phosphorodithioate). 402(a)(2)(B) and 408. These substances N-(Mercaptomethyl)phthalimide S-(O,O-di- are subject to regulation by the Food methyl phosphorothioate). and Drug Administration as food addi- Methomyl (S-methyl N- tives under FFDCA section 409. [(methylcarbamoyl)oxy]thioacetimidate). (a) Inert ingredients in food pack- 1-Methoxycarbonyl-1-propen-2-yl dimethyl aging treated with a pesticide, when phosphate and its beta isomer. such inert ingredients are the compo- m-(1-Methylbutyl)phenyl methylcarbamate. nents of the food packaging material Methyl parathion. (e.g. paper and paperboard, coatings, Naled (1,2-dibromo-2,2-dichloroethyl dimethyl phosphate). adhesives, and polymers). Oxamyl (methyl N′,N′-dimethyl-N- (b) [Reserved] [(methylcarbamoyl)oxy]-1- [63 FR 10720, Mar. 4, 1998, as amended at 73 thiooxamimidate) FR 54976, Sept. 24, 2008] Parathion. Phorate (O,O-diethyl S-(ethylthio)methyl § 180.5 Zero tolerances. phosphorodithioate) and its cholinesterase- inhibiting metabolites. A zero tolerance means that no Phosalone (S-(6-chloro-3-mercaptomethyl)-2- amount of the pesticide chemical may benzoxazolinone) O,O-diethyl remain on the raw agricultural com- phosphorodithioate). modity when it is offered for shipment.

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A zero tolerance for a pesticide chem- provided that tolerances can be estab- ical in or on a raw agricultural com- lished at the same time, on the basis of modity may be established because, the toxicological and other data avail- among other reasons: able, for the finite residues incurred in (a) A safe level of the pesticide chem- milk, eggs, meat, and/or poultry. When ical in the diet of two different species it is not possible to determine with cer- of warm-blooded animals has not been tainty whether finite residues will be reliably determined. incurred in milk, eggs, meat, and/or (b) The chemical is carcinogenic to poultry but there is a reasonable expec- or has other alarming physiological ef- tation of finite residues in light of data fects upon one or more of the species of reflecting exaggerated pesticides levels the test animals used, when fed in the in feeding studies, a tolerance will be diet of such animals. established on the raw agricultural (c) The pesticide chemical is toxic, commodity provided that appropriate but is normally used at times when, or tolerances can be established at the in such manner that, fruit, vegetables, same time, on the basis of the toxi- or other raw agricultural commodities cological and other data available, for will not bear or contain it. the finite residues likely to be incurred (d) All residue of the pesticide chem- in these foods through the feed use of ical is normally removed through good the raw agricultural commodity or its agricultural practice such as washing byproducts. When it is not possible to or brushing or through weathering or determine with certainty whether fi- other changes in the chemical itself, nite residues will be incurred in milk, prior to introduction of the raw agri- eggs, meat, and/or poultry but there is cultural commodity into interstate no reasonable expectation of finite res- commerce. idues in light of data such as those reflecting exaggerated pesticide levels in § 180.6 Pesticide tolerances regarding feeding studies and those elucidating milk, eggs, meat, and/or poultry; the biochemistry of the pesticide statement of policy. chemical in the animal, a tolerance (a) When establishing tolerances for may be established on the raw agricul- pesticide residues in or on raw agricultural commodity without the necessity tural commodities, consideration is al- of a tolerance on food products derived ways given to possible residues of those from the animal. pesticide chemicals or their conversion (c) The principles outlined in para- products entering the diet of man graphs (a) and (b) of this section will through the ingestion of milk, eggs, also be followed with respect to toler- meat, and/or poultry produced by ani- ances for residues which will actually mals fed agricultural products bearing be incurred or are reasonably to be ex- such pesticide residues. In each in- pected in milk, eggs, meat, and/or poul- stance an evaluation of all available try by the use of pesticides directly on data will result in a conclusion either: the animal or administered purposely (1) That finite residues will actually in the feed or drinking water. be incurred in these foods from feed use (d) Tolerances contemplated by para- of the raw agricultural commodity in- graphs (a) and (b) of this section will in cluding its byproducts; or addition to toxicological consider- (2) That it is not possible to establish ations be conditioned on the avail- with certainty whether finite residues ability of a practicable analytical will be incurred, but there is a reason- method to determine the pesticide res- able expectation of finite residues; or idue; that is, the method must be sen- (3) That it is not possible to establish sitive and reliable at the tolerance with certainty whether finite residues level or in special cases at a higher will be incurred, but there is no reason- level where such level is deemed satis- able expectation of finite residues. factory and safe in light of the toxicity (b) When the data show that finite of the pesticide residue and of the un- residues will actually be incurred in likelihood of such residue exceeding milk, eggs, meat, and/or poultry, a tol- the tolerance. The analytical methods erance will be established on the raw to be used for enforcement purposes agricultural commodity used as feed will be those set forth in the ‘‘Pesticide

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Analytical Manual’’ (see § 180.101(c)). safety of the pesticide chemical, in- The sensitivities of these methods are cluding full information as to the expressed in that manual. methods and controls used in con- ducting those tests and investigations. Subpart B—Procedural (6) Full reports of tests and inves- Regulations tigations made with respect to the na- ture and amount of the pesticide chem- § 180.7 Petitions proposing tolerances ical residue that is likely to remain in or exemptions for pesticide resi- or on the food, including a description dues in or on raw agricultural com- of the analytical methods used. (See modities or processed foods. § 180.34 for further information about (a) Petitions to be filed with the residue tests.) Agency under the provisions of FFDCA (7) Proposed tolerances for the pes- section 408(d) shall be submitted in du- ticide chemical residue if tolerances plicate. If any part of the material sub- are proposed. mitted is in a foreign language, it shall (8) Practicable methods for removing be accompanied by an accurate and any amount of the residue that would complete English translation. The peti- exceed any proposed tolerance. tion shall be accompanied by an ad- (9) A practical method for detecting vance deposit for fees described in and measuring the levels of the pes- § 180.33. The petition shall state the pe- ticide chemical residue in or on the titioner’s mail address to which notice food, or for exemptions, a statement of objection under FFDCA section why such a method is not needed. 408(g)(2) may be sent. The petition (10) If the petition relates to a toler- must be signed by the petitioner or by ance for a processed food, reports of in- his attorney or agent, or (if a corpora- vestigations conducted using the proc- tion) by an authorized official. essing method(s) used to produce that (b) Petitions shall include the fol- food. lowing information: (11) Such information as the Admin- (1) An informative summary of the istrator may require to make the de- petition and of the data, information, termination under FFDCA section and arguments submitted or cited in 408(b)(2)(C). support of the petition. Both a paper and electronic copy of the summary (12) Such information as the Admin- should be submitted. The electronic istrator may require on whether the copy should be formatted according to pesticide chemical may have an effect the Office of Pesticide Programs’ cur- in humans that is similar to an effect rent standard for electronic data sub- produced by a naturally occurring es- mission as specified at http:// trogen or other endocrine effects. www.epa.gov/pesticides/regulating/reg- (13) Information regarding exposure istering/submissions/index.htm. to the pesticide chemical residue due (2) A statement that the petitioner to any tolerance or exemption already agrees that such summary or any in- granted for such residue. formation it contains may be published (14) Information concerning any max- as a part of the notice of filing of the imum residue level established by the petition to be published under FFDCA Codex Alimentarius Commission for section 408(d)(3) and as a part of a pro- the pesticide chemical residue ad- posed or final regulation issued under dressed in the petition. If a Codex max- FFDCA section 408. imum residue level has been estab- (3) The name, chemical identity, and lished for the pesticide chemical res- composition of the pesticide chemical idue and the petitioner does not pro- residue and of the pesticide chemical pose that this level be adopted, a state- that produces the residue. ment explaining the reasons for this (4) Data showing the recommended departure from the Codex level. amount, frequency, method, and time (15) Such other data and information of application of the pesticide chem- as the Administrator requires by regu- ical. lation to support the petition. (5) Full reports of tests and inves- (16) Reasonable grounds in support of tigations made with respect to the the petition.

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(c) The data specified under para- www.regulations.gov where the full text graphs (b)(1) through (b)(16) of this sec- of the summary required in paragraph tion should be on separate sheets or (b) of this section is located, and refer sets of sheets, suitably identified. If interested parties to this document for such data have already been submitted further information on the petition. with an earlier application, the present The full text of the summary may be petition may incorporate it by ref- omitted from the notice. erence to the earlier one. (g) The Administrator may request a (d) Except as noted in paragraph (e) sample of the pesticide chemical at any of this section, a petition shall not be time while a petition is under consider- accepted for filing if any of the data ation. The Administrator shall specify prescribed by FFDCA section 408(d) are in its request for a sample of the pes- lacking or are not set forth so as to be ticide chemical, a quantity which it readily understood. The availability to deems adequate to permit tests of ana- the public of information provided to, lytical methods used to determine resi- or otherwise obtained by, the Agency dues of the pesticide chemical and of under this part shall be governed by methods proposed by the petitioner for part 2 of this chapter. The Adminis- removing any residues of the chemical trator shall make the full text of the that exceed the tolerance proposed. summary referenced in paragraph (b)(1) (h) The Administrator shall deter- of this section available to the public mine, in accordance with the Act, in the public docket at http:// whether to issue an order that estab- www.regulations.gov no later than pub- lishes, modifies, or revokes a tolerance lication in the FEDERAL REGISTER of regulation (whether or not in accord the notice of the petition filing. with the action proposed by the peti- (e) The Administrator shall notify tioner), whether to publish a proposed the petitioner within 15 days after its tolerance regulation and request public receipt of acceptance or nonacceptance comment thereon under § 180.29, or of a petition, and if not accepted the whether to deny the petition. The Ad- reasons therefor. If petitioner desires, ministrator shall publish in the FED- the petitioner may supplement a defi- ERAL REGISTER such order or proposed cient petition after notification as to regulation. After receiving comments deficiencies. If the petitioner does not on any proposed regulation, the Ad- wish to supplement or explain the peti- ministrator may issue an order that es- tion and requests in writing that it be tablishes, modifies, or revokes a toler- filed as submitted, the petition shall be ance regulation. An order published filed and the petitioner so notified. under this section shall describe briefly (f) A notice of the filing of a petition how to submit objections and requests for a pesticide chemical residue toler- for a hearing under part 178 of this ance that the Administrator deter- chapter. A regulation issued under this mines has met the requirements of section shall be effective on the date of paragraph (b) of this section shall be publication in the FEDERAL REGISTER published in the FEDERAL REGISTER by unless otherwise provided in the regu- the Administrator within 30 days after lation. such determination. The notice shall [70 FR 33360, June 8, 2005, as amended at 73 state the name of the pesticide chem- FR 75600, Dec. 12, 2008] ical residue and the commodities for which a tolerance is sought and an- § 180.8 Withdrawal of petitions with- nounce the availability of a description out prejudice. of the analytical methods available to In some cases the Administrator will the Administrator for the detection notify the petitioner that the petition, and measurement of the pesticide while technically complete, is inad- chemical residue with respect to which equate to justify the establishment of a the petition is filed or shall set forth tolerance or the tolerance requested by the petitioner’s statement of why such petitioner. This may be due to the fact a method is not needed. The notice that the data are not sufficiently clear shall explicitly reference the specific or complete. In such cases, the peti- docket identification number in the tioner may withdraw the petition pend- public docket at http:// ing its clarification or the obtaining of

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additional data. This withdrawal may States Courts of Appeal as to the fol- be without prejudice to a future filing. lowing actions: A deposit for fees as specified in § 180.33 (1) Regulations establishing general shall accompany the resubmission of procedures and requirements under the petition. FFDCA section 408(e)(1)(C). [70 FR 33361, June 8, 2005] (2) Orders issued under FFDCA section 408(f)(1)(C) requiring the submis- § 180.9 Substantive amendments to pe- sion of data. titions. (3) Orders issued under FFDCA sec- After a petition has been filed, the tion 408(g)(2)(C) ruling on objections to petitioner may submit additional in- establishment, modification, or revoca- formation or data in support thereof, tion of a tolerance or exemption under but in such cases the petition will be FFDCA section 408(d)(4), or any regula- given a new filing date. tion that is the subject of such an order. The underlying action here is [70 FR 33361, June 8, 2005] Agency disposition of a petition seeking the establishment, modification, or § 180.29 Establishment, modification, revocation of a tolerance or exemption. and revocation of tolerance on initiative of Administrator. (4) Orders issued under FFDCA section 408(g)(2)(C) ruling on objections to (a) Upon the Administrator’s own ini- the denial of a petition under FFDCA tiative, the Administrator may pro- section 408(d)(4). pose, under FFDCA section 408(e), the (5) Orders issued under FFDCA sec- issuance of a regulation establishing a tion 408(g)(2)(C) ruling on objections to tolerance for a pesticide chemical or the establishment, modification, sus- exempting it from the necessity of a pension, or revocation of a tolerance or tolerance, or a regulation modifying or exemption under FFDCA section revoking an existing tolerance or ex- 408(e)(1)(A) or (e)(1)(B). The underlying emption. action here is the establishment, modi- (b) The Administrator shall provide a fication, suspension, or revocation of a period of not less than 60 days for per- tolerance or exemption upon the initia- sons to comment on the proposed regu- tive of EPA including EPA actions pur- lation, except that a shorter period for suant to FFDCA sections comment may be provided if the Ad- 408(b)(2)(B)(v), 408(b)(2)(E)(ii), ministrator for good cause finds that it 408(d)(4)(C)(ii), 408(l)(4), and 408(q)(1). would be in the public interest to do so and states the reasons for the finding (6) Orders issued under FFDCA sec- in the notice of proposed rulemaking. tion 408(g)(2)(C) ruling on objections to the revocation or modification of a tol- (c) After reviewing any timely com- erance or exemption under FFDCA sec- ments received, the Administrator may tion 408(f)(2) for noncompliance with by order establish, modify, or revoke a requirements for the submission of tolerance regulation, which order and data. regulation shall be published in the (7) Orders issued under FFDCA sec- FEDERAL REGISTER. An order published under this section shall state that per- tion 408(g)(2)(C) ruling on objections to sons may submit objections and re- rules issued under FFDCA sections quests for a hearing in the manner de- 408(n)(3) and 408(d) or (e) regarding described in part 178 of this chapter. terminations pertaining to State authority to establish regulatory limits (d) Any final regulation issued under on pesticide chemical residues. this section shall be effective on the date of publication in the FEDERAL (8) Orders issued under FFDCA sec- REGISTER unless otherwise provided in tion 408(g)(2)(C) ruling on objections to the regulation. orders issued under FFDCA section 408(n)(5)(C) authorizing States to estab- [70 FR 33361, June 8, 2005] lish regulatory limits not identical to certain tolerances or exemptions. § 180.30 Judicial review. (b) Any issue as to which review is or (a) Under FFDCA section 408(h), judi- was obtainable under paragraph (a) of cial review is available in the United this section shall not be the subject of

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judicial review under any other provi- safety standard in FFDCA section sion of law. In part, this means that, 408(b)(2) or (c), as applicable. for the Agency actions subject to the (e) Conditions under which a tem- objection procedure in FFDCA section porary tolerance is established shall in- 408(g)(2), judicial review is not avail- clude: able unless an adversely affected party (1) A limitation on the amount of the exhausts these objection procedures, chemical to be used on the designated and any petition procedures prelimi- crops permitted under the experi- nary thereto. mental permit. [70 FR 33362, June 8, 2005] (2) A limitation for the use of the chemical on the designated crops to § 180.31 Temporary tolerances. bona fide experimental use by qualified persons as indicated in the experi- (a) A temporary tolerance (or exemp- mental permit. tion from a tolerance) established (3) A requirement that the person or under the authority of FFDCA section firm which obtains the experimental 408(r) shall be deemed to be a tolerance permit for which the temporary toler- (or exemption from the requirement of ance is established will immediately a tolerance) for the purposes of FFDCA inform the Environmental Protection section 408(a)(1) or (a)(2) and for the Agency of any reports on findings from purposes of § 180.30. the experimental use that have a bear- (b) A request for a temporary toler- ing on safety. ance or a temporary exemption from a (4) A requirement that the person or tolerance by a person who has obtained firm which obtained the experimental or is seeking an experimental permit permit for which the temporary toler- for a pesticide chemical under the Fed- ance is established will keep records of eral Insecticide, Fungicide, and production, distribution, and perform- Rodenticide Act shall be accompanied ance for a period of 2 years and, on re- by such data as are available on sub- quest, at any reasonable time, make jects outlined in § 180.7(b) and an ad- these records available to any author- vance deposit to cover fees as provided ized officer or employee of the Environ- in § 180.33. mental Protection Agency. (c) To obtain a temporary tolerance, a requestor must comply with the peti- [70 FR 33362, June 8, 2005] tion procedures specified in FFDCA section 408(d) and § 180.7 except as pro- § 180.32 Procedure for modifying and vided in this section. revoking tolerances or exemptions (d) A temporary tolerance or exemp- from tolerances. tion from a tolerance may be issued for (a) The Administrator on his/her own a period designed to allow the orderly initiative may propose the issuance of marketing of the raw agricultural com- a regulation modifying or revoking a modities produced while testing a pes- tolerance for a pesticide chemical res- ticide chemical under an experimental idue on raw agricultural commodities permit issued under authority of the or processed foods or modifying or re- Federal Insecticide, Fungicide, and voking an exemption from tolerance Rodenticide Act if the Administrator for such residue. concludes that the safety standard in (b) Any person may file with the Ad- FFDCA section 408(b)(2) or (c), as appli- ministrator a petition proposing the cable, is met. Subject to the require- issuance of a regulation modifying or ments of FFDCA section 408(e), a tem- revoking a tolerance or exemption porary tolerance or exemption from a from a tolerance for a pesticide chem- tolerance may be revoked if the experi- ical residue. The petition shall furnish mental permit is revoked, or may be reasonable grounds for the action revoked at any time if it develops that sought. Reasonable grounds shall in- the application for a temporary toler- clude an explanation showing wherein ance contains a misstatement of a ma- the person has a substantial interest in terial fact or that new scientific data such tolerance or exemption from tol- or experience with the pesticide chem- erance and an assertion of facts (sup- ical indicates that it does not meet the ported by data if available) showing

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that new uses for the pesticide chem- request to renew or extend such tem- ical have been developed or old uses porary tolerance or temporary exemp- abandoned, that new data are available tion shall be accompanied by a fee of as to toxicity of the chemical, or that $4,600. experience with the application of the (e) A petition or request for a tem- tolerance or exemption from tolerance porary tolerance for a pesticide chem- may justify its modification or revoca- ical which has a tolerance for other tion. Evidence that a person has reg- uses at the same numerical level or a istered or has submitted an application higher numerical level shall be accom- for the registration of a pesticide under panied by a fee of $16,075, plus $1,225 for the Federal Insecticide, Fungicide, and each raw agricultural commodity on Rodenticide Act will be regarded as which the temporary tolerance is evidence that the person has a substantial interest in a tolerance or exemp- sought. tion from the requirement of a toler- (f) Each petition for revocation of a ance for a pesticide chemical that con- tolerance shall be accompanied by a fee sists in whole or in part of the pes- of $10,125. Such fee is not required ticide. New data should be furnished in when, in connection with the change the form specified in § 180.7(b) for sub- sought under this paragraph, a petition mitting petitions, as applicable. is filed for the establishment of new (c) The procedures for completing ac- tolerances to take the place of those tion on an Administrator initiated pro- sought to be revoked and a fee is paid posal or a petition shall be those speci- as required by paragraph (a) of this sec- fied in §§ 180.29 and 180.7, as applicable. tion. [70 FR 33362, June 8, 2005] (g) If a petition or a request is not accepted for processing because it is § 180.33 Fees. technically incomplete, the fee, less (a) Each petition for the establish- $2,025 for handling and initial review, ment of a new tolerance or a tolerance shall be returned. If a petition is with- higher than already established, shall drawn by the petitioner after initial be accompanied by a fee of $80,950, plus processing, but before significant Agen- $2,025 for each raw agricultural com- cy scientific review has begun, the fee, modity more than nine on which the less $2,025 for handling and initial re- establishment of a tolerance is review, shall be returned. If an unaccept- quested, except as provided in para- able or withdrawn petition is resub- graphs (b), (d), and (h) of this section. mitted, it shall be accompanied by the (b) Each petition for the establish- fee that would be required if it were ment of a tolerance at a lower numer- being submitted for the first time. ical level or levels than a tolerance al- (h) Each petition for a crop group tol- ready established for the same pes- erance, regardless of the number of raw ticide chemical, or for the establish- agricultural commodities involved, ment of a tolerance on additional raw shall be accompanied by a fee equal to agricultural commodities at the same the fee required by the analogous cat- numerical level as a tolerance already egory for a single tolerance that is not established for the same pesticide a crop group tolerance, i.e., paragraphs chemical, shall be accompanied by a fee of $18,500 plus $1,225 for each raw (a) through (f) of this section, without agricultural commodity on which a tol- a charge for each commodity where erance is requested. that would otherwise apply. (c) Each petition for an exemption (i) Objections under section 408(d)(5) from the requirement of a tolerance or of the Act shall be accompanied by a repeal of an exemption shall be accom- filing fee of $4,050. panied by a fee of $14,925. (j) The person who files a petition for (d) Each petition or request for a judicial review of an order under sec- temporary tolerance or a temporary tion 408(h) of the Act shall pay the exemption from the requirement of a costs of preparing the record on which tolerance shall be accompanied by a fee the order is based unless the person has of $32,325 except as provided in para- no financial interest in the petition for graph (e) of this section. A petition or judicial review.

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(k) No fee under this section will be (n) This fee schedule will be changed imposed on the Interregional Research annually by the same percentage as the Project Number 4 (IR-4 Program). percent change in the Federal General (l) The Administrator may waive or Schedule (GS) pay scale. In addition, refund part or all of any fee imposed by processing costs and fees will periodi- this section if the Administrator deter- cally be reviewed and changes will be mines in his or her sole discretion that made to the schedule as necessary. such a waiver or refund will promote When automatic adjustments are made the public interest or that payment of based on the GS pay scale, the new fee the fee would work an unreasonable schedule will be published in the FED- hardship on the person on whom the ERAL REGISTER as a final rule to be- fee is imposed. A request for waiver or come effective 30 days or more after refund of a fee shall be submitted to publication, as specified in the rule. the Office of Pesticide Programs’ Docu- When changes are made based on peri- ment Processing Desk at the appro- odic reviews, the changes will be sub- priate address as set forth in 40 CFR ject to public comment. 150.17(a) or (b). A fee of $2,025 shall ac- (o) No fee required by this section company every request for a waiver or shall be levied during the period begin- refund, as specified in paragraph (m) of ning on October 1, 2003, and ending Sep- this section, except that the fee under tember 30, 2008. this paragraph shall not be imposed on [68 FR 24371, May 7, 2003, as amended at 69 any person who has no financial inter- FR 12544, Mar. 17, 2004; 70 FR 33363, June 8, est in any action requested by such 2005; 71 FR 35547, June 21, 2006] person under paragraphs (a) through (j) of this section. The fee for requesting a § 180.34 Tests on the amount of res- waiver or refund shall be refunded if idue remaining. the request is granted. (a) Data in a petition on the amount (m) All deposits and fees required by of residue remaining in or on a raw ag- the regulations in this part shall be ricultural commodity should establish paid by money order, bank draft, or the residue that may remain when the certified check drawn to the order of pesticide chemical is applied according the Environmental Protection Agency. to directions registered under the Fed- All deposits and fees shall be forwarded eral Insecticide, Fungicide, and to the Environmental Protection Agen- Rodenticide Act, or according to direc- cy, Headquarters Accounting Oper- tions contained in an application for ations Branch, Office of Pesticide Pro- registration. These data should estab- grams (Tolerance Fees), P.O. Box lish the residues that may remain 360277M, Pittsburgh, PA 15251. The pay- under conditions most likely to result ments should be specifically labeled in high residues on the commodity. ‘‘Tolerance Petition Fees’’ and should (b) The petition should establish the be accompanied only by a copy of the reliability of the residue data reported letter or petition requesting the toler- in it. Sufficient information should be ance. The actual letter or petition, submitted about the analytical method along with supporting data, shall be to permit competent analysts to apply forwarded within 30 days of payment to it successfully. the Office of Pesticide Programs’ Docu- (c) If the pesticide chemical is ab- ment Processing Desk at the appro- sorbed into a living plant or animal priate address as set forth in 40 CFR when applied (is systemic), residue 150.17(a) or (b). A petition will not be data may be needed on each plant or accepted for processing until the re- animal on which a tolerance or exemp- quired fees have been submitted. A pe- tion is requested. tition for which a waiver of fees has (d) If the pesticide chemical is not been requested will not be accepted for absorbed into the living plant or ani- processing until the fee has been mal when applied (is not systemic), it waived or, if the waiver has been de- may be possible to make a reliable es- nied, the proper fee is submitted after timate of the residues to be expected notice of denial. A request for waiver on each commodity in a group of re- or refund will not be accepted after sci- lated commodities on the basis of less entific review has begun on a petition. data than would be required for each

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commodity in the group, considered hay, fescue, lespedeza, lupines, orchard separately. grass, peanut hay, peavine hay, rye (e) Each of the following groups of grass, soybean hay, sudan grass, tim- crops lists raw agricultural commod- othy, and vetch. ities that are considered to be related (26) Corn forage, sorghum forage. for the purpose of paragraph (d) of this (27) Sugarcane, cane sorghum. section. Commodities not listed in this paragraph are not considered to be re- [36 FR 22540, Nov. 25, 1971, as amended at 39 lated for the purpose of paragraph (d) FR 28286, Aug. 6, 1974; 39 FR 28977, Aug. 13, of this section. 1974; 40 FR 6972, Feb. 18, 1975; 45 FR 82928, Dec. 17, 1980; 48 FR 29860, June 29, 1983; 60 FR (1) Apples, crabapples, pears, quinces. 26635, May 17, 1995; 73 FR 75600, Dec. 12, 2008] (2) Avocados, papayas. (3) Blackberries, boysenberries, § 180.35 Tests for potentiation. dewberries, loganberries, raspberries. (4) Blueberries, currants, goose- Experiments have shown that certain berries, huckleberries. cholinesterase-inhibiting pesticides (5) Cherries, plums, prunes. when fed together to test animals are (6) Oranges, citrus citron, grapefruit, more toxic than the sum of their indi- kumquats, lemons, limes, tangelos, vidual toxicities when fed separately. tangerines. One substance potentiates the toxicity (7) Mangoes, persimmons. of the other. Important toxicological (8) Peaches, apricots, nectarines. interactions also have been observed (9) Beans, peas, soybeans (each in dry between pesticides and other sub- form). stances. Wherever there is reason to (10) Beans, peas, soybeans (each in believe that a pesticide chemical for succulent form). which a tolerance is proposed may (11) Broccoli, brussels sprouts, cauli- interact with other pesticide chemicals flower, kohlrabi. or other substances to which man is ex- (12) Cantaloups, honeydew melons, posed, it may be necessary to require muskmelons, pumpkins, watermelons, special experimental data regarding winter squash. potentiation capacities to evaluate the (13) Carrots, garden beets, sugar safety of the proposed tolerance. This beets, horseradish, parsnips, radishes, necessarily will be determined on a rutabagas, salsify roots, turnips. case-by-case basis. (14) Celery, fennel. (15) Cucumbers, summer squash. § 180.40 Tolerances for crop groups. (16) Lettuce, endive (escarole), Chi- (a) Group or subgroup tolerances may nese cabbage, salsify tops. be established as a result of: (17) Onions, garlic, leeks, shallots (1) A petition from a person who has (green, or in dry bulb form). submitted an application for the reg- (18) Potatoes, Jerusalem-artichokes, sweetpotatoes, yams. istration of a pesticide under the Fed- (19) Spinach, beet tops, collards, dan- eral Insecticide, Fungicide, and delion, kale, mustard greens, parsley, Rodenticide Act. Swiss chard, turnip tops, watercress. (2) On the initiative of the Adminis- (20) Tomatoes, eggplants, peppers, pi- trator. mentos. (3) A petition by an interested per- (21) Pecans, almonds, brazil nuts, son. bush nuts, butternuts, chestnuts, fil- (b) The tables in § 180.41 are to be berts, hazelnuts, hickory nuts, wal- used in conjunction with this section nuts. for the establishment of crop group tol- (22) Field corn, popcorn, sweet corn erances. Each table in § 180.41 lists a (each in grain form). group of raw agricultural commodities (23) Milo, sorghum (each in grain that are considered to be related for form). the purposes of this section. Refer also (24) Wheat, barley, oats, rice, rye to § 180.1(g) for a listing of commodities (each in grain form). for which established tolerances may (25) Alfalfa, Bermuda grass, blue- be applied to certain other related and grass, brome grass, clovers, cowpea similar commodities.

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(c) When there is an established or the group, a group or subgroup toler- proposed tolerance for all of the rep- ance will ordinarily not be established. resentative commodities for a specific In this case individual crop tolerances, group or subgroup of related commod- rather than group tolerances, will nor- ities, a tolerance may be established mally be established. for all commodities in the associated (h) Alternatively, a commodity with group or subgroup. Tolerances may be a residue level significantly higher or established for a crop group or, alter- lower than the other commodities in a natively, tolerances may be established group may be excluded from the group for one or more of the subgroups of a tolerance (e.g., cereal grains, except crop group. corn). In this case an individual toler- (d) The representative crops are ance at the appropriate level for the given as an indication of the minimum unique commodity would be estab- residue chemistry data base acceptable lished, if necessary. The alternative ap- to the Agency for the purposes of es- proach of excluding a commodity with tablishing a group tolerance. The a significantly higher or lower residue Agency may, at its discretion, allow level will not be used to establish a tol- group tolerances when data on suitable erance for a commodity subgroup. Most substitutes for the representative crops subgroups have only two representa- are available (e.g., limes instead of tive commodities; to exclude one such lemons). commodity and its related residue data (e) Since a group tolerance reflects would likely provide insufficient res- maximum residues likely to occur on idue information to support the re- all individual crops within a group, the mainder of the subgroup. Residue data proposed or registered patterns of use from crops additional to those rep- for all crops in the group or subgroup resentative crops in a grouping may be must be similar before a group toler- required for systemic pesticides. ance is established. The pattern of use (i) The commodities included in the consists of the amount of pesticide ap- groups will be updated periodically ei- plied, the number of times applied, the ther at the initiative of the Agency or timing of the first application, the in- at the request of an interested party. terval between applications, and the Persons interested in updating this sec- interval between the last application tion should contact the Registration and harvest. The pattern of use will Division of the Office of Pesticide Pro- also include the type of application; for grams. example, soil or foliar application, or (j) When EPA amends a crop group in application by ground or aerial equip- a manner that expands or contracts the ment. commodities that are covered by the (f) When the crop grouping contains group, EPA will initially retain the commodities or byproducts that are pre-existing as well as the revised crop utilized for animal feed, any needed group in the CFR. The revised crop tolerance or exemption from a toler- group will have the same number as ance for the pesticide in meat, milk, the pre-existing crop group; however, poultry and/or eggs must be established the revised crop group number will be before a tolerance will be granted for followed by a hyphen and the final two the group as a whole. The representa- digits of the year in which it was estab- tive crops include all crops in the lished (e.g., if Crop Group 1 is amended group that could be processed such in 2007, the revised group will be des- that residues may concentrate in proc- ignated as Crop Group 1-07). If the pre- essed food and/or feed. Processing data existing crop group had crop sub- will be required prior to establishment groups, these subgroups will be num- of a group tolerance. Tolerances will bered in a similar fashion in the re- not be granted on a group basis as to vised crop group. The name of the re- processed foods prepared from crops vised crop group will not be changed covered by the group tolerance. from the pre-existing crop group unless (g) If maximum residues (tolerances) the revision so changes the composi- for the representative crops vary by tion of the crop group that the pre-ex- more than a factor of 5 from the max- isting name is no longer accurate. Once imum value observed for any crop in a revised crop group is established,

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EPA will no longer establish tolerances (i) Necessary tolerances for residues result- under the pre-existing crop group. At ing from crop group tolerances include: appropriate times, EPA will amend tol- (A) Tolerances for processed food, including processed animal feed, to the extent erances for crop groups that have been needed under FFDCA section 408(a)(2). superseded by revised crop groups to (B) Tolerances for raw commodities not conform the pre-existing crop group to covered by the crop group tolerance that are the revised crop group. Once all of the derivative of commodities in the group. tolerances for the pre-existing crop (C) Tolerances for meat, milk, or egg prod- group have been updated, the pre-exist- ucts that may contain residues as a result of ing crop group will be removed from livestock’s consumption of animal feed containing pesticide residues to the extent need- the CFR. ed under § 180.6(b). (k) Establishment of a tolerance does (ii) Notwithstanding the foregoing, a toler- not substitute for the additional need ance is not considered necessary for proc- to register the pesticide under a com- essed food, derivative raw commodities, or panion law, the Federal Insecticide, meat, milk, and eggs if the precursor raw Fungicide, and Rodenticide Act. The commodities are grown solely for sale as raw Registration Division of the Office of commodities and are completely segregated from commodities grown for the purpose of Pesticide Programs should be con- producing processed foods, derivative raw tacted concerning procedures for reg- commodities, and commodities, or fractions istration of new uses of a pesticide. thereof, that are used as animal feed. (2) Processed commodity and related raw com- [60 FR 26635, May 17, 1995, as amended at 70 modity crop group tolerances. EPA may estab- FR 33363, June 8, 2005; 72 FR 69155, Dec. 7, lish crop group tolerances for processed com- 2007; 75 FR 56014, Sept. 15, 2010] modities or fractions of commodities (e.g., EFFECTIVE DATE NOTE: At 81 FR 26476, May bran and flour from the Cereal Grains 3, 2016, § 180.40 was amended by revising para- Group), including processed fractions used as graphs (e) and (f), effective July 5, 2016. For animal feed (e.g., pomace from the Pome the convenience of the user, the revised text Fruit Group), produced from crops in the is set forth as follows: crop groups in § 180.41. EPA may establish crop group tolerances for raw commodities § 180.40 Tolerances for crop groups. or fractions of commodities, including fractions used as animal feed, derived from com- * * * * * modities covered by the crop groups in § 180.41 (e.g., aspirated grain dust associated (e) Since a group tolerance reflects max- with the Cereal Grains Group). Crop group imum residues likely to occur on all indi- tolerances on processed foods and derivative vidual crops within a group, the proposed or raw commodities may be based on data on registered patterns of use for all crops in the representative commodities for associated group or subgroup must be similar before a crop group. Paragraphs (c), (d), (e), (g), and group tolerance is established. The pattern (h) of § 180.40 apply to group tolerances au- of use consists of the amount of pesticide ap- thorized by paragraph (f)(2). plied, the number of times applied, the tim- (3) Representative crops. Unless indicated ing of the first application, the interval be- otherwise in §§ 180.40 and 180.41, the processed tween applications, and the interval between food and feed forms of the representative the last application and harvest. The pattern crops for a crop group are considered to be of use will also include the type of applica- representative of the processed food and feed tion; for example, soil or foliar application, forms and any derivative raw commodities or application by ground or aerial equip- not covered by the crop group, that are pro- ment. Additionally, since a group tolerance duced from any of the raw agricultural com- reflects maximum residues likely to occur modities covered by the crop group toler- on all individual foods within a group, food ance. Additionally, unless indicated other- processing practices must be similar for all wise in §§ 180.40 and 180.41, representative crops in the group or subgroup if the proc- commodities for such crop groups are se- essing practice has the potential to result in lected taking into consideration whether residues in a processed commodity at a high- their use as animal feed will result in resi- er concentration than the raw agricultural dues in or on meat, milk, and/or eggs at a commodity. level representative of the residues that (f)(1) General. EPA will not establish a crop would result from use of the other commod- group for a pesticide unless all tolerances ities or byproducts in the crop group as an made necessary by the presence of pesticide animal feed. residues in the crop group commodities have (4) Data. Processing data on representative been issued or are being issued simulta- crops are required prior to establishment of neously with the crop group tolerance. For a group tolerance if the processing of the purposes of paragraph (f)(1): representative commodity has the potential

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to result in residues in a processed com- paya, pawpaw, peanut, persimmon, modity at a higher concentration than in the pineapple, water chestnut, and water- representative commodity. Residue data are cress. required on raw commodities derived from the crops in the crop group tolerance but not (c) Each group is identified by a directly covered by the tolerance. Animal group name and consists of a list of feeding studies with a representative crop representative commodities followed are required if the representative crop is by a list of all commodity members for used as a significant animal feed. the group. If the group includes subgroups, each subgroup lists the sub- * * * * * group name, the representative commodity or commodities, and the mem- § 180.41 Crop group tables. ber commodities for the subgroup. Sub- (a) The tables in this section are to groups, which are a subset of their as- be used in conjunction with § 180.40 to sociated crop group, are established for establish crop group tolerances. some but not all crops groups. (b) Commodities not listed are not (1) Crop Group 1: Root and Tuber considered as included in the groups for Vegetables Group. the purposes of this paragraph, and in- (i) Representative commodities. Carrot, dividual tolerances must be estab- potato, radish, and sugar beet. lished. Miscellaneous commodities in- (ii) Table. The following table 1 lists tentionally not included in any group all the commodities included in Crop include asparagus, avocado, banana, Group 1 and identifies the related crop fig, globe artichoke, hops, mango, pa- subgroups.

TABLE 1—CROP GROUP 1: ROOT AND TUBER VEGETABLES

Related crop Commodities subgroups

Arracacha (Arracacia xanthorrhiza) ...... 1C, 1D Arrowroot (Maranta arundinacea) ...... 1C, 1D Artichoke, Chinese (Stachys affinis) ...... 1C, 1D Artichoke, Jerusalem (Helianthus tuberosus) ...... 1C, 1D Beet, garden (Beta vulgaris) ...... 1A, 1B Beet, sugar (Beta vulgaris) ...... 1A Burdock, edible (Arctium lappa) ...... 1A, 1B Canna, edible (Queensland arrowroot) (Canna indica) ...... 1C, 1D Carrot (Daucus carota) ...... 1A, 1B Cassava, bitter and sweet (Manihot esculenta) ...... 1C, 1D Celeriac (celery root) (Apium graveolens var. rapaceum) ...... 1A, 1B Chayote (root) (Sechium edule) ...... 1C, 1D Chervil, turnip-rooted (Chaerophyllum bulbosum)...... 1A, 1B Chicory (Cichorium intybus) ...... 1A, 1B Chufa (Cyperus esculentus) ...... 1C, 1D Dasheen (taro) (Colocasia esculenta) ...... 1C, 1D Ginger (Zingiber officinale) ...... 1C, 1D Ginseng (Panax quinquefolius) ...... 1A, 1B Horseradish (Armoracia rusticana) ...... 1A, 1B Leren (Calathea allouia) ...... 1C, 1D Parsley, turnip-rooted (Petroselinum crispum var. tuberosum) ...... 1A, 1B Parsnip (Pastinaca sativa) ...... 1A, 1B Potato (Solanum tuberosum) ...... 1C Radish (Raphanus sativus) ...... 1A, 1B Radish, oriental (daikon) (Raphanus sativus subvar. longipinnatus) ...... 1A, 1B Rutabaga (Brassica campestris var. napobrassica) ...... 1A, 1B Salsify (oyster plant) (Tragopogon porrifolius)...... 1A, 1B Salsify, black (Scorzonera hispanica) ...... 1A, 1B Salsify, Spanish (Scolymus hispanicus) ...... 1A, 1B Skirret (Sium sisarum) ...... 1A, 1B Sweet potato (Ipomoea batatas) ...... 1C, 1D Tanier (cocoyam) (Xanthosoma sagittifolium) ...... 1C, 1D Turmeric (Curcuma longa) ...... 1C, 1D Turnip (Brassica rapa var. rapa) ...... 1A, 1B Yam bean (jicama, manoic pea) (Pachyrhizus spp.) ...... 1C, 1D Yam, true (Dioscorea spp.) ...... 1C, 1D

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(iii) Table. The following table 2 iden- commodity(ies) for each subgroup, and tifies the crop subgroups for Crop lists all the commodities included in Group 1, specifies the representative each subgroup.

TABLE 2—CROP GROUP 1 SUBGROUP LISTING

Representative commodities Commodities

Crop Subgroup 1A. Root vegetables subgroup. Carrot, radish, and sugar beet...... Beet, garden; beet, sugar; burdock, edible; carrot; celeriac; chervil, turnip-rooted; chicory; ginseng; horseradish; parsley, turnip-rooted; parsnip; radish; radish, oriental; rutabaga; salsify; salsify, black; salsify, Spanish; skirret; turnip. Crop Subgroup 1B. Root vegetables (except sugar beet) subgroup. Carrot and radish...... Beet, garden; burdock, edible; carrot; celeriac; chervil, turnip-rooted; chicory; ginseng; horseradish; parsley, turnip-rooted; parsnip; radish; radish, oriental; rutabaga; salsify; salsify, black; salsify, Spanish; skirret; turnip. Crop Subgroup 1C. Tuberous and corm vegetables subgroup. Potato...... Arracacha; arrowroot; artichoke, Chinese; artichoke, Jerusalem; canna, edible; cassava, bitter and sweet; chayote (root); chufa; dasheen; ginger; leren; potato; sweet potato; tanier; turmeric; yam bean; yam, true. Crop Subgroup 1D. Tuberous and corm vegetables (except potato) subgroup. Sweet potato...... Arracacha; arrowroot; artichoke, Chinese; artichoke, Jerusalem; canna, edible; cassava, bitter and sweet; chayote (root); chufa; dasheen; ginger; leren; sweet potato; tanier; turmeric; yam bean; yam, true.

(2) Crop Group 2. Leaves of Root and Sweet potato (Ipomoea batatas) Tuber Vegetables (Human Food or Ani- Tanier (cocoyam) (Xanthosoma sagittifolium) mal Feed) Group (Human Food or Ani- Turnip (Brassica rapa var. rapa) mal Feed) Group. Yam, true (Dioscorea spp.) (i) Representative commodities. Turnip (3) Crop Group 3. Bulb Vegetables and garden beet or sugar beet. (Allium spp.) Group. (ii) Commodities. The following is a (i) Representative commodities. Onion, list of all the commodities included in green; and onion, dry bulb. Crop Group 2: (ii) Commodities. The following is a CROP GROUP 2: LEAVES OF ROOT AND TUBER list of all the commodities in Crop VEGETABLES (HUMAN FOOD OR ANIMAL Group 3. FEED) GROUP—COMMODITIES CROP GROUP 3: BULB VEGETABLE (Allium SPP.) Beet, garden (Beta vulgaris) Beet, sugar (Beta vulgaris) GROUP—COMMODITIES Burdock, edible (Arctium lappa) Garlic, bulb (Allium sativum) Carrot (Daucus carota) Garlic, great headed, (elephant) (Allium ampeloprasum var. Cassava, bitter and sweet (Manihot esculenta) ampeloprasum) Celeriac (celery root) (Apium graveolens var. Leek (Allium ampeloprasum, A. porrum, A. tricoccum) Onion, dry bulb and green (Allium cepa, A. fistulosum) rapaceum) Onion, Welsh, (Allium fistulosum) Chervil, turnip-rooted (Chaerophyllum Shallot (Allium cepa var. cepa) bulbosum) Chicory (Cichorium intybus) (4) Crop Group 3-07. Bulb Vegetable Dasheen (taro) (Colocasia esculenta) Group. Parsnip (Pastinaca sativa) (i) Representative Commodities. Onion, Radish (Raphanus sativus) bulb and onion, green. Radish, oriental (daikon) (Raphanus sativus subvar. longipinnatus) (ii) Table. The following Table 1 lists Rutabaga (Brassica campestris var. all the commodities listed in Crop napobrassica) Group 3-07 and identifies the related Salsify, black (Scorzonera hispanica) crop subgroups.

TABLE 1—CROP GROUP 3-07: BULB VEGETABLE GROUP

Commodities Related crop subgroups

Chive, fresh leaves (Allium schoenoprasum L.) ...... 3-07B Chive, Chinese, fresh leaves (Allium tuberosum Rottler ex Spreng) ...... 3-07B

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TABLE 1—CROP GROUP 3-07: BULB VEGETABLE GROUP—Continued

Commodities Related crop subgroups

Daylily, bulb (Hemerocallis fulva (L.) L. var. fulva) ...... 3-07A Elegans hosta (Hosta Sieboldiana (Hook.) Engl) ...... 3-07B Fritillaria, bulb (Fritillaria L. fritillary) ...... 3-07A Fritillaria, leaves (Fritillaria L. fritillary) ...... 3-07B Garlic, bulb (Allium sativum L. var. sativum) (A. sativum Common Garlic Group) ...... 3-07A Garlic, great headed, bulb (Allium ampeloprasum L. var. ampeloprasum) (A. ampeloprasum Great Headed Garlic Group) ...... 3-07A Garlic, Serpent, bulb (Allium sativum var. ophioscorodon or A. sativum Ophioscorodon Group) ...... 3-07A Kurrat (Allium kurrat Schweinf. Ex. K. Krause or A. ampeloprasum Kurrat Group) ...... 3-07B Lady’s leek (Allium cernuum Roth) ...... 3-07B Leek Allium porrum L. (syn: A. ampeloprasum L. var. porrum (L.) J. Gay) (A.ampeloprasum Leek Group) ...... 3-07B Leek, wild (Allium tricoccum Aiton) ...... 3-07B Lily, bulb (Lilium spp. (Lilium Leichtlinii var. maximowiczii, Lilium lancifolium)) ...... 3-07A Onion, Beltsville bunching (Allium x proliferum (Moench) Schrad.) (syn: Allium fistulosum L. x A. cepa L.) ...... 3-07B Onion, bulb (Allium cepa L. var. cepa) (A. cepa Common Onion Group) ...... 3-07A Onion, Chinese, bulb (Allium chinense G. Don.) (syn: A. bakeri Regel) ...... 3-07A Onion, fresh (Allium fistulosum L. var. caespitosum Makino) ...... 3-07B Onion, green (Allium cepa L. var. cepa) (A. cepa Common Onion Group) ...... 3-07B Onion, macrostem (Allium macrostemom Bunge) ...... 3-07B Onion, pearl (Allium porrum var. sectivum or A. ampeloprasum Pearl Onion Group) ...... 3-07A Onion, potato, bulb (Allium cepa L. var. aggregatum G. Don.) (A. cepa Aggregatum Group) ...... 3-07A Onion, tree, tops (Allium x proliferum (Moench) Schrad. ex Willd.) (syn: A. cepa var. proliferum (Moench) Regel; A. cepa L. var. bulbiferum L.H. Bailey; A. cepa L. var. viviparum (Metz.) Alef.) ...... 3-07B Onion, Welsh, tops (Allium fistulosum L.) ...... 3-07B Shallot, bulb (Allium cepa var. aggregatum G. Don.) ...... 3-07A Shallot, fresh leaves (Allium cepa var. aggregatum G. Don.) ...... 3-07B Cultivars, varieties, and/or hybrids of these......

(iii) Table. The following Table 2 commodities for each subgroup and identifies the crop subgroups for Crop lists all the commodities included in Group 3-07, specifies the representative each subgroup.

TABLE 2—CROP GROUP 3-07: SUBGROUP LISTING

Representative commodities Commodities

Crop subgroup 3-07A. Onion, bulb, sub- Daylily, bulb; fritillaria, bulb; garlic, bulb; garlic, great-headed, bulb; garlic, serpent, group. bulb; lily, bulb; onion, bulb; onion, Chinese, bulb; onion, pearl; onion, potato, Onion, bulb...... bulb; shallot, bulb; cultivars, varieties, and/or hybrids of these. Crop subgroup 3-07B. Onion, green, sub- Chive, fresh leaves; chive, Chinese, fresh leaves; elegans hosta; fritillaria, leaves; group. kurrat; lady’s leek; leek; leek, wild; Onion, Beltsville bunching; onion, fresh; Onion, green...... onion, green; onion, macrostem; onion, tree, tops; onion, Welsh, tops; shallot, fresh leaves; cultivars, varieties, and/or hybrids of these.

(5) Crop Group 4. Leafy Vegetables (ii) Table. The following table 1 lists (Except Brassica Vegetables) Group. all the commodities included in Crop (i) Representative commodities. Celery, Group 4 and identifies the related crop head lettuce, leaf lettuce, and spinach subgroups. (Spinacia oleracea).

TABLE 1—CROP GROUP 4: LEAFY VEGETABLES (EXCEPT BRASSICA VEGETABLES) GROUP

Related crop Commodities subgroups

Amaranth (leafy amaranth, Chinese spinach, tampala) (Amaranthus spp.) ...... 4A Arugula (Roquette) (Eruca sativa) ...... 4A Cardoon (Cynara cardunculus) ...... 4B Celery (Apium graveolens var. dulce) ...... 4B Celery, Chinese (Apium graveolens var. secalinum) ...... 4B Celtuce (Lactuca sativa var. angustana) ...... 4B Chervil (Anthriscus cerefolium) ...... 4A Chrysanthemum, edible-leaved (Chrysanthemum coronarium var. coronarium) ...... 4A

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TABLE 1—CROP GROUP 4: LEAFY VEGETABLES (EXCEPT BRASSICA VEGETABLES) GROUP— Continued

Related crop Commodities subgroups

Chrysanthemum, garland (Chrysanthemum coronarium var. spatiosum) ...... 4A Corn salad (Valerianella locusta) ...... 4A Cress, garden (Lepidium sativum) ...... 4A Cress, upland (yellow rocket, winter cress) (Barbarea vulgaris) ...... 4A Dandelion (Taraxacum officinale) ...... 4A Dock (sorrel) (Rumex spp.) ...... 4A Endive (escarole) (Cichorium endivia) ...... 4A Fennel, Florence (finochio) (Foeniculum vulgare Azoricum Group) ...... 4B Lettuce, head and leaf (Lactuca sativa) ...... 4A Orach (Atriplex hortensis) ...... 4A Parsley (Petroselinum crispum) ...... 4A Purslane, garden (Portulaca oleracea) ...... 4A Purslane, winter (Montia perfoliata) ...... 4A Radicchio (red chicory) (Cichorium intybus) ...... 4A Rhubarb (Rheum rhabarbarum) ...... 4B Spinach (Spinacia oleracea) ...... 4A Spinach, New Zealand (Tetragonia tetragonioides, T. expansa) ...... 4A Spinach, vine (Malabar spinach, Indian spinach) (Basella alba) ...... 4A Swiss chard (Beta vulgaris var. cicla) ...... 4B

(iii) Table. The following table 2 iden- commodities for each subgroup, and tifies the crop subgroups for Crop lists all the commodities included in Group 4, specifies the representative each subgroup.

TABLE 2—CROP GROUP 4 SUBGROUP LISTING

Representative commodities Commodities

Crop Subgroup 4A. Leafy greens subgroup. Head lettuce and leaf lettuce, and spinach Amaranth; arugula; chervil; chrysanthemum, edible-leaved; chrysanthemum, (Spinacia oleracea). garland; corn salad; cress, garden; cress, upland; dandelion; dock; endive; lettuce; orach; parsley; purslane, garden; purslane, winter; radicchio (red chicory); spinach; spinach, New Zealand; spinach, vine. Crop Subgroup 4B. Leaf petioles subgroup. Celery...... Cardoon; celery; celery, Chinese; celtuce; fennel, Florence; rhubarb; Swiss chard.

(6) Crop Group 5. Brassica (Cole) Leafy (ii) Table. The following table 1 lists Vegetables Group. all the commodities included in Crop (i) Representative commodities. Broc- Group 5 and identifies the related crop coli or cauliflower; cabbage; and mus- subgroups. tard greens.

TABLE 1—CROP GROUP 5: Brassica (COLE) LEAFY VEGETABLES

Related crop Commodities subgroups

Broccoli (Brassica oleracea var. botrytis) ...... 5A Broccoli, Chinese (gai lon) (Brassica alboglabra) ...... 5A Broccoli raab (rapini) (Brassica campestris) ...... 5B Brussels sprouts (Brassica oleracea var. gemmifera) ...... 5A Cabbage (Brassica oleracea) ...... 5A Cabbage, Chinese (bok choy) (Brassica chinensis) ...... 5B Cabbage, Chinese (napa) (Brassica pekinensis) ...... 5A Cabbage, Chinese mustard (gai choy) (Brassica campestris) ...... 5A Cauliflower (Brassica oleracea var. botrytis) ...... 5A Cavalo broccolo (Brassica oleracea var. botrytis) ...... 5A Collards (Brassica oleracea var. acephala) ...... 5B Kale (Brassica oleracea var. acephala) ...... 5B Kohlrabi (Brassica oleracea var. gongylodes) ...... 5A Mizuna (Brassica rapa Japonica Group) ...... 5B Mustard greens (Brassica juncea) ...... 5B

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TABLE 1—CROP GROUP 5: Brassica (COLE) LEAFY VEGETABLES—Continued

Related crop Commodities subgroups

Mustard spinach (Brassica rapa Perviridis Group) ...... 5B Rape greens (Brassica napus) ...... 5B

(iii) Table. The following table 2 iden- commodity(ies) for each subgroup, and tifies the crop subgroups for Crop lists all the commodities included in Group 5, specifies the representative each subgroup.

TABLE 2—CROP GROUP 5 SUBGROUP LISTING

Representative commodities Commodities

Crop Subgroup 5A. Head and stem Brassica subgroup Broccoli or cauliflower; and cabbage ...... Broccoli; broccoli, Chinese; brussels sprouts; cabbage; cabbage, Chinese (napa); cabbage, Chinese mustard; cauliflower; cavalo broccolo; kohlrabi Crop Subgroup 5B. Leafy Brassica greens subgroup. Mustard greens ...... Broccoli raab; cabbage, Chinese (bok choy); collards; kale; mizuna; mustard greens; mustard spinach; rape greens

(7) Crop Group 6. Legume Vegetables one succulent cultivar and one dried (Succulent or Dried) Group. cultivar); and soybean. (i) Representative commodities. Bean (ii) Table. The following table 1 lists (Phaseolus spp.; one succulent cultivar all the commodities included in Crop and one dried cultivar); pea (Pisum spp.; Group 6 and identifies the related crop subgroups.

TABLE 1—CROP GROUP 6: LEGUME VEGETABLES (SUCCULENT OR DRIED)

Related crop Commodities subgroups

Bean (Lupinus spp.) (includes grain lupin, sweet lupin, white lupin, and white sweet lupin) ...... 6C Bean (Phaseolus spp.) (includes field bean, kidney bean, lima bean, navy bean, pinto bean, runner bean, snap bean, tepary bean, wax bean) ...... 6A, 6B, 6C Bean (Vigna spp.) (includes adzuki bean, asparagus bean, blackeyed pea, catjang, Chinese longbean, cowpea, Crowder pea, moth bean, mung bean, rice bean, southern pea, urd bean, yardlong bean) ...... 6A, 6B, 6C Broad bean (fava bean) (Vicia faba) ...... 6B, 6C Chickpea (garbanzo bean) (Cicer arietinum) ...... 6C Guar (Cyamopsis tetragonoloba) ...... 6C Jackbean (Canavalia ensiformis) ...... 6A Lablab bean (hyacinth bean) (Lablab purpureus) ...... 6C Lentil (Lens esculenta) ...... 6C Pea (Pisum spp.) (includes dwarf pea, edible-pod pea, En glish pea, field pea, garden pea, green pea, snow pea, sugar snap pea) ...... 6A, 6B, 6C Pigeon pea (Cajanus cajan) ...... 6A, 6B, 6C Soybean (Glycine max) ...... N/A Soybean (immature seed) (Glycine max) ...... 6A Sword bean (Canavalia gladiata) ...... 6A

(iii) Table. The following table 2 iden- commodities for each subgroup, and tifies the crop subgroups for Crop lists all the commodities included in Group 6, specifies the representative each subgroup.

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TABLE 2—CROP GROUP 6 SUBGROUP LISTING

Representative commodities Commodities

Crop Subgroup 6A. Edible-podded legume vegetables subgroup. Any one succulent cultivar of edible-podded Bean (Phaseolus spp.) (includes runner bean, snap bean, wax bean); bean bean (Phaseolus spp.) and any one suc- (Vigna spp.) (includes asparagus bean, Chinese longbean, moth bean, culent cultivar of edible-podded pea (Pisum yardlong bean); jackbean; pea (Pisum spp.) (includes dwarf pea, edible-pod spp.).. pea, snow pea, sugar snap pea); pigeon pea; soybean (immature seed); sword bean. Crop Subgroup 6B. Succulent shelled pea and bean subgroup. Any succulent shelled cultivar of bean Bean (Phaseolus spp.) (includes lima bean (green)); broad bean (succulent); (Phaseolus spp.) and garden pea (Pisum bean (Vigna spp.) (includes blackeyed pea, cowpea, southern pea); pea spp.).. (Pisum spp.) (includes English pea, garden pea, green pea); pigeon pea. Crop Subgroup 6C. Dried shelled pea and bean (except soybean) subgroup Any one dried cultivar of bean (Phaseolus Dried cultivars of bean (Lupinus spp.) (includes grain lupin, sweet lupin, white spp.); and any one dried cultivar of pea lupin, and white sweet lupin); (Phaseolus spp.) (includes field bean, kidney (Pisum spp.). bean, lima bean (dry), navy bean, pinto bean; tepary bean; bean (Vigna spp.) (includes adzuki bean, blackeyed pea, catjang, cowpea, Crowder pea, moth bean, mung bean, rice bean, southern pea, urd bean); broad bean (dry); chickpea; guar; lablab bean; lentil; pea (Pisum spp.) (includes field pea); pigeon pea.

(8) Crop Group 7. Foliage of Legume (ii) Table. The following table 1 lists Vegetables Group. the commodities included in Crop (i) Representative commodities. Any Group 7. cultivar of bean (Phaseolus spp.), field pea (Pisum spp.), and soybean.

TABLE 1—CROP GROUP 7: FOLIAGE OF LEGUME VEGETABLES GROUP

Representative commodities Commodities

Any cultivar of bean (Phaseolus spp.) and field Plant parts of any legume vegetable included in the legume vegetables that will pea (Pisum spp.), and soybean (Glycine be used as animal feed. max).

(iii) Table. The following table 2 iden- modities for the subgroup, and lists all tifies the crop subgroup for Crop Group the commodities included in the sub- 7 and specifies the representative com- group.

TABLE 2—CROP GROUP 7 SUBGROUP LISTING

Representative commodities Commodities

Crop Subgroup 7A. Foliage of legume vegetables (except soybeans) subgroup Any cultivar of bean (Phaseolus spp.), and Plant parts of any legume vegetable (except soybeans) included in the legume field pea (Pisum spp.). vegetables group that will be used as animal feed.

(9) Crop Group 8. Fruiting Vegetables CROP GROUP 8: FRUITING VEGETABLES Group. (EXCEPT CUCURBITS)—COMMODITIES (i) Representative commodities. To- Eggplant (Solanum melongena) mato, bell pepper, and one cultivar of Groundcherry (Physalis spp.) non-bell pepper. Pepino (Solanum muricatum) (ii) Commodities. The following is a Pepper (Capsicum spp.) (includes bell pepper, list of all the commodities included in chili pepper, cooking pepper, pimento, Crop Group 8: sweet pepper) Tomatillo (Physalis ixocarpa) Tomato (Lycopersicon esculentum)

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(10) Crop Group 8–10. Fruiting Vege- small tomato; bell pepper and one table Group. cultivar of small nonbell pepper. (i) Representative commodities. To- (ii) Commodities. The following is a mato, standard size, and one cultivar of list of all commodities included in the Crop group 8–10.

TABLE 1—CROP GROUP 8–10: FRUITING VEGETABLE GROUP

Related crop sub- Commodities groups

African eggplant, Solanum macrocarpon L ...... 8–10B, 8–10C Bush tomato, Solanum centrale J.M. Black ...... 8–10A Cocona, Solanum sessiliflorum Dunal ...... 8–10A Currant tomato, Lycopersicon pimpinellifolium L ...... 8–10A Eggplant, Solanum melongena L ...... 8–10B, 8–10C Garden huckleberry, Solanum scabrum Mill ...... 8–10A Goji berry, Lycium barbarum L ...... 8–10A Groundcherry, Physalis alkekengi L., P. grisea (Waterf.) M. Martinez, P. peruviana L., P. pubescens L .. 8–10A Martynia, Proboscidea louisianica (Mill.) Thell ...... 8–10B, 8–10C Naranjilla, Solanum quitoense Lam ...... 8–10A Okra, Abelmoschus esculentus (L.) Moench ...... 8–10B, 8–10C Pea eggplant, Solanum torvum Sw...... 8–10B, 8–10C Pepino, Solanum muricatum Aiton ...... 8–10B, 8–10C Pepper, bell, Capsicum annuum L. var. annuum, Capsicum spp ...... 8–10B Pepper, nonbell, Capsicum chinese Jacq., C. annuum L. var. annuum, C. frutescens L., C. baccatum L., 8–10B, 8–10C C. pubescens Ruiz & Pav., Capsicum spp. Roselle, Hibiscus sabdariffa L ...... 8–10B, 8–10C Scarlet eggplant, Solanum aethiopicum L ...... 8–10B, 8–10C Sunberry, Solanum retroflexum Dunal ...... 8–10A Tomatillo, Physalis philadelphica Lam ...... 8–10A Tomato, Solanum lycopersicum L., Solanum lycopersicum L. var. lycopersicum ...... 8–10A Tree tomato, Solanum betaceum Cav ...... 8–10A Cultivars, varieties and/or hybrids of these ......

(iii) Table. The following Table 2 commodities for each subgroup and identifies the crop subgroups for Crop lists all the commodities included in Group 8–10, specifies the representative each subgroup.

TABLE 2—CROP GROUP 8–10. SUBGROUP LISTING

Representative commodities Commodities

Crop subgroup 8–10A. Tomato subgroup Tomato, standard size, and one cultivar of small tomato ...... Bush tomato; cocona; currant tomato; garden huckleberry; goji berry; groundcherry; naranjilla; sunberry; tomatillo; tomato; tree tomato; cultivars, varieties, and/or hybrids of these. Crop subgroup 8–10B. Pepper/Eggplant subgroup Bell pepper and one cultivar of small nonbell pepper ...... African eggplant; bell pepper; eggplant; Martynia; nonbell pepper; okra; pea eggplant; pepino; roselle; scarlet eggplant; cultivars, varieties, and/or hybrids of these. Crop subgroup 8–10C. Nonbell pepper/Eggplant subgroup One cultivar of small nonbell pepper or one cultivar of small African eggplant; eggplant; martynia; nonbell pepper; okra; pea eggplant. eggplant; pepino; roselle; scarlet eggplant; cultivars, varieties, and/or hybrids of these.

(11) Crop Group 9. Cucurbit Vegeta- (ii) Table. The following table 1 lists bles Group. all the commodities included in Crop (i) Representative commodities. Cucum- Group 9 and identifies the related sub- ber, muskmelon, and summer squash. groups.

TABLE 1—CROP GROUP 9: CUCURBIT VEGETABLES

Related crop Commodities subgroups

Chayote (fruit) (Sechium edule) ...... 9B

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TABLE 1—CROP GROUP 9: CUCURBIT VEGETABLES—Continued

Related crop Commodities subgroups

Chinese waxgourd (Chinese preserving melon) (Benincasa hispida) ...... 9B Citron melon (Citrullus lanatus var. citroides) ...... 9A Cucumber (Cucumis sativus) ...... 9B Gherkin (Cucumis anguria) ...... 9B Gourd, edible (Lagenaria spp.) (includes hyotan, cucuzza); (Luffa acutangula, L. cylindrica) (includes hechima, Chinese okra) ...... 9B Momordica spp. (includes balsam apple, balsam pear, bitter melon, Chinese cucumber) ...... 9B Muskmelon (hybrids and/or cultivars of Cucumis melo) (includes true cantaloupe, cantaloupe, casaba, crenshaw melon, golden pershaw melon, honeydew melon, honey balls, mango melon, Persian melon, pineapple melon, Santa Claus melon, and snake melon) ...... 9A Pumpkin (Cucurbita spp.) ...... 9B Squash, summer (Cucurbita pepo var. melopepo) (includes crookneck squash, scallop squash, straightneck squash, vegetable marrow, zucchini) ...... 9B Squash, winter (Cucurbita maxima; C. moschata) (includes butternut squash, calabaza, hubbard squash); (C. mixta; C. pepo) (includes acorn squash, spaghetti squash) ...... 9B Watermelon (includes hybrids and/or varieties of Citrullus lanatus) ...... 9A

(iii) Table. The following table 2 iden- commodities for each subgroup, and tifies the crop subgroups for Crop lists all the commodities included in Group 9, specifies the representative each subgroup.

TABLE 2—CROP GROUP 9 SUBGROUP LISTING

Representative commodities Commodities

Crop Subgroup 9A. Melon subgroup Cantaloupes ...... Citron melon; muskmelon; watermelon Crop Subgroup 9B. Squash/cucumber subgroup One cultivar of summer squash and cucumber. Chayote (fruit); Chinese waxgourd; cucumber; gherkin; gourd, edible; Momordica spp.; pumpkin; squash, summer; squash, winter.

(12) Crop Group 10. Citrus Fruit Kumquat (Fortunella spp.) Group. Lemon (Citrus jambhiri, Citrus limon) (i) Representative commodities. Sweet Lime (Citrus aurantiifolia) Mandarin (tangerine) (Citrus reticulata) orange; lemon and grapefruit. Orange, sour (Citrus aurantium) (ii) Commodities. The following is a Orange, sweet (Citrus sinensis) list of all the commodities in Crop Pummelo (Citrus grandis, Citrus maxima) Group 10: Satsuma mandarin (Citrus unshiu)

CROP GROUP 10: CITRUS FRUITS (CITRUS SPP., (13) Crop Group 10–10. Citrus Fruit FORTUNELLA SPP.) GROUP—COMMODITIES Group. (i) Representative commodities. Orange Calamondin (Citrus mitis × Citrofortunella mitis) or Tangerine/Mandarin, Lemon or Citrus citron (Citrus medica) Lime, and Grapefruit. Citrus hybrids (Citrus spp.) (includes (ii) Commodities. The following is a chironja, tangelo, tangor) list of all the commodities in Crop Grapefruit (Citrus paradisi) Group 10–10.

TABLE 1—CROP GROUP 10–10: CITRUS FRUIT GROUP

Related crop sub- Commodities groups

Australian desert lime, Eremocitrus glauca (Lindl.) Swingle ...... 10–10B Australian finger lime, Microcitrus australasica (F. Muell.) Swingle ...... 10–10B Australian round lime, Microcitrus australis (A. Cunn. Ex Mudie) Swingle ...... 10–10B Brown River finger lime, Microcitrus papuana Winters ...... 10–10B Calamondin, Citrofortunella microcarpa (Bunge) Wijnands ...... 10–10A Citron, Citrus medica L ...... 10–10A Citrus hybrids, Citrus spp. Eremocitrus spp., Fortunella spp., Microcitrus spp., and Poncirus spp ...... 10–10A Grapefruit, Citrus paradisi Macfad ...... 10–10C

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TABLE 1—CROP GROUP 10–10: CITRUS FRUIT GROUP—Continued

Related crop sub- Commodities groups

Japanese summer grapefruit, Citrus natsudaidai Hayata ...... 10–10C Kumquat, Fortunella spp ...... 10–10B Lemon, Citrus limon (L.) Burm. f ...... 10–10B Lime, Citrus aurantiifolia (Christm.) Swingle ...... 10–10B Mediterranean mandarin, Citrus deliciosa Ten ...... 10–10A Mount White lime, Microcitrus garrowayae (F.M. Bailey) Swingle ...... 10–10B New Guinea wild lime, Microcitrus warburgiana (F.M. Bailey) Tanaka ...... 10–10B Orange, sour, Citrus aurantium L ...... 10–10A Orange, sweet, Citrus sinensis (L.) Osbeck ...... 10–10A Pummelo, Citrus maxima (Burm.) Merr ...... 10–10C Russell River lime, Microcitrus inodora (F.M. Bailey) Swingle ...... 10–10B Satsuma mandarin, Citrus unshiu Marcow ...... 10–10A Sweet lime, Citrus limetta Risso ...... 10–10B Tachibana orange, Citrus tachibana (Makino) Tanaka ...... 10–10A Tahiti lime, Citrus latifolia (Yu. Tanaka) Tanaka ...... 10–10B Tangelo, Citrus xtangelo J.W. Ingram & H.E. Moore ...... 10–10A, 10–10C Tangerine (Mandarin), Citrus reticulata Blanco ...... 10–10A Tangor, Citrus nobilis Lour ...... 10–10A Trifoliate orange, Poncirus trifoliata (L.) Raf ...... 10–10A Uniq fruit, Citrus aurantium Tangelo group ...... 10–10C Cultivars, varieties and/or hybrids of these.

(iii) Table. The following Table 2 tive commodities for each subgroup identifies the crop subgroups for Crop and lists all the commodities included Group 10–10, specifies the representa- in each subgroup.

TABLE 2—CROP GROUP 10–10: SUBGROUP LISTING

Representative commodities Commodities

Crop Subgroup 10–10A. Orange subgroup Orange or tangerine/mandarin ...... Calamondin; citron; citrus hybrids; mediterranean mandarin; orange, sour; orange, sweet; satsuma mandarin; tachibana orange; tangerine (mandarin); tangelo; tangor; trifoliate orange; cultivars, varieties, and/or hybrids of these. Crop Subgroup 10–10B. Lemon/Lime subgroup Lemon or lime ...... Australian desert lime; Australian finger lime; Australian round lime; brown river finger lime; kumquat; lemon; lime; mount white lime; New Guinea wild lime; Russell River lime; sweet lime; Tahiti lime; cultivars , varieties, and/or hybrids of these. Crop Subgroup 10–10C. Grapefruit subgroup Grapefruit ...... Grapefruit; Japanese summer grapefruit; pummelo; tangelo; uniq fruit; cultivars, varieties, and/or hybrids of these.

(14) Crop Group 11: Pome Fruits Quince (Cydonia oblonga) Group. (15) Crop group 11–10. Pome Fruit (i) Representative commodities. Apple Group. and pear. (i) Representative commodities. Apple (ii) Commodities. The following is a and Pear list of all the commodities included in (ii) Commodities. The following is a Crop Group 11: list of all the commodities in Crop CROP GROUP 11: POME FRUITS GROUP— Group 11–10. COMMODITIES CROP GROUP 11–10: POME FRUIT GROUP— Apple (Malus domestica) COMMODITIES Crabapple (Malus spp.) Loquat (Eriobotrya japonica) Apple, Malus domestica Borkh. Mayhaw (Crataegus aestivalis, C. opaca, and C. Azarole, Crataegus azarolus L. rufula) Crabapple, Malus sylvestris (L.) Mill., M. Pear (Pyrus communis) prunifolia (Willd.) Borkh. Pear, oriental (Pyrus pyrifolia) Loquat, Eriobotrya japonica (Thunb.) Lindl.

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Mayhaw, Crataegus aestivalis (Walter) Torr. & CROP GROUP 12: STONE FRUITS GROUP— A. Gray, C. opaca COMMODITIES Hook. & Arn., and C. rufula Sarg. Medlar, Mespilus germanica L. Apricot (Prunus armeniaca) Pear, Pyrus communis L. Cherry, sweet (Prunus avium), Pear, Asian, Pyrus pyrifolia (Burm. f.) Nakai Cherry, tart (Prunus cerasus) var. culta (Makino) Nakai Nectarine (Prunus persica) Pseudocydonia sinensis (Thouin) C.K. Schneid. Peach (Prunus persica) Quince, Cydonia oblonga Mill. Plum (Prunus domestica, Prunus spp.) Quince, Chinese, Chaenomeles speciosa Plum, Chickasaw (Prunus angustifolia) (Sweet) Nakai, Plum, Damson (Prunus domestica spp. Quince, Japanese, Chaenomeles japonica insititia) (Thunb.) Lindl. ex Spach Tejocote, Crataegus mexicana DC. Plum, Japanese (Prunus salicina) Cultivars, varieties and/or hybrids of these. Plumcot (Prunus. armeniaca × P. domestica) Prune (fresh) (Prunus domestica, Prunus spp.) (16) Crop Group 12. Stone Fruits Group. (17) Crop Group 12–12: Stone Fruit (i) Representative commodities. Sweet Group. cherry or tart cherry; peach; and plum (i) Representative commodities. Sweet or fresh prune (Prunus domestica, cherry or Tart cherry; Peach; and Prunus spp.) Plum or Prune plum. (ii) Commodities. The following is a (ii) Commodities. The following Table list of all the commodities included in 1 is a list of all commodities included Crop Group 12: in Crop Group 12–12.

TABLE 1—CROP GROUP 12–12: STONE FRUIT GROUP

Related crop Commodities subgroup

Apricot (Prunus armeniaca L.) ...... 12–12C Apricot, Japanese (Prunus mume Siebold & Zucc.) ...... 12–12C Capulin (Prunus serotina Ehrh. var. salicifolia (Kunth) Koehne) ...... 12–12A Cherry, black (Prunus serotina Ehrh.) ...... 12–12A Cherry, Nanking (Prunus tomentosa Thunb.) ...... 12–12A Cherry, sweet (Prunus avium (L.) L.) ...... 12–12A Cherry, tart (Prunus cerasus L.) ...... 12–12A Jujube, Chinese (Ziziphus jujuba Mill.) ...... 12–12C Nectarine (Prunuspersica (L.) Batsch var. nucipersica (Suckow) C.K. Schneid) ...... 12–12B Peach (Prunus persica (L.) Batsch var. persica) ...... 12–12B Plum (Prunus domestica L. subsp. domestica) ...... 12–12C Plum, American (Prunus americana Marshall) ...... 12–12C Plum, beach (Prunus maritima Marshall) ...... 12–12C Plum, Canada (Prunus nigra Aiton) ...... 12–12C Plum, cherry (Prunus cerasifera Ehrh.) ...... 12–12C Plum, Chickasaw (Prunus angustifolia Marshall) ...... 12–12C Plum, Damson (Prunus domestica L. subsp. insititia (L.) C.K. Schneid.) ...... 12–12C Plum, Japanese (Prunus salicina Lindl.; P. salicina Lindl. var. salicina) ...... 12–12C Plum, Klamath (Prunus subcordata Benth.) ...... 12–12C Plum, prune (Prunus domestica L. subsp. domestica) ...... 12–12C Plumcot (Prunus hybr.) ...... 12–12C Sloe (Prunus spinosa L.) ...... 12–12C Cultivars, varieties, and/or hybrids of these.

(iii) Crop subgroups. The following resentative commodities for each sub- Table 2 identifies the crop subgroups group, and lists all the commodities in- for Crop Group 12–12, specifies the rep- cluded in each subgroup.

TABLE 2—CROP GROUP 12–12: SUBGROUP LISTING

Representative commodities Commodities

Crop subgroup 12–12A. Cherry subgroup

Cherry, sweet or Cherry, tart .... Capulin; Cherry, black; Cherry, Nanking; Cherry, sweet; Cherry, tart; cultivars, varieties, and/or hybrids of these.

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TABLE 2—CROP GROUP 12–12: SUBGROUP LISTING—Continued

Representative commodities Commodities

Crop subgroup 12–12B. Peach subgroup

Peach ...... Peach; Nectarine; cultivars, varieties, and/or hybrids of these.

Crop subgroup 12–12C. Plum subgroup

Plum or Prune plum ...... Apricot; Apricot, Japanese; Jujube, Chinese; Plum; Plum, American; Plum, beach; Plum, Can- ada; Plum, cherry; Plum, Chickasaw; Plum, Damson; Plum, Japanese; Plum, Klamath; Plumcot; Plum, prune; Sloe; cultivars, varieties, and/or hybrids of these.

(18) Crop Group 13. Berries Group. (ii) Table. The following table 1 lists (i) Representative commodities. Any all the commodities included in Crop one blackberry or any one raspberry; Group 13 and identifies the related sub- and blueberry. groups.

TABLE 1—CROP GROUP 13: BERRIES GROUP

Related crop Commodities subgroups

Blackberry (Rubus eubatus) (including bingleberry, black satin berry, boysenberry, Cherokee blackberry, Chesterberry, Cheyenne blackberry, coryberry, darrowberry, dewberry, Dirksen thornless berry, Himalayaberry, hullberry, Lavacaberry, lowberry, Lucretiaberry, mammoth blackberry, marionberry, nectarberry, olallieberry, Oregon evergreen berry, phenomenalberry, rangeberry, ravenberry, rossberry, Shawnee blackberry, youngberry, and varieties and/or hybrids of these) ...... 13A Blueberry (Vaccinium spp.) ...... 13B Currant (Ribes spp.) ...... 13B Elderberry (Sambucus spp.) ...... 13B Gooseberry (Ribes spp.) ...... 13B Huckleberry (Gaylussacia spp.) ...... 13B Loganberry (Rubus loganobaccus) ...... 13A Raspberry, black and red (Rubus occidentalis, Rubus strigosus, Rubus idaeus) ...... 13A

(iii) Table. The following table 2 iden- commodities for each subgroup, and tifies the crop subgroups for Crop lists all the commodities included in Group 13, specifies the representative each subgroup.

TABLE 2—CROP GROUP 13 SUBGROUPS LISTING

Representative commodities Commodities

Crop Subgroup 13A. Caneberry (blackberry and raspberry) subgroup. Any one blackberry or any one raspberry...... Blackberry; loganberry; red and black raspberry; cultivars and/or hybrids of these. Crop Subgroup 13B. Bushberry subgroup.. Blueberry, highbush...... Blueberry, highbush and lowbush; currant; elderberry; gooseberry; huckleberry.

(19) Crop Group 13-07. Berry and Small berry; grape; fuzzy kiwifruit, and Fruit Crop Group strawberry. (i) Representative commodities. Any (ii) Table. The following Table 1 lists one blackberry or any one raspberry; all the commodities listed in Crop highbush blueberry; elderberry or mul- Group 13-07 and identifies the related crop subgroups.

TABLE 1—CROP GROUP 13-07: BERRY AND SMALL FRUIT CROP GROUP

Commodities Related crop subgroups

Amur river grape (Vitis amurensis Rupr) ...... 13-07D, 13-07E, 13-07F Aronia berry (Aronia spp.) ...... 13-07B Bayberry (Myrica spp.) ...... 13-07C

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TABLE 1—CROP GROUP 13-07: BERRY AND SMALL FRUIT CROP GROUP—Continued

Commodities Related crop subgroups

Bearberry (Arctostaphylos uva-ursi) ...... 13-07G, 13-07H Bilberry (Vaccinium myrtillus L.) ...... 13-07G, 13-07H Blackberry (Rubus spp.) (including Andean blackberry, arctic blackberry, bingleberry, black satin berry, boysenberry, brombeere, California blackberry, Chesterberry, Cherokee blackberry, Chey- enne blackberry, common blackberry, coryberry, darrowberry, dewberry, Dirksen thornless berry, evergreen blackberry, Himalayaberry, hullberry, lavacaberry, loganberry, lowberry, Lucretiaberry, mammoth blackberry, marionberry, mora, mures deronce, nectarberry, Northern dewberry, olallieberry, Oregon evergreen berry, phenomenalberry, rangeberry, ravenberry, rossberry, Shaw- nee blackberry, Southern dewberry, tayberry, youngberry, zarzamora, and cultivars, varieties and/or hybrids of these.) ...... 13-07A Blueberry, highbush (Vaccinium spp.) ...... 13-07B Blueberry, lowbush (Vaccinium angustifolium Aiton) ...... 13-07B Buffalo currant (Ribes aureum Pursh) ...... 13-07B Buffaloberry (Shepherdia argentea (Pursh) Nutt.) ...... 13-07C Che (Cudrania tricuspidata Bur. Ex Lavallee) ...... 13-07C Chilean guava (Myrtus ugni Mol.) ...... 13-07B Chokecherry (Prunus virginiana L.) ...... 13-07C Cloudberry (Rubus chamaemorus L.) ...... 13-07G, 13-07H Cranberry (Vaccinium macrocarpon Aiton) ...... 13-07G, 13-07H Currant, black (Ribes nigrum L.) ...... 13-07B Currant, red (Ribes rubrum L.) ...... 13-07B Elderberry (Sambucus spp.) ...... 13-07B, 13-07C European barberry (Berberis vulgaris L.) ...... 13-07B Gooseberry (Ribes spp.) ...... 13-07B, 13-07D, 13- 07E, 13-07F Grape (Vitis spp.) ...... 13-07D, 13-07F Highbush cranberry (Viburnum opulus L. var. Americanum Aiton) ...... 13-07B Honeysuckle, edible (Lonicera caerula L. var. emphyllocalyx Nakai, Lonicera caerula L var . edulis Turcz. ex herder) ...... 13-07B Huckleberry (Gaylussacia spp.) ...... 13-07B Jostaberry (Ribes x nidigrolaria Rud. Bauer and A. Bauer) ...... 13-07B Juneberry (Saskatoon berry) (Amelanchier spp.) ...... 13-07B, 13-07C Kiwifruit, fuzzy (Actinidia deliciosa A. Chev.) (C.F. Liang and A.R. Fergusons, Actinida chinensis Planch.) ...... 13-07D, 13-07E Kiwifruit, hardy (Actinidia arguta (Siebold and Zucc.) Planch. ex Miq) ...... 13-07D, 13-07E, 13-07F Lingonberry (Vaccinium vitis-idaea L.) ...... 13-07B, 13-07G 13-07H Maypop (Passiflora incarnata L.) ...... 13-07E, 13-07F Mountain pepper berries (Tasmannia lanceolata)(Poir.) A.C.Sm...... 13-07C Mulberry (Morus spp.) ...... 13-07C Muntries (Kunzea pomifera F. Muell.) ...... 13-07G, 13-07H Native currant (Acrotriche depressa R. BR.) ...... 13-07B Partridgeberry (Mitchella repens L.) ...... 13-07G, 13-07H Phalsa (Grewia subinaequalis DC.) ...... 13-07C Pincherry (Prunus pensylvanica L.f.) ...... 13-07C Raspberry, black and red (Rubus spp.) ...... 13-07A Riberry (Syzygium luehmannii) ...... 13-07C Salal (Gaultheria shallon Pursh.) ...... 13-07B, 13-07C Schisandra berry (Schisandra chinensis (Turcz.) Baill.) ...... 13-07D, 13-07E, 13-07F Sea buckthorn (Hippophae rhamnoides L.) ...... 13-07B Serviceberry (Sorbus spp.) ...... 13-07C Strawberry (Fragaria x ananassa Duchesne) ...... 13-07G Wild raspberry (Rubus muelleri Lefevre ex P.J. Mull) ...... 13-07A Cultivars, varieties, and/or hybrids of these......

(iii) Table. The following Table 2 tive commodities for each subgroup identifies the crop subgroups for Crop and lists all the commodities included Group 13-07, specifies the representa- in each subgroup.

TABLE 2—CROP GROUP 13-07: SUBGROUP LISTING

Representative commodities Commodities

Crop Subgroup 13-07A. Caneberry subgroup Any one blackberry or any one rasp- Blackberry; loganberry; raspberry, red and black; wild raspberry; cultivars, vari- berry.. eties, and/or hybrids of these. Crop Subgroup 13-07B. Bushberry subgroup.

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TABLE 2—CROP GROUP 13-07: SUBGROUP LISTING—Continued

Representative commodities Commodities

Blueberry, highbush...... Aronia berry; blueberry, highbush; blueberry, lowbush; buffalo currant; Chilean guava; currant, black; currant, red; elderberry; European, barberry; gooseberry; cranberry, highbush; honeysuckle, edible; huckleberry; jostaberry; Juneberry; lingonberry; native currant; salal; sea buckthorn; cultivars, varieties, and/or hybrids of these. Crop Subgroup 13-07C. Large shrub/tree berry subgroup. Elderberry or mulberry...... Bayberry; buffaloberry; che; chokecherry; elderberry; Juneberry; mountain pepper berries; mulberry; phalsa; pincherry; riberry; salal; serviceberry; cultivars, varieties, and/or hybrids of these. Crop Subgroup 13-07D. Small fruit vine climbing subgroup. Grape and fuzzy kiwifruit...... Amur river grape; gooseberry; grape; kiwifruit, fuzzy; kiwifruit, hardy; Maypop; schisandra berry; cultivars, varieties, and /or hybrids of these. Crop Subgroup 13-07E. Small fruit vine climbing subgroup, except grape. Fuzzy kiwifruit...... Amur river grape; gooseberry; kiwifruit, fuzzy; kiwifruit, hardy; Maypop; schisandra berry; cultivars, varieties, and/or hybrids of these. Crop Subgroup 13-07F. Small fruit vine climbing subgroup except fuzzy kiwifruit. Grape...... Amur river grape; gooseberry; grape; kiwifruit, hardy; Maypop; schisandra berry; cultivars varieties, and/or hybrids of these. Crop Subgroup 13-07G. Low growing berry subgroup. Strawberry...... Bearberry; bilberry; blueberry, lowbush; cloudberry; cranberry; lingonberry; muntries; partridgeberry; strawberry; cultivars, varieties, and/or hybrids of these. Crop Subgroup 13-07H. Low growing berry subgroup, except strawberry. Cranberry ...... Bearberry; bilberry; blueberry, lowbush; cloudberry; cranberry; lingonberry; muntries; partridgeberry; cultivars, varieties, and/or cultivars of these.

(20) Crop Group 14. Tree Nuts Group. CROP GROUP 14–12: TREE NUT GROUP (i) Representative commodities. Almond African nut-tree (Ricinodendron heudelotii and pecan. (Baill.) Heckel) (ii) Commodities. The following is a Almond (Prunus dulcis (Mill.) D.A. Webb) list of all the commodities included in Beechnut (Fagus grandifolia Ehrh.; F. Crop Group 14: sylvatica L.) Brazil nut (Bertholletia excelsa Humb. & CROP GROUP 14: TREE NUTS—COMMODITIES Bonpl.) Brazilian pine (Araucaria angustifolia Almond (Prunus dulcis) (Bertol.) Kuntze) Beech nut (Fagus spp.) Bunya (Araucaria bidwillii Hook.) Brazil nut (Bertholletia excelsa) Bur oak (Quercus macrocarpa Michx.) Butternut (Juglans cinerea) Butternut (Juglans cinerea L.) Cashew (Anacardium occidentale) Cajou nut (Anacardium giganteum Hance ex Chestnut (Castanea spp.) Engl.) Chinquapin (Castanea pumila) Candlenut (Aleurites moluccanus (L.) Willd.) Cashew (Anacardium occidentale L.) Filbert (hazelnut) (Corylus spp.) Chestnut (Castanea crenata Siebold & Zucc.; Hickory nut (Carya spp.) C. dentata (Marshall) Borkh.; C. mollissima Macadamia nut (bush nut) (Macadamia spp.) Blume; C. sativa Mill.) Pecan (Carya illinoensis) Chinquapin (Castaneapumila (L.) Mill.) Walnut, black and English (Persian) (Juglans Coconut (Cocos nucifera L.) spp.) Coquito nut (Jubaea chilensis (Molina) Baill.) Dika nut (Irvingia gabonensis (Aubry- (21) Crop Group 14–12. Tree Nut Group. Lecomte ex O’Rorke) Baill.) (i) Representative commodities. Almond Ginkgo (Ginkgo biloba L.) and Pecan. Guiana chestnut (Pachira aquatica Aubl.) (ii) Commodities. The following is a Hazelnut (Filbert) (Corylus americana Mar- list of all commodities included in Crop shall; C. avellana L.; C. californica (A. DC.) Group 14–12. Rose; C. chinensis Franch.) Heartnut (Juglans ailantifolia Carrie`re var. cordiformis (Makino) Rehder)

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Hickory nut (Carya cathayensis Sarg.; C. (i) Representative commodities. Corn, glabra (Mill.) Sweet; C. laciniosa (F. Michx.) wheat, and any other cereal grain crop. W. P. C. Barton; C. myristiciformis (F. (ii) Commodities. The commodities in- Michx.) Elliott; C. ovata (Mill.) K. Koch; C. cluded in Crop Group 16 are: Forage, tomentosa (Lam.) Nutt.) Japanese horse-chestnut (Aesculus turbinate fodder, and straw of all commodities Blume) included in the group cereal grains Macadamia nut (Macadamia integrifolia Maid- group. en & Betche; M. tetraphylla L.A.S. John- (24) Crop Group 17. Grass Forage, Fod- son) der, and Hay Group. Mongongo nut (Schinziophyton rautanenii (i) Representative commodities. Ber- (Schinz) Radcl.-Sm.) muda grass; bluegrass; and bromegrass Monkey-pot (Lecythis pisonis Cambess.) or fescue. Monkey puzzle nut (Araucaria araucana (Molina) K. Koch) (ii) Commodities. The commodities in- Okari nut (Terminalia kaernbachii Warb.) cluded in Crop Group 17 are: Any grass, Pachira nut (Pachira insignis (Sw.) Savigny) Gramineae family (either green or Peach palm nut (Bactris gasipaes Kunth var. cured) except sugarcane and those in- gasipaes) cluded in the cereal grains group, that Pecan (Carya illinoinensis (Wangenh.) K. will be fed to or grazed by livestock, all Koch) pasture and range grasses and grasses Pequi (Caryocar brasiliense Cambess.; C. villosum (Aubl.) Pers; C. nuciferum L.) grown for hay or silage. Pili nut (Canarium ovatum Engl.; C. vulgare (25) Crop Group 18. Nongrass Animal Leenh.) Feeds (Forage, Fodder, Straw, and Pine nut (Pinus edulis Engelm.; P. koraiensis Hay) Group. Siebold & Zucc.; P. sibirica Du Tour; P. (i) Representative commodities. Alfalfa pumila (Pall.) Regel; P. gerardiana Wall. ex and clover (Trifolium spp.) D. Don; P. monophylla Torr. & Fre´m.; P. (ii) Commodities. The following is a quadrifolia Parl. ex Sudw.; P. pinea L.) list of all the commodities included in Pistachio (Pistacia vera L.) Sapucaia nut (Lecythis zabucaja Aubl.) Crop Group 18: Tropical almond (Terminalia catappa L.) CROP GROUP 18: NONGRASS ANIMAL FEEDS Walnut, black (Juglans nigra L.; J. hindsii (FORAGE, FODDER, STRAW, AND HAY) Jeps. ex R. E. Sm.; J. microcarpa Berland.) GROUP—COMMODITIES Walnut, English (Juglans regia L.) Yellowhorn (Xanthoceras sorbifolium Bunge) Alfalfa (Medicago sativa subsp. sativa) Cultivars, varieties, and/or hybrids of these Bean, velvet (Mucuna pruriens var. utilis) (22) Crop Group 15. Cereal Grains Clover (Trifolium spp., Melilotus spp.) Group. Kudzu (Pueraria lobata) Lespedeza (Lespedeza spp.) (i) Representative commodities. Corn Lupin (Lupinus spp.) (fresh sweet corn and dried field corn), Sainfoin (Onobrychis viciifolia); rice, sorghum, and wheat. Trefoil (Lotus spp.) (ii) Commodities. The following is a Vetch (Vicia spp.) list of all the commodities included in Vetch, crown (Coronilla varia) Crop Group 15: Vetch, milk (Astragalus spp). (26) Crop Group 19. Herbs and Spices CROP GROUP 15: CEREAL GRAINS— COMMODITIES Group. (i) Representative commodities. Basil Barley (Hordeum spp.) (fresh and dried); black pepper; chive; Buckwheat (Fagopyrum esculentum) and celery seed or dill seed. Corn (Zea mays) Millet, pearl (Pennisetum glaucum) (ii) Table. The following table 1 lists Millet, proso (Panicum milliaceum) all the commodities included in Crop Oats (Avena spp.) Group 19 and identifies the related sub- Popcorn (Zea mays var. everta) groups. Rice (Oryza sativa) Rye (Secale cereale) TABLE 1—CROP GROUP 19: HERBS AND SPICES Sorghum (milo) (Sorghum spp.) GROUP Teosinte (Euchlaena mexicana) Triticale (Triticum-Secale hybrids) Related Wheat (Triticum spp.) crop Commodities sub- Wild rice (Zizania aquatica) groups

(23) Crop Group 16. Forage, Fodder Allspice (Pimenta dioica) ...... 19B and Straw of Cereal Grains Group. Angelica (Angelica archangelica) ...... 19A

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TABLE 1—CROP GROUP 19: HERBS AND SPICES TABLE 1—CROP GROUP 19: HERBS AND SPICES GROUP—Continued GROUP—Continued

Related Related Commodities crop crop sub- Commodities subgroups groups

Anise (anise seed) (Pimpinella anisum) ...... 19B Lavender (Lavandula officinalis) ...... 19A Anise, star (Illicium verum) ...... 19B Lemongrass (Cymbopogon citratus) ...... 19A Annatto (seed) ...... 19B Lovage (leaf) (Levisticum officinale) ...... 19A Balm (lemon balm) (Melissa officinalis) ...... 19A Lovage (seed) (Levisticum officinale) ...... 19B Basil (Ocimum basilicum) ...... 19A Mace (Myristica fragrans) ...... 19B Borage (Borago officinalis) ...... 19A Marigold (Calendula officinalis) ...... 19A Burnet (Sanguisorba minor) ...... 19A Marjoram (Origanum spp.) (includes sweet or an- Camomile (Anthemis nobilis) ...... 19A nual marjoram, wild marjoram or oregano, and Caper buds (Capparis spinosa) ...... 19B pot marjoram) ...... 19A Caraway (Carum carvi) ...... 19B Mustard (seed) (Brassica juncea, B. hirta, B. nigra) 19B Caraway, black (Nigella sativa) ...... 19B Nasturtium (Tropaeolum majus) ...... 19A Cardamom (Elettaria cardamomum) ...... 19B Nutmeg (Myristica fragrans) ...... 19B Cassia bark (Cinnamomum aromaticum) ...... 19B Parsley (dried) (Petroselinum crispum) ...... 19A Cassia buds (Cinnamomum aromaticum) ...... 19B Catnip (Nepeta cataria) ...... 19A Pennyroyal (Mentha pulegium) ...... 19A Celery seed (Apicum graveolens) ...... 19B Pepper, black (Piper nigrum) ...... 19B Chervil (dried) (Anthriscus cerefolium) ...... 19A Pepper, white ...... 19B Chive (Allium schoenoprasum) ...... 19A Poppy (seed) (Papaver somniferum) ...... 19B Chive, Chinese (Allium tuberosum) ...... 19A Rosemary (Rosemarinus officinalis) ...... 19A Cinnamon (Cinnamomum verum) ...... 19B Rue (Ruta graveolens) ...... 19A Clary (Salvia sclarea) ...... 19A Saffron (Crocus sativus) ...... 19B Clove buds (Eugenia caryophyllata) ...... 19B Sage (Salvia officinalis) ...... 19A Coriander (cilantro or Chinese parsley) (leaf) Savory, summer and winter (Satureja spp.) ...... 19A (Coriandrum sativum) ...... 19A Sweet bay (bay leaf) (Laurus nobilis) ...... 19A Coriander (cilantro) (seed) (Coriandrum sativum) ... 19B Tansy (Tanacetum vulgare) ...... 19A Costmary (Chrysanthemum balsamita) ...... 19A Tarragon (Artemisia dracunculus) ...... 19A Culantro (leaf) (Eryngium foetidum) ...... 19A Thyme (Thymus spp.) ...... 19A Culantro (seed) (Eryngium foetidum) ...... 19B Vanilla (Vanilla planifolia) ...... 19B Cumin (Cuminum cyminum) ...... 19B Wintergreen (Gaultheria procumbens) ...... 19A Curry (leaf) (Murraya koenigii) ...... 19A Woodruff (Galium odorata) ...... 19A Dill (dillweed) (Anethum graveolens) ...... 19A Wormwood (Artemisia absinthium) ...... 19A Dill (seed) (Anethum graveolens) ...... 19B Fennel (common) (Foeniculum vulgare) ...... 19B (iii) Table. The following table 2 iden- Fennel, Florence (seed) (Foeniculum vulgare Azoricum Group) ...... 19B tifies the crop subgroups for Crop Fenugreek (Trigonella foenumgraecum) ...... 19B Group 19, specifies the representative Grains of paradise (Aframomum melegueta) ...... 19B commodities for each subgroup, and Horehound (Marrubium vulgare) ...... 19A Hyssop (Hyssopus officinalis) ...... 19A lists all the commodities included in Juniper berry (Juniperus communis) ...... 19B each subgroup.

TABLE 2—CROP GROUP 19 SUBGROUPS

Representative commodities Commodities

Crop Subgroup 19A. Herb subgroup. Basil (fresh and dried) and chive...... Angelica; balm; basil; borage; burnet; camomile; catnip; chervil (dried); chive; chive, Chinese, clary; coriander (leaf); costmary; culantro (leaf); curry (leaf); dillweed; horehound; hyssop; lavender; lemongrass; lovage (leaf); marigold; marjoram (Origanum spp.); nasturtium; parsley (dried); pennyroyal; rosemary; rue; sage; savory, summer and winter; sweet bay; tansy; tarragon; thyme; wintergreen; woodruff; and wormwood. Crop Subgroup 19B. Spice subgroup. Black pepper; and celery seed or dill seed...... Allspice; anise (seed); anise, star; annatto (seed); caper (buds); caraway; caraway, black; cardamom; cassia (buds); celery (seed); cinnamon; clove (buds); coriander (seed); culantro (seed); cumin; dill (seed); fennel, common; fennel, Florence (seed); fenugreek; grains of paradise; juniper (berry); lovage (seed); mace; mustard (seed); nutmeg; pepper, black; pepper, white; poppy (seed); saffron; and vanilla.

(27) Crop Group 20. Oilseed Group. (ii) Table. The following Table 1 lists (i) Representative commodities. all the commodities listed in Crop Rapeseed (canola varieties only); sun- Group 20 and identifies the related crop flower, seed and cottonseed.

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subgroups and includes cultivars and/or varieties of these commodities.

TABLE 1—CROP GROUP 20: OILSEED GROUP

Related crop Commodities subgroups

Borage, Borago officinalis L ...... 20A Calendula, Calendula officinalis L ...... 20B Castor oil plant, Ricinus communis L ...... 20B Chinese tallowtree, Triadica sebifera (L.) Small ...... 20B Cottonseed, Gossypium hirsutum L. Gossypium spp ...... 20C Crambe, Crambe hispanica L.; C. abyssinica Hochst. ex R.E. Fr ...... 20A Cuphea, Cuphea hyssopifolia Kunth ...... 20A Echium, Echium plantagineum L ...... 20A Euphorbia, Euphorbia esula L ...... 20B Evening primrose, Oenothera biennis L ...... 20B Flax seed, Linum usitatissimum L ...... 20A Gold of pleasure, Camelina sativa (L.) Crantz ...... 20A Hare’s ear mustard, Conringia orientalis (L.) Dumort ...... 20A Jojoba, Simmondsia chinensis (Link) C.K. Schneid ...... 20B Lesquerella, Lesquerella recurvata (Engelm. ex A. Gray) S. Watson ...... 20A Lunaria, Lunaria annua L ...... 20A Meadowfoam, Limnanthes alba Hartw. ex Benth ...... 20A Milkweed, Asclepias spp ...... 20A Mustard seed, Brassica hirta Moench, Sinapis alba L. subsp. Alba...... 20A Niger seed, Guizotia abyssinica (L.f.) Cass ...... 20B Oil radish, Raphanus sativus L. var. oleiformis Pers ...... 20A Poppy seed, Papaver somniferum L. subsp. Somniferum ...... 20A Rapeseed, Brassica spp.; B. napus L ...... 20A Rose hip, Rosa rubiginosa L ...... 20B Safflower, Carthamus tinctorious L ...... 20B Sesame, Sesamum indicum L., S. radiatum Schumach. & honn ...... 20A Stokes aster, Stokesia laevis (Hill) Greene ...... 20B Sunflower, Helianthus annuus L ...... 20B Sweet rocket, Hesperis matronalis L ...... 20A Tallowwood, Ximenia americana L ...... 20B Tea oil plant, Camellia oleifera C. Abel ...... 20B Vernonia, Vernonia galamensis (Cass.) Less ...... 20B Cultivars, varieties, and/or hybrids of these.

(iii) Table. The following Table 2 commodities for each subgroup and identifies the crop subgroups for Crop lists all the commodities included in Group 20, specifies the representative each subgroup.

TABLE 2—CROP GROUP 20: SUBGROUP LISTING

Representative commodities Commodities

Crop subgroup 20A. Rapeseed subgroup Rapeseed, canola varieties only ...... Borage; crambe; cuphea; echium; flax seed; gold of pleasure; hare’s ear mustard; lesquerella; lunaria; meadowfoam; milkweed; mustard seed; oil radish; poppy seed; rapeseed; sesame; sweet rocket cultivars, varieties, and/or hybrids of these. Crop subgroup 20B. Sunflower subgroup Sunflower, seed...... Calendula; castor oil plant; chinese tallowtree; euphorbia; evening primrose; jojoba; niger seed; rose hip; safflower; stokes aster; sunflower; tallowwood; tea oil plant; vernonia; cultivars, varieties, and/or hybrids of these. Crop subgroup 20C. Cottonseed subgroup Cottonseed ...... Cottonseed; cultivars, varieties, and/or hybrids of these.

(28) Crop Group 21. Edible fungi (i) Representative commodities. White Group. button mushroom and any one oyster mushroom or any Shiitake mushroom.

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(ii) Table. The following is a list of all EFFECTIVE DATE NOTE: At 81 FR 26477, May the commodities in Crop Group 21. 3, 2016, § 180.41 was amended by revising para- There are no related subgroups. graph (b); redesignating paragraphs (c)(6) through (28) as paragraphs (c)(7) through (29), respectively; adding a new paragraph (c)(6); CROP GROUP 21—EDIBLE FUNGI GROUP— redesignating newly redesignated paragraphs COMMODITIES (c)(8) through (29) as paragraphs (c)(9) Blewitt (Lepista nuda) through (30), respectively; adding a new Bunashimeji (Hypsizygus marrmoreus) paragraph (c)(8); revising newly redesignated Chinese mushroom (Volvariella volvacea) (Bull.) Singer paragraphs (c)(25)(ii), (c)(26)(ii), and (c)(27)(ii) Enoki (Flammulina velutipes) (Curt.) Singer introductory text; and adding paragraphs Hime-Matsutake (Agaricus blazei) Murill (c)(31), (32), and (33), effective July 5, 2016. Hirmeola (Auricularia auricular) For the convenience of the user, the added Maitake (Grifola frondosa) and revised text is set forth as follows: Morel (Morchella spp.) Nameko (Pholiota nameko) § 180.41 Crop group tables. Net Bearing (Dictyophora) Oyster mushroom (Pleurotus spp.) Pom Pom (Hericium erinaceus) * * * * * Reishi mushroom (Ganoderma lucidum (Leyss. Fr.) Karst.) Rodman’s agaricus (Agaricus bitorquis) (Quel.) Saccardo (b) Commodities not listed are not consid- Shiitake mushroom (Lentinula edodes (Berk.) Pegl.) ered as included in the groups for the pur- Shimeji (Tricholoma conglobatum) poses of paragraph (b), and individual toler- Stropharia (Stropharia spp.) ances must be established. Miscellaneous Truffle (Tuber spp.) commodities intentionally not included in White button mushroom (Agaricus bisporous (Lange) any group include globe artichoke, hops, pea- Imbach) nut, and water chestnut. White Jelly Fungi (Tremella fuciformis) (c) * * * (6) Crop Group 4–16. Leafy Vegetable Group. [60 FR 26635, May 17, 1995, as amended at 72 (i) Representative commodities. Head lettuce, FR 69156, 69157, Dec. 7, 2007; 73 FR 52, Jan. 2, leaf lettuce, mustard greens, and spinach. 2008; 75 FR 76289, Dec. 8, 2010; 77 FR 50620, (ii) Commodities. The following Table 1 lists Aug. 22, 2012] all commodities included in Crop Group 4–16.

TABLE 1—CROP GROUP 4–16: LEAFY VEGETABLE GROUP

Related crop sub- Commodities groups

Amaranth, Chinese (Amaranthus tricolor L.) ...... 4–16A Amaranth, leafy (Amaranthus spp.) ...... 4–16A Arugula (Eruca sativa Mill.) ...... 4–16B Aster, Indian (Kalimeris indica (L.) Sch. Bip.) ...... 4–16A Blackjack (Bidens pilosa L.) ...... 4–16A Broccoli, Chinese (Brassica oleracea var. alboglabra (L.H. Bailey) Musil) ...... 4–16B Broccoli raab (Brassica ruvo L.H. Bailey) ...... 4–16B Cabbage, abyssinian (Brassica carinata A. Braun) ...... 4–16B Cabbage, Chinese, bok choy (Brassica rapa subsp. chinensis (L.) Hanelt) ...... 4–16B Cabbage, seakale (Brassica oleracea L. var. costata DC.) ...... 4–16B Cat’s whiskers (Cleome gynandra L.) ...... 4–16A Cham-chwi (Doellingeria scabra (Thunb.) Nees) ...... 4–16A Cham-na-mul (Pimpinella calycina Maxim) ...... 4–16A Chervil, fresh leaves (Anthriscus cerefolium (L.) Hoffm.) ...... 4–16A Chipilin (Crotalaria longirostrata Hook & Arn) ...... 4–16A Chrysanthemum, garland (Glebionis coronaria (L.) Cass. ex Spach. Glebionis spp.) ...... 4–16A Cilantro, fresh leaves (Coriandrum sativum L.) ...... 4–16A Collards (Brassica oleracea L. var. viridis L.) ...... 4–16B Corn salad (Valerianella spp.) ...... 4–16A Cosmos (Cosmos caudatus Kunth) ...... 4–16A Cress, garden (Lepidium sativum L.) ...... 4–16B Cress, upland (Barbarea vulgaris W.T. Aiton) ...... 4–16B Dandelion, leaves (Taraxacum officinale F.H. Wigg. Aggr.) ...... 4–16A Dang-gwi, leaves (Angelica gigas Nakai) ...... 4–16A Dillweed (Anethum graveolens L.) ...... 4–16A Dock (Rumex patientia L.) ...... 4–16A Dol-nam-mul (Sedum sarmentosum Bunge) ...... 4–16A Ebolo (Crassocephalum crepidioides (Benth.) S. Moore) ...... 4–16A Endive (Cichorium endivia L.) ...... 4–16A Escarole (Cichorium endivia L.) ...... 4–16A Fameflower (Talinum fruticosum (L.) Juss.) ...... 4–16A Feather cockscomb (Glinus oppositifolius (L.) Aug. DC.) ...... 4–16A Good King Henry (Chenopodium bonus-henricus L.) ...... 4–16A Hanover salad (Brassica napus var. pabularia (DC.) Rchb.) ...... 4–16B

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TABLE 1—CROP GROUP 4–16: LEAFY VEGETABLE GROUP—Continued

Related crop sub- Commodities groups

Huauzontle (Chenopodium berlandieri Moq.) ...... 4–16A Jute, leaves (Corchorus spp.) ...... 4–16A Kale (Brassica oleracea L. var. Sabellica L.) ...... 4–16B Lettuce, bitter (Launaea cornuta (Hochst. ex Oliv. & Hiern) C. Jeffrey) ...... 4–16A Lettuce, head (Lactuca sativa L.; including Lactuca sativa var. capitata L.) ...... 4–16A Lettuce, leaf (Lactuca sativa L.; including Lactuca sativa var. longifolia Lam.; Lactuca sativa var. crispa L.) .. 4–16A Maca, leaves (Lepidium meyenii Walp.) ...... 4–16B Mizuna (Brassica rapa L. subsp. nipposinica (L.H. Bailey) Hanelt) ...... 4–16B Mustard greens (Brassica juncea subsp., including Brassica juncea (L.) Czern. subsp. integrifolia (H. West) Thell., Brassica juncea (L.) Czern. var. tsatsai (T.L. Mao) Gladis) ...... 4–16B Orach (Atriplex hortensis L.) ...... 4–16A Parsley, fresh leaves (Petroselinum crispum (Mill.) Fuss; Petroselinum crispum var. neapolitanum Danert) ... 4–16A Plantain, buckthorn (Plantago lanceolata L.) ...... 4–16A Primrose, English (Primula vulgaris Huds.) ...... 4–16A Purslane, garden (Portulaca oleracea L.) ...... 4–16A Purslane, winter (Claytonia perfoliata Donn ex Willd.) ...... 4–16A Radicchio (Cichorium intybus L.) ...... 4–16A Radish, leaves (Raphanus sativus L. var sativus, including Raphanus sativus L. var. mougri H. W. J. Helm (Raphanus sativus L. var. oleiformis Pers) ...... 4–16B Rape greens (Brassica napus L. var. napus, including Brassica rapa subsp. trilocularis (Roxb.) Hanelt; Brassica rapa subsp. dichotoma (Roxb.) Hanelt; Brassica rapa subsp. oleifera Met) ...... 4–16B Rocket, wild (Diplotaxis tenuifolia (L.) DC.) ...... 4–16B Shepherd’s purse (Capsella bursa-pastoris (L.) Medik) ...... 4–16B Spinach (Spinacia oleracea L.) ...... 4–16A Spinach, Malabar (Basella alba L.) ...... 4–16A Spinach, New Zealand (Tetragonia tetragonioides (Pall.) Kuntze) ...... 4–16A Spinach, tanier (Xanthosoma brasiliense (Desf.) Engl.) ...... 4–16A Swiss chard (Beta vulgaris L. ssp. vulgaris) ...... 4–16A Turnip greens (Brassica rapa L. ssp. rapa) ...... 4–16B Violet, Chinese, leaves (Asystasia gangetica (L.) T. Anderson) ...... 4–16A Watercress (Nasturtium officinale W.T. Aiton) ...... 4–16B Cultivars, varieties, and hybrids of these commodities.

(iii) Crop subgroups. The following Table 2 ities for each subgroup, and lists all the com- identifies the crop subgroups for Crop Group modities included in each subgroup. 4–16, specifies the representative commod-

TABLE 2—CROP GROUP 4–16: SUBGROUP LISTING

Representative commodities Commodities

Crop Subgroup 4–16A. Leafy greens subgroup

Head lettuce, leaf lettuce, and spinach ...... Amaranth, Chinese; amaranth, leafy; aster, Indian; blackjack; cat’s whiskers; cham-chwi; cham-na-mul; chervil, fresh leaves; chipilin; chrysanthemum, garland; cilantro, fresh leaves; corn salad; cosmos; dandelion, leaves; dang-gwi, leaves; dillweed; dock; dol-nam-mul; ebolo; endive; escarole; fameflower; feather cockscomb; Good King Henry; huauzontle; jute, leaves; lettuce, bitter; lettuce, head; lettuce, leaf; orach; parsley, fresh leaves; plantain, buckhorn; primrose, English; purslane, garden; purslane, winter; radicchio; spinach; spinach, Malabar; spinach, New Zealand; spinach, tanier; Swiss chard; violet, Chinese, leaves; cultivars, varieties, and hybrids of these commodities.

Crop Subgroup 4–16B. Brassica leafy greens subgroup

Mustard greens ...... Arugula; broccoli, Chinese; broccoli raab; cabbage, abyssinian; cabbage, Chinese, bok choy; cabbage, seakale; collards; cress, garden; cress, upland; hanover salad; kale; maca, leaves; mizuna; mustard greens; radish, leaves; rape greens; rocket, wild; shepherd’s purse; turnip greens; watercress; cultivars, varieties, and hybrids of these commodities.

* * * * * (8) Crop Group 5–16. Brassica Head and Stem Vegetable Group.

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(i) Representative commodities. Broccoli or (26) * * * cauliflower and cabbage. (ii) Commodities. The commodities included (ii) Commodities. The following List 1 con- in Crop Group 17 are: Forage, fodder, stover, tains all commodities included in Crop and hay of any grass, Gramineae/Poaceae fam- Group 5–16. ily (either green or cured) except sugarcane and those included in the cereal grains LIST 1—CROP GROUP 5–16: BRASSICA HEAD group, that will be fed to or grazed by live- AND STEM VEGETABLE GROUP stock, all pasture and range grasses and grasses grown for hay or silage. EPA may es- Commodities tablish separate group tolerances on forage, fodder, stover, or hay, if data on the rep- Broccoli (Brassica oleracea L. var. italica Plenck) Brussels sprouts (Brassica oleracea L. var. gemmifera resentative commodities indicate differences (DC.) Zenker) in the levels of residues on forage, fodder, Cabbage (Brassica oleracea L. var. capitata L.) stover, or hay. Cabbage, Chinese, napa (Brassica rapa L. subsp. (27) * * * pekinensis (Lour.) Hanelt) (ii) Commodities. EPA may establish sepa- Cauliflower (Brassica oleracea L. var. capitata L) rate group tolerances on forage, fodder, Cultivars, varieties, and hybrids of these commodities. straw, or hay, if data on the representative commodities indicate differences in the lev- * * * * * els of residues on forage, fodder, straw, or hay. The following is a list of all the com- (25) * * * modities included in Crop Group 18: (ii) Commodities. The commodities included in Crop Group 16 are: Forage, fodder, stover, * * * * * and straw of all commodities included in the group cereal grains group. EPA may estab- (31) Crop Group 22. Stalk, Stem and Leaf lish separate group tolerances on forage, fod- Petiole Vegetable Group. der, hay, stover, or straw, if data on the rep- (i) Representative commodities. Asparagus resentative commodities indicate differences and celery. in the levels of residues on forage, fodder, (ii) Commodities. The following Table 1 lists stover, or straw. all commodities included in Crop Group 22.

TABLE 1—CROP GROUP 22: STALK, STEM AND LEAF PETIOLE VEGETABLE GROUP

Related crop Commodities subgroups

Agave (Agave spp.) ...... 22A Aloe vera (Aloe vera (L.) Burm.f.) ...... 22A Asparagus (Asparagus officinalis L.) ...... 22A Bamboo, shoots (Arundinaria spp.; Bambusa spp., Chimonobambusa spp.; Dendrocalamus spp., Fargesia spp.; Gigantochloa spp., Nastus elatus; Phyllostachys spp.; Thyrsostachys spp.) ...... 22A Cardoon (Cynara cardunculus L.) ...... 22B Celery (Apium graveolens var. dulce (Mill.) Pers.) ...... 22B Celery, Chinese (Apium graveolens L. var. secalinum (Alef.) Mansf.) ...... 22B Celtuce (Lactuca sativa var. angustana L.H. Bailey) ...... 22A Fennel, Florence, fresh leaves and stalk (Foeniculum vulgare subsp. vulgare var. azoricum (Mill.) Thell.) ...... 22A Fern, edible, fiddlehead ...... 22A Fuki (Petasites japonicus (Siebold & Zucc.) Maxim.) ...... 22B Kale, sea (Crambe maritima L.) ...... 22A Kohlrabi (Brassica oleracea L. var gongylodes L.) ...... 22A Palm hearts (various species) ...... 22A Prickly pear, pads (Opuntia ficus-indica (L.) Mill., Opuntia spp.) ...... 22A Prickly pear, Texas, pads (Opuntia engelmannii Salm-Dyck ex Engelm. var. lindheimeri (Engelm.) B.D. Parfitt & Pinkav) ...... 22A Rhubarb (Rheum x rhabarbarum L.) ...... 22B Udo (Aralia cordata Thunb. ) ...... 22B Zuiki (Colocasia gigantea (Blume) Hook. f.) ...... 22B Cultivars, varieties, and hybrids of these commodities.

(iii) Crop subgroups. The following Table 2 for each subgroup, and lists all the commod- identifies the crop subgroups for Crop Group ities included in each subgroup. 22, specifies the representative commodities

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TABLE 2—CROP GROUP 22: SUBGROUP LISTING

Representative commodities Commodities

Crop Subgroup 22A. Stalk and stem vegetable subgroup

Asparagus ...... Agave; aloe vera; asparagus; bamboo, shoots; celtuce; fennel, florence, fresh leaves and stalk; fern, edible, fiddlehead; kale, sea; kohlrabi; palm hearts; prickly pear, pads; prickly pear, Texas, pads; cultivars, varieties, and hybrids of these commodities.

Crop Subgroup 22B. Leaf petiole vegetable subgroup

Celery ...... Cardoon; celery; celery, Chinese; fuki; rhubarb; udo; zuiki; cultivars, varieties, and hybrids of these commodities.

(32) Crop Group 23. Tropical and Sub- (ii) Commodities. The following Table 1 lists tropical Fruit, Edible Peel Group. all commodities included in Crop Group 23. (i) Representative commodities. Date, fig, guava, and olive.

TABLE 1—CROP GROUP 23: TROPICAL AND SUBTROPICAL FRUIT, EDIBLE PEEL GROUP

Related crop Commodities subgroups

Ac¸aı´ (Euterpe oleracea Mart.) ...... 23C Acerola (Malpighia emarginata DC.) ...... 23A Achachairu´ (Garcinia gardneriana (Planch. & Triana) Zappi) ...... 23B African plum (Vitex doniana Sweet) ...... 23A Agritos (Berberis trifoliolata Moric.) ...... 23A Almondette (Buchanania lanzan Spreng.) ...... 23A Ambarella (Spondias dulcis Sol. ex Parkinson) ...... 23B Apak palm (Brahea dulcis (Kunth) Mart.) ...... 23C Appleberry (Billardiera scandens Sm.) ...... 23A Araza´ (Eugenia stipitata McVaugh) ...... 23B Arbutus berry (Arbutus unedo L.) ...... 23A Babaco (Vasconcellea x heilbornii (V.M. Badillo) V.M. Badillo) ...... 23B Bacaba palm (Oenocarpus bacaba Mart.) ...... 23C Bacaba-de-leque (Oenocarpus distichus Mart.) ...... 23C Bayberry, red (Morella rubra Lour.) ...... 23A Bignay (Antidesma bunius (L.) Spreng.) ...... 23A Bilimbi (Averrhoa bilimbi L.) ...... 23B Borojo´ (Borojoa patinoi Cuatrec.) ...... 23B Breadnut (Brosimum alicastrum Sw.) ...... 23A Cabeluda (Plinia glomerata (O. Berg) Amshoff) ...... 23A Cajou, fruit (Anacardium giganteum Hance ex Engl.) ...... 23B Cambuca´ (Marlierea edulis Nied.) ...... 23B Carandas-plum (Carissa edulis Vahl) ...... 23A Carob (Ceratonia siliqua L.) ...... 23B Cashew apple (Anacardium occidentale L.) ...... 23B Ceylon iron wood (Manilkara hexandra (Roxb.) Dubard) ...... 23A Ceylon olive (Elaeocarpus serratus L.) ...... 23A Cherry-of-the-Rio-Grande (Eugenia aggregata (Vell.) Kiaersk.) ...... 23A Chinese olive, black (Canarium tramdenum C.D. Dai & Yakovlev) ...... 23A Chinese olive, white (Canarium album (Lour.) Raeusch.) ...... 23A Chirauli-nut (Buchanania latifolia Roxb.) ...... 23A Ciruela verde (Bunchosia armeniaca (Cav.) DC.) ...... 23B Cocoplum (Chrysobalanus icaco L.) ...... 23A Date (Phoenix dactylifera L.) ...... 23C Davidson’s plum (Davidsonia pruriens F. Muell.) ...... 23B Desert-date (Balanites aegyptiacus (L.) Delile) ...... 23A Doum palm coconut (Hyphaene thebaica (L.) Mart.) ...... 23C False sandalwood (Ximenia americana L.) ...... 23A Feijoa (Acca sellowiana (O. Berg) Burret) ...... 23B Fig (Ficus carica L.) ...... 23B Fragrant manjack (Cordia dichotoma G. Forst.) ...... 23A Gooseberry, abyssinian (Dovyalis abyssinica (A. Rich.) Warb.) ...... 23A Gooseberry, Ceylon (Dovyalis hebecarpa (Gardner) Warb.) ...... 23A Gooseberry, Indian (Phyllanthus emblica L.) ...... 23B Gooseberry, otaheite (Phyllanthus acidus (L.) Skeels) ...... 23A Governor’s plum (Flacourtia indica (Burm. F.) Merr.) ...... 23A Grumichama (Eugenia brasiliensis Lam) ...... 23A Guabiroba (Campomanesia xanthocarpa O. Berg) ...... 23A

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TABLE 1—CROP GROUP 23: TROPICAL AND SUBTROPICAL FRUIT, EDIBLE PEEL GROUP—Continued

Related crop Commodities subgroups

Guava (Psidium guajava L.) ...... 23B Guava berry (Myrciaria floribunda (H. West ex Willd.) O. Berg) ...... 23A Guava, Brazilian (Psidium guineense Sw.) ...... 23A Guava, cattley (Psidium cattleyanum Sabine) ...... 23B Guava, Costa Rican (Psidium friedrichsthalianum (O. Berg) Nied.) ...... 23A Guava, Para (Psidium acutangulum DC.) ...... 23B Guava, purple strawberry (Psidium cattleyanum Sabine var. cattleyanum) ...... 23B Guava, strawberry (Psidium cattleyanum Sabine var. littorale (Raddi) Fosberg) ...... 23B Guava, yellow strawberry (Psidium cattleyanum Sabine var. cattleyanum forma lucidum O. Deg.) ...... 23B Guayabillo (Psidium sartorianum (O. Berg) Nied.) ...... 23A Illawarra plum (Podocarpus elatus R. Br. Ex Endl.) ...... 23A Imbe´ (Garcinia livingstonei T. Anderson) ...... 23B Imbu (Spondias tuberosa Arruda ex Kost.) ...... 23B Indian-plum (Flacourtia jangomas (Lour.). basionym) ...... 23A Jaboticaba (Myrciaria cauliflora (Mart.) O. Berg) ...... 23B Jamaica-cherry (Muntingia calabura L.) ...... 23A Jambolan (Syzygium cumini (L.) Skeels) ...... 23A Jelly palm (Butia capitata (Mart.) Becc.) ...... 23C Jujube, Indian (Ziziphus mauritiana Lam.) ...... 23B Kaffir-plum (Harpephyllum caffrum Bernh. Ex C. Krauss) ...... 23A Kakadu plum (Terminalia latipes Benth. subsp. psilocarpa Pedley) ...... 23A Kapundung (Baccaurea racemosa (Reinw.) Mull. Arg.) ...... 23A Karanda (Carissa carandas L.) ...... 23A Kwai muk (Artocarpus hypargyreus Hance ex Benth.) ...... 23B Lemon aspen (Acronychia acidula F. Muell) ...... 23A Mangaba (Hancornia speciosa Gomes) ...... 23B Marian plum (Bouea macrophylla Griff.) ...... 23B Mombin, malayan (Spondias pinnata (J. Koenig ex L. f.) Kurz) ...... 23B Mombin, purple (Spondias purpurea L.) ...... 23B Mombin, yellow (Spondias mombin L.) ...... 23A Monkeyfruit (Artocarpus lacucha Buch. Ham.) ...... 23B Monos plum (Pseudanamomis umbellulifera (Kunth) Kausel) ...... 23A Mountain cherry (Bunchosia cornifolia Kunth) ...... 23A Nance (Byrsonima crassifolia (L.) Kunth) ...... 23B Natal plum (Carissa macrocarpa (Eckl.) A. DC.) ...... 23B Noni (Morinda citrifolia L.) ...... 23B Olive (Olea europaea L. subsp. europaea) ...... 23A Papaya, mountain (Vasconcellea pubescens A. DC.) ...... 23B Pataua´ (Oenocarpus bataua Mart.) ...... 23C Peach palm, fruit (Bactris gasipaes Kunth var. gasipaes) ...... 23C Persimmon, black (Diospyros texana Scheele) ...... 23A Persimmon, Japanese (Diospyros kaki Thunb.) ...... 23B Pitomba (Eugenia luschnathiana Klotzsch ex O. Berg) ...... 23A Plum-of-Martinique (Flacourtia inermis Roxb.) ...... 23A Pomerac (Syzygium malaccense (L.) Merr. & L.M. Perry) ...... 23B Rambai (Baccaurea motleyana (Mull. Arg.) Mull. Arg.) ...... 23B Rose apple (Syzygium jambos (L.) Alston) ...... 23B Rukam (Flacourtia rukam Zoll. & Moritizi) ...... 23A Rumberry (Myrciaria dubia (Kunth) McVaugh Myrtaceae) ...... 23A Sea grape (Coccoloba uvifera (L.) L.) ...... 23A Sentul (Sandoricum koetjape (Burm. F.) Merr.) ...... 23B Sete-capotes (Campomanesia guazumifolia (Cambess.) O. Berg) ...... 23A Silver aspen (Acronychia wilcoxian (F. Muell.) T.G. Hartley) ...... 23A Starfruit (Averrhoa carambola L.) ...... 23B Surinam cherry (Eugenia uniflora L.) ...... 23B Tamarind (Tamarindus indica L.) ...... 23B Uvalha (Eugenia pyriformis Cambess ) ...... 23B Water apple (Syzygium aqueum (Burm. F.) Alston) ...... 23A Water pear (Syzygium guineense (Willd.) DC) ...... 23A Water berry (Syzygium cordatum Hochst. Ex C. Krauss) ...... 23A Wax jambu (Syzygium samarangense (Blume) Merr. & L.M. Perry) ...... 23A Cultivars, varieties, and hybrids of these commodities.

(iii) Table. The following Table 2 identifies subgroup, and lists all the commodities in- the crop subgroups for Crop Group 23, speci- cluded in each subgroup. fies the representative commodities for each

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TABLE 2—CROP GROUP 23: SUBGROUP LISTING

Representative commodities Commodities

Crop Subgroup 23A. Tropical and Subtropical, Small fruit, edible peel subgroup

Olive ...... Acerola; African plum; agritos; almondette; appleberry; arbutus berry; bayberry, red; bignay; breadnut; cabeluda; carandas-plum; Ceylon iron wood; Ceylon olive; cherry-of-the-Rio-Grande; Chinese olive, black; Chinese olive, white; chirauli-nut; cocoplum; desert-date; false sandalwood; fragant manjack; gooseberry, abyssinian; gooseberry, Ceylon; gooseberry, otaheite; governor’s plum; grumichama; guabiroba; guava berry; guava, Brazilian; guava, Costa Rican; guayabillo; illawarra plum; Indian-plum; Jamaica-cherry; jambolan; kaffir-plum; kakadu plum; kapundung; karanda; lemon aspen; mombin, yellow; monos plum; mountain cherry; olive; persimmon, black; pitomba; plum-of-Martinique; rukam; rumberry; sea grape; sete-capotes; silver aspen; water apple; water pear; water berry; wax jambu; cultivars, varieties, and hybrids of these commodities.

Crop Subgroup 23B. Tropical and Subtropical, Medium to large fruit, edible peel subgroup

Fig and guava ...... Achachairu´; ambarella; araza´; babaco; bilimbi; borojo´; cajou, fruit; cambuca´; carob; cashew apple; ciruela verde; davidson’s plum; feijoa; fig; gooseberry, Indian; guava; guava, cattley; guava, Para; guava, purple strawberry; guava, strawberry; guava, yellow strawberry; imbe´; imbu; jaboticaba; jujube, Indian; kwai muk; mangaba; Marian plum; mombin, Malayan; mombin, purple; monkeyfruit; nance; natal plum; noni; papaya, mountain; persimmon, Japanese; pomerac; rambai; rose apple; sentul; starfruit; Surinam cherry; tamarind; uvalha; cultivars, varieties, and hybrids of these commodities.

Crop Subgroup 23C. Tropical and Subtropical, Palm fruit, edible peel subgroup

Date ...... Ac¸aı´; apak palm; bacaba palm; bacaba-de-leque; date; doum palm coconut; jelly palm; pataua´; peach palm, fruit; cultivars, varieties, and hybrids of these commodities.

(33) Crop Group 24. Tropical and Sub- granate, dragon fruit, lychee, passionfruit, tropical Fruit, Inedible Peel Group. pineapple, and prickly pear, fruit. (i) Representative commodities. Atemoya or (ii) Commodities. The following Table 1 lists sugar apple, avocado, banana or pome- all commodities included in Crop Group 24.

TABLE 1—CROP GROUP 24: TROPICAL AND SUBTROPICAL FRUIT, INEDIBLE PEEL GROUP

Related crop Commodities subgroups

Abiu (Pouteria caimito (Ruiz & Pav.) Radlk) ...... 24B Aisen (Boscia senegalensis (Pers.) Lam.) ...... 24A Akee apple (Blighia sapida K.D. Koenig) ...... 24B Atemoya (Annona cherimola Mill. X A. squamosa L.) ...... 24C Avocado (Persea americana Mill.) ...... 24B Avocado, Guatemalan (Persea americana Mill. var. guatemalensis) ...... 24B Avocado, Mexican (Persea americana Mill. var. drymifolia (Schltdl. & Cham.) S.F. Blak) ...... 24B Avocado, West Indian (Persea americana var. americana) ...... 24B Bacury (Platonia insignis Mart.) ...... 24B Bael fruit (Aegle marmelos (L.) Correˆa) ...... 24A Banana (Musa spp.) ...... 24B Banana, dwarf (Musa hybrids; Musa acuminata Colla) ...... 24B Binjai (Mangifera caesia Jack) ...... 24B Biriba (Annona mucosa Jacq.) ...... 24C Breadfruit (Artocarpus altilis (Parkinson) Fosberg) ...... 24C Burmese grape (Baccaurea ramiflora Lour.) ...... 24A Canistel (Pouteria campechiana (Kunth) Baehni) ...... 24B Cat’s-eyes (Dimocarpus longan Lour. subsp. malesianus Leenh.) ...... 24A Champedak (Artocarpus integer (Thunb.) Merr.) ...... 24C Cherimoya (Annona cherimola Mill.) ...... 24C Cupuacu´ (Theobroma grandiflorum (Willd. Ex Spreng.) K. Schum.) ...... 24B Custard apple (Annona reticulata L.) ...... 24C Dragon fruit (Hylocereus undatus (Haw.) Britton & Rose) ...... 24D Durian (Durio zibethinus L.) ...... 24C Elephant-apple (Limonia acidissima L.) ...... 24C Etambe (Mangifera zeylanica (Blume) Hook. F.) ...... 24B

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TABLE 1—CROP GROUP 24: TROPICAL AND SUBTROPICAL FRUIT, INEDIBLE PEEL GROUP—Continued

Related crop Commodities subgroups

Granadilla (Passiflora ligularis Juss.) ...... 24E Granadilla, giant (Passiflora quadrangularis L.) ...... 24E Ilama (Annona macroprophyllata Donn. Sm.) ...... 24C Inga´ (Inga vera Willd. subsp. affinis (DC.) T.D. Penn.) ...... 24A Jackfruit (Artocarpus heterophyllus Lam.) ...... 24C Jatoba´ (Hymenaea courbaril L.) ...... 24B Karuka (Pandanus julianettii Martelli) ...... 24C Kei apple (Dovyalis caffra (Hook. F. & Harv.) Warb.) ...... 24B Langsat (Lansium domesticum Correˆa) ...... 24B Lanjut (Mangifera lagenifera Griff.) ...... 24B Longan (Dimocarpus longan Lour.) ...... 24A Lucuma (Pouteria lucuma (Ruiz & Pav.) Kuntze) ...... 24B Lychee (Litchi chinensis Sonn.) ...... 24A Mabolo (Diospyros blancoi A. DC.) ...... 24B Madras-thorn (Pithecellobium dulce (Roxb.) Benth.) ...... 24A Mammy-apple (Mammea americana L.) ...... 24C Manduro (Balanites maughamii Sprague) ...... 24A Mango (Mangifera indica L.) ...... 24B Mango, horse (Mangifera foetida Lour.) ...... 24B Mango, Saipan (Mangifera odorata Griff.) ...... 24B Mangosteen (Garcinia mangostana L. ) ...... 24B Marang (Artocarpus odoratissimus Blanco) ...... 24C Marmaladebox (Genipa americana L.) ...... 24C Matisia (Matisia cordata Humb. & Bonpl.) ...... 24A Mesquite (Prosopis juliflora (Sw.) DC.) ...... 24A Mongongo, fruit (Schinziophyton rautanenii (Schinz) Radcl.-Sm) ...... 24A Monkey-bread-tree (Adansonia digitata L.) ...... 24C Monstera (Monstera deliciosa Liebm.) ...... 24E Nicobar-breadfruit (Pandanus leram Jones ex Fontana) ...... 24C Paho (Mangifera altissima Blanco) ...... 24B Pandanus (Pandanus utilis Bory) ...... 24C Papaya (Carica papaya L.) ...... 24B Passionflower, winged-stem (Passiflora alata Curtis) ...... 24E Passionfruit (Passiflora edulis Sims) ...... 24E Passionfruit, banana (Passiflora tripartita var. mollissima (Kunth) Holm-Niels. & P. Jorg.) ...... 24E Passionfruit, purple (Passiflora edulis Sims forma edulis) ...... 24E Passionfruit, yellow (Passiflora edulis Sims forma flavicarpa O. Deg.) ...... 24E Pawpaw, common (Asimina triloba (L.) Dunal) ...... 24B Pawpaw, small-flower (Asimina parviflora (Michx.) Dunal) ...... 24A Pelipisan (Mangifera casturi Kosterm.) ...... 24B Pequi (Caryocar brasiliense Cambess) ...... 24B Pequia (Caryocar villosum (Aubl.) Pers.) ...... 24B Persimmon, American (Diospyros virginiana L.) ...... 24B Pineapple (Ananas comosus (L.) Merr.) ...... 24C Pitahaya (Hylocereus polyrhizus (F.A.C. Weber) Britton & Rose) ...... 24D Pitaya (Hylocereus sp. including H. megalanthus (H. ocamponis and H. polychizus) ...... 24D Pitaya, amarilla (Hylocereus triangularis Britton & Rose) ...... 24D Pitaya, roja (Hylocereus ocamponis (Salm-Dyck) Britton & Rose) ...... 24D Pitaya, yellow (Hylocereus megalanthus (K. Schum. ex Vaupel) Ralf Bauer) ...... 24D Plantain (Musa paradisiaca L.) ...... 24B Pomegranate (Punica granatum L.) ...... 24B Poshte (Annona liebmanniana Baill.) ...... 24B Prickly pear, fruit (Opuntia ficus-indica (L.) Mill.) ...... 24D Prickly pear, Texas, fruit (Opuntia engelmannii Salm-Dyck ex Engelm. var. lindheimeri (Engelm.) B.D. Parfitt & Pinkav) ...... 24D Pulasan (Nephelium ramboutan-ake (Labill.) Leenh.) ...... 24C Quandong (Santalum acuminatum (R. Br.) DC.) ...... 24B Rambutan (Nephelium lappaceum L.) ...... 24C Saguaro (Carnegiea gigantea (Engelm.) Britton & Rose) ...... 24D Sapodilla (Manilkara zapota (L.) P. Royen) ...... 24C Sapote, black (Diospyros digyna Jacq.) ...... 24B Sapote, green (Pouteria viridis (Pittier) Cronquist) ...... 24B Sapote, mamey (Pouteria sapota (Jacq.) H.E. Moore & Stearn) ...... 24C Sapote, white (Casimiroa edulis La Llave & Lex) ...... 24B Sataw (Parkia speciosa Hassk.) ...... 24B Satinleaf (Chrysophyllum oliviforme L.) ...... 24A Screw-pine (Pandanus tectorius Parkinson) ...... 24B Sierra Leone-tamarind (Dialium guineense Willd.) ...... 24A Soncoya (Annona purpurea Moc. & Sesse´ ex Dunal) ...... 24C Soursop (Annona muricata L.) ...... 24C Spanish lime (Melicoccus bijugatus Jacq.) ...... 24A

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TABLE 1—CROP GROUP 24: TROPICAL AND SUBTROPICAL FRUIT, INEDIBLE PEEL GROUP—Continued

Related crop Commodities subgroups

Star apple (Chrysophyllum cainito L.) ...... 24B Sugar apple (Annona squamosa L.) ...... 24C Sun sapote (Licania platypus (Hemsl.) Fritsch) ...... 24C Tamarind-of-the-Indies (Vangueria madagascariensis J.F. Gmel.) ...... 24B Velvet tamarind (Dialium indum L.) ...... 24A Wampi (Clausena lansium (Lour.) Skeels) ...... 24A White star apple (Chrysophyllum albidum G. Don) ...... 24A Wild loquat (Uapaca kirkiana Mu¨ll. Arg.) ...... 24B Cultivars, varieties, and hybrids of these commodities.

(iii) Table. The following Table 2 identifies subgroup, and lists all the commodities in- the crop subgroups for Crop Group 24, speci- cluded in each subgroup. fies the representative commodities for each

TABLE 2—CROP GROUP 24: SUBGROUP LISTING

Representative commodities Commodities

Crop Subgroup 24A. Tropical and Subtropical, Small fruit, inedible peel subgroup

Lychee ...... Aisen; bael fruit; Burmese grape; cat’s-eyes; inga´; longan; lychee; madras-thorn; manduro; matisia; mesquite; mongongo, fruit; pawpaw, small-flower; satinleaf; Sierra Leone-tamarind; Spanish lime; velvet tamarind; wampi; white star apple; cultivars, varieties, and hybrids of these commodities.

Crop Subgroup 24B. Tropical and Subtropical, Medium to large fruit, smooth, inedible peel subgroup

Avocado, plus pomegranate or banana ...... Abiu; akee apple; avocado; avocado, Guatemalan; avocado, Mexican; avocado, West Indian; bacury; banana; banana, dwarf; binjai; canistel; cupuacu´; etambe; jatoba´; kei apple; langsat; lanjut; lucuma; mabolo; mango; mango, horse; mango, Saipan; mangosteen; paho; papaya; pawpaw, common; pelipisan; pequi; pequia; persimmon, American; plantain; pomegranate; poshte; quandong; sapote, black; sapote, green; sapote, white; sataw; screw-pine; star apple; tamarind-of-the-Indies; wild loquat; cultivars, varieties, and hybrids of these commodities.

Crop Subgroup 24C. Tropical and Subtropical, Medium to large fruit, rough or hairy, inedible peel subgroup

Pineapple, plus atemoya or sugar apple ...... Atemoya; biriba; breadfruit; champedak; cherimoya; custard apple; durian; elephant-apple; ilama; jackfruit; karuka; mammy-apple; marang; marmaladebox; monkey-bread tree; nicobar-breadfruit; pandanus; pineapple; pulasan; rambutan; sapodilla; sapote, mamey; soncoya; soursop; sugar apple; sun sapote; cultivars, varieties, and hybrids of these commodities.

Crop Subgroup 24D. Tropical and Subtropical, Cactus, inedible peel subgroup

Dragon fruit and Prickly pear fruit ...... Dragon fruit; pitahaya; pitaya; pitaya, amarilla; pitaya, roja; pitaya, yellow; prickly pear, fruit; prickly pear, Texas, fruit; saguaro; cultivars, varieties, and hybrids of these commodities.

Crop Subgroup 24E. Tropical and Subtropical, Vine, inedible peel subgroup

Passionfruit ...... Granadilla; granadilla, giant; monstera; passionflower, winged-stem; passionfruit; passionfruit, banana; passionfruit, purple; passionfruit, yellow; cultivars, varieties, and hybrids of these commodities.

Subpart C—Specific Tolerances 39430, July 1, 2003; 71 FR 74804, Dec. 13, 2006; 72 FR 53137, Sept. 18, 2007; 72 FR 61536, Oct. 31, 2007; 73 FR 60155, Oct. 10, 2008; 75 FR 56014, EDITORIAL NOTE: Nomenclature changes to Sept. 15, 2010; and 76 FR 34885, June 15, 2011. subpart C of part 180 appear at 67 FR 41803, June 19, 2002; 67 FR 42393, June 21, 2002; 68 FR

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§ 180.101 Specific tolerances; general Commodity Parts per provisions. million (a) The tolerances established for Pear ...... 25 .0 pesticide chemicals in this subpart C Plum, prune, fresh ...... 10.0 Rapeseed, forage ...... 0 .05 apply to residues resulting from their Rapeseed, seed ...... 0 .05 application prior to harvest or slaugh- Safflower, seed ...... 0 .05 ter, unless otherwise stated. Toler- Sesame, seed ...... 0 .05 ances are expressed in terms of parts Strawberry ...... 20.0 Sunflower, seed ...... 0.05 by weight of the pesticide chemical per Vegetable, brassica leafy, group 5 ...... 0 .05 one million parts by weight of the raw Vegetable, bulb, group 3 ...... 0 .05 agricultural commodity. Vegetable, cucurbit, group 9 ...... 0.05 (b) The poisonous and deleterious Vegetable, foliage of legume, group 7 ...... 0 .05 Vegetable, fruiting, group 8 ...... 0.05 substances for which tolerances are es- Vegetable, leafy, except brassica, group 4 ...... 0 .05 tablished by the regulations in this Vegetable, leaves of root and tuber, group 2 ..... 0 .05 subpart C are named by their common Vegetable, legume, group 6 ...... 0 .05 names wherever practicable, otherwise Vegetable, root and tuber, group 1 ...... 0 .05 by their chemical names. (c) The analytical methods to be used (2) Tolerances are established for the for determining whether pesticide resi- combined residues of the fungicide, dues, including negligible residues, in captan (N-trichloromethylthio-4- or on raw agricultural commodities are cyclohexene-1,2-dicarboximide) and its in compliance with the tolerances es- metabolite 1,2,3,6- tablished in this part 180 are identified tetrahydrophthalimide (THPI), meas- among the methods contained or ref- ured at THPI, in or on the following erenced in the Food and Drug Adminis- commodities: tration’s ‘‘Pesticide Analytical Man- Parts per ual’’ which is available from the Food Commodity million and Drug Administration, Department Cattle, fat ...... 0.15 of Health, Education, and Welfare, 200 Cattle, meat ...... 0 .20 C Street SW., Washington, DC 20204. Cattle, meat byproducts ...... 0.30 Goat, fat ...... 0 .15 § 180.103 Captan; tolerances for resi- Goat, meat ...... 0.20 dues. Goat, meat byproducts ...... 0 .30 Hog, fat ...... 0 .15 (a)(1) General. Tolerances are estab- Hog, meat ...... 0 .20 lished for residues of the fungicide, Hog, meat byproducts ...... 0 .30 Horse, fat ...... 0 .15 captan (N-trichloromethylthio-4- Horse, meat ...... 0 .20 cyclohexene-1,2-dicarboximide) in or on Horse, meat byproducts ...... 0 .30 the following commodities: Milk ...... 0.10 Sheep, fat ...... 0 .15 Parts per Sheep, meat ...... 0.20 Commodity million Sheep, meat byproducts ...... 0 .30

Almond ...... 0.25 Almond, hulls ...... 75 .0 (b) Section 18 emergency exemptions. Animal feed, nongrass, group 18 ...... 0 .05 [Reserved] Apple ...... 25.0 (c) Tolerances with regional registra- Apricot ...... 10 .0 tions. [Reserved] Blueberry ...... 20 .0 Caneberry, subgroup 13A ...... 25.0 (d) Indirect or inadvertent residues. Cherry, sweet ...... 50 .0 [Reserved] Cherry, tart ...... 50.0 Cotton, undelinted seed ...... 0 .05 [72 FR 52016, Sept. 12, 2007] Dill, seed ...... 0 .05 Flax, seed ...... 0 .05 § 180.106 Diuron; tolerances for resi- Grape ...... 25 .0 dues. Grain, cereal, forage, fodder and straw, group 16 ...... 0 .05 (a) General. Tolerances are estab- Grain, cereal, group 15 ...... 0.05 lished for the combined residues of the Grass, forage ...... 0 .05 Grass, hay ...... 0 .05 herbicide diuron, 3-(3,4- Nectarine ...... 25 .0 dichlorophenyl)-1,1-dimethylurea and Okra ...... 0.05 its metabolites convertible to 3,4- Peach ...... 15 .0 Peanut ...... 0 .05 dichloroaniline in or on food commod- Peanut, hay ...... 0.05 ities, as follows:

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Parts per Parts per Commodity million Commodity million

Alfalfa, forage ...... 3.0 Barley, bran ...... 0 .7 Alfalfa, hay ...... 2.0 Barley, grain ...... 0 .2 Apple ...... 0.1 Barley, hay ...... 2 Artichoke, globe ...... 1 Barley, straw ...... 1 .5 Asparagus ...... 7 Cactus ...... 0 .05 Banana ...... 0.1 Clover, forage ...... 0.1 Berry group 13 ...... 0 .1 Clover, hay ...... 1.0 Cattle, fat ...... 1 Oat, forage ...... 2 Cattle, meat ...... 1 Oat, grain ...... 0 .1 Cattle, meat byproducts ...... 1 Oat, hay ...... 2 Citrus, oil ...... 3.0 Oat, straw ...... 1.5 Corn, field, grain ...... 0 .1 Trefoil, forage ...... 0 .1 Corn, pop, grain ...... 0.1 Trefoil, hay ...... 1 .5 Cotton, undelinted seed ...... 0 .2 Vetch, forage ...... 0 .1 Fish – freshwater finfish, farm raised ...... 2 .0 Vetch, hay ...... 1 .5 Fruit, citrus, group 10, except lemon ...... 0 .05 Goat, fat ...... 1 (d) Indirect or inadvertent residues. Goat, meat ...... 1 Goat, meat byproducts ...... 1 [Reserved] Grain, aspirated fractions ...... 5 .0 [63 FR 2164, Jan. 14, 1998, as amended at 63 Grape ...... 0 .05 Grass, forage, except bermudagrass ...... 2 FR 57072, Oct. 26, 1998; 64 FR 41305, July 30, Grass, hay, except bermudagrass ...... 2 1999; 66 FR 28671, May 24, 2001; 67 FR 46883, Hazelnut ...... 0 .1 July 17, 2002; 69 FR 71717, Dec. 10, 2004; 72 FR Hog, fat ...... 1 32540, June 13, 2007; 72 FR 35666, June 29, 2007; Hog, meat ...... 1 73 FR 54958, Sept. 24, 2008; 76 FR 34885, June Hog, meat byproducts ...... 1 15, 2011] Horse, fat ...... 1 Horse, meat ...... 1 Horse, meat byproducts ...... 1 § 180.108 Acephate; tolerances for resi- Lemon ...... 0.5 dues. Nut, macadamia ...... 0.05 Olive ...... 1 (a) General. (1) Tolerances are estab- Papaya ...... 0 .5 lished for residues of acephate, O,S-di- Peach ...... 0 .1 methyl acetyl phosphoramidothioate, Pear ...... 1 including its metabolites and Pea, field, seed ...... 0 .1 Pea, field, vines ...... 2 degradates other than methamidophos, Pea, field, hay ...... 2 in or on the commodities in the fol- Pecan ...... 0 .05 lowing table. Compliance with the tol- Peppermint, tops ...... 1 .5 Pineapple ...... 0.1 erance levels specified in this para- Pineapple, process residue ...... 0 .4 graph is to be determined by measuring Sheep, fat ...... 1 only acephate, O,S-dimethyl acetyl Sheep, meat ...... 1 phosphoramidothioate, in or on the Sheep, meat byproducts ...... 1 Sorghum, grain, forage ...... 2 commodity. Sorghum, grain, grain ...... 0 .5 Parts per Sorghum, grain, stover ...... 2 Commodity 1 Spearmint, tops ...... 1 .5 million Sugarcane, cane ...... 0.2 Sugarcane, molasses ...... 0 .7 Bean, dry, seed ...... 3 .0 Walnut ...... 0 .05 Bean, succulent ...... 3 .0 Brussels sprouts ...... 3 .0 Wheat, bran ...... 0.7 Cattle, fat ...... 0.1 Wheat, forage ...... 2 Cattle, meat ...... 0 .1 Wheat, grain ...... 0 .5 Cattle, meat byproducts ...... 0.1 Wheat, hay ...... 2 Cauliflower ...... 2 .0 Wheat, straw ...... 1 .5 Celery ...... 10 Cotton, hulls ...... 1 .0 (b) Section 18 emergency exemptions. Cotton, meal ...... 1 .0 [Reserved] Cotton, undelinted seed ...... 0 .5 Cranberry ...... 0 .5 (c) Tolerances with regional registra- Egg ...... 0 .1 tions. Tolerances with a regional reg- Goat, fat ...... 0 .1 istration as defined in § 180.1(l) are es- Goat, meat ...... 0.1 tablished for the combined residues of Goat, meat byproducts ...... 0 .1 Hog, fat ...... 0 .1 the herbicide diuron (3-(3,4- Hog, meat ...... 0 .1 dichlorophenyl)-1,1-dimethylurea and Hog, meat byproducts ...... 0 .1 its metabolites convertible to 3,4- Horse, fat ...... 0 .1 Horse, meat ...... 0 .1 dichloroaniline) in or on the raw agri- Horse, meat byproducts ...... 0 .1 cultural commodities: Lettuce, head ...... 10

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Parts per methamidophos, O,S-dimethyl Commodity 1 million phosphoramidothioate, in or on the Milk ...... 0.1 commodity. Peanut ...... 0 .2 Pepper ...... 4 .0 Commodity Parts per Peppermint, tops ...... 27 million Poultry, fat ...... 0.1 Poultry, meat ...... 0 .1 Bean, dry, seed ...... 1 Poultry, meat byproducts ...... 0.1 Bean, succulent ...... 1 Sheep, fat ...... 0 .1 Brussels sprouts ...... 0 .5 Sheep, meat ...... 0.1 Cauliflower ...... 0 .5 Sheep, meat byproducts ...... 0 .1 Spearmint, tops ...... 27 Celery ...... 1 Soybean, seed ...... 1 .0 Cranberry ...... 0 .1 Lettuce, head ...... 1 1 Where there is a direct use of methamidophos on the commodity, residues of methamidophos resulting from Pepper ...... 1 methamidophos application are regulated under 40 CFR Peppermint, tops ...... 1 180.315. Spearmint, tops ...... 1 (2) A tolerance of 0.02 ppm is established for residues of acephate, O,S-di- (b) Section 18 emergency exemptions. methyl acetyl phosphoramidothioate, [Reserved] including its metabolites and (c) Tolerances with regional registra- degradates other than methamidophos, tions. A tolerance with a regional reg- in or on all food items (other than istration is established for residues of those already covered by a higher tol- acephate, O,S-dimethyl acetyl erance as a result of use on growing phosphoramidothioate, including its crops) in food handling establishments metabolites and degradates other than where food and food products are held, methamidophos, in or on the com- processed, prepared and served, includ- modity in the following table. Compli- ing food service, manufacturing and ance with the tolerance level specified processing establishments, such as resin this paragraph is to be determined taurants, cafeterias, supermarkets, by measuring only acephate, O,S-di- bakeries, breweries, dairies, meat methyl acetyl phosphoramidothioate, slaughtering and packing plants, and in or on the commodity. canneries, where application of Parts per acephate shall be limited solely to spot Commodity1 and/or crack and crevice treatment (a million coarse, low-pressure spray shall be used Nut, macadamia ...... 0.05 to avoid atomization or splashing of 1 Where there is a direct use of methamidophos on the the spray for spot treatments; equip- commodity, residues of methamidophos resulting from ment capable of delivering a pin- methamidophos application are regulated under 40 CFR stream of insecticide shall be used for 180.315. crack and crevice treatments). Spray (d) Indirect or inadvertent residues. concentration shall be limited to a [Reserved] maximum of 1.0 percent active ingredient. Contamination of food or food- [63 FR 13542, Mar. 20, 1998, as amended at 67 contact surfaces shall be avoided. Com- FR 49615, July 31, 2002; 73 FR 5108, Jan. 29, 2008; 75 FR 60237, Sept. 29, 2010] pliance with the tolerance levels specified in this paragraph is to be deter- EFFECTIVE DATE NOTE: At 81 FR 34905, June mined by measuring only acephate, 1, 2016, § 180.106 was amended by removing the O,S-dimethyl acetyl entries for ‘‘Bean, succulent’’ from the tables phosphoramidothioate, in or on the in paragraphs (a)(1) and (3), effective Nov. 28, commodity. 2016. (3) Tolerances are established for res- § 180.111 Malathion; tolerances for residues of methamidophos, O,S-dimethyl idues. phosphoramidothioate, including its metabolites and degradates, in or on (a) General. (1) Tolerances are estab- the commodities in the following table lished for residues of the insecticide as a result of the application of malathion (O,O-dimethyl acephate. Compliance with the toler- dithiophosphate of diethyl ance levels specified in this paragraph mercaptosuccinate) in or on the fol- is to be determined by measuring only lowing food commodities:

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Parts per Parts per Commodity million Commodity million

Alfalfa, forage ...... 135 Peach ...... 8 Alfalfa, hay ...... 135 Peanut, hay ...... 135 Almond, hulls ...... 50 Peanut, postharvest ...... 8 Almond, postharvest ...... 8 Pear ...... 8 Apple ...... 8 Pecan ...... 8 Apricot ...... 8 Pepper ...... 8 Asparagus ...... 8 Peppermint, tops ...... 8 Avocado ...... 8 Pineapple ...... 8 Barley, grain, postharvest ...... 8 Plum ...... 8 Bean, dry, seed ...... 8 Plum, prune ...... 8 Bean, succulent ...... 8 Potato ...... 8 Beet, garden, roots ...... 8 Pumpkin ...... 8 Beet, garden, tops ...... 8 Quince ...... 8 Beet, sugar, roots ...... 1 Radish ...... 8 Beet, sugar, tops ...... 8 Raspberry ...... 8 Blackberry ...... 8 Rice, grain, postharvest ...... 8 Blueberry ...... 8 Rice, wild ...... 8 Boysenberry ...... 8 Rutabaga ...... 8 Carrot, roots ...... 8 Rye, grain, postharvest ...... 8 Chayote, fruit ...... 8 Safflower, seed ...... 0 .2 Chayote, roots ...... 8 Salsify, roots ...... 8 Cherry ...... 8 Salsify, tops ...... 8 Chestnut ...... 1 Shallot, bulb ...... 8 Clover, forage ...... 135 Sorghum, grain, forage ...... 8 Clover, hay ...... 135 Sorghum, grain, grain, postharvest ...... 8 Corn, field, forage ...... 8 Soybean, forage ...... 135 Soybean, hay ...... 135 Corn, field, grain, postharvest ...... 8 Soybean, seed ...... 8 Corn, pop, grain, postharvest ...... 8 Soybean, vegetable, succulent ...... 8 Corn, sweet, forage ...... 8 Spearmint, tops ...... 8 Corn, sweet, kernel plus cob with husks re- Squash, summer ...... 8 moved ...... 2 Squash, winter ...... 8 Cowpea, forage ...... 135 Strawberry ...... 8 Cowpea, hay ...... 135 Sunflower, seed, postharvest ...... 8 Cranberry ...... 8 Sweet potato, roots ...... 1 Cucumber ...... 8 Tangerine ...... 8 Currant ...... 8 Tomato ...... 8 Date, dried fruit ...... 8 Trefoil, forage ...... 135 Dewberry ...... 8 Trefoil, hay ...... 135 Eggplant ...... 8 Turnip, greens ...... 8 Fig ...... 8 Turnip, roots ...... 8 Flax, seed ...... 0 .1 Vegetable, brassica, leafy, group 5 ...... 8 Garlic, bulb ...... 8 Vegetable, leafy, except brassica, group 4 ...... 8 Gooseberry ...... 8 Vetch, hay ...... 135 Grape ...... 8 Walnut ...... 8 Grapefruit ...... 8 Wheat, grain, postharvest ...... 8 Guava ...... 8 Hazelnut ...... 1 Hop, dried cones ...... 1 (2) Tolerances are established for the Horseradish ...... 8 combined residues of the insecticide Kumquat ...... 8 malathion (O,O-dimethyl Leek ...... 8 Lemon ...... 8 dithiophosphate of diethyl Lentil, seed ...... 8 mercaptosuccinate) and its metabolite, Lespedeza, hay ...... 135 malaoxon (O,O-dimethyl thiophosphate Lime ...... 8 of diethyl mercaptosuccinate), in or on Loganberry ...... 8 Lupin, seed ...... 8 the following food commodities: Mango ...... 8 Melon ...... 8 Commodity Parts per Mushroom ...... 8 million Nectarine ...... 8 Barley, straw ...... 50 Nut, macadamia ...... 1 Corn, field, stover ...... 30 .0 Oat, grain, postharvest ...... 8 Cotton, undelinted seed ...... 20 .0 Okra ...... 8 Grass, forage ...... 200 Onion, bulb ...... 8 Grass, hay ...... 270 Onion, green ...... 8 Oat, forage ...... 4 .0 Orange ...... 8 Oat, straw ...... 50 Papaya ...... 1 Rye, forage ...... 4 .0 Parsnip ...... 8 Rye, straw ...... 50 Passionfruit ...... 8 Watercress ...... 0 .2 Pea ...... 8 Wheat, forage ...... 4 .0 Pea, field, hay ...... 8 Wheat, straw ...... 50 Pea, field, vines ...... 8

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(3) Tolerances are established for resin citrus, dried pulp for cattle feed, idues of the insecticide malathion when present as the result of the appli- (O,O-dimethyl dithiophosphate of cation of the pesticide to bagged citrus diethyl mercaptosuccinate), in or on pulp during storage. Whether or not the following food commodities: tolerances for residues of malathion on the fresh fruit have been established Parts per Commodity million under section 408 of the Act, the total residue of malathion in the citrus, Cattle, fat ...... 4 dried pulp shall not exceed 50 parts per Cattle, meat1 ...... 4 Cattle, meat byproducts1 ...... 4 million. Egg ...... 0 .1 (ii) A tolerance of 10 parts per million Goat, fat ...... 4 is established for malathion in non- Goat, meat1 ...... 4 Goat, meat byproducts1 ...... 4 medicated cattle feed concentrate Hog, fat ...... 4 blocks resulting from its application as Hog, meat1 ...... 4 a pesticide to paper used in packaging Hog, meat byproducts1 ...... 4 Horse, fat ...... 4 the nonmedicated cattle feed con- Horse, meat1 ...... 4 centrate blocks. Horse, meat byproducts1 ...... 4 (b) Section 18 emergency exemptions. Milk, fat ...... 0 .5 Poultry, fat ...... 4 [Reserved] Poultry, meat1 ...... 4 (c) Tolerances with regional registra- Poultry, meat byproducts1 ...... 4 tions. [Reserved] Sheep, fat ...... 4 Sheep, meat1 ...... 4 (d) Indirect or inadvertent residues. Sheep, meat byproducts1 ...... 4 [Reserved] 1 The tolerance level shall not be exceeded in any cut of meat or in any meat byproducts from cattle, goat, hog, horse, [43 FR 22974, May 30, 1978, as amended at 43 poultry, or sheep. FR 45584, Oct. 3, 1978; 44 FR 38844, July 3, 1979; 45 FR 76145, Nov. 18, 1980; 47 FR 42738, (4) Malathion may be safely used in Sept. 29, 1982; 47 FR 55226, Dec. 8, 1982; 52 FR accordance with the following condi- 45183, Nov. 25, 1987; 62 FR 66023, 66025, Dec. 17, tions: 1997; 65 FR 33694, May 24, 2000; 72 FR 35665, (i) It is incorporated into paper trays June 29, 2007; 73 FR 54959, Sept. 24, 2008; 74 FR in amounts not exceeding 100 milli- 47455, Sept. 16, 2009; 75 FR 60238, Sept. 29, grams per square foot. 2010] (ii) Treated paper trays are intended for use only in the drying of grape (rai- § 180.114 Ferbam; tolerances for residues. sins). (iii) Total residues of malathion re- (a) General. Tolerances are estab- sulting from drying of grape on treated lished for residues of the fungicide trays and from application to grape be- ferbam (ferric fore harvest shall not exceed 12 parts dimethyldithiocarbamate), calculated per million on processed ready-to-eat as carbon disulfide, in or on the fol- raisins. lowing food commodities: (5) Residues of malathion in saf- Expiration/ flower, refined oil from application to Commodity Parts per Revocation the growing safflower plant shall not million Date exceed 0.6 parts per million. Apple ...... 4.0 1 None (6) Malathion may be safely used for Bean ...... 7.0 1 10/27/07 the control of insects during the drying Cabbage ...... 7.0 1 10/27/07 of grape (raisins) in compliance with Cherry ...... 4.0 1 None paragraph (a)(4) of this section by in- Cranberry ...... 4.0 1 None Fruit, citrus, group 10 ...... 4.0 1 None corporation into paper trays in Grape ...... 4.0 1 None amounts not exceeding 100 milligrams Lettuce ...... 7.0 1 10/27/07 per square foot. Nectarine ...... 4.0 1 None (7) Malathion (O,O-dimethyl Peach ...... 4.0 1 None dithiophosphate of diethyl Pear ...... 4.0 1 None Raspberry ...... 7.0 1 10/27/07 mercaptosuccinate) may be safely used 1Some of these tolerances were established on the basis of in feed in accordance with the fol- data acquired at the public hearings held in 1950 (formerly lowing conditions. § 180.101) and the remainder were established on the basis (i) A tolerance of 50 parts per million of pesticide petitions presented under the procedure specified in the amendment to the Federal Food, Drug, and Cosmetic is established for residues of malathion Act by Pub. L. 518, 83d Congress (68 Stat. 511)

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(b) Section 18 emergency exemptions. (d) Indirect or inadvertent residues. [Reserved] [Reserved] (c) Tolerances with regional registra- [68 FR 39437, July 1, 2003, as amended at 71 tions. Tolerances with regional reg- FR 54432, Sept. 15, 2006; 73 FR 54959, Sept. 24, istrations, as defined in § 180.1(l), are 2008; 77 FR 59123, Sept. 26, 2012] established for residues of the fungicide ferbam (ferric § 180.117 S-Ethyl dimethyldithiocarbamate), calculated dipropylthiocarbamate; tolerances as carbon disulfide, in or on the fol- for residues. lowing food commodities: (a) General. Tolerances are established for residues of the herbicide S- Commodity Parts per ethyl dipropylthiocarbamate, including million its metabolites and degradates, in or Mango ...... 4.0 1 on the commodities in the following table. Compliance with the tolerance 1 This tolerance was established on the basis of data acquired at the public hearings held in 1950 (formerly § 180.101) levels specified in this paragraph is to and the remainder was established on the basis of pesticide be determined by measuring only the petitions presented under the procedure specified in the amendment to the Federal Food, Drug, and Cosmetic Act by sum of S-ethyl dipropylthiocarbamate, Pub. L. 518, 83d Congress (68 Stat. 511) S-ethyl (2- (d) Indirect or inadvertent residues. hydroxypropyl)propylcarbamothioate, [Reserved] S-(2-hydroxyethyl)dipropylcarbamothioate, and S- [63 FR 57072, Oct. 26, 1998, as amended at 72 ethyl (3- FR 53453, Sept. 19, 2007] hydroxypropyl)propylcarbamothioate, calculated as the stoichiometric equiv- § 180.116 Ziram; tolerances for resi- alent of S-ethyl dues. dipropylthiocarbamate, in or on the (a) General. Tolerances are estab- commodity. lished for residues of the fungicide ziram (zinc dimethyldithiocarbamate), Parts per Commodity million calculated as zinc ethylenebisdithiocarbamate, in or on Alfalfa, forage ...... 0.2 Alfalfa, hay ...... 0.6 the following food commodities: Almond ...... 0.08 Almond, hulls ...... 0 .08 Parts per Expiration/ Bean, dry, seed ...... 0 .08 Commodity million revocation Bean, succulent ...... 0 .08 date Beet, garden, tops ...... 0 .5 Beet, sugar, molasses ...... 0 .4 1 Almond ...... 0.1 None Beet, sugar, tops ...... 0.5 Apple ...... 1 7.0 None Clover, forage ...... 0.1 Apricot ...... 1 7.0 None Clover, hay ...... 0.1 Blackberry ...... 1 7.0 5/11/13 Corn, field, forage ...... 0 .08 Blueberry ...... 1 7.0 None Corn, field, grain ...... 0 .08 Cherry, sweet ...... 1 7.0 None Corn, field, stover ...... 0 .08 Corn, pop, grain ...... 0.08 Cherry, tart ...... 1 7.0 None Corn, pop, stover ...... 0.08 Grape ...... 7.0 None Corn, sweet, forage ...... 0 .08 Huckleberry ...... 7.0 None Corn, sweet, kernel plus cob with husks re- Peach ...... 7.0 None moved ...... 0 .08 Pear ...... 1 7.0 None Corn, sweet, stover ...... 0 .08 Pecan ...... 0.1 None Cotton, gin byproducts ...... 0 .20 Quince ...... 1 7.0 None Cotton, undelinted seed ...... 0 .08 Fruit, citrus, group 10 ...... 0 .1 Strawberry ...... 7.0 None Lespedeza, forage ...... 0 .1 1 Tomato ...... 7.0 None Lespedeza, hay ...... 0.1 1 Some of these tolerances were established on the basis of Pea, succulent ...... 0 .08 data acquired at the public hearings held in 1950 (formerly Safflower, seed ...... 0 .08 § 180.101) and the remainder were established on the basis Sunflower, seed ...... 0.08 of pesticide petitions presented under the procedure specified Tomato ...... 0.08 in the amendment to the Federal Food, Drug, and Cosmetic Trefoil, forage ...... 0 .1 Act by Public Law 518, 83d Congress (68 Stat. 511). Trefoil, hay ...... 0 .1 Vegetable, root ...... 0 .1 (b) Section 18 emergency exemptions. Walnut ...... 0 .08 [Reserved] (c) Tolerances with regional registra- (b) Section 18 emergency exemptions. tions. [Reserved] [Reserved]

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(c) Tolerances with regional registra- § 180.123 Inorganic bromide residues tions. [Reserved] resulting from fumigation with (d) Indirect or inadvertent residues. methyl bromide; tolerances for resi- [Reserved] dues. (a) General. (1) Tolerances are estab- [75 FR 60239, Sept. 29, 2010] lished for residues of inorganic bro- § 180.121 Methyl parathion; tolerances mides (calculated as Br) in or on the for residues. following food commodities which have been fumigated with the antimicrobial (a) General. Tolerances are estab- agent and insecticide methyl bromide lished for residues of the insecticide after harvest (with the exception of methyl parathion, including its me- strawberry): tabolites and degradates, in or on the commodities in the table in this para- Parts per Expiration/ graph. Compliance with the tolerance Commodity Revocation million Date levels specified in this paragraph is to be determined by measuring only Alfalfa, hay, postharvest ...... 50.0 10/31/11 methyl parathion, O,O-dimethyl O-(4- Almond, postharvest ...... 200.0 None Apple, postharvest ...... 5.0 None nitrophenyl) phosphorothioate, in or Apricot, postharvest ...... 20.0 None on the commodity. Artichoke, jerusalem, postharvest ... 30.0 None Asparagus, postharvest ...... 100.0 None Expiration/ Avocado, postharvest ...... 75.0 None Parts per Barley, grain, postharvest ...... 50.0 None Commodity million Revocation date Bean, lima, postharvest ...... 50.0 None Bean, postharvest ...... 50.0 None Alfalfa, forage ...... 1.25 12/31/13 Bean, snap, succulent, postharvest 50.0 None Alfalfa, hay ...... 5.0 12/31/13 Bean, succulent, postharvest ...... 50.0 None Almond ...... 0.1 12/31/13 Beet, garden, roots, postharvest ..... 30.0 None Almond, hulls ...... 3.0 12/31/13 Beet, sugar, roots, postharvest ...... 30.0 None Barley ...... 1.0 12/31/13 Blueberry, postharvest ...... 20.0 None Corn, field, forage ...... 1.0 12/31/13 Butternut, postharvest ...... 200.0 None Corn, field, grain ...... 1.0 12/31/13 Cabbage, postharvest ...... 50.0 None Cacao bean, roasted bean, Corn, pop, grain ...... 1.0 12/31/13 postharvest ...... 50.0 None Corn, sweet, forage ...... 1.0 12/31/13 Cantaloupe, postharvest ...... 20.0 None Corn, sweet, kernel plus cob with Carrot, roots, postharvest ...... 30.0 None husks removed ...... 1.0 12/31/13 Cashew, postharvest ...... 200.0 None Cotton, undelinted seed ...... 0.75 12/31/13 Cherry, sweet, postharvest ...... 20.0 None Grass, forage ...... 1.0 12/31/13 Cherry, tart, postharvest ...... 20 None Oat ...... 1.0 12/31/13 Chestnut, postharvest ...... 200.0 None Onion ...... 1.0 12/31/13 Cippolini, bulb, postharvest ...... 50.0 None Pea, field, vines ...... 1.0 12/31/13 Citron, citrus, postharvest ...... 30.0 None Potato ...... 0.1 12/31/13 Coconut, copra, postharvest ...... 100.0 None Rapeseed, seed ...... 0.2 12/31/13 Coffee, bean, green, postharvest .... 75.0 None Rice, grain ...... 1.0 12/31/13 Corn, field, grain, postharvest ...... 50.0 None Soybean, hay ...... 1.0 12/31/13 Corn, pop, postharvest ...... 240.0 None Soybean, seed ...... 0.1 12/31/13 Corn, sweet, kernel plus cob with Sunflower, seed ...... 0.2 12/31/13 husks removed, postharvest ...... 50.0 None Sweet potato, roots ...... 0.1 12/31/13 Cotton, undelinted seed, Walnut ...... 0.1 12/31/13 postharvest ...... 200.0 10/31/11 Cucumber, postharvest ...... 30.0 None Wheat ...... 1.0 12/31/13 Cumin, seed, postharvest ...... 100.0 None Eggplant, postharvest ...... 20.0 None (b) Section 18 emergency exemptions. Garlic, postharvest ...... 50.0 None [Reserved] Ginger, postharvest ...... 100.0 None Grape, postharvest ...... 20.0 None (c) Tolerances with regional registra- Grapefruit, postharvest ...... 30.0 None tions. [Reserved] Hazelnut, postharvest ...... 200.0 None (d) Indirect or inadvertent residues. Horseradish, postharvest ...... 30.0 None [Reserved] Kumquat, postharvest ...... 30.0 None Lemon, postharvest ...... 30.0 None [66 FR 1245, Jan. 5, 2001, as amended at 66 FR Lime, postharvest ...... 30.0 None 38955, July 26, 2001; 67 FR 38603, June 5, 2002; Melon, honeydew, postharvest ...... 20.0 None Muskmelon, postharvest ...... 20.0 None 72 FR 35666, June 29, 2007; 73 FR 54959, Sept. Nectarine, postharvest ...... 20.0 None 24, 2008; 74 FR 46372, Sept. 9, 2009; 76 FR 56652, Nut, brazil, postharvest ...... 200.0 None Sept. 14, 2011; 78 FR 60721, Oct. 2, 2013] Nut, hickory, postharvest ...... 200.0 None Nut, macadamia, postharvest ...... 200.0 None EFFECTIVE DATE NOTE: At 81 FR 34905, June Oat, postharvest ...... 50.0 None 1, 2016, § 180.121 was removed, effective Nov. Okra, postharvest ...... 30.0 None 28, 2016. Onion, bulb, postharvest ...... 20.0 None

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(ii) When inorganic bromide residues Parts per Expiration/ Commodity Revocation are present in malt beverage, fer- million Date mented in accordance with 21 CFR Onion, green, postharvest ...... 20.0 None 172.730(a)(2), the amount shall not ex- Orange, postharvest ...... 30.0 None ceed 25 parts per million (calculated as Parsnip, roots, postharvest ...... 30.0 None Peach, postharvest ...... 20.0 None Br). Peanut, postharvest ...... 200.0 None (iii) Where tolerances are established Pear, postharvest ...... 5.0 None on both the raw agricultural commod- Pea, blackeyed, postharvest ...... 50.0 None ities and processed food made there- Pea, postharvest ...... 50.0 None Pecan, postharvest ...... 200.0 None from, the total residues of inorganic Pepper, postharvest ...... 30.0 None bromides in or on the processed food Pimento, postharvest ...... 30.0 None shall not be greater than those des- Pineapple, postharvest ...... 20.0 None Pistachio, postharvest ...... 200.0 None ignated in paragraph (a)(2) of this sec- Plum, postharvest ...... 20.0 None tion, unless a higher level is estab- Pomegranate, postharvest ...... 100.0 None lished elsewhere in this part. Potato, postharvest ...... 75.0 None (3) Tolerances are established for res- Pumpkin, postharvest ...... 20.0 None Quince, postharvest ...... 5.0 None idues of inorganic bromides (calculated Radish, postharvest ...... 30.0 None as Br) as follows: Rice, grain, postharvest ...... 50.0 None (i) 400 parts per million for residues Rutabaga, roots, postharvest ...... 30.0 None in or on dog food, resulting from fumi- Rutabaga, tops, postharvest ...... 30.0 None Rye, grain, postharvest ...... 50.0 None gation with methyl bromide. Salsify, roots, postharvest ...... 30.0 None (ii) 125 parts per million for residues Sorghum, grain, grain, postharvest 50.0 None in or on processed commodities for ani- Soybean, postharvest ...... 200.0 None Squash, summer, postharvest ...... 30.0 None mal feedstuffs from barley, corn, grain Squash, winter, postharvest ...... 20.0 None sorghum, oat, rice, rye and wheat, re- Squash, zucchini, postharvest ...... 20.0 None sulting directly from fumigation with Strawberry, postharvest ...... 60.0 None methyl bromide or from carryover and Sweet potato, postharvest ...... 75.0 None Tangerine, postharvest ...... 30.0 None concentration of residues of inorganic Timothy, hay, postharvest ...... 50.0 10/19/10 bromides from fumigation of the grains Tomato, postharvest ...... 20.0 None with methyl bromide. Turnip, roots, postharvest ...... 30.0 None (b) Section 18 emergency exemptions. Walnut, postharvest ...... 200.0 None Watermelon, postharvest ...... 20.0 None [Reserved] Wheat ...... 50.0 None (c) Tolerances with regional registrations. A tolerance with regional reg- (2) Inorganic bromide may be present istration, as defined in § 180.1(l), is es- as a residue in certain processed food tablished for residues of inorganic bro- in accordance with the following condi- mides (calculated as Br) in or on the tions: following food commodity grown in (i) When inorganic bromide residues soil fumigated with methyl bromide. are present as a result of fumigation of the processed food with methyl bro- Parts per Commodity million mide or from such fumigation in addition to the authorized use of methyl Ginger, postharvest ...... 100 bromide on the source raw agricultural commodity, as provided for in this (d) Indirect or inadvertent residues. part, the total residues of inorganic [Reserved] bromides (calculated as Br) shall not [71 FR 74812, Dec. 13, 2006, as amended at 75 exceed the following levels: FR 60239, Sept. 29, 2010] (A) 400 parts per million in or on egg, dried and herb, processed and spice. § 180.123a Inorganic bromide residues (B) 325 parts per million in or on in peanut hay and peanut hulls; cheese, parmesan and cheese, roquefort statement of policy. cheese. (a) Investigations by the Food and (C) 250 parts per million in or on to- Drug Administration show that peanut mato, concentrated products and fig, hay and peanut shells have been used dried fruit. as feed for meat and dairy animals. (D) 125 parts per million in or on While many growers now harvest pea- processed food other than those listed nuts with combines and leave the hay above. on the ground to be incorporated into

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the soil, some growers follow the prac- Commodity Parts per tice of curing peanuts on the vines in a million stack and save the hay for animal feed. Birdseed, mixtures, postharvest ...... 20 Peanut shells or hulls have been used Blackberry, postharvest ...... 8 to a minor extent as roughage for cat- Blueberry, postharvest ...... 8 Boysenberry, postharvest ...... 8 tle feed. It has been established that Buckwheat, grain, postharvest ...... 20 the feeding to cattle of peanut hay and Cattle, fat ...... 0.1 peanut hulls containing residues of in- Cattle, meat ...... 0 .1 organic bromides will contribute con- Cattle, meat byproducts ...... 0.1 Cherry, sweet, postharvest ...... 8 siderable residues of inorganic bro- Cherry, tart, postharvest ...... 8 mides to the meat and milk. Cacoa bean, roasted bean, postharvest ...... 8 (b) There are no tolerances for inor- Coconut, copra, postharvest ...... 8 ganic bromides in meat and milk to Corn, field, grain, postharvest ...... 20 Corn, pop, postharvest ...... 20 cover residues from use of such peanut Cotton, undelinted seed, postharvest ...... 8 hulls as animal feed. Peanut hulls con- Crabapple, postharvest ...... 8 taining residues of inorganic bromides Currant, postharvest ...... 8 from the use of methyl bromide are un- Dewberry, postharvest ...... 8 Egg ...... 1 suitable as an ingredient in the feed of Fig, postharvest ...... 8 meat and dairy animals and should not Flax, seed, postharvest ...... 8 be represented, sold, or used for that Goat, fat ...... 0 .1 Goat, meat ...... 0.1 purpose. Goat, meat byproducts ...... 0 .1 [58 FR 65555, Dec. 15, 1993] Gooseberry, postharvest ...... 8 Grape, postharvest ...... 8 Guava, postharvest ...... 8 § 180.124 Methyl bromide; tolerances Hog, fat ...... 0 .1 for residues. Hog, meat ...... 0 .1 (a) General. A tolerance is established Hog, meat byproducts ...... 0 .1 Horse, fat ...... 0 .1 for residues of the fumigant methyl Horse, meat ...... 0 .1 bromide, including metabolites and Horse, meat byproducts ...... 0 .1 degradates, in or on the commodity in Loganberry, postharvest ...... 8 Mango, postharvest ...... 8 the table below. Compliance with the Milk, fat ...... 0 .25 tolerance level specified below is to be Muskmelon, postharvest ...... 8 determined by measuring only methyl Oat, postharvest ...... 8 bromide. Orange, postharvest ...... 8 Peach, postharvest ...... 8 Peanut, postharvest ...... 8 Parts per Commodity million Pea, postharvest ...... 8 Pear, postharvest ...... 8 Cotton, undelinted seed ...... 150 Pineapple, postharvest ...... 8 Plum, prune, fresh, postharvest ...... 8 Potato, postharvest ...... 0 .25 (b) Section 18 emergency exemptions. Poultry, fat ...... 3 [Reserved] Poultry, meat ...... 3 (c) Tolerances with regional registra- Poultry, meat byproducts ...... 3 tions. [Reserved] Raspberry, postharvest ...... 8 Rice, postharvest ...... 20 (d) Indirect or inadvertent residues. Rye, postharvest ...... 20 [Reserved] Sheep, fat ...... 0 .1 Sheep, meat ...... 0.1 [77 FR 35298, June 13, 2012] Sheep, meat byproducts ...... 0 .1 Sorghum, grain, postharvest ...... 8 § 180.127 Piperonyl butoxide; toler- Sweet potato, postharvest ...... 0 .25 ances for residues. Tomato, postharvest ...... 8 Walnut, postharvest ...... 8 (a) General. (1) Tolerances for resi- Wheat, postharvest ...... 20 dues of the insecticide piperonyl butoxide [(butyl carbityl)(6-propyl (2) Piperonyl butoxide may be safely piperonyl)ether] are established in or used in accordance with the following on the following food commodities: prescribed conditions: (i) It is used or intended for use in Parts per Commodity million combination with pyrethrins for control of insects: Almond, postharvest ...... 8 (A) In cereal grain mills and in stor- Apple, postharvest ...... 8 Barley, postharvest ...... 20 age areas for milled cereal grain prod- Bean, postharvest ...... 8 ucts, whereby the amount of piperonyl

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butoxide is at least equal to but not sult of migration from its use on the more than 10 times the amount of cloth of cotton bags of 50 pounds or pyrethrins in the formulation. more capacity constructed with waxed (B) On the outer ply of multiwall paper liners. paper bags of 50 pounds or more capac- (E) Food treated in accordance with ity in amounts not exceeding 60 milli- paragraph (a)(2)(i)(D) and (E) of this grams per square foot, whereby the section. amount of piperonyl butoxide is equal (iv) To assure safe use of the pes- to 10 times the amount of pyrethrins in ticide, its label and labeling shall con- the formulation. Such treated bags are form to that registered with the U.S. to be used only for food, dried. Environmental Protection Agency, and (C) On cotton bags of 50 pounds or it shall be used in accordance with more capacity in amounts not exceed- such label and labeling. ing 55 milligrams per square foot of (v) Where tolerances are established cloth, whereby the amount of piperonyl on both raw agricultural commodities butoxide is equal to 10 times the and processed food made therefrom, the amount of pyrethrins in the formula- total residues of piperonyl butoxide in tion. Such treated bags are constructed or on the processed food shall not be with waxed paper liners and are to be greater than that permitted by the used only for food, dried that contain 4 larger of the two tolerances. percent fat or less. (3) Piperonyl butoxide may be safely (D) In two-ply bags consisting of cel- used in accordance with the following lophane/polyolefin sheets bound to- prescribed conditions: gether by an adhesive layer when it is (i) It is used or intended for use in incorporated in the adhesive. The combination with pyrethrins for con- treated sheets shall contain not more trol of insects: than 50 milligrams of piperonyl (A) On the outer ply of multiwall butoxide per square foot (538 milli- paper bags of 50 pounds or more capac- grams per square meter). Such treated ity in amounts not exceeding 60 milli- bags are to be used only for packaging grams per square foot. plum, prune, dried; grape, raisin; and (B) On cotton bags of 50 pounds or other fruit, dried and are to have a more capacity in amounts not exceed- maximum ratio of 3.12 milligrams of ing 55 milligrams per square foot of piperonyl butoxide per ounce of fruit cloth. Such treated bags are con- (0.10 milligram of piperonyl butoxide structed with waxed paper liners and per gram of product). are to be used only for feed, dried that (E) In food processing and food stor- contain 4 percent fat or less. age areas: Provided, That the food is (ii) It is used in combination with removed or covered prior to such use. pyrethrins, whereby the amount of (ii) It is used or intended for use in piperonyl butoxide is equal to 10 times combination with pyrethrins and N- the amount of pyrethrins in the formu- octylbicycloheptene dicarboximide for lation. Such treated bags are to be used insect control in accordance with 21 only for feed, dried. CFR 178.3730. (iii) A tolerance of 10 parts per mil- (iii) A tolerance of 10 parts per million is established for residues of lion is established for residues of piperonyl butoxide when present as the piperonyl butoxide in or on: result of migration: (A) Grain, cereal, milled fractions (A) In or on feed, dried from its use when present therein as a result of its on the outer ply of multiwall paper use in cereal grain mills and in storage bags of 50 pounds or more capacity. areas for milled cereal grain products. (B) In or on feed, dried that contain (B) Food, dried when present as a re- 4 percent fat, or less, from its use on sult of migration from its use on the cotton bags of 50 pounds or more capac- outer ply of multiwall paper bags of 50 ity constructed with waxed paper lin- pounds or more capacity. ers. (C) Food treated in accordance with (iv) To assure safe use of the pes- 21 CFR 178.3730. ticide, its label and labeling shall con- (D) Food, dried that contain 4 perform to that registered with the U.S. cent fat, or less, when present as a re- Environmental Protection Agency.

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(v) Where tolerances are established Commodity Parts per on both the raw agricultural commod- million ities and food, processed made there- Blackberry, postharvest ...... 1 .0 from, the total residues of piperonyl Blueberry, postharvest ...... 1 .0 butoxide in or on the processed food Boysenberry, postharvest ...... 1 .0 Buckwheat, grain, postharvest ...... 3 .0 shall not be greater than that per- Cacao bean, roasted bean, postharvest ...... 1.0 mitted by the larger of the two toler- Cattle, fat ...... 1.0 ances. Cattle, meat ...... 0 .05 (b) Section 18 emergency exemptions. Cattle, meat byproducts ...... 0.05 Cherry, sweet, postharvest ...... 1 .0 [Reserved] Cherry, tart, postharvest ...... 1 .0 (c) Tolerances with regional registra- Coconut, copra, postharvest ...... 1 .0 tions. [Reserved] Corn, field, grain, postharvest ...... 3 .0 Corn, pop, grain, postharvest ...... 3 .0 (d) Indirect or inadvertent residues. Cotton, undelinted seed, postharvest ...... 1.0 [Reserved] Crabapple, postharvest ...... 1 .0 Currant, postharvest ...... 1 .0 [71 FR 74813, Dec. 13, 2006] Dewberry, postharvest ...... 1 .0 Fig, postharvest ...... 1 .0 § 180.128 Pyrethrins; tolerances for Flax, seed, postharvest ...... 1 .0 residues. Goat, fat ...... 1 .0 Goat, meat ...... 0.05 (a) General. (1) Tolerances for resi- Goat, meat byproducts ...... 0 .05 dues of the insecticide pyrethrins ((1S)- Gooseberry, postharvest ...... 1 .0 2-methyl-4-oxo-3-(2Z)-2,4- Grape, postharvest ...... 1 .0 Guava, postharvest ...... 1 .0 pentadienylcyclopenten-1-yl (1R,3R)- Hog, fat ...... 1 .0 2,2-dimethyl-3-(2-methyl-1-pro- Hog, meat ...... 0 .05 penyl)cyclopropanecarboxylate (pyre- Hog, meat byproducts ...... 0 .05 Horse, fat ...... 1 .0 thrin 1), (1S)-2-methyl-4-oxo-3-(2Z)-2,4- Horse, meat ...... 0 .05 pentadienyl-2-cyclopenten-1-yl (1R,3R)- Horse, meat byproducts ...... 0 .05 3-[(1E)-3-methoxy-2-methyl-3-oxo-1-pro- Loganberry, postharvest ...... 1 .0 penyl]-2,2-dimethylcyclopropane- Mango, postharvest ...... 1 .0 Milk, fat (reflecting negligible residues in milk) ... 0 .05 carboxylate (pyrethrin 2), (1S)-3-(2Z)-2- Muskmelon, postharvest ...... 1.0 butenyl-2-methyl-4-oxo-2-cyclopenten- Oat, grain, postharvest ...... 1 .0 1-yl (1R,3R)-2,2-dimethyl-3-(2-methyl-1- Orange, postharvest ...... 1.0 Pea, dry, seed, postharvest ...... 1 .0 propenyl)cyclopropanecarboxylate Peach, postharvest ...... 1.0 (cinerin 1), (1S)-3-(2Z)-2-butenyl-2- Peanut, postharvest ...... 1 .0 methyl-4-oxo-2-cyclopenten-1-yl Pear, postharvest ...... 1.0 (1R,3R)-3-[(1E)-3-methoxy-2-methyl-3- Pineapple, postharvest ...... 1 .0 Plum, prune, fresh, postharvest ...... 1 .0 oxo-1-propenyl]-2,2- Potato, postharvest ...... 0 .05 dimethylcyclopropanecarboxylate Raspberry, postharvest ...... 1.0 (cinerin 2), (1S)-2-methyl-4-oxo-3-(2Z)-2- Rice, grain, postharvest ...... 3 .0 Rye, grain, postharvest ...... 3 .0 pentenyl-2-cyclopenten-1-yl (1R, 3R)- Sheep, fat ...... 1 .0 2,2-dimethyl-3-(2-methyl-1-pro- Sheep, meat ...... 0.05 penyl)cyclopropanecarboxylate Sheep, meat byproducts ...... 0 .05 (jasmolin 1), and (1S)-2-methyl-4-oxo-3- Sorghum, grain, grain, postharvest ...... 1.0 Sweet potato, postharvest ...... 0 .05 (2Z)-pentenyl-2-cyclopenten-1-yl Tomato, postharvest ...... 1 .0 (1R,3R)-3-[(1E)-3-methoxy-2-methyl-3- Walnut, postharvest ...... 1.0 oxo-1-propenyl]-2,2- Wheat, grain, postharvest ...... 3 .0 dimethylcyclopropanecarboxylate (jasmolin 2)), the insecticidally active (2) A tolerance of 1.0 ppm is estab- principles of Chrysanthemum lished for residues of the insecticide cinerariaefolium, which are measured pyrethrins in or on milled fractions de- as cumulative residues of pyrethrin 1, rived from grain, cereal when present cinerin 1, and jasmolin 1 are not to ex- as a result of its use in cereal grain ceed the following: mills and in storage areas for milled cereal grain products. Commodity Parts per (3) A tolerance of 1.0 ppm is estab- million lished for residues of the insecticide Almond, postharvest ...... 1 .0 pyrethrins in or on all food items in Apple, postharvest ...... 1 .0 food handling establishments where Barley, grain, postharvest ...... 3 .0 Bean, succulent, postharvest ...... 1.0 food and food products are held, proc- Birdseed, mixtures, postharvest ...... 3 .0 essed, prepared and/or served. Food

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must be removed or covered prior to established as follows: 50 parts per mil- use. lion in or on Fruit, citrus. (4) Where tolerances are established (b) Section 18 emergency exemptions. on both the raw agricultural commod- [Reserved] ities and processed foods made there- (c) Tolerances with regional registra- from, the total residues of pyrethrins tions. [Reserved] in or on the processed food shall not be (d) Indirect or inadvertent residues. greater than that permitted by the [Reserved] larger of the two tolerances. (b) Section 18 emergency exemptions. [64 FR 39077, July 21, 1999] [Reserved] § 180.132 Thiram; tolerances for resi- (c) Tolerances with regional registra- dues. tions. [Reserved] (d) Indirect or inadvertent residues. (a) General. (1) A tolerances for resi- [Reserved] dues of the fungicide thiram (tetramethyl thiuram disulfide), in- [71 FR 74814, Dec. 13, 2006, as amended at 73 cluding its metabolites and degradates, FR 5108, Jan. 29, 2008] in or on the commodities in the table in this paragraph. Compliance with the § 180.129 o-Phenylphenol and its sodium salt; tolerances for residues. tolerance level specified in this paragraph is to be determined by measuring (a) General. Tolerances are estab- only thiram. lished for combined residues of the fungicide o-phenylphenol and sodium o- Commodity Parts phenylphenate, each expressed as o- per million phenylphenol, from postharvest appli- Avocado 1 ...... 15 cation of either in or on the following 1 food commodities: No U.S. registrations as of September 23, 2009. (2) Tolerances are established for res- Parts per Commodity million idues of the fungicide thiram, tetramethyl thiuram disulfide, includ- Apple ...... 25 ing its metabolites and degradates, in Cantaloupe (NMT 10 ppm in edible portion) ...... 125 or on the commodities in the table in Carrot, roots ...... 20 Cherry ...... 5 this paragraph. Compliance with the Citrus fruits ...... 10 tolerance levels specified in this para- Cucumber ...... 10 graph is to be determined by measuring Lemon ...... 10 only those thiram residues convertible Nectarine ...... 5 Orange ...... 10 to and expressed in terms of the Pepper, bell ...... 10 degradate carbon disulfide, in or on the Peach ...... 20 commodity. Pear ...... 25 .0 Pineapple ...... 10 Commodity Parts Plum, prune, fresh ...... 20 per million Sweet potato, roots ...... 15 Tomato ...... 10 Apple ...... 5 Banana 1 ...... 2.0 (b) Section 18 emergency exemptions. Peach ...... 7 .0 [Reserved] Strawberry ...... 13 (c) Tolerances with regional registra- 1 There are no U.S. registrations as of September 23, 2009. tions. [Reserved] (b) Section 18 emergency exemptions. (d) Indirect or inadvertent residues. [Reserved] [Reserved] (c) Tolerances with regional registra- [73 FR 54960, Sept. 24, 2008] tions. [Reserved] (d) Indirect or inadvertent residues. § 180.130 Hydrogen Cyanide; toler- [Reserved] ances for residues. [67 FR 49615, July 31, 2002, as amended at 74 (a) General. A tolerance for residues FR 48391, Sept. 23, 2009; 79 FR 8301, Feb. 12, of the insecticide hydrogen cyanide 2014; 79 FR 18822, Apr. 4, 2014; 80 FR 16306, from postharvest fumigation as a re- Mar. 27, 2015; 80 FR 35252, June 19, 2015; 80 FR sult of application of sodium cyanide is 72597, Nov. 20, 2015]

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§ 180.142 2,4-D; tolerances for residues. Parts per Commodity million (a) General. Tolerances are established for residues of the herbicide, Sheep, meat ...... 0.3 Sheep, meat byproducts, except kidney ...... 0 .3 plant regulator, and fungicide 2,4-D, in- Shellfish ...... 1 .0 cluding its metabolites and degradates, Sorghum, grain, forage ...... 0.2 in or on the commodities in the table Sorghum, grain, grain ...... 0 .2 Sorghum, grain, stover ...... 0 .2 below. Compliance with the tolerance Soybean, forage ...... 0 .02 levels is to be determined by meas- Soybean, hay ...... 2 .0 uring residues of 2,4-D (2,4- Soybean, seed ...... 0 .02 dichlorophenoxyacetic acid), both free Strawberry ...... 0 .05 Sugarcane, cane ...... 0.05 and conjugated, determined as the Sugarcane, molasses ...... 0 .2 acid, in or on the following commod- Teff, bran ...... 4.0 ities: Teff, forage ...... 25.0 Teff, grain ...... 2 .0 Parts per Teff, straw ...... 50 .0 Commodity million Vegetable, leaves of root and tuber, group 2 ..... 0 .1 Vegetable, root and tuber, except potato, group Almond hulls ...... 0 .1 1 ...... 0 .1 Asparagus ...... 5.0 Wheat, bran ...... 4.0 Barley, bran ...... 4 .0 Wheat, forage ...... 25 Barley, grain ...... 2 .0 Wheat, grain ...... 2 .0 Barley, straw ...... 50 Wheat, straw ...... 50 Berry, group 13 ...... 0 .2 Cattle, fat ...... 0.3 (b) Section 18 emergency exemptions. Cattle, kidney ...... 4 .0 Cattle, meat ...... 0 .3 [Reserved] Cattle, meat byproducts, except kidney ...... 0.3 (c) Tolerances with regional registra- Corn, field, forage ...... 6 .0 tions. Tolerances with regional reg- Corn, field, grain ...... 0 .05 Corn, field, stover ...... 50 istration, as defined in § 180.1(l), are es- Corn, pop, grain ...... 0.05 tablished for residues of the herbicide, Corn, pop, stover ...... 50 plant regulator, and fungicide 2,4-D, in- Corn, sweet, forage ...... 6 .0 cluding its metabolites and degradates, Corn, sweet, kernel plus cob with husks removed ...... 0 .05 in or on the commodities in the table Corn, sweet, stover ...... 50 below. Compliance with the tolerance Cranberry ...... 0 .5 levels is to be determined by meas- Fish ...... 0 .1 Fruit, citrus, group 10 ...... 3 .0 uring residues of 2,4-D (2,4- Fruit, pome, group 11 ...... 0.05 dichlorophenoxyacetic acid), both free Fruit, stone, group 12 ...... 0 .05 and conjugated, determined as the Goat, fat ...... 0 .3 acid, in or on the follow commodities: Goat, kidney ...... 4 .0 Goat, meat ...... 0.3 Parts per Goat, meat byproducts, except kidney ...... 0 .3 Commodity million Grain, aspirated fractions ...... 40 Grape ...... 0 .05 Rice, wild, grain ...... 0.05 Grass, forage ...... 360 Grass, hay ...... 300 Hop, dried cones ...... 0 .2 (d) Indirect or inadvertent residues. Horse, fat ...... 0 .3 Tolerances are established for indirect Horse, kidney ...... 4 .0 or inadvertent residues of the herbi- Horse, meat ...... 0 .3 cide, plant regulator, and fungicide 2,4- Horse, meat byproducts, except kidney ...... 0 .3 Millet, forage ...... 25 D, including its metabolites and Millet, grain ...... 2 .0 degradates, in or on the commodities Millet, straw ...... 50 in the table below. Compliance with Milk ...... 0.05 Nut, tree, group 14 ...... 0 .2 the tolerances levels is to be deter- Oat, forage ...... 25 mined by measuring residues of 2,4-D Oat, grain ...... 2 .0 (2,4-dichlorophenoxyacetic acid), both Oat, straw ...... 50 free and conjugated, determined as the Pistachio ...... 0.05 Potato ...... 0 .4 acid, in or on the following commod- Rice, grain ...... 0 .5 ities: Rice, hulls ...... 2 .0 Rye, bran ...... 4 .0 Parts per Rye, forage ...... 25 Commodity million Rye, grain ...... 2.0 Rye, straw ...... 50 Animal feed, nongrass, group 18 ...... 0 .2 Sheep, fat ...... 0 .3 Avocado ...... 0 .05 Sheep, kidney ...... 4.0 Cotton, undelinted seed ...... 0 .05

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Parts per Parts per Commodity million Commodity million

Dill, seed ...... 0 .05 All processed food commodities not otherwise Okra ...... 0.05 listed ...... 70 Vegetable, brassica leafy, group 5 ...... 0 .4 Barley, bran, postharvest ...... 45 .0 Vegetable, bulb, group 3 ...... 0 .05 Barley, flour, postharvest ...... 45.0 Vegetable, cucurbit, group 9 ...... 0.05 Barley, grain, postharvest ...... 15 .0 Vegetable, foliage of legume, group 7 ...... 0 .2 Barley, pearled barley, postharvest ...... 45.0 Cattle, meat, dried ...... 40 Vegetable, fruiting, group 8 ...... 0.05 Cheese ...... 5 .0 Vegetable, leafy, except brassica, group 4 ...... 0 .4 Cacao bean, roasted bean, postharvest ...... 20 Vegetable, legume, group 6 ...... 0 .05 Coconut, postharvest ...... 40 Coffee, bean, green, postharvest ...... 15 Corn, field, flour, postharvest ...... 35 .0 [72 FR 52017, Sept. 12, 2007, as amended at 73 Corn, field, grain, postharvest ...... 10.0 FR 53737, Sept. 17, 2008; 74 FR 48411, Sept. 23, Corn, field, grits, postharvest ...... 10.0 2009; 76 FR 55817, Sept. 9, 2011; 80 FR 72597, Corn, field, meal, postharvest ...... 30 .0 Nov. 20, 2015] Corn, pop, grain, postharvest ...... 10 .0 Cotton, undelinted seed, postharvest ...... 70 Egg, dried ...... 900 § 180.145 Fluorine compounds; toler- Fruit, dried, except grape, raisin, postharvest ..... 3 .0 ances for residues. Ginger, postharvest ...... 70 (a) General. (1) Tolerances are estab- Grain, aspirated fractions, postharvest ...... 55 .0 Grape, raisin, postharvest ...... 7 .0 lished for combined residues of the in- Hog, meat ...... 20 secticidal fluorine compounds cryolite Herbs and spices group 19, postharvest ...... 70 and synthetic cryolite (sodium alu- Milk, powdered ...... 5 .0 Millet, grain, postharvest ...... 40.0 minum fluoride) in or on the following Nut, pine, postharvest ...... 20 agricultural commodities: Nut, tree, Group 14, postharvest ...... 10 .0 Oat, flour, postharvest ...... 75 .0 Oat, grain, postharvest ...... 25 .0 Commodity Parts per million Oat, groats/rolled oats ...... 75 .0 Peanut, postharvest ...... 15 Apricot ...... 7 Pistachio, postharvest ...... 10 .0 Blackberry ...... 7 Rice, bran, postharvest ...... 31 .0 Blueberry ...... 7 Rice, flour, postharvest ...... 45 Boysenberry ...... 7 Rice, grain, postharvest ...... 12.0 Broccoli ...... 7 Rice, hulls, postharvest ...... 35.0 Brussels sprouts ...... 7 Rice, polished rice, postharvest ...... 25.0 Cabbage ...... 7 Rice, wild, grain, postharvest ...... 25 .0 Sorghum, grain, postharvest ...... 40.0 Cauliflower ...... 7 Triticale, grain, postharvest ...... 40.0 Collards ...... 7 Vegetable, legume, group 6, postharvest ...... 70 Cranberry ...... 7 Wheat, bran, postharvest ...... 40 .0 Cucumber ...... 7 Wheat, flour, postharvest ...... 125 .0 Dewberry ...... 7 Wheat, germ, postharvest ...... 130 .0 Eggplant ...... 7 Wheat, grain, postharvest ...... 40.0 Fruit, citrus ...... 7 Wheat, milled byproducts, postharvest ...... 130.0 Grape ...... 7 Wheat, shorts, postharvest ...... 40.0 Kale ...... 7 Kohlrabi ...... 7 (b) Section 18 emergency exemptions. Lettuce, head ...... 7 [Reserved] Lettuce, leaf ...... 7 Loganberry ...... 7 (c) Tolerances with regional registra- Melon ...... 7 tions. Tolerances with regional reg- Nectarine ...... 7 istration, as defined by § 180.1(l), are es- Peach ...... 7 tablished for the combined residues of Pepper ...... 7 Plum, prune, fresh ...... 7 the insecticidal fluorine compounds, Pumpkin ...... 7 cryolite and synthetic cryolite (sodium Raspberry ...... 7 aluminum fluoride), in or on the fol- Squash, summer ...... 7 lowing raw agricultural commodities: Squash, winter ...... 7 Strawberry ...... 7 Parts per Tomato ...... 7 Commodity million Youngberry ...... 7 Kiwifruit ...... 15 (2) Tolerances are established for residues of fluoride in or on the following (d) Indirect or inadvertent residues. commodities from the postharvest fu- [Reserved] migation with sulfuryl fluoride for the [71 FR 74815, Dec. 13, 2006, as amended at 76 control of insects: FR 34885, June 15, 2011]

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§ 180.151 Ethylene oxide; tolerances Commodity Parts per mil- for residues. lion (a) General. (1) Tolerances are estab- Caneberry subgroup 13-07A ...... 0.75 lished for residues of the antimicrobial Carrot, roots ...... 0.75 Cattle, fat ...... 0.50 agent and insecticide ethylene oxide, Cherry, sweet ...... 0 .20 when used as a postharvest fumigant in Cherry, tart ...... 0 .20 or on the following food commodities: Cranberry ...... 0 .50 Endive ...... 0.70 Fig ...... 0 .50 Parts per Commodity million Ginseng ...... 0 .75 Grape ...... 0 .75 2 Herb and spice, group 19, dried, except basil .... 7 Hazelnut ...... 0 .50 1 Licorice, roots ...... 7 Kiwifruit ...... 0.75 Peppermint, tops, dried ...... 7 Lettuce ...... 0.70 Sesame, seed ...... 7 Melon ...... 0 .75 2 Spearmint, tops, dried ...... 7 Mushroom ...... 0 .75 Vegetable, dried ...... 7 Nectarine ...... 0 .20 Walnut ...... 50 Onion, bulb ...... 0 .75 Onion, green ...... 0 .75 Pea, succulent ...... 0 .50 (2) Tolerances are established for res- Peach ...... 0 .20 idues of the ethylene oxide reaction Pear ...... 0 .50 product, 2-chloroethanol, commonly Pineapple ...... 0.50 Plum, prune, fresh ...... 0.20 referred to as ethylene chlorohydrin, Radish ...... 0 .50 when ethylene oxide is used as a Rutabaga ...... 0 .75 postharvest fumigant in or on food Spinach ...... 0 .70 Strawberry ...... 0 .50 commodities as follows: Tomato ...... 0.75 Vegetable, brassica, leafy, group 5 ...... 0.70 Parts per Watercress ...... 0 .05 Commodity million 1There are no domestic registrations for kiwifruit as of Herb and spice, group 19, dried, except basil .... 940 March 6, 2002. Licorice, roots ...... 940 2The expiration/revocation date for this tolerance is 9/10/ Peppermint, tops, dried ...... 940 2010. Sesame, seed ...... 940 (b) Section 18 emergency exemptions. Spearmint, tops, dried ...... 940 Vegetable, dried ...... 940 [Reserved] (c) Tolerances with regional registra- (b) Section 18 emergency exemptions. tions. Tolerances with regional reg- [Reserved] istration, as defined in § 180.1(l), are es- (c) Tolerances with regional registra- tablished for residues of the insecticide tions. [Reserved] diazinon, O, O-diethyl O-[6-methyl-2-(1- (d) Indirect or inadvertent residues. methylethyl)-4-pyrimidinyl]- [Reserved] phosphorothioate (CAS No. 333–41–5), in [65 FR 33695, May 24, 2000, as amended at 74 or on the following food commodities: FR 46696, Sept. 11, 2009] Parts per Commodity million § 180.153 Diazinon; tolerances for residues. Almond ...... 0.50 Banana ...... 0.20 (a) General. Tolerances are estab- Celery ...... 0 .70 lished for residues of the insecticide Cucumber ...... 0 .75 Parsley, leaves ...... 0.75 diazinon, O,O-diethyl O-[6-methyl-2-(1- Parsnip ...... 0.50 methylethyl)-4- Pepper ...... 0 .5 pyrimidinyl]phosphorothioate (CAS Potato ...... 0 .10 No. 333–41–5), in or on the following Squash, summer ...... 0 .50 Squash, winter ...... 0 .75 food commodities: Sweet potato, roots ...... 0 .10 Swiss chard ...... 0.70 Commodity Parts per mil- Turnip, roots ...... 0 .50 lion Turnip, tops ...... 0.75 Almond, hulls ...... 3 .0 Apple ...... 0.50 (d) Indirect or inadvertent residues. Apricot ...... 0 .20 [Reserved] Bean, lima ...... 0 .50 Bean, snap, succulent ...... 0 .50 [47 FR 42738, Sept. 29, 1982] Beet, garden, roots ...... 0 .75 Beet, garden, tops ...... 0 .70 EDITORIAL NOTE: For FEDERAL REGISTER ci- Blueberry ...... 0 .50 tations affecting § 180.153, see the List of CFR

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Sections Affected, which appears in the metabolites and degradates in or on Finding Aids section of the printed volume the commodities in the following table. and at www.fdsys.gov. Compliance with the tolerance levels specified is to be determined by meas- § 180.154 Azinphos-methyl; tolerances for residues. uring only 1-naphthaleneacetic acid and its conjugates, calculated as the (a) General. Tolerances for residues of Stoichiometric equivalent of 1- the insecticide O,O-dimethyl S-[(4-oxo- naphthaleneacetic acid, in or on the 1,2,3-benzotriazin-3(4H)- commodity. yl)methyl]phosphorodithioate in or on the following raw agricultural com- Commodity Parts per modities: million Avocado ...... 0 .05 Parts per Expiration/ Cherry, sweet ...... 0 .1 Commodity Revocation Fruit, pome, group 11–10 ...... 0 .15 million Date Mango ...... 0.05 Olive ...... 0 .7 Almond1 ...... 0.2 None Orange ...... 0 .1 Almond, hulls1 ...... 5.0 None Pineapple1 ...... 0 .05 Apple2 ...... 1.5 None Pomegranate ...... 0 .05 Blackberry3 ...... 2.0 None Potato ...... 0 .01 Blueberry2 ...... 5.0 None Rambutan ...... 2 .0 Boysenberry3 ...... 2.0 None Sapote, mamey ...... 0 .05 Brussels sprouts4 ...... 2.0 None Tangerine ...... 0 .1 Cherry2 ...... 2.0 None Crabapple2 ...... 1.5 None 1 There are no U.S. registrations since 1988. Cranberry3 ...... 0.5 12/31/12 Loganberry3 ...... 2.0 None (b) Section 18 emergency exemptions. Parsley, leaves2 ...... 5.0 None [Reserved] Parsley, turnip rooted, roots2 ...... 2.0 None (c) Tolerances with regional registra- Peach3 ...... 2.0 None Pear2 ...... 1.5 None tions. [Reserved] Pistachio1 ...... 0.3 None (d) Indirect or inadvertent residues. Plum, prune5 ...... 2.0 None [Reserved] Quince5 ...... 1.5 None Raspberry3 ...... 2.0 None [78 FR 30218, May 22, 2013, as amended at 80 Walnut1 ...... 0.3 None FR 77260, Dec. 14, 2015]

1There are no U.S. registrations as of § 180.163 Dicofol; tolerances for resi- October 30, 2009. dues. 2There are no U.S. registrations as of (a) General. (1) Tolerances are estab- September 30, 2012. lished for residues of the insecticide 3There are no U.S. registrations since dicofol, including its metabolites and September 30, 2006. degradates, in or on the commodities 4There are no U.S. registrations since in the table in this paragraph. Compli- September 30, 2008. ance with the tolerance levels specified 5There are no U.S. registrations since in this paragraph is to be determined December 28, 2005. by measuring only dicofol as the sum (b) Section 18 emergency exemptions. of its p,p-dicofol and o,p-dicofol iso- [Reserved] mers: 4-chloro-a-(4-chlorophenyl)-a- (c) Tolerances with regional registra- (trichloromethyl)benzenemethanol and tions. [Reserved] 2-chloro-a-(4-chlorophenyl)-a- (d) Indirect or inadvertent residues. (trichloromethyl)benzenemethanol, in [Reserved] or on the commodity. [65 FR 38752, June 22, 2000, as amended at 74 Expiration/ FR 46697, Sept. 11, 2009] Commodity Parts per revocation million date EFFECTIVE DATE NOTE: At 81 FR 34905, June 1, 2016, § 180.154 was removed, effective Nov. Apple, wet pomace ...... 38.0 10/31/16 28, 2016. Bean, dry, seed ...... 0.5 10/31/16 Bean, succulent ...... 3.0 10/31/16 § 180.155 1-Naphthaleneacetic acid; tol- Butternut ...... 0.1 10/31/16 Caneberry subgroup 13A ...... 5.0 10/31/16 erances for residues. Chestnut ...... 0.1 10/31/16 (a) General. Tolerances are estab- Citrus, dried pulp ...... 12.0 10/31/16 Citrus oil ...... 200.0 10/31/16 lished for the residues of 1- Cotton, refined oil ...... 0.5 10/31/16 naphthaleneacetic acid, including its Cotton, undelinted seed ...... 0.1 10/31/16

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Expiration/ Expiration/ Commodity Parts per revocation Commodity Parts per Revocation million date million Date

Fruit, citrus, group 10 ...... 6.0 10/31/16 Horse, meat byproducts, except Fruit, pome, group 11 ...... 10.0 10/31/16 liver ...... 3.0 10/31/16 Fruit, stone, group 12 ...... 5.0 10/31/16 Milk, fat (reflecting 0.75 ppm in Grape ...... 5.0 10/31/16 whole milk) ...... 22.0 10/31/16 Grape, raisin ...... 20.0 10/31/16 Poultry, fat ...... 0.1 10/31/16 Hazelnut ...... 0.1 10/31/16 Poultry, meat ...... 0.1 10/31/16 Hop, dried cones ...... 65.0 10/31/16 Poultry, meat byproducts ...... 0.1 10/31/16 Nut, hickory ...... 0.1 10/31/16 Sheep, fat ...... 50.0 10/31/16 Nut, macadamia ...... 0.1 10/31/16 Sheep, liver ...... 5.0 10/31/16 Pecan ...... 0.1 10/31/16 Sheep, meat ...... 3.0 10/31/16 Peppermint, oil ...... 30.0 10/31/16 Sheep, meat byproducts, except Peppermint, tops ...... 25.0 10/31/16 liver ...... 3.0 10/31/16 Spearmint, oil ...... 30.0 10/31/16 Spearmint, tops ...... 25.0 10/31/16 (b) Section 18 emergency exemptions. Strawberry ...... 10.0 10/31/16 Tea, dried ...... 50.0 None [Reserved] Tea, plucked leaves ...... 30.0 None (c) Tolerances with regional registra- Vegetable, cucurbit, group 9 ...... 2.0 10/31/16 tions. [Reserved] Vegetable, fruiting, group 8 ...... 2.0 10/31/16 Walnut ...... 0.1 10/31/16 (d) Indirect or inadvertent residues. [Reserved] (2) Tolerances are established for res- [63 FR 34826, June 26, 1998, as amended at 72 idues of the insecticide dicofol, includ- FR 35665, June 29, 2007; 72 FR 41928, Aug. 1, ing its metabolites and degradates, in 2007; 77 FR 59124, Sept. 26, 2012] or on the commodities in the table in this paragraph. Compliance with the § 180.169 Carbaryl; tolerances for resi- tolerance levels specified in this para- dues. graph is to be determined by measuring (a) General. (1) Tolerances are estab- only the sum of p,p-dicofol, 4-chloro-a- lished for residues of the insecticide (4-chlorophenyl)-a- carbaryl, 1-naphthyl N- (trichloromethyl)benzenemethanol, its methylcarbamate per se, in or on the isomer o,p-dicofol, 2-chloro-a-(4- following food commodities: chlorophenyl)-a- (trichloromethyl)benzenemethanol, Expiration/ Commodity Parts per revocation and its metabolites 4-chloro-a-(4- million date chlorophenyl)-a- Alfalfa, forage ...... 50 None (dichloromethyl)benzenemethanol and Alfalfa, hay ...... 75 None 2-chloro-a-(4-chlorophenyl)-a- Almond, hulls ...... 50 None (dichloromethyl)benzenemethanol, cal- Apple, wet pomace ...... 15 None culated as the stoichiometric equiva- Asparagus ...... 15 None Banana ...... 5.0 None lent of p,p-dicofol, 4-chloro-a-(4- Beet, sugar, roots ...... 0.5 None chlorophenyl)-a- Beet, sugar, tops ...... 25 None (trichloromethyl)benzenemethanol, in Bushberry subgroup 13-07B ...... 3.0 None Cabbage ...... 21 None or on the commodity. Cactus, fruit ...... 5.0 None Cactus, pads ...... 12 None Expiration/ Caneberry subgroup 13-07A ...... 12.0 None Commodity Parts per Revocation million Date Citrus, oil ...... 20 None Clover, forage ...... 50 None Cattle, fat ...... 50.0 10/31/16 Clover, hay ...... 70 None Cattle, liver ...... 5.0 10/31/16 Corn, field, forage ...... 30 None Cattle, meat ...... 3.0 10/31/16 Corn, field, grain ...... 0.02 None Cattle, meat byproducts, except Corn, field, stover ...... 20 None liver ...... 3.0 10/31/16 Corn, pop, grain ...... 0.02 None Egg ...... 0.05 10/31/16 Corn, pop, stover ...... 20 None Goat, fat ...... 50.0 10/31/16 Corn, sweet, forage ...... 185 None Goat, liver ...... 5.0 10/31/16 Corn, sweet, kernel plus cob with Goat, meat ...... 3.0 10/31/16 husks removed ...... 0.1 None Goat, meat byproducts, except liver 3.0 10/31/16 Corn, sweet, stover ...... 215 None Hog, fat ...... 50.0 10/31/16 Cotton, undelinted seed ...... 5.0 10/31/09 Hog, liver ...... 5.0 10/31/16 Cranberry ...... 3.0 None Hog, meat ...... 3.0 10/31/16 Dandelion, leaves ...... 22 None Hog, meat byproducts, except liver 3.0 10/31/16 Endive ...... 10 None Horse, fat ...... 50.0 10/31/16 Flax, seed ...... 0.5 None Horse, liver ...... 5.0 10/31/16 Fruit, citrus, group 10 ...... 10 None Horse, meat ...... 3.0 10/31/16 Fruit, pome, group 11 ...... 12 None

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Expiration/ Expiration/ Commodity Parts per revocation Commodity Parts per revocation million date million date

Fruit, stone, group 12 ...... 10 None Cattle, fat ...... 0.5 None Grain, aspirated fractions ...... 70 None Cattle, meat ...... 1.0 None Grape ...... 10 None Cattle, meat byproducts ...... 3.0 None Grape, raisin ...... 12 None Egg ...... 0.5 10/31/09 Grass, forage ...... 100 None Goat, fat ...... 0.5 None Grass, hay ...... 15 None Goat, meat ...... 1.0 None Leaf petiole subgroup 4B ...... 3.0 None Goat, meat byproducts ...... 3.0 None Lettuce ...... 10 None Hog, fat ...... 0.5 None Millet, proso, grain ...... 1.0 None Hog, meat ...... 1.0 None Millet, proso, straw ...... 20 None Hog, meat byproducts ...... 3.0 None Horse, fat ...... 0.5 None Nut, tree group 14, except walnut ... 0.1 None Horse, meat ...... 1.0 None Okra ...... 4.0 None Horse, meat byproducts ...... 3.0 None Olive ...... 10 None Milk ...... 1.0 None Oyster ...... 0.25 None Poultry, fat ...... 5.0 10/31/09 Parsley, leaves ...... 22 None Poultry, meat ...... 5.0 10/31/09 Pea and bean, dried shelled, except Sheep, fat ...... 0.5 None soybean, subgroup 6C ...... 1.0 None Sheep, meat ...... 1.0 None Peanut ...... 0.05 None Sheep, meat byproducts ...... 3.0 None Peanut, hay ...... 20 None Pineapple ...... 2.0 None Pistachio ...... 0.1 None (b) Section 18 emergency exemptions. Rice, grain ...... 15 None [Reserved] Rice, hulls ...... 30 None (c) Tolerances with regional registra- Sorghum grain, forage ...... 30 None tions. Tolerances with regional reg- Sorghum grain, grain ...... 10 None Sorghum grain, stover ...... 30 None istrations, as defined in § 180.1(l), are Soybean, forage ...... 15 None established for residues of the insecti- Soybean, hay ...... 15 None cide carbaryl, 1-naphthyl N- Soybean, seed ...... 0.5 None methylcarbamate per se, in or on the Spinach ...... 22 None Strawberry ...... 4.0 None following food commodities: Sunflower, seed ...... 0.5 None Sweet potato, roots ...... 0.2 None Parts per Commodity million Trefoil, forage ...... 15 None Trefoil, hay ...... 25 None Dillweed, fresh leaves ...... 0 .2 Vegetable, brassica, leafy, group 5, except cabbage ...... 10 None Vegetable, cucurbit, group 9 ...... 3.0 None (d) Indirect or inadvertent residues. Vegetable, foliage of legume, sub- [Reserved] group 7A, except soybean ...... 60 None Vegetable, fruiting, group 8 ...... 5.0 None [65 FR 33695, May 24, 2000, as amended at 66 Vegetable, leaves of root and tuber, FR 38955, July 26, 2001; 67 FR 49615, July 31, group 2, except sugar beet tops 75 None 2002; 70 FR 44492, Aug. 3, 2005; 73 FR 52611, Vegetable, legume, edible podded, Sept. 10, 2008; 74 FR 10490, Mar. 11, 2009; 80 FR subgroup 6A ...... 10 None 72597, Nov. 20, 2015] Vegetable, root and tuber, group 1, except sugar beet and sweet potato ...... 2.0 None § 180.172 Dodine; tolerances for resi- Walnut ...... 1.0 None dues. Wheat, forage ...... 30 None (a) General. Tolerances are estab- Wheat, grain ...... 1.0 None Wheat, hay ...... 30 None lished for residues of the fungicide Wheat, straw ...... 20 None dodine, including its metabolites and degradates, in or on the commodities (2) Tolerances are established for res- listed in the table below. Compliance idues of the insecticide carbaryl, 1- with the tolerance levels specified in naphthyl N-methylcarbamate, includ- the table is to be determined by meas- ing its metabolites: 1-naphthol uring only dodine, N-dodecylguanidine (naphthyl-sulfate); 5,6- acetate; in or on the following com- dihydrodihydroxycarbaryl; and 5,6- modities. dihydrodihydroxy naphthol, calculated as 1-naphthyl N-methylcarbamate and Commodity Parts per million the free and conjugated residues of carbaryl: 5,6-dihydro-5,6-dihydroxy Almond, hull ...... 30 .0 carbaryl and 5-methoxy-6-hydroxy Apple ...... 5.0 Apple, wet pomace ...... 15.0 carbaryl, in or on the following food Banana ...... 0.50 commodities: Fruit, stone, crop group 12 ...... 5 .0

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Commodity Parts per § 180.176 Mancozeb; tolerances for res- million idues. Nuts, tree, crop group 14 ...... 0 .3 (a) General. Tolerances are estab- Peanut ...... 0 .013 lished for residues of mancozeb (a co- Pear ...... 5 .0 Strawberry ...... 5 .0 ordination product of zinc ion and maneb (manganese (b) Section 18 emergency exemptions. ethylenebisdithiocarbamate)), includ- [Reserved] ing its metabolites and degradates, in (c) Tolerances with regional registra- or on the commodities in the following tions. [Reserved] table. Compliance with the tolerance (d) Indirect or inadvertent residues. levels specified in this paragraph is to [Reserved] be determined by measuring only those [72 FR 52017, Sept. 12, 2007, as amended at 73 mancozeb residues convertible to and FR 45634, Aug. 6, 2008; 77 FR 72237, Dec. 5, expressed in terms of the degradate 2012] carbon disulfide.

Parts § 180.175 Maleic hydrazide; tolerances Commodity per million for residues. (a) General. (1) Tolerances for resi- Almond ...... 0.1 Almond, hulls ...... 4 dues of the herbicide and plant regu- Apple ...... 0.6 lator maleic hydrazide (1,2-dihydro-3,6- Asparagus ...... 0.1 pyridazinedione) are established in or Atemoya ...... 3 .0 Banana ...... 2 on the following raw agricultural com- Barley, bran ...... 2 modities: Barley, flour ...... 1 .2 Barley, grain ...... 1 Barley, hay ...... 30 Commodity Parts per million Barley, pearled barley ...... 20 Barley, straw ...... 25 Onion, bulb ...... 15.0 Beet, sugar, dried pulp ...... 3 .0 Potato ...... 50.0 Beet, sugar, roots ...... 1 .2 Beet, sugar, tops ...... 60 (2) A food additive known as maleic Broccoli ...... 7 Cabbage ...... 9 hydrazide (1,2-dihydro-3,6- Canistel ...... 15 .0 pyridazinedione) may be present in po- Cattle, kidney ...... 0 .5 tato, chips when used in accordance Cattle, liver ...... 0 .5 Cherimoya ...... 3 .0 with the following conditions: Corn, field, forage ...... 40 (i) The food additive is present as a Corn, field, grain ...... 0 .06 result of the application of a pesticide Corn, field, stover ...... 15 formulation containing maleic hydra- Corn, pop, grain ...... 0.1 Corn, pop, stover ...... 40 zide to the growing potato plant in ac- Corn, sweet, forage ...... 70 cordance with directions registered by Corn, sweet, kernel plus cob with husks re- the U.S. Environmental Protection moved ...... 0 .1 Corn, sweet, stover ...... 40 Agency. Cotton, undelinted seed ...... 0 .5 (ii) The label of the pesticide formu- Crabapple ...... 0 .6 lation containing the food additive Cranberry ...... 5 Custard apple ...... 3 .0 conforms to labeling registered by the Fennel ...... 2.5 U.S. Environmental Protection Agen- Flax, seed ...... 0 .15 cy. Ginseng ...... 1 .2 (iii) The food additive is present in an Goat, kidney ...... 0 .5 Goat, liver ...... 0.5 amount not to exceed 160 parts per mil- Grape ...... 1 .5 lion by weight of the finished food. Hog, kidney ...... 0.5 (b) Section 18 emergency exemptions. Hog, liver ...... 0 .5 Horse, kidney ...... 0 .5 [Reserved] Horse, liver ...... 0 .5 (c) Tolerances with regional registra- Lettuce, head ...... 3.5 tions. [Reserved] Lettuce, leaf ...... 18 (d) Indirect or inadvertent residues. Mango ...... 15.0 Oat, flour ...... 1 .2 [Reserved] Oat, grain ...... 1 Oat, groats/rolled oats ...... 20 [62 FR 64293, Dec. 5, 1997, as amended at 64 Oat, hay ...... 30 FR 11792, Mar. 10, 1999; 67 FR 35048, May 17, Oat, straw ...... 25 2002] Onion, bulb ...... 1 .5

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(d) Indirect or inadvertent residues. Commodity Parts per million [Reserved] Papaya ...... 9 [65 FR 33708, May 24, 2000, as amended at 65 Peanut ...... 0 .1 FR 49924, Aug. 16, 2000; 66 FR 64773, Dec. 14, Peanut, hay ...... 65 2001; 68 FR 2247, Jan. 16, 2003; 69 FR 29458, Pear ...... 0 .6 May 24, 2004; 71 FR 76199, Dec. 20, 2006; 74 FR Pepper ...... 12 46372, Sept. 9, 2009; 75 FR 770, Jan. 6, 2010; 75 Potato ...... 0 .2 FR 50913, Aug. 18, 2010; 76 FR 18915, Apr. 6, Poultry, kidney ...... 0 .5 2011; 78 FR 44455, July 24, 2013; 79 FR 27501, Poultry, liver ...... 0 .5 May 14, 2014; 80 FR 72597, Nov. 20, 2015] Quince ...... 0 .6 Rice, grain ...... 0 .06 § 180.178 Ethoxyquin; tolerances for Rye, bran ...... 2 residues. Rye, flour ...... 1 .2 Rye, grain ...... 1 (a) General. A tolerance is established Rye, straw ...... 25 for residues of the plant regulator Sapodilla ...... 15 .0 ethoxyquin (1,2-dihydro-6-ethoxy-2,2,4- Sapote, mamey ...... 15 .0 trimethylquinoline) from preharvest or Sapote, white ...... 15 .0 postharvest use in or on the following Sheep, kidney ...... 0.5 Sheep, liver ...... 0.5 commodity: Sorghum, grain, forage ...... 0.15 Parts per Sorghum, grain, grain ...... 0 .25 Commodity million Sorghum, grain, stover ...... 0 .15 Star apple ...... 15 .0 Pear ...... 3 Sugar apple ...... 3 .0 Tangerine 1 ...... 10 (b) Section 18 emergency exemptions. Tomato ...... 2.5 [Reserved] Vegetable, cucurbit, group 9 ...... 2.0 (c) Tolerances with regional registra- Walnut ...... 0 .70 tions. [Reserved] Wheat, bran ...... 2 Wheat, flour ...... 1 .2 (d) Indirect or inadvertent residues. Wheat, germ ...... 20 [Reserved] Wheat, grain ...... 1 [63 FR 57073, Oct. 26, 1998] Wheat, hay ...... 30 Wheat, middlings ...... 20 § 180.181 Chlorpropham; tolerances for Wheat, shorts ...... 2 residues. Wheat, straw ...... 25 (a) General. (1) Tolerances are estab- 1 There are no U.S. registrations for use of mancozeb on tangerine. lished for residues of the plant regulator and herbicide chlorpropham (iso- (b) Section 18 emergency exemptions. propyl m-chlorocarbanilate (CIPC) in [Reserved] or on the following food commodities: (c) Tolerances with regional registrations. A tolerance with regional reg- Parts per Commodity million istrations, as defined in § 180.1(l), is established for residues of the fungicide Potato ...... 30 mancozeb, (a coordination product of Potato, wet peel ...... 40 zinc ion and maneb (manganese (2) Tolerances are established for the ethylenebisdithiocarbamate)), includ- combined residues of the plant regu- ing its metabolites and degradates, in lator and herbicide chlorpropham (iso- or on the commodity in the following propyl m-chlorocarbanilate (CIPC) and table in this paragraph. Compliance its metabolite 4-hydroxychlorpropham- with the tolerance levels specified in O-sulfonic acid (4-HSA) in or on the fol- this paragraph is to be determined by lowing food commodities: measuring only those mancozeb residues convertible to and expressed in Parts per Commodity million terms of the degradate carbon disulfide. Cattle, fat ...... 0.20 Cattle, kidney ...... 0 .30 Cattle, meat ...... 0 .06 Parts per Commodity million Cattle, meat byproducts except kidney ...... 0 .06 Goat, fat ...... 0 .20 Carrot, roots ...... 1 Goat, kidney ...... 0 .30 Goat, meat ...... 0.06

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Parts per Expiration/ Commodity million Commodity Parts per revocation million date Goat, meat byproducts except kidney ...... 0 .06 Hog, fat ...... 0 .20 Cattle, liver ...... 5.0 7/31/16 Hog, kidney ...... 0.30 Cattle, meat ...... 2.0 7/31/16 Hog, meat ...... 0 .06 Cattle, meat byproducts, except Hog, meat byproducts except kidney ...... 0 .06 liver ...... 1.0 7/31/16 Horse, fat ...... 0 .20 Cauliflower ...... 2.0 7/31/12 Horse, kidney ...... 0 .30 Celery ...... 8.0 7/31/12 Horse, meat ...... 0 .06 Cherry, sweet ...... 2.0 7/31/12 Horse, meat byproducts except kidney ...... 0.06 Cherry, tart ...... 2.0 7/31/12 Milk ...... 0.30 Collards ...... 2.0 7/31/12 Sheep, fat ...... 0 .20 Cotton, gin byproducts ...... 30.0 7/31/12 Sheep, kidney ...... 0.30 Cotton, undelinted seed ...... 1.0 7/31/12 Sheep, meat ...... 0.06 Cucumber ...... 1.0 7/31/12 Sheep, meat byproducts except kidney ...... 0 .06 Eggplant ...... 1.0 7/31/12 Goat, fat ...... 13.0 7/31/16 (b) Section 18 emergency exemptions. Goat, liver ...... 5.0 7/31/16 Goat, meat ...... 2.0 7/31/16 [Reserved] Goat, meat byproducts, except liver 1.0 7/31/16 (c) Tolerances with regional registra- Hazelnut ...... 0.2 7/31/12 tions. [Reserved] Hog, fat ...... 13.0 7/31/16 (d) Indirect or inadvertent residues. Hog, liver ...... 5.0 7/31/16 Hog, meat ...... 2.0 7/31/16 [Reserved] Hog, meat byproducts, except liver 1.0 7/31/16 [43 FR 52487, Nov. 13, 1978, as amended at 63 Horse, fat ...... 13.0 7/31/16 Horse, liver ...... 5.0 7/31/16 FR 57073, Oct. 26, 1998; 72 FR 37653, July 11, Horse, meat ...... 2.0 7/31/16 2007] Horse, meat byproducts, except liver ...... 1.0 7/31/16 § 180.182 Endosulfan; tolerances for Kale ...... 2.0 7/31/12 residues. Lettuce, head ...... 11.0 7/31/12 Lettuce, leaf ...... 6.0 7/31/12 (a)(1) General. Tolerances are estab- Milk, fat ...... 2.0 7/31/16 lished for residues of the insecticide Muskmelon ...... 1.0 7/31/12 endosulfan, including its metabolites Mustard greens ...... 2.0 7/31/12 Mustard, seed ...... 0.2 7/31/12 and degradates, in or on the commod- Nectarine ...... 2.0 7/31/12 ities in the table in this paragraph. Nut, macadamia ...... 0.2 7/31/12 Compliance with the tolerance levels Peach ...... 2.0 7/31/12 Pear ...... 2.0 7/31/13 specified in this paragraph is to be de- Pineapple ...... 1.0 7/31/16 termined by measuring only the sum of Pineapple, process residue ...... 20.0 7/31/16 endosulfan, 6,7,8,9,10,10-hexachloro- Plum ...... 2.0 7/31/12 1,5,5a,6,9,9a-hexahydro-6,9-methano- Plum, prune ...... 2.0 7/31/12 Sheep, fat ...... 13.0 7/31/16 2,4,3-benzodioxathiepin 3-oxide (alpha Sheep, liver ...... 5.0 7/31/16 and beta isomers), and its metabolite Sheep, meat ...... 2.0 7/31/16 endosulfan sulfate, 6,7,8,9,10,10- Sheep, meat byproducts, except liver ...... 1.0 7/31/16 hexachloro-1,5,5a,6,9,9a-hexahydro-6,9- Squash, summer ...... 1.0 7/31/12 methano-2,4,3-benzodioxathiepin-3,3-di- Strawberry ...... 2.0 7/31/16 oxide, calculated as the stoichiometric Sweet potato, roots ...... 0.15 7/31/12 equivalent of endosulfan, in or on the Walnut ...... 0.2 7/31/12 Watermelon ...... 1.0 7/31/12 commodity. (2) A tolerance is established for the Parts per Expiration/ Commodity million revocation combined residues of the insecticide date endosulfan, 6,7,8,9,10,10-hexachloro- Almond ...... 0.3 7/31/12 1,5,5a,6,9,9a-hexahydro-6,9-methano-2, Almond, hulls ...... 1.0 7/31/12 4,3-benzodioxathiepin-3-oxide (alpha Apricot ...... 2.0 7/31/12 and beta isomers), and its metabolite Bean ...... 2.0 7/31/12 Broccoli ...... 3.0 7/31/12 endosulfan sulfate, 6,7,8,9,10,10- Brussels sprouts ...... 2.0 7/31/12 hexachloro-1,5,5a,6,9,9a-hexahydro-6,9- Cabbage ...... 4.0 7/31/12 methano-2, 4,3-benzodioxathiepin-3,3- Cantaloupe ...... 1.0 7/31/12 Carrot, roots ...... 0.2 7/31/12 dioxide in or on the commodity in the Cattle, fat ...... 13.0 7/31/16 following table:

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Expiration/ Commodity Parts per million revocation date

Tea, dried ...... 24 (reflecting less than 0.1 ppm in beverage tea) resulting from application of the insecticide 7/31/16 to growing tea.

(b) Section 18 emergency exemptions. benzodioxathiepin 3-oxide (alpha and [Reserved] beta isomers), and its metabolite (c) Tolerances with regional registra- endosulfan sulfate, 6,7,8,9,10,10- tions. (1) Tolerances with regional reg- hexachloro-1,5,5a,6,9,9a-hexahydro-6,9- istration, as defined in § 180.1(l), are es- methano-2,4,3-benzodioxathiepin-3,3-di- tablished for residues of the insecticide oxide, calculated as the stoichiometric endosulfan, including its metabolites equivalent of endosulfan, in or on the and degradates, in or on the commod- commodity. ities in the table in this paragraph, Expiration/ when endosulfan is used in the state of Commodity Parts per revocation Florida. Compliance with the tolerance million date levels specified in this paragraph is to Apple ...... 1.0 7/31/15 be determined by measuring only the Apple, wet pomace ...... 5.0 7/31/15 sum of endosulfan, 6,7,8,9,10,10- Blueberry ...... 0.3 7/31/15 hexachloro-1,5,5a,6,9,9a-hexahydro-6,9- Corn, sweet, forage ...... 12.0 7/31/15 methano-2,4,3-benzodioxathiepin 3- Corn, sweet, kernel plus cob with oxide (alpha and beta isomers), and its husks removed ...... 0.2 7/31/15 Corn, sweet, stover ...... 14.0 7/31/15 metabolite endosulfan sulfate, Pepper ...... 2.0 7/31/15 6,7,8,9,10,10-hexachloro-1,5,5a,6,9,9a- Potato ...... 0.2 7/31/15 hexahydro-6,9-methano-2,4,3- Pumpkin ...... 1.0 7/31/15 benzodioxathiepin-3,3-dioxide, cal- Squash, winter ...... 1.0 7/31/15 culated as the stoichiometric equiva- Tomato ...... 1.0 7/31/15 lent of endosulfan, in or on the commodity. (d) Indirect or inadvertent residues. [Reserved] Expiration/ Commodity Parts per revocation [65 FR 33696, May 24, 2000, as amended at 71 million date FR 54433, Sept. 15, 2006; 76 FR 56653, Sept. 14, 2011; 78 FR 8409, Feb. 6, 2013] Apple ...... 1.0 12/31/14 Apple, wet pomace ...... 5.0 12/31/14 Blueberry ...... 0.3 12/31/14 § 180.183 Disulfoton; tolerances for res- Corn, sweet, forage ...... 12.0 12/31/14 idues. Corn, sweet, kernel plus cob with (a) General. Tolerances are estab- husks removed ...... 0.2 12/31/14 Corn, sweet, stover ...... 14.0 12/31/14 lished for residues of the insecticide Pepper ...... 2.0 12/31/14 disulfoton, O,O-diethyl S-(2- Potato ...... 0.2 12/31/14 (ethylthio)ethyl) phosphorodithioate, Pumpkin ...... 1.0 12/31/14 Squash, winter ...... 1.0 12/31/14 including its metabolites and Tomato ...... 1.0 12/31/14 degradates, in or on the commodities in the following table. Compliance with (2) Tolerances with regional registra- the tolerance levels specified in this tions. Tolerances with regional reg- paragraph is to be determined by meas- istration, as defined in § 180.1(l), are es- uring only the sum of disulfoton, O,O- tablished for residues of the insecticide diethyl S-(2-(ethylthio)ethyl) endosulfan, including its metabolites phosphorodithioate, and its metabo- and degradates, in or on the commod- lites demeton-S, O,O-diethyl S-(2- ities in the table in this paragraph, (ethylthio)ethyl) phosphorothioate; when endosulfan is used in the United disulfoton sulfoxide, O,O-diethyl S-(2- States (except Florida). Compliance (ethylsulfinyl)ethyl) with the tolerance levels specified in phosphorodithioate; disulfoton oxygen this paragraph is to be determined by analog sulfoxide, O,O-diethyl S-(2- measuring only the sum of endosulfan, (ethylsulfinyl)ethyl) phosphorothioate, 6,7,8,9,10,10-hexachloro-1,5,5a,6,9,9a- disulfoton sulfone, O,O-diethyl S-(2- hexahydro-6,9-methano-2,4,3- (ethylsulfonyl)ethyl)

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phosphorodithioate; and disulfoton ox- (d) Indirect or inadvertent residues. ygen analog sulfone, O,O-diethyl S-(2- [Reserved] (ethylsulfonyl)ethyl) [63 FR 2165, Jan. 14, 1998, as amended at 63 phosphorothioate; calculated as the FR 57073, Oct. 26, 1998; 66 FR 38955, July 26, stoichiometric equivalent of 2001; 67 FR 41806, June 19, 2002; 67 FR 49615, disulfoton, in or on the commodity. July 31, 2002; 70 FR 44492, Aug. 3, 2005; 73 FR 54960, Sept. 24, 2008; 74 FR 46697, Sept. 11, 2009; 75 FR 60240, Sept. 29, 2010] Parts per Expiration/ Commodity million Revocation Date § 180.184 Linuron; tolerances for resi- Bean, lima ...... 0.75 12/31/13 dues. Bean, snap, succulent ...... 0.75 12/31/13 (a) General. Tolerances are estab- Broccoli ...... 0.75 12/31/13 lished for residues of the herbicide Brussels sprouts ...... 0.75 12/31/13 linuron (3-(3,4-dichlorophenyl)-1- Cabbage ...... 0.75 12/31/13 Cauliflower ...... 0.75 12/31/13 methoxy-1-methylurea), including its Coffee, green bean ...... 0.2 6/30/14 metabolites and degradates, in or on Cotton, undelinted seed ...... 0.75 12/31/13 the commodities in the table below. Lettuce, head ...... 0.75 12/31/14 Compliance with the tolerance levels Lettuce, leaf ...... 2 12/31/14 specified below is to be determined by measuring only those linuron residues (b) Section 18 emergency exemptions. convertible to 3,4-dichloroaniline, cal- [Reserved] culated as the stoichiometric equiva- (c) Tolerances with regional registra- lent of linuron, in or on the com- tions. A tolerance with regional reg- modity: istration is established for residues of Parts per the insecticide disulfoton, O,O-diethyl Commodity million S-(2-(ethylthio)ethyl) phosphorodithioate, including its me- Asparagus ...... 7.0 Carrot, roots ...... 1.0 tabolites and degradates, in or on the Cattle, fat ...... 0.2 commodity in the following table. Cattle, kidney ...... 2 .0 Cattle, liver ...... 2 .0 Compliance with the tolerance levels Cattle, meat ...... 0 .1 specified in this paragraph is to be de- Cattle, meat byproducts except kidney and liver 0 .1 termined by measuring only the sum of Celeriac ...... 1.0 Cilantro, dried leaves ...... 10 disulfoton, O,O-diethyl S-(2- Cilantro, fresh leaves ...... 3 .0 (ethylthio)ethyl) phosphorodithioate, Coriander, seed ...... 0 .01 and its metabolites demeton-S, O,O- Corn, field, forage ...... 1 .0 Corn, field, grain ...... 0 .1 diethyl S-(2-(ethylthio)ethyl) Corn, field, stover ...... 6 .0 phosphorothioate; disulfoton sulfoxide, Corn, sweet, forage ...... 1 .0 O,O-diethyl S-(2-(ethylsulfinyl)ethyl) Corn, sweet, kernel plus cob with husks removed ...... 0 .25 phosphorodithioate; disulfoton oxygen Corn, sweet, stover ...... 6 .0 analog sulfoxide, O,O-diethyl S-(2- Cotton, gin byproducts ...... 5 .0 Cotton, undelinted seed ...... 0 .25 (ethylsulfinyl)ethyl) phosphorothioate, Dill, oil ...... 2 .0 disulfoton sulfone, O,O-diethyl S-(2- Dill, seed ...... 0 .5 (ethylsulfonyl)ethyl) Dillweed, dried leaves ...... 5 .0 Dillweed, fresh leaves ...... 1 .5 phosphorodithioate; and disulfoton ox- Goat, fat ...... 0 .2 ygen analog sulfone, O,O-diethyl S-(2- Goat, kidney ...... 2 .0 (ethylsulfonyl)ethyl) Goat, liver ...... 2.0 Goat, meat ...... 0.1 phosphorothioate; calculated as the Goat, meat byproducts except kidney and liver .. 0 .1 stoichiometric equivalent of Hog, fat ...... 0 .05 disulfoton, in or on the commodity. Hog, meat ...... 0 .05 Hog, meat byproducts ...... 0 .1 Horse, fat ...... 0 .2 Expiration/ Horse, kidney ...... 2 .0 Commodity Parts per Revocation million Date Horse, liver ...... 2 .0 Horse, meat ...... 0 .1 Horse, meat byproducts except kidney and liver 0 .1 Asparagus ...... 0.1 12/31/13 Horseradish ...... 0.05 Milk ...... 0.05 Parsley, dried leaves ...... 9 .0 Parsley, leaves ...... 4.0 Parsnip, roots ...... 0 .05

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Parts per Parts per Commodity million Commodity million

Parsnip, tops ...... 0 .05 Wheat, straw ...... 2 .0 Pea, dry, seed ...... 0 .09 Rhubarb ...... 0 .5 (d) Indirect or inadvertent residues. Sheep, fat ...... 0 .2 Sheep, kidney ...... 2.0 [Reserved] Sheep, liver ...... 2.0 [64 FR 41822, Aug. 2, 1999, as amended at 72 Sheep, meat ...... 0.1 FR 37653, July 11, 2007; 73 FR 51727, Sept. 5, Sheep, meat byproducts except kidney and liver 0 .1 Sorghum, grain, forage ...... 1.0 2008; 76 FR 81396, Dec. 28, 2011; 79 FR 8307, Sorghum, grain, grain ...... 0 .25 Feb. 12, 2014] Sorghum, grain, stover ...... 1 .0 Soybean, seed ...... 1 .0 § 180.185 DCPA; tolerances for resi- Soybean, vegetable ...... 1 .0 dues. (a) General. Tolerances for the com- (b) Section 18 emergency exemptions. bined residues of the herbicide di- Time-limited tolerances are estab- methyl tetrachloroterephthalate lished for residues of the herbicide (DCPA) and its metabolites linuron [3-(3,4-dichlorophenyl)-1- monomethyltetrachloroterephthalate methoxy-1-methylurea], including its (MTP) and tetrachloroterephthalic metabolites and degradates, in or on acid (TCP) (calculated as dimethyl the commodities in the table below, re- tetrachloroterephthalate) are estab- sulting from use of the pesticide pursu- lished in or on the following food com- ant to FIFRA section 18 emergency ex- modities: emptions. Compliance with the tolerance levels specified below is to be de- Commodity Parts per termined by measuring only those million linuron residues convertible to 3.4- Cantaloupe ...... 1 .0 dichloroaniline, calculated as the stoi- Garlic ...... 1 .0 chiometric equivalent of linuron, in or Ginseng ...... 2 .0 Horseradish ...... 2.0 on the commodity. The tolerance ex- Muskmelon ...... 1 .0 pires and is revoked on the date speci- Onion, bulb ...... 1 .0 fied in the table. Onion, green ...... 1 .0 Strawberry ...... 2 .0 Expiration/ Tomato ...... 1.0 Commodity Parts per revocation Vegetable, brassica, leafy, group 5 ...... 5.0 million date Watermelon ...... 1.0

Lentil ...... 0.1 12/31/14 (b) Section 18 emergency exemptions. [Reserved] (c) Tolerances with regional registra- (c) Tolerances with regional registrations. Tolerances with regional reg- tions. Tolerances with regional registrations, as defined in § 180.1(l), are istration, as defined in § 180.1(l), are es- established for residues of the herbi- tablished for the combined inadvertent cide linuron (3-(3,4-dichlorophenyl)-1- residues of the herbicide dimethyl methoxy-1-methylurea), including its tetrachloroterephthalate (DCPA) and metabolites and degradates, in or on its metabolites monomethyl the commodities in the table below. tetrachloroterephthalate acid (MTP) Compliance with the tolerance levels and terachlorophthalic acid (TCP) (cal- specified below is to be determined by culated as DCPA) in or on the fol- measuring only those linuron residues lowing food commodities: convertible to 3,4-dichloroaniline, calculated as the stoichiometric equiva- Commodity Parts per lent of linuron, in or on the com- million modity. Radish, roots ...... 2 .0 Radish, tops ...... 15 .0 Commodity Parts per million (d) Indirect or inadvertent residues. Celery ...... 0 .5 Tolerances are established for the com- Potato ...... 0 .2 bined indirect or inadvertent residues Wheat, forage ...... 0 .5 Wheat, grain ...... 0 .05 of the herbicide dimethyl Wheat, hay ...... 0 .5 tetrachloroterephthalate (DCPA) and

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its metabolites monomethyl Commodity Parts per tetrachloroterephthalate acid (MTP) million and terachlorophthalic acid (TCP) (cal- Cattle, meat ...... 1 .0 culated as DCPA) in or on the fol- Cattle, meat byproducts ...... 1.0 lowing food commodities: Goat, fat ...... 1 .0 Goat, meat ...... 1.0 Goat, meat byproducts ...... 1 .0 Commodity Parts per million Hog, fat ...... 1 .0 Hog, meat ...... 1 .0 Basil, dried leaves ...... 20.0 Hog, meat byproducts ...... 1 .0 Basil, fresh leaves ...... 5 .0 Honey ...... 0.15 Bean, dry ...... 2.0 Honeycomb ...... 45 .0 Bean, mung, seed ...... 2 .0 Horse, fat ...... 1 .0 Bean, snap, succulent ...... 2 .0 Celeriac ...... 2.0 Horse, meat ...... 1 .0 Chicory, roots ...... 2 .0 Horse, meat byproducts ...... 1 .0 Chicory, tops ...... 5 .0 Milk, fat ( = n in whole milk) ...... 0 .5 Chive ...... 5 .0 Sheep, fat ...... 1 .0 Coriander, leaves ...... 5 .0 Sheep, meat ...... 1.0 Corn, field, forage ...... 0 .4 Sheep, meat byproducts ...... 1 .0 Corn, field, grain ...... 0 .05 Corn, field, stover ...... 0 .4 (b) Section 18 emergency exemptions. Corn, pop, forage ...... 0 .4 Corn, pop, grain ...... 0.05 [Reserved] Corn, pop, stover ...... 0.4 (c) Tolerances with regional registra- Corn, sweet, forage ...... 0 .4 tions. [Reserved] Corn, sweet, kernel plus cob with husks removed ...... 0 .05 (d) Indirect or inadvertent residues. Corn, sweet, stover ...... 0 .4 [Reserved] Cotton, undelinted seed ...... 0 .2 Cucumber ...... 1 .0 [64 FR 39077, July 21, 1999, as amended at 65 Dill ...... 5 .0 FR 49936, Aug. 16, 2000; 67 FR 46883, July 17, Eggplant ...... 1.0 2002; 69 FR 29458, May 24, 2004; 72 FR 28876, Lettuce ...... 2.0 May 23, 2007] Marjoram ...... 5 .0 Parsley, dried leaves ...... 20.0 Parsley, leaves ...... 5.0 § 180.190 Diphenylamine; tolerances Pea, blackeyed, seed ...... 2 .0 for residues. Pepper ...... 2 .0 Pimento ...... 2 .0 (a) General. Tolerances for residues of Potato ...... 2 .0 the plant regulator diphenylamine are Radicchio ...... 5.0 established in or on the following com- Radish, oriental, roots ...... 2 .0 Radish, oriental, tops ...... 2 .0 modities: Rutabaga ...... 2 .0 Soybean ...... 2.0 Commodity Parts per Squash, summer ...... 1 .0 million Squash, winter ...... 1 .0 Sweet potato ...... 2.0 Apple, wet pomace ...... 30.0 Turnip, roots ...... 2 .0 Apple from preharvest or postharvest use, in- Turnip, tops ...... 5.0 cluding use of impregnated wraps ...... 10.0 Yam, true, tuber ...... 2.0 Cattle, fat ...... 0.01 Cattle, liver ...... 0 .1 Cattle, meat byproducts, except liver ...... 0 .01 [72 FR 52018, Sept. 12, 2007, as amended at 73 Cattle, meat ...... 0 .01 FR 53737, Sept. 17, 2008; 73 FR 80302, Dec. 31, Goat, fat ...... 0 .01 2008; 74 FR 14744, Apr. 1, 2009] Goat, liver ...... 0.1 Goat, meat byproducts, except liver ...... 0 .01 § 180.189 Coumaphos; tolerances for Goat, meat ...... 0.01 residues. Horse, fat ...... 0 .01 Horse, liver ...... 0 .1 (a) General. Tolerances for residues of Horse, meat byproducts, except liver ...... 0 .01 the insecticide coumaphos (O,O-diethyl Horse, meat ...... 0 .01 O-3-chloro-4-methyl-2-oxo-2H-1- Milk ...... 0.01 Pear (post harvest) ...... 5 .0 benzopyran-7-yl phosphorothioate and Sheep, fat ...... 0 .01 its oxygen analog (O,O-diethyl O-3- Sheep, liver ...... 0.1 chloro-4-methyl-2-oxo-2H-1- Sheep, meat byproducts, except liver ...... 0 .01 benzopyran-7-yl phosphate) in or on Sheep, meat ...... 0.01 food commodities as follows: (b) Section 18 emergency exemptions. Commodity Parts per [Reserved] million (c) Tolerances with regional registra- Cattle, fat ...... 1.0 tions. [Reserved]

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(d) Indirect or inadvertent residues. Commodity Parts per [Reserved] million [64 FR 25848, May 13, 1999, as amended at 66 Cattle, meat byproducts 1 ...... 0.1 FR 63198, Dec. 5, 2001; 72 FR 16283, Apr. 4, 1 There are no U.S. registrations for cattle commodities as 2007; 76 FR 34885, June 15, 2011] of June 24, 1999. (b) Section 18 emergency exemptions. § 180.191 Folpet; tolerances for resi- [Reserved] dues. (c) Tolerances with regional registra- (a) General. Tolerances are estab- tions. [Reserved] lished for the fungicide folpet (N- (d) Indirect or inadvertent residues. (trichloromethylthio)phthalimide) in [Reserved] or on raw agricultural commodities as follows: [72 FR 54578, Sept. 26, 2007]

Parts per § 180.200 Dicloran; tolerances for resi- Commodity million dues.

Apple 1 ...... 5.0 (a) General. Tolerances are estab- Cranberry 1 ...... 15 .0 lished for residues of the fungicide Cucumber 1 ...... 2 .0 dicloran, including its metabolites and Grape 1 ...... 50 .0 degradates, in or on the commodities Grape, raisin 1 ...... 80.0 Hop, dried cones ...... 120 .0 in the table in this paragraph. Compli- Lettuce 1 ...... 50.0 ance with the tolerance levels specified Melon 1 ...... 3 .0 in this paragraph is to be determined Onion,bulb 1 ...... 2 .0 by measuring only dicloran, 2,6- Strawberry 1 ...... 5 .0 dichloro-4-nitroaniline, in or on the Tomato 1 ...... 25.0 commodity. 1 No U.S. registrations. Expiration/ (b) Section 18 emergency exemptions. Parts per Commodity million revocation [Reserved] date (c) Tolerances with regional registra- Apricot ...... 20 None tions. Tolerances with regional reg- Bean, snap, succulent ...... 20 None istrations as defined in § 180.1(l) are es- Carrot, roots ...... 10 11/2/11 Celery ...... 15 None tablished for the fungicide folpet (N- Cherry, sweet ...... 20 None (trichloromethylthio)phthalimide) in Cucumber ...... 5 None or on the following raw agricultural Endive ...... 10 None commodity: Garlic ...... 5 None Grape ...... 10 None Lettuce ...... 10 None Parts per Nectarine ...... 20 None Commodity million Onion ...... 10 None Avocado ...... 25.0 Peach ...... 20 None Plum, prune, fresh ...... 15 None Potato ...... 0.25 12/31/14 (d) Indirect or inadvertent residues. Rhubarb ...... 10 None [Reserved] Sweet potato, roots ...... 10 None Tomato ...... 5 None [61 FR 37222, July 17, 1996, as amended at 68 FR 10388, Mar. 5, 2003; 69 FR 52192, Aug. 25, (b) Section 18 emergency exemptions. 2004; 72 FR 41928, Aug. 1, 2007] [Reserved] (c) Tolerances with regional registra- § 180.198 Trichlorfon; tolerances for tions. [Reserved] residues. (d) Indirect or inadvertent residues. (a) General. Tolerances are estab- [Reserved] lished for residues of the insecticide trichlorfon (dimethyl (2,2,2-trichloro-1- [77 FR 40815, July 11, 2012] hydroxyethyl) phosphonate) in or on § 180.202 p-Chlorophenoxyacetic acid; the following food commodities: tolerances for residues.

Commodity Parts per (a) General. A tolerance is established million for the combined residues of the plant Cattle, fat 1 ...... 0.5 regulator p-chlorophenoxyacetic acid Cattle, meat 1 ...... 0 .2 and its metabolite p-chlorophenol to

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inhibit embryonic root development in Commodity Parts per or on the following food commodity: million Sheep, meat byproducts ...... 0 .02 Parts per Commodity million Sorghum, grain, forage ...... 0.1 Sorghum, grain, grain ...... 0 .1 Bean, mung, sprouts ...... 0.2 Sorghum, grain, stover ...... 0 .1 Soybean, forage ...... 2 .0 Soybean, hay ...... 2 .0 (b) Section 18 emergency exemptions. Soybean, seed ...... 0 .05 [Reserved] Swiss chard ...... 2.0 (c) Tolerances with regional registra- Tangerine ...... 2 .0 Tomato ...... 2.0 tions. [Reserved] Turnip, roots ...... 0 .2 (d) Indirect or inadvertent residues. Turnip, tops ...... 2.0 [Reserved] Wheat, forage ...... 2 .0 Wheat, grain ...... 0 .04 [68 FR 39439, July 1, 2003, as amended at 71 Wheat, hay ...... 2 .0 FR 56398, Sept. 27, 2006] Wheat, straw ...... 2 .0 1 There are U.S. registrations as of August 16, 1996. § 180.204 Dimethoate; tolerances for residues. (b) Section 18 emergency exemptions. [Reserved] (a) General. Tolerances are estab- (c) Tolerances with regional registra- lished for total residues of the insecti- tions. Tolerances with regional reg- cide dimethoate (O,O-dimethyl S-(N- istration, as defined in § 180.1(l), are es- methylcarbamoylmethyl) tablished for total residues of phosphorodithioate) including its oxy- dimethoate including its oxygen analog gen analog (O,O-dimethyl S-(N- in or on the following food commod- methylcarbamoylmethyl) ities: phosphorothioate) in or on the following food commodities: Parts per Commodity million Parts per Commodity million Asparagus ...... 0.15 Brussels sprouts ...... 5 .0 Alfalfa, forage ...... 2.0 Cherry, sweet ...... 2 .0 Alfalfa, hay ...... 2.0 Cherry, tart ...... 2 .0 Bean, dry, seed ...... 2 .0 Bean, lima ...... 2 .0 (d) Indirect or inadvertent residues. Bean, snap, succulent ...... 2 .0 Blueberry 1 ...... 1 .0 [Reserved] Broccoli ...... 2 .0 [65 FR 33697, May 24, 2000, as amended at 69 Cattle, meat byproducts ...... 0.02 Cauliflower ...... 2 .0 FR 6567, Feb. 11, 2004; 73 FR 53737, Sept. 17, Celery ...... 2 .0 2008] Citrus, dried pulp ...... 5 .0 Corn, field, forage ...... 1 .0 § 180.205 Paraquat; tolerances for resi- Corn, field, grain ...... 0 .1 dues. Corn, field, stover ...... 1 .0 Corn, pop, grain ...... 0.1 (a) General. Tolerances are estab- Corn, pop, stover ...... 1.0 lished for residues of the desiccant, de- Corn, sweet, forage ...... 1 .0 ′ Cotton, undelinted seed ...... 0 .1 foliant, and herbicide paraquat (1,1 -di- Egg ...... 0 .02 methyl-4,4′-bipyridinium-ion) derived Endive ...... 2.0 from application of either the Goat, meat byproducts ...... 0 .02 bis(methyl sulfate) or the dichloride Grapefruit ...... 2 .0 Hog, meat byproducts ...... 0 .02 salt (both calculated as the cation) in Horse, meat byproducts ...... 0 .02 or on the following food commodities: Kale ...... 2 .0 Lemon ...... 2.0 Parts per Lettuce, leaf ...... 2 .0 Commodity million Melon ...... 1 .0 Milk ...... 0.002 Acerola ...... 0.05 Mustard greens ...... 2.0 Almond, hulls ...... 0 .5 Orange ...... 2 .0 Animal feed, nongrass, group 18, forage ...... 75 .0 Pea ...... 2 .0 Animal feed, nongrass, group 18, hay ...... 210.0 Pear ...... 2 .0 Artichoke, globe ...... 0.05 Pecan ...... 0 .1 Asparagus ...... 0.5 Pepper ...... 2 .0 Atemoya ...... 0 .05 Potato ...... 0 .2 Avocado ...... 0 .05 Poultry, meat byproducts ...... 0.02 Banana ...... 0.05 Safflower, seed ...... 0 .1 Barley, grain ...... 0 .05

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Parts per Parts per Commodity million Commodity million

Barley, hay ...... 3 .5 Pea and bean, succulent shelled, subgroup 6B 0 .05 Barley, straw ...... 1 .0 Pea, field, hay ...... 0.8 Beet, sugar, roots ...... 0 .5 Pea, field, vines ...... 0 .2 Beet, sugar, tops ...... 0.05 Peanut ...... 0 .05 Berry group 13 ...... 0 .05 Peanut, hay ...... 0.5 Biriba ...... 0 .05 Peppermint, tops ...... 0 .5 Cacao bean, bean ...... 0 .05 Persimmon ...... 0 .05 Canistel ...... 0 .05 Pineapple ...... 0.05 Carrot, roots ...... 0.05 Pineapple, process residue ...... 0 .25 Cattle, fat ...... 0.05 Pistachio ...... 0.05 Cattle, kidney ...... 0 .5 Pomegranate ...... 0 .05 Cattle, meat ...... 0 .05 Pulasan ...... 0 .05 Cattle, meat byproducts, except kidney ...... 0.05 Rambutan ...... 0 .05 Cherimoya ...... 0 .05 Rhubarb ...... 0 .05 Coffee, bean, green ...... 0 .05 Rice, grain ...... 0 .05 Corn, field, forage ...... 3 .0 Safflower, seed ...... 0 .05 Corn, field, grain ...... 0 .1 Sapodilla ...... 0 .05 Corn, field, stover ...... 10 .0 Sapote, black ...... 0 .05 Corn, pop, grain ...... 0.1 Sapote, mamey ...... 0 .05 Corn, pop, stover ...... 10.0 Sapote, white ...... 0 .05 Corn, sweet, kernel plus cob with husks re- Sheep, fat ...... 0 .05 moved ...... 0 .05 Sheep, kidney ...... 0.5 Cotton, gin byproducts ...... 110.0 Sheep, meat ...... 0.05 Cotton, undelinted seed ...... 3 .5 Sheep, meat byproducts, except kidney ...... 0 .05 Sorghum, forage, forage ...... 0 .1 Cowpea, forage ...... 0 .1 Sorghum, grain, forage ...... 0.1 Cowpea, hay ...... 0 .4 Sorghum, grain, grain ...... 0 .05 Cranberry ...... 0 .05 Soursop ...... 0 .05 Custard apple ...... 0 .05 Soybean, forage ...... 0 .4 Egg ...... 0 .01 Soybean, hay ...... 10 .0 Endive ...... 0.05 Soybean, hulls ...... 4 .5 Feijoa ...... 0 .05 Soybean, seed ...... 0 .7 Fig ...... 0 .05 Spanish lime ...... 0 .05 Fruit, citrus, group 10 ...... 0 .05 Spearmint, tops ...... 0 .5 Fruit, pome, group 11 ...... 0.05 Star apple ...... 0 .05 Fruit, stone, group 12 ...... 0 .05 Starfruit ...... 0 .05 Goat, fat ...... 0 .05 Strawberry ...... 0 .25 Goat, kidney ...... 0 .5 Sugar apple ...... 0 .05 Goat, meat ...... 0.05 Sugarcane, cane ...... 0.5 Goat, meat byproducts, except kidney ...... 0 .05 Sugarcane, molasses ...... 3 .0 Grain, aspirated fractions ...... 65.0 Sunflower, seed ...... 2.0 Grape ...... 0 .05 Turnip, greens ...... 0.05 Grass, forage ...... 90 .0 Turnip, roots ...... 0 .05 Grass, hay ...... 40 .0 Vegetable, brassica, leafy, group 5 ...... 0.05 Guar, seed ...... 0.5 Vegetable, cucurbit, group 9 ...... 0.05 Guava ...... 0 .05 Vegetable, fruiting, group 8 ...... 0.05 Hog, fat ...... 0 .05 Vegetable, legume, edible podded, subgroup 6A 0 .05 Hog, kidney ...... 0.5 Vegetable, tuberous and corm, subgroup 1C ..... 0.50 Hog, meat ...... 0 .05 Wax jambu ...... 0 .05 Hog, meat byproducts, except kidney ...... 0 .05 Wheat, forage ...... 0 .5 Hop, dried cones ...... 0 .5 Wheat, grain ...... 1 .1 Horse, fat ...... 0 .05 Wheat, hay ...... 3 .5 Horse, kidney ...... 0 .5 Wheat, straw ...... 50 .0 Horse, meat ...... 0 .05 Horse, meat byproducts, except kidney ...... 0 .05 (b) Section 18 emergency exemptions. Ilama ...... 0 .05 [Reserved] Jaboticaba ...... 0 .05 Kiwifruit ...... 0.05 (c) Tolerances with regional registra- Lentil, seed ...... 0 .3 tions. Tolerances with regional reg- Lettuce ...... 0.05 istration as defined in § 180.1(l), are es- Longan ...... 0 .05 tablished for residues of the pesticide Lychee ...... 0 .05 Mango ...... 0.05 paraquat (1,1′-dimethyl-4,4′ Milk ...... 0.01 bipyridinium ion) derived from applica- Nut, tree, group 14 ...... 0 .05 tion of either the bis(methyl sulfate) or Okra ...... 0.05 Olive ...... 0 .05 the dichloride salt (both calculated as Onion, bulb ...... 0 .1 the cation) in or on the following food Onion, green ...... 0 .05 commodities: Papaya ...... 0 .05 Passionfruit ...... 0 .2 Parts per Pawpaw ...... 0 .05 Commodity million Pea and bean, dried shelled, except soybean, subgroup 6C, except guar bean ...... 0 .3 Pea, pigeon, seed ...... 0 .05

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Commodity Parts per § 180.207 Trifluralin; tolerances for million residues. Taro, corm ...... 0 .1 (a) General. Tolerances are estab- Tyfon ...... 0 .05 lished for residues of trifluralin, in- (d) Indirect or inadvertent residues. cluding its metabolites and degradates, [Reserved] in or on the commodities in the following table. Compliance with the tol- [46 FR 51614, Oct. 21, 1981] erance levels specified in the following EDITORIAL NOTE: For FEDERAL REGISTER ci- table is to be determined by only tations affecting § 180.205, see the List of CFR trifluralin a,a,a-trifluoro-2,6-dinitro- Sections Affected, which appears in the Finding Aids section of the printed volume N,N-dipropyl-p-toluidine, in or on the and at www.fdsys.gov. commodity.

Parts per § 180.206 Phorate; tolerances for resi- Commodity million dues. (a) General. Tolerances are estab- Alfalfa, forage ...... 3.0 lished for the combined residues of the Alfalfa, hay ...... 2.0 Almond, hulls ...... 0 .05 insecticide phorate (O,O-diethyl S Asparagus ...... 0.05 (ethylthio) meth- Barley, grain ...... 0 .05 yl]phosphorodithioate), phorate sulf- Barley, hay ...... 0 .05 oxide, phorate sulfone, phorate oxygen Barley, straw ...... 0 .05 analog, phorate oxygen analog sulf- Bean, mung, sprouts ...... 2.0 oxide, and phorate oxygen analog Carrot, roots ...... 1.0 sulfone in or on the following food Celery ...... 0 .05 Corn, field, forage ...... 0 .05 commodities: Corn, field, grain ...... 0 .05 Corn, field, stover ...... 0 .05 Parts per Commodity million Cotton, gin byproducts ...... 0 .05 Endive ...... 0.05 Bean, dry, seed ...... 0 .05 Fruit, citrus, group 10 ...... 0 .05 Bean, succulent ...... 0 .05 Fruit, stone, group 12 ...... 0 .05 Beet, sugar, roots ...... 0 .3 Grape ...... 0 .05 Beet, sugar, tops ...... 3.0 Hop, dried cones ...... 0 .05 Coffee, green bean 1 ...... 0 .02 Corn, field, forage ...... 0 .5 Nut, tree, group 14 ...... 0 .05 Corn, field, grain ...... 0 .05 Oilseed, crop group 20 ...... 0 .05 Corn, sweet, forage ...... 0 .5 Okra ...... 0.05 Corn, sweet, kernel plus cob with husks re- Peanut ...... 0 .05 moved ...... 0 .05 Peanut, hay ...... 0.05 Cotton, undelinted seed ...... 0 .05 Peppermint, oil ...... 2 .0 Hop, dried cones ...... 2 .0 Peppermint, tops ...... 0 .05 Peanut ...... 0 .1 Potato ...... 0 .2 Sorghum, grain, forage ...... 0.05 Sorghum, grain, grain ...... 0 .05 Sorghum, grain, grain ...... 0 .05 Sorghum, grain, stover ...... 0 .1 Sorghum, grain, stover ...... 0 .05 Soybean, seed ...... 0 .05 Spearmint, oil ...... 2 .0 Sugarcane, cane ...... 0.05 Spearmint, tops ...... 0 .05 Wheat, forage ...... 1 .5 Sugarcane, cane ...... 0.05 Wheat, grain ...... 0 .05 Vegetable, brassica, leafy group 5 ...... 0 .05 Wheat, hay ...... 1 .5 Wheat, straw ...... 0 .05 Vegetable, bulb, group 3 ...... 0 .05 Vegetable, cucurbit, group 9 ...... 0.05 1 There are no U.S. registrations as of September 1, 1993 Vegetable, foliage of legume, group 7 ...... 0 .05 for the use of phorate on the growing crop, coffee. Vegetable, fruiting, group 8 ...... 0.05 (b) Section 18 emergency exemptions. Vegetable, leaves of root and tuber, group 2 ..... 0 .05 [Reserved] Vegetable, legume, group 6 ...... 0 .05 (c) Tolerances with regional registra- Vegetable, root and tuber, group 1, except carrot ...... 0 .05 tions. [Reserved] Wheat, grain ...... 0 .05 (d) Indirect or inadvertent residues. Wheat, straw ...... 0 .05 [Reserved] [58 FR 62038, Nov. 24, 1993, as amended at 63 (b) Section 18 emergency exemptions. FR 2165, Jan. 14, 1998; 63 FR 57074, Oct. 26, [Reserved] 1998; 66 FR 50833, Oct. 5, 2001; 67 FR 49616, (c) Tolerances with regional registra- July 31, 2002; 71 FR 74816, Dec. 13, 2006; 73 FR tions. [Reserved] 53738, Sept. 17, 2008]

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(d) Indirect or inadvertent residues. Commodity Parts per [Reserved] million [45 FR 42619, June 25, 1980, as amended at 45 Strawberry ...... 0 .1 FR 56346, Aug. 25, 1980; 45 FR 86493, Dec. 31, Sugarcane, cane ...... 0.4 Watermelon ...... 1.0 1980; 46 FR 37250, July 20, 1981; 47 FR 13524, Mar. 31, 1982; 47 FR 20309, May 12, 1982; 63 FR (b) Section 18 emergency exemptions. 57074, Oct. 26, 1998; 64 FR 39082, July 21, 1999; 70 FR 21643, Apr. 27, 2005; 71 FR 54433, Sept. [Reserved] 15, 2006; 78 FR 46274, July 31, 2013] (c) Tolerances with regional registrations. [Reserved] § 180.208 Benfluralin; tolerances for (d) Indirect or inadvertent residues. residues. [Reserved] (a) General. Tolerances are estab- [71 FR 30818, May 31, 2006] lished for residues of the herbicide benfluralin, N-butyl-N-ethyl-aaa- § 180.210 Bromacil; tolerances for resi- trifluoro-2,6-dinitro-p-toluidine, in or dues. on the following food commodities: (a) General. Tolerances are established for residues of the herbicide Parts per Commodity million bromacil (5-bromo-3-sec-butyl-6- methyluracil) in or on the following Alfalfa, forage ...... 0.05 Alfalfa, hay ...... 0.05 food commodities: Clover, forage ...... 0.05 Clover, hay ...... 0.05 Commodity Parts per Lettuce ...... 0.05 million Trefoil, forage ...... 0 .05 Fruit, citrus ...... 0 .1 Trefoil, hay ...... 0 .05 Pineapple ...... 0.1

(b) Section 18 emergency exemptions. (b) Section 18 emergency exemptions. [Reserved] [Reserved] (c) Tolerances with regional registra- (c) Tolerances with regional registrations. [Reserved] tions. [Reserved] (d) Indirect or inadvertent residues. (d) Indirect or inadvertent residues. [Reserved] [Reserved] [68 FR 39439, July 1, 2003, as amended at 73 [68 FR 39439, July 1, 2003] FR 52613, Sept. 10, 2008] § 180.211 Propachlor; tolerances for § 180.209 Terbacil; tolerances for resi- residues. dues. (a) General. Tolerances are estab- (a) Tolerances are estab- General. lished for the combined residues of the lished for combined residues of the her- herbicide propachlor (2-chloro-N- bicide terbacil, (3-tert-butyl-5-chloro-6- isopropylacetanilide) and its metabo- methyluracil) and its metabolites [3- lites containing the N-isopropylaniline tert-butyl-5-chloro-6- moiety, calculated as 2-chloro-N- hydroxymethyluracil], [6-chloro-2,3- isopropylacetanilide, in or on the fol- dihydro-7-hydroxymethyl 3,3-dimethyl- lowing raw agricultural commodities: 5H-oxazolo(3,2-a) pyrimidin-5-one], and [6-chloro-2,3-dihydro-3,3,7-trimethyl- Commodity Parts per 5H-oxazolo(3,2-a) pyrimidin-5-one], cal- million culated as terbacil, in or on the fol- Cattle, fat ...... 0.05 lowing raw agricultural commodities: Cattle, kidney ...... 0 .2 Cattle, meat ...... 0 .02 Parts per Cattle, meat byproducts, except kidney ...... 0.05 Commodity million Corn, field, forage ...... 3 .0 Corn, field, grain ...... 0 .2 Alfalfa, forage ...... 1.0 Corn, field, stover ...... 1 .0 Alfalfa, hay ...... 2.0 Corn, sweet, forage ...... 3 .0 Apple ...... 0.3 Goat, fat ...... 0 .05 Asparagus ...... 0.4 Goat, kidney ...... 0 .2 Blueberry ...... 0 .2 Goat, meat ...... 0.02 Caneberry subgroup 13A ...... 0 .2 Goat, meat byproducts, except kidney ...... 0 .05 Peach ...... 0 .2 Hog, fat ...... 0 .02 Peppermint, tops ...... 2 .0 Hog, meat ...... 0 .02 Spearmint, tops ...... 2 .0 Hog, meat byproducts ...... 0 .02

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Parts per Parts per Commodity million Commodity million

Horse, fat ...... 0 .05 Almond ...... 0.25 Horse, kidney ...... 0 .2 Almond, hulls ...... 0 .25 Horse, meat ...... 0 .02 Apple ...... 0.20 Horse, meat byproducts, except kidney ...... 0 .05 Avocado ...... 0 .20 Milk ...... 0.02 Blackberry ...... 0 .20 Blueberry ...... 0 .20 Sheep, fat ...... 0 .05 Cattle, meat ...... 0 .03 Sheep, kidney ...... 0.2 Cattle, meat byproducts ...... 0.03 Sheep, meat ...... 0.02 Cherry ...... 0.25 Sheep, meat byproducts, except kidney ...... 0 .05 Corn, field, forage ...... 0 .20 Sorghum, forage, forage ...... 8 .0 Corn, field, grain ...... 0 .20 Sorghum, grain, forage ...... 8.0 Corn, field, stover ...... 0 .25 Sorghum, grain, grain ...... 0 .25 Corn, pop, grain ...... 0.20 Sorghum, grain, stover ...... 12 .0 Corn, pop, stover ...... 0.25 Corn, sweet, forage ...... 0 .20 Corn, sweet, kernel plus cob with husks re- (b) Section 18 emergency exemptions. moved ...... 0 .25 [Reserved] Corn, sweet, stover ...... 0 .25 (c) Tolerances with regional registra- Cranberry ...... 0 .25 Currant ...... 0 .25 tions. [Reserved] Egg ...... 0 .03 (d) Indirect or inadvertent residues. Goat, meat ...... 0.03 [Reserved] Goat, meat byproducts ...... 0 .03 Grape ...... 0 .20 [47 FR 25959, June 16, 1982, as amended at 47 Grapefruit ...... 0 .25 FR 28381, June 30, 1982; 47 FR 28626, July 1, Hazelnut ...... 0 .20 Horse, meat ...... 0 .03 1982; 47 FR 46701, Oct. 20, 1982; 63 FR 57074, Horse, meat byproducts ...... 0 .03 Oct. 26, 1998; 72 FR 53454, Sept. 19, 2007] Lemon ...... 0.25 Loganberry ...... 0 .20 § 180.212 S-Ethyl cyclohexylethylthio- Milk ...... 0.03 carbamate; tolerances for residues. Nut, macadamia ...... 0.25 Olive ...... 0 .20 (a) General. Tolerances are estab- Orange ...... 0 .25 Peach ...... 0 .20 lished for residues of the herbicide S- Pear ...... 0 .25 ethyl cyclohexylethylthiocarbamate in Pecan ...... 0 .20 or on the following food commodities: Plum ...... 0 .20 Raspberry ...... 0 .20 Parts per Sheep, meat ...... 0.03 Commodity million Sheep, meat byproducts ...... 0 .03 Strawberry ...... 0 .25 Beet, garden, roots ...... 0 .05(N) Walnut ...... 0 .2 Beet, garden, tops ...... 0 .05(N) Beet, sugar, roots ...... 0 .05(N) (b) Section 18 emergency exemptions. Beet, sugar, tops ...... 0.05(N) [Reserved] Spinach ...... 0 .05(N) (c) Tolerances with regional registrations. [Reserved] (b) Section 18 emergency exemptions. (d) Indirect or inadvertent residues. [Reserved] [Reserved] (c) Tolerances with regional registrations. [Reserved] [63 FR 2165, Jan. 14, 1998, as amended at 63 (d) Indirect or inadvertent residues. FR 57074, Oct. 26, 1998; 72 FR 35665, June 29, [Reserved] 2007; 72 FR 53454, Sept. 19, 2007] [68 FR 39439, July 1, 2003] § 180.215 Naled; tolerances for residues. § 180.213 Simazine; tolerances for resi- (a) General. (1) Tolerances are estab- dues. lished for residues of the insecticide (a) General. Tolerances are estab- naled (1,2-dibromo-2,2-dichloro-ethyl lished for the combined residues of the dimethyl phosphate) and its conversion herbicide simazine (2-chloro-4,6- product 2,2-dichlorovinyl dimethyl bis(ethylamino)-s-triazine) and its two phosphate, expressed as naled, result- chlorinated degradates (2-amino-4- ing from the application of the pes- chloro-6-ethylamino-s-triazine and 2,4- ticide to growing crops or from direct diamino-6-chloro-s-triazine), the total application to livestock and poultry, in residue to be measured in or on the fol- or on the following raw agricultural lowing food commodities: commodities:

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and disulfides), including its metabo- Commodity Parts per million lites and degradates, in or on the com- Almond, hulls ...... 0 .5 modities in the following table. Com- Almond ...... 0.5 pliance with the tolerance levels speci- Bean, dry, seed ...... 0 .5 fied in this paragraph is to be deter- Bean, succulent ...... 0 .5 Beet, sugar, roots ...... 0 .5 mined by measuring only those Beet, sugar, tops ...... 0.5 metiram residues convertible to and Broccoli ...... 1 expressed in terms of the degradate Brussels sprouts ...... 1 carbon disulfide. Cabbage ...... 1 Cauliflower ...... 1 Parts per Celery ...... 3 Commodity million Collards ...... 3 Cotton, undelinted seed ...... 0 .5 Apple ...... 0.5 Cucumber ...... 0 .5 Apple, pomace, wet ...... 2 Eggplant ...... 0.5 Banana 1 ...... 3 Grape ...... 0 .5 Grape, wine 1 ...... 5 Grapefruit ...... 3 Potato ...... 0 .2 Grass, forage ...... 10 1 Hop, dried cones ...... 0 .5 There are no U.S. registrations on bananas and grape, wine as of April 29, 2011. Kale ...... 3 Legume, forage ...... 10 (b) Section 18 emergency exemptions. Lemon ...... 3 Melon ...... 0 .5 [Reserved] Orange, sweet ...... 3 (c) Tolerances with regional registra- Peach ...... 0 .5 tions. [Reserved] Pea, succulent ...... 0 .5 (d) Indirect or inadvertent residues. Pepper ...... 0 .5 Pumpkin ...... 0.5 [Reserved] Safflower, seed ...... 0 .5 [63 FR 57074, Oct. 26, 1998, as amended at 76 Spinach ...... 3 Squash, summer ...... 0 .5 FR 23891, Apr. 29, 2011] Squash, winter ...... 0 .5 Strawberry ...... 1 § 180.220 Atrazine; tolerances for resi- Swiss chard ...... 3 dues. Tangerine ...... 3 Tomato ...... 0.5 (a) General. Tolerances are estab- Turnip, greens ...... 3 lished for the combined residues of the Walnut ...... 0 .5 herbicide atrazine (2-chloro-4- ethylamino-6-isopropylamino-s-tri- (2) A tolerance of 0.5 part per million azine) and its chlorinated metabolites is established for the pesticide naled in 2-amino-4-chloro-6-isopropylamino-s- or on all raw agricultural commodities, triazine, 2-amino-4-chloro-6- except those otherwise listed in this ethylamino-s-triazine, and 2,4-diamino- section, from use of the pesticide for 6-chloro-s-triazine, in or on the fol- area pest (mosquito and fly) control. lowing food commodities: (b) Section 18 emergency exemptions. [Reserved] Commodity Parts per (c) Tolerances with regional registra- million tions. [Reserved] Cattle, fat ...... 0.02 (d) Indirect or inadvertent residues. Cattle, meat ...... 0 .02 Cattle, meat byproducts ...... 0.02 [Reserved] Corn, field, forage ...... 1 .5 [42 FR 46304, Sept. 15, 1977, as amended at 54 Corn, field, grain ...... 0 .20 Corn, field, stover ...... 0 .5 FR 20125, May 10, 1989; 63 FR 57074, Oct. 26, Corn, pop, forage ...... 1 .5 1998; 66 FR 50833, Oct. 5, 2001; 77 FR 59124, Corn, pop, grain ...... 0.20 Sept. 26, 2012] Corn, pop, stover ...... 0.5 Corn, sweet, forage ...... 15 § 180.217 Metiram; tolerances for resi- Corn, sweet, kernel plus cob with husks re- dues. moved ...... 0 .20 Corn, sweet, stover ...... 2 .0 (a) General. Tolerances are estab- Goat, fat ...... 0 .02 lished for residues of a metiram (a mix- Goat, meat ...... 0.02 Goat, meat byproducts ...... 0 .02 ture of 5.2 parts by weight of ammoni- Grass, forage ...... 4 .0 ates of [ethylenebis (dithiocarbamato)] Grass, hay ...... 4 .0 zinc with 1 part by weight ethylenebis Guava ...... 0 .05 Horse, fat ...... 0 .02 [dithiocarbamic acid] bimolecular and Horse, meat ...... 0 .02 trimolecular cyclic anhydrosulfides Horse, meat byproducts ...... 0 .02

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Parts per Parts per Commodity million Commodity million

Milk ...... 0.02 Coriander, dried leaves ...... 9.0 Nut, macadamia ...... 0.20 Cotton, gin byproducts ...... 1 .0 Sheep, fat ...... 0 .02 Cotton, undelinted seed ...... 0 .25 Sheep, meat ...... 0.02 Dill, oil ...... 1 .3 Sheep, meat byproducts ...... 0 .02 Dillweed, dried leaves ...... 1 .1 Sorghum, forage, forage ...... 0 .25 Dillweed, fresh leaves ...... 0 .30 Sorghum, grain, forage ...... 0.25 Leaf petioles subgroup 4B ...... 0 .50 Sorghum, grain, grain ...... 0 .20 Okra ...... 0.05 Sorghum, grain, stover ...... 0 .50 Parsley, dried leaves ...... 1 .5 Sugarcane, cane ...... 0.20 Parsley, leaves ...... 0.60 Wheat, forage ...... 1 .5 Pea, pigeon, seed ...... 0 .25 Wheat, grain ...... 0 .10 Wheat, hay ...... 5 .0 Wheat, straw ...... 0 .50 (b) Section 18 emergency exemptions. [Reserved] (b) Section 18 emergency exemptions. (c) Tolerances with regional exemptions. [Reserved] [Reserved] (c) Tolerances with regional registra- (d) Indirect or inadvertent residues. tions. [Reserved] Tolerances are established for indirect (d) Indirect or inadvertent residues. or inadvertent residues of the herbicide Tolerances are established for indirect prometryn, including its metabolites or inadvertant residues of atrazine, 2- and degradates, in or on the commod- chloro-4-ethylamino-6-isopropylamino- ities in the following table. Compliance s-triazine, in or on the following raw with the tolerance levels specified in agricultural commodity when present the following table is to be determined therein as a result of application of by measuring only prometryn, 2,4- atrazine to the growing crops in para- bis(isopropylamino)-6-methylthio-s-tri- graph (a) of this section: azine, in or on the following raw agricultural commodities. Commodity Parts per million Parts per Commodity million Vegetable, leafy, except brassica, group 4 ...... 0 .25 Barley, forage ...... 0 .3 Barley, hay ...... 1 .0 [43 FR 29121, July 6, 1978, as amended at 44 Barley, straw ...... 0 .3 FR 67116, Nov. 23, 1979; 47 FR 3771, Jan. 27, Oat, forage ...... 0 .3 1982; 47 FR 8012, Feb. 24, 1982; 63 FR 57075, Oat, hay ...... 1.0 Oct. 26, 1998; 67 FR 46893, July 17, 2002; 69 FR Oat, straw ...... 0.3 6567, Feb. 11, 2004; 72 FR 35666, June 29, 2007; Rye, forage ...... 0 .3 72 FR 53454, Sept. 19, 2007; 73 FR 37852, July Rye, hay ...... 1 .0 Rye, straw ...... 0 .3 2, 2008; 76 FR 56654, Sept. 14, 2011] Triticale, forage ...... 0 .3 Triticale, hay ...... 1 .0 § 180.222 Prometryn; tolerances for Triticale, straw ...... 0 .3 residues. Wheat, forage ...... 0 .3 Wheat, hay ...... 1 .0 (a) General. Tolerances are estab- Wheat, straw ...... 0 .3 lished for residues of the herbicide prometryn, including its metabolites [43 FR 29121, July 6, 1978, as amended at 45 and degradates, in or on the commod- FR 51782, Aug. 5, 1980; 54 FR 6918, Feb. 15, ities in the following table. Compliance 1989; 60 FR 20434, Apr. 26, 1995; 63 FR 17692, with the tolerance levels specified in Apr. 10, 1998; 63 FR 57075, Oct. 26, 1998; 64 FR the following table is to be determined 39082, July 21, 1999; 74 FR 47456, Sept. 16, 2009; by measuring only prometryn, 2,4- 74 FR 67108, Dec. 18, 2009; 76 FR 34885, June bis(isopropylamino)-6-methylthio-s-tri- 15, 2011; 78 FR 55640, Sept. 11, 2013] azine, in or on the following raw agricultural commodities: § 180.225 Phosphine; tolerances for residues.

Commodity Parts per (a) General. (1) Tolerances are estab- million lished for residues of phosphine in or Bean, snap, succulent ...... 0 .05 on the following raw agricultural com- Carrot, roots ...... 0.45 modities (RACs) resulting from post- Celeriac, roots ...... 0 .05 Celeriac, tops ...... 0 .20 harvest fumigation for the control of Cilantro, leaves ...... 3 .5 insects with phosphine gas or

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phosphide compounds that produce Commodity Parts per phosphine gas. million Processed food ...... 0 .01 Parts per Commodity million (4) Residues resulting from fumigation Almond ...... 0.1 of animal feed: Avocado ...... 0 .01 Banana ...... 0.01 Parts per Barley, grain ...... 0 .1 Commodity million Cabbage, Chinese, bok choy ...... 0.01 Cabbage, Chinese, napa ...... 0 .01 Animal feed ...... 0.1 Cacao bean, dried bean ...... 0 .1 Cashew ...... 0 .1 (5) To assure safe use of this pes- Citron, citrus ...... 0 .01 Coffee, bean, green ...... 0 .1 ticide, it must be used in compliance Corn, field, grain ...... 0 .1 with the labeling conforming to that Corn, pop, grain ...... 0.1 registered by the U.S. Environmental Cotton, undelinted seed ...... 0 .1 Protection Agency (EPA) under Date, dried fruit ...... 0 .1 Dill, seed ...... 0 .01 FIFRA. Labeling shall bear a restric- Eggplant ...... 0.01 tion to aerate the finished food/feed for Endive ...... 0.01 48 hours before it is offered to the con- Grapefruit ...... 0 .01 sumer, unless EPA specifically deter- Hazelnut ...... 0 .1 Kumquat ...... 0 .01 mines that a different time period is Lemon ...... 0.01 appropriate. Where appropriate, a Lettuce ...... 0.01 warning shall state that under no con- Lime ...... 0.01 dition should any formulation con- Mango ...... 0.01 Millet, grain ...... 0 .1 taining aluminum or magnesium Mushroom ...... 0 .01 phosphide be used so that it will come Nut, brazil ...... 0 .1 in contact with any processed food, ex- Oat, grain ...... 0 .1 cept processed brewer’s rice, malt, and Okra ...... 0.01 Orange, sweet ...... 0 .01 corn grits stored in breweries for use in Papaya ...... 0 .01 the manufacture of beer. Peanut ...... 0 .1 (b) Section 18 emergency exemptions. Pecan ...... 0 .1 [Reserved] Pepper ...... 0 .01 Persimmon ...... 0 .01 (c) Tolerances with regional registra- Pistachio ...... 0.1 tions. [Reserved] Rice, grain ...... 0 .1 (d) Indirect or inadvertant residues. Rye, grain ...... 0.1 [Reserved] Safflower, seed ...... 0 .1 Salsify, tops ...... 0 .01 [64 FR 72950, Dec. 29, 1999, as amended at 71 Sesame, seed ...... 0 .1 FR 74816, Dec. 13, 2006; 72 FR 41929, Aug. 1, Sorghum, grain ...... 0 .1 2007; 74 FR 46372, Sept. 9, 2009] Soybean, seed ...... 0 .1 Sunflower, seed ...... 0.1 Sweet potato, roots ...... 0 .01 § 180.226 Diquat; tolerances for resi- Tangelo ...... 0 .01 dues. Tangerine ...... 0 .01 (a) General. (1) Tolerances are estab- Tomato ...... 0.01 Vegetable, legume, group 6, except soybean .... 0 .01 lished for residues of the plant growth Walnut ...... 0 .1 regulator and herbicide diquat, (6,7- Wheat, grain ...... 0 .1 dihydrodipyrido (1,2-a:2′1′- c)pyrazinediium) derived from applica- (2) Tolerances are established for res- tion of the dibromide salt and cal- idues of the fumigant in or on all RACs culated as the cation in or on the fol- resulting from preharvest treatment of lowing food commodities: pest burrows in agricultural and non- crop land areas. Parts per Commodity million Parts per Commodity million Alfalfa, seed ...... 3 .0 Cattle, fat ...... 0.05 All raw agricultural commodities resulting from Cattle, meat ...... 0 .05 preharvest treatment of pest burrows ...... 0 .01 Cattle, meat byproducts ...... 0.05 Canola, meal ...... 6 .0 Canola, seed ...... 2 .0 (3) Residues resulting from fumiga- Egg ...... 0 .05 tion of processed food: Goat, fat ...... 0 .05

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the aquatic uses cited in this para- Commodity Parts per million graph. Goat, meat ...... 0.05 (3) Tolerances are established for the Goat, meat byproducts ...... 0 .05 plant growth regulator diquat (6,7 Hog, fat ...... 0 .05 dihydrodipyrido(1,2-a:2’1’- Hog, meat ...... 0 .05 Hog, meat byproducts ...... 0 .05 c)pyrazinediium) derived from applica- Horse, fat ...... 0 .05 tion of the dibromide salt and cal- Horse, meat ...... 0 .05 culated as the cation in or on the fol- Horse, meat byproducts ...... 0 .05 Milk ...... 0.02 lowing food commodites: Potato ...... 0 .1 Poultry, fat ...... 0.05 Parts per Commodity million Poultry, meat ...... 0 .05 Poultry, meat byproducts ...... 0.05 Banana1 ...... 0 .05 Sheep, fat ...... 0 .05 Coffee, bean, green1 ...... 0 .05 Sheep, meat ...... 0.05 Soybean, hulls ...... 0 .6 Sheep, meat byproducts ...... 0 .05 1There are no U.S. registrations as of May 26, 2010. (2)(i) Tolerances are established for (4) A tolerance of 0.5 part per million residues of the herbicide diquat (6,7 is established for residues of diquat in dihydrodipyrido(1,2-a:2’1’- potato, granules/flakes and potato, c)pyrazinediium) (calculated as the chips. cation) derived from the application of (b) Section 18 emergency exemptions. the dibromide salt to ponds, lakes, res- [Reserved] ervoirs, marshes, drainage ditches, ca- (c) Tolerances with regional registra- nals, streams, and rivers which are tions. [Reserved] slow-moving or quiescent in programs (d) Indirect or inadvertent residues. of the Corp of Engineers or other Fed- [Reserved] eral or State public agencies and to ponds, lakes and drainage ditches only [65 FR 33709, May 24, 2000, as amended at 72 where there is little or no outflow of FR 41929, Aug. 1, 2007; 75 FR 29441, May 26, 2010; 75 FR 60241, Sept. 29, 2010] water and which are totally under the control of the user, in or on the fol- § 180.227 Dicamba; tolerances for resi- lowing food commodities: dues. (a) General. (1) Tolerances are estab- Commodity Parts per million lished for the residues of the herbicide Avocado ...... 0 .2 dicamba (3,6-dichloro-o-anisic acid), in- Berry group 13 ...... 0 .05 cluding its metabolites and degradates, Cotton, undelinted seed ...... 0 .2 in or on the commodities in the table Cranberry ...... 0 .05 below. Compliance with the tolerance Fish ...... 2 .0 Fruit, citrus, group 10 ...... 0 .05 levels is to be determined by meas- Fruit, pome, group 11 ...... 0.02 uring only the sum of the residues of Fruit, stone, group 12 ...... 0 .02 dicamba (3,6-dichloro-o-anisic acid) and Grain, cereal, forage, fodder and straw, group 16 ...... 0 .02 its metabolite, 3,6-dichloro-5-hydroxy- Grain, cereal, group 15 ...... 0.02 o-anisic acid, calculated as the stoi- Grape ...... 0 .05 chiometric equivalent of dicamba, in or Grass, forage, fodder and hay, group 17 ...... 0 .2 on the following commodities: Hop, dried cones ...... 0 .2 Nut, tree, group 14 ...... 0 .02 Parts per Shellfish ...... 20 .0 Commodity million Strawberry ...... 0 .05 Sugarcane, cane ...... 0.2 Barley, grain ...... 6 .0 Vegetable, brassica, leafy, group 5 ...... 0.05 Barley, hay ...... 2 .0 Vegetable, cucurbit, group 9 ...... 0.02 Barley, straw ...... 15 .0 Vegetable, foliage of legume, group 7 ...... 0 .2 Corn, field, forage ...... 3 .0 Vegetable, fruiting, group 8 ...... 0.05 Corn, field, grain ...... 0 .1 Vegetable, leafy, except brassica, group 4 ...... 0 .05 Corn, field, stover ...... 3 .0 Vegetable, root and tuber, group 1 ...... 0 .02 Corn, pop, grain ...... 0.1 Vegetable, seed and pod ...... 0 .05 Corn, pop, stover ...... 3.0 Corn, sweet, forage ...... 0 .50 (ii) Where tolerances are established Corn, sweet, kernel plus cob with husks re- at higher levels from other uses of moved ...... 0 .04 Corn, sweet, stover ...... 0 .50 diquat on the subject crops, the higher Cotton, undelinted seed ...... 0 .2 tolerances applies also to residues of Grass, forage, fodder and hay, group 17, forage 125 .0

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metabolites and degradates, in or on Commodity Parts per million the commodities in the table below. Grass, forage, fodder and hay, group 17, hay .... 200 .0 Compliance with the tolerance levels is Millet, proso, forage ...... 90.0 to be determined by measuring only Millet, proso, grain ...... 2 .0 the residues of dicamba, 3,6-dichloro-o- Millet, proso, hay ...... 40 .0 Millet, proso, straw ...... 30 .0 anisic acid, and its metabolites, 3,6- Oat, forage ...... 90 .0 dichloro-5-hydroxy-o-anisic acid, and Oat, grain ...... 2 .0 3,6-dichloro-2-hydroxybenzoic acid, cal- Oat, hay ...... 40.0 Oat, straw ...... 30.0 culated as the stoichiometric equiva- Rye, forage ...... 90 .0 lent of dicamba, in or on the following Rye, grain ...... 2.0 commodities: Rye, straw ...... 30 .0 Sorghum, grain, forage ...... 3.0 Parts per Sorghum, grain, grain ...... 4 .0 Commodity million Sorghum, grain, stover ...... 10 .0 Sugarcane, cane ...... 0.3 Grain, aspirated fractions ...... 1000 Sugarcane, molasses ...... 5 .0 Soybean, hulls ...... 30 .0 Teff, forage ...... 90.0 Soybean, seed ...... 10.0 Teff, grain ...... 6 .0 Teff, hay ...... 40.0 Teff, straw ...... 30 .0 (b) Section 18 emergency exemptions. Wheat, forage ...... 90.0 [Reserved] Wheat, grain ...... 2 .0 (c) Tolerances with regional registra- Wheat, hay ...... 40 .0 tions. [Reserved] Wheat, straw ...... 30 .0 (d) Indirect or inadvertent residues. (2) Tolerances are established for res- [Reserved] idues of the herbicide dicamba, 3,6- [65 FR 33709, May 24, 2000, as amended at 72 dichloro-o-anisic acid, including its FR 35665, June 29, 2007; 73 FR 17918, Apr. 2, metabolites and degradates, in or on 2008; 73 FR 54960, Sept. 24, 2008; 75 FR 60241, the commodities in the table below. Sept. 29, 2010; 76 FR 55806, Sept. 9, 2011] Compliance with the tolerance levels is § 180.229 Fluometuron; tolerances for to be determined by measuring only residues. the residues of dicamba (3,6-dichloro-o- anisic acid) and its metabolite, 3,6- (a) General. (1) Tolerances are estab- dichloro-2-hydroxybenzoic acid, cal- lished for the combined residues of the culated as the stoichiometric equiva- herbicide fluometuron, N, N-dimethyl- lent of dicamba, in or on the following N’-[3-(trifluoromethyl)phenyl]urea, and commodities: its metabolite, trifluoromethylaniline (TFMA) determined as TFMA, in or on Parts per the following food commodities: Commodity million Parts per Asparagus ...... 4.0 Commodity million Cattle, fat ...... 0.3 Cattle, kidney ...... 25 .0 Cotton, gin byproducts ...... 3 .5 Cattle, meat ...... 0 .25 Cotton, undelinted seed ...... 1 .0 Cattle, meat byproducts, except kidney ...... 3.0 Goat, fat ...... 0 .3 Goat, kidney ...... 25.0 (2) Tolerances are established for the Goat, meat ...... 0.25 combined residues of the herbicide Goat, meat byproducts, except kidney ...... 3 .0 fluometuron, N,N-dimethyl-N’-[3- Hog, fat ...... 0 .3 (trifluoromethyl)phenyl]urea, and its Hog, kidney ...... 25.0 Hog, meat ...... 0 .25 metabolites determined as TFMA and Hog, meat byproducts, except kidney ...... 3 .0 the hydroxylated metabolites: CGA- Horse, fat ...... 0 .3 236431, 1-(4-hydroxy-3- Horse, kidney ...... 25 .0 Horse, meat ...... 0 .25 trifluoromethylphenyl)urea; CGA- Horse, meat byproducts, except kidney ...... 3 .0 236432, 1-methyl-3-(4-hydroxy-3- Milk ...... 0.2 trifluoromethylphenyl)urea; and CGA- Sheep, fat ...... 0 .3 Sheep, kidney ...... 25.0 13211, 1,1-dimethyl-3-(4-hydroxy-3- Sheep, meat ...... 0.25 trifluoromethylphenyl)urea, in or on Sheep, meat byproducts, except kidney ...... 3 .0 the following food commodities:

(3) Tolerances are established for res- Commodity Parts per idues of the herbicide dicamba, 3,6- million dichloro-o-anisic acid, including its Cattle, meat byproducts ...... 0.1

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(b) Section 18 emergency exemptions. Commodity Parts per million [Reserved] Egg ...... 0 .1 (c) Tolerances with regional registra- Goat, meat byproducts ...... 0 .1 tion. [Reserved] Hog, meat byproducts ...... 0 .1 (d) Indirect or inadvertent residues. Horse, meat byproducts ...... 0 .1 [Reserved] Milk ...... 0.02 Poultry, fat ...... 0.1 [36 FR 22540, Nov. 25, 1971, as amended at 63 Poultry, meat ...... 0 .1 FR 57075, Oct. 26, 1998; 66 FR 63198, Dec. 5, Poultry, meat byproducts ...... 0.1 2001; 73 FR 50570, Aug. 27, 2008] Sheep, meat byproducts ...... 0 .1 § 180.232 Butylate; tolerances for resi- (b) Section 18 emergency exemptions. dues. [Reserved] (a) General. Tolerances are estab- (c) Tolerances with regional registra- lished for residues of the herbicide tions. [Reserved] butylate, including its metabolites and (d) Indirect or inadvertent residues. degradates, in or on the commodities Tolerances are established for the com- in the table in this paragraph. Compli- bined residues of the herbicide ance with the tolerance levels specified fluometuron, N, N-dimethyl-N’-[3- in this paragraph is to be determined (trifluoromethyl)phenyl]urea, and its by measuring only butylate, S-ethyl bis metabolite, trifluoromethylaniline (2-methylpropyl) carbamothioate, in or (TFMA) determined as TFMA, in or on on the commodity. the following food commodities.

Parts per Expiration/ Commodity Parts per Commodity revocation million million date

Grain, cereal, forage, fodder, and straw group Corn, field, forage ...... 0.1 3/23/13 16, forage ...... 3 .0 Corn, field, grain ...... 0.1 3/23/13 Grain, cereal, forage, fodder, and straw, group Corn, field, stover ...... 0.1 3/23/13 16, stover ...... 6 .0 Corn, pop, grain ...... 0.1 3/23/13 Grain, cereal, group 15 ...... 0.5 Corn, pop, stover ...... 0.1 3/23/13 Peanut ...... 0 .1 Corn, sweet, forage ...... 0.1 3/23/13 Peanut, hay ...... 4.0 Corn, sweet, kernel plus cob with Peanut, meal ...... 0 .2 husks removed ...... 0.1 3/23/13 Soybean, forage ...... 3 .0 Soybean, hay ...... 3 .0 (b) Section 18 emergency exemptions. Soybean, seed ...... 2 .0 [Reserved] Rice, hulls ...... 1 .0 Wheat, milled byproducts ...... 1 .0 (c) Tolerances with regional registrations. [Reserved] (d) Indirect or inadvertent residues. [73 FR 52613, Sept. 10, 2008] [Reserved] § 180.231 Dichlobenil; tolerances for [68 FR 39439, July 1, 2003, as amended at 76 residues. FR 23493, Apr. 27, 2011; 77 FR 59125, Sept. 26, (a) General. Tolerances are estab- 2012] lished for the combined residues of the EFFECTIVE DATE NOTE: At 81 FR 34905, June herbicide dichlobenil (2,6- 1, 2016, § 180.232 was removed, effective Nov. dichlorobenzonitrile) and its metabo- 28, 2016. lite 2,6-dichlorobenzamide in or on the following raw agricultural commod- § 180.235 Dichlorvos; tolerances for ities: residues. (a) General. (1) Tolerances for resi- Parts per dues of the insecticide 2,2-dichlorovinyl Commodity million dimethyl phosphate are established as Apple ...... 0.5 follows: Bushberry subgroup 13–07B ...... 0 .15 Caneberry subgroup 13–07A ...... 0.10 Commodity Parts per Cranberry ...... 0 .1 million Fruit, stone, group 12 ...... 0 .15 Grape ...... 0 .15 Cattle, fat ...... 0.02(N) Hazelnut ...... 0 .1 Cattle, meat ...... 0 .02(N) Pear ...... 0 .5 Cattle, meat byproducts ...... 0.02(N) Rhubarb ...... 0 .06 Egg ...... 0 .05(N) Goat, fat ...... 0 .02(N)

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oxide metabolites, expressed in terms Commodity Parts per million of parent TPTH, in or on the following Goat, meat ...... 0.02(N) raw agricultural commodities: Goat, meat byproducts ...... 0 .02(N) Horse, fat ...... 0 .02(N) Commodity Parts per Horse, meat ...... 0 .02(N) million Horse, meat byproducts ...... 0 .02(N) Milk ...... 0.02(N) Beet, sugar, roots ...... 0 .05 Mushroom (residues expressed as naled) ...... 0 .5 Beet, sugar, tops ...... 10.0 Poultry, fat ...... 0.05(N) Cattle, fat ...... 0.2 Poultry, meat ...... 0 .05(N) Cattle, kidney ...... 2 .0 Poultry, meat byproducts ...... 0.05(N) Cattle, liver ...... 4 .0 Raw agricultural commodities, nonperishable, Cattle, meat ...... 0 .5 bulk stored regardless of fat content, Goat, fat ...... 0 .2 postharvest ...... 0.5 Goat, kidney ...... 2 .0 Raw agricultural commodities nonperishable, Goat, liver ...... 4.0 Goat, meat ...... 0.5 packaged or bagged, containing 6 percent fat Hog, fat ...... 0 .3 or less, postharvest ...... 0.5 Hog, meat ...... 0 .06 Raw agricultural commodities, nonperishable, Hog, meat byproducts ...... 0 .3 packaged or bagged, containing more than 6 Horse, fat ...... 0 .2 percent fat, postharvest ...... 2 Horse, kidney ...... 2 .0 Sheep, fat ...... 0 .02(N) Horse, liver ...... 4 .0 Sheep, meat ...... 0.02(N) Horse, meat ...... 0 .5 Sheep, meat byproducts ...... 0 .02(N) Milk ...... 0.06 Pecan ...... 0 .05 (2) The tolerance of 0.1 part per mil- Potato ...... 0 .05 lion prescribed by 21 CFR 556.180 for Sheep, fat ...... 0 .2 Sheep, kidney ...... 2.0 negligible residues of 2,2-dichlorovinyl Sheep, liver ...... 4.0 dimethyl phosphate in hog, fat; hog, Sheep, meat ...... 0.5 meat; hog, meat byproducts; and hog, skin covers both its use as an anthel- (b) Section 18 emergency exemptions. mintic in swine feed and as an insecti- [Reserved] cide applied directly to swine. (c) Tolerances with regional registra- (3) Dichlorvos may be present as a tions. [Reserved] residue from application as an insecti- (d) Indirect or inadvertent residues. cide on packaged or bagged nonperish- [Reserved] able processed food (see: 21 CFR [72 FR 41929, Aug. 1, 2007] 170.3(j)) in an amount in such food not in excess of 0.5 part per million (ppm). § 180.241 Bensulide; tolerances for res- To assure safe use of the insecticide, idues. its label and labeling shall conform to (a) General. Tolerances are estab- the label and labeling registered by the lished for the residues of S-(O,O- U.S. Environmental Protection Agen- diisopropyl phosphorodithioate) of N- cy, and the usage employed shall con- (2-mercaptoethyl) benzenesulfonamide form with such label or labeling. including its oxygen analog S-(O,O- (b) Section 18 emergency exemptions. diisopropyl phosphorothioate) of N-(2- [Reserved] mercaptoethyl) benzenesulfonamide in (c) Tolerances with regional registra- or on the following food commodities: tions. [Reserved] (d) Indirect or inadvertent residues. Commodity Parts per [Reserved] million Onion, bulb ...... 0 .10 [47 FR 55223, Dec. 8, 1982, as amended at 55 Vegetable, brassica, leafy group 5 ...... 0 .15 FR 26440, June 28, 1990; 56 FR 29183, June 26, Vegetable, cucurbits group 9 ...... 0 .15 1991; 63 FR 57075, Oct. 26, 1998; 65 FR 33697, Vegetable, fruiting group 8 ...... 0 .10 May 24, 2000; 74 FR 46373, Sept. 9, 2009; 77 FR Vegetable, leafy except brassica group 4 ...... 0 .15 59125, Sept. 26, 2012] (b) Section 18 emergency exemptions. § 180.236 Triphenyltin hydroxide; tol- [Reserved] erances for residues. (c) Tolerances with regional registra- (a) General. Tolerances are estab- tions. Tolerances with regional reg- lished for the combined residues of the istration, as defined in § 180.1(l), are es- fungicide triphenyltin hydroxide tablished for the residues of S-(O,O- (TPTH) and its monophenyltin (MPTH) diisopropyl phosphorodithioate) of N- and diphenyltin (DPTH) hydroxide and (2-mercaptoethyl) benzenesulfonamide

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including its oxygen analog S-(O,O- Commodity Parts per diisopropyl phosphorothioate) of N-(2- million mercaptoethyl) benzenesulfonamide in Rye, forage ...... 0 .30 or on the following food commodities: Rye, grain ...... 0.05 Rye, straw ...... 0 .30 Soybean ...... 0.1 Commodity Parts per million Spinach ...... 0 .02 Strawberry 1 ...... 5 .0 Carrot, roots ...... 0.10 Sweet potato (postharvest to sweet potato intended only for use as seed) ...... 0 .05 (d) Indirect or inadvertent residues. Triticale, forage ...... 0 .30 [Reserved] Triticale, grain ...... 0 .05 Triticale, hay ...... 0 .30 [68 FR 39440, July 1, 2003, as amended at 73 Triticale, straw ...... 0 .30 FR 53738, Sept. 17, 2008] Vegetable, cucurbit, group 9 ...... 0.02 Vegetable, root (except sugarbeet), subgroup 1B ...... 0 .02 § 180.242 Thiabendazole; tolerances for Wheat, forage ...... 0 .30 residues. Wheat, grain ...... 0 .05 (a) General. (1) Tolerances are estab- Wheat, hay ...... 0 .30 Wheat, straw ...... 0 .30 lished for residues of thiabendazole, in- 1There are no U.S. registrations on the indicated cluding its metabolites and degradates, commodity. in or on the commodities in the table below. Compliance with the tolerance (2) Tolerances are established for res- levels specified below is to be deter- idues of thiabendazole, including its mined by measuring only the sum of metabolites and degradates, in or on thiabendazole (2-(4- the commodities in the table below. thiazolyl)benzimidazole) and its me- Compliance with the tolerance levels tabolite benzimidazole (free and con- specified below is to be determined by jugated), calculated as the stoichio- measuring only the sum of metric equivalent of thiabendazole, in thiabendazole (2-(4- or on the commodity. thiazolyl)benzimidazole) and its metabolites 5-hydroxythiabendazole (free Commodity Parts per and conjugated) and benzimidazole million (free and conjugated), calculated as the Alfalfa, forage ...... 0.02 stoichiometric equivalent of Alfalfa, hay ...... 0.02 thiabendazole, in or on the commodity. Apple, wet pomace ...... 12.0 1 Avocado ...... 10.0 Parts per Banana, postharvest ...... 3 .0 Commodity million Barley, grain ...... 0 .05 Barley, hay ...... 0 .30 Cattle, meat ...... 0 .1 Barley, straw ...... 0 .30 Cattle, meat byproducts ...... 0.4 Bean, dry, seed ...... 0 .1 Goat, meat byproducts ...... 0 .4 Brassica, head and stem, subgroup 5A ...... 0 .02 Hog, meat byproducts ...... 0 .3 Cantaloupe 1 ...... 15.0 Horse, meat byproducts ...... 0 .4 Carrot, roots, postharvest ...... 10 .0 Milk ...... 0.1 Citrus, oil ...... 15.0 Sheep, meat byproducts ...... 0 .4 Corn, field, forage ...... 0 .01 Corn, field, grain ...... 0 .01 Corn, field, stover ...... 0 .01 (b) Section 18 emergency exemptions. Corn, pop, forage ...... 0 .01 Time-limited tolerances specified in Corn, pop, grain ...... 0.01 the following table are established for Corn, pop, stover ...... 0.01 residues of the thiabendazole, includ- Corn, sweet, forage ...... 0 .01 Corn, sweet, kernels plus cop with husks re- ing its metabolites and degradates, in moved ...... 0 .01 or on the specified agricultural com- Corn, sweet, stover ...... 0 .01 modities, resulting from use of the pes- Fruit, citrus, group 10, postharvest ...... 10 .0 Fruit, pome, group 11, postharvest ...... 5 .0 ticide pursuant to FIFRA section 18 Mango ...... 10.0 emergency exemptions. Compliance Mushroom ...... 40 .0 with the tolerance levels specified Oats, forage ...... 0 .30 below is to be determined by measuring Oats, grain ...... 0 .05 Oats, hay ...... 0.30 only the sum of thiabendazole (2-(4- Oats, straw ...... 0.30 thiazolyl)benzimidazole) and its me- Onion, bulb, subgroup 3–07A ...... 0 .02 tabolite benzimidazole (free and con- Papaya, postharvest ...... 5 .0 Potato, postharvest ...... 10 .0 jugated), calculated as the stoichio- Radish, tops ...... 0 .02 metric equivalent of thiabendazole.

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The tolerances expire on the date spec- Commodity Parts per ified in the table. million Bean, dry, seed ...... 0 .5 Parts per Expiration Bean, succulent ...... 0 .5 Commodity million date Fruit, pome, group 11 ...... 0.25 Pea, succulent shelled ...... 0.02 12/31/18 (2) Tolerances are established for res- (c) Tolerances with regional exemptions. idues of the fungicide streptomycin [Reserved] from treatment of seedling plants be- (d) Indirect or inadvertent residues. fore transplanting in or on the fol- [Reserved] lowing food commodities: [42 FR 32783, June 28, 1977] Parts per Commodity million EDITORIAL NOTE: For FEDERAL REGISTER ci- Celery ...... 0 .25 tations affecting § 180.242, see the List of CFR Pepper ...... 0 .25 Sections Affected, which appears in the Tomato ...... 0.25 Finding Aids section of the printed volume and at www.fdsys.gov. (3) Tolerances are established for residues of the fungicide streptomycin § 180.243 Propazine; tolerances for res- from treatment of seed pieces in or on idues. the following food commodity: (a) General. Tolerances are established for residues of the herbicide Parts per Commodity million propazine, 2-chloro-4,6- bis(isopropylamino)-s-triazine, includ- Potato ...... 0 .25 ing its metabolites and degradates, in or on the commodities in the following (b) Section 18 emergency exemptions. table. Compliance with the tolerance Time-limited tolerances are estab- levels specified in this paragraph is to lished for residues of streptomycin, in be determined by measuring only the or on the agricultural commodities, as sum of propazine, 2-chloro-4,6- specified in the following table, result- bis(isopropylamino)-s-triazine, and its ing from use of the pesticide pursuant two chlorinated degradates, 2-amino-4- to FIFRA section 18 emergency exemp- chloro-6-isopropylamino-s-triazine and tions. Compliance with the tolerance 2,4-diamino-6-chloro-s-triazine, cal- levels listed in the following table is to culated as the stoichiometric equiva- be determined by measuring the levels lent of propazine, in or on the com- of streptomycin only, in or on the commodity. modities listed in the table. The tolerances expire on the dates specified in Parts per the table. Commodity million Parts per Expiration Sorghum, grain, forage ...... 0.25 Commodity million date Sorghum, grain, grain ...... 0 .25 Sorghum, grain, stover ...... 0 .25 Grapefruit ...... 0.15 12/31/2018 Grapefruit, dried pulp ...... 0.40 12/31/2018 (b) Section 18 emergency exemptions. (c) Tolerances with regional registra- [Reserved] tions. [Reserved] (c) Tolerances with regional registra- (d) Indirect or inadvertent residues. tions. [Reserved] [Reserved] (d) Indirect or inadvertent residues. [Reserved] [68 FR 39440, July 1, 2003, as amended at 73 FR 54960, Sept. 24, 2008; 78 FR 29055, May 17, [75 FR 60242, Sept. 29, 2010] 2013; 80 FR 78145, Dec. 16, 2015]

§ 180.245 Streptomycin; tolerances for § 180.249 Alachlor; tolerances for resi- residues. dues. (a) General. (1) Tolerances are estab- (a) General. Tolerances are established for residues of the fungicide lished for combined residues of streptomycin in or on food commod- alachlor (2-chloro-2′,6″-diethyl-N- ities as follows: (methoxymethyl)acetanilide) and its

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metabolites which can be converted to Commodity Parts per 2,6-diethylaniline (DEA) or 2-ethyl-6-(1- million hydroxyethyl)aniline (1-HEEA) upon Animal feed, nongrass, group 18, forage ...... 1 .4 basic hydrolysis, calculated as alachlor Animal feed, nongrass, group 18, hay ...... 1.2 in or on the following raw agricultural Grain, cereal, forage, and straw, group 16 ex- commodities. cept corn, sorghum, rice, straw ...... 0 .8 Grain, cereal, forage, fodder and straw, group Parts per 16 except corn, sorghum, rice, forage ...... 0 .6 Commodity million Grain, cereal, forage, fodder, and straw, group 16 except for corn, sorghum, rice, hay ...... 0 .8 Beans, dry ...... 0.1 Grain, cereal, group 15 except corn, sorghum, Beans, succulent lima ...... 0 .1 rice ...... 0 .05 Cattle, fat ...... 0.02 Cattle, meat byproducts ...... 0.02 Cattle, meat ...... 0 .02 [72 FR 54584, Sept. 26, 2007] Corn, field, forage ...... 2 .0 Corn, field, grain ...... 0 .2 § 180.252 Tetrachlorvinphos; toler- Corn, field, pop ...... 0 .2 ances for residues. Corn, field, stover ...... 2 .0 Corn, pop, stover ...... 2.0 (a) General. Tolerances are estab- Corn, sweet (K + CWHR) ...... 0 .05 lished for the combined residues of the Corn, sweet, stover ...... 2 .0 Cotton, gin byproducts ...... 0 .7 insecticide tetrachlorvinphos [(Z)-2- Cotton, undelinted seed ...... 0 .03 chloro-1-(2,4,5-trichlorophenyl) vinyl Cowpea, forage ...... 5 .0 dimethyl phosphate], including its me- Cowpea, hay ...... 5 .0 Egg ...... 0 .02 tabolites, 1-(2,4,5-trichlorophenyl)-eth- Goat, fat ...... 0 .02 anol (free and conjugated forms), 2,4,5- Goat, meat byproducts ...... 0 .02 trichloroacetophenone, and 1-(2,4,5- Goat, meat ...... 0.02 trichlorophenyl)-ethanediol, in or on Hog, fat ...... 0 .02 Hog meat byproducts ...... 0 .02 the following commodities: Hog, meat ...... 0 .02 Horse, fat ...... 0 .02 Commodity Parts per Horse, meat byproducts ...... 0 .02 million Horse, meat ...... 0 .02 Milk ...... 0.02 Cattle, fat (of which no more than 0.1 ppm is Peanut ...... 0 .5 tetrachlorvinphos per se) ...... 0 .2 Poultry, fat ...... 0.02 Cattle, kidney (of which no more than 0.05 Poultry, meat byproducts ...... 0.02 ppm is tetrachlorvinphos per se) ...... 1 .0 Poultry, meat ...... 0 .02 Cattle, liver (of which no more than 0.05 ppm Sheep, fat ...... 0 .02 is tetrachlorvinphos per se) ...... 0 .5 Sheep, meat byproducts ...... 0 .02 Cattle, meat (of which no more than 2.0 ppm is Sheep, meat ...... 0.02 tetrachlorvinphos per se) ...... 2 .0 Sorghum grain, forage ...... 2 .0 Cattle, meat byproducts, except kidney and Sorghum, grain, grain ...... 0 .1 liver ...... 1 .0 Sorghum, grain, stover ...... 1 .0 Egg (of which no more than 0.05 ppm is Soybeans, seed ...... 1 .0 tetrachlorvinphos per se) ...... 0 .2 Sunflower, meal ...... 3 .4 Hog, fat (of which no more than 0.1 ppm is Sunflower, seed ...... 2.5 tetrachlorvinphos per se) ...... 0 .2 Hog, kidney (of which no more than 0.05 ppm (b) Section 18 emergency exemptions. is tetrachlorvinphos per se) ...... 1.0 [Reserved] Hog, liver (of which no more than 0.05 ppm is tetrachlorvinphos per se) ...... 0 .5 (c) Tolerances with regional registra- Hog, meat (of which no more than 2.0 ppm is tions. [Reserved] tetrachlorvinphos per se) ...... 2.0 (d) Indirect or inadvertent residues. Hog, meat byproducts, except kidney and liver 1 .0 Tolerances are established for indirect Milk, fat (reflecting negligible residues in whole milk and of which no more than 0.05 ppm is or inadvertent residues of alachlor (2- tetrachlorvinphos per se) ...... 0 .05 chloro-2′,6′-diethyl-N- Poultry, fat (of which no more than 7.0 ppm is (methoxymethyl)acetanilide) and its tetrachlorvinphos per se) ...... 7 .0 metabolites which can be converted to Poultry, liver (of which no more than 0.05 ppm is tetrachlorvinphos per se) ...... 2 .0 2,6-diethylaniline (DEA) or 2-ethyl-6-(1- Poultry, meat (of which no more than 3.0 ppm hydroxyethyl)aniline (1-HEEA) upon is tetrachlorvinphos per se) ...... 3 .0 basic hydrolysis, calculated as Poultry, meat byproducts, except liver ...... 2 .0 alachlor, in or on the following raw agricultural commodities when present (b) Section 18 emergency exemptions. therein as a result of the application of [Reserved] alachlor to the growing crops in para- (c) Tolerances with regional registra- graph (a) of this section: tions. [Reserved]

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(d) Indirect or inadvertent residues. Parts per Expiration/ [Reserved] Commodity revocation million date [76 FR 57659, Sept. 16, 2011, as amended at 78 Oat, straw ...... 10 None FR 15882, Mar. 13, 2013; 78 FR 53684, Aug. 30, Onion, dry bulb ...... 0.2 None 2013] Onion, green ...... 3 None Orange ...... 2 None § 180.253 Methomyl; tolerances for res- Parsley, leaves ...... 6 None idues. Pea ...... 5 None (a) General. Tolerances are estab- Pea, field, vines ...... 10 None Peach ...... 5 None lished for residues of the insecticide Peanut ...... 0.1 None methomyl, including its metabolites Pecan ...... 0.1 None and degradates, in or on the commod- Pepper, bell ...... 2 None ities in the table in this paragraph. Pepper, nonbell ...... 2 None Compliance with the tolerance levels Peppermint, tops ...... 2 None Pomegranate ...... 0.2 None specified in this paragraph is to be de- Rye, forage ...... 10 None termined by measuring only Rye, grain ...... 1 None methomyl, methyl N- Rye, straw ...... 10 None [[(methylamino)carbonyl]oxy]ethani Sorghum, grain, forage ...... 1 None midothioate, in or on the commodity. Sorghum, grain, grain ...... 0.2 None Soybean, forage ...... 10 None Expiration/ Soybean, seed ...... 0.2 None Parts per Spearmint, tops ...... 2 None Commodity million revocation date Spinach ...... 6 None Swiss chard ...... 6 None Alfalfa, forage ...... 10 None Tangerine ...... 2 None Alfalfa, hay ...... 10 None Tomato ...... 1 None Apple ...... 1 None Turnip, greens ...... 6 None Asparagus ...... 2 None Vegetable, brassica, leafy, group 5 6.0 None Avocado ...... 2 None Vegetable, cucurbit, group 9 ...... 0.2 None Barley, grain ...... 1 None Barley, hay ...... 10 None Vegetable, fruiting, group 8 ...... 0.2 None Barley, straw ...... 10 None Vegetables, leafy 2 ...... 0.2 None Bean, dry, seed ...... 0.1 None Vegetable, root and tuber, group 1 0.2 None Bean, forage ...... 10 None Wheat, forage ...... 10 None Bean, succulent ...... 2 None Wheat, grain ...... 1 None Beet, garden, tops ...... 6 None Wheat, hay ...... 10 None Bermudagrass, forage ...... 10 None Wheat, straw ...... 10 None Bermudagrass, hay ...... 40 None Blueberry ...... 6 None 1 There are no U.S. registrations for use of methomyl on Broccoli ...... 3 None hop, dried cone, as of February 14, 1990. 2 Except for Beet (tops), broccoli, Brussels sprouts, cab- Brussels sprouts ...... 2 None bage, cabbage, Chinese, cauliflower, celery, collards, dan- Cabbage ...... 5 None delions, endive (escarole), kale, lettuce, mustard greens, pars- Cabbage, Chinese, bok choy ...... 5 None ley, spinach, Swiss chard, turnip, greens (tops), and Cabbage, Chinese, napa ...... 5 None watercress. Cauliflower ...... 2 None Celery ...... 3 None (b) Section 18 emergency exemptions. Collards ...... 6 None [Reserved] Corn, field, forage ...... 10 None Corn, field, grain ...... 0.1 None (c) Tolerances with regional registra- Corn, field, stover ...... 10 None tions. A tolerance with regional reg- Corn, pop, grain ...... 0.1 None istration, as defined in § 180.1(l), is es- Corn, pop, stover ...... 10 None tablished for residues of the insecticide Corn, sweet, forage ...... 10 None Corn, sweet, kernel plus cob with methomyl, including its metabolites husks removed ...... 0.1 None and degradates, in or on the com- Corn, sweet, stover ...... 10 None modity in the table in this paragraph. Cotton, undelinted seed ...... 0.1 None Dandelion, leaves ...... 6 None Compliance with the tolerance level Endive ...... 5 None specified in this paragraph is to be de- Grape ...... 5 12/31/16 termined by measuring only Grapefruit ...... 2 None Hop, dried cones 1 ...... 12 None methomyl, methyl N-[[ Kale ...... 6 None (methylamino)carbonyl]oxy] Lemon ...... 2 None ethanimidothioate, in or on the com- Lentil, seed ...... 0.1 None modity. Lettuce ...... 5 None Mustard greens ...... 6 None Parts Nectarine ...... 5 None Commodity per million Oat, forage ...... 10 None Oat, grain ...... 1 None Pear ...... 4 Oat, hay ...... 10 None

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(d) Indirect or inadvertent residues. metric equivalent of chloroneb, in or [Reserved] on the commodity. [65 FR 33697, May 24, 2000, as amended at 72 Parts per Expiration/ FR 35666, June 29, 2007; 74 FR 46373, Sept. 9, Commodity million revocation 2009; 75 FR 60242, Sept. 29, 2010; 76 FR 34885, date June 15, 2011; 77 FR 59125, Sept. 26, 2012; 80 FR Bean, dry, seed ...... 0.2 4/16/12 72598, Nov. 20, 2015] Bean, succulent ...... 0.2 4/16/12 Beet, sugar, roots ...... 0.2 4/16/12 § 180.254 Carbofuran; tolerances for Beet, sugar, tops ...... 0.2 4/16/12 residues. Cowpea, forage ...... 2.0 4/16/12 Cowpea, hay ...... 2.0 4/16/12 (a) General. Tolerances are estab- Cattle, fat ...... 0.2 4/16/12 lished for the combined residues of the Cattle, meat ...... 0.2 4/16/12 insecticide carbofuran (2,3-dihydro-2,2- Cattle, meat byproducts ...... 0.2 4/16/12 Cotton, gin byproducts ...... 1.0 4/16/12 dimethyl-7-benzofuranyl-N- Cotton, undelinted seed ...... 0.2 4/16/12 methylcarbamate), its carbamate me- Goat, fat ...... 0.2 4/16/12 tabolite-2,3-dihydro-2,2-dimethyl-3-hy- Goat, meat ...... 0.2 4/16/12 Goat, meat byproducts ...... 0.2 4/16/12 droxy-7-benzofuranyl-N- Hog, fat ...... 0.2 4/16/12 methylcarbamate, and its phenolic me- Hog, meat ...... 0.2 4/16/12 tabolites 2,3-dihydro-2,2-dimethyl-7- Hog, meat byproducts ...... 0.2 4/16/12 benzofuranol, 2,3-dihydro-2,2-dimethyl- Horse, fat ...... 0.2 4/16/12 Horse, meat ...... 0.2 4/16/12 3,-oxo-7-benzofuranol and 2,3-dihydro- Horse, meat byproducts ...... 0.2 4/16/12 2,2-dimethyl-3,7-benzofurandiol in or on Milk ...... 0.05 4/16/12 the following raw agricultural com- Sheep, fat ...... 0.2 4/16/12 Sheep, meat ...... 0.2 4/16/12 modities: Sheep, meat byproducts ...... 0.2 4/16/12 Soybean, forage ...... 2.0 4/16/12 Commodity Parts per Soybean, hay ...... 2.0 4/16/12 million Soybean, seed ...... 0.2 4/16/12 Banana 1 ...... 0.1 Coffee, bean, green 1 ...... 0 .1 (b) Section 18 emergency exemptions. Rice, grain 1 ...... 0 .2 [Reserved] 1 Sugarcane, cane ...... 0.1 (c) Tolerances with regional registra- 1 There are no U.S. registrations for use of carbofuran on tions. [Reserved] these commodities. (d) Indirect or inadvertent residues. (b) Section 18 emergency exemptions. [Reserved] [Reserved] (c) Tolerances with regional registra- [68 FR 39440, July 1, 2003, as amended at 72 tions. [Reserved] FR 53460, Sept. 19, 2007; 76 FR 56654, Sept. 14, 2011] (d) Indirect or inadvertent residues. [Reserved] EFFECTIVE DATE NOTE: At 81 FR 34905, June 1, 2016, § 180.257 was removed, effective Nov. [39 FR 20597, June 12, 1974] 28, 2016. EDITORIAL NOTE: For FEDERAL REGISTER citations affecting § 180.254, see the List of CFR § 180.258 Ametryn; tolerances for resi- Sections Affected, which appears in the dues. Finding Aids section of the printed volume (a) General. Tolerances are estab- and at www.fdsys.gov. lished for residues of the desiccant and herbicide (2-ethylamino)-4- § 180.257 Chloroneb; tolerances for residues. (isopropylamino)-6-(methylthio)-s-triazine in or on the following raw agri- (a) General. Tolerances are estab- cultural commodities: lished for residues of the fungicide chloroneb, including its metabolites Expiration/ Commodity Parts per Revocation and degradates, in or on the commod- million Date ities in the table in this paragraph. Compliance with the tolerance levels Banana ...... 0.25 6/16/10 Corn, field, forage ...... 0.1 None specified in this paragraph is to be de- Corn, field, grain ...... 0.05 None termined by measuring only the sum of Corn, field, stover ...... 0.05 None chloroneb, 1,4-dichloro-2,5- Corn, pop, grain ...... 0.05 None dimethoxybenzene, and its metabolite Corn, pop, stover ...... 0.05 None Corn, sweet, forage ...... 0.5 6/16/10 2,5-dichloro-4-methoxyphenol (free and Corn, sweet, kernel plus cob with conjugated), calculated as the stoichio- husks removed ...... 0.25 6/16/10

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Expiration/ Parts per Commodity Parts per Revocation Commodity million million Date Sorghum, grain, forage ...... 10.0 Corn, sweet, stover ...... 0.5 6/16/10 Sorghum, grain, grain ...... 5 .0 Pineapple ...... 0.05 None Sorghum, grain, stover ...... 10 .0 Sugarcane, cane ...... 0.05 None Spearmint, tops ...... 50 .0 Tea, dried ...... 10 .0 (b) Section 18 emergency exemptions. Walnut ...... 0 .1 [Reserved] (c) Tolerances with regional registra- (b) Section 18 emergency exemptions. tions. [Reserved] [Reserved] (d) Indirect or inadvertent residues. (c) Tolerances with regional registra- [Reserved] tions. Tolerances with regional registration, as defined in § 180.1(l), are es- [43 FR 29121, July 6, 1978, as amended at 48 tablished for residues of propargite in FR 13175, Mar. 30, 1983; 48 FR 21132, May 11, or on the following raw agricultural 1983; 52 FR 33237, Sept. 2, 1987; 63 FR 57075, commodities: Oct. 26, 1998; 73 FR 54961, Sept. 24, 2008; 74 FR 47456, Sept. 16, 2009] Parts per Commodity million § 180.259 Propargite; tolerances for residues. Corn, sweet, kernel plus cob with husks removed ...... 0 .1 (a) General. Tolerances are established for residues of the pesticide (d) Indirect or inadvertent residues. propargite (2-(p-tert-butylphenoxy) [Reserved] cyclohexyl 2-propynyl sulfite) in or on [65 FR 33710, May 24, 2000, as amended at 72 the following food commodities. FR 41930, Aug. 1, 2007; 73 FR 54961, Sept. 24, Parts per 2008; 76 FR 34885, June 15, 2011] Commodity million § 180.261 Phosmet; tolerances for resi- Almond ...... 0.1 dues. Almond, hulls ...... 55 .0 Bean, dry, seed ...... 0 .2 (a) General. Tolerances are estab- Cattle, fat ...... 0.1 lished for residues of the insecticide Cattle, meat ...... 0 .1 Cattle, meat byproducts ...... 0.1 phosmet, N-(mercaptomethyl) phthal- Citrus, oil ...... 30.0 imide S-(O,O-dimethyl Corn, field, forage ...... 10 .0 phosphorodithioate), including its me- Corn, field, grain ...... 0 .1 tabolites and degradates, in or on the Corn, field, stover ...... 10 .0 Corn, pop, grain ...... 0.1 commodities in the following table. Corn, pop, stover ...... 10.0 Compliance with the tolerance levels Corn, sweet, forage ...... 10 .0 specified in this paragraph is to be de- Corn, sweet, stover ...... 10.0 Cotton, undelinted seed ...... 0 .1 termined by measuring only the sum of Egg ...... 0 .1 phosmet, N-(mercaptomethyl) phthal- Goat, fat ...... 0 .1 imide S-(O,O-dimethyl Goat, meat ...... 0.1 Goat, meat byproducts ...... 0 .1 phosphorodithioate), and its oxygen Grain, aspirated fractions ...... 0 .4 analog, N-(mercaptomethyl) phthal- Grape ...... 10 .0 imide S-(O,O-dimethyl Grapefruit ...... 5 .0 Hog, fat ...... 0 .1 phosphorothioate, calculated as the Hog, meat ...... 0 .1 stoichiometric equivalent of phosmet, Hog, meat byproducts ...... 0 .1 in or on the commodity. Hop, dried cones ...... 100 .0 Horse, fat ...... 0 .1 Parts per Horse, meat ...... 0 .1 Commodity million Horse, meat byproducts ...... 0 .1 Lemon ...... 5.0 Alfalfa, forage ...... 20 Milk, fat (0.08 ppm in milk) ...... 2 .0 Alfalfa, hay ...... 40 Nectarine ...... 4 .0 Almond, hulls ...... 10 Orange ...... 10 .0 Apple ...... 10 Peanut ...... 0 .1 Apricot ...... 5 Peppermint, tops ...... 50 .0 Blueberry ...... 10 Poultry, fat ...... 0.1 Cattle, fat ...... 0.2 Potato ...... 0 .1 Cattle, meat ...... 0 .1 Sheep, fat ...... 0 .1 Cattle, meat byproducts ...... 0.1 Sheep, meat ...... 0.1 Cherry ...... 10 Sheep, meat byproducts ...... 0 .1 Cranberry ...... 10

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Commodity Parts per § 180.262 Ethoprop; tolerances for resi- million dues. Fruit, citrus, group 10 ...... 5 (a) General. Tolerances are estab- Goat, fat ...... 0 .1 Goat, meat ...... 0.1 lished for residues of the nematocide Goat, meat byproducts ...... 0 .1 and insecticide ethoprop, O-ethyl S,S- Grape ...... 10 dipropyl phosphorodithioate, including Hog, fat ...... 0 .2 Hog, meat ...... 0 .04 its metabolites and degradates, in or Hog, meat byproducts ...... 0 .04 on the commodities in the following Horse, fat ...... 0 .1 Horse, meat ...... 0 .1 table. Compliance with the tolerance Horse, meat byproducts ...... 0 .1 levels specified in this paragraph is to Kiwifruit ...... 25 be determined by measuring only Milk ...... 0.1 Nectarine ...... 5 ethoprop, O-ethyl S,S-dipropyl Nut, tree, group 14 ...... 0 .1 phosphorodithioate, in or on the com- Pea, dry, seed ...... 0 .5 Pea, field, hay ...... 20 modity. Pea, field, vines ...... 10 Pea, succulent ...... 1 Commodity Parts per Peach ...... 10 million Pear ...... 10 Plum, prune, fresh ...... 5 Banana ...... 0.02 Potato ...... 0 .1 Bean, lima ...... 0 .02 Sheep, fat ...... 0 .1 Bean, snap, succulent ...... 0 .02 Sheep, meat ...... 0.1 Cabbage ...... 0 .02 Sheep, meat byproducts ...... 0 .1 Corn, field, forage ...... 0 .02 Sweet potato, roots ...... 12 Corn, field, grain ...... 0 .02 Corn, field, stover ...... 0 .02 (b) Section 18 emergency exemptions. Corn, sweet, forage ...... 0 .02 [Reserved] Corn, sweet, kernel plus cob with husks re- (c) Tolerances with regional registra- moved ...... 0 .02 tions. Tolerances with regional reg- Corn, sweet, stover ...... 0 .02 istration are established for residues of Cucumber ...... 0 .02 Hop, dried cones ...... 0 .02 the insecticide phosmet, N- Peppermint, tops ...... 0 .02 (mercaptomethyl) phthalimide S-(O,O- Pineapple1 ...... 0 .02 dimethyl phosphorodithioate), includ- Potato ...... 0 .02 ing its metabolites and degradates, in Spearmint, tops ...... 0 .02 or on the commodities in the following Sugarcane, cane ...... 0.02 table. Compliance with the tolerance Sweet potato, roots ...... 0 .02 levels specified in this paragraph is to 1 There are no U.S. registrations as of July 23, 2009, except for existing stocks bearing old labeling whose sale, distribu- be determined by measuring only the tion, and use is allowed, provided it is consistent with the sum of phosmet, N-(mercaptomethyl) terms of the cancellation order of July 9, 2009; i.e., the EPA will allow the technical registrant to continue to sell and dis- phthalimide S-(O,O-dimethyl tribute existing stocks of the amended registered product phosphorodithioate), and its oxygen bearing old labeling for use on pineapple for 18 months (until January 9, 2011) and persons other than the registrant may analog, N-(mercaptomethyl) phthal- continue to sell and/or use existing stocks of product bearing imide S-(O,O-dimethyl the old labeling until such stocks are exhausted, provided that such use is consistent with the terms of the previously ap- phosphorothioate, calculated as the proved labeling on, or that accompanied, the modified stoichiometric equivalent of phosmet, product. in or on the commodity. (b) Section 18 emergency exemptions. [Reserved] Commodity Parts per million (c) Tolerances with regional registra- Crabapple ...... 20 tions. [Reserved] Pistachio ...... 0.1 (d) Indirect or inadvertent residues. [Reserved] (d) Indirect or inadvertent residues. [Reserved] [47 FR 53004, Nov. 24, 1982, as amended at 48 FR 51485, Nov. 9, 1983; 52 FR 33237, Sept. 2, [43 FR 46538, Oct. 10, 1978, as amended at 45 1987; 53 FR 30053, Aug. 10, 1988; 63 FR 57075, FR 8981, Feb. 11, 1980; 48 FR 37213, Aug. 17, Oct. 26, 1998; 64 FR 39078, July 21, 1999; 66 FR 1983; 52 FR 48539, Dec. 23, 1987; 53 FR 657, Jan. 38955, July 26, 2001; 67 FR 49616, July 31, 2002; 11, 1988; 53 FR 39090, Oct. 5, 1988; 63 FR 57075, 73 FR 53731, Sept. 17, 2008; 73 FR 54961, Sept. Oct. 26, 1998; 67 FR 49616, July 31, 2002; 74 FR 24, 2008; 74 FR 46373, Sept. 9, 2009; 75 FR 60242, 46698, Sept. 11, 2009; 75 FR 60242, Sept. 29, 2010] Sept. 29, 2010]

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§ 180.263 Phosalone; tolerances for res- Commodity Parts per idues. million (a) General. Tolerances are estab- Sorghum, grain, stover ...... 0 .5 lished for residues of the insecticide Soybean ...... 0.02 phosalone, S-(6-chloro-3- Sugarcane, cane ...... 0.02 Sweet potato, roots ...... 0 .1 (mercaptomethyl)-2-benzoxazolinone) O,O-diethyl phosphorodithioate, in or (b) Section 18 emergency exemptions. on the following food commodities: [Reserved] (c) Tolerances with regional registra- Parts per Expiration/ Commodity Revocation tions. [Reserved] million Date (d) Indirect or inadvertent residues. Apple1 ...... 10.0 9/30/13 [Reserved] Cherry1 ...... 15.0 9/30/13 Grape1 ...... 10.0 9/30/13 [65 FR 33710, May 24, 2000, as amended at 69 Peach1 ...... 15.0 9/30/13 FR 6567, Feb. 11, 2004; 73 FR 54961, Sept. 24, 1 Pear ...... 10.0 9/30/13 2008] Plum, prune, fresh1 ...... 15.0 9/30/13 1There are no U.S. registrations since 1992. EFFECTIVE DATE NOTE: At 81 FR 34905, June 1, 2016, § 180.269 was amended by remove the (b) Section 18 emergency exemptions. entries for ‘‘Sorghum, grain, bran,’’ ‘‘Sor- [Reserved] ghum, grain, grain,’’ and ‘‘Sorghum, grain, (c) Tolerances with regional registra- stover,’’ from the table in paragraph (a), ef- tions. [Reserved] fective Nov. 28, 2016. (d) Indirect or inadvertent residues. [Reserved] § 180.272 Tribuphos; tolerances for residues. [74 FR 46698, Sept. 11, 2009] (a) General. Tolerances are estab- EFFECTIVE DATE NOTE: At 81 FR 34905, June lished for residues of the defoliant 1, 2016, § 180.263 was removed, effective Nov. tribuphos (S,S,S-tributyl 28, 2016. phosphorotrithioate) in or on food com- § 180.269 Aldicarb; tolerances for resi- modities as follows: dues. Parts per (a) General. Tolerances are estab- Commodity million lished for combined residues of the in- Cattle, fat ...... 0.15 secticide and nematocide aldicarb (2- Cattle, meat ...... 0 .02 methyl-2-(methylthio)propionaldehyde Cattle, meat byproducts ...... 0.02 O-(methylcarbamoyl) oxime and its Cotton, gin byproducts ...... 40 .0 cholinesterase-inhibiting metabolites Cotton, undelinted seed ...... 4 .0 2-methyl 2-(methylsulfinyl) Goat, fat ...... 0 .15 propionaldehyde O-(methylcarbamoyl) Goat, meat ...... 0.02 Goat, meat byproducts ...... 0 .02 oxime and 2-methyl-2-(methylsulfonyl) Hog, fat ...... 0 .15 propionaldehyde O-(methylcarbamoyl) Hog, meat ...... 0 .02 oxime in or on the following food com- Hog, meat byproducts ...... 0 .02 modities: Horse, fat ...... 0 .15 Horse, meat ...... 0 .02 Horse, meat byproducts ...... 0 .02 Commodity Parts per million Milk ...... 0.01 Sheep, fat ...... 0 .15 Bean, dry, seed ...... 0 .1 Sheep, meat ...... 0.02 Beet, sugar, roots ...... 0 .05 Sheep, meat byproducts ...... 0 .02 Beet, sugar, tops ...... 1 Citrus, dried pulp ...... 0 .6 Coffee, bean, green ...... 0 .1 (b) Section 18 emergency exemptions. Cotton, undelinted seed ...... 0 .1 [Reserved] Cotton, hulls ...... 0 .3 Grapefruit ...... 0 .3 (c) Tolerances with regional registra- Lemon ...... 0.3 tions. [Reserved] Lime ...... 0.3 (d) Indirect or inadvertent residues. Orange, sweet ...... 0 .3 Peanut ...... 0 .05 [Reserved] Pecan ...... 0 .5 Potato ...... 1 [65 FR 33698, May 24, 2000, as amended at 67 Sorghum, grain, bran ...... 0 .5 FR 49616, July 31, 2002; 72 FR 53460, Sept. 19, Sorghum, grain, grain ...... 0 .2 2007]

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§ 180.274 Propanil; tolerances for resi- Commodity Parts per dues. million (a) General. Tolerances are estab- Brassica, head and stem, subgroup 5A ...... 5 .0 lished for the combined residues of the Carrot, roots ...... 1 ′ ′ Celery ...... 15 herbicide propanil (3 , 4 - Cherry, sweet ...... 0 .5 dichloropropionanilide) and its me- Cherry, tart ...... 0 .5 tabolites convertible to 3, 4- Cocoa bean, dried bean ...... 0 .05 dichloroaniline (3, 4-DCA) in or on the Coffee, bean, green ...... 0 .20 Corn, sweet, kernel plus cob with husks re- following food commodities: moved ...... 1 Cranberry ...... 5 .0 Commodity Parts per Ginseng ...... 4 .0 million Horseradish ...... 4.0 Lentil ...... 0.10 Cattle, fat ...... 0.10 Lychee ...... 15 Cattle, meat ...... 0 .05 Mango ...... 1.0 Cattle, meat byproducts ...... 1.0 Crayfish ...... 0.05 Mushroom ...... 1 .0 Egg ...... 0 .30 Nectarine ...... 0 .5 Goat, fat ...... 0 .10 Okra ...... 6.0 Goat, meat ...... 0.05 Onion, bulb ...... 0 .5 Goat, meat byproducts ...... 1 .0 Onion, green ...... 5 Hog, fat ...... 0 .10 Papaya ...... 15 Hog, meat ...... 0 .05 Parsnip, roots ...... 1 Hog, meat byproducts ...... 1 .0 Passionfruit ...... 3 Horse, fat ...... 0 .10 Pea, edible podded ...... 5 Horse, meat ...... 0 .05 Peach ...... 0 .5 Horse, meat byproducts ...... 1 .0 Peanut ...... 0 .3 Milk ...... 0.05 Pistachio ...... 0.2 Poultry, fat ...... 0.05 Plum ...... 0 .2 Poultry, meat ...... 0 .10 Plum, prune ...... 0 .2 Poultry, meat byproducts ...... 0.50 Potato ...... 0 .1 Rice, bran ...... 40 Rhubarb ...... 4 .0 Rice, grain ...... 10 Soybean ...... 0.2 Rice, hulls ...... 30 Starfruit ...... 3 .0 Sheep, fat ...... 0 .10 Tomato ...... 5 Sheep, meat ...... 0.05 Vegetable, cucurbit, group 9 ...... 5.0 Sheep, meat byproducts ...... 1 .0 Vegetable, fruiting, group 8, except tomato ...... 6 .0 Yam, true ...... 0 .10 (b) Section 18 emergency exemptions. [Reserved] (2) Tolerances are established for the (c) Tolerances with regional registra- metabolite 4-hydroxy-2,5,6- tions. [Reserved] trichloroisophthalonitrile in or on the (d) Indirect or inadvertent residues. following food commodities. [Reserved] Commodity Parts per [63 FR 34827, June 26, 1998, as amended at 72 million FR 28888, May 23, 2007; 80 FR 72598, Nov. 20, Cattle, fat ...... 0.1 2015] Cattle, kidney ...... 0 .5 Cattle, meat byproducts, except kidney ...... 0.05 § 180.275 Chlorothalonil; tolerances for Cattle, meat ...... 0 .03 residues. Goat, fat ...... 0 .1 Goat, kidney ...... 0 .5 (a) General. (1) Tolerances are estab- Goat, meat byproducts, except kidney ...... 0 .05 lished for the fungicide chlorothalonil Goat, meat ...... 0.03 (tetrachloroisophthalonitrile) and its Hog, fat ...... 0 .1 metabolite 4-hydroxy-2,5,6- Hog, kidney ...... 0.5 Hog, meat byproducts, except kidney ...... 0 .05 trichloroisophthalonitrile in or on the Hog, meat ...... 0 .03 following food commodities. Horse, fat ...... 0 .1 Horse, kidney ...... 0 .5 Horse, meat byproducts, except kidney ...... 0 .05 Commodity Parts per million Horse, meat ...... 0 .03 Milk ...... 0.1 Almond ...... 0.05 Sheep, fat ...... 0 .1 Almond, hulls ...... 1 .0 Sheep, kidney ...... 0.5 Apricot ...... 0 .5 Sheep, meat byproducts, except kidney ...... 0 .05 Asparagus ...... 0.1 Sheep, meat ...... 0.03 Banana (NMT 0.05 ppm in edible pulp) ...... 0 .5 Bean, dry, seed ...... 0 .1 Bean, snap, succulent ...... 5 (b) Section 18 emergency exemptions. Blueberry ...... 1 .0 [Reserved]

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(c) Tolerances with regional registra- § 180.278 Phenmedipham; tolerances tions. Tolerances with regional reg- for residues. istration, as defined in § 180.1(l), are es- (a) General. Tolerances are estab- tablished for the combined residues of lished for the combined residues of the chlorothalonil and its metabolite in or herbicide phenmedipham (3- on the following raw agricultural com- methoxycarbonylaminophenyl-3′- modities: methylcarbanilate) in or on the fol- Parts per lowing food commodities: Commodity million Commodity Parts per Hazelnut ...... 0 .1 million Peppermint, tops ...... 2 Beet, garden, roots ...... 0 .2 Persimmon ...... 1 .5 Beet, garden, tops ...... 0 .2 Spearmint, tops ...... 2 Beet, sugar, dried pulp ...... 0 .5 Beet, sugar, molasses ...... 0 .2 (d) Indirect or inadvertent residues. Beet, sugar, roots ...... 0 .1 Beet, sugar, tops ...... 0.1 [Reserved] Spinach ...... 4 .0 [42 FR 56114, Oct. 21, 1977] (b) Section 18 emergency exemptions. EDITORIAL NOTE: For FEDERAL REGISTER ci- [Reserved] tations affecting § 180.275, see the List of CFR (c) Tolerances with regional registra- Sections Affected, which appears in the Finding Aids section of the printed volume tions. [Reserved] and at www.fdsys.gov. (d) Indirect or inadvertent residues. [Reserved] § 180.276 Formetanate hydrochloride; [72 FR 28888, May 23, 2007] tolerances for residues. (a) General. Tolerances are estab- § 180.284 Zinc phosphide; tolerances lished for residues of the insecticide for residues. formetanate hydrochloride, including (a) General. Tolerances are estab- its metabolites and degradates, in or lished for residues of the phosphine re- on the commodities in the table in this sulting from the use of the rodenticide paragraph. Compliance with the toler- zinc phosphide in or on the raw agricul- ance levels specified in this paragraph tural commodities as follows: is to be determined by measuring only Parts per formetanate hydrochloride, N,N-di- Commodity million methyl-N’-[3-[(methylamino)carbonyl] oxy]phenyl]methanimidamide hydro- Alfalfa, forage ...... 0.2 Alfalfa, hay ...... 0.2 chloride, in or on the commodity. Barley, grain ...... 0 .05 Barley, hay ...... 0 .2 Parts per Expiration/ Barley, straw ...... 0 .2 Commodity million revocation Bean, dry, seed ...... 0 .05 date Beet, sugar, roots ...... 0 .05 Beet, sugar, tops ...... 0.2 Apple ...... 0.50 12/31/13 Grape ...... 0 .01 Apple, wet pomace ...... 1.5 12/31/13 Grass, rangeland, forage ...... 0 .1 Grapefruit ...... 1.5 None Grass, rangeland, hay ...... 0 .1 Lemon ...... 0.60 None Potato ...... 0 .05 Lime ...... 0.03 None Sugarcane, cane ...... 0.01 Nectarine ...... 0.40 None Timothy, hay ...... 0 .5 Orange ...... 1.5 None Timothy, forage ...... 0.5 Peach ...... 0.40 12/31/13 Wheat, forage ...... 0 .05 Pear ...... 0.50 12/31/13 Wheat, grain ...... 0 .05 Wheat, hay ...... 0 .05 Tangelo ...... 0.03 None Wheat, straw ...... 0 .05 Tangerine ...... 0.03 None (b) (b) Section 18 emergency exemptions. Section 18 emergency exemptions. [Reserved] [Reserved] (c) Tolerances with regional registra- (c) Tolerances with regional registrations. Tolerances with regional reg- tions. [Reserved] istration, as defined in § 180.1(l), are es- (d) Indirect or inadvertent residues. tablished for residues of phosphine re- [Reserved] sulting from the use of the rodenticide [77 FR 40815, July 11, 2012] zinc phosphide in or on the following

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raw agricultural commodities as fol- (d) Indirect or inadvertent residues. lows: [Reserved]

Parts per [44 FR 70145, Dec. 6, 1979, as amended at 51 Commodity million FR 16846, May 7, 1986; 52 FR 5767, Feb. 26, 1987; 57 FR 53568, Nov. 12, 1992; 58 FR 14316, Artichoke, globe ...... 0.01 Mar. 17, 1993; 60 FR 12704, Mar. 8, 1995; 67 FR Beet, sugar, roots ...... 0 .04 49616, July 31, 2002; 72 FR 53454, Sept. 19, 2007; Beet, sugar, tops ...... 0.02 74 FR 47456, Sept. 16, 2009; 78 FR 17133, Mar. 20, 2013; 80 FR 72598, Nov. 20, 2015] (d) Indirect or inadvertent residues. [Reserved] § 180.288 2-(Thiocyanomethyl- thio)benzothiazole; tolerances for [63 FR 45182, Aug. 25, 1998, as amended at 63 residues. FR 67799, Dec. 9, 1998; 64 FR 40772, July 28, (a) General. Tolerances are estab- 1999; 64 FR 61791, Nov. 15, 1999; 65 FR 8874, lished for residues of the fungicide 2- Feb. 23, 2000; 65 FR 49941, Aug. 16, 2000; 65 FR 62634, Oct. 19, 2000; 66 FR 64773, Dec. 14, 2001; (thiocyanomethylthio)benzothiazole in 68 FR 2247, Jan. 16, 2003; 68 FR 56195, Sept. 30, or on the following food commodities: 2003; 70 FR 7046, Feb. 10, 2005; 74 FR 46373, Parts per Sept. 9, 2009; 76 FR 34885, June 15, 2011] Commodity million

Barley, grain ...... 0 .1(N) § 180.287 Amitraz; tolerances for resi- Barley, straw ...... 0 .1(N) dues. Beet, sugar, roots ...... 0 .1(N) Beet, sugar, tops ...... 0.1(N) (a) General. Tolerances are estab- Corn, field, forage ...... 0 .1(N) lished for residues of the insecticide Corn, field, grain ...... 0 .1 amitraz (N’-[2,4-dimethylphenyl]-N- Corn, field, stover ...... 0 .1 Corn, pop, grain ...... 0.1 [[(2,4-dimethylphenyl)imino]methyl]]- Corn, pop, stover ...... 0.1 N-methylmethanimidamide), including Cotton, forage ...... 0.1(N) its metabolites and degradates, in or Cotton, undelinted seed ...... 0 .1(N) Oat, forage ...... 0 .1(N) on the commodities in the following Oat, grain ...... 0 .1(N) table. Compliance with the tolerance Oat, hay ...... 0.1(N) levels specified is to be determined by Oat, straw ...... 0.1(N) Rice, grain ...... 0 .1(N) measuring amitraz residues convertible Safflower, seed ...... 0 .1(N) to 2,4-dimethylaniline, expressed as the Sorghum, grain, forage ...... 0.1(N) Sorghum, grain, grain ...... 0 .1(N) stoichiometric equivalent of amitraz, Sorghum, grain, stover ...... 0 .1(N) in or on the following raw agricultural Wheat, forage ...... 0 .1(N) commodities: Wheat, grain ...... 0 .1(N) Wheat, hay ...... 0 .1(N) Wheat, straw ...... 0 .1(N) Parts per Commodity million (b) Section 18 emergency exemptions. Cattle, fat ...... 0.1 [Reserved] Cattle, meat ...... 0 .02 (c) Tolerances with regional registra- Cattle, meat byproducts ...... 0.2 Hog, fat ...... 0 .1 tions. [Reserved] Hog, kidney ...... 0.1 (d) Indirect or inadvertent residues. Hog, liver ...... 0 .1 [Reserved] Hog, meat ...... 0 .05 [68 FR 39440, July 1, 2003, as amended at 74 Hog, meat byproducts ...... 0 .3 Honey ...... 0.2 FR 46374, Sept. 9, 2009; 80 FR 72598, Nov. 20, Honeycomb ...... 9 2015] Milk ...... 0.03 Milk, fat ...... 0 .2 § 180.289 Methanearsonic acid; tolerances for residues. (b) Section 18 emergency exemptions. (a) General. Tolerances are estab- [Reserved] lished for residues of the herbicide (c) Tolerances with regional registra- methanearsonic acid, including its me- tions. [Reserved] tabolites and degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only

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methanearsonic acid, from application (d) Indirect or inadvertent residues. of the disodium and monosodium salts [Reserved] of methanearsonic acid, calculated as [74 FR 47456, Sept. 16, 2009] the stoichiometric equivalent of As2O3, in or on the commodity. § 180.292 Picloram; tolerances for resi- Expiration/ dues. Commodity Parts per Revocation million Date (a) General. Tolerances are established for residues of the herbicide Cotton, undelinted seed ...... 0.7 None picloram, 4-amino-3,5,6- Cotton, hulls ...... 0.9 None Fruit, citrus ...... 0.35 12/31/12 trichloropicolinic acid, including its metabolites and degradates, in or on (b) Section 18 emergency exemptions. the commodities in the following table [Reserved] from its application in the acid form or (c) Tolerances with regional registra- in the form of its salts. Compliance tions. [Reserved] with the tolerance levels specified in (d) Indirect or inadvertent residues. this paragraph is to be determined by [Reserved] measuring only picloram, 4-amino- [63 FR 34828, June 26, 1998, as amended at 77 3,5,6-trichloropicolinic acid, in or on FR 59126, Sept. 26, 2012] the commodity.

Parts per § 180.291 Pentachloronitrobenzene; tol- Commodity million erance for residues. (a) General. Tolerances are estab- Barley, grain ...... 0 .5 Barley, pearled barley ...... 3 .0 lished for the combined residues of the Barley, straw ...... 1 .0 fungicide pentachloronitrobenzene Cattle, fat ...... 0.4 (PCNB) and its metabolites Cattle, meat ...... 0 .4 pentachloroaniline (PCA), and Cattle, meat byproducts ...... 15 pentachlorothioanisole (PCTA), in or Egg ...... 0 .05 on the following food commodities: Goat, fat ...... 0 .4 Goat, meat ...... 0.4 Parts per Goat, meat byproducts ...... 15 Commodity million Grain, aspirated fractions ...... 4 .0 Grass, forage ...... 400 Bean ...... 0 .1 Grass, hay ...... 225 Brassica, head and stem, subgroup 5A ...... 0 .1 Hog, fat ...... 0 .05 Cotton, undelinted seed ...... 0 .1 Hog, meat ...... 0 .05 Garlic, bulb ...... 0.1 Hog, meat byproducts ...... 0 .05 Peanut ...... 1 .0 Potato ...... 0 .1 Horse, fat ...... 0 .4 Soybean, forage ...... 0 .02 Horse, meat ...... 0 .4 Soybean, hay ...... 0 .02 Horse, meat byproducts ...... 15 Soybean, seed ...... 0 .02 Milk ...... 0.25 Vegetable, fruiting, group 8 ...... 0.1 Oat, forage ...... 1 .0 Oat, grain ...... 0 .5 (b) Section 18 emergency exemptions. Oat, groats/rolled oats ...... 3 .0 [Reserved] Oat, straw ...... 1.0 (c) Tolerances with regional registra- Poultry, fat ...... 0.05 Poultry, meat ...... 0 .05 tions. Tolerances with regional reg- Poultry, meat byproducts ...... 0.05 istrations, as defined in § 180.1(l), are Sheep, fat ...... 0 .4 established for the combined residues Sheep, meat ...... 0.4 of the fungicide Sheep, meat byproducts ...... 15 pentachloronitrobenzene (PCNB) and Wheat, bran ...... 3.0 Wheat, forage ...... 1 .0 its metabolites pentachloroaniline Wheat, germ ...... 3 .0 (PCA), and pentachlorothioanisole Wheat, grain ...... 0 .5 (PCTA), in or on the following food Wheat, middlings ...... 3 .0 commodities: Wheat, shorts ...... 3 .0 Wheat, straw ...... 1 .0 Commodity Parts per million (b) Section 18 emergency exemptions. Collards ...... 0.2 [Reserved] Kale ...... 0 .2 (c) Tolerances with regional registra- Mustard, greens ...... 0 .2 tions. [Reserved]

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(d) Indirect or inadvertent residues. Commodity Parts per [Reserved] million [41 FR 19221, May 11, 1976, as amended at 47 Almond, hulls ...... 15 .0 Animal feed, nongrass, group 18, forage ...... 4 .0 FR 53005, Nov. 24, 1982; 64 FR 425, Jan. 5, 1999; Animal feed, nongrass, group 18, hay ...... 10 64 FR 39082, July 21, 1999; 72 FR 41930, Aug. 1, Apple, wet pomace ...... 0 .15 2007; 75 FR 60243, Sept. 29, 2010] Beet, sugar, molasses ...... 1 .5 Brassica, head and stem subgroup 5A ...... 0 .1 § 180.293 Endothall; tolerances for res- Brassica, leafy, subgroup 5B ...... 2 .0 idues. Bushberry subgroup 13-07B ...... 0 .6 Caneberry subgroup 13-07A ...... 0.6 (a) General. (1) Tolerances are estab- Cattle, fat ...... 0.01 lished for the residues of endothall, in- Cattle, kidney ...... 0 .20 Cattle, liver ...... 0 .10 cluding its metabolites and degradates, Cattle, meat ...... 0 .03 in or on the commodities in the table, Corn, field, grain ...... 0 .07 below. Compliance with the tolerance Corn, pop, grain ...... 0.07 Corn, sweet, kernel plus cob with husks re- levels specified, below, is to be deter- moved ...... 0 .3 mined by measuring only endothall (7- Citrus, dried pulp ...... 0 .1 oxabicylco [2.2.1] heptanes-2,3- Egg ...... 0 .05 Feed commodities not otherwise listed ...... 10 .0 dicarboxylic acid) and its mono-methyl Food commodities not otherwise listed ...... 5 .0 ester. Fruit, citrus group 10 ...... 0.05 Fruit, pome, group 11 ...... 0.05 Fruit, stone, group 12 ...... 0 .3 Commodity Parts per million Goat, fat ...... 0 .005 Goat, kidney ...... 0 .15 Apple ...... 0.05 Goat, liver ...... 0.05 Apple, wet pomace ...... 0 .15 Goat, meat ...... 0.015 Cotton, undelinted seed ...... 0 .1 Grain, aspirated fractions ...... 35.0 Fish ...... 0 .1 Grain cereal, forage, fodder and straw, group Hop, dried cones ...... 0 .1 16 ...... 10 .0 Potato ...... 0 .1 Grain, cereal, group 15, except corn ...... 4 .0 Rice, grain ...... 0 .05 Grape ...... 1 .0 Grape, raisin ...... 5 .0 Grass, forage, fodder, and hay group 17, for- (2) An interim tolerance of 0.2 parts age ...... 3 .5 per million is established for residues Grass, forage, fodder, and hay group 17, hay .. 18 .0 of the herbicide endothall (7 - Herb and spice, group 19 ...... 5 .0 Hog, fat ...... 0 .005 oxabicyclo[2.2.1] heptane-2,3- Hog, kidney ...... 0.10 dicarboxylic acid) in water, potable Hog, liver ...... 0 .05 from use of its potassium, sodium, di- Hog, meat ...... 0 .01 Milk ...... 0.03 N, N-dimethylalkylamine, and mono-N- Nut, tree, group 14 ...... 0 .05 N,-dimethylalkylamine salts as Okra ...... 0.05 algicides or herbicides to control Pea and bean, dried shelled, subgroup 6C ...... 0 .2 aquatic plants in canals, lakes, ponds, Pea and bean, succulent shelled, subgroup 6B 2 .0 Peppermint, tops ...... 5 .0 and other potential sources of water, Pistachio ...... 0.05 potable. Poultry, fat ...... 0.015 (b) Section 18 emergency exemptions. Poultry, liver ...... 0 .05 Poultry, meat ...... 0 .015 [Reserved] Poultry, meat byproducts ...... 0.20 (c) Tolerances with regional registra- Rice, hulls ...... 8 .0 tions. [Reserved] Sheep, fat ...... 0 .005 Sheep, kidney ...... 0.15 (d) Indirect or inadvertent residues. Sheep, liver ...... 0.05 Tolerances are established for the indi- Sheep, meat ...... 0.015 rect or inadvertent combined residues Soybean, hulls ...... 0 .5 Soybean, seed ...... 0 .2 of the herbicide, endothall (7 - Spearmint, tops ...... 5 .0 oxabicyclo[2.2.1] heptane-2,3- Tomato, paste ...... 0 .1 dicarboxylic acid) in potable water Tomato, puree ...... 0 .1 Vegetable, bulb, group 3-07 ...... 0 .5 from use of its potassium, sodium, di- Vegetable, cucurbit, group 9 ...... 1.5 N, N -dimethylalkylamine, and mono- Vegetable, foliage of legume, group 7 ...... 4 .0 N-N, -dimethylalkylamine salts as Vegetable, fruiting, group 8 ...... 0.05 algicides or herbicides to control Vegetable, leafy, except brassica, group 4 ...... 2 .0 Vegetable, leaves of root and tuber, group 2 ... 3 .0 aquatic plants in canals, lakes, ponds, Vegetable, legume, edible, podded, subgroup and other potable water sources that 6A ...... 2 .0 may lead to endothall residues in or on Vegetable, root and tuber, group 1 ...... 1 .0 the following commodities: Wheat, milled byproducts ...... 5 .0

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[41 FR 23717, June 11, 1976, as amended at 51 Parts per Expiration/ FR 4498, Feb. 5, 1986; 62 FR 49931, Sept. 24, Commodity million revocation 1997; 63 FR 42249, Aug. 7, 1998; 67 FR 35048, date May 17, 2002; 71 FR 47106, Aug. 16, 2006; 71 FR Sorghum, grain, forage ...... 2.0 12/31/16 74816, Dec. 13, 2006; 72 FR 52018, Sept. 12, 2007; Sorghum, grain, grain ...... 0.2 12/31/16 74 FR 67097, Dec. 18, 2009; 78 FR 76566, Dec. 18, Sorghum, grain, stover ...... 2.0 12/31/16 2013; 80 FR 72598, Nov. 20, 2015] Sunflower, seed ...... 0.5 12/31/16 Tangerine ...... 6.0 12/31/16 § 180.297 N-1-Naphthyl phthalamic acid; tolerances for residues. (b) Section 18 emergency exemptions. (a) General. Tolerances are estab- [Reserved] lished for residues of the herbicide N-1- (c) Tolerances with regional registra- naphthyl phthalamic acid from appli- tions. Tolerances with regional reg- cation of its sodium salt in or on the istration, as defined in § 180.1(l), are es- following raw agricultural commod- tablished for residues of the insecticide ities: methidathion, including its metabolites and degradates, in or on the com- Parts per modities in the table in this paragraph. Commodity million Compliance with the tolerance levels Cantaloupe ...... 0 .1(N) specified in this paragraph is to be de- Cucumber ...... 0 .1(N) termined by measuring only Muskmelon ...... 0 .1(N) Watermelon ...... 0.1(N) methidathion, S-[(5-methoxy-2-oxo- 1,3,4-thiadiazol-3(2H)-yl)methyl] O,O- (b) Section 18 emergency exemptions. dimethyl phosphorodithioate, in or on [Reserved] the commodity. (c) Tolerances with regional registra- Expiration/ tions. [Reserved] Commodity Parts per revocation (d) Indirect or inadvertent residues. million date [Reserved] Kiwifruit ...... 0.1 12/31/16 [45 FR 32306, May 16, 1980, as amended at 63 Longan ...... 0.1 12/31/16 FR 57075, Oct. 26, 1998] Starfruit ...... 0.1 12/31/16 Sugar apple ...... 0.2 12/31/16 § 180.298 Methidathion; tolerances for residues. (d) Indirect or inadvertent residues. [Reserved] (a) General. Tolerances are established for residues of the insecticide [43 FR 44845, Sept. 29, 1978] methidathion, including its metabo- EDITORIAL NOTE: For FEDERAL REGISTER ci- lites and degradates, in or on the com- tations affecting § 180.298, see the List of CFR modities in the table in this paragraph. Sections Affected, which appears in the Compliance with the tolerance levels Finding Aids section of the printed volume specified in this paragraph is to be de- and at www.fdsys.gov. termined by measuring only methidathion, S-[(5-methoxy-2-oxo- § 180.299 Dicrotophos; tolerances for 1,3,4-thiadiazol-3(2H)-yl)methyl] O,O- residues. dimethyl phosphorodithioate, in or on (a) General. Tolerances are estab- the commodity. lished for residues of the insecticide dicrotophos, dimethyl phosphate of 3- Expiration/ Commodity Parts per revocation hydroxy-N,N-dimethyl-cis- million date crotonamide, in or on the following food commodities: Almond, hulls ...... 6.0 12/31/16 Artichoke, globe ...... 0.05 12/31/16 Citrus, oil ...... 420.0 12/31/16 Parts per Commodity million Cotton, undelinted seed ...... 0.2 12/31/16 Fruit, citrus, group 10, except tan- Cotton, gin byproducts ...... 2 .0 gerine ...... 4.0 12/31/16 Cotton, undelinted seed ...... 0 .2 Fruit, pome, group 11 ...... 0.05 12/31/16 Fruit, stone, group 12 ...... 0.05 12/31/16 Mango ...... 0.05 12/31/16 (b) Section 18 emergency exemptions. Nut, tree, group 14 ...... 0.05 12/31/16 [Reserved] Olive ...... 0.05 12/31/16 Safflower, seed ...... 0.5 12/31/16 (c) Tolerances with regional registra- Sorghum, forage, forage ...... 2.0 12/31/16 tions. [Reserved]

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(d) Indirect or inadvertent residues. (c) Tolerances with regional registra- [Reserved] tions. A tolerance with regional registration, as defined in § 180.1(m), of 0.1 [73 FR 52613, Sept. 10, 2008] part per million is established for resi- § 180.300 Ethephon; tolerances for residues of the plant regulator ethephon dues. [(2-chloroethyl)phosphonic acid] in or on the food commodity sugarcane. (a) General. Tolerances are estab- (d) Indirect or inadvertent residues. lished for residues of the plant regu- [Reserved] lator ethephon [(2-chloroethyl) phosphonic acid] in or on food commodities [65 FR 33710, May 24, 2000, as amended at 72 as follows: FR 53455, Sept. 19, 2007; 75 FR 56015, Sept. 15, 2010; 80 FR 72598, Nov. 20, 2015] Commodity Parts per million § 180.301 Carboxin; tolerances for resi- Apple ...... 5.0 dues. Apple, juice ...... 10 .0 (a) General. Tolerances are estab- Barley, bran ...... 5 .0 lished for the combined residues of the Barley, grain ...... 2 .0 Barley, straw ...... 10 .0 fungicide carboxin (5,6-dihydro-2-meth- Blackberry ...... 30 .0 yl-1,4-oxathiin-3-carboxanilide) and its Blueberry ...... 20 .0 metabolites determined as aniline and Cantaloupe ...... 2 .0 expressed as parent compound, in or on Cattle, fat ...... 0.02 Cattle, kidney ...... 1 .0 food commodities as follows: Cattle, meat ...... 0 .02 Cattle, meat byproducts, except kidney ...... 0.2 Commodity Parts per Cherry ...... 10.0 million Coffee, bean, green ...... 0 .5 Barley, grain ...... 0 .2 Cotton, gin byproducts ...... 180.0 Barley, straw ...... 0 .2 Cotton, undelinted seed ...... 6 .0 Bean, dry, seed ...... 0 .2 Egg ...... 0 .002 Bean, succulent ...... 0 .2 Goat, fat ...... 0 .02 Canola, seed ...... 0 .03 Goat, kidney ...... 1 .0 Cattle, fat ...... 0.05 Goat, meat ...... 0.02 Cattle, meat byproducts ...... 0.1 Goat, meat byproducts, except kidney ...... 0 .2 Cattle, meat ...... 0 .05 Grape ...... 2 .0 Corn, field, forage ...... 0 .2 Grape, raisin ...... 12.0 Corn, field, grain ...... 0 .2 Hazelnut ...... 0 .80 Corn, field, stover ...... 0 .2 Hog, fat ...... 0 .02 Corn, pop, grain ...... 0.2 Hog, kidney ...... 1.0 Corn, pop, stover ...... 0.2 Hog, meat ...... 0 .02 Corn, sweet, forage ...... 0 .2 Hog, meat byproducts, except kidney ...... 0 .2 Corn, sweet, kernel plus cob with husks re- Horse, fat ...... 0 .02 moved ...... 0 .2 Horse, kidney ...... 1 .0 Corn, sweet, stover ...... 0 .2 Horse, meat ...... 0 .02 Cotton, undelinted seed ...... 0 .2 Horse, meat byproducts, except kidney ...... 0 .2 Egg ...... 0 .05 Milk ...... 0.01 Goat, fat ...... 0 .05 Nut, macadamia ...... 0.5 Goat, meat byproducts ...... 0 .1 Pepper ...... 30.0 Goat, meat ...... 0.05 Pineapple ...... 2.0 Hog, fat ...... 0 .05 Poultry, fat ...... 0.02 Hog, meat byproducts ...... 0 .1 Poultry, liver ...... 0 .05 Hog, meat ...... 0 .05 Poultry, meat ...... 0 .01 Horse, fat ...... 0 .05 Poultry, meat byproducts, except liver ...... 0 .01 Horse, meat byproducts ...... 0 .1 Sheep, fat ...... 0 .02 Horse, meat ...... 0 .05 Sheep, kidney ...... 1.0 Milk ...... 0.05 Sheep, meat ...... 0.02 Oat, forage ...... 0 .5 Sheep, meat byproducts, except kidney ...... 0 .2 Oat, grain ...... 0 .2 Sugarcane, molasses ...... 1 .5 Oat, straw ...... 0.2 Tomato ...... 2.0 Onion, bulb ...... 0 .2 Walnut ...... 0 .5 Peanut ...... 0 .2 Wheat, bran ...... 5.0 Peanut, hay ...... 0.2 Wheat, germ ...... 5 .0 Poultry, fat ...... 0.1 Wheat, grain ...... 2 .0 Poultry, meat byproducts ...... 0.1 Wheat, middlings ...... 5 .0 Poultry, meat ...... 0 .1 Wheat, shorts ...... 5 .0 Rice, grain ...... 0 .2 Wheat, straw ...... 10 .0 Safflower, seed ...... 0 .2 Sheep, fat ...... 0 .05 Sheep, meat byproducts ...... 0 .1 (b) Section 18 emergency exemptions. Sheep, meat ...... 0.05 [Reserved] Soybean, seed ...... 0 .2

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(d) Indirect or inadvertent residues. Commodity Parts per million [Reserved] Wheat, forage ...... 0 .5 [73 FR 54961, Sept. 24, 2008, as amended at Wheat, grain ...... 0 .2 72598, Nov. 20, 2015] Wheat, straw ...... 0 .2 § 180.304 Oryzalin; tolerances for resi- (b) Section 18 emergency exemptions. dues. [Reserved] (c) Tolerances with regional registra- (a) General. Tolerances are estab- tions. [Reserved] lished for residues of the herbicide (d) Indirect or inadvertent residues. oryzalin, 3,5-dinitro-N4,N4- [Reserved] dipropylsulfanilamide, in or on the following raw agricultural commodities: [47 FR 55222, Dec. 8, 1982, as amended at 50 FR 81, Jan. 2, 1985; 62 FR 4915, Feb. 3, 1997; 63 Commodity Parts per FR 4586, Jan. 30, 1998; 64 FR 11801, Mar. 10, million 1999; 66 FR 9773, Feb. 12, 2001; 66 FR 64773, Almond, hulls ...... 0 .05 Dec. 14, 2001; 67 FR 40218, June 12, 2002; 67 FR Avocado ...... 0 .05 72853, Dec. 9, 2002; 71 FR 56383, Sept. 27, 2006; Berry group 13 ...... 0 .05 80 FR 72598, Nov. 20, 2015] Cranberry ...... 0 .05 Fig ...... 0 .05 Fruit, citrus, group 10 ...... 0 .05 § 180.303 Oxamyl; tolerances for resi- Fruit, pome, group 11 ...... 0.05 dues. Fruit, stone, group 12 ...... 0 .05 (a) General. Tolerances are estab- Grape ...... 0 .05 Kiwifruit ...... 0.05 lished for the combined residues of the Nut, tree, group 14 ...... 0 .05 insecticide oxamyl, methyl N,N-di- Olive ...... 0 .05 methyl-N-[(methylcarbamoyl)-oxy]-1- Pistachio ...... 0.05 Pomegranate ...... 0 .05 thiooxamimidate, and its oxime me- Strawberry ...... 0 .05 tabolite methyl N,N-dimethyl-N-hydroxy-1-thiooxamimidate calculated as (b) Section 18 emergency exemptions. oxamyl in or on the following food [Reserved] commodities: (c) Tolerances with regional registrations. Tolerances with regional reg- Parts per Commodity million istration, as defined in § 180.1(l), are established for residues of oryzalin, 3,5- Apple ...... 2 dinitro-N ,N -dipropylsulfanilamide, in Banana ...... 0.3 4 4 Cantaloupe ...... 2 .0 or on the following raw agricultural Carrot ...... 0 .1 commodities: Celery ...... 10 .0 Cotton, undelinted seed ...... 0 .2 Commodity Parts per Cucumber ...... 2 .0 million Eggplant ...... 2.0 Fruit, citrus, group 10 ...... 3 Guava ...... 0 .05 Garlic, bulb ...... 0.2 Papaya ...... 0 .05 Melon, honeydew ...... 2.0 Onion, bulb ...... 0 .2 (d) Indirect or inadvertent residues. Peanut ...... 0 .05 Peanut, hay ...... 2.0 [Reserved] Pear ...... 2 .0 [71 FR 54434, Sept. 15, 2006, as amended at 76 Peppermint, tops ...... 10 .0 Pepper, bell ...... 2 .0 FR 34885, June 15, 2011] Pepper, nonbell ...... 5 .0 Pineapple ...... 1 § 180.311 Cacodylic acid; tolerances for Pineapple, process residue ...... 2 .0 residues. Pumpkin ...... 2.0 Spearmint, tops ...... 10 .0 (a) General. A tolerance is established Squash, summer ...... 2 .0 for residues of the defoliant cacodylic Squash, winter ...... 2 .0 acid, dimethylarsinic acid, including Tomato ...... 2 Vegetable, tuberous and corm, subgroup 1C ..... 0.1 its metabolites and degradates, in or Watermelon ...... 2.0 on the commodity in the following table. Compliance with the tolerance (b) Section 18 emergency exemptions. level specified in this paragraph is to [Reserved] be determined by measuring only those (c) Tolerances with regional registra- cacodylic acid residues convertible to tions. [Reserved] As2O3, expressed as the stoichiometric

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equivalent of cacodylic acid, in or on (d) Indirect or inadvertent residues. the commodity. [Reserved] [72 FR 28888, May 23, 2007, as amended at 73 Parts per Expiration/ Commodity million Revocation FR 5109, Jan. 29, 2008; 73 FR 53738, Sept. 17, Date 2008; 74 FR 29963, June 24, 2009] Cotton, undelinted seed ...... 2.8 1/1/12 § 180.315 Methamidophos; tolerances (b) Section 18 emergency exemptions. for residues. [Reserved] (a) General. Tolerances are estab- (c) Tolerances with regional registra- lished for residues of methamidophos, tions. [Reserved] O,S-dimethyl phosphoramidothioate, (d) Indirect or inadvertent residues. including its metabolites and [Reserved] degradates, in or on the commodities [69 FR 6567, Feb. 11, 2004, as amended at 75 in the following table as a result of the FR 60243, Sept. 29, 2010] application of methamidophos. Compli- ance with the tolerance levels specified EFFECTIVE DATE NOTE: At 81 FR 34905, June 1, 2016, § 180.311 was removed, effective Nov. in this paragraph is to be determined 28, 2016. by measuring only methamidophos, O,S-dimethyl phosphoramidothioate, in § 180.314 Triallate; tolerances for resi- or on the commodity. dues. Expiration/ (a) General. Tolerances are estab- Commodity Parts per Revocation lished for residues of triallate, S-2,3,4- million Date trichloroallyl Broccoli1 ...... 1.0 12/31/12 diisopropylthiocarbamate and its me- Cabbage2 ...... 1.0 12/31/12 tabolite 2,3,3-trichloroprop-2- Cotton, undelinted seed ...... 0.1 12/31/13 enesulfonic acid (TCPSA) in or on the Potato ...... 0.1 12/31/13 following food commodity: 1 There are no U.S. registrations since 1989. 2 There are no U.S. registrations since 2001. Commodity Parts per million (b) Section 18 emergency exemptions. Bermudagrass, hay ...... 0.3 [Reserved] (c) Tolerances with regional registra- (b) Section 18 emergency exemptions. tions. A tolerance with a regional reg- [Reserved] istration is established for residues of (c) Tolerances with regional registra- methamidophos, O,S-dimethyl tions. Tolerances with a regional reg- phosphoramidothioate, including its istration, as defined in 180.1(l),are es- metabolites and degradates, in or on tablished for residues of the herbicide the commodity in the following table (S-2, 3, 4-trichloroallyl as a result of the application of diisopropylthiocarbamate) and its me- methamidophos. Compliance with the tabolite 2, 3, 3-trichloroprop-2- tolerance levels specified in this para- enesulfonic acid (TCPSA) in or on the graph is to be determined by measuring following food commodities: only methamidophos, O,S-dimethyl phosphoramidothioate, in or on the Parts per Commodity million commodity.

Barley, grain ...... 0 .05 Parts per Expiration/ Barley, hay ...... 1 .0 Commodity million Revocation Barley, straw ...... 0 .3 Date Beet, sugar, dried pulp ...... 0 .2 Beet, sugar, roots ...... 0 .1 Tomato ...... 2.0 12/31/13 Beet, sugar, tops ...... 0.5 Pea, dry ...... 0 .2 (d) Indirect or inadvertent residues. Pea, field, hay ...... 1.0 [Reserved] Pea, field, vines ...... 0 .5 Pea, succulent ...... 0 .2 [75 FR 60243, Sept. 29, 2010] Wheat, forage ...... 0 .5 Wheat, grain ...... 0 .05 EFFECTIVE DATE NOTE: At 81 FR 34905, June Wheat, hay ...... 1 .0 1, 2016, § 180.315 was removed, effective Nov. Wheat, straw ...... 1 .0 28, 2016.

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§ 180.316 Pyrazon; tolerances for resi- Compliance with the tolerance levels dues. specified in this paragraph is to be de- (a) General. Tolerances are estab- termined by measuring only those lished for combined residues of the her- propyzamide residues convertible to bicide pyrazon (5-amino-4-chloro-2- methyl 3,5-dichlorobenzoate, expressed phenyl-3(2H)-pyridazinone) and its meas the stoichiometric equivalent of tabolites (calculated as pyrazon) in or propyzamide, 3,5-dichloro-N-(1,1-di- on the following food commodities: methyl-2-propynyl)benzamide, in or on the commodity. Commodity Parts per million Parts per Commodity million Beet, garden, roots ...... 0 .9 Beet, garden, tops ...... 7 .0 Alfalfa, seed ...... 10 .0 Beet, sugar, molasses ...... 1 .5 Animal feed, nongrass, group 18 ...... 10 .0 Beet, sugar, roots ...... 0 .2 Apple ...... 0.1 Beet, sugar, tops ...... 3.0 Artichoke, globe ...... 0.01 Cattle, fat ...... 0.10 Blackberry ...... 0 .05 Cattle, liver ...... 0 .15 Blueberry ...... 0 .05 Cattle, meat ...... 0 .10 Boysenberry ...... 0 .05 Cattle, meat byproducts, except liver ...... 0 .10 Cattle, fat ...... 0.2 Goat, fat ...... 0 .10 Cattle, kidney ...... 0 .4 Goat, liver ...... 0.15 Cattle, liver ...... 0 .4 Goat, meat ...... 0.10 Cattle, meat ...... 0 .02 Goat, meat byproducts, except liver ...... 0 .10 Cattle, meat byproducts, except kidney and liver 0.02 Horse, fat ...... 0 .10 Egg ...... 0 .02 Horse, liver ...... 0 .15 Endive ...... 1.0 Horse, meat ...... 0 .10 Fruit, stone, group 12 ...... 0 .1 Horse, meat byproducts, except liver ...... 0 .10 Goat, fat ...... 0 .2 Milk ...... 0.02 Goat, kidney ...... 0 .4 Sheep, fat ...... 0 .10 Goat, liver ...... 0.4 Sheep, liver ...... 0.15 Goat, meat ...... 0.02 Sheep, meat ...... 0.10 Goat, meat byproducts, except kidney and liver 0 .02 Sheep, meat byproducts, except liver ...... 0 .10 Grape ...... 0 .1 Hog, fat ...... 0 .2 (b) Section 18 emergency exemptions. Hog, kidney ...... 0.4 [Reserved] Hog, liver ...... 0 .4 Hog, meat ...... 0 .02 (c) Tolerances with regional registra- Hog, meat byproducts, except kidney and liver .. 0 .02 tions. [Reserved] Horse, fat ...... 0 .2 (d) Indirect or inadvertent residues. Horse, kidney ...... 0 .4 Horse, liver ...... 0 .4 Tolerances are established for com- Horse, meat ...... 0 .02 bined residues of the herbicide pyrazon, Horse, meat byproducts, except kidney and liver 0 .02 5-amino-4-chloro-2-phenyl-3(2H)- Lettuce, head ...... 1.0 pyridazinone, and its metabolites (cal- Lettuce, leaf ...... 1 .0 Milk ...... 0.02 culated as pyrazon), in or on the fol- Pear ...... 0 .1 lowing food commodities: Poultry, fat ...... 0.02 Poultry, liver ...... 0 .2 Parts per Poultry, meat ...... 0 .02 Commodity million Poultry, meat byproducts, except liver ...... 0 .02 Radicchio ...... 2.0 Corn, field, forage ...... 0 .5 Raspberry ...... 0 .05 Corn, field, stover ...... 0 .5 Sheep, fat ...... 0 .2 Soybean, forage ...... 0 .5 Sheep, kidney ...... 0.4 Soybean, hay ...... 0 .5 Sheep, liver ...... 0.4 Wheat, forage ...... 0 .3 Sheep, meat ...... 0.02 Wheat, hay ...... 0 .2 Sheep, meat byproducts, except kidney and Wheat, straw ...... 0 .1 liver ...... 0 .02

[68 FR 39441, July 1, 2003, as amended at 73 (b) Section 18 emergency exemptions. FR 52614, Sept. 10, 2008] [Reserved] (c) Tolerances with regional registra- § 180.317 Propyzamide; tolerances for tions. Tolerances with regional reg- residues. istration, as defined in § 180.1(l), are es- (a) General. Tolerances are estab- tablished for residues of the herbicide lished for residues of the herbicide propyzamide, including its metabolites propyzamide, including its metabolites and degradates, in or on the commod- and degradates, in or on the commodities in the table in this paragraph. ities in the table in this paragraph. Compliance with the tolerance levels

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specified in this paragraph is to be de- § 180.318 4-(2-Methyl-4-chlorophenoxy) termined by measuring only those butyric acid; tolerance for residues. propyzamide residues convertible to (a) General. (1) A tolerance is estab- methyl 3,5-dichlorobenzoate, expressed lished for the herbicide 4-(2-methyl-4- as the stoichiometric equivalent of chlorophenoxy) butyric acid in or on propyzamide, 3,5-dichloro-N-(1,1-di- the following food commodity: methyl-2-propynyl)benzamide, in or on Parts per the commodity. Commodity million

Parts per Pea ...... 0 .1(N) Commodity million

Pea, field, seed ...... 0 .05 (2) Tolerances are established for the Rhubarb ...... 0 .1 combined residues, free and conjugated, of the herbicide MCPB, 4-(4- (d) Indirect or inadvertent residues. chloro-2-methylphenoxy)butanoic acid, Tolerances are established for indirect and its metabolite MCPA, (4-chloro-2- or inadvertent residues of the herbicide methylphenoxy)acetic acid, in or on propyzamide, including its metabolites the following food commodities: and degradates, in or on the commod- Parts per ities in the table in this paragraph. Commodity million Compliance with the tolerance levels Peppermint, tops ...... 0 .20 specified in this paragraph is to be de- Spearmint, tops ...... 0 .20 termined by measuring only those propyzamide residues convertible to (b) Section 18 emergency exemptions. methyl 3,5-dichlorobenzoate, expressed [Reserved] as the stoichiometric equivalent of (c) Tolerances with regional registra- propyzamide, 3,5-dichloro-N-(1,1-di- tions. [Reserved] methyl-2-propynyl)benzamide, in or on (d) Indirect or inadvertent residues. the commodity. [Reserved] [68 FR 39441, July 1, 2003, as amended at 73 Parts per Commodity million FR 66785, Nov. 12, 2008]

Grain, cereal, forage, group 16 ...... 0 .6 § 180.319 Interim tolerances. Grain, cereal, hay, group 16 ...... 0 .2 (a) General. While petitions for toler- Grain, cereal, straw, group 16 ...... 0 .3 ances for negligible residues are pending and until action is completed on [72 FR 52018, Sept. 12, 2007, as amended at 76 these petitions, interim tolerances are FR 23493, Apr. 27, 2011; 81 FR 1531, Jan. 13, established for residues of the listed 2016] pesticide chemicals in or on the following raw agricultural commodities:

Raw Expiration/ Substances Uses Tolerance in parts per million agricultural revocation commodity date

Endothall (7-oxabicyclo- Herbicide ...... 0.2 ...... Beet, sugar ...... None (2,2,1)heptane 2,3-dicarboxylic acid. Methyl parathion ...... Herbicide ...... 0.5 ...... Rye ...... 12/31/13

(b) Section 18 emergency exemptions. § 180.324 Bromoxynil; tolerances for [Reserved] residues. (c) Tolerances with regional registra- (a) General. (1) Tolerances are estab- tions. [Reserved] lished for residues of the herbicide (d) Indirect or inadvertent residues. bromoxynil, including its metabolites [Reserved] and degradates, in or on the commod- [77 FR 59126, Sept. 26, 2012, as amended at 79 ities in the table below. Compliance FR 27502, May 14, 2014]

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with the tolerance levels is to be deter- Commodity Parts per mined by measuring only bromoxynil, million 3,5-dibromo-4-hydroxybenzonitrile, re- Hog, meat ...... 0 .5 sulting from application of its octanoic Horse, fat ...... 1 and/or heptanoic acid ester, in or on Horse, meat byproducts ...... 3 .5 Horse, meat ...... 0 .5 the commodities. Milk ...... 0.4 Poultry, fat ...... 0.05 Commodity Parts per Poultry, meat byproducts ...... 0.3 million Poultry, meat ...... 0 .05 Sheep, fat ...... 1 Alfalfa, forage ...... 0.1 Sheep, meat byproducts ...... 3 .5 Alfalfa, hay ...... 0.5 Sheep, meat ...... 0.5 Barley, grain ...... 0 .05 Barley, hay ...... 9 .0 Barley, straw ...... 4 .0 (b) Section 18 emergency exemptions. Corn, field, forage ...... 0 .3 [Reserved] Corn, field, grain ...... 0 .05 (c) Tolerances with regional registra- Corn, field, stover ...... 0 .2 Corn, pop, grain ...... 0.05 tions. [Reserved] Corn, pop, stover ...... 0.2 (d) Indirect or inadvertent residues. Flax, seed ...... 0 .1 [Reserved] Garlic ...... 0 .1 Grain, aspirated fractions ...... 1 .2 [62 FR 33023, June 18, 1997, as amended at 63 Grass, forage ...... 18 FR 26480, May 13, 1998; 66 FR 47402, Sept. 12, Grass, hay ...... 5 .0 2001; 70 FR 7046, Feb. 10, 2005; 72 FR 35666, Oat, forage ...... 0 .3 June 29, 2007; 72 FR 41930, Aug. 1, 2007; 76 FR Oat, grain ...... 0 .05 31491, June 1, 2011] Oat, hay ...... 9.0 Oat, straw ...... 4.0 Onion, bulb ...... 0 .1 § 180.328 Napropamide; tolerances for Peppermint, hay ...... 0 .1 residues. Rye, forage ...... 1 .0 (a) General. Tolerances are estab- Rye, grain ...... 0.05 Rye, straw ...... 2 .0 lished for residues of the herbicide Sorghum, grain, forage ...... 0.8 napropamide, N,N-diethyl-2-(1- Sorghum, grain, grain ...... 0 .2 napthalenyloxy) propionamide, in or on Sorghum, grain, stover ...... 0 .2 Spearmint, hay ...... 0 .1 the following food commodities: Wheat, forage ...... 1 .0 Wheat, grain ...... 0 .05 Expiration/ Commodity Parts per revocation Wheat, hay ...... 4 .0 million date Wheat, straw ...... 2 .0 Almond, hulls ...... 0.1 None (2) Tolerances are established for res- Asparagus ...... 0.1 None Basil ...... 0.1 None idues of the herbicide bromoxynil, 3,5- Berry group 13 ...... 0.1 None dibromo-4-hydroxybenzonitrile, includ- Coffee, green bean ...... 0.1 None ing its metabolites and degradates, in Cranberry ...... 0.1 None Grape ...... 0.1 None or on the commodities in the table Kiwifruit ...... 0.1 None below. Compliance with the tolerance Marjoram ...... 0.1 None levels is to be determined by meas- Nut, tree, group 14 ...... 0.1 None uring only bromoxynil and its metabo- Peppermint, tops ...... 0.1 None Persimmon ...... 0.1 None lite, 3,5-dibromo-4-hydroxybenzoic acid Rhubarb ...... 0.1 None (DBHA), resulting from application of Rosemary ...... 0.1 None its octanoic and/or heptanoic acid Savory, summer ...... 0.1 None Savory, winter ...... 0.1 None ester, in or on the commodities. Spearmint, tops ...... 0.1 None Strawberry ...... 0.1 None Commodity Parts per Sweet potato, roots ...... 0.1 None million Vegetable, brassica, leafy, group 5 0.1 None Vegetable, fruiting, group 8 ...... 0.1 None Cattle, fat ...... 1 Cattle, meat byproducts ...... 3.5 Cattle, meat ...... 0 .5 (b) Section 18 emergency exemptions. Cotton, gin byproducts ...... 7 .0 [Reserved] Cotton, hulls ...... 5 .0 (c) Tolerances with regional registra- Cotton, undelinted seed ...... 1 .5 tions. [Reserved] Egg ...... 0 .05 Goat, fat ...... 1 (d) Indirect or inadvertent residues. Goat, meat byproducts ...... 3 .5 [Reserved] Goat, meat ...... 0.5 Hog, fat ...... 1 [73 FR 52614, Sept. 10, 2008, as amended at 76 Hog, meat byproducts ...... 3 .5 FR 34885, June 15, 2011]

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§ 180.330 S-(2-(Ethylsulfinyl)ethyl) O,O- Commodity Parts per dimethyl phosphorothioate; toler- million ances for residues. Hog, meat ...... 0 .01 (a) General. (1) Tolerances are estab- Hog, meat byproducts ...... 0 .01 Horse, fat ...... 0 .01 lished for the combined residues of the Horse, meat ...... 0 .01 insecticide oxydemeton-methyl (S-(2- Horse, meat byproducts ...... 0 .01 (ethylsulfinyl)ethyl) O,O-dimethyl Milk ...... 0.01 Poultry, fat ...... 0.01 phosphorothioate) and its metabolite Poultry, meat ...... 0 .01 oxydemeton-methyl sulfone in or on Poultry, meat byproducts ...... 0.01 the following food commodities: Sheep, fat ...... 0 .01 Sheep, meat ...... 0.01 Parts per Sheep, meat byproducts ...... 0 .01 Commodity million (b) Section 18 emergency exemptions. Alfalfa, forage ...... 5.0 Alfalfa, hay ...... 11.0 [Reserved] Bean, lima ...... 0 .2 (c) Tolerances with regional registra- Beet, sugar, roots ...... 0 .3 tions. Tolerances with regional reg- Beet, sugar, tops ...... 0.5 Broccoli ...... 1 .0 istrations, as defined in § 180.1(l), are Brussels sprouts ...... 1 .0 established for the combined residues Cabbage ...... 2 .0 of the insecticide oxydemeton-methyl Cauliflower ...... 1 .0 (S-(2-(ethylsulfinyl)-ethyl) O,O-di- Clover, forage ...... 5.0 Clover, hay ...... 10.0 methyl phosphorothioate) and its me- Corn, sweet, forage ...... 1 .0 tabolite oxydemeton-methyl sulfone in Corn, sweet, kernel plus cob with husks re- or on the following food commodities: moved ...... 0 .5 Corn, sweet, stover ...... 3 .0 Commodity Parts per million Cotton, undelinted seed ...... 0 .02 Cucumber ...... 1 .0 Broccoli raab ...... 2 .0 Eggplant ...... 1.0 Grapefruit ...... 1 .0 Hazelnut ...... 0 .05 (d) Indirect or inadvertent residues. Lemon ...... 1.0 [Reserved] Lettuce, head ...... 2.0 Melon ...... 0 .2 [72 FR 54578, Sept. 26, 2007] Onion, bulb ...... 0 .05 Orange ...... 1 .0 § 180.331 4-(2,4-Dichlorophenoxy) bu- Pepper ...... 0 .75 tyric acid; tolerances for residues. Peppermint, tops ...... 12 .5 Pumpkin ...... 0.2 (a) General. Tolerances are estab- Safflower, seed ...... 1 .0 lished for residues of the herbicide 4- Sorghum, forage, forage ...... 2 .0 (2,4-dichlorophenoxy) butyric acid (2,4- Sorghum, grain, forage ...... 2.0 Sorghum, grain, grain ...... 0 .75 DB), both free and conjugated, deter- Spearmint, tops ...... 12 .5 mined as the acid, in or on food com- Squash, summer ...... 1 .0 modities, as follows: Squash, winter ...... 0 .3 Strawberry ...... 2 .0 Parts per Walnut ...... 0 .05 Commodity million (2) Tolerances are established for the Alfalfa, forage ...... 0.7 Alfalfa, hay ...... 2.0 combined residues of the insecticide Cattle, meat byproducts ...... 0.05 oxydemeton-methyl (S-(2- Clover, forage ...... 0.2 (ethylsulfinyl)ethyl) O,O-dimethyl Clover, hay ...... 0.2 phosphorothioate) and its cholin- Goat, meat byproducts ...... 0 .05 Hog, meat byproducts ...... 0 .05 esterase-inhibiting metabolites in or Horse, meat byproducts ...... 0 .05 on the following food commodities: Peanut ...... 0 .2 Peppermint, tops ...... 0 .2 Sheep, meat byproducts ...... 0 .05 Commodity Parts per million Soybean, forage ...... 0 .7 Soybean, hay ...... 2 .0 Cattle, fat ...... 0.01 Soybean, seed ...... 0 .5 Cattle, meat ...... 0 .01 Spearmint, tops ...... 0 .2 Cattle, meat byproducts ...... 0.01 Trefoil, forage ...... 0 .7 Egg ...... 0 .01 Trefoil, hay ...... 2 .0 Goat, fat ...... 0 .01 Goat, meat ...... 0.01 Goat, meat byproducts ...... 0 .01 (b) Section 18 emergency exemptions. Hog, fat ...... 0 .01 [Reserved]

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(c) Tolerances with regional registra- Commodity Parts per tions. [Reserved] million (d) Indirect or inadvertent residues. Tomato ...... 0.1 [Reserved] Wheat, bran ...... 3.0 Wheat, forage ...... 2 .0 [73 FR 54961, Sept. 24, 2008, as amended at 74 Wheat, germ ...... 3 .0 FR 46374, Sept. 9, 2009] Wheat, grain ...... 0 .75 Wheat, hay ...... 7 .0 Wheat, middlings ...... 3 .0 § 180.332 Metribuzin; tolerances for Wheat, shorts ...... 3 .0 residues. Wheat, straw ...... 1 .0 (a) General. Tolerances are established for combined residues of the her- (b) Section 18 emergency exemptions. bicide metribuzin (4-amino-6-(1,1- [Reserved] dimethylethyl)-3-(methylthio)-;1,2,4- (c) Tolerances with regional registra- triazin-5(4H)-one) and its triazinone tions. [Reserved] metabolites in or on food commodities: (d) Indirect or inadvertent residues. [Reserved] Parts per Commodity million [42 FR 62913, Dec. 14, 1977, as amended at 43 FR 41396, Sept. 18, 1978; 44 FR 26744, May 7, Alfalfa, forage ...... 2.0 1979; 44 FR 45387, Aug. 2, 1979; 52 FR 23654, Alfalfa, hay ...... 7.0 June 24, 1987; 55 FR 26440, June 28, 1990; 62 FR Asparagus ...... 0.1 66024, 66025, Dec. 17, 1997; 65 FR 33698, May 24, Barley, grain ...... 0 .75 Barley, hay ...... 7 .0 2000; 66 FR 63198, Dec. 5, 2001; 67 FR 49617, Barley, pearled barley ...... 3 .0 July 31, 2002] Barley, straw ...... 1 .0 Carrot, roots ...... 0.3 § 180.337 Oxytetracycline; tolerances Cattle, fat ...... 0.7 for residues. Cattle, meat ...... 0 .7 Cattle, meat byproducts ...... 0.7 (a) General. Tolerances are estab- Corn, field, forage ...... 0 .1 lished for residues of the fungicide/ Corn, field, grain ...... 0 .05 Corn, field, stover ...... 0 .1 bactericide oxytetracycline, including Corn, pop, grain ...... 0.05 its metabolites and degradates, in or Corn, sweet, forage ...... 0 .1 on the commodities in the table in this Corn, sweet, kernel plus cob with husks re- paragraph. Compliance with the toler- moved ...... 0 .05 Corn, sweet, stover ...... 0 .1 ance levels specified in this paragraph Egg ...... 0 .01 is to be determined by measuring only Goat, fat ...... 0 .7 oxytetracycline, Goat, meat ...... 0.7 Goat, meat byproducts ...... 0 .7 (4S,4aR,5S,5aR,6S,12aS)-4- Grass, forage ...... 2 .0 (dimethylamino)-1,4,4a,5,5a,6,11,12a- Grass, hay ...... 7 .0 octahydro-3,5,6,10,12,12a-hexahydroxy- Hog, fat ...... 0 .7 6-methyl-1,11-dioxo-2- Hog, meat ...... 0 .7 Hog, meat byproducts ...... 0 .7 naphthacenecarboxamide, in or on the Horse, fat ...... 0 .7 commodity. Horse, meat ...... 0 .7 Horse, meat byproducts ...... 0 .7 Commodity Parts per Lentil ...... 0.05 million Milk ...... 0.05 Pea, dry, seed ...... 0 .05 Apple ...... 0.35 Pea, field, hay ...... 4.0 Peach ...... 0 .35 Pea, field, vines ...... 0 .5 Pear ...... 0 .35 Pea, succulent ...... 0 .1 Potato ...... 0 .6 (b) Section 18 emergency exemptions. Potato, chips ...... 3 .0 Potato, processed potato waste ...... 3 .0 [Reserved] Poultry, fat ...... 0.7 (c) Tolerances with regional registra- Poultry, meat ...... 0 .7 tions. [Reserved] Poultry, meat byproducts ...... 0.7 (d) Indirect or inadvertent residues. Sainfoin, forage ...... 2 .0 Sainfoin, hay ...... 7 .0 [Reserved] Sheep, fat ...... 0 .7 [76 FR 23493, Apr. 27, 2011] Sheep, meat ...... 0.7 Sheep, meat byproducts ...... 0 .7 Soybean, seed ...... 0 .3 § 180.339 MCPA; tolerances for resi- Soybean, forage ...... 4 .0 dues. Soybean, hay ...... 4 .0 Sugarcane, cane ...... 0.1 (a) General. (1) Tolerances are estab- Sugarcane, molasses ...... 2 .0 lished for residues of the herbicide

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MCPA ((4-chloro-2- (b) Section 18 emergency exemptions. methylphenoxy)acetic acid), both free [Reserved] and conjugated, resulting from the di- (c) Tolerances with regional registra- rect application of MCPA or its sodium tions. [Reserved] or dimethylamine salts, or its 2- (d) Indirect or inadvertent residues. ethylhexyl ester in or on the following [Reserved] food commodities: [72 FR 28888, May 23, 2007, as amended at 73 FR 5109, Jan. 29, 2008] Parts per Commodity million § 180.341 2,4-Dinitro-6-octylphenyl cro- Alfalfa, forage ...... 0.5 tonate and 2,6-dinitro-4-octylphenyl Alfalfa, hay ...... 2.0 crotonate; tolerances for residues. Barley, grain ...... 1 .0 Barley, hay ...... 40 (a) General. Tolerances are estab- Barley, straw ...... 25 lished for combined negligible residues Clover, forage ...... 0.5 of a fungicide and insecticide that is a Clover, hay ...... 2.0 Flax, seed ...... 0 .1 mixture of 2,4-dinitro-6-octylphenyl Grain, aspirated fractions ...... 3 .0 crotonate and 2,6-dinitro-4-octylphenyl Grass, forage ...... 300 crotonate in or on raw agricultural Grass, hay ...... 20 Lespedeza, forage ...... 0 .5 commodities as follows: Lespedeza, hay ...... 2.0 Parts per Oat, forage ...... 20 Commodity million Oat, grain ...... 1 .0 Oat, hay ...... 115 Apple 1 ...... 0.1 Oat, straw ...... 25 Grape 1 ...... 0 .1 Pea, dry ...... 0 .1 Pea, field, hay ...... 0.1 1 There are no U.S. registrations on apple and grape as of Pea, succulent ...... 0 .1 October 24, 2002. Pea, field, vines ...... 0 .1 (b) Section 18 emergency exemptions. Rye, forage ...... 20 Rye, grain ...... 1.0 [Reserved] Rye, straw ...... 25 (c) Tolerances with regional registra- Trefoil, forage ...... 0 .5 tions. [Reserved] Trefoil, hay ...... 2 .0 (d) Indirect or inadvertent residues. Vetch, forage ...... 0 .5 Vetch, hay ...... 2 .0 [Reserved] Wheat, forage ...... 20 [40 FR 29715, July 15, 1975, as amended at 63 Wheat, grain ...... 1 .0 Wheat, hay ...... 115 FR 57076, Oct. 26, 1998; 69 FR 43924, July 23, Wheat, straw ...... 25 2004]

(2) Tolerances are established for res- § 180.342 Chlorpyrifos; tolerances for idues of the herbicide MCPA ((4-chloro- residues. 2-methylphenoxy)acetic acid) resulting (a) General. (1) Tolerances are estab- from the direct application of MCPA or lished for residues of the pesticide its sodium or dimethylamine salts, or chlorpyrifos per se (O,O-diethyl-O- its 2-ethylhexyl ester in or on the fol- (3,5,6-trichloro-2-pyridyl) lowing food commodities: phosphorothioate) in or on the following food commodities: Commodity Parts per million Parts per Commodity million Cattle, fat ...... 0.1 Cattle, meat ...... 0 .1 Alfalfa, forage ...... 3.0 Cattle, meat byproducts ...... 0.1 Alfalfa, hay ...... 13 Goat, fat ...... 0 .1 Almond ...... 0.2 Goat, meat ...... 0.1 Almond, hulls ...... 12 Goat, meat byproducts ...... 0 .1 Apple ...... 0.01 Hog, fat ...... 0 .1 Apple, wet pomace ...... 0 .02 Hog, meat ...... 0 .1 Banana ...... 0.1 Hog, meat byproducts ...... 0 .1 Beet, sugar, dried pulp ...... 5 .0 Horse, fat ...... 0 .1 Beet, sugar, molasses ...... 15 Horse, meat ...... 0 .1 Beet, sugar, roots ...... 1 .0 Horse, meat byproducts ...... 0 .1 Beet, sugar, tops ...... 8.0 Milk ...... 0.1 Cattle, fat ...... 0.3 Sheep, fat ...... 0 .1 Cattle, meat ...... 0 .05 Sheep meat ...... 0 .1 Cattle, meat byproducts ...... 0.05 Sheep meat byproducts ...... 0 .1 Cherry, sweet ...... 1 .0 Cherry, tart ...... 1 .0

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ment in food handling establishments Commodity Parts per million where food and food products are held, Citrus, dried pulp ...... 5 .0 processed, prepared or served. Contami- Citrus, oil ...... 20 nation of food or food contact surfaces Corn, field, forage ...... 8 .0 shall be avoided. Food must be re- Corn, field, grain ...... 0 .05 Corn, field, refined oil ...... 0 .25 moved or covered during treatment. Corn, field, stover ...... 8 .0 (ii) Spray concentration for spot Corn, sweet, forage ...... 8 .0 treatment shall be limited to a max- Corn, sweet, kernel plus cob with husk removed 0.05 Corn, sweet, stover ...... 8 .0 imum of 0.5 percent of the active ingre- Cotton, undelinted seed ...... 0 .2 dient by weight. A course, low-pressure Cranberry ...... 1 .0 spray shall be used to avoid atomiza- Cucumber ...... 0 .05 tion or splashing of the spray. Egg ...... 0 .01 Fig ...... 0 .01 (iii) Paint-on application for spot Fruit, citrus, group 10 ...... 1 .0 treatment shall be limited to a max- Goat, fat ...... 0 .2 imum of 2 percent of the active ingre- Goat, meat ...... 0.05 Goat, meat byproducts ...... 0 .05 dient by weight. Hazelnut ...... 0 .2 (iv) Crack and crevice treatment Hog, fat ...... 0 .2 shall be limited to a maximum of 2 per- Hog, meat ...... 0 .05 cent of the active ingredient by weight. Hog, meat byproducts ...... 0 .05 Horse, fat ...... 0 .25 Equipment capable of delivering a pin- Horse, meat ...... 0 .25 stream of insecticide shall be used. Horse, meat byproducts ...... 0 .25 (v) Application via adhesive strips Kiwifruit ...... 2.0 Milk, fat (Reflecting 0.01 ppm in whole milk) ...... 0 .25 shall contain a maximum of 10% by Nectarine ...... 0 .05 weight of the controlled-release prod- Onion, bulb ...... 0 .5 uct in food-handling establishments Peach ...... 0 .05 where food and food products are held, Peanut ...... 0 .2 Peanut, refined oil ...... 0.2 processed, prepared, or served. A max- Pear ...... 0 .05 imum of 36 strips (or 5.15 grams of Pecan ...... 0 .2 chlorpyrifos) is to be used per 100 Pepper ...... 1 .0 Peppermint, tops ...... 0 .8 square feet of floor space. The strips Peppermint, oil ...... 8 .0 are not to be placed in exposed areas Plum, prune, fresh ...... 0.05 where direct contact with food, uten- Poultry, fat ...... 0.1 sils, and food-contact surfaces would be Poultry, meat ...... 0 .1 Poultry, meat byproducts ...... 0.1 likely to occur. Pumpkin ...... 0.05 (vi) To assure safe use of the insecti- Radish ...... 2 .0 cide, its label and labeling shall con- Rutabaga ...... 0 .5 Sheep, fat ...... 0 .2 form to that registered by the U.S. En- Sheep, meat ...... 0.05 vironmental Protection Agency, and it Sheep, meat byproducts ...... 0 .05 shall be used in accordance with such Spearmint, tops ...... 0 .8 label and labeling. Spearmint, oil ...... 8 .0 Sorghum, grain, forage ...... 0.5 (3) A tolerance of 0.1 part per million Sorghum, grain, grain ...... 0 .5 is established for residues of Sorghum, grain, stover ...... 2 .0 chlorpyrifos, per se, in or on food com- Soybean, seed ...... 0 .3 Strawberry ...... 0 .2 modities (other than those already cov- Sunflower, seed ...... 0.1 ered by a higher tolerance as a result Sweet potato, roots ...... 0 .05 of use on growing crops) in food service Turnip, roots ...... 1 .0 establishments where food and food Turnip, tops ...... 0.3 Vegetable, brassica, leafy, group 5 ...... 1.0 products are prepared and served, as a Vegetable, legume, group 6. except soybean .... 0 .05 result of the application of chlorpyrifos Walnut ...... 0 .2 in microencapsulated form. Wheat, forage ...... 3 .0 Wheat, grain ...... 0 .5 (i) Application of a microencap- Wheat, straw ...... 6 .0 sulated product shall be limited solely to spot and/or crack and crevice treat- (2) Chlorpyrifos [O,O-diethyl O-(3,5,6- ment in food handling establishments trichloro-2-pyridyl) phosphorothioate] where food and food products are pre- may be safely used in accordance with pared and served. All treatments shall the following prescribed conditions. be applied in such a manner as to avoid (i) Application shall be limited solely contamination of food or food contact to spot and/or crack and crevice treat- surfaces.

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(ii) Spray concentrations shall be Commodity Parts per limited to a maximum of 0.5 percent of million the active ingredient by weight. Beet, sugar, tops ...... 4.0 (iii) For crack and crevice treatment, Cattle, fat ...... 0.05 equipment capable of delivering a pin Cattle, meat ...... 0 .05 Cattle, meat byproducts ...... 0.05 stream of spray directly into cracks Garlic ...... 0 .25 and crevices or capable of applying Goat, fat ...... 0 .05 small amounts of insecticide into Goat, meat ...... 0.05 Goat, meat byproducts ...... 0 .05 cracks and crevices shall be used. Grass, straw ...... 1 .0 (iv) For spot treatment, an individual Horse, fat ...... 0 .05 spot shall not exceed 2 square feet. Horse, meat ...... 0 .05 (v) To assure safe use of the insecti- Horse, meat byproducts ...... 0 .05 Onion, bulb ...... 0 .25 cide, its label and labeling shall con- Shallot, bulb ...... 0 .25 form to that registered by the U.S. En- Shallot, fresh leaves ...... 0 .25 vironmental Protection Agency, and it Sheep, fat ...... 0 .05 Sheep, meat ...... 0.05 shall be used in accordance with such Sheep, meat byproducts ...... 0 .05 label and labeling. (b) Section 18 emergency exemptions. (b) Section 18 emergency exemptions. [Reserved] [Reserved] (c) Tolerances with regional registra- (c) Tolerances with regional registrations. Tolerances with regional reg- tion. Tolerances with regional registra- istration, as defined in 180.1(l), are es- tion as defined in 40 CFR 180.1(l) are established for residues of the pesticide tablished for the combined residues of chlorpyrifos per se (O,O-diethyl- O- ethofumesate,(2-ethoxy -2, 3-dihydro-3, (3,5,6-trichloro-2-pyridyl) 3-dimethyl-5-benzofuranyl phosphorothioate) in or on the fol- methanesulfonate) and its metabolites lowing food commodities: 2-hydroxy-2,3-dihydro-3,3-dimethyl-5- benzofuranyl methanesulfonate and 2,3- Parts per Commodity million dihydro-3,3-dimethyl-2-oxo-5- benzofuranyl methanesulfonate (both Asparagus ...... 5.0 Grape ...... 0 .01 calculated as the parent compound) in or on the raw agricultural commod- (d) Indirect or inadvertent residues. ities: [Reserved] Commodity Parts per [65 FR 33711, May 24, 2000, as amended at 67 million FR 49617, July 31, 2002; 71 FR 74817, Dec. 13, Carrot, roots ...... 7.0 2006; 73 FR 53739, Sept. 17, 2008; 76 FR 56656, Sept. 14, 2011] (d) Indirect or inadvertent residues. § 180.345 Ethofumesate; tolerances for [Reserved] residues. [63 FR 34828, June 26, 1998, as amended at 71 (a) General. Tolerances for the com- FR 51516, Aug. 30, 2006; 72 FR 52019, Sept. 12, bined residues of the herbicide 2007] ethofumesate (2-ethoxy-2,3-dihydro-3,3- § 180.349 Fenamiphos; tolerances for dimethyl-5-benzofuranyl residues. methanesulfonate) and its metabolites 2-hydroxy-2,3-dihydro-3,3-dimethyl-5- (a) General. Tolerances are estab- benzofuranyl methanesulfonate and 2,3- lished for residues of the nematicide/in- dihydro-3,3-dimethyl-2-oxo-5- secticide fenamiphos, ethyl 3-methyl-4- benzofuranyl methanesulfonate both (methylthio)phenyl 1- calculated as parent compound in or on (methylethyl)phosphoramidate, includ- the following food commodities: ing its metabolites and degradates, in or on the commodities in the following Commodity Parts per table. Compliance with the tolerance million levels specified in this paragraph is to Beet, garden, roots ...... 0 .5 be determined by measuring only the Beet, garden, tops ...... 5 .0 sum of fenamiphos, ethyl 3-methyl-4- Beet, sugar, molasses ...... 0 .5 Beet, sugar, refined sugar ...... 0 .2 (methylthio)phenyl 1- Beet, sugar, roots ...... 0 .3 (methylethyl)phosphoramidate, and its

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cholinesterase inhibiting metabolites (d) Indirect or inadvertent residues. ethyl 3-methyl-4- [Reserved] (methylsulfinyl)phenyl 1- [46 FR 58315, Dec. 1, 1981, as amended at 47 (methylethyl)phosphoramidate and FR 22957, May 26, 1982; 52 FR 33238, Sept. 2, ethyl 3-methyl-4- 1987; 58 FR 32304, June 9, 1993; 63 FR 57076, (methylsulfonyl)phenyl 1- Oct. 26, 1998; 72 FR 53461, Sept. 19, 2007] (methylethyl)phosphoramidate, calculated as the stoichiometric equiva- § 180.352 Terbufos; tolerances for resi- lent of fenamiphos, in or on the com- dues. modity. (a) General. Tolerances are established for the combined residues of the Parts per Commodity million insecticide terbufos (phosphorodithioic acid, S-(t-butylthio)methyl O,O-diethyl Banana1 ...... 0 .1 Grape1 ...... 0 .1 ester) and its phosphorylated (cholin- Grape, raisin1 ...... 0 .3 esterase-inhibiting) metabolites Pineapple1 ...... 0 .3 (phosphorothioic acid, S-(t- 1 There are no U.S. registrations as of May 31, 2007. butylthio)methyl O,O-diethyl ester; (b) Section 18 emergency exemptions. phosphorothioic acid, S-(t- [Reserved] butylsulfinyl)methyl O,O-diethyl ester; (c) Tolerances with regional registra- phosphorothioic acid, S-(t- tions. [Reserved] butylsulfonyl)methyl O,O-diethyl (d) Indirect or inadvertent residues. ester; phosphorodithioic acid, S-(t- [Reserved] butylsulfinyl)methyl O,O-diethyl ester; and phosphorodithioic acid, S-(t- [65 FR 33712, May 24, 2000, as amended at 73 butylsulfonyl)methyl O,O-diethyl FR 53739, Sept. 17, 2008; 75 FR 60243, Sept. 29, ester) in or on food commodities: 2010] Parts per § 180.350 Nitrapyrin; tolerances for Commodity million residues. Banana ...... 0.025 (a) General. Tolerances are estab- Beet, sugar, roots ...... 0 .05 lished for the combined residues of the Beet, sugar, tops ...... 0.1 soil microbiocide nitrapyrin [2-chloro- Coffee, green bean 1 ...... 0 .05 6-(trichloromethyl) pyridine] and its Corn, field, forage ...... 0 .5 Corn, field, grain ...... 0 .5 metabolite, 6-chloropicolinic acid in or Corn, field, stover ...... 0 .5 on the following raw agricultural com- Corn, pop, grain ...... 0.5 modities: Corn, pop, stover ...... 0.5 Corn, sweet, kernel plus cob with husks re- Parts per moved ...... 0 .05 Commodity million Corn, sweet, forage ...... 0 .5 Corn, sweet, stover ...... 0 .5 Corn, field, forage ...... 1 .0 Sorghum, grain, forage ...... 0.5 Corn, field, grain ...... 0 .1 Sorghum, grain, grain ...... 0 .05 Corn, field, milled byproducts ...... 0 .2 Sorghum, grain, stover ...... 0 .5 Corn, field, stover ...... 1 .0 Corn, pop, grain ...... 0.1 1 There are no U. S. registrations as of August 2, 1995, for Corn, pop, stover ...... 1.0 the use of terbufos on the growing crop, coffee. Corn, sweet, forage ...... 1 .0 Corn, sweet, kernel plus cob with husks re- (b) Section 18 emergency exemptions. moved ...... 0 .1 [Reserved] Corn, sweet, stover ...... 1 .0 (c) Tolerances with regional registra- Sorghum, forage, forage ...... 0 .5 Sorghum, grain, forage ...... 0.5 tions. [Reserved] Sorghum, grain, grain ...... 0 .1 (d) Indirect or inadvertent residues. Sorghum, grain, stover ...... 0 .5 [Reserved] Wheat, bran ...... 3.0 Wheat, forage ...... 2 .0 [73 FR 53740, Sept. 17, 2008] Wheat, grain ...... 0 .5 Wheat, milled byproducts, except flour ...... 2 .0 Wheat, straw ...... 6 .0 § 180.353 Desmedipham; tolerances for residues. (b) Section 18 emergency exemptions. (a) General. Tolerances are estab- [Reserved] lished for residues of the herbicide (c) Tolerances with regional registra- desmedipham, (ethyl-m- tions. [Reserved] hydroxycarbanilate carbanilate) in or

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on the following raw agricultural com- (2) Tolerances are established for the modities in the table that follows: combined residues of the herbicide bentazon (3-isopropyl-1H-2,1,3- Parts per Commodity million benzothiadiazin-4(3H)-one-2,2-dioxide) and its metabolite 2-amino-N-isopropyl Beet, garden, roots ...... 0 .05 benzamide (AIBA) in or on the fol- Beet, garden, tops ...... 1 .0 lowing food commodities: Beet, sugar, roots ...... 0 .1 Beet, sugar, tops ...... 5.0 Parts per Spinach ...... 6 .0 Commodity million

(b) Section 18 emergency exemptions. Cattle, fat ...... 0.05 Cattle, meat byproducts ...... 0.05 [Reserved] Cattle, meat ...... 0 .05 (c) Tolerances with regional registra- Egg ...... 0 .05 tions. [Reserved] Goat, fat ...... 0 .05 Goat, meat byproducts ...... 0 .05 (d) Indirect or inadvertent residues. Goat, meat ...... 0.05 [Reserved] Hog, fat ...... 0 .05 Hog, meat byproducts ...... 0 .05 [40 FR 4658, Jan. 31, 1975, as amended at 62 Hog, meat ...... 0 .05 FR 45747, Aug. 29, 1997; 63 FR 49472, Sept. 16, Milk ...... 0.02 1998; 64 FR 46292, Aug. 25, 1999; 65 FR 82293, Poultry, fat ...... 0.05 Poultry, meat byproducts ...... 0.05 Dec. 28, 2000; 66 FR 64773, Dec. 14, 2001; 68 FR Poultry, meat ...... 0 .05 37764, June 25, 2003; 69 FR 71717, Dec. 10, 2004; Sheep, fat ...... 0 .05 72 FR 53449, Sept. 19, 2007; 73 FR 53740, Sept. Sheep, meat byproducts ...... 0 .05 17, 2008] Sheep, meat ...... 0.05

§ 180.355 Bentazon; tolerances for resi- (b) Section 18 emergency exemptions. dues. [Reserved] (a) General. (1) Tolerances are estab- (c) Tolerances with regional registra- lished for the combined residues of the tions. Tolerances with regional reg- herbicide bentazon (3-isopropyl-1H- istration as defined in § 180.1(m), are es- 2,1,3-benzothiadiazin-4(3H)-one-2,2-diox- tablished for combined residues of the ide) and its 6- and 8-hydroxy metabo- herbicide, bentazon (3-isopropyl-1H-2, lites in or on the following food com- 1,3-benzothiadiazin-4(3H)-one-2,2-diox- modities: ide) and its 6- and 8-hydroxy metabolites in or on the following food com- Parts per modities: Commodity million Commodity Parts per Bean, dry, seed ...... 0 .05 million Bean, succulent ...... 0 .5 Corn, field, forage ...... 3 .0 Clover, forage ...... 1.0 Corn, field, grain ...... 0 .05 Clover, hay ...... 2.0 Corn, field, stover ...... 3 .0 Corn, pop, grain ...... 0.05 (d) Indirect or inadvertent residues. Corn, sweet, kernel plus cob with husks re- [Reserved] moved ...... 0 .05 Cowpea, forage ...... 10 .0 [42 FR 26979, May 26, 1977] Cowpea, hay ...... 3 .0 Flax, seed ...... 1 .0 EDITORIAL NOTE: For FEDERAL REGISTER ci- Pea, dry, seed ...... 1 .0 tations affecting § 180.355, see the List of CFR Pea, field, hay ...... 8.0 Sections Affected, which appears in the Pea, field, vines ...... 3 .0 Finding Aids section of the printed volume Pea, succulent ...... 3 .0 and at www.fdsys.gov. Peanut ...... 0 .05 Peanut, hay ...... 3.0 § 180.356 Norflurazon; tolerances for Pepper, nonbell ...... 0 .05 residues. Peppermint, tops ...... 1 .0 Rice, grain ...... 0 .05 (a) General. Tolerances are estab- Rice, hulls ...... 0 .25 lished for the combined residues of the Sorghum, forage ...... 0 .20 herbicide norflurazon (4-chloro-5- Sorghum, grain, grain ...... 0 .05 Sorghum, grain, stover ...... 0 .05 (methylamino)-2-(alpha, alpha, alpha- Soybean, forage ...... 8 .0 trifluoro-m-tolyl)-3-(2H)-pyridazinone) Soybean, hay ...... 8 .0 and its desmethyl metabolite 4-chloro- Soybean, seed ...... 0 .05 5-(amino)-2-alpha, alpha, alpha- Spearmint, tops ...... 1 .0 trifluoro-m-tolyl)-3(2H)-pyridazinone in

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or on the following raw agricultural EDITORIAL NOTE: For FEDERAL REGISTER ci- commodities: tations affecting § 180.356, see the List of CFR Sections Affected, which appears in the Finding Aids section of the printed volume Commodity Parts per million and at www.fdsys.gov. Alfalfa, forage ...... 3.0 Alfalfa, hay ...... 5.0 § 180.360 Asulam; tolerance for resi- Alfalfa, seed ...... 0 .1 dues. Almond, hulls ...... 1 .0 (a) General. Tolerances are estab- Almond ...... 0.1 Apple ...... 0.1 lished for the combined residues of Apricot ...... 0 .1 asulam (methyl sulfanilylcarbamate) Asparagus ...... 0.05 and its sulfanilamide containing me- Avocado ...... 0 .20 Blackberry ...... 0 .1 tabolites in or on the following food Blueberry ...... 0 .2 commodities: Cattle, fat ...... 0.1 Cattle, liver ...... 0 .50 Commodity Parts per Cattle, meat ...... 0 .1 million Cattle, meat byproducts, except liver ...... 0 .1 Cherry ...... 0.1 Cattle, fat ...... 0.05 Citrus, dried pulp ...... 0 .4 Cattle, meat ...... 0 .05 Citrus, molasses ...... 1.0 Cattle, meat byproducts ...... 0.2 Cotton, undelinted seed ...... 0 .1 Goat, fat ...... 0 .05 Cranberry ...... 0 .1 Goat, meat ...... 0.05 Fruit, citrus ...... 0 .2 Goat, meat byproducts ...... 0 .2 Goat, fat ...... 0 .1 Hog, fat ...... 0 .05 Goat, liver ...... 0.50 Hog, meat ...... 0 .05 Goat, meat ...... 0.1 Hog, meat byproducts ...... 0 .2 Goat, meat byproducts, except liver ...... 0 .1 Horse, fat ...... 0 .05 Grape ...... 0 .1 Horse, meat ...... 0 .05 Hazelnut ...... 0 .1 Horse, meat byproducts ...... 0 .2 Hog, fat ...... 0 .1 Milk ...... 0.05 Hog, liver ...... 0 .50 Sheep, fat ...... 0 .05 Hog, meat ...... 0 .1 Sheep, meat ...... 0.05 Hog, meat byproducts, except liver ...... 0 .1 Sheep, meat byproducts ...... 0 .2 Hop, dried cones ...... 3 .0 Sugarcane, cane ...... 1.0 Hop, vines ...... 1 .0 Horse, fat ...... 0 .1 Sugarcane, molasses ...... 30 Horse, liver ...... 0 .50 Horse, meat ...... 0 .1 (b) Section 18 emergency exemptions. Horse, meat byproducts, except liver ...... 0 .1 [Reserved] Milk ...... 0.1 Nectarine ...... 0 .1 (c) Tolerances with regional registra- Peach ...... 0 .1 tions. [Reserved] Peanut ...... 0 .05 (d) Indirect or inadvertent residues. Peanut, hay ...... 5.50 [Reserved] Peanut, hay ...... 1.5 Pear ...... 0 .1 [68 FR 39441, July 1, 2003, as amended at 72 Pecan ...... 0 .1 FR 37654, July 11, 2007] Plum, prune, fresh ...... 0.1 Poultry, fat ...... 0.1 Poultry, meat ...... 0 .1 § 180.361 Pendimethalin; tolerances for Poultry, meat byproducts ...... 0.1 residues. Raspberry ...... 0 .2 Sheep, fat ...... 0 .1 (a)(1) General. Tolerances are estab- Sheep, liver ...... 0.50 lished for residues of the herbicide Sheep, meat ...... 0.1 pendimethalin, including its metabo- Sheep, meat byproducts, except liver ...... 0 .1 Soybean ...... 0.1 lites and degradates, in or on the com- Soybean, forage ...... 1 .0 modities. Compliance with the toler- Soybean, hay ...... 1 .0 ance levels specified in the following Walnut ...... 0 .1 table below is to be determined by measuring only pendimethalin, [N- (1- (b) Section 18 emergency exemptions. ethylpropyl)-3,4-dimethyl-2,6- [Reserved] dinitrobenzenamine], and its metabo- (c) Tolerances with regional registra- lite, 4-[(1-ethylpropyl)amino]-2-methyl- [Reserved] tion. 3,5-dinitrobenzyl alcohol, calculated as (d) Indirect or inadvertent residues. the stoichiometric equivalent of [Reserved] pendimethalin, in or on the following [47 FR 14909, Apr. 7, 1982] commodities:

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including its metabolites and Commodity Parts per million degradates, in or on commodities listed Alfalfa, forage ...... 3.5 in the following table. Compliance with Alfalfa, hay ...... 4.0 the tolerance levels is to be determined Alfalfa, seed ...... 0 .10 by measuring only the sum of Almond, hulls ...... 6 .0 Apple, wet pomace ...... 0 .20 pendimethalin (N-(1-ethylpropyl)-3,4-di- Artichoke, globe ...... 0.1 methyl-2,6-dinitrobenzenamine)) and Asparagus ...... 0.15 its metabolite, 1-(1-ethylpropyl)-5, 6-di- Beans ...... 0 .10 Beans, forage ...... 0 .10 methyl-7-nitro-1H-benzimidazole (me- Beans, hay ...... 0 .10 tabolite 6), calculated as the stoichio- Berry, low growing subgroup 13–07G ...... 0.1 metric equivalent of pendimethalin, in Brassica head and stem, subgroup 5-A ...... 0 .1 Brassica, leafy greens, subgroup 5B ...... 0 .20 or on the commodity. Bushberry subgroup 13–07B ...... 0 .10 Caneberry subgroup 13–07A ...... 0.10 Parts Commodity per Carrot ...... 0 .5 million Citrus, oil ...... 0.5 Corn, field, forage ...... 0 .1 Cattle, fat ...... 0.30 Corn, field, grain ...... 0 .1 Cattle, meat ...... 0 .10 Corn, field, stover ...... 0 .1 Corn, pop, grain ...... 0.1 Cattle, meat byproduct ...... 3.0 Corn, sweet, forage ...... 0 .1 Goats, fat ...... 0 .30 Corn, sweet, kernel plus cob with husks re- Goats, meat ...... 0.10 moved ...... 0 .1 Goats, meat byproduct ...... 3 .0 Corn, sweet, stover ...... 0 .1 Horse, fat ...... 0 .30 Cotton, gin byproducts ...... 3 .0 Horse, meat ...... 0 .10 Cotton, undelinted seed ...... 0 .1 Horse, byproduct ...... 3 .0 Crayfish ...... 0.05 Milk ...... 0.04 Fruit, citrus, group 10–10 ...... 0 .1 Sheep, fat ...... 0 .30 Fruit, pome, group 11–10 ...... 0 .1 Sheep, meat ...... 0.10 Fruit, small vine climbing, except grape, sub- Sheep, meat byproduct ...... 3 .0 group 13–07E ...... 0.10 Fruit, stone, group 12–12 ...... 0 .1 Grape ...... 0 .1 (b) Section 18 emergency exemptions. Grass, forage, fodder, and hay crop group 17, Time-limited tolerances specified in forage ...... 1,000 the following table are established for Grass, forage, fodder, and hay crop group 17, hay ...... 2,000 combined residues of the herbicide Hop, dried cones ...... 0 .1 pendimethalin, [N-(1-ethylpropyl)-3,4- Lettuce, leaf ...... 4 .0 dimethyl-2,6-dinitrobenzenamine], and Melon subgroup 9A ...... 0 .10 Nut, tree, group 14–12 ...... 0 .10 its metabolite 4-[(1- Olive ...... 0 .1 ethylpropyl)amino]-2-methyl-3,5- Onion, bulb subgroup 3–07A ...... 0.1 dinitrobenzyl alcohol, in or on the Onion, green subgroup 3–07B ...... 0.2 specified agricultural commodities, re- Peanut ...... 0 .1 Peanut, hay ...... 0.1 sulting from use of the pesticide pursu- Peas (except field peas) ...... 0.10 ant to FIFRA section 18 emergency ex- Peppermint, oil ...... 1 .0 emptions. The tolerances expire and Peppermint, tops ...... 0 .2 Pomegranate ...... 0 .10 are revoked on the date specified in the Potato ...... 0 .1 table. Rice, grain ...... 0 .1 Sorghum, forage ...... 0 .1 Parts per Expiration/ Sorghum, grain, grain ...... 0 .1 Commodity million revocation Sorghum, grain, stover ...... 0 .1 date Soybean, forage ...... 0 .1 Soybean, hay ...... 0 .1 Bermuda grass, forage ...... 25 12/31/10 Soybean, seed ...... 0 .1 Bermuda grass, hay ...... 60 12/31/10 Spearmint, oil ...... 1 .0 Spearmint, tops ...... 0 .2 (c) Tolerances with regional registra- Sugarcane, cane ...... 0.1 Sunflower subgroup 20B ...... 0.1 tions. [Reserved] Turnip greens ...... 0 .20 (d) Indirect or inadvertent residues. Vegetable, fruiting, group 8–10 ...... 0 .1 [Reserved] Vegetable, soybean, succulent ...... 0 .10 Wheat, grain ...... 0 .10 [49 FR 15293, Apr. 18, 1984] Wheat, forage ...... 3 .0 Wheat, hay ...... 0 .60 EDITORIAL NOTE: For FEDERAL REGISTER ci- Wheat, straw ...... 0 .30 tations affecting § 180.361, see the List of CFR Sections Affected, which appears in the (2) Tolerances are established for res- Finding Aids section of the printed volume idues of the herbicide pendimethalin, and at www.fdsys.gov.

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§ 180.362 Fenbutatin-oxide; tolerances Commodity Parts per for residues. million (a) General. (1) Tolerances are estab- Hog, meat byproducts ...... 0 .5 lished for residues of the miticide/acar- Horse, fat ...... 0 .5 Horse, meat ...... 0 .5 icide fenbutatin-oxide, including its Horse, meat byproducts ...... 0 .5 metabolites and degradates, in or on Milk, fat ...... 0 .1 the plant commodities in the table in Poultry, fat ...... 0.1 Poultry, meat ...... 0 .1 this paragraph. Compliance with the Poultry, meat byproducts ...... 0.1 tolerance levels specified in this para- Sheep, fat ...... 0 .5 graph is to be determined by measuring Sheep, meat ...... 0.5 only fenbutatin-oxide, hexakis (2-meth- Sheep, meat byproducts ...... 0 .5 yl-2-phenylpropyl) distannoxane, in or (b) Section 18 emergency exemptions. on the commodity. [Reserved] (c) Tolerances with regional registra- Commodity Parts per million tions. A tolerance with regional reg- Almond, hulls ...... 80 .0 istration, as defined in § 180.1(l), is es- Apple ...... 15.0 tablished for residues of the miticide/ Apple, wet pomace ...... 100.0 acaricide fenbutatin-oxide, including Cherry, sweet ...... 6 .0 Cherry, tart ...... 6 .0 its metabolites and degradates, in or Citrus, dried pulp ...... 100.0 on the plant commodity in the table in Citrus, oil ...... 140.0 this paragraph. Compliance with the Cucumber ...... 4 .0 Eggplant ...... 6.0 tolerance level specified in this para- Fruit, citrus, group 10 ...... 20 .0 graph is to be determined by measuring Grape ...... 5 .0 only fenbutatin-oxide, hexakis (2-meth- Grape, raisin ...... 20.0 Nut, tree, group 14 ...... 0 .5 yl-2-phenylpropyl) distannoxane, in or Papaya ...... 2 .0 on the commodity. Peach ...... 10 .0 Pear ...... 15 .0 Commodity Parts per Pistachio ...... 0.5 million Plum, prune, fresh ...... 4.0 Plum, prune, dried ...... 20.0 Raspberry ...... 10 .0 Strawberry ...... 10.0 (d) Indirect or inadvertent residues. (2) Tolerances are established for res- [Reserved] idues of the miticide/acaricide fenbutatin-oxide, including its metabo- [65 FR 33713, May 24, 2000, as amended at 72 lites and degradates, in or on the ani- FR 41930, Aug. 1, 2007; 73 FR 5109, Jan. 29, 2008; 76 FR 23494, Apr. 27, 2011] mal commodities in the table in this paragraph. Compliance with the toler- § 180.364 Glyphosate; tolerances for ance levels specified in this paragraph residues. is to be determined by measuring only (a) General. (1) Tolerances are estab- the sum of fenbutatin-oxide, hexakis lished for residues of glyphosate, in- (2-methyl-2-phenylpropyl) cluding its metabolites and degradates, distannoxane, and its organotin me- in or on the commodities listed below tabolites, dihydroxybis(2-methyl-2- resulting from the application of phenylpropyl) stannane and 2-methyl- glyphosate, the isopropylamine salt of 2-phenylpropylstannoic acid, cal- glyphosate, the ethanolamine salt of culated as the stoichiometric equiva- glyphosate, the dimethylamine salt of lent of fenbutatin-oxide, in or on the glyphosate, the ammonium salt of commodity. glyphosate, and the potassium salt of Parts per glyphosate. Compliance with the fol- Commodity million lowing tolerance levels is to be deter- Cattle, fat ...... 0.5 mined by measuring only glyphosate Cattle, meat ...... 0 .5 (N-(phosphonomethyl)glycine). Cattle, meat byproducts ...... 0.5 Egg ...... 0 .1 Commodity Parts per Goat, fat ...... 0 .5 million Goat, meat ...... 0.5 Goat, meat byproducts ...... 0 .5 Acerola ...... 0.2 Hog, fat ...... 0 .5 Alfalfa, seed ...... 0 .5 Hog, meat ...... 0 .5 Almond, hulls ...... 25

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Parts per Parts per Commodity million Commodity million

Aloe vera ...... 0 .5 Nut, tree, group 14 ...... 1 .0 Ambarella ...... 0 .2 Oilseeds, group 20, except canola ...... 40 Animal feed, nongrass, group 18 ...... 400 Okra ...... 0.5 Artichoke, globe ...... 0.2 Olive ...... 0 .2 Asparagus ...... 0.5 Oregano, Mexican, leaves ...... 2 .0 Atemoya ...... 0 .2 Palm heart ...... 0 .2 Avocado ...... 0 .2 Palm heart, leaves ...... 0 .2 Bamboo, shoots ...... 0 .2 Palm, oil ...... 0 .1 Banana ...... 0.2 Papaya ...... 0 .2 Barley, bran ...... 30 Papaya, mountain ...... 0.2 Beet, sugar, dried pulp ...... 25 Passionfruit ...... 0 .2 Beet, sugar, roots ...... 10 Pawpaw ...... 0 .2 Beet, sugar, tops ...... 10 Pea, dry ...... 8 .0 Berry and small fruit, group 13–07 ...... 0 .20 Peanut ...... 0 .1 Betelnut ...... 1 .0 Peanut, hay ...... 0.5 Biriba ...... 0 .2 Pepper leaf, fresh leaves ...... 0 .2 Blimbe ...... 0 .2 Peppermint, tops ...... 200 Breadfruit ...... 0 .2 Perilla, tops ...... 1 .8 Cacao bean, bean ...... 0 .2 Persimmon ...... 0 .2 Cactus, fruit ...... 0 .5 Pineapple ...... 0.1 Cactus, pads ...... 0 .5 Pistachio ...... 1.0 Canistel ...... 0 .2 Pomegranate ...... 0 .2 Carrot ...... 5 .0 Pulasan ...... 0 .2 Chaya ...... 1.0 Quinoa, grain ...... 5 .0 Cherimoya ...... 0 .2 Rambutan ...... 0 .2 Citrus, dried pulp ...... 1 .5 Rice, grain ...... 0 .1 Coconut ...... 0 .1 Rice, wild, grain ...... 0.1 Coffee, bean, green ...... 1 .0 Rose apple ...... 0 .2 Corn, pop, grain ...... 0.1 Sapodilla ...... 0 .2 Corn, sweet, kernel plus cob with husk removed 3.5 Sapote, black ...... 0 .2 Cotton, gin byproducts ...... 210 Sapote, mamey ...... 0 .2 Custard apple ...... 0 .2 Sapote, white ...... 0 .2 Date, dried fruit ...... 0 .2 Shellfish ...... 3 .0 Dokudami ...... 2 .0 Soursop ...... 0 .2 Durian ...... 0 .2 Spanish lime ...... 0 .2 Epazote ...... 1 .3 Spearmint, tops ...... 200 Feijoa ...... 0 .2 Spice subgroup 19B ...... 7 .0 Fig ...... 0 .2 Star apple ...... 0 .2 Fish ...... 0 .25 Starfruit ...... 0 .2 Fruit, citrus, group 10–10 ...... 0 .50 Stevia, dried leaves ...... 1 .0 Fruit, pome, group 11–10 ...... 0 .20 Sugar apple ...... 0 .2 Fruit, stone, group 12 ...... 0 .2 Sugarcane, cane ...... 2.0 Galangal, roots ...... 0 .2 Sugarcane, molasses ...... 30 Ginger, white, flower ...... 0 .2 Surinam cherry ...... 0 .2 Gourd, buffalo, seed ...... 0 .1 Sweet potato ...... 3.0 Governor’s plum ...... 0 .2 Tamarind ...... 0 .2 Gow kee, leaves ...... 0 .2 Tea, dried ...... 1 .0 Grain, cereal, forage, fodder and straw, group Tea, instant ...... 7 .0 16, except field corn, forage and field corn, Teff, forage ...... 100 stover ...... 100 Teff, grain ...... 5 .0 Grain, cereal, group 15 except field corn, pop- Teff, hay ...... 100 corn, rice, sweet corn, and wild rice ...... 30 Ti, leaves ...... 0 .2 Grass, forage, fodder and hay, group 17 ...... 300 Ti, roots ...... 0 .2 Guava ...... 0 .2 Ugli fruit ...... 0.5 Herbs subgroup 19A ...... 0 .2 Vegetable, bulb, group 3–07 ...... 0 .20 Hop, dried cones ...... 7 .0 Vegetable, cucurbit, group 9 ...... 0.5 Ilama ...... 0 .2 Vegetable, foliage of legume, subgroup 7A, ex- Imbe ...... 0 .2 cept soybean ...... 0 .2 Imbu ...... 0 .2 Vegetable, fruiting, group 8–10 (except okra) ..... 0 .10 Jaboticaba ...... 0 .2 Vegetable, leafy, brassica, group 5 ...... 0.2 Jackfruit ...... 0 .2 Vegetable, leafy, except brassica, group 4 ...... 0 .2 Kava, roots ...... 0 .2 Vegetable, leaves of root and tuber, group 2, Kenaf, forage ...... 200 except sugar beet tops ...... 0 .2 Leucaena, forage ...... 200 Vegetable, legume, group 6 except soybean Longan ...... 0 .2 and dry pea ...... 5 .0 Lychee ...... 0 .2 Vegetables, root and tuber, group 1, except car- Mamey apple ...... 0 .2 rot, sweet potato, and sugar beet ...... 0 .20 Mango ...... 0.2 Wasabi, roots ...... 0 .2 Mangosteen ...... 0 .2 Water spinach, tops ...... 0.2 Marmaladebox ...... 0 .2 Watercress, upland ...... 0 .2 Mioga, flower ...... 0 .2 Wax jambu ...... 0 .2 Noni ...... 0 .20 Yacon, tuber ...... 0.2 Nut, pine ...... 1 .0

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(2) Tolerances are established for res- and/or served, provided that the food is idues of glyphosate, including its me- removed or covered prior to such use, tabolites and degradates, in or on the except for bagged food in warehouse commodities listed below resulting storage which need not be removed or from the application of glyphosate, the covered prior to applications of formu- isopropylamine salt of glyphosate, the lations containing N-octyl ethanolamine salt of glyphosate, the bicycloheptene dicarboximide. Compli- dimethylamine salt of glyphosate, the ance with the tolerance level specified ammonium salt of glyphosate, and the in this paragraph is to be determined potassium salt of glyphosate. Compli- by measuring only N-octyl ance with the following tolerance lev- bicycloheptene dicarboximide, in or on els is to be determined by measuring the commodity. only glyphosate (N- (b) Section 18 emergency exemptions. (phosphonomethyl)glycine) and its me- [Reserved] tabolite N-acetyl-glyphosate (N-acetyl- (c) Tolerances with regional registra- N-(phosphonomethyl)glycine; cal- tions. [Reserved] culated as the stoichiometric equiva- (d) Indirect or inadvertent residues. lent of glyphosate). [Reserved]

Parts per [65 FR 33713, May 24, 2000, as amended at 75 Commodity Million FR 60243, Sept. 29, 2010]

Canola, seed ...... 20 § 180.368 Metolachlor; tolerances for Cattle, meat byproducts ...... 5.0 Corn, field, forage ...... 13 residues. Corn, field, grain ...... 5 .0 (a) General. (1) Tolerances are estab- Corn, field, stover ...... 100 Egg ...... 0 .05 lished for the combined residues (free Goat, meat byproducts ...... 5 .0 and bound) of the herbicide Grain aspirated fractions ...... 310 .0 metolachlor, 2-chloro-N-(2- ethyl-6- Hog, meat byproducts ...... 5 .0 methylphenyl)-N-(2-methoxy-1- Horse, meat byproducts ...... 5 .0 Poultry, meat ...... 0 .10 methylethyl)acetamide, and its me- Poultry, meat byproducts ...... 1.0 tabolites, determined as the deriva- Sheep, meat byproducts ...... 5 .0 tives, 2- [(2-ethyl-6- Soybean, forage ...... 100.0 Soybean, hay ...... 200.0 methylphenyl)amino]-1-propanol and 4- Soybean, hulls ...... 120 .0 (2-ethyl-6-methylphenyl)-2- hydroxy-5- Soybean, seed ...... 20.0 methyl-3-morpholinone, each expressed as the parent compound in the fol- (b) Section 18 emergency exemptions. lowing raw agricultural commodities: [Reserved] (c) Tolerances with regional registra- Commodity Parts per tions. [Reserved] million (d) Indirect or inadvertent residues. Almond, hulls ...... 0 .30 [Reserved] Animal feed, nongrass, group 18 ...... 1 .0 Cattle, fat ...... 0.02 [45 FR 64911, Oct. 1, 1980] Cattle, kidney ...... 0 .20 Cattle, liver ...... 0 .05 EDITORIAL NOTE: For FEDERAL REGISTER ci- Cattle, meat ...... 0 .02 tations affecting § 180.364, see the List of CFR Cattle, meat byproducts, except kidney and liver 0.04 Sections Affected, which appears in the Corn, field, forage ...... 6 .0 Finding Aids section of the printed volume Corn, field, grain ...... 0 .10 and at www.fdsys.gov. Corn, field, stover ...... 6 .0 Corn, pop, grain ...... 0.10 Corn, pop, stover ...... 6.0 § 180.367 n-Octyl bicycloheptenedi- Corn, sweet, forage ...... 6 .0 carboximide; tolerances for resi- Corn, sweet, kernel plus cob with husks re- dues. moved ...... 0 .10 Corn, sweet, stover ...... 6 .0 (a) General. A tolerance of 5 parts per Cotton, gin byproducts ...... 4 .0 million is established for residues of Cotton, undelinted seed ...... 0 .10 the insecticide synergist N-octyl Dillweed ...... 0 .50 Egg ...... 0 .02 bicycloheptene dicarboximide, includ- Goat, fat ...... 0 .02 ing its metabolites and degradates, in Goat, kidney ...... 0 .20 or on all food items in food handling Goat, liver ...... 0.05 Goat, meat ...... 0.02 establishments where food and food Goat, meat byproducts, except kidney and liver 0 .04 products are held, processed, prepared Grass, forage ...... 10

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Parts per Parts per Commodity million Commodity million

Grass, hay ...... 0 .20 Cattle, liver ...... 0 .05 Horse, fat ...... 0 .02 Cattle, meat ...... 0 .02 Horse, kidney ...... 0 .20 Cattle, meat byproducts, except kidney and liver 0.04 Horse, liver ...... 0 .05 Cilantro, leaves ...... 8 .0 Horse, meat ...... 0 .02 Coriander, seed ...... 0 .13 Horse, meat byproducts, except kidney and liver 0 .04 Corn, field, forage ...... 40 Milk ...... 0.02 Corn, field, grain ...... 0 .10 Nut, tree, group 14 ...... 0 .10 Corn, field, stover ...... 40 Okra ...... 0.50 Corn, pop, grain ...... 0.10 Peanut ...... 0 .20 Corn, pop, stover ...... 40 Peanut, hay ...... 20 Corn, sweet, forage ...... 40 Peanut, meal ...... 0 .40 Corn, sweet, kernel plus cob with husks re- Potato ...... 0 .20 moved ...... 0 .10 Poultry, fat ...... 0.02 Corn, sweet, stover ...... 40 Poultry, meat ...... 0 .02 Cotton, gin byproducts ...... 4 .0 Poultry, meat byproducts ...... 0.05 Cotton, undelinted seed ...... 0 .10 Safflower, seed ...... 0 .10 Egg ...... 0 .02 Sheep, fat ...... 0 .02 Grain, aspirated fractions ...... 0 .70 Sheep, kidney ...... 0.20 Goat, fat ...... 0 .02 Sheep, liver ...... 0.05 Goat, kidney ...... 0 .20 Sheep, meat ...... 0.02 Goat, liver ...... 0.05 Sheep, meat byproducts, except kidney and Goat, meat ...... 0.02 liver ...... 0 .04 Goat, meat byproducts, except kidney and liver 0 .04 Sorghum, grain, forage ...... 1.0 Grass, forage ...... 10 .0 Sorghum, grain, grain ...... 0 .30 Grass, hay ...... 0 .20 Sorghum, grain, stover ...... 4 .0 Horse, fat ...... 0 .02 Soybean, forage ...... 5 .0 Horse, kidney ...... 0 .20 Soybean, hay ...... 8 .0 Horse, liver ...... 0 .05 Soybean, seed ...... 0 .20 Horse, meat ...... 0 .02 Tomato ...... 0.10 Horse, meat byproducts, except kidney and liver 0 .04 Vegetable, foliage of legume, subgroup 7A, ex- Leaf petioles, subgroup 4B ...... 0 .10 cept soybean ...... 15.0 Lettuce ...... 1.5 Vegetable, legume, group 6 ...... 0 .30 Low growing berry subgroup 13–07G, except cranberry ...... 0 .40 (2) Tolerances are established for res- Milk ...... 0.02 idues of S-metolachlor, including its Onion, bulb, subgroup 3-07A ...... 0 .10 metabolites and degradates, in or on Onion, green, subgroup 3-07B ...... 2 .0 Peanut ...... 0 .20 the commodity(s), as defined. Compli- Peanut, hay ...... 20.0 ance with the tolerance levels specified Peanut, meal ...... 0 .40 in the following table below is to be de- Poultry, fat ...... 0.02 Poultry, meat ...... 0 .02 termined by measuring only the sum of Poultry, meat byproducts ...... 0.05 free and bound S-metolachlor, S-2- Safflower, seed ...... 0 .10 chloro-N-(2-ethyl-6-methylphenyl)-N- Sesame, seed ...... 0 .13 (2-methoxy-1-methylethyl)acetamide, Sheep, fat ...... 0 .02 Sheep, kidney ...... 0.20 its R-enantiomer, and its metabolites, Sheep, liver ...... 0.05 determined as the derivatives, 2-(2- Sheep, meat ...... 0.02 ethyl-6-methylphenyl)amino-1-pro- Sheep, meat byproducts, except kidney and liver ...... 0 .04 panol and 4-(2-ethyl-6-methylphenyl)-2- Sorghum, grain, forage ...... 1.0 hydroxy-5-methyl-3-morpholinone, cal- Sorghum, grain, grain ...... 0 .3 culated as the stoichiometric equiva- Sorghum, grain, stover ...... 4 .0 lent of S-metolachlor, in or on the Sorghum, sweet, stalk ...... 4.0 Soybean, forage ...... 5 .0 commodity. Soybean, hay ...... 8 .0 Soybean, seed ...... 0 .20 Commodity Parts per Spinach ...... 0 .50 million Sunflower, meal ...... 1 .0 Sunflower subgroup 20B ...... 1.0 Asparagus ...... 0.10 Tomato, paste ...... 0 .30 Beet, garden, leaves ...... 1 .8 Turnip, greens ...... 1.8 Beet, sugar, molasses ...... 2 .0 Vegetable, cucurbit group 9 ...... 0 .50 Beet, sugar, roots ...... 0 .5 Vegetable, foliage of legume, except soybean, Beet, sugar, tops ...... 15.0 subgroup 7A ...... 15 .0 Brassica, head and stem, subgroup 5A ...... 0 .60 Vegetable, fruiting, group 8–10, except tabasco Brassica, leafy greens, subgroup 5B ...... 1 .8 pepper ...... 0.10 Bushberry subgroup 13-07B ...... 0 .15 Vegetable, legume, group 6 ...... 0 .30 Caneberry subgroup 13-07A ...... 0.10 Vegetable, root, except sugar beet, subgroup Carrot, roots ...... 0.40 1B, except carrot ...... 0 .30 Cattle, fat ...... 0.02 Vegetable, tuberous and corm, subgroup 1C ..... 0.20 Cattle, kidney ...... 0 .20

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(b) Section 18 emergency exemptions. as the parent compound in the fol- [Reserved] lowing raw agricultural commodities: (c) Tolerances with regional registra- Parts per tions. (1) Tolerances with regional reg- Commodity million istration as defined in 180.1(l) are es- Animal feed, nongrass, group 18 ...... 1 .0 tablished for the combined residues Barley, grain ...... 0 .10 (free and bound) of the herbicide Barley, hay ...... 0 .80 metolachlor [2-chloro-N-(2-ethyl-6- Barley, straw ...... 0 .80 Buckwheat, grain ...... 0.10 methylphenyl)-N-(2-methoxy-1- Millet, forage ...... 0 .50 methylethyl)acetamide] and its me- Millet, grain ...... 0 .10 tabolites, determined as the deriva- Millet, hay ...... 0 .80 tives, 2-[2-ethyl-6- Millet, straw ...... 0 .80 Oat, forage ...... 0 .50 methylphenyl)amino]-1-propanol and 4- Oat, grain ...... 0 .10 (2-ethyl-6-methylphenyl)-2-hydroxy-5- Oat, hay ...... 0.80 methyl-3-morpholinone, each expressed Oat, straw ...... 0.80 Rice, grain ...... 0 .10 as the parent compound, in or on the Rye, forage ...... 0 .50 following raw agricultural commod- Rye, grain ...... 0.10 ities: Rye, straw ...... 0 .80 Wheat, forage ...... 0 .50 Wheat, grain ...... 0 .10 Commodity Parts per Wheat, hay ...... 0 .80 million Wheat, straw ...... 0 .80 Pepper, nonbell ...... 0 .50 (2) Tolerances for are established for (2) Tolerances with regional registra- the indirect or inadvertent residues of tion are established for residues of S- S-metolachlor, including its metabo- metolachlor, including its metabolites lites and degradates, in or on the com- and degradates, in or on the commod- modities identified in the following ities identified in the following table table below. Compliance with the toler- below. Compliance with the tolerance ance levels specified in the following levels specified in the following table table below is to be determined by below is to be determined by measuring measuring only the sum of free and only the sum of free and bound S- bound S-metolachlor, S-2-chloro-N-(2- metolachlor, S-2-chloro-N-(2-ethyl-6- ethyl-6-methylphenyl)-N-(2-methoxy-1- methylphenyl)-N-(2-methoxy-1- methylethyl)acetamide, its R- methylethyl)acetamide, its R- enantiomer, and its metabolites, deter- enantiomer, and its metabolites, determined as the derivatives, 2-(2-ethyl-6- mined as the derivatives, 2-(2-ethyl-6- methylphenyl)amino-1-propanol and 4- methylphenyl)amino-1-propanol and 4- (2-ethyl-6-methylphenyl)-2-hydroxy-5- (2-ethyl-6-methylphenyl)-2-hydroxy-5- methyl-3-morpholinone, calculated as methyl-3-morpholinone, calculated as the stoichiometric equivalent of S- the stoichiometric equivalent of S- metolachlor, in or on the commodity. metolachlor, in or on the commodity. Parts per Commodity million Commodity Parts per million Animal feed, nongrass, group 18 ...... 1 .0 Barley, grain ...... 0 .10 Pepper, tabasco ...... 0 .50 Barley, hay ...... 0 .50 Barley, straw ...... 0 .50 Buckwheat, grain ...... 0.10 (d) Indirect or inadvertent residues. (1) Millet, forage ...... 0 .50 Tolerances are established for the indi- Millet, grain ...... 0 .10 rect or inadvertent combined residues Millet, hay ...... 0 .50 (free and bound) of the herbicide Millet, straw ...... 0 .50 Oat, forage ...... 0 .50 metolachlor, 2-chloro-N-(2-ethyl-6- Oat, grain ...... 0 .10 methylphenyl)-N-(2-methoxy-1- Oat, hay ...... 0.50 methylethyl)acetamide, and its me- Oat, straw ...... 0.50 Rice, grain ...... 0 .10 tabolites, determined as the deriva- Rye, forage ...... 0 .50 tives, 2-[(2-ethyl-6- Rye, grain ...... 0.10 methylphenyl)amino]-1-propanol and 4- Rye, straw ...... 0 .50 Wheat, forage ...... 0 .50 (2-ethyl-6-methylphenyl)-2- hydroxy-5- Wheat, grain ...... 0 .10 methyl-3-morpholinone, each expressed Wheat, hay ...... 0 .50

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Parts per Parts per Commodity million Commodity million

Wheat, straw ...... 0 .50 Cotton, gin byproducts ...... 0.1 Cotton, undelinted seed ...... 0.1 Tomato ...... 0.15 [73 FR 53740, Sept. 17, 2008, as amended at 74 FR 48412, Sept. 23, 2009; 75 FR 56903, Sept. 17, 2010; 77 FR 48906, Aug. 15, 2012; 77 FR 59127, * * * * * Sept. 26, 2012; 79 FR 17441, Mar. 28, 2014; 80 FR 38986, July 8, 2015] § 180.371 Thiophanate-methyl; tolerances for residues. § 180.370 5-Ethoxy-3-(trichloromethyl)- (a) General. Tolerances are estab- 1,2,4-thiadiazole; tolerances for residues. lished for residues of thiophanate- methyl, dimethyl ((1,2-phenylene) bis (a) General. Tolerances are estab- (iminocarbonothioyl)) bis(carbamate), lished for residues of the fungicide 5- including its metabolites and ethoxy-3-(trichloromethyl)-1,2,4- degradates, in or on the commodities thiadiazole and its monoacid metabo- in the following table. Compliance with lite 3-carboxy-5-ethoxy-1,2,4- the tolerance levels specified in this thiadiazole in or on the following raw paragraph is to be determined by meas- agricultural commodities: uring only the sum of thiophanate- Parts per methyl, dimethyl ((1,2-phenylene) bis Commodity million (iminocarbonothioyl)) bis(carbamate), and its metabolite, methyl 2- Barley, grain ...... 0 .1 benzimidazoyl carbamate (MBC), cal- Barley, hay ...... 0 .1 Corn, field, forage ...... 0 .1 culated as the stoichiometric equiva- Corn, field, grain ...... 0 .1 lent of thiophanate-methyl, in or on Corn, field, stover ...... 0 .1 the commodity. Corn, sweet, forage ...... 0 .1 Corn, sweet, stover ...... 0 .1 Commodity Parts per Cotton, gin byproducts ...... 0 .1 million Cotton, undelinted seed ...... 0 .1 Peanut ...... 0 .1 Almond ...... 0.1 Peanut, hay ...... 0.1 Almond, hulls ...... 0 .5 Apple ...... 2.0 Safflower, seed ...... 0 .1 Apricot ...... 15 .0 Sorghum, grain, forage ...... 0.1 Banana ...... 2.0 Sorghum, grain, grain ...... 0 .1 Bean, dry, seed ...... 0 .2 Tomato ...... 0.15 Bean, snap, succulent ...... 2 .0 Vegetable, foliage of legume, group 7 ...... 0 .1 Beet, sugar, roots ...... 0 .2 Vegetable, legume, group 6 ...... 0 .1 Cherry, sweet ...... 20 .0 Wheat, forage ...... 0 .1 Cherry, tart ...... 20.0 Wheat, grain ...... 0 .1 Grain, aspirated fractions ...... 12 Wheat, straw ...... 0 .1 Grape ...... 5 .0 Onion, bulb ...... 0 .5 Onion, green ...... 3 .0 (b) Section 18 emergency exemptions. Peach ...... 3 .0 [Reserved] Peanut ...... 0 .1 (c) Tolerances with regional registra- Peanut, hay ...... 5.0 Pear ...... 3 .0 tions. [Reserved] Pecan ...... 0 .1 (d) Indirect or inadvertent residues. Pistachio ...... 0.1 [Reserved] Plum ...... 0 .5 Potato ...... 0 .1 [47 FR 49845, Nov. 3, 1982, as amended at 48 Soybean, hulls ...... 1 .5 FR 12088, Mar. 23, 1983; 63 FR 57076, Oct. 26, Soybean, seed ...... 0 .2 1998; 72 FR 41931, Aug. 1, 2007; 73 FR 54961, Strawberry ...... 7 .0 Vegetable, cucurbit, group 9 ...... 1.0 Sept. 24, 2008] Wheat, forage ...... 1 .1 Wheat, grain ...... 0 .1 EFFECTIVE DATE NOTE: At 81 FR 34905, June Wheat, hay ...... 0 .1 1, 2016, § 180.370 was amended by revising the Wheat, straw ...... 0 .1 table in paragraph (a), effective Nov. 28, 2016. For the convenience of the user, the revised (b) Section 18 emergency exemptions. text is set forth as follows: [Reserved] § 180.370 5-Ethoxy-3-(trichloromethyl)-1,2,4- (c) Tolerances with regional registra- thiadiazole; tolerances for residues. tions. A tolerance with a regional reg- (a) * * * istration is established for residues of

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thiophanate-methyl, dimethyl ((1,2- Commodity Parts per phenylene) bis(iminocarbonothioyl)) million bis(carbamate), including its metabo- Artichoke, globe ...... 6.0 lites and degradates, in or on the com- Cattle, fat ...... 0.05 modity in the following table. Compli- Cattle, meat ...... 0 .05 Cottonseed subgroup 20C ...... 0 .20 ance with the tolerance level specified Egg ...... 0 .07 in this paragraph is to be determined Goat, fat ...... 0 .05 by measuring only the sum of Goat, meat ...... 0.05 Hog, fat ...... 0 .05 thiophanate-methyl, dimethyl ((1,2- Hog, meat ...... 0 .05 phenylene) bis (iminocarbonothioyl)) Horse, fat ...... 0 .05 bis(carbamate), and its metabolite, Horse, meat ...... 0 .05 methyl 2-benzimidazoyl carbamate Milk ...... 0.05 Mushroom ...... 0 .2 (MBC), calculated as the stoichio- Poultry, fat ...... 0.10 metric equivalent of thiophanate- Poultry, meat byproducts ...... 0.08 methyl, in or on the commodity. Poultry, meat ...... 0 .05 Sheep, fat ...... 0 .05 Sheep, meat ...... 0.05 Parts per Soybean ...... 0.05 Commodity million Soybean, hulls ...... 0 .5 Canola, seed ...... 0 .1 (2) Tolerances are established for res- (d) Indirect or inadvertent residues. idues of the insecticide diflubenzuron [Reserved] (N-[[(4-chlorophenyl)amino]carbonyl]- 2,6-difluorobenzamide), in or on the [75 FR 60244, Sept. 29, 2010] commodities in the table below. Com- pliance with the tolerance levels speci- § 180.372 2,6-Dimethyl-4- fied below is to be determined by meas- tridecylmorpholine; tolerances for uring only the sum of diflubenzuron (N- residues. [[(4-chlorophenyl)amino]carbonyl]-2,6- (a) General. A tolerance is established difluorobenzamide), 4- for residues of the fungicide 2,6-di- chlorophenylyurea and 4-chloroaniline, methyl-4-tridecylmorpholine in or on calculated as the stoichiometric equiv- the following food commodity: alent of diflubenzuron, in or on the commodity. Parts per Commodity million Parts per Commodity million Banana 1 ...... 1.0 Almond, hulls ...... 6 .0 1 There are no U.S. registrations. Barley, grain ...... 0 .06 (b) Section 18 emergency exemptions. Barley, hay ...... 3 .0 Barley, straw ...... 1 .8 [Reserved] Brassica, leafy greens, subgroup 5B ...... 9 .0 (c) Tolerances with regional registra- Carrot, roots ...... 0.20 tions. [Reserved] Cattle, meat byproducts ...... 0.15 Citrus, oil ...... 32 (d) Indirect or inadvertent residues. Fruit, citrus, group 10–10 ...... 3 .0 [Reserved] Goat, meat byproducts ...... 0 .15 Grain, aspirated fractions ...... 11 [73 FR 54961, Sept. 24, 2008] Grass, forage, fodder, and hay, group 17 ...... 6 .0 Hog, meat byproducts ...... 0 .15 § 180.373 [Reserved] Horse, meat byproducts ...... 0 .15 Oat, forage ...... 7 .0 Oat, grain ...... 0 .06 § 180.377 Diflubenzuron; tolerances for Oat, hay ...... 6.0 residues. Oat, straw ...... 3.5 Peanut ...... 0 .10 (a) General. (1) Tolerances are estab- Peanut, hay ...... 55 lished for residues of diflubenzuron, in- Peanut, refined oil ...... 0.20 cluding its metabolites and degradates, Peach subgroup 12–12B ...... 0.50 in or on the commodities in the table Pear ...... 0 .50 Pepper/Eggplant subgroup 8–10B ...... 1 .0 below. Compliance with the tolerance Plum Subgroup 12–12C ...... 0 .50 levels specified below is to be deter- Nut, tree, group 14–12 ...... 0 .20 mined by measuring only diflubenzuron Rice, grain ...... 0 .02 Sheep, meat byproducts ...... 0 .15 (N-[[(4-chlorophenyl)amino]carbonyl]- Turnip greens ...... 9 .0 2,6-difluorobenzamide). Wheat, forage ...... 7 .0

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Parts per EDITORIAL NOTE: For FEDERAL REGISTER ci- Commodity million tations affecting § 180.377, see the List of CFR Sections Affected, which appears in the Wheat, grain ...... 0 .06 Finding Aids section of the printed volume Wheat, hay ...... 6 .0 Wheat, straw ...... 3 .5 and at www.fdsys.gov.

(b) Section 18 emergency exemptions. § 180.378 Permethrin; tolerances for Time-limited tolerances are estab- residues. lished for residues of the insecticide (a) General. Tolerances are estab- diflubenzuron (N-[[(4- lished for the combined residues of the chlorophenyl)amino]carbonyl]-2,6- insecticide cis- and trans-permethrin difluorobenzamide) and its metabo- isomers [cis-(3-phenoxyphenyl)methyl lites, in connection with use of the pes- 3-(2,2-dichloroethenyl)-2,2- ticide under section 18 emergency ex- dimethylcyclopropane carboxylate] emptions granted by EPA. Compliance and [trans-(3-phenoxyphenyl)methyl 3- with the tolerance levels specified (2,2-dichloroethenyl)-2,2- below is to be determined by measuring dimethylcyclopropane carboxylate] in/ only the sum of diflubenzuron (N-[[(4- on the following food commodities: chlorophenyl)amino]carbonyl]-2,6- Parts per difluorobenzamide), 4- Commodity million chlorophenylyurea and 4-chloroaniline, Alfalfa, forage ...... 20 calculated as the stoichiometric equiv- Alfalfa, hay ...... 45 alent of diflubenzuron, in or on the Almond ...... 0.05 commodity. The tolerances are speci- Almond, hulls ...... 20 fied in the following table, and will ex- Artichoke, globe ...... 5.0 Asparagus ...... 2.0 pire and are revoked on the dates speci- Avocado ...... 1 .0 fied. Broccoli ...... 2 .0 Brussels sprouts ...... 1 .0 Cabbage ...... 6 .0 Parts per Expiration/ Commodity million revocation Cattle, fat ...... 1.5 date Cattle, meat ...... 0 .10 Cattle, meat byproducts ...... 0.10 Alfalfa, forage ...... 6.0 12/31/17 Cauliflower ...... 0 .5 Alfalfa, hay ...... 6.0 12/31/17 Cherry, sweet ...... 4 .0 Lemon ...... 0.8 12/31/10 Cherry, tart ...... 4 .0 Corn, field, forage ...... 50 (c) Tolerances with regional registra- Corn, field, grain ...... 0 .05 tions. Tolerances with regional reg- Corn, field, stover ...... 30 Corn, pop, grain ...... 0.05 istration are established for residues of Corn, pop, stover ...... 30 the insecticide diflubenzuron (N-[[(4- Corn, sweet, forage ...... 50 chlorophenyl)amino]carbonyl]-2,6- Corn, sweet, kernel plus cob with husks removed ...... 0 .10 difluorobenzamide), in or on the com- Corn, sweet, stover ...... 30 modities in the table below. Compli- Egg ...... 0 .10 ance with the tolerance levels specified Eggplant ...... 0.50 Fruit, pome, group 11 ...... 0.05 below is to be determined by measuring Garlic, bulb ...... 0.10 only the sum of diflubenzuron (N-[[(4- Grain, aspirated fractions ...... 0 .50 chlorophenyl)amino]carbonyl]-2,6- Goat, fat ...... 1 .5 difluorobenzamide), 4- Goat, meat ...... 0.10 Goat, meat byproducts ...... 0 .10 chlorophenylyurea and 4-chloroaniline, Hazelnut ...... 0 .05 calculated as the stoichiometric equiv- Hog, fat ...... 0 .05 alent of diflubenzuron, in or on the Hog, meat ...... 0 .05 Hog, meat byproducts ...... 0 .05 commodity. Horse, fat ...... 1 .5 Horse, meat ...... 0 .10 Parts per Horse, meat byproducts ...... 0 .10 Commodity million Horseradish ...... 0.50 Alfalfa, forage ...... 6.0 Kiwifruit ...... 2.0 Alfalfa, hay ...... 20 Leaf petioles subgroup 4B ...... 5 .0 Alfalfa, seed ...... 0 .90 Leafy greens subgroup 4A ...... 20 Lettuce, head ...... 20 Milk, fat (reflecting 0.88 ppm in whole milk) ...... 3 .0 (d) Indirect or inadvertent residues. Mushroom ...... 5 .0 [Reserved] Onion, bulb ...... 0 .10 Peach ...... 1 .0 [65 FR 33699, May 24, 2000] Pepper, bell ...... 0 .50

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Parts per Expiration/ Commodity million Commodity Parts per Revocation million Date Pistachio ...... 0.10 Potato ...... 0 .05 Cattle, fat ...... 0.05 11/30/08 Poultry, fat ...... 0.15 Cattle, meat ...... 0.05 11/30/08 Poultry, meat ...... 0 .05 Cattle, meat byproducts ...... 0.05 11/30/08 Poultry, meat byproducts ...... 0.05 Egg ...... 0.05 11/30/08 Sheep, fat ...... 1 .5 Goat, fat ...... 0.05 11/30/08 Sheep, meat ...... 0.10 Goat, meat ...... 0.05 11/30/08 Sheep, meat byproducts ...... 0 .10 Goat, meat byproducts ...... 0.05 11/30/08 Soybean, seed ...... 0 .05 Grape, wine ...... 6. 0 None Spinach ...... 20 Hog, fat ...... 0.05 11/30/08 Tomato ...... 2.0 Hog, meat ...... 0.05 11/30/08 Vegetable, cucurbit, group 9 ...... 1.5 Hog, meat byproducts ...... 0.05 11/30/08 Walnut ...... 0 .05 Horse, fat ...... 0.05 11/30/08 Watercress ...... 5 .0 Horse, meat ...... 0.05 11/30/08 Horse, meat byproducts ...... 0.05 11/30/08 Lettuce, head ...... 10.0 11/30/05 (b) Section 18 emergency exemptions. Lettuce, leaf ...... 10.0 11/30/05 [Reserved] Milk ...... 0.05 11/30/08 (c) Tolerances with regional registra- Poultry, fat ...... 0.1 11/30/08 tions. Tolerances with regional reg- Poultry, meat ...... 0.1 11/30/08 Poultry, meat byproducts ...... 0.1 11/30/08 istration, as defined in § 180.1(l) are es- Sheep, fat ...... 0.05 11/30/08 tablished for the combined residues of Sheep, meat ...... 0.05 11/30/08 the insecticide cis- and trans- Sheep, meat byproducts ...... 0.05 11/30/08 permethrin isomers [cis-(3- (b) Section 18 emergency exemptions. phenoxyphenyl)methyl 3-(2,2- [Reserved] dichloroethenyl)-2,2- (c) Tolerances with regional registra- dimethylcyclopropane carboxylate] tions. [Reserved] and [trans-(3-phenoxyphenyl)methyl 3- (d) Indirect or inadvertent residues. (2,2-dichloroethenyl)-2,2- [Reserved] dimethylcyclopropane carboxylate] in/ (e) Revoked tolerances subject to the on the following food commodities: channel of trade provisions. The following table lists commodities with Commodity Parts per million residues of vinclozolin resulting from Collards ...... 15 lawful use are subject to the channels Grass, forage ...... 15 of trade provisions of section 408(l)(5) Grass, hay ...... 15 of the FFDCA: Papaya ...... 1 .0 Turnip, tops ...... 10 Parts per Turnip, roots ...... 0 .20 Commodity million (d) Indirect or inadvertent residues. Cucumber ...... 1 .0 Fruit, stone, except plum, prune, fresh ...... 25.0 [Reserved] Pepper, bell ...... 3 .0 [72 FR 52019, Sept. 12, 2007] Strawberry ...... 10.0

§ 180.380 Vinclozolin; tolerances for [62 FR 38474, July 18, 1997, as amended at 63 residues. FR 7308, Feb. 13, 1998; 65 FR 44468, July 18, (a) General. Tolerances are estab- 2000; 67 FR 40189, June 12, 2002; 68 FR 56189, lished for the combined residues of the Sept. 30, 2003; 68 FR 69323, Dec. 12, 2003; 70 FR 55268, Sept. 21, 2005] fungicide vinclozolin (3-(3,5- dichlorophenyl)-5-ethenyl-5-methyl-2,4- § 180.381 Oxyfluorfen; tolerances for oxazolidinedione) and its metabolites residues. containing the 3,5-dichloroaniline moi- (a) General. Tolerances are estab- ety in or on the food commodities in lished for residues of the herbicide the table below. There are no U.S. reg- oxyfluorfen [2-chloro-1-(3-ethoxy-4- istrations for grape (wine) as of July nitrophenoxy)-4- 30, 1997. (trifluoromethyl)benzene] in or on the following food commodities: Parts per Expiration/ Commodity million Revocation Date Parts per Commodity million Bean, succulent ...... 2.0 11/30/05 Canola, seed ...... 1.0 11/30/08 Almond, hulls ...... 0 .1

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(d) Indirect or inadvertent residues. Commodity Parts per million [Reserved] Artichoke, globe ...... 0.05 [45 FR 85022, Dec. 24, 1980] Avocado ...... 0 .05 Banana ...... 0.05 EDITORIAL NOTE: For FEDERAL REGISTER ci- Broccoli ...... 0 .05 tations affecting § 180.381, see the List of CFR Cabbage ...... 0 .05 Sections Affected, which appears in the Cacao bean, dried bean ...... 0 .05 Cattle, fat ...... 0.01 Finding Aids section of the printed volume Cattle, meat ...... 0 .01 and at www.fdsys.gov. Cattle, meat byproducts ...... 0.01 Cauliflower ...... 0 .05 § 180.383 Sodium salt of acifluorfen; Coffee, bean, green ...... 0 .05 tolerances for residues. Corn, field, grain ...... 0 .05 Cotton, undelinted seed ...... 0 .05 (a) General. Tolerances are estab- Date, dried fruit ...... 0 .05 lished for combined residues of the her- Egg ...... 0 .03 Feijoa ...... 0 .05 bicide sodium salt of acifluorfen, so- Fig ...... 0 .05 dium 5-[2-chloro-4- Fruit, pome, group 11 ...... 0.05 (trifluoromethyl)phenoxy]-2- Fruit, stone, group 12 ...... 0 .05 Goat, fat ...... 0 .01 nitrobenzoate, and its metabolites (the Goat, meat ...... 0.01 corresponding acid, methyl ester, and Goat, meat byproducts ...... 0 .01 amino analogues) in or on the fol- Grape ...... 0 .05 Hog, fat ...... 0 .01 lowing raw agricultural commodities: Hog, meat ...... 0 .01 Hog, meat byproducts ...... 0 .01 Commodity Parts per Horse, fat ...... 0 .01 million Horse, meat ...... 0 .01 Horse, meat byproducts ...... 0 .01 Peanut ...... 0 .1 Horseradish ...... 0.05 Rice, grain ...... 0 .1 Kiwifruit ...... 0.05 Soybean, seed ...... 0 .1 Milk ...... 0.01 Strawberry ...... 0 .05 Nut, tree, group 14 ...... 0 .05 Olive ...... 0 .05 (b) Section 18 emergency exemptions. Onion, bulb ...... 0 .05 [Reserved] Peppermint, tops ...... 0 .05 Persimmon ...... 0 .05 (c) Tolerances with regional restric- Pistachio ...... 0.05 tions. [Reserved] Pomegranate ...... 0 .05 (d) Indirect or inadvertent residues. Poultry, fat ...... 0.2 Poultry, meat ...... 0 .01 [Reserved] Poultry, meat byproducts ...... 0.01 Sheep, fat ...... 0 .01 [45 FR 24877, Apr. 11, 1980, as amended at 46 Sheep, meat ...... 0.01 FR 61272, Dec. 16, 1981; 47 FR 39490, Sept. 8, Sheep, meat byproducts ...... 0 .01 1982; 61 FR 30165, June 14, 1996; 62 FR 39974, Soybean ...... 0.05 July 25, 1997; 67 FR 35048, May 17, 2002; 69 FR Spearmint, tops ...... 0 .05 6567, Feb. 11, 2004; 71 FR 54434, Sept. 15, 2006; 80 FR 72598, Nov. 20, 2015] (b) Section 18 emergency exemptions. [Reserved] § 180.384 Mepiquat (N,N-dimethylpip- (c) Tolerances with regional registra- eridinium); tolerances for residues. tions. Tolerances with regional reg- (a) General. Tolerances are estab- istration are established for residues of lished for residues of the plant growth the herbicide oxyfluorfen [2-chloro-1-(3- regulator mepiquat, including its me- ethoxy-4-nitrophenoxy)-4- tabolites and degradates, in or on the (trifluoromethyl)benzene] in or on the commodities in the table in this para- following food commodities: graph. Compliance with the tolerance Parts per levels specified in this paragraph is to Commodity million be determined by measuring only mepiquat, N,N-dimethylpiperidinium, Blackberry ...... 0 .05 Chickpea, seed ...... 0 .05 in or on the commodity. Grass, forage ...... 0 .05 Grass, hay ...... 0 .05 Commodity Parts Grass, seed screenings ...... 0 .05 per million Guava ...... 0 .05 Papaya ...... 0 .05 Cattle, meat byproducts ...... 0.1 Raspberry ...... 0 .05 Cotton, gin byproducts ...... 6 .0 Taro, corm ...... 0 .05 Cotton, undelinted seed ...... 2 .0 Taro, leaves ...... 0 .05 Goat, meat byproducts ...... 0 .1 Grape ...... 1 .0

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N-(5-(1,1-dimethylethyl)-1,3,4- Commodity Parts per million thiadiazol-2-yl)-N’-hydroxymethyl-N- Grape, raisin ...... 5 .0 methylurea in or on the following raw Hog, meat byproducts ...... 0 .1 agricultural commodities: Horse, meat byproducts ...... 0 .1 Sheep, meat byproducts ...... 0 .1 Parts per Commodity million (b) Section 18 emergency exemptions. Grass, forage ...... 10 .0 [Reserved] Grass, hay ...... 10 .0 (c) Tolerances with regional registrations. [Reserved] (2) Tolerances are established for the (d) Indirect or inadvertent residues. combined residues of the herbicide [Reserved] tebuthiuron (N-(5-(1,1-dimethylethyl)- [67 FR 3118, Jan. 23, 2002, as amended at 80 1,3,4-thiadiazol-2-yl)-N,N’- FR 72598, Nov. 20, 2015] dimethylurea) and its metabolites N-(5- (1,1-dimethylethyl)-1,3,4-thiadiazol-2- § 180.385 Diclofop-methyl; tolerances yl)-N-methylurea, N-(5-(1,1- for residues. dimethylethyl)-1,3,4-thiadiazol-2- (a) General. Tolerances are estab- yl)urea, 2-dimethylethyl-5-amino-1,3,4- lished for the combined residues of the thiadiazole, and N-(5-(1,1- herbicide diclofop-methyl (methyl 2-[4- dimethylethyl)-1,3,4-thiadiazol-2-yl)-N’- (2,4- hydroxymethyl-N-methylurea in or on dichlorophenoxy)phenoxy]propanoate) the following raw agricultural com- and its metabolites, 2-[4-(2,4- modities: dichlorophenoxy)phenoxy]propanoic Parts per acid and 2-[4-(2,4-dichloro-5- Commodity million hydroxyphenoxy)phenoxy]propanoic acid, in or on the following raw agri- Cattle, fat ...... 1.0 Cattle, meat ...... 1 .0 cultural commodities: Cattle, meat byproducts ...... 5.0 Goat, fat ...... 1 .0 Commodity Parts per Goat, meat ...... 1.0 million Goat, meat byproducts ...... 5 .0 Horse, fat ...... 1 .0 Barley, grain ...... 0 .1 Horse, meat ...... 1 .0 Barley, straw ...... 0 .1 Horse, meat byproducts ...... 5 .0 Wheat, grain ...... 0 .1 Sheep, fat ...... 1 .0 Wheat, straw ...... 0 .1 Sheep, meat ...... 1.0 Sheep, meat byproducts ...... 5 .0 (b) Section 18 emergency exemptions. [Reserved] (3) A tolerance is established for the (c) Tolerances with regional registra- combined residues of the herbicide tions. [Reserved] tebuthiuron (N-(5-(1,1-dimethylethyl)- (d) Indirect or inadvertent residues. 1,3,4-thiadiazol-2-yl)-N,N’- [Reserved] dimethylurea) and its metabolites N-(5- [45 FR 23425, Apr. 7, 1980, as amended at 50 (1,1-dimethylethyl)-1,3,4-thiadiazol-2- FR 20211, May 15, 1985; 51 FR 3599, Jan. 29, yl)-N-methylurea, N-(5-(2-hydroxy-1,1- 1986; 51 FR 19176, May 28, 1986; 63 FR 57077, dimethylethyl)-1,3,4-thiadiazol-2-yl)-N- Oct. 26, 1998; 72 FR 41931, Aug. 1, 2007] methylurea, N-(5-(1,1-dimethylethyl)- 1,3,4-thiadiazol-2-yl)urea, N-(5-(1,1- §§ 180.388–180.389 [Reserved] dimethylethyl)-1,3,4-thiadiazol-2-yl)-N’- hydroxymethyl-N-methylurea, and N- § 180.390 Tebuthiuron; tolerances for residues. (5-(2-hydroxy-1,1-dimethylethyl)-1,3,4- thiadiazol-2-yl)-N’-hydroxymethyl-N- (a) General. (1) Tolerances are estab- methylurea in or on the following raw lished for the combined residues of the agricultural commodities: herbicide tebuthiuron (N-(5-(1,1- dimethylethyl)-1,3,4-thiadiazol-2-yl)- Commodity Parts per N,N’-dimethylurea) and its metabolites million N-(5-(2-hydroxy-1,1-dimethylethyl)- Milk ...... 0.8 1,3,4-thiadiazol-2-yl)-N,N’- dimethylurea, N-(5-(1,1-dimethylethyl)- (b) Section 18 emergency exemptions. 1,3,4-thiadiazol-2-yl)-N-methylurea, and [Reserved]

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(c) Tolerances with regional registra- cyclohexyl-1-methyl-1,3,5-triazine-2,4,6- tions. [Reserved] (1H, 3H, 5H)-trione, and metabolite E, (d) Indirect or inadvertent residues. 3-(4-hydroxycyclohexyl)-1-methyl-1,3,5- [Reserved] triazine-2,4,6-(1H, 3H, 5H)-trione, cal- [72 FR 53461, Sept. 19, 2007] culated as the stoichiometric equivalent of hexazinone, in or on the com- § 180.395 Hydramethylnon; tolerances modity. for residues. Parts per (a) General. Tolerances are estab- Commodity million lished for residues of the insecticide Alfalfa, forage ...... 2.0 tetrahydro-5,5-dimethyl-2(1H)- Alfalfa, hay ...... 4.0 pyrimidinone(3-(4- Alfalfa, seed ...... 2 .0 (trifluoromethyl)phenyl)-1-(2-(4- Blueberry ...... 0 .6 (trifluoromethyl)phenyl)ethenyl)-2- Grass, forage ...... 250 Grass, hay ...... 230 propenylidene)hydrazone in or on the Pineapple ...... 0.6 following raw agricultural commod- Sugarcane, cane ...... 0.6 ities: Sugarcane, molasses ...... 4 .0

Parts per (2) Tolerances are established for res- Commodity million idues of the herbicide hexazinone, 3- Grass, forage ...... 2 .0 cyclohexyl-6-(dimethylamino)-1-meth- Grass, hay ...... 2 .0 Pineapple ...... 0.05 yl-1,3,5-triazine-2,4-(1H, 3H)-dione, including its metabolites and degradates, (b) Section 18 emergency exemptions. in or on the commodities in the fol- [Reserved] lowing table. Compliance with the tol- (c) Tolerances with regional registra- erance levels specified in this para- tions. [Reserved] graph is to be determined by measuring (d) Indirect or inadvertent residues. only the sum of hexazinone, 3- [Reserved] cyclohexyl-6-(dimethylamino)-1-methyl-1,3,5-triazine-2,4-(1H, 3H)-dione, and [45 FR 55198, Aug. 19, 1980, as amended at 63 its animal tissue metabolites: metabo- FR 10543, Mar. 4, 1998; 63 FR 65073, Nov. 25, 1998; 66 FR 28672, May 24, 2001; 68 FR 37764, lite B, 3-cyclohexyl-6-(methylamino)-1- June 25, 2003; 68 FR 48312, Aug. 13, 2003; 72 FR methyl-1,3,5-triazine-2,4-(1H, 3H)-dione, 41931, Aug. 1, 2007] and metabolite F, 3-cyclohexyl-6- amino-1-methyl-1,3,5-triazine-2,4-(1H, § 180.396 Hexazinone; tolerances for 3H)-dione, calculated as the stoichio- residues. metric equivalent of hexazinone, in or (a) General. (1) Tolerances are estab- on the commodity. lished for residues of the herbicide Parts per hexazinone, 3-cyclohexyl-6- Commodity million (dimethylamino)-1-methyl-1,3,5-triazine-2,4-(1H, 3H)-dione, including its Cattle, fat ...... 0.1 metabolites and degradates, in or on Cattle, meat ...... 0 .5 Cattle, meat byproducts ...... 4.0 the commodities in the following table. Goat, fat ...... 0 .1 Compliance with the tolerance levels Goat, meat ...... 0.5 specified in this paragraph is to be de- Goat, meat byproducts ...... 4 .0 termined by measuring only the sum of Hog, fat ...... 0 .1 Hog, meat ...... 0 .5 hexazinone, 3-cyclohexyl-6- Hog, meat byproducts ...... 4 .0 (dimethylamino)-1-methyl-1,3,5-tri- Horse, fat ...... 0 .1 azine-2,4-(1H, 3H)-dione, and its plant Horse, meat ...... 0 .5 metabolites: metabolite A, 3-(4- Horse, meat byproducts ...... 4 .0 Sheep, fat ...... 0 .1 hydroxycyclohexyl)-6- Sheep, meat ...... 0.5 (dimethylamino)-1-methyl-1,3,5-tri- Sheep, meat byproducts ...... 4 .0 azine-2,4-(1H, 3H)-dione, metabolite B, 3-cyclohexyl-6-(methylamino)-1-meth- (3) A tolerance is established for resi- yl-1,3,5-triazine-2,4-(1H, 3H)-dione, me- dues of the herbicide hexazinone, 3- tabolite C, 3-(4-hydroxycyclohexyl)-6- cyclohexyl-6-(dimethylamino)-1-meth- (methylamino)-1-methyl-1,3,5-triazine- yl-1,3,5-triazine-2,4-(1H, 3H)-dione, in- 2,4-(1H, 3H)-dione, metabolite D, 3- cluding its metabolites and degradates,

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in or on the commodity in the fol- Commodity Parts per lowing table. Compliance with the tol- million erance level specified in this paragraph Cherry, sweet, postharvest ...... 20 .0 is to be determined by measuring only Cherry, tart ...... 20.0 the sum of hexazinone, 3-cyclohexyl-6- Cotton, undelinted seed ...... 0 .10 Cowpea, hay ...... 90 .0 (dimethylamino)-1-methyl-1,3,5-tri- Currant ...... 15.0 azine-2,4-(1H, 3H)-dione, and its me- Garlic ...... 0 .1 tabolites: metabolite B, 3-cyclohexyl-6- Ginseng ...... 2 .0 Ginseng, dried root ...... 4 .0 (methylamino)-1-methyl-1,3,5-triazine- Grape ...... 60 .0 2,4-(1H, 3H)-dione, metabolite C, 3-(4- Grape, raisin ...... 300 hydroxycyclohexyl)-6-(methylamino)-1- Kiwifruit ...... 10.0 methyl-1,3,5-triazine-2,4-(1H, 3H)-dione, Lettuce ...... 25.0 Nectarine, postharvest ...... 20.0 metabolite C-2, 3-(3- Onion, bulb ...... 0 .5 hydroxycyclohexyl)-6-(methylamino)-1- Peach, postharvest ...... 20.0 methyl-1,3,5-triazine-2,4-(1H, 3H)-dione, Peanut ...... 0 .5 Peanut, hay ...... 150.0 and metabolite F, 3-cyclohexyl-6- Plum, postharvest ...... 20 .0 amino-1-methyl-1,3,5-triazine-2,4-(1H, Plum, prune ...... 20.0 3H)-dione, calculated as the stoichio- Potato ...... 0 .5 Raspberry ...... 15 .0 metric equivalent of hexazinone, in or Rice, bran ...... 30.0 on the commodity. Rice, grain ...... 10 .0 Rice, hulls ...... 50 .0 Parts per Strawberry ...... 15.0 Commodity million

Milk ...... 11 (2) Tolerances are established for the combined residues of iprodione [3-(3,5- (b) Section 18 emergency exemptions. dichlorophenyl)-N-(1-methylethyl)-2,4- [Reserved] dioxo-1-imidazolidinecarboxamide], its (c) Tolerances with regional registra- isomer [3-(1-methylethyl)-N-(3,5- tions. [Reserved] dichlorophenyl)-2,4-dioxo-1- (d) Indirect or inadvertent residues. imidazolidinecarboxamide, and its me- [Reserved] tabolites [3-(3,5-dichlorophenyl)-2,4- [65 FR 33713, May 24, 2000, as amended at 71 dioxo-1-imidazolidine-carboxamide] FR 56399, Sept. 27, 2006; 75 FR 60244, Sept. 29, and [N-(3,5-dichloro-4-hydroxyphenyl)- 2010] ureido-carboxamide], all expressed as iprodione equivalents in or on the fol- § 180.399 Iprodione; tolerances for res- lowing food commodities of animal ori- idues. gin: (a) General. (1) Tolerances are estab- Parts per lished for the combined residues of the Commodity million fungicide iprodione [3-(3,5- dichlorophenyl)-N-(1-methylethyl)-2,4- Cattle, fat ...... 0.5 Cattle, kidney ...... 3 .0 dioxo-1-imidazolidinecarboxamide], its Cattle, liver ...... 3 .0 isomer 3-(1-methylethyl)-N-(3,5- Cattle, meat ...... 0 .5 dichlorophenyl)-2,4-dioxo-1- Cattle, meat byproducts, except kidney and liver 0.5 Egg ...... 1 .5 imidazolidinecarboxamide, and its me- Goat, fat ...... 0 .5 tabolite 3-(3,5-dichlorophenyl)-2,4- Goat, kidney ...... 3 .0 dioxo-1-imidazolidine-carboxamide in Goat, liver ...... 3.0 or on the following food commodities: Goat, meat ...... 0.5 Goat, meat byproducts, except kidney and liver 0 .5 Hog, fat ...... 0 .5 Parts per Commodity million Hog, kidney ...... 3.0 Hog, liver ...... 3 .0 Almond, hulls ...... 2 .0 Hog, meat ...... 0 .5 Almond ...... 0.3 Hog, meat byproducts, except kidney and liver .. 0 .5 Apricot ...... 20 .0 Horse, fat ...... 0 .5 Bean, dry, seed ...... 2 .0 Horse, kidney ...... 3 .0 Bean, forage ...... 90 .0 Horse, liver ...... 3 .0 Bean, succulent ...... 2 .0 Horse, meat ...... 0 .5 Blueberry ...... 15 .0 Horse, meat byproducts, except kidney and liver 0 .5 Boysenberry ...... 15 .0 Milk ...... 0.5 Broccoli ...... 25 .0 Poultry, fat ...... 3.5 Caneberry subgroup 13A ...... 25 .0 Poultry, liver ...... 5 .0 Carrot, roots ...... 5.0 Poultry, meat ...... 1 .0

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Parts per Part per Commodity million Commodity million

Poultry, meat byproducts, except liver ...... 1 .0 Horse, meat byproducts ...... 0 .2 Sheep, fat ...... 0 .5 Horse, meat ...... 0 .2 Sheep, kidney ...... 3.0 Milk ...... 0.05 Sheep, liver ...... 3.0 Poultry, fat ...... 0.2 Sheep, meat ...... 0.5 Poultry, meat byproducts ...... 0.2 Sheep, meat byproducts, except kidney and Poultry, meat ...... 0 .2 liver ...... 0 .5 Rice, grain ...... 0 .2 Sheep, fat ...... 0 .2 Sheep, meat byproducts ...... 0 .2 (b) Section 18 emergency exemptions. Sheep, meat ...... 0.2 [Reserved] (c) Tolerances with regional registra- (b) Section 18 emergency exemptions. tions. Tolerances with regional reg- [Reserved] istration, as defined in § 180.1(l), are es- (c) Tolerances with regional registra- tablished for the combined residues of tions. Tolerances with regional reg- the fungicide iprodione [3-(3,5- istration, as defined in § 180.1(l), are es- dichlorophenyl)-N-(1-methylethyl)-2,4- tablished for residues of the herbicide dioxo-1-imidazolidinecarboxamide], its thiobencarb (S-[(4-chloro- isomer [3-(1-methylethyl)-N-(3,5- phenyl)methyl]diethylcarbamothioate) dichlorophenyl)-2,4-dioxo-1- and its chlorobenzyl and chlorophenyl imidazolidinecarboxamide], and its me- moiety-containing metabolites in or on tabolite [3-(3,5-dichlorophenyl)-2,4- the following raw agricultural com- dioxo-1-imidazolidinecarboxamide] in modities: or on the following food commodity: Commodity Parts per Parts per million Commodity million Celery ...... 0 .2 Mustard greens ...... 15.0 Endive ...... 0.2 Lettuce ...... 0.2 (d) Indirect or inadvertent residues. [Reserved] (d) Indirect or inadvertent residues. [Reserved] [48 FR 40385, Sept. 7, 1983] [47 FR 6833, Feb. 17, 1982, as amended at 56 EDITORIAL NOTE: For FEDERAL REGISTER ci- FR 2440, Jan. 23, 1991; 76 FR 34885, June 15, tations affecting § 180.399, see the List of CFR 2011; 80 FR 72599, Nov. 20, 2015] Sections Affected, which appears in the Finding Aids section of the printed volume § 180.403 Thidiazuron; tolerances for and at www.fdsys.gov. residues. § 180.401 Thiobencarb; tolerances for (a) General. Tolerances are estab- residues. lished for the combined residues of the defoliant thidiazuron (N-phenyl-N-1,2,3- (a) General. Tolerances are estab- thiadiazol-5-ylurea) and its aniline con- lished for the combined residues of the taining metabolites in or on the fol- herbicide thiobencarb (S-[(4- lowing food commodities: chlorophenyl)methyl]diethylcarbamothioate) and its chlorobenzyl Commodity Parts per and chlorophenyl moiety-containing million metabolites in or on the following raw Cattle, fat ...... 0.4 agricultural commodities: Cattle, meat ...... 0 .4 Cattle, meat byproducts ...... 0.4 Part per Cotton, gin byproducts ...... 24 .0 Commodity million Cotton, undelinted seed ...... 0 .3 Goat, fat ...... 0 .4 Cattle, fat ...... 0.2 Goat, meat ...... 0.4 Cattle, meat byproducts ...... 0.2 Goat, meat byproducts ...... 0 .4 Cattle, meat ...... 0 .2 Hog, fat ...... 0 .4 Egg ...... 0 .2 Hog, meat ...... 0 .4 Goat, fat ...... 0 .2 Hog, meat byproducts ...... 0 .4 Goat, meat byproducts ...... 0 .2 Horse, fat ...... 0 .4 Goat, meat ...... 0.2 Horse, meat ...... 0 .4 Hog, fat ...... 0 .2 Horse, meat byproducts ...... 0 .4 Hog, meat byproducts ...... 0 .2 Milk ...... 0.05 Hog, meat ...... 0 .2 Sheep, fat ...... 0 .4 Horse, fat ...... 0 .2 Sheep, meat ...... 0.4

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Parts per Parts per Commodity million Commodity million

Sheep, meat byproducts ...... 0 .4 Barley, grain ...... 0 .1 Barley, straw ...... 0 .5 (b) Section 18 emergency exemptions. Oat, forage ...... 20 .0 [Reserved] Oat, grain ...... 0 .1 (c) Tolerances with regional registra- Oat, straw ...... 0.5 tions. [Reserved] Wheat, forage ...... 20.0 Wheat, grain ...... 0 .1 (d) Indirect or inadvertent residues. Wheat, straw ...... 0 .5 [Reserved] [65 FR 33700, May 24, 2000, as amended at 72 (2) Tolerances are established for res- FR 53462, Sept. 19, 2007] idues of chlorsulfuron (2-chloro-N-[(4- methoxy-6-methyl-1,3,5-triazin-2- § 180.404 Profenofos; tolerances for yl)aminocarbonyl] residues. benzenesulfonamide) in or on the fol- (a) General. Tolerances are estab- lowing raw agricultural commodities. lished for residues of the insecticide profenofos (O-(4-bromo-2- Parts per Commodity million chlorophenyl)-O-ethyl-S-propyl phosphorothioate) in or on the fol- Cattle, fat ...... 0.3 lowing food commodities: Cattle, meat ...... 0 .3 Cattle, meat byproducts ...... 0.3 Goat, fat ...... 0 .3 Commodity Parts per million Goat, meat ...... 0.3 Goat, meat byproducts ...... 0 .3 Cattle, fat ...... 0.05 Cattle, meat ...... 0 .05 Grass, forage ...... 11 .0 Cattle, meat byproducts ...... 0.05 Grass, hay ...... 19 .0 Cotton, gin byproducts ...... 55 .0 Hog, fat ...... 0 .3 Cotton, undelinted seed ...... 2 .0 Hog, meat ...... 0 .3 Goat, fat ...... 0 .05 Hog, meat byproducts ...... 0 .3 Goat, meat ...... 0.05 Horse, fat ...... 0 .3 Goat, meat byproducts ...... 0 .05 Horse, meat ...... 0 .3 Horse, fat ...... 0 .05 Horse, meat byproducts ...... 0 .3 Horse, meat ...... 0 .05 Horse, meat byproducts ...... 0 .05 Milk ...... 0.1 Milk ...... 0.01 Sheep, fat ...... 0 .3 Sheep, fat ...... 0 .05 Sheep, meat ...... 0.3 Sheep, meat ...... 0.05 Sheep, meat byproducts ...... 0 .3 Sheep, meat byproducts ...... 0 .05 (b) Section 18 emergency exemptions. (b) Section 18 emergency exemptions. [Reserved] [Reserved] (c) Tolerances with regional registra- (c) Tolerances with regional registrations. [Reserved] tions. [Reserved] (d) Indirect or inadvertent residues. (d) Indirect or inadvertent residues. [Reserved] [Reserved] [67 FR 52873, Aug. 14, 2002] [65 FR 33700, May 24, 2000, as amended at 66 FR 50833, Oct. 5, 2001; 67 FR 49617, July 31, 2002; 72 FR 54579, Sept. 26, 2007] § 180.407 Thiodicarb; tolerances for residues. § 180.405 Chlorsulfuron; tolerances for (a) General. Tolerances are estab- residues. lished for the combined residues of the (a) General. (1) Tolerances are estab- insecticide thiodicarb (dimethyl N,N′- lished for the combined residues of [thiobis[[(methylimino)carbonyloxy]] chlorsulfuron (2-chloro-N-[(4-methoxy- bis[ethanimidothioate]) and its me- 6-methyl-1,3,5-triazin-2- tabolite methomyl (S-methyl N- yl)aminocarbonyl]benzenesulfonamide) [(methylcarbamoyl) and its metabolite, 2-chloro-5-hydroxy- oxy]thioacetimidate) in or on the fol- N-[(4-methoxy-6-methyl-1,3,5-triazin-2- lowing food commodities or groups. yl)aminocarbonyl] benzenesulfonamide The time-limited tolerances expire and in or on the following raw agricultural are revoked on the dates listed in the commodities: following table:

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Expiration/ Parts per Commodity Parts per revocation Commodity million million date Clover, forage ...... 1.0 Broccoli ...... 7.0 None Clover, hay ...... 2.5 Cabbage ...... 7.0 None Cotton, undelinted seed ...... 0 .1 Cauliflower ...... 7.0 None Cranberry ...... 4 .0 Corn, sweet, kernel plus cob with Egg ...... 0 .05 husks removed ...... 2.0 None Fruit, citrus ...... 1 .0 Cotton, undelinted seed ...... 0.4 None Fruit, stone, group 12 ...... 1 .0 Soybean, hulls ...... 0.8 None Ginseng ...... 3 .0 Soybean ...... 0.2 None Goat, fat ...... 0 .4 Vegetable, leafy, except brassica, Goat, kidney ...... 0 .4 group 4 ...... 35 None Goat, liver ...... 0.4 Goat, meat ...... 0.05 (b) Section 18 emergency exemptions. Goat, meat byproducts, except kidney and liver 0 .05 [Reserved] Grain, cereal, group 15, except barley, oat and wheat ...... 0.1 (c) Tolerances with regional registra- Grain, crop ...... 0 .1 tions. [Reserved] Grape ...... 2 .0 (d) Indirect or inadvertent residues. Grape, raisin ...... 6 .0 [Reserved] Grass, forage ...... 10 .0 Grass, hay ...... 25 .0 [62 FR 44595, Aug. 22, 1997, as amended at 75 Hog, fat ...... 0 .4 FR 60245, Sept. 29, 2010] Hog, kidney ...... 0.4 Hog, liver ...... 0 .4 Hog, meat ...... 0 .05 § 180.408 Metalaxyl; tolerances for res- Hog, meat byproducts, except kidney and liver .. 0 .05 idues. Hop, dried cones ...... 20 (a) General. Tolerances are estab- Hop, vines ...... 2 .0 Horse, fat ...... 0 .4 lished for the combined residues of the Horse, kidney ...... 0 .4 fungicide metalaxyl [N-(2,6- Horse, liver ...... 0 .4 dmethylphyenyl)-N-(methoxyacetyl) Horse, meat ...... 0 .05 alanine methylester] and its metabo- Horse, meat byproducts, except kidney and liver 0 .05 Lettuce, head ...... 5.0 lites containing the 2,6- Milk ...... 0.02 dimethylaniline moiety, and N-(2-hy- Mustard greens ...... 5.0 droxy methyl-6-methylphenyl)-N- Onion, bulb ...... 3 .0 (methoxyacetyl)-alanine methyl ester, Onion, green ...... 10.0 Peanut ...... 0 .2 each expressed as metalaxyl equiva- Peanut, hay ...... 20.0 lents, in or on the following food com- Peanut, meal ...... 1 .0 modities: Peanut, hulls ...... 2 .0 Pineapple ...... 0.1 Parts per Pineapple, fodder ...... 0 .1 Commodity million Pineapple, forage ...... 0 .1 Plum, prune, dried ...... 4.0 Alfalfa, forage ...... 6.0 Potato, chips ...... 4 .0 Alfalfa, hay ...... 20.0 Potato, granules, flakes ...... 4.0 Almond ...... 0.5 Potato, processed potato waste ...... 4 .0 Almond, hulls ...... 10 .0 Potato, wet peel ...... 4 .0 Apple ...... 0.2 Poultry, fat ...... 0.4 Apple, wet pomace ...... 0 .4 Poultry, kidney ...... 0 .4 Apricot, dried ...... 4 .0 Poultry, liver ...... 0 .4 Asparagus ...... 7.0 Poultry, meat ...... 0 .05 Avocado ...... 4 .0 Poultry, meat byproducts, except kidney and Beet, garden, roots ...... 0 .1 liver ...... 0 .05 Beet, garden, tops ...... 0 .1 Potato ...... 0 .5 Beet, sugar ...... 0 .1 Raspberry ...... 0 .5 Beet, sugar, molasses ...... 1 .0 Sheep, fat ...... 0 .4 Beet, sugar, roots ...... 0 .5 Sheep, kidney ...... 0.4 Beet, sugar, tops ...... 10.0 Sheep, liver ...... 0.4 Blueberry ...... 2 .0 Sheep, meat ...... 0.05 Broccoli ...... 2 .0 Sheep, meat byproducts, except kidney and Brussels sprouts ...... 2 .0 liver ...... 0 .05 Cabbage ...... 1 .0 Soybean, hulls ...... 2 .0 Cattle, fat ...... 0.4 Soybean, meal ...... 2.0 Cattle, kidney ...... 0 .4 Soybean, seed ...... 1 .0 Cattle, liver ...... 0 .4 Spinach ...... 10 .0 Cattle, meat ...... 0 .05 Strawberry ...... 10.0 Cattle, meat byproducts, except kidney and liver 0.05 Sunflower, seed ...... 0.1 Cauliflower ...... 1 .0 Sunflower, forage ...... 0.1 Citrus, oil ...... 7.0 Tomato, paste ...... 3 .0 Citrus, dried pulp ...... 7 .0 Tomato, puree ...... 3 .0

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Parts per Part per Commodity million Commodity million

Vegetable, brassica, leafy, group 5, except broc- Wheat, forage ...... 2 .0 coli, cabbage, cauliflower, brussels sprouts, Wheat, germ ...... 1 .0 and mustard greens ...... 0 .1 Wheat, grain ...... 0 .2 Vegetable, cucurbit, group 9 ...... 1.0 Wheat, middlings ...... 1 .0 Vegetable, foilage of legume, group 7 ...... 8 .0 Wheat, shorts ...... 1 .0 Vegetable, fruiting, group 8 ...... 1.0 Wheat, straw ...... 2 .0 Vegetable, leafy, except brassica, group 4, except spinach ...... 5 .0 Vegetable, leaves of root and tuber, group 2 ..... 15 .0 [65 FR 33700, May 24, 2000, as amended at 72 Vegetable, legume, cannery waste ...... 5 .0 FR 35666, June 29, 2007; 74 FR 46374, Sept. 9, Vegetable, legume, group 6 ...... 0 .2 Vegetable, root and tuber, group 1 ...... 0 .5 2009; 75 FR 56015, Sept. 15, 2010] Walnut ...... 0 .5 § 180.409 Pirimiphos-methyl; toler- (b) Section 18 emergency exemptions. ances for residues. [Reserved] (a) General. Tolerances are estab- (c) Tolerances with regional registra- lished for residues of the insecticide tions. Tolerances with regional reg- pirimiphos-methyl (O-(2-diethylamino- istration (refer to § 180.1(m)) are estab- 6-methyl-4-pyrimidinyl) O,O-dimethyl lished for the combined residues of the phosphorothioate) in or on the fol- fungicide metalaxyl [N-(2,6- lowing raw agricultural commodities: dimethylphenyl)-N-(methoxyacetyl) alanine methyl ester] and its metabolites Parts per Commodity million containing the 2,6-dimethylaniline moiety, and N-(2-hydroxy methyl-6- Cattle, fat ...... 0.02 methyl)-N-(methoxyacetyl)-alanine Cattle, meat byproducts ...... 0.02 methylester, each expressed as Corn, field, grain ...... 8 .0 Corn, pop, grain ...... 8.0 metalaxyl, in or on the following raw Goat, fat ...... 0 .02 agricultural commodity: Goat, meat byproducts ...... 0 .02 Grain, aspirated fractions ...... 20.0 Commodity Parts per Hog, fat ...... 0 .02 million Hog, meat byproducts ...... 0 .02 Horse, fat ...... 0 .02 Papaya ...... 0 .1 Horse, meat byproducts ...... 0 .02 Poultry, fat ...... 0.02 (d) Indirect or inadvertent tolerances. Sheep, fat ...... 0 .02 Tolerances are established for indirect Sheep, meat byproducts ...... 0 .02 or inadvertent residues of metalaxyl in Sorghum, grain, grain ...... 8 .0 or on the food commodities when present therein as a result of the appli- (b) Section 18 emergency exemptions. cation of metalaxyl to growing crops [Reserved] listed in paragraph (a) of this section (c) Tolerances with regional registra- and other non-food crops to read as fol- tions. [Reserved] lows: (d) Indirect or inadvertent residues. [Reserved] Part per Commodity million [65 FR 33714, May 24, 2000, as amended at 67 FR 41807, June 19, 2002; 67 FR 49617, July 31, Barley, bran ...... 1 .0 2002; 70 FR 44492, Aug. 3, 2005; 72 FR 53462, Barley, flour ...... 1 .0 Sept. 19, 2007] Barley, grain ...... 0 .2 Barley, pearled barley ...... 1 .0 Barley, straw ...... 2 .0 § 180.410 Triadimefon; tolerances for Grain, cereal, forage, fodder and straw, group residues. 16, except barley, oat, and wheat; forage ...... 1 .0 Grain, cereal, forage, fodder and straw, group (a) General. Tolerances are estab- 16, except barley, oat, and wheat; stover ...... 1 .0 lished for the combined residues of the Grain, cereal, forage, fodder and straw, group fungicide triadimefon, 1-(4- 16, except barley, oat, and wheat; straw ...... 1 .0 Oat, flour ...... 1 .0 chlorophenoxy)-3,3-dimethyl-1-(1H- Oat, forage ...... 2 .0 1,2,4-triazol-1-yl)-2-butanone, and Oat, grain ...... 0 .2 triadimenol, b-(4-chlorophenoxy)-a-(1,1- Oat, groats, rolled oats ...... 1 .0 dimethylethyl)-1H-1,2,4-triazole-1-eth- Oat, straw ...... 2.0 Wheat, bran ...... 1.0 anol, expressed as triadimefon, in or on Wheat, flour ...... 1 .0 the following food commodities:

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Expiration/ Parts per Commodity Parts per Revocation Commodity million million Date Milk ...... 0.05 Pineapple ...... 2.0 None Nut, macadamia ...... 0.1 Onion, bulb ...... 0 .5 (b) Section 18 emergency exemptions. Peanut ...... 1 .5 Peanut, meal ...... 2 .2 [Reserved] Pecans ...... 0 .05 (c) Tolerances with regional registra- Poultry, fat ...... 0.05 tions. [Reserved] Poultry, meat ...... 0 .05 (d) Indirect or inadvertent residues. Poultry, meat byproducts ...... 0.05 Potato1 ...... 1 .0 [Reserved] Potato, chips1 ...... 2 .0 Potato, granules/flakes1 ...... 4 .0 [73 FR 54962, Sept. 24, 2008, as amended at 76 Sheep, fat ...... 0 .05 FR 34885, June 15, 2011] Sheep, meat ...... 0.05 Sheep, meat byproducts ...... 0 .05 § 180.411 Fluazifop-P-butyl; tolerances Soybean, seed ...... 2 .5 for residues. Sweet potato, roots ...... 1 .5 (a) General. Tolerances are estab- 1 No U.S. registrations. lished for residues of the herbicide (b) Section 18 emergency exemptions. fluazifop-P-butyl, including its me- [Reserved] tabolites and degradates, in or on the (c) Tolerances with regional registra- following commodities in the table. tions. Tolerances with regional reg- Compliance with the tolerance levels istrations are established for residues specified in the table below is to be de- of the herbicide fluazifop-P-butyl, in- termined by measuring only the sum of cluding its metabolites and degradates, fluazifop-P-butyl, butyl(R)-2-[4-[[5- in or on the following commodities in (trifluoromethyl)-2- the table. Compliance with the toler- pyridinyl]oxy]phenoxy]propanoate, and ance levels specified in the table below the free and conjugated forms of the re- is to be determined by measuring only solved isomer of fluazifop, (R)-2-[4-[[5- the sum of fluazifop-P-butyl, butyl(R)- (trifluoromethyl)-2- 2-[4-[[5-(trifluoromethyl)-2- pyridinyl]oxy]phenoxy]propanoic acid, pyridinyl]oxy]phenoxy]propanoate, and calculated as the stoichiometric equiv- the free and conjugated forms of the re- alent of fluazifop, in or on the com- solved isomer of fluazifop, (R)-2-[4-[[5- modity. (trifluoromethyl)-2- pyridinyl]oxy]phenoxy]propanoic acid, Parts per Commodity million calculated as the stoichiometric equivalent of fluazifop, in or on the com- Banana ...... 0.01 Beans, dry, seed ...... 50 modity. Beet, sugar, dried pulp ...... 1 .0 Beet, sugar, molasses ...... 3 .5 Commodity Parts per Beet, sugar, roots ...... 0 .25 million Carrot, roots ...... 2.0 Asparagus ...... 3.0 Cattle, fat ...... 0.05 Coffee, bean ...... 0 .1 Cattle, meat ...... 0 .05 Pepper, tabasco ...... 1 .0 Cattle, meat byproducts ...... 0.05 Citrus, dried pulp ...... 0 .40 Rhubarb ...... 0 .5 Citrus, juice ...... 0 .06 Citrus, oil ...... 30.0 (d) Indirect or inadvertent residues. Cotton, gin byproducts ...... 1 .5 [Reserved] Cotton, refined oil ...... 1.3 Cotton, undelinted seed ...... 1 .0 [65 FR 33714, May 24, 2000, as amended at 74 Egg ...... 0 .05 FR 9372, Mar. 4, 2009; 74 FR 46374, Sept. 9, Endive ...... 6.0 2009; 74 FR 47457, Sept. 16, 2009; 76 FR 5703, Fruit, citrus, group 10 ...... 0 .03 Fruit, stone ...... 0 .05 Feb. 2, 2011; 76 FR 59908, Sept. 28, 2011; 80 FR Goat, fat ...... 0 .05 46822, Aug. 6, 2015] Goat, meat ...... 0.05 Goat, meat byproducts ...... 0 .05 § 180.412 Sethoxydim; tolerances for Grape ...... 0 .01 residues. Hog, fat ...... 0 .05 Hog, meat ...... 0 .05 (a) Tolerances are established for the Hog, meat byproducts ...... 0 .05 herbicide sethoxydim, including its Horse, fat ...... 0 .05 Horse, meat ...... 0 .05 metabolites and degradates, in or on Horse, meat byproducts ...... 0 .05 the commodities in the table below.

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Compliance with the tolerance levels Commodity Parts per specified below is to be determined by illion measuring only the sum of the herbi- Horse, meat ...... 0 .2 cide 2-[1-(ethoxyimino)butyl]-5-[2- Horse, meat byproducts ...... 1 .0 (ethylthio)propyl]-3-hydroxy-2-cyclo- Jojoba, meal ...... 20 Juneberry 1 ...... 5 .0 hexen-1-one (CAS Reg. No. 74051–80–2) Lesquerella, meal ...... 40 and its metabolites containing the 2- Lingonberry 1 ...... 5.0 cyclohexen-1-one moiety, calculated as Lunaria, meal ...... 40 the stoichiometric equivalent of Meadowfoam, meal ...... 40 Milk ...... 0.5 sethoxydim, in or on the commodity. Milkweed, meal ...... 40 Mustard, meal ...... 40 Parts per Nectarine ...... 0 .2 Commodity illion Niger seed, meal ...... 20 Alfalfa, forage ...... 40 Nut, tree, group 14 ...... 0 .2 Alfalfa, hay ...... 40 Oil radish, meal ...... 40 Almond, hulls ...... 2 .0 Pea and bean, dried shelled, except soybean, Apricot ...... 0 .2 subgroup 6C ...... 25 Apple, wet pomace ...... 0 .8 Pea, field, hay ...... 40 Asparagus ...... 4.0 Pea, field, vines ...... 20 Bean, succulent ...... 15 Pea, succulent ...... 10 Beet, sugar, molasses ...... 10 Peach ...... 0 .2 Beet, sugar, tops ...... 3.0 Peanut ...... 25 Berry, low growing, subgroup 13–07H, except Peppermint, tops ...... 30 strawberry ...... 2 .5 Pistachio ...... 0.2 Borage, meal ...... 40 Poppy seed, meal ...... 40 Buckwheat, flour ...... 25 Potato granules/flakes ...... 8 .0 Buckwheat, grain ...... 19 Potato waste, processed ...... 8.0 Bushberry subgroup 13–07B ...... 4 .0 Poultry, fat ...... 0.2 Calendula, meal ...... 20 Poultry, meat ...... 0 .2 Caneberry subgroup 13–07A ...... 5.0 Poultry, meat byproducts ...... 2.0 Canola, meal ...... 40 Radish, tops ...... 4 .5 Castor oil plant, meal ...... 20 Rapeseed, meal ...... 40 Cattle, fat ...... 0.2 Rapeseed subgroup 20A ...... 35 Cattle, meat ...... 0 .2 Rose hip, meal ...... 20 Cattle, meat byproducts ...... 1.0 Safflower, seed ...... 15 Cherry, sweet ...... 0 .2 Salal 1 ...... 5 .0 Cherry, tart ...... 0 .2 Sesame, meal ...... 40 Chinese tallowtree, meal ...... 20 Sheep, fat ...... 0 .2 Citrus, dried pulp ...... 1 .5 Sheep, meat ...... 0.2 Clover, forage ...... 35 Sheep, meat byproducts ...... 1 .0 Clover, hay ...... 55 Soybean, hay ...... 10 Coriander, leaves ...... 4 .0 Soybean, seed ...... 16 Corn, field, forage ...... 2 .0 Spearmint, tops ...... 30 Corn, field, grain ...... 0 .5 Strawberry ...... 10 Corn, field, stover ...... 2 .5 Stokes aster, meal ...... 20 Corn, sweet, forage ...... 3 .0 Sunflower, meal ...... 20 Corn, sweet, kernel plus cob with husk removed 0.4 Sunflower subgroup 20B, except safflower ...... 7 .0 Corn, sweet, stover ...... 3 .5 Sweet rocket, meal ...... 40 Cottonseed subgroup 20C ...... 5 .0 Tallowwood, meal ...... 20 Cowpea, forage ...... 15 Tea oil plant, meal ...... 20 Cowpea, hay ...... 50 Turnip, tops ...... 5.0 Crambe, meal ...... 40 Vegetable, brassica, leafy, group 5 ...... 5.0 Cuphea, meal ...... 40 Vegetable, bulb, group 3–07 ...... 1 .0 Dillweed, fresh leaves ...... 10 Vegetable, cucurbit, group 9 ...... 4.0 Echium, meal ...... 40 Vegetable, fruiting, group 8–10 ...... 4 .0 Egg ...... 2 .0 Vegetable, leafy, except brassica, group 4 ...... 4 .0 Euphorbia, meal ...... 20 Vegetable, root and tuber, group 1 ...... 4 .0 Evening primrose, meal ...... 20 Vernonia, meal ...... 20 Flax seed, meal ...... 40 Fruit, citrus, group 10–10 ...... 0 .5 1 The individual tolerances for Juneberry, Lingonberry, and Fruit, pome, group 11–10 ...... 0 .2 Salal expire on December 15, 2015. Fruit, small, vine climbing, except fuzzy kiwifruit, subgroup 13–07F ...... 1 .0 (b) Section 18 emergency exemptions. Goat, fat ...... 0 .2 [Reserved] Goat, meat ...... 0.2 (c) Tolerances with regional registra- Goat, meat byproducts ...... 1 .0 tion. Tolerances are established for the Gold of pleasure, meal ...... 40 Grape, raisin ...... 2 .0 herbicide sethoxydim, including its Hare’s ear mustard, meal ...... 40 metabolites and degradates, in or on Hog, fat ...... 0 .2 the commodities in the table below. Hog, meat ...... 0 .2 Hog, meat byproducts ...... 1 .0 Compliance with the tolerance levels Horse, fat ...... 0 .2 specified below is to be determined by

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measuring only the sum of the herbi- Commodity Parts per cide 2-[1-(ethoxyimino)butyl]-5-[2- million (ethylthio)propyl]-3-hydroxy-2-cyclo- Goat, meat byproducts ...... 0 .2 hexen-1-one) and its metabolites con- Horse, fat ...... 0 .01 taining the 2-cyclohexen-1-one moiety, Horse, meat ...... 0 .01 Horse, meat byproducts ...... 0 .2 calculated as the stoichiometric equiv- Milk ...... 0.02 alent of sethoxydim, in or on the com- Sheep, fat ...... 0 .01 modity. Sheep, meat ...... 0.01 Sheep, meat byproducts ...... 0 .2 Commodity Parts per million (b) Section 18 emergency exemptions. Artichoke, globe ...... 5.0 [Reserved] Fescue, forage ...... 7.0 (c) Tolerances with regional registra- Fescue, hay ...... 4.0 tions. [Reserved] Rhubarb ...... 0 .3 (d) Indirect or inadvertent residues. (d) Indirect and inadvertent residues. [Reserved] [Reserved] [65 FR 33715, May 24, 2000, as amended at 67 [80 FR 34077, June 15, 2015] FR 46893, July 17, 2002; 71 FR 54434, Sept. 15, 2006] § 180.413 Imazalil; tolerances for residues. § 180.414 Cyromazine; tolerances for residues. (a) General. (1) Tolerances are established for the combined residues of the (a) General. (1) Tolerances are estab- fungicide imazalil, 1-[2-(2,4- lished for residues of the insecticide dichlorophenyl)-2-(2- cyromazine, including its metabolites propenyloxy)ethyl]-1H-imidazole, and and degradates, in or on the commod- its metabolite, 1-(2,4-dichlorophenyl)-2- ities in the table in this paragraph. (1H-imidazole-1-yl)-1-ethanol, in or on Compliance with the tolerance levels the following food commodities: specified in this paragraph is to be determined by measuring only Commodity Parts per cyromazine, N-cyclopropyl-1,3,5-tri- million azine-2,4,6-triamine, in or on the com- Banana ...... 3.0 modity. Barley, grain ...... 0 .1 Barley, hay ...... 0 .5 Commodity Parts per Barley, straw ...... 0 .5 million Citrus, dried pulp ...... 25 .0 Citrus, oil ...... 200.0 Bean, dry, except cowpea ...... 3 .0 Fruit, citrus, postharvest ...... 10.0 Bean, lima ...... 1 .0 Wheat, forage ...... 0 .5 Bean, succulent ...... 2 .0 Wheat, grain ...... 0 .1 Broccoli ...... 1 .0 Wheat, hay ...... 0 .5 Cabbage, abyssinian ...... 10 .0 Wheat, straw ...... 0 .5 Cabbage, seakale ...... 10.0 Cattle, fat ...... 0.05 (2) Tolerances are established for the Cattle, kidney ...... 0 .2 Cattle, meat ...... 0 .05 combined residues of the fungicide Cattle, meat byproducts, except kidney ...... 0.05 imazalil, 1-[2-(2,4-dichlorophenyl)-2-(2- Egg ...... 0 .25 propenyloxy)ethyl]-1H-imidazole, and Garlic ...... 0 .2 Garlic, great-headed, bulb ...... 0 .2 its metabolites, 3-[2-(2,4- Goat, fat ...... 0 .05 dichlorophenyl)-2-(2,3- Goat, kidney ...... 0 .2 dihydroxypropoxy)ethyl]-2,4- Goat, meat ...... 0.05 imidazolidinedione (FK772) and 3-[2- Goat, meat byproducts, except kidney ...... 0 .05 Hanover salad, leaves ...... 10 .0 (2,4-dichlorophenyl)-2-(hydroxy)]-2,4- Hog, fat ...... 0 .05 imidazolidinedione (FK284), in or on Hog, kidney ...... 0.2 the following food commodities: Hog, meat ...... 0 .05 Hog, meat byproducts, except kidney ...... 0 .05 Parts per Horse, fat ...... 0 .05 Commodity million Horse, kidney ...... 0 .2 Horse, meat ...... 0 .05 Cattle, fat ...... 0.01 Horse, meat byproducts, except kidney ...... 0 .05 Cattle, meat ...... 0 .01 Leek ...... 3 .0 Cattle, meat byproducts ...... 0.2 Mango 1 ...... 0.3 Goat, fat ...... 0 .01 Milk ...... 0.05 Goat, meat ...... 0.01 Mushroom ...... 1 .0

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when present therein as a result of the Commodity Parts per million application of cyromazine to growing Onion, bulb ...... 0 .2 crops listed in paragraph (a)(1) of this Onion, green ...... 3 .0 section. Compliance with the tolerance Onion, potato ...... 3 .0 levels specified in this paragraph is to Onion, tree ...... 3.0 Onion, welsh ...... 3.0 be determined by measuring only Pepper ...... 1 .0 cyromazine, N-cyclopropyl-1,3,5-tri- Potato ...... 0 .8 azine-2,4,6-triamine, in or on the com- Poultry, fat (from chicken layer hens and chick- modity. en breeder hens only) ...... 0 .05 Poultry, meat (from chicken layer hens and Parts per chicken breeder hens only) ...... 0 .05 Commodity million Poultry, meat byproducts (from chicken layer hens and chicken breeder hens only) ...... 0 .05 Cotton, undelinted seed ...... 0 .1 Rakkyo, bulb ...... 0.2 Corn, sweet, kernel plus cob with husks re- Shallot, bulb ...... 0 .2 moved ...... 0 .5 Shallot, fresh leaves ...... 3 .0 Corn, sweet, forage ...... 0 .5 Sheep, fat ...... 0 .05 Corn, sweet, stover ...... 0 .5 Sheep, kidney ...... 0.2 Radish, roots ...... 0 .5 Sheep, meat ...... 0.05 Radish, tops ...... 0 .5 Sheep, meat byproducts, except kidney ...... 0 .05 Tomato ...... 0.5 Turnip, greens ...... 10.0 [65 FR 25860, May 4, 2000, as amended at 67 Vegetable, brassica, leafy, group 5, except broc- FR 72593, Dec. 6, 2002; 68 FR 55269, Sept. 24, coli ...... 10 .0 2003; 75 FR 22256, Apr. 28, 2010; 76 FR 23494, Vegetable, leafy, except brassica, group 4 ...... 7 .0 Vegetable, cucurbit, group 9 ...... 1.0 Apr. 27, 2011] 1There are no U.S. registrations on mango as of May 4, 2000. § 180.415 Aluminum tris (O- ethylphosphonate); tolerances for (2) A tolerance of 5.0 parts per mil- residues. lion is established for residues of the (a) General. Tolerances are estab- insecticide cyromazine, including its lished for residues of the fungicide alu- metabolites and degradates, in or on minum tris (O-ethylphosphonate), in- poultry feed when used as a feed addi- cluding its metabolites and degradates, tive only in feed for chicken layer hens in or on the commodities in the table and chicken breeder hens at the rate of in this paragraph. Compliance with the not more than 0.01 pound of tolerance levels specified in this para- cyromazine per ton of poultry feed for graph is to be determined by measuring control of flies in manure of treated only aluminum tris (O- chicken layer hens and chicken breeder ethylphosphonate), in or on the com- hens, provided the feeding of modity. cyromazine-treated feed must stop at least 3 days (72 hours) before slaughter. Commodity Parts per If the feed is formulated by any person million other than the end user, the formulator Avocado ...... 25 must inform the end user, in writing, Banana ...... 3.0 of the 3-day (72 hours) pre-slaughter in- Bushberry subgroup 13B ...... 40 Caneberry subgroup 13A ...... 0 .1 terval. Compliance with the tolerance Cranberry ...... 0 .5 level specified in this paragraph is to Fruit, citrus, group 10 ...... 5 .0 be determined by measuring only Fruit, pome, group 11 ...... 10 Ginseng ...... 0 .1 cyromazine, N-cyclopropyl-1,3,5-tri- Hop, dried cones ...... 45 azine-2,4,6-triamine, in or on the com- Juneberry ...... 40 modity. Lingonberry ...... 40 (b) Section 18 emergency exemptions. Nut, macadamia ...... 0.20 Onion, bulb ...... 0 .5 [Reserved] Onion, green ...... 10.0 (c) Tolerances with regional registra- Pea, succulent ...... 0 .3 tions. [Reserved] Pepper/eggplant, subgroup 8–10B 1 ...... 0 .01 Pineapple ...... 0.1 (d) Indirect or inadvertent residues. Salal ...... 40 Tolerances are established for indirect Strawberry ...... 75 or inadvertent residues of the insecti- Tomato ...... 3 cide cyromazine, including its metabo- Turnip, greens ...... 40 Turnip, roots ...... 15 lites and degradates, in or on the com- Vegetable, brassica, leafy, group 5 ...... 60 modities in the table in this paragraph Vegetable, cucurbit, group 9 ...... 15

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(c) Tolerances with regional registra- Commodity Parts per million tions. [Reserved] Vegetable, leafy, except brassica, group 4 ...... 100 (d) Indirect or inadvertent residues. [Reserved] (b) Section 18 emergency exemptions. [49 FR 391, Jan. 4, 1984, as amended at 50 FR [Reserved] 4976, Feb. 5, 1985; 52 FR 11262, Apr. 8, 1987; 62 (c) Tolerances with regional registra- FR 66014, Dec. 17, 1997; 64 FR 5191, Feb. 3, tions. Tolerances with regional reg- 1999; 64 FR 54782, Oct. 8, 1999; 66 FR 37598, istration, as defined in § 180.1(l), are es- July 19, 2001; 66 FR 41454, Aug. 8, 2001; 67 FR tablished for residues of the fungicide 2342, Jan. 17, 2002; 67 FR 49617, July 31, 2002; aluminum tris (O-ethylphosphonate), 72 FR 68534, Dec. 5, 2007; 78 FR 40020, July 3, including its metabolites and 2013] degradates, in or on the commodities § 180.417 Triclopyr; tolerances for resi- in the table in this paragraph. Compli- dues. ance with the tolerance levels specified (a) General. (1) Tolerances are estab- in this paragraph is to be determined lished for residues of the herbicide by measuring only aluminum tris (O- triclopyr, including its metabolites and ethylphosphonate), in or on the com- degradates, in or on the commodities modity. in the table below resulting from the application of the butoxyethyl ester of Commodity Parts per million triclopyr, triethylamine salt of Asparagus ...... 0.1 triclopyr, or choline salt of triclopyr. Grape ...... 10 Compliance with the tolerance levels specified below is to be determined by (d) Indirect or inadvertent residues. measuring only triclopyr, 2-[(3,5,6- [Reserved] trichloro-2-pyridinyl)oxy]acetic acid.

[64 FR 36801, July 8, 1999, as amended at 64 Parts per FR 37875, July 14, 1999; 65 FR 50438, Aug. 18, Commodity million 2000; 67 FR 55346, Aug. 29, 2002; 68 FR 11335, Mar. 10, 2003; 70 FR 7047, Feb. 10, 2005; 76 FR Egg ...... 0 .05 23494, Apr. 27, 2011; 80 FR 2320, Jan. 16, 2015] Fish ...... 3 .0 Grass, forage ...... 700.0 Grass, hay ...... 200.0 § 180.416 Ethalfluralin; tolerances for Milk ...... 0.60 residues. Poultry, fat ...... 0.1 Poultry, meat ...... 0 .1 (a) General. Tolerances are estab- Poultry, meat byproducts, except kidney ...... 0.1 lished for residues of the herbicide Rice, grain ...... 0 .3 ethalfluralin, including its metabolites Shellfish ...... 3 .5 and degradates, in or on the commodities in the following table. Compliance (2) Tolerances are established for res- with the tolerance levels specified in idues of the herbicide triclopyr, includ- the following table is to be determined ing its metabolites and degradates, in by measuring only the residues of or on the commodities in the table below resulting from the application of ethalfluralin, N-ethyl-N-(2-methyl-2- propenyl)-2,6-dinitro-4- the butoxyethyl ester of triclopyr, (trifluoromethyl)benzenamine. triethylamine salt of triclopyr, or choline salt of triclopyr. Compliance with the tolerance levels specified Commodity Parts per million below is to be determined by measuring Bean, dry, seed ...... 0 .05 the combined residues of triclopyr, 2- Dill, dried leaves ...... 0 .05 [(3,5,6-trichloro-2-pyridinyl)oxy]acetic Dill, fresh leaves ...... 0 .05 acid, and its metabolite 3,5,6-trichloro- Peanut ...... 0 .05 Pea, dry, seed ...... 0 .05 2-pyridinol (TCP), calculated as the Potato ...... 0 .05 stoichiometric equivalent of triclopyr. Rapeseed subgroup 20A ...... 0 .05 Soybean ...... 0.05 Commodity Parts per Sunflower subgroup 20B ...... 0.05 million Vegetable, cucurbit, group 9 ...... 0.05 Cattle, fat ...... 0.10 Cattle, meat ...... 0 .10 (b) Section 18 emergency exemptions. Cattle, meat byproducts ...... 0.50 [Reserved] Goat, fat ...... 0 .10

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(2) Tolerances are established for res- Commodity Parts per million idues of zeta-cypermethrin, (S-cyano(3- Goat, meat ...... 0.10 phenoxyphenyl) methyl (±))(cis-trans 3- Goat, meat byproducts ...... 0 .50 (2,2-dichloroethenyl)-2,2 Hog, fat ...... 0 .10 dimethylcyclopropanecarboxylate), in- Hog, meat ...... 0 .10 Hog, meat byproducts ...... 0 .50 cluding its metabolites and degradates, Horse, fat ...... 0 .10 in or on the commodities in the fol- Horse, meat ...... 0 .10 lowing table. Compliance with the tol- Horse, meat byproducts ...... 0 .50 Sheep, fat ...... 0 .10 erance levels specified in the following Sheep, meat ...... 0.10 table is to be determined by measuring Sheep, meat byproducts ...... 0 .50 only total cypermethrin, cyano(3- phenoxyphenyl)methyl 3-(2,2- (b) Section 18 emergency exemptions. dichloroethenyl)-2,2- [Reserved] dimethylcyclopropane carboxylate, in (c) Tolerances with regional registra- or on the commodity. tions. [Reserved] (d) Indirect or inadvertent residues. Commodity Parts per [Reserved] million [50 FR 18486, May 1, 1985, as amended at 55 Alfalfa, forage ...... 15 FR 26440, June 28, 1990; 60 FR 4095, Jan. 20, Alfalfa, hay ...... 30 1995; 62 FR 46894, Sept. 5, 1997; 63 FR 45406, Alfalfa, seed ...... 0 .50 Aug. 26, 1998; 67 FR 35048, May 17, 2002; 67 FR Almond, hulls ...... 6 58725, Sept. 18, 2002; 72 FR 41931, Aug. 1, 2007; Animal feed, nongrass, group 18, forage ...... 8 Animal feed, nongrass, group 18, hay ...... 40 80 FR 72599, Nov. 20, 2015; 81 FR 9359, Feb. 25, Artichoke, globe ...... 0.60 2016] Avocado ...... 0 .50 Barley, grain ...... 3 .0 § 180.418 Cypermethrin and isomers Barley, hay ...... 6 .0 alpha-cypermethrin and zeta- Barley, straw ...... 20 .0 cypermethrin; tolerances for resi- Beet, sugar, roots ...... 0 .05 dues. Beet, sugar, tops ...... 0.20 Berry group 13 ...... 0 .8 (a) General. (1) Tolerances are estab- Borage, seed ...... 0 .2 lished for residues of the insecticide Brassica, head and stem, subgroup 5A ...... 2 .00 cypermethrin (±)alpha cyano-(3- Brassica, leafy greens, subgroup 5B ...... 14 .00 phenoxyphenyl)methyl(±)cis,trans- Buckwheat, grain ...... 3.0 Buckwheat, hay ...... 6 .0 3(2,2-dichloroethenyl-2,2- Buckwheat, straw ...... 20 .0 dimethylcyclopropanecarboxylate in or Cabbage ...... 2 .00 on the following commodities: Canistel ...... 0 .50 Castor oil plant, refined oil ...... 0.4 Castor oil plant, seed ...... 0 .2 Commodity Parts per million Cattle, fat ...... 1.00 Cattle, meat ...... 0 .2 Brassica, head and stem, subgroup 5A ...... 2 .0 Cattle, meat byproducts ...... 0.05 Brassica, leafy greens, subgroup 5B ...... 14 .0 Chinese tallowtree, refined oil ...... 0 .4 Cattle, fat ...... 1.0 Chinese tallowtree, seed ...... 0 .2 Cattle, meat ...... 0 .2 Cilantro, leaves ...... 10 Cattle, meat byproducts ...... 0.05 Citrus, dried pulp ...... 1 .8 Cotton, gin byproducts ...... 11 .0 Cotton, undelinted seed ...... 0 .5 Citrus, oil ...... 4.0 Egg ...... 0 .05 Corn, field, forage ...... 9 .0 Goat, fat ...... 1 .0 Corn, field, grain ...... 0 .05 Goat, meat ...... 0.2 Corn, field, stover ...... 30 Goat, meat byproducts ...... 0 .05 Corn, pop, grain ...... 0.05 Hog, fat ...... 0 .1 Corn, pop, stover ...... 30 Hog, meat ...... 0 .05 Corn, sweet, forage ...... 15 .00 Horse, fat ...... 1 .0 Corn, sweet, kernel plus cob with husks re- Horse, meat ...... 0 .2 moved ...... 0 .05 Horse, meat byproducts ...... 0 .05 Corn, sweet, stover ...... 15.00 Lettuce, head ...... 4.0 Cotton, undelinted seed ...... 0 .5 Milk, fat (reflecting 0.10 in whole milk) ...... 2 .5 Crambe, seed ...... 0.2 Onion, bulb ...... 0 .1 Cuphea, seed ...... 0 .2 Onion, green ...... 6 .0 Echium, seed ...... 0 .2 Pecan ...... 0 .05 Egg ...... 0 .05 Poultry, fat ...... 0.05 Euphorbia, refined oil ...... 0 .4 Poultry, meat ...... 0 .05 Euphorbia, seed ...... 0 .2 Sheep, fat ...... 1 .0 Evening primrose, refined oil ...... 0 .4 Sheep, meat ...... 0.2 Sheep, meat byproducts ...... 0 .05 Evening primrose, seed ...... 0 .2 Flax, seed ...... 0 .2

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Parts per Parts per Commodity million Commodity million

Food commodities/feed commodities (other than Stokes aster, refined oil ...... 0 .4 those covered by a higher tolerance as a re- Stokes aster, seed ...... 0 .2 sult of use on growing crops) in food/feed Sugarcane, cane ...... 0.60 handling establishments ...... 0 .05 Sunflower, refined oil ...... 0.5 Fruit, citrus, group 10 ...... 0 .35 Sunflower, seed ...... 0.2 Fruit, pome, group 11 ...... 2 Sweet rocket, seed ...... 0 .2 Fruit, stone, group 12 ...... 1 Tallowwood, refined oil ...... 0.4 Goat, fat ...... 1 .00 Tallowwood, seed ...... 0 .2 Goat, meat ...... 0.2 Tea oil plant, refined oil ...... 0 .4 Goat, meat byproducts ...... 0 .05 Tea oil plant, seed ...... 0 .2 Gold of pleasure, seed ...... 0 .2 Turnip, greens ...... 14 Grain, aspirated fractions ...... 10.0 Vegetable, cucurbit, group 9 ...... 0.2 Grape ...... 2 Vegetable, fruiting, group 8 ...... 0.2 Grass, forage, fodder, and hay, group 17, for- Vegetable, leafy, except brassica, group 4 ...... 10.00 age ...... 10 Vegetable, legume, edible podded, subgroup 6A 0 .5 Grass, forage, fodder and hay, group 17, hay .... 35 Vegetable, root and tuber, group 1, except Hare’s-ear mustard, seed ...... 0 .2 sugar beet ...... 0 .1 Hog, fat ...... 0 .1 Vernonia, refined oil ...... 0 .4 Hog, meat ...... 0 .05 Vernonia, seed ...... 0 .2 Horse, fat ...... 1 .00 Wheat, forage ...... 3 .0 Horse, meat ...... 0 .2 Wheat, grain ...... 0 .2 Horse, meat byproducts ...... 0 .05 Wheat, hay ...... 6 .0 Jojoba, refined oil ...... 0.4 Wheat, straw ...... 7 .0 Jojoba, seed ...... 0.2 Lesquerella, seed ...... 0 .2 (3) Tolerances are established for res- Lunaria, seed ...... 0 .2 idues of the insecticide, alpha- Mango ...... 0.70 Meadowfoam, seed ...... 0 .2 cypermethrin, (R)-cyano(3- Milk, fat (reflecting 0.10 in whole milk) ...... 2 .50 phenoxyphenyl)methyl (1S,3S)-rel-3- Milkweed, seed ...... 0 .2 (2,2-dichloroethenyl)-2,2- Mustard, seed ...... 0 .2 Niger seed, refined oil ...... 0 .4 dimethylcyclopropane carboxylate, in- Niger seed, seed ...... 0 .2 cluding its metabolites and degradates, Nut, tree, group 14 ...... 0 .05 in or on the commodities in the table Oat, grain ...... 3 .0 below. Compliance with the tolerance Oat, hay ...... 6.0 Oat, straw ...... 20.0 levels specified below is to be deter- Oil radish, seed ...... 0.2 mined by measuring only total Okra ...... 0.2 cypermethrin, cyano(3- Onion, bulb ...... 0 .10 Onion, green ...... 3 .00 phenoxyphenyl)methyl 3-(2,2- Papaya ...... 0 .50 dichloroethenyl)-2,2- Pea and bean, dried shelled, except soybean, dimethylcyclopropane carboxylate, in subgroup 6C ...... 0 .05 or on the commodity. Pea and bean, succulent shelled, subgroup 6B 0 .1 Peanut ...... 0 .05 Parts per Pecan ...... 0 .05 Commodity million Pistachio ...... 0.05 Poppy, seed ...... 0 .2 Alfalfa, hay ...... 15 Poultry, fat ...... 0.05 Beet, sugar, roots ...... 0 .05 Poultry, meat ...... 0 .05 Beet, sugar, tops ...... 0.20 Rapeseed ...... 0 .2 Brassica, head and stem, subgroup 5A ...... 2 .0 Rice, grain ...... 1 .50 Cattle, fat ...... 1.0 Rice, hulls ...... 6 .00 Cattle, meat ...... 0 .20 Rice, wild, grain ...... 1.5 Cattle, meat byproducts ...... 0.05 Rose hip, refined oil ...... 0.4 Citrus, dried pulp ...... 1 .8 Rose hip, seed ...... 0.2 Citrus, oil ...... 4.0 Rye, grain ...... 3.0 Corn, field, grain ...... 0 .05 Rye, hay ...... 6 .0 Corn, pop, grain ...... 0.05 Rye, straw ...... 20 .0 Corn, sweet, kernel plus cob with husks re- Safflower, seed ...... 0 .2 moved ...... 0 .05 Sapodilla ...... 0 .50 Cotton, undelinted seed ...... 0 .50 Sapote, black ...... 0 .50 Egg ...... 0 .05 Sapote, mamey ...... 0 .50 Food commodities/feed commodities (other than Sesame, seed ...... 0 .2 those covered by a higher tolerance as a re- Sheep, fat ...... 1 .00 sults of use on growing crops) in food/feed Sheep, meat ...... 0.2 handling establishments ...... 0 .05 Sheep, meat byproducts ...... 0 .05 Fruit, citrus, group 10–10 ...... 10 Sorghum, grain, forage ...... 0.1 Goat, fat ...... 1 .0 Sorghum, grain, grain ...... 0 .5 Goat, meat ...... 0.20 Sorghum, grain, stover ...... 5 .0 Goat, meat byproducts ...... 0 .05 Soybean, seed ...... 0 .05 Hog, fat ...... 1 .0 Star apple ...... 0 .50 Hog, meat ...... 0 .05

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Parts per Parts per Commodity million Commodity million

Horse, fat ...... 1 .0 Horse, meat byproducts ...... 0 .5 Horse, meat ...... 0 .20 Milk, fat (0.05 ppm (N) in whole milk ...... 1 .25 Horse, meat byproducts ...... 0 .05 Oat, grain ...... 6 .0 Milk, fat, reflecting 0.10 ppm in whole milk ...... 2 .5 Poultry, fat ...... 0.5 Nut, tree, group 14–12 ...... 0 .05 Poultry, meat ...... 5 Pea and bean, dried shelled, except soybean, Poultry, meat byproducts ...... 5 subgroup 6C ...... 0 .05 Rice, grain ...... 6 .0 Pea and bean, succulent shelled, subgroup 6B 0 .10 Sheep, fat ...... 0 .5 Poultry, fat ...... 0.05 Sheep, meat ...... 0.5 Poultry, meat ...... 0 .05 Sheep, meat byproducts ...... 0 .5 Rice, grain ...... 1 .5 Sorghum, grain ...... 6 .0 Sheep, fat ...... 1 .0 Wheat, grain ...... 6 .0 Sheep, meat ...... 0.20 Sheep, meat byproducts ...... 0 .05 Sorghum, grain, grain ...... 0 .50 (2) Tolerances are established for the Soybean, seed ...... 0 .05 combined residues of the insecticide Vegetable, cucurbit, group 9 ...... 0.20 Vegetable, fruiting, group 8–10 ...... 0 .20 chlorpyrifos-methyl (O,-O- dimethyl-O- Vegetable, leafy, group 4 ...... 10 (3,5,6-trichloro-2-pyridyl) Vegetable, legume, edible podded, subgroup 6A 0 .50 phosphorothioate and its metabolite Vegetable, root and tuber, group 1, except sugar beet ...... 0 .10 (3,5,6-trichloro-2-pyridinol) in or on the Wheat, grain ...... 0 .20 following food commodities when present therein as a result of applica- (b) Section 18 emergency exemptions. tion to stored grains: [Reserved] Parts per (c) Tolerances with regional registra- Commodity million tions. [Reserved] (d) Indirect or inadvertent residues. Barley, bran ...... 90 [Reserved] Barley, pearled barley ...... 90 Rice, bran ...... 30 [62 FR 63235, 63243, Nov. 26, 1997, as amended Rice, hulls ...... 30 at 63 FR 48586, Sept. 11, 1998; 66 FR 47993, Rice, polished rice ...... 30 Sept. 17, 2001; 67 FR 6430, Feb. 12, 2002; 67 FR Sorghum, grain, bran ...... 90 Wheat, bran ...... 30 56495, Sept. 4, 2002; 69 FR 71717, Dec. 10, 2004; Wheat, germ ...... 30 71 FR 78382, Dec. 29, 2006; 72 FR 53462, Sept. Wheat, middlings ...... 30 19, 2007; 72 FR 71801, Dec. 19, 2007; 73 FR 1525, Wheat, shorts ...... 30 Jan. 9, 2008; 77 FR 72984, Dec. 7, 2012; 78 FR 7275, Feb. 1, 2013; 79 FR 73213, Dec. 10, 2014; 79 (b) Section 18 emergency exemptions. FR 77394, Dec. 24, 2014; 80 FR 45438, July 30, [Reserved] 2015; 80 FR 72599, Nov. 20, 2015] (c) Tolerances with regional registra- § 180.419 Chlorpyrifos-methyl; toler- tions. [Reserved] ances for residues. (d) Indirect or inadvertent residues. [Reserved] (a) General. (1) Tolerances are established for the combined residues of the [65 FR 33715, May 24, 2000, as amended at 74 insecticide chlorpyrifos-methyl [O,-O,- FR 46374, Sept. 9, 2009] dimethyl O-(3,5,6-trichloro-2-pyridyl)] phosphorothioate and its metabolite § 180.420 Fluridone; tolerances for res- (3,5,6-trichloro-2-pyridinol) in or on the idues. following food commodities: (a) General. (1) Tolerances are established for residues of the herbicide Parts per fluridone, including its metabolites Commodity million and degradates, in or on the commod- Barley, grain ...... 6 .0 ities in the table in this paragraph. Cattle, fat ...... 0.5 Compliance with the tolerance levels Cattle, meat ...... 0 .5 Cattle, meat byproducts ...... 0.5 specified in this paragraph is to be de- Egg ...... 0 .1 termined by measuring only the sum of Goat, fat ...... 0 .5 fluridone, 1-methyl-3-phenyl-5-(3- Goat, meat ...... 0.5 Goat, meat byproducts ...... 0 .5 (trifluoromethyl)phenyl)-4(1H)- Hog, fat ...... 0 .5 pyridinone, and its bound residues, cal- Hog, meat ...... 0 .5 culated as the stoichiometric equiva- Hog, meat byproducts ...... 0 .5 Horse, fat ...... 0 .5 lent of fluridone, in or on the com- Horse, meat ...... 0 .5 modity.

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erances are established at higher levels Commodity Parts per million from other uses of fluridone on the Crayfish ...... 0.5 crops in the table in this paragraph, Fish ...... 0 .5 the higher tolerance also applies to residues in or on the irrigated commodity. (2) Tolerances are established for res- Compliance with the tolerance levels idues of the herbicide fluridone, includ- specified in this paragraph is to be de- ing its metabolites and degradates, in termined by measuring only fluridone, or on the commodities in the table in 1-methyl-3-phenyl-5-(3- this paragraph. Compliance with the (trifluoromethyl)phenyl)-4(1H)- tolerance levels specified in this para- pyridinone, in or on the commodity. graph is to be determined by measuring only fluridone, 1-methyl-3-phenyl-5-(3- Parts per Commodity million (trifluoromethyl)phenyl)-4(1H)- pyridinone, in or on the commodity. Animal feed, nongrass, group 18 ...... 0 .15 Avocado ...... 0 .1 Parts per Berry, group 13 ...... 0 .1 Commodity million Cranberry ...... 0 .1 Fruit, citrus, group 10 ...... 0 .1 Cattle, fat ...... 0.05 Fruit, pome, group 11 ...... 0.1 Cattle, kidney ...... 0 .1 Fruit, stone, group 12 ...... 0 .1 Cattle, liver ...... 0 .1 Grain, cereal, forage, fodder and straw, group Cattle, meat ...... 0 .05 16 ...... 0 .1 Cattle, meat byproducts ...... 0.05 Grain, cereal, group 15 ...... 0.1 Cotton, undelinted seed ...... 0 .1 Grape ...... 0 .1 Egg ...... 0 .05 Grass, forage ...... 0 .15 Goat, fat ...... 0 .05 Hop, dried cones ...... 0 .1 Goat, kidney ...... 0 .1 Nut, tree, group 14 ...... 0 .1 Goat, liver ...... 0.1 Okra ...... 0.1 Goat, meat ...... 0.05 Strawberry ...... 0 .1 Goat, meat byproducts ...... 0 .05 Vegetable, brassica, leafy, group 5 ...... 0.1 Hog, fat ...... 0 .05 Vegetable, cucurbit, group 9 ...... 0.1 Hog, kidney ...... 0.1 Vegetable, fruiting, group 8 ...... 0.1 Hog, liver ...... 0 .1 Vegetable, leafy, except brassica, group 4 ...... 0 .1 Hog, meat ...... 0 .05 Vegetable, leaves of root and tuber, group 2 ..... 0 .1 Hog, meat byproducts ...... 0 .05 Vegetable, legume, group 6 ...... 0 .1 Horse, fat ...... 0 .05 Vegetable, root and tuber, group 1 ...... 0 .1 Horse, kidney ...... 0 .1 Horse, liver ...... 0 .1 Horse, meat ...... 0 .05 [76 FR 23495, Apr. 27, 2011, as amended at 77 Horse, meat byproducts ...... 0 .05 FR 66720, Nov. 7, 2012; 80 FR 18143, Apr. 3, Milk ...... 0.05 2015; 81 FR 7987, Feb. 17, 2016] Poultry, fat ...... 0.05 Poultry, kidney ...... 0 .01 § 180.421 Fenarimol; tolerances for res- Poultry, liver ...... 0 .01 idues. Poultry, meat ...... 0 .05 Poultry, meat byproducts ...... 0.05 (a) General. Tolerances are estab- Sheep, fat ...... 0 .05 lished for residues of fenarimol, includ- Sheep, kidney ...... 0.1 Sheep, liver ...... 0.1 ing its metabolites and degradates, in Sheep, meat ...... 0.05 or on the commodities in the following Sheep, meat byproducts ...... 0 .05 table. Compliance with the tolerance levels specified in the following table is (b) Section 18 emergency exemptions. to be determined by measuring only [Reserved] fenarimol alpha-(2 chlorophenyl)- (c) Tolerances with regional registra- alpha-(4-chlorophenyl)-5- tions. [Reserved] pyrimidinemethanol. (d) Indirect or inadvertent residues. Tolerances are established for indirect Commodity Parts per or inadvertent residues of the herbicide million fluridone, including its metabolites Apple ...... 0.3 and degradates, in or on the irrigated Apple, wet pomace ...... 0 .3 crop commodities and crop groupings Banana ...... 0.25 Cattle, fat ...... 0.01 in the table in this paragraph, result- Cattle, kidney ...... 0 .01 ing from use of irrigation water con- Cattle, meat ...... 0 .01 taining residues of 0.15 parts per mil- Cattle, meat byproducts, except kidney ...... 0.05 Cherry, sweet ...... 1 .0 lion following applications of fluridone Cherry, tart ...... 1 .0 on or around aquatic sites. Where tol- Goat, fat ...... 0 .01

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Parts per Expiration/ Commodity million Commodity Parts per revocation million date Goat, kidney ...... 0 .01 Goat, meat ...... 0.01 Horse, meat byproducts, Goat, meat byproducts, except kidney ...... 0 .05 except kidney ...... 0.05 7/31/16 Grape ...... 0 .1. Pear ...... 0.1 7/31/16 Hazelnut ...... 0 .02 Pecan ...... 0.02 7/31/16 Hop, dried cones ...... 5 .0 Sheep, fat ...... 0.01 7/31/16 Horse, fat ...... 0 .01 Sheep, kidney ...... 0.01 7/31/16 Horse, kidney ...... 0 .01 Sheep, meat ...... 0.01 7/31/16 Horse, meat ...... 0 .01 Sheep, meat byproducts, Horse, meat byproducts, except kidney ...... 0 .05 except kidney ...... 0.05 7/31/16 Pear ...... 0 .1 Vegetable, cucurbit, group Pecan ...... 0 .02 9 2 ...... 0.20 None Sheep, fat ...... 0 .01 Sheep, kidney ...... 0.01 1 There are no U.S. registrations for bananas as of April 26, Sheep, meat ...... 0.01 1995. 2 There are no U.S. registrations for cucurbit vegetable Sheep, meat byproducts, except kidney ...... 0 .05 group 9 as of August 27, 2010. Vegetable, cucurbit, group 9* ...... 0 .20 *There are no U.S. registrations as of August 27, 2010. § 180.422 Tralomethrin; tolerances for (b) Section 18 emergency exemptions. residues. [Reserved] (a) General. (1) Tolerances are estab- (c) Tolerances with regional registra- lished for residues of the insecticide tions. [Reserved] tralomethrin, including its metabolites (d) Indirect or inadvertent residues. and degradates, in or on the commod- [Reserved] ities in the table in this paragraph. Compliance with the tolerance levels [51 FR 39662, Oct. 30, 1986, as amended at 53 specified in this paragraph is to be de- FR 27349, July 20, 1988; 53 FR 44403, Nov. 3, 1988; 54 FR 45734, Oct. 31, 1989; 60 FR 33354, termined by measuring only the sum of June 28, 1995; 62 FR 49937, Sept. 24, 1997; 62 FR tralomethrin, (S)-cyano(3- 61447, Nov. 18, 1997; 67 FR 35048, May 17, 2002; phenoxyphenyl)methyl (1R,3S)-2,2-di- 67 FR 41807, June 19, 2002; 69 FR 6567, Feb. 11, methyl-3-(1,2,2,2- 2004; 71 FR 32846, June 7, 2006; 71 FR 54434, tetrabromoethyl) Sept. 15, 2006; 74 FR 68173, Dec. 23, 2009; 75 FR cyclopropanecarboxylate, and its me- 56897, Sept. 17, 2010] tabolites (S)-cyano(3- EFFECTIVE DATE NOTE: At 81 FR 34905, June phenoxyphenyl)methyl (1R,3R)-3-(2,2- 1, 2016, § 180.421 was amended by revising the dibromoethenyl)-2,2- table in paragraph (a), effective Nov. 28, 2016. dimethylcyclopropanecarboxylate and For the convenience of the user, the revised (S)-cyano(3-phenoxyphenyl)methyl text is set forth as follows: (1S,3R)-3-(2,2-dibromoethenyl)-2,2- § 180.421 Fenarimol; tolerances for residues. dimethylcyclopropanecarboxylate, cal- (a) * * * culated as the stoichiometric equivalent of tralomethrin, in or on the com- Expiration/ modity. Commodity Parts per revocation million date Parts per Expiration/ Apple ...... 0.3 7/31/16 Commodity revocation million date Apple, wet pomace ...... 0.3 7/31/16 1 Banana ...... 0.25 None Broccoli ...... 0.5 7/9/13 Cattle, fat ...... 0.01 7/31/16 Cotton, undelinted seed ...... 0.02 7/9/13 Cattle, kidney ...... 0.01 7/31/16 Cotton, oil ...... 0.20 7/9/13 Cattle, meat ...... 0.01 7/31/16 Lettuce, head ...... 1.00 7/9/13 Cattle, meat byproducts, Lettuce, leaf ...... 3.00 7/9/13 except kidney ...... 0.05 7/31/16 Soybean, seed ...... 0.05 7/9/13 Cherry, sweet ...... 1.0 7/31/16 Sunflower, seed ...... 0.05 7/9/13 Cherry, tart ...... 1.0 7/31/16 Goat, fat ...... 0.01 7/31/16 Goat, kidney ...... 0.01 7/31/16 (2) A tolerance of 0.02 part per mil- Goat, meat ...... 0.01 7/31/16 lion with an expiration/revocation date Goat, meat byproducts, ex- of July 9, 2013 is established for resi- cept kidney ...... 0.05 7/31/16 Grape ...... 0.1 7/31/16 dues of the insecticide tralomethrin, Hazelnut ...... 0.02 7/31/16 including its metabolites and Hop, dried cones ...... 5.0 7/31/16 degradates, in or on food commodities Horse, fat ...... 0.01 7/31/16 Horse, kidney ...... 0.01 7/31/16 (other than those covered by a higher Horse, meat ...... 0.01 7/31/16 tolerance as a result of use on growing

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crops) in food-handling establishments. tolerance as a result of use on growing Compliance with the tolerance level crops) in feed-handling establishments. specified in this paragraph is to be de- Compliance with the tolerance level termined by measuring only the sum of specified in this paragraph is to be de- tralomethrin, (S)-cyano(3- termined by measuring only the sum of phenoxyphenyl)methyl (1R,3S)-2,2-di- tralomethrin, (S)-cyano(3- methyl-3-(1,2,2,2- phenoxyphenyl)methyl (1R,3S)-2,2-di- tetrabromoethyl) methyl-3-(1,2,2,2- cyclopropanecarboxylate, and its me- tetrabromoethyl) tabolites (S)-cyano(3- cyclopropanecarboxylate, and its me- phenoxyphenyl)methyl (1R,3R)-3-(2,2- tabolites (S)-cyano(3- dibromoethenyl)-2,2- phenoxyphenyl)methyl (1R,3R)-3-(2,2- dimethylcyclopropanecarboxylate and dibromoethenyl)-2,2- (S)-cyano(3-phenoxyphenyl)methyl dimethylcyclopropanecarboxylate and (1S,3R)-3-(2,2-dibromoethenyl)-2,2- (S)-cyano(3-phenoxyphenyl)methyl dimethylcyclopropanecarboxylate, cal- (1S,3R)-3-(2,2-dibromoethenyl)-2,2- culated as the stoichiometric equiva- dimethylcyclopropanecarboxylate, cal- lent of tralomethrin, in or on the com- culated as the stoichiometric equiva- modity. lent of tralomethrin, in or on the com- (i) The insecticide may be present as modity. a residue from application of (i) The insecticide may be present as tralomethrin in food-handling estab- a residue from application of lishments, including food service, man- tralomethrin in feed-handling estab- ufacturing, and processing establish- lishments, including feed manufac- ments, such as restaurants, cafeterias, turing and processing establishments. supermarkets, bakeries, breweries, (ii) The application shall be made in dairies, meat slaughtering and packing accordance with the following pre- plants, and canneries. scribed conditions: Application shall be (ii) The application shall be made in limited to a general surface and spot accordance with the following pre- and/or crack and crevice treatment in scribed conditions: Application shall be feed-handling establishments where limited to a general surface and spot feed and feed products are held or proc- and/or crack and crevice treatment in essed. General surface application may food-handling establishments where be used only when the facility is not in food and food products are held, proc- operation provided exposed feed has essed, prepared, and served. General been covered or removed from the area surface application may be used only being treated. All feed-contact surfaces when the facility is not in operation and equipment must be thoroughly provided exposed food has been covered cleaned after general surface applica- or removed from the area being treat- tions. Spot and/or crack and crevice ap- ed. All food-contact surfaces and equip- plication may be used while the facil- ment must be thoroughly cleaned after ity is in operation provided exposed general surface applications. Spot and/ feed is covered or removed from the or crack and crevice application may area being treated prior to application. be used while the facility is in oper- Spray concentration shall be limited to ation provided exposed food is covered a maximum of 0.06 percent active in- or removed from the area being treated gredient. Contamination of feed and prior to application. Spray concentra- feed-contact surfaces shall be avoided. tion shall be limited to a maximum of 0.06 percent active ingredient. Con- (b) Section 18 emergency exemptions. tamination of food and food-contact [Reserved] surfaces shall be avoided. (c) Tolerances with regional registra- (3) A tolerance of 0.02 part per mil- tions. [Reserved] lion with an expiration/revocation date (d) Indirect or inadvertent residues. of July 9, 2013 is established for resi- [Reserved] dues of the insecticide tralomethrin, [62 FR 63001, Nov. 26, 1997, as amended at 62 including its metabolites and FR 66025, Dec. 17, 1997; 65 FR 33701, May 24, degradates, in or on feed commodities 2000; 71 FR 74817, Dec. 13, 2006; 77 FR 59127, (other than those covered by a higher Sept. 26, 2012]

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EFFECTIVE DATE NOTE: At 81 FR 34906, June acid, in or on the raw agricultural com- 1, 2016, § 180.422 was removed, effective Nov. modity soybean at 0.05 part per mil- 28, 2016. lion. § 180.425 Clomazone; tolerances for [51 FR 13309, Apr. 2, 1986] residues. (a) General. Tolerances are estab- § 180.427 Tau-Fluvalinate; tolerances for residues. lished for residues of the herbicide clomazone, including its metabolites (a) General. Tolerances are estab- and degradates, in or on the commod- lished for residues of the insecticide ities in the table in this paragraph. tau-fluvalinate, cyano-(3- Compliance with the tolerance levels phenoxyphenyl)methyl N-[2-chloro-4- specified in this paragraph is to be de- (trifluoromethyl)phenyl]-D-valinate, in termined by measuring only or on the following food commodities: clomazone, 2-[(2-chlorophenyl)methyl]- Parts per 4,4-dimethyl-3-isoxazolidinone, in or on Commodity million the commodity. Honey ...... 0.02 Parts per Commodity million (b) Section 18 emergency exemptions. Bean, snap, succulent ...... 0 .05 [Reserved] Brassica, head and stem, subgroup 5A ...... 0 .10 (c) Tolerances with regional registra- Cotton, undelinted seed ...... 0 .05 tions. [Reserved] Cowpea, forage ...... 0 .05 Cowpea, hay ...... 0 .05 (d) Indirect and inadvertent residues. Cucumber ...... 0 .1 [Reserved] Pea, southern, dry seed ...... 0.05 Pea, southern, succulent seed ...... 0 .05 [65 FR 33701, May 24, 2000, as amended at 67 Pea, succulent ...... 0 .05 FR 49617, July 31, 2002; 73 FR 52616, Sept. 10, Pepper ...... 0 .05 2008] Peppermint, tops ...... 0 .05 Pumpkin ...... 0.1 § 180.428 Metsulfuron methyl; toler- Rhubarb ...... 0 .30 Rice, grain ...... 0 .02 ances for residues. Soybean ...... 0.05 (a) General. (1) Tolerances are estab- Spearmint, tops ...... 0 .05 Squash, summer ...... 0 .1 lished for the combined residues of the Squash, winter ...... 0 .1 herbicide metsulfuron methyl (methyl Sugarcane, cane ...... 0.05 2-[[[[(4-methoxy-6-methyl-1,3,5- triazin- Sweet potato, roots ...... 0 .05 Vegetable, cucurbit, group 9 ...... 0.05 2-yl)amino]carbonyl]amino] sulfonyl] Vegetable, tuberous and corm, except potato, benzoate) and its metabolite methyl 2- subgroup 1D ...... 0 .05 [[[[(4-methoxy-6-methyl-1-,3,5- triazin- 2-yl)amino]carbonyl]amino] sulfonyl]- (b) Section 18 emergency exemptions. 4-hydroxybenzoate in or on the fol- [Reserved] lowing raw material agricultural com- (c) Tolerances with regional registra- modities: tions. [Reserved] (d) Indirect or inadvertent residues. Commodity Parts per [Reserved] million [51 FR 9446, Mar. 19, 1986] Barley, grain ...... 0 .1 Barley, hay ...... 20 .0 EDITORIAL NOTE: For FEDERAL REGISTER ci- Barley, straw ...... 0 .3 tations affecting § 180.425, see the List of CFR Grass, forage ...... 15 .0 Sections Affected, which appears in the Grass, hay ...... 15 .0 Grass, straw ...... 15 .0 Finding Aids section of the printed volume Sorghum, grain, forage ...... 0.2 and at www.fdsys.gov. Sorghum, grain, grain ...... 0 .1 Sorghum, grain, stover ...... 0 .2 § 180.426 2-[4,5-Dihydro-4-methyl-4-(1- Sugarcane, cane ...... 0.05 methylethyl)-5-oxo-1H-imidazol-2- Wheat, forage ...... 5 .0 yl]-3-quinoline carboxylic acid; tol- Wheat, grain ...... 0 .1 Wheat, hay ...... 20 .0 erance for residues. Wheat, straw ...... 0 .3 A tolerance is established for residues of the herbicide 2-[4,5-dihydro-4- (2) Tolerances are established for res- methyl-4-(1-methylethyl)-5-oxo-1H- idues of metsulfuron methyl (methyl- imidazol-2-yl]-3-quinoline carboxylic 2[[[[(4-methoxy- 6-methyl-1,3,5-triazin-

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2- yl)amino]carbonyl]amino] sulfonyl] (b) Section 18 emergency exemptions. benzoate) in or on the following raw [Reserved] agricultural commodities: (c) Tolerances with regional registrations. [Reserved] Parts per Commodity million (d) Indirect or inadvertent residues. [Reserved] Cattle, fat ...... 0.1 Cattle, kidney ...... 0 .5 [74 FR 10494, Mar. 11, 2009, as amended at 74 Cattle, meat ...... 0 .1 FR 67087, Dec. 18, 2009] Cattle, meat byproducts ...... 0.1 Goat, fat ...... 0 .1 § 180.430 Fenoxaprop-ethyl; tolerances Goat, kidney ...... 0 .5 for residues. Goat, meat ...... 0.1 Goat, meat byproducts ...... 0 .1 (a) General. Tolerances are estab- Hog, fat ...... 0 .1 lished for residues of the herbicide Hog, kidney ...... 0.5 fenoxaprop-ethyl, including its me- Hog, meat ...... 0 .1 Hog, meat byproducts ...... 0 .1 tabolites and degradates, in or on the Horse, fat ...... 0 .1 commodities in the table in this para- Horse, kidney ...... 0 .5 graph. Compliance with the tolerance Horse, meat ...... 0 .1 levels specified in this paragraph is to Horse, meat byproducts ...... 0 .1 Milk ...... 0.05 be determined by measuring only the Sheep, fat ...... 0 .1 sum of fenoxaprop-ethyl, (±)-ethyl 2-[4- Sheep, kidney ...... 0.5 [(6-chloro-2- Sheep, meat ...... 0.1 Sheep, meat byproducts ...... 0 .1 benzoxazolyl)oxy]phenoxy]propanoate, and its metabolites, 2-[4-[(6-chloro-2- (b) Section 18 emergency exemptions. benzoxazolyl)oxy]phenoxy]propanoic [Reserved] acid and 6-chloro-2,3- (c) Tolerances with regional registra- dihydrobenzoxazol-2-one, calculated as tions. [Reserved] the stoichiometric equivalent of (d) Indirect or inadvertent residues. fenoxaprop-ethyl, in or on the com- [Reserved] modity.

[64 FR 70191, Dec. 16, 1999, as amended at 66 Commodity Parts per FR 64773, Dec. 14, 2001; 67 FR 51097, Aug. 7, million 2002] Barley, grain ...... 0 .05 Barley, straw ...... 0 .1 § 180.429 Chlorimuron ethyl; toler- Cattle, fat ...... 0.05 ances for residues. Cattle, meat byproducts ...... 0.05 Cattle, meat ...... 0 .05 (a) General. Tolerances are estab- Cotton, undelinted seed ...... 0 .05 lished for residues of the herbicide Goat, fat ...... 0 .05 Goat, meat byproducts ...... 0 .05 chlorimuron ethyl, including its me- Goat, meat ...... 0.05 tabolites and degradates, in or on the Hog, fat ...... 0 .05 commodities in the table below. Com- Hog, meat byproducts ...... 0 .05 Hog, meat ...... 0 .05 pliance with the tolerance levels speci- Horse, fat ...... 0 .05 fied in the following table is to be de- Horse, meat byproducts ...... 0 .05 termined by measuring only Horse, meat ...... 0 .05 Milk ...... 0.02 chlorimuron ethyl, ethyl 2-[[[[(4- Peanut ...... 0 .05 chloro-6-methoxypyrimidin- Peanut, hulls ...... 0 .05 2yl)amino]carbonyl]sulfonyl]benzoate] Rice, grain ...... 0 .05 Sheep, fat ...... 0 .05 in or on the following commodities: Sheep, meat byproducts ...... 0 .05 Sheep, meat ...... 0.05 Commodity Parts per Soybean ...... 0.05 million Wheat, grain ...... 0 .05 Wheat, straw ...... 0 .50 Berry, low growing, except strawberry, subgroup 13–07H ...... 0 .02 Corn, field, forage ...... 0 .5 (b) Section 18 emergency exemptions. Corn, field, grain ...... 0 .01 Time-limited tolerances are estab- Corn, field, stover ...... 2 .0 lished for residues of the herbicide Grain, aspirated fractions ...... 3 .0 Peanut ...... 0 .02 fenoxaprop-ethyl, including its me- Soybean, forage ...... 0 .45 tabolites and degradates, in or on the Soybean, hay ...... 1 .8 commodities in the table in this para- Soybean, seed ...... 0 .05 graph in connection with use of

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fenoxaprop-ethyl under section 18 § 180.431 Clopyralid; tolerances for emergency exemptions granted by residues. EPA. Compliance with the tolerance (a) General. Tolerances are estab- levels specified in this paragraph is to lished for residues of the herbicide be determined by measuring only the clopyralid, including its metabolites sum of fenoxaprop-ethyl, (±)-ethyl 2-[4- and degradates, in or on the commod- [(6-chloro-2- ities in the table below from its appli- benzoxazolyl)oxy]phenoxy]propanoate, cation in the acid form or in the form and its metabolites, 2-[4-[(6-chloro-2- of its salts. Compliance with the toler- benzoxazolyl)oxy]phenoxy]propanoic ance levels specified below is to be de- acid and 6-chloro-2,3- termined by measuring only clopyralid, dihydrobenzoxazol-2-one, calculated as (3,6-dichloro-2-pyridinecarboxylic acid), the stoichiometric equivalent of in or on the following commodities: fenoxaprop-ethyl, in or on the com- Parts per modity. The tolerances expire and are Commodity million revoked on the dates specified in the Apple ...... 0.05 table in this paragraph. Asparagus ...... 1.0 Barley, bran ...... 12 Parts per Expiration/ Barley, grain ...... 3 .0 Commodity million revocation Barley, hay ...... 9 .0 date Barley, pearled barley ...... 12 Barley, straw ...... 9 .0 Grass, forage ...... 0.05 12/31/16 Beet, garden, tops ...... 3 .0 Grass, hay ...... 0.05 12/31/16 Beet, garden, roots ...... 4 .0 Beet, sugar, molasses ...... 10 (c) Tolerances with regional registra- Beet, sugar, roots ...... 2 .0 Beet, sugar, tops ...... 3.0 tions. Tolerances with regional reg- Brassica, head and stem, subgroup 5A ...... 2 .0 istration, as defined in § 180.1(l), are es- Brassica, leafy greens, subgroup 5B ...... 5 .0 tablished for residues of the herbicide Bushberry subgroup 13-07B ...... 0 .50 Canola, meal ...... 6 .0 fenoxaprop-ethyl, including its me- Canola, seed ...... 3 .0 tabolites and degradates, in or on the Cattle, fat ...... 1.0 commodities in the table in this para- Cattle, liver ...... 3 .0 Cattle, meat ...... 1 .0 graph when fenoxaprop-ethyl is used in Cattle, meat byproducts, except liver ...... 36 .0 the states of Oregon, Washington, and Corn, field, forage ...... 3 .0 Utah. Compliance with the tolerance Corn, field, grain ...... 1 .0 Corn, field, milled byproducts ...... 1 .5 levels specified in this paragraph is to Corn, field, stover ...... 10 .0 be determined by measuring only the Corn, pop, grain ...... 1.0 sum of fenoxaprop-ethyl, (±)-ethyl 2-[4- Corn, pop, stover ...... 10.0 Corn, sweet, forage ...... 7 .0 [(6-chloro-2- Corn, sweet, kernel plus cob with husks re- benzoxazolyl)oxy]phenoxy]propanoate, moved ...... 1 .0 and its metabolites, 2-[4-[(6-chloro-2- Corn, sweet, stover ...... 10.0 Cranberry ...... 4 .0 benzoxazolyl)oxy]phenoxy]propanoic Egg ...... 0 .1 acid and 6-chloro-2,3- Flax, meal ...... 6 .0 dihydrobenzoxazol-2-one, calculated as Fruit, stone, group 12 ...... 0 .5 Goat, fat ...... 1 .0 the stoichiometric equivalent of Goat, liver ...... 3.0 fenoxaprop-ethyl, in or on the com- Goat, meat ...... 1.0 modity Goat, meat byproducts, except liver ...... 36 .0 Grass, forage ...... 500.0 Grass, hay ...... 500.0 Parts per Commodity million Hog, fat ...... 0 .2 Hog, meat ...... 0 .2 Grass, hay ...... 0 .09 Hog, meat byproducts ...... 0 .2 Hop, dried cones ...... 5 .0 Horse, fat ...... 1 .0 (d) Indirect or inadvertent residues. Horse, liver ...... 3 .0 [Reserved] Horse, meat ...... 1 .0 Horse, meat byproducts, except liver ...... 36 .0 [63 FR 1377, Jan. 9, 1998, as amended at 63 FR Milk ...... 0.2 19837, Apr. 22, 1998; 73 FR 33718, June 13, 2008; Oat, forage ...... 9 .0 75 FR 80346, Dec. 22, 2010; 76 FR 23495, Apr. 27, Oat, grain ...... 3 .0 Oat, groats/rolled oats ...... 12 2011; 78 FR 78748, Dec. 27, 2013; 79 FR 26164, Oat, straw ...... 9.0 May 7, 2014] Peppermint, tops ...... 3 .0

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(b) Section 18 emergency exemptions. Commodity Parts per million [Reserved] Plum, prune, dried ...... 1.5 (c) Tolerances with regional registra- Poultry, fat ...... 0.2 tions. Tolerances with regional reg- Poultry, meat ...... 0 .2 istration, as defined in § 180.1(l), are es- Poultry, meat byproducts ...... 0.2 Rapeseed, forage ...... 3 .0 tablished for residues of the herbicide Rapeseed, meal ...... 6 .0 lactofen, including its metabolites and Rapeseed, subgroup 20A, except gold of pleas- degradates, in or on the commodities ure ...... 3 .0 Sheep, fat ...... 1 .0 in the table in this paragraph. Compli- Sheep, liver ...... 3.0 ance with the tolerance levels specified Sheep, meat ...... 1.0 in this paragraph is to be determined Sheep, meat byproducts, except liver ...... 36 .0 Spearmint, tops ...... 3 .0 by measuring only lactofen, 2-ethoxy-1- Spinach ...... 5 .0 methyl-2-oxoethyl 5-[2-chloro-4- Strawberry ...... 4 .0 (trifluoromethyl)phenoxy]-2- Swiss chard ...... 3.0 nitrobenzoate, in or on the commodity. Teff, forage ...... 9 .0 Teff, grain ...... 3 .0 Parts per Teff, hay ...... 9 .0 Commodity million Teff, straw ...... 9 .0 Turnip, greens ...... 4.0 Okra ...... 0.02 Turnip, roots ...... 1 .0 Vegetables, fruiting, group 08 ...... 0 .02 Wheat, bran ...... 12 Wheat, forage ...... 9 .0 Wheat, germ ...... 12 (d) Indirect or inadvertent residues. Wheat, grain ...... 3 .0 [Reserved] Wheat, middling ...... 12 Wheat, shorts ...... 12 [69 FR 57216, Sept. 24, 2004, as amended at 72 Wheat, straw ...... 9 .0 FR 33906, June 20, 2007; 76 FR 23496, Apr. 27, 2011] (b) Section 18 emergency exemptions. [Reserved] § 180.433 Fomesafen; tolerances for (c) Tolerances with regional registra- residues. tions. [Reserved] (a) General. Tolerances are estab- (d) Indirect or inadvertent residues. lished for residues of the herbicide [Reserved] fomesafen, including its metabolites [52 FR 10566, Apr. 2, 1987] and degradates, in or on the following commodities. Compliance with the tol- EDITORIAL NOTE: For FEDERAL REGISTER ci- erance levels specified in the following tations affecting § 180.431, see the List of CFR table below is to be determined by Sections Affected, which appears in the Finding Aids section of the printed volume measuring only fomesafen, 5-[2-chloro- and at www.fdsys.gov. 4-(trifluoromethyl)phenoxy]-N- (methylsulfonyl)-2-nitrobenzamide, in § 180.432 Lactofen; tolerances for resi- or on the commodity. dues. Parts per (a) General. Tolerances are estab- Commodity million lished for residues of the herbicide Bean, dry ...... 0.05 lactofen, including its metabolites and Bean, lima, succulent ...... 0.05 degradates, in or on the commodities Bean, snap, succulent ...... 0.05 in the table in this paragraph. Compli- Cantaloupe ...... 0.025 Cotton, gin byproducts ...... 0.025 ance with the tolerance levels specified Cotton, undelinted seed ...... 0.025 in this paragraph is to be determined Cucumber ...... 0.025 by measuring only lactofen, 2-ethoxy-1- Pea, succulent ...... 0.025 Pepper, bell ...... 0.025 methyl-2-oxoethyl 5-[2-chloro-4- Pepper, non-bell ...... 0.025 (trifluoromethyl)phenoxy]-2- Potato ...... 0.025 nitrobenzoate, in or on the commodity. Pumpkin ...... 0.025 Soybean ...... 0.05 Parts per Soybean, vegetable, succulent ...... 0.05 Commodity million Squash, summer ...... 0.025 Squash, winter ...... 0.025 Beans, snap, succulent, except lima bean ...... 0 .01 Tomato ...... 0.025 Cotton, gin byproducts ...... 0 .02 Watermelon ...... 0.025 Cotton, undelinted seed ...... 0 .01 Peanut ...... 0 .01 (b) Section 18 emergency exemptions. Soybean, seed ...... 0 .01 [Reserved]

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(c) Tolerances with regional registra- Commodity Parts per tions. [Reserved] million (d) Indirect or inadvertent residues. Goat, meat ...... 0.05 [Reserved] Goat, meat byproducts, except liver and kidney 0 .05 Grain, aspirated fractions ...... 110 [71 FR 25951, May 3, 2006, as amended at 72 Grass, forage ...... 0 .5 FR 52020, Sept. 12, 2007; 76 FR 12882, Mar. 9, Grass, hay ...... 0 .5 2011; 78 FR 65570, Nov. 1, 2013; 80 FR 9391, Feb. Grass, straw ...... 40 23, 2015] Hog, kidney ...... 0.2 Hog, liver ...... 0 .2 § 180.434 Propiconazole; tolerances for Horse, fat ...... 0 .05 residues. Horse, kidney ...... 2 .0 Horse, liver ...... 2 .0 (a) General. (1) Tolerances are estab- Horse, meat ...... 0 .05 lished for residues of propiconazole, in- Horse, meat byproducts, except liver and kidney 0 .05 cluding its metabolites and degradates, Leaf petioles subgroup 4B ...... 5 .0 in or on the commodities in the table Low growing berry subgroup 13–07G, except cranberry ...... 1 .3 below. Compliance with the tolerance Milk ...... 0.05 levels specified below is to be deter- Mushroom ...... 0 .1 mined by measuring only those Nut, tree, group 14–12 ...... 0 .10 propiconazole residues convertible to Oat, forage ...... 4 .0 Oat, grain ...... 3 .0 2,4-dichlorobenzoic acid (2,4–DCBA), ex- Oat, hay ...... 15 pressed as the stoichiometric equiva- Oat, straw ...... 10 lent of propiconazole, in or on the com- Onion, bulb subgroup 3–07A ...... 0.2 modity in the table below: Onion, green, subgroup 3–07B ...... 9 .0 Parsley, fresh leaves ...... 13 Parts per Parsley, dried leaves ...... 35 Commodity million Peanut ...... 0 .2 Peanut, hay ...... 20 Almond, hulls ...... 7 .0 Peppermint, tops ...... 10 .0 Banana ...... 0.2 Pineapple ...... 4.5 Barley, bran ...... 6 .0 Pineapple, process residue ...... 7 .0 Barley, grain ...... 3 .0 Pistachio ...... 0.1 Barley, hay ...... 30 Plum ...... 0 .60 Barley, straw ...... 20 Rapeseed subgroup 20A ...... 0 .30 Bean, dry seed ...... 0 .40 Quinoa, grain ...... 3 .0 Bean, snap ...... 0 .70 Bean, succulent shelled ...... 0 .10 Radish, roots ...... 0 .04 Beet, garden, roots ...... 0 .30 Radish, tops ...... 0 .20 Beet, garden, tops ...... 5 .5 Rice, bran ...... 15 Beet, sugar, dried pulp ...... 1 .0 Rice, grain ...... 7 .0 Beet, sugar, molasses ...... 1 .5 Rice, hulls ...... 20 Beet, sugar, roots ...... 0 .3 Rye, bran ...... 0 .6 Beet, sugar, tops ...... 10 Rye, forage ...... 9 .0 Brassica leafy greens, subgroup 5B ...... 20 Rye, grain ...... 0.3 Bushberry, subgroup 13–07B ...... 1.0 Rye, straw ...... 10 Caneberry, subgroup 13–07A ...... 1 .0 Sheep, fat ...... 0 .05 Carrot, roots ...... 0.25 Sheep, kidney ...... 2.0 Cattle, fat ...... 0.05 Sheep, liver ...... 2.0 Cattle, kidney ...... 2 .0 Sheep, meat ...... 0.05 Cattle, liver ...... 2 .0 Sheep, meat byproducts, except liver and kid- Cattle, meat ...... 0 .05 ney ...... 0.05 Cattle, meat byproducts, except liver and kidney 0.05 Sorghum, grain, forage ...... 12 Cilantro, leaves ...... 13 Sorghum, grain, grain ...... 3 .5 Citrus, oil ...... 1000 Sorghum, grain, stover ...... 15 Corn, field, forage ...... 12 Corn, field, grain ...... 0 .2 Soybean, forage ...... 11 Corn, field, stover ...... 30 Soybean, hay ...... 30 Corn, pop, grain ...... 0.2 Soybean, seed ...... 2 .0 Corn, pop, stover ...... 30 Spearmint, tops ...... 10 .0 Corn, sweet, forage ...... 6 .0 Sugarcane, cane ...... 0.4 Corn, sweet, kernel plus cob with husks re- Ti palm, leaves ...... 10 moved ...... 0 .1 Ti palm, roots ...... 0.30 Corn, sweet, stover ...... 30 Tomato ...... 3.0 Dill, seed ...... 15 Vegetable, foliage of legume, group 7 ...... 30 Dillweed, dried leaves ...... 80 Watercress ...... 6 .0 Dillweed, fresh leaves ...... 30 Wheat, bran ...... 0.6 Fruit, citrus, group 10–10 ...... 8 .0 Wheat, forage ...... 15 Fruit, stone, group 12–12, except plum ...... 4.0 Wheat, grain ...... 0 .3 Goat, fat ...... 0 .05 Wheat, hay ...... 30 Goat, kidney ...... 2 .0 Wheat, straw ...... 20 Goat, liver ...... 2.0

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(2) Tolerances are established for commodities when present therein as a propiconazole, including its metabo- result of application of propiconazole lites and degradates, in or on the com- to growing crops in paragraphs (a) and modities in the table below. Compli- (c) of this section: ance with the tolerance levels specified Parts per below is to be determined by measuring Commodity million only propiconazole, 1-[[2-(2,4- dichlorophenyl)-4-propyl-1,3-dioxolan-2- Alfalfa, forage ...... 0.1 yl]methyl]-1H-1,2,4-triazole, in or on Alfalfa, hay ...... 0.1 the commodity. [71 FR 55306, Sept. 22, 2006, as amended at 72 Commodity Parts per FR 20439, Apr. 25, 2007; 74 FR 12613, Mar. 25, million 2009; 75 FR 80346, Dec. 22, 2010; 76 FR 27268, Tea 1 ...... 4.0 May 11, 2011; 77 FR 38204, June 27, 2012; 77 FR 75044, Dec. 19, 2012; 78 FR 23503, Apr. 19, 2013; 1 There are no United States registrations for use of 78 FR 78748, Dec. 27, 2013; 79 FR 18467, Apr. 2, propiconazole on tea as of December 24, 2015. 2014; 80 FR 72599, Nov. 20, 2015; 80 FR 79718, (b) Section 18 emergency exemptions. Dec. 23, 2015; 80 FR 80275, Dec. 24, 2015] Time-limited tolerances are established for residues of propiconazole (1- § 180.435 Deltamethrin; tolerances for [[2-(2,4-dichlorophenyl)-4-propyl-1,3- residues. dioxolan-2-yl] methyl]-1H-1,2,4-triazole) (a) General. (1) Tolerances are estab- and its metabolites determined as 2,4- lished for residues of deltamethrin, in- dichlorobenzoic acid and expressed as cluding its metabolites and degradates, parent compound, in connection with in or on the commodities listed in the use of the pesticide under section 18 following table. Compliance with the emergency exemptions granted by tolerance levels specified is to be deter- EPA. The tolerances will expire and mined by measuring only are revoked on the dates specified in deltamethrin, (1R,3R)-3-(2,2- the following table: dibromovinyl)-2,2- dimethylcyclopropanecarboxylic acid Expiration/ Commodity Parts per revocation (S)-alpha-cyano-3-phenoxybenzyl ester, million date and its major metabolites, trans- deltamethrin, (S)-alpha-cyano-m- Avocado ...... 10 12/31/16 Nectarine ...... 2.0 12/31/13 phenoxybenzyl(1R,3S)-3-(2,2- Peach ...... 2.0 12/31/13 dibromovinyl)-2,2- dimethylcyclopropanecarboxylate, and (c) Tolerances with regional registra- alpha-R-deltamethrin, (R)-alpha-cyano- tions. A tolerance with regional reg- m-phenoxybenzyl-(1R,3R)-3-(2,2- istration, as defined in § 180.1(l), is es- dibromovinyl)-2,2- tablished for residues of 1-[[2-(2,4- dimethylcyclopropanecarboxylate, in dichlorophenyl)-4-propyl-1,3-dioxolan-2- or on the commodity. yl]methyl]-1H-1,2,4-triazole and its metabolites determined as 2,4- Commodity Parts per dichlorobenzoic acid and expressed as million parent compound, in or on the fol- Almond, hulls ...... 2 .5 lowing commodities: Apple, wet pomace ...... 1 .0 Artichoke, globe ...... 0.5 Barley, bran ...... 5 .0 Parts per Commodity million Cattle, fat ...... 0.05 Cattle, meat ...... 0 .02 Cranberry ...... 1 .0 Cattle, meat byproducts ...... 0.05 Rice, wild, grain ...... 0.5 Corn, field, forage ...... 0 .7 Corn, field, refined oil ...... 2 .5 Corn, field, stover ...... 5 .0 (d) Indirect or inadvertent residues. Corn, pop, stover ...... 5.0 Tolerances are established for the com- Corn, sweet, forage ...... 10 bined residues of the fungicide 1-[[2- Corn, sweet, kernel plus cob with husks removed ...... 0 .03 (2,4-dichlorophenyl)-4-propyl-1,3- Corn, sweet, stover ...... 15 dioxolan-2-yl] methyl]-1H-1,2,4-triazole Cotton, refined oil ...... 0.2 and its metabolites determined as 2,4- Cotton, undelinted seed ...... 0 .04 Egg ...... 0 .02 dichlorobenzoic acid and expressed as Fish—freshwater finfish ...... 0.01 parent compound in or on the following Fish—freshwater finfish, farm raised ...... 0 .01

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dibromovinyl)-2,2- Commodity Parts per million dimethylcyclopropanecarboxylate, in Fish—saltwater finfish, other ...... 0 .01 or on the commodity. Fish—saltwater finfish, tuna ...... 0 .01 (b) Section 18 emergency exemptions. Fruit, pome, Group 11 ...... 0 .2 [Reserved] Goat, fat ...... 0 .05 Goat, meat ...... 0.02 (c) Tolerances with regional registra- Goat, meat byproducts ...... 0 .05 tions. [Reserved] Grain, aspirated fractions ...... 65 (d) Indirect or inadvertent residues. Grain, cereal, Group 15, except sweet corn ...... 1 .0 Hog, fat ...... 0 .05 [Reserved] Horse, fat ...... 0 .05 [62 FR 63001, Nov. 26, 1997, as amended at 63 Horse, meat ...... 0 .02 Horse, meat byproducts ...... 0 .05 FR 45414, Aug. 26, 1998; 69 FR 62614, Oct. 27, Lychee* ...... 0 .2 2004; 74 FR 46375, Sept. 9, 2009; 76 FR 34885, Milk, fat (reflecting 0.02 ppm in whole milk) ...... 0 .1 June 15, 2011; 79 FR 66301, Nov. 7, 2014; 80 FR Nut, tree, Group 14 ...... 0.1 16302, Mar. 27, 2015] Onion, bulb ...... 0 .1 Onion, green ...... 1 .5 § 180.436 Cyfluthrin and the isomer Poultry, fat ...... 0.05 Poultry, meat ...... 0 .02 beta-cyfluthrin; tolerances for resi- Poultry, meat byproducts ...... 0.02 dues. Radish, tops ...... 4 .0 (a) General. (1) Tolerances are estab- Rapeseed ...... 0 .2 Rice, hulls ...... 2 .5 lished for residues of the insecticide Rye, bran ...... 5 .0 cyfluthrin (cyano(4-fluoro-3- Sheep, fat ...... 0 .05 phenoxyphenyl)methyl-3-(2,2- Sheep, meat ...... 0.02 Sheep, meat byproducts ...... 0 .05 dichloroethenyl)-2,2dimethyl- Sorghum, grain, forage ...... 0.5 cyclopropane-carboxylate; CAS No. Sorghum, grain, stover ...... 1 .0 68359–37–5) in or on the following raw Soybean, seed ...... 0 .1 Soybean, hulls ...... 0 .2 agricultural commodities: Starfruit* ...... 0.2 Sunflower, seed ...... 0.1 Parts per Commodity million Tomato ...... 0.2 Tomato, paste ...... 1 .0 Alfalfa ...... 5 .0 Tomato, puree ...... 1 .0 Alfalfa, forage ...... 5.0 Vegetable, cucurbit, Group 9 ...... 0 .2 Alfalfa, hay ...... 13 Vegetable, fruiting, Group 8 ...... 0 .3 Almond, hulls ...... 0 .5 Vegetable, root, except sugar beet, Subgroup IB 0 .2 Barley, bran ...... 0 .5 Vegetable, tuberous and corm, Subgroup IC ..... 0 .04 Barley, grain ...... 0 .15 Wheat, bran ...... 5.0 Beet, sugar, dried pulp ...... 1 .0 *There are no U.S. registrations for use of deltamethrin on Beet, sugar, roots ...... 0 .10 starfruit and lychee. Brassica, head and stem, subgroup 5A ...... 2 .5 Brassica, leafy greens, subgroup 5B ...... 7 .0 (2) A tolerance of 0.05 ppm is estab- Buckwheat, grain ...... 0.15 lished for residues of the insecticide Carrot, roots ...... 0.20 Cattle, fat ...... 2.0 deltamethrin, including its metabolites Cattle, meat ...... 0 .10 and degradates, in or on all food/feed Cattle, meat byproducts ...... 0.10 items (other than those covered by a Citrus, dried pulp ...... 0 .3 Citrus, oil ...... 0.3 higher tolerance as a result of use on Corn, field, grain ...... 0 .05 growing crops) when deltamethrin is Corn, pop, grain ...... 0.05 used in food/feed handling establish- Corn, sweet, kernel plus cob with husks removed ...... 0 .05 ments or as a wide-area mosquito Cotton, hulls ...... 2 .0 adulticide. Compliance with the toler- Cotton, refined oil ...... 2.0 ance levels specified is to be deter- Cotton, undelinted seed ...... 1 .0 mined by measuring only Egg ...... 0 .01 Fruit, citrus, group 10 ...... 0 .2 deltamethrin, (1R,3R)-3-(2,2- Fruit, pome, group 11 ...... 0.5 dibromovinyl)-2,2- Fruit, stone, group 12 ...... 0 .3 dimethylcyclopropanecarboxylic acid Goat, fat ...... 2 .0 Goat, meat ...... 0.05 (S)-alpha-cyano-3-phenoxybenzyl ester, Goat, meat byproducts ...... 0 .05 and its major metabolites, trans- Grain, aspirated fractions ...... 150 deltamethrin, (S)-alpha-cyano-m- Grain, cereal, forage, fodder and hay, group 16, forage, except rice ...... 25 phenoxybenzyl(1R,3S)-3-(2,2- Grain, cereal, forage, fodder and hay, group 16, dibromovinyl)-2,2- hay, except rice ...... 6 .0 dimethylcyclopropanecarboxylate, and Grain, cereal, forage, fodder and hay, group 16, stover, except rice ...... 30 alpha-R-deltamethrin, (R)-alpha-cyano- Grain, cereal, forage, fodder and hay, group 16, m-phenoxybenzyl-(1R,3R)-3-(2,2- straw, except rice ...... 7 .0

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tablishments where food and food prod- Commodity Parts per million ucts are held, processed, prepared, or Grape ...... 1 .0 served. Treatments may be made by Grape, raisin ...... 3 .5 general surface, spot, and/or crack and Grass, forage, fodder and hay, group 17, forage 12 crevice applications. Grass, forage, fodder and hay, group 17, hay .... 50 Hog, fat ...... 0 .5 (i) General surface treatments shall Hog, meat ...... 0 .01 be limited to a maximum of 3.8 grams Hog, meat byproducts ...... 0 .01 of active ingredient per 1,000 square Hop, dried cones ...... 20 .0 feet, applying to walls, floors, and ceil- Hop, vines ...... 4 .0 Horse, fat ...... 2 .0 ings with a low-pressure system. Cover Horse, meat ...... 0 .05 or remove all food processing and/or Horse, meat byproducts ...... 0 .05 handling equipment during applica- Lettuce, head ...... 2.0 Lettuce, leaf ...... 3 .0 tion. Do not apply directly to food Milk ...... 0.2 products. Reapplications may be made Milk, fat ...... 5 .0 at 10-day intervals. Millet, grain ...... 0 .15 (ii) Crack and crevice or spot treat- Mustard greens ...... 7.0 Nut, tree, group 14 ...... 0 .01 ments shall be limited to a maximum Oat, bran ...... 0 .5 of 0.1 percent of the active ingredient Oat, grain ...... 0 .15 weight, applied with a low-pressure Pea and bean, dried shelled, except soybean, subgroup 6C ...... 0 .15 system with a pinpoint or variable-pat- Pea, dry, seed ...... 0 .15 tern nozzle. Dust formulation shall be Pea, southern, succulent ...... 0 .25 limited to a maximum of 0.1 percent of Peanut ...... 0 .01 the active ingredient by weight, ap- Peanut, hay ...... 6.0 Pepper ...... 0 .50 plied using a hand duster, power dust- Pistachio ...... 0.01 er, or other equipment capable of ap- Poultry, fat ...... 0.01 plying dust insecticide directly into Poultry, meat ...... 0 .01 Poultry, meat byproducts ...... 0.01 voids and cracks and crevices. Dust ap- Radish, roots ...... 1 .0 plications should be made in a manner Rye, bran ...... 0 .5 to avoid deposits on exposed surfaces Rye, grain ...... 0.15 or introducing the material into the Sheep, fat ...... 2 .0 Sheep, meat ...... 0.05 air. Cover exposed food or remove food Sheep, meat byproducts ...... 0 .05 from premises. Do not apply directly to Sorghum, grain, grain ...... 3 .5 food. Reapplications may be made at Soybean, forage ...... 8 .0 Soybean, hay ...... 4 .0 10-day intervals. Soybean, seed ...... 0 .03 (iii) To ensure safe use of the insecti- Sugarcane, cane ...... 0.05 cide, its label and labeling shall con- Sugarcane, molasses ...... 0 .20 form to that registered by the Environ- Sunflower, forage ...... 5.0 Sunflower, seed ...... 0.02 mental Protection Agency, and it shall Teosinte, grain ...... 0 .05 be used in accordance with such label Tomato ...... 0.20 and labeling. Tomato, dry pomace ...... 5.0 Tomato, paste ...... 0 .5 (3) A tolerance of 0.05 part per mil- Tomato, wet pomace ...... 5.0 lion is established for residues of the Triticale, grain ...... 0 .15 insecticide cyfluthrin (cyano(4-fluoro- Turnip, greens ...... 7.0 3-phenoxyphenyl)methyl-3-(2,2- Vegetable, cucurbit, group 9 ...... 0.1 Vegetable, fruiting, group 8 ...... 0.5 dichloroethenyl)-2,2- Vegetable, leafy, except brassica, group 4 ...... 6 .0 dimethylcyclopropanecarboxylate; Vegetable, tuberous and corm, subgroup 1C ..... 0.01 CAS Reg. No. 68359–37–5) in feed com- Wheat, bran ...... 0.5 Wheat, grain ...... 0 .15 modities exposed to the insecticide Wheat, shorts ...... 0 .5 during treatment of feed-handling establishments where feed and feed prod- (2) A tolerance of 0.05 ppm is estab- ucts are held, processed, prepared, or lished for residues of the insecticide served. Treatments may be made by cyfluthrin (cyano(4-fluoro-3- general surface, spot, and/or crack and phenoxyphenyl)methyl-3-(2,2- crevice applications. dichloroethenyl)-2,2- (i) General surface tratments shall be dimethylcyclopropanecarboxylate; limited to a maximum of 3.8 grams of CAS Reg. No. 69359–37–5) in food com- active ingredient per 1,000 square feet, modities exposed to the insecticide applying to walls, floors, and ceilings during treatment of food-handling es- with a low-pressure system. Cover or

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remove all feed processing and/or han- Commodity Parts per dling equipment during application. Do million not apply directly to feed products. Re- Beet, sugar, roots ...... 0 .10 applications may be made at 10-day in- Brassica, head and stem, subgroup 5A ...... 2 .5 tervals. Brassica, leafy greens, subgroup 5B ...... 7 .0 Buckwheat, grain ...... 0.15 (ii) Crack and crevice or spot treat- Carrot, roots ...... 0.20 ments shall be limited to a maximum Cattle, fat ...... 2.0 of 0.1 percent of the active ingredient Cattle, meat ...... 0 .10 by weight, applied with a low-pressure Cattle, meat byproducts ...... 0.10 Citrus, dried pulp ...... 0 .3 system with a pinpoint or variable-pat- Citrus, oil ...... 0.3 tern nozzle. Dust formulation shall be Corn, field, grain ...... 0 .05 limited to a maximum of 0.1 percent of Corn, pop, grain ...... 0.05 Corn, sweet, kernel plus cob with husks re- the active ingredient by weight, ap- moved ...... 0 .05 plied using a hand duster, power dust- Cotton, hulls ...... 2 .0 er, or other equipment capable of ap- Cotton, refined oil ...... 2.0 plying dust insecticide directly into Cotton, undelinted seed ...... 1 .0 Egg ...... 0 .01 voids and cracks and crevices. Dust ap- Fruit, citrus, group 10 ...... 0 .2 plications should be made in a manner Fruit, pome, group 11 ...... 0.5 to avoid deposits on exposed surfaces Fruit, stone, group 12 ...... 0 .3 Goat, fat ...... 2 .0 or introducing the material into the Goat, meat ...... 0.05 air. Cover exposed feed or remove feed Goat, meat byproducts ...... 0 .05 from premises. Do not apply directly to Grain, aspirated fractions ...... 150 feed. Reapplications may be made at Grain, cereal, forage, fodder and hay, group 16, forage, except rice ...... 25 10-day intervals. Grain, cereal, forage, fodder and hay, group 16, (iii) To ensure safe use of the insecti- hay, except rice ...... 6 .0 cide, its label and labeling shall con- Grain, cereal, forage, fodder and hay, group 16, stover, except rice ...... 30 form to that registered by EPA, and it Grain, cereal, forage, fodder and hay, group 16, shall be used in accordance with such straw, except rice ...... 7 .0 label and labeling. Grape ...... 1 .0 (4) Tolerances are established for res- Grape, raisin ...... 3 .5 Grass, forage, fodder and hay, group 17, forage 12 idues of the isomer, beta-cyfluthrin, Grass, forage, fodder and hay, group 17, hay .... 50 cyano(4-fluoro-3- Hog, fat ...... 0 .5 phenoxyphenyl)methyl-3-(2,2- Hog, meat ...... 0 .01 Hog, meat byproducts ...... 0 .01 dichloroethenyl)-2,2-dimethyl- Hop, dried cones ...... 20 .0 cyclopropanecarboxylate [mixture Hop, vines ...... 4 .0 comprising the enantiomeric pair (R)- Horse, fat ...... 2 .0 a-cyano-4-fluoro-3-phenoxybenzyl Horse, meat ...... 0 .05 Horse, meat byproducts ...... 0 .05 (1S,3S)-3-(2,2-dichlorovinyl)-2,2- Lettuce, head ...... 2.0 dimethylcyclopropanecarboxylate and Lettuce, leaf ...... 3 .0 (S)-a-cyano-4-fluoro-3-phenoxybenzyl Milk ...... 0.2 Milk, fat ...... 5 .0 (1R,3R)-3-(2,2-dichlorovinyl)-2,2- Millet, grain ...... 0 .15 dimethylcyclopropanecarboxylate with Mustard greens ...... 7.0 the enantiomeric pair (R)-a-cyano-4- Nut, tree, group 14 ...... 0 .01 fluoro-3-phenoxybenzyl (1S,3R)-3-(2,2- Oat, bran ...... 0 .5 Oat, grain ...... 0 .15 dichlorovinyl)-2,2- Pea and bean, dried shelled, except soybean, dimethylcyclopropanecarboxylate and subgroup 6C ...... 0 .15 (S)-a-cyano-4-fluoro-3-phenoxybenzyl Pea, dry, seed ...... 0 .15 Pea, southern, succulent ...... 0 .25 (1R,3S)-3-(2,2-dichlorovinyl)-2,2- Peanut ...... 0 .01 dimethylcyclopropanecarboxylate], in Peanut, hay ...... 6.0 or on the following raw agricultural Pepper ...... 0 .50 commodities: Pistachio ...... 0.01 Poultry, fat ...... 0.01 Poultry, meat ...... 0 .01 Parts per Commodity million Poultry, meat byproducts ...... 0.01 Radish, roots ...... 1 .0 Alfalfa ...... 5 .0 Rye, bran ...... 0 .5 Alfalfa, forage ...... 5.0 Rye, grain ...... 0.15 Alfalfa, hay ...... 13 Sheep, fat ...... 2 .0 Almond, hulls ...... 0 .5 Sheep, meat ...... 0.05 Barley, bran ...... 0 .5 Sheep, meat byproducts ...... 0 .05 Barley, grain ...... 0 .15 Sorghum, grain, grain ...... 3 .5 Beet, sugar, dried pulp ...... 1 .0 Soybean, forage ...... 8 .0

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Parts per § 180.437 Imazamethabenz-methyl; toler- Commodity million ances for residues. (a) General. Tolerances are established for Soybean, hay ...... 4 .0 residues of the herbicide imazamethabenz- Soybean, seed ...... 0 .03 Sugarcane, cane ...... 0.05 methyl, including its metabolites and Sugarcane, molasses ...... 0 .20 degradates, in or on the commodities in the Sunflower, forage ...... 5.0 table in this paragraph. Compliance with the Sunflower, seed ...... 0.02 tolerance levels specified in this paragraph is Teosinte, grain ...... 0 .05 to be determined by measuring only Tomato ...... 0.20 imazamethabenz-methyl (methyl 2-[4,5- Tomato, paste ...... 0 .5 dihydro-4-methyl-4-(1-methylethyl)-5-oxo-1H- Tomato, pomace ...... 5 .0 imidazol-2-yl]-4-methylbenzoate) or (methyl Triticale, grain ...... 0 .15 2-[4,5-dihydro-4-methyl-4-(1-methylethyl)-5- Turnip, greens ...... 7.0 oxo-1H-imidazol-2-yl]-5-methylbenzoate), as Vegetable, cucurbit, group 9 ...... 0.1 Vegetable, fruiting, group 8 ...... 0.5 the sum of its para- and meta-isomers in or Vegetable, leafy greens, except Brassica, group on the commodity. 4 ...... 6 .0 Vegetable, tuberous and corm, subgroup 1C ..... 0.01 Expiration/ Commodity Parts per revocation Wheat, bran ...... 0.5 million date Wheat, grain ...... 0 .15 Wheat, shorts ...... 0 .5 Barley, grain ...... 0.10 12/31/16 Barley, straw ...... 2.00 12/31/16 (b) Section 18 emergency exemptions. Sunflower, seed ...... 0.10 12/31/16 Wheat, grain ...... 0.10 12/31/16 [Reserved] Wheat, straw ...... 2.00 12/31/16 (c) Tolerances with regional registrations. [Reserved] (b) Section 18 emergency exemptions. [Re- (d) Indirect or inadvertent residues. served] [Reserved] (c) Tolerances with regional registrations. [Reserved] [53 FR 1924, Jan. 25, 1988] (d) Indirect or inadvertent residues. [Re- served] EDITORIAL NOTE: For FEDERAL REGISTER citations affecting § 180.436, see the List of CFR § 180.438 Lambda-cyhalothrin and an Sections Affected, which appears in the isomer gamma-cyhalothrin; toler- Finding Aids section of the printed volume ances for residues. and at www.fdsys.gov. (a) General. (1) Tolerances are estab- § 180.437 Methyl 2-(4-isopropyl-4-meth- lished for the combined residues of the yl-5-oxo-2-imidazolin-2-yl)-p-toluate pyrethroid lambda-cyhalothrin, 1:1 and methyl 6-(4-isopropyl-4-methyl- mixture of (S)-a-cyano-3- 5-oxo-2-imidazolin-2-yl)-m-toluate; phenoxybenzyl-(Z)-(1R,3R)-3-(2-chloro- tolerances for residues. 3,3,3-trifluoroprop-1-enyl)-2,2- Tolerances are established for the dimethylcyclopropanecarboxylate and combined residues of the herbicide (R)-a-cyano-3-phenoxybenzyl-(Z)- methyl 2-(4-isopropyl-4-methyl-5-oxo-2- (1S,3S)-3-(2-chloro-3,3,3-trifluoroprop-1- imidazolin-2-yl)-p-toluate and methyl enyl)-2,2- 6-(4-isopropyl-4-methyl-5-oxo-2- dimethylcyclopropanecarboxylate and imidazolin-2-yl)-m-toluate in or on the its epimer expressed as epimer of lamb- following raw agricultural commod- da-cyhalothrin, a 1:1 mixture of (S)-a- ities: cyano-3-phenoxybenzyl-(Z)-(1S,3S)-3-(2- chloro-3,3,3-trifluoroprop-1-enyl)-2,2- Parts per Commodity million dimethylcyclopropanecarboxylate and (R)-a-cyano-3-phenoxybenzyl-(Z)- Barley, grain ...... 0 .10 (1R,3R)-3-(2-chloro-3,3,3-trifluoroprop-1- Barley, straw ...... 2 .00 Sunflower, seed ...... 0.10 enyl)-2,2- Wheat, grain ...... 0 .10 dimethylcyclopropanecarboxylate, on Wheat, straw ...... 2 .00 plants and livestocks, as indicated in the following table. [53 FR 24069, June 27, 1988] Commodity Parts per EFFECTIVE DATE NOTE: At 81 FR 34905, June million 1, 2016, § 180.437 was revised, effective Nov. 28, Alfalfa, forage ...... 5.0 2016. For the convenience of the user, the re- Alfalfa, hay ...... 6.0 vised text is set forth as follows: Almond, hulls ...... 1 .5

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Parts per Parts per Commodity million Commodity million

Apple, wet pomace ...... 2 .50 Sugarcane, cane ...... 0.05 Avocado, imported ...... 0.20 Sunflower, forage ...... 0.2 Barley, bran ...... 0 .2 Sunflower, seed, hulls ...... 0 .50 Barley, grain ...... 0 .05 Sunflower, refined oil ...... 0.30 Barley, hay ...... 2 .0 Sunflower, seed ...... 0.2 Barley, straw ...... 2 .0 Tomato ...... 0.1 Brassica, head and stem, subgroup 5A ...... 0 .4 Tomato, dry pomace ...... 6.0 Buckwheat, grain ...... 0.05 Tomato, wet pomace ...... 6.0 Canola, refined oil ...... 2 .0 Vegetable, cucurbit, group 9 ...... 0.05 Canola, seed ...... 1 .0 Vegetable, fruiting, group 8 ...... 0.20 Cattle, fat ...... 3.0 Vegetable, legume, edible podded, subgroup 6A 0 .20 Cattle, meat ...... 0 .2 Vegetable, tuberous and corm, subgroup 1C ..... 0.02 Cattle, meat byproducts ...... 0.2 Wheat, grain ...... 0 .05 Corn, field, flour ...... 0 .15 Wheat, forage ...... 2 .0 Corn, field, forage ...... 6 .0 Wheat, hay ...... 2 .0 Corn, field, grain ...... 0 .05 Wheat, straw ...... 2 .0 Corn, field, stover ...... 1 .0 Wheat, bran ...... 0.2 Corn, pop, grain ...... 0.05 Corn, pop, grain, flour ...... 0 .05 (2) Tolerances 1 are established for Corn, pop, stover ...... 1.0 the combined residues of the Corn, sweet, forage ...... 6 .0 Corn, sweet, stover ...... 1 .0 pyrethroid [gamma-cyhalothrin (the Corn, sweet, kernel plus cob with husks re- isolated active isomer of lambda- moved ...... 0 .05 cyhalothrin) (S)-′-cyano-3- Cotton, undelinted seed ...... 0 .05 Egg ...... 0 .01 phenoxybenzyl (Z)-(1R,3R)-3-(2-chloro- Fruit, pome, group 11 ...... 0.30 3,3,3-trifluoroprop-1-enyl)-2,2- Fruit, stone, group 12 ...... 0 .50 dimethylcyclopropanecarboxylate)) Garlic ...... 0 .1 and its epimer (R)-′-cyano-3- Goat, fat ...... 3 .0 Goat, meat ...... 0.2 phenoxybenzyl (Z)-(1R,3R)-3-(2-chloro- Goat, meat byproducts ...... 0 .2 3,3,3-trifluoroprop-1-enyl)-2,2- Grain, aspirated fractions ...... 2 .0 dimethylcyclopropanecarboxylate in/ Grass, forage, fodder and hay, group 17 ...... 7 .0 Hog, fat ...... 0 .2 on the following commodities: Hog, meat ...... 0 .01 Hog, meat byproducts ...... 0 .02 Parts per Commodity million Hop, dried cones ...... 10 .0 Horse, fat ...... 3 .0 Alfalfa, forage ...... 5 Horse, meat ...... 0 .2 Alfalfa, hay ...... 6 Horse, meat byproducts ...... 0 .2 Almond, hulls ...... 1 .5 Lettuce, head ...... 2.0 Apple, pomace, wet ...... 2 .50 Lettuce, leaf ...... 2 .0 Avocado, imported ...... 0.20 Milk, fat (reflecting 0.4 ppm in whole milk) ...... 10 .0 Brassica, head and stem, subgroup 5A ...... 0 .4 Nut, tree, group 14 ...... 0 .05 Canola, seed ...... 0 .15 Oat, grain ...... 0 .05 Cattle, fat ...... 3 Oat, forage ...... 2 .0 Cattle, meat ...... 0 .2 Oat, hay ...... 2.0 Cattle, meat byproducts ...... 0.2 Oat, straw ...... 2.0 Corn, field, flour ...... 0 .15 Onion, bulb ...... 0 .1 Corn, field, forage ...... 6 .0 Pea and bean, dried shelled, except soybean, Corn, field, grain ...... 0 .05 subgroup 6C ...... 0 .10 Corn, field, stover ...... 1 .0 Pea and bean, succulent shelled, subgroup 6B 0 .01 Corn, pop, grain ...... 0.05 Peanut ...... 0 .05 Corn, pop, stover ...... 1.0 Peanut, hay ...... 3.0 Corn, sweet, forage ...... 6 .0 Pistachio ...... 0.05 Corn, sweet, kernel plus cob with husks re- Poultry, fat ...... 0.03 moved ...... 0 .05 Poultry, meat ...... 0 .01 Corn, sweet, stover ...... 1 .0 Poultry, meat byproducts ...... 0.01 Cotton, undelinted seed ...... 0 .05 Rice, grain ...... 1 .0 Egg ...... 0 .01 Rice, hulls ...... 5 .0 Fruit, pome, group 11 ...... 0.30 Rice, wild, grain ...... 1.0 Fruit, stone, group 12 ...... 0 .50 Rye, bran ...... 0 .2 Garlic ...... 0 .10 Rye, grain ...... 0.05 Goat, fat ...... 3 .0 Rye, forage ...... 2 .0 Goat, meat ...... 0.2 Rye, straw ...... 2 .0 Goat, meat byproducts ...... 0 .2 Sheep, fat ...... 3 .0 Grain, aspirated fractions ...... 2 .0 Sheep, meat ...... 0.2 Hog, fat ...... 3 .0 Sheep, meat byproducts ...... 0 .2 Hog, meat ...... 0 .2 Soybean ...... 0.01 Hog, meat byproducts ...... 0 .2 Sorghum, grain, grain ...... 0 .2 Horse, fat ...... 3 .0 Sorghum, grain, forage ...... 0.30 Horse, meat ...... 0 .2 Sorghum, grain, stover ...... 0 .50 Horse, meat byproducts ...... 0 .2

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Commodity Parts per § 180.439 Thifensulfuron methyl; toler- million ances for residues. Lettuce, head ...... 2.0 (a) General. Tolerances are estab- Lettuce, leaf ...... 2 .0 lished for residues of thifensulfuron Milk, fat (reflecting 0.20 ppm in whole milk) ...... 5 .0 Nut, tree, group 14 ...... 0 .05 methyl, including its metabolites and Okra ...... 0.20 degradates, in or on the commodities Onion, bulb ...... 0 .1 listed in the following table [below]. Pea and bean, dried shelled, except soybean, Compliance with the tolerance levels subgroup 6C ...... 0 .10 specified in the following table [below] Pea and bean, succulent shelled, subgroup 6B 0 .01 is to be determined by measuring only Peanut ...... 0 .05 Peanut, hay ...... 3.0 thifensulfuron methyl (methyl 3-[[[[(4- Pistachio ...... 0.05 methoxy-6-methyl-1,3,5-triazin-2- Poultry, fat ...... 0.03 yl)amino]carbonyl]amino] sulfonyl]-2- Poultry, meat ...... 0 .01 thiophenecarboxylate). Poultry, meat byproducts ...... 0.01 Rice, grain ...... 1 .0 Commodity Parts per Rice, hulls ...... 5 .0 million Sheep, fat ...... 3 .0 Sheep, meat ...... 0.2 Barley, grain ...... 0 .05 Sheep, meat byproducts ...... 0 .2 Barley, hay ...... 0 .8 Sorghum, grain, forage ...... 0.30 Barley, straw ...... 0 .10 Sorghum, grain, grain ...... 0 .20 Canola, seed ...... 0 .02 Sorghum, grain, stover ...... 0 .50 Chicory, roots ...... 0 .01 Soybean ...... 0.01 Chicory, tops ...... 0 .01 Sugarcane ...... 0 .05 Corn, field, forage ...... 0 .10 Sunflower, forage ...... 0.20 Corn, field, grain ...... 0 .05 Sunflower, refined oil ...... 0.30 Corn, field, stover ...... 0 .10 Sunflower, seed ...... 0.20 Cotton, gin byproducts ...... 0 .02 Sunflower, seed, hulls ...... 0 .50 Cotton, undelinted seed ...... 0 .02 Tomato ...... 0.10 Flax, seed ...... 0 .02 Tomato, dry pomace ...... 6.0 Oat, forage ...... 0 .2 Tomato, wet pomace ...... 6.0 Oat, grain ...... 0 .05 Vegetables, fruiting, group 8 ...... 0.20 Oat, hay ...... 0.05 Vegetable, legume, edible podded, subgroup 6A 0 .20 Oat, straw ...... 0.10 Wheat, bran ...... 2.0 Rice, grain ...... 0 .05 Wheat, forage ...... 2 .0 Sorghum, grain, forage...... 0 .05 Wheat, grain ...... 0 .05 Sorghum, grain, grain ...... 0 .05 Wheat, hay ...... 2 .0 Sorghum, grain, stover ...... 0 .05 Wheat, straw ...... 2 .0 Soybean ...... 0.10 Wheat, forage ...... 2 .5 1 The analytical enforcement methods for lambda- Wheat, grain ...... 0 .05 cyhalothrin are applicable for determination of gamma- Wheat, hay ...... 0 .7 cyhalothrin residues in plant and animal commodities. Wheat, straw ...... 0 .10 (3) A tolerance of 0.01 part per million is established for residues of the (b) Section 18 emergency exemptions. insecticide lamba-cyhalothrin and an [Reserved] isomer gamma-cyhalothrin in or on all (c) Tolerances with regional registra- food commodities (other than those al- tions. Tolerances are established for ready covered by a higher tolerance as residues of thifensulfuron methyl, in- a result of use on growing crops) in cluding its metabolites and degradates, food-handling establishments where in or on the commodities listed in the food products are held, processed, or following table [below]. Compliance prepared. with the tolerance levels specified in (b) Section 18 emergency exemptions. the following table [below] is to be de- [Reserved] termined by measuring only (c) Tolerances with regional registra- thifensulfuron methyl (methyl 3-[[[[(4- tions. [Reserved] methoxy-6-methyl-1,3,5-triazin-2- (d) Indirect or inadvertent residues. yl)amino]carbonyl]amino] sulfonyl]-2- [Reserved] thiophenecarboxylate).

[71 FR 74817, Dec. 13, 2006, as amended at 72 Commodity Parts per FR 45663, Aug. 15, 2007; 73 FR 39264, July 9, million 2008; 76 FR 34885, June 15, 2011; 80 FR 72599, Safflower, seed ...... 0 .05 Nov. 20, 2015]

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(d) Indirect or inadvertent residues. Commodity Parts per [Reserved] million [69 FR 55982, Sept. 17, 2004, as amended at 69 Barley, grain ...... 0 .05 Barley, hay ...... 0 .05 FR 63957, Nov. 3, 2004; 72 FR 13184, Mar. 21, Barley, straw ...... 0 .05 2007; 73 FR 47075, Aug. 13, 2008; 75 FR 19277, Bean, dry, seed ...... 0 .4 Apr. 14, 2010; 77 FR 52240, Aug. 29, 2012; 80 FR Bean, succulent ...... 0 .25 72599, Nov. 20, 2015] Beet, sugar, molasses ...... 0 .2 Beet, sugar, roots ...... 0 .1 Beet, sugar, tops ...... 0.5 § 180.440 Tefluthrin; tolerances for res- Cotton, undelinted seed ...... 0 .1 idues. Cowpea, forage ...... 3 .0 Cowpea, hay ...... 3 .0 (a) General. Tolerances are estab- Crambe, meal ...... 2 .0 lished for the combined residues of the Flax, seed ...... 0 .05 Gold of pleasure, meal ...... 2.0 insecticide tefluthrin (2,3,5,6 Lentil, seed ...... 0 .05 tetrafluroro-4-methylphenyl)methyl-(1 Pea, dry ...... 0 .25 alpha, 3 alpha)-(Z)-(±)-3(2-chloro-3,3,3- Pea, field, hay ...... 3.0 Pea, field, vines ...... 3 .0 trifluoro-1-propenyl)-2,2- Pea, succulent ...... 0 .3 diemthylcyclopropanecarboxylate) and Peppermint, tops ...... 2 .0 its metabolite (Z)-3-(2-chloro-3,3,3- Rapeseed, meal ...... 2 .0 Rapeseed subgroup 20A, except flax, seed ...... 1 .5 trifluroro-1-propenyl)-2,2- Sorghum, grain, aspirated grain fractions ...... 1 .0 dimethylcyclopropanecarboxylic acid Sorghum, grain, forage ...... 0.20 in or on the following commodities: Sorghum, grain, grain ...... 0 .20 Sorghum, grain, stover ...... 0 .30 Soybean, flour ...... 0 .5 Parts per Soybean, hulls ...... 0 .02 Commodity million Soybean, meal ...... 0.5 Soybean, seed ...... 0 .05 Corn, field, forage ...... 0 .06 Spearmint, tops ...... 2 .0 Corn, field, grain ...... 0 .06 Sunflower, seed ...... 1.9 Corn, field, stover ...... 0 .06 Wheat, forage ...... 0 .05 Corn, pop, grain ...... 0.06 Wheat, grain ...... 0 .05 Corn, pop, stover ...... 0.06 Wheat, hay ...... 0 .05 Corn, sweet, forage ...... 0 .06 Wheat, straw ...... 0 .05 Corn, sweet, kernel plus cob with husks removed ...... 0 .06 (2) Tolerances are established for res- Corn, sweet, stover ...... 0 .06 idues of the herbicide quizalofop ethyl, including its metabolites and (b) Section 18 emergency exemptions. degradates, in or on the commodities [Reserved] in the following table. Compliance with (c) Tolerances with regional registra- the tolerance levels specified in the fol- tions. [Reserved] lowing table is to be determined by (d) Indirect or inadvertent residues. measuring only those quizalofop ethyl [Reserved] residues convertible to quizalofop (2-[4- (6-chloroquinoxalin-2-yl- [62 FR 62961, Nov. 26, 1997, as amended at 74 oxy)phenoxy]propanoic acid), expressed FR 46375, Sept. 9, 2009] as quizalofop, in or on the commodity.

§ 180.441 Quizalofop ethyl; tolerances Parts per for residues. Commodity million

(a) General. (1) Tolerances are estab- Cattle, fat ...... 0.05 lished for residues of the herbicide Cattle, meat ...... 0 .02 Cattle, meat byproducts ...... 0.05 quizalofop ethyl, including its metabo- Egg ...... 0 .02 lites and degradates, in or on the com- Goat, fat ...... 0 .05 modities in the following table. Com- Goat, meat ...... 0.02 Goat, meat byproducts ...... 0 .05 pliance with the tolerance levels speci- Hog, fat ...... 0 .05 fied in the following table is to be de- Hog, meat ...... 0 .02 termined by measuring only those Hog, meat byproducts ...... 0 .05 Horse, fat ...... 0 .05 quizalofop ethyl residues convertible to Horse, meat ...... 0 .02 2-methoxy-6-chloroquinoxaline, ex- Horse, meat byproducts ...... 0 .05 pressed as the stoichiometric equiva- Milk ...... 0.01 Milk, fat ...... 0 .25 lent of quizalofop ethyl, in or on the Poultry, fat ...... 0.05 commodity. Poultry, meat ...... 0 .02

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Parts per Parts per Commodity million Commodity million

Poultry, meat byproducts ...... 0.05 Cattle, meat byproducts ...... 0.10 Sheep, fat ...... 0 .05 Cattle, meat ...... 0 .5 Sheep, meat ...... 0.02 Coriander, dried leaves ...... 25 Sheep, meat byproducts ...... 0 .05 Coriander, leaves ...... 6 .0 Coriander, seed ...... 5 .0 (b) Section 18 emergency exemptions. Corn, field, forage ...... 3 .0 Corn, field, grain ...... 0 .05 [Reserved] Corn, field, stover ...... 5 .0 (c) Tolerances with regional registra- Corn, pop, grain ...... 0.05 tions. Tolerances with regional reg- Corn, pop, stover ...... 5.0 Corn, sweet, forage ...... 3 .0 istration are established for residues of Corn, sweet, kernel plus cob with husk removed 0.05 the herbicide quizalofop ethyl, includ- Corn, sweet, stover ...... 5 .0 ing its metabolites and degradates, in Cotton, undelinted seed ...... 0 .5 or on the commodities in the following Eggplant ...... 0.05 Egg ...... 0 .05 table. Compliance with the tolerance Fruit, citrus, group 10 ...... 0 .05 levels specified in the following table is Goat, fat ...... 1 .0 to be determined by measuring only Goat, meat byproducts ...... 0 .10 Goat, meat ...... 0.5 those quizalofop ethyl residues con- Grain, aspirated fractions ...... 70 vertible to 2-methoxy-6- Grape ...... 0 .2 chloroquinoxaline, expressed as the Groundcherry ...... 0 .5 stoichiometric equivalent of quizalofop Herb subgroup 19A ...... 0 .05 Hog, fat ...... 1 .0 ethyl, in or on the commodity. Hog, meat byproducts ...... 0 .10 Hog, meat ...... 0 .5 Commodity Parts per Hop, dried cones ...... 10 .0 million Horse, fat ...... 1 .0 Horse, meat byproducts ...... 0 .10 Pineapple ...... 0.1 Horse, meat ...... 0 .5 Leafy petioles subgroup 4B ...... 3 .0 (d) Indirect or inadvertent residues. Lettuce, head ...... 3.0 [Reserved] Mayhaw ...... 1 .4 Milk, fat (reflecting 0.1 ppm in whole milk) ...... 1 .0 [63 FR 32759, June 16, 1998, as amended at 70 Nut, tree, group 14 ...... 0 .05 FR 7870, Feb. 16, 2005; 71 FR 56378, Sept. 27, Okra ...... 0.50 2006; 76 FR 56045, Sept. 15, 2010; 77 FR 23630, Pea and bean, dried shelled, expect soybean, Apr. 20, 2012; 80 FR 72599, Nov. 20, 2015] subgroup 6C ...... 0 .15 Pea and bean, succulent shelled, subgroup 6B 0 .05 Peanut ...... 0 .05 § 180.442 Bifenthrin; tolerances for res- Pear ...... 0 .5 idues. Pepino ...... 0 .5 Pepper, bell ...... 0 .5 (a) General. (1) Tolerances are estab- Pepper, nonbell ...... 0 .5 lished for residues of the insecticide Pistachio ...... 0.05 bifenthrin, including its metabolites Poultry, fat ...... 0.05 and degradates, in or on the commod- Poultry, meat byproducts ...... 0.05 Poultry, meat ...... 0 .05 ities in the table below. Compliance Radish, tops ...... 4 .5 with the tolerance levels specified Rapeseed, seed ...... 0 .05 below is to be determined by measuring Sheep, fat ...... 1 .0 ′ Sheep, meat byproducts ...... 0 .1 only bifenthrin, (2-methyl [1,1 - Sheep, meat ...... 0.5 biphenyl]-3-yl) methyl-3-(2-chloro- Soybean, hulls ...... 0 .50 3,3,3,-trifluoro-1-propenyl)-2,2- Soybean, refined oil ...... 0 .30 dimethylcyclopropanecarboxylate. Soybean, seed ...... 0 .2 Spinach ...... 0 .2 Strawberry ...... 3 .0 Parts per 1 Commodity million Tea, dried ...... 30 Tomato ...... 0.15 Almond, hulls ...... 2 .0 Turnip, greens ...... 3.5 Artichoke, globe ...... 1.0 Vegetable, cucurbit, group 9 ...... 0.4 Banana 1 ...... 0.1 Vegetable, legume, edible podded, subgroup 6A 0 .6 Beet, garden, roots ...... 0 .45 Vegetable, root, subgroup 1B except sugar beet Beet, garden, tops ...... 15 and garden beet ...... 0 .10 Brassica, head and stem, subgroup 5A, except Vegetable, tuberous and corm, subgroup 1C ..... 0.05 cabbage ...... 0 .6 1 There are no U.S. registrations. Brassica, leafy greens, subgroup 5B ...... 3 .5 Bushberry subgroup 13-07B ...... 1 .8 (2) A tolerance of 0.05 ppm is estab- Cabbage ...... 4 .0 Caneberry subgroup 13A ...... 1 .0 lished for residues of the insecticide Cattle, fat ...... 1.0 bifenthrin, (2-methyl[1,1′-biphenyl]-3-

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yl)methyl-3-(2-chloro-3,3,3-trifluoro-1- dimethylcyclopropanecarboxylate. propenyl)-2,2-dimethylcyclopropane- These tolerances will expire and are re- carboxylate, as follows: voked on the dates specified in the fol- (i) In or on all food/feed items (other lowing table: than those covered by a higher toler- Expiration/ ance as a result of use on growing Commodity Parts per revocation crops) in food/feed handling establish- million date ments. Apple ...... 0.5 12/31/18 (ii) The insecticide may be present as Nectarine ...... 0.5 12/31/18 a residue from application of bifenthrin Peach ...... 0.5 12/31/18 in food handling establishments, including food service, manufacturing (c) Tolerances with regional registra- and processing establishments, such as tions. Tolerances with regional reg- restaurants, cafeterias, supermarkets, istrations are established for residues bakeries, breweries, dairies, meat of the insecticide bifenthrin, including slaughtering and packing plants, and its metabolites and degradates, in or canneries, feed handling establish- on the commodities in the table below. ments including feed manufacturing Compliance with the tolerance levels and processing establishments, in ac- specified below is to be determined by cordance with the following prescribed measuring only bifenthrin, (2-methyl conditions: [1,1′-biphenyl]-3-yl) methyl-3-(2-chloro- (A) Application shall be limited to 3,3,3,-trifluoro-1-propenyl)-2,2- general surface and spot and/or crack dimethylcyclopropanecarboxylate. and crevice treatment in food/feed han- Parts per dling establishments where food/feed Commodity million and food/feed products are held, proc- Grass, forage ...... 4 .0 essed, prepared and served. General Grass, hay ...... 15 surface application may be used only when the facility is not in operation (d) Indirect or inadvertent residues. provided exposed food/feed has been [Reserved] covered or removed from the area [62 FR 31002, June 6, 1997] being treated. Spot and/or crack and crevice application may be used while EDITORIAL NOTE: For FEDERAL REGISTER ci- the facility is in operation provided ex- tations affecting § 180.442, see the List of CFR posed food/feed is covered or removed Sections Affected, which appears in the Finding Aids section of the printed volume from the area being treated prior to ap- and at www.fdsys.gov. plication. Spray concentration shall be limited to a maximum of 0.06 percent § 180.443 Myclobutanil; tolerances for active ingredient. Contamination of residues. food/feed or food/feed contact surfaces (a) General. Tolerances are estab- shall be avoided. lished for combined residues of the fun- (B) To assure safe use of the insecti- gicide myclobutanil alpha-butyl-alpha- cide, its label and labeling shall con- (4-chlorophenyl)-1H-1,2,4-triazole-1- form to that registered with the U.S. propanenitrile and its alcohol metabo- Environmental Protection Agency and lite (alpha-(3-hydroxybutyl)-alpha-(4- shall be used in accordance with such chlorophenyl)-1H-1,2,4-triazole-1- label and labeling. propanenitrile (free and bound), in or (b) Section 18 emergency exemptions. on the following food commodities: Time-limited tolerances are established for residues of the insecticide Commodity Parts per bifenthrin, including its metabolites million and degradates, in connection with use Almond ...... 0.1 of the pesticide under a Section 18 Almond, hulls ...... 2 .0 Apple ...... 0.5 emergency exemption granted by EPA. Apple, dry pomace ...... 5.0 Compliance with the tolerance levels Apple, wet pomace ...... 5 .0 specified below is to be determined by Artichoke, globe ...... 0.90 measuring only bifenthrin, (2-methyl Asparagus ...... 0.02 Banana, postharvest ...... 4 .0 [1,1′-biphenyl]-3-yl) methyl-3-(2-chloro- Bean, snap, succulent ...... 1 .0 3,3,3,-trifluoro-1-propenyl)-2,2- Caneberry subgroup 13A ...... 2 .0

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triazole-1-propanenitrile in or on the Commodity Parts per million following food commodities: Canistel ...... 3 .0 Cattle, fat ...... 0.05 Parts per Commodity million Cattle, liver ...... 1 .0 Cattle, meat ...... 0 .1 Animal feed, nongrass, group 18 ...... 0 .03 Cattle, meat byproducts, except liver ...... 0 .2 Grain, cereal, forage, fodder and straw, group Cherry, sweet ...... 5 .0 16 ...... 0 .03 Cherry, tart ...... 5 .0 Cilantro, leaves ...... 9 .0 Grain, cereal, group 15 ...... 0.03 Cotton, undelinted seed ...... 0 .02 Vegetable, brassica, leafy, group 5 ...... 0.03 Currant ...... 3 .0 Vegetable, foliage of legume, group 7 ...... 0 .03 Egg ...... 0 .02 Vegetable, fruiting, group 8 ...... 0.03 Fruit, stone, except cherry ...... 2.0 Vegetable, leafy, except brassica, group 4 ...... 0 .03 Goat, fat ...... 0 .05 Vegetable, leaves of root and tuber, group 2 ..... 0 .03 Goat, liver ...... 1.0 Vegetable, legume, group 6 ...... 0 .03 Goat, meat ...... 0.1 Vegetable, root and tuber, group 1 ...... 0 .03 Goat, meat byproducts, except liver ...... 0 .2 Gooseberry ...... 2 .0 Grain, aspirated fractions ...... 35 [54 FR 6131, Feb. 8, 1989] Grape ...... 1 .0 Grape, dried pomace ...... 10 .0 EDITORIAL NOTE: For FEDERAL REGISTER ci- Grape, raisin ...... 10.0 tations affecting § 180.443, see the List of CFR Grape, raisin, waste ...... 25 .0 Sections Affected, which appears in the Grape, wet pomace ...... 10 .0 Finding Aids section of the printed volume Hog, fat ...... 0 .05 and at www.fdsys.gov. Hog, liver ...... 1 .0 Hog, meat ...... 0 .1 Hog, meat byproducts, except liver ...... 0 .2 § 180.444 Sulfur dioxide; tolerances for Hop, dried cones ...... 10 residues. Horse, fat ...... 0 .05 Horse, liver ...... 1 .0 (a) General. A tolerance is established Horse, meat ...... 0 .1 as follows for sulfite residues of the Horse, meat byproducts, except liver ...... 0 .2 fungicide sulfur dioxide (determined as Leafy greens, subgroup 4A, except spinach ...... 9 .0 Mango ...... 3.0 (SO2)) in or on the following raw agri- Mayhaw ...... 0 .70 cultural commodity(ies): Milk ...... 0.2 Okra ...... 4.0 Parts per Papaya ...... 3 .0 Commodity million Peppermint, tops ...... 3 .0 Plum, prune, dried ...... 8.0 Grape, postharvest ...... 10.0 Poultry, fat ...... 0.02 Poultry, meat ...... 0 .02 Poultry, meat byproducts ...... 0.02 (b) Section 18 emergency exemptions. Sapodilla ...... 3 .0 Time-limited tolerances specified in Sapote, black ...... 3 .0 the following table are established for Sapote, mamey ...... 3 .0 residues of sulfur dioxide, including its Sheep, fat ...... 0 .05 Sheep, liver ...... 1.0 metabolites and degradates in or on Sheep, meat ...... 0.1 the specified agricultural commodities, Sheep, meat byproducts, except liver ...... 0 .2 resulting from use of the pesticide pur- Soybean, forage ...... 3 .5 Soybean, hay ...... 15 suant to FFIFRA section 18 emergency Soybean, refined oil ...... 0 .40 exemptions. Compliance with the toler- Soybean, seed ...... 0 .25 ance levels specified below is to be de- Spearmint, tops ...... 3 .0 Star apple ...... 3 .0 termined by measuring only sulfur di- Strawberry ...... 0 .50 oxide (SO2). The tolerances expire on Tomato ...... 0.30 the date specified in the table. Tomato, puree ...... 0 .50 Tomato, paste ...... 1 .0 Expiration/ Vegetable, cucurbit, group 9 ...... 0.20 Parts per Commodity million revocation Vegetable, fruiting, group 8, except tomato ...... 4 .0 date

(b) Section 18 emergency exemptions. Fig ...... 10 12/31/14 [Reserved] (c) Tolerances with regional registra- (c) Tolerances with regional registrations. [Reserved] tions. [Reserved] (d) Indirect or inadvertent residues. (d) Indirect or inadvertent residues. Tolerances are established for residues [Reserved] of the fungicide myclobutanil alpha- [54 FR 20126, May 10, 1989, as amended at 76 butyl-alpha-(4-chlorophenyl)-1H-1,2,4- FR 56648, Sept. 14, 2011]

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§ 180.445 Bensulfuron methyl; toler- by measuring only the sum of ances for residues. clofentezine, 3,6-bis(2-chlorophenyl)- (a) General. Tolerances are estab- 1,2,4,5-tetrazine, and its metabolite, 3- lished for residues of the herbicide (2-chloro-4-hydroxyphenyl)-6-(2- bensulfuron methyl (methyl-2[[[[[(4,6- chlorophenyl)-1,2,4,5-tetrazine, cal- dimethoxy-pyrimidin-2-yl) amino] car- culated as the stoichiometric equiva- bonyl] amino] sulfonyl] methyl] ben- lent of clofentezine, in or on com- zoate) in or on the following raw agri- modity. cultural commodities: Parts per Commodity million Commodity Parts per million Cattle, fat ...... 0.05 Cattle, liver ...... 0 .4 Crayfish ...... 0.05 Cattle, meat ...... 0 .05 Rice, grain ...... 0 .02 Cattle, meat byproducts, except liver ...... 0 .05 Goat, fat ...... 0 .05 (b) Section 18 emergency exemptions. Goat, liver ...... 0.4 [Reserved] Goat, meat ...... 0.05 (c) Tolerances with regional registra- Goat, meat byproducts, except liver ...... 0 .05 Hog, fat ...... 0 .05 tions. [Reserved] Hog, liver ...... 0 .4 (d) Indirect or inadvertent residues. Hog, meat ...... 0 .05 [Reserved] Hog, meat byproducts, except liver ...... 0 .05 Horse, fat ...... 0 .05 [63 FR 9435, Feb. 25, 1998, as amended at 80 Horse, liver ...... 0 .4 FR 72599, Nov. 20, 2015] Horse, meat ...... 0 .05 Horse, meat byproducts, except liver ...... 0 .05 § 180.446 Clofentezine; tolerances for Milk ...... 0.01 Sheep, fat ...... 0 .05 residues. Sheep, liver ...... 0.4 (a) General. (1) Tolerances are estab- Sheep, meat ...... 0.05 lished for residues of the insecticide Sheep, meat byproducts, except liver ...... 0 .05 clofentezine, including its metabolites (b) Section 18 emergency exemptions. and degradates, in or on the commod- [Reserved] ities in the table in this paragraph. (c) Tolerances with regional registra- Compliance with the tolerance levels tions. [Reserved] specified in this paragraph is to be de- (d) termined by measuring only Indirect or inadvertent residues. [Reserved] clofentezine, 3,6-bis(2-chlorophenyl)- 1,2,4,5-tetrazine, in or on the com- [56 FR 15503, Apr. 17, 1991, as amended at 56 modity. FR 22335, May 15, 1991; 59 FR 26947, May 25, 1994; 60 FR 12709, Mar. 8, 1995; 64 FR 19050, Commodity Parts per Apr. 19, 1999; 70 FR 11572, Mar. 9, 2005; 74 FR million 46375, Sept. 9, 2009; 76 FR 23496, Apr. 27, 2011; Almond, hulls ...... 5 .0 81 FR 38609, June 14, 2016] Almond ...... 0.5 Apple, dry pomace ...... 3.0 § 180.447 Imazethapyr; tolerances for Apple, wet pomace ...... 3 .0 residues. Apricot ...... 1 .0 Avocado ...... 0 .30 (a) General. (1) Tolerances are estab- Cherry, subgroup 12–12A ...... 1.0 lished for residues of the herbicide Fruit, pome, group 11–10 ...... 0 .50 imazethapyr, 2-[4,5-dihydro-4-methyl-4- Fruit, small, vine climbing, except fuzzy kiwifruit, Subgroup 13–07F ...... 1 .0 (1-methylethyl)-5-oxo- 1H-imidazol-2- Persimmon ...... 0 .05 yl]-5-ethyl-3-pyridine carboxylic acid, Papaya ...... 0 .30 applied as its acid or ammonium salt, Peach, subgroup 12–12B ...... 1 .0 Walnut ...... 0 .02 in or on the following raw agricultural commodities: (2) Tolerances are established for res- Parts per idues of the insecticide clofentezine, Commodity million including its metabolites and Canola, seed 1 ...... 0 .10 degradates, in or on the commodities Soybean ...... 0.1 in the table in this paragraph. Compli- Vegetable, legume, group 6 ...... 0 .1 ance with the tolerance levels specified 1 There are no U.S. registrations for canola as of March in this paragraph is to be determined 21, 2003.

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(2) Tolerances are established for the methylethyl)-5-oxo-1H-imidazol-2-yl]-5- sum of the residues of the herbicide (1- hydroxyethyl)-3-pyridine carboxylic imazethapyr, 2-[4,5-dihydro-4-methyl-4- acid, both free and conjugated, applied (1-methylethyl)-5-oxo- 1H-imidazol-2- as its acid or ammonium salt, in or on yl]-5-ethyl-3-pyridine carboxylic acid; the following raw agricultural com- its metabolite CL 288511, 2-[4,5-dihydro- modities: 4-methyl-4-(1-methylethyl)-5-oxo-1H- Parts per imidazol-2-yl]-5-(1-hydroxyethyl)-3-pyr- Commodity million idine carboxylic acid; and its metabolite CL 182704, 5-[1-(beta-D- Endive ...... 0.1 Lettuce, head ...... 0.1 glucopyranosyloxy)ethyl]-2-[4,5- Lettuce, leaf ...... 0 .1 dihydro-4-methyl-4-(1-methylethyl)-5- oxo-1H-imidazol-2-yl]-3- (d) Indirect or inadvertent residues. pyridinecarboxylic acid, applied as its [Reserved] acid or ammonium salt, in or on the [67 FR 55331, Aug. 29, 2002, as amended at 68 following commodities: FR 13849, Mar. 21, 2003; 71 FR 6359, Feb. 8, Parts per 2006; 76 FR 34885, June 15, 2011; 80 FR 72599, Commodity million Nov. 20, 2015] Alfalfa, seed ...... 0 .15 § 180.448 Hexythiazox; tolerance for Alfalfa, seed screenings ...... 0 .15 residues. Animal feed, nongrass, group 18, forage ...... 3 .0 Animal feed, nongrass, group 18, hay ...... 5.5 (a) General. Tolerances are estab- Peanut ...... 0 .1 lished for residues of hexythiazox, in- Rice, bran ...... 1.2 Rice, grain ...... 0 .3 cluding its metabolites and degradates, in or on the commodities in the table (3) A tolerance is established for the below. Compliance with the tolerance sum of residues of the herbicide levels specified below is to be deter- imazethapyr, 2-[4,5-dihydro-4-methyl-4- mined by measuring only hexythiazox (1-methylethyl)-5-oxo- 1H-imidazol-2- and its metabolites containing the (4- yl]-5-ethyl-3-pyridine carboxylic acid, chlorophenyl)-4-methyl-2-oxo-3- and its metabolite CL 288511, 2-[4,5- thiazolidine moiety, calculated as the dihydro-4-methyl-4-(1-methylethyl)-5- stoichiometric equivalent of oxo-1H-imidazol-2-yl]-5-(1-hydroxy- hexythiazox. ethyl)-3-pyridine carboxylic acid, ap- Parts per plied as its acid or ammonium salt, in Commodity million or on the following commodities: Almond, hulls ...... 10 Parts per Apple, wet pomace ...... 0 .40 Commodity million Berry, low growing, subgroup 13–07G ...... 6 Caneberry subgroup 13–07A ...... 1 Cattle, meat byproducts ...... 0.10 Cattle, fat ...... 0.05 Corn, field, forage ...... 0 .1 Cattle, meat byproducts ...... 0.5 Corn, field, grain ...... 0 .1 Citrus, oil ...... 25 Corn, field, stover ...... 0 .1 Corn, field, forage ...... 3 .0 Crayfish ...... 0.15 Corn, field, grain ...... 0 .02 Goat, meat byproducts ...... 0 .10 Corn, field, stover ...... 7 .0 Hog, meat byproducts ...... 0 .10 Cotton, gin byproducts ...... 15 Horse, meat byproducts ...... 0 .10 Cotton, undelinted seed ...... 0 .4 Sheep, meat byproducts ...... 0 .10 Date, dried fruit ...... 1 .0 Egg ...... 0 .05 Fruit, pome, group 11–10 ...... 0 .4 (b) Section 18 emergency exemptions. Fruit, small, vine climbing, subgroup 13–07F, [Reserved] except fuzzy kiwifruit ...... 1 (c) Tolerances with regional registra- Fruit, stone, group 12 ...... 1 .0 tions. Tolerances with regional reg- Goat, fat ...... 0 .05 Goat, meat byproducts ...... 0 .5 istration, as defined in § 180.1(l) of this Grain, aspirated fractions ...... 5 chapter, are established for the sum of Hog, fat ...... 0 .02 residues of the herbicide imazethapyr, Hog, meat byproducts ...... 0 .05 Hop, dried cones ...... 2 .0 2- [4,5-dihydro-4-methyl-4-(1- Horse, fat ...... 0 .05 methylethyl)-5-oxo-1H-imidazol-2-yl]-5- Horse, meat byproducts ...... 0 .5 ethyl- 3-pyridine carboxylic acid, as its Milk ...... 0.05 Nut, tree, group 14 ...... 0 .30 ammonium salt, and its metabolite, 2- Pepper/eggplant subgroup 8–10B ...... 1 .5 [4,5-dihydro-4-methyl-4-(1- Peppermint, tops ...... 2 .0

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Parts per Parts per Commodity million Commodity million

Pistachio ...... 0.30 Wheat, hay (EPA Regions 9–12 only) ...... 30 Plum, prune, dried ...... 1.3 Wheat, straw (EPA Regions 9–12 only) ...... 8.0 Poultry, fat ...... 0.05 Poultry, meat byproducts ...... 0.05 Sheep, fat ...... 0 .05 (d) Indirect or inadvertent residues. Sheep, meat byproducts ...... 0 .5 [Reserved] Spearmint, tops ...... 2 .0 Tomato ...... 0.50 [54 FR 17948, Apr. 26, 1989]

(b) Section 18 emergency exemptions. A EDITORIAL NOTE: For FEDERAL REGISTER ci- time-limited tolerance specified in the tations affecting § 180.448, see the List of CFR Sections Affected, which appears in the following table is established for resi- Finding Aids section of the printed volume dues of hexythiazox and its metabolites and at www.fdsys.gov. containing the (4-chlorophenyl)-4-

methyl-2-oxo-3-thiazolidine moiety, § 180.449 Avermectin B 1 and its delta- calculated as the stoichiometric equiv- 8,9-isomer; tolerances for residues. alent of hexythiazox, in or on the spec- (a) General. Tolerances are estab- ified agricultural commodity, resulting lished for residues of abamectin, in- from use of the pesticide pursuant to cluding its metabolites and degradates, FIFRA section 18 emergency exemp- in or on the commodities in the fol- tions. The tolerance expires on the lowing table. Compliance with the tol- date specified in the table. erance levels specified in the following Parts per Expiration table is to be determined by measuring Commodity million date only avermectin B1 a mixture of Beet, sugar, root ...... 0.15 12/31/19 avermectins containing greater than or equal to 80% avermectin B1 a (5-O- (c) Tolerances with regional registra- demethyl avermectin A1) and less than tions. Tolerances with regional reg- or equal to 20% avermectin B1b (5-O- istrations as defined by § 180.1(l), are es- demethyl-25-de(1-methylpropyl)-25-(1- tablished for residues of hexythiazox, methylethyl) avermectin A1) and its including its metabolites and delta-8,9-isomer in or on the following degradates, in or on the commodities commodities: in the table below. Compliance with the tolerance levels specified below is OMMODITY to be determined by measuring only Parts per hexythiazox and its metabolites con- Commodity million taining the (4-chlorophenyl)-4-methyl- 2-oxo-3-thiazolidine moiety, calculated Acerola ...... 0.015 as the stoichiometric equivalent of Almond, hulls ...... 0 .10 Apple, wet pomace ...... 0 .10 hexythiazox. Avocado ...... 0 .020 Bean ...... 0 .015 Parts per Commodity million Berry, low growing, subgroup 13–07G ...... 0 .05 Black sapote ...... 0 .40 Alfalfa, forage (EPA Regions 9–11 only) ...... 15 Caneberry subgroup 13–07A ...... 0.20 Alfalfa, hay (EPA Regions 9–11 only) ...... 30 Canistel ...... 0 .40 Bean, dried, seed (EPA Regions 7–12 only) ...... 0 .4 Cattle, fat ...... 0.05 Bean, succulent (EPA Regions 7–12 only) ...... 0.3 Cattle, meat ...... 0 .02 Corn, field, forage ...... 6 .0 Cattle, meat byproducts ...... 0.09 Corn, field, grain ...... 0 .02 Corn, field, stover ...... 2 .5 Celeriac, roots ...... 0 .05 Corn, sweet, forage (EPA Regions 7–12 only) ... 4 .0 Celeriac, tops ...... 0 .05 Corn, sweet, kernel plus cob with husks re- Chive, dried leaves ...... 0 .02 moved (EPA Regions 7–12 only) ...... 0 .1 Chive, fresh leaves ...... 0 .01 Fruit, citrus group 10–10 (CA, AZ, TX only) ...... 0 .6 Citrus, dried pulp ...... 0 .10 Fruit, citrus group 10 (CA, AZ, TX only) ...... 0 .35 Citrus, oil ...... 0.10 Potato ...... 0 .02 Corn, sweet, forage ...... 0 .20 Sorghum, grain, forage (EPA Regions 6–8 only) 5 Corn, sweet, kernel plus cob with husk re- Sorghum, grain, grain (EPA Regions 6–8 only) .. 3 moved ...... 0 .01 Sorghum, grain, stover (EPA Regions 6–8 only) 6 Timothy, forage (EPA Regions 9–11 only) ...... 40 Corn, sweet, stover ...... 0 .50 Timothy, hay (EPA Regions 9–11 only) ...... 40 Cotton, gin byproducts ...... 1 .0 Wheat, forage (EPA Regions 9–12 only) ...... 6 .0 Cotton, undelinted seed ...... 0 .02 Wheat, grain (EPA Regions 9–12 only) ...... 0 .02 Feijoa ...... 0 .015

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OMMODITY—Continued Finding Aids section of the printed volume and at www.fdsys.gov. Commodity Parts per million § 180.450 Beta-(4-Chlorophenoxy)- Food products in food handling establishments alpha-(1,1-dimethylethyl)-1H-1,2,4- (other than those already covered by higher triazole-1-ethanol; tolerances for tolerances as a result of use on growing residues. crops, and other than those already covered (a) General. Tolerances are estab- by tolerances on milk, meat, and meat byproducts) ...... 0.01 lished for the combined residues of the Fruit, citrus, group 10–10 ...... 0 .02 fungicide b-(4-chlorophenoxy)-a-(1,1- Fruit, pome, group 11–10 ...... 0 .02 dimethylethyl)-1H-1,2,4-triazole-1-eth- Fruit, small vine climbing, except fuzzy kiwifruit, subgroup 13–07F ...... 0.02 anol (triadimenol) and its butanediol Fruit, stone, group 12–12 ...... 0 .09 metabolite, 4-(4-chlorophenoxy)-2,2-di- Goat, fat ...... 0 .03 methyl-4-(1H-1,2,4-triazol-l-yl)-1,3- Goat, meat ...... 0.02 Goat, meat byproducts ...... 0 .04 butanediol, calculated as triadimenol, Grain, aspirated grain fractions ...... 0 .40 in or on the following commodities: Guava ...... 0 .015 Herb subgroup 19A, except chive ...... 0 .030 Parts per Expiration/ Hog, fat ...... 0 .01 Commodity million Revocation Hog, meat ...... 0 .02 Date Hog, meat byproducts ...... 0 .02 1 Hop, dried cones ...... 0 .20 Banana ...... 0.2 None Horse, fat ...... 0 .03 Barley, grain ...... 0.05 None Horse, meat ...... 0 .02 Barley, straw ...... 0.2 None Horse, meat byproducts ...... 0 .04 Corn, field, forage ...... 0.05 None Jaboticaba ...... 0 .015 Corn, field, grain ...... 0.05 None Longan ...... 0 .01 Corn, field, stover ...... 0.05 None Lychee ...... 0 .01 Corn, pop, grain ...... 0.05 None Mamey sapote ...... 0 .40 Corn, pop, stover ...... 0.05 None Milk ...... 0.015 Corn, sweet, forage ...... 0.05 None Nut, tree, group 14–12 ...... 0 .01 Corn, sweet, kernel plus cob with Onion, bulb, subgroup 3–07A ...... 0 .01 husks removed ...... 0.05 None Onion, green, subgroup 3–07B ...... 0 .08 Corn, sweet, stover ...... 0.05 None Cotton, undelinted seed ...... 0.02 None Papaya ...... 0 .40 Oat, forage ...... 2.5 None Passionfruit ...... 0 .015 Oat, grain ...... 0.05 None Peppermint, tops ...... 0 .010 Oat, straw ...... 0.2 None Pineapple ...... 0.015 Rye, forage ...... 2.5 None Plum, prune, dried ...... 0.025 Rye, grain ...... 0.05 None Poultry, meat ...... 0 .02 Rye, straw ...... 0.1 None Poultry, meat byproducts ...... 0.02 Wheat, forage ...... 2.5 None Pulasan ...... 0 .01 Wheat, grain ...... 0.05 None Rambutan ...... 0 .01 Wheat, straw ...... 0.2 None Sapodilla ...... 0 .40 Sheep, fat ...... 0 .03 1 There are no U.S. registrations for banana (whole) as of Sheep, meat ...... 0.02 September 22, 1993. Sheep, meat byproducts ...... 0 .04 Soybean, forage ...... 0 .30 (b) Section 18 emergency exemptions. Soybean, hay ...... 1 .0 [Reserved] Soybean, seed ...... 0 .01 (c) Tolerances with regional registra- Spanish lime ...... 0 .01 Spearmint, tops ...... 0 .010 tions. [Reserved] Star apple ...... 0 .40 (d) Indirect or inadvertent residues. Starfruit ...... 0 .015 [Reserved] Vegetable, cucurbit, group 9 ...... 0.005 Vegetable, fruiting, group 8–10 ...... 0 .07 [73 FR 54962, Sept. 24, 2008, as amended at 74 Vegetable, leafy, except brassica, group 4 ...... 0 .10 FR 47457, Sept. 16, 2009; 76 FR 34885, June 15, Vegetable, tuberous and corm, subgroup 01C 0 .01 2011] Wax jambu ...... 0 .015 § 180.451 Tribenuron methyl; toler- (b) Section 18 emergency exemptions. ances for residues. [Reserved] (a) General. Tolerances are estab- (c) Tolerances with regional registra- lished for residues of the herbicide tions. [Reserved] tribenuron methyl and its metabolites (d) Indirect or inadvertent residues. and degradates in or on the commod- [Reserved] ities in the following table. Compliance [62 FR 44095, Aug. 19, 1997] with the tolerance levels specified EDITORIAL NOTE: For FEDERAL REGISTER ci- below is to be determined by measuring tations affecting § 180.449, see the List of CFR only tribenuron methyl, methyl-2- Sections Affected, which appears in the [[[[N-(4-methoxy-6-methyl-1,3,5-triazin-

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2-yl) methylamino] carbonyl] amino] pyrimidin-2-yl]-1-(2- sulfonyl] benzoate, in or on the fol- methoxycarbonylphenylsulfonyl) urea) lowing commodities: in or on the following raw agricultural commodities. Parts per Commodity million Parts per Commodity million Barley, grain ...... 0 .05 Barley, hay ...... 0 .4 Cattle, fat ...... 0.10 Barley, straw ...... 0 .10 Cattle, meat ...... 0 .10 Canola, seed ...... 0 .02 Cattle, meat byproducts ...... 0.10 Corn, field, forage ...... 0 .15 Corn, field, forage ...... 0 .10 Corn, field, grain ...... 0 .01 Corn, field, grain ...... 0 .02 Corn, field, stover ...... 1 .1 Corn, field, stover ...... 0 .10 Cotton, gin byproducts ...... 0 .02 Corn, pop, grain ...... 0.02 Cotton, undelinted seed ...... 0 .02 Corn, pop, stover ...... 0.10 Flax, seed ...... 0 .02 Egg ...... 0 .10 Grain, aspirated fractions ...... 1 .5 Goat, fat ...... 0 .10 Oat, forage ...... 0 .05 Goat, meat ...... 0.10 Oat, grain ...... 0 .05 Goat, meat byproducts ...... 0 .10 Oat, hay ...... 0.05 Hog, fat ...... 0 .10 Oat, straw ...... 0.10 Hog, meat ...... 0 .10 Rice, grain ...... 0 .05 Sorghum, grain, forage ...... 0.05 Hog, meat byproducts ...... 0 .10 Sorghum, grain, grain ...... 0 .05 Horse, fat ...... 0 .10 Sorghum, grain, stover ...... 0 .05 Horse, meat ...... 0 .10 Soybean, forage ...... 0 .07 Horse, meat byproducts ...... 0 .10 Soybean, hay ...... 0 .35 Milk ...... 0.02 Soybean, hulls ...... 0 .04 Poultry, fat ...... 0.10 Soybean, seed ...... 0 .01 Poultry, meat ...... 0 .10 Sunflower, seed ...... 0.05 Poultry, meat byproducts ...... 0.10 Wheat, forage ...... 0 .3 Sheep, fat ...... 0 .10 Wheat, grain ...... 0 .05 Sheep, meat ...... 0.10 Wheat, hay ...... 0 .5 Sheep, meat byproducts ...... 0 .10 Wheat, straw ...... 0 .10 (b) Section 18 emergency exemptions. (b) Section 18 emergency exemptions. [Reserved] [Reserved] (c) Tolerances with regional registra- (c) Tolerances with regional registrations. [Reserved] tions. Tolerances with regional reg- (d) Indirect or inadvertent residues. istration, as defined in § 180.1(l) are es- [Reserved] tablished for residues of the herbicide [55 FR 21548, May 25, 1990, as amended at 62 tribenuron methyl (methyl-2-[[[[N-(4- FR 66020, Dec. 17, 1997; 63 FR 66458, Dec. 2, methoxy-6-methyl-1,3,5-triazin-2-yl) 1998; 67 FR 35049, May 17, 2002; 74 FR 46375, methylamino] car- Sept. 9, 2009; 74 FR 46699, Sept. 11, 2009; 77 FR bonyl]amino]sulfonyl] benzoate) in or 59128, Sept. 26, 2012] on the following raw agricultural commodities: § 180.454 Nicosulfuron; tolerances for residues. Parts per Commodity million (a) General. Tolerances are established for residues of the herbicide Grass, forage, fodder and hay, group 17, ex- nicosulfuron, including its metabolites cept bermudagrass; forage ...... 0 .10 Grass, forage, fodder and hay, group 17, ex- and degradates, in or on the commod- cept bermudagrass; hay ...... 0 .10 ities in the following table. Compliance with the tolerance levels specified in (d) Indirect or inadvertent residues. the following table is to be determined [Reserved] by measuring only nicosulfuron, 2- [69 FR 56718, Sept. 22, 2004, as amended at 72 [[[[(4,6-dimethoxy-2- FR 11789, Mar. 14, 2007; 73 FR 47065, Aug. 13, pyrimidinyl)amino]carbonyl]amino] 2008; 74 FR 67128, Dec. 18, 2009; 76 FR 34885, sulfonyl]-N,N-dimethyl-3- June 15, 2011; 80 FR 72599, Nov. 20, 2015] pyridinecarboxamide.

§ 180.452 Primisulfuron-methyl; toler- Commodity Parts per ances for residues. million (a) General. Tolerances are estab- Cattle, fat ...... 0.01 Cattle, meat ...... 0 .01 lished for residues of primisulfuron- Cattle, meat byproducts ...... 0.05 methyl (3-[4,6-bis-(difluoromethoxy)- Corn, field, forage ...... 0 .1

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(b) Section 18 emergency exemptions. Commodity Parts per million [Reserved] Corn, field, grain ...... 0 .1 (c) Tolerances with regional registra- Corn, field, stover ...... 0 .1 tions. [Reserved] Corn, pop, grain ...... 0.1 (d) Indirect or inadvertent residues. Corn, pop, stover ...... 0.1 [Reserved] Corn, sweet, forage ...... 0 .1 Corn, sweet, kernel plus cob with husks re- [74 FR 47457, Sept. 16, 2009] moved ...... 0 .1 Corn, sweet, stover ...... 0 .1 Goat, fat ...... 0 .01 § 180.458 Clethodim; tolerances for res- Goat, meat ...... 0.01 idues. Goat, meat byproducts ...... 0 .05 (a) General. Tolerances are estab- Grass, forage ...... 9 .0 Grass, hay ...... 25 .0 lished for residues of the herbicide Horse, fat ...... 0 .01 clethodim, including its metabolites Horse, meat ...... 0 .01 and degradates, in or on the commod- Horse, meat byproducts ...... 0 .05 ities in the table in this paragraph. Milk ...... 0.01 Sheep, fat ...... 0 .01 Compliance with the tolerance levels Sheep, meat ...... 0.01 specified in this paragraph is to be de- Sheep, meat byproducts ...... 0 .05 termined by measuring only the sum of Sorghum, grain, forage ...... 0.3 clethodim, 2-[(1E)-1-[[[(2E)-3-chloro-2- Sorghum, grain, grain ...... 0 .8 Sorghum, grain, stover ...... 0 .05 propenyl]oxy]imino]propyl]-5-[2- (ethylthio)propyl]-3-hydroxy-2-cyclo- (b) Section 18 emergency exemptions. hexen-1-one, and its metabolites con- [Reserved] taining the 5-(2- (c) Tolerances with regional registra- ethylthiopropyl)cyclohexene-3-one and tions. [Reserved] 5-(2-ethylthiopropyl)-5- (d) Indirect or inadvertent residues. hydroxycyclohexene-3-one moieties [Reserved] and their sulphoxides and sulphones, calculated as the stoichiometric equiv- [75 FR 17578, Apr. 7, 2010, as amended at 80 alent of clethodim, in or on the com- FR 68265, Nov. 4, 2015] modity.

§ 180.455 Procymidone; tolerances for Parts per residues. Commodity million

A tolerance is established for the res- Alfalfa, forage ...... 6.0 idues of the fungicide procymidone, N- Alfalfa, hay ...... 10 (3,5-dichlorophenyl)-1,2- Artichoke, globe ...... 1.2 Asparagus ...... 1.7 dimethylcyclopropane-1,2 Berry, low growing, subgroup 13–07G, except dicarboximide, in or on the following cranberry ...... 3.0 raw agricultural commodity: Beet, sugar, molasses ...... 1 .0 Beet, sugar, roots ...... 0 .20 Parts per Beet, sugar, tops ...... 1.0 Commodity million Brassica, head and stem, subgroup 5A ...... 3 .0 Brassica, leafy greens, subgroup 5B ...... 3 .0 Grape, wine ...... 5 .0 Bushberry subgroup 13–07B ...... 0 .20 Caneberry subgroup 13–07A ...... 0.30 Canola, meal ...... 1 .0 [59 FR 42514, Aug. 18, 1994] Cattle, fat ...... 0.2 Cattle, meat ...... 0 .2 § 180.457 Bitertanol; tolerances for res- Cattle, meat byproducts ...... 0.2 idues. Clover, forage ...... 10.0 Clover, hay ...... 20.0 (a) General. A tolerance is established Corn, field, forage ...... 0 .2 for the residues of the fungicide Corn, field, grain ...... 0 .2 ′ Corn, field, stover ...... 0 .2 bitertanol, b-([1,1 -biphenyl]-4-yloxy)-a- Cotton, meal ...... 2 .0 (1,1-dimethylethyl)-1H-1,2,4-triazole-1- Cottonseed subgroup 20C ...... 1 .0 ethanol, in or on the following raw ag- Cranberry ...... 0 .50 ricultural commodity: Egg ...... 0 .2 Flax, meal ...... 1 .0 Flax, seed ...... 0 .6 Parts per Commodity million Fruit, pome, group 11–10 ...... 0 .20 Fruit, stone, group 12–12 ...... 0 .20 Banana 1 ...... 0.5 Goat, fat ...... 0 .2 Goat, meat ...... 0.2 1 There are no U.S. registrations as of April 1, 1992. Goat, meat byproducts ...... 0 .2

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Parts per Parts per Commodity million Commodity million

Herb subgroup 19A ...... 12.0 Cattle, meat byproducts, except kidney ...... 0.1 Hog, fat ...... 0 .2 Cattle, meat ...... 0 .1 Hog, meat ...... 0 .2 Goat, fat ...... 0 .1 Hog, meat byproducts ...... 0 .2 Goat, kidney ...... 0 .5 Hop, dried cones ...... 0 .5 Goat, meat byproducts, except kidney ...... 0 .1 Horse, fat ...... 0 .2 Goat, meat ...... 0.1 Horse, meat ...... 0 .2 Grass, forage ...... 7 .0 Horse, meat byproducts ...... 0 .2 Grass, hay ...... 2 .0 Leaf petioles subgroup 4B ...... 0 .60 Hog, fat ...... 0 .1 Leafy greens subgroup 4A ...... 2 .0 Hog, kidney ...... 0.5 Melon subgroup 9A ...... 2 .0 Hog, meat byproducts ...... 0 .1 Milk ...... 0.05 Hog, meat ...... 0 .1 Onion, bulb, subgroup 3–07A ...... 0 .50 Horse, fat ...... 0 .1 Onion, green ...... 2 .0 Horse, kidney ...... 0 .5 Peanut ...... 3 .0 Horse, meat byproducts, except kidney ...... 0 .1 Peanut, hay ...... 3.0 Horse, meat ...... 0 .1 Peanut, meal ...... 5 .0 Milk ...... 0.02 Peppermint, tops ...... 5 .0 Sheep, fat ...... 0 .1 Potato, granules/flakes ...... 2 .0 Sheep, kidney ...... 0.5 Poultry, fat ...... 0.2 Sheep, meat byproducts, except kidney ...... 0 .1 Poultry, meat ...... 0 .2 Sheep, meat ...... 0.1 Poultry, meat byproducts ...... 0.2 Wheat, forage ...... 5 .0 Radish, tops ...... 0 .70 Wheat, grain ...... 0 .02 Rapeseed subgroup 20A, except flax seed ...... 0 .50 Wheat, straw ...... 2 .0 Safflower, meal ...... 10.0 Sheep, fat ...... 0 .2 (b) Section 18 emergency exemptions. Sheep, meat ...... 0.2 Sheep, meat byproducts ...... 0 .2 [Reserved] Soybean ...... 10.0 (c) Tolerances with regional registra- Spearmint, tops ...... 5 .0 tions. [Reserved] Squash/cucumber subgroup 9B ...... 0.50 Stevia, dried leaves ...... 12 (d) Indirect or inadvertent residues. Sunflower, meal ...... 10 .0 [Reserved] Sunflower subgroup 20B ...... 5.0 Turnip, greens ...... 3.0 [60 FR 36731, July 18, 1995, as amended at 63 Vegetable, fruiting, group 8–10 ...... 1 .0 FR 44152, Aug. 18, 1998; 63 FR 66449, Dec. 2, Vegetable, legume, group 6, except soybean .... 3 .5 1998] Vegetable, root, except sugar beet, subgroup 1B ...... 1 .0 § 180.460 Benoxacor; tolerances for Vegetable, tuberous and corm, subgroup 1C ..... 1.0 residues. (b) Section 18 emergency exemptions. (a) General. Tolerances are estab- [Reserved] lished for residues of the inert ingre- (c) Tolerances with regional registra- dient (safener) benoxacor (4- tions. [Reserved] (dichloroacetyl)-3,4-dihydro-3-methyl- (d) Indirect or inadvertent residues. 2H-1, 4-benzoxazine) at 0.01 parts per [Reserved] million (ppm) when used in pesticide formulations containing metolachlor [76 FR 23496, Apr. 27, 2011, as amended at 77 FR 59128, Sept. 26, 2012; 81 FR 27342, May 6, or S-metolachlor in or on raw agricul- 2016] tural commodities for which tolerances have been established for metolachlor § 180.459 Triasulfuron; tolerances for or S-metolachlor. residues. (b) Section 18 energency exemptions. (a) General. Tolerances are estab- [Reserved] lished for residues of the herbicide (c) Tolerances with regional registra- triasulfuron [3-(6-methoxy-4-methyl- tions. [Reserved] 1,3,5-triazin-2-yl)-1-(2-(2- (d) Indirect or inadvertent residues. chloroethoxy)phenylsulfonyl)urea] in [Reserved] or on the following raw agricultural [63 FR 7305, Feb. 13, 1998, as amended at 70 commodities: FR 21631, Apr. 27, 2005]

Commodity Parts per § 180.461 Cadusafos; tolerances for res- million idues. Barley, grain ...... 0 .02 A tolerance is established for the res- Barley, straw ...... 2 .0 Cattle, fat ...... 0.1 idues of the nematicide/insecticide Cattle, kidney ...... 0 .5 cadusafos, O-ethyl S,S-di-sec-butyl

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phosphorodithioate, in or on the fol- quinclorac, including its metabolites lowing raw agricultural commodity: and degradates, in or on the commodities in the table in this paragraph. Parts per Commodity million Compliance with the tolerance levels specified in this paragraph is to be de- Banana ...... 0.01 termined by measuring only quinclorac, 3,7-dichloro-8- There are no U.S. registrations as of quinolinecarboxylic acid, in or on the May 10, 1994, for the nematicide/ insecticid cadusafos. commodity.

[59 FR 39467, Aug. 3, 1994] Commodity Parts per million § 180.462 Pyridate; tolerances for resi- Barley, grain ...... 2 .0 dues. Berry, low growing, except strawberry, sub- (a) General. Tolerances are estab- group 13–07H ...... 1.5 lished for residues of the herbicide Cattle, fat ...... 0.7 pyridate, including its metabolites and Cattle, meat byproducts ...... 1.5 Cattle, meat ...... 0 .05 degradates, in or on the commodities Egg ...... 0 .05 in the table in this paragraph. Compli- Goat, fat ...... 0 .7 ance with the tolerance levels specified Goat, meat byproducts ...... 1 .5 in this paragraph is to be determined Goat, meat ...... 0.05 by measuring only the sum of pyridate, Grain, aspirated fractions ...... 1200 O-(6-chloro-3-phenyl-4-pyridazinyl)-S- Grass, forage ...... 150 octyl-carbonothioate, and its metabo- Grass, hay ...... 130 Hog, fat ...... 0 .7 lites, 6-chloro-3-phenyl-pyridazine-4-ol Hog, meat byproducts ...... 1 .5 and conjugates of 6-chloro-3-phenyl-py- Hog, meat ...... 0 .05 ridazine-4-ol, calculated as the stoi- Horse, fat ...... 0 .7 chiometric equivalent of pyridate, in Horse, meat byproducts ...... 1 .5 or on the commodity. Horse, meat ...... 0 .05 Milk ...... 0.05 Poultry, fat ...... 0.05 Commodity Parts per million Poultry, meat byproducts ...... 0.1 Poultry, meat ...... 0 .05 Brassica, head and stem, subgroup 5A ...... 0 .03 Rhubarb ...... 0 .5 Cabbage ...... 0 .03 Chickpea, seed ...... 0 .1 Rice, bran ...... 15.0 Collards ...... 0.03 Rice, grain ...... 5 .0 Corn, field, forage ...... 0 .03 Sheep, fat ...... 0 .7 Corn, field, grain ...... 0 .03 Sheep, meat byproducts ...... 1 .5 Corn, field, stover ...... 0 .03 Sheep, meat ...... 0.05 Corn, pop, grain ...... 0.03 Sorghum, grain, forage ...... 3.0 Corn, pop, stover ...... 0.03 Sorghum, grain, grain ...... 6 .0 Peanut ...... 0 .03 Sorghum, grain, stover ...... 1 .0 Peppermint, tops ...... 0 .20 Spearmint, tops ...... 0 .20 Wheat, forage ...... 1 .0 Wheat, germ ...... 0 .75 (b) Section 18 emergency exemptions. Wheat, grain ...... 0 .5 Wheat, hay ...... 0 .5 [Reserved] Wheat, straw ...... 0 .1 (c) Tolerances with regional registrations. [Reserved] (2) Tolerances are established for res- (d) Indirect or inadvertent residues. idues of the herbicide quinclorac, in- [Reserved] cluding its metabolites and degradates, [57 FR 54303, Nov. 18, 1992, as amended at 62 in or on the commodity in the fol- FR 44558, Aug. 22, 1997; 63 FR 53844, Oct. 7, lowing table. Compliance with the tol- 1998; 64 FR 46298, Aug. 25, 1999; 65 FR 25652, erance levels specified in this para- May 3, 2000; 67 FR 35049, May 17, 2002; 72 FR graph is to be determined by measuring 35665, June 29, 2007; 74 FR 46376, Sept. 9, 2009; 76 FR 23496, Apr. 27, 2011] only quinclorac, 3,7-dichloro-8- quinolinecarboxylic acid, and its meth- § 180.463 Quinclorac; tolerances for yl ester, methyl-3,7-dichloro-8- residues. quinolinecarboxylate, calculated as the (a)(1) General. Tolerances are estab- stoichiometric equivalent of lished for residues of the herbicide quinclorac, in or on the commodity.

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OMMODITY Parts per Commodity million Parts per Commodity million Corn, pop, forage ...... 0 .01 Corn, pop, grain ...... 0.01 Rapeseed, subgroup 20A 1 ...... 1.5 Corn, pop, stover ...... 0.01 1 There are no U.S. Registrations. Corn, sweet, forage ...... 0 .01 Corn, sweet, kernel plus cob with husks re- (b) Section 18 emergency exemptions. moved ...... 0 .01 Time-limited tolerances are estab- Corn, sweet, stover ...... 0 .01 lished for residues of the herbicide Cotton, gin byproducts ...... 1 .5 quinclorac, including its metabolites Cottonseed subgroup 20C ...... 0 .01 and degradates, in or on the com- Garlic ...... 0 .01 Grass, forage ...... 0 .15 modity in the table in this paragraph. Grass, hay ...... 2 .5 Compliance with the tolerance level Grass, seed screenings ...... 0 .01 specified in this paragraph is to be de- Grass, straw ...... 0 .01 termined by measuring only Hop, dried cones ...... 0 .05 quinclorac, 3,7-dichloro-8- Horseradish ...... 0.01 quinolinecarboxylic acid, in or on the Leek ...... 0 .01 Onion, bulb ...... 0 .01 commodity. The tolerance expires and Onion, green ...... 0 .01 is revoked on the date specified in the Onion, Welsh ...... 0 .01 table in this paragraph. Peanut ...... 0 .01 Peanut, hay ...... 0.01 Expiration/ Radish, roots ...... 0 .01 Commodity Parts per revocation million date Radish, tops ...... 0 .01 Rutabaga, roots ...... 0 .01 Cranberry ...... 15.0 12/31/12 Rutabaga, tops ...... 0 .1 Shallot, bulb ...... 0 .01 (c) Tolerances with regional registra- Shallot, fresh leaves ...... 0 .01 tions. [Reserved] Sorghum, grain, forage ...... 0.01 (d) Indirect or inadvertent residues. Sorghum, grain, grain ...... 0 .01 Sorghum, grain, stover ...... 0 .01 [Reserved] Soybean, seed ...... 0 .01 [57 FR 47996, Oct. 21, 1992, as amended at 64 Turnip, greens ...... 0.1 FR 6548, 6549, Feb. 10, 1999; 64 FR 14632, Mar. Turnip, roots ...... 0 .01 26, 1999; 65 FR 33701, May 24, 2000; 67 FR 35049, Turnip, tops ...... 0.1 May 17, 2002; 72 FR 55073, Sept. 28, 2007; 74 FR Vegetable, tuberous and corm, subgroup 1C ... 0.01 51490, Oct. 7, 2009; 74 FR 67090, Dec. 18, 2009; 76 FR 23497, Apr. 27, 2011; 77 FR 75566, Dec. 21, (b) Section 18 emergency exemptions. 2012; 78 FR 71528, Nov. 29, 2013; 80 FR 72599, [Reserved] Nov. 20, 2015] (c) Tolerances with regional registrations. Tolerances with regional reg- § 180.464 Dimethenamid; tolerances for istration are established for residues of residues. dimethenamid, 1 (R,S)-2-chloro-N-[(1- (a) General. Tolerances are estab- methyl-2-methoxy) ethyl]-N-(2,4- lished for residues of the herbicide dimethylthien-3-yl)-acetamide) in or dimethenamid, 1(R,S)-2-chloro-N-[(1- on the following raw agricultural com- methyl-2-methoxy)ethyl]-N-(2,4- modities: dimethylthien-3-yl)-acetamide, applied as either the 90:10 or 50:50 S:R isomers, Parts per Commodity million in or on the following food commodities: Pumpkin ...... 0.01 Squash, winter ...... 0 .01 Parts per Commodity million (d) Indirect or inadvertent residues. Bean, dry, seed ...... 0 .01 [Reserved] Beet, garden, roots ...... 0 .01 Beet, garden, tops ...... 0 .01 [65 FR 51551, Aug. 24, 2000, as amended at 67 Beet, sugar, dried pulp ...... 0 .01 FR 46884, July 17, 2002; 69 FR 29459, May 24, Beet, sugar, molasses ...... 0 .01 2004; 69 FR 57207, Sept. 24, 2004; 70 FR 24712, Beet, sugar, roots ...... 0 .01 Beet, sugar, tops ...... 0.01 May 11, 2005; 71 FR 25942, May 3, 2006; 71 FR Corn, field, forage ...... 0 .01 49354, Aug. 23, 2006; 72 FR 44388, Aug. 8, 2007; Corn, field, grain ...... 0 .01 72 FR 73630, Dec. 28, 2007; 80 FR 9215, Feb. 20, Corn, field, stover ...... 0 .01 2015]

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§ 180.465 4-(Dichloroacetyl)-1-oxa-4- Commodity Parts per azaspiro[4.5]decane. million (a) General. Tolerances are estab- Cotton, undelinted seed ...... 1 .0 lished for the residues of 4- Custard apple ...... 1 .5 (dichloroacetyl)-1-oxa-4- Egg ...... 0 .05 Feijoa ...... 3 .0 azaspiro[4.5]decane, (CAS No. 71526–07– Fruit, citrus, group 10–10 ...... 2 .0 3) when used as an inert ingredient Fruit, pome, group 11–10 ...... 5 .0 (safener) in or on the following raw ag- Fruit, small vine climbing, except fuzzy ricultural commodities: kiwifruit, subgroup 13–07F ...... 5.0 Fruit, stone, crop group 12, except cherry ...... 1 .4 Parts per mil- Commodity 1 Goat, fat ...... 1 .0 lion Goat, meat byproducts ...... 0 .1 Goat, meat ...... 0.1 Corn, field, forage ...... 0.005 Corn, field, grain ...... 0.005 Grape, raisin ...... 10.0 Corn, field, stover ...... 0.005 Guava ...... 3 .0 Corn, pop, grain ...... 0.005 Hog, fat ...... 1 .0 Corn, pop, stover ...... 0.005 Hog, meat byproducts ...... 0 .1 1There are no U.S. registered products containing 4- Hog, meat ...... 0 .1 (dichloroacetyl)-1-oxa-4-azaspiro[4.5]decane as of June 17, Horse, fat ...... 1 .0 2002. Horse, meat byproducts ...... 0 .1 (b) Section 18 emergency exemptions. Horse, meat ...... 0 .1 Ilama ...... 1 .5 [Reserved] Jaboticaba ...... 3 .0 (c) Tolerances with regional registra- Longan ...... 7 .0 tions. [Reserved] Lychee ...... 7 .0 (d) Indirect or inadvertent residues. Mango ...... 1.0 [Reserved] Melon subgroup 9A ...... 0 .5 Milk, fat (reflecting 0.08 ppm in whole milk) ..... 2 .0 [68 FR 4392, Jan. 29, 2003] Nut, tree, crop group 14 ...... 0 .10 Olive ...... 5 .0 § 180.466 Fenpropathrin; tolerances for Papaya ...... 1 .0 residues. Passionfruit ...... 3 .0 (a) General. Tolerances are estab- Pea, succulent ...... 0 .02 lished for residues of fenpropathrin, in- Peanut, hay ...... 20.0 Peanut ...... 0 .01 cluding its metabolites and degradates, Pistachio ...... 0.10 in or on the commodities in the fol- Poultry, fat ...... 0.05 lowing table. Compliance with the tol- Poultry, meat byproducts ...... 0.05 erance levels specified below is to be Poultry, meat ...... 0 .05 determined by measuring only Pulasan ...... 7 .0 fenpropathrin (alpha-cyano-3-phenoxy- Rambutan ...... 7 .0 Sapodilla ...... 1 .0 benzyl 2,2,3,3 Sapote, black ...... 1 .0 tetramethylcyclopropanecarboxylate). Sapote, mamey ...... 1 .0 Sheep, fat ...... 1 .0 Parts per Commodity million Sheep, meat byproducts ...... 0 .1 Sheep, meat ...... 0.1 Acerola ...... 3.0 Soursop ...... 1 .5 Almond, hulls ...... 4 .5 Spanish lime ...... 7 .0 Atemoya ...... 1 .5 Squash/Cucumber subgroup 9B ...... 0 .5 Avocado ...... 1 .0 Star apple ...... 1 .0 Barley, grain ...... 0 .04 Starfruit ...... 3 .0 Barley, hay ...... 3 .0 Barley, straw ...... 2 .0 Sugar apple ...... 1 .5 Berry, low growing, subgroup 13–07G ...... 2 .0 Tea, dried 1 ...... 2 .0 Biriba ...... 1 .5 Vegetable, fruiting, group 8–10 ...... 1 .0 Brassica, head and stem, subgroup 5A ...... 3 .0 Wax jambu ...... 3 .0 Bushberry subgroup 13–07B ...... 3 .0 Caneberry subgroup 13-07A ...... 12 1 There are no U.S. registrations as of November 28, 2012, Canistel ...... 1 .0 for the use of fenpropathrin on tea, dried. Cattle, fat ...... 1.0 Cattle, meat byproducts ...... 0.1 (b) Section 18 emergency exemptions. Cattle, meat ...... 0 .1 [Reserved] Cherimoya ...... 1 .5 (c) Tolerances with regional registra- Cherry, sweet ...... 5 .0 Cherry, tart ...... 5 .0 tions. [Reserved] Citrus, dried pulp ...... 4 .0 Citrus, oil ...... 75 Cotton, refined oil ...... 3.0

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(d) Indirect or inadvertent residues. (d) Indirect or inadvertent residues. [Reserved] [Reserved] [62 FR 63034, Nov. 26, 1997, as amended at 63 [76 FR 23497, Apr. 27, 2011] FR 48116, Sept. 9, 1998; 64 FR 3009, Jan. 20, 1999; 65 FR 11242, Mar. 2, 2000; 65 FR 24397, § 180.469 Dichlormid; tolerances for Apr. 26, 2000; 65 FR 48620, Aug. 9, 2000; 66 FR residues. 64774, Dec. 14, 2001; 67 FR 35049, May 17, 2002; (a) General. Tolerances are estab- 70 FR 38789, July 6, 2005; 70 FR 55747, Sept. 23, lished for residues of dichlormid, in- 2005; 74 FR 12606, Mar. 25, 2009; 77 FR 70908, Nov. 28, 2012; 78 FR 69569, Nov. 20, 2013] cluding its metabolites and degradates, when used as an inert ingredient (her- § 180.467 Carbon disulfide; tolerances bicide safener) in pesticide formula- for residues. tions, in or on the commodities in the following table. Compliance with the Tolerances are established for the tolerances is to be determined by meas- nematicide, insecticide, and fungicide uring only dichlormid (2,2-dichloro- carbon disulfide, from the application N,N-di-2-propenylacetamide). of sodium tetrathiocarbonate, in or on the following raw agricultural com- Commodity Parts per modities: million Corn, field, forage ...... 0 .05 Parts per Corn, field, grain ...... 0 .05 Commodity million Corn, field, stover ...... 0 .05 Corn, pop, grain ...... 0.05 Almond ...... 0.1 Corn, pop, stover ...... 0.05 Almond, hulls ...... 0 .1 Corn, sweet, forage ...... 0 .05 Grape ...... 0 .1 Corn, sweet, kernel plus cob with husks re- Grapefruit ...... 0 .1 moved ...... 0 .05 Lemon ...... 0.1 Corn, sweet, stover ...... 0 .05 Orange, sweet ...... 0 .1 Peach ...... 0 .1 (b) Section 18 emergency exemptions. Plum, prune, fresh ...... 0.1 [Reserved] (c) Tolerances with regional registra- [58 FR 33771, June 21, 1993, as amended at 62 tions. [Reserved] FR 26949, May 16, 1997] (d) Indirect or inadvertent residues. [Reserved] § 180.468 Flumetsulam; tolerances for residues. [65 FR 16149, Mar. 27, 2000, as amended at 67 FR 51105, Aug. 7, 2002; 69 FR 58290, Sept. 30, (a) General. Tolerances are estab- 2004; 70 FR 76699, Dec. 28, 2005; 74 FR 37623, lished for residues of the herbicide July 29, 2009; 76 FR 16310, Mar. 23, 2011] flumetsulam, including its metabolites and degradates, in or on the commod- § 180.470 Acetochlor; tolerances for ities in the table in this paragraph. residues. Compliance with the tolerance levels (a) General. Tolerances are estab- specified in this paragraph is to be de- lished for residues of acetochlor, in- termined by measuring only cluding its metabolites and degradates, flumetsulam, N-(2,6-difluorophenyl)-5- in or on the commodities in the table methyl-(1,2,4)-triazolo-(1,5a)-pyrimi- below. Compliance with the tolerance dine-2-sulfonamide, in or on the com- levels specified below is to be deter- modity. mined by measuring only acetochlor, 2- chloro-2’-methyl-6-ethyl-N- Parts per Commodity million ethoxymethylacetanilide, and its metabolites containing the ethyl methyl Bean, dry, seed ...... 0 .05 aniline (EMA) moiety and the hydroxy- Corn, field, forage ...... 0 .05 Corn, field, grain ...... 0 .05 ethyl methyl aniline (HEMA) moiety. Corn, field, stover ...... 0 .05 Both parent and the named metabo- Soybean, seed ...... 0 .05 lites shall be determined as ethyl methyl aniline (EMA) and hydroxy- (b) Section 18 emergency exemptions. ethyl methyl aniline (HEMA), and cal- [Reserved] culated as the stoichiometric equiva- (c) Tolerances with regional registra- lents of acetochlor, in or on the fol- tions. [Reserved] lowing commodities:

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Parts per Parts per Commodity million Commodity million

Beet, sugar, dried pulp ...... 0 .50 Grain, cereal, forage, fodder and straw, group Beet, sugar, molasses ...... 0 .80 16, except corn, grain sorghum, rice and Beet, sugar, roots ...... 0 .30 wheat, stover ...... 0 .1 Beet, sugar, tops ...... 0.70 Grain, cereal, forage, fodder and straw, group Corn, field, forage ...... 4 .5 16, except corn, grain sorghum, and wheat, Corn, field, grain ...... 0 .05 straw ...... 0 .3 Corn, field, stover ...... 2 .5 Grain, cereal, group 15, except corn, grain sor- Corn, pop, grain ...... 0.05 ghum, and wheat, grain ...... 0.05 Corn, pop, stover ...... 2.5 Pea and bean, dried shelled, except soybean, Corn, sweet, forage ...... 1 .5 subgroup 6C ...... 0 .05 Corn, sweet, kernels plus cob with husks re- Potato ...... 0 .05 Soybean, forage ...... 0 .7 moved ...... 0 .05 Soybean, hay ...... 1 .0 Corn, sweet, stover ...... 1 .0 Sunflower, seed ...... 0.05 Cotton, gin byproducts ...... 4 .0 Wheat, forage ...... 0 .5 Cotton, undelinted seed ...... 0 .6 Wheat, grain ...... 0 .02 Peanut ...... 0 .20 Wheat, hay ...... 2 .0 Peanut, hay ...... 7.0 Wheat, straw ...... 0 .1 Peanut, meal ...... 0 .25 Sorghum, grain, forage ...... 1.6 Sorghum, grain, grain ...... 0 .05 [72 FR 27468, May 16, 2007, as amended at 74 Sorghum, grain, stover ...... 1 .7 FR 29969, June 24, 2009; 74 FR 47450, Sept. 16, Soybean, meal ...... 1.2 2009; 78 FR 13268, Feb. 27, 2013; 79 FR 3517, Soybean, seed ...... 1 .0 Jan. 22, 2014]

(b) Section 18 emergency exemptions. § 180.471 Furilazole; tolerances for res- [Reserved] idues. (c) Tolerances with regional registra- (a) General. Tolerances are estab- tions. [Reserved] lished for residues of furilazole; 3- (d) Indirect or inadvertent residues. dichloroacetyl-5-(2-furanyl)-2, 2- Tolerances are established for indirect dimethyloxazolidine (CAS Reg. No. or inadvertent residues of acetochlor, 121776–33–8) when used as an inert in- including its metabolites and gredient (safener) in pesticide formula- degradates, in or on the raw agricul- tions in or on the following raw agri- tural commodities in the table to this cultural commodities: paragraph when present therein as a result of application of acetochlor to Commodity Parts per the growing crops in the table to para- million graph (a) of this section. Compliance Corn, field, forage ...... 0 .01 with the tolerance levels specified Corn, field, grain ...... 0 .01 Corn, field, stover ...... 0 .01 below is to be determined by measuring Corn, pop, grain ...... 0.01 only acetochlor, 2-chloro-2’-methyl-6- Corn, pop, stover ...... 0.01 ethyl-N-ethoxymethylacetanilide, and Sorghum, forage ...... 0 .01 Sorghum, grain ...... 0 .01 its metabolites containing the ethyl Sorghum, stover ...... 0 .01 methyl aniline (EMA) moiety and the hydroxyethyl methyl aniline (HEMA) (b) Section 18 emergency exemptions. moiety. Both parent and the named [Reserved] metabolites shall be determined as (c) Tolerances with regional registra- ethyl methyl aniline (EMA) and hy- tions. [Reserved] droxyethyl methyl aniline (HEMA), (d) Indirect or inadvertent residues. and calculated as the stoichiometric [Reserved] equivalents of acetochlor, in or on the [65 FR 8867, Feb. 23, 2000, as amended at 67 following commodities. FR 15735, Apr. 3, 2002; 72 FR 57492, Oct. 10, 2007] Parts per Commodity million § 180.472 Imidacloprid; tolerances for Animal feed, nongrass, group 18, forage ...... 1 .3 residues. Animal feed, nongrass, group 18, hay ...... 3.5 Grain, cereal, forage, fodder and straw, group (a) General. Tolerances are estab- 16, except corn, grain sorghum, rice and lished for residues of the insecticide wheat, forage ...... 0 .5 imidacloprid, including its metabolites Grain, cereal, forage, fodder and straw, group 16, except corn, grain sorghum, rice and and degradates, in or on the commod- wheat, hay ...... 2 .0 ities in the table below. Compliance

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with the tolerance levels specified Commodity Parts per below is to be determined by measuring million only the sum of imidacloprid (1-[6- Hog, meat byproducts ...... 0 .30 chloro-3-pyridinyl) methyl]-N-nitro-2- Hop, dried cones ...... 6 .0 imidazolidinimine) and its metabolites Horse, fat ...... 0 .30 Horse, meat ...... 0 .30 containing the 6-chloropyridinyl moi- Horse, meat byproducts ...... 0 .30 ety, calculated as the stoichiometric Huckleberry ...... 3 .5 equivalent of imidacloprid, in or on the Ilama ...... 0 .30 Jaboticaba ...... 1 .0 following commodities: Juneberry ...... 3 .5 Kava, leaves ...... 4 .0 Parts per Kava, roots ...... 0 .40 Commodity million Leaf petioles subgroup 4B ...... 6 .0 Acerola ...... 1.0 Leafy greens subgroup 4A ...... 3 .5 Almond, hulls ...... 4 .0 Lettuce, head ...... 3.5 Apple ...... 0.5 Lettuce, leaf ...... 3 .5 Apple, wet pomace ...... 3 .0 Lingonberry ...... 3.5 Artichoke, globe ...... 2.5 Longan ...... 3 .0 Aspirated grain fractions ...... 240 Lychee ...... 3 .0 Atemoya ...... 0 .30 Mango ...... 1.0 Avocado ...... 1 .0 Milk ...... 0.10 Banana ...... 0.50 Mustard, black, seed ...... 0 .05 Beet, sugar, molasses ...... 0 .30 Mustard, field, seed ...... 0 .05 Beet, sugar, roots ...... 0 .05 Mustard, Indian, seed ...... 0 .05 Beet, sugar, tops ...... 0.50 Mustard, rapeseed, seed ...... 0 .05 Biriba ...... 0 .30 Mustard, seed ...... 0 .05 Blueberry ...... 3 .5 Nut, tree, group 14 ...... 0 .05 Borage, seed ...... 0 .05 Okra ...... 1.0 Caneberry, subgroup 13-A ...... 2 .5 Onion, dry bulbs, subgroup 3-07A ...... 0 .15 Canistel ...... 1 .0 Onion, green, subgroup 3-07B ...... 2 .5 Canola, seed ...... 0 .05 Papaya ...... 1 .0 Cattle, fat ...... 0.30 Passionfruit ...... 1 .0 Cattle, meat ...... 0 .30 Peanut ...... 0 .45 Cattle, meat byproducts ...... 0.30 Peanut, hay ...... 35 Cherimoya ...... 0 .30 Peanut, meal ...... 0 .75 Citrus, dried pulp ...... 5 .0 Pecan ...... 0 .05 Coffee, bean, green ...... 0 .80 Persimmon ...... 3 .0 Cotton, gin byproducts ...... 4 .0 Pistachio ...... 0.05 Cotton, meal ...... 8 .0 Pomegranate ...... 0 .90 Cotton, undelinted seed ...... 6 .0 Potato, chip ...... 0 .40 Crambe, seed ...... 0.05 Potato, processed potato waste ...... 0 .90 Cranberry ...... 0 .05 Poultry, fat ...... 0.05 Currant ...... 3 .5 Poultry, meat ...... 0 .05 Custard apple ...... 0 .30 Poultry, meat byproducts ...... 0.05 Egg ...... 0 .02 Pulasan ...... 3 .0 Elderberry ...... 3 .5 Rambutan ...... 3 .0 Feijoa ...... 1 .0 Rapeseed, seed ...... 0 .05 Fish ...... 0 .05 Raspberry, wild ...... 2.5 Fish-shellfish, mollusc ...... 0 .05 Safflower, seed ...... 0 .05 Flax, seed ...... 0 .05 Salal ...... 3 .5 Fruit, citrus, group 10 ...... 0 .70 Sapodilla ...... 1 .0 Fruit, pome, group 11 ...... 0.6 Sapote, black ...... 1 .0 Fruit, stone, group 12 ...... 3 .0 Sapote, mamey ...... 1 .0 Goat, fat ...... 0 .30 Sheep, fat ...... 0 .30 Goat, meat ...... 0.30 Sheep, meat ...... 0.30 Goat, meat byproducts ...... 0 .30 Sheep, meat byproducts ...... 0 .30 Gooseberry ...... 3 .5 Soursop ...... 0 .30 Grain, cereal, forage, fodder and straw, group Soybean, forage ...... 8 .0 16, forage, except rice ...... 7 .0 Soybean, hay ...... 35 Grain, cereal, forage, fodder and straw, group Soybean, meal ...... 4.0 16, hay, except rice ...... 6 .0 Soybean, seed ...... 3 .5 Grain, cereal, forage, fodder and straw, group Spanish lime ...... 3 .0 16, stover, except rice ...... 0 .30 Star apple ...... 1 .0 Grain, cereal, forage, fodder and straw, group Starfruit ...... 1 .0 16, straw, except rice ...... 3.0 Strawberry ...... 0 .50 Grain, cereal, group 15, except rice ...... 0 .05 Sugar apple ...... 0 .30 Grape ...... 1 .0 Sunflower, seed ...... 0.05 Grape, juice ...... 1 .5 Tomato, paste ...... 6 .0 Grape, raisin ...... 1 .5 Tomato, puree ...... 3 .0 Guava ...... 1 .0 Vegetable, brassica leafy, group 5 ...... 3 .5 Herbs subgroup 19A, dried herbs ...... 48 Vegetable, cucurbit, group 9 ...... 0.5 Herbs subgroup 19-A, fresh herbs ...... 8 .0 Vegetable, fruiting, group 8 ...... 1.0 Hog, fat ...... 0 .30 Vegetable, leaves of root and tuber, group 2 ..... 4 .0 Hog, meat ...... 0 .30 Vegetable, legume, group 6, except soybean .... 4 .0

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Parts per [75 FR 22251, Apr. 28, 2010, as amended at 78 Commodity million FR 33743, June 5, 2013; 80 FR 78145, Dec. 16, 2015] Vegetable, root and tuber, group 1, except sugar beet ...... 0 .40 Watercress ...... 3 .5 § 180.473 Glufosinate ammonium; tol- Watercress, upland ...... 3 .5 erances for residues. Wax jambu ...... 1 .0 (a) General. Tolerances are established for residues of the herbicide (b) Section 18 emergency exemptions. glufosinate ammonium, including its Time-limited tolerances are estab- metabolites and degradates, in or on lished for residues of the insecticide the commodities in the table below. imidacloprid, including its metabolites Compliance with the tolerance levels and degradates in connection with use specified below is to be determined by of the pesticide under a Section 18 measuring the sum of glufosinate am- emergency exemption granted by EPA. monium, butanoic acid, 2-amino-4- Compliance with the tolerance levels (hydroxymethylphosphinyl) specified below is to be determined by monoammonium salt, and its metabo- measuring only the sum of lites, 2-(acetylamino)-4- imidacloprid (1-[6-chloro-3- (hydroxymethyl phosphinyl)butanoic pyridinyl)methyl]-N-nitro-2- acid, and 3- imidazolidinimine) and its metabolites (hydroxymethylphosphinyl)propanoic containing the 6-chloropyridinyl moi- acid, expressed as 2-amino-4- ety, calculated as the stoichiometric (hydroxymethylphosphinyl)butanoic equivalent of imidacloprid. These tol- acid equivalents: erances will expire and are revoked on the dates specified in the following Commodity Parts per table: million Almond, hulls ...... 0 .50 Expiration/ Commodity Parts per revocation Apple ...... 0.05 million date Banana ...... 0.30 Banana, pulp ...... 0 .20 Sugarcane, cane ...... 6.0 12/31/18 Beet, sugar, molasses ...... 5 .0 Sugarcane, molasses ...... 50 12/31/18 Beet, sugar, roots ...... 0 .9 Beet, sugar, tops (leaves) ...... 1 .5 Bushberry subgroup 13B ...... 0 .15 (c) Tolerances with regional registra- Canola, meal ...... 1 .1 tions. [Reserved] Canola, seed ...... 0 .40 (d) Indirect or inadvertent residues. Cattle, fat ...... 0.40 Tolerances are established for indirect Cattle, meat ...... 0 .15 Cattle, meat byproducts ...... 6.0 or inadvertent residues of the insecti- Corn, field forage ...... 4.0 cide imidacloprid, including its me- Corn, field, grain ...... 0 .20 tabolites and degradates, in or on the Corn, field, stover ...... 6 .0 Corn, sweet, forage ...... 1 .5 commodities in the table below. Com- Corn, sweet, kernels plus cob with husks re- pliance with the tolerance levels speci- moved ...... 0 .30 fied below is to be determined by meas- Corn, sweet, stover ...... 6 .0 Cotton, gin byproducts ...... 15 uring only the sum of imidacloprid (1- Cotton, undelinted seed ...... 4 .0 [6-chloro-3-pyridinyl) methyl]-N-nitro- Egg ...... 0 .15 2-imidazolidinimine) and its metabo- Fruit, citrus, group 10–10 ...... 0 .15 lites containing the 6-chloropyridinyl Fruit, pome, group 11–10 ...... 0 .25 Fruit, stone, group 12–12 ...... 0 .25 moiety, calculated as the stoichio- Goat, fat ...... 0 .40 metric equivalent of imidacloprid, in Goat, meat ...... 0.15 or on the following commodities, when Goat, meat byproducts ...... 6 .0 Grain aspirated fractions ...... 25 present therein as a result of the appli- Grape ...... 0 .05 cation of the pesticide to growing crops Hog, fat ...... 0 .40 listed in this section and other non- Hog, meat ...... 0 .15 food crops as follows: Hog, meat byproducts ...... 6 .0 Horse, fat ...... 0 .40 Horse, meat ...... 0 .15 Parts per Commodity million Horse, meat byproducts ...... 6 .0 Juneberry ...... 0 .10 Rice, grain ...... 0 .05 Lingonberry ...... 0.10 Vegetable, foliage of legume, group 7 ...... 2 .5 Milk ...... 0.15 Vegetable, legume, group 6 ...... 0 .3 Nut, tree, group 14 ...... 0 .10 Olive ...... 0 .15

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Commodity Parts per § 180.474 Tebuconazole; tolerances for million residues. Pistachio ...... 0.10 (a) General. (1) Tolerances are estab- Potato ...... 0 .80 lished for residues of tebuconazole, Potato, chips ...... 1 .6 alpha-[2-(4-chlorophenyl)ethyl]-alpha- Potato granules/flakes ...... 2 .0 Poultry, fat ...... 0.15 (1,1-dimethylethyl)-1H-1,2,4-triazole-1- Poultry, meat ...... 0 .15 ethanol, including its metabolites and Poultry, meat byproducts ...... 0.60 degradates, in or on the commodities Rice, grain ...... 1 .0 in the table below. Compliance with Rice, hull ...... 2 .0 the tolerance levels specified below is Salal ...... 0 .10 to be determined by measuring only Sheep, fat ...... 0 .40 tebuconazole [ -[2-(4-chlorophenyl) Sheep, meat ...... 0.15 a Sheep, meat byproducts ...... 6 .0 ethyl]-a-(1,1-dimethylethyl)-1H-1,2,4- Soybean ...... 2.0 triazole-1-ethanol], in or on the com- Soybean, hulls ...... 5 .0 modity.

Parts per (b) Section 18 emergency exemptions. Commodity million [Reserved] (c) Tolerances with regional restric- Almond, hulls ...... 6 .0 Apple, wet pomace ...... 0 .1 tions. [Reserved] Asparagus ...... 0.05 (d) Indirect or inadvertent residues. Banana ...... 0.05 Barley, grain ...... 0 .3 Tolerances are established for indirect Barley, hay ...... 7 .0 or inadvertent residues of glufosinate Barley, straw ...... 3 .5 ammonium, including its metabolites Bean, dry seed ...... 0 .1 Bean, succulent ...... 0 .1 and degradates, in or on the commod- Beet, garden, roots ...... 0 .70 ities in the table below, as a result of Beet, garden, tops ...... 7 .0 the application of glufosinate ammo- Brassica, leafy greens, subgroup 5B ...... 2 .5 nium to crops listed in paragraph (a) of Cherry, sweet, pre- and post-harvest ...... 5 .0 Cherry, tart, pre- and post-harvest ...... 5 .0 this section. Compliance with the tol- Coffee, green bean 1 ...... 0 .15 erance levels specified below is to be Coffee, roasted bean 1 ...... 0 .3 determined by measuring the sum of Corn, field, forage ...... 4 .0 Corn, field, grain ...... 0 .05 glufosinate ammonium, butanoic acid, Corn, field, stover ...... 3 .5 2-amino-4-(hydroxymethylphosphinyl) Corn, pop, grain ...... 0.05 monoammonium salt, and its metabo- Corn, pop, stover ...... 3.5 Corn, sweet, forage ...... 7 .0 lite, 3-(hydroxymethylphosphinyl) pro- Corn, sweet, kernel plus cob with husks re- panoic acid, expressed as 2-amino-4- moved ...... 0 .5 (hydroxymethylphosphinyl)butanoic Corn, sweet, stover ...... 6 .0 Cotton, gin byproducts ...... 25 .0 acid equivalents. Cotton, undelinted seed ...... 2 .0 Fruit, pome, group 11 ...... 0.05 Commodity Parts per Fruit, stone, group 12, except cherry ...... 1 .0 million Grain, aspirated fractions ...... 16.0 Grape ...... 5 .0 Barley, hay ...... 0 .40 Grass, forage ...... 8 .0 Barley, straw ...... 0 .40 Grass, hay ...... 25 .0 Buckwheat, fodder ...... 0 .40 Grass, seed screenings ...... 55.0 Buckwheat, forage ...... 0 .40 Grass, straw ...... 30 .0 Oat, forage ...... 0 .40 Hop, dried cones ...... 35 .0 Oat, hay ...... 0.40 Lychee ...... 1 .6 Mango, postharvest ...... 0 .15 Oat, straw ...... 0.40 Nut, tree, group 14 ...... 0 .05 Rye, forage ...... 0 .40 Oat, forage ...... 0 .10 Rye, straw ...... 0 .40 Oat, grain ...... 0 .15 Teosinte ...... 0 .40 Oat, hay ...... 0.10 Triticale ...... 0.40 Oat, straw ...... 0.10 Wheat, forage ...... 0 .40 Onion, bulb, subgroup 3-07A ...... 0 .2 Wheat, hay ...... 0 .40 Onion, green, subgroup 3-07B ...... 1 .3 Orange 1 ...... 1 .0 Wheat, straw ...... 0 .40 Orange, oil 1 ...... 10 Peach ...... 1 .0 [68 FR 55849, Sept. 29, 2003, as amended at 71 Peanut ...... 0 .1 Pistachio ...... 0.05 FR 25945, May 3, 2006; 72 FR 72625, Dec. 21, Plum, pre- and post-harvest ...... 1 .0 2007; 76 FR 23497, Apr. 27, 2011; 77 FR 59113, Soybean, forage ...... 25 Sept. 26, 2012; 80 FR 72599, Nov. 20, 2015] Soybean, hay ...... 50

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(d) Indirect or inadvertent residues. Commodity Parts per million [Reserved] Soybean, seed ...... 0 .08 [59 FR 39464, Aug. 3, 1994] Sunflower, seed ...... 0.05 Sunflower, meal ...... 0 .2 EDITORIAL NOTE: For FEDERAL REGISTER ci- Sunflower, refined oil ...... 0.2 tations affecting § 180.474, see the List of CFR Vegetable, cucurbit, group 9 ...... 0.4 Sections Affected, which appears in the Vegetable, fruiting, group 8–10 ...... 1 .3 Finding Aids section of the printed volume Wheat, forage ...... 3 .0 and at www.fdsys.gov. Wheat, germ ...... 0 .20 Wheat, grain ...... 0 .15 § 180.475 Difenoconazole; tolerances Wheat, hay ...... 7 .0 for residues. Wheat, shorts ...... 0 .20 (a) General. (1) Tolerances are estab- Wheat, straw ...... 1 .5 lished for residues of difenoconazole, 1There are no U.S. registrations. including its metabolites and (2) Tolerances are established for res- degradates, in or on the commodities idues of the fungicide tebuconazole, in- in the following table. Compliance with cluding its metabolites and degradates, the tolerance levels specified below is in or on the commodities in the fol- to be determined by measuring only lowing table. Compliance with the tol- difenoconazole, 1-[2-[2-chloro-4-(4- chlorophenoxy)phenyl]-4-methyl-1,3- erance levels specified in the following dioxolan-2-ylmethyl]-1H-1,2,4-triazole, table is to be determined by measuring in or on the following raw agricultural only the sum of tebuconazole (alpha-[2- commodities: (4-chlorophenyl)ethyl]-alpha-(1,1-

dimethylethyl)-1H-1,2,4-triazole-1-eth- Commodity Parts per anol) and its diol metabolite (1-(4- million chlorophenyl)-4,4-dimethyl-3-(1H -1,2,4- Almond, hulls ...... 7 .0 triazole-1-yl-methyl)-pentane-3,5-diol), Apple, wet pomace ...... 25 Artichoke, globe ...... 1.5 calculated as the stoichiometric equiv- Aspirated grain fractions ...... 95 alent of tebuconzole, in or on the com- Banana1 ...... 0 .2 modity. Barley, grain ...... 0 .1 Barley, hay ...... 0 .05 Barley, straw ...... 0 .05 Parts per Commodity million Beet, sugar ...... 0 .3 Beet, sugar, dried pulp ...... 1 .9 Berry, low growing, subgroup 13–07G, except Cattle, meat byproducts ...... 0.2 cranberry ...... 2.5 Goat, meat byproducts ...... 0 .2 Brassica, head and stem, subgroup 5A ...... 1 .9 Horse, meat byproducts ...... 0 .2 Brassica, leafy green, subgroup 5B ...... 35 Milk ...... 0.1 Bushberry subgroup 13–07B ...... 4 .0 Sheep, meat byproducts ...... 0 .2 Carrot ...... 0 .50 Citrus, dried pulp ...... 2 .0 Citrus, oil ...... 25 (b) Section 18 emergency exemptions. Corn, sweet, forage ...... 0 .01 [Reserved] Corn, sweet, kernel plus cob with husks re- (c) Tolerances with regional registra- moved ...... 0 .01 Corn, sweet, stover ...... 0 .01 tions. Tolerances are established for Cotton, gin byproducts ...... 0 .05 residues of the fungicide tebuconazole, Cotton, undelinted seed ...... 0 .05 including its metabolites and Dragonfruit1 ...... 1 .5 Fruit, citrus, group 10–10 ...... 0 .60 degradates, in or on the commodities Fruit, pome, group 11–10 ...... 5 .0 in the following table. Compliance with Fruit, stone, group 12–12 ...... 2 .5 the tolerance levels specified below is Ginseng ...... 1 .0 Grape ...... 4 .0 to be determined by measuring only Grape, raisin ...... 6 .0 tebuconazole, alpha-[2-(4- Mango 1 ...... 0.07 chlorophenyl)ethyl]-alpha-(1,1- Nut, tree, group 14–12 ...... 0 .03 Oat, forage ...... 0 .15 dimethylethyl)-1H-1,2,4-triazole-1-eth- Oat, grain ...... 0 .01 anol, in or on the commodity. Oat, hay ...... 0.05 Oat, straw ...... 0.05 Parts per Onion, bulb, subgroup 3-07A ...... 0 .20 Commodity million Onion, green, subgroup 3-07B ...... 6 .0 Papaya1 ...... 0 .30 Turnip, roots ...... 0 .5 Pea and bean, dried shelled, except soybean, Turnip, tops ...... 7.0 subgroup 6C ...... 0 .20 Pea, field, hay ...... 40

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(d) Indirect or inadvertent residues. Commodity Parts per million [Reserved] Pea, field, vines ...... 10 [64 FR 36254, July 6, 1999] Potato, wet peel ...... 7 .3 Rapeseed subgroup 20A ...... 0 .10 EDITORIAL NOTE: For FEDERAL REGISTER ci- Rye, forage ...... 0 .15 tations affecting § 180.475, see the List of CFR Rye, grain ...... 0.01 Sections Affected, which appears in the Rye, straw ...... 0 .05 Finding Aids section of the printed volume Soybean, hulls ...... 0 .20 and at www.fdsys.gov. Soybean, seed ...... 0 .15 Turnip, greens ...... 35 § 180.476 Triflumizole; tolerances for Vegetable, cucurbit, group 9 ...... 0.70 residues. Vegetable, fruiting, group 8–10 ...... 0 .60 Vegetable, tuberous and corm, subgroup 1C ..... 4.0 (a) General. (1) Tolerances are estab- Wax jambu 1 ...... 1 .5 lished for residues of the fungicide Wheat, forage ...... 0 .1 triflumizole, including its metabolites Wheat, grain ...... 0 .1 Wheat, hay ...... 0 .05 and degradates, in or on the commod- Wheat, straw ...... 0 .1 ities listed in the table below. Compli- ance with the tolerance levels specified 1There are no U.S. registrations. below is to be determined by measuring (2) Tolerances are established for res- only the parent compound triflumizole, idues of difenoconazole, including its 1-(1-((4-chloro-2- metabolites and degradates, in the (trifluoromethyl)phenyl)imino)-2- commodities in the table below. Com- propoxyethyl)-1 H -imidazole, and its pliance with the tolerance levels speci- metabolites containing the 4-chloro-2- fied below is to be determined by meas- trifluoromethylaniline moiety, cal- uring the sum of difenoconazole, 1-[2- culated as stoichiometric equivalent of [2-chloro-4-(4-chlorophenoxy)phenyl]-4- the parent compound. methyl-1,3-dioxolan-2-ylmethyl]-1H- 1,2,4-triazole, and its metabolite, CGA– Parts Commodity per million 205375, 1-[2-chloro-4-(4-chlorophenoxy)phenyl]-2-[1,2,4]triazol-1-yl- Berry, low growing, subgroup 13–07G, except ethanol, calculated as the stoichio- cranberry ...... 2.0 Brassica, head and stem, subgroup 5A ...... 8 .0 metric equivalent of difenoconazole, in Brassica, leafy greens, subgroup 5B ...... 40 the following commodities: Canistel ...... 2 .5 Cherry, sweet ...... 1 .5 Parts per Cherry, tart ...... 1 .5 Commodity million Cilantro, leaves ...... 35 Fruit, pome, group 11–10 ...... 0 .50 Cattle, fat ...... 0.10 Fruit, small, vine climbing, except fuzzy kiwifruit, Cattle, liver ...... 0 .40 subgroup 13–07F ...... 2 .5 Cattle, meat ...... 0 .05 Hazelnut ...... 0 .05 Hop, dried cones ...... 50 Cattle, meat byproduct (except liver) ...... 0 .10 Leafy greens subgroup 4A, except spinach ...... 35 Egg ...... 0 .02 Mango ...... 2.5 Goat, fat ...... 0 .10 Papaya ...... 2 .5 Goat, liver ...... 0.40 Pineapple ...... 4.0 Goat, meat ...... 0.05 Sapodilla ...... 2 .5 Goat, meat byproduct (except liver) ...... 0.10 Sapote, black ...... 2 .5 Hog, fat ...... 0 .10 Sapote, mamey ...... 2 .5 Hog, liver ...... 0 .40 Star apple ...... 2 .5 Hog, meat ...... 0 .05 Swiss chard ...... 18 Hog, meat byproduct (except liver) ...... 0 .10 Tomato ...... 1.5 Horse, fat ...... 0 .10 Turnip, greens ...... 40 Horse, liver ...... 0 .40 Vegetable, cucurbit, group 9 ...... 0.5 Horse, meat ...... 0 .05 Horse, meat byproduct (except liver) ...... 0 .10 (2) Tolerances are established for res- Milk ...... 0.02 idues of the fungicide triflumizole, in- Sheep, fat ...... 0 .10 cluding its metabolites and degradates, Sheep, liver ...... 0.40 Sheep, meat ...... 0.05 in or on the commodities of animal ori- Sheep, meat byproduct (except liver) ...... 0.10 gin listed in the table below. Compli- ance with the tolerance levels specified (b) Section 18 emergency exemptions. below is to be determined by measuring [Reserved] only the parent compound triflumizole, (c) Tolerances with regional registra- 1-(1-((4-chloro-2- tions. [Reserved] (trifluoromethyl)phenyl)imino)-2-

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propoxyethyl)-1 H -imidazole, the me- (d) Indirect or inadvertent residues. tabolite 4-chloro-2-hydroxy-6- [Reserved] trifluoromethylaniline sulfate, and [65 FR 33702, May 24, 2000, as amended at 71 other metabolites containing the 4- FR 11533, Mar. 8, 2006; 76 FR 23497, Apr. 27, chloro-2-trifluoromethylaniline moi- 2011] ety, calculated as the parent compound. § 180.478 Rimsulfuron; tolerances for residues. Parts Commodity per million (a) General. Tolerances are established for residues of the herbicide Cattle, fat ...... 0.10 rimsulfuron, including its metabolites Cattle, meat byproducts ...... 0.20 Goat, fat ...... 0 .10 and degradates, in or on the commod- Goat, meat byproducts ...... 0 .20 ities in the following table. Compliance Horse, fat ...... 0 .10 with the tolerance levels specified in Horse, meat byproducts ...... 0 .20 Sheep, fat ...... 0 .10 the following table is to be determined Sheep, meat byproducts ...... 0 .20 by measuring only rimsulfuron, N- [[(4,6-dimethoxy-2-pyrimidinyl)amino] (b) Section 18 emergency exemptions. carbonyl]-3-(ethylsulfonyl)-2- [Reserved] pyridinesulfonamide. (c) Tolerances with regional registra- Parts per tions. [Reserved] Commodity million (d) Indirect or inadvertent residues. [Reserved] Almond, hulls ...... 0 .09 Bushberry, subgroup 13–07B ...... 0.01 [65 FR 33702, May 24, 2000, as amended at 67 Caneberry, subgroup 13–07A ...... 0 .01 FR 40228, June 12, 2002; 67 FR 54587, Aug. 23, Chicory, roots ...... 0 .01 Chicory, tops ...... 0 .01 2002; 70 FR 7047, Feb. 10, 2005; 70 FR 17915, Corn, field, forage ...... 0 .4 Apr. 8, 2005; 71 FR 13279, Mar. 15, 2006; 71 FR Corn, field, grain ...... 0 .1 49358, Aug. 23, 2006; 74 FR 26543, June 3, 2009; Corn, field, stover ...... 2 .5 74 FR 46376, Sept. 9, 2009; 76 FR 34885, June 15, Fruit, citrus, group 10 ...... 0 .01 2011; 79 FR 12408, Mar. 5, 2014; 80 FR 72599, Fruit, pome, group 11 ...... 0.01 Nov. 20, 2015] Fruit, stone, group 12 ...... 0 .01 Grain, aspirated fractions ...... 4 .5 Grape ...... 0 .01 § 180.477 Flumiclorac pentyl; toler- Nut, tree, group 14 ...... 0 .01 ances for residues. Pistachio ...... 0.01 Potato ...... 0 .1 (a) General. Tolerances are estab- Sorghum, grain, forage ...... 0.01 lished for residues of the herbicide Sorghum, grain, grain ...... 0 .01 flumiclorac pentyl, including its me- Sorghum, grain, stover ...... 0 .01 Soybean, forage ...... 0 .25 tabolites and degradates, in or on the Soybean, hay ...... 1 .2 commodities in the table in this para- Soybean, hulls ...... 0 .04 graph. Compliance with the tolerance Soybean, seed ...... 0 .01 Tomato ...... 0.05 levels specified in this paragraph is to be determined by measuring only (b) Section 18 emergency exemptions. flumiclorac pentyl, pentyl(2-chloro-4- [Reserved] fluoro-5-(1,3,4,5,6,7-hexahydro-1,3-dioxo- (c) Tolerances with regional registra- 2H-isoindol-2-yl)phenoxy)acetate, in or tions. [Reserved] on the commodity. (d) Indirect or inadvertent residues. Parts per [Reserved] Commodity million [63 FR 16696, Apr. 6, 1998, as amended at 72 Corn, field, forage ...... 0 .01 FR 41913, Aug. 1, 2007; 74 FR 67137, Dec. 18, Corn, field, grain ...... 0 .01 2009; 77 FR 3625, Jan. 25, 2012; 77 FR 46306, Corn, field, stover ...... 0 .01 Aug. 3, 2012; 80 FR 66805, Oct. 30, 2015] Cotton, gin byproducts ...... 3 .0 Cotton, undelinted seed ...... 0 .2 § 180.479 Halosulfuron-methyl; toler- Soybean, hulls ...... 0 .02 Soybean, seed ...... 0 .01 ances for residues. (a) General. (1) Tolerances are estab- (b) Section 18 emergency exemptions. lished for residues of the herbicide [Reserved] halosulfuron-methyl, methyl 5-[(4,6- (c) Tolerances with regional registra- dimethoxy-2-pyrimidiny)amino] tions. [Reserved] carbonylaminosulfonyl]-3-chloro-1-

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methyl-1H-pyrazole-4-carboxylate, in- Commodity Parts per cluding its metabolites and degradates, million in or on the commodities in the fol- Melon subgroup 9A ...... 0 .1 lowing table. Compliance with the tol- Millet, proso, forage ...... 10 erance levels specified in the following Millet, proso, grain ...... 0 .01 Millet, proso, hay ...... 0 .01 table is to be determined by measuring Millet, proso, straw ...... 0 .01 only those halosulfuron-methyl resi- Nut, tree, group 14 ...... 0 .05 dues containing the 3- Okra ...... 0.05 Pea and bean, succulent shelled, subgroup 6 .. 0 .05 chlorosulfonamide (3-CSA) moiety, ex- Pea and bean, succulent shelled, subgroup 6B 0 .05 pressed as the stoichiometric equiva- Pistachio ...... 0.05 lent of halosulfuron-methyl, in or on Rhubarb ...... 0 .05 Rice, grain ...... 0 .05 the commodity. Sorghum, grain, forage ...... 0.05 Sorghum, grain, grain ...... 0 .05 Commodity Parts per Sorghum, grain, stover ...... 0 .1 million Soybean, seed ...... 0 .05 Squash/Cucumber subgroup 9B ...... 0 .5 Cattle, fat ...... 0.05 Sugarcane, cane ...... 0.05 Cattle, meat ...... 0 .05 Vegetable, fruiting, group 8 ...... 0.05 Cattle, meat byproducts ...... 1.0 Vegetable, tuberous and corm, subgroup 1C ... 0.05 Goat, fat ...... 0 .05 Goat, meat ...... 0.05 Goat, meat byproducts ...... 1 .0 (b) Section 18 emergency exemptions. Hog, meat byproducts ...... 0 .1 [Reserved] Horse, fat ...... 0 .05 (c) Tolerances with regional registra- Horse, meat ...... 0 .05 Horse, meat byproducts ...... 1 .0 tions. Tolerances with regional reg- Milk ...... 0.05 istrations are established for residues Sheep, fat ...... 0 .05 of the herbicide halosulfuron-methyl, Sheep, meat ...... 0.05 Sheep, meat byproducts ...... 1 .0 methyl 5-[(4,6-dimethoxy-2- pyrimidiny)amino] (2) Tolerances are established for res- carbonylaminosulfonyl]-3-chloro-1- idues of the herbicide halosulfuron- methyl-1H-pyrazole-4-carboxylate, in- methyl, methyl 5-[(4,6-dimethoxy-2- cluding its metabolites and degradates, pyrimidiny)amino] in or on the commodities in the fol- carbonylaminosulfonyl]-3-chloro-1- lowing table. Compliance with the tol- methyl-1H-pyrazole-4-carboxylate, in- erance levels specified in the following cluding its metabolites and degradates, table is to be determined by measuring in or on the commodities in the fol- only halosulfuron-methyl. lowing table. Compliance with the tol- Parts per erance levels specified in the following Commodity million table is to be determined by measuring Fruit, small vine climbing, except fuzzy kiwifruit, only halosulfuron-methyl. subgroup 13–07F ...... 0 .05 Parts per Commodity million (d) Indirect or inadvertent residues. [Reserved] Alfalfa, forage ...... 1.0 Alfalfa, hay ...... 2.0 [64 FR 25448, May 12, 1999, as amended at 65 Almond, hulls ...... 0 .2 FR 58433, Sept. 29, 2000; 66 FR 66340, Dec. 26, Artichoke ...... 0 .05 2001; 66 FR 66786, Dec. 27, 2001; 67 FR 45649, Asparagus ...... 0.8 Bean, dry, seed ...... 0 .05 July 10, 2002; 67 FR 59192, Sept. 20, 2002; 70 FR Bushberry, subgroup 13-07B ...... 0 .05 51622, Aug. 31, 2005; 72 FR 8927, Feb. 28, 2007; Caneberry subgroup 13–07A ...... 0.05 74 FR 48401, Sept. 23, 2009; 75 FR 46853, Aug. Corn, field, forage ...... 0 .2 4, 2010; 76 FR 34886, June 15, 2011; 77 FR 71561, Corn, field, grain ...... 0 .05 Dec. 3, 2012; 78 FR 53051, Aug. 28, 2013; 80 FR Corn, field, stover ...... 0 .8 55773, Sept. 17, 2015; 80 FR 72599, Nov. 20, 2015] Corn, pop, grain ...... 0.05 Corn, pop, stover ...... 0.8 Corn, sweet, forage ...... 0 .2 § 180.480 Fenbuconazole; tolerances Corn, sweet, kernel plus cob with husks re- for residues. moved ...... 0 .05 (a) Tolerances are established for res- Corn, sweet, stover ...... 0 .8 Cotton, gin byproducts ...... 0 .05 idues of the fungicide fenbuconazole, Cotton, undelinted seed ...... 0 .05 including its metabolites and Fruit, pome, group 11–10 ...... 0 .05 degradates, in or on the commodities Grass, forage, fodder, and hay, group 17, forage ...... 20 in the table below. Compliance with Grass, forage, fodder, and hay, group 17, hay 0 .5 the tolerance levels specified below is

604

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to be determined by measuring only degradates in or on the commodities in the sum of fenbuconazole, alpha-[2-(4- the table below. Compliance with the chlorophenyl)-ethyl]-alpha-phenyl-3- tolerance levels specified in the table (1H-1,2,4-triazole)-1-propanenitrile, and below is to be determined by measuring its metabolites RH-9129, cis-5-(4- only prosulfuron, 1-(4-methoxy-6-meth- chlorophenyl)-dihydro-3-phenyl-3-(1H- yl-triazin-2-yl)-3-[2-(3,3,3- 1,2,4-triazole-1-ylmethyl)-2-3 H- trifluoropropyl)-phenylsulfonyl]-urea, furanone, and RH-9130, trans-5-(4- in or on the commodity. chlorophenyl)-dihydro-3-phenyl-3-(1H- Parts per 1,2,4-triazole-1-ylmethyl)-2-3 H- Commodity million furanone, calculated as the stoichiometric equivalent of fenbuconazole, in Grain, cereal, forage, fodder, and straw, group 16, except rice, fodder ...... 0 .01 or on the following agricultural com- Grain, cereal, forage, fodder, and straw, group modities. 16, except rice, forage ...... 0 .10 Grain, cereal, forage, fodder, and straw, group Commodity Parts per 16, except rice, hay ...... 0 .20 million Grain, cereal, forage, fodder, and straw, group 16, except rice, straw ...... 0 .02 Almond ...... 0.05 Grain, cereal, group 15, except rice ...... 0 .01 Almond, hulls ...... 1 .0 Apple ...... 0.4 Apple, wet pomace ...... 1 .0 (b) Section 18 emergency exemptions. Banana ...... 0.3 [Reserved] Beet, sugar, dried pulp ...... 1 .0 (c) Tolerances with regional registra- Beet, sugar, molasses ...... 0 .4 Beet, sugar, roots ...... 0 .3 tion. [Reserved] Beet, sugar, tops ...... 9.0 (d) Indirect or inadvertent residues. Bushberry subgroup 13B ...... 0 .3 [Reserved] Cattle, meat byproducts ...... 0.05 Citrus, dried pulp ...... 5 .0 [74 FR 67118, Dec. 18, 2009] Citrus, oil ...... 40.0 Cranberry ...... 0 .5 § 180.482 Tebufenozide; tolerances for Fruit, citrus, group 10 ...... 1 .0 Fruit, stone, group 12 ...... 1 .0 residues. Goat, meat byproducts ...... 0 .05 (a) General. (1) Tolerances are estab- Grain, aspirated fractions ...... 6 .0 Grape 1 ...... 1 .0 lished for residues of the insecticide Horse, meat byproducts ...... 0 .05 tebufenozide, including its metabolites Peanut ...... 0 .1 and degradates, in or on the commod- Pecan ...... 0 .05 Pepper ...... 1 .0 ities in the table in this paragraph. Sheep, meat byproducts ...... 0 .05 Compliance with the tolerance levels Wheat, forage ...... 4 .0 specified in this paragraph is to be de- Wheat, grain ...... 0 .1 termined by measuring only Wheat, hay ...... 8 .0 Wheat, straw ...... 8 .0 tebufenozide, 3,5-dimethylbenzoic acid 1-(1,1-dimethylethyl)-2-(4- 1There are no United States registrations for grape as of August 2006. ethylbenzoyl)hydrazide, in or on the commodity. (b) Section 18 emergency exemptions. [Reserved] Commodity Parts per (c) Tolerances with regional registra- million tions. [Reserved] Almond, hulls ...... 25 (d) Indirect or inadvertent residues. Apple ...... 1.0 [Reserved] Apple, dry pomace ...... 3.0 Apple, wet pomace ...... 3 .0 [60 FR 11032, Mar. 1, 1995] Berry group 13 ...... 3 .0 Brassica, head and stem, subgroup 5A ...... 5 .0 EDITORIAL NOTE: For FEDERAL REGISTER ci- Brassica, leafy greens, subgroup 5B ...... 10 .0 tations affecting § 180.480, see the List of CFR Canola, refined oil ...... 4 .0 Sections Affected, which appears in the Canola, seed ...... 2 .0 Finding Aids section of the printed volume Citrus, oil ...... 15.0 and at www.fdsys.gov. Cotton ...... 1 .5 Cotton, gin byproducts ...... 30 Cranberry ...... 1 .0 § 180.481 Prosulfuron; tolerances for Fruit, citrus, group 10 ...... 0 .80 residues. Fruit, pome ...... 1.5 (a) General. Tolerances are estab- Grape ...... 3 .0 Kiwifruit 1 ...... 0.5 lished for residues of the herbicide Leaf petioles subgroup 4B ...... 2 .0 prosulfuron and its metabolites and Leafy greens subgroup 4A ...... 10 .0

605

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(d) Indirect or inadvertent residues. Commodity Parts per million Tolerances are established for indirect Nut, tree, group 14 ...... 0 .1 or inadvertent residues of the insecti- Peppermint, tops ...... 10 .0 cide tebufenozide, including its me- Pistachio ...... 0.1 tabolites and degradates, in or on the Spearmint, tops ...... 10 .0 commodities in the table in this para- Turnip, greens ...... 9.0 Turnip, roots ...... 0 .3 graph when present therein as a result Vegetable, fruiting, group 8 ...... 1.0 of the application of tebufenozide to Vegetable, tuberous and corm, except potato, growing crops listed in the table to subgroup 1D ...... 0 .015 Walnut ...... 0 .1 paragraph (a)(1) of this section. Com- pliance with the tolerance levels speci- 1There are no U.S. registrations on kiwifruit as of June 15, 1999. fied in this paragraph is to be determined by measuring only the sum of (2) Tolerances are established for res- tebufenozide, 3,5-dimethylbenzoic acid idues of the insecticide tebufenozide, 1-(1,1-dimethylethyl)-2-(4- including its metabolites and ethylbenzoyl)hydrazide, and its me- degradates, in or on the commodities tabolite, 3,5-dimethylbenzoic acid 1- in the table in this paragraph. Compli- (1,1-dimethylethyl)-2-(4-(1-hydroxy- ance with the tolerance levels specified ethyl)benzoyl)hydrazide, calculated as in this paragraph is to be determined the stoichiometric equivalent of by measuring only the sum of tebufenozide, in or on the commodity. tebufenozide, 3,5-dimethylbenzoic acid 1-(1,1-dimethylethyl)-2-(4- Commodity Parts per ethylbenzoyl)hydrazide, and its me- million tabolites, 3,5-dimethylbenzoic acid 1- Animal feed, nongrass, group 18 ...... 1 .0 (1,1-dimethylethyl)-2-((4- Grain, cereal, forage, fodder and straw, group 16 ...... 1 .0 carboxymethyl)benzoyl)hydrazide, 3- Grass, forage, fodder and hay, group 17 ...... 1 .0 hydroxymethyl-5-methylbenzoic acid 1- Vegetable, foliage of legume, group 7 ...... 0 .20 (1,1-dimethylethyl)-2-(4- ethylbenzoyl)hydrazide, stearic acid [60 FR 29347, May 31, 1995] conjugate of 3-hydroxymethyl-5- methylbenzoic acid 1-(1,1- EDITORIAL NOTE: For FEDERAL REGISTER citations affecting § 180.482, see the List of CFR dimethylethyl)-2-(4- Sections Affected, which appears in the ethylbenzoyl)hydrazide, and 3- Finding Aids section of the printed volume hydroxymethyl-5-methylbenzoic acid 1- and at www.fdsys.gov. (1,1-dimethylethyl)-2-(4-(1-hydroxyethyl)benzoyl)hydrazide, calculated as § 180.484 Flutolanil; tolerances for res- the stoichiometric equivalent of idues. tebufenozide, in or on the commodity. (a) General. Tolerances are established for residues of flutolanil, N-(3-(1- Parts per Commodity million methylethoxy) phenyl)-2- (trifluoromethyl)benzamide, including Cattle, fat ...... 0.1 its metabolites and degradates, in or Cattle, meat ...... 0 .08 Cattle, meat byproducts ...... 0.08 on the commodities in the table below. Goat, fat ...... 0 .1 Compliance with the tolerance levels Goat, meat ...... 0.08 specified below is to be determined by Goat, meat byproducts ...... 0 .08 Hog, fat ...... 0 .1 measuring only flutolanil and its me- Hog, meat ...... 0 .08 tabolites converted to 2- Hog, meat byproducts ...... 0 .08 (trifluoromethyl) benzoic acid and cal- Horse, fat ...... 0 .1 culated as flutolanil, in or on the fol- Horse, meat ...... 0 .08 Horse, meat byproducts ...... 0 .08 lowing commodities: Milk ...... 0.04 Sheep, fat ...... 0 .1 Commodity Parts per Sheep, meat ...... 0.08 million Sheep, meat byproducts ...... 0 .08 Cattle, fat ...... 0.10 Cattle, kidney ...... 1 .00 (b) Section 18 emergency exemptions. Cattle, liver ...... 2 .00 [Reserved] Cattle, meat byproducts ...... 0.05 Cattle, meat ...... 0 .05 (c) Tolerances with regional registra- Cotton, gin byproducts ...... 0 .20 tions. [Reserved] Cotton, undelinted seed ...... 0 .20

606

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Parts per [60 FR 42458, Aug. 16, 1995, as amended at 61 Commodity million FR 33044, June 26, 1996; 63 FR 42256, 42257, Aug. 7, 1998; 66 FR 10825, Feb. 20, 2001; 71 FR Egg ...... 0 .05 74818, Dec. 13, 2006; 72 FR 35665, June 29, 2007; Goat, fat ...... 0 .10 Goat, kidney ...... 1 .00 73 FR 33017, June 11, 2008; 75 FR 17570, Apr. 7, Goat, liver ...... 2.00 2010; 75 FR 80350, Dec. 22, 2010; 80 FR 72599, Goat, meat byproducts ...... 0 .05 Nov. 20, 2015] Goat, meat ...... 0.05 Hog, fat ...... 0 .10 § 180.485 Cyproconazole; tolerances for Hog, kidney ...... 1.00 Hog, liver ...... 2 .00 residues. Hog, meat byproducts ...... 0 .05 (a) General. (1) Tolerances are estab- Hog, meat ...... 0 .05 Horse, fat ...... 0 .10 lished for residues of the free and con- Horse, kidney ...... 1 .00 jugated forms of the fungicide Horse, liver ...... 2 .00 cyproconazole, including its metabo- Horse, meat byproducts ...... 0 .05 lites and degradates, in or on the com- Horse, meat ...... 0 .05 Milk ...... 0.05 modities in the table below. Compli- Peanut ...... 0 .5 ance with the proposed tolerance levels Peanut, hay ...... 15.0 specified below is to be determined by Peanut, meal ...... 1 .0 Potato ...... 0 .20 measuring only cyproconazole (a-(4- Potato, wet peel ...... 0 .30 chlorophenyl)-a-(1-cyclopropylethyl)- Poultry, fat ...... 0.05 1H-1,2,4-triazole-1-ethanol) in or on the Poultry, meat ...... 0 .05 Poultry, meat byproducts ...... 0.05 following commodities: Rice, bran ...... 10.0 Rice, grain ...... 7 .0 Parts per Commodity million Rice, hulls ...... 25 .0 Sheep, fat ...... 0 .10 Aspirated grain fractions ...... 2 .5 Sheep, kidney ...... 1.00 Cattle, fat ...... 0.01 Sheep, liver ...... 2.00 Cattle, meat byproducts (except liver) ...... 0 .01 Sheep, meat ...... 0.05 1 Sheep, meat byproducts ...... 0 .05 Coffee bean, green (Imported) ...... 0 .1 Soybean, forage ...... 8 .0 Corn, field, forage ...... 0 .60 Soybean, hay ...... 2 .5 Corn, field, grain ...... 0 .01 Soybean, seed ...... 0 .20 Corn, field, stover ...... 1 .2 Turnip, greens ...... 0.1 Goat, fat ...... 0 .01 Vegetable, brassica, leafy, group 5 ...... 0.1 Goat, meat byproducts (except liver) ...... 0.01 Horse, fat ...... 0 .01 (b) Section 18 emergency exemptions. Horse, meat byproducts (except liver) ...... 0 .01 Peanut ...... 0 .01 [Reserved] Peanut, hay ...... 6.0 (c) Tolerances with regional registra- Sheep, fat ...... 0 .01 tions. [Reserved] Sheep, meat byproducts (except liver) ...... 0.01 (d) Indirect or inadvertent residues. Soybean, forage ...... 1 .0 Soybean, hay ...... 3 .0 Tolerances are established for the indi- Soybean, oil ...... 0 .10 rect or inadvertent residues of Soybean, seed ...... 0 .05 flutolanil, N-(3-(1- Wheat, forage ...... 0 .80 methylethoxy)phenyl)-2- Wheat, grain ...... 0 .05 Wheat, grain, milled byproducts ...... 0 .10 (trifluoromethyl)benzamide, including Wheat, hay ...... 1 .3 its metabolites and degradates, in or Wheat, straw ...... 0 .90 on the commodities in the table below. 1There are no U.S. registrations as of February 15, 2008 for Compliance with the tolerance levels use on coffee bean. specified below is to be determined by (2) A tolerance is established for the measuring only flutolanil and its me- combined residues of the free and con- tabolites converted to 2- jugated forms of the fungicide (trifluoromethyl) benzoic acid and cal- cyproconazole, including its metabo- culated as flutolanil, in or on the fol- lites and degradates, in or on the com- lowing commodities. modity in the table below. Compliance Parts per with the tolerance level specified below Commodity million is to be determined by measuring only the sum of cyproconazole ( -(4- Wheat, bran ...... 0.20 a Wheat, forage ...... 2 .5 chlorophenyl)-a-(1-cyclopropylethyl)- Wheat, grain ...... 0 .05 1H-1,2,4-triazole-1-ethanol) and its me- Wheat, hay ...... 1 .2 tabolite d-(4-chlorophenyl)-b,d- Wheat, straw ...... 0 .20 dihydroxy-g-methyl-1H-1,2,4-triazole-1- 607

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hexenoic acid, calculated as the stoi- Commodity Parts per chiometric equivalent of million cyproconazole, in or on the following Corn, field, grain ...... 0 .01 commodity: Corn, field, stover ...... 0 .01 Corn, pop, grain ...... 0.01 Parts per Corn, pop, stover ...... 0.01 Commodity million Corn, sweet, forage ...... 0 .01 Corn, sweet, kernel plus cob with husks re- Milk ...... 0.02 moved ...... 0 .01 Corn, sweet, stover ...... 0 .01 (3) Tolerances are established for the combined residues of the free and con- (b) Section 18 emergency exemptions. jugated forms of the fungicide [Reserved] cyproconazole, including its metabo- (c) Tolerances with regional registra- lites and degradates, in or on the com- tions. [Reserved] modities in the table below. Compli- (d) Indirect or inadvertent residues. ance with the tolerance level specified [Reserved] below is to be determined by measuring [76 FR 23498, Apr. 27, 2011] only the sum of cyproconazole (a-(4- chlorophenyl)-a-(1-cyclopropylethyl)- § 180.487 Pyrithiobac sodium; toler- 1H-1,2,4-triazole-1-ethanol) and its me- ances for residues. tabolite 2-(4-chlorophenyl)-3- (a) General. Tolerances are estab- cyclopropyl-1-[1,2,4]triazol-1-yl-butane- lished for residues of the herbicide, 2,3-diol, calculated as the stoichio- pyrithiobac sodium, (sodium 2-chloro- metric equivalent of cyproconazole, in 6-[(4,6-dimethoxypyrimidin-2- or on the following commodities: yl)thio]benzoate), resulting from the application of the pesticide chemical in Parts per Commodity million or on the following foods/feeds:

Cattle, liver ...... 0 .50 Commodity Parts per Goat, liver ...... 0.50 million Hog, liver ...... 0 .01 Horse, liver ...... 0 .50 Cotton, gin byproducts ...... 0 .15 Sheep, liver ...... 0.50 Cotton, undelinted seed ...... 0 .02

§ 180.486 Chlorethoxyfos; tolerances § 180.490 Imazapic; tolerances for resi- for residues. dues. (a) General. Tolerances are estab- (a) General. (1) Tolerances are established for residues of the insecticide lished for residues of the herbicide chlorethoxyfos, including its metabo- imazapic, including its metabolites and lites and degradates, in or on the com- degradates, in or on the commodities modities in the table in this paragraph. listed in the following table. Compli- Compliance with the tolerance levels ance with the tolerance levels specified specified in this paragraph is to be de- is to be determined by measuring the termined by measuring only sum of imazapic (2-[4,5-dihydro-4-meth- chlorethoxyfos, O,O-diethyl O-(1,2,2,2- yl-4-(1-methylethyl)-5-oxo-1H-imidazol- tetrachloroethyl) phosphorothioate, in 2-yl]-5-methyl-3-pyridinecarboxylic or on the commodity. acid) and its metabolites (±)-2-[4,5- dihydro-4-methyl-4-(1-methylethyl)-5- Commodity Parts per oxo-1H-imidazol-2-yl]-5- million hydroxymethyl-3-pyridinecarboxylic Corn, field, forage ...... 0 .01 acid and (±)-2-[4,5-dihydro-4-methyl-4-

608

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(1-methylethyl)-5-oxo-1H-imidazol-2- § 180.491 Propylene oxide; tolerances yl]-5-(b-D-glucopyranosyloxy)methyl-3- for residues. pyridinecarboxylic acid, calculated as (a) General. (1) Tolerances are estab- the stoichiometric equivalent of lished for residues of the fumigant pro- imazapic. pylene oxide, including its metabolites Parts per and degradates, in or on the commod- Commodity million ities in the table in this paragraph. Compliance with the tolerance levels Grass, forage ...... 15 specified in this paragraph is to be de- Grass, hay ...... 30 Peanut ...... 0 .1 termined by measuring only propylene Soybean, seed 1 ...... 0 .40 oxide, when used as a postharvest fumi- Sugarcane, cane 2 ...... 0.03 gant, in or on the commodity. 1 There are no US registrations as of April 4, 2014. 2 There are no U.S. registrations as of June 4, 2014. Parts per Commodity million (2) Tolerances are established for res- Cacao bean, cocoa powder ...... 200 idues of the herbicide imazapic, includ- Cacao bean, dried bean ...... 200 ing its metabolites and degradates, in Fig ...... 3 .0 or on the commodities listed in the fol- Garlic, dried ...... 300 Grape, raisin ...... 1 .0 lowing table. Compliance with the tol- Herbs and spices, group 19, dried ...... 300 erance levels specified is to be deter- Nut, pine ...... 300 mined by measuring the sum of Nut, tree, group 14 ...... 300 Nutmeat, processed, except peanuts ...... 300 imazapic (2-[4,5-dihydro-4-methyl-4-(1- Onion, dried ...... 300 methylethyl)-5-oxo-1H-imidazol-2-yl]-5- Pistachio ...... 300 methyl-3-pyridinecarboxylic acid) and Plum, prune, dried ...... 2.0 its metabolite (±)-2-[4,5-dihydro-4- methyl-4-(1-methylethyl)-5-oxo-1H- (2) Tolerances are established for res- imidazol-2-yl]-5-hydroxymethyl-3- idues of the reaction product, pro- pyridinecarboxylic acid, calculated as pylene chlorohydrin, including its me- the stoichiometric equivalent of tabolites and degradates, in or on the imazapic. commodities in the table in this paragraph. Compliance with the tolerance Commodity Parts per levels specified in this paragraph is to million be determined by measuring only the Cattle, fat ...... 0.10 sum of propylene chlorohydrin (1- Cattle, kidney ...... 1 .0 chloro-2-propanol), and its isomer 2- Cattle, meat byproducts, except kidney ...... 0.1 chloro-1-propanol, calculated as the Cattle, meat ...... 0 .1 stoichiometric equivalent of propylene Goat, fat ...... 0 .1 Goat, kidney ...... 1 .0 chlorohydrin (1-chloro-2-propanol), Goat, meat byproducts, except kidney ...... 0 .1 that results from the use of propylene Goat, meat ...... 0.1 oxide as a postharvest fumigant, in or Horse, fat ...... 0 .1 on the commodity. Horse, kidney ...... 1 .0 Horse, meat byproducts, except kidney ...... 0 .1 OMMODITY Horse, meat ...... 0 .1 Milk ...... 0.1 Parts per Sheep, fat ...... 0 .1 Commodity million Sheep, kidney ...... 1.0 Sheep, meat byproducts, except kidney ...... 0 .1 Basil, dried leaves ...... 6000 Sheep, meat ...... 0.1 Cacao bean, cocoa powder ...... 20 .0 Cacao bean, dried bean ...... 20 .0 Fig ...... 3 .0 (b) Section 18 emergency exemptions. Garlic, dried ...... 6000 [Reserved] Grape, raisin ...... 4 .0 (c) Tolerances with regional registra- Herbs and spices, group 19, dried, except basil 1500 Nut, pine ...... 10 .0 tions. [Reserved] Nut, tree, group 14 ...... 10 .0 (d) Indirect or inadvertent residues. Nutmeat, processed, except peanuts ...... 10 .0 [Reserved] Onion, dried ...... 6000 Pistachio ...... 10.0 [64 FR 54224, Oct. 6, 1999, as amended at 66 FR Plum, prune, dried ...... 2.0 64774, Dec. 14, 2001; 66 FR 66332, Dec. 26, 2001; 78 FR 49932, Aug. 16, 2013; 79 FR 18818, Apr. 4, (b) Section 18 emergency exemptions. 2014; 79 FR 32170, June 4, 2014] [Reserved]

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(c) Tolerances with regional registra- Commodity Parts per tions. [Reserved] million (d) Indirect or inadvertent residues. Ginseng ...... 0 .90 [Reserved] Grape ...... 3 .0 Grape, raisin ...... 7 .0 [65 FR 33702, May 24, 2000, as amended at 68 Hop, dried cones ...... 60 FR 39430, July 1, 2003; 72 FR 49651, Aug. 29, Onion, bulb, subgroup 3–07A ...... 0 .6 2007; 73 FR 54963, Sept. 24, 2008; 76 FR 38037, Onion, green, subgroup 3–07B ...... 15 .0 June 29, 2011; 77 FR 28495, May 15, 2012] Papaya 1 ...... 1 .5 Potato ...... 0 .05 Potato, wet peel ...... 0 .20 § 180.492 Triflusulfuron-methyl; toler- Strawberry ...... 0 .90 ances for residues. Taro, corm ...... 0 .5 Taro, leaves ...... 6 .0 (a) General. Tolerances are estab- Turnip, greens ...... 20.0 lished for residues of triflusulfuron- Vegetable, cucurbit, group 9 ...... 0.5 methyl, including its metabolites and Vegetable, fruiting, group 8 ...... 1.5 degradates, in or on the commodities Vegetable, leafy (except Brassica) group 4 ...... 30 .0 listed in the table below. Compliance 1 There are no U.S. registrations as of January 20, 2015. with the tolerance levels specified (b) Section 18 emergency exemptions. below is to be determined by measuring [Reserved] only triflusulfuron-methyl (methyl 2- (c) Tolerances with regional registra- [[[[[4-(dimethylamino)-6-(2,2,2- tions. Tolerances with regional reg- trifluoroethoxy)-1,3,5-triazin-2- istrations are established for residues yl]amino]carbonyl]amino]sulfonyl]-3- of the fungicide dimethomorph, 4-[3-(4- methylbenzoate) in or on the following chlorophenyl)-3-(3,4-dimethoxyphenyl)- commodities: 1-oxo-2-propen-1-yl]morpholine, includ- Parts per ing its metabolites and degradates, in Commodity million or on the commodities in the following table. Compliance with the tolerance Beet, garden, roots ...... 0 .01 Beet, garden, tops ...... 0 .02 levels specified in the following table is Beet, sugar, roots ...... 0 .05 to be determined by measuring only Beet, sugar, tops ...... 0.05 dimethomorph in or on the commodity. Chicory, roots ...... 0 .05 Parts per (b) Section 18 emergency exemptions. Commodity million [Reserved] Bean, lima, succulent ...... 0 .60 (c) Tolerances with regional registrations. [Reserved] (d) Indirect or inadvertent residues. (d) Indirect or inadvertent residues. Tolerances are established for the indi- [Reserved] rect or inadvertent residues of the fun- [67 FR 40196, June 12, 2002, as amended at 76 gicide dimethomorph, 4-[3-(4- FR 22625, Apr. 22, 2011] chlorophenyl)-3-(3,4-dimethoxyphenyl)- 1-oxo-2-propen-1-yl]morpholine, includ- § 180.493 Dimethomorph; tolerances ing its metabolites and degradates, in for residues. or on the commodities in the following (a) General. Tolerances are estab- table. Compliance with the tolerance lished for residues of the fungicide levels specified in the following table is dimethomorph, 4-[3-(4-chlorophenyl)-3- to be determined by measuring only (3,4-dimethoxyphenyl)-1-oxo-2-propen- dimethomorph in or on the commodity. 1-yl]morpholine, including its metabo- Parts per lites and degradates, in or on the com- Commodity million modities in the following table. Com- pliance with the tolerance levels speci- Wheat, forage ...... 0 .15 Wheat, hay ...... 0 .15 fied in the following table is to be de- Wheat, straw ...... 0 .4 termined by measuring only dimethomorph in or on the commodities. [62 FR 26416, May 14, 1997] EDITORIAL NOTE: For FEDERAL REGISTER ci- Commodity Parts per tations affecting § 180.493, see the List of CFR million Sections Affected, which appears in the Brassica, head and stem, subgroup 5A ...... 6 .0 Finding Aids section of the printed volume Brassica, leafy greens, subgroup 5B ...... 30 .0 and at www.fdsys.gov.

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§ 180.494 Pyridaben; tolerance for resi- Commodity Parts per Expiration dues. million Date (a) General. Tolerances are estab- Cranberry ...... 0.5 None lished for residues of the insecticide pyridaben [2-tert-butyl-5-(4-tert- (d) Indirect or inadvertent residues. butylbenzylthio)-4-chloropyridazin- [Reserved] 3(2H)-one] on the following plants, and [65 FR 43712, July 14, 2000, as amended at 66 of the insecticide pyridaben and its me- FR 33199, June 21, 2001; 70 FR 55769, Sept. 23, tabolites (2-tert-butyl-5-(4-(1-carboxy-1- 2005; 76 FR 56015, Sept. 15, 2010] methylethyl)benzylthio)-4- chloropyridazin-3(2H)-one] and (2-tert- § 180.495 Spinosad; tolerances for resi- butyl-5-[4(-1,1-dimethyl-2- dues. hypdroxyethyl)benzylthio-4- (a) General. Tolerances are estab- chloropyridazinn-3(2H)-one) on ani- lished for residues of the insecticide mals, as indicated in the following spinosad, including its metabolites and table. degradates, in or on the commodities in the table below. Compliance with Revoca- the tolerance levels specified below is Commodity Parts per tion/expira- million tion date to be determined by measuring only the sum of spinosyn A (Factor A: CAS # Almond, hulls ...... 4.0 None Apple ...... 0.5 None 131929–60–7; Apple, wet pomace ...... 0.75 None (2R,3aS,5aR,5bS,9S,13S,14R,16aS,16bR)-2- Canistel ...... 0.10 None [(6-deoxy-2,3,4-tri-O-methyl-a-L- Cattle, fat ...... 0.05 None Cattle, meat ...... 0.05 None manno-pyranosyl)oxy]-13-[[5- Cattle, meat byproducts ...... 0.05 None (dimethylamino)-tetrahydro-6-methyl- Citrus ...... 0.5 None 2H-pyran-2-yl]oxy]-9-ethyl- Citrus, dried pulp ...... 1.5 None Citrus, oil ...... 10.0 None ,3,3a,5a,5b,6,9,10,11,12,13,14,16a,16b- Fruit, stone, group 12 ...... 2.5 None tetradecahydro-14-methyl-1H-as- Goat, fat ...... 0.0 None indaceno[3,2-d]oxacyclododecin-7,15- Goat, meat ...... 0.05 None dione; and spinosyn D (Factor D; CAS # Goat, meat byproducts ...... 0.05 None Grape ...... 1.5 None 131929–63–0; (2S,3aR,5aS,5bS,9S,13S, Hog, fat ...... 0.05 None 14R,16aS,16bS)-2-[(6-deoxy-2,3,4-tri-O- Hog, meat ...... 0.05 None methyl- -L-manno-pyranosyl)oxy]-13- Hog, meat byproducts ...... 0.05 None a Hop, dried cones ...... 10.0 None [[5-(dimethyl-amino)-tetrahydro-6- Horse, fat ...... 0.05 None methyl-2H-pyran-2-yl]oxy]-9-ethyl- Horse, meat ...... 0.05 None ,3,3a,5a,5b,6,9,10,11,12,13,14,16a,16b- Horse, meat byproducts ...... 0.05 None Mango ...... 0.10 None tetradecahydro-4,14-methyl-1H-as- Milk ...... 0.01 None indaceno[3,2-d]oxacyclododecin-7,15- Nut, tree, group 14 ...... 0.05 None dione, calculated as the stoichiometric Papaya ...... 0.10 None Pear ...... 0.75 None equivalent of spinosad. Pistachio ...... 0.05 None Sapodilla ...... 0.10 None Parts per mil- Commodity lion Sapote, black ...... 0.10 None Sapote, mamey ...... 0.10 None Acerola ...... 1.5 Sheep, fat ...... 0.05 None Alfalfa, seed ...... 0 .15 Sheep, meat ...... 0.05 None Alfalfa, seed screenings ...... 2 .0 Sheep, meat byproduct ...... 0.05 None Almond, hulls ...... 19 Star apple ...... 0.10 None Amaranth, grain, grain ...... 1 .0 Strawberry ...... 2.5 None Amaranth, grain, stover ...... 10 Tomato ...... 0.15 None Animal feed, nongrass, group, 18 ...... 0.02 Animal feed, nongrass, group, 18, forage ...... 35.0 (b) Section 18 emergency exemptions. Animal feed, nongrass, group, 18, hay ...... 30 .0 [Reserved] Apple, dry pomace ...... 0.5 Apple, wet pomace ...... 0 .5 (c) Tolerances with regional registra- Artichoke, globe ...... 0.3 tions. Tolerances with regional reg- Asparagus ...... 0.2 istration, as defined in § 180.1(m) are es- Atemoya ...... 0 .3 Avocado ...... 0 .3 tablished for residues of the insecticide Banana ...... 0.25 pyridaben [2-tert-butyl-5(4-tert- Beet, sugar, molasses ...... 0 .75 butylbenzylthio)-4-chloropyridazin- Berry, low growing, subgroup 13–07G, except cranberry ...... 0.90 3(2H)-one] in or on the following raw Biriba ...... 0 .3 agricultural commodity: Brassica, head and stem, subgroup 5A ...... 2 .0

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Parts per mil- Parts per mil- Commodity lion Commodity lion

Brassica, leafy greens, subgroup 5B ...... 10 .0 Peanut ...... 0 .02 Bushberry subgroup 13–07B ...... 0 .40 Peanut, hay ...... 11.0 Caneberry subgroup 13–07A ...... 1.0 Peppermint, tops ...... 3 .5 Canistel ...... 0 .3 Pineapple ...... 0.02 Cattle, fat ...... 50 Pineapple, process residue ...... 0 .08 Cattle, liver ...... 10 Pomegranate ...... 0 .30 Cattle, meat ...... 2 .0 Poultry, fat ...... 1.3 Cattle, meat byproducts, except liver ...... 5 .0 Poultry, meat ...... 0 .10 Cherimoya ...... 0 .3 Poultry, meat byproducts ...... 0.20 Citrus, oil ...... 3.0 Pulasan ...... 0 .3 Citrus, dried pulp ...... 0 .5 Quinoa, grain ...... 0 .02 Coffee, green bean ...... 0 .04 Rambutan ...... 0 .3 Corn, sweet, kernel plus cob with husks re- Rice, hulls ...... 4 .0 moved ...... 0 .02 Sapodilla ...... 0 .3 Cotton, gin byproducts ...... 1 .5 Sapote, black ...... 0 .3 Cottonseed subgroup 20C ...... 0 .02 Sapote, mamey ...... 0 .3 Cranberry ...... 0 .01 Sapote, white ...... 0 .3 Custard apple ...... 0 .3 Sheep, fat ...... 50 Date ...... 0 .10 Sheep, liver ...... 10 Egg ...... 0 .30 Sheep, meat ...... 2.0 Feijoa ...... 05 Sheep, meat byproducts, except liver ...... 5 .0 Fig ...... 0 .10 Soursop ...... 0 .3 Fish ...... 4 .0 Soybean ...... 0.02 Fish-shellfish, crustacean ...... 4 .0 Spanish lime ...... 0 .3 Fish-shellfish, mollusc ...... 4 .0 Spearmint, tops ...... 3 .5 Food commodities ...... 0 .02 Spice, subgroup 19B, except black pepper .... 1 .7 Fruit, citrus, group 10–10 ...... 0 .30 Star apple ...... 0 .3 Fruit, pome, group 11–10 ...... 0 .20 Starfruit ...... 0 .3 Fruit, small, vine climbing, subgroup13–07F, Sugar apple ...... 0 .3 except fuzzy kiwifruit ...... 0 .50 Ti, leaves ...... 10 .0 Fruit, stone 12–12 ...... 0.20 Vegetable, cucurbit, group 9 ...... 0.3 Goat, fat ...... 50 Vegetable, foliage of legume, group 7 ...... 8 .0 Goat, liver ...... 10 Vegetable, fruiting, group 8–10 ...... 0 .40 Goat, meat ...... 2.0 Vegetable, leafy, except brassica, group 4 ..... 8 .0 Goat, meat byproducts, except liver ...... 5 .0 Vegetable, leaves of root and tuber, group 2 10 .0 Grain, aspirated fractions ...... 200 Vegetable, legume, edible podded, subgroup Grain, cereal, group 15 ...... 1.5 6A ...... 0 .30 Grain, cereal, group 16, forage, except rice ... 2 .5 Vegetable, root and tuber, group 1 ...... 0 .10 Grain, cereal, group 16, hay, except rice ...... 10 .0 Watercress ...... 8 .0 Grain, cereal, group, 16, stover, except rice ... 10 .0 Wax jambu ...... 0 .3 Grain, cereal, group, 16, straw, except rice .... 1 .0 Grape, raisin ...... 1 .0 (b) Section 18 emergency exemptions. Grape, raisin ...... 0 .70 [Reserved] Grass, forage, fodder and hay, group 17, forage ...... 10 .0 (c) Tolerances with regional registra- Grass, forage, fodder and hay, group 17, hay 5 .0 tions. [Reserved] Guava ...... 0 .3 (d) Indirect or inadvertant residues. Herb subgroup 19A, dried ...... 22 [Reserved] Herb subgroup 19A, fresh ...... 3.0 Hog, fat ...... 5 .0 [72 FR 68540, Dec. 5, 2007, as amended at 74 Hog, meat ...... 0 .50 FR 46376, Sept. 9, 2009; 74 FR 48408, Sept. 23, Hog, meat byproducts ...... 2 .0 Hop, dried cones ...... 22 2009; 75 FR 60327, Sept. 30, 2010; 80 FR 72599, Horse, fat ...... 50 Nov. 20, 2015; 80 FR 80672, Dec. 28, 2015] Horse, liver ...... 10 Horse, meat ...... 2 .0 § 180.496 Thiazopyr; tolerances for res- Horse, meat byproducts, except liver ...... 5 .0 idues. Ilama ...... 0 .3 Jaboticaba ...... 0 .3 Tolerances are established for com- Longan ...... 0 .3 bined residues of the herbicide Lychee ...... 0 .3 thiazopyr (3-pyridinecaroxylic acid, 2- Mango ...... 0.3 Milk ...... 7.0 (difluoromethyl)-5-(4,5-dihydro-2- Milk, fat ...... 85 thiazolyl)-4-(2-methylpropyl)-6- Nut, tree, group 14–12 ...... 0 .10 (trifluoromethyl)-, methyl ester) and Onion, bulb, subgroup 3–07A ...... 0 .10 its metabolites determined as 2- Onion, green, subgroup 3–07B ...... 4 .0 Papaya ...... 0 .3 (difluoromethyl)-6-(trifluoromethyl)- Passionfruit ...... 0 .3 3,4,5-pyridinetricarboxylic acid, all ex- Pea and bean, dried shelled, except soybean, pressed as the parent equivalents in or subgroup 6C ...... 0 .02 Pea and bean, succulent shelled, subgroup on the following raw agricultural com- 6B ...... 0 .02 modities:

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(c) Tolerances with regional registra- Commodities Parts per million tions. [Reserved] Grapefruit ...... 0 .05 (d) Indirect or inadvertent residues. Orange, sweet ...... 0 .05 Tolerances are established for indirect or inadvertent residues of the plant [62 FR 9978, Mar. 5, 1997] growth regulator (hybridizing agent) clofencet, including its metabolites EFFECTIVE DATE NOTE: At 81 FR 34906, June and degradates, in or on the commod- 1, 2016, § 180.496 was removed, effective Nov. ities in the table in this paragraph. 28, 2016. Compliance with the tolerance levels § 180.497 Clofencet; tolerances for resi- specified in this paragraph is to be de- dues. termined by measuring only clofencet, potassium 2-(4-chlorophenyl)-3-ethyl- (a) General. Tolerances are estab- 2,5-dihydro-5-oxo-4- lished for residues of the plant growth pyridazinecarboxylate, expressed as the regulator (hybridizing agent) clofencet, free acid, in or on the commodity when including its metabolites and present therein as a result of the appli- degradates, in or on the commodities cation of clofencet to the growing in the table in this paragraph. Compli- crops in paragraph (a) of this section. ance with the tolerance levels specified in this paragraph is to be determined Parts per Expiration/ by measuring only clofencet, potas- Commodity revocation million date sium 2-(4-chlorophenyl)-3-ethyl-2,5- dihydro-5-oxo-4-pyridazinecarboxylate, Grain, cereal, forage, fodder and expressed as the free acid, in or on the straw, group 16, except rice, sweet corn, wheat, and wild rice; commodity. forage ...... 4.0 7/14/12 Grain, cereal, forage, fodder and Parts per Expiration/ straw, group 16, except rice, Commodity revocation sweet corn, wheat, and wild rice; million date hay ...... 15.0 7/14/12 Grain, cereal, forage, fodder and Cattle, fat ...... 0.04 7/14/12 straw, group 16, except rice, Cattle, kidney ...... 10.0 7/14/12 sweet corn, wheat, and wild rice; Cattle, meat ...... 0.15 7/14/12 stover ...... 1.0 7/14/12 Cattle, meat byproducts, except kid- Grain, cereal, forage, fodder and ney ...... 0.5 7/14/12 straw, group 16, except rice, Egg ...... 1.0 7/14/12 sweet corn, wheat, and wild rice; Goat, fat ...... 0.04 7/14/12 straw ...... 4.0 7/14/12 Goat, kidney ...... 10.0 7/14/12 Grain, cereal group 15, except rice, Goat, meat ...... 0.15 7/14/12 sweet corn, wheat, and wild rice 20.0 7/14/12 Goat, meat byproducts, except kid- Soybean ...... 30.0 7/14/12 ney ...... 0.5 7/14/12 Soybean, forage ...... 10.0 7/14/12 Hog, fat ...... 0.04 7/14/12 Soybean, hay ...... 10.0 7/14/12 Hog, kidney ...... 10.0 7/14/12 Hog, meat ...... 0.15 7/14/12 Hog, meat byproducts, except kid- [76 FR 56656, Sept. 14, 2011] ney ...... 0.5 7/14/12 EFFECTIVE DATE NOTE: At 81 FR 34906, June Horse, fat ...... 0.04 7/14/12 Horse, kidney ...... 10.0 7/14/12 1, 2016, § 180.497 was removed, effective Nov. Horse, meat ...... 0.15 7/14/12 28, 2016. Horse, meat byproducts, except kidney ...... 0.5 7/14/12 § 180.498 Sulfentrazone; tolerances for Milk ...... 0.02 7/14/12 residues. Poultry, fat ...... 0.04 7/14/12 Poultry, meat ...... 0.15 7/14/12 (a)(1) General. Tolerances are estab- Poultry, meat byproducts ...... 0.20 7/14/12 lished for the combined residues of the Sheep, fat ...... 0.04 7/14/12 free and conjugated forms of Sheep, kidney ...... 10.0 7/14/12 Sheep, meat ...... 0.15 7/14/12 sulfentrazone, including its metabo- Sheep, meat byproducts, except lites and degradates, in or on the com- kidney ...... 0.5 7/14/12 modities in the table below. Compli- Wheat, forage ...... 10.0 7/14/12 ance with the tolerance levels specified Wheat, grain ...... 250.0 7/14/12 Wheat, hay ...... 40.0 7/14/12 below is to be determined by measuring Wheat, straw ...... 50.0 7/14/12 only the sum of sulfentrazone (N-[2,4- dichloro-5-[4-(difluoromethyl)-4,5- (b) Section 18 emergency exemptions. dihydro-3-methyl-5-oxo-1H-1,2,4-triazol- [Reserved] 1-yl]phenyl]methanesulfonamide) and

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its metabolite HMS (N-(2,4-dichloro-5- Commodity Parts per (4-(difluoromethyl)-4,5-dihydro-3- million hydroxymethyl-5-oxo-1H-1,2,4-triazol-1- Vegetable, soybean, succulent ...... 0 .15 yl)phenyl)methanesulfonamide, cal- Vegetable, tuberous and corm, subgroup 1C ... 0.15 culated as the stoichiometric equivalent of sulfentrazone in or on the fol- (b) Section 18 emergency exemptions. lowing commodities. [Reserved] (c) Tolerances with regional registra- Commodity Parts per tions. Tolerances with regional reg- million istration are established for the com- Soybean, seed ...... 0 .05 bined residues of the free and conjugated forms of sulfentrazone, includ- (2) Tolerances are established for the ing its metabolites and degradates, in combined residues of the free and con- or on the commodities in the table jugated forms of sulfentrazone, includ- below. Compliance with the tolerance ing its metabolites and degradates, in levels specified below is to be deter- or on the commodities in the table mined by measuring only the sum of below. Compliance with the tolerance sulfentrazone (N-[2,4-dichloro-5-[4- levels specified below is to be deter- (difluoromethyl)-4,5-dihydro-3-methyl- mined by measuring only the sum of 5-oxo-1H-1,2,4-triazol-1- sulfentrazone (N-[2,4-dichloro-5-[4- yl]phenyl]methanesulfonamide) and its (difluoromethyl)-4,5-dihydro-3-methyl- metabolites HMS (N-(2,4-dichloro-5-(4- 5-oxo-1H-1,2,4-triazol-1- (difluoromethyl)-4,5-dihydro-3- yl]phenyl]methanesulfonamide) and its hydroxymethyl-5-oxo-1H-1,2,4-triazol-1- metabolites HMS (N-(2,4-dichloro-5-(4- yl)phenyl)methanesulfonamide) and (difluoromethyl)-4,5-dihydro-3- DMS (N-(2,4-dichloro-5-(4- hydroxymethyl-5-oxo-1H-1,2,4-triazol-1- (difluoromethyl)-4,5-dihydro-5-oxo-1H- yl)phenyl)methanesulfonamide) and 1,2,4-triazol-1- DMS (N-(2,4-dichloro-5-(4- yl)phenyl)methanesulfonamide, cal- (difluoromethyl)-4,5-dihydro-5-oxo-1H- culated as the stoichiometric equiva- 1,2,4-triazol-1- lent of sulfentrazone in or on the fol- yl)phenyl)methanesulfonamide, cal- lowing commodities. culated as the stoichiometric equiva- Parts per lent of sulfentrazone in or on the fol- Commodity million lowing commodities. Bean, lima, succulent ...... 0 .15 Parts per Cowpea, succulent ...... 0 .15 Commodity million Wheat, forage ...... 0 .50 Wheat, grain ...... 0 .15 Apple ...... 0.15 Wheat, hay ...... 0 .30 Asparagus ...... 0.15 Wheat, straw ...... 1 .5 Berry and small fruit, group 13–07 ...... 0 .15 Brassica, head and stem, subgroup 5A ...... 0 .20 (d) Indirect or inadvertent residues. Brassica, leafy greens, subgroup 5B ...... 0 .40 Corn, field, forage ...... 0 .20 Tolerances are established for inad- Corn, field, grain ...... 0 .15 vertent and indirect combined residues Corn, field, stover ...... 0 .30 of the free and conjugated forms of Flax ...... 0 .15 Fruit, citrus, group 10–10 ...... 0 .15 sulfentrazone, including its metabo- Horseradish ...... 0.20 lites and degradates, in or on the com- Melon, subgroup 9A ...... 0 .15 modities in the table below. Compli- Nut, tree, group 14 ...... 0 .15 Pea and bean, dried shelled, except soybean, ance with the tolerance levels specified subgroup 6C ...... 0 .15 below is to be determined by measuring Pea, succulent ...... 0 .15 only the sum of sulfentrazone (N-[2,4- Peanut ...... 0 .20 dichloro-5-[4-(difluoromethyl)-4,5- Peanut, meal ...... 0 .40 Peppermint, tops ...... 0 .30 dihydro-3-methyl-5-oxo-1H-1,2,4-triazol- Pistachio ...... 0.15 1-yl]phenyl]methanesulfonamide) and Rhubarb ...... 0 .15 its metabolites HMS (N-(2,4-dichloro-5- Spearmint, tops ...... 0 .30 Sugarcane, cane ...... 0.15 (4-(difluoromethyl)-4,5-dihydro-3- Sugarcane, molasses ...... 0 .20 hydroxymethyl-5-oxo-1H-1,2,4-triazol-1- Sunflower subgroup 20B ...... 0.20 yl)phenyl)methanesulfonamide) and Turnip, roots ...... 0 .15 Turnip, tops ...... 0.60 DMS (N-(2,4-dichloro-5-(4- Vegetable, fruiting, group 8–10 ...... 0 .15 (difluoromethyl)-4,5-dihydro-5-oxo-1H-

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1,2,4-triazol-1- Compliance with the following toler- yl)phenyl)methanesulfonamide, cal- ance levels is to be determined by culated as the stoichiometric equiva- measuring only propamocarb (propyl lent of sulfentrazone in or on the fol- N-[3- lowing commodities when present (dimethylamino)propyl]carbamate): therein as a result of the application of Parts per sulfentrazone to growing crops. Commodity million

Parts per Bean, lima, succulent ...... 2 .0 Commodity million

Grain, cereal (excluding sweet corn), Hulls ...... 0 .30 (d) Indirect or inadvertent residues. Grain, cereal, forage, fodder and straw, group [Reserved] 16, except sweet corn; forage ...... 0.2 Grain, cereal, forage, fodder and straw, group [62 FR 15620, Apr. 2, 1997, as amended at 62 16, except sweet corn; hay ...... 0.2 FR 26966, May 16, 1997; 63 FR 32136, June 12, Grain, cereal, forage, fodder and straw, group 1998; 64 FR 16843, Apr. 7, 1999; 65 FR 58399, 16, except sweet corn; stover ...... 0 .1 Sept. 29, 2000; 66 FR 37598, July 19, 2001; 66 FR Grain, cereal, forage, fodder and straw, group 48585, Sept. 21, 2001; 67 FR 35049, May 17, 2002; 16, except sweet corn; straw ...... 0 .6 Grain, cereal, group 15, except sweet corn ...... 0 .1 69 FR 47022, Aug. 4, 2004; 70 FR 7047, Feb. 10, Grain, cereal, group 15, except sweet corn; 2005; 78 FR 33736, June 5, 2013] bran ...... 0 .15 § 180.500 Imazapyr; tolerances for residues. [62 FR 10708, Mar. 10, 1997] (a) General. Tolerances are estab- EDITORIAL NOTE: For FEDERAL REGISTER citations affecting § 180.498, see the List of CFR lished for residues of the herbicide, Sections Affected, which appears in the imazapyr, including its metabolites Finding Aids section of the printed volume and degradates, in or on the commod- and at www.fdsys.gov. ities in the following table. Compliance with the tolerance levels specified in § 180.499 Propamocarb; tolerances for the following table is to be determined residues. by measuring only the residues of (a) General. Tolerances are estab- imazapyr [2-[4,5-dihydro-4-methyl-4-(1- lished for the residues of propamocarb, methylethyl)-5-oxo-1H-imidazol-2-yl]-3- including its metabolites and pyridinecarboxylic acid]. degradates, in or on the commodities Parts per specified in the following table result- Commodity million ing from the application of the hydrochloride salt of propamocarb. Compli- Cattle, fat ...... 0.05 Cattle, kidney ...... 0 .20 ance with the following tolerance lev- Cattle, meat ...... 0 .05 els is to be determined by measuring Cattle, meat byproducts, except kidney ...... 0.05 only propamocarb (propyl N-[3- Corn, field, forage ...... 0 .05 Corn, field, grain ...... 0 .05 (dimethylamino)propyl]carbamate): Corn, field, stover ...... 0 .05 Fish ...... 1 .0 Commodity Parts per Goat, fat ...... 0 .05 million Goat, kidney ...... 0 .20 Goat, meat ...... 0.05 Lettuce, head ...... 50 Goats, meat byproducts, except kidney ...... 0 .05 Lettuce, leaf ...... 90 Grass, forage ...... 100 Potato ...... 0 .06 Grass, hay ...... 30 Tomato, paste ...... 5 .0 Horse, fat ...... 0 .05 Vegetable, cucurbit, group 9 ...... 1.5 Horse, kidney ...... 0 .20 Vegetable, fruiting, group 8 ...... 2.0 Horse, meat ...... 0 .05 Horse, meat byproducts, except kidney ...... 0 .05 (b) Section 18 emergency exemptions. Lentil 1 ...... 0.2 [Reserved] Milk ...... 0.01 Rapeseed subgroup 20A 1 ...... 0 .05 (c) Tolerance with regional registra- Sheep, fat ...... 0 .05 tions. Tolerances with regional reg- Sheep, kidney ...... 0.20 istrations are established for the resi- Sheep, meat ...... 0.05 dues of propamocarb, including its me- Sheep, meat byproducts, except kidney ...... 0 .05 Shellfish ...... 0 .10 tabolites and degradates, in or on the Soybean, meal 1 ...... 4.5 commodities specified in the following Soybean, seed 1 ...... 4 .0 table resulting from the application of Sunflower subgroup 20B 1 ...... 0.05 the hydrochloride salt of propamocarb. 1 There are no U.S. Registrations.

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(b) Section 18 emergency exemptions. § 180.502 Aminoethoxyvinylglycine hy- [Reserved] drochloride (aviglycine HCl); toler- (c) Tolerances with regional registra- ances for residues. tions. [Reserved] (a) General. Tolerances are estab- (d) Indirect or inadvertent residues. lished for residues of [Reserved] aminoethoxyvinylglycine hydro- [68 FR 55484, Sept. 26, 2003, as amended at 78 chloride (aviglycine HCl) in or on the FR 66653, Nov. 6, 2013; 79 FR 19487, Apr. 9, following food commodities: 2014] Parts per Commodity million § 180.501 Hydroprene; tolerances for residues. Apple ...... 0.08 Fruit, stone, group 12, except cherry ...... 0 .170 (a) General. A tolerance of 0.2 part per Pear ...... 0 .08 million is established for residues of hydroprene [(S)-(Ethyl (2E,4E,7S)- (b) Section 18 emergency exemptions. 3,7,11-trimrthyl-2,4-dodecadienoate)], [Reserved] (CAS Reg. No. 65733–18–8) on food com- (c) Tolerances with regional registra- modities in food-handling establish- tions. [Reserved] ments in accordance with the following (d) Indirect or inadvertent residues. prescribed conditions: [Reserved] (1) Application shall be limited to spot, crack and crevice, perimeter and [62 FR 24838, May 7, 1997, as amended at 64 ultra low volume (ULV) fogging treat- FR 31129, June 10, 1999; 66 FR 36481, 36484, July 12, 2001; 69 FR 7606, Feb. 18, 2004] ment in food storage or food-handling establishments, including warehouses, § 180.503 Cymoxanil, tolerance for resi- food service, manufacturing, and proc- dues. essing establishments such as res- (a) Tolerances are estab- taurants, cafeterias, supermarkets, General. lished for residues of the fungicide, bakeries, breweries, dairies, meat cymoxanil, 2-cyano -N- slaughtering and packing plants, and [(ethylamino)carbonyl]-2- canneries where food and food products (methoxyimino) acetamide, in or on are held, processed, and served: Pro- the following food commodities: vided that the food is removed or covered prior to such use, and food-proc- Parts per essing surfaces are covered during Commodity million treatment or thoroughly cleaned before Caneberry, subgroup 13A-07 ...... 4 .0 using, or in the case of point-source de- Cilantro, leaves ...... 19 vice treatments, devices must not Hop, dried cones ...... 7 .0 come into direct contact with food Leafy greens, subgroup 4A ...... 19 preparation surfaces and must be in a Leaf petioles, subgroup 4B ...... 6 .0 1 minimum distance of 3 feet from ex- Lychee ...... 1 .0 Onion, bulb, subgroup 3-07A ...... 0 .05 posed foods. Onion, green, subgroup 3-07B ...... 1 .1 (2) To assure safe use of the insect Potato ...... 0 .05 growth regulator, the label and label- Vegetable, cucurbit, group 9 ...... 0.05 ing shall conform to that registered by Vegetable, fruiting, group 8 ...... 0.2 the U.S. Environmental Protection 1 There is no U.S. registration for lychee. Agency, and it shall be used in accord- (b) Section 18 emergency exemptions. ance with such label and labeling. [Reserved] (b) Section 18 emergency exemptions. (c) Tolerances with a regional registra- [Reserved] tion. Tolerances with a regional reg- (c) Tolerances with regional registra- istration as defined in § 180.1(l) are es- tions. [Reserved] tablished for the residues of the fun- (d) Indirect or inadvertent residues. gicide cymoxanil, 2-cyano -N- [Reserved] [(ethylamino)carbonyl]-2- [62 FR 61647, Nov. 19, 1997, as amended at 71 (methoxyimino) acetamide) in or on FR 74818, Dec. 13, 2006] the raw agricultural commodities:

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ities in the following table. Compliance Commodity Parts per million with the tolerance levels specified in Grape ...... 0 .10 the following table is to be determined by measuring only the sum of (d) Indirect or inadvertent residues. emamectin (MAB1a + MAB1b isomers) [Reserved] and the associated 8,9-Z isomers (8,9- ZB and 8,9-ZB ). [62 FR 26411, May 14, 1997, as amended at 62 1a 1b FR 39956, July 25, 1997; 63 FR 24949, May 6, Parts per 1998; 63 FR 66464, Dec. 2, 1998; 64 FR 6539, Feb. Commodity million 10, 1999; 64 FR 47689, Sept. 1, 1999; 66 FR 37598, July 19, 2001; 67 FR 35049, May 17, 2002; 68 FR Cattle, fat ...... 0.010 41936, July 16, 2003; 70 FR 7047, Feb. 10, 2005; Cattle, liver ...... 0 .050 Cattle, meat ...... 0 .003 72 FR 37646, July 11, 2007; 73 FR 58885, Oct. 8, Cattle, meat byproducts, except liver ...... 0 .020 2008; 76 FR 34885, June 15, 2011] Goat, fat ...... 0 .010 Goat, liver ...... 0.050 § 180.504 [Reserved] Goat, meat ...... 0.003 Goat, meat byproducts, except liver ...... 0 .020 § 180.505 Emamectin; tolerances for Hog, fat ...... 0 .003 residues. Hog, liver ...... 0 .020 Hog, meat ...... 0 .002 (a) General. (1) Tolerances are estab- Hog, meat byproducts (except liver) ...... 0 .005 lished for emamectin, including its me- Horse, fat ...... 0 .010 Horse, liver ...... 0 .050 tabolites and degradates, in or on the Horse, meat ...... 0 .003 commodities in the table below. Com- Horse, meat byproducts, except liver ...... 0 .020 pliance with the tolerance levels speci- Milk ...... 0.003 Sheep, fat ...... 0 .010 fied below is to be determined by meas- Sheep, liver ...... 0.050 uring only the sum of emamectin (a Sheep, meat ...... 0.003 mixture of a minimum of 90% 4′-epi- Sheep, meat byproducts, except liver ...... 0 .020 methylamino-4′-deoxyavermectin B1a and maximum of 10% 4′-epi- (b) Section 18 emergency exemptions. methylamino-4′-deoxyavermectin B1b) [Reserved] and its metabolites 8,9-isomer of the (c) Tolerances with regional registra- B1a and B1b component of the parent tions. [Reserved] (8,9-ZMA), or 4′-deoxy-4′-epi-amino- (d) Indirect and inadvertant residues. avermectin B1a and 4’-deoxy-4′-epi- [Reserved] ′ ′ amino-avermectin B1b; 4 -deoxy-4 -epi- [71 FR 18649, Apr. 12, 2006, as amended at 74 amino avermectin B1a (AB1a); 4′-deoxy- FR 2873, Jan. 16, 2009; 78 FR 18511, Mar. 27, 4′-epi-(N-formyl-N-methyl)amino- 2013; 78 FR 49939, Aug. 16, 2013] avermectin (MFB1a); and 4′-deoxy-4′- epi-(N-formyl)amino-avermectin B1a § 180.506 Cyclanilide; tolerances for residues. (FAB1a), calculated as the stoichiometric equivalent of emamectin. (a) General. Tolerances are established for residues of the plant growth Parts per Commodity million regulator, cyclanilide, [1-(2,4- dichlorophenylaminocarbonyl)- Almond, hulls ...... 0 .20 cyclopropane carboxylic acid] deter- Apple, wet pomace ...... 0 .075 Cotton, gin byproducts ...... 0 .050 mined as 2,4-dichloroaniline (cal- Cotton, undelinted seed ...... 0 .025 culated as cyclanilide) in or on the fol- Fruit, pome, group 11 ...... 0.025 lowing food commodities and processed Grape, wine 1 ...... 0 .03 Nut, tree, group 14 ...... 0 .02 feed: Pistachio ...... 0.02 Tomato, paste ...... 0 .150 Commodity Parts Per Turnip, greens ...... 0.050 Million Vegetable, Brassica, leafy, group 5 ...... 0 .050 Vegetable, cucurbit, group 9 ...... 0.02 Cattle, fat ...... 0.10 Vegetable, fruiting, group 8 ...... 0.020 Cattle, meat ...... 0 .02 Vegetable, leafy, except Brassica, group 4 ...... 0 .100 Cattle, meat byproducts, except kidney ...... 0.2 Cattle, kidney ...... 2 .0 1 There are no U.S. registrations for use of emamectin on Cotton, undelinted seed ...... 0 .60 grape, wine. Cotton, gin byproducts ...... 25 .0 (2) Tolerances are established for Goat, fat ...... 0 .10 Goat, meat ...... 0.02 emamectin, including its metabolites Goat, meat byproducts, except kidney ...... 0 .20 and degradates, in or on the commod- Goat, kidney ...... 2 .0

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Parts Per Parts per Commodity Million Commodity million

Horse, fat ...... 0 .10 Canistel ...... 2 .0 Horse, meat ...... 0 .02 Cherimoya ...... 2 .0 Horse, meat byproducts, except kidney ...... 0 .20 Cilantro, leaves ...... 30.0 Horse, kidney ...... 2 .0 Citrus, dried pulp ...... 20 .0 Hog, fat ...... 0 .10 Citrus, oil ...... 40.0 Hog, meat ...... 0 .02 Coffee, green bean 1 ...... 0 .03 Hog, meat byproducts, except kidney ...... 0 .20 Corn, field, forage ...... 12 .0 Hog, kidney ...... 2.0 Corn, field, grain ...... 0 .05 Milk ...... 0.04 Corn, field, refined oil ...... 0 .3 Sheep, fat ...... 0 .10 Corn, field, stover ...... 25 .0 Sheep, meat ...... 0.20 Corn, pop, grain ...... 0.05 Sheep, meat byproducts, except kidney ...... 0 .20 Corn, pop, stover ...... 25.0 Sheep, kidney ...... 2.0 Corn, sweet, forage ...... 12 .0 Corn, sweet, kernel plus cob with husks re- (b) Section 18 emergency exemptions. moved ...... 0 .05 Corn, sweet, stover ...... 25.0 [Reserved] Cotton, gin byproducts ...... 45 (c) Tolerances with regional registra- Cottonseed subgroup 20C ...... 0 .7 tions. [Reserved] Cranberry ...... 0 .50 Custard apple ...... 2 .0 (d) Indirect or inadvertent residues. Dragon fruit ...... 2 .0 [Reserved] Feijoa ...... 2 .0 Fruit, citrus, group 10–10 ...... 15 .0 [62 FR 28355, May 23, 1997; 62 FR 34182, June Fruit, small vine climbing, except fuzzy 25, 1997] kiwifruit, subgroup 13–07F ...... 2.0 Fruit, stone, group 12–12 ...... 2 .0 § 180.507 Azoxystrobin; tolerances for Ginseng 1 ...... 0 .5 residues. Grain, aspirated fractions ...... 420 Grass, forage ...... 15 (a) General. (1) Tolerances are estab- Grass, hay ...... 20 lished for residues of the fungicide, Guava ...... 2 .0 Herb Subgroup 19A, dried leaves ...... 260 azoxystrobin, including its metabolites Herb Subgroup 19A, fresh leaves ...... 50 and degradates, in or on the commod- Hop, dried cones ...... 20 .0 ities in the following table. Compliance Ilama ...... 2 .0 Jaboticaba ...... 2 .0 with the tolerance levels specified in Jackfruit ...... 2 .0 the table is to be determined by meas- Longan ...... 2 .0 uring only the sum of azoxystrobin, Loquat ...... 2 .0 [methyl(E)-2-(2-(6-(2-cyanophenoxy) Lychee ...... 2 .0 Mango ...... 2.0 pyrimidin-4-yloxy)phenyl)-3- Nut, tree, group 14–12, except pistachio ...... 0 .02 methoxyacrylate], and the Z-isomer of Oats, forage ...... 5 .0 azoxystrobin [methyl(Z)-2-(2-(6-(2- Oats, grain ...... 1 .5 Oats, hay ...... 10.0 cyanophenoxy)pyrimidin-4- Oats, straw ...... 3.0 yloxy)phenyl)-3 methoxyacrylate] in or Onion, bulb, subgroup 3–07A ...... 1 .0 on the commodity. Onion, green, subgroup 3–07B ...... 7 .5 Papaya ...... 2 .0 Parts per Passionfruit ...... 2 .0 Commodity million Pawpaw ...... 2 .0 Pea and bean, dried shelled, except soybean, Acerola ...... 2.0 subgroup 6C ...... 0 .5 Almond, hulls ...... 4 .0 Pea and bean, succulent shelled, subgroup 6B 0 .5 Animal feed, nongrass, group 18, forage ...... 45 Peanut ...... 0 .2 Animal feed, nongrass, group 18, hay ...... 120 Peanut, hay ...... 15.0 Artichoke, globe ...... 4.0 Peanut, refined oil ...... 0.6 Asparagus ...... 0.04 Pear, Asian 1 ...... 0 .07 Atemoya ...... 2 .0 Pepper/eggplant subgroup 8–10B ...... 3 .0 Avocado ...... 2 .0 Peppermint, tops ...... 30 Banana ...... * Persimmon ...... 2 .0 Barley, bran ...... 6 .0 Pistachio ...... 0.50 Barley, forage ...... 25 Pulasan ...... 2 .0 Barley, grain ...... 3 .0 Quinoa, grain ...... 3 .0 Barley, hay ...... 10 .0 Rambutan ...... 2 .0 Barley, straw ...... 15 .0 Rapeseed subgroup 20A ...... 1 .0 Berry, low growing, subgroup 13–07G, except Rice, grain ...... 5 .0 cranberry ...... 10.0 Rice, hulls ...... 20 Biriba ...... 2 .0 Rice, wild, grain ...... 5.0 Brassica, head and stem, subgroup 5A ...... 3 .0 Rye, forage ...... 7 .0 Brassica, leafy greens, subgroup 5B ...... 25 Rye, grain ...... 0.2 Bushberry subgroup 13–07B ...... 5 .0 Rye, straw ...... 1 .5 Caneberry subgroup 13–07A ...... 5.0 Sapodilla ...... 2 .0

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Parts per Parts per Commodity million Commodity million

Sapote, black ...... 2 .0 Horse, meat ...... 0 .01 Sapote, mamey ...... 2 .0 Horse, meat byproducts ...... 0 .07 Sapote, white ...... 2 .0 Milk...... 0 .006 Sorghum, grain, forage ...... 25 Sheep, fat ...... 0 .03 Sorghum, grain, grain ...... 11 Sheep, meat ...... 0.01 Sorghum, grain, stover ...... 40 Sheep, meat byproducts ...... 0 .07 Soursop ...... 2 .0 Soybean, hay ...... 55 .0 Soybean, hulls ...... 1 .0 (b) Section 18 emergency exemptions. Soybean, seed ...... 0 .5 [Reserved] Spanish lime ...... 2 .0 Spearmint, tops ...... 30 (c) Tolerances with regional registra- Spice Subgroup 19B, except black pepper ...... 38 tion. [Reserved] Star apple ...... 2 .0 (d) Indirect or inadvertent residues. Starfruit ...... 2 .0 Sugar apple ...... 2 .0 [Reserved] Sugarcane, cane ...... 0.2 [62 FR 32235, June 13, 1997] Sunflower subgroup 20B ...... 0.5 Tamarind ...... 2 .0 EDITORIAL NOTE: For FEDERAL REGISTER ci- 1 Tea, dried ...... 20 .0 tations affecting § 180.507, see the List of CFR Ti, leaves ...... 50 .0 Ti, roots ...... 0 .5 Sections Affected, which appears in the Tomato, paste ...... 0 .6 Finding Aids section of the printed volume Tomato subgroup 8–10A ...... 0 .2 and at www.fdsys.gov. Turnip, greens ...... 25 Vegetable, cucurbit, group 9 ...... 0.3 § 180.509 Mefenpyr-diethyl; tolerance Vegetable, foliage of legume, group 7 ...... 30.0 for residues. Vegetable, leafy, except brassica, group 4 ...... 30.0 Vegetable, leaves of root and tuber, group 2 ... 50 .0 (a) General. Tolerances are estab- Vegetable, legume, edible podded, subgroup lished for residues of the safener, 6A, except soybean ...... 3 .0 Vegetable, root, subgroup 1A ...... 0 .5 mefenpyr-diethyl, including its me- Vegetable, tuberous and corm, subgroup 1C ... 8.0 tabolites and degradates, when applied Wasabi, dry ...... 260 at a rate no greater than 0.053 pound Wasabi, fresh ...... 50 Watercress ...... 3 .0 safener per acre per growing season in Wax jambu ...... 2 .0 or on the commodities in the table Wheat, forage ...... 15.0 below. Compliance with the tolerance Wheat, grain ...... 0 .2 Wheat, hay ...... 30 .0 levels specified below is to be deter- Wheat, straw ...... 10 .0 mined by measuring only the sum of * 2.0 (of which not more than 0.1 is contained in the pulp) mefenpyr-diethyl (1-(2,4- 1 There are no United States registrations for use of dichlorophenyl)-4,5-dihydro-5-methyl- azoxystrobin on coffee, green bean; ginseng; pear, Asian and tea, dried. 1H-pyrazole-3,5-dicarboxylic acid, diethyl ester) and its 2,4- (2) Tolerances are established for res- dichlorophenyl-pyrazoline metabolites, idues of the fungicide, azoxystrobin, in- calculated as the stoichiometric equiv- cluding its metabolites and degradates, alent of mefenpyr-diethyl, in or on the in or on the commodities in the fol- commodity. lowing table. Compliance with the tolerance levels specified in the table is to Commodity Parts per be determined by measuring only million azoxystrobin, [methyl(E)-2-(2-(6-(2- Barley, grain ...... 0 .05 cyanophenoxy) pyrimidin-4- Barley, hay ...... 0 .2 yloxy)phenyl)-3-methoxyacrylate] in or Barley, straw ...... 0 .5 on the commodity. Cattle, meat byproducts ...... 0.1 Goat, meat byproducts ...... 0 .1 Grass, forage ...... 1 .6 Parts per Commodity million Grass, hay ...... 0 .2 Hog, meat byproducts ...... 0 .1 Cattle, fat ...... 0.03 Horse, meat byproducts ...... 0 .1 Cattle, meat ...... 0 .01 Sheep, meat byproducts ...... 0 .1 Cattle, meat byproducts ...... 0.07 Sorghum, grain, forage ...... 0.4 Goat, fat ...... 0 .03 Sorghum, grain, grain ...... 0 .04 Goat, meat ...... 0.01 Sorghum, grain, stover ...... 0 .2 Goat, meat byproducts ...... 0 .07 Wheat, forage ...... 0 .2 Hog, fat ...... 0 .010 Wheat, grain ...... 0 .05 Hog, meat ...... 0 .01 Wheat, hay ...... 0 .2 Hog, meat byproducts ...... 0 .010 Wheat, straw ...... 0 .5 Horse, fat ...... 0 .03

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(b) Section 18 emergency exemptions. Commodity Parts per [Reserved] million (c) Tolerances with regional registra- Biriba ...... 0 .20 tions. [Reserved] Brassica, head and stem, subgroup 5A ...... 0 .70 (d) Indirect or inadvertent residues. Brassica, leafy greens, subgroup 5B ...... 2 .0 Bushberry subgroup 13–07B ...... 1 .0 Tolerances are established for the indi- Cacao bean, dried ...... 0 .02 rect or inadvertent residues of Caneberry subgroup 13–07A ...... 1.0 mefenpyr-diethyl, including its me- Canistel ...... 1 .0 Canola, seed ...... 0 .20 tabolites and degradates, when applied Cherimoya ...... 0 .20 at a rate no greater than 0.053 pound Citrus, oil ...... 20 safener per acre per growing season in Citrus, dried pulp ...... 2 .0 or on the commodities identified in the Coffee, instant ...... 0 .10 Coffee, green bean ...... 0 .02 table below. Compliance with the toler- Cotton, gin byproducts ...... 2 .0 ance levels specified below is to be de- Cotton, undelinted seed ...... 0 .05 termined by measuring only the sum of Custard apple ...... 0 .20 Date ...... 0 .30 mefenpyr-diethyl (1-(2,4- Feijoa ...... 0 .10 dichlorophenyl)-4,5-dihydro-5-methyl- Fig ...... 0 .30 1H-pyrazole-3,5-dicarboxylic acid, Fig, dried fruit ...... 1 .0 Fruit, citrus, group 10–10 ...... 0 .50 diethyl ester) and its 2,4- Fruit, pome, group 11–10 ...... 0 .20 dichlorophenyl-pyrazoline metabolites, Fruit, small, vine climbing, except grape, sub- calculated as the stoichiometric equiv- group 13–07E ...... 0 .35 alent of mefenpyr-diethyl, in or on the Fruit, stone, group 12 ...... 1 .0 Grain, cereal, group 15 ...... 1.1 commodity. Grain, cereal, forage, fodder and straw, group 16 ...... 1 .1 Commodity Parts per Grape ...... 2 .5 million Grass, forage, fodder, and hay, group 17, forage ...... 0 .70 Canola, seed ...... 0 .02 Grass, forage, fodder, and hay, group 17, hay 1 .1 Soybean, forage ...... 0 .1 Guava ...... 0 .10 Soybean, hay ...... 0 .1 Herb subgroup 19A ...... 100 Soybean, seed ...... 0 .02 Ilama ...... 0 .20 Jaboticaba ...... 0 .10 [73 FR 74977, Dec. 10, 2008, as amended at 76 Lychee ...... 0 .30 FR 23903, Apr. 29, 2011] Mango ...... 1.0 Nut, tree, group 14 ...... 0 .02 Olive ...... 1 .0 § 180.510 Pyriproxyfen; tolerances for Olive, oil ...... 2 .0 residues. Papaya ...... 1 .0 Passionfruit ...... 0 .10 (a) General. (1) Tolerances are estab- Pawpaw ...... 1 .0 lished for residues of pyriproxyfen, in- Peanut ...... 0 .20 cluding its metabolites and degradates, Pineapple ...... 0.30 in or on the commodities in the fol- Pineapple, process residue ...... 1 .1 Pistachio ...... 0.02 lowing table. Compliance with the tol- Pomegranate ...... 0 .20 erance levels specified is determined by Potato, chips ...... 0 .75 measuring only pyriproxyfen, 2-[1- Potato, granules/flakes ...... 0 .75 Potato, wet peel ...... 0 .75 methyl-2-(4-phenoxyphenoxy) Pulasan ...... 0 .30 ethoxy]pyridine, in or on the com- Rambutan ...... 0 .30 modity. Rice, hulls ...... 5 .5 Safflower, seed ...... 0 .20 Parts per Sapodilla ...... 1 .0 Commodity million Sapote, black ...... 1 .0 Sapote, mamey ...... 1 .0 Acerola ...... 0.10 Sapote, white ...... 0 .30 Almond, hulls ...... 2 .0 Sesame, seed ...... 0 .02 Animal feed, nongrass, group 18, forage ...... 0 .70 Soursop ...... 0 .20 Animal feed, nongrass, group 18, hay ...... 1.1 Spanish lime ...... 0 .30 Animal feed, nongrass, group 18, seed ...... 2 .0 Star apple ...... 1 .0 Apple, wet pomace ...... 0 .8 Starfruit ...... 0 .10 Artichoke, globe ...... 2.0 Strawberry ...... 0 .30 Asparagus ...... 2.0 Sugar apple ...... 0 .20 Atemoya ...... 0 .20 Sugarcane ...... 1 .1 Avocado ...... 1 .0 Tea ...... 15 Banana ...... 0.20 Vegetable, bulb, group 3–07 ...... 0 .70 Beet, sugar, dried pulp ...... 3 .0 Vegetable, cucurbit, group 9 ...... 0.10 Berry, low growing, except strawberry, sub- Vegetable, foliage of legume, group 7 ...... 2 .0 group 13–07H ...... 1.0 Vegetable, fruiting, group 8–10 ...... 0 .80

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below. Compliance with the tolerance Commodity Parts per million levels specified below is to be deter- Vegetable, leafy, except Brassica, group 4 ...... 3 .0 mined by measuring only the Vegetable, leaves of root and tuber, group 2 ... 2 .0 buprofezin, 2-[(1,1- Vegetable, legume, group 6 ...... 0 .20 dimethylethyl)imino]tetrahydro-3(1- Vegetable, root and tuber, group 1 ...... 0 .15 Walnut ...... 0 .02 methylethyl)-5-phenyl-4H-1,3,5- Watercress ...... 2 .0 thiadiazin-4-one, in the commodity. Wax jambu ...... 0 .10 Commodity Parts per (2) A tolerance of 0.10 parts per mil- million lion is established for all food commod- Acerola ...... 0.30 ities as a result of the proposed use of Almond, hulls ...... 2 .0 Apricot ...... 9 .0 NYLAR in food handling establish- Atemoya ...... 0 .30 ments where food and food products are Avocado ...... 0 .30 held, prepared, processed or served. Ap- Banana ...... 0.20 plication is limited to space, general Bean, snap, succulent ...... 0 .02 Bean, succulent ...... 0 .02 surface, spot, and/or crack and crevice Berry, low growing, subgroup 13-07G ...... 2 .5 treatment in food handling establish- Birida ...... 0 .30 ments where food and food products are Brassica, head and stem, subgroup 5A ...... 12.0 Brassica, leafy greens, subgroup 5B ...... 60 held, processed, prepared and served. Canistel ...... 0 .90 Space and general surface application Cattle, fat ...... 0.05 may be used only when the facility is Cattle, kidney ...... 0 .05 Cattle, liver ...... 0 .05 not in operation provided exposed food Cattle, meat ...... 0 .05 is covered or removed from the area Cattle, meat byproducts ...... 0.05 being treated prior to application. Cherimoya ...... 0 .30 Citrus, dried pulp ...... 7 .5 Spot, and/or crack and crevice treat- Citrus, oil ...... 80 ment may be used while the facility is Coffee, green bean ...... 0 .35 in operation provided exposed food is Cotton, gin byproducts ...... 20 .0 covered or removed from the area Cotton, undelinted seed ...... 0 .35 Custard apple ...... 0 .30 being treated prior to application. Feijoa ...... 0 .30 Food contact surfaces should be thor- Fruit, citrus, group 10 ...... 2 .5 oughly washed with an effective clean- Fruit, pome, group 11–10, except pear and pear, Asian ...... 3 .0 ing compound and rinced with potable Fruit, stone, group 12, except apricot and water after use of the product. To as- peach ...... 1 .9 sure safe use of this additive, its label Goat, fat ...... 0 .05 Goat, kidney ...... 0 .05 and labeling shall conform to that reg- Goat, liver ...... 0.05 istered with the U.S. Environmental Goat, meat ...... 0.05 Protection Agency, and shall be used in Goat, meat byproducts ...... 0 .05 accordance with such label and label- Grape ...... 2 .5 Guava ...... 0 .3 ing. Hog, fat ...... 0 .05 (b) Section 18 emergency exemptions. Hog, kidney ...... 0.05 [Reserved] Hog, liver ...... 0 .05 Hog, meat ...... 0 .05 (c) Tolerances with regional registra- Hog, meat byproducts ...... 0 .05 tions. [Reserved] Horse, fat ...... 0 .05 (d) Indirect or inadvertent residues. Horse, kidney ...... 0 .05 Horse, liver ...... 0 .05 [Reserved] Horse, meat ...... 0 .05 [64 FR 10233, Mar. 3, 1999] Horse, meat byproducts ...... 0 .05 Ilama ...... 0 .30 EDITORIAL NOTE: For FEDERAL REGISTER ci- Jaboticaba ...... 0 .30 tations affecting § 180.510, see the List of CFR Lettuce, head ...... 6.0 Sections Affected, which appears in the Longan ...... 0 .30 Lychee ...... 0 .30 Finding Aids section of the printed volume Mango ...... 0.90 and at www.fdsys.gov. Milk ...... 0.01 Nut, tree group 14 ...... 0.05 § 180.511 Buprofezin; tolerances for Olive ...... 3 .5 residues. Olive, oil ...... 4 .8 Papaya ...... 0 .90 (a) General. Tolerances are estab- Passionfruit ...... 0 .30 lished for residues of buprofezin, in- Peach ...... 9 .0 Pear ...... 6 .0 cluding its metabolites and degradates Pear, Asian ...... 6 .0 in or on the commodities in the table Persimmon ...... 1 .9

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pared, held, processed, or served and in Commodity Parts per million accordance with the following pre- Pistachio ...... 0.05 scribed conditions: Pomegranate ...... 1 .9 (i) Application shall be no greater Pulasan ...... 0 .30 than a 0.5% active ingredient solution Radicchio ...... 6.0 Rambutan ...... 0 .30 for spot crack and crevice use in food/ Sapodilla ...... 0 .90 feed handling establishments, where Sapote, black ...... 0 .90 food and food products are held, proc- Sapote, mamey ...... 0 .90 Sheep, fat ...... 0 .05 essed, prepared and/or served. Sheep, kidney ...... 0.05 (ii) Application may only be under- Sheep, liver ...... 0.05 taken when the facility is not in oper- Sheep, meat ...... 0.05 Sheep, meat byproducts ...... 0 .05 ation, and provided exposed food has Soursop ...... 0 .30 been covered, or removed from the area Spanish lime ...... 0 .30 being treated prior to application. Star apple ...... 0 .90 Starfruit ...... 0 .30 (iii) Food contact surfaces and equip- Sugar apple ...... 0 .30 ment should be throughly washed with Tea1 ...... 20 an effective cleaning compound, and Turnip, greens ...... 60 rinsed with potable water after each Vegetable, cucurbit, group 9 ...... 0.50 Vegetable, fruiting, group 8–10 ...... 2 .0 use of the product. Vegetable, leafy, except Brassica, group 4, ex- (iv) Contamination of food or food cept head lettuce and radicchio ...... 35 contact surfaces shall be avoided. Ap- Wax jambu ...... 0 .30 plication excludes any direct applica- 1 There are no U.S. registrations at this time. tion to any food, food packaging, or (b) Section 18 emergency exemption. any food contact surfaces. [Reserved] (v) To assure safe use, the label and (c) Tolerances with regional registra- labeling shall conform to that reg- tions. [Reserved] istered by the U.S. Environmental Pro- (d) Indirect or inadvertent residues. tection Agency, and it shall be used in [Reserved] accordance with such label and labeling. [62 FR 40741, July 30, 1997] (b) Section 18 emergency exemptions. EDITORIAL NOTE: For FEDERAL REGISTER ci- [Reserved] tations affecting § 180.511, see the List of CFR (c) Tolerances with regional registra- Sections Affected, which appears in the Finding Aids section of the printed volume tions. [Reserved] and at www.fdsys.gov. (d) Indirect or inadvertent residues. [Reserved] § 180.512 [Reserved] [68 FR 55527, Sept. 26, 2003, as amended at 70 FR 3654, Jan. 26, 2005] § 180.513 Chlorfenapyr; tolerances for residues. § 180.514 Cloransulam-methyl; toler- (a) General. (1) Tolerances are estab- ances for residues. lished for residues of the insecticide (a) General. Tolerances are estab- chlorfenapyr [4-bromo-2-(4- lished for residues of the herbicide, chlorophenyl)-1-(ethoxymethyl)-5- cloransulam-methyl, N-(2- (trifluoromethyl)-1H-pyrrole-3- carboxymethyl-6-chlorophenyl)-5- carbonitrile] in or on the following raw ethoxy-7-fluoro-(1,2,4)-triazolo[1,5c]-py- agricultural commodities: rimidine-2-sulfonamide, plus its acid, Parts per cloransulam, calculated as parent ester Commodity million in or on the following raw agricultural commodities: Vegetable, fruiting, group 8 ...... 1.0 Parts per (2) A tolerance of 0.01 parts per mil- Commodity million lion is established for residues of Soybean, forage ...... 0 .1 chlorfenapyr in or on all food commod- Soybean, hay ...... 0 .2 ities (other than those covered by a Soybean, seed ...... 0 .02 higher tolerance as a result of use on growing crops) in food/feed handling (b) Section 18 emergency exemptions. areas where food/feed products are pre- [Reserved]

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(c) Tolerances with regional registra- Commodity Parts per tions. [Reserved] million (d) Indirect or inadvertent residues. Goat, meat ...... 0.10 [Reserved] Goat, meat byproducts ...... 0 .10 Grain, aspirated grain fractions ...... 1 .8 [62 FR 49163, Sept. 19, 1997] Grain, cereal, group 15 (except rice grain and sorghum grain) ...... 0 .10 § 180.515 Carfentrazone-ethyl; toler- Grain, cereal, group 16, forage ...... 1 .0 ances for residues. Grain, cereal, group 16, hay ...... 0 .30 Grain, cereal, group 16, stover ...... 0 .80 (a) General. Tolerances are estab- Grain, cereal, group 16, straw ...... 3 .0 lished for residues of the herbicide Grass, forage ...... 5 .0 Grass, hay ...... 8 .0 carfentrazone-ethyl, including its me- Guava ...... 0 .10 tabolites and degradates, in or on the Herbs and spices group 19 ...... 2.0 commodities listed in the following Hog, fat ...... 0 .10 Hog, meat ...... 0 .10 table. Compliance with the following Hog, meat byproducts ...... 0 .10 tolerance levels is to be determined by Hop, dried cones ...... 0 .10 measuring only the sum of Horse, fat ...... 0 .10 carfentrazone-ethyl (ethyl-alpha-2- Horse, meat ...... 0 .10 Horse, meat byproducts ...... 0 .10 dichloro-5-[-4-(difluoromethyl)-4,5- Horseradish ...... 0.10 dihydro-3-methyl-5-oxo-1H -1,2,4- Ilama ...... 0 .10 triazol-1-yl]-4- Jaboticaba ...... 0 .10 Kava, roots ...... 0 .10 fluorobenzenepropanoate) and its me- Kiwifruit ...... 0.10 tabolite carfentrazone-chloropropionic Longan ...... 0 .10 acid (alpha, 2-dichloro-5-[-4- Lychee ...... 0 .10 difluoromethyl)-4,5-dihydro-3-methyl-5- Mango ...... 0.10 Milk ...... 0.05 oxo-1H-1,2,4-triazol-1-yl]-4- Noni ...... 0 .10 fluorobenzenepropanoic acid), cal- Nut, tree, group 14–12 ...... 0 .10 culated as the stoichiometric equiva- Olive ...... 0 .10 Palm heart ...... 0 .10 lent of carfentrazone-ethyl, in or on Palm heart, leaves ...... 0 .10 the following commodities: Papaya ...... 0 .10 Passionfruit ...... 0 .10 Commodity Parts per Pawpaw ...... 0 .10 million Peanut ...... 0 .10 Peanut, hay ...... 0.10 Acerola ...... 0.10 Peppermint, tops ...... 0 .10 Almond, hulls ...... 0 .20 Persimmon ...... 0 .10 Animal feed, nongrass, crop group 18, forage 2 .0 Pomegranate ...... 0 .10 Animal feed, nongrass, crop group 18, hay ...... 5 .0 Poultry, meat byproducts ...... 0.10 Animal feed, nongrass, crop group 18, seed .... 15 .0 Psyllium, seed ...... 0 .10 Artichoke, globe ...... 0.10 Pulasan ...... 0 .10 Asparagus ...... 0.10 Quinoa, grain ...... 0 .10 Atemoya ...... 0 .10 Avocado ...... 0 .10 Rambutan ...... 0 .10 Banana ...... 0.10 Rapeseed, forage ...... 0 .10 Berry, low growing, subgroup 13–07G ...... 0 .10 Rapeseed subgroup 20A ...... 0 .10 Birida ...... 0 .10 Rice, grain ...... 1 .3 Bushberry subgroup 13–07B ...... 0 .10 Sapodilla ...... 0 .10 Cacao bean, bean ...... 0 .10 Sapote, black ...... 0 .10 Cactus ...... 0 .10 Sapote, mamey ...... 0 .10 Caneberry subgroup 13–07A ...... 0.10 Sheep, fat ...... 0 .10 Canistel ...... 0 .10 Sheep, meat ...... 0.10 Cattle, fat ...... 0.10 Sheep, meat byproducts ...... 0 .10 Cattle, meat ...... 0 .10 Shellfish ...... 0 .30 Cattle, meat byproducts ...... 0.10 Sorghum, grain ...... 0 .25 Cherimoya ...... 0 .10 Soursop ...... 0 .10 Coffee, bean, green ...... 0 .10 Soybean, seed ...... 0 .10 Cotton, gin byproducts ...... 10 Spanish lime ...... 0 .10 Cottonseed subgroup 20C ...... 0 .20 Spearmint, tops ...... 0 .10 Custard apple ...... 0 .10 Star apple ...... 0 .10 Date, dried fruit ...... 0 .10 Starfruit ...... 0 .10 Feijoa ...... 0 .10 Stevia ...... 0 .10 Fig ...... 0 .10 Strawberrypear ...... 0 .10 Fish ...... 0 .30 Sugar apple ...... 0 .10 Fruit, citrus, group 10–10 ...... 0 .10 Sugarcane ...... 0 .15 Fruit, pome, group 11–10 ...... 0 .10 Sunflower, subgroup 20B ...... 0 .10 Fruit, small vine climbing, subgroup 13–07F, Tea, dried ...... 0 .10 except Fuzzy kiwifruit ...... 0.10 Teff, forage ...... 1 .0 Fruit, stone, group 12–12 ...... 0 .10 Teff, grain ...... 0 .25 Goat, fat ...... 0 .10 Teff, hay ...... 0 .30

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Parts per Parts per Commodity million Commodity million

Teff, straw ...... 3 .0 Cotton, undelinted seed ...... 0 .05 Ti, leaves ...... 0 .10 Custard apple ...... 20 Ti, roots ...... 0 .10 Dragon fruit ...... 1 .0 Vanilla ...... 0 .10 Feijoa ...... 5 .0 Vegetable, brassica, leafy, group 5 ...... 0.10 Flax, seed ...... 0 .05 Vegetable, bulb, group 3–07 ...... 0 .10 Fruit, citrus, group 10–10 ...... 10 Vegetable, cucurbit, group 9 ...... 0.10 Fruit, pome, group 11–10 ...... 5 .0 Vegetable, foliage of legume, except soybean, Fruit, small vine climbing, except fuzzy kiwifruit, subgroup 7A ...... 0 .10 subgroup 13–07F ...... 2 .0 Vegetable, fruiting, group 8–10 ...... 0 .10 Fruit, stone, group 12–12 ...... 5 .0 Vegetable, leafy, except brassica, group 4 ...... 0 .10 Ginseng ...... 4 .0 Vegetable, leaves of root and tuber, group 2 ... 0 .10 Grain, cereal, group 15 ...... 0.02 Vegetable, legume, group 6 ...... 0 .10 Grain, cereal, forage, fodder, and straw, group Vegetable, root and tuber, group 1 ...... 0 .10 16 ...... 0 .01 Wasaba, roots ...... 0.10 Grass, forage, fodder and hay, group 17 ...... 0 .01 Wax jambu ...... 0 .10 Guava ...... 5 .0 1 Effective Date to be removed: May 18, 2016. Herb subgroup 19A, dried leaves ...... 65 Herb subgroup 19A, fresh leaves ...... 10 (b) Section 18 emergency exemptions. Ilama ...... 20 [Reserved] Jaboticaba ...... 5 .0 Kiwifruit, fuzzy ...... 20 (c) Tolerances with regional registra- Leaf petioles subgroup 4B ...... 15 tions. [Reserved] Leafy greens subgroup 4A ...... 30 (d) Indirect or inadvertent residues. Longan ...... 20 [Reserved] Lychee ...... 20 Mango ...... 5.0 [63 FR 52180, Sept. 30, 1998] Melon subgroup 9A ...... 0 .03 Onion, bulb, subgroup 3–07A ...... 0 .50 EDITORIAL NOTE: For FEDERAL REGISTER ci- Onion, green, subgroup 3–07B ...... 7 .0 tations affecting § 180.515, see the List of CFR Papaya ...... 5 .0 Sections Affected, which appears in the Passionfruit ...... 5 .0 Finding Aids section of the printed volume Peanut ...... 0 .01 Peanut, hay ...... 0.01 and at www.fdsys.gov. Pineapple ...... 20 Pistachio ...... 0.10 § 180.516 Fludioxonil; tolerances for Pomegranate ...... 5 .0 residues. Pulasan ...... 20 Rambutan ...... 20 (a) General. (1) Tolerances are estab- Rapeseed, forage ...... 0 .01 lished for residues of the fungicide Rapeseed subgroup 20A, except flax seed ...... 0 .01 fludioxonil, including its metabolites Safflower, seed ...... 0 .01 Sapodilla ...... 5 .0 and degradates, in or on the commod- Sapote, black ...... 5 .0 ities in the following table. Compliance Sapote, mamey ...... 5 .0 with the tolerance levels specified in Soursop ...... 20 the following table is to be determined Spanish lime ...... 20 Spice subgroup 19B ...... 0 .02 by measuring only fludioxonil, 4-(2,2- Star apple ...... 5 .0 difluoro-1,3-benzodioxol-4-yl)-1-H- Starfruit ...... 5 .0 pyrrole-3-carbonitrile). Sugar apple ...... 20 Sunflower, seed ...... 0.01 Parts per Tomato ...... 5.0 Commodity million Turnip, greens ...... 10 Vegetable, cucurbit, group 9 ...... 0.45 Acerola ...... 5.0 Vegetable, foliage of legume, group 7 ...... 0 .01 Animal feed, nongrass, group 18 ...... 0 .01 Vegetable, fruiting, group 8–10, except tomato .. 0 .50 Atemoya ...... 20 Vegetable, leaves of root and tuber, group 2 ..... 30 Avocado ...... 5 .0 Vegetable, legume, group 6 ...... 0 .01 Bean, dry ...... 0.4 Vegetable, root, except sugar beet, subgroup Bean, succulent ...... 0 .4 1B ...... 0 .75 Beet, sugar, roots ...... 0 .02 Vegetable, tuberous and corm, subgroup 1C ..... 6.0 Berry, low growing, subgroup 13–07G, except Watercress ...... 7 .0 cranberry ...... 3.0 Wax jambu ...... 5 .0 Biriba ...... 20 Yam, true, tuber ...... 8.0 Brassica, head and stem, subgroup 5A ...... 2 .0 Brassica, leafy greens, subgroup 5B ...... 10 (2) Tolerances are established for res- Bushberry subgroup 13–07B ...... 2 .0 Caneberry subgroup 13–07A ...... 5.0 idues of the fungicide fludioxonil, in- Canistel ...... 5 .0 cluding its metabolites and degradates, Carrots ...... 7 .0 in or on the commodities in the fol- Cherimoya ...... 20 Citrus, oil ...... 500 lowing table. Compliance with the tol- Cotton, gin byproducts ...... 0 .05 erance levels specified in the following

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table is to be determined by measuring Commodity Parts per only the sum of fludioxonil, 4-(2,2- million difluoro-1,3-benzodioxol-4-yl)-1-H- Cattle, liver ...... 0 .10 pyrrole-3-carbonitrile), and its metabo- Cattle, meat ...... 0 .04 lites converted to 2,2-difluoro-l,3- Cattle, meat byproducts, except liver ...... 0 .04 Corn, field, grain ...... 0 .02 benzodioxole-4-carboxylic acid, cal- Corn, field, stover ...... 0 .30 culated as the stoichiometric equiva- Corn, field, forage ...... 0 .15 lent of fludioxonil. Egg ...... 0 .03 Goat, fat ...... 0 .40 Goat, liver ...... 0.10 Parts per Commodity million Goat, meat ...... 0.04 Goat, meat byproducts, except liver ...... 0 .04 Cattle, fat ...... 0.05 Hog, fat ...... 0 .04 Cattle, meat ...... 0 .01 Hog, liver ...... 0 .02 Cattle, meat byproducts ...... 0.05 Hog, meat ...... 0 .01 Goat, fat ...... 0 .05 Hog, meat byproducts, except liver ...... 0 .01 Goat, meat ...... 0.01 Horse, fat ...... 0 .40 Goat, meat byproducts ...... 0 .05 Horse, liver ...... 0 .10 Horse, fat ...... 0 .05 Horse, meat ...... 0 .04 Horse, meat ...... 0 .01 Horse, meat byproducts, except liver ...... 0 .04 Milk, fat (reflecting 0.05 ppm in whole milk) ..... 1 .50 Horse, meat byproducts ...... 0 .05 Potato ...... 0 .03 Milk ...... 0.01 Potato, wet peel ...... 0 .10 Sheep, fat ...... 0 .05 Poultry, fat ...... 0.05 Sheep, meat ...... 0.01 Poultry, meat ...... 0 .02 Sheep, meat byproducts ...... 0 .05 Poultry, meat byproducts ...... 0.02 Rice, grain ...... 0 .04 (b) Section 18 emergency exemptions. Sheep, fat ...... 0 .40 [Reserved] Sheep, liver ...... 0.10 Sheep, meat ...... 0.04 (c) Tolerances with regional registra- Sheep, meat byproducts, except liver ...... 0 .04 tions. [Reserved] (d) Indirect or inadvertent residues. (b) Section 18 emergency exemptions.. [Reserved] Time-limited tolerances are estab- [62 FR 56082, Oct. 29, 1997] lished for combined residues of the insecticide, fipronil, 5-amino-1-(2,6- EDITORIAL NOTE: For FEDERAL REGISTER ci- dichloro-4-(trifluoromethyl) phenyl)-4- tations affecting § 180.516, see the List of CFR ((1,R,S)-trifluoromethyl)sulfinyl)-1-H- Sections Affected, which appears in the Finding Aids section of the printed volume pyrazole-3-carbonitrile and its 2 me- and at www.fdsys.gov. tabolites MB45950 (5-amino-1-(2,6- dichloro-4-(trifluoromethyl)phenyl)-4- § 180.517 Fipronil; tolerances for resi- [(trifluoromethyl)thio]-1H-pyrazole-3- dues. carbonitrile) and MB46136 (5-amino-1- (a) General. Therefore, tolerances are (2,6-dichloro-4- established for combined residues of (trifluoromethyl)phenyl)-4- the insecticide fipronil (5-amino-1-[2,6- [(trifluoromethyl)sulfonyl]-1H-pyr- dichloro-4-(trifluoromethyl)phenyl]-4- azole-3-carbonitrile) and its [(1R,S)-(trifluoromethyl)sulfinyl]-1H- photodegradate MB46513 (5-amino-1- pyrazole-3-carbonitrile) and its me- (2,6-dichloro-4- tabolites 5-amino-1-[2,6-dichloro-4- (trifluoromethyl)phenyl]-4-[(1R,S)- (trifluoromethyl)phenyl]-4- (trifluoromethyl)]-1H-pyrazole-3- [(trifluoromethyl) sulfonyl]-1H-pyr- carbonitrile), in connection with use of azole-3-carbonitrile and 5-amino-1-[2,6- the pesticide under Section 18 emer- dichloro-4-(trifluoromethyl) phenyl]-4- gency exemptions granted by EPA. The [(trifluoromethyl)thio]-1H-pyrazole-3- tolerances expire and are revoked on carbonitrile and its photodegradate 5- the dates specified in the table for this amino-1-(2,6-dichloro-4- paragraph. (trifluoromethyl)phenyl]-4-[(1R,S)- Parts per Expiration/ (trifluoromethyl)]-1H-pyrazole-3- Commodity million revocation carbonitrile in or on the following date items at the levels specified: Rutabaga ...... 1.0 12/31/16 Turnip ...... 1.0 12/31/16 Commodity Parts per million (c) Tolerances with regional registra- Cattle, fat ...... 0.40 tions. [Reserved]

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(d) Indirect or inadvertent residues. erance levels specified in the following Tolerances are established for com- table is to be determined by measuring bined indirect or inadvertent residues only the sum of pyrimethanil and its of the insecticide fipronil and its me- metabolite 4-[4,6-dimethyl-2- tabolites and photodegradate in or on pyrimidinyl)amino]phenol, calculated food commodities when present therein as the stoichiometric equivalent of as a result of the application of fipronil pyrimethanil. to growing crops listed in paragraphs (a) and (b) of this section and other Parts per Commodity million nonfood crops to read as follows: Cattle, fat ...... 0.01 Parts per Cattle, kidney ...... 2 .5 Commodity million Cattle, meat ...... 0 .01 Wheat, forage ...... 0 .02 Cattle, meat byproducts, except kidney ...... 0.01 Wheat, grain ...... 0 .005 Goat, fat ...... 0 .01 Wheat, hay ...... 0 .03 Goat, kidney ...... 2 .5 Wheat, straw ...... 0 .03 Goat, meat ...... 0.01 Goat, meat byproducts, except kidney ...... 0 .01 Horse, fat ...... 0 .01 [62 FR 62979, Nov. 26, 1997, as amended at 63 Horse, kidney ...... 2 .5 FR 38495, July 17, 1998; 72 FR 46913, Aug. 22, Horse, meat ...... 0 .01 2007; 74 FR 46377, Sept. 9, 2009; 75 FR 80346, Horse, meat byproducts, except kidney ...... 0 .01 Dec. 22, 2010; 78 FR 78748, Dec. 27, 2013; 80 FR Sheep, fat ...... 0 .01 72599, Nov. 20, 2015] Sheep, kidney ...... 2.5 Sheep, meat ...... 0.01 § 180.518 Pyrimethanil; tolerances for Sheep, meat byproducts, except kidney ...... 0 .01 residues. (3) Tolerances are established for res- (a) General. (1) Tolerances are estab- idues of the fungicide pyrimethanil, in- lished for residues of the fungicide cluding its metabolites and degradates, pyrimethanil, including its metabolites in or on the commodities in the fol- and degradates, in or on the commodities in the following table Compliance lowing table. Compliance with the tol- with the tolerance levels specified in erance levels specified in the following the following table is to be determined table is to be determined by measuring by measuring only pyrimethanil (4,6-di- only the sum of pyrimethanil and its metabolite 4,6-dimethyl-2- methyl-N-phenyl-2-pyrimidinamine). (phenylamino)-5-pyrimidinol, cal- Commodity Parts per culated as the stoichiometric equiva- million lent of pyrimethanil. Almond ...... 0.20 Almond, hulls ...... 12 Parts per Commodity million Apple, wet pomace ...... 40 Banana ...... 0.10 Milk ...... 0.05 Berry, low growing, subgroup 13–07G ...... 3 .0 Bushberry subgroup 13–07B ...... 8 .0 Caneberry subgroup 13–07A ...... 15 (b) Section 18 emergency exemptions. Citrus, oil ...... 150 [Reserved] Cucumber ...... 1 .5 Fruit, citrus, group 10–10 ...... 10 (c) Tolerances with regional registra- Fruit, pome, group 11–10 ...... 15 tions. [Reserved] Fruit, small, vine climbing, subgroup 13–07F, (d) Indirect or inadvertent residues. except fuzzy kiwifruit ...... 5 .0 Fruit, stone, group 12–12 ...... 10 [Reserved] Ginseng ...... 1 .5 Grape, raisin ...... 8 .0 [62 FR 63669, Dec. 2, 1997, as amended at 69 Onion, bulb, subgroup 3–07A ...... 0 .2 FR 52443, Aug. 26, 2004; 73 FR 64251, Oct. 29, Onion, green, subgroup 3–07B ...... 3 .0 2008; 74 FR 32448, July 8, 2009; 77 FR 45503, Pistachio ...... 0.20 Aug. 1, 2012; 80 FR 7975, Feb. 13, 2015; 80 FR Pomegranate ...... 5 .0 63691, Oct. 21, 2015] Tomato subgroup 8–10A ...... 0 .50 Vegetable, tuberous and corm, subgroup 1C ... 0.05 § 180.519 Bromide ion and residual (2) Tolerances are established for res- bromine; tolerances for residues. idues of the fungicide pyrimethanil, in- (a) General. The food additives, bro- cluding its metabolites and degradates, mide ion and residual bromine, may be in or on the commodities in the fol- present in water, potable in accordance lowing table. Compliance with the tol- with the following conditions:

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(1) The food additives are present as (d) Indirect or inadvertent residues. a result of treating water aboard ships [Reserved] with a polybrominated ion-exchange [40 FR 14156, Mar. 28, 1975. Redesignated at 41 resin (as a source of bromine) under the FR 26568, June 28, 1976, as amended at 49 FR supervision of trained personnel. 44459, Nov. 7, 1984. Further redesignated at 53 (2) Residual bromine levels are con- FR 24667, June 29, 1988, as amended at 54 FR trolled to not exceed 1.0 part per mil- 6130, Feb. 8, 1989. Further redesignated and lion (ppm) in the final treated water. amended at 63 FR 34319, June 24, 1998] Control is effected using calibrated re- § 180.522 Fumigants for processed circulating or proportioning bromine grains used in production of fer- feeder equipment and periodic checks mented malt beverage; tolerances of residual bromine using a bromine for residues. test kit. To assure safe use of the addi- (a) General. Fumigants for processed tives, the label and labeling of the dis- grain may be safely used, in accordance infectant formulation containing the with the following conditions. food additives shall conform to the (1) Methyl bromide. Total residues of label and labeling registered by the inorganic bromides (calculated as Br) U.S. Environmental Protection Agen- from the use of this fumigant shall not cy. exceed 125 parts per milion. (3) No tolerance is established for (2) Methyl bromide is used to fumi- bromide ion levels. gate corn grits and cracked rice in the (b) Section 18 emergency exemptions. production of fermented malt beverage. [Reserved] (3) To assure safe use of the fumi- (c) Tolerances with regional registra- gant, its label and labeling shall con- tions. [Reserved] form to the label and labeling reg- (d) Indirect or inadvertent residues. istered by the U.S. Environmental Pro- [Reserved] tection Agency, and the usage employed should conform with such label [41 FR 17893, Apr. 29, 1976. Redesignated at 41 or labeling. FR 26568, June 28, 1976, and at 53 FR 24667, (4) The total residue of inorganic bro- June 29, 1988. Redesignated and amended at mides in fermented malt beverage, re- 63 FR 34319, June 24, 1998; 71 FR 74818, Dec. sulting from the use of corn grits and 13, 2006] cracked rice fumigated with the fumi- § 180.521 Fumigants for grain-mill ma- gant described in paragraph (a)(2) of chinery; tolerances for residues. this section plus additional residues of inorganic bromides that may be (a) General. Fumigants may be safely present from uses in accordance with used in or on grain-mill machinery in other regulations in this chapter pro- accordance with the following pre- mulgated under section 408 and/or 409 scribed conditions: of the Act, does not exceed 25 parts per (1) The fumigants consist of methyl million bromide (calculated as Br). bromide. (b) Section 18 emergency exemptions. (2) To assure safe use of the fumi- [Reserved] gant, its label and labeling shall con- (c) Tolerances with regional registra- form to the label and labeling reg- tions. [Reserved] istered by the U.S. Environmental Pro- (d) Indirect or inadvertent residues. tection Agency. [Reserved] (3) Residues of inorganic bromides [71 FR 74818, Dec. 13, 2006] (calculated as Br) in milled fractions derived from cereal grain from all fu- § 180.523 Metaldehyde; tolerances for migation sources, including fumigation residues. of grain-mill machinery, shall not ex- (a) General. Tolerances are estab- ceed 125 parts per million. lished for residues of the molluscicide (b) Section 18 emergency exemptions. metaldehyde, including its metabolites [Reserved] and degradates, in or on the commod- (c) Tolerances with regional registra- ities listed in the following table. Com- tions. [Reserved] pliance with the specified tolerance

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levels is to be determined by meas- § 180.525 Resmethrin; tolerances for uring only metaldehyde, 2,4,6,8- residues. tetramethyl-1,3,5,7-tetroxocane, in or (a) General. Tolerances are estab- on the commodity. lished for residues of the insecticide resmethrin [5-(phenylmethyl)-3- Commodity Parts per million furanyl] methyl 2,2-dimethyl-3-(2- Artichoke, globe ...... 0.07 methyl-1-propenyl) Berry, low growing, subgroup 13–07G ...... 6 .25 cyclopropanecarboxylate in or on food Bushberry subgroup 13–07B ...... 0 .15 commodities at 3.0 ppm resulting from Cactus ...... 0 .07 use of the insecticide in food handling Caneberry subgroup 13–07A ...... 0.15 Corn, field, forage ...... 0 .30 and storage areas as a space concentra- Corn, field, grain ...... 0 .05 tion for spot/or crack and crevice treat- Corn, field, stover ...... 0 .10 ment and shall be limited to a max- Corn, sweet, forage ...... 0 .30 imum of 3.00 percent of the active in- Corn, sweet, kernel plus cob with husks removed ...... 0 .05 gredient by weight, and as a space Corn, sweet, stover ...... 0 .10 treatment shall be limited to a max- Fruit, citrus, group 10–10 ...... 0 .26 imum of 0.5 fluid ounce of 3.0 percent Ginseng ...... 0 .05 Grass, forage ...... 2 .0 active ingredient by weight per 1000 Grass, hay ...... 2 .0 cubic feet of space provided that the Leaf petioles subgroup 4B ...... 0 .50 food is removed or covered prior to Lettuce ...... 1.73 such use. To assure safe use of the ad- Pea and bean, succulent shelled, subgroup 6B 0 .20 Peppermint, oil ...... 12 ditive, its label and labeling shall con- Peppermint, tops ...... 4 .0 form to that registered with the U.S. Spearmint, oil ...... 12 Environmental Protection Agency, and Spearmint, tops ...... 4 .0 shall be used in accordance with such Taro, corm ...... 0 .15 Taro, leaves ...... 1 .0 label and labeling. Tomato subgroup 8–10A ...... 0 .24 (b) Section 18 emergency exemptions. Vegetable, brassica, leafy, group 5 ...... 2.5 [Reserved] Vegetable, foliage of legume, except soybean, subgroup 7A ...... 1 .5 (c) Tolerances with regional registra- Vegetable, legume, edible podded subgroup 6A 0 .80 tions. [Reserved] Watercress ...... 3 .2 (d) Indirect or inadvertent residues. [Reserved] (b) Section 18 emergency exemptions. [Reserved] [71 FR 74819, Dec. 13, 2006] (c) Tolerances with regional registrations. Tolerances with a regional reg- § 180.526 Synthetic isoparaffinic petro- istration as defined in § 180.1(l) are es- leum hydrocarbons; tolerances for tablished for residues of the residues. molluscicide metaldehyde, including (a) General. Synthetic isoparaffinic its metabolites and degradates, in or petroleum hydrocarbons complying on the following commodities. Compli- with 21 CFR 172.882 (a) and (b) may be ance with the specified tolerance level safely used as a component of insecti- is to be determined by measuring only cide formulations for use on animal metaldehyde, 2,4,6,8-tetramethyl- feed in an amount no greater than rea- 1,3,5,7-tetroxocane, in or on the com- sonably required to accomplish its in- modity. tended effect as an adjuvant in the insecticide formulation and shall not be Parts per Commodity million intended to accomplish any effect in animal feed. It is used or intended for Clover, forage ...... 0.60 Clover, hay ...... 0.60 use as a component of insecticide for- Soybean, seed ...... 0.05 mulations used in compliance with regulations issued in 40 CFR part 180 and (d) Indirect or inadvertent residues. in this part. [Reserved] (b) Section 18 emergency exemptions. [73 FR 54963, Sept. 24, 2008, as amended at 78 [Reserved] FR 70869, Nov. 27, 2013; 80 FR 11588, Mar. 4, (c) Tolerances with regional registra- 2015] tions. [Reserved]

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(d) Indirect or inadvertent residues. flufenacet, N-(4-fluorophenyl)-N-(1- [Reserved] methylethyl)-2-[[5-(trifluoromethyl)- 1,3,4-thiadiazol-2-yl]oxy]acetamide and [40 FR 14161, Mar. 28, 1975, as amended at 50 FR 2959, Jan. 23, 1985, and amended at 53 FR its metabolites containing the 4-fluoro- 24668, 24669, June 29, 1988. Redesignated and N-methylethyl benzenamine moiety in amended at 63 FR 34319, June 24, 1998] or on the following raw agricultural commodities when present therein as a § 180.527 Flufenacet, N-(4- result of application of flufenacet to fluorophenyl)-N-(1-methylethyl)-2- the growing crops in paragraph (a) of [[5-(trifluoromethyl)-1, 3, 4- this section. thiadiazol-2-yl] oxy]acetamide and its metabolites containing the 4- Parts per fluoro-N-methylethyl benzenamine Commodity million tolerances for residues. Alfalfa, forage ...... 0.1 (a) General. Tolerances are estab- Alfalfa, hay ...... 0.1 lished for the combined residues of the Alfalfa, seed ...... 0 .1 Clover, forage ...... 0.1 herbicide flufenacet, N-(4- Clover, hay ...... 0.1 fluorophenyl)-N-(1-methylethyl)-2-[[5- Grain, cereal, group 15, except rice ...... 0 .1 (trifluoromethyl)-1, 3, 4-thiadiazol-2-yl] Grain, cereal, forage, fodder, and straw, group 16, except rice ...... 0 .1 oxy]acetamide and its metabolites con- Grass, forage, fodder, and hay, group 17 ...... 0 .1 taining the 4-fluoro-N-methylethyl benzenamine moiety in or on the following commodities. [63 FR 26473, May 13, 1998, as amended at 63 FR 50791, Sept. 23, 1998; 64 FR 42846, Aug. 6, Parts per 1999; 65 FR 64366, Oct. 27, 2000; 68 FR 2247, Commodity million Jan. 16, 2003; 68 FR 37759, June 25, 2003; 70 FR 37696, June 30, 2005; 71 FR 76200, Dec. 20, 2006; Cattle, kidney ...... 0 .05 72 FR 26310, May 9, 2007] Corn, field, forage ...... 0 .4 Corn, field, grain ...... 0 .05 Corn, field, stover ...... 0 .4 § 180.530 2,2-Dimethyl-1,3-benzodioxol- Corn, sweet, forage ...... 0 .45 4-ol methylcarbamate; tolerances Corn, sweet, kernel plus cob with husks re- for residues. moved ...... 0 .05 Corn, sweet, stover ...... 0 .30 (a) General. (1) The insecticide 2,2-di- Goat, kidney ...... 0 .05 methyl-1,3-benzodioxol-4-yl Hog, kidney ...... 0.05 methylcarbamate may be safely used Horse, kidney ...... 0 .05 Sheep, kidney ...... 0.05 in spot and/or crack and crevice treat- Soybean, seed ...... 0 .1 ments in animal feed handling estab- Wheat, bran ...... 0.80 lishments, including feed manufac- Wheat, forage ...... 6 .0 Wheat, grain ...... 0 .60 turing and processing establishments, Wheat, hay ...... 1 .2 such as stores, supermarkets, dairies, Wheat, straw ...... 0 .35 meat slaughtering and packing plants, and canneries until the tolerance expi- (b) Section 18 emergency exemptions. ration/revocation date of April 26, 2005. [Reserved] (2) The insecticide 2,2-dimethyl-1,3- (c) Tolerances with regional registra- benzodioxol-4-yl methylcarbamate may tions. Tolerances are established for be safely used in spot and/or crack and combined residues of flufenacet, N-(4- crevice treatments in food handling es- fluorophenyl)-N-(1-methylethyl)-2-[[5- tablishments, including food service, (trifluoromethyl)-1, 3, 4-thiadiazol-2-yl] manufacturing and processing estab- oxy]acetamide, and its metabolites lishments, such as restaurants, cafe- containing the 4-fluoro-N-methylethyl terias, supermarkets, bakeries, brew- benzenamine moiety, with regional eries, dairies, meat slaughtering and registration. packing plants, and canneries until the Parts per tolerance expiration/revocation date of Commodity million April 26, 2005. Grass, forage ...... 7 .0 (3) To ensure safe use of the additive, Grass, hay ...... 0 .4 its label and labeling shall conform to that registered with the U.S. Environ- (d) Indirect or inadvertent residues. mental Protection Agency and it shall Tolerances are established for indirect be used in accordance with such label or inadvertent residues of the herbicide and labeling.

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(b) Section 18 emergency exemptions. Commodity Parts per [Reserved] million (c) Tolerances with regional registra- Parsley, dried leaves ...... 170 tions. [Reserved] Parsley, leaves ...... 35 (d) Indirect or inadvertent residues. Passionfruit ...... 1 .5 Pistachio ...... 0.10 [Reserved] Pomegranate ...... 10 Pulasan ...... 2 .0 [63 FR 34828, June 26, 1998, as amended at 69 Rambutan ...... 2 .0 FR 58083, Sept. 29, 2004] Sapodilla ...... 1 .2 Sapote, black ...... 1 .2 EFFECTIVE DATE NOTE: At 81 FR 34906, June Sapote, mamey ...... 1 .2 1, 2016, § 180.530 was removed, effective Nov. Spanish lime ...... 2 .0 28, 2016. Star apple ...... 1 .2 Starfruit ...... 1 .5 § 180.532 Cyprodinil; tolerances for Turnip, greens ...... 10.0 residues. Vegetable, cucurbit, group 9 ...... 0.70 Vegetable, fruiting, group 8–10 ...... 1 .5 (a) General. (1) Tolerances are estab- Vegetable, leaves of root and tuber, group 2 ..... 10 lished for residues of the fungicide Vegetable, root, except sugarbeet, subgroup 1B 0 .75 Watercress ...... 20 cyprodinil, including its metabolites Wax jambu ...... 1 .5 and degradates, in or on the commod- 1 Import only. ities in the table below. Compliance with the tolerance levels specified (2) Tolerances are established for res- below is to be determined by measuring idues of the fungicide cyprodinil, in- only cyprodinil 4-cyclopropyl-6-meth- cluding its metabolites and degradates, yl-N-phenyl-2-pyrimidinamine. in the commodities in the table below. Compliance with the tolerance levels Commodity Parts per specified below is to be determined by million measuring only the sum of cyprodinil Acerola ...... 1.5 4-cyclopropyl-6-methyl-N-phenyl-2- Almond ...... 0.02 pyrimidinamine and free and con- Almond, hulls ...... 8 .0 jugated CGA–304075 4-(4-cyclopropyl-6- Apple, wet pomace ...... 4 .6 Artichoke, globe ...... 4.0 methyl-pyrimidin-2-ylamino)-phenol, Avocado ...... 1 .2 calculated as the stoichiometric equiv- Bean, dry ...... 0.6 alent of cyprodinil. Bean, succulent ...... 0 .6 Berry, low growing, subgroup 13–07G, except Parts per cranberry ...... 5.0 Commodity million Brassica, head and stem, subgroup 5A ...... 1 .0 Brassica, leafy greens, subgroup 5B ...... 10 .0 Cattle, meat byproducts ...... 0.02 Bushberry subgroup 13–07B ...... 3 .0 Goat, meat byproducts ...... 0 .02 Caneberry subgroup 13–07A ...... 10 Horse, meat byproducts ...... 0 .02 Canistel ...... 1 .2 Sheep, meat byproducts ...... 0 .02 Canola, seed 1 ...... 0 .03 Citrus, dried pulp ...... 8 .0 (b) Section 18 emergency exemptions. Citrus, oil ...... 60 Dragon fruit ...... 2 .0 [Reserved] Feijoa ...... 1 .5 (c) Tolerances with regional registra- Fruit, pome, group 11–10 ...... 1 .7 tions. [Reserved] Fruit, small vine climbing, except fuzzy kiwifruit, (d) Indirect or inadvertent residues. subgroup 13–07F ...... 3 .0 Fruit, stone, group 12–12 ...... 2 .0 [Reserved] Grape, raisin ...... 5 .0 [63 FR 17706, Apr. 10, 1998] Guava ...... 1 .5 Herb subgroup 19A, dried, except parsley ...... 15 .0 EDITORIAL NOTE: For FEDERAL REGISTER ci- Herb subgroup 19A, fresh, except parsley ...... 3 .0 tations affecting § 180.532, see the List of CFR Jaboticaba ...... 1 .5 Sections Affected, which appears in the Kiwifruit ...... 1.8 Leaf petioles subgroup 4B ...... 30 Finding Aids section of the printed volume Leafy greens subgroup 4A ...... 50 and at www.fdsys.gov. Lemon ...... 0.60 Lime ...... 0.60 § 180.533 Esfenvalerate; tolerances for Longan ...... 2 .0 residues. Lychee ...... 2 .0 Mango ...... 1.2 (a) General. (1) Tolerances are estab- Nut, tree, group 14–12; except almond and pis- lished for the combined residues of the tachio ...... 0 .04 insecticide esfenvalerate, (S)-cyano(3- Onion, bulb, subgroup 3–07A ...... 0 .6 Onion, green, subgroup 3–07B ...... 4 .0 phenoxyphenyl)methyl-(S)-4-chloro-a- Papaya ...... 1 .2 (1-methylethyl)benzeneacetate, its

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non-racemic isomer, (R)-cyano(3- Commodity Parts per phenoxyphenyl)methyl-(R)-4-chloro-a- million (1-methylethyl)benzeneacetate and its Poultry, fat ...... 0.3 diastereomers (S)-cyano(3- Poultry, liver ...... 0 .03 phenoxyphenyl)methyl-(R)-4-chloro-a- Poultry, meat ...... 0 .03 Poultry, meat byproducts, except liver ...... 0 .3 (1-methylethyl)benzeneacetate and (R)- Pumpkin ...... 0.5 cyano(3-phenoxyphenyl)methyl-(S)-4- Radish, roots ...... 0 .3 chloro-a-(1- Radish, tops ...... 3 .0 Sheep, fat ...... 1 .5 methylethyl)benzeneacetate, in or on Sheep, meat ...... 1.5 food commodities as follows: Sheep, meat byproducts ...... 1 .5 Sorghum, grain, forage ...... 10.0 Parts per Sorghum, grain, grain ...... 5 .0 Commodity million Sorghum, grain, stover ...... 10 .0 Soybean, hulls ...... 0 .5 Almond ...... 0.2 Soybean, seed ...... 0 .05 Almond, hulls ...... 5 .0 Squash, summer ...... 0 .5 Apple ...... 1.0 Squash, winter ...... 0 .5 Artichoke, globe ...... 1.0 Sugarcane, cane ...... 1.0 Bean, dry, seed ...... 0 .25 Sunflower, seed ...... 0.5 Bean, snap, succulent ...... 1 .0 Sweet potato, roots ...... 0 .05 Beet, sugar, roots ...... 0 .05 Tomato ...... 0.5 Beet, sugar, tops ...... 5.0 Turnip, greens ...... 7.0 Blueberry ...... 1 .0 Turnip, roots ...... 0 .5 Broccoli ...... 1 .0 Walnut ...... 0 .2 Cabbage, except Chinese cabbage ...... 3.0 Watermelon ...... 0.5 Caneberry subgroup 13A ...... 1 .0 Cantaloupe ...... 0 .5 (2) A tolerance of 0.05 ppm on raw ag- Carrot, roots ...... 0.5 Cattle, fat ...... 1.5 ricultural food commodities (other Cattle, meat ...... 1 .5 than those food commodities already Cattle, meat byproducts ...... 1.5 covered by a higher tolerance as a re- Cauliflower ...... 0 .5 sult of use on growing crops) is estab- Collards ...... 3.0 Corn, field, forage ...... 15 .0 lished for the combined residues of the Corn, field, grain ...... 0 .02 insecticide esfenvalerate, (S)-cyano(3- Corn, field, stover ...... 15 .0 phenoxyphenyl)methyl-(S)-4-chloro-a- Corn, pop, grain ...... 0.02 Corn, pop, stover ...... 15.0 (1-methylethyl)benzeneacetate, its Corn, sweet, forage ...... 15 .0 non-racemic isomer, (R)-cyano(3- Corn, sweet, kernel plus cob with husks re- phenoxyphenyl)methyl-(R)-4-chloro-a- moved ...... 0 .1 (1-methylethyl)benzeneacetate and its Corn, sweet, stover ...... 15.0 Cotton, undelinted seed ...... 0 .2 diastereomers (S)-cyano(3- Cucumber ...... 0 .5 phenoxyphenyl)methyl-(R)-4-chloro-a- Egg ...... 0 .03 (1-methylethyl)benzeneacetate and (R)- Eggplant ...... 0.5 Elderberry ...... 1 .0 cyano(3-phenoxyphenyl)methyl-(S)-4- Fruit, stone, group 12 ...... 3 .0 chloro-a-(1- Goat, fat ...... 1 .5 methylethyl)benzeneacetate as a result Goat, meat ...... 1.5 Goat, meat byproducts ...... 1 .5 of the use of esfenvalerate in food-han- Gooseberry ...... 1 .0 dling establishments. Hazelnut ...... 0 .2 (b) Section 18 emergency exemptions. Hog, fat ...... 1 .5 [Reserved] Hog, meat ...... 1 .5 Hog, meat byproducts ...... 1 .5 (c) Tolerances with regional registra- Horse, fat ...... 1 .5 tions. Tolerances with regional reg- Horse, meat ...... 1 .5 istration are established for the com- Horse, meat byproducts ...... 1 .5 Kiwifruit ...... 0.5 bined residues of the insecticide Lentil, seed ...... 0 .25 esfenvalerate, (S)-cyano(3- Melon, honeydew ...... 0.5 phenoxyphenyl)methyl-(S)-4-chloro-a- Milk ...... 0.3 Milk, fat ...... 7 .0 (1-methylethyl)benzeneacetate, its Muskmelon ...... 0 .5 non-racemic isomer, (R)-cyano(3- Mustard greens ...... 5.0 phenoxyphenyl)methyl-(R)-4-chloro-a- Okra ...... 0.5 (1-methylethyl)benzeneacetate and its Pea, dry, seed ...... 0 .25 Pea, succulent ...... 0 .5 diastereomers (S)-cyano(3- Peanut ...... 0 .02 phenoxyphenyl)methyl-(R)-4-chloro-a- Pear ...... 1 .0 (1-methylethyl)benzeneacetate and (R)- Pecan ...... 0 .2 Pepper ...... 0 .5 cyano(3-phenoxyphenyl)methyl-(S)-4- Potato ...... 0 .02 chloro-a-(1- 631

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methylethyl)benzeneacetate, in or on Commodity Parts per food commodities as follows: million Horse, fat ...... 0 .1 Parts per Commodity million Horse, kidney ...... 1 .5 Horse, meat ...... 0 .1 Cabbage, chinese, bok choy ...... 1 .0 Horse, meat byproducts ...... 0 .1 Kohlrabi ...... 2 .0 Milk ...... 0.3 Lettuce, head ...... 5.0 Millet, forage ...... 12.0 Millet, grain ...... 0 .5 (d) Indirect or inadvertent residues. Millet, hay ...... 20.0 Millet, proso, straw ...... 12 .0 [Reserved] Oat, forage ...... 12 .0 Oat, grain ...... 0 .5 [63 FR 23401, Apr. 29, 1998, as amended at 63 Oat, hay ...... 20.0 FR 48615, Sept. 11, 1998; 74 FR 46699, Sept. 11, Oat, straw ...... 12.0 2009] Onion, bulb ...... 0 .03 Rice, bran ...... 3.0 § 180.535 Fluroxypyr 1-methylheptyl Rice, grain ...... 1 .5 ester; tolerances for residues. Shallot, bulb ...... 0 .03 Sheep, fat ...... 0 .1 (a) General. Tolerances are estab- Sheep, kidney ...... 1.5 lished for combined residues of Sheep, meat ...... 0.1 fluroxypyr 1-methylheptyl ester [1- Sheep, meat byproducts ...... 0 .1 Sorghum, grain, forage ...... 2.0 methylheptyl ((4-amino-3,5-dichloro-6- Sorghum, grain, grain ...... 0 .02 fluoro-2-pyridinyl)oxy)acetate] and its Sorghum, grain, stover ...... 4 .0 metabolite fluroxypyr [((4-amino-3,5- Wheat, forage ...... 12.0 Wheat, grain ...... 0 .5 dichloro-6-fluoro-2-pyridinyl)oxy)acetic Wheat, hay ...... 20 .0 acid] in or on the following raw agri- Wheat, straw ...... 12 .0 cultural commodities. Compliance with the established tolerance levels is de- (b) Section 18 emergency exemptions. termined by measuring only the sum of [Reserved] fluroxypyr 1-methylheptyl ester [1- (c) Tolerances with regional registra- methylheptyl ((4-amino-3, 5-dichloro-6- tions. [Reserved] fluoro-2-pyridinyl)oxy)acetate] and its (d) Indirect or inadvertent residues. metabolite fluroxypyr [((4-amino-3,5- [Reserved] dichloro-6-fluoro-2-pyridinyl)oxy)acetic [63 FR 52169, Sept. 30, 1998, as amended at 64 acid] calculated as the stoichiometric FR 22799, Apr. 28, 1999; 66 FR 37598, July 19, equivalent of fluroxypyr. 2001; 66 FR 47971, Sept. 17, 2001; 67 FR 46884, July 17, 2002; 67 FR 60146, Sept. 25, 2002; 68 FR Parts per Commodity million 75438, Dec. 31, 2003; 69 FR 2074, Jan. 14, 2004; 70 FR 3649, Jan. 26, 2005; 70 FR 7047, Feb. 10, Barley, grain ...... 0 .5 2005; 71 FR 76204, Dec. 20, 2006; 72 FR 73635, Barley, hay ...... 12 .0 Dec. 28, 2007; 78 FR 3333, Jan. 16, 2013] Barley, hay ...... 20 .0 Barley, straw ...... 12 .0 Cattle, fat ...... 0.1 § 180.537 Isoxaflutole; tolerances for Cattle, kidney ...... 1 .5 residues. Cattle, meat ...... 0 .1 (a) General. Tolerances are estab- Cattle, meat byproducts ...... 0.1 Corn, field, forage ...... 1 .0 lished for residues of the herbicide, Corn, field, grain ...... 0 .02 isoxaflutole, including its metabolites Corn, field, stover ...... 0 .5 and degradates, in or on the commod- Corn, sweet, forage ...... 1 .0 Corn, sweet, kernel plus cob with husks re- ities in the table below. Compliance moved ...... 0 .02 with the tolerance levels specified Corn, sweet, stover ...... 2 .0 below is to be determined by measuring Fruit, pome, group 11 ...... 0.02 only the sum of isoxaflutole ((5- Garlic, bulb ...... 0.03 Goat, fat ...... 0 .1 cyclopropyl-4-isoxazolyl) [2- Goat, kidney ...... 1 .5 (methylsulfonyl)-4- Goat, meat ...... 0.1 (trifluoromethyl)phenyl] methanone) Goat, meat byproducts ...... 0 .1 Grain, aspirated fractions ...... 0 .6 and its metabolite 1-(2-methylsulfonyl- Grass, forage ...... 120 4-trifluoromethylphenyl)-2-cyano-3- Grass, hay ...... 160 cyclopropyl propan-1,3-dione (RPA Hog, fat ...... 0 .1 202248), calculated as the stoichio- Hog, kidney ...... 1.5 Hog, meat ...... 0 .1 metric equivalent of isoxaflutole, in or Hog, meat byproducts ...... 0 .1 on the commodity:

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(d) Indirect or inadvertent residues. Commodity Parts per million [Reserved] Corn, field, forage ...... 0 .04 [73 FR 54963, Sept. 24, 2008] Corn, field, grain ...... 0 .02 Corn, field, stover ...... 0 .02 Grain, aspirated fractions ...... 0 .30 § 180.543 Diclosulam; tolerances for Soybean, seed ...... 0 .05 residues. (a) General. Tolerances are estab- (b) Section 18 emergency exemptions. lished for residues of the herbicide [Reserved] diclosulam [N-(2,6-dichlorophenyl)-5- (c) Tolerances with regional registra- ethoxy-7-fluoro[1,2,4] triazolo[1,5- tions. [Reserved] c]pyrimidine-2-sulfonamide] in or on (d) Indirect or inadvertent residues. the following raw agricultural com- [Reserved] modities as follows:

[63 FR 50784, Sept. 23, 1998, as amended at 73 Parts per FR 75608, Dec. 12, 2008; 76 FR 76314, Dec. 7, Commodity million 2011] Peanut ...... 0 .020 § 180.539 d-Limonene; tolerances for Soybean, seed ...... 0 .020 residues. (b) Section 18 emergency exemptions. (a) General. (1) The insecticide d-lim- [Reserved] onene may be safely used in insect-re- (c) Tolerances with regional registra- pellent tablecloths and in insect-repel- tions. [Reserved] lent strips used in food- or feed-han- (d) Indirect or inadvertent residues. dling establishments. [Reserved] (2) To assure safe use of the insect repellent, its label and labeling shall con- [65 FR 12134, Mar. 8, 2000] form to that registered by the U.S. En- § 180.544 Methoxyfenozide; tolerances vironmental Protection Agency, and it for residues. shall be used in accordance with such label and labeling. (a) General. (1) Tolerances are estab- (b) Section 18 emergency exemptions. lished for residues of the insecticide [Reserved] methoxyfenozide, including its metabo- (c) Tolerances with regional registra- lites and degradates, in or on the com- tions. [Reserved] modities listed in the following table. (d) Indirect or inadvertent residues. Compliance with the tolerance levels [Reserved] specified in the following table is to be determined by measuring only [65 FR 33715, May 24, 2000, as amended at 70 methoxyfenozide (3-methoxy-2- FR 55268, Sept. 21, 2005] methylbenzoic acid 2-(3,5- dimethylbenzoyl)-2-(1,1-dimethylethyl) § 180.540 Fenitrothion; tolerances for residues. hydrazide) in or on the commodity.

(a) General. Tolerances are estab- Commodity Parts per lished for residues of the insecticide million fenitrothion, O,O-dimethyl O-(4-nitro- Acerola ...... 0.4 m-tolyl) phosphorothioate, from the Almond, hulls ...... 25 postharvest application of the insecti- Animal feed, nongrass, group 18, forage ...... 50 .0 Animal feed, nongrass, group 18, hay ...... 150.0 cide to stored wheat in Australia, in or Apple, wet pomace ...... 7 .0 on the following food commodity: Artichoke, globe ...... 3.0 Atemoya ...... 0 .60 Avocado ...... 0 .6 Commodity Parts per million Beet, sugar, roots ...... 0 .50 Berry, low growing, subgroup 13–07G, except Wheat, gluten 1 ...... 3.0 cranberry ...... 2.0 Biriba ...... 0 .60 1 There are no U.S. registrations on food commodities since 1987. Brassica, head and stem, subgroup 5A ...... 7 .0 Brassica, leafy greens, subgroup 5B ...... 30 (b) Section 18 emergency exemptions. Bushberry subgroup 13-07B ...... 3 .0 [Reserved] Caneberry subgroup 13–07A ...... 6.0 Canistel ...... 0 .6 (c) Tolerances with regional registra- Cattle, fat ...... 0.50 tions. [Reserved] Cattle, meat ...... 0 .02

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Parts per Parts per Commodity million Commodity million

Cherimoya ...... 0 .60 Sorghum, grain, forage ...... 15 Chive, fresh leaves ...... 30 Sorghum, grain, grain ...... 6 .0 Citrus, oil ...... 100 Sorghum, grain, stover ...... 20 Corn, field, forage ...... 15 Sorghum, sweet, forage ...... 15 Corn, field, grain ...... 0 .05 Sorghum, sweet, grain ...... 6 .0 Corn, field, refined oil ...... 0 .20 Sorghum, sweet, stalk ...... 15 Corn, field, stover ...... 125 Sorghum, sweet, stover ...... 20 Corn, pop, grain ...... 0.05 Soursop ...... 0 .60 Corn, pop, stover ...... 125 Soybean, aspirated grain fractions ...... 160 Corn, sweet, forage ...... 30 Soybean, forage ...... 30 Corn, sweet, kernel plus cob with husks re- Soybean, hay ...... 80 moved ...... 0 .05 Soybean, hulls ...... 2 .0 Corn, sweet, stover ...... 60 Soybean, seed ...... 1 .0 Cotton, gin byproducts ...... 35 Spanish lime ...... 2 .0 Cotton, undelinted seed ...... 2 .0 Spearmint, tops ...... 7 .0 Cranberry ...... 0 .5 Star apple ...... 0 .6 Custard apple ...... 0 .60 Starfruit ...... 0 .4 Date ...... 8 .0 Sugar apple ...... 0 .60 Feijoa ...... 0 .4 Turnip, greens ...... 30 Fruit, citrus, group 10–10 ...... 3 .0 Vegetable, cucurbit, group 9 ...... 0.3 Fruit, pome, group 11–10 ...... 2 .0 Vegetable, foliage of legume, except soybean, Fruit, small, vine climbing, except fuzzy subgroup 7A ...... 35 kiwifruit, subgroup 13–07F ...... 1 .0 Vegetable, fruiting, group 8–10 ...... 2 .0 Fruit, stone, group 12–12, except plum, prune, Vegetable, leaves of root and tuber, group 2 ... 30 fresh ...... 3 .0 Vegetable, legume, edible podded, subgroup Goat, fat ...... 0 .50 6A ...... 1 .5 Goat, meat ...... 0.02 Vegetable, root, except sugar beet, Subgroup Grain, aspirated grain fractions ...... 120 1B ...... 0 .90 Grape, raisin ...... 1 .5 Vegetable, tuberous and corm, except potato, Grass, forage, fodder and hay, group 17, for- subgroup 1D ...... 0 .02 age ...... 18 .0 Wax jambu ...... 0 .4 Grass, forage, fodder and hay, group 17, hay .. 30 .0 Guava ...... 0 .4 Herb subgroup 19A, except chive, fresh leaves 400 (2) Tolerances are established for res- Hog, fat ...... 0 .1 idues of the insecticide Hog, meat ...... 0 .02 methoxyfenozide, including its metabo- Horse, fat ...... 0 .50 lites and degradates, in or on the com- Horse, meat ...... 0 .02 Ilama ...... 0 .60 modities in the following table. Com- Jaboticaba ...... 0 .4 pliance with the tolerance levels speci- Leaf petioles subgroup 4B ...... 25 fied in the following table is to be de- Leafy greens subgroup 4A ...... 30 Longan ...... 2 .0 termined by measuring only the sum of Lychee ...... 2 .0 methoxyfenozide [3-methoxy-2- Mango ...... 0.6 methylbenzoic acid 2-(3,5- Milk ...... 0.10 dimethylbenzoyl)-2-(1,1-dimethylethyl) Nut, tree, group 14–12 ...... 0 .10 Onion, green, subgroup 3–07B, except chive, hydrazide] and its glucuronide metabo- fresh leaves ...... 5 .0 lite (b-D-Glucopyranuronic acid, 3-[[2- Papaya ...... 0 .6 (1,1-dimethylethyl)-2-(3,5- Passionfruit ...... 0 .4 Pea and bean, dried shelled, except soybean, dimethylbenzoyl)-hydrazino]carbonyl]- subgroup 6C, except pea, blackeyed, seed 2-methylphenyl-), calculated as the and pea, southern, seed ...... 0.50 stoichiometric equivalent of Pea and bean, succulent shelled, subgroup 6B 0 .2 methoxyfenozide. Pea, blackeyed, seed ...... 4 .0 Pea, southern, seed ...... 4.0 Peanut ...... 0 .02 Parts per Commodity million Peanut, hay ...... 55.0 Peanut, oil ...... 0 .04 Cattle, liver ...... 0 .40 Peppermint, tops ...... 7 .0 Cattle, meat byproducts, except liver ...... 0 .10 Pineapple ...... 0.70 Egg ...... 0 .02 Plum, prune, fresh ...... 0.30 Goat, liver ...... 0.40 Pomegranate ...... 0 .6 Goat, meat byproducts, except liver ...... 0 .10 Poultry, fat ...... 0.02 Hog, liver ...... 0 .1 Poultry, meat ...... 0 .02 Hog, meat byproducts, except liver ...... 0 .02 Pulasan ...... 2 .0 Horse, liver ...... 0 .40 Rambutan ...... 2 .0 Horse, meat byproducts, except liver ...... 0 .10 Sapodilla ...... 0 .6 Poultry, liver ...... 0 .10 Sapote, black ...... 0 .6 Poultry, meat byproducts, except liver ...... 0 .02 Sapote, mamey ...... 0 .6 Sheep, liver ...... 0.40 Sheep, fat ...... 0 .50 Sheep, meat byproducts, except liver ...... 0 .10 Sheep, meat ...... 0.02

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(b) Section 18 emergency exemptions. dimethylbenzoyl)-2-(1,1-dimethylethyl) Time-limited tolerances are estab- hydrazide] and the following metabo- lished for residues of the insecticide lites (all calculated as the stoichio- methoxyfenozide, including its metabo- metric equivalent of methoxyfenozide): lites and degradates in or on the com- free phenol of methoxyfenozide [3,5- modities listed in the table below, re- dimethylbenzoic acid N-tert-butyl-N′- sulting from use of the pesticide under (3-hydroxy-2-methylbenzoyl) hydra- a Section 18 emergency exemption zide], the glucose conjugate of the phe- granted by EPA. Compliance with the nol [3,5-dimethyl benzoic acid N-tert- tolerance levels specified in the fol- butyl-N′-[3 (b-D-glucopyranosyloxy)-2- lowing table is to be determined by methylbenzoyl]-hydrazide] and the measuring only methoxyfenozide (3- malonylglycosyl conjugate of the phe- methoxy-2-methylbenzoic acid 2-(3,5- nol [3,5-dimethyl benzoic acid N-tert- dimethylbenzoyl)-2-(1,1-dimethylethyl) butyl-N′-[3 (b-D-6-malonyl- hydrazide) in or on the commodity. glucopyranosyl-1-oxy)-2- methylbenzoyl]-hydrazide]. Expiration/ Commodity Parts per revocation million date Parts per Commodity million Rice, bran ...... 4.0 12/31/19 Rice, grain ...... 0.50 12/31/19 Animal feed, nongrass, group 18, straw ...... 8.0 Grain, cereal, forage, fodder and straw group 16, except corn ...... 6 .0 (c) Tolerances with regional registra- Rapeseed subgroup 20A ...... 1 .0 tions. [Reserved] Spice subgroup 19B ...... 4 .5 (d) Indirect or inadvertent tolerances. Sunflower subgroup 20B ...... 1.0 (1) Tolerances are established for the indirect or inadvertent residues of the [67 FR 59203, Sept. 20, 2002, as amended at 68 insecticide methoxyfenozide, including FR 32389, May 30, 2003; 68 FR 37765, June 25, its metabolites and degradates, in or 2003; 69 FR 58097, Sept. 29, 2004; 70 FR 7047, on the raw agricultural commodities in Feb. 10, 2005; 70 FR 51604, Aug. 31, 2005; 70 FR the following table, when present 75739, Dec. 21, 2005; 71 FR 32853, June 7, 2006; therein as a result of the application of 73 FR 11826, Mar. 5, 2008; 74 FR 22468, May 13, methoxyfenozide to growing crops as 2009; 74 FR 45335, Sept. 2, 2009; 76 FR 34886, listed in paragraph (a) of this section. June 15, 2011; 77 FR 40812, July 11, 2012; 78 FR 60714, Oct. 2, 2013; 79 FR 51106, Aug. 27, 2014; Compliance with the tolerance levels 80 FR 65968, Oct. 28, 2015; 81 FR 27336, May 6, specified in the following table is to be 2016] determined by measuring only methoxyfenozide [3-methoxy-2- § 180.545 Prallethrin; tolerances for methylbenzoic acid 2-(3,5- residues. dimethylbenzoyl)-2-(1,1-dimethylethyl) (a) General. Tolerances are estab- hydrazide]. lished for residues of the insecticide Parts per prallethrin, including its metabolites Commodity million and degradates, in or on all raw agricultural commodities and processed Onion, bulb, subgroup 3–07A ...... 0 .10 Potato ...... 0 .02 food from use of prallethrin in food handling establishments where food (2) Tolerances are established for the and food products are held, processed, indirect or inadvertent residues of the prepared and/or served, or as a wide- insecticide methoxyfenozide, including area mosquito adulticide at 1.0 part per its metabolites and degradates, in or million (ppm). Compliance with the on the raw agricultural commodities in tolerance level specified is to be deter- the following table, when present mined by measuring only prallethrin, therein as a result of the application of 2-methyl-4-oxo-3-(2-propyn-1-yl)-2- methoxyfenozide to growing crops as cyclopenten-1-yl-2,2-dimethyl-3-(2- listed in paragraph (a) of this section. methyl-1-propen-1- Compliance with the tolerance levels yl)cyclopropanecarboxylate. specified in the following table is to be (b) Section 18 emergency exemptions. determined by measuring only the sum [Reserved] of methoxyfenozide [3-methoxy-2- (c) Tolerances with regional registra- methylbenzoic acid, 2-(3,5- tions. [Reserved]

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(d) Indirect or inadvertent residues. propionylcyclohex-3-enecarboxylate)’’ [Reserved] in or on the following commodities.

[79 FR 64330, Oct. 29, 2014] Parts per Commodity million § 180.546 Mefenoxam; tolerances for Cattle, kidney ...... 0 .10 residues. Cattle, meat byproducts, except kidney ...... 0.05 (a) General. Tolerances are estab- Cherry, sweet ...... 0 .40 lished for residues of mefenoxam, in- Fruit, pome, group 11 ...... 3.0 Goat, kidney ...... 0 .10 cluding its metabolites and degradates, Goat, meat byproducts, except kidney ...... 0 .05 in or on the commodities in the table Grass, forage 1 ...... 0 .10 below. Compliance with the tolerance Grass, hay 1 ...... 0 .10 Grass, seed screenings 1 ...... 3 .5 levels specified below is to be deter- Grass, straw 1 ...... 1 .2 mined by measuring only metalaxyl Hog, kidney ...... 0.10 (methyl N-(2,6-dimethylphenyl)-N- Hog, meat byproducts, except kidney ...... 0 .05 (methoxyacetyl)-DL-alaninate). Horse, kidney ...... 0 .10 Horse, meat byproducts, except kidney ...... 0 .05 Peanut ...... 1 .0 Parts per Peanut, hay ...... 0.60 Commodity million Sheep, kidney ...... 0.10 Artichoke, globe ...... 0.05 Sheep, meat byproducts, except kidney ...... 0 .05 Atemoya ...... 0 .20 Strawberry ...... 0 .30 Watercress ...... 4 .0 Bean, snap, succulent ...... 0 .20 Bushberry subgroup 13–07B ...... 2 .0 1Registration is limited to grass grown for seed. Caneberry subgroup 13–07A ...... 0.70 Canistel ...... 0 .40 (b) Section 18 emergency exemptions. Custard apple ...... 0 .20 [Reserved] Herbs, dried ...... 55 (c) Tolerances with regional registra- Herbs, fresh ...... 8 .0 Kiwifruit ...... 0.10 tions. [Reserved] Mango ...... 0.40 (d) Indirect or inadvertent residues. Onion, bulb, subgroup 3–07A ...... 3 .0 [Reserved] Onion, green, subgroup 3–07B ...... 10 Papaya ...... 0 .40 [65 FR 25660, May 3, 2000, as amended at 66 Rapeseed subgroup 20A ...... 0 .05 FR 29712, June 1, 2001; 76 FR 71464, Nov. 18, Sapodilla ...... 0 .40 2011; 80 FR 38980, July 8, 2015] Sapote, black ...... 0 .40 Sapote, mamey ...... 0 .40 Spinach ...... 10 § 180.548 Tralkoxydim; tolerances for Star apple ...... 0 .40 residues. Starfruit ...... 0 .20 (a) General. Tolerances are estab- Sugar apple ...... 0 .20 lished for residues of the herbicide, (b) Section 18 emergency exemptions. tralkoxydim, 2-Cyclohexen-1-one, 2-[1- [Reserved] (ethoxyimino)propyl]-3-hydroxy-5- (c) Tolerances with regional registra- (2,4,6-trimethylphenyl)-(9Cl) in or on tions. [Reserved] the raw agricultural commodities: (d) Indirect or inadvertant residues. Parts per [Reserved] Commodity million [65 FR 57556, Sept. 25, 2000, as amended at 66 Barley, grain ...... 0 .02 FR 48003, Sept. 17, 2001; 67 FR 35050, May 17, Barley, hay ...... 0 .02 2002; 76 FR 4548, Jan. 26, 2011; 81 FR 26727, Barley, straw ...... 0 .05 Wheat, forage ...... 0 .05 May 4, 2016] Wheat, grain ...... 0 .02 Wheat, hay ...... 0 .02 § 180.547 Prohexadione calcium; toler- Wheat, straw ...... 0 .05 ances for residues. (a) General. Tolerances are estab- (b) Section 18 emergency exemptions. lished for residues of the growth regu- [Reserved] lator, prohexadione calcium, including (c) Tolerances with regional registra- its metabolites and degradates, in or tions. [Reserved] on the commodities in the table below. (d) Indirect or inadvertent residues. Compliance with the tolerance levels [Reserved] specified below is to be determined by [63 FR 69199, Dec. 16, 1998, as amended at 68 measuring only prohexadione calcium FR 48302, Aug. 13, 2003; 70 FR 70739, Nov. 23, (calcium 3-oxido-5-oxo-4- 2005]

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EFFECTIVE DATE NOTE: At 81 FR 34906, June (2) A tolerance is established for the 1, 2016, § 180.548 was removed, effective Nov. combined residues of the herbicide 28, 2016. fluthiacet-methyland its acid metabolite: acetic acid, [[2-chloro-4-fluoro-5- § 180.549 Diflufenzopyr; tolerances for residues. [tetrahydro-3-oxo-1H,3H- [1,3,4]thiadiazolo[3,4-a]pyridazin-1- (a) General. Tolerances are estab- ylidene)amino]phenyl]thio]-methyl lished for combined residues of ester, and its acid metabolite, acetic diflufenzopyr, 2-(1-[([3,5- acid, [[2-chloro-4-fluoro-5-[(tetrahydro- difluorophenylamino] car- 3-oxo-1H,3H-[1,3,4]thiadiazolo[3,4- bonyl)hydrazono]ethyl)-3- a]pyridazin-1- pyridinecarboxylic acid, and its me- ylidene)amino]phenyl]thio]- , in or on tabolites convertible to 8- the following food commodities: methylpyrido[2,3-d]pyridazin-5(6H)-one, expressed as diflufenzopyr, in or on the Commodity Parts per following raw agricultural commod- million ities: Cotton, gin byproducts ...... 0 .20 Cotton, undelinted seed ...... 0 .020 Commodity Parts per million (b) Section 18 emergency exemptions. Corn, field, forage ...... 0 .05 [Reserved] Corn, field, grain ...... 0 .05 (c) Tolerances with regional registra- Corn, field, stover ...... 0 .05 Corn, pop, grain ...... 0.05 tions. [Reserved] Corn, pop, stover ...... 0.05 (d) Indirect or inadvertent residues. Corn, sweet, forage ...... 0 .05 [Reserved] Corn, sweet, kernel plus cob with husks removed ...... 0 .05 [64 FR 18357, Apr. 14, 1999, as amended at 66 Corn, sweet, stover ...... 0 .05 FR 65850, Dec. 21, 2001; 71 FR 77625, Dec. 27, Grass, forage ...... 22 .0 Grass, hay ...... 7 .0 2006]

(b) Section 18 emergency exemptions. § 180.552 Sulfosulfuron; tolerances for residues. [Reserved] (c) Tolerances with regional registra- (a) General. Tolerances are estab- tions. [Reserved] lished for residues of the herbicide (d) Indirect or inadvertent residues. sulfosulfuron, 1–(4,6- [Reserved] dimethoxypyrimidin-2-yl)-3-[(2- ethanesulfonyl-imidazo[1,2-a]pyridine- [64 FR 4308, Jan. 28, 1999, as amended at 67 3-yl) sulfonyl]urea and its metabolites FR 55338, Aug. 29, 2002; 76 FR 34886, June 15, 2011] converted to 2-(ethylsulfonyl)- imidazo[1,2-a]pyridine and calculated § 180.551 Fluthiacet-methyl; tolerances as sulfosulfuron in or on the raw agri- for residues. cultural commodities.

(a) General. (1) A tolerance is estab- Parts per lished for residues of the herbicide, Commodity million fluthiacet-methyl, acetic acid [[2- Cattle, fat ...... 0.02 chloro-4-fluoro-5-[(tetrahydro-3-oxo- Cattle, meat ...... 0 .01 1H,3H-[1,3,4]thiadiazolo[3,4-a]pyridazin- Cattle, meat byproducts ...... 0.3 1-ylidene)amino]phenyl]thio]-methyl Goat, fat ...... 0 .02 Goat, meat ...... 0.01 ester, in or on the food commodity: Goat, meat byproducts ...... 0 .3 Grass, forage, fodder and hay, group 17, for- Commodity Parts per age ...... 14 million Grass, forage, fodder and hay, group 17, hay .. 25 Hog, fat ...... 0 .005 Corn, field, forage ...... 0 .050 Hog, meat ...... 0 .005 Corn, field, grain ...... 0 .010 Hog, meat byproducts ...... 0 .05 Corn, field, stover ...... 0 .050 Horse, fat ...... 0 .02 Corn, pop, grain ...... 0.010 Horse, meat ...... 0 .01 Corn, pop, stover ...... 0.050 Corn, sweet, forage ...... 0 .050 Horse, meat byproducts ...... 0 .3 Corn, sweet, kernel plus cob with husks re- Milk ...... 0.02 moved ...... 0 .010 Sheep, fat ...... 0 .02 Corn, sweet, stover ...... 0 .050 Sheep, meat ...... 0.01 Soybean, seed ...... 0 .01 Sheep, meat byproducts ...... 0 .3 Wheat, forage ...... 4 .0

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Commodity Parts per § 180.554 Kresoxim-methyl; tolerances million for residues. Wheat, grain ...... 0 .02 (a) General. (1) Tolerances are estab- Wheat, hay ...... 0 .3 lished for the combined residues of the Wheat, straw ...... 0 .1 fungicide kresoxim-methyl (methyl (b) Section 18 emergency exemptions. (E)-2-[2-(2-methylphenoxy)-meth- [Reserved] yl]phenyl-2-(methoxyimido)acetate) (c) Tolerances with regional registra- and its metabolites as follows: (E)-2-[2- tions. [Reserved] (2-methylphenoxy)methyl]-phenyl-2- (d) Indirect or inadvertent residues. (methoxyimido)acetic acid; (E)-2-[2-(2- [Reserved] hydroxymethylphenoxy)methyl]- phenyl-2-(methoxyimido)acetic acid [64 FR 27192, May 19, 1999, as amended at 70 (free and glucose conjugated); and (E)- FR 69464, Nov. 16, 2005; 72 FR 54574, Sept. 26, 2007] 2-[2-(4-hydroxy-2-methylphenoxy)- methyl]phenyl-2-(methoxyimido)acetic § 180.553 Fenhexamid; tolerances for acid (free and glucose conjugated) in or residues. on the following commodities:

(a) General. Tolerances are estab- Parts per lished for the residues of the fungicide Commodity million fenhexamid (N-2,3-dichloro-4- Apple, dry pomace ...... 1.0 hydroxyphenyl)-1-methyl Apple, wet pomace ...... 1 .0 cyclohexanecarboxamide) in or on the Fruit, pome ...... 0.5 following commodities: Grape ...... 1 .0 Grape, raisin ...... 1 .5 Parts per Pecan ...... 0 .15 Commodity million Vegetable, cucurbit, group 9 ...... 0.40 Almond, hulls ...... 2 .0 (2) Tolerances are established in or Almond ...... 0.02 Asparagus ...... 0.02 on the following commodities for the Bushberry subgroup 13B ...... 5 .0 residues of the metabolite (E)-2-[2-(2- Caneberry subgroup 13A ...... 20 .0 methylphenoxy)methyl]-phenyl-2- Cilantro, leaves ...... 30.0 Cucumber ...... 2 .0 (methoxyimido)acetic acid resulting Fruit, stone, group 12, except plum, prune, from the use of the fungicide kresoxim- fresh, postharvest ...... 10.0 methyl: Ginseng ...... 0 .3 Grape ...... 4 .0 Parts per Grape, raisin ...... 6 .0 Commodity million Juneberry ...... 5 .0 Kiwifruit, postharvest ...... 15 .0 Cattle, meat byproducts ...... 0.01 Leafy greens subgroup 4A, except spinach ...... 30 .0 Goat, meat byproducts ...... 0 .01 Lingonberry ...... 5.0 Sheep, meat byproducts ...... 0 .01 Pear ...... 10 Pepper, nonbell ...... 0 .02 Pistachio ...... 0.02 (b) Section 18 emergency exemptions. Plum, prune, dried ...... 2.5 [Reserved] Plum, prune, fresh ...... 1.5 (c) Tolerances with regional registra- Pomegranate ...... 2 .0 Salal ...... 5 .0 tions. [Reserved] Strawberry ...... 3 .0 (d) Indirect or inadvertent residues. Vegetable, fruiting, group 8, except nonbell [Reserved] pepper ...... 2 .0 [64 FR 31136, June 10, 1999, as amended at 71 (b) Section 18 emergency exemptions. FR 50359, Aug. 25, 2006; 74 FR 46377, Sept. 9, [Reserved] 2009] (c) Tolerances with regional registrations. [Reserved] § 180.555 Trifloxystrobin; tolerances (d) Indirect or inadvertent residues. for residues. [Reserved] (a) General. Tolerances are established for residues of trifloxystrobin, [64 FR 28924, May 28, 1999, as amended at 65 including its metabolites and FR 19849, Apr. 13, 2000; 65 FR 69883, Nov. 21, 2000; 67 FR 19120, Apr. 18, 2002; 68 FR 2247, degradates, in or on the commodities Jan. 16, 2003; 68 FR 55519, Sept. 26, 2003; 71 FR in the table below. Compliance with 15617, Mar. 29, 2006; 71 FR 43664, Aug. 2, 2006; the tolerance levels specified below is 73 FR 19154, Apr. 9, 2008] to be determined by measuring only

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the sum of trifloxystrobin, Commodity Parts per benzeneacetic acid, (E,E)-a- million (methoxyimino)-2-[[[[1-[3- Horse, meat byproducts ...... 0 .1 (trifluoromethyl) phenyl]ethylidene] Leaf petioles subgroup 4B ...... 9 .0 amino]oxy]methyl]-, methyl ester, and Leafy greens, subgroup 4A ...... 30 Mango ...... 0.7 the free form of its acid metabolite Milk ...... 0.02 CGA–321113, (E,E)-methoxyimino-[2-[1- Nut, tree, group 14 ...... 0 .04 (3-trifluoromethyl-phenyl)- Oat, forage ...... 0 .3 Oat, grain ...... 0 .05 ethylideneaminooxymethyl]- Oat, hay ...... 0.3 phenyl]acetic acid, calculated as the Oat, straw ...... 5.0 stoichiometric equivalent of Papaya ...... 0 .7 Pea, dry, seed ...... 0 .06 trifloxystrobin, in or on the com- Pea, field, hay ...... 15 modity. Pea, field, vines ...... 4 Peanut, hay ...... 4.0 Peanut ...... 0 .05 Commodity Parts per million Pistachio ...... 0.04 Poultry, fat ...... 0.04 Alfalfa, forage ...... 0.01 Poultry, meat ...... 0 .04 Alfalfa, hay ...... 0.01 Poultry, meat byproducts ...... 0.04 Almond, hulls ...... 9 .0 Radish, tops ...... 10 Apple, wet pomace ...... 5 .0 Rice, grain ...... 3 .5 Artichoke, globe ...... 1.0 Rice, hulls ...... 8 Asparagus ...... 0.07 Sapodilla ...... 0 .7 Banana 1 ...... 0.10 Sapote, black ...... 0 .7 Barley, grain ...... 0 .05 Sapote, mamey ...... 0 .7 Barley, hay ...... 0 .3 Sheep, fat ...... 0 .1 Barley, straw ...... 5 .0 Sheep, meat ...... 0.1 Beet, sugar, dried pulp ...... 0 .4 Sheep, meat byproducts ...... 0 .1 Beet, sugar, molasses ...... 0 .2 Soybean, forage ...... 10 .0 Beet, sugar, roots ...... 0 .1 Soybean, hay ...... 25 .0 Beet, sugar, tops ...... 4.0 Soybean, seed ...... 0 .08 Berry, low growing subgroup 13–07G ...... 1.5 Star apple ...... 0 .7 Brassica, head and stem, subgroup 5A ...... 2 .0 Vegetable, cucurbit, group 9 ...... 0.50 Brassica, leafy greens, subgroup 5B ...... 30 Vegetable, fruiting ...... 0.5 Canistel ...... 0 .7 Vegetable, root, except sugar beet, subgroup Cattle, fat ...... 0.1 1B ...... 0 .1 Cattle, meat ...... 0 .1 Vegetable, tuberous and corm, subgroup 1C ... 0.04 Cattle, meat byproducts ...... 0.1 Wheat, bran ...... 0.15 Citrus, dried pulp ...... 1 .0 Wheat, forage ...... 0 .3 Citrus, oil ...... 38 Wheat, grain ...... 0 .05 Coffee, green bean 2 ...... 0 .02 Wheat, hay ...... 0 .2 Corn, field, forage ...... 6 .0 Wheat, straw ...... 5 .0 Corn, field, grain ...... 0 .05 1 There are no U.S. registrations as of September 27, 1999 Corn, field, stover ...... 7 for use on banana. Corn, field, refined oil ...... 0 .1 2 There are no U.S. registrations as of January 18, 2012 for Corn, pop, grain ...... 0.05 use on coffee, green bean. Corn, pop, stover ...... 7 Corn, sweet, cannery waste ...... 0 .6 (b) Section 18 emergency exemptions. Corn, sweet, forage ...... 7 .0 [Reserved] Corn, sweet, kernel plus cob with husks removed ...... 0 .04 (c) Tolerances with regional registra- Corn, sweet, stover ...... 4 .0 tions. [Reserved] Dill, seed ...... 30 (d) Indirect or inadvertent residues. Egg ...... 0 .04 [Reserved] Fruit, citrus, group 10 ...... 0 .6 Fruit, pome ...... 0.5 [64 FR 51907, Sept. 27, 1999] Fruit, small vine climbing, except fuzzy kiwifruit, subgroup 13–07F ...... 2.0 EDITORIAL NOTE: For FEDERAL REGISTER ci- Fruit, stone, group 12 ...... 2 tations affecting § 180.555, see the List of CFR Goat, fat ...... 0 .1 Sections Affected, which appears in the Goat, meat ...... 0.1 Finding Aids section of the printed volume Goat, meat byproducts ...... 0 .1 Grain, aspirated fractions ...... 5 .0 and at www.fdsys.gov. Grape, raisin ...... 5 .0 Grass, forage ...... 12 § 180.556 Pymetrozine; tolerances for Grass, hay ...... 17 residues. Herbs, subgroup 19A ...... 200 Hog, fat ...... 0 .05 (a) General. Tolerances are estab- Hog, meat ...... 0 .05 lished for residues of the insecticide Hog, meat byproducts ...... 0 .05 pymetrozine 1,2,4-triazin-3(2H)-one,4,5- Hop, dried cones ...... 11 .0 Horse, fat ...... 0 .1 dihydro-6-methyl-4-[(3- Horse, meat ...... 0 .1 pyridinylmethylene) amino] in or on

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the following raw agricultural com- Commodity Parts per modities. The tolerance level for each million commodity is expressed in terms of the Goat, meat byproducts (except liver) ...... 0.15 parent insecticide only, which serves as Hog, fat ...... 0 .01 an indicator of the use of pymetrozine Hog, liver ...... 0 .05 on these raw agricultural commodities. Hog, meat ...... 0 .01 Hog, meat byproducts (except liver) ...... 0 .01 Parts per Horse, fat ...... 0 .15 Commodity million Horse, liver ...... 1 .50 Horse, meat ...... 0 .01 Asparagus ...... 0.04 Horse, meat byproducts (except liver) ...... 0 .15 Brassica, head and stem, subgroup 5A ...... 0 .5 Low growing berry subgroup 13–07G, except Brassica, leafy greens, subgroup 5B ...... 0 .25 cranberry ...... 0 .25 Cotton, gin byproducts ...... 2 .0 Milk ...... 0.03 Cotton, undelinted seed ...... 0 .3 Milk, fat ...... 0 .75 Hop, dried cones ...... 6 .0 Peanut ...... 0 .03 Pecan ...... 0 .02 Peanut, oil ...... 0 .10 Turnip, greens ...... 0.25 Pecan ...... 0 .04 Vegetable, fruiting, group 8 ...... 0.2 Poultry, fat ...... 0.05 Vegetable, cucurbit, group 9 ...... 0.1 Vegetable, leafy, execpt brassica, group 4 ...... 0 .6 Poultry, meat ...... 0 .01 Vegetable, tuberous and corm, subgroup 1C ... 0.02 Poultry meat byproducts ...... 0 .05 Sheep, fat ...... 0 .15 Sheep, liver ...... 1.50 (b) Section 18 emergency exemptions. Sheep, meat ...... 0.01 [Reserved] Sheep, meat byproducts (except liver) ...... 0.15 (c) Tolerances with regional registra- Small fruit vine climbing, except fuzzy kiwifruit, tions. [Reserved] subgroup 13–07F ...... 0.20 Soybean, refined oil ...... 0 .80 (d) Indirect or inadvertent residues. Soybean, seed ...... 0 .15 [Reserved] [65 FR 48634, Aug. 9, 2000, as amended at 66 (b) Section 18 emergency exemptions. FR 14846, Mar. 14, 2001; 66 FR 66794, Dec. 27, [Reserved] 2001; 70 FR 7047, Feb. 10, 2005; 70 FR 43298, (c) Tolerances with regional registra- July 27, 2005] tions. [Reserved] (d) Indirect or inadvertent residues. § 180.557 Tetraconazole; tolerances for [Reserved] residues. (a) General. Tolerances are estab- [70 FR 20830, Apr. 22, 2005, as amended at 70 FR 31359, June 1, 2005; 72 FR 18134, Apr. 11, lished for residues of tetraconazole, in- 2007; 73 FR 67406, Nov. 14, 2008; 76 FR 53648, cluding its metabolites and degradates, Aug. 29, 2011] in or on the commodities listed below. Compliance with the following toler- § 180.559 Clodinafop-propargyl; tolerance levels is to be determined by ances for residues. measuring only tetraconazole (1-[2-(2,4- (a) General. Tolerances are estab- dichlorophenyl)-3-(1,1,2,2- lished for clodinafop-propargyl, includ- tetrafluoroethoxy)propyl]-1H-1,2,4-tri- ing its metabolites and degradates, in azole), in or on the following commod- or on the commodities in the following ities. table. Compliance with the tolerance Parts per levels specified in the following table is Commodity million to be determined by measuring only clodinafop-propargyl [(2R)-2-[4-[(5- Aspirated grain fractions ...... 1 .0 Beet sugar, dried pulp ...... 0 .15 chloro-3-fluoro-2- Beet sugar, molasses ...... 0 .15 pyridinyl)oxy]phenoxy]propanoic acid, Beet sugar, root ...... 0 .05 2-propynyl ester] and its metabolite Cattle, fat ...... 0.15 Cattle, liver ...... 1 .50 clodinafop [(2R)-2-[4-[(5-chloro-3-fluoro- Cattle, meat ...... 0 .01 2- pyridinyl)oxy]phenoxy]propanoic Cattle, meat byproducts (except liver) ...... 0 .15 acid]. Corn, field, forage ...... 1 .1 Corn, field, grain ...... 0 .01 Parts per Corn, field, stover ...... 1 .7 Commodity million Corn, pop, grain ...... 0.01 Corn, pop, stover ...... 1.7 Wheat, forage ...... 0 .1 Eggs ...... 0 .02 Wheat, grain ...... 0 .02 Goat, fat ...... 0 .15 Wheat, hay ...... 0 .1 Goat, liver ...... 1.50 Wheat, straw ...... 0 .5 Goat, meat ...... 0.01

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(b) Section 18 emergency exemptions. boxylic acid (CGA–210007), expressed as [Reserved] the stoichiometric equivalent of (c) Tolerances with regional registra- acibenzolar-S-methyl, in or on the fol- tions. [Reserved] lowing raw agricultural commodities. (d) Indirect or inadvertent residues. Parts per [Reserved] Commodity million [65 FR 38774, June 22, 2000, as amended at 77 Banana 1 ...... 0.1 FR 72226, Dec. 5, 2012] Berry, low growing, subgroup 13–07G ...... 0 .15 Fruit, citrus, group 10–10 ...... 0 .02 § 180.560 Cloquintocet-mexyl; toler- Fruit, pome, group 11–10 ...... 0 .03 ances for residues. Onion, bulb, subgroup 3–07A ...... 0 .1 Spinach ...... 1 .0 (a) General. Tolerances are estab- Tomato, paste ...... 3 .0 lished for the combined residues of Vegetable, brassica, leafy, group 5 ...... 1.0 cloquintocet-mexyl, (acetic acid [(5- Vegetable, cucurbit, group 9 ...... 2.0 Vegetable, fruiting, group 8 ...... 1.0 chloro-8-quinolinyl)oxy]-,1- Vegetable, leafy, group 4 ...... 0 .25 methylhexyl ester; CAS Reg. No. 99607– 1 70–2) and its acid metabolite (5-chloro- There are no United States registrations for banana. 8-quinolinoxyacetic acid), when used as (2) Tolerances are established for res- an inert ingredient (safener) in pes- idues of acibenzolar- S -methyl, ticide formulations containing the ac- benzo(1,2,3)thiadiazole-7-carbothioic tive ingredients clodinafop-propargyl acid- S -methyl ester, including its me- (wheat only), dicamba (wheat only), tabolites and degradates, in or on the flucarbazone-sodium (wheat only), commodities in the table below. Com- pinoxaden (wheat or barley), or pliance with the tolerance levels speci- pyroxsulum (wheat only) in or on the fied below is to be determined by meas- following food commodities: uring only those acibenzolar- S -methyl residues convertible to Parts per Commodity million benzo(1,2,3)thiadiazole-7-carboxylic acid (CGA–210007), expressed as the Barley, grain ...... 0 .1 Stoichiometric equivalent of Barley, hay ...... 0 .1 Barley, straw ...... 0 .1 acibenzolar- S -methyl, in or on the fol- Wheat, forage ...... 0 .2 lowing raw agricultural commodities. Wheat, grain ...... 0 .1 Wheat, hay ...... 0 .5 Expiration/ Wheat, straw ...... 0 .1 Commodity Parts per revocation million date (b) Section 18 emergency exemptions. Apple ...... 0.05 12/31/15 [Reserved] Grapefruit ...... 0.05 12/31/15 (c) Tolerances with regional registra- Pear ...... 0.05 12/31/15 tions. [Reserved] (d) Indirect or inadvertent residues. (b) Section 18 emergency exemptions. [Reserved] [Reserved] (c) Tolerances with regional registra- [65 FR 38764, June 22, 2000, as amended at 70 FR 74688, Dec. 16, 2005; 73 FR 11820, Mar. 5, tions. [Reserved] 2008; 75 FR 16020, Mar. 31, 2010; 76 FR 38035, (d) Indirect or inadvertent residues. June 29, 2011] [Reserved] [65 FR 50446, Aug. 18, 2000, as amended at 70 § 180.561 Acibenzolar-S-methyl; toler- FR 7861, Feb. 16, 2005; 71 FR 76200, Dec. 20, ances for residues. 2006; 74 FR 24710, May 26, 2009; 76 FR 34886, (a) General. (1) Tolerances are estab- June 15, 2011; 77 FR 21676, Apr. 11, 2012; 77 FR lished for residues of acibenzolar-S- 30406, May 23, 2012; 80 FR 58620, Sept. 30, 2015] methyl, benzo(1,2,3)thiadiazole-7- carbothioic acid-S-methyl ester, in- § 180.562 Flucarbazone-sodium; toler- cluding its metabolites and degradates, ances for residues. in or on the commodities in the table (a) General. Tolerances are estab- below. Compliance with the tolerance lished for combined residues of the her- levels specified below is to be deter- bicide flucarbazone-sodium, 4,5- mined by measuring only those dihydro-3-methoxy-4-methyl-5-oxo-N- acibenzolar-S-methyl residues convert- [[2(trifluoromethoxy)phenyl] sulfonyl]- ible to benzo(1,2,3)thiadiazole-7-car- 1H-1,2,4-triazole 1-carboxamide, sodium

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salt) and its N-desmethyl metabolite; § 180.564 Indoxacarb; tolerances for and its metabolites converted to 2- residues. (trifluoromethoxy)benzene sulfonamide (a) General. (1) Tolerances are estab- and calculated as flucarbazone-sodium lished for residues of indoxacarb, in- in or on the following food commod- cluding its metabolites and degradates, ities: in or on the commodities in the table Parts per below. Compliance with the tolerance Commodity million levels specified below is to be determined by measuring only indoxacarb, Cattle, liver ...... 1 .50 Cattle, meat ...... 0 .01 (S)-methyl 7-chloro-2,5-dihydro-2-[[(me- Cattle, meat byproducts, except liver ...... 0 .01 thoxycarbonyl)[4- Goat, liver ...... 1.50 (trifluoromethoxy)phenyl] Goat, meat ...... 0.01 Goat, meat byproducts, except liver ...... 0 .01 amino]carbonyl]indeno[1,2- Hog, liver ...... 1 .50 e][1,3,4][oxadiazine-4a(3H)-carboxylate, Hog, meat ...... 0 .01 and its R-enantiomer, (R)-methyl 7- Hog, meat byproducts, except liver ...... 0 .01 Horse, liver ...... 1 .50 chloro-2,5-dihydro-2-[[(methoxycar- Horse, meat ...... 0 .01 bonyl)[4-(trifluoromethoxy) Horse, meat byproducts, except liver ...... 0 .01 phenyl]amino]carbonyl]indeno[1,2-e] Milk ...... 0.005 [1,3,4][oxadiazine-4a(3H)-carboxylate. Sheep, liver ...... 1.50 Sheep, meat ...... 0.01 Parts per Sheep, meat byproducts, except liver ...... 0 .01 Commodity million Wheat, forage ...... 0 .30 Wheat, grain ...... 0 .01 Apple, wet pomace ...... 3 .0 Wheat, hay ...... 0 .10 Alfalfa, forage ...... 10 Wheat, straw ...... 0 .05 Alfalfa, hay ...... 50 Bean, dry, seed ...... 0 .2 (b) Section 18 emergency exemptions. Bean, succulent ...... 0 .9 Beet, garden, roots ...... 0 .30 [Reserved] Beet, garden, tops ...... 6 .0 (c) Tolerances with regional registra- Berry, low growing, except strawberry, subgroup tions. [Reserved] 13–07H ...... 1 (d) Indirect or inadvertant residues. Bushberry subgroup 13–07B ...... 1 .5 Cattle, fat ...... 1.5 [Reserved] Cattle, meat ...... 0 .05 Cattle, meat byproducts ...... 0.03 [70 FR 67915, Nov. 9, 2005, as amended at 71 Corn, sweet, forage ...... 10 FR 76931, Dec. 22, 2006] Corn, sweet, kernel plus cob with husk removed 0.02 Corn, sweet, stover ...... 15 § 180.563 Ethametsulfuron-methyl; tol- Cotton, gin byproducts ...... 15 erances for residues. Cotton, undelinted seed ...... 2 .0 Cowpea, forage ...... 50 (a) General. A tolerance is established Cowpea, hay ...... 100 for residues of ethametsulfuron methyl Fruit, pome, except pear, group 11 ...... 1 .0 Fruit, small vine climbing, except fuzzy kiwifruit, (methyl 2- ((((4-ethoxy-6- subgroup 13–07F ...... 2 (methylamino)-1,3,5- triazin-2-yl) Fruit, stone, group 12 ...... 0 .90 amino) carbonyl) amino) sulfonyl) ben- Goat, fat ...... 1 .5 zoate) in or on the following raw agri- Goat, meat ...... 0.05 Goat, meat byproducts ...... 0 .03 cultural commodities. Grain, aspirated fractions ...... 45 Grape, raisin ...... 5 .0 Commodity Parts per Hog, fat ...... 1 .5 million Hog, meat ...... 0 .05 Hog, meat byproducts ...... 0 .03 Canola, seed ...... 0 .02 Horse, fat ...... 1 .5 Crambe, seed ...... 0.02 Horse, meat ...... 0 .05 Rapeseed, seed ...... 0 .02 Horse, meat byproducts ...... 0 .03 Milk ...... 0.15 (b) Section 18 emergency exemptions. Milk, fat ...... 4 .0 [Reserved] Okra ...... 0.50 Pea, southern, seed ...... 0.10 (c) Tolerances with regional registra- Peanut ...... 0 .01 tions. [Reserved] Peanut, hay ...... 40 (d) Indirect of inadvertent residues. Pear ...... 0 .20 Pear, oriental ...... 0.20 [Reserved] Peppermint, tops ...... 11 Sheep, fat ...... 1 .5 [65 FR 57972, Sept. 27, 2000, as amended at 66 Sheep, meat ...... 0.05 FR 18207, Apr. 6, 2001; 67 FR 35050, May 17, Sheep, meat byproducts ...... 0 .03 2002] Soybean, hulls ...... 4 .0

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(d) Indirect or inadvertent residues. Commodity Parts per million [Reserved] Soybean, seed ...... 0 .80 [65 FR 58424, Sept. 29, 2000, as amended at 67 Spearmint, tops ...... 11 FR 41807, June 19, 2002; 67 FR 47309, July 18, Turnip, greens ...... 12 2002; 67 FR 58730, Sept. 18, 2002; 68 FR 25830, Vegetable, Brassica, leafy, group 5 ...... 12 Vegetable, cucurbit, group 9 ...... 0.60 May 14, 2003; 68 FR 27746, May 21, 2003; 69 FR Vegetable, fruiting, group 8 ...... 0.50 28842, May 19, 2004; 69 FR 29459, May 24, 2004; Vegetable, leafy, except Brassica, group 4 ...... 14 69 FR 32282, June 9, 2004; 72 FR 37641, July 11, Vegetable, tuberous and corm, subgroup 1-C .... 0.01 2007; 74 FR 33165, July 10, 2009; 77 FR 8749, Feb. 15, 2012; 78 FR 78738, Dec. 27, 2013] (2) Tolerances are established for residues of indoxacarb, including its me- § 180.565 Thiamethoxam; tolerances for residues. tabolites and degradates, in or on the commodities in the table below. Com- (a) General. Tolerances are estab- pliance with the tolerance levels speci- lished for residues of the insecticide fied below is to be determined by meas- thiamethoxam, including its metabo- uring only the sum of indoxacarb, (S)- lites and degradates, in or on the fol- methyl-7-chloro-2,5-dihydro-2-[[(me- lowing commodities. Compliance with thoxycarbonyl)[4-(trifluoromethoxy)- the tolerance levels specified below is phenyl]amino]carbonyl]indeno[1,2e] to be determined by measuring only [1,3,4]oxadiazine-4a(3H)-carboxylate, its thiamethoxam 3-[(2-chloro-5- R-enantiomer, (R)-methyl 7-chloro-2,5- thiazolyl)methyl]tetrahydro-5-methyl- dihydro-2-[[(methoxycarbonyl)[4- N-nitro-4H-1,3,5-oxadiazin-4-imine and (trifluoromethoxy) its metabolite CGA–322704 N-[(2-chlorophenyl]amino]carbonyl]indeno [1,2-e] thiazol-5-yl)methyl]-N′-methyl-N″- [1,3,4] oxadiazine-4a(3H)-carboxylate, nitro-guanidine, calculated as the stoi- and the metabolites: IN–JT333, methyl chiometric equivalent of 7-chloro-2,5-dihydro-2-[[[4- thiamethoxam, in or on the following (trifluoromethoxy)phenyl]- commodities: amino]carbonyl]indeno[1,2- Parts per e][1,3,4]oxadiazine-4a(3H)-carboxylate; Commodity million IN–KT319, (E)-methyl 5-chloro-2,3,- Alfalfa, forage ...... 0.05 dihydro-2-hydroxy-1-[[[(methoxycar- Alfalfa, hay ...... 0.12 bonyl)[4- Almond, hulls ...... 1 .2 (trifluoromethoxy)phenyl]amino]-car- Artichoke, globe ...... 0.45 Avocado ...... 0 .40 bonyl]hydrazono]-1H-indene-2- Barley, grain ...... 0 .4 carboxylate; IN–JU873, methyl 5- Barley, hay ...... 0 .40 chloro-2,3-dihydro-2-hydroxy-1-[[[[4- Barley, straw ...... 0 .40 Bean, succulent ...... 0 .02 (triflurormethoxy)- Berry, low growing, subgroup 13–07G, except phenyl]amino]carbonyl]hydrazono]-1H- cranberry ...... 0.30 indene-2-carboxylate; IN–KG433, meth- Borage, seed ...... 0 .02 Brassica, head and stem, subgroup 5–A ...... 4.5 yl 5-chloro-2,3,-dihydro-2-hydroxy-1- Brassica, leafy greens, subgroup 5–B ...... 3 .0 [[[(methoxycarbonyl)[4- Buckwheat, forage ...... 0 .50 (trifluoromethoxy)phenyl] Buckwheat, hay ...... 0 .02 amino]carbonyl]-hydrazono]-1H-indene- Buckwheat, straw ...... 0 .02 Bushberry subgroup 13–07B, except lingonberry 2-carboxylate; and IN–KB687, methyl and blueberry, lowbush ...... 0 .20 [4- Caneberry subgroup 13–07A ...... 0.35 (trifluoromethoxy)phenyl]carbamate, Canistel ...... 0 .40 Canola, seed ...... 0 .02 calculated as the stoichiometric equiv- Cattle, meat ...... 0 .02 alent of indoxacarb in the commodity. Cattle, meat byproducts ...... 0.04 Citrus, dried pulp ...... 0 .60 Parts per Coffee, green, bean 1 ...... 0 .20 Commodity million Corn, field, forage ...... 0 .10 Corn, field, stover ...... 0 .05 Egg ...... 0 .20 Corn, pop, forage ...... 0 .10 Poultry, fat ...... 0.20 Corn, pop, stover ...... 0.05 Poultry, meat ...... 0 .06 Corn, sweet, forage ...... 0 .10 Poultry, meat byproducts ...... 0.06 Corn, sweet, kernel plus cob with husks removed ...... 0 .02 Corn, sweet, stover ...... 0 .05 (c) Tolerances with regional registra- Cotton, gin byproducts ...... 1 .5 tions. [Reserved] Cotton, undelinted seed ...... 0 .10

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(b) Section 18 emergency exemptions. Commodity Parts per million [Reserved] Crambe, seed ...... 0.02 (c) Tolerances with regional registra- Cranberry ...... 0 .02 tions. [Reserved] Flax, seed ...... 0 .02 (d) Indirect or inadvertent residues. Food commodities and feed commodities (other [Reserved] than those covered by a higher tolerance as a result of use on growing crops) in food/feed [65 FR 79762, Dec. 20, 2000] handling establishments ...... 0 .02 Fruit, citrus, group 10 ...... 0 .40 EDITORIAL NOTE: For FEDERAL REGISTER ci- Fruit, pome, group 11 ...... 0.2 tations affecting § 180.565, see the List of CFR Fruit, small, vine climbing, subgroup 13–07F, Sections Affected, which appears in the except fuzzy kiwifruit ...... 0 .20 Finding Aids section of the printed volume Fruit, stone, group 12 ...... 0 .5 and at www.fdsys.gov. Goat, meat ...... 0.02 Goat, meat byproducts ...... 0 .04 Grain, aspirated fractions ...... 2 .0 § 180.566 Fenpyroximate; tolerances Grain, cereal, group 15, except barley ...... 0.02 for residues. Grape, raisin ...... 0 .30 (a) General. (1) Tolerances are estab- Hog, meat ...... 0 .02 Hog, meat byproducts ...... 0 .02 lished for residues of the insecticide Hop, dried cones ...... 0 .10 fenpyroximate, including its metabo- Horse, meat ...... 0 .02 lites and degradates, in or on the com- Horse, meat byproducts ...... 0 .04 modities in the table below. Compli- Mango ...... 0.40 Milk ...... 0.02 ance with the tolerance levels specified Millet, pearl, forage ...... 0 .02 in the table is to be determined by Millet, pearl, stover ...... 0 .02 measuring only the sum of Millet, proso, forage ...... 0 .02 fenpyroximate, (E)-1,1-dimethylethyl 4- Millet, proso, stover ...... 0 .02 Millet, proso, straw ...... 0 .02 [[[[(1,3-dimethyl-5-phenoxy-1H-pyrazol- Mustard, seed ...... 0 .02 4-yl)methylene] Nut, tree, group 14 ...... 0 .02 amino]oxy]methyl]benzoate and its Z- Oat, forage ...... 0 .50 isomer, (Z)-1,1-dimethylethyl 4-[[[[(1,3- Oat, hay ...... 0.02 Oat, straw ...... 0.02 dimethyl-5-phenoxy-1H-pyrazol-4- Onion, dry bulb ...... 0 .03 yl)methylene] Papaya ...... 0 .40 amino]oxy]methyl]benzoate, calculated Peanut ...... 0 .05 Peanut, hay ...... 0.25 as the stoichiometric equivalent of Peanut, meal ...... 0 .15 fenpyroximate. Peppermint, tops ...... 1 .5 Pistachio ...... 0.02 Commodity Parts per Potato ...... 0 .25 million Radish, tops ...... 0 .80 Almond, hulls ...... 3 .0 Rapeseed, seed ...... 0 .02 Avocado ...... 0 .15 Rye, forage ...... 0 .50 Bean, snap, succulent ...... 0 .40 Rye, straw ...... 0 .02 Berry, low growing, subgroup 13–07G ...... 1 .0 Safflower, seed ...... 0 .02 Canistel ...... 0 .15 Sapodilla ...... 0 .40 Citrus, dried pulp ...... 2 .5 Sapote, black ...... 0 .40 Citrus, oil ...... 10 Sapote, mamey ...... 0 .40 Corn, field, forage ...... 2 .0 Sheep, meat ...... 0.02 Corn, field, grain ...... 0 .02 Sheep, meat byproducts ...... 0 .04 Corn, field, refined oil ...... 0 .05 Sorghum, forage ...... 0 .02 Corn, field, stover ...... 7 .0 Sorghum, grain, stover ...... 0 .02 Corn, pop, forage ...... 2 .0 Soybean, hulls ...... 0 .08 Corn, pop, grain ...... 0.02 Spearmint, tops ...... 1 .5 Corn, pop, stover ...... 7.0 Star apple ...... 0 .40 Cotton, gin byproducts ...... 10 Sunflower ...... 0 .02 Cotton, undelinted seed ...... 0 .10 Tea, dried 1 ...... 20 Cucumber ...... 0 .40 Tomato, paste ...... 0 .80 Fruit, citrus, group 10–10 ...... 0 .50 Vegetable, cucurbit, group 9 ...... 0.2 Fruit, pome, group 11–10 ...... 0 .30 Vegetable, fruiting, group 8 ...... 0.25 Fruit, small, vine climbing, except fuzzy Vegetable, leafy, except brassica, group 4 ...... 4 .0 kiwifruit, subgroup 13–07F ...... 1 .0 Vegetable, legume, group 6 ...... 0 .02 Fruit, stone, group 12–12 ...... 2 .0 Vegetable, root, subgroup 1A ...... 0 .05 Grain, aspirated fractions ...... 0 .40 Vegetable, tuberous and corm, except potato, Hop, dried cones ...... 10 subgroup 1D ...... 0 .02 Mango ...... 0.15 Wheat, forage ...... 0 .50 Melon subgroup 9A ...... 0 .10 Wheat, hay ...... 0 .02 Nut, tree, group 14 ...... 0 .10 Wheat, straw ...... 0 .02 Papaya ...... 0 .15 Peppermint, tops ...... 7 .0 1 There are no U.S. registrations as of March 27, 2013. Pistachio ...... 0.10

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methyleneaminooxymethyl]benzoic Commodity Parts per million acid, calculated as the stoichiometric Sapodilla ...... 0 .15 equivalent of fenpyroximate. Sapote, black ...... 0 .15 Sapote, mamey ...... 0 .15 Commodity Parts per Spearmint, tops ...... 7 .0 million Star, apple ...... 0 .15 Tea, dried 1 ...... 20 Cattle, kidney ...... 0 .25 Vegetable, fruiting, group 8–10 ...... 0 .20 Cattle, liver ...... 0 .25 Vegetable, tuberous and corm, subgroup 1C ... 0.10 Goat, kidney ...... 0 .25 Goat, liver ...... 0.25 1 There are no U.S. Registrations. Horse, kidney ...... 0 .25 (2) Tolerances are established for res- Horse, liver ...... 0 .25 Sheep, kidney ...... 0.25 idues of the insecticide fenpyroximate, Sheep, liver ...... 0.25 including its metabolites and degradates, in or on the commodities (b) Section 18 emergency exemptions. in the table below. Compliance with Time-limited tolerances are estab- the tolerance levels specified in the lished for residues of the insecticide table is to be determined by measuring fenpyroximate, including its metabo- only the sum of fenpyroximate, (E)-1,1- lites and degradates in or on the com- dimethylethyl 4-[[[[(1,3-dimethyl-5- modities in the table below. Compli- phenoxy-1H-pyrazol-4-yl)methylene] ance with the tolerance levels specified amino]oxy]methyl]benzoate and its in the table is to be determined by metabolites (E)-4-[(1,3-dimethyl-5- measuring only the sum of phenoxypyrazol-4-yl)- fenpyroximate, (E)-1,1-dimethylethyl 4- methyleneaminooxymethyl]benzoic [[[[(1,3-dimethyl-5-phenoxy-1H-pyrazol- acid and (E)-1,1-dimethylethyl-2-hy- 4-yl) meth- droxyethyl 4-[[[[(1,3-dimethyl-5- ylene]amino]oxy]methyl]benzoate and phenoxy-1H-pyrazol-4-yl)methylene] its Z-isomer, (Z)-1,1-dimethylethyl 4- amino]oxy]methyl]benzoate, calculated [[[[(1,3-dimethyl-5-phenoxy-1H-pyrazol- as the stoichiometric equivalent of 4-yl)methylene] fenpyroximate. amino]oxy]methyl]benzoate, calculated Parts per as the stoichiometric equivalent of Commodity million fenpyroximate.

Cattle, fat ...... 0.03 Expiration/revoca- Cattle, meat ...... 0 .03 Commodity Parts per million tion date Cattle, meat byproducts, except kidney and liver ...... 0 .03 Honey ...... 0.10 12/31/13 Goat, fat ...... 0 .03 Goat, meat ...... 0.03 Goat, meat byproducts, except kidney and liver 0 .03 (c) Tolerances with regional registra- Horse, fat ...... 0 .03 tions. [Reserved] Horse, meat ...... 0 .03 (d) Indirect or inadvertent residues. Horse, meat byproducts, except kidney and liver ...... 0 .03 [Reserved] Milk ...... 0.015 Sheep, fat ...... 0 .03 [66 FR 18568, Apr. 10, 2001, as amended at 69 Sheep, meat ...... 0.03 FR 32464, June 10, 2004; 71 FR 49368, Aug. 23, Sheep, meat byproducts, except kidney and 2006; 72 FR 26321, May 9, 2007; 74 FR 37617, liver ...... 0 .03 July 29, 2009; 74 FR 63079, Dec. 2, 2009; 75 FR 80346, Dec. 22, 2010; 77 FR 73951, Dec. 12, 2012; (3) Tolerances are established for res- 78 FR 36097, June 17, 2013] idues of the insecticide fenpyroximate, including its metabolites and § 180.567 Zoxamide; tolerances for resi- degradates, in or on the commodities dues. in the table below. Compliance with (a) General. (1) Tolerances are estab- the tolerance levels specified in the lished for residues of zoxamide includ- table is to be determined by measuring ing metabolites and degradates, in or only the sum of fenpyroximate, (E)-1,1- on the commodities in the table below. dimethylethyl 4-[[[[(1,3-dimethyl-5- Compliance with the tolerance levels phenoxy-1H-pyrazol-4-yl)methylene] specified below is to be determined by amino]oxy]methyl]benzoate and its measuring only zoxamide (3,5-dichloro- metabolite (E)-4-[(1,3-dimethyl-5- N-(3-chloro-1-ethyl-1-methyl-2- phenoxypyrazol-4-yl)- oxopropyl)-4-methylbenzamide).

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Parts per Parts per Commodity million Commodity million

Fruit, small vine climbing, except fuzzy kiwifruit, Almond, hulls ...... 0 .70 subgroup 13–07F ...... 5 .0 Artichoke, globe ...... 0.02 Grape, raisin ...... 15.0 Asparagus ...... 0.02 Tomato subgroup 8–10A ...... 2 .0 Bushberry subgroup 13–07B ...... 0 .02 Vegetable, cucurbit, group 9 ...... 1.0 Cabbage ...... 0 .02 Cabbage, Chinese, napa ...... 0 .02 (2) Tolerances are established for res- Corn, field, forage ...... 0 .02 Corn, field, grain ...... 0 .02 idues of zoxamide including metabo- Corn, field, stover ...... 0 .02 lites and degradates, in or on the com- Cotton, gin byproducts ...... 0 .60 modities in the table below. Compli- Cotton, undelinted seed ...... 0 .02 ance with the tolerance levels specified Fish, freshwater ...... 1 .5 Fruit, pome, group 11 ...... 0.02 below is to be determined by measuring Fruit, stone, group 12 ...... 0 .02 only the sum of zoxamide (3,5-dichloro- Garlic ...... 0 .02 N-(3-chloro-1-ethyl-1-methyl-2- Grain, aspirated fractions ...... 100 oxopropyl)-4-methylbenzamide) and its Grape ...... 0 .02 Hop, dried cones ...... 0 .05 metabolites 3,5-dichloro-1,4- Leaf petioles subgroup 4B ...... 0 .02 benzenedicarboxylic acid (RH–1455 and Nut, tree, group 14 ...... 0 .02 RH–141455) and 3,5-dichloro-4- Okra ...... 0.02 Olive ...... 0 .02 hydroxymethylbenzoic acid (RH–1452 Onion, bulb ...... 0 .02 and RH–141452) calculated as the stoi- Pea and bean, dried shelled, except soybean, chiometric equivalent of zoxamide. subgroup 6C ...... 0 .07 Peanut ...... 0 .02 Parts per Peppermint, tops ...... 0 .04 Commodity million Pistachio ...... 0.02 Pomegranate ...... 0 .02 Ginseng ...... 0 .30 Prickly pear, fruit ...... 0 .07 Onion, bulb, subgroup 3–07A ...... 0 .7 Prickly pear, pads ...... 0.06 Potato, granules/flakes ...... 0 .30 Rapeseed subgroup 20A ...... 0 .40 Potato, wet peel ...... 0 .10 Shallot, bulb ...... 0 .02 Vegetable, tuberous and corm, subgroup 1C ... 0.06 Soybean, seed ...... 0 .02 Spearmint, tops ...... 0 .04 (b) Section 18 emergency exemptions. Strawberry ...... 0 .07 [Reserved] Sugarcane, cane ...... 0.20 Sunflower subgroup 20B ...... 0.50 (c) Tolerances with regional registra- Vegetable, cucurbit, group 9 ...... 0.03 tions. [Reserved] Vegetable, fruiting, group 8 ...... 0.02 (d) Indirect or inadvertent residues. Vegetable, tuberous and corm, subgroup 1C ..... 0.02 Wheat, forage ...... 0 .02 [Reserved] Wheat, grain ...... 0 .40 [66 FR 18733, Apr. 11, 2001, as amended at 66 Wheat, hay ...... 0 .02 Wheat, straw ...... 6 .0 FR 49118, Sept. 26, 2001; 69 FR 16805, Mar. 31, 2004; 71 FR 31104, June 1, 2006; 71 FR 76200, Dec. 20, 2006; 75 FR 770, Jan. 6, 2010; 79 FR (b) Section 18 emergency exemptions. 41915, July 18, 2014; 81 FR 12015, Mar. 8, 2016] [Reserved] (c) Tolerances with regional registra- § 180.568 Flumioxazin; tolerances for tions. [Reserved] residues. (d) Indirect or inadvertent residues. (a) General. Tolerances are estab- [Reserved] lished for residues of flumioxazin, 2-[7- [66 FR 19878, Apr. 18, 2001, as amended at 68 fluoro-3,4-dihydro-3-oxo-4-(2-propynyl)- FR 51471, Aug. 27, 2003; 69 FR 16831, Mar. 31, 2H-1,4-benzoxazin-6-yl]-4,5,6,7- 2004; 69 FR 52198, Aug. 25, 2004; 71 FR 25956, tetrahydro-1H-isoindole-1,3(2H)-dione, May 3, 2006; 71 FR 61413, Oct. 18, 2006; 73 FR including its metabolites and 11831, Mar. 5, 2008; 73 FR 39251, July 9, 2008; 75 degradates, in or on the commodities FR 8265, Feb. 24, 2010; 75 FR 69009, Nov. 10, in the table below. Compliance with 2010; 77 FR 58499, Sept. 21, 2012; 78 FR 20466, Apr. 5, 2013] the tolerance levels specified below is to be determined by measuring only § 180.569 Forchlorfenuron; tolerances flumioxazin. for residues. (a) General. (1) Tolerances are estab- Commodity Parts per million lished for residues of forchlorfenuron, Alfalfa, forage ...... 3.0 including its metabolites and Alfalfa, hay ...... 8.0 degradates, in or on the commodities

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in the table below. Compliance with Commodity Parts per the tolerance levels specified below is million to be determined by measuring only Corn, field, forage ...... 0 .20 forchlorfenuron (N-(2-chloro-4- Corn, field, grain ...... 0 .08 pyridinyl)-N-phenylurea). Corn, field, stover ...... 0 .40 Corn, oil ...... 0 .50 Corn, pop, grain ...... 0.04 Parts per Commodity million Corn, pop, stover ...... 0.25 Corn, sweet, forage ...... 0 .30 Almond ...... 0.01 Corn, sweet, kernel plus cob with husk removed 0.04 Almond, hulls ...... 0 .15 Corn, sweet, stover ...... 0 .45 Bushberry subgroup 13–07B ...... 0 .01 Cherry, sweet ...... 0 .01 (2) Tolerances are established for the Fig ...... 0 .01 residues of isoxadifen-ethyl (3- Grape ...... 0 .03 isoxazolecarboxylic acid, 4,5-dihydro- Grape, raisin ...... 0 .06 Kiwifruit ...... 0.04 5,5-diphenyl-, ethyl ester (CAS No. Pear ...... 0 .01 164520–33–0)), and its metabolites 4,5- Pistachio ...... 0.01 dihydro-5,5-diphenyl-3- Plum, prune, fresh ...... 0.01 isoxazolecarboxylic acid and b-hydroxy- -benzenepropanenitrile when (2) Temporary tolerances are estab- b used as an inert ingredient (safener) in lished for residues of forchlorfenuron, or on the following raw agricultural including its metabolites and commodities: degradates, in or on the commodities in the table below. Compliance with Commodity Parts per the tolerance levels specified below is million to be determined by measuring on Rice, grain ...... 0 .10 forchlorfenuron (N-(2-chloro-4- Rice, hulls ...... 0 .50 pyridinyl)-N′-phenylurea). (b) Section 18 emergency exemptions. Expiration/ [Reserved] Commodity Parts per revocation million date (c) Tolerances with regional registrations. [Reserved] Almond ...... 0.01 12/31/15 (d) Indirect or inadvertent residues. Almond, hulls ...... 0.15 12/31/15 Cherry, sweet ...... 0.01 12/31/15 [Reserved] Fig ...... 0.01 12/31/15 Pear ...... 0.01 12/31/15 [66 FR 33187, June 21, 2001, as amended at 66 Pistachio ...... 0.01 12/31/15 FR 40141, Aug. 2, 2001; 67 FR 12878, Mar. 20, Plum, prune, fresh ...... 0.01 12/31/15 2002; 69 FR 29890, May 26, 2004; 72 FR 63997, Nov. 14, 2007; 80 FR 72599, Nov. 20, 2016] (b) Section 18 emergency exemptions. [Reserved] § 180.571 Mesotrione; tolerances for (c) Tolerances with regional restric- residues. tions. [Reserved] (a) General. Tolerances are estab- (d) Indirect or inadvertent residues. lished for residues of the herbicide [Reserved] mesotrione, including its metabolites and degradates, in or on the commod- [66 FR 22936, May 7, 2001, as amended at 69 ities in the table below. Compliance FR 48805, Aug. 11, 2004; 69 FR 58322, Sept. 30, with the tolerance levels specified 2004; 73 FR 47846, Aug. 15, 2008; 78 FR 46283, July 31, 2013; 79 FR 18471, Apr. 2, 2014] below is to be determined by measuring only mesotrione, 2-[4-(methylsulfonyl)- § 180.570 Isoxadifen-ethyl; tolerances 2-nitrobenzoyl]-1,3-cyclohexanedione, for residues. in or on the following raw agricultural (a) General. (1) Tolerances are estab- commodities: lished for residues of isoxadifen-ethyl Parts per (ethyl 5,5-diphenyl-2-isoxazoline-3- Commodity million carboxylate, (CAS No. 163520–33–0), and Almond, hulls ...... 0 .02 its metabolite: 4,5-dihydro-5,5-di- Asparagus ...... 0.01 phenyl-3-isoxazolecarboxylic acid, Berry, group 13 ...... 0 .01 when used as an inert ingredient Corn, field, forage ...... 0 .01 Corn, field, grain ...... 0 .01 (safener) in or on the following raw ag- Corn, field, stover ...... 0 .01 ricultural commodities: Corn, pop, grain ...... 0.01

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Parts per Parts per Commodity million Commodity million

Corn, pop, stover ...... 0.01 Acerola ...... 0.90 Corn, sweet, forage ...... 0 .5 Almond, hulls ...... 15 Corn, sweet, kernel plus cob with husks re- Apple, wet pomace ...... 1 .2 moved ...... 0 .01 Atemoya ...... 1 .6 Corn, sweet, stover ...... 1 .5 Avocado ...... 7 .0 Cranberry ...... 0 .02 Bean, dry seed ...... 0 .60 Flax, seed ...... 0 .01 Berry, low-growing subgroup 13–07G ...... 1 .5 Fruit, citrus, group 10–10 ...... 0 .01 Biriba ...... 1 .6 Fruit, pome, group 11–10 ...... 0 .01 Black sapote ...... 7 .0 Fruit, stone, group 12–12 ...... 0 .01 Caneberry subgroup 13-07A ...... 5.0 Grass, forage ...... 0 .01 Canistel ...... 7 .0 Grass, hay ...... 0 .01 Cattle, fat ...... 0.10 Grass, seed screenings ...... 0 .10 Cherimoya ...... 1 .6 Grass, straw ...... 0 .10 Cotton, gin byproducts ...... 35 Lingonberry ...... 0.01 Cotton, undelinted seed ...... 0 .75 Millet, forage ...... 0 .01 Custard apple ...... 1 .6 Millet, grain ...... 0 .01 Feijoa ...... 0 .90 Millet, hay ...... 0 .02 Fruit, pome, group 11–10 ...... 0 .7 Millet, straw ...... 0 .02 Fruit, small, vine climbing subgroup 13–07F, ex- Nut, tree, group 14–12 ...... 0 .01 cept fuzzy kiwifruit ...... 1 .0 Oat, forage ...... 0 .01 Oat, grain ...... 0 .01 Fruit, stone, group 12, except plum ...... 2 .5 Oat, hay ...... 0.01 Goat, fat ...... 0 .10 Oat, straw ...... 0.01 Grape ...... 0 .75 Okra ...... 0.01 Grape, raisin ...... 1 .2 Rhubarb ...... 0 .01 Guava ...... 0 .9 Sorghum, grain, forage ...... 0.01 Herb, subgroup 19A, except chervil and chive ... 300 Sorghum, grain, grain ...... 0 .01 Hog, fat ...... 0 .10 Sorghum, grain, stover ...... 0 .01 Hop, dried cones ...... 15 Sorghum, sweet ...... 0 .01 Horse, fat ...... 0 .10 Soybean, seed ...... 0 .01 Jaboticaba ...... 0 .90 Sugarcane, cane ...... 0.01 Ilama ...... 1 .6 Longan ...... 5 .0 Lychee ...... 5 .0 (b) Section 18 emergency exemptions. Mango ...... 7.0 [Reserved] Nut, tree, group 14 ...... 0 .20 (c) Tolerances with regional registra- Okra ...... 2.0 tions. [Reserved] Papaya ...... 7 .0 Passionfruit ...... 0 .90 (d) Indirect or inadvertent residues. Pea and bean, succulent shelled, subgroup 6B 0 .70 [Reserved] Peppermint, tops ...... 25 Pistachio ...... 0.20 [66 FR 33195, June 21, 2001, as amended at 67 Plum ...... 0 .20 FR 45656, July 10, 2002; 68 FR 273, Jan. 3, 2003; Pulasan ...... 5 .0 69 FR 58310, Sept. 30, 2004; 70 FR 14551, Mar. Rambutan ...... 5 .0 23, 2005; 72 FR 71802, Dec. 19, 2007; 73 FR 1512, Sapodilla ...... 7 .0 Jan. 9, 2008; 73 FR 9226, Feb. 20, 2008; 74 FR Sapote, mamey ...... 7 .0 67123, Dec. 18, 2009; 76 FR 34886, June 15, 2011; Sheep, fat ...... 0 .10 80 FR 30630, May 29, 2015] Soursop ...... 1 .6 Soybean, succulent shelled ...... 0 .70 Spanish lime ...... 5 .0 § 180.572 Bifenazate; tolerance for resi- Spearmint, tops ...... 25 dues. Star apple ...... 7 .0 Starfruit ...... 0 .90 (a) General. (1) Tolerances are estab- Strawberry ...... 1 .5 lished for residues of bifenazate (1- Sugar apple ...... 1 .6 methylethyl 2-(4-methoxy[1,1′- Vegetable, cucurbit, group 9 ...... 0.75 biphenyl]-3-yl)hydrazinecarboxylate) Vegetable, fruiting, group 8–10 ...... 4 .0 Vegetable, legume, edible-podded, subgroup 6A 6.0 including its metabolites and Vegetable, tuberous and corm, subgroup 1C ..... 0.10 degradates, in or on the commodities Wax jambu ...... 0 .90 listed in the following table. Compli- ance with the tolerance levels specified (2) Tolerances are established for res- are to be determined by measuring idues of bifenazate (1-methylethyl 2-(4- only the sum of bifenazate and its me- methoxy[1,1′-biphenyl]-3-yl) tabolite, diazinecarboxylic acid, 2-(4- hydrazinecarboxylate) including its methoxy-[1,1′-biphenyl]-3-yl), 1- metabolites and degradates, in or on methylethyl ester, (calculated as the the commodities listed in the following stoichiometric equivalent of table. Compliance with the tolerance bifenazate) in or on the following food levels specified are to be determined by commodities: measuring only the sum of bifenazate

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and its metabolites diazinecarboxylic in or on the commodities in the table acid, 2-(4-methoxy-[1,1′-biphenyl]-3-yl), below. Compliance with the tolerance 1-methylethyl ester; 1,1′-biphenyl, 4-ol; levels specified below is to be deter- and 1,1′-biphenyl, 4-oxysulfonic acid mined by measuring only the combined (calculated as the stoichiometric residues of tepraloxydim, (2-[1-[[[(2E)-3- equivalent of bifenazate) in or on the chloro-2-propen-1-yl]oxy]imino]propyl]- following food commodities: 3-hydroxy-5-(tetrahydro-2H-pyran-4-yl)- 2-cyclohexen-1-one) and its metabolites Parts per mil- Commodity lion convertible to GP (3-(tetrahydropyran- 4-yl)pentane-1,5-dioic acid) and OH–GP Cattle, meat ...... 0.02 (3-hydroxy-3-(tetrahydropyran-4- Cattle, meat byproducts ...... 0.02 Goat, meat ...... 0.02 yl)pentane-1,5-dioic acid), calculated as Goat, meat byproducts ...... 0.02 tepraloxydim, in or on the commod- Hog, meat ...... 0.02 ities. Hog, meat byproducts ...... 0.02 Horse, meat ...... 0.02 Parts per Horse, meat byproducts ...... 0.02 Commodity million Milk ...... 0.02 Sheep, meat ...... 0.02 Cotton, undelinted seed ...... 0 .2 Sheep, meat byproducts ...... 0.02 Cotton, gin byproducts ...... 3 .0 Flax, seed ...... 0 .10 Grain, aspirated fraction ...... 1200.0 (b) Section 18 emergency exemptions. Pea and bean, dried shelled, except soybean, [Reserved] subgroup 6C 1 ...... 0 .10 (c) Tolerances with regional registra- Soybean, seed ...... 6 .0 tions. Tolerances with regional reg- Soybean, hulls ...... 8 .0 Sunflower subgroup 20B 1 ...... 0.20 istration, as defined in § 180.1(l), are es- 1 There are no U.S. registrations for commodities in this tablished for residues of bifenazate (1- subgroup. methylethyl 2-(4-methoxy[1,1′- biphenyl]-3-yl)hydrazinecarboxylate) (2) Tolerances are established for res- including its metabolites and idues of tepraloxydim, including its degradates, in or on the commodities metabolites and degradates, in or on listed in the following table. Compli- the commodities in the table below. ance with the tolerance levels specified Compliance with the tolerance levels are to be determined by measuring specified below is to be determined by only the sum of bifenazate and its me- measuring only the combined residues tabolite, diazinecarboxylic acid, 2-(4- of tepraloxydim (2-[1-[[[(2E)-3-chloro-2- methoxy-[1,1′-biphenyl]-3-yl), 1- propen-1-yl]oxy]imino]propyl]-3-hy- methylethyl ester, (calculated as the droxy-5-(tetrahydro-2H-pyran-4-yl)-2- stoichiometric equivalent of cyclohexen-1-one) and its metabolites bifenazate) in or on the following food convertible to GP (3-(tetrahydropyran- commodities: 4-yl)pentane-1,5-dioic acid), OH–GP (3- hydroxy-3-(tetrahydropyran-4- Commodity Parts per yl)pentane-1,5-dioic acid), and GL (3-(2- million oxotetrahydropyran-4-yl)-1,5-dioic Timothy, forage ...... 200 acid), calculated as tepraloxydim, in or Timothy, hay ...... 150 on the commodities.

(d) Indirect or inadvertent residues. Commodity Parts per [Reserved] million Cattle, fat ...... 0.15 [66 FR 34569, June 29, 2001] Cattle, kidney ...... 0 .50 EDITORIAL NOTE: For FEDERAL REGISTER ci- Cattle, meat ...... 0 .20 tations affecting § 180.572, see the List of CFR Cattle, meat byproducts, except kidney ...... 0.20 Egg ...... 0 .20 Sections Affected, which appears in the Goat, fat ...... 0 .15 Finding Aids section of the printed volume Goat, kidney ...... 0 .50 and at www.fdsys.gov. Goat, meat ...... 0.20 Goat, meat byproducts, except kidney ...... 0 .20 § 180.573 Tepraloxydim; tolerances for Hog, fat ...... 0 .15 Hog, kidney ...... 0.50 residues. Hog, meat ...... 0 .20 (a) General. (1) Tolerances are estab- Hog, meat byproducts, except kidney ...... 0 .20 Horse, fat ...... 0 .15 lished for residues of tepraloxydim, in- Horse, kidney ...... 0 .50 cluding its metabolites and degradates, Horse, meat ...... 0 .20

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Parts per Expiration/ Commodity million Commodity Parts per revocation million date Horse, meat byproducts, except kidney ...... 0 .20 Milk ...... 0.10 Grain, aspirated fraction .... 1200.0 12/31/18 Poultry, fat ...... 0.30 Pea and bean, dried Poultry, liver ...... 1 .00 shelled, except soybean, Poultry, meat ...... 0 .20 subgroup 6C 1 ...... 0.10 12/31/18 Poultry, meat byproducts, except liver ...... 0 .20 Soybean, seed ...... 6.0 12/31/18 Sheep, fat ...... 0 .15 Soybean, hulls ...... 8.0 12/31/18 Sheep, kidney ...... 0.50 Sunflower subgroup 20B 1 0.20 12/31/18 Sheep, meat ...... 0.20 1 Sheep, meat byproducts, except kidney ...... 0 .20 There are no U.S. registrations for commodities in this subgroup. (b) Section 18 emergency exemptions. (2) * * * [Reserved] Expiration/ (c) Tolerances with regional registra- Commodity Parts per revocation tions. A tolerance with regional reg- million date istration, as defined in § 180.1(l), is es- Cattle, fat ...... 0.15 12/31/18 tablished for residues of tepraloxydim, Cattle, kidney ...... 0.50 12/31/18 including its metabolites and Cattle, meat ...... 0.20 12/31/18 degradates, in or on the commodities Cattle, meat byproducts, except kidney ...... 0.20 12/31/18 in the table below. Compliance with Egg ...... 0.20 12/31/18 the tolerance levels specified below is Goat, fat ...... 0.15 12/31/18 to be determined by measuring only Goat, kidney ...... 0.50 12/31/18 the combined residues of tepraloxydim Goat, meat ...... 0.20 12/31/18 Goat, meat byproducts, ex- (2-[1-[[[(2E)-3-chloro-2-propen-1- cept kidney ...... 0.20 12/31/18 yl]oxy]imino]propyl]-3-hydroxy-5- Hog, fat ...... 0.15 12/31/18 (tetrahydro-2H-pyran-4-yl)-2-cyclo- Hog, kidney ...... 0.50 12/31/18 hexen-1-one) and its metabolites con- Hog, meat ...... 0.20 12/31/18 Hog, meat byproducts, ex- vertible to GP (3-(tetrahydropyran-4- cept kidney ...... 0.20 12/31/18 yl)pentane-1,5-dioic acid) and OH–GP Horse, fat ...... 0.15 12/31/18 (3-hydroxy-3-(tetrahydropyran-4- Horse, kidney ...... 0.50 12/31/18 Horse, meat ...... 0.20 12/31/18 yl)pentane-1,5-dioic acid), calculated as Horse, meat byproducts, tepraloxydim, in or on the commod- except kidney ...... 0.20 12/31/18 ities. Milk ...... 0.10 12/31/18 Poultry, fat ...... 0.30 12/31/18 Parts per Poultry, liver ...... 1.00 12/31/18 Commodity million Poultry, meat ...... 0.20 12/31/18 Poultry, meat byproducts, Canola, seed ...... 0 .50 except liver ...... 0.20 12/31/18 Sheep, fat ...... 0.15 12/31/18 (d) Indirect or inadvertent residues. Sheep, kidney ...... 0.50 12/31/18 Sheep, meat ...... 0.20 12/31/18 [Reserved] Sheep, meat byproducts, [66 FR 40150, Aug. 2, 2001, as amended at 72 except kidney ...... 0.20 12/31/18 FR 54588, Sept. 26, 2007; 76 FR 34885, June 15, 2011; 76 FR 82152, Dec. 30, 2011] * * * * * EFFECTIVE DATE NOTE: At 81 FR 34906, June 1, 2016, § 180.573 was amended by revising the (c) * * * tables in paragraphs (a)(1), (a)(2), and (c), ef- Expiration/ fective Nov. 28, 2016. For the convenience of Commodity Parts per revocation the user, the revised text is set forth as fol- million date lows: Canola, seed ...... 0.50 12/31/18 § 180.573 Tepraloxydim; tolerances for residues. (a) * * * * * * * * (1) * * * § 180.574 Fluazinam; tolerances for Expiration/ residues. Commodity Parts per revocation million date (a) General. (1) Tolerances are established for residues of fluazinam (3- Cotton, undelinted seed .... 0.2 12/31/18 Cotton, gin byproducts ...... 3.0 12/31/18 chloro-N-[3-chloro-2,6-dinitro-4- Flax, seed ...... 0.10 12/31/18 (trifluoromethyl)phenyl]-5-

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(trifluoromethyl)-2-pyridinamine), in- chloro-2-(2,6-diamino-3-chloro-a,a,a.- cluding its metabolites and degradates, trifluoro-p-toluidino)-5- in or on the commodities in the table (trifluoromethyl)pyridine), and their below. Compliance with the tolerance sulfamate conjugates. levels specified below is to be deter- Parts per mined by measuring only fluazinam. Commodity million

Commodity Parts per Cattle, fat ...... 0.05 million Cattle, meat byproducts ...... 0.05 Goat, fat ...... 0 .05 Apple ...... 2.0 Goat, meat byproducts ...... 0 .05 Apple, wet pomace ...... 5 .0 Horse, fat ...... 0 .05 Bushberry subgroup 13-07B ...... 7 .0 Horse, meat byproducts ...... 0 .05 Cabbage ...... 3 .0 Sheep, fat ...... 0 .05 Carrot, roots ...... 0.70 Sheep, meat byproducts ...... 0 .05 Ginseng ...... 4 .5 Lettuce, head ...... 0.02 Lettuce, leaf ...... 2 .0 (b) Section 18 emergency exemptions. Mayhaw ...... 2 .0 [Reserved] Onion, bulb, subgroup 3-07A ...... 0 .20 (c) Tolerances with regional registra- Pea and bean, dried shelled, except soybean, subgroup 6C, except pea ...... 0.02 tions. [Reserved] Pea and bean, succulent shelled, subgroup 6B, (d) Indirect or inadvertent residues. except pea ...... 0 .04 [Reserved] Peanut ...... 0 .02 Pepper/eggplant subgroup 8–10B ...... 0 .09 [66 FR 46738, Sept. 7, 2001, as amended at 67 Soybean, seed ...... 0 .01 FR 19130, Apr. 18, 2002; 72 FR 60260, Oct. 24, Soybean, hulls ...... 0 .05 Turnip, greens ...... 0.01 2007; 75 FR 26667, May 12, 2010; 76 FR 3029, Vegetable, Brassica leafy, group 5, except cab- Jan. 19, 2011; 77 FR 66729, Nov. 7, 2012; 81 FR bage ...... 0.01 20550, Apr. 8, 2016; 81 FR 34283, May 31, 2016] Vegetable, cucurbit, group 9 ...... 0.07 Vegetable, legume, edible-podded, subgroup § 180.575 Sulfuryl fluoride; tolerances 6A, except pea ...... 0.10 for residues. Vegetable, tuberous and corm, subgroup 1C ..... 0.02 (a)(1) General. Tolerances are estab- (2) Tolerances are established for res- lished for residues of sulfuryl fluoride idues of fluazinam, including its me- in or on the following commodities tabolites and degradates, in or on the from the postharvest fumigation with commodities in the table below. Com- sulfuryl fluoride for the control of in- pliance with the tolerance levels speci- sects: fied below is to be determined by meas- Parts per uring only fluazinam and its metabo- Commodity million lite AMGT (3-[[4-amino-3-[[3-chloro-5- (trifluoromethyl)-2-pyridinyl]amino]-2- All processed food commodities not otherwise nitro-6-(trifluoromethyl) phenyl]thio]- listed ...... 2 .0 Barley, bran, postharvest ...... 0 .05 2-(beta-D-glucopyranosyloxy) propionic Barley, flour, postharvest ...... 0.05 acid). Barley, grain, postharvest ...... 0 .1 Barley, pearled barley, postharvest ...... 0 .05 Parts per Cacao bean, roasted bean, postharvest ...... 0.2 Commodity million Cattle, meat, dried ...... 0.01 Cheese ...... 2 .0 Grape, wine 1 ...... 3 .0 Coconut, postharvest ...... 1 .0 Coffee, bean, roasted bean, postharvest ...... 1 .0 1 No US registration as of March 15, 2002. Corn, field, flour, postharvest ...... 0 .01 (3) Tolerances are established for res- Corn, field, grain, postharvest ...... 0 .05 Corn, field, grits, postharvest ...... 15.0 idues of fluazinam (3-chloro-N-[3- Corn, field, meal, postharvest ...... 0 .01 chloro-2,6-dinitro-4- Corn, pop, grain, postharvest ...... 0 .05 (trifluoromethyl)phenyl]-5- Cotton, undelinted seed, postharvest ...... 0.5 (trifluoromethyl)-2-pyridinamine), in- Egg, dried ...... 1 .0 Fruit, dried, postharvest ...... 0 .05 cluding its metabolites and degradates, Ginger, postharvest ...... 0 .5 in or on the commodities in the table Grain, aspirated fractions, postharvest ...... 0 .05 below. Compliance with the tolerance Herbs and spices group 19, postharvest ...... 0 .5 Hog, meat ...... 0 .02 levels specified below is to be deter- Milk, powdered ...... 2 .0 mined by measuring only fluazinam, Millet, grain, postharvest ...... 0.1 AMPA (2-(6-amino-3-chloro-a,a,a- Nut, pine, postharvest ...... 0.2 Nut, tree, Group 14, postharvest ...... 3 .0 trifluoro-2-nitro-p-toluidino)-3-chloro- Oat, flour, postharvest ...... 0 .05 5-(trifluoromethyl) pyridine), DAPA (3- Oat, grain, postharvest ...... 0 .1

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(d) Indirect or inadvertent residues. Commodity Parts per million [Reserved] Oat, groats/rolled oats, postharvest ...... 0 .1 [67 FR 43256, June 27, 2002, as amended at 74 Peanut, postharvest ...... 0 .5 FR 15880, Apr. 8, 2009; 76 FR 82157, Dec. 30, Pistachio, postharvest ...... 3 .0 2011] Rice, bran, postharvest ...... 0 .01 Rice, flour, postharvest ...... 0 .05 § 180.577 Bispyribac-sodium; toler- Rice, grain, postharvest ...... 0 .04 Rice, hulls, postharvest ...... 0.1 ances for residues. Rice, polished rice, postharvest ...... 0 .01 (a) General. Tolerances are estab- Rice, wild, grain, postharvest ...... 0 .05 lished for residues of the herbicide Sorghum, grain, grain, postharvest ...... 0.1 bispyribac-sodium, including its me- Triticale, grain, postharvest ...... 0 .1 Vegetable, legume, group 6, postharvest ...... 0.5 tabolites and degradates, in or on the Wheat, bran, postharvest ...... 0 .05 commodity listed below. Compliance Wheat, flour, postharvest ...... 0 .05 with the tolerance level specified below Wheat, germ, postharvest ...... 0 .02 is to be determined by measuring only Wheat, grain, postharvest ...... 0 .1 bispyribac-sodium, (2,6-bis[(4,6- Wheat, milled byproducts, postharvest ...... 0 .05 Wheat, shorts, postharvest ...... 0 .05 dimethoxy-2-pyrimidinyl)oxy]benzoic acid, sodium salt), in or on the fol- (2) To assure safe use of this pesticide lowing raw agricultural commodities: commodities treated with sulfuryl flu- Parts per oride must be aerated for at least 24 Commodity million hours prior to entering commerce. Fish, freshwater ...... 0 .01 (b) Section 18 emergency exemptions. Rice, grain ...... 0 .02 [Reserved] (c) Tolerances with regional registra- (b) Section 18 emergency exemptions. tion. [Reserved] [Reserved] (d) Indirect or inadvertant residues. (c) Tolerances with regional registra- [Reserved] tions. [Reserved] (d) Indirect or inadvertent residues. [67 FR 5740, Feb. 7, 2002, as amended at 69 FR [Reserved] 3257, Jan. 23, 2004; 70 FR 40908, July 15, 2005] [66 FR 48097, Sept. 18, 2001, as amended at 76 § 180.576 Cyhalofop-butyl; tolerances FR 5716, Feb. 2, 2011; 80 FR 72599, Nov. 20, for residues. 2015] (a) General. Tolerances are estab- § 180.578 Acetamiprid; tolerances for lished for residues of cyhalofop-butyl, residues. including its metabolites and (a) General. (1) Tolerances are estab- degradates, in or on the commodities lished for residues of the insecticide listed in the table below. Compliance acetamiprid (1E)-N-[(6-chloro-3- with the tolerance levels specified pyridinyl)methyl]-N’-cyano-N- below is to be determined by measuring methylethanimidamide, including its cyhalofop butyl [R-( + )-n-butyl-2-(4(4- metabolites and degradates, in or on cyano-2-fluorophenoxy)- the commodities in the table below as phenoxy)propionate], cyhalofop acid a result of the application of [R-( + )-2-(4(4-cyano-2-fluorophenoxy)- acetamiprid. Compliance with the tol- phenoxy)propionic acid], and the di- erance levels specified below is to be acid metabolite [(2R)-4-(4-(1- determined by measuring only carboxyethoxy)phenoxy)-3- acetamiprid in or on the following fluorobenzoic acid]. commodities. Parts per Commodity million Parts per Commodity million Rice, grain ...... 0 .40 Almond, hulls ...... 5 .0 Wild rice, grain ...... 0 .40 Asparagus ...... 0.80 Berry, low growing subgroups 13–07G ...... 0.60 (b) Section 18 emergency exemptions. Brassica, head and stem, subgroup 5A ...... 1 .20 [Reserved] Brassica, leafy greens, subgroup 5B ...... 15 Bushberry subgroup 13–07B ...... 1 .6 (c) Tolerances with regional registra- Caneberry subgroup 13–07A ...... 1.6 tions. [Reserved] Canola, seed ...... 0 .010

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Parts per Parts per Commodity million Commodity million

Citrus, dried pulp ...... 1 .20 Poultry, meat ...... 0 .010 Corn, sweet, forage ...... 15 Sheep, fat ...... 0 .20 Corn, sweet, kernel plus cob with husks re- Sheep, meat ...... 0.30 moved ...... 0 .01 Sheep, meat byproducts ...... 0 .70 Corn, sweet, stover ...... 30 Cotton, gin byproducts ...... 20 .0 (3) A tolerances of 0.01 ppm is estab- Cotton, undelinted seed ...... 0 .60 Fruit, citrus, group 10–10 ...... 1 .0 lished for residues of the insecticide Fruit, pome, group 11–10 ...... 1 .0 acetamiprid, including its metabolites Fruit, small, vine climbing, except fuzzy and degradates, in or on all food/feed kiwifruit, subgroup 13-07F ...... 0 .35 items (other than those covered by a Fruit, stone, group 12, except plum, prune ...... 1 .20 Grain, aspirated fractions ...... 5 .0 higher tolerance in paragraph (a)(1) or Mustard, seed ...... 0 .010 (a)(2) of this section as a result of the Nut, tree, group 14 ...... 0 .10 use on growing crops) as a result of the Onion, bulb, subgroup 3–07A ...... 0 .02 Onion, green, subgroup 3–07B ...... 4 .5 application of acetamiprid in food/feed Pea and bean, succulent shelled, subgroup 6B 0 .40 handling establishments. Compliance Pistachio ...... 0.10 with the 0.01 ppm tolerance level is to Plum, prune, dried ...... 0.40 be determined by measuring only Plum, prune, fresh ...... 0.20 Soybean, hulls ...... 0 .04 acetamiprid (1E)-N-[(6-chloro-3- Soybean, seed ...... 0 .03 pyridinyl)methyl]-N′-cyano-N- Tea, dried1 ...... 50.0 methylethanimidamide in or on the Tomato, paste ...... 0 .40 commodities. Turnip greens ...... 15 Vegetable, cucurbit, group 9 ...... 0.50 (b) Section 18 emergency exemptions. Vegetable, fruiting, group 8–10 ...... 0 .20 [Reserved] Vegetable, leafy, except brassica, group 4 ...... 3 .00 (c) Tolerances with regional registra- Vegetable, legume, edible podded, subgroup tions. Tolerances with regional reg- 6A ...... 0 .60 Vegetable, tuberous and corm, group 1 ...... 0 .01 istrations are established for residues of the insecticide acetamiprid (1E)-N- 1There are no U.S. registrations as of February 10, 2010, for the use of acetamiprid on dried tea. [(6-chloro-3-pyridinyl)methyl]-N′- cyano-N-methylethanimidamide, in- (2) Tolerances are established for res- cluding its metabolites and degradates, idues of the insecticide acetamiprid in or on the commodities in the table (1E)-N-[(6-chloro-3-pyridinyl)methyl]- below as a result of the application of ′-cyano- -methylethanimidamide, in- N N acetamiprid. Compliance with the tol- cluding its metabolites and degradates, erance levels specified below is to be in or on the commodities in the table determined by measuring only below as a result of the application of acetamiprid in or on the following acetamiprid. Compliance with the tol- commodities. erance levels specified below is to be determined by measuring acetamiprid Commodity Parts per and (1E)-N-[(6-chloro-3- million pyridinyl)methyl]-N′-cyano-N- Clover, forage ...... 0.30 ethanimidamide in or on the following Clover, hay ...... 2.0 commodities. (d) Indirect or inadvertent residues. Parts per [Reserved] Commodity million [67 FR 14659, Mar. 27, 2002, as amended at 68 Cattle, fat ...... 0.20 FR 52352, Sept. 3, 2003; 70 FR 19293, Apr. 13, Cattle, meat ...... 0 .30 2005; 72 FR 67262, Nov. 28, 2007; 73 FR 2811, Cattle, meat byproducts ...... 0.70 Egg ...... 0 .010 Jan. 16, 2008; 75 FR 6582, Feb. 10, 2010; 77 FR Goat, fat ...... 0 .20 18716, Mar. 28, 2012; 77 FR 43529, July 25, 2012; Goat, meat ...... 0.30 78 FR 36676, June 19, 2013; 80 FR 68778, Nov. 6, Goat, meat byproducts ...... 0 .70 2015] Hog, fat ...... 0 .10 Hog, meat ...... 0 .10 § 180.579 Fenamidone; tolerances for Hog, meat byproducts ...... 0 .20 residues. Horse, fat ...... 0 .20 Horse, meat ...... 0 .30 (a) General. (1) Tolerances are estab- Horse, meat byproducts ...... 0 .70 lished for residues of the fungicide, Milk ...... 0.30 Poultry, fat ...... 0.010 fenamidone, including its metabolites Poultry, liver ...... 0 .050 and degradates, in or on the following

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commodities. Compliance with the tolerance levels is to be determined by erance levels is to be determined by measuring only fenamidone (4H- measuring only fenamidone (4H- Imidazol-4-one, 3,5-dihydro-5-methyl-2- Imidazol-4-one, 3,5-dihydro-5-methyl-2- (methylthio)-5-phenyl-3 (phenylam- (methylthio)-5-phenyl-3 (phenylamino)- ino)-,(S)-), in or on the commodity: ,(S)-), in or on the commodities: Commodity Parts per Parts per million Commodity million Grape1 ...... 1 .0 Bean, succulent, except cowpea ...... 0 .80 1 Applicable to grapes grown East of the Rocky Mountains. Brassica, head and stem, subgroup 5A ...... 5 .0 Brassica, leafy greens, subgroup 5B ...... 55 (d) Indirect or inadvertent residues. Cilantro, leaves ...... 60 Tolerances are established for residues Cotton, gin byproducts ...... 0 .02 Cotton, undelinted seed ...... 0 .02 of the fungicide fenamidone, including Ginseng ...... 0 .80 its metabolites and degradates, in or Okra ...... 3.5 on the following commodities. Compli- Onion, bulb, subgroup 3–07A ...... 0 .20 Onion, green, subgroup 3–07B ...... 1 .5 ance with the tolerance levels is to be Pepper, nonbell ...... 3 .5 determined by measuring fenamidone Sunflower ...... 0 .02 (4H-Imidazol-4-one, 3,5-dihydro-5-meth- Tomato, paste ...... 2 .2 Tomato, puree ...... 2 .0 yl-2-(methylthio)-5-phenyl-3 Turnip, greens ...... 55 (phenylamino)-,(S)-), and its metabo- Vegetable, cucurbit, group 9 ...... 0.15 lite RPA 717879 (2,4-imidazolidinedione, Vegetable, fruiting, group 8, except nonbell pepper ...... 1 .0 5-methyl-5-phenyl), in or on the fol- Vegetable, leafy, except Brassica, group 4 ...... 60 lowing commodities when present Vegetable, root, except sugar beet, subgroup therein as a result of application of 1B, except radish ...... 0 .15 Vegetable, tuberous and corm, subgroup 1C ..... 0.02 fenamidone to the crops in paragraph (a)(1). (2) Tolerances are established for res- Parts per idues of the fungicide fenamidone, in- Commodity million cluding its metabolites and degradates, Grain, cereal, group 15, except rice ...... 0 .1 in or on the following commodities. Grain, cereal, forage, fodder and straw, group Compliance with the tolerance levels is 16, except rice ...... 0 .5 to be determined by measuring Soybean, forage ...... 0 .15 fenamidone (4H-Imidazol-4-one, 3,5- Soybean, hay ...... 0 .25 Soybean, seed ...... 0 .02 dihydro-5-methyl-2-(methylthio)-5- Strawberry ...... 0 .02 phenyl-3 (phenylamino)-,(S)-), and its metabolite RPA 717879 (2,4- [67 FR 60976, Sept. 27, 2002, as amended at 69 imidazolidinedione, 5-methyl-5-phenyl), FR 58066, Sept. 29, 2004; 71 FR 55293, Sept. 22, in or on the commodities: 2006; 72 FR 60272, Oct. 24, 2007; 74 FR 34257, July 15, 2009; 76 FR 34885, June 15, 2011; 76 FR Parts per Commodity million 70895, Nov. 16, 2011; 77 FR 32401, June 1, 2012; 79 FR 13882, Mar. 12, 2014] Cattle, fat ...... 0.10 Cattle, meat ...... 0 .10 § 180.580 Iodosulfuron-Methyl-Sodium; Cattle, meat byproducts ...... 0.10 tolerances for residues. Goat, fat ...... 0 .10 Goat, meat ...... 0.10 (a) General. Tolerances are estab- Goat, meat byproducts ...... 0 .10 lished for residues of the herbicide Milk ...... 0.02 Sheep, fat ...... 0 .10 Iodosulfuron-Methyl-Sodium (methyl 4- Sheep, meat ...... 0.10 iodo-2-[3-(4-methoxy-6-methyl-1,3,5 Sheep, meat byproducts ...... 0 .10 triazin-2-yl)ureidosulfonyl]benzoate, sodium salt) in or on the following com- (b) Section 18 emergency exemptions. modities: [Reserved] (c) Tolerances with regional registra- Commodity Parts per tions. A tolerance with regional reg- million istration as defined in § 180.1(l) is estab- Corn, field, forage ...... 0 .05 lished for residues of the fungicide Corn, field, grain ...... 0 .03 fenamidone, including its metabolites Corn, field, stover ...... 0 .05 Wheat, forage ...... 0 .10 and degradates, in or on the following Wheat, grain ...... 0 .02 commodities. Compliance with the tol- Wheat, hay ...... 0 .05

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Parts per Parts per Commodity million Commodity million

Wheat, straw ...... 0 .05 Alfalfa, hay ...... 30 Almond, hulls ...... 7 .0 (b) Section 18 emergency exemptions. Apple, wet pomace ...... 8 .0 Artichoke, globe ...... 3.0 [Reserved] Avocado ...... 0 .6 (c) Tolerances with regional registra- Banana ...... 0.04 tions. [Reserved] Barley, grain ...... 1 .4 Barley, hay ...... 25 (d) Indirect or inadvertent residues. Barley, straw ...... 6 .0 [Reserved] Bean, succulent shelled ...... 0 .5 Beet, sugar, dried pulp ...... 1 .0 [67 FR 57532, Sept. 11, 2002, as amended at 74 Beet, sugar, roots ...... 0 .2 FR 23644, May 20, 2009] Beet, sugar, tops ...... 8.0 Berry, low growing, subgroup 13–07G, except § 180.581 Iprovalicarb; tolerances for cranberry ...... 1.2 residues. Brassica, head and stem, subgroup 5A ...... 5 .0 Brassica, leafy greens, subgroup 5B ...... 16 .0 (a) General. Tolerances are estab- Bushberry subgroup 13–07B ...... 4 .0 lished for residues of iprovalicarb, [2- Caneberry subgroup 13–07A ...... 4.0 Canistel ...... 0 .6 methyl-1[[[(1S)-(4-methylphenyl) ethyl] Citrus, dried pulp ...... 12 .5 amino]carbonyl] propyl]carbamic acid Citrus, oil ...... 9.0 methylethylester, in or on the fol- Coffee, green bean ...... 1 0 .3 lowing commodities. Corn, field, forage ...... 5 .0 Corn, field, grain ...... 0 .1 Parts per Corn, field, refined oil ...... 0 .2 Commodity million Corn, field, stover ...... 17 .0 Corn, pop, grain ...... 0.1 Grape 1 ...... 2 .0 Corn, pop, stover ...... 17.0 Tomato 1 ...... 1.0 Corn, sweet, forage ...... 5 .0 Corn, sweet, kernel plus cob with husks re- 1 There is no U.S. registration as of September 1, 2005. moved ...... 0 .04 (b) Section 18 emergency exemptions. Corn, sweet, stover ...... 23.0 Cotton, gin byproducts ...... 30 [Reserved] Dill, seed ...... 40 (c) Tolerances with regional registra- Endive, belgium ...... 4 .0 tions. [Reserved] Fruit, citrus, group 10–10 ...... 2 .0 (d) Indirect or inadvertent residues. Fruit, pome, group 11–10 ...... 1 .5 Fruit, small vine climbing, except fuzzy [Reserved] kiwifruit, subgroup 13–07F ...... 2.0 Fruit, stone, group 12–12 ...... 2 .5 [67 FR 54359, Aug. 22, 2002, as amended at 70 Grain, aspirated fractions ...... 2 .5 FR 55281, Sept. 21, 2005] Grape, raisin ...... 7 .0 Grass, forage ...... 10 § 180.582 Pyraclostrobin; tolerances Grass, hay ...... 4 .5 for residues. Grass, seed screenings ...... 27 Grass, straw ...... 14 (a) General. (1) Tolerances are estab- Herb subgroup 19A ...... 40 lished for residues of the fungicide Hop, dried cones ...... 23 .0 pyradostrobin, including its metabo- Mango ...... 0.6 Nut, tree, group 14–12, except pistachio ...... 0 .04 lites and degradates, in or on the com- Oat, grain ...... 1 .2 modities in the table below. Compli- Oat, hay ...... 18 ance with the tolerance levels specified Oat, straw ...... 15 below is to be determined by measuring Oilseed group 20 ...... 0 .45 Papaya ...... 0 .6 only the sum of pyraclostrobin (car- Pea, succulent ...... 0 .2 bamic acid, [2-[[[ 1-(4-chlorophenyl)-1H- Pea and bean, dried shelled, except soybean, pyrazol-3-yl]oxy] meth- subgroup 6C ...... 0 .5 yl]phenyl]methoxy-, methyl ester) and Peanut ...... 0 .05 Peanut, refined oil ...... 0.1 its desmethoxy metabolite (methyl-N- Peppermint, tops ...... 8 .0 [[[1-(4-chlorophenyl)-1H-pyrazol-3- Persimmon ...... 3 .0 yl]oxy]methyl] phenylcarbamate), cal- Pistachio ...... 0.7 Radish, tops ...... 16 culated as the stoichiometric equiva- Rye, grain ...... 0.04 lent of pyraclostrobin, in or on the Rye, straw ...... 0 .5 commodity. Sapodilla ...... 0 .6 Sapote, black ...... 0 .6 Parts per Sapote, mamey ...... 0 .6 Commodity million Sorghum, grain, forage ...... 5.0 Sorghum, grain, grain ...... 0 .60 Alfalfa, forage ...... 10 Sorghum, grain, stover ...... 0 .80

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pyraclostrobin, (carbamic acid, [2-[[[1- Commodity Parts per million (4-chlorophenyl)-1H-pyrazol-3- Soybean, forage ...... 11 yl]oxy]methyl] phenyl]methoxy-, Soybean, hay ...... 14 methyl ester) and its desmethoxy me- Soybean, hulls ...... 0 .06 Soybean, seed ...... 0 .04 tabolite (methyl-N-[[[1-(4- Spearmint, tops ...... 8 .0 chlorophenyl) pyrazol-3-yl]oxy]o- Star apple ...... 0 .6 tolyl]carbamate) in connection with Sugarcane, cane ...... 0.20 Vegetable, bulb, group 3–07 ...... 0 .9 use of the pesticide under section 18 Vegetable, cucurbit, group 9 ...... 0.5 emergency exemptions granted by Vegetable, foliage of legume, except soybean, EPA. The time-limited tolerance will subgroup 7A ...... 25 .0 Vegetable, fruiting, group 8–10 ...... 1 .4 expire and is revoked on the date speci- Vegetable, leafy, except brassica, group 4 ...... 29.0 fied in the following table. Vegetable, leaves of root and tuber, group 2, except sugar beet ...... 16 .0 Expiration/ Vegetable, legume, edible podded, subgroup Commodity Parts per revocation 6A ...... 0 .5 million date Vegetable, root, except sugar beet, subgroup 1B ...... 0 .4 Endive, belgium ...... 11.0 12/31/13 Vegetable, tuberous and corm, subgroup 1C ... 0.04 Vegetables, foliage of legume, group 7 ...... 25 Wheat, grain ...... 0 .02 (c) Tolerances with regional registra- Wheat, hay ...... 6 .0 tions. [Reserved] Wheat, straw ...... 8 .5 (d) Indirect or inadvertent residues. [Reserved] (2) Tolerances are established for combined residues of the fungicide [67 FR 60901, Sept. 27, 2002, as amended at 69 pyraclostrobin carbamic acid, [2-[[[1-(4- FR 63100, Oct. 29, 2004; 71 FR 17021, Apr. 5, chlorophenyl)-1H-pyrazol-3- 2006; 72 FR 54569, Sept. 26, 2007; 73 FR 15431, yl]oxy]methyl]phenyl]methoxy-, meth- Mar. 24, 2008; 73 FR 21842, Apr. 23, 2008; 73 FR yl ester and its metabolites convertible 44167, July 30, 2008; 74 FR 11499, Mar. 18, 2009; to 1-(4-chlorophenyl)-1H-pyrazol-3-ol 74 FR 51496, Oct. 7, 2009; 75 FR 770, Jan. 6, and 1-(4-chloro-2-hydroxyphenyl)-1H- 2010; 75 FR 42329, July 21, 2010; 75 FR 80346, Dec. 22, 2010; 76 FR 81396, Dec. 28, 2011; 78 FR pyrazol-3-ol, expressed as parent com- 53046, Aug. 28, 2013; 80 FR 19238, Apr. 10, 2015] pound, in or on the following raw agricultural commodities. § 180.583 Triticonazole; tolerances for residues. Commodity Parts per million (a) General. Tolerances are estab- Cattle, fat ...... 0.1 lished for residues of the fungicide Cattle, liver ...... 1 .5 triticonazole, (1RS)-(E)-5-[(4- Cattle, meat ...... 0 .1 Cattle, meat byproducts, except liver ...... 0 .2 chlorophenyl)methylene]-2,2-dimethyl- Goat, fat ...... 0 .1 1-(1H-1,2,4-triazol-1- Goat, liver ...... 1.5 ylmethyl)cyclopentanol, from the Goat, meat ...... 0.1 Goat, meat byproducts, except liver ...... 0 .2 treatment of seed prior to planting in Hog, fat ...... 0 .1 or on raw agricultural commodities as Hog, liver ...... 1 .5 follows: Hog, meat ...... 0 .1 Hog, meat byproducts, except liver ...... 0 .2 Parts per Horse, fat ...... 0 .1 Commodity million Horse, liver ...... 0 .1 Horse, meat ...... 0 .1 Grain, cereal, forage, fodder and straw, group Horse, meat byproducts, except liver ...... 0 .2 16, except rice ...... 0 .10 Milk ...... 0.1 Grain, cereal, group 15, except rice ...... 0 .01 Poultry, eggs ...... 0 .10 Poultry, fat ...... 0.10 Poultry, meat ...... 0 .10 (b) Section 18 emergency exemptions. Poultry, meat byproducts ...... 0.10 [Reserved] Sheep, fat ...... 0 .1 Sheep, liver ...... 1.5 (c) Tolerances with regional registra- Sheep, meat ...... 0.1 tions. [Reserved] Sheep, meat byproducts, except liver ...... 0 .2 (d) Indirect or inadvertent residues. [Reserved] (b) Section 18 emergency exemptions. A time-limited tolerance is established [67 FR 60959, Sept. 27, 2002, as amended at 75 for combined residues of the fungicide FR 4288, Jan. 27, 2010]

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§ 180.584 Tolylfluanid; tolerances for Commodity Parts per residues. million (a) General. Tolerances are estab- Almond, hulls ...... 0 .02 lished for residues of tolylfluanid, 1,1- Cattle, fat ...... 0.03 dichloro-N-[(dimethylamino)-sulfonyl]- Cattle, meat ...... 0 .03 Cattle, meat byproducts ...... 0.03 1-fluoro-N-(4- Corn, field, forage ...... 0 .01 methylphenyl)methanesulfenamide in Corn, field, grain ...... 0 .01 or on the following commodities. Corn, field, stover ...... 0 .01 Cotton, gin byproducts ...... 1 .5 Commodity Parts per Cotton, undelinted seed ...... 0 .04 million Fruit, pome, group 11–10 ...... 0 .01 Fruit, stone, group 12 ...... 0 .01 Apple 1 ...... 5.0 Grape 1 ...... 11 Goat, fat ...... 0 .03 Hop, dried cones 1 ...... 30 Goat, meat ...... 0.03 Tomato 1 ...... 2.0 Goat, meat byproducts ...... 0 .03 Grape ...... 0 .01 1 No U.S. registration as of August 31, 2002. Grass, forage, group 17 ...... 1 .0 (b) Section 18 emergency exemptions. Grass, hay, group 17 ...... 1 .4 [Reserved] Horse, fat ...... 0 .03 Horse, meat ...... 0 .03 (c) Tolerances with regional registra- Horse, meat byproducts ...... 0 .03 tions. [Reserved] Milk ...... 0.03 (d) Indirect or inadvertent residues. Nut, tree, group 14 ...... 0 .01 [Reserved] Olive ...... 0 .01 Peanut ...... 0 .01 [67 FR 60141, Sept. 25, 2002] Peanut, hay ...... 0.07 Pistachio ...... 0.01 § 180.585 Pyraflufen-ethyl; tolerances Pomegranate ...... 0 .01 for residues. Potato ...... 0 .02 Sheep, fat ...... 0 .03 (a) General. Tolerances are estab- Sheep, meat ...... 0.03 lished for residues of the herbicide, Sheep, meat byproducts ...... 0 .03 pyraflufen-ethyl, including its metabo- Soybean, forage ...... 0 .05 lites and degradates, in the commod- Soybean, hay ...... 0 .10 Soybean, seed ...... 0 .01 ities in the table below. Compliance Wheat, forage ...... 0 .02 with the plant commodity tolerance Wheat, grain ...... 0 .01 levels specified in the table is to be de- Wheat, hay ...... 0 .01 termined by measuring only the sum of Wheat, straw ...... 0 .01 the parent pyraflufen-ethyl, ethyl 2-[2- chloro-5-(4-chloro-5-difluoromethoxy)- (b) Section 18 emergency exemptions. 1-methyl-1H-pyrazol-3-yl]-4- [Reserved] fluorophenoxy] acetate, and its acid (c) Tolerances with regional registra- metabolite, E–1, 2-chloro-5-(4-chloro-5- tions. [Reserved] difluoromethoxy-1-methyl-1H-pyrazol- (d) Indirect or inadvertent residues. 3-yl)-4-fluorophenoxyacetic acid, cal- [Reserved] culated as the stoichiometric equiva- [68 FR 23055, Apr. 30, 2003, as amended at 68 lent of pyraflufen-ethyl in or on the FR 27739, May 21, 2003; 69 FR 26312, May 12, commodity. Compliance with the live- 2004; 73 FR 51743, Sept. 5, 2008; 76 FR 31484, stock commodity tolerance levels spec- June 11, 2011; 77 FR 75861, Dec. 26, 2012; 78 FR ified in the table is to be determined by 13263, Feb. 27, 2013] measuring only the sum of the parent pyraflufen-ethyl, ethyl 2-[2-chloro-5-(4- § 180.586 Clothianidin; tolerances for chloro-5-difluoromethoxy)-1-methyl- residues. 1H-pyrazol-3-yl]-4-fluorophenoxy] ace- (a) General. (1) Tolerances are estab- tate and its acid metabolites: E–1, 2- lished for residues of the insecticide chloro-5-(4-chloro-5-difluoromethoxy-1- clothianidin, including its metabolites methyl-1H-pyrazol-3-yl)-4- and degradates. Compliance with the fluorophenoxyacetic acid, and E–9, 2- tolerance levels specified below is to be chloro-5-(4-chloro-5-difluoromethoxy- determined by measuring only 1H-pyrazol-3-yl)-4-fluorophenoxyacetic clothianidin, (E)-N-[(2-Chloro-5- acid, both calculated as the stoichio- thiazolyl)methyl]-N′ -methyl-N″ metric equivalent of pyraflufen-ethyl -nitroguanidine, in or on the following in or on the commodity. raw agricultural commodities:

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tions. This tolerance expires on the Commodity Parts per million date specified in the table. Almond, hulls ...... 1 .5 Parts per Expiration Beet, sugar, dried pulp ...... 0 .03 Commodity million date Beet, sugar, molasses ...... 0 .05 Beet, sugar, roots ...... 0 .02 Fruit, citrus, group 10–10 ...... 0.07 12/31/17 Berry, low-growing, subgroup 13-07H, except strawberry ...... 0.01 Canola, seed ...... 0 .01 (c) Tolerances with regional registra- Cotton, gin byproducts ...... 4 .5 tions. [Reserved] Cotton, undelinted seed ...... 0 .20 (d) Indirect and inadvertant residues. Fig ...... 0 .05 Fruit, pome ...... 1.0 Tolerances are established for the indi- Grain, cereal, forage, fodder and straw, group rect or inadvertent residues of the in- 16, except rice, forage ...... 0 .35 secticide clothianidin, including its Grain, cereal, forage, fodder and straw, group metabolites and degradates. Compli- 16, except rice, hay ...... 0 .07 Grain, cereal, forage, fodder and straw, group ance with the tolerance levels specified 16, except rice, stover ...... 0 .1 below is to be determined by measuring Grain, cereal, forage, fodder and straw, group only clothianidin, (E)-1-(2-chloro-1,3- 16, except rice, straw ...... 0.05 Grain, cereal, group 15, except rice ...... 0 .01 thiazol-5-ylmethyl)-3-methyl-2- Grape ...... 0 .60 nitroguanidine, in or on the following Milk ...... 0.01 raw agricultural commodities when Mustard, seed ...... 0 .01 Nut, tree, group 14 ...... 0 .01 present therein as a result of the appli- Peach ...... 0 .80 cation of clothianidin to crops listed in Pepper ...... 0 .80 paragraph (a) of this section: Pomegranate ...... 0 .20 Potato, chips ...... 0 .6 Parts per Potato, granules/flakes ...... 1 .5 Commodity million Rice, grain ...... 0 .01 Soybean, seed ...... 0 .02 Animal feed, nongrass, group 18 ...... 0 .02 Tea, dried 1 ...... 70 Grass, forage, fodder and hay, group 17 ...... 0 .02 Vegetable, brassica, leafy, group 5 ...... 1.9 Soybean, forage ...... 0 .02 Vegetable, bulb, group 3-07 ...... 0 .45 Soybean, hay ...... 0 .02 Vegetable, cucurbit, group 9 ...... 0.06 Vegetable, fruiting, group 8, except pepper ...... 0.20 Vegetable, leafy, except brassica, group 4 ...... 3 .0 [74 FR 65028, Dec. 9, 2009, as amended at 76 Vegetable, root, except sugar beet, subgroup FR 7718, Feb. 11, 2011; 76 FR 25246, May 4, 1B ...... 0 .8 2011; 76 FR 34886, June 15, 2011; 77 FR 52252, Vegetable, tuberous and corm, subgroup 1C ..... 0.3 Aug. 29, 2012; 78 FR 19136, Mar. 29, 2013; 80 FR 1 No U.S. registrations. 10007, Feb. 25, 2015] (2) Time-limited tolerances are estab- § 180.587 Famoxadone; tolerance for lished for residues of the insecticide residues. clothianidin, including its metabolites (a) General. Tolerances are estab- and degradates. Compliance with the lished for residues of the fungicide tolerance levels specified below is to be famoxadone (3-anilino-5-methyl-5-(4- determined by measuring only phenoxyphenyl)-1,3-oxazolidine-2,4- clothianidin, (E)-1-(2-chloro-1,3-thiazol- dione) in or on the following commod- 5-ylmethyl)-3-methyl-2-nitroguanidine, ities: in or on the following raw agricultural commodity: Parts per Commodity million Expiration/ Commodity Parts per revocation Caneberry subgroup 13–07A ...... 10 million date Cattle, fat ...... 0.02 Cattle, liver ...... 0 .05 Rice, seed ...... 0.01 6/23/12 Cilantro, leaves ...... 25 Goat, fat ...... 0 .02 (b) Section 18 emergency exemptions. A Goat, liver ...... 0.05 Grape, raisin 1 ...... 4 .0 time-limited tolerance specified in the Hop, dried cone ...... 80 following table is established for resi- Horse, fat ...... 0 .02 dues of clothianidin, (E)-N-[(2-chloro-5- Horse, liver ...... 0 .05 Milk, fat (reflecting negligible residues in whole thiazolyl)methyl]-N’-methyl-N’’- milk) ...... 0 .06 nitroguanidine, in or on the specified Onion, bulb, subgroup 3–07A ...... 0 .45 agricultural commodity, resulting Onion, green, subgroup 3–07B ...... 40 Potato ...... 0 .02 from use of the pesticide pursuant to Sheep, fat ...... 0 .02 FIFRA section 18 emergency exemp- Sheep, liver ...... 0.05

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(d) Indirect or inadvertent residues. Commodity Parts per million [Reserved] Spinach ...... 50 [68 FR 55858, Sept. 29, 2003, as amended at 70 Tomato ...... 1.0 FR 4032, Jan. 28, 2005; 71 FR 50354, Aug. 25, Vegetable, cucurbit, group 9 ...... 0.30 2006; 74 FR 14743, Apr. 1, 2009; 78 FR 57280, Vegetable, fruiting, group 8, except tomato ...... 4 .0 Vegetable, leafy, except Brassica, group 4, ex- Sept. 18, 2013] cept spinach ...... 25 § 180.589 Boscalid; tolerances for resi- 1 There are no U.S. registrations as of May 15, 2003. dues. (b) Section 18 emergency exemptions. (a) General. (1) Tolerances are estab- [Reserved] lished for residues of the fungicide (c) Tolerances with a regional registra- boscalid, including its metabolites and tions. Tolerances with a regional reg- degradates, in or on the commodities istration as defined in § 180.1(l) are es- listed below. Compliance with the tol- tablished for the residues of the fun- erance levels specified below is to be gicide famoxadone, 3-anilino-5-methyl- determined by measuring only 5-(4-phenoxyphenyl)-1,3-oxazolidine-2,4- boscalid, 3-pyridinecarboxamide, 2- dione) in or on the raw agricultural chloro-N-(4′-chloro[1,1′-biphenyl]-2-yl), commodities: in or on the following raw agricultural commodities: Parts per Commodity million Commodity Parts per Grape ...... 2 .5 million Alfalfa, forage ...... 30.0 (d) Indirect or inadvertant residues. Alfalfa, hay ...... 65.0 [Reserved] Almond, hulls ...... 17 Apple, wet pomace ...... 10 [68 FR 39471, July 2, 2003, as amended at 72 Artichoke, globe ...... 6.0 FR 28881, May 23, 2007; 74 FR 9364, Mar. 4, Avocado ...... 1 .5 Banana, import 1 ...... 0 .40 2009; 76 FR 34885, June 15, 2011] Berry, low growing, subgroup 13–07G, except cranberry ...... 4.5 § 180.588 Quinoxyfen; tolerances for Brassica, head and stem, subgroup 5A ...... 3 .0 residues. Brassica, leafy greens, subgroup 5B ...... 18 .0 Bushberry subgroup 13–07B ...... 13 .0 (a) General. Tolerances are estab- Caneberry subgroup 13–07A ...... 10.0 lished for residues of the fungicide Canistel ...... 1 .5 quinoxyfen, including its metabolites Canola, refined oil ...... 5 .0 Citrus, dried pulp ...... 4 .5 and degradates, in or on the commod- Citrus, oil ...... 85.0 ities in the following table. Compliance Coffee, green bean, import 1 ...... 0 .05 with the tolerance levels specified in Cotton, gin byproducts ...... 55 .0 Cucumber ...... 0 .5 the following table is to be determined Dill, seed ...... 100 by measuring only quinoxyfen (5,7- Endive, Belgium ...... 6 .0 dichloro-4-(4-fluorophenoxy)quinoline). Fruit, citrus, group 10–10 ...... 2 .0 Fruit, pome, group 11–10 ...... 3 .0 Parts per Fruit, small vine climbing, except fuzzy kiwifruit, Commodity million subgroup 13–07F ...... 5 .0 Fruit, stone, group 12–12 ...... 3 .5 Artichoke, globe ...... 1.4 Grain, aspirated fractions ...... 3 .0 Berry, low growing, subgroup 13–07G ...... 1 .0 Grape, raisin ...... 8 .5 Fruit, small vine climbing, except fuzzy kiwifruit, Herb subgroup 19A ...... 150 subgroup 13–07F ...... 2 .0 Hop, dried cones ...... 35 Fruit, stone, group 12 ...... 0 .70 Leaf petioles subgroup 4B ...... 45 Hop, dried cones ...... 3 .0 Leafy greens subgroup 4A, except head lettuce Gourd, edible ...... 0 .20 and leaf lettuce ...... 60 Lettuce, head ...... 7.0 Lettuce, head ...... 6.5 Lettuce, leaf ...... 19 Lettuce, leaf ...... 11 .0 Melon, subgroup 9A ...... 0 .08 Mango ...... 1.5 Nut, tree, group 14–12 ...... 0 .70 Pumpkin ...... 0.20 Oilseed group 20 ...... 3 .5 Squash, winter ...... 0 .20 Papaya ...... 1 .5 Vegetable, fruiting, group 8–10 ...... 1 .7 Pea and bean, dried shelled, except soybean, subgroup 6C, except cowpea, field pea and (b) Section 18 emergency exemptions. grain lupin ...... 2 .5 [Reserved] Pea and bean, succulent shelled, subgroup 6B, except cowpea ...... 0 .6 (c) Tolerances with regional registra- Peanut ...... 0 .05 tions. [Reserved] Peanut, meal ...... 0 .15

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the pesticide under section 18 emer- Commodity Parts per million gency exemptions granted by EPA. Peanut, refined oil ...... 0.15 Compliance with the tolerance level Peppermint, tops ...... 30 .0 specified below is to be determined by Persimmon ...... 8 .0 Sapodilla ...... 1 .5 measuring only boscalid, 3- Sapote, black ...... 1 .5 pyridinecarboxamide, 2-chloro-N-(4′- Sapote, mamey ...... 1 .5 chloro[1,1′-biphenyl]-2-yl). This toler- Soybean, hulls ...... 0 .2 Soybean, seed ...... 0 .1 ance will expire and is revoked on the Soybean, vegetable ...... 2 .0 date specified in the following table: Spearmint, tops ...... 30 .0 Star apple ...... 1 .5 Expiration/ Turnip, greens ...... 40.0 Parts per Commodity million revocation Vegetable, bulb, group 3–07 ...... 5 .0 date Vegetable, cucurbit, group 9, except cucumber 1.6 Vegetable, fruiting, group 8–10 ...... 3 .0 Endive, Belgian ...... 16 12/31/13 Vegetable, legume, edible podded, subgroup 6A 1 .6 Vegetable, root, subgroup 1A, except sugar beet, garden beet, radish, and turnip ...... 1.0 (c) Tolerances with regional registra- Vegetable, tuberous and corm, subgroup 1C ..... 0.05 tion. [Reserved] 1No US registrations as of September 16, 2009. (d) Indirect or inadvertent residues. Tolerances are established for the indi- (2) Tolerances are established for res- rect or inadvertent residues of the fun- idues of the fungicide boscalid, includ- gicide boscalid, including its metabo- ing its metabolites and degradates, in or on the commodities listed below. lites and degradates, in or on the com- Compliance with the tolerance levels modities listed below. Compliance with specified below is to be determined by the tolerance levels specified below is measuring only the sum of boscalid, 3- to be determined by measuring only pyridinecarboxamide, 2-chloro-N-(4′- boscalid, 3-pyridinecarboxamide, 2- chloro[1,1′-biphenyl]-2-yl), and metabo- chloro-N-(4′-chloro[1,1′-biphenyl]-2-yl), lites 2-chloro-N-(4’-chloro-5-hydroxy- in or on the following commodities: biphenyl-2-yl) nicotinamide and glucu- Parts per ronic acid conjugate of 2-chloro-N-(4′- Commodity million chloro-5-hydroxy-biphenyl-2-yl) nicotinamide, calculated as the stoichio- Animal feed, nongrass, group 18, forage, except alfalfa ...... 1.0 metric equivalent of boscalid in or on Animal feed, nongrass, group 18, hay, except the following food commodities: alfalfa ...... 2.0 Animal feed, nongrass, group 18, seed ...... 0 .05 Parts per Beet, garden, roots ...... 0 .1 Commodity million Beet, sugar, roots ...... 0 .1 Cattle, fat ...... 0.30 Cowpea, seed ...... 0 .1 Cattle, meat ...... 0 .10 Grain, cereal, forage, fodder and straw, group Cattle, meat byproducts ...... 0.35 16, forage ...... 2 .0 Egg ...... 0 .02 Grain, cereal, forage, fodder and straw, group Goat, fat ...... 0 .30 16, stover ...... 1 .5 Goat, meat ...... 0.10 Grain, cereal, forage, fodder and straw, group Goat, meat byproducts ...... 0 .35 16, straw ...... 3 .0 Hog, fat ...... 0 .20 Grain, cereal, group 15 ...... 0.20 Hog, meat ...... 0 .05 Grass, forage, fodder, and hay, group 17, for- Hog, meat byproducts ...... 0 .10 age ...... 2 .0 Horse, fat ...... 0 .30 Horse, meat ...... 0 .10 Grass, forage, fodder, and hay, group 17, hay ... 8 .0 Horse, meat byproducts ...... 0 .35 Grass, forage, fodder, and hay, group 17, seed Milk ...... 0.10 screenings ...... 0 .20 Poultry, fat ...... 0.20 Grass, forage, fodder, and hay, group 17, straw 0 .30 Poultry, meat ...... 0 .05 Lupin, grain, grain ...... 0 .1 Poultry, meat byproducts ...... 0.20 Pea, field, seed ...... 0 .1 Sheep, fat ...... 0 .30 Radish, roots ...... 0 .1 Sheep, meat ...... 0.10 Rice, hulls ...... 0 .50 Sheep, meat byproducts ...... 0 .35 Turnip, roots ...... 0 .1 Vegetable, foliage of legume, group 7, forage .... 1 .5 (b) Section 18 emergency exemptions. Vegetable, foliage of legume, group 7, hay ...... 2 .0 Time-limited tolerances are estab- Vegetable, foliage of legume, group 7, vines ..... 0 .05 lished for residues of the fungicide Vegetable, leafy, except brassica, group 4, ex- boscalid, including its metabolites and cept celery, lettuce and spinach ...... 1 .0 degradates, in connection with use of Vegetable, leaves of root and tuber, group 2 ..... 0 .1

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[68 FR 44651, July 30, 2003, as amended at 69 Parts per FR 19774, Apr. 14, 2004; 70 FR 55293, Sept. 21, Commodity million 2005; 71 FR 6364, Feb. 8, 2006; 71 FR 25961, May 3, 2006; 71 FR 76190, Dec. 20, 2006; 73 FR 16558, Fruit, citrus, Group 10 ...... 0.03 Mar. 28, 2008; 74 FR 47445, Sept. 16, 2009; 75 FR Cotton, undelinted seed ...... 0 .05 Cotton, gin byproducts ...... 1 .0 770, Jan. 6, 2010; 75 FR 29907, May 28, 2010; 75 Sugarcane ...... 0 .01 FR 80346, Dec. 22, 2010; 78 FR 67048, Nov. 8, Tomato ...... 0.01 2013; 80 FR 14014, Mar. 18, 2015] (b) Section 18 emergency exemptions. § 180.590 2, 6-Diisopropylnaphthalene (2, 6-DIPN); tolerances for residues. [Reserved] (c) Tolerances with regional registra- (a) General. Tolerances are estab- tions. [Reserved] lished for residues of the growth inhib- (d) Indirect or inadvertent residues. itor 2,6-DIPN, including its metabolites [Reserved] and degradates, in or on the commodities in the following table. Compliance [68 FR 54386, Sept. 17, 2003] with the tolerance levels specified in the following table is to be determined § 180.592 Butafenacil; tolerances for by measuring only 2,6- residues. Diisopropylnaphthalene. (a) General. (1) Tolerances are established for residues of the herbicide Parts per Commodity million butafenacil, (1,1-dimethyl-2-oxo-2-(2- propenyloxy)ethyl 2-chloro-5-[3,6- Cattle, fat ...... 0.2 dihydro-3-methyl-2,6-dioxo-4- Cattle, meat ...... 0 .02 Cattle, meat byproducts, except fat ...... 0 .02 (trifluoromethyl)-1(2H)-pyrimidinyl] Goat, fat ...... 0 .2 benzoate) in or on the following raw Goat, meat ...... 0.02 agricultural commodities: Goat, meat byproducts, except fat ...... 0 .02 Horse, fat ...... 0 .2 Parts per Horse, meat ...... 0 .02 Commodity million Horse, meat byproducts, except fat ...... 0.02 Milk, fat ...... 0 .02 Cotton, gin byproducts ...... 10 Potato, granules/flakes ...... 5 .5 Cotton, undelinted seed ...... 0 .50 Potato, wet peel ...... 6 .0 Potato, whole ...... 2 .0 Sheep, fat ...... 0 .2 (2) Tolerances are established for res- Sheep, meat ...... 0.02 idues of the herbicide butafenacil, (1,1- Sheep, meat byproducts, except fat ...... 0 .02 dimethyl-2-oxo-2-(2-propenyloxy)ethyl 2-chloro-5-[3,6-dihydro-3-methyl-2,6- (b) Section 18 emergency exemptions. dioxo-4-(trifluoromethyl)-1(2H)- [Reserved] pyrimidinyl] benzoate) and its metabo- (c) Tolerances with regional registra- lite CGA-293731 (1-carboxy-1- tions. [Reserved] methylethyl 2-chloro-5-[3,6-dihydro-3- (d) Indirect or inadvertent residues. methyl-2,6-dioxo-4-(trifluoromethyl)- [Reserved] 1(2H)-pyrimidinyl] benzoate), in or on [71 FR 52011, Sept. 1, 2006, as amended at 74 the following livestock commodities: FR 66579, Dec. 16, 2009; 77 FR 32406, June 1, 2012] Parts per Commodity million

§ 180.591 Trifloxysulfuron; tolerances Cattle, kidney ...... 0 .05 for residues. Cattle, liver ...... 0 .50 (a) General. Tolerances are estab- Goat, kidney ...... 0 .05 lished for residues of the herbicide Goat, liver ...... 0.50 Hog, kidney ...... 0.05 trifloxysulfuron, N-[[(4,6-dimethoxy-2- Hog, liver ...... 0 .50 pyrimidinyl)amino]carbonyl]-3-(2,2,2- Horse, kidney ...... 0 .05 trifluoroethoxy)-2-pyridinesulfonamide Horse, liver ...... 0 .50 in or on the following raw agricultural Sheep, kidney ...... 0.05 commodities. Sheep, liver ...... 0.50

Parts per (b) Section 18 emergency exemptions. Commodity million [Reserved] Almond ...... 0.02 (c) Tolerances with regional registra- Almond, hulls ...... 0 .01 tions. [Reserved]

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(d) Indirect and inadvertant residues. Commodity Parts per [Reserved] million [68 FR 54827, Sept. 19, 2003] Tomato ...... 0.20 1There are no U.S. registrations for use of etoxazole on § 180.593 Etoxazole; tolerances for resi- tangerines as of September 26, 2003. * There are currently no U.S. registrations for tea as of April dues. 13, 2011. 2 There are no U.S. registrations for orange and orange, oil (a) General. Tolerances are estab- as of December 2, 2015. lished for residues of etoxazole, including its metabolites and degradates, in (b) Section 18 emergency exemptions. or on the commodities in the table [Reserved] below. Compliance with the tolerance (c) Tolerances with regional registra- levels specified below is to be deter- tions. [Reserved] mined by measuring only etoxazole (2- (d) Indirect and inadvertant residues. (2,6-difluorophenyl)-4-[4-(1,1- [Reserved] dimethylethyl)-2-ethoxyphenyl]-4,5- [68 FR 55493, Sept. 26, 2003, as amended at 70 dihydrooxazole) in or on the com- FR 41625, July 20, 2005; 72 FR 72963, Dec. 26, modity. 2007; 74 FR 25160, May 27, 2009; 76 FR 20542, Apr. 13, 2011; 77 FR 3621, Jan. 25, 2012; 80 FR Parts per 75430, Dec. 2, 2015] Commodity million

Almond, hulls ...... 2 .0 § 180.594 Thiacloprid; tolerances for Apple, wet pomace ...... 0 .50 residues. Avocado ...... 0 .20 (a) General. Tolerances are estab- Berry, low growing, subgroup 13–07G ...... 0 .50 Caneberry subgroup 13–07A ...... 1.5 lished for residues of the insecticide Canistel ...... 0 .20 thiacloprid, including its metabolites Cattle, fat ...... 0.02 and degradates in or on the commod- Cattle, liver ...... 0 .01 Corn, field, forage ...... 0 .80 ities in the following table. Compliance Corn, field, grain ...... 0 .01 with the tolerance levels specified in Corn, field, refined oil ...... 0 .03 the following table is to be determined Corn, field, stover ...... 4 .0 Corn, pop, grain ...... 0.01 by measuring only thiacloprid ([3-[(6- Corn, pop, stover ...... 4.0 chloro-3-pyridinyl)methyl]-2- Cotton, gin byproducts ...... 1 .0 thiazolidinylidene] cyanamide) in or on Cotton, undelinted seed ...... 0 .05 Fruit, pome, group 11 ...... 0.20 the commodity. Fruit, small vine climbing, except fuzzy kiwifruit, subgroup 13–07F ...... 0 .50 Parts per Commodity million Fruit, stone, group 12, except plum ...... 1 .0 Goat, fat ...... 0 .02 Apple, wet pomace ...... 0 .60 Goat, liver ...... 0.01 Cattle, fat ...... 0.020 Grape, raisin ...... 1 .5 Cattle, kidney ...... 0 .050 Hop, dried cones ...... 7 .0 Cattle, liver ...... 0 .15 Horse, fat ...... 0 .02 Cattle, meat ...... 0 .030 Horse, liver ...... 0 .01 Cattle, meat byproducts ...... 0.050 Mango ...... 0.20 Cherry subgroup 12–12A ...... 0 .5 Melon subgroup 9A ...... 0 .20 Cotton, gin byproducts ...... 11 .0 Milk, fat ...... 0 .01 Cotton, undelinted seed ...... 0 .020 Nut, tree, group 14 ...... 0 .01 Fruit, pome, group 11 ...... 0.30 2 Orange ...... 0 .10 Goat, fat ...... 0 .020 2 Orange, oil ...... 1 .0 Goat, kidney ...... 0 .050 Papaya ...... 0 .20 Goat, liver ...... 0.15 Pepper/eggplant subgroup 8–10B ...... 0 .20 Goat, meat ...... 0.030 Peppermint, oil ...... 20 Goat, meat byproducts ...... 0 .050 Peppermint, tops ...... 10 Horse, fat ...... 0 .020 Pistachio ...... 0.01 Horse, kidney ...... 0 .050 Plum ...... 0 .15 Horse, liver ...... 0 .15 Plum, prune, dried ...... 0.30 Horse, meat ...... 0 .030 Sapodilla ...... 0 .20 Horse, meat byproducts ...... 0 .050 Sapote, black ...... 0 .20 Milk ...... 0.030 Sapote, mamey ...... 0 .20 Peach subgroup 12–12B ...... 0.5 Sheep, fat ...... 0 .02 Pepper ...... 1 .0 Sheep, liver ...... 0.01 Plum subgroup 12–12C ...... 0 .05 Spearmint, oil ...... 20 Sheep, fat ...... 0 .020 Spearmint, tops ...... 10 Sheep, kidney ...... 0.050 Squash/cucumber subgroup 9B ...... 0.02 Sheep, liver ...... 0.15 Star apple ...... 0 .20 Sheep, meat ...... 0.030 1 Tangerine ...... 0 .10 Sheep, meat byproducts ...... 0 .050 Tea, dried * ...... 15

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(b) Section 18 emergency exemptions. Commodity Parts per [Reserved] million (c) Tolerances with regional registra- Soybean, seed ...... 0 .01 tions. [Reserved] Sugarcane, cane ...... 0.01 (d) Indirect or inadvertent residues. [Reserved] (2) Tolerances are established for res- [68 FR 55512, Sept. 26, 2003, as amended at 78 idues of the herbicide flufenpyr-ethyl; FR 8416, Feb. 6, 2013] acetic acid, [2-chloro-4-fluoro-5-[5- methyl-6-oxo-4-(trifluoromethyl)-1- EFFECTIVE DATE NOTE: At 81 FR 34906, June 1, 2016, § 180.594 was amended by revising the (6H)-pyridazinyl]-phenoxy]-ethyl table in paragraph (a), effective Nov. 28, 2016. ester], and its metabolite, S-3153 acid- For the convenience of the user, the revised 4-OH; [2-chloro-4-hydroxy-5-[5-methyl- text is set forth as follows: 6- oxo-4-(trifluoromethyl)-1-(6H)- pyridazinyl]-phenoxy]-acetic acid, free § 180.594 Thiacloprid; tolerances for residues. and conjugated, in or on the following (a) * * * commodities:

Parts per Commodity Parts per Commodity million million

Apple, wet pomace 1 ...... 0.60 Corn, field, forage ...... 0 .05 Cattle, fat 1 ...... 0.020 Corn, field, stover ...... 0 .05 Cattle, kidney 1 ...... 0.050 Cattle, liver 1 ...... 0.15 Cattle, meat 1 ...... 0.030 (b) Section 18 emergency exemptions. Cattle, meat byproducts 1 ...... 0.050 [Reserved] Cherry subgroup 12–12A 1 ...... 0.5 (c) Tolerances with regional registra- Cotton, gin byproducts 1 ...... 11.0 Cotton, undelinted seed 1 ...... 0.020 tions. [Reserved] Fruit, pome, group 11 1 ...... 0.30 (d) Indirect or inadvertent residues. Goat, fat 1 ...... 0.020 Goat, kidney 1 ...... 0.050 [Reserved] Goat, liver 1 ...... 0.15 Goat, meat 1 ...... 0.030 [68 FR 54842, Sept. 19, 2003] Goat, meat byproducts 1 ...... 0.050 Horse, fat 1 ...... 0.020 § 180.596 Fosthiazate; tolerances for Horse, kidney 1 ...... 0.050 residues. Horse, liver 1 ...... 0.15 Horse, meat 1 ...... 0.030 (a) General. A tolerance is established Horse, meat byproducts 1 ...... 0.050 for residues of the insecticide Milk 1 ...... 0.030 Peach subgroup 12–12B 1 ...... 0.5 fosthiazate, including its metabolites Peach subgroup 12–12C 1 ...... 0.05 and degradates, in or on the com- Pepper 1 ...... 1.0 modity in the table in this paragraph. Sheep, fat 1 ...... 0.020 Sheep, kidney 1 ...... 0.050 Compliance with the tolerance level Sheep, liver 1 ...... 0.15 specified in this paragraph is to be de- Sheep, meat 1 ...... 0.030 termined by measuring only the sum of Sheep, meat byproducts 1 ...... 0.050 fosthiazate, O-ethyl S-(1- 1 There are no U.S. registrations for the commodity since August 6, 2014. methylpropyl)(2-oxo-3- thiazolidinyl)phosphonothioate, and its * * * * * metabolite, O-ethyl S-(1- methylpropyl)(2- § 180.595 Flufenpyr-ethyl; tolerances (methylsulfonyl)ethyl) for residues. phosphoramidothioate, calculated as (a) General. (1) Tolerances are estab- the stoichiometric equivalent of lished for residues of the herbicide, fosthiazate, in or on the commodity. flufenpyr-ethyl; acetic acid, [2-chloro- Parts per 4-fluoro-5-[5-methyl-6-oxo-4- Commodity million (trifluoromethyl)-1-(6H)-pyridazinyl]- phenoxy]-ethyl ester], in or on the fol- Tomato ...... 0.02 lowing commodities: (b) Section 18 emergency exemptions. [Reserved] Commodity Parts per million (c) Tolerances with regional registra- Corn, field, grain ...... 0 .01 tions. [Reserved]

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(d) Indirect or inadvertent residues. Commodity Parts per [Reserved] million [69 FR 18275, Apr. 7, 2004, as amended at 76 Carrot ...... 0 .05 FR 23498, Apr. 27, 2011] Cattle, fat ...... 11 Cattle, kidney ...... 1 .0 § 180.597 Mesosulfuron-methyl; toler- Cattle, liver ...... 1 .0 Cattle, meat ...... 0 .60 ances for residues. Cattle, meat byproducts, except kidney and liver 11 (a) General. Tolerances are estab- Cherry subgroup 12–12A ...... 8 .0 lished for residues of the herbicide Corn, sweet, forage ...... 16 mesosulfuron-methyl, (methyl 2- Corn, sweet, kernel plus cob with husks removed ...... 0 .05 [[[[(4,6-dimethoxy-2-pyrimidinyl) Corn, sweet, stover ...... 50 amino]carbonyl]amino]sulfonyl] -4- Cotton, gin byproducts ...... 30 [[(methylsulfonyl)amino] meth- Cotton, undelinted seed ...... 0 .60 yl]benzoate]) in or on the following raw Egg ...... 1 .5 Food commodities and feed commodities (other agricultural commodities: than those covered by a higher tolerance as a result of use on growing crops) in food and Parts per feed handling establishments ...... 0 .01 Commodity million Fruit, pome, group 11–10 ...... 3 .0 Cattle, meat byproducts ...... 0.01 Goat, fat ...... 11 Goat, meat byproducts ...... 0 .01 Goat, kidney ...... 1 .0 Grain, aspirated fractions ...... 0 .60 Goat, liver ...... 1.0 Horse, meat byproducts ...... 0 .01 Goat, meat ...... 0.60 Sheep, meat byproducts ...... 0 .01 Goat, meat byproducts, except kidney and liver 11 Wheat, forage ...... 0 .60 Grain, aspirated fractions ...... 25 Wheat, germ ...... 0 .10 Hog, fat ...... 1 .5 Wheat, grain ...... 0 .03 Hog, kidney ...... 0.10 Wheat, hay ...... 0 .06 Hog, liver ...... 0 .10 Wheat, straw ...... 0 .30 Hog, meat ...... 0 .07 Hog, meat byproducts, except kidney and liver .. 1 .5 (b) Section 18 emergency exemptions. Horse, fat ...... 11 [Reserved] Horse, kidney ...... 1 .0 (c) Tolerances with regional registra- Horse, liver ...... 1 .0 Horse, meat ...... 0 .60 tions. [Reserved] Horse, meat byproducts, except kidney and liver 11 (d) Indirect or inadvertent residues. Milk ...... 1.0 [Reserved] Milk, fat ...... 20 Peach subgroup 12–12B ...... 1.9 [69 FR 18263, Apr. 7, 2004] Peanut ...... 0 .01 Plum, prune, dried ...... 3.0 § 180.598 Novaluron; tolerances for Plum subgroup 12–12C ...... 1 .9 residues. Poultry, fat ...... 7.0 Poultry, kidney ...... 0 .80 (a) General. Tolerances are estab- Poultry, liver ...... 0 .80 lished for residues of the insecticide Poultry, meat ...... 0 .40 novaluron, including its metabolites Poultry, meat byproducts, except kidney and and degradates, in or on the following liver ...... 7 .0 commodities. Compliance with the tol- Sheep, fat ...... 11 Sheep, kidney ...... 1.0 erance levels specified in the following Sheep, liver ...... 1.0 table is to be determined by measuring Sheep, meat ...... 0.60 only novaluron, (N-[[[3-chloro-4-[1,1,2- Sheep, meat byproducts, except kidney and trifluoro-2- (trifluoromethoxy)ethoxy] liver ...... 11 Sorghum, grain, forage ...... 6.0 phenyl]amino]carbonyl]-2,6- Sorghum, grain, grain ...... 3 .0 difluorobenzamide), in or on the fol- Sorghum, grain, stover ...... 40 lowing raw agricultural commodities: Soybean, seed ...... 0 .07 Sugarcane, cane ...... 0.50 Commodity Parts per Swiss chard ...... 12 million Turnip, greens ...... 25 Vegetable, cucurbit, group 9 ...... 0.20 Apple, wet pomace ...... 8 .0 Vegetable, fruiting, group 8–10 ...... 1 .0 Avocado ...... 0 .60 Vegetable, tuberous and corm, subgroup 1C ..... 0.05 Bean, dry, seed ...... 0 .30 Bean, succulent ...... 0 .70 Berry, low growing, subgroup 13-07G, except (b) Section 18 emergency exemptions. lowbush blueberry ...... 0 .45 [Reserved] Brassica, head and stem, subgroup 5A ...... 0 .50 Brassica, leafy greens, subgroup 5B ...... 25 (c) Tolerances with regional registra- Bushberry subgroup 13-07B ...... 7 .0 tions. [Reserved]

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(d) Indirect or inadvertant residues. (d) Indirect or inadvertent residues. [Reserved] [Reserved] [69 FR 31021, June 2, 2004, as amended at 71 [69 FR 43533, July 21, 2004, as amended at 73 FR 17014, Apr. 5, 2006; 71 FR 61911, Oct. 20, FR 17910, Apr. 2, 2008; 75 FR 70148, Nov. 17, 2006; 73 FR 74982, Dec. 10, 2008; 74 FR 637, Jan. 2010; 77 FR 25909, May 2, 2012; 81 FR 21756, 7, 2009; 74 FR 20891, May 6, 2009; 74 FR 65033, Apr. 13, 2016] Dec. 9, 2009; 75 FR 4278, Jan. 27, 2010; 75 FR 29447, May 26, 2010; 76 FR 55814, Sept. 9, 2011; § 180.600 Propoxycarbazone; toler- 78 FR 40033, July 3, 2013; 80 FR 43335, July 22, ances for residues. 2015] (a) General. (1) Tolerances are estab- § 180.599 Acequinocyl; tolerances for lished for combined residues of the her- residues. bicide propoxycarbazone methyl 2- (a) General. Tolerances are estab- [[[(4,5-dihydro-4-methyl-5-oxo-3- lished for residues of acequinocyl, in- propoxy-1H-1,2,4-triazol-1- cluding its metabolites and degradates, yl)carbonyl]amino]sulfonyl]benzoate in or on the commodities in the table and its metabolite methyl 2-[[[(4,5- below. Compliance with the tolerance dihydro-3-(2-hydroxypropoxy)-4-meth- levels specified below is to be deter- yl-5-oxo-1H-1,2,4-triazol-1- mined by measuring only the sum of yl)carbonyl]amino]sulfonyl]benzoate acequinocyl [2-(acetyloxy)-3-dodecyl- in/on the following raw agricultural 1,4-naphthalenedione] and its metabo- commodities: lite, 2-dodecyl-3-hydroxy-1,4- Parts per naphthoquinone, calculated as the stoi- Commodity million chiometric equivalent of acequinocyl, in or on the commodity. Grass, forage ...... 20 Grass, hay ...... 25 Wheat, forage ...... 17 Parts per Commodity million Wheat, grain ...... 0 .02 Wheat, hay ...... 0 .15 Almond, hulls ...... 2 .0 Wheat, straw ...... 0 .05 Apple, wet pomace ...... 1 .0 Bean, edible podded ...... 0 .25 (2) Tolerances are established for res- Bean, succulent shelled ...... 0 .30 Berry, low growing, subgroup 13–07G ...... 0 .50 idues of the herbicide Caneberry subgroup 13–07A ...... 4.0 propoxycarbazone methyl 2-[[[(4,5- Cattle, fat ...... 0.02 dihydro-4-methyl-5-oxo-3-propoxy-1H- Cattle, meat byproducts ...... 0.02 1,2,4-triazol-1-yl)carbonyl] Cherry, sweet ...... 0 .50 amino]sulfonyl]benzoate in/on the fol- Cherry, tart ...... 1 .0 Citrus, oil ...... 30 lowing raw agricultural commodities: Cowpea, forage ...... 6 .0 Cowpea, hay ...... 18 Commodity Parts per Cucumber ...... 0 .15 million Fruit, citrus, group 10 ...... 0 .20 Cattle, meat ...... 0 .05 Fruit, pome, group 11 ...... 0.40 Fruit, small vine climbing, except fuzzy kiwifruit, Cattle, meat byproducts ...... 0.3 subgroup 13–07F ...... 1 .6 Goat, meat ...... 0.05 Goat, fat ...... 0 .02 Goat, meat byproducts ...... 0 .3 Goat, meat byproducts ...... 0 .02 Horse, meat ...... 0 .05 Hop, dried cones ...... 15 Horse, meat byproducts ...... 0 .3 Horse, fat ...... 0 .02 Milk ...... 0.03 Horse, meat byproducts ...... 0 .02 Sheep, meat ...... 0.05 Melon subgroup 9A ...... 0 .15 Sheep, meat byproducts ...... 0 .3 Nut, tree, group 14 ...... 0 .02 Okra ...... 0.70 Pistachio ...... 0.02 (b) Section 18 emergency exemptions. Sheep, fat ...... 0 .02 [Reserved] Sheep, meat byproducts ...... 0 .02 (c) Tolerances with regional registra- Soybean, vegetable, succulent ...... 0 .25 tions. [Reserved] Vegetable, fruiting, group 8 ...... 0.70 (d) Indirect or inadvertent residues. (b) Section 18 emergency exemptions. [Reserved] [Reserved] [69 FR 40781, July 7, 2004, as amended at 71 (c) Tolerances with regional registra- FR 52487, Sept. 6, 2006; 74 FR 9377, Mar. 4, tions. [Reserved] 2009]

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§ 180.601 Cyazofamid; tolerances for of the fungicide cyazofamid, including residues. its metabolites and degradates, in or (a) General. Tolerances are estab- on the commodities in the following lished for residues of the fungicide table. Compliance with the tolerance cyazofamid, including its metabolites levels specified in the following table is and degradates, in or on the commod- to be determined by measuring only ities in the following table. Compliance the sum of 4-chloro-2-cyano-N,N-di- with the tolerance levels specified in methyl-5-(4-methylphenyl)-1H-imid- the following table is to be determined azole-1-sulfonamide and its metabolite, by measuring only the sum of 4-chloro- 4-chloro-5-(4-methylphenyl)-1H-imid- 2-cyano-N,N-dimethyl-5-(4- azole-2-carbonitrile, calculated as the methylphenyl)-1H-imidazole-1-sul- stoichiometric equivalent of fonamide and its metabolite, 4-chloro- cyazofamid, in or on the following 5-(4-methylphenyl)-1H-imidazole-2- commodities: carbonitrile, calculated as the stoichio- Parts per metric equivalent of cyazofamid, in or Commodity million on the following commodities: Grape ...... 1 .5 Commodity Parts per million (d) Indirect or inadvertent residues. Bean, succulent ...... 0 .5 [Reserved] Bean, succulent shelled ...... 0 .08 Brassica, head and stem, subgroup 5A ...... 1 .2 [69 FR 58299, Sept. 30, 2004, as amended at 73 Brassica, leafy greens, subgroup 5B ...... 12 .0 FR 21839, Apr. 23, 2008; 74 FR 32453, July 8, Bulb vegetables, group3–07 ...... 2 .0 2009; 75 FR 40751, July 14, 2010; 77 FR 4252, Carrot, roots ...... 0.09 Jan. 27, 2012; 77 FR 59119, Sept. 26, 2012; 81 FR Herb subgroup 19A ...... 19A 5605, Feb. 3, 2016] Hop dried cones ...... 10.0 Leafy greens subgroup 4A ...... 10 Turnip, greens ...... 12.0 § 180.602 Spiroxamine; tolerances for Vegetable, cucurbit, group 9 ...... 0.10 residues. Vegetable, fruiting, group 8–10 ...... 0 .9 Vegetable, tuberous and corm, subgroup 1C ..... 0.02 (a) General. Tolerances are established for residues of the fungicide (b) Section 18 emergency exemptions. spiroxamine, including its metabolites Time-limited tolerances are estab- and degradates, in or on the commod- lished for residues of the fungicide ities in the table below. Compliance cyazofamid, including its metabolites with the tolerance levels specified in and degradates, in or on the commod- the following table is to be determined ities in the following table. Compliance by measuring only spiroxamine, [(8- with the tolerance levels specified in (1,1-dimethylethyl)-N-ethyl-N-propyl- the following table is to be determined 1,4-dioxaspiro[4,5]decane-2- by measuring only the sum of methanamine) in or on the commod- cyazofamid, 4-chloro-2-cyano-N,N-di- ities. methyl-5-(4-methylphenyl)-1H-imidazole-1-sulfonamide and its metabolite Parts per Commodity million CCIM, 4-chloro-5-(4-methylphenyl)-1H- imidazole-2-carbonitrile, calculated as Artichoke, globe, import 1 ...... 0 .7 the stoichiometric equivalent of Asparagus 1 ...... 0.05 cyazofamid, resulting from use of the Banana (import) ...... 3 .0 Grape (import) ...... 1 .0 pesticide under FIFRA section 18 emer- Vegetable, fruiting , crop group 8 1 ...... 1 .2 gency exemptions. The tolerances ex- 1 No U.S. registration as of December 1, 2010. pire and are revoked on the date specified in the table. (b) Section 18 emergency exemptions. [Reserved] Expiration/ Commodity Parts per revocation (c) Tolerances with regional registra- million date tions. [Reserved] (d) Indirect or inadvertent residues. Basil, dried ...... 144 12/31/14 [Reserved] (c) Tolerances with regional registra- [69 FR 42570, July 16, 2004, as amended at 75 tions. Tolerances with regional reg- FR 74640, Dec. 1, 2010; 80 FR 72599, Nov. 20, istrations are established for residues 2015]

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§ 180.603 Dinotefuran; tolerances for Commodity Parts per residues. million (a) General. (1) Tolerances are estab- Cattle, meat byproducts ...... 0.05 lished for residues of dinotefuran, (RS)- Egg ...... 0 .01 Goat, fat ...... 0 .05 1-methyl-2-nitro-3-((tetrahydro-3- Goat, meat ...... 0.05 furanyl)methyl)guanidine, including Goat, meat byproducts ...... 0 .05 its metabolites and degradates, in or Hog, fat ...... 0 .05 Hog, meat ...... 0 .05 on the commodities listed in the fol- Hog, meat byproducts ...... 0 .05 lowing table. Compliance with the tol- Horse, fat ...... 0 .05 erance levels specified below is to be Horse, meat ...... 0 .05 Horse, meat byproducts ...... 0 .05 determined by measuring only the sum Milk ...... 0.05 of dinotefuran and its metabolites DN, Poultry, meat byproducts ...... 0.01 1-methyl-3-(tetrahydro-3- Sheep, fat ...... 0 .05 furylmethyl)guanidine, and UF, 1- Sheep, meat ...... 0.05 Sheep, meat byproducts ...... 0 .05 methyl-3-(tetrahydro-3- furylmethyl)urea, calculated as the (3) A tolerance of 0.01 parts per mil- stoichiometric equivalent of lion is established for residues of the dinotefuran, in or on the commodities insecticide dinotefuran, (RS)-1-methyl- listed in the table below: 2-nitro-3-((tetrahydro-3- Parts per furanyl)methyl)guanidine, including Commodity million its metabolites and degradates, in or on all food and/or feed commodities Berry, low growing, except strawberry, subgroup 13–07H ...... 0 .2 (other than those covered by a higher Brassica, head and stem, subgroup 5A ...... 1 .4 tolerance as a result of use on growing Brassica, leafy greens, subgroup 5B ...... 15 .0 crops or inadvertent residues) when Cotton, undelinted seed ...... 0 .4 Cotton, gin byproducts ...... 8 .0 residues result from application of Fruit, small vine climbing, except fuzzy kiwifruit, dinotefuran in food and/or feed han- subgroup 13–07F ...... 0 .9 dling establishments where food and/or Grape, raisin ...... 2 .5 Onion, bulb, subgroup 3–07A ...... 0 .15 feed products are held, stored, proc- Onion, green, subgroup 3–07B ...... 5 .0 essed, prepared, or served. Compliance Peach ...... 1 .0 with the tolerance level is to be deter- Potato, chips ...... 0 .1 mined by measuring only dinotefuran. Potato, granules/flakes ...... 0 .15 Rice, grain ...... 9 .0 (b) Section 18 emergency exemptions. Tea, dried1 ...... 50 Time-limited tolerances are estab- Tomato, paste ...... 1 .0 lished for residues of dinotefuran, (RS)- Turnip, greens ...... 15.0 Vegetable, fruiting, group 8 ...... 0.7 1-methyl-2-nitro-3-((tetrahydro-3- Vegetable, cucurbit, group 9 ...... 0.5 furanyl)methyl)guanidine, including Vegetable, leafy, except Brassica, group 4 ...... 5 .0 its metabolites and degradates, in or Vegetable, tuberous and corm, subgroup 1C ..... 0.05 Watercress ...... 8 .0 on the commodities in the table below resulting from use of the pesticide pur- 1 There are no U.S. registrations for tea. suant to FIFRA section 18 emergency (2) Tolerances are established for res- exemptions. Compliance with the toler- idues of dinotefuran, (RS)-1-methyl-2- ance levels specified below is to be de- nitro-3-((tetrahydro-3- termined by measuring only the sum of furanyl)methyl)guanidine, including dinotefuran and its metabolites DN, 1- its metabolites and degradates, in or methyl-3-(tetrahydro-3- on the commodities listed in the fol- furylmethyl)guanidine, and UF, 1- lowing table. Compliance with the tol- methyl-3-(tetrahydro-3- erance levels specified below is to be furylmethyl)urea, calculated as the determined by measuring only the sum stoichiometric equivalent of of dinotefuran, (RS)-1-methyl-2-nitro-3- dinotefuran, in or on the commodities ((tetrahydro-3- listed in the table below. The toler- furanyl)methyl)guanidine in or on the ances expire and are revoked on the commodities listed in the table below: dates specified in the table.

Commodity Parts per Expiration/ million Commodity Parts per revocation million date Cattle, fat ...... 0.05 Cattle, meat ...... 0 .05 Fruit, pome, Group 11 ...... 2.0 12/31/18

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Expiration/ Parts per Commodity Parts per revocation Commodity million million date Almond, hulls ...... 0 .01 Fruit, stone, Group 12 ...... 2.0 12/31/18 Fish ...... 0 .01 Fish, shellfish, crustacean ...... 0 .01 (c) Tolerances with regional registra- Fish, shellfish, mollusc ...... 0 .02 Fruit, pome, group 11–10 ...... 0 .01 tions. [Reserved] Fruit, small, vine climbing, subgroup 13–07F, (d) Indirect or inadvertent residues. except fuzzy kiwifruit ...... 0 .01 [Reserved] Fruit, stone, group 12–12 ...... 0 .01 Nut, tree, group 14–12 ...... 0 .01 [70 FR 14546, Mar. 23, 2005, as amended at 74 Olive ...... 0 .01 FR 12601, Mar. 25, 2009; 74 FR 67104, Dec. 18, Pomegranate ...... 0 .01 Rice, grain ...... 0 .02 2009; 75 FR 770, Jan. 6, 2010; 77 FR 56138, Sept. 12, 2012; 77 FR 67285, Nov. 9, 2012; 77 FR 70913, (b) Section 18 emergency exemptions. Nov. 28, 2012; 78 FR 21272, Apr. 10, 2013; 78 FR 24683, Apr. 26, 2013; 79 FR 3512, Jan. 22, 2014; [Reserved] 80 FR 78145, Dec. 16, 2015] (c) Tolerances with regional registrations. [Reserved] § 180.604 Mepanipyrim; tolerances for (d) Indirect or inadvertent residues. residues. [Reserved] (a) General. [Reserved] [69 FR 57197, Sept. 24, 2004, as amended at 72 (b) Section 18 emergency exemptions. FR 40763, July 25, 2007; 74 FR 18648, Apr. 24, [Reserved] 2009; 80 FR 72599, Nov. 20, 2015; 81 FR 10776, (c) Tolerances with regional registra- Mar. 2, 2016] tions. [Reserved] (d) Indirect of inadvertent residues. § 180.607 Spiromesifen; tolerances for residues. [Reserved] (e) Revoked tolerances subject to the (a) General. (1) Tolerances are estab- channel of trade provisions. [Reserved] lished for residues of the insecticide/ (f) Import tolerances. Tolerances are miticide spiromesifen, including its established for the combined residues metabolites and degradates, in or on of mepanipyrim, 4-methyl-N-phenyl-6- the commodities listed below. Compli- (1-propynyl)-2-pyrimidinamine, and its ance with the tolerance levels specified metabolite, 4-methyl-N-phenyl-6-(2- below is to be determined by measuring hydroxypropylk)-2-pyrimidinamine, only the sum of spiromesifen [2-oxo-3- both free and conjugated in or on the (2,4,6-trimethylphenyl)-1- following commodities: oxaspiro[4.4]non-3-en-4-yl 3,3- dimethylbutanoate] and 4-hydroxy-3- Commodity Parts per (2,4,6-trimethylphenyl)-1- million oxaspiro[4.4]non-3-en-2-one, calculated Grape ...... 1 .5 as the stoichiometric equivalent of Grape, raisin ...... 3 .0 spiromesifen, in or on the following Strawberry ...... 1 .5 Tomato ...... 0.5 primary crop commodities:

Commodity Parts per [68 FR 60827, Oct. 13, 2004] million Bean, dry ...... 0.02 § 180.605 Penoxsulam; tolerances for Bean, edible podded ...... 0 .80 residues. Bean, succulent ...... 0 .10 Berry and small fruit, low growing berry, sub- (a) General. Tolerances are estab- group 13-07G ...... 2 .0 lished for residues of penoxsulam, in- Brassica, head and stem, subgroup 5A ...... 2 .0 cluding its metabolites and degradates, Brassica, leafy greens, subgroup 5B ...... 12 Corn, field, forage ...... 5 .0 in or on the commodities listed in the Corn, field, grain ...... 0 .02 table below. Compliance with the toler- Corn, field, stover ...... 8 .0 ance levels specified below is to be de- Corn, pop, grain ...... 0.02 termined by measuring only Corn, pop, stover ...... 4.0 Corn, sweet, forage ...... 17 penoxsulam 2-(2,2-difluoroethoxy)-N- Corn, sweet, kernel plus cob with husks re- (5,8-dimethoxy[1,2,4]triazolo[1,5-c] moved ...... 0 .02 pyrimidin-2-yl)-6-(trifluoromethyl) Corn, sweet, stover ...... 12 Cotton, gin byproducts ...... 15 benzenesulfonamide, in or on the com- Cotton, undelinted seed ...... 0 .50 modity. Cowpea, forage ...... 30

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as the stoichiometric equivalent of Commodity Parts per million spiromesifen, in or on the specified ag- Cowpea, hay ...... 86 ricultural commodities, resulting from Leaf petiole subgroup 4B ...... 6 .0 use of the pesticide pursuant to FIFRA Leafy greens subgroup 4A ...... 12 section 18 emergency exemptions. The Pea, dry, seed ...... 0 .20 Peppermint, tops ...... 45 tolerances expire and are revoked on Spearmint, tops ...... 45 the date specified in the table. Tea, dry ...... 40 Tomato, paste ...... 0 .80 Expiration/ Vegetable, cucurbit, group 9 ...... 0.10 Parts per Commodity million revocation Vegetable, fruiting, group 8 ...... 0.45 date Vegetable, tuberous and corm, subgroup 1C ..... 0.02 Soybean, forage ...... 30 12/31/14 (2) Tolerances are established for res- Soybean, hay ...... 86 12/31/14 Soybean, seed ...... 0.02 12/31/14 idues of the insecticide/miticide spiromesifen, including its metabolites (c) Tolerances with regional registra- and degradates, in or on the commod- tions. [Reserved] ities listed below. Compliance with the (d) Indirect or inadvertent residues. tolerance levels specified below is to be Tolerances are established for the inad- determined by measuring only the sum vertent or indirect residues of the in- of spiromesifen [2-oxo-3-(2,4,6- secticide/miticide spiromesifen, includ- trimethylphenyl)-1-oxaspiro[4.4]non-3- ing its metabolites and degradates, in en-4-yl 3,3-dimethylbutanoate] and its or on the commodities listed below. metabolites containing the 4-hydroxy- Compliance with the tolerance levels 3-(2,4,6-trimethylphenyl)-1- specified below is to be determined by oxaspiro[4.4]non-3-en-2-one and 4-hy- measuring only the sum of droxy-3-[4-(hydroxymethyl)-2,6- spiromesifen [2-oxo-3-(2,4,6- dimethylphenyl]-1-oxaspiro[4.4]non-3- trimethylphenyl)-1-oxaspiro[4.4]non-3- en-2-one moieties, calculated as the en-4-yl 3,3-dimethylbutanoate], 4-hy- stoichiometric equivalent of droxy-3-(2,4,6-trimethylphenyl)-1- spiromesifen, in the following livestock oxaspiro[4.4]non-3-en-2-one, and its me- commodities: tabolites containing the 4-hydroxy-3-[4- Parts per (hydroxymethyl)-2,6-dimethylphenyl]- Commodity million 1-oxaspiro[4.4]non-3-en-2-one moiety, Cattle, fat ...... 0.10 calculated as the stoichiometric equiv- Cattle, meat ...... 0 .02 alent of spiromesifen, in the following Cattle, meat byproducts ...... 0.20 rotational crop commodities: Goat, fat ...... 0 .10 Goat, meat ...... 0.02 Parts per Goat, meat byproducts ...... 0 .20 Commodity million Horse, fat ...... 0 .10 Horse, meat ...... 0 .02 Alfalfa, forage ...... 1.5 Horse, meat byproducts ...... 0 .20 Alfalfa, hay ...... 3.0 Milk ...... 0.01 Barley, grain ...... 0 .03 Milk, fat ...... 0 .25 Barley, hay ...... 0 .25 Sheep, fat ...... 0 .10 Barley, straw ...... 0 .15 Sheep, meat ...... 0.02 Beet, sugar, roots ...... 0 .03 Sheep, meat byproducts ...... 0 .20 Beet, sugar, tops ...... 0.20 Oat, forage ...... 0 .20 (b) Section 18 emergency exemptions. Oat, grain ...... 0 .03 Time-limited tolerances specified in Oat, hay ...... 0.25 Oat, straw ...... 0.25 the following table are established for Vegetable, bulb, group 3-07 ...... 0 .09 residues of the insecticide/miticide Wheat, forage ...... 0 .20 spiromesifen, including its metabolites Wheat, grain ...... 0 .03 and degradates, in or on the commod- Wheat, hay ...... 0 .15 Wheat, straw ...... 0 .25 ities listed below. Compliance with the tolerance levels specified below is to be determined by measuring only the sum [70 FR 43283, July 27, 2005, as amended at 72 of spiromesifen [2-oxo-3-(2,4,6- FR 3079, Jan. 24, 2007; 73 FR 13140, Mar. 12, 2008; 73 FR 52606, Sept. 10, 2008; 74 FR 8492, trimethylphenyl)-1-oxaspiro[4.4]non-3- Feb. 25, 2009; 74 FR 15886, Apr. 8, 2009; 75 FR en-4-yl 3,3-dimethylbutanoate] and 4- 5526, Feb. 3, 2010; 75 FR 53586, Sept. 1, 2010; 76 hydroxy-3-(2,4,6-trimethylphenyl)-1- FR 81396, Dec. 28, 2011; 78 FR 3337, Jan. 16, oxaspiro[4.4]non-3-en-2-one, calculated 2013]

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§ 180.608 Spirodiclofen; tolerances for (b) Section 18 emergency exemptions. residues. [Reserved] (a) General. (1) Tolerances are estab- (c) Tolerances with regional registra- lished for residues of spirodiclofen, in- tions. [Reserved] cluding its metabolites and degradates, (d) Indirect or inadvertent residues. in or on the commodities listed below. [Reserved] Compliance with the following toler- [70 FR 40211, July 13, 2005, as amended at 73 ance levels is to be determined by FR 25539, May 7, 2008; 75 FR 24434, May 5, measuring only spirodiclofen (3-(2,4- 2010; 77 FR 73939, Dec. 12, 2012; 79 FR 33464, dichlorophenyl)-2-oxo-1- June 11, 2014] oxaspiro[4.5]dec-3-en-4-yl 2,2- dimethylbutanoate). § 180.609 Fluoxastrobin; tolerances for residues.

Commodity Parts per (a) General. (1) Tolerances are estab- million lished for residues of fluoxastrobin, in- Almond, hulls ...... 20 .0 cluding its metabolites and degradates, Apple, wet pomace ...... 2 .4 in or on the commodities in the table Avocado ...... 1 .0 Black sapote ...... 1 .0 below. Compliance with the tolerance Canistel ...... 1 .0 levels specified below is to be deter- Citrus, juice ...... 0 .60 mined by measuring only Citrus, oil ...... 35 Fruit, citrus, group 10 ...... 0 .50 fluoxastrobin, (1E)-[2-[[6-(2-chlorophen Fruit, pome, group 11 ...... 0.80 oxy)-5-fluoro-4- Fruit, stone, group 12 ...... 1 .0 pyrimidinyl]oxy]phenyl](5,6-dihydro- Grape ...... 2 .0 1,4,2-dioxazin-3-yl)methanone O- Grape, raisin ...... 6 .0 Hop, dried cones ...... 30 methyloxime and its Z isomer, (1Z)-[2- Mamey sapote ...... 1 .0 [[6-(2-chlorophenoxy)-5-fluoro-4- Mango ...... 1.0 pyrimidinyl]oxy]phenyl](5,6-dihydro- Nut, tree, group 14 ...... 0 .10 Papaya ...... 1 .0 1,4,2-dioxazin-3-yl)methanone O- Pistachio ...... 0.10 methyloxime, calculated as the stoi- Sapodilla ...... 1 .0 chiometric equivalent of fluoxastrobin. Star apple ...... 1 .0 Commodity Parts per (2) Tolerances are established for res- million idues of spirodiclofen, including its me- Berry, low growing, subgroup 13-07G ...... 1 .9 tabolites and degradates, in or on the Corn, field, forage ...... 3 .0 commodities listed below. Compliance Corn, field, grain ...... 0 .02 Corn, field, stover ...... 4 .5 with the following tolerance levels is Corn, sweet, forage ...... 13 to be determined by measuring only Corn, sweet, kernel plus cob with husks re- spirodiclofen (3-(2,4-dichlorophenyl)-2- moved ...... 0 .01 Corn, sweet, stover ...... 10 oxo-1-oxaspiro[4.5]dec-3-en-4-yl 2,2- Grain, aspirated grain fractions ...... 60 dimethylbutanoate) and its metabolite Leaf petioles subgroup 4B ...... 4 .0 3-(2,4-dichlorophenyl)-4-hydroxy-1- Melon subgroup 9A ...... 1 .5 Peanut ...... 0 .02 oxaspiro[4,5] dec-3-en-2-one, calculated Peanut, hay ...... 20.0 as the stoichiometric equivalent of Peanut, refined oil ...... 0.06 spirodiclofen. Rice, grain ...... 4 .0 Sorghum, grain, forage ...... 5.0 Parts per Sorghum, grain, grain ...... 1 .5 Commodity million Sorghum, grain, stover ...... 5 .0 Soybean, forage ...... 9 .0 Cattle, fat ...... 0.02 Soybean, hay ...... 1 .2 Cattle, meat byproducts ...... 0.10 Soybean, hulls ...... 0 .20 Cattle, meat ...... 0 .02 Soybean, seed ...... 0 .05 Goat, fat ...... 0 .02 Squash/cucumber subgroup 9B ...... 0.50 Goat, meat byproducts ...... 0 .1 Tomato, paste ...... 1 .5 Goat, meat ...... 0.02 Vegetable, fruiting, group 8 ...... 1.0 Horse, fat ...... 0 .02 Vegetable, tuberous and corm, subgroup 1C ... 0.010 Horse, meat byproducts ...... 0 .1 Wheat, forage ...... 7 .0 Horse, meat ...... 0 .02 Wheat, grain ...... 0 .15 Milk ...... 0.01 Wheat, hay ...... 17 Milk, fat ...... 0 .03 Wheat, straw ...... 11 Sheep, fat ...... 0 .02 Sheep. meat byproducts ...... 0 .1 (2) Tolerances are established for res- Sheep. meat ...... 0.02 idues of fluoxastrobin, including its

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metabolites and degradates, in or on methyloxime, calculated as the stoi- the commodities in the table below. chiometric equivalent of fluoxastrobin. Compliance with the tolerance levels Parts per specified below is to be determined by Commodity million measuring only fluoxastrobin, (1E)-[2- [[6-(2-chlorophenoxy)-5-fluoro-4- Alfalfa, forage ...... 0.050 Alfalfa, hay ...... 0.10 pyrimidinyl]oxy]phenyl](5,6-dihydro- Cotton, gin byproducts ...... 0 .020 1,4,2-dioxazin-3-yl)methanone O- Grain, cereal, forage, fodder, and straw, group methyloxime, its Z isomer, (1Z)-[2-[[6- 16, except corn ...... 0.10 Grass, forage ...... 0 .10 (2-chlorophenoxy)-5-fluoro-4- Grass, hay ...... 0 .50 pyrimidinyl]oxy]phenyl](5,6-dihydro- Vegetable, foliage of legume, group 7 ...... 0 .050 1,4,2-dioxazin-3-yl)methanone O- methyloxime, and its phenoxy-hydroxy [74 FR 67113, Dec. 18, 2009, as amended at 75 pyrimidine, 6-(2-chlorophenoxy)-5- FR 60333, Sept. 30, 2010; 76 FR 50898, Aug. 17, fluoro-4-pyrimidinol, calculated as the 2011; 77 FR 26471, May 4, 2012; 77 FR 64915, stoichiometric equivalent of Oct. 24, 2012; 79 FR 20105, Apr. 11, 2014; 79 FR fluoxastrobin. 59119, Oct. 1, 2014]

Commodity Parts per § 180.610 Aminopyralid; tolerances for million residues. Cattle, fat ...... 0.10 (a) General. (1) Tolerances are estab- Cattle, meat ...... 0 .05 lished for residues of the herbicide Cattle, meat byproducts ...... 0.20 aminopyralid, 4-amino-3,6-dichloro-2- Goat, fat ...... 0 .10 Goat, meat ...... 0.05 pyridinecarboxylic acid, including its Goat, meat byproducts ...... 0 .20 metabolites and degradates, in or on Hog, fat ...... 0 .03 the commodities in the table below. Hog, meat byproducts ...... 0 .06 Compliance with the tolerance levels Horse, fat ...... 0 .10 Horse, meat ...... 0 .05 specified below is to be determined by Horse, meat byproducts ...... 0 .20 measuring only free and conjugated Milk ...... 0.03 aminopyralid. Milk, fat ...... 0 .75 Poultry, liver ...... 0 .06 Commodity Parts per Sheep, fat ...... 0 .10 million Sheep, meat ...... 0.05 Corn, field, forage ...... 0 .30 Sheep, meat byproducts ...... 0 .20 Corn, field, grain ...... 0 .20 Corn, field, stover ...... 0 .20 (b) Section 18 emergency exemptions. Grain, aspirated fractions ...... 0 .2 [Reserved] Grass, forage ...... 25 (c) Tolerances with regional registra- Grass, hay ...... 50 Wheat, bran ...... 0.1 tions. [Reserved] Wheat, forage ...... 2 .0 (d) Indirect or inadvertent residues. Wheat, grain ...... 0 .04 Tolerances are established for the indi- Wheat, hay ...... 4 .0 Wheat, straw ...... 0 .25 rect or inadvertent residues of fluoxastrobin, including its metabo- (2) Tolerances are established for res- lites and degradates, in or on the com- idues of the herbicide aminopyralid, 4- modities in the table below, when amino-3,6-dichloro-2- present therein as a result of the appli- pyridinecarboxylic acid, including its cation of fluoxastrobin to the growing metabolites and degradates, in or on crops listed in paragraph (a)(1) of this the commodities in the table below. section. Compliance with the tolerance Compliance with the tolerance levels levels specified below is to be deter- specified below is to be determined by mined by measuring only measuring only aminopyralid. fluoxastrobin, (1E)-[2-[[6-(2- chlorophenoxy)-5-fluoro-4- Commodity Parts per pyrimidinyl]oxy]phenyl](5,6-dihydro- million 1,4,2-dioxazin-3-yl)methanone O- Cattle, fat ...... 0.02 methyloxime and its Z isomer, (1Z)-[2- Cattle, kidney ...... 0 .3 [[6-(2-chlorophenoxy)-5-fluoro-4- Cattle, meat ...... 0 .02 Cattle, meat byproducts, except kidney ...... 0.02 pyrimidinyl]oxy]phenyl](5,6-dihydro- Goat, fat ...... 0 .02 1,4,2-dioxazin-3-yl)methanone O- Goat, kidney ...... 0 .3

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tabolites M2, 8-(2,6-diethyl-4-methyl- Commodity Parts per million phenyl)-tetrahydro-pyrazolo[1,2- Goat, meat ...... 0.02 d][1,4,5]oxadiazepine-7,9-dione, and free Goat, meat byproducts, except kidney ...... 0 .02 and conjugated forms of M4, 8-(2,6- Horse, fat ...... 0 .02 diethyl-4-hydroxymethyl-phenyl)- Horse, kidney ...... 0 .3 Horse, meat ...... 0 .02 tetrahydro-pyrazolo[1,2-d][1,4,5] Horse, meat byproducts, except kidney ...... 0 .02 oxadiazepine-7,9-dione, calculated as Milk ...... 0.03 pinoxaden, in/on the following com- Sheep, fat ...... 0 .02 Sheep, kidney ...... 0.3 modities: Sheep, meat ...... 0.02 Sheep, meat byproducts, except kidney ...... 0 .02 Parts per Commodity million

(b) Section 18 emergency exemptions. Cattle, fat ...... 0.04 [Reserved] Cattle, meat ...... 0 .04 (c) Tolerances with regional registra- Cattle, meat byproducts ...... 0.04 tions. [Reserved] Milk ...... 0.02 (d) Indirect or inadvertent residues. (b) Section 18 emergency exemptions. [Reserved] [Reserved] [70 FR 46428, Aug. 10, 2005, as amended at 75 (c) Tolerances with regional registra- FR 17584, Apr. 7, 2010] tions. [Reserved] (d) Indirect or inadvertent residues. § 180.611 Pinoxaden; tolerances for [Reserved] residues. (a) General. (1) Tolerances are estab- [70 FR 43322, July 27, 2005] lished for the combined residues of pinoxaden (8-(2,6-diethyl-4- § 180.612 Topramezone; tolerances for residues. methylphenyl)-1,2,4,5-tetrahydro-7-oxo- 7H-pyrazolo[1,2-d][1,4,5] oxadiazepin-9- (a) General. Tolerances are estab- yl 2,2-dimethylpropanoate), and its me- lished for residues of the herbicide tabolites 8-(2,6-diethyl-4-methyl- topramezone, including its metabolites phenyl)-tetrahydro-pyrazolo[1,2- and degradates, in or on the following d][1,4,5]oxadiazepine-7,9-dione (M2), and commodities. Compliance with the fol- free and conjugated forms of 8-(2,6- lowing tolerance levels is to be deter- diethyl-4-hydroxymethyl-phenyl)- mined by measuring only topramezone tetrahydro-pyrazolo[1,2-d][1,4,5] ([3-(4,5-dihydro-3-isoxazolyl)-2-methyl- oxadiazepine-7,9-dione (M4), and 4-(7,9- 4-(methylsulfonyl)phenyl](5-hydroxy-1- dioxo-hexahydro-pyrazolo[1,2-d] methyl-1H-pyrazol-4-yl)methanone) in [1,4,5]oxadiazepin-8-yl)-3,5-diethyl-ben- or on the following commodities: zoic acid (M6), calculated as pinoxaden, Parts per in/on the following commodities: Commodity million

Cattle, meat byproducts ...... 0.80 Commodity Parts per million Corn, field, forage ...... 0 .05 Corn, field, grain ...... 0 .01 Barley, bran ...... 1 .6 Corn, field, stover ...... 0 .05 Barley, grain ...... 0 .9 Corn, pop, grain ...... 0.01 Barley, hay ...... 1 .5 Corn, pop, stover ...... 0.05 Barley, straw ...... 1 .0 Corn, sweet, forage ...... 0 .05 Egg ...... 0 .06 Corn, sweet, kernel plus cob with husks re- Poultry, fat ...... 0.06 moved ...... 0 .01 Poultry, meat ...... 0 .06 Poultry, meat byproducts ...... 0.06 Corn, sweet, stover ...... 0 .05 Wheat, bran ...... 3.0 Fish-freshwater finfish ...... 0.05 Wheat, forage ...... 3 .5 Fish-saltwater finfish ...... 0 .05 Wheat, grain ...... 1 .3 Fish-shellfish, crustacean ...... 0 .05 Wheat, hay ...... 2 .0 Fish-shellfish, mollusk ...... 0 .05 Wheat, straw ...... 1 .5 Goat, meat byproducts ...... 0 .80 Hog, meat byproducts ...... 0 .40 Horse, meat byproducts ...... 0 .80 (2) For the combined residues of Poultry, meat byproducts ...... 0.02 pinoxaden, 8-(2,6-diethyl-4- Sheep, meat byproducts ...... 0 .80 methylphenyl)-1,2,4,5-tetrahydro-7-oxo- 7H-pyrazolo[1,2-d][1,4,5] oxadiazepin-9- (b) Section 18 emergency exemptions. yl 2,2-dimethylpropanoate), and its me- [Reserved]

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(c) Tolerances with regional registra- degradates, in or on the commodities tions. [Reserved] in the table below. Compliance with (d) Indirect or inadvertent residues. the tolerance levels specified below is [Reserved] to be determined by measuring only the sum of flonicamid, N- [78 FR 48074, Aug. 7, 2013] (cyanomethyl)-4-(trifluoromethyl)-3- § 180.613 Flonicamid; tolerances for pyridinecarboxamide, and its metabo- residues. lites, TFNA (4- trifluoromethylnicotinic acid), and (a) General. (1) Tolerances are estab- TFNA–AM (4- lished for the residues of the insecti- trifluoromethylnicotinamide), cal- cide flonicamid, including its metabo- culated as the Stoichiometric equiva- lites and degradates, in or on the com- lent of flonicamid, in or on the fol- modities in the table below. Compli- lowing commodities. ance with the tolerance levels specified below is to be determined by measuring Parts per only the sum of flonicamid, N- Commodity million (cyanomethyl)-4-(trifluoromethyl)-3- Cattle, fat ...... 0.03 pyridinecarboxamide, and its metabo- Cattle, meat ...... 0 .08 lites, TFNA (4- Cattle, meat byproducts ...... 0.08 trifluoromethylnicotinic acid), TFNA– Egg ...... 0 .04 AM (4-trifluoromethylnicotinamide), Goat, fat ...... 0 .03 and TFNG, N-(4- Goat, meat ...... 0.08 Goat, meat byproducts ...... 0 .08 trifluoromethylnicotinoyl)glycine, cal- Hog, fat ...... 0 .03 culated as the stoichiometric equiva- Hog, meat ...... 0 .03 lent of flonicamid, in or on the fol- Hog, meat byproducts ...... 0 .03 lowing commodities. Horse, fat ...... 0 .03 Horse, meat ...... 0 .08 Parts per Horse, meat byproducts ...... 0 .08 Commodity million Milk ...... 0.05 Poultry, fat ...... 0.03 Alfalfa, forage ...... 10.0 Poultry, meat ...... 0 .03 Alfalfa, hay ...... 1.0 Poultry, meat byproducts ...... 0.03 Alfalfa, seed ...... 1 .5 Sheep, fat ...... 0 .03 Almond, hulls ...... 9 .0 Sheep, meat ...... 0.08 Berry, low growing, subgroup 13–07G ...... 1 .5 Sheep, meat byproducts ...... 0 .08 Brassica, head and stem, subgroup 5A ...... 1 .5 Brassica, leafy greens, subgroup 5B ...... 16 Cotton, gin byproducts ...... 6 .0 (b) Section 18 emergency exemptions. Cotton, hulls ...... 2 .0 [Reserved] Cotton, meal ...... 1 .0 Cotton, undelinted seed ...... 0 .50 (c) Tolerances with regional registra- Cucumber ...... 1 .5 tions. [Reserved] Fruit, pome, group 11–10 ...... 0 .20 (d) Indirect or inadvertent residues. Fruit, stone, group 12–12 ...... 0 .60 Hop, dried cones ...... 7 .0 [Reserved] Nut, tree, group 14–12 ...... 0 .15 [70 FR 51614, Aug. 31, 2005, as amended at 71 Okra ...... 0.40 Peppermint, tops ...... 7 .0 FR 15608, Mar. 29, 2006; 73 FR 17923, Apr. 2, Potato, granules/flakes ...... 0 .40 2008; 77 FR 67776, Nov. 14, 2012; 78 FR 75266, Radish, tops ...... 16 Dec. 11, 2013] Rapeseed subgroup 20A ...... 1 .5 Spearmint, tops ...... 7 .0 § 180.614 Kasugamycin; tolerances for Spinach ...... 9 .0 residues. Tomato, paste ...... 2 .0 Tomato, puree ...... 0 .50 (a) General. Tolerances are estab- Turnip, greens ...... 16 lished for residues of kasugamycin, in- Vegetable, cucurbit, group 9 ...... 1.5 Vegetable, fruiting, group 8–10 ...... 0 .40 cluding its metabolites and degradates, Vegetable, leafy, except brassica, group 4, ex- in or on the commodities listed in the cept spinach ...... 4 .0 following table. Compliance with the Vegetable, root, except sugar beet, subgroup 1B ...... 0 .60 tolerance levels specified is to be deter- Vegetable, tuberous and corm, subgroup 1C ..... 0.20 mined by measuring only kasugamycin (3-O-[2-amino-4-[(carboxyimino-meth- (2) Tolerances are established for the yl)amino]-2,3,4,6-tetradeoxy-a-D- residues of the insecticide flonicamid, arabino-hexopyranosyl]-D-chiro-ino- including its metabolites and sitol) in or on the commodity.

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(d) Indirect or inadvertent residues. Commodity Parts per million Tolerances are established for the indi- Fruit, pome, group 11–10 ...... 0 .20 rect or inadvertent residues of Vegetable, fruiting, group 8 1 ...... 0.04 amicarbazone [4-amino-4, 5-dihydro-N- 1 There is no U.S. registration as of September 1, 2005. (1,1-dimethylethyl)-3-(1-methylethyl)-5- oxo-1H-1,2,4-triazole-1-carboxamide] (b) Section 18 emergency exemptions. and its metabolites DA amicarbazone [Reserved] [N-(1,1-dimethylethyl)-4,5-dihydro-3-(1- (c) Tolerances with regional registra- methylethyl)-5-oxo-1H-1,2,4-triazole-1- tions. [Reserved] carboxamide] and iPr-2-OH DA (d) Indirect or inadvertent residues. amicarbazone [N-(1,1-dimethylethyl)- [Reserved] 4,5-dihydro-3-(1-hydroxy-1- [79 FR 51497, Aug. 29, 2014] methylethyl)-5-oxo-1H-1,2,4-triazole-1- carboxamide], calculated as parent § 180.615 Amicarbazone; tolerances for equivalents, in or on the following residues. commodities when present therein as a (a) General. Tolerances are estab- result of application of amicarbazone lished for combined residues of the her- to the growing crops in paragraph (a) bicide, amicarbazone [4-amino-4, 5- of this section: dihydro- N-(1,1-dimethylethyl)-3-(1- Parts per methylethyl)-5-oxo-1H-1,2,4-triazole-1- Commodity million carboxamide] and its metabolites DA Alfalfa, forage ...... 0.05 amicarbazone [N-(1,1-dimethylethyl)- Alfalfa, hay ...... 0.10 4,5-dihydro-3-(1-methylethyl)-5-oxo-1H- Cotton, gin byproducts ...... 0 .30 1,2,4-triazole-1-carboxamide] and iPr-2- Cotton, undelinted seed ...... 0 .07 Soybean, forage ...... 1 .50 OH DA amicarbazone [N-(1,1- Soybean, hay ...... 5 .0 dimethylethyl)-4,5-dihydro-3-(1-hy- Soybean, seed ...... 0 .80 droxy-1-methylethyl)-5-oxo-1H-1,2,4-tri- Wheat, bran ...... 0.15 Wheat, flour ...... 0 .15 azole-1-carboxamide], calculated as Wheat, forage ...... 0 .50 parent equivalents, in or on the fol- Wheat, germ ...... 0 .15 lowing commodities: Wheat, grain ...... 0 .10 Wheat, hay ...... 1 .0 Parts per Wheat, middlings, ...... 0.15 Commodity million Wheat, shorts ...... 0 .15 Wheat, straw ...... 0 .50 Cattle, fat ...... 0.01 Cattle, liver ...... 1 .0 Cattle, meat ...... 0 .01 [70 FR 55760, Sept. 23, 2005, as amended at 74 Cattle, meat byproducts, except liver ...... 0 .10 FR 46377, Sept. 9, 2009] Corn, field, forage ...... 0 .80 Corn, field, grain ...... 0 .05 § 180.616 Fenpropimorph; tolerances Corn, field, stover ...... 1 .0 for residues. Goat, fat ...... 0 .01 Goat, liver ...... 1.0 Tolerances are established for the Goat, meat ...... 0.01 residues of the fungicide Goat, meat byproducts, except liver ...... 0 .10 fenpropimorph (rel-(2R,6S)-4-[3-[4-(1,1- Hog, fat ...... 0 .01 dimethylethyl)phenyl]-2- Hog, liver ...... 0 .10 Hog, meat ...... 0 .01 methylpropyl]-2,6-dimethylmorpholine) Hog, meat byproducts, except liver ...... 0 .01 in or on the following commodity: Horse, fat ...... 0 .01 Horse, liver ...... 1 .0 Commodity Parts per Horse, meat ...... 0 .01 million Horse, meat byproducts, except liver ...... 0 .10 Milk ...... 0.01 Banana* ...... 2 .0 Sheep, fat ...... 0 .01 *No U.S. registration as of February 10, 2006. Sheep, liver ...... 1.0 Sheep, meat ...... 0.01 (b) Section 18 emergency exemptions. Sheep, meat byproducts, except liver ...... 0 .10 [Reserved] Poultry, liver ...... 0 .10 (c) Tolerances with regional registra- (b) Section 18 emergency exemptions. tions. [Reserved] [Reserved] (d) Indirect or inadvertent residues. (c) Tolerances with regional registra- [Reserved] tions. [Reserved] [71 FR 15612, Mar. 29, 2006]

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§ 180.617 Metconazole; tolerances for (c) Tolerances with regional registra- residues. tions. [Reserved] (a) General. Tolerances are estab- (d) Indirect or inadvertent residues. lished for residues of metconazole, in- [Reserved] cluding its metabolites and degradates, [71 FR 56388, Sept. 27, 2006, as amended at 71 in or on the commodities in the fol- FR 76196, Dec. 20, 2006; 73 FR 22828, Apr. 28, lowing table. Compliance with the tol- 2008; 74 FR 21266, May 7, 2009; 76 FR 50904, erance levels specified below is to be Aug. 17, 2011; 76 FR 81396, Dec. 28, 2011; 77 FR determined by measuring only 26456, May 4, 2012; 77 FR 66723, Nov. 7, 2012; 79 metconazole [5-[(4- FR 12411, Mar. 5, 2014; 80 FR 30625. May 29, 2015] chlorophenyl)methyl]-2,2-dimethyl-1- (1H-1,2,4-triazol-1- § 180.618 Benthiavalicarb-isopropyl; ylmethyl)cyclopentanol] as the sum of tolerance for residues. its cis- and trans-isomers in or on the (a) General. Tolerances are estab- following commodities: lished for the combined residues of Parts per benthiavalicarb-isopropyl, Commodity million isopropyl[(S)-1-[[[(1R)-1-(6-fluoro-2- Almond, hulls ...... 4 .0 benzothiazolyl)ethyl]amino] carbonyl]- Banana 1 ...... 0.1 2-methylpropyl]carbamate and Barley, grain ...... 2 .5 isopropyl[(S)-1-[[[(1S)-1-(6-fluoro-2- Barley, hay ...... 7 .0 Barley, straw ...... 7 .0 benzothiazolyl)ethyl]amino] carbonyl]- Beet, sugar, dried pulp ...... 0 .70 2-methylpropyl]carbamate, in or on the Beet, sugar, molasses ...... 0 .08 following raw agricultural commod- Beet, sugar, roots ...... 0 .07 ities: Bushberry subgroup 13–07B ...... 0 .40 Cattle, meat byproducts ...... 0.04 Corn, field, forage ...... 3 .0 Parts per Commodity million Corn, field, grain ...... 0 .02 Corn, field, stover ...... 30 Grape, imported ...... 0 .25 Corn, pop, grain ...... 0.02 Grape, raisin ...... 1 .0 Corn, pop, stover ...... 30 Tomato ...... 0.45 Corn, sweet, forage ...... 3 .0 Corn, sweet, kernel plus cob with husks re- Note: There are no U.S. registrations as of July 30, 2006. moved ...... 0 .01 Corn, sweet, stover ...... 30.0 (b) Section 18 emergency exemptions. Cotton, gin byproducts ...... 8 .0 [Reserved] Cotton, undelinted seed ...... 0 .25 (c) Tolerances with regional registra- Egg ...... 0 .04 Fruit, stone, group 12–12 ...... 0 .2 tions. [Reserved] Goat, meat byproducts ...... 0 .04 (d) Indirect of inadvertent residues. Grain, aspirated grain fractions ...... 7 .0 [Reserved] Horse, meat byproducts ...... 0 .04 Nut, tree, group 14–12 ...... 0 .04 [71 FR 52003, Sept. 1, 2006] Oat, grain ...... 1 .0 Oat, hay ...... 17 Oat, straw ...... 6.0 § 180.619 Epoxiconazole; tolerances for Pea and bean, dried shelled, except soybean, residues. subgroup 6C ...... 0 .15 (a) General. Tolerances are estab- Peanut ...... 0 .04 Peanut, refined oil ...... 0.05 lished for the residues of the fungicide Rapeseed subgroup 20A ...... 0 .08 epoxiconazole [(rel-1-[[(2R,3S)-3-(2- Rye, grain ...... 0.25 chlorophenyl)-2-(4- Rye, straw ...... 14 Sheep, meat byproducts ...... 0 .04 fluorophenyl)oxiranyl]methyl]-1H-1,2,4- Soybean, forage ...... 3 .0 triazole]) in or on the following com- Soybean, hay ...... 6 .0 modities: Soybean, hulls ...... 0 .08 Soybean, seed ...... 0 .05 Parts per Sugarcane, cane ...... 0.06 Commodity million Sunflower subgroup 20B ...... 0.7 Vegetable, tuberous and corn, subgroup 1C ...... 0.04 Banana* ...... 0 .5 Wheat, grain ...... 0 .15 Coffee* ...... 0 .05 Wheat, hay ...... 16 Wheat, milled byproducts ...... 0 .20 *No U.S. Registration as of August 4, 2006 Wheat, straw ...... 18 (b) Section 18 emergency exemptions. 1 No U.S. registration as of August 30, 2006. [Reserved] (b) Section 18 emergency exemptions. (c) Tolerances with regional Registra- [Reserved] tions. [Reserved]

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(d) Indirect or inadvertent residues. Commodity Parts per [Reserved] million [71 FR 53989, Sept. 13, 2006] Fruit, pome, group 111 ...... 5 Grape 2 ...... 3 1 § 180.620 Etofenprox; tolerances for Hop, dried cones ...... 100 residues. 1No U.S. registration as of September 5, 2006. 2No U.S. registration as of January 29, 2010. (a) General. A tolerance is established for residues of the insecticide (b) Section 18 emergency exemptions. etofenprox, including its metabolites [Reserved] and degradates, in or on the com- (c) Tolerances with regional registra- modity in the table in this paragraph. tions. [Reserved] Compliance with the tolerance level (d) Indirect or inadvertent residues. specified in this paragraph is to be de- [Reserved] termined by measuring only [75 FR 5522, Feb. 3, 2010] etofenprox, 2-(4-ethoxyphenyl)-2- methylpropyl 3-phenoxybenzyl ether, § 180.622 Ethaboxam; tolerances for in or on the commodity. residues. (a) General. Tolerances are estab- Parts per Commodity million lished for residues of ethaboxam, N- (cyano-2-thienylmethyl)-4-ethyl-2- Cattle, fat ...... 10.0 (ethlyamino)-5-thiazolecarboxamide in Cattle, meat ...... 0 .40 Cattle, meat byproducts ...... 10.0 or on the following commodity: Egg ...... 0 .40 All food commodities (including feed commod- Commodity Parts per ities) not otherwise listed in this subsection .... 5 .0 million Goat, fat ...... 10 .0 Goat, meat ...... 0.40 Grape 1 ...... 6 .0 Goat, meat byproducts ...... 10 .0 1 There is no U.S. registration as of September 27, 2006 Hog, fat ...... 4 .0 Hog, meat ...... 0 .20 (b) Section 18 emergency exemptions. Hog, meat byproducts ...... 4 .0 Horse, fat ...... 10 .0 [Reserved] Horse, meat ...... 0 .40 (c) Tolerances with regional registra- Horse, meat byproducts ...... 10 .0 tions. [Reserved] Milk ...... 0.60 Poultry, fat ...... 1.0 (d) Indirect or inadvertent residues. Poultry, meat ...... 0 .01 [Reserved] Poultry, meat byproducts ...... 1.0 Rice, grain ...... 0 .01 [71 FR 56392, Sept. 27, 2006] Sheep, fat ...... 10 .0 Sheep, meat ...... 0.40 § 180.623 Flufenoxuron; tolerances for Sheep, meat byproducts ...... 10 .0 residues. (b) Section 18 emergency exemptions. (a) General. Tolerances are estab- [Reserved] lished for residues of the insecticide, (c) Tolerances with regional registra- flufenoxuron, 1-[4-(2-chloro-a,a,a- tions. [Reserved] trifluoro-p-tolyloxy)-2-fluorophenyl]-3- (d) Indirect or inadvertent residues. (2,6-difluorobenzoyl)urea, in or on the [Reserved] following food commodities.

[76 FR 23498, Apr. 27, 2011, as amended at 78 Commodity Parts per FR 70877, Nov. 27, 2013] million Apple 1 ...... 0.50 § 180.621 Dithianon; tolerances for res- Cattle, fat 1 ...... 4.5 idues. Cattle, meat 1 ...... 0 .10 Cattle, meat byproducts 1 ...... 0.50 (a) General. Tolerances are estab- Goat, fat 1 ...... 4 .5 lished for residues of dithianon, includ- Goat, meat 1 ...... 0.10 ing its metabolites and degradates, in Goat, meat byproducts 1 ...... 0 .50 Grape 1 ...... 0 .70 or on the commodities in the table Grape, raisin 1 ...... 2 .0 below. Compliance with the tolerance Horse, fat 1 ...... 4 .5 levels specified below is to be deter- Horse, meat 1 ...... 0 .10 mined by measuring only dithianon, 5, Horse, meat byproducts 1 ...... 0 .50 Milk ...... 0.20 10-dihydro-5,10-dioxonaphtho(2,3-b)-1,4- Milk, fat 1 ...... 4 .0 dithiin-2,3-dicarbonitrile. Orange 1 ...... 0 .30

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phenylsulfamoyl] urea) per se in or on Commodity Parts per million the following commodities: Orange, oil 1 ...... 60 1 Parts per Pear ...... 0 .50 Commodity million Sheep, fat 1 ...... 4 .5 Sheep, meat 1 ...... 0.10 Rice, grain ...... 0 .05 Sheep, meat byproducts 1 ...... 0 .50 1There are no U.S. registrations as of September 30, 2006. (b) Section 18 emergency exemptions. [Reserved] (b) Section 18 emergency exemptions. (c) Tolerances with regional registra- [Reserved] tions. [Reserved] (c) Tolerances with regional restric- (d) Indirect and inadvertant residues. tions. [Reserved] [Reserved] (d) Indirect or inadvertent residues. [Reserved] [72 FR 8931, Feb. 28, 2007, as amended at 80 FR 72599, Nov. 20, 2015] [71 FR 57436, Sept. 29, 2006] § 180.626 Prothioconazole; tolerances § 180.624 Metrafenone; tolerances for for residues. residues. (a) General. (1) Tolerances are estab- (a) General. Tolerances are established for residues of prothioconazole, lished for residues of the fungicide 2-[2-(1-chlorocylcopropyl)-3-(2- metrafenone, including its metabolites chlorophenyl)-2-hydroxypropyl]-1,2- and degradates, in or on the commod- dihydro-3H-1,2,4-triazole-3-thion, in- ities in the table below. Compliance cluding its metabolites and degradates, with the tolerance levels specified in in or on the commodities in the table the following table is to be determined below. Compliance with the tolerance by measuring only metrafenone (3- levels specified below is to be deter- bromo-6-methoxy-2- mined by measuring only methylphenyl)(2,3,4-trimethoxy-6- prothioconazole and its metabolite methylphenyl)methanone in or on the prothioconazole-desthio, or a-(1- following commodities: chlorocyclopropyl)-a-[(2- Parts per chlorophenyl)methyl]-1H-1,2,4-triazole- Commodity million 1-ethanol, calculated as parent in or on the commodity. Apricot ...... 0 .70 Cherry subgroup 12–12A ...... 2 .0 Parts per Fruit, pome, group 11–10 ...... 1 .5 Commodity million Fruit, small, vine climbing, except fuzzy kiwifruit, subgroup 13–07F ...... 4 .5 Alfalfa, forage ...... 0.02 Grape, raisin ...... 17 Alfalfa, hay ...... 0.02 Hop, dried cones ...... 70 Beet, sugar, roots ...... 0 .25 Peach subgroup 12–12B ...... 0.70 Berry, low growing, except strawberry, subgroup Vegetable, cucurbit, group 9 ...... 0.50 13–07H ...... 0 .20 Vegetable, fruiting, group 8–10 ...... 0 .90 Bushberry, subgroup 13–07B ...... 2.0 Corn, sweet kernel plus cob with husks re- (b) Section 18 emergency exemption. moved ...... 0 .04 Grain, aspirated grain fractions ...... 11 [Reserved] Grain, cereal, forage, fodder and straw, group (c) Tolerances with regional registra- 16, except sorghum, and rice; forage ...... 8 .0 tions. [Reserved] Grain, cereal, forage, fodder and straw, group (d) Indirect or inadvertent residues. 16, except sorghum, and rice; hay ...... 7 .0 Grain, cereal, forage, fodder and straw, group [Reserved] 16, except sorghum, and rice; stover ...... 10 Grain, cereal, forage, fodder and straw, group [71 FR 54917, Sept. 20, 2006, as amended at 75 16, except sorghum, straw ...... 5 .0 FR 75393, Dec. 3, 2010; 79 FR 63053, Oct. 22, Grain, cereal, group 15, except sweet corn and 2014] sorghum ...... 0 .35 Pea and bean, dried shelled, except soybean, § 180.625 Orthosulfamuron; tolerances subgroup 6C ...... 0 .9 for residues. Peanut ...... 0 .02 Potato ...... 0 .02 (a) General. Tolerances are estab- Rapeseed, seed ...... 0 .15 lished for residues of orthosulfamuron Rice, hulls ...... 0 .90 Soybean, forage ...... 4 .5 1-(4,6-dimethoxypyrimidin-2-yl)-3-[2- Soybean, hay ...... 17 (dimethylcarbamoyl)- Soybean, seed ...... 0 .15

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determined by measuring only Commodity Parts per million fluopicolide [2,6-dichloro-N-[[3-chloro-5- Vegetable, cucurbit, crop group 9 ...... 0.30 (trifluoromethyl)-2- pyridinyl]methyl]benzamide] in or on (2) Tolerances are established for res- the commodity. idues of prothioconazole, 2-[2-(1- Parts per chlorocylcopropyl)-3-(2-chlorophenyl)- Commodity million 2-hydroxypropyl]-1,2-dihydro-3H-1,2,4- triazole-3-thion, including its metabo- Brassica, head and stem, subgroup 5A ...... 5 .0 Grape ...... 2 .0 lites and degradates, in or on the com- Grape, raisin ...... 6 .0 modities in the table below. Compli- Potato, processed potato waste ...... 1 .0 ance with the tolerance levels specified Vegetable, brassica (cole) leafy subgroup 5B .... 18 Vegetable, bulb, crop group 3–07 ...... 7.0 below is to be determined by measuring Vegetable, cucurbit, group 9 ...... 0.50 only prothioconazole and its metabo- Vegetable, fruiting, group 8 ...... 1.60 lites prothioconazole-desthio, or a-(1- Vegetable, leafy, except brassica, group 4 ...... 25 chlorocyclopropyl)-a-[(2- Vegetable, leaves of root and tuber, group 2 ..... 15 .0 Vegetable root, subgroup 1A ...... 0.15 chlorophenyl)methyl]-1H-1,2,4-triazole- Vegetable, tuberous and corm subgroup 1C ...... 0 .3 1-ethanol, and conjugates that can be converted to these two compounds by (b) Section 18 emergency exemptions. acid hydrolysis, calculated as parent in [Reserved] or on the commodity. (c) Tolerances with regional registrations. [Reserved] Parts per Commodity million (d) Indirect or inadvertent residues. Tolerances are established for residues Cattle, fat ...... 0.1 Cattle, meat ...... 0 .02 of the fungicide fluopicolide [2,6- Cattle, meat byproducts ...... 0.2 dichloro-N-[[3-chloro-5- Goat, fat ...... 0 .1 (trifluoromethyl)-2- Goat, meat ...... 0.02 Goat, meat byproducts ...... 0 .2 pyridinyl]methyl]benzamide], includ- Hog, meat byproducts ...... 0 .05 ing its metabolites and degradates, in Horse, fat ...... 0 .1 or on the commodities in the table in Horse, meat ...... 0 .02 Horse, meat byproducts ...... 0 .2 this paragraph. Compliance with the Milk ...... 0.02 tolerance levels specified below is to be Poultry liver ...... 0 .02 determined by measuring only Sheep, fat ...... 0 .1 Sheep, meat ...... 0.02 fluopicolide [2,6-dichloro-N-[[3-chloro-5- Sheep, meat byproducts ...... 0 .2 (trifluoromethyl)-2- pyridinyl]methyl]benzamide] in or on (b) Section 18 emergency exemptions. the commodity. [Reserved] Parts per (c) Tolerances with regional registra- Commodity million tions. [Reserved] (d) Indirect or inadvertent residues. Corn, field, forage ...... 0 .08 [Reserved] Corn, field, grain ...... 0 .01 Corn, field, stover ...... 0 .20 [72 FR 11783, Mar. 14, 2007, as amended at 73 Wheat, aspirated grain fractions ...... 0.07 FR 14719, Mar. 19, 2008; 74 FR 14749, Apr. 1, Wheat, forage ...... 0 .20 Wheat, grain ...... 0 .02 2009; 74 FR 46699, Sept. 11, 2009; 75 FR 29914, Wheat, hay ...... 0 .50 May 28, 2010; 76 FR 61592, Oct. 5, 2011; 78 FR Wheat, milled byproducts ...... 0 .07 67052, Nov. 8, 2013] Wheat, straw ...... 0 .50 § 180.627 Fluopicolide; tolerances for residues. [72 FR 14447, Mar. 28, 2007, as amended at 73 FR 5455, Jan. 30, 2008; 73 FR 30498, May 28, (a) General. Tolerances are estab- 2008; 76 FR 22054, Apr. 20, 2011; 79 FR 12401, lished for residues of the fungicide Mar. 5, 2014; 79 FR 45693, Aug. 6, 2014] fluopicolide [2,6-dichloro-N-[[3-chloro-5- (trifluoromethyl)-2- § 180.628 Chlorantraniliprole; toler- pyridinyl]methyl]benzamide], includ- ances for residues. ing its metabolites and degradates, in (a) General. Tolerances are estab- or on the commodities in the table in lished for residues of the insecticide this paragraph. Compliance with the chlorantraniliprole, including its me- tolerance levels specified below is to be tabolites and degradates, in or on the

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commodities in the table below. Com- Commodity Parts per pliance with the tolerance levels speci- million fied below is to be determined by meas- Herb subgroup 19A, dried leaves ...... 90 uring only chlorantraniliprole, 3- Herb subgroup 19A, fresh leaves ...... 25 bromo-N-[4-chloro-2-methyl-6- Hog, fat ...... 0 .05 Hog, meat ...... 0 .02 [(methylamino)carbonyl]phenyl]-1-(3- Hog, meat byproducts ...... 0 .05 chloro-2-pyridinyl)-1H-pyrazole-5- Hop, dried cones 1 ...... 90 carboxamide. Hop, dried cones ...... 40 Horse, fat ...... 0 .5 Parts per Horse, meat ...... 0 .1 Commodity million Horse, meat byproducts ...... 0 .5 Ilama ...... 4 .0 Acerola ...... 2.0 Jaboticaba ...... 2 .0 Alfalfa, seed ...... 7 .0 Longan ...... 4 .0 Almond, hulls ...... 5 .0 Lychee ...... 2 .0 Animal feed, nongrass, group 18, forage ...... 25 Mango ...... 4.0 Animal feed, nongrass, group 18, hay ...... 90 Milk ...... 0.1 Apple, wet pomace ...... 2 .5 Nut, tree, group 14 1 ...... 0 .04 Artichoke, globe 1 ...... 4.0 Nut, tree, group 14–12 ...... 0 .02 Artichoke, globe ...... 2.0 Olive ...... 4 .0 Asparagus ...... 13 Olive, oil ...... 40 Atemoya ...... 4 .0 Onion, bulb, subgroup 3–07A ...... 0 .30 Avocado ...... 4 .0 Onion, green, subgroup 3–07B ...... 3 .0 Banana ...... 4.0 Papaya ...... 4 .0 Beet, sugar, molasses ...... 9 .0 Passionfruit ...... 4 .0 Berry, large shrub/tree, subgroup 13–07C ...... 2 .5 Peanut ...... 0 .06 Berry, low growing, subgroup 13–07G ...... 1 .0 Peanut, hay ...... 90 Biriba ...... 4 .0 Peppermint, tops ...... 9 .0 Brassica, head and stem, subgroup 5A ...... 4 .0 Persimmon ...... 4 .0 Brassica, leafy greens, subgroup 5B ...... 11 Pineapple ...... 1.5 Bushberry, subgroup 13–07B ...... 2.5 Pineapple, process residue ...... 3 .0 Cacao bean ...... 0 .08 Pistachio 1 ...... 0.04 Cacao bean, chocolate ...... 1 .5 Pomegranate ...... 4 .0 Cacao bean, cocoa powder ...... 1 .5 Poultry, fat ...... 0.2 Cacao bean, roasted bean ...... 0 .8 Poultry, meat ...... 0 .05 Cactus ...... 13 Poultry, meat byproducts ...... 0.2 Canistel ...... 4 .0 Pulasan ...... 4 .0 Cattle, fat ...... 0.5 Rambutan ...... 4 .0 Cattle, meat ...... 0 .1 Rapeseed subgroup 20A ...... 2 .0 Cattle, meat byproducts ...... 0.5 Rice, grain ...... 0 .15 Cherimoya ...... 4 .0 Rice, hulls ...... 0 .4 Citrus, dried pulp ...... 14 Sapodilla ...... 4 .0 Coffee, green bean ...... 0 .4 Sapote, black ...... 4 .0 Coffee, instant ...... 2 .0 Sapote, mamey ...... 4 .0 Corn, field, grain ...... 0 .04 Sapote, white ...... 4 .0 Corn, field, milled byproducts ...... 0 .1 Sheep, fat ...... 0 .5 Corn, pop, grain ...... 0.04 Sheep, meat ...... 0.1 Corn, sweet, kernel plus cobs with husk re- Sheep meat byproducts ...... 0 .5 moved ...... 0 .02 Soursop ...... 4 .0 Cotton, gin byproduct ...... 30 Spanish lime ...... 4 .0 Cotton, hulls ...... 0 .40 Spearmint, tops ...... 9 .0 Cottonseed subgroup 20C ...... 0 .3 Spice, subgroup 19B ...... 90 Crayfish ...... 8.0 Star apple ...... 4 .0 Custard apple ...... 4 .0 Starfruit ...... 4 .0 Egg ...... 1 .0 Sugar apple ...... 4 .0 Feijoa ...... 4 .0 Sugarcane, cane ...... 14 Fig ...... 4 .0 Sugarcane, molasses ...... 420 Fruit, caneberry, subgroup 13–07A ...... 1 .8 Sunflower subgroup 20B ...... 2.0 Fruit, citrus, group 10–10 ...... 1 .4 Tea, dried ...... 50 .0 Fruit, pome, group 11–10 ...... 1 .2 Ti, leaves ...... 13 .0 Fruit, small vine climbing, subgroup 13–07F ...... 2.5 Ti, root ...... 0 .3 Fruit, stone, group 12–12 ...... 2 .5 Vegetable, cucurbit, group 9 ...... 0.5 Fruit, stone, group 12–12, except cherry, chicka- Vegetable, foliage of legume, group 7 ...... 90 saw plum, and damson plum 1 ...... 4 .0 Vegetable, fruiting, group 8–10 ...... 1 .4 Goat, fat ...... 0 .5 Vegetable, leafy, except brassica, group 4 ...... 13 Goat, meat ...... 0.1 Vegetable, leaves of root and tuber, group 2 ..... 40 .0 Goat, meat byproducts ...... 0 .5 Vegetable, legume, group 6 ...... 2 .0 Grain, aspirated grain fractions ...... 640 Vegetable, root and tuber, group 1 ...... 0 .30 Grain, cereal, except rice and corn, group 15 .... 6.0 Wax jambu ...... 4 .0 Grain, cereal, forage, fodder and straw, group 16 ...... 40 1 This tolerance expires on December 14, 2016. Grape, raisin ...... 5 .0 Grass forage, fodder and hay, group 17 ...... 90 (b) Section 18 emergency exemptions. Guava ...... 4 .0 [Reserved]

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(c) Tolerances with regional registra- Commodity Parts per tions. [Reserved] million (d) Indirect or inadvertent residues. Hog, fat ...... 0 .01 [Reserved] Hog, meat byproducts ...... 0 .05 Hog, muscle ...... 0.01 [75 FR 5532, Feb. 3, 2010, as amended at 75 FR Hop, dried cones ...... 20 17566, Apr. 7, 2010; 76 FR 44821, July 27, 2011; Horse, fat ...... 0 .05 76 FR 59909, Sept. 28, 2011; 77 FR 60315, Oct. 3, Horse, liver ...... 1 .0 2012; 77 FR 75561, Dec. 21, 2012; 78 FR 57285, Horse, meat byproducts, except liver ...... 0 .05 Sept. 18, 2013; 79 FR 7401, Feb. 7, 2014; 81 FR Horse, muscle ...... 0.05 38604, June 14, 2016] Japanese horse-chestnut ...... 0 .02 Lettuce, head ...... 1.5 Macadamia nut ...... 0 .02 § 180.629 Flutriafol; tolerances for resi- Milk ...... 0.02 dues. Mongongo nut ...... 0 .02 (a) General. Tolerances are estab- Monkey-pot ...... 0 .02 Pachira nut ...... 0 .02 lished for the residues of flutriafol, Peanut ...... 0 .09 [(±)-a-(2-fluorophenyl)-a-(4- Peanut, hay ...... 15 fluorophenyl)-1H-1,2,4-triazole-1-eth- Pecan ...... 0 .02 anol], including its metabolites and Poultry, fat ...... 0.01 Poultry, meat byproducts ...... 0.01 degradates in or on the following com- Radicchio ...... 1.5 modities. Compliance with the fol- Sapucaia nut ...... 0.02 lowing tolerances is to be determined Sheep, fat ...... 0 .05 by measuring flutriafol only. Sheep, liver ...... 1.0 Sheep, meat byproducts, except liver ...... 0 .05 Sheep, muscle ...... 0 .05 Parts per Commodity million Sorghum, grain, forage ...... 2.0 Sorghum, grain, grain ...... 1 .5 African tree nut ...... 0 .02 Sorghum, grain, stover ...... 6 .0 Almond ...... 0.60 Soybean, seed ...... 0 .35 Almond, hull ...... 15 Strawberry ...... 1 .5 Banana 1 ...... 0.30 Tomato, paste ...... 1 .5 Beet sugar ...... 0 .08 Vegetable, cucurbit, group 9 ...... 0.30 Brassica, head and stem (subgroup 5A) ...... 1 .5 Vegetable, fruiting, group 8–10 ...... 1 .0 Brassica, leafy greens (subgroup 5B) ...... 7 .0 Vegetable, leafy, except Brassica, crop group 4, Brazil nut ...... 0 .02 except head lettuce and radicchio ...... 10 Bur oak ...... 0 .02 Walnut, black ...... 0 .02 Butternut ...... 0 .02 Walnut, English ...... 0.02 Cajou ...... 0 .02 Wheat, bran ...... 0.30 Cashew ...... 0 .02 Wheat, forage ...... 30 Castanha-do-maranhao ...... 0.02 Wheat, germ ...... 0 .25 Cattle, fat ...... 0.05 Wheat, grain ...... 0 .15 Cattle, liver ...... 1 .0 Wheat, hay ...... 15 Cattle, meat byproducts, except liver ...... 0 .05 Wheat, straw ...... 9 .0 Cattle, muscle ...... 0 .05 1 Coconut ...... 0 .02 There are no U.S. registrations as of October 22, 2013. Coffee, green, bean 1 ...... 0 .15 (b) Section 18 emergency exemptions. Coffee, instant 1 ...... 0 .30 Coquito nut ...... 0 .02 [Reserved] Corn, field, forage ...... 5 .0 (c) Tolerances with regional registra- Corn, field, grain ...... 0 .01 tions [Reserved] Corn, field, refined oil ...... 0 .02 Corn, field, stover ...... 15 (d) Indirect or inadvertent residues. Corn, pop ...... 0 .01 Tolerances are established for the indi- Corn, pop, stover ...... 15 rect or inadvertent residues of the fun- Cotton, gin byproducts ...... 6 .0 gicide flutriafol, including its metabo- Cotton, undelinted seed ...... 0 .50 Dika nut ...... 0 .02 lites and degradates, in or on the com- Egg ...... 0 .01 modities in the table below when Fruit, pome, group 11–09 ...... 0 .40 present therein as a result of the appli- Fruit, stone, group 12–10 ...... 1 .5 Goat, fat ...... 0 .05 cation of flutriafol to the growing Goat, liver ...... 1.0 crops listed in the table to paragraph Goat, meat byproducts, except liver ...... 0 .05 (a) of this section. Compliance with the Goat, muscle ...... 0 .05 following tolerance levels specified Grain, aspirated fractions ...... 6 .0 Grape ...... 1 .5 below is to be determined by measuring Grape, raisin ...... 2 .4 only flutriafol ((±)-a-(2-fluorophenyl)-a- Guiana chestnut ...... 0 .02 (4-fluorophenyl)-1H-1,2,4-triazole-1-eth- Hazelnut ...... 0 .02 Heartnut ...... 0 .02 anol) in or on the following commod- Hickory nut ...... 0 .02 ities:

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calculated as the stoichiometric equiv- Commodity Parts per million alent of pyrasulfotole, in or on the Corn, sweet, forage ...... 0 .09 commodities: Corn, sweet, kernel plus cob with husk removed 0.01 Corn, sweet, stover ...... 0 .07 Parts per Commodity million

[75 FR 26673, May 12, 2010, as amended at 76 Aspirated grain fractions ...... 0 .40 FR 69647, Nov. 9, 2011; 77 FR 47301, Aug. 8, Barley, grain ...... 0 .02 Barley, hay ...... 0 .30 2012; 77 FR 48901, Aug. 15, 2012; 78 FR 75262, Barley, straw ...... 0 .20 Dec. 11, 2013; 79 FR 32673, June 6, 2014; 80 FR Cattle, fat ...... 0.03 5951, Feb. 4, 2015; 80 FR 71952, Nov. 18, 2015] Cattle, liver ...... 3 .0 Cattle, meat ...... 0 .02 § 180.630 Flusilazole; tolerances for Cattle, meat byproducts, except liver ...... 0 .70 residues. Eggs ...... 0 .02 Goat, fat ...... 0 .03 (a) General. [Reserved] Goat, liver ...... 3.0 (b) Section 18 emergency exemptions. Goat, meat ...... 0.02 Goat, meat byproducts, except liver ...... 0 .70 Time-limited tolerances are estab- Grass, forage ...... 25 lished for residues of the fungicide, Grass, hay ...... 3 .5 flusilazole, (1-[[bis(4- Hog, fat ...... 0 .02 Hog, liver ...... 0 .30 fluorophenyl)methylsilyl]methyl]-1H- Hog, meat ...... 0 .02 1,2,4-triazole) in connection with use of Hog, meat byproducts, except liver ...... 0 .05 the pesticide under Section 18 emer- Horse, fat ...... 0 .03 Horse, liver ...... 3 .0 gency exemptions granted by EPA. The Horse, meat ...... 0 .02 tolerances expire and are revoked on Horse, meat byproducts, except liver ...... 0 .70 the dates specified in the following Milk ...... 0.03 table. Oat, forage ...... 0 .10 Oat, grain ...... 0 .08 Oat, hay ...... 0.50 Expiration/ Commodity Parts per revocation Oat, straw ...... 0.20 million date Poultry, fat ...... 0.02 Poultry, meat ...... 0 .02 Soybean, aspirated grain fractions 2.6 12/31/10 Poultry, meat byproducts ...... 0.20 Soybean, seed ...... 0.04 12/31/10 Rye, forage ...... 0 .20 Soybean, oil ...... 0.10 12/31/10 Rye, grain ...... 0.02 Rye, straw ...... 0 .20 (c) Tolerances with regional registra- Sheep, fat ...... 0 .03 Sheep, liver ...... 3.0 tions. [Reserved] Sheep, meat ...... 0.02 (d) Indirect or inadvertant residues. Sheep, meat byproducts, except liver ...... 0 .70 [Reserved] Sorghum, grain, forage ...... 1.5 Sorghum, grain, grain ...... 0 .70 [72 FR 49660, Aug. 29, 2007] Sorghum, grain, stover ...... 0 .80 Wheat, forage ...... 0 .20 EFFECTIVE DATE NOTE: At 81 FR 34907, June Wheat, grain ...... 0 .02 1, 2016, § 180.630 was removed, effective Nov. Wheat, hay ...... 0 .80 28, 2016. Wheat, straw ...... 0 .20

§ 180.631 Pyrasulfotole; tolerances for (b) Section 18 emergency exemptions. residues. [Reserved] (a) General. Tolerances are estab- (c) Tolerances with regional registra- lished for residues of the herbicide tions. [Reserved] pyrasulfotole, including its metabo- (d) Indirect or inadvertent residues. lites and degradates, in or on the com- [Reserved] modities in the table below. Compli- [72 FR 45649, Aug. 15, 2007, as amended at 76 ance with the tolerance levels specified FR 23898, Apr. 29, 2011] below is to be determined by measuring only the sum of pyrasulfotole ((5-hy- § 180.632 Fenazaquin; Tolerances for droxy-1,3-dimethyl-1H-pyrazol-4-yl)[2- residues. (methylsulfonyl)-4- (a) General. Tolerances are estab- (trifluoromethyl)phenyl]methanone) lished for residues of the insecticide and its desmethyl metabolite (5-hy- fenazaquin, including its metabolites droxy-3-methyl-1H-pyrazol-4-yl)[2- and degradates, in or on the commod- (methylsulfonyl)-4- ities in the table below. Compliance (trifluoromethyl)phenyl]methanone), with the tolerance levels specified

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below is to be determined by measuring ities listed in the table to this para- only fenazaquin, or 4-[2-[4-(1,1- graph. Compliance with the tolerance dimethylethyl)phenyl]- levels specified below is to be deter- ethoxy]quinazoline. mined by measuring only the sum of tembotrione, 2-[2-chloro-4- Parts per Commodity million (methylsulfonyl)-3-[(2,2,2- trifluoroethoxy)methyl]benzoyl]-1,3- Almond ...... 0.02 Almond, hulls ...... 4 .0 cyclohexanedione and its metabolite, 2- Apple ...... 0.2 [2-chloro-4-(methylsulfonyl)-3-[(2,2,2- Cherry ...... 2.0 trifluoroethoxy) methyl]benzoyl]-4,6- Citrus Oil ...... 10 Fruit, Citrus, Group 10 except Grape fruit ...... 0 .5 dihydroxy-1,3-cyclohexanedione, cal- Pear ...... 0 .2 culated as the stoichiometric equivalent of tembotrione, in or on the fol- (b) Section is emergency exempotions. lowing commodities. [Reserved] (c) Tolerances with regional registra- Commodity Parts per tion. [Reserved] million (d) Indirect or inadvertent residues. Cattle, liver ...... 0 .40 [Reserved] Cattle, meat byproducts, except liver ...... 0 .07 [72 FR 44393, Aug. 8, 2007, as amended at 80 Corn, field, forage ...... 0 .60 FR 25958, May 6, 2015] Corn, field, grain ...... 0 .02 Corn, field, stover ...... 0 .45 § 180.633 Florasulam; tolerances for Corn, pop, grain ...... 0.02 residues. Corn, pop, stover ...... 0.35 Corn, sweet, forage ...... 0 .35 (a) General. Tolerances are estab- Corn, sweet, stover ...... 0 .60 lished for residues of the herbicide Goat, liver ...... 0.40 florasulam N-(2,6-difluorophenyl)-8- Goat, meat byproducts, except liver ...... 0 .07 fluoro-5-methoxy(1,2,4)triazolo(1,5- Horse, liver ...... 0 .40 c)pyrimidine-2-sulfonamide in or on Horse, meat byproducts, except liver ...... 0 .07 Poultry, liver ...... 0 .07 the following commodities: Sheep, liver ...... 0.40 Sheep, meat byproducts, except liver ...... 0 .07 Parts per Commodity million (2) Tolerances are established for res- Barley, grain ...... 0 .01 Barley, hay ...... 0 .05 idues of the herbicide tembotrione, in- Barley, straw ...... 0 .05 cluding its metabolites and degradates, Oat, forage ...... 0 .05 in or on the commodities listed in the Oat, grain ...... 0 .01 Oat, hay ...... 0.05 table to this paragraph. Compliance Oat, straw ...... 0.05 with the tolerance levels specified Rye, forage ...... 0 .05 below is to be determined by measuring Rye, grain ...... 0.01 Rye, straw ...... 0 .05 only tembotrione, 2-[2-chloro-4- Wheat, forage ...... 0 .05 (methylsulfonyl)-3-[(2,2,2- Wheat, grain ...... 0 .01 trifluoroethoxy)methyl]benzoyl]-1,3- Wheat, hay ...... 0 .05 Wheat, straw ...... 0 .05 cyclohexanedione in or on the following commodities. (b) Section 18 emergency exemptions. Parts per [Reserved] Commodity million (c) Tolerances with regional registrations. [Reserved] Corn, sweet, kernel plus cob with husks re- (d) Indirect or inadvertent residues. moved ...... 0 .01 [Reserved] (b) Section 18 emergency exemptions. [72 FR 55077, Sept. 28, 2007] [Reserved] § 180.634 Tembotrione; tolerances for (c) Tolerances with regional registra- residues. tions. [Reserved] (d) Indirect or inadvertent residues. (a) General. (1) Tolerances are estab- [Reserved] lished for residues of the herbicide tembotrione, including its metabolites [72 FR 55085, Sept. 28, 2007, as amended at 74 and degradates, in or on the commod- FR 47894, Sept. 18, 2009]

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§ 180.635 Spinetoram; tolerances for Commodity Parts per residues. million (a) General. Tolerances are estab- Caneberry subgroup 13–07A ...... 0.80 lished for residues of the insecticide Canistel ...... 0 .30 Cattle, fat ...... 5.5 spinetoram, including its metabolites Cattle, liver ...... 0 .85 and degradates, in or on the commod- Cattle, meat ...... 0 .20 ities in the table below. Compliance Cattle, meat byproducts (except liver) ...... 0 .60 Cherimoya ...... 0 .30 with the tolerance levels specified Citrus, dried pulp ...... 0 .50 below is to be determined by measuring Citrus, oil ...... 3.0 only the sum of XDE–175–J: 1-H-as- Coffee, green bean ...... 0 .04 indaceno[3,2-d]oxacyclododecin-7,15- Corn, sweet, kernel plus cob with husks removed ...... 0 .04 dione,2-[(6deoxy-3-O-ethyl-2,4-di-O- Cotton, gin byproducts ...... 1 .5 methyl-a-L-mannopyranosyl)oxy]-13- Cottonseed subgroup 20C ...... 0 .04 [[(2R,5S,6R)-5(dimethylamino) Cranberry ...... 0 .04 Custard apple ...... 0 .30 tetrahydro-6-methyl-2H-pyran-2-yl] Date ...... 0 .10 oxy]-9-ethyl-2,3,3a,4,5,5a,5b,6,9,10,11,12, Egg ...... 0 .04 13,14,16a,16b-hexadecahydro-14-methyl-, Feijoa ...... 0 .30 (2 Fig ...... 0 .10 Fruit, citrus, group 10–10 ...... 0 .30 XDE–175–L: 1 Fruit, pome, group 11–10 ...... 0 .20 oxacyclododecin-7,15-dione,2-[(6deoxy-3 Fruit, small, vine climbing, subgroup 13–07F, - except fuzzy kiwifruit ...... 0 .50 Fruit, stone 12–12 ...... 0.30 mannopyranosyl)oxy]-13-[[(2 Goat, fat ...... 5 .5 (dimethylamino)tetrahydro-6-methyl- Goat, liver ...... 0.85 2H-pyran-2-yl]oxy]-9-ethyl-2,3,3a,5a,5b, Goat, meat ...... 0.20 6,9,10,11,12,13,14,16a,16b-tetradecahydro- Goat, meat byproducts (except liver) ...... 0.60 Grain, aspirated fractions ...... 20 4,14-dimethyl-,(2 Grain, cereal, group 15, except rice, sorghum, R,16a pearl millet and proso millet ...... 0 .04 13 Grain, cereal, group 16, forage ...... 3 .5 [[(2S,5 Grain, cereal, group 16, hay ...... 10 Grain, cereal, group 16, stover ...... 10 tetrahydro-2H-pyran-2-yl]oxy]-7,15- Grain, cereal, straw, group 16, except rice ...... 1 .0 dioxo2,3,3a,4,5,5a,5b,6,7,9,10,11,12,13,14,15, Grape, raisin ...... 0 .70 16a,16b-octadecahydro-1H-as-indaceno Guava ...... 0 .30 [3,2d]oxacyclododecin-2-yl-6-deoxy-3-O- Herb, dried, subgroup 19A ...... 22 Herb, fresh, subgroup 19A ...... 3 .0 ethyl-2,4-di-O-methyl-a-L- Hog, fat ...... 0 .40 mannopyranoside; and NF–J: (2R,3S,6S)-6 Hog, meat ...... 0 .04 -([(2R,3aR,5aR,5bS,9S,13S,14R,16aS,16bR)- Hog, meat byproducts ...... 0 .04 Hop, dried cones ...... 22 2-[(6-deoxy-3- Horse, fat ...... 5 .5 L-mannopyranosyl)oxy]-9-ethyl-14-methyl Horse, liver ...... 0 .85 -7,15-dioxo-2,3,3a,4,5,5a,5b,6,7,9,10,11,12, Horse, meat ...... 0 .20 13,14,15,16a,16b-octadecahydro-1H-as- Horse, meat byproducts (except liver) ...... 0 .60 Ilama ...... 0 .30 indaceno[3,2d]oxacyclododecin-13-yl]oxy)- Jaboticaba ...... 0 .30 2-methyltetrahydro-2H-pyran-3-yl(methyl)Longan ...... 0 .30 formamide, calculated as the stoichio-Lychee ...... 0 .30 Mango ...... 0.30 metric equivalent of spinetoram. Milk ...... 0.30 Milk, fat ...... 7 .5 Parts per Millet, pearl, grain ...... 1 .0 Commodity million Millet, proso, grain ...... 1 .0 Acerola ...... 0.30 Nut, tree, group 14–12 ...... 0 .10 Almond, hulls ...... 19 Onion, bulb, subgroup 3–07A ...... 0 .10 Amaranth grain, grain ...... 1 .0 Onion, green, subgroup 3–07B ...... 2 .0 Apple, wet pomace ...... 0 .50 Papaya ...... 0 .30 Artichoke, globe ...... 0.30 Passionfruit ...... 0 .30 Asparagus ...... 0.04 Pea and bean, dried shelled, except soybean, Atemoya ...... 0 .30 subgroup 6C ...... 0 .04 Avocado ...... 0 .30 Pea and bean, succulent shelled, subgroup 6B 0 .04 Banana ...... 0.25 Peanut ...... 0 .04 Beet, sugar, molasses ...... 0 .75 Peanut, hay ...... 11 Berry, low growing, subgroup 13–07G, except Peppermint, tops ...... 3 .5 cranberry ...... 0.90 Pineapple ...... 0.04 Biriba ...... 0 .30 Pineapple, processed residue ...... 0 .15 Brassica, head and stem, subgroup 5A ...... 2 .0 Pomegranate ...... 0 .30 Brassica, leafy greens, subgroup 5B ...... 10 Poultry, fat ...... 0.10 Bushberry subgroup 13–07B ...... 0 .50 Poultry, meat ...... 0 .04

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(d) Indirect or inadvertent residues. Commodity Parts per million [Reserved] Poultry, meat byproducts ...... 0.04 [73 FR 8218, Feb. 13, 2008] Pulasan ...... 0 .30 Quinoa, grain ...... 0 .04 Rambutan ...... 0 .30 § 180.637 Mandipropamid; tolerances Sapodilla ...... 0 .30 for residues. Sapote, black ...... 0 .30 Sapote, mamey ...... 0 .30 (a) General. Tolerances are estab- Sapote, white ...... 0 .30 lished for residues of mandipropamid, Sheep, fat ...... 5 .5 Sheep, liver ...... 0.85 including its metabolites and Sheep, meat ...... 0.20 degradates, in or on the commodities Sheep, meat products (except liver) ...... 0 .60 listed in the table below. Compliance Sorghum, grain, grain ...... 1 .0 Soursop ...... 0 .30 with the tolerance levels specified Soybean, seed ...... 0 .04 below is to be determined by measuring Spanish lime ...... 0 .30 only mandipropamid (4-chloro-N-[2-[3- Spearmint, tops ...... 3 .5 Spice, subgroup 19B, except black pepper ...... 1 .7 methoxy-4-(2- Star apple ...... 0 .30 propynyloxy)phenyl]ethyl]-a-(2- Star fruit ...... 0 .30 propynyloxy)benzeneacetamide) in or Sugar apple ...... 0 .30 Ti, leaves ...... 10 on the commodity. Vegetable, cucurbit, group 9 ...... 0.30 Vegetable, foliage of legume, group 7 ...... 8 .0 Commodity Parts per Vegetable, fruiting, group 8–10 ...... 0 .40 million Vegetable, leafy, except Brassica, group 4 ...... 8 .0 Vegetable, leaves of root and tuber, group 2 ..... 10 Basil, dried leaves ...... 200 Vegetable, legume, edible podded, subgroup 6A 0 .30 Basil, fresh leaves ...... 30 Vegetable, root and tuber, group 1 ...... 0 .10 Bean, snap ...... 0 .90 Watercress ...... 8 .0 Brassica, head and stem, subgroup 5A ...... 3 Wax jambu ...... 0 .30 Brassica, leafy greens, subgroup 5B ...... 25 Fruit, small vine climbing, except fuzzy kiwifruit, (b) Section 18 emergency exemptions. subgroup 13–07F ...... 1 .4 [Reserved] Ginseng ...... 0 .30 (c) Tolerances with regional registra- Grape, raisin ...... 3 .0 tion. [Reserved] Hop, dried cones ...... 50 (d) Indirect and invertent residues. [Re- Onion, bulb, subgroup 3–07A ...... 0 .05 Onion, green, subgroup 3–07B ...... 4 .0 served] Potato, wet peel ...... 0 .15 [72 FR 57499, Oct. 10, 2007, as amended at 73 Vegetable, cucurbit, group 9 ...... 0.6 FR 14714, Mar. 19, 2008; 74 FR 40759, Aug. 13, Vegetable, fruiting, group 8–10 ...... 1 .0 2009; 80 FR 80282, Dec. 24, 2015] Vegetable, leafy except Brassica, group 4 ...... 20 Vegetable, tuberous and corm, subgroup 1C ..... 0.09 § 180.636 1,3-dichloropropene; tolerances for residues. (b) Section 18 emergency exemptions. Time-limited tolerances are estab- (a) General. Tolerances are established for residues of mandipropamid, lished for the combined residues of the including its metabolites and fungicide cis- and trans-1,3- dichloropropene and its metabolites degradates, in or on the commodities cis- and trans-3-chloroacrylic acid, and listed in the table below resulting from cis- and trans-3-chloroallyl alcohol in or use of the pesticide pursuant to on the following commodities. FFIFRA section 18 emergency exemptions. Compliance with the tolerance Commodity Parts per levels specified below is to be deter- million mined by measuring only Grape ...... 0.018 mandipropamid (4-chloro-N-[2-[3- methoxy-4-(2- (b) Section 18 emergency exemptions. propynyloxy)phenyl]ethyl]-a-(2- [Reserved] propynyloxy)benzeneacetamide) in or (c) Tolerances with regional registra- on the commodity. The tolerances ex- tions. [Reserved] pire on the date specified in the table.

Parts per Expiration/revocation Commodity million date

Basil, dried ...... 240 12/31/15

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(c) Tolerances with regional registra- Commodity Parts per tions. [Reserved] million (d) Indirect or inadvertent tolerances. Corn, sweet, kernel plus cob with husks re- [Reserved] moved ...... 0 .01 Corn, sweet, stover ...... 25 [73 FR 2816, Jan. 16, 2008, as amended at 74 Cotton gin byproducts ...... 60 FR 33169, July 10, 2009; 76 FR 55804, Sept. 9, Cotton, undelinted seed ...... 0 .90 2011; 77 FR 74119, Dec. 13, 2012; 78 FR 76992, Fruit, pome, group 11 ...... 1.5 Dec. 20, 2013; 81 FR 17088, Mar. 28, 2016] Fruit, stone, group 12 ...... 1 .6 Grape ...... 1 .4 Nut, tree, group 14 ...... 0 .06 § 180.638 Pyroxsulam; tolerances for Okra ...... 0.30 residues. Vegetable, cucurbit, group 9 ...... 0.20 Vegetable, fruiting, group 8 ...... 0.60 (a) General. Tolerances are estab- Vegetable, leafy, except Brassica, group 4 ...... 11 lished for residues of the herbicide pyroxsulam, N-(5,7- (2) Tolerances are established for res- dimethoxy[1,2,4]triazolo[1,5- idues of flubendiamide, including its a]pyrimidin-2-yl)-2-methoxy-4- metabolites and degradates, in or on (trifluoromethyl)-3- the commodities in the table below. pyridinesulfonamide in or on the raw Compliance with the tolerance levels agricultural commodities: specified in the table is to be determined by measuring only Parts per 2 Commodity million flubendiamide N -[1,1-dimethyl-2- (methylsulfonyl)ethyl]-3-iodo-N1-[2- Wheat, forage ...... 0 .06 methyl-4-[1,2,2,2-tetrafluoro-1- Wheat, grain ...... 0 .01 Wheat, hay ...... 0 .01 (trifluoromethyl)ethyl]phenyl]-1,2- Wheat, straw ...... 0 .03 benzenedicarboxamide, in or on the following commodities: (b) Section 18 emergency exemptions. Parts per [Reserved] Commodity million (c) Tolerances with regional registrations. [Reserved] Alfalfa, forage ...... 25 Alfalfa, hay ...... 65 (d) Indirect or inadvertent residues. Artichoke, globe ...... 1.6 [Reserved] Berry, low growing, subgroup 13–07G, except cranberry ...... 1.5 [73 FR 10402, Feb. 27, 2008] Brassica, head and stem, subgroup 5A ...... 3 .0 Brassica, leafy greens, subgroup 5B ...... 25 § 180.639 Flubendiamide; tolerances Cattle, fat ...... 0.70 Cattle, meat ...... 0 .08 for residues. Cattle, meat byproducts ...... 0.60 (a) General. (1) Tolerances are estab- Egg ...... 0 .40 Fruit, small fruit vine climbing except fuzzy lished for residues of flubendiamide, in- kiwifruit, subgroup 13–07F ...... 1 .4 cluding its metabolites and degradates, Goat, fat ...... 0 .70 in or on the commodities in the table Goat, meat ...... 0.08 below. Compliance with the tolerance Goat, meat byproducts ...... 0 .60 Grain, aspirated grain fractions ...... 153 levels specified in the table is to be de- Hog, fat ...... 0 .15 termined by measuring only Hog, meat ...... 0 .03 flubendiamide N2-[1, 1-dimethyl-2- Hog, meat byproducts ...... 0 .15 1 Horse, fat ...... 0 .70 (methylsulfonyl)ethyl]-3-iodo-N -[2- Horse, meat ...... 0 .08 methyl-4- [1,2,2,2-tetrafluoro-1- Horse, meat byproducts ...... 0 .60 (trifluoromethyl)ethyl]phenyl]-1,2- Milk ...... 0.15 Milk, fat ...... 1 .0 benzenedicarboxamide, in or on the fol- Pea and bean, dried shelled, except soybean, lowing commodities: subgroup 6C ...... 0 .60 Pea and bean, succulent shelled, subgroup 6B 0 .05 Commodity Parts per Peanut, hay ...... 60 million Peanut, meal ...... 0 .03 Peanut, nutmeat ...... 0 .02 Almond, hulls ...... 9 .0 Peanut, refined oil ...... 0.03 Apple, wet pomace ...... 5 .0 Pistachio ...... 0.06 Corn, field, forage ...... 8 .0 Poultry, fat ...... 3.0 Corn, field, grain ...... 0 .03 Poultry, liver ...... 0 .60 Corn, field, stover ...... 15 Poultry, meat ...... 0 .10 Corn, pop, grain ...... 0.02 Rice, grain 1 ...... 0 .50 Corn, pop, stover ...... 15 Safflower, seed ...... 5 .0 Corn, sweet, forage ...... 9 .0 Sheep, fat ...... 0 .70

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Parts per [76 FR 16307, Mar. 23, 2011, as amended at 76 Commodity million FR 55273, Sept. 7, 2011; 77 FR 73945, Dec. 12, 2012] Sheep, meat ...... 0.08 Sheep, meat byproducts ...... 0 .60 Sorghum, grain, forage ...... 12 § 180.640 Pyridalyl; tolerances for resi- Sorghum, grain, grain ...... 5 .0 dues. Sorghum, grain, stover ...... 14 (a) General. Tolerances are estab- Soybean, forage ...... 18 lished for residues of pyridalyl, pyri- Soybean, hay ...... 60 Soybean, hulls ...... 0 .80 dine,2-[3-[2,6-dichloro-4-[(3,3-dichloro-2- Soybean, seed ...... 0 .25 propenyl)oxy]phenoxy]propoxy]-5- Sugarcane, cane ...... 0.30 (trifluoromethyl, in or on the following Sunflower, seed ...... 5.0 raw agricultural commodities:) Turnip, greens ...... 25 Vegetable, foliage of legume, except soybean, Parts per subgroup 7A ...... 35 Commodity million Vegetable, legume, edible podded, subgroup 6A ...... 0 .50 Brassica, head and stem, subgroup 5A ...... 3 .5 Mustard greens ...... 30 1 There are no U.S. registrations for rice, grain. Turnip greens ...... 30 (b) Section 18 emergency exemptions. Vegetable, fruiting, group 8 ...... 1.0 Vegetables, leafy, except Brassica, group 4 ...... 20 [Reserved] (c) Tolerances with regional registra- (b) Section 18 emergency exemptions. tions. [Reserved] [Reserved] (d) Indirect or inadvertent residues. (c) Tolerances with regional registra- Tolerances are established for residues tions. [Reserved] of flubendiamide, including its metabo- (d) Indirect or inadvertent residues. lites and degradates, in or on the com- [Reserved] modities in the table below. Compli- ance with the tolerance levels specified [73 FR 25533, May 7, 2008] in the table is to be determined by § 180.641 Spirotetramat; tolerances for measuring only flubendiamide N2-[1, 1- residues. dimethyl-2-(methylsulfonyl)ethyl]-3- (a) General. (1) Tolerances are estab- iodo-N1-[2-methyl-4- [1,2,2,2- lished for residues of the insecticide tetrafluoro-1- spirotetramat, including its metabo- (trifluoromethyl)ethyl]phenyl]-1, 2- lites and degradates, in or on the com- benzenedicarboxamide, in or on the fol- modities in the table below. Compli- lowing commodities: ance with the tolerance levels specified Parts per below is to be determined by measuring Commodity million only the sum of spirotetramat (cis-3- Barley, hay ...... 0 .04 (2,5-dimethlyphenyl)-8-methoxy-2-oxo- Barley, straw ...... 0 .07 1-azaspiro[4.5]dec-3-en-4-yl-ethyl car- Buckwheat ...... 0 .07 bonate) and its metabolites cis-3-(2,5- Clover, forage ...... 0.15 dimethylphenyl)-4-hydroxy-8-methoxy- Clover, hay ...... 0.04 1-azaspiro[4.5]dec-3-en-2-one, cis-3-(2,5- Grass, forage ...... 0 .15 Grass, hay ...... 0 .04 dimethylphenyl)-3-hydroxy-8-methoxy- Millet, pearl, forage ...... 0 .15 1-azaspiro[4.5]decane-2,4-dione, cis-3- Millet, pearl, hay ...... 0.04 (2,5-dimethylphenyl)-8-methoxy-2-oxo- Millet, proso, forage ...... 0 .15 1-azaspiro[4.5]dec-3-en-4-yl beta-D-glu- Millet, proso, hay ...... 0 .04 Millet, proso, straw ...... 0 .07 copyranoside, and cis-3-(2,5- Oats, forage ...... 0 .15 dimethylphenyl)-4-hydroxy-8-methoxy- Oats, hay ...... 0.04 1-azaspiro[4.5]decan-2-one, calculated Oats, straw ...... 0.07 Rye, forage ...... 0 .15 as the stoichiometric equivalent of Rye, straw ...... 0 .07 spirotetramat, in or on the following Teosinte, forage ...... 0 .15 commodities. Teosinte, hay ...... 0 .04 Teosinte, straw ...... 0.07 Commodity Parts per Triticale, forage ...... 0 .15 million Triticale, hay ...... 0 .04 Triticale, straw ...... 0 .07 Acerola ...... 2.5 Wheat, forage ...... 0 .15 Almond, hulls ...... 9 .0 Wheat, hay ...... 0 .03 Artichoke, globe ...... 1.5 Wheat, straw ...... 0 .03 Aspirated grain fractions ...... 10 .0 Avocado ...... 0 .60

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bonate]) and its metabolite cis-3-(2,5- Commodity Parts per million dimethylphenyl)-4-hydroxy-8-methoxy- Berry, low growing, except strawberry, subgroup 1-azaspiro[4.5]dec-3-en-2-one, calculated 13–07H ...... 0 .30 as the stoichiometric equivalent of Black sapote ...... 0 .60 Brassica, head and stem, subgroup 5A ...... 2 .5 spirotetramat, in or on the following Brassica, leafy, subgroup 5B ...... 8 .0 commodities: Bushberry subgroup 13–07B ...... 3 .0 Canistel ...... 0 .60 Parts per Citrus, oil ...... 6.0 Commodity million Coffee, green bean ...... 0 .20 Coffee, instant ...... 0 .50 Cattle, fat ...... 0.02 Corn, sweet, kernel plus cob with husks re- Cattle, meat ...... 0 .02 moved ...... 1 .5 Cattle, meat byproducts ...... 0.20 Cotton gin byproducts1 ...... 10 .0 Cotton, undelinted seed1 ...... 0 .30 Eggs ...... 0 .02 Feijoa ...... 2 .5 Goat, fat ...... 0 .02 Fruit, citrus, group 10–10 ...... 0 .60 Goat, meat ...... 0.02 Fruit, pome, group 11–10 ...... 0 .70 Goat, meat byproducts ...... 0 .20 Fruit, stone, group 12 ...... 4 .5 Hog, meat byproducts ...... 0 .02 Grape, raisin ...... 3 .0 Horse, fat ...... 0 .02 Guava ...... 2 .5 Horse, meat ...... 0 .02 Hop, dried cones ...... 10 .0 Jaboticaba ...... 2 .5 Horse, meat byproducts ...... 0 .20 Longan ...... 13 .0 Milk ...... 0.01 Lychee ...... 13.0 Poultry, meat byproducts ...... 0.02 Mamey sapote ...... 0 .60 Sheep, fat ...... 0 .02 Mango ...... 0.60 Sheep, meat ...... 0.02 Nut, tree, group 14 ...... 0 .25 Sheep, meat byproducts ...... 0 .20 Papaya ...... 0 .40 Passionfruit ...... 2 .5 Persimmon ...... 2 .5 (b) Section 18 emergency exemptions. Pineapple ...... 0.30 [Reserved] Pistachio ...... 0.25 Pomegranate ...... 0 .50 (c) Tolerances with regional registra- Potato, flakes ...... 1 .6 tions. Tolerances with regional reg- Pulasan ...... 13 .0 istrations are established for residues Rambutan ...... 13 .0 Sapodilla ...... 0 .60 of the insecticide spirotetramat, in- Small fruit vine climbing subgroup, except fuzzy cluding its metabolites and degradates, kiwifruit, subgroup 13–07F ...... 1.3 in or on the commodities in the table Soybean forage ...... 8.0 Soybean hay ...... 16.0 below. Compliance with the tolerance Soybean seed ...... 5 .0 levels specified below is to be deter- Spanish lime ...... 13 Star apple ...... 0 .60 mined by measuring only the sum of Starfruit ...... 2 .5 spirotetramat (cis-3-(2,5- Strawberry1 ...... 0 .40 dimethlyphenyl)-8-methoxy-2-oxo-1- Taro, leaves ...... 9 .0 Vegetable, bulb, group 3–07 ...... 0 .80 azaspiro[4.5]dec-3-en-4-yl-ethyl car- Vegetable, cucurbit, group 9 ...... 0.30 bonate) and its metabolites cis-3-(2,5- Vegetable, foliage of legume, except soybean, dimethylphenyl)-4-hydroxy-8-methoxy- subgroup 07A ...... 7 .0 Vegetable, fruiting, group 8–10 ...... 2 .5 1-azaspiro[4.5]dec-3-en-2-one, cis-3-(2,5- Vegetable, leafy, except brassica, group 4 ...... 9 .0 dimethylphenyl)-3-hydroxy-8-methoxy- Vegetable, legume, group 06, except soybean .. 2 .5 1-azaspiro[4.5]decane-2,4-dione, cis-3- Vegetable, tuberous and corm, subgroup 1C ..... 0.60 Watercress ...... 2 .0 (2,5-dimethylphenyl)-8-methoxy-2-oxo- Wax jambu ...... 2 .5 1-azaspiro[4.5]dec-3-en-4-yl beta-D-glu- White sapote ...... 0 .60 copyranoside, and cis-3-(2,5- 1 Import tolerance only. There are no U.S. registrations for dimethylphenyl)-4-hydroxy-8-methoxy- cotton or strawberry. 1-azaspiro[4.5]decan-2-one, calculated (2) Tolerances are also established for as the stoichiometric equivalent of residues of the insecticide spirotetramat, in or on the following spirotetramat, including its metabo- commodities. lites and degradates, in or on the commodities in the table below. Compli- Parts per Commodity ance with the tolerance levels specified million below is to be determined by measuring Banana ...... 4.0 only the sum of spirotetramat (cis-3- (2,5-dimethlyphenyl)-8-methoxy-2-oxo- 1-azaspiro[4.5]dec-3-en-4-yl-ethyl car-

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(d) Indirect or inadvertant residues. § 180.644 Cyprosulfamide; tolerances [Reserved] for residues. [73 FR 39256, July 9, 2008, as amended at 76 (a) General. (1) Tolerances are estab- FR 28681, May 18, 2011; 77 FR 8746, Feb. 15, lished for residues of the herbicide 2012; 77 FR 75859, Dec. 26, 2012; 78 FR 28512, safener cyprosulfamide, N-[[4- May 15, 2013; 78 FR 66651, Nov. 6, 2013] [(cyclopropylamino)carbonyl] phenyl]sulfonyl]-2-methoxybenzamide, § 180.642 Gentamicin; tolerances for in or on the following raw agricultural residues. commodities: (a) General. [Reserved] Commodity Parts per (b) Section 18 emergency exemptions. million Time-limited tolerances specified in Corn, field, forage ...... 0 .20 the following table are established for Corn, field, grain ...... 0 .01 residues of gentamicin in or on the Corn, field, stover ...... 0 .20 specified agricultural commodities, re- Corn, pop, grain ...... 0.01 Corn, pop, stover ...... 0.20 sulting from use of the pesticide pursu- Corn, sweet, forage ...... 0 .40 ant to FIFRA section 18 emergency ex- Corn, sweet, kernel plus cob with husks re- emptions. The tolerances expire and moved ...... 0 .01 are revoked on the date specified in the Corn, sweet, stover ...... 0 .35 following table. (2) Tolerances are established for residues of the herbicide safener Parts per Expiration/ Commodity million revocation cyprosulfamide, N-[[4- date [(cyclopropylamino)carbonyl] Apple ...... 0.10 12/31/10 phenyl]sulfonyl]-2-methoxybenzamide, and its metabolite 4-(aminosulfonyl)-N- (c) Tolerance with regional restrictions. cyclopropylbenzamide, calculated as [Reserved] cyprosulfamide, in or on the following (d) Indirect or inadvertant residues. raw agricultural commodities:

[Reserved] Parts per Commodity million [73 FR 44162, July 30, 2008] Cattle, meat byproducts ...... 0.02 EFFECTIVE DATE NOTE: At 81 FR 34907, June Goat, meat byproducts ...... 0 .02 1, 2016, § 180.642 was removed, effective Nov. Horse, meat byproducts ...... 0 .02 28, 2016. Sheep, meat byproducts ...... 0 .02

§ 180.643 Uniconazole; tolerances for (b) Section 18 emergency exemptions. residues. [Reserved] (a) General. Tolerances are estab- (c) Tolerances with regional registra- lished for residues of the fungicide/ tions. [Reserved] plant growth regulator uniconazole-P, (d) Indirect or inadvertant residues. (E)-(S)-1-(4-chlorophenyl)-4,4-dimethyl- [Reserved] 2-(1H-1,2,4-triazol-1-yl)pent-1-en-3-ol, [73 FR 60974, Oct. 15, 2008] its R-enantiomer and its Z-isomer in or on the following raw agricultural com- § 180.645 Thiencarbazone-methyl; tol- modities: erances for residues. (a) General. (1) Tolerances are estab- Parts per Commodity million lished for residues of thiencarbazone- methyl [methyl 4-[[[(4,5-dihydro-3- Vegetable, fruiting, group 8 ...... 0.01 methoxy-4-methyl-5-oxo-1H-1,2,4- triazol-1-yl)-carbonyl]amino]sulfonyl]- (b) Section 18 emergency exemptions. 5-methyl-3-thiophenecarboxylate], per [Reserved] se, in or on the following food and feed (c) Tolerances with regional registra- commodities: tions. [Reserved] Parts per (d) Indirect or inadvertant residues. Commodity million [Reserved] Corn, field, forage ...... 0 .04 [73 FR 51736, Sept. 5, 2008] Corn, field, grain ...... 0 .01

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termined by measuring only ipconazole Commodity Parts per million (2-[(4-chlorophenyl)methyl]-5-(1- Corn, field, stover ...... 0 .02 methylethyl)-1-(1H-1,2,4-triazol-1- Corn, pop, grain ...... 0.01 ylmethyl)cyclopentanol) in or on the Corn, pop, stover ...... 0.01 commodity. Corn, sweet, forage ...... 0 .05 Corn, sweet, kernel plus cob with husks re- Parts per moved ...... 0 .01 Commodity million Corn, sweet, stover ...... 0 .05 Wheat, forage ...... 0 .10 Cotton, gin byproducts ...... 0 .01 Wheat, grain ...... 0 .01 Cotton, undelinted seed ...... 0 .01 Wheat, hay ...... 0 .01 Grain, cereal, forage, fodder and straw, group Wheat, straw ...... 0 .01 16, except rice ...... 0 .01 Grain, cereal group 15, except rice ...... 0.01 (2) Tolerances are established for Peanut ...... 0 .01 combined residues of thiencarbazone- Soybean, forage ...... 0 .01 methyl and its metabolite BYH 18636- Vegetable, legume, group 6 ...... 0 .01 MMT [5-methoxy-4-methyl-2,4-dihydro- 3H-1,2,4-triazol-3-one], calculated as the (b) Section 18 emergency exemptions. parent compound, in or on the fol- [Reserved] lowing food commodities of animal ori- (c) Tolerances with regional registra- gin: tions. [Reserved] (d) Indirect or inadvertent residues. Parts per [Reserved] Commodity million [73 FR 69559, Nov. 19, 2008, as amended at 79 Cattle, meat ...... 0 .02 FR 15240, Mar. 19, 2014] Cattle, meat byproducts ...... 0.02 Goat, meat ...... 0.02 Goat, meat byproducts ...... 0 .02 § 180.647 d-Phenothrin; tolerances for Horse, meat ...... 0 .02 residues. Horse, meat byproducts ...... 0 .02 Milk ...... 0.02 (a) General. A tolerance of 0.01 parts Sheep, meat ...... 0.02 per million is established for residues Sheep, meat byproducts ...... 0 .02 of the insecticide d-phenothrin in or on all food/feed crops following wide-area (b) Section 18 emergency exemptions. mosquito adulticide applications. [Reserved] (b) Section 18 emergency exemptions. (c) Tolerances with regional registra- [Reserved] tions. [Reserved] (c) Tolerances with regional registra- (d) Indirect or inadvertent residues. tions. [Reserved] Tolerances are established for indirect or inadvertent combined residues of (d) Indirect or inadvertent residues. thiencarbazone-methyl and its metabo- [Reserved] lite BYH 18636-MMT-glucoside [2- [74 FR 32443, July 8, 2009] hexopyranosyl-5-methoxy-4-methyl-2,4- dihydro-3H-1,2,4-triazol-3-one], cal- § 180.648 Meptyldinocap; tolerances culated as the parent compound, in or for residues. on the following food commodities: (a) General. Tolerances are established for the combined residues of the Parts per Commodity million fungicide meptyldinocap, 2-(1- methylheptyl)-4,6-dinitrophenyl (2E)-2- Soybean, forage ...... 0 .04 butenoate and 2,4-DNOP, 2,4-dinitro-6- Soybean, hay ...... 0 .15 (1-methylheptyl)phenol expressed as meptyldinocap in or on the following [73 FR 60968, Oct. 15, 2008] commodities:

§ 180.646 Ipconazole; tolerances for Parts Per Mil- residues. Commodity lion

(a) General. Tolerances are estab- Grape ...... 0.20 lished for residues of ipconazole, including its metabolites and degradates, (b) Section 18 emergency exemptions. in or on the commodities listed in the [Reserved] table below. Compliance with the toler- (c) Tolerances with regional registra- ance levels specified below is to be de- tions. [Reserved]

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(d) Indirect or inadvertent residues. Commodity Parts per [Reserved] million [74 FR 48396, Sept. 23, 2009] Sunflower subgroup 20B ...... 1.0 Vegetable, foliage of legume, group 7 (except § 180.649 Saflufenacil; tolerances for pea, hay) ...... 0.10 residues. Vegetable, legume, edible podded, subgroup 6A 0 .03 Wheat, grain ...... 0 .60 (a) General. (1) Tolerances are estab- Wheat, straw ...... 6 .0 lished for residues of saflufenacil, in- 1 No U.S. registration as of December 7, 2011. cluding its metabolites and degradates, 2 No U.S. registration as of February 21, 2014. in or on the commodities in the table below. Compliance with the tolerance (2) Tolerances are established for res- levels specified below is to be deter- idues of saflufenacil, including its me- mined by measuring only the sum of tabolites and degradates, in or on the saflufenacil, 2-chloro-5-[3,6-dihydro-3- commodities in the table below. Com- methyl-2,6-dioxo-4-(trifluoromethyl)- pliance with the tolerance levels speci- 1(2H)-pyrimidinyl]-4-fluoro-N-[[meth- fied below is to be determined by meas- yl(1-methylethyl)amino] uring only saflufenacil, 2-chloro-5-[3,6- sulfonyl]benzamide, and its metabo- dihydro-3-methyl-2,6-dioxo-4- lites N-[2-chloro-5-(2,6-dioxo-4- (trifluoromethyl)-1(2H)-pyrimidinyl]-4- (trifluoromethyl)-3,6-dihydro-1(2H)- fluoro-N-[[methyl(1- pyrimidinyl)-4-fluorobenzoyl]-N′- methylethyl)amino] isopropylsulfamide and N-[4-chloro-2- sulfonyl]benzamide, in or on the com- fluoro-5-({[(isopropylamino)sulfonyl] modities. amino}carbonyl)phenyl]urea, calculated as the stoichiometric equiva- Parts per Commodity million lent of saflufenacil, in or on the commodities. Cattle, fat ...... 0.04 Cattle, liver ...... 50 Commodity Parts per Cattle, meat ...... 0 .02 million Cattle, meat byproducts, except liver ...... 0 .30 Alfalfa, forage ...... 0.08 Fish-freshwater finfish ...... 0.01 Alfalfa, hay ...... 0.10 Fish-shellfish, crustacean ...... 0 .01 Almond, hulls ...... 0 .10 Goat, fat ...... 0 .04 Banana 1 ...... 0.03 Goat, liver ...... 50 Barley, bran ...... 1 .5 Goat, meat ...... 0.02 Barley, grain ...... 1 .0 Goat, meat byproducts, except liver ...... 0 .30 Barley, straw ...... 15 Hog, fat ...... 0 .01 Coffee, green bean 1 ...... 0 .03 Hog, liver ...... 2 .0 Cotton, gin byproducts ...... 0 .45 Cottonseed subgroup 20C ...... 0 .20 Hog, meat ...... 0 .01 Fruit, citrus, group 10 ...... 0 .03 Hog, meat byproducts, except liver ...... 0 .02 Fruit, pome, group 11 ...... 0.03 Horse, fat ...... 0 .04 Fruit, stone, group 12 ...... 0 .03 Horse, liver ...... 50 Grain, aspirated grain fractions ...... 50 Horse, meat ...... 0 .02 Grain, cereal, forage, fodder and straw group 16 Horse, meat byproducts, except liver ...... 0 .30 (except barley and wheat straw) ...... 0 .10 Milk ...... 0.01 Grain, cereal, group 15 (except barley and Sheep, fat ...... 0 .04 wheat grain) ...... 0 .03 Grape ...... 0 .03 Sheep, liver ...... 50 Grass, forage ...... 15 Sheep, meat ...... 0.02 Grass, hay ...... 20 Sheep, meat byproducts, except liver ...... 0 .30 Grass, seed screenings ...... 0 .15 Grass, straw ...... 0 .15 (b) Section 18 emergency exemptions. Mango 1 ...... 0.03 Nut, tree, group 14 ...... 0 .03 [Reserved] Olive ...... 0 .03 (c) Tolerances with regional registra- Pea and bean, dried shelled, except soybean, tions. [Reserved] subgroup 6C ...... 0 .30 Pea and bean, succulent shelled, subgroup 6B 0 .03 (d) Indirect or inadvertent residues. Pea, hay ...... 17 [Reserved] Pistachio ...... 0.03 Pomegranate ...... 0 .03 [74 FR 46689, Sept. 11, 2009, as amended at 76 Rapeseed subgroup 20A ...... 0 .45 FR 27261, May 11, 2011; 76 FR 76309, Dec. 7, Soybean, hulls ...... 0 .50 2011; 79 FR 9866, Feb. 21, 2014; 79 FR 52219, Soybean, seed ...... 0 .10 Sugarcane, cane 2 ...... 0.05 Sept. 3, 2014; 80 FR 22420, Apr. 22, 2015; 80 FR Sugarcane, molasses 2 ...... 0 .08 73667, Nov. 25, 2015]

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§ 180.650 Isoxaben; tolerances for resi- § 180.652 Ethiprole; tolerances for residues. dues. (a) General. Tolerances are estab- (a) General. Tolerances (without U.S. lished for residues of the herbicide registrations) are established for resi- isoxaben, including its metabolites and dues of the insecticide ethiprole, in- degradates, in or on the commodities cluding its metabolites and degradate, in the table below. Compliance with in or on the following commodities the tolerance levels specified below is listed in the table. Compliance with to be determined by measuring only the tolerance levels specified in the isoxaben, N-[3-(1-ethyl-1- table is to be determined by measuring methylpropyl)-5-isoxazolyl]-2, 6- only ethiprole [5-amino-1-[2,6-dichloro- dimethoxybenzamide, in or on the com- 4-(trifluoromethyl)phenyl]-4-[(ethyl)- modity. sulfinyl]-1H-pyrazole-3-carbonitrile], in or on the following commodities: Parts per Commodity million Parts per Commodity million Almond, hulls ...... 0 .40 Grape ...... 0 .01 Rice, grain 1 ...... 1 .7 Nut, tree, Group 14 ...... 0.02 Tea, dried 1 ...... 30 Pistachio ...... 0.02 1 There are no U.S. registrations for rice and tea. (b) Section 18 emergency exemptions. (b) Section 18 emergency exemptions. [Reserved] [Reserved] (c) Tolerances with regional registra- (c) Tolerances with regional registrations. [Reserved] tions. [Reserved] (d) Indirect or inadvertent residues. (d) Indirect or inadvertent residues. [Reserved] [Reserved] [75 FR 69360, Nov. 12, 2010] [76 FR 18921, Apr. 6, 2011]

§ 180.651 Imazosulfuron; tolerances for § 180.653 Indaziflam; tolerances for residues. residues. (a) General. Tolerances are estab- (a) General. Tolerances are established for residues of the herbicide lished for residues of the herbicide imazosulfuron, including its metabo- indaziflam, N-[(1R,2S)-2,3-dihydro-2,6- lites and degradates, in or on the fol- dimethyl-1H-inden-1-yl]-6-(1- lowing commodities. Compliance with fluoroethyl)-1,3,5-triazine-2,4-diamine, the tolerance levels specified in the fol- including its metabolites and lowing table below is to be determined degradates, in or on the commodities by measuring only imazosulfuron, 2- in the following table. Compliance with chloro-N-[[(4,6-dimethoxy-2- the tolerance levels specified in the pyrimidinyl)amino]carbonyl]imidazo- table below is to be determined by [1,2-a]pyridine-3-sulfonamide, in or on measuring only indaziflam, in or on the the commodity. commodity. Parts per Commodity million Parts per Commodity million Melon subgroup 9A ...... 0 .02 Almond, hulls ...... 0 .15 Pepper, bell ...... 0 .02 Banana 1 ...... 0.01 Pepper, non-bell ...... 0.02 Coffee, green bean 1 ...... 0 .01 Rice, grain ...... 0 .02 Fruit, citrus, group 10–10 ...... 0 .01 Tomato ...... 0.02 Fruit, pome, group 11–10 ...... 0 .01 Vegetable, tuberous and corm, subgroup 1C ..... 0.02 Fruit, stone, group 12 ...... 0 .01 Grape ...... 0 .01 (b) Section 18 emergency exemptions. Nut, tree, group 14 ...... 0 .01 [Reserved] Olive ...... 0 .01 Palm, oil 1 ...... 0 .03 (c) Tolerances with regional registra- Pistachio ...... 0.01 tions. [Reserved] Sugarcane, refined sugar 1 ...... 0 .01 (d) Indirect or inadvertent residues. 1 No U.S. Registrations as of 12/02/2013. [Reserved] 2 Tolerance without a corresponding U.S. registration. [75 FR 81884, Dec. 29, 2010, as amended at 78 (b) Section 18 emergency exemptions. FR 44444, July 24, 2013] [Reserved]

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(c) Tolerances with regional registra- pyrimidinyl)amino]carbonyl]-3- tions. [Reserved] (trifluoromethyl)-2- (d) Indirect or inadvertent residues. pyridinesulfonamide). [Reserved] Commodity Parts per [76 FR 18905, Apr. 6, 2011, as amended at 79 million FR 4630, Jan. 29, 2014] Almond, hulls ...... 0 .01 Fruit, citrus, group 10–10 ...... 0 .01 § 180.654 Isopyrazam; tolerances for Grape ...... 0 .01 residues. Nut, tree, group 14–12 ...... 0 .01 (a) General. Tolerances are estab- Sugarcane ...... 0 .01 lished for residues of the fungicide (b) Section 18 emergency exemptions. isopyrazam, including its metabolites [Reserved] and degradates, in or on the commod- (c) Tolerances with regional registra- ities listed in the following table. Com- tions. [Reserved] pliance with the tolerance levels speci- (d) Indirect or inadvertent residues. fied in the following table is to be de- [Reserved] termined by measuring only isopyrazam (3-(difluoromethyl)-1-meth- [77 FR 10968, Feb. 24, 2012, as amended at 79 yl-N-[1,2,3,4-tetrahydro-9-(1- FR 52989, Sept. 5, 2014] methylethyl)-1,4-methano-naphthalen- 5-yl]-1H-pyrazole-4-carboxamide), as § 180.656 Amisulbrom; tolerances for the sum of its syn-isomer (3- residues. (difluoromethyl)-1-methyl-N-[(1RS, (a) General. Tolerances are estab- 4SR, 9RS)-1,2,3,4-tetrahydro-9-(1- lished for residues of the fungicide methylethyl)-1,4-methanonaphthalen- amisulbrom, including its metabolites 5-yl]-1H-pyrazole-4-carboxamide) and and degradates, in or on the commod- anti-isomer (3-(difluoromethyl)-1-meth- ities listed below. Compliance with the yl-N-[(1RS, 4SR, 9SR)-1,2,3,4- tolerance levels is to be determined by tetrahydro-9-(1-methylethyl)-1,4- measuring only amisulbrom, 3-[(3- methano-naphthalen-5-yl]-1H-pyrazole- bromo-6-fluoro-2-methyl-1H-indole-1- 4-carboxamide) in or on the com- yl) sulfonyl]-N, N-dimethyl-1H-1, 2, 4- modity. triazole-1-sulfonamide].

Parts per Parts per Commodity 1 Commodity million million

Apple1 ...... 0 .70 Grape ...... 0 .40 Banana1 ...... 0 .05 Grape, raisin ...... 1 .0 Peanut1 ...... 0 .01 Tomato ...... 0.50 Tomato, paste ...... 1 .2 1 There are no U.S. registrations for use of isopyrazam on apple, banana, or peanut. 1 There is no U.S. registration for use of amisulbrom on grape or tomato. (b) Section 18 emergency exemptions. [Reserved] (b) Section 18 emergency exemptions. (c) Tolerances with regional registra- [Reserved] tions. [Reserved] (c) Tolerances with regional registra- (d) Indirect or inadvertent residues. tions. [Reserved] [Reserved] (d) Indirect or inadvertent residues. [Reserved] [76 FR 61596, Oct. 5, 2011, as amended at 78 FR 78745, Dec. 27, 2013] [76 FR 59914, Sept. 28, 2011]

§ 180.655 Flazasulfuron; tolerances for § 180.657 Metaflumizone; tolerances residues. for residues. (a) General. Tolerances are estab- (a) General. Tolerances are established for residues of flazasulfuron, in- lished for residues of the insecticide cluding its metabolites and degradates, metaflumizone, including its metabo- in or on the commodities in the table lites and degradates, in or on the com- below. Compliance with the tolerance modities listed in the following table. levels specified below is to be deter- Compliance with the tolerance levels mined by measuring only flazasulfuron specified in the following table is to be (N-[[(4,6-dimethoxy-2- determined by measuring only the sum

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of metaflumizone (E and Z isomers; 2- Commodity Parts per [2-(4-cyanophenyl)-1-[3- million (trifluoromethyl) phenyl]ethylidene]- Corn, field, forage ...... 40 N-[4-(trifluoromethoxy)phenyl] Corn, field, grain ...... 0 .01 hydrazinecarboxamide) and its metabo- Corn, field, refined oil ...... 0 .05 { Corn, field, stover ...... 15 lite 4- 2-oxo-2-[3-(trifluoromethyl) Corn, pop, grain ...... 0.01 phenyl]ethyl}-benzonitrile, calculated Corn, sweet, kernel plus cob with husks re- as the stoichiometric equivalent of moved ...... 0 .01 Cotton, seed ...... 1.5 metaflumizone, in or on the following Cotton, gin byproducts ...... 15 commodities: Fruit, pome, group 11–10 ...... 0 .50 Fruit, stone, group 12 ...... 4 .0 Commodity Parts per Grain, aspirated fractions ...... 30 million Millet, spp...... 0 .80 Nut, tree, group 14 ...... 0 .06 Almond, hulls ...... 0 .04 Oat, forage ...... 40 Eggplant 1 ...... 1.5 Oat, grain ...... 0 .15 Fruit, citrus, group 10–10 ...... 0 .04 Oat, hay ...... 80 Fruit, pome, group 11–10 ...... 0 .04 Oat, straw ...... 1.0 Fruit, stone, group 12–12 ...... 0 .04 Pea and bean, dried shelled, except soybean, Grape ...... 0 .04 subgroup 6C ...... 0 .40 Nut, tree, group 14–12 ...... 0 .04 Peanut ...... 0 .04 Pepper 1 ...... 1 .5 Peanut, hay ...... 30 Tomato 1 ...... 0.60 Peanut, refined oil ...... 0.06 Tomato, paste 1 ...... 1 .2 Pistachio ...... 0.06 1 There are no U.S. registrations as of April 4, 2014. Potato, processed potato waste ...... 0 .20 Rye, forage ...... 40 (b) Section 18 emergency exemptions. Rye, grain ...... 0.15 [Reserved] Rye, straw ...... 1 .0 Sorghum, forage ...... 40 (c) Tolerances with regional registra- Sorghum, grain, grain ...... 0 .80 tions. [Reserved] Sorghum, stover ...... 15 (d) Indirect or inadvertent residues. Soybean, seed ...... 0 .40 Sunflower, seed ...... 1.5 [Reserved] Teosinte, grain ...... 0 .15 [77 FR 10386, Feb. 22, 2012, as amended at 79 Tomato, paste ...... 3 .5 Triticale, forage ...... 40 FR 18810, Apr. 4, 2014; 80 FR 66800, Oct. 30, Triticale, grain ...... 0 .15 2015] Triticale, hay ...... 80 Triticale, straw ...... 1 .0 § 180.658 Penthiopyrad; tolerances for Vegetable, bulb, group 3–07 ...... 3 .0 residues. Vegetable, cucurbit, group 9 ...... 0.60 Vegetable, foliage of legume, group 7, hay ...... 200 (a) General. (1) Tolerances are estab- Vegetable, foliage of legume, group 7, vines/for- lished for residues of penthiopyrad, in- age ...... 50 Vegetable, fruiting, group 8–10 ...... 3 .0 cluding its metabolites and degradates, Vegetable, leafy, except brassica, group 4 ...... 30 in or on the commodities in the table Vegetable, leaves of root and tuber, group 2 ..... 50 below. Compliance with the tolerance Vegetable, legume, edible podded, subgroup 6A 4 .0 levels specified below is to be deter- Vegetable, legume, succulent shelled, subgroup 6B ...... 0 .40 mined by measuring only penthiopyrad Vegetable, root, subgroup 1B, except sugar (N-[2-(1,3-dimethylbutyl)-3-thienyl]-1- beet ...... 3 .0 methyl-3-(trifluoromethyl)-1H-pyr- Vegetable, tuber and corm, subgroup 1C ...... 0 .06 Wheat, forage ...... 40 azole-4-carboxamide). Wheat, grain ...... 0 .15 Wheat, hay ...... 80 Parts per Wheat, milled byproducts ...... 0 .30 Commodity million Wheat, straw ...... 1 .0 Alfalfa, forage ...... 7.0 Alfalfa, hay ...... 20 (2) Tolerances are established for res- Almond, hulls ...... 6 .0 idues of penthiopyrad, including its Apple, wet pomace ...... 1 .5 Barley, grain ...... 0 .15 metabolites and degradates, in or on Barley, hay ...... 80 the commodities in the table below. Barley, milled byproducts ...... 0.90 Compliance with the tolerance levels Barley, straw ...... 1 .0 Beet, sugar, dried pulp ...... 1 .5 specified below is to be determined by Beet, sugar, roots ...... 0 .5 measuring only the sum of Berry, low growing, subgroup 13–07G ...... 3 .0 penthiopyrad (N-[2-(1,3-dimethylbutyl)- Brassica, head and stem, subgroup 5A ...... 5 .0 3-thienyl]-1-methyl-3- Brassica, leafy greens, subgroup 5B ...... 50 Buckwheat, grain ...... 0.15 (trifluoromethyl)-1H-pyrazole-4- Canola ...... 1 .5 carboxamide) and its metabolite (1-

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methyl-3-trifluoromethyl-1H-pyrazole- the tolerance levels specified below is 4-carboxamide), calculated as the stoi- to be determined by measuring only chiometric equivalent of penthiopyrad, the sum of pyroxasulfone, 3-[[[5- in or on the commodity. (difluoromethoxy)-1-methyl-3- (trifluoromethyl)-1H-pyrazol-4- Parts per Commodity million yl]methyl]sulfonyl]-4,5-dihydro-5,5- dimethylisoxazole, and its metabolites, Cattle, fat ...... 0.03 5-(difluoromethoxy)-1-methyl-3- Cattle, meat ...... 0 .03 Cattle, meat byproducts ...... 0.09 (trifluoromethyl)-1H-pyrazol-4- Goat, fat ...... 0 .03 yl]methanesulfonic acid (M–1); 5- Goat, meat ...... 0.03 (difluoromethoxy)-1-methyl-3- Goat, meat byproducts ...... 0 .09 (trifluoromethyl)-1H-pyrazol-4-car- Horse, fat ...... 0 .03 Horse, meat ...... 0 .03 boxylic acid (M-3); and [5- Horse, meat byproducts ...... 0 .09 (difluoromethoxy)-3-(trifluoromethyl)- Milk ...... 0.02 1H-pyrazol-4-yl]methanesulfonic acid Sheep, fat ...... 0 .03 Sheep, meat ...... 0.03 (M-25), calculated as the stoichiometric Sheep, meat byproducts ...... 0 .09 equivalent of pyroxasulfone, in or on the commodity. (b) Section 18 emergency exemptions. [Reserved] Parts per Commodity million (c) Tolerances with regional registrations. [Reserved] Corn, field, forage ...... 0 .09 (d) Indirect or inadvertent residues. Corn, field, stover ...... 0 .15 [Reserved] Corn, pop, stover ...... 0.15 Corn, sweet, forage ...... 0 .10 [77 FR 14297, Mar. 9, 2012] Corn, sweet, stover ...... 0 .15 Cotton, gin byproducts ...... 0 .20 § 180.659 Pyroxasulfone; tolerances for Soybean, forage ...... 1 .0 residues. Soybean, hay ...... 2 .0 Wheat, forage ...... 6 .0 (a) General. (1) Tolerances are estab- Wheat, hay ...... 1 .0 lished for residues of the herbicide Wheat, straw ...... 0 .60 pyroxasulfone, including its metabolites and degradates, in or on the com- (3) Tolerances are established for res- modities in the table below. Compli- idues of the herbicide pyroxasulfone, ance with the tolerance levels specified including its metabolites and below is to be determined by measuring degradates, in or on the commodities only the sum of pyroxasulfone, 3-[[[5- in the table below. Compliance with (difluoromethoxy)-1-methyl-3- the tolerance levels specified below is (trifluoromethyl)-1H-pyrazol-4- to be determined by measuring only yl]methyl]sulfonyl]-4,5-dihydro-5,5- the sum of pyroxasulfone, 3-[[[5- dimethylisoxazole, and its metabolite, (difluoromethoxy)-1-methyl-3- 5-(difluoromethoxy)-1-methyl-3- (trifluoromethyl)-1H-pyrazol-4- (trifluoromethyl)-1H-pyrazol-4-car- yl]methyl]sulfonyl]-4,5-dihydro-5,5- boxylic acid (M-3), calculated as the dimethylisoxazole, and its metabolites, stoichiometric equivalent of 5-(difluoromethoxy)-1-methyl-3- pyroxasulfone, in or on the commodity. (trifluoromethyl)-1H-pyrazol-4-carboxylic acid (M–3); [5- Parts per Commodity million (difluoromethoxy)-3-(trifluoromethyl)- 1H-pyrazol-4-yl]methanesulfonic acid Corn, field, grain ...... 0 .02 (M–25); and 3-[1-carboxy-2-(5,5-di- Corn, pop, grain ...... 0.015 Corn, sweet, kernel plus cob with husks re- methyl-4,5-dihydroisoxazol-3- moved ...... 0 .015 ylthio)ethylamino]-3-oxopropanoic acid Cotton, undelinted seed ...... 0 .04 (M–28), calculated as the stoichio- Wheat, grain ...... 0 .03 metric equivalent of pyroxasulfone, in (2) Tolerances are established for res- or on the commodity. idues of the herbicide pyroxasulfone, Parts per including its metabolites and Commodity million degradates, in or on the commodities in the table below. Compliance with Soybean, seed ...... 0 .06

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(4) Tolerances are established for res- (c) Tolerances with regional registra- idues of the herbicide pyroxasulfone, tions. [Reserved] including its metabolites and (d) Indirect or inadvertent residues. degradates, in or on the commodities [Reserved] in the following table. Compliance with [77 FR 13506, Mar. 7, 2012] the tolerance levels specified in the following table is to be determined by § 180.661 Fluopyram; tolerances for measuring only the sum of residues. pyroxasulfone [3-[[[5- (a) General. (1) Tolerances are estab- (difluoromethoxy)-1-methyl-3- lished for residues of the fungicide (trifluoromethyl)-1H-pyrazol-4- Fluopyram, N-[2-[3-chloro-5- yl]methyl]sulfonyl]-4,5-dihydro-5,5- (trifluoromethyl)-2-pyridinyl]ethyl]-2- dimethylisoxazole] and its metabolites (trifluoromethyl)benzamide, including [5-(difluoromethoxy)-1-methyl-3- its metabolites and degradates in or on (trifluoromethyl)-1H-pyrazol-4- the commodities in the table below. yl]methanesulfonic acid (M–1) and 5- Compliance with the tolerance levels (difluoromethoxy)-1-methyl-3- specified in the table is to be deter- (trifluoromethyl)-1H-pyrazol-4-car- mined by measuring only fluopyram in boxylic acid (M–3), calculated as the or on the commodity. stoichiometric equivalent of pyroxasulfone, in or on the commodity. Parts per Commodity million Parts per Commodity million Almond, hulls ...... 10 Artichoke, globe ...... 4.0 Milk ...... 0.003 Banana 1 ...... 1.0 Bean, dry ...... 0.70 Beet, sugar ...... 0 .10 (b) Section 18 emergency exemptions. Berry, low growing, except cranberry, subgroup [Reserved] 13–07G ...... 2.0 (c) Tolerances with regional registra- Brassica, head and stem, subgroup 5A ...... 4 .0 Brassica, leafy greens, subgroup 5B ...... 50 tions. [Reserved] Bushberry subgroup 13–07B ...... 7 .0 (d) Indirect or inadvertent residues. Caneberry subgroup 13–07A ...... 5.0 [Reserved] Cherry subgroup 12–12A ...... 2 .0 Citrus, oil ...... 8.0 [77 FR 12213, Feb. 29, 2012, as amended at 78 Corn, field, grain ...... 0 .02 Corn, pop, grain ...... 0.02 FR 13257, Feb. 27, 2013; 78 FR 46279, July 31, Corn, sweet, kernel plus cob with husks re- 2013; 79 FR 34633, June 18, 2014] moved ...... 0 .01 Cotton, gin byproducts ...... 30 § 180.660 Pyriofenone; tolerances for Cottonseed subgroup 20C ...... 0 .80 residues. Dill, seed ...... 70 Fruit, citrus, group 10–10 ...... 1 .0 (a) General. Tolerances are estab- Fruit, pome, group 11–10 ...... 0 .80 lished for residues of the fungicide Fruit, small vine climbing, except fuzzy kiwifruit, subgroup 13–07F ...... 2.0 pyriofenone, including its metabolites Grain, aspirated grain fractions ...... 50 and degradates, in or on the following Grain, cereal, forage, fodder and straw, group commodities listed in the table. Com- 16 ...... 20 pliance with the tolerance levels speci- Grain, cereal, group 15, except corn and rice .. 4.0 Grape, raisin ...... 3 .0 fied in the table is to be determined by Herb subgroup 19A ...... 40 measuring only pyriofenone, (5-chloro- Hop, dried cones ...... 60 2-methoxy-4-methyl-3-pyridinyl)(2,3,4- Leafy greens subgroup 4A ...... 40 Leafy petioles subgroup 4B ...... 20 trimethoxy-6-methylphenyl) Melon subgroup 9A ...... 1 .0 methanone, in or on the following com- Nut, tree, group 14–12 ...... 0 .05 modities: Onion, bulb, subgroup 3–07A ...... 0 .40 Onion, green, subgroup 3–07B ...... 15 Parts per Pea and bean, succulent shelled, subgroup 6B 0 .20 Commodity million Peach subgroup 12–12B ...... 1.0 Peanut ...... 0 .20 Grape 1 ...... 0 .30 Pepper/eggplant subgroup 8–10B ...... 4 .0 Grape, raisin 1 ...... 0 .50 Plum subgroup 12–12C ...... 0 .50 Potato, wet peel ...... 0 .30 1 There are no U.S. registrations for grape and grape, Rapeseed subgroup 20A ...... 5 .0 raisin. Soybean, seed ...... 0 .30 Squash/cucumber subgroup 9B ...... 0.60 (b) Section 18 emergency exemptions. Sunflower subgroup 20B ...... 0.70 [Reserved] Tomato subgroup 8–10A ...... 1 .0

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Parts per Parts per Commodity million Commodity million

Vegetable, leaves of root and tuber, group 2 ... 30 Sugarcane, cane ...... 0.08 Vegetable, legume, edible podded, subgroup 6A ...... 4 .0 (d) Indirect or inadvertent residues. It Vegetable, root, except sugar beet, subgroup is recommended that tolerances be es- 1B ...... 0 .30 Vegetable, tuberous and corm, subgroup 1C ... 0.10 tablished for indirect or inadvertent residues of fungicide fluopyram, N-[2- 1 There are no U.S. registrations. [3-chloro-5-(trifluoromethyl)-2- (2) Tolerances are established for res- pyridinyl]ethyl]-2- idues of the fungicide fluopyram, N-[2- (trifluoromethyl)benzamide, including [3-chloro-5-(trifluoromethyl)-2- its metabolites and degradates, in or pyridinyl]ethyl]-2- on the commodities in the table below. (trifluoromethyl)benzamide, including Compliance with the tolerance levels its metabolites and degradates. Com- specified in the table is to be deter- pliance with the tolerance levels speci- mined by measuring only fluopyram in fied in the table below is to be deter- or on the commodity. mined by measuring only the sum of Parts per fluopyram and its metabolite, 2- Commodity million (trifluoromethyl)benzamide, calculated as the stoichiometric equivalent of Alfalfa, forage ...... 0.45 Alfalfa, hay ...... 1.1 fluopyram, in or on the commodity. Soybean, seed ...... 0 .10

Commodity Parts per million [81 FR 12023, Mar. 8, 2016]

Cattle, fat ...... 0.70 § 180.662 Trinexapac-ethyl; tolerances Cattle, meat ...... 0 .80 for residues. Cattle, meat byproducts ...... 7.5 Egg ...... 0 .08 (a) General. Tolerances are estab- Goat, fat ...... 0 .70 lished for residues of the plant growth Goat, meat ...... 0.80 inhibitor, trinexapac-ethyl, including Goat, meat byproducts ...... 7 .5 Hog, fat ...... 0 .20 its metabolites and degradates, in or Hog, meat ...... 0 .02 on the commodities in the table below. Hog, meat byproducts ...... 0 .20 Compliance with the tolerance levels Horse, fat ...... 0 .70 specified below is to be determined by Horse, meat ...... 0 .80 measuring both trinexapac-ethyl, ethyl Horse, meat byproducts ...... 7 .5 4-(cyclopropylhydroxymethylene)-3,5- Milk ...... 0.40 Poultry, fat ...... 0.04 dioxocyclohexanecarboxylate and the Poultry, meat ...... 0 .04 associated metabolite, trinexpac, 4- Poultry, meat byproducts ...... 0.20 (cyclopropylhydroxymethylene)-3,5- Sheep, fat ...... 0 .70 dioxocyclohexanecarboxylic acid, cal- Sheep, meat ...... 0.80 culated as the stoichiometric equiva- Sheep, meat byproducts ...... 7 .5 lent of trinexapac-ethyl, in or on the (b) Section 18 emergency exemptions. commodity. [Reserved] Parts per (c) Tolerances with regional registra- Commodity million tions. Tolerances with regional reg- Barley, bran ...... 2 .5 istration, as defined in § 180.1(1), are es- Barley, grain ...... 2 .0 tablished for indirect or inadvertent Barley, hay ...... 0 .8 residues of fungicide fluopyram, N-[2- Barley, straw ...... 0 .4 Cattle, fat ...... 0.02 [3-chloro-5-(trifluoromethyl)-2- Cattle, meat ...... 0 .02 pyridinyl]ethyl]-2- Cattle, meat byproducts ...... 0.04 (trifluoromethyl)benzamide, including Goat, fat ...... 0 .02 Goat, meat ...... 0.02 its metabolites and degradates, in or Goat, meat byproducts ...... 0 .04 on the commodities in the table below. Grass, forage ...... 1 .5 Compliance with the tolerance levels Grass, hay ...... 4 .0 specified in the table is to be deter- Grass, seed screenings ...... 40.0 Grass, straw ...... 10 .0 mined by measuring only fluopyram in Hog, fat ...... 0 .02 or on the commodity. Hog, meat ...... 0 .02

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Parts per Parts per Commodity million Commodity million

Hog, meat by-products ...... 0 .03 Vegetable, tuberous and corm, subgroup 1C ..... 0.05 Horse, fat ...... 0 .02 Horse, meat ...... 0 .02 Horse, meat byproducts ...... 0 .04 (b) Section 18 emergency exemptions. Oat, forage ...... 1 .0 [Reserved] Oat, grain ...... 4 .0 (c) Tolerances with regional registra- Oat, hay ...... 1.5 Oat, straw ...... 0.9 tions. [Reserved] Rice, bran ...... 1.5 (d) Indirect or inadvertent residues. Rice, grain ...... 0 .4 [Reserved] Rice, straw ...... 0 .07 Rice, wild, grain ...... 0.4 [77 FR 21734, May 9, 2012] Rye, bran ...... 6 .0 Rye, grain ...... 4.0 Rye, hay ...... 1 .5 § 180.664 Penflufen; tolerances for resi- Rye, straw ...... 0 .9 dues. Sheep, fat ...... 0 .02 (a) General. Tolerances are estab- Sheep, meat ...... 0.02 Sheep, meat byproducts ...... 0 .04 lished for residues of the fungicide Sugarcane, cane ...... 0.8 penflufen, including its metabolites Sugarcane, molasses ...... 2 .5 and degradates, in or on the following Wheat, bran ...... 6.0 Wheat, forage ...... 1 .0 commodities listed in the table. Com- Wheat, grain ...... 4 .0 pliance with the tolerance levels speci- Wheat, hay ...... 1 .5 fied in the table is to be determined by Wheat, middlings ...... 10 .5 Wheat, straw ...... 0 .9 measuring only penflufen N-[2-(1,3- dimethylbutyl)phenyl]-5-fluoro-1,3-di- (b) Section 18 emergency exemptions. methyl-1H-pyrazole-4-carboxamide, in [Reserved] or on the following commodities. (c) Tolerances with regional registra- Parts per tions. [Reserved] Commodity million (d) Indirect or inadvertent residues. [Reserved] Alfalfa, forage ...... 0.01 Alfalfa, hay ...... 0.01 [77 FR 12745, Mar. 2, 2012, as amended at 77 Cotton, gin by-products ...... 0 .01 FR 60919, Oct. 3, 2012; 80 FR 28848, May 20, Grain cereal, forage, fodder and straw, group 2015] 16 ...... 0 .01 Grain, cereal, group 15 ...... 0.01 Oilseed, group 20 ...... 0 .01 § 180.663 Ametoctradin; tolerances for Vegetable, foliage of legume, group 7 ...... 0 .01 residues. Vegetable, legume, group 6 ...... 0 .01 (a) General. Tolerances are estab- Vegetable, tuberous and corm subgroup 1C .... 0 .01 lished for residues of the fungicide ametoctradin, including its metabo- (b) Section 18 emergency exemptions. lites and degradates, in or on the com- [Reserved] modities in the following table. Com- (c) Tolerances with regional registra- pliance with the tolerance levels speci- tions. [Reserved] fied in the following table is to be de- (d) Indirect or inadvertent residues. termined by measuring only [Reserved] ametoctradin (5-ethyl-6- [77 FR 28281, May 14, 2012] octyl[1,2,4]triazolo[1,5-a]pyrimidin-7- amine). § 180.665 Sedaxane; tolerances for residues. Parts per Commodity million (a) General. Tolerances are established for residues of the fungicide Brassica, head and stem, subgroup 5A ...... 9 .0 Brassica, leafy greens, subgroup 5B ...... 50 sedaxane, including its metabolites and Grape ...... 4 .0 degradates, in or on the commodities Grape, raisin ...... 8 .0 in the following table. Compliance with Hop, dried cones ...... 10 .0 the tolerance levels specified in the fol- Onion, bulb, subgroup 3–07A ...... 1 .5 Onion, green, subgroup 3–07B ...... 20 .0 lowing table is to be determined by Spinach ...... 50 .0 measuring only sedaxane, N-[2-[1,1′- Vegetable, cucurbit, group 9 ...... 3.0 bicyclopropyl]-2-ylphenyl]-3- Vegetable, fruiting, group 8–10 ...... 1 .5 Vegetable, leafy, except Brassica, group 4, ex- (difluoromethyl)-1-methyl-1H-pyrazole- cept spinach ...... 40 .0 4-carboxamide, as the sum of its cis-

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and trans-isomers in or on the com- biphenyl]-2-yl)-1H-pyrazole-4- modity. carboxamide in or on the commodity.

Parts per Commodity Parts per Commodity million million

Barley, grain ...... 0 .01 Almond, hulls ...... 4 .0 Barley, hay ...... 0 .04 Apple, wet pomace ...... 2 .0 Barley, straw ...... 0 .01 Beet, sugar ...... 0 .1 Beet, sugar, roots ...... 0 .01 Beet, sugar, dried pulp ...... 0 .1 Canola, seed ...... 0 .01 Beet, sugar, tops ...... 7.0 Corn, field, forage ...... 0 .01 Berry, low growing, subgroup 13–07G ...... 4 .0 Corn, field, grain ...... 0 .01 Bushberry, subgroup 13–07B ...... 7.0 Corn, field, stover ...... 0 .01 Caneberry, subgroup 13–07A ...... 5 .0 Corn, pop, grain ...... 0.01 Cattle, fat ...... 0.06 Cattle, meat ...... 0 .01 Corn, pop, stover ...... 0.01 Cattle, meat byproduct ...... 0.04 Corn, sweet, forage ...... 0 .01 Citrus, dried pulp ...... 3 .0 Corn, sweet, kernel plus cob with husks re- Citrus, oil ...... 40 moved ...... 0 .01 Corn, field, grain ...... 0 .01 Corn, sweet, stover ...... 0 .01 Corn, oil ...... 0 .03 Cotton, undelinted seed ...... 0 .01 Corn, pop, grain ...... 0.01 Cotton, gin byproducts ...... 0 .01 Corn, sweet, kernels plus cobs with husks re- Oat, forage ...... 0 .015 moved ...... 0 .15 Oat, grain ...... 0 .01 Cotton, gin byproducts ...... 20 Oat, hay ...... 0.06 Cotton, undelinted seed ...... 0 .30 Oat, straw ...... 0.01 Egg ...... 0 .01 Pea and bean, dried shelled, except soybean, Fish-freshwater finfish ...... 0.01 subgroup 6C ...... 0 .01 Fish-shellfish, crustacean ...... 0 .01 Potato ...... 0 .02 Fruit, citrus, group 10–10 ...... 1 .0 Potato, wet peel ...... 0 .075 Fruit, pome, group 11 ...... 0.8 Rapeseed, subgroup 20A ...... 0.01 Fruit, small, vine climbing, except fuzzy Rye, forage ...... 0 .015 kiwifruit, subgroup 13–07F ...... 2 .0 Rye, grain ...... 0.01 Fruit, stone, group 12–12 ...... 3 .0 Rye, straw ...... 0 .01 Goat, fat ...... 0 .06 Sorghum, grain, forage ...... 0.01 Goat, meat ...... 0.01 Sorghum, grain, grain ...... 0 .01 Goat, meat byproduct ...... 0 .04 Sorghum, grain, stover ...... 0 .01 Grain, aspirated fractions ...... 20.0 Soybean, forage ...... 0 .05 Grain, cereal, forage, fodder and straw, group Soybean, hay ...... 0 .04 16 ...... 20 Soybean, seed ...... 0 .01 Grain, cereal, group 15, (except corn, field, Vegetable, foliage of legume, except soybean, grain; except corn, pop, grain; except corn, subgroup 7A ...... 0 .01 kernels plus cobs with husks removed; ex- Wheat, forage ...... 0 .015 cept rice; except wheat ...... 3 .0 Wheat, grain ...... 0 .01 Grape, raisin ...... 5 .7 Wheat, hay ...... 0 .06 Grass, forage, fodder and hay, group 17 ...... 40 Wheat, straw ...... 0 .01 Hog, meat byproducts ...... 0 .01 Horse, fat ...... 0 .06 Horse, meat ...... 0 .01 (b) Section 18 emergency exemptions. Horse, meat byproduct ...... 0 .04 [Reserved] Milk ...... 0.01 (c) Tolerances with regional registra- Milk, fat ...... 0 .15 Non-grass animal feed, group 18 ...... 30 tions. [Reserved] Nut, tree, group 14–12 ...... 0 .06 (d) Indirect inadvertent residues. [Re- Oilseeds, group 20 (except cottonseed) ...... 0 .9 served] Pea and bean, dried shelled except soybean, subgroup 6C ...... 0 .4 [77 FR 36924, June 20, 2012, as amended at 78 Pea and bean, succulent shelled, subgroup 6B 0 .5 FR 33748, June 5, 2013; 78 FR 60719, Oct. 2, Peanut ...... 0 .01 2013; 80 FR 43329, July 22, 2015] Peanut, refined oil ...... 0.02 Plum, prune, dried ...... 3.0 Potato, wet peel ...... 0 .1 § 180.666 Fluxapyroxad; tolerances for Poultry, fat ...... 0.01 residues. Poultry, meat ...... 0 .01 Poultry, meat byproduct ...... 0.01 (a) General. Tolerances are estab- Rice, bran ...... 4.5 lished for residues of the fungicide Rice, bran ...... 8.5 fluxapyroxad, including its metabolites Rice, grain ...... 5 .0 and degradates, in or on the commod- Rice, hulls ...... 8 .0 Rice, hulls ...... 15 .0 ities listed in the table below. Compli- Sheep, fat ...... 0 .06 ance with the tolerance levels specified Sheep, meat ...... 0.01 below is to be determined by measuring Sheep, meat byproduct ...... 0 .04 Soybean, hulls ...... 0 .3 only fluxapyroxad, 3-(difluoromethyl)- Soybean, seed ...... 0 .15 1-methyl-N-(3′,4′,5′-trifluoro[1,1′- Sugarcane, cane ...... 3.0

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Parts per Parts per Commodity million Commodity million

Vegetable, brassica leafy, group 5 ...... 4 .0 Fruit, pome, group 11 ...... 0.06 Vegetable, bulb, group 3–07 ...... 1 .5 Fruit, small vine climbing, except fuzzy kiwifruit, Vegetable, cucurbit, group 9 ...... 0.50 subgroup 13–07F ...... 0.15 Vegetable, foliage of legume, group 7 ...... 30 Grape, raisin ...... 0.30 Vegetables, fruiting, group 8 ...... 0.7 Vegetable, cucurbit, group 9 ...... 0.07 Vegetable, leafy, except brassica, group 4 ...... 30 Vegetable, legume, edible podded, subgroup (b) Section 18 emergency exemptions. 6A ...... 2 .0 Vegetable, root, except sugarbeet, subgroup [Reserved] 1B ...... 0.90 (c) Tolerances with regional registra- Vegetable, tuberous and corm, subgroup 1C ... 0.02 tions. [Reserved] Wheat, bran ...... 0.6 Wheat, grain ...... 0 .3 (d) Indirect or inadvertent residues. [Reserved] (b) Section 18 emergency exemptions. [77 FR 38210, June 27, 2012] [Reserved] (c) Tolerances with regional registra- § 180.668 Sulfoxaflor; tolerances for tions. [Reserved] residues. (d) Indirect or inadvertent residues. (a) General. Tolerances are estab- Tolerances are established for the com- lished for residues of the insecticide bined indirect or inadvertent residues sulfoxaflor, including its metabolites of the fungicide fluxapyroxad, includ- and degradates, in or on the commod- ing its metabolites and degradates, in ities in the table. Compliance with the or on the commodities listed in the tolerance levels specified is to be deter- table below. Compliance with the toler- mined by measuring only sulfoxaflor ance levels specified below is to be de- (N-[methyloxido[1-[6-(trifluoromethyl)- termined by measuring only 3-pyridinyl]ethyl]-g4- fluxapyroxad, 3-(difluoromethyl)-1- sulfanylidene]cyanamide). methyl-N-(3′,4′,5′-trifluoro[1,1′- biphenyl]-2-yl)-1H-pyrazole-4- Commodity Parts per mil- carboxamide in or on the commodity. lion Almond, hulls ...... 6 .0 Commodity Parts per Barley, grain ...... 0 .40 million Barley, hay ...... 1 .0 Barley, straw ...... 2 .0 Peppermint, tops ...... 0 .01 Bean, dry seed ...... 0 .20 Spearmint, tops ...... 0 .01 Bean, succulent ...... 4 .0 Beet, sugar, dried pulp ...... 0 .07 [77 FR 28275, May 14, 2012, as amended at 77 Beet, sugar, molasses ...... 0 .25 Berry, low growing, subgroup 13–7G ...... 0 .70 FR 46307, Aug. 3, 2012; 79 FR 10677, Feb. 26, Cattle, fat ...... 0.10 2014; 80 FR 45078, July 29, 2015; 81 FR 27025, Cattle, meat ...... 0 .15 May 5, 2016] Cattle, meat byproducts ...... 0.40 Cauliflower ...... 0 .08 § 180.667 Cyflufenamid, tolerance for Citrus, dried pulp ...... 3 .6 residues. Cotton, gin byproducts ...... 6 .0 Cotton, hulls ...... 0 .35 (a) General. Tolerances are estab- Cottonseed subgroup 20C ...... 0 .20 lished for residues of the fungicide Fruit, citrus, group 10–10 ...... 0 .70 Fruit, pome, group 11–10 ...... 0 .50 cyflufenamid, including its metabolites Fruit, small, vine climbing, subgroup 13– and degradates, in or on the commod- 07F, except fuzzy kiwi fruit ...... 2 .0 ities in the table below. Compliance Fruit, stone, group 12 ...... 3 .0 Goat, fat ...... 0 .10 with the tolerance levels specified Goat, meat ...... 0.15 below is to be determined by measuring Goat, meat byproducts ...... 0 .40 only cyflufenamid, [N(Z)]-N- Grain, aspirated fractions ...... 20.0 Grape, raisin ...... 6 .0 [[(cyclopropylmethoxy)amino][2,3- Hog, fat ...... 0 .01 difluoro-6-(trifluoromethyl)phenyl] Hog, meat ...... 0 .01 methylene]benzeneacetamide. Hog, meat byproducts ...... 0 .01 Horse, fat ...... 0 .10 Parts per Horse, meat ...... 0 .15 Commodity million Horse, meat byproducts ...... 0 .40 Leafy greens, subgroup 4A ...... 6.0 Apple, wet pomace ...... 0.10 Leafy petiole, subgroup 4B ...... 2 .0 Berry, low growing, subgroup 13–07G, except Milk ...... 0.15 cranberry ...... 0.20 Nuts, tree, group 14 ...... 0 .015

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Commodity Parts per mil- § 180.669 Picoxystrobin; tolerances for lion residues. Onion, bulb, subgroup 3–07A ...... 0 .01 (a) General. Tolerances are estab- Onion, green, subgroup 3–07B ...... 0 .70 lished for residues of the fungicide Pistachio ...... 0.015 picoxystrobin, including its metabo- Poultry, eggs ...... 0 .01 Poultry, fat ...... 0.01 lites and degradates, in or on the com- Poultry, meat ...... 0 .01 modities listed below. Compliance with Poultry, meat byproducts ...... 0.01 the tolerance levels specified below is Rapeseed, meal ...... 0 .50 to be determined by measuring only Rapeseed subgroup 20A ...... 0 .40 picoxystrobin, methyl (aE)-a- Sheep, fat ...... 0 .10 (methoxymethylene)-2-[[[6- Sheep, meat ...... 0.15 (trifluoromethyl)-2- Sheep, meat byproducts ...... 0 .40 Soybean, seed ...... 0 .20 pyridinyl]oxy]methyl]benzeneacetate. Tomato, paste ...... 2 .60 Parts per Tomato, puree ...... 1 .20 Commodity million Vegetable, brassica, leafy, group 5, except cauliflower ...... 2 .0 Barley, bran ...... 0 .5 Vegetable, cucurbit, group 9 ...... 0.40 Barley, grain ...... 0 .3 Vegetable, fruiting, group 8–10 ...... 0 .70 Cattle, fat ...... 0.01 Vegetable, leaves of root and tuber, group 2 3 .0 Cattle, meat ...... 0 .01 Vegetable, legume, foliage, group 7 ...... 3.0 Cattle, meat byproducts ...... 0.01 Vegetable, root and tuber, group 1 ...... 0 .05 Corn, field, refined oil ...... 0 .07 Watercress ...... 6 .0 Eggs ...... 0 .01 Goat, fat ...... 0 .01 Wheat, forage ...... 1 .0 Goat, meat ...... 0.01 Wheat, grain ...... 0 .08 Goat, meat byproducts ...... 0 .01 Wheat, hay ...... 1 .5 Grain, aspirated grain fractions ...... 10 Wheat, straw ...... 2 .0 Grain, cereal, forage, fodder, and straw, group 16, forage ...... 15 (b) Section 18 emergency exemptions. Grain, cereal, forage, fodder, and straw, group 16, hay ...... 5 Time-limited tolerances specified in Grain, cereal, forage, fodder, and straw, group the following table are established for 16, stover ...... 10 residues of sulfoxaflor (N- Grain, cereal, forage, fodder, and straw, group 16, straw ...... 2 [methyloxido[1-[6-(trifluoromethyl)-3- Grain, cereal, group 15, except rice and barley 0 .04 pyridinyl]ethyl]- λ4- Hog, fat ...... 0 .01 sulfanylidene]cyanamide), including its Hog, meat ...... 0 .01 Hog, meat byproducts ...... 0 .01 metabolites and degradates, in or on Horse, fat ...... 0 .01 the specified agricultural commodities, Horse, meat ...... 0 .01 resulting from use of the pesticide pur- Horse, meat byproducts ...... 0 .01 Milk ...... 0.01 suant to FIFRA section 18 emergency Pea and bean, dried shelled, except soybean, exemptions. Compliance with the toler- subgroup 6C ...... 0 .06 ance levels specified in the following Poultry, fat ...... 0.01 Poultry, meat ...... 0 .01 table is to be determined by measuring Poultry, meat byproducts ...... 0.01 only sulfoxaflor in or on the com- Rapeseed subgroup 20A ...... 0 .08 modity. The tolerances expire on the Sheep, fat ...... 0 .01 Sheep, meat ...... 0.01 date specified in the table. Sheep, meat byproducts ...... 0 .01 Soybean, forage ...... 1 Parts Expiration/ Soybean, hay ...... 3 Commodity per revocation Soybean, hulls ...... 0 .2 million date Soybean, seed ...... 0 .05 Vegetable, foliage of legume, except soybean, Sorghum, forage ...... 0.40 12/31/17 subgroup 7A ...... 40 Sorghum, grain ...... 0.30 12/31/17 Wheat, bran ...... 0.06 Sorghum, stover ...... 0.90 12/31/17 Wheat, germ ...... 0 .09

(c) Tolerances with regional registra- (b) Section 18 emergency exemptions. tions. [Reserved] [Reserved] (d) Indirect or inadvertent residues. (c) Tolerances with regional registra- [Reserved] tions. [Reserved] (d) Indirect or inadvertent residues. [77 FR 59565, Sept. 28, 2012, as amended at 78 [Reserved] FR 38227, June 26, 2013; 80 FR 4515, Jan. 28, 2015] [77 FR 72231, Dec. 5, 2012]

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§ 180.671 Fenpyrazamine; tolerances Commodity Parts per for residues. million (a) General. Tolerances are estab- Citrus, oil ...... 2.4 lished for residues of the fungicide Cotton, gin byproducts ...... 10 Fruit, citrus (group 10–10) ...... 0 .70 fenpyrazamine, in or on the following Fruit, pome (group 11–10) ...... 1 .5 commodities. Compliance with the tol- Goat, fat ...... 0 .01 erance levels specified in the following Goat, meat ...... 0.01 Goat, meat byproducts ...... 0 .01 table is to be determined by measuring Horse, fat ...... 0 .01 only fenpyrazamine S-allyl 5-amino-2- Horse, meat ...... 0 .01 isopropyl-4-(2-methylphenyl)-3-oxo-2,3- Horse, meat byproducts ...... 0 .01 Milk ...... 0.01 dihydropyrazole-1-carbothioate, in or Nut, tree (group 14–12) ...... 0 .04 on the following commodities: Oilseed (group 20) ...... 1 .5 Onion, bulb (subgroup 3–07A) ...... 0 .04 Commodity Parts per Onion, green (subgroup 3–07B) ...... 8 .0 million Peach (subgroup 12–12B) ...... 1 .5 Plum (subgroup 12–12C) ...... 0 .50 Almond ...... 0.02 Sheep, fat ...... 0 .01 Almond, hulls ...... 1 .5 Sheep, meat ...... 0.01 Berry, low growing, subgroup 13–07G ...... 3 Sheep, meat byproducts ...... 0 .01 Bushberry subgroup 13–07B ...... 5 Vegetable, cucurbit (group 9) ...... 0 .40 Caneberry subgroup 13–07A ...... 5 Vegetable, fruiting (group 8–10) ...... 2 .0 Fruit, small vine climbing, except fuzzy kiwifruit, Vegetable, leafy (except Brassica) (group 4) ...... 20 subgroup 13–07F ...... 3 Vegetable, tuberous and corm (subgroup 1C) .... 0 .15 Ginseng ...... 0 .7 Grape, juice ...... 4 Lettuce, head ...... 1.5 (b) Section 18 emergency exemptions. Lettuce, leaf ...... 2 [Reserved] Pistachio ...... 0.02 (c) Tolerances with regional registrations. [Reserved] (b) Section 18 emergency exemptions. (d) Indirect or inadvertent residues. [Reserved] Tolerances are established for indirect (c) Tolerances with regional registra- or inadvertent tolerances for residues tions. [Reserved] of cyantraniliprole, 3-bromo-1-(3- (d) Indirect or inadvertent residues. chloro-2-pyridinyl)-N-[4-cyano-2-meth- [Reserved] yl-6-[(methylamino)carbonyl]phenyl]- [78 FR 14465, Mar. 6, 2013] 1H-pyrazole-5-carboxamide, including its metabolites and degradates, in or § 180.672 Cyantraniliprole; tolerances on commodities in the following table. for residues. Compliance with the tolerance levels (a) General. Tolerances are estab- specified in the following table is to be lished for the combined residues of the determined by measuring only insecticide cyantraniliprole, 3-bromo-1- cyantraniliprole in or on the com- (3-chloro-2-pyridinyl)-N-[4-cyano-2- modity. methyl-6- Parts per [(methylamino)carbonyl]phenyl]-1H- Commodity million pyrazole-5-carboxamide, including its metabolites and degradates, in or on Animal feed, nongrass (group 18) ...... 0.20 Grain, cereal, forage, fodder and straw (group commodities in the following table. 16) ...... 0 .50 Compliance with the tolerance levels Grass forage, fodder and hay (group 17) ...... 0 .50 specified in the following table is to be Peanut, hay ...... 0.01 determined by measuring only Vegetable, foliage of legume (group 7) ...... 0 .70 Vegetable, leaves of root and tuber vegetables cyantraniliprole in or on the com- (group 2) ...... 0 .04 modity. Vegetable, root (subgroup 1A) ...... 0 .02

Parts per Commodity million [79 FR 6833, Feb. 5, 2014] Almond, hulls ...... 8 .0 § 180.673 Triforine; tolerances for resi- Brassica head and stem (subgroup 5A) ...... 3 .0 dues. Brassica leafy vegetables (subgroup 5B) ...... 30 Bushberry (subgroup 13–07B) ...... 4 .0 (a) General. Tolerances are estab- Cattle, fat ...... 0.01 lished for residues of triforine, includ- Cattle, meat ...... 0 .01 Cattle, meat byproducts ...... 0.01 ing its metabolites and degradates. Cherry (subgroup 12–12A) ...... 6 .0 Compliance with the tolerance levels

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specified in the following table is to be tolyloxy)benzyl]pyrazole-5- determined by measuring only triforine carboxamide. (N,N′-[1,2-piperazinediylbis(2,2,2- Parts per trichloroehylidene)]bis[formamide]), in Commodity million or on the following commodities. Almond hulls ...... 6 .0 Parts per Citrus, dried pulp ...... 8 .0 Commodity million Citrus, oil ...... 70.0 Cotton, gin byproducts ...... 15 .0 Blueberry 1 ...... 1 .0 Cotton, undelinted seed ...... 0 .70 Tomato 1 ...... 0.5 Fruit, stone, group 12–12 ...... 2 .0 Fruits, citrus, group 10–10 ...... 1 .5 1 There are no U.S. registrations for blueberry and tomato. Grape ...... 2 .0 (b) Section 18 emergency exemptions. Grape, raisin ...... 6 .0 Nuts, tree, group 14–12 ...... 0 .05 [Reserved] Persimmon ...... 2 .0 (c) Tolerances with regional registra- Plum, prune ...... 3 .0 tions. [Reserved] Pomegranate ...... 2 .0 Potato ...... 0 .01 (d) Indirect or inadvertent residues. Tea ...... 30 .0 [Reserved] Vegetable, leafy, except Brassica, group 4 ...... 30 .0

[78 FR 32151, May 29, 2013. Redesignated at 78 (2) Tolerances are established for res- FR 36677, June 19, 2013] idues of the insecticide tolfenpyrad, in- § 180.674 Proquinazid; tolerances for cluding its metabolites and degradates, residues. in or on the commodities in the following table. Compliance with the tol- (a) General. Tolerances are estab- erance levels specified below is to be lished for residues of the fungicide, determined by measuring only the sum proquinazid, including its metabolites of tolfenpyrad, 4-chloro-3-ethyl-1-meth- and degradates, in or on the commod- yl-N-[4-(p-tolyloxy)benzyl]pyrazole-5- ities listed in the following table. Com- carboxamide, and its metabolite 4-[4- pliance with the tolerance levels speci- [(4-chloro-3-ethyl-1-methylpyrazol-5- fied in the following table is to be de- yl)carbonylamino-methyl]phenoxy]- termined by measuring only benzoic acid, calculated as the stoi- proquinazid, [6-Iodo-2-propoxy-3- chiometric equivalent of tolfenpyrad. propyl-3H-quinazolin-4-one), in or on the following commodities: Parts per Commodity million Parts per Commodity million Cattle, fat ...... 0.01 Cattle, meat ...... 0 .01 Grape 1 ...... 0 .50 Cattle, meat byproducts ...... 0.35 Grape, raisin 1 ...... 1 .0 Goat, fat ...... 0 .01 Goat, meat ...... 0.01 1 No U.S. registrations for Proquinazid. Goat, meat byproducts ...... 0 .35 (b) Section 18 emergency exemptions. Horse, fat ...... 0 .01 Horse, meat ...... 0 .01 [Reserved] Horse, meat byproducts ...... 0 .35 (c) Tolerances with regional registra- Milk ...... 0.03 tions. [Reserved] Sheep, fat ...... 0 .01 Sheep, meat ...... 0.01 (d) Indirect or inadvertent residues. Sheep, meat byproducts ...... 0 .35 [Reserved] [79 FR 18815, Apr. 4, 2014] (b) Section 18 emergency exemptions. [Reserved] § 180.675 Tolfenpyrad; tolerances for (c) Tolerances with regional registra- residues. tion. [Reserved] (a) General. (1) Tolerances are estab- (d) Indirect or inadvertent residues. lished for residues of the insecticide [Reserved] tolfenpyrad, including its metabolites [79 FR 1605, Jan. 9, 2014] and degradates, in or on the commodities in the table below. Compliance § 180.676 Fenpropidin; tolerances for with the tolerance levels specified residues. below is to be determined by measuring (a) General. Tolerances are estab- only tolfenpyrad, 4-chloro-3-ethyl-1- lished for the residues of fenpropidin, methyl-N-[4-(p- including its metabolites and

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degradates, in or on the commodities with the tolerance levels specified in the table below. Compliance with below is to be determined by measuring the tolerance levels specified below is only tricyclazole (5-methyl-1,2,4- to be determined by measuring only triazolo[3,4-b ]benzothiazole). fenpropidin (1-[3-[4-(1,1- Parts dimethylethyl)phenyl]-2- Commodity per million methylpropyl]piperidine). Rice, grain 1 ...... 3 .0

Parts per 1 Commodity million There are no U.S. Registrations on Rice as of June 11, 2014. Banana 1 ...... 10 (b) Section 18 emergency exemptions. 1 There are no U.S. registrations as of December 13, 2013. [Reserved] (b) Section 18 tolerance. [Reserved] (c) Tolerances with regional registra- (c) Tolerances with regional registrations. [Reserved] tions. [Reserved] (d) Indirect or inadvertent residues. (d) Indirect or inadvertent residues. [Reserved] [Reserved] [79 FR 33468, June 11, 2014] [79 FR 8096, Feb. 11, 2014] § 180.679 Flupyradifurone; tolerances § 180.677 Cyflumetofen; tolerances for for residues. residues. (a) General. Tolerances are estab- (a) General. Tolerances are established for residues of the insecticide lished for residues of the insecticide flupyradifurone, including its metabo- cyflumetofen, including its metabolites lites and degradates, in or on the com- and degradates, in or on the commod- modities in the following table. Com- ities in the table below. Compliance pliance with the tolerance levels speci- with the tolerance levels for fied in the following table is to be de- cyflumetofen is to be determined by termined by measuring only measuring only cyflumetofen, 2- flupyradifurone, 4-[[(6-chloro-3- methoxyethyl a-cyano-a-[4-(1,1- pyridinyl)methyl](2,2- dimethylethyl)phenyl]-b-oxo-2- difluoroethyl)amino]- 2(5H)-furanone. (trifluoromethyl)benzenepropanoate, in Parts per or on the commodity. Commodity million

Commodity Parts per Alfalfa, forage ...... 9.0 million Alfalfa, hay ...... 20 Almond, hulls ...... 15 Almond, hulls ...... 4 .0 Bean, succulent ...... 0 .20 Citrus, oil ...... 16 Fruit, citrus, group 10–10 ...... 0 .30 Berry, low growing, except cranberry subgroup Fruit, pome, group 11–10 ...... 0 .30 13–07G ...... 1 .5 Grape ...... 0 .60 Brassica, head and stem subgroup 5A ...... 6 .0 Nut, tree, group 14–12 ...... 0 .01 Brassica, leafy greens subgroup 5B ...... 40 Strawberry ...... 0 .60 Bushberry, except cranberry subgroup 13–07B 4 .0 Tomato ...... 0.40 Cactus, fruit ...... 0 .30 Cactus, pads ...... 0 .70 Cattle, fat ...... 0.20 (b) Section 18 emergency exemptions. Cattle, meat ...... 0 .30 [Reserved] Cattle, meat byproducts ...... 1.0 (c) Tolerances with regional registra- Coffee, green bean 1 ...... 1 .5 tions. [Reserved] Corn, field, grain ...... 0 .05 Corn, pop, grain ...... 0.05 (d) Indirect or inadvertent residues. Corn, sweet, kernels plus cobs with husks re- [Reserved] moved ...... 0 .05 Cotton, gin byproducts ...... 40 [79 FR 29108, May 21, 2014] Cottonseed, subgroup 20C ...... 0 .80 Egg ...... 0 .01 § 180.678 Tricyclazole; tolerances for Fruit, citrus, dried pulp ...... 10 residues. Fruit, citrus, group 10–10 ...... 3 .0 Fruit, pome, group 11–10 ...... 0 .70 (a) General. (1) Tolerances are estab- Fruit, small vine climbing, except fuzzy lished for residues of the fungicide kiwifruit, subgroup 13–07F ...... 3.0 tricyclazole, including its metabolites Goat, fat ...... 0 .20 Goat, meat ...... 0.30 and degradates, in or on the commod- Goat, meat byproducts ...... 1 .0 ities in the table below. Compliance Grain, aspirated grain fractions ...... 40

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Commodity Parts per § 180.680 Fluensulfone; tolerances for million residues. Grain, cereal, forage, fodder and straw, group (a) General. Tolerances are estab- 16 ...... 30 lished for residues of the nematicide Grain, cereal, group 15, except rice and corn .. 3.0 fluensulfone, including its metabolites Grape, raisin ...... 5 .0 Hog, fat ...... 0 .01 and degradates, in or on the commod- Hog, meat ...... 0 .01 ities in the table below. Compliance Hog, meat byproducts ...... 0 .04 with the tolerance levels specified Hops, dried cones ...... 10 below is to be determined by measuring Horse, fat ...... 0 .20 only 3,4,4-trifluoro-but-3-ene-1-sulfonic Horse, meat ...... 0 .30 acid. Horse, meat byproducts ...... 1 .0 Leaf petioles, subgroup 4B ...... 9 .0 Parts per Leafy greens, subgroup 4A ...... 30 Commodity million Milk ...... 0.15 Nut, tree, group 14–12 ...... 0 .02 Berry, low growing, subgroup 13–07G ...... 0 .30 Onion, bulb, subgroup 3–07A ...... 0 .09 Brassica, head and stem, subgroup 5A ...... 1 .50 Brassica, leafy greens, subgroup 5B ...... 9 .0 Onion, green, subgroup 3–07B ...... 3 .0 Potato, chips ...... 0 .60 Pea and bean, dried, shelled except soybean, Potato, granules/flakes ...... 0 .80 subgroup 6C ...... 3 .0 Tomato, paste ...... 1 .0 Pea, succulent ...... 2 .0 Vegetables, cucurbits, group 9 ...... 0.50 Peanut ...... 0 .04 Vegetables, fruiting, group 8–10 ...... 0 .50 Peanut, hay ...... 20 Vegetables, leafy, except Brassica, group 4 ..... 2 .0 Pitaya ...... 0 .30 Vegetables, leaves of root and tuber, group 2, Sheep, fat ...... 0 .20 except sugar beet ...... 30 Sheep, meat ...... 0.30 Vegetables, root, except sugar beet, subgroup Sheep, meat byproducts ...... 1 .0 1B ...... 3 .0 Vegetables, tuberous and corm, subgroup 1C 0.50 Soybean, seed ...... 1 .5 Taro leaves ...... 30 Turnip greens ...... 40 (b) Section 18 emergency exemptions. Vegetable, cucurbit, group 9 ...... 0.40 [Reserved] Vegetable, foliage of legume, group 7 ...... 30 (c) Tolerances with regional registra- Vegetable, fruiting, group 8–10 ...... 1 .5 tions. [Reserved] Vegetable, legume, edible podded, subgroup (d) Indirect or inadvertant residues. 6A ...... 3 .0 Vegetable, root, except sugar beet, subgroup [Reserved] 1B ...... 0 .90 [81 FR 34901, June 1, 2016] Vegetable, tuberous and corm, subgroup 1C ... 0.05 1 No U.S. registration. § 180.681 Isofetamid; tolerances for residues. (b) Section 18 emergency exemptions. [Reserved] (a) General. Tolerances are estab- (c) Tolerances with regional restric- lished for residues of the fungicide tions. Tolerances are established for isofetamid, including its metabolites residues of the insecticide and degradates, in or on the commod- flupyradifurone, including its metabo- ities in the table below. Compliance lites and degradates, in or on the com- with the tolerance levels specified modities in the following table. Com- below is to be determined by measuring pliance with the tolerance levels speci- only isofetamid, N-[1,1-dimethyl-2-[2- fied in the following table is to be demethyl-4-(1-methylethoxy)phenyl]-2- termined by measuring only oxoethyl]-3-methyl-2- flupyradifurone, 4-[[(6-chloro-3- thiophenecarboxamide, in or on the fol- pyridinyl)methyl](2,2- lowing commodities: difluoroethyl)amino]- 2(5H)-furanone. Parts per Commodity million Parts per Commodity million Almond ...... 0.01 Almond, hulls ...... 0 .01 Clover, forage ...... 20 Berry, low growing, subgroup 13–07G ...... 4 .0 Clover, hay ...... 30 Canola, refined oil ...... 0 .03 Flax, seed, oil ...... 0 .03 Fruit, small vine climbing, except fuzzy (d) Indirect or inadvertent residues. kiwifruit, subgroup 13–07F ...... 3.0 [Reserved] Grape, raisin ...... 5 .0 Lettuce, head ...... 5.0 [80 FR 3487, Jan. 23, 2015] Lettuce, leaf ...... 7 .0

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Commodity Parts per § 180.684 Benalaxyl-M; tolerances for million residues. Mustard, seed, oil ...... 0 .03 (a) General. Tolerances are estab- Rapeseed subgroup 20A ...... 0 .015 lished for residues of the fungicide Sesame, oil ...... 0 .03 benalaxyl-M, including its metabolites and degradates, in or on the commod- (b) Section 18 emergency exemptions. ities in the table below. Compliance [Reserved] with the tolerance levels specified (c) Tolerances with regional registra- below is to be determined by measuring tions. [Reserved] only benalaxyl [methyl N-(2,6- (d) Indirect or inadvertent residues. dimethylphenyl)-N-(phenylacetyl)-DL- [Reserved] alaninate] in or on the commodity. [80 FR 45443, July 30, 2015] Parts per Commodity million § 180.682 Bicyclopyrone; tolerances for residues. Grape 1 ...... 3 .0 Tomato 1 ...... 0.20 (a) General. (1) Tolerances are estab- 1 There is no U.S. registration for use on this commodity as lished for residues of the herbicide of July 30, 2015. bicyclopyrone (4-hydroxy-3-[[2-[(2- methoxyethoxy)methyl]-6- (b) Section 18 emergency exemptions. (trifluoromethyl)-3- [Reserved] pyridinyl]carbonyl]bicyclo[3.2.1]oct-3- (c) Tolerances with regional registra- en-2-one), including its metabolites and tions. [Reserved] (d) degradates, in or on the commodities Indirect or inadvertent residues. [Reserved] in the table below. Compliance with the tolerance levels specified below is [80 FR 45448, July 30, 2015] to be determined by measuring only the sum of the common moieties § 180.685 Oxathiapiprolin; tolerances SYN503780 (2-[(2- for residues. methoxyethoxy)methyl]-6- (a) General. (1) Tolerances are estab- (trifluoromethyl)-3-pyridinecarboxylic lished for residues of the fungicide acid) and CSCD686480 (2-[(2- oxathiapiprolin, including its metabo- hydroxyethoxy)methyl]-6- lites and degradates, in or on the com- (trifluoromethyl)-3-pyridinecarboxylic modities in the table below. Compli- acid), calculated as the stoichiometric ance with the tolerance levels specified equivalent of bicyclopyrone, in or on below is to be determined by measuring the commodities. only oxathiapiprolin, 1-[4-[4-[5-(2,6- difluorophenyl)-4,5-dihydro-3- Parts per Commodity million isoxazolyl]-2-thiazolyl]-1-piperidinyl]-2- [5-methyl-3-(trifluoromethyl)-1H- Corn, field, forage ...... 0 .30 pyrazol-1-yl]-ethanone, in or on the Corn, field, grain ...... 0 .02 commodity. Corn, field, stover ...... 0 .40 Corn, pop, grain ...... 0.02 Parts per Corn, pop, stover ...... 0.40 Commodity million Corn, sweet, forage ...... 0 .40 Corn, sweet, kernel plus cob with husks re- Brassica, head and stem, subgroup 5A ...... 1 .5 moved ...... 0 .03 Ginseng ...... 0 .15 1 Corn, sweet, stover ...... 0 .70 Grape ...... 0 .70 Sugarcane, cane 1 ...... 0.02 Leafy greens subgroup 4A ...... 15 Onion, bulb, subgroup 3–07A ...... 0 .04 Cattle, meat byproducts ...... 1.5 Onion, green, subgroup 3–07B ...... 2 .0 Goat, meat byproducts ...... 1 .5 Pea, edible-podded ...... 1 .0 Sheep, meat byproducts ...... 1 .5 Pea, succulent shelled ...... 0 .05 Horse, meat byproducts ...... 1 .5 Tomato, dried ...... 3 .0 Hog, meat byproducts ...... 0 .15 Vegetable, cucurbit, group 9 ...... 0.20 Vegetable, fruiting, group 8–10 ...... 0 .50 1 There are no U.S. Registrations on Sugarcane as of March 13, 2015. Vegetable, tuberous and corm, subgroup 1C ... 0.01 1 There is no associated U.S. registration as of September (2) [Reserved] 4, 2015. (b) [Reserved] (b) Section 18 emergency exemptions. [80 FR 22654, Apr. 23, 2015] [Reserved]

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(c) Tolerances with regional registra- Commodity Parts per tions. [Reserved] million (d) Indirect or inadvertent residues. Goat, fat ...... 0 .02 Tolerances are established for residues Goat, liver ...... 0.06 of the fungicide oxathiapiprolin, in- Goat, meat ...... 0.01 cluding its metabolites and degradates, Goat, meat byproducts, except liver ...... 0 .01 Grain, aspirated fractions ...... 15.0 in or on the commodities in the table Grape, raisin ...... 3 .0 below. Compliance with the tolerance Horse, fat ...... 0 .02 levels specified below is to be deter- Horse, liver ...... 0 .06 mined by measuring only Horse, meat ...... 0 .01 Horse, meat byproducts, except liver ...... 0 .01 oxathiapiprolin, 1-[4-[4-[5-(2,6- Milk ...... 0.01 difluorophenyl)-4,5-dihydro-3- Milk, fat ...... 0 .02 isoxazolyl]-2-thiazolyl]-1-piperidinyl]-2- Oat, grain ...... 1 .5 [5-methyl-3-(trifluoromethyl)-1H- Oat, hay ...... 15.0 Oat, straw ...... 15.0 pyrazol-1-yl]-ethanone, in or on the Pea and bean, dried shelled, except soybean, commodity. subgroup 6C ...... 0 .20 Pea, field, hay ...... 7.0 Commodity Parts per Pea, field, vine ...... 1 .5 million Peanut ...... 0 .01 Peanut, hay ...... 15.0 All other food commodities/feed commodities Potato, processed potato waste ...... 0 .10 (other than those covered by a tolerance as a Rapeseed, subgroup 20A ...... 0.15 result of use on growing crops) ...... 0.10 Rye, grain ...... 0.1 Rye, hay ...... 15 .0 [80 FR 53473, Sept. 4, 2015] Rye, straw ...... 15 .0 Sheep, fat ...... 0 .02 § 180.686 Benzovindiflupyr; tolerances Sheep, liver ...... 0.06 Sheep, meat ...... 0.01 for residues. Sheep meat byproducts, except liver ...... 0 .01 (a) General. Tolerances are estab- Soybean, forage ...... 15 .0 lished for residues of the fungicide Soybean, hay ...... 50 .0 Soybean, hulls ...... 0 .20 benzovindiflupyr, including its metabo- Soybean, seed ...... 0 .07 lites and degradates, in or on the com- Sugarcane, cane1 ...... 0 .04 modities in the table below. Compli- Tomato, dried ...... 4 .0 ance with the tolerance levels specified Vegetable, cucurbit, group 9 ...... 0.30 Vegetable, fruiting, group 8–10 ...... 1 .5 below is to be determined by measuring Vegetable, tuberous and corm, subgroup 1C ... 0.02 only benzovindiflupyr (N-[9- Wheat, forage ...... 4 .0 (dichloromethylene)-1,2,3,4-tetrahydro- Wheat, grain ...... 0 .10 1,4-methanonaphthalen-5-yl]-3- Wheat, hay ...... 15 .0 Wheat, straw ...... 15 .0 (difluoromethyl)-1-methyl-1H-pyrazole- 4-carboxamide) in or on the com- 1 There is no U.S. registration for use of benzovindiflupyr. modity. (b) Section 18 emergency exemptions. [Reserved] Parts per Commodity million (c) Tolerances with regional registrations. [Reserved] Barley, grain ...... 1 .5 Barley, hay ...... 15 .0 (d) Indirect or inadvertent residues. Barley, straw ...... 15 .0 [Reserved] Cattle, fat ...... 0.02 Cattle, liver ...... 0 .06 [80 FR 59633, Oct. 2, 2015] Cattle, meat ...... 0 .01 Cattle, meat byproducts, except liver ...... 0 .01 § 180.687 Teflubenzuron; tolerances for Coffee, green bean1 ...... 0 .09 residues. Corn, field, forage ...... 3 .0 Corn, field, grain ...... 0 .02 (a) General. (1) Tolerances are estab- Corn, field, stover ...... 15 .0 lished for residues of the insecticide Corn, pop, grain ...... 0.02 Corn, pop, stover ...... 15.0 teflubenzuron, including its metabo- Corn, sweet, forage ...... 4 .0 lites and degradates, in or on the com- Corn, sweet, kernel plus cob with husks re- modities in the table below. Compli- moved ...... 0 .01 Corn, sweet, stover ...... 5 .0 ance with the tolerance levels specified Cottonseed, subgroup 20C ...... 0 .15 below is to be determined by measuring Cotton, gin byproducts ...... 3 .0 only teflubenzuron (N-[[(3,5-dichloro- Fruit, pome, group 11–10 ...... 0 .20 Fruit, small vine climbing, except fuzzy 2,4-difluorophenyl)amino]carbonyl]-2,6- kiwifruit, subgroup 13–07F ...... 1.0 difluorobenzamide).

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Commodity Parts per Subpart D—Exemptions From million Tolerances Apple 1 ...... 1.0 Broccoli 1 ...... 0 .20 § 180.900 Exemptions from the require- Cauliflower 1 ...... 0 .01 ment of a tolerance. Citrus, oil 1 ...... 100 Coffee, bean, green 1 ...... 0 .60 An exemption from a tolerance shall Corn, field, grain 1 ...... 0 .01 be granted when it appears that the Corn, field, refined oil 1 ...... 0 .02 total quantity of the pesticide chem- Lemon 1 ...... 0.80 ical in or on all raw agricultural com- Mango 1 ...... 1.5 modities for which it is useful under 1 Melon, subgroup 9A ...... 0 .30 conditions of use currently prevailing Orange 1 ...... 0 .60 Papaya 1 ...... 0 .50 or proposed will involve no hazard to Pineapple 1 ...... 0.80 the public health. Soybean, seed 1 ...... 0 .05 Soybean, hulls 1 ...... 0 .15 [69 FR 23117, Apr. 28, 2004] Sugarcane, cane 1 ...... 0.01 Sunflower, seed 1 ...... 0.30 § 180.905 Pesticide chemicals; exemp- Tomato 1 ...... 1.5 tions from the requirement of a tolerance. 1 There are no U.S. registrations as of October 30, 2015. (a) When applied to growing crops, in (b) Section 18 emergency exemptions. accordance with good agricultural [Reserved] practice, the following pesticide chemi- (c) Tolerances with regional registra- cals are exempt from the requirement tions. [Reserved] of a tolerance: (d) Indirect or inadvertent residues. (1) Petroleum oils. [Reserved] (2) Piperonyl butoxide. [80 FR 66809, Oct. 30, 2015] (3) Pyrethrins. (4) Sabadilla. § 180.688 Diethofencarb; tolerance for (b) When applied to growing crops, in residue. accordance with good agricultural (a) General. (1) Tolerances are estab- practice, the pesticides rotenone or lished for residues of the fungicide derris or cube roots are exempt from diethofencarb, including its metabo- the requirement of a tolerance. There lites and degradates, in or on the com- are no U.S. registrations for use of ro- modities in the table below. Compli- tenone, derris, or cube roots on food ance with the tolerance levels specified commodities as of March 23, 2011. below is to be determined by measuring (c) These pesticides are not exempted only diethofencarb (1-methylethyl N- from the requirement of a tolerance (3,4-diethoxyphenyl)carbamate). when applied to a crop at the time of or after harvest. Parts per Commodity million [77 FR 59128, Sept. 26, 2012]

Banana * ...... 0 .10 § 180.910 Inert ingredients used pre- and post-harvest; exemptions from * There is no U.S. registration for use on this commodity as of November 4, 2015. the requirement of a tolerance. (b) Section 18 emergency exemptions. Residues of the following materials [Reserved] are exempted from the requirement of (c) Tolerances with regional registra- a tolerance when used in accordance tions. [Reserved] with good agricultural practice as inert (d) Indirect or inadvertent residues [Re- (or occasionally active) ingredients in served] pesticide formulations applied to growing crops or to raw agricultural com- [80 FR 68261, Nov. 4, 2015] modities after harvest:

Inert ingredients Limits Uses

Acetic acid ...... Catalyst Acetic anhydride ...... Solvent, cosolvent Acetone ...... Do.

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Inert ingredients Limits Uses

Alkanoic and alkenoic acids, mono- and diesters of ...... Emulsifiers a-hydro-w-hydroxypoly (oxyethylene) with molecular weight (in amu) range of 200 to 6,000.

Alkyl (C8-C24) benzenesulfonic acid and its ammo- ...... Surfactants, related adjuvants of surfactants nium, calcium, magnesium, potassium, sodium, and zinc salts.

C10-C18-Alkyl dimethyl amine oxides (CAS Reg. 15% by weight in pesticide Surfactant Nos. 1643–20–5, 2571–88–2, 2605–79–0, 3332– formulation. 27–2, 61788–90–7, 68955–55–5, 70592–80–2, 7128–91–8, 85408–48–6, and 85408–49–7).

a-alkyl(C6- C15)-w-hydroxypoly(oxyethylene)sulfate, Not to exceed 30% of for- Surfactants, related adjuvants of surfactants. and its ammonium, calcium, magnesium, potas- mulation. sium, sodium, and zinc salts, poly(oxyethylene) content averages 2–4 moles (CAS Reg. Nos.: 3088–31–1, 3694–74–4, 9004–82–4, 9004–84– 6, 9021–91–4, 9086–52–6, 13150–00–0, 15826– 16–1, 25446–78–0, 26183–44–8, 27140–00–7, 27731–62–0, 32612–48–9, 34431–25–9, 35015– 74–8, 50602–06–7, 52286–18–7, 52286–19–8, 54116–08–4, 55901–67–2, 61702–79–2, 61894– 66–4, 62755–21–9, 63428–85–3, 63428–86–4, 63428–87–5, 65086–57–9, 65086–79–5, 65104– 74–7, 65122–38–5, 67674–66–2, 67762–19–0, 67762–21–4, 67845–82–3, 67845–83–4, 67923– 90–4, 68037–05–8, 68037–06–9, 68171–41–5, 68424–50–0, 68511–39–7, 68585–34–2, 68610– 66–2, 68611–29–0, 68611–55–2, 68649–53–6, 68890–88–0, 68891–29–2, 68891–30–5, 68891– 38–3, 69011–37–6, 73665–22–2, 75422–21–8, 78330–16–2, 78330–17–3, 78330–25–3, 78330– 26–4, 78330–27–5, 78330–28–6, 78330–29–7, 78330–30–0, 96130–61–9, 106597–03–9, 110392–50–2, 119432–41–6, 125301–88–4, 125301–89–5, 125301–92–0, 125736–54–1, 157707–85–2, 160104–51–8, 160901–27–9, 160901–28–0, 160901–29–1, 160901–30–4, 161025–28–1, 161074–79–9, 162063–19–6, 219756–63–5).

a-alkyl (C12-C15)-w-hydroxypoly (oxypropylene) Not more than 20% of pes- Surfactant poly (oxyethylene) copolymers (where the poly ticide formulations. (oxypropylene) content is 3–60 moles and the poly (oxyethylene) content is 5–80 moles). a-alkyl-w-hydroxypoly (oxypropylene) and/or poly ...... Surfactants, related adjuvants of surfactants (oxyethylene) polymers where the alkyl chain contains a minimum of six carbons (CAS Reg. Nos.: 9002–92–0; 9004–95–9; 9004–98–2; 9005–00–9; 9035–85–2; 9038–29–3; 9038–43– 1; 9040–05–5; 9043–30–5; 9087–53–0; 25190– 05–0; 24938–91–8; 25231–21–4; 251553–55–6; 26183–52–8; 26468–86–0; 26636–39–5; 27252– 75–1; 27306–79–2; 31726–34–8; 34398–01–1; 34398–05–5; 37251–67–5; 37311–00–5; 37311– 01–6; 37311–02–7; 37311–04–9; 39587–22–9; 50861–66–0; 52232–09–4; 52292–17–8; 52609– 19–5; 57679–21–7; 59112–62–8; 60828–78–6; 61702–78–1; 61725–89–1; 61791–13–7; 61791– 20–6; 61791–28–4; 61804–34–0; 61827–42–7; 61827–84–7; 62648–50–4; 63303–01–5; 63658– 45–7; 63793–60–2; 64366–70–7; 64415–24–3; 64415–25–4; 64425–86–1; 65104–72–5; 65150– 81–4; 66455–14–9: 66455–15–0; 67254–71–1; 67763–08–0; 68002–96–0; 68002–97–1; 68131– 39–5; 68131–40–8; 68154–96–1; 68154–97–2; 68154–98–3; 68155–01–1; 68213–23–0; 68213– 24–1; 68238–81–3; 68238–82–4; 68409–58–5; 68409–59–6; 68439–30–5; 68439–45–2; 68439– 46–3; 68439–48–5; 68439–49–6; 68439–50–9; 68439–51–0; 68439–53–2; 68439–54–3; 68458– 88–8;.

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Inert ingredients Limits Uses

68526–94–3; 68526–95–4; 68551–12–2; 68551– 13–3; 68551–14–4; 68603–20–3; 68603–25–8; 68920–66–1; 68920–69–4; 68937–66–6; 68951– 67–7; 68954–94–9; 68987–81–5; 68991–48–0; 69011–36–5; 69013–18–9; 69013–19–0; 69227– 20–9; 69227–21–0; 69227–22–1; 69364–63–2; 70750–27–5; 70879–83–3; 70955–07–6; 71011– 10–4; 71060–57–6; 71243–46–4; 72066–65–0; 72108–90–8; 72484–69–6; 72854–13–8; 72905– 87–4; 73018–31–2; 73049–34–0; 74432–13–6; 74499–34–6; 78330–19–5; 78330–20–8; 78330– 21–9; 78330–23–1; 79771–03–2; 84133–50–6; 85422–93–1; 97043–91–9; 97953–22–5; 102782–43–4; 103331–86–8; 103657–84–7; 103657–85–8; 103818–93–5; 103819–03–0; 106232–83–1; 111905–54–5; 116810–31–2; 116810–32–3; 116810–33–4; 120313–48–6; 120944–68–5; 121617–09–2; 126646–02–4; 126950–62–7; 127036–24–2; 139626–71–4; 152231–44–2; 154518–36–2; 157627–86–6; 157627–88–8; 157707–41–0; 157707–43–2; 159653–49–3; 160875–66–1; 160901–20–2; 160901–09–7; 160901–19–9; 161025–21–4; 161025–22–5; 166736–08–9; 169107–21–5; 172588–43–1; 176022–76–7; 196823–11–7; 287935–46–0; 288260–45–7; 303176–75–2; 954108–36–2)

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Inert ingredients Limits Uses

a-alkyl (minimum C6 linear, branched, saturated Not to exceed 30% of for- Surfactants, related adjuvants of surfactants. and/or unsaturated)-w-hydroxypolyoxyethylene mulation. polymer with or without polyoxypropylene, mixture of di- and monohydrogen phosphate esters and the corresponding ammonium, calcium, magnesium, monoethanolamine, potassium, sodium, and zinc salts of the phosphate esters; minimum oxyethylene content is 2 moles; minimum oxypropylene content is 0 moles (CAS Reg. Nos.: 9004–80–2, 9046–01–9, 26982–05– 8, 31800–89–2, 37280–82–3, 37281–86–0, 39341–09–8, 39341–65–6, 39464–66–9, 39464– 69–2, 42612–52–2, 50643–20–4, 50668–50–3, 51325–10–1, 51884–64–1, 52019–36–0, 57486– 09–6, 58206–38–5, 58318–92–6, 58857–49–1, 59112–71–9, 60267–55–2, 61837–79–4, 62362– 49–6, 62482–61–5, 63747–86–4, 63887–54–7, 63887–55–8, 66020–37–9, 66272–25–1, 66281– 20–7, 67711–84–6, 67786–06–5, 67989–06–4, 68070–99–5, 68071–17–0, 68071–35–2, 68071– 37–4, 68130–44–9, 68130–45–0, 68130–46–1, 68130–47–2, 68186–29–8, 68186–34–5, 68186– 36–7, 68186–37–8, 68238–84–6, 68311–02–4, 68311–04–6, 68332–75–2, 68389–72–0, 68400– 75–9, 68413–78–5, 68425–73–0, 68425–75–2, 68439–39–4, 68458–48–0, 68511–15–9, 68511– 36–4, 68511–37–5, 68551–05–3, 68585–15–9, 68585–16–0, 68585–17–1, 68585–36–4, 68585– 39–7, 68603–24–7, 68607–14–7, 68610–64–0, 68610–65–1, 68649–29–6, 68649–30–9, 68650– 84–0, 68815–11–2, 68855–46–9, 68856–03–1, 68890–90–4, 68890–91–5, 68891–12–3, 68891– 13–4, 68891–26–9, 68908–64–5, 68909–65–9, 68909–67–1, 68909–69–3, 68921–24–4, 68921– 60–8, 68954–87–0, 68954–88–1, 68954–92–7, 68987–35–9, 69029–43–2, 69980–69–4, 70247– 99–3, 70248–14–5, 70844–96–1, 70903–63–8, 71965–23–6, 71965–24–7, 72480–27–4, 72623– 67–7, 72623–68–8, 72828–56–9, 72828–57–0, 73018–34–5, 73038–25–2, 73050–08–5, 73050– 09–6, 73361–29–2, 73378–71–9, 73378–72–0, 73559–42–9, 73559–43–0, 73559–44–1, 73559– 45–2, 74499–76–6, 76930–25–1, 78041–18–6, 78330–22–0, 78330–24–2, 82465–25–6, 84843– 37–8, 91254–26–1, 93925–54–3, 95014–34–9, 96416–89–6, 99924–51–3, 103170–31–6, 103170–32–7, 106233–09–4, 106233–10–7, 108818–88–8, 110392–49–9, 111798–26–6, 111905–50–1, 116671–23–9, 117584–36–8, 119415–05–3, 120913–45–3, 121158–61–0, 121158–63–2, 123339–53–7, 125139–13–1, 125301–86–2, 125301–87–3, 126646–03–5, 129208–04–4, 129870–77–5, 129870–80–0, 130354–37–9, 136504–88–6, 143372–50–3, 143372–51–4, 144336–75–4, 146815–57–8, 151688–56–1, 154518–39–5, 154518–40–8, 155240–11–2, 159704–69–5, 160498–49–7, 160611–24–5, 171543–66–1, 172027–16–6, 172274–69–0, 176707–42–9, 181963–82–6, 188741–55–1, 191940–53–1, 210493–60–0, 210993–53–6, 246159–55–7, 251298–11–0, 261627–68–3, 290348–69–5, 290348–70–8, 317833–96–8, 340681–28–9 , 422563–19–7, 422563–26–6, 522613–09–8, 717140–06–2, 717140–09–5, 717827–29–7, 762245–80–7, 762245–81–8, 866538–89–8, 866538–90–1, 873662–29–4, 913068–96–9, 936100–29–7, 936100–30–0, 1072943–56–6, 1087209–87–7, 1174313–54–2, 1187742–89–7, 1187743–35–6, 1205632–03–6, 1233235–49–8, 1451002–50–8, 1456802–88–2, 1456802–89–3, 1456803–12–5).

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Inert ingredients Limits Uses

N-alkyl (C8-C18) primary amines and their acetate Concentration in formu- Surfactants, related adjuvants of surfactants salts where the alkyl group is linear and may be lated end-use products saturated and/or unsaturated (CAS Reg. Nos. not to exceed 10% by 61790–57–6, 61790–58–7, 61790–59–8, 61790– weight in herbicide prod- 60–1, 61788–46–3, 61790–33–8, 68155–38–4). ucts, 4% by weight in insecticide products, and 4% by weight in fungicide products. Alkyl (C8-C18) sulfate and its ammonium, calcium, ...... Surfactants. isopropylamine, magnesium, potassium, sodium, and zinc salts. Aluminum hydroxide ...... Diluent, carrier Aluminum oxide ...... Diluent Aluminum stearate ...... Surfactant Amides, C5-C9, N-[3-(dimethylamino) propyl] (CAS ...... Surfactant Reg. No. 1044764–00–2). Amides, C6-C12, N-[3-(dimethylamino) propyl] (CAS ...... Surfactant Reg. No. 1044764–06–8). Ammonium bicarbonate ...... Surfactant, suspending agent, dispersing agent Ammonium carbamate...... Synergist in aluminum phosphide formulations Ammonium chloride ...... Intensifier when used with ammonium nitrate as a dessicant or defoliant. Fire suppressant in aluminum phosphide and magnesium phosphide formulations Ammonium hydroxide ...... Solvent, cosolvent, neutralizer, solubilizing agent Ammonium salts of fatty acids (C8-C18 saturated) ...... Surfactant (CAS Reg. No. 5972–76–9, 63718–65–0, 16530–70–4, 32582–95–9, 2437–23–2, 191799– 95–8, 16530–71–5, 93917–76–1, 5297–93–8, 94266–36–1, 1002–89–7). Ammonium stearate ...... Surfactant Ammonium sulfate ...... Solid diluent, carrier Ammonium thiosulfate ...... Intensifier when used with ammonium nitrate as desiccant or defoliant Amyl acetate ...... Solvent, cosolvent, attractant Ascorbyl palmitate ...... Preservative Attapulgite-type clay ...... Solid diluent, carrier, thickener Bacillus thuringiensis fermentation solids and/or ...... Diluent, carrier solubles. Bentonite ...... Solid diluent, carrier Benzoic acid ...... Preservative for formulation Bicyclo[3.1.1]hept–2–ene, 2,6,6–trimethyl–, ...... Surfactants, related adjuvants of surfactants homopolymer (Alpha-pinene, homopolymer)(CAS Reg. No. 25766–18–1). Bicyclo[3.1.1]heptane, 6,6–dimethyl–2–methylene–, ...... Surfactants, related adjuvants of surfactants homopolymer (Beta-pinene, homopolymer) (CAS Reg. No. 25719–60–2). Bicyclo[3.1.1]hept–2–ene, 2,6,6–trimethyl–, poly- ...... Surfactants, related adjuvants of surfactants mer with 6,6–dimethyl–2–methylenebicyclo [3.1.1] heptane (Copolymer of alpha- and beta- pinene) (CAS Reg. No. 31393–98–3). 2-Bromo-2-nitro-1,3-propanediol (CAS Reg. No. 0.04% or less by weight of In-can preservative 52–51–7). the total pesticide formulation. Butane ...... Propellant Butanedioic acid, 2-sulfo-, C-C9-11-isoalkyl esters, Not to exceed 10% by Surfactant C10-rich, disodium salts (CAS Reg. No. weight in pesticide for- 815583–91–6). mulation for agricultural use. n-Butanol (CAS Reg. No. 71–36–3) ...... Solvent, cosolvent n-Butyl benzoate (CAS Reg. No.136–60–7) ...... Solvent Butylated hydroxyanisole ...... Antioxidant Butylated hydroxytoluene ...... Do. Calcareous shale ...... Solid diluent carrier Calcite ...... Do. Calcium carbonate ...... Do. Calcium chloride ...... Stabilizer Calcium phosphate ...... Solid diluent, carrier Calcium hydroxide ...... Do. Calcium hypochlorite ...... Sanitizing and bleaching agent

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Inert ingredients Limits Uses

Calcium lactate pentahydrate (CAS Reg. No...... Nutrient, stabilizer 5743–47–5). Calcium oxide ...... Solid diluent, carrier Calcium salt of partially dimerized rosin, con- ...... Coating agent forming to 21 CFR 172.210. Calcium silicate ...... Solid diluent, carrier Calcium stearate ...... Do. Carbon Dioxide (CAS Reg. No. 124–38–9) ...... None ...... Propellant Carrageenan, conforming to 21 CFR 172.620 ...... Minimum molecular weight Thickener (in amu): 100,000. Cetyl alcohol (CAS Reg. No. 36653–82–4) ...... Not more than 5.0% of Evaporation retardant pesticide formulation. Charcoal, activated ...... Meets specifications in the Carrier Food Chemical Codex. Coconut shells ...... Solid diluent and carrier Cod liver oil ...... Solvent, cosolvent Croscarmellose sodium (CAS Reg. No. 74811–65– ...... Disintegrant, solid diluent, carrier, and thick- 7). ener n-Decyl alcohol (CAS Reg. No. 112–30–1) ...... Solvent or co-solvent Dialkyl (C8-C18) dimethyl ammonium chloride ...... Not more than 0.2% in sili- Flocculating agent in the manufacture of silica, hydrated silica. ca, hydrated silica for use as a solid diluent, carrier Diatomite (diatomaceous earth) ...... Solid diluent carrier Diethylaminoethanol, ethoxylated, propoxylated, re- ...... Surfactant action products with fatty acid dimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173188–75–4). Diethylaminoethanol, ethoxylated, propoxylated, re- ...... Surfactant action products with fatty acid trimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173188–83–4). Diethylaminoethanol, ethoxylated, reaction product ...... Surfactant with fatty acid dimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173188–72–1). Diethylaminoethanol, ethoxylated, reaction prod- ...... Surfactant ucts with fatty acid trimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173188–81–2). Diethylene glycol abietate ...... Surfactants, related adjuvants of surfactants 1,1-Difluoroethane (CAS Reg. No. 75–37–6) ...... For aerosol pesticide for- Aerosol propellant mulations used for insect control in food- and feed-handling establishments and animals. 1,2-Dihydro-6-ethoxy-2,2,4-trimethylquinolene ...... Not more than 0.02% of Antioxidant pesticide formulation. Diisopropanolamine (CAS Reg. No. 110–97–4) ...... Not to exceed 10% by Neutralizer or stabilizer weight of pesticide formulation. Diisopropyl adipate (CAS Reg. No. 6938–94–9) .... 40% in mosquito control Solvent, co-solvent. formulations. Dimethyl adipate (CAS no. 627–93–0) ...... None ...... Solvent/co-solvent Dimethylaminoethanol, ethoxylated, propoxylated, ...... Surfactant reaction products with fatty acid dimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173188–42–5). Dimethylaminoethanol, ethoxylated, propoxylated, ...... Surfactant reaction products with fatty acid trimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173188–67–4). Dimethylaminoethanol, ethoxylated, reaction prod- ...... Surfactant ucts with fatty acid dimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173188–38–9). Dimethylaminoethanol, ethoxylated, reaction prod- ...... Surfactant ucts with fatty acid trimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173188–49–2). Dimethyl ether (methane, oxybis-) (CAS Reg. No...... Propellant 115–10–6). Dimethyl glutarate (CAS no. 1119–40–0) ...... None ...... Solvent/co-solvent 3,6-Dimethyl-4-octyn-3,6-diol ...... Not more than 2.5% of Surfactants, related adjuvants of surfactants pesticide formulation.

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Inert ingredients Limits Uses

Dimethyl succinate (CAS no. 106–65–0) ...... None ...... Solvent/co-solvent Di-n-butyl carbonate (CAS Reg. No. 542–52–9) ...... Solvent Dipropylene glycol ...... Solvent, cosolvent Disodium phosphate ...... Anticaking agent, conditioning agent Disodium zinc ethylenediaminetetraacetate ...... Sequestrant dihydride. Distillates, (Fishcher-Tropsch), heavy, C18-C50, ...... Solvent, diluent and/or dust suppressant branched, cyclic and linear (CAS Reg. No. 848301–69–9). Dolomite ...... Solid diluent, carrier Epoxidized linseed oil ...... Surfactants, related adjuvants of surfactants Epoxidized soybean oil ...... Do. Ethanesulfonic acid, 2-hydroxy- (CAS Reg. No...... Chelator, sequestrant, or conditioning agent 107–36–8). Ethanesulfonic acid, 2-hydroxy-, ammonium salts ...... Do. (CAS Reg. No. 57267–78–4). Ethanesulfonic acid, 2-hydroxy-, calcium salts ...... Do. (CAS Reg. No. 10550–47–7). Ethanesulfonic acid, 2-hydroxy-, magnesium salts ...... Do. (CAS Reg. No. 17345–56–1). Ethanesulfonic acid, 2-hydroxy-, potassium salts ...... Do. (CAS Reg. No. 1561–99–5). Ethanesulfonic acid, 2-hydroxy-, sodium salts (CAS ...... Do. Reg. No. 1562–00–1). Ethanesulfonic acid, 2-hydroxy-, zinc salts (CAS ...... Do. Reg. No. 129756–32–7). Ethyl acetate ...... Solvent, cosolvent Ethyl alcohol ...... Do. Ethyl esters of fatty acids derived from edible fats ...... Solvent, cosolvent and oils. Ethyl maltol (CAS Reg. No.4940–11–8) ...... Not more than 0.2 % of Odor masking agent the pesticide formulation. Ethylene glycol (CAS Reg. No. 107–21–1) ...... Without limitation ...... Encapsulating agent for pesticides being applied post-harvest as residual, and crack and crevice sprays in and around food and nonfood areas of residential and nonresi- dential structures, including food handling establishments Ethylene oxide adducts of 2,4,7,9-tetramethyl-5- ...... Surfactants, related adjuvants of surfactants decynediol, the ethylene oxide content averages 3.5, 10 or 30 moles (CAS Reg. No. 9014–85–1). (S,S)-Ethylenediamine disuccinic acid trisodium ...... Sequestrant or chelating agent salt (CAS Reg. No. 178949–82–1). Ethylenediaminetetraacetic acid ...... 3% of pesticide formulation Sequestrant Ethylenediaminetetraacetic acid, tetrasodium salt .. 5% of pesticide formulation Sequestrant 2–Ethyl-1-hexanol (CAS Reg. No. 104–76–7) ...... Not more than 10% of pes- Solvent, adjuvant of surfactants ticide. Fatty acids, conforming to 21 CFR 172.860 ...... Binder, defoaming agent, lubricant FD&C Blue No. 1 ...... Not more than 0.2% of Dye pesticide formulation. FD&C Red No. 40 (CAS Reg. No. 25956–17–6) Not to exceed 0.002% by Dye, coloring agent conforming to 21 CFR 74.340. weight of pesticide formulation. Ferric Citrate (CAS Reg. No. 2338–05–8) ...... Stabilizer Ferric sulfate ...... Solid diluent, carrier Furcelleran ...... Thickener D-Glucitol, 1-deoxy-1-(methyl-amino)-, N-C8-10 acyl Not more than 40% by Surfactant derivatives (CAS Reg. No. 1591782–62–5). weight in pesticide formulation. D-glucopyranose, oligomeric, C10–16-alkyl ...... Surfactant glycosides (CAS Reg. No. 110615–47–9). D-glucopyranose, oligomeric, 6-(dihydrogen cit- ...... Surfactant rates), C8–20 branched and linear alkyl glycosides, sodium salts (CAS Reg. No. 1079993–97–7). D-glucopyranose, oligomeric, 6-(hydrogen ...... Surfactant sulfosuccinates), C8–20 branched and linear alkyl glycosides, sodium salts (CAS Reg. No. 1079993–92–2). D-glucopyranose, oligomeric, lactates, C8–20 ...... Surfactant branched and linear alkyl glycosides (CAS Reg. No. 1079993–94–4).

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Inert ingredients Limits Uses

D-glucurono-6-deoxy-L-manno-D-glucan, acetate, ...... Stabilizer/suspension agent. calcium magnesium potassium sodium salt (diutan gum) (CAS Reg. No. 595585–15–2). Glycerides, edible fats and oils derived from plants ...... Emulsifier, dispersing agent and animals, reaction products with sucrose (CAS Reg. Nos. 100403–38–1, 100403–41–6, 100403–39–2, 100403–40–5). Glycerol mono-, di-, and triacetate ...... Solvent, cosolvent Glyceryl monostearate ...... Emulsifier Granite ...... Do. Graphite ...... Solid diluent, carrier Gum arabic (acacia) ...... Surfactant, suspending agent, dispersing agent Gypsum ...... Solid diluent, carrier Hexamethylenetetramine ...... For use in citrus washing Preservative solutions only at not more than 1%. 3-hexen-1-ol, (3Z)- (CAS Reg. No. 928-96-1) ...... Not more than 0.4% of the Odorant, alerting agent pesticide formulation. n-Hexyl alcohol (CAS Reg. No. 111–27–3) ...... Solvent, cosolvent C9 rich aromatic hydrocarbons (CAS Reg. No...... Solvent 64742–95–6). C10–11 rich aromatic hydrocarbons (CAS Reg. No...... Solvent 64742–94–5). C11–12 rich aromatic hydrocarbons (CAS Reg. No...... Solvent 64742–94–5). Hydrochloric acid ...... Solvent, neutralizer Hydroxyethylmorpholine, ethoxylated, ...... Surfactant propoxylated, reaction products with fatty acid dimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173189– 06–4). Hydroxyethylmorpholine, ethoxylated, ...... Surfactant propoxylated, reaction products with fatty acid trimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173189– 17–7). Hydroxyethylmorpholine, ethoxylated, reaction ...... Surfactant products with fatty acid dimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173189–00–8). Hydroxyethylmorpholine, ethoxylated, reaction ...... Surfactant products with fatty acid trimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173189–09–7). Hydroxyethylpiperidine, ethoxylated, propoxylated, ...... Surfactant reaction products with fatty acid dimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173189–22–4. Hydroxyethylpiperidine, ethoxylated, propoxylated, ...... Surfactant reaction products with fatty acid trimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173189–28–0). Hydroxyethylpiperidine, ethoxylated, reaction prod- ...... Surfactant ucts with fatty acid dimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173189–20–2). Hydroxyethylpiperidine, ethoxylated, reaction prod- ...... Surfactant ucts with fatty acid trimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173189–25–7). Hydroxyethylidine diphosphonic acid (HEDP) (CAS For use in antimicrobial Stabilizer, chelator Reg. No. 2809–21–4). pesticide formulations at not more than 1 percent. Iron oxide ...... Solid diluent, carrier Isobutane (CAS Reg. No. 75–28–5) ...... None ...... Propellant Isopropyl myristate (CAS Reg. No. 110–27–0) ...... Solvent Kaolinite-type clay ...... Solid diluent, carrier Lactic acid ...... Solvent Lactic acid, 2-ethylhexyl ester (CAS Reg. No...... Solvent 6283–86–9). Lactic acid, 2-ethylhexyl ester, (2S)- (CAS Reg...... Solvent No. 186817–80–1).

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Inert ingredients Limits Uses

Lactic acid, n-propyl ester, (S); (CAS Reg. No...... Solvent 53651–69–7). Lauryl alcohol ...... Surfactant Lignin (CAS Reg. No. 9005–53–2) ...... Surfactant, related adjuvants of surfactants Lignin, alkali (CAS Reg. No. 8068–05–1) ...... Do. Lignin, alkali, oxidized, sodium salt (CAS Reg. No...... Do. 68201–23–0). Lignin alkali reaction products with disodium sulfite ...... Do. and formaldehyde (CAS Reg. No. 105859–97–0). Lignin alkali reaction products with formaldehyde ...... Do. and sodium bisulfite (CAS Reg. No. 68512–35– 6). Lignosulfonic acid (CAS Reg. No. 8062–15–5) ...... Do. Lignosulfonic acid, ammonium calcium salt (CAS ...... Do. Reg. No. 12710–04–2). Lignosulfonic acid, ammonium magnesium salt ...... Do. (CAS Reg. No. 123175–37–1). Lignosulfonic acid, ammonium salt (CAS Reg. No...... Do. 8061–53–8). Lignosulfonic acid, ammonium sodium salt (CAS ...... Do. Reg. No. 166798–73–8). Lignosulfonic acid, calcium magnesium salt (CAS ...... Do. Reg. No. 55598–86–2). Lignosulfonic acid, calcium salt (CAS Reg. No...... Do. 8061–52–7). Lignosulfonic acid, calcium sodium salt (CAS Reg...... Do. No. 37325–33–0). Lignosulfonic acid, ethoxylated, sodium salt (CAS ...... Do. Reg. No. 68611–14–3). Lignosulfonic acid, magnesium salt (CAS Reg. No...... Do. 8061–54–9). Lignosulfonic acid, potassium salt (CAS Reg. No...... Do. 37314–65–1). Lignosulfonic acid, sodium salt (CAS Reg. No...... Do. 8061–51–6). Lignosulfonic acid, sodium salt, oxidized (CAS ...... Do. Reg. No. 68855–41–4). Lignosulfonic acid, sodium salt, polymer with form- ...... Do. aldehyde and phenol (CAS Reg. No. 37207–89– 9). Lignosulfonic acid, sodium salt, sulfomethylated ...... Do. (CAS Reg. No. 68512–34–5). Lignosulfonic acid, zinc salt (CAS Reg. No. 57866– ...... Do. 49–6). d-Limonene (CAS Reg. No. 5989–27–5) ...... Solvent, fragrance Magnesium carbonate ...... Anticaking agent, conditioning agent Magnesium chloride ...... Safener Magnesium lime ...... Solid diluent, carrier Magnesium oxide ...... Do. Magnesium silicate ...... Do. Magnesium stearate ...... Surfactant Magnesium sulfate ...... Solid diluent, carrier, safener Methyl alcohol ...... Solvent Methyl n-amyl ketone (CAS Reg. No. 110–43–0) ...... Solvent, cosolvent Methyl 5-(dimethylamino)-2-methyl-5- ...... Solvent oxopentanoate (1174627–68–9). Methyl esters of fatty acids derived from edible fats ...... Solvent, cosolvent and oils. Methyl esters of higher fatty acids conforming to ...... Antidusting agent, surfactant 21 CFR 573.640. Methyl isobutyl ketone ...... Solvent 2-methyl-2,4-pentanediol (CAS Reg. No. 107–41– Without limitation ...... Growing crops and food animals 5). 2-methyl-1,3-propanediol (CAS Reg. No. 2163–42– ...... Solvent, surfactant 0). Methylated silicones ...... Antifoaming agent Mono-, di-, and trimethylnapthalenesulfonic acids ...... Surfactants, related adjuvants of surfactants and napthalenesulfonic acids formaldehyde condensates, ammonium and sodium salts (CAS Reg. Nos 9008–63–3, 9069–80–1, 9084–06–4, 36290–04–7, 91078–68–1, 141959–43–5, 68425–94–5). Mica ...... Solid diluent, carrier

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Inert ingredients Limits Uses

Mineral oil, U.S.P., or conforming to 21 CFR ...... Diluent, carrier, and solvent 172.878 or 178.3620(a) (CAS Reg. No. 8012– 95–1). Monoammonium phosphate ...... No more than 3.75% by Postharvest fumigation in formulation with weight in formulation. aluminum phosphide

Mono- and diglycerides of C 8-C18 fatty acids ...... Surfactants, related adjuvants of surfactants Montmorillonite-type clay ...... Solid diluent, carrier Nonyl, decyl, and undecyl glycoside mixture with a ...... Surfactant. mixture of nonyl, decyl, and undecyl oligosaccharides and related reaction products (primarily decanol and undecanol) produced as an aqueous-based liquid (50 to 65% solids) from the reaction of primary alcohols (containing 15 to 20% secondary alcohol isomers) in a ratio of 20% C9, 40% C10, and 40% C11 with carbohydrates (average glucose to alkyl chain ratio 1.3 to 1.8). a-(p-Nonylphenol)-w-hydroxypoly(oxyethylene) mix- Not to exceed 7% of pes- Surfactants, related adjuvants of surfactants ture of dihydrogen phosphate and ticide formulation. monohydrogen phosphate esters and the corresponding ammonium, calcium, magnesium, potassium, sodium, and zinc salts of the phosphate esters; the nonyl group is a propylene trimer isomer and the poly(oxyethylene) content averages 4–14 or 30 moles (CAS Reg. Nos. 51811–79–1, 59139–23–0, 67922–57–0, 68412– 53–3, 68553–97–9, 68954–84–7, 99821–14–4, 152143–22–1, 51609–41–7, 37340–60–6, 106151–63–7, 68584–47–4, 52503–15–8, 68458–49–1). a-(p-Nonylphenyl)-w-hydroxypoly(oxyethylene) pro- ...... Surfactants, related adjuvants of surfactants duced by the condensation of 1 mole of nonylphenol (nonyl group is a propylene trimer isomer) with an average of 4-14 or 30-90 moles of ethylene oxide; if a blend of products is used, the average number of moles of ethylene oxide reacted to produce any product that is a component of the blend shall be in the range of 4-14 or 30-90. a-(p-Nonylphenol)-w-hydroxypoly(oxyethylene) sul- Not to exceed 7% of pes- Surfactants, related adjuvants of surfactants fate, ammonium, calcium, magnesium, potas- ticide formulation. sium, sodium, and zinc salts the nonyl group is propylene trimer isomer and the poly(oxyethylene) content averages 4 moles (CAS Reg. Nos. 9014–90–8, 9051–57–4, 9081– 17–8, 68649–55–8, 68891–33–8. 1-Octanal (CAS Reg. No. 124–13–0) ...... Not more than 0.2% of the Odor masking agent pesticide formulation. n-Octyl alcohol (CAS Reg. No. 111–87–5) ...... Solvent or co-solvent Octyl and decyl glucosides mixture with a mixture ...... Surfactants, related adjuvants of surfactants of octyl and decyloligosaccharides and related reaction products (primarily n- decanol) produced as an aqueous-based liquid (68-72% solids) from the reaction of straight chain alcohols (C8(45%), C10 (55%)) with anhydrous glucose. Oleic acid ...... Diluent Oleic acid diester of a-hydro-w-hydroxypoly (oxy- ...... Surfactants, related adjuvants of surfactants ethylene); the poly(oxyethylene) having average molecular weight (in amu) 400. a-Oleoyl-w-hydroxypoly(oxyethylene), average mo- ...... Emulsifier lecular weight (in amu) of 600. Oleyl alcohol (CAS Reg. No. 143–28–2 ...... 15% ...... Cosolvent Oxalic acid ...... No more oxalic acid should Calcium chelating hard water inhibitor be used than is necessary to chelate calcium and in no case should more than 2 lb oxalic acid per acre be used. Palmitic acid ...... Diluent Pentaerythritol ester of maleic anhydride modified ...... Plasticizer wood rosin.

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Inert ingredients Limits Uses

Pentaerythritol tetrakis (3-(3,5-di-tert-butyl-4- Not to exceed 5% by Antioxidant, stabilizer hydroxyphenyl)propionate) (CAS Reg. No. 6683– weight of the pesticide 19–8). formulation. Petrolatum, conforming to 21 CFR 172.880 ...... Coating agent Petroleum hydrocarbons, light odorless conforming ...... Solvent, diluent. to 21 CFR 172.884. Petroleum hydrocarbons, synthetic isoparaffinic, ...... Do. conforming to 21 CFR 172.882. Petroleum naphtha, conforming to 21 CFR ...... Component of coating agent 172.250(d). Petroleum wax, conforming to 21 CFR 172.886(d) ...... Coating agent Phosphoric acid ...... Buffer Polyethylene, conforming to 21 CFR 177.1520(c) ...... Binder, carrier, and coating agent Polyethylene glycol[a-hydro-w- ...... Surfactants, related adjuvants of surfactants hydroxypoly(oxyethylene)]; mean molecular weight (in amu) 194 to 9,500 conforms to 21 CFR 178.3750. Polyglycerol esters of fatty acids conforming to 21 ...... Surfactants, related adjuvants of surfactants CFR 172.854. Polyglyceryl phthalate ester of coconut oil fatty None ...... Surfactants, related adjuvants of surfactants acids, including fatty acid coco polymers with glyceryl and phthalic anhydride (CAS No. 67746–02–5) and coconut oil polymer with glyceryl and phthalic anhydride (CAS No. 66070– 87–9). Poly(oxy-1,2-ethanediyl), a-(carboxymethyl)-w- ...... Surfactant (nonylphenoxy) produced by the condensation of 1 mole of nonylphenol (nonyl group is a propylene trimer isomer) with an average of 4-14 or 30-90 moles of ethylene oxide. The molecular weight (in amu) ranges are 454-894 and 1598- 4238. Poly(oxy-1,2-ethanediyl), a-[tris(1- For use in post-harvest ap- Surfactants phenylethyl)phenyl]-w-hydroxy-, (CAS Reg. No. plications; not to exceed 99734–09–5). 15% by weight in pesticide formulations. Poly(oxy-1,2-ethanediyl), a-(3-carboxy-1- Not to exceed 10% by Surfactant oxosulfopropyl)-w-hydroxy-, C10-12-alkyl ethers, weight of pesticide for- disodium salts, the poly(oxyethylene) content mulation. averages 5–15 moles (CAS Reg. No. 68954– 91–6). Poly(oxy-1,2-ethanediyl), a-(3-carboxy-1- Not to exceed 10% by Surfactant oxosulfopropyl)-w-hydroxy-, C10-16-alkyl ethers, weight of pesticide for- disodium salts, the poly(oxyethylene) content mulation. averages 5–15 moles (CAS Reg, No. 68815– 56–5). Poly(oxy-1,2-ethanediyl), a-(3-carboxy-1- Not to exceed 10% by Surfactant oxosulfopropyl)-w-hydroxy-, C12-14-alkyl ethers, weight of pesticide for- disodium salts, the poly(oxyethylene) content mulation. averages 5–15 moles (CAS Reg. No. 1024612– 24–5). Poly(oxy-1,2-ethanediyl), a-(3-carboxy-1- Not to exceed 10% by Surfactant oxosulfopropyl)-w-(isotridecyloxy)-, sodium salt weight of pesticide for- (1:2), the poly(oxyethylene) content averages 5– mulation. 15 moles (CAS Reg. No. 1013906–64–3). Polyoxyethylene (20) sorbitan monostearate ...... Surfactants, related adjuvants of surfactants [Poly[oxy(methyl-1,2-ethanediyl)], a-[2-bis(2-hy- Not to exceed 15% in the Surfactant droxyethyl)amino]propyl]-w-hydroxy,-ether with formulated product; only a-hydro-w-hydroxypoly(oxy-1,2-ethanediyl) (1:2), for use with glyphosate. mono-C12–16 alkyl ethers, (CAS Reg. No. 176022–82–5). Polysorbate 65, conforming to 21 CFR 172.838 ...... Emulsifier Potassium aluminum silicate ...... Solid diluent, carrier Potassium benzoate (Cas No. 582–25–2) ...... None ...... Preservative Potassium hydroxide ...... Neutralizer Potassium phosphate ...... Buffer Potassium sulfate ...... Solid diluent Propanamide, 2-hydroxy-N, N-dimethyl- (CAS Reg. Not to exceed 20% by Solvent/co-solvent No. 35123–06–9). weight in pesticide formulation. Propane ...... Propellant 1,3-Propanediol (CAS Reg. No. 504–63–2) ...... Solvent, co-solvent, diluent, or freeze-point depressant

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Inert ingredients Limits Uses

Propanoic acid, 2-methyl-, monoester with 2,2,4- ...... Solvent, co-solvent trimethyl-1,3-pentanediol (CAS Reg. No. 25265– 77–4). 2-Propanol, 1,1′,1″-nitrilotris- (CAS No. 122–20–3) Without limitation ...... Neutralizer n-Propanol ...... Solvent, cosolvent 2-Propenoic acid, 2-methyl-, polymer with ethyl 2- ...... Encapsulating agent, dispensers, resins, fi- propenoate and methyl 2-methyl-2-propenoate, bers and beads ammonium salt (CAS Registration No. 55989– 05–4), minimum number average molecular weight (in amu), 18,900.. Propyl gallate ...... Antioxidant Propyl p-hydroxybenzoate ...... Preservative for formulations Propylene glycol ...... Solvent, cosolvent. Propylene glycol alginate (as defined in 21 CFR ...... Defoaming agent 172.858). Propylene glycol monomethyl ether (CAS No. 107– none ...... solvent 98–2). Pyrophyllite ...... Solid diluent, carrier Rhizobium inoculants (e.g. Sinorhizobium, ...... All leguminous food commodities Bradyrhizobium & Rhizobium). Rosin, partially dimerized (as defined in 21 CFR ...... Surfactants, related adjuvants of surfactants 172.615). Rosin, partially hydrogenated (as defined in 21 ...... Do. CFR 172.615). Rosin, wood ...... Do. Salicylaldehyde (CAS Reg. No. 90–02–8) ...... Not to exceed 14% by Penetration aid weight of pesticide formulation. Salts of fatty acids, conforming to 21 CFR 172.863 ...... Binder, emulsifier, anticaking agent Sand ...... Solid diluent, carrier Shellac, bleached; refined, food grade, arsenic and ...... Coating agent rosin-free. Silver nitrate (Cas Reg. No. 7761–88–8) ...... For use on potatoes as Stabilizer post-harvest treatment to control sprouting at no more than 0.06% by weight in pesticide formulations. Soapstone ...... Solid diluent Sodium acid pyrophosphate ...... Surfactant, suspending agent, dispersing agent, buffer Sodium alkyl naphthalenesulfonates (CAS Reg. Limited to no more than Surfactants, related adjuvants of surfactants Nos. 68909–83–1, 68909–84–2, 68909–82–0, 30% by weight in pes- 27213–90–7, 26264–58–4, 27178–87–6, ticide end-use products. 111163–74–7, 908356–16–1, 25417–20–3, 25638–17–9, 145578–88–7, 1322–93–6, 1323– 19–9, 7403–47–6, 68442–09–1, 127646–44–0, 908356–18–3). Sodium aluminum silicate ...... Solid diluent, carrier Sodium dioctylsulfosuccinate ...... Surfactants, related adjuvants of surfactants Sodium 1,4-dihexyl sulfosuccinate (CAS Reg. No...... Surfactants, related adjuvants of surfactants 3006–15–3). Sodium 1,4-diisobutyl sulfosuccinate (CAS Reg...... Surfactants, related adjuvants of surfactants No. 127–39–9). Sodium 1,4-dipentyl sulfosuccinate (CAS Reg. No...... Surfactants, related adjuvants of surfactants 922–80–5). Sodium DL-lactate (CAS Reg. No. 72–17–3) ...... Surfactant Sodium hexametaphosphate...... Surfactant, emulsifier, wetting agent, suspending agent, dispersing agent, buffer Sodium hydroxide ...... Neutralizer Sodium L-lactate (CAS Reg. No. 867–56–1) ...... Surfactant Sodium metasilicate ...... Surfactants, emulsifiers, wetting agents, dispersing agents, buffer Sodium monoalkyl and dialkyl (C6-C16) phenoxy Not to exceed 20% in pes- Surfactants, related adjuvants of surfactants benzenedisulfonates and related acids (CAS ticide formulations. Reg. Nos. 147732–59–0, 147732–60–3, 169662–22–0, 70191–75–2, 36445–71–3, 39354–74–0, 70146–13–3, 119345–03–8, 149119–20–0, 149119–19–7, 119345–04–9, 28519–02–0, 25167–32–2, 30260–73–2, 65143– 89–7, 70191–76–3). Sodium a-olefinsulfonate (sodium C14-C16) (Olefin ...... Surfactants, related adjuvants of surfactants sulfonate).

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Inert ingredients Limits Uses

SodiumN-oleoyl- N-methyl taurine (CAS Reg. No...... Surfactants, related adjuvants of surfactants 137–20–2).

Sodium and potassium salts of N-alkyl (C8–C18)- Concentration in formu- Surfactants, related adjuvants of surfactants beta-iminodipropionic acid where the C8–C18 is lated end-use products linear and may be saturated and/or unsaturated not to exceed 30% by (CAS Reg. Nos. 110676–19–2, 3655–00–3, weight in pesticide for- 61791–56–8, 14960–06–6, 26256–79–1, 90170– mulations. 43–7, 91696–17–2, 97862–48–1). Sodium salt of sulfated oleic acid ...... Surfactants, related adjuvants of surfactants Sodium silicate ...... Surfactant, emulsifier, wetting agent, stabilizer, inhibitor Sodium starch glycolate (CAS Reg. No. 9063–38– Granular and tableted Disintegrant 1). products only; not to exceed 8% of the formulated product. Sodium sulfate ...... Solid diluent, carrier Sodium tripolyphosphate ...... Buffer, surfactant, suspending agent, dispersing agent, anticaking agent, conditioning agent Sorbic acid (CAS Reg. No. 110–44–1) ...... Preservative for formulations

Sorbitan fatty acid esters (fatty acids limited to C12, ...... Surfactants, related adjuvants or surfactants. C14, C16, and C18 containing minor amounts of associated fatty acids) and their derivatives; the poly(oxyethylene) content averages 5-20 moles. Soybean flour ...... Expires May 24, 2005...... Surfactant Soybean oil-derived fatty acids ...... Solvent, cosolvent Stearic acid ...... Diluent a-Stearoyl-w-hydroxypoly(oxyethylene), average ...... Emulsifier molecular weight (in amu) of 600. a-Stearoyl-w-hydroxypoly(oxyethylene); the ...... Surfactants, related adjuvants of surfactants poly(oxyethylene) content averages either 8, 9, or 40 moles; if a blend of products is used, the average number of moles ethylene oxide reacted to produce any product that is a component of the blend shall be either 8, 9, or 40. Sucrose octaacetate ...... Adhesive Sulfite liquors and cooking liquors, spent, oxidized ...... Surfactant, related adjuvants of surfactants (CAS Reg. No. 68514–09–0). Sulfuric acid (CAS Reg. No.7664–93–9) ...... Not to exceed 10% of the pH Control agent pesticide formulation; non-aerosol formulations only. Sweet orange peel tincture (CAS Reg. No. 8028– Not to exceed 10% Surfactant, fragrance, related adjuvants of 48–6). (weight/weight) in pes- surfactants ticide formulation. Synthetic paraffin and its succinic derivatives con- ...... Carrier, binder, and carrying agent forming to 21 CFR 172.275. Synthetic petroleum wax, conforming to 21 CFR ...... Binder, carrier, and coating agent 172.888. Talc ...... Solid diluent, carriers Tall oil; fatty acids not less than 58%, rosin acids ...... Surfactants, related adjuvants of surfactants not more than 44%, unsaponifiables not more than 8%. Tartrazine ...... Dye Terpenes and terpenoids, turpentine oil, alpha-pi- ...... Surfactants, related adjuvants of surfactants nene fraction, polymd. (CAS Reg. No. 70750– 57–1). 1,1,1,2-Tetrafluoroethane, (CAS Reg. No. 811–97– ...... Aerosol propellant 2). Trans-1,3,3,3-tetrafluoroprop-1-ene (CAS Reg. No...... Propellant 29118–24–9). Tetrahydrofurfuryl alcohol (THFA) (CAS Reg. No Expires February 9, 2008 Solvent/cosolvent 97–99–4). N,N,N′,N″,-tetrakis-(2-hydroxypropyl) ethylene- Concentration in formu- Stabilizer for formulation. diamine (CAS Reg. No. 102–60–3). lated end-use products not to exceed 20% by weight in pesticide formulations.

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Inert ingredients Limits Uses

a-[p-(1,1,3,3-tetramethylbutyl)phenyl]-w- Not to exceed 7% of pes- Surfactants related adjuvants of surfactants hydroxypoly(oxyethylene) produced by the con- ticide formulation. densation of 1 mole of p-(1,1,3,3- tetramethylbutyl)phenol with a range of 1–14 or 30–70 moles of ethylene oxide: If a blend of products is used, the average range number of moles of ethylene oxide reacted to produce any product that is a component of the blend shall be in the range of 1–14 or 30–70 (CAS Reg. Nos. 9036–19–5, 9002–93–1). 2,4,7,9-Tetramethyl-5-decyn-4, 7-diol ...... Not more than 2.5% of Surfactants, related adjuvants of surfactants pesticide formulation. Tetrasodium pyrophosphate ...... Anticaking agent, conditioning agent Thiosulfuric acid, disodium salt, anhydrous. (CAS ...... Dechlorinator, reducing agent Reg. No 7772–98–7). Thiosulfuric acid, disodium salt, pentahydrate...... Do. (CAS Reg. No. 10102–17–7). d-Alpha tocopherol (CAS Reg. No. 9–02–9 ...... None ...... Safener d-Alpha tocopheryl acetate (CAS Reg. No. 58–95– None ...... Do. 7). dl-Alpha tocopherol (CAS Reg. No.10191–41–0) ... None ...... Do. dl-Alpha tocopheryl acetate (CAS Reg. No. 7695– None ...... Do. 91–2). Tricalcium phosphate ...... Surfactant, suspending agent, dispersing agent, anticaking agent, conditioning agent Trisodium phosphate ...... Surfactant, emulsifier, wetting agent Vermiculite ...... Solid diluent, carrier. Vitamin E (CAS Reg. No. 1406–18–4) ...... None ...... Safener Walnut shells ...... Leaching inhibitor, binder for water-dispers- ible aggregates, sticker and suspension stabilizer Wintergreen oil ...... Attractant Wood flour ...... Derived from wood free of Solid diluent and carrier chemical preservatives. Xanthan gum-modified, produced by the reaction Not more than 0.5% of Surfactant of xanthan gum and glyoxal (maximum 0.3% by pesticide formulation. weight). Xylene meeting the specifications listed in 21 CFR In pesticide formulations Solvent, cosolvent 172.884(b)(4). for grain storage only. Zeolite (hydrated alkali aluminum silicate) ...... Solid diluent, carrier Zinc oxide ...... Coating agent Zinc sulfate (basic and monohydrate) ...... Do. Zinc sulfate (basic and monohydrate) ...... Solid diluent, carrier

[69 FR 23117, Apr. 28, 2004]

EDITORIAL NOTE: For FEDERAL REGISTER citations affecting § 180.910, see the List of CFR Sections Affected, which appears in the Finding Aids section of the printed volume and at www.fdsys.gov.

§ 180.920 Inert ingredients used pre- when used in accordance with good ag- harvest; exemptions from the re- ricultural practice as inert (or occa- quirement of a tolerance. sionally active) ingredients in pesticide The following materials are exempt- formulations applied to growing crops ed from the requirement of a tolerance only:

Inert ingredients Limits Uses

Acetophenone ...... Attractant Adenosine (CAS Reg. No. 58–61–7) ...... Maximum of 0.5% of formu- Synergist lation. Alder bark ...... Seed germination stimulator

Alkyl (C12-C16) dimethyl ammonio acetate (CAS 20% by weight in pesticide Surfactant Reg. Nos. 683–10–3, 2601–33–4 and 693– formulation. 33–4.

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Inert ingredients Limits Uses

a-Alkyl (minimum C6 linear, branched, saturated Not to exceed 30% of pes- Surfactants, related adjuvants of surfactants and/or unsaturated)-w-hydroxypolyoxyethylene ticide formulation. polymer with or without polyoxypropylene, mixture of di- and monohydrogen phosphate esters and the corresponding ammonium, calcium, magnesium, monoethanolamine, potassium, sodium, and zinc salts of the phosphate esters; minimum oxyethylene content is 2 moles; minimum oxypropylene content is 0 moles (CAS Reg. Nos. 9046–01–9, 37280– 82–3, 39464–66–9, 42612–52–2, 50643–20– 4, 52019–36–0, 58318–92–6, 60267–55–2, 61837–79–4, 67711–84–6, 68070–99–5, 68071–35–2, 68071–17–0, 68130–47–2, 68186–37–8, 68186–36–7, 68311–02–4, 68425–73–0, 68458–48–0, 68511–37–5, 68610–65–1, 68585–36–4, 68649–29–6, 68815–11–2, 68908–64–5, 68891–13–4, 73038–25–2, 78330–24–2, 108818–88–8, 154518–39–5, 317833–96–8, 873662–29–4, 936100–29–7, 936100–30–0).

N-alkyl(C8-C18) dimethylamidopropylamines Not to exceed 20% by Surfactants, related adjuvants of surfactants where the alkyl group is linear and may be weight in herbicide formu- saturated and/or unsaturated (CAS Reg. Nos. lations. 109–28–4, 3179–80–4, 7651–02–7, 22890– 10–4, 22890–11–5, 39669–97–1, 45267–19– 4, 68140–01–2, 1147459–12–8, 146987–98– 6).

N-alkyl (C8-C18) primary amines and their ace- Concentration in formulated Surfactants, related adjuvants of surfactants tate salts where the alkyl group is linear and end-use products not to may be saturated and/or unsaturated (CAS exceed 10% by weight in Reg. Nos. 61790–57–6, 61790–58–7, 61790– herbicide products, 4% 59–8, 61790–60–1, 61788–46–3, 61790–33– by weight in insecticide 8, 68155–38–4). products, and 4% by weight in fungicide products. N,N-Bis-a-ethyl-w-hydroxypoly(oxy-1,2- Not to exceed 25% in herbi- Surfactants, related adjuvants of surfactants ethanediyl) C8–C18 saturated and unsatu- cide formulations and rated alkylamines; the poly(oxy-1,2-ethanediyl) 10% in insecticide and content is 2–60 moles (CAS Reg. Nos. fungicide formulations. 10213–78–2, 25307–17–9, 26635–92–7, 26635–93–8, 288259–52–9, 58253–49–9, 61790–82–7, 61791–14–8, 61791–24–0, 61791–26–2, 61791–31–9, 61791–44–4, 68155–33–9, 68155–39–5, 68155–40– 8,70955–14–5, 73246–96–5, 1266162–49–5). N,N–Bis-a-ethyl-w-hydroxypoly(oxy-1,2- Not to exceed 25% in herbi- Surfactants, related adjuvants of surfactants ethanediyl/oxy(methyl-1,2-ethanediyl) C8-C18 cide formulations and saturated and unsaturated alkylamines; the 10% in insecticide and poly(oxy-1,2-ethanediyl/oxy(methyl-1,2- fungicide formulations. ethanediyl) content is 2–60 moles (CAS Reg. Nos. 68213–26–3, 68153–97–9, 75601–76–2). Aluminum sulfate ...... Safener adjuvant Ammonium acetate (CAS No. 631–61–8) ...... 15% ...... Buffering Agent. Ammonium chloride (CAS Reg. No. 12125–02– ...... Carrier/nutrient 9). Ammonium formate (CAS Reg. No. 540–69–2) ...... Complexing or fixing agent Ammonium nitrate (CAS Reg. No. 6484–52–2) ...... Adjuvant/ intensifier for herbicides Ammonium polyphosphate (CAS Reg. No...... Sequestrant, buffer, or surfactant 68333–79–9). Barium sulfate ...... Carrier Quaternary ammonium compounds, Not to exceed 1.0% by Suspending or structuring agent benzylbis(hydrogenated tallow alkyl)methyl, weight of pesticide formu- bis(hydrogenated tallow alkyl)di- lation. methylammonium salts with saponite (CAS Reg. No. 1588523–05–0). Quaternary ammonium compounds, Not to exceed 2.0% by Suspending or structuring agent benzylbis(hydrogenated tallow alkyl)methyl, weight of pesticide formu- bis(hydrogenated tallow alkyl)di- lation, asbestos free and methylammonium salts with sepiolite (CAS containing less than 1% Reg. No. 1574487–61–8). crystalline silica.

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Inert ingredients Limits Uses

1,4-Benzenedicarboxylic acid, dimethyl ester, For use in honeybee hive Component of controlled release agent polymer with 1,4-butanediol, adipic acid, and miticide formulations. hexamethylene diisocyanate, minimum number average molecular weight (in amu) 30,000 (CAS Reg. No. 55231–08–8). 1,2-Benzisothiazolin-3-one ...... Not more than 0.1% of for- Preservative/stabilizer mulation. Not more than 0.02 lb to be applied per acre. Benzyl acetate (CAS Reg. No. 140–11–4) ...... Solvent Boric acid ...... Sequestrant Buffalo gourd root powder (Cucurbita No more than 2.5 lbs/acre/ Gustatory stimulant foetidissima root powder); or, Zucchini juice season (3.4 gm/acre/sea- (Cucurbita pepo juice) or Hawkesbury melon son of Cucurbitacin). Citrullus lanatus.. Butyl stearate ...... Defoamer g-Butyrolactone ...... Solvent C.I. Pigment Blue #15 (CAS Reg. No. 147–14– For seed treament use only Dye, coloring agent 8; containing no more than 50 ppm poly- chlorinated biphenyls (PCBs)). C.I. Pigment Green #7 (CAS Reg. No. 1328– For seed treatment use Dye, coloring agent 53–6; containing no more than 50 ppm poly- only. chlorinated biphenyls (PCBs)). C.I. Pigment Red #112 (CAS Reg. No. 6535– Seed treatment use only. Coloring agent 46–2). Limited to 10% w/w of pesticide formulation. C.I. Pigment Violet #23 (CAS Reg. No. 6358– For seed treatment use Dye, coloring agent 30–1; containing no more than 20 ppb of poly- only. chlorinated dibenzo-p-dioxins and/or poly- chlorinated dibenzofurans). C.I. Pigment Yellow 1 (CAS Reg. No. 2512–29– Not to exceed 10% (weight/ Colorant 0). weight) in pesticide formulation. Calcium gluconate (CAS Reg. No. 299–28–5) ...... Sequestrant Camphor (CAS Reg. No. 76–22–2) ...... Not more than 5% weight to Deodorant, melting point adjustment weight (w/w) of pesticide formulations. Carbon Black (CAS Reg. No. 1333–86–4) ...... For seed treatment use Colorant only. Carbonic acid, dipotassium salt (CAS Reg. No...... Buffering agent 584–08–7). Carbonic acid, dipotassium salt, trihydrate (CAS ...... Buffering agent Reg. No. 18662–52–7). Carboxymethyl guar gum sodium salt (CAS Without limitation ...... Thicker/drift reduction agent Reg. No. 39346–76–4). Carboxymethyl-hydroxypropyl guar (CAS Reg. Without limitation ...... Thicker/drift reduction agent No. 68130–15–4). Carous chloride ...... 10 ppm in formulation ...... Tagging agent Carrageenan, conforming to 21 CFR 172.260 .... Not more than 0.15% of Thickener and stabilizer for pesticide formula- pesticide formulation. tions applied to seeds before planting Chlorobenzene ...... Contains not more than 1% Solvent, cosolvent impurities. Not for use after edible parts of plant begin to form. Do not graze livestock in treated areas within 48 hours after application. 5-Chloro-2-methyl-4-isothiazolin-3-one (in com- Not more than 0.0022% Preservative bination with 2-methyl-4-isothiazolin-3-one). (22.5 ppm) in the formulation; 0.00022% (or 2.25 ppm) in the final solution applied to growing crops. Choline chloride (CAS Reg. No. 67–48–1) ...... As a solvent Choline hydroxide (CAS Reg No. 123–41–1) ..... Without limitation ...... Neutralizer Cis-isomer of 1-(3-chloroallyl)-3,5,7-triaza-1- Maximum of 0.14% by Preservative azoniaadamantane chloride (CAS Reg. No. weight of formulation. 51229–78–8). Coco alkyl dimethyl amines (CAS Reg. No. Not to exceed 0.5% in pes- Emulsifier 61788–93–0). ticide formulation. Copper naphthenate ...... Not more than 2.5% of for- Mercaptan scavenger in technical pesticide mulation; application limited to before edible por- tions of plants begin to form.

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Inert ingredients Limits Uses

Cyclohexane ...... Solvent, cosolvent Cyclohexanone ...... Do. Cysteine (CAS Reg. No. 52–90–4) ...... Maximum of 0.5% of formu- Synergist lation. D&C Green No. 6 ...... Dye D&C Red No. 17, technical grade ...... Dye D&C Red No. 33 (CAS Reg. No. 3567–66–6); ...... Dye meeting the specifications listed in 21 CFR 74.1333. D&C Violet No. 2, technical grade ...... Not more than 0.005% of Dye pesticide formulation. Decanamide, N,N-dimethyl (CAS Reg. No...... Emulsifier, solvent, cosolvent 14433–76–2). Diammonium phosphate (CAS Reg. No. 7783– ...... Buffer, surfactant 28–0). dibenzylidene sorbitol (32647–67–9) ...... Thinning agent Diethanolamine ...... Stabilizer, inhibitor for formulations used before crop emerges from soil

Diethanolamine salts of alkyl (C8-C24) Not to exceed 7% of pes- Surfactants, related adjuvants of surfactants. benzenesulfonic acid (CAS Reg. Nos. 26545– ticide formulation. 53–9, 67815–95–6, 67889–94–5, 67889–95– 6, 68259–34–7, 68478–47–7, 68567–68–0, 68815–34–9, 68815–37–2, 68891–02–1, 68953–97–9, 84989–15–1, 85338–09–6, 90194–39–1, 90194–40–4, 90218–08–9). Diethylene glycol ...... Deactivator, adjuvant for formulations used before crop emerges from soil Diethylene Glycol (CAS No. 111–46–6) ...... Without limitation ...... Solvent, stabilizer and/or antifreeze Diethylene glycol and diethylene glycol ...... Deactivator for formulations used before crop monobutyl, monoethyl, and monomethyl emerges from soil, stabilizer ethers. Diethylene glycol mono butyl ether (CAS Reg. Without limitation ...... Pesticide inert ingredient as a solvent, sta- No. 112–34–5). bilizer and/or antifreeze Diethylene Glycol MonoEthyl Ether (CAS Reg. Without limitation ...... Solvent, stabilizer and/or antifreeze No. 111–90–0). Dimethylaminopropylamine, isopropylamine, eth- ...... Surfactants, related adjuvants of surfactants. anolamine, and triethanolamine salts of alkyl (C8-C24) benzenesulfonic acid (CAS Reg. Nos. 3088–30–0, 12068–12–1, 26264–05–1, 26836–07–7, 27323–41–7, 55470–69–4, 58089–99–9, 61886–59–7, 61931–76–8, 67924–05–4, 68110–32–7, 68259–35–8, 68411–31–4, 68442–72–8, 68567–69–1, 68584–24–7, 68584–25–8, 68648–81–7, 68648–96–4, 68649–00–3, 68815–30–5, 68815–35–0, 68910–32–7, 68953–93–5, 68953–98–0, 70528–84–6, 72391–21–0, 84961–74–0, 85480–55–3, 85480–56–4, 85995–82–0, 90194–42–6, 90194–53–9, 90194–54–0, 90194–55–1, 90218–09–0, 90218–11–4, 90218–35–2, 96687–54–6, 99924–49–9, 121617–08–1, 157966–96–6, 193562–36–6, 319926–68–6, 877677–48–0, 1093628–27–3). 3,6-Dimethyl-4-octyn-3,6-diol ...... In pesticide formulations, Surfactants, related adjuvants of surfactants for soil prior to planting or to plants before edible parts form. Dimethyl sulfoxide ...... Solvent or cosolvent for formulations used before crop emerges from soil or prior to formation of edible parts of food plants

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Inert ingredients Limits Uses

Dimethyl sulfoxide (CAS No. 67–68–5) ...... For pesticide formulations Solvent or co-solvent used before crop emerges from soil or prior to formation of edible parts of food plants; for pesticide formulations used after crop emerges but before harvest, provided that the potential for increased residues of the formulation’s active ingredient(s) in or on food commodities has been assessed. Dipotassium hydrogen phosphate ...... Buffering agent Dipropylene glycol monomethyl ether ...... Stabilizer Douglas-fir bark, ground ...... Solid diluent, carrier Dysprosium chloride ...... 10 ppm in formulation ...... Tagging agent 1,2-ethanediamine,N,N,N″, N″-tetramethyl-, poly- For use in pesticide formu- Adjuvant or water conditioner mer with 1,1′-oxybis[2-chloroethane] (CAS lations applied to cotton Reg. No. 31075–24–8). or wheat only. (S,S)–Ethylenediaminedisuccinic acid (CAS ...... Sequestrant or chelating agent Reg. No. 20846–91–7). Ethylene glycol ...... Antifreeze, deactivator for all pesticides used before crop emerges from soil and in herbicides before or after crop emerges Ethylene glycol (CAS Reg. No. 107–21–1) ...... Without limitation ...... Pesticide inert ingredient as a solvent, stabilizer and/or antifreeze. Ethylene glycol monobutyl ether ...... 2-Ethylhexanol ...... Cosolvent, defoamer, solvent for all pesticides used before crop emerges from soil and in herbicides before or after crop emerges Europic chloride ...... 10 ppm in formulation ...... Tagging agent FD&C Blue No. 1 (CAS Reg. No. 3844–45–9) ... For seed treatment use Dye, coloring agent only. FD&C Blue No. 1, methyl-polyethylene glycol For seed treatment use Dye, coloring agent derivative (CAS Reg. No. 9079–34–9). only; Number average molecular weight (in amu) is greater than 1,000; Not to exceed 5% of the formulated pesticide product. FD&C Blue No. 1, polyethylene glycol derivative For seed treatment use Dye, coloring agent (CAS Reg. No. 9079–33–8). only; Number average molecular weight (in amu) is greater than 1,000; Not to exceed 5% of the formulated pesticide product. FD&C Red No. 40 (CAS Reg. No. 25956–17–6) For seed treatment use Dye, coloring agent only. Not to exceed 2% by weight of the pesticide formulation. Ferric chloride ...... Not greater than 2% of suspending, dispersing agent, pesticide formulation Fluoroapatite ...... Solid diluent, carrier Folic acid (CAS Reg. No. 59–30–3) ...... Maximum of 0.5% of formu- Synergist lation. Gluconic acid (and sodium salt) ...... Sequestrant l-Glutamic acid (C5 H9 NO4´ CAS Reg. No. 56– Seet treatment use only ..... Plant nutrient 86–0). [alpha]-D-glucopyranoside, 2-ethylhexyl 6-O- ...... Surfactant [alpha]-D glucopyranosyl- (CAS Reg. No. 330980–61–5). [alpha]-D-glucopyranoside, 2-ethylhexyl (CAS ...... Surfactant Reg. No. 125590–73–0). Glutamine (CAS Reg. No. 56–85–9) ...... Maximum of 0.5% of formu- Synergist lation. Glycerol—propylene oxide polymer (CAS Reg...... Component in water-soluble film No. 25791–96–2). Glyceryl triacetate ...... Stabilizer Glyceryl tris-12-hydroxystearate ...... Flow control agent Graphite ...... Treatment aid for seeds Guar hydroxypropyltrimethylammonium chloride ...... Thickener/drift reduction agent (CAS Reg. No. 71329–50–5).

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Inert ingredients Limits Uses

Hexamethylenetetramine ...... Stabilizer for carriers in solid pesticide formulations 2-(2′-hydroxy-3′,5′-di-tert-amylphenyl) Maximum concentration of Ultraviolet (UV) stabilizer benzotriazole (CAS Reg. No. 25973–55–1). 0.6% in insecticide formulations applied to adzuki beans, canola, chickpeas, cotton, faba beans, field peas, lentils, linola, linseed, lucerne, lupins, mung beans, navy beans, pigeon peas, safflower, sunflower, and vetch. 2-Hydroxy-4-n-octoxybenzophenone (CAS Reg. Not more than 0.2 pt of Light stabilizer No. 1843–05–6). pesticide formulation. Hydroxypropyl guar gum ...... Thickener Isobornyl acetate ...... Solvent Isobutyl alcohol ...... Do. Isobutylene-butene copolymers ...... For soil application only ...... Binder Isooctadecanol ...... Not more than 2% of pes- Defoaming agent ticide formulation. Lanthanum chloride ...... 10 ppm in formulation ...... Tagging agent. Magnesium nitrate (in combination with 2-meth- None ...... Preservation yl-4-isothiazolin-3-one and 5-chloro-2-methyl- 4-isothiazolin-3-one). Maleic acid ...... For pesticide formulations Stabilizer applied to apples with a minimum preharvest interval of 21 days. Maleic anhydride (CAS Reg. No. 108–31–6) ...... Not to exceed 3.5% in pes- Stabilizer ticide formulations; or for pesticide formulations applied to apples with a minimum preharvest interval of 21 days. Manganese carbonate ...... Plant nutrient D-mannose (CAS Reg. No. 3458–28–4) ...... Sequestrant, binder, filler Mesityl oxide ...... Not for use after edible Solvent, cosolvent parts of plant begin to form. Do not graze livestock in treated areas within 48 hours after application. Methionine (CAS Reg. No. 59–51–8) ...... Maximum of 0.5% of formu- Synergist lation. Methyl alcohol ...... Do. Methyl ethyl ketone ...... Surfactant Methyl p- hydroxybenzoate ...... Preservative for formulations Methyl isobutyl ketone ...... Solvent, cosolvent 2-Methyl-4-isothiazolin-3-one (in combination Not more than 0.0022% Preservative with 5-chloro-2-methyl-4-isothiazolin-3-one). (22.5 ppm) in the formulation; 0.00022% (or 2.25 ppm) in the final solution applied to growing crops. Mono-, di-, and trimethylnapthalenesulfonic ...... Surfactants, related adjuvants of surfactants acids and napthalenesulfonic acids formaldehyde condensates, ammonium and sodium salts (CAS Reg. Nos. 9008–63–3, 9069–80–1, 9084–06–4, 36290–04–7, 91078–68–1, 141959–43–5, 68425–94–5). Methyl oleate ...... Surfactant 2-Methyl-2,4-pentanediol ...... Solvent for formulations used before crop emerges from soil

Methyl poly(oxyethylene)C8–C18 alkylammonium Concentration in formulated Surfactants, related adjuvants of surfactants chlorides where the poly(oxyethylene) content end use products not to is n = 2–15 and where C8–C18 alkyl is linear exceed 10% by weight in and may be saturated or unsaturated (CAS herbicide products and Reg. Nos. 3010–24–0, 18448–65–2, 70750– 5% by weight in all other 47–9, 22340–01–8, 67784–77–4, 64755–05– pesticide products. 1, 61791–10–4, 28724–32–5, 28880–55–9, 68187–69–9, 68607–27–2, 60687–90–3. N-Methylpyrrolidone (CAS Reg. No. 872-504) ...... Solvent, cosolvent

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Inert ingredients Limits Uses

Mixed phytosterols (consisting of campesterol, ...... Surfactant sitosterol and stigmasterol, with minor amounts of associated plant sterols) derived from edible vegetable oils. Mono- and bis-(1H, 1H, 2H, 2H-perfluoroalkyl) Not more than 0.5% of pes- Surfactant, related adjvants of surfactants phosphates where the alkyl group is even ticide formulation. Expires numbered and in the C6-C12 range. February 9, 2008. Mono- and dialkyl (C8-C18) methylated ammo- ...... Surfactants, related adjuvants of surfactants nium chloride compounds, where the alkyl group(s) (C8-C18) are derived from coconut, cottonseed, soya, tallow, or hogfat fatty acids. Morpholine 4-C6-12 Acyl Derivatives (CAS Reg...... As a solvent No. 887947–29–7). Nicotinamide (CAS Reg. No. 98–92–0) ...... Maximum of 0.5% of formu- Synergist lation. a-(p-Nonylphenyl)-w-hydroxypoly(oxyethylene); ...... Surfactant produced by the condensation of 1 mole of nonylphenol (nonyl group is a propylene trimer isomer) with an average of 4-14 or 30- 100 moles of ethylene oxide; if a blend of products is used, the average number of moles of ethylene oxide reacted to produce any product that is a component of the blend shall be in the range 4-14 or 30-100. Octanamide, N,N-dimethyl (CAS Reg. No...... Emulsifier, solvent, cosolvent 1118–92–9). a-Oleoyl-w-(oleoyloxy) poly(oxyethylene) derived ...... Component of defoamers from a-hydro-w-hydroxypoly(oxyethylene) (molecular weight 600 amu). Oxo-decyl acetate (CAS reg. No. 108419–33–6) ...... Solvent Oxo-heptyl acetate (CAS Reg. No. 90438–79–2) ...... Solvent Oxo-hexyl acetate (CAS Reg. No. 88230–35–7) ...... Solvent Oxo-nonyl acetate (CAS Reg. No. 108419–34– ...... Solvent 7). Oxo-octyl acetate (CAS Reg. No. 108419–32–5) ...... Solvent Oxo-tridecyl acetate (CAS Reg. No. 108419– ...... Solvent 35–8). Phenol ...... Solvent, cosolvent Phenol, 2-(2H-benzotriazol-2-yl)-6-dodecyl-4- Not more than 10% by UV stabilizer. methyl-, (CAS Reg. No. 23328–53–2). weight of pesticide formulations. Phenolsulfonic acid—formaldehyde—urea con- Applied to growing plants Dispersant surfactant densate and its sodium salt. only. (Phthalocyaninato (2)) copper; (C.I. pigment When used as a colorant in Coloring agent, pigment blue No. 15). low-density plastic films. Pigment red 48 ...... For seed treatment use Dye only. a-Pinene ...... Not more than 2% of formu- Stabilizer lation by weight. Poly(oxy-1,2-ethanediyl), a-isotridecyl-w- At a maximum of 10% in Surfactant methoxy (CAS Reg. No. 345642–79–7). formulation. Poly(oxy-1,2-ethanediyl), a-(3-carboxy-1- Not to exceed 0.125% for Surfactant. oxosulfopropyl)-w-hydroxy-, (C10–C12)-alkyl seed treatment use only. ethers, disodium salts, polyoxylene content averages 4–5 moles (CAS Reg. No. 68815– 56–5). Poly(oxy-1,2-ethanediyl), a-(3-carboxy-1- Not to exceed 0.125% for Surfactant oxosulfopropyl)-w-hydroxy-, (C10–C16)-alkyl seed treatment use only. ethers, disodium salts, polyoxyethylene content averages 5 moles (CAS Reg. No. 68954– 91–6). Poly(oxyethylene) adducts of mixed phytosterols ...... Surfactant, related adjuvants (such sterols to consist of campesterol, stigmasterol and sitosterol with minor amounts of associated plant sterols) derived from edible vegetable oils; polyoxyethylene content averaging 5-26 moles. Polyoxyethylene polyoxypropylene mono(di-sec- Limited to herbicide formu- Surfactants, related adjuvants of surfactants butylphenyl) ether (CAS Reg. No. 69029–39– lations only, and to no 6). more than 30% by weight in herbicide formulations intended for application to turf. Poly(oxyethylene) (5) sorbitan monooleate ...... Surfactants, related adjuvants of surfactants

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Inert ingredients Limits Uses

Polysorbate 60, conforming to 21 CFR 172.836 ...... Surfactant Potassium dihydrogen phosphate ...... Buffering agent 2-Propanamine, compound with a-phosphono-w- Not more than 15% in the Surfactant butoxypoly (oxy-1,2-ethanediyl) (2:1) (CAS formulated product. Reg. No. 431040–31–2). 2-Propanamine, compounds with polyethylene Not more than 15% in the Surfactant glycol dihydrogen phosphate C8–10- alkyl ether formulated product. (2:1) (CAS Reg. No. 431062–72–5). 1,2-Propanediol, 3-[3-[1, 3, 3, 3-tetramethyl-1- Not to exceed 5% by Antifoaming agent. [(trimethylsilyl)oxy]-1-disiloxyanyl] propoxy]- weight of pesticide formu- (CAS Reg. No. 70280–68–1). lation. Propylene glycol monomethyl ether ...... Solvent Pyridoxine (CAS Reg. No. 65–23–6) ...... Maximum of 0.5% of formu- Synergist lation. Rosin, dark wood (as defined in 21 CFR ...... Surfactants, related adjuvants of surfactants 178.3870(a)(1)(v)). Rosin, gum ...... Do. Rosin, tall oil ...... Do. Scandium chloride ...... 10 ppm in formulation ...... Tagging agent Sodium bisulfate (CAS Reg. No. 7681–38–1) ...... Acidifying/buffering agent Sodium 1,4-dicyclohexyl sulfosuccinate ...... Surfactants, related adjuvants of surfactants Sodium 1,4-dihexyl sulfosuccinate (CAS Reg...... Surfactants, related adjuvants of surfactants No. 3006–15–3). Sodium dihydrogen phosphate (CAS Reg. No...... Buffering agent 7558–80–7) conforming to 21 CFR 182.6778. Sodium 1,4-diisobutyl sulfosuccinate (CAS Reg...... Surfactants, related adjuvants of surfactants No. 127–39–9). Sodium 1,4-dipentyl sulfosuccinate (CAS Reg...... Surfactants, related adjuvants of surfactants No. 922–80–5). Sodium metaborate ...... Sequestrant Sodium molybdate ...... Plant nutrient Sodium nitrate ...... Solid diluent Sodium nitrite ...... Not more than 3% of pes- Stabilizer, inhibitor. ticide formulation. Sodium o-phenylphenate ...... Not more than 0.1% of pes- Preservative for formulation ticide formulation. Sodium salt of the insoluble fraction of rosin ...... Surfactants, related adjuvants of surfactants Sodium salts of N-alkyl (C8-C18)-beta- Concentration in formulated Surfactants, related adjuvants of surfactants iminodipropionic acid where the C8-C18 is lin- end-use products not to ear and may be saturated and/or unsaturated exceed 30% by weight in (CAS Reg. Nos. 3655-00-3, 61791-56-8, pesticide formulations. 14960-06-6, 26256-79-1, 90170-43-7, 91696- 17-2, 97862-48-1). Sodium tetraborate ...... Not more than 2% of pes- Buffering agent; corrosion inhibitor ticide formulation. Sulfonic acids, C13-17-sec-alkane, sodium salts Not to exceed 40% by Surfactant (CAS Reg. No. 85711–69–9). weight in non-residential use pesticide formulation only. Sulfonic acids, C14-17-sec-alkane, sodium salts Not to exceed 40% by Surfactant (CAS Reg. No. 97489–15–1). weight in non-residential pesticide formulation only. Tallowamine, ethoxylated, mixture of dihydrogen Not to exceed 20% of pes- Surfactants, related adjuvants of surfactants phosphate and monohydrogen phosphate ticide formulation. esters and the corresponding ammonium, calcium, potassium, and sodium salts of the phosphate esters, where the poly(oxyethylene) content averages 2–20 moles (CAS Reg. No. 68308–48–5). Tannin ...... Dispersing agent Tertiary butylhydroquinone ...... Antioxidant 1-Tetradecanamine, N,N-dimethyl-, N-oxide ...... Component in water-soluble film (CAS Reg. No. 3332–27–2). Tetraethylene glycol (CAS Reg. No. 112–60–7) ...... Solvent N,N,N′,N″-Tetrakis-(2-hydroxypropyl) ethylene- Concentration in formulated Stabilizer for formulations diamine (CAS Reg. No. 102–60–3). end-use products not to exceed 20% by weight in pesticide formulations. 2,4,7,9-Tetramethyl-5-decyne 4,7-diol ...... In pesticide formulations, Surfactants, related adjuvants of surfactants for application to soil prior to planting or to plants before edible parts form. Tetrapotassium pyrophosphate (CAS Reg. No. Not to exceed 10% of for- Sequestrant, anticaking agent, conditioning 7320–345). mulation. agent

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Inert ingredients Limits Uses

Titanium dioxide (CAS Reg. No. 13463–67–7) ...... Pigment/coloring agent in plastic bags used to wrap growing banana (preharvest), colorant on seeds for planting Toluenesulfonic acid and its ammonium, cal- ...... Solvent, cosolvent cium, magnesium, potassium, sodium, and zinc salts. Triethanolamine ...... Stabilizer, inhibitor for formulations used before crop emerges from soil Triethanolamine (CAS Reg. No. 102–71–6) ...... Stabilizer, inhibitor Triethylene glycol ...... Deactivator Triethyl phosphate ...... Stabilizer for formulations used before crop emerges from soil Trimethylolpropane (CAS Reg. No. 77–99–6) .... Not to exceed 15% by Component in water-soluble film weight of the film. a-[2,4,6-Tris[1-(phenyl)ethyl]phenyl]-w-hydroxy Not more than 15% of the Surfactant. poly(oxyethylene), the poly(oxyethylene) con- formulation. tent averages 4-150 moles). a-[2,4,6-Tris[1-(phenyl)ethyl]phenyl]-w-hydroxy Not more than 15% of the Do. poly(oxyethylene); mixture of monohydrogen formulation. and dihydrogen phosphate esters and the corresponding ammonium, calcium, magnesium, potassium, sodium, and zinc salts, the poly(oxyethylene) content averages 4-150 moles). a-[2,4,6-Tris[1-(phenyl)ethyl]phenyl]-w-hydroxy Not more than 15% of the Do. poly(oxyethylene) sulfate, and the cor- pesticide formulation. responding ammonium, calcium, magnesium, potassium, sodium, and zinc salts, the poly(oxyethylene) content averages 4-150 moles. Tryptophan (CAS Reg. No. 73–22–3) ...... Maximum of 0.5% of formu- Synergist lation. Valeric acid, normal ...... Not more than 2% in pes- Stenching agent or odorant ticide formulations. Xylene ...... Solvent, cosolvent Xylenesulfonic acid its ammonium calcium, mag- ...... Surfactants, related adjuvants of surfactants nesium, potassium, sodium, and zinc salts. Yucca extract from Yucca schidigera ...... Wetting agent Ytterbium chloride ...... 10 ppm in formulation ...... Tagging agent Yttrium chloride ...... 10 ppm in formulation ...... Tagging agent Zinc orthophosphate ...... Plant nutrient and safener Zinc stearate, conforming to 21 CFR 182.5994 ...... Flow control agent and 582.5994.

[69 FR 23124, Apr. 28, 2004]

EDITORIAL NOTE: For FEDERAL REGISTER citations affecting § 180.920, see the List of CFR Sections Affected, which appears in the Finding Aids section of the printed volume and at www.fdsys.gov.

§ 180.930 Inert ingredients applied to when used in accordance with good ag- animals; exemptions from the re- ricultural practice as inert (or occa- quirement of a tolerance. sionally active) ingredients in pesticide The following materials are exempt- formulations applied to animals: ed from the requirement of a tolerance

Inert ingredients Limits Uses

Acetic acid (CAS Reg. No. 64–19–7) ...... Not more than 0.5% of pesticide Catalyst formulation. Acetic anhydride ...... Solvent, cosolvent, stabilizer Acetone (Cas Reg. No. 67–64–1) ...... Solvent or cosolvent Alkanoic and alkenoic acids, mono- and diesters of a-hydro- ...... Emulsifiers w-hydroxypoly(oxyethylene) with molecular weight (in amu) range of 200 to 6,000.

Alkyl (C8-C24) benzenesulfonic acid and its ammonium, cal- ...... Surfactants, emulsifier, related adjuvants of surfactants cium, magnesium, potassium, sodium, and zinc salts.

Alkyl (C12-C16) dimethyl ammonio acetate (CAS Reg. Nos. 20% by weight in pesticide for- Surfactant 683–10–3, 2601–33–4 and 693–33–4. mulation.

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Inert ingredients Limits Uses

a-alkyl(C6- C15)-w-hydroxypoly(oxyethylene)sulfate, and its Not to exceed 30% of formula- Surfactants, related adjuvants of surfactants. ammonium, calcium, magnesium, potassium, sodium, and tion. zinc salts, poly(oxyethylene) content averages 2–4 moles (CAS Reg. Nos.: 3088–31–1, 3694–74–4, 9004–82–4, 9004–84–6, 9021–91–4, 9086–52–6, 13150–00–0, 15826– 16–1, 25446–78–0, 26183–44–8, 27140–00–7, 27731–61– 9, 27731–61–9, 27731–62–0, 32612–48–9, 34431–25–9, 35015–74–8, 50602–06–7, 52286–18–7, 52286–19–8, 54116–08–4, 55901–67–2, 61702–79–2, 61894–66–4, 62755–21–9, 63428–85–3, 63428–86–4, 63428–87–5, 65086–57–9, 65086–79–5, 65104–74–7, 65122–38–5, 67674–66–2, 67762–19–0, 67762–21–4, 67845–82–3, 67845–83–4, 67923–90–4, 68037–05–8, 68037–06–9, 68171–41–5, 68424–50–0, 68511–39–7, 68585–34–2, 68610–66–2, 68611–29–0, 68611–55–2, 68649–53–6, 68890–88–0, 68891–29–2, 68891–30–5, 68891–38–3, 69011–37–6, 73665–22–2, 75422–21–8, 78330–16–2, 78330–17–3, 78330–25–3, 78330–26–4, 78330–27–5, 78330–28–6, 78330–29–7, 78330–30–0, 96130–61–9, 106597–03–9, 110392–50–2, 119432–41–6, 125301–88–4, 125301–89–5, 125301–92–0, 125736–54–1, 157707–85–2, 160104–51–8, 160901–27–9, 160901–28–0, 160901–29–1, 160901–30–4, 161025–28–1, 161074–79–9, 162063–19–6, 219756–63–5).

a-alkyl (C12-C15)-w-hydroxypoly (oxypropylene)poly (oxy- Not to exceed 20% of pesticide Surfactant ethylene)copolymers (where the poly(oxypropylene) content formulations. is 3-60 moles and the poly(oxyethylene) content is 5-80 moles), the resulting ethoxylated propoxylated (C12-C15) alcohols having a minimum molecular weight (in amu) of 1,500, CAS Reg. No. 68551–13–3. a-alkyl-w-hydroxypoly (oxypropylene) and/or poly (oxy- ...... Surfactants, related adjuvants of surfactants ethylene) polymers where the alkyl chain contains a minimum of six carbons (CAS Reg. Nos.: 9002–92–0; 9004– 95–9; 9004–98–2; 9005–00–9; 9035–85–2; 9038–29–3; 9038–43–1; 9040–05–5; 9043–30–5; 9087–53–0; 25190– 05–0; 24938–91–8; 25231–21–4; 251553–55–6; 26183–52– 8; 26468–86–0; 26636–39–5; 27252–75–1; 27306–79–2; 31726–34–8; 34398–01–1; 34398–05–5; 37251–67–5; 37311–00–5; 37311–01–6; 37311–02–7; 37311–04–9; 39587–22–9; 50861–66–0; 52232–09–4; 52292–17–8; 52609–19–5; 57679–21–7; 59112–62–8; 60828–78–6; 61702–78–1; 61725–89–1; 61791–13–7; 61791–20–6; 61791–28–4; 61804–34–0; 61827–42–7; 61827–84–7; 62648–50–4; 63303–01–5; 63658–45–7; 63793–60–2; 64366–70–7; 64415–24–3; 64415–25–4; 64425–86–1; 65104–72–5; 65150–81–4; 66455–14–9: 66455–15–0; 67254–71–1; 67763–08–0; 68002–96–0; 68002–97–1; 68131–39–5; 68131–40–8; 68154–96–1; 68154–97–2; 68154–98–3; 68155–01–1; 68213–23–0; 68213–24–1; 68238–81–3; 68238–82–4; 68409–58–5; 68409–59–6; 68439–30–5; 68439–45–2; 68439–46–3; 68439–48–5; 68439–49–6; 68439–50–9; 68439–51–0; 68439–53–2; 68439–54–3; 68458–88–8; 68526–94–3; 68526–95–4; 68551–12–2; 68551–13–3; 68551–14–4; 68603–20–3; 68603–25–8; 68920–66–1; 68920–69–4; 68937–66–6; 68951–67–7; 68954–94–9; 68987–81–5; 68991–48–0; 69011–36–5; 69013–18–9; 69013–19–0; 69227–20–9; 69227–21–0; 69227–22–1; 69364–63–2; 70750–27–5; 70879–83–3; 70955–07–6; 71011–10–4; 71060–57–6; 71243–46–4; 72066–65–0; 72108–90–8; 72484–69–6; 72854–13–8; 72905–87–4; 73018–31–2; 73049–34–0; 74432–13–6; 74499–34–6; 78330–19–5; 78330–20–8; 78330–21–9; 78330–23–1; 79771–03–2; 84133–50–6; 85422–93–1; 97043–91–9; 97953–22–5; 102782–43–4; 103331–86–8; 103657–84–7; 103657–85–8; 103818–93–5; 103819–03–0; 106232–83–1; 111905–54–5; 116810–31–2; 116810–32–3; 116810–33–4; 120313–48–6; 120944–68–5; 121617–09–2; 126646–02–4; 126950–62–7; 127036–24–2; 139626–71–4; 152231–44–2; 154518–36–2; 157627–86–6; 157627–88–8; 157707–41–0; 157707–43–2; 159653–49–3; 160875–66–1; 160901–20–2; 160901–09–7; 160901–19–9; 161025–21–4; 161025–22–5; 166736–08–9; 169107–21–5; 172588–43–1; 176022–76–7; 196823–11–7; 287935–46–0; 288260–45–7; 303176–75–2; 954108–36–2).

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Inert ingredients Limits Uses

a-alkyl (minimum C6 linear, branched, saturated and/or un- Not to exceed 30% of formula- Surfactants, related adjuvants of surfactants. saturated)-w-hydroxypolyoxyethylene polymer with or with- tion. out polyoxypropylene, mixture of di- and monohydrogen phosphate esters and the corresponding ammonium, calcium, magnesium, monoethanolamine, potassium, sodium, and zinc salts of the phosphate esters; minimum oxyethylene content is 2 moles; minimum oxypropylene content is 0 moles, (CAS Reg. Nos.: 9004–80–2, 9046–01–9, 26982–05–8, 31800–89–2, 37280–82–3, 37281–86–0, 39341–09–8, 39341–65–6, 39464–66–9, 39464–69–2, 42612–52–2, 50643–20–4, 50668–50–3, 51325–10–1, 51884–64–1, 52019–36–0, 52019–38–2, 52019–38–2, 57486–09–6, 58206–38–5, 58318–92–6, 58857–49–1, 59112–71–9, 60267–55–2, 61837–79–4, 62362–49–6, 62482–61–5, 63747–86–4, 63887–54–7, 63887–55–8, 66020–37–9, 66272–25–1, 66281–20–7, 67711–84–6, 67786–06–5, 67989–06–4, 68070–99–5, 68071–17–0, 68071–35–2, 68071–37–4, 68130–44–9, 68130–45–0, 68130–46–1, 68130–47–2, 68186–29–8, 68186–34–5, 68186–36–7, 68186–37–8, 68238–84–6, 68311–02–4, 68311–04–6, 68332–75–2, 68389–72–0, 68400–75–9, 68413–78–5, 68425–73–0, 68425–75–2, 68439–39–4, 68458–48–0, 68511–15–9, 68511–36–4, 68511–37–5, 68551–05–3, 68585–15–9, 68585–16–0, 68585–17–1, 68585–36–4, 68585–39–7, 68603–24–7, 68607–14–7, 68610–64–0, 68610–65–1, 68649–29–6, 68649–30–9, 68650–84–0, 68815–11–2, 68855–46–9, 68856–03–1, 68890–90–4, 68890–91–5, 68891–12–3, 68891–13–4, 68891–26–9, 68908–64–5, 68909–65–9, 68909–67–1, 68909–69–3, 68921–24–4, 68921–60–8, 68954–87–0, 68954–88–1, 68954–92–7, 68987–35–9, 69029–43–2, 69980–69–4, 70247–99–3, 70248–14–5, 70844–96–1, 70903–63–8, 71965–23–6, 71965–24–7, 72480–27–4, 72623–67–7, 72623–68–8, 72828–56–9, 72828–57–0, 73018–34–5, 73038–25–2, 73050–08–5, 73050–09–6, 73361–29–2, 73378–71–9, 73378–72–0, 73559–42–9, 73559–43–0, 73559–44–1, 73559–45–2, 74499–76–6, 76930–25–1, 78041–18–6, 78330–22–0, 78330–24–2, 82465–25–6, 84843–37–8, 91254–26–1, 93925–54–3, 95014–34–9, 96416–89–6, 99924–51–3, 103170–31–6, 103170–32–7, 106233–09–4, 106233–10–7, 108818–88–8, 110392–49–9, 111798–26–6, 111905–50–1, 116671–23–9, 117584–36–8, 119415–05–3, 120913–45–3, 121158–61–0, 121158–63–2, 123339–53–7, 125139–13–1, 125301–86–2, 125301–87–3, 126646–03–5, 129208–04–4, 129870–77–5, 129870–80–0, 130354–37–9, 136504–88–6, 143372–50–3, 143372–51–4, 144336–75–4, 146815–57–8, 151688–56–1, 154518–39–5, 154518–40–8, 155240–11–2, 159704–69–5, 160498–49–7, 160611–24–5, 171543–66–1, 172027–16–6, 172274–69–0, 176707–42–9, 181963–82–6, 188741–55–1, 191940–53–1, 210493–60–0, 210993–53–6, 246159–55–7, 251298–11–0, 261627–68–3, 290348–69–5, 290348–70–8, 317833–96–8, 340681–28–9, 422563–19–7, 422563–26–6, 522613–09–8, 717140–06–2, 717140–09–5, 717827–29–7, 762245–80–7, 762245–81–8, 866538–89–8, 866538–90–1, 873662–29–4, 913068–96–9, 936100–29–7, 936100–30–0, 1072943–56–6, 1087209–87–7, 1174313–54–2, 1187742– 89–7, 1187743–35–6, 1205632–03–6, 1233235–49–8, 1451002–50–8, 1456802–88–2, 1456802–89–3, 1456803– 12–5). N-alkyl (C8-C18) primary amines and their acetate salts Concentration in formulated Surfactants, related adjuvants of surfactants where the alkyl group is linear and may be saturated and/or end-use products not to ex- unsaturated (CAS Reg. Nos. 61790–57–6, 61790–58–7, ceed 10% by weight in herbi- 61790–59–8, 61790–60–1, 61788–46–3, 61790–33–8, cide products, 4% by weight 68155–38–4). in insecticide products, and 4% by weight in fungicide products. Alkyl (C8-C18) sulfate and its ammonium, calcium, magnesium, ...... Surfactant potassium, sodium, and zinc salts. N,N-Bis-a-ethyl-w-hydroxypoly(oxy-1,2-ethanediyl) C8–C18 Not to exceed 25% in herbicide Surfactants, related adjuvants of surfactants saturated and unsaturated alkylamines; the poly(oxy-1,2- formulations and 10% in in- ethanediyl) content is 2–60 moles (CAS Reg. Nos. 10213– secticide and fungicide formu- 78–2, 25307–17–9, 26635–92–7, 26635–93–8, 288259–52– lations. 9, 58253–49–9, 61790–82–7, 61791–14–8, 61791–24–0, 61791–26–2, 61791–31–9, 61791–44–4, 68155–33–9, 68155–39–5, 68155–40–8,70955–14–5, 73246–96–5, 1266162–49–5). N,N-Bis-a-ethyl-w-hydroxypoly(oxy-1,2-ethanediyl/oxy(methyl- Not to exceed 25% in herbicide Surfactants, related adjuvants of surfactants 1,2-ethanediyl) C8-C18 saturated and unsaturated formulations and 10% in in- alkylamines; the poly(oxy-1,2-ethanediyl/oxy(methyl-1,2- secticide and fungicide formu- ethanediyl) content is 2–60 moles (CAS Reg. Nos. 68213– lations. 26–3, 68153–97–9, 75601–76–2). Ascorbyl palmitate ...... Preservative Attapulgite-type clay ...... Solid diluent, carrier Barium sulfate (CAS Reg. No. 7727–43–7) ...... Carrier, density control agent Benzoic acid ...... Preservative for formulations

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Inert ingredients Limits Uses

2-Bromo-2-nitro-1,3-propanediol (CAS Reg. No. 52–51–7) ...... 0.04% or less by weight of the In-can preservative total pesticide formulation. Butane ...... Propellant n-Butanol (CAS Reg. No. 71–36–3) ...... Solvent for blended emulsifiers n-Butyl benzoate (CAS RN 136–60–7) ...... Solvent Butylated hydroxyanisole ...... Antioxidant Butylated hydroxytoluene ...... Do. Calcium carbonate ...... Solid diluent, carrier Calcium chloride ...... Stabilizer Calcium silicate, hydrated calcium silicate ...... Anticaking agent, solid diluent, carrier C9 rich aromatic hydrocarbons (CAS Reg. No. 64742–95–6) ...... Solvent. C10–11 rich aromatic hydrocarbons (CAS Reg. No. 64742–94– ...... Solvent. 5). C11–12 rich aromatic hydrocarbons (CAS Reg. No. 64742–94– ...... Solvent. 5). Calcium stearate (CAS Reg. No. 1592–23–0) ...... Stabilizer, component of plastic animal tag Calcium sulfate ...... Solid diluent, carrier Carbon black (CAS Reg. No. 1333–86–4) ...... Colorant/pigment in animal tag Carbon Dioxide (CAS Reg. No. 124–38–9) ...... None ...... Propellant Carrageenan, conforming to 21 CFR 172.620 ...... Minimum molecular weight (in Thickener amu): 100,000. Cyclohexanone ...... Solvent, cosolvent D&C Green No. 6 ...... Dye, coloring agent D&C Red No. 17 ...... Do. D&C Violet No. 2 ...... Do. Dialkyl (C8-C18) dimethylammonium chloride ...... Not more than 0.2% in silica hy- Flocculating agent in the manufacture of silica hydrated silica. drated silica for use as a solid diluent, carrier Diatomite (diatomaceous earth) ...... Solid diluent, carrier Diethanolamine salts of alkyl (C8-C24) benzenesulfonic acid Not to exceed 7% of pesticide Surfactants, related adjuvants of surfactants. (CAS Reg. Nos. 26545–53–9, 67815–95–6, 67889–94–5, formulation. 67889–95–6, 68259–34–7, 68478–47–7, 68567–68–0, 68815–34–9, 68815–37–2, 68891–02–1, 68953–97–9, 84989–15–1, 85338–09–6, 90194–39–1, 90194–40–4, 90218–08–9). Diethylaminoethanol, ethoxylated, propoxylated, reaction prod- ...... Surfactant ucts with fatty acid dimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173188–75– 4). Diethylaminoethanol, ethoxylated, propoxylated, reaction prod- ...... Surfactant ucts with fatty acid trimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173188–83– 4). Diethylaminoethanol, ethoxylated, reaction products with acid ...... Surfactant trimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173188–81–2). Diethylaminoethanol, ethoxylated, reaction product with fatty ...... Surfactant acid dimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173188–72–1). Diethylphthalate ...... Solvent, cosolvent 1,1-Difluoroethane (CAS Reg. No. 75–37–6) ...... For aerosol pesticide formula- Aerosol propellant tions used for insect control in food- and feed-handling establishments and animals. Dimethyl ether (CAS Reg. No. 115–10–6) ...... Propellant Dimethylaminoethanol, ethoxylated, propoxylated, reaction ...... Surfactant products with fatty acid dimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173188– 42–5). Dimethylaminoethanol, ethoxylated, propoxylated reaction ...... Surfactant products with fatty acid trimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173188– 67–4). Dimethylaminoethanol, ethoxylated, reaction products with ...... Surfactant fatty acid trimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173188–38–9). Dimethylaminoethanol, ethoxylated, reaction products with ...... Surfactant fatty acid trimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173188–49–2). Dimethylaminopropylamine, isopropylamine, ethanolamine, ...... Surfactants, related adjuvants of surfactants. and triethanolamine salts of alkyl (C8-C24) benzenesulfonic acid (CAS Reg. Nos. 3088–30–0, 12068–12–1, 26264–05– 1, 26836–07–7, 27323–41–7, 55470–69–4, 58089–99–9, 61886–59–7, 61931–76–8, 67924–05–4, 68110–32–7, 68259–35–8, 68411–31–4, 68442–72–8, 68567–69–1, 68584–24–7, 68584–25–8, 68648–81–7, 68648–96–4, 68649–00–3, 68815–30–5, 68815–35–0, 68910–32–7 68953–93–5, 68953–98–0, 70528–84–6, 72391–21–0, 84961– 74–0, 85480–55–3, 85480–56–4, 85995–82–0, 90194–42– 6, 90194–53–9, 90194–54–0, 90194–55–1, 90218–09–0, 90218–11–4, 90218–35–2, 96687–54–6, 99924–49–9, 121617–08–1, 157966–96–6, 193562–36–6, 319926–68–6, 877677–48–0, 1093628–27–3).. 3,6-Dimethyl-4-octyne-3,6-diol ...... Not more than 2.5% of pesticide Surfactants, related adjuvants of surfactants formulation. Dimethylpolysiloxane (CAS Reg. No. 9016–00–6) ...... Defoaming agent Di-n-butyl carbonate (CAS Reg. No. 542–52–9) ...... Solvent Dipropylene glycol monomethyl ether ...... Surfactants, related adjuvants of surfactants

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Inert ingredients Limits Uses

Epoxidized soybean oil (CAS Reg. No. 8013–07–8) ...... Stabilizer, plasticizer, component animal tag Ethanesulfonic acid, 2-hydroxy- (CAS Reg. No. 107–36–8) ...... Chelator, sequestrant, or conditioning agent. Ethanesulfonic acid, 2-hydroxy-, ammonium salts (CAS Reg...... Do. No. 57267–78–4). Ethanesulfonic acid, 2-hydroxy-, calcium salts (CAS Reg. No...... Do. 10550–47–7). Ethanesulfonic acid, 2-hydroxy-, magnesium salts (CAS Reg...... Do. No. 17345–56–1). Ethanesulfonic acid, 2-hydroxy-, potassium salts (CAS Reg...... Do. No. 1561–99–5). Ethanesulfonic acid, 2-hydroxy-, sodium salts (CAS Reg. No...... Do. 1562–00–1). Ethanesulfonic acid, 2-hydroxy-, zinc salts (CAS Reg. No...... Do. 129756–32–7). Ethyl alcohol ...... Solvent, cosolvent Ethyl maltol (CAS Reg. No.4940–11–8) ...... Not more than 0.2 % of the pes- Odor masking agent ticide formulation. Ethylene oxide adducts of 2,4,7,9-tetramethyl-5-decynediol, ...... Surfactants, related adjuvants of surfactants the ethylene oxide content averages 3.5, 10 or 30 moles (CAS Reg. No. 9014–85–1). 2-Ethyl-1-hexanol (CAS Reg. No. 104–76–7) ...... Not more than 10% of pesticide Solvent, adjuvant of surfactants FD&C Blue No. 1 ...... Dye, coloring agent FD&C Yellow No. 6 Aluminum Lake (CAS Reg. No. 15790– Not more than 2% by weight of Pigment in animal tag and similar slow-release devices 07–5). pesticide formulation. D-glucopyranose, oligomeric, C10–16-alkyl glycosides (CAS ...... Surfactant Reg. No. 110615–47–9). Glycerol monooleate ...... Surfactants, related adjuvants of surfactants Glyceryl monostearate ...... Emulsifier Glyceryl tris-12-hydroxystearate ...... Flow control agent Graphite ...... Solid diluent, carrier n-Hexyl alcohol (CAS Reg. No. 111–27–3) ...... Solvent, cosolvent Hydroxyethylmorpholine, ethoxylated, propoxylated, reaction ...... Surfactant products with fatty acid dimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173189– 06–4). Hydroxyethylmorpholine, ethoxylated, propoxylated, reaction ...... Surfactant products with fatty acid trimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173188– 67–4). Hydroxyethylmorpholine, ethoxylated, reaction products with ...... Surfactant fatty acid dimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173189–00–8). Hydroxyethylmorpholine, ethoxylated, reaction products with ...... Surfactant fatty acid trimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173189–09–7). Hydroxyethylpiperidine, ethoxylated, propoxylated, reaction ...... Surfactant products with fatty acid dimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173189– 22–4). Hydroxyethylpiperidine, ethoxylated, propoxylated, reaction ...... Surfactant products with fatty acid trimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173189– 28–0). Hydroxyethylpiperidine, ethoxylated, reaction products with ...... Surfactant fatty acid dimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173189–20–2). Hydroxyethylpiperidine, ethoxylated, reaction products with ...... Surfactant fatty acid trimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173189–25–7). 2-(2′-Hydroxy-5′-methylphenyl)benzotriazole (CAS Reg. No. Not more than 0.5% by weight Ultraviolet light absorber/stabilizer in animal tag and 2440–22–4). of pesticide formulation. similar slow-release devices Iron oxide (CAS Reg. No. 1309–37–1) ...... Colorant in pesticide formulations for animal tags Isobutane (CAS Reg. No. 75–28–5) ...... None ...... Propellant Isopropyl myristate, CAS Reg. No. 110–27–0 ...... Solvent Kaolinite-type clay ...... Solid diluent, carrier Kerosene, U.S.P. reagent ...... Solvent, cosolvent Lactic acid ...... Solvent Lactic acid, 2-ethylhexyl ester (CAS Reg. No. 6283–86–9) ...... Solvent Lactic acid, 2-ethylhexyl ester, (2S)- (CAS Reg. No. 186817– ...... Solvent 80–1). Lactic acid, n-propyl ester, (S); (CAS Reg. No. 53651–69–7) ...... Solvent Lignin (CAS Reg. No. 9005–53–2) ...... Surfactant, related adjuvants of surfactants Lignin, alkali (CAS Reg. No. 8068–05–1) ...... Do. Lignin, alkali, oxidized, sodium salt (CAS Reg. No. 68201–23– ...... Do. 0). Lignin alkali reaction products with disodium sulfite and form- ...... Do. aldehyde (CAS Reg. No. 105859–97–0). Lignin alkali reaction products with formaldehyde and sodium ...... Do. bisulfite (CAS Reg. No. 68512–35–6). Lignosulfonic acid (CAS Reg. No. 8062–15–5) ...... Do. Lignosulfonic acid, ammonium calcium salt (CAS Reg. No...... Do. 12710–04–2). Lignosulfonic acid, ammonium magnesium salt (CAS Reg. No...... Do. 123175–37–1). Lignosulfonic acid, ammonium salt (CAS Reg. No. 8061–53– ...... Do. 8).

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Inert ingredients Limits Uses

Lignosulfonic acid, ammonium sodium salt (CAS Reg. No...... Do. 166798–73–8). Lignosulfonic acid, calcium magnesium salt (CAS Reg. No...... Do. 55598–86–2). Lignosulfonic acid, calcium salt (CAS Reg. No. 8061–52–7) ...... Do. Lignosulfonic acid, calcium sodium salt (CAS Reg. No...... Do. 37325–33–0). Lignosulfonic acid, ethoxylated, sodium salt (CAS Reg. No...... Do. 68611–14–3). Lignosulfonic acid, magnesium salt (CAS Reg. No. 8061–54– ...... Do. 9). Lignosulfonic acid, potassium salt (CAS Reg. No. 37314–65– ...... Do. 1). Lignosulfonic acid, sodium salt (CAS Reg. No. 8061–51–6) ...... Do. Lignosulfonic acid, sodium salt, oxidized (CAS Reg. No...... Do. 68855–41–4). Lignosulfonic acid, sodium salt, polymer with formaldehyde ...... Do. and phenol (CAS Reg. No. 37207–89–9). Lignosulfonic acid, sodium salt, sulfomethylated (CAS Reg...... Do. No. 68512–34–5). Lignosulfonic acid, zinc salt (CAS Reg. No. 57866–49–6) ...... Do. d-Limonene (CAS Reg. No. 5989–27–5) ...... Solvent, fragrance Magnesium carbonate ...... Solid diluent, carrier Magnesium silicate, hydrated magnesium silicate ...... Do. Methane sulfonic acid (CAS Reg. No. 75–75–2) ...... Not to exceed 3.0% by weight in Acidifying agent pesticide formulation. Methyl alcohol ...... Solvent, cosolvent Methyl n-amyl ketone (CAS Reg. No. 110–43–0) ...... Solvent, cosolvent Methyl esters of higher fatty acids conforming to 21 CFR ...... Antidusting agent 573.640. Methyl-p-hydroxybenzoate (Methyl paraben)...... Meets specifications of Food Preservative Chemicals Codex; not to exceed 0.1% in formulations. Methyl isobutyl ketone ...... Solvent, cosolvent 2-methyl-2,4-pentanediol (CAS Reg. No.–107–41–5) ...... Without limitation ...... Growing crops and food animals 2-methyl-1,3-propanediol (CAS Reg. No. 2163–42–0) ...... Solvent, surfactant Mineral oil, U.S.P., or conforming to 21 CFR 172.878 or ...... Solvent, diluent 178.3620(a), (b). Montmorillonite-type clay ...... Solid diluent, carrier Nonyl, decyl, and undecyl glycoside mixture with a mixture of ...... Surfactant nonyl, decyl, and undecyl oligosaccharides and related reaction products (primarily decanol and undecanol) produced as an aqueous-based liquid (50 to 65% solids) from the reaction of primary alcohols (containing 15 to 20% secondary alcohol isomers) in a ratio of 20% C9, 40% C10, and 40% C11 with carbohydrates (average glucose to alkyl chain ratio 1.3 to 1.8). a-(p-Nonylphenol)-w-hydroxypoly(oxyethylene) mixture of di- Not to exceed 7% of pesticide Surfactants, related adjuvants of surfactants hydrogen phosphate and monohydrogen phosphate esters formulation. and the corresponding ammonium, calcium, magnesium, potassium, sodium, and zinc salts of the phosphate esters; the nonyl group is a propylene trimer isomer and the poly(oxyethylene) content averages 4–14 or 30 moles (CAS Reg. Nos. 51811–79–1, 59139–23–0, 67922–57–0, 68412– 53–3, 68553–97–9, 68954–84–7, 99821–14–4, 152143–22– 1, 51609–41–7, 37340–60–6, 106151–63–7, 68584–47–4, 52503–15–8, 68458–49–1). a-(p-Nonylphenol)-w-hydroxypoly(oxyethylene) sulfate, ammo- Not to exceed 7% of pesticide Surfactants, related adjuvants of surfactants nium, calcium, magnesium, potassium, sodium, and zinc formulation. salts the nonyl group is propylene trimer isomer and the poly(oxyethylene) content averages 4 moles (CAS Reg. Nos. 9014–90–8, 9051–57–4, 9081–17–8, 68649–55–8, 68891–33–8. a-(p-Nonylphenyl)-w-hydroxypoly(oxyethylene) produced by ...... Surfactants, emulsifier, related adjuvants of the condensation of 1 mole of nonylphenol (nonyl group is a surfactants. propylene trimer isomer) with an average of 4-15 or 30-90 moles of ethylene oxide; if a blend of products is used, the average number of moles of ethylene oxide reacted to produce any product that is a component of the blend shall be in the range of 4-15 or 30-90 moles. Octadecyl 3,5-di-tert-butyl-4-hydroxyhydro cinnamate (CAS Not more than 0.5% by weight Thermal stabilizer/antioxidant in animal tag and similar Reg. No. 2082–79–3). of pesticide formulation. slow-release devices 1-Octanal (CAS Reg. No. 124–13–0) ...... Not more than 0.2% of the pes- Odor masking agent ticide formulation. Octyl and decyl glucosides mixture with a mixture of octyl and ...... Thermal stabilizer/antioxidant in animal tag and similar decyl oligosaccharides and related reaction products (pri- slow-release devices marily n-decanol) produced as an aqueous-based liquid (68-72% solids) from the reaction of straight chain alcohols (C8(45%), C10) with anhydrous glucose. Octyl epoxytallate (CAS Reg. No. 61788–72–5) ...... Plasticizer, component animal tag Oleic acid, conforming to 21 CFR 172.862 (CAS Reg. No...... Defoaming agent 112–80–1). a-Oleoyl-w-hydroxypoly(oxyethylene), average molecular ...... Emulsifier weight (in amu) of 600. a-Oleoyl-w-(oleyloxy)poly(oxyethylene) derived from a-hydro- ...... Emulsifier, defoaming agent w-hydroxypoly(oxyethylene), molecular weight (in amu) 600.

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Inert ingredients Limits Uses

Pentaerythritol tetrakis (3-(3,5-di-tert-butyl-4- Not to exceed 3% by weight of Antioxidant, stabilizer. hydroxyphenyl)propionate) (CAS Reg. No. 6683–19–8). the pesticide formulation. Petroleum hydrocarbons, light, odorless, conforming to 21 ...... Solvent, diluent CFR 172.884 or 178.3650. Petroleum hydrocarbons, synthetic isoparaffinic, conforming to ...... Do. 21 CFR 172.882 or 178.3530. Phenol ...... Solvent, cosolvent a-Pinene ...... Not more than 2% of formulation Stabilizer by weight. Polyethylene (CAS Reg. No. 9002–88–4) conforming to 21 ...... Component of plastic slow release tag CFR 172.615. Polyethylene glycol [a-hydro-w-hydroxypoly(oxyethylene)]; ...... Surfactants, related adjuvants of surfactants mean molecular weight (in amu) 194 to 9,500 conforms to 21 CFR 178.3750. Potassium benzoate (Cas No. 582–25–2) ...... None ...... Preservative Potassium hydroxide ...... Meeting Food Chemicals, Codex Neutralizer specifications. Propanamide, 2-hydroxy-N, N-dimethyl- (CAS Reg. No. Not to exceed 20% by weight in Solvent/co-solvent 35123–06–9). pesticide formulation. Propane ...... Propellant 1,2,3-Propanetriol, homopolymer diisooctadecanoate (CAS ...... Emulsifier Reg. No. 63705–03–3). n-Propanol ...... Solvent, for blended emulsifiers 2-Propenoic acid, 2-methyl-, polymer with ethyl 2-propenoate ...... Encapsulating agent,dispensers, resins, fibers and and methyl 2-methyl-2-propenoate, ammonium salt (CAS beads Registration No. 55989–05–4), minimum number average molecular weight (in amu), 18,900.. Propylene glycol ...... Solvent, cosolvent Propylene glycol monomethyl ether ...... Deactivator, emmolient Propyl gallate ...... Antioxidant Propyl p-hydroxybenzoate (Propyl paraben)...... Meets specifications of Food Preservative Chemicals Codex; not to exceed 0.1% in formulations. Pyrophylite ...... Solid diluent, carrier Silica, hydrated silica ...... Anticaking agent, solid diluent, carrier Silica aerogel (finely powdered microcellular silica foam hav- ...... Component of antifoaming agent ing a minimum silica content of 89.5%). Soapstone ...... Solid diluent Sodium alkyl naphthalenesulfonates (CAS Reg. Nos. 68909– Limited to no more than 30% by Surfactants, related adjuvants of surfactants 83–1, 68909–84–2, 68909–82–0, 27213–90–7, 26264–58– weight in pesticide end-use 4, 27178–87–6, 111163–74–7, 908356–16–1, 25417–20–3, products. 25638–17–9, 145578–88–7, 1322–93–6, 1323–19–9, 7403– 47–6, 68442–09–1, 127646–44–0, 908356–18–3). Sodium 1,4-dihexyl sulfosuccinate (CAS Reg. No. 3006–15–3) ...... Surfactants, related adjuvants of surfactants Sodium 1,4-diisobutyl sulfosuccinate (CAS Reg. No. 127–39– ...... Surfactants, related adjuvants of surfactants 9). Sodium dioctylsulfosuccinate ...... Surfactants, related adjuvants of surfactants Sodium 1,4-dipentyl sulfosuccinate (CAS Reg. No. 922–80–5) ...... Surfactants, related adjuvants of surfactants Sodium hydroxide ...... Neutralizer Sodium monoalkyl and dialkyl (C6-C16) phenoxy Not to exceed 20% in pesticide Surfactants, related adjuvants of surfactants benzenedisulfonates and related acids (CAS Reg. Nos. formulations. 147732–59–0, 147732–60–3, 169662–22–0, 70191–75–2, 36445–71–3, 39354–74–0, 70146–13–3, 119345–03–8, 149119–20–0, 149119–19–7, 119345–04–9, 28519–02–0, 25167–32–2, 30260–73–2, 65143–89–7, 70191–76–3). Sodium N-oleoyl-N-methyl taurine (CAS Reg. No. 137–20–2) ...... Surfactants, related adjuvants of surfactants Sodium and potassium salts of N-alkyl (C8–C18)-beta- Concentration in formulated Surfactants, related adjuvants of surfactants iminodipropionic acid where the C8–C18 is linear and may end-use products not to ex- be saturated and/or unsaturated (CAS Reg. Nos. 110676– ceed 30% by weight in pes- 19–2, 3655–00–3, 61791–56–8, 14960–06–6, 26256–79–1, ticide formulations. 90170–43–7, 91696–17–2, 97862–48–1). Sodium starch glycolate (CAS Reg. No. 9063–38–1) ...... Granular and tableted products Disintegrant only; not to exceed 8% of the formulated product. Sodium sulfate ...... Solid diluent, carrier Sorbitan fatty acid esters (fatty acids limited to C12, C14, C16, ...... Buffering agent; corrosion inhibition and C18 containing minor amounts of associated fatty acids) and poly(oxyethylene) derivatives of sorbitan fatty acid esters; the poly(oxyethylene) content averages 16-20 moles. Sorbitol ...... Antidusting agent. Stearic acid (CAS Reg. No. 57–11–4) ...... Lubricant, component animal tag a-Stearoyl-w-hydroxypoly(oxyethylene), average molecular ...... Emulsifier weight (in amu) of 600. a-Stearoyl-w-hydroxypoly(oxyethylene); the poly(oxyethylene) ...... Surfactants; related adjuvants of surfactants content averages 8, 9, or 40 moles; if a blend of products is used, the average number of moles of ethylene oxide reacted to produce any product that is a component of the blend shall be 8, 9, or 40. Sulfite liquors and cooking liquors, spent, oxidized (CAS Reg...... Surfactant, related adjuvants of surfactants No. 68514–09–0). Sulfur (CAS Reg. No. 7704–34–9) ...... Stabilizer Talc ...... Do. Tall oil; fatty acids not less than 58%, rosin acids not more ...... Surfactants, related adjuvants of surfactants than 44%, unsaponifiables not more than 8%. Tartrazine ...... Dye, coloring agent

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Inert ingredients Limits Uses

N,N,N′,N″,-tetrakis-(2-hydroxypropyl) ethylenediamine (CAS Concentration in formulated Stabilizer for formulation. Reg. No. 102–60–3). end-use products not to exceed 20% by weight in pesticide formulations. Trans-1,3,3,3-tetrafluoroprop-1-ene (CAS Reg. No. 29118– ...... Propellant. 24–9). 2,4,7,9-Tetramethyl-5-decyne-4.7-diol ...... Not more than 2.5% of pesticide Surfactants, related adjuvants of surfactants formulation. Titanium dioxide (CAS Reg. No. 13463–67–7) ...... Pigment/colorant in pesticide formulations for animal tag Toluenesulfonic acid and its ammonium, calcium, magnesium, ...... Do. potassium, sodium, and zinc salts. Triacetin (glyceryl triacetate) ...... Solvent, cosolvent Trisodium phosphate ...... Precipitant, buffer, filler Xylene ...... Solvent, cosolvent Xylenesulfonic acid and its ammonium, calcium, magnesium, ...... Surfactants, related adjuvants of surfactants potassium, sodium, and zinc salts. Zinc oxide ...... Solid diluent, carrier Zinc stearate, conforming to 21 CFR 182.5994 and 582.5994 ...... Water repellant, dessicant, and coating agent. Zinc stearate (CAS Reg. No. 557–05–1) ...... Water repellant, desiccant, and coating agent; stabilizer, component of plastic animal tag Zinc sulfate (basic and monohydrate) ...... Water repellant, dessicant, and coating agent

[69 FR 23130, Apr. 28, 2004]

EDITORIAL NOTE: For FEDERAL REGISTER citations affecting § 180.930, see the List of CFR Sections Affected, which appears in the Finding Aids section of the printed volume and at www.fdsys.gov.

§ 180.940 Tolerance exemptions for ac- semi-permanent or permanent food- tive and inert ingredients for use in contact surface (other than being ap- antimicrobial formulations (Food- plied on food packaging) with adequate contact surface sanitizing solu- draining before contact with food. tions). (a) The following chemical sub- Residues of the following chemical stances when used as ingredients in an substances are exempted from the re- antimicrobial pesticide formulation quirement of a tolerance when used in may be applied to: Food-contact sur- accordance with good manufacturing faces in public eating places, dairy- practice as ingredients in an anti- processing equipment, and food-proc- microbial pesticide formulation, provided that the substance is applied on a essing equipment and utensils.

Pesticide Chemical CAS Reg. No. Limits

Acetic acid ...... 64–19–7 ...... When ready for use, the end-use concentration is not to exceed 100 ppm Allyl cylcohexylpropionate ...... 2705–87–5 ...... When ready for use, the end-use concentration is not to exceed 100 ppm

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Pesticide Chemical CAS Reg. No. Limits

a-alkyl-w-hydroxypoly (oxypropylene) and/or poly (oxyethylene) 9002–92–0; 9004–95–9; 9004– polymers where the alkyl chain contains a minimum of six 98–2; 9005–00–9; 9035–85– carbons (CAS Reg. No 251553–55–6). 2; 9038–29–3; 9038–43–1; 9040–05–5; 9043–30–5; 9087–53–0; 25190–05–0; 24938–91–8; 25231–21–4; 251553–55–6; 26183–52–8; 26468–86–0; 26636–39–5; 27252–75–1; 27306–79–2; 31726–34–8; 34398–01–1; 34398–05–5; 37251–67–5; 37311–00–5; 37311–01–6; 37311–02–7; 37311–04–9; 39587–22–9; 50861–66–0; 52232–09–4; 52292–17–8; 52609–19–5; 57679–21–7; 59112–62–8; 60828–78–6; 61702–78–1; 61725–89–1; 61791–13–7; 61791–20–6; 61791–28–4; 61804–34–0; 61827–42–7; 61827–84–7; 62648–50–4; 63303–01–5; 63658–45–7; 63793–60–2; 64366–70–7; 64415–24–3; 64415–25–4; 64425–86–1; 65104–72–5; 65150–81–4; 66455–14–9: 66455–15–0; 67254–71–1; 67763–08–0; 68002–96–0; 68002–97–1; 68131–39–5; 68131–40–8; 68154–96–1; 68154–97–2; 68154–98–3;68155–01–1; 68213–23–0; 68213–24–1; 68238–81–3; 68238–82–4; 68409–58–5; 68409–59–6; 68439–30–5; 68439–45–2; 68439–46–3; 68439–48–5; 68439–49–6; 68439–50–9; 68439–51–0; 68439–53–2; 68439–54–3; 68458–88–8; 68526–94–3; 68526–95–4; 68551–12–2; 68551–13–3; 68551–14–4; 68603–20–3; 68603–25–8; 68920–66–1; 68920–69–4; 68937–66–6; 68951–67–7; 68954–94–9; 68987–81–5; 68991–48–0; 69011–36–5; 69013–18–9; 69013–19–0; 69227–20–9; 69227–21–0; 69227–22–1; 69364–63–2; 70750–27–5; 70879–83–3; 70955–07–6; 71011–10–4; 71060–57–6; 71243–46–4; 72066–65–0; 72108–90–8; 72484–69–6; 72854–13–8; 72905–87–4; 73018–31–2; 73049–34–0; 74432–13–6; 74499–34–6; 78330–19–5; 78330–20–8; 78330–21–9; 78330–23–1; 79771–03–2; 84133–50–6; 85422–93–1; 97043–91–9; 97953–22–5; 102782–43–4; 103331–86–8; 103657–84–7; 103657–85–8; 103818–93–5; 103819–03–0; 106232–83–1; 111905–54–5; 116810–31–2; 116810–32–3; 116810–33–4; 120313–48–6; 120944–68–5; 121617–09–2; 126646–02–4; 126950–62–7; 127036–24–2; 139626–71–4; 152231–44–2; 154518–36–2; 157627–86–6; 157627–88–8; 157707–41–0; 157707–43–2; 159653–49–3; 160875–66–1; 160901–20–2; 160901–09–7; 160901–19–9; 161025–21–4; 161025–22–5; 166736–08–9; 169107–21–5; 172588–43–1; 176022–76–7; 196823–11–7; 287935–46–0; 288260–45–7; 303176–75–2; 954108–36–2. Aluminum sulfate 10043–01–3 ...... When ready for use, the end-use concentration is not to exceed 50 ppm

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Pesticide Chemical CAS Reg. No. Limits

2-propen-1-aminium, N,N-dimethyl-N-propenyl-, chloride, 26062–79–3 ...... When ready for use, the end-use concentration is not homopolymer to exceed 0.6% Ammonium chloride 12125–02–9 When ready for use, the end-use concentration is not to exceed 48 ppm Amylopectin, acid-hydrolyzed, 1-oxtenylbutanedioate 113894–85–2 None Amylopectin, hydrogen 1-octadecenylbutanedioate 125109–81–1 None Butryic acid ...... 107–92–6 ...... When ready for use, the end-use concentration is not to exceed 100 ppm Butyl alcohol ...... 71–36–3 ...... When ready for use, the end-use concentration is not to exceed 100 ppm n-Butyl benzoate ...... 136–60–7 ...... When ready for use, the end-use concentration is not to exceed 15,000 ppm Citral ...... 5392–40–5 ...... When ready for use, the end-use concentration is not to exceed 100 ppm Citronellol ...... 106–22–9 ...... When ready for use, the end-use concentration is not to exceed 100 ppm Citronellyl acetate ...... 150–84–5 ...... When ready for use, the end-use concentration is not to exceed 100 ppm Copper sulfate pentahydrate 7758–99–8 When ready for use, the end-use concentration is not to exceed 80 ppm b-Damascone, (Z)- ...... 23726–92–3 ...... When ready for use, the end-use concentration is not to exceed 100 ppm Decanal ...... 112–31–2 ...... When ready for use, the end-use concentration is not to exceed 100 ppm Decanoic acid ...... 334–48–5 ...... When ready for use, the end-use concentration is not to exceed 100 ppm 1-Decanol ...... 112–30–1 ...... When ready for use, the end-use concentration is not to exceed 100 ppm (E)-4-Decenal ...... 65405–70–1 ...... When ready for use, the end-use concentration is not to exceed 100 ppm D-Glucopyranose, oligomeric, decyl octyl glycosides 68515–73–1 None 2,6-Dimethyl-5-heptanal ...... 106–72–9 ...... When ready for use, the end-use concentration is not to exceed 100 ppm Di-n-butyl carbonate 542–52–9 ...... When ready for use, the end-use concentration is not to exceed 15,000 ppm 2-Dodecanol, (2E)- ...... 20407–84–5 ...... When ready for use, the end-use concentration is not to exceed 100 ppm Ethanol 64–17–5 None Ethyl 2-methylbutyrate ...... 452–79–1 ...... When ready for use, the end-use concentration is not to exceed 100 ppm Ethylenediaminetetraacetic acid (EDTA), tetrasodium salt 64–02–8 None FD&C Green No. 3 CAS Reg. No. 2353–45–9 None FD&C Red No. 40 25956–17–6 ...... When ready for use, the end-use concentration is not to exceed 20 ppm. FD&C Yellow No. 5 1934–21–0 When ready for use, the end-use concentration is not to exceed 1000 ppm (E)-Geraniol ...... 106–24–1 ...... When ready for use, the end-use concentration is not to exceed 100 ppm (E)-Geraniol acetate ...... 105–87–3 ...... When ready for use, the end-use concentration is not to exceed 100 ppm D-glucurono-6-deoxy-L-manno-D-glucan, acetate, calcium mag- (CAS No. 595585–15–2) ...... None nesium potassium sodium salt (diutan gum). Heptanal ...... 111–71–7 ...... When ready for use, the end-use concentration is not to exceed 100 ppm Heptanoic acid ...... 111–14–8 ...... When ready for use, the end-use concentration is not to exceed 100 ppm Heptyl alcohol ...... 111–70–6 ...... When ready for use, the end-use concentration is not to exceed 100 ppm Hexanal ...... 66–25–1 ...... When ready for use, the end-use concentration is not to exceed 100 ppm Hexanoic acid ...... 142–62–1 ...... When ready for use, the end-use concentration is not to exceed 100 ppm n-Hexanol ...... 111–27–3 ...... When ready for use, the end-use concentration is not to exceed 100 ppm (Z)-3-Hexenol ...... 928–96–1 ...... When ready for use, the end-use concentration is not to exceed 100 ppm (Z)-3-Hexenol acetate ...... 3681–71–8 ...... When ready for use, the end-use concentration is not to exceed 100 ppm Hexyl acetate ...... 142–92–7 ...... When ready for use, the end-use concentration is not to exceed 100 ppm Hydrogen peroxide 7722–84–1 When ready for use, the end-use concentration is not to exceed 91 ppm Hypochlorous acid, sodium salt 7681–52–9 When ready for use, the end-use concentration of all hypochlorous acid chemicals in the solution is not to exceed 200 ppm determined as total available chlorine Iodine 7553–56–2 When ready for use, the total end-use concentration of all iodide-producing chemicals in the solution is not to exceed 25 ppm of titratable iodine Lauric acid ...... 143–07–7 ...... When ready for use, the end-use concentration is not to exceed 100 ppm Lauric aldehyde ...... 112–54–9 ...... When ready for use, the end-use concentration is not to exceed 100 ppm Lauryl alcohol ...... 112–53–8 ...... When ready for use, the end-use concentration is not to exceed 100 ppm d-Limonene ...... 5989–27–5 ...... When ready for use, the end-use concentration is not to exceed 100 ppm

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Pesticide Chemical CAS Reg. No. Limits

Lipase, triacylglycerol 9001–62–1 When ready for use, the end-use concentration is not to exceed 500 ppm Magnesium oxide 1309–48–4 None Methane sulfonic acid 75–75–2 When ready for use, the end use concentration is not to exceed 5,000 ppm Methylene blue 61–73–4 When ready for use, the end-use concentration is not to exceed 0.4 ppm Methyl-a-ionone ...... 127–42–4 ...... When ready for use, the end-use concentration is not to exceed 100 ppm 3-Methyl-2-butenyl acetate ...... 1191–16–8 ...... When ready for use, the end-use concentration is not to exceed 100 ppm 2-Methylundecanal ...... 110–41–8 ...... When ready for use, the end-use concentration is not to exceed 100 ppm 2-Methyl-1,3-propanediol 2163–42–0 None Myristaldehyde ...... 124–25–4 ...... When ready for use, the end-use concentration is not to exceed 100 ppm Myristic acid ...... 544–63–8 ...... When ready for use, the end-use concentration is not to exceed 100 ppm Neryl acetate ...... 141–12–8 ...... When ready for use, the end-use concentration is not to exceed 100 ppm Nitric acid 7697–37–2 When ready for use, the end-use concentration is not to exceed 1,000 ppm Nonanal ...... 124–19–6 ...... When ready for use, the end-use concentration is not to exceed 100 ppm Nonanoic acid ...... 112–05–0 ...... When ready for use, the end-use concentration is not to exceed 100 ppm Nonyl alcohol ...... 143–08–8 ...... When ready for use, the end-use concentration is not to exceed 100 ppm a-(p-Nonylphenyl)-w-hydroxypoly (oxyethylene) average None None poly(oxyethylene) content 11 moles) Octadecanoic acid, calcium salt 1592–23–0 None 9-Octadecenoic acid (9Z)-, sulfonated, oxidized 1315321–93–7 ...... When ready for use, the end-use concentration is not to exceed 250 ppm. 9-Octadecenoic acid (9Z)-, sulfonated, oxidized, potassium salts 1315321–94–8 ...... When ready for use, the end-use concentration is not to exceed 250 ppm. 9-Octadecenoic acid (9Z)-, sulfonated, oxidized, sodium salts 1315321–95–9 ...... When ready for use, the end-use concentration is not to exceed 250 ppm. Octanal ...... 124–13–0 ...... When ready for use, the end-use concentration is not to exceed 100 ppm 1-Octanesulfonic acid, sodium salt 5324–84–5 When ready for use, the end-use concentration is not to exceed 46 ppm Octanoic acid 124–07–2 When ready for use, the end-use concentration is not to exceed 52 ppm Octanoic acid ...... 124–07–2 ...... When ready for use, the end-use concentration is not to exceed 100 ppm 1-Octanol ...... 111–87–5 ...... When ready for use, the end-use concentration is not to exceed 100 ppm Oxirane, methyl-, polymer with oxirane, minimum molecular 9003–11–6 None weight (in amu), 1900 Palmitic acid ...... 57–10–3 ...... When ready for use, the end-use concentration is not to exceed 100 ppm Peroxyacetic acid 79–21–0 When ready for use, the end-use concentration is not to exceed 58 ppm Peroxyoctanoic acid 33734–57–5 When ready for use, the end-use concentration is not to exceed 52 ppm Phosphonic acid, (1-hydroxyethylidene)bis- 2809–21–4 When ready for use, the end-use concentration is not to exceed 14 ppm Phosphoric acid, trisodium salt 7601–54–9 When ready for use, the end-use concentration is not to exceed 5916 ppm Potassium bromide 7758–02–3 When ready for use, the end-use concentration is not to exceed 46 ppm total available halogen Potassium iodide 7681–11–0 When ready for use, the total end-use concentration of all iodide-producing chemicals in the solution is not to exceed 25 ppm of titratable iodine 1,3-Propanediol 504–63–2 None Propionic acid ...... 79–09–4 ...... When ready for use, the end-use concentration is not to exceed 100 ppm Propylene glycol 57–55–6 None Quaternary ammonium compounds, alkyl (C12-C18) 8001–54–5 When ready for use, the end-use concentration of all benzyldimethyl, chlorides quaternary chemicals in the solution is not to exceed 200 ppm of active quaternary compound Quaternary ammonium compounds: n-alkyl (C12-18) dimethyl 68424–85–1 When ready for use, the end-use concentration of all benzyl ammonium chloride quaternary chemicals in solution is not to exceed 400 ppm of active quaternary compound Quaternary Ammonium Compounds: n-alkyl (C 12-14) dimethyl 85409–23–0 When ready for use, the end-use concentration of all ethylbenzyl ammonium chloride, average molecular weight (in quaternary chemicals in solution is not to exceed amu), 377 to 384 400 ppm of active quaternary compound. Quaternary ammonium compounds n-alkyl (C12-C18) dimethyl None When ready for use, the end-use concentration of all ethylbenzyl ammonium chloride average molecular weight (in quaternary chemicals in the solution is not to ex- amu) 384 ceed 200 ppm of active quaternary compound Quaternary ammonium compounds, Di-n-Alkyl (C8-10) dimethyl None When ready for use, the end-use concentration of ammonium chloride, average molecular weight (in amu) 332 these specific in quaternary ammonium compounds to 361 is not to exceed 240 ppm of active quaternary ammonium compound; the end-use concentration of all quaternary chemicals in the solution is not to exceed 400 ppm of active quaternary compound

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Pesticide Chemical CAS Reg. No. Limits

Quaternary ammonium compounds, didecyl dimethyl ammo- 148788–55–0/148812–654–1 When ready for use, the end-use concentration of nium carbonate/didecyl dimethyl ammonium bicarbonate these specific ammonium compounds is not to exceed 400 ppm of active quaternary ammonium compound Silver ions resulting from the use of electrolytically-generated 14701–21–4 When ready for use, the end-use concentration of sil- silver ions stabilized in citric acid as silver dihydrogen citrate ver ions is not to exceed 50 ppm of active silver (does not include metallic silver) Sodium bisulfate 7681–38–1 When ready for use, the end-use concentration is not to exceed 2,000 ppm. Sorbitan, mono-9-octadecenoate, poly(oxy-1,2-ethanediyl) 9005–65–6 None derivs., (Z)- Stearic acid...... 57–11–4 ...... When ready for use, the end-use concentration is not to exceed 100 ppm Sulfuric acid ...... 7664–93–9 ...... Food-contact surfaces in public eating places, dairy- processing equipment, and food-processing equipment and utensils in antimicrobial formulations. Not to exceed 600 ppm. Sulfuric acid monododecyl ester, sodium salt (sodium lauryl sul- 151–21–3 When ready for use, the end-use concentration is not fate) to exceed 350 ppm Trans-1,3,3,3-tetrafluoroprop-1-ene ...... 29118–24–9 ...... None 1,3,5-Triazine-2,4,6(1H,3H,5H)-trione, 1,3-dichloro-, sodium salt 2893–78–9 When ready for use, the end-use concentration of all di- or trichloroisocyanuric acid chemicals in the solution is not to exceed 100 ppm determined as total available chlorine 2-Tridecanal ...... 7774–82–5 ...... When ready for use, the end-use concentration is not to exceed 100 ppm 3,5,5-Trimethylhexanal ...... 5435–64–3 ...... When ready for use, the end-use concentration is not to exceed 100 ppm Undecanal ...... 112–44–7 ...... When ready for use, the end-use concentration is not to exceed 100 ppm Undecyl alcohol ...... 112–42–5 ...... When ready for use, the end-use concentration is not to exceed 100 ppm Valeraldehyde ...... 110–62–3 ...... When ready for use, the end-use concentration is not to exceed 100 ppm Valeric acid ...... 109–52–4 ...... When ready for use, the end-use concentration is not to exceed 100 ppm Xylenesulfonic acid, sodium salt 1300–72–7 When ready for use, the end-use concentration is not to exceed 500 ppm

(b) The following chemical sub- may be applied to: Dairy processing stances when used as ingredients in an equipment, and food-processing equip- antimicrobial pesticide formulation ment and utensils.

Pesticide Chemical CAS Reg. No. Limits

Acetic acid 64–19–7 When ready for use, the end-use concentration is not to exceed 1200 ppm Acetic acid, chloro-, sodium salt, reaction prod- 68608–66–2 When ready for use, the end-use concentration ucts with 4,5-dihydro-2-undecyl-1H-imidazole- is not to exceed 42 ppm chloroacetic acid 1-ethanol and sodium hydroxide Benzenesulfonic acid, dodecyl- 27176–87–0 When ready for use, the end-use concentration is not to exceed 5.5 ppm Butanedioic acid, octenyl- 28805–58–5 When ready for use, the end-use concentration is not to exceed 156 ppm Butoxy monoether of mixed (ethylene-propylene) None None polyalkylene glycol, minimum average molecular weight (in amu), 2400 Calcium chloride 10043–52–4 When ready for use, the end-use concentration is not to exceed 17 ppm n-Carboxylic acids (C6-C12), consisting of a mix- None When ready for use, the end-use concentration ture of not less than 56% octanoic acid and is not to exceed 39 ppm not less than 40% decanoic acid Decanoic acid 334–48–5 When ready for use, the end-use concentration is not to exceed 90 ppm Ethanesulfonic acid, 2-[cyclohexyl (1- 132–43–4 When ready for use, the end-use concentration oxohexadecyl) amino]-, sodium salt is not to exceed 237 ppm Ethylenediaminetetraacetic acid (EDTA), diso- 139–33–3 When ready for use, the end-use concentration dium salt is not to exceed 1400 ppm FD&C Yellow No. 5 (Tartrazine) (conforming to 1934–21–0 None 21 CFR 74.705) D-Gluconic acid, monosodium salt 527–07–1 When ready for use, the end-use concentration is not to exceed 760 ppm Hydriodic acid 10034–85–2 When ready for use, the total end-use concentration of all iodide-producing chemicals is not to exceed 25 ppm of titratable iodine Hydrogen peroxide 7722–84–1 When ready for use, the end-use concentration is not to exceed 465 ppm

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Pesticide Chemical CAS Reg. No. Limits

Hypochlorous acid 7790–92–3 When ready for use, the end-use concentration of all hypochlorous acid chemicals in the solution is not to exceed 200 ppm determined as total available chlorine Iodine 7553–56–2 When ready for use, the total end-use concentration of all iodide-producing chemicals in the solution is not to exceed 25 ppm of titratable iodine Lactic acid 50–21–5 When ready for use, the end-use concentration is not to exceed 138 ppm Nonanoic acid 112–05–0 When ready for use, the end-use concentration is not to exceed 90 ppm 1-Octanamine, N,N-dimethyl- 7378–99–6 When ready for use, the end-use concentration is not to exceed 113 ppm 1,2-Octanedisulfonic acid 113669–58–2 When ready for use, the end-use concentration is not to exceed 102 ppm 1-Octanesulfonic acid 3944–72–7 When ready for use, the end-use concentration is not to exceed 172 ppm 1-Octanesulfonic acid, sodium salt 5324–84–5 When ready for use, the end-use concentration is not to exceed 297 ppm 1-Octanesulfonic acid, 2-sulfino- 113652–56–5 When ready for use, the end-use concentration is not to exceed 102 ppm Octanoic acid 124–07–2 When ready for use, the end-use concentration is not to exceed 176 ppm Oxychloro species (including chlorine dioxide) None When ready for use, the end-use concentration generated by acidification of an aqueous solu- is not to exceed 200 ppm of chlorine dioxide tion of sodium chlorite as determined by the method titled, Iodometric Method for the Determination of Available Chlorine Dioxide (50-250 ppm available chlorine dioxide) Peroxyacetic acid 79–21–0 When ready for use, the end-use concentration is not to exceed 315 ppm Peroxyoctanoic acid 33734–57–5 When ready for use, the end-use concentration is not to exceed 122 ppm Phosphonic acid, (1-hydroxyethylidene)bis- 2809–21–4 When ready for use, the end-use concentration is not to exceed 34 ppm Phosphoric acid 7664–38–2 None Phosphoric acid, monosodium salt 7558–80–7 When ready for use, the end-use concentration is not to exceed 350 ppm Potassium iodide 7681–11–0 When ready for use, the total end-use concentration of all iodide-producing chemicals in the solution is not to exceed 25 ppm of titratable iodine Propanoic acid 79–09–4 When ready for use, the end-use concentration is not to exceed 297 ppm 2,6-Pyridinedicarboxylic acid 499–83–2 When ready for use, the end-use concentration is not to exceed 1.2 ppm Sulfuric acid monododecyl ester, sodium salt 151–21–3 When ready for use, the end-use concentration (sodium lauryl sulfate) is not to exceed 350 ppm

(c) The following chemical sub- may be applied to: Food-processing stances when used as ingredients in an equipment and utensils. antimicrobial pesticide formulation

Pesticide Chemical CAS Reg. No. Limits

Acetic acid 64–19–7 When ready for use, the end-use concentration is not to exceed 1,200 ppm Acetic acid, chloro-, sodium salt, reaction prod- 68608–66–2 When ready for use, the end-use concentration ucts with 4,5-dihydro-2-undecyl-1H-imidazole- is not to exceed 42 ppm chloroacetic acid 1-ethanol and sodium hydroxide Ammonium chloride 12125–02–9 When ready for use, the end-use concentration is not to exceed 48 ppm Benzenesulfonic acid, dodecyl- 27176–87–0 When ready for use, the end-use concentration is not to exceed 400 ppm Benzenesulfonic acid, dodecyl-, sodium salt 25155–30–0 When ready for use, the end-use concentration is not to exceed 430 ppm [1,1′-Biphenyl]-2-ol 90–43–7 When ready for use, the end-use concentration is not to exceed 400 ppm Boric acid, sodium salt 7775–19–1 None

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Pesticide Chemical CAS Reg. No. Limits

Butanedioic acid, octenyl- 28805–58–5 When ready for use, the end-use concentration is not to exceed 156 ppm Butanedioic acid, sulfo-, 1,4-dioctyl ester, so- 1639–66–3 None dium salt Butoxy monoether of mixed (ethylene-propylene) None None polyalkylene glycol, cloudpoint of 90 - 100oC in 0.5 aqueous solution, average molecular weight (in amu), 3300 Butoxy monoether of mixed (ethylene-propylene) None None polyalkylene glycol, minimum average molecular weight (in amu), 2400 Calcium chloride 10043–52–4 When ready for use, the end-use concentration is not to exceed 17 ppm n-Carboxylic acids (C6-C12), consisting of a mix- None When ready for use, the end-use concentration ture of not less than 56% octanoic acid and is not to exceed 39 ppm not less than 40% decanoic acid 3-Cyclohexene-1-methanol,a,a,4-trimethyl- 98–55–5 None 1-Decanaminium, N-decyl-N, N-dimethyl-, chlo- 7173–51–5 When ready for use, the end-use concentration ride is not to exceed 200 ppm of active quaternary compound Decanoic acid 3347–48–5 When ready for use, the end-use concentration is not to exceed 234 ppm Ethanesulfonic acid, 2-[cyclohexyl (1- 132–43–4 When ready for use, the end-use concentration oxohexadecyl) amino]-, sodium salt is not to exceed 237 ppm Ethanol 64–17–5 None Ethanol, 2 butoxy- 111–76–2 None Ethanol, 2-(2-ethoxyethoxy)- 111–90–0 None Ethylenediaminetetraacetic acid (EDTA), diso- 139–33–3 When ready for use, the end-use concentration dium salt is not to exceed 1400 ppm Ethylenediaminetetraacetic acid (EDTA), 64–02–8 None tetrasodium salt Fatty acids, coco, potassium salts 61789–30–8 None Fatty acids, tall-oil, sulfonated, sodium salts 68309–27–3 When ready for use, the end-use concentration is not to exceed 66 ppm FD&C Yellow No. 5 (Tartrazine) (conforming to 1934–21–0 None 21 CFR 74.705) D-Gluconic acid, monosodium salt 527–07–1 When ready for use, the end-use concentration is not to exceed 760 ppm Hydriodic acid 10034–85–2 When ready for use, the total end-use concentration of all iodide-producing chemicals in the solution is not to exceed 25 ppm of titratable iodine Hydrogen peroxide 7722–84–1 When ready for use, the end-use concentration is not to exceed 1100 ppm Hypochlorous acid 7790–92–3 When ready for use, the end-use concentration of all hypochlorous acid chemicals in the solution is not to exceed 200 ppm determined as total available chlorine Hypochlorous acid, calcium salt 7778–54–3 When ready for use, the end-use concentration of all hypochlorous acid chemicals in the solution is not to exceed 200 ppm determined as total available chlorine Hypochlorous acid, lithium salt 13840–33–0 When ready for use, the end-use concentration of all hypochlorous acid chemicals in the solution is not to exceed 200 ppm determined as total available chlorine and 30 ppm lithium Hypochlorous acid, potassium salt 7778–66–7 When ready for use, the end-use concentration of all hypochlorous acid chemicals in the solution is not to exceed 200 ppm determined as total available chlorine Hypochlorous acid, sodium salt 7681–52–9 When ready for use, the end-use concentration of all hypochlorous acid chemicals in the solution is not to exceed 200 ppm determined as total available chlorine Iodine 7553–56–2 When ready for use, the total end-use concentration of all iodide-producing chemicals in the solution is not to exceed 25 ppm of titratable iodine Lactic acid 50–21–5 None Magnesium oxide 1309–48–4 None Methylene blue 61–73–4 When ready for use, the end-use concentration is not to exceed 0.4 ppm Neodecanoic acid 26896–20–8 When ready for use, the end-use concentration is not to exceed 174 ppm

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Pesticide Chemical CAS Reg. No. Limits

Nonanoic acid 112–05–0 When ready for use, the end-use concentration is not to exceed 90 ppm a-(p-Nonylphenyl)-w-hydroxypoly (oxyethylene) None None maximum average molecular weight (in amu), 748 a-(p-Nonylphenol)-w-hydroxypoly (oxyethylene) None None average poly(oxyethylene) content 11 moles a-(p-Nonylphenyl)-w-hydroxypoly (oxyethylene) None None produced by the condensation of 1 mole p- nonylphenol with 9 to 12 moles ethylene oxide a-(p-Nonylphenyl)-w-hydroxypoly (oxyethylene), None None 9 to 13 moles ethylene oxide Octadecanoic acid, calcium salt 1592–23–0 None 9-Octadecenoic acid (9Z)-, sulfonated 68988–76–1 When ready for use, the end-use concentration is not to exceed 312 ppm 9-Octadecenoic acid (9Z)-sulfonated, sodium 68443–05–0 When ready for use, the end-use concentration salts is not to exceed 200 ppm 1-Octanamine, N,N-dimethyl- 7378–99–6 When ready for use, the end-use concentration is not to exceed 113 ppm 1,2-Octanedisulfonic acid 113669–58–2 When ready for use, the end-use concentration is not to exceed 102 ppm 1-Octanesulfonic acid 3944–72–7 When ready for use, the end-use concentration is not to exceed 172 ppm 1-Octanesulfonic acid, sodium salt 5324–84–5 When ready for use, the end-use concentration is not to exceed 312 ppm 1-Octanesulfonic acid, 2-sulfino- 113652–56–5 When ready for use, the end-use concentration is not to exceed 102 ppm Octanoic acid 124–07–2 When ready for use, the end-use concentration is not to exceed 234 ppm Oxirane, methyl-, polymer with oxirane, min- 9003–11–6 None imum molecular weight (in amu), 1900 Oxirane, methyl-, polymer with oxirane, block, 106392–12–5 None average molecular weight (in amu), 1900 Oxirane, methyl-, polymer with oxirane, block, None None minimum average molecular weight (in amu), 2000 Oxirane, methyl-, polymer with oxirane, block, None None 27 to 31 moles of polyoxypropylene, average molecular weight (in amu) 2000 Oxychloro species (predominantly chlorite, chlo- None When ready for use, the end-use concentration rate and chlorine dioxide in an equilibrium is not to exceed 200 ppm of chlorine dioxide mixture) generated either (i) by directly meter- as determined by the method titled, ing a concentrated chlorine dioxide solution ‘‘Iodometric Method for the Determination of prepared just prior to use, into potable water, Available Chlorine Dioxide (50-250 ppm or (ii) by acidification of an aqueous alkaline available chlorine dioxide)’’ solution of oxychloro species (predominately chlorite and chlorate) followed by dilution with potable water Oxychloro species (including chlorine dioxide) None When ready for use, the end-use concentration generated by acidification of an aqueous solu- is not to exceed 200 ppm of chlorine dioxide tion of sodium chlorite as determined by the method titled, ‘‘Iodometric Method for the Determination of Available Chlorine Dioxide (50-250 ppm available chlorine dioxide)’’ 2,4-Pentanediol, 2-methyl- 107–41–5 None Peroxyacetic acid 79–21–0 When ready for use, the end-use concentration is not to exceed 315 ppm Peroxyoctanoic acid 33734–57–5 When ready for use, the end-use concentration is not to exceed 122 ppm Phenol, 4-chloro-2-(phenylmethyl)- 120–32–1 When ready for use, the end-use concentration is not to exceed 320 ppm Phenol, 4-(1,1-dimethylpropyl)- 80–46–6 When ready for use, the end-use concentration is not to exceed 80 ppm Phosphonic acid, (1-hydroxyethylidene)bis- 2809–21–4 When ready for use, the end-use concentration is not to exceed 34 ppm Phosphoric acid 7664–38–2 None Phosphoric acid, monosodium salt 7558–80–7 When ready for use, the end-use concentration is not to exceed 350 ppm Phosphoric acid, trisodium salt 7601–54–9 When ready for use, the end-use concentration is not to exceed 5916 ppm Poly(oxy-1,2-ethanediyl), a-[(1,1,3,3- None None tetramethylbutyl) phenyl]-w-hydroxy-, produced with one mole of the phenol and 4 to 14 moles ethylene oxide

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Pesticide Chemical CAS Reg. No. Limits

Potassium bromide 7758–02–3 When ready for use, the end-use concentration of all bromide-producing chemicals in the solution is not to exceed 200 ppm total available halogen Potassium iodide 7681–11–0 When ready for use, the total end-use concentration of all iodide-producing chemicals in the solution is not to exceed 25 ppm of titratable iodine Propanoic acid 79–09–4 When ready for use, the end-use concentration is not to exceed 297 ppm 2,6-Pyridinedicarboxylic acid 499–83–2 When ready for use, the end-use concentration is not to exceed 1.2 ppm

Quaternary ammonium compounds, alkyl (C12- 8001–54–5 When ready for use, the end-use concentration C18) benzyldimethyl, chlorides of this specific quaternary compound is not to exceed 200 ppm within the end-use total concentration that is not to exceed 400 ppm active quaternary compound

Quaternary ammonium compounds, n-alkyl (C12- None When ready for use, the end-use concentration C14) dimethyl ethylbenzyl ammonium chloride, of this specific quaternary compound is not average molecular weight (in amu), 377 to to exceed 200 ppm within the end-use total 384 concentration that is not to exceed 400 ppm active quaternary compound

Quaternary ammonium compounds, n-alkyl (C12- None When ready for use, the end-use concentration C18) dimethyl ethylbenzyl ammonium chloride of this specific quaternary compound is not average molecular weight (in amu) 384 to exceed 200 ppm within the end-use total concentration that is not to exceed 400 ppm active quaternary compound Quaternary ammonium compounds, di-n-Alkyl None When ready for use, the end-use concentration (C8-C10) dimethyl ammonium chloride, aver- of this specific quaternary compound is not age molecular weight (in amu), 332 to 361 to exceed 240 ppm within the end-use total concentration that is not to exceed 400 ppm active quaternary compound

Sodium-a-alkyl(C12-C15)-w-hydroxypoly (oxy- None None ethylene) sulfate with the poly(oxyethylene) content averaging one mole Sodium bromide 7647–15–6 When ready for use, the end-use concentration of all bromide-producing chemicals in the solution is not to exceed 200 ppm total available halogen Sodium iodide 7681–82–5 When ready for use, the total end-use concentration of all iodide-producing chemicals in the solution is not to exceed 25 ppm of titratable iodine Sulfuric acid monododecyl ester, sodium salt 151–21–3 None (sodium lauryl sulfate) 1,3,5-Triazine-2,4,6(1H,3H,5H)-trione, 1,3- 2782–57–2 When ready for use, the end-use concentration dichloro- of all di- or trichloroisocyanuric acid chemicals in the solution is not to exceed 100 ppm determined as total available chlorine 1,3,5-Triazine-2,4,6(1H,3H,5H)-trione, 1,3- 2244–21–5 When ready for use, the end-use concentration dichloro-, potassium salt of all di- or trichloroisocyanuric acid chemicals in the solution is not to exceed 100 ppm determined as total available chlorine 1,3,5-Triazine-2,4,6(1H,3H,5H)-trione, 1,3- 2893–78–9 When ready for use, the end-use concentration dichloro-, sodium salt of all di- or trichloroisocyanuric acid chemicals in the solution is not to exceed 100 ppm determined as total available chlorine 1,3,5-Triazine-2,4,6(1H,3H,5H)-trione, 1,3,5- 87–90–1 When ready for use, the end-use concentration trichloro- of all di- or trichloroisocyanuric acid chemicals in the solution is not to exceed 100 ppm determined as total available chlorine 1,3,5-Triazine, N,N′,N″-trichloro-2,4,6-triamino- 7673–09–8 When ready for use, the end-use concentration of all di- or trichloroisocyanuric acid chemicals in the solution is not to exceed 200 ppm determined as total available chlorine

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[69 FR 23136, Apr. 28, 2004, as amended at 71 FR 30811, May 31, 2006; 71 FR 45423, Aug. 9, 2006; 71 FR 46125, Aug. 11, 2006; 72 FR 51186, Sept. 6, 2007; 73 FR 37858, July 2, 2008; 73 FR 49107, Aug. 20, 2008; 73 FR 53725, Sept. 17, 2008; 74 FR 27454, June 10, 2009; 74 FR 38944, Aug. 5, 2009; 74 FR 40509, Aug. 12, 2009; 75 FR 40735, July 14, 2010; 76 FR 55267, Sept. 7, 2011; 77 FR 45498, Aug. 1, 2012; 77 FR 50617, Aug. 22, 2012; 77 FR 53150, Aug. 31, 2012; 77 FR 68692, Nov. 16, 2012; 78 FR 35147, June 12, 2013; 78 FR 46264, July 31, 2013; 78 FR 48621, Aug. 9, 2013; 78 FR 59269, Sept. 26, 2013; 78 FR 65565, Nov. 1, 2013; 78 FR 67042, Nov. 8, 2013; 78 FR 78731, Dec. 27, 2013; 79 FR 6096, Feb. 3, 2014; 79 FR 26152, May 7, 2014; 79 FR 32666, June 6, 2014; 79 FR 33473, June 11, 2014; 79 FR 52993, Sept. 5, 2014; 79 FR 66312, Nov. 7, 2014; 80 FR 11593, Mar. 4, 2015; 80 FR 28842, May 20, 2015; 80 FR 32033, 32038, June 5, 2015; 80 FR 34070, June 15, 2015; 80 FR 48752, Aug. 14, 2015; 80 FR 50211, Aug. 19, 2015; 80 FR 61122, Oct. 9, 2015; 80 FR 62466, Oct. 16, 2015; 81 FR 38100, 38104, June 13, 2016]

§ 180.950 Tolerance exemptions for processed forms of peanuts, tree nuts, minimal risk active and inert ingre- milk, soybeans, eggs, fish, crustacea, dients. and wheat. Meat meal is an animal feed Unless specifically excluded, residues composed of dried animal fat and pro- resulting from the use of the following tein that has been sterilized. Other substances as either an inert or an ac- than meat meal, the term animal feed tive ingredient in a pesticide chemical item does not extend to any item de- formulation, including antimicrobial signed to be fed to animals that con- pesticide chemicals, are exempted from tains, to any extent, components of the requirement of a tolerance under animals. Included within the term ani- FFDCA section 408, if such use is in ac- mal feed items are: cordance with good agricultural or (1) The hulls and shells of the com- manufacturing practices. modities specified in paragraph (a) Commonly consumed food commod- (a)(2)(ii) of this section, and cocoa ities. Commonly consumed food com- bean. (2) Bird feed such as canary seed. modities means foods that are com- (3) Any feed component of a medi- monly consumed for their nutrient cated feed meeting the definition of an properties. The term commonly con- animal feed item. sumed food commodities shall only (c) Edible fats and oils. Edible fats and apply to food commodities (whether a oils means all edible (food or feed) fats raw agricultural commodity or a proc- and oils, derived from either plants or essed commodity) in the form the com- animals, whether or not commonly modity is sold or distributed to the consumed, including products derived public for consumption. from hydrogenating (food or feed) oils, (1) Included within the term com- or liquefying (food or feed) fats. monly consumed food commodities are: (1) Included within the term edible (i) Sugars such as sucrose, lactose, fats and oils are oils (such as soybean dextrose and fructose, and invert sugar oil) that are derived from the commod- and syrup. ities specified in paragraph (a)(2)(ii) of (ii) Spices such as cinnamon, cloves, this section when such oils are highly and red pepper. refined via a solvent extraction proce- (iii) Herbs such as basil, anise, or dure. fenugreek. (2) Excluded from the term edible (2) Excluded from the term com- fats and oils are plant oils used in the monly consumed food commodities are: pesticide chemical formulation specifi- (i) Any food commodity that is adul- cally to impart their characteristic terated under 21 U.S.C. 342. fragrance and/or flavoring. (ii) Both the raw and processed forms (d) [Reserved] of peanuts, tree nuts, milk, soybeans, (e) Specific chemical substances. Resi- eggs, fish, crustacea, and wheat. dues resulting from the use of the fol- (iii) Alcoholic beverages. lowing substances as either an inert or (iv) Dietary supplements. an active ingredient in a pesticide (b) Animal feed items. Animal feed chemical formulation, including anti- items means meat meal and all items microbial pesticide chemicals, are ex- derived from field crops that are fed to empted from the requirement of a tol- livestock excluding both the raw and erance under FFDCA section 408, if

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such use is in accordance with good ag- Chemical CAS No. ricultural or manufacturing practices. Coffee grounds ...... 68916–18–7 Chemical CAS No. Dextrins ...... 9004–53–9 1,3-Dioxolan-2-one, 4-methyl-(propylene car- Acetic acid, sodium salt ...... 127–09–3 bonate) ...... 108–32–7 Alpha-cyclodextrin ...... 10016–20–3 Fumaric acid ...... 110–17–8 Amylopectin, acid-hydrolyzed, 1- Gamma-cyclodextrin ...... 17465–86–0 octenylbutanedioate ...... 113894–85– Gellan gum ...... 71010–52–1 2 D-Glucitol (sorbitol) ...... 50–70–4 Amylopectin, hydrogen 1- Glycerol (glycerin) (1,2,3-propanetriol) ...... 56–81–5 octadecenylbutanedioate ...... 125109–81– Guar gum ...... 9000–30–0 1 Humic acid ...... 1413–93–6 Animal glue ...... None Humic acid, potassium salt ...... 68514–28–3 Ascorbic acid (vitamin C) ...... 50–81–7 Humic acid, sodium salt ...... 68131–04–4 Beeswax ...... 8012–89–3 Lactic acid, n-butyl ester ...... 138–22–7 Benzoic acid, sodium salt ...... 532–32–1 Lactic acid, n-butyl ester, (S) ...... 34451–19–9 Beta-cyclodextrin ...... 7585–39–9 Lactic acid, ethyl ester ...... 97–64–3 Carbonic acid, monopotassium salt ...... 298–14–6 Lactic acid, ethyl ester,(S) ...... 687–47–8 Carbonic acid, monosodium salt (sodium bicar- Lanolin ...... 8006–54–0 bonate) ...... 144–55–8 Carnauba wax ...... 8015–86–9 Lecithins ...... 8002–43–5 Carob gum (locust bean gum) ...... 9000–40–2 Lecithins, soya ...... 8030–76–0 Castor oil ...... 8001–79–4 Licorice Extract ...... 68916–91–6 Castor oil, hydrogenated ...... 8001–78–3 Maltodextrin ...... 9050–36–6 Cellulose ...... 9004–34–6 Paper ...... None Cellulose acetate ...... 9004–35–7 Potassium chloride ...... 7447–40–7 Cellulose, carboxy methyl ether, sodium salt ... 9004–32–4 2-Propanol (isopropyl alcohol) ...... 67–63–0 Cellulose, 2-hydroxyethyl ether ...... 9004–62–0 Red cabbage color, expressed from edible red Cellulose, 2-hydroxypropyl ether ...... 9004–64–2 cabbage heads via a pressing process using Cellulose, 2-hydroxypropyl methyl ether ...... 9004–65–3 only acidified water ...... None Cellulose, methyl ether ...... 9004–67–5 Silica, amorphous, fumed (crystalline free) ...... 112945–52– Cellulose, mixture with cellulose carboxymethyl 5 ether, sodium salt ...... 51395–75–6 Silica, amorphous, precipitated and gel ...... 7699–41–4 Cellulose, pulp ...... 65996–61–4 Silica gel ...... 63231–67–4 Cellulose, regenerated ...... 68442–85–3 Silica gel, precipitated, crystalline-free ...... 112926–00– Citric acid ...... 77–92–9 8 Citric acid, 2-(acetyloxy)-, tributyl ester ...... 77–90–7 Silica, hydrate ...... 10279–57–9 Citric acid, calcium salt ...... 7693–13–2 Silica, vitreous ...... 60676–86–0 Citric acid, calcium salt (2:3) ...... 813–94–5 Soap (The water soluble sodium or potassium Citric acid, dipotassium salt ...... 3609–96–9 salts of fatty acids produced by either the Citric acid, disodium salt ...... 144–33–2 saponification of fats and oils, or the neutral- Citric acid, monohydrate ...... 5949–29–1 ization of fatty acid) ...... None Citric acid, monopotassium salt ...... 866–83–1 Sorbic acid, potassium salt ...... 24634–61–5 Citric acid, monosodium salt ...... 18996–35–5 Soapbark (Quillaja saponin) ...... 1393–03–9 Citric acid, potassium salt ...... 7778–49–6 Sodium alginate ...... 9005–38–3 Citric acid, triethyl ester ...... 77–93–0 Sodium chloride ...... 7647–14–5 Citric acid, tripotassium salt ...... 866–84–2 Syrups, hydrolyzed starch, hydrogenated ...... 68425–17–2 Citric acid, tripotassium salt, monohydrate ...... 6100–05–6 Ultramarine blue (C.I. Pigment Blue 29) ...... 57455–37–5 Citric acid, sodium salt ...... 994–36–5 Urea ...... 57–13–6 Citric acid, trisodium salt ...... 68–04–2 Vanillin ...... 121–33–5 Citric acid, trisodium salt, dihydrate ...... 6132–04–3 Xanthan gum ...... 11138–66–2 Citric acid, trisodium salt, pentahydrate ...... 6858–44–2

[67 FR 36537, May 24, 2002]

EDITORIAL NOTE: For FEDERAL REGISTER citations affecting § 180.950, see the List of CFR Sections Affected, which appears in the Finding Aids section of the printed volume and at www.fdsys.gov.

§ 180.960 Polymers; exemptions from dient in a pesticide chemical formula- the requirement of a tolerance. tion, including antimicrobial pesticide Residues resulting from the use of chemical formulations, are exempted the following substances, that meet the from the requirement of a tolerance definition of a polymer and the criteria under FFDCA section 408, if such use is specified for defining a low-risk poly- in accordance with good agricultural or mer in 40 CFR 723.250, as an inert ingre- manufacturing practices.

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Polymer CAS No.

Acetic acid ethenyl ester, polymer with ethane, ethenyltriethoxysilane and so- 913187–38–9 dium ethenesulfonate (1:1); minimum number average molecular weight (in amu), 16,200

Acetic acid ethenyl ester, polymer with ethenol and (a)-2-propenyl-(w)- 137091–12–4 hydroxypoly (oxy-1,2-ethanediyl) minimum number average molecular weight (in amu), 15,000

Acetic acid ethenyl ester, polymer with 1-ethenyl-2-pyrrolidinone 25086–89–9

Acetic acid ethenyl ester, polymer with oxirane, minimum number average mo- 25820–49–9 lecular weight (in amu), 17,000

Acetic acid ethenyl ester, polymer with sodium 2-methyl-2-[(1-oxo-2-propen-1- 924892–37–5 yl)amino]-1-propanesulfonate (1:1), hydrolyzed, minimum number average molecular weight (in amu), 61,000

Acrylic acid-benzyl methacrylate-1-propanesulfonic acid, 2-methyl-2-[(1-oxo-2- 1152297–42–1 propenyl)amino]-, monosodium salt, minimum number average molecular weight (in amu), 1500

Acrylic acid, polymerized, and its ethyl and methyl esters None

Acrylic acid-sodium acrylate-sodium-2-methylpropanesulfonate copolymer, min- 97953–25–8 imum average molecular weight (in amu), 4,500

Acrylic acid-stearyl methacrylate copolymer, minimum number average molec- 27756–15–6 ular weight (in amu), 2,500

Acrylic acid, styrene, a-methyl styrene copolymer, ammonium salt, minimum 89678–90–0 number average molecular weight (in amu), 1,250

Acrylic acid terpolymer, partial sodium salt, minimum number average molec- 151006–66–5 ular weight (in amu), 2,400

Acrylic polymers composed of one or more of the following monomers: Acrylic None acid, methyl acrylate, ethyl acrylate, butyl acrylate, hydroxyethyl acrylate, hydroxypropyl acrylate, hydroxybutyl acrylate, carboxyethyl acrylate, methacrylic acid, methyl methacrylate, ethyl methacrylate, butyl methacrylate, isobutyl methacrylate, hydroxyethyl methacrylate, hydroxypropyl methacrylate, hydroxybutyl methacrylate, lauryl methacrylate, and stearyl methacrylate; with none and/or one or more of the following monomers: Acrylamide, N-methyl acrylamide, N,N-dimethyl acrylamide, N-octylacrylamide, maleic anhydride, maleic acid, monoethyl maleate, diethyl maleate, monooctyl maleate, dioctyl maleate; and their corresponding sodium, potassium, ammonium, isopropylamine, triethylamine, monoethanolamine, and/or triethanolamine salts; the resulting polymer having a minimum number average molecular weight (in amu), 1,200

Acrylonitrile-butadiene copolymer conforming to 21 CFR 180.22, minimum aver- 9003–18–3 age molecular weight (in amu), 1,000

Acrylonitrile-styrene-hydroxypropyl methacrylate copolymer, minimum number None average molecular weight (in amu), 447,000

a-alkyl (C12–C15) - w- hydroxypoly(oxypropylene)poly(oxyethylene)copolymers 68551–13–3 (where the poly(oxypropylene) content is 3–60 moles and the poly(oxyethylene) content is 5–80 moles), the resulting ethoxylated propoxylated (C12–C15) alcohols having a minimum molecular weight (in amu), 1,500

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Polymer CAS No.

a-alkyl-w-hydroxypoly (oxypropylene) and/or poly (oxyethylene) polymers where 9002–92–0; 9004–95–9; 9004–98–2; 9005– the alkyl chain contains a minimum of six carbons and a minimum number 00–9; 9035–85–2; 9038–29–3; 9038–43–1; average molecular weight (in amu) 1,100. 9040–05–5; 9043–30–5; 9087–53–0; 25190–05–0; 24938–91–8; 25231–21–4; 251553–55–6; 26183–52–8; 26468–86–0; 26636–39–5; 27252–75–1; 27306–79–2; 31726–34–8; 34398–01–1; 34398–05–5; 37251–67–5; 37311–00–5; 37311–01–6; 37311–02–7; 37311–04–9; 39587–22–9; 50861–66–0; 52232–09–4; 52292–17–8; 52609–19–5; 57679–21–7; 59112–62–8; 60828–78–6; 61702–78–1; 61725–89–1; 61791–13–7; 61791–20–6; 61791–28–4; 61804–34–0; 61827–42–7; 61827–84–7; 62648–50–4; 63303–01–5; 63658–45–7; 63793–60–2; 64366–70–7; 64415–24–3; 64415–25–4; 64425–86–1; 65104–72–5; 65150–81–4; 66455–14–9: 66455–15–0; 67254–71–1; 67763–08–0; 68002–96–0; 68002–97–1; 68131–39–5; 68131–40–8; 68154–96–1; 68154–97–2; 68154–98–3; 68155–01–1; 68213–23–0; 68213–24–1; 68238–81–3; 68238–82–4; 68409–58–5; 68409–59–6; 68439–30–5; 68439–45– 2;68439–46–3; 68439–48–5; 68439–49–6; 68439–50–9; 68439–51–0; 68439–53–2; 68439–54–3; 68458–88–8; 68526–94–3; 68526–95–4; 68551–12–2; 68551–13–3; 68551–14–4; 68603–20–3; 68603–25–8; 68920–66–1; 68920–69–4; 68937–66–6; 68951–67–7; 68954–94–9; 68987–81–5; 68991–48–0; 69011–36–5; 69013–18–9; 69013–19–0; 69227–20–9; 69227–21–0; 69227–22–1; 69364–63–2; 70750–27–5; 70879–83–3; 70955–07–6; 71011–10–4; 71060–57–6; 71243–46–4; 72066–65–0; 72108–90–8; 72484–69–6; 72854–13–8; 72905–87–4; 73018–31–2; 73049–34–0; 74432–13–6; 74499–34–6; 78330–19–5; 78330–20–8; 78330–21–9; 78330–23–1; 79771–03–2; 84133–50–6; 85422–93–1; 97043–91–9; 97953–22–5; 102782–43–4; 103331–86–8; 103657–84–7; 103657–85–8; 103818–93–5; 103819–03–0; 106232–83–1; 111905–54–5; 116810–31–2; 116810–32–3; 116810–33–4; 120313–48–6; 120944–68–5; 121617–09–2; 126646–02–4; 126950–62–7; 127036–24–2; 139626–71–4; 152231–44–2; 154518–36–2; 157627–86–6; 157627–88–8; 157707–41–0; 157707–43–2; 159653–49–3; 160875–66–1; 160901–20–2; 160901–09–7; 160901–19–9; 161025–21–4; 161025–22–5; 166736–08–9; 169107–21–5; 172588–43–1; 176022–76–7; 196823–11–7; 287935–46–0; 288260–45–7; 303176–75–2; 954108–36–2. 2H-Azepin-2-one, 1-ethenylhexahydro-, homopolymer 25189–83–7

1,3 Benzene dicarboxylic acid, 5-sulfo-, 1,3-dimethyl ester, sodium salt, poly- 212842–88–1 mer with 1,3-benzene dicarboxylic acid, 1,4-benzene dicarboxylic acid, dimethyl 1,4-benzene dicarboxylate and 1,2-ethanediol, minimum number average molecular weight (in amu), 2,580

3,5-Bis(6-isocyanatohexyl)-2H-1,3,5-oxadiazine-2,4,6-(3H,5H)-trione, polymer 87823–33–4 with diethylenetriamine, minimum number average molecular weight (in amu), 1,000,000

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Polymer CAS No.

Polymer of one or more diglycidyl ethers of bisphenol A, resorcinol, glycerol, None cyclohexanedimethanol, neopentyl glycol, and polyethylene glycol with one or more of the following: Polyoxypropylene diamine, polyoxypropylene triamine, N-aminoethyl-piperazine, trimethyl-1,6-hexanediamine isophorone diamine, N,N-dimethyl-1,3-diaminopropane, nadic methyl anhydride, 1,2-cyclohexane- dicarboxylic anhydride and 1,2,3,6-tetrahydrophthalic anhydride, minimum number average molecular weight (in amu), 400,000

Butadiene-styrene copolymer None

Butanedioic acid, 2-methylene-, homopolymer, sodium salt, minimum number 26099–89–8 average molecular weight (in amu), 3936

Butanedioic acid, 2-methylene-, polymer with 2,5-furandione, sodium and am- 556055–76–6 monium salts, hydrogen peroxide-initiated, minimum number average molec- 701908–99–8 ular weight (in amu), 2,500–3,000

1,4-Butanediol-methylenebis(4-phenylisocyanate)-poly(tetramethylene glycol) 9018–04–6 copolymer, minimum molecular weight (in amu) 158,000

Butene, homopolymer 9003–29–6

2-butenedioic acid (2Z)-, monobutyl ester, polymer with methoxyethene, sodium 205193–99–3 salt, minimum number average molecular weight (in amu), 18,200

2-Butenedioic acid (Z)-, polymer with ethenol and ethenyl acetate, sodium salt, 139871–83–3 minimum number average molecular weight (in amu), 75,000

Butyl acrylate-vinyl acetate-acrylic acid copolymer, minimum number average 65405–40–5 molecular weight (in amu), 18,000

Carbonic acid, diethyl ester, polymer with a-hydro-w-hydroxypoly[oxy(methyl- 1147260–65–8 1,2-ethanediyl)] ether with 2-ethyl-2-(hydroxymethyl)-1,3-propanediol (3:1), ester with a-[[[[5-(carboxyamino)-1,3,3- trimethylcyclohexyl]methyl]amino]carbonyl]-w-methoxypoly(oxy-1,2- ethanediyl), minimum number average molecular weight (in amu), 1,900

Castor oil, ethoxylated, dioleate, minimum number average molecular weight (in 110531–96–9 amu), 1260.

Castor oil, ethoxylated, oleate, minimum number average molecular weight (in 220037–02–5 amu), 1,600

Castor oil, polymer with adipic acid, linoleic acid, oleic acid and ricinoleic acid, 1357486–09–9 minimum number average molecular weight (in amu), 3,500

Castor oil, polyoxyethylated; the poly(oxyethylene) content averages 5–54 None moles

Cellulose carboxymethyl ether, potassium salt, minimum number average mo- 54848–04–3 lecular weight 9587 Daltons

Chlorinated polyethylene 64754–90–1

Cross-linked nylon-type polymer formed by the reaction of a mixture of None sebacoyl chloride and polymethylene polyphenylisocycanate with a mixture of ethylenediamine and diethylenetriamine

Cross-linked polyurea-type encapsulating polymer None

D-Glucitol, polymer with decanedioic acid, docosanoate, minimum number av- 943440–33–3 erage molecular weight (in amu) 1,100. D-Glucitol, polymer with decanedioic acid, docosanoate, minimum number av- 1681043–28–6 erage molecular weight (in amu) 1,100. D-Glucitol, polymer with decanedioic acid, octadecanoate, minimum number av- 68562–93–6 erage molecular weight (in amu) 1,100. D-Glucitol, polymer with decanedioic acid and 1,3-propanediol, minimum num- 1681043–31–1 ber average molecular weight (in amu) 1,100. D-Glucitol, polymer with decanedioic acid and 1,3-propanediol, octadecanoate, 1681043–33–3 minimum number average molecular weight (in amu) 1,100. Dimethylpolysiloxane minimum number average molecular weight (in amu), 63148–62–9 6,800

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Polymer CAS No.

Dimethyl silicone polymer with silica, minimum number average molecular 67762–90–7 weight (in amu), 1,100,000

a-(o,p-Dinonylphenyl)-w-hydroxypoly(oxyethylene) produced by condensation of 9014–93–1 1 mole of dinonylphenol (nonyl group is a propylene trimer isomer) with an average of 140-160 moles of ethylene oxide

Docosyl methacrylate-acrylic acid copolymer, or docosyl methacrylate-octadecyl None methacrylate-acrylic acid copolymer, minimum number average molecular weight (in amu), 3,000

1,12-Dodecanediol dimethacrylate polymer, minimum molecular weight (in None amu), 100,000

a-(p-Dodecylphenyl)-w-hydroxypoly(oxyethylene) produced by the condensation 9014–92–0 of 1 mole of dodecylphenol (dodecyl group is a propylene tetramer isomer) 26401–47–8 with an average of 30-70 moles of ethylene oxide

1,2-Ethanediamine, N1-(2-aminoethyl)-, polymer with 2,4-diisocyanato-1- 35297–61–1 methylbenzene, minimum number average molecular weight (in amu), one million

1, 2-Ethanediamine, polymer with methyl oxirane and oxirane, minimum num- 26316–40–5 ber average molecular weight (in amu), 1,100

Ethylene glycol dimethyacrylate-lauryl methacrylate copolymer, minimum mo- None lecular weight (in amu), 100,000

Ethylene glycol dimethacrylate polymer, minimum molecular weight (in amu), None 100,000

Fatty acids, C18-unsatd., dimers, polymers with docosanoic acid and sorbitol, 1685270–83–0 minimum number average molecular weight (in amu) 1,100

Fatty acids, C18-unsatd., dimers, polymers with docosenoic acid and sorbitol, 1685271–02–6 minimum number average molecular weight (in amu) 1,100

Fatty acids, C18-unsatd., dimers, polymers with docosenoic acid, 1,3- 1685271–04–8 propanediol and sorbitol, minimum number average molecular weight (in amu) 1,100

Fatty acids, C18-unsatd., dimers, polymers with docosanoic acid, 1,3- 1685270–84–1 propanediol and stearic acid, minimum number average molecular weight (in amu) 1,100

Fatty acids, C18-unsatd., dimers, polymers with 1,3-propanediol, sorbitol and 1685271–01–5 stearic acid

Fatty acids, C18-unsatd., dimers, polymers with sorbitol and stearic acid, min- 1685270–99–8 imum number average molecular weight (in amu) 1,100

Fatty acids, C18-unsatd., dimers, polymers with ethylenediamine and stearyl al- 363162–42–9 cohol, minimum number average molecular weight (in amu) 1,400

Fatty acids, C18-unsatd., dimers, hydrogenated, polymers with ethylenediamine, 678991–29–2 neopentyl glycol and stearyl alcohol, minimum number average molecular weight (in amu) 1,400

Fatty acids, C18-unsatd., dimers, hydrogenated, polymers with ethylenediamine 951153–32–5 and stearyl alcohol, minimum number average molecular weight (in amu) 1,400

Fatty acids, C18-unsatd., dimers, polymers with 1-docosanol and ethylene- 1699751–19–3 diamine, minimum number average molecular weight (in amu) 1,400

Fatty acids, C18-unsatd., dimers, polymers with cetyl alcohol, neopentyl glycol 1699751–23–9 and trimethylenediamine, minimum number average molecular weight (in amu) 1,400

Fatty acids, C18-unsatd., dimers, polymers with hexamethylenediamine and ste- 1699751–24–0 aryl alcohol, minimum number average molecular weight (in amu) 1,400

Fatty acids, C18-unsatd., dimers, hydrogenated, polymers with cetyl alcohol and 1699751–25–1 ethylenediamine, minimum number average molecular weight (in amu) 1,400

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Polymer CAS No.

Fatty acids, C18-unsatd., dimers, hydrogenated, polymers with neopentyl glycol, 1699751–28–4 stearyl alcohol and trimethylenediamine, minimum number average molecular weight (in amu) 1,400

Fatty acids, C18-unsatd., dimers, polymers with 1-docosanol and 1699751–29–5 trimethylenediamine, minimum number average molecular weight (in amu) 1,400

Fatty acids, C18-unsatd., dimers, polymers with 1-docosanol, 1699751–31–9 hexamethylenediamine and neopentyl glycol, minimum number average molecular weight (in amu) 1,400

Fatty acids, C18-unsatd., dimers, polymers with docosanoic acid, 1,3- 1685271–04–8 propanediol and sorbitol, minimum number average molecular weight (in amu) 1,400

Fatty acids, tall-oil, ethoxylated propoxylated, minimum number average molec- 67784–86–5 ular weight (in amu), 2,009

Formaldehyde, polymer with a-[bis(1-phenylethyl)phenyl]-w-hydroxypoly(oxy- 157291–93–5 1,2-ethanediyl), number average molecular weight (in amu), 1,803

Formaldehyde, polymer with 2-methyloxirane and 4-nonylphenol, minimum 37523–33–4 number average molecular weight (in amu), 4,000

Fumaric acid-isophthalic acid-styrene-ethylene/propylene glycol copolymer, min- None imum average molecular weight (in amu), 1 × 1018

2,5-Furandione, polymer with ethenylbenzene, hydrolyzed, 3- 1062609–13–5 (dimethylamino)propyl imide, imide with polyethylene-polypropylene glycol 2- aminopropyl me ether, 2,2′-(1,2-diazenediyl)bis[2-methylbutanenitrile]-initiated, minimum number average molecular weight (in amu), 5,816

2,5-Furandione, polymer with ethenylbenzene, reaction products with poly- 162568–32–3 ethylene-polypropylene glycol 2-aminopropyl Me ether; minimum number average molecular weight (in amu), 14,000

2,5-Furandione, polymer with methoxyethene, butyl ethyl ester, sodium salt, 1471342–08–1 minimum number average molecular weight (in amu), 18,200

Hexadecyl acrylate-acrylic acid copolymer, hexadecyl acrylate-butyl acrylate- None acrylic acid copolymer, or hexadecyl acrylate-dodecyl acrylate-acrylic acid copolymer, minimum number average molecular weight (in amu), 3,000

Hexamethyl disilizane, reaction product with silica, minimum number average 68909–20–6 molecular weight (in amu), 645,000

1,6-Hexanediol dimethyacrylate polymer, minimum molecular weight (in amu), None 100,000

a-Hydro-w-hydroxy-poly(oxyethylene) C8 alkyl ether citrates, poly(oxyethylene) 330977–00–9 content is 4–12 moles, minimum number average molecular weight (in amu) 1,300

a-Hydro-w-hydroxy-poly(oxyethylene) C10–C16-alkyl ether citrates, 330985–58–5 poly(oxyethylene) content is 4–12 moles, minimum number average molecular weight (in amu) 1,100

a-Hydro-w-hydroxy-poly(oxyethylene) C16–C18-alkyl ether citrates, 330985–61–0 poly(oxyethylene) content is 4–12 moles, minimum number average molecular weight (in amu) 1,300

a-Hydro-w-hydroxypoly(oxyethylene), minimum number average molecular 25322–68–3 weight (in amu), 17,000

a-Hydro-w-hydroxypoly(oxyethylene)poly (oxypropylene) poly(oxyethylene) None block copolymer; the minimum poly(oxypropylene) content is 27 moles and the minimum molecular weight (in amu) is 1,900

a-Hydro-w-hydroxypoly(oxypropylene); minimum molecular weight (in amu) None 2,000

12-Hydroxystearic acid-polyethylene glycol copolymer, minimum number aver- 70142–34–6 age molecular weight (in amu), 3,690

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Polymer CAS No.

Isodecyl alcohol ethoxylated (2–8 moles) polymer with chloromethyl oxirane, None minimum number average molecular weight (in amu) 2,500

Lauryl methacrylate-1,6-hexanediol dimethacrylate copolymer, minimum molec- None ular weight (in amu), 100,000

Maleic acid-butadiene copolymer None

Maleic acid monobutyl ester-vinyl methyl ether copolymer, minimum average 25119–68–0 molecular weight (in amu), 52,000

Maleic acid monoethyl ester-vinyl methyl ether copolymer, minimum average 25087–06–3 molecular weight (in amu), 46,000

Maleic acid monoisopropyl ester-vinyl methyl ether copolymer, minimum aver- 31307–95–6 age molecular weight (in amu), 49,000

Maleic anhydride-diisobutylene copolymer, sodium salt, minimum number aver- 37199–81–8 age molecular weight (in amu) 5,0007–18,000

Maleic anhydride-methylstyrene copolymer sodium salt, minimum number aver- 60092–15–1 age molecular weight (in amu), 15,000

Maleic anhydride-methyl vinyl ether, copolymer, average molecular weight (in None amu), 250,000

Methacrylic acid-methyl methacrylate-polyethylene glycol methyl ether meth- 100934–04–1 acrylate copolymer, minimum number averge molecular weight (in amu), 3,700

Methacrylic acid-methyl methacrylate-polyethylene glycol monomethyl ether 111740–36–4 methacrylate graft copolymer, minimum number average molecular weight (in amu), 1,800

Methacrylic copolymer, minimum number average molecular weight (in amu), 63150–03–8 15,000

Methyl methacrylate-methacrylic acid-monomethoxypolyethylene glycol meth- 119724–54–8 acrylate copolymer,) minimum number average molecular weight (in amu), 2,730

Methyl methacrylate-2-sulfoethyl methacrylate-dimethylaminoethylmethacrylate- None glycidyl methacrylate-styrene-2-ethylhexyl acrylate graft copolymer, minimum average molecular weight (in amu), 9,600

Methyl vinyl ether-maleic acid copolymer), minimum number average molecular 25153–40–6 weight (in amu), 75,000

Methyl vinyl ether-maleic acid copolymer, calcium sodium salt, minimum num- 62386–95–2 ber average molecular weight (in amu), 900,000

Monophosphate ester of the block copolymer a-hydro-w- None hydroxypoly(oxyethylene) poly(oxypropylene) poly(oxyethylene); the poly(oxypropylene) content averages 37–41 moles, average molecular weight (in amu), 8,000

a-(p-Nonylphenyl)-w-hydroxypoly(oxyethylene) mixture of dihydrogen phosphate None and monohydrogen phosphate esters and the corresponding ammonium, calcium, magnesium, monoethanolamine, potassium, sodium, and zinc salts of the phosphate esters; the nonyl group is a propylene trimer isomer and the poly(oxyethylene) content averages 30 moles

a-(p-Nonylphenyl)-w-hydroxypoly(oxyethylene) sulfate, and its ammonium, cal- None cium, magnesium, monoethanolamine, potassium, sodium, and zinc salts; the nonyl group is a propylene trimer isomer and the poly(oxyethylene) content averages 30-90 moles of ethylene oxide

a-(p-Nonylphenyl-w-hydroxypoly(oxypropylene) block polymer with None poly(oxyethylene); polyoxypropylene content of 10–60 moles; polyoxyethylene content of 10–80 moles; molecular weight (in amu), 1,200– 7,100.

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Polymer CAS No.

a-(r-Nonylphenyl)poly(oxypropylene) block polymer with poly(oxyethylene); poly 37251–69–7 oxyethylene content 30 to 90 moles; minimum number average molecular weight (in amu), 1,889

Octadecanoic Acid, 12-Hydroxy-, Homopolymer Ester with 2-Methylloxirane 1373125–59–7 Polymer with Oxirane monobutyl Ether, minimum number average molecular weight (in amu), 4,500

Octadecanoic acid, 12-hydroxy-, homopolymer, octadecanoate minimum num- 58128–22–6) ber average molecular weight (in amu), 1,370

a-cis-9-Octadecenyl-w-hydroxypoly(oxyethylene); the octadecenyl group is de- None rived from oleyl alcohol and the poly(oxyethylene) content averages 20 moles

Octadecyl acrylate-acrylic acid copolymer, octadecyl acrylate-dodecyl acrylate- None acrylic acid copolymer, octadecyl methacrylate-butyl acrylate-acrylic acid copolymer, octadecyl methacrylate-hexyl acrylate-acrylic acid copolymer, octadecyl methacrylate-dodecyl acrylate-acrylic acid copolymer, or octadecyl methacrylate-dodecyl methacrylate-acrylic acid copolymer, minimum number average molecular weight (in amu) 3,000

Oleic acid diester of a-hydro-w-hydroxypoly(oxyethylene); the None poly(oxyethylene), average molecular weight (in amu), 2,300

2-oxepanone, homopolymer, minimum number average molecular weight (in 24980–41–4 amu) 52,000

Oxirane, decyl-, reaction products with polyethylene-polypropylene glycol ether 903890–89–1 with trimethylolpropane (3:1)

Oxirane, hexadecyl-, reaction products with polyethylene-polypropylene glycol 893427–80–0 ether with trimethylolpropane (3:1)

Oxirane, 2-methyl-, polymer with oxirane, dimethyl ether, minimum number av- 61419–46–3 erage molecular weight (in amu), 2,800

Oxirane, methyl-, polymer with oxirane, ether with 2-ethyl-2-(hydroxymethyl)- 903890–90–4 1,3-propanediol (3:1), reaction products with tetradecyloxirane

Oxirane, methyl-, polymer with oxirane, mono[2-(2-butoxyethoxy) ethyl] ether, 85637–75–8 minimum number average molecular weight (in amu), 2,500

Oxirane, methyl-, polymer with Oxirane, Monobutyl Ether 9038–95–3

Oxirane, 2-methyl-, polymer with oxirane, minimum number average molecular 9003–11–6 weight (in amu), 1,100

Oxirane, 2-methyl-, polymer with oxirane, mono [2-[2-(2- 926031–36–9 butoxymethylethoxy)methylethoxy]methylethyl] ether, minimum number average molecular weight (in amu), 3,000

Oxirane, phenyl, polymer with oxirane, monooctyl ether, minimum average mo- 83653–00–3 lecular weight (in amu) 1,200

Polyamide polymer derived from sebacic acid, vegetable oil acids with or with- None out dimerization, terephthalic acid and/or ethylenediamine

Polyethylene glycol-polyisobutenyl anhydride-tall oil fatty acid copolymer, min- 68650–28–2 imum number average molecular weight (in amu), 2,960

Polyethylene, oxidized, minimum number average molecular weight (in amu), None 1,200

Polymers produced by the reaction of either 1,6-hexanediisocyanate; 2,4,4- 1161844–26–3, 1161844–30–9, 1161844–43– trimethyl-1,6-hexanediisocyanate; 5-isocyanato-1-(isocyanatomethyl)- 4, 1161844–51–4, 1161844–53–6, 693252– fxsp0;1,3,3-trimethyIcyclohexane (isophoronediisocyanate); 4,4′-methylene- 31–2, 162993–60–4, 630102–86–2 bis-1,1′-cyclohexanediisocyanate; 4,4′-methylene-bis-1,1′ benzyldiisocyanate; or 1,3-bis-(2-isocyanatopropan-2-yl)benzene with polyethylene glycol and end-capped with one or a mixture of more than one of octanol, decanol, dodecanol, tetradecanol, hexadecanol, octadecanol, and octadec-9-enol or polyethyleneglycol ethers of octanol, decanol, dodecanol, tetradecanol, hexadecanol, octadecanol, and octadec-9-enol, minimum number average molecular weight (in amu), 20,000

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Polymer CAS No.

Polymethylene polyphenylisocyanate, polymer with ethylene diamine, None diethylene triamine and sebacoyl chloride, cross-linked; minimum number average molecular weight (in amu), 100,000

Polyoxyalkylated glycerol fatty acid esters; the mono-, di-, or triglyceride mix- 61791–23–9, 68201–46–7, 68440–49–3, tures of C8 through C22, primarily C8 through C18 saturated and unsaturated, 68458–88–8, 68606–12–2, 68648–38–4, fatty acids containing up to 15% water by weight reacted with a minimum of 70377–91–2, 70914–02–2, 72245–12–6, three moles of either ethylene oxide or propylene oxide; the resulting poly- 72698–41–3, 180254–52–8, 248273–72–5, oxyalkylated glycerol ester polymer minimum number average molecular 308063–50–5, 952722–33–7 weight (in amu), 1,500

Polyoxyalkylated sorbitan fatty acid esters with C6 through C22 aliphatic 81776–11–6, 87090–31–1, 88895–72–1, alkanoic and/or alkenoic fatty acids, branched or linear, the resulting 103171–31–9, 161026–53–5, 1472644–80– polyoxyalkylene sorbitan esters minimum number average molecular weight 6, 1472644–81–7, 1472644–84–0, (in amu), 1,300 1472644–85–1, 1472644–87–3, 1472644– 88–4, 1472654–83–3, 1472655–32–5, 1472661–05–4, 1472661–17–8, 1472663– 59–4, 1472663–64–1, 1472663–66–3, 1472663–92–5, 1472668–03–3

Polyoxyalkylated trimethylopropanes with 20 to 80 moles of ethylene and/or 25765–36–0; 29860–47–7; 37339–03–0; propylene oxide, fatty acid esters with C8 through C22 aliphatic alkanoic and/ 52624–57–4; 58090–24–7; 63964–38–5; or alkenoic fatty acids, branched or linear; minimum number average molec- 72939–62–9; 74521–14–5; 75300–70–8; ular weight (in amu), 3,000 75300–90–2; 84271–03–4; 84271–04–5; 86850–92–2; 107120–02–5; 133331–01–8; 137587–60–1; 149797–40–0; 149797–41–1; 150695–97–9; 152130–24–0; 163349–94–8; 163349–95–9; 163349–96–0; 163349–97–1; 163349–98–2; 165467–70–9; 183619–46–7; 183619–50–3; 185260–01–9; 202606–04–0; 210420–84–1; 233660–70–3; 263011–96–7; 283602–94–8; 701980–40–7; 872038–58–9; 875709–44–7; 875709–45–8; 875709–46–9; 875709–47–0; 879898–63–2; 910038–01–6; 1190748–04–9; 1225384–02–0; 1428944– 41–5; 1446498–15–2.

Poly(oxy-1,2-ethanediyl), a-hydro-w-hydroxy-, polymer with 1, 1′-methylene-bis- 39444–87–6 [4-isocyanatocyclohexane], minimum number average molecular weight (in amu), 1800

Polyoxyethylated primary amine (C14–C18); the fatty amine is derived from an None animal source and contains 3% water; the poly(oxyethylene) content averages 20 moles

Polyoxyethylated sorbitol fatty acid esters; the polyoxyethylated sorbitol solution None containing 15% water is reacted with fatty acids limited to C12, C14, C16, and C18, containing minor amounts of associated fatty acids; the poly(oxyethylene) content averages 30 moles.

Polyoxyethylated sorbitol fatty acid esters; the sorbitol solution containing up to None 15% water is reacted with 20–50 moles of ethylene oxide and aliphatic alkanoic and/or alkenoic fatty acids C8 through C22 with minor amounts of associated fatty acids; the resulting polyoxyethylene sorbitol ester having a minimum molecular weight (in amu), 1,300

Poly(oxyethylene/oxypropylene) monoalkyl (C6–C10) ether sodium fumarate 102900–02–7 adduct, minimum number average molecular weight (in amu), 1,900

Poly[oxy(methyl-1,2-ethanediyl)], a-[(9Z)-1-oxo-9-octadecen-1-yl]-w-[[(9Z)-1-oxo- 26571–49–3 9-octadecen-1yl]oxy]-, minimum number average molecular weight (in amu) 2,300

Polyoxymethylene copolymer, minimum number average molecular weight (in None amu), 15,000

Poly(oxypropylene) block polymer with poly(oxyethylene), molecular weight (in None amu), 1,800–16,000

Poly(phenylhexylurea), cross-linked, minimum average molecular weight (in None amu), 36,000

Polypropylene 9003–07–0

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Polymer CAS No.

Polystyrene, minimum number average molecular weight (in amu), 50,000 9003–53–6

Polytetrafluoroethylene 9002–84–0

Polyvinyl acetate, copolymer with maleic anhydride, partially hydrolyzed, so- None dium salt, minimum number average molecular weight (in amu), 53,000

Polyvinylpyrrolidone butylated polymer, minimum number average molecular 26160–96–3 weight (in amu), 9,500

Polyvinyl acetate, minimum molecular weight (in amu), 2,000 None

Polyvinyl acetate—polyvinyl alcohol copolymer, minimum number average mo- 25213–24–5 lecular weight (in amu), 50,000

Polyvinyl alcohol 9002–89–5

Polyvinyl chloride None

Polyvinyl chloride, minimum number average molecular weight (in amu), 29,000 9002–86–2

Poly(vinylpyrrolidone), minimum number average molecular weight (in amu), 9003–39–8 4,000

Poly(vinylpyrrolidone-1-eicosene), minimum average molecular weight (in amu), 28211–18–9 3,000

Poly(vinylpyrrolidone-1-hexadecene), minimum average molecular weight (in 63231–81–2 amu), 4,700

1-propanesulfonic acid, 2-methyl-2-[(1-oxo-2-propenyl)amino]-, monosodium 107568–12–7 salt, polymer with ethenol and ethenyl acetate, minimum number average molecular weight (in amu) 50,000

2-Propene-1-sulfonic acid sodium salt, polymer with ethenol and ethenyl ace- None tate, number average molecular weight (in amu) 6,000–12,000

2-Propenoic acid, butyl ester, polymer with 1,6-diisocyanatohexane, N- 1469998–09–1 (hydroxymethyl)-2-methyl-2-propenamide and 2-propenenitrile, minimum number average molecular weight (in amu), 100,000

2-propenoic acid, butyl ester, polymer with ethenylbenzene, methyl 2-methyl-2- 27306–39–4 propenoate and 2-propenoic acid (in amu), 1900.

2-Propenoic acid, butyl ester, polymer with ethyl 2-propenoate and N- 33438–19–6 (hydroxymethyl)-2-propenamide, minimum number average molecular weight (in amu), 30,000

2-Propenoic acid, 2-ethylhexyl ester, polymer with ethenylbenzene 14,000 dal- 25153–46–2 tons

2-Propenoic acid, 2-ethylhexyl ester, polymer with ethenylbenzene and 2- 68240–06–2 methylpropyl 2-methyl-2-propenoate, minimum number average molecular weight (in amu), 18,000

2-propenoic acid, homopolymer, ester with a-[2,4,6-tris(1-phenylethyl)phenyl]-w- 1477613–46–9 hydroxypoly(oxy-1,2-ethanediyl), compd. with 2,2′,2″-nitrilotris[ethanol]), minimum number average molecular weight (in amu), 10,000. 2-Propenoic acid, 2-hydroxyethyl ester, polymer with a-[4-(ethenyloxy)butyl]-w- 1007234–89–0 hydroxypoly (oxy-1,2-ethanediyl), minimum number average molecular weight (in amu), 17,000

[2-propenoic acid, 2-methyl-, C12-16-alkyl esters, telomers with 1- 950207–35–9 dodecanethiol, polyethylene-polypropylene glycol ether with propylene glycol monomethacrylate (1:1), and styrene 2,2’-(1,2-diazenediyl)bis[2- methylbutanenitrile]-initiated, minimum number average molecular weight (in amu), 4,000

2-Propenoic acid, methyl ester, polymer with ethenyl acetate, hydrolyzed, so- 886993–11–9 dium salts

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Polymer CAS No.

2-Propenoic acid, 2-methyl-, 2-ethylhexyl ester, telomer with 1-dodecanethiol, 1283712–50–4 ethenylbenzene and 2-methyloxirane polymer with oxirane monoether with 1,2-propanediol mono(2-methyl-2-propenoate), hydrogen 2-sulfobutanedioate, sodium salt, 2, 2′-(1,2-diazenediyl)bis[2-methylpropanenitrile]-initiated, minimum number average molecular weight (in amu), 1,200

2-Propenoic acid, 2-methyl-, 2-methylpropyl ester, homopolymer, minimum 9011–15–8 number average molecular weight (in amu), 55,000

2-propenoic acid, 2-methyl-, 2-oxiranylmethyl ester, polymer with ethene, eth- 518057–54–0 enyl acetate, ethenyltrimethoxysilane and sodium ethenesulfonate (1:1), minimum number average molecular weight (in amu), 20,000.

2-Propenoic acid, 2-methyl-, phenylmethyl ester, polymer with 2-propenoic acid, 1574486–33–1 peroxydisulfuric acid ([(HO)S(O)2]2O2) sodium salt (1:2)-initiated, compounds with diethanolamine, minimum number average molecular weight (in amu), 2,000

2-Propenoic acid, 2-methyl-, phenylmethyl ester, polymer with 2-propenoic acid CASRN 1246766–57–3 and sodium 2-methyl-2-[(1-oxo-2-propen-1-yl)amino]-1-propanesulfonate (1:1), peroxydisulfuric acid ([HO)S(O)2]202) sodium salt (1:2)-initiated minimum number average molecular weight >1,000 Daltons; maximum number average molecular weight 10,000 Daltons

2-Propenoic acid, 2-methyl-, polymer with butyl 2-propenoate and 25036–16–2 ethenylbenzene, minimum number average molecular weight (in amu), 17,000

2-Propenoic acid, 2-Methyl-, Polymer with Butyl 2-Propenoate, Methyl 2-Methyl- 153163–36–1 2-Propenoate, Methyl 2-Propenoate and 2-Propenoic Acid, graft, Compound with 2-Amino-2-Methyl-1-Propanol

2-Propenoic Acid, 2-Methyl-, Polymer with Ethenylbenzene, 2-Ethylhexyl 2- 146753–99–3 Propenoate, 2-Hydroxyethyl 2-Propenoate, N-(Hydroxymethyl) -2-Methyl-2- Propenamide and Methyl 2-Methyl-2-Propenoate, Ammonium Salt

2-Propenoic acid, 2-methyl-, polymers with Bu acrylate, Et acrylate, Me meth- 890051–63–5 acrylate and polyethylene glycol methacrylate C16-18-alkyl ethers, minimum number average molecular weight (in amu), 13,000

2-propenoic acid, 2-methyl-, polymers with tert-Bu acrylate, Me methacrylate, 1515872–09–9 polyethylene glycol methacrylate C16-C18-alkyl ethers and vinylpyrrolidone, tert-Bu 2-ethylhexaneperoxoate-initiated, compounds with 2-amino-2-methyl- 1-propanol, minimum number average molecular weight (in amu), 2,600. 2-Propenoic acid, 2-methyl-, telomer with 2-ethylhexyl 2-propenoate, 2-propanol 1260001–65–7 and sodium 2-methyl-2-[(1-oxo-2-propen-1-yl) amino]-1-propanesulfonate (1:1), sodium salt, minimum number average molecular weight (in amu): 2,900

2-Propenoic acid, monoester with 1,2-propanediol, polymer with a-[4- 955015–23–3 (ethenyloxy) butyl]-w-hydroxypoly (oxy-1,2-ethanediyl) and 2,5-furandione, minimum number average molecular weight (in amu), 25,000

2-propenoic acid polymer, with 1,3-butadiene and ethenylbenzene, minimum 25085–39–6 number average molecular weight (in amu), 9400

2-Propenoic acid, polymer with ethenyl acetate, ethenylbenzene, 2-ethylhexyl 85075–52–1 2-propenoate and ethyl 2-propenoate, minimum number average molecular weight (50,149 Daltons)

2-Propenoic acid, polymer with ethenylbenzene and (1-methylethenyl)benzene, 52831–04–6 minimum number average molecular weight (in amu), 2,000

2-Propenoic acid, polymer with ethenylbenzene and (1-methylethenyl) benzene, 129811–24–1 sodium salt, minimum number average molecular weight (in amu), 2,800

2-Propenoic acid, polymer with a-[4-(ethenyloxy) butyl]-w-hydroxypoly (oxy-1,2- 251479–97–7 ethanediyl) and 2,5-furandione, sodium salt, minimum number average molecular weight (in amu), 25,000

2-Propenoic acid, polymer with a-[4-(ethenyloxy) butyl]-w-hydroxypoly (oxy-1,2- 518026–64–7 ethanediyl) and 1,2-propanediol mono-2-propenoate, potassium sodium salt, minimum number average molecular weight (in amu), 16,000

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Polymer CAS No.

2-Propenoic acid, polymer with a-[4-(ethenyloxy) butyl]-w-hydroxypoly (oxy-1, 2- 250591–84–5 ethanediyl), sodium salt, minimum number average molecular weight (in amu), 24,000

2-Propenoic acid, polymer with 2-propenamide, sodium salt, minimum number 25085–02–3 average molecular weight (in amu), 18,000

2-Propenoic acid, sodium salt, polymer with 2-propenamide, minimum number 25987–30–8 average molecular weight (in amu), 18,000

2-Propenoic, 2-methyl-, polymers with ethyl acrylate and polyethylene glycol 888969–14–0 methylacrylate C18-22 alkyl ethers

2-Pyrrolidone, 1-ethenyl-, polymer with ethenol, minimum number average mo- 26008–54–8 lecular weight (in amu), 23,000

Silane, dichloromethyl- reaction product with silica minimum number average 68611–44–9 molecular weight (in amu), 3,340,000

Silane, trimethoxy[3-(oxiranylmethoxy)propyl]-, hydrolysis products with silica, 68584–82–7 minimum number average molecular weight (in amu), 640,000

Silicic acid, sodium salt, reaction products with chlorotrimethylsilane and iso- None propyl alcohol, reaction with poly(oxypropylene)-poly(oxyethylene) glycol, minimum number average molecular weight (in amu), 75,000

Sodium polyflavinoidsulfonate, consisting chiefly of the copolymer of catechin None and leucocyanidin

Soybean oil, ethoxylated; the poly(oxyethylene) content averages 10 moles or 61791–23–9 greater

Starch, oxidized, polymers with Bu acrylate, tert-Bu acrylate and styrene, min- 204142–80–3 imum number average molecular weight (in amu), 10,000

Stearyl methacrylate-1,6-hexanediol dimethacrylate copolymer, minimum mo- None lecular weight (in amu), 100,000

Styrene, copolymers with acrylic acid and/or methacrylic acid, with none and/or None one or more of the following monomers: Acrylamidopropyl methyl sulfonic acid, methallyl sulfonic acid, 3-sulfopropyl acrylate, 3-sulfopropyl methacrylate, hydroxypropyl methacrylate, hydroxypropyl acrylate, hydroxyethyl methacrylate, hydroxyethyl acrylate, and/or lauryl methacrylate; and its sodium, potassium, ammonium, monoethanolamine, and triethanolamine salts; the resulting polymer having a minimum number average molecular weight (in amu), 1200

Styrene-ethylene-propylene block copolymer, minimum number average molec- 108388–87–0 ular weight (in amu), 125,000

Styrene, 2-ethylhexyl acrylate, butyl acrylate copolymer, minimum number aver- 30795–23–4 age molecular weight (in amu), 4,200

Styrene-2-ethylhexyl acrylate-glycidyl methacrylate-2-acrylamido-2- None methylpropanesulfonic acid graft copolymer, minimum number average molecular weight (in amu), 12,500

Styrene-maleic anhydride copolymer None

Styrene-maleic anhydride copolymer, ester derivative None

Tall oil, polymer with polyethylene glycol and succinic anhydride 1398573–80–2 monopolyisobutylene derivs., minimum number average molecular weight (in amu), 1,200

Tamarind seed gum, 2-hydroxypropyl ether polymer, minimum number average 68551–04–2 molecular weight (in amu), 10,000

Tetradecyl acrylate-acrylic acid copolymer, minimum number average molecular None weight (in amu), 3,000

Tetraethoxysilane, polymer with hexamethyldisiloxane, minimum number aver- 104133–09–7 age molecular weight (in amu), 2,500

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Polymer CAS No.

Tetraethoxysilane, polymer with hexamethyldisiloxane, minimum number aver- 104133–09–7 age molecular weight (in amu), 6,500

a-[p-(1,1,3,3-Tetramethylbutyl)phenyl]-w-hydroxypoly(oxyethylene) produced by 9036–19–5 the condensation of 1 mole of p-(1,1,3,3-tetramethylbutyl)phenol with a range 9002–93–1 of 30-70 moles of ethylene oxide

a-[p-(1,1,3,3-Tetramethylbutyl)phenyl] poly(oxypropylene) block polymer with None poly(oxyethylene); the poly(oxypropylene) content averages 25 moles, the poly(oxyethylene) content averages 40 moles, the molecular weight (in amu) averages 3,400

a-[2,4,6-Tris[1-(phenyl)ethyl]phenyl]-w-hydroxy poly(oxyethylene) None poly(oxypropylene) copolymer, the poly(oxypropylene) content averages 2–8 moles, the poly(oxyethylene) content averages 16–30moles, average molecular weight (in amu), 1,500

Alpha-[2,4,6-Tris[1-(phenyl)ethyl]phenyl]-Omega-hydroxy poly(oxyethylene) 70880–56–7 poly(oxypropylene) copolymer, the poly(oxypropylene) content averages 2–8 moles, the poly(oxyethylene) content averages 16–60 moles. Minimum number-average molecular weight (in amu) of 1,500

Urea-formaldehyde copolymer, minimum average molecular weight (in amu), 9011–05–6 30,000

Vinyl acetate-allyl acetate-monomethyl maleate copolymer, minimum average None molecular weight (in amu), 20,000

Vinyl acetate-ethylene copolymer, minimum number average molecular weight 24937–78–8 (in amu), 69,000

Vinyl acetate polymer with none and/or one or more of the following monomers: None Ethylene, propylene, N-methyl acrylamide, acrylamide, monoethyl maleate, diethyl maleate, monooctyl maleate, dioctyl maleate, maleic anhydride, maleic acid, octyl acrylate, butyl acrylate, ethyl acrylate, methyl acrylate, acrylic acid, octyl methacrylate, butyl methacrylate, ethyl methacrylate, methyl methacrylate, methacrylic acid, carboxyethyl acrylate, and diallyl phthalate; and their corresponding sodium, potassium, ammonium, isopropylamine, triethylamine, monoethanolamine and/or triethanolamine salts; the resulting polymer having a minimum number average molecular weight (in amu), 1,200

Vinyl acetate-vinyl alcohol-alkyl lactone copolymer, minimum number average None molecular weight (in amu), 40,000; minimum viscosity of 18 centipoise

Vinyl alcohol-disodium itaconate copolymer, minimum average molecular None weight (in amu), 50,290

Vinyl alcohol-vinyl acetate copolymer, benzaldehyde-o-sodium sulfonate con- None densate, minimum number average molecular weight (in amu), 20,000

Vinyl alcohol-vinyl acetate-monomethyl maleate, sodium salt-maleic acid, diso- None dium salt-g-butyrolactone acetic acid, sodium salt copolymer, minimum number average molecular weight (in amu), 20,000

Vinyl chloride-vinyl acetate copolymers None

Vinyl pyrrolidone-acrylic acid copolymer, minimum number average molecular 28062–44–4 weight (in amu), 6,000

Vinyl pyrrolidone-dimethylaminoethylmethacrylate copolymer, minimum number 30581–59–0 average molecular weight (in amu), 20,000

Vinyl pyrrolidone-styrene copolymer 25086–29–7

[67 FR 36528, May 24, 2002]

EDITORIAL NOTE: For FEDERAL REGISTER citations affecting § 180.960, see the List of CFR Sections Affected, which appears in the Finding Aids section of the printed volume and at www.fdsys.gov.

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§ 180.1011 Viable spores of the micro- cordance with good agricultural prac- organism Bacillus thuringiensis tices. Berliner; exemption from the requirement of a tolerance. [36 FR 22540, Nov. 25, 1971, as amended at 38 FR 19045, July 17, 1973; 42 FR 28540, June 3, (a) For the purposes of this section 1977; 45 FR 43721, June 30, 1980; 45 FR 56347, the microbial insecticide for which ex- Aug. 25, 1980; 74 FR 26533, June 3, 2009] emption from the requirement of a tolerance is being established shall have § 180.1016 Ethylene; exemption from the following specifications: the requirement of a tolerance. (1) The microorganism shall be an au- Ethylene is exempted from the re- thentic strain of Bacillus thuringiensis quirement of a tolerance for residues Berliner conforming to the morpho- when: logical and biochemical characteristics (a) For all food commodities, it is of Bacillus thuringiensis as described in used as a plant regulator on plants, Bergey’s Manual of Determinative Bac- seeds, or cuttings and on all food com- teriology, Eighth Edition. modities after harvest and when ap- (2) Spore preparations of Bacillus plied in accordance with good agricul- thuringiensis Berliner shall be produced tural practices. by pure culture fermentation proce- (b) Injected into the soil to cause pre- dures with adequate control measures mature germination of witchweed in during production to detect any bean (lima and string), cabbage, canta- changes from the characteristics of the loupe, collard, corn, cotton, cucumber, parent strain or contamination by eggplant, okra, onion, pasture grass, other microorganisms. pea (field and sweet), peanut, pepper, (3) Each lot of spore preparation, potato, sweet potato, sorghum, soy- prior to the addition of other mate- bean, squash, tomato, turnip, and wa- rials, shall be tested by subcutaneous termelon fields as part of the U.S. De- injection of at least 1 million spores partment of Agriculture witchweed into each of five laboratory test mice control program. weighing 17 grams to 23 grams. Such test shall show no evidence of infection [39 FR 33315, Sept. 17, 1974, as amended at 40 or injury in the test animals when ob- FR 19477, May 5, 1975; 64 FR 31505, June 11, served for 7 days following injection. 1999] (4) Spore preparations shall be free of § 180.1017 Diatomaceous earth; exemp- the Bacillus thuringiensis b-exotoxin tion from the requirement of a tol- when tested with the fly larvae tox- erance. icity test (‘‘Microbial Control of In- sects and Mites,’’ R.P.M. Bond et al., p. (a) Diatomaceous earth is exempted 280 ff., 1971). This specification can be from the requirement of a tolerance for satisfied either by determining that residues when used in accordance with each master seed lot brought into pro- good agricultural practice in pesticide duction is a Bacillus thuringiensis strain formulations applied to growing crops, which does not produce b-exotoxin to food commodities after harvest, and under standard manufacturing condi- to animals. tions or by periodically determining (b) Diatomaceous earth may be safely that b-exotoxin synthesized during used in accordance with the following spore production is eliminated by the conditions. Application shall be lim- subsequent spore-harvesting procedure. ited solely to spot and/or crack and (b) Exemption from the requirement crevice treatments in food or feed proc- of a tolerance is established for resi- essing and food or feed storage areas in dues of the microbial insecticide Bacil- accordane with the precribed condi- lus thuringiensis Berliner, as specified tions: in paragraph (a) of this section, in or (1) It is used or intended for use for on honey and honeycomb and all other control of insects in food or feed proc- raw agricultural commodities when it essing and food or feed storage areas: is applied either to growing crops, or Provided, That the food or feed is re- when it is applied after harvest in ac- moved or covered prior to such use.

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(2) To assure safe use of the insecti- Rice, straw cide, its label and labeling shall con- Safflower, seed form to that registered by the U.S. En- Sorghum, forage, forage vironmental Protection Agency, and it Sorghum, grain, forage Sorghum, grain, grain shall be used in accordance with such Sorghum, grain, stover label and labeling. Soybean, forage [65 FR 33716, May 24, 2000] Soybean, hay Soybean, seed § 180.1019 Sulfuric acid; exemption Sunflower, seed from the requirement of a toler- Wheat, grain ance. [74 FR 47457, Sept. 16, 2009] (a) Residues of sulfuric acid are exempted from the requirement of a tol- § 180.1021 Copper; exemption from the erance when used in accordance with requirement of a tolerance. good agricultural practice when used (a) Copper is exempted from the re- as a herbicide in the production of gar- quirement of a tolerance in cattle, lic and onions, and as a potato vine meat; goat, meat; hog, meat; horse, dessicant in the production of potatoes. meat; sheep, meat; milk, poultry, fat; (b) Residues of sulfuric acid are ex- poultry, meat; poultry, meat byprod- empted from the requirement of a tol- ucts; egg, fish, shellfish, and irrigated erance in cattle, meat; goat, meat; hog, crops when it results from the use of: meat; horse, meat; sheep, meat; poul- (1) Copper sulfate as an algicide or try, fat; poultry, meat; poultry, meat, herbicide in irrigation conveyance sys- byproducts; egg; milk; fish, shellfish, tems and lakes, ponds, reservoirs, or and irrigated crops when it results bodies of water in which fish or shell- from the use of sulfuric acid as an inert fish are cultivated. ingredient in a pesticide product used (2) Basic copper carbonate (mala- in irrigation conveyance systems and chite) as an algicide or herbicide in im- lakes, ponds, reservoirs, or bodies of pounded and stagnant bodies of water water in which fish or shellfish are cul- (3) Copper triethanolamine and cop- tivated. The sulfuric acid is not to ex- per monoethanolamine as an algicide ceed 10% of the pesticide formulation or herbicide in fish hatcheries, lakes, (non-aerosol formulations only). ponds, and reservoirs (4) Cuprous oxide bearing antifouling [69 FR 40787, July 7, 2004, as amended at 74 coatings for control of algae or other FR 26533, June 3, 2009] coatings for control of algae or other § 180.1020 Sodium chlorate; exemption organisms on submerged concrete or from the requirement of a toler- other (irrigation) structures. ance. (5) Copper oxide embedded in polymer Sodium chlorate is exempted from emitter heads used in irrigation sys- the requirement of a tolerance for resi- tems for root incursion prevention. dues when used as a defoliant or des- (b) The following copper compounds iccant in accordance with good agricul- are exempt from the requirement of a tural practice on the following crops: tolerance when applied (primarily) as a fungicide to growing crops using good Bean, dry, seed agricultural practices: Corn, field, forage Corn, field, grain Copper compounds CAS Reg. No. Corn, field, stover Corn, pop, grain Basic copper carbonate (mala- Corn, pop, stover chite) ...... 1184–64–1 Corn, sweet, forage Copper ammonia complex ...... 16828–95–8 Copper ethylenediamine complex 13426–91–0 Corn, sweet, stover Copper hydroxide ...... 20427–59–2 Cotton, undelinted seed Copper octanoate ...... 20543–04–8 Flax, seed Copper oxychloride ...... 1332–65–6 Grain, aspirated fractions Copper oxychloride sulfate ...... 8012–69–9 Guar, seed Copper salts of fatty and rosin Pea, southern acids ...... 9007–39–0 Pepper, nonbell Copper sulfate basic ...... 1344–73–6 Potato Copper sulfate pentahydrate ...... 7758–99–8 Cuprous oxide ...... 1317–19–1 Rice, grain

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(c) Copper sulfate pentahydrate (CAS grain; corn, pop, grain; cowpea, hay; Reg. No. 7758–99–8) is exempt from the fescue, forage; fescue, hay; lespedeza, requirement of a tolerance when ap- forage; lespedeza, hay; lupin; oat, plied as a fungicide to growing crops or grain; orchardgrass, forage; to raw agricultural commodities after orchardgrass, hay; peanut, hay; pea, harvest, and as a bactericide/fungicide field, hay; ryegrass, Italian, hay; sor- in or on meat, fat and meat by-prod- ghum, grain, grain; soybean, hay; ucts of cattle, sheep, hogs, goats, sudangrass, forage; sudangrass, hay; horses and poultry, milk and eggs when timothy, forage; timothy, hay; vetch, applied as a bactericide/fungicide to forage; vetch, hay; and wheat, grain. animal premises and bedding. (b) Propanoic acid is exempt from the (d) Copper (II) hydroxide (CAS Reg. requirement of a tolerance for residues No. 20427–59–2) is exempt from the re- in or on cattle, meat; cattle, meat by- quirement of a tolerance when applied products; goat, meat; goat, meat by- to growing crops or to raw agricultural products; hog, meat; hog meat byprod- commodities as an inert ingredient (for ucts; horse, meat; horse, meat byprod- pH control) in pesticide products. ucts; sheep, meat; sheep meat byproducts; and, poultry, fat; poultry meat; [65 FR 68912, Nov. 15, 2000, as amended at 69 FR 4069, Jan. 28, 2004; 71 FR 46110, Aug. 11, poultry meat byproducts; milk, and 2006; 74 FR 26534, June 3, 2009; 74 FR 47457, egg when applied as a bactericide/fun- Sept. 16, 2009; 80 FR 37551, July 1, 2015] gicide to livestock drinking water, poultry litter, and storage areas for si- § 180.1022 Iodine-detergent complex; lage and grain. exemption from the requirement of (c) Preharvest and postharvest appli- a tolerance. cation of propanoic acid (CAS Reg. No. The aqueous solution of hydriodic 79–09–4), propanioc acid, calcium salt acid and elemental iodine, including (CAS Reg. No. 4075–81–4), and propanioc one or both of the surfactants (a) sodium salt (CAS Reg. No. 137–40–6) are polyoxypropylene-polyoxyethylene gly- exempted from the requirement of a col nomionic block polymers (min- tolerance on all crops when used as ei- imum average molecular weight 1,900) ther an active or inert ingredient in ac- and (b) a-(p- nonylphenyl)-omega- cordance with good agricultural prac- hydroxypoly (oxyethylene) having a tice in pesticide formulations applied maximum average molecular weight of to growing crops, to raw agricultural 748 and in which the nonyl group is a commodities before and after harvest propylene trimer isomer, is exempted and to animals. from the requirement of a tolerance for [69 FR 47025, Aug. 4, 2004, as amended at 74 residues in egg, and poultry, fat; poul- FR 26534, June 3, 2009] try, meat; poultry, meat byproducts when used as a sanitizer in poultry § 180.1025 Xylene; exemption from the drinking water. requirement of a tolerance. [74 FR 26534, June 3, 2009] Xylene is exempted from the requirement of a tolerance when used as an § 180.1023 Propanoic acid; exemptions aquatic herbicide applied to irrigation from the requirement of a toler- conveyance systems in accordance with ance. the following conditions: (a) Postharvest application of pro- (a) It is to be used only in programs panoic acid or a mixture of methylene of the Bureau of Reclamation, U.S. De- bispropionate and oxy(bismethylene) partment of Interior, and cooperating bisproprionate when used as a fun- water user organizations. gicide is exempted from the require- (b) It is to be applied as an emulsion ment of a tolerance for residues in or at an initial concentration not to ex- on the following raw agricultural com- ceed 750 parts per million. modities: Alfalfa, forage; alfalfa, hay; (c) It is not to be applied when there alfalfa, seed; barley, grain; is any likelihood that the irrigation Bermudagrass, forage; Bermudagrass, water will be used as a source of raw hay; bluegrass, forage; bluegrass, hay; water for a potable water system or bromegrass, forage; bromegrass, hay; where return flows of such treated irri- clover, forage; clover, hay; corn, field, gation water into receiving rivers and

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streams would contain residues of xy- § 180.1037 Polybutenes; exemption lene in excess of 10 parts per million. from the requirement of a toler- (d) Xylene to be used as an aquatic ance. herbicide shall meet the requirement (a) Polybutenes are exempt from the limiting the presence of a polynuclear requirement of a tolerance for residues aromatic hydrocarbons as listed in 21 in or on the raw agricultural com- CFR 172.250. modity cotton, undelinted seed when [38 FR 16352, June 22, 1973, as amended at 50 used as a sticker agent for formula- FR 2980, Jan. 3, 1985] tions of the attractant gossyplure (1:1 mixture of (Z,Z)- and (Z,E)-7,11- § 180.1027 Nuclear polyhedrosis virus hexadecadien-1-ol acetate) to disrupt of Heliothis zea; exemption from the mating of the pink bollworm. the requirement of a tolerance. (b) Polybutenes are exempt from the (a) For the purposes of this section, requirement of a tolerance for residues the viral insecticide must be produced in or on the raw agricultural com- with an unaltered and unadulterated modity artichoke when used as a stick- inoculum of the single-embedded er agent in multi-layered laminted Heliothis zea nuclear polyhedrosis virus controlled-release dispensers of (Z)-11- (HzSNPV). The identity of the seed hexaadecenal to disrupt the mating of virus must be assured by periodic the artichoke plume moth. checks. [74 FR 26534, June 3, 2009] (b) Each lot of active ingredient of the viral insecticide shall have the fol- § 180.1040 Ethylene glycol; exemption lowing specifications: from the requirement of a toler- (1) The level of extraneous bacterial ance. contamination of the final Ethylene glycol as a component of unformulated viral insecticide should pesticide formulations is exempt from not exceed 107 colonies per gram as de- the requirement of a tolerance when termined by an aerobic plate on used in foliar applications to peanut trypticase soy agar. plants. (2) Human pathogens, e.g., Sal- [43 FR 41393, Sept. 18, 1978] monella, Shigella, or Vibrio, must be absent. § 180.1041 Nosema locustae; exemption (3) Safety to mice as determined by from the requirement of a toler- an intraperitoneal injection study ance. must be demonstrated. The insecticide Nosema locustae is ex- (4) Identity of the viral product, as empted from the requirement of a tol- determined by the most sensitive and erance for residues in or on all raw ag- standardized analytical technique, e.g., ricultural commodities. restriction endonuclease and/or SDS- [47 FR 21537, May 19, 1982] PAGE analysis, must be demonstrated. (c) Exemptions from the requirement § 180.1043 Gossyplure; exemption from of a tolerance are established for the the requirement of a tolerance. residues of the microbial insecticide The pheromone gossyplure, a 1:1 mix- Heliothis zea NPV, as specified in para- ture of (Z,Z)- and (Z,E)-7,11- graphs (a) and (b) of this section, in or hexadecadien-1-ol acetate) is exempt on all agricultural commodities. from the requirement of a tolerance in [60 FR 42460, Aug. 16, 1995, as amended at 74 or on the raw agricultural commodity FR 26534, June 3, 2009] cotton, undelinted seed when applied to cotton from capillary fibers. § 180.1033 Methoprene; exemption from the requirement of a toler- [74 FR 26534, June 3, 2009] ance. § 180.1049 Carbon dioxide; exemption Methoprene is exempt from the re- from the requirement of a toler- quirement of a tolerance in or on all ance. food commodities when used to control The insecticide carbon dioxide is ex- insect larvae. empted from the requirement of a tol- [68 FR 34829, June 11, 2003] erance when used after harvest in

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modified atmospheres for stored insect sist of ‘‘boiled linseed oil.’’ This exemp- control on food commodities. tion is limited to use on rice before edible parts form. [65 FR 33716, May 24, 2000] [46 FR 33270, June 29, 1981] § 180.1050 Nitrogen; exemption from the requirements of a tolerance. § 180.1057 Phytophthora palmivora; The insecticide nitrogen is exempted exemption from requirement of tol- from the requirements of a tolerance erance. when used after harvest in modified Phytophthora palmivora is exempted atmospheres for stored product insect from the requirement of a tolerance in control on all food commodities. or on the raw agricultural commodity fruit, citrus. [65 FR 33716, May 24, 2000] [74 FR 26534, June 3, 2009] § 180.1052 2,2,5-trimethyl-3-dichloroacetyl-1,3-oxazolidine; exemption § 180.1058 Sodium diacetate; exemp- from the requirement of a toler- tion from the requirement of a tol- ance. erance. 2,2,5-trimethyl-3-dichloroacetyl-1,3- Sodium diacetate, when used oxazolidine is exempted from the re- postharvest as a fungicide, is exempt quirement of a tolerance when used as from the requirement of a tolerance for an inert ingredient in formulations of residues in or on alfalfa, hay; the herbicides S-ethyl Bermudagrass, hay; bluegrass, hay; dipropylthiocarbamate, S-propyl bromegrass, hay; clover,hay; corm, dipropylthiocarbamate, and S-ethyl field, grain; corn, pop, grain; oat, grain; diisobutylthiocarbamate applied to orchardgrass, hay; sorghum, grain, corn fields before the corn plants grain; sudangrass, hay; ryegrass, emerge from the soil with a maximum Italian, hay; timothy, hay. of 0.5 pound of the inert ingredient per acre. [74 FR 26534, June 3, 2009] [45 FR 51201, Aug. 1, 1980] § 180.1064 Tomato pinworm insect pheromone; exemption from the re- § 180.1054 Calcium hypochlorite; ex- quirement of a tolerance. emptions from the requirement of a An exemption from the requirement tolerance. of a tolerance is established for com- (a) Calcium hypochlorite is exempted bined residues of both components of from the requirement of a tolerance the tomato pinworm insect pheromone when used preharvest or postharvest in (E)-4-tridecen-1-yl acetate and (Z)-4- solution on all raw agricultural com- tridecen-1-yl acetate in or on all raw modities. agricultural commodities (preharvest) (b) Calcium hypochlorite is exempted in accordance with the following pre- from the requirement of a tolerance in scribed conditions: or on grape when used as a fumigant (a) Application shall be limited sole- postharvest by means of a chlorine ly to point source dispensers or point generator pad. source chopped fibers containing the [59 FR 59165, Nov. 16, 1994, as amended at 74 tomato pinworm insect pheromone. FR 26534, June 3, 2009] (b) Cumulative yearly application cannot exceed 200 grams of tomato § 180.1056 Boiled linseed oil; exemp- pinworm pheromone per acre. tion from requirement of tolerance. [58 FR 34376, June 25, 1993] Boiled linseed oil (containing no more than 0.33 percent manganese § 180.1065 2-Amino-4,5-dihydro-6-meth- naphthenate and no more than 0.33 per- yl-4-propyl-s-triazolo(1,5- cent cobalt naphthenate) is exempt alpha)pyrimidin-5-one; exemption from the requirement of a tolerance from the requirement of a toler- when used as a coating agent for S- ance. ethyl hexahydro-1H-azepine-1- The inert ingredient, 2-amino-4,5- carbothioate. No more than 15 percent dihydro-6-methyl-4-propyl-s- of the pesticide formulation may con- triazolo(1,5-alpha)pyrimidin-5-one is

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exempted from the requirement of a § 180.1069 (Z)-11-Hexadecenal; exemp- tolerance when used as an emetic at tion from the requirement of a tol- not more than 0.3 percent in formula- erance. tions of paraquat dichloride. Further An exemption from the requirement restrictions on this exemption are that of a tolerance is established for resi- this ingredient may not be advertised dues of the biological insecticide as an emetic and the paraquat product (pheromone) (Z)-11-hexadecenal when may not be promoted in any way be- used as a sex attractant on artichoke cause of the inclusion of this inert in- plants to control the artichoke plume gredient. moth. [70 FR 46431, Aug. 10, 2005] [47 FR 14906, Apr. 7, 1982]

§ 180.1067 Methyl eugenol and mala- § 180.1070 Sodium chlorite; exemption thion combination; exemption from from the requirement of a toler- the requirement of a tolerance. ance. The insect attractant methyl eugenol Sodium chlorite is exempted from the requirement of a tolerance for resi- and the insecticide malathion are ex- dues when used in accordance with empt from the requirement of toler- good agricultural practice as a seed- ances on all raw agricultural commod- soak treatment in the growing of the ities when used in combination in Ori- raw agricultural commodities vege- ental fruit fly eradication programs table, brassica, leafy, group 5 and rad- under the authority of the U.S. Depart- ish, roots and radish, tops. ment of Agriculture, in accordance with the following directions and speci- [74 FR 26534, June 3, 2009] fications: § 180.1071 Peanuts, Tree Nuts, Milk, (a) The combination shall be at the Soybeans, Eggs, Fish, Crustacea, ratio of three parts methyl eugenol to and Wheat; exemption from the re- one part technical malathion (3:1). quirement of a tolerance. (b) This combination is to be impreg- (a) General. Residues resulting from nated on a carrier (cigarette filter tips the following uses of the food com- (cellulose acetate); cotton strings; fi- modity forms of peanuts, tree nuts, berboard squares) or mixed with a jel milk, soybeans, eggs (including putres- cleared under 40 CFR 180.920 or 180.950. cent eggs), fish, crustacea, and wheat (c) The maximum actual dosage per are exempted from the requirement of application per acre shall be 28.35 a tolerance in or on all food commod- grams (one ounce avoirdupois) methyl ities under FFDCA section 408 (when eugenol and 9.45 grams (one-third (0.33) used as either an inert or an active in- ounce avoirdupois) technical mala- gredient in a pesticide formulation), if thion. such use is in accordance with good agricultural practices: [47 FR 9002, Mar. 3, 1982, as amended at 69 FR (1) Use in pesticide products intended 23142, Apr. 28, 2004] to treat seeds. (2) Use in nursery and greenhouse op- § 180.1068 C 12-C 18 fatty acid potassium erations, as defined in 40 CFR 170.3, salts; exemption from the require- which includes seeding, potting and ment of a tolerance. transplanting activities. C12-C18 fatty acids (saturated and un- (3) Pre-plant and at-transplant appli- saturated) potassium salts are exempt- cations. ed from the requirement of a tolerance (4) Incorporation into seedling and for residues in or on all raw agricul- planting beds. tural commodities when used in ac- (5) Applications to cuttings and bare cordance with good agricultural prac- roots. tice. (6) Applications to the field that occur after the harvested crop has been [60 FR 34871, July 5, 1995] removed. (7) Soil-directed applications around and adjacent to all plants.

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(8) Applications to rangelands, which regulator poly-D-glucosamine when is land, mostly grasslands, whose used as a pesticide in the production plants can provide food (i.e., forage) for any raw agricultural commodity. grazing or browsing animals. (9) Use in chemigation and irrigation [60 FR 19524, Apr. 19, 1995] systems (via flood, drip, or furrow ap- § 180.1073 Isomate-M; exemption from plication with no overhead spray appli- the requirement of a tolerance. cations). (10) Application as part of a dry fer- The oriental fruit moth pheromone tilizer on which an active ingredient is (Isomate-M) (Z-8-dodecen-l-yl acetate, impregnated. E-8-dodecen-l-yl acetate, Z-8-dodecen-l- (11) Aerial and ground applications ol) is exempt from the requirement of a that occur when no above-ground har- tolerance in or on all the raw agricul- vestable food commodities are present tural commodities (food and feed) in- (usually pre-bloom). cluding, peach; quince; nectarine; and (12) Application as part of an animal nut, macadamia when used in orchards feed-through product. with encapsulated polyethylene tubing (13) Applications as gel and solid to control oriental fruit moth. (non-liquid/non-spray) crack and crevice treatments that place the gel or [74 FR 26534, June 3, 2009] bait directly into or on top of the cracks and crevices via a mechanism § 180.1074 F.D.&C. Blue No. 1; exemp- such as a syringe. tion from the requirement of a tolerance. (14) Applications to the same crop from which the food commodity is de- F.D.&C. Blue No. 1 is exempted from rived, whether the plant fraction(s) in- the requirement of a tolerance when tended for harvest are present or not, used as an aquatic plant control agent. e.g., applications of peanut meal when [47 FR 25963, June 16, 1982] applied to peanut plants. (b) Specific chemical substances. Resi- § 180.1075 Colletotrichum dues resulting from the use of the fol- gloeosporioides f. sp. aeschynomene; lowing substances as either an inert or exemption from the requirement of an active ingredient in a pesticide for- a tolerance. mulation are exempted from the requirement of a tolerance under FFDCA An exemption from the requirement section 408, if such use is in accordance of a tolerance is established for resi- with good agricultural practices and dues of the mycoherbicide such use is included in paragraph (a): Colletotrichum gloeosporioides f. sp. aeschynomene in or on the following Chemical Substance CAS No. raw agricultural commodities: Caseins ...... 9000–71–9 COMMODITY Caseins, ammonium complexes ...... 9005–42–9 Caseins, hydrolyzates ...... 65072–00–6 Aspirated grain fractions Caseins, potassium complexes ...... 68131–54–4 Caseins, sodium complexes ...... 9005–46–3 Rice, grain Soybean, forage Soybean, hay [70 FR 1360, Jan. 7, 2005] Soybean, seed § 180.1072 Poly-D-glucosamine [47 FR 25742, June 15, 1982, as amended at 74 (chitosan); exemption from the re- FR 26534, June 3, 2009] quirement of a tolerance. (a) An exemption from the require- § 180.1076 Viable spores of the micro- ment of a tolerance is established for organism Bacillus popilliae; exemp- residues of the biological plant growth tion from the requirement of a tol- regulator poly-D-glucosamine when erance. used as a seed treatment in or on bar- (a) For the purposes of this section ley, beans, oats, peas, rice, and wheat. the microbial insecticide for which ex- (b) An exemption from the require- emption from the requirement of a tol- ment of a tolerance is established for erance is being established shall have residues of the biological plant growth the following specifications:

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(1) The microorganism shall be an au- vent in formulations with the following thentic strain of Bacillus popilliae con- pesticides when used in accordance forming to the morphological and bio- with good agricultural practices in or chemical characteristics of Bacillus on the following raw agricultural com- popilliae as described in Bergey’s Man- modities: ual of Determinative Bacteriology, (a) Carbaryl (1-naphthyl methyl-car- Eighth Edition. bamate) (2) Spore preparations of Bacillus Pea, dry, seed popilliae shall be produced by an ex- Pea, succulent traction process from diseased Japa- nese beetles, and may contain a small (b) O-O-Diethyl O-(2-isopropyl-6- percentage of the naturally occurring methyl-4-pyrimidinyl) milky disease bacterium Bacillus phosphorothioate lentimorbus. Pea, dry, seed (3) Each lot of spore preparation, Pea, succulent prior to the addition of other mate- [48 FR 54819, Dec. 7, 1983, as amended at 74 rials, shall be tested by subcutaneous FR 26535, June 3, 2009] injection of at least 1 million spores into each of five laboratory test mice § 180.1084 Monocarbamide dihydrogen weighing 17 grams to 23 grams. Such sulfate; exemption from the require- test shall show no evidence of infection ment of a tolerance. of injury in the test animals when ob- Monocarbamide dihydrogen sulfate is served for 7 days following injection. exempted from the requirement of a (b) Exemption from the requirement tolerance when used as a herbicide or of a tolerance is established for resi- desiccant in or on all raw agricultural dues of the microbial insecticide Bacil- commodities. lus popilliae, as specified in paragraph (a) of this section in or on grass, pas- [53 FR 12152, Apr. 13, 1988] ture, forage and grass, rangeland, for- § 180.1086 3,7,11-Trimethyl-1,6,10- age when it is applied to growing crops dodecatriene-1-ol and 3,7,11- in accordance with good agricultural trimethyl-2,6,10-dodecatriene-3-ol; practices. exemption from the requirement of a tolerance. [47 FR 38535, Sept. 1, 1982, as amended at 74 FR 26535, June 3, 2009] The insect pheromone containing the active ingredients 3,7,11-trimethyl- § 180.1080 Plant volatiles and 1,6,10-dodecatriene-1-ol and 3,7,11- pheromone; exemptions from the trimethyl-2,6,10-dodecatriene-3-ol is ex- requirement of a tolerance. empted from the requirement of a tol- An exemption from the requirement erance in or on all raw agricultural of a tolerance is established for resi- commodities. dues of the plant volatiles cyclic decadiene, cyclic decene, cyclic [52 FR 12165, Apr. 15, 1987; 52 FR 29014, Aug. 5, 1987] pentadecatriene, and decatriene and the pheromone Z-2-isopropenyl-1- § 180.1087 Sesame stalks; exemption methylcyclobutaneethanol; Z-3,3-di- from the requirement of a toler- methyl-D1,b-cyclohexaneethanol; Z-3,3- ance. dimethyl-D1,a-cyclohexaneethanal; E- An exemption from the requirement 3,3-dimethyl-D1,a-cyclohexaneethanal of a tolerance is established for resi- combination when applied to cotton in dues of the biorational nematicide ses- hollow synthetic fibers. ame stalk in or on the following raw [48 FR 28442, June 22, 1983] agricultural commodities: Almond; almond, hulls; cotton, undelinted seed; § 180.1083 Dimethyl sulfoxide; exemp- cotton, gin byproducts; soybean, seed; tion from the requirement of a tol- soybean, forage; soybean, hay; aspi- erance. rated grain fractions; potato; beet, Dimethyl sulfoxide (DMSO) [CAS sugar, roots; beet, sugar, tops; tomato; Registry Number 67–68–5] is exempted pepper, bell; squash; strawberry; egg- from the requirement of a tolerance plant; cucumber; carrot, roots; radish, when used as an inert solvent or cosol- roots; radish, top; turnip, roots; turnip,

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tops; onion; pea, dry; pea, succulent; § 180.1095 Chlorine gas; exemptions melon; grape; walnut; orange; grape- from the requirement of a toler- fruit; mulberry; peach; apple; apricot; ance. blackberry; loganberry; pecan; cherry; Chlorine gas is exempted from the re- plum, and cranberry. quirement of a tolerance when used [74 FR 26535, June 3, 2009] preharvest or postharvest in solution on all raw agricultural commodities. § 180.1089 Poly-N-acetyl-D-glu- [56 FR 21309, May 8, 1991] cosamine; exemption from the requirement of tolerance. § 180.1097 GBM-ROPE; exemption from An exemption from the requirement the requirement of a tolerance. of a tolerance is established for resi- The grape berry moth pheromone dues of the biochemical nematicide (GBM-ROPE) containing the active in- poly-N-acetyl-D-glucosamine on a vari- gredients (Z)-9-dedecenyl acetate and ety of agricultural crops. (Z)-11-tetradecenyl acetate is exempt [53 FR 10249, Mar. 30, 1988] from the requirement of a tolerance in or on the raw agricultural commodity § 180.1090 Lactic acid; exemption from grape when used in orchards with en- the requirement of a tolerance. capsulated polyethylene tubing to con- Lactic acid (2-hydroxypropanoic trol grape berry moth. acid) is exempted from the requirement [74 FR 26535, June 3, 2009] of a tolerance when used as a plant growth regulator in or on all raw agri- § 180.1098 Gibberellins [Gibberellic cultural commodities. Acids (GA3 and GA4 + GA7), and So- dium or Potassium Gibberellate]; [53 FR 15286, May 4, 1988] exemption from the requirement of a tolerance. § 180.1091 Aluminum isopropoxide and aluminum secondary butoxide; ex- An exemption from the requirement emption from the requirement of a of a tolerance is established for resi- tolerance. dues of gibberellins [gibberellic acids Aluminum isopropoxide (CAS Reg. (GA3 and GA4 + GA7), and sodium or No. 555–31–7) and aluminum secondary potassium gibberellate] in or on all butoxide (CAS Reg. No. 2269–22–9) are food commodities when used as plant exempted from the requirement of a regulators on plants, seeds, or cuttings tolerance when used in accordance and on all food commodities after har- with good agricultural practices as sta- vest in accordance with good agricul- bilizers in formulations of the insecti- tural practices. cide amitraz [N′-(2,4-dimethylphenyl)- [64 FR 31505, June 11, 1999] N-[[(2,4-dimethylphenyl)imino]-N- methylmethanimidamide] applied to § 180.1100 Gliocladium virens isolate growing crops or animals. GL-21; exemption from the requirement of a tolerance. [53 FR 34509, Sept. 7, 1988; 53 FR 36696, Sept. 21, 1988] An exemption from the requirement of a tolerance is established for resi- § 180.1092 Menthol; exemption from dues of the biofungicide Gliocladium the requirement of a tolerance. virens GL-21 in or on all raw agricul- An exemption from the requirement tural commodities when used either as of a tolerance is established for resi- a fungicide for inoculation of plant dues of the pesticidal chemical men- growth media in greenhouses or on ter- thol in or on honey and honeycomb restrial food crops grown outdoors in when used in accordance with good ag- accordance with good agricultural ricultural practice in over-wintering practices. bee hives. [60 FR 48659, Sept. 20, 1995; 60 FR 52248, Oct. [74 FR 26535, June 3, 2009] 5, 1995]

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§ 180.1101 Parasitic (parasitoid) and § 180.1107 Delta endotoxin of Bacillus predatory insects; exemption from thuringiensis variety kurstaki en- the requirement of a tolerance. capsulated into killed Pseudomonas fluorescens; exemption from the re- Parasitic (parasitoid) and predatory quirement of a tolerance. insects are exempted from the requirement of a tolerance for residues when The delta endotoxin of Bacillus they are used in accordance with good thuringiensis variety kurstaki encapsulated into killed Pseudomonas agricultural and pest control practices fluorescens is exempt from the require- to control insect pests of stored raw ments of a tolerance in or on all raw whole grains such as corn, small agricultural commodities. grains, rice, soybeans, peanuts, and other legumes either bulk or [56 FR 28328, June 20, 1991] warehoused in bags. For the purposes EFFECTIVE DATE NOTE: At 81 FR 34907, June of this rule, the parasites (parasitoids) 1, 2016, § 180.1107 was removed, effective Nov. and predators are considered to be spe- 28, 2016. cies of Hymenoptera in the genera Trichogramma, Trichogrammatidae; § 180.1108 Delta endotoxin of Bacillus Bracon, Braconidae; Venturia, thuringiensis variety San Diego encapsulated into killed Pseudomonas Mesostenus, Ichneumonidae; fluorescens; exemption from the re- Anisopteromalus, Choetospila, quirement of a tolerance. Lariophagus, Dibrachys, Habrocytus, The delta endotoxin of Bacillus Pteromalus, Pteromalidae; thuringiensis variety San Diego encap- Cephalonomia, Holepyris, Laelius, sulated into killed Pseudomonas Bethylidae; and of Hemiptera in the fluorescens is exempt from the require- genera Xylocoris, Lyctocoris, and ments of a tolerance in or on all raw Dufouriellus, Anthocoridae. Whole in- agricultural commodities. sects, fragments, parts, and other residues of these parasites and predators [56 FR 28326, June 20, 1991] remain subject to 21 U.S.C. 342(a)(3). EFFECTIVE DATE NOTE: At 81 FR 34907, June 1, 2016, § 180.1108 was removed, effective Nov. [57 FR 14646, Apr. 22, 1992] 28, 2016.

§ 180.1102 Trichoderma harzianum § 180.1110 3-Carbamyl-2,4,5-trichloro- KRL-AG2 (ATCC #20847) strain T– benzoic acid; exemption from the 22; exemption from requirement of requirement of a tolerance. a tolerance. An exemption from the requirement An exemption from the requirement of a tolerance is established for the res- of a tolerance is established for resi- idues of 3-carbamyl-2,4,5- dues of the biofungicide Trichoderma trichlorobenzoic acid in or on all raw harzianum KRL-AG2 (ATCC #20847); agricultural commodities which occur also known as strain T-22 when applied from the direct application of in/or on all food commodities. chlorothalonil to crops in § 180.275 (a) and (b) and/or as an inadvertent residue [64 FR 16860, Apr. 7, 1999] resulting from the soil metabolism of § 180.1103 Isomate-C; exemption from chlorothalonil when applied to crops in the requirement of a tolerance. § 180.275 (a) and (b), and subsequent up- take by rotated crops when used ac- The codling moth pheromone cording to approved agricultural prac- (Isomate-C) E,E-8,10-dodecenyl alcohol, tices. dodecanol, tetradecanol is exempt from the requirements of a tolerance in or [57 FR 24552, June 10, 1992] on all raw agricultural commodities § 180.1111 Bacillus subtilis GB03; ex- when formulated in polyethylene emption from the requirement of a pheromone dispensers for use in or- tolerance. chards with encapsulated polyethylene The biofungicide Bacillus subtilis GB03 tubing to control codling moth. is exempted from the requirement of a [74 FR 26535, June 3, 2009] tolerance in or on all raw agricultural

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commodities when used in accordance pesticide at 20 grams or less per acre on with good agricultural practices. all raw agricultural commodities. [73 FR 50556, Aug. 27, 2008] [58 FR 8696, Feb. 17, 1993]

§ 180.1113 Lagenidium giganteum; ex- § 180.1120 Streptomyces sp. strain K61; emption from the requirement of a exemption from the requirement of tolerance. a tolerance. Lagenidium giganteum (a fungal orga- The biological pesticide Streptomyces nism) is exempt from the requirement sp. strain K61 is exempted from the re- of a tolerance in or on the raw agricul- quirement of a tolerance in or on all tural commodities aspirated grain frac- raw agricultural commodities when tions; grass, forage; grass, hay; rice, used as a fungicide for the treatment of grain; rice, straw; soybean, seed; soy- seeds, cuttings, transplants, and plants bean, forage; soybean, hay; rice, wild, of agricultural crops in accordance grain. with good agricultural practices. [74 FR 26535, June 3, 2009] [58 FR 21403, Apr. 21, 1993] EFFECTIVE DATE NOTE: At 81 FR 34907, June 1, 2016, § 180.1113 was removed, effective Nov. § 180.1121 Boric acid and its salts, 28, 2016. borax (sodium borate decahydrate), disodium octaborate tetrahydrate, § 180.1114 Pseudomonas fluorescens boric oxide (boric anhydride), so- A506, Pseudomonas fluorescens dium borate and sodium metabo- 1629RS, and Pseudomonas syringae rate; exemptions from the require- 742RS; exemptions from the re- ment of a tolerance. quirement of a tolerance. An exemption from the requirement The biological pesticides of a tolerance is established for resi- Pseudomonas fluorescens A506, dues of the pesticidal chemical boric Pseudomonas fluorescens 1629RS, and acid and its salts, borax (sodium borate Pseudomonas syringae 742RS are ex- decahydrate), disodium octaborate tet- empted from the requirement of a tol- rahydrate, boric oxide (boric anhy- erance in or on all raw agricultural dride), sodium borate and sodium met- commodities when applied as a frost aborate, in or on raw agricultural com- protection agent or biological control modities when used as an active ingre- agent to growing agricultural crops in dient in insecticides, herbicides, or fun- accordance with good agricultural gicides preharvest or postharvest in ac- practices. cordance with good agricultural prac- [57 FR 42700, Sept. 16, 1992] tices. [58 FR 44283, Aug. 20, 1993] § 180.1118 Spodoptera exigua nuclear polyhedrosis virus; exemption from the requirement of a tolerance. § 180.1122 Inert ingredients of semiochemical dispensers; exemp- An exemption from the requirement tions from the requirement of a tol- of a tolerance is established for the mi- erance. crobial pest control agent Spodoptera (a) All inert ingredients of exigua nuclear polyhedrosis virus when semiochemical dispenser products for- used as a pesticide control agent on all mulated with, and/or contained in, dis- raw agricultural commodities. pensers made of polymeric matrix ma- [58 FR 25784, Apr. 28, 1993] terials (including the monomers, plas- ticizers, dispersing agents, anti- § 180.1119 Azadirachtin; exemption oxidants, UV protectants, stabilizers, from the requirement of a toler- and other inert ingredients) are ex- ance. empted from the requirement of a tol- An exemption from the requirement erance when used as carriers in pes- of a tolerance is established for the bio- ticide formulations for application to chemical azadirachtin, which is iso- growing crops only. These dispensers lated from the berries of the Neem tree shall conform to the following speci- (Azadirachta indica), when used as a fications:

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(1) Exposure must be limited to inad- (1) Commodity exposure must be lim- vertent physical contact only. The de- ited to inadvertent physical contact. sign of the dispenser must be such as to The design of the dispenser must be preclude any contamination by its such as to preclude any exposure of its components of the raw agricultural components to the raw agricultural commodity (RAC) or processed foods/ commodity (RAC) or processed foods/ feeds derived from the commodity by feeds derived from the commodity due virtue of its proximity to the RAC or to its proximity to the RAC or as a re- as a result of its physical size. sult of its physical size. Dispensers (2) The dispensers must be applied must be of such size and construction discretely. This exemption does not that they are readily recognized post- apply to components of semiochemical application. formulations applied in a broadcast (2) The dispensers must be applied manner either to a crop field plot or to discretely, i.e., placed in the field in individual plants. easily perceived distinct locations in a (b) A semiochemical dispenser is a manner that does not prevent later re- single enclosed or semi-enclosed unit trieval. This exemption does not apply that releases semiochemical(s) into the to codlure applied in a broadcast man- surrounding atmosphere via volatiliza- ner either to a crop field plot or to in- tion and is applied in a manner to pro- dividual plants. vide discrete application of the (b) A codlure dispenser is a single en- semiochemical(s) into the environ- closed or semi-enclosed unit that re- ment. leases codlure into the surrounding at- (c) Semiochemicals are chemicals mosphere via volatilization and is ap- that are emitted by plants or animals plied in a manner to provide discrete and modify the behavior of receiving application (i.e., in easily perceived dis- organisms. These chemicals must be tinct locations in a manner that does naturally occurring or substantially not prevent later retrieval) of the identical to naturally occurring codlure into the environment. semiochemicals. [59 FR 9931, Mar. 2, 1994] [58 FR 64494, Dec. 8, 1993] § 180.1127 Biochemical pesticide plant § 180.1124 Arthropod pheromones; ex- floral volatile attractant com- emption from the requirement of a pounds: cinnamaldehyde, cinnamyl tolerance. alcohol, 4-methoxy cinnamaldehyde, 3-phenyl propanol, 4-methoxy Arthropod pheromones, as described phenethyl alcohol, indole, and 1,2,4- in § 152.25(b) of this chapter, when used trimethoxybenzene; exemptions in retrievably sized polymeric matrix from the requirement of a toler- dispensers are exempt from the re- ance. quirement of a tolerance in or on all Residues of the biochemical pesticide raw agricultural commodities when ap- plant floral volatile attractant com- plied to growing crops only at a rate pounds: cinnamaldehyde, cinnamyl al- not to exceed 150 grams active ingre- cohol, 4-methoxy cinnamaldehyde, 3- dient/acre/year in accordance with good phenyl propanol, 4-methoxy phenethyl agricultural practices. alcohol, indole, and 1,2,4- [59 FR 14759, Mar. 30, 1994] trimethoxybenzene are exempt from the requirement of a tolerance in or on § 180.1126 Codlure, (E,E)-8,10- the following raw agricultural com- Dodecadien-1-ol; exemption from modities: the following field crops—al- the requirement of a tolerance. falfa, clover, cotton, dandelion, pea- An exemption from the requirement nuts (including hay), rice, sorghum of a tolerance is established for the in- (milo), soybeans, sunflower, sweet po- sect pheromone codlure, (E,E)-8,10- tatoes, and wheat; the following vege- dodecadien-1-ol, on all raw agricultural table crops—asparagus, beans (includ- commodities in accordance with the ing forage hay), beets, carrots, celery, following prescribed conditions: cole crops (cabbage, broccoli, brussels (a) Application shall be limited sole- sprouts, cauliflower), collards (kale, ly to codlure dispensers that conform mustard greens, turnip greens, kohl- to the following specifications: rabi), corn, fresh (field, sweet, pop,

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seed), corn fodder and forage, chinese an active ingredient at a concentration cabbage, cowpeas, cucurbitis (cucum- not to exceed 20% by weight. bers, squash, pumpkin), egg plant, en- [79 FR 10682, Feb. 26, 2014] dive (escarole), horseradish (radish, rutabagas, turnip roots), leafy greens § 180.1131 Ampelomyces quisqualis iso- (spinach, swiss chard), lettuce (head late M10; exemption from the re- leaf), okra, parsley, parsnip, peas, peas quirement of a tolerance. with pods, peppers, potatoes, sugar beets, tomatoes; the following tree The biological fungicide Ampelomyces fruit, berry and nut crops—almonds, quisqualis isolate M10 is exempted from apples, apricots, berries (blackberry, the requirement of a tolerance in or on boysenberry, dewberry, loganberry, all raw agricultural commodities when raspberry), blueberry, cherry, citrus used as a fungicide on agricultural (grapefruit, kumquat, lemon, lime, or- crops in accordance with good agricul- ange, tangelo, and tangerine) cran- tural practices. berry, grapes, melons, (watermelon, [59 FR 33437, June 29, 1994] honeydew, crenshaw, cantaloupe, casaba, persian), nectarines, pears, pe- EFFECTIVE DATE NOTE: At 81 FR 34907, June cans, peaches, and strawberry as dis- 1, 2016, § 180.1131 was removed, effective Nov. 28, 2016. persed from the end-use product Corn ® Rootworm Bait , a pesticidal bait, in § 180.1135 Pasteuria penetrans; exemp- accordance with the prescribed condi- tion from the requirement of a tol- tions in paragraph (a) of this section. erance. (a) Cumulative yearly application The biological nematicide Pasteuria cannot exceed 20 grams of each floral penetrans is exempted from the require- attractant/acre/application. ment of a tolerance in or on all raw ag- (b) [Reserved] ricultural commodities, except roots [59 FR 15857, Apr. 5, 1994] and tubers, when used as a nematicide in the production of fruits and vegeta- § 180.1128 Bacillus amyloliquefaciens bles in greenhouses. MBI600; exemption from the requirement of a tolerance. [59 FR 66741, Dec. 28, 1994]

An exemption from the requirement § 180.1139 Sodium 5-nitroguaiacolate; of a tolerance is established for resi- exemption from the requirement of dues of the biofungicide Bacillus a tolerance. amyloliquefaciens MBI600 (antecedent Bacillus subtilis MBI600) in or on all The biochemical sodium 5- food commodities, including residues nitroguiacolate is exempted from the resulting from post-harvest uses, when requirement of a tolerance when used applied or used in accordance wi as a plant growth regulator in end-use products at a concentration of 0.1% by [80 FR 78143, Dec. 16, 2015] weight and applied at an application rate of 20 g of a.i. per acre or less per § 180.1130 N-(n-octyl)-2-pyrrolidone application, in or on all food commod- and N-(n-dodecyl)-2-pyrrolidone; exemptions from the requirement of a ities. tolerance. [65 FR 66181, Nov. 3, 2000] (a) N-(n-octyl)-2-pyrrolidone and N- (n-dodecyl)-2-pyrrolidone are exempt § 180.1140 Sodium o-nitrophenolate; from the requirement of a tolerance exemption from the requirement of when used as solvents in cotton defo- a tolerance. liant formulations containing The biochemical sodium o- thidiazuron and diuron as active ingre- nitrophenolate is exempted from the dients. requirement of a tolerance when used (b) N-(n-octyl)-2-pyrrolidone is ex- as a plant growth regulator in end-use empt from the requirement of a toler- products at a concentration of 0.2% by ance when used as a solvent in formu- weight and applied at an application lations containing pyraflufen-ethyl as rate of 20 g of a.i. per acre or less per

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application, in or on all food commod- § 180.1145 Pseudomonas syringae; ex- ities. emption from the requirement of a tolerance. [65 FR 66181, Nov. 3, 2000] Pseudomonas syringae is exempted § 180.1141 Sodium p-nitrophenolate; from the requirement of a tolerance on exemption from the requirement of all raw agricultural commodities when a tolerance. applied postharvest according to good agricultural practices. The biochemical sodium p- nitrophenolate is exempted from the [60 FR 12703, Mar. 8, 1995] requirement of a tolerance when used as a plant growth regulator in end-use § 180.1146 Beauveria bassiana Strain product at a concentration of 0.3% by GHA; exemption from the requirement of a tolerance. weight and applied at an application rate of 20 g of a.i. per acre or less per Beauveria bassiana Strain GHA is ex- application, in or on all food commod- empted from the requirement of a tol- ities. erance in or on all raw agricultural commodities when applied to growing [65 FR 66181, Nov. 3, 2000] crops according to good agricultural practices. § 180.1142 1,4-Dimethylnaphthalene; exemption from the requirement of [60 FR 18547, Apr. 12, 1995] a tolerance. § 180.1148 Occlusion Bodies of the An exemption from the requirement Granulosis Virus of Cydia of a tolerance is established for the res- pomenella; tolerance exemption. idues of the plant growth regulator, An exemption from the requirement 1,4-dimethylnaphthalene (1,4-DMN), of a tolerance is established for resi- when applied postharvest to all sprout- dues of the microbial pest control ing root, tuber, and bulb crops in ac- agent Occlusion Bodies of the cordance with good agricultural prac- Granulosis Virus of Cydia pomonella tices. (codling moth) in or on all raw agricul- [77 FR 68697, Nov. 16, 2012] tural commodities. [60 FR 42450, Aug. 16, 1995] § 180.1143 Methyl anthranilate; exemption from the requirement of a tol- § 180.1149 Inclusion bodies of the erance. multi-nuclear polyhedrosis virus of Residues of methyl anthranilate, a Anagrapha falcifera; exemption from the requirement of a toler- biochemical pesticide, are exempt from ance. the requirement of a tolerance in or on all food commodities, when used in ac- The microbial pest control agent in- cordance with good agricultural prac- clusion bodies of the multi-nuclear polyhedrosis virus of Anagrapha tices. falcifera is exempted from the require- [67 FR 51088, Aug. 7, 2002] ment of a tolerance in or on all raw agricultural commodities when used to § 180.1144 Candida oleophila isolate I- control certain lepidopteran pest spe- 182; exemption from the require- cies. ment of a tolerance. [60 FR 37020, July 19, 1995] Candida oleophila isolate I-182, when used as a post-harvest biological fun- § 180.1150 6-Benzyladenine; exemption gicide, is exempted from the require- from the requirement of a toler- ment of a tolerance in or on all raw ag- ance. ricultural commodities. The biochemical plant regulator 6- [60 FR 11033, Mar. 1, 1995] benzyladenine (6–BA) is exempt from the requirement of a tolerance in or on EFFECTIVE DATE NOTE: At 81 FR 34907, June apple and pear when applied at a rate 1, 2016, § 180.1144 was removed, effective Nov. of ≤182 grams of active ingredient per 28, 2016. acre per season, and in or on pistachio

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when applied at a rate of ≤60 grams of food commodities, when used as a fun- active ingredient per acre per season. gicide, insecticide, and algaecide in accordance with good agricultual prac- [72 FR 13179, Mar. 21, 2007] tices. § 180.1153 Lepidopteran pheromones; [64 FR 7804, Feb. 17, 1999; 64 FR 14099, Mar. 24, exemption from the requirement of 1999] a tolerance. Lepidopteran pheromones that are § 180.1157 Cytokinins; exemption from naturally occurring compounds, or the requirement of a tolerance. identical or substantially similar syn- An exemption from the requirement thetic compounds, designated by an of a tolerance is established for resi- unbranched aliphatic chain (between 9 dues of cytokinins (specifically: aque- and 18 carbons) ending in an alcohol, ous extract of seaweed meal and aldehyde or acetate functional group kinetin) in or on all food commodities and containing up to 3 double bonds in when used as plant regulators on the aliphatic backbone, are exempt plants, seeds, or cuttings and on all from the requirement of a tolerance in food commodities after harvest in ac- or on all raw agricultural commodities. cordance with good agricultural prac- This exemption only pertains to those tices. situations when the pheromone is: Ap- plied to growing crops at a rate not to [64 FR 31505, June 11, 1999] exceed 150 grams active ingredient/ acre/year in accordance with good agri- § 180.1158 Auxins; exemption from the cultural practices; and applied as a requirement of a tolerance. post-harvest treatment to stored food An exemption from the requirement commodities at a rate not to exceed 3.5 of a tolerance is established for resi- grams active ingredient/1,000 ft2/year dues of auxins (specifically: indole-3- (equivalent to 150 grams active ingre- acetic acid and indole-3-butyric acid) dient/acre/year) in accordance with in or on all food commodities when good agricultural practices. used as plant regulators on plants, [71 FR 45399, Aug. 9, 2006] seeds, or cuttings and on all food commodities after harvest in accordance § 180.1154 CryIA(c) and CryIC derived with good agricultural practices. delta-endotoxins of Bacillus thuringiensis var. kurstaki encap- [64 FR 31505, June 11, 1999] sulated in killed Pseudomonas fluorescens, and the expression § 180.1159 Pelargonic acid; exemption plasmid and cloning vector genetic from the requirement of tolerances. constructs. (a) An exemption from the require- CryIA(c) and CryIC derived delta- ment of a tolerance is established for endotoxins of Bacillus thuringiensis var. residues of pelargonic acid in or on all kurstaki encapsulated in killed food commodities when used as a plant Pseudomonas fluorescens and the expres- regulator on plants, seeds, or cuttings sion plasmid and cloning vector ge- and on all food commodities after har- netic constructs are exempt from the vest in accordance with good agricul- requirement of a tolerance when used tural practices. in or on all raw agricultural commod- (b) Pelargonic acid when used as an ities. herbicide is exempt from the require- [60 FR 47489, Sept. 13, 1995] ment of a tolerance on all plant food commodities provided that: EFFECTIVE DATE NOTE: At 81 FR 34907, June 1, 2016, § 180.1154 was removed, effective Nov. (1) Applications are not made di- 28, 2016. rectly to the food commodity except when used as a harvest aid or desiccant § 180.1156 Cinnamaldehyde; exemption to: any root and tuber vegetable, bulb from the requirement of a toler- vegetable or cotton. ance. (2) When pelargonic acid is used as a Cinnamaldehyde (3-phenyl-2- harvest aid or desiccant, applications propenal) is exempted from the re- must be made no later than 24 hours quirement of a tolerance in or on all prior to harvest.

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(c) An exemption from the require- meet the polymer tolerance exemption ment of a tolerance is established for from requirements of residues of pelargonic acid in or on all premanufacturing notification under 40 raw agricultural commodities and in CFR 723.250. Polymers exempted can be processed commodities, when such resi- used as dispensers, resins, fibers, and dues result from the use of pelargonic beads, as long as the fibers, beads and acid as an antimicrobial treatment in resins particle sizes are greater than 10 solutions containing a diluted end-use microns and insoluble in water. This concentration of pelargonic acid up to exemption pertains to the acrylate 170 ppm per application on food contact polymers/copolymers used as inert in- surfaces such as equipment, pipelines, gredients for sprayable and dispenser tanks, vats, fillers, evaporators, pesticide formulations that are applied pasteurizers and aseptic equipment in on food crops. Any acrylate polymers/ restaurants, food service operations, dairies, breweries, wineries, beverage copolymers used for encapsulating ma- and food processing plants. terial must be cleared as an inert ingredient when used in pesticide formu- [62 FR 28364, May 23, 1997, as amended at 64 lation applied on food crops. FR 31505, June 11, 1999; 68 FR 7935, Feb. 19, (b) For the purposes of this exemp- 2003] tion, acrylate polymers/copolymers § 180.1160 Jojoba oil; exemption from used as inert ingredients in an end-use the requirement of a tolerance. formulation must meet the definition The insecticide and spray tank adju- for a polymer as given in 40 CFR vant jojoba oil is exempted from the 723.250(b), are not automatically ex- requirement of a tolerance in or on all cluded by 40 723.250(d), and meet the raw agricultural commodities when ap- tolerance exemption criteria in 40 CFR plied at the rate of 1.0% or less of the 723.250(e)(1), 40 CFR 723.250 (e)(2) or 40 final spray in accordance with good ag- CFR 723.250(e)(3). Therefore, acrylate ricultural practices, provided the polymers and copolymers that are al- jojoba oil does not contain ready listed in the TSCA inventory or simmondsin, simmondsin-2-ferulate, will meet the polymer tolerance ex- and related conjugated organonitriles emption under 40 CFR 723.250 as including demethyl simmondsin and amended on March 29, 1995 are covered didemethylsimmondsin. by this exemption. [61 FR 2121, Jan. 25, 1996] [61 FR 6551, Feb. 21, 1996]

§ 180.1161 Clarified hydrophobic ex- § 180.1163 Killed Myrothecium tract of neem oil; exemption from verrucaria; exemption from the re- the requirement of a tolerance. quirement of a tolerance. Clarified hydrophobic extract of Killed Myrothecium verrucaria is ex- neem oil is exempt from the require- empted from the requirement of a tol- ment of a tolerance on all food com- erance in or on all raw agricultural modities when used as a botanical fun- commodities when applied as a pre- gicide/insecticide/miticide. seed or pre- or post-planting soil treat- [67 FR 43552, June 28, 2002] ment alone or mixed with water and the mixed suspension be applied § 180.1162 Acrylate polymers and co- through drip or border irrigation sys- polymers; exemption from the re- tems and the indicator mycotoxin lev- quirement of a tolerance. els do not exceed 15 ppm. (a) Acrylate polymers and copolymers are exempt from the requirement [61 FR 11315, Mar. 20, 1996, as amended at 61 of a tolerance when used as inert ingre- FR 58332, Nov. 14, 1996] dients in pesticidal formulations applied to growing, raw agricultural com- § 180.1165 Capsaicin; exemption from modities. This tolerance exemption the requirement of a tolerance. covers the acrylate polymers/copoly- Capsaicin is exempt from the require- mers that are intrinsically safe and al- ment of a tolerance in or on all food ready listed in TSCA inventory or will commodities when used in accordance

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with approved label rates and good ag- § 180.1179 Plant extract derived from ricultural practice. Opuntia lindheimeri, Quercus falcata, Rhus aromatica, and [63 FR 39521, July 23, 1998] Rhizophoria mangle; exemption from the requirement of a toler- § 180.1167 Allyl isothiocyanate as a ance. component of food grade oil of mustard; exemption from the require- The biochemical pesticide plant ex- ment of a tolerance. tract derived from Opuntia lindheimeri, Quercus falcata, Rhus aromatica, and The insecticide and repellent Allyl Rhizophoria mangle is exempted from isothiocyanate is exempt from the re- the requirement of a tolerance in or on quirement of a tolerance for residues all raw agricultural commodities when when used as a component of food applied as a nematicide/plant regulator grade oil of mustard, in or on all raw in accordance with good agricultural agricultural commodities, when ap- practices. plied according to approved labeling. [62 FR 24842, May 7, 1997] [61 FR 24894, May 17, 1996] § 180.1180 Kaolin; exemption from the § 180.1176 Sodium bicarbonate; exemp- requirement of a tolerance. tion from the requirement of a tolerance. (a) The biochemical pesticide kaolin is temporarily exempted from the re- The biochemical pesticide sodium bi- quirement of a tolerance for residues of carbonate is exempted from the re- the insecticide Kaolin, when used on quirement of a tolerance in or on all crops (apples, apricots, bananas, beans, raw agricultural commodities when ap- cane berries, citrus fruits, corn, cotton, plied as a fungicide or post-harvest fun- cranberries, cucurbits, grapes, melons, gicide in accordance with good agricul- nuts, ornamentals, peaches, peanuts, tural practices. pears, peppers, plums, potatoes, seed [61 FR 67473, Dec. 23, 1996] crops, small grains, soybeans, strawberries, sugar beets, and tomatoes) to § 180.1177 Potassium bicarbonate; ex- control certain insect, fungus, and bac- emption from the requirement of a terial damage to plants. This tem- tolerance. porary exemption from the require- The biochemical pesticide potassium ment of a tolerance will permit the bicarbonate is exempted from the re- marketing of the food commodities in quirement of a tolerance in or on all this paragraph when treated in accord- raw agricultural commodities when ap- ance with the provisions of experimental use permit 70060–EUP–1, which plied as a fungicide or post-harvest fun- is being issued under the Federal Insec- gicide in accordance with good agricul- ticide, Fungicide, and Rodenticide Act tural practices. (FIFRA), as amended (7 U.S.C. 136). [61 FR 67473, Dec. 23, 1996] This temporary exemption from the requirement of a tolerance expires and is § 180.1178 Formic acid; exemption revoked December 31, 1999. This tem- from the requirement of a toler- porary exemption from the require- ance. ment of a tolerance may be revoked at The pesticide formic acid is exempted any time if the experimental use per- from the requirement of a tolerance in mit is revoked or if any experience or on honey and honeycomb when used with or scientific data on this pesticide to control tracheal mites and suppress indicate that the tolerance is not safe. varroa mites in bee colonies, and ap- (b) Kaolin is exempted from the re- plied in accordance with label use di- quirement of a tolerance for residues rections. when used on or in food commodities to aid in the control of insects, fungi, and [74 FR 26535, June 3, 2009] bacteria (food/feed use). [62 FR 19685, Apr. 23, 1997, as amended at 63 FR 9430, Feb. 25, 1998]

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EFFECTIVE DATE NOTE: At 81 FR 34907, June § 180.1191 Ferric phosphate; exemp- 1, 2016, § 180.1180 was revised, effective Nov. tion from the requirement of a tol- 28, 2016. For the convenience of the user, the erance. revised text is set forth as follows: An exemption from the requirement § 180.1180 Kaolin; exemption from the re- of a tolerance is established for resi- quirement of a tolerance. dues of the biochemical pesticide, fer- Kaolin is exempted from the requirement ric phosphate (FePO4, CAS No. 11045– of a tolerance for residues when used on or in 86–0) in or on all food commodities. food commodities to aid in the control of in- [62 FR 56105, Oct. 29, 1997] sects, fungi, and bacteria (food/feed use). § 180.1193 Potassium dihydrogen phos- § 180.1181 Bacillus cereus strain BPO1; phate; exemption from the require- exemption from the requirement of ment of a tolerance. a tolerance. Potassium dihydrogen phosphate is An exemption from the requirement exempted from the requirement of a of a tolerance for residues of the Bacil- tolerance in or on all food commodities lus cereus strain BPO1 in or on all raw when applied as a fungicide in accord- agricultural commodities when ap- ance with good agricultural practices. plied/used in accordance with label di- [63 FR 43085, Aug. 12, 1998] rections. § 180.1195 Titanium dioxide. [67 FR 70017, Nov. 20, 2002] Titanium dioxide (CAS Reg. No. § 180.1187 L-glutamic acid; exemption 13463–67–7) is exempted from the re- from the requirement of a toler- quirement of a tolerance for residues in ance. or on growing crops, when used as an inert ingredient (UV protectant) in L-glutamic acid is exempt from the microencapsulated formulations of the requirement of a tolerance on all food insecticide lambda cyhalothrin at no commodities when used in accordance more than 3.0% by weight of the formu- with good agricultural practices. lation and as an inert ingredient (UV- [66 FR 33198, June 21, 2001] stabilizer) at no more than 5% in pesticide formulations containing the ac- § 180.1188 Gamma aminobutyric acid; tive ingredient napropamide. exemption from the requirement of [77 FR 44155, July 27, 2012] a tolerance. Gamma aminobutyric acid is exempt § 180.1196 Peroxyacetic acid; exemp- from the requirement of a tolerance on tion from the requirement of a tol- all food commodities when used in ac- erance. cordance with good agricultural prac- (a) An exemption from the require- tices. ment of a tolerance is established for residues of peroxyacetic acid in or on [66 FR 33198, June 21, 2001] all food commodities, when such residues result from the use of peroxy- § 180.1189 Methyl salicylate; exemption acetic acid as an antimicrobial treat- from the requirement of a toler- ment in solutions containing a diluted ance. end use concentration of peroxyacetic The biochemical pesticide methyl sa- acid up to 100 ppm per application on licylate is exempt from the require- fruits, vegetables, tree nuts, cereal ment of a tolerance for residues in or grains, herbs, and spices. on food or feed when used as an insect (b) An exemption from the require- repellant in food packaging and animal ment of a tolerance is established for feed packaging at an application rate residues of peroxyacetic acid, in or on that does not exceed 0.2 mg of methyl all food commodities when used in salicylate per square inch of packaging sanitizing solutions containing a di- materials. luted end-use concentration of peroxyacetic acid up to 500 ppm, and applied [62 FR 61639, Nov. 19, 1997] to tableware, utensils, dishes, pipelines, tanks, vats, fillers, evaporators,

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pasteurizers, aseptic equipment, milk- § 180.1200 Pseudomonas fluorescens ing equipment, and other food proc- strain PRA–25; temporary exemp- essing equipment in food handling es- tion from the requirement of a tol- tablishments including, but not limited erance. to dairies, dairy barns, restaurants, A temporary exemption from the re- food service operations, breweries, quirement of a tolerance is established wineries, and beverage and food proc- for residues of the microbial pesticide, essing plants. pseudomonas fluorescens strain PRA–25 (c) An exemption from the require- when used on peas, snap beans and ment of a tolerance is established for sweet corn and will expire July 31, 2001. residues of the biochemical pesticide [63 FR 38498, July 17, 1998] peroxyacetic acid and its metabolites EFFECTIVE DATE NOTE: At 81 FR 34907, June and degradates, including hydrogen 1, 2016, § 180.1200 was removed, effective Nov. peroxide and acetic acid, in or on all 28, 2016. food commodities, when used in accordance with good agricultural prac- § 180.1201 Trichoderma harzianum tices. strain T-39; exemption from the requirement of a tolerance. [74 FR 26535, June 3, 2009, as amended at 76 FR 11969, Mar. 4, 2011] Trichoderma harzianum strain T-39 is exempt from the requirement of a tol- § 180.1197 Hydrogen peroxide; exemp- erance on all food commodities. tion from the requirement of a tol- [65 FR 38757, June 22, 2000] erance. EFFECTIVE DATE NOTE: At 81 FR 34907, June An exemption from the requirement 1, 2016, § 180.1201 was removed, effective Nov. of a tolerance is established for resi- 28, 2016. dues of hydrogen peroxide in or on all food commodities at the rate of ≤1% § 180.1202 Bacillus sphaericus; exemp- hydrogen peroxide per application on tion from the requirement of a tolerance. growing and postharvest crops. An exemption from the requirement [67 FR 41844, June 20, 2002] of a tolerance is established for residues of the microbial pesticides, Bacil- § 180.1198 Gliocladium catenulatum lus sphaericus when used in or on all strain J1446; exemption from the food crops. requirement of a tolerance. An exemption from the requirement [63 FR 48597, Sept. 11, 1998] of a tolerance is established for resi- § 180.1204 Harpin protein; exemption dues of the microbial pesticide, from the requirement of a toler- Gliocladium catenulatum strain J1446 ance. when used in or on all food commod- An exemption from the requirement ities. of a tolerance is established for resi- [63 FR 37288, July 10, 1998] dues of individual harpin proteins that meet specified physiochemical and tox- § 180.1199 icological criteria when used as bio- Lysophosphatidylethanolamine chemical pesticides on all food com- (LPE); exemption from the require- modities to enhance plant growth, ment of a tolerance. quality and yield, to improve overall An exemption from the requirement plant health, and to aid in pest man- of a tolerance is established for resi- agement. The physiochemical and toxi- dues of the biochemical pesticide cological criteria identifying harpin lysophosphatidylethanolamine in or on proteins are as follows: all food commodities. (a) Consists of a protein less than 100 kD in size, that is acidic (pI<7.0), gly- [67 FR 17636, Apr. 11, 2002] cine rich (>10%), and contains no more than one cystine residue. (b) The source(s) of genetic material encoding the protein are bacterial

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plant pathogens not known to be mam- pop, grain; and corn, pop, stover, when malian pathogens. applied/used as an antifungal agent. (c) Elicits the hypersensitive re- (d) Section 18 emergency exemptions. A sponse (HR) which is characterized as time-limited exemption from the re- rapid, localized cell death in plant tis- quirement of a tolerance is established sue after infiltration of harpin into the for residues of Aspergillus flavus AF36, intercellular spaces of plant leaves. in or on dried figs, resulting from use (d) Possesses a common secondary of the pesticide pursuant to a FIFRA structure consisting of a and b units section 18 emergency exemption. This that form an HR domain. time-limited exemption from the re- (e) Is heat stable (retains HR activity quirement of a tolerance for residues of when heated to 65 °C for 20 minutes). Aspergillus flavus AF36 in or on dried (f) Is readily degraded by a proteinase figs will expire and is revoked on De- representative of environmental condi- cember 31, 2017. tions (no protein fragments >3.5 kD after 15 minutes degradation with [68 FR 41541, July 14, 2003, as amended at 72 Subtilisin A). FR 28871, May 23, 2007; 72 FR 72965, Dec. 26, (g) Exhibits a rat acute oral toxicity 2007; 74 FR 26535, 26546, June 3, 2009; 76 FR 16301, Mar. 23, 2011; 77 FR 14291, Mar. 9, 2012; (LD50) of greater than 5,000 mg product/ 81 FR 1894, Jan. 14, 2016] kg body weight. [69 FR 24996, May 5, 2004] § 180.1207 N-acyl sarcosines and sodium N-acyl sarcosinates; exemp- § 180.1205 Beauveria bassiana ATCC tion from the requirement of a tol- #74040; exemption from the require- erance. ments of a tolerance. An exemption from the requirement An exemption from the requirement of a tolerance is established for resi- of a tolerance is established for residues of the following substances when dues of the insecticide Beauveria used as inert ingredients (surfactants) bassiana (ATCC #74040) in or on all food at levels not to exceed 10% in pesticide commodities when applied or used as formulations containing glyphosate: ground and aerial foliar sprays for use only on terrestrial crops. CAS Reg. Name No. [64 FR 22796, Apr. 28, 1999] N-acyl sarcosines. § 180.1206 Aspergillus flavus AF36; ex- N-cocoyl sarcosine mixture ...... 68411-97-2 emption from the requirement of a N-lauroyl sarcosine ...... 97-78-9 tolerance. N-myristoyl sarcosine ...... 52558-73-3 N-oleoyl sarcosine ...... 110-25-8 (a) An exemption from the require- N-stearoyl sarcosine ...... 142-48-3 ment of a tolerance is established for Sodium N-acyl sarcosinates. residues of the microbial pesticide As- N-cocoyl sarcosine sodium salt mixture ...... 61791-59-1 pergillus flavus AF36 in or on cotton, N-methyl-N-(1-oxo-9-octodecenyl) glycine .... 3624-77-9 N-methyl-N-(1-oxododecyl) glycine ...... 137-16-6 gin byproducts; cotton, hulls; cotton, N-methyl-N-(1-oxooctadecyl) glycine ...... 5136-55-0 meal; cotton, refined oil; cotton, N-methyl-N-(1-oxotetradecyl glycine ...... 30364-51-3 undelinted seed. (b) An exemption from the require- [64 FR 68046, Dec. 6, 1999] ment of a tolerance is established for residues of Aspergillus flavus AF36 in or § 180.1209 Bacillus subtilis strain QST on pistachio when applied as an 713 and strain QST 713 variant soil; antifungal agent and used in accord- exemption from the requirement of ance with good agricultural practices. a tolerance. (c) An exemption from the require- An exemption from the requirement ment of a tolerance is established for of a tolerance is established for resi- residues of Aspergillus flavus AF36 in or dues of the microbial pesticides Bacil- on corn, field, forage; corn, field, grain; lus subtilis strain QST 713 and strain corn, field, stover; corn, field, aspirated QST 713 variant soil when used in or on grain fractions; corn, sweet, kernel all food commodities. plus cob with husk removed; corn, sweet, forage; corn, sweet, stover; corn, [77 FR 73937, Dec. 12, 2012]

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§ 180.1210 Phosphorous acid; exemp- herbicide in accordance with good agri- tion from the requirement of a tol- cultural practices. erance. [74 FR 26535, June 3, 2009] An exemption from the requirement of a tolerance is established for resi- § 180.1220 1-Methylcyclopropene; ex- dues of phosphorous acid and its am- emption from the requirement of a monium, sodium, and potassium salts tolerance. in or on all food commodities when An exemption from the requirement used as an agricultural fungicide and in of a tolerance is established for resi- or on potatoes when applied as a post- dues of the 1-Methylcyclopropene in or harvest treatment at 35,600 ppm or less on fruits and vegetables when: phosphorous acid. (a) Used as a post harvest plant [71 FR 49373, Aug. 23, 2006] growth regulator, i.e., for the purpose of inhibiting the effects of ethylene. § 180.1212 Pseudomonas chlororaphis (b) Applied or used outdoors for pre- Strain 63–28; exemption from the requirement of a tolerance. harvest treatments. An exemption from the requirement [73 FR 19150, Apr. 9, 2008] of a tolerance is established for residues of the microbial pesticide § 180.1221 Pseudozyma flocculosa Pseudomonas chlororaphis Strain 63–28 strain PF-A22 UL; exemption from the requirement of a tolerance. in or on all food commodities. An exemption from the requirement [66 FR 53346, Oct. 22, 2001] of a tolerance is established for resi- § 180.1213 Coniothyrium minitans dues of Pseudozyma flocculosa strain strain CON/M/91–08; exemption PF-A22 UL in or on all food commod- from the requirement of a toler- ities. ance. [67 FR 60966, Sept. 27, 2002] An exemption from the requirement of a tolerance is established for resi- EFFECTIVE DATE NOTE: At 81 FR 34907, June 1, 2016, § 180.1221 was removed, effective Nov. dues of the microbial pesticide 28, 2016. Coniothyrium minitans strain CON/M/91– 08 when used in or on all food commod- § 180.1222 Sucrose octanoate esters; ities. exemption from the requirement of [66 FR 16874, Mar. 28, 2001] a tolerance. An exemption from the requirement § 180.1218 Indian Meal Moth of a tolerance is established for resi- Granulosis Virus; exemption from dues of sucrose octanoate esters [(a-D- the requirement of a tolerance. glucopyranosyl-b-D-fructofuranosyl-oc- An exemption from the requirement tanoate), mono-, di-, and triesters of of a tolerance is established for resi- sucrose octanoate] in or on all food dues of the microbial pesticide Indian commodities when used in accordance Meal Moth Granulosis Virus when used with good agricultural practices. in or on all food commodities. [67 FR 60152, Sept. 25, 2002] [68 FR 55875, Sept. 29, 2003] § 180.1223 Imazamox; exemption from § 180.1219 Foramsulfuron; exemption the requirement of a tolerance. from the requirement of a tolerance. The herbicide imazamox, (±) 2, -[4,5- dihydro-4-methyl-4-(1-methylethyl)-5- The pesticide foramsulfuron is ex- oxo-1H-imidazol-2-yl]-5- empted from the requirement of a tol- (methoxymethyl)-3-pyridinecarboxylic erance in corn, field, grain/corn, field, acid, is exempt from the requirement forage/ corn, field, stover/corn, pop, of a tolerance on all food commodities grain/corn, pop, forage/corn, pop, sto- when applied as a herbicide in accord- ver; corn, sweet, forage; corn, sweet, ance with good agricultural practices. kernel plus cob with husks removed; corn, sweet, stover when applied as a [68 FR 7433, Feb. 14, 2003]

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§ 180.1224 Bacillus pumilus GB34; ex- § 180.1230 Ferrous sulfate; exemption emption from the requirement of a from the requirement of a toler- tolerance. ance. An exemption from the requirement An exemption from the requirement of a tolerance is established for resi- of a tolerance is established for residues of the microbial pesticide Bacillus dues of ferrous sulfate. pumilus GB34 when used as a seed treatment in or on all food commodities. An [70 FR 33363, June 8, 2005] exemption is also granted for such resi- § 180.1231 Lime; exemption from the dues on treated but unplanted soybean requirement of a tolerance. seeds. An exemption from the requirement [69 FR 76625, Dec. 22, 2004] of a tolerance is established for residues of lime. § 180.1225 Decanoic acid; exemption from the requirement of a toler- [70 FR 33363, June 8, 2005] ance. An exemption from the requirement § 180.1232 Lime-sulfur; exemption from the requirement of a tolerance. of a tolerance is established for residues of decanoic acid in or on all raw An exemption from the requirement agricultural commodities and in proc- of a tolerance is established for resi- essed commodities, when such residues dues of lime-sulfur. result from the use of decanoic acid as [70 FR 33363, June 8, 2005] an antimicrobial treatment in solutions containing a diluted end-use con- § 180.1233 Potassium sorbate; exemp- centration of decanoic acid (up to 170 tion from the requirement of a tol- ppm per application) on food contact erance. surfaces such as equipment, pipelines, tanks, vats, fillers, evaporators, An exemption from the requirement pasteurizers and aseptic equipment in of a tolerance is established for resi- restaurants, food service operations, dues of potassium sorbate. dairies, breweries, wineries, beverage [70 FR 33363, June 8, 2005] and food processing plants. § 180.1234 Sodium carbonate; exemp- [68 FR 7939, Feb. 19, 2003; 68 FR 17308, Apr. 9, tion from the requirement of a tol- 2003] erance. § 180.1226 Bacillus pumilus strain An exemption from the requirement QST2808; temporary exemption of a tolerance is established for resi- from the requirement of a toler- dues of sodium carbonate. ance. A temporary exemption from the re- [70 FR 33363, June 8, 2005] quirement of a tolerance is established § 180.1235 Sodium hypochlorite; ex- for residues of the microbial pesticide emption from the requirement of a Bacillus pumilus strain QST2808 when tolerance. used in or on all agricultural commodities when applied/used in accordance An exemption from the requirement with label directions. of a tolerance is established for residues of sodium hypochlorite. [68 FR 36480, June 18, 2003] [70 FR 33363, June 8, 2005] § 180.1228 Diallyl sulfides; exemption from the requirement of a toler- § 180.1236 Sulfur; exemption from the ance. requirement of a tolerance. An exemption from the requirement An exemption from the requirement of a tolerance is established for resi- of a tolerance is established for residues of diallyl sulfides when used in/on dues of sulfur. garlic, leeks, onions, and shallots. [70 FR 33363, June 8, 2005] [68 FR 40808, July 9, 2003]

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§ 180.1237 Sodium metasilicate; exemp- ance for residues of eucalyptus oil will tion from the requirement of a tol- expire and are revoked on June 30, 2007. erance. [70 FR 37696, June 30, 2005] (a) An exemption from the requirement of a tolerance is established for EFFECTIVE DATE NOTE: At 81 FR 34907, June residues of sodium metasilicate in or 1, 2016, § 180.1241 was removed, effective Nov. on all food commodities when used in 28, 2016. accordance with approved label rates § 180.1243 Bacillus subtilis var. and good agricultural practices as a amyloliquefaciens strain FZB24; ex- plant desiccant, so long as the sodium emption from the requirement of a metasilicate does not exceed 4% by tolerance. weight in aqueous solution. (b) An exemption from the require- An exemption from the requirement ment of a tolerance is established for of a tolerance for residues of the Bacil- residues of sodium metasilicate in or lus subtilis var. amyloliquefaciens strain on all food commodities when used in FZB24 in or on all agricultural com- accordance with approved label rates modities when applied/used in accord- and good agricultural practices as an ance with label directions. insecticide and fungicide, so long as [68 FR 44640, July 30, 2003] the sodium metasilicate does not exceed 2.41% by weight in aqueous solu- § 180.1244 Ammonium bicarbonate; ex- tion. emption from the requirement of a [71 FR 19441, Apr. 14, 2006] tolerance. An exemption from the requirement § 180.1240 Thymol; exemption from the of tolerance is established for residues requirement of a tolerance. of ammonium bicarbonate used in or (a) Time-limited exemptions from on all food commodities when used in the requirement of a tolerance are es- accordance with good agricultural tablished for residues of thymol on practices. honey and honeycomb in connection with use of the pesticide under section [69 FR 13745, Mar. 24, 2004] 18 emergency exemptions granted by the EPA. These time-limited exemp- § 180.1245 Rhamnolipid biosurfactant; tions from the requirement of a toler- exemption from the requirement of ance for residues of thymol will expire a tolerance. and are revoked on June 30, 2007. An exemption from the requirement (b) An exemption from the require- of a tolerance is established for resi- ment of a tolerance for residues of the dues of rhamnolipid biosurfactant thymol (as present in thyme oil) in or when used in accordance with good ag- on food commodities when applied/used ricultural practices as a fungicide in or in/on public eating places, dairy proc- on all food commodities. essing equipment, and/or food processing equipment and utensils. [69 FR 16800, Mar. 31, 2004] [70 FR 37696, June 30, 2005, as amended at 71 § 180.1246 Yeast Extract Hydrolysate FR 2895, Jan. 18, 2006; 74 FR 12617, Mar. 25, from Saccharomyces cerevisiae: ex- 2009] emption from the requirement of a tolerance. § 180.1241 Eucalyptus oil; exemption from the requirement of a toler- This regulation establishes an ex- ance. emption from the requirement of a tol- Time-limited exemptions from the erance for residues of the biochemical requirement of a tolerance are estab- pesticide Yeast Extract Hydrolysate lished for residues of eucalyptus oil on from Saccharomyces cerevisiae on all honey and honeycomb in connection food commodities when applied/used with use of the pesticide under section for the management of plant diseases. 18 emergency exemptions granted by [69 FR 9958, Mar. 3, 2004] the EPA. These time-limited exemptions from the requirement of a toler-

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§ 180.1248 Exemption of citronellol residues of Aspergillus flavus NRRL from the requirement of a toler- 21882 on corn, field, forage; corn, field, ance. grain; corn, field, stover; corn, field, as- An exemption from the requirement pirated grain fractions; corn, sweet, of a tolerance is established for resi- kernel plus cob with husk removed; dues of the biochemical pesticide corn, sweet, forage; corn, sweet, stover; citronellol in or on all food commod- corn, pop, grain; and corn, pop, stover. ities. [75 FR 6576, Feb. 10, 2010] [69 FR 23146, Apr. 28, 2004] § 180.1255 Bacillus pumilus strain QST § 180.1250 C8, C10, and C12 fatty acid 2808; exemption from the require- monoesters of glycerol and pro- ment of a tolerance. pylene glycol; exemption from the An exemption from the requirement requirement of a tolerance. of a tolerance is established for resi- The C8, C10, and C12 straight-chain dues of the microbial pesticide Bacillus fatty acid monoesters of glycerol (glyc- pumilus strain QST 2808 when used in or erol monocaprylate, glycerol on all agricultural commodities when monocaprate, and glycerol applied/used in accordance with label monolaurate) and propylene glycol directions. (propylene glycol monocaprylate, pro- [69 FR 63954, Nov. 3, 2004] pylene glycol monocaprate, and propylene glycol monolaurate) are exempt § 180.1256 Alternaria destruens strain from the requirement of a tolerance in 059; exemption from the require- or on all food commodities when used ment of a tolerance. in accordance with approved label rates An exemption from the requirement and good agricultural practice. of a tolerance is established for resi- [69 FR 34944, June 23, 2004] dues of the microbial pesticide Alternaria destruens Strain 059 when § 180.1251 Geraniol; exemption from used in or on all raw agricultural com- the requirement of a tolerance. modities when applied/used in accord- An exemption from the requirement ance with label directions. of a tolerance is established for resi- [70 FR 28459, May 18, 2005] dues of the biochemical pesticide geraniol in or on all food commodities. EFFECTIVE DATE NOTE: At 81 FR 34907, June 1, 2016, § 180.1256 was removed, effective Nov. [69 FR 23151, Apr. 28, 2004] 28, 2016.

§ 180.1253 Streptomyces lydicus WYEC § 180.1257 Paecilomyces lilacinus 108; exemption from the require- strain 251; exemption from the re- ment of a tolerance. quirement of a tolerance. An exemption from the requirement An exemption from the requirement of a tolerance is established for resi- of a tolerance is established for residues of the microbial pesticide dues of the microbial pesticide Streptomyces lydicus WYEC 108 when Paecilomyces lilacinus strain 251 when used in or on all agricultural commod- used in or on all agricultural commodities when applied/used in accordance ities when applied/used in accordance with label directions. with label directions. [69 FR 31301, June 3, 2004] [70 FR 19283, Apr. 13, 2005]

§ 180.1254 Aspergillus flavus NRRL § 180.1258 Acetic acid; exemption from 21882; exemption from the require- the requirement of a tolerance. ment of a tolerance. (a) An exemption from the require- (a) An exemption from the requirement of a tolerance is established for ment of a tolerance is established for residues of the biochemical pesticide residues of Aspergillus flavus NRRL acetic acid when used as a preservative 21882 on peanut; peanut, hay; peanut, on post-harvest agricultural commod- meal; and peanut, refined oil. ities intended for animal feed, includ- (b) An exemption from the require- ing Alfalfa, seed; alfalfa, hay; barley, ment of a tolerance is established for grain; bermudagrass, hay; bluegrass,

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hay; bromegrass, hay; clover, hay; § 180.1262 Sorbitol octanoate; exemp- corn, field, grain; corn, pop, grain; tion from the requirement of a tol- cowpea, hay; fescue, hay; lespedeza, erance. hay; lupin; oat, grain; orchardgrass, An exemption from the requirement hay; peanut, hay; timothy, hay; vetch, of a tolerance is established for resi- hay; and wheat, grain, or commodities dues of sorbitol octanoate in or on all described as grain or hay. food commodities when used in accord- (b) An exemption from the require- ance with label directions. ment of a tolerance is established for residues of acetic acid in or on all food [71 FR 4518, Jan. 27, 2006] crops resulting from unintentional § 180.1263 Tetrahydrofurfuryl alcohol; spray and drift to non-target vegeta- exemption from the requirement of tion including non-food, food and feed a tolerance. crops when used as a non-selective contact herbicide spray. Tetrahydrofurfuryl alcohol (THFA, CAS Reg. No. 97–99–4) is exempt from [75 FR 40741, July 14, 2010] the requirement of a tolerance in or on all raw agricultural commodities when § 180.1259 Reynoutria sachalinensis ex- used in accordance with good agricul- tract; exemption from the require- tural practices as an inert ingredient ment of a tolerance. applied only: Residues of the biochemical pesticide (a) For use as a seed treatment. Reynoutria sachalinensis extract, when (b) For applications prior to planting derived from the whole plant extract, and at the time of planting. are exempt from the requirement of a (c) For use on cotton. tolerance in or on all food commod- (d) For use in herbicides with one ap- ities. plication to wheat and barley prior to [70 FR 55277, Sept. 21, 2005] the pre-boot stage, and two applications to canola and soybeans pre- § 180.1260 Muscodor albus QST 20799 bloom. and the volatiles produced on re- (e) For use in herbicides with two ap- hydration; exemption from the re- plications to field corn up to 24 inches quirement of a tolerance. tall (V 5 stage). An exemption from the requirement of a tolerance is established on all food/ [71 FR 45415, Aug. 9, 2006] feed commodities, for residues of § 180.1267 Pantoea agglomerans strain Muscodor albus QST 20799, and the C9–1; exemption from the require- volatiles produced on its rehydration, ment of a tolerance. when the pesticide is used for all agri- An exemption from the requirement cultural applications, including seed, of a tolerance is established for resi- propagule and post harvest treatments. dues of Pantoea agglomerans strain C9–1 [70 FR 56576, Sept. 28, 2005] when used on apples and pears.

§ 180.1261 Xanthomonas campestris pv. [71 FR 24596, Apr. 26, 2006] vesicatoria and Pseudomonas syringae pv. tomato specific § 180.1268 Potassium silicate; exemp- Bacteriophages. tion from the requirement of a tolerance. An exemption from the requirement of a tolerance is established for resi- Potassium silicate is exempt from dues of Xanthomonas campestris pv. the requirement of a tolerance in or on vesicatoria and Pseudomonas syringae pv. all food commodities so long as the po- tomato specific bacteriophages in or on tassium silicate is not applied at rates pepper and tomato. exceeding 1% by weight in aqueous solution and when used in accordance [74 FR 26536, June 3, 2009] with good agricultural practices. [71 FR 34272, June 14, 2006]

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§ 180.1269 Bacillus mycoides isolate J; § 180.1274 Tris (2-ethylhexyl) phos- exemption from the requirement of phate; exemption from the require- a tolerance. ment of a tolerance. Bacillus mycoides isolate J is tempo- Tris (2-ethylhexyl) phosphate (TEHP, rarily exempt from the requirement of CAS Reg. No. 78–42–2) is exempt from a tolerance when used as a fungicide on the requirement of a tolerance for resi- potatoes in accordance with a valid dues in grain, aspirated fractions; bar- Federal Insecticide, Fungicide, and ley, grain, barley, hay, barley, straw; Rodenticide Act (FIFRA) section 18 wheat, grain; wheat, forage; wheat, emergency exemption. This temporary hay; wheat, straw when used under the exemption from the requirement of a following conditions: tolerance expires and is revoked on De- (a) The use is in accordance with cember 31, 2015. good agricultural practices; [78 FR 24353, Apr. 25, 2013] (b) Tris (2-ethylhexyl) phosphate is used as an inert ingredient in pesticide § 180.1270 Isophorone; exemption from formulations with the active ingredi- the requirement of a tolerance. ents pinoxaden, clodinafop-propargyl, Isophorone (CAS Reg. No. 78–59–1) is and tralkoxydium; exempt from the requirement of a tol- (c) Tris (2-ethylhexyl) phosphate is erance when used as an inert ingre- applied no more than twice per season; dient in pesticide formulations applied and to beets, ginseng, rice, spinach, sugar (d) The applications occur no later beets, and Swiss chard. than the pre-boot stage (prior to formation of edible grain). [71 FR 45408, Aug. 9, 2006] [72 FR 5624, Feb. 7, 2007, as amended at 74 FR § 180.1271 Eucalyptus oil; exemption 26536, June 3, 2009] from the requirement of a tolerance. § 180.1275 Pythium; exception from the An exemption from the requirement requirement of a tolerance. of tolerance is established for residues An exemption from the requirement of eucalyptus oil in or on honey, hon- of tolerance is established on all food/ eycomb, and honeycomb with honey feed commodities, for residues of when used at 2g or less eucalyptus oil pythium oligandrum DV 74 when the pes- per hive, where the eucalyptus oil con- ticide is used on food crops. tains 80% or more eucalyptol. [72 FR 27452, May 16, 2007]

[71 FR 53979, Sept. 13, 2006] EFFECTIVE DATE NOTE: At 81 FR 34907, June 1, 2016, § 180.1275 was revised, effective Nov. § 180.1272 Pantoea agglomerans strain 28, 2016. For the convenience of the user, the E325; exemption from the require- revised text is set forth as follows: ment of a tolerance. An exemption from the requirement § 180.1275 Pythium oligandrum DV 74; exemption from the requirement of a toler- of a tolerance is established for resi- ance. dues of Pantoea agglomerans strain E325 An exemption from the requirement of a when used on apples and pears. tolerance is established on all food/feed com- [71 FR 54933, Sept. 20, 2006] modities for residues of Pythium oligandrum DV 74 when the pesticide is used on food § 180.1273 Beauveria bassiana HF23; crops. exemption from the requirement of a tolerance. § 180.1276 Tobacco mild green mosaic tobamovirus strain U2; exemption Residues of Beauveria bassiana HF23 from the requirement of a toler- are exempt from the requirement of a ance. tolerance on all food/feed commodities, An exemption from the requirement when the pesticide is used for the of a tolerance is established for resi- treatment of chicken and livestock fa- dues of Tobacco mild green mosaic cilities, including the treatment of tobamovirus strain U2 in or on all com- chicken and livestock manure. modities of crop groups 17 and 18 when [75 FR 10190, Mar. 5, 2010] applied as a post-emergent herbicide

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and used in accordance with label di- § 180.1281 S-Abscisic Acid, (S)-5-(1-hy- rections and good agricultural prac- droxy-2,6,6-trimethyl-4-oxo-1- tices. cyclohex-2-enyl)-3-methyl-penta- (2Z,4E)-dienoic Acid; exemption [79 FR 75756, Dec. 19, 2014] from the requirement of a tolerance. § 180.1277 Dibasic esters; exemption from the requirement of a toler- An exemption from the requirement ance. of a tolerance is established for resi- Dibasic esters (CAS Reg. No. 95481–62– dues of S-Abscisic Acid in or on all food 2) is exempted from the requirement of commodities when applied or used a tolerance for residues when used as preharvest as a plant regulator. an inert ingredient (solvent and/or [75 FR 11744, Mar. 12, 2010] anti-freeze) at 10% W/W or less in microencapsulated pesticide formula- § 180.1282 Bacillus firmus I-1582; ex- tions with the active ingredient emption from the requirement of a cyfluthrin. tolerance. [73 FR 10398, Feb. 27, 2008] An exemption from the requirement of a tolerance is established in/on all § 180.1278 Quillaja saponaria extract food/feed commodities, for residues of (saponins); exemption from the re- Bacillus firmus I-1582 when used as a soil quirement of a tolerance. application or seed treatment. Residues of the biochemical pesticide [73 FR 25528, May 7, 2008] Quillaja saponaria extract (saponins) are exempt from the requirement of a § 180.1283 (Z)-7,8-epoxy-2- tolerance in or on all food commod- methyloctadecane (Disparlure); ex- ities. emption from the requirement of a [72 FR 41935, Aug. 1, 2007] tolerance. An exemption from the requirement § 180.1279 Zucchini yellow mosaic of a tolerance is established for resi- virus—weak strain; exemption from dues of (Z)-7,8-epoxy-2- the requirement of a tolerance. methyloctadecane on all food and feed An exemption from the requirement crops that occur when it is used to of a tolerance for residues of the treat trees, shrubs, and pastures and ZYMV–WK strain in or on all raw such use results in unintentional spray cucurbit when applied/used in accord- and drift to non-target vegetation in- ance with label directions. cluding non-food, food, and feed crops. [74 FR 26536, June 3, 2009] This active ingredient is also known as Disparlure. EFFECTIVE DATE NOTE: At 81 FR 34907, June 1, 2016, § 180.1279 was removed, effective Nov. [73 FR 33714, June 13, 2008] 28, 2016. § 180.1284 Ammonium salts of higher § 180.1280 fatty acids (C 8-C 18 saturated; C 8-C 12 Poly(hexamethylenebiguanide) hy- unsaturated); exemption from the drochloride (PHMB); exemption requirement of a tolerance. from the requirement of a tolerance. Ammonium salts of C8-C18 saturated and C -C unsaturated higher fatty Poly(hexamethylenebiguanide) hy- 8 12 drochloride (PHMB)(CAS Reg. No. acids are exempted from the require- 32289–58–0) is exempt from the requirement of a tolerance for residues in or ment of a tolerance for residues of the on all food commodities when used in antimicrobial in or on all food com- accordance with good agricultural modities when the residues are the re- practice. sult of the lawful application of a food [74 FR 47457, Sept. 16, 2009] contact surface sanitizer containing PHMB at 550 parts per million (ppm). [73 FR 1517, Jan. 9, 2008]

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§ 180.1285 Polyoxin D zinc salt; exemp- § 180.1290 Pasteuria usgae; exemption tion from the requirement of a tol- from the requirement of a toler- erance. ance. An exemption from the requirement An exemption from the requirement of a tolerance is established for the res- of a tolerance is established for resi- idues of polyoxin D zinc salt in or on dues of Pasteuria usgae in or on all food all food commodities when applied as a commodities when applied preharvest fungicide and used in accordance with and used as a nematicide in accordance good agricultural practices. with good agricultural practices. [77 FR 56133, Sept. 12, 2012] [75 FR 37737, June 30, 2010]

§ 180.1287 Extract of Chenopodium § 180.1291 Cold pressed neem oil; ex- ambrosioides near ambrosioides; exemption from the requirement of a emption from the requirement of a tolerance. tolerance. Residues of the biochemical pesticide An exemption from the requirement cold pressed neem oil are exempt from of a tolerance is established for the res- the requirement of a tolerance in or on idues of Extract of Chenopodium all food commodities. ambrosioides near ambrosioides when [74 FR 55463, Oct. 28, 2009] used as an insecticide/acaricide on all food commodities. § 180.1292 Ulocladium oudemansii (U3 [74 FR 634, Jan. 7, 2009] Strain); exemption from the requirement of a tolerance. § 180.1288 Tristyrylphenol ethoxylates; An exemption from the requirement exemption from the requirement of of a tolerance is established in/on all a tolerance. food commodities for residues of An exemption from the requirement Ulocladium oudemansii (U3 Strain), of a tolerance is established for resi- when applied or used pre-harvest-only, dues of poly(oxy-1,2-ethanediyl), a- excluding applications made post-har- [2,4,6-tris(1-phenylethyl)phenyl]-w-hy- vest or to processed commodities, as a droxy-, (CAS Reg. No. 70559–25–0) and microbial fungicide in accordance with poly(oxy-1,2-ethanediyl), a-[tris(1- good agricultural practices. phenylethyl)phenyl]-w-hydroxy-, (CAS [74 FR 55458, Oct. 28, 2009] Reg. No. 99734–09–5) on citrus crops, group 10, when used as inert ingredi- § 180.1293 Trichoderma gamsii strain ents under the following conditions: ICC 080; exemption from the re- (a) They are applied post-harvest; quirement of a tolerance. (b) They are used as inert ingredients Trichoderma gamsii strain ICC 080 is in pesticide formulations with exempted from the requirement of a azoxystrobin and fludioxonil; and tolerance in or on all food and feed (c) They constitute no more than commodities when applied preharvest 10.0% of the formulated pesticide prod- and used in accordance with good agri- uct. cultural practices. [74 FR 12625, Mar. 25, 2009] [75 FR 8507, Feb. 25, 2010]

§ 180.1289 Candida oleophila Strain O; § 180.1294 Trichoderma asperellum exemption from the requirement of strain ICC 012; exemption from the a tolerance. requirement of a tolerance. An exemption from the requirement Trichoderma asperellum strain ICC 012 of a tolerance is established for the res- is exempted from the requirement of a idues of the microbial pesticide, tolerance in or on all food and feed Candida oleophila Strain O, on apples commodities when applied pre-harvest and pears when applied/used as a post- and used in accordance with good agri- harvest biofungicide. cultural practices. [74 FR 22464, May 13, 2009] [75 FR 9530, Mar. 3, 2010]

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§ 180.1295 Laminarin; exemption from apple and grape pre-harvest, in accord- the requirement of a tolerance. ance with label directions and good ag- An exemption from the requirement ricultural practices. of a tolerance is established for resi- [78 FR 75257, Dec. 11, 2013] dues of laminarin in or on all food commodities when laminarin is applied § 180.1300 Potassium hypochlorite; ex- preharvest. emption from the requirement of a [75 FR 8256, Feb. 24, 2010] tolerance. An exemption from the requirement α § 180.1296 Terpene Constituents -ter- of a tolerance is established for resi- pinene, d-limonene and p-cymene, dues of potassium hypochlorite in or on of the Extract of Chenopodium ambrosioides near ambrosioides as all commodities. Synthetically Manufactured; exemp- [76 FR 11343, Mar. 2, 2011] tion from the requirement of a tolerance. § 180.1301 Escherichia coli O157:H7 An exemption from the requirement specific bacteriophages; temporary of a tolerance is established for the res- exemption from the requirement of idues of the biochemical pesticide Ter- a tolerance. pene Constituents a-terpinene, d-limo- A temporary exemption from the re- nene and p-cymene, of the Extract of quirement of a tolerance is established Chenopodium ambrosioides near for residues of lytic bacteriophages ambrosioides as Synthetically Manufac- that are specific to Escherichia coli tured when used as an insecticide/acar- O157:H7, sequence negative for shiga icide in or on all food commodities. toxins I and II, and grown on [75 FR 39455, July 9, 2010] atoxigenic host bacteria when used/applied on food contact surfaces in food § 180.1297 Homobrassinolide; exemp- processing plants in accordance with tion from the requirement of a tolerance. the terms of Experimental Use Permit (EUP) No. 74234–EUP–2. This temporary An exemption from the requirement exemption expires on April 1, 2013. of a tolerance is established for the residues of homobrassinolide in or on all [76 FR 20546, Apr. 13, 2011] food commodities when applied/used as a plant growth regulator in accordance § 180.1302 Sodium Ferric Ethylene- with good agricultural practices. diaminetetraacetate (EDTA); exemption from the requirement of a [75 FR 39459, July 9, 2010] tolerance. § 180.1298 Trichoderma hamatum iso- An exemption from the requirement late 382; exemption from the re- of a tolerance is established for resi- quirement of a tolerance. dues of sodium ferric EDTA in or on all An exemption from the requirement food commodities when applied as a of a tolerance is established for resi- molluscicide and used in accordance dues of Trichoderma hamatum isolate 382 with good agricultural practices. in or on all food commodities when ap- [76 FR 17561, Mar. 30, 2011] plied as a fungicide and used in accordance with good agricultural practices. § 180.1303 Metarhizium anisopliae [75 FR 43076, July 23, 2010] strain F52; exemption from the requirement of a tolerance. § 180.1299 Prohydrojasmon; exemption An exemption from the requirement from the requirement of a tolerance. of a tolerance is established for residues of Metarhizium anisopliae strain An exemption from the requirement F52 in or on all food commodities when of a tolerance is established for resi- applied as an insecticide, miticide, or dues of the biochemical pesticide ixodicide and used in accordance with prohydrojasmon (PDJ), propyl-3-oxo-2- good agricultural practices. pentylcyclo-pentylacetate, when used as a plant growth regulator in or on [76 FR 26198, May 6, 2011]

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§ 180.1304 Pseudomonas fluorescens dues of the microbial pesticide, Bacillus strain CL145A; exemption from the amyloliquefaciens strain D747 in or on requirement of a tolerance. all food commodities when used in ac- An exemption from the requirement cordance with good agricultural prac- of a tolerance is established for resi- tices. dues of Pseudomonas fluorescens strain [77 FR 749, Jan. 6, 2012. Redesignated at 77 CL145A in or on all food commodities FR 2911, Jan. 20, 2012] when applied as a molluscicide. [76 FR 52875, Aug. 24, 2011] § 180.1309 Bacillus subtilis strain CX– 9060; exemption from the require- § 180.1305 Chromobacterium ment of a tolerance. subtsugae strain PRAA4–1T; exemption from the requirement of a tol- An exemption from the requirement erance. of a tolerance is established for residues of the microbial pesticide Bacillus An exemption from the requirement subtilis strain CX–9060, in or on all food of a tolerance is established for residues of Chromobacterium subtsugae commodities, when applied or used in strain PRAA4–1T in or on all food com- accordance with good agricultural modities when applied as an insecticide practices. or miticide and used in accordance [77 FR 1637, Jan. 11, 2012] with good agricultural practices. [76 FR 55272, Sept. 7, 2011] § 180.1310 Trichoderma virens strain G–41; exemption from the require- § 180.1306 Isaria fumosorosea (for- ment of a tolerance. merly Paecilomyces fumosoroseus) An exemption from the requirement Apopka strain 97; exemption from of a tolerance is established for resi- the requirement of a tolerance. dues of Trichoderma virens strain G–41, An exemption from the requirement in or on all food commodities, when ap- of a tolerance is established for resi- plied as a fungicide and used in accord- dues of Isaria fumosorosea (formerly ance with good agricultural practices. Paecilomyces fumosoroseus) Apopka strain 97 in or on all food commodities [77 FR 4908, Feb. 1, 2012] when applied as an insecticide or miticide and used in accordance with § 180.1311 Pasteuria nishizawae—Pn1; good agricultural practices. exemption from the requirement of a tolerance. [76 FR 59905, Sept. 28, 2011] An exemption from the requirement § 180.1307 Bacteriophage of of a tolerance is established for resi- Clavibacter michiganensis sub- dues of Pasteuria nishizawae—Pn1 in or species michiganensis; exemption on all food commodities when applied from the requirement of a toler- as a nematicide and used in accordance ance. with good agricultural practices. An exemption from the requirement of a tolerance is established for resi- [77 FR 8741, Feb. 15, 2012] dues of lytic bacteriophage of Clavibacter michiganensis subspecies § 180.1312 Aureobasidium pullulans michiganensis produced in Clavibacter strains DSM 14940 and DSM 14941; exemption from the requirement of michiganensis subspecies a tolerance. michiganensis in or on tomato when applied as a bactericide in accordance An exemption from the requirement with good agricultural practices. of a tolerance is established for residues of Aureobasidium pullulans strains [76 FR 66192, Oct. 26, 2011] DSM 14940 and DSM 14941 in or on all § 180.1308 Bacillus amyloliquefaciens food commodities when used in accord- strain D747; exemption from the re- ance with label directions and good ag- quirement of a tolerance. ricultural practices. An exemption from the requirement [80 FR 73662, Nov. 25, 2015] of a tolerance is established for resi-

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§ 180.1313 Bacillus pumilus strain dues of Didecyl dimethyl ammonium GHA 180; exemption from the re- chloride in or on broccoli resulting quirement of a tolerance. from the use of Didecyl dimethyl am- An exemption from the requirement monium chloride as a seed treatment of a tolerance is established for resi- at a treatment concentration of 1200 dues of Bacillus pumilus strain GHA 180 ppm prior to planting by immersion. in or on all food commodities when [77 FR 47296, Aug. 8, 2012] used in accordance with good agricultural practices. § 180.1318 3-decen-2-one; exemption [77 FR 19112, Mar. 30, 2012] from the requirement of a tolerance. § 180.1314 Killed, nonviable An exemption from the requirement Streptomyces acidiscabies strain of a tolerance is established for resi- T RL–110 ; exemption from the re- dues of the biochemical pesticide, 3- quirement of a tolerance. decen-2-one, in or on potatoes when ap- An exemption from the requirement plied as a potato sprout inhibitor and of a tolerance is established for resi- used in accordance with label direc- dues of killed, nonviable Streptomyces tions and good agricultural practices. acidiscabies strain RL–110T in or on all food commodities when applied as a [78 FR 11766, Feb. 20, 2013] pre- or post-emergent herbicide and § 180.1319 Banda de Lupinus albus used in accordance with good agricul- doce (BLAD); exemption from the tural practices. requirement of a tolerance. [77 FR 35295, June 13, 2012] An exemption from the requirement of a tolerance is established for the res- § 180.1315 Natamycin; exemption from idues of Banda de Lupinus albus doce the requirement of a tolerance. (BLAD), a naturally occurring An exemption from the requirement polypeptide from the catabolism of a of a tolerance is established for resi- seed storage protein (b-conglutin) of dues of natamycin in or on mushrooms sweet lupines (Lupinus albus), in or on when applied as a fungistat to prevent all food commodities when applied as a the germination of fungal spores on fungicide and used in accordance with mushrooms produced in enclosed mush- label directions and good agricultural room production facilities, and in or on practices. pineapples when applied as a fungistat in accordance with label directions and [78 FR 17604, Mar. 22, 2013] good agricultural practices. § 180.1320 Methyl jasmonate; exemp- [79 FR 75068, Dec. 17, 2014] tion from the requirement of a tolerance. § 180.1316 Pasteuria spp. An exemption from the requirement (Rotylenchulus reniformis nematode)—Pr3; exemption from the re- of a tolerance is established for resi- quirement of a tolerance. dues of methyl jasmonate in or on all food commodities when methyl An exemption from the requirement jasmonate is applied pre-harvest. of a tolerance is established for residues of Pasteuria spp. (Rotylenchulus [78 FR 22794, Apr. 17, 2013] reniformis nematode)—Pr3 in or on all food commodities when applied as a § 180.1321 Complex Polymeric nematicide and used in accordance Polyhydroxy Acids; exemption from the requirement of a tolerance. with label directions and good agricultural practices. An exemption from the requirement of a tolerance is established for the res- [77 FR 40276, July 9, 2012] idues of complex polymeric § 180.1317 Pesticide chemicals; exemp- polyhydroxy acids in or on all food tion from the requirements of a tol- commodities when applied as a plant erance. growth regulator and used in accordance with good agricultural practices. An exemption from the requirement of a tolerance is established for resi- [78 FR 46267, July 31, 2013]

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§ 180.1322 Bacillus pumilus strain BU § 180.1326 Pseudomonas fluorescens F–33; exemption from the require- strain D7; exemption from the re- ment of a tolerance. quirement of a tolerance. An exemption from the requirement An exemption from the requirement of a tolerance is established for resi- of a tolerance is established for residues of Bacillus pumilus strain BU F–33 dues of Pseudomonas fluorescens strain in or on all food commodities when ap- D7 in or on all food commodities when plied to elicit induced systemic resist- used in accordance with label direc- ance in plants and used in accordance tions and good agricultural practices. with label directions and good agricul- [79 FR 60750, Oct. 8, 2014] tural practices. [78 FR 35149, June 12, 2013] § 180.1327 Tetraacetylethylenediamine (TAED) and its metabolite § 180.1323 Ethyl-2E,4Z-decadienoate Diacetylethylenediamine (DAED); (Pear Ester); exemption from the exemption from the requirement of requirement of a tolerance. a tolerance. An exemption from the requirement An exemption from the requirement of a tolerance is established for resi- of a tolerance is established for residues of the pesticide, dues of the biochemical pesticide, tetraacetylethylenediamine (TAED), ethyl-2E,4Z-decadienoate (pear ester), and its metabolite in or on all food commodities, when diacetylethylenediamine (DAED), in or used in accordance with label direc- on rice and strawberries, when used as tions and good agricultural practices. a fungicide and bactericide in accord- [78 FR 53054, Aug. 28, 2013] ance with label directions and good agricultural practices. § 180.1324 GS-omega/kappa-Hxtx-Hv1a; exemption from the requirement of [79 FR 59121, Oct. 1, 2014] a tolerance. § 180.1328 Beauveria bassiana strain An exemption from the requirement ANT–03; exemption from the re- of a tolerance is established for resi- quirement of a tolerance. dues of the pesticide GS-omega/kappa- An exemption from the requirement Hxtx-Hv1a in or on all food commod- of a tolerance is established for resi- ities when applied or used in accord- dues of Beauveria bassiana strain ANT– ance with label directions and good ag- 03 in or on all food commodities, when ricultural practices. applied as a microbial insecticide and [79 FR 10685, Feb. 26, 2014] used in accordance with label directions and good agricultural practices. § 180.1325 Heat-killed Burkholderia [79 FR 77396, Dec. 24, 2014] spp. strain A396 cells and spent fermentation media exemption from the requirement of a tolerance. § 180.1329 Bacillus subtilis strain IAB/ BS03, exemption from the require- An exemption from the requirement ment of a tolerance. of a tolerance is established for resi- An exemption from the requirement dues of heat-killed Burkholderia spp. of a tolerance is established for resi- strain A396 cells and spent fermenta- dues of Bacillus subtilis strain IAB/BS03 tion media in or on all food commod- in or on all food commodities when ities when applied as a biological insec- used in accordance with label direc- ticide to agricultural crops and used in tions and good agricultural practices. accordance with label directions and good agricultural practices. [80 FR 9217, Feb. 20, 2015] [79 FR 15704, Mar. 21, 2014] § 180.1330

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An exemption from the requirement dues of Choline Chloride in or on all of a tolerance is established for resi- food commodities when Choline Chlo- dues of 1-octanol in or on root and ride is applied pre-harvest and used in tuber vegetables when applied as a accordance with label directions and plant growth regulator in accordance good agricultural practices. with label directions and good agricultural practices. [80 FR 78149, Dec. 16, 2015] [80 FR 25953, May 6, 2015] § 180.1336 Bacillus amyloliquefaciens strain PTA–4838; exemption from § 180.1331 Trichoderma asperelloides the requirement of a tolerance. strain JM41R; exemption from the requirement of a tolerance. An exemption from the requirement of a tolerance is established for resi- An exemption from the requirement dues of Bacillus amyloliquefaciens strain of a tolerance is established for resi- PTA–4838 in or on all food commod- dues of Trichoderma asperelloides strain ities. JM41R in or on all food commodities when used in accordance with label di- [81 FR 41222, June 24, 2016] rections and good agricultural practices. Subpart E—Pesticide Chemicals [80 FR 28203, May 18, 2015] Not Requiring a Tolerance or an Exemption From a Toler- § 180.1332 Lavandulyl senecioate; ex- ance emption from the requirement of a tolerance. SOURCE: 66 FR 66772, Dec. 27, 2001, unless An exemption from the requirement otherwise noted. of a tolerance is established for residues of the arthropod pheromone, § 180.2000 Scope. lavandulyl senecioate (5-methyl-2-(1- methylethenyl)-4-hexenyl 3-methyl-2- This subpart sets forth the pesticide butonate), in or on all raw agricultural chemicals for use in agricultural or commodities when applied or used in other food-related settings for which microbeads/dispensers at a rate not to neither a tolerance nor an exemption is exceed 150 grams active ingredient/ deemed to be needed by EPA. acre/year in accordance with good agricultural practices. § 180.2003 Definitions. (a) Food uses are the uses of a pes- [80 FR 49171, Aug. 17, 2015] ticide chemical that are likely to yield § 180.1333 Potassium Salts of Hops residues in food or feed crops, meat, Beta acids; exemption from the re- milk, poultry or egg. quirement of a tolerance. (b) Non-food uses are those uses that An exemption from the requirement are not likely to yield residues in food of a tolerance is established for resi- or feed crops, meat, milk, poultry or dues of the biochemical potassium egg. salts of hops beta acids in or on honey [66 FR 66772, Dec. 27, 2001, as amended at 73 and honeycomb, when used for the con- FR 60158, Oct. 10, 2008] trol of Varroa mites in accordance with label directions and good agricultural § 180.2010 Threshold of regulation de- practices. terminations. [80 FR 63683, Oct. 21, 2015] The following pesticide chemical uses on food or feed, or food or feed crops, § 180.1334 Choline Chloride; Exemp- do not need a tolerance or exemption tion from the Requirement of a Tol- from the requirement of a tolerance, erance. and may be registered under the Fed- An exemption from the requirement eral Insecticide, Fungicide, and of a tolerance is established for resi- Rodenticide Act, 7 U.S.C. 136 et seq.,

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without obtaining such tolerance or ex- tion that the uses are below the thresh- emption, based on EPA’s determina- old of regulation.

Pesticide Chemical CAS Reg. No. Use/Limits Analytical Method

Thiabendazole 148–79–8 As a seed treatment for dry pea (including field pea, pigeon High Perform- pea, chickpea or lentil), using a maximum application rate of ance Liquid 0.075 pounds of active ingredient per 100 pounds of seed. Chroma- Vines or hay grown from treated seed may not be fed to live- tography/Flo- stock.. rescence De- tector method 1; Modification of Ion-Pairing Liq- uid Chromatograp- hic Determina- tion of Benz- imidazole Fun- gicides in Foods, Gilvydis and Walters, JAOAC, vol. 73, no. 5, 1990. 1Available from: Chief, Analytical Chemistry Branch, Environmental Science Center, 701 Mapes Rd., Ft. Meade, MD 20755– 5350; telephone number: (410) 305–2905; e-mail address: [email protected]

[73 FR 1978, Jan. 11, 2008]

§ 180.2020 Non-food determinations. from the requirement of a tolerance based on EPA’s determination that The following pesticide chemical uses they are not likely to result in residues do not need a tolerance or exemption in or on food.

Pesticide Chemical CAS Reg. No. Limits Uses

Methyl bromide 74–83–9 When applied as a pre-plant soil fumigant All pre-plant soil uses Potassium 12298–68–9 When applied to growing crops in foreign countries Bananas, grapes, triiodide (KI3) and melons Rhodamine B 81–88–9 Not to exceed 2% by weight of the formulated product and 60 ppm on Dye for seed treat- the treated seed ment

[66 FR 66772, Dec. 27, 2001, as amended at 70 FR 40201, July 13, 2005; 71 FR 45402, Aug. 9, 2006]

PARTS 181–189 [RESERVED]

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