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Home , Benfluralin, Clomazone, Cyantraniliprole, Ethephon, Flazasulfuron, Fluroxypyr

Pt. 180 40 CFR Ch. I (7–1–15 Edition)

at any time before the filing of the ini- 180.124 Methyl bromide; tolerances for resi- tial decision. dues. 180.127 Piperonyl butoxide; tolerances for [55 FR 50293, Dec. 5, 1990, as amended at 70 residues. FR 33360, June 8, 2005] 180.128 ; tolerances for residues. 180.129 o-Phenylphenol and its sodium salt; PART 180—TOLERANCES AND EX- tolerances for residues. 180.130 Hydrogen Cyanide; tolerances for EMPTIONS FOR CHEM- residues. ICAL RESIDUES IN FOOD 180.132 Thiram; tolerances for residues. 180.142 2,4-D; tolerances for residues. Subpart A—Definitions and Interpretative 180.145 Fluorine compounds; tolerances for Regulations residues. 180.151 oxide; tolerances for resi- Sec. dues. 180.1 Definitions and interpretations. 180.153 ; tolerances for residues. 180.3 Tolerances for related pesticide chemi- 180.154 Azinphos-methyl; tolerances for resi- cals. dues. 180.4 Exceptions. 180.155 1-Naphthaleneacetic acid; tolerances 180.5 Zero tolerances. for residues. 180.6 Pesticide tolerances regarding milk, 180.163 ; tolerances for residues. eggs, meat, and/or poultry; statement of 180.169 ; tolerances for residues. policy. 180.172 Dodine; tolerances for residues. 180.175 Maleic hydrazide; tolerances for resi- Subpart B—Procedural Regulations dues. 180.176 Mancozeb; tolerances for residues. 180.7 Petitions proposing tolerances or ex- 180.178 Ethoxyquin; tolerances for residues. emptions for pesticide residues in or on 180.181 Chlorpropham; tolerances for resi- raw agricultural commodities or proc- dues. essed foods. 180.182 ; tolerances for residues. 180.8 Withdrawal of petitions without preju- 180.183 ; tolerances for residues. dice. 180.184 ; tolerances for residues. 180.9 Substantive amendments to petitions. 180.185 DCPA; tolerances for residues. 180.29 Establishment, modification, and rev- 180.189 ; tolerances for residues. ocation of tolerance on initiative of Ad- 180.190 Diphenylamine; tolerances for resi- ministrator. dues. 180.30 Judicial review. 180.191 Folpet; tolerances for residues. 180.31 Temporary tolerances. 180.198 Trichlorfon; tolerances for residues. 180.32 Procedure for modifying and revoking 180.200 Dicloran; tolerances for residues. tolerances or exemptions from toler- 180.202 p-Chlorophenoxyacetic acid; toler- ances. ances for residues. 180.33 Fees. 180.204 ; tolerances for residues. 180.34 Tests on the amount of residue re- 180.205 ; tolerances for residues. maining. 180.35 Tests for potentiation. 180.206 ; tolerances for residues. 180.40 Tolerances for crop groups. 180.207 ; tolerances for residues. 180.41 Crop group tables. 180.208 ; tolerances for residues. 180.209 Terbacil; tolerances for residues. Subpart C—Specific Tolerances 180.210 Bromacil; tolerances for residues. 180.211 ; tolerances for residues. 180.101 Specific tolerances; general provi- 180.212 S-Ethyl cyclohexylethylthiocarba- sions. mate; tolerances for residues. 180.103 Captan; tolerances for residues. 180.213 ; tolerances for residues. 180.106 Diuron; tolerances for residues. 180.215 ; tolerances for residues. 180.108 ; tolerances for residues. 180.217 Metiram; tolerances for residues. 180.111 ; tolerances for residues. 180.220 ; tolerances for residues. 180.114 Ferbam; tolerances for residues. 180.222 Prometryn; tolerances for residues. 180.116 Ziram; tolerances for residues. 180.225 Phosphine; tolerances for residues. 180.117 S-Ethyl dipropylthiocarbamate; tol- 180.226 ; tolerances for residues. erances for residues. 180.227 ; tolerances for residues. 180.121 Methyl ; tolerances for res- 180.229 Fluometuron; tolerances for resi- idues. dues. 180.123 Inorganic bromide residues resulting 180.231 Dichlobenil; tolerances for residues. from fumigation with methyl bromide; 180.232 Butylate; tolerances for residues. tolerances for residues. 180.235 ; tolerances for residues. 180.123a Inorganic bromide residues in pea- 180.236 Triphenyltin hydroxide; tolerances nut hay and peanut hulls; statement of for residues. policy. 180.241 ; tolerances for residues.

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180.242 Thiabendazole; tolerances for resi- 180.339 MCPA; tolerances for residues. dues. 180.341 2,4-Dinitro-6-octylphenyl crotonate 180.243 Propazine; tolerances for residues. and 2,6-dinitro-4-octylphenyl crotonate; 180.245 Streptomycin; tolerances for resi- tolerances for residues. dues. 180.342 ; tolerances for residues. 180.249 ; tolerances for residues. 180.345 Ethofumesate; tolerances for resi- 180.252 ; tolerances for dues. residues. 180.349 ; tolerances for residues. 180.253 ; tolerances for residues. 180.350 Nitrapyrin; tolerances for residues. 180.254 ; tolerances for residues. 180.352 ; tolerances for residues. 180.257 Chloroneb; tolerances for residues. 180.353 Desmedipham; tolerances for resi- 180.258 Ametryn; tolerances for residues. dues. 180.259 Propargite; tolerances for residues. 180.355 ; tolerances for residues. 180.261 ; tolerances for residues. 180.356 Norflurazon; tolerances for residues. 180.262 Ethoprop; tolerances for residues. 180.360 ; tolerance for residues. 180.263 ; tolerances for residues. 180.361 ; tolerances for resi- 180.269 ; tolerances for residues. dues. 180.272 Tribuphos; tolerances for residues. 180.362 Fenbutatin-oxide; tolerances for res- 180.274 ; tolerances for residues. idues. 180.275 Chlorothalonil; tolerances for resi- 180.364 ; tolerances for residues. dues. 180.367 n-Octyl bicycloheptenedicarbox- 180.276 hydrochloride; toler- imide; tolerances for residues. ances for residues. 180.368 ; tolerances for residues. 180.278 Phenmedipham; tolerances for resi- 180.370 5-Ethoxy-3-(trichloromethyl)-1, 2, 4- dues. thiadiazole; tolerances for residues. 180.284 Zinc phosphide; tolerances for resi- 180.371 Thiophanate-methyl; tolerances for dues. residues. 180.287 ; tolerances for residues. 180.372 2,6-Dimethyl-4-tridecylmorpholine; 180.288 2-(Thiocyanomethylthio) tolerances for residues. benzothiazole; tolerances for residues. 180.373 [Reserved] 180.289 Methanearsonic acid; tolerances for 180.377 ; tolerances for resi- residues. dues. 180.291 Pentachloronitrobenzene; tolerance 180.378 ; tolerances for residues. for residues. 180.380 Vinclozolin; tolerances for residues. 180.292 ; tolerances for residues. 180.381 Oxyfluorfen; tolerances for residues. 180.293 ; tolerances for residues. 180.383 Sodium salt of ; toler- 180.297 N-1-Naphthyl phthalamic acid; toler- ances for residues. ances for residues. 180.384 Mepiquat (N,N-dimethylpiperidin- 180.298 ; tolerances for resi- ium); tolerances for residues. dues. 180.385 Diclofop-methyl; tolerances for resi- 180.299 ; tolerances for residues. dues. 180.300 ; tolerances for residues. 180.388–180.389 [Reserved] 180.301 Carboxin; tolerances for residues. 180.390 ; tolerances for residues. 180.303 ; tolerances for residues. 180.395 ; tolerances for resi- 180.304 Oryzalin; tolerances for residues. dues. 180.311 ; tolerances for resi- 180.396 ; tolerances for residues. dues. 180.399 Iprodione; tolerances for residues. 180.314 Triallate; tolerances for residues. 180.401 Thiobencarb; tolerances for residues. 180.315 ; tolerances for resi- 180.403 Thidiazuron; tolerances for residues. dues. 180.404 ; tolerances for residues. 180.316 Pyrazon; tolerances for residues. 180.405 Chlorsulfuron; tolerances for resi- 180.317 Propyzamide; tolerances for resi- dues. dues. 180.407 Thiodicarb; tolerances for residues. 180.318 4-(2-Methyl-4-chlorophenoxy) bu- 180.408 Metalaxyl; tolerances for residues. tyric acid; tolerance for residues. 180.409 Pirimiphos-methyl; tolerances for 180.319 Interim tolerances. residues. 180.324 ; tolerances for residues. 180.410 Triadimefon; tolerances for residues. 180.328 Napropamide; tolerances for resi- 180.411 -P-butyl; tolerances for res- dues. idues. 180.330 S-(2-(Ethylsulfinyl)ethyl) O,O-di- 180.412 ; tolerances for residues. methyl phosphorothioate; tolerances for 180.413 Imazalil; tolerances for residues. residues. 180.414 ; tolerances for residues. 180.331 4-(2,4-Dichlorophenoxy) butyric acid; 180.415 Aluminum tris (O-ethylphospho- tolerances for residues. nate); tolerances for residues. 180.332 ; tolerances for residues. 180.416 Ethalfluralin; tolerances for resi- 180.337 Oxytetracycline; tolerances for resi- dues. dues. 180.417 ; tolerances for residues.

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180.418 and isomers alpha- 180.457 Bitertanol; tolerances for residues. cypermethrin and zeta-cypermethrin; 180.458 Clethodim; tolerances for residues. tolerances for residues. 180.459 Triasulfuron; tolerances for residues. 180.419 Chlorpyrifos-methyl; tolerances for 180.460 Benoxacor; tolerances for residues. residues. 180.461 Cadusafos; tolerances for residues. 180.420 Fluridone; tolerances for residues. 180.462 Pyridate; tolerances for residues. 180.421 Fenarimol; tolerances for residues. 180.463 ; tolerances for residues. 180.422 ; tolerances for resi- 180.464 ; tolerances for resi- dues. dues. 180.425 ; tolerances for residues. 180.465 4-(Dichloroacetyl)-1-oxa-4- 180.426 2-[4,5-Dihydro-4-methyl-4-(1- azaspiro[4.5]decane. methylethyl)-5-oxo-1H-imidazol-2-yl]-3- 180.466 ; tolerances for resi- quinoline carboxylic acid; tolerance for dues. residues. 180.467 Carbon disulfide; tolerances for resi- 180.427 Tau-Fluvalinate; tolerances for resi- dues. dues. 180.468 Flumetsulam; tolerances for resi- 180.428 Metsulfuron methyl; tolerances for dues. residues. 180.469 Dichlormid; tolerances for residues. 180.429 Chlorimuron ethyl; tolerances for 180.470 ; tolerances for residues. residues. 180.471 Furilazole; tolerances for residues. 180.430 Fenoxaprop-ethyl; tolerances for res- 180.472 ; tolerances for resi- idues. dues. 180.431 ; tolerances for residues. 180.473 ; tolerances 180.432 ; tolerances for residues. for residues. 180.433 ; tolerances for residues. 180.474 Tebuconazole; tolerances for resi- 180.434 Propiconazole; tolerances for resi- dues. dues. 180.475 Difenoconazole; tolerances for resi- 180.435 ; tolerances for resi- dues. dues. 180.476 Triflumizole; tolerances for residues. 180.436 and the isomer beta- 180.477 Flumiclorac pentyl; tolerances for cyfluthrin; tolerances for residues. residues. 180.437 Methyl 2-(4-isopropyl-4-methyl-5- 180.478 Rimsulfuron; tolerances for residues. oxo-2-imidazolin-2-yl)-p-toluate and 180.479 Halosulfuron-methyl; tolerances for methyl 6-(4-isopropyl-4-methyl-5-oxo-2- residues. imidazolin-2-yl)-m-toluate; tolerances for 180.480 Fenbuconazole; tolerances for resi- residues. dues. 180.438 Lambda- and an isomer 180.481 Prosulfuron; tolerances for residues. gamma-cyhalothrin; tolerances for resi- 180.482 ; tolerances for resi- dues. dues. 180.439 Thifensulfuron methyl; tolerances 180.484 Flutolanil; tolerances for residues. for residues. 180.485 Cyproconazole; tolerances for resi- 180.440 ; tolerances for residues. dues. 180.441 Quizalofop ethyl; tolerances for resi- 180.486 ; tolerances for resi- dues. dues. 180.442 ; tolerances for residues. 180.487 Pyrithiobac sodium; tolerances for 180.443 Myclobutanil; tolerances for resi- residues. dues. 180.490 ; tolerances for residues. 180.444 Sulfur dioxide; tolerances for resi- 180.491 Propylene oxide; tolerances for resi- dues. dues. 180.445 Bensulfuron methyl; tolerances for 180.492 Triflusulfuron-methyl; tolerances residues. for residues. 180.446 Clofentezine; tolerances for residues. 180.493 Dimethomorph; tolerances for resi- 180.447 Imazethapyr; tolerances for residues. dues. 180.448 Hexythiazox; tolerance for residues. 180.494 Pyridaben; tolerance for residues. 180.449 Avermectin B1 and its delta-8,9-iso- 180.495 ; tolerances for residues. mer; tolerances for residues. 180.496 Thiazopyr; tolerances for residues. 180.450 Beta-(4-Chlorophenoxy)-alpha-(1,1- 180.497 Clofencet; tolerances for residues. dimethylethyl)-1H-1,2,4-triazole-1-eth- 180.498 ; tolerances for resi- anol; tolerances for residues. dues. 180.451 Tribenuron methyl; tolerances for 180.499 Propamocarb; tolerances for resi- residues. dues. 180.452 Primisulfuron-methyl; tolerances for 180.500 ; tolerances for residues. residues. 180.501 ; tolerances for residues. 180.454 Nicosulfuron; tolerances for resi- 180.502 Aminoethoxyvinylglycine hydro- dues. chloride (aviglycine HCl); tolerances for 180.455 Procymidone; tolerances for resi- residues. dues. 180.503 Cymoxanil, tolerance for residues.

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180.504 [Reserved] 180.552 Sulfosulfuron; tolerances for resi- 180.505 Emamectin; tolerances for residues. dues. 180.506 Cyclanilide; tolerances for residues. 180.553 Fenhexamid; tolerances for residues. 180.507 Azoxystrobin; tolerances for resi- 180.554 Kresoxim-methyl; tolerances for res- dues. idues. 180.509 Mefenpyr-diethyl; tolerance for resi- 180.555 Trifloxystrobin; tolerances for resi- dues. dues. 180.510 ; tolerances for resi- 180.556 Pymetrozine; tolerances for resi- dues. dues. 180.511 ; tolerances for residues. 180.557 Tetraconazole; tolerances for resi- 180.512 [Reserved] dues. 180.513 ; tolerances for resi- 180.559 Clodinafop-propargyl; tolerances for dues. residues. 180.514 Cloransulam-methyl; tolerances for 180.560 Cloquintocet-mexyl; tolerances for residues. residues. 180.515 Carfentrazone-ethyl; tolerances for 180.561 Acibenzolar-S-methyl; tolerances for residues. residues. 180.516 Fludioxonil; tolerances for residues. 180.562 Flucarbazone-sodium; tolerances for 180.517 ; tolerances for residues. residues. 180.518 Pyrimethanil; tolerances for resi- 180.563 Ethametsulfuron-methyl; tolerances dues. for residues. 180.519 Bromide ion and residual bromine; 180.564 ; tolerances for residues. tolerances for residues. 180.565 ; tolerances for resi- 180.521 Fumigants for grain-mill machinery; dues. tolerances for residues. 180.566 Fenpyroximate; tolerances for resi- 180.522 Fumigants for processed grains used dues. in production of fermented malt bev- 180.567 Zoxamide; tolerances for residues. erage; tolerances for residues. 180.568 Flumioxazin; tolerances for residues. 180.523 Metaldehyde; tolerances for resi- 180.569 Forchlorfenuron; tolerances for resi- dues. dues. 180.525 ; tolerances for residues. 180.570 Isoxadifen-ethyl; tolerances for resi- 180.526 Synthetic isoparaffinic petroleum dues. hydrocarbons; tolerances for residues. 180.571 ; tolerances for residues. 180.527 Flufenacet, N-(4-fluorophenyl)-N-(1- 180.572 Bifenazate; tolerance for residues. methylethyl)-2-[[5-(trifluoromethyl)-1, 3, 180.573 Tepraloxydim; tolerances for resi- 4-thiadiazol-2-yl] oxy]acetamide and its dues. metabolites containing the 4-fluoro-N- 180.574 Fluazinam; tolerances for residues. methylethyl benzenamine tolerances for 180.575 Sulfuryl fluoride; tolerances for resi- residues. dues. 180.530 2,2-Dimethyl-1,3-benzodioxol-4-ol 180.576 Cyhalofop-butyl; tolerances for resi- methylcarbamate; tolerances for resi- dues. dues. 180.577 Bispyribac-sodium; tolerances for 180.532 Cyprodinil; tolerances for residues. residues. 180.533 ; tolerances for resi- 180.578 ; tolerances for residues. dues. 180.579 Fenamidone; tolerances for residues. 180.535 1-methylheptyl ester; 180.580 Iodosulfuron-Methyl-Sodium; toler- tolerances for residues. ances for residues. 180.537 Isoxaflutole; tolerances for residues. 180.581 Iprovalicarb; tolerances for residues. 180.539 d-; tolerances for residues. 180.582 Pyraclostrobin; tolerances for resi- 180.540 ; tolerances for resi- dues. dues. 180.583 Triticonazole; tolerances for resi- 180.541 Propetamphos; tolerances for resi- dues. dues. 180.584 Tolylfluanid; tolerances for residues. 180.543 Diclosulam; tolerances for residues. 180.585 Pyraflufen-ethyl; tolerances for resi- 180.544 Methoxyfenozide; tolerances for resi- dues. dues. 180.586 ; tolerances for residues. 180.545 ; tolerances for residues. 180.587 Famoxadone; tolerance for residues. 180.546 Mefenoxam; tolerances for residues. 180.588 Quinoxyfen; tolerances for residues. 180.547 Prohexadione calcium; tolerances 180.589 Boscalid; tolerances for residues. for residues. 180.590 2, 6-Diisopropylnaphthalene (2, 6- 180.548 Tralkoxydim; tolerances for resi- DIPN); tolerances for residues. dues. 180.591 Trifloxysulfuron; tolerances for resi- 180.549 Diflufenzopyr; tolerances for resi- dues. dues. 180.592 ; tolerances for residues. 180.551 Fluthiacet-methyl; tolerances for 180.593 Etoxazole; tolerances for residues. residues. 180.594 ; tolerances for residues.

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180.595 Flufenpyr-ethyl; tolerances for resi- 180.640 Pyridalyl; tolerances for residues. dues. 180.641 Spirotetramat; tolerances for resi- 180.596 Fosthiazate; tolerances for residues. dues. 180.597 Mesosulfuron-methyl; tolerances for 180.642 Gentamicin; tolerances for residues. residues. 180.643 Uniconazole; tolerances for residues. 180.598 Novaluron; tolerances for residues. 180.644 Cyprosulfamide; tolerances for resi- 180.599 Acequinocyl; tolerances for residues. dues. 180.600 Propoxycarbazone; tolerances for 180.645 Thiencarbazone-methyl; tolerances residues for residues. 180.601 Cyazofamid; tolerances for residues. 180.646 Ipconazole; tolerances for residues. 180.602 Spiroxamine; tolerances for residues. 180.647 d-; tolerances for resi- 180.603 ; tolerances for residues. dues. 180.604 Mepanipyrim; tolerances for resi- 180.648 Meptyldinocap; tolerances for resi- dues. dues. 180.605 Penoxsulam; tolerances for residues. 180.649 ; tolerances for residues. 180.607 Spiromesifen; tolerances for resi- 180.650 Isoxaben; tolerances for residues. dues. 180.651 Imazosulfuron; tolerances for resi- 180.608 Spirodiclofen; tolerances for resi- dues. dues. 180.652 Ethiprole; tolerances for residues. 180.609 Fluoxastrobin; tolerances for resi- 180.653 ; tolerances for residues. dues. 180.654 Isopyrazam; tolerances for residues. 180.610 ; tolerances for resi- 180.655 ; tolerances for resi- dues. 180.611 Pinoxaden; tolerances for residues. dues. 180.612 Topramezone; tolerances for resi- 180.656 Amisulbrom; tolerances for residues. dues. 180.657 ; tolerances for resi- 180.613 Flonicamid; tolerances for residues. dues. 180.614 Kasugamycin; tolerances for resi- 180.658 Penthiopyrad; tolerances for resi- dues. dues. 180.615 Amicarbazone; tolerances for resi- 180.659 Pyroxasulfone; tolerances for resi- dues. dues. 180.616 Fenpropimorph; tolerances for resi- 180.660 Pyriofenone; tolerances for residues. dues. 180.661 Fluopyram; tolerances for residues. 180.617 Metconazole; tolerances for residues. 180.662 Trinexapac-ethyl; tolerances for res- 180.618 Benthiavalicarb-isopropyl; tolerance idues. for residues. 180.663 Ametoctradin; tolerances for resi- 180.619 Epoxiconazole; tolerances for resi- dues. dues. 180.664 Penflufen; tolerances for residues. 180.620 ; tolerances for residues. 180.665 Sedaxane; tolerances for residues. 180.621 Dithianon; tolerances for residues. 180.666 Fluxapyroxad; tolerances for resi- 180.622 Ethaboxam; tolerances for residues. dues. 180.623 ; tolerances for resi- 180.667 Cyflufenamid, tolerance for residues. dues. 180.668 ; tolerances for residues. 180.624 Metrafenone; tolerances for residues. 180.669 Picoxystrobin; tolerances for resi- 180.625 Orthosulfamuron; tolerances for res- dues. idues. 180.671 Fenpyrazamine; tolerances for resi- 180.626 Prothioconazole; tolerances for resi- dues. dues. 180.672 Cyantraniliprole; tolerances for resi- 180.627 Fluopicolide; tolerances for residues. dues. 180.628 ; tolerances for 180.673 Triforine; tolerances for residues. residues. 180.674 Proquinazid; tolerances for residues. 180.629 Flutriafol; tolerances for residues. 180.675 Tolfenpyrad; tolerances for residues. 180.630 Flusilazole; tolerances for residues. 180.676 Fenpropidin; tolerances for residues. 180.631 Pyrasulfotole; tolerances for resi- 180.677 Cyflumetofen; tolerances for resi- dues. dues. 180.632 Fenazaquin; Tolerances for residues. 180.678 Tricyclazole; tolerances for residues. 180.633 Florasulam; tolerances for residues. 180.679 Flupyradifurone; tolerances for resi- 180.634 Tembotrione; tolerances for resi- dues. dues. 180.680 Fluensulfone; tolerances for resi- 180.635 Spinetoram; tolerances for residues. dues. 180.636 1,3-dichloropropene; tolerances for 180.682 Bicyclopyrone; tolerances for resi- residues. dues. 180.637 Mandipropamid; tolerances for resi- dues. Subpart D—Exemptions From Tolerances 180.638 Pyroxsulam; tolerances for residues. 180.639 ; tolerances for resi- 180.900 Exemptions from the requirement of dues. a tolerance.

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180.905 Pesticide chemicals; exemptions 180.1064 Tomato pinworm insect pheromone; from the requirement of a tolerance. exemption from the requirement of a tol- 180.910 Inert ingredients used pre- and post- erance. harvest; exemptions from the require- 180.1065 2-Amino-4,5-dihydro-6-methyl-4- ment of a tolerance. propyl-s-triazolo(1,5-alpha)pyrimidin-5- 180.920 Inert ingredients used pre-harvest; one; exemption from the requirement of exemptions from the requirement of a a tolerance. tolerance. 180.1067 Methyl eugenol and malathion com- 180.930 Inert ingredients applied to animals; bination; exemption from the require- exemptions from the requirement of a ment of a tolerance. tolerance. 180.1068 C12-C18 fatty acid potassium salts; 180.940 Tolerance exemptions for active and exemption from the requirement of a tol- inert ingredients for use in antimicrobial erance. formulations (Food-contact surface sani- 180.1069 (Z)-11-Hexadecenal; exemption from tizing solutions). the requirement of a tolerance. 180.950 Tolerance exemptions for minimal 180.1070 Sodium chlorite; exemption from risk active and inert ingredients. the requirement of a tolerance. 180.960 Polymers; exemptions from the re- 180.1071 Peanuts, Tree Nuts, Milk, Soy- quirement of a tolerance. beans, Eggs, Fish, Crustacea, and Wheat; 180.1011 Viable spores of the microorganism exemption from the requirement of a tol- Bacillus thuringiensis Berliner; exemption erance. from the requirement of a tolerance. 180.1072 Poly-D-glucosamine (chitosan); ex- 180.1016 Ethylene; exemption from the re- emption from the requirement of a toler- quirement of a tolerance. ance. 180.1017 Diatomaceous earth; exemption 180.1073 Isomate-M; exemption from the re- from the requirement of a tolerance. quirement of a tolerance. 180.1019 Sulfuric acid; exemption from the 180.1074 F.D.&C. Blue No. 1; exemption from requirement of a tolerance. the requirement of a tolerance. 180.1020 Sodium chlorate; exemption from 180.1075 Colletotrichum gloeosporioides f. sp. the requirement of a tolerance. aeschynomene; exemption from the re- 180.1021 Copper; exemption from the re- quirement of a tolerance. quirement of a tolerance. 180.1076 Viable spores of the microorganism 180.1022 Iodine-detergent complex; exemp- Bacillus popilliae; exemption from the re- tion from the requirement of a tolerance. quirement of a tolerance. 180.1023 Propanoic acid; exemptions from 180.1080 volatiles and pheromone; ex- the requirement of a tolerance. emptions from the requirement of a tol- 180.1025 Xylene; exemption from the re- erance. quirement of a tolerance. 180.1083 Dimethyl sulfoxide; exemption 180.1027 Nuclear polyhedrosis virus of from the requirement of a tolerance. Heliothis zea; exemption from the re- 180.1084 Monocarbamide dihydrogen sulfate; quirement of a tolerance. exemption from the requirement of a tol- 180.1033 ; exemption from the re- erance. quirement of a tolerance. 180.1086 3,7,11-Trimethyl-1,6,10-dodecatriene- 180.1037 Polybutenes; exemption from the 1-ol and 3,7,11-trimethyl-2,6,10- requirement of a tolerance. dodecatriene-3-ol; exemption from the re- 180.1040 Ethylene glycol; exemption from quirement of a tolerance. the requirement of a tolerance. 180.1087 Sesame stalks; exemption from the 180.1041 Nosema locustae; exemption from requirement of a tolerance. the requirement of a tolerance. 180.1089 Poly-N-acetyl-D-glucosamine; ex- 180.1043 Gossyplure; exemption from the re- emption from the requirement of a toler- quirement of a tolerance. ance. 180.1049 Carbon dioxide; exemption from the 180.1090 Lactic acid; exemption from the re- requirement of a tolerance. quirement of a tolerance. 180.1050 Nitrogen; exemption from the re- 180.1091 Aluminum isopropoxide and alu- quirements of a tolerance. minum secondary butoxide; exemption 180.1052 2,2,5-trimethyl-3-dichloroacetyl-1,3- from the requirement of a tolerance. oxazolidine; exemption from the require- 180.1092 Menthol; exemption from the re- ment of a tolerance. quirement of a tolerance. 180.1054 Calcium hypochlorite; exemptions 180.1095 Chlorine gas; exemptions from the from the requirement of a tolerance. requirement of a tolerance. 180.1056 Boiled linseed oil; exemption from 180.1097 GBM-ROPE; exemption from the re- requirement of tolerance. quirement of a tolerance. 180.1057 Phytophthora palmivora; exemp- 180.1098 Gibberellins [Gibberellic Acids (GA3 tion from requirement of tolerance. and GA4 + GA7), and Sodium or Potas- 180.1058 Sodium diacetate; exemption from sium Gibberellate]; exemption from the the requirement of a tolerance. requirement of a tolerance.

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180.1100 Gliocladium virens isolate GL-21; ex- 180.1131 Ampelomyces quisqualis isolate M10; emption from the requirement of a toler- exemption from the requirement of a tol- ance. erance. 180.1101 Parasitic (parasitoid) and predatory 180.1135 Pasteuria penetrans; exemption from insects; exemption from the requirement the requirement of a tolerance. of a tolerance. 180.1139 Sodium 5-nitroguaiacolate; exemp- 180.1102 Trichoderma harzianum KRL-AG2 tion from the requirement of a tolerance. (ATCC #20847) strain T–22; exemption 180.1140 Sodium o-nitrophenolate; exemp- from requirement of a tolerance. tion from the requirement of a tolerance. 180.1103 Isomate-C; exemption from the re- 180.1141 Sodium p-nitrophenolate; exemp- quirement of a tolerance. tion from the requirement of a tolerance. 180.1107 Delta endotoxin of Bacillus 180.1142 1,4-Dimethylnaphthalene; exemp- thuringiensis variety kurstaki encap- tion from the requirement of a tolerance. sulated into killed Pseudomonas 180.1143 Methyl anthranilate; exemption fluorescens; exemption from the require- from the requirement of a tolerance. ment of a tolerance. 180.1144 Candida oleophila isolate I-182; ex- 180.1108 Delta endotoxin of Bacillus emption from the requirement of a toler- thuringiensis variety San Diego encap- ance. sulated into killed Pseudomonas 180.1145 Pseudomonas syringae; exemption fluorescens; exemption from the require- from the requirement of a tolerance. ment of a tolerance. 180.1146 Beauveria bassiana Strain GHA; ex- 180.1110 3-Carbamyl-2,4,5-trichlorobenzoic emption from the requirement of a toler- acid; exemption from the requirement of ance. a tolerance. 180.1148 Occlusion Bodies of the Granulosis 180.1111 Bacillus subtilis GB03; exemption Virus of Cydia pomenella; tolerance ex- from the requirement of a tolerance. emption. 180.1113 Lagenidium giganteum; exemption 180.1149 Inclusion bodies of the multi-nu- from the requirement of a tolerance. clear polyhedrosis virus of Anagrapha falcifera; exemption from the require- 180.1114 Pseudomonas fluorescens A506, ment of a tolerance. Pseudomonas fluorescens 1629RS, and 180.1150 6-Benzyladenine; exemption from Pseudomonas syringae 742RS; exemptions the requirement of a tolerance. from the requirement of a tolerance. 180.1153 Lepidopteran pheromones; exemp- 180.1118 Spodoptera exigua nuclear poly- tion from the requirement of a tolerance. hedrosis virus; exemption from the re- 180.1154 CryIA(c) and CryIC derived delta- quirement of a tolerance. endotoxins of Bacillus thuringiensis var. 180.1119 ; exemption from the kurstaki encapsulated in killed requirement of a tolerance. Pseudomonas fluorescens, and the expres- 180.1120 sp. strain K61; exemp- sion plasmid and cloning vector genetic tion from the requirement of a tolerance. constructs. 180.1121 and its salts, borax (so- 180.1156 Cinnamaldehyde; exemption from dium borate decahydrate), disodium the requirement of a tolerance. octaborate tetrahydrate, boric oxide 180.1157 Cytokinins; exemption from the re- (boric anhydride), sodium borate and so- quirement of a tolerance. dium metaborate; exemptions from the 180.1158 ; exemption from the re- requirement of a tolerance. quirement of a tolerance. 180.1122 Inert ingredients of semiochemical 180.1159 Pelargonic acid; exemption from dispensers; exemptions from the require- the requirement of tolerances. ment of a tolerance. 180.1160 Jojoba oil; exemption from the re- 180.1124 Arthropod pheromones; exemption quirement of a tolerance. from the requirement of a tolerance. 180.1161 Clarified hydrophobic extract of 180.1126 Codlure, (E,E)-8,10-Dodecadien-1-ol; neem oil; exemption from the require- exemption from the requirement of a tol- ment of a tolerance. erance. 180.1162 Acrylate polymers and copolymers; 180.1127 Biochemical pesticide plant floral exemption from the requirement of a tol- volatile attractant compounds: cinna- erance. maldehyde, cinnamyl alcohol, 4-methoxy 180.1163 Killed Myrothecium verrucaria; ex- cinnamaldehyde, 3-phenyl propanol, 4- emption from the requirement of a toler- methoxy phenethyl alcohol, indole, and ance. 1,2,4-trimethoxybenzene; exemptions 180.1165 Capsaicin; exemption from the re- from the requirement of a tolerance. quirement of a tolerance. 180.1128 Bacillus subtilis MBI 600; exemption 180.1167 Allyl isothiocyanate as a compo- from the requirement of a tolerance. nent of food grade oil of mustard; exemp- 180.1130 N-(n-octyl)-2-pyrrolidone and N-(n- tion from the requirement of a tolerance. dodecyl)-2-pyrrolidone; exemptions from 180.1176 Sodium bicarbonate; exemption the requirement of a tolerance. from the requirement of a tolerance.

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180.1177 Potassium bicarbonate; exemption 180.1219 Foramsulfuron; exemption from the from the requirement of a tolerance. requirement of a tolerance. 180.1178 Formic acid; exemption from the 180.1220 1-Methylcyclopropene; exemption requirement of a tolerance. from the requirement of a tolerance. 180.1179 Plant extract derived from Opuntia 180.1221 Pseudozyma flocculosa strain PF-A22 lindheimeri, Quercus falcata, Rhus UL; exemption from the requirement of a aromatica, and Rhizophoria mangle; ex- tolerance. emption from the requirement of a toler- 180.1222 Sucrose octanoate esters; exemp- ance. tion from the requirement of a tolerance. 180.1180 Kaolin; exemption from the require- 180.1223 Imazamox; exemption from the re- ment of a tolerance. quirement of a tolerance. 180.1181 Bacillus cereus strain BPO1; exemp- 180.1224 Bacillus pumilus GB34; exemption tion from the requirement of a tolerance. from the requirement of a tolerance. 180.1187 L-; exemption from 180.1225 Decanoic acid; exemption from the the requirement of a tolerance. requirement of a tolerance. 180.1188 Gamma aminobutyric acid; exemp- 180.1226 Bacillus pumilus strain QST2808; tion from the requirement of a tolerance. temporary exemption from the require- 180.1189 Methyl salicylate; exemption from ment of a tolerance. the requirement of a tolerance. 180.1228 Diallyl sulfides; exemption from the 180.1191 Ferric phosphate; exemption from requirement of a tolerance. the requirement of a tolerance. 180.1230 Ferrous sulfate; exemption from 180.1193 Potassium dihydrogen phosphate; the requirement of a tolerance. exemption from the requirement of a tol- 180.1231 Lime; exemption from the require- erance. ment of a tolerance. 180.1195 Titanium dioxide. 180.1232 Lime-sulfur; exemption from the re- 180.1196 Peroxyacetic acid; exemption from quirement of a tolerance. the requirement of a tolerance. 180.1233 Potassium sorbate; exemption from 180.1197 Hydrogen peroxide; exemption from the requirement of a tolerance. the requirement of a tolerance. 180.1234 Sodium carbonate; exemption from 180.1198 Gliocladium catenulatum strain the requirement of a tolerance. J1446; exemption from the requirement of 180.1235 Sodium hypochlorite; exemption a tolerance. from the requirement of a tolerance. 180.1199 Lysophosphatidylethanolamine 180.1236 Sulfur; exemption from the require- (LPE); exemption from the requirement ment of a tolerance. of a tolerance. 180.1237 Sodium metasilicate; exemption 180.1200 Pseudomonas fluorescens strain from the requirement of a tolerance. PRA–25; temporary exemption from the 180.1240 Thymol; exemption from the re- requirement of a tolerance. quirement of a tolerance. 180.1201 Trichoderma harzianum strain T-39; 180.1241 Eucalyptus oil; exemption from the exemption from the requirement of a tol- requirement of a tolerance. erance. 180.1243 Bacillus subtilis var. amylolique- 180.1202 Bacillus sphaericus; exemption from faciens strain FZB24; exemption from the the requirement of a tolerance. requirement of a tolerance. 180.1204 Harpin protein; exemption from the 180.1244 Ammonium bicarbonate; exemption requirement of a tolerance. from the requirement of a tolerance. 180.1205 Beauveria bassiana ATCC #74040; ex- 180.1245 Rhamnolipid biosurfactant; exemp- emption from the requirements of a tol- tion from the requirement of a tolerance. erance. 180.1246 Yeast Extract Hydrolysate from 180.1206 Aspergillus flavus AF36; exemption Saccharomyces cerevisiae: exemption from from the requirement of a tolerance. the requirement of a tolerance. 180.1207 N-acyl sarcosines and sodium N- 180.1248 Exemption of citronellol from the acyl sarcosinates; exemption from the re- requirement of a tolerance. quirement of a tolerance. 180.1250 C8, C10, and C12 fatty acid mono- 180.1209 Bacillus subtilis strain QST 713 and esters of glycerol and propylene glycol; strain QST 713 variant soil; exemption exemption from the requirement of a tol- from the requirement of a tolerance. erance. 180.1210 Phosphorous acid; exemption from 180.1251 Geraniol; exemption from the re- the requirement of a tolerance. quirement of a tolerance. 180.1212 Pseudomonas chlororaphis Strain 63– 180.1253 Streptomyces lydicus WYEC 108; ex- 28; exemption from the requirement of a emption from the requirement of a toler- tolerance. ance. 180.1213 Coniothyrium minitans strain CON/ 180.1254 Aspergillus flavus NRRL 21882; ex- M/91–08; exemption from the requirement emption from the requirement of a toler- of a tolerance. ance. 180.1218 Indian Meal Moth Granulosis Virus; 180.1255 Bacillus pumilus strain QST 2808; ex- exemption from the requirement of a tol- emption from the requirement of a toler- erance. ance.

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180.1256 Alternaria destruens strain 059; ex- 180.1284 Ammonium salts of higher fatty emption from the requirement of a toler- acids (C8-C18 saturated; C8-C12 unsatu- ance. rated); exemption from the requirement 180.1257 Paecilomyces lilacinus strain 251; ex- of a tolerance. emption from the requirement of a toler- 180.1285 Polyoxin D zinc salt; exemption ance. from the requirement of a tolerance. 180.1258 Acetic acid; exemption from the re- 180.1287 Extract of Chenopodium ambrosioides quirement of a tolerance. near ambrosioides; exemption from the re- 180.1259 Reynoutria sachalinensis extract; ex- quirement of a tolerance. emption from the requirement of a toler- 180.1288 Tristyrylphenol ethoxylates; ex- ance. emption from the requirement of a toler- 180.1260 Muscodor albus QST 20799 and the ance. volatiles produced on rehydration; ex- 180.1289 Candida oleophila Strain O; exemp- emption from the requirement of a toler- tion from the requirement of a tolerance. ance. 180.1290 Pasteuria usgae; exemption from the 180.1261 Xanthomonas campestris pv. requirement of a tolerance. vesicatoria and Pseudomonas syringae pv. 180.1291 Cold pressed neem oil; exemption tomato specific Bacteriophages. from the requirement of a tolerance. 180.1262 Sorbitol octanoate; exemption from 180.1292 Ulocladium oudemansii (U3 Strain); the requirement of a tolerance. exemption from the requirement of a tol- 180.1263 Tetrahydrofurfuryl alcohol; exemp- erance. tion from the requirement of a tolerance. 180.1293 Trichoderma gamsii strain ICC 080; 180.1267 Pantoea agglomerans strain C9–1; ex- exemption from the requirement of a tol- emption from the requirement of a toler- erance. ance. 180.1294 Trichoderma asperellum strain ICC 180.1268 Potassium silicate; exemption from 012; exemption from the requirement of a the requirement of a tolerance. tolerance. 180.1269 Bacillus mycoides isolate J; exemp- 180.1295 Laminarin; exemption from the re- tion from the requirement of a tolerance. quirement of a tolerance. 180.1270 Isophorone; exemption from the re- 180.1296 Terpene Constituents a-terpinene, quirement of a tolerance. d-limonene and p-cymene, of the Extract 180.1271 Eucalyptus oil; exemption from the of Chenopodium ambrosioides near requirement of a tolerance. ambrosioides as Synthetically Manufac- 180.1272 Pantoea agglomerans strain E325; ex- tured; exemption from the requirement emption from the requirement of a toler- of a tolerance. ance. 180.1297 Homobrassinolide; exemption from 180.1273 Beauveria bassiana HF23; exemp- the requirement of a tolerance. tion from the requirement of a tolerance. 180.1298 Trichoderma hamatum isolate 382; 180.1274 Tris (2-ethylhexyl) phosphate; ex- exemption from the requirement of a tol- emption from the requirement of a toler- erance. ance. 180.1299 Prohydrojasmon; exemption from 180.1275 Pythium; exception from the re- the requirement of a tolerance. quirement of a tolerance. 180.1300 Potassium hypochlorite; exemption 180.1276 mild green mosaic from the requirement of a tolerance. tobamovirus strain U2; exemption from 180.1301 Escherichia coli O157:H7 specific the requirement of a tolerance. bacteriophages; temporary exemption 180.1277 Dibasic esters; exemption from the from the requirement of a tolerance. requirement of a tolerance. 180.1302 Sodium Ferric Ethylenediamine- 180.1278 Quillaja saponaria extract tetraacetate (EDTA); exemption from (saponins); exemption from the require- the requirement of a tolerance. ment of a tolerance. 180.1303 Metarhizium anisopliae strain F52; 180.1279 Zucchini yellow mosaic virus— exemption from the requirement of a tol- weak strain; exemption from the require- erance. ment of a tolerance. 180.1304 Pseudomonas fluorescens strain 180.1280 Poly(hexamethylenebiguanide) hy- CL145A; exemption from the requirement drochloride (PHMB); exemption from the of a tolerance. requirement of a tolerance. 180.1305 Chromobacterium subtsugae strain 180.1281 S-Abscisic Acid, (S)-5-(1-hydroxy- PRAA4–1T; exemption from the require- 2,6,6-trimethyl-4-oxo-1-cyclohex-2-enyl)- ment of a tolerance. 3-methyl-penta-(2Z,4E)-dienoic Acid; ex- 180.1306 Isaria fumosorosea (formerly emption from the requirement of a toler- Paecilomyces fumosoroseus) Apopka ance. strain 97; exemption from the require- 180.1282 Bacillus firmus I-1582; exemption ment of a tolerance. from the requirement of a tolerance. 180.1307 Bacteriophage of Clavibacter 180.1283 (Z)-7,8-epoxy-2-methyloctadecane michiganensis subspecies michiganensis; (Disparlure); exemption from the re- exemption from the requirement of a tol- quirement of a tolerance. erance.

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180.1308 Bacillus amyloliquefaciens strain 180.1329 Bacillus subtilis strain IAB/BS03, D747; exemption from the requirement of exemption from the requirement of a tol- a tolerance. erance. 180.1309 Bacillus subtilis strain CX–9060; ex- emption from the requirement of a toler- Subpart E—Pesticide Chemicals Not Re- ance. quiring a Tolerance or an Exemption 180.1310 Trichoderma virens strain G–41; ex- from a Tolerance emption from the requirement of a toler- ance. 180.1330 1-Octanol; exemption from the re- quirement of a tolerance. 180.1311 Pasteuria nishizawae—Pn1; exemp- tion from the requirement of a tolerance. 180.1331 Trichoderma asperelloides strain JM41R; exemption from the requirement 180.1312 Aureobasidium pullulans strains of a tolerance. DSM 14940 and DSM 14941; exemption from the requirement of a tolerance. Subpart E—Pesticide Chemicals Not Re- 180.1313 Bacillus pumilus strain GHA 180; ex- quiring a Tolerance or an Exemption emption from the requirement of a toler- From a Tolerance ance. 180.1314 Killed, nonviable Streptomyces 180.2000 Scope. acidiscabies strain RL–110T; exemption 180.2003 Definitions. from the requirement of a tolerance. 180.2010 Threshold of regulation determina- 180.1315 Natamycin; exemption from the re- tions. quirement of a tolerance. 180.2020 Non-food determinations. 180.1316 Pasteuria spp. (Rotylenchulus reniformis nematode)—Pr3; exemption AUTHORITY: 21 U.S.C. 321(q), 346a and 371. from the requirement of a tolerance. SOURCE: 36 FR 22540, Nov. 25, 1971, unless 180.1317 Pesticide chemicals; exemption otherwise noted. from the requirements of a tolerance. EDITORIAL NOTE: Nomenclature changes to 180.1318 3-decen-2-one; exemption from the part 180 appear at 62 FR 66023, Dec. 17, 1997. requirement of a tolerance. 180.1319 Banda de Lupinus albus doce GLOSSARY (BLAD); exemption from the requirement NOTE: The items in this glossary were com- of a tolerance. piled as an aid to the users of the Code of 180.1320 Methyl jasmonate; exemption from Federal Regulations. Inclusion or exclusion the requirement of a tolerance. from this glossary has no legal significance. 180.1321 Complex Polymeric Polyhydroxy APPLI = APPLICATION Acids; exemption from the requirement C-I MET = CHOLINESTERASE-INHIBITING of a tolerance. METABOLITES 180.1322 Bacillus pumilus strain BU F–33; ex- CARB = emption from the requirement of a toler- EPWRR = EDIBLE PORTION WITH RIND ance. REMOVED 180.1323 Ethyl-2E,4Z-decadienoate (Pear EXC = EXCEPT Ester); exemption from the requirement I (IN PPM COLUMN) = INTERIM TOLER- of a tolerance. ANCE 180.1324 GS-omega/kappa-Hxtx-Hv1a; ex- INC = INCLUDING emption from the requirement of a toler- K=CWHR = KERNEL PLUS COB WITH ance. HUSK REMOVED 180.1325 Heat-killed Burkholderia spp. strain MBYP = MEAT BYPRODUCTS A396 cells and spent fermentation media MIN = MINIMUM exemption from the requirement of a tol- N (IN PPM COLUMN) = NEGLIGIBLE RESI- erance. DUES 180.1326 Pseudomonas fluorescens strain D7; NMT = NOT MORE THAN exemption from the requirement of a tol- NON-PER BAG/PKGD RAC = NON-PERISH- erance. ABLE PACKAGED OR BAGGED RAW AG- 180.1327 Tetraacetylethylenediamine RICULTURAL COMMODITY (TAED) and its metabolite PPM = PART(S) PER MILLION Diacetylethylenediamine (DAED); ex- POST-H = POSTHARVEST APPLICATION emption from the requirement of a toler- PRE-H = PREHARVEST APPLICATION ance. PRE-S = PRESLAUGHTER APPLICATION 180.1328 Beauveria bassiana strain ANT–03; PRODS = PRODUCTS rollert exemption from the requirement of a tol- T (IN PPM COLUMN) = TEMPORARY TOL- erance. ERANCE [41 FR 4537, Jan. 30, 1976]

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Subpart A—Definitions and 402 and 408(a), despite the lack of a tol- Interpretative Regulations erance or exemption for the pesticide chemical residue in the processed food, § 180.1 Definitions and interpretations. if: (a) Administrator, without qualifica- (1) The pesticide chemical has been tion, means the Administrator of the used in or on the raw agricultural com- Environmental Protection Agency. modity in conformity with a tolerance (b) Agency, without qualification, under this section; means the Environmental Protection (2) The pesticide chemical residue Agency. has been removed to the extent pos- (c) FFDCA means the Federal Food, sible in good manufacturing practice; Drug, and Cosmetic Act, as amended, and 21 U.S.C. 301–392. (3) The concentration of the pesticide (d) Raw agricultural commodities in- chemical residue in the processed food clude, among other things, fresh fruits, is not greater than the tolerance pre- whether or not they have been washed scribed for the pesticide chemical res- and colored or otherwise treated in idue on the raw agricultural com- their unpeeled natural form; vegetables modity. in their raw or natural state, whether (f) For the purpose of computing fees or not they have been stripped of their as required by § 180.33, each group of re- outer leaves, waxed, prepared into lated crops listed in § 180.34(e) and each fresh green salads, etc.; grains, nuts, crop group or subgroup listed in § 180.41 eggs, raw milk, meats, and similar ag- is counted as a single raw agricultural ricultural produce. It does not include commodity in a petition or request for foods that have been processed, fab- tolerances or exemption from the re- ricated, or manufactured by cooking, quirement of a tolerance. freezing, dehydrating, or milling. (g) Tolerances and exemptions estab- (e) Where a raw agricultural com- lished for pesticide chemicals in or on modity bearing a pesticide chemical the general category of raw agricul- residue that has been exempted from tural commodities listed in column A the requirement of a tolerance, or apply to the corresponding specific raw which is within a tolerance permitted agricultural commodities listed in col- under FFDCA section 408, is used in umn B. However, a tolerance or exemp- preparing a processed food, the proc- tion for a specific commodity in col- essed food will not be considered unsafe umn B does not apply to the general within the meaning of FFDCA sections category in column A.

A B

Alfalfa Medicago sativa L. Subsp. sativa, (alfalfa, lucerne); Onobrychis viciifolia Scop. (sainfoin, holy clover, esparcet); and Lotus corniculatus L. (trefoil); and varieties and/or hybrids of these.

Banana Banana, plantain.

Bean Cicer arietinum (chickpea, garbanzo bean); Lupinus spp. (including sweet lupine, white sweet lupine, white lupine, and grain lupine). Phaseolus spp. (including kidney bean, lima bean, mung bean, navy bean, pinto bean, snap bean, and waxbean; Vicia faba (broad bean, fava bean); Vigna spp. (including asparagus bean, blackeyed pea and cowpea).

Bean, dry All beans above in dry form only.

Bean, succulent All beans above in succulent form only.

Blackberry Rubus eubatus (including bingleberry, black satin , boysenberry Cherokee blackberry, Chesterberry, Cheyenne blackberry, coryberry, darrowberry, dewberry, Dirksen thornless berry, Himalayaberry, hullberry, Lavacaberry, lowberry, Lucretiaberry, mammoth blackberry, marionberry, nectarberry, olallieberry, Oregon evergreen berry, phenomenalberry, rangerberry, ravenberry, rossberry, Shawnee blackberry, and varieties and/or hybrids of these).

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A B

Broccoli Broccoli, chinese broccoli (gia lon, white flowering broccoli).

Cabbage Cabbage, Chinese cabbage (tight-heading varieties only).

Caneberry Rubus spp. (including blackberry); Rubus caesius (youngberry); Rubus loganbaccus (loganberry); Rubus idaeus (red and black raspberry); cultivars, varieties, and/or hy- brids of these.

Celery Celery, Florence fennel (sweet anise, sweet fennel, finochio) (fresh leaves and stalks only).

Cherry Cherry, sweet, and cherry, tart.

Endive Endive, escarole.

Fruit, citrus Grapefruit, lemon, lime, orange, tangelo, tangerine, citrus citron, kum- quat, and hybrids of these.

Garlic , great headed; garlic, and serpent garlic.

Lettuce Lettuce, head; and lettuce, leaf

Lettuce, head Lettuce, head; crisphead varieties only

Lettuce, leaf Lettuce, leaf; cos (romaine), butterhead varieties

Marjoram Origanum spp. (includes sweet or annual marjoram, wild marjoram or oregano, and pot marjoram).

Melon Muskmelon, including hybrids and/or varieties of Cucumis melo (includ- ing true cantaloupe, cantaloupe, casaba, Santa Claus melon, cren- shaw melon, honeydew melon, honey balls, Persian melon, golden pershaw melon, mango melon, pineapple melon, snake melon); and watermelon, including hybrids and/or varieties of (Citrullus spp.).

Muskmelon Cucumis melo (includes true cantaloupe, cantaloupe, casaba, Santa Claus melon, crenshaw melon, honeydew melon, honey balls, Per- sian melon, golden pershaw melon, mango melon, pineapple melon, snake melon, and other varieties and/or hybrids of these.)

Onion ; green onion; and garlic.

Onion, bulb Bulb onion; garlic; great headed garlic; serpent garlic; Chinese onion; ; ; and , bulb.

Onion, green Green onion; lady’s ; leek; wild leek; Beltsville bunching onion; fresh onion; tree onion, tops; Welsh onion; and shallot, fresh leaves.

Peach Peach, nectarine

Pea Cajanus cajan (includes pigeon pea); Cicer spp. (includes chickpea and garbanzo bean); Lens culinaris (lentil); Pisum spp. (includes dwarf pea, garden pea, green pea, English pea, field pea, and edible pod pea). [Note: A variety of pesticide tolerances have been pre- viously established for pea and/or bean. Chickpea/garbanzo bean is now classified in both the bean and the pea categories. For garbanzo bean/chickpea only, the highest established pea or bean tolerance will apply to pesticide residues found in this commodity.]

Pea, dry All peas in dry form only.

Pea, succulent All peas in succulent form only.

Pepper All varieties of pepper including pimento and bell, hot, and sweet pep- per.

Radish, oriental, roots Raphanus sativus var. longipinnatus (roots and tops), including Chi- nese or Japanese radish (both white and red), winter radish, daikon, lobok, lo pak, and other cultivars and/or hybrids of these.

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A B

Radish, oriental, tops) Raphanus sativus var. longipinnatus (roots and tops), including Chi- nese or Japanese radish (both white and red), winter radish, daikon, lobok, lo pak, and other cultivars and/or hybrids of these.

Rapeseed Brassica napus, B. campestris, and Crambe abyssinica (oilseed-pro- ducing varieties only which include canola and crambe.)

Raspberry Rubus spp. (including bababerry; black raspberry; blackcap; caneberry; framboise; frambueso; himbeere; keriberry; mayberry; red raspberry; thimbleberry; tulameen; yellow raspberry; and cultivars, varieties, and/or hybrids of these).

Sorghum, grain, grain Sorghum spp. [sorghum, grain, sudangrass (seed crop), and hybrids of these grown for its seed].

Sorghum, forage, stover Sorghum spp. [sorghum, forage; sorghum, stover; sudangrass, and hy- brids of these grown for forage and/or stover.

Squash Pumpkin, summer squash, and winter squash.

Sugar apple Annona squamosa L. (sugar apple, sweetsop, anon), and its hybrid A. squamosa L. x A. cherimoya M. (atemoya). Also A. reticulata L. (true custard apple).

Squash, summer Fruits of the gourd (Cucurbitaceae) family that are consumed when im- mature, 100% of the fruit is edible either cooked or raw, once picked it cannot be stored, has a soft rind which is easily penetrated, and if seeds were harvested they would not germinate; e.g., Cucurbita pepo (i.e., crookneck squash, straightneck squash, scallop squash, and vegetable marrow); Lagenaria spp. (i.e., spaghetti squash, hyotan, cucuzza); Luffa spp. (i.e., hechima, Chinese okra); Momordica spp. (i.e., bitter melon, balsam pear, balsam apple, Chi- nese cucumber); Sechium edule (chayote); and other cultivars and/or hybrids of these.

Sweet potato Sweet potato, yam.

Tangerine Tangerine (mandarin or mandarin orange); clementine; Mediterranean mandarin; satsuma mandarin; tangelo; tangor; cultivars, varieties, and/or hybrids of these.

Tomato Tomato, tomatillo.

Turnip tops or turnip greens Broccoli raab (raab, raab salad), hanover salad, turnip tops (turnip greens).

Wheat Wheat, triticale.

(h) Unless otherwise specified in this (4) Stems shall be removed and dis- paragraph or in tolerance regulations carded from melons before examination prescribed in this part for specific pes- for pesticide residues. ticide chemicals, the raw agricultural (5) Roots, stems, and outer sheaths commodity or processed food to be ex- (or husks) shall be removed and dis- amined for pesticide residues, shall carded from garlic and dry bulb consist of the whole raw agricultural , and only the garlic cloves and commodity or processed food. onion bulbs shall be examined for pes- ticide residues. (1) The raw agricultural commodity (6) Where a tolerance is established bananas, when examined for pesticide on a root vegetable including tops and/ residues, shall not include any crown or with tops, and the tops and the roots tissue or stalk. are marketed together, they shall be (2) Shell shall be removed and dis- analyzed separately and neither the carded from nuts before examination pesticide residue on the roots nor the for pesticide residues. pesticide residue on the tops shall ex- (3) Caps (hulls) shall be removed and ceed the tolerance level, except that in discarded from strawberries before ex- the case of carrots, parsnips, and ruta- amination for pesticide residues. bagas, the tops shall be removed and

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discarded before analyzing roots for field-dried beans, field-dried peas, pesticide residues. grains, and nuts. Not included are eggs, (7) The crowns (leaves at the top of milk, meat, poultry, fresh fruits, and the fruit) shall be removed and dis- vegetables such as onions, parsnips, po- carded from pineapples before examina- tatoes, and carrots. tion for pesticide residues. (l) The term tolerance with regional (8) The term lima beans means the registration means any tolerance which beans and the pod. is established for pesticide residues re- (9) The term peanuts means the pea- sulting from the use of the pesticide nut meat after removal of the hulls. pursuant to a regional registration. (10) For processed foods consisting Such a tolerance is supported by res- primarily of one ingredient and sold in idue data from specific growing regions a form requiring further preparation for a raw agricultural commodity. Indi- prior to consumption (e.g., fruit juice vidual tolerances with regional reg- concentrates, dehydrated vegetables, istration are designated in separate and powdered potatoes), the processed subsections in 40 CFR 180.101 through food to be examined for residues shall 180.999, as appropriate. Additional res- be the whole processed commodity idue data which are representative of after compensating for or reconsti- the proposed use area are required to tuting to the commodity’s normal expand the geographical area of usage moisture content, unless a tolerance of a pesticide on a raw agricultural for the concentrated or dehydrated commodity having an established ‘‘tol- food form is included in this part. If erance with regional registration.’’ there exists a tolerance for a specific Persons seeking geographically broad- pesticide on the processed food in its er registration of a crop having a ‘‘tol- concentrated or dehydrated food form, erance with regional registration’’ for the purpose of determining whether should contact the appropriate EPA the food is in compliance with that tol- product manager concerning additional erance, the processed food to be exam- residue data required to expand the use ined for residues shall be the whole area. processed commodity on an ‘‘as is’’ (m) The term pesticide chemical res- basis. idue shall have the meaning specified (i) The term pesticide chemical shall in FFDCA section 201(q)(2), as amend- have the meaning specified in FFDCA ed, except as provided in § 180.4. section 201(q)(1), as amended, except as (n) The term food commodity means: provided in § 180.4. (1) Any raw agricultural commodity (j) The term negligible residue means (food or feed) as defined in section any amount of a pesticide chemical re- 201(r) of the Federal Food, Drug, and maining in or on a raw agricultural Cosmetic Act (FFDCA); and commodity or group of raw agricul- (2) Any processed food or feed as de- tural commodities that would result in fined in section 201(gg) of the FFDCA. a daily intake regarded as toxicologically insignificant on the [36 FR 22540, Nov. 25, 1971] basis of scientific judgment of ade- EDITORIAL NOTE: For FEDERAL REGISTER ci- quate safety data. Ordinarily this will tations affecting § 180.1, see the List of CFR add to the diet an amount which will Sections Affected, which appears in the be less than 1/2,000th of the amount Finding Aids section of the printed volume that has been demonstrated to have no and at www.fdsys.gov. effect from feeding studies on the most sensitive animal species tested. Such § 180.3 Tolerances for related pesticide studies shall usually include chemicals. at least 90-day feeding studies in two (a) Pesticide chemicals that cause re- species of mammals. lated pharmacological effects will be (k) The term nonperishable raw agri- regarded, in the absence of evidence to cultural commodity means any raw agri- the contrary, as having an additive del- cultural commodity not subject to eterious action. (For example, many rapid decay or deterioration that would pesticide chemicals within each of the render it unfit for consumption. Exam- following groups have related pharma- ples are cocoa beans, coffee beans, cological effects: Chlorinated organic

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, -containing chemi- and (a mixture of O,O-diethyl cals, metallic dithiocarbamates, cho- O-(and S-) [2-(ethylthio)ethyl] linesterase-inhibiting pesticides.) phosphorothioates) on the same raw (b) Tolerances established for such agricultural commodity, the total related pesticide chemicals may limit amount of such pesticides shall not the amount of a common component yield more residue than that permitted (such as As2O3) that may be present, or by the larger of the two tolerances, cal- may limit the amount of biological ac- culated as demeton. tivity (such as cholinesterase inhibi- (3) Where tolerances are established tion) that may be present, or may limit for both terpene polychlorinates the total amount of related pesticide (chlorinated mixture of camphene, pi- chemicals (such as chlorinated organic nene, and related terpenes, containing pesticides) that may be present. 65–66 percent chlorine) and (c)(1) Where tolerances for inorganic (chlorinated camphene containing 67–69 bromide in or on the same raw agricul- percent chlorine) on the same raw agri- tural commodity are set in two or cultural commodities, the total more sections in this part (example: amount of such pesticides shall not §§ 180.123 and 180.199), the overall quan- yield more residue than that permitted tity of inorganic bromide to be toler- by the larger of the two tolerances, cal- ated from use of the same pesticide in culated as a chlorinated terpene of mo- different modes of application or from lecular weight 396.6 containing 67 per- two or more pesticide chemicals for cent chlorine. which tolerances are established is the (4) Where a tolerance is established highest of the separate applicable tol- for more than one pesticide containing erances. For example, where the bro- arsenic found in, or on a raw agricul- mide tolerance on asparagus from tural commodity, the total amount of methyl bromide commodity fumigation such pesticide shall not exceed the is 100 parts per million (40 CFR 180.123) highest established tolerance cal- and on asparagus from methyl bromide culated as As2O3. soil treatment is 300 parts per million (5) Where tolerances are established (40 CFR 180.199), the overall inorganic for more than one member of the class bromide tolerance for asparagus grown of dithiocarbamates listed in para- on methyl bromide-treated soil and graph (e)(3) of this section on the same also fumigated with methyl bromide raw agricultural commodity, the total after harvest is 300 parts per million. residue of such pesticides shall not ex- (2) Where tolerances are established ceed that permitted by the highest tol- in terms of inorganic bromide residues erance established for any one member only from use of organic bromide fumi- of the class, calculated both as zinc gants on raw agricutural commodities, ethylenebisdithiocarbamate and car- such tolerances are sufficient to pro- bon disulfide. The tolerance based on tect the public health, and no addi- zinc ethylenebisdithiocarbamate shall tional concurrent tolerances for the or- first be multiplied by 0.6 to convert it ganic pesticide chemicals from such to the equivalent carbon disulfide tol- use are necessary. This conclusion is erance, and then the carbon disulfide based on evidence of the dissipation of tolerance levels will be compared to de- the organic pesticide or its conversion termine the highest tolerance level per to inorganic bromide residues in the raw agricultural commodity. food when ready to eat. (6) Where tolerances are established (d)(1) Where tolerances are estab- for residues of both S,S,S-tributyl lished for both calcium cyanide and hy- phosphorotrithioate and tributyl drogen cyanide on the same raw agri- phosphorotrithioite in or on the same cultural commodity, the total amount raw agricultural commodity, the total of such pesticides shall not yield more amount of such pesticides shall not residue than that permitted by the yield more residue than that permitted larger of the two tolerances, calculated by the higher of the two tolerances, as hydrogen cyanide. calculated as S,S,S-tributyl (2) Where tolerances are established phosphorotrithioate. for residues of both O,O-diethyl S-[2- (7) Where tolerances are established (ethylthio)ethyl] phosphorodithioate for residues of O,S-dimethyl

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phosphoramidothioate, resulting from the same as that for the chemical hav- the use of acephate (O,S-dimethyl ing the lowest numerical tolerance in acetylphos-phoramidothioate) and/or this class, unless a higher tolerance O,S - dimethylphosphoramidothioate level is specifically provided for the on the same agricultural commodity, combined residues by a regulation in the total amount of O,S-dimethyl- this part. phosphoramidothioate shall not yield (1) Where residues from two or more more residue than that permitted by chemicals in the same class are present the higher of the two tolerances. in or on a raw agricultural commodity (8) Where a tolerance is established and there are available methods that for more than one pesticide having the permit quantitative determination of metabolites 1-(3,4-dichlorophenyl)-3- each residue, the quantity of combined methylurea (DCPMU) and 3,4- residues that are within the tolerance dichlorophenylurea (DCPU) found in or may be determined as follows: on a raw agricultural commodity, the (i) Determine the quantity of each total amount of such residues shall not residue present. exceed the highest established toler- (ii) Divide the quantity of each res- ance for a pesticide having these me- idue by the tolerance that would apply tabolites. if it occurred alone, and multiply by (9) Where a tolerance is established 100 to determine the percentage of the for more than one pesticide having as permitted amount of residue present. metabolites compounds containing the (iii) Add the percentages so obtained benzimidazole moiety found in or on a raw agricultural commodity, the total for all residues present. amount of such residues shall not ex- (iv) The sum of the percentages shall ceed the highest established tolerance not exceed 100 percent. for a pesticide having these metabo- (2) Where residues from two or more lites. chemicals in the same class are present (10) Where a tolerance is established in or on a raw agricultural commodity for triclopyr, chloropyrifos, and and there are available methods that chlorpyrifos-methyl having the com- permit quantitative determinations of mon metabolite 3,5,6-trichloro-2- one or more, but not all, of the resi- pyridinol on the same raw agricultural dues, the amounts of such residues as commodity, the total amount of such may be determinable shall be deducted residues shall not exceed the highest from the total amount of residues established tolerance for any of the present and the remainder shall have pesticides having the metabolites. the same tolerance as that for the (11) Where tolerances are established chemical having the lowest numerical for more than one pesticide having the tolerance in that class. The quantity of metabolite 3,5,6-trichloro-2-pyridinol combined residues that are within the found in or on the raw agricultural tolerance may be determined as fol- commodity, the total amount of such lows: residues shall not exceed the highest (i) Determine the quantity of each established tolerance for a pesticide determinable residue present. having this metabolite. (ii) Deduct the amounts of such resi- (12) Where tolerances are established dues from the total amount of residues for residues of methomyl, resulting present and consider the remainder to from the use of thiodicarb and/or have the same tolerance as that for the methomyl on the same raw agricul- chemical having the lowest numerical tural commodity, the total amount of tolerance in that class. methomyl shall not yield more residue (iii) Divide the quantity of each de- than that permitted by the higher of terminable residue by the tolerance the two tolerances. that would apply if it occurred alone (e) Except as noted in paragraphs and the quantity of the remaining res- (e)(1) and (2) of this section, where resi- idue by the tolerance for the chemical dues from two or more chemicals in the having the lowest numerical tolerance same class are present in or on a raw in that class and multiply by 100 to de- agricultural commodity the tolerance termine the percentage of the per- for the total of such residues shall be mitted amount of residue present.

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(iv) Add the percentages so obtained Sesone (sodium 2,4-dichlorophenoxyethyl for all residues present. sulfate, SES). (v) The sum of the percentages shall Sodium 2,4-dichlorophenoxyacetate. not exceed 100 percent. Sodium trichloroacetate. Sulphenone (p-chlorophenyl phenyl sulfone). (3) The following pesticides are mem- Terpene polychlorinates (chlorinated mix- bers of the class of dithiocarbamates: ture of camphene, pinene, and related A mixture of 5.2 parts by weight of ammoni- terpenes 65-66 percent chlorine). ates of [ethylenebis (dithiocarbamato)] 2,3,5,6-Tetrachloronitrobenzene. ′ zinc with 1 part by weight ethylenebis (2,4,5,4 -tetrachlorodiphenyl [dithiocarbamic acid] bimolecular and sulfone). trimolecular cyclic anhydrosulfides and Toxaphene (chlorinated camphene). disulfides. Trichlorobenzoic acid. 2-Chloroallyl diethyldithiocarbamate. Trichlorobenzyl chloride. Coordination product of zinc ion and maneb (5) The following are members of the containing 20 percent manganese, 2.5 per- class of cholinesterase-inhibiting pes- cent zinc, and 77.5 percent ticides: ethylenebisdithiocarbamate. Ferbam. Acephate (O,S-dimethyl acetyl- Maneb. phosphoramidothioate) and its cholin- Manganous dimethyldithiocarbamate. esterase-inhibiting metabolite O,S-di- Sodium dimethyldithiocarbamate. methyl phosphoramidothioate. Thiram. Aldicarb (2-methyl-2-(methylthio) Zineb. propionaldehyde O- Ziram. (methylcarbamoyl)oxime) and its (4) The following are members of the chlorinesterase-inhibiting metabolites 2- methyl-2-(methylsulfinyl)propionaldehyde class of chlorinated organic pesticides: O-(methycarbamoyl) oxime and 2-methyl- . 2-(methylsulfonyl)propionaldehyde O- BHC (benzene hexachloride). (methylcarbamoyl)oxime. 1,1-Bis(p-chlorophenyl)-2,2,2- 4-tert-Butyl-2-chlorophenyl methyl methyl trichloroethanol. phosphoramidate. Chlorbenside (p-chlorobenzyl p-chlorophenyl S-[(tert-Butylthio)methyl] O,O-diethyl sulfide). phosphorodithioate and its cholinesterase- . inhibiting metabolites. Chlorobenzilate (ethyl 4,4′- Carbaryl (1-naphthyl N-methylcarbamate). dichlorobenzilate). Carbofuran (2,3,-dihydro-2,2-dimethyl-7- p-Chlorophenoxyacetic acid. benzofuranyl-N-methylcarbamate). p-Chlorophenyl-2,4,5-trichlorophenyl sulfide. Carbofuran metabolite (2,3-dihydro-2,2-di- 2,4-D (2,4-dichlorophenoxyacetic acid). methyl-3-hydroxy-7-benofuranyl N- DDD (TDE). methylcarbamate). DDT. (S-[(p-chlorophenyl) 1,1-Dichloro-2,2-bis(p-ethylphenyl) ethane. thiolmethyl] O,O-diethyl 2,6-Dichloro-4-nitroaniline. phosphorodithioate) and its cholinesterase- 2,4-Dichlorophenyl p-nitrophenyl ether. inhibiting metabolites. . Chlorpyrifos (O,O-diethyl O-(3,5,6-trichloro- Dodecachlorooctahydro-1,3,4-metheno-2H- 2-pyridyl)phosphorothioate). cyclobuta[cd]pentalene. Chlorpyrifos-methyl (O,O-dimethyl-O-(3,5,6- Endosulfan (6,7,8,9,10,10-hexachloro-1,5,5a, trichloro-2-pyridyl) phosphorothioate. 6,9,9a-hexahydro-6,9-methano-2,4,3- 2-Chloro-1-(2,4,5-trichlorophenyl)vinyl di- benzodioxathiepin-3-oxide). methyl phosphate. Endosulfan sulfate (6,7,8,9,10,10-hexachloro- 2-Chloro-1-(2,4-dichlorophenyl) vinyl diethyl 1,5,5a,6,9,9a-hexahydro-6,9-methano-2,4,3- phosphate. benzodioxathiepin-3,3-dioxide). Coumaphos (O,O-diethyl O-3-chloro-4-meth- (1,4,5,6,7,8,8-heptachlor-3a,4,7, 7a- yl-2-oxo-2H-1-benzopyran-7-yl phosran-7-yl tetrahydro-4,7-methanoindene). phosphate). Heptachlor epoxide (1,4,5,6,7,8,8-heptachloro- Coumaphos oxygen analog (O,O-diethyl O-3- 2,3-epoxy-2,3,3a,4,7,7a-hexahydro-4,7- chloro-4-methyl-2-oxo-2H-1- methanoindene). benzopyphorothioate). (2,2′-methylenebis(3,4,6- (S-(2-chloro-1-phthalimidoethyl) trichlorophenol) and its monosodium salt. O,O-diethyl phosphorodithioate). Isopropyl 4,4′-dichlorobenzilate. Dialifor oxygen analog (S-(2-chloro-1- . phthalimidoethyl) O,O-diethyl . phosphorothioate). Ovex (p-chlorophenyl p- Demeton (a mixture of O,O-diethyl O-(and S) chlorobenzenesulfonate). [2-ethylthio)ethyl] phosphorothioates).

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Ethiolate (S-ethyl diethylthiocarbamate). O-Ethyl S,S-dipropylphosphorodithioate. 2,2-Dichlorovinyl dimethyl phosphate. Ethyl 3-methyl-4-(methylthio)phenyl (1- O,O-Diethyl S-[2-(ethylthio)ethyl] methylethyl) phosphoramidate and its cho- phosphorodithioate and its cholinesterase- linesterase-inhibiting metabolites. inhibiting metabolites. O-Ethyl S-phenyl ethylphosphonodithioate. O,O-Diethyl O-(2-diethylamino-6-methyl-4- O-Ethyl S-phenyl ethylphosphonothiolate. pyrimidinyl) phosphorothioate and its oxy- m-(1-Ethylpropyl)phenyl methylcarbamate. gen analog diethyl 2-diethylamino-6-meth- S-[2-Ethylsulfinyl)ethyl] O,O-dimethyl yl-4-pyrimidinyl phosphate. phosphorothioate and its cholinesterase-in- O,O-Diethyl O-(2-isoprophyl-4-methyl-6- hibiting metabolites, (primarily S-[2- pyrimidinyl) phosphorothioate. (ethyl-sulfonyl)ethyl] O,O-dimethyl O,O-Diethyl O-[p-(methylsulfinyl)phenyl] phosphorothioate). phosphorothioate and its cholinesterase-in- hibiting metabolites. (O,O-dimethyl O-[3-methyl-4- Diethyl 2-pyrazinyl phosphate. (methylthio)phenyl]phosphorothioate and O,O-Diethyl O-2-pyrazinyl phosphorothioate. its cholinesterase-inhibiting metabolites. S-(O,O-Diisopropyl phosphorodithioate) of N- Malathion. (2-mercaptoethyl) benzenesulfonamide N-(Mercaptomethyl)phthalimide S-(O,O-di- S-(O,O-Diisopropyl phosphorodithioate) of N- methyl phosphorodithioate). (2-mercaptoethyl) benzenesulfonamide N-(Mercaptomethyl)phthalimide S-(O,O-di- 2-(Dimethylamino)-5.6-dimethyl-4- methyl phosphorothioate). pyrimidinyl dimethylcarbamate and its Methomyl (S-methyl N- metabolites 5,6-dimethyl-2- [(methylcarbamoyl)oxy]thioacetimidate). (formylmethylamino)-4-pyrimidinyl 1-Methoxycarbonyl-1-propen-2-yl dimethyl dimethylcarbamate and 5,6-dimethyl-2- phosphate and its beta isomer. (methylamino)-4-pyrimidinyl m-(1-Methylbutyl)phenyl methylcarbamate. dimethylcarbamate (both calculated as Methyl parathion. parent). Naled (1,2-dibromo-2,2-dichloroethyl di- Dimethoate (O,O-dimethyl S-(N-methyl- methyl phosphate). carbamoylmethyl) phosphorodithioate). Oxamyl (methyl N′,N′-dimethyl-N- Dimethoate oxygen analog (O,O-dimethyl S- [(methylcarbamoyl)oxy]-1- (N-methylcarbamoylmethyl) thiooxamimidate) phosphorothioate). Parathion. O,O-Dimethyl O-p-(dimethylsulfamoyl) Phorate (O,O-diethyl S-(ethylthio)methyl phenyl phosphate. phosphorodithioate) and its cholinesterase- O,O-Dimethyl O-p-(dimethylsulfamoyl) inhibiting metabolites. phenyl phosphorothioate. Phosalone ( -(6-chloro-3-mercaptomethyl)-2- 3,5-Dimethyl-4-(methylthio) phenyl S benzoxazolinone) -diethyl methylcarbamate. O,O O,O-Dimethyl S-[4-oxo-1,2,3-benzotriazin-3- phosphorodithioate). (4H)-ylmethyl] phosphorodithioate. (2-chloro-2-diethylcarbamoyl- Dimethyl phosphate of 3-hydroxy-N,N-di- 1-methylvinyl dimethyl phosphate) includ- methyl-cis-crotonamide. ing all of its related cholinesterase-inhib- Dimethyl phosphate of 3-hydroxy-N-methyl- iting compounds. cis-crotonamide. Pirimiphos-methyl O-[2-diethylamino-6- Dimethyl phosphate of a-methylbenzyl 3-hy- methyl-pyrimidinyl) O,O-dimethyl droxy-cis-crotonate. phosphorothioate O,O-Dimethyl 2,2,2-trichloro-1-hydroxyethyl Ronnel. phosphonate. (octamethylpyrophosphoramide). O,O-Dimethyl phosphorodithioate, S-ester . with 4-(mercaptomethyl)-2-methozy-D2- O,O,O′,O′-Tetramethyl O,O′-sulfinyldi-p- 1,3,4-thiadiazolin-5-one. phenylene phosphorothioate. (2,3-p-dioxanedithiol S,S-bis (O,O- O,O,O′,O′-Tetramethyl O,O′-thiodi-p-phen- diethylphosphorodithioate)) containing ap- ylene phosphorothioate. proximately 70 percent cis and trans iso- Tributyl phosphorotritlioite. mers and approximately 30 percent related S,S,S-Tributyl phosphorothrithioate. compounds. 3,4,5-Trimethylphenyl methylcarbamate and EPN. its isomer 2,3,5-trimethylphenyl Ethephon ((2- - chloroethyl) phosphonic methylcarbamate. acid). . (6) The following pesticides are mem- Ethion oxygen analog (S- bers of the class of dinitrophenols: [[(diethoxyphosphinothioyl)thio] methyl] O,O-diethyl phosphorothioate). 2,4-Dinitro-6-octylphenyl crotonate and 2,6- O- Ethyl O-[4-(methylthio) phenyl] S-propyl dinitro-4-octylphenyl crotonate, mixture phosphorodithioate and its cholinesterase- of. inhibiting metabolites. 4,6-Dinitro-o-cresol and its sodium salt.

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Dinoseb (2-sec-butyl-4,6-dinitrophenol) and prior to introduction of the raw agri- its alkanolamine, ammonium, and sodium cultural commodity into interstate salts. commerce. [41 FR 8969, Mar. 2, 1976] § 180.6 Pesticide tolerances regarding EDITORIAL NOTE: For FEDERAL REGISTER ci- milk, eggs, meat, and/or poultry; tations affecting § 180.3, see the List of CFR Sections Affected, which appears in the statement of policy. Finding Aids section of the printed volume (a) When establishing tolerances for and at www.fdsys.gov. pesticide residues in or on raw agricul- tural commodities, consideration is al- § 180.4 Exceptions. ways given to possible residues of those The substances listed in this section pesticide chemicals or their conversion are excepted from the definitions of products entering the diet of man ‘‘pesticide chemical’’ and ‘‘pesticide through the ingestion of milk, eggs, chemical residue’’ under FFDCA sec- meat, and/or poultry produced by ani- tion 201(q)(3) and are therefore exempt mals fed agricultural products bearing from regulation under FFDCA section such pesticide residues. In each in- 402(a)(2)(B) and 408. These substances stance an evaluation of all available are subject to regulation by the Food data will result in a conclusion either: and Drug Administration as food addi- (1) That finite residues will actually tives under FFDCA section 409. be incurred in these foods from feed use (a) Inert ingredients in food pack- of the raw agricultural commodity in- aging treated with a pesticide, when cluding its byproducts; or such inert ingredients are the compo- (2) That it is not possible to establish nents of the food packaging material with certainty whether finite residues (e.g. paper and paperboard, coatings, will be incurred, but there is a reason- adhesives, and polymers). able expectation of finite residues; or (b) [Reserved] (3) That it is not possible to establish [63 FR 10720, Mar. 4, 1998, as amended at 73 with certainty whether finite residues FR 54976, Sept. 24, 2008] will be incurred, but there is no reason- able expectation of finite residues. § 180.5 Zero tolerances. (b) When the data show that finite A zero tolerance means that no residues will actually be incurred in amount of the pesticide chemical may milk, eggs, meat, and/or poultry, a tol- remain on the raw agricultural com- erance will be established on the raw modity when it is offered for shipment. agricultural commodity used as feed A zero tolerance for a pesticide chem- provided that tolerances can be estab- ical in or on a raw agricultural com- lished at the same time, on the basis of modity may be established because, the toxicological and other data avail- among other reasons: able, for the finite residues incurred in (a) A safe level of the pesticide chem- milk, eggs, meat, and/or poultry. When ical in the diet of two different species it is not possible to determine with cer- of warm-blooded animals has not been tainty whether finite residues will be reliably determined. incurred in milk, eggs, meat, and/or (b) The chemical is carcinogenic to poultry but there is a reasonable expec- or has other alarming physiological ef- tation of finite residues in light of data fects upon one or more of the species of reflecting exaggerated pesticides levels the test animals used, when fed in the in feeding studies, a tolerance will be diet of such animals. established on the raw agricultural (c) The pesticide chemical is toxic, commodity provided that appropriate but is normally used at times when, or tolerances can be established at the in such manner that, fruit, vegetables, same time, on the basis of the toxi- or other raw agricultural commodities cological and other data available, for will not bear or contain it. the finite residues likely to be incurred (d) All residue of the pesticide chem- in these foods through the feed use of ical is normally removed through good the raw agricultural commodity or its agricultural practice such as washing byproducts. When it is not possible to or brushing or through weathering or determine with certainty whether fi- other changes in the chemical itself, nite residues will be incurred in milk,

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eggs, meat, and/or poultry but there is 408(g)(2) may be sent. The petition no reasonable expectation of finite res- must be signed by the petitioner or by idues in light of data such as those re- his attorney or agent, or (if a corpora- flecting exaggerated pesticide levels in tion) by an authorized official. feeding studies and those elucidating (b) Petitions shall include the fol- the biochemistry of the pesticide lowing information: chemical in the animal, a tolerance (1) An informative summary of the may be established on the raw agricul- petition and of the data, information, tural commodity without the necessity and arguments submitted or cited in of a tolerance on food products derived support of the petition. Both a paper from the animal. and electronic copy of the summary (c) The principles outlined in para- should be submitted. The electronic graphs (a) and (b) of this section will copy should be formatted according to also be followed with respect to toler- the Office of Pesticide Programs’ cur- ances for residues which will actually rent standard for electronic data sub- be incurred or are reasonably to be ex- mission as specified at http:// pected in milk, eggs, meat, and/or poul- www.epa.gov/pesticides/regulating/reg- try by the use of pesticides directly on istering/submissions/index.htm. the animal or administered purposely (2) A statement that the petitioner in the feed or drinking water. agrees that such summary or any in- (d) Tolerances contemplated by para- formation it contains may be published graphs (a) and (b) of this section will in as a part of the notice of filing of the addition to toxicological consider- petition to be published under FFDCA ations be conditioned on the avail- section 408(d)(3) and as a part of a pro- ability of a practicable analytical posed or final regulation issued under method to determine the pesticide res- FFDCA section 408. idue; that is, the method must be sen- (3) The name, chemical identity, and sitive and reliable at the tolerance composition of the pesticide chemical level or in special cases at a higher residue and of the pesticide chemical level where such level is deemed satis- that produces the residue. factory and safe in light of the toxicity (4) Data showing the recommended of the pesticide residue and of the un- amount, frequency, method, and time likelihood of such residue exceeding of application of the pesticide chem- the tolerance. The analytical methods ical. to be used for enforcement purposes (5) Full reports of tests and inves- will be those set forth in the ‘‘Pesticide tigations made with respect to the Analytical Manual’’ (see § 180.101(c)). safety of the pesticide chemical, in- The sensitivities of these methods are cluding full information as to the expressed in that manual. methods and controls used in con- ducting those tests and investigations. Subpart B—Procedural (6) Full reports of tests and inves- Regulations tigations made with respect to the na- ture and amount of the pesticide chem- § 180.7 Petitions proposing tolerances ical residue that is likely to remain in or exemptions for pesticide resi- or on the food, including a description dues in or on raw agricultural com- of the analytical methods used. (See modities or processed foods. § 180.34 for further information about (a) Petitions to be filed with the residue tests.) Agency under the provisions of FFDCA (7) Proposed tolerances for the pes- section 408(d) shall be submitted in du- ticide chemical residue if tolerances plicate. If any part of the material sub- are proposed. mitted is in a foreign language, it shall (8) Practicable methods for removing be accompanied by an accurate and any amount of the residue that would complete English translation. The peti- exceed any proposed tolerance. tion shall be accompanied by an ad- (9) A practical method for detecting vance deposit for fees described in and measuring the levels of the pes- § 180.33. The petition shall state the pe- ticide chemical residue in or on the titioner’s mail address to which notice food, or for exemptions, a statement of objection under FFDCA section why such a method is not needed.

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(10) If the petition relates to a toler- lication in the FEDERAL REGISTER of ance for a processed food, reports of in- the notice of the petition filing. vestigations conducted using the proc- (e) The Administrator shall notify essing method(s) used to produce that the petitioner within 15 days after its food. receipt of acceptance or nonacceptance (11) Such information as the Admin- of a petition, and if not accepted the istrator may require to make the de- reasons therefor. If petitioner desires, termination under FFDCA section the petitioner may supplement a defi- 408(b)(2)(C). cient petition after notification as to (12) Such information as the Admin- deficiencies. If the petitioner does not istrator may require on whether the wish to supplement or explain the peti- pesticide chemical may have an effect tion and requests in writing that it be in humans that is similar to an effect filed as submitted, the petition shall be produced by a naturally occurring es- filed and the petitioner so notified. trogen or other endocrine effects. (f) A notice of the filing of a petition (13) Information regarding exposure for a pesticide chemical residue toler- to the pesticide chemical residue due ance that the Administrator deter- to any tolerance or exemption already mines has met the requirements of granted for such residue. paragraph (b) of this section shall be published in the FEDERAL REGISTER by (14) Information concerning any max- the Administrator within 30 days after imum residue level established by the such determination. The notice shall Codex Alimentarius Commission for state the name of the pesticide chem- the pesticide chemical residue ad- ical residue and the commodities for dressed in the petition. If a Codex max- which a tolerance is sought and an- imum residue level has been estab- nounce the availability of a description lished for the pesticide chemical res- of the analytical methods available to idue and the petitioner does not pro- the Administrator for the detection pose that this level be adopted, a state- and measurement of the pesticide ment explaining the reasons for this chemical residue with respect to which departure from the Codex level. the petition is filed or shall set forth (15) Such other data and information the petitioner’s statement of why such as the Administrator requires by regu- a method is not needed. The notice lation to support the petition. shall explicitly reference the specific (16) Reasonable grounds in support of docket identification number in the the petition. public docket at http:// (c) The data specified under para- www.regulations.gov where the full text graphs (b)(1) through (b)(16) of this sec- of the summary required in paragraph tion should be on separate sheets or (b) of this section is located, and refer sets of sheets, suitably identified. If interested parties to this document for such data have already been submitted further information on the petition. with an earlier application, the present The full text of the summary may be petition may incorporate it by ref- omitted from the notice. erence to the earlier one. (g) The Administrator may request a (d) Except as noted in paragraph (e) sample of the pesticide chemical at any of this section, a petition shall not be time while a petition is under consider- accepted for filing if any of the data ation. The Administrator shall specify prescribed by FFDCA section 408(d) are in its request for a sample of the pes- lacking or are not set forth so as to be ticide chemical, a quantity which it readily understood. The availability to deems adequate to permit tests of ana- the public of information provided to, lytical methods used to determine resi- or otherwise obtained by, the Agency dues of the pesticide chemical and of under this part shall be governed by methods proposed by the petitioner for part 2 of this chapter. The Adminis- removing any residues of the chemical trator shall make the full text of the that exceed the tolerance proposed. summary referenced in paragraph (b)(1) (h) The Administrator shall deter- of this section available to the public mine, in accordance with the Act, in the public docket at http:// whether to issue an order that estab- www.regulations.gov no later than pub- lishes, modifies, or revokes a tolerance

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regulation (whether or not in accord issuance of a regulation establishing a with the action proposed by the peti- tolerance for a pesticide chemical or tioner), whether to publish a proposed exempting it from the necessity of a tolerance regulation and request public tolerance, or a regulation modifying or comment thereon under § 180.29, or revoking an existing tolerance or ex- whether to deny the petition. The Ad- emption. ministrator shall publish in the FED- (b) The Administrator shall provide a ERAL REGISTER such order or proposed period of not less than 60 days for per- regulation. After receiving comments sons to comment on the proposed regu- on any proposed regulation, the Ad- lation, except that a shorter period for ministrator may issue an order that es- comment may be provided if the Ad- tablishes, modifies, or revokes a toler- ministrator for good cause finds that it ance regulation. An order published would be in the public interest to do so under this section shall describe briefly and states the reasons for the finding how to submit objections and requests in the notice of proposed rulemaking. for a hearing under part 178 of this (c) After reviewing any timely com- chapter. A regulation issued under this ments received, the Administrator may section shall be effective on the date of by order establish, modify, or revoke a publication in the FEDERAL REGISTER tolerance regulation, which order and unless otherwise provided in the regu- regulation shall be published in the lation. FEDERAL REGISTER. An order published under this section shall state that per- [70 FR 33360, June 8, 2005, as amended at 73 sons may submit objections and re- FR 75600, Dec. 12, 2008] quests for a hearing in the manner de- § 180.8 Withdrawal of petitions with- scribed in part 178 of this chapter. out prejudice. (d) Any final regulation issued under this section shall be effective on the In some cases the Administrator will date of publication in the FEDERAL notify the petitioner that the petition, REGISTER unless otherwise provided in while technically complete, is inad- the regulation. equate to justify the establishment of a tolerance or the tolerance requested by [70 FR 33361, June 8, 2005] petitioner. This may be due to the fact that the data are not sufficiently clear § 180.30 Judicial review. or complete. In such cases, the peti- (a) Under FFDCA section 408(h), judi- tioner may withdraw the petition pend- cial review is available in the United ing its clarification or the obtaining of States Courts of Appeal as to the fol- additional data. This withdrawal may lowing actions: be without prejudice to a future filing. (1) Regulations establishing general A deposit for fees as specified in § 180.33 procedures and requirements under shall accompany the resubmission of FFDCA section 408(e)(1)(C). the petition. (2) Orders issued under FFDCA sec- tion 408(f)(1)(C) requiring the submis- [70 FR 33361, June 8, 2005] sion of data. (3) Orders issued under FFDCA sec- § 180.9 Substantive amendments to pe- titions. tion 408(g)(2)(C) ruling on objections to establishment, modification, or revoca- After a petition has been filed, the tion of a tolerance or exemption under petitioner may submit additional in- FFDCA section 408(d)(4), or any regula- formation or data in support thereof, tion that is the subject of such an but in such cases the petition will be order. The underlying action here is given a new filing date. Agency disposition of a petition seek- [70 FR 33361, June 8, 2005] ing the establishment, modification, or revocation of a tolerance or exemption. § 180.29 Establishment, modification, (4) Orders issued under FFDCA sec- and revocation of tolerance on ini- tion 408(g)(2)(C) ruling on objections to tiative of Administrator. the denial of a petition under FFDCA (a) Upon the Administrator’s own ini- section 408(d)(4). tiative, the Administrator may pro- (5) Orders issued under FFDCA sec- pose, under FFDCA section 408(e), the tion 408(g)(2)(C) ruling on objections to

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the establishment, modification, sus- eral , Fungicide, and pension, or revocation of a tolerance or Rodenticide Act shall be accompanied exemption under FFDCA section by such data as are available on sub- 408(e)(1)(A) or (e)(1)(B). The underlying jects outlined in § 180.7(b) and an ad- action here is the establishment, modi- vance deposit to cover fees as provided fication, suspension, or revocation of a in § 180.33. tolerance or exemption upon the initia- (c) To obtain a temporary tolerance, tive of EPA including EPA actions pur- a requestor must comply with the peti- suant to FFDCA sections tion procedures specified in FFDCA 408(b)(2)(B)(v), 408(b)(2)(E)(ii), section 408(d) and § 180.7 except as pro- 408(d)(4)(C)(ii), 408(l)(4), and 408(q)(1). vided in this section. (6) Orders issued under FFDCA sec- (d) A temporary tolerance or exemp- tion 408(g)(2)(C) ruling on objections to tion from a tolerance may be issued for the revocation or modification of a tol- a period designed to allow the orderly erance or exemption under FFDCA sec- marketing of the raw agricultural com- tion 408(f)(2) for noncompliance with modities produced while testing a pes- requirements for the submission of ticide chemical under an experimental data. permit issued under authority of the (7) Orders issued under FFDCA sec- Federal Insecticide, Fungicide, and tion 408(g)(2)(C) ruling on objections to Rodenticide Act if the Administrator rules issued under FFDCA sections concludes that the safety standard in 408(n)(3) and 408(d) or (e) regarding de- FFDCA section 408(b)(2) or (c), as appli- terminations pertaining to State au- cable, is met. Subject to the require- thority to establish regulatory limits ments of FFDCA section 408(e), a tem- on pesticide chemical residues. porary tolerance or exemption from a (8) Orders issued under FFDCA sec- tolerance may be revoked if the experi- tion 408(g)(2)(C) ruling on objections to mental permit is revoked, or may be orders issued under FFDCA section revoked at any time if it develops that 408(n)(5)(C) authorizing States to estab- the application for a temporary toler- lish regulatory limits not identical to ance contains a misstatement of a ma- certain tolerances or exemptions. terial fact or that new scientific data (b) Any issue as to which review is or or experience with the pesticide chem- was obtainable under paragraph (a) of ical indicates that it does not meet the this section shall not be the subject of safety standard in FFDCA section judicial review under any other provi- 408(b)(2) or (c), as applicable. sion of law. In part, this means that, (e) Conditions under which a tem- for the Agency actions subject to the porary tolerance is established shall in- objection procedure in FFDCA section clude: 408(g)(2), judicial review is not avail- (1) A limitation on the amount of the able unless an adversely affected party chemical to be used on the designated exhausts these objection procedures, crops permitted under the experi- and any petition procedures prelimi- mental permit. nary thereto. (2) A limitation for the use of the [70 FR 33362, June 8, 2005] chemical on the designated crops to bona fide experimental use by qualified § 180.31 Temporary tolerances. persons as indicated in the experi- (a) A temporary tolerance (or exemp- mental permit. tion from a tolerance) established (3) A requirement that the person or under the authority of FFDCA section firm which obtains the experimental 408(r) shall be deemed to be a tolerance permit for which the temporary toler- (or exemption from the requirement of ance is established will immediately a tolerance) for the purposes of FFDCA inform the Environmental Protection section 408(a)(1) or (a)(2) and for the Agency of any reports on findings from purposes of § 180.30. the experimental use that have a bear- (b) A request for a temporary toler- ing on safety. ance or a temporary exemption from a (4) A requirement that the person or tolerance by a person who has obtained firm which obtained the experimental or is seeking an experimental permit permit for which the temporary toler- for a pesticide chemical under the Fed- ance is established will keep records of

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production, distribution, and perform- § 180.33 Fees. ance for a period of 2 years and, on re- (a) Each petition for the establish- quest, at any reasonable time, make ment of a new tolerance or a tolerance these records available to any author- higher than already established, shall ized officer or employee of the Environ- be accompanied by a fee of $80,950, plus mental Protection Agency. $2,025 for each raw agricultural com- [70 FR 33362, June 8, 2005] modity more than nine on which the establishment of a tolerance is re- § 180.32 Procedure for modifying and quested, except as provided in para- revoking tolerances or exemptions graphs (b), (d), and (h) of this section. from tolerances. (b) Each petition for the establish- ment of a tolerance at a lower numer- (a) The Administrator on his/her own ical level or levels than a tolerance al- initiative may propose the issuance of ready established for the same pes- a regulation modifying or revoking a ticide chemical, or for the establish- tolerance for a pesticide chemical res- ment of a tolerance on additional raw idue on raw agricultural commodities agricultural commodities at the same or processed foods or modifying or re- numerical level as a tolerance already voking an exemption from tolerance established for the same pesticide for such residue. chemical, shall be accompanied by a (b) Any person may file with the Ad- fee of $18,500 plus $1,225 for each raw ministrator a petition proposing the agricultural commodity on which a tol- issuance of a regulation modifying or erance is requested. revoking a tolerance or exemption (c) Each petition for an exemption from a tolerance for a pesticide chem- from the requirement of a tolerance or ical residue. The petition shall furnish repeal of an exemption shall be accom- reasonable grounds for the action panied by a fee of $14,925. sought. Reasonable grounds shall in- (d) Each petition or request for a clude an explanation showing wherein temporary tolerance or a temporary the person has a substantial interest in exemption from the requirement of a such tolerance or exemption from tol- tolerance shall be accompanied by a fee erance and an assertion of facts (sup- of $32,325 except as provided in para- ported by data if available) showing graph (e) of this section. A petition or that new uses for the pesticide chem- request to renew or extend such tem- ical have been developed or old uses porary tolerance or temporary exemp- abandoned, that new data are available tion shall be accompanied by a fee of as to toxicity of the chemical, or that $4,600. experience with the application of the (e) A petition or request for a tem- tolerance or exemption from tolerance porary tolerance for a pesticide chem- may justify its modification or revoca- ical which has a tolerance for other tion. Evidence that a person has reg- uses at the same numerical level or a istered or has submitted an application higher numerical level shall be accom- for the registration of a pesticide under panied by a fee of $16,075, plus $1,225 for the Federal Insecticide, Fungicide, and each raw agricultural commodity on Rodenticide Act will be regarded as which the temporary tolerance is evidence that the person has a substan- sought. tial interest in a tolerance or exemp- (f) Each petition for revocation of a tion from the requirement of a toler- tolerance shall be accompanied by a fee ance for a pesticide chemical that con- of $10,125. Such fee is not required sists in whole or in part of the pes- when, in connection with the change ticide. New data should be furnished in sought under this paragraph, a petition the form specified in § 180.7(b) for sub- is filed for the establishment of new mitting petitions, as applicable. tolerances to take the place of those (c) The procedures for completing ac- sought to be revoked and a fee is paid tion on an Administrator initiated pro- as required by paragraph (a) of this sec- posal or a petition shall be those speci- tion. (g) If a petition or a request is not ac- fied in §§ 180.29 and 180.7, as applicable. cepted for processing because it is [70 FR 33362, June 8, 2005] technically incomplete, the fee, less

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$2,025 for handling and initial review, (m) All deposits and fees required by shall be returned. If a petition is with- the regulations in this part shall be drawn by the petitioner after initial paid by money order, bank draft, or processing, but before significant Agen- certified check drawn to the order of cy scientific review has begun, the fee, the Environmental Protection Agency. less $2,025 for handling and initial re- All deposits and fees shall be forwarded view, shall be returned. If an unaccept- to the Environmental Protection Agen- able or withdrawn petition is resub- cy, Headquarters Accounting Oper- mitted, it shall be accompanied by the ations Branch, Office of Pesticide Pro- fee that would be required if it were grams (Tolerance Fees), P.O. Box being submitted for the first time. 360277M, Pittsburgh, PA 15251. The pay- (h) Each petition for a crop group tol- ments should be specifically labeled erance, regardless of the number of raw ‘‘Tolerance Petition Fees’’ and should agricultural commodities involved, be accompanied only by a copy of the shall be accompanied by a fee equal to letter or petition requesting the toler- the fee required by the analogous cat- ance. The actual letter or petition, egory for a single tolerance that is not along with supporting data, shall be a crop group tolerance, i.e., paragraphs forwarded within 30 days of payment to (a) through (f) of this section, without the Office of Pesticide Programs’ Docu- a charge for each commodity where ment Processing Desk at the appro- that would otherwise apply. priate address as set forth in 40 CFR (i) Objections under section 408(d)(5) 150.17(a) or (b). A petition will not be of the Act shall be accompanied by a filing fee of $4,050. accepted for processing until the re- quired fees have been submitted. A pe- (j) The person who files a petition for judicial review of an order under sec- tition for which a waiver of fees has tion 408(h) of the Act shall pay the been requested will not be accepted for costs of preparing the record on which processing until the fee has been the order is based unless the person has waived or, if the waiver has been de- no financial interest in the petition for nied, the proper fee is submitted after judicial review. notice of denial. A request for waiver (k) No fee under this section will be or refund will not be accepted after sci- imposed on the Interregional Research entific review has begun on a petition. Project Number 4 (IR-4 Program). (n) This fee schedule will be changed (l) The Administrator may waive or annually by the same percentage as the refund part or all of any fee imposed by percent change in the Federal General this section if the Administrator deter- Schedule (GS) pay scale. In addition, mines in his or her sole discretion that processing costs and fees will periodi- such a waiver or refund will promote cally be reviewed and changes will be the public interest or that payment of made to the schedule as necessary. the fee would work an unreasonable When automatic adjustments are made hardship on the person on whom the based on the GS pay scale, the new fee fee is imposed. A request for waiver or schedule will be published in the FED- refund of a fee shall be submitted to ERAL REGISTER as a final rule to be- the Office of Pesticide Programs’ Docu- come effective 30 days or more after ment Processing Desk at the appro- publication, as specified in the rule. priate address as set forth in 40 CFR When changes are made based on peri- 150.17(a) or (b). A fee of $2,025 shall ac- odic reviews, the changes will be sub- company every request for a waiver or ject to public comment. refund, as specified in paragraph (m) of (o) No fee required by this section this section, except that the fee under shall be levied during the period begin- this paragraph shall not be imposed on ning on October 1, 2003, and ending Sep- any person who has no financial inter- tember 30, 2008. est in any action requested by such person under paragraphs (a) through (j) [68 FR 24371, May 7, 2003, as amended at 69 of this section. The fee for requesting a FR 12544, Mar. 17, 2004; 70 FR 33363, June 8, waiver or refund shall be refunded if 2005; 71 FR 35547, June 21, 2006] the request is granted.

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§ 180.34 Tests on the amount of res- (10) Beans, peas, (each in idue remaining. succulent form). (a) Data in a petition on the amount (11) Broccoli, brussels sprouts, cauli- of residue remaining in or on a raw ag- flower, kohlrabi. ricultural commodity should establish (12) Cantaloups, honeydew melons, the residue that may remain when the muskmelons, pumpkins, watermelons, pesticide chemical is applied according winter squash. to directions registered under the Fed- (13) Carrots, garden beets, sugar eral Insecticide, Fungicide, and beets, horseradish, parsnips, radishes, Rodenticide Act, or according to direc- rutabagas, salsify roots, turnips. tions contained in an application for (14) Celery, fennel. registration. These data should estab- (15) Cucumbers, summer squash. lish the residues that may remain (16) Lettuce, endive (escarole), Chi- under conditions most likely to result nese cabbage, salsify tops. in high residues on the commodity. (17) Onions, garlic, , (b) The petition should establish the (green, or in dry bulb form). reliability of the residue data reported (18) Potatoes, Jerusalem-artichokes, in it. Sufficient information should be sweetpotatoes, yams. submitted about the analytical method (19) Spinach, beet tops, collards, dan- to permit competent analysts to apply delion, kale, mustard greens, parsley, it successfully. Swiss chard, turnip tops, watercress. (c) If the pesticide chemical is ab- (20) Tomatoes, eggplants, peppers, pi- sorbed into a living plant or animal mentos. when applied (is systemic), residue (21) Pecans, almonds, brazil nuts, data may be needed on each plant or bush nuts, butternuts, chestnuts, fil- animal on which a tolerance or exemp- berts, hazelnuts, hickory nuts, wal- tion is requested. nuts. (d) If the pesticide chemical is not (22) Field corn, popcorn, sweet corn absorbed into the living plant or ani- (each in grain form). mal when applied (is not systemic), it (23) Milo, sorghum (each in grain may be possible to make a reliable es- form). timate of the residues to be expected (24) Wheat, barley, oats, rice, rye on each commodity in a group of re- (each in grain form). lated commodities on the basis of less (25) Alfalfa, Bermuda grass, blue- data than would be required for each grass, brome grass, clovers, cowpea commodity in the group, considered hay, fescue, lespedeza, lupines, orchard separately. grass, peanut hay, peavine hay, rye (e) Each of the following groups of grass, hay, sudan grass, tim- crops lists raw agricultural commod- othy, and vetch. ities that are considered to be related (26) Corn forage, sorghum forage. for the purpose of paragraph (d) of this (27) Sugarcane, cane sorghum. section. Commodities not listed in this [36 FR 22540, Nov. 25, 1971, as amended at 39 paragraph are not considered to be re- FR 28286, Aug. 6, 1974; 39 FR 28977, Aug. 13, lated for the purpose of paragraph (d) 1974; 40 FR 6972, Feb. 18, 1975; 45 FR 82928, of this section. Dec. 17, 1980; 48 FR 29860, June 29, 1983; 60 FR (1) Apples, crabapples, pears, quinces. 26635, May 17, 1995; 73 FR 75600, Dec. 12, 2008] (2) Avocados, papayas. (3) Blackberries, boysenberries, § 180.35 Tests for potentiation. dewberries, loganberries, raspberries. Experiments have shown that certain (4) Blueberries, currants, goose- cholinesterase-inhibiting pesticides , huckleberries. when fed together to test animals are (5) Cherries, plums, prunes. more toxic than the sum of their indi- (6) Oranges, citrus citron, grapefruit, vidual when fed separately. kumquats, lemons, limes, tangelos, One substance potentiates the toxicity tangerines. of the other. Important toxicological (7) Mangoes, persimmons. interactions also have been observed (8) Peaches, apricots, nectarines. between pesticides and other sub- (9) Beans, peas, soybeans (each in dry stances. Wherever there is reason to form). believe that a pesticide chemical for

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which a tolerance is proposed may must be similar before a group toler- interact with other pesticide chemicals ance is established. The pattern of use or other substances to which man is ex- consists of the amount of pesticide ap- posed, it may be necessary to require plied, the number of times applied, the special experimental data regarding timing of the first application, the in- potentiation capacities to evaluate the terval between applications, and the safety of the proposed tolerance. This interval between the last application necessarily will be determined on a and harvest. The pattern of use will case-by-case basis. also include the type of application; for example, soil or foliar application, or § 180.40 Tolerances for crop groups. application by ground or aerial equip- (a) Group or subgroup tolerances may ment. be established as a result of: (f) When the crop grouping contains (1) A petition from a person who has commodities or byproducts that are submitted an application for the reg- utilized for animal feed, any needed istration of a pesticide under the Fed- tolerance or exemption from a toler- eral Insecticide, Fungicide, and ance for the pesticide in meat, milk, Rodenticide Act. (2) On the initiative of the Adminis- poultry and/or eggs must be established trator. before a tolerance will be granted for (3) A petition by an interested per- the group as a whole. The representa- son. tive crops include all crops in the (b) The tables in § 180.41 are to be group that could be processed such used in conjunction with this section that residues may concentrate in proc- for the establishment of crop group tol- essed food and/or feed. Processing data erances. Each table in § 180.41 lists a will be required prior to establishment group of raw agricultural commodities of a group tolerance. Tolerances will that are considered to be related for not be granted on a group basis as to the purposes of this section. Refer also processed foods prepared from crops to § 180.1(g) for a listing of commodities covered by the group tolerance. for which established tolerances may (g) If maximum residues (tolerances) be applied to certain other related and for the representative crops vary by similar commodities. more than a factor of 5 from the max- (c) When there is an established or imum value observed for any crop in proposed tolerance for all of the rep- the group, a group or subgroup toler- resentative commodities for a specific ance will ordinarily not be established. group or subgroup of related commod- In this case individual crop tolerances, ities, a tolerance may be established rather than group tolerances, will nor- for all commodities in the associated mally be established. group or subgroup. Tolerances may be (h) Alternatively, a commodity with established for a crop group or, alter- a residue level significantly higher or natively, tolerances may be established lower than the other commodities in a for one or more of the subgroups of a group may be excluded from the group crop group. (d) The representative crops are tolerance (e.g., cereal grains, except given as an indication of the minimum corn). In this case an individual toler- residue chemistry data base acceptable ance at the appropriate level for the to the Agency for the purposes of es- unique commodity would be estab- tablishing a group tolerance. The lished, if necessary. The alternative ap- Agency may, at its discretion, allow proach of excluding a commodity with group tolerances when data on suitable a significantly higher or lower residue substitutes for the representative crops level will not be used to establish a tol- are available (e.g., limes instead of erance for a commodity subgroup. Most lemons). subgroups have only two representa- (e) Since a group tolerance reflects tive commodities; to exclude one such maximum residues likely to occur on commodity and its related residue data all individual crops within a group, the would likely provide insufficient res- proposed or registered patterns of use idue information to support the re- for all crops in the group or subgroup mainder of the subgroup. Residue data

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from crops additional to those rep- to register the pesticide under a com- resentative crops in a grouping may be panion law, the Federal Insecticide, required for systemic pesticides. Fungicide, and Rodenticide Act. The (i) The commodities included in the Registration Division of the Office of groups will be updated periodically ei- Pesticide Programs should be con- ther at the initiative of the Agency or tacted concerning procedures for reg- at the request of an interested party. istration of new uses of a pesticide. Persons interested in updating this sec- tion should contact the Registration [60 FR 26635, May 17, 1995, as amended at 70 Division of the Office of Pesticide Pro- FR 33363, June 8, 2005; 72 FR 69155, Dec. 7, grams. 2007; 75 FR 56014, Sept. 15, 2010] (j) When EPA amends a crop group in § 180.41 Crop group tables. a manner that expands or contracts the commodities that are covered by the (a) The tables in this section are to group, EPA will initially retain the be used in conjunction with § 180.40 to pre-existing as well as the revised crop establish crop group tolerances. group in the CFR. The revised crop (b) Commodities not listed are not group will have the same number as considered as included in the groups for the pre-existing crop group; however, the purposes of this paragraph, and in- the revised crop group number will be dividual tolerances must be estab- followed by a hyphen and the final two lished. Miscellaneous commodities in- digits of the year in which it was estab- tentionally not included in any group lished (e.g., if Crop Group 1 is amended include asparagus, avocado, banana, in 2007, the revised group will be des- fig, globe artichoke, hops, mango, pa- ignated as Crop Group 1-07). If the pre- paya, pawpaw, peanut, persimmon, existing crop group had crop sub- pineapple, water chestnut, and water- groups, these subgroups will be num- cress. bered in a similar fashion in the re- (c) Each group is identified by a vised crop group. The name of the re- group name and consists of a list of vised crop group will not be changed representative commodities followed from the pre-existing crop group unless by a list of all commodity members for the revision so changes the composi- the group. If the group includes sub- tion of the crop group that the pre-ex- groups, each subgroup lists the sub- isting name is no longer accurate. Once group name, the representative com- a revised crop group is established, modity or commodities, and the mem- EPA will no longer establish tolerances under the pre-existing crop group. At ber commodities for the subgroup. Sub- appropriate times, EPA will amend tol- groups, which are a subset of their as- erances for crop groups that have been sociated crop group, are established for superseded by revised crop groups to some but not all crops groups. conform the pre-existing crop group to (1) Crop Group 1: Root and Tuber the revised crop group. Once all of the Vegetables Group. tolerances for the pre-existing crop (i) Representative commodities. Carrot, group have been updated, the pre-exist- potato, radish, and sugar beet. ing crop group will be removed from (ii) Table. The following table 1 lists the CFR. all the commodities included in Crop (k) Establishment of a tolerance does Group 1 and identifies the related crop not substitute for the additional need subgroups.

TABLE 1—CROP GROUP 1: ROOT AND TUBER VEGETABLES

Related crop Commodities subgroups

Arracacha (Arracacia xanthorrhiza) ...... 1C, 1D Arrowroot (Maranta arundinacea) ...... 1C, 1D Artichoke, Chinese (Stachys affinis) ...... 1C, 1D Artichoke, Jerusalem (Helianthus tuberosus) ...... 1C, 1D Beet, garden (Beta vulgaris) ...... 1A, 1B Beet, sugar (Beta vulgaris) ...... 1A Burdock, edible (Arctium lappa) ...... 1A, 1B Canna, edible (Queensland arrowroot) (Canna indica) ...... 1C, 1D Carrot (Daucus carota) ...... 1A, 1B

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TABLE 1—CROP GROUP 1: ROOT AND TUBER VEGETABLES—Continued

Related crop Commodities subgroups

Cassava, bitter and sweet (Manihot esculenta) ...... 1C, 1D Celeriac (celery root) (Apium graveolens var. rapaceum) ...... 1A, 1B Chayote (root) (Sechium edule) ...... 1C, 1D Chervil, turnip-rooted (Chaerophyllum bulbosum)...... 1A, 1B Chicory (Cichorium intybus) ...... 1A, 1B Chufa (Cyperus esculentus) ...... 1C, 1D Dasheen (taro) (Colocasia esculenta) ...... 1C, 1D Ginger (Zingiber officinale) ...... 1C, 1D Ginseng (Panax quinquefolius) ...... 1A, 1B Horseradish (Armoracia rusticana) ...... 1A, 1B Leren (Calathea allouia) ...... 1C, 1D Parsley, turnip-rooted (Petroselinum crispum var. tuberosum) ...... 1A, 1B Parsnip (Pastinaca sativa) ...... 1A, 1B Potato (Solanum tuberosum) ...... 1C Radish (Raphanus sativus) ...... 1A, 1B Radish, oriental (daikon) (Raphanus sativus subvar. longipinnatus) ...... 1A, 1B Rutabaga (Brassica campestris var. napobrassica) ...... 1A, 1B Salsify (oyster plant) (Tragopogon porrifolius)...... 1A, 1B Salsify, black (Scorzonera hispanica) ...... 1A, 1B Salsify, Spanish (Scolymus hispanicus) ...... 1A, 1B Skirret (Sium sisarum) ...... 1A, 1B Sweet potato (Ipomoea batatas) ...... 1C, 1D Tanier (cocoyam) (Xanthosoma sagittifolium) ...... 1C, 1D Turmeric (Curcuma longa) ...... 1C, 1D Turnip (Brassica rapa var. rapa) ...... 1A, 1B Yam bean (jicama, manoic pea) (Pachyrhizus spp.) ...... 1C, 1D Yam, true (Dioscorea spp.) ...... 1C, 1D

(iii) Table. The following table 2 iden- commodity(ies) for each subgroup, and tifies the crop subgroups for Crop lists all the commodities included in Group 1, specifies the representative each subgroup.

TABLE 2—CROP GROUP 1 SUBGROUP LISTING

Representative commodities Commodities

Crop Subgroup 1A. Root vegetables subgroup. Carrot, radish, and sugar beet...... Beet, garden; beet, sugar; burdock, edible; carrot; celeriac; chervil, turnip-root- ed; chicory; ginseng; horseradish; parsley, turnip-rooted; parsnip; radish; rad- ish, oriental; rutabaga; salsify; salsify, black; salsify, Spanish; skirret; turnip. Crop Subgroup 1B. Root vegetables (except sugar beet) subgroup. Carrot and radish...... Beet, garden; burdock, edible; carrot; celeriac; chervil, turnip-rooted; chicory; ginseng; horseradish; parsley, turnip-rooted; parsnip; radish; radish, oriental; rutabaga; salsify; salsify, black; salsify, Spanish; skirret; turnip. Crop Subgroup 1C. Tuberous and corm vegetables subgroup. Potato...... Arracacha; arrowroot; artichoke, Chinese; artichoke, Jerusalem; canna, edible; cassava, bitter and sweet; chayote (root); chufa; dasheen; ginger; leren; po- tato; sweet potato; tanier; turmeric; yam bean; yam, true. Crop Subgroup 1D. Tuberous and corm vegetables (except potato) subgroup. Sweet potato...... Arracacha; arrowroot; artichoke, Chinese; artichoke, Jerusalem; canna, edible; cassava, bitter and sweet; chayote (root); chufa; dasheen; ginger; leren; sweet potato; tanier; turmeric; yam bean; yam, true.

(2) Crop Group 2. Leaves of Root and (ii) Commodities. The following is a Tuber Vegetables (Human Food or Ani- list of all the commodities included in mal Feed) Group (Human Food or Ani- Crop Group 2: mal Feed) Group. (i) Representative commodities. Turnip and garden beet or sugar beet.

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CROP GROUP 2: LEAVES OF ROOT AND TUBER (3) Crop Group 3. Bulb Vegetables VEGETABLES (HUMAN FOOD OR ANIMAL ( spp.) Group. FEED) GROUP—COMMODITIES (i) Representative commodities. Onion, Beet, garden (Beta vulgaris) green; and onion, dry bulb. Beet, sugar (Beta vulgaris) (ii) Commodities. The following is a Burdock, edible (Arctium lappa) list of all the commodities in Crop Carrot (Daucus carota) Group 3. Cassava, bitter and sweet (Manihot esculenta) Celeriac (celery root) (Apium graveolens var. CROP GROUP 3: BULB VEGETABLE (Allium SPP.) rapaceum) GROUP—COMMODITIES Chervil, turnip-rooted (Chaerophyllum Garlic, bulb (Allium sativum) bulbosum) Garlic, great headed, (elephant) ( var. Chicory (Cichorium intybus) ampeloprasum) Dasheen (taro) (Colocasia esculenta) Leek (Allium ampeloprasum, A. porrum, A. tricoccum) Onion, dry bulb and green (Allium cepa, A. fistulosum) Parsnip (Pastinaca sativa) Onion, Welsh, () Radish (Raphanus sativus) Shallot (Allium cepa var. cepa) Radish, oriental (daikon) (Raphanus sativus subvar. longipinnatus) (4) Crop Group 3-07. Bulb Vegetable Rutabaga (Brassica campestris var. Group. napobrassica) (i) Representative Commodities. Onion, Salsify, black (Scorzonera hispanica) bulb and onion, green. Sweet potato (Ipomoea batatas) (ii) Table. The following Table 1 lists Tanier (cocoyam) (Xanthosoma sagittifolium) all the commodities listed in Crop Turnip (Brassica rapa var. rapa) Group 3-07 and identifies the related Yam, true (Dioscorea spp.) crop subgroups.

TABLE 1—CROP GROUP 3-07: BULB VEGETABLE GROUP

Commodities Related crop subgroups

Chive, fresh leaves (Allium schoenoprasum L.) ...... 3-07B Chive, Chinese, fresh leaves ( Rottler ex Spreng) ...... 3-07B Daylily, bulb (Hemerocallis fulva (L.) L. var. fulva) ...... 3-07A Elegans hosta (Hosta Sieboldiana (Hook.) Engl) ...... 3-07B Fritillaria, bulb (Fritillaria L. fritillary) ...... 3-07A Fritillaria, leaves (Fritillaria L. fritillary) ...... 3-07B Garlic, bulb (Allium sativum L. var. sativum) (A. sativum Common Garlic Group) ...... 3-07A Garlic, great headed, bulb (Allium ampeloprasum L. var. ampeloprasum) (A. ampeloprasum Great Headed Garlic Group) ...... 3-07A Garlic, Serpent, bulb (Allium sativum var. ophioscorodon or A. sativum Ophioscorodon Group) ...... 3-07A Kurrat (Allium kurrat Schweinf. Ex. K. Krause or A. ampeloprasum Kurrat Group) ...... 3-07B Lady’s leek ( Roth) ...... 3-07B Leek Allium porrum L. (syn: A. ampeloprasum L. var. porrum (L.) J. Gay) (A.ampeloprasum Leek Group) ...... 3-07B Leek, wild ( Aiton) ...... 3-07B Lily, bulb (Lilium spp. (Lilium Leichtlinii var. maximowiczii, Lilium lancifolium)) ...... 3-07A Onion, Beltsville bunching (Allium x proliferum (Moench) Schrad.) (syn: Allium fistulosum L. x A. cepa L.) ...... 3-07B Onion, bulb (Allium cepa L. var. cepa) (A. cepa Common Onion Group) ...... 3-07A Onion, Chinese, bulb ( G. Don.) (syn: A. bakeri Regel) ...... 3-07A Onion, fresh (Allium fistulosum L. var. caespitosum Makino) ...... 3-07B Onion, green (Allium cepa L. var. cepa) (A. cepa Common Onion Group) ...... 3-07B Onion, macrostem (Allium macrostemom Bunge) ...... 3-07B Onion, pearl (Allium porrum var. sectivum or A. ampeloprasum Pearl Onion Group) ...... 3-07A Onion, potato, bulb (Allium cepa L. var. aggregatum G. Don.) (A. cepa Aggregatum Group) ...... 3-07A Onion, tree, tops (Allium x proliferum (Moench) Schrad. ex Willd.) (syn: A. cepa var. proliferum (Moench) Regel; A. cepa L. var. bulbiferum L.H. Bailey; A. cepa L. var. viviparum (Metz.) Alef.) ...... 3-07B Onion, Welsh, tops (Allium fistulosum L.) ...... 3-07B Shallot, bulb (Allium cepa var. aggregatum G. Don.) ...... 3-07A Shallot, fresh leaves (Allium cepa var. aggregatum G. Don.) ...... 3-07B Cultivars, varieties, and/or hybrids of these......

(iii) Table. The following Table 2 commodities for each subgroup and identifies the crop subgroups for Crop lists all the commodities included in Group 3-07, specifies the representative each subgroup.

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TABLE 2—CROP GROUP 3-07: SUBGROUP LISTING

Representative commodities Commodities

Crop subgroup 3-07A. Onion, bulb, sub- Daylily, bulb; fritillaria, bulb; garlic, bulb; garlic, great-headed, bulb; garlic, serpent, group. bulb; lily, bulb; onion, bulb; onion, Chinese, bulb; onion, pearl; onion, potato, Onion, bulb...... bulb; shallot, bulb; cultivars, varieties, and/or hybrids of these. Crop subgroup 3-07B. Onion, green, sub- Chive, fresh leaves; chive, Chinese, fresh leaves; elegans hosta; fritillaria, leaves; group. kurrat; lady’s leek; leek; leek, wild; Onion, Beltsville bunching; onion, fresh; Onion, green...... onion, green; onion, macrostem; onion, tree, tops; onion, Welsh, tops; shallot, fresh leaves; cultivars, varieties, and/or hybrids of these.

(5) Crop Group 4. Leafy Vegetables (ii) Table. The following table 1 lists (Except Brassica Vegetables) Group. all the commodities included in Crop (i) Representative commodities. Celery, Group 4 and identifies the related crop head lettuce, leaf lettuce, and spinach subgroups. (Spinacia oleracea).

TABLE 1—CROP GROUP 4: LEAFY VEGETABLES (EXCEPT BRASSICA VEGETABLES) GROUP

Related crop Commodities subgroups

Amaranth (leafy amaranth, Chinese spinach, tampala) (Amaranthus spp.) ...... 4A Arugula (Roquette) (Eruca sativa) ...... 4A Cardoon (Cynara cardunculus) ...... 4B Celery (Apium graveolens var. dulce) ...... 4B Celery, Chinese (Apium graveolens var. secalinum) ...... 4B Celtuce (Lactuca sativa var. angustana) ...... 4B Chervil (Anthriscus cerefolium) ...... 4A Chrysanthemum, edible-leaved (Chrysanthemum coronarium var. coronarium) ...... 4A Chrysanthemum, garland (Chrysanthemum coronarium var. spatiosum) ...... 4A Corn salad (Valerianella locusta) ...... 4A Cress, garden (Lepidium sativum) ...... 4A Cress, upland (yellow rocket, winter cress) (Barbarea vulgaris) ...... 4A Dandelion (Taraxacum officinale) ...... 4A Dock (sorrel) (Rumex spp.) ...... 4A Endive (escarole) (Cichorium endivia) ...... 4A Fennel, Florence (finochio) (Foeniculum vulgare Azoricum Group) ...... 4B Lettuce, head and leaf (Lactuca sativa) ...... 4A Orach (Atriplex hortensis) ...... 4A Parsley (Petroselinum crispum) ...... 4A Purslane, garden (Portulaca oleracea) ...... 4A Purslane, winter (Montia perfoliata) ...... 4A Radicchio (red chicory) (Cichorium intybus) ...... 4A Rhubarb (Rheum rhabarbarum) ...... 4B Spinach (Spinacia oleracea) ...... 4A Spinach, New Zealand (Tetragonia tetragonioides, T. expansa) ...... 4A Spinach, vine (Malabar spinach, Indian spinach) (Basella alba) ...... 4A Swiss chard (Beta vulgaris var. cicla) ...... 4B

(iii) Table. The following table 2 iden- commodities for each subgroup, and tifies the crop subgroups for Crop lists all the commodities included in Group 4, specifies the representative each subgroup.

TABLE 2—CROP GROUP 4 SUBGROUP LISTING

Representative commodities Commodities

Crop Subgroup 4A. Leafy greens subgroup. Head lettuce and leaf lettuce, and spinach Amaranth; arugula; chervil; chrysanthemum, edible-leaved; chrysanthemum, (Spinacia oleracea). garland; corn salad; cress, garden; cress, upland; dandelion; dock; endive; lettuce; orach; parsley; purslane, garden; purslane, winter; radicchio (red chicory); spinach; spinach, New Zealand; spinach, vine. Crop Subgroup 4B. Leaf petioles subgroup. Celery...... Cardoon; celery; celery, Chinese; celtuce; fennel, Florence; rhubarb; Swiss chard.

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(6) Crop Group 5. Brassica (Cole) Leafy (ii) Table. The following table 1 lists Vegetables Group. all the commodities included in Crop (i) Representative commodities. Broc- Group 5 and identifies the related crop coli or cauliflower; cabbage; and mus- subgroups. tard greens.

TABLE 1—CROP GROUP 5: Brassica (COLE) LEAFY VEGETABLES

Related crop Commodities subgroups

Broccoli (Brassica oleracea var. botrytis) ...... 5A Broccoli, Chinese (gai lon) (Brassica alboglabra) ...... 5A Broccoli raab (rapini) (Brassica campestris) ...... 5B Brussels sprouts (Brassica oleracea var. gemmifera) ...... 5A Cabbage (Brassica oleracea) ...... 5A Cabbage, Chinese (bok choy) (Brassica chinensis) ...... 5B Cabbage, Chinese (napa) (Brassica pekinensis) ...... 5A Cabbage, Chinese mustard (gai choy) (Brassica campestris) ...... 5A Cauliflower (Brassica oleracea var. botrytis) ...... 5A Cavalo broccolo (Brassica oleracea var. botrytis) ...... 5A Collards (Brassica oleracea var. acephala) ...... 5B Kale (Brassica oleracea var. acephala) ...... 5B Kohlrabi (Brassica oleracea var. gongylodes) ...... 5A Mizuna (Brassica rapa Japonica Group) ...... 5B Mustard greens (Brassica juncea) ...... 5B Mustard spinach (Brassica rapa Perviridis Group) ...... 5B Rape greens (Brassica napus) ...... 5B

(iii) Table. The following table 2 iden- commodity(ies) for each subgroup, and tifies the crop subgroups for Crop lists all the commodities included in Group 5, specifies the representative each subgroup.

TABLE 2—CROP GROUP 5 SUBGROUP LISTING

Representative commodities Commodities

Crop Subgroup 5A. Head and stem Brassica subgroup Broccoli or cauliflower; and cabbage ...... Broccoli; broccoli, Chinese; brussels sprouts; cabbage; cabbage, Chinese (napa); cabbage, Chinese mustard; cauliflower; cavalo broccolo; kohlrabi Crop Subgroup 5B. Leafy Brassica greens subgroup. Mustard greens ...... Broccoli raab; cabbage, Chinese (bok choy); collards; kale; mizuna; mustard greens; mustard spinach; rape greens

(7) Crop Group 6. Legume Vegetables one succulent cultivar and one dried (Succulent or Dried) Group. cultivar); and soybean. (i) Representative commodities. Bean (ii) Table. The following table 1 lists (Phaseolus spp.; one succulent cultivar all the commodities included in Crop and one dried cultivar); pea (Pisum spp.; Group 6 and identifies the related crop subgroups.

TABLE 1—CROP GROUP 6: LEGUME VEGETABLES (SUCCULENT OR DRIED)

Related crop Commodities subgroups

Bean (Lupinus spp.) (includes grain lupin, sweet lupin, white lupin, and white sweet lupin) ...... 6C Bean (Phaseolus spp.) (includes field bean, kidney bean, lima bean, navy bean, pinto bean, runner bean, snap bean, tepary bean, wax bean) ...... 6A, 6B, 6C Bean (Vigna spp.) (includes adzuki bean, asparagus bean, blackeyed pea, catjang, Chinese longbean, cowpea, Crowder pea, moth bean, mung bean, rice bean, southern pea, urd bean, yardlong bean) ...... 6A, 6B, 6C Broad bean (fava bean) (Vicia faba) ...... 6B, 6C Chickpea (garbanzo bean) (Cicer arietinum) ...... 6C Guar (Cyamopsis tetragonoloba) ...... 6C Jackbean (Canavalia ensiformis) ...... 6A

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TABLE 1—CROP GROUP 6: LEGUME VEGETABLES (SUCCULENT OR DRIED)—Continued

Related crop Commodities subgroups

Lablab bean (hyacinth bean) (Lablab purpureus) ...... 6C Lentil (Lens esculenta) ...... 6C Pea (Pisum spp.) (includes dwarf pea, edible-pod pea, En glish pea, field pea, garden pea, green pea, snow pea, sugar snap pea) ...... 6A, 6B, 6C Pigeon pea (Cajanus cajan) ...... 6A, 6B, 6C Soybean (Glycine max) ...... N/A Soybean (immature seed) (Glycine max) ...... 6A Sword bean (Canavalia gladiata) ...... 6A

(iii) Table. The following table 2 iden- commodities for each subgroup, and tifies the crop subgroups for Crop lists all the commodities included in Group 6, specifies the representative each subgroup.

TABLE 2—CROP GROUP 6 SUBGROUP LISTING

Representative commodities Commodities

Crop Subgroup 6A. Edible-podded legume vegetables subgroup. Any one succulent cultivar of edible-podded Bean (Phaseolus spp.) (includes runner bean, snap bean, wax bean); bean bean (Phaseolus spp.) and any one suc- (Vigna spp.) (includes asparagus bean, Chinese longbean, moth bean, culent cultivar of edible-podded pea (Pisum yardlong bean); jackbean; pea (Pisum spp.) (includes dwarf pea, edible-pod spp.).. pea, snow pea, sugar snap pea); pigeon pea; soybean (immature seed); sword bean. Crop Subgroup 6B. Succulent shelled pea and bean subgroup. Any succulent shelled cultivar of bean Bean (Phaseolus spp.) (includes lima bean (green)); broad bean (succulent); (Phaseolus spp.) and garden pea (Pisum bean (Vigna spp.) (includes blackeyed pea, cowpea, southern pea); pea spp.).. (Pisum spp.) (includes English pea, garden pea, green pea); pigeon pea. Crop Subgroup 6C. Dried shelled pea and bean (except soybean) subgroup Any one dried cultivar of bean (Phaseolus Dried cultivars of bean (Lupinus spp.) (includes grain lupin, sweet lupin, white spp.); and any one dried cultivar of pea lupin, and white sweet lupin); (Phaseolus spp.) (includes field bean, kidney (Pisum spp.). bean, lima bean (dry), navy bean, pinto bean; tepary bean; bean (Vigna spp.) (includes adzuki bean, blackeyed pea, catjang, cowpea, Crowder pea, moth bean, mung bean, rice bean, southern pea, urd bean); broad bean (dry); chickpea; guar; lablab bean; lentil; pea (Pisum spp.) (includes field pea); pigeon pea.

(8) Crop Group 7. Foliage of Legume (ii) Table. The following table 1 lists Vegetables Group. the commodities included in Crop (i) Representative commodities. Any Group 7. cultivar of bean (Phaseolus spp.), field pea (Pisum spp.), and soybean.

TABLE 1—CROP GROUP 7: FOLIAGE OF LEGUME VEGETABLES GROUP

Representative commodities Commodities

Any cultivar of bean (Phaseolus spp.) and field Plant parts of any legume vegetable included in the legume vegetables that will pea (Pisum spp.), and soybean (Glycine be used as animal feed. max).

(iii) Table. The following table 2 iden- modities for the subgroup, and lists all tifies the crop subgroup for Crop Group the commodities included in the sub- 7 and specifies the representative com- group.

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TABLE 2—CROP GROUP 7 SUBGROUP LISTING

Representative commodities Commodities

Crop Subgroup 7A. Foliage of legume vegetables (except soybeans) subgroup Any cultivar of bean (Phaseolus spp.), and Plant parts of any legume vegetable (except soybeans) included in the legume field pea (Pisum spp.). vegetables group that will be used as animal feed.

(9) Crop Group 8. Fruiting Vegetables Pepper (Capsicum spp.) (includes bell pepper, Group. chili pepper, cooking pepper, pimento, (i) Representative commodities. To- sweet pepper) Tomatillo (Physalis ixocarpa) mato, bell pepper, and one cultivar of Tomato (Lycopersicon esculentum) non-bell pepper. (ii) Commodities. The following is a (10) Crop Group 8–10. Fruiting Vege- list of all the commodities included in table Group. Crop Group 8: (i) Representative commodities. To- mato, standard size, and one cultivar of CROP GROUP 8: FRUITING VEGETABLES small tomato; bell pepper and one (EXCEPT CUCURBITS)—COMMODITIES cultivar of small nonbell pepper. Eggplant (Solanum melongena) (ii) Commodities. The following is a Groundcherry (Physalis spp.) list of all commodities included in the Pepino (Solanum muricatum) Crop group 8–10.

TABLE 1—CROP GROUP 8–10: FRUITING VEGETABLE GROUP

Related crop sub- Commodities groups

African eggplant, Solanum macrocarpon L ...... 8–10B, 8–10C Bush tomato, Solanum centrale J.M. Black ...... 8–10A Cocona, Solanum sessiliflorum Dunal ...... 8–10A Currant tomato, Lycopersicon pimpinellifolium L ...... 8–10A Eggplant, Solanum melongena L ...... 8–10B, 8–10C Garden huckleberry, Solanum scabrum Mill ...... 8–10A Goji berry, Lycium barbarum L ...... 8–10A Groundcherry, Physalis alkekengi L., P. grisea (Waterf.) M. Martinez, P. peruviana L., P. pubescens L .. 8–10A Martynia, Proboscidea louisianica (Mill.) Thell ...... 8–10B, 8–10C Naranjilla, Solanum quitoense Lam ...... 8–10A Okra, Abelmoschus esculentus (L.) Moench ...... 8–10B, 8–10C Pea eggplant, Solanum torvum Sw...... 8–10B, 8–10C Pepino, Solanum muricatum Aiton ...... 8–10B, 8–10C Pepper, bell, Capsicum annuum L. var. annuum, Capsicum spp ...... 8–10B Pepper, nonbell, Capsicum chinese Jacq., C. annuum L. var. annuum, C. frutescens L., C. baccatum L., 8–10B, 8–10C C. pubescens Ruiz & Pav., Capsicum spp. Roselle, Hibiscus sabdariffa L ...... 8–10B, 8–10C Scarlet eggplant, Solanum aethiopicum L ...... 8–10B, 8–10C Sunberry, Solanum retroflexum Dunal ...... 8–10A Tomatillo, Physalis philadelphica Lam ...... 8–10A Tomato, Solanum lycopersicum L., Solanum lycopersicum L. var. lycopersicum ...... 8–10A Tree tomato, Solanum betaceum Cav ...... 8–10A Cultivars, varieties and/or hybrids of these ......

(iii) Table. The following Table 2 commodities for each subgroup and identifies the crop subgroups for Crop lists all the commodities included in Group 8–10, specifies the representative each subgroup.

TABLE 2—CROP GROUP 8–10. SUBGROUP LISTING

Representative commodities Commodities

Crop subgroup 8–10A. Tomato subgroup Tomato, standard size, and one cultivar of small tomato ...... Bush tomato; cocona; currant tomato; garden huckleberry; goji berry; groundcherry; naranjilla; sunberry; tomatillo; tomato; tree tomato; cultivars, varieties, and/or hybrids of these.

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TABLE 2—CROP GROUP 8–10. SUBGROUP LISTING—Continued

Representative commodities Commodities

Crop subgroup 8–10B. Pepper/Eggplant subgroup Bell pepper and one cultivar of small nonbell pepper ...... African eggplant; bell pepper; eggplant; Martynia; nonbell pep- per; okra; pea eggplant; pepino; roselle; scarlet eggplant; cultivars, varieties, and/or hybrids of these. Crop subgroup 8–10C. Nonbell pepper/Eggplant subgroup One cultivar of small nonbell pepper or one cultivar of small African eggplant; eggplant; martynia; nonbell pepper; okra; pea eggplant. eggplant; pepino; roselle; scarlet eggplant; cultivars, vari- eties, and/or hybrids of these.

(11) Crop Group 9. Cucurbit Vegeta- (ii) Table. The following table 1 lists bles Group. all the commodities included in Crop (i) Representative commodities. Cucum- Group 9 and identifies the related sub- ber, muskmelon, and summer squash. groups.

TABLE 1—CROP GROUP 9: CUCURBIT VEGETABLES

Related crop Commodities subgroups

Chayote (fruit) (Sechium edule) ...... 9B Chinese waxgourd (Chinese preserving melon) (Benincasa hispida) ...... 9B Citron melon (Citrullus lanatus var. citroides) ...... 9A Cucumber (Cucumis sativus) ...... 9B Gherkin (Cucumis anguria) ...... 9B Gourd, edible (Lagenaria spp.) (includes hyotan, cucuzza); (Luffa acutangula, L. cylindrica) (includes hechima, Chinese okra) ...... 9B Momordica spp. (includes balsam apple, balsam pear, bitter melon, Chinese cucumber) ...... 9B Muskmelon (hybrids and/or cultivars of Cucumis melo) (includes true cantaloupe, cantaloupe, casaba, cren- shaw melon, golden pershaw melon, honeydew melon, honey balls, mango melon, Persian melon, pine- apple melon, Santa Claus melon, and snake melon) ...... 9A Pumpkin (Cucurbita spp.) ...... 9B Squash, summer (Cucurbita pepo var. melopepo) (includes crookneck squash, scallop squash, straightneck squash, vegetable marrow, zucchini) ...... 9B Squash, winter (Cucurbita maxima; C. moschata) (includes butternut squash, calabaza, hubbard squash); (C. mixta; C. pepo) (includes acorn squash, spaghetti squash) ...... 9B Watermelon (includes hybrids and/or varieties of Citrullus lanatus) ...... 9A

(iii) Table. The following table 2 iden- commodities for each subgroup, and tifies the crop subgroups for Crop lists all the commodities included in Group 9, specifies the representative each subgroup.

TABLE 2—CROP GROUP 9 SUBGROUP LISTING

Representative commodities Commodities

Crop Subgroup 9A. Melon subgroup Cantaloupes ...... Citron melon; muskmelon; watermelon Crop Subgroup 9B. Squash/cucumber subgroup One cultivar of summer squash and cucumber. Chayote (fruit); Chinese waxgourd; cucumber; gherkin; gourd, edible; Momordica spp.; pumpkin; squash, summer; squash, winter.

(12) Crop Group 10. Citrus Fruit CROP GROUP 10: CITRUS FRUITS (CITRUS SPP., Group. FORTUNELLA SPP.) GROUP—COMMODITIES (i) Representative commodities. Sweet Calamondin (Citrus mitis×Citrofortunella mitis) orange; lemon and grapefruit. Citrus citron (Citrus medica) (ii) Commodities. The following is a Citrus hybrids (Citrus spp.) (includes list of all the commodities in Crop chironja, tangelo, tangor) Grapefruit (Citrus paradisi) Group 10: Kumquat (Fortunella spp.) Lemon (Citrus jambhiri, Citrus limon)

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Lime (Citrus aurantiifolia) (i) Representative commodities. Orange Mandarin (tangerine) (Citrus reticulata) or Tangerine/Mandarin, Lemon or Orange, sour (Citrus aurantium) Lime, and Grapefruit. Orange, sweet (Citrus sinensis) Pummelo (Citrus grandis, Citrus maxima) (ii) Commodities. The following is a Satsuma mandarin (Citrus unshiu) list of all the commodities in Crop Group 10–10. (13) Crop Group 10–10. Citrus Fruit Group.

TABLE 1—CROP GROUP 10–10: CITRUS FRUIT GROUP

Related crop sub- Commodities groups

Australian desert lime, Eremocitrus glauca (Lindl.) Swingle ...... 10–10B Australian finger lime, Microcitrus australasica (F. Muell.) Swingle ...... 10–10B Australian round lime, Microcitrus australis (A. Cunn. Ex Mudie) Swingle ...... 10–10B Brown River finger lime, Microcitrus papuana Winters ...... 10–10B Calamondin, Citrofortunella microcarpa (Bunge) Wijnands ...... 10–10A Citron, Citrus medica L ...... 10–10A Citrus hybrids, Citrus spp. Eremocitrus spp., Fortunella spp., Microcitrus spp., and Poncirus spp ...... 10–10A Grapefruit, Citrus paradisi Macfad ...... 10–10C Japanese summer grapefruit, Citrus natsudaidai Hayata ...... 10–10C Kumquat, Fortunella spp ...... 10–10B Lemon, Citrus limon (L.) Burm. f ...... 10–10B Lime, Citrus aurantiifolia (Christm.) Swingle ...... 10–10B Mediterranean mandarin, Citrus deliciosa Ten ...... 10–10A Mount White lime, Microcitrus garrowayae (F.M. Bailey) Swingle ...... 10–10B New Guinea wild lime, Microcitrus warburgiana (F.M. Bailey) Tanaka ...... 10–10B Orange, sour, Citrus aurantium L ...... 10–10A Orange, sweet, Citrus sinensis (L.) Osbeck ...... 10–10A Pummelo, Citrus maxima (Burm.) Merr ...... 10–10C Russell River lime, Microcitrus inodora (F.M. Bailey) Swingle ...... 10–10B Satsuma mandarin, Citrus unshiu Marcow ...... 10–10A Sweet lime, Citrus limetta Risso ...... 10–10B Tachibana orange, Citrus tachibana (Makino) Tanaka ...... 10–10A Tahiti lime, Citrus latifolia (Yu. Tanaka) Tanaka ...... 10–10B Tangelo, Citrus xtangelo J.W. Ingram & H.E. Moore ...... 10–10A, 10–10C Tangerine (Mandarin), Citrus reticulata Blanco ...... 10–10A Tangor, Citrus nobilis Lour ...... 10–10A Trifoliate orange, Poncirus trifoliata (L.) Raf ...... 10–10A Uniq fruit, Citrus aurantium Tangelo group ...... 10–10C Cultivars, varieties and/or hybrids of these.

(iii) Table. The following Table 2 tive commodities for each subgroup identifies the crop subgroups for Crop and lists all the commodities included Group 10–10, specifies the representa- in each subgroup.

TABLE 2—CROP GROUP 10–10: SUBGROUP LISTING

Representative commodities Commodities

Crop Subgroup 10–10A. Orange subgroup Orange or tangerine/mandarin ...... Calamondin; citron; citrus hybrids; mediterranean mandarin; or- ange, sour; orange, sweet; satsuma mandarin; tachibana or- ange; tangerine (mandarin); tangelo; tangor; trifoliate orange; cultivars, varieties, and/or hybrids of these. Crop Subgroup 10–10B. Lemon/Lime subgroup Lemon or lime ...... Australian desert lime; Australian finger lime; Australian round lime; brown river finger lime; kumquat; lemon; lime; mount white lime; New Guinea wild lime; Russell River lime; sweet lime; Tahiti lime; cultivars , varieties, and/or hybrids of these. Crop Subgroup 10–10C. Grapefruit subgroup Grapefruit ...... Grapefruit; Japanese summer grapefruit; pummelo; tangelo; uniq fruit; cultivars, varieties, and/or hybrids of these.

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(14) Crop Group 11: Pome Fruits Quince, Cydonia oblonga Mill. Group. Quince, Chinese, Chaenomeles speciosa (i) Representative commodities. Apple (Sweet) Nakai, and pear. Quince, Japanese, Chaenomeles japonica (ii) Commodities. The following is a (Thunb.) Lindl. ex Spach Tejocote, Crataegus mexicana DC. list of all the commodities included in Cultivars, varieties and/or hybrids of these. Crop Group 11: (16) Crop Group 12. Stone Fruits CROP GROUP 11: POME FRUITS GROUP— Group. COMMODITIES (i) Representative commodities. Sweet Apple (Malus domestica) cherry or tart cherry; peach; and plum Crabapple (Malus spp.) or fresh prune (Prunus domestica, Loquat (Eriobotrya japonica) Mayhaw (Crataegus aestivalis, C. opaca, and C. Prunus spp.) rufula) (ii) Commodities. The following is a Pear (Pyrus communis) list of all the commodities included in Pear, oriental (Pyrus pyrifolia) Crop Group 12: Quince (Cydonia oblonga) CROP GROUP 12: STONE FRUITS GROUP— (15) Crop group 11–10. Pome Fruit COMMODITIES Group. (i) Representative commodities. Apple Apricot (Prunus armeniaca) and Pear Cherry, sweet (Prunus avium), Cherry, tart (Prunus cerasus) (ii) Commodities. The following is a Nectarine (Prunus persica) list of all the commodities in Crop Peach (Prunus persica) Group 11–10. Plum (Prunus domestica, Prunus spp.) Plum, Chickasaw (Prunus angustifolia) CROP GROUP 11–10: POME FRUIT GROUP— Plum, Damson (Prunus domestica spp. COMMODITIES insititia) Apple, Malus domestica Borkh. Plum, Japanese (Prunus salicina) Azarole, Crataegus azarolus L. Plumcot (Prunus. armeniaca×P. domestica) Crabapple, Malus sylvestris (L.) Mill., M. Prune (fresh) (Prunus domestica, Prunus spp.) prunifolia (Willd.) Borkh. Loquat, Eriobotrya japonica (Thunb.) Lindl. (17) Crop Group 12–12: Stone Fruit Mayhaw, Crataegus aestivalis (Walter) Torr. & Group. A. Gray, C. opaca (i) Representative commodities. Sweet Hook. & Arn., and C. rufula Sarg. cherry or Tart cherry; Peach; and Medlar, Mespilus germanica L. Pear, Pyrus communis L. Plum or Prune plum. Pear, Asian, Pyrus pyrifolia (Burm. f.) Nakai (ii) Commodities. The following Table var. culta (Makino) Nakai 1 is a list of all commodities included Pseudocydonia sinensis (Thouin) C.K. Schneid. in Crop Group 12–12.

TABLE 1—CROP GROUP 12–12: STONE FRUIT GROUP

Related crop Commodities subgroup

Apricot (Prunus armeniaca L.) ...... 12–12C Apricot, Japanese (Prunus mume Siebold & Zucc.) ...... 12–12C Capulin (Prunus serotina Ehrh. var. salicifolia (Kunth) Koehne) ...... 12–12A Cherry, black (Prunus serotina Ehrh.) ...... 12–12A Cherry, Nanking (Prunus tomentosa Thunb.) ...... 12–12A Cherry, sweet (Prunus avium (L.) L.) ...... 12–12A Cherry, tart (Prunus cerasus L.) ...... 12–12A Jujube, Chinese (Ziziphus jujuba Mill.) ...... 12–12C Nectarine (Prunuspersica (L.) Batsch var. nucipersica (Suckow) C.K. Schneid) ...... 12–12B Peach (Prunus persica (L.) Batsch var. persica) ...... 12–12B Plum (Prunus domestica L. subsp. domestica) ...... 12–12C Plum, American (Prunus americana Marshall) ...... 12–12C Plum, beach (Prunus maritima Marshall) ...... 12–12C Plum, Canada (Prunus nigra Aiton) ...... 12–12C Plum, cherry (Prunus cerasifera Ehrh.) ...... 12–12C Plum, Chickasaw (Prunus angustifolia Marshall) ...... 12–12C Plum, Damson (Prunus domestica L. subsp. insititia (L.) C.K. Schneid.) ...... 12–12C Plum, Japanese (Prunus salicina Lindl.; P. salicina Lindl. var. salicina) ...... 12–12C Plum, Klamath (Prunus subcordata Benth.) ...... 12–12C Plum, prune (Prunus domestica L. subsp. domestica) ...... 12–12C Plumcot (Prunus hybr.) ...... 12–12C

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TABLE 1—CROP GROUP 12–12: STONE FRUIT GROUP—Continued

Related crop Commodities subgroup

Sloe (Prunus spinosa L.) ...... 12–12C Cultivars, varieties, and/or hybrids of these.

(iii) Crop subgroups. The following resentative commodities for each sub- Table 2 identifies the crop subgroups group, and lists all the commodities in- for Crop Group 12–12, specifies the rep- cluded in each subgroup.

TABLE 2—CROP GROUP 12–12: SUBGROUP LISTING

Representative commodities Commodities

Crop subgroup 12–12A. Cherry subgroup

Cherry, sweet or Cherry, tart .... Capulin; Cherry, black; Cherry, Nanking; Cherry, sweet; Cherry, tart; cultivars, varieties, and/or hybrids of these.

Crop subgroup 12–12B. Peach subgroup

Peach ...... Peach; Nectarine; cultivars, varieties, and/or hybrids of these.

Crop subgroup 12–12C. Plum subgroup

Plum or Prune plum ...... Apricot; Apricot, Japanese; Jujube, Chinese; Plum; Plum, American; Plum, beach; Plum, Can- ada; Plum, cherry; Plum, Chickasaw; Plum, Damson; Plum, Japanese; Plum, Klamath; Plumcot; Plum, prune; Sloe; cultivars, varieties, and/or hybrids of these.

(18) Crop Group 13. Berries Group. (ii) Table. The following table 1 lists (i) Representative commodities. Any all the commodities included in Crop one blackberry or any one raspberry; Group 13 and identifies the related sub- and blueberry. groups.

TABLE 1—CROP GROUP 13: BERRIES GROUP

Related crop Commodities subgroups

Blackberry (Rubus eubatus) (including bingleberry, black satin berry, boysenberry, Cherokee blackberry, Chesterberry, Cheyenne blackberry, coryberry, darrowberry, dewberry, Dirksen thornless berry, Himalayaberry, hullberry, Lavacaberry, lowberry, Lucretiaberry, mammoth blackberry, marionberry, nectarberry, olallieberry, Oregon evergreen berry, phenomenalberry, rangeberry, ravenberry, rossberry, Shawnee blackberry, youngberry, and varieties and/or hybrids of these) ...... 13A Blueberry (Vaccinium spp.) ...... 13B Currant (Ribes spp.) ...... 13B Elderberry (Sambucus spp.) ...... 13B Gooseberry (Ribes spp.) ...... 13B Huckleberry (Gaylussacia spp.) ...... 13B Loganberry (Rubus loganobaccus) ...... 13A Raspberry, black and red (Rubus occidentalis, Rubus strigosus, Rubus idaeus) ...... 13A

(iii) Table. The following table 2 iden- commodities for each subgroup, and tifies the crop subgroups for Crop lists all the commodities included in Group 13, specifies the representative each subgroup.

TABLE 2—CROP GROUP 13 SUBGROUPS LISTING

Representative commodities Commodities

Crop Subgroup 13A. Caneberry (blackberry and raspberry) subgroup. Any one blackberry or any one raspberry...... Blackberry; loganberry; red and black raspberry; cultivars and/or hybrids of these. Crop Subgroup 13B. Bushberry subgroup..

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TABLE 2—CROP GROUP 13 SUBGROUPS LISTING—Continued

Representative commodities Commodities

Blueberry, highbush...... Blueberry, highbush and lowbush; currant; elderberry; gooseberry; huckleberry.

(19) Crop Group 13-07. Berry and Small berry; grape; fuzzy kiwifruit, and Fruit Crop Group strawberry. (i) Representative commodities. Any (ii) Table. The following Table 1 lists one blackberry or any one raspberry; all the commodities listed in Crop highbush blueberry; elderberry or mul- Group 13-07 and identifies the related crop subgroups.

TABLE 1—CROP GROUP 13-07: BERRY AND SMALL FRUIT CROP GROUP

Commodities Related crop subgroups

Amur river grape (Vitis amurensis Rupr) ...... 13-07D, 13-07E, 13-07F Aronia berry (Aronia spp.) ...... 13-07B Bayberry (Myrica spp.) ...... 13-07C Bearberry (Arctostaphylos uva-ursi) ...... 13-07G, 13-07H Bilberry (Vaccinium myrtillus L.) ...... 13-07G, 13-07H Blackberry (Rubus spp.) (including Andean blackberry, arctic blackberry, bingleberry, black satin berry, boysenberry, brombeere, California blackberry, Chesterberry, Cherokee blackberry, Chey- enne blackberry, common blackberry, coryberry, darrowberry, dewberry, Dirksen thornless berry, evergreen blackberry, Himalayaberry, hullberry, lavacaberry, loganberry, lowberry, Lucretiaberry, mammoth blackberry, marionberry, mora, mures deronce, nectarberry, Northern dewberry, olallieberry, Oregon evergreen berry, phenomenalberry, rangeberry, ravenberry, rossberry, Shaw- nee blackberry, Southern dewberry, tayberry, youngberry, zarzamora, and cultivars, varieties and/or hybrids of these.) ...... 13-07A Blueberry, highbush (Vaccinium spp.) ...... 13-07B Blueberry, lowbush (Vaccinium angustifolium Aiton) ...... 13-07B Buffalo currant (Ribes aureum Pursh) ...... 13-07B Buffaloberry (Shepherdia argentea (Pursh) Nutt.) ...... 13-07C Che (Cudrania tricuspidata Bur. Ex Lavallee) ...... 13-07C Chilean guava (Myrtus ugni Mol.) ...... 13-07B Chokecherry (Prunus virginiana L.) ...... 13-07C Cloudberry (Rubus chamaemorus L.) ...... 13-07G, 13-07H Cranberry (Vaccinium macrocarpon Aiton) ...... 13-07G, 13-07H Currant, black (Ribes nigrum L.) ...... 13-07B Currant, red (Ribes rubrum L.) ...... 13-07B Elderberry (Sambucus spp.) ...... 13-07B, 13-07C European barberry (Berberis vulgaris L.) ...... 13-07B Gooseberry (Ribes spp.) ...... 13-07B, 13-07D, 13- 07E, 13-07F Grape (Vitis spp.) ...... 13-07D, 13-07F Highbush cranberry (Viburnum opulus L. var. Americanum Aiton) ...... 13-07B Honeysuckle, edible (Lonicera caerula L. var. emphyllocalyx Nakai, Lonicera caerula L var . edulis Turcz. ex herder) ...... 13-07B Huckleberry (Gaylussacia spp.) ...... 13-07B Jostaberry (Ribes x nidigrolaria Rud. Bauer and A. Bauer) ...... 13-07B Juneberry (Saskatoon berry) (Amelanchier spp.) ...... 13-07B, 13-07C Kiwifruit, fuzzy (Actinidia deliciosa A. Chev.) (C.F. Liang and A.R. Fergusons, Actinida chinensis Planch.) ...... 13-07D, 13-07E Kiwifruit, hardy (Actinidia arguta (Siebold and Zucc.) Planch. ex Miq) ...... 13-07D, 13-07E, 13-07F Lingonberry (Vaccinium vitis-idaea L.) ...... 13-07B, 13-07G 13-07H Maypop (Passiflora incarnata L.) ...... 13-07E, 13-07F Mountain pepper berries (Tasmannia lanceolata)(Poir.) A.C.Sm...... 13-07C Mulberry (Morus spp.) ...... 13-07C Muntries (Kunzea pomifera F. Muell.) ...... 13-07G, 13-07H Native currant (Acrotriche depressa R. BR.) ...... 13-07B Partridgeberry (Mitchella repens L.) ...... 13-07G, 13-07H Phalsa (Grewia subinaequalis DC.) ...... 13-07C Pincherry (Prunus pensylvanica L.f.) ...... 13-07C Raspberry, black and red (Rubus spp.) ...... 13-07A Riberry (Syzygium luehmannii) ...... 13-07C Salal (Gaultheria shallon Pursh.) ...... 13-07B, 13-07C Schisandra berry (Schisandra chinensis (Turcz.) Baill.) ...... 13-07D, 13-07E, 13-07F Sea buckthorn (Hippophae rhamnoides L.) ...... 13-07B Serviceberry (Sorbus spp.) ...... 13-07C Strawberry (Fragaria x ananassa Duchesne) ...... 13-07G Wild raspberry (Rubus muelleri Lefevre ex P.J. Mull) ...... 13-07A

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TABLE 1—CROP GROUP 13-07: BERRY AND SMALL FRUIT CROP GROUP—Continued

Commodities Related crop subgroups

Cultivars, varieties, and/or hybrids of these......

(iii) Table. The following Table 2 tive commodities for each subgroup identifies the crop subgroups for Crop and lists all the commodities included Group 13-07, specifies the representa- in each subgroup.

TABLE 2—CROP GROUP 13-07: SUBGROUP LISTING

Representative commodities Commodities

Crop Subgroup 13-07A. Caneberry subgroup Any one blackberry or any one rasp- Blackberry; loganberry; raspberry, red and black; wild raspberry; cultivars, vari- berry.. eties, and/or hybrids of these. Crop Subgroup 13-07B. Bushberry subgroup. Blueberry, highbush...... Aronia berry; blueberry, highbush; blueberry, lowbush; buffalo currant; Chilean guava; currant, black; currant, red; elderberry; European, barberry; goose- berry; cranberry, highbush; honeysuckle, edible; huckleberry; jostaberry; Juneberry; lingonberry; native currant; salal; sea buckthorn; cultivars, vari- eties, and/or hybrids of these. Crop Subgroup 13-07C. Large shrub/tree berry subgroup. Elderberry or mulberry...... Bayberry; buffaloberry; che; chokecherry; elderberry; Juneberry; mountain pep- per berries; mulberry; phalsa; pincherry; riberry; salal; serviceberry; cultivars, varieties, and/or hybrids of these. Crop Subgroup 13-07D. Small fruit vine climbing subgroup. Grape and fuzzy kiwifruit...... Amur river grape; gooseberry; grape; kiwifruit, fuzzy; kiwifruit, hardy; Maypop; schisandra berry; cultivars, varieties, and /or hybrids of these. Crop Subgroup 13-07E. Small fruit vine climb- ing subgroup, except grape. Fuzzy kiwifruit...... Amur river grape; gooseberry; kiwifruit, fuzzy; kiwifruit, hardy; Maypop; schisandra berry; cultivars, varieties, and/or hybrids of these. Crop Subgroup 13-07F. Small fruit vine climb- ing subgroup except fuzzy kiwifruit. Grape...... Amur river grape; gooseberry; grape; kiwifruit, hardy; Maypop; schisandra berry; cultivars varieties, and/or hybrids of these. Crop Subgroup 13-07G. Low growing berry subgroup. Strawberry...... Bearberry; bilberry; blueberry, lowbush; cloudberry; cranberry; lingonberry; muntries; partridgeberry; strawberry; cultivars, varieties, and/or hybrids of these. Crop Subgroup 13-07H. Low growing berry subgroup, except strawberry. Cranberry ...... Bearberry; bilberry; blueberry, lowbush; cloudberry; cranberry; lingonberry; muntries; partridgeberry; cultivars, varieties, and/or cultivars of these.

(20) Crop Group 14. Tree Nuts Group. Macadamia nut (bush nut) (Macadamia spp.) (i) Representative commodities. Almond Pecan (Carya illinoensis) and pecan. Walnut, black and English (Persian) (Juglans (ii) Commodities. The following is a spp.) list of all the commodities included in (21) Crop Group 14–12. Tree Nut Group. Crop Group 14: (i) Representative commodities. Almond CROP GROUP 14: TREE NUTS—COMMODITIES and Pecan. Almond (Prunus dulcis) (ii) Commodities. The following is a Beech nut (Fagus spp.) list of all commodities included in Crop Brazil nut (Bertholletia excelsa) Group 14–12. Butternut (Juglans cinerea) Cashew (Anacardium occidentale) CROP GROUP 14–12: TREE NUT GROUP Chestnut (Castanea spp.) African nut-tree (Ricinodendron heudelotii Chinquapin (Castanea pumila) (Baill.) Heckel) Filbert (hazelnut) (Corylus spp.) Almond (Prunus dulcis (Mill.) D.A. Webb) Hickory nut (Carya spp.)

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Beechnut (Fagus grandifolia Ehrh.; F. (22) Crop Group 15. Cereal Grains sylvatica L.) Group. Brazil nut (Bertholletia excelsa Humb. & (i) Representative commodities. Corn Bonpl.) (fresh sweet corn and dried field corn), Brazilian pine (Araucaria angustifolia (Bertol.) Kuntze) rice, sorghum, and wheat. Bunya (Araucaria bidwillii Hook.) (ii) Commodities. The following is a Bur oak (Quercus macrocarpa Michx.) list of all the commodities included in Butternut (Juglans cinerea L.) Crop Group 15: Cajou nut (Anacardium giganteum Hance ex Engl.) CROP GROUP 15: CEREAL GRAINS— Candlenut (Aleurites moluccanus (L.) Willd.) COMMODITIES Cashew (Anacardium occidentale L.) Barley (Hordeum spp.) Chestnut (Castanea crenata Siebold & Zucc.; Buckwheat (Fagopyrum esculentum) C. dentata (Marshall) Borkh.; C. mollissima Corn (Zea mays) Blume; C. sativa Mill.) Millet, pearl (Pennisetum glaucum) Chinquapin (Castaneapumila (L.) Mill.) Millet, proso (Panicum milliaceum) Coconut (Cocos nucifera L.) Oats (Avena spp.) Coquito nut (Jubaea chilensis (Molina) Baill.) Popcorn (Zea mays var. everta) Dika nut (Irvingia gabonensis (Aubry- Rice (Oryza sativa) Lecomte ex O’Rorke) Baill.) Rye (Secale cereale) Ginkgo (Ginkgo biloba L.) Sorghum (milo) (Sorghum spp.) Guiana chestnut (Pachira aquatica Aubl.) Teosinte (Euchlaena mexicana) Hazelnut (Filbert) (Corylus americana Mar- Triticale (Triticum-Secale hybrids) shall; C. avellana L.; C. californica (A. DC.) Wheat (Triticum spp.) Rose; C. chinensis Franch.) Wild rice (Zizania aquatica) Heartnut (Juglans ailantifolia Carrie`re var. (23) Crop Group 16. Forage, Fodder cordiformis (Makino) Rehder) and Straw of Cereal Grains Group. Hickory nut (Carya cathayensis Sarg.; C. glabra (Mill.) Sweet; C. laciniosa (F. Michx.) (i) Representative commodities. Corn, W. P. C. Barton; C. myristiciformis (F. wheat, and any other cereal grain crop. Michx.) Elliott; C. ovata (Mill.) K. Koch; C. (ii) Commodities. The commodities in- tomentosa (Lam.) Nutt.) cluded in Crop Group 16 are: Forage, Japanese horse-chestnut (Aesculus turbinate fodder, and straw of all commodities Blume) included in the group cereal grains Macadamia nut (Macadamia integrifolia Maid- group. en & Betche; M. tetraphylla L.A.S. John- (24) Crop Group 17. Grass Forage, Fod- son) Mongongo nut (Schinziophyton rautanenii der, and Hay Group. (Schinz) Radcl.-Sm.) (i) Representative commodities. Ber- Monkey-pot (Lecythis pisonis Cambess.) muda grass; bluegrass; and bromegrass Monkey puzzle nut (Araucaria araucana or fescue. (Molina) K. Koch) (ii) Commodities. The commodities in- Okari nut (Terminalia kaernbachii Warb.) cluded in Crop Group 17 are: Any grass, Pachira nut (Pachira insignis (Sw.) Savigny) Gramineae family (either green or Peach palm nut (Bactris gasipaes Kunth var. cured) except sugarcane and those in- gasipaes) cluded in the cereal grains group, that Pecan (Carya illinoinensis (Wangenh.) K. Koch) will be fed to or grazed by livestock, all Pequi (Caryocar brasiliense Cambess.; C. pasture and range grasses and grasses villosum (Aubl.) Pers; C. nuciferum L.) grown for hay or silage. Pili nut (Canarium ovatum Engl.; C. vulgare (25) Crop Group 18. Nongrass Animal Leenh.) Feeds (Forage, Fodder, Straw, and Pine nut (Pinus edulis Engelm.; P. koraiensis Hay) Group. Siebold & Zucc.; P. sibirica Du Tour; P. (i) Representative commodities. Alfalfa pumila (Pall.) Regel; P. gerardiana Wall. ex and clover (Trifolium spp.) ´ D. Don; P. monophylla Torr. & Frem.; P. (ii) Commodities. The following is a quadrifolia Parl. ex Sudw.; P. pinea L.) Pistachio (Pistacia vera L.) list of all the commodities included in Sapucaia nut (Lecythis zabucaja Aubl.) Crop Group 18: Tropical almond (Terminalia catappa L.) CROP GROUP 18: NONGRASS ANIMAL FEEDS Walnut, black (Juglans nigra L.; J. hindsii (FORAGE, FODDER, STRAW, AND HAY) Jeps. ex R. E. Sm.; J. microcarpa Berland.) GROUP—COMMODITIES Walnut, English (Juglans regia L.) Yellowhorn (Xanthoceras sorbifolium Bunge) Alfalfa (Medicago sativa subsp. sativa) Cultivars, varieties, and/or hybrids of these Bean, velvet (Mucuna pruriens var. utilis)

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Clover (Trifolium spp., Melilotus spp.) TABLE 1—CROP GROUP 19: HERBS AND SPICES Kudzu (Pueraria lobata) GROUP—Continued Lespedeza (Lespedeza spp.) Lupin (Lupinus spp.) Related Sainfoin (Onobrychis viciifolia); crop Commodities sub- Trefoil (Lotus spp.) groups Vetch (Vicia spp.) Vetch, crown (Coronilla varia) Culantro (seed) (Eryngium foetidum) ...... 19B Vetch, milk (Astragalus spp). Cumin (Cuminum cyminum) ...... 19B Curry (leaf) (Murraya koenigii) ...... 19A (26) Crop Group 19. Herbs and Spices Dill (dillweed) (Anethum graveolens) ...... 19A Group. Dill (seed) (Anethum graveolens) ...... 19B (i) Representative commodities. Basil Fennel (common) (Foeniculum vulgare) ...... 19B Fennel, Florence (seed) (Foeniculum vulgare (fresh and dried); black pepper; chive; Azoricum Group) ...... 19B and celery seed or dill seed. Fenugreek (Trigonella foenumgraecum) ...... 19B (ii) Table. The following table 1 lists Grains of paradise (Aframomum melegueta) ...... 19B all the commodities included in Crop Horehound (Marrubium vulgare) ...... 19A Hyssop (Hyssopus officinalis) ...... 19A Group 19 and identifies the related sub- Juniper berry (Juniperus communis) ...... 19B groups. Lavender (Lavandula officinalis) ...... 19A Lemongrass (Cymbopogon citratus) ...... 19A TABLE 1—CROP GROUP 19: HERBS AND SPICES Lovage (leaf) (Levisticum officinale) ...... 19A Lovage (seed) (Levisticum officinale) ...... 19B GROUP Mace (Myristica fragrans) ...... 19B Marigold (Calendula officinalis) ...... 19A Related Marjoram (Origanum spp.) (includes sweet or an- crop Commodities sub- nual marjoram, wild marjoram or oregano, and groups pot marjoram) ...... 19A Mustard (seed) (Brassica juncea, B. hirta, B. nigra) 19B Allspice (Pimenta dioica) ...... 19B Nasturtium (Tropaeolum majus) ...... 19A Angelica (Angelica archangelica) ...... 19A Nutmeg (Myristica fragrans) ...... 19B Anise (anise seed) (Pimpinella anisum) ...... 19B Parsley (dried) (Petroselinum crispum) ...... 19A Anise, star (Illicium verum) ...... 19B Pennyroyal (Mentha pulegium) ...... 19A Annatto (seed) ...... 19B Pepper, black (Piper nigrum) ...... 19B Balm (lemon balm) (Melissa officinalis) ...... 19A Pepper, white ...... 19B Basil (Ocimum basilicum) ...... 19A Poppy (seed) (Papaver somniferum) ...... 19B Borage (Borago officinalis) ...... 19A Rosemary (Rosemarinus officinalis) ...... 19A Burnet (Sanguisorba minor) ...... 19A Rue (Ruta graveolens) ...... 19A Camomile (Anthemis nobilis) ...... 19A Saffron (Crocus sativus) ...... 19B Caper buds (Capparis spinosa) ...... 19B Sage (Salvia officinalis) ...... 19A Caraway (Carum carvi) ...... 19B Savory, summer and winter (Satureja spp.) ...... 19A Caraway, black (Nigella sativa) ...... 19B Sweet bay (bay leaf) (Laurus nobilis) ...... 19A Cardamom (Elettaria cardamomum) ...... 19B Tansy (Tanacetum vulgare) ...... 19A Cassia bark (Cinnamomum aromaticum) ...... 19B Tarragon (Artemisia dracunculus) ...... 19A Cassia buds (Cinnamomum aromaticum) ...... 19B Thyme (Thymus spp.) ...... 19A Catnip (Nepeta cataria) ...... 19A Vanilla (Vanilla planifolia) ...... 19B Celery seed (Apicum graveolens) ...... 19B Wintergreen (Gaultheria procumbens) ...... 19A Chervil (dried) (Anthriscus cerefolium) ...... 19A Woodruff (Galium odorata) ...... 19A Chive (Allium schoenoprasum) ...... 19A Wormwood (Artemisia absinthium) ...... 19A Chive, Chinese (Allium tuberosum) ...... 19A Cinnamon (Cinnamomum verum) ...... 19B (iii) Table. The following table 2 iden- Clary (Salvia sclarea) ...... 19A Clove buds (Eugenia caryophyllata) ...... 19B tifies the crop subgroups for Crop Coriander (cilantro or Chinese parsley) (leaf) Group 19, specifies the representative (Coriandrum sativum) ...... 19A commodities for each subgroup, and Coriander (cilantro) (seed) (Coriandrum sativum) ... 19B Costmary (Chrysanthemum balsamita) ...... 19A lists all the commodities included in Culantro (leaf) (Eryngium foetidum) ...... 19A each subgroup.

TABLE 2—CROP GROUP 19 SUBGROUPS

Representative commodities Commodities

Crop Subgroup 19A. Herb subgroup. Basil (fresh and dried) and chive...... Angelica; balm; basil; borage; burnet; camomile; catnip; chervil (dried); chive; chive, Chinese, clary; coriander (leaf); costmary; culantro (leaf); curry (leaf); dillweed; horehound; hyssop; lavender; lemongrass; lovage (leaf); marigold; marjoram (Origanum spp.); nasturtium; parsley (dried); pennyroyal; rose- mary; rue; sage; savory, summer and winter; sweet bay; tansy; tarragon; thyme; wintergreen; woodruff; and wormwood.

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TABLE 2—CROP GROUP 19 SUBGROUPS—Continued

Representative commodities Commodities

Crop Subgroup 19B. Spice subgroup. Black pepper; and celery seed or dill seed...... Allspice; anise (seed); anise, star; annatto (seed); caper (buds); caraway; cara- way, black; cardamom; cassia (buds); celery (seed); cinnamon; clove (buds); coriander (seed); culantro (seed); cumin; dill (seed); fennel, common; fennel, Florence (seed); fenugreek; grains of paradise; juniper (berry); lovage (seed); mace; mustard (seed); nutmeg; pepper, black; pepper, white; poppy (seed); saffron; and vanilla.

(27) Crop Group 20. Oilseed Group. (ii) Table. The following Table 1 lists (i) Representative commodities. all the commodities listed in Crop Rapeseed (canola varieties only); sun- Group 20 and identifies the related crop flower, seed and cottonseed. subgroups and includes cultivars and/or varieties of these commodities.

TABLE 1—CROP GROUP 20: OILSEED GROUP

Related crop Commodities subgroups

Borage, Borago officinalis L ...... 20A Calendula, Calendula officinalis L ...... 20B Castor oil plant, Ricinus communis L ...... 20B Chinese tallowtree, Triadica sebifera (L.) Small ...... 20B Cottonseed, Gossypium hirsutum L. Gossypium spp ...... 20C Crambe, Crambe hispanica L.; C. abyssinica Hochst. ex R.E. Fr ...... 20A Cuphea, Cuphea hyssopifolia Kunth ...... 20A Echium, Echium plantagineum L ...... 20A Euphorbia, Euphorbia esula L ...... 20B Evening primrose, Oenothera biennis L ...... 20B Flax seed, Linum usitatissimum L ...... 20A Gold of pleasure, Camelina sativa (L.) Crantz ...... 20A Hare’s ear mustard, Conringia orientalis (L.) Dumort ...... 20A Jojoba, Simmondsia chinensis (Link) C.K. Schneid ...... 20B Lesquerella, Lesquerella recurvata (Engelm. ex A. Gray) S. Watson ...... 20A Lunaria, Lunaria annua L ...... 20A Meadowfoam, Limnanthes alba Hartw. ex Benth ...... 20A Milkweed, Asclepias spp ...... 20A Mustard seed, Brassica hirta Moench, Sinapis alba L. subsp. Alba...... 20A Niger seed, Guizotia abyssinica (L.f.) Cass ...... 20B Oil radish, Raphanus sativus L. var. oleiformis Pers ...... 20A Poppy seed, Papaver somniferum L. subsp. Somniferum ...... 20A Rapeseed, Brassica spp.; B. napus L ...... 20A Rose hip, Rosa rubiginosa L ...... 20B Safflower, Carthamus tinctorious L ...... 20B Sesame, Sesamum indicum L., S. radiatum Schumach. & honn ...... 20A Stokes aster, Stokesia laevis (Hill) Greene ...... 20B Sunflower, Helianthus annuus L ...... 20B Sweet rocket, Hesperis matronalis L ...... 20A Tallowwood, Ximenia americana L ...... 20B Tea oil plant, Camellia oleifera C. Abel ...... 20B Vernonia, Vernonia galamensis (Cass.) Less ...... 20B Cultivars, varieties, and/or hybrids of these.

(iii) Table. The following Table 2 commodities for each subgroup and identifies the crop subgroups for Crop lists all the commodities included in Group 20, specifies the representative each subgroup.

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TABLE 2—CROP GROUP 20: SUBGROUP LISTING

Representative commodities Commodities

Crop subgroup 20A. Rapeseed subgroup Rapeseed, canola varieties only ...... Borage; crambe; cuphea; echium; flax seed; gold of pleasure; hare’s ear mustard; lesquerella; lunaria; meadowfoam; milk- weed; mustard seed; oil radish; poppy seed; rapeseed; ses- ame; sweet rocket cultivars, varieties, and/or hybrids of these. Crop subgroup 20B. Sunflower subgroup Sunflower, seed...... Calendula; castor oil plant; chinese tallowtree; euphorbia; evening primrose; jojoba; niger seed; rose hip; safflower; stokes aster; sunflower; tallowwood; tea oil plant; vernonia; cultivars, varieties, and/or hybrids of these. Crop subgroup 20C. Cottonseed subgroup Cottonseed ...... Cottonseed; cultivars, varieties, and/or hybrids of these.

(28) Crop Group 21. Edible fungi § 180.101 Specific tolerances; general Group. provisions. (i) Representative commodities. White (a) The tolerances established for button mushroom and any one oyster pesticide chemicals in this subpart C mushroom or any Shiitake mushroom. apply to residues resulting from their (ii) Table. The following is a list of all application prior to harvest or slaugh- the commodities in Crop Group 21. ter, unless otherwise stated. Toler- There are no related subgroups. ances are expressed in terms of parts by weight of the pesticide chemical per CROP GROUP 21—EDIBLE FUNGI GROUP— one million parts by weight of the raw COMMODITIES agricultural commodity. Blewitt (Lepista nuda) (b) The poisonous and deleterious Bunashimeji (Hypsizygus marrmoreus) Chinese mushroom (Volvariella volvacea) (Bull.) Singer substances for which tolerances are es- Enoki (Flammulina velutipes) (Curt.) Singer tablished by the regulations in this Hime-Matsutake (Agaricus blazei) Murill subpart C are named by their common Hirmeola (Auricularia auricular) names wherever practicable, otherwise Maitake (Grifola frondosa) Morel (Morchella spp.) by their chemical names. Nameko (Pholiota nameko) (c) The analytical methods to be used Net Bearing (Dictyophora) for determining whether pesticide resi- Oyster mushroom (Pleurotus spp.) Pom Pom (Hericium erinaceus) dues, including negligible residues, in Reishi mushroom (Ganoderma lucidum (Leyss. Fr.) Karst.) or on raw agricultural commodities are Rodman’s agaricus (Agaricus bitorquis) (Quel.) Saccardo in compliance with the tolerances es- Shiitake mushroom (Lentinula edodes (Berk.) Pegl.) tablished in this part 180 are identified Shimeji (Tricholoma conglobatum) Stropharia (Stropharia spp.) among the methods contained or ref- Truffle (Tuber spp.) erenced in the Food and Drug Adminis- White button mushroom (Agaricus bisporous (Lange) tration’s ‘‘Pesticide Analytical Man- Imbach) White Jelly Fungi (Tremella fuciformis) ual’’ which is available from the Food and Drug Administration, Department [60 FR 26635, May 17, 1995, as amended at 72 of Health, Education, and Welfare, 200 FR 69156, 69157, Dec. 7, 2007; 73 FR 52, Jan. 2, C Street SW., Washington, DC 20204. 2008; 75 FR 76289, Dec. 8, 2010; 77 FR 50620, Aug. 22, 2012] § 180.103 Captan; tolerances for resi- dues. Subpart C—Specific Tolerances (a)(1) General. Tolerances are estab- lished for residues of the fungicide, EDITORIAL NOTE: Nomenclature changes to captan (N-trichloromethylthio-4- subpart C of part 180 appear at 67 FR 41803– cyclohexene-1,2-dicarboximide) in or on 41808, June 19, 2002; 67 FR 42393–42397, June the following commodities: 21, 2002; 68 FR 39430–39435, July 1, 2003; 71 FR 74804–74812, Dec. 13, 2006; 72 FR 53137–53151, Parts per Commodity million Sept. 18, 2007; 72 FR 61536, Oct. 31, 2007; 73 FR 60155–60157, Oct. 10, 2008; 75 FR 56014, Sept. 15, Almond ...... 0.25 2010; and 76 FR 34885, June 15, 2011. Almond, hulls ...... 75 .0

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(c) Tolerances with regional registra- Commodity Parts per million tions. [Reserved] Animal feed, nongrass, group 18 ...... 0 .05 (d) Indirect or inadvertent residues. Apple ...... 25.0 [Reserved] Apricot ...... 10 .0 Blueberry ...... 20 .0 [72 FR 52016, Sept. 12, 2007] Caneberry, subgroup 13A ...... 25.0 Cherry, sweet ...... 50 .0 § 180.106 Diuron; tolerances for resi- Cherry, tart ...... 50.0 dues. Cotton, undelinted seed ...... 0 .05 Dill, seed ...... 0 .05 (a) General. Tolerances are estab- Flax, seed ...... 0 .05 lished for the combined residues of the Grape ...... 25 .0 Grain, cereal, forage, fodder and straw, group diuron, 3-(3,4- 16 ...... 0 .05 dichlorophenyl)-1,1-dimethylurea and Grain, cereal, group 15 ...... 0.05 its metabolites convertible to 3,4- Grass, forage ...... 0 .05 Grass, hay ...... 0 .05 dichloroaniline in or on food commod- Nectarine ...... 25 .0 ities, as follows: Okra ...... 0.05 Peach ...... 15 .0 Commodity Parts per Peanut ...... 0 .05 million Peanut, hay ...... 0.05 Pear ...... 25 .0 Alfalfa, forage ...... 3.0 Plum, prune, fresh ...... 10.0 Alfalfa, hay ...... 2.0 Rapeseed, forage ...... 0 .05 Apple ...... 0.1 Rapeseed, seed ...... 0 .05 Artichoke, globe ...... 1 Safflower, seed ...... 0 .05 Asparagus ...... 7 Sesame, seed ...... 0 .05 Banana ...... 0.1 Strawberry ...... 20.0 Berry group 13 ...... 0 .1 Sunflower, seed ...... 0.05 Cattle, fat ...... 1 Vegetable, brassica leafy, group 5 ...... 0 .05 Cattle, meat ...... 1 Vegetable, bulb, group 3 ...... 0 .05 Cattle, meat byproducts ...... 1 Vegetable, cucurbit, group 9 ...... 0.05 Citrus, oil ...... 3.0 Vegetable, foliage of legume, group 7 ...... 0 .05 Corn, field, grain ...... 0 .1 Vegetable, fruiting, group 8 ...... 0.05 Corn, pop, grain ...... 0.1 Vegetable, leafy, except brassica, group 4 ...... 0 .05 Cotton, undelinted seed ...... 0 .2 Vegetable, leaves of root and tuber, group 2 ..... 0 .05 Fish – freshwater finfish, farm raised ...... 2 .0 Fruit, citrus, group 10, except lemon ...... 0 .05 Vegetable, legume, group 6 ...... 0 .05 Goat, fat ...... 1 Vegetable, root and tuber, group 1 ...... 0 .05 Goat, meat ...... 1 Goat, meat byproducts ...... 1 (2) Tolerances are established for the Grain, aspirated fractions ...... 5 .0 combined residues of the fungicide, Grape ...... 0 .05 Grass, forage, except bermudagrass ...... 2 captan (N-trichloromethylthio-4- Grass, hay, except bermudagrass ...... 2 cyclohexene-1,2-dicarboximide) and its Hazelnut ...... 0 .1 metabolite 1,2,3,6- Hog, fat ...... 1 tetrahydrophthalimide (THPI), meas- Hog, meat ...... 1 Hog, meat byproducts ...... 1 ured at THPI, in or on the following Horse, fat ...... 1 commodities: Horse, meat ...... 1 Horse, meat byproducts ...... 1 Parts per Lemon ...... 0.5 Commodity million Nut, macadamia ...... 0.05 Olive ...... 1 Cattle, fat ...... 0.15 Papaya ...... 0 .5 Cattle, meat ...... 0 .20 Peach ...... 0 .1 Cattle, meat byproducts ...... 0.30 Pear ...... 1 Goat, fat ...... 0 .15 Pea, field, seed ...... 0 .1 Goat, meat ...... 0.20 Pea, field, vines ...... 2 Goat, meat byproducts ...... 0 .30 Pea, field, hay ...... 2 Hog, fat ...... 0 .15 Pecan ...... 0 .05 Hog, meat ...... 0 .20 Peppermint, tops ...... 1 .5 Hog, meat byproducts ...... 0 .30 Pineapple ...... 0.1 Horse, fat ...... 0 .15 Pineapple, process residue ...... 0 .4 Horse, meat ...... 0 .20 Sheep, fat ...... 1 Horse, meat byproducts ...... 0 .30 Sheep, meat ...... 1 Milk ...... 0.10 Sheep, meat byproducts ...... 1 Sheep, fat ...... 0 .15 Sorghum, grain, forage ...... 2 Sheep, meat ...... 0.20 Sorghum, grain, grain ...... 0 .5 Sheep, meat byproducts ...... 0 .30 Sorghum, grain, stover ...... 2 Spearmint, tops ...... 1 .5 Sugarcane, cane ...... 0.2 (b) Section 18 emergency exemptions. Sugarcane, molasses ...... 0 .7 [Reserved] Walnut ...... 0 .05

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Parts per 1 Parts per Commodity million Commodity million

Wheat, bran ...... 0.7 Bean, dry, seed ...... 3 .0 Wheat, forage ...... 2 Bean, succulent ...... 3 .0 Wheat, grain ...... 0 .5 Brussels sprouts ...... 3 .0 Wheat, hay ...... 2 Cattle, fat ...... 0.1 Wheat, straw ...... 1 .5 Cattle, meat ...... 0 .1 Cattle, meat byproducts ...... 0.1 Cauliflower ...... 2 .0 (b) Section 18 emergency exemptions. Celery ...... 10 [Reserved] Cotton, hulls ...... 1 .0 Cotton, meal ...... 1 .0 (c) Tolerances with regional registra- Cotton, undelinted seed ...... 0 .5 tions. Tolerances with a regional reg- Cranberry ...... 0 .5 istration as defined in § 180.1(l) are es- Egg ...... 0 .1 tablished for the combined residues of Goat, fat ...... 0 .1 Goat, meat ...... 0.1 the herbicide diuron (3-(3,4- Goat, meat byproducts ...... 0 .1 dichlorophenyl)-1,1-dimethylurea and Hog, fat ...... 0 .1 its metabolites convertible to 3,4- Hog, meat ...... 0 .1 Hog, meat byproducts ...... 0 .1 dichloroaniline) in or on the raw agri- Horse, fat ...... 0 .1 cultural commodities: Horse, meat ...... 0 .1 Horse, meat byproducts ...... 0 .1 Parts per Lettuce, head ...... 10 Commodity million Milk ...... 0.1 Peanut ...... 0 .2 Barley, bran ...... 0 .7 Pepper ...... 4 .0 Barley, grain ...... 0 .2 Peppermint, tops ...... 27 Barley, hay ...... 2 Poultry, fat ...... 0.1 Barley, straw ...... 1 .5 Poultry, meat ...... 0 .1 Cactus ...... 0 .05 Poultry, meat byproducts ...... 0.1 Clover, forage ...... 0.1 Sheep, fat ...... 0 .1 Sheep, meat ...... 0.1 Clover, hay ...... 1.0 Sheep, meat byproducts ...... 0 .1 Oat, forage ...... 2 Spearmint, tops ...... 27 Oat, grain ...... 0 .1 Soybean, seed ...... 1 .0 Oat, hay ...... 2 Oat, straw ...... 1.5 1 Where there is a direct use of methamidophos on the Trefoil, forage ...... 0 .1 commodity, residues of methamidophos resulting from methamidophos application are regulated under 40 CFR Trefoil, hay ...... 1 .5 180.315. Vetch, forage ...... 0 .1 Vetch, hay ...... 1 .5 (2) A tolerance of 0.02 ppm is estab- lished for residues of acephate, O,S-di- (d) Indirect or inadvertent residues. methyl acetyl phosphoramidothioate, [Reserved] including its metabolites and degradates other than methamidophos, [63 FR 2164, Jan. 14, 1998, as amended at 63 in or on all food items (other than FR 57072, Oct. 26, 1998; 64 FR 41305, July 30, 1999; 66 FR 28671, May 24, 2001; 67 FR 46883, those already covered by a higher tol- July 17, 2002; 69 FR 71717, Dec. 10, 2004; 72 FR erance as a result of use on growing 32540, June 13, 2007; 72 FR 35666, June 29, 2007; crops) in food handling establishments 73 FR 54958, Sept. 24, 2008; 76 FR 34885, June where food and food products are held, 15, 2011] processed, prepared and served, includ- ing food service, manufacturing and § 180.108 Acephate; tolerances for resi- processing establishments, such as res- dues. taurants, cafeterias, supermarkets, (a) General. (1) Tolerances are estab- bakeries, breweries, dairies, meat lished for residues of acephate, O,S-di- slaughtering and packing , and methyl acetyl phosphoramidothioate, canneries, where application of including its metabolites and acephate shall be limited solely to spot degradates other than methamidophos, and/or crack and crevice treatment (a in or on the commodities in the fol- coarse, low-pressure spray shall be used lowing table. Compliance with the tol- to avoid atomization or splashing of erance levels specified in this para- the spray for spot treatments; equip- graph is to be determined by measuring ment capable of delivering a pin- only acephate, O,S-dimethyl acetyl stream of insecticide shall be used for phosphoramidothioate, in or on the crack and crevice treatments). Spray commodity. concentration shall be limited to a

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maximum of 1.0 percent active ingre- (d) Indirect or inadvertent residues. dient. Contamination of food or food- [Reserved] contact surfaces shall be avoided. Com- [63 FR 13542, Mar. 20, 1998, as amended at 67 pliance with the tolerance levels speci- FR 49615, July 31, 2002; 73 FR 5108, Jan. 29, fied in this paragraph is to be deter- 2008; 75 FR 60237, Sept. 29, 2010] mined by measuring only acephate, O,S-dimethyl acetyl § 180.111 Malathion; tolerances for res- phosphoramidothioate, in or on the idues. commodity. (a) General. (1) Tolerances are estab- (3) Tolerances are established for res- lished for residues of the insecticide idues of methamidophos, O,S-dimethyl malathion (O,O-dimethyl phosphoramidothioate, including its dithiophosphate of diethyl metabolites and degradates, in or on mercaptosuccinate) in or on the fol- the commodities in the following table lowing food commodities: as a result of the application of Commodity Parts per acephate. Compliance with the toler- million ance levels specified in this paragraph Alfalfa, forage ...... 135 is to be determined by measuring only Alfalfa, hay ...... 135 methamidophos, O,S-dimethyl Almond, hulls ...... 50 Almond, postharvest ...... 8 phosphoramidothioate, in or on the Apple ...... 8 commodity. Apricot ...... 8 Asparagus ...... 8 Avocado ...... 8 Parts per Commodity million Barley, grain, postharvest ...... 8 Bean, dry, seed ...... 8 Bean, dry, seed ...... 1 Bean, succulent ...... 8 Beet, garden, roots ...... 8 Bean, succulent ...... 1 Beet, garden, tops ...... 8 Brussels sprouts ...... 0 .5 Beet, sugar, roots ...... 1 Cauliflower ...... 0 .5 Beet, sugar, tops ...... 8 Celery ...... 1 Blackberry ...... 8 Cranberry ...... 0 .1 Blueberry ...... 8 Lettuce, head ...... 1 Boysenberry ...... 8 Pepper ...... 1 Carrot, roots ...... 8 Peppermint, tops ...... 1 Chayote, fruit ...... 8 Spearmint, tops ...... 1 Chayote, roots ...... 8 Cherry ...... 8 Chestnut ...... 1 (b) Section 18 emergency exemptions. Clover, forage ...... 135 [Reserved] Clover, hay ...... 135 Corn, field, forage ...... 8 (c) Tolerances with regional registra- Corn, field, grain, postharvest ...... 8 tions. A tolerance with a regional reg- Corn, pop, grain, postharvest ...... 8 istration is established for residues of Corn, sweet, forage ...... 8 Corn, sweet, kernel plus cob with husks re- acephate, O,S-dimethyl acetyl moved ...... 2 phosphoramidothioate, including its Cowpea, forage ...... 135 metabolites and degradates other than Cowpea, hay ...... 135 Cranberry ...... 8 methamidophos, in or on the com- Cucumber ...... 8 modity in the following table. Compli- Currant ...... 8 ance with the tolerance level specified Date, dried fruit ...... 8 Dewberry ...... 8 in this paragraph is to be determined Eggplant ...... 8 by measuring only acephate, O,S-di- Fig ...... 8 methyl acetyl phosphoramidothioate, Flax, seed ...... 0 .1 Garlic, bulb ...... 8 in or on the commodity. Gooseberry ...... 8 Grape ...... 8 Parts per Commodity1 Grapefruit ...... 8 million Guava ...... 8 Hazelnut ...... 1 Nut, macadamia ...... 0.05 Hop, dried cones ...... 1 Horseradish ...... 8 1 Where there is a direct use of methamidophos on the commodity, residues of methamidophos resulting from Kumquat ...... 8 methamidophos application are regulated under 40 CFR Leek ...... 8 180.315. Lemon ...... 8 Lentil, seed ...... 8 Lespedeza, hay ...... 135

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of diethyl mercaptosuccinate), in or on Commodity Parts per million the following food commodities: Lime ...... 8 Parts per Loganberry ...... 8 Commodity million Lupin, seed ...... 8 Mango ...... 8 Barley, straw ...... 50 Melon ...... 8 Corn, field, stover ...... 30 .0 Mushroom ...... 8 Cotton, undelinted seed ...... 20 .0 Nectarine ...... 8 Grass, forage ...... 200 Nut, macadamia ...... 1 Oat, grain, postharvest ...... 8 Grass, hay ...... 270 Okra ...... 8 Oat, forage ...... 4 .0 Onion, bulb ...... 8 Oat, straw ...... 50 Onion, green ...... 8 Rye, forage ...... 4 .0 Orange ...... 8 Rye, straw ...... 50 Papaya ...... 1 Watercress ...... 0 .2 Parsnip ...... 8 Wheat, forage ...... 4 .0 Passionfruit ...... 8 Wheat, straw ...... 50 Pea ...... 8 Pea, field, hay ...... 8 (3) Tolerances are established for res- Pea, field, vines ...... 8 Peach ...... 8 idues of the insecticide malathion Peanut, hay ...... 135 (O,O-dimethyl dithiophosphate of Peanut, postharvest ...... 8 diethyl mercaptosuccinate), in or on Pear ...... 8 Pecan ...... 8 the following food commodities: Pepper ...... 8 Peppermint, tops ...... 8 Commodity Parts per Pineapple ...... 8 million Plum ...... 8 Cattle, fat ...... 4 Plum, prune ...... 8 Cattle, meat1 ...... 4 Potato ...... 8 1 Pumpkin ...... 8 Cattle, meat byproducts ...... 4 Quince ...... 8 Egg ...... 0 .1 Radish ...... 8 Goat, fat ...... 4 1 Raspberry ...... 8 Goat, meat ...... 4 1 Rice, grain, postharvest ...... 8 Goat, meat byproducts ...... 4 Rice, wild ...... 8 Hog, fat ...... 4 Rutabaga ...... 8 Hog, meat1 ...... 4 Rye, grain, postharvest ...... 8 Hog, meat byproducts1 ...... 4 Safflower, seed ...... 0 .2 Horse, fat ...... 4 Salsify, roots ...... 8 Horse, meat1 ...... 4 Salsify, tops ...... 8 Horse, meat byproducts1 ...... 4 Shallot, bulb ...... 8 Milk, fat ...... 0 .5 Sorghum, grain, forage ...... 8 Poultry, fat ...... 4 Sorghum, grain, grain, postharvest ...... 8 Poultry, meat1 ...... 4 Soybean, forage ...... 135 Poultry, meat byproducts1 ...... 4 Soybean, hay ...... 135 Sheep, fat ...... 4 Soybean, seed ...... 8 Sheep, meat1 ...... 4 Soybean, vegetable, succulent ...... 8 Sheep, meat byproducts1 ...... 4 Spearmint, tops ...... 8 1 The tolerance level shall not be exceeded in any cut of Squash, summer ...... 8 meat or in any meat byproducts from cattle, goat, hog, horse, Squash, winter ...... 8 poultry, or sheep. Strawberry ...... 8 Sunflower, seed, postharvest ...... 8 (4) Malathion may be safely used in Sweet potato, roots ...... 1 accordance with the following condi- Tangerine ...... 8 Tomato ...... 8 tions: Trefoil, forage ...... 135 (i) It is incorporated into paper trays Trefoil, hay ...... 135 in amounts not exceeding 100 milli- Turnip, greens ...... 8 Turnip, roots ...... 8 grams per square foot. Vegetable, brassica, leafy, group 5 ...... 8 (ii) Treated paper trays are intended Vegetable, leafy, except brassica, group 4 ...... 8 for use only in the drying of grape (rai- Vetch, hay ...... 135 sins). Walnut ...... 8 Wheat, grain, postharvest ...... 8 (iii) Total residues of malathion re- sulting from drying of grape on treated (2) Tolerances are established for the trays and from application to grape be- combined residues of the insecticide fore harvest shall not exceed 12 parts malathion (O,O-dimethyl per million on processed ready-to-eat dithiophosphate of diethyl raisins. mercaptosuccinate) and its metabolite, (5) Residues of malathion in saf- (O,O-dimethyl thiophosphate flower, refined oil from application to

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the growing safflower plant shall not Expiration/ Commodity Parts per Revocation exceed 0.6 parts per million. million Date (6) Malathion may be safely used for the control of insects during the drying Apple ...... 4.0 1 None Bean ...... 7.0 1 10/27/07 of grape (raisins) in compliance with Cabbage ...... 7.0 1 10/27/07 paragraph (a)(4) of this section by in- Cherry ...... 4.0 1 None Cranberry ...... 4.0 1 None corporation into paper trays in Fruit, citrus, group 10 ...... 4.0 1 None amounts not exceeding 100 milligrams Grape ...... 4.0 1 None per square foot. Lettuce ...... 7.0 1 10/27/07 Nectarine ...... 4.0 1 None (7) Malathion (O,O-dimethyl Peach ...... 4.0 1 None dithiophosphate of diethyl Pear ...... 4.0 1 None mercaptosuccinate) may be safely used Raspberry ...... 7.0 1 10/27/07 in feed in accordance with the fol- 1Some of these tolerances were established on the basis of data acquired at the public hearings held in 1950 (formerly lowing conditions. § 180.101) and the remainder were established on the basis of pesticide petitions presented under the procedure specified (i) A tolerance of 50 parts per million in the amendment to the Federal Food, Drug, and Cosmetic is established for residues of malathion Act by Pub. L. 518, 83d Congress (68 Stat. 511) in citrus, dried pulp for cattle feed, (b) Section 18 emergency exemptions. when present as the result of the appli- [Reserved] cation of the pesticide to bagged citrus (c) Tolerances with regional registra- pulp during storage. Whether or not tions. Tolerances with regional reg- tolerances for residues of malathion on istrations, as defined in § 180.1(l), are the fresh fruit have been established established for residues of the fun- under section 408 of the Act, the total gicide ferbam (ferric residue of malathion in the citrus, dimethyldithiocarbamate), calculated dried pulp shall not exceed 50 parts per as carbon disulfide, in or on the fol- million. lowing food commodities: (ii) A tolerance of 10 parts per million is established for malathion in non- Commodity Parts per million medicated cattle feed concentrate Mango ...... 4.0 1 blocks resulting from its application as 1 This tolerance was established on the basis of data ac- a pesticide to paper used in packaging quired at the public hearings held in 1950 (formerly § 180.101) and the remainder was established on the basis of pesticide the nonmedicated cattle feed con- petitions presented under the procedure specified in the centrate blocks. amendment to the Federal Food, Drug, and Cosmetic Act by Pub. L. 518, 83d Congress (68 Stat. 511) (b) Section 18 emergency exemptions. [Reserved] (d) Indirect or inadvertent residues. [Reserved] (c) Tolerances with regional registra- tions. [Reserved] [63 FR 57072, Oct. 26, 1998, as amended at 72 (d) Indirect or inadvertent residues. FR 53453, Sept. 19, 2007] [Reserved] § 180.116 Ziram; tolerances for resi- [43 FR 22974, May 30, 1978, as amended at 43 dues. FR 45584, Oct. 3, 1978; 44 FR 38844, July 3, (a) General. Tolerances are estab- 1979; 45 FR 76145, Nov. 18, 1980; 47 FR 42738, lished for residues of the fungicide Sept. 29, 1982; 47 FR 55226, Dec. 8, 1982; 52 FR ziram (zinc dimethyldithiocarbamate), 45183, Nov. 25, 1987; 62 FR 66023, 66025, Dec. 17, calculated as zinc 1997; 65 FR 33694, May 24, 2000; 72 FR 35665, June 29, 2007; 73 FR 54959, Sept. 24, 2008; 74 FR ethylenebisdithiocarbamate, in or on 47455, Sept. 16, 2009; 75 FR 60238, Sept. 29, the following food commodities: 2010] Parts per Expiration/ Commodity million revocation § 180.114 Ferbam; tolerances for resi- date dues. Almond ...... 1 0.1 None (a) General. Tolerances are estab- Apple ...... 1 7.0 None Apricot ...... 1 7.0 None lished for residues of the fungicide Blackberry ...... 1 7.0 5/11/13 ferbam (ferric Blueberry ...... 1 7.0 None dimethyldithiocarbamate), calculated Cherry, sweet ...... 1 7.0 None Cherry, tart ...... 1 7.0 None as carbon disulfide, in or on the fol- Grape ...... 7.0 None lowing food commodities: Huckleberry ...... 7.0 None

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Expiration/ Parts per Commodity Parts per revocation Commodity million million date Corn, pop, stover ...... 0.08 Peach ...... 7.0 None Corn, sweet, forage ...... 0 .08 Pear ...... 1 7.0 None Corn, sweet, kernel plus cob with husks re- Pecan ...... 0.1 None moved ...... 0 .08 Quince ...... 1 7.0 None Corn, sweet, stover ...... 0 .08 Strawberry ...... 7.0 None Cotton, gin byproducts ...... 0 .20 Tomato ...... 1 7.0 None Cotton, undelinted seed ...... 0 .08 1 Some of these tolerances were established on the basis of Fruit, citrus, group 10 ...... 0 .1 data acquired at the public hearings held in 1950 (formerly Lespedeza, forage ...... 0 .1 § 180.101) and the remainder were established on the basis Lespedeza, hay ...... 0.1 of pesticide petitions presented under the procedure specified Pea, succulent ...... 0 .08 in the amendment to the Federal Food, Drug, and Cosmetic Safflower, seed ...... 0 .08 Act by Public Law 518, 83d Congress (68 Stat. 511). Sunflower, seed ...... 0.08 Tomato ...... 0.08 (b) Section 18 emergency exemptions. Trefoil, forage ...... 0 .1 [Reserved] Trefoil, hay ...... 0 .1 (c) Tolerances with regional registra- Vegetable, root ...... 0 .1 tions. [Reserved] Walnut ...... 0 .08 (d) Indirect or inadvertent residues. [Reserved] (b) Section 18 emergency exemptions. [Reserved] [68 FR 39437, July 1, 2003, as amended at 71 (c) Tolerances with regional registra- FR 54432, Sept. 15, 2006; 73 FR 54959, Sept. 24, tions. [Reserved] 2008; 77 FR 59123, Sept. 26, 2012] (d) Indirect or inadvertent residues. [Reserved] § 180.117 S-Ethyl dipropylthiocarbamate; tolerances [75 FR 60239, Sept. 29, 2010] for residues. (a) General. Tolerances are estab- § 180.121 Methyl parathion; tolerances lished for residues of the herbicide S- for residues. ethyl dipropylthiocarbamate, including (a) General. Tolerances are estab- its metabolites and degradates, in or lished for residues of the insecticide on the commodities in the following methyl parathion, including its me- table. Compliance with the tolerance tabolites and degradates, in or on the levels specified in this paragraph is to commodities in the table in this para- be determined by measuring only the graph. Compliance with the tolerance sum of S-ethyl dipropylthiocarbamate, levels specified in this paragraph is to S-ethyl (2- be determined by measuring only hydroxypropyl)propylcarbamothioate, methyl parathion, O,O-dimethyl O-(4- S-(2-hydroxy- nitrophenyl) phosphorothioate, in or ethyl)dipropylcarbamothioate, and S- on the commodity. ethyl (3- Expiration/ hydroxypropyl)propylcarbamothioate, Commodity Parts per Revocation calculated as the stoichiometric equiv- million date alent of S-ethyl Alfalfa, forage ...... 1.25 12/31/13 dipropylthiocarbamate, in or on the Alfalfa, hay ...... 5.0 12/31/13 commodity. Almond ...... 0.1 12/31/13 Almond, hulls ...... 3.0 12/31/13 Parts per Barley ...... 1.0 12/31/13 Commodity million Corn, field, forage ...... 1.0 12/31/13 Corn, field, grain ...... 1.0 12/31/13 Alfalfa, forage ...... 0.2 Corn, pop, grain ...... 1.0 12/31/13 Alfalfa, hay ...... 0.6 Corn, sweet, forage ...... 1.0 12/31/13 Almond ...... 0.08 Corn, sweet, kernel plus cob with Almond, hulls ...... 0 .08 husks removed ...... 1.0 12/31/13 Bean, dry, seed ...... 0 .08 Cotton, undelinted seed ...... 0.75 12/31/13 Bean, succulent ...... 0 .08 Grass, forage ...... 1.0 12/31/13 Beet, garden, tops ...... 0 .5 Oat ...... 1.0 12/31/13 Beet, sugar, molasses ...... 0 .4 Onion ...... 1.0 12/31/13 Beet, sugar, tops ...... 0.5 Pea, field, vines ...... 1.0 12/31/13 Clover, forage ...... 0.1 Potato ...... 0.1 12/31/13 Clover, hay ...... 0.1 Rapeseed, seed ...... 0.2 12/31/13 Corn, field, forage ...... 0 .08 Rice, grain ...... 1.0 12/31/13 Corn, field, grain ...... 0 .08 Soybean, hay ...... 1.0 12/31/13 Corn, field, stover ...... 0 .08 Soybean, seed ...... 0.1 12/31/13 Corn, pop, grain ...... 0.08 Sunflower, seed ...... 0.2 12/31/13

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Expiration/ Expiration/ Commodity Parts per Revocation Commodity Parts per Revocation million date million Date

Sweet potato, roots ...... 0.1 12/31/13 Cotton, undelinted seed, Walnut ...... 0.1 12/31/13 postharvest ...... 200.0 10/31/11 Wheat ...... 1.0 12/31/13 Cucumber, postharvest ...... 30.0 None Cumin, seed, postharvest ...... 100.0 None (b) Section 18 emergency exemptions. Eggplant, postharvest ...... 20.0 None [Reserved] Garlic, postharvest ...... 50.0 None Ginger, postharvest ...... 100.0 None (c) Tolerances with regional registra- Grape, postharvest ...... 20.0 None tions. [Reserved] Grapefruit, postharvest ...... 30.0 None (d) Indirect or inadvertent residues. Hazelnut, postharvest ...... 200.0 None [Reserved] Horseradish, postharvest ...... 30.0 None Kumquat, postharvest ...... 30.0 None [66 FR 1245, Jan. 5, 2001, as amended at 66 FR Lemon, postharvest ...... 30.0 None 38955, July 26, 2001; 67 FR 38603, June 5, 2002; Lime, postharvest ...... 30.0 None 72 FR 35666, June 29, 2007; 73 FR 54959, Sept. Melon, honeydew, postharvest ...... 20.0 None 24, 2008; 74 FR 46372, Sept. 9, 2009; 76 FR 56652, Muskmelon, postharvest ...... 20.0 None Nectarine, postharvest ...... 20.0 None Sept. 14, 2011; 78 FR 60721, Oct. 2, 2013] Nut, brazil, postharvest ...... 200.0 None Nut, hickory, postharvest ...... 200.0 None § 180.123 Inorganic bromide residues Nut, macadamia, postharvest ...... 200.0 None resulting from fumigation with Oat, postharvest ...... 50.0 None methyl bromide; tolerances for resi- Okra, postharvest ...... 30.0 None dues. Onion, bulb, postharvest ...... 20.0 None Onion, green, postharvest ...... 20.0 None (a) General. (1) Tolerances are estab- Orange, postharvest ...... 30.0 None lished for residues of inorganic bro- Parsnip, roots, postharvest ...... 30.0 None mides (calculated as Br) in or on the Peach, postharvest ...... 20.0 None following food commodities which have Peanut, postharvest ...... 200.0 None Pear, postharvest ...... 5.0 None been fumigated with the antimicrobial Pea, blackeyed, postharvest ...... 50.0 None agent and insecticide methyl bromide Pea, postharvest ...... 50.0 None after harvest (with the exception of Pecan, postharvest ...... 200.0 None strawberry): Pepper, postharvest ...... 30.0 None Pimento, postharvest ...... 30.0 None Pineapple, postharvest ...... 20.0 None Expiration/ Commodity Parts per Revocation Pistachio, postharvest ...... 200.0 None million Date Plum, postharvest ...... 20.0 None Pomegranate, postharvest ...... 100.0 None Alfalfa, hay, postharvest ...... 50.0 10/31/11 Potato, postharvest ...... 75.0 None Almond, postharvest ...... 200.0 None Pumpkin, postharvest ...... 20.0 None Apple, postharvest ...... 5.0 None Quince, postharvest ...... 5.0 None Apricot, postharvest ...... 20.0 None Radish, postharvest ...... 30.0 None Artichoke, jerusalem, postharvest ... 30.0 None Rice, grain, postharvest ...... 50.0 None Asparagus, postharvest ...... 100.0 None Rutabaga, roots, postharvest ...... 30.0 None Avocado, postharvest ...... 75.0 None Rutabaga, tops, postharvest ...... 30.0 None Barley, grain, postharvest ...... 50.0 None Rye, grain, postharvest ...... 50.0 None Bean, lima, postharvest ...... 50.0 None Salsify, roots, postharvest ...... 30.0 None Bean, postharvest ...... 50.0 None Sorghum, grain, grain, postharvest 50.0 None Bean, snap, succulent, postharvest 50.0 None Soybean, postharvest ...... 200.0 None Bean, succulent, postharvest ...... 50.0 None Squash, summer, postharvest ...... 30.0 None Beet, garden, roots, postharvest ..... 30.0 None Beet, sugar, roots, postharvest ...... 30.0 None Squash, winter, postharvest ...... 20.0 None Blueberry, postharvest ...... 20.0 None Squash, zucchini, postharvest ...... 20.0 None Butternut, postharvest ...... 200.0 None Strawberry, postharvest ...... 60.0 None Cabbage, postharvest ...... 50.0 None Sweet potato, postharvest ...... 75.0 None Cacao bean, roasted bean, Tangerine, postharvest ...... 30.0 None postharvest ...... 50.0 None Timothy, hay, postharvest ...... 50.0 10/19/10 Cantaloupe, postharvest ...... 20.0 None Tomato, postharvest ...... 20.0 None Carrot, roots, postharvest ...... 30.0 None Turnip, roots, postharvest ...... 30.0 None Cashew, postharvest ...... 200.0 None Walnut, postharvest ...... 200.0 None Cherry, sweet, postharvest ...... 20.0 None Watermelon, postharvest ...... 20.0 None Cherry, tart, postharvest ...... 20 None Wheat ...... 50.0 None Chestnut, postharvest ...... 200.0 None Cippolini, bulb, postharvest ...... 50.0 None (2) Inorganic bromide may be present Citron, citrus, postharvest ...... 30.0 None Coconut, copra, postharvest ...... 100.0 None as a residue in certain processed food Coffee, bean, green, postharvest .... 75.0 None in accordance with the following condi- Corn, field, grain, postharvest ...... 50.0 None tions: Corn, pop, postharvest ...... 240.0 None Corn, sweet, kernel plus cob with (i) When inorganic bromide residues husks removed, postharvest ...... 50.0 None are present as a result of fumigation of

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the processed food with methyl bro- Commodity Parts per mide or from such fumigation in addi- million tion to the authorized use of methyl Ginger, postharvest ...... 100 bromide on the source raw agricultural commodity, as provided for in this (d) Indirect or inadvertent residues. part, the total residues of inorganic [Reserved] bromides (calculated as Br) shall not [71 FR 74812, Dec. 13, 2006, as amended at 75 exceed the following levels: FR 60239, Sept. 29, 2010] (A) 400 parts per million in or on egg, dried and herb, processed and spice. § 180.123a Inorganic bromide residues (B) 325 parts per million in or on in peanut hay and peanut hulls; cheese, parmesan and cheese, roquefort statement of policy. cheese. (a) Investigations by the Food and (C) 250 parts per million in or on to- Drug Administration show that peanut mato, concentrated products and fig, hay and peanut shells have been used dried fruit. as feed for meat and dairy animals. (D) 125 parts per million in or on While many growers now harvest pea- processed food other than those listed nuts with combines and leave the hay above. on the ground to be incorporated into (ii) When inorganic bromide residues the soil, some growers follow the prac- are present in malt beverage, fer- tice of curing peanuts on the vines in a mented in accordance with 21 CFR stack and save the hay for animal feed. 172.730(a)(2), the amount shall not ex- Peanut shells or hulls have been used to a minor extent as roughage for cat- ceed 25 parts per million (calculated as tle feed. It has been established that Br). the feeding to cattle of peanut hay and (iii) Where tolerances are established peanut hulls containing residues of in- on both the raw agricultural commod- organic bromides will contribute con- ities and processed food made there- siderable residues of inorganic bro- from, the total residues of inorganic mides to the meat and milk. bromides in or on the processed food (b) There are no tolerances for inor- shall not be greater than those des- ganic bromides in meat and milk to ignated in paragraph (a)(2) of this sec- cover residues from use of such peanut tion, unless a higher level is estab- hulls as animal feed. Peanut hulls con- lished elsewhere in this part. taining residues of inorganic bromides (3) Tolerances are established for res- from the use of methyl bromide are un- idues of inorganic bromides (calculated suitable as an ingredient in the feed of as Br) as follows: meat and dairy animals and should not (i) 400 parts per million for residues be represented, sold, or used for that in or on dog food, resulting from fumi- purpose. gation with methyl bromide. (ii) 125 parts per million for residues [58 FR 65555, Dec. 15, 1993] in or on processed commodities for ani- § 180.124 Methyl bromide; tolerances mal feedstuffs from barley, corn, grain for residues. sorghum, oat, rice, rye and wheat, re- (a) General. A tolerance is established sulting directly from fumigation with for residues of the fumigant methyl methyl bromide or from carryover and bromide, including metabolites and concentration of residues of inorganic degradates, in or on the commodity in bromides from fumigation of the grains the table below. Compliance with the with methyl bromide. tolerance level specified below is to be (b) Section 18 emergency exemptions. determined by measuring only methyl [Reserved] bromide. (c) Tolerances with regional registra- Parts per tions. A tolerance with regional reg- Commodity istration, as defined in § 180.1(l), is es- million tablished for residues of inorganic bro- Cotton, undelinted seed ...... 150 mides (calculated as Br) in or on the following food commodity grown in (b) Section 18 emergency exemptions. soil fumigated with methyl bromide. [Reserved]

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(c) Tolerances with regional registra- Commodity Parts per tions. [Reserved] million (d) Indirect or inadvertent residues. Rye, postharvest ...... 20 [Reserved] Sheep, fat ...... 0 .1 Sheep, meat ...... 0.1 [77 FR 35298, June 13, 2012] Sheep, meat byproducts ...... 0 .1 Sorghum, grain, postharvest ...... 8 § 180.127 Piperonyl butoxide; toler- Sweet potato, postharvest ...... 0 .25 ances for residues. Tomato, postharvest ...... 8 (a) General. (1) Tolerances for resi- Walnut, postharvest ...... 8 Wheat, postharvest ...... 20 dues of the insecticide piperonyl butoxide [(butyl carbityl)(6-propyl (2) Piperonyl butoxide may be safely piperonyl)ether] are established in or used in accordance with the following on the following food commodities: prescribed conditions: Parts per (i) It is used or intended for use in Commodity million combination with pyrethrins for con- trol of insects: Almond, postharvest ...... 8 Apple, postharvest ...... 8 (A) In cereal grain mills and in stor- Barley, postharvest ...... 20 age areas for milled cereal grain prod- Bean, postharvest ...... 8 ucts, whereby the amount of piperonyl Birdseed, mixtures, postharvest ...... 20 Blackberry, postharvest ...... 8 butoxide is at least equal to but not Blueberry, postharvest ...... 8 more than 10 times the amount of Boysenberry, postharvest ...... 8 pyrethrins in the formulation. Buckwheat, grain, postharvest ...... 20 Cattle, fat ...... 0.1 (B) On the outer ply of multiwall Cattle, meat ...... 0 .1 paper bags of 50 pounds or more capac- Cattle, meat byproducts ...... 0.1 ity in amounts not exceeding 60 milli- Cherry, sweet, postharvest ...... 8 Cherry, tart, postharvest ...... 8 grams per square foot, whereby the Cacoa bean, roasted bean, postharvest ...... 8 amount of piperonyl butoxide is equal Coconut, copra, postharvest ...... 8 to 10 times the amount of pyrethrins in Corn, field, grain, postharvest ...... 20 the formulation. Such treated bags are Corn, pop, postharvest ...... 20 Cotton, undelinted seed, postharvest ...... 8 to be used only for food, dried. Crabapple, postharvest ...... 8 (C) On cotton bags of 50 pounds or Currant, postharvest ...... 8 more capacity in amounts not exceed- Dewberry, postharvest ...... 8 Egg ...... 1 ing 55 milligrams per square foot of Fig, postharvest ...... 8 cloth, whereby the amount of piperonyl Flax, seed, postharvest ...... 8 butoxide is equal to 10 times the Goat, fat ...... 0 .1 Goat, meat ...... 0.1 amount of pyrethrins in the formula- Goat, meat byproducts ...... 0 .1 tion. Such treated bags are constructed Gooseberry, postharvest ...... 8 with waxed paper liners and are to be Grape, postharvest ...... 8 used only for food, dried that contain 4 Guava, postharvest ...... 8 Hog, fat ...... 0 .1 percent fat or less. Hog, meat ...... 0 .1 (D) In two-ply bags consisting of cel- Hog, meat byproducts ...... 0 .1 lophane/polyolefin sheets bound to- Horse, fat ...... 0 .1 Horse, meat ...... 0 .1 gether by an adhesive layer when it is Horse, meat byproducts ...... 0 .1 incorporated in the adhesive. The Loganberry, postharvest ...... 8 treated sheets shall contain not more Mango, postharvest ...... 8 than 50 milligrams of piperonyl Milk, fat ...... 0 .25 Muskmelon, postharvest ...... 8 butoxide per square foot (538 milli- Oat, postharvest ...... 8 grams per square meter). Such treated Orange, postharvest ...... 8 bags are to be used only for packaging Peach, postharvest ...... 8 Peanut, postharvest ...... 8 plum, prune, dried; grape, raisin; and Pea, postharvest ...... 8 other fruit, dried and are to have a Pear, postharvest ...... 8 maximum ratio of 3.12 milligrams of Pineapple, postharvest ...... 8 piperonyl butoxide per ounce of fruit Plum, prune, fresh, postharvest ...... 8 Potato, postharvest ...... 0 .25 (0.10 milligram of piperonyl butoxide Poultry, fat ...... 3 per gram of product). Poultry, meat ...... 3 (E) In food processing and food stor- Poultry, meat byproducts ...... 3 Raspberry, postharvest ...... 8 age areas: Provided, That the food is Rice, postharvest ...... 20 removed or covered prior to such use.

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(ii) It is used or intended for use in piperonyl butoxide is equal to 10 times combination with pyrethrins and N- the amount of pyrethrins in the formu- octylbicycloheptene dicarboximide for lation. Such treated bags are to be used insect control in accordance with 21 only for feed, dried. CFR 178.3730. (iii) A tolerance of 10 parts per mil- (iii) A tolerance of 10 parts per mil- lion is established for residues of lion is established for residues of piperonyl butoxide when present as the piperonyl butoxide in or on: result of migration: (A) Grain, cereal, milled fractions (A) In or on feed, dried from its use when present therein as a result of its on the outer ply of multiwall paper use in cereal grain mills and in storage bags of 50 pounds or more capacity. areas for milled cereal grain products. (B) In or on feed, dried that contain (B) Food, dried when present as a re- 4 percent fat, or less, from its use on sult of migration from its use on the cotton bags of 50 pounds or more capac- outer ply of multiwall paper bags of 50 ity constructed with waxed paper lin- pounds or more capacity. ers. (C) Food treated in accordance with (iv) To assure safe use of the pes- 21 CFR 178.3730. ticide, its label and labeling shall con- (D) Food, dried that contain 4 per- form to that registered with the U.S. cent fat, or less, when present as a re- Environmental Protection Agency. sult of migration from its use on the (v) Where tolerances are established cloth of cotton bags of 50 pounds or on both the raw agricultural commod- more capacity constructed with waxed ities and food, processed made there- paper liners. from, the total residues of piperonyl (E) Food treated in accordance with butoxide in or on the processed food paragraph (a)(2)(i)(D) and (E) of this shall not be greater than that per- section. mitted by the larger of the two toler- (iv) To assure safe use of the pes- ances. ticide, its label and labeling shall con- (b) Section 18 emergency exemptions. form to that registered with the U.S. [Reserved] Environmental Protection Agency, and (c) Tolerances with regional registra- it shall be used in accordance with tions. [Reserved] such label and labeling. (d) Indirect or inadvertent residues. (v) Where tolerances are established [Reserved] on both raw agricultural commodities [71 FR 74813, Dec. 13, 2006] and processed food made therefrom, the total residues of piperonyl butoxide in § 180.128 Pyrethrins; tolerances for or on the processed food shall not be residues. greater than that permitted by the (a) General. (1) Tolerances for resi- larger of the two tolerances. dues of the insecticide pyrethrins ((1S)- (3) Piperonyl butoxide may be safely 2-methyl-4-oxo-3-(2Z)-2,4- used in accordance with the following pentadienylcyclopenten-1-yl (1R,3R)- prescribed conditions: 2,2-dimethyl-3-(2-methyl-1-pro- (i) It is used or intended for use in penyl)cyclopropanecarboxylate (pyre- combination with pyrethrins for con- thrin 1), (1S)-2-methyl-4-oxo-3-(2Z)-2,4- trol of insects: pentadienyl-2-cyclopenten-1-yl (1R,3R)- (A) On the outer ply of multiwall 3-[(1E)-3-methoxy-2-methyl-3-oxo-1-pro- paper bags of 50 pounds or more capac- penyl]-2,2-dimethylcyclopropane- ity in amounts not exceeding 60 milli- carboxylate ( 2), (1S)-3-(2Z)-2- grams per square foot. butenyl-2-methyl-4-oxo-2-cyclopenten- (B) On cotton bags of 50 pounds or 1-yl (1R,3R)-2,2-dimethyl-3-(2-methyl-1- more capacity in amounts not exceed- propenyl)cyclopropanecarboxylate ing 55 milligrams per square foot of (cinerin 1), (1S)-3-(2Z)-2-butenyl-2- cloth. Such treated bags are con- methyl-4-oxo-2-cyclopenten-1-yl structed with waxed paper liners and (1R,3R)-3-[(1E)-3-methoxy-2-methyl-3- are to be used only for feed, dried that oxo-1-propenyl]-2,2- contain 4 percent fat or less. dimethylcyclopropanecarboxylate (ii) It is used in combination with (cinerin 2), (1S)-2-methyl-4-oxo-3-(2Z)-2- pyrethrins, whereby the amount of pentenyl-2-cyclopenten-1-yl (1R, 3R)-

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2,2-dimethyl-3-(2-methyl-1-pro- Commodity Parts per penyl)cyclopropanecarboxylate million (jasmolin 1), and (1S)-2-methyl-4-oxo-3- Sweet potato, postharvest ...... 0 .05 (2Z)-pentenyl-2-cyclopenten-1-yl Tomato, postharvest ...... 1 .0 (1R,3R)-3-[(1E)-3-methoxy-2-methyl-3- Walnut, postharvest ...... 1.0 oxo-1-propenyl]-2,2- Wheat, grain, postharvest ...... 3 .0 dimethylcyclopropanecarboxylate (2) A tolerance of 1.0 ppm is estab- (jasmolin 2)), the insecticidally active lished for residues of the insecticide principles of Chrysanthemum pyrethrins in or on milled fractions de- cinerariaefolium, which are measured rived from grain, cereal when present as cumulative residues of pyrethrin 1, as a result of its use in cereal grain cinerin 1, and jasmolin 1 are not to ex- mills and in storage areas for milled ceed the following: cereal grain products. Parts per (3) A tolerance of 1.0 ppm is estab- Commodity million lished for residues of the insecticide pyrethrins in or on all food items in Almond, postharvest ...... 1 .0 Apple, postharvest ...... 1 .0 food handling establishments where Barley, grain, postharvest ...... 3 .0 food and food products are held, proc- Bean, succulent, postharvest ...... 1.0 essed, prepared and/or served. Food Birdseed, mixtures, postharvest ...... 3 .0 Blackberry, postharvest ...... 1 .0 must be removed or covered prior to Blueberry, postharvest ...... 1 .0 use. Boysenberry, postharvest ...... 1 .0 (4) Where tolerances are established Buckwheat, grain, postharvest ...... 3 .0 Cacao bean, roasted bean, postharvest ...... 1.0 on both the raw agricultural commod- Cattle, fat ...... 1.0 ities and processed foods made there- Cattle, meat ...... 0 .05 from, the total residues of pyrethrins Cattle, meat byproducts ...... 0.05 Cherry, sweet, postharvest ...... 1 .0 in or on the processed food shall not be Cherry, tart, postharvest ...... 1 .0 greater than that permitted by the Coconut, copra, postharvest ...... 1 .0 larger of the two tolerances. Corn, field, grain, postharvest ...... 3 .0 (b) Section 18 emergency exemptions. Corn, pop, grain, postharvest ...... 3 .0 Cotton, undelinted seed, postharvest ...... 1.0 [Reserved] Crabapple, postharvest ...... 1 .0 (c) Tolerances with regional registra- Currant, postharvest ...... 1 .0 tions. [Reserved] Dewberry, postharvest ...... 1 .0 Fig, postharvest ...... 1 .0 (d) Indirect or inadvertent residues. Flax, seed, postharvest ...... 1 .0 [Reserved] Goat, fat ...... 1 .0 Goat, meat ...... 0.05 [71 FR 74814, Dec. 13, 2006, as amended at 73 Goat, meat byproducts ...... 0 .05 FR 5108, Jan. 29, 2008] Gooseberry, postharvest ...... 1 .0 Grape, postharvest ...... 1 .0 § 180.129 o-Phenylphenol and its so- Guava, postharvest ...... 1 .0 Hog, fat ...... 1 .0 dium salt; tolerances for residues. Hog, meat ...... 0 .05 (a) General. Tolerances are estab- Hog, meat byproducts ...... 0 .05 Horse, fat ...... 1 .0 lished for combined residues of the fun- Horse, meat ...... 0 .05 gicide o-phenylphenol and sodium o- Horse, meat byproducts ...... 0 .05 phenylphenate, each expressed as o- Loganberry, postharvest ...... 1 .0 phenylphenol, from postharvest appli- Mango, postharvest ...... 1 .0 Milk, fat (reflecting negligible residues in milk) ... 0 .05 cation of either in or on the following Muskmelon, postharvest ...... 1.0 food commodities: Oat, grain, postharvest ...... 1 .0 Orange, postharvest ...... 1.0 Parts per Pea, dry, seed, postharvest ...... 1 .0 Commodity million Peach, postharvest ...... 1.0 Peanut, postharvest ...... 1 .0 Apple ...... 25 Pear, postharvest ...... 1.0 Cantaloupe (NMT 10 ppm in edible portion) ...... 125 Pineapple, postharvest ...... 1 .0 Carrot, roots ...... 20 Plum, prune, fresh, postharvest ...... 1 .0 Cherry ...... 5 Potato, postharvest ...... 0 .05 Citrus fruits ...... 10 Raspberry, postharvest ...... 1.0 Cucumber ...... 10 Rice, grain, postharvest ...... 3 .0 Lemon ...... 10 Rye, grain, postharvest ...... 3 .0 Nectarine ...... 5 Sheep, fat ...... 1 .0 Orange ...... 10 Sheep, meat ...... 0.05 Pepper, bell ...... 10 Sheep, meat byproducts ...... 0 .05 Peach ...... 20 Sorghum, grain, grain, postharvest ...... 1.0 Pear ...... 25 .0

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(d) Indirect or inadvertent residues. Commodity Parts per million [Reserved] Pineapple ...... 10 [67 FR 49615, July 31, 2002, as amended at 74 Plum, prune, fresh ...... 20 FR 48391, Sept. 23, 2009; 79 FR 8301, Feb. 12, Sweet potato, roots ...... 15 2014; 79 FR 18822, Apr. 4, 2014; 80 FR 16306, Tomato ...... 10 Mar. 27, 2015; 80 FR 35252, June 19, 2015]

(b) Section 18 emergency exemptions. § 180.142 2,4-D; tolerances for residues. [Reserved] (a) General. Tolerances are estab- (c) Tolerances with regional registra- lished for residues of the herbicide, tions. [Reserved] plant regulator, and fungicide 2,4-D, in- (d) Indirect or inadvertent residues. cluding its metabolites and degradates, [Reserved] in or on the commodities in the table below. Compliance with the tolerance [73 FR 54960, Sept. 24, 2008] levels is to be determined by meas- § 180.130 Hydrogen Cyanide; toler- uring residues of 2,4-D (2,4- ances for residues. dichlorophenoxyacetic acid), both free and conjugated, determined as the (a) General. A tolerance for residues acid, in or on the following commod- of the insecticide hydrogen cyanide ities: from postharvest fumigation as a re- sult of application of sodium cyanide is Parts per Commodity million established as follows: 50 parts per mil- lion in or on Fruit, citrus. Almond hulls ...... 0 .1 Asparagus ...... 5.0 (b) Section 18 emergency exemptions. Barley, bran ...... 4 .0 [Reserved] Barley, grain ...... 2 .0 Barley, straw ...... 50 (c) Tolerances with regional registra- Berry, group 13 ...... 0 .2 tions. [Reserved] Cattle, fat ...... 0.3 (d) Indirect or inadvertent residues. Cattle, kidney ...... 4 .0 Cattle, meat ...... 0 .3 [Reserved] Cattle, meat byproducts, except kidney ...... 0.3 Corn, field, forage ...... 6 .0 [64 FR 39077, July 21, 1999] Corn, field, grain ...... 0 .05 Corn, field, stover ...... 50 § 180.132 Thiram; tolerances for resi- Corn, pop, grain ...... 0.05 dues. Corn, pop, stover ...... 50 Corn, sweet, forage ...... 6 .0 (a) General. Tolerances for residues of Corn, sweet, kernel plus cob with husks re- moved ...... 0 .05 the fungicide thiram (tetramethyl Corn, sweet, stover ...... 50 thiuram disulfide), including its me- Cranberry ...... 0 .5 tabolites and degradates, in or on the Fish ...... 0 .1 Fruit, citrus, group 10 ...... 3 .0 commodities in the table below. Com- Fruit, pome, group 11 ...... 0.05 pliance with the tolerance levels speci- Fruit, stone, group 12 ...... 0 .05 fied is to be determined by measuring Goat, fat ...... 0 .3 Goat, kidney ...... 4 .0 only thiram. Goat, meat ...... 0.3 Goat, meat byproducts, except kidney ...... 0 .3 Grain, aspirated fractions ...... 40 Commodity Parts per million Grape ...... 0 .05 Grass, forage ...... 360 Apple ...... 7.0 Grass, hay ...... 300 Avocado 1 ...... 15 Hop, dried cones ...... 0 .2 Banana 1 ...... 0.80 Horse, fat ...... 0 .3 Peach ...... 7 .0 Horse, kidney ...... 4 .0 Horse, meat ...... 0 .3 Strawberry ...... 20 Horse, meat byproducts, except kidney ...... 0 .3 1 No U.S. registrations as of September 23, 2009. Millet, forage ...... 25 Millet, grain ...... 2 .0 (b) Section 18 emergency exemptions. Millet, straw ...... 50 [Reserved] Milk ...... 0.05 Nut, tree, group 14 ...... 0 .2 (c) Tolerances with regional registra- Oat, forage ...... 25 tions. [Reserved] Oat, grain ...... 2 .0 Oat, straw ...... 50 Pistachio ...... 0.05 Potato ...... 0 .4

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acid, in or on the following commod- Commodity Parts per million ities: Rice, grain ...... 0 .5 Parts per Rice, hulls ...... 2 .0 Commodity million Rice, straw ...... 10 Rye, bran ...... 4 .0 Animal feed, nongrass, group 18 ...... 0 .2 Rye, forage ...... 25 Avocado ...... 0 .05 Rye, grain ...... 2.0 Cotton, undelinted seed ...... 0 .05 Rye, straw ...... 50 Dill, seed ...... 0 .05 Sheep, fat ...... 0 .3 Okra ...... 0.05 Sheep, kidney ...... 4.0 Vegetable, brassica leafy, group 5 ...... 0 .4 Sheep, meat ...... 0.3 Vegetable, bulb, group 3 ...... 0 .05 Sheep, meat byproducts, except kidney ...... 0 .3 Vegetable, cucurbit, group 9 ...... 0.05 Shellfish ...... 1 .0 Vegetable, foliage of legume, group 7 ...... 0 .2 Sorghum, grain, forage ...... 0.2 Vegetable, fruiting, group 8 ...... 0.05 Sorghum, grain, grain ...... 0 .2 Vegetable, leafy, except brassica, group 4 ...... 0 .4 Sorghum, grain, stover ...... 0 .2 Vegetable, legume, group 6 ...... 0 .05 Soybean, forage ...... 0 .02 Soybean, hay ...... 2 .0 Soybean, seed ...... 0 .02 [72 FR 52017, Sept. 12, 2007, as amended at 73 Strawberry ...... 0 .05 FR 53737, Sept. 17, 2008; 74 FR 48411, Sept. 23, Sugarcane, cane ...... 0.05 Sugarcane, molasses ...... 0 .2 2009; 76 FR 55817, Sept. 9, 2011] Teff, bran ...... 4.0 Teff, forage ...... 25.0 § 180.145 Fluorine compounds; toler- Teff, grain ...... 2 .0 ances for residues. Teff, straw ...... 50 .0 Vegetable, leaves of root and tuber, group 2 ..... 0 .1 (a) General. (1) Tolerances are estab- Vegetable, root and tuber, except potato, group lished for combined residues of the in- 1 ...... 0 .1 secticidal fluorine compounds cryolite Wheat, bran ...... 4.0 Wheat, forage ...... 25 and synthetic cryolite (sodium alu- Wheat, grain ...... 2 .0 minum fluoride) in or on the following Wheat, straw ...... 50 agricultural commodities:

(b) Section 18 emergency exemptions. Commodity Parts per [Reserved] million (c) Tolerances with regional registra- Apricot ...... 7 tions. Tolerances with regional reg- Blackberry ...... 7 istration, as defined in § 180.1(l), are es- Blueberry ...... 7 Boysenberry ...... 7 tablished for residues of the herbicide, Broccoli ...... 7 plant regulator, and fungicide 2,4-D, in- Brussels sprouts ...... 7 cluding its metabolites and degradates, Cabbage ...... 7 in or on the commodities in the table Cauliflower ...... 7 Collards ...... 7 below. Compliance with the tolerance Cranberry ...... 7 levels is to be determined by meas- Cucumber ...... 7 uring residues of 2,4-D (2,4- Dewberry ...... 7 dichlorophenoxyacetic acid), both free Eggplant ...... 7 Fruit, citrus ...... 7 and conjugated, determined as the Grape ...... 7 acid, in or on the follow commodities: Kale ...... 7 Kohlrabi ...... 7 Commodity Parts per Lettuce, head ...... 7 million Lettuce, leaf ...... 7 Loganberry ...... 7 Rice, wild, grain ...... 0.05 Melon ...... 7 Nectarine ...... 7 (d) Indirect or inadvertent residues. Peach ...... 7 Tolerances are established for indirect Pepper ...... 7 or inadvertent residues of the herbi- Plum, prune, fresh ...... 7 Pumpkin ...... 7 cide, plant regulator, and fungicide 2,4- Raspberry ...... 7 D, including its metabolites and Squash, summer ...... 7 degradates, in or on the commodities Squash, winter ...... 7 Strawberry ...... 7 in the table below. Compliance with Tomato ...... 7 the tolerances levels is to be deter- Youngberry ...... 7 mined by measuring residues of 2,4-D (2,4-dichlorophenoxyacetic acid), both (2) Tolerances are established for res- free and conjugated, determined as the idues of fluoride in or on the following

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commodities from the postharvest fu- (d) Indirect or inadvertent residues. migation with sulfuryl fluoride for the [Reserved] control of insects: [71 FR 74815, Dec. 13, 2006, as amended at 76 Parts per FR 34885, June 15, 2011] Commodity million § 180.151 Ethylene oxide; tolerances All processed food commodities not otherwise for residues. listed ...... 70 Barley, bran, postharvest ...... 45 .0 (a) General. (1) Tolerances are estab- Barley, flour, postharvest ...... 45.0 lished for residues of the antimicrobial Barley, grain, postharvest ...... 15 .0 agent and insecticide ethylene oxide, Barley, pearled barley, postharvest ...... 45.0 Cattle, meat, dried ...... 40 when used as a postharvest fumigant in Cheese ...... 5 .0 or on the following food commodities: Cacao bean, roasted bean, postharvest ...... 20 Coconut, postharvest ...... 40 Commodity Parts per Coffee, bean, green, postharvest ...... 15 million Corn, field, flour, postharvest ...... 35 .0 Corn, field, grain, postharvest ...... 10.0 Herb and spice, group 19, dried, except basil .... 7 Corn, field, grits, postharvest ...... 10.0 Licorice, roots ...... 7 Corn, field, meal, postharvest ...... 30 .0 Peppermint, tops, dried ...... 7 Sesame, seed ...... 7 Corn, pop, grain, postharvest ...... 10 .0 Spearmint, tops, dried ...... 7 Cotton, undelinted seed, postharvest ...... 70 Vegetable, dried ...... 7 Egg, dried ...... 900 Walnut ...... 50 Fruit, dried, except grape, raisin, postharvest ..... 3 .0 Ginger, postharvest ...... 70 Grain, aspirated fractions, postharvest ...... 55 .0 (2) Tolerances are established for res- Grape, raisin, postharvest ...... 7 .0 idues of the ethylene oxide reaction Hog, meat ...... 20 product, 2-chloroethanol, commonly Herbs and spices group 19, postharvest ...... 70 Milk, powdered ...... 5 .0 referred to as ethylene chlorohydrin, Millet, grain, postharvest ...... 40.0 when ethylene oxide is used as a Nut, pine, postharvest ...... 20 postharvest fumigant in or on food Nut, tree, Group 14, postharvest ...... 10 .0 commodities as follows: Oat, flour, postharvest ...... 75 .0 Oat, grain, postharvest ...... 25 .0 Parts per Oat, groats/rolled oats ...... 75 .0 Commodity million Peanut, postharvest ...... 15 Pistachio, postharvest ...... 10 .0 Herb and spice, group 19, dried, except basil .... 940 Rice, bran, postharvest ...... 31 .0 Licorice, roots ...... 940 Rice, flour, postharvest ...... 45 Peppermint, tops, dried ...... 940 Rice, grain, postharvest ...... 12.0 Sesame, seed ...... 940 Rice, hulls, postharvest ...... 35.0 Spearmint, tops, dried ...... 940 Rice, polished rice, postharvest ...... 25.0 Vegetable, dried ...... 940 Rice, wild, grain, postharvest ...... 25 .0 Sorghum, grain, postharvest ...... 40.0 (b) Section 18 emergency exemptions. Triticale, grain, postharvest ...... 40.0 Vegetable, legume, group 6, postharvest ...... 70 [Reserved] Wheat, bran, postharvest ...... 40 .0 (c) Tolerances with regional registra- Wheat, flour, postharvest ...... 125 .0 tions. [Reserved] Wheat, germ, postharvest ...... 130 .0 (d) Indirect or inadvertent residues. Wheat, grain, postharvest ...... 40.0 Wheat, milled byproducts, postharvest ...... 130.0 [Reserved] Wheat, shorts, postharvest ...... 40.0 [65 FR 33695, May 24, 2000, as amended at 74 FR 46696, Sept. 11, 2009] (b) Section 18 emergency exemptions. [Reserved] § 180.153 Diazinon; tolerances for resi- (c) Tolerances with regional registra- dues. tions. Tolerances with regional reg- (a) General. Tolerances are estab- istration, as defined by § 180.1(l), are es- lished for residues of the insecticide tablished for the combined residues of diazinon, O,O-diethyl O-[6-methyl-2-(1- the insecticidal fluorine compounds, methylethyl)-4- cryolite and synthetic cryolite (sodium pyrimidinyl]phosphorothioate (CAS aluminum fluoride), in or on the fol- No. 333–41–5), in or on the following lowing raw agricultural commodities: food commodities: Parts per Commodity million Commodity Parts per million

Kiwifruit ...... 15 Almond, hulls ...... 3.0 Apple ...... 0.50

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Commodity Parts per million (d) Indirect or inadvertent residues. [Reserved] Apricot ...... 0.20 Bean, lima ...... 0.50 [47 FR 42738, Sept. 29, 1982] Bean, snap, succulent ...... 0.50 Beet, garden, roots ...... 0.75 EDITORIAL NOTE: For FEDERAL REGISTER ci- Beet, garden, tops ...... 0.70 tations affecting § 180.153, see the List of CFR Blueberry ...... 0.50 Sections Affected, which appears in the Caneberry subgroup 13-07A ...... 0.75 Finding Aids section of the printed volume Carrot, roots ...... 0.75 and at www.fdsys.gov. Cattle, fat ...... 0.50 Cherry, sweet ...... 0.20 Cherry, tart ...... 0.20 § 180.154 Azinphos-methyl; tolerances Cranberry ...... 0.50 for residues. Endive ...... 0.70 Fig ...... 0.50 (a) General. Tolerances for residues of Ginseng ...... 0.75 the insecticide O,O-dimethyl S-[(4-oxo- Grape ...... 0.75 2 1,2,3-benzotriazin-3(4H)- Hazelnut ...... 0.50 yl)methyl]phosphorodithioate in or on Kiwifruit 1 ...... 0.75 Lettuce ...... 0.70 the following raw agricultural com- Melon ...... 0.75 modities: Mushroom ...... 0.75 2 Nectarine ...... 0.20 Parts per Expiration/ Onion, bulb ...... 0.75 Commodity million Revocation Onion, green ...... 0.75 Date Pea, succulent ...... 0.50 Peach ...... 0.20 Almond1 ...... 0.2 None Pear ...... 0.50 Almond, hulls1 ...... 5.0 None Pineapple ...... 0.50 Apple2 ...... 1.5 None Plum, prune, fresh ...... 0.20 Blackberry3 ...... 2.0 None Radish ...... 0.50 Blueberry2 ...... 5.0 None Rutabaga ...... 0.75 Boysenberry3 ...... 2.0 None Spinach ...... 0.70 Brussels sprouts4 ...... 2.0 None Strawberry ...... 0.50 Cherry2 ...... 2.0 None Tomato ...... 0.75 Crabapple2 ...... 1.5 None Vegetable, brassica, leafy, group 5 0.70 Cranberry3 ...... 0.5 12/31/12 Watercress ...... 0.05 Loganberry3 ...... 2.0 None 1There are no domestic registrations for kiwifruit as of Parsley, leaves2 ...... 5.0 None March 6, 2002. Parsley, turnip rooted, roots2 ...... 2.0 None 2The expiration/revocation date for this tolerance is 9/10/ 2010. Peach3 ...... 2.0 None Pear2 ...... 1.5 None (b) Section 18 emergency exemptions. Pistachio1 ...... 0.3 None [Reserved] Plum, prune5 ...... 2.0 None (c) Tolerances with regional registra- Quince5 ...... 1.5 None tions. Tolerances with regional reg- Raspberry3 ...... 2.0 None 1 istration, as defined in § 180.1(l), are es- Walnut ...... 0.3 None tablished for residues of the insecticide 1There are no U.S. registrations as of diazinon, O, O-diethyl O-[6-methyl-2-(1- methylethyl)-4-pyrimidinyl]- October 30, 2009. 2 phosphorothioate (CAS No. 333–41–5), in There are no U.S. registrations as of or on the following food commodities: September 30, 2012. 3There are no U.S. registrations since Parts per September 30, 2006. Commodity million 4There are no U.S. registrations since Almond ...... 0.50 September 30, 2008. Banana ...... 0.20 5There are no U.S. registrations since Celery ...... 0 .70 Cucumber ...... 0 .75 December 28, 2005. Parsley, leaves ...... 0.75 (b) Section 18 emergency exemptions. Parsnip ...... 0.50 [Reserved] Pepper ...... 0 .5 Potato ...... 0 .10 (c) Tolerances with regional registra- Squash, summer ...... 0 .50 tions. [Reserved] Squash, winter ...... 0 .75 (d) Indirect or inadvertent residues. Sweet potato, roots ...... 0 .10 Swiss chard ...... 0.70 [Reserved] Turnip, roots ...... 0 .50 [65 FR 38752, June 22, 2000, as amended at 74 Turnip, tops ...... 0.75 FR 46697, Sept. 11, 2009]

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§ 180.155 1-Naphthaleneacetic acid; tol- Expiration/ Commodity Parts per revocation erances for residues. million date (a) General. Tolerances are estab- Chestnut ...... 0.1 10/31/16 lished for the residues of 1- Citrus, dried pulp ...... 12.0 10/31/16 naphthaleneacetic acid, including its Citrus oil ...... 200.0 10/31/16 metabolites and degradates in or on Cotton, refined oil ...... 0.5 10/31/16 the commodities in the following table. Cotton, undelinted seed ...... 0.1 10/31/16 Fruit, citrus, group 10 ...... 6.0 10/31/16 Compliance with the tolerance levels Fruit, pome, group 11 ...... 10.0 10/31/16 specified is to be determined by meas- Fruit, stone, group 12 ...... 5.0 10/31/16 uring only 1-naphthaleneacetic acid Grape ...... 5.0 10/31/16 Grape, raisin ...... 20.0 10/31/16 and its conjugates, calculated as the Hazelnut ...... 0.1 10/31/16 Stoichiometric equivalent of 1- Hop, dried cones ...... 65.0 10/31/16 naphthaleneacetic acid, in or on the Nut, hickory ...... 0.1 10/31/16 Nut, macadamia ...... 0.1 10/31/16 commodity. Pecan ...... 0.1 10/31/16 Peppermint, oil ...... 30.0 10/31/16 Commodity Parts per Peppermint, tops ...... 25.0 10/31/16 million Spearmint, oil ...... 30.0 10/31/16 Spearmint, tops ...... 25.0 10/31/16 Avocado ...... 0 .05 Strawberry ...... 10.0 10/31/16 Cherry, sweet ...... 0 .1 Fruit, pome, group 11–10 ...... 0 .15 Tea, dried ...... 50.0 None Mango ...... 0.05 Tea, plucked leaves ...... 30.0 None Olive ...... 0 .7 Vegetable, cucurbit, group 9 ...... 2.0 10/31/16 Orange ...... 0 .1 Vegetable, fruiting, group 8 ...... 2.0 10/31/16 Pineapple1 ...... 0 .05 Walnut ...... 0.1 10/31/16 Potato ...... 0 .01 Rambutan ...... 2 .0 (2) Tolerances are established for res- Sapote, mamey ...... 0 .05 idues of the insecticide dicofol, includ- Tangerine ...... 0 .1 ing its metabolites and degradates, in 1 There are no U.S. registrations since 1988. or on the commodities in the table in (b) Section 18 emergency exemptions. this paragraph. Compliance with the [Reserved] tolerance levels specified in this para- (c) Tolerances with regional registra- graph is to be determined by measuring tions. [Reserved] only the sum of p,p-dicofol, 4-chloro-a- (d) Indirect or inadvertent residues. (4-chlorophenyl)-a- [Reserved] (trichloromethyl)benzenemethanol, its isomer o,p-dicofol, 2-chloro- -(4- [78 FR 30218, May 22, 2013] a chlorophenyl)-a- § 180.163 Dicofol; tolerances for resi- (trichloromethyl)benzenemethanol, dues. and its metabolites 4-chloro-a-(4- (a) General. (1) Tolerances are estab- chlorophenyl)-a- lished for residues of the insecticide (dichloromethyl)benzenemethanol and dicofol, including its metabolites and 2-chloro-a-(4-chlorophenyl)-a- degradates, in or on the commodities (dichloromethyl)benzenemethanol, cal- in the table in this paragraph. Compli- culated as the stoichiometric equiva- ance with the tolerance levels specified lent of p,p-dicofol, 4-chloro-a-(4- in this paragraph is to be determined chlorophenyl)-a- by measuring only dicofol as the sum (trichloromethyl)benzenemethanol, in of its p,p-dicofol and o,p-dicofol iso- or on the commodity. mers: 4-chloro-a-(4-chlorophenyl)-a- Parts per Expiration/ (trichloromethyl)benzenemethanol and Commodity million Revocation 2-chloro-a-(4-chlorophenyl)-a- Date (trichloromethyl)benzenemethanol, in Cattle, fat ...... 50.0 10/31/16 or on the commodity. Cattle, liver ...... 5.0 10/31/16 Cattle, meat ...... 3.0 10/31/16 Expiration/ Cattle, meat byproducts, except Parts per liver ...... 3.0 10/31/16 Commodity million revocation date Egg ...... 0.05 10/31/16 Goat, fat ...... 50.0 10/31/16 Apple, wet pomace ...... 38.0 10/31/16 Goat, liver ...... 5.0 10/31/16 Bean, dry, seed ...... 0.5 10/31/16 Goat, meat ...... 3.0 10/31/16 Bean, succulent ...... 3.0 10/31/16 Goat, meat byproducts, except liver 3.0 10/31/16 Butternut ...... 0.1 10/31/16 Hog, fat ...... 50.0 10/31/16 Caneberry subgroup 13A ...... 5.0 10/31/16 Hog, liver ...... 5.0 10/31/16

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Expiration/ Expiration/ Commodity Parts per Revocation Commodity Parts per revocation million Date million date

Hog, meat ...... 3.0 10/31/16 Dandelion, leaves ...... 22 None Hog, meat byproducts, except liver 3.0 10/31/16 Endive ...... 10 None Horse, fat ...... 50.0 10/31/16 Flax, seed ...... 0.5 None Horse, liver ...... 5.0 10/31/16 Fruit, citrus, group 10 ...... 10 None Horse, meat ...... 3.0 10/31/16 Fruit, pome, group 11 ...... 12 None Horse, meat byproducts, except Fruit, stone, group 12 ...... 10 None liver ...... 3.0 10/31/16 Grain, aspirated fractions ...... 70 None Milk, fat (reflecting 0.75 ppm in Grape ...... 10 None whole milk) ...... 22.0 10/31/16 Grape, raisin ...... 12 None Poultry, fat ...... 0.1 10/31/16 Grass, forage ...... 100 None Poultry, meat ...... 0.1 10/31/16 Grass, hay ...... 15 None Poultry, meat byproducts ...... 0.1 10/31/16 Leaf petiole subgroup 4B ...... 3.0 None Sheep, fat ...... 50.0 10/31/16 Lettuce ...... 10 None Sheep, liver ...... 5.0 10/31/16 Millet, proso, grain ...... 1.0 None Sheep, meat ...... 3.0 10/31/16 Millet, proso, straw ...... 20 None Sheep, meat byproducts, except Nut, tree group 14, except walnut ... 0.1 None liver ...... 3.0 10/31/16 Okra ...... 4.0 None Olive ...... 10 None Oyster ...... 0.25 None (b) Section 18 emergency exemptions. Parsley, leaves ...... 22 None [Reserved] Pea and bean, dried shelled, except (c) Tolerances with regional registra- soybean, subgroup 6C ...... 1.0 None Peanut ...... 0.05 None tions. [Reserved] Peanut, hay ...... 20 None (d) Indirect or inadvertent residues. Pineapple ...... 2.0 None [Reserved] Pistachio ...... 0.1 None Rice, grain ...... 15 None [63 FR 34826, June 26, 1998, as amended at 72 Rice, hulls ...... 30 None Rice, straw ...... 60 None FR 35665, June 29, 2007; 72 FR 41928, Aug. 1, Sorghum grain, forage ...... 30 None 2007; 77 FR 59124, Sept. 26, 2012] Sorghum grain, grain ...... 10 None Sorghum grain, stover ...... 30 None § 180.169 Carbaryl; tolerances for resi- Soybean, forage ...... 15 None dues. Soybean, hay ...... 15 None Soybean, seed ...... 0.5 None (a) General. (1) Tolerances are estab- Spinach ...... 22 None lished for residues of the insecticide Strawberry ...... 4.0 None Sunflower, seed ...... 0.5 None carbaryl, 1-naphthyl N- Sweet potato, roots ...... 0.2 None methylcarbamate per se, in or on the Trefoil, forage ...... 15 None following food commodities: Trefoil, hay ...... 25 None Vegetable, brassica, leafy, group 5, Expiration/ except cabbage ...... 10 None Parts per Vegetable, cucurbit, group 9 ...... 3.0 None Commodity million revocation date Vegetable, foliage of legume, sub- group 7A, except soybean ...... 60 None Alfalfa, forage ...... 50 None Vegetable, fruiting, group 8 ...... 5.0 None Alfalfa, hay ...... 75 None Vegetable, leaves of root and tuber, Almond, hulls ...... 50 None group 2, except sugar beet tops 75 None Apple, wet pomace ...... 15 None Vegetable, legume, edible podded, Asparagus ...... 15 None subgroup 6A ...... 10 None Banana ...... 5.0 None Vegetable, root and tuber, group 1, Beet, sugar, roots ...... 0.5 None except sugar beet and sweet po- Beet, sugar, tops ...... 25 None tato ...... 2.0 None Bushberry subgroup 13-07B ...... 3.0 None Walnut ...... 1.0 None Cabbage ...... 21 None Wheat, forage ...... 30 None Cactus, fruit ...... 5.0 None Wheat, grain ...... 1.0 None Cactus, pads ...... 12 None Wheat, hay ...... 30 None Caneberry subgroup 13-07A ...... 12.0 None Wheat, straw ...... 20 None Citrus, oil ...... 20 None Clover, forage ...... 50 None (2) Tolerances are established for res- Clover, hay ...... 70 None Corn, field, forage ...... 30 None idues of the insecticide carbaryl, 1- Corn, field, grain ...... 0.02 None naphthyl N-methylcarbamate, includ- Corn, field, stover ...... 20 None ing its metabolites: 1-naphthol Corn, pop, grain ...... 0.02 None Corn, pop, stover ...... 20 None (naphthyl-sulfate); 5,6- Corn, sweet, forage ...... 185 None dihydrodihydroxycarbaryl; and 5,6- Corn, sweet, kernel plus cob with dihydrodihydroxy naphthol, calculated husks removed ...... 0.1 None as 1-naphthyl N-methylcarbamate and Corn, sweet, stover ...... 215 None Cotton, undelinted seed ...... 5.0 10/31/09 the free and conjugated residues of Cranberry ...... 3.0 None carbaryl: 5,6-dihydro-5,6-dihydroxy

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carbaryl and 5-methoxy-6-hydroxy Commodity Parts per million carbaryl, in or on the following food commodities: Banana ...... 0.50 Fruit, stone, crop group 12 ...... 5 .0 Expiration/ Nuts, tree, crop group 14 ...... 0 .3 Parts per Peanut ...... 0 .013 Commodity million revocation date Pear ...... 5 .0 Strawberry ...... 5 .0 Cattle, fat ...... 0.5 None Cattle, meat ...... 1.0 None Cattle, meat byproducts ...... 3.0 None (b) Section 18 emergency exemptions. Egg ...... 0.5 10/31/09 [Reserved] Goat, fat ...... 0.5 None Goat, meat ...... 1.0 None (c) Tolerances with regional registra- Goat, meat byproducts ...... 3.0 None tions. [Reserved] Hog, fat ...... 0.5 None Hog, meat ...... 1.0 None (d) Indirect or inadvertent residues. Hog, meat byproducts ...... 3.0 None [Reserved] Horse, fat ...... 0.5 None Horse, meat ...... 1.0 None [72 FR 52017, Sept. 12, 2007, as amended at 73 Horse, meat byproducts ...... 3.0 None FR 45634, Aug. 6, 2008; 77 FR 72237, Dec. 5, Milk ...... 1.0 None 2012] Poultry, fat ...... 5.0 10/31/09 Poultry, meat ...... 5.0 10/31/09 Sheep, fat ...... 0.5 None § 180.175 Maleic hydrazide; tolerances Sheep, meat ...... 1.0 None for residues. Sheep, meat byproducts ...... 3.0 None (a) General. (1) Tolerances for resi- (b) Section 18 emergency exemptions. dues of the herbicide and plant regu- [Reserved] lator maleic hydrazide (1,2-dihydro-3,6- (c) Tolerances with regional registra- pyridazinedione) are established in or tions. Tolerances with regional reg- on the following raw agricultural com- istrations, as defined in § 180.1(l), are modities: established for residues of the insecti- cide carbaryl, 1-naphthyl N- Commodity Parts per methylcarbamate per se, in or on the million following food commodities: Onion, bulb ...... 15.0 Potato ...... 50.0 Parts per Commodity million (2) A food additive known as maleic Dillweed, fresh leaves ...... 0 .2 hydrazide (1,2-dihydro-3,6- pyridazinedione) may be present in po- (d) Indirect or inadvertent residues. tato, chips when used in accordance [Reserved] with the following conditions: [65 FR 33695, May 24, 2000, as amended at 66 (i) The food additive is present as a FR 38955, July 26, 2001; 67 FR 49615, July 31, result of the application of a pesticide 2002; 70 FR 44492, Aug. 3, 2005; 73 FR 52611, Sept. 10, 2008; 74 FR 10490, Mar. 11, 2009] formulation containing maleic hydra- zide to the growing potato plant in ac- § 180.172 Dodine; tolerances for resi- cordance with directions registered by dues. the U.S. Environmental Protection (a) General. Tolerances are estab- Agency. lished for residues of the fungicide (ii) The label of the pesticide formu- dodine, including its metabolites and lation containing the food additive degradates, in or on the commodities conforms to labeling registered by the listed in the table below. Compliance U.S. Environmental Protection Agen- with the tolerance levels specified in cy. the table is to be determined by meas- (iii) The food additive is present in an uring only dodine, N-dodecylguanidine amount not to exceed 160 parts per mil- acetate; in or on the following com- lion by weight of the finished food. modities. (b) Section 18 emergency exemptions. Commodity Parts per million [Reserved] (c) Tolerances with regional registra- Almond, hull ...... 30 .0 Apple ...... 5.0 tions. [Reserved] Apple, wet pomace ...... 15.0

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(d) Indirect or inadvertent residues. Commodity Parts per [Reserved] million [62 FR 64293, Dec. 5, 1997, as amended at 64 Mango ...... 15.0 FR 11792, Mar. 10, 1999; 67 FR 35048, May 17, Oat, flour ...... 20 2002] Oat, grain ...... 5 Oat, groats/rolled oats ...... 20 Oat, straw ...... 25 § 180.176 Mancozeb; tolerances for res- Onion, bulb ...... 1 .5 idues. Papaya ...... 10 (a) General. Tolerances are estab- Peanut ...... 0 .1 Peanut, hay ...... 65 lished for residues of mancozeb (a co- Pear ...... 0 .6 ordination product of zinc ion and Pepper ...... 12 maneb (manganese Potato ...... 0 .2 ethylenebisdithiocarbamate)), includ- Poultry, kidney ...... 0 .5 Poultry, liver ...... 0 .5 ing its metabolites and degradates, in Quince ...... 0 .6 or on the commodities in the following Rice, grain ...... 0 .06 table. Compliance with the tolerance Rye, bran ...... 20 levels specified in this paragraph is to Rye, grain ...... 5 Rye, straw ...... 25 be determined by measuring only those Sapodilla ...... 15 .0 mancozeb residues convertible to and Sapote, mamey ...... 15 .0 expressed in terms of the degradate Sapote, white ...... 15 .0 carbon disulfide. Sheep, kidney ...... 0.5 Sheep, liver ...... 0.5 Sorghum, grain, forage ...... 0.15 Parts per Commodity million Sorghum, grain, grain ...... 0 .25 Sorghum, grain, stover ...... 0 .15 Almond ...... 0.1 Star apple ...... 15 .0 Almond, hulls ...... 4 Sugar apple ...... 3 .0 Apple ...... 0.6 Tangerine 1 ...... 10 Asparagus ...... 0.1 Tomato ...... 2.5 Atemoya ...... 3 .0 Vegetable, cucurbit, group 9 ...... 2.0 Banana ...... 2 Walnut ...... 0 .70 Barley, bran ...... 20 Wheat, bran ...... 20 Barley, flour ...... 20 Wheat, flour ...... 20 Barley, grain ...... 5 Wheat, germ ...... 20 Barley, pearled barley ...... 20 Wheat, grain ...... 5 Barley, straw ...... 25 Wheat, middlings ...... 20 Beet, sugar, dried pulp ...... 3 .0 Wheat, shorts ...... 20 Beet, sugar, roots ...... 1 .2 Wheat, straw ...... 25 Beet, sugar, tops ...... 60 Broccoli ...... 7 1 There are no U.S. registrations for use of mancozeb on Cabbage ...... 9 tangerine. Canistel ...... 15 .0 Cattle, kidney ...... 0 .5 (b) Section 18 emergency exemptions. Cattle, liver ...... 0 .5 [Reserved] Cherimoya ...... 3 .0 (c) Tolerances with regional registra- Corn, field, forage ...... 40 tions. A tolerance with regional reg- Corn, field, grain ...... 0 .1 Corn, field, stover ...... 15 istrations, as defined in § 180.1(l), is es- Corn, pop, grain ...... 0.1 tablished for residues of the fungicide Corn, pop, stover ...... 40 mancozeb, (a coordination product of Corn, sweet, forage ...... 70 Corn, sweet, kernel plus cob with husks re- zinc ion and maneb (manganese moved ...... 0 .1 ethylenebisdithiocarbamate)), includ- Corn, sweet, stover ...... 40 ing its metabolites and degradates, in Cotton, undelinted seed ...... 0 .5 or on the commodity in the following Crabapple ...... 0 .6 Cranberry ...... 5 table in this paragraph. Compliance Custard apple ...... 3 .0 with the tolerance levels specified in Fennel ...... 2.5 this paragraph is to be determined by Flax, seed ...... 0 .15 Ginseng ...... 1 .2 measuring only those mancozeb resi- Goat, kidney ...... 0 .5 dues convertible to and expressed in Goat, liver ...... 0.5 terms of the degradate carbon disul- Grape ...... 1 .5 fide. Hog, kidney ...... 0.5 Hog, liver ...... 0 .5 Parts per Horse, kidney ...... 0 .5 Commodity million Horse, liver ...... 0 .5 Lettuce, head ...... 3.5 Carrot, roots ...... 1 Lettuce, leaf ...... 18

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(d) Indirect or inadvertent residues. Commodity Parts per [Reserved] million [65 FR 33708, May 24, 2000, as amended at 65 Goat, meat byproducts except kidney ...... 0 .06 FR 49924, Aug. 16, 2000; 66 FR 64773, Dec. 14, Hog, fat ...... 0 .20 Hog, kidney ...... 0.30 2001; 68 FR 2247, Jan. 16, 2003; 69 FR 29458, Hog, meat ...... 0 .06 May 24, 2004; 71 FR 76199, Dec. 20, 2006; 74 FR Hog, meat byproducts except kidney ...... 0 .06 46372, Sept. 9, 2009; 75 FR 770, Jan. 6, 2010; 75 Horse, fat ...... 0 .20 FR 50913, Aug. 18, 2010; 76 FR 18915, Apr. 6, Horse, kidney ...... 0 .30 2011; 78 FR 44455, July 24, 2013; 79 FR 27501, Horse, meat ...... 0 .06 May 14, 2014] Horse, meat byproducts except kidney ...... 0.06 Milk ...... 0.30 Sheep, fat ...... 0 .20 § 180.178 Ethoxyquin; tolerances for Sheep, kidney ...... 0.30 residues. Sheep, meat ...... 0.06 (a) General. A tolerance is established Sheep, meat byproducts except kidney ...... 0 .06 for residues of the plant regulator (b) Section 18 emergency exemptions. ethoxyquin (1,2-dihydro-6-ethoxy-2,2,4- [Reserved] trimethylquinoline) from preharvest or (c) Tolerances with regional registra- postharvest use in or on the following tions. [Reserved] commodity: (d) Indirect or inadvertent residues. Parts per [Reserved] Commodity million [43 FR 52487, Nov. 13, 1978, as amended at 63 Pear ...... 3 FR 57073, Oct. 26, 1998; 72 FR 37653, July 11, 2007] (b) Section 18 emergency exemptions. [Reserved] § 180.182 Endosulfan; tolerances for (c) Tolerances with regional registra- residues. tions. [Reserved] (a)(1) General. Tolerances are estab- (d) Indirect or inadvertent residues. lished for residues of the insecticide [Reserved] endosulfan, including its metabolites and degradates, in or on the commod- [63 FR 57073, Oct. 26, 1998] ities in the table in this paragraph. § 180.181 Chlorpropham; tolerances for Compliance with the tolerance levels residues. specified in this paragraph is to be de- (a) General. (1) Tolerances are estab- termined by measuring only the sum of lished for residues of the plant regu- endosulfan, 6,7,8,9,10,10-hexachloro- lator and herbicide chlorpropham (iso- 1,5,5a,6,9,9a-hexahydro-6,9-methano- propyl m-chlorocarbanilate (CIPC) in 2,4,3-benzodioxathiepin 3-oxide (alpha or on the following food commodities: and beta isomers), and its metabolite endosulfan sulfate, 6,7,8,9,10,10- Commodity Parts per hexachloro-1,5,5a,6,9,9a-hexahydro-6,9- million methano-2,4,3-benzodioxathiepin-3,3-di- Potato ...... 30 oxide, calculated as the stoichiometric Potato, wet peel ...... 40 equivalent of endosulfan, in or on the commodity. (2) Tolerances are established for the combined residues of the plant regu- Expiration/ Commodity Parts per revocation lator and herbicide chlorpropham (iso- million date propyl m-chlorocarbanilate (CIPC) and its metabolite 4-hydroxychlorpropham- Almond ...... 0.3 7/31/12 Almond, hulls ...... 1.0 7/31/12 O-sulfonic acid (4-HSA) in or on the fol- Apricot ...... 2.0 7/31/12 lowing food commodities: Bean ...... 2.0 7/31/12 Broccoli ...... 3.0 7/31/12 Parts per Brussels sprouts ...... 2.0 7/31/12 Commodity million Cabbage ...... 4.0 7/31/12 Cantaloupe ...... 1.0 7/31/12 Cattle, fat ...... 0.20 Carrot, roots ...... 0.2 7/31/12 Cattle, kidney ...... 0 .30 Cattle, fat ...... 13.0 7/31/16 Cattle, meat ...... 0 .06 Cattle, liver ...... 5.0 7/31/16 Cattle, meat byproducts except kidney ...... 0 .06 Cattle, meat ...... 2.0 7/31/16 Goat, fat ...... 0 .20 Cattle, meat byproducts, except Goat, kidney ...... 0 .30 liver ...... 1.0 7/31/16 Goat, meat ...... 0.06 Cauliflower ...... 2.0 7/31/12

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Expiration/ Expiration/ Commodity Parts per revocation Commodity Parts per revocation million date million date

Celery ...... 8.0 7/31/12 Pear ...... 2.0 7/31/13 Cherry, sweet ...... 2.0 7/31/12 Pineapple ...... 1.0 7/31/16 Cherry, tart ...... 2.0 7/31/12 Pineapple, process residue ...... 20.0 7/31/16 Collards ...... 2.0 7/31/12 Plum ...... 2.0 7/31/12 Cotton, gin byproducts ...... 30.0 7/31/12 Plum, prune ...... 2.0 7/31/12 Cotton, undelinted seed ...... 1.0 7/31/12 Sheep, fat ...... 13.0 7/31/16 Cucumber ...... 1.0 7/31/12 Eggplant ...... 1.0 7/31/12 Sheep, liver ...... 5.0 7/31/16 Goat, fat ...... 13.0 7/31/16 Sheep, meat ...... 2.0 7/31/16 Goat, liver ...... 5.0 7/31/16 Sheep, meat byproducts, except Goat, meat ...... 2.0 7/31/16 liver ...... 1.0 7/31/16 Goat, meat byproducts, except liver 1.0 7/31/16 Squash, summer ...... 1.0 7/31/12 Hazelnut ...... 0.2 7/31/12 Strawberry ...... 2.0 7/31/16 Hog, fat ...... 13.0 7/31/16 Sweet potato, roots ...... 0.15 7/31/12 Hog, liver ...... 5.0 7/31/16 Walnut ...... 0.2 7/31/12 Hog, meat ...... 2.0 7/31/16 Watermelon ...... 1.0 7/31/12 Hog, meat byproducts, except liver 1.0 7/31/16 Horse, fat ...... 13.0 7/31/16 Horse, liver ...... 5.0 7/31/16 (2) A tolerance is established for the Horse, meat ...... 2.0 7/31/16 combined residues of the insecticide Horse, meat byproducts, except endosulfan, 6,7,8,9,10,10-hexachloro- liver ...... 1.0 7/31/16 Kale ...... 2.0 7/31/12 1,5,5a,6,9,9a-hexahydro-6,9-methano-2, Lettuce, head ...... 11.0 7/31/12 4,3-benzodioxathiepin-3-oxide (alpha Lettuce, leaf ...... 6.0 7/31/12 and beta isomers), and its metabolite Milk, fat ...... 2.0 7/31/16 Muskmelon ...... 1.0 7/31/12 endosulfan sulfate, 6,7,8,9,10,10- Mustard greens ...... 2.0 7/31/12 hexachloro-1,5,5a,6,9,9a-hexahydro-6,9- Mustard, seed ...... 0.2 7/31/12 methano-2, 4,3-benzodioxathiepin-3,3- Nectarine ...... 2.0 7/31/12 Nut, macadamia ...... 0.2 7/31/12 dioxide in or on the commodity in the Peach ...... 2.0 7/31/12 following table:

Expiration/ Commodity Parts per million revocation date

Tea, dried ...... 24 (reflecting less than 0.1 ppm in beverage tea) resulting from application of the insecticide 7/31/16 to growing tea.

(b) Section 18 emergency exemptions. Parts per Expiration/ [Reserved] Commodity revocation million date (c) Tolerances with regional registra- tions. (1) Tolerances with regional reg- Apple ...... 1.0 12/31/14 Apple, wet pomace ...... 5.0 12/31/14 istration, as defined in § 180.1(l), are es- Blueberry ...... 0.3 12/31/14 tablished for residues of the insecticide Corn, sweet, forage ...... 12.0 12/31/14 endosulfan, including its metabolites Corn, sweet, kernel plus cob with husks removed ...... 0.2 12/31/14 and degradates, in or on the commod- Corn, sweet, stover ...... 14.0 12/31/14 ities in the table in this paragraph, Pepper ...... 2.0 12/31/14 when endosulfan is used in the state of Potato ...... 0.2 12/31/14 Pumpkin ...... 1.0 12/31/14 Florida. Compliance with the tolerance Squash, winter ...... 1.0 12/31/14 levels specified in this paragraph is to Tomato ...... 1.0 12/31/14 be determined by measuring only the sum of endosulfan, 6,7,8,9,10,10- (2) Tolerances with regional registra- hexachloro-1,5,5a,6,9,9a-hexahydro-6,9- tions. Tolerances with regional reg- methano-2,4,3-benzodioxathiepin 3- istration, as defined in § 180.1(l), are es- oxide (alpha and beta isomers), and its tablished for residues of the insecticide metabolite endosulfan sulfate, endosulfan, including its metabolites 6,7,8,9,10,10-hexachloro-1,5,5a,6,9,9a- and degradates, in or on the commod- hexahydro-6,9-methano-2,4,3- ities in the table in this paragraph, benzodioxathiepin-3,3-dioxide, cal- when endosulfan is used in the United culated as the stoichiometric equiva- States (except Florida). Compliance lent of endosulfan, in or on the com- with the tolerance levels specified in modity. this paragraph is to be determined by

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measuring only the sum of endosulfan, stoichiometric equivalent of 6,7,8,9,10,10-hexachloro-1,5,5a,6,9,9a- disulfoton, in or on the commodity. hexahydro-6,9-methano-2,4,3- Expiration/ benzodioxathiepin 3-oxide (alpha and Commodity Parts per Revocation beta isomers), and its metabolite million Date endosulfan sulfate, 6,7,8,9,10,10- hexachloro-1,5,5a,6,9,9a-hexahydro-6,9- Bean, lima ...... 0.75 12/31/13 Bean, snap, succulent ...... 0.75 12/31/13 methano-2,4,3-benzodioxathiepin-3,3-di- Broccoli ...... 0.75 12/31/13 oxide, calculated as the stoichiometric Brussels sprouts ...... 0.75 12/31/13 equivalent of endosulfan, in or on the Cabbage ...... 0.75 12/31/13 commodity. Cauliflower ...... 0.75 12/31/13 Coffee, green bean ...... 0.2 6/30/14 Parts per Expiration/ Cotton, undelinted seed ...... 0.75 12/31/13 Commodity revocation Lettuce, head ...... 0.75 12/31/14 million date Lettuce, leaf ...... 2 12/31/14 Apple ...... 1.0 7/31/15 Apple, wet pomace ...... 5.0 7/31/15 (b) Section 18 emergency exemptions. Blueberry ...... 0.3 7/31/15 [Reserved] Corn, sweet, forage ...... 12.0 7/31/15 (c) Tolerances with regional registra- Corn, sweet, kernel plus cob with husks removed ...... 0.2 7/31/15 tions. A tolerance with regional reg- Corn, sweet, stover ...... 14.0 7/31/15 istration is established for residues of Pepper ...... 2.0 7/31/15 the insecticide disulfoton, O,O-diethyl Potato ...... 0.2 7/31/15 S-(2-(ethylthio)ethyl) Pumpkin ...... 1.0 7/31/15 phosphorodithioate, including its me- Squash, winter ...... 1.0 7/31/15 Tomato ...... 1.0 7/31/15 tabolites and degradates, in or on the commodity in the following table. (d) Indirect or inadvertent residues. Compliance with the tolerance levels [Reserved] specified in this paragraph is to be de- termined by measuring only the sum of [65 FR 33696, May 24, 2000, as amended at 71 disulfoton, O,O-diethyl S-(2- FR 54433, Sept. 15, 2006; 76 FR 56653, Sept. 14, (ethylthio)ethyl) phosphorodithioate, 2011; 78 FR 8409, Feb. 6, 2013] and its metabolites demeton-S, O,O- § 180.183 Disulfoton; tolerances for res- diethyl S-(2-(ethylthio)ethyl) idues. phosphorothioate; disulfoton sulfoxide, O,O-diethyl S-(2-(ethylsulfinyl)ethyl) (a) General. Tolerances are estab- phosphorodithioate; disulfoton oxygen lished for residues of the insecticide analog sulfoxide, O,O-diethyl S-(2- disulfoton, O,O-diethyl S-(2- (ethylsulfinyl)ethyl) phosphorothioate, (ethylthio)ethyl) phosphorodithioate, disulfoton sulfone, O,O-diethyl S-(2- including its metabolites and (ethylsulfonyl)ethyl) degradates, in or on the commodities phosphorodithioate; and disulfoton ox- in the following table. Compliance with ygen analog sulfone, O,O-diethyl S-(2- the tolerance levels specified in this (ethylsulfonyl)ethyl) paragraph is to be determined by meas- phosphorothioate; calculated as the uring only the sum of disulfoton, O,O- stoichiometric equivalent of diethyl S-(2-(ethylthio)ethyl) disulfoton, in or on the commodity. phosphorodithioate, and its metabo- lites demeton-S, O,O-diethyl S-(2- Parts per Expiration/ (ethylthio)ethyl) phosphorothioate; Commodity million Revocation disulfoton sulfoxide, O,O-diethyl S-(2- Date (ethylsulfinyl)ethyl) Asparagus ...... 0.1 12/31/13 phosphorodithioate; disulfoton oxygen analog sulfoxide, O,O-diethyl S-(2- (d) Indirect or inadvertent residues. (ethylsulfinyl)ethyl) phosphorothioate, [Reserved] disulfoton sulfone, O,O-diethyl S-(2- (ethylsulfonyl)ethyl) [63 FR 2165, Jan. 14, 1998, as amended at 63 FR 57073, Oct. 26, 1998; 66 FR 38955, July 26, phosphorodithioate; and disulfoton ox- 2001; 67 FR 41806, June 19, 2002; 67 FR 49615, ygen analog sulfone, O,O-diethyl S-(2- July 31, 2002; 70 FR 44492, Aug. 3, 2005; 73 FR (ethylsulfonyl)ethyl) 54960, Sept. 24, 2008; 74 FR 46697, Sept. 11, phosphorothioate; calculated as the 2009; 75 FR 60240, Sept. 29, 2010]

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§ 180.184 Linuron; tolerances for resi- Commodity Parts per dues. million (a) General. Tolerances are estab- Soybean, seed ...... 1 .0 lished for residues of the herbicide Soybean, vegetable ...... 1 .0 linuron (3-(3,4-dichlorophenyl)-1- methoxy-1-methylurea), including its (b) Section 18 emergency exemptions. metabolites and degradates, in or on Time-limited tolerances are estab- the commodities in the table below. lished for residues of the herbicide Compliance with the tolerance levels linuron [3-(3,4-dichlorophenyl)-1- specified below is to be determined by methoxy-1-methylurea], including its measuring only those linuron residues metabolites and degradates, in or on convertible to 3,4-dichloroaniline, cal- the commodities in the table below, re- culated as the stoichiometric equiva- sulting from use of the pesticide pursu- lent of linuron, in or on the com- ant to FIFRA section 18 emergency ex- modity: emptions. Compliance with the toler- ance levels specified below is to be de- Commodity Parts per termined by measuring only those million linuron residues convertible to 3.4- Asparagus ...... 7.0 dichloroaniline, calculated as the stoi- Carrot, roots ...... 1.0 chiometric equivalent of linuron, in or Cattle, fat ...... 0.2 Cattle, kidney ...... 2 .0 on the commodity. The tolerance ex- Cattle, liver ...... 2 .0 pires and is revoked on the date speci- Cattle, meat ...... 0 .1 fied in the table. Cattle, meat byproducts except kidney and liver 0 .1 Celeriac ...... 1.0 Expiration/ Cilantro, dried leaves ...... 10 Commodity Parts per revocation Cilantro, fresh leaves ...... 3 .0 million date Coriander, seed ...... 0 .01 Corn, field, forage ...... 1 .0 Lentil ...... 0.1 12/31/14 Corn, field, grain ...... 0 .1 Corn, field, stover ...... 6 .0 Corn, sweet, forage ...... 1 .0 (c) Tolerances with regional registra- Corn, sweet, kernel plus cob with husks re- tions. Tolerances with regional reg- moved ...... 0 .25 istrations, as defined in § 180.1(l), are Corn, sweet, stover ...... 6 .0 Cotton, gin byproducts ...... 5 .0 established for residues of the herbi- Cotton, undelinted seed ...... 0 .25 cide linuron (3-(3,4-dichlorophenyl)-1- Dill, oil ...... 2 .0 methoxy-1-methylurea), including its Dill, seed ...... 0 .5 Dillweed, dried leaves ...... 5 .0 metabolites and degradates, in or on Dillweed, fresh leaves ...... 1 .5 the commodities in the table below. Goat, fat ...... 0 .2 Compliance with the tolerance levels Goat, kidney ...... 2 .0 specified below is to be determined by Goat, liver ...... 2.0 Goat, meat ...... 0.1 measuring only those linuron residues Goat, meat byproducts except kidney and liver .. 0 .1 convertible to 3,4-dichloroaniline, cal- Hog, fat ...... 0 .05 culated as the stoichiometric equiva- Hog, meat ...... 0 .05 Hog, meat byproducts ...... 0 .1 lent of linuron, in or on the com- Horse, fat ...... 0 .2 modity. Horse, kidney ...... 2 .0 Horse, liver ...... 2 .0 Parts per Horse, meat ...... 0 .1 Commodity million Horse, meat byproducts except kidney and liver 0 .1 Horseradish ...... 0.05 Celery ...... 0 .5 Milk ...... 0.05 Potato ...... 0 .2 Parsley, dried leaves ...... 9 .0 Wheat, forage ...... 0 .5 Parsley, leaves ...... 4.0 Wheat, grain ...... 0 .05 Parsnip, roots ...... 0 .05 Wheat, hay ...... 0 .5 Parsnip, tops ...... 0 .05 Pea, dry, seed ...... 0 .09 Wheat, straw ...... 2 .0 Rhubarb ...... 0 .5 Sheep, fat ...... 0 .2 (d) Indirect or inadvertent residues. Sheep, kidney ...... 2.0 [Reserved] Sheep, liver ...... 2.0 Sheep, meat ...... 0.1 [64 FR 41822, Aug. 2, 1999, as amended at 72 Sheep, meat byproducts except kidney and liver 0 .1 Sorghum, grain, forage ...... 1.0 FR 37653, July 11, 2007; 73 FR 51727, Sept. 5, Sorghum, grain, grain ...... 0 .25 2008; 76 FR 81396, Dec. 28, 2011; 79 FR 8307, Sorghum, grain, stover ...... 1 .0 Feb. 12, 2014]

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§ 180.185 DCPA; tolerances for resi- Commodity Parts per dues. million (a) General. Tolerances for the com- Bean, snap, succulent ...... 2 .0 bined residues of the herbicide di- Celeriac ...... 2.0 Chicory, roots ...... 2 .0 methyl tetrachloroterephthalate Chicory, tops ...... 5 .0 (DCPA) and its metabolites Chive ...... 5 .0 monomethyltetrachloroterephthalate Coriander, leaves ...... 5 .0 Corn, field, forage ...... 0 .4 (MTP) and tetrachloroterephthalic Corn, field, grain ...... 0 .05 acid (TCP) (calculated as dimethyl Corn, field, stover ...... 0 .4 tetrachloroterephthalate) are estab- Corn, pop, forage ...... 0 .4 Corn, pop, grain ...... 0.05 lished in or on the following food com- Corn, pop, stover ...... 0.4 modities: Corn, sweet, forage ...... 0 .4 Corn, sweet, kernel plus cob with husks re- Commodity Parts per moved ...... 0 .05 million Corn, sweet, stover ...... 0 .4 Cotton, undelinted seed ...... 0 .2 Cantaloupe ...... 1 .0 Cucumber ...... 1 .0 Garlic ...... 1 .0 Dill ...... 5 .0 Ginseng ...... 2 .0 Eggplant ...... 1.0 Horseradish ...... 2.0 Lettuce ...... 2.0 Muskmelon ...... 1 .0 Marjoram ...... 5 .0 Onion, bulb ...... 1 .0 Parsley, dried leaves ...... 20.0 Onion, green ...... 1 .0 Parsley, leaves ...... 5.0 Strawberry ...... 2 .0 Pea, blackeyed, seed ...... 2 .0 Tomato ...... 1.0 Pepper ...... 2 .0 Vegetable, brassica, leafy, group 5 ...... 5.0 Pimento ...... 2 .0 Watermelon ...... 1.0 Potato ...... 2 .0 Radicchio ...... 5.0 (b) Section 18 emergency exemptions. Radish, oriental, roots ...... 2 .0 [Reserved] Radish, oriental, tops ...... 2 .0 Rutabaga ...... 2 .0 (c) Tolerances with regional registra- Soybean ...... 2.0 tions. Tolerances with regional reg- Squash, summer ...... 1 .0 istration, as defined in § 180.1(l), are es- Squash, winter ...... 1 .0 Sweet potato ...... 2.0 tablished for the combined inadvertent Turnip, roots ...... 2 .0 residues of the herbicide dimethyl Turnip, tops ...... 5.0 tetrachloroterephthalate (DCPA) and Yam, true, tuber ...... 2.0 its metabolites monomethyl tetrachloroterephthalate acid (MTP) [72 FR 52018, Sept. 12, 2007, as amended at 73 and terachlorophthalic acid (TCP) (cal- FR 53737, Sept. 17, 2008; 73 FR 80302, Dec. 31, culated as DCPA) in or on the fol- 2008; 74 FR 14744, Apr. 1, 2009] lowing food commodities: § 180.189 Coumaphos; tolerances for Parts per residues. Commodity million (a) General. Tolerances for residues of Radish, roots ...... 2 .0 the insecticide coumaphos (O,O-diethyl Radish, tops ...... 15 .0 O-3-chloro-4-methyl-2-oxo-2H-1- benzopyran-7-yl phosphorothioate and (d) Indirect or inadvertent residues. its oxygen analog (O,O-diethyl O-3- Tolerances are established for the com- chloro-4-methyl-2-oxo-2H-1- bined indirect or inadvertent residues benzopyran-7-yl phosphate) in or on of the herbicide dimethyl food commodities as follows: tetrachloroterephthalate (DCPA) and its metabolites monomethyl Commodity Parts per tetrachloroterephthalate acid (MTP) million and terachlorophthalic acid (TCP) (cal- Cattle, fat ...... 1.0 culated as DCPA) in or on the fol- Cattle, meat ...... 1 .0 lowing food commodities: Cattle, meat byproducts ...... 1.0 Goat, fat ...... 1 .0 Parts per Goat, meat ...... 1.0 Commodity million Goat, meat byproducts ...... 1 .0 Hog, fat ...... 1 .0 Basil, dried leaves ...... 20.0 Hog, meat ...... 1 .0 Basil, fresh leaves ...... 5 .0 Hog, meat byproducts ...... 1 .0 Bean, dry ...... 2.0 Honey ...... 0.15 Bean, mung, seed ...... 2 .0 Honeycomb ...... 45 .0

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Commodity Parts per § 180.191 Folpet; tolerances for resi- million dues. Horse, fat ...... 1 .0 (a) General. Tolerances are estab- Horse, meat ...... 1 .0 lished for the fungicide folpet (N- Horse, meat byproducts ...... 1 .0 (trichloromethylthio)phthalimide) in Milk, fat (=n in whole milk) ...... 0.5 Sheep, fat ...... 1 .0 or on raw agricultural commodities as Sheep, meat ...... 1.0 follows: Sheep, meat byproducts ...... 1 .0 Parts per Commodity million (b) Section 18 emergency exemptions. [Reserved] Apple 1 ...... 5.0 Cranberry 1 ...... 15 .0 (c) Tolerances with regional registra- Cucumber 1 ...... 2 .0 tions. [Reserved] Grape 1 ...... 50 .0 Grape, raisin 1 ...... 80.0 (d) Indirect or inadvertent residues. Hop, dried cones ...... 120 .0 [Reserved] Lettuce 1 ...... 50.0 Melon 1 ...... 3 .0 [64 FR 39077, July 21, 1999, as amended at 65 Onion,bulb 1 ...... 2 .0 FR 49936, Aug. 16, 2000; 67 FR 46883, July 17, Strawberry 1 ...... 5 .0 2002; 69 FR 29458, May 24, 2004; 72 FR 28876, Tomato 1 ...... 25.0 May 23, 2007] 1 No U.S. registrations.

§ 180.190 Diphenylamine; tolerances (b) Section 18 emergency exemptions. for residues. [Reserved] (c) Tolerances with regional registra- (a) General. Tolerances for residues of tions. Tolerances with regional reg- the plant regulator diphenylamine are istrations as defined in § 180.1(l) are es- established in or on the following com- tablished for the fungicide folpet (N- modities: (trichloromethylthio)phthalimide) in or on the following raw agricultural Parts per Commodity million commodity:

Apple, wet pomace ...... 30.0 Commodity Parts per Apple from preharvest or postharvest use, in- million cluding use of impregnated wraps ...... 10.0 Avocado ...... 25.0 Cattle, fat ...... 0.01 Cattle, liver ...... 0 .1 Cattle, meat byproducts, except liver ...... 0 .01 (d) Indirect or inadvertent residues. Cattle, meat ...... 0 .01 [Reserved] Goat, fat ...... 0 .01 [61 FR 37222, July 17, 1996, as amended at 68 Goat, liver ...... 0.1 FR 10388, Mar. 5, 2003; 69 FR 52192, Aug. 25, Goat, meat byproducts, except liver ...... 0 .01 2004; 72 FR 41928, Aug. 1, 2007] Goat, meat ...... 0.01 Horse, fat ...... 0 .01 Horse, liver ...... 0 .1 § 180.198 Trichlorfon; tolerances for Horse, meat byproducts, except liver ...... 0 .01 residues. Horse, meat ...... 0 .01 (a) General. Tolerances are estab- Milk ...... 0.01 lished for residues of the insecticide Pear (post harvest) ...... 5 .0 trichlorfon (dimethyl (2,2,2-trichloro-1- Sheep, fat ...... 0 .01 Sheep, liver ...... 0.1 hydroxyethyl) phosphonate) in or on Sheep, meat byproducts, except liver ...... 0 .01 the following food commodities: Sheep, meat ...... 0.01 Parts per Commodity million (b) Section 18 emergency exemptions. [Reserved] Cattle, fat 1 ...... 0.5 Cattle, meat 1 ...... 0 .2 (c) Tolerances with regional registra- Cattle, meat byproducts 1 ...... 0.1 tions. [Reserved] 1 There are no U.S. registrations for cattle commodities as (d) Indirect or inadvertent residues. of June 24, 1999. [Reserved] (b) Section 18 emergency exemptions. [64 FR 25848, May 13, 1999, as amended at 66 [Reserved] FR 63198, Dec. 5, 2001; 72 FR 16283, Apr. 4, (c) Tolerances with regional registra- 2007; 76 FR 34885, June 15, 2011] tions. [Reserved]

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(d) Indirect or inadvertent residues. (c) Tolerances with regional registra- [Reserved] tions. [Reserved] (d) Indirect or inadvertent residues. [72 FR 54578, Sept. 26, 2007] [Reserved] § 180.200 Dicloran; tolerances for resi- [68 FR 39439, July 1, 2003, as amended at 71 dues. FR 56398, Sept. 27, 2006] (a) General. Tolerances are estab- lished for residues of the fungicide § 180.204 Dimethoate; tolerances for residues. dicloran, including its metabolites and degradates, in or on the commodities (a) General. Tolerances are estab- in the table in this paragraph. Compli- lished for total residues of the insecti- ance with the tolerance levels specified cide dimethoate (O,O-dimethyl S-(N- in this paragraph is to be determined methylcarbamoylmethyl) by measuring only dicloran, 2,6- phosphorodithioate) including its oxy- dichloro-4-nitroaniline, in or on the gen analog (O,O-dimethyl S-(N- commodity. methylcarbamoylmethyl) phosphorothioate) in or on the fol- Expiration/ lowing food commodities: Commodity Parts per revocation million date Parts per Commodity million Apricot ...... 20 None Bean, snap, succulent ...... 20 None Alfalfa, forage ...... 2.0 Carrot, roots ...... 10 11/2/11 Alfalfa, hay ...... 2.0 Celery ...... 15 None Bean, dry, seed ...... 2 .0 Cherry, sweet ...... 20 None Bean, lima ...... 2 .0 Cucumber ...... 5 None Bean, snap, succulent ...... 2 .0 Endive ...... 10 None Blueberry 1 ...... 1 .0 Garlic ...... 5 None Broccoli ...... 2 .0 Grape ...... 10 None Cattle, meat byproducts ...... 0.02 Lettuce ...... 10 None Cauliflower ...... 2 .0 Nectarine ...... 20 None Celery ...... 2 .0 Onion ...... 10 None Citrus, dried pulp ...... 5 .0 Peach ...... 20 None Corn, field, forage ...... 1 .0 Corn, field, grain ...... 0 .1 Plum, prune, fresh ...... 15 None Corn, field, stover ...... 1 .0 Potato ...... 0.25 12/31/14 Corn, pop, grain ...... 0.1 Rhubarb ...... 10 None Corn, pop, stover ...... 1.0 Sweet potato, roots ...... 10 None Corn, sweet, forage ...... 1 .0 Tomato ...... 5 None Cotton, undelinted seed ...... 0 .1 Egg ...... 0 .02 (b) Section 18 emergency exemptions. Endive ...... 2.0 [Reserved] Goat, meat byproducts ...... 0 .02 Grapefruit ...... 2 .0 (c) Tolerances with regional registra- Hog, meat byproducts ...... 0 .02 tions. [Reserved] Horse, meat byproducts ...... 0 .02 (d) Indirect or inadvertent residues. Kale ...... 2 .0 Lemon ...... 2.0 [Reserved] Lettuce, leaf ...... 2 .0 Melon ...... 1 .0 [77 FR 40815, July 11, 2012] Milk ...... 0.002 Mustard greens ...... 2.0 § 180.202 p-Chlorophenoxyacetic acid; Orange ...... 2 .0 tolerances for residues. Pea ...... 2 .0 Pear ...... 2 .0 (a) General. A tolerance is established Pecan ...... 0 .1 for the combined residues of the plant Pepper ...... 2 .0 regulator p-chlorophenoxyacetic acid Potato ...... 0 .2 Poultry, meat byproducts ...... 0.02 and its metabolite p-chlorophenol to Safflower, seed ...... 0 .1 inhibit embryonic root development in Sheep, meat byproducts ...... 0 .02 or on the following food commodity: Sorghum, grain, forage ...... 0.1 Sorghum, grain, grain ...... 0 .1 Parts per Sorghum, grain, stover ...... 0 .1 Commodity million Soybean, forage ...... 2 .0 Soybean, hay ...... 2 .0 Bean, mung, sprouts ...... 0.2 Soybean, seed ...... 0 .05 Swiss chard ...... 2.0 Tangerine ...... 2 .0 (b) Section 18 emergency exemptions. Tomato ...... 2.0 [Reserved] Turnip, roots ...... 0 .2

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Parts per Parts per Commodity million Commodity million

Turnip, tops ...... 2.0 Cattle, meat ...... 0 .05 Wheat, forage ...... 2 .0 Cattle, meat byproducts, except kidney ...... 0.05 Wheat, grain ...... 0 .04 Cherimoya ...... 0 .05 Wheat, hay ...... 2 .0 Coffee, bean, green ...... 0 .05 Wheat, straw ...... 2 .0 Corn, field, forage ...... 3 .0 Corn, field, grain ...... 0 .1 1 There are U.S. registrations as of August 16, 1996. Corn, field, stover ...... 10 .0 (b) Section 18 emergency exemptions. Corn, pop, grain ...... 0.1 Corn, pop, stover ...... 10.0 [Reserved] Corn, sweet, kernel plus cob with husks re- (c) Tolerances with regional registra- moved ...... 0 .05 tions. Tolerances with regional reg- Cotton, gin byproducts ...... 110.0 istration, as defined in § 180.1(l), are es- Cotton, undelinted seed ...... 3 .5 Cowpea, forage ...... 0 .1 tablished for total residues of Cowpea, hay ...... 0 .4 dimethoate including its oxygen analog Cranberry ...... 0 .05 in or on the following food commod- Custard apple ...... 0 .05 Egg ...... 0 .01 ities: Endive ...... 0.05 Feijoa ...... 0 .05 Commodity Parts per Fig ...... 0 .05 million Fruit, citrus, group 10 ...... 0 .05 Fruit, pome, group 11 ...... 0.05 Asparagus ...... 0.15 Fruit, stone, group 12 ...... 0 .05 Brussels sprouts ...... 5 .0 Goat, fat ...... 0 .05 Cherry, sweet ...... 2 .0 Goat, kidney ...... 0 .5 Cherry, tart ...... 2 .0 Goat, meat ...... 0.05 Goat, meat byproducts, except kidney ...... 0 .05 (d) Indirect or inadvertent residues. Grain, aspirated fractions ...... 65.0 [Reserved] Grape ...... 0 .05 Grass, forage ...... 90 .0 [65 FR 33697, May 24, 2000, as amended at 69 Grass, hay ...... 40 .0 FR 6567, Feb. 11, 2004; 73 FR 53737, Sept. 17, Guar, seed ...... 0.5 2008] Guava ...... 0 .05 Hog, fat ...... 0 .05 Hog, kidney ...... 0.5 § 180.205 Paraquat; tolerances for resi- Hog, meat ...... 0 .05 dues. Hog, meat byproducts, except kidney ...... 0 .05 (a) General. Tolerances are estab- Hop, dried cones ...... 0 .5 Horse, fat ...... 0 .05 lished for residues of the desiccant, de- Horse, kidney ...... 0 .5 foliant, and herbicide paraquat (1,1′-di- Horse, meat ...... 0 .05 methyl-4,4′-bipyridinium-ion) derived Horse, meat byproducts, except kidney ...... 0 .05 Ilama ...... 0 .05 from application of either the Jaboticaba ...... 0 .05 bis(methyl sulfate) or the dichloride Kiwifruit ...... 0.05 salt (both calculated as the cation) in Lentil, seed ...... 0 .3 or on the following food commodities: Lettuce ...... 0.05 Longan ...... 0 .05 Lychee ...... 0 .05 Parts per Commodity million Mango ...... 0.05 Milk ...... 0.01 Acerola ...... 0.05 Nut, tree, group 14 ...... 0 .05 Almond, hulls ...... 0 .5 Okra ...... 0.05 Animal feed, nongrass, group 18, forage ...... 75 .0 Olive ...... 0 .05 Animal feed, nongrass, group 18, hay ...... 210.0 Onion, bulb ...... 0 .1 Artichoke, globe ...... 0.05 Onion, green ...... 0 .05 Asparagus ...... 0.5 Papaya ...... 0 .05 Atemoya ...... 0 .05 Passionfruit ...... 0 .2 Avocado ...... 0 .05 Pawpaw ...... 0 .05 Banana ...... 0.05 Pea and bean, dried shelled, except soybean, Barley, grain ...... 0 .05 subgroup 6C, except guar bean ...... 0 .3 Barley, hay ...... 3 .5 Pea and bean, succulent shelled, subgroup 6B 0 .05 Barley, straw ...... 1 .0 Pea, field, hay ...... 0.8 Beet, sugar, roots ...... 0 .5 Pea, field, vines ...... 0 .2 Beet, sugar, tops ...... 0.05 Peanut ...... 0 .05 Berry group 13 ...... 0 .05 Peanut, hay ...... 0.5 Biriba ...... 0 .05 Peppermint, tops ...... 0 .5 Cacao bean, bean ...... 0 .05 Persimmon ...... 0 .05 Canistel ...... 0 .05 Pineapple ...... 0.05 Carrot, roots ...... 0.05 Pineapple, process residue ...... 0 .25 Cattle, fat ...... 0.05 Pistachio ...... 0.05 Cattle, kidney ...... 0 .5 Pomegranate ...... 0 .05

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Parts per EDITORIAL NOTE: For FEDERAL REGISTER ci- Commodity million tations affecting § 180.205, see the List of CFR Sections Affected, which appears in the Pulasan ...... 0 .05 Finding Aids section of the printed volume Rambutan ...... 0 .05 and at www.fdsys.gov. Rhubarb ...... 0 .05 Rice, grain ...... 0 .05 Rice, straw ...... 0 .06 § 180.206 Phorate; tolerances for resi- Safflower, seed ...... 0 .05 dues. Sapodilla ...... 0 .05 (a) General. Tolerances are estab- Sapote, black ...... 0 .05 Sapote, mamey ...... 0 .05 lished for the combined residues of the Sapote, white ...... 0 .05 insecticide phorate (O,O-diethyl S Sheep, fat ...... 0 .05 (ethylthio) meth- Sheep, kidney ...... 0.5 Sheep, meat ...... 0.05 yl]phosphorodithioate), phorate sulf- Sheep, meat byproducts, except kidney ...... 0 .05 oxide, phorate sulfone, phorate oxygen Sorghum, forage, forage ...... 0 .1 analog, phorate oxygen analog sulf- Sorghum, grain, forage ...... 0.1 oxide, and phorate oxygen analog Sorghum, grain, grain ...... 0 .05 Soursop ...... 0 .05 sulfone in or on the following food Soybean, forage ...... 0 .4 commodities: Soybean, hay ...... 10 .0 Soybean, hulls ...... 4 .5 Commodity Parts per Soybean, seed ...... 0 .7 million Spanish lime ...... 0 .05 Bean, dry, seed ...... 0 .05 Spearmint, tops ...... 0 .5 Bean, succulent ...... 0 .05 Star apple ...... 0 .05 Beet, sugar, roots ...... 0 .3 Starfruit ...... 0 .05 Beet, sugar, tops ...... 3.0 Strawberry ...... 0 .25 Coffee, green bean 1 ...... 0 .02 Sugar apple ...... 0 .05 Corn, field, forage ...... 0 .5 Sugarcane, cane ...... 0.5 Corn, field, grain ...... 0 .05 Sugarcane, molasses ...... 3 .0 Corn, sweet, forage ...... 0 .5 Sunflower, seed ...... 2.0 Corn, sweet, kernel plus cob with husks re- Turnip, greens ...... 0.05 moved ...... 0 .05 Turnip, roots ...... 0 .05 Cotton, undelinted seed ...... 0 .05 Vegetable, brassica, leafy, group 5 ...... 0.05 Hop, dried cones ...... 2 .0 Vegetable, cucurbit, group 9 ...... 0.05 Peanut ...... 0 .1 Vegetable, fruiting, group 8 ...... 0.05 Potato ...... 0 .2 Vegetable, legume, edible podded, subgroup 6A 0 .05 Sorghum, grain, grain ...... 0 .05 Vegetable, tuberous and corm, subgroup 1C ..... 0.50 Sorghum, grain, stover ...... 0 .1 Wax jambu ...... 0 .05 Soybean, seed ...... 0 .05 Wheat, forage ...... 0 .5 Sugarcane, cane ...... 0.05 Wheat, grain ...... 1 .1 Wheat, forage ...... 1 .5 Wheat, hay ...... 3 .5 Wheat, grain ...... 0 .05 Wheat, straw ...... 50 .0 Wheat, hay ...... 1 .5 Wheat, straw ...... 0 .05 (b) Section 18 emergency exemptions. 1 There are no U.S. registrations as of September 1, 1993 [Reserved] for the use of phorate on the growing crop, coffee. (c) Tolerances with regional registra- (b) Section 18 emergency exemptions. tions. Tolerances with regional reg- [Reserved] istration as defined in § 180.1(l), are es- (c) Tolerances with regional registra- tablished for residues of the pesticide tions. [Reserved] paraquat (1,1′-dimethyl-4,4′ (d) Indirect or inadvertent residues. bipyridinium ion) derived from applica- [Reserved] tion of either the bis(methyl sulfate) or [58 FR 62038, Nov. 24, 1993, as amended at 63 the dichloride salt (both calculated as FR 2165, Jan. 14, 1998; 63 FR 57074, Oct. 26, the cation) in or on the following food 1998; 66 FR 50833, Oct. 5, 2001; 67 FR 49616, commodities: July 31, 2002; 71 FR 74816, Dec. 13, 2006; 73 FR 53738, Sept. 17, 2008] Commodity Parts per million § 180.207 Trifluralin; tolerances for Pea, pigeon, seed ...... 0 .05 residues. Taro, corm ...... 0 .1 (a) General. Tolerances are estab- Tyfon ...... 0 .05 lished for residues of trifluralin, in- cluding its metabolites and degradates, (d) Indirect or inadvertent residues. in or on the commodities in the fol- [Reserved] lowing table. Compliance with the tol- [46 FR 51614, Oct. 21, 1981] erance levels specified in the following

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table is to be determined by only benfluralin, N-butyl-N-ethyl-aaa- trifluralin a,a,a-trifluoro-2,6-dinitro- trifluoro-2,6-dinitro-p-toluidine, in or N,N-dipropyl-p-toluidine, in or on the on the following food commodities: commodity. Commodity Parts per Parts per million Commodity million Alfalfa, forage ...... 0.05 Alfalfa, forage ...... 3.0 Alfalfa, hay ...... 0.05 Alfalfa, hay ...... 2.0 Clover, forage ...... 0.05 Almond, hulls ...... 0 .05 Clover, hay ...... 0.05 Asparagus ...... 0.05 Lettuce ...... 0.05 Barley, grain ...... 0 .05 Barley, hay ...... 0 .05 Trefoil, forage ...... 0 .05 Barley, straw ...... 0 .05 Trefoil, hay ...... 0 .05 Bean, mung, sprouts ...... 2.0 Carrot, roots ...... 1.0 (b) Section 18 emergency exemptions. Celery ...... 0 .05 Corn, field, forage ...... 0 .05 [Reserved] Corn, field, grain ...... 0 .05 (c) Tolerances with regional registra- Corn, field, stover ...... 0 .05 tions. [Reserved] Cotton, gin byproducts ...... 0 .05 Endive ...... 0.05 (d) Indirect or inadvertent residues. Fruit, citrus, group 10 ...... 0 .05 [Reserved] Fruit, stone, group 12 ...... 0 .05 Grape ...... 0 .05 [68 FR 39439, July 1, 2003, as amended at 73 Hop, dried cones ...... 0 .05 FR 52613, Sept. 10, 2008] Nut, tree, group 14 ...... 0 .05 Oilseed, crop group 20 ...... 0 .05 Okra ...... 0.05 § 180.209 Terbacil; tolerances for resi- Peanut ...... 0 .05 dues. Peanut, hay ...... 0.05 (a) General. Tolerances are estab- Peppermint, oil ...... 2 .0 Peppermint, tops ...... 0 .05 lished for combined residues of the her- Sorghum, grain, forage ...... 0.05 bicide terbacil, (3-tert-butyl-5-chloro-6- Sorghum, grain, grain ...... 0 .05 methyluracil) and its metabolites [3- Sorghum, grain, stover ...... 0 .05 Spearmint, oil ...... 2 .0 tert-butyl-5-chloro-6- Spearmint, tops ...... 0 .05 hydroxymethyluracil], [6-chloro-2,3- Sugarcane, cane ...... 0.05 dihydro-7-hydroxymethyl 3,3-dimethyl- Vegetable, brassica, leafy group 5 ...... 0 .05 5H-oxazolo(3,2-a) pyrimidin-5-one], and Vegetable, bulb, group 3 ...... 0 .05 Vegetable, cucurbit, group 9 ...... 0.05 [6-chloro-2,3-dihydro-3,3,7-trimethyl- Vegetable, foliage of legume, group 7 ...... 0 .05 5H-oxazolo(3,2-a) pyrimidin-5-one], cal- Vegetable, fruiting, group 8 ...... 0.05 culated as terbacil, in or on the fol- Vegetable, leaves of root and tuber, group 2 ..... 0 .05 Vegetable, legume, group 6 ...... 0 .05 lowing raw agricultural commodities: Vegetable, root and tuber, group 1, except car- rot ...... 0 .05 Commodity Parts per Wheat, grain ...... 0 .05 million Wheat, straw ...... 0 .05 Alfalfa, forage ...... 1.0 Alfalfa, hay ...... 2.0 (b) Section 18 emergency exemptions. Apple ...... 0.3 [Reserved] Asparagus ...... 0.4 (c) Tolerances with regional registra- Blueberry ...... 0 .2 tions. [Reserved] Caneberry subgroup 13A ...... 0 .2 (d) Indirect or inadvertent residues. Peach ...... 0 .2 [Reserved] Peppermint, tops ...... 2 .0 Spearmint, tops ...... 2 .0 [45 FR 42619, June 25, 1980, as amended at 45 Strawberry ...... 0 .1 FR 56346, Aug. 25, 1980; 45 FR 86493, Dec. 31, Sugarcane, cane ...... 0.4 1980; 46 FR 37250, July 20, 1981; 47 FR 13524, Watermelon ...... 1.0 Mar. 31, 1982; 47 FR 20309, May 12, 1982; 63 FR 57074, Oct. 26, 1998; 64 FR 39082, July 21, 1999; (b) Section 18 emergency exemptions. 70 FR 21643, Apr. 27, 2005; 71 FR 54433, Sept. [Reserved] 15, 2006; 78 FR 46274, July 31, 2013] (c) Tolerances with regional registra- tions. [Reserved] § 180.208 Benfluralin; tolerances for residues. (d) Indirect or inadvertent residues. [Reserved] (a) General. Tolerances are estab- lished for residues of the herbicide [71 FR 30818, May 31, 2006]

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§ 180.210 Bromacil; tolerances for resi- (c) Tolerances with regional registra- dues. tions. [Reserved] (a) General. Tolerances are estab- (d) Indirect or inadvertent residues. lished for residues of the herbicide [Reserved] bromacil (5-bromo-3-sec-butyl-6- [47 FR 25959, June 16, 1982, as amended at 47 methyluracil) in or on the following FR 28381, June 30, 1982; 47 FR 28626, July 1, food commodities: 1982; 47 FR 46701, Oct. 20, 1982; 63 FR 57074, Oct. 26, 1998; 72 FR 53454, Sept. 19, 2007] Commodity Parts per million § 180.212 S-Ethyl cyclohexylethylthio- Fruit, citrus ...... 0 .1 ; tolerances for residues. Pineapple ...... 0.1 (a) General. Tolerances are estab- lished for residues of the herbicide S- (b) Section 18 emergency exemptions. ethyl cyclohexylethylthiocarbamate in [Reserved] or on the following food commodities: (c) Tolerances with regional registra- tions. [Reserved] Commodity Parts per (d) Indirect or inadvertent residues. million [Reserved] Beet, garden, roots ...... 0 .05(N) Beet, garden, tops ...... 0 .05(N) [68 FR 39439, July 1, 2003] Beet, sugar, roots ...... 0 .05(N) Beet, sugar, tops ...... 0.05(N) § 180.211 Propachlor; tolerances for Spinach ...... 0 .05(N) residues. (b) Section 18 emergency exemptions. (a) General. Tolerances are estab- [Reserved] lished for the combined residues of the (c) Tolerances with regional registra- herbicide propachlor (2-chloro-N- tions. [Reserved] isopropylacetanilide) and its metabo- (d) Indirect or inadvertent residues. lites containing the N-isopropylaniline [Reserved] moiety, calculated as 2-chloro-N- isopropylacetanilide, in or on the fol- [68 FR 39439, July 1, 2003] lowing raw agricultural commodities: § 180.213 Simazine; tolerances for resi- Parts per dues. Commodity million (a) General. Tolerances are estab- Cattle, fat ...... 0.05 lished for the combined residues of the Cattle, kidney ...... 0 .2 herbicide simazine (2-chloro-4,6- Cattle, meat ...... 0 .02 Cattle, meat byproducts, except kidney ...... 0.05 bis(ethylamino)-s-triazine) and its two Corn, field, forage ...... 3 .0 chlorinated degradates (2-amino-4- Corn, field, grain ...... 0 .2 chloro-6-ethylamino-s-triazine and 2,4- Corn, field, stover ...... 1 .0 diamino-6-chloro-s-triazine), the total Corn, sweet, forage ...... 3 .0 Goat, fat ...... 0 .05 residue to be measured in or on the fol- Goat, kidney ...... 0 .2 lowing food commodities: Goat, meat ...... 0.02 Goat, meat byproducts, except kidney ...... 0 .05 Parts per Hog, fat ...... 0 .02 Commodity million Hog, meat ...... 0 .02 Hog, meat byproducts ...... 0 .02 Almond ...... 0.25 Horse, fat ...... 0 .05 Almond, hulls ...... 0 .25 Horse, kidney ...... 0 .2 Apple ...... 0.20 Horse, meat ...... 0 .02 Avocado ...... 0 .20 Horse, meat byproducts, except kidney ...... 0 .05 Blackberry ...... 0 .20 Milk ...... 0.02 Blueberry ...... 0 .20 Sheep, fat ...... 0 .05 Cattle, meat ...... 0 .03 Sheep, kidney ...... 0.2 Cattle, meat byproducts ...... 0.03 Sheep, meat ...... 0.02 Cherry ...... 0.25 Sheep, meat byproducts, except kidney ...... 0 .05 Corn, field, forage ...... 0 .20 Sorghum, forage, forage ...... 8 .0 Corn, field, grain ...... 0 .20 Sorghum, grain, forage ...... 8.0 Corn, field, stover ...... 0 .25 Sorghum, grain, grain ...... 0 .25 Corn, pop, grain ...... 0.20 Sorghum, grain, stover ...... 12 .0 Corn, pop, stover ...... 0.25 Corn, sweet, forage ...... 0 .20 Corn, sweet, kernel plus cob with husks re- (b) Section 18 emergency exemptions. moved ...... 0 .25 [Reserved] Corn, sweet, stover ...... 0 .25

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Parts per Parts per Commodity million Commodity million

Cranberry ...... 0 .25 Cucumber ...... 0 .5 Currant ...... 0 .25 Eggplant ...... 0.5 Egg ...... 0 .03 Grape ...... 0 .5 Goat, meat ...... 0.03 Grapefruit ...... 3 Goat, meat byproducts ...... 0 .03 Grass, forage ...... 10 Grape ...... 0 .20 Hop, dried cones ...... 0 .5 Grapefruit ...... 0 .25 Kale ...... 3 Hazelnut ...... 0 .20 Legume, forage ...... 10 Horse, meat ...... 0 .03 Lemon ...... 3 Horse, meat byproducts ...... 0 .03 Lemon ...... 0.25 Melon ...... 0 .5 Loganberry ...... 0 .20 Orange, sweet ...... 3 Milk ...... 0.03 Peach ...... 0 .5 Nut, macadamia ...... 0.25 Pea, succulent ...... 0 .5 Olive ...... 0 .20 Pepper ...... 0 .5 Orange ...... 0 .25 Pumpkin ...... 0.5 Peach ...... 0 .20 Safflower, seed ...... 0 .5 Pear ...... 0 .25 Spinach ...... 3 Pecan ...... 0 .20 Squash, summer ...... 0 .5 Plum ...... 0 .20 Squash, winter ...... 0 .5 Raspberry ...... 0 .20 Strawberry ...... 1 Sheep, meat ...... 0.03 Swiss chard ...... 3 Sheep, meat byproducts ...... 0 .03 Tangerine ...... 3 Strawberry ...... 0 .25 Tomato ...... 0.5 Walnut ...... 0 .2 Turnip, greens ...... 3 Walnut ...... 0 .5 (b) Section 18 emergency exemptions. [Reserved] (2) A tolerance of 0.5 part per million (c) Tolerances with regional registra- is established for the pesticide naled in tions. [Reserved] or on all raw agricultural commodities, (d) Indirect or inadvertent residues. except those otherwise listed in this [Reserved] section, from use of the pesticide for area pest (mosquito and fly) control. [63 FR 2165, Jan. 14, 1998, as amended at 63 FR 57074, Oct. 26, 1998; 72 FR 35665, June 29, (b) Section 18 emergency exemptions. 2007; 72 FR 53454, Sept. 19, 2007] [Reserved] (c) Tolerances with regional registra- § 180.215 Naled; tolerances for resi- tions. [Reserved] dues. (d) Indirect or inadvertent residues. (a) General. (1) Tolerances are estab- [Reserved] lished for residues of the insecticide [42 FR 46304, Sept. 15, 1977, as amended at 54 naled (1,2-dibromo-2,2-dichloro-ethyl FR 20125, May 10, 1989; 63 FR 57074, Oct. 26, dimethyl phosphate) and its conversion 1998; 66 FR 50833, Oct. 5, 2001; 77 FR 59124, product 2,2-dichlorovinyl dimethyl Sept. 26, 2012] phosphate, expressed as naled, result- ing from the application of the pes- § 180.217 Metiram; tolerances for resi- ticide to growing crops or from direct dues. application to livestock and poultry, in (a) General. Tolerances are estab- or on the following raw agricultural lished for residues of a metiram (a mix- commodities: ture of 5.2 parts by weight of ammoni- ates of [ethylenebis (dithiocarbamato)] Parts per Commodity million zinc with 1 part by weight ethylenebis [dithiocarbamic acid] bimolecular and Almond, hulls ...... 0 .5 trimolecular cyclic anhydrosulfides Almond ...... 0.5 Bean, dry, seed ...... 0 .5 and disulfides), including its metabo- Bean, succulent ...... 0 .5 lites and degradates, in or on the com- Beet, sugar, roots ...... 0 .5 modities in the following table. Com- Beet, sugar, tops ...... 0.5 Broccoli ...... 1 pliance with the tolerance levels speci- Brussels sprouts ...... 1 fied in this paragraph is to be deter- Cabbage ...... 1 mined by measuring only those Cauliflower ...... 1 metiram residues convertible to and Celery ...... 3 Collards ...... 3 expressed in terms of the degradate Cotton, undelinted seed ...... 0 .5 carbon disulfide.

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Parts per Parts per Commodity million Commodity million

Apple ...... 0.5 Wheat, hay ...... 5 .0 Apple, pomace, wet ...... 2 Wheat, straw ...... 0 .50 Banana 1 ...... 3 Grape, wine 1 ...... 5 (b) Section 18 emergency exemptions. Potato ...... 0 .2 [Reserved] 1 There are no U.S. registrations on bananas and grape, wine as of April 29, 2011. (c) Tolerances with regional registra- tions. [Reserved] (b) Section 18 emergency exemptions. (d) Indirect or inadvertent residues. [Reserved] Tolerances are established for indirect (c) Tolerances with regional registra- or inadvertant residues of atrazine, 2- tions. [Reserved] chloro-4-ethylamino-6-isopropylamino- (d) Indirect or inadvertent residues. s-triazine, in or on the following raw [Reserved] agricultural commodity when present [63 FR 57074, Oct. 26, 1998, as amended at 76 therein as a result of application of FR 23891, Apr. 29, 2011] atrazine to the growing crops in para- graph (a) of this section: § 180.220 Atrazine; tolerances for resi- dues. Parts per Commodity million (a) General. Tolerances are estab- lished for the combined residues of the Vegetable, leafy, except brassica, group 4 ...... 0 .25 herbicide atrazine (2-chloro-4- ethylamino-6-isopropylamino-s-tri- [43 FR 29121, July 6, 1978, as amended at 44 azine) and its chlorinated metabolites FR 67116, Nov. 23, 1979; 47 FR 3771, Jan. 27, 2-amino-4-chloro-6-isopropylamino-s- 1982; 47 FR 8012, Feb. 24, 1982; 63 FR 57075, triazine, 2-amino-4-chloro-6- Oct. 26, 1998; 67 FR 46893, July 17, 2002; 69 FR 6567, Feb. 11, 2004; 72 FR 35666, June 29, 2007; ethylamino-s-triazine, and 2,4-diamino- 72 FR 53454, Sept. 19, 2007; 73 FR 37852, July 6-chloro-s-triazine, in or on the fol- 2, 2008; 76 FR 56654, Sept. 14, 2011] lowing food commodities: § 180.222 Prometryn; tolerances for Parts per Commodity million residues. (a) General. Tolerances are estab- Cattle, fat ...... 0.02 Cattle, meat ...... 0 .02 lished for residues of the herbicide Cattle, meat byproducts ...... 0.02 prometryn, including its metabolites Corn, field, forage ...... 1 .5 and degradates, in or on the commod- Corn, field, grain ...... 0 .20 Corn, field, stover ...... 0 .5 ities in the following table. Compliance Corn, pop, forage ...... 1 .5 with the tolerance levels specified in Corn, pop, grain ...... 0.20 the following table is to be determined Corn, pop, stover ...... 0.5 by measuring only prometryn, 2,4- Corn, sweet, forage ...... 15 Corn, sweet, kernel plus cob with husks re- bis(isopropylamino)-6-methylthio-s-tri- moved ...... 0 .20 azine, in or on the following raw agri- Corn, sweet, stover ...... 2 .0 cultural commodities: Goat, fat ...... 0 .02 Goat, meat ...... 0.02 Parts per Goat, meat byproducts ...... 0 .02 Commodity million Grass, forage ...... 4 .0 Grass, hay ...... 4 .0 Bean, snap, succulent ...... 0 .05 Guava ...... 0 .05 Carrot, roots ...... 0.45 Horse, fat ...... 0 .02 Celeriac, roots ...... 0 .05 Horse, meat ...... 0 .02 Celeriac, tops ...... 0 .20 Horse, meat byproducts ...... 0 .02 Cilantro, leaves ...... 3 .5 Milk ...... 0.02 Coriander, dried leaves ...... 9.0 Nut, macadamia ...... 0.20 Cotton, gin byproducts ...... 1 .0 Sheep, fat ...... 0 .02 Cotton, undelinted seed ...... 0 .25 Sheep, meat ...... 0.02 Dill, oil ...... 1 .3 Sheep, meat byproducts ...... 0 .02 Dillweed, dried leaves ...... 1 .1 Sorghum, forage, forage ...... 0 .25 Dillweed, fresh leaves ...... 0 .30 Sorghum, grain, forage ...... 0.25 Leaf petioles subgroup 4B ...... 0 .50 Sorghum, grain, grain ...... 0 .20 Okra ...... 0.05 Sorghum, grain, stover ...... 0 .50 Parsley, dried leaves ...... 1 .5 Sugarcane, cane ...... 0.20 Parsley, leaves ...... 0.60 Wheat, forage ...... 1 .5 Pea, pigeon, seed ...... 0 .25 Wheat, grain ...... 0 .10

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(b) Section 18 emergency exemptions. Commodity Parts per [Reserved] million (c) Tolerances with regional exemptions. Coffee, bean, green ...... 0 .1 [Reserved] Corn, field, grain ...... 0 .1 (d) Indirect or inadvertent residues. Corn, pop, grain ...... 0.1 Cotton, undelinted seed ...... 0 .1 Tolerances are established for indirect Date, dried fruit ...... 0 .1 or inadvertent residues of the herbicide Dill, seed ...... 0 .01 prometryn, including its metabolites Eggplant ...... 0.01 Endive ...... 0.01 and degradates, in or on the commod- Grapefruit ...... 0 .01 ities in the following table. Compliance Hazelnut ...... 0 .1 with the tolerance levels specified in Kumquat ...... 0 .01 the following table is to be determined Lemon ...... 0.01 Lettuce ...... 0.01 by measuring only prometryn, 2,4- Lime ...... 0.01 bis(isopropylamino)-6-methylthio-s-tri- Mango ...... 0.01 azine, in or on the following raw agri- Millet, grain ...... 0 .1 Mushroom ...... 0 .01 cultural commodities. Nut, brazil ...... 0 .1 Oat, grain ...... 0 .1 Commodity Parts per Okra ...... 0.01 million Orange, sweet ...... 0 .01 Papaya ...... 0 .01 Barley, forage ...... 0 .3 Peanut ...... 0 .1 Barley, hay ...... 1 .0 Pecan ...... 0 .1 Barley, straw ...... 0 .3 Pepper ...... 0 .01 Oat, forage ...... 0 .3 Persimmon ...... 0 .01 Oat, hay ...... 1.0 Pistachio ...... 0.1 Oat, straw ...... 0.3 Rice, grain ...... 0 .1 Rye, forage ...... 0 .3 Rye, grain ...... 0.1 Rye, hay ...... 1 .0 Safflower, seed ...... 0 .1 Rye, straw ...... 0 .3 Salsify, tops ...... 0 .01 Triticale, forage ...... 0 .3 Sesame, seed ...... 0 .1 Triticale, hay ...... 1 .0 Sorghum, grain ...... 0 .1 Triticale, straw ...... 0 .3 Soybean, seed ...... 0 .1 Wheat, forage ...... 0 .3 Sunflower, seed ...... 0.1 Wheat, hay ...... 1 .0 Sweet potato, roots ...... 0 .01 Wheat, straw ...... 0 .3 Tangelo ...... 0 .01 Tangerine ...... 0 .01 [43 FR 29121, July 6, 1978, as amended at 45 Tomato ...... 0.01 FR 51782, Aug. 5, 1980; 54 FR 6918, Feb. 15, Vegetable, legume, group 6, except soybean .... 0 .01 Walnut ...... 0 .1 1989; 60 FR 20434, Apr. 26, 1995; 63 FR 17692, Wheat, grain ...... 0 .1 Apr. 10, 1998; 63 FR 57075, Oct. 26, 1998; 64 FR 39082, July 21, 1999; 74 FR 47456, Sept. 16, 2009; (2) Tolerances are established for res- 74 FR 67108, Dec. 18, 2009; 76 FR 34885, June 15, 2011; 78 FR 55640, Sept. 11, 2013] idues of the fumigant in or on all RACs resulting from preharvest treatment of § 180.225 Phosphine; tolerances for pest burrows in agricultural and non- residues. crop land areas.

(a) General. (1) Tolerances are estab- Parts per lished for residues of phosphine in or Commodity million on the following raw agricultural com- All raw agricultural commodities resulting from modities (RACs) resulting from post- preharvest treatment of pest burrows ...... 0 .01 harvest fumigation for the control of insects with phosphine gas or (3) Residues resulting from fumiga- phosphide compounds that produce tion of processed food: phosphine gas. Commodity Parts per Parts per million Commodity million Processed food ...... 0 .01 Almond ...... 0.1 Avocado ...... 0 .01 (4) Residues resulting from fumigation Banana ...... 0.01 of animal feed: Barley, grain ...... 0 .1 Cabbage, Chinese, bok choy ...... 0.01 Parts per Cabbage, Chinese, napa ...... 0 .01 Commodity million Cacao bean, dried bean ...... 0 .1 Cashew ...... 0 .1 Animal feed ...... 0.1 Citron, citrus ...... 0 .01

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(5) To assure safe use of this pes- Commodity Parts per ticide, it must be used in compliance million with the labeling conforming to that Sheep, meat ...... 0.05 registered by the U.S. Environmental Sheep, meat byproducts ...... 0 .05 Protection Agency (EPA) under FIFRA. Labeling shall bear a restric- (2)(i) Tolerances are established for tion to aerate the finished food/feed for residues of the herbicide diquat (6,7 48 hours before it is offered to the con- dihydrodipyrido(1,2-a:2’1’- sumer, unless EPA specifically deter- c)pyrazinediium) (calculated as the mines that a different time period is cation) derived from the application of appropriate. Where appropriate, a the dibromide salt to ponds, lakes, res- warning shall state that under no con- ervoirs, marshes, drainage ditches, ca- dition should any formulation con- nals, streams, and rivers which are taining aluminum or magnesium slow-moving or quiescent in programs phosphide be used so that it will come of the Corp of Engineers or other Fed- in contact with any processed food, ex- eral or State public agencies and to cept processed brewer’s rice, malt, and ponds, lakes and drainage ditches only corn grits stored in breweries for use in where there is little or no outflow of the manufacture of beer. water and which are totally under the (b) Section 18 emergency exemptions. control of the user, in or on the fol- [Reserved] lowing food commodities: (c) Tolerances with regional registra- Parts per tions. [Reserved] Commodity million (d) Indirect or inadvertant residues. [Reserved] Avocado ...... 0 .2 Berry group 13 ...... 0 .05 [64 FR 72950, Dec. 29, 1999, as amended at 71 Cotton, undelinted seed ...... 0 .2 FR 74816, Dec. 13, 2006; 72 FR 41929, Aug. 1, Cranberry ...... 0 .05 2007; 74 FR 46372, Sept. 9, 2009] Fish ...... 2 .0 Fruit, citrus, group 10 ...... 0 .05 § 180.226 Diquat; tolerances for resi- Fruit, pome, group 11 ...... 0.02 dues. Fruit, stone, group 12 ...... 0 .02 Grain, cereal, forage, fodder and straw, group (a) General. (1) Tolerances are estab- 16 ...... 0 .02 lished for residues of the plant growth Grain, cereal, group 15 ...... 0.02 regulator and herbicide diquat, (6,7- Grape ...... 0 .05 dihydrodipyrido (1,2-a:2′1′- Grass, forage, fodder and hay, group 17 ...... 0 .2 c)pyrazinediium) derived from applica- Hop, dried cones ...... 0 .2 Nut, tree, group 14 ...... 0 .02 tion of the dibromide salt and cal- Shellfish ...... 20 .0 culated as the cation in or on the fol- Strawberry ...... 0 .05 lowing food commodities: Sugarcane, cane ...... 0.2 Vegetable, brassica, leafy, group 5 ...... 0.05 Commodity Parts per Vegetable, cucurbit, group 9 ...... 0.02 million Vegetable, foliage of legume, group 7 ...... 0 .2 Vegetable, fruiting, group 8 ...... 0.05 Alfalfa, seed ...... 3 .0 Vegetable, leafy, except brassica, group 4 ...... 0 .05 Cattle, fat ...... 0.05 Cattle, meat ...... 0 .05 Vegetable, root and tuber, group 1 ...... 0 .02 Cattle, meat byproducts ...... 0.05 Vegetable, seed and pod ...... 0 .05 Canola, meal ...... 6 .0 Canola, seed ...... 2 .0 (ii) Where tolerances are established Egg ...... 0 .05 at higher levels from other uses of Goat, fat ...... 0 .05 Goat, meat ...... 0.05 diquat on the subject crops, the higher Goat, meat byproducts ...... 0 .05 tolerances applies also to residues of Hog, fat ...... 0 .05 the aquatic uses cited in this para- Hog, meat ...... 0 .05 Hog, meat byproducts ...... 0 .05 graph. Horse, fat ...... 0 .05 (3) Tolerances are established for the Horse, meat ...... 0 .05 plant growth regulator diquat (6,7 Horse, meat byproducts ...... 0 .05 Milk ...... 0.02 dihydrodipyrido(1,2-a:2’1’- Potato ...... 0 .1 c)pyrazinediium) derived from applica- Poultry, fat ...... 0.05 tion of the dibromide salt and cal- Poultry, meat ...... 0 .05 Poultry, meat byproducts ...... 0.05 culated as the cation in or on the fol- Sheep, fat ...... 0 .05 lowing food commodites:

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Parts per Parts per Commodity million Commodity million

Banana1 ...... 0 .05 Sorghum, grain, grain ...... 4 .0 Coffee, bean, green1 ...... 0 .05 Sorghum, grain, stover ...... 10 .0 Soybean, hulls ...... 0 .6 Sugarcane, cane ...... 0.3 1There are no U.S. registrations as of May 26, 2010. Sugarcane, molasses ...... 5 .0 Teff, forage ...... 90.0 (4) A tolerance of 0.5 part per million Teff, grain ...... 6 .0 is established for residues of diquat in Teff, hay ...... 40.0 potato, granules/flakes and potato, Teff, straw ...... 30 .0 chips. Wheat, forage ...... 90.0 (b) Section 18 emergency exemptions. Wheat, grain ...... 2 .0 Wheat, hay ...... 40 .0 [Reserved] Wheat, straw ...... 30 .0 (c) Tolerances with regional registra- tions. [Reserved] (2) Tolerances are established for res- (d) Indirect or inadvertent residues. idues of the herbicide dicamba, 3,6- [Reserved] dichloro-o-anisic acid, including its [65 FR 33709, May 24, 2000, as amended at 72 metabolites and degradates, in or on FR 41929, Aug. 1, 2007; 75 FR 29441, May 26, the commodities in the table below. 2010; 75 FR 60241, Sept. 29, 2010] Compliance with the tolerance levels is to be determined by measuring only § 180.227 Dicamba; tolerances for resi- the residues of dicamba (3,6-dichloro-o- dues. anisic acid) and its metabolite, 3,6- (a) General. (1) Tolerances are estab- dichloro-2-hydroxybenzoic acid, cal- lished for the residues of the herbicide culated as the stoichiometric equiva- dicamba (3,6-dichloro-o-anisic acid), in- lent of dicamba, in or on the following cluding its metabolites and degradates, commodities: in or on the commodities in the table below. Compliance with the tolerance Parts per Commodity million levels is to be determined by meas- uring only the sum of the residues of Asparagus ...... 4.0 dicamba (3,6-dichloro-o-anisic acid) and Cattle, fat ...... 0.3 its metabolite, 3,6-dichloro-5-hydroxy- Cattle, kidney ...... 25 .0 Cattle, meat ...... 0 .25 o-anisic acid, calculated as the stoi- Cattle, meat byproducts, except kidney ...... 3.0 chiometric equivalent of dicamba, in or Goat, fat ...... 0 .3 on the following commodities: Goat, kidney ...... 25.0 Goat, meat ...... 0.25 Commodity Parts per Goat, meat byproducts, except kidney ...... 3 .0 million Hog, fat ...... 0 .3 Barley, grain ...... 6 .0 Hog, kidney ...... 25.0 Barley, hay ...... 2 .0 Hog, meat ...... 0 .25 Barley, straw ...... 15 .0 Hog, meat byproducts, except kidney ...... 3 .0 Corn, field, forage ...... 3 .0 Horse, fat ...... 0 .3 Corn, field, grain ...... 0 .1 Horse, kidney ...... 25 .0 Corn, field, stover ...... 3 .0 Horse, meat ...... 0 .25 Corn, pop, grain ...... 0.1 Horse, meat byproducts, except kidney ...... 3 .0 Corn, pop, stover ...... 3.0 Milk ...... 0.2 Corn, sweet, forage ...... 0 .50 Sheep, fat ...... 0 .3 Corn, sweet, kernel plus cob with husks re- Sheep, kidney ...... 25.0 moved ...... 0 .04 Corn, sweet, stover ...... 0 .50 Sheep, meat ...... 0.25 Cotton, undelinted seed ...... 0 .2 Sheep, meat byproducts, except kidney ...... 3 .0 Grass, forage, fodder and hay, group 17, forage 125 .0 Grass, forage, fodder and hay, group 17, hay .... 200 .0 (3) Tolerances are established for res- Millet, proso, forage ...... 90.0 idues of the herbicide dicamba, 3,6- Millet, proso, grain ...... 2 .0 Millet, proso, hay ...... 40 .0 dichloro-o-anisic acid, including its Millet, proso, straw ...... 30 .0 metabolites and degradates, in or on Oat, forage ...... 90 .0 the commodities in the table below. Oat, grain ...... 2 .0 Oat, hay ...... 40.0 Compliance with the tolerance levels is Oat, straw ...... 30.0 to be determined by measuring only Rye, forage ...... 90 .0 the residues of dicamba, 3,6-dichloro-o- Rye, grain ...... 2.0 Rye, straw ...... 30 .0 anisic acid, and its metabolites, 3,6- Sorghum, grain, forage ...... 3.0 dichloro-5-hydroxy-o-anisic acid, and

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3,6-dichloro-2-hydroxybenzoic acid, cal- Commodity Parts per culated as the stoichiometric equiva- million lent of dicamba, in or on the following Sheep, meat byproducts ...... 0 .1 commodities: (b) Section 18 emergency exemptions. Parts per Commodity million [Reserved] (c) Tolerances with regional registra- Grain, aspirated fractions ...... 1000 Soybean, hulls ...... 30 .0 tions. [Reserved] Soybean, seed ...... 10.0 (d) Indirect or inadvertent residues. Tolerances are established for the com- (b) Section 18 emergency exemptions. bined residues of the herbicide [Reserved] fluometuron, N, N-dimethyl-N’-[3- (c) Tolerances with regional registra- (trifluoromethyl)phenyl], and its tions. [Reserved] metabolite, trifluoromethylaniline (d) Indirect or inadvertent residues. (TFMA) determined as TFMA, in or on [Reserved] the following food commodities.

[65 FR 33709, May 24, 2000, as amended at 72 Parts per FR 35665, June 29, 2007; 73 FR 17918, Apr. 2, Commodity million 2008; 73 FR 54960, Sept. 24, 2008; 75 FR 60241, Sept. 29, 2010; 76 FR 55806, Sept. 9, 2011] Grain, cereal, forage, fodder, and straw group 16, forage ...... 3 .0 § 180.229 Fluometuron; tolerances for Grain, cereal, forage, fodder, and straw, group residues. 16, stover ...... 6 .0 Grain, cereal, group 15 ...... 0.5 (a) General. (1) Tolerances are estab- Peanut ...... 0 .1 lished for the combined residues of the Peanut, hay ...... 4.0 herbicide fluometuron, N, N-dimethyl- Peanut, meal ...... 0 .2 N’-[3-(trifluoromethyl)phenyl]urea, and Soybean, forage ...... 3 .0 Soybean, hay ...... 3 .0 its metabolite, trifluoromethylaniline Soybean, seed ...... 2 .0 (TFMA) determined as TFMA, in or on Rice, hulls ...... 1 .0 the following food commodities: Wheat, milled byproducts ...... 1 .0

Commodity Parts per million [73 FR 52613, Sept. 10, 2008]

Cotton, gin byproducts ...... 3 .5 Cotton, undelinted seed ...... 1 .0 § 180.231 Dichlobenil; tolerances for residues. (2) Tolerances are established for the (a) General. Tolerances are estab- combined residues of the herbicide lished for the combined residues of the fluometuron, N,N-dimethyl-N’-[3- herbicide dichlobenil (2,6- (trifluoromethyl)phenyl]urea, and its dichlorobenzonitrile) and its metabo- metabolites determined as TFMA and lite 2,6-dichlorobenzamide in or on the the hydroxylated metabolites: CGA- following raw agricultural commod- 236431, 1-(4-hydroxy-3- ities: trifluoromethylphenyl)urea; CGA- 236432, 1-methyl-3-(4-hydroxy-3- Parts per Commodity million trifluoromethylphenyl)urea; and CGA- 13211, 1,1-dimethyl-3-(4-hydroxy-3- Apple ...... 0.5 trifluoromethylphenyl)urea, in or on Bushberry subgroup 13–07B ...... 0 .15 the following food commodities: Caneberry subgroup 13–07A ...... 0.10 Cranberry ...... 0 .1 Fruit, stone, group 12 ...... 0 .15 Commodity Parts per million Grape ...... 0 .15 Hazelnut ...... 0 .1 Cattle, meat byproducts ...... 0.1 Pear ...... 0 .5 Egg ...... 0 .1 Rhubarb ...... 0 .06 Goat, meat byproducts ...... 0 .1 Hog, meat byproducts ...... 0 .1 Horse, meat byproducts ...... 0 .1 (b) Section 18 emergency exemptions. Milk ...... 0.02 [Reserved] Poultry, fat ...... 0.1 Poultry, meat ...... 0 .1 (c) Tolerances with regional registra- Poultry, meat byproducts ...... 0.1 tion. [Reserved]

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(d) Indirect or inadvertent residues. Commodity Parts per [Reserved] million [36 FR 22540, Nov. 25, 1971, as amended at 63 Poultry, meat byproducts ...... 0.05(N) FR 57075, Oct. 26, 1998; 66 FR 63198, Dec. 5, Raw agricultural commodities, nonperishable, bulk stored regardless of fat content, 2001; 73 FR 50570, Aug. 27, 2008] postharvest ...... 0.5 Raw agricultural commodities nonperishable, § 180.232 Butylate; tolerances for resi- packaged or bagged, containing 6 percent fat dues. or less, postharvest ...... 0.5 Raw agricultural commodities, nonperishable, (a) General. Tolerances are estab- packaged or bagged, containing more than 6 lished for residues of the herbicide percent fat, postharvest ...... 2 butylate, including its metabolites and Sheep, fat ...... 0 .02(N) Sheep, meat ...... 0.02(N) degradates, in or on the commodities Sheep, meat byproducts ...... 0 .02(N) in the table in this paragraph. Compli- ance with the tolerance levels specified (2) The tolerance of 0.1 part per mil- in this paragraph is to be determined lion prescribed by 21 CFR 556.180 for by measuring only butylate, S-ethyl bis negligible residues of 2,2-dichlorovinyl (2-methylpropyl) carbamothioate, in or dimethyl phosphate in hog, fat; hog, on the commodity. meat; hog, meat byproducts; and hog, skin covers both its use as an anthel- Expiration/ Parts per mintic in swine feed and as an insecti- Commodity million revocation date cide applied directly to swine. Corn, field, forage ...... 0.1 3/23/13 (3) Dichlorvos may be present as a Corn, field, grain ...... 0.1 3/23/13 residue from application as an insecti- Corn, field, stover ...... 0.1 3/23/13 cide on packaged or bagged nonperish- Corn, pop, grain ...... 0.1 3/23/13 Corn, pop, stover ...... 0.1 3/23/13 able processed food (see: 21 CFR Corn, sweet, forage ...... 0.1 3/23/13 170.3(j)) in an amount in such food not Corn, sweet, kernel plus cob with in excess of 0.5 part per million (ppm). husks removed ...... 0.1 3/23/13 To assure safe use of the insecticide, its label and labeling shall conform to (b) Section 18 emergency exemptions. the label and labeling registered by the [Reserved] U.S. Environmental Protection Agen- (c) Tolerances with regional registra- cy, and the usage employed shall con- tions. [Reserved] form with such label or labeling. (d) Indirect or inadvertent residues. (b) Section 18 emergency exemptions. [Reserved] [Reserved] [68 FR 39439, July 1, 2003, as amended at 76 (c) Tolerances with regional registra- FR 23493, Apr. 27, 2011; 77 FR 59125, Sept. 26, tions. [Reserved] 2012] (d) Indirect or inadvertent residues. [Reserved] § 180.235 Dichlorvos; tolerances for residues. [47 FR 55223, Dec. 8, 1982, as amended at 55 FR 26440, June 28, 1990; 56 FR 29183, June 26, (a) General. (1) Tolerances for resi- 1991; 63 FR 57075, Oct. 26, 1998; 65 FR 33697, dues of the insecticide 2,2-dichlorovinyl May 24, 2000; 74 FR 46373, Sept. 9, 2009; 77 FR dimethyl phosphate are established as 59125, Sept. 26, 2012] follows: § 180.236 Triphenyltin hydroxide; tol- Parts per erances for residues. Commodity million (a) General. Tolerances are estab- Cattle, fat ...... 0.02(N) lished for the combined residues of the Cattle, meat ...... 0 .02(N) Cattle, meat byproducts ...... 0.02(N) fungicide triphenyltin hydroxide Egg ...... 0 .05(N) (TPTH) and its monophenyltin (MPTH) Goat, fat ...... 0 .02(N) and diphenyltin (DPTH) hydroxide and Goat, meat ...... 0.02(N) Goat, meat byproducts ...... 0 .02(N) oxide metabolites, expressed in terms Horse, fat ...... 0 .02(N) of parent TPTH, in or on the following Horse, meat ...... 0 .02(N) raw agricultural commodities: Horse, meat byproducts ...... 0 .02(N) Milk ...... 0.02(N) Parts per Mushroom (residues expressed as naled) ...... 0 .5 Commodity million Poultry, fat ...... 0.05(N) Poultry, meat ...... 0 .05(N) Beet, sugar, roots ...... 0 .05

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Parts per Parts per Commodity million Commodity million

Beet, sugar, tops ...... 10.0 Carrot, roots ...... 0.10 Cattle, fat ...... 0.2 Cattle, kidney ...... 2 .0 (d) Indirect or inadvertent residues. Cattle, liver ...... 4 .0 Cattle, meat ...... 0 .5 [Reserved] Goat, fat ...... 0 .2 Goat, kidney ...... 2 .0 [68 FR 39440, July 1, 2003, as amended at 73 Goat, liver ...... 4.0 FR 53738, Sept. 17, 2008] Goat, meat ...... 0.5 Hog, fat ...... 0 .3 § 180.242 Thiabendazole; tolerances for Hog, meat ...... 0 .06 residues. Hog, meat byproducts ...... 0 .3 Horse, fat ...... 0 .2 (a) General. (1) Tolerances are estab- Horse, kidney ...... 2 .0 lished for residues of thiabendazole, in- Horse, liver ...... 4 .0 Horse, meat ...... 0 .5 cluding its metabolites and degradates, Milk ...... 0.06 in or on the commodities in the table Pecan ...... 0 .05 below. Compliance with the tolerance Potato ...... 0 .05 Sheep, fat ...... 0 .2 levels specified below is to be deter- Sheep, kidney ...... 2.0 mined by measuring only the sum of Sheep, liver ...... 4.0 thiabendazole (2-(4- Sheep, meat ...... 0.5 thiazolyl)benzimidazole) and its me- tabolite benzimidazole (free and con- (b) Section 18 emergency exemptions. jugated), calculated as the stoichio- [Reserved] metric equivalent of thiabendazole, in (c) Tolerances with regional registra- or on the commodity. tions. [Reserved] (d) Indirect or inadvertent residues. Commodity Parts per [Reserved] million [72 FR 41929, Aug. 1, 2007] Alfalfa, forage ...... 0.02 Alfalfa, hay ...... 0.02 Apple, wet pomace ...... 12.0 § 180.241 Bensulide; tolerances for res- Avocado 1 ...... 10.0 idues. Banana, postharvest ...... 3 .0 (a) General. Tolerances are estab- Barley, grain ...... 0 .05 Barley, hay ...... 0 .30 lished for the residues of S-(O,O- Barley, straw ...... 0 .30 diisopropyl phosphorodithioate) of N- Bean, dry, seed ...... 0 .1 (2-mercaptoethyl) benzenesulfonamide Brassica, head and stem, subgroup 5A ...... 0 .02 Cantaloupe 1 ...... 15.0 including its oxygen analog S-(O,O- Carrot, roots, postharvest ...... 10 .0 diisopropyl phosphorothioate) of N-(2- Citrus, oil ...... 15.0 mercaptoethyl) benzenesulfonamide in Corn, field, forage ...... 0 .01 Corn, field, grain ...... 0 .01 or on the following food commodities: Corn, field, stover ...... 0 .01 Corn, pop, forage ...... 0 .01 Parts per Corn, pop, grain ...... 0.01 Commodity million Corn, pop, stover ...... 0.01 Corn, sweet, forage ...... 0 .01 Onion, bulb ...... 0 .10 Corn, sweet, kernels plus cop with husks re- Vegetable, brassica, leafy group 5 ...... 0 .15 moved ...... 0 .01 Vegetable, cucurbits group 9 ...... 0 .15 Vegetable, fruiting group 8 ...... 0 .10 Corn, sweet, stover ...... 0 .01 Vegetable, leafy except brassica group 4 ...... 0 .15 Fruit, citrus, group 10, postharvest ...... 10 .0 Fruit, pome, group 11, postharvest ...... 5 .0 Mango ...... 10.0 (b) Section 18 emergency exemptions. Mushroom ...... 40 .0 [Reserved] Oats, forage ...... 0 .30 (c) Tolerances with regional registra- Oats, grain ...... 0 .05 Oats, hay ...... 0.30 tions. Tolerances with regional reg- Oats, straw ...... 0.30 istration, as defined in § 180.1(l), are es- Onion, bulb, subgroup 3–07A ...... 0 .02 tablished for the residues of S-(O,O- Papaya, postharvest ...... 5 .0 diisopropyl phosphorodithioate) of N- Potato, postharvest ...... 10 .0 Radish, tops ...... 0 .02 (2-mercaptoethyl) benzenesulfonamide Rye, forage ...... 0 .30 including its oxygen analog S-(O,O- Rye, grain ...... 0.05 diisopropyl phosphorothioate) of N-(2- Rye, straw ...... 0 .30 Soybean ...... 0.1 mercaptoethyl) benzenesulfonamide in Spinach ...... 0 .02 or on the following food commodities: Strawberry 1 ...... 5 .0

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table. Compliance with the tolerance Commodity Parts per million levels specified in this paragraph is to Sweet potato (postharvest to sweet potato in- be determined by measuring only the tended only for use as seed) ...... 0 .05 sum of propazine, 2-chloro-4,6- Triticale, forage ...... 0 .30 bis(isopropylamino)-s-triazine, and its Triticale, grain ...... 0 .05 Triticale, hay ...... 0 .30 two chlorinated degradates, 2-amino-4- Triticale, straw ...... 0 .30 chloro-6-isopropylamino-s-triazine and Vegetable, cucurbit, group 9 ...... 0.02 2,4-diamino-6-chloro-s-triazine, cal- Vegetable, root (except sugarbeet), subgroup 1B ...... 0 .02 culated as the stoichiometric equiva- Wheat, forage ...... 0 .30 lent of propazine, in or on the com- Wheat, grain ...... 0 .05 modity. Wheat, hay ...... 0 .30 Wheat, straw ...... 0 .30 Commodity Parts per 1There are no U.S. registrations on the indicated million commodity. Sorghum, grain, forage ...... 0.25 (2) Tolerances are established for res- Sorghum, grain, grain ...... 0 .25 idues of thiabendazole, including its Sorghum, grain, stover ...... 0 .25 metabolites and degradates, in or on the commodities in the table below. (b) Section 18 emergency exemptions. Compliance with the tolerance levels [Reserved] specified below is to be determined by (c) Tolerances with regional registra- measuring only the sum of tions. [Reserved] thiabendazole (2-(4- (d) Indirect or inadvertent residues. thiazolyl)benzimidazole) and its me- [Reserved] tabolites 5-hydroxythiabendazole (free and conjugated) and benzimidazole [75 FR 60242, Sept. 29, 2010] (free and conjugated), calculated as the stoichiometric equivalent of § 180.245 Streptomycin; tolerances for residues. thiabendazole, in or on the commodity. (a) General. (1) Tolerances are estab- Parts per lished for residues of the fungicide Commodity million streptomycin in or on food commod- Cattle, meat ...... 0 .1 ities as follows: Cattle, meat byproducts ...... 0.4 Goat, meat byproducts ...... 0 .4 Parts per Hog, meat byproducts ...... 0 .3 Commodity million Horse, meat byproducts ...... 0 .4 Milk ...... 0.1 Bean, dry, seed ...... 0 .5 Sheep, meat byproducts ...... 0 .4 Bean, succulent ...... 0 .5 Fruit, pome, group 11 ...... 0.25 (b) Section 18 emergency exemptions. [Reserved] (2) Tolerances are established for res- (c) Tolerances with regional exemptions. idues of the fungicide streptomycin [Reserved] from treatment of seedling plants be- (d) Indirect or inadvertent residues. fore transplanting in or on the fol- [Reserved] lowing food commodities: [42 FR 32783, June 28, 1977] Commodity Parts per EDITORIAL NOTE: For FEDERAL REGISTER ci- million tations affecting § 180.242, see the List of CFR Sections Affected, which appears in the Celery ...... 0 .25 Finding Aids section of the printed volume Pepper ...... 0 .25 and at www.fdsys.gov. Tomato ...... 0.25

§ 180.243 Propazine; tolerances for res- (3) Tolerances are established for res- idues. idues of the fungicide streptomycin (a) General. Tolerances are estab- from treatment of seed pieces in or on lished for residues of the herbicide the following food commodity: propazine, 2-chloro-4,6- Parts per bis(isopropylamino)-s-triazine, includ- Commodity million ing its metabolites and degradates, in or on the commodities in the following Potato ...... 0 .25

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(b) Section 18 emergency exemptions. Commodity Parts per Time-limited tolerances are estab- million lished for residues of streptomycin, in Hog, meat ...... 0 .02 or on the agricultural commodities, as Horse, fat ...... 0 .02 specified in the following table, result- Horse, meat byproducts ...... 0 .02 Horse, meat ...... 0 .02 ing from use of the pesticide pursuant Milk ...... 0.02 to FIFRA section 18 emergency exemp- Peanut ...... 0 .5 tions. Compliance with the tolerance Poultry, fat ...... 0.02 levels listed in the following table is to Poultry, meat byproducts ...... 0.02 Poultry, meat ...... 0 .02 be determined by measuring the levels Sheep, fat ...... 0 .02 of streptomycin only, in or on the com- Sheep, meat byproducts ...... 0 .02 modities listed in the table. The toler- Sheep, meat ...... 0.02 Sorghum grain, forage ...... 2 .0 ances expire on the dates specified in Sorghum, grain, grain ...... 0 .1 the table. Sorghum, grain, stover ...... 1 .0 Soybeans, seed ...... 1 .0 Sunflower, meal ...... 3 .4 Commodity Parts per Expiration million date Sunflower, seed ...... 2.5

Grapefruit ...... 0.15 12/31/2015 Grapefruit, dried pulp ...... 0.40 12/31/2015 (b) Section 18 emergency exemptions. [Reserved] (c) Tolerances with regional registra- (c) Tolerances with regional registra- tions. [Reserved] tions. [Reserved] (d) Indirect or inadvertent residues. (d) Indirect or inadvertent residues. [Reserved] Tolerances are established for indirect or inadvertent residues of alachlor (2- [68 FR 39440, July 1, 2003, as amended at 73 chloro-2′,6′-diethyl-N- FR 54960, Sept. 24, 2008; 78 FR 29055, May 17, 2013] (methoxymethyl)acetanilide) and its metabolites which can be converted to § 180.249 Alachlor; tolerances for resi- 2,6-diethylaniline (DEA) or 2-ethyl-6-(1- dues. hydroxyethyl) (1-HEEA) upon (a) General. Tolerances are estab- basic hydrolysis, calculated as lished for combined residues of alachlor, in or on the following raw ag- alachlor (2-chloro-2′,6′’-diethyl-N- ricultural commodities when present (methoxymethyl)acetanilide) and its therein as a result of the application of metabolites which can be converted to alachlor to the growing crops in para- 2,6-diethylaniline (DEA) or 2-ethyl-6-(1- graph (a) of this section: hydroxyethyl)aniline (1-HEEA) upon Parts per basic hydrolysis, calculated as alachlor Commodity million in or on the following raw agricultural Animal feed, nongrass, group 18, forage ...... 1 .4 commodities. Animal feed, nongrass, group 18, hay ...... 1.2 Grain, cereal, forage, and straw, group 16 ex- Commodity Parts per cept corn, sorghum, rice, straw ...... 0 .8 million Grain, cereal, forage, fodder and straw, group 16 except corn, sorghum, rice, forage ...... 0 .6 Beans, dry ...... 0.1 Grain, cereal, forage, fodder, and straw, group Beans, succulent lima ...... 0 .1 16 except for corn, sorghum, rice, hay ...... 0 .8 Cattle, fat ...... 0.02 Grain, cereal, group 15 except corn, sorghum, Cattle, meat byproducts ...... 0.02 rice ...... 0 .05 Cattle, meat ...... 0 .02 Corn, field, forage ...... 2 .0 Corn, field, grain ...... 0 .2 [72 FR 54584, Sept. 26, 2007] Corn, field, pop ...... 0 .2 Corn, field, stover ...... 2 .0 Corn, pop, stover ...... 2.0 § 180.252 Tetrachlorvinphos; toler- Corn, sweet (K+CWHR) ...... 0.05 ances for residues. Corn, sweet, stover ...... 2 .0 Cotton, gin byproducts ...... 0 .7 (a) General. Tolerances are estab- Cotton, undelinted seed ...... 0 .03 lished for the combined residues of the Cowpea, forage ...... 5 .0 insecticide tetrachlorvinphos [(Z)-2- Cowpea, hay ...... 5 .0 Egg ...... 0 .02 chloro-1-(2,4,5-trichlorophenyl) vinyl Goat, fat ...... 0 .02 dimethyl phosphate], including its me- Goat, meat byproducts ...... 0 .02 tabolites, 1-(2,4,5-trichlorophenyl)-eth- Goat, meat ...... 0.02 Hog, fat ...... 0 .02 anol (free and conjugated forms), 2,4,5- Hog meat byproducts ...... 0 .02 trichloroacetophenone, and 1-(2,4,5-

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trichlorophenyl)-ethanediol, in or on Parts per Expiration/ the following commodities: Commodity revocation million date

Parts per Asparagus ...... 2 None Commodity million Avocado ...... 2 None Cattle, fat (of which no more than 0.1 ppm is Barley, grain ...... 1 None Barley, hay ...... 10 None tetrachlorvinphos per se) ...... 0 .2 Barley, straw ...... 10 None Cattle, kidney (of which no more than 0.05 Bean, dry, seed ...... 0.1 None ppm is tetrachlorvinphos per se) ...... 1 .0 Bean, forage ...... 10 None Cattle, liver (of which no more than 0.05 ppm Bean, succulent ...... 2 None is tetrachlorvinphos per se) ...... 0 .5 Beet, garden, tops ...... 6 None Cattle, meat (of which no more than 2.0 ppm is Bermudagrass, forage ...... 10 None tetrachlorvinphos per se) ...... 2 .0 Bermudagrass, hay ...... 40 None Cattle, meat byproducts, except kidney and Blueberry ...... 6 None liver ...... 1 .0 Egg (of which no more than 0.05 ppm is Broccoli ...... 3 None Brussels sprouts ...... 2 None tetrachlorvinphos per se) ...... 0 .2 Hog, fat (of which no more than 0.1 ppm is Cabbage ...... 5 None tetrachlorvinphos per se) ...... 0 .2 Cabbage, Chinese, bok choy ...... 5 None Hog, kidney (of which no more than 0.05 ppm Cabbage, Chinese, napa ...... 5 None is tetrachlorvinphos per se) ...... 1.0 Cauliflower ...... 2 None Hog, liver (of which no more than 0.05 ppm is Celery ...... 3 None tetrachlorvinphos per se) ...... 0 .5 Collards ...... 6 None Hog, meat (of which no more than 2.0 ppm is Corn, field, forage ...... 10 None tetrachlorvinphos per se) ...... 2.0 Corn, field, grain ...... 0.1 None Hog, meat byproducts, except kidney and liver 1 .0 Corn, field, stover ...... 10 None Milk, fat (reflecting negligible residues in whole Corn, pop, grain ...... 0.1 None milk and of which no more than 0.05 ppm is Corn, pop, stover ...... 10 None tetrachlorvinphos per se) ...... 0 .05 Corn, sweet, forage ...... 10 None Poultry, fat (of which no more than 7.0 ppm is Corn, sweet, kernel plus cob with tetrachlorvinphos per se) ...... 7 .0 husks removed ...... 0.1 None Poultry, liver (of which no more than 0.05 ppm Corn, sweet, stover ...... 10 None is tetrachlorvinphos per se) ...... 2 .0 Cotton, undelinted seed ...... 0.1 None Poultry, meat (of which no more than 3.0 ppm Dandelion, leaves ...... 6 None is tetrachlorvinphos per se) ...... 3 .0 Endive ...... 5 None Poultry, meat byproducts, except liver ...... 2 .0 Grape ...... 5 12/31/16 Grapefruit ...... 2 None Hop, dried cones 1 ...... 12 None (b) Section 18 emergency exemptions. Kale ...... 6 None [Reserved] Lemon ...... 2 None (c) Tolerances with regional registra- Lentil, seed ...... 0.1 None Lettuce ...... 5 None tions. [Reserved] Mustard greens ...... 6 None (d) Indirect or inadvertent residues. Nectarine ...... 5 None [Reserved] Oat, forage ...... 10 None Oat, grain ...... 1 None [76 FR 57659, Sept. 16, 2011, as amended at 78 Oat, hay ...... 10 None FR 15882, Mar. 13, 2013; 78 FR 53684, Aug. 30, Oat, straw ...... 10 None 2013] Onion, green ...... 3 None Orange ...... 2 None Parsley, leaves ...... 6 None § 180.253 Methomyl; tolerances for res- Pea ...... 5 None idues. Pea, field, vines ...... 10 None (a) General. Tolerances are estab- Peach ...... 5 None Peanut ...... 0.1 None lished for residues of the insecticide Pecan ...... 0.1 None methomyl, including its metabolites Pepper, bell ...... 2 None and degradates, in or on the commod- Pepper, nonbell ...... 2 None Peppermint, tops ...... 2 None ities in the table in this paragraph. Pomegranate ...... 0.2 None Compliance with the tolerance levels Rye, forage ...... 10 None specified in this paragraph is to be de- Rye, grain ...... 1 None termined by measuring only Rye, straw ...... 10 None Sorghum, grain, forage ...... 1 None methomyl, methyl N-[(methylamino) Sorghum, grain, grain ...... 0.2 None carbonyl]oxy]ethanimidothioate, in or Soybean, forage ...... 10 None on the commodity. Soybean, seed ...... 0.2 None Spearmint, tops ...... 2 None Expiration/ Spinach ...... 6 None Commodity Parts per revocation Swiss chard ...... 6 None million date Tangerine ...... 2 None Tomato ...... 1 None Alfalfa, forage ...... 10 None Turnip, greens ...... 6 None Alfalfa, hay ...... 10 None Vegetable, brassica, leafy, group 5 6.0 None Apple ...... 1 None Vegetable, cucurbit, group 9 ...... 0.2 None

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Expiration/ Parts per Commodity Parts per revocation Commodity million million date Sugarcane, cane 1 ...... 0.1 Vegetable, fruiting, group 8 ...... 0.2 None 1 Vegetables, leafy 2 ...... 0.2 None There are no U.S. registrations for use of carbofuran on these commodities. Vegetable, root and tuber, group 1 0.2 None Wheat, forage ...... 10 None (b) Section 18 emergency exemptions. Wheat, grain ...... 1 None [Reserved] Wheat, hay ...... 10 None (c) Tolerances with regional registra- Wheat, straw ...... 10 None tions. [Reserved] 1 There are no U.S. registrations for use of methomyl on (d) Indirect or inadvertent residues. hop, dried cone, as of February 14, 1990. 2 Except for Beet (tops), broccoli, Brussels sprouts, cab- [Reserved] bage, cabbage, Chinese, cauliflower, celery, collards, dan- delions, endive (escarole), kale, lettuce, mustard greens, pars- [39 FR 20597, June 12, 1974] ley, spinach, Swiss chard, turnip, greens (tops), and watercress. EDITORIAL NOTE: For FEDERAL REGISTER ci- tations affecting § 180.254, see the List of CFR (b) Section 18 emergency exemptions. Sections Affected, which appears in the [Reserved] Finding Aids section of the printed volume (c) Tolerances with regional registra- and at www.fdsys.gov. tions. A tolerance with regional reg- § 180.257 Chloroneb; tolerances for res- istration, as defined in § 180.1(l), is es- idues. tablished for residues of the insecticide methomyl, including its metabolites (a) General. Tolerances are estab- and degradates, in or on the com- lished for residues of the fungicide modity in the table in this paragraph. chloroneb, including its metabolites Compliance with the tolerance level and degradates, in or on the commod- specified in this paragraph is to be de- ities in the table in this paragraph. termined by measuring only Compliance with the tolerance levels specified in this paragraph is to be de- methomyl, methyl N-[(methylamino) termined by measuring only the sum of carbonyl]oxy]ethanimidothioate, in or chloroneb, 1,4-dichloro-2,5- on the commodity. dimethoxybenzene, and its metabolite (d) Indirect or inadvertent residues. 2,5-dichloro-4-methoxyphenol (free and [Reserved] conjugated), calculated as the stoichio- [65 FR 33697, May 24, 2000, as amended at 72 metric equivalent of chloroneb, in or FR 35666, June 29, 2007; 74 FR 46373, Sept. 9, on the commodity. 2009; 75 FR 60242, Sept. 29, 2010; 76 FR 34885, June 15, 2011; 77 FR 59125, Sept. 26, 2012] Expiration/ Commodity Parts per revocation million date § 180.254 Carbofuran; tolerances for residues. Bean, dry, seed ...... 0.2 4/16/12 Bean, succulent ...... 0.2 4/16/12 (a) General. Tolerances are estab- Beet, sugar, roots ...... 0.2 4/16/12 lished for the combined residues of the Beet, sugar, tops ...... 0.2 4/16/12 Cowpea, forage ...... 2.0 4/16/12 insecticide carbofuran (2,3-dihydro-2,2- Cowpea, hay ...... 2.0 4/16/12 dimethyl-7-benzofuranyl-N- Cattle, fat ...... 0.2 4/16/12 methylcarbamate), its carbamate me- Cattle, meat ...... 0.2 4/16/12 Cattle, meat byproducts ...... 0.2 4/16/12 tabolite-2,3-dihydro-2,2-dimethyl-3-hy- Cotton, gin byproducts ...... 1.0 4/16/12 droxy-7-benzofuranyl-N- Cotton, undelinted seed ...... 0.2 4/16/12 methylcarbamate, and its phenolic me- Goat, fat ...... 0.2 4/16/12 Goat, meat ...... 0.2 4/16/12 tabolites 2,3-dihydro-2,2-dimethyl-7- Goat, meat byproducts ...... 0.2 4/16/12 benzofuranol, 2,3-dihydro-2,2-dimethyl- Hog, fat ...... 0.2 4/16/12 3,-oxo-7-benzofuranol and 2,3-dihydro- Hog, meat ...... 0.2 4/16/12 Hog, meat byproducts ...... 0.2 4/16/12 2,2-dimethyl-3,7-benzofurandiol in or on Horse, fat ...... 0.2 4/16/12 the following raw agricultural com- Horse, meat ...... 0.2 4/16/12 modities: Horse, meat byproducts ...... 0.2 4/16/12 Milk ...... 0.05 4/16/12 Parts per Sheep, fat ...... 0.2 4/16/12 Commodity million Sheep, meat ...... 0.2 4/16/12 Sheep, meat byproducts ...... 0.2 4/16/12 Banana 1 ...... 0.1 Soybean, forage ...... 2.0 4/16/12 Soybean, hay ...... 2.0 4/16/12 Coffee, bean, green 1 ...... 0 .1 Soybean, seed ...... 0.2 4/16/12 Rice, grain 1 ...... 0 .2

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(b) Section 18 emergency exemptions. Commodity Parts per [Reserved] million (c) Tolerances with regional registra- Corn, field, forage ...... 10 .0 tions. [Reserved] Corn, field, grain ...... 0 .1 (d) Indirect or inadvertent residues. Corn, field, stover ...... 10 .0 Corn, pop, grain ...... 0.1 [Reserved] Corn, pop, stover ...... 10.0 [68 FR 39440, July 1, 2003, as amended at 72 Corn, sweet, forage ...... 10 .0 Corn, sweet, stover ...... 10.0 FR 53460, Sept. 19, 2007; 76 FR 56654, Sept. 14, Cotton, undelinted seed ...... 0 .1 2011] Egg ...... 0 .1 Goat, fat ...... 0 .1 § 180.258 Ametryn; tolerances for resi- Goat, meat ...... 0.1 dues. Goat, meat byproducts ...... 0 .1 Grain, aspirated fractions ...... 0 .4 (a) General. Tolerances are estab- Grape ...... 10 .0 lished for residues of the desiccant and Grapefruit ...... 5 .0 Hog, fat ...... 0 .1 herbicide (2-ethylamino)-4- Hog, meat ...... 0 .1 (isopropylamino)-6-(methylthio)-s-tri- Hog, meat byproducts ...... 0 .1 azine in or on the following raw agri- Hop, dried cones ...... 100 .0 cultural commodities: Horse, fat ...... 0 .1 Horse, meat ...... 0 .1 Horse, meat byproducts ...... 0 .1 Expiration/ Commodity Parts per Revocation Lemon ...... 5.0 million Date Milk, fat (0.08 ppm in milk) ...... 2 .0 Nectarine ...... 4 .0 Banana ...... 0.25 6/16/10 Orange ...... 10 .0 Corn, field, forage ...... 0.1 None Peanut ...... 0 .1 Corn, field, grain ...... 0.05 None Peppermint, tops ...... 50 .0 Corn, field, stover ...... 0.05 None Poultry, fat ...... 0.1 Corn, pop, grain ...... 0.05 None Potato ...... 0 .1 Corn, pop, stover ...... 0.05 None Sheep, fat ...... 0 .1 Corn, sweet, forage ...... 0.5 6/16/10 Sheep, meat ...... 0.1 Corn, sweet, kernel plus cob with Sheep, meat byproducts ...... 0 .1 husks removed ...... 0.25 6/16/10 Sorghum, grain, forage ...... 10.0 Corn, sweet, stover ...... 0.5 6/16/10 Sorghum, grain, grain ...... 5 .0 Pineapple ...... 0.05 None Sorghum, grain, stover ...... 10 .0 Sugarcane, cane ...... 0.05 None Spearmint, tops ...... 50 .0 Tea, dried ...... 10 .0 (b) Section 18 emergency exemptions. Walnut ...... 0 .1 [Reserved] (c) Tolerances with regional registra- (b) Section 18 emergency exemptions. tions. [Reserved] [Reserved] (d) Indirect or inadvertent residues. (c) Tolerances with regional registra- [Reserved] tions. Tolerances with regional reg- istration, as defined in § 180.1(l), are es- [43 FR 29121, July 6, 1978, as amended at 48 tablished for residues of propargite in FR 13175, Mar. 30, 1983; 48 FR 21132, May 11, or on the following raw agricultural 1983; 52 FR 33237, Sept. 2, 1987; 63 FR 57075, commodities: Oct. 26, 1998; 73 FR 54961, Sept. 24, 2008; 74 FR 47456, Sept. 16, 2009] Parts per Commodity million § 180.259 Propargite; tolerances for residues. Corn, sweet, kernel plus cob with husks re- moved ...... 0 .1 (a) General. Tolerances are estab- lished for residues of the pesticide (d) Indirect or inadvertent residues. propargite (2-(p-tert-butylphenoxy) [Reserved] cyclohexyl 2-propynyl sulfite) in or on [65 FR 33710, May 24, 2000, as amended at 72 the following food commodities. FR 41930, Aug. 1, 2007; 73 FR 54961, Sept. 24, Parts per 2008; 76 FR 34885, June 15, 2011] Commodity million § 180.261 Phosmet; tolerances for resi- Almond ...... 0.1 dues. Almond, hulls ...... 55 .0 Bean, dry, seed ...... 0 .2 (a) General. Tolerances are estab- Cattle, fat ...... 0.1 lished for residues of the insecticide Cattle, meat ...... 0 .1 Cattle, meat byproducts ...... 0.1 phosmet, N-(mercaptomethyl) phthal- Citrus, oil ...... 30.0 imide S-(O,O-dimethyl

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phosphorodithioate), including its me- be determined by measuring only the tabolites and degradates, in or on the sum of phosmet, N-(mercaptomethyl) commodities in the following table. phthalimide S-(O,O-dimethyl Compliance with the tolerance levels phosphorodithioate), and its oxygen specified in this paragraph is to be de- analog, N-(mercaptomethyl) phthal- termined by measuring only the sum of imide S-(O,O-dimethyl phosmet, N-(mercaptomethyl) phthal- phosphorothioate, calculated as the imide S-(O,O-dimethyl stoichiometric equivalent of phosmet, phosphorodithioate), and its oxygen in or on the commodity. analog, N-(mercaptomethyl) phthal- imide S-(O,O-dimethyl Commodity Parts per phosphorothioate, calculated as the million stoichiometric equivalent of phosmet, Crabapple ...... 20 in or on the commodity. Pistachio ...... 0.1

Parts per Commodity million (d) Indirect or inadvertent residues. [Reserved] Alfalfa, forage ...... 20 Alfalfa, hay ...... 40 [43 FR 46538, Oct. 10, 1978, as amended at 45 Almond, hulls ...... 10 FR 8981, Feb. 11, 1980; 48 FR 37213, Aug. 17, Apple ...... 10 Apricot ...... 5 1983; 52 FR 48539, Dec. 23, 1987; 53 FR 657, Jan. Blueberry ...... 10 11, 1988; 53 FR 39090, Oct. 5, 1988; 63 FR 57075, Cattle, fat ...... 0.2 Oct. 26, 1998; 67 FR 49616, July 31, 2002; 74 FR Cattle, meat ...... 0 .1 46698, Sept. 11, 2009; 75 FR 60242, Sept. 29, Cattle, meat byproducts ...... 0.1 Cherry ...... 10 2010] Cranberry ...... 10 Fruit, citrus, group 10 ...... 5 § 180.262 Ethoprop; tolerances for resi- Goat, fat ...... 0 .1 dues. Goat, meat ...... 0.1 Goat, meat byproducts ...... 0 .1 (a) General. Tolerances are estab- Grape ...... 10 lished for residues of the nematocide Hog, fat ...... 0 .2 Hog, meat ...... 0 .04 and insecticide ethoprop, O-ethyl S,S- Hog, meat byproducts ...... 0 .04 dipropyl phosphorodithioate, including Horse, fat ...... 0 .1 Horse, meat ...... 0 .1 its metabolites and degradates, in or Horse, meat byproducts ...... 0 .1 on the commodities in the following Kiwifruit ...... 25 table. Compliance with the tolerance Milk ...... 0.1 Nectarine ...... 5 levels specified in this paragraph is to Nut, tree, group 14 ...... 0 .1 be determined by measuring only Pea, dry, seed ...... 0 .5 ethoprop, O-ethyl S,S-dipropyl Pea, field, hay ...... 20 Pea, field, vines ...... 10 phosphorodithioate, in or on the com- Pea, succulent ...... 1 modity. Peach ...... 10 Pear ...... 10 Parts per Plum, prune, fresh ...... 5 Commodity million Potato ...... 0 .1 Sheep, fat ...... 0 .1 Banana ...... 0.02 Sheep, meat ...... 0.1 Bean, lima ...... 0 .02 Sheep, meat byproducts ...... 0 .1 Bean, snap, succulent ...... 0 .02 Sweet potato, roots ...... 12 Cabbage ...... 0 .02 Corn, field, forage ...... 0 .02 (b) Section 18 emergency exemptions. Corn, field, grain ...... 0 .02 [Reserved] Corn, field, stover ...... 0 .02 (c) Tolerances with regional registra- Corn, sweet, forage ...... 0 .02 tions. Tolerances with regional reg- Corn, sweet, kernel plus cob with husks re- istration are established for residues of moved ...... 0 .02 the insecticide phosmet, N- Corn, sweet, stover ...... 0 .02 Cucumber ...... 0 .02 (mercaptomethyl) phthalimide S-(O,O- Hop, dried cones ...... 0 .02 dimethyl phosphorodithioate), includ- Peppermint, tops ...... 0 .02 ing its metabolites and degradates, in Pineapple1 ...... 0 .02 or on the commodities in the following Potato ...... 0 .02 table. Compliance with the tolerance Spearmint, tops ...... 0 .02 levels specified in this paragraph is to Sugarcane, cane ...... 0.02

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methyl-2-(methylthio)propionaldehyde Commodity Parts per million O-(methylcarbamoyl) oxime and its Sweet potato, roots ...... 0 .02 cholinesterase-inhibiting metabolites 2-methyl 2-(methylsulfinyl) 1 There are no U.S. registrations as of July 23, 2009, except for existing stocks bearing old labeling whose sale, distribu- propionaldehyde O-(methylcarbamoyl) tion, and use is allowed, provided it is consistent with the oxime and 2-methyl-2-(methylsulfonyl) terms of the cancellation order of July 9, 2009; i.e., the EPA will allow the technical registrant to continue to sell and dis- propionaldehyde O-(methylcarbamoyl) tribute existing stocks of the amended registered product oxime in or on the following food com- bearing old labeling for use on pineapple for 18 months (until January 9, 2011) and persons other than the registrant may modities: continue to sell and/or use existing stocks of product bearing the old labeling until such stocks are exhausted, provided that Parts per such use is consistent with the terms of the previously ap- Commodity million proved labeling on, or that accompanied, the modified product. Bean, dry, seed ...... 0 .1 Beet, sugar, roots ...... 0 .05 (b) Section 18 emergency exemptions. Beet, sugar, tops ...... 1 [Reserved] Citrus, dried pulp ...... 0 .6 (c) Tolerances with regional registra- Coffee, bean, green ...... 0 .1 tions. [Reserved] Cotton, undelinted seed ...... 0 .1 Cotton, hulls ...... 0 .3 (d) Indirect or inadvertent residues. Grapefruit ...... 0 .3 [Reserved] Lemon ...... 0.3 Lime ...... 0.3 [47 FR 53004, Nov. 24, 1982, as amended at 48 Orange, sweet ...... 0 .3 FR 51485, Nov. 9, 1983; 52 FR 33237, Sept. 2, Peanut ...... 0 .05 1987; 53 FR 30053, Aug. 10, 1988; 63 FR 57075, Pecan ...... 0 .5 Oct. 26, 1998; 64 FR 39078, July 21, 1999; 66 FR Potato ...... 1 Sorghum, grain, bran ...... 0 .5 38955, July 26, 2001; 67 FR 49616, July 31, 2002; Sorghum, grain, grain ...... 0 .2 73 FR 53731, Sept. 17, 2008; 73 FR 54961, Sept. Sorghum, grain, stover ...... 0 .5 24, 2008; 74 FR 46373, Sept. 9, 2009; 75 FR 60242, Soybean ...... 0.02 Sept. 29, 2010] Sugarcane, cane ...... 0.02 Sweet potato, roots ...... 0 .1 § 180.263 Phosalone; tolerances for res- idues. (b) Section 18 emergency exemptions. (a) General. Tolerances are estab- [Reserved] (c) lished for residues of the insecticide Tolerances with regional registra- tions. [Reserved] phosalone, S-(6-chloro-3- (d) Indirect or inadvertent residues. (mercaptomethyl)-2-benzoxazolinone) [Reserved] O,O-diethyl phosphorodithioate, in or on the following food commodities: [65 FR 33710, May 24, 2000, as amended at 69 FR 6567, Feb. 11, 2004; 73 FR 54961, Sept. 24, Expiration/ 2008] Commodity Parts per Revocation million Date § 180.272 Tribuphos; tolerances for res- Apple1 ...... 10.0 9/30/13 idues. Cherry1 ...... 15.0 9/30/13 Grape1 ...... 10.0 9/30/13 (a) General. Tolerances are estab- Peach1 ...... 15.0 9/30/13 lished for residues of the defoliant Pear1 ...... 10.0 9/30/13 tribuphos (S,S,S-tributyl 1 Plum, prune, fresh ...... 15.0 9/30/13 phosphorotrithioate) in or on food com- 1There are no U.S. registrations since 1992. modities as follows: (b) Section 18 emergency exemptions. Parts per [Reserved] Commodity million (c) Tolerances with regional registra- Cattle, fat ...... 0.15 tions. [Reserved] Cattle, meat ...... 0 .02 (d) Indirect or inadvertent residues. Cattle, meat byproducts ...... 0.02 [Reserved] Cotton, gin byproducts ...... 40 .0 Cotton, undelinted seed ...... 4 .0 [74 FR 46698, Sept. 11, 2009] Goat, fat ...... 0 .15 Goat, meat ...... 0.02 § 180.269 Aldicarb; tolerances for resi- Goat, meat byproducts ...... 0 .02 Hog, fat ...... 0 .15 dues. Hog, meat ...... 0 .02 (a) General. Tolerances are estab- Hog, meat byproducts ...... 0 .02 Horse, fat ...... 0 .15 lished for combined residues of the in- Horse, meat ...... 0 .02 secticide and nematocide aldicarb (2- Horse, meat byproducts ...... 0 .02

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Commodity Parts per § 180.275 Chlorothalonil; tolerances for million residues. Milk ...... 0.01 (a) General. (1) Tolerances are estab- Sheep, fat ...... 0 .15 lished for the fungicide chlorothalonil Sheep, meat ...... 0.02 Sheep, meat byproducts ...... 0 .02 (tetrachloroisophthalonitrile) and its metabolite 4-hydroxy-2,5,6- (b) Section 18 emergency exemptions. trichloroisophthalonitrile in or on the [Reserved] following food commodities. (c) Tolerances with regional registra- Parts per tions. [Reserved] Commodity million

(d) Indirect or inadvertent residues. Almond ...... 0.05 [Reserved] Almond, hulls ...... 1 .0 Apricot ...... 0 .5 [65 FR 33698, May 24, 2000, as amended at 67 Asparagus ...... 0.1 FR 49616, July 31, 2002; 72 FR 53460, Sept. 19, Banana (NMT 0.05 ppm in edible pulp) ...... 0 .5 2007] Bean, dry, seed ...... 0 .1 Bean, snap, succulent ...... 5 Blueberry ...... 1 .0 § 180.274 Propanil; tolerances for resi- Brassica, head and stem, subgroup 5A ...... 5 .0 dues. Carrot, roots ...... 1 (a) General. Tolerances are estab- Celery ...... 15 Cherry, sweet ...... 0 .5 lished for the combined residues of the Cherry, tart ...... 0 .5 herbicide propanil (3′, 4′- Cocoa bean, dried bean ...... 0 .05 dichloropropionanilide) and its me- Coffee, bean, green ...... 0 .20 Corn, sweet, kernel plus cob with husks re- tabolites convertible to 3, 4- moved ...... 1 dichloroaniline (3, 4-DCA) in or on the Cranberry ...... 5 .0 following food commodities: Ginseng ...... 4 .0 Horseradish ...... 4.0 Parts per Lentil ...... 0.10 Commodity million Lychee ...... 15 Mango ...... 1.0 Cattle, fat ...... 0.10 Mushroom ...... 1 .0 Cattle, meat ...... 0 .05 Nectarine ...... 0 .5 Cattle, meat byproducts ...... 1.0 Okra ...... 6.0 Onion, bulb ...... 0 .5 Crayfish ...... 0.05 Onion, green ...... 5 Egg ...... 0 .30 Papaya ...... 15 Goat, fat ...... 0 .10 Parsnip, roots ...... 1 Goat, meat ...... 0.05 Passionfruit ...... 3 Goat, meat byproducts ...... 1 .0 Pea, edible podded ...... 5 Hog, fat ...... 0 .10 Peach ...... 0 .5 Hog, meat ...... 0 .05 Peanut ...... 0 .3 Hog, meat byproducts ...... 1 .0 Pistachio ...... 0.2 Horse, fat ...... 0 .10 Plum ...... 0 .2 Horse, meat ...... 0 .05 Plum, prune ...... 0 .2 Horse, meat byproducts ...... 1 .0 Potato ...... 0 .1 Milk ...... 0.05 Rhubarb ...... 4 .0 Poultry, fat ...... 0.05 Soybean ...... 0.2 Poultry, meat ...... 0 .10 Starfruit ...... 3 .0 Tomato ...... 5 Poultry, meat byproducts ...... 0.50 Vegetable, cucurbit, group 9 ...... 5.0 Rice, bran ...... 40 Vegetable, fruiting, group 8, except tomato ...... 6 .0 Rice, grain ...... 10 Yam, true ...... 0 .10 Rice, hulls ...... 30 Rice, straw ...... 75 Sheep, fat ...... 0 .10 (2) Tolerances are established for the Sheep, meat ...... 0.05 metabolite 4-hydroxy-2,5,6- Sheep, meat byproducts ...... 1 .0 trichloroisophthalonitrile in or on the following food commodities. (b) Section 18 emergency exemptions. [Reserved] Parts per Commodity million (c) Tolerances with regional registra- tions. [Reserved] Cattle, fat ...... 0.1 Cattle, kidney ...... 0 .5 (d) Indirect or inadvertent residues. Cattle, meat byproducts, except kidney ...... 0.05 [Reserved] Cattle, meat ...... 0 .03 Goat, fat ...... 0 .1 [63 FR 34827, June 26, 1998, as amended at 72 Goat, kidney ...... 0 .5 FR 28888, May 23, 2007] Goat, meat byproducts, except kidney ...... 0 .05

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Parts per Expiration/ Commodity million Commodity Parts per revocation million date Goat, meat ...... 0.03 Hog, fat ...... 0 .1 Lemon ...... 0.60 None Hog, kidney ...... 0.5 Lime ...... 0.03 None Hog, meat byproducts, except kidney ...... 0 .05 Nectarine ...... 0.40 None Hog, meat ...... 0 .03 Orange ...... 1.5 None Horse, fat ...... 0 .1 Peach ...... 0.40 12/31/13 Horse, kidney ...... 0 .5 Pear ...... 0.50 12/31/13 Horse, meat byproducts, except kidney ...... 0 .05 Tangelo ...... 0.03 None Horse, meat ...... 0 .03 Tangerine ...... 0.03 None Milk ...... 0.1 Sheep, fat ...... 0 .1 (b) Section 18 emergency exemptions. Sheep, kidney ...... 0.5 Sheep, meat byproducts, except kidney ...... 0 .05 [Reserved] Sheep, meat ...... 0.03 (c) Tolerances with regional registra- tions. [Reserved] (b) Section 18 emergency exemptions. (d) Indirect or inadvertent residues. [Reserved] [Reserved] (c) Tolerances with regional registra- tions. Tolerances with regional reg- [77 FR 40815, July 11, 2012] istration, as defined in § 180.1(l), are es- § 180.278 Phenmedipham; tolerances tablished for the combined residues of for residues. chlorothalonil and its metabolite in or on the following raw agricultural com- (a) General. Tolerances are estab- modities: lished for the combined residues of the herbicide phenmedipham (3- Commodity Parts per methoxycarbonylaminophenyl-3′- million methylcarbanilate) in or on the fol- Hazelnut ...... 0 .1 lowing food commodities: Peppermint, tops ...... 2 Persimmon ...... 1 .5 Commodity Parts per Spearmint, tops ...... 2 million

Beet, garden, roots ...... 0 .2 (d) Indirect or inadvertent residues. Beet, garden, tops ...... 0 .2 [Reserved] Beet, sugar, dried pulp ...... 0 .5 Beet, sugar, molasses ...... 0 .2 [42 FR 56114, Oct. 21, 1977] Beet, sugar, roots ...... 0 .1 EDITORIAL NOTE: For FEDERAL REGISTER ci- Beet, sugar, tops ...... 0.1 tations affecting § 180.275, see the List of CFR Spinach ...... 4 .0 Sections Affected, which appears in the Finding Aids section of the printed volume (b) Section 18 emergency exemptions. and at www.fdsys.gov. [Reserved] (c) Tolerances with regional registra- § 180.276 Formetanate hydrochloride; tions. [Reserved] tolerances for residues. (d) Indirect or inadvertent residues. (a) General. Tolerances are estab- [Reserved] lished for residues of the insecticide [72 FR 28888, May 23, 2007] formetanate hydrochloride, including its metabolites and degradates, in or § 180.284 Zinc phosphide; tolerances on the commodities in the table in this for residues. paragraph. Compliance with the toler- (a) General. Tolerances are estab- ance levels specified in this paragraph lished for residues of the phosphine re- is to be determined by measuring only sulting from the use of the rodenticide formetanate hydrochloride, N,N-di- zinc phosphide in or on the raw agricul- methyl-N’-[3-[(methylamino)car- tural commodities as follows: bonyl]oxy]phenyl]methanimidamide hydrochloride, in or on the commodity. Parts per Commodity million Expiration/ Commodity Parts per revocation Alfalfa, forage ...... 0.2 million date Alfalfa, hay ...... 0.2 Barley, grain ...... 0 .05 Apple ...... 0.50 12/31/13 Barley, hay ...... 0 .2 Apple, wet pomace ...... 1.5 12/31/13 Barley, straw ...... 0 .2 Grapefruit ...... 1.5 None Bean, dry, seed ...... 0 .05

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Parts per Parts per Commodity million Commodity million

Beet, sugar, roots ...... 0 .05 Cattle, fat ...... 0.1 Beet, sugar, tops ...... 0.2 Cattle, meat ...... 0 .02 Grape ...... 0 .01 Cattle, meat byproducts ...... 0.2 Grass, rangeland, forage ...... 0 .1 Cotton, undelinted seed 1 ...... 1 .0 Grass, rangeland, hay ...... 0 .1 Hog, fat ...... 0 .1 Potato ...... 0 .05 Hog, kidney ...... 0.1 Hog, liver ...... 0 .1 Sugarcane, cane ...... 0.01 Hog, meat ...... 0 .05 Timothy, hay ...... 0 .5 Hog, meat byproducts ...... 0 .3 Timothy, forage ...... 0.5 Honey ...... 0.2 Wheat, forage ...... 0 .05 Honeycomb ...... 9 Wheat, grain ...... 0 .05 Milk ...... 0.03 Wheat, hay ...... 0 .05 Milk, fat ...... 0 .2 Wheat, straw ...... 0 .05 1There are no U.S. registrations on cottonseed as of May 3, 2006. (b) Section 18 emergency exemptions. (b) Section 18 emergency exemptions. [Reserved] [Reserved] (c) Tolerances with regional registra- (c) Tolerances with regional registra- tions. Tolerances with regional reg- tions. [Reserved] istration, as defined in § 180.1(l), are es- (d) Indirect or inadvertent residues. tablished for residues of phosphine re- [Reserved] sulting from the use of the rodenticide zinc phosphide in or on the following [44 FR 70145, Dec. 6, 1979, as amended at 51 raw agricultural commodities as fol- FR 16846, May 7, 1986; 52 FR 5767, Feb. 26, 1987; 57 FR 53568, Nov. 12, 1992; 58 FR 14316, lows: Mar. 17, 1993; 60 FR 12704, Mar. 8, 1995; 67 FR 49616, July 31, 2002; 72 FR 53454, Sept. 19, 2007; Parts per Commodity million 74 FR 47456, Sept. 16, 2009; 78 FR 17133, Mar. 20, 2013] Artichoke, globe ...... 0.01 Beet, sugar, roots ...... 0 .04 § 180.288 2-(Thiocyanomethyl- Beet, sugar, tops ...... 0.02 thio)benzothiazole; tolerances for residues. (d) Indirect or inadvertent residues. (a) General. Tolerances are estab- [Reserved] lished for residues of the fungicide 2- [63 FR 45182, Aug. 25, 1998, as amended at 63 (thiocyanomethylthio)benzothiazole in FR 67799, Dec. 9, 1998; 64 FR 40772, July 28, or on the following food commodities: 1999; 64 FR 61791, Nov. 15, 1999; 65 FR 8874, Parts per Feb. 23, 2000; 65 FR 49941, Aug. 16, 2000; 65 FR Commodity million 62634, Oct. 19, 2000; 66 FR 64773, Dec. 14, 2001; 68 FR 2247, Jan. 16, 2003; 68 FR 56195, Sept. 30, Barley, grain ...... 0 .1(N) 2003; 70 FR 7046, Feb. 10, 2005; 74 FR 46373, Barley, straw ...... 0 .1(N) Sept. 9, 2009; 76 FR 34885, June 15, 2011] Beet, sugar, roots ...... 0 .1(N) Beet, sugar, tops ...... 0.1(N) Corn, field, forage ...... 0 .1(N) § 180.287 Amitraz; tolerances for resi- Corn, field, grain ...... 0 .1 dues. Corn, field, stover ...... 0 .1 Corn, pop, grain ...... 0.1 (a) General. Tolerances are estab- Corn, pop, stover ...... 0.1 lished for residues of the insecticide Cotton, forage ...... 0.1(N) amitraz (N’-[2,4-dimethylphenyl]-N- Cotton, undelinted seed ...... 0 .1(N) Oat, forage ...... 0 .1(N) [[(2,4-dimethylphenyl)imino]methyl]]- Oat, grain ...... 0 .1(N) N-methylmethanimidamide), including Oat, hay ...... 0.1(N) its metabolites and degradates, in or Oat, straw ...... 0.1(N) on the commodities in the following Rice, grain ...... 0 .1(N) Rice, straw ...... 0 .1(N) table. Compliance with the tolerance Safflower, seed ...... 0 .1(N) levels specified is to be determined by Sorghum, grain, forage ...... 0.1(N) measuring amitraz residues convertible Sorghum, grain, grain ...... 0 .1(N) Sorghum, grain, stover ...... 0 .1(N) to 2,4-dimethylaniline, expressed as the Wheat, forage ...... 0 .1(N) stoichiometric equivalent of amitraz, Wheat, grain ...... 0 .1(N) in or on the following raw agricultural Wheat, hay ...... 0 .1(N) commodities: Wheat, straw ...... 0 .1(N)

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(b) Section 18 emergency exemptions. Commodity Parts per [Reserved] million (c) Tolerances with regional registra- Vegetable, fruiting, group 8 ...... 0.1 tions. [Reserved] (d) Indirect or inadvertent residues. (b) Section 18 emergency exemptions. [Reserved] [Reserved] [68 FR 39440, July 1, 2003, as amended at 74 (c) Tolerances with regional registra- FR 46374, Sept. 9, 2009] tions. Tolerances with regional reg- istrations, as defined in § 180.1(l), are § 180.289 Methanearsonic acid; toler- established for the combined residues ances for residues. of the fungicide (a) General. Tolerances are estab- pentachloronitrobenzene (PCNB) and lished for residues of the herbicide its metabolites pentachloroaniline methanearsonic acid, including its me- (PCA), and pentachlorothioanisole tabolites and degradates, in or on the (PCTA), in or on the following food commodities in the table in this para- commodities: graph. Compliance with the tolerance Parts per levels specified in this paragraph is to Commodity million be determined by measuring only Collards ...... 0.2 methanearsonic acid, from application Kale ...... 0 .2 of the disodium and monosodium salts Mustard, greens ...... 0 .2 of methanearsonic acid, calculated as the stoichiometric equivalent of As2O3, (d) Indirect or inadvertent residues. in or on the commodity. [Reserved] [74 FR 47456, Sept. 16, 2009] Parts per Expiration/ Commodity million Revocation Date § 180.292 Picloram; tolerances for resi- dues. Cotton, undelinted seed ...... 0.7 None Cotton, hulls ...... 0.9 None (a) General. Tolerances are estab- Fruit, citrus ...... 0.35 12/31/12 lished for residues of the herbicide picloram, 4-amino-3,5,6- (b) Section 18 emergency exemptions. trichloropicolinic acid, including its [Reserved] metabolites and degradates, in or on (c) Tolerances with regional registra- the commodities in the following table tions. [Reserved] (d) Indirect or inadvertent residues. from its application in the acid form or [Reserved] in the form of its salts. Compliance with the tolerance levels specified in [63 FR 34828, June 26, 1998, as amended at 77 this paragraph is to be determined by FR 59126, Sept. 26, 2012] measuring only picloram, 4-amino- 3,5,6-trichloropicolinic acid, in or on § 180.291 Pentachloronitrobenzene; tol- erance for residues. the commodity.

(a) General. Tolerances are estab- Commodity Parts per lished for the combined residues of the million fungicide pentachloronitrobenzene Barley, grain ...... 0 .5 (PCNB) and its metabolites Barley, pearled barley ...... 3 .0 Barley, straw ...... 1 .0 pentachloroaniline (PCA), and Cattle, fat ...... 0.4 pentachlorothioanisole (PCTA), in or Cattle, meat ...... 0 .4 on the following food commodities: Cattle, meat byproducts ...... 15 Egg ...... 0 .05 Parts per Goat, fat ...... 0 .4 Commodity million Goat, meat ...... 0.4 Goat, meat byproducts ...... 15 Bean ...... 0 .1 Grain, aspirated fractions ...... 4 .0 Brassica, head and stem, subgroup 5A ...... 0 .1 Grass, forage ...... 400 Cotton, undelinted seed ...... 0 .1 Grass, hay ...... 225 Garlic, bulb ...... 0.1 Hog, fat ...... 0 .05 Peanut ...... 1 .0 Hog, meat ...... 0 .05 Potato ...... 0 .1 Hog, meat byproducts ...... 0 .05 Soybean, forage ...... 0 .02 Horse, fat ...... 0 .4 Soybean, hay ...... 0 .02 Horse, meat ...... 0 .4 Soybean, seed ...... 0 .02 Horse, meat byproducts ...... 15

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aquatic plants in canals, lakes, ponds, Commodity Parts per million and other potential sources of water, Milk ...... 0.25 potable. Oat, forage ...... 1 .0 (b) Section 18 emergency exemptions. Oat, grain ...... 0 .5 [Reserved] Oat, groats/rolled oats ...... 3 .0 Oat, straw ...... 1.0 (c) Tolerances with regional registra- Poultry, fat ...... 0.05 tions. [Reserved] Poultry, meat ...... 0 .05 (d) Indirect or inadvertent residues. Poultry, meat byproducts ...... 0.05 Sheep, fat ...... 0 .4 Tolerances are established for the indi- Sheep, meat ...... 0.4 rect or inadvertent combined residues Sheep, meat byproducts ...... 15 of the herbicide, endothall (7 - Wheat, bran ...... 3.0 Wheat, forage ...... 1 .0 oxabicyclo[2.2.1] heptane-2,3- Wheat, germ ...... 3 .0 dicarboxylic acid) in potable water Wheat, grain ...... 0 .5 from use of its potassium, sodium, di- Wheat, middlings ...... 3 .0 Wheat, shorts ...... 3 .0 N, N -dimethylalkylamine, and mono- Wheat, straw ...... 1 .0 N-N, -dimethylalkylamine salts as algicides or to control (b) Section 18 emergency exemptions. aquatic plants in canals, lakes, ponds, [Reserved] and other potable water sources that (c) Tolerances with regional registra- may lead to endothall residues in or on tions. [Reserved] the following commodities: (d) Indirect or inadvertent residues. Parts per [Reserved] Commodity million

[41 FR 19221, May 11, 1976, as amended at 47 Almond, hulls ...... 15 .0 FR 53005, Nov. 24, 1982; 64 FR 425, Jan. 5, 1999; Animal feed, nongrass, group 18, forage ...... 4 .0 64 FR 39082, July 21, 1999; 72 FR 41930, Aug. 1, Animal feed, nongrass, group 18, hay ...... 10 2007; 75 FR 60243, Sept. 29, 2010] Apple, wet pomace ...... 0 .15 Beet, sugar, molasses ...... 1 .5 § 180.293 Endothall; tolerances for res- Brassica, head and stem subgroup 5A ...... 0 .1 Brassica, leafy, subgroup 5B ...... 2 .0 idues. Bushberry subgroup 13-07B ...... 0 .6 (a) General. (1) Tolerances are estab- Caneberry subgroup 13-07A ...... 0.6 Cattle, fat ...... 0.01 lished for the residues of endothall, in- Cattle, kidney ...... 0 .20 cluding its metabolites and degradates, Cattle, liver ...... 0 .10 in or on the commodities in the table, Cattle, meat ...... 0 .03 Corn, field, grain ...... 0 .07 below. Compliance with the tolerance Corn, pop, grain ...... 0.07 levels specified, below, is to be deter- Corn, sweet, kernel plus cob with husks re- mined by measuring only endothall (7- moved ...... 0 .3 Citrus, dried pulp ...... 0 .1 oxabicylco [2.2.1] heptanes-2,3- Egg ...... 0 .05 dicarboxylic acid) and its mono-methyl Feed commodities not otherwise listed ...... 10 .0 ester. Food commodities not otherwise listed ...... 5 .0 Fruit, citrus group 10 ...... 0.05 Parts per Fruit, pome, group 11 ...... 0.05 Commodity million Fruit, stone, group 12 ...... 0 .3 Goat, fat ...... 0 .005 Apple ...... 0.05 Goat, kidney ...... 0 .15 Apple, wet pomace ...... 0 .15 Goat, liver ...... 0.05 Cotton, undelinted seed ...... 0 .1 Goat, meat ...... 0.015 Fish ...... 0 .1 Grain, aspirated fractions ...... 35.0 Hop, dried cones ...... 0 .1 Grain cereal, forage, fodder and straw, group Potato ...... 0 .1 16 ...... 10 .0 Rice, grain ...... 0 .05 Grain, cereal, group 15, except corn ...... 4 .0 Rice, straw ...... 0 .05 Grape ...... 1 .0 Grape, raisin ...... 5 .0 (2) An interim tolerance of 0.2 parts Grass, forage, fodder, and hay group 17, for- age ...... 3 .5 per million is established for residues Grass, forage, fodder, and hay group 17, hay .. 18 .0 of the herbicide endothall (7 - Herb and spice, group 19 ...... 5 .0 oxabicyclo[2.2.1] heptane-2,3- Hog, fat ...... 0 .005 Hog, kidney ...... 0.10 dicarboxylic acid) in water, potable Hog, liver ...... 0 .05 from use of its potassium, sodium, di- Hog, meat ...... 0 .01 N, N-dimethylalkylamine, and mono-N- Milk ...... 0.03 Nut, tree, group 14 ...... 0 .05 N,-dimethylalkylamine salts as Okra ...... 0.05 algicides or herbicides to control Pea and bean, dried shelled, subgroup 6C ...... 0 .2

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Commodity Parts per § 180.298 Methidathion; tolerances for million residues. Pea and bean, succulent shelled, subgroup 6B 2 .0 (a) General. Tolerances are estab- Peppermint, tops ...... 5 .0 lished for residues of the insecticide Pistachio ...... 0.05 Poultry, fat ...... 0.015 methidathion, including its metabo- Poultry, liver ...... 0 .05 lites and degradates, in or on the com- Poultry, meat ...... 0 .015 modities in the table in this paragraph. Poultry, meat byproducts ...... 0.20 Compliance with the tolerance levels Rice, hulls ...... 8 .0 specified in this paragraph is to be de- Sheep, fat ...... 0 .005 termined by measuring only Sheep, kidney ...... 0.15 Sheep, liver ...... 0.05 methidathion, S-[(5-methoxy-2-oxo- Sheep, meat ...... 0.015 1,3,4-thiadiazol-3(2H)-yl)methyl] O,O- Soybean, hulls ...... 0 .5 dimethyl phosphorodithioate, in or on Soybean, seed ...... 0 .2 the commodity. Spearmint, tops ...... 5 .0 Tomato, paste ...... 0 .1 Parts per Expiration/ Tomato, puree ...... 0 .1 Commodity million revocation Vegetable, bulb, group 3-07 ...... 0 .5 date Vegetable, cucurbit, group 9 ...... 1.5 Almond, hulls ...... 6.0 12/31/16 Vegetable, foliage of legume, group 7 ...... 4 .0 Artichoke, globe ...... 0.05 12/31/16 Vegetable, fruiting, group 8 ...... 0.05 Citrus, oil ...... 420.0 12/31/16 Vegetable, leafy, except brassica, group 4 ...... 2 .0 Cotton, undelinted seed ...... 0.2 12/31/16 Vegetable, leaves of root and tuber, group 2 ... 3 .0 Fruit, citrus, group 10, except tan- Vegetable, legume, edible, podded, subgroup gerine ...... 4.0 12/31/16 6A ...... 2 .0 Fruit, pome, group 11 ...... 0.05 12/31/16 Vegetable, root and tuber, group 1 ...... 1 .0 Fruit, stone, group 12 ...... 0.05 12/31/16 Wheat, milled byproducts ...... 5 .0 Mango ...... 0.05 12/31/16 Nut, tree, group 14 ...... 0.05 12/31/16 [41 FR 23717, June 11, 1976, as amended at 51 Olive ...... 0.05 12/31/16 FR 4498, Feb. 5, 1986; 62 FR 49931, Sept. 24, Safflower, seed ...... 0.5 12/31/16 1997; 63 FR 42249, Aug. 7, 1998; 67 FR 35048, Sorghum, forage, forage ...... 2.0 12/31/16 May 17, 2002; 71 FR 47106, Aug. 16, 2006; 71 FR Sorghum, grain, forage ...... 2.0 12/31/16 74816, Dec. 13, 2006; 72 FR 52018, Sept. 12, 2007; Sorghum, grain, grain ...... 0.2 12/31/16 74 FR 67097, Dec. 18, 2009; 78 FR 76566, Dec. 18, Sorghum, grain, stover ...... 2.0 12/31/16 2013] Sunflower, seed ...... 0.5 12/31/16 Tangerine ...... 6.0 12/31/16 § 180.297 N-1-Naphthyl phthalamic acid; tolerances for residues. (b) Section 18 emergency exemptions. [Reserved] (a) General. Tolerances are estab- (c) Tolerances with regional registra- lished for residues of the herbicide N-1- tions. Tolerances with regional reg- naphthyl phthalamic acid from appli- istration, as defined in § 180.1(l), are es- cation of its sodium salt in or on the tablished for residues of the insecticide following raw agricultural commod- methidathion, including its metabo- ities: lites and degradates, in or on the com- Parts per modities in the table in this paragraph. Commodity million Compliance with the tolerance levels specified in this paragraph is to be de- Cantaloupe ...... 0 .1(N) Cucumber ...... 0 .1(N) termined by measuring only Muskmelon ...... 0 .1(N) methidathion, S-[(5-methoxy-2-oxo- Watermelon ...... 0.1(N) 1,3,4-thiadiazol-3(2H)-yl)methyl] O,O- dimethyl phosphorodithioate, in or on (b) Section 18 emergency exemptions. the commodity. [Reserved] (c) Tolerances with regional registra- Parts per Expiration/ Commodity million revocation tions. [Reserved] date (d) Indirect or inadvertent residues. Kiwifruit ...... 0.1 12/31/16 [Reserved] Longan ...... 0.1 12/31/16 [45 FR 32306, May 16, 1980, as amended at 63 Starfruit ...... 0.1 12/31/16 Sugar apple ...... 0.2 12/31/16 FR 57075, Oct. 26, 1998]

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(d) Indirect or inadvertent residues. Commodity Parts per [Reserved] million [43 FR 44845, Sept. 29, 1978] Grape, raisin ...... 12.0 Hazelnut ...... 0 .80 EDITORIAL NOTE: For FEDERAL REGISTER ci- Hog, fat ...... 0 .02 tations affecting § 180.298, see the List of CFR Hog, kidney ...... 1.0 Sections Affected, which appears in the Hog, meat ...... 0 .02 Finding Aids section of the printed volume Hog, meat byproducts, except kidney ...... 0 .2 Horse, fat ...... 0 .02 and at www.fdsys.gov. Horse, kidney ...... 1 .0 Horse, meat ...... 0 .02 § 180.299 Dicrotophos; tolerances for Horse, meat byproducts, except kidney ...... 0 .2 residues. Milk ...... 0.01 Nut, macadamia ...... 0.5 (a) General. Tolerances are estab- Pepper ...... 30.0 lished for residues of the insecticide Pineapple ...... 2.0 dicrotophos, dimethyl phosphate of 3- Poultry, fat ...... 0.02 Poultry, liver ...... 0 .05 hydroxy-N,N-dimethyl-cis- Poultry, meat ...... 0 .01 crotonamide, in or on the following Poultry, meat byproducts, except liver ...... 0 .01 food commodities: Sheep, fat ...... 0 .02 Sheep, kidney ...... 1.0 Sheep, meat ...... 0.02 Parts per Commodity million Sheep, meat byproducts, except kidney ...... 0 .2 Sugarcane, molasses ...... 1 .5 Cotton, gin byproducts ...... 2 .0 Tomato ...... 2.0 Cotton, undelinted seed ...... 0 .2 Walnut ...... 0 .5 Wheat, bran ...... 5.0 Wheat, germ ...... 5 .0 (b) Section 18 emergency exemptions. Wheat, grain ...... 2 .0 [Reserved] Wheat, middlings ...... 5 .0 (c) Tolerances with regional registra- Wheat, shorts ...... 5 .0 tions. [Reserved] Wheat, straw ...... 10 .0 (d) Indirect or inadvertent residues. (b) Section 18 emergency exemptions. [Reserved] [Reserved] [73 FR 52613, Sept. 10, 2008] (c) Tolerances with regional registra- tions. A tolerance with regional reg- § 180.300 Ethephon; tolerances for resi- istration, as defined in § 180.1(m), of 0.1 dues. part per million is established for resi- (a) General. Tolerances are estab- dues of the plant regulator ethephon lished for residues of the plant regu- [(2-chloroethyl)phosphonic acid] in or lator ethephon [(2-chloroethyl) phos- on the food commodity sugarcane. phonic acid] in or on food commodities (d) Indirect or inadvertent residues. as follows: [Reserved]

Parts per [65 FR 33710, May 24, 2000, as amended at 72 Commodity million FR 53455, Sept. 19, 2007; 75 FR 56015, Sept. 15, 2010] Apple ...... 5.0 Apple, juice ...... 10 .0 Barley, bran ...... 5 .0 § 180.301 Carboxin; tolerances for resi- Barley, grain ...... 2 .0 dues. Barley, straw ...... 10 .0 (a) General. Tolerances are estab- Blackberry ...... 30 .0 Blueberry ...... 20 .0 lished for the combined residues of the Cantaloupe ...... 2 .0 fungicide carboxin (5,6-dihydro-2-meth- Cattle, fat ...... 0.02 yl-1,4-oxathiin-3-carboxanilide) and its Cattle, kidney ...... 1 .0 Cattle, meat ...... 0 .02 metabolites determined as aniline and Cattle, meat byproducts, except kidney ...... 0.2 expressed as parent compound, in or on Cherry ...... 10.0 food commodities as follows: Coffee, bean, green ...... 0 .5 Cotton, gin byproducts ...... 180.0 Parts per Cotton, undelinted seed ...... 6 .0 Commodity million Cucumber ...... 0 .1 Egg ...... 0 .002 Barley, grain ...... 0 .2 Goat, fat ...... 0 .02 Barley, straw ...... 0 .2 Goat, kidney ...... 1 .0 Bean, dry, seed ...... 0 .2 Goat, meat ...... 0.02 Bean, succulent ...... 0 .2 Goat, meat byproducts, except kidney ...... 0 .2 Canola, seed ...... 0 .03 Grape ...... 2 .0 Cattle, fat ...... 0.05

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Parts per Parts per Commodity million Commodity million

Cattle, meat byproducts ...... 0.1 Apple ...... 2 Cattle, meat ...... 0 .05 Banana ...... 0.3 Corn, field, forage ...... 0 .2 Cantaloupe ...... 2 .0 Corn, field, grain ...... 0 .2 Carrot ...... 0 .1 Corn, field, stover ...... 0 .2 Celery ...... 10 .0 Corn, pop, grain ...... 0.2 Cotton, undelinted seed ...... 0 .2 Corn, pop, stover ...... 0.2 Cucumber ...... 2 .0 Corn, sweet, forage ...... 0 .2 Eggplant ...... 2.0 Corn, sweet, kernel plus cob with husks re- Fruit, citrus, group 10 ...... 3 moved ...... 0 .2 Garlic, bulb ...... 0.2 Corn, sweet, stover ...... 0 .2 Cotton, undelinted seed ...... 0 .2 Melon, honeydew ...... 2.0 Egg ...... 0 .05 Onion, bulb ...... 0 .2 Goat, fat ...... 0 .05 Peanut ...... 0 .05 Goat, meat byproducts ...... 0 .1 Peanut, hay ...... 2.0 Goat, meat ...... 0.05 Pear ...... 2 .0 Hog, fat ...... 0 .05 Peppermint, tops ...... 10 .0 Hog, meat byproducts ...... 0 .1 Pepper, bell ...... 2 .0 Hog, meat ...... 0 .05 Pepper, nonbell ...... 5 .0 Horse, fat ...... 0 .05 Pineapple ...... 1 Horse, meat byproducts ...... 0 .1 Pineapple, process residue ...... 2 .0 Horse, meat ...... 0 .05 Pumpkin ...... 2.0 Milk ...... 0.05 Soybean, seed ...... 0 .1 Oat, forage ...... 0 .5 Spearmint, tops ...... 10 .0 Oat, grain ...... 0 .2 Squash, summer ...... 2 .0 Oat, straw ...... 0.2 Squash, winter ...... 2 .0 Onion, bulb ...... 0 .2 Tomato ...... 2 Peanut ...... 0 .2 Vegetable, tuberous and corm, subgroup 1C ..... 0.1 Peanut, hay ...... 0.2 Poultry, fat ...... 0.1 Watermelon ...... 2.0 Poultry, meat byproducts ...... 0.1 Poultry, meat ...... 0 .1 (b) Section 18 emergency exemptions. Rice, grain ...... 0 .2 [Reserved] Rice, straw ...... 0 .2 Safflower, seed ...... 0 .2 (c) Tolerances with regional registra- Sheep, fat ...... 0 .05 tions. [Reserved] Sheep, meat byproducts ...... 0 .1 (d) Indirect or inadvertent residues. Sheep, meat ...... 0.05 Soybean, seed ...... 0 .2 [Reserved] Wheat, forage ...... 0 .5 Wheat, grain ...... 0 .2 [73 FR 54961, Sept. 24, 2008] Wheat, straw ...... 0 .2 § 180.304 Oryzalin; tolerances for resi- (b) Section 18 emergency exemptions. dues. [Reserved] (a) General. Tolerances are estab- (c) Tolerances with regional registra- lished for residues of the herbicide tions. [Reserved] oryzalin, 3,5-dinitro-N4,N4- (d) Indirect or inadvertent residues. dipropylsulfanilamide, in or on the fol- [Reserved] lowing raw agricultural commodities:

[47 FR 55222, Dec. 8, 1982, as amended at 50 Parts per FR 81, Jan. 2, 1985; 62 FR 4915, Feb. 3, 1997; 63 Commodity million FR 4586, Jan. 30, 1998; 64 FR 11801, Mar. 10, 1999; 66 FR 9773, Feb. 12, 2001; 66 FR 64773, Almond, hulls ...... 0 .05 Dec. 14, 2001; 67 FR 40218, June 12, 2002; 67 FR Avocado ...... 0 .05 72853, Dec. 9, 2002; 71 FR 56383, Sept. 27, 2006] Berry group 13 ...... 0 .05 Cranberry ...... 0 .05 Fig ...... 0 .05 § 180.303 Oxamyl; tolerances for resi- Fruit, citrus, group 10 ...... 0 .05 dues. Fruit, pome, group 11 ...... 0.05 Fruit, stone, group 12 ...... 0 .05 (a) General. Tolerances are estab- Grape ...... 0 .05 lished for the combined residues of the Kiwifruit ...... 0.05 insecticide oxamyl, methyl N,N-di- Nut, tree, group 14 ...... 0 .05 methyl-N-[(methylcarbamoyl)-oxy]-1- Olive ...... 0 .05 Pistachio ...... 0.05 thiooxamimidate, and its oxime me- Pomegranate ...... 0 .05 tabolite methyl N,N-dimethyl-N-hy- Strawberry ...... 0 .05 droxy-1-thiooxamimidate calculated as oxamyl in or on the following food (b) Section 18 emergency exemptions. commodities: [Reserved]

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(c) Tolerances with regional registra- (b) Section 18 emergency exemptions. tions. Tolerances with regional reg- [Reserved] istration, as defined in § 180.1(l), are es- (c) Tolerances with regional registra- tablished for residues of oryzalin, 3,5- tions. Tolerances with a regional reg- dinitro-N4,N4-dipropylsulfanilamide, in istration, as defined in 180.1(l),are es- or on the following raw agricultural tablished for residues of the herbicide commodities: (S-2, 3, 4-trichloroallyl diisopropylthiocarbamate) and its me- Parts per Commodity million tabolite 2, 3, 3-trichloroprop-2- enesulfonic acid (TCPSA) in or on the Guava ...... 0 .05 Papaya ...... 0 .05 following food commodities:

Parts per (d) Indirect or inadvertent residues. Commodity million [Reserved] Barley, grain ...... 0 .05 [71 FR 54434, Sept. 15, 2006, as amended at 76 Barley, hay ...... 1 .0 FR 34885, June 15, 2011] Barley, straw ...... 0 .3 Beet, sugar, dried pulp ...... 0 .2 § 180.311 Cacodylic acid; tolerances for Beet, sugar, roots ...... 0 .1 residues. Beet, sugar, tops ...... 0.5 (a) General. A tolerance is established Pea, dry ...... 0 .2 Pea, field, hay ...... 1.0 for residues of the defoliant cacodylic Pea, field, vines ...... 0 .5 acid, dimethylarsinic acid, including Pea, succulent ...... 0 .2 its metabolites and degradates, in or Wheat, forage ...... 0 .5 on the commodity in the following Wheat, grain ...... 0 .05 table. Compliance with the tolerance Wheat, hay ...... 1 .0 level specified in this paragraph is to Wheat, straw ...... 1 .0 be determined by measuring only those (d) Indirect or inadvertent residues. cacodylic acid residues convertible to [Reserved] As2O3, expressed as the stoichiometric equivalent of cacodylic acid, in or on [72 FR 28888, May 23, 2007, as amended at 73 the commodity. FR 5109, Jan. 29, 2008; 73 FR 53738, Sept. 17, 2008; 74 FR 29963, June 24, 2009] Expiration/ Commodity Parts per Revocation million Date § 180.315 Methamidophos; tolerances for residues. Cotton, undelinted seed ...... 2.8 1/1/12 (a) General. Tolerances are estab- (b) Section 18 emergency exemptions. lished for residues of methamidophos, [Reserved] O,S-dimethyl phosphoramidothioate, (c) Tolerances with regional registra- including its metabolites and tions. [Reserved] degradates, in or on the commodities (d) Indirect or inadvertent residues. in the following table as a result of the [Reserved] application of methamidophos. Compli- ance with the tolerance levels specified [69 FR 6567, Feb. 11, 2004, as amended at 75 in this paragraph is to be determined FR 60243, Sept. 29, 2010] by measuring only methamidophos, § 180.314 Triallate; tolerances for resi- O,S-dimethyl phosphoramidothioate, in dues. or on the commodity. (a) General. Tolerances are estab- Parts per Expiration/ lished for residues of triallate, S-2,3,4- Commodity million Revocation trichloroallyl Date diisopropylthiocarbamate and its me- Broccoli1 ...... 1.0 12/31/12 tabolite 2,3,3-trichloroprop-2- Cabbage2 ...... 1.0 12/31/12 enesulfonic acid (TCPSA) in or on the Cotton, undelinted seed ...... 0.1 12/31/13 following food commodity: Potato ...... 0.1 12/31/13 1 There are no U.S. registrations since 1989. Parts per 2 There are no U.S. registrations since 2001. Commodity million (b) Section 18 emergency exemptions. Bermudagrass, hay ...... 0.3 [Reserved]

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(c) Tolerances with regional registra- 5-amino-4-chloro-2-phenyl-3(2H)- tions. A tolerance with a regional reg- pyridazinone, and its metabolites (cal- istration is established for residues of culated as pyrazon), in or on the fol- methamidophos, O,S-dimethyl lowing food commodities: phosphoramidothioate, including its Parts per metabolites and degradates, in or on Commodity million the commodity in the following table as a result of the application of Corn, field, forage ...... 0 .5 Corn, field, stover ...... 0 .5 methamidophos. Compliance with the Soybean, forage ...... 0 .5 tolerance levels specified in this para- Soybean, hay ...... 0 .5 graph is to be determined by measuring Wheat, forage ...... 0 .3 Wheat, hay ...... 0 .2 only methamidophos, O,S-dimethyl Wheat, straw ...... 0 .1 phosphoramidothioate, in or on the commodity. [68 FR 39441, July 1, 2003, as amended at 73 FR 52614, Sept. 10, 2008] Parts per Expiration/ Commodity million Revocation Date § 180.317 Propyzamide; tolerances for Tomato ...... 2.0 12/31/13 residues. (a) General. Tolerances are estab- (d) Indirect or inadvertent residues. lished for residues of the herbicide [Reserved] propyzamide, including its metabolites [75 FR 60243, Sept. 29, 2010] and degradates, in or on the commod- ities in the table in this paragraph. § 180.316 Pyrazon; tolerances for resi- Compliance with the tolerance levels dues. specified in this paragraph is to be de- (a) General. Tolerances are estab- termined by measuring only those lished for combined residues of the her- propyzamide residues convertible to bicide pyrazon (5-amino-4-chloro-2- methyl 3,5-dichlorobenzoate, expressed phenyl-3(2H)-pyridazinone) and its me- as the stoichiometric equivalent of tabolites (calculated as pyrazon) in or propyzamide, 3,5-dichloro-N-(1,1-di- on the following food commodities: methyl-2-propynyl)benzamide, in or on the commodity. Commodity Parts per million Parts per Commodity million Beet, garden, roots ...... 0 .9 Beet, garden, tops ...... 7 .0 Alfalfa, seed ...... 10 .0 Beet, sugar, molasses ...... 1 .5 Animal feed, nongrass, group 18 ...... 10 .0 Beet, sugar, roots ...... 0 .2 Apple ...... 0.1 Beet, sugar, tops ...... 3.0 Artichoke, globe ...... 0.01 Cattle, fat ...... 0.10 Blackberry ...... 0 .05 Cattle, liver ...... 0 .15 Blueberry ...... 0 .05 Cattle, meat ...... 0 .10 Boysenberry ...... 0 .05 Cattle, meat byproducts, except liver ...... 0 .10 Cattle, fat ...... 0.2 Goat, fat ...... 0 .10 Cattle, kidney ...... 0 .4 Goat, liver ...... 0.15 Cattle, liver ...... 0 .4 Goat, meat ...... 0.10 Cattle, meat ...... 0 .02 Goat, meat byproducts, except liver ...... 0 .10 Cattle, meat byproducts, except kidney and liver 0.02 Horse, fat ...... 0 .10 Egg ...... 0 .02 Horse, liver ...... 0 .15 Endive ...... 1.0 Horse, meat ...... 0 .10 Fruit, stone, group 12 ...... 0 .1 Horse, meat byproducts, except liver ...... 0 .10 Goat, fat ...... 0 .2 Milk ...... 0.02 Goat, kidney ...... 0 .4 Sheep, fat ...... 0 .10 Goat, liver ...... 0.4 Sheep, liver ...... 0.15 Goat, meat ...... 0.02 Sheep, meat ...... 0.10 Goat, meat byproducts, except kidney and liver 0 .02 Sheep, meat byproducts, except liver ...... 0 .10 Grape ...... 0 .1 Hog, fat ...... 0 .2 (b) Section 18 emergency exemptions. Hog, kidney ...... 0.4 [Reserved] Hog, liver ...... 0 .4 Hog, meat ...... 0 .02 (c) Tolerances with regional registra- Hog, meat byproducts, except kidney and liver .. 0 .02 tions. [Reserved] Horse, fat ...... 0 .2 (d) Indirect or inadvertent residues. Horse, kidney ...... 0 .4 Horse, liver ...... 0 .4 Tolerances are established for com- Horse, meat ...... 0 .02 bined residues of the herbicide pyrazon, Horse, meat byproducts, except kidney and liver 0 .02

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methyl-2-propynyl)benzamide, in or on Commodity Parts per million the commodity. Lettuce, head ...... 1.0 Parts per Milk ...... 0.02 Commodity million Pear ...... 0 .1 Poultry, fat ...... 0.02 Grain, cereal, forage, group 16 ...... 0 .6 Poultry, liver ...... 0 .2 Grain, cereal, hay, group 16 ...... 0 .2 Poultry, meat ...... 0 .02 Grain, cereal, straw, group 16 ...... 0 .3 Poultry, meat byproducts, except liver ...... 0 .02 Radicchio ...... 2.0 Raspberry ...... 0 .05 [72 FR 52018, Sept. 12, 2007, as amended at 76 Sheep, fat ...... 0 .2 FR 23493, Apr. 27, 2011] Sheep, kidney ...... 0.4 Sheep, liver ...... 0.4 § 180.318 4-(2-Methyl-4-chlorophenoxy) Sheep, meat ...... 0.02 butyric acid; tolerance for residues. Sheep, meat byproducts, except kidney and liver ...... 0 .02 (a) General. (1) A tolerance is estab- lished for the herbicide 4-(2-methyl-4- (b) Section 18 emergency exemptions. chlorophenoxy) butyric acid in or on [Reserved] the following food commodity: (c) Tolerances with regional registra- Parts per tions. Tolerances with regional reg- Commodity million istration, as defined in § 180.1(l), are es- tablished for residues of the herbicide Pea ...... 0 .1(N) propyzamide, including its metabolites and degradates, in or on the commod- (2) Tolerances are established for the ities in the table in this paragraph. combined residues, free and con- Compliance with the tolerance levels jugated, of the herbicide MCPB, 4-(4- specified in this paragraph is to be de- chloro-2-methylphenoxy)butanoic acid, termined by measuring only those and its metabolite MCPA, (4-chloro-2- propyzamide residues convertible to methylphenoxy)acetic acid, in or on methyl 3,5-dichlorobenzoate, expressed the following food commodities: as the stoichiometric equivalent of Parts per propyzamide, 3,5-dichloro-N-(1,1-di- Commodity million methyl-2-propynyl)benzamide, in or on Peppermint, tops ...... 0 .20 the commodity. Spearmint, tops ...... 0 .20

Parts per Commodity million (b) Section 18 emergency exemptions. [Reserved] Pea, field, seed ...... 0 .05 (c) Tolerances with regional registra- Rhubarb ...... 0 .1 tions. [Reserved] (d) Indirect or inadvertent residues. (d) Indirect or inadvertent residues. [Reserved] Tolerances are established for indirect or inadvertent residues of the herbicide [68 FR 39441, July 1, 2003, as amended at 73 propyzamide, including its metabolites FR 66785, Nov. 12, 2008] and degradates, in or on the commod- ities in the table in this paragraph. § 180.319 Interim tolerances. Compliance with the tolerance levels (a) General. While petitions for toler- specified in this paragraph is to be de- ances for negligible residues are pend- termined by measuring only those ing and until action is completed on propyzamide residues convertible to these petitions, interim tolerances are methyl 3,5-dichlorobenzoate, expressed established for residues of the listed as the stoichiometric equivalent of pesticide chemicals in or on the fol- propyzamide, 3,5-dichloro-N-(1,1-di- lowing raw agricultural commodities:

Raw Expiration/ Substances Uses Tolerance in parts per million agricultural revocation commodity date

Endothall (7-oxabicyclo- Herbicide ...... 0.2 ...... Beet, sugar ...... None (2,2,1)heptane 2,3-dicarboxylic acid.

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Raw Expiration/ Substances Uses Tolerance in parts per million agricultural revocation commodity date

Methyl parathion ...... Herbicide ...... 0.5 ...... Rye ...... 12/31/13

(b) Section 18 emergency exemptions. dibromo-4-hydroxybenzonitrile, includ- [Reserved] ing its metabolites and degradates, in (c) Tolerances with regional registra- or on the commodities in the table tions. [Reserved] below. Compliance with the tolerance (d) Indirect or inadvertent residues. levels is to be determined by meas- [Reserved] uring only bromoxynil and its metabo- lite, 3,5-dibromo-4-hydroxybenzoic acid [77 FR 59126, Sept. 26, 2012, as amended at 79 FR 27502, May 14, 2014] (DBHA), resulting from application of its octanoic and/or heptanoic acid § 180.324 Bromoxynil; tolerances for ester, in or on the commodities. residues. Parts per (a) General. (1) Tolerances are estab- Commodity million lished for residues of the herbicide bromoxynil, including its metabolites Cattle, fat ...... 1 Cattle, meat byproducts ...... 3.5 and degradates, in or on the commod- Cattle, meat ...... 0 .5 ities in the table below. Compliance Cotton, gin byproducts ...... 7 .0 with the tolerance levels is to be deter- Cotton, hulls ...... 5 .0 mined by measuring only bromoxynil, Cotton, undelinted seed ...... 1 .5 3,5-dibromo-4-hydroxybenzonitrile, re- Egg ...... 0 .05 Goat, fat ...... 1 sulting from application of its octanoic Goat, meat byproducts ...... 3 .5 and/or heptanoic acid ester, in or on Goat, meat ...... 0.5 the commodities. Hog, fat ...... 1 Hog, meat byproducts ...... 3 .5 Commodity Parts per Hog, meat ...... 0 .5 million Horse, fat ...... 1 Alfalfa, forage ...... 0.1 Horse, meat byproducts ...... 3 .5 Alfalfa, hay ...... 0.5 Horse, meat ...... 0 .5 Barley, grain ...... 0 .05 Milk ...... 0.4 Barley, hay ...... 9 .0 Poultry, fat ...... 0.05 Barley, straw ...... 4 .0 Poultry, meat byproducts ...... 0.3 Corn, field, forage ...... 0 .3 Poultry, meat ...... 0 .05 Corn, field, grain ...... 0 .05 Sheep, fat ...... 1 Corn, field, stover ...... 0 .2 Sheep, meat byproducts ...... 3 .5 Corn, pop, grain ...... 0.05 Sheep, meat ...... 0.5 Corn, pop, stover ...... 0.2 Flax, seed ...... 0 .1 Garlic ...... 0 .1 (b) Section 18 emergency exemptions. Grain, aspirated fractions ...... 1 .2 [Reserved] Grass, forage ...... 18 Grass, hay ...... 5 .0 (c) Tolerances with regional registra- Oat, forage ...... 0 .3 tions. [Reserved] Oat, grain ...... 0 .05 (d) Indirect or inadvertent residues. Oat, hay ...... 9.0 Oat, straw ...... 4.0 [Reserved] Onion, bulb ...... 0 .1 Peppermint, hay ...... 0 .1 [62 FR 33023, June 18, 1997, as amended at 63 Rye, forage ...... 1 .0 FR 26480, May 13, 1998; 66 FR 47402, Sept. 12, Rye, grain ...... 0.05 2001; 70 FR 7046, Feb. 10, 2005; 72 FR 35666, Rye, straw ...... 2 .0 June 29, 2007; 72 FR 41930, Aug. 1, 2007; 76 FR Sorghum, grain, forage ...... 0.8 31491, June 1, 2011] Sorghum, grain, grain ...... 0 .2 Sorghum, grain, stover ...... 0 .2 Spearmint, hay ...... 0 .1 § 180.328 Napropamide; tolerances for Wheat, forage ...... 1 .0 residues. Wheat, grain ...... 0 .05 Wheat, hay ...... 4 .0 (a) General. Tolerances are estab- Wheat, straw ...... 2 .0 lished for residues of the herbicide napropamide, N,N-diethyl-2-(1- (2) Tolerances are established for res- napthalenyloxy) propionamide, in or on idues of the herbicide bromoxynil, 3,5- the following food commodities:

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Expiration/ Parts per Commodity Parts per revocation Commodity million million date Melon ...... 0 .2 Almond, hulls ...... 0.1 None Onion, bulb ...... 0 .05 Asparagus ...... 0.1 None Orange ...... 1 .0 Basil ...... 0.1 None Pepper ...... 0 .75 Berry group 13 ...... 0.1 None Peppermint, tops ...... 12 .5 Coffee, green bean ...... 0.1 None Pumpkin ...... 0.2 Cranberry ...... 0.1 None Safflower, seed ...... 1 .0 Grape ...... 0.1 None Sorghum, forage, forage ...... 2 .0 Kiwifruit ...... 0.1 None Sorghum, grain, forage ...... 2.0 Marjoram ...... 0.1 None Sorghum, grain, grain ...... 0 .75 Nut, tree, group 14 ...... 0.1 None Spearmint, tops ...... 12 .5 Peppermint, tops ...... 0.1 None Squash, summer ...... 1 .0 Persimmon ...... 0.1 None Squash, winter ...... 0 .3 Rhubarb ...... 0.1 None Strawberry ...... 2 .0 Rosemary ...... 0.1 None Walnut ...... 0 .05 Savory, summer ...... 0.1 None Savory, winter ...... 0.1 None (2) Tolerances are established for the Spearmint, tops ...... 0.1 None Strawberry ...... 0.1 None combined residues of the insecticide Sweet potato, roots ...... 0.1 None oxydemeton-methyl (S-(2- Vegetable, brassica, leafy, group 5 0.1 None (ethylsulfinyl)ethyl) O,O-dimethyl Vegetable, fruiting, group 8 ...... 0.1 None phosphorothioate) and its cholin- (b) Section 18 emergency exemptions. esterase-inhibiting metabolites in or [Reserved] on the following food commodities: (c) Tolerances with regional registra- Parts per tions. [Reserved] Commodity million (d) Indirect or inadvertent residues. Cattle, fat ...... 0.01 [Reserved] Cattle, meat ...... 0 .01 Cattle, meat byproducts ...... 0.01 [73 FR 52614, Sept. 10, 2008, as amended at 76 Egg ...... 0 .01 FR 34885, June 15, 2011] Goat, fat ...... 0 .01 Goat, meat ...... 0.01 § 180.330 S-(2-(Ethylsulfinyl)ethyl) O,O- Goat, meat byproducts ...... 0 .01 dimethyl phosphorothioate; toler- Hog, fat ...... 0 .01 Hog, meat ...... 0 .01 ances for residues. Hog, meat byproducts ...... 0 .01 (a) General. (1) Tolerances are estab- Horse, fat ...... 0 .01 Horse, meat ...... 0 .01 lished for the combined residues of the Horse, meat byproducts ...... 0 .01 insecticide oxydemeton-methyl (S-(2- Milk ...... 0.01 (ethylsulfinyl)ethyl) O,O-dimethyl Poultry, fat ...... 0.01 Poultry, meat ...... 0 .01 phosphorothioate) and its metabolite Poultry, meat byproducts ...... 0.01 oxydemeton-methyl sulfone in or on Sheep, fat ...... 0 .01 the following food commodities: Sheep, meat ...... 0.01 Sheep, meat byproducts ...... 0 .01 Parts per Commodity million (b) Section 18 emergency exemptions. Alfalfa, forage ...... 5.0 [Reserved] Alfalfa, hay ...... 11.0 (c) Tolerances with regional registra- Bean, lima ...... 0 .2 tions. Tolerances with regional reg- Beet, sugar, roots ...... 0 .3 istrations, as defined in § 180.1(l), are Beet, sugar, tops ...... 0.5 Broccoli ...... 1 .0 established for the combined residues Brussels sprouts ...... 1 .0 of the insecticide oxydemeton-methyl Cabbage ...... 2 .0 (S-(2-(ethylsulfinyl)-ethyl) O,O-di- Cauliflower ...... 1 .0 Clover, forage ...... 5.0 methyl phosphorothioate) and its me- Clover, hay ...... 10.0 tabolite oxydemeton-methyl sulfone in Corn, sweet, forage ...... 1 .0 or on the following food commodities: Corn, sweet, kernel plus cob with husks re- moved ...... 0 .5 Commodity Parts per million Corn, sweet, stover ...... 3 .0 Cotton, undelinted seed ...... 0 .02 Broccoli raab ...... 2 .0 Cucumber ...... 1 .0 Eggplant ...... 1.0 Grapefruit ...... 1 .0 (d) Indirect or inadvertent residues. Hazelnut ...... 0 .05 [Reserved] Lemon ...... 1.0 Lettuce, head ...... 2.0 [72 FR 54578, Sept. 26, 2007]

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§ 180.331 4-(2,4-Dichlorophenoxy) bu- Commodity Parts per tyric acid; tolerances for residues. million (a) General. Tolerances are estab- Corn, sweet, stover ...... 0 .1 lished for residues of the herbicide 4- Egg ...... 0 .01 Goat, fat ...... 0 .7 (2,4-dichlorophenoxy) butyric acid (2,4- Goat, meat ...... 0.7 DB), both free and conjugated, deter- Goat, meat byproducts ...... 0 .7 mined as the acid, in or on food com- Grass, forage ...... 2 .0 modities, as follows: Grass, hay ...... 7 .0 Hog, fat ...... 0 .7 Parts per Hog, meat ...... 0 .7 Commodity million Hog, meat byproducts ...... 0 .7 Horse, fat ...... 0 .7 Alfalfa, forage ...... 0.7 Horse, meat ...... 0 .7 Alfalfa, hay ...... 2.0 Horse, meat byproducts ...... 0 .7 Cattle, meat byproducts ...... 0.05 Lentil ...... 0.05 Clover, forage ...... 0.2 Milk ...... 0.05 Clover, hay ...... 0.2 Pea, dry, seed ...... 0 .05 Goat, meat byproducts ...... 0 .05 Pea, field, hay ...... 4.0 Hog, meat byproducts ...... 0 .05 Pea, field, vines ...... 0 .5 Horse, meat byproducts ...... 0 .05 Pea, succulent ...... 0 .1 Peanut ...... 0 .2 Potato ...... 0 .6 Peppermint, tops ...... 0 .2 Potato, chips ...... 3 .0 Sheep, meat byproducts ...... 0 .05 Potato, processed potato waste ...... 3 .0 Soybean, forage ...... 0 .7 Poultry, fat ...... 0.7 Soybean, hay ...... 2 .0 Poultry, meat ...... 0 .7 Soybean, seed ...... 0 .5 Poultry, meat byproducts ...... 0.7 Spearmint, tops ...... 0 .2 Trefoil, forage ...... 0 .7 Sainfoin, forage ...... 2 .0 Trefoil, hay ...... 2 .0 Sainfoin, hay ...... 7 .0 Sheep, fat ...... 0 .7 Sheep, meat ...... 0.7 (b) Section 18 emergency exemptions. Sheep, meat byproducts ...... 0 .7 [Reserved] Soybean, seed ...... 0 .3 (c) Tolerances with regional registra- Soybean, forage ...... 4 .0 tions. [Reserved] Soybean, hay ...... 4 .0 Sugarcane, cane ...... 0.1 (d) Indirect or inadvertent residues. Sugarcane, molasses ...... 2 .0 [Reserved] Tomato ...... 0.1 Wheat, bran ...... 3.0 [73 FR 54961, Sept. 24, 2008, as amended at 74 Wheat, forage ...... 2 .0 FR 46374, Sept. 9, 2009] Wheat, germ ...... 3 .0 Wheat, grain ...... 0 .75 § 180.332 Metribuzin; tolerances for Wheat, hay ...... 7 .0 residues. Wheat, middlings ...... 3 .0 Wheat, shorts ...... 3 .0 (a) General. Tolerances are estab- Wheat, straw ...... 1 .0 lished for combined residues of the her- bicide metribuzin (4-amino-6-(1,1- (b) Section 18 emergency exemptions. dimethyl- ethyl)-3-(methylthio)-;1,2,4- [Reserved] triazin-5(4H)-one) and its triazinone (c) Tolerances with regional registra- metabolites in or on food commodities: tions. [Reserved] (d) Indirect or inadvertent residues. Parts per Commodity million [Reserved]

Alfalfa, forage ...... 2.0 [42 FR 62913, Dec. 14, 1977, as amended at 43 Alfalfa, hay ...... 7.0 FR 41396, Sept. 18, 1978; 44 FR 26744, May 7, Asparagus ...... 0.1 1979; 44 FR 45387, Aug. 2, 1979; 52 FR 23654, Barley, grain ...... 0 .75 June 24, 1987; 55 FR 26440, June 28, 1990; 62 FR Barley, hay ...... 7 .0 66024, 66025, Dec. 17, 1997; 65 FR 33698, May 24, Barley, pearled barley ...... 3 .0 2000; 66 FR 63198, Dec. 5, 2001; 67 FR 49617, Barley, straw ...... 1 .0 Carrot, roots ...... 0.3 July 31, 2002] Cattle, fat ...... 0.7 Cattle, meat ...... 0 .7 § 180.337 Oxytetracycline; tolerances Cattle, meat byproducts ...... 0.7 for residues. Corn, field, forage ...... 0 .1 Corn, field, grain ...... 0 .05 (a) General. Tolerances are estab- Corn, field, stover ...... 0 .1 lished for residues of the fungicide/ Corn, pop, grain ...... 0.05 bactericide oxytetracycline, including Corn, sweet, forage ...... 0 .1 Corn, sweet, kernel plus cob with husks re- its metabolites and degradates, in or moved ...... 0 .05 on the commodities in the table in this

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paragraph. Compliance with the toler- Commodity Parts per ance levels specified in this paragraph million is to be determined by measuring only Vetch, hay ...... 2 .0 oxytetracycline, Wheat, forage ...... 20 (4S,4aR,5S,5aR,6S,12aS)-4- Wheat, grain ...... 1 .0 Wheat, hay ...... 115 (dimethylamino)-1,4,4a,5,5a,6,11,12a- Wheat, straw ...... 25 octahydro-3,5,6,10,12,12a-hexahydroxy- 6-methyl-1,11-dioxo-2- (2) Tolerances are established for res- naphthacenecarboxamide, in or on the idues of the herbicide MCPA ((4-chloro- commodity. 2-methylphenoxy)acetic acid) resulting Parts per from the direct application of MCPA or Commodity million its sodium or dimethylamine salts, or its 2-ethylhexyl ester in or on the fol- Apple ...... 0.35 Peach ...... 0 .35 lowing food commodities: Pear ...... 0 .35 Parts per Commodity million (b) Section 18 emergency exemptions. [Reserved] Cattle, fat ...... 0.1 (c) Tolerances with regional registra- Cattle, meat ...... 0 .1 Cattle, meat byproducts ...... 0.1 tions. [Reserved] Goat, fat ...... 0 .1 (d) Indirect or inadvertent residues. Goat, meat ...... 0.1 [Reserved] Goat, meat byproducts ...... 0 .1 Hog, fat ...... 0 .1 [76 FR 23493, Apr. 27, 2011] Hog, meat ...... 0 .1 Hog, meat byproducts ...... 0 .1 § 180.339 MCPA; tolerances for resi- Horse, fat ...... 0 .1 dues. Horse, meat ...... 0 .1 Horse, meat byproducts ...... 0 .1 (a) General. (1) Tolerances are estab- Milk ...... 0.1 lished for residues of the herbicide Sheep, fat ...... 0 .1 MCPA ((4-chloro-2- Sheep meat ...... 0 .1 Sheep meat byproducts ...... 0 .1 methylphenoxy)acetic acid), both free and conjugated, resulting from the di- (b) Section 18 emergency exemptions. rect application of MCPA or its sodium [Reserved] or dimethylamine salts, or its 2- (c) Tolerances with regional registra- ethylhexyl ester in or on the following tions. [Reserved] food commodities: (d) Indirect or inadvertent residues. Parts per [Reserved] Commodity million [72 FR 28888, May 23, 2007, as amended at 73 Alfalfa, forage ...... 0.5 FR 5109, Jan. 29, 2008] Alfalfa, hay ...... 2.0 Barley, grain ...... 1 .0 § 180.341 2,4-Dinitro-6-octylphenyl cro- Barley, hay ...... 40 Barley, straw ...... 25 tonate and 2,6-dinitro-4-octylphenyl Clover, forage ...... 0.5 crotonate; tolerances for residues. Clover, hay ...... 2.0 (a) General. Tolerances are estab- Flax, seed ...... 0 .1 Grain, aspirated fractions ...... 3 .0 lished for combined negligible residues Grass, forage ...... 300 of a fungicide and insecticide that is a Grass, hay ...... 20 mixture of 2,4-dinitro-6-octylphenyl Lespedeza, forage ...... 0 .5 Lespedeza, hay ...... 2.0 crotonate and 2,6-dinitro-4-octylphenyl Oat, forage ...... 20 crotonate in or on raw agricultural Oat, grain ...... 1 .0 commodities as follows: Oat, hay ...... 115 Oat, straw ...... 25 Parts per Pea, dry ...... 0 .1 Commodity million Pea, field, hay ...... 0.1 Pea, succulent ...... 0 .1 Apple 1 ...... 0.1 Pea, field, vines ...... 0 .1 Grape 1 ...... 0 .1 Rye, forage ...... 20 Rye, grain ...... 1.0 1 There are no U.S. registrations on apple and grape as of Rye, straw ...... 25 October 24, 2002. Trefoil, forage ...... 0 .5 Trefoil, hay ...... 2 .0 (b) Section 18 emergency exemptions. Vetch, forage ...... 0 .5 [Reserved]

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(c) Tolerances with regional registra- Commodity Parts per tions. [Reserved] million (d) Indirect or inadvertent residues. Peppermint, oil ...... 8 .0 [Reserved] Plum, prune, fresh ...... 0.05 Poultry, fat ...... 0.1 [40 FR 29715, July 15, 1975, as amended at 63 Poultry, meat ...... 0 .1 FR 57076, Oct. 26, 1998; 69 FR 43924, July 23, Poultry, meat byproducts ...... 0.1 2004] Pumpkin ...... 0.05 Radish ...... 2 .0 Rutabaga ...... 0 .5 § 180.342 Chlorpyrifos; tolerances for Sheep, fat ...... 0 .2 residues. Sheep, meat ...... 0.05 (a) General. (1) Tolerances are estab- Sheep, meat byproducts ...... 0 .05 Spearmint, tops ...... 0 .8 lished for residues of the pesticide Spearmint, oil ...... 8 .0 chlorpyrifos per se (O,O-diethyl-O- Sorghum, grain, forage ...... 0.5 (3,5,6-trichloro-2-pyridyl) Sorghum, grain, grain ...... 0 .5 Sorghum, grain, stover ...... 2 .0 phosphorothioate) in or on the fol- Soybean, seed ...... 0 .3 lowing food commodities: Strawberry ...... 0 .2 Sunflower, seed ...... 0.1 Commodity Parts per Sweet potato, roots ...... 0 .05 million Turnip, roots ...... 1 .0 Turnip, tops ...... 0.3 Alfalfa, forage ...... 3.0 Vegetable, brassica, leafy, group 5 ...... 1.0 Alfalfa, hay ...... 13 Vegetable, legume, group 6. except soybean .... 0 .05 Almond ...... 0.2 Walnut ...... 0 .2 Almond, hulls ...... 12 Wheat, forage ...... 3 .0 Apple ...... 0.01 Wheat, grain ...... 0 .5 Apple, wet pomace ...... 0 .02 Wheat, straw ...... 6 .0 Banana ...... 0.1 Beet, sugar, dried pulp ...... 5 .0 Beet, sugar, molasses ...... 15 (2) Chlorpyrifos [O,O-diethyl O-(3,5,6- Beet, sugar, roots ...... 1 .0 trichloro-2-pyridyl) phosphorothioate] Beet, sugar, tops ...... 8.0 may be safely used in accordance with Cattle, fat ...... 0.3 Cattle, meat ...... 0 .05 the following prescribed conditions. Cattle, meat byproducts ...... 0.05 (i) Application shall be limited solely Cherry, sweet ...... 1 .0 to spot and/or crack and crevice treat- Cherry, tart ...... 1 .0 Citrus, dried pulp ...... 5 .0 ment in food handling establishments Citrus, oil ...... 20 where food and food products are held, Corn, field, forage ...... 8 .0 processed, prepared or served. Contami- Corn, field, grain ...... 0 .05 Corn, field, refined oil ...... 0 .25 nation of food or food contact surfaces Corn, field, stover ...... 8 .0 shall be avoided. Food must be re- Corn, sweet, forage ...... 8 .0 moved or covered during treatment. Corn, sweet, kernel plus cob with husk removed 0.05 Corn, sweet, stover ...... 8 .0 (ii) Spray concentration for spot Cotton, undelinted seed ...... 0 .2 treatment shall be limited to a max- Cranberry ...... 1 .0 imum of 0.5 percent of the active ingre- Cucumber ...... 0 .05 dient by weight. A course, low-pressure Egg ...... 0 .01 Fig ...... 0 .01 spray shall be used to avoid atomiza- Fruit, citrus, group 10 ...... 1 .0 tion or splashing of the spray. Goat, fat ...... 0 .2 (iii) Paint-on application for spot Goat, meat ...... 0.05 Goat, meat byproducts ...... 0 .05 treatment shall be limited to a max- Hazelnut ...... 0 .2 imum of 2 percent of the active ingre- Hog, fat ...... 0 .2 dient by weight. Hog, meat ...... 0 .05 Hog, meat byproducts ...... 0 .05 (iv) Crack and crevice treatment Horse, fat ...... 0 .25 shall be limited to a maximum of 2 per- Horse, meat ...... 0 .25 cent of the active ingredient by weight. Horse, meat byproducts ...... 0 .25 Equipment capable of delivering a pin- Kiwifruit ...... 2.0 Milk, fat (Reflecting 0.01 ppm in whole milk) ...... 0 .25 stream of insecticide shall be used. Nectarine ...... 0 .05 (v) Application via adhesive strips Onion, bulb ...... 0 .5 shall contain a maximum of 10% by Peach ...... 0 .05 Peanut ...... 0 .2 weight of the controlled-release prod- Peanut, refined oil ...... 0.2 uct in food-handling establishments Pear ...... 0 .05 where food and food products are held, Pecan ...... 0 .2 Pepper ...... 1 .0 processed, prepared, or served. A max- Peppermint, tops ...... 0 .8 imum of 36 strips (or 5.15 grams of

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chlorpyrifos) is to be used per 100 Commodity Parts per square feet of floor space. The strips million are not to be placed in exposed areas Asparagus ...... 5.0 where direct contact with food, uten- Grape ...... 0 .01 sils, and food-contact surfaces would be likely to occur. (d) Indirect or inadvertent residues. (vi) To assure safe use of the insecti- [Reserved] cide, its label and labeling shall con- [65 FR 33711, May 24, 2000, as amended at 67 form to that registered by the U.S. En- FR 49617, July 31, 2002; 71 FR 74817, Dec. 13, vironmental Protection Agency, and it 2006; 73 FR 53739, Sept. 17, 2008; 76 FR 56656, shall be used in accordance with such Sept. 14, 2011] label and labeling. § 180.345 Ethofumesate; tolerances for (3) A tolerance of 0.1 part per million residues. is established for residues of (a) General. Tolerances for the com- chlorpyrifos, per se, in or on food com- bined residues of the herbicide modities (other than those already cov- ethofumesate (2-ethoxy-2,3-dihydro-3,3- ered by a higher tolerance as a result dimethyl-5-benzofuranyl of use on growing crops) in food service methanesulfonate) and its metabolites establishments where food and food 2-hydroxy-2,3-dihydro-3,3-dimethyl-5- products are prepared and served, as a benzofuranyl methanesulfonate and 2,3- result of the application of chlorpyrifos dihydro-3,3-dimethyl-2-oxo-5- in microencapsulated form. benzofuranyl methanesulfonate both (i) Application of a microencap- calculated as parent compound in or on sulated product shall be limited solely the following food commodities: to spot and/or crack and crevice treat- ment in food handling establishments Commodity Parts per where food and food products are pre- million pared and served. All treatments shall Beet, garden, roots ...... 0 .5 be applied in such a manner as to avoid Beet, garden, tops ...... 5 .0 Beet, sugar, molasses ...... 0 .5 contamination of food or food contact Beet, sugar, refined sugar ...... 0 .2 surfaces. Beet, sugar, roots ...... 0 .3 (ii) Spray concentrations shall be Beet, sugar, tops ...... 4.0 Cattle, fat ...... 0.05 limited to a maximum of 0.5 percent of Cattle, meat ...... 0 .05 the active ingredient by weight. Cattle, meat byproducts ...... 0.05 (iii) For crack and crevice treatment, Garlic ...... 0 .25 Goat, fat ...... 0 .05 equipment capable of delivering a pin Goat, meat ...... 0.05 stream of spray directly into cracks Goat, meat byproducts ...... 0 .05 and crevices or capable of applying Grass, straw ...... 1 .0 Horse, fat ...... 0 .05 small amounts of insecticide into Horse, meat ...... 0 .05 cracks and crevices shall be used. Horse, meat byproducts ...... 0 .05 Onion, bulb ...... 0 .25 (iv) For spot treatment, an individual Shallot, bulb ...... 0 .25 spot shall not exceed 2 square feet. Shallot, fresh leaves ...... 0 .25 (v) To assure safe use of the insecti- Sheep, fat ...... 0 .05 Sheep, meat ...... 0.05 cide, its label and labeling shall con- Sheep, meat byproducts ...... 0 .05 form to that registered by the U.S. En- vironmental Protection Agency, and it (b) Section 18 emergency exemptions. shall be used in accordance with such [Reserved] label and labeling. (c) Tolerances with regional registra- (b) Section 18 emergency exemptions. tion. Tolerances with regional registra- [Reserved] tion as defined in 40 CFR 180.1(l) are es- (c) Tolerances with regional registra- tablished for the combined residues of tions. Tolerances with regional reg- ethofumesate,(2-ethoxy -2, 3-dihydro-3, istration, as defined in 180.1(l), are es- 3-dimethyl-5-benzofuranyl tablished for residues of the pesticide methanesulfonate) and its metabolites chlorpyrifos per se (O,O-diethyl- O- 2-hydroxy-2,3-dihydro-3,3-dimethyl-5- (3,5,6-trichloro-2-pyridyl) benzofuranyl methanesulfonate and 2,3- phosphorothioate) in or on the fol- dihydro-3,3-dimethyl-2-oxo-5- lowing food commodities: benzofuranyl methanesulfonate (both

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calculated as the parent compound) in § 180.350 Nitrapyrin; tolerances for or on the raw agricultural commod- residues. ities: (a) General. Tolerances are estab- lished for the combined residues of the Parts per Commodity million soil microbiocide nitrapyrin [2-chloro- 6-(trichloromethyl) ] and its Carrot, roots ...... 7.0 metabolite, 6-chloropicolinic acid in or on the following raw agricultural com- (d) Indirect or inadvertent residues. modities: [Reserved] Commodity Parts per [63 FR 34828, June 26, 1998, as amended at 71 million FR 51516, Aug. 30, 2006; 72 FR 52019, Sept. 12, 2007] Corn, field, forage ...... 1 .0 Corn, field, grain ...... 0 .1 Corn, field, milled byproducts ...... 0 .2 § 180.349 Fenamiphos; tolerances for Corn, field, stover ...... 1 .0 residues. Corn, pop, grain ...... 0.1 (a) General. Tolerances are estab- Corn, pop, stover ...... 1.0 Corn, sweet, forage ...... 1 .0 lished for residues of the nematicide/in- Corn, sweet, kernel plus cob with husks re- secticide fenamiphos, ethyl 3-methyl-4- moved ...... 0 .1 (methylthio)phenyl 1- Corn, sweet, stover ...... 1 .0 Sorghum, forage, forage ...... 0 .5 (methylethyl)phosphoramidate, includ- Sorghum, grain, forage ...... 0.5 ing its metabolites and degradates, in Sorghum, grain, grain ...... 0 .1 or on the commodities in the following Sorghum, grain, stover ...... 0 .5 table. Compliance with the tolerance Wheat, bran ...... 3.0 Wheat, forage ...... 2 .0 levels specified in this paragraph is to Wheat, grain ...... 0 .5 be determined by measuring only the Wheat, milled byproducts, except flour ...... 2 .0 sum of fenamiphos, ethyl 3-methyl-4- Wheat, straw ...... 6 .0 (methylthio)phenyl 1- (b) Section 18 emergency exemptions. (methylethyl)phosphoramidate, and its [Reserved] cholinesterase inhibiting metabolites (c) Tolerances with regional registra- ethyl 3-methyl-4- tions. [Reserved] (methylsulfinyl)phenyl 1- (d) Indirect or inadvertent residues. (methylethyl)phosphoramidate and [Reserved] ethyl 3-methyl-4- (methylsulfonyl)phenyl 1- [46 FR 58315, Dec. 1, 1981, as amended at 47 (methylethyl)phosphoramidate, cal- FR 22957, May 26, 1982; 52 FR 33238, Sept. 2, 1987; 58 FR 32304, June 9, 1993; 63 FR 57076, culated as the stoichiometric equiva- Oct. 26, 1998; 72 FR 53461, Sept. 19, 2007] lent of fenamiphos, in or on the com- modity. § 180.352 Terbufos; tolerances for resi- dues. Parts per Commodity million (a) General. Tolerances are estab- lished for the combined residues of the Banana1 ...... 0 .1 insecticide terbufos (phosphorodithioic Grape1 ...... 0 .1 Grape, raisin1 ...... 0 .3 acid, S-(t-butylthio)methyl O,O-diethyl Pineapple1 ...... 0 .3 ester) and its phosphorylated (cholin- esterase-inhibiting) metabolites 1 There are no U.S. registrations as of May 31, 2007. (phosphorothioic acid, S-(t- (b) Section 18 emergency exemptions. butylthio)methyl O,O-diethyl ester; [Reserved] phosphorothioic acid, S-(t- (c) Tolerances with regional registra- butylsulfinyl)methyl O,O-diethyl ester; tions. [Reserved] phosphorothioic acid, S-(t- (d) Indirect or inadvertent residues. butylsulfonyl)methyl O,O-diethyl [Reserved] ester; phosphorodithioic acid, S-(t- butylsulfinyl)methyl O,O-diethyl ester; [65 FR 33712, May 24, 2000, as amended at 73 and phosphorodithioic acid, S-(t- FR 53739, Sept. 17, 2008; 75 FR 60243, Sept. 29, butylsulfonyl)methyl O,O-diethyl 2010] ester) in or on food commodities:

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herbicide bentazon (3-isopropyl-1H- Commodity Parts per million 2,1,3-benzothiadiazin-4(3H)-one-2,2-diox- Banana ...... 0.025 ide) and its 6- and 8-hydroxy metabo- Beet, sugar, roots ...... 0 .05 lites in or on the following food com- Beet, sugar, tops ...... 0.1 modities: Coffee, green bean 1 ...... 0 .05 Corn, field, forage ...... 0 .5 Parts per Corn, field, grain ...... 0 .5 Commodity million Corn, field, stover ...... 0 .5 Corn, pop, grain ...... 0.5 Bean, dry, seed ...... 0 .05 Corn, pop, stover ...... 0.5 Bean, succulent ...... 0 .5 Corn, sweet, kernel plus cob with husks re- Corn, field, forage ...... 3 .0 moved ...... 0 .05 Corn, field, grain ...... 0 .05 Corn, sweet, forage ...... 0 .5 Corn, sweet, stover ...... 0 .5 Corn, field, stover ...... 3 .0 Sorghum, grain, forage ...... 0.5 Corn, pop, grain ...... 0.05 Sorghum, grain, grain ...... 0 .05 Corn, sweet, kernel plus cob with husks re- Sorghum, grain, stover ...... 0 .5 moved ...... 0 .05 Cowpea, forage ...... 10 .0 1 There are no U. S. registrations as of August 2, 1995, for Cowpea, hay ...... 3 .0 the use of terbufos on the growing crop, coffee. Flax, seed ...... 1 .0 (b) Section 18 emergency exemptions. Pea, dry, seed ...... 1 .0 Pea, field, hay ...... 8.0 [Reserved] Pea, field, vines ...... 3 .0 (c) Tolerances with regional registra- Pea, succulent ...... 3 .0 tions. [Reserved] Peanut ...... 0 .05 (d) Indirect or inadvertent residues. Peanut, hay ...... 3.0 [Reserved] Pepper, nonbell ...... 0 .05 Peppermint, tops ...... 1 .0 [73 FR 53740, Sept. 17, 2008] Rice, grain ...... 0 .05 Rice, hulls ...... 0 .25 § 180.353 Desmedipham; tolerances for Rice, straw ...... 3 .0 Sorghum, forage ...... 0 .20 residues. Sorghum, grain, grain ...... 0 .05 (a) General. Tolerances are estab- Sorghum, grain, stover ...... 0 .05 lished for residues of the herbicide Soybean, forage ...... 8 .0 Soybean, hay ...... 8 .0 desmedipham, (ethyl-m- Soybean, seed ...... 0 .05 hydroxycarbanilate carbanilate) in or Spearmint, tops ...... 1 .0 on the following raw agricultural com- modities in the table that follows: (2) Tolerances are established for the combined residues of the herbicide Parts per Commodity million bentazon (3-isopropyl-1H-2,1,3- benzothiadiazin-4(3H)-one-2,2-dioxide) Beet, garden, roots ...... 0 .05 and its metabolite 2-amino-N-isopropyl Beet, garden, tops ...... 1 .0 Beet, sugar, roots ...... 0 .1 benzamide (AIBA) in or on the fol- Beet, sugar, tops ...... 5.0 lowing food commodities: Spinach ...... 6 .0 Commodity Parts per (b) Section 18 emergency exemptions. million [Reserved] Cattle, fat ...... 0.05 (c) Tolerances with regional registra- Cattle, meat byproducts ...... 0.05 tions. [Reserved] Cattle, meat ...... 0 .05 Egg ...... 0 .05 (d) Indirect or inadvertent residues. Goat, fat ...... 0 .05 [Reserved] Goat, meat byproducts ...... 0 .05 Goat, meat ...... 0.05 [40 FR 4658, Jan. 31, 1975, as amended at 62 Hog, fat ...... 0 .05 FR 45747, Aug. 29, 1997; 63 FR 49472, Sept. 16, Hog, meat byproducts ...... 0 .05 1998; 64 FR 46292, Aug. 25, 1999; 65 FR 82293, Hog, meat ...... 0 .05 Dec. 28, 2000; 66 FR 64773, Dec. 14, 2001; 68 FR Milk ...... 0.02 37764, June 25, 2003; 69 FR 71717, Dec. 10, 2004; Poultry, fat ...... 0.05 72 FR 53449, Sept. 19, 2007; 73 FR 53740, Sept. Poultry, meat byproducts ...... 0.05 17, 2008] Poultry, meat ...... 0 .05 Sheep, fat ...... 0 .05 Sheep, meat byproducts ...... 0 .05 § 180.355 Bentazon; tolerances for resi- Sheep, meat ...... 0.05 dues. (a) General. (1) Tolerances are estab- (b) Section 18 emergency exemptions. lished for the combined residues of the [Reserved]

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(c) Tolerances with regional registra- Commodity Parts per tions. Tolerances with regional reg- million istration as defined in § 180.1(m), are es- Hog, fat ...... 0 .1 tablished for combined residues of the Hog, liver ...... 0 .50 herbicide, bentazon (3-isopropyl-1H-2, Hog, meat ...... 0 .1 Hog, meat byproducts, except liver ...... 0 .1 1,3-benzothiadiazin-4(3H)-one-2,2-diox- Hop, dried cones ...... 3 .0 ide) and its 6- and 8-hydroxy metabo- Hop, vines ...... 1 .0 lites in or on the following food com- Horse, fat ...... 0 .1 Horse, liver ...... 0 .50 modities: Horse, meat ...... 0 .1 Horse, meat byproducts, except liver ...... 0 .1 Parts per Milk ...... 0.1 Commodity million Nectarine ...... 0 .1 Clover, forage ...... 1.0 Peach ...... 0 .1 Clover, hay ...... 2.0 Peanut ...... 0 .05 Peanut, hay ...... 5.50 Peanut, hay ...... 1.5 (d) Indirect or inadvertent residues. Pear ...... 0 .1 [Reserved] Pecan ...... 0 .1 Plum, prune, fresh ...... 0.1 [42 FR 26979, May 26, 1977] Poultry, fat ...... 0.1 Poultry, meat ...... 0 .1 EDITORIAL NOTE: For FEDERAL REGISTER ci- Poultry, meat byproducts ...... 0.1 tations affecting § 180.355, see the List of CFR Raspberry ...... 0 .2 Sections Affected, which appears in the Sheep, fat ...... 0 .1 Finding Aids section of the printed volume Sheep, liver ...... 0.50 and at www.fdsys.gov. Sheep, meat ...... 0.1 Sheep, meat byproducts, except liver ...... 0 .1 Soybean ...... 0.1 § 180.356 Norflurazon; tolerances for Soybean, forage ...... 1 .0 residues. Soybean, hay ...... 1 .0 (a) General. Tolerances are estab- Walnut ...... 0 .1 lished for the combined residues of the (b) Section 18 emergency exemptions. herbicide norflurazon (4-chloro-5- [Reserved] (methylamino)-2-(alpha, alpha, alpha- (c) Tolerances with regional registra- trifluoro-m-tolyl)-3-(2H)-pyridazinone) tion. [Reserved] and its desmethyl metabolite 4-chloro- (d) Indirect or inadvertent residues. 5-(amino)-2-alpha, alpha, alpha- [Reserved] trifluoro-m-tolyl)-3(2H)-pyridazinone in or on the following raw agricultural [47 FR 14909, Apr. 7, 1982] commodities: EDITORIAL NOTE: For FEDERAL REGISTER ci- tations affecting § 180.356, see the List of CFR Parts per Commodity million Sections Affected, which appears in the Finding Aids section of the printed volume Alfalfa, forage ...... 3.0 and at www.fdsys.gov. Alfalfa, hay ...... 5.0 Alfalfa, seed ...... 0 .1 § 180.360 Asulam; tolerance for resi- Almond, hulls ...... 1 .0 Almond ...... 0.1 dues. Apple ...... 0.1 (a) General. Tolerances are estab- Apricot ...... 0 .1 Asparagus ...... 0.05 lished for the combined residues of Avocado ...... 0 .20 asulam (methyl sulfanilylcarbamate) Blackberry ...... 0 .1 and its sulfanilamide containing me- Blueberry ...... 0 .2 Cattle, fat ...... 0.1 tabolites in or on the following food Cattle, liver ...... 0 .50 commodities: Cattle, meat ...... 0 .1 Cattle, meat byproducts, except liver ...... 0 .1 Commodity Parts per Cherry ...... 0.1 million Citrus, dried pulp ...... 0 .4 Citrus, molasses ...... 1.0 Cattle, fat ...... 0.05 Cotton, undelinted seed ...... 0 .1 Cattle, meat ...... 0 .05 Cranberry ...... 0 .1 Cattle, meat byproducts ...... 0.2 Fruit, citrus ...... 0 .2 Goat, fat ...... 0 .05 Goat, fat ...... 0 .1 Goat, meat ...... 0.05 Goat, liver ...... 0.50 Goat, meat byproducts ...... 0 .2 Goat, meat ...... 0.1 Hog, fat ...... 0 .05 Goat, meat byproducts, except liver ...... 0 .1 Hog, meat ...... 0 .05 Grape ...... 0 .1 Hog, meat byproducts ...... 0 .2 Hazelnut ...... 0 .1 Horse, fat ...... 0 .05

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Parts per Parts per Commodity million Commodity million

Horse, meat ...... 0 .05 Fruit, citrus, group 10–10 ...... 0 .1 Horse, meat byproducts ...... 0 .2 Fruit, pome, group 11–10 ...... 0 .1 Milk ...... 0.05 Fruit, small vine climbing, except grape, sub- Sheep, fat ...... 0 .05 group 13–07E ...... 0.10 Sheep, meat ...... 0.05 Fruit, stone, group 12–12 ...... 0 .1 Sheep, meat byproducts ...... 0 .2 Grape ...... 0 .1 Sugarcane, cane ...... 1.0 Grass forage, fodder, and hay crop group 17, Sugarcane, molasses ...... 30 forage ...... 20 Grass forage, fodder, and hay crop group 17, (b) Section 18 emergency exemptions. hay ...... 13 Grass forage, fodder, and hay crop group 17, [Reserved] straw ...... 4.0 (c) Tolerances with regional registra- Hop, dried cones ...... 0 .1 tions. [Reserved] Juneberry ...... 0 .10 Lettuce, leaf ...... 4 .0 (d) Indirect or inadvertent residues. Melon subgroup 9A ...... 0 .10 [Reserved] Nut, tree, group 14 ...... 0 .1 Olive ...... 0 .1 [68 FR 39441, July 1, 2003, as amended at 72 Onion, bulb subgroup 3–07A ...... 0.1 FR 37654, July 11, 2007] Onion, green subgroup 3–07B ...... 0.2 Peanut ...... 0 .1 § 180.361 Pendimethalin; tolerances for Peanut, hay ...... 0.1 residues. Peas (except field peas) ...... 0.10 Peppermint, oil ...... 1 .0 (a) General. Tolerances are estab- Peppermint, tops ...... 0 .2 lished for residues of the herbicide Pistachio ...... 0.1 Pomegranate ...... 0 .10 pendimethalin, including its metabo- Potato ...... 0 .1 lites and degradates, in or on the com- Rice, grain ...... 0 .1 modities. Compliance with the toler- Rice, straw ...... 0 .1 Sorghum, forage ...... 0 .1 ance levels specified in the following Sorghum, grain, grain ...... 0 .1 table below is to be determined by Sorghum, grain, stover ...... 0 .1 measuring only pendimethalin, [N- (1- Soybean, forage ...... 0 .1 Soybean, hay ...... 0 .1 ethylpropyl)-3,4-dimethyl-2,6- Soybean, seed ...... 0 .1 dinitrobenzenamine], and its metabo- Spearmint, oil ...... 1 .0 lite, 4-[(1-ethylpropyl)amino]-2-methyl- Spearmint, tops ...... 0 .2 3,5-dinitrobenzyl alcohol, calculated as Sugarcane, cane ...... 0.1 Sunflower subgroup 20B ...... 0.1 the stoichiometric equivalent of Turnip greens ...... 0 .20 pendimethalin, in or on the following Vegetable, fruiting, group 8–10 ...... 0 .1 commodities: Vegetable, soybean, succulent ...... 0 .10 Wheat, grain ...... 0 .10 Parts per Wheat, forage ...... 3 .0 Commodity million Wheat, hay ...... 0 .60 Wheat, straw ...... 0 .30 Alfalfa, forage ...... 3.5 Alfalfa, hay ...... 4.0 (b) Section 18 emergency exemptions. Alfalfa, seed ...... 0 .10 Almond, hulls ...... 6 .0 Time-limited tolerances specified in Apple, wet pomace ...... 0 .20 the following table are established for Artichoke, globe ...... 0.1 combined residues of the herbicide Asparagus ...... 0.15 pendimethalin, [N-(1-ethylpropyl)-3,4- Beans ...... 0 .10 Beans, forage ...... 0 .10 dimethyl-2,6-dinitrobenzenamine], and Beans, hay ...... 0 .10 its metabolite 4-[(1- Berry, low growing subgroup 13–07G ...... 0.1 ethylpropyl)amino]-2-methyl-3,5- Brassica head and stem, subgroup 5-A ...... 0 .1 Brassica, leafy greens, subgroup 5B ...... 0 .20 dinitrobenzyl alcohol, in or on the Carrot ...... 0 .5 specified agricultural commodities, re- Citrus, oil ...... 0.5 sulting from use of the pesticide pursu- Corn, field, forage ...... 0 .1 ant to FIFRA section 18 emergency ex- Corn, field, grain ...... 0 .1 Corn, field, stover ...... 0 .1 emptions. The tolerances expire and Corn, pop, grain ...... 0.1 are revoked on the date specified in the Corn, sweet, forage ...... 0 .1 table. Corn, sweet, kernel plus cob with husks re- moved ...... 0 .1 Expiration/ Corn, sweet, stover ...... 0 .1 Commodity Parts per revocation Cotton, gin byproducts ...... 3 .0 million date Cotton, undelinted seed ...... 0 .1 Crayfish ...... 0.05 Bermuda grass, forage ...... 25 12/31/10

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tabolites, dihydroxybis(2-methyl-2- Parts per Expiration/ Commodity revocation phenylpropyl) stannane and 2-methyl- million date 2-phenylpropylstannoic acid, cal- Bermuda grass, hay ...... 60 12/31/10 culated as the stoichiometric equiva- lent of fenbutatin-oxide, in or on the (c) Tolerances with regional registra- commodity. tions. [Reserved] (d) Indirect or inadvertent residues. Commodity Parts per [Reserved] million [49 FR 15293, Apr. 18, 1984] Cattle, fat ...... 0.5 Cattle, meat ...... 0 .5 EDITORIAL NOTE: For FEDERAL REGISTER ci- Cattle, meat byproducts ...... 0.5 tations affecting § 180.361, see the List of CFR Egg ...... 0 .1 Goat, fat ...... 0 .5 Sections Affected, which appears in the Goat, meat ...... 0.5 Finding Aids section of the printed volume Goat, meat byproducts ...... 0 .5 and at www.fdsys.gov. Hog, fat ...... 0 .5 Hog, meat ...... 0 .5 § 180.362 Fenbutatin-oxide; tolerances Hog, meat byproducts ...... 0 .5 for residues. Horse, fat ...... 0 .5 Horse, meat ...... 0 .5 (a) General. (1) Tolerances are estab- Horse, meat byproducts ...... 0 .5 lished for residues of the miticide/acar- Milk, fat ...... 0 .1 Poultry, fat ...... 0.1 icide fenbutatin-oxide, including its Poultry, meat ...... 0 .1 metabolites and degradates, in or on Poultry, meat byproducts ...... 0.1 the plant commodities in the table in Sheep, fat ...... 0 .5 Sheep, meat ...... 0.5 this paragraph. Compliance with the Sheep, meat byproducts ...... 0 .5 tolerance levels specified in this para- graph is to be determined by measuring (b) Section 18 emergency exemptions. only fenbutatin-oxide, hexakis (2-meth- [Reserved] yl-2-phenylpropyl) distannoxane, in or (c) Tolerances with regional registra- on the commodity. tions. A tolerance with regional reg- istration, as defined in § 180.1(l), is es- Parts per Commodity million tablished for residues of the miticide/ acaricide fenbutatin-oxide, including Almond, hulls ...... 80 .0 Apple ...... 15.0 its metabolites and degradates, in or Apple, wet pomace ...... 100.0 on the plant commodity in the table in Cherry, sweet ...... 6 .0 this paragraph. Compliance with the Cherry, tart ...... 6 .0 Citrus, dried pulp ...... 100.0 tolerance level specified in this para- Citrus, oil ...... 140.0 graph is to be determined by measuring Cucumber ...... 4 .0 only fenbutatin-oxide, hexakis (2-meth- Eggplant ...... 6.0 Fruit, citrus, group 10 ...... 20 .0 yl-2-phenylpropyl) distannoxane, in or Grape ...... 5 .0 on the commodity. Grape, raisin ...... 20.0 Nut, tree, group 14 ...... 0 .5 Commodity Parts per Papaya ...... 2 .0 million Peach ...... 10 .0 Pear ...... 15 .0 Raspberry ...... 10 .0 Pistachio ...... 0.5 Plum, prune, fresh ...... 4.0 (d) Indirect or inadvertent residues. Plum, prune, dried ...... 20.0 Strawberry ...... 10.0 [Reserved] [65 FR 33713, May 24, 2000, as amended at 72 (2) Tolerances are established for res- FR 41930, Aug. 1, 2007; 73 FR 5109, Jan. 29, idues of the miticide/acaricide 2008; 76 FR 23494, Apr. 27, 2011] fenbutatin-oxide, including its metabo- lites and degradates, in or on the ani- § 180.364 Glyphosate; tolerances for mal commodities in the table in this residues. paragraph. Compliance with the toler- (a) General. (1) Tolerances are estab- ance levels specified in this paragraph lished for residues of glyphosate, in- is to be determined by measuring only cluding its metabolites and degradates, the sum of fenbutatin-oxide, hexakis in or on the commodities listed below (2-methyl-2-phenylpropyl) resulting from the application of distannoxane, and its organotin me- glyphosate, the salt of

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glyphosate, the ethanolamine salt of Commodity Parts per glyphosate, the dimethylamine salt of million glyphosate, the ammonium salt of Jaboticaba ...... 0 .2 glyphosate, and the potassium salt of Jackfruit ...... 0 .2 glyphosate. Compliance with the fol- Kava, roots ...... 0 .2 Kenaf, forage ...... 200 lowing tolerance levels is to be deter- Leucaena, forage ...... 200 mined by measuring only glyphosate Longan ...... 0 .2 (N-(phosphonomethyl)glycine). Lychee ...... 0 .2 Mamey apple ...... 0 .2 Parts per Mango ...... 0.2 Commodity million Mangosteen ...... 0 .2 Marmaladebox ...... 0 .2 Acerola ...... 0.2 Mioga, flower ...... 0 .2 Alfalfa, seed ...... 0 .5 Noni ...... 0 .20 Almond, hulls ...... 25 Nut, pine ...... 1 .0 Aloe vera ...... 0 .5 Nut, tree, group 14 ...... 1 .0 Ambarella ...... 0 .2 Oilseeds, group 20, except canola ...... 40 Animal feed, nongrass, group 18 ...... 400 Okra ...... 0.5 Artichoke, globe ...... 0.2 Olive ...... 0 .2 Asparagus ...... 0.5 Oregano, Mexican, leaves ...... 2 .0 Atemoya ...... 0 .2 Palm heart ...... 0 .2 Avocado ...... 0 .2 Palm heart, leaves ...... 0 .2 Bamboo, shoots ...... 0 .2 Palm, oil ...... 0 .1 Banana ...... 0.2 Papaya ...... 0 .2 Barley, bran ...... 30 Papaya, mountain ...... 0.2 Beet, sugar, dried pulp ...... 25 Passionfruit ...... 0 .2 Beet, sugar, roots ...... 10 Pawpaw ...... 0 .2 Beet, sugar, tops ...... 10 Pea, dry ...... 8 .0 Berry and small fruit, group 13–07 ...... 0 .20 Peanut ...... 0 .1 Betelnut ...... 1 .0 Peanut, hay ...... 0.5 Biriba ...... 0 .2 Pepper leaf, fresh leaves ...... 0 .2 Blimbe ...... 0 .2 Peppermint, tops ...... 200 Breadfruit ...... 0 .2 Perilla, tops ...... 1 .8 Cacao bean, bean ...... 0 .2 Persimmon ...... 0 .2 Cactus, fruit ...... 0 .5 Pineapple ...... 0.1 Cactus, pads ...... 0 .5 Pistachio ...... 1.0 Canistel ...... 0 .2 Pomegranate ...... 0 .2 Carrot ...... 5 .0 Pulasan ...... 0 .2 Chaya ...... 1.0 Quinoa, grain ...... 5 .0 Cherimoya ...... 0 .2 Rambutan ...... 0 .2 Citrus, dried pulp ...... 1 .5 Rice, grain ...... 0 .1 Coconut ...... 0 .1 Rice, wild, grain ...... 0.1 Coffee, bean, green ...... 1 .0 Rose apple ...... 0 .2 Corn, pop, grain ...... 0.1 Sapodilla ...... 0 .2 Corn, sweet, kernel plus cob with husk removed 3.5 Sapote, black ...... 0 .2 Cotton, gin byproducts ...... 210 Sapote, mamey ...... 0 .2 Custard apple ...... 0 .2 Sapote, white ...... 0 .2 Date, dried fruit ...... 0 .2 Shellfish ...... 3 .0 Dokudami ...... 2 .0 Soursop ...... 0 .2 Durian ...... 0 .2 Spanish lime ...... 0 .2 Epazote ...... 1 .3 Spearmint, tops ...... 200 Feijoa ...... 0 .2 Spice subgroup 19B ...... 7 .0 Fig ...... 0 .2 Star apple ...... 0 .2 Fish ...... 0 .25 Starfruit ...... 0 .2 Fruit, citrus, group 10–10 ...... 0 .50 Stevia, dried leaves ...... 1 .0 Fruit, pome, group 11–10 ...... 0 .20 Sugar apple ...... 0 .2 Fruit, stone, group 12 ...... 0 .2 Sugarcane, cane ...... 2.0 Galangal, roots ...... 0 .2 Sugarcane, molasses ...... 30 Ginger, white, flower ...... 0 .2 Surinam cherry ...... 0 .2 Gourd, buffalo, seed ...... 0 .1 Sweet potato ...... 3.0 Governor’s plum ...... 0 .2 Tamarind ...... 0 .2 Gow kee, leaves ...... 0 .2 Tea, dried ...... 1 .0 Grain, cereal, forage, fodder and straw, group Tea, instant ...... 7 .0 16, except field corn, forage and field corn, Teff, forage ...... 100 stover ...... 100 Teff, grain ...... 5 .0 Grain, cereal, group 15 except field corn, pop- Teff, hay ...... 100 corn, rice, sweet corn, and wild rice ...... 30 Ti, leaves ...... 0 .2 Grass, forage, fodder and hay, group 17 ...... 300 Ti, roots ...... 0 .2 Guava ...... 0 .2 Ugli fruit ...... 0.5 Herbs subgroup 19A ...... 0 .2 Vegetable, bulb, group 3–07 ...... 0 .20 Hop, dried cones ...... 7 .0 Vegetable, cucurbit, group 9 ...... 0.5 Ilama ...... 0 .2 Vegetable, foliage of legume, subgroup 7A, ex- Imbe ...... 0 .2 cept soybean ...... 0 .2 Imbu ...... 0 .2 Vegetable, fruiting, group 8–10 (except okra) ..... 0 .10

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Parts per Finding Aids section of the printed volume Commodity million and at www.fdsys.gov.

Vegetable, leafy, brassica, group 5 ...... 0.2 § 180.367 n-Octyl bicycloheptenedi- Vegetable, leafy, except brassica, group 4 ...... 0 .2 Vegetable, leaves of root and tuber, group 2, carboximide; tolerances for resi- except sugar beet tops ...... 0 .2 dues. Vegetable, legume, group 6 except soybean (a) General. A tolerance of 5 parts per and dry pea ...... 5 .0 Vegetables, root and tuber, group 1, except car- million is established for residues of rot, sweet potato, and sugar beet ...... 0 .20 the insecticide synergist N-octyl Wasabi, roots ...... 0 .2 bicycloheptene dicarboximide, includ- Water spinach, tops ...... 0.2 Watercress, upland ...... 0 .2 ing its metabolites and degradates, in Wax jambu ...... 0 .2 or on all food items in food handling Yacon, tuber ...... 0.2 establishments where food and food products are held, processed, prepared (2) Tolerances are established for res- and/or served, provided that the food is idues of glyphosate, including its me- removed or covered prior to such use, tabolites and degradates, in or on the except for bagged food in warehouse commodities listed below resulting storage which need not be removed or from the application of glyphosate, the covered prior to applications of formu- isopropylamine salt of glyphosate, the lations containing N-octyl ethanolamine salt of glyphosate, the bicycloheptene dicarboximide. Compli- dimethylamine salt of glyphosate, the ance with the tolerance level specified ammonium salt of glyphosate, and the in this paragraph is to be determined potassium salt of glyphosate. Compli- by measuring only N-octyl ance with the following tolerance lev- bicycloheptene dicarboximide, in or on els is to be determined by measuring the commodity. only glyphosate (N- (b) Section 18 emergency exemptions. (phosphonomethyl)glycine) and its me- [Reserved] tabolite N-acetyl-glyphosate (N-acetyl- (c) Tolerances with regional registra- N-(phosphonomethyl)glycine; cal- tions. [Reserved] culated as the stoichiometric equiva- (d) Indirect or inadvertent residues. lent of glyphosate). [Reserved]

Commodity Parts per [65 FR 33713, May 24, 2000, as amended at 75 Million FR 60243, Sept. 29, 2010] Canola, seed ...... 20 Cattle, meat byproducts ...... 5.0 § 180.368 Metolachlor; tolerances for Corn, field, forage ...... 13 residues. Corn, field, grain ...... 5 .0 Corn, field, stover ...... 100 (a) General. (1) Tolerances are estab- Egg ...... 0 .05 lished for the combined residues (free Goat, meat byproducts ...... 5 .0 and bound) of the herbicide Grain aspirated fractions ...... 310 .0 Hog, meat byproducts ...... 5 .0 metolachlor, 2-chloro-N-(2- ethyl-6- Horse, meat byproducts ...... 5 .0 methylphenyl)-N-(2-methoxy-1- Poultry, meat ...... 0 .10 methylethyl)acetamide, and its me- Poultry, meat byproducts ...... 1.0 tabolites, determined as the deriva- Sheep, meat byproducts ...... 5 .0 Soybean, forage ...... 100.0 tives, 2- [(2-ethyl-6- Soybean, hay ...... 200.0 methylphenyl)amino]-1-propanol and 4- Soybean, hulls ...... 120 .0 (2-ethyl-6-methylphenyl)-2- hydroxy-5- Soybean, seed ...... 20.0 methyl-3-morpholinone, each expressed as the parent compound in the fol- (b) Section 18 emergency exemptions. lowing raw agricultural commodities: [Reserved] (c) Tolerances with regional registra- Commodity Parts per tions. [Reserved] million (d) Indirect or inadvertent residues. Almond, hulls ...... 0 .30 [Reserved] Animal feed, nongrass, group 18 ...... 1 .0 Cattle, fat ...... 0.02 [45 FR 64911, Oct. 1, 1980] Cattle, kidney ...... 0 .20 Cattle, liver ...... 0 .05 EDITORIAL NOTE: For FEDERAL REGISTER ci- Cattle, meat ...... 0 .02 tations affecting § 180.364, see the List of CFR Cattle, meat byproducts, except kidney and liver 0.04 Sections Affected, which appears in the Corn, field, forage ...... 6 .0

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lent of S-metolachlor, in or on the Commodity Parts per million commodity. Corn, field, grain ...... 0 .10 Parts per Corn, field, stover ...... 6 .0 Commodity million Corn, pop, grain ...... 0.10 Corn, pop, stover ...... 6.0 Asparagus ...... 0.10 Corn, sweet, forage ...... 6 .0 Beet, garden, leaves ...... 1 .8 Corn, sweet, kernel plus cob with husks re- Beet, sugar, molasses ...... 2 .0 moved ...... 0 .10 Beet, sugar, roots ...... 0 .5 Corn, sweet, stover ...... 6 .0 Beet, sugar, tops ...... 15.0 Cotton, gin byproducts ...... 4 .0 Brassica, head and stem, subgroup 5A ...... 0 .60 Cotton, undelinted seed ...... 0 .10 Brassica, leafy greens, subgroup 5B ...... 1 .8 Dillweed ...... 0 .50 Bushberry subgroup 13-07B ...... 0 .15 Egg ...... 0 .02 Caneberry subgroup 13-07A ...... 0.10 Goat, fat ...... 0 .02 Carrot, roots ...... 0.40 Goat, kidney ...... 0 .20 Cattle, fat ...... 0.02 Goat, liver ...... 0.05 Cattle, kidney ...... 0 .20 Goat, meat ...... 0.02 Cattle, liver ...... 0 .05 Goat, meat byproducts, except kidney and liver 0 .04 Cattle, meat ...... 0 .02 Grass, forage ...... 10 Cattle, meat byproducts, except kidney and liver 0.04 Grass, hay ...... 0 .20 Cilantro, leaves ...... 8 .0 Horse, fat ...... 0 .02 Coriander, seed ...... 0 .13 Horse, kidney ...... 0 .20 Corn, field, forage ...... 40 Horse, liver ...... 0 .05 Corn, field, grain ...... 0 .10 Horse, meat ...... 0 .02 Corn, field, stover ...... 40 Horse, meat byproducts, except kidney and liver 0 .04 Corn, pop, grain ...... 0.10 Milk ...... 0.02 Corn, pop, stover ...... 40 Nut, tree, group 14 ...... 0 .10 Corn, sweet, forage ...... 40 Okra ...... 0.50 Corn, sweet, kernel plus cob with husks re- Peanut ...... 0 .20 moved ...... 0 .10 Peanut, hay ...... 20 Corn, sweet, stover ...... 40 Peanut, meal ...... 0 .40 Cotton, gin byproducts ...... 4 .0 Potato ...... 0 .20 Cotton, undelinted seed ...... 0 .10 Poultry, fat ...... 0.02 Cucumber ...... 0 .13 Poultry, meat ...... 0 .02 Egg ...... 0 .02 Poultry, meat byproducts ...... 0.05 Grain, aspirated fractions ...... 0 .70 Safflower, seed ...... 0 .10 Goat, fat ...... 0 .02 Sheep, fat ...... 0 .02 Goat, kidney ...... 0 .20 Sheep, kidney ...... 0.20 Goat, liver ...... 0.05 Sheep, liver ...... 0.05 Goat, meat ...... 0.02 Sheep, meat ...... 0.02 Goat, meat byproducts, except kidney and liver 0 .04 Sheep, meat byproducts, except kidney and Grass, forage ...... 10 .0 liver ...... 0 .04 Grass, hay ...... 0 .20 Sorghum, grain, forage ...... 1.0 Horse, fat ...... 0 .02 Sorghum, grain, grain ...... 0 .30 Horse, kidney ...... 0 .20 Sorghum, grain, stover ...... 4 .0 Horse, liver ...... 0 .05 Soybean, forage ...... 5 .0 Horse, meat ...... 0 .02 Soybean, hay ...... 8 .0 Horse, meat byproducts, except kidney and liver 0 .04 Soybean, seed ...... 0 .20 Leaf petioles, subgroup 4B ...... 0 .10 Tomato ...... 0.10 Melon, subgroup 9A ...... 0 .10 Vegetable, foliage of legume, subgroup 7A, ex- Milk ...... 0.02 cept soybean ...... 15.0 Okra ...... 0.10 Vegetable, legume, group 6 ...... 0 .30 Onion, bulb, subgroup 3-07A ...... 0 .10 Onion, green, subgroup 3-07B ...... 2 .0 Peanut ...... 0 .20 (2) Tolerances are established for res- Peanut, hay ...... 20.0 idues of S-metolachlor, including its Peanut, meal ...... 0 .40 metabolites and degradates, in or on Poultry, fat ...... 0.02 the commodity(s), as defined. Compli- Poultry, meat ...... 0 .02 Poultry, meat byproducts ...... 0.05 ance with the tolerance levels specified Pumpkin ...... 0.10 in the following table below is to be de- Safflower, seed ...... 0 .10 termined by measuring only the sum of Sesame, seed ...... 0 .13 Sheep, fat ...... 0 .02 free and bound S-metolachlor, S-2- Sheep, kidney ...... 0.20 chloro-N-(2-ethyl-6-methylphenyl)-N- Sheep, liver ...... 0.05 (2-methoxy-1-methylethyl)acetamide, Sheep, meat ...... 0.02 its R-enantiomer, and its metabolites, Sheep, meat byproducts, except kidney and liver ...... 0 .04 determined as the derivatives, 2-(2- Sorghum, grain, forage ...... 1.0 ethyl-6-methylphenyl)amino-1-pro- Sorghum, grain, grain ...... 0 .3 panol and 4-(2-ethyl-6-methylphenyl)-2- Sorghum, grain, stover ...... 4 .0 Sorghum, sweet, stalk ...... 4.0 hydroxy-5-methyl-3-morpholinone, cal- Soybean, forage ...... 5 .0 culated as the stoichiometric equiva- Soybean, hay ...... 8 .0

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Parts per Parts per Commodity million Commodity million

Soybean, seed ...... 0 .20 Pepper, tabasco ...... 0 .50 Spinach ...... 0 .50 Squash, winter ...... 0 .10 (d) Indirect or inadvertent residues. (1) Sunflower, seed ...... 0.50 Tolerances are established for the indi- Sunflower, meal ...... 1 .0 Tomato, paste ...... 0 .30 rect or inadvertent combined residues Turnip, greens ...... 1.8 (free and bound) of the herbicide Vegetable, foliage of legume, except soybean, metolachlor, 2-chloro-N-(2-ethyl-6- subgroup 7A ...... 15 .0 methylphenyl)-N-(2-methoxy-1- Vegetable, fruiting, group 8, except tabasco methylethyl)acetamide, and its me- pepper ...... 0 .10 Vegetable, legume, group 6 ...... 0 .30 tabolites, determined as the deriva- Vegetable, root, except sugar beet, subgroup tives, 2-[(2-ethyl-6- 1B, except carrot ...... 0 .30 methylphenyl)amino]-1-propanol and 4- Vegetable, tuberous and corm, subgroup 1C ..... 0.20 (2-ethyl-6-methylphenyl)-2- hydroxy-5- methyl-3-morpholinone, each expressed (b) Section 18 emergency exemptions. as the parent compound in the fol- [Reserved] lowing raw agricultural commodities: (c) Tolerances with regional registra- Parts per tions. (1) Tolerances with regional reg- Commodity million istration as defined in 180.1(l) are es- tablished for the combined residues Animal feed, nongrass, group 18 ...... 1 .0 (free and bound) of the herbicide Barley, grain ...... 0 .10 Barley, hay ...... 0 .80 metolachlor [2-chloro-N-(2-ethyl-6- Barley, straw ...... 0 .80 methylphenyl)-N-(2-methoxy-1- Buckwheat, grain ...... 0.10 methylethyl)acetamide] and its me- Millet, forage ...... 0 .50 tabolites, determined as the deriva- Millet, grain ...... 0 .10 tives, 2-[2-ethyl-6- Millet, hay ...... 0 .80 Millet, straw ...... 0 .80 methylphenyl)amino]-1-propanol and 4- Oat, forage ...... 0 .50 (2-ethyl-6-methylphenyl)-2-hydroxy-5- Oat, grain ...... 0 .10 methyl-3-morpholinone, each expressed Oat, hay ...... 0.80 as the parent compound, in or on the Oat, straw ...... 0.80 Rice, grain ...... 0 .10 following raw agricultural commod- Rye, forage ...... 0 .50 ities: Rye, grain ...... 0.10 Rye, straw ...... 0 .80 Commodity Parts per Wheat, forage ...... 0 .50 million Wheat, grain ...... 0 .10 Wheat, hay ...... 0 .80 Pepper, nonbell ...... 0 .50 Wheat, straw ...... 0 .80

(2) Tolerances with regional registra- (2) Tolerances for are established for tion are established for residues of S- the indirect or inadvertent residues of metolachlor, including its metabolites S-metolachlor, including its metabo- and degradates, in or on the commod- lites and degradates, in or on the com- ities identified in the following table modities identified in the following below. Compliance with the tolerance table below. Compliance with the toler- levels specified in the following table ance levels specified in the following below is to be determined by measuring table below is to be determined by only the sum of free and bound S- measuring only the sum of free and metolachlor, S-2-chloro-N-(2-ethyl-6- bound S-metolachlor, S-2-chloro-N-(2- methylphenyl)-N-(2-methoxy-1- ethyl-6-methylphenyl)-N-(2-methoxy-1- methylethyl)acetamide, its R- methylethyl)acetamide, its R- enantiomer, and its metabolites, deter- enantiomer, and its metabolites, deter- mined as the derivatives, 2-(2-ethyl-6- mined as the derivatives, 2-(2-ethyl-6- methylphenyl)amino-1-propanol and 4- methylphenyl)amino-1-propanol and 4- (2-ethyl-6-methylphenyl)-2-hydroxy-5- (2-ethyl-6-methylphenyl)-2-hydroxy-5- methyl-3-morpholinone, calculated as methyl-3-morpholinone, calculated as the stoichiometric equivalent of S- the stoichiometric equivalent of S- metolachlor, in or on the commodity. metolachlor, in or on the commodity.

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(d) Indirect or inadvertent residues. Commodity Parts per million [Reserved] Animal feed, nongrass, group 18 ...... 1 .0 [47 FR 49845, Nov. 3, 1982, as amended at 48 Barley, grain ...... 0 .10 FR 12088, Mar. 23, 1983; 63 FR 57076, Oct. 26, Barley, hay ...... 0 .50 1998; 72 FR 41931, Aug. 1, 2007; 73 FR 54961, Barley, straw ...... 0 .50 Buckwheat, grain ...... 0.10 Sept. 24, 2008] Millet, forage ...... 0 .50 Millet, grain ...... 0 .10 § 180.371 Thiophanate-methyl; toler- Millet, hay ...... 0 .50 ances for residues. Millet, straw ...... 0 .50 Oat, forage ...... 0 .50 (a) General. Tolerances are estab- Oat, grain ...... 0 .10 lished for residues of thiophanate- Oat, hay ...... 0.50 methyl, dimethyl ((1,2-phenylene) bis Oat, straw ...... 0.50 (iminocarbonothioyl)) bis(carbamate), Rice, grain ...... 0 .10 Rye, forage ...... 0 .50 including its metabolites and Rye, grain ...... 0.10 degradates, in or on the commodities Rye, straw ...... 0 .50 in the following table. Compliance with Wheat, forage ...... 0 .50 the tolerance levels specified in this Wheat, grain ...... 0 .10 Wheat, hay ...... 0 .50 paragraph is to be determined by meas- Wheat, straw ...... 0 .50 uring only the sum of thiophanate- methyl, dimethyl ((1,2-phenylene) bis [73 FR 53740, Sept. 17, 2008, as amended at 74 (iminocarbonothioyl)) bis(carbamate), FR 48412, Sept. 23, 2009; 75 FR 56903, Sept. 17, and its metabolite, methyl 2- 2010; 77 FR 48906, Aug. 15, 2012; 77 FR 59127, benzimidazoyl carbamate (MBC), cal- Sept. 26, 2012; 79 FR 17441, Mar. 28, 2014] culated as the stoichiometric equiva- lent of thiophanate-methyl, in or on § 180.370 5-Ethoxy-3-(trichloromethyl)- the commodity. 1,2,4-thiadiazole; tolerances for resi- dues. Parts per Commodity million (a) General. Tolerances are estab- lished for residues of the fungicide 5- Almond ...... 0.1 Almond, hulls ...... 0 .5 ethoxy-3-(trichloromethyl)-1,2,4- Apple ...... 2.0 thiadiazole and its monoacid metabo- Apricot ...... 15 .0 lite 3-carboxy-5-ethoxy-1,2,4- Banana ...... 2.0 Bean, dry, seed ...... 0 .2 thiadiazole in or on the following raw Bean, snap, succulent ...... 2 .0 agricultural commodities: Beet, sugar, roots ...... 0 .2 Cherry, sweet ...... 20 .0 Commodity Parts per Cherry, tart ...... 20.0 million Grain, aspirated fractions ...... 12 Grape ...... 5 .0 Barley, grain ...... 0 .1 Onion, bulb ...... 0 .5 Barley, hay ...... 0 .1 Onion, green ...... 3 .0 Corn, field, forage ...... 0 .1 Peach ...... 3 .0 Corn, field, grain ...... 0 .1 Peanut ...... 0 .1 Corn, field, stover ...... 0 .1 Peanut, hay ...... 5.0 Corn, sweet, forage ...... 0 .1 Pear ...... 3 .0 Corn, sweet, stover ...... 0 .1 Pecan ...... 0 .1 Cotton, gin byproducts ...... 0 .1 Pistachio ...... 0.1 Cotton, undelinted seed ...... 0 .1 Plum ...... 0 .5 Peanut ...... 0 .1 Potato ...... 0 .1 Peanut, hay ...... 0.1 Soybean, hulls ...... 1 .5 Safflower, seed ...... 0 .1 Soybean, seed ...... 0 .2 Sorghum, grain, forage ...... 0.1 Strawberry ...... 7 .0 Sorghum, grain, grain ...... 0 .1 Vegetable, cucurbit, group 9 ...... 1.0 Tomato ...... 0.15 Wheat, forage ...... 1 .1 Vegetable, foliage of legume, group 7 ...... 0 .1 Wheat, grain ...... 0 .1 Wheat, hay ...... 0 .1 Vegetable, legume, group 6 ...... 0 .1 Wheat, straw ...... 0 .1 Wheat, forage ...... 0 .1 Wheat, grain ...... 0 .1 Wheat, straw ...... 0 .1 (b) Section 18 emergency exemptions. [Reserved] (b) Section 18 emergency exemptions. (c) Tolerances with regional registra- [Reserved] tions. A tolerance with a regional reg- (c) Tolerances with regional registra- istration is established for residues of tions. [Reserved] thiophanate-methyl, dimethyl ((1,2-

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phenylene) bis(iminocarbonothioyl)) Commodity Parts per bis(carbamate), including its metabo- million lites and degradates, in or on the com- Artichoke, globe ...... 6.0 modity in the following table. Compli- Cattle, fat ...... 0.05 Cattle, meat ...... 0 .05 ance with the tolerance level specified Cotton, undelinted seed ...... 0 .2 in this paragraph is to be determined Egg ...... 0 .05 by measuring only the sum of Goat, fat ...... 0 .05 Goat, meat ...... 0.05 thiophanate-methyl, dimethyl ((1,2- Hog, fat ...... 0 .05 phenylene) bis (iminocarbonothioyl)) Hog, meat ...... 0 .05 bis(carbamate), and its metabolite, Horse, fat ...... 0 .05 Horse, meat ...... 0 .05 methyl 2-benzimidazoyl carbamate Milk ...... 0.05 (MBC), calculated as the stoichio- Mushroom ...... 0 .2 metric equivalent of thiophanate- Poultry, fat ...... 0.05 Poultry, meat byproducts ...... 0.05 methyl, in or on the commodity. Poultry, meat ...... 0 .05 Sheep, fat ...... 0 .05 Commodity Parts per Sheep, meat ...... 0.05 million Soybean ...... 0.05 Soybean, hulls ...... 0 .5 Canola, seed ...... 0 .1 (2) Tolerances are established for res- (d) Indirect or inadvertent residues. idues of the insecticide diflubenzuron [Reserved] (N-[[(4-chlorophenyl)amino]carbonyl]- [75 FR 60244, Sept. 29, 2010] 2,6-difluorobenzamide), in or on the commodities in the table below. Com- § 180.372 2,6-Dimethyl-4- pliance with the tolerance levels speci- tridecylmorpholine; tolerances for fied below is to be determined by meas- residues. uring only the sum of diflubenzuron (N- (a) General. A tolerance is established [[(4-chlorophenyl)amino]carbonyl]-2,6- for residues of the fungicide 2,6-di- difluorobenzamide), 4- methyl-4-tridecylmorpholine in or on chlorophenylyurea and 4-chloroaniline, calculated as the stoichiometric equiv- the following food commodity: alent of diflubenzuron, in or on the Parts per commodity. Commodity million Commodity Parts per Banana 1 ...... 1.0 million

1 There are no U.S. registrations. Almond, hulls ...... 6 .0 Barley, grain ...... 0 .06 (b) Section 18 emergency exemptions. Barley, hay ...... 3 .0 [Reserved] Barley, straw ...... 1 .8 Brassica, leafy greens, subgroup 5B ...... 9 .0 (c) Tolerances with regional registra- Cattle, meat byproducts ...... 0.15 tions. [Reserved] Citrus, oil ...... 32 (d) Indirect or inadvertent residues. Fruit, citrus, group 10–10 ...... 3 .0 Fruit, stone, group 12, except cherry ...... 0 .07 [Reserved] Goat, meat byproducts ...... 0 .15 Grain, aspirated fractions ...... 11 [73 FR 54961, Sept. 24, 2008] Grass, forage, fodder, and hay, group 17 ...... 6 .0 Hog, meat byproducts ...... 0 .15 § 180.373 [Reserved] Horse, meat byproducts ...... 0 .15 Nut, tree, group 14 ...... 0 .06 § 180.377 Diflubenzuron; tolerances for Oat, forage ...... 7 .0 Oat, grain ...... 0 .06 residues. Oat, hay ...... 6.0 (a) General. (1) Tolerances are estab- Oat, straw ...... 3.5 Peanut ...... 0 .10 lished for residues of diflubenzuron, in- Peanut, hay ...... 55 cluding its metabolites and degradates, Peanut, refined oil ...... 0.20 in or on the commodities in the table Pear ...... 0 .50 Pepper ...... 1 .0 below. Compliance with the tolerance Pistachio ...... 0.06 levels specified below is to be deter- Rice, grain ...... 0 .02 mined by measuring only diflubenzuron Rice, straw ...... 0 .8 Sheep, meat byproducts ...... 0 .15 (N-[[(4-chlorophenyl)amino]carbonyl]- Turnip greens ...... 9 .0 2,6-difluorobenzamide). Wheat, forage ...... 7 .0

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Parts per Parts per Commodity million Commodity million

Wheat, grain ...... 0 .06 Alfalfa, forage ...... 20 Wheat, hay ...... 6 .0 Alfalfa, hay ...... 45 Wheat, straw ...... 3 .5 Almond ...... 0.05 Almond, hulls ...... 20 Artichoke, globe ...... 5.0 (b) Section 18 emergency exemptions. Asparagus ...... 2.0 Time-limited tolerances are estab- Avocado ...... 1 .0 Broccoli ...... 2 .0 lished for residues of the insecticide Brussels sprouts ...... 1 .0 diflubenzuron (N-[[(4- Cabbage ...... 6 .0 chlorophenyl)amino]carbonyl]-2,6- Cattle, fat ...... 1.5 Cattle, meat ...... 0 .10 difluorobenzamide) and its metabo- Cattle, meat byproducts ...... 0.10 lites, in connection with use of the pes- Cauliflower ...... 0 .5 ticide under section 18 emergency ex- Cherry, sweet ...... 4 .0 Cherry, tart ...... 4 .0 emptions granted by EPA. Compliance Corn, field, forage ...... 50 with the tolerance levels specified Corn, field, grain ...... 0 .05 below is to be determined by measuring Corn, field, stover ...... 30 only the sum of diflubenzuron (N-[[(4- Corn, pop, grain ...... 0.05 Corn, pop, stover ...... 30 chlorophenyl)amino]carbonyl]-2,6- Corn, sweet, forage ...... 50 difluorobenzamide), 4- Corn, sweet, kernel plus cob with husks re- chlorophenylyurea and 4-chloroaniline, moved ...... 0 .10 Corn, sweet, stover ...... 30 calculated as the stoichiometric equiv- Egg ...... 0 .10 alent of diflubenzuron, in or on the Eggplant ...... 0.50 commodity. The tolerances are speci- Fruit, pome, group 11 ...... 0.05 Garlic, bulb ...... 0.10 fied in the following table, and will ex- Grain, aspirated fractions ...... 0 .50 pire and are revoked on the dates speci- Goat, fat ...... 1 .5 fied. Goat, meat ...... 0.10 Goat, meat byproducts ...... 0 .10 Hazelnut ...... 0 .05 Expiration/ Hog, fat ...... 0 .05 Commodity Parts per revocation million date Hog, meat ...... 0 .05 Hog, meat byproducts ...... 0 .05 Alfalfa, forage ...... 6.0 12/31/17 Horse, fat ...... 1 .5 Alfalfa, hay ...... 6.0 12/31/17 Horse, meat ...... 0 .10 Horse, meat byproducts ...... 0 .10 Lemon ...... 0.8 12/31/10 Horseradish ...... 0.50 Kiwifruit ...... 2.0 (c) Tolerances with regional registra- Leaf petioles subgroup 4B ...... 5 .0 tions. [Reserved] Leafy greens subgroup 4A ...... 20 Lettuce, head ...... 20 (d) Indirect or inadvertent residues. Milk, fat (reflecting 0.88 ppm in whole milk) ...... 3 .0 [Reserved] Mushroom ...... 5 .0 Onion, bulb ...... 0 .10 [65 FR 33699, May 24, 2000] Peach ...... 1 .0 Pepper, bell ...... 0 .50 EDITORIAL NOTE: For FEDERAL REGISTER ci- Pistachio ...... 0.10 tations affecting § 180.377, see the List of CFR Potato ...... 0 .05 Sections Affected, which appears in the Poultry, fat ...... 0.15 Finding Aids section of the printed volume Poultry, meat ...... 0 .05 Poultry, meat byproducts ...... 0.05 and at www.fdsys.gov. Sheep, fat ...... 1 .5 Sheep, meat ...... 0.10 § 180.378 Permethrin; tolerances for Sheep, meat byproducts ...... 0 .10 residues. Soybean, seed ...... 0 .05 Spinach ...... 20 (a) General. Tolerances are estab- Tomato ...... 2.0 lished for the combined residues of the Vegetable, cucurbit, group 9 ...... 1.5 Walnut ...... 0 .05 insecticide cis- and trans-permethrin Watercress ...... 5 .0 isomers [cis-(3-phenoxyphenyl)methyl 3-(2,2-dichloroethenyl)-2,2- (b) Section 18 emergency exemptions. dimethylcyclopropane carboxylate] [Reserved] and [trans-(3-phenoxyphenyl)methyl 3- (c) Tolerances with regional registra- (2,2-dichloroethenyl)-2,2- tions. Tolerances with regional reg- dimethylcyclopropane carboxylate] in/ istration, as defined in § 180.1(l) are es- on the following food commodities: tablished for the combined residues of

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the insecticide cis- and trans- (c) Tolerances with regional registra- permethrin isomers [cis-(3- tions. [Reserved] phenoxyphenyl)methyl 3-(2,2- (d) Indirect or inadvertent residues. dichloroethenyl)-2,2- [Reserved] dimethylcyclopropane carboxylate] (e) Revoked tolerances subject to the and [trans-(3-phenoxyphenyl)methyl 3- channel of trade provisions. The fol- (2,2-dichloroethenyl)-2,2- lowing table lists commodities with dimethylcyclopropane carboxylate] in/ residues of vinclozolin resulting from on the following food commodities: lawful use are subject to the channels of trade provisions of section 408(l)(5) Parts per Commodity million of the FFDCA:

Collards ...... 15 Commodity Parts per Grass, forage ...... 15 million Grass, hay ...... 15 Papaya ...... 1 .0 Cucumber ...... 1 .0 Turnip, tops ...... 10 Fruit, stone, except plum, prune, fresh ...... 25.0 Turnip, roots ...... 0 .20 Pepper, bell ...... 3 .0 Strawberry ...... 10.0 (d) Indirect or inadvertent residues. [Reserved] [62 FR 38474, July 18, 1997, as amended at 63 FR 7308, Feb. 13, 1998; 65 FR 44468, July 18, [72 FR 52019, Sept. 12, 2007] 2000; 67 FR 40189, June 12, 2002; 68 FR 56189, Sept. 30, 2003; 68 FR 69323, Dec. 12, 2003; 70 FR § 180.380 Vinclozolin; tolerances for 55268, Sept. 21, 2005] residues. (a) General. Tolerances are estab- § 180.381 Oxyfluorfen; tolerances for lished for the combined residues of the residues. fungicide vinclozolin (3-(3,5- (a) General. Tolerances are estab- dichlorophenyl)-5-ethenyl-5-methyl-2,4- lished for residues of the herbicide oxazolidinedione) and its metabolites oxyfluorfen [2-chloro-1-(3-ethoxy-4- containing the 3,5-dichloroaniline moi- nitrophenoxy)-4- ety in or on the food commodities in (trifluoromethyl)benzene] in or on the the table below. There are no U.S. reg- following food commodities: istrations for grape (wine) as of July Parts per 30, 1997. Commodity million

Parts per Expiration/ Almond, hulls ...... 0 .1 Commodity Revocation Artichoke, globe ...... 0.05 million Date Avocado ...... 0 .05 Bean, succulent ...... 2.0 11/30/05 Banana ...... 0.05 Canola, seed ...... 1.0 11/30/08 Broccoli ...... 0 .05 Cattle, fat ...... 0.05 11/30/08 Cabbage ...... 0 .05 Cattle, meat ...... 0.05 11/30/08 Cacao bean, dried bean ...... 0 .05 Cattle, meat byproducts ...... 0.05 11/30/08 Cattle, fat ...... 0.01 Egg ...... 0.05 11/30/08 Cattle, meat ...... 0 .01 Goat, fat ...... 0.05 11/30/08 Cattle, meat byproducts ...... 0.01 Goat, meat ...... 0.05 11/30/08 Cauliflower ...... 0 .05 Goat, meat byproducts ...... 0.05 11/30/08 Coffee, bean, green ...... 0 .05 Grape, wine ...... 6. 0 None Corn, field, grain ...... 0 .05 Hog, fat ...... 0.05 11/30/08 Cotton, undelinted seed ...... 0 .05 Hog, meat ...... 0.05 11/30/08 Date, dried fruit ...... 0 .05 Hog, meat byproducts ...... 0.05 11/30/08 Egg ...... 0 .03 Horse, fat ...... 0.05 11/30/08 Feijoa ...... 0 .05 Horse, meat ...... 0.05 11/30/08 Fig ...... 0 .05 Horse, meat byproducts ...... 0.05 11/30/08 Fruit, pome, group 11 ...... 0.05 Lettuce, head ...... 10.0 11/30/05 Fruit, stone, group 12 ...... 0 .05 Lettuce, leaf ...... 10.0 11/30/05 Goat, fat ...... 0 .01 Milk ...... 0.05 11/30/08 Goat, meat ...... 0.01 Poultry, fat ...... 0.1 11/30/08 Goat, meat byproducts ...... 0 .01 Poultry, meat ...... 0.1 11/30/08 Grape ...... 0 .05 Poultry, meat byproducts ...... 0.1 11/30/08 Hog, fat ...... 0 .01 Sheep, fat ...... 0.05 11/30/08 Hog, meat ...... 0 .01 Sheep, meat ...... 0.05 11/30/08 Hog, meat byproducts ...... 0 .01 Sheep, meat byproducts ...... 0.05 11/30/08 Horse, fat ...... 0 .01 Horse, meat ...... 0 .01 Horse, meat byproducts ...... 0 .01 (b) Section 18 emergency exemptions. Horseradish ...... 0.05 [Reserved] Kiwifruit ...... 0.05

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Parts per Parts per Commodity million Commodity million

Milk ...... 0.01 Peanut ...... 0 .1 Nut, tree, group 14 ...... 0 .05 Rice, grain ...... 0 .1 Olive ...... 0 .05 Rice, straw ...... 0 .2 Onion, bulb ...... 0 .05 Soybean, seed ...... 0 .1 Peppermint, tops ...... 0 .05 Strawberry ...... 0 .05 Persimmon ...... 0 .05 Pistachio ...... 0.05 (b) Section 18 emergency exemptions. Pomegranate ...... 0 .05 [Reserved] Poultry, fat ...... 0.2 Poultry, meat ...... 0 .01 (c) Tolerances with regional restric- Poultry, meat byproducts ...... 0.01 tions. [Reserved] Sheep, fat ...... 0 .01 (d) Indirect or inadvertent residues. Sheep, meat ...... 0.01 [Reserved] Sheep, meat byproducts ...... 0 .01 Soybean ...... 0.05 [45 FR 24877, Apr. 11, 1980, as amended at 46 Spearmint, tops ...... 0 .05 FR 61272, Dec. 16, 1981; 47 FR 39490, Sept. 8, 1982; 61 FR 30165, June 14, 1996; 62 FR 39974, (b) Section 18 emergency exemptions. July 25, 1997; 67 FR 35048, May 17, 2002; 69 FR [Reserved] 6567, Feb. 11, 2004; 71 FR 54434, Sept. 15, 2006] (c) Tolerances with regional registra- § 180.384 Mepiquat (N,N-dimethylpip- tions. Tolerances with regional reg- eridinium); tolerances for residues. istration are established for residues of the herbicide oxyfluorfen [2-chloro-1-(3- (a) General. (1) Tolerances are estab- ethoxy-4-nitrophenoxy)-4- lished for residues of the plant growth (trifluoromethyl)benzene] in or on the regulator mepiquat (N,N- following food commodities: dimethylpiperidinium) in or on the fol- lowing commodities: Commodity Parts per million Parts per Commodity million Blackberry ...... 0 .05 Chickpea, seed ...... 0 .05 Cattle, meat byproducts ...... 0.1 Grass, forage ...... 0 .05 Cotton, gin byproducts ...... 6 .0 Grass, hay ...... 0 .05 Cotton, undelinted seed ...... 2 .0 Grass, seed screenings ...... 0 .05 Goat, meat byproducts ...... 0 .1 Guava ...... 0 .05 Hog, meat byproducts ...... 0 .1 Horse, meat byproducts ...... 0 .1 Papaya ...... 0 .05 Sheep, meat byproducts ...... 0 .1 Raspberry ...... 0 .05 Taro, corm ...... 0 .05 Taro, leaves ...... 0 .05 (2) Tolerances are established for res- idues of the plant growth regulator (d) Indirect or inadvertent residues. mepiquat chloride (N,N- [Reserved] dimethylpiperidinium chloride) in or on the following commodities: [45 FR 85022, Dec. 24, 1980] Parts per EDITORIAL NOTE: For FEDERAL REGISTER ci- Commodity million tations affecting § 180.381, see the List of CFR Sections Affected, which appears in the Cattle, fat ...... 0.1 Finding Aids section of the printed volume Cattle, meat ...... 0 .1 and at www.fdsys.gov. Goat, fat ...... 0 .1 Goat, meat ...... 0.1 § 180.383 Sodium salt of acifluorfen; Grape ...... 1 .0 Grape, raisin ...... 5 .0 tolerances for residues. Hog, fat ...... 0 .1 (a) General. Tolerances are estab- Hog, meat ...... 0 .1 lished for combined residues of the her- Horse, fat ...... 0 .1 Horse, meat ...... 0 .1 bicide sodium salt of acifluorfen, so- Sheep, fat ...... 0 .1 dium 5-[2-chloro-4- Sheep, meat ...... 0.1 (trifluoromethyl)phenoxy]-2- nitrobenzoate, and its metabolites (the (b) Section 18 emergency exemptions. corresponding acid, methyl ester, and [Reserved] amino analogues) in or on the fol- (c) Tolerances with regional registra- lowing raw agricultural commodities: tions. [Reserved]

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(d) Indirect or inadvertent residues. tebuthiuron (N-(5-(1,1-dimethylethyl)- [Reserved] 1,3,4-thiadiazol-2-yl)-N,N’- dimethylurea) and its metabolites N-(5- [67 FR 3118, Jan. 23, 2002] (1,1-dimethylethyl)-1,3,4-thiadiazol-2- § 180.385 Diclofop-methyl; tolerances yl)-N-methylurea, N-(5-(1,1- for residues. dimethylethyl)-1,3,4-thiadiazol-2- (a) General. Tolerances are estab- yl)urea, 2-dimethylethyl-5-amino-1,3,4- lished for the combined residues of the thiadiazole, and N-(5-(1,1- herbicide diclofop-methyl (methyl 2-[4- dimethylethyl)-1,3,4-thiadiazol-2-yl)-N’- (2,4- hydroxymethyl-N-methylurea in or on dichlorophenoxy)phenoxy]propanoate) the following raw agricultural com- and its metabolites, 2-[4-(2,4- modities: dichlorophenoxy)phenoxy]propanoic Parts per acid and 2-[4-(2,4-dichloro-5- Commodity million hydroxyphenoxy)phenoxy]propanoic Cattle, fat ...... 1.0 acid, in or on the following raw agri- Cattle, meat ...... 1 .0 cultural commodities: Cattle, meat byproducts ...... 5.0 Goat, fat ...... 1 .0 Parts per Goat, meat ...... 1.0 Commodity million Goat, meat byproducts ...... 5 .0 Horse, fat ...... 1 .0 Barley, grain ...... 0 .1 Horse, meat ...... 1 .0 Barley, straw ...... 0 .1 Horse, meat byproducts ...... 5 .0 Wheat, grain ...... 0 .1 Sheep, fat ...... 1 .0 Wheat, straw ...... 0 .1 Sheep, meat ...... 1.0 Sheep, meat byproducts ...... 5 .0 (b) Section 18 emergency exemptions. [Reserved] (3) A tolerance is established for the (c) Tolerances with regional registra- combined residues of the herbicide tions. [Reserved] tebuthiuron (N-(5-(1,1-dimethylethyl)- (d) Indirect or inadvertent residues. 1,3,4-thiadiazol-2-yl)-N,N’- [Reserved] dimethylurea) and its metabolites N-(5- (1,1-dimethylethyl)-1,3,4-thiadiazol-2- [45 FR 23425, Apr. 7, 1980, as amended at 50 FR 20211, May 15, 1985; 51 FR 3599, Jan. 29, yl)-N-methylurea, N-(5-(2-hydroxy-1,1- 1986; 51 FR 19176, May 28, 1986; 63 FR 57077, dimethylethyl)-1,3,4-thiadiazol-2-yl)-N- Oct. 26, 1998; 72 FR 41931, Aug. 1, 2007] methylurea, N-(5-(1,1-dimethylethyl)- 1,3,4-thiadiazol-2-yl)urea, N-(5-(1,1- §§ 180.388–180.389 [Reserved] dimethylethyl)-1,3,4-thiadiazol-2-yl)-N’- hydroxymethyl-N-methylurea, and N- § 180.390 Tebuthiuron; tolerances for (5-(2-hydroxy-1,1-dimethylethyl)-1,3,4- residues. thiadiazol-2-yl)-N’-hydroxymethyl-N- (a) General. (1) Tolerances are estab- methylurea in or on the following raw lished for the combined residues of the agricultural commodities: herbicide tebuthiuron (N-(5-(1,1- dimethylethyl)-1,3,4-thiadiazol-2-yl)- Commodity Parts per N,N’-dimethylurea) and its metabolites million N-(5-(2-hydroxy-1,1-dimethylethyl)- Milk ...... 0.8 1,3,4-thiadiazol-2-yl)-N,N’- dimethylurea, N-(5-(1,1-dimethylethyl)- (b) Section 18 emergency exemptions. 1,3,4-thiadiazol-2-yl)-N-methylurea, and [Reserved] N-(5-(1,1-dimethylethyl)-1,3,4- (c) Tolerances with regional registra- thiadiazol-2-yl)-N’-hydroxymethyl-N- tions. [Reserved] methylurea in or on the following raw (d) Indirect or inadvertent residues. agricultural commodities: [Reserved]

Parts per [72 FR 53461, Sept. 19, 2007] Commodity million § 180.395 Hydramethylnon; tolerances Grass, forage ...... 10 .0 for residues. Grass, hay ...... 10 .0 (a) General. Tolerances are estab- (2) Tolerances are established for the lished for residues of the insecticide combined residues of the herbicide tetrahydro-5,5-dimethyl-2(1H)-

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pyrimidinone(3-(4- Commodity Parts per (trifluoromethyl)phenyl)-1-(2-(4- million (trifluoromethyl)phenyl)ethenyl)-2- Alfalfa, seed ...... 2 .0 propenylidene)hydrazone in or on the Blueberry ...... 0 .6 following raw agricultural commod- Grass, forage ...... 250 Grass, hay ...... 230 ities: Pineapple ...... 0.6 Sugarcane, cane ...... 0.6 Parts per Sugarcane, molasses ...... 4 .0 Commodity million

Grass, forage ...... 2 .0 (2) Tolerances are established for res- Grass, hay ...... 2 .0 idues of the herbicide hexazinone, 3- Pineapple ...... 0.05 cyclohexyl-6-(dimethylamino)-1-meth- (b) Section 18 emergency exemptions. yl-1,3,5-triazine-2,4-(1H, 3H)-dione, in- [Reserved] cluding its metabolites and degradates, (c) Tolerances with regional registra- in or on the commodities in the fol- tions. [Reserved] lowing table. Compliance with the tol- (d) Indirect or inadvertent residues. erance levels specified in this para- [Reserved] graph is to be determined by measuring only the sum of hexazinone, 3- [45 FR 55198, Aug. 19, 1980, as amended at 63 cyclohexyl-6-(dimethylamino)-1-meth- FR 10543, Mar. 4, 1998; 63 FR 65073, Nov. 25, yl-1,3,5-triazine-2,4-(1H, 3H)-dione, and 1998; 66 FR 28672, May 24, 2001; 68 FR 37764, June 25, 2003; 68 FR 48312, Aug. 13, 2003; 72 FR its animal tissue metabolites: metabo- 41931, Aug. 1, 2007] lite B, 3-cyclohexyl-6-(methylamino)-1- methyl-1,3,5-triazine-2,4-(1H, 3H)-dione, § 180.396 Hexazinone; tolerances for and metabolite F, 3-cyclohexyl-6- residues. amino-1-methyl-1,3,5-triazine-2,4-(1H, (a) General. (1) Tolerances are estab- 3H)-dione, calculated as the stoichio- lished for residues of the herbicide metric equivalent of hexazinone, in or hexazinone, 3-cyclohexyl-6- on the commodity. (dimethylamino)-1-methyl-1,3,5-tri- Parts per azine-2,4-(1H, 3H)-dione, including its Commodity million metabolites and degradates, in or on Cattle, fat ...... 0.1 the commodities in the following table. Cattle, meat ...... 0 .5 Compliance with the tolerance levels Cattle, meat byproducts ...... 4.0 specified in this paragraph is to be de- Goat, fat ...... 0 .1 termined by measuring only the sum of Goat, meat ...... 0.5 Goat, meat byproducts ...... 4 .0 hexazinone, 3-cyclohexyl-6- Hog, fat ...... 0 .1 (dimethylamino)-1-methyl-1,3,5-tri- Hog, meat ...... 0 .5 azine-2,4-(1H, 3H)-dione, and its plant Hog, meat byproducts ...... 4 .0 Horse, fat ...... 0 .1 metabolites: metabolite A, 3-(4- Horse, meat ...... 0 .5 hydroxycyclohexyl)-6- Horse, meat byproducts ...... 4 .0 (dimethylamino)-1-methyl-1,3,5-tri- Sheep, fat ...... 0 .1 azine-2,4-(1H, 3H)-dione, metabolite B, Sheep, meat ...... 0.5 Sheep, meat byproducts ...... 4 .0 3-cyclohexyl-6-(methylamino)-1-meth- yl-1,3,5-triazine-2,4-(1H, 3H)-dione, me- (3) A tolerance is established for resi- tabolite C, 3-(4-hydroxycyclohexyl)-6- dues of the herbicide hexazinone, 3- (methylamino)-1-methyl-1,3,5-triazine- cyclohexyl-6-(dimethylamino)-1-meth- 2,4-(1H, 3H)-dione, metabolite D, 3- yl-1,3,5-triazine-2,4-(1H, 3H)-dione, in- cyclohexyl-1-methyl-1,3,5-triazine-2,4,6- cluding its metabolites and degradates, (1H, 3H, 5H)-trione, and metabolite E, in or on the commodity in the fol- 3-(4-hydroxycyclohexyl)-1-methyl-1,3,5- lowing table. Compliance with the tol- triazine-2,4,6-(1H, 3H, 5H)-trione, cal- erance level specified in this paragraph culated as the stoichiometric equiva- is to be determined by measuring only lent of hexazinone, in or on the com- the sum of hexazinone, 3-cyclohexyl-6- modity. (dimethylamino)-1-methyl-1,3,5-tri- Parts per azine-2,4-(1H, 3H)-dione, and its me- Commodity million tabolites: metabolite B, 3-cyclohexyl-6- Alfalfa, forage ...... 2.0 (methylamino)-1-methyl-1,3,5-triazine- Alfalfa, hay ...... 4.0 2,4-(1H, 3H)-dione, metabolite C, 3-(4-

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hydroxycyclohexyl)-6-(methylamino)-1- Commodity Parts per methyl-1,3,5-triazine-2,4-(1H, 3H)-dione, million metabolite C-2, 3-(3- Onion, bulb ...... 0 .5 hydroxycyclohexyl)-6-(methylamino)-1- Peach, postharvest ...... 20.0 methyl-1,3,5-triazine-2,4-(1H, 3H)-dione, Peanut ...... 0 .5 and metabolite F, 3-cyclohexyl-6- Peanut, hay ...... 150.0 Plum, postharvest ...... 20 .0 amino-1-methyl-1,3,5-triazine-2,4-(1H, Plum, prune ...... 20.0 3H)-dione, calculated as the stoichio- Potato ...... 0 .5 metric equivalent of hexazinone, in or Raspberry ...... 15 .0 on the commodity. Rice, bran ...... 30.0 Rice, grain ...... 10 .0 Rice, hulls ...... 50 .0 Parts per Commodity million Rice, straw ...... 20 .0 Strawberry ...... 15.0 Milk ...... 11 (2) Tolerances are established for the (b) Section 18 emergency exemptions. combined residues of iprodione [3-(3,5- [Reserved] dichlorophenyl)-N-(1-methylethyl)-2,4- (c) Tolerances with regional registra- dioxo-1-imidazolidinecarboxamide], its tions. [Reserved] isomer [3-(1-methylethyl)-N-(3,5- (d) Indirect or inadvertent residues. dichlorophenyl)-2,4-dioxo-1- [Reserved] imidazolidinecarboxamide, and its me- [65 FR 33713, May 24, 2000, as amended at 71 tabolites [3-(3,5-dichlorophenyl)-2,4- FR 56399, Sept. 27, 2006; 75 FR 60244, Sept. 29, dioxo-1-imidazolidine-carboxamide] 2010] and [N-(3,5-dichloro-4-hydroxyphenyl)- ureido-carboxamide], all expressed as § 180.399 Iprodione; tolerances for res- iprodione equivalents in or on the fol- idues. lowing food commodities of animal ori- (a) General. (1) Tolerances are estab- gin: lished for the combined residues of the Parts per fungicide iprodione [3-(3,5- Commodity million dichlorophenyl)-N-(1-methylethyl)-2,4- dioxo-1-imidazolidinecarboxamide], its Cattle, fat ...... 0.5 isomer 3-(1-methylethyl)-N-(3,5- Cattle, kidney ...... 3 .0 Cattle, liver ...... 3 .0 dichlorophenyl)-2,4-dioxo-1- Cattle, meat ...... 0 .5 imidazolidinecarboxamide, and its me- Cattle, meat byproducts, except kidney and liver 0.5 tabolite 3-(3,5-dichlorophenyl)-2,4- Egg ...... 1 .5 dioxo-1-imidazolidine-carboxamide in Goat, fat ...... 0 .5 Goat, kidney ...... 3 .0 or on the following food commodities: Goat, liver ...... 3.0 Goat, meat ...... 0.5 Parts per Goat, meat byproducts, except kidney and liver 0 .5 Commodity million Hog, fat ...... 0 .5 Almond, hulls ...... 2 .0 Hog, kidney ...... 3.0 Almond ...... 0.3 Hog, liver ...... 3 .0 Apricot ...... 20 .0 Hog, meat ...... 0 .5 Bean, dry, seed ...... 2 .0 Hog, meat byproducts, except kidney and liver .. 0 .5 Bean, forage ...... 90 .0 Horse, fat ...... 0 .5 Bean, succulent ...... 2 .0 Horse, kidney ...... 3 .0 Blueberry ...... 15 .0 Horse, liver ...... 3 .0 Boysenberry ...... 15 .0 Horse, meat ...... 0 .5 Broccoli ...... 25 .0 Horse, meat byproducts, except kidney and liver 0 .5 Caneberry subgroup 13A ...... 25 .0 Milk ...... 0.5 Carrot, roots ...... 5.0 Poultry, fat ...... 3.5 Cherry, sweet, postharvest ...... 20 .0 Poultry, liver ...... 5 .0 Cherry, tart ...... 20.0 Poultry, meat ...... 1 .0 Cotton, undelinted seed ...... 0 .10 Poultry, meat byproducts, except liver ...... 1 .0 Cowpea, hay ...... 90 .0 Sheep, fat ...... 0 .5 Currant ...... 15.0 Sheep, kidney ...... 3.0 Garlic ...... 0 .1 Sheep, liver ...... 3.0 Ginseng ...... 2 .0 Sheep, meat ...... 0.5 Ginseng, dried root ...... 4 .0 Sheep, meat byproducts, except kidney and Grape ...... 60 .0 liver ...... 0 .5 Grape, raisin ...... 300 Kiwifruit ...... 10.0 Lettuce ...... 25.0 (b) Section 18 emergency exemptions. Nectarine, postharvest ...... 20.0 [Reserved]

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(c) Tolerances with regional registra- (b) Section 18 emergency exemptions. tions. Tolerances with regional reg- [Reserved] istration, as defined in § 180.1(l), are es- (c) Tolerances with regional registra- tablished for the combined residues of tions. Tolerances with regional reg- the fungicide iprodione [3-(3,5- istration, as defined in § 180.1(l), are es- dichlorophenyl)-N-(1-methylethyl)-2,4- tablished for residues of the herbicide dioxo-1-imidazolidinecarboxamide], its thiobencarb (S-[(4-chloro- isomer [3-(1-methylethyl)-N-(3,5- phenyl)methyl]diethylcarbamothioate) dichlorophenyl)-2,4-dioxo-1- and its chlorobenzyl and chlorophenyl imidazolidinecarboxamide], and its me- moiety-containing metabolites in or on tabolite [3-(3,5-dichlorophenyl)-2,4- the following raw agricultural com- dioxo-1-imidazolidinecarboxamide] in modities: or on the following food commodity: Parts per Commodity million Parts per Commodity million Celery ...... 0 .2 Mustard greens ...... 15.0 Endive ...... 0.2 Lettuce ...... 0.2 (d) Indirect or inadvertent residues. (d) Indirect or inadvertent residues. [Reserved] [Reserved] [48 FR 40385, Sept. 7, 1983] [47 FR 6833, Feb. 17, 1982, as amended at 56 EDITORIAL NOTE: For FEDERAL REGISTER ci- FR 2440, Jan. 23, 1991; 76 FR 34885, June 15, tations affecting § 180.399, see the List of CFR 2011] Sections Affected, which appears in the Finding Aids section of the printed volume § 180.403 Thidiazuron; tolerances for and at www.fdsys.gov. residues. (a) General. Tolerances are estab- § 180.401 Thiobencarb; tolerances for lished for the combined residues of the residues. defoliant thidiazuron (N-phenyl-N-1,2,3- (a) General. Tolerances are estab- thiadiazol-5-ylurea) and its aniline con- lished for the combined residues of the taining metabolites in or on the fol- herbicide thiobencarb (S-[(4- lowing food commodities: chlorophenyl)methyl]diethyl- carbamothioate) and its chlorobenzyl Parts per Commodity million and chlorophenyl moiety-containing metabolites in or on the following raw Cattle, fat ...... 0.4 agricultural commodities: Cattle, meat ...... 0 .4 Cattle, meat byproducts ...... 0.4 Cotton, gin byproducts ...... 24 .0 Part per Commodity million Cotton, undelinted seed ...... 0 .3 Goat, fat ...... 0 .4 Cattle, fat ...... 0.2 Goat, meat ...... 0.4 Cattle, meat byproducts ...... 0.2 Goat, meat byproducts ...... 0 .4 Cattle, meat ...... 0 .2 Hog, fat ...... 0 .4 Egg ...... 0 .2 Hog, meat ...... 0 .4 Hog, meat byproducts ...... 0 .4 Goat, fat ...... 0 .2 Horse, fat ...... 0 .4 Goat, meat byproducts ...... 0 .2 Horse, meat ...... 0 .4 Goat, meat ...... 0.2 Horse, meat byproducts ...... 0 .4 Hog, fat ...... 0 .2 Milk ...... 0.05 Hog, meat byproducts ...... 0 .2 Sheep, fat ...... 0 .4 Hog, meat ...... 0 .2 Sheep, meat ...... 0.4 Horse, fat ...... 0 .2 Sheep, meat byproducts ...... 0 .4 Horse, meat byproducts ...... 0 .2 Horse, meat ...... 0 .2 Milk ...... 0.05 (b) Section 18 emergency exemptions. Poultry, fat ...... 0.2 [Reserved] Poultry, meat byproducts ...... 0.2 (c) Tolerances with regional registra- Poultry, meat ...... 0 .2 tions. [Reserved] Rice, grain ...... 0 .2 (d) Indirect or inadvertent residues. Rice, straw ...... 1 .0 Sheep, fat ...... 0 .2 [Reserved] Sheep, meat byproducts ...... 0 .2 [65 FR 33700, May 24, 2000, as amended at 72 Sheep, meat ...... 0.2 FR 53462, Sept. 19, 2007]

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§ 180.404 Profenofos; tolerances for yl)aminocarbonyl] residues. benzenesulfonamide) in or on the fol- (a) General. Tolerances are estab- lowing raw agricultural commodities. lished for residues of the insecticide Parts per profenofos (O-(4-bromo-2- Commodity million chlorophenyl)-O-ethyl-S-propyl Cattle, fat ...... 0.3 phosphorothioate) in or on the fol- Cattle, meat ...... 0 .3 lowing food commodities: Cattle, meat byproducts ...... 0.3 Goat, fat ...... 0 .3 Parts per Goat, meat ...... 0.3 Commodity million Goat, meat byproducts ...... 0 .3 Grass, forage ...... 11 .0 Cattle, fat ...... 0.05 Grass, hay ...... 19 .0 Cattle, meat ...... 0 .05 Hog, fat ...... 0 .3 Cattle, meat byproducts ...... 0.05 Hog, meat ...... 0 .3 Cotton, gin byproducts ...... 55 .0 Hog, meat byproducts ...... 0 .3 Cotton, undelinted seed ...... 2 .0 Horse, fat ...... 0 .3 Goat, fat ...... 0 .05 Horse, meat ...... 0 .3 Goat, meat ...... 0.05 Horse, meat byproducts ...... 0 .3 Goat, meat byproducts ...... 0 .05 Milk ...... 0.1 Horse, fat ...... 0 .05 Sheep, fat ...... 0 .3 Horse, meat ...... 0 .05 Sheep, meat ...... 0.3 Horse, meat byproducts ...... 0 .05 Sheep, meat byproducts ...... 0 .3 Milk ...... 0.01 Sheep, fat ...... 0 .05 (b) Section 18 emergency exemptions. Sheep, meat ...... 0.05 [Reserved] Sheep, meat byproducts ...... 0 .05 (c) Tolerances with regional registra- (b) Section 18 emergency exemptions. tions. [Reserved] [Reserved] (d) Indirect or inadvertent residues. (c) Tolerances with regional registra- [Reserved] tions. [Reserved] [67 FR 52873, Aug. 14, 2002] (d) Indirect or inadvertent residues. [Reserved] § 180.407 Thiodicarb; tolerances for residues. [65 FR 33700, May 24, 2000, as amended at 66 FR 50833, Oct. 5, 2001; 67 FR 49617, July 31, (a) General. Tolerances are estab- 2002; 72 FR 54579, Sept. 26, 2007] lished for the combined residues of the insecticide thiodicarb (dimethyl N,N′- § 180.405 Chlorsulfuron; tolerances for [thiobis[[(methylimino)carbonyloxy]] residues. bis[ethanimidothioate]) and its me- (a) General. (1) Tolerances are estab- tabolite methomyl (S-methyl N- lished for the combined residues of [(methylcarbamoyl) chlorsulfuron (2-chloro-N-[(4-methoxy- oxy]thioacetimidate) in or on the fol- 6-methyl-1,3,5-triazin-2- lowing food commodities or groups. yl)aminocarbonyl]benzenesulfonamide) The time-limited tolerances expire and and its metabolite, 2-chloro-5-hydroxy- are revoked on the dates listed in the N-[(4-methoxy-6-methyl-1,3,5-triazin-2- following table: yl)aminocarbonyl] benzenesulfonamide Expiration/ in or on the following raw agricultural Commodity Parts per revocation commodities: million date

Parts per Broccoli ...... 7.0 None Commodity million Cabbage ...... 7.0 None Cauliflower ...... 7.0 None Barley, grain ...... 0 .1 Corn, sweet, kernel plus cob with Barley, straw ...... 0 .5 husks removed ...... 2.0 None Oat, forage ...... 20 .0 Cotton, undelinted seed ...... 0.4 None Oat, grain ...... 0 .1 Soybean, hulls ...... 0.8 None Oat, straw ...... 0.5 Soybean ...... 0.2 None Wheat, forage ...... 20.0 Vegetable, leafy, except brassica, Wheat, grain ...... 0 .1 group 4 ...... 35 None Wheat, straw ...... 0 .5 (b) Section 18 emergency exemptions. (2) Tolerances are established for res- [Reserved] idues of chlorsulfuron (2-chloro-N-[(4- (c) Tolerances with regional registra- methoxy-6-methyl-1,3,5-triazin-2- tions. [Reserved]

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(d) Indirect or inadvertent residues. Commodity Parts per [Reserved] million [62 FR 44595, Aug. 22, 1997, as amended at 75 Hog, kidney ...... 0.4 FR 60245, Sept. 29, 2010] Hog, liver ...... 0 .4 Hog, meat ...... 0 .05 Hog, meat byproducts, except kidney and liver .. 0 .05 § 180.408 Metalaxyl; tolerances for res- Hop, dried cones ...... 20 idues. Hop, vines ...... 2 .0 Horse, fat ...... 0 .4 (a) General. Tolerances are estab- Horse, kidney ...... 0 .4 lished for the combined residues of the Horse, liver ...... 0 .4 fungicide metalaxyl [N-(2,6- Horse, meat ...... 0 .05 dmethylphyenyl)-N-(methoxyacetyl) Horse, meat byproducts, except kidney and liver 0 .05 Lettuce, head ...... 5.0 methylester] and its metabo- Milk ...... 0.02 lites containing the 2,6- Mustard greens ...... 5.0 dimethylaniline moiety, and N-(2-hy- Onion, bulb ...... 3 .0 Onion, green ...... 10.0 droxy methyl-6-methylphenyl)-N- Peanut ...... 0 .2 (methoxyacetyl)-alanine methyl ester, Peanut, hay ...... 20.0 each expressed as metalaxyl equiva- Peanut, meal ...... 1 .0 lents, in or on the following food com- Peanut, hulls ...... 2 .0 Pineapple ...... 0.1 modities: Pineapple, fodder ...... 0 .1 Pineapple, forage ...... 0 .1 Commodity Parts per Plum, prune, dried ...... 4.0 million Potato, chips ...... 4 .0 Potato, granules, flakes ...... 4.0 Alfalfa, forage ...... 6.0 Potato, processed potato waste ...... 4 .0 Alfalfa, hay ...... 20.0 Potato, wet peel ...... 4 .0 Almond ...... 0.5 Poultry, fat ...... 0.4 Almond, hulls ...... 10 .0 Poultry, kidney ...... 0 .4 Apple ...... 0.2 Poultry, liver ...... 0 .4 Apple, wet pomace ...... 0 .4 Poultry, meat ...... 0 .05 Apricot, dried ...... 4 .0 Poultry, meat byproducts, except kidney and Asparagus ...... 7.0 liver ...... 0 .05 Avocado ...... 4 .0 Potato ...... 0 .5 Beet, garden, roots ...... 0 .1 Beet, garden, tops ...... 0 .1 Raspberry ...... 0 .5 Beet, sugar ...... 0 .1 Sheep, fat ...... 0 .4 Beet, sugar, molasses ...... 1 .0 Sheep, kidney ...... 0.4 Beet, sugar, roots ...... 0 .5 Sheep, liver ...... 0.4 Beet, sugar, tops ...... 10.0 Sheep, meat ...... 0.05 Blueberry ...... 2 .0 Sheep, meat byproducts, except kidney and Broccoli ...... 2 .0 liver ...... 0 .05 Brussels sprouts ...... 2 .0 Soybean, hulls ...... 2 .0 Cabbage ...... 1 .0 Soybean, meal ...... 2.0 Cattle, fat ...... 0.4 Soybean, seed ...... 1 .0 Cattle, kidney ...... 0 .4 Spinach ...... 10 .0 Cattle, liver ...... 0 .4 Strawberry ...... 10.0 Cattle, meat ...... 0 .05 Sunflower, seed ...... 0.1 Cattle, meat byproducts, except kidney and liver 0.05 Sunflower, forage ...... 0.1 Cauliflower ...... 1 .0 Tomato, paste ...... 3 .0 Citrus, oil ...... 7.0 Tomato, puree ...... 3 .0 Citrus, dried pulp ...... 7 .0 Vegetable, brassica, leafy, group 5, except broc- Clover, forage ...... 1.0 coli, cabbage, cauliflower, brussels sprouts, Clover, hay ...... 2.5 and mustard greens ...... 0 .1 Cotton, undelinted seed ...... 0 .1 Vegetable, cucurbit, group 9 ...... 1.0 Cranberry ...... 4 .0 Vegetable, foilage of legume, group 7 ...... 8 .0 Egg ...... 0 .05 Vegetable, fruiting, group 8 ...... 1.0 Fruit, citrus ...... 1 .0 Vegetable, leafy, except brassica, group 4, ex- Fruit, stone, group 12 ...... 1 .0 cept spinach ...... 5 .0 Ginseng ...... 3 .0 Vegetable, leaves of root and tuber, group 2 ..... 15 .0 Goat, fat ...... 0 .4 Vegetable, legume, cannery waste ...... 5 .0 Goat, kidney ...... 0 .4 Vegetable, legume, group 6 ...... 0 .2 Goat, liver ...... 0.4 Vegetable, root and tuber, group 1 ...... 0 .5 Goat, meat ...... 0.05 Walnut ...... 0 .5 Goat, meat byproducts, except kidney and liver 0 .05 Grain, cereal, group 15, except barley, oat and (b) Section 18 emergency exemptions. wheat ...... 0.1 Grain, crop ...... 0 .1 [Reserved] Grape ...... 2 .0 (c) Tolerances with regional registra- Grape, raisin ...... 6 .0 tions. Tolerances with regional reg- Grass, forage ...... 10 .0 Grass, hay ...... 25 .0 istration (refer to § 180.1(m)) are estab- Hog, fat ...... 0 .4 lished for the combined residues of the

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fungicide metalaxyl [N-(2,6- Commodity Parts per dimethylphenyl)-N-(methoxyacetyl) al- million anine methyl ester] and its metabolites Cattle, fat ...... 0.02 containing the 2,6-dimethylaniline Cattle, meat byproducts ...... 0.02 moiety, and N-(2-hydroxy methyl-6- Corn, field, grain ...... 8 .0 Corn, pop, grain ...... 8.0 methyl)-N-(methoxyacetyl)-alanine Goat, fat ...... 0 .02 methylester, each expressed as Goat, meat byproducts ...... 0 .02 metalaxyl, in or on the following raw Grain, aspirated fractions ...... 20.0 Hog, fat ...... 0 .02 agricultural commodity: Hog, meat byproducts ...... 0 .02 Horse, fat ...... 0 .02 Commodity Parts per Horse, meat byproducts ...... 0 .02 million Poultry, fat ...... 0.02 Sheep, fat ...... 0 .02 Papaya ...... 0 .1 Sheep, meat byproducts ...... 0 .02 Sorghum, grain, grain ...... 8 .0 (d) Indirect or inadvertent tolerances. Tolerances are established for indirect (b) Section 18 emergency exemptions. or inadvertent residues of metalaxyl in [Reserved] or on the food commodities when (c) Tolerances with regional registra- present therein as a result of the appli- tions. [Reserved] cation of metalaxyl to growing crops (d) Indirect or inadvertent residues. listed in paragraph (a) of this section [Reserved] and other non-food crops to read as fol- [65 FR 33714, May 24, 2000, as amended at 67 lows: FR 41807, June 19, 2002; 67 FR 49617, July 31, 2002; 70 FR 44492, Aug. 3, 2005; 72 FR 53462, Part per Sept. 19, 2007] Commodity million

Barley, bran ...... 1 .0 § 180.410 Triadimefon; tolerances for Barley, flour ...... 1 .0 residues. Barley, grain ...... 0 .2 (a) General. Tolerances are estab- Barley, pearled barley ...... 1 .0 lished for the combined residues of the Barley, straw ...... 2 .0 fungicide triadimefon, 1-(4- Grain, cereal, forage, fodder and straw, group 16, except barley, oat, and wheat; forage ...... 1 .0 chlorophenoxy)-3,3-dimethyl-1-(1H- Grain, cereal, forage, fodder and straw, group 1,2,4-triazol-1-yl)-2-butanone, and 16, except barley, oat, and wheat; stover ...... 1 .0 triadimenol, b-(4-chlorophenoxy)-a-(1,1- Grain, cereal, forage, fodder and straw, group dimethylethyl)-1H-1,2,4-triazole-1-eth- 16, except barley, oat, and wheat; straw ...... 1 .0 Oat, flour ...... 1 .0 anol, expressed as triadimefon, in or on Oat, forage ...... 2 .0 the following food commodities: Oat, grain ...... 0 .2 Oat, groats, rolled oats ...... 1 .0 Expiration/ Commodity Parts per Revocation Oat, straw ...... 2.0 million Date Wheat, bran ...... 1.0 Wheat, flour ...... 1 .0 Pineapple ...... 2.0 None Wheat, forage ...... 2 .0 Wheat, germ ...... 1 .0 (b) Section 18 emergency exemptions. Wheat, grain ...... 0 .2 [Reserved] Wheat, middlings ...... 1 .0 Wheat, shorts ...... 1 .0 (c) Tolerances with regional registra- Wheat, straw ...... 2 .0 tions. [Reserved] (d) Indirect or inadvertent residues. [65 FR 33700, May 24, 2000, as amended at 72 [Reserved] FR 35666, June 29, 2007; 74 FR 46374, Sept. 9, [73 FR 54962, Sept. 24, 2008, as amended at 76 2009; 75 FR 56015, Sept. 15, 2010] FR 34885, June 15, 2011]

§ 180.409 Pirimiphos-methyl; toler- § 180.411 Fluazifop-P-butyl; tolerances ances for residues. for residues. (a) General. Tolerances are estab- (a) General. Tolerances are estab- lished for residues of the insecticide lished for residues of the herbicide pirimiphos-methyl (O-(2-diethylamino- fluazifop-P-butyl, including its me- 6-methyl-4-pyrimidinyl) O,O-dimethyl tabolites and degradates, in or on the phosphorothioate) in or on the fol- following commodities in the table. lowing raw agricultural commodities: Compliance with the tolerance levels

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specified in the table below is to be de- in or on the following commodities in termined by measuring only the sum of the table. Compliance with the toler- fluazifop-P-butyl, butyl(R)-2-[4-[[5- ance levels specified in the table below (trifluoromethyl)-2- is to be determined by measuring only pyridinyl]oxy]phenoxy]propanoate, and the sum of fluazifop-P-butyl, butyl(R)- the free and conjugated forms of the re- 2-[4-[[5-(trifluoromethyl)-2- solved isomer of fluazifop, (R)-2-[4-[[5- pyridinyl]oxy]phenoxy]propanoate, and (trifluoromethyl)-2- the free and conjugated forms of the re- pyridinyl]oxy]phenoxy]propanoic acid, solved isomer of fluazifop, (R)-2-[4-[[5- calculated as the stoichiometric equiv- (trifluoromethyl)-2- alent of fluazifop, in or on the com- pyridinyl]oxy]phenoxy]propanoic acid, modity. calculated as the stoichiometric equiv- alent of fluazifop, in or on the com- Parts per Commodity million modity.

Banana ...... 0.01 Commodity Parts per Beans, dry, seed ...... 50 million Beet, sugar, dried pulp ...... 1 .0 Beet, sugar, molasses ...... 3 .5 Asparagus ...... 3.0 Beet, sugar, roots ...... 0 .25 Coffee, bean ...... 0 .1 Pepper, tabasco ...... 1 .0 Carrot, roots ...... 2.0 Rhubarb ...... 0 .5 Cattle, fat ...... 0.05 Cattle, meat ...... 0 .05 Cattle, meat byproducts ...... 0.05 (d) Indirect or inadvertent residues. Citrus, dried pulp ...... 0 .40 [Reserved] Citrus, juice ...... 0 .06 Citrus, oil ...... 30.0 [65 FR 33714, May 24, 2000, as amended at 74 Cotton, gin byproducts ...... 1 .5 FR 9372, Mar. 4, 2009; 74 FR 46374, Sept. 9, Cotton, refined oil ...... 1.3 2009; 74 FR 47457, Sept. 16, 2009; 76 FR 5703, Cotton, undelinted seed ...... 1 .0 Egg ...... 0 .05 Feb. 2, 2011; 76 FR 59908, Sept. 28, 2011] Endive ...... 6.0 Fruit, citrus, group 10 ...... 0 .03 § 180.412 Sethoxydim; tolerances for Fruit, stone ...... 0 .05 residues. Goat, fat ...... 0 .05 Goat, meat ...... 0.05 (a) Tolerances are established for the Goat, meat byproducts ...... 0 .05 herbicide sethoxydim, including its Grape ...... 0 .01 metabolites and degradates, in or on Hog, fat ...... 0 .05 Hog, meat ...... 0 .05 the commodities in the table below. Hog, meat byproducts ...... 0 .05 Compliance with the tolerance levels Horse, fat ...... 0 .05 specified below is to be determined by Horse, meat ...... 0 .05 Horse, meat byproducts ...... 0 .05 measuring only the sum of the herbi- Milk ...... 0.05 cide 2-[1-(ethoxyimino)butyl]-5-[2- Nut, macadamia ...... 0.1 (ethylthio)propyl]-3-hydroxy-2-cyclo- Onion, bulb ...... 0 .5 hexen-1-one (CAS Reg. No. 74051–80–2) Peanut ...... 1 .5 Peanut, meal ...... 2 .2 and its metabolites containing the 2- Pecans ...... 0 .05 cyclohexen-1-one moiety, calculated as Poultry, fat ...... 0.05 the stoichiometric equivalent of Poultry, meat ...... 0 .05 Poultry, meat byproducts ...... 0.05 sethoxydim, in or on the commodity. Potato1 ...... 1 .0 Potato, chips1 ...... 2 .0 Commodity Parts per Potato, granules/flakes1 ...... 4 .0 illion Sheep, fat ...... 0 .05 Alfalfa, forage ...... 40 Sheep, meat ...... 0.05 Alfalfa, hay ...... 40 Sheep, meat byproducts ...... 0 .05 Almond, hulls ...... 2 .0 Soybean, seed ...... 2 .5 Apricot ...... 0 .2 Sweet potato, roots ...... 0 .05 Apple, wet pomace ...... 0 .8 1 No U.S. registrations. Asparagus ...... 4.0 Bean, succulent ...... 15 (b) Section 18 emergency exemptions. Beet, sugar, molasses ...... 10 [Reserved] Beet, sugar, tops ...... 3.0 Berry, low growing, subgroup 13–07H, except (c) Tolerances with regional registra- strawberry ...... 2 .5 tions. Tolerances with regional reg- Borage, meal ...... 40 istrations are established for residues Buckwheat, flour ...... 25 Buckwheat, grain ...... 19 of the herbicide fluazifop-P-butyl, in- Bushberry subgroup 13–07B ...... 4 .0 cluding its metabolites and degradates, Calendula, meal ...... 20

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Parts per Parts per Commodity illion Commodity illion

Caneberry subgroup 13–07A ...... 5.0 Poultry, meat byproducts ...... 2.0 Canola, meal ...... 40 Radish, tops ...... 4 .5 Castor oil plant, meal ...... 20 Rapeseed, meal ...... 40 Cattle, fat ...... 0.2 Rapeseed subgroup 20A ...... 35 Cattle, meat ...... 0 .2 Rose hip, meal ...... 20 Cattle, meat byproducts ...... 1.0 Safflower, seed ...... 15 Cherry, sweet ...... 0 .2 Salal 1 ...... 5 .0 Cherry, tart ...... 0 .2 Sesame, meal ...... 40 Chinese tallowtree, meal ...... 20 Sheep, fat ...... 0 .2 Citrus, dried pulp ...... 1 .5 Sheep, meat ...... 0.2 Clover, forage ...... 35 Sheep, meat byproducts ...... 1 .0 Clover, hay ...... 55 Soybean, hay ...... 10 Coriander, leaves ...... 4 .0 Soybean, seed ...... 16 Corn, field, forage ...... 2 .0 Spearmint, tops ...... 30 Corn, field, grain ...... 0 .5 Strawberry ...... 10 Corn, field, stover ...... 2 .5 Stokes aster, meal ...... 20 Corn, sweet, forage ...... 3 .0 Sunflower, meal ...... 20 Corn, sweet, kernel plus cob with husk removed 0.4 Sunflower subgroup 20B, except safflower ...... 7 .0 Corn, sweet, stover ...... 3 .5 Sweet rocket, meal ...... 40 Cottonseed subgroup 20C ...... 5 .0 Tallowwood, meal ...... 20 Cowpea, forage ...... 15 Tea oil plant, meal ...... 20 Cowpea, hay ...... 50 Turnip, tops ...... 5.0 Crambe, meal ...... 40 Vegetable, brassica, leafy, group 5 ...... 5.0 Cuphea, meal ...... 40 Vegetable, bulb, group 3–07 ...... 1 .0 Vegetable, cucurbit, group 9 ...... 4.0 Dillweed, fresh leaves ...... 10 Vegetable, fruiting, group 8–10 ...... 4 .0 Echium, meal ...... 40 Vegetable, leafy, except brassica, group 4 ...... 4 .0 Egg ...... 2 .0 Vegetable, root and tuber, group 1 ...... 4 .0 Euphorbia, meal ...... 20 Vernonia, meal ...... 20 Evening primrose, meal ...... 20 Flax seed, meal ...... 40 1 The individual tolerances for Juneberry, Lingonberry, and Fruit, citrus, group 10–10 ...... 0 .5 Salal expire on December 15, 2015. Fruit, pome, group 11–10 ...... 0 .2 Fruit, small, vine climbing, except fuzzy kiwifruit, (b) Section 18 emergency exemptions. subgroup 13–07F ...... 1 .0 [Reserved] Goat, fat ...... 0 .2 (c) Tolerances with regional registra- Goat, meat ...... 0.2 tion. Tolerances are established for the Goat, meat byproducts ...... 1 .0 Gold of pleasure, meal ...... 40 herbicide sethoxydim, including its Grape, raisin ...... 2 .0 metabolites and degradates, in or on Hare’s ear mustard, meal ...... 40 the commodities in the table below. Hog, fat ...... 0 .2 Hog, meat ...... 0 .2 Compliance with the tolerance levels Hog, meat byproducts ...... 1 .0 specified below is to be determined by Horse, fat ...... 0 .2 measuring only the sum of the herbi- Horse, meat ...... 0 .2 cide 2-[1-(ethoxyimino)butyl]-5-[2- Horse, meat byproducts ...... 1 .0 Jojoba, meal ...... 20 (ethylthio)propyl]-3-hydroxy-2-cyclo- Juneberry 1 ...... 5 .0 hexen-1-one) and its metabolites con- Lesquerella, meal ...... 40 taining the 2-cyclohexen-1-one moiety, Lingonberry 1 ...... 5.0 Lunaria, meal ...... 40 calculated as the stoichiometric equiv- Meadowfoam, meal ...... 40 alent of sethoxydim, in or on the com- Milk ...... 0.5 modity. Milkweed, meal ...... 40 Mustard, meal ...... 40 Parts per Nectarine ...... 0 .2 Commodity million Niger seed, meal ...... 20 Nut, tree, group 14 ...... 0 .2 Artichoke, globe ...... 5.0 Oil radish, meal ...... 40 Fescue, forage ...... 7.0 Pea and bean, dried shelled, except soybean, Fescue, hay ...... 4.0 subgroup 6C ...... 25 Rhubarb ...... 0 .3 Pea, field, hay ...... 40 Pea, field, vines ...... 20 (d) Indirect and inadvertent residues. Pea, succulent ...... 10 Peach ...... 0 .2 [Reserved] Peanut ...... 25 [80 FR 34077, June 15, 2015] Peppermint, tops ...... 30 Pistachio ...... 0.2 Poppy seed, meal ...... 40 § 180.413 Imazalil; tolerances for resi- Potato granules/flakes ...... 8 .0 dues. Potato waste, processed ...... 8.0 Poultry, fat ...... 0.2 (a) General. (1) Tolerances are estab- Poultry, meat ...... 0 .2 lished for the combined residues of the

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fungicide imazalil, 1-[2-(2,4- ities in the table in this paragraph. dichlorophenyl)-2-(2- Compliance with the tolerance levels propenyloxy)ethyl]-1H-imidazole, and specified in this paragraph is to be de- its metabolite, 1-(2,4-dichlorophenyl)-2- termined by measuring only (1H-imidazole-1-yl)-1-ethanol, in or on cyromazine, N-cyclopropyl-1,3,5-tri- the following food commodities: azine-2,4,6-triamine, in or on the com- modity. Commodity Parts per million Parts per Commodity million Banana ...... 3.0 Barley, grain ...... 0 .1 Bean, dry, except cowpea ...... 3 .0 Barley, hay ...... 0 .5 Bean, lima ...... 1 .0 Barley, straw ...... 0 .5 Bean, succulent ...... 2 .0 Citrus, dried pulp ...... 25 .0 Broccoli ...... 1 .0 Citrus, oil ...... 200.0 Cabbage, abyssinian ...... 10 .0 Fruit, citrus, postharvest ...... 10.0 Cabbage, seakale ...... 10.0 Wheat, forage ...... 0 .5 Cattle, fat ...... 0.05 Wheat, grain ...... 0 .1 Cattle, kidney ...... 0 .2 Wheat, hay ...... 0 .5 Cattle, meat ...... 0 .05 Wheat, straw ...... 0 .5 Cattle, meat byproducts, except kidney ...... 0.05 Egg ...... 0 .25 (2) Tolerances are established for the Garlic ...... 0 .2 combined residues of the fungicide Garlic, great-headed, bulb ...... 0 .2 Goat, fat ...... 0 .05 imazalil, 1-[2-(2,4-dichlorophenyl)-2-(2- Goat, kidney ...... 0 .2 propenyloxy)ethyl]-1H-imidazole, and Goat, meat ...... 0.05 its metabolites, 3-[2-(2,4- Goat, meat byproducts, except kidney ...... 0 .05 Hanover salad, leaves ...... 10 .0 dichlorophenyl)-2-(2,3- Hog, fat ...... 0 .05 dihydroxypropoxy)ethyl]-2,4- Hog, kidney ...... 0.2 imidazolidinedione (FK772) and 3-[2- Hog, meat ...... 0 .05 Hog, meat byproducts, except kidney ...... 0 .05 (2,4-dichlorophenyl)-2-(hydroxy)]-2,4- Horse, fat ...... 0 .05 imidazolidinedione (FK284), in or on Horse, kidney ...... 0 .2 the following food commodities: Horse, meat ...... 0 .05 Horse, meat byproducts, except kidney ...... 0 .05 Parts per Leek ...... 3 .0 Commodity million Mango 1 ...... 0.3 Milk ...... 0.05 Cattle, fat ...... 0.01 Mushroom ...... 1 .0 Cattle, meat ...... 0 .01 Onion, bulb ...... 0 .2 Cattle, meat byproducts ...... 0.2 Onion, green ...... 3 .0 Goat, fat ...... 0 .01 Onion, potato ...... 3 .0 Goat, meat ...... 0.01 Onion, tree ...... 3.0 Goat, meat byproducts ...... 0 .2 Onion, welsh ...... 3.0 Horse, fat ...... 0 .01 Pepper ...... 1 .0 Horse, meat ...... 0 .01 Potato ...... 0 .8 Horse, meat byproducts ...... 0 .2 Poultry, fat (from chicken layer hens and chick- Milk ...... 0.02 en breeder hens only) ...... 0 .05 Sheep, fat ...... 0 .01 Poultry, meat (from chicken layer hens and Sheep, meat ...... 0.01 chicken breeder hens only) ...... 0 .05 Sheep, meat byproducts ...... 0 .2 Poultry, meat byproducts (from chicken layer hens and chicken breeder hens only) ...... 0 .05 (b) Section 18 emergency exemptions. Rakkyo, bulb ...... 0.2 Shallot, bulb ...... 0 .2 [Reserved] Shallot, fresh leaves ...... 3 .0 (c) Tolerances with regional registra- Sheep, fat ...... 0 .05 tions. [Reserved] Sheep, kidney ...... 0.2 Sheep, meat ...... 0.05 (d) Indirect or inadvertent residues. Sheep, meat byproducts, except kidney ...... 0 .05 [Reserved] Tomato ...... 0.5 Turnip, greens ...... 10.0 [65 FR 33715, May 24, 2000, as amended at 67 Vegetable, brassica, leafy, group 5, except broc- FR 46893, July 17, 2002; 71 FR 54434, Sept. 15, coli ...... 10 .0 2006] Vegetable, leafy, except brassica, group 4 ...... 7 .0 Vegetable, cucurbit, group 9 ...... 1.0 § 180.414 Cyromazine; tolerances for 1There are no U.S. registrations on mango as of May 4, residues. 2000. (a) General. (1) Tolerances are estab- (2) A tolerance of 5.0 parts per mil- lished for residues of the insecticide lion is established for residues of the cyromazine, including its metabolites insecticide cyromazine, including its and degradates, in or on the commod- metabolites and degradates, in or on

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poultry feed when used as a feed addi- cluding its metabolites and degradates, tive only in feed for chicken layer hens in or on the commodities in the table and chicken breeder hens at the rate of in this paragraph. Compliance with the not more than 0.01 pound of tolerance levels specified in this para- cyromazine per ton of poultry feed for graph is to be determined by measuring control of flies in manure of treated only aluminum tris (O- chicken layer hens and chicken breeder ethylphosphonate), in or on the com- hens, provided the feeding of modity. cyromazine-treated feed must stop at Parts per least 3 days (72 hours) before slaughter. Commodity million If the feed is formulated by any person other than the end user, the formulator Avocado ...... 25 Banana ...... 3.0 must inform the end user, in writing, Bushberry subgroup 13B ...... 40 of the 3-day (72 hours) pre-slaughter in- Caneberry subgroup 13A ...... 0 .1 terval. Compliance with the tolerance Cranberry ...... 0 .5 level specified in this paragraph is to Fruit, citrus, group 10 ...... 5 .0 Fruit, pome, group 11 ...... 10 be determined by measuring only Ginseng ...... 0 .1 cyromazine, N-cyclopropyl-1,3,5-tri- Hop, dried cones ...... 45 azine-2,4,6-triamine, in or on the com- Juneberry ...... 40 modity. Lingonberry ...... 40 Nut, macadamia ...... 0.20 (b) Section 18 emergency exemptions. Onion, bulb ...... 0 .5 [Reserved] Onion, green ...... 10.0 (c) Tolerances with regional registra- Pea, succulent ...... 0 .3 tions. [Reserved] Pepper/eggplant, subgroup 8–10B 1 ...... 0 .01 Pineapple ...... 0.1 (d) Indirect or inadvertent residues. Salal ...... 40 Tolerances are established for indirect Strawberry ...... 75 or inadvertent residues of the insecti- Tomato ...... 3 cide cyromazine, including its metabo- Turnip, greens ...... 40 Turnip, roots ...... 15 lites and degradates, in or on the com- Vegetable, brassica, leafy, group 5 ...... 60 modities in the table in this paragraph Vegetable, cucurbit, group 9 ...... 15 when present therein as a result of the Vegetable, leafy, except brassica, group 4 ...... 100 application of cyromazine to growing crops listed in paragraph (a)(1) of this (b) Section 18 emergency exemptions. section. Compliance with the tolerance [Reserved] levels specified in this paragraph is to (c) Tolerances with regional registra- be determined by measuring only tions. Tolerances with regional reg- cyromazine, N-cyclopropyl-1,3,5-tri- istration, as defined in § 180.1(l), are es- azine-2,4,6-triamine, in or on the com- tablished for residues of the fungicide modity. aluminum tris (O-ethylphosphonate), including its metabolites and Commodity Parts per degradates, in or on the commodities million in the table in this paragraph. Compli- Cotton, undelinted seed ...... 0 .1 ance with the tolerance levels specified Corn, sweet, kernel plus cob with husks re- in this paragraph is to be determined moved ...... 0 .5 by measuring only aluminum tris (O- Corn, sweet, forage ...... 0 .5 Corn, sweet, stover ...... 0 .5 ethylphosphonate), in or on the com- Radish, roots ...... 0 .5 modity. Radish, tops ...... 0 .5 Parts per Commodity million [65 FR 25860, May 4, 2000, as amended at 67 FR 72593, Dec. 6, 2002; 68 FR 55269, Sept. 24, Asparagus ...... 0.1 2003; 75 FR 22256, Apr. 28, 2010; 76 FR 23494, Grape ...... 10 Apr. 27, 2011] (d) Indirect or inadvertent residues. § 180.415 Aluminum tris (O- [Reserved] ethylphosphonate); tolerances for residues. [64 FR 36801, July 8, 1999, as amended at 64 FR 37875, July 14, 1999; 65 FR 50438, Aug. 18, (a) General. Tolerances are estab- 2000; 67 FR 55346, Aug. 29, 2002; 68 FR 11335, lished for residues of the fungicide alu- Mar. 10, 2003; 70 FR 7047, Feb. 10, 2005; 76 FR minum tris (O-ethylphosphonate), in- 23494, Apr. 27, 2011; 80 FR 2320, Jan. 16, 2015]

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§ 180.416 Ethalfluralin; tolerances for Commodity Parts per residues. million (a) General. Tolerances are estab- Shellfish ...... 3 .5 lished for residues of the herbicide ethalfluralin, including its metabolites (2) Tolerances for the combined resi- and degradates, in or on the commod- dues of the herbicide triclopyr ((3,5,6- ities in the following table. Compliance trichloro-2-pyridinyl)oxy) acetic acid with the tolerance levels specified in and its metabolite 3,5,6-trichloro-2- the following table is to be determined pyridinol (TCP), as a result of the ap- by measuring only the residues of plication/use of butoxyethyl ester of ethalfluralin, N-ethyl-N-(2-methyl-2- triclopyr or the triethylamine salt of propenyl)-2,6-dinitro-4- triclopyr, are established in or on the (trifluoromethyl)benzenamine. following raw agricultural commod- ities: Commodity Parts per million Parts per Commodity million Bean, dry, seed ...... 0 .05 Dill, dried leaves ...... 0 .05 Cattle, fat ...... 0.05 Dill, fresh leaves ...... 0 .05 Cattle, kidney ...... 0 .5 Peanut ...... 0 .05 Cattle, liver ...... 0 .5 Pea, dry, seed ...... 0 .05 Cattle, meat ...... 0 .05 Potato ...... 0 .05 Cattle, meat byproducts, except kidney and liver 0.05 Rapeseed subgroup 20A ...... 0 .05 Goat, fat ...... 0 .05 Soybean ...... 0.05 Goat, kidney ...... 0 .5 Sunflower subgroup 20B ...... 0.05 Goat, liver ...... 0.5 Vegetable, cucurbit, group 9 ...... 0.05 Goat, meat ...... 0.05 Goat, meat byproducts, except kidney and liver 0 .05 (b) Section 18 emergency exemptions. Hog, fat ...... 0 .05 [Reserved] Hog, kidney ...... 0.5 Hog, liver ...... 0 .5 (c) Tolerances with regional registra- Hog, meat ...... 0 .05 tions. [Reserved] Hog, meat byproducts, except kidney and liver .. 0 .05 (d) Indirect or inadvertent residues. Horse, fat ...... 0 .05 Horse, kidney ...... 0 .5 [Reserved] Horse, liver ...... 0 .5 [49 FR 391, Jan. 4, 1984, as amended at 50 FR Horse, meat ...... 0 .05 Horse, meat byproducts, except kidney and liver 0 .05 4976, Feb. 5, 1985; 52 FR 11262, Apr. 8, 1987; 62 Sheep, fat ...... 0 .05 FR 66014, Dec. 17, 1997; 64 FR 5191, Feb. 3, Sheep, kidney ...... 0.5 1999; 64 FR 54782, Oct. 8, 1999; 66 FR 37598, Sheep, liver ...... 0.5 July 19, 2001; 66 FR 41454, Aug. 8, 2001; 67 FR Sheep, meat ...... 0.05 2342, Jan. 17, 2002; 67 FR 49617, July 31, 2002; Sheep, meat byproducts, except kidney and 72 FR 68534, Dec. 5, 2007; 78 FR 40020, July 3, liver ...... 0 .05 2013] (b) Section 18 emergency exemptions. § 180.417 Triclopyr; tolerances for resi- [Reserved] dues. (c) Tolerances with regional registra- (a) General. (1) Tolerances for resi- tions. [Reserved] dues of the herbicide triclopyr per se, (d) Indirect or inadvertent residues. as a result of the application/use of [Reserved] butoxyethyl ester of triclopyr and [50 FR 18486, May 1, 1985, as amended at 55 triethyylamine salt of triclopyr, are es- FR 26440, June 28, 1990; 60 FR 4095, Jan. 20, tablished in or on the following raw ag- 1995; 62 FR 46894, Sept. 5, 1997; 63 FR 45406, ricultural commodities: Aug. 26, 1998; 67 FR 35048, May 17, 2002; 67 FR 58725, Sept. 18, 2002; 72 FR 41931, Aug. 1, 2007] Commodity Parts per million § 180.418 Cypermethrin and isomers Egg ...... 0 .05 alpha-cypermethrin and zeta- Fish ...... 3 .0 cypermethrin; tolerances for resi- Grass, forage ...... 700.0 dues. Grass, hay ...... 200.0 Milk ...... 0.01 (a) General. (1) Tolerances are estab- Poultry, fat ...... 0.1 lished for residues of the insecticide Poultry, meat ...... 0 .1 cypermethrin (±)alpha cyano-(3- Poultry, meat byproducts, except kidney ...... 0.1 ± Rice, grain ...... 0 .3 phenoxyphenyl)methyl( )cis,trans- Rice, straw ...... 10 .0 3(2,2-dichloroethenyl-2,2-

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dimethylcyclopropanecarboxylate in or Commodity Parts per on the following commodities: million Cabbage ...... 2 .00 Parts per Commodity million Canistel ...... 0 .50 Castor oil plant, refined oil ...... 0.4 Brassica, head and stem, subgroup 5A ...... 2 .0 Castor oil plant, seed ...... 0 .2 Brassica, leafy greens, subgroup 5B ...... 14 .0 Cattle, fat ...... 1.00 Cattle, fat ...... 1.0 Cattle, meat ...... 0 .2 Cattle, meat ...... 0 .2 Cattle, meat byproducts ...... 0.05 Cattle, meat byproducts ...... 0.05 Chinese tallowtree, refined oil ...... 0 .4 Cotton, gin byproducts ...... 11 .0 Chinese tallowtree, seed ...... 0 .2 Cotton, undelinted seed ...... 0 .5 Cilantro, leaves ...... 10 Egg ...... 0 .05 Citrus, dried pulp ...... 1 .8 Goat, fat ...... 1 .0 Citrus, oil ...... 4.0 Goat, meat ...... 0.2 Corn, field, forage ...... 0 .20 Goat, meat byproducts ...... 0 .05 Corn, field, grain ...... 0 .05 Hog, fat ...... 0 .1 Corn, field, stover ...... 3 .00 Hog, meat ...... 0 .05 Corn, pop, grain ...... 0.05 Horse, fat ...... 1 .0 Corn, pop, stover ...... 3.00 Horse, meat ...... 0 .2 Corn, sweet, forage ...... 15 .00 Horse, meat byproducts ...... 0 .05 Corn, sweet, kernel plus cob with husks re- Lettuce, head ...... 4.0 moved ...... 0 .05 Milk, fat (reflecting 0.10 in whole milk) ...... 2 .5 Corn, sweet, stover ...... 15.00 Onion, bulb ...... 0 .1 Cotton, undelinted seed ...... 0 .5 Onion, green ...... 6 .0 Crambe, seed ...... 0.2 Pecan ...... 0 .05 Cuphea, seed ...... 0 .2 Poultry, fat ...... 0.05 Echium, seed ...... 0 .2 Poultry, meat ...... 0 .05 Egg ...... 0 .05 Sheep, fat ...... 1 .0 Euphorbia, refined oil ...... 0 .4 Sheep, meat ...... 0.2 Euphorbia, seed ...... 0 .2 Sheep, meat byproducts ...... 0 .05 Evening primrose, refined oil ...... 0 .4 Evening primrose, seed ...... 0 .2 (2) Tolerances are established for res- Flax, seed ...... 0 .2 Food commodities/feed commodities (other than idues of zeta-cypermethrin, (S-cyano(3- those covered by a higher tolerance as a re- phenoxyphenyl) methyl (±))(cis-trans 3- sult of use on growing crops) in food/feed (2,2-dichloroethenyl)-2,2 handling establishments ...... 0 .05 Fruit, citrus, group 10 ...... 0 .35 dimethylcyclopropanecarboxylate), in- Fruit, pome, group 11 ...... 2 cluding its metabolites and degradates, Fruit, stone, group 12 ...... 1 in or on the commodities in the fol- Goat, fat ...... 1 .00 lowing table. Compliance with the tol- Goat, meat ...... 0.2 Goat, meat byproducts ...... 0 .05 erance levels specified in the following Gold of pleasure, seed ...... 0 .2 table is to be determined by measuring Grain, aspirated fractions ...... 10.0 only total cypermethrin, cyano(3- Grape ...... 2 Grass, forage, fodder, and hay, group 17, for- phenoxyphenyl)methyl 3-(2,2- age ...... 10 dichloroethenyl)-2,2- Grass, forage, fodder and hay, group 17, hay .... 35 dimethylcyclopropane carboxylate, in Hare’s-ear mustard, seed ...... 0 .2 or on the commodity. Hog, fat ...... 0 .1 Hog, meat ...... 0 .05 Horse, fat ...... 1 .00 Parts per Commodity million Horse, meat ...... 0 .2 Horse, meat byproducts ...... 0 .05 Alfalfa, forage ...... 15 Jojoba, refined oil ...... 0.4 Alfalfa, hay ...... 30 Jojoba, seed ...... 0.2 Alfalfa, seed ...... 0 .50 Lesquerella, seed ...... 0 .2 Almond, hulls ...... 6 Lunaria, seed ...... 0 .2 Animal feed, nongrass, group 18, forage ...... 8 Mango ...... 0.70 Animal feed, nongrass, group 18, hay ...... 40 Meadowfoam, seed ...... 0 .2 Artichoke, globe ...... 0.60 Milk, fat (reflecting 0.10 in whole milk) ...... 2 .50 Avocado ...... 0 .50 Milkweed, seed ...... 0 .2 Barley, grain ...... 3 .0 Mustard, seed ...... 0 .2 Barley, hay ...... 6 .0 Niger seed, refined oil ...... 0 .4 Barley, straw ...... 20 .0 Niger seed, seed ...... 0 .2 Beet, sugar, roots ...... 0 .05 Nut, tree, group 14 ...... 0 .05 Beet, sugar, tops ...... 0.20 Oat, grain ...... 3 .0 Berry group 13 ...... 0 .8 Oat, hay ...... 6.0 Borage, seed ...... 0 .2 Oat, straw ...... 20.0 Brassica, head and stem, subgroup 5A ...... 2 .00 Oil radish, seed ...... 0.2 Brassica, leafy greens, subgroup 5B ...... 14 .00 Okra ...... 0.2 Buckwheat, grain ...... 3.0 Onion, bulb ...... 0 .10 Buckwheat, hay ...... 6 .0 Onion, green ...... 3 .00 Buckwheat, straw ...... 20 .0 Papaya ...... 0 .50

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dichloroethenyl)-2,2- Commodity Parts per million dimethylcyclopropane carboxylate, in Pea and bean, dried shelled, except soybean, or on the commodity. subgroup 6C ...... 0 .05 Pea and bean, succulent shelled, subgroup 6B 0 .1 Commodity Parts per Peanut ...... 0 .05 million Pecan ...... 0 .05 Pistachio ...... 0.05 Alfalfa, hay ...... 15 Poppy, seed ...... 0 .2 Beet, sugar, roots ...... 0 .05 Poultry, fat ...... 0.05 Beet, sugar, tops ...... 0.20 Poultry, meat ...... 0 .05 Brassica, head and stem, subgroup 5A ...... 2 .0 Rapeseed ...... 0 .2 Cattle, fat ...... 1.0 Rice, grain ...... 1 .50 Cattle, meat ...... 0 .20 Rice, hulls ...... 6 .00 Cattle, meat byproducts ...... 0.05 Rice, straw ...... 2 .00 Citrus, dried pulp ...... 1 .8 Rice, wild, grain ...... 1.5 Citrus, oil ...... 4.0 Rose hip, refined oil ...... 0.4 Corn, field, grain ...... 0 .05 Rose hip, seed ...... 0.2 Corn, pop, grain ...... 0.05 Rye, grain ...... 3.0 Corn, sweet, kernel plus cob with husks re- Rye, hay ...... 6 .0 moved ...... 0 .05 Rye, straw ...... 20 .0 Cotton, undelinted seed ...... 0 .50 Safflower, seed ...... 0 .2 Egg ...... 0 .05 Sapodilla ...... 0 .50 Food commodities/feed commodities (other than Sapote, black ...... 0 .50 those covered by a higher tolerance as a re- Sapote, mamey ...... 0 .50 sults of use on growing crops) in food/feed Sesame, seed ...... 0 .2 handling establishments ...... 0 .05 Sheep, fat ...... 1 .00 Fruit, citrus, group 10–10 ...... 10 Sheep, meat ...... 0.2 Goat, fat ...... 1 .0 Sheep, meat byproducts ...... 0 .05 Goat, meat ...... 0.20 Sorghum, grain, forage ...... 0.1 Goat, meat byproducts ...... 0 .05 Sorghum, grain, grain ...... 0 .5 Hog, fat ...... 1 .0 Sorghum, grain, stover ...... 5 .0 Hog, meat ...... 0 .05 Soybean, seed ...... 0 .05 Horse, fat ...... 1 .0 Star apple ...... 0 .50 Horse, meat ...... 0 .20 Stokes aster, refined oil ...... 0 .4 Horse, meat byproducts ...... 0 .05 Stokes aster, seed ...... 0 .2 Milk, fat, reflecting 0.10 ppm in whole milk ...... 2 .5 Sugarcane, cane ...... 0.60 Nut, tree, group 14–12 ...... 0 .05 Sunflower, refined oil ...... 0.5 Pea and bean, dried shelled, except soybean, Sunflower, seed ...... 0.2 subgroup 6C ...... 0 .05 Sweet rocket, seed ...... 0 .2 Pea and bean, succulent shelled, subgroup 6B 0 .10 Tallowwood, refined oil ...... 0.4 Poultry, fat ...... 0.05 Tallowwood, seed ...... 0 .2 Poultry, meat ...... 0 .05 Tea oil plant, refined oil ...... 0 .4 Rice, grain ...... 1 .5 Tea oil plant, seed ...... 0 .2 Sheep, fat ...... 1 .0 Turnip, greens ...... 14 Sheep, meat ...... 0.20 Vegetable, cucurbit, group 9 ...... 0.2 Sheep, meat byproducts ...... 0 .05 Vegetable, fruiting, group 8 ...... 0.2 Sorghum, grain, grain ...... 0 .50 Vegetable, leafy, except brassica, group 4 ...... 10.00 Soybean, seed ...... 0 .05 Vegetable, legume, edible podded, subgroup 6A 0 .5 Vegetable, cucurbit, group 9 ...... 0.20 Vegetable, root and tuber, group 1, except Vegetable, fruiting, group 8–10 ...... 0 .20 sugar beet ...... 0 .1 Vegetable, leafy, group 4 ...... 10 Vernonia, refined oil ...... 0 .4 Vegetable, legume, edible podded, subgroup 6A 0 .50 Vernonia, seed ...... 0 .2 Vegetable, root and tuber, group 1, except Wheat, forage ...... 3 .0 sugar beet ...... 0 .10 Wheat, grain ...... 0 .2 Wheat, grain ...... 0 .20 Wheat, hay ...... 6 .0 Wheat, straw ...... 7 .0 (b) Section 18 emergency exemptions. [Reserved] (3) Tolerances are established for res- (c) Tolerances with regional registra- idues of the insecticide, alpha- tions. [Reserved] cypermethrin, (R)-cyano(3- (d) Indirect or inadvertent residues. phenoxyphenyl)methyl (1 3 )-rel-3- S, S [Reserved] (2,2-dichloroethenyl)-2,2- dimethylcyclopropane carboxylate, in- [62 FR 63235, 63243, Nov. 26, 1997, as amended cluding its metabolites and degradates, at 63 FR 48586, Sept. 11, 1998; 66 FR 47993, in or on the commodities in the table Sept. 17, 2001; 67 FR 6430, Feb. 12, 2002; 67 FR below. Compliance with the tolerance 56495, Sept. 4, 2002; 69 FR 71717, Dec. 10, 2004; 71 FR 78382, Dec. 29, 2006; 72 FR 53462, Sept. levels specified below is to be deter- 19, 2007; 72 FR 71801, Dec. 19, 2007; 73 FR 1525, mined by measuring only total Jan. 9, 2008; 77 FR 72984, Dec. 7, 2012; 78 FR cypermethrin, cyano(3- 7275, Feb. 1, 2013; 79 FR 73213, Dec. 10, 2014; 79 phenoxyphenyl)methyl 3-(2,2- FR 77394, Dec. 24, 2014]

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§ 180.419 Chlorpyrifos-methyl; toler- (d) Indirect or inadvertent residues. ances for residues. [Reserved] (a) General. (1) Tolerances are estab- [65 FR 33715, May 24, 2000, as amended at 74 lished for the combined residues of the FR 46374, Sept. 9, 2009] insecticide chlorpyrifos-methyl [O,-O,- dimethyl O-(3,5,6-trichloro-2-pyridyl)] § 180.420 Fluridone; tolerances for res- phosphorothioate and its metabolite idues. (3,5,6-trichloro-2-pyridinol) in or on the (a) General. (1) Tolerances are estab- following food commodities: lished for residues of the herbicide fluridone, including its metabolites Commodity Parts per and degradates, in or on the commod- million ities in the table in this paragraph. Barley, grain ...... 6 .0 Compliance with the tolerance levels Cattle, fat ...... 0.5 specified in this paragraph is to be de- Cattle, meat ...... 0 .5 termined by measuring only the sum of Cattle, meat byproducts ...... 0.5 Egg ...... 0 .1 fluridone, 1-methyl-3-phenyl-5-(3- Goat, fat ...... 0 .5 (trifluoromethyl)phenyl)-4(1H)- Goat, meat ...... 0.5 pyridinone, and its bound residues, cal- Goat, meat byproducts ...... 0 .5 culated as the stoichiometric equiva- Hog, fat ...... 0 .5 Hog, meat ...... 0 .5 lent of fluridone, in or on the com- Hog, meat byproducts ...... 0 .5 modity. Horse, fat ...... 0 .5 Horse, meat ...... 0 .5 Parts per Commodity million Horse, meat byproducts ...... 0 .5 Milk, fat (0.05 ppm (N) in whole milk ...... 1 .25 Crayfish ...... 0.5 Oat, grain ...... 6 .0 Fish ...... 0 .5 Poultry, fat ...... 0.5 Poultry, meat ...... 5 Poultry, meat byproducts ...... 5 (2) Tolerances are established for res- Rice, grain ...... 6 .0 idues of the herbicide fluridone, includ- Sheep, fat ...... 0 .5 ing its metabolites and degradates, in Sheep, meat ...... 0.5 or on the commodities in the table in Sheep, meat byproducts ...... 0 .5 this paragraph. Compliance with the Sorghum, grain ...... 6 .0 Wheat, grain ...... 6 .0 tolerance levels specified in this para- graph is to be determined by measuring (2) Tolerances are established for the only fluridone, 1-methyl-3-phenyl-5-(3- combined residues of the insecticide (trifluoromethyl)phenyl)-4(1H)- chlorpyrifos-methyl (O,-O- dimethyl-O- pyridinone, in or on the commodity. (3,5,6-trichloro-2-pyridyl) Parts per phosphorothioate and its metabolite Commodity million (3,5,6-trichloro-2-pyridinol) in or on the Cattle, fat ...... 0.05 following food commodities when Cattle, kidney ...... 0 .1 present therein as a result of applica- Cattle, liver ...... 0 .1 tion to stored grains: Cattle, meat ...... 0 .05 Cattle, meat byproducts ...... 0.05 Parts per Egg ...... 0 .05 Commodity million Goat, fat ...... 0 .05 Goat, kidney ...... 0 .1 Barley, bran ...... 90 Goat, liver ...... 0.1 Barley, pearled barley ...... 90 Goat, meat ...... 0.05 Rice, bran ...... 30 Goat, meat byproducts ...... 0 .05 Rice, hulls ...... 30 Hog, fat ...... 0 .05 Rice, polished rice ...... 30 Hog, kidney ...... 0.1 Sorghum, grain, bran ...... 90 Hog, liver ...... 0 .1 Hog, meat ...... 0 .05 Wheat, bran ...... 30 Hog, meat byproducts ...... 0 .05 Wheat, germ ...... 30 Horse, fat ...... 0 .05 Wheat, middlings ...... 30 Horse, kidney ...... 0 .1 Wheat, shorts ...... 30 Horse, liver ...... 0 .1 Horse, meat ...... 0 .05 (b) Section 18 emergency exemptions. Horse, meat byproducts ...... 0 .05 [Reserved] Milk ...... 0.05 Poultry, fat ...... 0.05 (c) Tolerances with regional registra- Poultry, kidney ...... 0 .01 tions. [Reserved] Poultry, liver ...... 0 .01

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Parts per Parts per Commodity million Commodity million

Poultry, meat ...... 0 .05 Berry, group 13 ...... 0 .1 Poultry, meat byproducts ...... 0.05 Cotton, undelinted seed ...... 0 .1 Sheep, fat ...... 0 .05 Cranberry ...... 0 .1 Sheep, kidney ...... 0.1 Fruit, citrus, group 10 ...... 0 .1 Sheep, liver ...... 0.1 Fruit, pome, group 11 ...... 0.1 Sheep, meat ...... 0.05 Fruit, stone, group 12 ...... 0 .1 Sheep, meat byproducts ...... 0 .05 Grain, cereal, forage, fodder and straw, group 16 ...... 0 .1 (b) Section 18 emergency exemptions. Grain, cereal, group 15 ...... 0.1 Grape ...... 0 .1 Time-limited tolerances specified in Grass, forage ...... 0 .15 the following table are established for Hop, dried cones ...... 0 .1 residues of the herbicide fluridone, 1- Nut, tree, group 14 ...... 0 .1 Okra ...... 0.1 methyl-3-phenyl-5-(3- Strawberry ...... 0 .1 (trifluoromethyl)phenyl)-4(1H)- Vegetable, brassica, leafy, group 5 ...... 0.1 pyridinone, including its metabolites Vegetable, cucurbit, group 9 ...... 0.1 Vegetable, fruiting, group 8 ...... 0.1 and degradates in or on the specified Vegetable, leafy, except brassica, group 4 ...... 0 .1 agricultural commodities, resulting Vegetable, leaves of root and tuber, group 2 ..... 0 .1 from use of the pesticide pursuant to Vegetable, legume, group 6 ...... 0 .1 the Federal Insecticide, Fungicide, and Vegetable, root and tuber, group 1 ...... 0 .1 Rodenticide Act (FIFRA) section 18 emergency exemptions. Compliance [76 FR 23495, Apr. 27, 2011, as amended at 77 with the tolerance levels specified FR 66720, Nov. 7, 2012; 80 FR 18143, Apr. 3, below is to be determined by measuring 2015] only fluridone. The tolerances expire § 180.421 Fenarimol; tolerances for res- on the date specified in the table. idues. Expiration/ (a) General. Tolerances are estab- Commodity Parts per revocation million date lished for residues of fenarimol, includ- ing its metabolites and degradates, in Cotton, undelinted seed ...... 0.1 12/31/17 or on the commodities in the following table. Compliance with the tolerance (c) Tolerances with regional registra- levels specified in the following table is [Reserved] tions. to be determined by measuring only (d) Indirect or inadvertent residues. fenarimol alpha-(2 chlorophenyl)- Tolerances are established for indirect alpha-(4-chlorophenyl)-5- or inadvertent residues of the herbicide pyrimidinemethanol. fluridone, including its metabolites and degradates, in or on the irrigated Commodity Parts per crop commodities and crop groupings million in the table in this paragraph, result- Apple ...... 0.3 ing from use of irrigation water con- Apple, wet pomace ...... 0 .3 taining residues of 0.15 parts per mil- Banana ...... 0.25 Cattle, fat ...... 0.01 lion following applications of fluridone Cattle, kidney ...... 0 .01 on or around aquatic sites. Where tol- Cattle, meat ...... 0 .01 erances are established at higher levels Cattle, meat byproducts, except kidney ...... 0.05 from other uses of fluridone on the Cherry, sweet ...... 1 .0 Cherry, tart ...... 1 .0 crops in the table in this paragraph, Goat, fat ...... 0 .01 the higher tolerance also applies to res- Goat, kidney ...... 0 .01 idues in or on the irrigated commodity. Goat, meat ...... 0.01 Goat, meat byproducts, except kidney ...... 0 .05 Compliance with the tolerance levels Grape ...... 0 .1. specified in this paragraph is to be de- Hazelnut ...... 0 .02 termined by measuring only fluridone, Hop, dried cones ...... 5 .0 Horse, fat ...... 0 .01 1-methyl-3-phenyl-5-(3- Horse, kidney ...... 0 .01 (trifluoromethyl)phenyl)-4(1H)- Horse, meat ...... 0 .01 pyridinone, in or on the commodity. Horse, meat byproducts, except kidney ...... 0 .05 Pear ...... 0 .1 Parts per Pecan ...... 0 .02 Commodity million Sheep, fat ...... 0 .01 Sheep, kidney ...... 0.01 Animal feed, nongrass, group 18 ...... 0 .15 Sheep, meat ...... 0.01 Avocado ...... 0 .1 Sheep, meat byproducts, except kidney ...... 0 .05

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including its metabolites and Commodity Parts per million degradates, in or on food commodities Vegetable, cucurbit, group 9* ...... 0 .20 (other than those covered by a higher *There are no U.S. registrations as of August 27, 2010. tolerance as a result of use on growing crops) in food-handling establishments. (b) Section 18 emergency exemptions. Compliance with the tolerance level [Reserved] specified in this paragraph is to be de- (c) Tolerances with regional registra- termined by measuring only the sum of tions. [Reserved] tralomethrin, (S)-cyano(3- (d) Indirect or inadvertent residues. phenoxyphenyl)methyl (1R,3S)-2,2-di- [Reserved] methyl-3-(1,2,2,2- [51 FR 39662, Oct. 30, 1986, as amended at 53 tetrabromoethyl) FR 27349, July 20, 1988; 53 FR 44403, Nov. 3, cyclopropanecarboxylate, and its me- 1988; 54 FR 45734, Oct. 31, 1989; 60 FR 33354, tabolites (S)-cyano(3- June 28, 1995; 62 FR 49937, Sept. 24, 1997; 62 FR 61447, Nov. 18, 1997; 67 FR 35048, May 17, 2002; phenoxyphenyl)methyl (1R,3R)-3-(2,2- 67 FR 41807, June 19, 2002; 69 FR 6567, Feb. 11, dibromoethenyl)-2,2- 2004; 71 FR 32846, June 7, 2006; 71 FR 54434, dimethylcyclopropanecarboxylate and Sept. 15, 2006; 74 FR 68173, Dec. 23, 2009; 75 FR (S)-cyano(3-phenoxyphenyl)methyl 56897, Sept. 17, 2010] (1S,3R)-3-(2,2-dibromoethenyl)-2,2- dimethylcyclopropanecarboxylate, cal- § 180.422 Tralomethrin; tolerances for culated as the stoichiometric equiva- residues. lent of tralomethrin, in or on the com- (a) General. (1) Tolerances are estab- modity. lished for residues of the insecticide (i) The insecticide may be present as tralomethrin, including its metabolites a residue from application of and degradates, in or on the commod- tralomethrin in food-handling estab- ities in the table in this paragraph. lishments, including food service, man- Compliance with the tolerance levels ufacturing, and processing establish- specified in this paragraph is to be de- ments, such as restaurants, cafeterias, termined by measuring only the sum of supermarkets, bakeries, breweries, tralomethrin, (S)-cyano(3- dairies, meat slaughtering and packing phenoxyphenyl)methyl (1R,3S)-2,2-di- plants, and canneries. methyl-3-(1,2,2,2- (ii) The application shall be made in tetrabromoethyl) accordance with the following pre- cyclopropanecarboxylate, and its me- scribed conditions: Application shall be tabolites (S)-cyano(3- limited to a general surface and spot phenoxyphenyl)methyl (1R,3R)-3-(2,2- and/or crack and crevice treatment in dibromoethenyl)-2,2- food-handling establishments where dimethylcyclopropanecarboxylate and food and food products are held, proc- (S)-cyano(3-phenoxyphenyl)methyl essed, prepared, and served. General (1S,3R)-3-(2,2-dibromoethenyl)-2,2- dimethylcyclopropanecarboxylate, cal- surface application may be used only culated as the stoichiometric equiva- when the facility is not in operation lent of tralomethrin, in or on the com- provided exposed food has been covered modity. or removed from the area being treat- ed. All food-contact surfaces and equip- Expiration/ ment must be thoroughly cleaned after Commodity Parts per revocation million date general surface applications. Spot and/ or crack and crevice application may Broccoli ...... 0.5 7/9/13 be used while the facility is in oper- Cotton, undelinted seed ...... 0.02 7/9/13 Cotton, oil ...... 0.20 7/9/13 ation provided exposed food is covered Lettuce, head ...... 1.00 7/9/13 or removed from the area being treated Lettuce, leaf ...... 3.00 7/9/13 prior to application. Spray concentra- Soybean, seed ...... 0.05 7/9/13 Sunflower, seed ...... 0.05 7/9/13 tion shall be limited to a maximum of 0.06 percent active ingredient. Con- (2) A tolerance of 0.02 part per mil- tamination of food and food-contact lion with an expiration/revocation date surfaces shall be avoided. of July 9, 2013 is established for resi- (3) A tolerance of 0.02 part per mil- dues of the insecticide tralomethrin, lion with an expiration/revocation date

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of July 9, 2013 is established for resi- (d) Indirect or inadvertent residues. dues of the insecticide tralomethrin, [Reserved] including its metabolites and [62 FR 63001, Nov. 26, 1997, as amended at 62 degradates, in or on feed commodities FR 66025, Dec. 17, 1997; 65 FR 33701, May 24, (other than those covered by a higher 2000; 71 FR 74817, Dec. 13, 2006; 77 FR 59127, tolerance as a result of use on growing Sept. 26, 2012] crops) in feed-handling establishments. Compliance with the tolerance level § 180.425 Clomazone; tolerances for specified in this paragraph is to be de- residues. termined by measuring only the sum of (a) General. Tolerances are estab- tralomethrin, (S)-cyano(3- lished for residues of the herbicide phenoxyphenyl)methyl (1R,3S)-2,2-di- clomazone, including its metabolites methyl-3-(1,2,2,2- and degradates, in or on the commod- tetrabromoethyl) ities in the table in this paragraph. cyclopropanecarboxylate, and its me- Compliance with the tolerance levels tabolites (S)-cyano(3- specified in this paragraph is to be de- phenoxyphenyl)methyl (1R,3R)-3-(2,2- termined by measuring only dibromoethenyl)-2,2- clomazone, 2-[(2-chlorophenyl)methyl]- dimethylcyclopropanecarboxylate and 4,4-dimethyl-3-isoxazolidinone, in or on (S)-cyano(3-phenoxyphenyl)methyl the commodity. (1S,3R)-3-(2,2-dibromoethenyl)-2,2- dimethylcyclopropanecarboxylate, cal- Commodity Parts per culated as the stoichiometric equiva- million lent of tralomethrin, in or on the com- Bean, snap, succulent ...... 0 .05 modity. Brassica, head and stem, subgroup 5A ...... 0 .10 (i) The insecticide may be present as Cotton, undelinted seed ...... 0 .05 a residue from application of Cowpea, forage ...... 0 .05 Cowpea, hay ...... 0 .05 tralomethrin in feed-handling estab- Cucumber ...... 0 .1 lishments, including feed manufac- Pea, southern, dry seed ...... 0.05 turing and processing establishments. Pea, southern, succulent seed ...... 0 .05 (ii) The application shall be made in Pea, succulent ...... 0 .05 accordance with the following pre- Pepper ...... 0 .05 Peppermint, tops ...... 0 .05 scribed conditions: Application shall be Pumpkin ...... 0.1 limited to a general surface and spot Rhubarb ...... 0 .30 and/or crack and crevice treatment in Rice, grain ...... 0 .02 feed-handling establishments where Rice, straw ...... 0 .02 feed and feed products are held or proc- Soybean ...... 0.05 Spearmint, tops ...... 0 .05 essed. General surface application may Squash, summer ...... 0 .1 be used only when the facility is not in Squash, winter ...... 0 .1 operation provided exposed feed has Sugarcane, cane ...... 0.05 been covered or removed from the area Sweet potato, roots ...... 0 .05 being treated. All feed-contact surfaces Vegetable, cucurbit, group 9 ...... 0.05 Vegetable, tuberous and corm, except potato, and equipment must be thoroughly subgroup 1D ...... 0 .05 cleaned after general surface applica- tions. Spot and/or crack and crevice ap- (b) Section 18 emergency exemptions. plication may be used while the facil- [Reserved] ity is in operation provided exposed (c) Tolerances with regional registra- feed is covered or removed from the tions. [Reserved] area being treated prior to application. (d) Indirect or inadvertent residues. Spray concentration shall be limited to [Reserved] a maximum of 0.06 percent active in- gredient. Contamination of feed and [51 FR 9446, Mar. 19, 1986] feed-contact surfaces shall be avoided. EDITORIAL NOTE: For FEDERAL REGISTER ci- (b) Section 18 emergency exemptions. tations affecting § 180.425, see the List of CFR [Reserved] Sections Affected, which appears in the (c) Tolerances with regional registra- Finding Aids section of the printed volume tions. [Reserved] and at www.fdsys.gov.

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§ 180.426 2-[4,5-Dihydro-4-methyl-4-(1- Commodity Parts per methylethyl)-5-oxo-1H-imidazol-2- million yl]-3-quinoline carboxylic acid; tol- Sugarcane, cane ...... 0.05 erance for residues. Wheat, forage ...... 5 .0 A tolerance is established for resi- Wheat, grain ...... 0 .1 dues of the herbicide 2-[4,5-dihydro-4- Wheat, hay ...... 20 .0 Wheat, straw ...... 0 .3 methyl-4-(1-methylethyl)-5-oxo-1H- imidazol-2-yl]-3-quinoline carboxylic (2) Tolerances are established for res- acid, in or on the raw agricultural com- idues of metsulfuron methyl (methyl- modity soybean at 0.05 part per mil- 2[[[[(4-methoxy- 6-methyl-1,3,5-triazin- lion. 2- yl)amino]carbonyl]amino] sulfonyl] [51 FR 13309, Apr. 2, 1986] benzoate) in or on the following raw agricultural commodities: § 180.427 Tau-Fluvalinate; tolerances for residues. Parts per Commodity million (a) General. Tolerances are estab- lished for residues of the insecticide Cattle, fat ...... 0.1 tau-fluvalinate, cyano-(3- Cattle, kidney ...... 0 .5 Cattle, meat ...... 0 .1 phenoxyphenyl)methyl N-[2-chloro-4- Cattle, meat byproducts ...... 0.1 (trifluoromethyl)phenyl]-D-valinate, in Goat, fat ...... 0 .1 or on the following food commodities: Goat, kidney ...... 0 .5 Goat, meat ...... 0.1 Goat, meat byproducts ...... 0 .1 Commodity Parts per million Hog, fat ...... 0 .1 Hog, kidney ...... 0.5 Honey ...... 0.02 Hog, meat ...... 0 .1 Hog, meat byproducts ...... 0 .1 (b) Section 18 emergency exemptions. Horse, fat ...... 0 .1 [Reserved] Horse, kidney ...... 0 .5 (c) Tolerances with regional registra- Horse, meat ...... 0 .1 tions. [Reserved] Horse, meat byproducts ...... 0 .1 Milk ...... 0.05 (d) Indirect and inadvertent residues. Sheep, fat ...... 0 .1 [Reserved] Sheep, kidney ...... 0.5 Sheep, meat ...... 0.1 [65 FR 33701, May 24, 2000, as amended at 67 Sheep, meat byproducts ...... 0 .1 FR 49617, July 31, 2002; 73 FR 52616, Sept. 10, 2008] (b) Section 18 emergency exemptions. [Reserved] § 180.428 Metsulfuron methyl; toler- ances for residues. (c) Tolerances with regional registra- tions. [Reserved] (a) General. (1) Tolerances are estab- (d) Indirect or inadvertent residues. lished for the combined residues of the [Reserved] herbicide metsulfuron methyl (methyl 2-[[[[(4-methoxy-6-methyl-1,3,5- triazin- [64 FR 70191, Dec. 16, 1999, as amended at 66 2-yl)amino]carbonyl]amino] sulfonyl] FR 64773, Dec. 14, 2001; 67 FR 51097, Aug. 7, benzoate) and its metabolite methyl 2- 2002] [[[[(4-methoxy-6-methyl-1-,3,5- triazin- 2-yl)amino]carbonyl]amino] sulfonyl]- § 180.429 Chlorimuron ethyl; toler- ances for residues. 4-hydroxybenzoate in or on the fol- lowing raw material agricultural com- (a) General. Tolerances are estab- modities: lished for residues of the herbicide chlorimuron ethyl, including its me- Parts per tabolites and degradates, in or on the Commodity million commodities in the table below. Com- Barley, grain ...... 0 .1 pliance with the tolerance levels speci- Barley, hay ...... 20 .0 fied in the following table is to be de- Barley, straw ...... 0 .3 Grass, forage ...... 15 .0 termined by measuring only Grass, hay ...... 15 .0 chlorimuron ethyl, ethyl 2-[[[[(4- Grass, straw ...... 15 .0 chloro-6-methoxypyrimidin- Sorghum, grain, forage ...... 0.2 Sorghum, grain, grain ...... 0 .1 2yl)amino]carbonyl]sulfonyl]benzoate] Sorghum, grain, stover ...... 0 .2 in or on the following commodities:

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Parts per Parts per Commodity million Commodity million

Berry, low growing, except strawberry, subgroup Sheep, meat ...... 0.05 13–07H ...... 0 .02 Soybean ...... 0.05 Corn, field, forage ...... 0 .5 Wheat, grain ...... 0 .05 Corn, field, grain ...... 0 .01 Wheat, straw ...... 0 .50 Corn, field, stover ...... 2 .0 Grain, aspirated fractions ...... 3 .0 Peanut ...... 0 .02 (b) Section 18 emergency exemptions. Soybean, forage ...... 0 .45 Time-limited tolerances are estab- Soybean, hay ...... 1 .8 Soybean, seed ...... 0 .05 lished for residues of the herbicide fenoxaprop-ethyl, including its me- (b) Section 18 emergency exemptions. tabolites and degradates, in or on the [Reserved] commodities in the table in this para- (c) Tolerances with regional registra- graph in connection with use of tions. [Reserved] fenoxaprop-ethyl under section 18 (d) Indirect or inadvertent residues. emergency exemptions granted by [Reserved] EPA. Compliance with the tolerance levels specified in this paragraph is to [74 FR 10494, Mar. 11, 2009, as amended at 74 be determined by measuring only the FR 67087, Dec. 18, 2009] sum of fenoxaprop-ethyl, (±)-ethyl 2-[4- § 180.430 Fenoxaprop-ethyl; tolerances [(6-chloro-2- for residues. benzoxazolyl)oxy]phenoxy]propanoate, and its metabolites, 2-[4-[(6-chloro-2- (a) General. Tolerances are estab- lished for residues of the herbicide benzoxazolyl)oxy]phenoxy]propanoic fenoxaprop-ethyl, including its me- acid and 6-chloro-2,3- tabolites and degradates, in or on the dihydrobenzoxazol-2-one, calculated as commodities in the table in this para- the stoichiometric equivalent of graph. Compliance with the tolerance fenoxaprop-ethyl, in or on the com- levels specified in this paragraph is to modity. The tolerances expire and are be determined by measuring only the revoked on the dates specified in the sum of fenoxaprop-ethyl, (±)-ethyl 2-[4- table in this paragraph. [(6-chloro-2- Parts per Expiration/ benzoxazolyl)oxy]phenoxy]propanoate, Commodity million revocation and its metabolites, 2-[4-[(6-chloro-2- date benzoxazolyl)oxy]phenoxy]propanoic Grass, forage ...... 0.05 12/31/16 acid and 6-chloro-2,3- Grass, hay ...... 0.05 12/31/16 dihydrobenzoxazol-2-one, calculated as the stoichiometric equivalent of (c) Tolerances with regional registra- fenoxaprop-ethyl, in or on the com- tions. Tolerances with regional reg- modity. istration, as defined in § 180.1(l), are es- tablished for residues of the herbicide Parts per fenoxaprop-ethyl, including its me- Commodity million tabolites and degradates, in or on the Barley, grain ...... 0 .05 commodities in the table in this para- Barley, straw ...... 0 .1 Cattle, fat ...... 0.05 graph when fenoxaprop-ethyl is used in Cattle, meat byproducts ...... 0.05 the states of Oregon, Washington, and Cattle, meat ...... 0 .05 Utah. Compliance with the tolerance Cotton, undelinted seed ...... 0 .05 levels specified in this paragraph is to Goat, fat ...... 0 .05 Goat, meat byproducts ...... 0 .05 be determined by measuring only the Goat, meat ...... 0.05 sum of fenoxaprop-ethyl, (±)-ethyl 2-[4- Hog, fat ...... 0 .05 [(6-chloro-2- Hog, meat byproducts ...... 0 .05 Hog, meat ...... 0 .05 benzoxazolyl)oxy]phenoxy]propanoate, Horse, fat ...... 0 .05 and its metabolites, 2-[4-[(6-chloro-2- Horse, meat byproducts ...... 0 .05 benzoxazolyl)oxy]phenoxy]propanoic Horse, meat ...... 0 .05 Milk ...... 0.02 acid and 6-chloro-2,3- Peanut ...... 0 .05 dihydrobenzoxazol-2-one, calculated as Peanut, hulls ...... 0 .05 the stoichiometric equivalent of Rice, grain ...... 0 .05 Sheep, fat ...... 0 .05 fenoxaprop-ethyl, in or on the com- Sheep, meat byproducts ...... 0 .05 modity

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Parts per Parts per Commodity million Commodity million

Grass, hay ...... 0 .09 Grass, hay ...... 500.0 Hog, fat ...... 0 .2 (d) Indirect or inadvertent residues. Hog, meat ...... 0 .2 Hog, meat byproducts ...... 0 .2 [Reserved] Hop, dried cones ...... 5 .0 Horse, fat ...... 1 .0 [63 FR 1377, Jan. 9, 1998, as amended at 63 FR Horse, liver ...... 3 .0 19837, Apr. 22, 1998; 73 FR 33718, June 13, 2008; Horse, meat ...... 1 .0 75 FR 80346, Dec. 22, 2010; 76 FR 23495, Apr. 27, Horse, meat byproducts, except liver ...... 36 .0 2011; 78 FR 78748, Dec. 27, 2013; 79 FR 26164, Milk ...... 0.2 May 7, 2014] Oat, forage ...... 9 .0 Oat, grain ...... 3 .0 Oat, groats/rolled oats ...... 12 § 180.431 Clopyralid; tolerances for Oat, straw ...... 9.0 residues. Peppermint, tops ...... 3 .0 Plum, prune, dried ...... 1.5 (a) General. Tolerances are estab- Poultry, fat ...... 0.2 lished for residues of the herbicide Poultry, meat ...... 0 .2 clopyralid, including its metabolites Poultry, meat byproducts ...... 0.2 Rapeseed, forage ...... 3 .0 and degradates, in or on the commod- Rapeseed, meal ...... 6 .0 ities in the table below from its appli- Rapeseed, subgroup 20A, except gold of pleas- cation in the acid form or in the form ure ...... 3 .0 Sheep, fat ...... 1 .0 of its salts. Compliance with the toler- Sheep, liver ...... 3.0 ance levels specified below is to be de- Sheep, meat ...... 1.0 termined by measuring only clopyralid, Sheep, meat byproducts, except liver ...... 36 .0 Spearmint, tops ...... 3 .0 (3,6-dichloro-2-pyridinecarboxylic acid), Spinach ...... 5 .0 in or on the following commodities: Strawberry ...... 4 .0 Swiss chard ...... 3.0 Commodity Parts per Teff, forage ...... 9 .0 million Teff, grain ...... 3 .0 Teff, hay ...... 9 .0 Apple ...... 0.05 Teff, straw ...... 9 .0 Asparagus ...... 1.0 Turnip, greens ...... 4.0 Barley, bran ...... 12 Turnip, roots ...... 1 .0 Barley, grain ...... 3 .0 Wheat, bran ...... 12 Barley, hay ...... 9 .0 Wheat, forage ...... 9 .0 Barley, pearled barley ...... 12 Wheat, germ ...... 12 Barley, straw ...... 9 .0 Wheat, grain ...... 3 .0 Beet, garden, tops ...... 3 .0 Wheat, middling ...... 12 Beet, garden, roots ...... 4 .0 Wheat, shorts ...... 12 Beet, sugar, molasses ...... 10 Wheat, straw ...... 9 .0 Beet, sugar, roots ...... 2 .0 Beet, sugar, tops ...... 3.0 Brassica, head and stem, subgroup 5A ...... 2 .0 (b) Section 18 emergency exemptions. Brassica, leafy greens, subgroup 5B ...... 5 .0 [Reserved] Bushberry subgroup 13-07B ...... 0 .50 (c) Tolerances with regional registra- Canola, meal ...... 6 .0 tions. [Reserved] Canola, seed ...... 3 .0 Cattle, fat ...... 1.0 (d) Indirect or inadvertent residues. Cattle, liver ...... 3 .0 [Reserved] Cattle, meat ...... 1 .0 Cattle, meat byproducts, except liver ...... 36 .0 [52 FR 10566, Apr. 2, 1987] Corn, field, forage ...... 3 .0 Corn, field, grain ...... 1 .0 EDITORIAL NOTE: For FEDERAL REGISTER ci- Corn, field, milled byproducts ...... 1 .5 tations affecting § 180.431, see the List of CFR Corn, field, stover ...... 10 .0 Sections Affected, which appears in the Corn, pop, grain ...... 1.0 Finding Aids section of the printed volume Corn, pop, stover ...... 10.0 and at www.fdsys.gov. Corn, sweet, forage ...... 7 .0 Corn, sweet, kernel plus cob with husks re- § 180.432 Lactofen; tolerances for resi- moved ...... 1 .0 Corn, sweet, stover ...... 10.0 dues. Cranberry ...... 4 .0 (a) General. Tolerances are estab- Egg ...... 0 .1 Flax, meal ...... 6 .0 lished for residues of the herbicide Fruit, stone, group 12 ...... 0 .5 lactofen, including its metabolites and Goat, fat ...... 1 .0 degradates, in or on the commodities Goat, liver ...... 3.0 in the table in this paragraph. Compli- Goat, meat ...... 1.0 Goat, meat byproducts, except liver ...... 36 .0 ance with the tolerance levels specified Grass, forage ...... 500.0 in this paragraph is to be determined

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by measuring only lactofen, 2-ethoxy-1- Commodity Parts per methyl-2-oxoethyl 5-[2-chloro-4- million (trifluoromethyl)phenoxy]-2- Cucumber ...... 0.025 nitrobenzoate, in or on the commodity. Pea, succulent ...... 0.025 Pepper, bell ...... 0.025 Parts per Pepper, non-bell ...... 0.025 Commodity million Potato ...... 0.025 Pumpkin ...... 0.025 Beans, snap, succulent, except lima bean ...... 0 .01 Soybean ...... 0.05 Cotton, gin byproducts ...... 0 .02 Soybean, vegetable, succulent ...... 0.05 Cotton, undelinted seed ...... 0 .01 Squash, summer ...... 0.025 Peanut ...... 0 .01 Squash, winter ...... 0.025 Soybean, seed ...... 0 .01 Tomato ...... 0.025 Watermelon ...... 0.025 (b) Section 18 emergency exemptions. [Reserved] (b) Section 18 emergency exemptions. (c) Tolerances with regional registra- [Reserved] tions. Tolerances with regional reg- (c) Tolerances with regional registra- istration, as defined in § 180.1(l), are es- tions. [Reserved] tablished for residues of the herbicide (d) Indirect or inadvertent residues. lactofen, including its metabolites and [Reserved] degradates, in or on the commodities [71 FR 25951, May 3, 2006, as amended at 72 in the table in this paragraph. Compli- FR 52020, Sept. 12, 2007; 76 FR 12882, Mar. 9, ance with the tolerance levels specified 2011; 78 FR 65570, Nov. 1, 2013; 80 FR 9391, Feb. in this paragraph is to be determined 23, 2015] by measuring only lactofen, 2-ethoxy-1- methyl-2-oxoethyl 5-[2-chloro-4- § 180.434 Propiconazole; tolerances for (trifluoromethyl)phenoxy]-2- residues. nitrobenzoate, in or on the commodity. (a) General. Tolerances are estab- lished for residues of propiconazole, in- Parts per cluding its metabolites and degradates, Commodity million in or on the commodities in the table Okra ...... 0.02 below. Compliance with the tolerance Vegetables, fruiting, group 08 ...... 0 .02 levels specified below is to be deter- mined by measuring only those (d) Indirect or inadvertent residues. propiconazole residues convertible to [Reserved] 2,4-dichlorobenzoic acid (2,4–DCBA), ex- [69 FR 57216, Sept. 24, 2004, as amended at 72 pressed as the stoichiometric equiva- FR 33906, June 20, 2007; 76 FR 23496, Apr. 27, lent of propiconazole, in or on the com- 2011] modity in the table below:

§ 180.433 Fomesafen; tolerances for Commodity Parts per residues. million (a) General. Tolerances are estab- Almond, hulls ...... 7 .0 lished for residues of the herbicide Banana ...... 0.2 Barley, bran ...... 6 .0 fomesafen, including its metabolites Barley, grain ...... 3 .0 and degradates, in or on the following Barley, hay ...... 30 commodities. Compliance with the tol- Barley, straw ...... 20 Bean, dry seed ...... 0 .40 erance levels specified in the following Bean, snap ...... 0 .70 table below is to be determined by Bean, succulent shelled ...... 0 .10 measuring only fomesafen, 5-[2-chloro- Beet, garden, roots ...... 0 .30 4-(trifluoromethyl)phenoxy]-N- Beet, garden, tops ...... 5 .5 Beet, sugar, dried pulp ...... 1 .0 (methylsulfonyl)-2-nitrobenzamide, in Beet, sugar, molasses ...... 1 .5 or on the commodity. Beet, sugar, roots ...... 0 .3 Beet, sugar, tops ...... 10 Parts per Bushberry, subgroup 13–07B ...... 1.0 Commodity million Caneberry, subgroup 13–07A ...... 1 .0 Carrot, roots ...... 0.25 Bean, dry ...... 0.05 Cattle, fat ...... 0.05 Bean, lima, succulent ...... 0.05 Cattle, kidney ...... 2 .0 Bean, snap, succulent ...... 0.05 Cattle, liver ...... 2 .0 Cantaloupe ...... 0.025 Cattle, meat ...... 0 .05 Cotton, gin byproducts ...... 0.025 Cattle, meat byproducts, except liver and kidney 0.05 Cotton, undelinted seed ...... 0.025 Cilantro, leaves ...... 13

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Parts per Parts per Commodity million Commodity million

Citrus, oil ...... 1000 Vegetable, foliage of legume, group 7 ...... 30 Corn, field, forage ...... 12 Wheat, bran ...... 0.6 Corn, field, grain ...... 0 .2 Wheat, forage ...... 15 Corn, field, stover ...... 30 Wheat, grain ...... 0 .3 Corn, pop, grain ...... 0.2 Wheat, hay ...... 30 Corn, pop, stover ...... 30 Wheat, straw ...... 20 Corn, sweet, forage ...... 6 .0 Corn, sweet, kernel plus cob with husks re- (b) Section 18 emergency exemptions. moved ...... 0 .1 Corn, sweet, stover ...... 30 Time-limited tolerances are estab- Fruit, citrus, group 10–10 ...... 8 .0 lished for residues of propiconazole (1- Fruit, stone, group 12, except plum ...... 4 .0 [[2-(2,4-dichlorophenyl)-4-propyl-1,3- Goat, fat ...... 0 .05 Goat, kidney ...... 2 .0 dioxolan-2-yl] methyl]-1H-1,2,4-triazole) Goat, liver ...... 2.0 and its metabolites determined as 2,4- Goat, meat ...... 0.05 dichlorobenzoic acid and expressed as Goat, meat byproducts, except liver and kidney 0 .05 Grain, aspirated fractions ...... 110 parent compound, in connection with Grass, forage ...... 0 .5 use of the pesticide under section 18 Grass, hay ...... 0 .5 emergency exemptions granted by Grass, straw ...... 40 EPA. The tolerances will expire and Hog, kidney ...... 0.2 Hog, liver ...... 0 .2 are revoked on the dates specified in Horse, fat ...... 0 .05 the following table: Horse, kidney ...... 2 .0 Horse, liver ...... 2 .0 Parts per Expiration/ Horse, meat ...... 0 .05 Commodity million revocation Horse, meat byproducts, except liver and kidney 0 .05 date Leaf petioles subgroup 4B ...... 5 .0 Low growing berry subgroup 13–07G, except Avocado ...... 10 12/31/16 cranberry ...... 1 .3 Nectarine ...... 2.0 12/31/13 Milk ...... 0.05 Peach ...... 2.0 12/31/13 Mushroom ...... 0 .1 Nut, tree, group 14 ...... 0 .1 (c) Tolerances with regional registra- Oat, forage ...... 4 .0 tions. A tolerance with regional reg- Oat, grain ...... 3 .0 Oat, hay ...... 15 istration, as defined in § 180.1(l), is es- Oat, straw ...... 10 tablished for residues of 1-[[2-(2,4- Onion, bulb subgroup 3–07A ...... 0.2 dichlorophenyl)-4-propyl-1,3-dioxolan-2- Onion, green, subgroup 3–07B ...... 9 .0 yl]methyl]-1H-1,2,4-triazole and its me- Parsley, fresh leaves ...... 13 Parsley, dried leaves ...... 35 tabolites determined as 2,4- Peanut ...... 0 .2 dichlorobenzoic acid and expressed as Peanut, hay ...... 20 parent compound, in or on the fol- Peppermint, tops ...... 10 .0 Pineapple ...... 4.5 lowing commodities: Pineapple, process residue ...... 7 .0 Pistachio ...... 0.1 Commodity Parts per Plum ...... 0 .60 million Rapeseed subgroup 20A ...... 0 .30 Cranberry ...... 1 .0 Rice, bran ...... 15 Rice, wild, grain ...... 0.5 Rice, grain ...... 7 .0 Rice, hulls ...... 20 Rice, straw ...... 18 (d) Indirect or inadvertent residues. Rye, bran ...... 0 .6 Tolerances are established for the com- Rye, forage ...... 9 .0 bined residues of the fungicide 1-[[2- Rye, grain ...... 0.3 Rye, straw ...... 10 (2,4-dichlorophenyl)-4-propyl-1,3- Sheep, fat ...... 0 .05 dioxolan-2-yl] methyl]-1H-1,2,4-triazole Sheep, kidney ...... 2.0 and its metabolites determined as 2,4- Sheep, liver ...... 2.0 Sheep, meat ...... 0.05 dichlorobenzoic acid and expressed as Sheep, meat byproducts, except liver and kid- parent compound in or on the following ney ...... 0.05 commodities when present therein as a Sorghum, grain, forage ...... 12 result of application of propiconazole Sorghum, grain, grain ...... 3 .5 Sorghum, grain, stover ...... 15 to growing crops in paragraphs (a) and Soybean, forage ...... 11 (c) of this section: Soybean, hay ...... 30 Soybean, seed ...... 2 .0 Commodity Parts per Spearmint, tops ...... 10 .0 million Sugarcane, cane ...... 0.4 Tomato ...... 3.0 Alfalfa, forage ...... 0.1

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Parts per Parts per Commodity million Commodity million

Alfalfa, hay ...... 0.1 Hog, fat ...... 0 .05 Horse, fat ...... 0 .05 Horse, meat ...... 0 .02 [71 FR 55306, Sept. 22, 2006, as amended at 72 Horse, meat byproducts ...... 0 .05 FR 20439, Apr. 25, 2007; 74 FR 12613, Mar. 25, Lychee* ...... 0 .2 2009; 75 FR 80346, Dec. 22, 2010; 76 FR 27268, Milk, fat (reflecting 0.02 ppm in whole milk) ...... 0 .1 May 11, 2011; 77 FR 38204, June 27, 2012; 77 FR Nut, tree, Group 14 ...... 0.1 75044, Dec. 19, 2012; 78 FR 23503, Apr. 19, 2013; Onion, bulb ...... 0 .1 78 FR 78748, Dec. 27, 2013; 79 FR 18467, Apr. 2, Onion, green ...... 1 .5 2014] Poultry, fat ...... 0.05 Poultry, meat ...... 0 .02 Poultry, meat byproducts ...... 0.02 § 180.435 Deltamethrin; tolerances for Radish, tops ...... 4 .0 residues. Rapeseed ...... 0 .2 (a) General. (1) Tolerances are estab- Rice, hulls ...... 2 .5 Rye, bran ...... 5 .0 lished for residues of deltamethrin, in- Sheep, fat ...... 0 .05 cluding its metabolites and degradates, Sheep, meat ...... 0.02 in or on the commodities listed in the Sheep, meat byproducts ...... 0 .05 following table. Compliance with the Sorghum, grain, forage ...... 0.5 Sorghum, grain, stover ...... 1 .0 tolerance levels specified is to be deter- Soybean, seed ...... 0 .1 mined by measuring only Soybean, hulls ...... 0 .2 deltamethrin, (1R,3R)-3-(2,2- Starfruit* ...... 0.2 dibromovinyl)-2,2- Sunflower, seed ...... 0.1 Tomato ...... 0.2 dimethylcyclopropanecarboxylic acid Tomato, paste ...... 1 .0 (S)-alpha-cyano-3-phenoxybenzyl ester, Tomato, puree ...... 1 .0 and its major metabolites, trans- Vegetable, cucurbit, Group 9 ...... 0 .2 deltamethrin, (S)-alpha-cyano-m- Vegetable, fruiting, Group 8 ...... 0 .3 Vegetable, root, except sugar beet, Subgroup IB 0 .2 phenoxybenzyl(1R,3S)-3-(2,2- Vegetable, tuberous and corm, Subgroup IC ..... 0 .04 dibromovinyl)-2,2- Wheat, bran ...... 5.0 dimethylcyclopropanecarboxylate, and *There are no U.S. registrations for use of deltamethrin on alpha-R-deltamethrin, (R)-alpha-cyano- starfruit and lychee. m-phenoxybenzyl-(1R,3R)-3-(2,2- (2) A tolerance of 0.05 ppm is estab- dibromovinyl)-2,2- lished for residues of the insecticide dimethylcyclopropanecarboxylate, in deltamethrin, including its metabolites or on the commodity. and degradates, in or on all food/feed Parts per items (other than those covered by a Commodity million higher tolerance as a result of use on growing crops) when deltamethrin is Almond, hulls ...... 2 .5 Apple, wet pomace ...... 1 .0 used in food/feed handling establish- Artichoke, globe ...... 0.5 ments or as a wide-area mosquito Barley, bran ...... 5 .0 adulticide. Compliance with the toler- Cattle, fat ...... 0.05 Cattle, meat ...... 0 .02 ance levels specified is to be deter- Cattle, meat byproducts ...... 0.05 mined by measuring only Corn, field, forage ...... 0 .7 deltamethrin, (1R,3R)-3-(2,2- Corn, field, refined oil ...... 2 .5 Corn, field, stover ...... 5 .0 dibromovinyl)-2,2- Corn, pop, stover ...... 5.0 dimethylcyclopropanecarboxylic acid Corn, sweet, forage ...... 10 (S)-alpha-cyano-3-phenoxybenzyl ester, Corn, sweet, kernel plus cob with husks re- moved ...... 0 .03 and its major metabolites, trans- Corn, sweet, stover ...... 15 deltamethrin, (S)-alpha-cyano-m- Cotton, refined oil ...... 0.2 phenoxybenzyl(1R,3S)-3-(2,2- Cotton, undelinted seed ...... 0 .04 Egg ...... 0 .02 dibromovinyl)-2,2- Fish—freshwater finfish ...... 0.01 dimethylcyclopropanecarboxylate, and Fish—freshwater finfish, farm raised ...... 0 .01 alpha-R-deltamethrin, (R)-alpha-cyano- Fish—saltwater finfish, other ...... 0 .01 m-phenoxybenzyl-(1R,3R)-3-(2,2- Fish—saltwater finfish, tuna ...... 0 .01 Fruit, pome, Group 11 ...... 0 .2 dibromovinyl)-2,2- Goat, fat ...... 0 .05 dimethylcyclopropanecarboxylate, in Goat, meat ...... 0.02 or on the commodity. Goat, meat byproducts ...... 0 .05 Grain, aspirated fractions ...... 65 (b) Section 18 emergency exemptions. Grain, cereal, Group 15, except sweet corn ...... 1 .0 [Reserved]

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(c) Tolerances with regional registra- Commodity Parts per tions. [Reserved] million (d) Indirect or inadvertent residues. Hog, meat byproducts ...... 0 .01 [Reserved] Hop, dried cones ...... 20 .0 Hop, vines ...... 4 .0 [62 FR 63001, Nov. 26, 1997, as amended at 63 Horse, fat ...... 2 .0 FR 45414, Aug. 26, 1998; 69 FR 62614, Oct. 27, Horse, meat ...... 0 .05 2004; 74 FR 46375, Sept. 9, 2009; 76 FR 34885, Horse, meat byproducts ...... 0 .05 June 15, 2011; 79 FR 66301, Nov. 7, 2014; 80 FR Lettuce, head ...... 2.0 16302, Mar. 27, 2015] Lettuce, leaf ...... 3 .0 Milk ...... 0.2 Milk, fat ...... 5 .0 § 180.436 Cyfluthrin and the isomer Millet, grain ...... 0 .15 beta-cyfluthrin; tolerances for resi- Mustard greens ...... 7.0 dues. Nut, tree, group 14 ...... 0 .01 Oat, bran ...... 0 .5 (a) General. (1) Tolerances are estab- Oat, grain ...... 0 .15 lished for residues of the insecticide Pea and bean, dried shelled, except soybean, cyfluthrin (cyano(4-fluoro-3- subgroup 6C ...... 0 .15 Pea, dry, seed ...... 0 .15 phenoxyphenyl)methyl-3-(2,2- Pea, southern, succulent ...... 0 .25 dichloroethenyl)-2,2dimethyl- Peanut ...... 0 .01 cyclopropane-carboxylate; CAS No. Peanut, hay ...... 6.0 Pepper ...... 0 .50 68359–37–5) in or on the following raw Pistachio ...... 0.01 agricultural commodities: Poultry, fat ...... 0.01 Poultry, meat ...... 0 .01 Poultry, meat byproducts ...... 0.01 Commodity Parts per million Radish, roots ...... 1 .0 Rye, bran ...... 0 .5 Alfalfa ...... 5 .0 Rye, grain ...... 0.15 Alfalfa, forage ...... 5.0 Sheep, fat ...... 2 .0 Alfalfa, hay ...... 13 Sheep, meat ...... 0.05 Almond, hulls ...... 0 .5 Sheep, meat byproducts ...... 0 .05 Barley, bran ...... 0 .5 Sorghum, grain, grain ...... 3 .5 Barley, grain ...... 0 .15 Soybean, forage ...... 8 .0 Beet, sugar, dried pulp ...... 1 .0 Soybean, hay ...... 4 .0 Beet, sugar, roots ...... 0 .10 Soybean, seed ...... 0 .03 Brassica, head and stem, subgroup 5A ...... 2 .5 Sugarcane, cane ...... 0.05 Brassica, leafy greens, subgroup 5B ...... 7 .0 Sugarcane, molasses ...... 0 .20 Buckwheat, grain ...... 0.15 Sunflower, forage ...... 5.0 Carrot, roots ...... 0.20 Sunflower, seed ...... 0.02 Cattle, fat ...... 2.0 Teosinte, grain ...... 0 .05 Cattle, meat ...... 0 .10 Tomato ...... 0.20 Cattle, meat byproducts ...... 0.10 Tomato, dry pomace ...... 5.0 Citrus, dried pulp ...... 0 .3 Tomato, paste ...... 0 .5 Citrus, oil ...... 0.3 Tomato, wet pomace ...... 5.0 Corn, field, grain ...... 0 .05 Triticale, grain ...... 0 .15 Corn, pop, grain ...... 0.05 Turnip, greens ...... 7.0 Corn, sweet, kernel plus cob with husks re- Vegetable, cucurbit, group 9 ...... 0.1 moved ...... 0 .05 Vegetable, fruiting, group 8 ...... 0.5 Cotton, hulls ...... 2 .0 Vegetable, leafy, except brassica, group 4 ...... 6 .0 Cotton, refined oil ...... 2.0 Vegetable, tuberous and corm, subgroup 1C ..... 0.01 Cotton, undelinted seed ...... 1 .0 Egg ...... 0 .01 Wheat, bran ...... 0.5 Fruit, citrus, group 10 ...... 0 .2 Wheat, grain ...... 0 .15 Fruit, pome, group 11 ...... 0.5 Wheat, shorts ...... 0 .5 Fruit, stone, group 12 ...... 0 .3 Goat, fat ...... 2 .0 (2) A tolerance of 0.05 ppm is estab- Goat, meat ...... 0.05 lished for residues of the insecticide Goat, meat byproducts ...... 0 .05 Grain, aspirated fractions ...... 150 cyfluthrin (cyano(4-fluoro-3- Grain, cereal, forage, fodder and hay, group 16, phenoxyphenyl)methyl-3-(2,2- forage, except rice ...... 25 dichloroethenyl)-2,2- Grain, cereal, forage, fodder and hay, group 16, hay, except rice ...... 6 .0 dimethylcyclopropanecarboxylate; Grain, cereal, forage, fodder and hay, group 16, CAS Reg. No. 69359–37–5) in food com- stover, except rice ...... 30 modities exposed to the insecticide Grain, cereal, forage, fodder and hay, group 16, during treatment of food-handling es- straw, except rice ...... 7 .0 Grape ...... 1 .0 tablishments where food and food prod- Grape, raisin ...... 3 .5 ucts are held, processed, prepared, or Grass, forage, fodder and hay, group 17, forage 12 served. Treatments may be made by Grass, forage, fodder and hay, group 17, hay .... 50 Hog, fat ...... 0 .5 general surface, spot, and/or crack and Hog, meat ...... 0 .01 crevice applications.

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(i) General surface treatments shall (ii) Crack and crevice or spot treat- be limited to a maximum of 3.8 grams ments shall be limited to a maximum of active ingredient per 1,000 square of 0.1 percent of the active ingredient feet, applying to walls, floors, and ceil- by weight, applied with a low-pressure ings with a low-pressure system. Cover system with a pinpoint or variable-pat- or remove all food processing and/or tern nozzle. Dust formulation shall be handling equipment during applica- limited to a maximum of 0.1 percent of tion. Do not apply directly to food the active ingredient by weight, ap- products. Reapplications may be made plied using a hand duster, power dust- at 10-day intervals. er, or other equipment capable of ap- (ii) Crack and crevice or spot treat- plying dust insecticide directly into ments shall be limited to a maximum voids and cracks and crevices. Dust ap- of 0.1 percent of the active ingredient plications should be made in a manner weight, applied with a low-pressure to avoid deposits on exposed surfaces system with a pinpoint or variable-pat- or introducing the material into the tern nozzle. Dust formulation shall be air. Cover exposed feed or remove feed limited to a maximum of 0.1 percent of from premises. Do not apply directly to the active ingredient by weight, ap- feed. Reapplications may be made at plied using a hand duster, power dust- 10-day intervals. er, or other equipment capable of ap- (iii) To ensure safe use of the insecti- plying dust insecticide directly into cide, its label and labeling shall con- voids and cracks and crevices. Dust ap- form to that registered by EPA, and it plications should be made in a manner shall be used in accordance with such to avoid deposits on exposed surfaces label and labeling. or introducing the material into the (4) Tolerances are established for res- air. Cover exposed food or remove food idues of the isomer, beta-cyfluthrin, from premises. Do not apply directly to cyano(4-fluoro-3- food. Reapplications may be made at phenoxyphenyl)methyl-3-(2,2- 10-day intervals. dichloroethenyl)-2,2-dimethyl- (iii) To ensure safe use of the insecti- cyclopropanecarboxylate [mixture cide, its label and labeling shall con- comprising the enantiomeric pair (R)- form to that registered by the Environ- a-cyano-4-fluoro-3-phenoxybenzyl mental Protection Agency, and it shall (1S,3S)-3-(2,2-dichlorovinyl)-2,2- be used in accordance with such label dimethylcyclopropanecarboxylate and and labeling. (S)-a-cyano-4-fluoro-3-phenoxybenzyl (3) A tolerance of 0.05 part per mil- (1R,3R)-3-(2,2-dichlorovinyl)-2,2- lion is established for residues of the dimethylcyclopropanecarboxylate with insecticide cyfluthrin (cyano(4-fluoro- the enantiomeric pair (R)-a-cyano-4- 3-phenoxyphenyl)methyl-3-(2,2- fluoro-3-phenoxybenzyl (1S,3R)-3-(2,2- dichloroethenyl)-2,2- dichlorovinyl)-2,2- dimethylcyclopropanecarboxylate; dimethylcyclopropanecarboxylate and CAS Reg. No. 68359–37–5) in feed com- (S)-a-cyano-4-fluoro-3-phenoxybenzyl modities exposed to the insecticide (1R,3S)-3-(2,2-dichlorovinyl)-2,2- during treatment of feed-handling es- dimethylcyclopropanecarboxylate], in tablishments where feed and feed prod- or on the following raw agricultural ucts are held, processed, prepared, or commodities: served. Treatments may be made by Parts per general surface, spot, and/or crack and Commodity million crevice applications. (i) General surface tratments shall be Alfalfa ...... 5 .0 Alfalfa, forage ...... 5.0 limited to a maximum of 3.8 grams of Alfalfa, hay ...... 13 active ingredient per 1,000 square feet, Almond, hulls ...... 0 .5 applying to walls, floors, and ceilings Barley, bran ...... 0 .5 Barley, grain ...... 0 .15 with a low-pressure system. Cover or Beet, sugar, dried pulp ...... 1 .0 remove all feed processing and/or han- Beet, sugar, roots ...... 0 .10 dling equipment during application. Do Brassica, head and stem, subgroup 5A ...... 2 .5 not apply directly to feed products. Re- Brassica, leafy greens, subgroup 5B ...... 7 .0 Buckwheat, grain ...... 0.15 applications may be made at 10-day in- Carrot, roots ...... 0.20 tervals. Cattle, fat ...... 2.0

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Parts per Parts per Commodity million Commodity million

Cattle, meat ...... 0 .10 Teosinte, grain ...... 0 .05 Cattle, meat byproducts ...... 0.10 Tomato ...... 0.20 Citrus, dried pulp ...... 0 .3 Tomato, paste ...... 0 .5 Citrus, oil ...... 0.3 Tomato, pomace ...... 5 .0 Corn, field, grain ...... 0 .05 Triticale, grain ...... 0 .15 Corn, pop, grain ...... 0.05 Turnip, greens ...... 7.0 Corn, sweet, kernel plus cob with husks re- Vegetable, cucurbit, group 9 ...... 0.1 moved ...... 0 .05 Vegetable, fruiting, group 8 ...... 0.5 Cotton, hulls ...... 2 .0 Vegetable, leafy greens, except Brassica, group Cotton, refined oil ...... 2.0 4 ...... 6 .0 Cotton, undelinted seed ...... 1 .0 Vegetable, tuberous and corm, subgroup 1C ..... 0.01 Egg ...... 0 .01 Wheat, bran ...... 0.5 Fruit, citrus, group 10 ...... 0 .2 Wheat, grain ...... 0 .15 Fruit, pome, group 11 ...... 0.5 Wheat, shorts ...... 0 .5 Fruit, stone, group 12 ...... 0 .3 Goat, fat ...... 2 .0 (b) Section 18 emergency exemptions. Goat, meat ...... 0.05 Goat, meat byproducts ...... 0 .05 [Reserved] Grain, aspirated fractions ...... 150 (c) Tolerances with regional registra- Grain, cereal, forage, fodder and hay, group 16, tions. [Reserved] forage, except rice ...... 25 Grain, cereal, forage, fodder and hay, group 16, (d) Indirect or inadvertent residues. hay, except rice ...... 6 .0 [Reserved] Grain, cereal, forage, fodder and hay, group 16, stover, except rice ...... 30 [53 FR 1924, Jan. 25, 1988] Grain, cereal, forage, fodder and hay, group 16, EDITORIAL NOTE: For FEDERAL REGISTER ci- straw, except rice ...... 7 .0 Grape ...... 1 .0 tations affecting § 180.436, see the List of CFR Grape, raisin ...... 3 .5 Sections Affected, which appears in the Grass, forage, fodder and hay, group 17, forage 12 Finding Aids section of the printed volume Grass, forage, fodder and hay, group 17, hay .... 50 and at www.fdsys.gov. Hog, fat ...... 0 .5 Hog, meat ...... 0 .01 § 180.437 Methyl 2-(4-isopropyl-4-meth- Hog, meat byproducts ...... 0 .01 yl-5-oxo-2-imidazolin-2-yl)-p-toluate Hop, dried cones ...... 20 .0 Hop, vines ...... 4 .0 and methyl 6-(4-isopropyl-4-methyl- Horse, fat ...... 2 .0 5-oxo-2-imidazolin-2-yl)-m-toluate; Horse, meat ...... 0 .05 tolerances for residues. Horse, meat byproducts ...... 0 .05 Lettuce, head ...... 2.0 Tolerances are established for the Lettuce, leaf ...... 3 .0 combined residues of the herbicide Milk ...... 0.2 methyl 2-(4-isopropyl-4-methyl-5-oxo-2- Milk, fat ...... 5 .0 imidazolin-2-yl)-p-toluate and methyl Millet, grain ...... 0 .15 Mustard greens ...... 7.0 6-(4-isopropyl-4-methyl-5-oxo-2- Nut, tree, group 14 ...... 0 .01 imidazolin-2-yl)-m-toluate in or on the Oat, bran ...... 0 .5 following raw agricultural commod- Oat, grain ...... 0 .15 Pea and bean, dried shelled, except soybean, ities: subgroup 6C ...... 0 .15 Pea, dry, seed ...... 0 .15 Parts per Commodity million Pea, southern, succulent ...... 0 .25 Peanut ...... 0 .01 Barley, grain ...... 0 .10 Peanut, hay ...... 6.0 Barley, straw ...... 2 .00 Pepper ...... 0 .50 Sunflower, seed ...... 0.10 Pistachio ...... 0.01 Wheat, grain ...... 0 .10 Poultry, fat ...... 0.01 Wheat, straw ...... 2 .00 Poultry, meat ...... 0 .01 Poultry, meat byproducts ...... 0.01 Radish, roots ...... 1 .0 [53 FR 24069, June 27, 1988] Rye, bran ...... 0 .5 Rye, grain ...... 0.15 Sheep, fat ...... 2 .0 § 180.438 Lambda-cyhalothrin and an Sheep, meat ...... 0.05 isomer gamma-cyhalothrin; toler- Sheep, meat byproducts ...... 0 .05 ances for residues. Sorghum, grain, grain ...... 3 .5 (a) General. (1) Tolerances are estab- Soybean, forage ...... 8 .0 Soybean, hay ...... 4 .0 lished for the combined residues of the Soybean, seed ...... 0 .03 lambda-cyhalothrin, 1:1 Sugarcane, cane ...... 0.05 mixture of (S)-a-cyano-3- Sugarcane, molasses ...... 0 .20 Sunflower, forage ...... 5.0 phenoxybenzyl-(Z)-(1R,3R)-3-(2-chloro- Sunflower, seed ...... 0.02 3,3,3-trifluoroprop-1-enyl)-2,2-

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dimethylcyclopropanecarboxylate and Commodity Parts per (R)-a-cyano-3-phenoxybenzyl-(Z)- million (1S,3S)-3-(2-chloro-3,3,3-trifluoroprop-1- Onion, bulb ...... 0 .1 enyl)-2,2- Pea and bean, dried shelled, except soybean, dimethylcyclopropanecarboxylate and subgroup 6C ...... 0 .10 Pea and bean, succulent shelled, subgroup 6B 0 .01 its epimer expressed as epimer of lamb- Peanut ...... 0 .05 da-cyhalothrin, a 1:1 mixture of (S)-a- Peanut, hay ...... 3.0 cyano-3-phenoxybenzyl-(Z)-(1S,3S)-3-(2- Pistachio ...... 0.05 Poultry, fat ...... 0.03 chloro-3,3,3-trifluoroprop-1-enyl)-2,2- Poultry, meat ...... 0 .01 dimethylcyclopropanecarboxylate and Poultry, meat byproducts ...... 0.01 (R)-a-cyano-3-phenoxybenzyl-(Z)- Rice, grain ...... 1 .0 Rice, hulls ...... 5 .0 (1R,3R)-3-(2-chloro-3,3,3-trifluoroprop-1- Rice, straw ...... 1 .8 enyl)-2,2- Rice, wild, grain ...... 1.0 dimethylcyclopropanecarboxylate, on Rye, bran ...... 0 .2 Rye, grain ...... 0.05 plants and livestocks, as indicated in Rye, forage ...... 2 .0 the following table. Rye, straw ...... 2 .0 Sheep, fat ...... 3 .0 Commodity Parts per Sheep, meat ...... 0.2 million Sheep, meat byproducts ...... 0 .2 Soybean ...... 0.01 Alfalfa, forage ...... 5.0 Sorghum, grain, grain ...... 0 .2 Alfalfa, hay ...... 6.0 Sorghum, grain, forage ...... 0.30 Almond, hulls ...... 1 .5 Sorghum, grain, stover ...... 0 .50 Apple, wet pomace ...... 2 .50 Sugarcane, cane ...... 0.05 Avocado, imported ...... 0.20 Sunflower, forage ...... 0.2 Barley, bran ...... 0 .2 Sunflower, seed, hulls ...... 0 .50 Barley, grain ...... 0 .05 Sunflower, refined oil ...... 0.30 Barley, hay ...... 2 .0 Sunflower, seed ...... 0.2 Barley, straw ...... 2 .0 Tomato ...... 0.1 Brassica, head and stem, subgroup 5A ...... 0 .4 Tomato, dry pomace ...... 6.0 Buckwheat, grain ...... 0.05 Tomato, wet pomace ...... 6.0 Canola, refined oil ...... 2 .0 Vegetable, cucurbit, group 9 ...... 0.05 Canola, seed ...... 1 .0 Vegetable, fruiting, group 8 ...... 0.20 Cattle, fat ...... 3.0 Vegetable, legume, edible podded, subgroup 6A 0 .20 Cattle, meat ...... 0 .2 Vegetable, tuberous and corm, subgroup 1C ..... 0.02 Cattle, meat byproducts ...... 0.2 Wheat, grain ...... 0 .05 Corn, field, flour ...... 0 .15 Wheat, forage ...... 2 .0 Corn, field, forage ...... 6 .0 Wheat, hay ...... 2 .0 Corn, field, grain ...... 0 .05 Wheat, straw ...... 2 .0 Corn, field, stover ...... 1 .0 Wheat, bran ...... 0.2 Corn, pop, grain ...... 0.05 Corn, pop, grain, flour ...... 0 .05 1 Corn, pop, stover ...... 1.0 (2) Tolerances are established for Corn, sweet, forage ...... 6 .0 the combined residues of the Corn, sweet, stover ...... 1 .0 pyrethroid [gamma-cyhalothrin (the Corn, sweet, kernel plus cob with husks re- moved ...... 0 .05 isolated active isomer of lambda- Cotton, undelinted seed ...... 0 .05 cyhalothrin) (S)-′-cyano-3- Egg ...... 0 .01 phenoxybenzyl (Z)-(1R,3R)-3-(2-chloro- Fruit, pome, group 11 ...... 0.30 3,3,3-trifluoroprop-1-enyl)-2,2- Fruit, stone, group 12 ...... 0 .50 Garlic ...... 0 .1 dimethylcyclopropanecarboxylate)) Goat, fat ...... 3 .0 and its epimer (R)-′-cyano-3- Goat, meat ...... 0.2 phenoxybenzyl (Z)-(1R,3R)-3-(2-chloro- Goat, meat byproducts ...... 0 .2 Grain, aspirated fractions ...... 2 .0 3,3,3-trifluoroprop-1-enyl)-2,2- Grass, forage, fodder and hay, group 17 ...... 7 .0 dimethylcyclopropanecarboxylate in/ Hog, fat ...... 0 .2 on the following commodities: Hog, meat ...... 0 .01 Hog, meat byproducts ...... 0 .02 Parts per Hop, dried cones ...... 10 .0 Commodity million Horse, fat ...... 3 .0 Horse, meat ...... 0 .2 Alfalfa, forage ...... 5 Horse, meat byproducts ...... 0 .2 Alfalfa, hay ...... 6 Lettuce, head ...... 2.0 Almond, hulls ...... 1 .5 Lettuce, leaf ...... 2 .0 Apple, pomace, wet ...... 2 .50 Milk, fat (reflecting 0.4 ppm in whole milk) ...... 10 .0 Avocado, imported ...... 0.20 Nut, tree, group 14 ...... 0 .05 Brassica, head and stem, subgroup 5A ...... 0 .4 Oat, grain ...... 0 .05 Canola, seed ...... 0 .15 Oat, forage ...... 2 .0 Cattle, fat ...... 3 Oat, hay ...... 2.0 Cattle, meat ...... 0 .2 Oat, straw ...... 2.0 Cattle, meat byproducts ...... 0.2

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food commodities (other than those al- Commodity Parts per million ready covered by a higher tolerance as Corn, field, flour ...... 0 .15 a result of use on growing crops) in Corn, field, forage ...... 6 .0 food-handling establishments where Corn, field, grain ...... 0 .05 food products are held, processed, or Corn, field, stover ...... 1 .0 Corn, pop, grain ...... 0.05 prepared. Corn, pop, stover ...... 1.0 (b) Section 18 emergency exemptions. Corn, sweet, forage ...... 6 .0 [Reserved] Corn, sweet, kernel plus cob with husks re- moved ...... 0 .05 (c) Tolerances with regional registra- Corn, sweet, stover ...... 1 .0 tions. [Reserved] Cotton, undelinted seed ...... 0 .05 (d) Indirect or inadvertent residues. Egg ...... 0 .01 Fruit, pome, group 11 ...... 0.30 [Reserved] Fruit, stone, group 12 ...... 0 .50 Garlic ...... 0 .10 [71 FR 74817, Dec. 13, 2006, as amended at 72 Goat, fat ...... 3 .0 FR 45663, Aug. 15, 2007; 73 FR 39264, July 9, Goat, meat ...... 0.2 2008; 76 FR 34885, June 15, 2011] Goat, meat byproducts ...... 0 .2 Grain, aspirated fractions ...... 2 .0 § 180.439 Thifensulfuron methyl; toler- Hog, fat ...... 3 .0 Hog, meat ...... 0 .2 ances for residues. Hog, meat byproducts ...... 0 .2 (a) General. Tolerances are estab- Horse, fat ...... 3 .0 Horse, meat ...... 0 .2 lished for residues of thifensulfuron Horse, meat byproducts ...... 0 .2 methyl, including its metabolites and Lettuce, head ...... 2.0 degradates, in or on the commodities Lettuce, leaf ...... 2 .0 Milk, fat (reflecting 0.20 ppm in whole milk) ...... 5 .0 listed in the following table [below]. Nut, tree, group 14 ...... 0 .05 Compliance with the tolerance levels Okra ...... 0.20 specified in the following table [below] Onion, bulb ...... 0 .1 Pea and bean, dried shelled, except soybean, is to be determined by measuring only subgroup 6C ...... 0 .10 thifensulfuron methyl (methyl 3-[[[[(4- Pea and bean, succulent shelled, subgroup 6B 0 .01 methoxy-6-methyl-1,3,5-triazin-2- Peanut ...... 0 .05 yl)amino]carbonyl]amino] sulfonyl]-2- Peanut, hay ...... 3.0 Pistachio ...... 0.05 thiophenecarboxylate). Poultry, fat ...... 0.03 Poultry, meat ...... 0 .01 Commodity Parts per Poultry, meat byproducts ...... 0.01 million Rice, grain ...... 1 .0 Rice, hulls ...... 5 .0 Barley, grain ...... 0 .05 Rice, straw ...... 1 .8 Barley, hay ...... 0 .8 Sheep, fat ...... 3 .0 Barley, straw ...... 0 .10 Sheep, meat ...... 0.2 Canola, seed ...... 0 .02 Sheep, meat byproducts ...... 0 .2 Chicory, roots ...... 0 .01 Sorghum, grain, forage ...... 0.30 Chicory, tops ...... 0 .01 Sorghum, grain, grain ...... 0 .20 Corn, field, forage ...... 0 .10 Sorghum, grain, stover ...... 0 .50 Corn, field, grain ...... 0 .05 Soybean ...... 0.01 Corn, field, stover ...... 0 .10 Sugarcane ...... 0 .05 Cotton, gin byproducts ...... 0 .02 Sunflower, forage ...... 0.20 Cotton, undelinted seed ...... 0 .02 Sunflower, refined oil ...... 0.30 Flax, seed ...... 0 .02 Sunflower, seed ...... 0.20 Oat, forage ...... 0 .2 Sunflower, seed, hulls ...... 0 .50 Oat, grain ...... 0 .05 Tomato ...... 0.10 Oat, hay ...... 0.05 Tomato, dry pomace ...... 6.0 Oat, straw ...... 0.10 Tomato, wet pomace ...... 6.0 Rice, grain ...... 0 .05 Vegetables, fruiting, group 8 ...... 0.20 Rice, straw ...... 0 .05 Vegetable, legume, edible podded, subgroup 6A 0 .20 Sorghum, grain, forage...... 0 .05 Wheat, bran ...... 2.0 Sorghum, grain, grain ...... 0 .05 Wheat, forage ...... 2 .0 Sorghum, grain, stover ...... 0 .05 Wheat, grain ...... 0 .05 Soybean ...... 0.10 Wheat, hay ...... 2 .0 Wheat, straw ...... 2 .0 Wheat, forage ...... 2 .5 Wheat, grain ...... 0 .05 1 The analytical enforcement methods for lambda- Wheat, hay ...... 0 .7 cyhalothrin are applicable for determination of gamma- Wheat, straw ...... 0 .10 cyhalothrin residues in plant and animal commodities. (3) A tolerance of 0.01 part per mil- (b) Section 18 emergency exemptions. lion is established for residues of the [Reserved] insecticide lamba-cyhalothrin and an (c) Tolerances with regional registra- isomer gamma-cyhalothrin in or on all tions. Tolerances are established for

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residues of thifensulfuron methyl, in- § 180.441 Quizalofop ethyl; tolerances cluding its metabolites and degradates, for residues. in or on the commodities listed in the (a) General. (1) Tolerances are estab- following table [below]. Compliance lished for residues of the herbicide with the tolerance levels specified in quizalofop ethyl, including its metabo- the following table [below] is to be de- lites and degradates, in or on the com- termined by measuring only modities in the following table. Com- thifensulfuron methyl (methyl 3-[[[[(4- pliance with the tolerance levels speci- methoxy-6-methyl-1,3,5-triazin-2- fied in the following table is to be de- yl)amino]carbonyl]amino] sulfonyl]-2- termined by measuring only those thiophenecarboxylate). quizalofop ethyl residues convertible to 2-methoxy-6-chloroquinoxaline, ex- Commodity Parts per pressed as the stoichiometric equiva- million lent of quizalofop ethyl, in or on the Safflower, seed ...... 0 .05 commodity.

Parts per (d) Indirect or inadvertent residues. Commodity million [Reserved] Barley, grain ...... 0 .05 [69 FR 55982, Sept. 17, 2004, as amended at 69 Barley, hay ...... 0 .05 Barley, straw ...... 0 .05 FR 63957, Nov. 3, 2004; 72 FR 13184, Mar. 21, Bean, dry, seed ...... 0 .4 2007; 73 FR 47075, Aug. 13, 2008; 75 FR 19277, Bean, succulent ...... 0 .25 Apr. 14, 2010; 77 FR 52240, Aug. 29, 2012] Beet, sugar, molasses ...... 0 .2 Beet, sugar, roots ...... 0 .1 Beet, sugar, tops ...... 0.5 § 180.440 Tefluthrin; tolerances for res- Cotton, undelinted seed ...... 0 .1 idues. Cowpea, forage ...... 3 .0 Cowpea, hay ...... 3 .0 (a) General. Tolerances are estab- Crambe, meal ...... 2 .0 lished for the combined residues of the Flax, seed ...... 0 .05 insecticide tefluthrin (2,3,5,6 Gold of pleasure, meal ...... 2.0 Lentil, seed ...... 0 .05 tetrafluroro-4-methylphenyl)methyl-(1 Pea, dry ...... 0 .25 alpha, 3 alpha)-(Z)-(±)-3(2-chloro-3,3,3- Pea, field, hay ...... 3.0 Pea, field, vines ...... 3 .0 trifluoro-1-propenyl)-2,2- Pea, succulent ...... 0 .3 diemthylcyclopropanecarboxylate) and Peppermint, tops ...... 2 .0 its metabolite (Z)-3-(2-chloro-3,3,3- Rapeseed, meal ...... 2 .0 Rapeseed subgroup 20A, except flax, seed ...... 1 .5 trifluroro-1-propenyl)-2,2- Sorghum, grain, aspirated grain fractions ...... 1 .0 dimethylcyclopropanecarboxylic acid Sorghum, grain, forage ...... 0.20 in or on the following commodities: Sorghum, grain, grain ...... 0 .20 Sorghum, grain, stover ...... 0 .30 Soybean, flour ...... 0 .5 Commodity Parts per Soybean, hulls ...... 0 .02 million Soybean, meal ...... 0.5 Soybean, seed ...... 0 .05 Corn, field, forage ...... 0 .06 Soybean, soapstock ...... 1 .0 Corn, field, grain ...... 0 .06 Spearmint, tops ...... 2 .0 Corn, field, stover ...... 0 .06 Sunflower, seed ...... 1.9 Corn, pop, grain ...... 0.06 Wheat, forage ...... 0 .05 Corn, pop, stover ...... 0.06 Wheat, grain ...... 0 .05 Corn, sweet, forage ...... 0 .06 Wheat, hay ...... 0 .05 Wheat, straw ...... 0 .05 Corn, sweet, kernel plus cob with husks re- moved ...... 0 .06 Corn, sweet, stover ...... 0 .06 (2) Tolerances are established for res- idues of the herbicide quizalofop ethyl, (b) Section 18 emergency exemptions. including its metabolites and [Reserved] degradates, in or on the commodities (c) Tolerances with regional registra- in the following table. Compliance with tions. [Reserved] the tolerance levels specified in the fol- (d) Indirect or inadvertent residues. lowing table is to be determined by measuring only those quizalofop ethyl [Reserved] residues convertible to quizalofop (2-[4- [62 FR 62961, Nov. 26, 1997, as amended at 74 (6-chloroquinoxalin-2-yl- FR 46375, Sept. 9, 2009] oxy)phenoxy]propanoic acid), expressed as quizalofop, in or on the commodity.

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3,3,3,-trifluoro-1-propenyl)-2,2- Commodity Parts per million dimethylcyclopropanecarboxylate. Cattle, fat ...... 0.05 Parts per Cattle, meat ...... 0 .02 Commodity million Cattle, meat byproducts ...... 0.05 Egg ...... 0 .02 Almond, hulls ...... 2 .0 Goat, fat ...... 0 .05 Artichoke, globe ...... 1.0 Goat, meat ...... 0.02 Banana 1 ...... 0.1 Goat, meat byproducts ...... 0 .05 Beet, garden, roots ...... 0 .45 Hog, fat ...... 0 .05 Beet, garden, tops ...... 15 Hog, meat ...... 0 .02 Brassica, head and stem, subgroup 5A, except Hog, meat byproducts ...... 0 .05 cabbage ...... 0 .6 Horse, fat ...... 0 .05 Brassica, leafy greens, subgroup 5B ...... 3 .5 Horse, meat ...... 0 .02 Bushberry subgroup 13-07B ...... 1 .8 Horse, meat byproducts ...... 0 .05 Cabbage ...... 4 .0 Milk ...... 0.01 Caneberry subgroup 13A ...... 1 .0 Milk, fat ...... 0 .25 Cattle, fat ...... 1.0 Poultry, fat ...... 0.05 Cattle, meat byproducts ...... 0.10 Poultry, meat ...... 0 .02 Cattle, meat ...... 0 .5 Coriander, dried leaves ...... 25 Poultry, meat byproducts ...... 0.05 Coriander, leaves ...... 6 .0 Sheep, fat ...... 0 .05 Coriander, seed ...... 5 .0 Sheep, meat ...... 0.02 Corn, field, forage ...... 3 .0 Sheep, meat byproducts ...... 0 .05 Corn, field, grain ...... 0 .05 Corn, field, stover ...... 5 .0 (b) Section 18 emergency exemptions. Corn, pop, grain ...... 0.05 [Reserved] Corn, pop, stover ...... 5.0 Corn, sweet, forage ...... 3 .0 (c) Tolerances with regional registra- Corn, sweet, kernel plus cob with husk removed 0.05 tions. Tolerances with regional reg- Corn, sweet, stover ...... 5 .0 istration are established for residues of Cotton, undelinted seed ...... 0 .5 Eggplant ...... 0.05 the herbicide quizalofop ethyl, includ- Egg ...... 0 .05 ing its metabolites and degradates, in Fruit, citrus, group 10 ...... 0 .05 or on the commodities in the following Goat, fat ...... 1 .0 table. Compliance with the tolerance Goat, meat byproducts ...... 0 .10 Goat, meat ...... 0.5 levels specified in the following table is Grain, aspirated fractions ...... 70 to be determined by measuring only Grape ...... 0 .2 those quizalofop ethyl residues con- Groundcherry ...... 0 .5 Herb subgroup 19A ...... 0 .05 vertible to 2-methoxy-6- Hog, fat ...... 1 .0 chloroquinoxaline, expressed as the Hog, meat byproducts ...... 0 .10 stoichiometric equivalent of quizalofop Hog, meat ...... 0 .5 Hop, dried cones ...... 10 .0 ethyl, in or on the commodity. Horse, fat ...... 1 .0 Horse, meat byproducts ...... 0 .10 Parts per Horse, meat ...... 0 .5 Commodity million Leafy petioles subgroup 4B ...... 3 .0 Pineapple ...... 0.1 Lettuce, head ...... 3.0 Mayhaw ...... 1 .4 Milk, fat (reflecting 0.1 ppm in whole milk) ...... 1 .0 (d) Indirect or inadvertent residues. Nut, tree, group 14 ...... 0 .05 [Reserved] Okra ...... 0.50 Pea and bean, dried shelled, expect soybean, [63 FR 32759, June 16, 1998, as amended at 70 subgroup 6C ...... 0 .15 FR 7870, Feb. 16, 2005; 71 FR 56378, Sept. 27, Pea and bean, succulent shelled, subgroup 6B 0 .05 2006; 76 FR 56045, Sept. 15, 2010; 77 FR 23630, Peanut ...... 0 .05 Apr. 20, 2012] Pear ...... 0 .5 Pepino ...... 0 .5 Pepper, bell ...... 0 .5 § 180.442 Bifenthrin; tolerances for res- Pepper, nonbell ...... 0 .5 idues. Pistachio ...... 0.05 Poultry, fat ...... 0.05 (a) General. (1) Tolerances are estab- Poultry, meat byproducts ...... 0.05 lished for residues of the insecticide Poultry, meat ...... 0 .05 bifenthrin, including its metabolites Radish, tops ...... 4 .5 and degradates, in or on the commod- Rapeseed, seed ...... 0 .05 Sheep, fat ...... 1 .0 ities in the table below. Compliance Sheep, meat byproducts ...... 0 .1 with the tolerance levels specified Sheep, meat ...... 0.5 below is to be determined by measuring Soybean, hulls ...... 0 .50 ′ Soybean, refined oil ...... 0 .30 only bifenthrin, (2-methyl [1,1 - Soybean, seed ...... 0 .2 biphenyl]-3-yl) methyl-3-(2-chloro- Spinach ...... 0 .2

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shall be used in accordance with such Commodity Parts per million label and labeling. Strawberry ...... 3 .0 (b) Section 18 emergency exemptions. Tea, dried 1 ...... 30 Time-limited tolerances are estab- Tomato ...... 0.15 lished for residues of the insecticide Turnip, greens ...... 3.5 Vegetable, cucurbit, group 9 ...... 0.4 bifenthrin, including its metabolites Vegetable, legume, edible podded, subgroup 6A 0 .6 and degradates, in connection with use Vegetable, root, subgroup 1B except sugar beet of the pesticide under a Section 18 and garden beet ...... 0 .10 emergency exemption granted by EPA. Vegetable, tuberous and corm, subgroup 1C ..... 0.05 Compliance with the tolerance levels 1 There are no U.S. registrations. specified below is to be determined by (2) A tolerance of 0.05 ppm is estab- measuring only bifenthrin, (2-methyl lished for residues of the insecticide [1,1′-biphenyl]-3-yl) methyl-3-(2-chloro- bifenthrin, (2-methyl[1,1′-biphenyl]-3- 3,3,3,-trifluoro-1-propenyl)-2,2- yl)methyl-3-(2-chloro-3,3,3-trifluoro-1- dimethylcyclopropanecarboxylate. propenyl)-2,2-dimethylcyclopropane- These tolerances will expire and are re- carboxylate, as follows: voked on the dates specified in the fol- (i) In or on all food/feed items (other lowing table: than those covered by a higher toler- Expiration/ ance as a result of use on growing Parts per Commodity million revocation crops) in food/feed handling establish- date ments. Apple ...... 0.5 12/31/15 (ii) The insecticide may be present as Nectarine ...... 0.5 12/31/15 a residue from application of bifenthrin Peach ...... 0.5 12/31/15 in food handling establishments, in- cluding food service, manufacturing (c) Tolerances with regional registra- and processing establishments, such as tions. Tolerances with regional reg- istrations are established for residues restaurants, cafeterias, supermarkets, of the insecticide bifenthrin, including bakeries, breweries, dairies, meat its metabolites and degradates, in or slaughtering and packing plants, and on the commodities in the table below. canneries, feed handling establish- Compliance with the tolerance levels ments including feed manufacturing specified below is to be determined by and processing establishments, in ac- measuring only bifenthrin, (2-methyl cordance with the following prescribed [1,1′-biphenyl]-3-yl) methyl-3-(2-chloro- conditions: 3,3,3,-trifluoro-1-propenyl)-2,2- (A) Application shall be limited to dimethylcyclopropanecarboxylate. general surface and spot and/or crack and crevice treatment in food/feed han- Commodity Parts per dling establishments where food/feed million and food/feed products are held, proc- Grass, forage ...... 4 .0 essed, prepared and served. General Grass, hay ...... 15 surface application may be used only when the facility is not in operation (d) Indirect or inadvertent residues. provided exposed food/feed has been [Reserved] covered or removed from the area [62 FR 31002, June 6, 1997] being treated. Spot and/or crack and EDITORIAL NOTE: For FEDERAL REGISTER ci- crevice application may be used while tations affecting § 180.442, see the List of CFR the facility is in operation provided ex- Sections Affected, which appears in the posed food/feed is covered or removed Finding Aids section of the printed volume from the area being treated prior to ap- and at www.fdsys.gov. plication. Spray concentration shall be limited to a maximum of 0.06 percent § 180.443 Myclobutanil; tolerances for active ingredient. Contamination of residues. food/feed or food/feed contact surfaces (a) General. Tolerances are estab- shall be avoided. lished for combined residues of the fun- (B) To assure safe use of the insecti- gicide myclobutanil alpha-butyl-alpha- cide, its label and labeling shall con- (4-chlorophenyl)-1H-1,2,4-triazole-1- form to that registered with the U.S. propanenitrile and its alcohol metabo- Environmental Protection Agency and lite (alpha-(3-hydroxybutyl)-alpha-(4-

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chlorophenyl)-1H-1,2,4-triazole-1- Commodity Parts per propanenitrile (free and bound), in or million on the following food commodities: Tomato, paste ...... 1 .0 Vegetable, cucurbit, group 9 ...... 0.20 Parts per Commodity million Vegetable, fruiting, group 8, except tomato ...... 4 .0 Almond ...... 0.1 (b) Section 18 emergency exemptions. Almond, hulls ...... 2 .0 Apple ...... 0.5 [Reserved] Apple, dry pomace ...... 5.0 (c) Tolerances with regional registra- Apple, wet pomace ...... 5 .0 tions. [Reserved] Artichoke, globe ...... 0.90 Asparagus ...... 0.02 (d) Indirect or inadvertent residues. Banana, postharvest ...... 4 .0 Tolerances are established for residues Bean, snap, succulent ...... 1 .0 of the fungicide myclobutanil alpha- Caneberry subgroup 13A ...... 2 .0 Canistel ...... 3 .0 butyl-alpha-(4-chlorophenyl)-1H-1,2,4- Cattle, fat ...... 0.05 triazole-1-propanenitrile in or on the Cattle, liver ...... 1 .0 Cattle, meat ...... 0 .1 following food commodities: Cattle, meat byproducts, except liver ...... 0 .2 Cherry, sweet ...... 5 .0 Commodity Parts per Cherry, tart ...... 5 .0 million Cilantro, leaves ...... 9 .0 Cotton, undelinted seed ...... 0 .02 Animal feed, nongrass, group 18 ...... 0 .03 Currant ...... 3 .0 Grain, cereal, forage, fodder and straw, group Egg ...... 0 .02 16 ...... 0 .03 Fruit, stone, except cherry ...... 2.0 Grain, cereal, group 15 ...... 0.03 Goat, fat ...... 0 .05 Vegetable, brassica, leafy, group 5 ...... 0.03 Goat, liver ...... 1.0 Vegetable, foliage of legume, group 7 ...... 0 .03 Goat, meat ...... 0.1 Vegetable, fruiting, group 8 ...... 0.03 Goat, meat byproducts, except liver ...... 0 .2 Vegetable, leafy, except brassica, group 4 ...... 0 .03 Gooseberry ...... 2 .0 Grain, aspirated fractions ...... 35 Vegetable, leaves of root and tuber, group 2 ..... 0 .03 Grape ...... 1 .0 Vegetable, legume, group 6 ...... 0 .03 Grape, dried pomace ...... 10 .0 Vegetable, root and tuber, group 1 ...... 0 .03 Grape, raisin ...... 10.0 Grape, raisin, waste ...... 25 .0 Grape, wet pomace ...... 10 .0 [54 FR 6131, Feb. 8, 1989] Hog, fat ...... 0 .05 Hog, liver ...... 1 .0 EDITORIAL NOTE: For FEDERAL REGISTER ci- Hog, meat ...... 0 .1 tations affecting § 180.443, see the List of CFR Hog, meat byproducts, except liver ...... 0 .2 Sections Affected, which appears in the Hop, dried cones ...... 10 Finding Aids section of the printed volume Horse, fat ...... 0 .05 Horse, liver ...... 1 .0 and at www.fdsys.gov. Horse, meat ...... 0 .1 Horse, meat byproducts, except liver ...... 0 .2 § 180.444 Sulfur dioxide; tolerances for Leafy greens, subgroup 4A, except spinach ...... 9 .0 residues. Mango ...... 3.0 Mayhaw ...... 0 .70 (a) General. A tolerance is established Milk ...... 0.2 as follows for sulfite residues of the Okra ...... 4.0 Papaya ...... 3 .0 fungicide sulfur dioxide (determined as Peppermint, tops ...... 3 .0 (SO2)) in or on the following raw agri- Plum, prune, dried ...... 8.0 Poultry, fat ...... 0.02 cultural commodity(ies): Poultry, meat ...... 0 .02 Poultry, meat byproducts ...... 0.02 Commodity Parts per Sapodilla ...... 3 .0 million Sapote, black ...... 3 .0 Sapote, mamey ...... 3 .0 Grape, postharvest ...... 10.0 Sheep, fat ...... 0 .05 Sheep, liver ...... 1.0 (b) Section 18 emergency exemptions. Sheep, meat ...... 0.1 Sheep, meat byproducts, except liver ...... 0 .2 Time-limited tolerances specified in Soybean, forage ...... 3 .5 the following table are established for Soybean, hay ...... 15 residues of sulfur dioxide, including its Soybean, refined oil ...... 0 .40 Soybean, seed ...... 0 .25 metabolites and degradates in or on Spearmint, tops ...... 3 .0 the specified agricultural commodities, Star apple ...... 3 .0 resulting from use of the pesticide pur- Strawberry ...... 0 .50 Tomato ...... 0.30 suant to FFIFRA section 18 emergency Tomato, puree ...... 0 .50

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exemptions. Compliance with the toler- Commodity Parts per ance levels specified below is to be de- million termined by measuring only sulfur di- Apple, dry pomace ...... 3.0 oxide (SO2). The tolerances expire on Apple, wet pomace ...... 3 .0 the date specified in the table. Apricot ...... 1 .0 Cherry ...... 1.0 Grape ...... 1 .0 Parts per Expiration/ Commodity million revocation Nectarine ...... 1 .0 date Peach ...... 1 .0 Fig ...... 10 12/31/14 Pear ...... 0 .5 Persimmon ...... 0 .05 Walnut ...... 0 .02 (c) Tolerances with regional registra- tions. [Reserved] (2) Tolerances are established for res- (d) Indirect or inadvertent residues. idues of the insecticide clofentezine, [Reserved] including its metabolites and [54 FR 20126, May 10, 1989, as amended at 76 degradates, in or on the commodities FR 56648, Sept. 14, 2011] in the table in this paragraph. Compli- ance with the tolerance levels specified § 180.445 Bensulfuron methyl; toler- in this paragraph is to be determined ances for residues. by measuring only the sum of (a) General. Tolerances are estab- clofentezine, 3,6-bis(2-chlorophenyl)- lished for residues of the herbicide 1,2,4,5-tetrazine, and its metabolite, 3- bensulfuron methyl (methyl-2[[[[[(4,6- (2-chloro-4-hydroxyphenyl)-6-(2- dimethoxy-pyrimidin-2-yl) amino] car- chlorophenyl)-1,2,4,5-tetrazine, cal- bonyl] amino] sulfonyl] methyl] ben- culated as the stoichiometric equiva- zoate) in or on the following raw agri- lent of clofentezine, in or on com- cultural commodities: modity. Parts per Commodity million Parts per Commodity million Crayfish ...... 0.05 Cattle, fat ...... 0.05 Rice, grain ...... 0 .02 Rice, straw ...... 0 .3 Cattle, liver ...... 0 .4 Cattle, meat ...... 0 .05 Cattle, meat byproducts, except liver ...... 0 .05 (b) Section 18 emergency exemptions. Goat, fat ...... 0 .05 [Reserved] Goat, liver ...... 0.4 (c) Tolerances with regional registra- Goat, meat ...... 0.05 tions. [Reserved] Goat, meat byproducts, except liver ...... 0 .05 (d) Indirect or inadvertent residues. Hog, fat ...... 0 .05 Hog, liver ...... 0 .4 [Reserved] Hog, meat ...... 0 .05 [63 FR 9435, Feb. 25, 1998] Hog, meat byproducts, except liver ...... 0 .05 Horse, fat ...... 0 .05 § 180.446 Clofentezine; tolerances for Horse, liver ...... 0 .4 Horse, meat ...... 0 .05 residues. Horse, meat byproducts, except liver ...... 0 .05 (a) General. (1) Tolerances are estab- Milk ...... 0.01 lished for residues of the insecticide Sheep, fat ...... 0 .05 Sheep, liver ...... 0.4 clofentezine, including its metabolites Sheep, meat ...... 0.05 and degradates, in or on the commod- Sheep, meat byproducts, except liver ...... 0 .05 ities in the table in this paragraph. Compliance with the tolerance levels (b) Section 18 emergency exemptions. specified in this paragraph is to be de- [Reserved] termined by measuring only (c) Tolerances with regional registra- clofentezine, 3,6-bis(2-chlorophenyl)- tions. [Reserved] 1,2,4,5-tetrazine, in or on the com- (d) Indirect or inadvertent residues. modity. [Reserved]

Commodity Parts per [56 FR 15503, Apr. 17, 1991, as amended at 56 million FR 22335, May 15, 1991; 59 FR 26947, May 25, Almond, hulls ...... 5 .0 1994; 60 FR 12709, Mar. 8, 1995; 64 FR 19050, Almond ...... 0.5 Apr. 19, 1999; 70 FR 11572, Mar. 9, 2005; 74 FR Apple ...... 0.5 46375, Sept. 9, 2009; 76 FR 23496, Apr. 27, 2011]

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§ 180.447 Imazethapyr; tolerances for Commodity Parts per residues. million (a) General. (1) Tolerances are estab- Corn, field, grain ...... 0 .1 lished for residues of the herbicide Corn, field, stover ...... 0 .1 Crayfish ...... 0.15 imazethapyr, 2-[4,5-dihydro-4-methyl-4- Goat, meat byproducts ...... 0 .10 (1-methylethyl)-5-oxo- 1H-imidazol-2- Hog, meat byproducts ...... 0 .10 yl]-5-ethyl-3-pyridine carboxylic acid, Horse, meat byproducts ...... 0 .10 applied as its acid or ammonium salt, Sheep, meat byproducts ...... 0 .10 in or on the following raw agricultural (b) Section 18 emergency exemptions. commodities: [Reserved] Parts per (c) Tolerances with regional registra- Commodity million tions. Tolerances with regional reg- Canola, seed 1 ...... 0 .10 istration, as defined in § 180.1(l) of this Soybean ...... 0.1 chapter, are established for the sum of Vegetable, legume, group 6 ...... 0 .1 residues of the herbicide imazethapyr, 1 There are no U.S. registrations for canola as of March 2- [4,5-dihydro-4-methyl-4-(1- 21, 2003. methylethyl)-5-oxo-1H-imidazol-2-yl]-5- (2) Tolerances are established for the ethyl- 3-pyridine carboxylic acid, as its sum of the residues of the herbicide ammonium salt, and its metabolite, 2- imazethapyr, 2-[4,5-dihydro-4-methyl-4- [4,5-dihydro-4-methyl-4-(1- (1-methylethyl)-5-oxo- 1H-imidazol-2- methylethyl)-5-oxo-1H-imidazol-2-yl]-5- yl]-5-ethyl-3-pyridine carboxylic acid; (1- hydroxyethyl)-3-pyridine carboxylic its metabolite CL 288511, 2-[4,5-dihydro- acid, both free and conjugated, applied 4-methyl-4-(1-methylethyl)-5-oxo-1H- as its acid or ammonium salt, in or on imidazol-2-yl]-5-(1-hydroxyethyl)-3-pyr- the following raw agricultural com- idine carboxylic acid; and its metabo- modities: lite CL 182704, 5-[1-(beta-D- Parts per glucopyranosyloxy)ethyl]-2-[4,5- Commodity million dihydro-4-methyl-4-(1-methylethyl)-5- oxo-1H-imidazol-2-yl]-3- Endive ...... 0.1 Lettuce, head ...... 0.1 pyridinecarboxylic acid, applied as its Lettuce, leaf ...... 0 .1 acid or ammonium salt, in or on the following commodities: (d) Indirect or inadvertent residues. [Reserved] Commodity Parts per million [67 FR 55331, Aug. 29, 2002, as amended at 68 Alfalfa, seed ...... 0 .15 FR 13849, Mar. 21, 2003; 71 FR 6359, Feb. 8, Alfalfa, seed screenings ...... 0 .15 2006; 76 FR 34885, June 15, 2011] Animal feed, nongrass, group 18, forage ...... 3 .0 Animal feed, nongrass, group 18, hay ...... 5.5 § 180.448 Hexythiazox; tolerance for Peanut ...... 0 .1 residues. Rice, bran ...... 1.2 Rice, grain ...... 0 .3 (a) General. Tolerances are estab- Rice, straw ...... 0 .4 lished for residues of hexythiazox, in- cluding its metabolites and degradates, (3) A tolerance is established for the in or on the commodities in the table sum of residues of the herbicide below. Compliance with the tolerance imazethapyr, 2-[4,5-dihydro-4-methyl-4- levels specified below is to be deter- (1-methylethyl)-5-oxo- 1H-imidazol-2- mined by measuring only hexythiazox yl]-5-ethyl-3-pyridine carboxylic acid, and its metabolites containing the (4- and its metabolite CL 288511, 2-[4,5- chlorophenyl)-4-methyl-2-oxo-3- dihydro-4-methyl-4-(1-methylethyl)-5- thiazolidine moiety, calculated as the oxo-1H-imidazol-2-yl]-5-(1-hydroxy- stoichiometric equivalent of ethyl)-3-pyridine carboxylic acid, ap- hexythiazox. plied as its acid or ammonium salt, in or on the following commodities: Parts per Commodity million Parts per Commodity million Almond, hulls ...... 10 Apple, wet pomace ...... 0 .40 Cattle, meat byproducts ...... 0.10 Berry, low growing, subgroup 13–07G ...... 6 Corn, field, forage ...... 0 .1 Caneberry subgroup 13–07A ...... 1

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as the stoichiometric equivalent of Commodity Parts per million hexythiazox. Cattle, fat ...... 0.05 Parts per Cattle, meat byproducts ...... 0.5 Commodity million Citrus, dried pulp ...... 0 .60 Citrus, oil ...... 24 Alfalfa, forage (EPA Regions 9–11 only) ...... 15 Corn, field, forage ...... 3 .0 Alfalfa, hay (EPA Regions 9–11 only) ...... 30 Corn, field, grain ...... 0 .02 Bean, dried, seed (EPA Regions 7–12 only) ...... 0 .4 Corn, field, stover ...... 7 .0 Bean, succulent (EPA Regions 7–12 only) ...... 0.3 Date, dried fruit ...... 1 .0 Corn, field, forage ...... 6 .0 Egg ...... 0 .05 Corn, field, grain ...... 0 .02 Fruit, pome, group 11–10 ...... 0 .4 Corn, field, stover ...... 2 .5 Fruit, small, vine climbing, subgroup 13–07F, Corn, sweet, forage (EPA Regions 7–12 only) ... 4 .0 except fuzzy kiwifruit ...... 1 Corn, sweet, kernel plus cob with husks re- Fruit, stone, group 12 ...... 1 .0 moved (EPA Regions 7–12 only) ...... 0 .1 Goat, fat ...... 0 .05 Cotton, gin byproducts, CA and AZ only ...... 3 .0 Goat, meat byproducts ...... 0 .5 Cotton, undelinted seed, CA and AZ only ...... 0 .20 Grain, aspirated fractions ...... 5 Fruit, citrus group 10 (CA, AZ, TX only) ...... 0 .35 Hog, fat ...... 0 .02 Potato ...... 0 .02 Hog, meat byproducts ...... 0 .05 Sorghum, grain, forage (EPA Regions 6–8 only) 5 Hop, dried cones ...... 2 .0 Sorghum, grain, grain (EPA Regions 6–8 only) .. 3 Horse, fat ...... 0 .05 Sorghum, grain, stover (EPA Regions 6–8 only) 6 Horse, meat byproducts ...... 0 .5 Timothy, forage (EPA Regions 9–11 only) ...... 40 Milk ...... 0.05 Timothy, hay (EPA Regions 9–11 only) ...... 40 Nut, tree, group 14 ...... 0 .30 Pepper/eggplant subgroup 8–10B ...... 1 .5 (d) Indirect or inadvertent residues. Peppermint, tops ...... 2 .0 [Reserved] Pistachio ...... 0.30 Plum, prune, dried ...... 1.3 [54 FR 17948, Apr. 26, 1989] Poultry, fat ...... 0.05 Poultry, meat byproducts ...... 0.05 EDITORIAL NOTE: For FEDERAL REGISTER ci- Sheep, fat ...... 0 .05 tations affecting § 180.448, see the List of CFR Sheep, meat byproducts ...... 0 .5 Sections Affected, which appears in the Spearmint, tops ...... 2 .0 Finding Aids section of the printed volume Tomato ...... 0.50 and at www.fdsys.gov.

(b) Section 18 emergency exemptions. A § 180.449 Avermectin B 1 and its delta- time-limited tolerance specified in the 8,9-isomer; tolerances for residues. following table is established for resi- (a) General. Tolerances are estab- dues of hexythiazox and its metabolites lished for residues of abamectin, in- containing the (4-chlorophenyl)-4- cluding its metabolites and degradates, methyl-2-oxo-3-thiazolidine moiety, in or on the commodities in the fol- calculated as the stoichiometric equiv- lowing table. Compliance with the tol- alent of hexythiazox, in or on the spec- erance levels specified in the following ified agricultural commodity, resulting table is to be determined by measuring from use of the pesticide pursuant to only avermectin B1 a mixture of FIFRA section 18 emergency exemp- avermectins containing greater than or tions. The tolerance expires on the equal to 80% avermectin B1 a (5-O- date specified in the table. demethyl avermectin A1) and less than Parts per Expiration or equal to 20% avermectin B1b (5-O- Commodity million date demethyl-25-de(1-methylpropyl)-25-(1- methylethyl) avermectin A1) and its Beet, sugar, root ...... 0.15 12/31/19 delta-8,9-isomer in or on the following (c) Tolerances with regional registra- commodities: tions. Tolerances with regional reg- Parts per istrations as defined by § 180.1(l), are es- Commodity million tablished for residues of hexythiazox, Almond, hulls ...... 0 .10 including its metabolites and Apple ...... 0.020 degradates, in or on the commodities Apple, wet pomace ...... 0 .10 in the table below. Compliance with Avocado ...... 0 .020 Bean, dry, seed ...... 0 .01 the tolerance levels specified below is Cattle, fat ...... 0.03 to be determined by measuring only Cattle, meat ...... 0 .02 hexythiazox and its metabolites con- Cattle, meat byproducts ...... 0.06 Celeriac, roots ...... 0 .05 taining the (4-chlorophenyl)-4-methyl- Celeriac, tops ...... 0 .05 2-oxo-3-thiazolidine moiety, calculated Chive, dried leaves ...... 0 .02

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methyl-4-(1H-1,2,4-triazol-l-yl)-1,3- Commodity Parts per million butanediol, calculated as triadimenol, Chive, fresh leaves ...... 0 .01 in or on the following commodities: Citrus, dried pulp ...... 0 .10 Citrus, oil ...... 0.10 Parts per Expiration/ Citrus ...... 0 .02 Commodity million Revocation Cotton, gin byproducts ...... 1 .0 Date Cotton, undelinted seed ...... 0 .02 Banana 1 ...... 0.2 None Food products in food handling establishments Barley, grain ...... 0.05 None (other than those already covered by higher Barley, straw ...... 0.2 None tolerances as a result of use on growing Corn, field, forage ...... 0.05 None crops, and other than those already covered Corn, field, grain ...... 0.05 None by tolerances on milk, meat, and meat by- Corn, field, stover ...... 0.05 None products) ...... 0.01 Corn, pop, grain ...... 0.05 None Fruit, stone, group 12 ...... 0 .09 Corn, pop, stover ...... 0.05 None Goat, fat ...... 0 .01 Corn, sweet, forage ...... 0.05 None Goat, meat ...... 0.02 Corn, sweet, kernel plus cob with Goat, meat byproducts ...... 0 .02 husks removed ...... 0.05 None Grape ...... 0 .02 Corn, sweet, stover ...... 0.05 None Herb subgroup 19A, except chive ...... 0 .030 Cotton, undelinted seed ...... 0.02 None Hog, fat ...... 0 .01 Oat, forage ...... 2.5 None Hog, meat ...... 0 .02 Oat, grain ...... 0.05 None Hog, meat byproducts ...... 0 .02 Oat, straw ...... 0.2 None Hop, dried cones ...... 0 .20 Horse, fat ...... 0 .01 Rye, forage ...... 2.5 None Horse, meat ...... 0 .02 Rye, grain ...... 0.05 None Horse, meat byproducts ...... 0 .02 Rye, straw ...... 0.1 None Milk ...... 0.005 Wheat, forage ...... 2.5 None Nut, tree, group 14 ...... 0 .01 Wheat, grain ...... 0.05 None Onion, bulb, subgroup 3–07A ...... 0 .01 Wheat, straw ...... 0.2 None Pear ...... 0 .02 1 There are no U.S. registrations for banana (whole) as of Peppermint, tops ...... 0 .010 September 22, 1993. Pistachio ...... 0.01 Plum, prune, dried ...... 0.025 (b) Section 18 emergency exemptions. Poultry, meat ...... 0 .02 [Reserved] Poultry, meat byproducts ...... 0.02 Sheep, fat ...... 0 .01 (c) Tolerances with regional registra- Sheep, meat ...... 0.02 tions. [Reserved] Sheep, meat byproducts ...... 0 .02 (d) Indirect or inadvertent residues. Spearmint, tops ...... 0 .010 Strawberry ...... 0 .05 [Reserved] Vegetable, cucurbit, group 9 ...... 0.005 [73 FR 54962, Sept. 24, 2008, as amended at 74 Vegetable, fruiting, group 8 ...... 0.020 Vegetable, leafy, except brassica, group 4 ...... 0 .10 FR 47457, Sept. 16, 2009; 76 FR 34885, June 15, Vegetable, tuberous and corm, subgroup 01C 0 .01 2011]

(b) Section 18 emergency exemptions. § 180.451 Tribenuron methyl; toler- [Reserved] ances for residues. (c) Tolerances with regional registra- (a) General. Tolerances are estab- tions. [Reserved] lished for residues of the herbicide (d) Indirect or inadvertent residues. tribenuron methyl and its metabolites [Reserved] and degradates in or on the commod- ities in the following table. Compliance [62 FR 44095, Aug. 19, 1997] with the tolerance levels specified EDITORIAL NOTE: For FEDERAL REGISTER ci- below is to be determined by measuring tations affecting § 180.449, see the List of CFR only tribenuron methyl, methyl-2- Sections Affected, which appears in the [[[[N-(4-methoxy-6-methyl-1,3,5-triazin- Finding Aids section of the printed volume and at www.fdsys.gov. 2-yl) methylamino] carbonyl] amino] sulfonyl] benzoate, in or on the fol- § 180.450 Beta-(4-Chlorophenoxy)- lowing commodities: alpha-(1,1-dimethylethyl)-1H-1,2,4- Parts per triazole-1-ethanol; tolerances for Commodity million residues. (a) General. Tolerances are estab- Barley, grain ...... 0 .05 Barley, hay ...... 0 .4 lished for the combined residues of the Barley, straw ...... 0 .10 fungicide b-(4-chlorophenoxy)-a-(1,1- Canola, seed ...... 0 .02 dimethylethyl)-1H-1,2,4-triazole-1-eth- Corn, field, forage ...... 0 .15 Corn, field, grain ...... 0 .01 anol (triadimenol) and its butanediol Corn, field, stover ...... 1 .1 metabolite, 4-(4-chlorophenoxy)-2,2-di- Cotton, gin byproducts ...... 0 .02

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Parts per Parts per Commodity million Commodity million

Cotton, undelinted seed ...... 0 .02 Cattle, meat byproducts ...... 0.10 Flax, seed ...... 0 .02 Corn, field, forage ...... 0 .10 Grain, aspirated fractions ...... 1 .5 Corn, field, grain ...... 0 .02 Oat, forage ...... 0 .05 Corn, field, stover ...... 0 .10 Oat, grain ...... 0 .05 Corn, pop, grain ...... 0.02 Oat, hay ...... 0.05 Corn, pop, stover ...... 0.10 Oat, straw ...... 0.10 Egg ...... 0 .10 Rice, grain ...... 0 .05 Goat, fat ...... 0 .10 Rice, straw ...... 0 .05 Goat, meat ...... 0.10 Sorghum, grain, forage ...... 0.05 Goat, meat byproducts ...... 0 .10 Sorghum, grain, grain ...... 0 .05 Hog, fat ...... 0 .10 Sorghum, grain, stover ...... 0 .05 Hog, meat ...... 0 .10 Soybean, forage ...... 0 .07 Hog, meat byproducts ...... 0 .10 Soybean, hay ...... 0 .35 Horse, fat ...... 0 .10 Soybean, hulls ...... 0 .04 Horse, meat ...... 0 .10 Soybean, seed ...... 0 .01 Horse, meat byproducts ...... 0 .10 Sunflower, seed ...... 0.05 Milk ...... 0.02 Wheat, forage ...... 0 .3 Poultry, fat ...... 0.10 Wheat, grain ...... 0 .05 Poultry, meat ...... 0 .10 Wheat, hay ...... 0 .5 Poultry, meat byproducts ...... 0.10 Wheat, straw ...... 0 .10 Sheep, fat ...... 0 .10 Sheep, meat ...... 0.10 (b) Section 18 emergency exemptions. Sheep, meat byproducts ...... 0 .10 [Reserved] (b) Section 18 emergency exemptions. (c) Tolerances with regional registra- [Reserved] tions. Tolerances with regional reg- (c) Tolerances with regional registra- istration, as defined in § 180.1(l) are es- tions. [Reserved] tablished for residues of the herbicide (d) Indirect or inadvertent residues. tribenuron methyl (methyl-2-[[[[N-(4- [Reserved] methoxy-6-methyl-1,3,5-triazin-2-yl) methylamino] car- [55 FR 21548, May 25, 1990, as amended at 62 bonyl]amino]sulfonyl] benzoate) in or FR 66020, Dec. 17, 1997; 63 FR 66458, Dec. 2, on the following raw agricultural com- 1998; 67 FR 35049, May 17, 2002; 74 FR 46375, modities: Sept. 9, 2009; 74 FR 46699, Sept. 11, 2009; 77 FR 59128, Sept. 26, 2012] Parts per Commodity million § 180.454 Nicosulfuron; tolerances for residues. Grass, forage, fodder and hay, group 17, ex- cept bermudagrass; forage ...... 0 .10 (a) General. Tolerances are estab- Grass, forage, fodder and hay, group 17, ex- lished for residues of the herbicide cept bermudagrass; hay ...... 0 .10 nicosulfuron, including its metabolites and degradates, in or on the commod- (d) Indirect or inadvertent residues. ities in the following table [below]. [Reserved] Compliance with the tolerance levels [69 FR 56718, Sept. 22, 2004, as amended at 72 specified in the following table [below] FR 11789, Mar. 14, 2007; 73 FR 47065, Aug. 13, is to be determined by measuring only 2008; 74 FR 67128, Dec. 18, 2009; 76 FR 34885, nicosulfuron, 3-Pyridinecarboxamide, June 15, 2011] 2-[[[[(4,6-dimethoxy-2- § 180.452 Primisulfuron-methyl; toler- pyrimidinyl)amino] car- ances for residues. bonyl]amino]sulfonyl]-N,N-dimethyl-.

(a) General. Tolerances are estab- Commodity Parts per lished for residues of primisulfuron- million methyl (3-[4,6-bis-(difluoromethoxy)- Cattle, fat ...... 0.01 pyrimidin-2-yl]-1-(2- Cattle, meat ...... 0 .01 methoxycarbonylphenylsulfonyl) urea) Cattle, meat byproducts ...... 0.05 Corn, field, forage ...... 0 .1 in or on the following raw agricultural Corn, field, grain ...... 0 .1 commodities. Corn, field, stover ...... 0 .1 Corn, pop, grain ...... 0.1 Parts per Corn, pop, stover ...... 0.1 Commodity million Corn, sweet, forage ...... 0 .1 Corn, sweet, kernel plus cob with husks re- Cattle, fat ...... 0.10 moved ...... 0 .1 Cattle, meat ...... 0 .10 Corn, sweet, stover ...... 0 .1

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(1,1-dimethylethyl)-1H-1,2,4-triazole-1- Commodity Parts per million ethanol, in or on the following raw ag- Goat, fat ...... 0 .01 ricultural commodity: Goat, meat ...... 0.01 Goat, meat byproducts ...... 0 .05 Commodity Parts per Grass, forage ...... 9 .0 million Grass, hay ...... 25 .0 1 Horse, fat ...... 0 .01 Banana ...... 0.5 Horse, meat ...... 0 .01 1 There are no U.S. registrations as of April 1, 1992. Horse, meat byproducts ...... 0 .05 Milk ...... 0.01 (b) Section 18 emergency exemptions. Sheep, fat ...... 0 .01 [Reserved] Sheep, meat ...... 0.01 Sheep, meat byproducts ...... 0 .05 (c) Tolerances with regional registra- tions. [Reserved] (b) Section 18 emergency exemptions. (d) Indirect or inadvertent residues. Time-limited tolerances specified in [Reserved] the following table [below] are estab- [74 FR 47457, Sept. 16, 2009] lished for residues of the herbicide nicosulfuron, 3-Pyridinecarboxamide, § 180.458 Clethodim; tolerances for res- 2-[[[[(4,6-dimethoxy-2- idues. pyrimidinyl)amino] car- (a) General. Tolerances are estab- bonyl]amino]sulfonyl]-N,N-dimethyl-, lished for residues of the herbicide in or on the specified agricultural com- clethodim, including its metabolites modities, resulting from use of the pes- and degradates, in or on the commod- ticide pursuant to FFIFRA section 18 ities in the table in this paragraph. emergency exemptions. The tolerances Compliance with the tolerance levels expire and are revoked on the date specified in this paragraph is to be de- specified in the table. termined by measuring only the sum of clethodim, 2-[(1E)-1-[[[(2E)-3-chloro-2- Expiration/ Parts per propenyl]oxy]imino]propyl]-5-[2- Commodity million Revokation Date (ethylthio)propyl]-3-hydroxy-2-cyclo- Bermuda grass, forage ...... 10 12/31/11 hexen-1-one, and its metabolites con- Bermuda grass, hay ...... 25 12/31/11 taining the 5-(2- ethylthiopropyl)cyclohexene-3-one and (c) Tolerances with regional registra- 5-(2-ethylthiopropyl)-5- tions. [Reserved] hydroxycyclohexene-3-one moieties (d) Indirect or inadvertent residues. and their sulphoxides and sulphones, [Reserved] calculated as the stoichiometric equiv- [75 FR 17578, Apr. 7, 2010] alent of clethodim, in or on the com- modity. § 180.455 Procymidone; tolerances for Parts per residues. Commodity million A tolerance is established for the res- Alfalfa, forage ...... 6.0 idues of the fungicide procymidone, N- Alfalfa, hay ...... 10 (3,5-dichlorophenyl)-1,2- Artichoke, globe ...... 1.2 dimethylcyclopropane-1,2 Asparagus ...... 1.7 Bean, dry, seed ...... 2 .5 dicarboximide, in or on the following Beet, sugar, molasses ...... 1 .0 raw agricultural commodity: Beet, sugar, roots ...... 0 .20 Beet, sugar, tops ...... 1.0 Parts per Brassica, head and stem, subgroup 5A ...... 3 .0 Commodity million Brassica, leafy greens, subgroup 5B ...... 3 .0 Bushberry subgroup 13–07B ...... 0 .20 Grape, wine ...... 5 .0 Caneberry subgroup 13–07A ...... 0.30 Canola, meal ...... 1 .0 Canola, seed ...... 0 .50 [59 FR 42514, Aug. 18, 1994] Cattle, fat ...... 0.2 Cattle, meat ...... 0 .2 § 180.457 Bitertanol; tolerances for res- Cattle, meat byproducts ...... 0.2 Clover, forage ...... 10.0 idues. Clover, hay ...... 20.0 (a) General. A tolerance is established Corn, field, forage ...... 0 .2 Corn, field, grain ...... 0 .2 for the residues of the fungicide Corn, field, stover ...... 0 .2 bitertanol, b-([1,1′-biphenyl]-4-yloxy)-a- Cotton, meal ...... 2 .0

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chloroethoxy)phenylsulfonyl)urea] in Commodity Parts per million or on the following raw agricultural Cotton, undelinted seed ...... 1 .0 commodities: Cranberry ...... 0 .50 Egg ...... 0 .2 Commodity Parts per Flax, meal ...... 1 .0 million Flax, seed ...... 0 .6 Goat, fat ...... 0 .2 Barley, grain ...... 0 .02 Goat, meat ...... 0.2 Barley, straw ...... 2 .0 Goat, meat byproducts ...... 0 .2 Cattle, fat ...... 0.1 Herb subgroup 19A ...... 12.0 Cattle, kidney ...... 0 .5 Hog, fat ...... 0 .2 Cattle, meat byproducts, except kidney ...... 0.1 Hog, meat ...... 0 .2 Cattle, meat ...... 0 .1 Hog, meat byproducts ...... 0 .2 Hop, dried cones ...... 0 .5 Goat, fat ...... 0 .1 Horse, fat ...... 0 .2 Goat, kidney ...... 0 .5 Horse, meat ...... 0 .2 Goat, meat byproducts, except kidney ...... 0 .1 Horse, meat byproducts ...... 0 .2 Goat, meat ...... 0.1 Leaf petioles subgroup 4B ...... 0 .60 Grass, forage ...... 7 .0 Leafy greens subgroup 4A ...... 2 .0 Grass, hay ...... 2 .0 Melon subgroup 9A ...... 2 .0 Hog, fat ...... 0 .1 Milk ...... 0.05 Hog, kidney ...... 0.5 Mustard, seed ...... 0 .50 Hog, meat byproducts ...... 0 .1 Onion, bulb ...... 0 .20 Onion, green ...... 2 .0 Hog, meat ...... 0 .1 Peach ...... 0 .20 Horse, fat ...... 0 .1 Peanut ...... 3 .0 Horse, kidney ...... 0 .5 Peanut, hay ...... 3.0 Horse, meat byproducts, except kidney ...... 0 .1 Peanut, meal ...... 5 .0 Horse, meat ...... 0 .1 Peppermint, tops ...... 5 .0 Milk ...... 0.02 Potato ...... 0 .5 Sheep, fat ...... 0 .1 Potato, granules/flakes ...... 2 .0 Sheep, kidney ...... 0.5 Poultry, fat ...... 0.2 Sheep, meat byproducts, except kidney ...... 0 .1 Poultry, meat ...... 0 .2 Poultry, meat byproducts ...... 0.2 Sheep, meat ...... 0.1 Radish, tops ...... 0 .70 Wheat, forage ...... 5 .0 Safflower, meal ...... 10.0 Wheat, grain ...... 0 .02 Safflower, seed ...... 5 .0 Wheat, straw ...... 2 .0 Sesame, seed ...... 0 .35 Sheep, fat ...... 0 .2 (b) Section 18 emergency exemptions. Sheep, meat ...... 0.2 Sheep, meat byproducts ...... 0 .2 [Reserved] Soybean ...... 10.0 (c) Tolerances with regional registra- Spearmint, tops ...... 5 .0 tions. [Reserved] Squash/cucumber subgroup 9B ...... 0.50 Strawberry ...... 3 .0 (d) Indirect or inadvertent residues. Sunflower, meal ...... 10 .0 [Reserved] Sunflower, seed ...... 5.0 Turnip, greens ...... 3.0 [60 FR 36731, July 18, 1995, as amended at 63 Vegetable, fruiting group 8 ...... 1 .0 FR 44152, Aug. 18, 1998; 63 FR 66449, Dec. 2, Vegetable, legume, group 6, except soybean .... 3 .5 1998] Vegetable, root, except sugar beet, subgroup 1B ...... 1 .0 Vegetable, tuberous and corm, subgroup 1C ..... 1.0 § 180.460 Benoxacor; tolerances for residues. (b) Section 18 emergency exemptions. (a) General. Tolerances are estab- [Reserved] lished for residues of the inert ingre- (c) Tolerances with regional registra- dient (safener) benoxacor (4- tions. [Reserved] (dichloroacetyl)-3,4-dihydro-3-methyl- (d) Indirect or inadvertent residues. 2H-1, 4-benzoxazine) at 0.01 parts per [Reserved] million (ppm) when used in pesticide [76 FR 23496, Apr. 27, 2011, as amended at 77 formulations containing metolachlor FR 59128, Sept. 26, 2012] or S-metolachlor in or on raw agricul- tural commodities for which tolerances § 180.459 Triasulfuron; tolerances for have been established for metolachlor residues. or S-metolachlor. (a) General. Tolerances are estab- (b) Section 18 energency exemptions. lished for residues of the herbicide [Reserved] triasulfuron [3-(6-methoxy-4-methyl- (c) Tolerances with regional registra- 1,3,5-triazin-2-yl)-1-(2-(2- tions. [Reserved]

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(d) Indirect or inadvertent residues. (d) Indirect or inadvertent residues. [Reserved] [Reserved] [63 FR 7305, Feb. 13, 1998, as amended at 70 [57 FR 54303, Nov. 18, 1992, as amended at 62 FR 21631, Apr. 27, 2005] FR 44558, Aug. 22, 1997; 63 FR 53844, Oct. 7, 1998; 64 FR 46298, Aug. 25, 1999; 65 FR 25652, § 180.461 Cadusafos; tolerances for res- May 3, 2000; 67 FR 35049, May 17, 2002; 72 FR idues. 35665, June 29, 2007; 74 FR 46376, Sept. 9, 2009; 76 FR 23496, Apr. 27, 2011] A tolerance is established for the res- idues of the nematicide/insecticide § 180.463 Quinclorac; tolerances for cadusafos, O-ethyl S,S-di-sec-butyl residues. phosphorodithioate, in or on the fol- (a)(1) General. Tolerances are estab- lowing raw agricultural commodity: lished for residues of the herbicide quinclorac, including its metabolites Parts per Commodity million and degradates, in or on the commod- ities in the table in this paragraph. Banana ...... 0.01 Compliance with the tolerance levels specified in this paragraph is to be de- There are no U.S. registrations as of termined by measuring only May 10, 1994, for the nematicide/ quinclorac, 3,7-dichloro-8- insecticid cadusafos. quinolinecarboxylic acid, in or on the [59 FR 39467, Aug. 3, 1994] commodity. Parts per § 180.462 Pyridate; tolerances for resi- Commodity million dues. Barley, grain ...... 2 .0 (a) General. Tolerances are estab- Berry, low growing, except strawberry, sub- lished for residues of the herbicide group 13–07H ...... 1.5 pyridate, including its metabolites and Cattle, fat ...... 0.7 Cattle, meat byproducts ...... 1.5 degradates, in or on the commodities Cattle, meat ...... 0 .05 in the table in this paragraph. Compli- Egg ...... 0 .05 ance with the tolerance levels specified Goat, fat ...... 0 .7 in this paragraph is to be determined Goat, meat byproducts ...... 1 .5 Goat, meat ...... 0.05 by measuring only the sum of pyridate, Grain, aspirated fractions ...... 1200 O-(6-chloro-3-phenyl-4-pyridazinyl)-S- Grass, forage ...... 150 octyl-carbonothioate, and its metabo- Grass, hay ...... 130 lites, 6-chloro-3-phenyl-pyridazine-4-ol Hog, fat ...... 0 .7 Hog, meat byproducts ...... 1 .5 and conjugates of 6-chloro-3-phenyl-py- Hog, meat ...... 0 .05 ridazine-4-ol, calculated as the stoi- Horse, fat ...... 0 .7 chiometric equivalent of pyridate, in Horse, meat byproducts ...... 1 .5 or on the commodity. Horse, meat ...... 0 .05 Milk ...... 0.05 Poultry, fat ...... 0.05 Parts per Commodity million Poultry, meat byproducts ...... 0.1 Poultry, meat ...... 0 .05 Brassica, head and stem, subgroup 5A ...... 0 .03 Rhubarb ...... 0 .5 Rice, bran ...... 15.0 Cabbage ...... 0 .03 Rice, grain ...... 5 .0 Chickpea, seed ...... 0 .1 Rice, straw ...... 12 .0 Collards ...... 0.03 Sheep, fat ...... 0 .7 Corn, field, forage ...... 0 .03 Sheep, meat byproducts ...... 1 .5 Corn, field, grain ...... 0 .03 Sheep, meat ...... 0.05 Corn, field, stover ...... 0 .03 Sorghum, grain, forage ...... 3.0 Corn, pop, grain ...... 0.03 Sorghum, grain, grain ...... 6 .0 Corn, pop, stover ...... 0.03 Sorghum, grain, stover ...... 1 .0 Peanut ...... 0 .03 Wheat, forage ...... 1 .0 Peppermint, tops ...... 0 .20 Wheat, germ ...... 0 .75 Wheat, grain ...... 0 .5 Spearmint, tops ...... 0 .20 Wheat, hay ...... 0 .5 Wheat, straw ...... 0 .1 (b) Section 18 emergency exemptions. [Reserved] (2) Tolerances are established for res- (c) Tolerances with regional registra- idues of the herbicide quinclorac, in- tions. [Reserved] cluding its metabolites and degradates,

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in or on the commodity in the fol- Commodity Parts per lowing table. Compliance with the tol- million erance levels specified in this para- Bean, dry, seed ...... 0 .01 graph is to be determined by measuring Beet, garden, roots ...... 0 .01 only quinclorac, 3,7-dichloro-8- Beet, garden, tops ...... 0 .01 quinolinecarboxylic acid, and its meth- Beet, sugar, dried pulp ...... 0 .01 yl ester, methyl-3,7-dichloro-8- Beet, sugar, molasses ...... 0 .01 quinolinecarboxylate, calculated as the Beet, sugar, roots ...... 0 .01 Beet, sugar, tops ...... 0.01 stoichiometric equivalent of Corn, field, forage ...... 0 .01 quinclorac, in or on the commodity. Corn, field, grain ...... 0 .01 Corn, field, stover ...... 0 .01 OMMODITY Corn, pop, forage ...... 0 .01 Corn, pop, grain ...... 0.01 Parts per Corn, pop, stover ...... 0.01 Commodity million Corn, sweet, forage ...... 0 .01 Rapeseed, subgroup 20A 1 ...... 1.5 Corn, sweet, kernel plus cob with husks re- moved ...... 0 .01 1 There are no U.S. Registrations. Corn, sweet, stover ...... 0 .01 Cotton, gin byproducts ...... 1 .5 (b) Section 18 emergency exemptions. Cottonseed subgroup 20C ...... 0 .01 Time-limited tolerances are estab- Garlic ...... 0 .01 lished for residues of the herbicide Grass, forage ...... 0 .15 quinclorac, including its metabolites Grass, hay ...... 2 .5 and degradates, in or on the com- Grass, seed screenings ...... 0 .01 modity in the table in this paragraph. Grass, straw ...... 0 .01 Compliance with the tolerance level Hop, dried cones ...... 0 .05 Horseradish ...... 0.01 specified in this paragraph is to be de- Leek ...... 0 .01 termined by measuring only Onion, bulb ...... 0 .01 quinclorac, 3,7-dichloro-8- Onion, green ...... 0 .01 quinolinecarboxylic acid, in or on the Onion, Welsh ...... 0 .01 commodity. The tolerance expires and Peanut ...... 0 .01 is revoked on the date specified in the Peanut, hay ...... 0.01 Radish, roots ...... 0 .01 table in this paragraph. Radish, tops ...... 0 .01 Rutabaga, roots ...... 0 .01 Expiration/ Commodity Parts per revocation Rutabaga, tops ...... 0 .1 million date Shallot, bulb ...... 0 .01 Shallot, fresh leaves ...... 0 .01 Cranberry ...... 15.0 12/31/12 Sorghum, grain, forage ...... 0.01 Sorghum, grain, grain ...... 0 .01 (c) Tolerances with regional registra- Sorghum, grain, stover ...... 0 .01 tions. [Reserved] Soybean, seed ...... 0 .01 (d) Indirect or inadvertent residues. Turnip, greens ...... 0.1 Turnip, roots ...... 0 .01 [Reserved] Turnip, tops ...... 0.1 [57 FR 47996, Oct. 21, 1992, as amended at 64 Vegetable, tuberous and corm, subgroup 1C ... 0.01 FR 6548, 6549, Feb. 10, 1999; 64 FR 14632, Mar. 26, 1999; 65 FR 33701, May 24, 2000; 67 FR 35049, (b) Section 18 emergency exemptions. May 17, 2002; 72 FR 55073, Sept. 28, 2007; 74 FR [Reserved] 51490, Oct. 7, 2009; 74 FR 67090, Dec. 18, 2009; (c) Tolerances with regional registra- 76 FR 23497, Apr. 27, 2011; 77 FR 75566, Dec. 21, tions. Tolerances with regional reg- 2012; 78 FR 71528, Nov. 29, 2013] istration are established for residues of § 180.464 Dimethenamid; tolerances for dimethenamid, 1 (R,S)-2-chloro-N-[(1- residues. methyl-2-methoxy) ethyl]-N-(2,4- (a) General. Tolerances are estab- dimethylthien-3-yl)-acetamide) in or lished for residues of the herbicide on the following raw agricultural com- dimethenamid, 1(R,S)-2-chloro-N-[(1- modities: methyl-2-methoxy)ethyl]-N-(2,4- Parts per dimethylthien-3-yl)-acetamide, applied Commodity million as either the 90:10 or 50:50 S:R isomers, in or on the following food commod- Pumpkin ...... 0.01 Squash, winter ...... 0 .01 ities:

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(d) Indirect or inadvertent residues. Commodity Parts per [Reserved] million [65 FR 51551, Aug. 24, 2000, as amended at 67 Brassica, head and stem, subgroup 5A ...... 3 .0 FR 46884, July 17, 2002; 69 FR 29459, May 24, Bushberry subgroup 13–07B ...... 3 .0 Caneberry subgroup 13-07A ...... 12 2004; 69 FR 57207, Sept. 24, 2004; 70 FR 24712, Canistel ...... 1 .0 May 11, 2005; 71 FR 25942, May 3, 2006; 71 FR Cattle, fat ...... 1.0 49354, Aug. 23, 2006; 72 FR 44388, Aug. 8, 2007; Cattle, meat byproducts ...... 0.1 72 FR 73630, Dec. 28, 2007; 80 FR 9215, Feb. 20, Cattle, meat ...... 0 .1 2015] Cherimoya ...... 1 .5 Cherry, sweet ...... 5 .0 Cherry, tart ...... 5 .0 § 180.465 4-(Dichloroacetyl)-1-oxa-4- Citrus, dried pulp ...... 4 .0 azaspiro[4.5]decane. Citrus, oil ...... 75 (a) General. Tolerances are estab- Cotton, refined oil ...... 3.0 Cotton, undelinted seed ...... 1 .0 lished for the residues of 4- Custard apple ...... 1 .5 (dichloroacetyl)-1-oxa-4- Egg ...... 0 .05 azaspiro[4.5]decane, (CAS No. 71526–07– Feijoa ...... 3 .0 Fruit, citrus, group 10–10 ...... 2 .0 3) when used as an inert ingredient Fruit, pome, group 11–10 ...... 5 .0 (safener) in or on the following raw ag- Fruit, small vine climbing, except fuzzy ricultural commodities: kiwifruit, subgroup 13–07F ...... 5.0 Fruit, stone, crop group 12, except cherry ...... 1 .4 Goat, fat ...... 1 .0 1 Parts per mil- Commodity lion Goat, meat byproducts ...... 0 .1 Goat, meat ...... 0.1 Corn, field, forage ...... 0.005 Grape, raisin ...... 10.0 Corn, field, grain ...... 0.005 Guava ...... 3 .0 Corn, field, stover ...... 0.005 Hog, fat ...... 1 .0 Corn, pop, grain ...... 0.005 Hog, meat byproducts ...... 0 .1 Corn, pop, stover ...... 0.005 Hog, meat ...... 0 .1 Horse, fat ...... 1 .0 1There are no U.S. registered products containing 4- Horse, meat byproducts ...... 0 .1 (dichloroacetyl)-1-oxa-4-azaspiro[4.5]decane as of June 17, Horse, meat ...... 0 .1 2002. Ilama ...... 1 .5 (b) Section 18 emergency exemptions. Jaboticaba ...... 3 .0 Longan ...... 7 .0 [Reserved] Lychee ...... 7 .0 (c) Tolerances with regional registra- Mango ...... 1.0 tions. [Reserved] Melon subgroup 9A ...... 0 .5 Milk, fat (reflecting 0.08 ppm in whole milk) ..... 2 .0 (d) Indirect or inadvertent residues. Nut, tree, crop group 14 ...... 0 .10 [Reserved] Olive ...... 5 .0 Papaya ...... 1 .0 [68 FR 4392, Jan. 29, 2003] Passionfruit ...... 3 .0 Pea, succulent ...... 0 .02 § 180.466 Fenpropathrin; tolerances for Peanut, hay ...... 20.0 residues. Peanut ...... 0 .01 Pistachio ...... 0.10 (a) General. Tolerances are estab- Poultry, fat ...... 0.05 lished for residues of fenpropathrin, in- Poultry, meat byproducts ...... 0.05 Poultry, meat ...... 0 .05 cluding its metabolites and degradates, Pulasan ...... 7 .0 in or on the commodities in the fol- Rambutan ...... 7 .0 lowing table. Compliance with the tol- Sapodilla ...... 1 .0 erance levels specified below is to be Sapote, black ...... 1 .0 Sapote, mamey ...... 1 .0 determined by measuring only Sheep, fat ...... 1 .0 fenpropathrin (alpha-cyano-3-phenoxy- Sheep, meat byproducts ...... 0 .1 benzyl 2,2,3,3 Sheep, meat ...... 0.1 Soursop ...... 1 .5 tetramethylcyclopropanecarboxylate). Spanish lime ...... 7 .0 Squash/Cucumber subgroup 9B ...... 0 .5 Commodity Parts per Star apple ...... 1 .0 million Starfruit ...... 3 .0 Sugar apple ...... 1 .5 Acerola ...... 3.0 Tea, dried 1 ...... 2 .0 Almond, hulls ...... 4 .5 Vegetable, fruiting, group 8–10 ...... 1 .0 Atemoya ...... 1 .5 Wax jambu ...... 3 .0 Avocado ...... 1 .0 Barley, grain ...... 0 .04 1 There are no U.S. registrations as of November 28, 2012, Barley, hay ...... 3 .0 for the use of fenpropathrin on tea, dried. Barley, straw ...... 2 .0 Berry, low growing, subgroup 13–07G ...... 2 .0 (b) Section 18 emergency exemptions. Biriba ...... 1 .5 [Reserved]

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(c) Tolerances with regional registra- (d) Indirect or inadvertent residues. tions. [Reserved] [Reserved] (d) Indirect or inadvertent residues. [76 FR 23497, Apr. 27, 2011] [Reserved] [62 FR 63034, Nov. 26, 1997, as amended at 63 § 180.469 Dichlormid; tolerances for FR 48116, Sept. 9, 1998; 64 FR 3009, Jan. 20, residues. 1999; 65 FR 11242, Mar. 2, 2000; 65 FR 24397, (a) General. Tolerances are estab- Apr. 26, 2000; 65 FR 48620, Aug. 9, 2000; 66 FR lished for residues of dichlormid, in- 64774, Dec. 14, 2001; 67 FR 35049, May 17, 2002; cluding its metabolites and degradates, 70 FR 38789, July 6, 2005; 70 FR 55747, Sept. 23, 2005; 74 FR 12606, Mar. 25, 2009; 77 FR 70908, when used as an inert ingredient (her- Nov. 28, 2012; 78 FR 69569, Nov. 20, 2013] bicide safener) in pesticide formula- tions, in or on the commodities in the § 180.467 Carbon disulfide; tolerances following table. Compliance with the for residues. tolerances is to be determined by meas- Tolerances are established for the uring only dichlormid (2,2-dichloro- nematicide, insecticide, and fungicide N,N-di-2-propenylacetamide). carbon disulfide, from the application Parts per of sodium tetrathiocarbonate, in or on Commodity million the following raw agricultural com- modities: Corn, field, forage ...... 0 .05 Corn, field, grain ...... 0 .05 Corn, field, stover ...... 0 .05 Parts per Corn, pop, grain ...... 0.05 Commodity million Corn, pop, stover ...... 0.05 Almond ...... 0.1 Corn, sweet, forage ...... 0 .05 Almond, hulls ...... 0 .1 Corn, sweet, kernel plus cob with husks re- Grape ...... 0 .1 moved ...... 0 .05 Grapefruit ...... 0 .1 Corn, sweet, stover ...... 0 .05 Lemon ...... 0.1 Orange, sweet ...... 0 .1 (b) Section 18 emergency exemptions. Peach ...... 0 .1 [Reserved] Plum, prune, fresh ...... 0.1 (c) Tolerances with regional registra- tions. [Reserved] [58 FR 33771, June 21, 1993, as amended at 62 (d) Indirect or inadvertent residues. FR 26949, May 16, 1997] [Reserved] § 180.468 Flumetsulam; tolerances for [65 FR 16149, Mar. 27, 2000, as amended at 67 residues. FR 51105, Aug. 7, 2002; 69 FR 58290, Sept. 30, (a) General. Tolerances are estab- 2004; 70 FR 76699, Dec. 28, 2005; 74 FR 37623, lished for residues of the herbicide July 29, 2009; 76 FR 16310, Mar. 23, 2011] flumetsulam, including its metabolites § 180.470 Acetochlor; tolerances for and degradates, in or on the commod- residues. ities in the table in this paragraph. Compliance with the tolerance levels (a) General. Tolerances are estab- specified in this paragraph is to be de- lished for residues of acetochlor, in- termined by measuring only cluding its metabolites and degradates, flumetsulam, N-(2,6-difluorophenyl)-5- in or on the commodities in the table methyl-(1,2,4)-triazolo-(1,5a)-pyrimi- below. Compliance with the tolerance dine-2-sulfonamide, in or on the com- levels specified below is to be deter- modity. mined by measuring only acetochlor, 2- chloro-2’-methyl-6-ethyl-N- Commodity Parts per ethoxymethylacetanilide, and its me- million tabolites containing the ethyl methyl Bean, dry, seed ...... 0 .05 aniline (EMA) moiety and the hydroxy- Corn, field, forage ...... 0 .05 ethyl methyl aniline (HEMA) moiety. Corn, field, grain ...... 0 .05 Both parent and the named metabo- Corn, field, stover ...... 0 .05 Soybean, seed ...... 0 .05 lites shall be determined as ethyl methyl aniline (EMA) and hydroxy- (b) Section 18 emergency exemptions. ethyl methyl aniline (HEMA), and cal- [Reserved] culated as the stoichiometric equiva- (c) Tolerances with regional registra- lents of acetochlor, in or on the fol- tions. [Reserved] lowing commodities:

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Parts per Parts per Commodity million Commodity million

Beet, sugar, dried pulp ...... 0 .50 Grain, cereal, forage, fodder and straw, group Beet, sugar, molasses ...... 0 .80 16, except corn, grain sorghum, rice and Beet, sugar, roots ...... 0 .30 wheat, stover ...... 0 .1 Beet, sugar, tops ...... 0.70 Grain, cereal, forage, fodder and straw, group Corn, field, forage ...... 4 .5 16, except corn, grain sorghum, and wheat, Corn, field, grain ...... 0 .05 straw ...... 0 .3 Corn, field, stover ...... 2 .5 Grain, cereal, group 15, except corn, grain sor- Corn, pop, grain ...... 0.05 ghum, and wheat, grain ...... 0.05 Corn, pop, stover ...... 2.5 Pea and bean, dried shelled, except soybean, Corn, sweet, forage ...... 1 .5 subgroup 6C ...... 0 .05 Corn, sweet, kernels plus cob with husks re- Potato ...... 0 .05 Soybean, forage ...... 0 .7 moved ...... 0 .05 Soybean, hay ...... 1 .0 Corn, sweet, stover ...... 1 .0 Sunflower, seed ...... 0.05 Cotton, gin byproducts ...... 4 .0 Wheat, forage ...... 0 .5 Cotton, undelinted seed ...... 0 .6 Wheat, grain ...... 0 .02 Peanut ...... 0 .20 Wheat, hay ...... 2 .0 Peanut, hay ...... 7.0 Wheat, straw ...... 0 .1 Peanut, meal ...... 0 .25 Sorghum, grain, forage ...... 1.6 Sorghum, grain, grain ...... 0 .05 [72 FR 27468, May 16, 2007, as amended at 74 Sorghum, grain, stover ...... 1 .7 FR 29969, June 24, 2009; 74 FR 47450, Sept. 16, Soybean, meal ...... 1.2 2009; 78 FR 13268, Feb. 27, 2013; 79 FR 3517, Soybean, seed ...... 1 .0 Jan. 22, 2014]

(b) Section 18 emergency exemptions. § 180.471 Furilazole; tolerances for res- [Reserved] idues. (c) Tolerances with regional registra- (a) General. Tolerances are estab- tions. [Reserved] lished for residues of furilazole; 3- (d) Indirect or inadvertent residues. dichloroacetyl-5-(2-furanyl)-2, 2- Tolerances are established for indirect dimethyloxazolidine (CAS Reg. No. or inadvertent residues of acetochlor, 121776–33–8) when used as an inert in- including its metabolites and gredient (safener) in pesticide formula- degradates, in or on the raw agricul- tions in or on the following raw agri- tural commodities in the table to this cultural commodities: paragraph when present therein as a result of application of acetochlor to Commodity Parts per the growing crops in the table to para- million graph (a) of this section. Compliance Corn, field, forage ...... 0 .01 with the tolerance levels specified Corn, field, grain ...... 0 .01 Corn, field, stover ...... 0 .01 below is to be determined by measuring Corn, pop, grain ...... 0.01 only acetochlor, 2-chloro-2’-methyl-6- Corn, pop, stover ...... 0.01 ethyl-N-ethoxymethylacetanilide, and Sorghum, forage ...... 0 .01 Sorghum, grain ...... 0 .01 its metabolites containing the ethyl Sorghum, stover ...... 0 .01 methyl aniline (EMA) moiety and the hydroxyethyl methyl aniline (HEMA) (b) Section 18 emergency exemptions. moiety. Both parent and the named [Reserved] metabolites shall be determined as (c) Tolerances with regional registra- ethyl methyl aniline (EMA) and hy- tions. [Reserved] droxyethyl methyl aniline (HEMA), (d) Indirect or inadvertent residues. and calculated as the stoichiometric [Reserved] equivalents of acetochlor, in or on the [65 FR 8867, Feb. 23, 2000, as amended at 67 following commodities. FR 15735, Apr. 3, 2002; 72 FR 57492, Oct. 10, 2007] Parts per Commodity million § 180.472 Imidacloprid; tolerances for Animal feed, nongrass, group 18, forage ...... 1 .3 residues. Animal feed, nongrass, group 18, hay ...... 3.5 Grain, cereal, forage, fodder and straw, group (a) General. Tolerances are estab- 16, except corn, grain sorghum, rice and lished for residues of the insecticide wheat, forage ...... 0 .5 imidacloprid, including its metabolites Grain, cereal, forage, fodder and straw, group 16, except corn, grain sorghum, rice and and degradates, in or on the commod- wheat, hay ...... 2 .0 ities in the table below. Compliance

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with the tolerance levels specified Commodity Parts per below is to be determined by measuring million only the sum of imidacloprid (1-[6- Hog, meat byproducts ...... 0 .30 chloro-3-pyridinyl) methyl]-N-nitro-2- Hop, dried cones ...... 6 .0 imidazolidinimine) and its metabolites Horse, fat ...... 0 .30 Horse, meat ...... 0 .30 containing the 6-chloropyridinyl moi- Horse, meat byproducts ...... 0 .30 ety, calculated as the stoichiometric Huckleberry ...... 3 .5 equivalent of imidacloprid, in or on the Ilama ...... 0 .30 Jaboticaba ...... 1 .0 following commodities: Juneberry ...... 3 .5 Kava, leaves ...... 4 .0 Parts per Kava, roots ...... 0 .40 Commodity million Leaf petioles subgroup 4B ...... 6 .0 Acerola ...... 1.0 Leafy greens subgroup 4A ...... 3 .5 Almond, hulls ...... 4 .0 Lettuce, head ...... 3.5 Apple ...... 0.5 Lettuce, leaf ...... 3 .5 Apple, wet pomace ...... 3 .0 Lingonberry ...... 3.5 Artichoke, globe ...... 2.5 Longan ...... 3 .0 Aspirated grain fractions ...... 240 Lychee ...... 3 .0 Atemoya ...... 0 .30 Mango ...... 1.0 Avocado ...... 1 .0 Milk ...... 0.10 Banana ...... 0.50 Mustard, black, seed ...... 0 .05 Beet, sugar, molasses ...... 0 .30 Mustard, field, seed ...... 0 .05 Beet, sugar, roots ...... 0 .05 Mustard, Indian, seed ...... 0 .05 Beet, sugar, tops ...... 0.50 Mustard, rapeseed, seed ...... 0 .05 Biriba ...... 0 .30 Mustard, seed ...... 0 .05 Blueberry ...... 3 .5 Nut, tree, group 14 ...... 0 .05 Borage, seed ...... 0 .05 Okra ...... 1.0 Caneberry, subgroup 13-A ...... 2 .5 Onion, dry bulbs, subgroup 3-07A ...... 0 .15 Canistel ...... 1 .0 Onion, green, subgroup 3-07B ...... 2 .5 Canola, seed ...... 0 .05 Papaya ...... 1 .0 Cattle, fat ...... 0.30 Passionfruit ...... 1 .0 Cattle, meat ...... 0 .30 Peanut ...... 0 .45 Cattle, meat byproducts ...... 0.30 Peanut, hay ...... 35 Cherimoya ...... 0 .30 Peanut, meal ...... 0 .75 Citrus, dried pulp ...... 5 .0 Pecan ...... 0 .05 Coffee, bean, green ...... 0 .80 Persimmon ...... 3 .0 Cotton, gin byproducts ...... 4 .0 Pistachio ...... 0.05 Cotton, meal ...... 8 .0 Pomegranate ...... 0 .90 Cotton, undelinted seed ...... 6 .0 Potato, chip ...... 0 .40 Crambe, seed ...... 0.05 Potato, processed potato waste ...... 0 .90 Cranberry ...... 0 .05 Poultry, fat ...... 0.05 Currant ...... 3 .5 Poultry, meat ...... 0 .05 Custard apple ...... 0 .30 Poultry, meat byproducts ...... 0.05 Egg ...... 0 .02 Pulasan ...... 3 .0 Elderberry ...... 3 .5 Rambutan ...... 3 .0 Feijoa ...... 1 .0 Rapeseed, seed ...... 0 .05 Fish ...... 0 .05 Raspberry, wild ...... 2.5 Fish-shellfish, mollusc ...... 0 .05 Safflower, seed ...... 0 .05 Flax, seed ...... 0 .05 Salal ...... 3 .5 Fruit, citrus, group 10 ...... 0 .70 Sapodilla ...... 1 .0 Fruit, pome, group 11 ...... 0.6 Sapote, black ...... 1 .0 Fruit, stone, group 12 ...... 3 .0 Sapote, mamey ...... 1 .0 Goat, fat ...... 0 .30 Sheep, fat ...... 0 .30 Goat, meat ...... 0.30 Sheep, meat ...... 0.30 Goat, meat byproducts ...... 0 .30 Sheep, meat byproducts ...... 0 .30 Gooseberry ...... 3 .5 Soursop ...... 0 .30 Grain, cereal, forage, fodder and straw, group Soybean, forage ...... 8 .0 16, forage, except rice ...... 7 .0 Soybean, hay ...... 35 Grain, cereal, forage, fodder and straw, group Soybean, meal ...... 4.0 16, hay, except rice ...... 6 .0 Soybean, seed ...... 3 .5 Grain, cereal, forage, fodder and straw, group Spanish lime ...... 3 .0 16, stover, except rice ...... 0 .30 Star apple ...... 1 .0 Grain, cereal, forage, fodder and straw, group Starfruit ...... 1 .0 16, straw, except rice ...... 3.0 Strawberry ...... 0 .50 Grain, cereal, group 15, except rice ...... 0 .05 Sugar apple ...... 0 .30 Grape ...... 1 .0 Sunflower, seed ...... 0.05 Grape, juice ...... 1 .5 Tomato, paste ...... 6 .0 Grape, raisin ...... 1 .5 Tomato, puree ...... 3 .0 Guava ...... 1 .0 Vegetable, brassica leafy, group 5 ...... 3 .5 Herbs subgroup 19A, dried herbs ...... 48 Vegetable, cucurbit, group 9 ...... 0.5 Herbs subgroup 19-A, fresh herbs ...... 8 .0 Vegetable, fruiting, group 8 ...... 1.0 Hog, fat ...... 0 .30 Vegetable, leaves of root and tuber, group 2 ..... 4 .0 Hog, meat ...... 0 .30 Vegetable, legume, group 6, except soybean .... 4 .0

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Parts per [75 FR 22251, Apr. 28, 2010, as amended at 78 Commodity million FR 33743, June 5, 2013]

Vegetable, root and tuber, group 1, except § 180.473 Glufosinate ammonium; tol- sugar beet ...... 0 .40 Watercress ...... 3 .5 erances for residues. Watercress, upland ...... 3 .5 (a) General. Tolerances are estab- Wax jambu ...... 1 .0 lished for residues of the herbicide (b) Section 18 emergency exemptions. glufosinate ammonium, including its Time-limited tolerances are estab- metabolites and degradates, in or on lished for residues of the insecticide the commodities in the table below. imidacloprid, including its metabolites Compliance with the tolerance levels and degradates in connection with use specified below is to be determined by of the pesticide under a Section 18 measuring the sum of glufosinate am- emergency exemption granted by EPA. monium, butanoic acid, 2-amino-4- Compliance with the tolerance levels (hydroxymethylphosphinyl) specified below is to be determined by monoammonium salt, and its metabo- measuring only the sum of lites, 2-(acetylamino)-4- imidacloprid (1-[6-chloro-3- (hydroxymethyl phosphinyl)butanoic pyridinyl)methyl]-N-nitro-2- acid, and 3- imidazolidinimine) and its metabolites (hydroxymethylphosphinyl)propanoic containing the 6-chloropyridinyl moi- acid, expressed as 2-amino-4- ety, calculated as the stoichiometric (hydroxymethylphosphinyl)butanoic equivalent of imidacloprid. These tol- acid equivalents: erances will expire and are revoked on Parts per the dates specified in the following Commodity million table: Almond, hulls ...... 0 .50 Apple ...... 0.05 Expiration/ Banana ...... 0.30 Commodity Parts per revocation million date Banana, pulp ...... 0 .20 Beet, sugar, molasses ...... 5 .0 Sugarcane, cane ...... 6.0 12/31/15 Beet, sugar, roots ...... 0 .9 Sugarcane, molasses ...... 50 12/31/15 Beet, sugar, tops (leaves) ...... 1 .5 Bushberry subgroup 13B ...... 0 .15 Canola, meal ...... 1 .1 (c) Tolerances with regional registra- Canola, seed ...... 0 .40 tions. [Reserved] Cattle, fat ...... 0.40 (d) Indirect or inadvertent residues. Cattle, meat ...... 0 .15 Cattle, meat byproducts ...... 6.0 Tolerances are established for indirect Corn, field forage ...... 4.0 or inadvertent residues of the insecti- Corn, field, grain ...... 0 .20 cide imidacloprid, including its me- Corn, field, stover ...... 6 .0 tabolites and degradates, in or on the Corn, sweet, forage ...... 1 .5 Corn, sweet, kernels plus cob with husks re- commodities in the table below. Com- moved ...... 0 .30 pliance with the tolerance levels speci- Corn, sweet, stover ...... 6 .0 fied below is to be determined by meas- Cotton, gin byproducts ...... 15 Cotton, undelinted seed ...... 4 .0 uring only the sum of imidacloprid (1- Egg ...... 0 .15 [6-chloro-3-pyridinyl) methyl]-N-nitro- Fruit, citrus, group 10–10 ...... 0 .15 2-imidazolidinimine) and its metabo- Fruit, pome, group 11–10 ...... 0 .25 lites containing the 6-chloropyridinyl Fruit, stone, group 12–12 ...... 0 .25 Goat, fat ...... 0 .40 moiety, calculated as the stoichio- Goat, meat ...... 0.15 metric equivalent of imidacloprid, in Goat, meat byproducts ...... 6 .0 or on the following commodities, when Grain aspirated fractions ...... 25 Grape ...... 0 .05 present therein as a result of the appli- Hog, fat ...... 0 .40 cation of the pesticide to growing crops Hog, meat ...... 0 .15 listed in this section and other non- Hog, meat byproducts ...... 6 .0 food crops as follows: Horse, fat ...... 0 .40 Horse, meat ...... 0 .15 Horse, meat byproducts ...... 6 .0 Parts per Commodity million Juneberry ...... 0 .10 Lingonberry ...... 0.10 Rice, grain ...... 0 .05 Milk ...... 0.15 Vegetable, foliage of legume, group 7 ...... 2 .5 Nut, tree, group 14 ...... 0 .10 Vegetable, legume, group 6 ...... 0 .3 Olive ...... 0 .15 Pistachio ...... 0.10

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Commodity Parts per § 180.474 Tebuconazole; tolerances for million residues. Potato ...... 0 .80 (a) General. (1) Tolerances are estab- Potato, chips ...... 1 .6 lished for residues of tebuconazole, Potato granules/flakes ...... 2 .0 alpha-[2-(4-chlorophenyl)ethyl]-alpha- Poultry, fat ...... 0.15 Poultry, meat ...... 0 .15 (1,1-dimethylethyl)-1H-1,2,4-triazole-1- Poultry, meat byproducts ...... 0.60 ethanol, including its metabolites and Rice, grain ...... 1 .0 degradates, in or on the commodities Rice, hull ...... 2 .0 in the table below. Compliance with Rice, straw ...... 2 .0 the tolerance levels specified below is Salal ...... 0 .10 to be determined by measuring only Sheep, fat ...... 0 .40 tebuconazole [ -[2-(4-chlorophenyl) Sheep, meat ...... 0.15 a Sheep, meat byproducts ...... 6 .0 ethyl]-a-(1,1-dimethylethyl)-1H-1,2,4- Soybean ...... 2.0 triazole-1-ethanol], in or on the com- Soybean, hulls ...... 5 .0 modity.

Parts per (b) Section 18 emergency exemptions. Commodity million [Reserved] (c) Tolerances with regional restric- Almond, hulls ...... 6 .0 Apple, wet pomace ...... 0 .1 tions. [Reserved] Asparagus ...... 0.05 (d) Indirect or inadvertent residues. Banana ...... 0.05 Barley, grain ...... 0 .3 Tolerances are established for indirect Barley, hay ...... 7 .0 or inadvertent residues of glufosinate Barley, straw ...... 3 .5 ammonium, including its metabolites Bean, dry seed ...... 0 .1 Bean, succulent ...... 0 .1 and degradates, in or on the commod- Beet, garden, roots ...... 0 .70 ities in the table below, as a result of Beet, garden, tops ...... 7 .0 the application of glufosinate ammo- Brassica, leafy greens, subgroup 5B ...... 2 .5 nium to crops listed in paragraph (a) of Cherry, sweet, pre- and post-harvest ...... 5 .0 Cherry, tart, pre- and post-harvest ...... 5 .0 this section. Compliance with the tol- Coffee, green bean 1 ...... 0 .15 erance levels specified below is to be Coffee, roasted bean 1 ...... 0 .3 determined by measuring the sum of Corn, field, forage ...... 4 .0 Corn, field, grain ...... 0 .05 glufosinate ammonium, butanoic acid, Corn, field, stover ...... 3 .5 2-amino-4-(hydroxymethylphosphinyl) Corn, pop, grain ...... 0.05 monoammonium salt, and its metabo- Corn, pop, stover ...... 3.5 Corn, sweet, forage ...... 7 .0 lite, 3-(hydroxymethylphosphinyl) pro- Corn, sweet, kernel plus cob with husks re- panoic acid, expressed as 2-amino-4- moved ...... 0 .5 (hydroxymethylphosphinyl)butanoic Corn, sweet, stover ...... 6 .0 Cotton, gin byproducts ...... 25 .0 acid equivalents. Cotton, undelinted seed ...... 2 .0 Fruit, pome, group 11 ...... 0.05 Commodity Parts per Fruit, stone, group 12, except cherry ...... 1 .0 million Grain, aspirated fractions ...... 16.0 Grape ...... 5 .0 Barley, hay ...... 0 .40 Grass, forage ...... 8 .0 Barley, straw ...... 0 .40 Grass, hay ...... 25 .0 Buckwheat, fodder ...... 0 .40 Grass, seed screenings ...... 55.0 Buckwheat, forage ...... 0 .40 Grass, straw ...... 30 .0 Oat, forage ...... 0 .40 Hop, dried cones ...... 35 .0 Oat, hay ...... 0.40 Lychee ...... 1 .6 Mango, postharvest ...... 0 .15 Oat, straw ...... 0.40 Nut, tree, group 14 ...... 0 .05 Rye, forage ...... 0 .40 Oat, forage ...... 0 .10 Rye, straw ...... 0 .40 Oat, grain ...... 0 .15 Teosinte ...... 0 .40 Oat, hay ...... 0.10 Triticale ...... 0.40 Oat, straw ...... 0.10 Wheat, forage ...... 0 .40 Onion, bulb, subgroup 3-07A ...... 0 .2 Wheat, hay ...... 0 .40 Onion, green, subgroup 3-07B ...... 1 .3 Orange 1 ...... 1 .0 Wheat, straw ...... 0 .40 Orange, oil 1 ...... 10 Peach ...... 1 .0 [68 FR 55849, Sept. 29, 2003, as amended at 71 Peanut ...... 0 .1 Pistachio ...... 0.05 FR 25945, May 3, 2006; 72 FR 72625, Dec. 21, Plum, pre- and post-harvest ...... 1 .0 2007; 76 FR 23497, Apr. 27, 2011; 77 FR 59113, Soybean, forage ...... 25 Sept. 26, 2012] Soybean, hay ...... 50

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(d) Indirect or inadvertent residues. Commodity Parts per million [Reserved] Soybean, seed ...... 0 .08 [59 FR 39464, Aug. 3, 1994] Sunflower, seed ...... 0.05 Sunflower, meal ...... 0 .2 EDITORIAL NOTE: For FEDERAL REGISTER ci- Sunflower, refined oil ...... 0.2 tations affecting § 180.474, see the List of CFR Vegetable, cucurbit, group 9 ...... 0.4 Sections Affected, which appears in the Vegetable, fruiting, group 8–10 ...... 1 .3 Finding Aids section of the printed volume Wheat, forage ...... 3 .0 and at www.fdsys.gov. Wheat, germ ...... 0 .20 Wheat, grain ...... 0 .15 § 180.475 Difenoconazole; tolerances Wheat, hay ...... 7 .0 for residues. Wheat, shorts ...... 0 .20 (a) General. (1) Tolerances are estab- Wheat, straw ...... 1 .5 lished for residues of difenoconazole, 1There are no U.S. registrations. including its metabolites and (2) Tolerances are established for res- degradates, in or on the commodities idues of the fungicide tebuconazole, in- in the following table. Compliance with cluding its metabolites and degradates, the tolerance levels specified below is in or on the commodities in the fol- to be determined by measuring only lowing table. Compliance with the tol- difenoconazole, 1-[2-[2-chloro-4-(4- chlorophenoxy)phenyl]-4-methyl-1,3- erance levels specified in the following dioxolan-2-ylmethyl]-1H-1,2,4-triazole, table is to be determined by measuring in or on the following raw agricultural only the sum of tebuconazole (alpha-[2- commodities: (4-chlorophenyl)ethyl]-alpha-(1,1-

dimethylethyl)-1H-1,2,4-triazole-1-eth- Commodity Parts per anol) and its diol metabolite (1-(4- million chlorophenyl)-4,4-dimethyl-3-(1H -1,2,4- Almond, hulls ...... 7 .0 triazole-1-yl-methyl)-pentane-3,5-diol), Apple, wet pomace ...... 25 Aspirated grain fractions ...... 95 calculated as the stoichiometric equiv- Banana1 ...... 0 .2 alent of tebuconzole, in or on the com- Barley, grain ...... 0 .1 modity. Barley, hay ...... 0 .05 Barley, straw ...... 0 .05 Beet, sugar ...... 0 .3 Parts per Commodity million Beet, sugar, dried pulp ...... 1 .9 Berry, low growing, subgroup 13–07G, except cranberry ...... 2.5 Cattle, meat byproducts ...... 0.2 Brassica, head and stem, subgroup 5A ...... 1 .9 Goat, meat byproducts ...... 0 .2 Brassica, leafy green, subgroup 5B ...... 35 Horse, meat byproducts ...... 0 .2 Bushberry subgroup 13–07B ...... 4 .0 Milk ...... 0.1 Carrot ...... 0 .50 Sheep, meat byproducts ...... 0 .2 Citrus, dried pulp ...... 2 .0 Citrus, oil ...... 25 Corn, sweet, forage ...... 0 .01 (b) Section 18 emergency exemptions. Corn, sweet, kernel plus cob with husks re- [Reserved] moved ...... 0 .01 (c) Tolerances with regional registra- Corn, sweet, stover ...... 0 .01 Cotton, gin byproducts ...... 0 .05 tions. Tolerances are established for Cotton, undelinted seed ...... 0 .05 residues of the fungicide tebuconazole, Dragonfruit1 ...... 1 .5 including its metabolites and Fruit, citrus, group 10–10 ...... 0 .60 Fruit, pome, group 11–10 ...... 5 .0 degradates, in or on the commodities Fruits, stone, group 12 ...... 2 .5 in the following table. Compliance with Grape ...... 4 .0 the tolerance levels specified below is Grape, raisin ...... 6 .0 Mango 1 ...... 0.07 to be determined by measuring only Nut, tree, group 14 ...... 0 .03 tebuconazole, alpha-[2-(4- Oat, forage ...... 0 .15 chlorophenyl)ethyl]-alpha-(1,1- Oat, grain ...... 0 .01 Oat, hay ...... 0.05 dimethylethyl)-1H-1,2,4-triazole-1-eth- Oat, straw ...... 0.05 anol, in or on the commodity. Onion, bulb, subgroup 3-07A ...... 0 .20 Onion, green, subgroup 3-07B ...... 6 .0 Parts per Papaya1 ...... 0 .30 Commodity million Pea and bean, dried shelled, except soybean, subgroup 6C ...... 0 .20 Turnip, roots ...... 0 .5 Pea, field, hay ...... 40 Turnip, tops ...... 7.0 Pea, field, vines ...... 10 Pistachio ...... 0.03

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Parts per EDITORIAL NOTE: For FEDERAL REGISTER ci- Commodity million tations affecting § 180.475, see the List of CFR Sections Affected, which appears in the Potato, wet peel ...... 7 .3 Finding Aids section of the printed volume Rapeseed subgroup 20A ...... 0 .10 Rye, forage ...... 0 .15 and at www.fdsys.gov. Rye, grain ...... 0.01 Rye, straw ...... 0 .05 § 180.476 Triflumizole; tolerances for Soybean, hulls ...... 0 .20 residues. Soybean, seed ...... 0 .15 Turnip, greens ...... 35 (a) General. (1) Tolerances are estab- Vegetable, cucurbit, group 9 ...... 0.70 lished for residues of the fungicide Vegetable, fruiting, group 8–10 ...... 0 .60 Vegetable, tuberous and corm, subgroup 1C ..... 4.0 triflumizole, including its metabolites Wax jambu 1 ...... 1 .5 and degradates, in or on the commod- Wheat, forage ...... 0 .1 ities listed in the table below. Compli- Wheat, grain ...... 0 .1 ance with the tolerance levels specified Wheat, hay ...... 0 .05 Wheat, straw ...... 0 .1 below is to be determined by measuring 1There are no U.S. registrations. only the parent compound triflumizole, 1-(1-((4-chloro-2- (2) Tolerances are established for res- (trifluoromethyl)phenyl)imino)-2- idues of difenoconazole, including its propoxyethyl)-1 H -imidazole, and its metabolites and degradates, in the metabolites containing the 4-chloro-2- commodities in the table below. Com- trifluoromethylaniline moiety, cal- pliance with the tolerance levels speci- culated as stoichiometric equivalent of fied below is to be determined by meas- the parent compound. uring the sum of difenoconazole, 1-[2- [2-chloro-4-(4-chlorophenoxy)phenyl]-4- Commodity Parts per methyl-1,3-dioxolan-2-ylmethyl]-1H- million 1,2,4-triazole, and its metabolite, CGA– Apple, dry pomace ...... 2.0 205375, 1-[2-chloro-4-(4-chloro- Apple, wet pomace ...... 2 .0 Berry, low growing, subgroup 13–07G, except phenoxy)phenyl]-2-[1,2,4]triazol-1-yl- cranberry ...... 2.0 ethanol, calculated as the stoichio- Brassica, head and stem, subgroup 5A ...... 8 .0 metric equivalent of difenoconazole, in Brassica, leafy greens, subgroup 5B ...... 40 Canistel ...... 2 .5 the following commodities: Cherry, sweet ...... 1 .5 Cherry, tart ...... 1 .5 Commodity Parts per Cilantro, leaves ...... 35 million Fruit, pome, group 11–10 ...... 0 .50 Fruit, small, vine climbing, except fuzzy Cattle, fat ...... 0.10 kiwifruit, subgroup 13–07F ...... 2 .5 Cattle, liver ...... 0 .40 Grape, dried pomace ...... 15 .0 Cattle, meat ...... 0 .05 Grape, raisin, waste ...... 10 .0 Cattle, meat byproduct (except liver) ...... 0 .10 Grape, wet pomace ...... 15 .0 Egg ...... 0 .02 Hazelnut ...... 0 .05 Goat, fat ...... 0 .10 Hop, dried cones ...... 50 Goat, liver ...... 0.40 Leafy greens subgroup 4A, except spinach ...... 35 Goat, meat ...... 0.05 Mango ...... 2.5 Goat, meat byproduct (except liver) ...... 0.10 Papaya ...... 2 .5 Hog, fat ...... 0 .10 Pineapple ...... 4.0 Hog, liver ...... 0 .40 Sapodilla ...... 2 .5 Hog, meat ...... 0 .05 Sapote, black ...... 2 .5 Hog, meat byproduct (except liver) ...... 0 .10 Sapote, mamey ...... 2 .5 Horse, fat ...... 0 .10 Star apple ...... 2 .5 Horse, liver ...... 0 .40 Swiss chard ...... 18 Horse, meat ...... 0 .05 Tomato ...... 1.5 Horse, meat byproduct (except liver) ...... 0 .10 Turnip, greens ...... 40 Milk ...... 0.02 Sheep, fat ...... 0 .10 Vegetable, cucurbit, Group 9 ...... 0 .5 Sheep, liver ...... 0.40 Sheep, meat ...... 0.05 (2) Tolerances are established for res- Sheep, meat byproduct (except liver) ...... 0.10 idues of the fungicide triflumizole, in- cluding its metabolites and degradates, (b) Section 18 emergency exemptions. in or on the commodities of animal ori- [Reserved] gin listed in the table below. Compli- (c) Tolerances with regional registra- ance with the tolerance levels specified tions. [Reserved] below is to be determined by measuring (d) Indirect or inadvertent residues. only the parent compound triflumizole, [Reserved] 1-(1-((4-chloro-2- [64 FR 36254, July 6, 1999] (trifluoromethyl)phenyl)imino)-2-

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propoxyethyl)-1 H -imidazole, the me- Commodity Parts per tabolite 4-chloro-2-hydroxy-6- million trifluoromethylaniline sulfate, and Cotton, gin byproducts ...... 3 .0 other metabolites containing the 4- Cotton, undelinted seed ...... 0 .2 chloro-2-trifluoromethylaniline moi- Soybean, hulls ...... 0 .02 ety, calculated as the parent com- Soybean, seed ...... 0 .01 pound. (b) Section 18 emergency exemptions. Parts per [Reserved] Commodity million (c) Tolerances with regional registra- Cattle, fat ...... 0.5 tions. [Reserved] Cattle, meat ...... 0 .05 Cattle, meat byproducts ...... 0.5 (d) Indirect or inadvertent residues. Egg ...... 0 .05 [Reserved] Goat, fat ...... 0 .5 Goat, meat ...... 0.05 [65 FR 33702, May 24, 2000, as amended at 71 Goat, meat byproducts ...... 0 .5 FR 11533, Mar. 8, 2006; 76 FR 23497, Apr. 27, Hog, fat ...... 0 .5 Hog, meat ...... 0 .05 2011] Hog, meat byproducts ...... 0 .5 Horse, fat ...... 0 .5 § 180.478 Rimsulfuron; tolerances for Horse, meat ...... 0 .05 residues. Horse, meat byproducts ...... 0 .5 Milk ...... 0.05 (a) General. Tolerances are estab- Poultry, fat ...... 0.05 Poultry, meat ...... 0 .05 lished for residues of the herbicide Poultry, meat byproducts ...... 0.1 rimsulfuron, including its metabolites Sheep, fat ...... 0 .5 and degradates, in or on the commod- Sheep, meat ...... 0.05 Sheep, meat byproducts ...... 0 .5 ities in the table below. Compliance with the tolerance levels specified (b) Section 18 emergency exemptions. below is to be determined by measuring [Reserved] only rimsulfuron, N-((4,6- (c) Tolerances with regional registra- dimethoxypyrimidin-2- tions. [Reserved] yl)aminocarbonyl)-3-(ethylsulfonyl)-2- (d) Indirect or inadvertent residues. pyridinesulfonamide), in or on the [Reserved] commodities. [65 FR 33702, May 24, 2000, as amended at 67 Parts per FR 40228, June 12, 2002; 67 FR 54587, Aug. 23, Commodity million 2002; 70 FR 7047, Feb. 10, 2005; 70 FR 17915, Apr. 8, 2005; 71 FR 13279, Mar. 15, 2006; 71 FR Almond, hulls ...... 0 .09 49358, Aug. 23, 2006; 74 FR 26543, June 3, 2009; Bushberry, subgroup 13–07B ...... 0.01 74 FR 46376, Sept. 9, 2009; 76 FR 34885, June 15, Caneberry, subgroup 13–07A ...... 0 .01 2011; 79 FR 12408, Mar. 5, 2014] Chicory, roots ...... 0 .01 Chicory, tops ...... 0 .01 § 180.477 Flumiclorac pentyl; toler- Corn, field, forage ...... 0 .4 ances for residues. Corn, field, grain ...... 0 .1 Corn, field, stover ...... 2 .5 (a) General. Tolerances are estab- Fruit, citrus, group 10 ...... 0 .01 lished for residues of the herbicide Fruit, pome, group 11 ...... 0.01 flumiclorac pentyl, including its me- Fruit, stone, group 12 ...... 0 .01 tabolites and degradates, in or on the Grain, aspirated fractions ...... 4 .5 commodities in the table in this para- Grape ...... 0 .01 graph. Compliance with the tolerance Nut, tree, group 14 ...... 0 .01 levels specified in this paragraph is to Pistachio ...... 0.01 Potato ...... 0 .1 be determined by measuring only Soybean, forage ...... 0 .25 flumiclorac pentyl, pentyl(2-chloro-4- Soybean, hay ...... 1 .2 fluoro-5-(1,3,4,5,6,7-hexahydro-1,3-dioxo- Soybean, hulls ...... 0 .04 2H-isoindol-2-yl)phenoxy)acetate, in or Soybean, seed ...... 0 .01 on the commodity. Tomato ...... 0.05

Commodity Parts per (b) Section 18 emergency exemptions. million [Reserved] Corn, field, forage ...... 0 .01 (c) Tolerances with regional registra- Corn, field, grain ...... 0 .01 tions. [Reserved] Corn, field, stover ...... 0 .01

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(d) Indirect or inadvertent residues. Commodity Parts per [Reserved] million [63 FR 16696, Apr. 6, 1998, as amended at 72 Asparagus ...... 0.8 FR 41913, Aug. 1, 2007; 74 FR 67137, Dec. 18, Bean, dry, seed ...... 0 .05 Bushberry, subgroup 13-07B ...... 0 .05 2009; 77 FR 3625, Jan. 25, 2012; 77 FR 46306, Caneberry subgroup 13–07A ...... 0.05 Aug. 3, 2012] Corn, field, forage ...... 0 .2 Corn, field, grain ...... 0 .05 § 180.479 Halosulfuron-methyl; toler- Corn, field, stover ...... 0 .8 ances for residues. Corn, pop, grain ...... 0.05 Corn, pop, stover ...... 0.8 (a) General. (1) Tolerances are estab- Corn, sweet, forage ...... 0 .2 lished for residues of the herbicide Corn, sweet, kernel plus cob with husks re- halosulfuron-methyl, methyl 5-[(4,6- moved ...... 0 .05 Corn, sweet, stover ...... 0 .8 dimethoxy-2-pyrimidiny)amino] Cotton, gin byproducts ...... 0 .05 carbonylaminosulfonyl]-3-chloro-1- Cotton, undelinted seed ...... 0 .05 methyl-1H-pyrazole-4-carboxylate, in- Grass, forage, fodder, and hay, group 17, for- age ...... 20 cluding its metabolites and degradates, Grass, forage, fodder, and hay, group 17, hay 0 .5 in or on the commodities in the fol- Melon subgroup 9A ...... 0 .1 lowing table. Compliance with the tol- Millet, proso, forage ...... 10 erance levels specified in the following Millet, proso, grain ...... 0 .01 Millet, proso, hay ...... 0 .01 table is to be determined by measuring Millet, proso, straw ...... 0 .01 only those halosulfuron-methyl resi- Nut, tree, group 14 ...... 0 .05 dues containing the 3- Okra ...... 0.05 Pea and bean, succulent shelled, subgroup 6 .. 0 .05 chlorosulfonamide (3-CSA) moiety, ex- Pea and bean, succulent shelled, subgroup 6B 0 .05 pressed as the stoichiometric equiva- Pistachio ...... 0.05 lent of halosulfuron-methyl, in or on Rhubarb ...... 0 .05 Rice, grain ...... 0 .05 the commodity. Rice, straw ...... 0 .2 Sorghum, grain, forage ...... 0.05 Parts per Sorghum, grain, grain ...... 0 .05 Commodity million Sorghum, grain, stover ...... 0 .1 Cattle, fat ...... 0.05 Soybean, seed ...... 0 .05 Cattle, meat ...... 0 .05 Squash/Cucumber subgroup 9B ...... 0 .5 Cattle, meat byproducts ...... 1.0 Sugarcane, cane ...... 0.05 Goat, fat ...... 0 .05 Vegetable, fruiting, group 8 ...... 0.05 Goat, meat ...... 0.05 Vegetable, tuberous and corm, subgroup 1C ... 0.05 Goat, meat byproducts ...... 1 .0 Hog, meat byproducts ...... 0 .1 (b) Section 18 emergency exemptions. Horse, fat ...... 0 .05 Horse, meat ...... 0 .05 [Reserved] Horse, meat byproducts ...... 1 .0 (c) Tolerances with regional registra- Milk ...... 0.05 tions. [Reserved] Sheep, fat ...... 0 .05 Sheep, meat ...... 0.05 (d) Indirect or inadvertent residues. Sheep, meat byproducts ...... 1 .0 [Reserved] [64 FR 25448, May 12, 1999, as amended at 65 (2) Tolerances are established for res- FR 58433, Sept. 29, 2000; 66 FR 66340, Dec. 26, idues of the herbicide halosulfuron- 2001; 66 FR 66786, Dec. 27, 2001; 67 FR 45649, methyl, methyl 5-[(4,6-dimethoxy-2- July 10, 2002; 67 FR 59192, Sept. 20, 2002; 70 FR pyrimidiny)amino] 51622, Aug. 31, 2005; 72 FR 8927, Feb. 28, 2007; carbonylaminosulfonyl]-3-chloro-1- 74 FR 48401, Sept. 23, 2009; 75 FR 46853, Aug. methyl-1H-pyrazole-4-carboxylate, in- 4, 2010; 76 FR 34886, June 15, 2011; 77 FR 71561, cluding its metabolites and degradates, Dec. 3, 2012; 78 FR 53051, Aug. 28, 2013] in or on the commodities in the fol- § 180.480 Fenbuconazole; tolerances lowing table. Compliance with the tol- for residues. erance levels specified in the following table is to be determined by measuring (a) Tolerances are established for res- only halosulfuron-methyl. idues of the fungicide fenbuconazole, including its metabolites and Commodity Parts per degradates, in or on the commodities million in the table below. Compliance with Alfalfa, forage ...... 1.0 the tolerance levels specified below is Alfalfa, hay ...... 2.0 to be determined by measuring only Almond, hulls ...... 0 .2 Apple ...... 0.05 the sum of fenbuconazole, alpha-[2-(4- Artichoke ...... 0 .05 chlorophenyl)-ethyl]-alpha-phenyl-3-

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(1H-1,2,4-triazole)-1-propanenitrile, and below is to be determined by measuring its metabolites RH-9129, cis-5-(4- only prosulfuron, 1-(4-methoxy-6-meth- chlorophenyl)-dihydro-3-phenyl-3-(1H- yl-triazin-2-yl)-3-[2-(3,3,3- 1,2,4-triazole-1-ylmethyl)-2-3 H- trifluoropropyl)-phenylsulfonyl]-urea, furanone, and RH-9130, trans-5-(4- in or on the commodity. chlorophenyl)-dihydro-3-phenyl-3-(1H- Parts per 1,2,4-triazole-1-ylmethyl)-2-3 H- Commodity million furanone, calculated as the stoichio- metric equivalent of fenbuconazole, in Grain, cereal, forage, fodder, and straw, group 16, except rice, fodder ...... 0 .01 or on the following agricultural com- Grain, cereal, forage, fodder, and straw, group modities. 16, except rice, forage ...... 0 .10 Grain, cereal, forage, fodder, and straw, group Commodity Parts per 16, except rice, hay ...... 0 .20 million Grain, cereal, forage, fodder, and straw, group 16, except rice, straw ...... 0 .02 Almond ...... 0.05 Grain, cereal, group 15, except rice ...... 0 .01 Almond, hulls ...... 1 .0 Apple ...... 0.4 Apple, wet pomace ...... 1 .0 (b) Section 18 emergency exemptions. Banana ...... 0.3 [Reserved] Beet, sugar, dried pulp ...... 1 .0 (c) Tolerances with regional registra- Beet, sugar, molasses ...... 0 .4 Beet, sugar, roots ...... 0 .3 tion. [Reserved] Beet, sugar, tops ...... 9.0 (d) Indirect or inadvertent residues. Bushberry subgroup 13B ...... 0 .3 [Reserved] Cattle, meat byproducts ...... 0.05 Citrus, dried pulp ...... 5 .0 [74 FR 67118, Dec. 18, 2009] Citrus, oil ...... 40.0 Cranberry ...... 0 .5 § 180.482 Tebufenozide; tolerances for Fruit, citrus, group 10 ...... 1 .0 Fruit, stone, group 12 ...... 1 .0 residues. Goat, meat byproducts ...... 0 .05 (a) General. (1) Tolerances are estab- Grain, aspirated fractions ...... 6 .0 Grape 1 ...... 1 .0 lished for residues of the insecticide Horse, meat byproducts ...... 0 .05 tebufenozide, including its metabolites Peanut ...... 0 .1 and degradates, in or on the commod- Pecan ...... 0 .05 ities in the table in this paragraph. Pepper ...... 1 .0 Sheep, meat byproducts ...... 0 .05 Compliance with the tolerance levels Wheat, forage ...... 4 .0 specified in this paragraph is to be de- Wheat, grain ...... 0 .1 termined by measuring only Wheat, hay ...... 8 .0 Wheat, straw ...... 8 .0 tebufenozide, 3,5-dimethylbenzoic acid 1-(1,1-dimethylethyl)-2-(4- 1There are no United States registrations for grape as of August 2006. ethylbenzoyl)hydrazide, in or on the commodity. (b) Section 18 emergency exemptions. [Reserved] Commodity Parts per (c) Tolerances with regional registra- million tions. [Reserved] Almond, hulls ...... 25 (d) Indirect or inadvertent residues. Apple ...... 1.0 [Reserved] Apple, dry pomace ...... 3.0 Apple, wet pomace ...... 3 .0 [60 FR 11032, Mar. 1, 1995] Berry group 13 ...... 3 .0 Brassica, head and stem, subgroup 5A ...... 5 .0 EDITORIAL NOTE: For FEDERAL REGISTER ci- Brassica, leafy greens, subgroup 5B ...... 10 .0 tations affecting § 180.480, see the List of CFR Canola, refined oil ...... 4 .0 Sections Affected, which appears in the Canola, seed ...... 2 .0 Finding Aids section of the printed volume Citrus, oil ...... 15.0 and at www.fdsys.gov. Cotton ...... 1 .5 Cotton, gin byproducts ...... 30 Cranberry ...... 1 .0 § 180.481 Prosulfuron; tolerances for Fruit, citrus, group 10 ...... 0 .80 residues. Fruit, pome ...... 1.5 Grape ...... 3 .0 (a) General. Tolerances are estab- Kiwifruit 1 ...... 0.5 lished for residues of the herbicide Leaf petioles subgroup 4B ...... 2 .0 prosulfuron and its metabolites and Leafy greens subgroup 4A ...... 10 .0 degradates in or on the commodities in Nut, tree, group 14 ...... 0 .1 Peppermint, tops ...... 10 .0 the table below. Compliance with the Pistachio ...... 0.1 tolerance levels specified in the table Spearmint, tops ...... 10 .0

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tabolites and degradates, in or on the Commodity Parts per million commodities in the table in this para- Turnip, greens ...... 9.0 graph when present therein as a result Turnip, roots ...... 0 .3 of the application of tebufenozide to Vegetable, fruiting, group 8 ...... 1.0 growing crops listed in the table to Vegetable, tuberous and corm, except potato, subgroup 1D ...... 0 .015 paragraph (a)(1) of this section. Com- Walnut ...... 0 .1 pliance with the tolerance levels speci- 1There are no U.S. registrations on kiwifruit as of June 15, fied in this paragraph is to be deter- 1999. mined by measuring only the sum of (2) Tolerances are established for res- tebufenozide, 3,5-dimethylbenzoic acid idues of the insecticide tebufenozide, 1-(1,1-dimethylethyl)-2-(4- including its metabolites and ethylbenzoyl)hydrazide, and its me- degradates, in or on the commodities tabolite, 3,5-dimethylbenzoic acid 1- in the table in this paragraph. Compli- (1,1-dimethylethyl)-2-(4-(1-hydroxy- ance with the tolerance levels specified ethyl)benzoyl)hydrazide, calculated as in this paragraph is to be determined the stoichiometric equivalent of by measuring only the sum of tebufenozide, in or on the commodity. tebufenozide, 3,5-dimethylbenzoic acid Parts per 1-(1,1-dimethylethyl)-2-(4- Commodity million ethylbenzoyl)hydrazide, and its me- Animal feed, nongrass, group 18 ...... 1 .0 tabolites, 3,5-dimethylbenzoic acid 1- Grain, cereal, forage, fodder and straw, group (1,1-dimethylethyl)-2-((4- 16 ...... 1 .0 carboxymethyl)benzoyl)hydrazide, 3- Grass, forage, fodder and hay, group 17 ...... 1 .0 hydroxymethyl-5-methylbenzoic acid 1- Vegetable, foliage of legume, group 7 ...... 0 .20 (1,1-dimethylethyl)-2-(4- ethylbenzoyl)hydrazide, stearic acid [60 FR 29347, May 31, 1995] conjugate of 3-hydroxymethyl-5- EDITORIAL NOTE: For FEDERAL REGISTER ci- methylbenzoic acid 1-(1,1- tations affecting § 180.482, see the List of CFR dimethylethyl)-2-(4- Sections Affected, which appears in the ethylbenzoyl)hydrazide, and 3- Finding Aids section of the printed volume hydroxymethyl-5-methylbenzoic acid 1- and at www.fdsys.gov. (1,1-dimethylethyl)-2-(4-(1-hydroxy- ethyl)benzoyl)hydrazide, calculated as § 180.484 Flutolanil; tolerances for res- idues. the stoichiometric equivalent of tebufenozide, in or on the commodity. (a) General. Tolerances are estab- lished for residues of flutolanil, N-(3-(1- Commodity Parts per methylethoxy) phenyl)-2- million (trifluoromethyl)benzamide, including Cattle, fat ...... 0.1 its metabolites and degradates, in or Cattle, meat ...... 0 .08 on the commodities in the table below. Cattle, meat byproducts ...... 0.08 Goat, fat ...... 0 .1 Compliance with the tolerance levels Goat, meat ...... 0.08 specified below is to be determined by Goat, meat byproducts ...... 0 .08 measuring only flutolanil and its me- Hog, fat ...... 0 .1 Hog, meat ...... 0 .08 tabolites converted to 2- Hog, meat byproducts ...... 0 .08 (trifluoromethyl) benzoic acid and cal- Horse, fat ...... 0 .1 culated as flutolanil, in or on the fol- Horse, meat ...... 0 .08 Horse, meat byproducts ...... 0 .08 lowing commodities: Milk ...... 0.04 Sheep, fat ...... 0 .1 Commodity Parts per Sheep, meat ...... 0.08 million Sheep, meat byproducts ...... 0 .08 Cattle, fat ...... 0.10 Cattle, kidney ...... 1 .00 (b) Section 18 emergency exemptions. Cattle, liver ...... 2 .00 [Reserved] Cattle, meat byproducts ...... 0.05 (c) Tolerances with regional registra- Cattle, meat ...... 0 .05 Cotton, gin byproducts ...... 0 .20 tions. [Reserved] Cotton, undelinted seed ...... 0 .20 (d) Indirect or inadvertent residues. Egg ...... 0 .05 Tolerances are established for indirect Goat, fat ...... 0 .10 Goat, kidney ...... 1 .00 or inadvertent residues of the insecti- Goat, liver ...... 2.00 cide tebufenozide, including its me- Goat, meat byproducts ...... 0 .05

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Parts per [60 FR 42458, Aug. 16, 1995, as amended at 61 Commodity million FR 33044, June 26, 1996; 63 FR 42256, 42257, Aug. 7, 1998; 66 FR 10825, Feb. 20, 2001; 71 FR Goat, meat ...... 0.05 74818, Dec. 13, 2006; 72 FR 35665, June 29, 2007; Hog, fat ...... 0 .10 73 FR 33017, June 11, 2008; 75 FR 17570, Apr. 7, Hog, kidney ...... 1.00 2010; 75 FR 80350, Dec. 22, 2010] Hog, liver ...... 2 .00 Hog, meat byproducts ...... 0 .05 Hog, meat ...... 0 .05 § 180.485 Cyproconazole; tolerances for Horse, fat ...... 0 .10 residues. Horse, kidney ...... 1 .00 (a) General. (1) Tolerances are estab- Horse, liver ...... 2 .00 lished for residues of the free and con- Horse, meat byproducts ...... 0 .05 jugated forms of the fungicide Horse, meat ...... 0 .05 Milk ...... 0.05 cyproconazole, including its metabo- Peanut ...... 0 .5 lites and degradates, in or on the com- Peanut, hay ...... 15.0 modities in the table below. Compli- Peanut, meal ...... 1 .0 ance with the proposed tolerance levels Potato ...... 0 .20 specified below is to be determined by Potato, wet peel ...... 0 .30 Poultry, fat ...... 0.05 measuring only cyproconazole (a-(4- Poultry, meat ...... 0 .05 chlorophenyl)-a-(1-cyclopropylethyl)- Poultry, meat byproducts ...... 0.05 1H-1,2,4-triazole-1-ethanol) in or on the Rice, bran ...... 10.0 following commodities: Rice, grain ...... 7 .0 Rice, hulls ...... 25 .0 Commodity Parts per Rice, straw ...... 10 .0 million Sheep, fat ...... 0 .10 Aspirated grain fractions ...... 2 .5 Sheep, kidney ...... 1.00 Cattle, fat ...... 0.01 Sheep, liver ...... 2.00 Cattle, meat byproducts (except liver) ...... 0 .01 Sheep, meat ...... 0.05 Coffee bean, green (Imported) 1 ...... 0 .1 Sheep, meat byproducts ...... 0 .05 Corn, field, forage ...... 0 .60 Soybean, forage ...... 8 .0 Corn, field, grain ...... 0 .01 Soybean, hay ...... 2 .5 Corn, field, stover ...... 1 .2 Soybean, seed ...... 0 .20 Goat, fat ...... 0 .01 Turnip, greens ...... 0.1 Goat, meat byproducts (except liver) ...... 0.01 Vegetable, brassica, leafy, group 5 ...... 0.1 Horse, fat ...... 0 .01 Horse, meat byproducts (except liver) ...... 0 .01 Peanut ...... 0 .01 (b) Section 18 emergency exemptions. Peanut, hay ...... 6.0 [Reserved] Sheep, fat ...... 0 .01 (c) Tolerances with regional registra- Sheep, meat byproducts (except liver) ...... 0.01 Soybean, forage ...... 1 .0 tions. [Reserved] Soybean, hay ...... 3 .0 (d) Indirect or inadvertent residues. Soybean, oil ...... 0 .10 Tolerances are established for the indi- Soybean, seed ...... 0 .05 Wheat, forage ...... 0 .80 rect or inadvertent residues of Wheat, grain ...... 0 .05 flutolanil, N-(3-(1- Wheat, grain, milled byproducts ...... 0 .10 methylethoxy)phenyl)-2- Wheat, hay ...... 1 .3 Wheat, straw ...... 0 .90 (trifluoromethyl)benzamide, including 1There are no U.S. registrations as of February 15, 2008 for its metabolites and degradates, in or use on coffee bean. on the commodities in the table below. Compliance with the tolerance levels (2) A tolerance is established for the specified below is to be determined by combined residues of the free and con- measuring only flutolanil and its me- jugated forms of the fungicide tabolites converted to 2- cyproconazole, including its metabo- (trifluoromethyl) benzoic acid and cal- lites and degradates, in or on the com- culated as flutolanil, in or on the fol- modity in the table below. Compliance lowing commodities. with the tolerance level specified below is to be determined by measuring only Commodity Parts per the sum of cyproconazole (a-(4- million chlorophenyl)-a-(1-cyclopropylethyl)- Wheat, bran ...... 0.20 1H-1,2,4-triazole-1-ethanol) and its me- Wheat, forage ...... 2 .5 tabolite d-(4-chlorophenyl)-b,d- Wheat, grain ...... 0 .05 dihydroxy-g-methyl-1H-1,2,4-triazole-1- Wheat, hay ...... 1 .2 hexenoic acid, calculated as the stoi- Wheat, straw ...... 0 .20 chiometric equivalent of

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cyproconazole, in or on the following Commodity Parts per commodity: million Corn, pop, stover ...... 0.01 Parts per Commodity million Corn, sweet, forage ...... 0 .01 Corn, sweet, kernel plus cob with husks re- Milk ...... 0.02 moved ...... 0 .01 Corn, sweet, stover ...... 0 .01 (3) Tolerances are established for the combined residues of the free and con- (b) Section 18 emergency exemptions. jugated forms of the fungicide [Reserved] cyproconazole, including its metabo- (c) Tolerances with regional registra- lites and degradates, in or on the com- tions. [Reserved] modities in the table below. Compli- (d) Indirect or inadvertent residues. ance with the tolerance level specified [Reserved] below is to be determined by measuring [76 FR 23498, Apr. 27, 2011] only the sum of cyproconazole (a-(4- chlorophenyl)-a-(1-cyclopropylethyl)- § 180.487 Pyrithiobac sodium; toler- 1H-1,2,4-triazole-1-ethanol) and its me- ances for residues. tabolite 2-(4-chlorophenyl)-3- (a) General. Tolerances are estab- cyclopropyl-1-[1,2,4]triazol-1-yl-butane- lished for residues of the herbicide, 2,3-diol, calculated as the stoichio- pyrithiobac sodium, (sodium 2-chloro- metric equivalent of cyproconazole, in 6-[(4,6-dimethoxypyrimidin-2- or on the following commodities: yl)thio]benzoate), resulting from the application of the pesticide chemical in Parts per Commodity million or on the following foods/feeds:

Cattle, liver ...... 0 .50 Commodity Parts per Goat, liver ...... 0.50 million Hog, liver ...... 0 .01 Horse, liver ...... 0 .50 Cotton, gin byproducts ...... 0 .15 Sheep, liver ...... 0.50 Cotton, undelinted seed ...... 0 .02

(b) Section 18 emergency exemptions. (b) Section 18 emergency exemptions. [Reserved] [Reserved] (c) Tolerances with regional registra- (c) Tolerances with regional registra- tions. [Reserved] tions. [Reserved] (d) Indirect or inadvertent residues. (d) Indirect or inadvertent residues. [Reserved] [Reserved] [63 FR 53835, Oct. 7, 1998, as amended at 71 FR [62 FR 54783, Oct. 22, 1997, as amended at 64 71058, Dec. 8, 2006; 73 FR 27760, May 14, 2008; FR 56469, Oct. 20, 1999; 67 FR 72110, Dec. 4, 78 FR 37473, June 21, 2013] 2002]

§ 180.486 Chlorethoxyfos; tolerances § 180.490 Imazapic; tolerances for resi- for residues. dues. (a) General. Tolerances are estab- (a) General. (1) Tolerances are estab- lished for residues of the insecticide lished for residues of the herbicide chlorethoxyfos, including its metabo- imazapic, including its metabolites and lites and degradates, in or on the com- degradates, in or on the commodities modities in the table in this paragraph. listed in the following table. Compli- Compliance with the tolerance levels ance with the tolerance levels specified specified in this paragraph is to be de- is to be determined by measuring the termined by measuring only sum of imazapic (2-[4,5-dihydro-4-meth- chlorethoxyfos, O,O-diethyl O-(1,2,2,2- yl-4-(1-methylethyl)-5-oxo-1H-imidazol- tetrachloroethyl) phosphorothioate, in 2-yl]-5-methyl-3-pyridinecarboxylic or on the commodity. acid) and its metabolites (±)-2-[4,5- dihydro-4-methyl-4-(1-methylethyl)-5- Parts per Commodity million oxo-1H-imidazol-2-yl]-5- hydroxymethyl-3-pyridinecarboxylic Corn, field, forage ...... 0 .01 acid and (±)-2-[4,5-dihydro-4-methyl-4- Corn, field, grain ...... 0 .01 Corn, field, stover ...... 0 .01 (1-methylethyl)-5-oxo-1H-imidazol-2- Corn, pop, grain ...... 0.01 yl]-5-(b-D-glucopyranosyloxy)methyl-3-

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pyridinecarboxylic acid, calculated as § 180.491 Propylene oxide; tolerances the stoichiometric equivalent of for residues. imazapic. (a) General. (1) Tolerances are estab- lished for residues of the fumigant pro- Parts per Commodity million pylene oxide, including its metabolites and degradates, in or on the commod- Grass, forage ...... 15 ities in the table in this paragraph. Grass, hay ...... 30 Compliance with the tolerance levels Peanut ...... 0 .1 Soybean, seed 1 ...... 0 .40 specified in this paragraph is to be de- Sugarcane, cane 2 ...... 0.03 termined by measuring only propylene oxide, when used as a postharvest fumi- 1 There are no US registrations as of April 4, 2014. 2 There are no U.S. registrations as of June 4, 2014. gant, in or on the commodity.

(2) Tolerances are established for res- Commodity Parts per idues of the herbicide imazapic, includ- million ing its metabolites and degradates, in Cacao bean, cocoa powder ...... 200 or on the commodities listed in the fol- Cacao bean, dried bean ...... 200 Fig ...... 3 .0 lowing table. Compliance with the tol- Garlic, dried ...... 300 erance levels specified is to be deter- Grape, raisin ...... 1 .0 Herbs and spices, group 19, dried ...... 300 mined by measuring the sum of Nut, pine ...... 300 imazapic (2-[4,5-dihydro-4-methyl-4-(1- Nut, tree, group 14 ...... 300 methylethyl)-5-oxo-1H-imidazol-2-yl]-5- Nutmeat, processed, except peanuts ...... 300 Onion, dried ...... 300 methyl-3-pyridinecarboxylic acid) and Pistachio ...... 300 its metabolite (±)-2-[4,5-dihydro-4- Plum, prune, dried ...... 2.0 methyl-4-(1-methylethyl)-5-oxo-1H- imidazol-2-yl]-5-hydroxymethyl-3- (2) Tolerances are established for res- pyridinecarboxylic acid, calculated as idues of the reaction product, pro- the stoichiometric equivalent of pylene chlorohydrin, including its me- imazapic. tabolites and degradates, in or on the commodities in the table in this para- Commodity Parts per graph. Compliance with the tolerance million levels specified in this paragraph is to Cattle, fat ...... 0.10 be determined by measuring only the Cattle, kidney ...... 1 .0 sum of propylene chlorohydrin (1- Cattle, meat byproducts, except kidney ...... 0.1 chloro-2-propanol), and its isomer 2- Cattle, meat ...... 0 .1 chloro-1-propanol, calculated as the Goat, fat ...... 0 .1 stoichiometric equivalent of propylene Goat, kidney ...... 1 .0 Goat, meat byproducts, except kidney ...... 0 .1 chlorohydrin (1-chloro-2-propanol), Goat, meat ...... 0.1 that results from the use of propylene Horse, fat ...... 0 .1 oxide as a postharvest fumigant, in or Horse, kidney ...... 1 .0 on the commodity. Horse, meat byproducts, except kidney ...... 0 .1 Horse, meat ...... 0 .1 OMMODITY Milk ...... 0.1 Sheep, fat ...... 0 .1 Commodity Parts per Sheep, kidney ...... 1.0 million Sheep, meat byproducts, except kidney ...... 0 .1 Basil, dried leaves ...... 6000 Sheep, meat ...... 0.1 Cacao bean, cocoa powder ...... 20 .0 Cacao bean, dried bean ...... 20 .0 (b) Section 18 emergency exemptions. Fig ...... 3 .0 Garlic, dried ...... 6000 [Reserved] Grape, raisin ...... 4 .0 (c) Tolerances with regional registra- Herbs and spices, group 19, dried, except basil 1500 tions. [Reserved] Nut, pine ...... 10 .0 Nut, tree, group 14 ...... 10 .0 (d) Indirect or inadvertent residues. Nutmeat, processed, except peanuts ...... 10 .0 [Reserved] Onion, dried ...... 6000 Pistachio ...... 10.0 [64 FR 54224, Oct. 6, 1999, as amended at 66 FR Plum, prune, dried ...... 2.0 64774, Dec. 14, 2001; 66 FR 66332, Dec. 26, 2001; 78 FR 49932, Aug. 16, 2013; 79 FR 18818, Apr. 4, (b) Section 18 emergency exemptions. 2014; 79 FR 32170, June 4, 2014] [Reserved]

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(c) Tolerances with regional registra- Commodity Parts per tions. [Reserved] million (d) Indirect or inadvertent residues. Onion, green, subgroup 3–07B ...... 15 .0 [Reserved] Papaya 1 ...... 1 .5 Potato ...... 0 .05 [65 FR 33702, May 24, 2000, as amended at 68 Potato, wet peel ...... 0 .20 FR 39430, July 1, 2003; 72 FR 49651, Aug. 29, Taro, corm ...... 0 .5 2007; 73 FR 54963, Sept. 24, 2008; 76 FR 38037, Taro, leaves ...... 6 .0 June 29, 2011; 77 FR 28495, May 15, 2012] Turnip, greens ...... 20.0 Vegetable, cucurbit, group 9 ...... 0.5 Vegetable, fruiting, group 8 ...... 1.5 § 180.492 Triflusulfuron-methyl; toler- Vegetable, leafy (except Brassica) group 4 ...... 30 .0 ances for residues. 1 There are no U.S. registrations as of January 20, 2015. (a) General. Tolerances are estab- lished for residues of triflusulfuron- (b) Section 18 emergency exemptions. methyl, including its metabolites and [Reserved] degradates, in or on the commodities (c) Tolerances with regional registra- listed in the table below. Compliance tions. Tolerances with regional reg- with the tolerance levels specified istrations are established for residues below is to be determined by measuring of the fungicide dimethomorph, (E,Z) 4- only triflusulfuron-methyl (methyl 2- [3-(4-chlorophenyl)-3-(3,4- [[[[[4-(dimethylamino)-6-(2,2,2- dimethoxyphenyl)-1-oxo-2-pro- trifluoroethoxy)-1,3,5-triazin-2- penyl]morpholine, in or on the fol- yl]amino]carbonyl]amino]sulfonyl]-3- lowing commodities: methylbenzoate) in or on the following Parts per commodities: Commodity million

Parts per Bean, lima, succulent ...... 0 .60 Commodity million

Beet, garden, roots ...... 0 .01 (d) Indirect or inadvertent residues. Beet, garden, tops ...... 0 .02 Tolerances are established for the indi- Beet, sugar, roots ...... 0 .05 rect or inadvertent residues of the fun- Beet, sugar, tops ...... 0.05 gicide dimethomorph, in or on the Chicory, roots ...... 0 .05 commodities in the following table. (b) Section 18 emergency exemptions. Compliance with the following toler- [Reserved] ance levels specified in the following (c) Tolerances with regional registra- table is to be determined by measuring tions. [Reserved] only dimethomorph (E,Z)-4-[3-(4- (d) Indirect or inadvertent residues. chlorophenyl)-3-(3,4- [Reserved] dimethoxyphenyl)acryloyl]morpholine calculated in or on the following com- [67 FR 40196, June 12, 2002, as amended at 76 modities: FR 22625, Apr. 22, 2011] Parts per § 180.493 Dimethomorph; tolerances Commodity million for residues. Wheat, forage ...... 0 .15 (a) General. Tolerances are estab- Wheat, hay ...... 0 .15 lished for the residues of the fungicide Wheat, straw ...... 0 .4 dimethomorph, (E,Z) 4-[3-(4- chlorophenyl)-3-(3,4-dimethoxyphenyl)- [62 FR 26416, May 14, 1997] 1-oxo-2-propenyl]morpholine, in or on EDITORIAL NOTE: For FEDERAL REGISTER ci- the following commodities: tations affecting § 180.493, see the List of CFR Sections Affected, which appears in the Parts per Commodity million Finding Aids section of the printed volume and at www.fdsys.gov. Brassica, head and stem, subgroup 5A ...... 6 .0 Brassica, leafy greens, subgroup 5B ...... 30 .0 § 180.494 Pyridaben; tolerance for resi- Ginseng ...... 0 .90 dues. Grape ...... 3 .0 Grape, raisin ...... 7 .0 (a) General. Tolerances are estab- Hop, dried cones ...... 60 lished for residues of the insecticide Lettuce, head ...... 10 Lettuce, leaf ...... 10 pyridaben [2-tert-butyl-5-(4-tert- Onion, bulb, subgroup 3–07A ...... 0 .6 butylbenzylthio)-4-chloropyridazin-

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3(2H)-one] on the following plants, and (d) Indirect or inadvertent residues. of the insecticide pyridaben and its me- [Reserved] tabolites (2-tert-butyl-5-(4-(1-carboxy-1- [65 FR 43712, July 14, 2000, as amended at 66 methylethyl)benzylthio)-4- FR 33199, June 21, 2001; 70 FR 55769, Sept. 23, chloropyridazin-3(2H)-one] and (2-tert- 2005; 76 FR 56015, Sept. 15, 2010] butyl-5-[4(-1,1-dimethyl-2- hypdroxyethyl)benzylthio-4- § 180.495 Spinosad; tolerances for resi- chloropyridazinn-3(2H)-one) on ani- dues. mals, as indicated in the following (a) General. Tolerances are estab- table. lished for residues of the insecticide spinosad in or on the food commodities Revoca- Parts per in the table to this paragraph. Commodity million tion/expira- tion date Spinosad is a fermentation product of Almond, hulls ...... 4.0 None Saccharopolyspora spinosa. The product Apple ...... 0.5 None consists of two related active ingredi- Apple, wet pomace ...... 0.75 None ents: Spinosyn A (Factor A: CAS # Canistel ...... 0.10 None 131929–60–7) or 2-[(6-deoxy-2,3,4-tri-O Cattle, fat ...... 0.05 None -methyl- -L-manno-pyranosyl)oxy]-13- Cattle, meat ...... 0.05 None a Cattle, meat byproducts ...... 0.05 None [[5-(dimethylamino)-tetrahydro-6- Citrus ...... 0.5 None methyl-2H-pyran-2-yl]oxy]-9-ethyl- Citrus, dried pulp ...... 1.5 None 2,3,3a,5a,5b,6,9,10,11,12,13,14,16a,16b- Citrus, oil ...... 10.0 None tetradecahydro-14-methyl-1H-as- Fruit, stone, group 12 ...... 2.5 None Goat, fat ...... 0.0 None Indaceno[3,2-d]oxacyclododecin-7,15- Goat, meat ...... 0.05 None dione; and Spinosyn D (Factor D; CAS Goat, meat byproducts ...... 0.05 None # 131929–63–0) or 2-[(6-deoxy-2,3,4-tri-O- Grape ...... 1.5 None methyl-a-L-manno-pyranosyl)oxy]-13- Hog, fat ...... 0.05 None Hog, meat ...... 0.05 None [[5-(dimethyl-amino)-tetrahydro-6- Hog, meat byproducts ...... 0.05 None methyl-2H-pyran-2-yl]oxy]-9-ethyl- Hop, dried cones ...... 10.0 None 2,3,3a,5a,5b,6,9,10,11,12,13,14,16a,16b- Horse, fat ...... 0.05 None tetradecahydro-4,14-methyl-1H-as- Horse, meat ...... 0.05 None Indaceno[3,2-d]oxacyclododecin-7,15- Horse, meat byproducts ...... 0.05 None Mango ...... 0.10 None dione. Milk ...... 0.01 None Nut, tree, group 14 ...... 0.05 None Parts per mil- Commodity lion Papaya ...... 0.10 None Pear ...... 0.75 None Acerola ...... 1.5 Pistachio ...... 0.05 None Alfalfa, seed ...... 0 .15 Sapodilla ...... 0.10 None Alfalfa, seed screenings ...... 2 .0 Sapote, black ...... 0.10 None Almond, hulls ...... 19 Sapote, mamey ...... 0.10 None Amaranth, grain, grain ...... 1 .0 Sheep, fat ...... 0.05 None Amaranth, grain, stover ...... 10 Sheep, meat ...... 0.05 None Animal feed, nongrass, group, 18 ...... 0.02 Sheep, meat byproduct ...... 0.05 None Animal feed, nongrass, group, 18, forage ...... 35.0 Star apple ...... 0.10 None Animal feed, nongrass, group, 18, hay ...... 30 .0 Strawberry ...... 2.5 None Apple, dry pomace ...... 0.5 Tomato ...... 0.15 None Apple, wet pomace ...... 0 .5 Artichoke, globe ...... 0.3 Asparagus ...... 0.2 (b) Section 18 emergency exemptions. Atemoya ...... 0 .3 [Reserved] Avocado ...... 0 .3 (c) Tolerances with regional registra- Banana ...... 0.25 Beet, sugar, molasses ...... 0 .75 tions. Tolerances with regional reg- Biriba ...... 0 .3 istration, as defined in § 180.1(m) are es- Brassica, head and stem, subgroup 5A ...... 2 .0 tablished for residues of the insecticide Brassica, leafy greens, subgroup 5B ...... 10 .0 Bushberry subgroup 13B ...... 0 .250 pyridaben [2-tert-butyl-5(4-tert- Caneberry subgroup 13A ...... 0 .7 butylbenzylthio)-4-chloropyridazin- Canistel ...... 0 .3 3(2H)-one] in or on the following raw Cattle, fat ...... 50 agricultural commodity: Cattle, liver ...... 10 Cattle, meat ...... 2 .0 Cattle, meat byproducts, except liver ...... 5 .0 Parts per Expiration Commodity million Date Cherimoya ...... 0 .3 Citrus, oil ...... 3.0 Cranberry ...... 0.5 None Citrus, dried pulp ...... 0 .5 Coriander, leaves ...... 8 .0

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Parts per mil- Parts per mil- Commodity lion Commodity lion

Corn, sweet, kernel plus cob with husks re- Rice, hulls ...... 4 .0 moved ...... 0 .02 Salal ...... 0 .250 Cotton, gin byproducts ...... 1 .5 Sapodilla ...... 0 .3 Cotton, undelinted seed ...... 0 .02 Sapote, black ...... 0 .3 Cranberry ...... 0 .01 Sapote, mamey ...... 0 .3 Custard apple ...... 0 .3 Sapote, white ...... 0 .3 Date ...... 0 .10 Sheep, fat ...... 50 Egg ...... 0 .30 Sheep, liver ...... 10 Feijoa ...... 05 Sheep, meat ...... 2.0 Fig ...... 0 .10 Sheep, meat byproducts, except liver ...... 5 .0 Fish ...... 4 .0 Soursop ...... 0 .3 Fish-shellfish, crustacean ...... 4 .0 Soybean ...... 0.02 Fish-shellfish, mollusc ...... 4 .0 Spanish lime ...... 0 .3 Food commodities ...... 0 .02 Spearmint, tops ...... 3 .5 Fruit, citrus, group 10 ...... 0 .3 Spice, subgroup 19B, except black pepper .... 1 .7 Fruit, pome, group 11 ...... 0.20 Fruit, stone, group 12 ...... 0 .20 Star apple ...... 0 .3 Goat, fat ...... 50 Starfruit ...... 0 .3 Goat, liver ...... 10 Strawberry ...... 1 .0 Goat, meat ...... 2.0 Sugar apple ...... 0 .3 Goat, meat byproducts, except liver ...... 5 .0 Ti, leaves ...... 10 .0 Grain, aspirated fractions ...... 200 Vegetable, bulb, group 3, except green onion 0.10 Grain, cereal, group 15 ...... 1.5 Vegetable, cucurbit, group 9 ...... 0.3 Grain, cereal, group 16, forage, except rice ... 2 .5 Vegetable, foliage of legume, group 7 ...... 8 .0 Grain, cereal, group 16, hay, except rice ...... 10 .0 Vegetable, fruiting, group 8 ...... 0.4 Grain, cereal, group, 16, stover, except rice ... 10 .0 Vegetable, leafy, except brassica, group 4 ..... 8 .0 Grain, cereal, group, 16, straw, except rice .... 1 .0 Vegetable, leaves of root and tuber, group 2 10 .0 Grape ...... 0 .50 Vegetable, legume, edible podded, subgroup Grape, raisin ...... 0 .70 6A ...... 0 .30 Grass, forage, fodder and hay, group 17, for- Vegetable, root and tuber, group 1 ...... 0 .10 age ...... 10 .0 Watercress ...... 8 .0 Grass, forage, fodder and hay, group 17, hay 5 .0 Wax jambu ...... 0 .3 Guava ...... 0 .3 Herb subgroup 19A, dried ...... 22 (b) Section 18 emergency exemptions. Herb subgroup 19A, fresh ...... 3.0 Hog, fat ...... 5 .0 [Reserved] Hog, meat ...... 0 .50 (c) Tolerances with regional registra- Hog, meat byproducts ...... 2 .0 tions. [Reserved] Hop, dried cones ...... 22 (d) Indirect or inadvertant residues. Horse, fat ...... 50 Horse, liver ...... 10 [Reserved] Horse, meat ...... 2 .0 Horse, meat byproducts, except liver ...... 5 .0 [72 FR 68540, Dec. 5, 2007, as amended at 74 Ilama ...... 0 .3 FR 46376, Sept. 9, 2009; 74 FR 48408, Sept. 23, Jaboticaba ...... 0 .3 2009; 75 FR 60327, Sept. 30, 2010] Juneberry ...... 0 .25 Lingonberry ...... 0.250 § 180.496 Thiazopyr; tolerances for res- Longan ...... 0 .3 idues. Lychee ...... 0 .3 Mango ...... 0.3 Tolerances are established for com- Milk ...... 7.0 bined residues of the herbicide Milk, fat ...... 85 Nut, tree, group 14 ...... 0 .10 thiazopyr (3-pyridinecaroxylic acid, 2- Okra ...... 0.40 (difluoromethyl)-5-(4,5-dihydro-2- Onion, green ...... 2 .0 thiazolyl)-4-(2-methylpropyl)-6- Papaya ...... 0 .3 (trifluoromethyl)-, methyl ester) and Passionfruit ...... 0 .3 Pea and bean, dried shelled, except soybean, its metabolites determined as 2- subgroup 6C ...... 0 .02 (difluoromethyl)-6-(trifluoromethyl)- Pea and bean, succulent shelled, subgroup 3,4,5-pyridinetricarboxylic acid, all ex- 6B ...... 0 .02 Peanut ...... 0 .02 pressed as the parent equivalents in or Peanut, hay ...... 11.0 on the following raw agricultural com- Peppermint, tops ...... 3 .5 modities: Pineapple ...... 0.02 Pineapple, process residue ...... 0 .08 Commodities Parts per Pistachio ...... 0.10 million Pomegranate ...... 0 .30 Poultry, fat ...... 1.3 Grapefruit ...... 0 .05 Poultry, meat ...... 0 .10 Orange, sweet ...... 0 .05 Poultry, meat byproducts ...... 0.20 Pulasan ...... 0 .3 Rambutan ...... 0 .3 [62 FR 9978, Mar. 5, 1997]

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§ 180.497 Clofencet; tolerances for resi- termined by measuring only clofencet, dues. potassium 2-(4-chlorophenyl)-3-ethyl- (a) General. Tolerances are estab- 2,5-dihydro-5-oxo-4- lished for residues of the plant growth pyridazinecarboxylate, expressed as the regulator (hybridizing agent) clofencet, free acid, in or on the commodity when including its metabolites and present therein as a result of the appli- degradates, in or on the commodities cation of clofencet to the growing in the table in this paragraph. Compli- crops in paragraph (a) of this section. ance with the tolerance levels specified Expiration/ in this paragraph is to be determined Commodity Parts per revocation by measuring only clofencet, potas- million date sium 2-(4-chlorophenyl)-3-ethyl-2,5- Grain, cereal, forage, fodder and dihydro-5-oxo-4-pyridazinecarboxylate, straw, group 16, except rice, expressed as the free acid, in or on the sweet corn, wheat, and wild rice; commodity. forage ...... 4.0 7/14/12 Grain, cereal, forage, fodder and straw, group 16, except rice, Parts per Expiration/ Commodity million revocation sweet corn, wheat, and wild rice; date hay ...... 15.0 7/14/12 Grain, cereal, forage, fodder and Cattle, fat ...... 0.04 7/14/12 straw, group 16, except rice, Cattle, kidney ...... 10.0 7/14/12 sweet corn, wheat, and wild rice; Cattle, meat ...... 0.15 7/14/12 stover ...... 1.0 7/14/12 Cattle, meat byproducts, except kid- ney ...... 0.5 7/14/12 Grain, cereal, forage, fodder and Egg ...... 1.0 7/14/12 straw, group 16, except rice, Goat, fat ...... 0.04 7/14/12 sweet corn, wheat, and wild rice; Goat, kidney ...... 10.0 7/14/12 straw ...... 4.0 7/14/12 Goat, meat ...... 0.15 7/14/12 Grain, cereal group 15, except rice, Goat, meat byproducts, except kid- sweet corn, wheat, and wild rice 20.0 7/14/12 ney ...... 0.5 7/14/12 Soybean ...... 30.0 7/14/12 Hog, fat ...... 0.04 7/14/12 Soybean, forage ...... 10.0 7/14/12 Hog, kidney ...... 10.0 7/14/12 Soybean, hay ...... 10.0 7/14/12 Hog, meat ...... 0.15 7/14/12 Hog, meat byproducts, except kid- ney ...... 0.5 7/14/12 [76 FR 56656, Sept. 14, 2011] Horse, fat ...... 0.04 7/14/12 Horse, kidney ...... 10.0 7/14/12 Horse, meat ...... 0.15 7/14/12 § 180.498 Sulfentrazone; tolerances for Horse, meat byproducts, except kid- residues. ney ...... 0.5 7/14/12 Milk ...... 0.02 7/14/12 (a)(1) General. Tolerances are estab- Poultry, fat ...... 0.04 7/14/12 lished for the combined residues of the Poultry, meat ...... 0.15 7/14/12 free and conjugated forms of Poultry, meat byproducts ...... 0.20 7/14/12 Sheep, fat ...... 0.04 7/14/12 sulfentrazone, including its metabo- Sheep, kidney ...... 10.0 7/14/12 lites and degradates, in or on the com- Sheep, meat ...... 0.15 7/14/12 modities in the table below. Compli- Sheep, meat byproducts, except kidney ...... 0.5 7/14/12 ance with the tolerance levels specified Wheat, forage ...... 10.0 7/14/12 below is to be determined by measuring Wheat, grain ...... 250.0 7/14/12 Wheat, hay ...... 40.0 7/14/12 only the sum of sulfentrazone (N-[2,4- Wheat, straw ...... 50.0 7/14/12 dichloro-5-[4-(difluoromethyl)-4,5- dihydro-3-methyl-5-oxo-1H-1,2,4-triazol- (b) Section 18 emergency exemptions. 1-yl]phenyl]methanesulfonamide) and [Reserved] its metabolite HMS (N-(2,4-dichloro-5- (c) Tolerances with regional registra- (4-(difluoromethyl)-4,5-dihydro-3- tions. [Reserved] hydroxymethyl-5-oxo-1H-1,2,4-triazol-1- (d) Indirect or inadvertent residues. yl)phenyl)methanesulfonamide, cal- Tolerances are established for indirect culated as the stoichiometric equiva- or inadvertent residues of the plant lent of sulfentrazone in or on the fol- growth regulator (hybridizing agent) lowing commodities. clofencet, including its metabolites and degradates, in or on the commod- Commodity Parts per ities in the table in this paragraph. million Compliance with the tolerance levels Soybean, seed ...... 0 .05 specified in this paragraph is to be de-

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(2) Tolerances are established for the below. Compliance with the tolerance combined residues of the free and con- levels specified below is to be deter- jugated forms of sulfentrazone, includ- mined by measuring only the sum of ing its metabolites and degradates, in sulfentrazone (N-[2,4-dichloro-5-[4- or on the commodities in the table (difluoromethyl)-4,5-dihydro-3-methyl- below. Compliance with the tolerance 5-oxo-1H-1,2,4-triazol-1- levels specified below is to be deter- yl]phenyl]methanesulfonamide) and its mined by measuring only the sum of metabolites HMS (N-(2,4-dichloro-5-(4- sulfentrazone (N-[2,4-dichloro-5-[4- (difluoromethyl)-4,5-dihydro-3- (difluoromethyl)-4,5-dihydro-3-methyl- hydroxymethyl-5-oxo-1H-1,2,4-triazol-1- 5-oxo-1H-1,2,4-triazol-1- yl)phenyl)methanesulfonamide) and yl]phenyl]methanesulfonamide) and its DMS (N-(2,4-dichloro-5-(4- metabolites HMS (N-(2,4-dichloro-5-(4- (difluoromethyl)-4,5-dihydro-5-oxo-1H- (difluoromethyl)-4,5-dihydro-3- 1,2,4-triazol-1- hydroxymethyl-5-oxo-1H-1,2,4-triazol-1- yl)phenyl)methanesulfonamide, cal- yl)phenyl)methanesulfonamide) and culated as the stoichiometric equiva- DMS (N-(2,4-dichloro-5-(4- lent of sulfentrazone in or on the fol- (difluoromethyl)-4,5-dihydro-5-oxo-1H- lowing commodities. 1,2,4-triazol-1- Parts per yl)phenyl)methanesulfonamide, cal- Commodity million culated as the stoichiometric equiva- Bean, lima, succulent ...... 0 .15 lent of sulfentrazone in or on the fol- Cowpea, succulent ...... 0 .15 lowing commodities. Wheat, forage ...... 0 .50 Wheat, grain ...... 0 .15 Wheat, hay ...... 0 .30 Commodity Parts per million Wheat, straw ...... 1 .5

Apple ...... 0.15 Asparagus ...... 0.15 (d) Indirect or inadvertent residues. Berry and small fruit, group 13–07 ...... 0 .15 Tolerances are established for inad- Brassica, head and stem, subgroup 5A ...... 0 .20 vertent and indirect combined residues Brassica, leafy greens, subgroup 5B ...... 0 .40 Corn, field, forage ...... 0 .20 of the free and conjugated forms of Corn, field, grain ...... 0 .15 sulfentrazone, including its metabo- Corn, field, stover ...... 0 .30 lites and degradates, in or on the com- Flax ...... 0 .15 modities in the table below. Compli- Fruit, citrus, group 10–10 ...... 0 .15 Horseradish ...... 0.20 ance with the tolerance levels specified Melon, subgroup 9A ...... 0 .15 below is to be determined by measuring Nut, tree, group 14 ...... 0 .15 only the sum of sulfentrazone (N-[2,4- Pea and bean, dried shelled, except soybean, subgroup 6C ...... 0 .15 dichloro-5-[4-(difluoromethyl)-4,5- Pea, succulent ...... 0 .15 dihydro-3-methyl-5-oxo-1H-1,2,4-triazol- Peanut ...... 0 .20 1-yl]phenyl]methanesulfonamide) and Peanut, meal ...... 0 .40 Peppermint, tops ...... 0 .30 its metabolites HMS (N-(2,4-dichloro-5- Pistachio ...... 0.15 (4-(difluoromethyl)-4,5-dihydro-3- Rhubarb ...... 0 .15 hydroxymethyl-5-oxo-1H-1,2,4-triazol-1- Spearmint, tops ...... 0 .30 yl)phenyl)methanesulfonamide) and Sugarcane, cane ...... 0.15 Sugarcane, molasses ...... 0 .20 DMS (N-(2,4-dichloro-5-(4- Sunflower subgroup 20B ...... 0.20 (difluoromethyl)-4,5-dihydro-5-oxo-1H- Turnip, roots ...... 0 .15 1,2,4-triazol-1- Turnip, tops ...... 0.60 Vegetable, fruiting, group 8–10 ...... 0 .15 yl)phenyl)methanesulfonamide, cal- Vegetable, soybean, succulent ...... 0 .15 culated as the stoichiometric equiva- Vegetable, tuberous and corm, subgroup 1C ... 0.15 lent of sulfentrazone in or on the fol- lowing commodities when present (b) Section 18 emergency exemptions. therein as a result of the application of [Reserved] sulfentrazone to growing crops. (c) Tolerances with regional registra- tions. Tolerances with regional reg- Commodity Parts per istration are established for the com- million bined residues of the free and con- Grain, cereal (excluding sweet corn), Hulls ...... 0 .30 jugated forms of sulfentrazone, includ- Grain, cereal, forage, fodder and straw, group 16, except sweet corn; forage ...... 0.2 ing its metabolites and degradates, in Grain, cereal, forage, fodder and straw, group or on the commodities in the table 16, except sweet corn; hay ...... 0.2

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(d) Indirect or inadvertent residues. Commodity Parts per million [Reserved] Grain, cereal, forage, fodder and straw, group [62 FR 15620, Apr. 2, 1997, as amended at 62 16, except sweet corn; stover ...... 0 .1 FR 26966, May 16, 1997; 63 FR 32136, June 12, Grain, cereal, forage, fodder and straw, group 1998; 64 FR 16843, Apr. 7, 1999; 65 FR 58399, 16, except sweet corn; straw ...... 0 .6 Sept. 29, 2000; 66 FR 37598, July 19, 2001; 66 FR Grain, cereal, group 15, except sweet corn ...... 0 .1 48585, Sept. 21, 2001; 67 FR 35049, May 17, 2002; Grain, cereal, group 15, except sweet corn; bran ...... 0 .15 69 FR 47022, Aug. 4, 2004; 70 FR 7047, Feb. 10, 2005; 78 FR 33736, June 5, 2013]

[62 FR 10708, Mar. 10, 1997] § 180.500 Imazapyr; tolerances for resi- dues. EDITORIAL NOTE: For FEDERAL REGISTER ci- tations affecting § 180.498, see the List of CFR (a) General. Tolerances are estab- Sections Affected, which appears in the lished for residues of the herbicide, Finding Aids section of the printed volume imazapyr, including its metabolites and at www.fdsys.gov. and degradates, in or on the commod- ities in the following table. Compliance § 180.499 Propamocarb; tolerances for with the tolerance levels specified in residues. the following table is to be determined (a) General. Tolerances are estab- by measuring only the residues of lished for the residues of propamocarb, imazapyr [2-[4,5-dihydro-4-methyl-4-(1- including its metabolites and methylethyl)-5-oxo-1H-imidazol-2-yl]-3- degradates, in or on the commodities pyridinecarboxylic acid]. specified in the following table result- Parts per ing from the application of the hydro- Commodity million chloride salt of propamocarb. Compli- ance with the following tolerance lev- Cattle, fat ...... 0.05 Cattle, kidney ...... 0 .20 els is to be determined by measuring Cattle, meat ...... 0 .05 only propamocarb (propyl N-[3- Cattle, meat byproducts, except kidney ...... 0.05 (dimethylamino)propyl]carbamate): Corn, field, forage ...... 0 .05 Corn, field, grain ...... 0 .05 Corn, field, stover ...... 0 .05 Commodity Parts per Fish ...... 1 .0 million Goat, fat ...... 0 .05 Goat, kidney ...... 0 .20 Lettuce, head ...... 50 Goat, meat ...... 0.05 Lettuce, leaf ...... 90 Goats, meat byproducts, except kidney ...... 0 .05 Potato ...... 0 .06 Grass, forage ...... 100 Tomato, paste ...... 5 .0 Grass, hay ...... 30 Vegetable, cucurbit, group 9 ...... 1.5 Horse, fat ...... 0 .05 Vegetable, fruiting, group 8 ...... 2.0 Horse, kidney ...... 0 .20 Horse, meat ...... 0 .05 Horse, meat byproducts, except kidney ...... 0 .05 (b) Section 18 emergency exemptions. Lentil 1 ...... 0.2 [Reserved] Milk ...... 0.01 (c) Tolerance with regional registra- Rapeseed subgroup 20A 1 ...... 0 .05 Sheep, fat ...... 0 .05 tions. Tolerances with regional reg- Sheep, kidney ...... 0.20 istrations are established for the resi- Sheep, meat ...... 0.05 dues of propamocarb, including its me- Sheep, meat byproducts, except kidney ...... 0 .05 Shellfish ...... 0 .10 tabolites and degradates, in or on the Soybean, meal 1 ...... 4.5 commodities specified in the following Soybean, seed 1 ...... 4 .0 table resulting from the application of Sunflower subgroup 20B 1 ...... 0.05 the hydrochloride salt of propamocarb. 1 There are no U.S. Registrations. Compliance with the following toler- (b) Section 18 emergency exemptions. ance levels is to be determined by [Reserved] measuring only propamocarb (propyl (c) Tolerances with regional registra- N-[3- tions. [Reserved] (dimethylamino)propyl]carbamate): (d) Indirect or inadvertent residues. [Reserved] Commodity Parts per million [68 FR 55484, Sept. 26, 2003, as amended at 78 FR 66653, Nov. 6, 2013; 79 FR 19487, Apr. 9, Bean, lima, succulent ...... 2 .0 2014]

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§ 180.501 Hydroprene; tolerances for Commodity Parts per residues. million (a) General. A tolerance of 0.2 part per Fruit, stone, group 12, except cherry ...... 0 .170 million is established for residues of Pear ...... 0 .08 hydroprene [(S)-(Ethyl (2E,4E,7S)- 3,7,11-trimrthyl-2,4-dodecadienoate)], (b) Section 18 emergency exemptions. (CAS Reg. No. 65733–18–8) on food com- [Reserved] modities in food-handling establish- (c) Tolerances with regional registra- ments in accordance with the following tions. [Reserved] prescribed conditions: (d) Indirect or inadvertent residues. (1) Application shall be limited to [Reserved] spot, crack and crevice, perimeter and ultra low volume (ULV) fogging treat- [62 FR 24838, May 7, 1997, as amended at 64 ment in food storage or food-handling FR 31129, June 10, 1999; 66 FR 36481, 36484, July 12, 2001; 69 FR 7606, Feb. 18, 2004] establishments, including warehouses, food service, manufacturing, and proc- § 180.503 Cymoxanil, tolerance for resi- essing establishments such as res- dues. taurants, cafeterias, supermarkets, bakeries, breweries, dairies, meat (a) General. Tolerances are estab- slaughtering and packing plants, and lished for residues of the fungicide, canneries where food and food products cymoxanil, 2-cyano -N- are held, processed, and served: Pro- [(ethylamino)carbonyl]-2- vided that the food is removed or cov- (methoxyimino) acetamide, in or on ered prior to such use, and food-proc- the following food commodities: essing surfaces are covered during Parts per treatment or thoroughly cleaned before Commodity million using, or in the case of point-source de- vice treatments, devices must not Caneberry, subgroup 13A-07 ...... 4 .0 come into direct contact with food Cilantro, leaves ...... 19 preparation surfaces and must be in a Hop, dried cones ...... 7 .0 Leafy greens, subgroup 4A ...... 19 minimum distance of 3 feet from ex- Leaf petioles, subgroup 4B ...... 6 .0 posed foods. Lychee 1 ...... 1 .0 (2) To assure safe use of the insect Onion, bulb, subgroup 3-07A ...... 0 .05 growth regulator, the label and label- Onion, green, subgroup 3-07B ...... 1 .1 ing shall conform to that registered by Potato ...... 0 .05 the U.S. Environmental Protection Vegetable, cucurbit, group 9 ...... 0.05 Agency, and it shall be used in accord- Vegetable, fruiting, group 8 ...... 0.2 ance with such label and labeling. 1 There is no U.S. registration for lychee. (b) Section 18 emergency exemptions. (b) Section 18 emergency exemptions. [Reserved] [Reserved] (c) Tolerances with regional registra- tions. [Reserved] (c) Tolerances with a regional registra- (d) Indirect or inadvertent residues. tion. Tolerances with a regional reg- [Reserved] istration as defined in § 180.1(l) are es- tablished for the residues of the fun- [62 FR 61647, Nov. 19, 1997, as amended at 71 gicide cymoxanil, 2-cyano -N- FR 74818, Dec. 13, 2006] [(ethylamino)carbonyl]-2- § 180.502 Aminoethoxyvinylglycine hy- (methoxyimino) acetamide) in or on drochloride (aviglycine HCl); toler- the raw agricultural commodities: ances for residues. Parts per (a) General. Tolerances are estab- Commodity million lished for residues of aminoethoxyvinylglycine hydro- Grape ...... 0 .10 chloride (aviglycine HCl) in or on the following food commodities:

Parts per Commodity million

Apple ...... 0.08

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(d) Indirect or inadvertent residues. emamectin (MAB1a + MAB1b isomers) [Reserved] and the associated 8,9-Z isomers (8,9- ZB and 8,9-ZB ). [62 FR 26411, May 14, 1997, as amended at 62 1a 1b FR 39956, July 25, 1997; 63 FR 24949, May 6, Parts per 1998; 63 FR 66464, Dec. 2, 1998; 64 FR 6539, Feb. Commodity million 10, 1999; 64 FR 47689, Sept. 1, 1999; 66 FR 37598, July 19, 2001; 67 FR 35049, May 17, 2002; 68 FR Cattle, fat ...... 0.010 41936, July 16, 2003; 70 FR 7047, Feb. 10, 2005; Cattle, liver ...... 0 .050 Cattle, meat ...... 0 .003 72 FR 37646, July 11, 2007; 73 FR 58885, Oct. 8, Cattle, meat byproducts, except liver ...... 0 .020 2008; 76 FR 34885, June 15, 2011] Goat, fat ...... 0 .010 Goat, liver ...... 0.050 § 180.504 [Reserved] Goat, meat ...... 0.003 Goat, meat byproducts, except liver ...... 0 .020 § 180.505 Emamectin; tolerances for Hog, fat ...... 0 .003 residues. Hog, liver ...... 0 .020 Hog, meat ...... 0 .002 (a) General. (1) Tolerances are estab- Hog, meat byproducts (except liver) ...... 0 .005 lished for emamectin, including its me- Horse, fat ...... 0 .010 Horse, liver ...... 0 .050 tabolites and degradates, in or on the Horse, meat ...... 0 .003 commodities in the table below. Com- Horse, meat byproducts, except liver ...... 0 .020 pliance with the tolerance levels speci- Milk ...... 0.003 fied below is to be determined by meas- Sheep, fat ...... 0 .010 Sheep, liver ...... 0.050 uring only the sum of emamectin (a Sheep, meat ...... 0.003 mixture of a minimum of 90% 4′-epi- Sheep, meat byproducts, except liver ...... 0 .020 methylamino-4′-deoxyavermectin B1a and maximum of 10% 4′-epi- (b) Section 18 emergency exemptions. methylamino-4′-deoxyavermectin B1b) [Reserved] and its metabolites 8,9-isomer of the (c) Tolerances with regional registra- B1a and B1b component of the parent tions. [Reserved] (8,9-ZMA), or 4′-deoxy-4′-epi-amino- (d) Indirect and inadvertant residues. avermectin B1a and 4’-deoxy-4’-epi- [Reserved] ′ ′ amino-avermectin B1b; 4 -deoxy-4 -epi- [71 FR 18649, Apr. 12, 2006, as amended at 74 ′ amino avermectin B1a (AB1a); 4 -deoxy- FR 2873, Jan. 16, 2009; 78 FR 18511, Mar. 27, 4′-epi-(N-formyl-N-methyl)amino- 2013; 78 FR 49939, Aug. 16, 2013] avermectin (MFB1a); and 4′-deoxy-4′- epi-(N-formyl)amino-avermectin B1a § 180.506 Cyclanilide; tolerances for (FAB1a), calculated as the stoichio- residues. metric equivalent of emamectin. (a) General. Tolerances are estab- lished for residues of the plant growth Parts per Commodity million regulator, cyclanilide, [1-(2,4- dichlorophenylaminocarbonyl)- Almond, hulls ...... 0 .20 Apple, wet pomace ...... 0 .075 cyclopropane carboxylic acid] deter- Cotton, gin byproducts ...... 0 .050 mined as 2,4-dichloroaniline (cal- Cotton, undelinted seed ...... 0 .025 culated as cyclanilide) in or on the fol- Fruit, pome, group 11 ...... 0.025 Grape, wine 1 ...... 0 .03 lowing food commodities and processed Nut, tree, group 14 ...... 0 .02 feed: Pistachio ...... 0.02 Tomato, paste ...... 0 .150 Commodity Parts Per Turnip, greens ...... 0.050 Million Vegetable, Brassica, leafy, group 5 ...... 0 .050 Vegetable, cucurbit, group 9 ...... 0.02 Cattle, fat ...... 0.10 Vegetable, fruiting, group 8 ...... 0.020 Cattle, meat ...... 0 .02 Vegetable, leafy, except Brassica, group 4 ...... 0 .100 Cattle, meat byproducts, except kidney ...... 0.2 Cattle, kidney ...... 2 .0 1 There are no U.S. registrations for use of emamectin on Cotton, undelinted seed ...... 0 .60 grape, wine. Cotton, gin byproducts ...... 25 .0 (2) Tolerances are established for Goat, fat ...... 0 .10 Goat, meat ...... 0.02 emamectin, including its metabolites Goat, meat byproducts, except kidney ...... 0 .20 and degradates, in or on the commod- Goat, kidney ...... 2 .0 ities in the following table. Compliance Horse, fat ...... 0 .10 with the tolerance levels specified in Horse, meat ...... 0 .02 Horse, meat byproducts, except kidney ...... 0 .20 the following table is to be determined Horse, kidney ...... 2 .0 by measuring only the sum of Hog, fat ...... 0 .10

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Parts Per Parts per Commodity Million Commodity million

Hog, meat ...... 0 .02 Coffee, green bean 1 ...... 0 .03 Hog, meat byproducts, except kidney ...... 0 .20 Corn, field, forage ...... 12 .0 Hog, kidney ...... 2.0 Corn, field, grain ...... 0 .05 Milk ...... 0.04 Corn, field, refined oil ...... 0 .3 Sheep, fat ...... 0 .10 Corn, field, stover ...... 25 .0 Sheep, meat ...... 0.20 Corn, pop, grain ...... 0.05 Sheep, meat byproducts, except kidney ...... 0 .20 Corn, pop, stover ...... 25.0 Sheep, kidney ...... 2.0 Corn, sweet, forage ...... 12 .0 Corn, sweet, kernel plus cob with husks re- (b) Section 18 emergency exemptions. moved ...... 0 .05 Corn, sweet, stover ...... 25.0 [Reserved] Cotton, gin byproducts ...... 45 (c) Tolerances with regional registra- Cottonseed subgroup 20C ...... 0 .7 tions. [Reserved] Cranberry ...... 0 .50 Custard apple ...... 2 .0 (d) Indirect or inadvertent residues. Dragon fruit ...... 2 .0 [Reserved] Feijoa ...... 2 .0 Fruit, citrus, group 10–10 ...... 15 .0 [62 FR 28355, May 23, 1997; 62 FR 34182, June Fruit, small vine climbing, except fuzzy 25, 1997] kiwifruit, subgroup 13–07F ...... 2.0 Fruit, stone, group 12 ...... 1 .5 § 180.507 Azoxystrobin; tolerances for Ginseng 1 ...... 0 .5 residues. Grain, aspirated fractions ...... 420 Grass, forage ...... 15 (a) General. (1) Tolerances are estab- Grass, hay ...... 20 lished for residues of the fungicide, Guava ...... 2 .0 Herb Subgroup 19A, dried leaves ...... 260 azoxystrobin, including its metabolites Herb Subgroup 19A, fresh leaves ...... 50 and degradates, in or on the commod- Hop, dried cones ...... 20 .0 ities in the following table. Compliance Ilama ...... 2 .0 Jaboticaba ...... 2 .0 with the tolerance levels specified in Jackfruit ...... 2 .0 the table is to be determined by meas- Longan ...... 2 .0 uring only the sum of azoxystrobin, Loquat ...... 2 .0 [methyl(E)-2-(2-(6-(2-cyanophenoxy) Lychee ...... 2 .0 Mango ...... 2.0 pyrimidin-4-yloxy)phenyl)-3- Nut, tree, group 14 ...... 0 .02 methoxyacrylate], and the Z-isomer of Oats, forage ...... 5 .0 azoxystrobin [methyl(Z)-2-(2-(6-(2- Oats, grain ...... 1 .5 Oats, hay ...... 10.0 cyanophenoxy)pyrimidin-4- Oats, straw ...... 3.0 yloxy)phenyl)-3 methoxyacrylate] in or Onion, bulb, subgroup 3–07A ...... 1 .0 on the commodity. Onion, green, subgroup 3–07B ...... 7 .5 Papaya ...... 2 .0 Parts per Passionfruit ...... 2 .0 Commodity million Pawpaw ...... 2 .0 Pea and bean, dried shelled, except soybean, Acerola ...... 2.0 subgroup 6C ...... 0 .5 Almond, hulls ...... 4 .0 Pea and bean, succulent shelled, subgroup 6B 0 .5 Animal feed, nongrass, group 18, forage ...... 45 Peanut ...... 0 .2 Animal feed, nongrass, group 18, hay ...... 120 Peanut, hay ...... 15.0 Artichoke, globe ...... 4.0 Peanut, refined oil ...... 0.6 Asparagus ...... 0.04 Pear, Asian 1 ...... 0 .07 Atemoya ...... 2 .0 Pepper/eggplant subgroup 8–10B ...... 3 .0 Avocado ...... 2 .0 Peppermint, tops ...... 30 Banana ...... * Persimmon ...... 2 .0 Barley, bran ...... 6 .0 Pistachio ...... 0.50 Barley, forage ...... 25 Pulasan ...... 2 .0 Barley, grain ...... 3 .0 Rambutan ...... 2 .0 Barley, hay ...... 10 .0 Rapeseed subgroup 20A ...... 1 .0 Barley, straw ...... 15 .0 Rice, grain ...... 5 .0 Berry, low growing, subgroup 13–07G, except Rice, hulls ...... 20 cranberry ...... 10.0 Rice, straw ...... 12 Biriba ...... 2 .0 Rice, wild, grain ...... 5.0 Brassica, head and stem, subgroup 5A ...... 3 .0 Rye, forage ...... 7 .0 Brassica, leafy greens, subgroup 5B ...... 25 Rye, grain ...... 0.2 Bushberry subgroup 13–07B ...... 5 .0 Rye, straw ...... 1 .5 Caneberry subgroup 13–07A ...... 5.0 Sapodilla ...... 2 .0 Canistel ...... 2 .0 Sapote, black ...... 2 .0 Cherimoya ...... 2 .0 Sapote, mamey ...... 2 .0 Cilantro, leaves ...... 30.0 Sapote, white ...... 2 .0 Citrus, dried pulp ...... 20 .0 Sorghum, grain, forage ...... 25 Citrus, oil ...... 40.0 Sorghum, grain, grain ...... 11

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(b) Section 18 emergency exemptions. Commodity Parts per million [Reserved] Sorghum, grain, stover ...... 40 (c) Tolerances with regional registra- Soursop ...... 2 .0 tion. [Reserved] Soybean, hay ...... 55 .0 (d) Indirect or inadvertent residues. Soybean, hulls ...... 1 .0 Soybean, seed ...... 0 .5 [Reserved] Spanish lime ...... 2 .0 [62 FR 32235, June 13, 1997] Spearmint, tops ...... 30 Spice Subgroup 19B, except black pepper ...... 38 EDITORIAL NOTE: For FEDERAL REGISTER ci- Star apple ...... 2 .0 tations affecting § 180.507, see the List of CFR Starfruit ...... 2 .0 Sections Affected, which appears in the Sugar apple ...... 2 .0 Sugarcane, cane ...... 0.2 Finding Aids section of the printed volume Sunflower subgroup 20B ...... 0.5 and at www.fdsys.gov. Tamarind ...... 2 .0 Tea, dried 1 ...... 20 .0 § 180.509 Mefenpyr-diethyl; tolerance Tomato, paste ...... 0 .6 for residues. Tomato subgroup 8–10A ...... 0 .2 Turnip, greens ...... 25 (a) General. Tolerances are estab- Vegetable, cucurbit, group 9 ...... 0.3 lished for residues of the safener, Vegetable, foliage of legume, group 7 ...... 30.0 Vegetable, leafy, except brassica, group 4 ...... 30.0 mefenpyr-diethyl, including its me- Vegetable, leaves of root and tuber, group 2 ... 50 .0 tabolites and degradates, when applied Vegetable, legume, edible podded, subgroup at a rate no greater than 0.053 pound 6A, except soybean ...... 3 .0 safener per acre per growing season in Vegetable, root, subgroup 1A ...... 0 .5 Vegetable, tuberous and corm, subgroup 1C ... 8.0 or on the commodities in the table Wasabi, dry ...... 260 below. Compliance with the tolerance Wasabi, fresh ...... 50 levels specified below is to be deter- Watercress ...... 3 .0 Wax jambu ...... 2 .0 mined by measuring only the sum of Wheat, forage ...... 15.0 mefenpyr-diethyl (1-(2,4- Wheat, grain ...... 0 .2 dichlorophenyl)-4,5-dihydro-5-methyl- Wheat, hay ...... 30 .0 Wheat, straw ...... 10 .0 1H-pyrazole-3,5-dicarboxylic acid, diethyl ester) and its 2,4- * 2.0 (of which not more than 0.1 is contained in the pulp) 1 There are no United States registrations for use of dichlorophenyl-pyrazoline metabolites, azoxystrobin on coffee, green bean; ginseng; pear, Asian and calculated as the stoichiometric equiv- tea, dried. alent of mefenpyr-diethyl, in or on the (2) Tolerances are established for res- commodity. idues of the fungicide, azoxystrobin, in- Parts per cluding its metabolites and degradates, Commodity million in or on the commodities in the fol- lowing table. Compliance with the tol- Barley, grain ...... 0 .05 Barley, hay ...... 0 .2 erance levels specified in the table is to Barley, straw ...... 0 .5 be determined by measuring only Cattle, meat byproducts ...... 0.1 azoxystrobin, [methyl(E)-2-(2-(6-(2- Goat, meat byproducts ...... 0 .1 Grass, forage ...... 1 .6 cyanophenoxy) pyrimidin-4- Grass, hay ...... 0 .2 yloxy)phenyl)-3-methoxyacrylate] in or Hog, meat byproducts ...... 0 .1 on the commodity. Horse, meat byproducts ...... 0 .1 Sheep, meat byproducts ...... 0 .1 Parts per Sorghum, grain, forage ...... 0.4 Commodity million Sorghum, grain, grain ...... 0 .04 Sorghum, grain, stover ...... 0 .2 Cattle, fat ...... 0.03 Wheat, forage ...... 0 .2 Cattle, meat ...... 0 .01 Wheat, grain ...... 0 .05 Cattle, meat byproducts ...... 0.07 Wheat, hay ...... 0 .2 Goat, fat ...... 0 .03 Wheat, straw ...... 0 .5 Goat, meat ...... 0.01 Goat, meat byproducts ...... 0 .07 (b) Section 18 emergency exemptions. Hog, fat ...... 0 .010 Hog, meat ...... 0 .01 [Reserved] Hog, meat byproducts ...... 0 .010 (c) Tolerances with regional registra- Horse, fat ...... 0 .03 tions. [Reserved] Horse, meat ...... 0 .01 (d) Indirect or inadvertent residues. Horse, meat byproducts ...... 0 .07 Milk...... 0 .006 Tolerances are established for the indi- Sheep, fat ...... 0 .03 rect or inadvertent residues of Sheep, meat ...... 0.01 mefenpyr-diethyl, including its me- Sheep, meat byproducts ...... 0 .07 tabolites and degradates, when applied

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at a rate no greater than 0.053 pound Commodity Parts per safener per acre per growing season in million or on the commodities identified in the Coffee, green bean ...... 0 .02 table below. Compliance with the toler- Cotton, gin byproducts ...... 2 .0 ance levels specified below is to be de- Cotton, undelinted seed ...... 0 .05 Custard apple ...... 0 .20 termined by measuring only the sum of Date ...... 0 .30 mefenpyr-diethyl (1-(2,4- Feijoa ...... 0 .10 dichlorophenyl)-4,5-dihydro-5-methyl- Fig ...... 0 .30 Fig, dried fruit ...... 1 .0 1H-pyrazole-3,5-dicarboxylic acid, Fruit, citrus, group 10–10 ...... 0 .50 diethyl ester) and its 2,4- Fruit, pome, group 11–10 ...... 0 .20 dichlorophenyl-pyrazoline metabolites, Fruit, small, vine climbing, except grape, sub- calculated as the stoichiometric equiv- group 13–07E ...... 0 .35 Fruit, stone, group 12 ...... 1 .0 alent of mefenpyr-diethyl, in or on the Grain, cereal, group 15 ...... 1.1 commodity. Grain, cereal, forage, fodder and straw, group 16 ...... 1 .1 Parts per Grape ...... 2 .5 Commodity million Grass, forage, fodder, and hay, group 17, for- age ...... 0 .70 Canola, seed ...... 0 .02 Grass, forage, fodder, and hay, group 17, hay 1 .1 Soybean, forage ...... 0 .1 Guava ...... 0 .10 Soybean, hay ...... 0 .1 Herb subgroup 19A ...... 100 Soybean, seed ...... 0 .02 Ilama ...... 0 .20 Jaboticaba ...... 0 .10 Lychee ...... 0 .30 [73 FR 74977, Dec. 10, 2008, as amended at 76 Mango ...... 1.0 FR 23903, Apr. 29, 2011] Nut, tree, group 14 ...... 0 .02 Olive ...... 1 .0 § 180.510 Pyriproxyfen; tolerances for Olive, oil ...... 2 .0 residues. Papaya ...... 1 .0 Passionfruit ...... 0 .10 (a) General. (1) Tolerances are estab- Pawpaw ...... 1 .0 lished for residues of pyriproxyfen, in- Peanut ...... 0 .20 Pineapple ...... 0.30 cluding its metabolites and degradates, Pineapple, process residue ...... 1 .1 in or on the commodities in the fol- Pistachio ...... 0.02 lowing table. Compliance with the tol- Pomegranate ...... 0 .20 erance levels specified is determined by Potato, chips ...... 0 .75 Potato, granules/flakes ...... 0 .75 measuring only pyriproxyfen, 2-[1- Potato, wet peel ...... 0 .75 methyl-2-(4-phenoxyphenoxy) Pulasan ...... 0 .30 ethoxy]pyridine, in or on the com- Rambutan ...... 0 .30 Rice, hulls ...... 5 .5 modity. Safflower, seed ...... 0 .20 Sapodilla ...... 1 .0 Parts per Sapote, black ...... 1 .0 Commodity million Sapote, mamey ...... 1 .0 Acerola ...... 0.10 Sapote, white ...... 0 .30 Almond, hulls ...... 2 .0 Sesame, seed ...... 0 .02 Animal feed, nongrass, group 18, forage ...... 0 .70 Soursop ...... 0 .20 Animal feed, nongrass, group 18, hay ...... 1.1 Spanish lime ...... 0 .30 Animal feed, nongrass, group 18, seed ...... 2 .0 Star apple ...... 1 .0 Apple, wet pomace ...... 0 .8 Starfruit ...... 0 .10 Artichoke, globe ...... 2.0 Strawberry ...... 0 .30 Asparagus ...... 2.0 Sugar apple ...... 0 .20 Atemoya ...... 0 .20 Sugarcane ...... 1 .1 Avocado ...... 1 .0 Tea ...... 0 .02 Banana ...... 0.20 Vegetable, bulb, group 3–07 ...... 0 .70 Beet, sugar, dried pulp ...... 3 .0 Vegetable, cucurbit, group 9 ...... 0.10 Berry, low growing, except strawberry, sub- Vegetable, foliage of legume, group 7 ...... 2 .0 group 13–07H ...... 1.0 Vegetable, fruiting, group 8–10 ...... 0 .80 Biriba ...... 0 .20 Vegetable, leafy, except Brassica, group 4 ...... 3 .0 Brassica, head and stem, subgroup 5A ...... 0 .70 Vegetable, leaves of root and tuber, group 2 ... 2 .0 Brassica, leafy greens, subgroup 5B ...... 2 .0 Vegetable, legume, group 6 ...... 0 .20 Bushberry subgroup 13–07B ...... 1 .0 Vegetable, root and tuber, group 1 ...... 0 .15 Cacao bean, dried ...... 0 .02 Walnut ...... 0 .02 Caneberry subgroup 13–07A ...... 1.0 Watercress ...... 2 .0 Canistel ...... 1 .0 Wax jambu ...... 0 .10 Canola, seed ...... 0 .20 Cherimoya ...... 0 .20 (2) A tolerance of 0.10 parts per mil- Citrus, oil ...... 20 Citrus, dried pulp ...... 2 .0 lion is established for all food commod- Coffee, instant ...... 0 .10 ities as a result of the proposed use of

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NYLAR in food handling establish- Commodity Parts per ments where food and food products are million held, prepared, processed or served. Ap- Atemoya ...... 0 .30 plication is limited to space, general Avocado ...... 0 .30 surface, spot, and/or crack and crevice Banana ...... 0.20 Bean, snap, succulent ...... 0 .02 treatment in food handling establish- Bean, succulent ...... 0 .02 ments where food and food products are Berry, low growing, subgroup 13-07G ...... 2 .5 held, processed, prepared and served. Birida ...... 0 .30 Space and general surface application Brassica, head and stem, subgroup 5A ...... 12.0 Brassica, leafy greens, subgroup 5B ...... 60 may be used only when the facility is Canistel ...... 0 .90 not in operation provided exposed food Cattle, fat ...... 0.05 is covered or removed from the area Cattle, kidney ...... 0 .05 Cattle, liver ...... 0 .05 being treated prior to application. Cattle, meat ...... 0 .05 Spot, and/or crack and crevice treat- Cattle, meat byproducts ...... 0.05 ment may be used while the facility is Cherimoya ...... 0 .30 in operation provided exposed food is Citrus, dried pulp ...... 7 .5 Citrus, oil ...... 80 covered or removed from the area Coffee, green bean ...... 0 .35 being treated prior to application. Cotton, gin byproducts ...... 20 .0 Food contact surfaces should be thor- Cotton, undelinted seed ...... 0 .35 Custard apple ...... 0 .30 oughly washed with an effective clean- Feijoa ...... 0 .30 ing compound and rinced with potable Fruit, citrus, group 10 ...... 2 .5 water after use of the product. To as- Fruit, pome, group 11–10, except pear and sure safe use of this additive, its label pear, Asian ...... 3 .0 Fruit, stone, group 12, except apricot and and labeling shall conform to that reg- peach ...... 1 .9 istered with the U.S. Environmental Goat, fat ...... 0 .05 Protection Agency, and shall be used in Goat, kidney ...... 0 .05 accordance with such label and label- Goat, liver ...... 0.05 Goat, meat ...... 0.05 ing. Goat, meat byproducts ...... 0 .05 (b) Section 18 emergency exemptions. Grape ...... 2 .5 [Reserved] Guava ...... 0 .3 Hog, fat ...... 0 .05 (c) Tolerances with regional registra- Hog, kidney ...... 0.05 tions. [Reserved] Hog, liver ...... 0 .05 (d) Indirect or inadvertent residues. Hog, meat ...... 0 .05 [Reserved] Hog, meat byproducts ...... 0 .05 Horse, fat ...... 0 .05 [64 FR 10233, Mar. 3, 1999] Horse, kidney ...... 0 .05 Horse, liver ...... 0 .05 EDITORIAL NOTE: For FEDERAL REGISTER ci- Horse, meat ...... 0 .05 tations affecting § 180.510, see the List of CFR Horse, meat byproducts ...... 0 .05 Sections Affected, which appears in the Ilama ...... 0 .30 Finding Aids section of the printed volume Jaboticaba ...... 0 .30 and at www.fdsys.gov. Lettuce, head ...... 6.0 Longan ...... 0 .30 Lychee ...... 0 .30 § 180.511 Buprofezin; tolerances for Mango ...... 0.90 residues. Milk ...... 0.01 (a) General. Tolerances are estab- Nut, tree group 14 ...... 0.05 Olive ...... 3 .5 lished for residues of buprofezin, in- Olive, oil ...... 4 .8 cluding its metabolites and degradates Papaya ...... 0 .90 in or on the commodities in the table Passionfruit ...... 0 .30 Peach ...... 9 .0 below. Compliance with the tolerance Pear ...... 6 .0 levels specified below is to be deter- Pear, Asian ...... 6 .0 mined by measuring only the Persimmon ...... 1 .9 buprofezin, 2-[(1,1- Pistachio ...... 0.05 Pomegranate ...... 1 .9 dimethylethyl)imino]tetrahydro-3(1- Pulasan ...... 0 .30 methylethyl)-5-phenyl-4H-1,3,5- Radicchio ...... 6.0 thiadiazin-4-one, in the commodity. Rambutan ...... 0 .30 Sapodilla ...... 0 .90 Parts per Sapote, black ...... 0 .90 Commodity million Sapote, mamey ...... 0 .90 Sheep, fat ...... 0 .05 Acerola ...... 0.30 Sheep, kidney ...... 0.05 Almond, hulls ...... 2 .0 Sheep, liver ...... 0.05 Apricot ...... 9 .0 Sheep, meat ...... 0.05

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(ii) Application may only be under- Commodity Parts per million taken when the facility is not in oper- Sheep, meat byproducts ...... 0 .05 ation, and provided exposed food has Soursop ...... 0 .30 been covered, or removed from the area Spanish lime ...... 0 .30 being treated prior to application. Star apple ...... 0 .90 Starfruit ...... 0 .30 (iii) Food contact surfaces and equip- Sugar apple ...... 0 .30 ment should be throughly washed with Tea1 ...... 20 Turnip, greens ...... 60 an effective cleaning compound, and Vegetable, cucurbit, group 9 ...... 0.50 rinsed with potable water after each Vegetable, fruiting, group 8–10 ...... 2 .0 use of the product. Vegetable, leafy, except Brassica, group 4, ex- cept head lettuce and radicchio ...... 35 (iv) Contamination of food or food Wax jambu ...... 0 .30 contact surfaces shall be avoided. Ap- 1 There are no U.S. registrations at this time. plication excludes any direct applica- tion to any food, food packaging, or (b) Section 18 emergency exemption. any food contact surfaces. [Reserved] (c) Tolerances with regional registra- (v) To assure safe use, the label and tions. [Reserved] labeling shall conform to that reg- (d) Indirect or inadvertent residues. istered by the U.S. Environmental Pro- [Reserved] tection Agency, and it shall be used in accordance with such label and label- [62 FR 40741, July 30, 1997] ing. EDITORIAL NOTE: For FEDERAL REGISTER ci- (b) Section 18 emergency exemptions. tations affecting § 180.511, see the List of CFR [Reserved] Sections Affected, which appears in the Finding Aids section of the printed volume (c) Tolerances with regional registra- and at www.fdsys.gov. tions. [Reserved] (d) Indirect or inadvertent residues. § 180.512 [Reserved] [Reserved] § 180.513 Chlorfenapyr; tolerances for [68 FR 55527, Sept. 26, 2003, as amended at 70 residues. FR 3654, Jan. 26, 2005] (a) General. (1) Tolerances are estab- § 180.514 Cloransulam-methyl; toler- lished for residues of the insecticide ances for residues. chlorfenapyr [4-bromo-2-(4- chlorophenyl)-1-(ethoxymethyl)-5- (a) General. Tolerances are estab- (trifluoromethyl)-1H-pyrrole-3- lished for residues of the herbicide, carbonitrile] in or on the following raw cloransulam-methyl, N-(2- agricultural commodities: carboxymethyl-6-chlorophenyl)-5- ethoxy-7-fluoro-(1,2,4)-triazolo[1,5c]-py- Parts per Commodity million rimidine-2-sulfonamide, plus its acid, cloransulam, calculated as parent ester Vegetable, fruiting, group 8 ...... 1.0 in or on the following raw agricultural commodities: (2) A tolerance of 0.01 parts per mil- lion is established for residues of Parts per chlorfenapyr in or on all food commod- Commodity million ities (other than those covered by a Soybean, forage ...... 0 .1 higher tolerance as a result of use on Soybean, hay ...... 0 .2 growing crops) in food/feed handling Soybean, seed ...... 0 .02 areas where food/feed products are pre- pared, held, processed, or served and in (b) Section 18 emergency exemptions. accordance with the following pre- [Reserved] scribed conditions: (c) Tolerances with regional registra- (i) Application shall be no greater tions. [Reserved] than a 0.5% active ingredient solution (d) Indirect or inadvertent residues. for spot crack and crevice use in food/ [Reserved] feed handling establishments, where food and food products are held, proc- [62 FR 49163, Sept. 19, 1997] essed, prepared and/or served.

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§ 180.515 Carfentrazone-ethyl; toler- Commodity Parts per ances for residues. million (a) General. Tolerances are estab- Goat, fat ...... 0 .10 lished for residues of the herbicide Goat, meat ...... 0.10 Goat, meat byproducts ...... 0 .10 carfentrazone-ethyl, including its me- Grain, aspirated grain fractions ...... 1 .8 tabolites and degradates, in or on the Grain, cereal, forage, fodder and straw group commodities listed in the following 16, except corn and sorghum; forage ...... 1 .0 Grain, cereal, forage, fodder and straw, group table. Compliance with the following 16, hay ...... 0 .30 tolerance levels is to be determined by Grain, cereal, forage, fodder and straw, group measuring only the sum of 16, stover ...... 0 .30 Grain, cereal, forage, fodder and straw, group carfentrazone-ethyl (ethyl-alpha-2- 16, except rice; straw ...... 0.10 dichloro-5-[-4-(difluoromethyl)-4,5- Grain, cereal, group 15 ...... 0.10 dihydro-3-methyl-5-oxo-1H -1,2,4- Grain, cereal, group 15 (except rice grain and triazol-1-yl]-4- sorghum grain) ...... 0 .10 Grain, cereal, stover ...... 0 .80 fluorobenzenepropanoate) and its me- Grain, cereal, straw ...... 3 .0 tabolite carfentrazone-chloropropionic Grape ...... 0 .10 acid (alpha, 2-dichloro-5-[-4- Grass, forage ...... 5 .0 Grass, hay ...... 8 .0 difluoromethyl)-4,5-dihydro-3-methyl-5- Guava ...... 0 .10 oxo-1H-1,2,4-triazol-1-yl]-4- Herbs and spices group 19 ...... 2.0 fluorobenzenepropanoic acid), cal- Hog, fat ...... 0 .10 Hog, meat ...... 0 .10 culated as the stoichiometric equiva- Hog, meat byproducts ...... 0 .10 lent of carfentrazone-ethyl, in or on Hop, dried cones ...... 0 .10 the following commodities: Horse, fat ...... 0 .10 Horse, meat ...... 0 .10 Parts per Horse, meat byproducts ...... 0 .10 Commodity million Horseradish ...... 0.10 Ilama ...... 0 .10 Acerola ...... 0.10 Jaboticaba ...... 0 .10 Almond, hulls ...... 0 .20 Juneberry ...... 0 .10 Animal feed, nongrass, crop group 18, forage 2 .0 Kava, roots ...... 0 .10 Animal feed, nongrass, crop group 18, hay ...... 5 .0 Kiwifruit ...... 0.10 Animal feed, nongrass, crop group 18, seed .... 15 .0 Lingonberry ...... 0.10 Atemoya ...... 0 .10 Longan ...... 0 .10 Avocado ...... 0 .10 Lychee ...... 0 .10 Banana ...... 0.20 Mango ...... 0.10 Barley, bran ...... 0 .80 Milk ...... 0.05 Barley, flour ...... 0 .80 Millet, flour ...... 0 .80 Berry group 13 ...... 0 .10 Mustard, seed ...... 0 .10 Birida ...... 0 .10 Noni ...... 0 .10 Borage ...... 0 .10 Nut, tree, group 14 ...... 0 .10 Cacao bean, bean ...... 0 .10 Oat, flour ...... 0 .80 Cactus ...... 0 .10 Okra ...... 0.10 Caneberry subgroup 13A ...... 0 .1 Canistel ...... 0 .10 Olive ...... 0 .10 Canola ...... 0 .10 Palm heart ...... 0 .10 Cattle, fat ...... 0.10 Palm heart, leaves ...... 0 .10 Cattle, meat ...... 0 .10 Papaya ...... 0 .10 Cattle, meat byproducts ...... 0.10 Passionfruit ...... 0 .10 Cherimoya ...... 0 .10 Pawpaw ...... 0 .10 Coconut ...... 0 .10 Peanut ...... 0 .10 Coffee, bean, green ...... 0 .10 Peanut, hay ...... 0.10 Corn, field, forage ...... 0 .20 Persimmon ...... 0 .10 Corn, sweet, forage ...... 0 .20 Pistachio ...... 0.10 Corn, sweet, kernel plus cob with husk re- Pomegranate ...... 0 .10 moved ...... 0 .10 Poultry, meat byproducts ...... 0.10 Cotton, gin byproducts ...... 10 Pulasan ...... 0 .10 Cotton, undelinted seed ...... 0 .20 Pummelo ...... 0 .10 Cotton, hulls ...... 0 .60 Rambutan ...... 0 .10 Cotton, meal ...... 0 .35 Rapeseed, forage ...... 0 .10 Cotton, refined oil ...... 1.0 Rapeseed, seed ...... 0 .10 Crambe, seed ...... 0.10 Rice, grain ...... 1 .3 Custard apple ...... 0 .10 Rice, hulls ...... 3 .5 Date, dried fruit ...... 0 .10 Rice, straw ...... 1 .0 Feijoa ...... 0 .10 Rye, bran ...... 0 .80 Fig ...... 0 .10 Rye, flour ...... 0 .80 Fish ...... 0 .30 Safflower, seed ...... 0 .10 Flax, seed ...... 0 .10 Salal ...... 0 .10 Fruit, citrus, group 10 ...... 0 .10 Sapodilla ...... 0 .10 Fruit, pome, group 11 ...... 0.10 Sapote, black ...... 0 .10 Fruit, stone, group 12 ...... 0 .10 Sapote, mamey ...... 0 .10

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Parts per Parts per Commodity million Commodity million

Sheep, fat ...... 0 .10 Acerola ...... 5.0 Sheep, meat ...... 0.10 Animal feed, nongrass, group 18 ...... 0 .01 Sheep, meat byproducts ...... 0 .10 Atemoya ...... 20 Shellfish ...... 0 .30 Avocado ...... 5 .0 Sorghum, forage ...... 0 .20 Bean, dry ...... 0.4 Sorghum, grain ...... 0 .25 Bean, succulent ...... 0 .4 Sorghum, sweet ...... 0 .10 Beet, sugar, roots ...... 0 .02 Soursop ...... 0 .10 Berry, low growing, subgroup 13–07G, except Soybean, seed ...... 0 .10 cranberry ...... 3.0 Spanish lime ...... 0 .10 Biriba ...... 20 Star apple ...... 0 .10 Brassica, head and stem, subgroup 5A ...... 2 .0 Starfruit ...... 0 .10 Brassica, leafy greens, subgroup 5B ...... 10 Stevia ...... 0 .10 Bushberry subgroup 13–07B ...... 2 .0 Strawberry ...... 0 .10 Caneberry subgroup 13–07A ...... 5.0 Strawberrypear ...... 0 .10 Canistel ...... 5 .0 Sugar apple ...... 0 .10 Cherimoya ...... 20 Sugarcane ...... 0 .15 Citrus, oil ...... 500 Sunflower, seed ...... 0.10 Cotton, gin byproducts ...... 0 .05 Tea, dried ...... 0 .10 Cotton, undelinted seed ...... 0 .05 Ti, leaves ...... 0 .10 Custard apple ...... 20 Ti, roots ...... 0 .10 Dragon fruit ...... 1 .0 Vanilla ...... 0 .10 Feijoa ...... 5 .0 Vegetable, brassica, leafy, group 5 ...... 0.10 Flax, seed ...... 0 .05 Vegetable, bulb, group 3 ...... 0 .10 Fruit, citrus, group 10–10 ...... 10 Vegetable, cucurbit, group 9 ...... 0.10 Fruit, pome, group 11–10 ...... 5 .0 Vegetable, foliage of legume, except soybean, Fruit, small vine climbing, except fuzzy kiwifruit, subgroup 7A ...... 0 .10 subgroup 13–07F ...... 2 .0 Vegetable, fruiting, group 8 ...... 0.10 Fruit, stone, group 12 ...... 5 .0 Vegetable, leafy, except brassica, group 4 ...... 0 .10 Ginseng ...... 4 .0 Vegetable, leaves of root and tuber, group 2 ... 0 .10 Grain, cereal, group 15 ...... 0.02 Vegetable, legume, group 6 ...... 0 .10 Grain, cereal, forage, fodder, and straw, group Vegetable, root and tuber, group 1 ...... 0 .10 16 ...... 0 .01 Wasaba, roots ...... 0.10 Grass, forage, fodder and hay, group 17 ...... 0 .01 Wax jambu ...... 0 .10 Guava ...... 5 .0 Wheat, bran ...... 0.80 Herb subgroup 19A, dried leaves ...... 65 Wheat, flour ...... 0 .80 Herb subgroup 19A, fresh leaves ...... 10 Wheat, germ ...... 0 .80 Ilama ...... 20 Wheat, middlings ...... 0 .80 Jaboticaba ...... 5 .0 Wheat, shorts ...... 0 .80 Kiwifruit, fuzzy ...... 20 Leaf petioles subgroup 4B ...... 15 Leafy greens subgroup 4A ...... 30 (b) Section 18 emergency exemptions. Longan ...... 20 [Reserved] Lychee ...... 20 (c) Tolerances with regional registra- Mango ...... 5.0 tions. [Reserved] Melon subgroup 9A ...... 0 .03 Onion, bulb, subgroup 3–07A ...... 0 .50 (d) Indirect or inadvertent residues. Onion, green, subgroup 3–07B ...... 7 .0 [Reserved] Papaya ...... 5 .0 Passionfruit ...... 5 .0 [63 FR 52180, Sept. 30, 1998] Peanut ...... 0 .01 Peanut, hay ...... 0.01 EDITORIAL NOTE: For FEDERAL REGISTER ci- Pineapple ...... 20 tations affecting § 180.515, see the List of CFR Pistachio ...... 0.10 Sections Affected, which appears in the Pomegranate ...... 5 .0 Finding Aids section of the printed volume Pulasan ...... 20 and at www.fdsys.gov. Rambutan ...... 20 Rapeseed, forage ...... 0 .01 Rapeseed, seed ...... 0 .01 § 180.516 Fludioxonil; tolerances for Safflower, seed ...... 0 .01 residues. Sapodilla ...... 5 .0 (a) General. (1) Tolerances are estab- Sapote, black ...... 5 .0 Sapote, mamey ...... 5 .0 lished for residues of the fungicide Soursop ...... 20 fludioxonil, including its metabolites Spanish lime ...... 20 and degradates, in or on the commod- Spice subgroup 19B ...... 0 .02 ities in the following table. Compliance Star apple ...... 5 .0 Starfruit ...... 5 .0 with the tolerance levels specified in Sugar apple ...... 20 the following table is to be determined Sunflower, seed ...... 0.01 by measuring only fludioxonil, 4-(2,2- Tomato ...... 5.0 Turnip, greens ...... 10 difluoro-1,3-benzodioxol-4-yl)-1-H- Vegetable, cucurbit, group 9 ...... 0.45 pyrrole-3-carbonitrile). Vegetable, foliage of legume, group 7 ...... 0 .01

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tabolites 5-amino-1-[2,6-dichloro-4- Commodity Parts per million (trifluoromethyl)phenyl]-4- Vegetable, fruiting, group 8–10, except tomato .. 0 .50 [(trifluoromethyl) sulfonyl]-1H-pyr- Vegetable, leaves of root and tuber, group 2 ..... 30 azole-3-carbonitrile and 5-amino-1-[2,6- Vegetable, legume, group 6 ...... 0 .01 dichloro-4-(trifluoromethyl) phenyl]-4- Vegetable, root, except sugar beet, subgroup 1B ...... 0 .75 [(trifluoromethyl)thio]-1H-pyrazole-3- Vegetable, tuberous and corm, subgroup 1C ..... 6.0 carbonitrile and its photodegradate 5- Watercress ...... 7 .0 amino-1-(2,6-dichloro-4- Wax jambu ...... 5 .0 Yam, true, tuber ...... 8.0 (trifluoromethyl)phenyl]-4-[(1R,S)- (trifluoromethyl)]-1H-pyrazole-3- (2) Tolerances are established for res- carbonitrile in or on the following idues of the fungicide fludioxonil, in- items at the levels specified: cluding its metabolites and degradates, Parts per in or on the commodities in the fol- Commodity million lowing table. Compliance with the tol- Cattle, fat ...... 0.40 erance levels specified in the following Cattle, liver ...... 0 .10 table is to be determined by measuring Cattle, meat ...... 0 .04 only the sum of fludioxonil, 4-(2,2- Cattle, meat byproducts, except liver ...... 0 .04 Corn, field, grain ...... 0 .02 difluoro-1,3-benzodioxol-4-yl)-1-H- Corn, field, stover ...... 0 .30 pyrrole-3-carbonitrile), and its metabo- Corn, field, forage ...... 0 .15 lites converted to 2,2-difluoro-l,3- Egg ...... 0 .03 benzodioxole-4-carboxylic acid, cal- Goat, fat ...... 0 .40 Goat, liver ...... 0.10 culated as the stoichiometric equiva- Goat, meat ...... 0.04 lent of fludioxonil. Goat, meat byproducts, except liver ...... 0 .04 Hog, fat ...... 0 .04 Parts per Hog, liver ...... 0 .02 Commodity million Hog, meat ...... 0 .01 Hog, meat byproducts, except liver ...... 0 .01 Cattle, fat ...... 0.05 Horse, fat ...... 0 .40 Cattle, meat ...... 0 .01 Horse, liver ...... 0 .10 Cattle, meat byproducts ...... 0.05 Horse, meat ...... 0 .04 Goat, fat ...... 0 .05 Horse, meat byproducts, except liver ...... 0 .04 Goat, meat ...... 0.01 Milk, fat (reflecting 0.05 ppm in whole milk) ..... 1 .50 Goat, meat byproducts ...... 0 .05 Potato ...... 0 .03 Horse, fat ...... 0 .05 Potato, wet peel ...... 0 .10 Horse, meat ...... 0 .01 Poultry, fat ...... 0.05 Horse, meat byproducts ...... 0 .05 Poultry, meat ...... 0 .02 Milk ...... 0.01 Poultry, meat byproducts ...... 0.02 Sheep, fat ...... 0 .05 Rice, grain ...... 0 .04 Sheep, meat ...... 0.01 Rice, straw ...... 0 .10 Sheep, meat byproducts ...... 0 .05 Sheep, fat ...... 0 .40 Sheep, liver ...... 0.10 (b) Section 18 emergency exemptions. Sheep, meat ...... 0.04 Sheep, meat byproducts, except liver ...... 0 .04 [Reserved] (c) Tolerances with regional registra- (b) Section 18 emergency exemptions.. tions. [Reserved] Time-limited tolerances are estab- (d) Indirect or inadvertent residues. lished for combined residues of the in- [Reserved] secticide, fipronil, 5-amino-1-(2,6- [62 FR 56082, Oct. 29, 1997] dichloro-4-(trifluoromethyl) phenyl)-4- ((1,R,S)-trifluoromethyl)sulfinyl)-1-H- EDITORIAL NOTE: For FEDERAL REGISTER ci- tations affecting § 180.516, see the List of CFR pyrazole-3-carbonitrile and its 2 me- Sections Affected, which appears in the tabolites MB45950 (5-amino-1-(2,6- Finding Aids section of the printed volume dichloro-4-(trifluoromethyl)phenyl)-4- and at www.fdsys.gov. [(trifluoromethyl)thio]-1H-pyrazole-3- carbonitrile) and MB46136 (5-amino-1- § 180.517 Fipronil; tolerances for resi- (2,6-dichloro-4- dues. (trifluoromethyl)phenyl)-4- (a) General. Therefore, tolerances are [(trifluoromethyl)sulfonyl]-1H-pyr- established for combined residues of azole-3-carbonitrile) and its the insecticide fipronil (5-amino-1-[2,6- photodegradate MB46513 (5-amino-1- dichloro-4-(trifluoromethyl)phenyl]-4- (2,6-dichloro-4- [(1R,S)-(trifluoromethyl)sulfinyl]-1H- (trifluoromethyl)phenyl]-4-[(1R,S)- pyrazole-3-carbonitrile) and its me- (trifluoromethyl)]-1H-pyrazole-3-

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carbonitrile), in connection with use of Commodity Parts per the pesticide under Section 18 emer- million gency exemptions granted by EPA. The Fruit, stone, group 12 ...... 10 tolerances expire and are revoked on Ginseng ...... 1 .5 the dates specified in the table for this Grape, raisin ...... 8 .0 paragraph. Lemon, preharvest and postharvest ...... 11 Onion, bulb, subgroup 3–07A ...... 2 .0 Expiration/ Onion, green, subgroup 3–07B ...... 3 .0 Commodity Parts per revocation Pistachio ...... 0.20 million date Pomegranate ...... 5 .0 Tomato ...... 0.50 Rutabaga ...... 1.0 12/31/16 Vegetable, tuberous and corm, subgroup 1C ... 0.05 Turnip ...... 1.0 12/31/16 (2) Tolerances are established for res- (c) Tolerances with regional registra- idues of the fungicide pyrimethanil, in- tions. [Reserved] cluding its metabolites and degradates, (d) Indirect or inadvertent residues. in or on the commodities in the fol- Tolerances are established for com- lowing table. Compliance with the tol- bined indirect or inadvertent residues erance levels specified in the following of the insecticide fipronil and its me- table is to be determined by measuring tabolites and photodegradate in or on only the sum of pyrimethanil and its food commodities when present therein metabolite 4-[4,6-dimethyl-2- as a result of the application of fipronil pyrimidinyl)amino]phenol, calculated to growing crops listed in paragraphs as the stoichiometric equivalent of (a) and (b) of this section and other pyrimethanil. nonfood crops to read as follows: Parts per Parts per Commodity million Commodity million Cattle, fat ...... 0.01 Wheat, forage ...... 0 .02 Cattle, kidney ...... 2 .5 Wheat, grain ...... 0 .005 Wheat, hay ...... 0 .03 Cattle, meat ...... 0 .01 Wheat, straw ...... 0 .03 Cattle, meat byproducts, except kidney ...... 0.01 Goat, fat ...... 0 .01 Goat, kidney ...... 2 .5 [62 FR 62979, Nov. 26, 1997, as amended at 63 Goat, meat ...... 0.01 FR 38495, July 17, 1998; 72 FR 46913, Aug. 22, Goat, meat byproducts, except kidney ...... 0 .01 2007; 74 FR 46377, Sept. 9, 2009; 75 FR 80346, Horse, fat ...... 0 .01 Dec. 22, 2010; 78 FR 78748, Dec. 27, 2013] Horse, kidney ...... 2 .5 Horse, meat ...... 0 .01 Horse, meat byproducts, except kidney ...... 0 .01 § 180.518 Pyrimethanil; tolerances for Sheep, fat ...... 0 .01 residues. Sheep, kidney ...... 2.5 (a) General. (1) Tolerances are estab- Sheep, meat ...... 0.01 lished for residues of the fungicide Sheep, meat byproducts, except kidney ...... 0 .01 pyrimethanil, including its metabolites (3) Tolerances are established for res- and degradates, in or on the commod- idues of the fungicide pyrimethanil, in- ities in the following table Compliance cluding its metabolites and degradates, with the tolerance levels specified in in or on the commodities in the fol- the following table is to be determined lowing table. Compliance with the tol- by measuring only pyrimethanil (4,6-di- erance levels specified in the following methyl-N-phenyl-2-pyrimidinamine). table is to be determined by measuring only the sum of pyrimethanil and its Commodity Parts per million metabolite 4,6-dimethyl-2- Almond ...... 0.20 (phenylamino)-5-pyrimidinol, cal- Almond, hulls ...... 12 culated as the stoichiometric equiva- Apple, wet pomace ...... 40 lent of pyrimethanil. Banana ...... 0.10 Berry, low growing, subgroup 13–07G ...... 3 .0 Parts per Citrus, oil ...... 150 Commodity million Fruit, citrus, group 10, except lemon, postharvest ...... 10 Milk ...... 0.05 Fruit, pome, group 11 (pre-harvest and post- harvest) ...... 14 Fruit, small, vine climbing, subgroup 13–07F, (b) Section 18 emergency exemptions. except fuzzy kiwifruit ...... 5 .0 [Reserved]

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(c) Tolerances with regional registra- istered by the U.S. Environmental Pro- tions. [Reserved] tection Agency. (d) Indirect or inadvertent residues. (3) Residues of inorganic bromides [Reserved] (calculated as Br) in milled fractions [62 FR 63669, Dec. 2, 1997, as amended at 69 derived from cereal grain from all fu- FR 52443, Aug. 26, 2004; 73 FR 64251, Oct. 29, migation sources, including fumigation 2008; 74 FR 32448, July 8, 2009; 77 FR 45503, of grain-mill machinery, shall not ex- Aug. 1, 2012; 80 FR 7975, Feb. 13, 2015] ceed 125 parts per million. (b) Section 18 emergency exemptions. § 180.519 Bromide ion and residual [Reserved] bromine; tolerances for residues. (c) Tolerances with regional registra- (a) General. The food additives, bro- tions. [Reserved] mide ion and residual bromine, may be (d) Indirect or inadvertent residues. present in water, potable in accordance [Reserved] with the following conditions: (1) The food additives are present as [40 FR 14156, Mar. 28, 1975. Redesignated at 41 a result of treating water aboard ships FR 26568, June 28, 1976, as amended at 49 FR with a polybrominated ion-exchange 44459, Nov. 7, 1984. Further redesignated at 53 resin (as a source of bromine) under the FR 24667, June 29, 1988, as amended at 54 FR supervision of trained personnel. 6130, Feb. 8, 1989. Further redesignated and amended at 63 FR 34319, June 24, 1998] (2) Residual bromine levels are con- trolled to not exceed 1.0 part per mil- § 180.522 Fumigants for processed lion (ppm) in the final treated water. grains used in production of fer- Control is effected using calibrated re- mented malt beverage; tolerances circulating or proportioning bromine for residues. feeder equipment and periodic checks (a) General. Fumigants for processed of residual bromine using a bromine grain may be safely used, in accordance test kit. To assure safe use of the addi- with the following conditions. tives, the label and labeling of the dis- (1) Methyl bromide. Total residues of infectant formulation containing the inorganic bromides (calculated as Br) food additives shall conform to the from the use of this fumigant shall not label and labeling registered by the exceed 125 parts per milion. U.S. Environmental Protection Agen- cy. (2) Methyl bromide is used to fumi- (3) No tolerance is established for gate corn grits and cracked rice in the bromide ion levels. production of fermented malt beverage. (b) Section 18 emergency exemptions. (3) To assure safe use of the fumi- [Reserved] gant, its label and labeling shall con- (c) Tolerances with regional registra- form to the label and labeling reg- tions. [Reserved] istered by the U.S. Environmental Pro- (d) Indirect or inadvertent residues. tection Agency, and the usage em- [Reserved] ployed should conform with such label or labeling. [41 FR 17893, Apr. 29, 1976. Redesignated at 41 (4) The total residue of inorganic bro- FR 26568, June 28, 1976, and at 53 FR 24667, June 29, 1988. Redesignated and amended at mides in fermented malt beverage, re- 63 FR 34319, June 24, 1998; 71 FR 74818, Dec. sulting from the use of corn grits and 13, 2006] cracked rice fumigated with the fumi- gant described in paragraph (a)(2) of § 180.521 Fumigants for grain-mill ma- this section plus additional residues of chinery; tolerances for residues. inorganic bromides that may be (a) General. Fumigants may be safely present from uses in accordance with used in or on grain-mill machinery in other regulations in this chapter pro- accordance with the following pre- mulgated under section 408 and/or 409 scribed conditions: of the Act, does not exceed 25 parts per (1) The fumigants consist of methyl million bromide (calculated as Br). bromide. (b) Section 18 emergency exemptions. (2) To assure safe use of the fumi- [Reserved] gant, its label and labeling shall con- (c) Tolerances with regional registra- form to the label and labeling reg- tions. [Reserved]

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(d) Indirect or inadvertent residues. Commodity Parts per [Reserved] million [71 FR 74818, Dec. 13, 2006] Clover, forage ...... 0.60 Clover, hay ...... 0.60 Soybean, seed ...... 0.05 § 180.523 Metaldehyde; tolerances for residues. (d) Indirect or inadvertent residues. (a) General. Tolerances are estab- [Reserved] lished for residues of the molluscicide [73 FR 54963, Sept. 24, 2008, as amended at 78 metaldehyde, including its metabolites FR 70869, Nov. 27, 2013; 80 FR 11588, Mar. 4, and degradates, in or on the commod- 2015] ities listed in the following table. Com- pliance with the specified tolerance § 180.525 Resmethrin; tolerances for levels is to be determined by meas- residues. uring only metaldehyde, 2,4,6,8- (a) General. Tolerances are estab- tetramethyl-1,3,5,7-tetroxocane, in or lished for residues of the insecticide on the commodity. resmethrin [5-(phenylmethyl)-3- furanyl] methyl 2,2-dimethyl-3-(2- Parts per Commodity million methyl-1-propenyl) cyclopropanecarboxylate in or on food Artichoke, globe ...... 0.07 commodities at 3.0 ppm resulting from Berry, low growing, subgroup 13–07G ...... 6 .25 Bushberry subgroup 13–07B ...... 0 .15 use of the insecticide in food handling Cactus ...... 0 .07 and storage areas as a space concentra- Caneberry subgroup 13–07A ...... 0.15 tion for spot/or crack and crevice treat- Corn, field, forage ...... 0 .30 ment and shall be limited to a max- Corn, field, grain ...... 0 .05 Corn, field, stover ...... 0 .10 imum of 3.00 percent of the active in- Corn, sweet, forage ...... 0 .30 gredient by weight, and as a space Corn, sweet, kernel plus cob with husks re- treatment shall be limited to a max- moved ...... 0 .05 imum of 0.5 fluid ounce of 3.0 percent Corn, sweet, stover ...... 0 .10 Fruit, citrus, group 10–10 ...... 0 .26 active ingredient by weight per 1000 Ginseng ...... 0 .05 cubic feet of space provided that the Grass, forage ...... 2 .0 food is removed or covered prior to Grass, hay ...... 2 .0 Leaf petioles subgroup 4B ...... 0 .50 such use. To assure safe use of the ad- Lettuce ...... 1.73 ditive, its label and labeling shall con- Pea and bean, succulent shelled, subgroup 6B 0 .20 form to that registered with the U.S. Peppermint, oil ...... 12 Environmental Protection Agency, and Peppermint, tops ...... 4 .0 Spearmint, oil ...... 12 shall be used in accordance with such Spearmint, tops ...... 4 .0 label and labeling. Taro, corm ...... 0 .15 (b) Section 18 emergency exemptions. Taro, leaves ...... 1 .0 [Reserved] Tomato subgroup 8–10A ...... 0 .24 Vegetable, brassica, leafy, group 5 ...... 2.5 (c) Tolerances with regional registra- Vegetable, foliage of legume, except soybean, tions. [Reserved] subgroup 7A ...... 1 .5 (d) Indirect or inadvertent residues. Vegetable, legume, edible podded subgroup 6A 0 .80 [Reserved] Watercress ...... 3 .2 [71 FR 74819, Dec. 13, 2006] (b) Section 18 emergency exemptions. [Reserved] § 180.526 Synthetic isoparaffinic petro- (c) Tolerances with regional registra- leum hydrocarbons; tolerances for tions. Tolerances with a regional reg- residues. istration as defined in § 180.1(l) are es- (a) General. Synthetic isoparaffinic tablished for residues of the petroleum hydrocarbons complying molluscicide metaldehyde, including with 21 CFR 172.882 (a) and (b) may be its metabolites and degradates, in or safely used as a component of insecti- on the following commodities. Compli- cide formulations for use on animal ance with the specified tolerance level feed in an amount no greater than rea- is to be determined by measuring only sonably required to accomplish its in- metaldehyde, 2,4,6,8-tetramethyl- tended effect as an adjuvant in the in- 1,3,5,7-tetroxocane, in or on the com- secticide formulation and shall not be modity. intended to accomplish any effect in

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animal feed. It is used or intended for benzenamine moiety, with regional use as a component of insecticide for- registration. mulations used in compliance with reg- ulations issued in 40 CFR part 180 and Parts per Commodity million in this part. (b) Section 18 emergency exemptions. Grass, forage ...... 7 .0 [Reserved] Grass, hay ...... 0 .4 (c) Tolerances with regional registra- tions. [Reserved] (d) Indirect or inadvertent residues. (d) Indirect or inadvertent residues. Tolerances are established for indirect [Reserved] or inadvertent residues of the herbicide flufenacet, N-(4-fluorophenyl)-N-(1- [40 FR 14161, Mar. 28, 1975, as amended at 50 methylethyl)-2-[[5-(trifluoromethyl)- FR 2959, Jan. 23, 1985, and amended at 53 FR 1,3,4-thiadiazol-2-yl]oxy]acetamide and 24668, 24669, June 29, 1988. Redesignated and amended at 63 FR 34319, June 24, 1998] its metabolites containing the 4-fluoro- N-methylethyl benzenamine moiety in § 180.527 Flufenacet, N-(4- or on the following raw agricultural fluorophenyl)-N-(1-methylethyl)-2- commodities when present therein as a [[5-(trifluoromethyl)-1, 3, 4- result of application of flufenacet to thiadiazol-2-yl] oxy]acetamide and the growing crops in paragraph (a) of its metabolites containing the 4- this section. fluoro-N-methylethyl benzenamine tolerances for residues. Commodity Parts per (a) General. Tolerances are estab- million lished for the combined residues of the Alfalfa, forage ...... 0.1 herbicide flufenacet, N-(4- Alfalfa, hay ...... 0.1 fluorophenyl)-N-(1-methylethyl)-2-[[5- Alfalfa, seed ...... 0 .1 (trifluoromethyl)-1, 3, 4-thiadiazol-2-yl] Clover, forage ...... 0.1 oxy]acetamide and its metabolites con- Clover, hay ...... 0.1 taining the 4-fluoro-N-methylethyl Grain, cereal, group 15, except rice ...... 0 .1 Grain, cereal, forage, fodder, and straw, group benzenamine moiety in or on the fol- 16, except rice ...... 0 .1 lowing commodities. Grass, forage, fodder, and hay, group 17 ...... 0 .1

Commodity Parts per million [63 FR 26473, May 13, 1998, as amended at 63 FR 50791, Sept. 23, 1998; 64 FR 42846, Aug. 6, Cattle, kidney ...... 0 .05 1999; 65 FR 64366, Oct. 27, 2000; 68 FR 2247, Corn, field, forage ...... 0 .4 Corn, field, grain ...... 0 .05 Jan. 16, 2003; 68 FR 37759, June 25, 2003; 70 FR Corn, field, stover ...... 0 .4 37696, June 30, 2005; 71 FR 76200, Dec. 20, 2006; Corn, sweet, forage ...... 0 .45 72 FR 26310, May 9, 2007] Corn, sweet, kernel plus cob with husks re- moved ...... 0 .05 § 180.530 2,2-Dimethyl-1,3-benzodioxol- Corn, sweet, stover ...... 0 .30 4-ol methylcarbamate; tolerances Goat, kidney ...... 0 .05 Hog, kidney ...... 0.05 for residues. Horse, kidney ...... 0 .05 (a) General. (1) The insecticide 2,2-di- Sheep, kidney ...... 0.05 Soybean, seed ...... 0 .1 methyl-1,3-benzodioxol-4-yl Wheat, bran ...... 0.80 methylcarbamate may be safely used Wheat, forage ...... 6 .0 in spot and/or crack and crevice treat- Wheat, grain ...... 0 .60 ments in animal feed handling estab- Wheat, hay ...... 1 .2 Wheat, straw ...... 0 .35 lishments, including feed manufac- turing and processing establishments, (b) Section 18 emergency exemptions. such as stores, supermarkets, dairies, [Reserved] meat slaughtering and packing plants, (c) Tolerances with regional registra- and canneries until the tolerance expi- tions. Tolerances are established for ration/revocation date of April 26, 2005. combined residues of flufenacet, N-(4- (2) The insecticide 2,2-dimethyl-1,3- fluorophenyl)-N-(1-methylethyl)-2-[[5- benzodioxol-4-yl methylcarbamate may (trifluoromethyl)-1, 3, 4-thiadiazol-2-yl] be safely used in spot and/or crack and oxy]acetamide, and its metabolites crevice treatments in food handling es- containing the 4-fluoro-N-methylethyl tablishments, including food service,

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manufacturing and processing estab- Commodity Parts per lishments, such as restaurants, cafe- million terias, supermarkets, bakeries, brew- Lychee ...... 2 .0 eries, dairies, meat slaughtering and Mango ...... 1.2 packing plants, and canneries until the Onion, bulb, subgroup 3–07A ...... 0 .6 Onion, green, subgroup 3–07B ...... 4 .0 tolerance expiration/revocation date of Papaya ...... 1 .2 April 26, 2005. Parsley, dried leaves ...... 170 (3) To ensure safe use of the additive, Parsley, leaves ...... 35 Pistachio ...... 0.10 its label and labeling shall conform to Pulasan ...... 2 .0 that registered with the U.S. Environ- Rambutan ...... 2 .0 mental Protection Agency and it shall Sapodilla ...... 1 .2 Sapote, black ...... 1 .2 be used in accordance with such label Sapote, mamey ...... 1 .2 and labeling. Spanish lime ...... 2 .0 (b) Section 18 emergency exemptions. Star apple ...... 1 .2 Turnip, greens ...... 10.0 [Reserved] Vegetable, cucurbit, group 9 ...... 0.70 (c) Tolerances with regional registra- Vegetable, fruiting, group 8–10 ...... 1 .5 tions. [Reserved] Vegetable, leaves of root and tuber, group 2 ..... 10 (d) Indirect or inadvertent residues. Vegetable, root, except sugarbeet, subgroup 1B 0 .75 Watercress ...... 20 [Reserved] 1 Import only. [63 FR 34828, June 26, 1998, as amended at 69 FR 58083, Sept. 29, 2004] (2) Tolerances are established for res- idues of the fungicide cyprodinil, in- § 180.532 Cyprodinil; tolerances for cluding its metabolites and degradates, residues. in the commodities in the table below. (a) General. (1) Tolerances are estab- Compliance with the tolerance levels lished for residues of the fungicide specified below is to be determined by cyprodinil, including its metabolites measuring only the sum of cyprodinil and degradates, in or on the commod- 4-cyclopropyl-6-methyl-N-phenyl-2- ities in the table below. Compliance pyrimidinamine and free and con- with the tolerance levels specified jugated CGA–304075 4-(4-cyclopropyl-6- below is to be determined by measuring methyl-pyrimidin-2-ylamino)-phenol, only cyprodinil 4-cyclopropyl-6-meth- calculated as the stoichiometric equiv- yl-N-phenyl-2-pyrimidinamine. alent of cyprodinil.

Parts per Commodity Parts per Commodity million million

Almond ...... 0.02 Cattle, meat byproducts ...... 0.02 Almond, hulls ...... 8 .0 Goat, meat byproducts ...... 0 .02 Apple, wet pomace ...... 4 .6 Horse, meat byproducts ...... 0 .02 Avocado ...... 1 .2 Sheep, meat byproducts ...... 0 .02 Bean, dry ...... 0.6 Bean, succulent ...... 0 .6 (b) Section 18 emergency exemptions. Berry, low growing, subgroup 13–07G, except [Reserved] cranberry ...... 5.0 Brassica, head and stem, subgroup 5A ...... 1 .0 (c) Tolerances with regional registra- Brassica, leafy greens, subgroup 5B ...... 10 .0 tions. [Reserved] Bushberry subgroup 13–07B ...... 3 .0 (d) Indirect or inadvertent residues. Caneberry subgroup 13–07A ...... 10 Canistel ...... 1 .2 [Reserved] 1 Canola, seed ...... 0 .03 [63 FR 17706, Apr. 10, 1998] Citrus, dried pulp ...... 8 .0 Citrus, oil ...... 60 EDITORIAL NOTE: For FEDERAL REGISTER ci- Dragon fruit ...... 2 .0 tations affecting § 180.532, see the List of CFR Fruit, pome, group 11–10 ...... 1 .7 Sections Affected, which appears in the Fruit, small vine climbing, except fuzzy kiwifruit, subgroup 13–07F ...... 3 .0 Finding Aids section of the printed volume Fruit, stone, group 12 ...... 2 .0 and at www.fdsys.gov. Grape, raisin ...... 5 .0 Herb subgroup 19A, dried, except parsley ...... 15 .0 § 180.533 Esfenvalerate; tolerances for Herb subgroup 19A, fresh, except parsley ...... 3 .0 residues. Kiwifruit ...... 1.8 Leaf petioles subgroup 4B ...... 30 (a) General. (1) Tolerances are estab- Leafy greens subgroup 4A ...... 50 lished for the combined residues of the Lemon ...... 0.60 Lime ...... 0.60 insecticide esfenvalerate, (S)-cyano(3- Longan ...... 2 .0 phenoxyphenyl)methyl-(S)-4-chloro-a-

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(1-methylethyl)benzeneacetate, its Commodity Parts per non-racemic isomer, (R)-cyano(3- million phenoxyphenyl)methyl-(R)-4-chloro-a- Pepper ...... 0 .5 (1-methylethyl)benzeneacetate and its Potato ...... 0 .02 diastereomers (S)-cyano(3- Poultry, fat ...... 0.3 Poultry, liver ...... 0 .03 phenoxyphenyl)methyl-(R)-4-chloro-a- Poultry, meat ...... 0 .03 (1-methylethyl)benzeneacetate and (R)- Poultry, meat byproducts, except liver ...... 0 .3 cyano(3-phenoxyphenyl)methyl-(S)-4- Pumpkin ...... 0.5 Radish, roots ...... 0 .3 chloro-a-(1- Radish, tops ...... 3 .0 methylethyl)benzeneacetate, in or on Sheep, fat ...... 1 .5 food commodities as follows: Sheep, meat ...... 1.5 Sheep, meat byproducts ...... 1 .5 Parts per Sorghum, grain, forage ...... 10.0 Commodity million Sorghum, grain, grain ...... 5 .0 Sorghum, grain, stover ...... 10 .0 Almond ...... 0.2 Soybean, hulls ...... 0 .5 Almond, hulls ...... 5 .0 Soybean, seed ...... 0 .05 Apple ...... 1.0 Squash, summer ...... 0 .5 Artichoke, globe ...... 1.0 Squash, winter ...... 0 .5 Bean, dry, seed ...... 0 .25 Sugarcane, cane ...... 1.0 Bean, snap, succulent ...... 1 .0 Sunflower, seed ...... 0.5 Beet, sugar, roots ...... 0 .05 Sweet potato, roots ...... 0 .05 Beet, sugar, tops ...... 5.0 Tomato ...... 0.5 Blueberry ...... 1 .0 Turnip, greens ...... 7.0 Broccoli ...... 1 .0 Turnip, roots ...... 0 .5 Cabbage, except Chinese cabbage ...... 3.0 Walnut ...... 0 .2 Caneberry subgroup 13A ...... 1 .0 Watermelon ...... 0.5 Cantaloupe ...... 0 .5 Carrot, roots ...... 0.5 (2) A tolerance of 0.05 ppm on raw ag- Cattle, fat ...... 1.5 Cattle, meat ...... 1 .5 ricultural food commodities (other Cattle, meat byproducts ...... 1.5 than those food commodities already Cauliflower ...... 0 .5 covered by a higher tolerance as a re- Collards ...... 3.0 sult of use on growing crops) is estab- Corn, field, forage ...... 15 .0 Corn, field, grain ...... 0 .02 lished for the combined residues of the Corn, field, stover ...... 15 .0 insecticide esfenvalerate, (S)-cyano(3- Corn, pop, grain ...... 0.02 phenoxyphenyl)methyl-(S)-4-chloro-a- Corn, pop, stover ...... 15.0 Corn, sweet, forage ...... 15 .0 (1-methylethyl)benzeneacetate, its Corn, sweet, kernel plus cob with husks re- non-racemic isomer, (R)-cyano(3- moved ...... 0 .1 phenoxyphenyl)methyl-(R)-4-chloro-a- Corn, sweet, stover ...... 15.0 (1-methylethyl)benzeneacetate and its Cotton, undelinted seed ...... 0 .2 Cucumber ...... 0 .5 diastereomers (S)-cyano(3- Egg ...... 0 .03 phenoxyphenyl)methyl-(R)-4-chloro-a- Eggplant ...... 0.5 (1-methylethyl)benzeneacetate and (R)- Elderberry ...... 1 .0 Fruit, stone, group 12 ...... 3 .0 cyano(3-phenoxyphenyl)methyl-(S)-4- Goat, fat ...... 1 .5 chloro-a-(1- Goat, meat ...... 1.5 methylethyl)benzeneacetate as a result Goat, meat byproducts ...... 1 .5 of the use of esfenvalerate in food-han- Gooseberry ...... 1 .0 Hazelnut ...... 0 .2 dling establishments. Hog, fat ...... 1 .5 (b) Section 18 emergency exemptions. Hog, meat ...... 1 .5 [Reserved] Hog, meat byproducts ...... 1 .5 (c) Tolerances with regional registra- Horse, fat ...... 1 .5 Horse, meat ...... 1 .5 tions. Tolerances with regional reg- Horse, meat byproducts ...... 1 .5 istration are established for the com- Kiwifruit ...... 0.5 bined residues of the insecticide Lentil, seed ...... 0 .25 Melon, honeydew ...... 0.5 esfenvalerate, (S)-cyano(3- Milk ...... 0.3 phenoxyphenyl)methyl-(S)-4-chloro-a- Milk, fat ...... 7 .0 (1-methylethyl)benzeneacetate, its Muskmelon ...... 0 .5 non-racemic isomer, (R)-cyano(3- Mustard greens ...... 5.0 Okra ...... 0.5 phenoxyphenyl)methyl-(R)-4-chloro-a- Pea, dry, seed ...... 0 .25 (1-methylethyl)benzeneacetate and its Pea, succulent ...... 0 .5 diastereomers (S)-cyano(3- Peanut ...... 0 .02 Pear ...... 1 .0 phenoxyphenyl)methyl-(R)-4-chloro-a- Pecan ...... 0 .2 (1-methylethyl)benzeneacetate and (R)-

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cyano(3-phenoxyphenyl)methyl-(S)-4- Commodity Parts per chloro-a-(1- million methylethyl)benzeneacetate, in or on Hog, meat ...... 0 .1 food commodities as follows: Hog, meat byproducts ...... 0 .1 Horse, fat ...... 0 .1 Commodity Parts per Horse, kidney ...... 1 .5 million Horse, meat ...... 0 .1 Horse, meat byproducts ...... 0 .1 Cabbage, chinese, bok choy ...... 1 .0 Kohlrabi ...... 2 .0 Milk ...... 0.3 Lettuce, head ...... 5.0 Millet, forage ...... 12.0 Millet, grain ...... 0 .5 (d) Indirect or inadvertent residues. Millet, hay ...... 20.0 Millet, proso, straw ...... 12 .0 [Reserved] Oat, forage ...... 12 .0 [63 FR 23401, Apr. 29, 1998, as amended at 63 Oat, grain ...... 0 .5 FR 48615, Sept. 11, 1998; 74 FR 46699, Sept. 11, Oat, hay ...... 20.0 Oat, straw ...... 12.0 2009] Onion, bulb ...... 0 .03 Rice, bran ...... 3.0 § 180.535 Fluroxypyr 1-methylheptyl Rice, grain ...... 1 .5 ester; tolerances for residues. Shallot, bulb ...... 0 .03 (a) General. Tolerances are estab- Sheep, fat ...... 0 .1 Sheep, kidney ...... 1.5 lished for combined residues of Sheep, meat ...... 0.1 fluroxypyr 1-methylheptyl ester [1- Sheep, meat byproducts ...... 0 .1 methylheptyl ((4-amino-3,5-dichloro-6- Sorghum, grain, forage ...... 2.0 fluoro-2-pyridinyl)oxy)acetate] and its Sorghum, grain, grain ...... 0 .02 metabolite fluroxypyr [((4-amino-3,5- Sorghum, grain, stover ...... 4 .0 Wheat, forage ...... 12.0 dichloro-6-fluoro-2-pyridinyl)oxy)acetic Wheat, grain ...... 0 .5 acid] in or on the following raw agri- Wheat, hay ...... 20 .0 cultural commodities. Compliance with Wheat, straw ...... 12 .0 the established tolerance levels is de- termined by measuring only the sum of (b) Section 18 emergency exemptions. fluroxypyr 1-methylheptyl ester [1- [Reserved] methylheptyl ((4-amino-3, 5-dichloro-6- (c) Tolerances with regional registra- fluoro-2-pyridinyl)oxy)acetate] and its tions. [Reserved] metabolite fluroxypyr [((4-amino-3,5- (d) Indirect or inadvertent residues. dichloro-6-fluoro-2-pyridinyl)oxy)acetic [Reserved] acid] calculated as the stoichiometric [63 FR 52169, Sept. 30, 1998, as amended at 64 equivalent of fluroxypyr. FR 22799, Apr. 28, 1999; 66 FR 37598, July 19, 2001; 66 FR 47971, Sept. 17, 2001; 67 FR 46884, Parts per Commodity million July 17, 2002; 67 FR 60146, Sept. 25, 2002; 68 FR 75438, Dec. 31, 2003; 69 FR 2074, Jan. 14, 2004; Barley, grain ...... 0 .5 70 FR 3649, Jan. 26, 2005; 70 FR 7047, Feb. 10, Barley, hay ...... 12 .0 2005; 71 FR 76204, Dec. 20, 2006; 72 FR 73635, Barley, hay ...... 20 .0 Barley, straw ...... 12 .0 Dec. 28, 2007; 78 FR 3333, Jan. 16, 2013] Cattle, fat ...... 0.1 Cattle, kidney ...... 1 .5 § 180.537 Isoxaflutole; tolerances for Cattle, meat ...... 0 .1 residues. Cattle, meat byproducts ...... 0.1 Corn, field, forage ...... 1 .0 (a) General. Tolerances are estab- Corn, field, grain ...... 0 .02 lished for residues of the herbicide, Corn, field, stover ...... 0 .5 Corn, sweet, forage ...... 1 .0 isoxaflutole, including its metabolites Corn, sweet, kernel plus cob with husks re- and degradates, in or on the commod- moved ...... 0 .02 ities in the table below. Compliance Corn, sweet, stover ...... 2 .0 Fruit, pome, group 11 ...... 0.02 with the tolerance levels specified Garlic, bulb ...... 0.03 below is to be determined by measuring Goat, fat ...... 0 .1 only the sum of isoxaflutole ((5- Goat, kidney ...... 1 .5 cyclopropyl-4-isoxazolyl) [2- Goat, meat ...... 0.1 Goat, meat byproducts ...... 0 .1 (methylsulfonyl)-4- Grain, aspirated fractions ...... 0 .6 (trifluoromethyl)phenyl] methanone) Grass, forage ...... 120 and its metabolite 1-(2-methylsulfonyl- Grass, hay ...... 160 Hog, fat ...... 0 .1 4-trifluoromethylphenyl)-2-cyano-3- Hog, kidney ...... 1.5 cyclopropyl propan-1,3-dione (RPA

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202248), calculated as the stoichio- (b) Section 18 emergency exemptions. metric equivalent of isoxaflutole, in or [Reserved] on the commodity: (c) Tolerances with regional registra- tions. [Reserved] Parts per Commodity million (d) Indirect or inadvertent residues. [Reserved] Corn, field, forage ...... 0 .04 Corn, field, grain ...... 0 .02 [73 FR 54963, Sept. 24, 2008] Corn, field, stover ...... 0 .02 Grain, aspirated fractions ...... 0 .30 § 180.541 Propetamphos; tolerances for Soybean, seed ...... 0 .05 residues. (b) Section 18 emergency exemptions. (a) General. A tolerance of 0.1 part per [Reserved] million is established for residues of (c) Tolerances with regional registra- the insecticide propetamphos, includ- tions. [Reserved] ing its metabolites and degradates, in (d) Indirect or inadvertent residues. or on food or feed commodities when [Reserved] present therein as a result of the treat- ment of food- or feed-handling estab- [63 FR 50784, Sept. 23, 1998, as amended at 73 lishments with propetamphos. Direct FR 75608, Dec. 12, 2008; 76 FR 76314, Dec. 7, application shall be limited solely to 2011] spot and/or crack and crevice treat- § 180.539 d-Limonene; tolerances for ment in food- or feed-handling estab- residues. lishments where food or feed and food or feed products are held, processed, (a) General. (1) The insecticide d-lim- prepared, served, or sold. Spray and onene may be safely used in insect-re- dust concentrations shall be limited to pellent tablecloths and in insect-repel- lent strips used in food- or feed-han- a maximum of 1 percent active ingre- dling establishments. dient. For crack and crevice treatment, equipment capable of delivering a dust (2) To assure safe use of the insect re- or a pin-stream of spray directly into pellent, its label and labeling shall con- cracks and crevices shall be used. For form to that registered by the U.S. En- spot treatment, a coarse, low-pressure vironmental Protection Agency, and it spray shall be used to avoid contamina- shall be used in accordance with such tion of food, feed, or food-contact/feed- label and labeling. contact surfaces. Compliance with the (b) Section 18 emergency exemptions. tolerance level specified in this para- [Reserved] graph is to be determined by measuring (c) Tolerances with regional registra- only propetamphos, 1-methylethyl- tions. [Reserved] (2E)-3- (d) Indirect or inadvertent residues. ((ethylamino)methoxyphosphinothioyl) [Reserved] oxy)-2-butenoate, in or on the com- [65 FR 33715, May 24, 2000, as amended at 70 modity. FR 55268, Sept. 21, 2005] (b) Section 18 emergency exemptions. [Reserved] § 180.540 Fenitrothion; tolerances for (c) Tolerances with regional registra- residues. tions. [Reserved] (a) General. Tolerances are estab- (d) Indirect or inadvertent residues. lished for residues of the insecticide [Reserved] fenitrothion, O,O-dimethyl O-(4-nitro- m-tolyl) phosphorothioate, from the [65 FR 33716, May 24, 2000, as amended at 76 postharvest application of the insecti- FR 23498, Apr. 27, 2011] cide to stored wheat in Australia, in or § 180.543 Diclosulam; tolerances for on the following food commodity: residues.

Commodity Parts per (a) General. Tolerances are estab- million lished for residues of the herbicide Wheat, gluten 1 ...... 3.0 diclosulam [N-(2,6-dichlorophenyl)-5- 1 There are no U.S. registrations on food commodities since ethoxy-7-fluoro[1,2,4] triazolo[1,5- 1987. c]pyrimidine-2-sulfonamide] in or on

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the following raw agricultural com- Commodity Parts per modities as follows: million Custard apple ...... 0 .60 Parts per Commodity million Date ...... 8 .0 Feijoa ...... 0 .4 Peanut ...... 0 .020 Fruit, citrus, group 10–10 ...... 3 .0 Soybean, seed ...... 0 .020 Fruit, pome, group 11–10 ...... 2 .0 Fruit, small, vine climbing, except fuzzy kiwifruit, subgroup 13–07F ...... 1 .0 (b) Section 18 emergency exemptions. Fruit, stone, group 12, except plum, prune, [Reserved] fresh ...... 3 .0 (c) Tolerances with regional registra- Goat, fat ...... 0 .50 Goat, meat ...... 0.02 tions. [Reserved] Grain, aspirated grain fractions ...... 120 (d) Indirect or inadvertent residues. Grape, raisin ...... 1 .5 [Reserved] Grass, forage, fodder and hay, group 17, for- age ...... 18 .0 [65 FR 12134, Mar. 8, 2000] Grass, forage, fodder and hay, group 17, hay .. 30 .0 Guava ...... 0 .4 § 180.544 Methoxyfenozide; tolerances Herb subgroup 19A, except chive ...... 400 Hog, fat ...... 0 .1 for residues. Hog, meat ...... 0 .02 (a) General. (1) Tolerances are estab- Horse, fat ...... 0 .50 Horse, meat ...... 0 .02 lished for residues of the insecticide Ilama ...... 0 .60 methoxyfenozide, including its metabo- Jaboticaba ...... 0 .4 lites and degradates, in or on the com- Leaf petioles subgroup 4B ...... 25 modities listed in the following table. Leafy greens subgroup 4A ...... 30 Longan ...... 2 .0 Compliance with the tolerance levels Lychee ...... 2 .0 specified in the following table is to be Mango ...... 0.6 determined by measuring only Milk ...... 0.10 Nut, tree, group 14 ...... 0 .10 methoxyfenozide (3-methoxy-2- Onion, green, subgroup 3-07B ...... 5 .0 methylbenzoic acid 2-(3,5- Papaya ...... 0 .6 dimethylbenzoyl)-2-(1,1-dimethylethyl) Passionfruit ...... 0 .4 hydrazide) in or on the commodity. Pea and bean, dried shelled, except soybean, subgroup 6C, except pea, blackeyed, seed and pea, southern, seed ...... 0.50 Parts per Commodity million Pea and bean, succulent shelled, subgroup 6B 0 .2 Pea, blackeyed, seed ...... 4 .0 Acerola ...... 0.4 Pea, southern, seed ...... 4.0 Almond, hulls ...... 25 Peanut ...... 0 .02 Animal feed, nongrass, group 18, forage ...... 50 .0 Peanut, hay ...... 55.0 Animal feed, nongrass, group 18, hay ...... 150.0 Peanut, oil ...... 0 .04 Apple, wet pomace ...... 7 .0 Peppermint, tops ...... 7 .0 Artichoke, globe ...... 3.0 Pineapple ...... 0.70 Atemoya ...... 0 .60 Pistachio ...... 0.10 Avocado ...... 0 .6 Plum, prune, fresh ...... 0.30 Beet, sugar, roots ...... 0 .50 Pomegranate ...... 0 .6 Berry, low growing, subgroup 13–07G, except Poultry, fat ...... 0.02 cranberry ...... 2.0 Poultry, meat ...... 0 .02 Biriba ...... 0 .60 Pulasan ...... 2 .0 Brassica, head and stem, subgroup 5A ...... 7 .0 Rambutan ...... 2 .0 Brassica, leafy greens, subgroup 5B ...... 30 Sapodilla ...... 0 .6 Bushberry subgroup 13-07B ...... 3 .0 Sapote, black ...... 0 .6 Caneberry subgroup 13–07A ...... 6.0 Sapote, mamey ...... 0 .6 Canistel ...... 0 .6 Sheep, fat ...... 0 .50 Cattle, fat ...... 0.50 Sheep, meat ...... 0.02 Cattle, meat ...... 0 .02 Sorghum, grain, forage ...... 15 Cherimoya ...... 0 .60 Sorghum, grain, grain ...... 6 .0 Citrus, oil ...... 100 Sorghum, grain, stover ...... 20 Corn, field, forage ...... 15 Sorghum, sweet, forage ...... 15 Corn, field, grain ...... 0 .05 Sorghum, sweet, grain ...... 6 .0 Corn, field, refined oil ...... 0 .20 Sorghum, sweet, stalk ...... 15 Corn, field, stover ...... 125 Sorghum, sweet, stover ...... 20 Corn, pop, grain ...... 0.05 Soursop ...... 0 .60 Corn, pop, stover ...... 125 Soybean, aspirated grain fractions ...... 160 Corn, sweet, forage ...... 30 Soybean, forage ...... 30 Corn, sweet, kernel plus cob with husks re- Soybean, hay ...... 80 moved ...... 0 .05 Soybean, hulls ...... 2 .0 Corn, sweet, stover ...... 60 Soybean, seed ...... 1 .0 Cotton, gin byproducts ...... 35 Spanish lime ...... 2 .0 Cotton, undelinted seed ...... 2 .0 Spearmint, tops ...... 7 .0 Cranberry ...... 0 .5 Star apple ...... 0 .6

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methoxyfenozide to growing crops as Commodity Parts per million listed in paragraph (a) of this section. Starfruit ...... 0 .4 Compliance with the tolerance levels Sugar apple ...... 0 .60 specified in the following table is to be Turnip, greens ...... 30 Vegetable, cucurbit, group 9 ...... 0.3 determined by measuring only Vegetable, foliage of legume, except soybean, methoxyfenozide [3-methoxy-2- subgroup 7A ...... 35 methylbenzoic acid 2-(3,5- Vegetable, fruiting, group 8–10 ...... 2 .0 Vegetable, leaves of root and tuber, group 2 ... 30 dimethylbenzoyl)-2-(1,1-dimethylethyl) Vegetable, legume, edible podded, subgroup hydrazide]. 6A ...... 1 .5 Vegetable, root, except sugar beet, Subgroup Commodity Parts per 1B ...... 0 .90 million Vegetable, tuberous and corm, except potato, subgroup 1D ...... 0 .02 Onion, bulb, subgroup 3–07A ...... 0 .10 Wax jambu ...... 0 .4 Potato ...... 0 .02

(2) Tolerances are established for res- (2) Tolerances are established for the idues of the insecticide indirect or inadvertent residues of the methoxyfenozide, including its metabo- insecticide methoxyfenozide, including lites and degradates, in or on the com- its metabolites and degradates, in or modities in the following table. Com- on the raw agricultural commodities in pliance with the tolerance levels speci- the following table, when present fied in the following table is to be de- therein as a result of the application of termined by measuring only the sum of methoxyfenozide to growing crops as methoxyfenozide [3-methoxy-2- listed in paragraph (a) of this section. methylbenzoic acid 2-(3,5- Compliance with the tolerance levels dimethylbenzoyl)-2-(1,1-dimethylethyl) hydrazide] and its glucuronide metabo- specified in the following table is to be lite (b-D-Glucopyranuronic acid, 3-[[2- determined by measuring only the sum (1,1-dimethylethyl)-2-(3,5- of methoxyfenozide [3-methoxy-2- dimethylbenzoyl)-hydrazino]carbonyl]- methylbenzoic acid, 2-(3,5- 2-methylphenyl-), calculated as the dimethylbenzoyl)-2-(1,1-dimethylethyl) stoichiometric equivalent of hydrazide] and the following metabo- methoxyfenozide. lites (all calculated as the stoichio- metric equivalent of methoxyfenozide): Parts per Commodity million free phenol of methoxyfenozide [3,5- dimethylbenzoic acid N-tert-butyl-N′- Cattle, liver ...... 0 .40 (3-hydroxy-2-methylbenzoyl) hydra- Cattle, meat byproducts, except liver ...... 0 .10 Egg ...... 0 .02 zide], the glucose conjugate of the phe- Goat, liver ...... 0.40 nol [3,5-dimethyl benzoic acid N-tert- Goat, meat byproducts, except liver ...... 0 .10 butyl-N′-[3 (b-D-glucopyranosyloxy)-2- Hog, liver ...... 0 .1 Hog, meat byproducts, except liver ...... 0 .02 methylbenzoyl]-hydrazide] and the Horse, liver ...... 0 .40 malonylglycosyl conjugate of the phe- Horse, meat byproducts, except liver ...... 0 .10 nol [3,5-dimethyl benzoic acid N-tert- Poultry, liver ...... 0 .10 Poultry, meat byproducts, except liver ...... 0 .02 butyl-N′-[3 (b-D-6-malonyl- Sheep, liver ...... 0.40 glucopyranosyl-1-oxy)-2- Sheep, meat byproducts, except liver ...... 0 .10 methylbenzoyl]-hydrazide].

(b) Section 18 emergency exemptions. Parts per [Reserved] Commodity million (c) Tolerances with regional registra- Animal feed, nongrass, group 18, straw ...... 8.0 tions. [Reserved] Chive ...... 4 .5 (d) Indirect or inadvertent tolerances. Grain, cereal, forage, fodder and straw group (1) Tolerances are established for the 16, except corn ...... 6 .0 indirect or inadvertent residues of the Rapeseed subgroup 20A ...... 1 .0 insecticide methoxyfenozide, including Spice subgroup 19B ...... 4 .5 its metabolites and degradates, in or Sunflower subgroup 20B ...... 1.0 on the raw agricultural commodities in the following table, when present therein as a result of the application of

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[67 FR 59203, Sept. 20, 2002, as amended at 68 Parts per FR 32389, May 30, 2003; 68 FR 37765, June 25, Commodity million 2003; 69 FR 58097, Sept. 29, 2004; 70 FR 7047, Feb. 10, 2005; 70 FR 51604, Aug. 31, 2005; 70 FR Onion, green, subgroup 3–07B ...... 10 75739, Dec. 21, 2005; 71 FR 32853, June 7, 2006; Papaya ...... 0 .40 73 FR 11826, Mar. 5, 2008; 74 FR 22468, May 13, Sapodilla ...... 0 .40 2009; 74 FR 45335, Sept. 2, 2009; 76 FR 34886, Sapote, black ...... 0 .40 June 15, 2011; 77 FR 40812, July 11, 2012; 78 FR Sapote, mamey ...... 0 .40 Spinach ...... 10 60714, Oct. 2, 2013; 79 FR 51106, Aug. 27, 2014] Star apple ...... 0 .40 Starfruit ...... 0 .20 § 180.545 Prallethrin; tolerances for Sugar apple ...... 0 .20 residues. (a) General. Tolerances are estab- (b) Section 18 emergency exemptions. lished for residues of the insecticide [Reserved] prallethrin, including its metabolites (c) Tolerances with regional registra- and degradates, in or on all raw agri- tions. [Reserved] cultural commodities and processed (d) Indirect or inadvertant residues. food from use of prallethrin in food [Reserved] handling establishments where food and food products are held, processed, [65 FR 57556, Sept. 25, 2000, as amended at 66 prepared and/or served, or as a wide- FR 48003, Sept. 17, 2001; 67 FR 35050, May 17, area mosquito adulticide at 1.0 part per 2002; 76 FR 4548, Jan. 26, 2011] million (ppm). Compliance with the tolerance level specified is to be deter- § 180.547 Prohexadione calcium; toler- ances for residues. mined by measuring only prallethrin, 2-methyl-4-oxo-3-(2-propyn-1-yl)-2- (a) General. Tolerances are estab- cyclopenten-1-yl-2,2-dimethyl-3-(2- lished for residues of the growth regu- methyl-1-propen-1- lator, prohexadione calcium, including yl)cyclopropanecarboxylate. its metabolites and degradates, in or (b) Section 18 emergency exemptions. on the commodities in the table below. [Reserved] Compliance with the tolerance levels (c) Tolerances with regional registra- specified below is to be determined by tions. [Reserved] measuring only prohexadione calcium (d) Indirect or inadvertent residues. (calcium 3-oxido-5-oxo-4- [Reserved] propionylcyclohex-3-enecarboxylate)’’ in or on the following commodities. [79 FR 64330, Oct. 29, 2014] Parts per § 180.546 Mefenoxam; tolerances for Commodity million residues. (a) General. Tolerances are estab- Cattle, kidney ...... 0 .10 Cattle, meat byproducts, except kidney ...... 0.05 lished for residues of mefenoxam, in- Cherry, sweet ...... 0 .40 cluding its metabolites and degradates, Fruit, pome, group 11 ...... 3.0 in or on the commodities in the table Goat, kidney ...... 0 .10 below. Compliance with the tolerance Goat, meat byproducts, except kidney ...... 0 .05 levels specified below is to be deter- Grass, forage 1 ...... 0 .10 1 mined by measuring only metalaxyl Grass, hay ...... 0 .10 Grass, seed screenings 1 ...... 3 .5 (methyl N-(2,6-dimethylphenyl)-N- Grass, straw 1 ...... 1 .2 (methoxyacetyl)-DL-alaninate). Hog, kidney ...... 0.10 Hog, meat byproducts, except kidney ...... 0 .05 Parts per Horse, kidney ...... 0 .10 Commodity million Horse, meat byproducts, except kidney ...... 0 .05 Artichoke, globe ...... 0.05 Peanut ...... 1 .0 Atemoya ...... 0 .20 Peanut, hay ...... 0.60 Bean, snap, succulent ...... 0 .20 Sheep, kidney ...... 0.10 Bushberry subgroup 13–07B ...... 2 .0 Sheep, meat byproducts, except kidney ...... 0 .05 Caneberry subgroup 13–07A ...... 0.70 Canistel ...... 0 .40 1Registration is limited to grass grown for seed. Custard apple ...... 0 .20 Herbs, dried ...... 55 (b) Section 18 emergency exemptions. Herbs, fresh ...... 8 .0 [Reserved] Kiwifruit ...... 0.10 Mango ...... 0.40 (c) Tolerances with regional registra- Onion, bulb, subgroup 3–07A ...... 3 .0 tions. [Reserved]

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(d) Indirect or inadvertent residues. (b) Section 18 emergency exemptions. [Reserved] [Reserved] (c) Tolerances with regional registra- [65 FR 25660, May 3, 2000, as amended at 66 FR 29712, June 1, 2001; 76 FR 71464, Nov. 18, tions. [Reserved] 2011] (d) Indirect or inadvertent residues. [Reserved] § 180.548 Tralkoxydim; tolerances for residues. [64 FR 4308, Jan. 28, 1999, as amended at 67 FR 55338, Aug. 29, 2002; 76 FR 34886, June 15, (a) General. Tolerances are estab- 2011] lished for residues of the herbicide, tralkoxydim, 2-Cyclohexen-1-one, 2-[1- § 180.551 Fluthiacet-methyl; tolerances (ethoxyimino)propyl]-3-hydroxy-5- for residues. (2,4,6-trimethylphenyl)-(9Cl) in or on (a) General. (1) A tolerance is estab- the raw agricultural commodities: lished for residues of the herbicide, fluthiacet-methyl, acetic acid [[2- Parts per Commodity million chloro-4-fluoro-5-[(tetrahydro-3-oxo- 1H,3H-[1,3,4]thiadiazolo[3,4-a]pyridazin- Barley, grain ...... 0 .02 1-ylidene)amino]phenyl]thio]-methyl Barley, hay ...... 0 .02 Barley, straw ...... 0 .05 ester, in or on the food commodity: Wheat, forage ...... 0 .05 Wheat, grain ...... 0 .02 Parts per Commodity million Wheat, hay ...... 0 .02 Wheat, straw ...... 0 .05 Corn, field, forage ...... 0 .050 Corn, field, grain ...... 0 .010 (b) Section 18 emergency exemptions. Corn, field, stover ...... 0 .050 [Reserved] Corn, pop, grain ...... 0.010 (c) Tolerances with regional registra- Corn, pop, stover ...... 0.050 Corn, sweet, forage ...... 0 .050 tions. [Reserved] Corn, sweet, kernel plus cob with husks re- (d) Indirect or inadvertent residues. moved ...... 0 .010 [Reserved] Corn, sweet, stover ...... 0 .050 Soybean, seed ...... 0 .01 [63 FR 69199, Dec. 16, 1998, as amended at 68 FR 48302, Aug. 13, 2003; 70 FR 70739, Nov. 23, (2) A tolerance is established for the 2005] combined residues of the herbicide fluthiacet-methyland its acid metabo- § 180.549 Diflufenzopyr; tolerances for residues. lite: acetic acid, [[2-chloro-4-fluoro-5- [tetrahydro-3-oxo-1H,3H- (a) General. Tolerances are estab- [1,3,4]thiadiazolo[3,4-a]pyridazin-1- lished for combined residues of ylidene)amino]phenyl]thio]-methyl diflufenzopyr, 2-(1-[([3,5- ester, and its acid metabolite, acetic difluorophenylamino] car- acid, [[2-chloro-4-fluoro-5-[(tetrahydro- bonyl)hydrazono]ethyl)-3- 3-oxo-1H,3H-[1,3,4]thiadiazolo[3,4- pyridinecarboxylic acid, and its me- a]pyridazin-1- tabolites convertible to 8- ylidene)amino]phenyl]thio]- , in or on methylpyrido[2,3-d]pyridazin-5(6H)-one, the following food commodities: expressed as diflufenzopyr, in or on the following raw agricultural commod- Commodity Parts per ities: million Cotton, gin byproducts ...... 0 .20 Parts per Cotton, undelinted seed ...... 0 .020 Commodity million

Corn, field, forage ...... 0 .05 (b) Section 18 emergency exemptions. Corn, field, grain ...... 0 .05 [Reserved] Corn, field, stover ...... 0 .05 Corn, pop, grain ...... 0.05 (c) Tolerances with regional registra- Corn, pop, stover ...... 0.05 tions. [Reserved] Corn, sweet, forage ...... 0 .05 (d) Indirect or inadvertent residues. Corn, sweet, kernel plus cob with husks re- [Reserved] moved ...... 0 .05 Corn, sweet, stover ...... 0 .05 [64 FR 18357, Apr. 14, 1999, as amended at 66 Grass, forage ...... 22 .0 FR 65850, Dec. 21, 2001; 71 FR 77625, Dec. 27, Grass, hay ...... 7 .0 2006]

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§ 180.552 Sulfosulfuron; tolerances for Commodity Parts per residues. million (a) General. Tolerances are estab- Cilantro, leaves ...... 30.0 lished for residues of the herbicide Cucumber ...... 2 .0 Fruit, stone, group 12, except plum, prune, sulfosulfuron, 1–(4,6- fresh, postharvest ...... 10.0 dimethoxypyrimidin-2-yl)-3-[(2- Ginseng ...... 0 .3 ethanesulfonyl-imidazo[1,2-a]pyridine- Grape ...... 4 .0 3-yl) sulfonyl]urea and its metabolites Grape, raisin ...... 6 .0 Juneberry ...... 5 .0 converted to 2-(ethylsulfonyl)- Kiwifruit, postharvest ...... 15 .0 imidazo[1,2-a]pyridine and calculated Leafy greens subgroup 4A, except spinach ...... 30 .0 as sulfosulfuron in or on the raw agri- Lingonberry ...... 5.0 cultural commodities. Pear ...... 10 Pepper, nonbell ...... 0 .02 Pistachio ...... 0.02 Parts per Commodity million Plum, prune, dried ...... 2.5 Plum, prune, fresh ...... 1.5 Cattle, fat ...... 0.02 Pomegranate ...... 2 .0 Cattle, meat ...... 0 .01 Salal ...... 5 .0 Cattle, meat byproducts ...... 0.3 Strawberry ...... 3 .0 Goat, fat ...... 0 .02 Vegetable, fruiting, group 8, except nonbell Goat, meat ...... 0.01 pepper ...... 2 .0 Goat, meat byproducts ...... 0 .3 Grass, forage, fodder and hay, group 17, for- (b) Section 18 emergency exemptions. age ...... 14 Grass, forage, fodder and hay, group 17, hay .. 25 [Reserved] Hog, fat ...... 0 .005 (c) Tolerances with regional registra- Hog, meat ...... 0 .005 tions. [Reserved] Hog, meat byproducts ...... 0 .05 Horse, fat ...... 0 .02 (d) Indirect or inadvertent residues. Horse, meat ...... 0 .01 [Reserved] Horse, meat byproducts ...... 0 .3 Milk ...... 0.02 [64 FR 28924, May 28, 1999, as amended at 65 Sheep, fat ...... 0 .02 FR 19849, Apr. 13, 2000; 65 FR 69883, Nov. 21, Sheep, meat ...... 0.01 2000; 67 FR 19120, Apr. 18, 2002; 68 FR 2247, Sheep, meat byproducts ...... 0 .3 Jan. 16, 2003; 68 FR 55519, Sept. 26, 2003; 71 FR Wheat, forage ...... 4 .0 15617, Mar. 29, 2006; 71 FR 43664, Aug. 2, 2006; Wheat, grain ...... 0 .02 Wheat, hay ...... 0 .3 73 FR 19154, Apr. 9, 2008] Wheat, straw ...... 0 .1 § 180.554 Kresoxim-methyl; tolerances (b) Section 18 emergency exemptions. for residues. [Reserved] (a) General. (1) Tolerances are estab- (c) Tolerances with regional registra- lished for the combined residues of the tions. [Reserved] fungicide kresoxim-methyl (methyl (d) Indirect or inadvertent residues. (E)-2-[2-(2-methylphenoxy)-meth- [Reserved] yl]phenyl-2-(methoxyimido)acetate) [64 FR 27192, May 19, 1999, as amended at 70 and its metabolites as follows: (E)-2-[2- FR 69464, Nov. 16, 2005; 72 FR 54574, Sept. 26, (2-methylphenoxy)methyl]-phenyl-2- 2007] (methoxyimido)acetic acid; (E)-2-[2-(2- hydroxymethylphenoxy)methyl]- § 180.553 Fenhexamid; tolerances for phenyl-2-(methoxyimido)acetic acid residues. (free and glucose conjugated); and (E)- (a) General. Tolerances are estab- 2-[2-(4-hydroxy-2-methylphenoxy)- lished for the residues of the fungicide methyl]phenyl-2-(methoxyimido)acetic fenhexamid (N-2,3-dichloro-4- acid (free and glucose conjugated) in or hydroxyphenyl)-1-methyl on the following commodities: cyclohexanecarboxamide) in or on the Parts per following commodities: Commodity million

Commodity Parts per Apple, dry pomace ...... 1.0 million Apple, wet pomace ...... 1 .0 Fruit, pome ...... 0.5 Almond, hulls ...... 2 .0 Grape ...... 1 .0 Almond ...... 0.02 Grape, raisin ...... 1 .5 Asparagus ...... 0.02 Pecan ...... 0 .15 Bushberry subgroup 13B ...... 5 .0 Vegetable, cucurbit, group 9 ...... 0.40 Caneberry subgroup 13A ...... 20 .0

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(2) Tolerances are established in or Commodity Parts per on the following commodities for the million residues of the metabolite (E)-2-[2-(2- Canistel ...... 0 .7 methylphenoxy)methyl]-phenyl-2- Cattle, fat ...... 0.1 (methoxyimido)acetic acid resulting Cattle, meat ...... 0 .1 Cattle, meat byproducts ...... 0.1 from the use of the fungicide kresoxim- Citrus, dried pulp ...... 1 .0 methyl: Citrus, oil ...... 38 Coffee, green bean 2 ...... 0 .02 Corn, field, forage ...... 6 .0 Commodity Parts per million Corn, field, grain ...... 0 .05 Corn, field, stover ...... 7 Cattle, meat byproducts ...... 0.01 Corn, field, refined oil ...... 0 .1 Goat, meat byproducts ...... 0 .01 Corn, pop, grain ...... 0.05 Sheep, meat byproducts ...... 0 .01 Corn, pop, stover ...... 7 Corn, sweet, cannery waste ...... 0 .6 (b) Section 18 emergency exemptions. Corn, sweet, forage ...... 7 .0 Corn, sweet, kernel plus cob with husks re- [Reserved] moved ...... 0 .04 (c) Tolerances with regional registra- Corn, sweet, stover ...... 4 .0 tions. [Reserved] Egg ...... 0 .04 (d) Indirect or inadvertent residues. Fruit, citrus, group 10 ...... 0 .6 Fruit, pome ...... 0.5 [Reserved] Fruit, stone, group 12 ...... 2 [64 FR 31136, June 10, 1999, as amended at 71 Goat, fat ...... 0 .1 Goat, meat ...... 0.1 FR 50359, Aug. 25, 2006; 74 FR 46377, Sept. 9, Goat, meat byproducts ...... 0 .1 2009] Grain, aspirated fractions ...... 5 .0 Grape ...... 2 .0 § 180.555 Trifloxystrobin; tolerances Grape, raisin ...... 5 .0 for residues. Grass, forage ...... 12 Grass, hay ...... 17 (a) General. Tolerances are estab- Hog, fat ...... 0 .05 lished for residues of trifloxystrobin, Hog, meat ...... 0 .05 including its metabolites and Hog, meat byproducts ...... 0 .05 Hop, dried cones ...... 11 .0 degradates, in or on the commodities Horse, fat ...... 0 .1 in the table below. Compliance with Horse, meat ...... 0 .1 the tolerance levels specified below is Horse, meat byproducts ...... 0 .1 Leaf petioles subgroup 4B ...... 3 .5 to be determined by measuring only Mango ...... 0.7 the sum of trifloxystrobin, Milk ...... 0.02 benzeneacetic acid, (E,E)-a- Nut, tree, group 14 ...... 0 .04 (methoxyimino)-2-[[[[1-[3- Oat, forage ...... 0 .3 Oat, grain ...... 0 .05 (trifluoromethyl) phenyl]ethylidene] Oat, hay ...... 0.3 amino]oxy]methyl]-, methyl ester, and Oat, straw ...... 5.0 the free form of its acid metabolite Papaya ...... 0 .7 Pea, dry, seed ...... 0 .06 CGA–321113, (E,E)-methoxyimino-[2-[1- Pea, field, hay ...... 15 (3-trifluoromethyl-phenyl)- Pea, field, vines ...... 4 ethylideneaminooxymethyl]- Peanut, hay ...... 4.0 phenyl]acetic acid, calculated as the Peanut ...... 0 .05 Pistachio ...... 0.04 stoichiometric equivalent of Potato ...... 0 .04 trifloxystrobin, in or on the com- Poultry, fat ...... 0.04 modity. Poultry, meat ...... 0 .04 Poultry, meat byproducts ...... 0.04 Parts per Radish, tops ...... 10 Commodity million Rice, grain ...... 3 .5 Rice, hulls ...... 8 Alfalfa, forage ...... 0.01 Rice, straw ...... 7 .5 Alfalfa, hay ...... 0.01 Sapodilla ...... 0 .7 Almond, hulls ...... 9 .0 Sapote, black ...... 0 .7 Apple, wet pomace ...... 5 .0 Sapote, mamey ...... 0 .7 Artichoke, globe ...... 1.0 Sheep, fat ...... 0 .1 Asparagus ...... 0.07 Sheep, meat ...... 0.1 Banana 1 ...... 0.10 Sheep, meat byproducts ...... 0 .1 Barley, grain ...... 0 .05 Soybean, forage ...... 10 .0 Barley, hay ...... 0 .3 Soybean, hay ...... 25 .0 Barley, straw ...... 5 .0 Soybean, seed ...... 0 .08 Beet, sugar, dried pulp ...... 0 .4 Star apple ...... 0 .7 Beet, sugar, molasses ...... 0 .2 Strawberry ...... 1 .1 Beet, sugar, roots ...... 0 .1 Vegetable, cucurbit, group 9 ...... 0.50 Beet, sugar, tops ...... 4.0 Vegetable, fruiting ...... 0.5

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(d) Indirect or inadvertent residues. Commodity Parts per million [Reserved] Vegetable, root, except sugar beet, subgroup [65 FR 48634, Aug. 9, 2000, as amended at 66 1B ...... 0 .1 FR 14846, Mar. 14, 2001; 66 FR 66794, Dec. 27, Wheat, bran ...... 0.15 2001; 70 FR 7047, Feb. 10, 2005; 70 FR 43298, Wheat, forage ...... 0 .3 July 27, 2005] Wheat, grain ...... 0 .05 Wheat, hay ...... 0 .2 § 180.557 Tetraconazole; tolerances for Wheat, straw ...... 5 .0 residues. 1 There are no U.S. registrations as of September 27, 1999 for use on banana. (a) General. Tolerances are estab- 2 There are no U.S. registrations as of January 18, 2012 for lished for residues of tetraconazole, in- use on coffee, green bean. cluding its metabolites and degradates, (b) Section 18 emergency exemptions. in or on the commodities listed below. [Reserved] Compliance with the following toler- (c) Tolerances with regional registra- ance levels is to be determined by measuring only tetraconazole (1-[2-(2,4- tions. [Reserved] dichlorophenyl)-3-(1,1,2,2- (d) Indirect or inadvertent residues. tetrafluoroethoxy)propyl]-1H-1,2,4-tri- [Reserved] azole), in or on the following commod- [64 FR 51907, Sept. 27, 1999] ities.

EDITORIAL NOTE: For FEDERAL REGISTER ci- Commodity Parts per tations affecting § 180.555, see the List of CFR million Sections Affected, which appears in the Aspirated grain fractions ...... 1 .0 Finding Aids section of the printed volume Beet sugar, dried pulp ...... 0 .15 and at www.fdsys.gov. Beet sugar, molasses ...... 0 .15 Beet sugar, root ...... 0 .05 Cattle, fat ...... 0.15 § 180.556 Pymetrozine; tolerances for Cattle, liver ...... 1 .50 residues. Cattle, meat ...... 0 .01 Cattle, meat byproducts (except liver) ...... 0 .15 (a) General. Tolerances are estab- Corn, field, forage ...... 1 .1 lished for residues of the insecticide Corn, field, grain ...... 0 .01 pymetrozine 1,2,4-triazin-3(2H)-one,4,5- Corn, field, stover ...... 1 .7 Corn, pop, grain ...... 0.01 dihydro-6-methyl-4-[(3- Corn, pop, stover ...... 1.7 pyridinylmethylene) amino] in or on Eggs ...... 0 .02 Goat, fat ...... 0 .15 the following raw agricultural com- Goat, liver ...... 1.50 modities. The tolerance level for each Goat, meat ...... 0.01 commodity is expressed in terms of the Goat, meat byproducts (except liver) ...... 0.15 Hog, fat ...... 0 .01 parent insecticide only, which serves as Hog, liver ...... 0 .05 an indicator of the use of pymetrozine Hog, meat ...... 0 .01 Hog, meat byproducts (except liver) ...... 0 .01 on these raw agricultural commodities. Horse, fat ...... 0 .15 Horse, liver ...... 1 .50 Commodity Parts per Horse, meat ...... 0 .01 million Horse, meat byproducts (except liver) ...... 0 .15 Low growing berry subgroup 13–07G, except Asparagus ...... 0.04 cranberry ...... 0 .25 Brassica, head and stem, subgroup 5A ...... 0 .5 Milk ...... 0.03 Brassica, leafy greens, subgroup 5B ...... 0 .25 Milk, fat ...... 0 .75 Cotton, gin byproducts ...... 2 .0 Peanut ...... 0 .03 Cotton, undelinted seed ...... 0 .3 Peanut, oil ...... 0 .10 Pecan ...... 0 .04 Hop, dried cones ...... 6 .0 Poultry, fat ...... 0.05 Pecan ...... 0 .02 Poultry, meat ...... 0 .01 Turnip, greens ...... 0.25 Poultry meat byproducts ...... 0 .05 Vegetable, fruiting, group 8 ...... 0.2 Sheep, fat ...... 0 .15 Vegetable, cucurbit, group 9 ...... 0.1 Sheep, liver ...... 1.50 Vegetable, leafy, execpt brassica, group 4 ...... 0 .6 Sheep, meat ...... 0.01 Vegetable, tuberous and corm, subgroup 1C ... 0.02 Sheep, meat byproducts (except liver) ...... 0.15 Small fruit vine climbing, except fuzzy kiwifruit, subgroup 13–07F ...... 0.20 (b) Section 18 emergency exemptions. Soybean, refined oil ...... 0 .80 [Reserved] Soybean, seed ...... 0 .15 (c) Tolerances with regional registra- (b) Section 18 emergency exemptions. tions. [Reserved] [Reserved]

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(c) Tolerances with regional registra- Commodity Parts per tions. [Reserved] million (d) Indirect or inadvertent residues. Barley, grain ...... 0 .1 [Reserved] Barley, hay ...... 0 .1 Barley, straw ...... 0 .1 [70 FR 20830, Apr. 22, 2005, as amended at 70 Wheat, forage ...... 0 .2 FR 31359, June 1, 2005; 72 FR 18134, Apr. 11, Wheat, grain ...... 0 .1 2007; 73 FR 67406, Nov. 14, 2008; 76 FR 53648, Wheat, hay ...... 0 .5 Wheat, straw ...... 0 .1 Aug. 29, 2011] (b) Section 18 emergency exemptions. § 180.559 Clodinafop-propargyl; toler- ances for residues. [Reserved] (c) Tolerances with regional registra- (a) General. Tolerances are estab- tions. [Reserved] lished for clodinafop-propargyl, includ- (d) Indirect or inadvertent residues. ing its metabolites and degradates, in [Reserved] or on the commodities in the following table. Compliance with the tolerance [65 FR 38764, June 22, 2000, as amended at 70 levels specified in the following table is FR 74688, Dec. 16, 2005; 73 FR 11820, Mar. 5, 2008; 75 FR 16020, Mar. 31, 2010; 76 FR 38035, to be determined by measuring only June 29, 2011] clodinafop-propargyl [(2R)-2-[4-[(5- chloro-3-fluoro-2- § 180.561 Acibenzolar-S-methyl; toler- pyridinyl)oxy]phenoxy]propanoic acid, ances for residues. 2-propynyl ester] and its metabolite (a) General. (1) Tolerances are estab- clodinafop [(2R)-2-[4-[(5-chloro-3-fluoro- lished for residues of acibenzolar-S- 2- pyridinyl)oxy]phenoxy]propanoic methyl, benzo(1,2,3)thiadiazole-7- acid]. carbothioic acid-S-methyl ester, in- cluding its metabolites and degradates, Parts per Commodity million in or on the commodities in the table below. Compliance with the tolerance Wheat, forage ...... 0 .1 Wheat, grain ...... 0 .02 levels specified below is to be deter- Wheat, hay ...... 0 .1 mined by measuring only those Wheat, straw ...... 0 .5 acibenzolar-S-methyl residues convert- ible to benzo(1,2,3)thiadiazole-7-car- (b) Section 18 emergency exemptions. boxylic acid (CGA–210007), expressed as [Reserved] the stoichiometric equivalent of (c) Tolerances with regional registra- acibenzolar-S-methyl, in or on the fol- tions. [Reserved] lowing raw agricultural commodities. (d) Indirect or inadvertent residues. Parts per [Reserved] Commodity million

[65 FR 38774, June 22, 2000, as amended at 77 Banana 1 ...... 0.1 FR 72226, Dec. 5, 2012] Berry, low growing, subgroup 13–07G ...... 0 .15 Onion, bulb, subgroup 3–07A ...... 0 .1 § 180.560 Cloquintocet-mexyl; toler- Spinach ...... 1 .0 ances for residues. Tomato, paste ...... 3 .0 Vegetable, brassica, leafy, group 5 ...... 1.0 (a) General. Tolerances are estab- Vegetable, cucurbit, group 9 ...... 2.0 Vegetable, fruiting, group 8 ...... 1.0 lished for the combined residues of Vegetable, leafy, group 4 ...... 0 .25 cloquintocet-mexyl, (acetic acid [(5- 1 chloro-8-quinolinyl)oxy]-,1- There are no United States registrations for banana. methylhexyl ester; CAS Reg. No. 99607– (2) Tolerances are established for res- 70–2) and its acid metabolite (5-chloro- idues of acibenzolar- S -methyl, 8-quinolinoxyacetic acid), when used as benzo(1,2,3)thiadiazole-7-carbothioic an inert ingredient (safener) in pes- acid- S -methyl ester, including its me- ticide formulations containing the ac- tabolites and degradates, in or on the tive ingredients clodinafop-propargyl commodities in the table below. Com- (wheat only), dicamba (wheat only), pliance with the tolerance levels speci- flucarbazone-sodium (wheat only), fied below is to be determined by meas- pinoxaden (wheat or barley), or uring only those acibenzolar- S -methyl pyroxsulum (wheat only) in or on the residues convertible to following food commodities: benzo(1,2,3)thiadiazole-7-carboxylic

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acid (CGA–210007), expressed as the (c) Tolerances with regional registra- Stoichiometric equivalent of tions. [Reserved] acibenzolar- S -methyl, in or on the fol- (d) Indirect or inadvertant residues. lowing raw agricultural commodities. [Reserved]

Expiration/ [70 FR 67915, Nov. 9, 2005, as amended at 71 Commodity Parts per revocation FR 76931, Dec. 22, 2006] million date § 180.563 Ethametsulfuron-methyl; tol- Apple ...... 0.05 12/31/15 Grapefruit ...... 0.05 12/31/15 erances for residues. Pear ...... 0.05 12/31/15 (a) General. A tolerance is established for residues of ethametsulfuron methyl (b) Section 18 emergency exemptions. (methyl 2- ((((4-ethoxy-6- [Reserved] (methylamino)-1,3,5- triazin-2-yl) (c) Tolerances with regional registra- amino) carbonyl) amino) sulfonyl) ben- tions. [Reserved] zoate) in or on the following raw agri- (d) Indirect or inadvertent residues. cultural commodities. [Reserved] Parts per [65 FR 50446, Aug. 18, 2000, as amended at 70 Commodity million FR 7861, Feb. 16, 2005; 71 FR 76200, Dec. 20, 2006; 74 FR 24710, May 26, 2009; 76 FR 34886, Canola, seed ...... 0 .02 Crambe, seed ...... 0.02 June 15, 2011; 77 FR 21676, Apr. 11, 2012; 77 FR Rapeseed, seed ...... 0 .02 30406, May 23, 2012] (b) Section 18 emergency exemptions. § 180.562 Flucarbazone-sodium; toler- [Reserved] ances for residues. (c) Tolerances with regional registra- (a) General. Tolerances are estab- tions. [Reserved] lished for combined residues of the her- (d) Indirect of inadvertent residues. bicide flucarbazone-sodium, 4,5- [Reserved] dihydro-3-methoxy-4-methyl-5-oxo-N- [[2(trifluoromethoxy)phenyl] sulfonyl]- [65 FR 57972, Sept. 27, 2000, as amended at 66 FR 18207, Apr. 6, 2001; 67 FR 35050, May 17, 1H-1,2,4-triazole 1-carboxamide, sodium 2002] salt) and its N-desmethyl metabolite; and its metabolites converted to 2- § 180.564 Indoxacarb; tolerances for (trifluoromethoxy)benzene sulfonamide residues. and calculated as flucarbazone-sodium (a) General. (1) Tolerances are estab- in or on the following food commod- lished for residues of indoxacarb, in- ities: cluding its metabolites and degradates, Parts per in or on the commodities in the table Commodity million below. Compliance with the tolerance levels specified below is to be deter- Cattle, liver ...... 1 .50 Cattle, meat ...... 0 .01 mined by measuring only indoxacarb, Cattle, meat byproducts, except liver ...... 0 .01 (S)-methyl 7-chloro-2,5-dihydro-2-[[(me- Goat, liver ...... 1.50 thoxycarbonyl)[4- Goat, meat ...... 0.01 (trifluoromethoxy)phenyl]amino]car- Goat, meat byproducts, except liver ...... 0 .01 Hog, liver ...... 1 .50 bonyl]indeno[1,2-e][1,3,4][oxadiazine-4a Hog, meat ...... 0 .01 (3H)-carboxylate, and its R- Hog, meat byproducts, except liver ...... 0 .01 enantiomer, (R)-methyl 7-chloro-2,5- Horse, liver ...... 1 .50 dihydro-2-[[(methoxycarbonyl)[4- Horse, meat ...... 0 .01 Horse, meat byproducts, except liver ...... 0 .01 (trifluoromethoxy)phenyl] Milk ...... 0.005 amino]carbonyl]indeno[1,2- Sheep, liver ...... 1.50 e][1,3,4][oxadiazine-4a(3H)-carboxylate. Sheep, meat ...... 0.01 Sheep, meat byproducts, except liver ...... 0 .01 Parts per Wheat, forage ...... 0 .30 Commodity million Wheat, grain ...... 0 .01 Wheat, hay ...... 0 .10 Apple, wet pomace ...... 3 .0 Wheat, straw ...... 0 .05 Alfalfa, forage ...... 10 Alfalfa, hay ...... 50 Bean, dry, seed ...... 0 .2 (b) Section 18 emergency exemptions. Bean, succulent ...... 0 .9 [Reserved] Beet, garden, roots ...... 0 .30

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7-chloro-2,5-dihydro-2-[[[4- Commodity Parts per million (trifluoromethoxy)phenyl]- Beet, garden, tops ...... 6 .0 amino]carbonyl]indeno[1,2- Berry, low growing, except strawberry, subgroup e][1,3,4]oxadiazine-4a(3H)-carboxylate; 13–07H ...... 1 IN–KT319, (E)-methyl 5-chloro-2,3,- Bushberry subgroup 13–07B ...... 1 .5 Cattle, fat ...... 1.5 dihydro-2-hydroxy-1-[[[(methoxycar- Cattle, meat ...... 0 .05 bonyl)[4- Cattle, meat byproducts ...... 0.03 (trifluoromethoxy)phenyl]amino]-car- Corn, sweet, forage ...... 10 bonyl]hydrazono]-1H-indene-2- Corn, sweet, kernel plus cob with husk removed 0.02 Corn, sweet, stover ...... 15 carboxylate; IN–JU873, methyl 5- Cotton, gin byproducts ...... 15 chloro-2,3-dihydro-2-hydroxy-1-[[[[4- Cotton, undelinted seed ...... 2 .0 (triflurormethoxy)- Cowpea, forage ...... 50 Cowpea, hay ...... 100 phenyl]amino]carbonyl]hydrazono]-1H- Fruit, pome, except pear, group 11 ...... 1 .0 indene-2-carboxylate; IN–KG433, meth- Fruit, small vine climbing, except fuzzy kiwifruit, yl 5-chloro-2,3,-dihydro-2-hydroxy-1- subgroup 13–07F ...... 2 [[[(methoxycarbonyl)[4- Fruit, stone, group 12 ...... 0 .90 Goat, fat ...... 1 .5 (trifluoromethoxy)phenyl]amino]car- Goat, meat ...... 0.05 bonyl]-hydrazono]-1H-indene-2- Goat, meat byproducts ...... 0 .03 carboxylate; and IN–KB687, methyl [4- Grain, aspirated fractions ...... 45 Grape, raisin ...... 5 .0 (trifluoromethoxy)phenyl]carbamate, Hog, fat ...... 1 .5 calculated as the stoichiometric equiv- Hog, meat ...... 0 .05 alent of indoxacarb in the commodity. Hog, meat byproducts ...... 0 .03 Horse, fat ...... 1 .5 Parts per Horse, meat ...... 0 .05 Commodity million Horse, meat byproducts ...... 0 .03 Milk ...... 0.15 Egg ...... 0 .20 Milk, fat ...... 4 .0 Poultry, fat ...... 0.20 Okra ...... 0.50 Poultry, meat ...... 0 .06 Pea, southern, seed ...... 0.10 Poultry, meat byproducts ...... 0.06 Peanut ...... 0 .01 Peanut, hay ...... 40 (c) Tolerances with regional registra- Pear ...... 0 .20 tions. [Reserved] Pear, oriental ...... 0.20 Peppermint, tops ...... 11 (d) Indirect or inadvertent residues. Sheep, fat ...... 1 .5 [Reserved] Sheep, meat ...... 0.05 Sheep, meat byproducts ...... 0 .03 [65 FR 58424, Sept. 29, 2000, as amended at 67 Soybean, hulls ...... 4 .0 FR 41807, June 19, 2002; 67 FR 47309, July 18, Soybean, seed ...... 0 .80 2002; 67 FR 58730, Sept. 18, 2002; 68 FR 25830, Spearmint, tops ...... 11 May 14, 2003; 68 FR 27746, May 21, 2003; 69 FR Turnip, greens ...... 12 28842, May 19, 2004; 69 FR 29459, May 24, 2004; Vegetable, Brassica, leafy, group 5 ...... 12 69 FR 32282, June 9, 2004; 72 FR 37641, July 11, Vegetable, cucurbit, group 9 ...... 0.60 Vegetable, fruiting, group 8 ...... 0.50 2007; 74 FR 33165, July 10, 2009; 77 FR 8749, Vegetable, leafy, except Brassica, group 4 ...... 14 Feb. 15, 2012; 78 FR 78738, Dec. 27, 2013] Vegetable, tuberous and corm, subgroup 1-C .... 0.01 § 180.565 Thiamethoxam; tolerances (2) Tolerances are established for res- for residues. idues of indoxacarb, including its me- (a) General. Tolerances are estab- tabolites and degradates, in or on the lished for residues of the insecticide commodities in the table below. Com- thiamethoxam, including its metabo- pliance with the tolerance levels speci- lites and degradates, in or on the fol- fied below is to be determined by meas- lowing commodities. Compliance with uring only the sum of indoxacarb, (S)- the tolerance levels specified below is methyl-7-chloro-2,5-dihydro-2-[[(me- to be determined by measuring only thoxycarbonyl)[4-(trifluoromethoxy)- thiamethoxam 3-[(2-chloro-5- phenyl]amino]carbonyl]indeno[1,2e] thiazolyl)methyl]tetrahydro-5-methyl- [1,3,4]oxadiazine-4a(3H)-carboxylate, its N-nitro-4H-1,3,5-oxadiazin-4-imine and R-enantiomer, (R)-methyl 7-chloro-2,5- its metabolite CGA–322704 N-[(2-chloro- dihydro-2-[[(methoxycarbonyl)[4- thiazol-5-yl)methyl]-N′-methyl-N″- (trifluoromethoxy) nitro-guanidine, calculated as the stoi- phenyl]amino]carbonyl]indeno [1,2-e] chiometric equivalent of [1,3,4] oxadiazine-4a(3H)-carboxylate, thiamethoxam, in or on the following and the metabolites: IN–JT333, methyl commodities:

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Parts per Parts per Commodity million Commodity million

Alfalfa, forage ...... 0.05 Peanut, hay ...... 0.25 Alfalfa, hay ...... 0.12 Peanut, meal ...... 0 .15 Almond, hulls ...... 1 .2 Peppermint, tops ...... 1 .5 Artichoke, globe ...... 0.45 Pistachio ...... 0.02 Avocado ...... 0 .40 Potato ...... 0 .25 Barley, grain ...... 0 .4 Radish, tops ...... 0 .80 Barley, hay ...... 0 .40 Rapeseed, seed ...... 0 .02 Barley, straw ...... 0 .40 Rye, forage ...... 0 .50 Bean, succulent ...... 0 .02 Rye, straw ...... 0 .02 Berry, low growing, subgroup 13–07G, except Safflower, seed ...... 0 .02 cranberry ...... 0.30 Sapodilla ...... 0 .40 Borage, seed ...... 0 .02 Sapote, black ...... 0 .40 Brassica, head and stem, subgroup 5–A ...... 4.5 Brassica, leafy greens, subgroup 5–B ...... 3 .0 Sapote, mamey ...... 0 .40 Buckwheat, forage ...... 0 .50 Sheep, meat ...... 0.02 Buckwheat, hay ...... 0 .02 Sheep, meat byproducts ...... 0 .04 Buckwheat, straw ...... 0 .02 Sorghum, forage ...... 0 .02 Bushberry subgroup 13–07B, except lingonberry Sorghum, grain, stover ...... 0 .02 and blueberry, lowbush ...... 0 .20 Soybean, hulls ...... 0 .08 Caneberry subgroup 13–07A ...... 0.35 Spearmint, tops ...... 1 .5 Canistel ...... 0 .40 Star apple ...... 0 .40 Canola, seed ...... 0 .02 Sunflower ...... 0 .02 Cattle, meat ...... 0 .02 Tea, dried 1 ...... 20 Cattle, meat byproducts ...... 0.04 Tomato, paste ...... 0 .80 Citrus, dried pulp ...... 0 .60 Vegetable, cucurbit, group 9 ...... 0.2 Coffee, green, bean 1 ...... 0 .20 Vegetable, fruiting, group 8 ...... 0.25 Corn, field, forage ...... 0 .10 Vegetable, leafy, except brassica, group 4 ...... 4 .0 Corn, field, stover ...... 0 .05 Vegetable, legume, group 6 ...... 0 .02 Corn, pop, forage ...... 0 .10 Vegetable, root, subgroup 1A ...... 0 .05 Corn, pop, stover ...... 0.05 Vegetable, tuberous and corm, except potato, Corn, sweet, forage ...... 0 .10 subgroup 1D ...... 0 .02 Corn, sweet, kernel plus cob with husks re- Wheat, forage ...... 0 .50 moved ...... 0 .02 Wheat, hay ...... 0 .02 Corn, sweet, stover ...... 0 .05 Wheat, straw ...... 0 .02 Cotton, gin byproducts ...... 1 .5 Cotton, undelinted seed ...... 0 .10 1 There are no U.S. registrations as of March 27, 2013. Crambe, seed ...... 0.02 Cranberry ...... 0 .02 (b) Section 18 emergency exemptions. Flax, seed ...... 0 .02 [Reserved] Food commodities and feed commodities (other (c) Tolerances with regional registra- than those covered by a higher tolerance as a tions. [Reserved] result of use on growing crops) in food/feed handling establishments ...... 0 .02 (d) Indirect or inadvertent residues. Fruit, citrus, group 10 ...... 0 .40 [Reserved] Fruit, pome, group 11 ...... 0.2 Fruit, small, vine climbing, subgroup 13–07F, [65 FR 79762, Dec. 20, 2000] except fuzzy kiwifruit ...... 0 .20 Fruit, stone, group 12 ...... 0 .5 EDITORIAL NOTE: For FEDERAL REGISTER ci- Goat, meat ...... 0.02 tations affecting § 180.565, see the List of CFR Goat, meat byproducts ...... 0 .04 Sections Affected, which appears in the Grain, aspirated fractions ...... 2 .0 Finding Aids section of the printed volume Grain, cereal, group 15, except barley ...... 0.02 and at www.fdsys.gov. Grape, raisin ...... 0 .30 Hog, meat ...... 0 .02 Hog, meat byproducts ...... 0 .02 § 180.566 Fenpyroximate; tolerances Hop, dried cones ...... 0 .10 for residues. Horse, meat ...... 0 .02 (a) General. (1) Tolerances are estab- Horse, meat byproducts ...... 0 .04 Mango ...... 0.40 lished for residues of the insecticide Milk ...... 0.02 fenpyroximate, including its metabo- Millet, pearl, forage ...... 0 .02 lites and degradates, in or on the com- Millet, pearl, stover ...... 0 .02 Millet, proso, forage ...... 0 .02 modities in the table below. Compli- Millet, proso, stover ...... 0 .02 ance with the tolerance levels specified Millet, proso, straw ...... 0 .02 in the table is to be determined by Mustard, seed ...... 0 .02 measuring only the sum of Nut, tree, group 14 ...... 0 .02 Oat, forage ...... 0 .50 fenpyroximate, (E)-1,1-dimethylethyl 4- Oat, hay ...... 0.02 [[[[(1,3-dimethyl-5-phenoxy-1H-pyrazol- Oat, straw ...... 0.02 4-yl)methylene]amino]oxy]meth- Onion, dry bulb ...... 0 .03 Papaya ...... 0 .40 yl]benzoate and its Z-isomer, (Z)-1,1- Peanut ...... 0 .05 dimethylethyl 4-[[[[(1,3-dimethyl-5-

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phenoxy-1H-pyrazol-4-yl)meth- Commodity Parts per ylene]amino]oxy]methyl]benzoate, cal- million culated as the stoichiometric equiva- Cattle, fat ...... 0.03 lent of fenpyroximate. Cattle, meat ...... 0 .03 Cattle, meat byproducts, except kidney and Parts per liver ...... 0 .03 Commodity million Goat, fat ...... 0 .03 Goat, meat ...... 0.03 Almond, hulls ...... 3 .0 Goat, meat byproducts, except kidney and liver 0 .03 Avocado ...... 0 .15 Horse, fat ...... 0 .03 Bean, snap, succulent ...... 0 .40 Horse, meat ...... 0 .03 Berry, low growing, subgroup 13–07G ...... 1 .0 Horse, meat byproducts, except kidney and Canistel ...... 0 .15 liver ...... 0 .03 Citrus, dried pulp ...... 2 .5 Milk ...... 0.015 Citrus, oil ...... 10 Sheep, fat ...... 0 .03 Sheep, meat ...... 0.03 Corn, field, forage ...... 2 .0 Sheep, meat byproducts, except kidney and Corn, field, grain ...... 0 .02 liver ...... 0 .03 Corn, field, refined oil ...... 0 .05 Corn, field, stover ...... 7 .0 Corn, pop, forage ...... 2 .0 (3) Tolerances are established for res- Corn, pop, grain ...... 0.02 idues of the insecticide fenpyroximate, Corn, pop, stover ...... 7.0 including its metabolites and Cotton, gin byproducts ...... 10 degradates, in or on the commodities Cotton, undelinted seed ...... 0 .10 Cucumber ...... 0 .40 in the table below. Compliance with Fruit, citrus, group 10–10 ...... 0 .50 the tolerance levels specified in the Fruit, pome, group 11–10 ...... 0 .30 table is to be determined by measuring Fruit, small, vine climbing, except fuzzy only the sum of fenpyroximate, (E)-1,1- kiwifruit, subgroup 13–07F ...... 1 .0 Fruit, stone, group 12–12 ...... 2 .0 dimethylethyl 4-[[[[(1,3-dimethyl-5- Grain, aspirated fractions ...... 0 .40 phenoxy-1H-pyrazol-4-yl)methylene] Hop, dried cones ...... 10 amino]oxy]methyl]benzoate and its Mango ...... 0.15 metabolite (E)-4-[(1,3-dimethyl-5- Melon subgroup 9A ...... 0 .10 Nut, tree, group 14 ...... 0 .10 phenoxypyrazol-4-yl)- Papaya ...... 0 .15 methyleneaminooxymethyl]benzoic Peppermint, tops ...... 7 .0 acid, calculated as the stoichiometric Pistachio ...... 0.10 equivalent of fenpyroximate. Sapodilla ...... 0 .15 Sapote, black ...... 0 .15 Parts per Sapote, mamey ...... 0 .15 Commodity million Spearmint, tops ...... 7 .0 Star, apple ...... 0 .15 Cattle, kidney ...... 0 .25 Tea, dried 1 ...... 20 Cattle, liver ...... 0 .25 Vegetable, fruiting, group 8–10 ...... 0 .20 Goat, kidney ...... 0 .25 Vegetable, tuberous and corm, subgroup 1C ... 0.10 Goat, liver ...... 0.25 Horse, kidney ...... 0 .25 1 There are no U.S. Registrations. Horse, liver ...... 0 .25 Sheep, kidney ...... 0.25 (2) Tolerances are established for res- Sheep, liver ...... 0.25 idues of the insecticide fenpyroximate, including its metabolites and (b) Section 18 emergency exemptions. degradates, in or on the commodities Time-limited tolerances are estab- in the table below. Compliance with lished for residues of the insecticide the tolerance levels specified in the fenpyroximate, including its metabo- table is to be determined by measuring lites and degradates in or on the com- only the sum of fenpyroximate, (E)-1,1- modities in the table below. Compli- dimethylethyl 4-[[[[(1,3-dimethyl-5- ance with the tolerance levels specified phenoxy-1H-pyrazol-4-yl)methylene] in the table is to be determined by amino]oxy]methyl]benzoate and its measuring only the sum of metabolites (E)-4-[(1,3-dimethyl-5- fenpyroximate, (E)-1,1-dimethylethyl 4- phenoxypyrazol-4-yl)- [[[[(1,3-dimethyl-5-phenoxy-1H-pyrazol- methyleneaminooxymethyl]benzoic 4-yl) meth- acid and (E)-1,1-dimethylethyl-2-hy- ylene]amino]oxy]methyl]benzoate and droxyethyl 4-[[[[(1,3-dimethyl-5- its Z-isomer, (Z)-1,1-dimethylethyl 4- phenoxy-1H-pyrazol-4-yl)methylene] [[[[(1,3-dimethyl-5-phenoxy-1H-pyrazol- amino]oxy]methyl]benzoate, calculated 4-yl)methylene]amino]oxy]meth- as the stoichiometric equivalent of yl]benzoate, calculated as the stoichio- fenpyroximate. metric equivalent of fenpyroximate.

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(d) Indirect or inadvertent residues. Commodity Parts per million Expiration/revoca- tion date [Reserved] Honey ...... 0.10 12/31/13 [66 FR 18733, Apr. 11, 2001, as amended at 66 FR 49118, Sept. 26, 2001; 69 FR 16805, Mar. 31, (c) Tolerances with regional registra- 2004; 71 FR 31104, June 1, 2006; 71 FR 76200, tions. [Reserved] Dec. 20, 2006; 75 FR 770, Jan. 6, 2010; 79 FR (d) Indirect or inadvertent residues. 41915, July 18, 2014] [Reserved] § 180.568 Flumioxazin; tolerances for [66 FR 18568, Apr. 10, 2001, as amended at 69 residues. FR 32464, June 10, 2004; 71 FR 49368, Aug. 23, 2006; 72 FR 26321, May 9, 2007; 74 FR 37617, (a) General. Tolerances are estab- July 29, 2009; 74 FR 63079, Dec. 2, 2009; 75 FR lished for residues of flumioxazin, 2-[7- 80346, Dec. 22, 2010; 77 FR 73951, Dec. 12, 2012; fluoro-3,4-dihydro-3-oxo-4-(2-propynyl)- 78 FR 36097, June 17, 2013] 2H-1,4-benzoxazin-6-yl]-4,5,6,7- tetrahydro-1H-isoindole-1,3(2H)-dione, § 180.567 Zoxamide; tolerances for resi- including its metabolites and dues. degradates, in or on the commodities (a) General. (1) Tolerances are estab- in the table below. Compliance with lished for residues of zoxamide includ- the tolerance levels specified below is ing metabolites and degradates, in or to be determined by measuring only on the commodities in the table below. flumioxazin. Compliance with the tolerance levels Parts per specified below is to be determined by Commodity million measuring only zoxamide (3,5-dichloro- N-(3-chloro-1-ethyl-1-methyl-2- Alfalfa, forage ...... 3.0 Alfalfa, hay ...... 8.0 oxopropyl)-4-methylbenzamide). Almond, hulls ...... 0 .70 Artichoke, globe ...... 0.02 Commodity Parts per Asparagus ...... 0.02 million Bushberry subgroup 13–07B ...... 0 .02 Cabbage ...... 0 .02 Grape ...... 3 .0 Cabbage, Chinese, napa ...... 0 .02 Grape, raisin ...... 15.0 Corn, field, forage ...... 0 .02 Tomato ...... 2.0 Corn, field, grain ...... 0 .02 Vegetable, cucurbit, group 9 ...... 1.0 Corn, field, stover ...... 0 .02 Cotton, gin byproducts ...... 0 .60 (2) Tolerances are established for res- Cotton, undelinted seed ...... 0 .02 Fish, freshwater ...... 1 .5 idues of zoxamide including metabo- Fruit, pome, group 11 ...... 0.02 lites and degradates, in or on the com- Fruit, stone, group 12 ...... 0 .02 modities in the table below. Compli- Garlic ...... 0 .02 Grain, aspirated fractions ...... 100 ance with the tolerance levels specified Grape ...... 0 .02 below is to be determined by measuring Hop, dried cones ...... 0 .05 only the sum of zoxamide (3,5-dichloro- Leaf petioles subgroup 4B ...... 0 .02 N-(3-chloro-1-ethyl-1-methyl-2- Nut, tree, group 14 ...... 0 .02 Okra ...... 0.02 oxopropyl)-4-methylbenzamide) and its Olive ...... 0 .02 metabolites 3,5-dichloro-1,4- Onion, bulb ...... 0 .02 benzenedicarboxylic acid (RH–1455 and Pea and bean, dried shelled, except soybean, subgroup 6C ...... 0 .07 RH–141455) and 3,5-dichloro-4- Peanut ...... 0 .02 hydroxymethylbenzoic acid (RH–1452 Peppermint, tops ...... 0 .04 and RH–141452) calculated as the stoi- Pistachio ...... 0.02 Pomegranate ...... 0 .02 chiometric equivalent of zoxamide. Prickly pear, fruit ...... 0 .07 Prickly pear, pads ...... 0.06 Parts per Rapeseed subgroup 20A ...... 0 .40 Commodity million Shallot, bulb ...... 0 .02 Soybean, seed ...... 0 .02 Onion, bulb, subgroup 3–07A ...... 0 .7 Spearmint, tops ...... 0 .04 Potato ...... 0 .060 Strawberry ...... 0 .07 Potato, granules/flakes ...... 0 .30 Sugarcane, cane ...... 0.20 Potato, wet peel ...... 0 .10 Sunflower subgroup 20B ...... 0.50 Vegetable, cucurbit, group 9 ...... 0.03 (b) Section 18 emergency exemptions. Vegetable, fruiting, group 8 ...... 0.02 [Reserved] Vegetable, tuberous and corm, subgroup 1C ..... 0.02 Wheat, forage ...... 0 .02 (c) Tolerances with regional registra- Wheat, grain ...... 0 .40 tions. [Reserved] Wheat, hay ...... 0 .02

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Parts per Expiration/ Commodity million Commodity Parts per revocation million date Wheat, straw ...... 6 .0 Plum, prune, fresh ...... 0.01 12/31/15 (b) Section 18 emergency exemptions. [Reserved] (b) Section 18 emergency exemptions. (c) Tolerances with regional registra- [Reserved] tions. [Reserved] (c) Tolerances with regional restric- (d) Indirect or inadvertent residues. tions. [Reserved] [Reserved] (d) Indirect or inadvertent residues. [Reserved] [66 FR 19878, Apr. 18, 2001, as amended at 68 FR 51471, Aug. 27, 2003; 69 FR 16831, Mar. 31, [66 FR 22936, May 7, 2001, as amended at 69 2004; 69 FR 52198, Aug. 25, 2004; 71 FR 25956, FR 48805, Aug. 11, 2004; 69 FR 58322, Sept. 30, May 3, 2006; 71 FR 61413, Oct. 18, 2006; 73 FR 2004; 73 FR 47846, Aug. 15, 2008; 78 FR 46283, 11831, Mar. 5, 2008; 73 FR 39251, July 9, 2008; 75 July 31, 2013; 79 FR 18471, Apr. 2, 2014] FR 8265, Feb. 24, 2010; 75 FR 69009, Nov. 10, 2010; 77 FR 58499, Sept. 21, 2012; 78 FR 20466, § 180.570 Isoxadifen-ethyl; tolerances Apr. 5, 2013] for residues. (a) General. (1) Tolerances are estab- § 180.569 Forchlorfenuron; tolerances lished for residues of isoxadifen-ethyl for residues. (ethyl 5,5-diphenyl-2-isoxazoline-3- (a) General. (1) Tolerances are estab- carboxylate, (CAS No. 163520–33–0), and lished for residues of forchlorfenuron, its metabolite: 4,5-dihydro-5,5-di- including its metabolites and phenyl-3-isoxazolecarboxylic acid, degradates, in or on the commodities when used as an inert ingredient in the table below. Compliance with (safener) in or on the following raw ag- the tolerance levels specified below is ricultural commodities: to be determined by measuring only forchlorfenuron (N-(2-chloro-4- Commodity Parts per pyridinyl)-N-phenylurea). million Corn, field, forage ...... 0 .20 Commodity Parts per Corn, field, grain ...... 0 .08 million Corn, field, stover ...... 0 .40 Corn, oil ...... 0 .50 Almond ...... 0.01 Corn, pop, grain ...... 0.04 Almond, hulls ...... 0 .15 Bushberry subgroup 13–07B ...... 0 .01 Corn, pop, stover ...... 0.25 Cherry, sweet ...... 0 .01 Corn, sweet, forage ...... 0 .30 Fig ...... 0 .01 Corn, sweet, kernel plus cob with husk removed 0.04 Grape ...... 0 .03 Corn, sweet, stover ...... 0 .45 Grape, raisin ...... 0 .06 Kiwifruit ...... 0.04 (2) Tolerances are established for the Pear ...... 0 .01 residues of isoxadifen-ethyl (3- Pistachio ...... 0.01 Plum, prune, fresh ...... 0.01 isoxazolecarboxylic acid, 4,5-dihydro- 5,5-diphenyl-, ethyl ester (CAS No. (2) Temporary tolerances are estab- 164520–33–0)), and its metabolites 4,5- lished for residues of forchlorfenuron, dihydro-5,5-diphenyl-3- including its metabolites and isoxazolecarboxylic acid and b-hy- degradates, in or on the commodities droxy-b-benzenepropanenitrile when in the table below. Compliance with used as an inert ingredient (safener) in the tolerance levels specified below is or on the following raw agricultural to be determined by measuring on commodities: forchlorfenuron (N-(2-chloro-4- ′ Parts per pyridinyl)-N -phenylurea). Commodity million

Parts per Expiration/ Rice, grain ...... 0 .10 Commodity revocation Rice, hulls ...... 0 .50 million date Rice, straw ...... 0 .25 Almond ...... 0.01 12/31/15 Almond, hulls ...... 0.15 12/31/15 (b) Section 18 emergency exemptions. Cherry, sweet ...... 0.01 12/31/15 [Reserved] Fig ...... 0.01 12/31/15 Pear ...... 0.01 12/31/15 (c) Tolerances with regional registra- Pistachio ...... 0.01 12/31/15 tions. [Reserved]

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(d) Indirect or inadvertent residues. (d) Indirect or inadvertent residues. [Reserved] [Reserved] [66 FR 33187, June 21, 2001, as amended at 66 [66 FR 33195, June 21, 2001, as amended at 67 FR 40141, Aug. 2, 2001; 67 FR 12878, Mar. 20, FR 45656, July 10, 2002; 68 FR 273, Jan. 3, 2003; 2002; 69 FR 29890, May 26, 2004; 72 FR 63997, 69 FR 58310, Sept. 30, 2004; 70 FR 14551, Mar. Nov. 14, 2007] 23, 2005; 72 FR 71802, Dec. 19, 2007; 73 FR 1512, Jan. 9, 2008; 73 FR 9226, Feb. 20, 2008; 74 FR § 180.571 Mesotrione; tolerances for 67123, Dec. 18, 2009; 76 FR 34886, June 15, 2011; residues. 80 FR 30630, May 29, 2015] (a) General. Tolerances are estab- § 180.572 Bifenazate; tolerance for resi- lished for residues of the herbicide dues. mesotrione, including its metabolites (a) General. (1) Tolerances are estab- and degradates, in or on the commod- lished for residues of bifenazate (1- ities in the table below. Compliance methylethyl 2-(4-methoxy[1,1′- with the tolerance levels specified biphenyl]-3-yl)hydrazinecarboxylate) below is to be determined by measuring including its metabolites and only mesotrione, 2-[4-(methylsulfonyl)- degradates, in or on the commodities 2-nitrobenzoyl]-1,3-cyclohexanedione, listed in the following table. Compli- in or on the following raw agricultural ance with the tolerance levels specified commodities: are to be determined by measuring only the sum of bifenazate and its me- Commodity Parts per million tabolite, diazinecarboxylic acid, 2-(4- ′ Almond, hulls ...... 0 .02 methoxy-[1,1 -biphenyl]-3-yl), 1- Asparagus ...... 0.01 methylethyl ester, (calculated as the Berry, group 13 ...... 0 .01 stoichiometric equivalent of Corn, field, forage ...... 0 .01 bifenazate) in or on the following food Corn, field, grain ...... 0 .01 Corn, field, stover ...... 0 .01 commodities: Corn, pop, grain ...... 0.01 Corn, pop, stover ...... 0.01 Parts per Commodity million Corn, sweet, forage ...... 0 .5 Corn, sweet, kernel plus cob with husks re- Acerola ...... 0.90 moved ...... 0 .01 Almond, hulls ...... 15 Corn, sweet, stover ...... 1 .5 Apple, wet pomace ...... 1 .2 Cranberry ...... 0 .02 Atemoya ...... 1 .6 Flax, seed ...... 0 .01 Avocado ...... 7 .0 Fruit, citrus, group 10–10 ...... 0 .01 Bean, dry seed ...... 0 .60 Fruit, pome, group 11–10 ...... 0 .01 Berry, low-growing subgroup 13–07G ...... 1 .5 Fruit, stone, group 12–12 ...... 0 .01 Biriba ...... 1 .6 Grass, forage ...... 0 .01 Black sapote ...... 7 .0 Grass, hay ...... 0 .01 Caneberry subgroup 13-07A ...... 5.0 Grass, seed screenings ...... 0 .10 Canistel ...... 7 .0 Grass, straw ...... 0 .10 Cattle, fat ...... 0.10 Lingonberry ...... 0.01 Cherimoya ...... 1 .6 Millet, forage ...... 0 .01 Cotton, gin byproducts ...... 35 Millet, grain ...... 0 .01 Cotton, undelinted seed ...... 0 .75 Millet, hay ...... 0 .02 Custard apple ...... 1 .6 Millet, straw ...... 0 .02 Feijoa ...... 0 .90 Nut, tree, group 14–12 ...... 0 .01 Fruit, pome, group 11–10 ...... 0 .7 Oat, forage ...... 0 .01 Fruit, small, vine climbing subgroup 13–07F, ex- Oat, grain ...... 0 .01 cept fuzzy kiwifruit ...... 1 .0 Oat, hay ...... 0.01 Fruit, stone, group 12, except plum ...... 2 .5 Oat, straw ...... 0.01 Goat, fat ...... 0 .10 Okra ...... 0.01 Grape ...... 0 .75 Rhubarb ...... 0 .01 Grape, raisin ...... 1 .2 Sorghum, grain, forage ...... 0.01 Guava ...... 0 .9 Sorghum, grain, grain ...... 0 .01 Herb, subgroup 19A, except chervil and chive ... 300 Hog, fat ...... 0 .10 Sorghum, grain, stover ...... 0 .01 Hop, dried cones ...... 15 Sorghum, sweet ...... 0 .01 Horse, fat ...... 0 .10 Soybean, seed ...... 0 .01 Jaboticaba ...... 0 .90 Sugarcane, cane ...... 0.01 Ilama ...... 1 .6 Longan ...... 5 .0 (b) Section 18 emergency exemptions. Lychee ...... 5 .0 [Reserved] Mango ...... 7.0 Nut, tree, group 14 ...... 0 .20 (c) Tolerances with regional registra- Okra ...... 2.0 tions. [Reserved] Papaya ...... 7 .0

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listed in the following table. Compli- Commodity Parts per million ance with the tolerance levels specified Passionfruit ...... 0 .90 are to be determined by measuring Pea and bean, succulent shelled, subgroup 6B 0 .70 only the sum of bifenazate and its me- Peppermint, tops ...... 25 tabolite, diazinecarboxylic acid, 2-(4- Pistachio ...... 0.20 Plum ...... 0 .20 methoxy-[1,1′-biphenyl]-3-yl), 1- Pulasan ...... 5 .0 methylethyl ester, (calculated as the Rambutan ...... 5 .0 stoichiometric equivalent of Sapodilla ...... 7 .0 Sapote, mamey ...... 7 .0 bifenazate) in or on the following food Sheep, fat ...... 0 .10 commodities: Soursop ...... 1 .6 Soybean, succulent shelled ...... 0 .70 Parts per Spanish lime ...... 5 .0 Commodity million Spearmint, tops ...... 25 Star apple ...... 7 .0 Timothy, forage ...... 200 Starfruit ...... 0 .90 Timothy, hay ...... 150 Strawberry ...... 1 .5 Sugar apple ...... 1 .6 (d) Indirect or inadvertent residues. Vegetable, cucurbit, group 9 ...... 0.75 Vegetable, fruiting, group 8–10 ...... 4 .0 [Reserved] Vegetable, legume, edible-podded, subgroup 6A 6.0 Vegetable, tuberous and corm, subgroup 1C ..... 0.10 [66 FR 34569, June 29, 2001] Wax jambu ...... 0 .90 EDITORIAL NOTE: For FEDERAL REGISTER ci- tations affecting § 180.572, see the List of CFR (2) Tolerances are established for res- Sections Affected, which appears in the idues of bifenazate (1-methylethyl 2-(4- Finding Aids section of the printed volume methoxy[1,1′-biphenyl]-3-yl) and at www.fdsys.gov. hydrazinecarboxylate) including its metabolites and degradates, in or on § 180.573 Tepraloxydim; tolerances for the commodities listed in the following residues. table. Compliance with the tolerance (a) General. (1) Tolerances are estab- levels specified are to be determined by lished for residues of tepraloxydim, in- measuring only the sum of bifenazate cluding its metabolites and degradates, and its metabolites diazinecarboxylic in or on the commodities in the table acid, 2-(4-methoxy-[1,1′-biphenyl]-3-yl), below. Compliance with the tolerance 1-methylethyl ester; 1,1′-biphenyl, 4-ol; levels specified below is to be deter- and 1,1′-biphenyl, 4-oxysulfonic acid mined by measuring only the combined (calculated as the stoichiometric residues of tepraloxydim, (2-[1-[[[(2E)-3- equivalent of bifenazate) in or on the chloro-2-propen-1-yl]oxy]imino]propyl]- following food commodities: 3-hydroxy-5-(tetrahydro-2H-pyran-4-yl)- 2-cyclohexen-1-one) and its metabolites Parts per mil- Commodity lion convertible to GP (3-(tetrahydropyran- 4-yl)pentane-1,5-dioic acid) and OH–GP Cattle, meat ...... 0.02 (3-hydroxy-3-(tetrahydropyran-4- Cattle, meat byproducts ...... 0.02 Goat, meat ...... 0.02 yl)pentane-1,5-dioic acid), calculated as Goat, meat byproducts ...... 0.02 tepraloxydim, in or on the commod- Hog, meat ...... 0.02 ities. Hog, meat byproducts ...... 0.02 Horse, meat ...... 0.02 Parts per Horse, meat byproducts ...... 0.02 Commodity million Milk ...... 0.02 Sheep, meat ...... 0.02 Cotton, undelinted seed ...... 0 .2 Sheep, meat byproducts ...... 0.02 Cotton, gin byproducts ...... 3 .0 Flax, seed ...... 0 .10 (b) Section 18 emergency exemptions. Grain, aspirated fraction ...... 1200.0 Pea and bean, dried shelled, except soybean, [Reserved] subgroup 6C 1 ...... 0 .10 (c) Tolerances with regional registra- Soybean, seed ...... 6 .0 tions. Tolerances with regional reg- Soybean, hulls ...... 8 .0 istration, as defined in § 180.1(l), are es- Sunflower subgroup 20B 1 ...... 0.20 tablished for residues of bifenazate (1- 1 There are no U.S. registrations for commodities in this methylethyl 2-(4-methoxy[1,1′- subgroup. biphenyl]-3-yl)hydrazinecarboxylate) (2) Tolerances are established for res- including its metabolites and idues of tepraloxydim, including its degradates, in or on the commodities metabolites and degradates, in or on

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the commodities in the table below. tepraloxydim, in or on the commod- Compliance with the tolerance levels ities. specified below is to be determined by Parts per measuring only the combined residues Commodity million of tepraloxydim (2-[1-[[[(2E)-3-chloro-2- propen-1-yl]oxy]imino]propyl]-3-hy- Canola, seed ...... 0 .50 droxy-5-(tetrahydro-2H-pyran-4-yl)-2- cyclohexen-1-one) and its metabolites (d) Indirect or inadvertent residues. convertible to GP (3-(tetrahydropyran- [Reserved] 4-yl)pentane-1,5-dioic acid), OH–GP (3- [66 FR 40150, Aug. 2, 2001 as amended at 72 FR hydroxy-3-(tetrahydropyran-4- 54588, Sept. 26, 2007; 76 FR 34885, June 15, 2011; yl)pentane-1,5-dioic acid), and GL (3-(2- 76 FR 82152, Dec. 30, 2011] oxotetrahydropyran-4-yl)-1,5-dioic acid), calculated as tepraloxydim, in or § 180.574 Fluazinam; tolerances for on the commodities. residues. (a) General. (1) Tolerances are estab- Parts per Commodity million lished for residues of fluazinam (3- chloro-N-[3-chloro-2,6-dinitro-4- Cattle, fat ...... 0.15 (trifluoromethyl)phenyl]-5- Cattle, kidney ...... 0 .50 Cattle, meat ...... 0 .20 (trifluoromethyl)-2-pyridinamine), in- Cattle, meat byproducts, except kidney ...... 0.20 cluding its metabolites and degradates, Egg ...... 0 .20 in or on the commodities in the table Goat, fat ...... 0 .15 Goat, kidney ...... 0 .50 below. Compliance with the tolerance Goat, meat ...... 0.20 levels specified below is to be deter- Goat, meat byproducts, except kidney ...... 0 .20 mined by measuring only fluazinam. Hog, fat ...... 0 .15 Hog, kidney ...... 0.50 Parts per Hog, meat ...... 0 .20 Commodity million Hog, meat byproducts, except kidney ...... 0 .20 Horse, fat ...... 0 .15 Apple ...... 2.0 Horse, kidney ...... 0 .50 Apple, wet pomace ...... 5 .0 Horse, meat ...... 0 .20 Bushberry subgroup 13-07B ...... 7 .0 Horse, meat byproducts, except kidney ...... 0 .20 Carrot, roots ...... 0.70 Milk ...... 0.10 Ginseng ...... 4 .5 Poultry, fat ...... 0.30 Lettuce, head ...... 0.02 Poultry, liver ...... 1 .00 Poultry, meat ...... 0 .20 Lettuce, leaf ...... 2 .0 Poultry, meat byproducts, except liver ...... 0 .20 Melon subgroup 9A ...... 0 .07 Sheep, fat ...... 0 .15 Onion, bulb, subgroup 3-07A ...... 0 .20 Sheep, kidney ...... 0.50 Pea and bean, dried shelled, except soybean, Sheep, meat ...... 0.20 subgroup 6C, except pea ...... 0.02 Sheep, meat byproducts, except kidney ...... 0 .20 Pea and bean, succulent shelled, subgroup 6B, except pea ...... 0 .04 (b) Section 18 emergency exemptions. Peanut ...... 0 .02 Pepper/eggplant subgroup 8–10B ...... 0 .09 [Reserved] Potato ...... 0 .02 (c) Tolerances with regional registra- Soybean, seed ...... 0 .01 tions. A tolerance with regional reg- Soybean, hulls ...... 0 .05 istration, as defined in § 180.1(l), is es- Turnip, greens ...... 0.01 Vegetable, Brassica leafy, group 5 ...... 0.01 tablished for residues of tepraloxydim, Vegetable, legume, edible-podded, subgroup including its metabolites and 6A, except pea ...... 0.10 degradates, in or on the commodities in the table below. Compliance with (2) Tolerances are established for res- the tolerance levels specified below is idues of fluazinam, including its me- to be determined by measuring only tabolites and degradates, in or on the the combined residues of tepraloxydim commodities in the table below. Com- (2-[1-[[[(2E)-3-chloro-2-propen-1- pliance with the tolerance levels speci- yl]oxy]imino]propyl]-3-hydroxy-5- fied below is to be determined by meas- (tetrahydro-2H-pyran-4-yl)-2-cyclo- uring only fluazinam and its metabo- hexen-1-one) and its metabolites con- lite AMGT (3-[[4-amino-3-[[3-chloro-5- vertible to GP (3-(tetrahydropyran-4- (trifluoromethyl)-2-pyridinyl]amino]-2- yl)pentane-1,5-dioic acid) and OH–GP nitro-6-(trifluoromethyl) phenyl]thio]- (3-hydroxy-3-(tetrahydropyran-4- 2-(beta-D-glucopyranosyloxy) propionic yl)pentane-1,5-dioic acid), calculated as acid).

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Parts per Parts per Commodity million Commodity million

Grape, wine 1 ...... 3 .0 Cattle, meat, dried ...... 0.01

1 Cheese ...... 2 .0 No US registration as of March 15, 2002. Coconut, postharvest ...... 1 .0 (3) Tolerances are established for res- Coffee, bean, roasted bean, postharvest ...... 1 .0 Corn, field, flour, postharvest ...... 0 .01 idues of fluazinam (3-chloro-N-[3- Corn, field, grain, postharvest ...... 0 .05 chloro-2,6-dinitro-4- Corn, field, grits, postharvest ...... 15.0 (trifluoromethyl)phenyl]-5- Corn, field, meal, postharvest ...... 0 .01 Corn, pop, grain, postharvest ...... 0 .05 (trifluoromethyl)-2-pyridinamine), in- Cotton, undelinted seed, postharvest ...... 0.5 cluding its metabolites and degradates, Egg, dried ...... 1 .0 in or on the commodities in the table Fruit, dried, postharvest ...... 0 .05 Ginger, postharvest ...... 0 .5 below. Compliance with the tolerance Grain, aspirated fractions, postharvest ...... 0 .05 levels specified below is to be deter- Herbs and spices group 19, postharvest ...... 0 .5 mined by measuring only fluazinam, Hog, meat ...... 0 .02 Milk, powdered ...... 2 .0 AMPA (2-(6-amino-3-chloro-a,a,a- Millet, grain, postharvest ...... 0.1 trifluoro-2-nitro-p-toluidino)-3-chloro- Nut, pine, postharvest ...... 0.2 5-(trifluoromethyl) pyridine), DAPA (3- Nut, tree, Group 14, postharvest ...... 3 .0 Oat, flour, postharvest ...... 0 .05 chloro-2-(2,6-diamino-3-chloro-a,a,a.- Oat, grain, postharvest ...... 0 .1 trifluoro-p-toluidino)-5- Oat, groats/rolled oats, postharvest ...... 0 .1 (trifluoromethyl)pyridine), and their Peanut, postharvest ...... 0 .5 Pistachio, postharvest ...... 3 .0 sulfamate conjugates. Rice, bran, postharvest ...... 0 .01 Rice, flour, postharvest ...... 0 .05 Parts per Rice, grain, postharvest ...... 0 .04 Commodity million Rice, hulls, postharvest ...... 0.1 Cattle, fat ...... 0.05 Rice, polished rice, postharvest ...... 0 .01 Cattle, meat byproducts ...... 0.05 Rice, wild, grain, postharvest ...... 0 .05 Goat, fat ...... 0 .05 Sorghum, grain, grain, postharvest ...... 0.1 Goat, meat byproducts ...... 0 .05 Triticale, grain, postharvest ...... 0 .1 Horse, fat ...... 0 .05 Vegetable, legume, group 6, postharvest ...... 0.5 Horse, meat byproducts ...... 0 .05 Wheat, bran, postharvest ...... 0 .05 Sheep, fat ...... 0 .05 Wheat, flour, postharvest ...... 0 .05 Sheep, meat byproducts ...... 0 .05 Wheat, germ, postharvest ...... 0 .02 Wheat, grain, postharvest ...... 0 .1 Wheat, milled byproducts, postharvest ...... 0 .05 (b) Section 18 emergency exemptions. Wheat, shorts, postharvest ...... 0 .05 [Reserved] (c) Tolerances with regional registra- (2) To assure safe use of this pesticide tions. [Reserved] commodities treated with sulfuryl flu- (d) Indirect or inadvertent residues. oride must be aerated for at least 24 [Reserved] hours prior to entering commerce. [66 FR 46738, Sept. 7, 2001, as amended at 67 (b) Section 18 emergency exemptions. FR 19130, Apr. 18, 2002; 72 FR 60260, Oct. 24, [Reserved] 2007; 75 FR 26667, May 12, 2010; 76 FR 3029, (c) Tolerances with regional registra- Jan. 19, 2011; 77 FR 66729, Nov. 7, 2012] tion. [Reserved] (d) Indirect or inadvertant residues. § 180.575 Sulfuryl fluoride; tolerances [Reserved] for residues. [67 FR 5740, Feb. 7, 2002, as amended at 69 FR (a)(1) General. Tolerances are estab- 3257, Jan. 23, 2004; 70 FR 40908, July 15, 2005] lished for residues of sulfuryl fluoride in or on the following commodities § 180.576 Cyhalofop-butyl; tolerances from the postharvest fumigation with for residues. sulfuryl fluoride for the control of in- (a) General. Tolerances are estab- sects: lished for residues of cyhalofop-butyl, Parts per including its metabolites and Commodity million degradates, in or on the commodities All processed food commodities not otherwise listed in the table below. Compliance listed ...... 2 .0 with the tolerance levels specified Barley, bran, postharvest ...... 0 .05 below is to be determined by measuring Barley, flour, postharvest ...... 0.05 cyhalofop butyl [R-(+)-n-butyl-2-(4(4- Barley, grain, postharvest ...... 0 .1 Barley, pearled barley, postharvest ...... 0 .05 cyano-2-fluorophenoxy)- Cacao bean, roasted bean, postharvest ...... 0.2 phenoxy)propionate], cyhalofop acid

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[R-(+)-2-(4(4-cyano-2-fluorophenoxy)- acetamiprid. Compliance with the tol- phenoxy)propionic acid], and the di- erance levels specified below is to be acid metabolite [(2R)-4-(4-(1- determined by measuring only carboxyethoxy)phenoxy)-3- acetamiprid in or on the following fluorobenzoic acid]. commodities.

Commodity Parts per Parts per million Commodity million

Rice, grain ...... 0 .40 Almond, hulls ...... 5 .0 Wild rice, grain ...... 0 .40 Asparagus ...... 0.80 Berry, low growing subgroups 13–07G ...... 0.60 (b) Section 18 emergency exemptions. Brassica, head and stem, subgroup 5A ...... 1 .20 Brassica, leafy greens, subgroup 5B ...... 15 [Reserved] Bushberry subgroup 13–07B ...... 1 .6 (c) Tolerances with regional registra- Caneberry subgroup 13–07A ...... 1.6 tions. [Reserved] Canola, seed ...... 0 .010 Citrus, dried pulp ...... 1 .20 (d) Indirect or inadvertent residues. Corn, sweet, forage ...... 15 [Reserved] Corn, sweet, kernel plus cob with husks re- moved ...... 0 .01 [67 FR 43256, June 27, 2002, as amended at 74 Corn, sweet, stover ...... 30 FR 15880, Apr. 8, 2009; 76 FR 82157, Dec. 30, Cotton, gin byproducts ...... 20 .0 2011] Cotton, undelinted seed ...... 0 .60 Fruit, citrus, group 10–10 ...... 1 .0 § 180.577 Bispyribac-sodium; toler- Fruit, pome, group 11–10 ...... 1 .0 Fruit, small, vine climbing, except fuzzy ances for residues. kiwifruit, subgroup 13-07F ...... 0 .35 (a) General. Tolerances are estab- Fruit, stone, group 12, except plum, prune ...... 1 .20 lished for residues of the herbicide Grain, aspirated fractions ...... 5 .0 Mustard, seed ...... 0 .010 bispyribac-sodium, including its me- Nut, tree, group 14 ...... 0 .10 tabolites and degradates, in or on the Onion, bulb, subgroup 3–07A ...... 0 .02 commodity listed below. Compliance Onion, green, subgroup 3–07B ...... 4 .5 Pea and bean, succulent shelled, subgroup 6B 0 .40 with the tolerance level specified below Pistachio ...... 0.10 is to be determined by measuring only Plum, prune, dried ...... 0.40 bispyribac-sodium, (2,6-bis[(4,6- Plum, prune, fresh ...... 0.20 dimethoxy-2-pyrimidinyl)oxy]benzoic Soybean, hulls ...... 0 .04 Soybean, seed ...... 0 .03 acid, sodium salt), in or on the fol- Tea, dried1 ...... 50.0 lowing raw agricultural commodities: Tomato, paste ...... 0 .40 Turnip greens ...... 15 Vegetable, cucurbit, group 9 ...... 0.50 Commodity Parts per million Vegetable, fruiting, group 8–10 ...... 0 .20 Vegetable, leafy, except brassica, group 4 ...... 3 .00 Fish, freshwater ...... 0 .01 Vegetable, legume, edible podded, subgroup Rice, grain ...... 0 .02 6A ...... 0 .60 Rice, straw ...... 0 .02 Vegetable, tuberous and corm, group 1 ...... 0 .01 1There are no U.S. registrations as of February 10, 2010, (b) Section 18 emergency exemptions. for the use of acetamiprid on dried tea. [Reserved] (c) Tolerances with regional registra- (2) Tolerances are established for res- tions. [Reserved] idues of the insecticide acetamiprid (d) Indirect or inadvertent residues. (1E)-N-[(6-chloro-3-pyridinyl)methyl]- ′ [Reserved] N -cyano-N-methylethanimidamide, in- cluding its metabolites and degradates, [66 FR 48097, Sept. 18, 2001, as amended at 76 in or on the commodities in the table FR 5716, Feb. 2, 2011] below as a result of the application of acetamiprid. Compliance with the tol- § 180.578 Acetamiprid; tolerances for residues. erance levels specified below is to be determined by measuring acetamiprid (a) General. (1) Tolerances are estab- and (1E)-N-[(6-chloro-3- lished for residues of the insecticide pyridinyl)methyl]-N′-cyano-N- acetamiprid (1E)-N-[(6-chloro-3- ethanimidamide in or on the following pyridinyl)methyl]-N’-cyano-N- commodities. methylethanimidamide, including its metabolites and degradates, in or on Commodity Parts per the commodities in the table below as million a result of the application of Cattle, fat ...... 0.20

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(d) Indirect or inadvertent residues. Commodity Parts per million [Reserved] Cattle, meat ...... 0 .30 [67 FR 14659, Mar. 27, 2002, as amended at 68 Cattle, meat byproducts ...... 0.70 FR 52352, Sept. 3, 2003; 70 FR 19293, Apr. 13, Egg ...... 0 .010 2005; 72 FR 67262, Nov. 28, 2007; 73 FR 2811, Goat, fat ...... 0 .20 Jan. 16, 2008; 75 FR 6582, Feb. 10, 2010; 77 FR Goat, meat ...... 0.30 18716, Mar. 28, 2012; 77 FR 43529, July 25, 2012; Goat, meat byproducts ...... 0 .70 78 FR 36676, June 19, 2013] Hog, fat ...... 0 .10 Hog, meat ...... 0 .10 § 180.579 Fenamidone; tolerances for Hog, meat byproducts ...... 0 .20 residues. Horse, fat ...... 0 .20 Horse, meat ...... 0 .30 (a) General. (1) Tolerances are estab- Horse, meat byproducts ...... 0 .70 lished for residues of the fungicide, Milk ...... 0.30 fenamidone, including its metabolites Poultry, fat ...... 0.010 and degradates, in or on the following Poultry, liver ...... 0 .050 Poultry, meat ...... 0 .010 commodities. Compliance with the tol- Sheep, fat ...... 0 .20 erance levels is to be determined by Sheep, meat ...... 0.30 measuring only fenamidone (4H- Sheep, meat byproducts ...... 0 .70 Imidazol-4-one, 3,5-dihydro-5-methyl-2- (methylthio)-5-phenyl-3 (phenylamino)- (3) A tolerances of 0.01 ppm is estab- ,(S)-), in or on the commodities: lished for residues of the insecticide Parts per acetamiprid, including its metabolites Commodity million and degradates, in or on all food/feed items (other than those covered by a Bean, succulent, except cowpea ...... 0 .80 Brassica, head and stem, subgroup 5A ...... 5 .0 higher tolerance in paragraph (a)(1) or Brassica, leafy greens, subgroup 5B ...... 55 (a)(2) of this section as a result of the Cilantro, leaves ...... 60 Cotton, gin byproducts ...... 0 .02 use on growing crops) as a result of the Cotton, undelinted seed ...... 0 .02 application of acetamiprid in food/feed Ginseng ...... 0 .80 handling establishments. Compliance Okra ...... 3.5 Onion, bulb, subgroup 3–07A ...... 0 .20 with the 0.01 ppm tolerance level is to Onion, green, subgroup 3–07B ...... 1 .5 be determined by measuring only Pepper, nonbell ...... 3 .5 acetamiprid (1E)-N-[(6-chloro-3- Sunflower ...... 0 .02 Tomato, paste ...... 2 .2 pyridinyl)methyl]-N′-cyano-N- Tomato, puree ...... 2 .0 methylethanimidamide in or on the Turnip, greens ...... 55 commodities. Vegetable, cucurbit, group 9 ...... 0.15 Vegetable, fruiting, group 8, except nonbell pep- (b) Section 18 emergency exemptions. per ...... 1 .0 [Reserved] Vegetable, leafy, except Brassica, group 4 ...... 60 Vegetable, root, except sugar beet, subgroup (c) Tolerances with regional registra- 1B, except radish ...... 0 .15 tions. Tolerances with regional reg- Vegetable, tuberous and corm, subgroup 1C ..... 0.02 istrations are established for residues of the insecticide acetamiprid (1E)-N- (2) Tolerances are established for res- [(6-chloro-3-pyridinyl)methyl]-N′- idues of the fungicide fenamidone, in- cyano-N-methylethanimidamide, in- cluding its metabolites and degradates, cluding its metabolites and degradates, in or on the following commodities. in or on the commodities in the table Compliance with the tolerance levels is below as a result of the application of to be determined by measuring acetamiprid. Compliance with the tol- fenamidone (4H-Imidazol-4-one, 3,5- erance levels specified below is to be dihydro-5-methyl-2-(methylthio)-5- phenyl-3 (phenylamino)-,(S)-), and its determined by measuring only metabolite RPA 717879 (2,4- acetamiprid in or on the following imidazolidinedione, 5-methyl-5-phenyl), commodities. in or on the commodities: Parts per Commodity million Parts per Commodity million

Clover, forage ...... 0.10 Cattle, fat ...... 0.10 Clover, hay ...... 0.01 Cattle, meat ...... 0 .10 Cattle, meat byproducts ...... 0.10

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Commodity Parts per § 180.580 Iodosulfuron-Methyl-Sodium; million tolerances for residues. Goat, fat ...... 0 .10 (a) General. Tolerances are estab- Goat, meat ...... 0.10 lished for residues of the herbicide Goat, meat byproducts ...... 0 .10 Milk ...... 0.02 Iodosulfuron-Methyl-Sodium (methyl 4- Sheep, fat ...... 0 .10 iodo-2-[3-(4-methoxy-6-methyl-1,3,5 Sheep, meat ...... 0.10 triazin-2-yl)ureidosulfonyl]benzoate, so- Sheep, meat byproducts ...... 0 .10 dium salt) in or on the following com- (b) Section 18 emergency exemptions. modities: [Reserved] Parts per (c) Tolerances with regional registra- Commodity million tions. A tolerance with regional reg- Corn, field, forage ...... 0 .05 istration as defined in § 180.1(l) is estab- Corn, field, grain ...... 0 .03 lished for residues of the fungicide Corn, field, stover ...... 0 .05 fenamidone, including its metabolites Wheat, forage ...... 0 .10 Wheat, grain ...... 0 .02 and degradates, in or on the following Wheat, hay ...... 0 .05 commodities. Compliance with the tol- Wheat, straw ...... 0 .05 erance levels is to be determined by measuring only fenamidone (4H- (b) Section 18 emergency exemptions. Imidazol-4-one, 3,5-dihydro-5-methyl-2- [Reserved] (methylthio)-5-phenyl-3 (phenylam- (c) Tolerances with regional registra- ino)-,(S)-), in or on the commodity: tions. [Reserved] (d) Indirect or inadvertent residues. Parts per [Reserved] Commodity million [67 FR 57532, Sept. 11, 2002, as amended at 74 1 Grape ...... 1 .0 FR 23644, May 20, 2009] 1 Applicable to grapes grown East of the Rocky Mountains. (d) Indirect or inadvertent residues. § 180.581 Iprovalicarb; tolerances for residues. Tolerances are established for residues of the fungicide fenamidone, including (a) General. Tolerances are estab- its metabolites and degradates, in or lished for residues of iprovalicarb, [2- on the following commodities. Compli- methyl-1[[[(1S)-(4-methylphenyl) ethyl] ance with the tolerance levels is to be amino]carbonyl] propyl]carbamic acid determined by measuring fenamidone methylethylester, in or on the fol- (4H-Imidazol-4-one, 3,5-dihydro-5-meth- lowing commodities. yl-2-(methylthio)-5-phenyl-3 Parts per (phenylamino)-,(S)-), and its metabo- Commodity million lite RPA 717879 (2,4-imidazolidinedione, Grape 1 ...... 2 .0 5-methyl-5-phenyl), in or on the fol- Tomato 1 ...... 1.0 lowing commodities when present 1There is no U.S. registration as of September 1, 2005. therein as a result of application of fenamidone to the crops in paragraph (b) Section 18 emergency exemptions. (a)(1). [Reserved] (c) Tolerances with regional registra- Commodity Parts per tions. [Reserved] million (d) Indirect or inadvertent residues. Grain, cereal, group 15, except rice ...... 0 .1 [Reserved] Grain, cereal, forage, fodder and straw, group 16, except rice ...... 0 .5 [67 FR 54359, Aug. 22, 2002, as amended at 70 Soybean, forage ...... 0 .15 FR 55281, Sept. 21, 2005] Soybean, hay ...... 0 .25 Soybean, seed ...... 0 .02 § 180.582 Pyraclostrobin; tolerances Strawberry ...... 0 .02 for residues. (a) General. (1) Tolerances are estab- [67 FR 60976, Sept. 27, 2002, as amended at 69 lished for residues of the fungicide FR 58066, Sept. 29, 2004; 71 FR 55293, Sept. 22, 2006; 72 FR 60272, Oct. 24, 2007; 74 FR 34257, pyradostrobin, including its metabo- July 15, 2009; 76 FR 34885, June 15, 2011; 76 FR lites and degradates, in or on the com- 70895, Nov. 16, 2011; 77 FR 32401, June 1, 2012; modities in the table below. Compli- 79 FR 13882, Mar. 12, 2014] ance with the tolerance levels specified

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below is to be determined by measuring Commodity Parts per only the sum of pyraclostrobin (car- million bamic acid, [2-[[[ 1-(4-chlorophenyl)-1H- Pea and bean, dried shelled, except soybean, pyrazol-3-yl]oxy] meth- subgroup 6C ...... 0 .5 yl]phenyl]methoxy-, methyl ester) and Peanut ...... 0 .05 Peanut, refined oil ...... 0.1 its desmethoxy metabolite (methyl-N- Peppermint, tops ...... 8 .0 [[[1-(4-chlorophenyl)-1H-pyrazol-3- Persimmon ...... 3 .0 yl]oxy]methyl] phenylcarbamate), cal- Pistachio ...... 0.7 Radish, tops ...... 16 culated as the stoichiometric equiva- Rye, grain ...... 0.04 lent of pyraclostrobin, in or on the Rye, straw ...... 0 .5 commodity. Sapodilla ...... 0 .6 Sapote, black ...... 0 .6 Parts per Sapote, mamey ...... 0 .6 Commodity million Sorghum, grain, forage ...... 5.0 Sorghum, grain, grain ...... 0 .60 Alfalfa, forage ...... 10 Sorghum, grain, stover ...... 0 .80 Alfalfa, hay ...... 30 Soybean, forage ...... 11 Almond, hulls ...... 7 .0 Soybean, hay ...... 14 Apple, wet pomace ...... 8 .0 Soybean, hulls ...... 0 .06 Artichoke, globe ...... 3.0 Soybean, seed ...... 0 .04 Avocado ...... 0 .6 Spearmint, tops ...... 8 .0 Banana ...... 0.04 Star apple ...... 0 .6 Barley, grain ...... 1 .4 Sugarcane, cane ...... 0.20 Barley, hay ...... 25 Vegetable, bulb, group 3–07 ...... 0 .9 Barley, straw ...... 6 .0 Vegetable, cucurbit, group 9 ...... 0.5 Bean, succulent shelled ...... 0 .5 Vegetable, foliage of legume, except soybean, Beet, sugar, dried pulp ...... 1 .0 subgroup 7A ...... 25 .0 Beet, sugar, roots ...... 0 .2 Vegetable, fruiting, group 8–10 ...... 1 .4 Beet, sugar, tops ...... 8.0 Vegetable, leafy, except brassica, group 4 ...... 29.0 Berry, low growing, subgroup 13–07G, except Vegetable, leaves of root and tuber, group 2, cranberry ...... 1.2 except sugar beet ...... 16 .0 Brassica, head and stem, subgroup 5A ...... 5 .0 Vegetable, legume, edible podded, subgroup Brassica, leafy greens, subgroup 5B ...... 16 .0 6A ...... 0 .5 Bushberry subgroup 13–07B ...... 4 .0 Vegetable, root, except sugar beet, subgroup Caneberry subgroup 13–07A ...... 4.0 1B ...... 0 .4 Canistel ...... 0 .6 Vegetable, tuberous and corm, subgroup 1C ... 0.04 Citrus, dried pulp ...... 12 .5 Vegetables, foliage of legume, group 7 ...... 25 Citrus, oil ...... 9.0 Wheat, grain ...... 0 .02 Coffee, green bean ...... 1 0 .3 Wheat, hay ...... 6 .0 Corn, field, forage ...... 5 .0 Wheat, straw ...... 8 .5 Corn, field, grain ...... 0 .1 Corn, field, refined oil ...... 0 .2 (2) Tolerances are established for Corn, field, stover ...... 17 .0 Corn, pop, grain ...... 0.1 combined residues of the fungicide Corn, pop, stover ...... 17.0 pyraclostrobin carbamic acid, [2-[[[1-(4- Corn, sweet, forage ...... 5 .0 chlorophenyl)-1H-pyrazol-3- Corn, sweet, kernel plus cob with husks re- yl]oxy]methyl]phenyl]methoxy-, meth- moved ...... 0 .04 Corn, sweet, stover ...... 23.0 yl ester and its metabolites convertible Cotton, gin byproducts ...... 30 to 1-(4-chlorophenyl)-1H-pyrazol-3-ol Dill, seed ...... 40 and 1-(4-chloro-2-hydroxyphenyl)-1H- Endive, belgium ...... 4 .0 Fruit, citrus, group 10–10 ...... 2 .0 pyrazol-3-ol, expressed as parent com- Fruit, pome, group 11–10 ...... 1 .5 pound, in or on the following raw agri- Fruit, small vine climbing, except fuzzy cultural commodities. kiwifruit, subgroup 13–07F ...... 2.0 Fruit, stone, group 12–12 ...... 2 .5 Parts per Grain, aspirated fractions ...... 2 .5 Commodity million Grape, raisin ...... 7 .0 Grass, forage ...... 10 Cattle, fat ...... 0.1 Grass, hay ...... 4 .5 Cattle, liver ...... 1 .5 Grass, seed screenings ...... 27 Cattle, meat ...... 0 .1 Grass, straw ...... 14 Cattle, meat byproducts, except liver ...... 0 .2 Herb subgroup 19A ...... 40 Goat, fat ...... 0 .1 Hop, dried cones ...... 23 .0 Goat, liver ...... 1.5 Mango ...... 0.6 Goat, meat ...... 0.1 Nut, tree, group 14–12, except pistachio ...... 0 .04 Goat, meat byproducts, except liver ...... 0 .2 Oat, grain ...... 1 .2 Hog, fat ...... 0 .1 Oat, hay ...... 18 Hog, liver ...... 1 .5 Oat, straw ...... 15 Hog, meat ...... 0 .1 Oilseed group 20 ...... 0 .45 Hog, meat byproducts, except liver ...... 0 .2 Papaya ...... 0 .6 Horse, fat ...... 0 .1 Pea, succulent ...... 0 .2 Horse, liver ...... 0 .1

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Parts per Parts per Commodity million Commodity million

Horse, meat ...... 0 .1 Grain, cereal, forage, fodder and straw, group Horse, meat byproducts, except liver ...... 0 .2 16, except rice ...... 0 .10 Milk ...... 0.1 Grain, cereal, group 15, except rice ...... 0 .01 Poultry, eggs ...... 0 .10 Poultry, fat ...... 0.10 (b) Section 18 emergency exemptions. Poultry, meat ...... 0 .10 [Reserved] Poultry, meat byproducts ...... 0.10 (c) Tolerances with regional registra- Sheep, fat ...... 0 .1 Sheep, liver ...... 1.5 tions. [Reserved] Sheep, meat ...... 0.1 (d) Indirect or inadvertent residues. Sheep, meat byproducts, except liver ...... 0 .2 [Reserved] [67 FR 60959, Sept. 27, 2002, as amended at 75 (b) Section 18 emergency exemptions. A FR 4288, Jan. 27, 2010] time-limited tolerance is established for combined residues of the fungicide § 180.584 Tolylfluanid; tolerances for pyraclostrobin, (carbamic acid, [2-[[[1- residues. (4-chlorophenyl)-1H-pyrazol-3- (a) General. Tolerances are estab- yl]oxy]methyl] phenyl]methoxy-, lished for residues of tolylfluanid, 1,1- methyl ester) and its desmethoxy me- dichloro-N-[(dimethylamino)-sulfonyl]- tabolite (methyl-N-[[[1-(4- 1-fluoro-N-(4- chlorophenyl) pyrazol-3-yl]oxy]o- methylphenyl)methanesulfenamide in tolyl]carbamate) in connection with or on the following commodities. use of the pesticide under section 18 emergency exemptions granted by Commodity Parts per EPA. The time-limited tolerance will million expire and is revoked on the date speci- Apple 1 ...... 5.0 fied in the following table. Grape 1 ...... 11 Hop, dried cones 1 ...... 30 Tomato 1 ...... 2.0 Parts per Expiration/ Commodity revocation 1 million date No U.S. registration as of August 31, 2002. (b) Section 18 emergency exemptions. Endive, belgium ...... 11.0 12/31/13 [Reserved] (c) Tolerances with regional registra- (c) Tolerances with regional registra- tions. [Reserved] tions. [Reserved] (d) Indirect or inadvertent residues. (d) Indirect or inadvertent residues. [Reserved] [Reserved] [67 FR 60141, Sept. 25, 2002] [67 FR 60901, Sept. 27, 2002, as amended at 69 FR 63100, Oct. 29, 2004; 71 FR 17021, Apr. 5, § 180.585 Pyraflufen-ethyl; tolerances 2006; 72 FR 54569, Sept. 26, 2007; 73 FR 15431, for residues. Mar. 24, 2008; 73 FR 21842, Apr. 23, 2008; 73 FR 44167, July 30, 2008; 74 FR 11499, Mar. 18, 2009; (a) General. Tolerances are estab- 74 FR 51496, Oct. 7, 2009; 75 FR 770, Jan. 6, lished for residues of the herbicide, 2010; 75 FR 42329, July 21, 2010; 75 FR 80346, pyraflufen-ethyl, including its metabo- Dec. 22, 2010; 76 FR 81396, Dec. 28, 2011; 78 FR lites and degradates, in the commod- 53046, Aug. 28, 2013; 80 FR 19238, Apr. 10, 2015] ities in the table below. Compliance with the plant commodity tolerance § 180.583 Triticonazole; tolerances for levels specified in the table is to be de- residues. termined by measuring only the sum of (a) General. Tolerances are estab- the parent pyraflufen-ethyl, ethyl 2-[2- lished for residues of the fungicide chloro-5-(4-chloro-5-difluoromethoxy)- triticonazole, (1RS)-(E)-5-[(4- 1-methyl-1H-pyrazol-3-yl]-4- chlorophenyl)methylene]-2,2-dimethyl- fluorophenoxy] acetate, and its acid 1-(1H-1,2,4-triazol-1- metabolite, E–1, 2-chloro-5-(4-chloro-5- ylmethyl)cyclopentanol, from the difluoromethoxy-1-methyl-1H-pyrazol- treatment of seed prior to planting in 3-yl)-4-fluorophenoxyacetic acid, cal- or on raw agricultural commodities as culated as the stoichiometric equiva- follows: lent of pyraflufen-ethyl in or on the

609

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commodity. Compliance with the live- (d) Indirect or inadvertent residues. stock commodity tolerance levels spec- [Reserved] ified in the table is to be determined by [68 FR 23055, Apr. 30, 2003, as amended at 68 measuring only the sum of the parent FR 27739, May 21, 2003; 69 FR 26312, May 12, pyraflufen-ethyl, ethyl 2-[2-chloro-5-(4- 2004; 73 FR 51743, Sept. 5, 2008; 76 FR 31484, chloro-5-difluoromethoxy)-1-methyl- June 11, 2011; 77 FR 75861, Dec. 26, 2012; 78 FR 1H-pyrazol-3-yl]-4-fluorophenoxy] ace- 13263, Feb. 27, 2013] tate and its acid metabolites: E–1, 2- § 180.586 Clothianidin; tolerances for chloro-5-(4-chloro-5-difluoromethoxy-1- residues. methyl-1H-pyrazol-3-yl)-4- (a) General. (1) Tolerances are estab- fluorophenoxyacetic acid, and E–9, 2- lished for residues of the insecticide chloro-5-(4-chloro-5-difluoromethoxy- clothianidin, including its metabolites 1H-pyrazol-3-yl)-4-fluorophenoxyacetic and degradates. Compliance with the acid, both calculated as the stoichio- tolerance levels specified below is to be metric equivalent of pyraflufen-ethyl determined by measuring only in or on the commodity. clothianidin, (E)-N-[(2-Chloro-5- thiazolyl)methyl]-N′ -methyl-N″ Parts per Commodity million -nitroguanidine, in or on the following raw agricultural commodities: Almond, hulls ...... 0 .02 Cattle, fat ...... 0.03 Commodity Parts per Cattle, meat ...... 0 .03 million Cattle, meat byproducts ...... 0.03 Almond, hulls ...... 1 .5 Corn, field, forage ...... 0 .01 Beet, sugar, dried pulp ...... 0 .03 Corn, field, grain ...... 0 .01 Beet, sugar, molasses ...... 0 .05 Corn, field, stover ...... 0 .01 Beet, sugar, roots ...... 0 .02 Cotton, gin byproducts ...... 1 .5 Berry, low-growing, subgroup 13-07H, except Cotton, undelinted seed ...... 0 .04 strawberry ...... 0.01 Fruit, pome, group 11–10 ...... 0 .01 Canola, seed ...... 0 .01 Fruit, stone, group 12 ...... 0 .01 Cotton, gin byproducts ...... 4 .5 Cotton, undelinted seed ...... 0 .20 Goat, fat ...... 0 .03 Fig ...... 0 .05 Goat, meat ...... 0.03 Fruit, pome ...... 1.0 Goat, meat byproducts ...... 0 .03 Grain, cereal, forage, fodder and straw, group Grape ...... 0 .01 16, except rice, forage ...... 0 .35 Grass, forage, group 17 ...... 1 .0 Grain, cereal, forage, fodder and straw, group Grass, hay, group 17 ...... 1 .4 16, except rice, hay ...... 0 .07 Horse, fat ...... 0 .03 Grain, cereal, forage, fodder and straw, group 16, except rice, stover ...... 0 .1 Horse, meat ...... 0 .03 Grain, cereal, forage, fodder and straw, group Horse, meat byproducts ...... 0 .03 16, except rice, straw ...... 0.05 Milk ...... 0.03 Grain, cereal, group 15, except rice ...... 0 .01 Nut, tree, group 14 ...... 0 .01 Grape ...... 0 .60 Olive ...... 0 .01 Milk ...... 0.01 Peanut ...... 0 .01 Mustard, seed ...... 0 .01 Peanut, hay ...... 0.07 Nut, tree, group 14 ...... 0 .01 Peach ...... 0 .80 Pistachio ...... 0.01 Pepper ...... 0 .80 Pomegranate ...... 0 .01 Pomegranate ...... 0 .20 Potato ...... 0 .02 Potato, chips ...... 0 .6 Sheep, fat ...... 0 .03 Potato, granules/flakes ...... 1 .5 Sheep, meat ...... 0.03 Rice, grain ...... 0 .01 Sheep, meat byproducts ...... 0 .03 Soybean, seed ...... 0 .02 1 Soybean, forage ...... 0 .05 Tea, dried ...... 70 Vegetable, brassica, leafy, group 5 ...... 1.9 Soybean, hay ...... 0 .10 Vegetable, bulb, group 3-07 ...... 0 .45 Soybean, seed ...... 0 .01 Vegetable, cucurbit, group 9 ...... 0.06 Wheat, forage ...... 0 .02 Vegetable, fruiting, group 8, except pepper ...... 0.20 Wheat, grain ...... 0 .01 Vegetable, leafy, except brassica, group 4 ...... 3 .0 Wheat, hay ...... 0 .01 Vegetable, root, except sugar beet, subgroup Wheat, straw ...... 0 .01 1B ...... 0 .8 Vegetable, tuberous and corm, subgroup 1C ..... 0.3 (b) Section 18 emergency exemptions. 1 No U.S. registrations. [Reserved] (2) Time-limited tolerances are estab- (c) Tolerances with regional registra- lished for residues of the insecticide tions. [Reserved] clothianidin, including its metabolites and degradates. Compliance with the

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tolerance levels specified below is to be § 180.587 Famoxadone; tolerance for determined by measuring only residues. clothianidin, (E)-1-(2-chloro-1,3-thiazol- (a) General. Tolerances are estab- 5-ylmethyl)-3-methyl-2-nitroguanidine, lished for residues of the fungicide in or on the following raw agricultural famoxadone (3-anilino-5-methyl-5-(4- commodity: phenoxyphenyl)-1,3-oxazolidine-2,4- dione) in or on the following commod- Expiration/ Commodity Parts per revocation ities: million date Commodity Parts per Rice, seed ...... 0.01 6/23/12 million Caneberry subgroup 13–07A ...... 10 (b) Section 18 emergency exemptions. A Cattle, fat ...... 0.02 time-limited tolerance specified in the Cattle, liver ...... 0 .05 Cilantro, leaves ...... 25 following table is established for resi- Goat, fat ...... 0 .02 dues of clothianidin, (E)-N-[(2-chloro-5- Goat, liver ...... 0.05 Grape, raisin 1 ...... 4 .0 thiazolyl)methyl]-N’-methyl-N’’- Hop, dried cone ...... 80 nitroguanidine, in or on the specified Horse, fat ...... 0 .02 agricultural commodity, resulting Horse, liver ...... 0 .05 Milk, fat (reflecting negligible residues in whole from use of the pesticide pursuant to milk) ...... 0 .06 FIFRA section 18 emergency exemp- Onion, bulb, subgroup 3–07A ...... 0 .45 tions. This tolerance expires on the Onion, green, subgroup 3–07B ...... 40 Potato ...... 0 .02 date specified in the table. Sheep, fat ...... 0 .02 Sheep, liver ...... 0.05 Parts per Expiration Spinach ...... 50 Commodity million date Tomato ...... 1.0 Vegetable, cucurbit, group 9 ...... 0.30 Fruit, citrus, group 10–10 ...... 0.07 12/31/17 Vegetable, fruiting, group 8, except tomato ...... 4 .0 Vegetable, leafy, except Brassica, group 4, ex- (c) Tolerances with regional registra- cept spinach ...... 25 tions. [Reserved] 1 There are no U.S. registrations as of May 15, 2003. (d) Indirect and inadvertant residues. (b) Section 18 emergency exemptions. Tolerances are established for the indi- [Reserved] rect or inadvertent residues of the in- (c) Tolerances with a regional registra- secticide clothianidin, including its tions. Tolerances with a regional reg- metabolites and degradates. Compli- istration as defined in § 180.1(l) are es- ance with the tolerance levels specified tablished for the residues of the fun- below is to be determined by measuring gicide famoxadone, 3-anilino-5-methyl- only clothianidin, (E)-1-(2-chloro-1,3- 5-(4-phenoxyphenyl)-1,3-oxazolidine-2,4- thiazol-5-ylmethyl)-3-methyl-2- dione) in or on the raw agricultural commodities: nitroguanidine, in or on the following raw agricultural commodities when Commodity Parts per present therein as a result of the appli- million cation of clothianidin to crops listed in Grape ...... 2 .5 paragraph (a) of this section: (d) Indirect or inadvertant residues. Parts per [Reserved] Commodity million [68 FR 39471, July 2, 2003, as amended at 72 Animal feed, nongrass, group 18 ...... 0 .02 FR 28881, May 23, 2007; 74 FR 9364, Mar. 4, Grass, forage, fodder and hay, group 17 ...... 0 .02 2009; 76 FR 34885, June 15, 2011] Soybean, forage ...... 0 .02 Soybean, hay ...... 0 .02 § 180.588 Quinoxyfen; tolerances for residues. [74 FR 65028, Dec. 9, 2009, as amended at 76 (a) General. Tolerances are estab- FR 7718, Feb. 11, 2011; 76 FR 25246, May 4, lished for residues of the fungicide 2011; 76 FR 34886, June 15, 2011; 77 FR 52252, quinoxyfen, including its metabolites Aug. 29, 2012; 78 FR 19136, Mar. 29, 2013; 80 FR and degradates, in or on the commod- 10007, Feb. 25, 2015] ities in the following table. Compliance with the tolerance levels specified in

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the following table is to be determined Commodity Parts per by measuring only quinoxyfen (5,7- million dichloro-4-(4-fluorophenoxy)quinoline). Dill, seed ...... 100 Endive, Belgium ...... 6 .0 Commodity Parts per Fruit, citrus, group 10–10 ...... 2 .0 million Fruit, pome, group 11–10 ...... 3 .0 Fruit, small vine climbing, except fuzzy kiwifruit, Artichoke, globe ...... 1.4 subgroup 13–07F ...... 5 .0 Berry, low growing, subgroup 13–07G ...... 1 .0 Fruit, stone, group 12–12 ...... 3 .5 Fruit, small vine climbing, except fuzzy kiwifruit, Grain, aspirated fractions ...... 3 .0 subgroup 13–07F ...... 2 .0 Grape, raisin ...... 8 .5 Fruit, stone, group 12 ...... 0 .70 Herb subgroup 19A ...... 150 Hop, dried cones ...... 3 .0 Hop, dried cones ...... 35 Gourd, edible ...... 0 .20 Leaf petioles subgroup 4B ...... 45 Lettuce, head ...... 7.0 Leafy greens subgroup 4A, except head lettuce Lettuce, leaf ...... 19 and leaf lettuce ...... 60 Melon, subgroup 9A ...... 0 .08 Lettuce, head ...... 6.5 Pumpkin ...... 0.20 Lettuce, leaf ...... 11 .0 Squash, winter ...... 0 .20 Mango ...... 1.5 Vegetable, fruiting, group 8–10 ...... 1 .7 Nut, tree, group 14–12 ...... 0 .70 Oilseed group 20 ...... 3 .5 (b) Section 18 emergency exemptions. Papaya ...... 1 .5 [Reserved] Pea and bean, dried shelled, except soybean, subgroup 6C, except cowpea, field pea and (c) Tolerances with regional registra- grain lupin ...... 2 .5 tions. [Reserved] Pea and bean, succulent shelled, subgroup 6B, (d) Indirect or inadvertent residues. except cowpea ...... 0 .6 [Reserved] Peanut ...... 0 .05 Peanut, meal ...... 0 .15 [68 FR 55858, Sept. 29, 2003, as amended at 70 Peanut, refined oil ...... 0.15 FR 4032, Jan. 28, 2005; 71 FR 50354, Aug. 25, Peppermint, tops ...... 30 .0 Persimmon ...... 8 .0 2006; 74 FR 14743, Apr. 1, 2009; 78 FR 57280, Sapodilla ...... 1 .5 Sept. 18, 2013] Sapote, black ...... 1 .5 Sapote, mamey ...... 1 .5 § 180.589 Boscalid; tolerances for resi- Soybean, hulls ...... 0 .2 dues. Soybean, seed ...... 0 .1 Soybean, vegetable ...... 2 .0 (a) General. (1) Tolerances are estab- Spearmint, tops ...... 30 .0 lished for residues of the fungicide Star apple ...... 1 .5 Turnip, greens ...... 40.0 boscalid, including its metabolites and Vegetable, bulb, group 3–07 ...... 5 .0 degradates, in or on the commodities Vegetable, cucurbit, group 9, except cucumber 1.6 listed below. Compliance with the tol- Vegetable, fruiting, group 8–10 ...... 3 .0 erance levels specified below is to be Vegetable, legume, edible podded, subgroup 6A 1 .6 Vegetable, root, subgroup 1A, except sugar determined by measuring only beet, garden beet, radish, and turnip ...... 1.0 boscalid, 3-pyridinecarboxamide, 2- Vegetable, tuberous and corm, subgroup 1C ..... 0.05 chloro-N-(4′-chloro[1,1’-biphenyl]-2-yl), 1No US registrations as of September 16, 2009. in or on the following raw agricultural commodities: (2) Tolerances are established for res- idues of the fungicide boscalid, includ- Commodity Parts per ing its metabolites and degradates, in million or on the commodities listed below. Alfalfa, forage ...... 30.0 Compliance with the tolerance levels Alfalfa, hay ...... 65.0 specified below is to be determined by Almond, hulls ...... 17 measuring only the sum of boscalid, 3- Apple, wet pomace ...... 10 Artichoke, globe ...... 6.0 pyridinecarboxamide, 2-chloro-N-(4’- Avocado ...... 1 .5 chloro[1,1’-biphenyl]-2-yl), and metabo- Banana, import 1 ...... 0 .40 lites 2-chloro-N-(4’-chloro-5-hydroxy- Berry, low growing, subgroup 13–07G, except cranberry ...... 4.5 biphenyl-2-yl) nicotinamide and glucu- Brassica, head and stem, subgroup 5A ...... 3 .0 ronic acid conjugate of 2-chloro-N-(4′- Brassica, leafy greens, subgroup 5B ...... 18 .0 chloro-5-hydroxy-biphenyl-2-yl) nico- Bushberry subgroup 13–07B ...... 13 .0 Caneberry subgroup 13–07A ...... 10.0 tinamide, calculated as the stoichio- Canistel ...... 1 .5 metric equivalent of boscalid in or on Canola, refined oil ...... 5 .0 the following food commodities: Citrus, dried pulp ...... 4 .5 Citrus, oil ...... 85.0 Parts per Coffee, green bean, import 1 ...... 0 .05 Commodity million Cotton, gin byproducts ...... 55 .0 Cucumber ...... 0 .5 Cattle, fat ...... 0.30

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Parts per Parts per Commodity million Commodity million

Cattle, meat ...... 0 .10 Grain, cereal, forage, fodder and straw, group Cattle, meat byproducts ...... 0.35 16, forage ...... 2 .0 Egg ...... 0 .02 Grain, cereal, forage, fodder and straw, group Goat, fat ...... 0 .30 16, stover ...... 1 .5 Goat, meat ...... 0.10 Grain, cereal, forage, fodder and straw, group Goat, meat byproducts ...... 0 .35 16, straw ...... 3 .0 Hog, fat ...... 0 .20 Grain, cereal, group 15 ...... 0.20 Hog, meat ...... 0 .05 Grass, forage, fodder, and hay, group 17, for- Hog, meat byproducts ...... 0 .10 age ...... 2 .0 Horse, fat ...... 0 .30 Grass, forage, fodder, and hay, group 17, hay ... 8 .0 Horse, meat ...... 0 .10 Grass, forage, fodder, and hay, group 17, seed Horse, meat byproducts ...... 0 .35 screenings ...... 0 .20 Milk ...... 0.10 Grass, forage, fodder, and hay, group 17, straw 0 .30 Poultry, fat ...... 0.20 Lupin, grain, grain ...... 0 .1 Poultry, meat ...... 0 .05 Pea, field, seed ...... 0 .1 Poultry, meat byproducts ...... 0.20 Radish, roots ...... 0 .1 Sheep, fat ...... 0 .30 Rice, hulls ...... 0 .50 Sheep, meat ...... 0.10 Turnip, roots ...... 0 .1 Sheep, meat byproducts ...... 0 .35 Vegetable, foliage of legume, group 7, forage .... 1 .5 Vegetable, foliage of legume, group 7, hay ...... 2 .0 (b) Section 18 emergency exemptions. Vegetable, foliage of legume, group 7, vines ..... 0 .05 Vegetable, leafy, except brassica, group 4, ex- Time-limited tolerances are estab- cept celery, lettuce and spinach ...... 1 .0 lished for residues of the fungicide Vegetable, leaves of root and tuber, group 2 ..... 0 .1 boscalid, including its metabolites and degradates, in connection with use of [68 FR 44651, July 30, 2003, as amended at 69 the pesticide under section 18 emer- FR 19774, Apr. 14, 2004; 70 FR 55293, Sept. 21, gency exemptions granted by EPA. 2005; 71 FR 6364, Feb. 8, 2006; 71 FR 25961, May Compliance with the tolerance level 3, 2006; 71 FR 76190, Dec. 20, 2006; 73 FR 16558, specified below is to be determined by Mar. 28, 2008; 74 FR 47445, Sept. 16, 2009; 75 FR measuring only boscalid, 3- 770, Jan. 6, 2010; 75 FR 29907, May 28, 2010; 75 pyridinecarboxamide, 2-chloro-N-(4′- FR 80346, Dec. 22, 2010; 78 FR 67048, Nov. 8, 2013; 80 FR 14014, Mar. 18, 2015] chloro[1,1’-biphenyl]-2-yl). This toler- ance will expire and is revoked on the § 180.590 2, 6-Diisopropylnaphthalene date specified in the following table: (2, 6-DIPN); tolerances for residues. (a) General. Tolerances are estab- Parts per Expiration/ Commodity million revocation lished for residues of the growth inhib- date itor 2,6-DIPN, including its metabolites Endive, Belgian ...... 16 12/31/13 and degradates, in or on the commod- ities in the following table. Compliance (c) Tolerances with regional registra- with the tolerance levels specified in tion. [Reserved] the following table is to be determined (d) Indirect or inadvertent residues. by measuring only 2,6- Tolerances are established for the indi- Diisopropylnaphthalene. rect or inadvertent residues of the fun- gicide boscalid, including its metabo- Parts per Commodity million lites and degradates, in or on the com- modities listed below. Compliance with Cattle, fat ...... 0.2 the tolerance levels specified below is Cattle, meat ...... 0 .02 Cattle, meat byproducts, except fat ...... 0 .02 to be determined by measuring only Goat, fat ...... 0 .2 boscalid, 3-pyridinecarboxamide, 2- Goat, meat ...... 0.02 chloro-N-(4′-chloro[1,1’-biphenyl]-2-yl), Goat, meat byproducts, except fat ...... 0 .02 Horse, fat ...... 0 .2 in or on the following commodities: Horse, meat ...... 0 .02 Horse, meat byproducts, except fat ...... 0.02 Commodity Parts per Milk, fat ...... 0 .02 million Potato, granules/flakes ...... 5 .5 Potato, wet peel ...... 6 .0 Animal feed, nongrass, group 18, forage, except Potato, whole ...... 2 .0 alfalfa ...... 1.0 Sheep, fat ...... 0 .2 Animal feed, nongrass, group 18, hay, except Sheep, meat ...... 0.02 alfalfa ...... 2.0 Sheep, meat byproducts, except fat ...... 0 .02 Animal feed, nongrass, group 18, seed ...... 0 .05 Beet, garden, roots ...... 0 .1 Beet, sugar, roots ...... 0 .1 (b) Section 18 emergency exemptions. Cowpea, seed ...... 0 .1 [Reserved]

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(c) Tolerances with regional registra- 1(2H)-pyrimidinyl] benzoate), in or on tions. [Reserved] the following livestock commodities: (d) Indirect or inadvertent residues. Parts per [Reserved] Commodity million

[71 FR 52011, Sept. 1, 2006, as amended at 74 Cattle, kidney ...... 0 .05 FR 66579, Dec. 16, 2009; 77 FR 32406, June 1, Cattle, liver ...... 0 .50 2012] Goat, kidney ...... 0 .05 Goat, liver ...... 0.50 § 180.591 Trifloxysulfuron; tolerances Hog, kidney ...... 0.05 for residues. Hog, liver ...... 0 .50 Horse, kidney ...... 0 .05 (a) General. Tolerances are estab- Horse, liver ...... 0 .50 lished for residues of the herbicide Sheep, kidney ...... 0.05 trifloxysulfuron, N-[[(4,6-dimethoxy-2- Sheep, liver ...... 0.50 pyrimidinyl)amino]carbonyl]-3-(2,2,2- (b) Section 18 emergency exemptions. trifluoroethoxy)-2-pyridinesulfonamide [Reserved] in or on the following raw agricultural (c) Tolerances with regional registra- commodities. tions. [Reserved] Parts per (d) Indirect and inadvertant residues. Commodity million [Reserved] Almond ...... 0.02 [68 FR 54827, Sept. 19, 2003] Almond, hulls ...... 0 .01 Fruit, citrus, Group 10 ...... 0.03 Cotton, undelinted seed ...... 0 .05 § 180.593 Etoxazole; tolerances for resi- Cotton, gin byproducts ...... 1 .0 dues. Sugarcane ...... 0 .01 (a) General. Tolerances are estab- Tomato ...... 0.01 lished for residues of etoxazole, includ- (b) Section 18 emergency exemptions. ing its metabolites and degradates, in [Reserved] or on the commodities in the table (c) Tolerances with regional registra- below. Compliance with the tolerance tions. [Reserved] levels specified below is to be deter- (d) Indirect or inadvertent residues. mined by measuring only etoxazole (2- [Reserved] (2,6-difluorophenyl)-4-[4-(1,1- dimethylethyl)-2-ethoxyphenyl]-4,5- [68 FR 54386, Sept. 17, 2003] dihydrooxazole) in or on the com- § 180.592 Butafenacil; tolerances for modity. residues. Commodity Parts per (a) General. (1) Tolerances are estab- million lished for residues of the herbicide Almond, hulls ...... 2 .0 butafenacil, (1,1-dimethyl-2-oxo-2-(2- Apple, wet pomace ...... 0 .50 propenyloxy)ethyl 2-chloro-5-[3,6- Avocado ...... 0 .20 Berry, low growing, subgroup 13–07G ...... 0 .50 dihydro-3-methyl-2,6-dioxo-4- Caneberry subgroup 13–07A ...... 1.5 (trifluoromethyl)-1(2H)-pyrimidinyl] Canistel ...... 0 .20 benzoate) in or on the following raw Cattle, fat ...... 0.02 agricultural commodities: Cattle, liver ...... 0 .01 Corn, field, forage ...... 0 .80 Corn, field, grain ...... 0 .01 Parts per Commodity million Corn, field, refined oil ...... 0 .03 Corn, field, stover ...... 4 .0 Cotton, gin byproducts ...... 10 Corn, pop, grain ...... 0.01 Cotton, undelinted seed ...... 0 .50 Corn, pop, stover ...... 4.0 Cotton, gin byproducts ...... 1 .0 Cotton, undelinted seed ...... 0 .05 (2) Tolerances are established for res- Fruit, pome, group 11 ...... 0.20 idues of the herbicide butafenacil, (1,1- Fruit, small vine climbing, except fuzzy kiwifruit, dimethyl-2-oxo-2-(2-propenyloxy)ethyl subgroup 13–07F ...... 0 .50 2-chloro-5-[3,6-dihydro-3-methyl-2,6- Fruit, stone, group 12, except plum ...... 1 .0 Goat, fat ...... 0 .02 dioxo-4-(trifluoromethyl)-1(2H)- Goat, liver ...... 0.01 pyrimidinyl] benzoate) and its metabo- Grape, raisin ...... 1 .5 lite CGA-293731 (1-carboxy-1- Hop, dried cones ...... 7 .0 Horse, fat ...... 0 .02 methylethyl 2-chloro-5-[3,6-dihydro-3- Horse, liver ...... 0 .01 methyl-2,6-dioxo-4-(trifluoromethyl)- Mango ...... 0.20

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Parts per Parts per Commodity million Commodity million

Melon subgroup 9A ...... 0 .20 Goat, liver ...... 0.15 Milk, fat ...... 0 .01 Goat, meat ...... 0.030 Nut, tree, group 14 ...... 0 .01 Goat, meat byproducts ...... 0 .050 Papaya ...... 0 .20 Horse, fat ...... 0 .020 Pepper/eggplant subgroup 8–10B ...... 0 .20 Horse, kidney ...... 0 .050 Peppermint, oil ...... 20 Horse, liver ...... 0 .15 Peppermint, tops ...... 10 Horse, meat ...... 0 .030 Pistachio ...... 0.01 Horse, meat byproducts ...... 0 .050 Plum ...... 0 .15 Milk ...... 0.030 Plum, prune, dried ...... 0.30 Peach subgroup 12–12B ...... 0.5 Sapodilla ...... 0 .20 Pepper ...... 1 .0 Sapote, black ...... 0 .20 Plum subgroup 12–12C ...... 0 .05 Sapote, mamey ...... 0 .20 Sheep, fat ...... 0 .020 Sheep, fat ...... 0 .02 Sheep, kidney ...... 0.050 Sheep, liver ...... 0.01 Sheep, liver ...... 0.15 Spearmint, oil ...... 20 Sheep, meat ...... 0.030 Spearmint, tops ...... 10 Sheep, meat byproducts ...... 0 .050 Squash/cucumber subgroup 9B ...... 0.02 Star apple ...... 0 .20 (b) Section 18 emergency exemptions. Tangerine 1 ...... 0 .10 Tea, dried * ...... 15 [Reserved] Tomato ...... 0.20 (c) Tolerances with regional registra- 1There are no U.S. registrations for use of etoxazole on tions. [Reserved] tangerines as of September 26, 2003. (d) Indirect or inadvertent residues. * There are currently no U.S. registrations for tea as of April 13, 2011. [Reserved] (b) Section 18 emergency exemptions. [68 FR 55512, Sept. 26, 2003, as amended at 78 [Reserved] FR 8416, Feb. 6, 2013] (c) Tolerances with regional registra- § 180.595 Flufenpyr-ethyl; tolerances tions. [Reserved] for residues. (d) Indirect and inadvertant residues. [Reserved] (a) General. (1) Tolerances are estab- lished for residues of the herbicide, [68 FR 55493, Sept. 26, 2003, as amended at 70 flufenpyr-ethyl; acetic acid, [2-chloro- FR 41625, July 20, 2005; 72 FR 72963, Dec. 26, 4-fluoro-5-[5-methyl-6-oxo-4- 2007; 74 FR 25160, May 27, 2009; 76 FR 20542, (trifluoromethyl)-1-(6H)-pyridazinyl]- Apr. 13, 2011; 77 FR 3621, Jan. 25, 2012] phenoxy]-ethyl ester], in or on the fol- § 180.594 Thiacloprid; tolerances for lowing commodities: residues. Parts per (a) General. Tolerances are estab- Commodity million lished for residues of the insecticide Corn, field, grain ...... 0 .01 thiacloprid, including its metabolites Soybean, seed ...... 0 .01 and degradates in or on the commod- Sugarcane, cane ...... 0.01 ities in the following table. Compliance with the tolerance levels specified in (2) Tolerances are established for res- the following table is to be determined idues of the herbicide flufenpyr-ethyl; by measuring only thiacloprid ([3-[(6- acetic acid, [2-chloro-4-fluoro-5-[5- chloro-3-pyridinyl)methyl]-2- methyl-6-oxo-4-(trifluoromethyl)-1- thiazolidinylidene] cyanamide) in or on (6H)-pyridazinyl]-phenoxy]-ethyl the commodity. ester], and its metabolite, S-3153 acid- 4-OH; [2-chloro-4-hydroxy-5-[5-methyl- Commodity Parts per 6- oxo-4-(trifluoromethyl)-1-(6H)- million pyridazinyl]-phenoxy]-acetic acid, free Apple, wet pomace ...... 0 .60 and conjugated, in or on the following Cattle, fat ...... 0.020 commodities: Cattle, kidney ...... 0 .050 Cattle, liver ...... 0 .15 Parts per Cattle, meat ...... 0 .030 Commodity million Cattle, meat byproducts ...... 0.050 Cherry subgroup 12–12A ...... 0 .5 Corn, field, forage ...... 0 .05 Cotton, gin byproducts ...... 11 .0 Corn, field, stover ...... 0 .05 Cotton, undelinted seed ...... 0 .020 Fruit, pome, group 11 ...... 0.30 Goat, fat ...... 0 .020 (b) Section 18 emergency exemptions. Goat, kidney ...... 0 .050 [Reserved]

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(c) Tolerances with regional registra- Commodity Parts per tions. [Reserved] million (d) Indirect or inadvertent residues. Wheat, straw ...... 0 .30 [Reserved] [68 FR 54842, Sept. 19, 2003] (b) Section 18 emergency exemptions. [Reserved] § 180.596 Fosthiazate; tolerances for (c) Tolerances with regional registra- residues. tions. [Reserved] (a) General. A tolerance is established (d) Indirect or inadvertent residues. for residues of the insecticide [Reserved] fosthiazate, including its metabolites [69 FR 18263, Apr. 7, 2004] and degradates, in or on the com- modity in the table in this paragraph. § 180.598 Novaluron; tolerances for Compliance with the tolerance level residues. specified in this paragraph is to be de- (a) General. Tolerances are estab- termined by measuring only the sum of lished for residues of the insecticide fosthiazate, O-ethyl S-(1- novaluron, including its metabolites methylpropyl)(2-oxo-3- and degradates, in or on the following thiazolidinyl)phosphonothioate, and its commodities. Compliance with the tol- metabolite, O-ethyl S-(1- erance levels specified in the following methylpropyl)(2- table is to be determined by measuring (methylsulfonyl)ethyl) only novaluron, (N-[[[3-chloro-4-[1,1,2- phosphoramidothioate, calculated as trifluoro-2- (trifluoromethoxy)ethoxy] the stoichiometric equivalent of phenyl]amino]carbonyl]-2,6- fosthiazate, in or on the commodity. difluorobenzamide), in or on the fol- lowing raw agricultural commodities: Parts per Commodity million Parts per Commodity million Tomato ...... 0.02 Apple, wet pomace ...... 8 .0 (b) Section 18 emergency exemptions. Bean, dry, seed ...... 0 .30 [Reserved] Bean, snap, succulent ...... 0 .60 (c) Tolerances with regional registra- Berry, low growing, subgroup 13-07G, except lowbush blueberry ...... 0 .45 tions. [Reserved] Brassica, head and stem, subgroup 5A ...... 0 .50 (d) Indirect or inadvertent residues. Brassica, leafy greens, subgroup 5B ...... 25 [Reserved] Bushberry subgroup 13-07B ...... 7 .0 Cattle, fat ...... 11 [69 FR 18275, Apr. 7, 2004, as amended at 76 Cattle, kidney ...... 1 .0 FR 23498, Apr. 27, 2011] Cattle, liver ...... 1 .0 Cattle, meat ...... 0 .60 Cattle, meat byproducts, except kidney and liver 11 § 180.597 Mesosulfuron-methyl; toler- Cherry ...... 8.0 ances for residues. Cocona ...... 1 .0 (a) General. Tolerances are estab- Corn, sweet, forage ...... 16 Corn, sweet, kernel plus cob with husks re- lished for residues of the herbicide moved ...... 0 .05 mesosulfuron-methyl, (methyl 2- Corn, sweet, stover ...... 50 [[[[(4,6-dimethoxy-2-pyrimidinyl) Cotton, gin byproducts ...... 30 amino]carbonyl]amino]sulfonyl] -4- Cotton, undelinted seed ...... 0 .60 Egg ...... 1 .5 [[(methylsulfonyl)amino] meth- Eggplant, African ...... 1 .0 yl]benzoate]) in or on the following raw Eggplant, pea ...... 1 .0 agricultural commodities: Eggplant, scarlet ...... 1 .0 Food commodities and feed commodities (other Parts per than those covered by a higher tolerance as a Commodity million result of use on growing crops) in food and feed handling establishments ...... 0 .01 Cattle, meat byproducts ...... 0.01 Fruit, pome, group 11 ...... 2.0 Goat, meat byproducts ...... 0 .01 Fruit, stone, group 12, except cherry ...... 1 .9 Grain, aspirated fractions ...... 0 .60 Goat, fat ...... 11 Horse, meat byproducts ...... 0 .01 Goat, kidney ...... 1 .0 Sheep, meat byproducts ...... 0 .01 Goat, liver ...... 1.0 Wheat, forage ...... 0 .60 Goat, meat ...... 0.60 Wheat, germ ...... 0 .10 Goat, meat byproducts, except kidney and liver 11 Wheat, grain ...... 0 .03 Goji berry ...... 1 .0 Wheat, hay ...... 0 .06 Grain, aspirated fractions ...... 25

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levels specified below is to be deter- Commodity Parts per million mined by measuring only the sum of Hog, fat ...... 1 .5 acequinocyl [2-(acetyloxy)-3-dodecyl- Hog, kidney ...... 0.10 1,4-naphthalenedione] and its metabo- Hog, liver ...... 0 .10 lite, 2-dodecyl-3-hydroxy-1,4- Hog, meat ...... 0 .07 Hog, meat byproducts, except kidney and liver .. 1 .5 naphthoquinone, calculated as the stoi- Horse, fat ...... 11 chiometric equivalent of acequinocyl, Horse, kidney ...... 1 .0 in or on the commodity. Horse, liver ...... 1 .0 Horse, meat ...... 0 .60 Parts per Horse, meat byproducts, except kidney and liver 11 Commodity million Huckleberry, garden ...... 1 .0 Martynia ...... 1 .0 Almond, hulls ...... 2 .0 Milk ...... 1.0 Apple, wet pomace ...... 1 .0 Milk, fat ...... 20 Bean, edible podded ...... 0 .25 Naranjilla ...... 1.0 Bean, succulent shelled ...... 0 .30 Okra ...... 1.0 Berry, low growing, subgroup 13–07G ...... 0 .50 Peanut ...... 0 .01 Caneberry subgroup 13–07A ...... 4.0 Plum, prune, dried ...... 2.6 Cattle, fat ...... 0.02 Poultry, fat ...... 7.0 Cattle, meat byproducts ...... 0.02 Poultry, kidney ...... 0 .80 Cherry, sweet ...... 0 .50 Poultry, liver ...... 0 .80 Cherry, tart ...... 1 .0 Poultry, meat ...... 0 .40 Citrus, oil ...... 30 Poultry, meat byproducts, except kidney and Cowpea, forage ...... 6 .0 liver ...... 7 .0 Cowpea, hay ...... 18 Roselle ...... 1 .0 Sheep, fat ...... 11 Cucumber ...... 0 .15 Sheep, kidney ...... 1.0 Fruit, citrus, group 10 ...... 0 .20 Sheep, liver ...... 1.0 Fruit, pome, group 11 ...... 0.40 Sheep, meat ...... 0.60 Fruit, small vine climbing, except fuzzy kiwifruit, Sheep, meat byproducts, except kidney and subgroup 13–07F ...... 1 .6 liver ...... 11 Goat, fat ...... 0 .02 Sorghum, grain, forage ...... 6.0 Goat, meat byproducts ...... 0 .02 Sorghum, grain, grain ...... 3 .0 Hop, dried cones ...... 4 .0 Sorghum, grain, stover ...... 40 Horse, fat ...... 0 .02 Soybean, seed ...... 0 .07 Horse, meat byproducts ...... 0 .02 Sugarcane, cane ...... 0.50 Melon subgroup 9A ...... 0 .15 Sunberry ...... 1.0 Nut, tree, group 14 ...... 0 .02 Swiss chard ...... 12 Okra ...... 0.70 Tomato, bush ...... 1 .0 Pistachio ...... 0.02 Tomato, currant ...... 1 .0 Sheep, fat ...... 0 .02 Tomato, tree ...... 1 .0 Sheep, meat byproducts ...... 0 .02 Turnip, greens ...... 25 Soybean, vegetable, succulent ...... 0 .25 Vegetable, cucurbit, group 9 ...... 0.15 Vegetable, fruiting, group 8 ...... 0.70 Vegetable, fruiting, group 8 ...... 1.0 Vegetable, tuberous and corm, subgroup 1C ..... 0.05 (b) Section 18 emergency exemptions. [Reserved] (b) Section 18 emergency exemptions. (c) Tolerances with regional registra- [Reserved] tions. [Reserved] (c) Tolerances with regional registra- (d) Indirect or inadvertent residues. tions. [Reserved] [Reserved] (d) Indirect or inadvertant residues. [Reserved] [69 FR 43533, July 21, 2004, as amended at 73 FR 17910, Apr. 2, 2008; 75 FR 70148, Nov. 17, [69 FR 31021, June 2, 2004, as amended at 71 2010; 77 FR 25909, May 2, 2012] FR 17014, Apr. 5, 2006; 71 FR 61911, Oct. 20, 2006; 73 FR 74982, Dec. 10, 2008; 74 FR 637, Jan. § 180.600 Propoxycarbazone; toler- 7, 2009; 74 FR 20891, May 6, 2009; 74 FR 65033, ances for residues. Dec. 9, 2009; 75 FR 4278, Jan. 27, 2010; 75 FR 29447, May 26, 2010; 76 FR 55814, Sept. 9, 2011; (a) General. (1) Tolerances are estab- 78 FR 40033, July 3, 2013] lished for combined residues of the her- bicide propoxycarbazone methyl 2- § 180.599 Acequinocyl; tolerances for [[[(4,5-dihydro-4-methyl-5-oxo-3- residues. propoxy-1H-1,2,4-triazol-1- (a) General. Tolerances are estab- yl)carbonyl]amino]sulfonyl]benzoate lished for residues of acequinocyl, in- and its metabolite methyl 2-[[[(4,5- cluding its metabolites and degradates, dihydro-3-(2-hydroxypropoxy)-4-meth- in or on the commodities in the table yl-5-oxo-1H-1,2,4-triazol-1- below. Compliance with the tolerance yl)carbonyl]amino]sulfonyl]benzoate

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in/on the following raw agricultural Commodity Parts per commodities: million Basil, dried leaves ...... 90 Parts per Commodity million Basil, fresh leaves ...... 30 Bean, succulent ...... 0 .5 Grass, forage ...... 20 Bean, succulent shelled ...... 0 .08 Grass, hay ...... 25 Brassica, head and stem, subgroup 5A ...... 1 .2 Wheat, forage ...... 17 Brassica, leafy greens, subgroup 5B ...... 12 .0 Wheat, grain ...... 0 .02 Carrot, roots ...... 0.09 Wheat, hay ...... 0 .15 Hop dried cones ...... 10.0 Wheat, straw ...... 0 .05 Leafy greens subgroup 4A ...... 10 Turnip, greens ...... 12.0 (2) Tolerances are established for res- Vegetable, cucurbit, group 9 ...... 0.10 idues of the herbicide Vegetable, fruiting, group 8–10 ...... 0 .9 Vegetable, tuberous and corm, subgroup 1C ..... 0.02 propoxycarbazone methyl 2-[[[(4,5- dihydro-4-methyl-5-oxo-3-propoxy-1H- (b) Section 18 emergency exemptions. 1,2,4-triazol-1- Time-limited tolerances are estab- yl)carbonyl]amino]sulfonyl]benzoate lished for residues of the fungicide in/on the following raw agricultural cyazofamid, including its metabolites commodities: and degradates, in or on the commod- ities in the following table. Compliance Commodity Parts per million with the tolerance levels specified in Cattle, meat ...... 0 .05 the following table is to be determined Cattle, meat byproducts ...... 0.3 by measuring only the sum of Goat, meat ...... 0.05 cyazofamid, 4-chloro-2-cyano-N,N-di- Goat, meat byproducts ...... 0 .3 methyl-5-(4-methylphenyl)-1H-imid- Horse, meat ...... 0 .05 azole-1-sulfonamide and its metabolite Horse, meat byproducts ...... 0 .3 Milk ...... 0.03 CCIM, 4-chloro-5-(4-methylphenyl)-1H- Sheep, meat ...... 0.05 imidazole-2-carbonitrile, calculated as Sheep, meat byproducts ...... 0 .3 the stoichiometric equivalent of cyazofamid, resulting from use of the (b) Section 18 emergency exemptions. pesticide under FIFRA section 18 emer- [Reserved] gency exemptions. The tolerances ex- (c) Tolerances with regional registra- pire and are revoked on the date speci- tions. [Reserved] fied in the table. (d) Indirect or inadvertent residues. [Reserved] Parts per Expiration/ Commodity million revocation [69 FR 40781, July 7, 2004, as amended at 71 date FR 52487, Sept. 6, 2006; 74 FR 9377, Mar. 4, Basil, dried ...... 144 12/31/14 2009] (c) Tolerances with regional registra- § 180.601 Cyazofamid; tolerances for residues. tions. Tolerances with regional reg- istrations are established for residues (a) General. Tolerances are estab- of the fungicide cyazofamid, including lished for residues of the fungicide its metabolites and degradates, in or cyazofamid, including its metabolites on the commodities in the following and degradates, in or on the commod- table. Compliance with the tolerance ities in the following table. Compliance levels specified in the following table is with the tolerance levels specified in to be determined by measuring only the following table is to be determined the sum of 4-chloro-2-cyano-N,N-di- by measuring only the sum of 4-chloro- 2-cyano-N,N-dimethyl-5-(4- methyl-5-(4-methylphenyl)-1H-imid- methylphenyl)-1H-imidazole-1-sul- azole-1-sulfonamide and its metabolite, fonamide and its metabolite, 4-chloro- 4-chloro-5-(4-methylphenyl)-1H-imid- 5-(4-methylphenyl)-1H-imidazole-2- azole-2-carbonitrile, calculated as the carbonitrile, calculated as the stoichio- stoichiometric equivalent of metric equivalent of cyazofamid, in or cyazofamid, in or on the following on the following commodities: commodities:

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furylmethyl)urea, calculated as the Commodity Parts per million stoichiometric equivalent of Grape ...... 1 .5 dinotefuran, in or on the commodities listed in the table below: (d) Indirect or inadvertent residues. Parts per [Reserved] Commodity million

[69 FR 58299, Sept. 30, 2004, as amended at 73 Berry, low growing, except strawberry, subgroup FR 21839, Apr. 23, 2008; 74 FR 32453, July 8, 13–07H ...... 0 .2 2009; 75 FR 40751, July 14, 2010; 77 FR 4252, Brassica, head and stem, subgroup 5A ...... 1 .4 Jan. 27, 2012; 77 FR 59119, Sept. 26, 2012] Brassica, leafy greens, subgroup 5B ...... 15 .0 Cotton, undelinted seed ...... 0 .4 Cotton, gin byproducts ...... 8 .0 § 180.602 Spiroxamine; tolerances for Fruit, small vine climbing, except fuzzy kiwifruit, residues. subgroup 13–07F ...... 0 .9 (a) General. Tolerances are estab- Grape, raisin ...... 2 .5 Onion, bulb, subgroup 3–07A ...... 0 .15 lished for residues of the fungicide Onion, green, subgroup 3–07B ...... 5 .0 spiroxamine, including its metabolites Peach ...... 1 .0 and degradates, in or on the commod- Potato, chips ...... 0 .1 Potato, granules/flakes ...... 0 .15 ities in the table below. Compliance Rice, grain ...... 9 .0 with the tolerance levels specified in Tea, dried1 ...... 50 the following table is to be determined Tomato, paste ...... 1 .0 Turnip, greens ...... 15.0 by measuring only spiroxamine, [(8- Vegetable, fruiting, group 8 ...... 0.7 (1,1-dimethylethyl)-N-ethyl-N-propyl- Vegetable, cucurbit, group 9 ...... 0.5 1,4-dioxaspiro[4,5]decane-2- Vegetable, leafy, except Brassica, group 4 ...... 5 .0 methanamine) in or on the commod- Vegetable, tuberous and corm, subgroup 1C ..... 0.05 Watercress ...... 8 .0 ities. 1 There are no U.S. registrations for tea. Parts per Commodity million (2) Tolerances are established for res- idues of dinotefuran, (RS)-1-methyl-2- Artichoke, globe, import 1 ...... 0 .7 nitro-3-((tetrahydro-3- Asparagus 1 ...... 0.05 Banana (import) ...... 3 .0 furanyl)methyl)guanidine, including Grape (import) ...... 1 .0 its metabolites and degradates, in or Hop, dried cones ...... 50 on the commodities listed in the fol- Vegetable, fruiting , crop group 8 1 ...... 1 .2 lowing table. Compliance with the tol- 1 No U.S. registration as of December 1, 2010. erance levels specified below is to be (b) Section 18 emergency exemptions. determined by measuring only the sum [Reserved] of dinotefuran, (RS)-1-methyl-2-nitro-3- (c) Tolerances with regional registra- ((tetrahydro-3- tions. [Reserved] furanyl)methyl)guanidine in or on the (d) Indirect or inadvertent residues. commodities listed in the table below: [Reserved] Parts per Commodity million [69 FR 42570, July 16, 2004, as amended at 75 FR 74640, Dec. 1, 2010] Cattle, fat ...... 0.05 Cattle, meat ...... 0 .05 § 180.603 Dinotefuran; tolerances for Cattle, meat byproducts ...... 0.05 residues. Egg ...... 0 .01 Goat, fat ...... 0 .05 (a) General. (1) Tolerances are estab- Goat, meat ...... 0.05 lished for residues of dinotefuran, (RS)- Goat, meat byproducts ...... 0 .05 Hog, fat ...... 0 .05 1-methyl-2-nitro-3-((tetrahydro-3- Hog, meat ...... 0 .05 furanyl)methyl)guanidine, including Hog, meat byproducts ...... 0 .05 its metabolites and degradates, in or Horse, fat ...... 0 .05 Horse, meat ...... 0 .05 on the commodities listed in the fol- Horse, meat byproducts ...... 0 .05 lowing table. Compliance with the tol- Milk ...... 0.05 erance levels specified below is to be Poultry, meat byproducts ...... 0.01 Sheep, fat ...... 0 .05 determined by measuring only the sum Sheep, meat ...... 0.05 of dinotefuran and its metabolites DN, Sheep, meat byproducts ...... 0 .05 1-methyl-3-(tetrahydro-3- furylmethyl)guanidine, and UF, 1- (3) A tolerance of 0.01 parts per mil- methyl-3-(tetrahydro-3- lion is established for residues of the

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insecticide dinotefuran, (RS)-1-methyl- (c) Tolerances with regional registra- 2-nitro-3-((tetrahydro-3- tions. [Reserved] furanyl)methyl)guanidine, including (d) Indirect of inadvertent residues. its metabolites and degradates, in or [Reserved] on all food and/or feed commodities (e) Revoked tolerances subject to the (other than those covered by a higher channel of trade provisions. [Reserved] tolerance as a result of use on growing (f) Import tolerances. Tolerances are crops or inadvertent residues) when established for the combined residues residues result from application of of mepanipyrim, 4-methyl-N-phenyl-6- dinotefuran in food and/or feed han- (1-propynyl)-2-pyrimidinamine, and its dling establishments where food and/or metabolite, 4-methyl-N-phenyl-6-(2- feed products are held, stored, proc- hydroxypropylk)-2-pyrimidinamine, essed, prepared, or served. Compliance both free and conjugated in or on the with the tolerance level is to be deter- following commodities: mined by measuring only dinotefuran. Parts per (b) Section 18 emergency exemptions. Commodity million Time-limited tolerances are estab- lished for residues of dinotefuran, (RS)- Grape ...... 1 .5 Grape, raisin ...... 3 .0 1-methyl-2-nitro-3-((tetrahydro-3- Strawberry ...... 1 .5 furanyl)methyl)guanidine, including Tomato ...... 0.5 its metabolites and degradates, in or on the commodities in the table below [68 FR 60827, Oct. 13, 2004] resulting from use of the pesticide pur- suant to FIFRA section 18 emergency § 180.605 Penoxsulam; tolerances for exemptions. Compliance with the toler- residues. ance levels specified below is to be de- (a) General. Tolerances are estab- termined by measuring only the sum of lished for the herbicide, penoxsulam (2- dinotefuran and its metabolites DN, 1- (2,2-difluoroethoxy)-N-(5,8- methyl-3-(tetrahydro-3- dimethoxy[1,2,4] triazolo[1,5- furylmethyl)guanidine, and UF, 1- c]pyrimidin-2-yl)-6- methyl-3-(tetrahydro-3- (trifluoromethyl)benzenesulfonamide) furylmethyl)urea, calculated as the in/on the following raw agricultural stoichiometric equivalent of commodities: dinotefuran, in or on the commodities Parts per listed in the table below. The toler- Commodity million ances expire and are revoked on the dates specified in the table. Almond, hulls ...... 0 .01 Fish ...... 0 .01 Expiration/ Fish, shellfish, crustacean ...... 0 .01 Commodity Parts per revocation Fish, shellfish, mollusc ...... 0 .02 million date Grape ...... 0 .01 Nut, tree, group 14 ...... 0 .01 Fruit, pome, Group 11 ...... 2.0 12/31/15 Pistachio ...... 0.01 Fruit, stone, Group 12 ...... 2.0 12/31/15 Rice, grain ...... 0 .02 Rice, straw ...... 0 .50 (c) Tolerances with regional registra- tions. [Reserved] (b) Section 18 emergency exemptions. (d) Indirect or inadvertent residues. [Reserved] [Reserved] (c) Tolerances with regional registra- tions. [Reserved] [70 FR 14546, Mar. 23, 2005, as amended at 74 (d) Indirect or inadvertent residues. FR 12601, Mar. 25, 2009; 74 FR 67104, Dec. 18, [Reserved] 2009; 75 FR 770, Jan. 6, 2010; 77 FR 56138, Sept. 12, 2012; 77 FR 67285, Nov. 9, 2012; 77 FR 70913, [69 FR 57197, Sept. 24, 2004, as amended at 72 Nov. 28, 2012; 78 FR 21272, Apr. 10, 2013; 78 FR FR 40763, July 25, 2007; 74 FR 18648, Apr. 24, 24683, Apr. 26, 2013; 79 FR 3512, Jan. 22, 2014] 2009]

§ 180.604 Mepanipyrim; tolerances for § 180.607 Spiromesifen; tolerances for residues. residues. (a) General. [Reserved] (a) General. (1) Tolerances are estab- (b) Section 18 emergency exemptions. lished for residues of the insecticide/ [Reserved] miticide spiromesifen, including its

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metabolites and degradates, in or on Commodity Parts per the commodities listed below. Compli- million ance with the tolerance levels specified Cattle, fat ...... 0.10 below is to be determined by measuring Cattle, meat ...... 0 .02 only the sum of spiromesifen [2-oxo-3- Cattle, meat byproducts ...... 0.20 Goat, fat ...... 0 .10 (2,4,6-trimethylphenyl)-1- Goat, meat ...... 0.02 oxaspiro[4.4]non-3-en-4-yl 3,3- Goat, meat byproducts ...... 0 .20 dimethylbutanoate] and 4-hydroxy-3- Horse, fat ...... 0 .10 Horse, meat ...... 0 .02 (2,4,6-trimethylphenyl)-1- Horse, meat byproducts ...... 0 .20 oxaspiro[4.4]non-3-en-2-one, calculated Milk ...... 0.01 as the stoichiometric equivalent of Milk, fat ...... 0 .25 spiromesifen, in or on the following Sheep, fat ...... 0 .10 Sheep, meat ...... 0.02 primary crop commodities: Sheep, meat byproducts ...... 0 .20

Parts per Commodity million (b) Section 18 emergency exemptions. Time-limited tolerances specified in Bean, dry ...... 0.02 the following table are established for Bean, edible podded ...... 0 .80 Bean, succulent ...... 0 .10 residues of the insecticide/miticide Berry and small fruit, low growing berry, sub- spiromesifen, including its metabolites group 13-07G ...... 2 .0 and degradates, in or on the commod- Brassica, head and stem, subgroup 5A ...... 2 .0 Brassica, leafy greens, subgroup 5B ...... 12 ities listed below. Compliance with the Corn, field, forage ...... 5 .0 tolerance levels specified below is to be Corn, field, grain ...... 0 .02 determined by measuring only the sum Corn, field, stover ...... 8 .0 Corn, pop, grain ...... 0.02 of spiromesifen [2-oxo-3-(2,4,6- Corn, pop, stover ...... 4.0 trimethylphenyl)-1-oxaspiro[4.4]non-3- Corn, sweet, forage ...... 17 en-4-yl 3,3-dimethylbutanoate] and 4- Corn, sweet, kernel plus cob with husks re- hydroxy-3-(2,4,6-trimethylphenyl)-1- moved ...... 0 .02 Corn, sweet, stover ...... 12 oxaspiro[4.4]non-3-en-2-one, calculated Cotton, gin byproducts ...... 15 as the stoichiometric equivalent of Cotton, undelinted seed ...... 0 .50 spiromesifen, in or on the specified ag- Cowpea, forage ...... 30 Cowpea, hay ...... 86 ricultural commodities, resulting from Leaf petiole subgroup 4B ...... 6 .0 use of the pesticide pursuant to FIFRA Leafy greens subgroup 4A ...... 12 section 18 emergency exemptions. The Pea, dry, seed ...... 0 .20 Peppermint, tops ...... 45 tolerances expire and are revoked on Spearmint, tops ...... 45 the date specified in the table. Tea, dry ...... 40 Tomato, paste ...... 0 .80 Parts per Expiration/ Vegetable, cucurbit, group 9 ...... 0.10 Commodity million revocation Vegetable, fruiting, group 8 ...... 0.45 date Vegetable, tuberous and corm, subgroup 1C ..... 0.02 Soybean, forage ...... 30 12/31/14 Soybean, hay ...... 86 12/31/14 (2) Tolerances are established for res- Soybean, seed ...... 0.02 12/31/14 idues of the insecticide/miticide spiromesifen, including its metabolites (c) Tolerances with regional registra- and degradates, in or on the commod- tions. [Reserved] ities listed below. Compliance with the (d) Indirect or inadvertent residues. tolerance levels specified below is to be Tolerances are established for the inad- determined by measuring only the sum vertent or indirect residues of the in- of spiromesifen [2-oxo-3-(2,4,6- secticide/miticide spiromesifen, includ- trimethylphenyl)-1-oxaspiro[4.4]non-3- ing its metabolites and degradates, in en-4-yl 3,3-dimethylbutanoate] and its or on the commodities listed below. metabolites containing the 4-hydroxy- Compliance with the tolerance levels 3-(2,4,6-trimethylphenyl)-1- specified below is to be determined by oxaspiro[4.4]non-3-en-2-one and 4-hy- measuring only the sum of droxy-3-[4-(hydroxymethyl)-2,6- spiromesifen [2-oxo-3-(2,4,6- dimethylphenyl]-1-oxaspiro[4.4]non-3- trimethylphenyl)-1-oxaspiro[4.4]non-3- en-2-one moieties, calculated as the en-4-yl 3,3-dimethylbutanoate], 4-hy- stoichiometric equivalent of droxy-3-(2,4,6-trimethylphenyl)-1- spiromesifen, in the following livestock oxaspiro[4.4]non-3-en-2-one, and its me- commodities: tabolites containing the 4-hydroxy-3-[4-

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(hydroxymethyl)-2,6-dimethylphenyl]- (2) Tolerances are established for res- 1-oxaspiro[4.4]non-3-en-2-one moiety, idues of spirodiclofen, including its me- calculated as the stoichiometric equiv- tabolites and degradates, in or on the alent of spiromesifen, in the following commodities listed below. Compliance rotational crop commodities: with the following tolerance levels is to be determined by measuring only Parts per Commodity million spirodiclofen (3-(2,4-dichlorophenyl)-2- oxo-1-oxaspiro[4.5]dec-3-en-4-yl 2,2- Alfalfa, forage ...... 1.5 dimethylbutanoate) and its metabolite Alfalfa, hay ...... 3.0 Barley, grain ...... 0 .03 3-(2,4-dichlorophenyl)-4-hydroxy-1- Barley, hay ...... 0 .25 oxaspiro[4,5] dec-3-en-2-one, calculated Barley, straw ...... 0 .15 as the stoichiometric equivalent of Beet, sugar, roots ...... 0 .03 Beet, sugar, tops ...... 0.20 spirodiclofen. Oat, forage ...... 0 .20 Oat, grain ...... 0 .03 Commodity Parts per Oat, hay ...... 0.25 million Oat, straw ...... 0.25 Vegetable, bulb, group 3-07 ...... 0 .09 Cattle, fat ...... 0.02 Wheat, forage ...... 0 .20 Cattle, meat byproducts ...... 0.10 Wheat, grain ...... 0 .03 Cattle, meat ...... 0 .02 Wheat, hay ...... 0 .15 Goat, fat ...... 0 .02 Wheat, straw ...... 0 .25 Goat, meat byproducts ...... 0 .1 Goat, meat ...... 0.02 [70 FR 43283, July 27, 2005, as amended at 72 Horse, fat ...... 0 .02 FR 3079, Jan. 24, 2007; 73 FR 13140, Mar. 12, Horse, meat byproducts ...... 0 .1 2008; 73 FR 52606, Sept. 10, 2008; 74 FR 8492, Horse, meat ...... 0 .02 Milk ...... 0.01 Feb. 25, 2009; 74 FR 15886, Apr. 8, 2009; 75 FR Milk, fat ...... 0 .03 5526, Feb. 3, 2010; 75 FR 53586, Sept. 1, 2010; 76 Sheep, fat ...... 0 .02 FR 81396, Dec. 28, 2011; 78 FR 3337, Jan. 16, Sheep. meat byproducts ...... 0 .1 2013] Sheep. meat ...... 0.02

§ 180.608 Spirodiclofen; tolerances for (b) Section 18 emergency exemptions. residues. [Reserved] (a) General. (1) Tolerances are estab- (c) Tolerances with regional registra- lished for residues of spirodiclofen, in- tions. [Reserved] cluding its metabolites and degradates, (d) Indirect or inadvertent residues. in or on the commodities listed below. [Reserved] Compliance with the following toler- ance levels is to be determined by [70 FR 40211, July 13, 2005, as amended at 73 measuring only spirodiclofen (3-(2,4- FR 25539, May 7, 2008; 75 FR 24434, May 5, dichlorophenyl)-2-oxo-1- 2010; 77 FR 73939, Dec. 12, 2012; 79 FR 33464, June 11, 2014] oxaspiro[4.5]dec-3-en-4-yl 2,2- dimethylbutanoate). § 180.609 Fluoxastrobin; tolerances for residues. Commodity Parts per million (a) General. (1) Tolerances are estab- Almond, hulls ...... 20 .0 lished for residues of fluoxastrobin, in- Apple, wet pomace ...... 2 .4 cluding its metabolites and degradates, Avocado ...... 1 .0 in or on the commodities in the table Black sapote ...... 1 .0 Canistel ...... 1 .0 below. Compliance with the tolerance Citrus, juice ...... 0 .60 levels specified below is to be deter- Citrus, oil ...... 35 mined by measuring only Fruit, citrus, group 10 ...... 0 .50 Fruit, pome, group 11 ...... 0.80 fluoxastrobin, (1E)-[2-[[6-(2- Fruit, stone, group 12 ...... 1 .0 chlorophenoxy)-5-fluoro-4- Grape ...... 2 .0 pyrimidinyl]oxy]phenyl](5,6-dihydro- Grape, raisin ...... 6 .0 Hop, dried cones ...... 30 1,4,2-dioxazin-3-yl)methanone O- Mamey sapote ...... 1 .0 methyloxime and its Z isomer, (1Z)-[2- Mango ...... 1.0 [[6-(2-chlorophenoxy)-5-fluoro-4- Nut, tree, group 14 ...... 0 .10 Papaya ...... 1 .0 pyrimidinyl]oxy]phenyl](5,6-dihydro- Pistachio ...... 0.10 1,4,2-dioxazin-3-yl)methanone O- Sapodilla ...... 1 .0 methyloxime, calculated as the stoi- Star apple ...... 1 .0 chiometric equivalent of fluoxastrobin.

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Parts per Parts per Commodity million Commodity million

Berry, low growing, subgroup 13-07G ...... 1 .9 Sheep, fat ...... 0 .10 Corn, field, forage ...... 3 .0 Sheep, meat ...... 0.05 Corn, field, grain ...... 0 .02 Sheep, meat byproducts ...... 0 .20 Corn, field, stover ...... 4 .5 Corn, sweet, forage ...... 13 (b) Section 18 emergency exemptions. Corn, sweet, kernel plus cob with husks re- moved ...... 0 .01 [Reserved] Corn, sweet, stover ...... 10 (c) Tolerances with regional registra- Grain, aspirated grain fractions ...... 60 tions. [Reserved] Leaf petioles subgroup 4B ...... 4 .0 Melon subgroup 9A ...... 1 .5 (d) Indirect or inadvertent residues. Peanut ...... 0 .02 Tolerances are established for the indi- Peanut, hay ...... 20.0 rect or inadvertent residues of Peanut, refined oil ...... 0.06 fluoxastrobin, including its metabo- Rice, grain ...... 4 .0 Sorghum, grain, forage ...... 5.0 lites and degradates, in or on the com- Sorghum, grain, grain ...... 1 .5 modities in the table below, when Sorghum, grain, stover ...... 5 .0 present therein as a result of the appli- Soybean, forage ...... 9 .0 Soybean, hay ...... 1 .2 cation of fluoxastrobin to the growing Soybean, hulls ...... 0 .20 crops listed in paragraph (a)(1) of this Soybean, seed ...... 0 .05 section. Compliance with the tolerance Squash/cucumber subgroup 9B ...... 0.50 levels specified below is to be deter- Tomato, paste ...... 1 .5 Vegetable, fruiting, group 8 ...... 1.0 mined by measuring only Vegetable, tuberous and corm, subgroup 1C ... 0.010 fluoxastrobin, (1E)-[2-[[6-(2- Wheat, forage ...... 7 .0 chlorophenoxy)-5-fluoro-4- Wheat, grain ...... 0 .15 Wheat, hay ...... 17 pyrimidinyl]oxy]phenyl](5,6-dihydro- Wheat, straw ...... 11 1,4,2-dioxazin-3-yl)methanone O- methyloxime and its Z isomer, (1Z)-[2- (2) Tolerances are established for res- [[6-(2-chlorophenoxy)-5-fluoro-4- idues of fluoxastrobin, including its pyrimidinyl]oxy]phenyl](5,6-dihydro- metabolites and degradates, in or on 1,4,2-dioxazin-3-yl)methanone O- the commodities in the table below. methyloxime, calculated as the stoi- Compliance with the tolerance levels chiometric equivalent of fluoxastrobin. specified below is to be determined by Parts per measuring only fluoxastrobin, (1E)-[2- Commodity million [[6-(2-chlorophenoxy)-5-fluoro-4- pyrimidinyl]oxy]phenyl](5,6-dihydro- Alfalfa, forage ...... 0.050 Alfalfa, hay ...... 0.10 1,4,2-dioxazin-3-yl)methanone O- Cotton, gin byproducts ...... 0 .020 methyloxime, its Z isomer, (1Z)-[2-[[6- Grain, cereal, forage, fodder, and straw, group (2-chlorophenoxy)-5-fluoro-4- 16, except corn ...... 0.10 Grass, forage ...... 0 .10 pyrimidinyl]oxy]phenyl](5,6-dihydro- Grass, hay ...... 0 .50 1,4,2-dioxazin-3-yl)methanone O- Vegetable, foliage of legume, group 7 ...... 0 .050 methyloxime, and its phenoxy- hydroxypyrimidine, 6-(2- [74 FR 67113, Dec. 18, 2009, as amended at 75 chlorophenoxy)-5-fluoro-4-pyrimidinol, FR 60333, Sept. 30, 2010; 76 FR 50898, Aug. 17, calculated as the stoichiometric equiv- 2011; 77 FR 26471, May 4, 2012; 77 FR 64915, alent of fluoxastrobin. Oct. 24, 2012; 79 FR 20105, Apr. 11, 2014; 79 FR 59119, Oct. 1, 2014] Commodity Parts per million § 180.610 Aminopyralid; tolerances for Cattle, fat ...... 0.10 residues. Cattle, meat ...... 0 .05 (a) General. (1) Tolerances are estab- Cattle, meat byproducts ...... 0.20 lished for residues of the herbicide Goat, fat ...... 0 .10 Goat, meat ...... 0.05 aminopyralid, 4-amino-3,6-dichloro-2- Goat, meat byproducts ...... 0 .20 pyridinecarboxylic acid, including its Hog, fat ...... 0 .03 metabolites and degradates, in or on Hog, meat byproducts ...... 0 .06 Horse, fat ...... 0 .10 the commodities in the table below. Horse, meat ...... 0 .05 Compliance with the tolerance levels Horse, meat byproducts ...... 0 .20 specified below is to be determined by Milk ...... 0.03 Milk, fat ...... 0 .75 measuring only free and conjugated Poultry, liver ...... 0 .06 aminopyralid.

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diethyl-4-hydroxymethyl-phenyl)- Commodity Parts per million tetrahydro-pyrazolo[1,2-d][1,4,5] Corn, field, forage ...... 0 .30 oxadiazepine-7,9-dione (M4), and 4-(7,9- Corn, field, grain ...... 0 .20 dioxo-hexahydro-pyrazolo[1,2-d] Corn, field, stover ...... 0 .20 [1,4,5]oxadiazepin-8-yl)-3,5-diethyl-ben- Grain, aspirated fractions ...... 0 .2 Grass, forage ...... 25 zoic acid (M6), calculated as pinoxaden, Grass, hay ...... 50 in/on the following commodities: Wheat, bran ...... 0.1 Wheat, forage ...... 2 .0 Commodity Parts per Wheat, grain ...... 0 .04 million Wheat, hay ...... 4 .0 Wheat, straw ...... 0 .25 Barley, bran ...... 1 .6 Barley, grain ...... 0 .9 Barley, hay ...... 1 .5 (2) Tolerances are established for res- Barley, straw ...... 1 .0 idues of the herbicide aminopyralid, 4- Egg ...... 0 .06 amino-3,6-dichloro-2- Poultry, fat ...... 0.06 Poultry, meat ...... 0 .06 pyridinecarboxylic acid, including its Poultry, meat byproducts ...... 0.06 metabolites and degradates, in or on Wheat, bran ...... 3.0 the commodities in the table below. Wheat, forage ...... 3 .5 Wheat, grain ...... 1 .3 Compliance with the tolerance levels Wheat, hay ...... 2 .0 specified below is to be determined by Wheat, straw ...... 1 .5 measuring only aminopyralid. (2) For the combined residues of Parts per Commodity million pinoxaden, 8-(2,6-diethyl-4- methylphenyl)-1,2,4,5-tetrahydro-7-oxo- Cattle, fat ...... 0.02 7H-pyrazolo[1,2-d][1,4,5] oxadiazepin-9- Cattle, kidney ...... 0 .3 Cattle, meat ...... 0 .02 yl 2,2-dimethylpropanoate), and its me- Cattle, meat byproducts, except kidney ...... 0.02 tabolites M2, 8-(2,6-diethyl-4-methyl- Goat, fat ...... 0 .02 phenyl)-tetrahydro-pyrazolo[1,2- Goat, kidney ...... 0 .3 d][1,4,5]oxadiazepine-7,9-dione, and free Goat, meat ...... 0.02 Goat, meat byproducts, except kidney ...... 0 .02 and conjugated forms of M4, 8-(2,6- Horse, fat ...... 0 .02 diethyl-4-hydroxymethyl-phenyl)- Horse, kidney ...... 0 .3 tetrahydro-pyrazolo[1,2-d][1,4,5] Horse, meat ...... 0 .02 Horse, meat byproducts, except kidney ...... 0 .02 oxadiazepine-7,9-dione, calculated as Milk ...... 0.03 pinoxaden, in/on the following com- Sheep, fat ...... 0 .02 modities: Sheep, kidney ...... 0.3 Sheep, meat ...... 0.02 Parts per Sheep, meat byproducts, except kidney ...... 0 .02 Commodity million (b) Section 18 emergency exemptions. Cattle, fat ...... 0.04 Cattle, meat ...... 0 .04 [Reserved] Cattle, meat byproducts ...... 0.04 (c) Tolerances with regional registra- Milk ...... 0.02 tions. [Reserved] (d) Indirect or inadvertent residues. (b) Section 18 emergency exemptions. [Reserved] [Reserved] (c) Tolerances with regional registra- [70 FR 46428, Aug. 10, 2005, as amended at 75 FR 17584, Apr. 7, 2010] tions. [Reserved] (d) Indirect or inadvertent residues. § 180.611 Pinoxaden; tolerances for [Reserved] residues. [70 FR 43322, July 27, 2005] (a) General. (1) Tolerances are estab- lished for the combined residues of § 180.612 Topramezone; tolerances for pinoxaden (8-(2,6-diethyl-4- residues. methylphenyl)-1,2,4,5-tetrahydro-7-oxo- (a) General. Tolerances are estab- 7H-pyrazolo[1,2-d][1,4,5] oxadiazepin-9- lished for residues of the herbicide yl 2,2-dimethylpropanoate), and its me- topramezone, including its metabolites tabolites 8-(2,6-diethyl-4-methyl- and degradates, in or on the following phenyl)-tetrahydro-pyrazolo[1,2- commodities. Compliance with the fol- d][1,4,5]oxadiazepine-7,9-dione (M2), and lowing tolerance levels is to be deter- free and conjugated forms of 8-(2,6- mined by measuring only topramezone

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([3-(4,5-dihydro-3-isoxazolyl)-2-methyl- Commodity Parts per 4-(methylsulfonyl)phenyl](5-hydroxy-1- million methyl-1H-pyrazol-4-yl)methanone) in Cotton, gin byproducts ...... 6 .0 or on the following commodities: Cotton, hulls ...... 2 .0 Cotton, meal ...... 1 .0 Parts per Cotton, undelinted seed ...... 0 .50 Commodity million Cucumber ...... 1 .5 Fruit, pome, group 11–10 ...... 0 .20 Cattle, meat byproducts ...... 0.80 Fruit, stone, group 12–12 ...... 0 .60 Corn, field, forage ...... 0 .05 Hop, dried cones ...... 7 .0 Corn, field, grain ...... 0 .01 Nut, tree, group 14–12 ...... 0 .15 Corn, field, stover ...... 0 .05 Okra ...... 0.40 Corn, pop, grain ...... 0.01 Peppermint, tops ...... 7 .0 Corn, pop, stover ...... 0.05 Potato, granules/flakes ...... 0 .40 Corn, sweet, forage ...... 0 .05 Radish, tops ...... 16 Corn, sweet, kernel plus cob with husks re- Rapeseed subgroup 20A ...... 1 .5 moved ...... 0 .01 Spearmint, tops ...... 7 .0 Corn, sweet, stover ...... 0 .05 Spinach ...... 9 .0 Fish-freshwater finfish ...... 0.05 Tomato, paste ...... 2 .0 Fish-saltwater finfish ...... 0 .05 Tomato, puree ...... 0 .50 Fish-shellfish, crustacean ...... 0 .05 Turnip, greens ...... 16 Fish-shellfish, mollusk ...... 0 .05 Vegetable, cucurbit, group 9 ...... 1.5 Goat, meat byproducts ...... 0 .80 Vegetable, fruiting, group 8–10 ...... 0 .40 Hog, meat byproducts ...... 0 .40 Vegetable, leafy, except brassica, group 4, ex- Horse, meat byproducts ...... 0 .80 cept spinach ...... 4 .0 Poultry, meat byproducts ...... 0.02 Vegetable, root, except sugar beet, subgroup Sheep, meat byproducts ...... 0 .80 1B ...... 0 .60 Vegetable, tuberous and corm, subgroup 1C ..... 0.20 (b) Section 18 emergency exemptions. [Reserved] (2) Tolerances are established for the (c) Tolerances with regional registra- residues of the insecticide flonicamid, tions. [Reserved] including its metabolites and (d) Indirect or inadvertent residues. degradates, in or on the commodities [Reserved] in the table below. Compliance with the tolerance levels specified below is [78 FR 48074, Aug. 7, 2013] to be determined by measuring only § 180.613 Flonicamid; tolerances for the sum of flonicamid, N- residues. (cyanomethyl)-4-(trifluoromethyl)-3- pyridinecarboxamide, and its metabo- (a) General. (1) Tolerances are estab- lites, TFNA (4- lished for the residues of the insecti- trifluoromethylnicotinic acid), and cide flonicamid, including its metabo- TFNA–AM (4- lites and degradates, in or on the com- trifluoromethylnicotinamide), cal- modities in the table below. Compli- culated as the Stoichiometric equiva- ance with the tolerance levels specified lent of flonicamid, in or on the fol- below is to be determined by measuring lowing commodities. only the sum of flonicamid, N- (cyanomethyl)-4-(trifluoromethyl)-3- Parts per pyridinecarboxamide, and its metabo- Commodity million lites, TFNA (4- Cattle, fat ...... 0.03 trifluoromethylnicotinic acid), TFNA– Cattle, meat ...... 0 .08 AM (4-trifluoromethylnicotinamide), Cattle, meat byproducts ...... 0.08 Egg ...... 0 .04 and TFNG, N-(4- Goat, fat ...... 0 .03 trifluoromethylnicotinoyl)glycine, cal- Goat, meat ...... 0.08 culated as the stoichiometric equiva- Goat, meat byproducts ...... 0 .08 lent of flonicamid, in or on the fol- Hog, fat ...... 0 .03 Hog, meat ...... 0 .03 lowing commodities. Hog, meat byproducts ...... 0 .03 Horse, fat ...... 0 .03 Commodity Parts per Horse, meat ...... 0 .08 million Horse, meat byproducts ...... 0 .08 Milk ...... 0.05 Alfalfa, forage ...... 10.0 Poultry, fat ...... 0.03 Alfalfa, hay ...... 1.0 Poultry, meat ...... 0 .03 Alfalfa, seed ...... 1 .5 Poultry, meat byproducts ...... 0.03 Almond, hulls ...... 9 .0 Sheep, fat ...... 0 .03 Berry, low growing, subgroup 13–07G ...... 1 .5 Sheep, meat ...... 0.08 Brassica, head and stem, subgroup 5A ...... 1 .5 Sheep, meat byproducts ...... 0 .08 Brassica, leafy greens, subgroup 5B ...... 16

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(b) Section 18 emergency exemptions. Commodity Parts per [Reserved] million (c) Tolerances with regional registra- Cattle, liver ...... 1 .0 tions. [Reserved] Cattle, meat ...... 0 .01 (d) Indirect or inadvertent residues. Cattle, meat byproducts, except liver ...... 0 .10 Corn, field, forage ...... 0 .80 [Reserved] Corn, field, grain ...... 0 .05 [70 FR 51614, Aug. 31, 2005, as amended at 71 Corn, field, stover ...... 1 .0 Goat, fat ...... 0 .01 FR 15608, Mar. 29, 2006; 73 FR 17923, Apr. 2, Goat, liver ...... 1.0 2008; 77 FR 67776, Nov. 14, 2012; 78 FR 75266, Goat, meat ...... 0.01 Dec. 11, 2013] Goat, meat byproducts, except liver ...... 0 .10 Hog, fat ...... 0 .01 § 180.614 Kasugamycin; tolerances for Hog, liver ...... 0 .10 Hog, meat ...... 0 .01 residues. Hog, meat byproducts, except liver ...... 0 .01 (a) General. Tolerances are estab- Horse, fat ...... 0 .01 lished for residues of kasugamycin, in- Horse, liver ...... 1 .0 Horse, meat ...... 0 .01 cluding its metabolites and degradates, Horse, meat byproducts, except liver ...... 0 .10 in or on the commodities listed in the Milk ...... 0.01 following table. Compliance with the Sheep, fat ...... 0 .01 Sheep, liver ...... 1.0 tolerance levels specified is to be deter- Sheep, meat ...... 0.01 mined by measuring only kasugamycin Sheep, meat byproducts, except liver ...... 0 .10 (3-O-[2-amino-4-[(carboxyimino-meth- Poultry, liver ...... 0 .10 yl)amino]-2,3,4,6-tetradeoxy-a-D- arabino-hexopyranosyl]-D-chiro-ino- (b) Section 18 emergency exemptions. sitol) in or on the commodity. [Reserved] (c) Tolerances with regional registra- Commodity Parts per tions. [Reserved] million (d) Indirect or inadvertent residues. Fruit, pome, group 11–10 ...... 0 .20 Tolerances are established for the indi- Vegetable, fruiting, group 8 1 ...... 0.04 rect or inadvertent residues of 1 There is no U.S. registration as of September 1, 2005. amicarbazone [4-amino-4, 5-dihydro-N- (b) Section 18 emergency exemptions. (1,1-dimethylethyl)-3-(1-methylethyl)-5- [Reserved] oxo-1H-1,2,4-triazole-1-carboxamide] (c) Tolerances with regional registra- and its metabolites DA amicarbazone tions. [Reserved] [N-(1,1-dimethylethyl)-4,5-dihydro-3-(1- (d) Indirect or inadvertent residues. methylethyl)-5-oxo-1H-1,2,4-triazole-1- [Reserved] carboxamide] and iPr-2-OH DA amicarbazone [N-(1,1-dimethylethyl)- [79 FR 51497, Aug. 29, 2014] 4,5-dihydro-3-(1-hydroxy-1- methylethyl)-5-oxo-1H-1,2,4-triazole-1- § 180.615 Amicarbazone; tolerances for carboxamide], calculated as parent residues. equivalents, in or on the following (a) General. Tolerances are estab- commodities when present therein as a lished for combined residues of the her- result of application of amicarbazone bicide, amicarbazone [4-amino-4, 5- to the growing crops in paragraph (a) dihydro- N-(1,1-dimethylethyl)-3-(1- of this section: methylethyl)-5-oxo-1H-1,2,4-triazole-1- carboxamide] and its metabolites DA Commodity Parts per amicarbazone [N-(1,1-dimethylethyl)- million 4,5-dihydro-3-(1-methylethyl)-5-oxo-1H- Alfalfa, forage ...... 0.05 1,2,4-triazole-1-carboxamide] and iPr-2- Alfalfa, hay ...... 0.10 Cotton, gin byproducts ...... 0 .30 OH DA amicarbazone [N-(1,1- Cotton, undelinted seed ...... 0 .07 dimethylethyl)-4,5-dihydro-3-(1-hy- Soybean, forage ...... 1 .50 droxy-1-methylethyl)-5-oxo-1H-1,2,4-tri- Soybean, hay ...... 5 .0 Soybean, seed ...... 0 .80 azole-1-carboxamide], calculated as Wheat, bran ...... 0.15 parent equivalents, in or on the fol- Wheat, flour ...... 0 .15 lowing commodities: Wheat, forage ...... 0 .50 Wheat, germ ...... 0 .15 Parts per Wheat, grain ...... 0 .10 Commodity million Wheat, hay ...... 1 .0 Wheat, middlings, ...... 0.15 Cattle, fat ...... 0.01 Wheat, shorts ...... 0 .15

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Parts per Parts per Commodity million Commodity million

Wheat, straw ...... 0 .50 Corn, sweet, kernel plus cob with husks re- moved ...... 0 .01 Corn, sweet, stover ...... 30.0 [70 FR 55760, Sept. 23, 2005, as amended at 74 Cotton, gin byproducts ...... 8 .0 FR 46377, Sept. 9, 2009] Cotton, undelinted seed ...... 0 .25 Egg ...... 0 .04 § 180.616 Fenpropimorph; tolerances Fruit, stone, group 12–12 ...... 0 .2 for residues. Goat, meat byproducts ...... 0 .04 Tolerances are established for the Grain, aspirated grain fractions ...... 7 .0 Horse, meat byproducts ...... 0 .04 residues of the fungicide Nut, tree, group 14–12 ...... 0 .04 fenpropimorph (rel-(2R,6S)-4-[3-[4-(1,1- Oat, grain ...... 1 .0 dimethylethyl)phenyl]-2- Oat, hay ...... 17 methylpropyl]-2,6-dimethylmorpholine) Oat, straw ...... 6.0 in or on the following commodity: Pea and bean, dried shelled, except soybean, subgroup 6C ...... 0 .15 Parts per Peanut ...... 0 .04 Commodity million Peanut, refined oil ...... 0.05 Rapeseed subgroup 20A ...... 0 .08 Banana* ...... 2 .0 Rye, grain ...... 0.25 *No U.S. registration as of February 10, 2006. Rye, straw ...... 14 Sheep, meat byproducts ...... 0 .04 (b) Section 18 emergency exemptions. Soybean, forage ...... 3 .0 [Reserved] Soybean, hay ...... 6 .0 (c) Tolerances with regional registra- Soybean, hulls ...... 0 .08 tions. [Reserved] Soybean, seed ...... 0 .05 (d) Indirect or inadvertent residues. Sugarcane, cane ...... 0.06 Sunflower subgroup 20B ...... 0.7 [Reserved] Vegetable, tuberous and corn, subgroup 1C ...... 0.04 [71 FR 15612, Mar. 29, 2006] Wheat, grain ...... 0 .15 Wheat, hay ...... 16 § 180.617 Metconazole; tolerances for Wheat, milled byproducts ...... 0 .20 residues. Wheat, straw ...... 18 1 (a) General. Tolerances are estab- No U.S. registration as of August 30, 2006. lished for residues of metconazole, in- (b) Section 18 emergency exemptions. cluding its metabolites and degradates, [Reserved] in or on the commodities in the fol- (c) Tolerances with regional registra- lowing table. Compliance with the tol- tions. [Reserved] erance levels specified below is to be (d) Indirect or inadvertent residues. determined by measuring only [Reserved] metconazole [5-[(4- chlorophenyl)methyl]-2,2-dimethyl-1- [71 FR 56388, Sept. 27, 2006, as amended at 71 (1H-1,2,4-triazol-1- FR 76196, Dec. 20, 2006; 73 FR 22828, Apr. 28, 2008; 74 FR 21266, May 7, 2009; 76 FR 50904, ylmethyl)cyclopentanol] as the sum of Aug. 17, 2011; 76 FR 81396, Dec. 28, 2011; 77 FR its cis- and trans-isomers in or on the 26456, May 4, 2012; 77 FR 66723, Nov. 7, 2012; 79 following commodities: FR 12411, Mar. 5, 2014; 80 FR 30625. May 29, 2015] Parts per Commodity million § 180.618 Benthiavalicarb-isopropyl; Almond, hulls ...... 4 .0 tolerance for residues. Banana 1 ...... 0.1 Barley, grain ...... 2 .5 (a) General. Tolerances are estab- Barley, hay ...... 7 .0 lished for the combined residues of Barley, straw ...... 7 .0 benthiavalicarb-isopropyl, Beet, sugar, dried pulp ...... 0 .70 Beet, sugar, molasses ...... 0 .08 isopropyl[(S)-1-[[[(1R)-1-(6-fluoro-2- Beet, sugar, roots ...... 0 .07 benzothiazolyl)ethyl]amino] carbonyl]- Bushberry subgroup 13–07B ...... 0 .40 2-methylpropyl]carbamate and Cattle, meat byproducts ...... 0.04 Corn, field, forage ...... 3 .0 isopropyl[(S)-1-[[[(1S)-1-(6-fluoro-2- Corn, field, grain ...... 0 .02 benzothiazolyl)ethyl]amino] carbonyl]- Corn, field, stover ...... 30 2-methylpropyl]carbamate, in or on the Corn, pop, grain ...... 0.02 Corn, pop, stover ...... 30 following raw agricultural commod- Corn, sweet, forage ...... 3 .0 ities:

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Parts per Parts per Commodity million Commodity million

Grape, imported ...... 0 .25 Goat, fat ...... 10 .0 Grape, raisin ...... 1 .0 Goat, meat ...... 0.40 Tomato ...... 0.45 Goat, meat byproducts ...... 10 .0 Hog, fat ...... 4 .0 Note: There are no U.S. registrations as of July 30, 2006. Hog, meat ...... 0 .20 (b) Section 18 emergency exemptions. Hog, meat byproducts ...... 4 .0 Horse, fat ...... 10 .0 [Reserved] Horse, meat ...... 0 .40 (c) Tolerances with regional registra- Horse, meat byproducts ...... 10 .0 tions. [Reserved] Milk ...... 0.60 Poultry, fat ...... 1.0 (d) Indirect of inadvertent residues. Poultry, meat ...... 0 .01 [Reserved] Poultry, meat byproducts ...... 1.0 Rice, grain ...... 0 .01 [71 FR 52003, Sept. 1, 2006] Sheep, fat ...... 10 .0 Sheep, meat ...... 0.40 § 180.619 Epoxiconazole; tolerances for Sheep, meat byproducts ...... 10 .0 residues. (b) Section 18 emergency exemptions. (a) General. Tolerances are estab- [Reserved] lished for the residues of the fungicide (c) Tolerances with regional registra- epoxiconazole [(rel-1-[[(2R,3S)-3-(2- tions. [Reserved] chlorophenyl)-2-(4- (d) Indirect or inadvertent residues. fluorophenyl)oxiranyl]methyl]-1H-1,2,4- [Reserved] triazole]) in or on the following com- modities: [76 FR 23498, Apr. 27, 2011, as amended at 78 FR 70877, Nov. 27, 2013] Parts per Commodity million § 180.621 Dithianon; tolerances for res- idues. Banana* ...... 0 .5 Coffee* ...... 0 .05 (a) General. Tolerances are estab- *No U.S. Registration as of August 4, 2006 lished for residues of dithianon, includ- ing its metabolites and degradates, in (b) Section 18 emergency exemptions. or on the commodities in the table [Reserved] below. Compliance with the tolerance (c) Tolerances with regional Registra- levels specified below is to be deter- tions. [Reserved] mined by measuring only dithianon, 5, (d) Indirect or inadvertent residues. 10-dihydro-5,10-dioxonaphtho(2,3-b)-1,4- [Reserved] dithiin-2,3-dicarbonitrile. [71 FR 53989, Sept. 13, 2006] Parts per Commodity million § 180.620 Etofenprox; tolerances for residues. Fruit, pome, group 111 ...... 5 Grape 2 ...... 3 (a) General. A tolerance is established Hop, dried cones1 ...... 100 for residues of the insecticide 1No U.S. registration as of September 5, 2006. etofenprox, including its metabolites 2No U.S. registration as of January 29, 2010. and degradates, in or on the com- (b) Section 18 emergency exemptions. modity in the table in this paragraph. [Reserved] Compliance with the tolerance level (c) Tolerances with regional registra- specified in this paragraph is to be de- tions. [Reserved] termined by measuring only (d) Indirect or inadvertent residues. etofenprox, 2-(4-ethoxyphenyl)-2- [Reserved] methylpropyl 3-phenoxybenzyl ether, in or on the commodity. [75 FR 5522, Feb. 3, 2010]

Parts per § 180.622 Ethaboxam; tolerances for Commodity million residues. Cattle, fat ...... 10.0 (a) General. Tolerances are estab- Cattle, meat ...... 0 .40 lished for residues of ethaboxam, N- Cattle, meat byproducts ...... 10.0 (cyano-2-thienylmethyl)-4-ethyl-2- Egg ...... 0 .40 All food commodities (including feed commod- (ethlyamino)-5-thiazolecarboxamide in ities) not otherwise listed in this subsection .... 5 .0 or on the following commodity:

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bromo-6-methoxy-2- Commodity Parts per million methylphenyl)(2,3,4-trimethoxy-6- Grape 1 ...... 6 .0 methylphenyl)methanone in or on the following commodities: 1 There is no U.S. registration as of September 27, 2006 (b) Section 18 emergency exemptions. Parts per Commodity million [Reserved] (c) Tolerances with regional registra- Apricot ...... 0 .70 tions. [Reserved] Cherry subgroup 12–12A ...... 2 .0 Fruit, pome, group 11–10 ...... 1 .5 (d) Indirect or inadvertent residues. Fruit, small, vine climbing, except fuzzy kiwifruit, [Reserved] subgroup 13–07F ...... 4 .5 Grape, raisin ...... 17 [71 FR 56392, Sept. 27, 2006] Hop, dried cones ...... 70 Peach subgroup 12–12B ...... 0.70 § 180.623 Flufenoxuron; tolerances for Vegetable, cucurbit, group 9 ...... 0.50 residues. Vegetable, fruiting, group 8–10 ...... 0 .90 (a) General. Tolerances are estab- (b) Section 18 emergency exemption. lished for residues of the insecticide, [Reserved] flufenoxuron, 1-[4-(2-chloro-a,a,a- (c) Tolerances with regional registra- trifluoro-p-tolyloxy)-2-fluorophenyl]-3- tions. [Reserved] (2,6-difluorobenzoyl)urea, in or on the (d) Indirect or inadvertent residues. following food commodities. [Reserved]

Commodity Parts per [71 FR 54917, Sept. 20, 2006, as amended at 75 million FR 75393, Dec. 3, 2010; 79 FR 63053, Oct. 22, Apple 1 ...... 0.50 2014] Cattle, fat 1 ...... 4.5 Cattle, meat 1 ...... 0 .10 § 180.625 Orthosulfamuron; tolerances Cattle, meat byproducts 1 ...... 0.50 for residues. Goat, fat 1 ...... 4 .5 Goat, meat 1 ...... 0.10 (a) General. Tolerances are estab- Goat, meat byproducts 1 ...... 0 .50 lished for residues of orthosulfamuron Grape 1 ...... 0 .70 1-(4,6-dimethoxypyrimidin-2-yl)-3-[2- Grape, raisin 1 ...... 2 .0 Horse, fat 1 ...... 4 .5 (dimethylcarbamoyl)- Horse, meat 1 ...... 0 .10 phenylsulfamoyl] urea) per se in or on Horse, meat byproducts 1 ...... 0 .50 the following commodities: Milk ...... 0.20 Milk, fat 1 ...... 4 .0 1 Parts per Orange ...... 0 .30 Commodity million Orange, oil 1 ...... 60 1 Pear ...... 0 .50 Rice, grain ...... 0 .05 1 Sheep, fat ...... 4 .5 Rice, straw ...... 0 .05 Sheep, meat 1 ...... 0.10 Sheep, meat byproducts 1 ...... 0 .50 (b) Section 18 emergency exemptions. 1There are no U.S. registrations as of September 30, 2006. [Reserved] (b) Section 18 emergency exemptions. (c) Tolerances with regional registra- [Reserved] tions. [Reserved] (c) Tolerances with regional restric- (d) Indirect and inadvertant residues. tions. [Reserved] [Reserved] (d) Indirect or inadvertent residues. [72 FR 8931, Feb. 28, 2007] [Reserved] [71 FR 57436, Sept. 29, 2006] § 180.626 Prothioconazole; tolerances for residues. § 180.624 Metrafenone; tolerances for (a) General. (1) Tolerances are estab- residues. lished for residues of prothioconazole, (a) General. Tolerances are estab- 2-[2-(1-chlorocylcopropyl)-3-(2- lished for residues of the fungicide chlorophenyl)-2-hydroxypropyl]-1,2- metrafenone, including its metabolites dihydro-3H-1,2,4-triazole-3-thion, in- and degradates, in or on the commod- cluding its metabolites and degradates, ities in the table below. Compliance in or on the commodities in the table with the tolerance levels specified in below. Compliance with the tolerance the following table is to be determined levels specified below is to be deter- by measuring only metrafenone (3- mined by measuring only

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prothioconazole and its metabolite Commodity Parts per prothioconazole-desthio, or a-(1- million chlorocyclopropyl)-a-[(2- Horse, meat byproducts ...... 0 .2 chlorophenyl)methyl]-1H-1,2,4-triazole- Milk ...... 0.02 1-ethanol, calculated as parent in or on Poultry liver ...... 0 .02 the commodity. Sheep, fat ...... 0 .1 Sheep, meat ...... 0.02 Parts per Sheep, meat byproducts ...... 0 .2 Commodity million (b) Section 18 emergency exemptions. Alfalfa, forage ...... 0.02 Alfalfa, hay ...... 0.02 [Reserved] Beet, sugar, roots ...... 0 .25 (c) Tolerances with regional registra- Berry, low growing, except strawberry, subgroup tions. [Reserved] 13–07H ...... 0 .20 Bushberry, subgroup 13–07B ...... 2.0 (d) Indirect or inadvertent residues. Corn, sweet kernel plus cob with husks re- [Reserved] moved ...... 0 .04 Grain, aspirated grain fractions ...... 11 [72 FR 11783, Mar. 14, 2007, as amended at 73 Grain, cereal, forage, fodder and straw, group FR 14719, Mar. 19, 2008; 74 FR 14749, Apr. 1, 16, except sorghum, and rice; forage ...... 8 .0 2009; 74 FR 46699, Sept. 11, 2009; 75 FR 29914, Grain, cereal, forage, fodder and straw, group May 28, 2010; 76 FR 61592, Oct. 5, 2011; 78 FR 16, except sorghum, and rice; hay ...... 7 .0 67052, Nov. 8, 2013] Grain, cereal, forage, fodder and straw, group 16, except sorghum, and rice; stover ...... 10 Grain, cereal, forage, fodder and straw, group § 180.627 Fluopicolide; tolerances for 16, except sorghum, straw ...... 5 .0 residues. Grain, cereal, group 15, except sweet corn and sorghum ...... 0 .35 (a) General. Tolerances are estab- Pea and bean, dried shelled, except soybean, lished for residues of the fungicide subgroup 6C ...... 0 .9 fluopicolide [2,6-dichloro-N-[[3-chloro-5- Peanut ...... 0 .02 Potato ...... 0 .02 (trifluoromethyl)-2- Rapeseed, seed ...... 0 .15 pyridinyl]methyl]benzamide], includ- Rice, hulls ...... 0 .90 ing its metabolites and degradates, in Soybean, forage ...... 4 .5 or on the commodities in the table in Soybean, hay ...... 17 Soybean, seed ...... 0 .15 this paragraph. Compliance with the Vegetable, cucurbit, crop group 9 ...... 0.30 tolerance levels specified below is to be determined by measuring only (2) Tolerances are established for res- fluopicolide [2,6-dichloro-N-[[3-chloro-5- idues of prothioconazole, 2-[2-(1- (trifluoromethyl)-2- chlorocylcopropyl)-3-(2-chlorophenyl)- pyridinyl]methyl]benzamide] in or on 2-hydroxypropyl]-1,2-dihydro-3H-1,2,4- the commodity. triazole-3-thion, including its metabo- lites and degradates, in or on the com- Commodity Parts per modities in the table below. Compli- million ance with the tolerance levels specified Brassica, head and stem, subgroup 5A ...... 5 .0 below is to be determined by measuring Grape ...... 2 .0 only prothioconazole and its metabo- Grape, raisin ...... 6 .0 Potato, processed potato waste ...... 1 .0 lites prothioconazole-desthio, or a-(1- Vegetable, brassica (cole) leafy subgroup 5B .... 18 chlorocyclopropyl)-a-[(2- Vegetable, bulb, crop group 3–07 ...... 7.0 chlorophenyl)methyl]-1H-1,2,4-triazole- Vegetable, cucurbit, group 9 ...... 0.50 1-ethanol, and conjugates that can be Vegetable, fruiting, group 8 ...... 1.60 Vegetable, leafy, except brassica, group 4 ...... 25 converted to these two compounds by Vegetable, leaves of root and tuber, group 2 ..... 15 .0 acid hydrolysis, calculated as parent in Vegetable root, subgroup 1A ...... 0.15 or on the commodity. Vegetable, tuberous and corm subgroup 1C ...... 0 .3

Commodity Parts per (b) Section 18 emergency exemptions. million [Reserved] Cattle, fat ...... 0.1 (c) Tolerances with regional registra- Cattle, meat ...... 0 .02 tions. [Reserved] Cattle, meat byproducts ...... 0.2 Goat, fat ...... 0 .1 (d) Indirect or inadvertent residues. Goat, meat ...... 0.02 Tolerances are established for residues Goat, meat byproducts ...... 0 .2 of the fungicide fluopicolide [2,6- Hog, meat byproducts ...... 0 .05 Horse, fat ...... 0 .1 dichloro-N-[[3-chloro-5- Horse, meat ...... 0 .02 (trifluoromethyl)-2-

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pyridinyl]methyl]benzamide], includ- Commodity Parts per ing its metabolites and degradates, in million or on the commodities in the table in Cacao bean, roasted bean ...... 0 .8 this paragraph. Compliance with the Cactus ...... 13 tolerance levels specified below is to be Canistel ...... 4 .0 Cattle, fat ...... 0.5 determined by measuring only Cattle, meat ...... 0 .1 fluopicolide [2,6-dichloro-N-[[3-chloro-5- Cattle, meat byproducts ...... 0.5 (trifluoromethyl)-2- Cherimoya ...... 4 .0 Cherry, sweet ...... 2 .0 pyridinyl]methyl]benzamide] in or on Cherry, tart ...... 2 .0 the commodity. Citrus, dried pulp ...... 14 Coffee, green bean ...... 0 .4 Commodity Parts per Coffee, instant ...... 2 .0 million Corn, field, grain ...... 0 .04 Corn, field, milled byproducts ...... 0 .1 Corn, field, forage ...... 0 .08 Corn, pop, grain ...... 0.04 Corn, field, grain ...... 0 .01 Corn, sweet, kernel plus cobs with husk re- Corn, field, stover ...... 0 .20 moved ...... 0 .02 Wheat, aspirated grain fractions ...... 0.07 Cotton, gin byproduct ...... 30 Wheat, forage ...... 0 .20 Cotton, hulls ...... 0 .40 Wheat, grain ...... 0 .02 Cottonseed subgroup 20C ...... 0 .3 Wheat, hay ...... 0 .50 Crayfish ...... 8.0 Wheat, milled byproducts ...... 0 .07 Custard apple ...... 4 .0 Wheat, straw ...... 0 .50 Egg ...... 0 .2 Feijoa ...... 4 .0 [72 FR 14447, Mar. 28, 2007, as amended at 73 Fig ...... 4 .0 Fruit, caneberry, subgroup 13–07A ...... 1 .8 FR 5455, Jan. 30, 2008; 73 FR 30498, May 28, Fruit, citrus, group 10–10 ...... 1 .4 2008; 76 FR 22054, Apr. 20, 2011; 79 FR 12401, Fruit, pome, group 11–10 ...... 1 .2 Mar. 5, 2014; 79 FR 45693, Aug. 6, 2014] Fruit, small vine climbing, subgroup 13–07F ...... 2.5 Fruit, stone, group 12–12, except cherry, chicka- § 180.628 Chlorantraniliprole; toler- saw plum, and damson plum ...... 4 .0 ances for residues. Goat, fat ...... 0 .5 Goat, meat ...... 0.1 (a) General. Tolerances are estab- Goat, meat byproducts ...... 0 .5 lished for residues of the insecticide Grain, aspirated grain fractions ...... 640 Grain, cereal, except rice and corn, group 15 .... 6.0 chlorantraniliprole, including its me- Grain, cereal, forage, fodder and straw, group tabolites and degradates, in or on the 16 ...... 40 commodities in the table below. Com- Grape, raisin ...... 5 .0 pliance with the tolerance levels speci- Grass forage, fodder and hay, group 17 ...... 90 Guava ...... 4 .0 fied below is to be determined by meas- Herb subgroup 19A, dried leaves ...... 90 uring only chlorantraniliprole, 3- Herb subgroup 19A, fresh leaves ...... 25 bromo-N-[4-chloro-2-methyl-6- Hog, fat ...... 0 .05 Hog, meat ...... 0 .02 [(methylamino)carbonyl]phenyl]-1-(3- Hog, meat byproducts ...... 0 .05 chloro-2-pyridinyl)-1H-pyrazole-5- Hop, dried cones ...... 90 carboxamide. Horse, fat ...... 0 .5 Horse, meat ...... 0 .1 Parts per Horse, meat byproducts ...... 0 .5 Commodity million Ilama ...... 4 .0 Jaboticaba ...... 2 .0 Acerola ...... 2.0 Longan ...... 4 .0 Alfalfa, seed ...... 7 .0 Lychee ...... 2 .0 Almond, hulls ...... 5 .0 Mango ...... 4.0 Animal feed, nongrass, group 18, forage ...... 25 Milk ...... 0.1 Animal feed, nongrass, group 18, hay ...... 90 Nut, tree, group 14 ...... 0 .04 Apple, wet pomace ...... 2 .5 Olive ...... 4 .0 Artichoke, globe ...... 4.0 Olive, oil ...... 40 Asparagus ...... 13 Onion, bulb, subgroup 3–07A ...... 0 .30 Atemoya ...... 4 .0 Onion, green, subgroup 3–07B ...... 3 .0 Avocado ...... 4 .0 Papaya ...... 4 .0 Banana ...... 4.0 Passionfruit ...... 4 .0 Beet, sugar, molasses ...... 9 .0 Peanut ...... 0 .06 Berry, large shrub/tree, subgroup 13–07C ...... 2 .5 Peanut, hay ...... 90 Berry, low growing, subgroup 13–07G ...... 1 .0 Peppermint, tops ...... 9 .0 Biriba ...... 4 .0 Persimmon ...... 4 .0 Brassica, head and stem, subgroup 5A ...... 4 .0 Pineapple ...... 1.5 Brassica, leafy greens, subgroup 5B ...... 11 Pineapple, process residue ...... 3 .0 Bushberry, subgroup 13–07B ...... 2.5 Pistachio ...... 0.04 Cacao bean ...... 0 .08 Plum, chickasaw ...... 2 .0 Cacao bean, chocolate ...... 1 .5 Plum, damson ...... 2 .0 Cacao bean, cocoa powder ...... 1 .5 Pomegranate ...... 4 .0

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Parts per Parts per Commodity million Commodity million

Poultry, fat ...... 0.2 African tree nut ...... 0 .02 Poultry, meat ...... 0 .05 Almond ...... 0.60 Poultry, meat byproducts ...... 0.2 Almond, hull ...... 15 Pulasan ...... 4 .0 Banana 1 ...... 0.30 Rambutan ...... 4 .0 Beet sugar ...... 0 .08 Rapeseed subgroup 20A ...... 2 .0 Brassica, head and stem (subgroup 5A) ...... 1 .5 Rice, grain ...... 0 .15 Brassica, leafy greens (subgroup 5B) ...... 7 .0 Rice, hulls ...... 0 .4 Brazil nut ...... 0 .02 Sapodilla ...... 4 .0 Bur oak ...... 0 .02 Sapote, black ...... 4 .0 Butternut ...... 0 .02 Sapote, mamey ...... 4 .0 Cajou ...... 0 .02 Sapote, white ...... 4 .0 Cashew ...... 0 .02 Sheep, fat ...... 0 .5 Castanha-do-maranhao ...... 0.02 Sheep, meat ...... 0.1 Cattle, fat ...... 0.05 Sheep meat byproducts ...... 0 .5 Cattle, liver ...... 1 .0 Soursop ...... 4 .0 Cattle, meat byproducts, except liver ...... 0 .05 Spanish lime ...... 4 .0 Cattle, muscle ...... 0 .05 Spearmint, tops ...... 9 .0 Coconut ...... 0 .02 Spice, subgroup 19B ...... 90 Coffee, green, bean 1 ...... 0 .15 Star apple ...... 4 .0 Coffee, instant 1 ...... 0 .30 Starfruit ...... 4 .0 Coquito nut ...... 0 .02 Sugar apple ...... 4 .0 Corn, field, forage ...... 5 .0 Sugarcane, cane ...... 14 Corn, field, grain ...... 0 .01 Sugarcane, molasses ...... 420 Corn, field, refined oil ...... 0 .02 Sunflower subgroup 20B ...... 2.0 Corn, field, stover ...... 15 Tea, dried ...... 50 .0 Corn, pop ...... 0 .01 Ti, leaves ...... 13 .0 Corn, pop, stover ...... 15 Ti, root ...... 0 .3 Cotton, gin byproducts ...... 6 .0 Vegetable, cucurbit, group 9 ...... 0.5 Cotton, undelinted seed ...... 0 .50 Vegetable, foliage of legume, group 7 ...... 90 Dika nut ...... 0 .02 Vegetable, fruiting, group 8–10 ...... 1 .4 Egg ...... 0 .01 Vegetable, leafy, except brassica, group 4 ...... 13 Fruit, pome, group 11–09 ...... 0 .40 Vegetable, leaves of root and tuber, group 2 ..... 40 .0 Fruit, stone, group 12–10 ...... 1 .5 Vegetable, legume, group 6 ...... 2 .0 Goat, fat ...... 0 .05 Vegetable, root and tuber, group 1 ...... 0 .30 Goat, liver ...... 1.0 Wax jambu ...... 4 .0 Goat, meat byproducts, except liver ...... 0 .05 Goat, muscle ...... 0 .05 (b) Section 18 emergency exemptions. Grain, aspirated fractions ...... 6 .0 Grape ...... 1 .5 [Reserved] Grape, raisin ...... 2 .4 (c) Tolerances with regional registra- Guiana chestnut ...... 0 .02 tions. [Reserved] Hazelnut ...... 0 .02 (d) Indirect or inadvertent residues. Heartnut ...... 0 .02 Hickory nut ...... 0 .02 [Reserved] Hog, fat ...... 0 .01 Hog, meat byproducts ...... 0 .05 [75 FR 5532, Feb. 3, 2010, as amended at 75 FR Hog, muscle ...... 0.01 17566, Apr. 7, 2010; 76 FR 44821, July 27, 2011; Horse, fat ...... 0 .05 76 FR 59909, Sept. 28, 2011; 77 FR 60315, Oct. 3, Horse, liver ...... 1 .0 2012; 77 FR 75561, Dec. 21, 2012; 78 FR 57285, Horse, meat byproducts, except liver ...... 0 .05 Sept. 18, 2013; 79 FR 7401, Feb. 7, 2014] Horse, muscle ...... 0.05 Japanese horse-chestnut ...... 0 .02 EDITORIAL NOTE: At 78 FR 57285, Sept. 18, Lettuce, head ...... 1.5 2013, § 180.628 was amended by revising the Macadamia nut ...... 0 .02 commodity ‘‘Egg’’ in the table in paragraph Milk ...... 0.02 (a); however, no revised text was provided, so Mongongo nut ...... 0 .02 the amendment could not be incorporated. Monkey-pot ...... 0 .02 Pachira nut ...... 0 .02 Peanut ...... 0 .09 § 180.629 Flutriafol; tolerances for resi- Peanut, hay ...... 15 dues. Pecan ...... 0 .02 Poultry, fat ...... 0.01 (a) General. Tolerances are estab- Poultry, meat byproducts ...... 0.01 lished for the residues of flutriafol, Radicchio ...... 1.5 [(±)-a-(2-fluorophenyl)-a-(4- Sapucaia nut ...... 0.02 fluorophenyl)-1H-1,2,4-triazole-1-eth- Sheep, fat ...... 0 .05 Sheep, liver ...... 1.0 anol], including its metabolites and Sheep, meat byproducts, except liver ...... 0 .05 degradates in or on the following com- Sheep, muscle ...... 0 .05 modities. Compliance with the fol- Sorghum, grain, forage ...... 2.0 Sorghum, grain, grain ...... 1 .5 lowing tolerances is to be determined Sorghum, grain, stover ...... 6 .0 by measuring flutriafol only. Soybean, seed ...... 0 .35

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tolerances expire and are revoked on Commodity Parts per million the dates specified in the following Strawberry ...... 1 .5 table. Tomato, paste ...... 1 .5 Vegetable, cucurbit, group 9 ...... 0.30 Parts per Expiration/ Vegetable, fruiting, group 8–10 ...... 1 .0 Commodity million revocation Vegetable, leafy, except Brassica, crop group 4, date except head lettuce and radicchio ...... 10 Soybean, aspirated grain fractions 2.6 12/31/10 Walnut, black ...... 0 .02 Soybean, seed ...... 0.04 12/31/10 Walnut, English ...... 0.02 Soybean, oil ...... 0.10 12/31/10 Wheat, bran ...... 0.30 Wheat, forage ...... 30 Wheat, germ ...... 0 .25 (c) Tolerances with regional registra- Wheat, grain ...... 0 .15 tions. [Reserved] Wheat, hay ...... 15 Wheat, straw ...... 9 .0 (d) Indirect or inadvertant residues. [Reserved] 1 There are no U.S. registrations as of October 22, 2013. [72 FR 49660, Aug. 29, 2007] (b) Section 18 emergency exemptions. [Reserved] § 180.631 Pyrasulfotole; tolerances for (c) Tolerances with regional registra- residues. tions [Reserved] (a) General. Tolerances are estab- (d) Indirect or inadvertent residues. lished for residues of the herbicide Tolerances are established for the indi- rect or inadvertent residues of the fun- pyrasulfotole, including its metabo- gicide flutriafol, including its metabo- lites and degradates, in or on the com- lites and degradates, in or on the com- modities in the table below. Compli- modities in the table below when ance with the tolerance levels specified present therein as a result of the appli- below is to be determined by measuring cation of flutriafol to the growing only the sum of pyrasulfotole ((5-hy- crops listed in the table to paragraph droxy-1,3-dimethyl-1H-pyrazol-4-yl)[2- (a) of this section. Compliance with the (methylsulfonyl)-4- following tolerance levels specified (trifluoromethyl)phenyl]methanone) below is to be determined by measuring and its desmethyl metabolite (5-hy- droxy-3-methyl-1H-pyrazol-4-yl)[2- only flutriafol ((±)-a-(2-fluorophenyl)-a- (4-fluorophenyl)-1H-1,2,4-triazole-1-eth- (methylsulfonyl)-4- anol) in or on the following commod- (trifluoromethyl)phenyl]methanone), ities: calculated as the stoichiometric equiv- alent of pyrasulfotole, in or on the Parts per commodities: Commodity million Parts per Corn, sweet, forage ...... 0 .09 Commodity million Corn, sweet, kernel plus cob with husk removed 0.01 Corn, sweet, stover ...... 0 .07 Aspirated grain fractions ...... 0 .40 Cotton, gin byproducts ...... 0 .02 Barley, grain ...... 0 .02 Cotton, undelinted seed ...... 0 .01 Barley, hay ...... 0 .30 Barley, straw ...... 0 .20 Cattle, fat ...... 0.03 [75 FR 26673, May 12, 2010, as amended at 76 Cattle, liver ...... 3 .0 FR 69647, Nov. 9, 2011; 77 FR 47301, Aug. 8, Cattle, meat ...... 0 .02 2012; 77 FR 48901, Aug. 15, 2012; 78 FR 75262, Cattle, meat byproducts, except liver ...... 0 .70 Dec. 11, 2013; 79 FR 32673, June 6, 2014; 80 FR Eggs ...... 0 .02 5951, Feb. 4, 2015] Goat, fat ...... 0 .03 Goat, liver ...... 3.0 Goat, meat ...... 0.02 § 180.630 Flusilazole; tolerances for Goat, meat byproducts, except liver ...... 0 .70 residues. Grass, forage ...... 25 Grass, hay ...... 3 .5 (a) General. [Reserved] Hog, fat ...... 0 .02 (b) Section 18 emergency exemptions. Hog, liver ...... 0 .30 Time-limited tolerances are estab- Hog, meat ...... 0 .02 lished for residues of the fungicide, Hog, meat byproducts, except liver ...... 0 .05 Horse, fat ...... 0 .03 flusilazole, (1-[[bis(4- Horse, liver ...... 3 .0 fluorophenyl)methylsilyl]methyl]-1H- Horse, meat ...... 0 .02 1,2,4-triazole) in connection with use of Horse, meat byproducts, except liver ...... 0 .70 Milk ...... 0.03 the pesticide under Section 18 emer- Oat, forage ...... 0 .10 gency exemptions granted by EPA. The Oat, grain ...... 0 .08

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Commodity Parts per § 180.633 Florasulam; tolerances for million residues. Oat, hay ...... 0.50 (a) General. Tolerances are estab- Oat, straw ...... 0.20 lished for residues of the herbicide Poultry, fat ...... 0.02 florasulam N-(2,6-difluorophenyl)-8- Poultry, meat ...... 0 .02 Poultry, meat byproducts ...... 0.20 fluoro-5-methoxy(1,2,4)triazolo(1,5- Rye, forage ...... 0 .20 c)pyrimidine-2-sulfonamide in or on Rye, grain ...... 0.02 the following commodities: Rye, straw ...... 0 .20 Sheep, fat ...... 0 .03 Commodity Parts per Sheep, liver ...... 3.0 million Sheep, meat ...... 0.02 Sheep, meat byproducts, except liver ...... 0 .70 Barley, grain ...... 0 .01 Barley, hay ...... 0 .05 Sorghum, grain, forage ...... 1.5 Barley, straw ...... 0 .05 Sorghum, grain, grain ...... 0 .70 Oat, forage ...... 0 .05 Sorghum, grain, stover ...... 0 .80 Oat, grain ...... 0 .01 Wheat, forage ...... 0 .20 Oat, hay ...... 0.05 Wheat, grain ...... 0 .02 Oat, straw ...... 0.05 Wheat, hay ...... 0 .80 Rye, forage ...... 0 .05 Wheat, straw ...... 0 .20 Rye, grain ...... 0.01 Rye, straw ...... 0 .05 Wheat, forage ...... 0 .05 (b) Section 18 emergency exemptions. Wheat, grain ...... 0 .01 [Reserved] Wheat, hay ...... 0 .05 (c) Tolerances with regional registra- Wheat, straw ...... 0 .05 tions. [Reserved] (d) Indirect or inadvertent residues. (b) Section 18 emergency exemptions. [Reserved] [Reserved] (c) Tolerances with regional registra- [72 FR 45649, Aug. 15, 2007, as amended at 76 tions. [Reserved] FR 23898, Apr. 29, 2011] (d) Indirect or inadvertent residues. [Reserved] § 180.632 Fenazaquin; Tolerances for residues. [72 FR 55077, Sept. 28, 2007] (a) General. Tolerances are estab- § 180.634 Tembotrione; tolerances for lished for residues of the insecticide residues. fenazaquin, including its metabolites and degradates, in or on the commod- (a) General. (1) Tolerances are estab- ities in the table below. Compliance lished for residues of the herbicide with the tolerance levels specified tembotrione, including its metabolites below is to be determined by measuring and degradates, in or on the commod- only fenazaquin, or 4-[2-[4-(1,1- ities listed in the table to this para- dimethylethyl)phenyl]- graph. Compliance with the tolerance ethoxy]quinazoline. levels specified below is to be deter- mined by measuring only the sum of tembotrione, 2-[2-chloro-4- Commodity Parts per million (methylsulfonyl)-3-[(2,2,2- Almond ...... 0.02 trifluoroethoxy)methyl]benzoyl]-1,3- Almond, hulls ...... 4 .0 cyclohexanedione and its metabolite, 2- Apple ...... 0.2 [2-chloro-4-(methylsulfonyl)-3-[(2,2,2- Cherry ...... 2.0 trifluoroethoxy) methyl]benzoyl]-4,6- Citrus Oil ...... 10 dihydroxy-1,3-cyclohexanedione, cal- Fruit, Citrus, Group 10 except Grape fruit ...... 0 .5 Pear ...... 0 .2 culated as the stoichiometric equiva- lent of tembotrione, in or on the fol- (b) Section is emergency exempotions. lowing commodities. [Reserved] Parts per (c) Tolerances with regional registra- Commodity million tion. [Reserved] Cattle, liver ...... 0 .40 (d) Indirect or inadvertent residues. Cattle, meat byproducts, except liver ...... 0 .07 [Reserved] Corn, field, forage ...... 0 .60 Corn, field, grain ...... 0 .02 [72 FR 44393, Aug. 8, 2007, as amended at 80 Corn, field, stover ...... 0 .45 FR 25958, May 6, 2015] Corn, pop, grain ...... 0.02

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2,3,3a,5a,5b,6,9, 10,11,12,13,14,16a,16b- Commodity Parts per million tetradecahydro-4,14-dimethyl-, Corn, pop, stover ...... 0.35 (2S,3aR,5aS,5bS,9S, 13S,14R,16aS,16bS); Corn, sweet, forage ...... 0 .35 ND-J: (2R,3aR,5aR,5bS,9S, Corn, sweet, stover ...... 0 .60 13S,14R,16aS,16bR)-9-ethyl-14-methyl- Goat, liver ...... 0.40 Goat, meat byproducts, except liver ...... 0 .07 13-[[(2S,5S,6R)-6- methyl-5- Horse, liver ...... 0 .40 (methylamino)tetrahydro- 2H-pyran-2- Horse, meat byproducts, except liver ...... 0 .07 yl]oxy]-7,15-dioxo-2,3,3a,4,5,5a,5b,6,7,9, Poultry, liver ...... 0 .07 10,11,12,13,14,15,16a,16b- octadecahydro- Sheep, liver ...... 0.40 Sheep, meat byproducts, except liver ...... 0 .07 1H-as- indaceno[3,2-d]oxacyclododecin- 2-yl 6-deoxy-3-O-ethyl-2,4-di-O-methyl- (2) Tolerances are established for res- alpha-L-mannopyranoside; and NF-J: idues of the herbicide tembotrione, in- (2R,3S,6S)-6-([(2R,3aR,5aR,5bS,9S, cluding its metabolites and degradates, 13S,14R,16aS,16bR)- 2-[(6-deoxy-3-O- in or on the commodities listed in the ethyl-2,4-di-O- methyl-alpha-L- table to this paragraph. Compliance mannopyranosyl) oxy]-9-ethyl-14-meth- with the tolerance levels specified yl-7,15-dioxo-2, 3,3a,4,5,5a,5b,6,7,9, below is to be determined by measuring 10,11,12,13,14,15,16a,16b- octadecahydro- only tembotrione, 2-[2-chloro-4- 1H-as- indaceno[3,2-d]oxacyclododecin- (methylsulfonyl)-3-[(2,2,2- 13-yl] oxy)-2-methyltetrahydro- 2H- trifluoroethoxy)methyl]benzoyl]-1,3- pyran-3-yl(methyl)formamide, in or on cyclohexanedione in or on the fol- the following raw agricultural com- lowing commodities. modities:

Parts per Commodity Parts per Commodity million million

Corn, sweet, kernel plus cob with husks re- Acerola ...... 0.30 moved ...... 0 .01 Almond, hulls ...... 19 Amaranth grain, grain ...... 1 .0 Apple, wet pomace ...... 0 .50 (b) Section 18 emergency exemptions. Artichoke, globe ...... 0.30 [Reserved] Asparagus ...... 0.04 (c) Tolerances with regional registra- Atemoya ...... 0 .30 Avocado ...... 0 .30 tions. [Reserved] Banana ...... 0.25 (d) Indirect or inadvertent residues. Beet, sugar, molasses ...... 0 .75 [Reserved] Biriba ...... 0 .30 Brassica, head and stem, subgroup 5A ...... 2 .0 [72 FR 55085, Sept. 28, 2007, as amended at 74 Brassica, leafy greens, subgroup 5B ...... 10 FR 47894, Sept. 18, 2009] Bushberry, subgroup 13B ...... 0 .25 Caneberry, subgroup 13A ...... 0.70 Canistel ...... 0 .30 § 180.635 Spinetoram; tolerances for Cattle, fat ...... 5.5 residues. Cattle, liver ...... 0 .85 Cattle, meat ...... 0 .20 (a) General. Tolerances are estab- Cattle, meat byproducts (except liver) ...... 0 .60 lished for the combined residues of the Cherimoya ...... 0 .30 insecticide spinetoram, expressed as a Citrus, dried pulp ...... 0 .50 combination of XDE-175-J: 1-H-as- Citrus, oil ...... 3.0 Corn, sweet, kernel plus cob with husks re- indaceno[3,2-d]oxacyclododecin-7,15- moved ...... 0 .04 dione, 2-[(6-deoxy-3-O-ethyl-2,4-di-O- Cotton, gin byproducts ...... 1 .5 methyl-a-L-mannopyranosyl) oxy]-13- Cotton, undelinted seed ...... 0 .04 Cranberry ...... 0 .04 [[(2R,5S,6R)-5- Custard apple ...... 0 .30 (dimethylamino)tetrahydro-6-methyl- Date ...... 0 .10 2H-pyran-2-yl] oxy]-9-ethyl- Egg ...... 0 .04 Feijoa ...... 0 .30 2,3,3a,4,5,5a,5b,6,9, 10,11,12,13,14,16a,16b- Fig ...... 0 .10 hexadecahydro 14-methyl-, Fruit, citrus, group 10 ...... 0 .30 (2R,3aR,5aR,5bS,9S, 13S,14R,16aS,16bR); Fruit, pome, group 11 ...... 0.20 XDE-175-L: 1H-as-indaceno[3,2- Fruit, stone, group 12 ...... 0 .20 Goat, fat ...... 5 .5 d]oxacyclododecin-7,15-dione, 2-[(6- Goat, liver ...... 0.85 deoxy-3-O- ethyl-2,4-di-O-methyl-a-L- Goat, meat ...... 0.20 mannopyranosyl)oxy]-13-[[(2R,5S,6R)-5- Goat, meat byproducts (except liver) ...... 0.60 Grain, aspirated fractions ...... 20 (dimethylamino)tetrahydro-6-methyl- Grain, cereal, group 15, except rice, sorghum, 2H-pyran-2-yl]oxy]-9-ethyl- pearl millet and proso millet ...... 0 .04

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Parts per Parts per Commodity million Commodity million

Grain, cereal, group 16, forage ...... 3 .5 Vegetable, leaves of root and tuber, group 2 ..... 10 Grain, cereal, group 16, hay ...... 10 Vegetable, legume, edible podded, subgroup 6A 0 .30 Grain, cereal, group 16, stover ...... 10 Vegetable, root and tuber, group 1 ...... 0 .10 Grain, cereal, straw, group 16, except rice ...... 1 .0 Watercress ...... 8 .0 Grape ...... 0 .50 Wax jambu ...... 0 .30 Grape, raisin ...... 0 .70 Guava ...... 0 .30 (b) Section 18 emergency exemptions. Herb, dried, subgroup 19A ...... 22 Herb, fresh, subgroup 19A ...... 3 .0 [Reserved] Hog, fat ...... 0 .40 (c) Tolerances with regional registra- Hog, meat ...... 0 .04 tion. [Reserved] Hog, meat byproducts ...... 0 .04 (d) Indirect and invertent residues. [Re- Hop, dried cones ...... 22 Horse, fat ...... 5 .5 served] Horse, liver ...... 0 .85 Horse, meat ...... 0 .20 [72 FR 57499, Oct. 10, 2007, as amended at 73 Horse, meat byproducts (except liver) ...... 0 .60 FR 14714, Mar. 19, 2008; 74 FR 40759, Aug. 13, Ilama ...... 0 .30 2009] Jaboticaba ...... 0 .30 Juneberry ...... 0 .25 § 180.636 1,3-dichloropropene; toler- Lingonberry ...... 0.25 ances for residues. Longan ...... 0 .30 Lychee ...... 0 .30 (a) General. Tolerances are estab- Mango ...... 0.30 lished for the combined residues of the Milk ...... 0.30 Milk, fat ...... 7 .5 fungicide cis- and trans-1,3- Millet, pearl, grain ...... 1 .0 dichloropropene and its metabolites Millet, proso, grain ...... 1 .0 cis- and trans-3-chloroacrylic acid, and Nut, tree, group 14 ...... 0 .10 cis- and trans-3-chloroallyl alcohol in or Okra ...... 0.40 Onion, green ...... 2 .0 on the following commodities. Papaya ...... 0 .30 Passionfruit ...... 0 .30 Parts per Commodity million Pea and bean, dried shelled, except soybean, subgroup 6C ...... 0 .04 Grape ...... 0.018 Pea and bean, succulent shelled, subgroup 6B 0 .04 Peanut ...... 0 .04 Peanut, hay ...... 11 (b) Section 18 emergency exemptions. Peppermint, tops ...... 3 .5 [Reserved] Pineapple ...... 0.04 (c) Tolerances with regional registra- Pineapple, processed residue ...... 0 .15 Pistachio ...... 0.10 tions. [Reserved] Pomegranate ...... 0 .30 (d) Indirect or inadvertent residues. Poultry, fat ...... 0.10 [Reserved] Poultry, meat ...... 0 .04 Poultry, meat byproducts ...... 0.04 [73 FR 8218, Feb. 13, 2008] Pulasan ...... 0 .30 Rambutan ...... 0 .30 § 180.637 Mandipropamid; tolerances Salal ...... 0 .25 for residues. Sapodilla ...... 0 .30 Sapote, black ...... 0 .30 (a) General. Tolerances are estab- Sapote, mamey ...... 0 .30 lished for residues of mandipropamid, Sapote, white ...... 0 .30 Sheep, fat ...... 5 .5 including its metabolites and Sheep, liver ...... 0.85 degradates, in or on the commodities Sheep, meat ...... 0.20 listed in the table below. Compliance Sheep, meat products (except liver) ...... 0 .60 with the tolerance levels specified Sorghum, grain, grain ...... 1 .0 Soursop ...... 0 .30 below is to be determined by measuring Soybean, seed ...... 0 .04 only mandipropamid (4-chloro-N-[2-[3- Spanish lime ...... 0 .30 methoxy-4-(2- Spearmint, tops ...... 3 .5 Spice, subgroup 19B, except black pepper ...... 1 .7 propynyloxy)phenyl]ethyl]-a-(2- Star apple ...... 0 .30 propynyloxy)benzeneacetamide) in or Star fruit ...... 0 .30 on the commodity. Strawberry ...... 1 .0 Sugar apple ...... 0 .30 Parts per Ti, leaves ...... 10 Commodity million Vegetable, bulb, group 3, except green onion .... 0.10 Vegetable, cucurbit, group 9 ...... 0.30 Basil, dried leaves ...... 200 Vegetable, foliage of legume, group 7 ...... 8 .0 Basil, fresh leaves ...... 30 Vegetable, fruiting, group 8 ...... 0.40 Bean, snap ...... 0 .90 Vegetable, leafy, except Brassica, group 4 ...... 8 .0 Brassica, head and stem, subgroup 5A ...... 3

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lished for residues of mandipropamid, Commodity Parts per million including its metabolites and Brassica, leafy greens, subgroup 5B ...... 25 degradates, in or on the commodities Fruit, small vine climbing, except fuzzy kiwifruit, listed in the table below resulting from subgroup 13–07F ...... 1 .4 use of the pesticide pursuant to Ginseng ...... 0 .30 Grape, raisin ...... 3 .0 FFIFRA section 18 emergency exemp- Hop, dried cones ...... 50 tions. Compliance with the tolerance Onion, bulb, subgroup 3–07A ...... 0 .05 Onion, green, subgroup 3–07B ...... 4 .0 levels specified below is to be deter- Potato, wet peel ...... 0 .03 mined by measuring only Vegetable, cucurbit, group 9 ...... 0.6 mandipropamid (4-chloro-N-[2-[3- Vegetable, fruiting, group 8–10 ...... 1 .0 methoxy-4-(2- Vegetable, leafy except Brassica, group 4 ...... 20 Vegetable, tuberous and corm, subgroup 1C ..... 0.01 propynyloxy)phenyl]ethyl]-a-(2- propynyloxy)benzeneacetamide) in or (b) Section 18 emergency exemptions. on the commodity. The tolerances ex- Time-limited tolerances are estab- pire on the date specified in the table.

Parts per Expiration/revocation Commodity million date

Basil, dried ...... 240 12/31/15

(c) Tolerances with regional registra- § 180.639 Flubendiamide; tolerances tions. [Reserved] for residues. (d) Indirect or inadvertent tolerances. (a) General. (1) Tolerances are estab- [Reserved] lished for residues of flubendiamide, in- [73 FR 2816, Jan. 16, 2008, as amended at 74 cluding its metabolites and degradates, FR 33169, July 10, 2009; 76 FR 55804, Sept. 9, in or on the commodities in the table 2011; 77 FR 74119, Dec. 13, 2012; 78 FR 76992, below. Compliance with the tolerance Dec. 20, 2013] levels specified in the table is to be de- termined by measuring only § 180.638 Pyroxsulam; tolerances for flubendiamide N2-[1, 1-dimethyl-2- residues. (methylsulfonyl)ethyl]-3-iodo-N1-[2- (a) General. Tolerances are estab- methyl-4- [1,2,2,2-tetrafluoro-1- lished for residues of the herbicide (trifluoromethyl)ethyl]phenyl]-1,2- benzenedicarboxamide, in or on the fol- pyroxsulam, N-(5,7- lowing commodities: dimethoxy[1,2,4]triazolo[1,5- a]pyrimidin-2-yl)-2-methoxy-4- Commodity Parts per (trifluoromethyl)-3- million pyridinesulfonamide in or on the raw Almond, hulls ...... 9 .0 agricultural commodities: Apple, wet pomace ...... 5 .0 Corn, field, forage ...... 8 .0 Parts per Corn, field, grain ...... 0 .03 Commodity million Corn, field, stover ...... 15 Corn, pop, grain ...... 0.02 Wheat, forage ...... 0 .06 Corn, pop, stover ...... 15 Wheat, grain ...... 0 .01 Corn, sweet, forage ...... 9 .0 Wheat, hay ...... 0 .01 Corn, sweet, kernel plus cob with husks re- moved ...... 0 .01 Wheat, straw ...... 0 .03 Corn, sweet, stover ...... 25 Cotton gin byproducts ...... 60 (b) Section 18 emergency exemptions. Cotton, undelinted seed ...... 0 .90 [Reserved] Fruit, pome, group 11 ...... 1.5 Fruit, stone, group 12 ...... 1 .6 (c) Tolerances with regional registra- Grape ...... 1 .4 tions. [Reserved] Nut, tree, group 14 ...... 0 .06 Okra ...... 0.30 (d) Indirect or inadvertent residues. Vegetable, cucurbit, group 9 ...... 0.20 [Reserved] Vegetable, fruiting, group 8 ...... 0.60 Vegetable, leafy, except Brassica, group 4 ...... 11 [73 FR 10402, Feb. 27, 2008] (2) Tolerances are established for res- idues of flubendiamide, including its

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metabolites and degradates, in or on (b) Section 18 emergency exemptions. the commodities in the table below. [Reserved] Compliance with the tolerance levels (c) Tolerances with regional registra- specified in the table is to be deter- tions. [Reserved] mined by measuring only (d) Indirect or inadvertent residues. flubendiamide N2-[1,1-dimethyl-2- Tolerances are established for residues (methylsulfonyl)ethyl]-3-iodo-N1-[2- of flubendiamide, including its metabo- methyl-4-[1,2,2,2-tetrafluoro-1- lites and degradates, in or on the com- (trifluoromethyl)ethyl]phenyl]-1,2- modities in the table below. Compli- benzenedicarboxamide, in or on the fol- ance with the tolerance levels specified lowing commodities: in the table is to be determined by measuring only flubendiamide N2-[1, 1- Parts per Commodity million dimethyl-2-(methylsulfonyl)ethyl]-3- iodo-N1-[2-methyl-4- [1,2,2,2- Alfalfa, forage ...... 25 tetrafluoro-1- Alfalfa, hay ...... 65 (trifluoromethyl)ethyl]phenyl]-1, 2- Artichoke, globe ...... 1.6 Berry, low growing, subgroup 13–07G, except benzenedicarboxamide, in or on the fol- cranberry ...... 1.5 lowing commodities: Brassica, head and stem, subgroup 5A ...... 3 .0 Brassica, leafy greens, subgroup 5B ...... 25 Commodity Parts per Cattle, fat ...... 0.70 million Cattle, meat ...... 0 .08 Cattle, meat byproducts ...... 0.60 Barley, hay ...... 0 .04 Barley, straw ...... 0 .07 Egg ...... 0 .40 Buckwheat ...... 0 .07 Fruit, small fruit vine climbing except fuzzy Clover, forage ...... 0.15 kiwifruit, subgroup 13–07F ...... 1 .4 Clover, hay ...... 0.04 Goat, fat ...... 0 .70 Grass, forage ...... 0 .15 Goat, meat ...... 0.08 Grass, hay ...... 0 .04 Goat, meat byproducts ...... 0 .60 Millet, pearl, forage ...... 0 .15 Grain, aspirated grain fractions ...... 153 Millet, pearl, hay ...... 0.04 Hog, fat ...... 0 .15 Millet, proso, forage ...... 0 .15 Hog, meat ...... 0 .03 Millet, proso, hay ...... 0 .04 Hog, meat byproducts ...... 0 .15 Millet, proso, straw ...... 0 .07 Horse, fat ...... 0 .70 Oats, forage ...... 0 .15 Horse, meat ...... 0 .08 Oats, hay ...... 0.04 Horse, meat byproducts ...... 0 .60 Oats, straw ...... 0.07 Milk ...... 0.15 Rye, forage ...... 0 .15 Milk, fat ...... 1 .0 Rye, straw ...... 0 .07 Pea and bean, dried shelled, except soybean, Teosinte, forage ...... 0 .15 subgroup 6C ...... 0 .60 Teosinte, hay ...... 0 .04 Pea and bean, succulent shelled, subgroup 6B 0 .05 Teosinte, straw ...... 0.07 Peanut, hay ...... 60 Triticale, forage ...... 0 .15 Peanut, meal ...... 0 .03 Triticale, hay ...... 0 .04 Peanut, nutmeat ...... 0 .02 Triticale, straw ...... 0 .07 Peanut, refined oil ...... 0.03 Wheat, forage ...... 0 .15 Wheat, hay ...... 0 .03 Pistachio ...... 0.06 Wheat, straw ...... 0 .03 Poultry, fat ...... 3.0 Poultry, liver ...... 0 .60 Poultry, meat ...... 0 .10 [76 FR 16307, Mar. 23, 2011, as amended at 76 1 Rice, grain ...... 0 .50 FR 55273, Sept. 7, 2011; 77 FR 73945, Dec. 12, Safflower, seed ...... 5 .0 2012] Sheep, fat ...... 0 .70 Sheep, meat ...... 0.08 Sheep, meat byproducts ...... 0 .60 § 180.640 Pyridalyl; tolerances for resi- Sorghum, grain, forage ...... 12 dues. Sorghum, grain, grain ...... 5 .0 (a) General. Tolerances are estab- Sorghum, grain, stover ...... 14 Soybean, forage ...... 18 lished for residues of pyridalyl, pyri- Soybean, hay ...... 60 dine,2-[3-[2,6-dichloro-4-[(3,3-dichloro-2- Soybean, hulls ...... 0 .80 propenyl)oxy]phenoxy]propoxy]-5- Soybean, seed ...... 0 .25 Sugarcane, cane ...... 0.30 (trifluoromethyl, in or on the following Sunflower, seed ...... 5.0 raw agricultural commodities:) Turnip, greens ...... 25 Vegetable, foliage of legume, except soybean, Commodity Parts per subgroup 7A ...... 35 million Vegetable, legume, edible podded, subgroup 6A ...... 0 .50 Brassica, head and stem, subgroup 5A ...... 3 .5 Mustard greens ...... 30 1 There are no U.S. registrations for rice, grain. Turnip greens ...... 30

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Parts per Parts per Commodity million Commodity million

Vegetable, fruiting, group 8 ...... 1.0 Grape, raisin ...... 3 .0 Vegetables, leafy, except Brassica, group 4 ...... 20 Guava ...... 2 .5 Hop, dried cones ...... 10 .0 (b) Section 18 emergency exemptions. Jaboticaba ...... 2 .5 Longan ...... 13 .0 [Reserved] Lychee ...... 13.0 (c) Tolerances with regional registra- Mamey sapote ...... 0 .60 tions. [Reserved] Mango ...... 0.60 Nut, tree, group 14 ...... 0 .25 (d) Indirect or inadvertent residues. Papaya ...... 0 .40 [Reserved] Passionfruit ...... 2 .5 Persimmon ...... 2 .5 [73 FR 25533, May 7, 2008] Pineapple ...... 0.30 Pistachio ...... 0.25 § 180.641 Spirotetramat; tolerances for Pomegranate ...... 0 .50 residues. Potato, flakes ...... 1 .6 Pulasan ...... 13 .0 (a) General. (1) Tolerances are estab- Rambutan ...... 13 .0 lished for residues of the insecticide Sapodilla ...... 0 .60 Small fruit vine climbing subgroup, except fuzzy spirotetramat, including its metabo- kiwifruit, subgroup 13–07F ...... 1.3 lites and degradates, in or on the com- Soybean forage ...... 8.0 modities in the table below. Compli- Soybean hay ...... 16.0 ance with the tolerance levels specified Soybean seed ...... 5 .0 Spanish lime ...... 13 below is to be determined by measuring Star apple ...... 0 .60 only the sum of spirotetramat (cis-3- Starfruit ...... 2 .5 (2,5-dimethlyphenyl)-8-methoxy-2-oxo- Strawberry1 ...... 0 .40 Taro, leaves ...... 9 .0 1-azaspiro[4.5]dec-3-en-4-yl-ethyl car- Vegetable, bulb, group 3–07 ...... 0 .80 bonate) and its metabolites cis-3-(2,5- Vegetable, cucurbit, group 9 ...... 0.30 dimethylphenyl)-4-hydroxy-8-methoxy- Vegetable, foliage of legume, except soybean, subgroup 07A ...... 7 .0 1-azaspiro[4.5]dec-3-en-2-one, cis-3-(2,5- Vegetable, fruiting, group 8–10 ...... 2 .5 dimethylphenyl)-3-hydroxy-8-methoxy- Vegetable, leafy, except brassica, group 4 ...... 9 .0 1-azaspiro[4.5]decane-2,4-dione, cis-3- Vegetable, legume, group 06, except soybean .. 2 .5 Vegetable, tuberous and corm, subgroup 1C ..... 0.60 (2,5-dimethylphenyl)-8-methoxy-2-oxo- Watercress ...... 2 .0 1-azaspiro[4.5]dec-3-en-4-yl beta-D-glu- Wax jambu ...... 2 .5 copyranoside, and cis-3-(2,5- White sapote ...... 0 .60 dimethylphenyl)-4-hydroxy-8-methoxy- 1 Import tolerance only. There are no U.S. registrations for 1-azaspiro[4.5]decan-2-one, calculated cotton or strawberry. as the stoichiometric equivalent of (2) Tolerances are also established for spirotetramat, in or on the following residues of the insecticide commodities. spirotetramat, including its metabo- lites and degradates, in or on the com- Parts per Commodity million modities in the table below. Compli- ance with the tolerance levels specified Acerola ...... 2.5 Almond, hulls ...... 9 .0 below is to be determined by measuring Artichoke, globe ...... 1.5 only the sum of spirotetramat (cis-3- Aspirated grain fractions ...... 10 .0 (2,5-dimethlyphenyl)-8-methoxy-2-oxo- Avocado ...... 0 .60 1-azaspiro[4.5]dec-3-en-4-yl-ethyl car- Berry, low growing, except strawberry, subgroup 13–07H ...... 0 .30 bonate]) and its metabolite cis-3-(2,5- Black sapote ...... 0 .60 dimethylphenyl)-4-hydroxy-8-methoxy- Brassica, head and stem, subgroup 5A ...... 2 .5 1-azaspiro[4.5]dec-3-en-2-one, calculated Brassica, leafy, subgroup 5B ...... 8 .0 Bushberry subgroup 13–07B ...... 3 .0 as the stoichiometric equivalent of Canistel ...... 0 .60 spirotetramat, in or on the following Citrus, oil ...... 6.0 commodities: Coffee, green bean ...... 0 .20 Coffee, instant ...... 0 .50 Parts per Corn, sweet, kernel plus cob with husks re- Commodity million moved ...... 1 .5 Cotton gin byproducts1 ...... 10 .0 Cattle, fat ...... 0.02 Cotton, undelinted seed1 ...... 0 .30 Cattle, meat ...... 0 .02 Feijoa ...... 2 .5 Cattle, meat byproducts ...... 0.20 Fruit, citrus, group 10–10 ...... 0 .60 Eggs ...... 0 .02 Fruit, pome, group 11–10 ...... 0 .70 Goat, fat ...... 0 .02 Fruit, stone, group 12 ...... 4 .5 Goat, meat ...... 0.02

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ant to FIFRA section 18 emergency ex- Commodity Parts per million emptions. The tolerances expire and Goat, meat byproducts ...... 0 .20 are revoked on the date specified in the Hog, meat byproducts ...... 0 .02 following table. Horse, fat ...... 0 .02 Horse, meat ...... 0 .02 Parts per Expiration/ Horse, meat byproducts ...... 0 .20 Commodity million revocation Milk ...... 0.01 date Poultry, meat byproducts ...... 0.02 Sheep, fat ...... 0 .02 Apple ...... 0.10 12/31/10 Sheep, meat ...... 0.02 Sheep, meat byproducts ...... 0 .20 (c) Tolerance with regional restrictions. [Reserved] (b) Section 18 emergency exemptions. (d) Indirect or inadvertant residues. [Reserved] [Reserved] (c) Tolerances with regional registra- tions. Tolerances with regional reg- [73 FR 44162, July 30, 2008] istrations are established for residues of the insecticide spirotetramat, in- § 180.643 Uniconazole; tolerances for residues. cluding its metabolites and degradates, in or on the commodities in the table (a) General. Tolerances are estab- below. Compliance with the tolerance lished for residues of the fungicide/ levels specified below is to be deter- plant growth regulator uniconazole-P, mined by measuring only the sum of (E)-(S)-1-(4-chlorophenyl)-4,4-dimethyl- spirotetramat (cis-3-(2,5- 2-(1H-1,2,4-triazol-1-yl)pent-1-en-3-ol, dimethlyphenyl)-8-methoxy-2-oxo-1- its R-enantiomer and its Z-isomer in or azaspiro[4.5]dec-3-en-4-yl-ethyl car- on the following raw agricultural com- bonate) and its metabolites cis-3-(2,5- modities: dimethylphenyl)-4-hydroxy-8-methoxy- Parts per 1-azaspiro[4.5]dec-3-en-2-one, cis-3-(2,5- Commodity million dimethylphenyl)-3-hydroxy-8-methoxy- 1-azaspiro[4.5]decane-2,4-dione, cis-3- Vegetable, fruiting, group 8 ...... 0.01 (2,5-dimethylphenyl)-8-methoxy-2-oxo- (b) Section 18 emergency exemptions. 1-azaspiro[4.5]dec-3-en-4-yl beta-D-glu- [Reserved] copyranoside, and cis-3-(2,5- dimethylphenyl)-4-hydroxy-8-methoxy- (c) Tolerances with regional registra- 1-azaspiro[4.5]decan-2-one, calculated tions. [Reserved] as the stoichiometric equivalent of (d) Indirect or inadvertant residues. spirotetramat, in or on the following [Reserved] commodities. [73 FR 51736, Sept. 5, 2008]

Commodity Parts per § 180.644 Cyprosulfamide; tolerances million for residues. Banana ...... 4.0 (a) General. (1) Tolerances are estab- lished for residues of the herbicide (d) Indirect or inadvertant residues. safener cyprosulfamide, N-[[4- [Reserved] [(cyclopropylamino)carbonyl] [73 FR 39256, July 9, 2008, as amended at 76 phenyl]sulfonyl]-2-methoxybenzamide, FR 28681, May 18, 2011; 77 FR 8746, Feb. 15, in or on the following raw agricultural 2012; 77 FR 75859, Dec. 26, 2012; 78 FR 28512, commodities: May 15, 2013; 78 FR 66651, Nov. 6, 2013] Parts per § 180.642 Gentamicin; tolerances for Commodity million residues. Corn, field, forage ...... 0 .20 (a) General. [Reserved] Corn, field, grain ...... 0 .01 (b) Section 18 emergency exemptions. Corn, field, stover ...... 0 .20 Corn, pop, grain ...... 0.01 Time-limited tolerances specified in Corn, pop, stover ...... 0.20 the following table are established for Corn, sweet, forage ...... 0 .40 residues of gentamicin in or on the Corn, sweet, kernel plus cob with husks re- specified agricultural commodities, re- moved ...... 0 .01 sulting from use of the pesticide pursu- Corn, sweet, stover ...... 0 .35

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(2) Tolerances are established for res- Commodity Parts per idues of the herbicide safener million cyprosulfamide, N-[[4- Cattle, meat ...... 0 .02 [(cyclopropylamino)carbonyl] Cattle, meat byproducts ...... 0.02 phenyl]sulfonyl]-2-methoxybenzamide, Goat, meat ...... 0.02 and its metabolite 4-(aminosulfonyl)-N- Goat, meat byproducts ...... 0 .02 Horse, meat ...... 0 .02 cyclopropylbenzamide, calculated as Horse, meat byproducts ...... 0 .02 cyprosulfamide, in or on the following Milk ...... 0.02 raw agricultural commodities: Sheep, meat ...... 0.02 Sheep, meat byproducts ...... 0 .02 Parts per Commodity million (b) Section 18 emergency exemptions. [Reserved] Cattle, meat byproducts ...... 0.02 Goat, meat byproducts ...... 0 .02 (c) Tolerances with regional registra- Horse, meat byproducts ...... 0 .02 tions. [Reserved] Sheep, meat byproducts ...... 0 .02 (d) Indirect or inadvertent residues. Tolerances are established for indirect (b) Section 18 emergency exemptions. or inadvertent combined residues of [Reserved] thiencarbazone-methyl and its metabo- (c) Tolerances with regional registra- lite BYH 18636-MMT-glucoside [2- tions. [Reserved] hexopyranosyl-5-methoxy-4-methyl-2,4- (d) Indirect or inadvertant residues. dihydro-3H-1,2,4-triazol-3-one], cal- [Reserved] culated as the parent compound, in or on the following food commodities: [73 FR 60974, Oct. 15, 2008] Commodity Parts per § 180.645 Thiencarbazone-methyl; tol- million erances for residues. Soybean, forage ...... 0 .04 (a) General. (1) Tolerances are estab- Soybean, hay ...... 0 .15 lished for residues of thiencarbazone- methyl [methyl 4-[[[(4,5-dihydro-3- [73 FR 60968, Oct. 15, 2008] methoxy-4-methyl-5-oxo-1H-1,2,4- triazol-1-yl)-carbonyl]amino]sulfonyl]- § 180.646 Ipconazole; tolerances for 5-methyl-3-thiophenecarboxylate], per residues. se, in or on the following food and feed (a) General. Tolerances are estab- commodities: lished for residues of ipconazole, in- cluding its metabolites and degradates, Parts per in or on the commodities listed in the Commodity million table below. Compliance with the toler- Corn, field, forage ...... 0 .04 ance levels specified below is to be de- Corn, field, grain ...... 0 .01 termined by measuring only ipconazole Corn, field, stover ...... 0 .02 (2-[(4-chlorophenyl)methyl]-5-(1- Corn, pop, grain ...... 0.01 methylethyl)-1-(1H-1,2,4-triazol-1- Corn, pop, stover ...... 0.01 Corn, sweet, forage ...... 0 .05 ylmethyl)cyclopentanol) in or on the Corn, sweet, kernel plus cob with husks re- commodity. moved ...... 0 .01 Corn, sweet, stover ...... 0 .05 Parts per Commodity million Wheat, forage ...... 0 .10 Wheat, grain ...... 0 .01 Cotton, gin byproducts ...... 0 .01 Wheat, hay ...... 0 .01 Cotton, undelinted seed ...... 0 .01 Wheat, straw ...... 0 .01 Grain, cereal, forage, fodder and straw, group 16, except rice ...... 0 .01 (2) Tolerances are established for Grain, cereal group 15, except rice ...... 0.01 Peanut ...... 0 .01 combined residues of thiencarbazone- Soybean, forage ...... 0 .01 methyl and its metabolite BYH 18636- Vegetable, legume, group 6 ...... 0 .01 MMT [5-methoxy-4-methyl-2,4-dihydro- 3H-1,2,4-triazol-3-one], calculated as the (b) Section 18 emergency exemptions. parent compound, in or on the fol- [Reserved] lowing food commodities of animal ori- (c) Tolerances with regional registra- gin: tions. [Reserved]

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(d) Indirect or inadvertent residues. dihydro-1(2H)-pyrimidinyl)-4- [Reserved] fluorobenzoyl]-N′-isopropylsulfamide and N-[4-chloro-2-fluoro-5-({ [73 FR 69559, Nov. 19, 2008, as amended at 79 FR 15240, Mar. 19, 2014] [(isopropylamino)sulfonyl] amino}carbonyl)phenyl]urea, cal- § 180.647 d-Phenothrin; tolerances for culated as the stoichiometric equiva- residues. lent of saflufenacil, in or on the com- (a) General. A tolerance of 0.01 parts modities. per million is established for residues Parts per of the insecticide d-phenothrin in or on Commodity million all food/feed crops following wide-area Alfalfa, forage ...... 0.08 mosquito adulticide applications. Alfalfa, hay ...... 0.10 (b) Section 18 emergency exemptions. Almond, hulls ...... 0 .10 [Reserved] Banana 1 ...... 0.03 (c) Tolerances with regional registra- Barley, bran ...... 1 .5 Barley, grain ...... 1 .0 tions. [Reserved] Barley, straw ...... 15 (d) Indirect or inadvertent residues. Coffee, green bean 1 ...... 0 .03 [Reserved] Cotton, gin byproducts ...... 0 .45 Cottonseed subgroup 20C ...... 0 .20 [74 FR 32443, July 8, 2009] Fruit, citrus, group 10 ...... 0 .03 Fruit, pome, group 11 ...... 0.03 § 180.648 Meptyldinocap; tolerances Fruit, stone, group 12 ...... 0 .03 for residues. Grain, aspirated grain fractions ...... 50 Grain, cereal, forage, fodder and straw group 16 (a) General. Tolerances are estab- (except barley and wheat straw) ...... 0 .10 lished for the combined residues of the Grain, cereal, group 15 (except barley and wheat grain) ...... 0 .03 fungicide meptyldinocap, 2-(1- Grape ...... 0 .03 methylheptyl)-4,6-dinitrophenyl (2E)-2- Grass, forage ...... 15 butenoate and 2,4-DNOP, 2,4-dinitro-6- Grass, hay ...... 20 (1-methylheptyl)phenol expressed as Grass, seed screenings ...... 0 .15 Grass, straw ...... 0 .15 meptyldinocap in or on the following Mango 1 ...... 0.03 commodities: Nut, tree, group 14 ...... 0 .03 Olive ...... 0 .03 Commodity Parts Per Mil- Pea and bean, dried shelled, except soybean, lion subgroup 6C ...... 0 .30 Pea and bean, succulent shelled, subgroup 6B 0 .03 Grape ...... 0.20 Pea, hay ...... 17 Pistachio ...... 0.03 (b) Section 18 emergency exemptions. Rapeseed subgroup 20A ...... 0 .45 [Reserved] Soybean, hulls ...... 0 .50 (c) Tolerances with regional registra- Soybean, seed ...... 0 .10 Sugarcane, cane 2 ...... 0.05 tions. [Reserved] Sugarcane, molasses 2 ...... 0 .08 (d) Indirect or inadvertent residues. Sunflower subgroup 20B ...... 1.0 [Reserved] Vegetable, foliage of legume, group 7 (except pea, hay) ...... 0.10 [74 FR 48396, Sept. 23, 2009] Vegetable, legume, edible podded, subgroup 6A 0 .03 Wheat, grain ...... 0 .60 § 180.649 Saflufenacil; tolerances for Wheat, straw ...... 6 .0 residues. 1 No U.S. registration as of December 7, 2011. 2 (a) General. (1) Tolerances are estab- No U.S. registration as of February 21, 2014. lished for residues of saflufenacil, in- (2) Tolerances are established for res- cluding its metabolites and degradates, idues of saflufenacil, including its me- in or on the commodities in the table tabolites and degradates, in or on the below. Compliance with the tolerance commodities in the table below. Com- levels specified below is to be deter- pliance with the tolerance levels speci- mined by measuring only the sum of fied below is to be determined by meas- saflufenacil, 2-chloro-5-[3,6-dihydro-3- uring only saflufenacil, 2-chloro-5-[3,6- methyl-2,6-dioxo-4-(trifluoromethyl)- dihydro-3-methyl-2,6-dioxo-4- 1(2H)-pyrimidinyl]-4-fluoro-N-[[meth- (trifluoromethyl)-1(2H)-pyrimidinyl]-4- yl(1-methylethyl)amino]sulfonyl]benz- fluoro-N-[[methyl(1-methylethyl) , and its metabolites N-[2-chloro- amino]sulfonyl]benzamide, in or on the 5-(2,6-dioxo-4-(trifluoromethyl)-3,6- commodities.

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Commodity Parts per § 180.651 Imazosulfuron; tolerances for million residues. Cattle, fat ...... 0.04 (a) General. Tolerances are estab- Cattle, liver ...... 50 Cattle, meat ...... 0 .02 lished for residues of the herbicide Cattle, meat byproducts, except liver ...... 0 .30 imazosulfuron, including its metabo- Fish-freshwater finfish ...... 0.01 lites and degradates, in or on the fol- Fish-shellfish, crustacean ...... 0 .01 Goat, fat ...... 0 .04 lowing commodities. Compliance with Goat, liver ...... 50 the tolerance levels specified in the fol- Goat, meat ...... 0.02 Goat, meat byproducts, except liver ...... 0 .30 lowing table below is to be determined Hog, fat ...... 0 .01 by measuring only imazosulfuron, 2- Hog, liver ...... 2 .0 chloro-N-[[(4,6-dimethoxy-2- Hog, meat ...... 0 .01 Hog, meat byproducts, except liver ...... 0 .02 pyrimidinyl)amino]carbonyl]imidazo- Horse, fat ...... 0 .04 [1,2-a]pyridine-3-sulfonamide, in or on Horse, liver ...... 50 the commodity. Horse, meat ...... 0 .02 Horse, meat byproducts, except liver ...... 0 .30 Milk ...... 0.01 Parts per Commodity million Sheep, fat ...... 0 .04 Sheep, liver ...... 50 Sheep, meat ...... 0.02 Melon subgroup 9A ...... 0 .02 Sheep, meat byproducts, except liver ...... 0 .30 Pepper, bell ...... 0 .02 Pepper, non-bell ...... 0.02 (b) Section 18 emergency exemptions. Rice, grain ...... 0 .02 [Reserved] Tomato ...... 0.02 Vegetable, tuberous and corm, subgroup 1C ..... 0.02 (c) Tolerances with regional registra- tions. [Reserved] (b) Section 18 emergency exemptions. (d) Indirect or inadvertent residues. [Reserved] [Reserved] (c) Tolerances with regional registra- [74 FR 46689, Sept. 11, 2009, as amended at 76 tions. [Reserved] FR 27261, May 11, 2011; 76 FR 76309, Dec. 7, (d) Indirect or inadvertent residues. 2011; 79 FR 9866, Feb. 21, 2014; 79 FR 52219, Sept. 3, 2014; 80 FR 22420, Apr. 22, 2015] [Reserved] [75 FR 81884, Dec. 29, 2010, as amended at 78 § 180.650 Isoxaben; tolerances for resi- FR 44444, July 24, 2013] dues. (a) General. Tolerances are estab- § 180.652 Ethiprole; tolerances for resi- lished for residues of the herbicide dues. isoxaben, including its metabolites and (a) General. Tolerances (without U.S. degradates, in or on the commodities registrations) are established for resi- in the table below. Compliance with dues of the insecticide ethiprole, in- the tolerance levels specified below is cluding its metabolites and degradate, to be determined by measuring only in or on the following commodities isoxaben, N-[3-(1-ethyl-1- listed in the table. Compliance with methylpropyl)-5-isoxazolyl]-2, 6- the tolerance levels specified in the dimethoxybenzamide, in or on the com- table is to be determined by measuring modity. only ethiprole [5-amino-1-[2,6-dichloro- 4-(trifluoromethyl)phenyl]-4-[(ethyl)- Commodity Parts per million sulfinyl]-1H-pyrazole-3-carbonitrile], in Almond, hulls ...... 0 .40 or on the following commodities: Grape ...... 0 .01 Nut, tree, Group 14 ...... 0.02 Commodity Parts per Pistachio ...... 0.02 million

(b) Section 18 emergency exemptions. Rice, grain 1 ...... 1 .7 Tea, dried 1 ...... 30 [Reserved] (c) Tolerances with regional registra- 1 There are no U.S. registrations for rice and tea. tions. [Reserved] (b) Section 18 emergency exemptions. (d) Indirect or inadvertent residues. [Reserved] [Reserved] (c) Tolerances with regional registra- [75 FR 69360, Nov. 12, 2010] tions. [Reserved]

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(d) Indirect or inadvertent residues. methylethyl)-1,4-methanonaphthalen- [Reserved] 5-yl]-1H-pyrazole-4-carboxamide) and anti-isomer (3-(difluoromethyl)-1-meth- [76 FR 18921, Apr. 6, 2011] yl-N-[(1RS, 4SR, 9SR)-1,2,3,4- § 180.653 Indaziflam; tolerances for tetrahydro-9-(1-methylethyl)-1,4- residues. methano-naphthalen-5-yl]-1H-pyrazole- (a) General. Tolerances are estab- 4-carboxamide) in or on the com- lished for residues of the herbicide modity. indaziflam, N-[(1R,2S)-2,3-dihydro-2,6- Parts per dimethyl-1H-inden-1-yl]-6-(1- Commodity million fluoroethyl)-1,3,5-triazine-2,4-diamine, Apple1 ...... 0 .70 including its metabolites and Banana1 ...... 0 .05 degradates, in or on the commodities Peanut1 ...... 0 .01 in the following table. Compliance with 1 There are no U.S. registrations for use of isopyrazam on the tolerance levels specified in the apple, banana, or peanut. table below is to be determined by (b) Section 18 emergency exemptions. measuring only indaziflam, in or on the [Reserved] commodity. (c) Tolerances with regional registra- tions. [Reserved] Parts per Commodity million (d) Indirect or inadvertent residues. [Reserved] Almond, hulls ...... 0 .15 Banana 1 ...... 0.01 [76 FR 61596, Oct. 5, 2011, as amended at 78 FR Coffee, green bean 1 ...... 0 .01 78745, Dec. 27, 2013] Fruit, citrus, group 10–10 ...... 0 .01 Fruit, pome, group 11–10 ...... 0 .01 Fruit, stone, group 12 ...... 0 .01 § 180.655 Flazasulfuron; tolerances for Grape ...... 0 .01 residues. Nut, tree, group 14 ...... 0 .01 Olive ...... 0 .01 (a) General. Tolerances are estab- Palm, oil 1 ...... 0 .03 lished for residues of flazasulfuron, in- Pistachio ...... 0.01 cluding its metabolites and degradates, 1 Sugarcane, refined sugar ...... 0 .01 in or on the commodities in the table 1 No U.S. Registrations as of 12/02/2013. below. Compliance with the tolerance 2 Tolerance without a corresponding U.S. registration. levels specified below is to be deter- (b) Section 18 emergency exemptions. mined by measuring only flazasulfuron [Reserved] (N-[[(4,6-dimethoxy-2- (c) Tolerances with regional registra- pyrimidinyl)amino]carbonyl]-3- tions. [Reserved] (trifluoromethyl)-2- (d) Indirect or inadvertent residues. pyridinesulfonamide). [Reserved] Parts per [76 FR 18905, Apr. 6, 2011, as amended at 79 Commodity million FR 4630, Jan. 29, 2014] Almond, hulls ...... 0 .01 Fruit, citrus, group 10–10 ...... 0 .01 § 180.654 Isopyrazam; tolerances for Grape ...... 0 .01 residues. Nut, tree, group 14–12 ...... 0 .01 (a) General. Tolerances are estab- Sugarcane ...... 0 .01 lished for residues of the fungicide isopyrazam, including its metabolites (b) Section 18 emergency exemptions. and degradates, in or on the commod- [Reserved] ities listed in the following table. Com- (c) Tolerances with regional registra- pliance with the tolerance levels speci- tions. [Reserved] fied in the following table is to be de- (d) Indirect or inadvertent residues. termined by measuring only [Reserved] isopyrazam (3-(difluoromethyl)-1-meth- [77 FR 10968, Feb. 24, 2012, as amended at 79 yl-N-[1,2,3,4-tetrahydro-9-(1- FR 52989, Sept. 5, 2014] methylethyl)-1,4-methano-naphthalen- 5-yl]-1H-pyrazole-4-carboxamide), as § 180.656 Amisulbrom; tolerances for the sum of its syn-isomer (3- residues. (difluoromethyl)-1-methyl-N-[(1RS, (a) General. Tolerances are estab- 4SR, 9RS)-1,2,3,4-tetrahydro-9-(1- lished for residues of the fungicide

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amisulbrom, including its metabolites (d) Indirect or inadvertent residues. and degradates, in or on the commod- [Reserved] ities listed below. Compliance with the [77 FR 10386, Feb. 22, 2012, as amended at 79 tolerance levels is to be determined by FR 18810, Apr. 4, 2014] measuring only amisulbrom, 3-[(3- bromo-6-fluoro-2-methyl-1H-indole-1- § 180.658 Penthiopyrad; tolerances for yl) sulfonyl]-N, N-dimethyl-1H-1, 2, 4- residues. triazole-1-sulfonamide]. (a) General. (1) Tolerances are estab- lished for residues of penthiopyrad, in- 1 Parts per Commodity million cluding its metabolites and degradates, Grape ...... 0 .40 in or on the commodities in the table Grape, raisin ...... 1 .0 below. Compliance with the tolerance Tomato ...... 0.50 levels specified below is to be deter- Tomato, paste ...... 1 .2 mined by measuring only penthiopyrad 1 There is no U.S. registration for use of amisulbrom on (N-[2-(1,3-dimethylbutyl)-3-thienyl]-1- grape or tomato. methyl-3-(trifluoromethyl)-1H-pyr- (b) Section 18 emergency exemptions. azole-4-carboxamide). [Reserved] (c) Tolerances with regional registra- Parts per Commodity million tions. [Reserved] (d) Indirect or inadvertent residues. Alfalfa, forage ...... 7.0 [Reserved] Alfalfa, hay ...... 20 Almond, hulls ...... 6 .0 [76 FR 59914, Sept. 28, 2011] Apple, wet pomace ...... 1 .5 Barley, grain ...... 0 .15 Barley, hay ...... 80 § 180.657 Metaflumizone; tolerances Barley, milled byproducts ...... 0.90 for residues. Barley, straw ...... 1 .0 (a) General. Tolerances are estab- Beet, sugar, dried pulp ...... 1 .5 Beet, sugar, roots ...... 0 .5 lished for residues of the insecticide Berry, low growing, subgroup 13–07G ...... 3 .0 metaflumizone, including its metabo- Brassica, head and stem, subgroup 5A ...... 5 .0 lites and degradates, in or on the com- Brassica, leafy greens, subgroup 5B ...... 50 modities listed in the following table. Buckwheat, grain ...... 0.15 Canola ...... 1 .5 Compliance with the tolerance levels Corn, field, forage ...... 40 specified in the following table is to be Corn, field, grain ...... 0 .01 determined by measuring only the sum Corn, field, refined oil ...... 0 .05 Corn, field, stover ...... 15 of metaflumizone (E and Z isomers; 2- Corn, pop, grain ...... 0.01 [2-(4-cyanophenyl)-1-[3- Corn, sweet, kernel plus cob with husks re- (trifluoromethyl) phenyl]ethylidene]- moved ...... 0 .01 N-[4-(trifluoromethoxy)phenyl] Cotton, seed ...... 1.5 Cotton, gin byproducts ...... 15 hydrazinecarboxamide) and its metabo- Fruit, pome, group 11–10 ...... 0 .50 lite 4-{2-oxo-2-[3-(trifluoromethyl) Fruit, stone, group 12 ...... 4 .0 phenyl]ethyl}-benzonitrile, calculated Grain, aspirated fractions ...... 30 Millet, spp...... 0 .80 as the stoichiometric equivalent of Nut, tree, group 14 ...... 0 .06 metaflumizone, in or on the following Oat, forage ...... 40 commodities: Oat, grain ...... 0 .15 Oat, hay ...... 80 Parts per Oat, straw ...... 1.0 Commodity million Pea and bean, dried shelled, except soybean, subgroup 6C ...... 0 .40 Almond, hulls ...... 0 .04 Peanut ...... 0 .04 Eggplant 1 ...... 1.5 Peanut, hay ...... 30 Fruit, citrus, group 10 ...... 0 .04 Peanut, refined oil ...... 0.06 Grape ...... 0 .04 Pistachio ...... 0.06 Nut, tree, group 14 ...... 0 .04 Potato, processed potato waste ...... 0 .20 Pepper 1 ...... 1 .5 Rye, forage ...... 40 Tomato 1 ...... 0.60 Rye, grain ...... 0.15 Tomato, paste 1 ...... 1 .2 Rye, straw ...... 1 .0 1 There are no U.S. registrations as of April 4, 2014. Sorghum, forage ...... 40 Sorghum, grain, grain ...... 0 .80 (b) Section 18 emergency exemptions. Sorghum, stover ...... 15 [Reserved] Soybean, seed ...... 0 .40 Sunflower, seed ...... 1.5 (c) Tolerances with regional registra- Teosinte, grain ...... 0 .15 tions. [Reserved] Tomato, paste ...... 3 .5

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Commodity Parts per § 180.659 Pyroxasulfone; tolerances for million residues. Triticale, forage ...... 40 (a) General. (1) Tolerances are estab- Triticale, grain ...... 0 .15 lished for residues of the herbicide Triticale, hay ...... 80 Triticale, straw ...... 1 .0 pyroxasulfone, including its metabo- Vegetable, bulb, group 3–07 ...... 3 .0 lites and degradates, in or on the com- Vegetable, cucurbit, group 9 ...... 0.60 modities in the table below. Compli- Vegetable, foliage of legume, group 7, hay ...... 200 ance with the tolerance levels specified Vegetable, foliage of legume, group 7, vines/for- below is to be determined by measuring age ...... 50 Vegetable, fruiting, group 8–10 ...... 3 .0 only the sum of pyroxasulfone, 3-[[[5- Vegetable, leafy, except brassica, group 4 ...... 30 (difluoromethoxy)-1-methyl-3- Vegetable, leaves of root and tuber, group 2 ..... 50 (trifluoromethyl)-1H-pyrazol-4- Vegetable, legume, edible podded, subgroup 6A 4 .0 yl]methyl]sulfonyl]-4,5-dihydro-5,5- Vegetable, legume, succulent shelled, subgroup 6B ...... 0 .40 dimethylisoxazole, and its metabolite, Vegetable, root, subgroup 1B, except sugar 5-(difluoromethoxy)-1-methyl-3- beet ...... 3 .0 (trifluoromethyl)-1H-pyrazol-4-car- Vegetable, tuber and corm, subgroup 1C ...... 0 .06 boxylic acid (M-3), calculated as the Wheat, forage ...... 40 Wheat, grain ...... 0 .15 stoichiometric equivalent of Wheat, hay ...... 80 pyroxasulfone, in or on the commodity. Wheat, milled byproducts ...... 0 .30 Wheat, straw ...... 1 .0 Parts per Commodity million

(2) Tolerances are established for res- Corn, field, grain ...... 0 .02 idues of penthiopyrad, including its Corn, pop, grain ...... 0.015 metabolites and degradates, in or on Corn, sweet, kernel plus cob with husks re- moved ...... 0 .015 the commodities in the table below. Cotton, undelinted seed ...... 0 .04 Compliance with the tolerance levels Wheat, grain ...... 0 .03 specified below is to be determined by measuring only the sum of (2) Tolerances are established for res- penthiopyrad (N-[2-(1,3-dimethylbutyl)- idues of the herbicide pyroxasulfone, 3-thienyl]-1-methyl-3- including its metabolites and (trifluoromethyl)-1H-pyrazole-4- degradates, in or on the commodities carboxamide) and its metabolite (1- in the table below. Compliance with methyl-3-trifluoromethyl-1H-pyrazole- the tolerance levels specified below is 4-carboxamide), calculated as the stoi- to be determined by measuring only chiometric equivalent of penthiopyrad, the sum of pyroxasulfone, 3-[[[5- in or on the commodity. (difluoromethoxy)-1-methyl-3- (trifluoromethyl)-1H-pyrazol-4- Commodity Parts per yl]methyl]sulfonyl]-4,5-dihydro-5,5- million dimethylisoxazole, and its metabolites, Cattle, fat ...... 0.03 5-(difluoromethoxy)-1-methyl-3- Cattle, meat ...... 0 .03 (trifluoromethyl)-1H-pyrazol-4- Cattle, meat byproducts ...... 0.09 yl]methanesulfonic acid (M–1); 5- Goat, fat ...... 0 .03 Goat, meat ...... 0.03 (difluoromethoxy)-1-methyl-3- Goat, meat byproducts ...... 0 .09 (trifluoromethyl)-1H-pyrazol-4-car- Horse, fat ...... 0 .03 boxylic acid (M-3); and [5- Horse, meat ...... 0 .03 (difluoromethoxy)-3-(trifluoromethyl)- Horse, meat byproducts ...... 0 .09 Milk ...... 0.02 1H-pyrazol-4-yl]methanesulfonic acid Sheep, fat ...... 0 .03 (M-25), calculated as the stoichiometric Sheep, meat ...... 0.03 equivalent of pyroxasulfone, in or on Sheep, meat byproducts ...... 0 .09 the commodity.

(b) Section 18 emergency exemptions. Commodity Parts per [Reserved] million (c) Tolerances with regional registra- Corn, field, forage ...... 0 .09 tions. [Reserved] Corn, field, stover ...... 0 .15 Corn, pop, stover ...... 0.15 (d) Indirect or inadvertent residues. Corn, sweet, forage ...... 0 .10 [Reserved] Corn, sweet, stover ...... 0 .15 Cotton, gin byproducts ...... 0 .20 [77 FR 14297, Mar. 9, 2012] Soybean, forage ...... 1 .0

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(b) Section 18 emergency exemptions. Commodity Parts per million [Reserved] Soybean, hay ...... 2 .0 (c) Tolerances with regional registra- Wheat, forage ...... 6 .0 tions. [Reserved] Wheat, hay ...... 1 .0 (d) Indirect or inadvertent residues. Wheat, straw ...... 0 .60 [Reserved] (3) Tolerances are established for res- [77 FR 12213, Feb. 29, 2012, as amended at 78 idues of the herbicide pyroxasulfone, FR 13257, Feb. 27, 2013; 78 FR 46279, July 31, including its metabolites and 2013; 79 FR 34633, June 18, 2014] degradates, in or on the commodities in the table below. Compliance with § 180.660 Pyriofenone; tolerances for the tolerance levels specified below is residues. to be determined by measuring only (a) General. Tolerances are estab- the sum of pyroxasulfone, 3-[[[5- lished for residues of the fungicide (difluoromethoxy)-1-methyl-3- pyriofenone, including its metabolites (trifluoromethyl)-1H-pyrazol-4- and degradates, in or on the following yl]methyl]sulfonyl]-4,5-dihydro-5,5- commodities listed in the table. Com- dimethylisoxazole, and its metabolites, pliance with the tolerance levels speci- 5-(difluoromethoxy)-1-methyl-3- fied in the table is to be determined by (trifluoromethyl)-1H-pyrazol-4-car- measuring only pyriofenone, (5-chloro- boxylic acid (M–3); [5- 2-methoxy-4-methyl-3-pyridinyl)(2,3,4- (difluoromethoxy)-3-(trifluoromethyl)- trimethoxy-6-methylphenyl) 1H-pyrazol-4-yl]methanesulfonic acid methanone, in or on the following com- (M–25); and 3-[1-carboxy-2-(5,5-di- modities: methyl-4,5-dihydroisoxazol-3- Parts per ylthio)ethylamino]-3-oxopropanoic acid Commodity million (M–28), calculated as the stoichio- metric equivalent of pyroxasulfone, in Grape 1 ...... 0 .30 Grape, raisin 1 ...... 0 .50 or on the commodity. 1 There are no U.S. registrations for grape and grape, raisin. Commodity Parts per million (b) Section 18 emergency exemptions. Soybean, seed ...... 0 .06 [Reserved] (c) Tolerances with regional registra- (4) Tolerances are established for res- tions. [Reserved] idues of the herbicide pyroxasulfone, (d) Indirect or inadvertent residues. including its metabolites and [Reserved] degradates, in or on the commodities [77 FR 13506, Mar. 7, 2012] in the following table. Compliance with the tolerance levels specified in the fol- § 180.661 Fluopyram; tolerances for lowing table is to be determined by residues. measuring only the sum of (a) General. (1) Tolerances are estab- pyroxasulfone [3-[[[5- lished for residues of the fungicide (difluoromethoxy)-1-methyl-3- Fluopyram, N-[2-[3-chloro-5- (trifluoromethyl)-1H-pyrazol-4- (trifluoromethyl)-2-pyridinyl]ethyl]-2- yl]methyl]sulfonyl]-4,5-dihydro-5,5- (trifluoromethyl)benzamide, including dimethylisoxazole] and its metabolites its metabolites and degradates in or on [5-(difluoromethoxy)-1-methyl-3- the commodities in the table below. (trifluoromethyl)-1H-pyrazol-4- Compliance with the tolerance levels yl]methanesulfonic acid (M–1) and 5- specified in the table is to be deter- (difluoromethoxy)-1-methyl-3- mined by measuring only fluopyram in (trifluoromethyl)-1H-pyrazol-4-car- or on the commodity. boxylic acid (M–3), calculated as the stoichiometric equivalent of Commodity Parts pyroxasulfone, in or on the commodity. per million Almond, hull ...... 8 .0 Parts per Commodity million Apple ...... 0.30 Apple, wet pomace ...... 0 .60 1 Milk ...... 0.003 Banana ...... 1.0 Bean, dry ...... 0.09

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Compliance with the tolerance levels Commodity Parts per million specified in the table is to be deter- Beet, sugar, root ...... 0 .04 mined by measuring only fluopyram in Cotton, gin byproducts ...... 0 .70 or on the commodity. Cotton, undelinted seed ...... 0 .01 Cherry ...... 0.60 Parts per Grape, wine ...... 2 .0 Commodity million Nut, tree, group 14 ...... 0 .05 Peanut ...... 0 .09 Alfalfa, forage ...... 0.45 Pistachio ...... 0.05 Alfalfa, hay ...... 1.1 Potato ...... 0 .02 Canola, seed ...... 1 .8 Potato, processed potato waste ...... 0 .08 Grain, cereal, except rice, group 15 ...... 0 .03 Soybean, seed ...... 0 .04 Grain, cereal, forage, fodder and straw, group Strawberry ...... 1 .5 16 ...... 2 .0 Watermelon ...... 1.0 Soybean, forage ...... 4 .0 Soybean, hay ...... 15 1 There are no U.S. registrations. Soybean, seed ...... 0 .10 (2) Tolerances are established for res- idues of the fungicide fluopyram, N-[2- [77 FR 10975, Feb. 24, 2012, as amended at 79 [3-chloro-5-(trifluoromethyl)-2- FR 75065, Dec. 17, 2014] pyridinyl]ethyl]-2- (trifluoromethyl)benzamide, including § 180.662 Trinexapac-ethyl; tolerances its metabolites and degradates. Com- for residues. pliance with the tolerance levels speci- (a) General. Tolerances are estab- fied in the table below is to be deter- lished for residues of the plant growth mined by measuring only the sum of inhibitor, trinexapac-ethyl, including fluopyram and its metabolite, 2- its metabolites and degradates, in or (trifluoromethyl)benzamide, calculated on the commodities in the table below. as the stoichiometric equivalent of Compliance with the tolerance levels fluopyram, in or on the commodity. specified below is to be determined by measuring both trinexapac-ethyl, ethyl Parts per Commodity million 4-(cyclopropylhydroxymethylene)-3,5- dioxocyclohexanecarboxylate and the Cattle, fat ...... 0.05 associated metabolite, trinexpac, 4- Cattle, meat ...... 0 .05 Cattle, meat byproducts ...... 0.40 (cyclopropylhydroxymethylene)-3,5- Egg ...... 0 .06 dioxocyclohexanecarboxylic acid, cal- Goat, fat ...... 0 .11 culated as the stoichiometric equiva- Goat, meat ...... 0.15 Goat, meat byproducts ...... 1 .1 lent of trinexapac-ethyl, in or on the Hog, fat ...... 0 .02 commodity. Hog, meat ...... 0 .02 Hog, meat byproducts ...... 0 .03 Parts per Horse, fat ...... 0 .11 Commodity million Horse, meat ...... 0 .15 Horse, meat byproducts ...... 1 .1 Barley, bran ...... 2 .5 Milk ...... 0.06 Barley, grain ...... 2 .0 Poultry, fat ...... 0.03 Barley, hay ...... 0 .8 Poultry, meat ...... 0 .03 Barley, straw ...... 0 .4 Poultry, meat byproducts ...... 0.10 Cattle, fat ...... 0.02 Sheep, fat ...... 0 .11 Cattle, meat ...... 0 .02 Sheep, meat ...... 0.15 Cattle, meat byproducts ...... 0.04 Sheep, meat byproducts ...... 1 .1 Goat, fat ...... 0 .02 Goat, meat ...... 0.02 (b) Section 18 emergency exemptions. Goat, meat byproducts ...... 0 .04 Grass, forage ...... 1 .5 [Reserved] Grass, hay ...... 4 .0 (c) Tolerances with regional registra- Grass, seed screenings ...... 40.0 tions. [Reserved] Grass, straw ...... 10 .0 Hog, fat ...... 0 .02 (d) Indirect or inadvertent residues. It Hog, meat ...... 0 .02 is recommended that tolerances be es- Hog, meat by-products ...... 0 .03 tablished for indirect or inadvertent Horse, fat ...... 0 .02 residues of fungicide fluopyram, N-[2- Horse, meat ...... 0 .02 Horse, meat byproducts ...... 0 .04 [3-chloro-5-(trifluoromethyl)-2- Oat, forage ...... 1 .0 pyridinyl]ethyl]-2- Oat, grain ...... 4 .0 (trifluoromethyl)benzamide, including Oat, hay ...... 1.5 Oat, straw ...... 0.9 its metabolites and degradates, in or Rice, bran ...... 1.5 on the commodities in the table below. Rice, grain ...... 0 .4

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(d) Indirect or inadvertent residues. Commodity Parts per million [Reserved] Rice, straw ...... 0 .07 [77 FR 21734, May 9, 2012] Rice, wild, grain ...... 0.4 Rye, bran ...... 6 .0 § 180.664 Penflufen; tolerances for resi- Rye, grain ...... 4.0 Rye, hay ...... 1 .5 dues. Rye, straw ...... 0 .9 (a) General. Tolerances are estab- Sheep, fat ...... 0 .02 lished for residues of the fungicide Sheep, meat ...... 0.02 Sheep, meat byproducts ...... 0 .04 penflufen, including its metabolites Sugarcane, cane ...... 0.8 and degradates, in or on the following Sugarcane, molasses ...... 2 .5 commodities listed in the table. Com- Wheat, bran ...... 6.0 pliance with the tolerance levels speci- Wheat, forage ...... 1 .0 Wheat, grain ...... 4 .0 fied in the table is to be determined by Wheat, hay ...... 1 .5 measuring only penflufen N-[2-(1,3- Wheat, middlings ...... 10 .5 dimethylbutyl)phenyl]-5-fluoro-1,3-di- Wheat, straw ...... 0 .9 methyl-1H-pyrazole-4-carboxamide, in or on the following commodities. (b) Section 18 emergency exemptions. [Reserved] Commodity Parts per (c) Tolerances with regional registra- million tions. [Reserved] Alfalfa, forage ...... 0.01 (d) Indirect or inadvertent residues. Alfalfa, hay ...... 0.01 Cotton, gin by-products ...... 0 .01 [Reserved] Grain cereal, forage, fodder and straw, group 16 ...... 0 .01 [77 FR 12745, Mar. 2, 2012, as amended at 77 Grain, cereal, group 15 ...... 0.01 FR 60919, Oct. 3, 2012; 80 FR 28848, May 20, Oilseed, group 20 ...... 0 .01 2015] Vegetable, foliage of legume, group 7 ...... 0 .01 Vegetable, legume, group 6 ...... 0 .01 § 180.663 Ametoctradin; tolerances for Vegetable, tuberous and corm subgroup 1C .... 0 .01 residues. (b) Section 18 emergency exemptions. (a) General. Tolerances are estab- [Reserved] lished for residues of the fungicide (c) Tolerances with regional registra- ametoctradin, including its metabo- tions. [Reserved] lites and degradates, in or on the com- (d) Indirect or inadvertent residues. modities in the following table. Com- [Reserved] pliance with the tolerance levels speci- fied in the following table is to be de- [77 FR 28281, May 14, 2012] termined by measuring only § 180.665 Sedaxane; tolerances for resi- ametoctradin (5-ethyl-6- dues. octyl[1,2,4]triazolo[1,5-a]pyrimidin-7- amine). (a) General. Tolerances are estab- lished for residues of the fungicide Commodity Parts per sedaxane, including its metabolites and million degradates, in or on the commodities Brassica, head and stem, subgroup 5A ...... 9 .0 in the following table. Compliance with Brassica, leafy greens, subgroup 5B ...... 50 the tolerance levels specified in the fol- Grape ...... 4 .0 lowing table is to be determined by Grape, raisin ...... 8 .0 ′ Hop, dried cones ...... 10 .0 measuring only sedaxane, N-[2-[1,1 - Onion, bulb, subgroup 3–07A ...... 1 .5 bicyclopropyl]-2-ylphenyl]-3- Onion, green, subgroup 3–07B ...... 20 .0 (difluoromethyl)-1-methyl-1H-pyrazole- Spinach ...... 50 .0 4-carboxamide, as the sum of its cis- Vegetable, cucurbit, group 9 ...... 3.0 and trans-isomers in or on the com- Vegetable, fruiting, group 8–10 ...... 1 .5 Vegetable, leafy, except Brassica, group 4, ex- modity. cept spinach ...... 40 .0 Vegetable, tuberous and corm, subgroup 1C ..... 0.05 Commodity Parts per million

(b) Section 18 emergency exemptions. Barley, grain ...... 0 .01 [Reserved] Barley, hay ...... 0 .04 Barley, straw ...... 0 .01 (c) Tolerances with regional registra- Canola, seed ...... 0 .01 tions. [Reserved] Corn, field, forage ...... 0 .01

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Parts per Parts per Commodity million Commodity million

Corn, field, grain ...... 0 .01 Bushberry, subgroup 13–07B ...... 7.0 Corn, field, stover ...... 0 .01 Caneberry, subgroup 13–07A ...... 5 .0 Corn, pop, grain ...... 0.01 Cattle, fat ...... 0.05 Corn, pop, stover ...... 0.01 Cattle, meat ...... 0 .01 Corn, sweet, forage ...... 0 .01 Cattle, meat byproducts ...... 0.03 Corn, sweet, kernel plus cob with husks re- Corn, field, grain ...... 0 .01 moved ...... 0 .01 Corn, oil ...... 0 .03 Corn, sweet, stover ...... 0 .01 Corn, pop, grain ...... 0.01 Oat, forage ...... 0 .015 Corn, sweet, kernels plus cobs with husks re- Oat, grain ...... 0 .01 moved ...... 0 .15 Oat, hay ...... 0.06 Cotton, gin byproducts ...... 0 .01 Oat, straw ...... 0.01 Cotton, undelinted seed ...... 0 .01 Pea and bean, dried shelled, except soybean, Egg ...... 0 .002 subgroup 6C ...... 0 .01 Fish-freshwater finfish ...... 0.01 Potato ...... 0 .02 Fish-shellfish, crustacean ...... 0 .01 Potato, wet peel ...... 0 .075 Fruit, pome, group 11 ...... 0.8 Rapeseed, subgroup 20A ...... 0.01 Fruit, small, vine climbing, except fuzzy Rye, forage ...... 0 .015 kiwifruit, subgroup 13–07F ...... 2 .0 Rye, grain ...... 0.01 Fruit, stone, group 12–12 ...... 3 .0 Rye, straw ...... 0 .01 Goat, fat ...... 0 .05 Sorghum, grain, forage ...... 0.01 Goat, meat ...... 0.01 Goat, meat byproducts ...... 0 .03 Sorghum, grain, grain ...... 0 .01 Grain, aspirated fractions ...... 20.0 Sorghum, grain, stover ...... 0 .01 Grain, cereal, forage, fodder and straw, group Soybean, forage ...... 0 .05 16 ...... 20 Soybean, hay ...... 0 .04 Grain, cereal, group 15, (except corn, field, Soybean, seed ...... 0 .01 grain; except corn, pop, grain; except corn, Vegetable, foliage of legume, except soybean, kernels plus cobs with husks removed; ex- subgroup 7A ...... 0 .01 cept rice; except wheat ...... 3 .0 Wheat, forage ...... 0 .015 Grape, raisin ...... 5 .7 Wheat, grain ...... 0 .01 Hog, meat byproducts ...... 0 .01 Wheat, hay ...... 0 .06 Horse, fat ...... 0 .05 Wheat, straw ...... 0 .01 Horse, meat ...... 0 .01 Horse, meat byproducts ...... 0 .03 (b) Section 18 emergency exemptions. Milk ...... 0.005 [Reserved] Nut, tree, group 14–12 ...... 0 .06 Oilseeds, group 20 (except cottonseed) ...... 0 .9 (c) Tolerances with regional registra- Pea and bean, dried shelled except soybean, tions. [Reserved] subgroup 6C ...... 0 .4 (d) Indirect inadvertent residues. [Re- Pea and bean, succulent shelled, subgroup 6B 0 .5 Peanut ...... 0 .01 served] Peanut, refined oil ...... 0.02 Plum, prune, dried ...... 3.0 [77 FR 36924, June 20, 2012, as amended at 78 Potato, wet peel ...... 0 .1 FR 33748, June 5, 2013; 78 FR 60719, Oct. 2, Rice, bran ...... 4.5 2013] Rice, bran ...... 8.5 Rice, grain ...... 5 .0 § 180.666 Fluxapyroxad; tolerances for Rice, hulls ...... 8 .0 Rice, hulls ...... 15 .0 residues. Sheep, fat ...... 0 .05 (a) General. Tolerances are estab- Sheep, meat ...... 0.01 Sheep, meat byproducts ...... 0 .03 lished for residues of the fungicide Soybean, hulls ...... 0 .3 fluxapyroxad, including its metabolites Soybean, seed ...... 0 .15 and degradates, in or on the commod- Sugarcane, cane ...... 3.0 Vegetable, brassica leafy, group 5 ...... 4 .0 ities listed in the table below. Compli- Vegetable, bulb, group 3–07 ...... 1 .5 ance with the tolerance levels specified Vegetable, cucurbit, group 9 ...... 0.50 below is to be determined by measuring Vegetable, foliage of legume, group 7 ...... 30 only fluxapyroxad, 3-(difluoromethyl)- Vegetables, fruiting, group 8 ...... 0.7 Vegetable, leafy, except brassica, group 4 ...... 30 1-methyl-N-(3′,4′,5′-trifluoro[1,1′- Vegetable, legume, edible podded, subgroup biphenyl]-2-yl)-1H-pyrazole-4- 6A ...... 2 .0 carboxamide in or on the commodity. Vegetable, root, except sugarbeet, subgroup 1B ...... 0.90 Vegetable, tuberous and corm, subgroup 1C ... 0.02 Parts per Commodity million Wheat, bran ...... 0.6 Wheat, grain ...... 0 .3 Almond, hulls ...... 4 .0 Apple, wet pomace ...... 2 .0 (b) Section 18 emergency exemptions. Beet, sugar ...... 0 .1 [Reserved] Beet, sugar, dried pulp ...... 0 .1 Beet, sugar, tops ...... 7.0 (c) Tolerances with regional registra- Berry, low growing, subgroup 13–07G ...... 4 .0 tions. [Reserved]

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(d) Indirect or inadvertent residues. sulfoxaflor, including its metabolites Tolerances are established for the com- and degradates, in or on the commod- bined indirect or inadvertent residues ities in the table. Compliance with the of the fungicide fluxapyroxad, includ- tolerance levels specified is to be deter- ing its metabolites and degradates, in mined by measuring only sulfoxaflor or on the commodities listed in the (N-[methyloxido[1-[6-(trifluoromethyl)- table below. Compliance with the toler- 3-pyridinyl]ethyl]-g4-sulfanylidene]cy- ance levels specified below is to be de- anamide). termined by measuring only Parts per fluxapyroxad, 3-(difluoromethyl)-1- Commodity million methyl-N-(3′,4′,5′-trifluoro[1,1′- biphenyl]-2-yl)-1H-pyrazole-4- Almond, hulls ...... 6 .0 Barley, grain ...... 0 .40 carboxamide in or on the commodity. Barley, hay ...... 1 .0 Barley, straw ...... 2 .0 Commodity Parts per Bean, dry seed ...... 0 .20 million Bean, succulent ...... 4 .0 Beet, sugar, dried pulp ...... 0 .07 Nongrass animal feeds, group18 ...... 0 .30 Beet, sugar, molasses ...... 0 .25 Peppermint, tops ...... 0 .01 Berry, low growing, subgroup 13–7G ...... 0 .70 Spearmint, tops ...... 0 .01 Cattle, fat ...... 0.10 Cattle, meat ...... 0 .15 Cattle, meat byproducts ...... 0.40 [77 FR 28275, May 14, 2012, as amended at 77 Cauliflower ...... 0 .08 FR 46307, Aug. 3, 2012; 79 FR 10677, Feb. 26, Citrus, dried pulp ...... 3 .6 2014] Cotton, gin byproducts ...... 6 .0 Cotton, hulls ...... 0 .35 § 180.667 Cyflufenamid, tolerance for Cottonseed subgroup 20C ...... 0 .20 residues. Fruit, citrus, group 10–10 ...... 0 .70 Fruit, pome, group 11–10 ...... 0 .50 (a) General. Tolerances are estab- Fruit, small, vine climbing, subgroup 13–07F, lished for residues of the fungicide except fuzzy kiwi fruit ...... 2.0 Fruit, stone, group 12 ...... 3 .0 cyflufenamid, including its metabolites Goat, fat ...... 0 .10 and degradates, in or on the commod- Goat, meat ...... 0.15 ities in the table below. Compliance Goat, meat byproducts ...... 0 .40 with the tolerance levels specified Grain, aspirated fractions ...... 20.0 Grape, raisin ...... 6 .0 below is to be determined by measuring Hog, fat ...... 0 .01 only cyflufenamid, [N(Z)]-N- Hog, meat ...... 0 .01 [[(cyclopropylmethoxy)amino][2,3- Hog, meat byproducts ...... 0 .01 Horse, fat ...... 0 .10 difluoro-6-(trifluoromethyl)phenyl] Horse, meat ...... 0 .15 methylene]benzeneacetamide. Horse, meat byproducts ...... 0 .40 Leafy greens, subgroup 4A ...... 6.0 Commodity Parts per Leafy petiole, subgroup 4B ...... 2 .0 million Milk ...... 0.15 Nuts, tree, group 14 ...... 0 .015 Apple, wet pomace ...... 0.10 Onion, bulb, subgroup 3–07A ...... 0 .01 Berry, low growing, subgroup 13–07G, except Onion, green, subgroup 3–07B ...... 0 .70 cranberry ...... 0.20 Pistachio ...... 0.015 Fruit, pome, group 11 ...... 0.06 Poultry, eggs ...... 0 .01 Fruit, small vine climbing, except fuzzy kiwifruit, Poultry, fat ...... 0.01 subgroup 13–07F ...... 0.15 Poultry, meat ...... 0 .01 Grape, raisin ...... 0.30 Poultry, meat byproducts ...... 0.01 Vegetable, cucurbit, group 9 ...... 0.07 Rapeseed, meal ...... 0 .50 Rapeseed subgroup 20A ...... 0 .40 (b) Section 18 emergency exemptions. Sheep, fat ...... 0 .10 [Reserved] Sheep, meat ...... 0.15 Sheep, meat byproducts ...... 0 .40 (c) Tolerances with regional registra- Soybean, seed ...... 0 .20 tions. [Reserved] Tomato, paste ...... 2 .60 (d) Indirect or inadvertent residues. Tomato, puree ...... 1 .20 Vegetable, brassica, leafy, group 5, except [Reserved] cauliflower ...... 2 .0 [77 FR 38210, June 27, 2012] Vegetable, cucurbit, group 9 ...... 0.40 Vegetable, fruiting, group 8–10 ...... 0 .70 Vegetable, leaves of root and tuber, group 2 ... 3 .0 § 180.668 Sulfoxaflor; tolerances for Vegetable, legume, foliage, group 7 ...... 3.0 residues. Vegetable, root and tuber, group 1 ...... 0 .05 Watercress ...... 6 .0 (a) General. Tolerances are estab- Wheat, forage ...... 1 .0 lished for residues of the insecticide Wheat, grain ...... 0 .08

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Parts per Parts per Commodity million Commodity million

Wheat, hay ...... 1 .5 Goat, meat ...... 0.01 Wheat, straw ...... 2 .0 Goat, meat byproducts ...... 0 .01 Grain, aspirated grain fractions ...... 10 (b) Section 18 emergency exemptions. Grain, cereal, forage, fodder, and straw, group 16, forage ...... 15 Time-limited tolerances specified in Grain, cereal, forage, fodder, and straw, group the following table are established for 16, hay ...... 5 residues of sulfoxaflor (N- Grain, cereal, forage, fodder, and straw, group [methyloxido[1-[6-(trifluoromethyl)-3- 16, stover ...... 10 Grain, cereal, forage, fodder, and straw, group 4 pyridinyl]ethyl]- λ - 16, straw ...... 2 sulfanylidene]cyanamide), including its Grain, cereal, group 15, except rice and barley 0 .04 metabolites and degradates, in or on Hog, fat ...... 0 .01 Hog, meat ...... 0 .01 the specified agricultural commodities, Hog, meat byproducts ...... 0 .01 resulting from use of the pesticide pur- Horse, fat ...... 0 .01 suant to FIFRA section 18 emergency Horse, meat ...... 0 .01 exemptions. Compliance with the toler- Horse, meat byproducts ...... 0 .01 Milk ...... 0.01 ance levels specified in the following Pea and bean, dried shelled, except soybean, table is to be determined by measuring subgroup 6C ...... 0 .06 only sulfoxaflor in or on the com- Poultry, fat ...... 0.01 modity. The tolerances expire on the Poultry, meat ...... 0 .01 Poultry, meat byproducts ...... 0.01 date specified in the table. Rapeseed subgroup 20A ...... 0 .08 Sheep, fat ...... 0 .01 Parts Expiration/ Sheep, meat ...... 0.01 Commodity per revocation million date Sheep, meat byproducts ...... 0 .01 Soybean, forage ...... 1 Sorghum, forage ...... 0.40 12/31/17 Soybean, hay ...... 3 Sorghum, grain ...... 0.30 12/31/17 Soybean, hulls ...... 0 .2 Sorghum, stover ...... 0.90 12/31/17 Soybean, seed ...... 0 .05 Vegetable, foliage of legume, except soybean, subgroup 7A ...... 40 (c) Tolerances with regional registra- Wheat, bran ...... 0.06 tions. [Reserved] Wheat, germ ...... 0 .09 (d) Indirect or inadvertent residues. [Reserved] (b) Section 18 emergency exemptions. [Reserved] [77 FR 59565, Sept. 28, 2012, as amended at 78 FR 38227, June 26, 2013; 80 FR 4515, Jan. 28, (c) Tolerances with regional registra- 2015] tions. [Reserved] (d) Indirect or inadvertent residues. § 180.669 Picoxystrobin; tolerances for [Reserved] residues. [77 FR 72231, Dec. 5, 2012] (a) General. Tolerances are estab- lished for residues of the fungicide § 180.671 Fenpyrazamine; tolerances picoxystrobin, including its metabo- for residues. lites and degradates, in or on the com- (a) General. Tolerances are estab- modities listed below. Compliance with lished for residues of the fungicide the tolerance levels specified below is fenpyrazamine, in or on the following to be determined by measuring only commodities. Compliance with the tol- picoxystrobin, methyl (aE)-a- erance levels specified in the following (methoxymethylene)-2-[[[6- table is to be determined by measuring (trifluoromethyl)-2- only fenpyrazamine S-allyl 5-amino-2- pyridinyl]oxy]methyl]benzeneacetate. isopropyl-4-(2-methylphenyl)-3-oxo-2,3- Parts per dihydropyrazole-1-carbothioate, in or Commodity million on the following commodities:

Barley, bran ...... 0 .5 Parts per Barley, grain ...... 0 .3 Commodity million Cattle, fat ...... 0.01 Cattle, meat ...... 0 .01 Almond ...... 0.02 Cattle, meat byproducts ...... 0.01 Almond, hulls ...... 1 .5 Corn, field, refined oil ...... 0 .07 Berry, low growing, subgroup 13–07G ...... 3 Eggs ...... 0 .01 Bushberry subgroup 13–07B ...... 5 Goat, fat ...... 0 .01 Caneberry subgroup 13–07A ...... 5

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Parts per Parts per Commodity million Commodity million

Fruit, small vine climbing, except fuzzy kiwifruit, Vegetable, leafy (except Brassica) (group 4) ...... 20 subgroup 13–07F ...... 3 Vegetable, tuberous and corm (subgroup 1C) .... 0 .15 Ginseng ...... 0 .7 Grape, juice ...... 4 Lettuce, head ...... 1.5 (b) Section 18 emergency exemptions. Lettuce, leaf ...... 2 [Reserved] Pistachio ...... 0.02 (c) Tolerances with regional registra- tions. [Reserved] (b) Section 18 emergency exemptions. [Reserved] (d) Indirect or inadvertent residues. (c) Tolerances with regional registra- Tolerances are established for indirect tions. [Reserved] or inadvertent tolerances for residues (d) Indirect or inadvertent residues. of cyantraniliprole, 3-bromo-1-(3- [Reserved] chloro-2-pyridinyl)-N-[4-cyano-2-meth- yl-6-[(methylamino)carbonyl]phenyl]- [78 FR 14465, Mar. 6, 2013] 1H-pyrazole-5-carboxamide, including its metabolites and degradates, in or § 180.672 Cyantraniliprole; tolerances on commodities in the following table. for residues. Compliance with the tolerance levels (a) General. Tolerances are estab- specified in the following table is to be lished for the combined residues of the determined by measuring only insecticide cyantraniliprole, 3-bromo-1- cyantraniliprole in or on the com- (3-chloro-2-pyridinyl)-N-[4-cyano-2- modity. methyl-6- [(methylamino)carbonyl]phenyl]-1H- Commodity Parts per pyrazole-5-carboxamide, including its million metabolites and degradates, in or on Animal feed, nongrass (group 18) ...... 0.20 commodities in the following table. Grain, cereal, forage, fodder and straw (group Compliance with the tolerance levels 16) ...... 0 .50 specified in the following table is to be Grass forage, fodder and hay (group 17) ...... 0 .50 Peanut, hay ...... 0.01 determined by measuring only Vegetable, foliage of legume (group 7) ...... 0 .70 cyantraniliprole in or on the com- Vegetable, leaves of root and tuber vegetables modity. (group 2) ...... 0 .04 Vegetable, root (subgroup 1A) ...... 0 .02 Parts per Commodity million [79 FR 6833, Feb. 5, 2014] Almond, hulls ...... 8 .0 Brassica head and stem (subgroup 5A) ...... 3 .0 Brassica leafy vegetables (subgroup 5B) ...... 30 § 180.673 Triforine; tolerances for resi- Bushberry (subgroup 13–07B) ...... 4 .0 dues. Cattle, fat ...... 0.01 Cattle, meat ...... 0 .01 (a) General. Tolerances are estab- Cattle, meat byproducts ...... 0.01 lished for residues of triforine, includ- Cherry (subgroup 12–12A) ...... 6 .0 ing its metabolites and degradates. Citrus, oil ...... 2.4 Compliance with the tolerance levels Cotton, gin byproducts ...... 10 Fruit, citrus (group 10–10) ...... 0 .70 specified in the following table is to be Fruit, pome (group 11–10) ...... 1 .5 determined by measuring only triforine Goat, fat ...... 0 .01 (N,N′-[1,2-piperazinediylbis(2,2,2- Goat, meat ...... 0.01 Goat, meat byproducts ...... 0 .01 trichloroehylidene)]bis[formamide]), in Horse, fat ...... 0 .01 or on the following commodities. Horse, meat ...... 0 .01 Horse, meat byproducts ...... 0 .01 Parts per Milk ...... 0.01 Commodity million Nut, tree (group 14–12) ...... 0 .04 Oilseed (group 20) ...... 1 .5 Blueberry 1 ...... 1 .0 Onion, bulb (subgroup 3–07A) ...... 0 .04 Tomato 1 ...... 0.5 Onion, green (subgroup 3–07B) ...... 8 .0 Peach (subgroup 12–12B) ...... 1 .5 1 There are no U.S. registrations for blueberry and tomato. Plum (subgroup 12–12C) ...... 0 .50 Sheep, fat ...... 0 .01 (b) Section 18 emergency exemptions. Sheep, meat ...... 0.01 [Reserved] Sheep, meat byproducts ...... 0 .01 Vegetable, cucurbit (group 9) ...... 0 .40 (c) Tolerances with regional registra- Vegetable, fruiting (group 8–10) ...... 2 .0 tions. [Reserved]

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(d) Indirect or inadvertent residues. Commodity Parts per [Reserved] million [78 FR 32151, May 29, 2013. Redesignated at 78 Potato ...... 0 .01 FR 36677, June 19, 2013] Tea ...... 30 .0 Vegetable, leafy, except Brassica, group 4 ...... 30 .0 § 180.674 Proquinazid; tolerances for residues. (2) Tolerances are established for res- idues of the insecticide tolfenpyrad, in- (a) General. Tolerances are estab- cluding its metabolites and degradates, lished for residues of the fungicide, in or on the commodities in the fol- proquinazid, including its metabolites lowing table. Compliance with the tol- and degradates, in or on the commod- erance levels specified below is to be ities listed in the following table. Com- determined by measuring only the sum pliance with the tolerance levels speci- of tolfenpyrad, 4-chloro-3-ethyl-1-meth- fied in the following table is to be de- yl-N-[4-(p-tolyloxy)benzyl]pyrazole-5- termined by measuring only carboxamide, and its metabolite 4-[4- proquinazid, [6-Iodo-2-propoxy-3- [(4-chloro-3-ethyl-1-methylpyrazol-5- propyl-3H-quinazolin-4-one), in or on yl)carbonylamino-methyl]phenoxy]- the following commodities: benzoic acid, calculated as the stoi- Parts per chiometric equivalent of tolfenpyrad. Commodity million Commodity Parts per Grape 1 ...... 0 .50 million Grape, raisin 1 ...... 1 .0 Cattle, fat ...... 0.01 1 No U.S. registrations for Proquinazid. Cattle, meat ...... 0 .01 Cattle, meat byproducts ...... 0.35 (b) Section 18 emergency exemptions. Goat, fat ...... 0 .01 [Reserved] Goat, meat ...... 0.01 (c) Tolerances with regional registra- Goat, meat byproducts ...... 0 .35 Horse, fat ...... 0 .01 tions. [Reserved] Horse, meat ...... 0 .01 (d) Indirect or inadvertent residues. Horse, meat byproducts ...... 0 .35 [Reserved] Milk ...... 0.03 Sheep, fat ...... 0 .01 [79 FR 18815, Apr. 4, 2014] Sheep, meat ...... 0.01 Sheep, meat byproducts ...... 0 .35 § 180.675 Tolfenpyrad; tolerances for residues. (b) Section 18 emergency exemptions. (a) General. (1) Tolerances are estab- [Reserved] lished for residues of the insecticide (c) Tolerances with regional registra- tolfenpyrad, including its metabolites tion. [Reserved] and degradates, in or on the commod- (d) Indirect or inadvertent residues. ities in the table below. Compliance [Reserved] with the tolerance levels specified [79 FR 1605, Jan. 9, 2014] below is to be determined by measuring only tolfenpyrad, 4-chloro-3-ethyl-1- § 180.676 Fenpropidin; tolerances for methyl-N-[4-(p- residues. tolyloxy)benzyl]pyrazole-5- (a) General. Tolerances are estab- carboxamide. lished for the residues of fenpropidin, including its metabolites and Parts per Commodity million degradates, in or on the commodities in the table below. Compliance with Almond hulls ...... 6 .0 the tolerance levels specified below is Citrus, dried pulp ...... 8 .0 Citrus, oil ...... 70.0 to be determined by measuring only Cotton, gin byproducts ...... 15 .0 fenpropidin (1-[3-[4-(1,1- Cotton, undelinted seed ...... 0 .70 dimethylethyl)phenyl]-2- Fruit, stone, group 12–12 ...... 2 .0 Fruits, citrus, group 10–10 ...... 1 .5 methylpropyl]piperidine). Grape ...... 2 .0 Grape, raisin ...... 6 .0 Parts per Commodity million Nuts, tree, group 14–12 ...... 0 .05 Persimmon ...... 2 .0 Banana 1 ...... 10 Plum, prune ...... 3 .0 Pomegranate ...... 2 .0 1 There are no U.S. registrations as of December 13, 2013.

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(b) Section 18 tolerance. [Reserved] (c) Tolerances with regional registra- (c) Tolerances with regional registra- tions. [Reserved] tions. [Reserved] (d) Indirect or inadvertent residues. (d) Indirect or inadvertent residues. [Reserved] [Reserved] [79 FR 33468, June 11, 2014] [79 FR 8096, Feb. 11, 2014] § 180.679 Flupyradifurone; tolerances § 180.677 Cyflumetofen; tolerances for for residues. residues. (a) General. Tolerances are estab- (a) General. Tolerances are estab- lished for residues of the insecticide lished for residues of the insecticide flupyradifurone, including its metabo- cyflumetofen, including its metabolites lites and degradates, in or on the com- and degradates, in or on the commod- modities in the following table. Com- ities in the table below. Compliance pliance with the tolerance levels speci- with the tolerance levels for fied in the following table is to be de- cyflumetofen is to be determined by termined by measuring only measuring only cyflumetofen, 2- flupyradifurone, 4-[[(6-chloro-3- methoxyethyl a-cyano-a-[4-(1,1- pyridinyl)methyl](2,2- dimethylethyl)phenyl]-b-oxo-2- difluoroethyl)amino]- 2(5H)-furanone. (trifluoromethyl)benzenepropanoate, in Parts per or on the commodity. Commodity million

Commodity Parts per Alfalfa, forage ...... 9.0 million Alfalfa, hay ...... 20 Almond, hulls ...... 15 Almond, hulls ...... 4 .0 Bean, succulent ...... 0 .20 Citrus, oil ...... 16 Berry, low growing, except cranberry subgroup Fruit, citrus, group 10–10 ...... 0 .30 13–07G ...... 1 .5 Fruit, pome, group 11–10 ...... 0 .30 Brassica, head and stem subgroup 5A ...... 6 .0 Grape ...... 0 .60 Brassica, leafy greens subgroup 5B ...... 40 Nut, tree, group 14–12 ...... 0 .01 Bushberry, except cranberry subgroup 13–07B 4 .0 Strawberry ...... 0 .60 Cactus, fruit ...... 0 .30 Tomato ...... 0.40 Cactus, pads ...... 0 .70 Cattle, fat ...... 0.20 (b) Section 18 emergency exemptions. Cattle, meat ...... 0 .30 Cattle, meat byproducts ...... 1.0 [Reserved] Coffee, green bean 1 ...... 1 .5 (c) Tolerances with regional registra- Corn, field, grain ...... 0 .05 tions. [Reserved] Corn, pop, grain ...... 0.05 Corn, sweet, kernels plus cobs with husks re- (d) Indirect or inadvertent residues. moved ...... 0 .05 [Reserved] Cotton, gin byproducts ...... 40 Cottonseed, subgroup 20C ...... 0 .80 [79 FR 29108, May 21, 2014] Egg ...... 0 .01 Fruit, citrus, dried pulp ...... 10 § 180.678 Tricyclazole; tolerances for Fruit, citrus, group 10–10 ...... 3 .0 residues. Fruit, pome, group 11–10 ...... 0 .70 Fruit, small vine climbing, except fuzzy (a) General. (1) Tolerances are estab- kiwifruit, subgroup 13–07F ...... 3.0 lished for residues of the fungicide Goat, fat ...... 0 .20 Goat, meat ...... 0.30 tricyclazole, including its metabolites Goat, meat byproducts ...... 1 .0 and degradates, in or on the commod- Grain, aspirated grain fractions ...... 40 ities in the table below. Compliance Grain, cereal, forage, fodder and straw, group with the tolerance levels specified 16 ...... 30 Grain, cereal, group 15, except rice and corn .. 3.0 below is to be determined by measuring Grape, raisin ...... 5 .0 only tricyclazole (5-methyl-1,2,4- Hog, fat ...... 0 .01 triazolo[3,4-b ]benzothiazole). Hog, meat ...... 0 .01 Hog, meat byproducts ...... 0 .04 Hops, dried cones ...... 10 Parts Commodity per million Horse, fat ...... 0 .20 Horse, meat ...... 0 .30 Rice, grain 1 ...... 3 .0 Horse, meat byproducts ...... 1 .0 Leaf petioles, subgroup 4B ...... 9 .0 1 There are no U.S. Registrations on Rice as of June 11, Leafy greens, subgroup 4A ...... 30 2014. Milk ...... 0.15 Nut, tree, group 14–12 ...... 0 .02 (b) Section 18 emergency exemptions. Onion, bulb, subgroup 3–07A ...... 0 .09 [Reserved] Onion, green, subgroup 3–07B ...... 3 .0

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Parts per Parts per Commodity million Commodity million

Pea and bean, dried, shelled except soybean, Vegetables, fruiting, group 8–10 ...... 0 .50 subgroup 6C ...... 3 .0 Pea, succulent ...... 2 .0 Peanut ...... 0 .04 (b) Section 18 emergency exemptions. Peanut, hay ...... 20 [Reserved] Pitaya ...... 0 .30 (c) Tolerances with regional registra- Sheep, fat ...... 0 .20 Sheep, meat ...... 0.30 tions. [Reserved] Sheep, meat byproducts ...... 1 .0 (d) Indirect or inadvertant residues. Soybean, seed ...... 1 .5 [Reserved] Taro leaves ...... 30 Turnip greens ...... 40 [79 FR 56968, Sept. 24, 2014] Vegetable, cucurbit, group 9 ...... 0.40 Vegetable, foliage of legume, group 7 ...... 30 Vegetable, fruiting, group 8–10 ...... 1 .5 § 180.682 Bicyclopyrone; tolerances for Vegetable, legume, edible podded, subgroup residues. 6A ...... 3 .0 Vegetable, root, except sugar beet, subgroup (a) General. (1) Tolerances are estab- 1B ...... 0 .90 lished for residues of the herbicide Vegetable, tuberous and corm, subgroup 1C ... 0.05 bicyclopyrone (4-hydroxy-3-[[2-[(2- 1 No U.S. registration. methoxyethoxy)methyl]-6- (b) Section 18 emergency exemptions. (trifluoromethyl)-3- [Reserved] pyridinyl]carbonyl]bicyclo[3.2.1]oct-3- (c) Tolerances with regional restric- en-2-one), including its metabolites and tions. Tolerances are established for degradates, in or on the commodities residues of the insecticide in the table below. Compliance with flupyradifurone, including its metabo- the tolerance levels specified below is lites and degradates, in or on the com- to be determined by measuring only modities in the following table. Com- the sum of the common moieties pliance with the tolerance levels speci- SYN503780 (2-[(2- fied in the following table is to be de- methoxyethoxy)methyl]-6- termined by measuring only (trifluoromethyl)-3-pyridinecarboxylic flupyradifurone, 4-[[(6-chloro-3- acid) and CSCD686480 (2-[(2- pyridinyl)methyl](2,2- hydroxyethoxy)methyl]-6- difluoroethyl)amino]- 2(5H)-furanone. (trifluoromethyl)-3-pyridinecarboxylic Parts per acid), calculated as the stoichiometric Commodity million equivalent of bicyclopyrone, in or on Clover, forage ...... 20 the commodities. Clover, hay ...... 30 Parts per Commodity million (d) Indirect or inadvertent residues. [Reserved] Corn, field, forage ...... 0 .30 Corn, field, grain ...... 0 .02 [80 FR 3487, Jan. 23, 2015] Corn, field, stover ...... 0 .40 Corn, pop, grain ...... 0.02 § 180.680 Fluensulfone; tolerances for Corn, pop, stover ...... 0.40 residues. Corn, sweet, forage ...... 0 .40 (a) General. Tolerances are estab- Corn, sweet, kernel plus cob with husks re- lished for residues of the nematicide moved ...... 0 .03 Corn, sweet, stover ...... 0 .70 fluensulfone, including its metabolites Sugarcane, cane 1 ...... 0.02 and degradates, in or on the commod- Cattle, meat byproducts ...... 1.5 ities in the table below. Compliance Goat, meat byproducts ...... 1 .5 with the tolerance levels specified Sheep, meat byproducts ...... 1 .5 below is to be determined by measuring Horse, meat byproducts ...... 1 .5 only 3,4,4-trifluoro-but-3-ene-1-sulfonic Hog, meat byproducts ...... 0 .15 acid, calculated as the stoichiometric 1 There are no U.S. Registrations on Sugarcane as of equivalent of fluensulfone. March 13, 2015. (2) [Reserved] Parts per Commodity million (b) [Reserved]

Vegetables, cucurbits, group 9 ...... 0.50 [80 FR 22654, Apr. 23, 2015]

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Subpart D—Exemptions From (4) Sabadilla. Tolerances (b) When applied to growing crops, in accordance with good agricultural § 180.900 Exemptions from the require- practice, the pesticides rotenone or ment of a tolerance. derris or cube roots are exempt from An exemption from a tolerance shall the requirement of a tolerance. There be granted when it appears that the are no U.S. registrations for use of ro- total quantity of the pesticide chem- tenone, derris, or cube roots on food ical in or on all raw agricultural com- commodities as of March 23, 2011. modities for which it is useful under (c) These pesticides are not exempted conditions of use currently prevailing from the requirement of a tolerance or proposed will involve no to when applied to a crop at the time of or the public health. after harvest. [69 FR 23117, Apr. 28, 2004] [77 FR 59128, Sept. 26, 2012]

§ 180.905 Pesticide chemicals; exemp- § 180.910 Inert ingredients used pre- tions from the requirement of a tol- and post-harvest; exemptions from erance. the requirement of a tolerance. (a) When applied to growing crops, in Residues of the following materials accordance with good agricultural are exempted from the requirement of practice, the following pesticide chemi- a tolerance when used in accordance cals are exempt from the requirement with good agricultural practice as inert of a tolerance: (or occasionally active) ingredients in (1) Petroleum oils. pesticide formulations applied to grow- (2) Piperonyl butoxide. ing crops or to raw agricultural com- (3) Pyrethrins. modities after harvest:

Inert ingredients Limits Uses

Acetic acid ...... Catalyst Acetic anhydride ...... Solvent, cosolvent Acetone ...... Do. Alkanoic and alkenoic acids, mono- and diesters of a- ...... Emulsifiers hydro-w-hydroxypoly (oxyethylene) with molecular weight (in amu) range of 200 to 6,000.

Alkyl (C8-C24) benzenesulfonic acid and its ammonium, ...... Surfactants, related adjuvants of calcium, magnesium, potassium, sodium, and zinc surfactants salts.

C10-C18-Alkyl dimethyl amine oxides (CAS Reg. Nos. 15% by weight in pesticide for- Surfactant 1643–20–5, 2571–88–2, 2605–79–0, 3332–27–2, mulation. 61788–90–7, 68955–55–5, 70592–80–2, 7128–91–8, 85408–48–6, and 85408–49–7).

a-alkyl(C6- C15)-w-hydroxypoly(oxyethylene)sulfate, and Not to exceed 30% of formula- Surfactants, related adjuvants of its ammonium, calcium, magnesium, potassium, so- tion. surfactants. dium, and zinc salts, poly(oxyethylene) content aver- ages 2–4 moles (CAS Reg. Nos.: 3088–31–1, 3694– 74–4, 9004–82–4, 9004–84–6, 9021–91–4, 9086–52– 6, 13150–00–0, 15826–16–1, 25446–78–0, 26183–44– 8, 27140–00–7, 27731–62–0, 32612–48–9, 34431–25– 9, 35015–74–8, 50602–06–7, 52286–18–7, 52286–19– 8, 54116–08–4, 55901–67–2, 61702–79–2, 61894–66– 4, 62755–21–9, 63428–85–3, 63428–86–4, 63428–87– 5, 65086–57–9, 65086–79–5, 65104–74–7, 65122–38– 5, 67674–66–2, 67762–19–0, 67762–21–4, 67845–82– 3, 67845–83–4, 67923–90–4, 68037–05–8, 68037–06– 9, 68171–41–5, 68424–50–0, 68511–39–7, 68585–34– 2, 68610–66–2, 68611–29–0, 68611–55–2, 68649–53– 6, 68890–88–0, 68891–29–2, 68891–30–5, 68891–38– 3, 69011–37–6, 73665–22–2, 75422–21–8, 78330–16– 2, 78330–17–3, 78330–25–3, 78330–26–4, 78330–27– 5, 78330–28–6, 78330–29–7, 78330–30–0, 96130–61– 9, 106597–03–9, 110392–50–2, 119432–41–6, 125301–88–4, 125301–89–5, 125301–92–0, 125736– 54–1, 157707–85–2, 160104–51–8, 160901–27–9, 160901–28–0, 160901–29–1, 160901–30–4, 161025– 28–1, 161074–79–9, 162063–19–6, 219756–63–5).

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Inert ingredients Limits Uses

a-alkyl (C12-C15)-w-hydroxypoly (oxypropylene) poly (oxy- Not more than 20% of pesticide Surfactant ethylene) copolymers (where the poly (oxypropylene) formulations. content is 3–60 moles and the poly (oxyethylene) con- tent is 5–80 moles). a-alkyl-w-hydroxypoly (oxypropylene) and/or poly (oxy- ...... Surfactants, related adjuvants of ethylene) polymers where the alkyl chain contains a surfactants. minimum of six carbons (CAS Reg. No.: 9002–92–0; 9004–95–9; 9004–98–2; 9005–00–9; 9035–85–2; 9038–29–3; 9038–43–1; 9040–05–5; 9043–30–5; 9087–53–0; 25190–05–0; 24938–91–8; 25231–21–4; 26183–52–8; 26468–86–0; 26636–39–5; 27252–75–1; 27306–79–2; 31726–34–8; 34398–01–1; 34398–05–5; 37251–67–5; 37311–00–5; 37311–01–6; 37311–02–7; 37311–04–9; 39587–22–9; 50861–66–0; 52232–09–4; 52292–17–8; 52609–19–5; 57679–21–7; 59112–62–8; 60828–78–6; 61702–78–1; 61725–89–1; 61791–13–7; 61791–20–6; 61791–28–4; 61804–34–0; 61827–42–7; 61827–84–7; 62648–50–4; 63303–01–5; 63658–45–7; 63793–60–2; 64366–70–7; 64415–24–3; 64415–25–4; 64425–86–1; 65104–72–5; 65150–81–4; 66455–14–9: 66455–15–0; 67254–71–1; 67763–08–0; 68002–96–0; 68002–97–1; 68131–39–5; 68131–40–8; 68154–96–1; 68154–97–2; 68154–98–3; 68155–01–1; 68213–23–0; 68213–24–1; 68238–81–3; 68238–82–4; 68409–58–5; 68409–59–6; 68439–30–5; 68439–45–2; 68439–46–3; 68439–48–5; 68439–49–6; 68439–50–9; 68439–51–0; 68439–53–2; 68439–54–3; 68458–88–8; 68526–94–3; 68526–95–4; 68551–12–2; 68551–13–3; 68551–14–4; 68603–20–3; 68603–25–8; 68920–66–1; 68920–69–4; 68937–66–6; 68951–67–7; 68954–94–9; 68987–81–5; 68991–48–0; 69011–36–5; 69013–18–9; 69013–19–0; 69227–20–9; 69227–21–0; 69227–22–1; 69364–63–2; 70750–27–5; 70879–83–3; 70955–07–6; 71011–10–4; 71060–57–6; 71243–46–4; 72066–65–0; 72108–90–8; 72484–69–6; 72854–13–8; 72905–87–4; 73018–31–2; 73049–34–0; 74432–13–6; 74499–34–6; 78330–19–5; 78330–20–8; 78330–21–9; 78330–23–1; 79771–03–2; 84133–50–6; 85422–93–1; 97043–91–9; 97953–22–5; 102782–43–4; 103331–86–8; 103657–84–7; 103657– 85–8; 103818–93–5; 103819–03–0; 106232–83–1; 111905–54–5; 116810–31–2; 116810–32–3; 116810– 33–4; 120313–48–6; 120944–68–5; 121617–09–2; 126646–02–4; 126950–62–7; 127036–24–2; 139626– 71–4; 152231–44–2; 154518–36–2; 157627–86–6; 157627–88–8; 157707–41–0; 157707–43–2; 159653– 49–3; 160875–66–1; 160901–20–2; 160901–09–7; 160901–19–9; 161025–21–4; 161025–22–5; 166736– 08–9; 169107–21–5; 172588–43–1; 176022–76–7; 196823–11–7; 287935–46–0; 288260–45–7; 303176– 75–2; 954108–36–2).

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Inert ingredients Limits Uses

a-alkyl (minimum C6 linear, branched, saturated and/or Not to exceed 30% of formula- Surfactants, related adjuvants of unsaturated)-w-hydroxypolyoxyethylene polymer with tion. surfactants. or without polyoxypropylene, mixture of di- and monohydrogen phosphate esters and the cor- responding ammonium, calcium, magnesium, monoethanolamine, potassium, sodium, and zinc salts of the phosphate esters; minimum oxyethylene content is 2 moles; minimum oxypropylene content is 0 moles (CAS Reg. Nos.: 9004–80–2, 9046–01–9, 26982–05– 8, 31800–89–2, 37280–82–3, 37281–86–0, 39341–09– 8, 39341–65–6, 39464–66–9, 39464–69–2, 42612–52– 2, 50643–20–4, 50668–50–3, 51325–10–1, 51884–64– 1, 52019–36–0, 57486–09–6, 58206–38–5, 58318–92– 6, 58857–49–1, 59112–71–9, 60267–55–2, 61837–79– 4, 62362–49–6, 62482–61–5, 63747–86–4, 63887–54– 7, 63887–55–8, 66020–37–9, 66272–25–1, 66281–20– 7, 67711–84–6, 67786–06–5, 67989–06–4, 68070–99– 5, 68071–17–0, 68071–35–2, 68071–37–4, 68130–44– 9, 68130–45–0, 68130–46–1, 68130–47–2, 68186–29– 8, 68186–34–5, 68186–36–7, 68186–37–8, 68238–84– 6, 68311–02–4, 68311–04–6, 68332–75–2, 68389–72– 0, 68400–75–9, 68413–78–5, 68425–73–0, 68425–75– 2, 68439–39–4, 68458–48–0, 68511–15–9, 68511–36– 4, 68511–37–5, 68551–05–3, 68585–15–9, 68585–16– 0, 68585–17–1, 68585–36–4, 68585–39–7, 68603–24– 7, 68607–14–7, 68610–64–0, 68610–65–1, 68649–29– 6, 68649–30–9, 68650–84–0, 68815–11–2, 68855–46– 9, 68856–03–1, 68890–90–4, 68890–91–5, 68891–12– 3, 68891–13–4, 68891–26–9, 68908–64–5, 68909–65– 9, 68909–67–1, 68909–69–3, 68921–24–4, 68921–60– 8, 68954–87–0, 68954–88–1, 68954–92–7, 68987–35– 9, 69029–43–2, 69980–69–4, 70247–99–3, 70248–14– 5, 70844–96–1, 70903–63–8, 71965–23–6, 71965–24– 7, 72480–27–4, 72623–67–7, 72623–68–8, 72828–56– 9, 72828–57–0, 73018–34–5, 73038–25–2, 73050–08– 5, 73050–09–6, 73361–29–2, 73378–71–9, 73378–72– 0, 73559–42–9, 73559–43–0, 73559–44–1, 73559–45– 2, 74499–76–6, 76930–25–1, 78041–18–6, 78330–22– 0, 78330–24–2, 82465–25–6, 84843–37–8, 91254–26– 1, 93925–54–3, 95014–34–9, 96416–89–6, 99924–51– 3, 103170–31–6, 103170–32–7, 106233–09–4, 106233–10–7, 108818–88–8, 110392–49–9, 111798– 26–6, 111905–50–1, 116671–23–9, 117584–36–8, 119415–05–3, 120913–45–3, 121158–61–0, 121158– 63–2, 123339–53–7, 125139–13–1, 125301–86–2, 125301–87–3, 126646–03–5, 129208–04–4, 129870– 77–5, 129870–80–0, 130354–37–9, 136504–88–6, 143372–50–3, 143372–51–4, 144336–75–4, 146815– 57–8, 151688–56–1, 154518–39–5, 154518–40–8, 155240–11–2, 159704–69–5, 160498–49–7, 160611– 24–5, 171543–66–1, 172027–16–6, 172274–69–0, 176707–42–9, 181963–82–6, 188741–55–1, 191940– 53–1, 210493–60–0, 210993–53–6, 246159–55–7, 251298–11–0, 261627–68–3, 290348–69–5, 290348– 70–8, 317833–96–8, 340681–28–9 , 422563–19–7, 422563–26–6, 522613–09–8, 717140–06–2, 717140– 09–5, 717827–29–7, 762245–80–7, 762245–81–8, 866538–89–8, 866538–90–1, 873662–29–4, 913068– 96–9, 936100–29–7, 936100–30–0, 1072943–56–6, 1087209–87–7, 1174313–54–2, 1187742–89–7, 1187743–35–6, 1205632–03–6, 1233235–49–8, 1451002–50–8, 1456802–88–2, 1456802–89–3, 1456803–12–5). N-alkyl (C8-C18) primary amines and their acetate salts Concentration in formulated end- Surfactants, related adjuvants of where the alkyl group is linear and may be saturated use products not to exceed surfactants and/or unsaturated (CAS Reg. Nos. 61790–57–6, 10% by weight in herbicide 61790–58–7, 61790–59–8, 61790–60–1, 61788–46–3, products, 4% by weight in in- 61790–33–8, 68155–38–4). secticide products, and 4% by weight in fungicide products.

Alkyl (C8-C18) sulfate and its ammonium, calcium, ...... Surfactants. isopropylamine, magnesium, potassium, sodium, and zinc salts. Aluminum hydroxide ...... Diluent, carrier

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Inert ingredients Limits Uses

Aluminum oxide ...... Diluent Aluminum stearate ...... Surfactant , C5-C9, N-[3-(dimethylamino) propyl] (CAS Reg...... Surfactant No. 1044764–00–2). Amides, C6-C12, N-[3-(dimethylamino) propyl] (CAS Reg...... Surfactant No. 1044764–06–8). Ammonium bicarbonate ...... Surfactant, suspending agent, dispersing agent Ammonium carbamate ...... Synergist in aluminum phosphide formulations Ammonium chloride ...... Intensifier when used with am- monium nitrate as a dessicant or defoliant. Fire suppressant in aluminum phosphide and magnesium phosphide formu- lations Ammonium hydroxide ...... Solvent, cosolvent, neutralizer, solubilizing agent Ammonium salts of fatty acids (C8-C18 saturated) (CAS ...... Surfactant Reg. No. 5972–76–9, 63718–65–0, 16530–70–4, 32582–95–9, 2437–23–2, 191799–95–8, 16530–71–5, 93917–76–1, 5297–93–8, 94266–36–1, 1002–89–7). Ammonium stearate ...... Surfactant ...... Solid diluent, carrier Ammonium thiosulfate ...... Intensifier when used with am- monium nitrate as desiccant or defoliant Amyl acetate ...... Solvent, cosolvent, attractant Ascorbyl palmitate ...... Preservative Attapulgite-type clay ...... Solid diluent, carrier, thickener Bacillus thuringiensis fermentation solids and/or solubles ...... Diluent, carrier Bentonite ...... Solid diluent, carrier Benzoic acid ...... Preservative for formulation Bicyclo[3.1.1]hept–2–ene, 2,6,6–trimethyl–, homopolymer ...... Surfactants, related adjuvants of (Alpha-pinene, homopolymer)(CAS Reg. No. 25766– surfactants 18–1). Bicyclo[3.1.1]heptane, 6,6–dimethyl–2–methylene–, ...... Surfactants, related adjuvants of homopolymer (Beta-pinene, homopolymer) (CAS Reg. surfactants No. 25719–60–2). Bicyclo[3.1.1]hept–2–ene, 2,6,6–trimethyl–, polymer with ...... Surfactants, related adjuvants of 6,6–dimethyl–2–methylenebicyclo [3.1.1] heptane (Co- surfactants polymer of alpha- and beta-pinene) (CAS Reg. No. 31393–98–3). 2-Bromo-2-nitro-1,3-propanediol (CAS Reg. No. 52–51– 0.04% or less by weight of the In-can preservative 7). total pesticide formulation. Butane ...... Propellant n-Butanol (CAS Reg. No. 71–36–3) ...... Solvent, cosolvent n-Butyl benzoate (CAS Reg. No.136–60–7) ...... Solvent Butylated hydroxyanisole ...... Antioxidant Butylated hydroxytoluene ...... Do. Calcareous shale ...... Solid diluent carrier Calcite ...... Do. Calcium carbonate ...... Do. Calcium chloride ...... Stabilizer Calcium phosphate ...... Solid diluent, carrier Calcium hydroxide ...... Do. Calcium hypochlorite ...... Sanitizing and bleaching agent Calcium lactate pentahydrate (CAS Reg. No. 5743–47–5) ...... Nutrient, stabilizer Calcium oxide ...... Solid diluent, carrier Calcium salt of partially dimerized rosin, conforming to 21 ...... Coating agent CFR 172.210. Calcium silicate ...... Solid diluent, carrier Calcium stearate ...... Do. Carbon Dioxide (CAS Reg. No. 124–38–9) ...... None ...... Propellant Carrageenan, conforming to 21 CFR 172.620 ...... Minimum molecular weight (in Thickener amu): 100,000. Cetyl alcohol (CAS Reg. No. 36653–82–4) ...... Not more than 5.0% of pesticide Evaporation retardant formulation. Charcoal, activated ...... Meets specifications in the Food Carrier Chemical Codex. Coconut shells ...... Solid diluent and carrier Cod liver oil ...... Solvent, cosolvent Croscarmellose sodium (CAS Reg. No. 74811–65–7) ...... Disintegrant, solid diluent, carrier, and thickener

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Inert ingredients Limits Uses

n-Decyl alcohol (CAS Reg. No. 112–30–1) ...... Solvent or co-solvent

Dialkyl (C8-C18) dimethyl ammonium chloride ...... Not more than 0.2% in silica, hy- Flocculating agent in the manu- drated silica. facture of silica, hydrated silica for use as a solid diluent, car- rier Diatomite (diatomaceous earth) ...... Solid diluent carrier Diethylaminoethanol, ethoxylated, propoxylated, reaction ...... Surfactant products with fatty acid dimers, minimum number aver- age molecular weight (in amu), 1,200 (CAS Reg. No. 1173188–75–4). Diethylaminoethanol, ethoxylated, propoxylated, reaction ...... Surfactant products with fatty acid trimers, minimum number aver- age molecular weight (in amu), 1,200 (CAS Reg. No. 1173188–83–4). Diethylaminoethanol, ethoxylated, reaction product with ...... Surfactant fatty acid dimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173188–72–1). Diethylaminoethanol, ethoxylated, reaction products with ...... Surfactant fatty acid trimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173188–81–2). Diethylene glycol abietate ...... Surfactants, related adjuvants of surfactants 1,1-Difluoroethane (CAS Reg. No. 75–37–6) ...... For aerosol pesticide formula- Aerosol propellant tions used for insect control in food- and feed-handling estab- lishments and animals. 1,2-Dihydro-6-ethoxy-2,2,4-trimethylquinolene ...... Not more than 0.02% of pes- Antioxidant ticide formulation. Diisopropanolamine (CAS Reg. No. 110–97–4) ...... Not to exceed 10% by weight of Neutralizer or stabilizer pesticide formulation. Diisopropyl adipate (CAS Reg. No. 6938–94–9) ...... 40% in mosquito control formula- Solvent, co-solvent. tions. Dimethyl adipate (CAS no. 627–93–0) ...... None ...... Solvent/co-solvent Dimethylaminoethanol, ethoxylated, propoxylated, reac- ...... Surfactant tion products with fatty acid dimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173188–42–5). Dimethylaminoethanol, ethoxylated, propoxylated, reac- ...... Surfactant tion products with fatty acid trimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173188–67–4). Dimethylaminoethanol, ethoxylated, reaction products ...... Surfactant with fatty acid dimers, minimum number average mo- lecular weight (in amu), 1,200 (CAS Reg. No. 1173188–38–9). Dimethylaminoethanol, ethoxylated, reaction products ...... Surfactant with fatty acid trimers, minimum number average mo- lecular weight (in amu), 1,200 (CAS Reg. No. 1173188–49–2). Dimethyl ether (methane, oxybis-) (CAS Reg. No. 115– ...... Propellant 10–6). Dimethyl glutarate (CAS no. 1119–40–0) ...... None ...... Solvent/co-solvent 3,6-Dimethyl-4-octyn-3,6-diol ...... Not more than 2.5% of pesticide Surfactants, related adjuvants of formulation. surfactants Dimethyl succinate (CAS no. 106–65–0) ...... None ...... Solvent/co-solvent Di-n-butyl carbonate (CAS Reg. No. 542–52–9) ...... Solvent Dipropylene glycol ...... Solvent, cosolvent Disodium phosphate ...... Anticaking agent, conditioning agent Disodium zinc ethylenediaminetetraacetate dihydride ...... Sequestrant Dolomite ...... Solid diluent, carrier Epoxidized linseed oil ...... Surfactants, related adjuvants of surfactants Epoxidized soybean oil ...... Do. Ethyl acetate ...... Solvent, cosolvent Ethyl alcohol ...... Do. Ethyl esters of fatty acids derived from edible fats and ...... Solvent, cosolvent oils. Ethyl maltol (CAS Reg. No.4940–11–8) ...... Not more than 0.2 % of the pes- Odor masking agent ticide formulation.

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Inert ingredients Limits Uses

Ethylene glycol (CAS Reg. No. 107–21–1) ...... Without limitation ...... Encapsulating agent for pes- ticides being applied post-har- vest as residual, and crack and crevice sprays in and around food and nonfood areas of residential and non- residential structures, including food handling establishments Ethylene oxide adducts of 2,4,7,9-tetramethyl-5- ...... Surfactants, related adjuvants of decynediol, the ethylene oxide content averages 3.5, surfactants 10 or 30 moles (CAS Reg. No. 9014–85–1). (S,S)-Ethylenediamine disuccinic acid trisodium salt ...... Sequestrant or chelating agent (CAS Reg. No. 178949–82–1). Ethylenediaminetetraacetic acid ...... 3% of pesticide formulation ...... Sequestrant Ethylenediaminetetraacetic acid, tetrasodium salt ...... 5% of pesticide formulation ...... Sequestrant 2–Ethyl-1-hexanol (CAS Reg. No. 104–76–7) ...... Not more than 10% of pesticide Solvent, adjuvant of surfactants Fatty acids, conforming to 21 CFR 172.860 ...... Binder, defoaming agent, lubri- cant FD&C Blue No. 1 ...... Not more than 0.2% of pesticide Dye formulation. FD&C Red No. 40 (CAS Reg. No. 25956–17–6) con- Not to exceed 0.002% by weight Dye, coloring agent forming to 21 CFR 74.340. of pesticide formulation. Ferric Citrate (CAS Reg. No. 2338–05–8) ...... Stabilizer Ferric sulfate ...... Solid diluent, carrier Furcelleran ...... Thickener D-glucopyranose, oligomeric, C10–16-alkyl glycosides ...... Surfactant (CAS Reg. No. 110615–47–9). D-glucopyranose, oligomeric, 6-(dihydrogen citrates), ...... Surfactant C8–20 branched and linear alkyl glycosides, sodium salts (CAS Reg. No. 1079993–97–7). D-glucopyranose, oligomeric, 6-(hydrogen ...... Surfactant sulfosuccinates), C8–20 branched and linear alkyl glycosides, sodium salts (CAS Reg. No. 1079993–92– 2). D-glucopyranose, oligomeric, lactates, C8–20 branched ...... Surfactant and linear alkyl glycosides (CAS Reg. No. 1079993– 94–4). Glycerides, edible fats and oils derived from plants and ...... Emulsifier, dispersing agent animals, reaction products with sucrose (CAS Reg. Nos. 100403–38–1, 100403–41–6, 100403–39–2, 100403–40–5). Glycerol mono-, di-, and triacetate ...... Solvent, cosolvent Glyceryl monostearate ...... Emulsifier Granite ...... Do. Graphite ...... Solid diluent, carrier Gum arabic (acacia) ...... Surfactant, suspending agent, dispersing agent Gypsum ...... Solid diluent, carrier Hexamethylenetetramine ...... For use in citrus washing solu- Preservative tions only at not more than 1%. 3-hexen-1-ol, (3Z)- (CAS Reg. No. 928-96-1) ...... Not more than 0.4% of the pes- Odorant, alerting agent ticide formulation. n-Hexyl alcohol (CAS Reg. No. 111–27–3) ...... Solvent, cosolvent C9 rich aromatic hydrocarbons (CAS Reg. No. 64742– ...... Solvent 95–6). C10–11 rich aromatic hydrocarbons (CAS Reg. No...... Solvent 64742–94–5). C11–12 rich aromatic hydrocarbons (CAS Reg. No...... Solvent 64742–94–5). Hydrochloric acid ...... Solvent, neutralizer Hydroxyethylmorpholine, ethoxylated, propoxylated, reac- ...... Surfactant tion products with fatty acid dimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173189–06–4). Hydroxyethylmorpholine, ethoxylated, propoxylated, reac- ...... Surfactant tion products with fatty acid trimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173189–17–7). Hydroxyethylmorpholine, ethoxylated, reaction products ...... Surfactant with fatty acid dimers, minimum number average mo- lecular weight (in amu), 1,200 (CAS Reg. No. 1173189–00–8).

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Inert ingredients Limits Uses

Hydroxyethylmorpholine, ethoxylated, reaction products ...... Surfactant with fatty acid trimers, minimum number average mo- lecular weight (in amu), 1,200 (CAS Reg. No. 1173189–09–7). Hydroxyethylpiperidine, ethoxylated, propoxylated, reac- ...... Surfactant tion products with fatty acid dimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173189–22–4. Hydroxyethylpiperidine, ethoxylated, propoxylated, reac- ...... Surfactant tion products with fatty acid trimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173189–28–0). Hydroxyethylpiperidine, ethoxylated, reaction products ...... Surfactant with fatty acid dimers, minimum number average mo- lecular weight (in amu), 1,200 (CAS Reg. No. 1173189–20–2). Hydroxyethylpiperidine, ethoxylated, reaction products ...... Surfactant with fatty acid trimers, minimum number average mo- lecular weight (in amu), 1,200 (CAS Reg. No. 1173189–25–7). Hydroxyethylidine diphosphonic acid (HEDP) (CAS Reg. For use in antimicrobial pesticide Stabilizer, chelator No. 2809–21–4). formulations at not more than 1 percent. Iron oxide ...... Solid diluent, carrier Isobutane (CAS Reg. No. 75–28–5) ...... None ...... Propellant Isopropyl myristate (CAS Reg. No. 110–27–0) ...... Solvent Kaolinite-type clay ...... Solid diluent, carrier Lactic acid ...... Solvent Lactic acid, 2-ethylhexyl ester (CAS Reg. No. 6283–86– ...... Solvent 9). Lactic acid, 2-ethylhexyl ester, (2S)- (CAS Reg. No...... Solvent 186817–80–1). Lactic acid, n-propyl ester, (S); (CAS Reg. No. 53651– ...... Solvent 69–7). Lauryl alcohol ...... Surfactant Lignin (CAS Reg. No. 9005–53–2) ...... Surfactant, related adjuvants of surfactants Lignin, alkali (CAS Reg. No. 8068–05–1) ...... Do. Lignin, alkali, oxidized, sodium salt (CAS Reg. No...... Do. 68201–23–0). Lignin alkali reaction products with disodium sulfite and ...... Do. formaldehyde (CAS Reg. No. 105859–97–0). Lignin alkali reaction products with formaldehyde and so- ...... Do. dium bisulfite (CAS Reg. No. 68512–35–6). Lignosulfonic acid (CAS Reg. No. 8062–15–5) ...... Do. Lignosulfonic acid, ammonium calcium salt (CAS Reg...... Do. No. 12710–04–2). Lignosulfonic acid, ammonium magnesium salt (CAS ...... Do. Reg. No. 123175–37–1). Lignosulfonic acid, ammonium salt (CAS Reg. No. 8061– ...... Do. 53–8). Lignosulfonic acid, ammonium sodium salt (CAS Reg...... Do. No. 166798–73–8). Lignosulfonic acid, calcium magnesium salt (CAS Reg...... Do. No. 55598–86–2). Lignosulfonic acid, calcium salt (CAS Reg. No. 8061–52– ...... Do. 7). Lignosulfonic acid, calcium sodium salt (CAS Reg. No...... Do. 37325–33–0). Lignosulfonic acid, ethoxylated, sodium salt (CAS Reg...... Do. No. 68611–14–3). Lignosulfonic acid, magnesium salt (CAS Reg. No...... Do. 8061–54–9). Lignosulfonic acid, potassium salt (CAS Reg. No. 37314– ...... Do. 65–1). Lignosulfonic acid, sodium salt (CAS Reg. No. 8061–51– ...... Do. 6). Lignosulfonic acid, sodium salt, oxidized (CAS Reg. No...... Do. 68855–41–4). Lignosulfonic acid, sodium salt, polymer with formalde- ...... Do. hyde and phenol (CAS Reg. No. 37207–89–9). Lignosulfonic acid, sodium salt, sulfomethylated (CAS ...... Do. Reg. No. 68512–34–5). Lignosulfonic acid, zinc salt (CAS Reg. No. 57866–49–6) ...... Do.

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Inert ingredients Limits Uses

d-Limonene (CAS Reg. No. 5989–27–5) ...... Solvent, fragrance Magnesium carbonate ...... Anticaking agent, conditioning agent Magnesium chloride ...... Safener Magnesium lime ...... Solid diluent, carrier Magnesium oxide ...... Do. Magnesium silicate ...... Do. Magnesium stearate ...... Surfactant Magnesium sulfate ...... Solid diluent, carrier, safener Methyl alcohol ...... Solvent Methyl n-amyl ketone (CAS Reg. No. 110–43–0) ...... Solvent, cosolvent Methyl 5-(dimethylamino)-2-methyl-5-oxopentanoate ...... Solvent (1174627–68–9). Methyl esters of fatty acids derived from edible fats and ...... Solvent, cosolvent oils. Methyl esters of higher fatty acids conforming to 21 CFR ...... Antidusting agent, surfactant 573.640. Methyl isobutyl ketone ...... Solvent 2-methyl-2,4-pentanediol (CAS Reg. No. 107–41–5) ...... Without limitation ...... Growing crops and food animals 2-methyl-1,3-propanediol (CAS Reg. No. 2163–42–0) ...... Solvent, surfactant Methylated silicones ...... Antifoaming agent Mono-, di-, and trimethylnapthalenesulfonic acids and ...... Surfactants, related adjuvants of napthalenesulfonic acids formaldehyde condensates, surfactants ammonium and sodium salts (CAS Reg. Nos 9008– 63–3, 9069–80–1, 9084–06–4, 36290–04–7, 91078– 68–1, 141959–43–5, 68425–94–5). Mica ...... Solid diluent, carrier Mineral oil, U.S.P., or conforming to 21 CFR 172.878 or ...... Diluent, carrier, and solvent 178.3620(a) (CAS Reg. No. 8012–95–1). Monoammonium phosphate ...... No more than 3.75% by weight Postharvest fumigation in formu- in formulation. lation with aluminum phosphide Mono- and diglycerides of C 8-C18 fatty acids ...... Surfactants, related adjuvants of surfactants Montmorillonite-type clay ...... Solid diluent, carrier Nonyl, decyl, and undecyl glycoside mixture with a mix- ...... Surfactant. ture of nonyl, decyl, and undecyl oligosaccharides and related reaction products (primarily decanol and undecanol) produced as an aqueous-based liquid (50 to 65% solids) from the reaction of primary alcohols (containing 15 to 20% secondary alcohol isomers) in a ratio of 20% C9, 40% C10, and 40% C11 with carbo- hydrates (average glucose to alkyl chain ratio 1.3 to 1.8). a-(p-Nonylphenol)-w-hydroxypoly(oxyethylene) mixture of Not to exceed 7% of pesticide Surfactants, related adjuvants of dihydrogen phosphate and monohydrogen phosphate formulation. surfactants esters and the corresponding ammonium, calcium, magnesium, potassium, sodium, and zinc salts of the phosphate esters; the nonyl group is a propylene trimer isomer and the poly(oxyethylene) content aver- ages 4–14 or 30 moles (CAS Reg. Nos. 51811–79–1, 59139–23–0, 67922–57–0, 68412–53–3, 68553–97–9, 68954–84–7, 99821–14–4, 152143–22–1, 51609–41– 7, 37340–60–6, 106151–63–7, 68584–47–4, 52503– 15–8, 68458–49–1). a-(p-Nonylphenyl)-w-hydroxypoly(oxyethylene) produced ...... Surfactants, related adjuvants of by the condensation of 1 mole of nonylphenol (nonyl surfactants group is a propylene trimer isomer) with an average of 4-14 or 30-90 moles of ethylene oxide; if a blend of products is used, the average number of moles of ethylene oxide reacted to produce any product that is a component of the blend shall be in the range of 4-14 or 30-90. a-(p-Nonylphenol)-w-hydroxypoly(oxyethylene) sulfate, Not to exceed 7% of pesticide Surfactants, related adjuvants of ammonium, calcium, magnesium, potassium, sodium, formulation. surfactants and zinc salts the nonyl group is propylene trimer iso- mer and the poly(oxyethylene) content averages 4 moles (CAS Reg. Nos. 9014–90–8, 9051–57–4, 9081– 17–8, 68649–55–8, 68891–33–8. 1-Octanal (CAS Reg. No. 124–13–0) ...... Not more than 0.2% of the pes- Odor masking agent ticide formulation. n-Octyl alcohol (CAS Reg. No. 111–87–5) ...... Solvent or co-solvent

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Inert ingredients Limits Uses

Octyl and decyl glucosides mixture with a mixture of octyl ...... Surfactants, related adjuvants of and decyloligosaccharides and related reaction prod- surfactants ucts (primarily n- decanol) produced as an aqueous- based liquid (68-72% solids) from the reaction of straight chain alcohols (C8(45%), C10 (55%)) with an- hydrous glucose. Oleic acid ...... Diluent Oleic acid diester of a-hydro-w-hydroxypoly (oxy- ...... Surfactants, related adjuvants of ethylene); the poly(oxyethylene) having average mo- surfactants lecular weight (in amu) 400. a-Oleoyl-w-hydroxypoly(oxyethylene), average molecular ...... Emulsifier weight (in amu) of 600. Oleyl alcohol (CAS Reg. No. 143–28–2 ...... 15% ...... Cosolvent Oxalic acid ...... No more oxalic acid should be Calcium chelating hard water in- used than is necessary to hibitor chelate calcium and in no case should more than 2 lb oxalic acid per acre be used. Palmitic acid ...... Diluent Pentaerythritol ester of maleic anhydride modified wood ...... Plasticizer rosin. Petrolatum, conforming to 21 CFR 172.880 ...... Coating agent Petroleum hydrocarbons, light odorless conforming to 21 ...... Solvent, diluent. CFR 172.884. Petroleum hydrocarbons, synthetic isoparaffinic, con- ...... Do. forming to 21 CFR 172.882. Petroleum naphtha, conforming to 21 CFR 172.250(d) ...... Component of coating agent Petroleum wax, conforming to 21 CFR 172.886(d) ...... Coating agent Phosphoric acid ...... Buffer Polyethylene, conforming to 21 CFR 177.1520(c) ...... Binder, carrier, and coating agent Polyethylene glycol[a-hydro-w-hydroxypoly(oxyethylene)]; ...... Surfactants, related adjuvants of mean molecular weight (in amu) 194 to 9,500 con- surfactants forms to 21 CFR 178.3750. Polyglycerol esters of fatty acids conforming to 21 CFR ...... Surfactants, related adjuvants of 172.854. surfactants Polyglyceryl phthalate ester of coconut oil fatty acids, in- None ...... Surfactants, related adjuvants of cluding fatty acid coco polymers with glyceryl and surfactants phthalic anhydride (CAS No. 67746–02–5) and coco- nut oil polymer with glyceryl and phthalic anhydride (CAS No. 66070–87–9). Poly(oxy-1,2-ethanediyl), a-(carboxymethyl)-w- ...... Surfactant (nonylphenoxy) produced by the condensation of 1 mole of nonylphenol (nonyl group is a propylene trimer isomer) with an average of 4-14 or 30-90 moles of ethylene oxide. The molecular weight (in amu) ranges are 454-894 and 1598-4238. Poly(oxy-1,2-ethanediyl), a-[tris(1-phenylethyl)phenyl]-w- For use in post-harvest applica- Surfactants hydroxy-, (CAS Reg. No. 99734–09–5). tions; not to exceed 15% by weight in pesticide formula- tions. Polyoxyethylene (20) sorbitan monostearate ...... Surfactants, related adjuvants of surfactants [Poly[oxy(methyl-1,2-ethanediyl)], a-[2-bis(2-hydroxy- Not to exceed 15% in the formu- Surfactant ethyl)amino]propyl]-w-hydroxy,-ether with a-hydro-w- lated product; only for use with hydroxypoly(oxy-1,2-ethanediyl) (1:2), mono-C12–16 glyphosate. alkyl ethers, (CAS Reg. No. 176022–82–5). Polysorbate 65, conforming to 21 CFR 172.838 ...... Emulsifier Potassium aluminum silicate ...... Solid diluent, carrier Potassium benzoate (Cas No. 582–25–2) ...... None ...... Preservative Potassium hydroxide ...... Neutralizer Potassium phosphate ...... Buffer Potassium sulfate ...... Solid diluent Propane ...... Propellant 1,3-Propanediol (CAS Reg. No. 504–63–2) ...... Solvent, co-solvent, diluent, or freeze-point depressant 2-Propanol, 1,1′,1″-nitrilotris- (CAS No. 122–20–3) ...... Without limitation ...... Neutralizer n-Propanol ...... Solvent, cosolvent 2-Propenoic acid, 2-methyl-, polymer with ethyl 2- ...... Encapsulating agent, dispensers, propenoate and methyl 2-methyl-2-propenoate, ammo- resins, fibers and beads nium salt (CAS Registration No. 55989–05–4), min- imum number average molecular weight (in amu), 18,900.. Propylene glycol ...... Solvent, cosolvent. Propylene glycol alginate (as defined in 21 CFR 172.858) ...... Defoaming agent

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Inert ingredients Limits Uses

Propyl gallate ...... Antioxidant Propyl p-hydroxybenzoate ...... Preservative for formulations Pyrophyllite ...... Solid diluent, carrier Rhizobium inoculants (e.g. Sinorhizobium, ...... All leguminous food commodities Bradyrhizobium & Rhizobium). Rosin, partially dimerized (as defined in 21 CFR ...... Surfactants, related adjuvants of 172.615). surfactants Rosin, partially hydrogenated (as defined in 21 CFR ...... Do. 172.615). Rosin, wood ...... Do. Salts of fatty acids, conforming to 21 CFR 172.863 ...... Binder, emulsifier, anticaking agent Sand ...... Solid diluent, carrier Shellac, bleached; refined, food grade, arsenic and rosin- ...... Coating agent free. Silver nitrate (Cas Reg. No. 7761–88–8) ...... For use on potatoes as post-har- Stabilizer vest treatment to control sprouting at no more than 0.06% by weight in pesticide formulations. Soapstone ...... Solid diluent Sodium acid pyrophosphate ...... Surfactant, suspending agent, dispersing agent, buffer Sodium alkyl naphthalenesulfonates (CAS Reg. Nos. Limited to no more than 30% by Surfactants, related adjuvants of 68909–83–1, 68909–84–2, 68909–82–0, 27213–90–7, weight in pesticide end-use surfactants 26264–58–4, 27178–87–6, 111163–74–7, 908356–16– products. 1, 25417–20–3, 25638–17–9, 145578–88–7, 1322–93– 6, 1323–19–9, 7403–47–6, 68442–09–1, 127646–44– 0, 908356–18–3). Sodium aluminum silicate ...... Solid diluent, carrier Sodium dioctylsulfosuccinate ...... Surfactants, related adjuvants of surfactants Sodium 1,4-dihexyl sulfosuccinate (CAS Reg. No. 3006– ...... Surfactants, related adjuvants of 15–3). surfactants Sodium 1,4-diisobutyl sulfosuccinate (CAS Reg. No...... Surfactants, related adjuvants of 127–39–9). surfactants Sodium 1,4-dipentyl sulfosuccinate (CAS Reg. No. 922– ...... Surfactants, related adjuvants of 80–5). surfactants Sodium DL-lactate (CAS Reg. No. 72–17–3) ...... Surfactant Sodium hexametaphosphate ...... Surfactant, emulsifier, wetting agent, suspending agent, dis- persing agent, buffer Sodium hydroxide ...... Neutralizer Sodium L-lactate (CAS Reg. No. 867–56–1) ...... Surfactant Sodium metasilicate ...... Surfactants, emulsifiers, wetting agents, dispersing agents, buffer Sodium monoalkyl and dialkyl (C6-C16) phenoxy Not to exceed 20% in pesticide Surfactants, related adjuvants of benzenedisulfonates and related acids (CAS Reg. Nos. formulations. surfactants 147732–59–0, 147732–60–3, 169662–22–0, 70191– 75–2, 36445–71–3, 39354–74–0, 70146–13–3, 119345–03–8, 149119–20–0, 149119–19–7, 119345– 04–9, 28519–02–0, 25167–32–2, 30260–73–2, 65143– 89–7, 70191–76–3).

Sodium a-olefinsulfonate (sodium C14-C16) (Olefin ...... Surfactants, related adjuvants of sulfonate). surfactants SodiumN-oleoyl- N-methyl taurine (CAS Reg. No. 137– ...... Surfactants, related adjuvants of 20–2). surfactants

Sodium and potassium salts of N-alkyl (C8–C18)-beta- Concentration in formulated end- Surfactants, related adjuvants of iminodipropionic acid where the C8–C18 is linear and use products not to exceed surfactants may be saturated and/or unsaturated (CAS Reg. Nos. 30% by weight in pesticide for- 110676–19–2, 3655–00–3, 61791–56–8, 14960–06–6, mulations. 26256–79–1, 90170–43–7, 91696–17–2, 97862–48–1). Sodium salt of sulfated oleic acid ...... Surfactants, related adjuvants of surfactants Sodium silicate ...... Surfactant, emulsifier, wetting agent, stabilizer, inhibitor Sodium starch glycolate (CAS Reg. No. 9063–38–1) ...... Granular and tableted products Disintegrant only; not to exceed 8% of the formulated product. Sodium sulfate ...... Solid diluent, carrier

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Inert ingredients Limits Uses

Sodium tripolyphosphate ...... Buffer, surfactant, suspending agent, dispersing agent, anticaking agent, conditioning agent Sorbic acid (CAS Reg. No. 110–44–1) ...... Preservative for formulations Sorbitan fatty acid esters (fatty acids limited to C12, C14, ...... Surfactants, related adjuvants or C16, and C18 containing minor amounts of associated surfactants. fatty acids) and their derivatives; the poly(oxyethylene) content averages 5-20 moles. Soybean flour ...... Expires May 24, 2005...... Surfactant Soybean oil-derived fatty acids ...... Solvent, cosolvent Stearic acid ...... Diluent a-Stearoyl-w-hydroxypoly(oxyethylene), average molec- ...... Emulsifier ular weight (in amu) of 600. a-Stearoyl-w-hydroxypoly(oxyethylene); the ...... Surfactants, related adjuvants of poly(oxyethylene) content averages either 8, 9, or 40 surfactants moles; if a blend of products is used, the average number of moles ethylene oxide reacted to produce any product that is a component of the blend shall be either 8, 9, or 40. Sucrose octaacetate ...... Adhesive Sulfite liquors and cooking liquors, spent, oxidized (CAS ...... Surfactant, related adjuvants of Reg. No. 68514–09–0). surfactants Sulfuric acid (CAS Reg. No.7664–93–9) ...... Not to exceed 10% of the pes- pH Control agent ticide formulation; non-aerosol formulations only. Sweet orange peel tincture (CAS Reg. No. 8028–48–6) .. Not to exceed 10% (weight/ Surfactant, fragrance, related ad- weight) in pesticide formulation. juvants of surfactants Synthetic paraffin and its succinic derivatives conforming ...... Carrier, binder, and carrying to 21 CFR 172.275. agent Synthetic petroleum wax, conforming to 21 CFR 172.888 ...... Binder, carrier, and coating agent Talc ...... Solid diluent, carriers Tall oil; fatty acids not less than 58%, rosin acids not ...... Surfactants, related adjuvants of more than 44%, unsaponifiables not more than 8%. surfactants Tartrazine ...... Dye Terpenes and terpenoids, turpentine oil, alpha-pinene ...... Surfactants, related adjuvants of fraction, polymd. (CAS Reg. No. 70750–57–1). surfactants 1,1,1,2-Tetrafluoroethane, (CAS Reg. No. 811–97–2) ...... Aerosol propellant Tetrahydrofurfuryl alcohol (THFA) (CAS Reg. No 97–99– Expires February 9, 2008 ...... Solvent/cosolvent 4). N,N,N′,N″,-tetrakis-(2-hydroxypropyl) ethylenediamine Concentration in formulated end- Stabilizer for formulation. (CAS Reg. No. 102–60–3). use products not to exceed 20% by weight in pesticide for- mulations. a-[p-(1,1,3,3-tetramethylbutyl)phenyl]-w- Not to exceed 7% of pesticide Surfactants related adjuvants of hydroxypoly(oxyethylene) produced by the condensa- formulation. surfactants tion of 1 mole of p-(1,1,3,3-tetramethylbutyl)phenol with a range of 1–14 or 30–70 moles of ethylene oxide: If a blend of products is used, the average range number of moles of ethylene oxide reacted to produce any product that is a component of the blend shall be in the range of 1–14 or 30–70 (CAS Reg. Nos. 9036–19– 5, 9002–93–1). 2,4,7,9-Tetramethyl-5-decyn-4, 7-diol ...... Not more than 2.5% of pesticide Surfactants, related adjuvants of formulation. surfactants Tetrasodium pyrophosphate ...... Anticaking agent, conditioning agent Thiosulfuric acid, disodium salt, anhydrous. (CAS Reg...... Dechlorinator, reducing agent No 7772–98–7). Thiosulfuric acid, disodium salt, pentahydrate. (CAS Reg...... Do. No. 10102–17–7). d-Alpha (CAS Reg. No. 9–02–9 ...... None ...... Safener d-Alpha tocopheryl acetate (CAS Reg. No. 58–95–7) ...... None ...... Do. dl-Alpha tocopherol (CAS Reg. No.10191–41–0) ...... None ...... Do. dl-Alpha tocopheryl acetate (CAS Reg. No. 7695–91–2) None ...... Do. Tricalcium phosphate ...... Surfactant, suspending agent, dispersing agent, anticaking agent, conditioning agent Trisodium phosphate ...... Surfactant, emulsifier, wetting agent Vermiculite ...... Solid diluent, carrier. Vitamin E (CAS Reg. No. 1406–18–4) ...... None ...... Safener

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Inert ingredients Limits Uses

Walnut shells ...... Leaching inhibitor, binder for water-dispersible aggregates, sticker and suspension sta- bilizer Wintergreen oil ...... Attractant Wood flour ...... Derived from wood free of chem- Solid diluent and carrier ical preservatives. Xanthan gum-modified, produced by the reaction of xan- Not more than 0.5% of pesticide Surfactant than gum and glyoxal (maximum 0.3% by weight). formulation. Xylene meeting the specifications listed in 21 CFR In pesticide formulations for grain Solvent, cosolvent 172.884(b)(4). storage only. Zeolite (hydrated alkali aluminum silicate) ...... Solid diluent, carrier Zinc oxide ...... Coating agent Zinc sulfate (basic and monohydrate) ...... Do. Zinc sulfate (basic and monohydrate) ...... Solid diluent, carrier

[69 FR 23117, Apr. 28, 2004]

EDITORIAL NOTE: For FEDERAL REGISTER citations affecting § 180.910, see the List of CFR Sections Affected, which appears in the Finding Aids section of the printed volume and at www.fdsys.gov.

§ 180.920 Inert ingredients used pre- when used in accordance with good ag- harvest; exemptions from the re- ricultural practice as inert (or occa- quirement of a tolerance. sionally active) ingredients in pesticide The following materials are exempt- formulations applied to growing crops ed from the requirement of a tolerance only:

Inert ingredients Limits Uses

Acetophenone ...... Attractant Adenosine (CAS Reg. No. 58–61–7) ...... Maximum of 0.5% of formulation Synergist Alder bark ...... Seed germination stimulator

Alkyl (C12-C16) dimethyl ammonio acetate (CAS Reg. 20% by weight in pesticide for- Surfactant Nos. 683–10–3, 2601–33–4 and 693–33–4. mulation.

a-Alkyl (minimum C6 linear, branched, saturated and/or Not to exceed 30% of pesticide Surfactants, related adjuvants of unsaturated)-w-hydroxypolyoxyethylene polymer with formulation. surfactants or without polyoxypropylene, mixture of di- and monohydrogen phosphate esters and the cor- responding ammonium, calcium, magnesium, monoethanolamine, potassium, sodium, and zinc salts of the phosphate esters; minimum oxyethylene content is 2 moles; minimum oxypropylene content is 0 moles (CAS Reg. Nos. 9046–01–9, 37280–82–3, 39464–66– 9, 42612–52–2, 50643–20–4, 52019–36–0, 58318–92– 6, 60267–55–2, 61837–79–4, 67711–84–6, 68070–99– 5, 68071–35–2, 68071–17–0, 68130–47–2, 68186–37– 8, 68186–36–7, 68311–02–4, 68425–73–0, 68458–48– 0, 68511–37–5, 68610–65–1, 68585–36–4, 68649–29– 6, 68815–11–2, 68908–64–5, 68891–13–4, 73038–25– 2, 78330–24–2, 108818–88–8, 154518–39–5, 317833– 96–8, 873662–29–4, 936100–29–7, 936100–30–0).

N-alkyl(C8-C18) dimethylamidopropylamines where the Not to exceed 20% by weight in Surfactants, related adjuvants of alkyl group is linear and may be saturated and/or un- herbicide formulations. surfactants saturated (CAS Reg. Nos. 109–28–4, 3179–80–4, 7651–02–7, 22890–10–4, 22890–11–5, 39669–97–1, 45267–19–4, 68140–01–2, 1147459–12–8, 146987– 98–6).

N-alkyl (C8-C18) primary amines and their acetate salts Concentration in formulated end- Surfactants, related adjuvants of where the alkyl group is linear and may be saturated use products not to exceed surfactants and/or unsaturated (CAS Reg. Nos. 61790–57–6, 10% by weight in herbicide 61790–58–7, 61790–59–8, 61790–60–1, 61788–46–3, products, 4% by weight in in- 61790–33–8, 68155–38–4). secticide products, and 4% by weight in fungicide products.

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Inert ingredients Limits Uses

N,N-Bis-a-ethyl-w-hydroxypoly(oxy-1,2-ethanediyl) C8– Not to exceed 25% in herbicide Surfactants, related adjuvants of C18 saturated and unsaturated alkylamines; the formulations and 10% in insec- surfactants poly(oxy-1,2-ethanediyl) content is 2–60 moles (CAS ticide and fungicide formula- Reg. Nos. 10213–78–2, 25307–17–9, 26635–92–7, tions. 26635–93–8, 288259–52–9, 58253–49–9, 61790–82– 7, 61791–14–8, 61791–24–0, 61791–26–2, 61791–31– 9, 61791–44–4, 68155–33–9, 68155–39–5, 68155–40– 8,70955–14–5, 73246–96–5, 1266162–49–5). N,N–Bis-a-ethyl-w-hydroxypoly(oxy-1,2-ethanediyl/ Not to exceed 25% in herbicide Surfactants, related adjuvants of oxy(methyl-1,2-ethanediyl) C8-C18 saturated and un- formulations and 10% in insec- surfactants saturated alkylamines; the poly(oxy-1,2-ethanediyl/ ticide and fungicide formula- oxy(methyl-1,2-ethanediyl) content is 2–60 moles (CAS tions. Reg. Nos. 68213–26–3, 68153–97–9, 75601–76–2). Aluminum sulfate ...... Safener adjuvant Ammonium chloride (CAS Reg. No. 12125–02–9) ...... Carrier/nutrient Ammonium formate (CAS Reg. No. 540–69–2) ...... Complexing or fixing agent Ammonium nitrate (CAS Reg. No. 6484–52–2) ...... Adjuvant/ intensifier for herbi- cides Ammonium polyphosphate (CAS Reg. No. 68333–79–9) ...... Sequestrant, buffer, or surfactant Barium sulfate ...... Carrier 1,4-Benzenedicarboxylic acid, dimethyl ester, polymer For use in honeybee hive Component of controlled release with 1,4-butanediol, adipic acid, and hexamethylene miticide formulations. agent diisocyanate, minimum number average molecular weight (in amu) 30,000 (CAS Reg. No. 55231–08–8). 1,2-Benzisothiazolin-3-one ...... Not more than 0.1% of formula- Preservative/stabilizer tion. Not more than 0.02 lb to be applied per acre. Boric acid ...... Sequestrant Buffalo gourd root powder (Cucurbita foetidissima root No more than 2.5 lbs/acre/sea- Gustatory stimulant powder); or, Zucchini juice (Cucurbita pepo juice) or son (3.4 gm/acre/season of Hawkesbury melon Citrullus lanatus.. Cucurbitacin). Butyl stearate ...... Defoamer g-Butyrolactone ...... Solvent C.I. Pigment Blue #15 (CAS Reg. No. 147–14–8; con- For seed treament use only ...... Dye, coloring agent taining no more than 50 ppm polychlorinated biphenyls (PCBs)). C.I. Pigment Green #7 (CAS Reg. No. 1328–53–6; con- For seed treatment use only ...... Dye, coloring agent taining no more than 50 ppm polychlorinated biphenyls (PCBs)). C.I. Pigment Red #112 (CAS Reg. No. 6535–46–2) ...... Seed treatment use only. Limited Coloring agent to 10% w/w of pesticide formu- lation. C.I. Pigment Violet #23 (CAS Reg. No. 6358–30–1; con- For seed treatment use only ...... Dye, coloring agent taining no more than 20 ppb of polychlorinated dibenzo-p-dioxins and/or polychlorinated dibenzofurans). C.I. Pigment Yellow 1 (CAS Reg. No. 2512–29–0) ...... Not to exceed 10% (weight/ Colorant weight) in pesticide formulation. Calcium gluconate (CAS Reg. No. 299–28–5) ...... Sequestrant Camphor (CAS Reg. No. 76–22–2) ...... Not more than 5% weight to Deodorant, adjust- weight (w/w) of pesticide for- ment mulations. Carbon Black (CAS Reg. No. 1333–86–4) ...... For seed treatment use only ...... Colorant Carbonic acid, dipotassium salt (CAS Reg. No. 584–08– ...... Buffering agent 7). Carbonic acid, dipotassium salt, trihydrate (CAS Reg...... Buffering agent No. 18662–52–7). Carboxymethyl guar gum sodium salt (CAS Reg. No. Without limitation ...... Thicker/drift reduction agent 39346–76–4). Carboxymethyl-hydroxypropyl guar (CAS Reg. No. Without limitation ...... Thicker/drift reduction agent 68130–15–4). Carous chloride ...... 10 ppm in formulation ...... Tagging agent Carrageenan, conforming to 21 CFR 172.260 ...... Not more than 0.15% of pes- Thickener and stabilizer for pes- ticide formulation. ticide formulations applied to seeds before planting Chlorobenzene ...... Contains not more than 1% im- Solvent, cosolvent purities. Not for use after edi- ble parts of plant begin to form. Do not graze livestock in treated areas within 48 hours after application.

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Inert ingredients Limits Uses

5-Chloro-2-methyl-4-isothiazolin-3-one (in combination Not more than 0.0022% (22.5 Preservative with 2-methyl-4-isothiazolin-3-one). ppm) in the formulation; 0.00022% (or 2.25 ppm) in the final solution applied to grow- ing crops. chloride (CAS Reg. No. 67–48–1) ...... As a solvent Choline hydroxide (CAS Reg No. 123–41–1) ...... Without limitation ...... Neutralizer Cis-isomer of 1-(3-chloroallyl)-3,5,7-triaza-1- Maximum of 0.14% by weight of Preservative azoniaadamantane chloride (CAS Reg. No. 51229–78– formulation. 8). Coco alkyl dimethyl amines (CAS Reg. No. 61788–93–0) Not to exceed 0.5% in pesticide Emulsifier formulation. Copper naphthenate ...... Not more than 2.5% of formula- Mercaptan scavenger in tech- tion; application limited to be- nical pesticide fore edible portions of plants begin to form. Cyclohexane ...... Solvent, cosolvent Cyclohexanone ...... Do. Cysteine (CAS Reg. No. 52–90–4) ...... Maximum of 0.5% of formulation Synergist D&C Green No. 6 ...... Dye D&C Red No. 17, technical grade ...... Dye D&C Red No. 33 (CAS Reg. No. 3567–66–6); meeting ...... Dye the specifications listed in 21 CFR 74.1333. D&C Violet No. 2, technical grade ...... Not more than 0.005% of pes- Dye ticide formulation. Decanamide, N,N-dimethyl (CAS Reg. No. 14433–76–2) ...... Emulsifier, solvent, cosolvent Diammonium phosphate (CAS Reg. No. 7783–28–0) ...... Buffer, surfactant dibenzylidene sorbitol (32647–67–9) ...... Thinning agent Diethanolamine ...... Stabilizer, inhibitor for formula- tions used before crop emerges from soil Diethanolamine salts of alkyl (C8-C24) benzenesulfonic Not to exceed 7% of pesticide Surfactants, related adjuvants of acid (CAS Reg. Nos. 26545–53–9, 67815–95–6, formulation. surfactants. 67889–94–5, 67889–95–6, 68259–34–7, 68478–47–7, 68567–68–0, 68815–34–9, 68815–37–2, 68891–02–1, 68953–97–9, 84989–15–1, 85338–09–6, 90194–39–1, 90194–40–4, 90218–08–9). Diethylene glycol ...... Deactivator, adjuvant for formula- tions used before crop emerges from soil Diethylene Glycol (CAS No. 111–46–6) ...... Without limitation ...... Solvent, stabilizer and/or anti- freeze Diethylene glycol and diethylene glycol monobutyl, ...... Deactivator for formulations used monoethyl, and monomethyl ethers. before crop emerges from soil, stabilizer Diethylene glycol mono butyl ether (CAS Reg. No. 112– Without limitation...... Pesticide inert ingredient as a 34–5). solvent, stabilizer and/or anti- freeze Diethylene Glycol MonoEthyl Ether (CAS Reg. No. 111– Without limitation...... Solvent, stabilizer and/or anti- 90–0). freeze Dimethylaminopropylamine, isopropylamine, ethanol- ...... Surfactants, related adjuvants of amine, and triethanolamine salts of alkyl (C8-C24) surfactants. benzenesulfonic acid (CAS Reg. Nos. 3088–30–0, 12068–12–1, 26264–05–1, 26836–07–7, 27323–41–7, 55470–69–4, 58089–99–9, 61886–59–7, 61931–76–8, 67924–05–4, 68110–32–7, 68259–35–8, 68411–31–4, 68442–72–8, 68567–69–1, 68584–24–7, 68584–25–8, 68648–81–7, 68648–96–4, 68649–00–3, 68815–30–5, 68815–35–0, 68910–32–7, 68953–93–5, 68953–98–0, 70528–84–6, 72391–21–0, 84961–74–0, 85480–55–3, 85480–56–4, 85995–82–0, 90194–42–6, 90194–53–9, 90194–54–0, 90194–55–1, 90218–09–0, 90218–11–4, 90218–35–2, 96687–54–6, 99924–49–9, 121617–08– 1, 157966–96–6, 193562–36–6, 319926–68–6, 877677–48–0, 1093628–27–3). 3,6-Dimethyl-4-octyn-3,6-diol ...... In pesticide formulations, for soil Surfactants, related adjuvants of prior to planting or to plants surfactants before edible parts form. Dimethyl sulfoxide ...... Solvent or cosolvent for formula- tions used before crop emerges from soil or prior to formation of edible parts of food plants Dipotassium hydrogen phosphate ...... Buffering agent

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Inert ingredients Limits Uses

Dipropylene glycol monomethyl ether ...... Stabilizer Douglas-fir bark, ground ...... Solid diluent, carrier Dysprosium chloride ...... 10 ppm in formulation ...... Tagging agent 1,2-ethanediamine,N,N,N″, N″-tetramethyl-, polymer with For use in pesticide formulations Adjuvant or water conditioner 1,1′-oxybis[2-chloroethane] (CAS Reg. No. 31075–24– applied to cotton or wheat only. 8). (S,S)–Ethylenediaminedisuccinic acid (CAS Reg. No...... Sequestrant or chelating agent 20846–91–7). Ethylene glycol ...... Antifreeze, deactivator for all pesticides used before crop emerges from soil and in her- bicides before or after crop emerges Ethylene glycol (CAS Reg. No. 107–21–1) ...... Without limitation ...... Pesticide inert ingredient as a solvent, stabilizer and/or anti- freeze. Ethylene glycol monobutyl ether ...... 2-Ethylhexanol ...... Cosolvent, defoamer, solvent for all pesticides used before crop emerges from soil and in her- bicides before or after crop emerges Europic chloride ...... 10 ppm in formulation ...... Tagging agent FD&C Blue No. 1 (CAS Reg. No. 3844–45–9) ...... For seed treatment use only ...... Dye, coloring agent FD&C Blue No. 1, methyl-polyethylene glycol derivative For seed treatment use only; Dye, coloring agent (CAS Reg. No. 9079–34–9). Number average molecular weight (in amu) is greater than 1,000; Not to exceed 5% of the formulated pesticide prod- uct. FD&C Blue No. 1, polyethylene glycol derivative (CAS For seed treatment use only; Dye, coloring agent Reg. No. 9079–33–8). Number average molecular weight (in amu) is greater than 1,000; Not to exceed 5% of the formulated pesticide prod- uct. FD&C Red No. 40 (CAS Reg. No. 25956–17–6) ...... For seed treatment use only. Not Dye, coloring agent to exceed 2% by weight of the pesticide formulation. Ferric chloride ...... Not greater than 2% of sus- pending, dispersing agent, pesticide formulation Fluoroapatite ...... Solid diluent, carrier Folic acid (CAS Reg. No. 59–30–3) ...... Maximum of 0.5% of formulation Synergist Gluconic acid (and sodium salt) ...... Sequestrant l-Glutamic acid (C5 H9 NO4´ CAS Reg. No. 56–86–0) ..... Seet treatment use only ...... Plant nutrient [alpha]-D-glucopyranoside, 2-ethylhexyl 6-O-[alpha]-D ...... Surfactant glucopyranosyl- (CAS Reg. No. 330980–61–5). [alpha]-D-glucopyranoside, 2-ethylhexyl (CAS Reg. No...... Surfactant 125590–73–0). (CAS Reg. No. 56–85–9) ...... Maximum of 0.5% of formulation Synergist Glycerol—propylene oxide polymer (CAS Reg. No...... Component in water-soluble film 25791–96–2). Glyceryl triacetate ...... Stabilizer Glyceryl tris-12-hydroxystearate ...... Flow control agent Graphite ...... Treatment aid for seeds Guar hydroxypropyltrimethylammonium chloride (CAS ...... Thickener/drift reduction agent Reg. No. 71329–50–5). Hexamethylenetetramine ...... Stabilizer for carriers in solid pesticide formulations 2-(2’-hydroxy-3′,5′-di-tert-amylphenyl) benzotriazole (CAS Maximum concentration of 0.6% Ultraviolet (UV) stabilizer Reg. No. 25973–55–1). in insecticide formulations ap- plied to adzuki beans, canola, chickpeas, cotton, faba beans, field peas, lentils, linola, lin- seed, lucerne, lupins, mung beans, navy beans, pigeon peas, safflower, sunflower, and vetch. 2-Hydroxy-4-n-octoxybenzophenone (CAS Reg. No. Not more than 0.2 pt of pesticide Light stabilizer 1843–05–6). formulation. Hydroxypropyl guar gum ...... Thickener Isobornyl acetate ...... Solvent Isobutyl alcohol ...... Do.

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Inert ingredients Limits Uses

Isobutylene-butene copolymers ...... For soil application only ...... Binder Isooctadecanol ...... Not more than 2% of pesticide Defoaming agent formulation. Lanthanum chloride ...... 10 ppm in formulation ...... Tagging agent. Magnesium nitrate (in combination with 2-methyl-4- None ...... Preservation isothiazolin-3-one and 5-chloro-2-methyl-4-isothiazolin- 3-one). Maleic acid and maleic anhydride ...... For pesticide formulations ap- Stabilizer plied to apples with a minimum preharvest interval of 21 days. Manganese carbonate ...... Plant nutrient D-mannose (CAS Reg. No. 3458–28–4) ...... Sequestrant, binder, filler Mesityl oxide ...... Not for use after edible parts of Solvent, cosolvent plant begin to form. Do not graze livestock in treated areas within 48 hours after ap- plication. Methionine (CAS Reg. No. 59–51–8) ...... Maximum of 0.5% of formulation Synergist Methyl alcohol ...... Do. Methyl ethyl ketone ...... Surfactant Methyl p- hydroxybenzoate ...... Preservative for formulations Methyl isobutyl ketone ...... Solvent, cosolvent 2-Methyl-4-isothiazolin-3-one (in combination with 5- Not more than 0.0022% (22.5 Preservative chloro-2-methyl-4-isothiazolin-3-one). ppm) in the formulation; 0.00022% (or 2.25 ppm) in the final solution applied to grow- ing crops. Mono-, di-, and trimethylnapthalenesulfonic acids and ...... Surfactants, related adjuvants of napthalenesulfonic acids formaldehyde condensates, surfactants ammonium and sodium salts (CAS Reg. Nos. 9008– 63–3, 9069–80–1, 9084–06–4, 36290–04–7, 91078– 68–1, 141959–43–5, 68425–94–5). Methyl oleate ...... Surfactant 2-Methyl-2,4-pentanediol ...... Solvent for formulations used be- fore crop emerges from soil Methyl poly(oxyethylene)C8–C18 alkylammonium Concentration in formulated end Surfactants, related adjuvants of chlorides where the poly(oxyethylene) content is n=2– use products not to exceed surfactants 15 and where C8–C18 alkyl is linear and may be satu- 10% by weight in herbicide rated or unsaturated (CAS Reg. Nos. 3010–24–0, products and 5% by weight in 18448–65–2, 70750–47–9, 22340–01–8, 67784–77–4, all other pesticide products. 64755–05–1, 61791–10–4, 28724–32–5, 28880–55–9, 68187–69–9, 68607–27–2, 60687–90–3. N-Methylpyrrolidone (CAS Reg. No. 872-504) ...... Solvent, cosolvent Mixed phytosterols (consisting of campesterol, sitosterol ...... Surfactant and stigmasterol, with minor amounts of associated plant sterols) derived from edible vegetable oils. Mono- and bis-(1H, 1H, 2H, 2H-perfluoroalkyl) Not more than 0.5% of pesticide Surfactant, related adjvants of phosphates where the alkyl group is even numbered formulation. Expires February surfactants and in the C6-C12 range. 9, 2008. Mono- and dialkyl (C8-C18) methylated ammonium chlo- ...... Surfactants, related adjuvants of ride compounds, where the alkyl group(s) (C8-C18) are surfactants derived from coconut, cottonseed, soya, tallow, or hogfat fatty acids. Morpholine 4-C6-12 Acyl Derivatives (CAS Reg. No...... As a solvent 887947–29–7). Nicotinamide (CAS Reg. No. 98–92–0) ...... Maximum of 0.5% of formulation Synergist a-(p-Nonylphenyl)-w-hydroxypoly(oxyethylene); produced ...... Surfactant by the condensation of 1 mole of nonylphenol (nonyl group is a propylene trimer isomer) with an average of 4-14 or 30-100 moles of ethylene oxide; if a blend of products is used, the average number of moles of ethylene oxide reacted to produce any product that is a component of the blend shall be in the range 4-14 or 30-100. Octanamide, N,N-dimethyl (CAS Reg. No. 1118–92–9) ...... Emulsifier, solvent, cosolvent a-Oleoyl-w-(oleoyloxy) poly(oxyethylene) derived from a- ...... Component of defoamers hydro-w-hydroxypoly(oxyethylene) (molecular weight 600 amu). Oxo-decyl acetate (CAS reg. No. 108419–33–6) ...... Solvent Oxo-heptyl acetate (CAS Reg. No. 90438–79–2) ...... Solvent Oxo-hexyl acetate (CAS Reg. No. 88230–35–7) ...... Solvent Oxo-nonyl acetate (CAS Reg. No. 108419–34–7) ...... Solvent Oxo-octyl acetate (CAS Reg. No. 108419–32–5) ...... Solvent Oxo-tridecyl acetate (CAS Reg. No. 108419–35–8) ...... Solvent

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Inert ingredients Limits Uses

Phenol ...... Solvent, cosolvent Phenol, 2-(2H-benzotriazol-2-yl)-6-dodecyl-4-methyl-, Not more than 10% by weight of UV stabilizer. (CAS Reg. No. 23328–53–2). pesticide formulations. Phenolsulfonic acid—formaldehyde—urea condensate Applied to growing plants only .... Dispersant surfactant and its sodium salt. (Phthalocyaninato (2)) copper; (C.I. pigment blue No. 15) When used as a colorant in low- Coloring agent, pigment density plastic films. Pigment red 48 ...... For seed treatment use only ...... Dye a-Pinene ...... Not more than 2% of formulation Stabilizer by weight. Poly(oxy-1,2-ethanediyl), a-isotridecyl-w-methoxy (CAS At a maximum of 10% in formu- Surfactant Reg. No. 345642–79–7). lation. Poly(oxy-1,2-ethanediyl), a-(3-carboxy-1-oxosulfopropyl)- Not to exceed 0.125% for seed Surfactant. w-hydroxy-, (C10–C12)-alkyl ethers, disodium salts, treatment use only. polyoxylene content averages 4–5 moles (CAS Reg. No. 68815–56–5). Poly(oxy-1,2-ethanediyl), a-(3-carboxy-1-oxosulfopropyl)- Not to exceed 0.125% for seed Surfactant w-hydroxy-, (C10–C16)-alkyl ethers, disodium salts, treatment use only. polyoxyethylene content averages 5 moles (CAS Reg. No. 68954–91–6). Poly(oxyethylene) adducts of mixed phytosterols (such ...... Surfactant, related adjuvants sterols to consist of campesterol, stigmasterol and sito- sterol with minor amounts of associated plant sterols) derived from edible vegetable oils; polyoxyethylene content averaging 5-26 moles. Polyoxyethylene polyoxypropylene mono(di-sec- Limited to herbicide formulations Surfactants, related adjuvants of butylphenyl) ether (CAS Reg. No. 69029–39–6). only, and to no more than 30% surfactants by weight in herbicide formula- tions intended for application to turf. Poly(oxyethylene) (5) sorbitan monooleate ...... Surfactants, related adjuvants of surfactants Polysorbate 60, conforming to 21 CFR 172.836 ...... Surfactant Potassium dihydrogen phosphate ...... Buffering agent 2-Propanamine, compound with a-phosphono-w- Not more than 15% in the formu- Surfactant butoxypoly (oxy-1,2-ethanediyl) (2:1) (CAS Reg. No. lated product. 431040–31–2). 2-Propanamine, compounds with polyethylene glycol di- Not more than 15% in the formu- Surfactant hydrogen phosphate C8–10- alkyl ether (2:1) (CAS Reg. lated product. No. 431062–72–5). Propylene glycol monomethyl ether ...... Solvent Pyridoxine (CAS Reg. No. 65–23–6) ...... Maximum of 0.5% of formulation Synergist Rosin, dark wood (as defined in 21 CFR ...... Surfactants, related adjuvants of 178.3870(a)(1)(v)). surfactants Rosin, gum ...... Do. Rosin, tall oil ...... Do. Scandium chloride ...... 10 ppm in formulation ...... Tagging agent Sodium bisulfate (CAS Reg. No. 7681–38–1) ...... Acidifying/buffering agent Sodium 1,4-dicyclohexyl sulfosuccinate ...... Surfactants, related adjuvants of surfactants Sodium 1,4-dihexyl sulfosuccinate (CAS Reg. No. 3006– ...... Surfactants, related adjuvants of 15–3). surfactants Sodium dihydrogen phosphate (CAS Reg. No. 7558–80– ...... Buffering agent 7) conforming to 21 CFR 182.6778. Sodium 1,4-diisobutyl sulfosuccinate (CAS Reg. No...... Surfactants, related adjuvants of 127–39–9). surfactants Sodium 1,4-dipentyl sulfosuccinate (CAS Reg. No. 922– ...... Surfactants, related adjuvants of 80–5). surfactants Sodium metaborate ...... Sequestrant Sodium molybdate ...... Plant nutrient Sodium nitrate ...... Solid diluent Sodium nitrite ...... Not more than 3% of pesticide Stabilizer, inhibitor. formulation. Sodium o-phenylphenate ...... Not more than 0.1% of pesticide Preservative for formulation formulation. Sodium salt of the insoluble fraction of rosin ...... Surfactants, related adjuvants of surfactants Sodium salts of N-alkyl (C8-C18)-beta-iminodipropionic Concentration in formulated end- Surfactants, related adjuvants of acid where the C8-C18 is linear and may be saturated use products not to exceed surfactants and/or unsaturated (CAS Reg. Nos. 3655-00-3, 61791- 30% by weight in pesticide for- 56-8, 14960-06-6, 26256-79-1, 90170-43-7, 91696-17- mulations. 2, 97862-48-1). Sodium tetraborate ...... Not more than 2% of pesticide Buffering agent; corrosion inhib- formulation. itor

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Inert ingredients Limits Uses

Sulfonic acids, C13-17-sec-alkane, sodium salts (CAS Not to exceed 40% by weight in Surfactant Reg. No. 85711–69–9). non-residential use pesticide formulation only. Sulfonic acids, C14-17-sec-alkane, sodium salts (CAS Not to exceed 40% by weight in Surfactant Reg. No. 97489–15–1). non-residential pesticide for- mulation only. Tallowamine, ethoxylated, mixture of dihydrogen phos- Not to exceed 20% of pesticide Surfactants, related adjuvants of phate and monohydrogen phosphate esters and the formulation. surfactants corresponding ammonium, calcium, potassium, and so- dium salts of the phosphate esters, where the poly(oxyethylene) content averages 2–20 moles (CAS Reg. No. 68308–48–5). Tannin ...... Dispersing agent Tertiary butylhydroquinone ...... Antioxidant 1-Tetradecanamine, N,N-dimethyl-, N-oxide (CAS Reg...... Component in water-soluble film No. 3332–27–2). N,N,N′,N″-Tetrakis-(2-hydroxypropyl) ethylenediamine Concentration in formulated end- Stabilizer for formulations (CAS Reg. No. 102–60–3). use products not to exceed 20% by weight in pesticide for- mulations. 2,4,7,9-Tetramethyl-5-decyne 4,7-diol ...... In pesticide formulations, for ap- Surfactants, related adjuvants of plication to soil prior to planting surfactants or to plants before edible parts form. Tetrapotassium pyrophosphate (CAS Reg. No. 7320– Not to exceed 10% of formula- Sequestrant, anticaking agent, 345). tion. conditioning agent Titanium dioxide (CAS Reg. No. 13463–67–7) ...... Pigment/coloring agent in plastic bags used to wrap growing ba- nana (preharvest), colorant on seeds for planting Toluenesulfonic acid and its ammonium, calcium, magne- ...... Solvent, cosolvent sium, potassium, sodium, and zinc salts. Triethanolamine ...... Stabilizer, inhibitor for formula- tions used before crop emerges from soil Triethanolamine (CAS Reg. No. 102–71–6) ...... Stabilizer, inhibitor Triethylene glycol ...... Deactivator Triethyl phosphate ...... Stabilizer for formulations used before crop emerges from soil Trimethylolpropane (CAS Reg. No. 77–99–6) ...... Not to exceed 15% by weight of Component in water-soluble film the film. a-[2,4,6-Tris[1-(phenyl)ethyl]phenyl]-w-hydroxy Not more than 15% of the formu- Surfactant. poly(oxyethylene), the poly(oxyethylene) content aver- lation. ages 4-150 moles). a-[2,4,6-Tris[1-(phenyl)ethyl]phenyl]-w-hydroxy Not more than 15% of the formu- Do. poly(oxyethylene); mixture of monohydrogen and di- lation. hydrogen phosphate esters and the corresponding am- monium, calcium, magnesium, potassium, sodium, and zinc salts, the poly(oxyethylene) content averages 4- 150 moles). a-[2,4,6-Tris[1-(phenyl)ethyl]phenyl]-w-hydroxy Not more than 15% of the pes- Do. poly(oxyethylene) sulfate, and the corresponding am- ticide formulation. monium, calcium, magnesium, potassium, sodium, and zinc salts, the poly(oxyethylene) content averages 4- 150 moles. Tryptophan (CAS Reg. No. 73–22–3) ...... Maximum of 0.5% of formulation Synergist Valeric acid, normal ...... Not more than 2% in pesticide Stenching agent or odorant formulations. Xylene ...... Solvent, cosolvent Xylenesulfonic acid its ammonium calcium, magnesium, ...... Surfactants, related adjuvants of potassium, sodium, and zinc salts. surfactants Yucca extract from Yucca schidigera ...... Wetting agent Ytterbium chloride ...... 10 ppm in formulation ...... Tagging agent Yttrium chloride ...... 10 ppm in formulation ...... Tagging agent Zinc orthophosphate ...... Plant nutrient and safener Zinc stearate, conforming to 21 CFR 182.5994 and ...... Flow control agent 582.5994.

[69 FR 23124, Apr. 28, 2004]

EDITORIAL NOTE: For FEDERAL REGISTER citations affecting § 180.920, see the List of CFR Sections Affected, which appears in the Finding Aids section of the printed volume and at www.fdsys.gov.

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§ 180.930 Inert ingredients applied to when used in accordance with good ag- animals; exemptions from the re- ricultural practice as inert (or occa- quirement of a tolerance. sionally active) ingredients in pesticide The following materials are exempt- formulations applied to animals: ed from the requirement of a tolerance

Inert ingredients Limits Uses

Acetic acid (CAS Reg. No. 64–19–7) ...... Not more than 0.5% of pesticide Catalyst formulation. Acetic anhydride ...... Solvent, cosolvent, stabilizer Acetone (Cas Reg. No. 67–64–1) ...... Solvent or cosolvent Alkanoic and alkenoic acids, mono- and diesters of a- ...... Emulsifiers hydro-w-hydroxypoly(oxyethylene) with molecular weight (in amu) range of 200 to 6,000.

Alkyl (C8-C24) benzenesulfonic acid and its ammonium, ...... Surfactants, emulsifier, related calcium, magnesium, potassium, sodium, and zinc adjuvants of surfactants salts.

Alkyl (C12-C16) dimethyl ammonio acetate (CAS Reg. 20% by weight in pesticide for- Surfactant Nos. 683–10–3, 2601–33–4 and 693–33–4. mulation.

a-alkyl(C6- C15)-w-hydroxypoly(oxyethylene)sulfate, and Not to exceed 30% of formula- Surfactants, related adjuvants of its ammonium, calcium, magnesium, potassium, so- tion. surfactants. dium, and zinc salts, poly(oxyethylene) content aver- ages 2–4 moles (CAS Reg. Nos.: 3088–31–1, 3694– 74–4, 9004–82–4, 9004–84–6, 9021–91–4, 9086–52– 6, 13150–00–0, 15826–16–1, 25446–78–0, 26183–44– 8, 27140–00–7, 27731–61–9, 27731–61–9, 27731–62– 0, 32612–48–9, 34431–25–9, 35015–74–8, 50602–06– 7, 52286–18–7, 52286–19–8, 54116–08–4, 55901–67– 2, 61702–79–2, 61894–66–4, 62755–21–9, 63428–85– 3, 63428–86–4, 63428–87–5, 65086–57–9, 65086–79– 5, 65104–74–7, 65122–38–5, 67674–66–2, 67762–19– 0, 67762–21–4, 67845–82–3, 67845–83–4, 67923–90– 4, 68037–05–8, 68037–06–9, 68171–41–5, 68424–50– 0, 68511–39–7, 68585–34–2, 68610–66–2, 68611–29– 0, 68611–55–2, 68649–53–6, 68890–88–0, 68891–29– 2, 68891–30–5, 68891–38–3, 69011–37–6, 73665–22– 2, 75422–21–8, 78330–16–2, 78330–17–3, 78330–25– 3, 78330–26–4, 78330–27–5, 78330–28–6, 78330–29– 7, 78330–30–0, 96130–61–9, 106597–03–9, 110392– 50–2, 119432–41–6, 125301–88–4, 125301–89–5, 125301–92–0, 125736–54–1, 157707–85–2, 160104– 51–8, 160901–27–9, 160901–28–0, 160901–29–1, 160901–30–4, 161025–28–1, 161074–79–9, 162063– 19–6, 219756–63–5).

a-alkyl (C12-C15)-w-hydroxypoly (oxypropylene)poly Not to exceed 20% of pesticide Surfactant (oxyethylene)copolymers (where the formulations. poly(oxypropylene) content is 3-60 moles and the poly(oxyethylene) content is 5-80 moles), the resulting ethoxylated propoxylated (C12-C15) alcohols having a minimum molecular weight (in amu) of 1,500, CAS Reg. No. 68551–13–3.

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Inert ingredients Limits Uses

a-alkyl-w-hydroxypoly (oxypropylene) and/or poly (oxy- ...... Surfactants, related adjuvants of ethylene) polymers where the alkyl chain contains a surfactants. minimum of six carbons (CAS Reg. No.: 9002–92–0; 9004–95–9; 9004–98–2; 9005–00–9; 9035–85–2; 9038–29–3; 9038–43–1; 9040–05–5; 9043–30–5; 9087–53–0; 25190–05–0; 24938–91–8; 25231–21–4; 26183–52–8; 26468–86–0; 26636–39–5; 27252–75–1; 27306–79–2; 31726–34–8; 34398–01–1; 34398–05–5; 37251–67–5; 37311–00–5; 37311–01–6; 37311–02–7; 37311–04–9; 39587–22–9; 50861–66–0; 52232–09–4; 52292–17–8; 52609–19–5; 57679–21–7; 59112–62–8; 60828–78–6; 61702–78–1; 61725–89–1; 61791–13–7; 61791–20–6; 61791–28–4; 61804–34–0; 61827–42–7; 61827–84–7; 62648–50–4; 63303–01–5; 63658–45–7; 63793–60–2; 64366–70–7; 64415–24–3; 64415–25–4; 64425–86–1; 65104–72–5; 65150–81–4; 66455–14–9: 66455–15–0; 67254–71–1; 67763–08–0; 68002–96–0; 68002–97–1; 68131–39–5; 68131–40–8; 68154–96–1; 68154–97–2; 68154–98–3; 68155–01–1; 68213–23–0; 68213–24–1; 68238–81–3; 68238–82–4; 68409–58–5; 68409–59–6; 68439–30–5; 68439–45–2; 68439–46–3; 68439–48–5; 68439–49–6; 68439–50–9; 68439–51–0; 68439–53–2; 68439–54–3; 68458–88–8; 68526–94–3; 68526–95–4; 68551–12–2; 68551–13–3; 68551–14–4; 68603–20–3; 68603–25–8; 68920–66–1; 68920–69–4; 68937–66–6; 68951–67–7; 68954–94–9; 68987–81–5; 68991–48–0; 69011–36–5; 69013–18–9; 69013–19–0; 69227–20–9; 69227–21–0; 69227–22–1; 69364–63–2; 70750–27–5; 70879–83–3; 70955–07–6; 71011–10–4; 71060–57–6; 71243–46–4; 72066–65–0; 72108–90–8; 72484–69–6; 72854–13–8; 72905–87–4; 73018–31–2; 73049–34–0; 74432–13–6; 74499–34–6; 78330–19–5; 78330–20–8; 78330–21–9; 78330–23–1; 79771–03–2; 84133–50–6; 85422–93–1; 97043–91–9; 97953–22–5; 102782–43–4; 103331–86–8; 103657–84–7; 103657– 85–8; 103818–93–5; 103819–03–0; 106232–83–1; 111905–54–5; 116810–31–2; 116810–32–3; 116810– 33–4; 120313–48–6; 120944–68–5; 121617–09–2; 126646–02–4; 126950–62–7; 127036–24–2; 139626– 71–4; 152231–44–2; 154518–36–2; 157627–86–6; 157627–88–8; 157707–41–0; 157707–43–2; 159653– 49–3; 160875–66–1; 160901–20–2; 160901–09–7; 160901–19–9; 161025–21–4; 161025–22–5; 166736– 08–9; 169107–21–5; 172588–43–1; 176022–76–7; 196823–11–7; 287935–46–0; 288260–45–7; 303176– 75–2; 954108–36–2).

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Inert ingredients Limits Uses

a-alkyl (minimum C6 linear, branched, saturated and/or Not to exceed 30% of formula- Surfactants, related adjuvants of unsaturated)-w-hydroxypolyoxyethylene polymer with tion. surfactants. or without polyoxypropylene, mixture of di- and monohydrogen phosphate esters and the cor- responding ammonium, calcium, magnesium, monoethanolamine, potassium, sodium, and zinc salts of the phosphate esters; minimum oxyethylene content is 2 moles; minimum oxypropylene content is 0 moles, (CAS Reg. Nos.: 9004–80–2, 9046–01–9, 26982–05– 8, 31800–89–2, 37280–82–3, 37281–86–0, 39341–09– 8, 39341–65–6, 39464–66–9, 39464–69–2, 42612–52– 2, 50643–20–4, 50668–50–3, 51325–10–1, 51884–64– 1, 52019–36–0, 52019–38–2, 52019–38–2, 57486–09– 6, 58206–38–5, 58318–92–6, 58857–49–1, 59112–71– 9, 60267–55–2, 61837–79–4, 62362–49–6, 62482–61– 5, 63747–86–4, 63887–54–7, 63887–55–8, 66020–37– 9, 66272–25–1, 66281–20–7, 67711–84–6, 67786–06– 5, 67989–06–4, 68070–99–5, 68071–17–0, 68071–35– 2, 68071–37–4, 68130–44–9, 68130–45–0, 68130–46– 1, 68130–47–2, 68186–29–8, 68186–34–5, 68186–36– 7, 68186–37–8, 68238–84–6, 68311–02–4, 68311–04– 6, 68332–75–2, 68389–72–0, 68400–75–9, 68413–78– 5, 68425–73–0, 68425–75–2, 68439–39–4, 68458–48– 0, 68511–15–9, 68511–36–4, 68511–37–5, 68551–05– 3, 68585–15–9, 68585–16–0, 68585–17–1, 68585–36– 4, 68585–39–7, 68603–24–7, 68607–14–7, 68610–64– 0, 68610–65–1, 68649–29–6, 68649–30–9, 68650–84– 0, 68815–11–2, 68855–46–9, 68856–03–1, 68890–90– 4, 68890–91–5, 68891–12–3, 68891–13–4, 68891–26– 9, 68908–64–5, 68909–65–9, 68909–67–1, 68909–69– 3, 68921–24–4, 68921–60–8, 68954–87–0, 68954–88– 1, 68954–92–7, 68987–35–9, 69029–43–2, 69980–69– 4, 70247–99–3, 70248–14–5, 70844–96–1, 70903–63– 8, 71965–23–6, 71965–24–7, 72480–27–4, 72623–67– 7, 72623–68–8, 72828–56–9, 72828–57–0, 73018–34– 5, 73038–25–2, 73050–08–5, 73050–09–6, 73361–29– 2, 73378–71–9, 73378–72–0, 73559–42–9, 73559–43– 0, 73559–44–1, 73559–45–2, 74499–76–6, 76930–25– 1, 78041–18–6, 78330–22–0, 78330–24–2, 82465–25– 6, 84843–37–8, 91254–26–1, 93925–54–3, 95014–34– 9, 96416–89–6, 99924–51–3, 103170–31–6, 103170– 32–7, 106233–09–4, 106233–10–7, 108818–88–8, 110392–49–9, 111798–26–6, 111905–50–1, 116671– 23–9, 117584–36–8, 119415–05–3, 120913–45–3, 121158–61–0, 121158–63–2, 123339–53–7, 125139– 13–1, 125301–86–2, 125301–87–3, 126646–03–5, 129208–04–4, 129870–77–5, 129870–80–0, 130354– 37–9, 136504–88–6, 143372–50–3, 143372–51–4, 144336–75–4, 146815–57–8, 151688–56–1, 154518– 39–5, 154518–40–8, 155240–11–2, 159704–69–5, 160498–49–7, 160611–24–5, 171543–66–1, 172027– 16–6, 172274–69–0, 176707–42–9, 181963–82–6, 188741–55–1, 191940–53–1, 210493–60–0, 210993– 53–6, 246159–55–7, 251298–11–0, 261627–68–3, 290348–69–5, 290348–70–8, 317833–96–8, 340681– 28–9, 422563–19–7, 422563–26–6, 522613–09–8, 717140–06–2, 717140–09–5, 717827–29–7, 762245– 80–7, 762245–81–8, 866538–89–8, 866538–90–1, 873662–29–4, 913068–96–9, 936100–29–7, 936100– 30–0, 1072943–56–6, 1087209–87–7, 1174313–54–2, 1187742–89–7, 1187743–35–6, 1205632–03–6, 1233235–49–8, 1451002–50–8, 1456802–88–2, 1456802–89–3, 1456803–12–5). N-alkyl (C8-C18) primary amines and their acetate salts Concentration in formulated end- Surfactants, related adjuvants of where the alkyl group is linear and may be saturated use products not to exceed surfactants and/or unsaturated (CAS Reg. Nos. 61790–57–6, 10% by weight in herbicide 61790–58–7, 61790–59–8, 61790–60–1, 61788–46–3, products, 4% by weight in in- 61790–33–8, 68155–38–4). secticide products, and 4% by weight in fungicide products.

Alkyl (C8-C18) sulfate and its ammonium, calcium, mag- ...... Surfactant nesium, potassium, sodium, and zinc salts.

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Inert ingredients Limits Uses

N,N-Bis-a-ethyl-w-hydroxypoly(oxy-1,2-ethanediyl) C8– Not to exceed 25% in herbicide Surfactants, related adjuvants of C18 saturated and unsaturated alkylamines; the formulations and 10% in insec- surfactants poly(oxy-1,2-ethanediyl) content is 2–60 moles (CAS ticide and fungicide formula- Reg. Nos. 10213–78–2, 25307–17–9, 26635–92–7, tions. 26635–93–8, 288259–52–9, 58253–49–9, 61790–82– 7, 61791–14–8, 61791–24–0, 61791–26–2, 61791–31– 9, 61791–44–4, 68155–33–9, 68155–39–5, 68155–40– 8,70955–14–5, 73246–96–5, 1266162–49–5). N,N-Bis-a-ethyl-w-hydroxypoly(oxy-1,2-ethanediyl/ Not to exceed 25% in herbicide Surfactants, related adjuvants of oxy(methyl-1,2-ethanediyl) C8-C18 saturated and un- formulations and 10% in insec- surfactants saturated alkylamines; the poly(oxy-1,2-ethanediyl/ ticide and fungicide formula- oxy(methyl-1,2-ethanediyl) content is 2–60 moles (CAS tions. Reg. Nos. 68213–26–3, 68153–97–9, 75601–76–2). Ascorbyl palmitate ...... Preservative Attapulgite-type clay ...... Solid diluent, carrier Barium sulfate (CAS Reg. No. 7727–43–7) ...... Carrier, density control agent Benzoic acid ...... Preservative for formulations 2-Bromo-2-nitro-1,3-propanediol (CAS Reg. No. 52–51– 0.04% or less by weight of the In-can preservative 7). total pesticide formulation. Butane ...... Propellant n-Butanol (CAS Reg. No. 71–36–3) ...... Solvent for blended emulsifiers n-Butyl benzoate (CAS RN 136–60–7) ...... Solvent Butylated hydroxyanisole ...... Antioxidant Butylated hydroxytoluene ...... Do. Calcium carbonate ...... Solid diluent, carrier Calcium chloride ...... Stabilizer Calcium silicate, hydrated calcium silicate ...... Anticaking agent, solid diluent, carrier C9 rich aromatic hydrocarbons (CAS Reg. No. 64742– ...... Solvent. 95–6). C10–11 rich aromatic hydrocarbons (CAS Reg. No...... Solvent. 64742–94–5). C11–12 rich aromatic hydrocarbons (CAS Reg. No...... Solvent. 64742–94–5). Calcium stearate (CAS Reg. No. 1592–23–0) ...... Stabilizer, component of plastic animal tag Calcium sulfate ...... Solid diluent, carrier Carbon black (CAS Reg. No. 1333–86–4) ...... Colorant/pigment in animal tag Carbon Dioxide (CAS Reg. No. 124–38–9) ...... None ...... Propellant Carrageenan, conforming to 21 CFR 172.620 ...... Minimum molecular weight (in Thickener amu): 100,000. Cyclohexanone ...... Solvent, cosolvent D&C Green No. 6 ...... Dye, coloring agent D&C Red No. 17 ...... Do. D&C Violet No. 2 ...... Do. Dialkyl (C8-C18) dimethylammonium chloride ...... Not more than 0.2% in silica hy- Flocculating agent in the manu- drated silica. facture of silica hydrated silica for use as a solid diluent, car- rier Diatomite (diatomaceous earth) ...... Solid diluent, carrier Diethanolamine salts of alkyl (C8-C24) benzenesulfonic Not to exceed 7% of pesticide Surfactants, related adjuvants of acid (CAS Reg. Nos. 26545–53–9, 67815–95–6, formulation. surfactants. 67889–94–5, 67889–95–6, 68259–34–7, 68478–47–7, 68567–68–0, 68815–34–9, 68815–37–2, 68891–02–1, 68953–97–9, 84989–15–1, 85338–09–6, 90194–39–1, 90194–40–4, 90218–08–9). Diethylaminoethanol, ethoxylated, propoxylated, reaction ...... Surfactant products with fatty acid dimers, minimum number aver- age molecular weight (in amu), 1,200 (CAS Reg. No. 1173188–75–4). Diethylaminoethanol, ethoxylated, propoxylated, reaction ...... Surfactant products with fatty acid trimers, minimum number aver- age molecular weight (in amu), 1,200 (CAS Reg. No. 1173188–83–4). Diethylaminoethanol, ethoxylated, reaction products with ...... Surfactant acid trimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173188–81–2). Diethylaminoethanol, ethoxylated, reaction product with ...... Surfactant fatty acid dimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173188–72–1). Diethylphthalate ...... Solvent, cosolvent

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Inert ingredients Limits Uses

1,1-Difluoroethane (CAS Reg. No. 75–37–6) ...... For aerosol pesticide formula- Aerosol propellant tions used for insect control in food- and feed-handling estab- lishments and animals. Dimethyl ether (CAS Reg. No. 115–10–6) ...... Propellant Dimethylaminoethanol, ethoxylated, propoxylated, reac- ...... Surfactant tion products with fatty acid dimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173188–42–5). Dimethylaminoethanol, ethoxylated, propoxylated reac- ...... Surfactant tion products with fatty acid trimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173188–67–4). Dimethylaminoethanol, ethoxylated, reaction products ...... Surfactant with fatty acid trimers, minimum number average mo- lecular weight (in amu), 1,200 (CAS Reg. No. 1173188–38–9). Dimethylaminoethanol, ethoxylated, reaction products ...... Surfactant with fatty acid trimers, minimum number average mo- lecular weight (in amu), 1,200 (CAS Reg. No. 1173188–49–2). Dimethylaminopropylamine, isopropylamine, ethanol- ...... Surfactants, related adjuvants of amine, and triethanolamine salts of alkyl (C8-C24) surfactants. benzenesulfonic acid (CAS Reg. Nos. 3088–30–0, 12068–12–1, 26264–05–1, 26836–07–7, 27323–41–7, 55470–69–4, 58089–99–9, 61886–59–7, 61931–76–8, 67924–05–4, 68110–32–7, 68259–35–8, 68411–31–4, 68442–72–8, 68567–69–1, 68584–24–7, 68584–25–8, 68648–81–7, 68648–96–4, 68649–00–3, 68815–30–5, 68815–35–0, 68910–32–7 68953–93–5, 68953–98–0, 70528–84–6, 72391–21–0, 84961–74–0, 85480–55–3, 85480–56–4, 85995–82–0, 90194–42–6, 90194–53–9, 90194–54–0, 90194–55–1, 90218–09–0, 90218–11–4, 90218–35–2, 96687–54–6, 99924–49–9, 121617–08–1, 157966–96–6, 193562– 36–6, 319926–68–6, 877677–48–0, 1093628–27–3).. 3,6-Dimethyl-4-octyne-3,6-diol ...... Not more than 2.5% of pesticide Surfactants, related adjuvants of formulation. surfactants Dimethylpolysiloxane (CAS Reg. No. 9016–00–6) ...... Defoaming agent Di-n-butyl carbonate (CAS Reg. No. 542–52–9) ...... Solvent Dipropylene glycol monomethyl ether ...... Surfactants, related adjuvants of surfactants Epoxidized soybean oil (CAS Reg. No. 8013–07–8) ...... Stabilizer, plasticizer, component animal tag Ethyl alcohol ...... Solvent, cosolvent Ethyl maltol (CAS Reg. No.4940–11–8) ...... Not more than 0.2 % of the pes- Odor masking agent ticide formulation. Ethylene oxide adducts of 2,4,7,9-tetramethyl-5- ...... Surfactants, related adjuvants of decynediol, the ethylene oxide content averages 3.5, surfactants 10 or 30 moles (CAS Reg. No. 9014–85–1). 2-Ethyl-1-hexanol (CAS Reg. No. 104–76–7) ...... Not more than 10% of pesticide Solvent, adjuvant of surfactants FD&C Blue No. 1 ...... Dye, coloring agent FD&C Yellow No. 6 Aluminum Lake (CAS Reg. No. Not more than 2% by weight of Pigment in animal tag and similar 15790–07–5). pesticide formulation. slow-release devices D-glucopyranose, oligomeric, C10–16-alkyl glycosides ...... Surfactant (CAS Reg. No. 110615–47–9). Glycerol monooleate ...... Surfactants, related adjuvants of surfactants Glyceryl monostearate ...... Emulsifier Glyceryl tris-12-hydroxystearate ...... Flow control agent Graphite ...... Solid diluent, carrier n-Hexyl alcohol (CAS Reg. No. 111–27–3) ...... Solvent, cosolvent Hydroxyethylmorpholine, ethoxylated, propoxylated, reac- ...... Surfactant tion products with fatty acid dimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173189–06–4). Hydroxyethylmorpholine, ethoxylated, propoxylated, reac- ...... Surfactant tion products with fatty acid trimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173188–67–4). Hydroxyethylmorpholine, ethoxylated, reaction products ...... Surfactant with fatty acid dimers, minimum number average mo- lecular weight (in amu), 1,200 (CAS Reg. No. 1173189–00–8).

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Inert ingredients Limits Uses

Hydroxyethylmorpholine, ethoxylated, reaction products ...... Surfactant with fatty acid trimers, minimum number average mo- lecular weight (in amu), 1,200 (CAS Reg. No. 1173189–09–7). Hydroxyethylpiperidine, ethoxylated, propoxylated, reac- ...... Surfactant tion products with fatty acid dimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173189–22–4). Hydroxyethylpiperidine, ethoxylated, propoxylated, reac- ...... Surfactant tion products with fatty acid trimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173189–28–0). Hydroxyethylpiperidine, ethoxylated, reaction products ...... Surfactant with fatty acid dimers, minimum number average mo- lecular weight (in amu), 1,200 (CAS Reg. No. 1173189–20–2). Hydroxyethylpiperidine, ethoxylated, reaction products ...... Surfactant with fatty acid trimers, minimum number average mo- lecular weight (in amu), 1,200 (CAS Reg. No. 1173189–25–7). 2-(2′-Hydroxy-5′-methylphenyl)benzotriazole (CAS Reg. Not more than 0.5% by weight of Ultraviolet light absorber/sta- No. 2440–22–4). pesticide formulation. bilizer in animal tag and similar slow-release devices Iron oxide (CAS Reg. No. 1309–37–1) ...... Colorant in pesticide formulations for animal tags Isobutane (CAS Reg. No. 75–28–5) ...... None ...... Propellant Isopropyl myristate, CAS Reg. No. 110–27–0 ...... Solvent Kaolinite-type clay ...... Solid diluent, carrier Kerosene, U.S.P. reagent ...... Solvent, cosolvent Lactic acid ...... Solvent Lactic acid, 2-ethylhexyl ester (CAS Reg. No. 6283–86– ...... Solvent 9). Lactic acid, 2-ethylhexyl ester, (2S)- (CAS Reg. No...... Solvent 186817–80–1). Lactic acid, n-propyl ester, (S); (CAS Reg. No. 53651– ...... Solvent 69–7). Lignin (CAS Reg. No. 9005–53–2) ...... Surfactant, related adjuvants of surfactants Lignin, alkali (CAS Reg. No. 8068–05–1) ...... Do. Lignin, alkali, oxidized, sodium salt (CAS Reg. No...... Do. 68201–23–0). Lignin alkali reaction products with disodium sulfite and ...... Do. formaldehyde (CAS Reg. No. 105859–97–0). Lignin alkali reaction products with formaldehyde and so- ...... Do. dium bisulfite (CAS Reg. No. 68512–35–6). Lignosulfonic acid (CAS Reg. No. 8062–15–5) ...... Do. Lignosulfonic acid, ammonium calcium salt (CAS Reg...... Do. No. 12710–04–2). Lignosulfonic acid, ammonium magnesium salt (CAS ...... Do. Reg. No. 123175–37–1). Lignosulfonic acid, ammonium salt (CAS Reg. No. 8061– ...... Do. 53–8). Lignosulfonic acid, ammonium sodium salt (CAS Reg...... Do. No. 166798–73–8). Lignosulfonic acid, calcium magnesium salt (CAS Reg...... Do. No. 55598–86–2). Lignosulfonic acid, calcium salt (CAS Reg. No. 8061–52– ...... Do. 7). Lignosulfonic acid, calcium sodium salt (CAS Reg. No...... Do. 37325–33–0). Lignosulfonic acid, ethoxylated, sodium salt (CAS Reg...... Do. No. 68611–14–3). Lignosulfonic acid, magnesium salt (CAS Reg. No...... Do. 8061–54–9). Lignosulfonic acid, potassium salt (CAS Reg. No. 37314– ...... Do. 65–1). Lignosulfonic acid, sodium salt (CAS Reg. No. 8061–51– ...... Do. 6). Lignosulfonic acid, sodium salt, oxidized (CAS Reg. No...... Do. 68855–41–4). Lignosulfonic acid, sodium salt, polymer with formalde- ...... Do. hyde and phenol (CAS Reg. No. 37207–89–9). Lignosulfonic acid, sodium salt, sulfomethylated (CAS ...... Do. Reg. No. 68512–34–5).

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Inert ingredients Limits Uses

Lignosulfonic acid, zinc salt (CAS Reg. No. 57866–49–6) ...... Do. d-Limonene (CAS Reg. No. 5989–27–5) ...... Solvent, fragrance Magnesium carbonate ...... Solid diluent, carrier Magnesium silicate, hydrated magnesium silicate ...... Do. Methyl alcohol ...... Solvent, cosolvent Methyl n-amyl ketone (CAS Reg. No. 110–43–0) ...... Solvent, cosolvent Methyl esters of higher fatty acids conforming to 21 CFR ...... Antidusting agent 573.640. Methyl-p-hydroxybenzoate (Methyl paraben)...... Meets specifications of Food Preservative Chemicals Codex; not to ex- ceed 0.1% in formulations. Methyl isobutyl ketone ...... Solvent, cosolvent 2-methyl-2,4-pentanediol (CAS Reg. No.–107–41–5) ...... Without limitation ...... Growing crops and food animals 2-methyl-1,3-propanediol (CAS Reg. No. 2163–42–0) ...... Solvent, surfactant Mineral oil, U.S.P., or conforming to 21 CFR 172.878 or ...... Solvent, diluent 178.3620(a), (b). Montmorillonite-type clay ...... Solid diluent, carrier Nonyl, decyl, and undecyl glycoside mixture with a mix- ...... Surfactant ture of nonyl, decyl, and undecyl oligosaccharides and related reaction products (primarily decanol and undecanol) produced as an aqueous-based liquid (50 to 65% solids) from the reaction of primary alcohols (containing 15 to 20% secondary alcohol isomers) in a ratio of 20% C9, 40% C10, and 40% C11 with carbo- hydrates (average glucose to alkyl chain ratio 1.3 to 1.8). a-(p-Nonylphenol)-w-hydroxypoly(oxyethylene) mixture of Not to exceed 7% of pesticide Surfactants, related adjuvants of dihydrogen phosphate and monohydrogen phosphate formulation. surfactants esters and the corresponding ammonium, calcium, magnesium, potassium, sodium, and zinc salts of the phosphate esters; the nonyl group is a propylene trimer isomer and the poly(oxyethylene) content aver- ages 4–14 or 30 moles (CAS Reg. Nos. 51811–79–1, 59139–23–0, 67922–57–0, 68412–53–3, 68553–97–9, 68954–84–7, 99821–14–4, 152143–22–1, 51609–41– 7, 37340–60–6, 106151–63–7, 68584–47–4, 52503– 15–8, 68458–49–1). a-(p-Nonylphenol)-w-hydroxypoly(oxyethylene) sulfate, Not to exceed 7% of pesticide Surfactants, related adjuvants of ammonium, calcium, magnesium, potassium, sodium, formulation. surfactants and zinc salts the nonyl group is propylene trimer iso- mer and the poly(oxyethylene) content averages 4 moles (CAS Reg. Nos. 9014–90–8, 9051–57–4, 9081– 17–8, 68649–55–8, 68891–33–8. a-(p-Nonylphenyl)-w-hydroxypoly(oxyethylene) produced ...... Surfactants, emulsifier, related by the condensation of 1 mole of nonylphenol (nonyl adjuvants of surfactants. group is a propylene trimer isomer) with an average of 4-15 or 30-90 moles of ethylene oxide; if a blend of products is used, the average number of moles of ethylene oxide reacted to produce any product that is a component of the blend shall be in the range of 4-15 or 30-90 moles. Octadecyl 3,5-di-tert-butyl-4-hydroxyhydro cinnamate Not more than 0.5% by weight of Thermal stabilizer/antioxidant in (CAS Reg. No. 2082–79–3). pesticide formulation. animal tag and similar slow-re- lease devices 1-Octanal (CAS Reg. No. 124–13–0) ...... Not more than 0.2% of the pes- Odor masking agent ticide formulation. Octyl and decyl glucosides mixture with a mixture of octyl ...... Thermal stabilizer/antioxidant in and decyl oligosaccharides and related reaction prod- animal tag and similar slow-re- ucts (primarily n-decanol) produced as an aqueous- lease devices based liquid (68-72% solids) from the reaction of straight chain alcohols (C8(45%), C10) with anhydrous glucose. Octyl epoxytallate (CAS Reg. No. 61788–72–5) ...... Plasticizer, component animal tag Oleic acid, conforming to 21 CFR 172.862 (CAS Reg...... Defoaming agent No. 112–80–1). a-Oleoyl-w-hydroxypoly(oxyethylene), average molecular ...... Emulsifier weight (in amu) of 600. a-Oleoyl-w-(oleyloxy)poly(oxyethylene) derived from a- ...... Emulsifier, defoaming agent hydro-w-hydroxypoly(oxyethylene), molecular weight (in amu) 600. Petroleum hydrocarbons, light, odorless, conforming to ...... Solvent, diluent 21 CFR 172.884 or 178.3650.

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Inert ingredients Limits Uses

Petroleum hydrocarbons, synthetic isoparaffinic, con- ...... Do. forming to 21 CFR 172.882 or 178.3530. Phenol ...... Solvent, cosolvent a-Pinene ...... Not more than 2% of formulation Stabilizer by weight. Polyethylene (CAS Reg. No. 9002–88–4) conforming to ...... Component of plastic slow re- 21 CFR 172.615. lease tag Polyethylene glycol [a-hydro-w- ...... Surfactants, related adjuvants of hydroxypoly(oxyethylene)]; mean molecular weight (in surfactants amu) 194 to 9,500 conforms to 21 CFR 178.3750. Potassium benzoate (Cas No. 582–25–2) ...... None ...... Preservative Potassium hydroxide ...... Meeting Food Chemicals, Codex Neutralizer specifications. Propane ...... Propellant 1,2,3-Propanetriol, homopolymer diisooctadecanoate ...... Emulsifier (CAS Reg. No. 63705–03–3). n-Propanol ...... Solvent, for blended emulsifiers 2-Propenoic acid, 2-methyl-, polymer with ethyl 2- ...... Encapsulating agent,dispensers, propenoate and methyl 2-methyl-2-propenoate, ammo- resins, fibers and beads nium salt (CAS Registration No. 55989–05–4), min- imum number average molecular weight (in amu), 18,900.. Propylene glycol ...... Solvent, cosolvent Propylene glycol monomethyl ether ...... Deactivator, emmolient Propyl gallate ...... Antioxidant Propyl p-hydroxybenzoate (Propyl paraben)...... Meets specifications of Food Preservative Chemicals Codex; not to ex- ceed 0.1% in formulations. Pyrophylite ...... Solid diluent, carrier Silica, hydrated silica ...... Anticaking agent, solid diluent, carrier Silica aerogel (finely powdered microcellular silica foam ...... Component of antifoaming agent having a minimum silica content of 89.5%). Soapstone ...... Solid diluent Sodium alkyl naphthalenesulfonates (CAS Reg. Nos. Limited to no more than 30% by Surfactants, related adjuvants of 68909–83–1, 68909–84–2, 68909–82–0, 27213–90–7, weight in pesticide end-use surfactants 26264–58–4, 27178–87–6, 111163–74–7, 908356–16– products. 1, 25417–20–3, 25638–17–9, 145578–88–7, 1322–93– 6, 1323–19–9, 7403–47–6, 68442–09–1, 127646–44– 0, 908356–18–3). Sodium 1,4-dihexyl sulfosuccinate (CAS Reg. No. 3006– ...... Surfactants, related adjuvants of 15–3). surfactants Sodium 1,4-diisobutyl sulfosuccinate (CAS Reg. No...... Surfactants, related adjuvants of 127–39–9). surfactants Sodium dioctylsulfosuccinate ...... Surfactants, related adjuvants of surfactants Sodium 1,4-dipentyl sulfosuccinate (CAS Reg. No. 922– ...... Surfactants, related adjuvants of 80–5). surfactants Sodium hydroxide ...... Neutralizer Sodium monoalkyl and dialkyl (C6-C16) phenoxy Not to exceed 20% in pesticide Surfactants, related adjuvants of benzenedisulfonates and related acids (CAS Reg. Nos. formulations. surfactants 147732–59–0, 147732–60–3, 169662–22–0, 70191– 75–2, 36445–71–3, 39354–74–0, 70146–13–3, 119345–03–8, 149119–20–0, 149119–19–7, 119345– 04–9, 28519–02–0, 25167–32–2, 30260–73–2, 65143– 89–7, 70191–76–3). Sodium N-oleoyl-N-methyl taurine (CAS Reg. No. 137– ...... Surfactants, related adjuvants of 20–2). surfactants Sodium and potassium salts of N-alkyl (C8–C18)-beta- Concentration in formulated end- Surfactants, related adjuvants of iminodipropionic acid where the C8–C18 is linear and use products not to exceed surfactants may be saturated and/or unsaturated (CAS Reg. Nos. 30% by weight in pesticide for- 110676–19–2, 3655–00–3, 61791–56–8, 14960–06–6, mulations. 26256–79–1, 90170–43–7, 91696–17–2, 97862–48–1). Sodium starch glycolate (CAS Reg. No. 9063–38–1) ...... Granular and tableted products Disintegrant only; not to exceed 8% of the formulated product. Sodium sulfate ...... Solid diluent, carrier Sorbitan fatty acid esters (fatty acids limited to C12, C14, ...... Buffering agent; corrosion inhibi- C16, and C18 containing minor amounts of associated tion fatty acids) and poly(oxyethylene) derivatives of sorbi- tan fatty acid esters; the poly(oxyethylene) content averages 16-20 moles. Sorbitol ...... Antidusting agent. Stearic acid (CAS Reg. No. 57–11–4) ...... Lubricant, component animal tag

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Inert ingredients Limits Uses

a-Stearoyl-w-hydroxypoly(oxyethylene), average molec- ...... Emulsifier ular weight (in amu) of 600. a-Stearoyl-w-hydroxypoly(oxyethylene); the ...... Surfactants; related adjuvants of poly(oxyethylene) content averages 8, 9, or 40 moles; surfactants if a blend of products is used, the average number of moles of ethylene oxide reacted to produce any prod- uct that is a component of the blend shall be 8, 9, or 40. Sulfite liquors and cooking liquors, spent, oxidized (CAS ...... Surfactant, related adjuvants of Reg. No. 68514–09–0). surfactants Sulfur (CAS Reg. No. 7704–34–9) ...... Stabilizer Talc ...... Do. Tall oil; fatty acids not less than 58%, rosin acids not ...... Surfactants, related adjuvants of more than 44%, unsaponifiables not more than 8%. surfactants Tartrazine ...... Dye, coloring agent N,N,N′,N″,-tetrakis-(2-hydroxypropyl) ethylenediamine Concentration in formulated end- Stabilizer for formulation. (CAS Reg. No. 102–60–3). use products not to exceed 20% by weight in pesticide for- mulations. 2,4,7,9-Tetramethyl-5-decyne-4.7-diol ...... Not more than 2.5% of pesticide Surfactants, related adjuvants of formulation. surfactants Titanium dioxide (CAS Reg. No. 13463–67–7) ...... Pigment/colorant in pesticide for- mulations for animal tag Toluenesulfonic acid and its ammonium, calcium, magne- ...... Do. sium, potassium, sodium, and zinc salts. Triacetin (glyceryl triacetate) ...... Solvent, cosolvent Trisodium phosphate ...... Precipitant, buffer, filler Xylene ...... Solvent, cosolvent Xylenesulfonic acid and its ammonium, calcium, magne- ...... Surfactants, related adjuvants of sium, potassium, sodium, and zinc salts. surfactants Zinc oxide ...... Solid diluent, carrier Zinc stearate, conforming to 21 CFR 182.5994 and ...... Water repellant, dessicant, and 582.5994. coating agent. Zinc stearate (CAS Reg. No. 557–05–1) ...... Water repellant, desiccant, and coating agent; stabilizer, com- ponent of plastic animal tag Zinc sulfate (basic and monohydrate) ...... Water repellant, dessicant, and coating agent

[69 FR 23130, Apr. 28, 2004]

EDITORIAL NOTE: For FEDERAL REGISTER citations affecting § 180.930, see the List of CFR Sections Affected, which appears in the Finding Aids section of the printed volume and at www.fdsys.gov.

§ 180.940 Tolerance exemptions for ac- semi-permanent or permanent food- tive and inert ingredients for use in contact surface (other than being ap- antimicrobial formulations (Food- plied on food packaging) with adequate contact surface sanitizing solu- draining before contact with food. tions). (a) The following chemical sub- Residues of the following chemical stances when used as ingredients in an substances are exempted from the re- antimicrobial pesticide formulation quirement of a tolerance when used in may be applied to: Food-contact sur- accordance with good manufacturing faces in public eating places, dairy- practice as ingredients in an anti- processing equipment, and food-proc- microbial pesticide formulation, pro- essing equipment and utensils. vided that the substance is applied on a

Pesticide Chemical CAS Reg. No. Limits

Acetic acid ...... 64–19–7 ...... When ready for use, the end-use con- centration is not to exceed 100 ppm Allyl cylcohexylpropionate ...... 2705–87–5 ...... When ready for use, the end-use con- centration is not to exceed 100 ppm

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Pesticide Chemical CAS Reg. No. Limits

a-alkyl-w-hydroxypoly (oxypropylene) and/ 9002–92–0; 9004–95–9; 9004–98–2; or poly (oxyethylene) polymers where the 9005–00–9; 9035–85–2; 9038–29– alkyl chain contains a minimum of six 3; 9038–43–1; 9040–05–5; 9043– carbons. 30–5; 9087–53–0; 25190–05–0; 24938–91–8; 25231–21–4; 26183– 52–8; 26468–86–0; 26636–39–5; 27252–75–1; 27306–79–2; 31726– 34–8; 34398–01–1; 34398–05–5; 37251–67–5; 37311–00–5; 37311– 01–6; 37311–02–7; 37311–04–9; 39587–22–9; 50861–66–0; 52232– 09–4; 52292–17–8; 52609–19–5; 57679–21–7; 59112–62–8; 60828– 78–6; 61702–78–1; 61725–89–1; 61791–13–7; 61791–20–6; 61791– 28–4; 61804–34–0; 61827–42–7; 61827–84–7; 62648–50–4; 63303– 01–5; 63658–45–7; 63793–60–2; 64366–70–7; 64415–24–3; 64415– 25–4; 64425–86–1; 65104–72–5; 65150–81–4; 66455–14–9: 66455– 15–0; 67254–71–1; 67763–08–0; 68002–96–0; 68002–97–1; 68131– 39–5; 68131–40–8; 68154–96–1; 68154–97–2; 68154–98–3; 68155– 01–1; 68213–23–0; 68213–24–1; 68238–81–3; 68238–82–4; 68409– 58–5; 68409–59–6; 68439–30–5; 68439–45–2; 68439–46–3; 68439– 48–5; 68439–49–6; 68439–50–9; 68439–51–0; 68439–53–2; 68439– 54–3; 68458–88–8; 68526–94–3; 68526–95–4; 68551–12–2; 68551– 13–3; 68551–14–4; 68603–20–3; 68603–25–8; 68920–66–1; 68920– 69–4; 68937–66–6; 68951–67–7; 68954–94–9; 68987–81–5; 68991– 48–0; 69011–36–5; 69013–18–9; 69013–19–0; 69227–20–9; 69227– 21–0; 69227–22–1; 69364–63–2; 70750–27–5; 70879–83–3; 70955– 07–6; 71011–10–4; 71060–57–6; 71243–46–4; 72066–65–0; 72108– 90–8; 72484–69–6; 72854–13–8; 72905–87–4; 73018–31–2; 73049– 34–0; 74432–13–6; 74499–34–6; 78330–19–5; 78330–20–8; 78330– 21–9; 78330–23–1; 79771–03–2; 84133–50–6; 85422–93–1; 97043– 91–9; 97953–22–5; 102782–43–4; 103331–86–8; 103657–84–7; 103657–85–8; 103818–93–5; 103819–03–0; 106232–83–1; 111905–54–5; 116810–31–2; 116810–32–3; 116810–33–4; 120313–48–6; 120944–68–5; 121617–09–2; 126646–02–4; 126950–62–7; 127036–24–2; 139626–71–4; 152231–44–2; 154518–36–2; 157627–86–6; 157627–88–8; 157707–41–0; 157707–43–2; 159653–49–3; 160875–66–1; 160901–20–2; 160901–09–7; 160901–19–9; 161025–21–4; 161025–22–5; 166736–08–9; 169107–21–5; 172588–43–1; 176022–76–7; 196823–11–7; 287935–46–0; 288260–45–7; 303176–75–2; 954108–36–2. Aluminum sulfate 10043–01–3 ...... When ready for use, the end-use con- centration is not to exceed 50 ppm

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Pesticide Chemical CAS Reg. No. Limits

Ammonium chloride 12125–02–9 When ready for use, the end-use con- centration is not to exceed 48 ppm Amylopectin, acid-hydrolyzed, 1- 113894–85–2 None oxtenylbutanedioate Amylopectin, hydrogen 1- 125109–81–1 None octadecenylbutanedioate Butryic acid ...... 107–92–6 ...... When ready for use, the end-use con- centration is not to exceed 100 ppm Butyl alcohol ...... 71–36–3 ...... When ready for use, the end-use con- centration is not to exceed 100 ppm n-Butyl benzoate...... 136–60–7 ...... When ready for use, the end-use con- centration is not to exceed 15,000 ppm Citral ...... 5392–40–5 ...... When ready for use, the end-use con- centration is not to exceed 100 ppm Citronellol ...... 106–22–9 ...... When ready for use, the end-use con- centration is not to exceed 100 ppm Citronellyl acetate ...... 150–84–5 ...... When ready for use, the end-use con- centration is not to exceed 100 ppm Copper sulfate pentahydrate 7758–99–8 When ready for use, the end-use con- centration is not to exceed 80 ppm b-Damascone, (Z)- ...... 23726–92–3 ...... When ready for use, the end-use con- centration is not to exceed 100 ppm Decanal ...... 112–31–2 ...... When ready for use, the end-use con- centration is not to exceed 100 ppm Decanoic acid ...... 334–48–5 ...... When ready for use, the end-use con- centration is not to exceed 100 ppm 1-Decanol ...... 112–30–1 ...... When ready for use, the end-use con- centration is not to exceed 100 ppm (E)-4-Decenal ...... 65405–70–1 ...... When ready for use, the end-use con- centration is not to exceed 100 ppm D-Glucopyranose, oligomeric, decyl octyl 68515–73–1 None glycosides 2,6-Dimethyl-5-heptanal ...... 106–72–9 ...... When ready for use, the end-use con- centration is not to exceed 100 ppm Di-n-butyl carbonate 542–52–9 ...... When ready for use, the end-use con- centration is not to exceed 15,000 ppm 2-Dodecanol, (2E)- ...... 20407–84–5 ...... When ready for use, the end-use con- centration is not to exceed 100 ppm Ethanol 64–17–5 None Ethyl 2-methylbutyrate ...... 452–79–1 ...... When ready for use, the end-use con- centration is not to exceed 100 ppm Ethylenediaminetetraacetic acid (EDTA), 64–02–8 None tetrasodium salt FD&C Green No. 3 CAS Reg. No. 2353–45–9 None FD&C Red No. 40 25956–17–6 ...... When ready for use, the end-use con- centration is not to exceed 20 ppm. FD&C Yellow No. 5 1934–21–0 When ready for use, the end-use con- centration is not to exceed 1000 ppm (E)-Geraniol ...... 106–24–1 ...... When ready for use, the end-use con- centration is not to exceed 100 ppm (E)-Geraniol acetate ...... 105–87–3 ...... When ready for use, the end-use con- centration is not to exceed 100 ppm Heptanal ...... 111–71–7 ...... When ready for use, the end-use con- centration is not to exceed 100 ppm Heptanoic acid ...... 111–14–8 ...... When ready for use, the end-use con- centration is not to exceed 100 ppm Heptyl alcohol ...... 111–70–6 ...... When ready for use, the end-use con- centration is not to exceed 100 ppm Hexanal ...... 66–25–1 ...... When ready for use, the end-use con- centration is not to exceed 100 ppm Hexanoic acid ...... 142–62–1 ...... When ready for use, the end-use con- centration is not to exceed 100 ppm n-Hexanol ...... 111–27–3 ...... When ready for use, the end-use con- centration is not to exceed 100 ppm (Z)-3-Hexenol ...... 928–96–1 ...... When ready for use, the end-use con- centration is not to exceed 100 ppm (Z)-3-Hexenol acetate...... 3681–71–8 ...... When ready for use, the end-use con- centration is not to exceed 100 ppm Hexyl acetate ...... 142–92–7 ...... When ready for use, the end-use con- centration is not to exceed 100 ppm Hydrogen peroxide 7722–84–1 When ready for use, the end-use con- centration is not to exceed 91 ppm

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Pesticide Chemical CAS Reg. No. Limits

Hypochlorous acid, sodium salt 7681–52–9 When ready for use, the end-use con- centration of all hypochlorous acid chemicals in the solution is not to ex- ceed 200 ppm determined as total available chlorine Iodine 7553–56–2 When ready for use, the total end-use concentration of all iodide-producing chemicals in the solution is not to ex- ceed 25 ppm of titratable iodine Lauric acid ...... 143–07–7 ...... When ready for use, the end-use con- centration is not to exceed 100 ppm Lauric aldehyde ...... 112–54–9 ...... When ready for use, the end-use con- centration is not to exceed 100 ppm Lauryl alcohol ...... 112–53–8 ...... When ready for use, the end-use con- centration is not to exceed 100 ppm d-Limonene ...... 5989–27–5 ...... When ready for use, the end-use con- centration is not to exceed 100 ppm Lipase, triacylglycerol 9001–62–1 When ready for use, the end-use con- centration is not to exceed 500 ppm Magnesium oxide 1309–48–4 None Methylene blue 61–73–4 When ready for use, the end-use con- centration is not to exceed 0.4 ppm Methyl-a-ionone ...... 127–42–4 ...... When ready for use, the end-use con- centration is not to exceed 100 ppm 3-Methyl-2-butenyl acetate ...... 1191–16–8 ...... When ready for use, the end-use con- centration is not to exceed 100 ppm 2-Methylundecanal ...... 110–41–8 ...... When ready for use, the end-use con- centration is not to exceed 100 ppm 2-Methyl-1,3-propanediol 2163–42–0 None Myristaldehyde ...... 124–25–4 ...... When ready for use, the end-use con- centration is not to exceed 100 ppm Myristic acid ...... 544–63–8 ...... When ready for use, the end-use con- centration is not to exceed 100 ppm Neryl acetate ...... 141–12–8 ...... When ready for use, the end-use con- centration is not to exceed 100 ppm Nitric acid 7697–37–2 When ready for use, the end-use con- centration is not to exceed 1,000 ppm Nonanal ...... 124–19–6 ...... When ready for use, the end-use con- centration is not to exceed 100 ppm Nonanoic acid ...... 112–05–0 ...... When ready for use, the end-use con- centration is not to exceed 100 ppm Nonyl alcohol ...... 143–08–8 ...... When ready for use, the end-use con- centration is not to exceed 100 ppm a-(p-Nonylphenyl)-w-hydroxypoly (oxy- None None ethylene) average poly(oxyethylene) con- tent 11 moles) Octadecanoic acid, calcium salt 1592–23–0 None 9-Octadecenoic acid (9Z)-, sulfonated, 1315321–93–7 ...... When ready for use, the end-use con- oxidized centration is not to exceed 250 ppm. 9-Octadecenoic acid (9Z)-, sulfonated, 1315321–94–8 ...... When ready for use, the end-use con- oxidized, potassium salts centration is not to exceed 250 ppm. 9-Octadecenoic acid (9Z)-, sulfonated, 1315321–95–9 ...... When ready for use, the end-use con- oxidized, sodium salts centration is not to exceed 250 ppm. Octanal ...... 124–13–0 ...... When ready for use, the end-use con- centration is not to exceed 100 ppm 1-Octanesulfonic acid, sodium salt 5324–84–5 When ready for use, the end-use con- centration is not to exceed 46 ppm Octanoic acid 124–07–2 When ready for use, the end-use con- centration is not to exceed 52 ppm Octanoic acid ...... 124–07–2 ...... When ready for use, the end-use con- centration is not to exceed 100 ppm 1-Octanol ...... 111–87–5 ...... When ready for use, the end-use con- centration is not to exceed 100 ppm Oxirane, methyl-, polymer with oxirane, 9003–11–6 None minimum molecular weight (in amu), 1900 Palmitic acid ...... 57–10–3 ...... When ready for use, the end-use con- centration is not to exceed 100 ppm Peroxyacetic acid 79–21–0 When ready for use, the end-use con- centration is not to exceed 58 ppm Peroxyoctanoic acid 33734–57–5 When ready for use, the end-use con- centration is not to exceed 52 ppm Phosphonic acid, (1-hydroxyethylidene)bis- 2809–21–4 When ready for use, the end-use con- centration is not to exceed 14 ppm

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Pesticide Chemical CAS Reg. No. Limits

Phosphoric acid, trisodium salt 7601–54–9 When ready for use, the end-use con- centration is not to exceed 5916 ppm Potassium bromide 7758–02–3 When ready for use, the end-use con- centration is not to exceed 46 ppm total available halogen Potassium iodide 7681–11–0 When ready for use, the total end-use concentration of all iodide-producing chemicals in the solution is not to ex- ceed 25 ppm of titratable iodine 1,3-Propanediol 504–63–2 None Propionic acid ...... 79–09–4 ...... When ready for use, the end-use con- centration is not to exceed 100 ppm Propylene glycol 57–55–6 None Quaternary ammonium compounds, alkyl 8001–54–5 When ready for use, the end-use con- (C12-C18) benzyldimethyl, chlorides centration of all quaternary chemicals in the solution is not to exceed 200 ppm of active quaternary compound Quaternary ammonium compounds: n-alkyl 68424–85–1 When ready for use, the end-use con- (C12-18) dimethyl benzyl ammonium chlo- centration of all quaternary chemicals in ride solution is not to exceed 400 ppm of active quaternary compound Quaternary Ammonium Compounds: n- 85409–23–0 When ready for use, the end-use con- alkyl (C 12-14) dimethyl ethylbenzyl am- centration of all quaternary chemicals in monium chloride, average molecular solution is not to exceed 400 ppm of weight (in amu), 377 to 384 active quaternary compound. Quaternary ammonium compounds n-alkyl None When ready for use, the end-use con- (C12-C18) dimethyl ethylbenzyl ammo- centration of all quaternary chemicals in nium chloride average molecular weight the solution is not to exceed 200 ppm (in amu) 384 of active quaternary compound Quaternary ammonium compounds, Di-n- None When ready for use, the end-use con- Alkyl (C8-10) dimethyl ammonium chlo- centration of these specific in quater- ride, average molecular weight (in amu) nary ammonium compounds is not to 332 to 361 exceed 240 ppm of active quaternary ammonium compound; the end-use concentration of all quaternary chemi- cals in the solution is not to exceed 400 ppm of active quaternary compound Quaternary ammonium compounds, didecyl 148788–55–0/148812–654–1 When ready for use, the end-use con- dimethyl ammonium carbonate/didecyl centration of these specific ammonium dimethyl ammonium bicarbonate compounds is not to exceed 400 ppm of active quaternary ammonium com- pound Silver ions resulting from the use of elec- 14701–21–4 When ready for use, the end-use con- trolytically-generated silver ions stabilized centration of silver ions is not to exceed in citric acid as silver dihydrogen citrate 50 ppm of active silver (does not include metallic silver) Sodium bisulfate 7681–38–1 When ready for use, the end-use con- centration is not to exceed 2,000 ppm. Sorbitan, mono-9-octadecenoate, poly(oxy- 9005–65–6 None 1,2-ethanediyl) derivs., (Z)- Stearic acid...... 57–11–4 ...... When ready for use, the end-use con- centration is not to exceed 100 ppm Sulfuric acid ...... 7664–93–9 ...... Food-contact surfaces in public eating places, dairy-processing equipment, and food-processing equipment and utensils in antimicrobial formulations. Not to exceed 600 ppm. Sulfuric acid monododecyl ester, sodium 151–21–3 When ready for use, the end-use con- salt (sodium lauryl sulfate) centration is not to exceed 350 ppm 1,3,5-Triazine-2,4,6(1H,3H,5H)-trione, 1,3- 2893–78–9 When ready for use, the end-use con- dichloro-, sodium salt centration of all di- or trichloroisocyanuric acid chemicals in the solution is not to exceed 100 ppm determined as total available chlorine 2-Tridecanal ...... 7774–82–5 ...... When ready for use, the end-use con- centration is not to exceed 100 ppm 3,5,5-Trimethylhexanal ...... 5435–64–3 ...... When ready for use, the end-use con- centration is not to exceed 100 ppm Undecanal ...... 112–44–7 ...... When ready for use, the end-use con- centration is not to exceed 100 ppm Undecyl alcohol ...... 112–42–5 ...... When ready for use, the end-use con- centration is not to exceed 100 ppm Valeraldehyde ...... 110–62–3 ...... When ready for use, the end-use con- centration is not to exceed 100 ppm

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Pesticide Chemical CAS Reg. No. Limits

Valeric acid ...... 109–52–4 ...... When ready for use, the end-use con- centration is not to exceed 100 ppm Xylenesulfonic acid, sodium salt 1300–72–7 When ready for use, the end-use con- centration is not to exceed 500 ppm

(b) The following chemical sub- may be applied to: Dairy processing stances when used as ingredients in an equipment, and food-processing equip- antimicrobial pesticide formulation ment and utensils.

Pesticide Chemical CAS Reg. No. Limits

Acetic acid 64–19–7 When ready for use, the end-use concentration is not to exceed 686 ppm Acetic acid, chloro-, sodium salt, reaction prod- 68608–66–2 When ready for use, the end-use concentration ucts with 4,5-dihydro-2-undecyl-1H-imidazole- is not to exceed 42 ppm chloroacetic acid 1-ethanol and sodium hydroxide Benzenesulfonic acid, dodecyl- 27176–87–0 When ready for use, the end-use concentration is not to exceed 5.5 ppm Butanedioic acid, octenyl- 28805–58–5 When ready for use, the end-use concentration is not to exceed 156 ppm Butoxy monoether of mixed (ethylene-propylene) None None polyalkylene glycol, minimum average molec- ular weight (in amu), 2400 Calcium chloride 10043–52–4 When ready for use, the end-use concentration is not to exceed 17 ppm

n-Carboxylic acids (C6-C12), consisting of a mix- None When ready for use, the end-use concentration ture of not less than 56% octanoic acid and is not to exceed 39 ppm not less than 40% decanoic acid Decanoic acid 334–48–5 When ready for use, the end-use concentration is not to exceed 90 ppm Ethanesulfonic acid, 2-[cyclohexyl (1- 132–43–4 When ready for use, the end-use concentration oxohexadecyl) amino]-, sodium salt is not to exceed 237 ppm Ethylenediaminetetraacetic acid (EDTA), diso- 139–33–3 When ready for use, the end-use concentration dium salt is not to exceed 1400 ppm FD&C Yellow No. 5 (Tartrazine) (conforming to 1934–21–0 None 21 CFR 74.705) D-Gluconic acid, monosodium salt 527–07–1 When ready for use, the end-use concentration is not to exceed 760 ppm Hydriodic acid 10034–85–2 When ready for use, the total end-use con- centration of all iodide-producing chemicals is not to exceed 25 ppm of titratable iodine Hydrogen peroxide 7722–84–1 When ready for use, the end-use concentration is not to exceed 465 ppm Hypochlorous acid 7790–92–3 When ready for use, the end-use concentration of all hypochlorous acid chemicals in the so- lution is not to exceed 200 ppm determined as total available chlorine Iodine 7553–56–2 When ready for use, the total end-use con- centration of all iodide-producing chemicals in the solution is not to exceed 25 ppm of ti- tratable iodine Lactic acid 50–21–5 When ready for use, the end-use concentration is not to exceed 138 ppm Nonanoic acid 112–05–0 When ready for use, the end-use concentration is not to exceed 90 ppm 1-Octanamine, N,N-dimethyl- 7378–99–6 When ready for use, the end-use concentration is not to exceed 113 ppm 1,2-Octanedisulfonic acid 113669–58–2 When ready for use, the end-use concentration is not to exceed 102 ppm 1-Octanesulfonic acid 3944–72–7 When ready for use, the end-use concentration is not to exceed 172 ppm 1-Octanesulfonic acid, sodium salt 5324–84–5 When ready for use, the end-use concentration is not to exceed 297 ppm 1-Octanesulfonic acid, 2-sulfino- 113652–56–5 When ready for use, the end-use concentration is not to exceed 102 ppm Octanoic acid 124–07–2 When ready for use, the end-use concentration is not to exceed 176 ppm

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Pesticide Chemical CAS Reg. No. Limits

Oxychloro species (including chlorine dioxide) None When ready for use, the end-use concentration generated by acidification of an aqueous solu- is not to exceed 200 ppm of chlorine dioxide tion of sodium chlorite as determined by the method titled, Iodometric Method for the Determination of Available Chlorine Dioxide (50-250 ppm available chlorine dioxide) Peroxyacetic acid 79–21–0 When ready for use, the end-use concentration is not to exceed 315 ppm Peroxyoctanoic acid 33734–57–5 When ready for use, the end-use concentration is not to exceed 122 ppm Phosphonic acid, (1-hydroxyethylidene)bis- 2809–21–4 When ready for use, the end-use concentration is not to exceed 34 ppm Phosphoric acid 7664–38–2 None Phosphoric acid, monosodium salt 7558–80–7 When ready for use, the end-use concentration is not to exceed 350 ppm Potassium iodide 7681–11–0 When ready for use, the total end-use con- centration of all iodide-producing chemicals in the solution is not to exceed 25 ppm of ti- tratable iodine Propanoic acid 79–09–4 When ready for use, the end-use concentration is not to exceed 297 ppm 2,6-Pyridinedicarboxylic acid 499–83–2 When ready for use, the end-use concentration is not to exceed 1.2 ppm Sulfuric acid monododecyl ester, sodium salt 151–21–3 When ready for use, the end-use concentration (sodium lauryl sulfate) is not to exceed 350 ppm

(c) The following chemical sub- may be applied to: Food-processing stances when used as ingredients in an equipment and utensils. antimicrobial pesticide formulation

Pesticide Chemical CAS Reg. No. Limits

Acetic acid 64–19–7 When ready for use, the end-use concentration is not to exceed 686 ppm Acetic acid, chloro-, sodium salt, reaction prod- 68608–66–2 When ready for use, the end-use concentration ucts with 4,5-dihydro-2-undecyl-1H-imidazole- is not to exceed 42 ppm chloroacetic acid 1-ethanol and sodium hydroxide Ammonium chloride 12125–02–9 When ready for use, the end-use concentration is not to exceed 48 ppm Benzenesulfonic acid, dodecyl- 27176–87–0 When ready for use, the end-use concentration is not to exceed 400 ppm Benzenesulfonic acid, dodecyl-, sodium salt 25155–30–0 When ready for use, the end-use concentration is not to exceed 430 ppm [1,1′-Biphenyl]-2-ol 90–43–7 When ready for use, the end-use concentration is not to exceed 400 ppm Boric acid, sodium salt 7775–19–1 None Butanedioic acid, octenyl- 28805–58–5 When ready for use, the end-use concentration is not to exceed 156 ppm Butanedioic acid, sulfo-, 1,4-dioctyl ester, so- 1639–66–3 None dium salt Butoxy monoether of mixed (ethylene-propylene) None None polyalkylene glycol, cloudpoint of 90 - 100oC in 0.5 aqueous solution, average molecular weight (in amu), 3300 Butoxy monoether of mixed (ethylene-propylene) None None polyalkylene glycol, minimum average molec- ular weight (in amu), 2400 Calcium chloride 10043–52–4 When ready for use, the end-use concentration is not to exceed 17 ppm n-Carboxylic acids (C6-C12), consisting of a mix- None When ready for use, the end-use concentration ture of not less than 56% octanoic acid and is not to exceed 39 ppm not less than 40% decanoic acid 3-Cyclohexene-1-methanol,a,a,4-trimethyl- 98–55–5 None 1-Decanaminium, N-decyl-N, N-dimethyl-, chlo- 7173–51–5 When ready for use, the end-use concentration ride is not to exceed 200 ppm of active quater- nary compound Decanoic acid 3347–48–5 When ready for use, the end-use concentration is not to exceed 234 ppm Ethanesulfonic acid, 2-[cyclohexyl (1- 132–43–4 When ready for use, the end-use concentration oxohexadecyl) amino]-, sodium salt is not to exceed 237 ppm Ethanol 64–17–5 None

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Pesticide Chemical CAS Reg. No. Limits

Ethanol, 2 butoxy- 111–76–2 None Ethanol, 2-(2-ethoxyethoxy)- 111–90–0 None Ethylenediaminetetraacetic acid (EDTA), diso- 139–33–3 When ready for use, the end-use concentration dium salt is not to exceed 1400 ppm Ethylenediaminetetraacetic acid (EDTA), 64–02–8 None tetrasodium salt Fatty acids, coco, potassium salts 61789–30–8 None Fatty acids, tall-oil, sulfonated, sodium salts 68309–27–3 When ready for use, the end-use concentration is not to exceed 66 ppm FD&C Yellow No. 5 (Tartrazine) (conforming to 1934–21–0 None 21 CFR 74.705) D-Gluconic acid, monosodium salt 527–07–1 When ready for use, the end-use concentration is not to exceed 760 ppm Hydriodic acid 10034–85–2 When ready for use, the total end-use con- centration of all iodide-producing chemicals in the solution is not to exceed 25 ppm of ti- tratable iodine Hydrogen peroxide 7722–84–1 When ready for use, the end-use concentration is not to exceed 1100 ppm Hypochlorous acid 7790–92–3 When ready for use, the end-use concentration of all hypochlorous acid chemicals in the so- lution is not to exceed 200 ppm determined as total available chlorine Hypochlorous acid, calcium salt 7778–54–3 When ready for use, the end-use concentration of all hypochlorous acid chemicals in the so- lution is not to exceed 200 ppm determined as total available chlorine Hypochlorous acid, lithium salt 13840–33–0 When ready for use, the end-use concentration of all hypochlorous acid chemicals in the so- lution is not to exceed 200 ppm determined as total available chlorine and 30 ppm lithium Hypochlorous acid, potassium salt 7778–66–7 When ready for use, the end-use concentration of all hypochlorous acid chemicals in the so- lution is not to exceed 200 ppm determined as total available chlorine Hypochlorous acid, sodium salt 7681–52–9 When ready for use, the end-use concentration of all hypochlorous acid chemicals in the so- lution is not to exceed 200 ppm determined as total available chlorine Iodine 7553–56–2 When ready for use, the total end-use con- centration of all iodide-producing chemicals in the solution is not to exceed 25 ppm of ti- tratable iodine Lactic acid 50–21–5 None Magnesium oxide 1309–48–4 None Methylene blue 61–73–4 When ready for use, the end-use concentration is not to exceed 0.4 ppm Neodecanoic acid 26896–20–8 When ready for use, the end-use concentration is not to exceed 174 ppm Nonanoic acid 112–05–0 When ready for use, the end-use concentration is not to exceed 90 ppm a-(p-Nonylphenyl)-w-hydroxypoly (oxyethylene) None None maximum average molecular weight (in amu), 748 a-(p-Nonylphenol)-w-hydroxypoly (oxyethylene) None None average poly(oxyethylene) content 11 moles a-(p-Nonylphenyl)-w-hydroxypoly (oxyethylene) None None produced by the condensation of 1 mole p- nonylphenol with 9 to 12 moles ethylene oxide a-(p-Nonylphenyl)-w-hydroxypoly (oxyethylene), None None 9 to 13 moles ethylene oxide Octadecanoic acid, calcium salt 1592–23–0 None 9-Octadecenoic acid (9Z)-, sulfonated 68988–76–1 When ready for use, the end-use concentration is not to exceed 312 ppm 9-Octadecenoic acid (9Z)-sulfonated, sodium 68443–05–0 When ready for use, the end-use concentration salts is not to exceed 200 ppm 1-Octanamine, N,N-dimethyl- 7378–99–6 When ready for use, the end-use concentration is not to exceed 113 ppm 1,2-Octanedisulfonic acid 113669–58–2 When ready for use, the end-use concentration is not to exceed 102 ppm 1-Octanesulfonic acid 3944–72–7 When ready for use, the end-use concentration is not to exceed 172 ppm 1-Octanesulfonic acid, sodium salt 5324–84–5 When ready for use, the end-use concentration is not to exceed 312 ppm

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Pesticide Chemical CAS Reg. No. Limits

1-Octanesulfonic acid, 2-sulfino- 113652–56–5 When ready for use, the end-use concentration is not to exceed 102 ppm Octanoic acid 124–07–2 When ready for use, the end-use concentration is not to exceed 234 ppm Oxirane, methyl-, polymer with oxirane, min- 9003–11–6 None imum molecular weight (in amu), 1900 Oxirane, methyl-, polymer with oxirane, block, 106392–12–5 None average molecular weight (in amu), 1900 Oxirane, methyl-, polymer with oxirane, block, None None minimum average molecular weight (in amu), 2000 Oxirane, methyl-, polymer with oxirane, block, None None 27 to 31 moles of polyoxypropylene, average molecular weight (in amu) 2000 Oxychloro species (predominantly chlorite, chlo- None When ready for use, the end-use concentration rate and chlorine dioxide in an equilibrium is not to exceed 200 ppm of chlorine dioxide mixture) generated either (i) by directly meter- as determined by the method titled, ing a concentrated chlorine dioxide solution ‘‘Iodometric Method for the Determination of prepared just prior to use, into potable water, Available Chlorine Dioxide (50-250 ppm or (ii) by acidification of an aqueous alkaline available chlorine dioxide)’’ solution of oxychloro species (predominately chlorite and chlorate) followed by dilution with potable water Oxychloro species (including chlorine dioxide) None When ready for use, the end-use concentration generated by acidification of an aqueous solu- is not to exceed 200 ppm of chlorine dioxide tion of sodium chlorite as determined by the method titled, ‘‘Iodometric Method for the Determination of Available Chlorine Dioxide (50-250 ppm available chlorine dioxide)’’ 2,4-Pentanediol, 2-methyl- 107–41–5 None Peroxyacetic acid 79–21–0 When ready for use, the end-use concentration is not to exceed 315 ppm Peroxyoctanoic acid 33734–57–5 When ready for use, the end-use concentration is not to exceed 122 ppm Phenol, 4-chloro-2-(phenylmethyl)- 120–32–1 When ready for use, the end-use concentration is not to exceed 320 ppm Phenol, 4-(1,1-dimethylpropyl)- 80–46–6 When ready for use, the end-use concentration is not to exceed 80 ppm Phosphonic acid, (1-hydroxyethylidene)bis- 2809–21–4 When ready for use, the end-use concentration is not to exceed 34 ppm Phosphoric acid 7664–38–2 None Phosphoric acid, monosodium salt 7558–80–7 When ready for use, the end-use concentration is not to exceed 350 ppm Phosphoric acid, trisodium salt 7601–54–9 When ready for use, the end-use concentration is not to exceed 5916 ppm Poly(oxy-1,2-ethanediyl), a-[(1,1,3,3- None None tetramethylbutyl) phenyl]-w-hydroxy-, pro- duced with one mole of the phenol and 4 to 14 moles ethylene oxide Potassium bromide 7758–02–3 When ready for use, the end-use concentration of all bromide-producing chemicals in the so- lution is not to exceed 200 ppm total avail- able halogen Potassium iodide 7681–11–0 When ready for use, the total end-use con- centration of all iodide-producing chemicals in the solution is not to exceed 25 ppm of ti- tratable iodine Propanoic acid 79–09–4 When ready for use, the end-use concentration is not to exceed 297 ppm 2,6-Pyridinedicarboxylic acid 499–83–2 When ready for use, the end-use concentration is not to exceed 1.2 ppm

Quaternary ammonium compounds, alkyl (C12- 8001–54–5 When ready for use, the end-use concentration C18) benzyldimethyl, chlorides of this specific quaternary compound is not to exceed 200 ppm within the end-use total concentration that is not to exceed 400 ppm active quaternary compound

Quaternary ammonium compounds, n-alkyl (C12- None When ready for use, the end-use concentration C14) dimethyl ethylbenzyl ammonium chloride, of this specific quaternary compound is not average molecular weight (in amu), 377 to to exceed 200 ppm within the end-use total 384 concentration that is not to exceed 400 ppm active quaternary compound

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Pesticide Chemical CAS Reg. No. Limits

Quaternary ammonium compounds, n-alkyl (C12- None When ready for use, the end-use concentration C18) dimethyl ethylbenzyl ammonium chloride of this specific quaternary compound is not average molecular weight (in amu) 384 to exceed 200 ppm within the end-use total concentration that is not to exceed 400 ppm active quaternary compound Quaternary ammonium compounds, di-n-Alkyl None When ready for use, the end-use concentration (C8-C10) dimethyl ammonium chloride, aver- of this specific quaternary compound is not age molecular weight (in amu), 332 to 361 to exceed 240 ppm within the end-use total concentration that is not to exceed 400 ppm active quaternary compound Sodium-a-alkyl(C12-C15)-w-hydroxypoly (oxy- None None ethylene) sulfate with the poly(oxyethylene) content averaging one mole Sodium bromide 7647–15–6 When ready for use, the end-use concentration of all bromide-producing chemicals in the so- lution is not to exceed 200 ppm total avail- able halogen Sodium iodide 7681–82–5 When ready for use, the total end-use con- centration of all iodide-producing chemicals in the solution is not to exceed 25 ppm of ti- tratable iodine Sulfuric acid monododecyl ester, sodium salt 151–21–3 None (sodium lauryl sulfate) 1,3,5-Triazine-2,4,6(1H,3H,5H)-trione, 1,3- 2782–57–2 When ready for use, the end-use concentration dichloro- of all di- or trichloroisocyanuric acid chemi- cals in the solution is not to exceed 100 ppm determined as total available chlorine 1,3,5-Triazine-2,4,6(1H,3H,5H)-trione, 1,3- 2244–21–5 When ready for use, the end-use concentration dichloro-, potassium salt of all di- or trichloroisocyanuric acid chemi- cals in the solution is not to exceed 100 ppm determined as total available chlorine 1,3,5-Triazine-2,4,6(1H,3H,5H)-trione, 1,3- 2893–78–9 When ready for use, the end-use concentration dichloro-, sodium salt of all di- or trichloroisocyanuric acid chemi- cals in the solution is not to exceed 100 ppm determined as total available chlorine 1,3,5-Triazine-2,4,6(1H,3H,5H)-trione, 1,3,5- 87–90–1 When ready for use, the end-use concentration trichloro- of all di- or trichloroisocyanuric acid chemi- cals in the solution is not to exceed 100 ppm determined as total available chlorine 1,3,5-Triazine, N,N′,N″-trichloro-2,4,6-triamino- 7673–09–8 When ready for use, the end-use concentration of all di- or trichloroisocyanuric acid chemi- cals in the solution is not to exceed 200 ppm determined as total available chlorine

[69 FR 23136, Apr. 28, 2004, as amended at 71 FR 30811, May 31, 2006; 71 FR 45423, Aug. 9, 2006; 71 FR 46125, Aug. 11, 2006; 72 FR 51186, Sept. 6, 2007; 73 FR 37858, July 2, 2008; 73 FR 49107, Aug. 20, 2008; 73 FR 53725, Sept. 17, 2008; 74 FR 27454, June 10, 2009; 74 FR 38944, Aug. 5, 2009; 74 FR 40509, Aug. 12, 2009; 75 FR 40735, July 14, 2010; 76 FR 55267, Sept. 7, 2011; 77 FR 45498, Aug. 1, 2012; 77 FR 50617, Aug. 22, 2012; 77 FR 53150, Aug. 31, 2012; 77 FR 68692, Nov. 16, 2012; 78 FR 35147, June 12, 2013; 78 FR 46264, July 31, 2013; 78 FR 48621, Aug. 9, 2013; 78 FR 59269, Sept. 26, 2013; 78 FR 65565, Nov. 1, 2013; 78 FR 67042, Nov. 8, 2013; 78 FR 78731, Dec. 27, 2013; 79 FR 6096, Feb. 3, 2014; 79 FR 26152, May 7, 2014; 79 FR 32666, June 6, 2014; 79 FR 33473, June 11, 2014; 79 FR 52993, Sept. 5, 2014; 79 FR 66312, Nov. 7, 2014; 80 FR 11593, Mar. 4, 2015; 80 FR 28842, May 20, 2015; 80 FR 32033, 32038, June 5, 2015; 80 FR 34070, June 15, 2015]

§ 180.950 Tolerance exemptions for cordance with good agricultural or minimal risk active and inert ingre- manufacturing practices. dients. (a) Commonly consumed food commod- Unless specifically excluded, residues ities. Commonly consumed food com- resulting from the use of the following modities means foods that are com- substances as either an inert or an ac- monly consumed for their nutrient tive ingredient in a pesticide chemical properties. The term commonly con- formulation, including antimicrobial sumed food commodities shall only pesticide chemicals, are exempted from apply to food commodities (whether a the requirement of a tolerance under FFDCA section 408, if such use is in ac-

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raw agricultural commodity or a proc- (2) Excluded from the term edible essed commodity) in the form the com- fats and oils are plant oils used in the modity is sold or distributed to the pesticide chemical formulation specifi- public for consumption. cally to impart their characteristic (1) Included within the term com- fragrance and/or flavoring. monly consumed food commodities are: (d) [Reserved] (i) Sugars such as sucrose, lactose, (e) Specific chemical substances. Resi- dextrose and fructose, and invert sugar dues resulting from the use of the fol- and syrup. lowing substances as either an inert or (ii) Spices such as cinnamon, cloves, an active ingredient in a pesticide and red pepper. chemical formulation, including anti- (iii) Herbs such as basil, anise, or microbial pesticide chemicals, are ex- fenugreek. empted from the requirement of a tol- (2) Excluded from the term com- erance under FFDCA section 408, if monly consumed food commodities are: such use is in accordance with good ag- (i) Any food commodity that is adul- ricultural or manufacturing practices. terated under 21 U.S.C. 342. (ii) Both the raw and processed forms Chemical CAS No. of peanuts, tree nuts, milk, soybeans, Acetic acid, sodium salt ...... 127–09–3 eggs, fish, crustacea, and wheat. Alpha-cyclodextrin ...... 10016–20–3 Amylopectin, acid-hydrolyzed, 1- (iii) Alcoholic beverages. octenylbutanedioate ...... 113894–85– (iv) Dietary supplements. 2 (b) Animal feed items. Animal feed Amylopectin, hydrogen 1- items means meat meal and all items octadecenylbutanedioate ...... 125109–81– 1 derived from field crops that are fed to Animal glue ...... None livestock excluding both the raw and Ascorbic acid (vitamin C) ...... 50–81–7 processed forms of peanuts, tree nuts, Beeswax ...... 8012–89–3 Benzoic acid, sodium salt ...... 532–32–1 milk, soybeans, eggs, fish, crustacea, Beta-cyclodextrin ...... 7585–39–9 and wheat. Meat meal is an animal feed Carbonic acid, monopotassium salt ...... 298–14–6 composed of dried animal fat and pro- Carbonic acid, monosodium salt (sodium bicar- bonate) ...... 144–55–8 tein that has been sterilized. Other Carnauba wax ...... 8015–86–9 than meat meal, the term animal feed Carob gum (locust bean gum) ...... 9000–40–2 item does not extend to any item de- Castor oil ...... 8001–79–4 signed to be fed to animals that con- Castor oil, hydrogenated ...... 8001–78–3 ...... 9004–34–6 tains, to any extent, components of Cellulose acetate ...... 9004–35–7 animals. Included within the term ani- Cellulose, carboxy methyl ether, sodium salt ... 9004–32–4 mal feed items are: Cellulose, 2-hydroxyethyl ether ...... 9004–62–0 Cellulose, 2-hydroxypropyl ether ...... 9004–64–2 (1) The hulls and shells of the com- Cellulose, 2-hydroxypropyl methyl ether ...... 9004–65–3 modities specified in paragraph Cellulose, methyl ether ...... 9004–67–5 (a)(2)(ii) of this section, and cocoa Cellulose, mixture with cellulose carboxymethyl ether, sodium salt ...... 51395–75–6 bean. Cellulose, pulp ...... 65996–61–4 (2) Bird feed such as canary seed. Cellulose, regenerated ...... 68442–85–3 (3) Any feed component of a medi- Citric acid ...... 77–92–9 cated feed meeting the definition of an Citric acid, 2-(acetyloxy)-, tributyl ester ...... 77–90–7 Citric acid, calcium salt ...... 7693–13–2 animal feed item. Citric acid, calcium salt (2:3) ...... 813–94–5 (c) Edible fats and oils. Edible fats and Citric acid, dipotassium salt ...... 3609–96–9 oils means all edible (food or feed) fats Citric acid, disodium salt ...... 144–33–2 Citric acid, monohydrate ...... 5949–29–1 and oils, derived from either plants or Citric acid, monopotassium salt ...... 866–83–1 animals, whether or not commonly Citric acid, monosodium salt ...... 18996–35–5 consumed, including products derived Citric acid, potassium salt ...... 7778–49–6 Citric acid, triethyl ester ...... 77–93–0 from hydrogenating (food or feed) oils, Citric acid, tripotassium salt ...... 866–84–2 or liquefying (food or feed) fats. Citric acid, tripotassium salt, monohydrate ...... 6100–05–6 (1) Included within the term edible Citric acid, sodium salt ...... 994–36–5 fats and oils are oils (such as soybean Citric acid, trisodium salt ...... 68–04–2 Citric acid, trisodium salt, dihydrate ...... 6132–04–3 oil) that are derived from the commod- Citric acid, trisodium salt, pentahydrate ...... 6858–44–2 ities specified in paragraph (a)(2)(ii) of Coffee grounds ...... 68916–18–7 this section when such oils are highly Dextrins ...... 9004–53–9 1,3-Dioxolan-2-one, 4-methyl-(propylene car- refined via a solvent extraction proce- bonate) ...... 108–32–7 dure. Fumaric acid ...... 110–17–8

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Chemical CAS No. Chemical CAS No.

Gamma-cyclodextrin ...... 17465–86–0 Silica, amorphous, fumed (crystalline free) ...... 112945–52– Gellan gum ...... 71010–52–1 5 D-Glucitol (sorbitol) ...... 50–70–4 Silica, amorphous, precipitated and gel ...... 7699–41–4 Glycerol (glycerin) (1,2,3-propanetriol) ...... 56–81–5 Silica gel ...... 63231–67–4 Guar gum ...... 9000–30–0 Silica gel, precipitated, crystalline-free ...... 112926–00– Humic acid ...... 1413–93–6 8 Humic acid, potassium salt ...... 68514–28–3 Silica, hydrate ...... 10279–57–9 Humic acid, sodium salt ...... 68131–04–4 Silica, vitreous ...... 60676–86–0 Lactic acid, n-butyl ester ...... 138–22–7 Lactic acid, n-butyl ester, (S) ...... 34451–19–9 Soap (The water soluble sodium or potassium Lactic acid, ethyl ester ...... 97–64–3 salts of fatty acids produced by either the Lactic acid, ethyl ester,(S) ...... 687–47–8 saponification of fats and oils, or the neutral- Lanolin ...... 8006–54–0 ization of fatty acid) ...... None Lecithins ...... 8002–43–5 Sorbic acid, potassium salt ...... 24634–61–5 Lecithins, soya ...... 8030–76–0 Soapbark (Quillaja saponin) ...... 1393–03–9 Licorice Extract ...... 68916–91–6 Sodium alginate ...... 9005–38–3 Maltodextrin ...... 9050–36–6 Sodium chloride ...... 7647–14–5 Paper ...... None Syrups, hydrolyzed starch, hydrogenated ...... 68425–17–2 Potassium chloride ...... 7447–40–7 Ultramarine blue (C.I. Pigment Blue 29) ...... 57455–37–5 2-Propanol (isopropyl alcohol) ...... 67–63–0 Urea ...... 57–13–6 Red cabbage color, expressed from edible red Vanillin ...... 121–33–5 cabbage heads via a pressing process using Xanthan gum ...... 11138–66–2 only acidified water ...... None

[67 FR 36537, May 24, 2002]

EDITORIAL NOTE: For FEDERAL REGISTER citations affecting § 180.950, see the List of CFR Sections Affected, which appears in the Finding Aids section of the printed volume and at www.fdsys.gov.

§ 180.960 Polymers; exemptions from dient in a pesticide chemical formula- the requirement of a tolerance. tion, including antimicrobial pesticide Residues resulting from the use of chemical formulations, are exempted the following substances, that meet the from the requirement of a tolerance definition of a polymer and the criteria under FFDCA section 408, if such use is specified for defining a low-risk poly- in accordance with good agricultural or mer in 40 CFR 723.250, as an inert ingre- manufacturing practices.

Polymer CAS No.

Acetic acid ethenyl ester, polymer with ethane, ethenyltriethoxysilane 913187–38–9 and sodium ethenesulfonate (1:1); minimum number average molec- ular weight (in amu), 16,200

Acetic acid ethenyl ester, polymer with ethenol and (a)-2-propenyl-(w)- 137091–12–4 hydroxypoly (oxy-1,2-ethanediyl) minimum number average molec- ular weight (in amu), 15,000

Acetic acid ethenyl ester, polymer with 1-ethenyl-2-pyrrolidinone 25086–89–9

Acetic acid ethenyl ester, polymer with oxirane, minimum number av- 25820–49–9 erage molecular weight (in amu), 17,000

Acetic acid ethenyl ester, polymer with sodium 2-methyl-2-[(1-oxo-2- 924892–37–5 propen-1-yl)amino]-1-propanesulfonate (1:1), hydrolyzed, minimum number average molecular weight (in amu), 61,000

Acrylic acid-benzyl methacrylate-1-propanesulfonic acid, 2-methyl-2- 1152297–42–1 [(1-oxo-2-propenyl)amino]-, monosodium salt, minimum number av- erage molecular weight (in amu), 1500

Acrylic acid, polymerized, and its ethyl and methyl esters None

Acrylic acid-sodium acrylate-sodium-2-methylpropanesulfonate copoly- 97953–25–8 mer, minimum average molecular weight (in amu), 4,500

Acrylic acid-stearyl methacrylate copolymer, minimum number average 27756–15–6 molecular weight (in amu), 2,500

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Polymer CAS No.

Acrylic acid, styrene, a-methyl styrene copolymer, ammonium salt, 89678–90–0 minimum number average molecular weight (in amu), 1,250

Acrylic acid terpolymer, partial sodium salt, minimum number average 151006–66–5 molecular weight (in amu), 2,400

Acrylic polymers composed of one or more of the following monomers: None Acrylic acid, methyl acrylate, ethyl acrylate, butyl acrylate, hydroxy- ethyl acrylate, hydroxypropyl acrylate, hydroxybutyl acrylate, carboxyethyl acrylate, methacrylic acid, methyl methacrylate, ethyl methacrylate, butyl methacrylate, isobutyl methacrylate, hydroxyethyl methacrylate, hydroxypropyl methacrylate, hydroxybutyl methacry- late, lauryl methacrylate, and stearyl methacrylate; with none and/or one or more of the following monomers: Acrylamide, N-methyl acryl- amide, N,N-dimethyl acrylamide, N-octylacrylamide, maleic anhy- dride, maleic acid, monoethyl maleate, diethyl maleate, monooctyl maleate, dioctyl maleate; and their corresponding sodium, potas- sium, ammonium, isopropylamine, triethylamine, monoethanolamine, and/or triethanolamine salts; the resulting polymer having a min- imum number average molecular weight (in amu), 1,200

Acrylonitrile-butadiene copolymer conforming to 21 CFR 180.22, min- 9003–18–3 imum average molecular weight (in amu), 1,000

Acrylonitrile-styrene-hydroxypropyl methacrylate copolymer, minimum None number average molecular weight (in amu), 447,000

a-alkyl (C12–C15) - w- hydroxypoly(oxypropylene)poly(oxyethylene)co- 68551–13–3 polymers (where the poly(oxypropylene)c content is 3–60 moles and the poly(oxyethylene) content is 5–80 moles), the resulting ethoxylated propoxylated (C12–C15) alcohols having a minimum mo- lecular weight (in amu), 1,500

695

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Polymer CAS No.

a-alkyl-w-hydroxypoly (oxypropylene) and/or poly (oxyethylene) poly- 9002–92–0; 9004–95–9; 9004–98–2; 9005–00–9; mers where the alkyl chain contains a minimum of six carbons and 9035–85–2; 9038–29–3; 9038–43–1; 9040–05–5; a minimum number average molecular weight (in amu) 1,100. 9043–30–5; 9087–53–0; 25190–05–0; 24938–91–8; 25231–21–4; 26183–52–8; 26468–86–0; 26636–39– 5; 27252–75–1; 27306–79–2; 31726–34–8; 34398– 01–1; 34398–05–5; 37251–67–5; 37311–00–5; 37311–01–6; 37311–02–7; 37311–04–9; 39587–22– 9; 50861–66–0; 52232–09–4; 52292–17–8; 52609– 19–5; 57679–21–7; 59112–62–8; 60828–78–6; 61702–78–1; 61725–89–1; 61791–13–7; 61791–20– 6; 61791–28–4; 61804–34–0; 61827–42–7; 61827– 84–7; 62648–50–4; 63303–01–5; 63658–45–7; 63793–60–2; 64366–70–7; 64415–24–3; 64415–25– 4; 64425–86–1; 65104–72–5; 65150–81–4; 66455– 14–9: 66455–15–0; 67254–71–1; 67763–08–0; 68002–96–0; 68002–97–1; 68131–39–5; 68131–40– 8; 68154–96–1; 68154–97–2; 68154–98–3; 68155– 01–1; 68213–23–0; 68213–24–1; 68238–81–3; 68238–82–4; 68409–58–5; 68409–59–6; 68439–30– 5; 68439–45–2; 68439–46–3; 68439–48–5; 68439– 49–6; 68439–50–9; 68439–51–0; 68439–53–2; 68439–54–3; 68458–88–8; 68526–94–3; 68526–95– 4; 68551–12–2; 68551–13–3; 68551–14–4; 68603– 20–3; 68603–25–8; 68920–66–1; 68920–69–4; 68937–66–6; 68951–67–7; 68954–94–9; 68987–81– 5; 68991–48–0; 69011–36–5; 69013–18–9; 69013– 19–0; 69227–20–9; 69227–21–0; 69227–22–1; 69364–63–2; 70750–27–5; 70879–83–3; 70955–07– 6; 71011–10–4; 71060–57–6; 71243–46–4; 72066– 65–0; 72108–90–8; 72484–69–6; 72854–13–8; 72905–87–4; 73018–31–2; 73049–34–0; 74432–13– 6; 74499–34–6; 78330–19–5; 78330–20–8; 78330– 21–9; 78330–23–1; 79771–03–2; 84133–50–6; 85422–93–1; 97043–91–9; 97953–22–5; 102782–43– 4; 103331–86–8; 103657–84–7; 103657–85–8; 103818–93–5; 103819–03–0; 106232–83–1; 111905– 54–5; 116810–31–2; 116810–32–3; 116810–33–4; 120313–48–6; 120944–68–5; 121617–09–2; 126646– 02–4; 126950–62–7; 127036–24–2; 139626–71–4; 152231–44–2; 154518–36–2; 157627–86–6; 157627– 88–8; 157707–41–0; 157707–43–2; 159653–49–3; 160875–66–1; 160901–20–2; 160901–09–7; 160901– 19–9; 161025–21–4; 161025–22–5; 166736–08–9; 169107–21–5; 172588–43–1; 176022–76–7; 196823– 11–7; 287935–46–0; 288260–45–7; 303176–75–2; 954108–36–2

Alkyl (C12–C20) methacrylate-methacrylic acid copolymer, minimum None molecular weight (in amu), 11,900

2H-Azepin-2-one, 1-ethenylhexahydro-, homopolymer 25189–83–7

1,3 Benzene dicarboxylic acid, 5-sulfo-, 1,3-dimethyl ester, sodium 212842–88–1 salt, polymer with 1,3-benzene dicarboxylic acid, 1,4-benzene dicarboxylic acid, dimethyl 1,4-benzene dicarboxylate and 1,2- ethanediol, minimum number average molecular weight (in amu), 2,580

3,5-Bis(6-isocyanatohexyl)-2H-1,3,5-oxadiazine-2,4,6-(3H,5H)-trione, 87823–33–4 polymer with diethylenetriamine, minimum number average molec- ular weight (in amu), 1,000,000

Polymer of one or more diglycidyl ethers of bisphenol A, resorcinol, None glycerol, cyclohexanedimethanol, neopentyl glycol, and polyethylene glycol with one or more of the following: Polyoxypropylene diamine, polyoxypropylene triamine, N-aminoethyl-piperazine, trimethyl-1,6- hexanediamine isophorone diamine, N,N-dimethyl-1,3- diaminopropane, nadic methyl anhydride, 1,2-cyclohexane- dicarboxylic anhydride and 1,2,3,6-tetrahydrophthalic anhydride, minimum number average molecular weight (in amu), 400,000

Butadiene-styrene copolymer None

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Polymer CAS No.

Butanedioic acid, 2-methylene-, polymer with 2,5-furandione, sodium 556055–76–6 and ammonium salts, hydrogen peroxide-initiated, minimum number 701908–99–8 average molecular weight (in amu), 2,500–3,000

1,4-Butanediol-methylenebis(4-phenylisocyanate)-poly(tetramethylene 9018–04–6 glycol) copolymer, minimum molecular weight (in amu) 158,000

Butene, homopolymer 9003–29–6

2-butenedioic acid (2Z)-, monobutyl ester, polymer with 205193–99–3 methoxyethene, sodium salt, minimum number average molecular weight (in amu), 18,200

2-Butenedioic acid (Z)-, polymer with ethenol and ethenyl acetate, so- 139871–83–3 dium salt, minimum number average molecular weight (in amu), 75,000

Butyl acrylate-vinyl acetate-acrylic acid copolymer, minimum number 65405–40–5 average molecular weight (in amu), 18,000

Carbonic acid, diethyl ester, polymer with a-hydro-w- 1147260–65–8 hydroxypoly[oxy(methyl-1,2-ethanediyl)] ether with 2-ethyl-2- (hydroxymethyl)-1,3-propanediol (3:1), ester with a-[[[[5- (carboxyamino)-1,3,3-trimethylcyclohexyl]methyl]amino]carbonyl]-w- methoxypoly(oxy-1,2-ethanediyl), minimum number average molec- ular weight (in amu), 1,900

Castor oil, ethoxylated, dioleate, minimum number average molecular 110531–96–9 weight (in amu), 1260.

Castor oil, ethoxylated, oleate, minimum number average molecular 220037–02–5 weight (in amu), 1,600

Castor oil, polymer with adipic acid, linoleic acid, oleic acid and ricin- 1357486–09–9 oleic acid, minimum number average molecular weight (in amu), 3,500

Castor oil, polyoxyethylated; the poly(oxyethylene) content averages None 5–54 moles

Chlorinated polyethylene 64754–90–1

Cross-linked nylon-type polymer formed by the reaction of a mixture of None sebacoyl chloride and polymethylene polyphenylisocycanate with a mixture of ethylenediamine and diethylenetriamine

Cross-linked polyurea-type encapsulating polymer None

Dimethylpolysiloxane minimum number average molecular weight (in 63148–62–9 amu), 6,800

Dimethyl silicone polymer with silica, minimum number average molec- 67762–90–7 ular weight (in amu), 1,100,000

a-(o,p-Dinonylphenyl)-w-hydroxypoly(oxyethylene) produced by con- 9014–93–1 densation of 1 mole of dinonylphenol (nonyl group is a propylene trimer isomer) with an average of 140-160 moles of ethylene oxide

Docosyl methacrylate-acrylic acid copolymer, or docosyl methacrylate- None octadecyl methacrylate-acrylic acid copolymer, minimum number av- erage molecular weight (in amu), 3,000

1,12-Dodecanediol dimethacrylate polymer, minimum molecular weight None (in amu), 100,000

a-(p-Dodecylphenyl)-w-hydroxypoly(oxyethylene) produced by the con- 9014–92–0 densation of 1 mole of dodecylphenol (dodecyl group is a propylene 26401–47–8 tetramer isomer) with an average of 30-70 moles of ethylene oxide

1,2-Ethanediamine, N1-(2-aminoethyl)-, polymer with 2,4-diisocyanato- 35297–61–1 1-methylbenzene, minimum number average molecular weight (in amu), one million

697

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Polymer CAS No.

1, 2-Ethanediamine, polymer with methyl oxirane and oxirane, min- 26316–40–5 imum number average molecular weight (in amu), 1,100

Ethylene glycol dimethyacrylate-lauryl methacrylate copolymer, min- None imum molecular weight (in amu), 100,000

Ethylene glycol dimethacrylate polymer, minimum molecular weight (in None amu), 100,000

Fatty acids, tall-oil, ethoxylated propoxylated, minimum number aver- 67784–86–5 age molecular weight (in amu), 2,009

Formaldehyde, polymer with a-[bis(1-phenylethyl)phenyl]-w- 157291–93–5 hydroxypoly(oxy-1,2-ethanediyl), number average molecular weight (in amu), 1,803

Formaldehyde, polymer with 2-methyloxirane and 4-nonylphenol, min- 37523–33–4 imum number average molecular weight (in amu), 4,000

Fumaric acid-isophthalic acid-styrene-ethylene/propylene glycol co- None polymer, minimum average molecular weight (in amu), 1×1018

2,5-Furandione, polymer with ethenylbenzene, hydrolyzed, 3- 1062609–13–5 (dimethylamino)propyl imide, imide with polyethylene-polypropylene glycol 2-aminopropyl me ether, 2,2′-(1,2-diazenediyl)bis[2- methylbutanenitrile]-initiated, minimum number average molecular weight (in amu), 5,816

2,5-Furandione, polymer with ethenylbenzene, reaction products with 162568–32–3 polyethylene-polypropylene glycol 2-aminopropyl Me ether; minimum number average molecular weight (in amu), 14,000

2,5-Furandione, polymer with methoxyethene, butyl ethyl ester, sodium 1471342–08–1 salt, minimum number average molecular weight (in amu), 18,200

Hexadecyl acrylate-acrylic acid copolymer, hexadecyl acrylate-butyl None acrylate-acrylic acid copolymer, or hexadecyl acrylate-dodecyl acry- late-acrylic acid copolymer, minimum number average molecular weight (in amu), 3,000

Hexamethyl disilizane, reaction product with silica, minimum number 68909–20–6 average molecular weight (in amu), 645,000

1,6-Hexanediol dimethyacrylate polymer, minimum molecular weight None (in amu), 100,000

a-Hydro-w-hydroxy-poly(oxyethylene) C8 alkyl ether citrates, 330977–00–9 poly(oxyethylene) content is 4–12 moles, minimum number average molecular weight (in amu) 1,300

a-Hydro-w-hydroxy-poly(oxyethylene) C10–C16-alkyl ether citrates, 330985–58–5 poly(oxyethylene) content is 4–12 moles, minimum number average molecular weight (in amu) 1,100

a-Hydro-w-hydroxy-poly(oxyethylene) C16–C18-alkyl ether citrates, 330985–61–0 poly(oxyethylene) content is 4–12 moles, minimum number average molecular weight (in amu) 1,300

a-Hydro-w-hydroxypoly(oxyethylene), minimum number average mo- 25322–68–3 lecular weight (in amu), 17,000

a-Hydro-w-hydroxypoly(oxyethylene)poly (oxypropylene) None poly(oxyethylene) block copolymer; the minimum poly(oxypropylene) content is 27 moles and the minimum molecular weight (in amu) is 1,900

a-Hydro-w-hydroxypoly(oxypropylene); minimum molecular weight (in None amu) 2,000

12-Hydroxystearic acid-polyethylene glycol copolymer, minimum num- 70142–34–6 ber average molecular weight (in amu), 3,690

Isodecyl alcohol ethoxylated (2–8 moles) polymer with chloromethyl None oxirane, minimum number average molecular weight (in amu) 2,500

698

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Polymer CAS No.

Lauryl methacrylate-1,6-hexanediol dimethacrylate copolymer, min- None imum molecular weight (in amu), 100,000

Maleic acid-butadiene copolymer None

Maleic acid monobutyl ester-vinyl methyl ether copolymer, minimum 25119–68–0 average molecular weight (in amu), 52,000

Maleic acid monoethyl ester-vinyl methyl ether copolymer, minimum 25087–06–3 average molecular weight (in amu), 46,000

Maleic acid monoisopropyl ester-vinyl methyl ether copolymer, min- 31307–95–6 imum average molecular weight (in amu), 49,000

Maleic anhydride-diisobutylene copolymer, sodium salt, minimum num- 37199–81–8 ber average molecular weight (in amu) 5,0007–18,000

Maleic anhydride-methylstyrene copolymer sodium salt, minimum 60092–15–1 number average molecular weight (in amu), 15,000

Maleic anhydride-methyl vinyl ether, copolymer, average molecular None weight (in amu), 250,000

Methacrylic acid-methyl methacrylate-polyethylene glycol methyl ether 100934–04–1 methacrylate copolymer, minimum number averge molecular weight (in amu), 3,700

Methacrylic acid-methyl methacrylate-polyethylene glycol monomethyl 111740–36–4 ether methacrylate graft copolymer, minimum number average mo- lecular weight (in amu), 1,800

Methacrylic copolymer, minimum number average molecular weight (in 63150–03–8 amu), 15,000

Methyl methacrylate-methacrylic acid-monomethoxypolyethylene glycol 119724–54–8 methacrylate copolymer,) minimum number average molecular weight (in amu), 2,730

Methyl methacrylate-2-sulfoethyl methacrylate- None dimethylaminoethylmethacrylate-glycidyl methacrylate-styrene-2- ethylhexyl acrylate graft copolymer, minimum average molecular weight (in amu), 9,600

Methyl vinyl ether-maleic acid copolymer), minimum number average 25153–40–6 molecular weight (in amu), 75,000

Methyl vinyl ether-maleic acid copolymer, calcium sodium salt, min- 62386–95–2 imum number average molecular weight (in amu), 900,000

Monophosphate ester of the block copolymer a-hydro-w- None hydroxypoly(oxyethylene) poly(oxypropylene) poly(oxyethylene); the poly(oxypropylene) content averages 37–41 moles, average molec- ular weight (in amu), 8,000

a-(p-Nonylphenyl)-w-hydroxypoly(oxyethylene) mixture of dihydrogen None phosphate and monohydrogen phosphate esters and the cor- responding ammonium, calcium, magnesium, monoethanolamine, potassium, sodium, and zinc salts of the phosphate esters; the nonyl group is a propylene trimer isomer and the poly(oxyethylene) content averages 30 moles

a-(p-Nonylphenyl)-w-hydroxypoly(oxyethylene) sulfate, and its ammo- None nium, calcium, magnesium, monoethanolamine, potassium, sodium, and zinc salts; the nonyl group is a propylene trimer isomer and the poly(oxyethylene) content averages 30-90 moles of ethylene oxide

a-(p-Nonylphenyl-w-hydroxypoly(oxypropylene) block polymer with None poly(oxyethylene); polyoxypropylene content of 10–60 moles; polyoxyethylene content of 10–80 moles; molecular weight (in amu), 1,200–7,100.

a-(r-Nonylphenyl)poly(oxypropylene) block polymer with 37251–69–7 poly(oxyethylene); poly oxyethylene content 30 to 90 moles; min- imum number average molecular weight (in amu), 1,889

699

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Polymer CAS No.

Octadecanoic Acid, 12-Hydroxy-, Homopolymer Ester with 2- 1373125–59–7 Methylloxirane Polymer with Oxirane monobutyl Ether, minimum number average molecular weight (in amu), 4,500

Octadecanoic acid, 12-hydroxy-, homopolymer, octadecanoate min- 58128–22–6) imum number average molecular weight (in amu), 1,370

a-cis-9-Octadecenyl-w-hydroxypoly(oxyethylene); the octadecenyl None group is derived from oleyl alcohol and the poly(oxyethylene) con- tent averages 20 moles

Octadecyl acrylate-acrylic acid copolymer, octadecyl acrylate-dodecyl None acrylate-acrylic acid copolymer, octadecyl methacrylate-butyl acry- late-acrylic acid copolymer, octadecyl methacrylate-hexyl acrylate- acrylic acid copolymer, octadecyl methacrylate-dodecyl acrylate- acrylic acid copolymer, or octadecyl methacrylate-dodecyl methacry- late-acrylic acid copolymer, minimum number average molecular weight (in amu) 3,000

Oleic acid diester of a-hydro-w-hydroxypoly(oxyethylene); the None poly(oxyethylene), average molecular weight (in amu), 2,300

2-oxepanone, homopolymer, minimum number average molecular 24980–41–4 weight (in amu) 52,000

Oxirane, decyl-, reaction products with polyethylene-polypropylene gly- 903890–89–1 col ether with trimethylolpropane (3:1)

Oxirane, hexadecyl-, reaction products with polyethylene-poly- 893427–80–0 propylene glycol ether with trimethylolpropane (3:1)

Oxirane, 2-methyl-, polymer with oxirane, dimethyl ether, minimum 61419–46–3 number average molecular weight (in amu), 2,800

Oxirane, methyl-, polymer with oxirane, ether with 2-ethyl-2- 903890–90–4 (hydroxymethyl)-1,3-propanediol (3:1), reaction products with tetradecyloxirane

Oxirane, methyl-, polymer with oxirane, mono[2-(2-butoxyethoxy) ethyl] 85637–75–8 ether, minimum number average molecular weight (in amu), 2,500

Oxirane, methyl-, polymer with Oxirane, Monobutyl Ether 9038–95–3

Oxirane, 2-methyl-, polymer with oxirane, minimum number average 9003–11–6 molecular weight (in amu), 1,100

Oxirane, 2-methyl-, polymer with oxirane, mono [2-[2-(2- 926031–36–9 butoxymethylethoxy)methylethoxy]methylethyl] ether, minimum num- ber average molecular weight (in amu), 3,000

Oxirane, phenyl, polymer with oxirane, monooctyl ether, minimum av- 83653–00–3 erage molecular weight (in amu) 1,200

Polyamide polymer derived from sebacic acid, vegetable oil acids with None or without dimerization, terephthalic acid and/or ethylenediamine

Polyethylene glycol-polyisobutenyl anhydride-tall oil fatty acid copoly- 68650–28–2 mer, minimum number average molecular weight (in amu), 2,960

Polyethylene, oxidized, minimum number average molecular weight (in None amu), 1,200

Polymers produced by the reaction of either 1,6-hexanediisocyanate; 1161844–26–3, 1161844–30–9, 1161844–43–4, 2,4,4-trimethyl-1,6-hexanediisocyanate; 5-isocyanato-1- 1161844–51–4, 1161844–53–6, 693252–31–2, (isocyanatomethyl)-fxsp0;1,3,3fxsp0;-trimethyIcyclohexane 162993–60–4, 630102–86–2 (isophoronediisocyanate); 4,4′-methylene-bis-1,1′- cyclohexanediisocyanate; 4,4′-methylene-bis-1,1′ benzyldiisocyanate; or 1,3-bis-(2-isocyanatopropan-2-yl)benzene with polyethylene glycol and end-capped with one or a mixture of more than one of octanol, decanol, dodecanol, tetradecanol, hexadecanol, octadecanol, and octadec-9-enol or polyethyleneglycol ethers of octanol, decanol, dodecanol, tetradecanol, hexadecanol, octadecanol, and octadec-9-enol, minimum number average molec- ular weight (in amu), 20,000

700

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Polymer CAS No.

Polymethylene polyphenylisocyanate, polymer with ethylene diamine, None diethylene triamine and sebacoyl chloride, cross-linked; minimum number average molecular weight (in amu), 100,000

Polyoxyalkylated glycerol fatty acid esters; the mono-, di-, or 61791–23–9, 68201–46–7, 68440–49–3, 68458–88–8, triglyceride mixtures of C8 through C22, primarily C8 through C18 68606–12–2, 68648–38–4, 70377–91–2, 70914–02– saturated and unsaturated, fatty acids containing up to 15% water 2, 72245–12–6, 72698–41–3, 180254–52–8, by weight reacted with a minimum of three moles of either ethylene 248273–72–5, 308063–50–5, 952722–33–7 oxide or propylene oxide; the resulting polyoxyalkylated glycerol ester polymer minimum number average molecular weight (in amu), 1,500

Polyoxyalkylated sorbitan fatty acid esters with C6 through C22 ali- 81776–11–6, 87090–31–1, 88895–72–1, 103171–31–9, phatic alkanoic and/or alkenoic fatty acids, branched or linear, the 161026–53–5, 1472644–80–6, 1472644–81–7, resulting polyoxyalkylene sorbitan esters minimum number average 1472644–84–0, 1472644–85–1, 1472644–87–3, molecular weight (in amu), 1,300 1472644–88–4, 1472654–83–3, 1472655–32–5, 1472661–05–4, 1472661–17–8, 1472663–59–4, 1472663–64–1, 1472663–66–3, 1472663–92–5, 1472668–03–3

Polyoxyalkylated trimethylopropanes with 20 to 80 moles of ethylene 25765–36–0; 29860–47–7; 37339–03–0; 52624–57–4; and/or propylene oxide, fatty acid esters with C8 through C22 ali- 58090–24–7; 63964–38–5; 72939–62–9; 74521–14– phatic alkanoic and/or alkenoic fatty acids, branched or linear; min- 5; 75300–70–8; 75300–90–2; 84271–03–4; 84271– imum number average molecular weight (in amu), 3,000 04–5; 86850–92–2; 107120–02–5; 133331–01–8; 137587–60–1; 149797–40–0; 149797–41–1; 150695– 97–9; 152130–24–0; 163349–94–8; 163349–95–9; 163349–96–0; 163349–97–1; 163349–98–2; 165467– 70–9; 183619–46–7; 183619–50–3; 185260–01–9; 202606–04–0; 210420–84–1; 233660–70–3; 263011– 96–7; 283602–94–8; 701980–40–7; 872038–58–9; 875709–44–7; 875709–45–8; 875709–46–9; 875709– 47–0; 879898–63–2; 910038–01–6; 1190748–04–9; 1225384–02–0; 1428944–41–5; 1446498–15–2.

Poly(oxy-1,2-ethanediyl), a-hydro-w-hydroxy-, polymer with 1, 1′-meth- 39444–87–6 ylene-bis-[4-isocyanatocyclohexane], minimum number average mo- lecular weight (in amu), 1800

Polyoxyethylated primary amine (C14–C18); the fatty amine is derived None from an animal source and contains 3% water; the poly(oxyethylene) content averages 20 moles

Polyoxyethylated sorbitol fatty acid esters; the polyoxyethylated sor- None bitol solution containing 15% water is reacted with fatty acids limited to C12, C14, C16, and C18, containing minor amounts of associated fatty acids; the poly(oxyethylene) content averages 30 moles.

Polyoxyethylated sorbitol fatty acid esters; the sorbitol solution con- None taining up to 15% water is reacted with 20–50 moles of ethylene oxide and aliphatic alkanoic and/or alkenoic fatty acids C8 through C22 with minor amounts of associated fatty acids; the resulting polyoxyethylene sorbitol ester having a minimum molecular weight (in amu), 1,300

Poly(oxyethylene/oxypropylene) monoalkyl (C6–C10) ether sodium fu- 102900–02–7 marate adduct, minimum number average molecular weight (in amu), 1,900

Polyoxymethylene copolymer, minimum number average molecular None weight (in amu), 15,000

Poly(oxypropylene) block polymer with poly(oxyethylene), molecular None weight (in amu), 1,800–16,000

Poly(phenylhexylurea), cross-linked, minimum average molecular None weight (in amu), 36,000

Polypropylene 9003–07–0

Polystyrene, minimum number average molecular weight (in amu), 9003–53–6 50,000

Polytetrafluoroethylene 9002–84–0

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Polymer CAS No.

Polyvinyl acetate, copolymer with maleic anhydride, partially None hydrolyzed, sodium salt, minimum number average molecular weight (in amu), 53,000

Polyvinylpyrrolidone butylated polymer, minimum number average mo- 26160–96–3 lecular weight (in amu), 9,500

Polyvinyl acetate, minimum molecular weight (in amu), 2,000 None

Polyvinyl acetate—polyvinyl alcohol copolymer, minimum number av- 25213–24–5 erage molecular weight (in amu), 50,000

Polyvinyl alcohol 9002–89–5

Polyvinyl chloride None

Polyvinyl chloride, minimum number average molecular weight (in 9002–86–2 amu), 29,000

Poly(vinylpyrrolidone), minimum number average molecular weight (in 9003–39–8 amu), 4,000

Poly(vinylpyrrolidone-1-eicosene), minimum average molecular weight 28211–18–9 (in amu), 3,000

Poly(vinylpyrrolidone-1-hexadecene), minimum average molecular 63231–81–2 weight (in amu), 4,700

1-propanesulfonic acid, 2-methyl-2-[(1-oxo-2-propenyl)amino]-, mono- 107568–12–7 sodium salt, polymer with ethenol and ethenyl acetate, minimum number average molecular weight (in amu) 50,000

2-Propene-1-sulfonic acid sodium salt, polymer with ethenol and eth- None enyl acetate, number average molecular weight (in amu) 6,000– 12,000

2-Propenoic acid, butyl ester, polymer with 1,6-diisocyanatohexane, N- 1469998–09–1 (hydroxymethyl)-2-methyl-2-propenamide and 2-propenenitrile, min- imum number average molecular weight (in amu), 100,000

2-propenoic acid, butyl ester, polymer with ethenylbenzene, methyl 2- 27306–39–4 methyl-2-propenoate and 2-propenoic acid (in amu), 1900.

2-Propenoic acid, butyl ester, polymer with ethyl 2-propenoate and N- 33438–19–6 (hydroxymethyl)-2-propenamide, minimum number average molec- ular weight (in amu), 30,000

2-Propenoic acid, 2-ethylhexyl ester, polymer with ethenylbenzene 25153–46–2 14,000 daltons

2-Propenoic acid, 2-ethylhexyl ester, polymer with ethenylbenzene and 68240–06–2 2-methylpropyl 2-methyl-2-propenoate, minimum number average molecular weight (in amu), 18,000

2-Propenoic acid, 2-hydroxyethyl ester, polymer with a-[4- 1007234–89–0 (ethenyloxy)butyl]-w-hydroxypoly (oxy-1,2-ethanediyl), minimum number average molecular weight (in amu), 17,000

[2-propenoic acid, 2-methyl-, C12-16-alkyl esters, telomers with 1- 950207–35–9 dodecanethiol, polyethylene-polypropylene glycol ether with pro- pylene glycol monomethacrylate (1:1), and styrene 2,2’-(1,2- diazenediyl)bis[2-methylbutanenitrile]-initiated, minimum number av- erage molecular weight (in amu), 4,000

2-Propenoic acid, methyl ester, polymer with ethenyl acetate, 886993–11–9 hydrolyzed, sodium salts

2-Propenoic acid, 2-methyl-, 2-ethylhexyl ester, telomer with 1- 1283712–50–4 dodecanethiol, ethenylbenzene and 2-methyloxirane polymer with oxirane monoether with 1,2-propanediol mono(2-methyl-2- propenoate), hydrogen 2-sulfobutanedioate, sodium salt, 2, 2′-(1,2- diazenediyl)bis[2-methylpropanenitrile]-initiated, minimum number average molecular weight (in amu), 1,200

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Polymer CAS No.

≤2-Propenoic acid, 2-methyl-, 2-methylpropyl ester, homopolymer, min- 9011–15–8 imum number average molecular weight (in amu), 55,000

2-Propenoic acid, 2-methyl-, phenylmethyl ester, polymer with 2-prope- 1574486–33–1 noic acid, peroxydisulfuric acid ([(HO)S(O)2]2O2) sodium salt (1:2)- initiated, compounds with diethanolamine, minimum number average molecular weight (in amu), 2,000

2-Propenoic acid, 2-methyl-, phenylmethyl ester, polymer with 2-prope- CASRN 1246766–57–3 noic acid and sodium 2-methyl-2-[(1-oxo-2-propen-1-yl)amino]-1- propanesulfonate (1:1), peroxydisulfuric acid ([HO)S(O)2]202) so- dium salt (1:2)-initiated minimum number average molecular weight >1,000 Daltons; maximum number average molecular weight 10,000 Daltons

2-Propenoic acid, 2-methyl-, polymer with butyl 2-propenoate and 25036–16–2 ethenylbenzene, minimum number average molecular weight (in amu), 17,000

2-Propenoic acid, 2-Methyl-, Polymer with Butyl 2-Propenoate, Methyl 153163–36–1 2-Methyl-2-Propenoate, Methyl 2-Propenoate and 2-Propenoic Acid, graft, Compound with 2-Amino-2-Methyl-1-Propanol

2-Propenoic Acid, 2-Methyl-, Polymer with Ethenylbenzene, 2- 146753–99–3 Ethylhexyl 2-Propenoate, 2-Hydroxyethyl 2-Propenoate, N- (Hydroxymethyl) -2-Methyl-2-Propenamide and Methyl 2-Methyl-2- Propenoate, Ammonium Salt

2-Propenoic acid, 2-methyl-, polymers with Bu acrylate, Et acrylate, 890051–63–5 Me methacrylate and polyethylene glycol methacrylate C16-18-alkyl ethers, minimum number average molecular weight (in amu), 13,000

2-Propenoic acid, 2-methyl-, telomer with 2-ethylhexyl 2-propenoate, 1260001–65–7 2-propanol and sodium 2-methyl-2-[(1-oxo-2-propen-1-yl) amino]-1- propanesulfonate (1:1), sodium salt, minimum number average mo- lecular weight (in amu): 2,900

2-Propenoic acid, monoester with 1,2-propanediol, polymer with a-[4- 955015–23–3 (ethenyloxy) butyl]-w-hydroxypoly (oxy-1,2-ethanediyl) and 2,5- furandione, minimum number average molecular weight (in amu), 25,000

2-propenoic acid polymer, with 1,3-butadiene and ethenylbenzene, 25085–39–6 minimum number average molecular weight (in amu), 9400

2-Propenoic acid, polymer with ethenyl acetate, ethenylbenzene, 2- 85075–52–1 ethylhexyl 2-propenoate and ethyl 2-propenoate, minimum number average molecular weight (50,149 Daltons)

2-Propenoic acid, polymer with ethenylbenzene and (1-methylethenyl) 129811–24–1 benzene, sodium salt, minimum number average molecular weight (in amu), 2,800

2-Propenoic acid, polymer with a-[4-(ethenyloxy) butyl]-w-hydroxypoly 251479–97–7 (oxy-1,2-ethanediyl) and 2,5-furandione, sodium salt, minimum num- ber average molecular weight (in amu), 25,000

2-Propenoic acid, polymer with a-[4-(ethenyloxy) butyl]-w-hydroxypoly 518026–64–7 (oxy-1,2-ethanediyl) and 1,2-propanediol mono-2-propenoate, potas- sium sodium salt, minimum number average molecular weight (in amu), 16,000

2-Propenoic acid, polymer with a-[4-(ethenyloxy) butyl]-w-hydroxypoly 250591–84–5 (oxy-1, 2-ethanediyl), sodium salt, minimum number average molec- ular weight (in amu), 24,000

2-Propenoic acid, polymer with 2-propenamide, sodium salt, minimum 25085–02–3 number average molecular weight (in amu), 18,000

2-Propenoic acid, sodium salt, polymer with 2-propenamide, minimum 25987–30–8 number average molecular weight (in amu), 18,000

2-Propenoic, 2-methyl-, polymers with ethyl acrylate and polyethylene 888969–14–0 glycol methylacrylate C18-22 alkyl ethers

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Polymer CAS No.

2-Pyrrolidone, 1-ethenyl-, polymer with ethenol, minimum number av- 26008–54–8 erage molecular weight (in amu), 23,000

Silane, dichloromethyl- reaction product with silica minimum number 68611–44–9 average molecular weight (in amu), 3,340,000

Silane, trimethoxy[3-(oxiranylmethoxy)propyl]-, hydrolysis products with 68584–82–7 silica, minimum number average molecular weight (in amu), 640,000

Silicic acid, sodium salt, reaction products with chlorotrimethylsilane None and iso-propyl alcohol, reaction with poly(oxypropylene)- poly(oxyethylene) glycol, minimum number average molecular weight (in amu), 75,000

Sodium polyflavinoidsulfonate, consisting chiefly of the copolymer of None catechin and leucocyanidin

Soybean oil, ethoxylated; the poly(oxyethylene) content averages 10 61791–23–9 moles or greater

Starch, oxidized, polymers with Bu acrylate, tert-Bu acrylate and sty- 204142–80–3 rene, minimum number average molecular weight (in amu), 10,000

Stearyl methacrylate-1,6-hexanediol dimethacrylate copolymer, min- None imum molecular weight (in amu), 100,000

Styrene, copolymers with acrylic acid and/or methacrylic acid, with None none and/or one or more of the following monomers: Acrylamidopropyl methyl sulfonic acid, methallyl sulfonic acid, 3- sulfopropyl acrylate, 3-sulfopropyl methacrylate, hydroxypropyl meth- acrylate, hydroxypropyl acrylate, hydroxyethyl methacrylate, hy- droxyethyl acrylate, and/or lauryl methacrylate; and its sodium, po- tassium, ammonium, monoethanolamine, and triethanolamine salts; the resulting polymer having a minimum number average molecular weight (in amu), 1200

Styrene-ethylene-propylene block copolymer, minimum number aver- 108388–87–0 age molecular weight (in amu), 125,000

Styrene, 2-ethylhexyl acrylate, butyl acrylate copolymer, minimum 30795–23–4 number average molecular weight (in amu), 4,200

Styrene-2-ethylhexyl acrylate-glycidyl methacrylate-2-acrylamido-2- None methylpropanesulfonic acid graft copolymer, minimum number aver- age molecular weight (in amu), 12,500

Styrene-maleic anhydride copolymer None

Styrene-maleic anhydride copolymer, ester derivative None

Tall oil, polymer with polyethylene glycol and succinic anhydride 1398573–80–2 monopolyisobutylene derivs., minimum number average molecular weight (in amu), 1,200

Tetradecyl acrylate-acrylic acid copolymer, minimum number average None molecular weight (in amu), 3,000

Tetraethoxysilane, polymer with hexamethyldisiloxane, minimum num- 104133–09–7 ber average molecular weight (in amu), 2,500

Tetraethoxysilane, polymer with hexamethyldisiloxane, minimum num- 104133–09–7 ber average molecular weight (in amu), 6,500

a-[p-(1,1,3,3-Tetramethylbutyl)phenyl]-w-hydroxypoly(oxyethylene) pro- 9036–19–5 duced by the condensation of 1 mole of p-(1,1,3,3- 9002–93–1 tetramethylbutyl)phenol with a range of 30-70 moles of ethylene oxide

a-[p-(1,1,3,3-Tetramethylbutyl)phenyl] poly(oxypropylene) block poly- None mer with poly(oxyethylene); the poly(oxypropylene) content aver- ages 25 moles, the poly(oxyethylene) content averages 40 moles, the molecular weight (in amu) averages 3,400

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Polymer CAS No.

a-[2,4,6-Tris[1-(phenyl)ethyl]phenyl]-w-hydroxy poly(oxyethylene) None poly(oxypropylene) copolymer, the poly(oxypropylene) content aver- ages 2–8 moles, the poly(oxyethylene) content averages 16– 30moles, average molecular weight (in amu), 1,500

Urea-formaldehyde copolymer, minimum average molecular weight (in 9011–05–6 amu), 30,000

Vinyl acetate-allyl acetate-monomethyl maleate copolymer, minimum None average molecular weight (in amu), 20,000

Vinyl acetate-ethylene copolymer, minimum number average molec- 24937–78–8 ular weight (in amu), 69,000

Vinyl acetate polymer with none and/or one or more of the following None monomers: Ethylene, propylene, N-methyl acrylamide, acrylamide, monoethyl maleate, diethyl maleate, monooctyl maleate, dioctyl ma- leate, maleic anhydride, maleic acid, octyl acrylate, butyl acrylate, ethyl acrylate, methyl acrylate, acrylic acid, octyl methacrylate, butyl methacrylate, ethyl methacrylate, methyl methacrylate, methacrylic acid, carboxyethyl acrylate, and diallyl phthalate; and their cor- responding sodium, potassium, ammonium, isopropylamine, triethylamine, monoethanolamine and/or triethanolamine salts; the resulting polymer having a minimum number average molecular weight (in amu), 1,200

Vinyl acetate-vinyl alcohol-alkyl lactone copolymer, minimum number None average molecular weight (in amu), 40,000; minimum viscosity of 18 centipoise

Vinyl alcohol-disodium itaconate copolymer, minimum average molec- None ular weight (in amu), 50,290

Vinyl alcohol-vinyl acetate copolymer, benzaldehyde-o-sodium None sulfonate condensate, minimum number average molecular weight (in amu), 20,000

Vinyl alcohol-vinyl acetate-monomethyl maleate, sodium salt-maleic None acid, disodium salt-g-butyrolactone acetic acid, sodium salt copoly- mer, minimum number average molecular weight (in amu), 20,000

Vinyl chloride-vinyl acetate copolymers None

Vinyl pyrrolidone-acrylic acid copolymer, minimum number average 28062–44–4 molecular weight (in amu), 6,000

Vinyl pyrrolidone-dimethylaminoethylmethacrylate copolymer, minimum 30581–59–0 number average molecular weight (in amu), 20,000

Vinyl pyrrolidone-styrene copolymer 25086–29–7

[67 FR 36528, May 24, 2002]

EDITORIAL NOTE: For FEDERAL REGISTER citations affecting § 180.960, see the List of CFR Sections Affected, which appears in the Finding Aids section of the printed volume and at www.fdsys.gov.

§ 180.1011 Viable spores of the micro- (1) The microorganism shall be an au- organism Bacillus thuringiensis thentic strain of Bacillus thuringiensis Berliner; exemption from the re- Berliner conforming to the morpho- quirement of a tolerance. logical and biochemical characteristics (a) For the purposes of this section of Bacillus thuringiensis as described in the microbial insecticide for which ex- Bergey’s Manual of Determinative Bac- teriology, Eighth Edition. emption from the requirement of a tol- (2) Spore preparations of Bacillus erance is being established shall have thuringiensis Berliner shall be produced the following specifications: by pure culture fermentation proce- dures with adequate control measures

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during production to detect any eggplant, okra, onion, pasture grass, changes from the characteristics of the pea (field and sweet), peanut, pepper, parent strain or contamination by potato, sweet potato, sorghum, soy- other microorganisms. bean, squash, tomato, turnip, and wa- (3) Each lot of spore preparation, termelon fields as part of the U.S. De- prior to the addition of other mate- partment of witchweed rials, shall be tested by subcutaneous control program. injection of at least 1 million spores [39 FR 33315, Sept. 17, 1974, as amended at 40 into each of five laboratory test mice FR 19477, May 5, 1975; 64 FR 31505, June 11, weighing 17 grams to 23 grams. Such 1999] test shall show no evidence of infection or injury in the test animals when ob- § 180.1017 Diatomaceous earth; exemp- served for 7 days following injection. tion from the requirement of a tol- (4) Spore preparations shall be free of erance. the Bacillus thuringiensis b-exotoxin (a) Diatomaceous earth is exempted when tested with the fly larvae tox- from the requirement of a tolerance for icity test (‘‘Microbial Control of In- residues when used in accordance with sects and Mites,’’ R.P.M. Bond et al., p. good agricultural practice in pesticide 280 ff., 1971). This specification can be formulations applied to growing crops, satisfied either by determining that to food commodities after harvest, and each master seed lot brought into pro- to animals. duction is a Bacillus thuringiensis strain (b) Diatomaceous earth may be safely which does not produce b-exotoxin used in accordance with the following under standard manufacturing condi- conditions. Application shall be lim- tions or by periodically determining ited solely to spot and/or crack and that b-exotoxin synthesized during crevice treatments in food or feed proc- spore production is eliminated by the essing and food or feed storage areas in subsequent spore-harvesting procedure. accordane with the precribed condi- (b) Exemption from the requirement tions: of a tolerance is established for resi- (1) It is used or intended for use for dues of the microbial insecticide Bacil- control of insects in food or feed proc- lus thuringiensis Berliner, as specified essing and food or feed storage areas: in paragraph (a) of this section, in or Provided, That the food or feed is re- on honey and honeycomb and all other moved or covered prior to such use. raw agricultural commodities when it (2) To assure safe use of the insecti- is applied either to growing crops, or cide, its label and labeling shall con- when it is applied after harvest in ac- form to that registered by the U.S. En- cordance with good agricultural prac- vironmental Protection Agency, and it tices. shall be used in accordance with such label and labeling. [36 FR 22540, Nov. 25, 1971, as amended at 38 FR 19045, July 17, 1973; 42 FR 28540, June 3, [65 FR 33716, May 24, 2000] 1977; 45 FR 43721, June 30, 1980; 45 FR 56347, Aug. 25, 1980; 74 FR 26533, June 3, 2009] § 180.1019 Sulfuric acid; exemption from the requirement of a toler- § 180.1016 Ethylene; exemption from ance. the requirement of a tolerance. (a) Residues of sulfuric acid are ex- Ethylene is exempted from the re- empted from the requirement of a tol- quirement of a tolerance for residues erance when used in accordance with when: good agricultural practice when used (a) For all food commodities, it is as a herbicide in the production of gar- used as a plant regulator on plants, lic and onions, and as a potato vine seeds, or cuttings and on all food com- dessicant in the production of potatoes. modities after harvest and when ap- (b) Residues of sulfuric acid are ex- plied in accordance with good agricul- empted from the requirement of a tol- tural practices. erance in cattle, meat; goat, meat; hog, (b) Injected into the soil to cause pre- meat; horse, meat; sheep, meat; poul- mature germination of witchweed in try, fat; poultry, meat; poultry, meat, bean (lima and string), cabbage, canta- byproducts; egg; milk; fish, shellfish, loupe, collard, corn, cotton, cucumber, and irrigated crops when it results

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from the use of sulfuric acid as an inert bodies of water in which fish or shell- ingredient in a pesticide product used fish are cultivated. in irrigation conveyance systems and (2) Basic copper carbonate (mala- lakes, ponds, reservoirs, or bodies of chite) as an algicide or herbicide in im- water in which fish or shellfish are cul- pounded and stagnant bodies of water tivated. The sulfuric acid is not to ex- (3) Copper triethanolamine and cop- ceed 10% of the pesticide formulation per monoethanolamine as an algicide (non-aerosol formulations only). or herbicide in fish hatcheries, lakes, [69 FR 40787, July 7, 2004, as amended at 74 ponds, and reservoirs FR 26533, June 3, 2009] (4) Cuprous oxide bearing antifouling coatings for control of algae or other § 180.1020 Sodium chlorate; exemption coatings for control of algae or other from the requirement of a toler- organisms on submerged concrete or ance. other (irrigation) structures. Sodium chlorate is exempted from (5) Copper oxide embedded in polymer the requirement of a tolerance for resi- emitter heads used in irrigation sys- dues when used as a defoliant or des- tems for root incursion prevention. iccant in accordance with good agricul- (b) The following copper compounds tural practice on the following crops: are exempt from the requirement of a Bean, dry, seed tolerance when applied (primarily) as a Corn, field, forage fungicide to growing crops using good Corn, field, grain agricultural practices: Corn, field, stover Corn, pop, grain Copper compounds CAS Reg. No. Corn, pop, stover Corn, sweet, forage Basic copper carbonate (mala- Corn, sweet, stover chite) ...... 1184–64–1 Copper complex ...... 16828–95–8 Cotton, undelinted seed Copper ethylenediamine complex 13426–91–0 Flax, seed Copper hydroxide ...... 20427–59–2 Grain, aspirated fractions Copper octanoate ...... 20543–04–8 Guar, seed Copper oxychloride ...... 1332–65–6 Pea, southern Copper oxychloride sulfate ...... 8012–69–9 Pepper, nonbell Copper salts of fatty and rosin Potato acids ...... 9007–39–0 Rice, grain Copper sulfate basic ...... 1344–73–6 Rice, straw Copper sulfate pentahydrate ...... 7758–99–8 Safflower, seed Cuprous oxide ...... 1317–19–1 Sorghum, forage, forage Sorghum, grain, forage (c) Copper sulfate pentahydrate (CAS Sorghum, grain, grain Reg. No. 7758–99–8) is exempt from the Sorghum, grain, stover requirement of a tolerance when ap- Soybean, forage plied as a fungicide to growing crops or Soybean, hay Soybean, seed to raw agricultural commodities after Sunflower, seed harvest, and as a bactericide/fungicide Wheat, grain in or on meat, fat and meat by-prod- ucts of cattle, sheep, hogs, goats, [74 FR 47457, Sept. 16, 2009] horses and poultry, milk and eggs when § 180.1021 Copper; exemption from the applied as a bactericide/fungicide to requirement of a tolerance. animal premises and bedding. (a) Copper is exempted from the re- (d) Copper (II) hydroxide (CAS Reg. quirement of a tolerance in cattle, No. 20427–59–2) is exempt from the re- meat; goat, meat; hog, meat; horse, quirement of a tolerance when applied meat; sheep, meat; milk, poultry, fat; to growing crops or to raw agricultural poultry, meat; poultry, meat byprod- commodities as an inert ingredient (for ucts; egg, fish, shellfish, and irrigated pH control) in pesticide products. crops when it results from the use of: [65 FR 68912, Nov. 15, 2000, as amended at 69 (1) Copper sulfate as an algicide or FR 4069, Jan. 28, 2004; 71 FR 46110, Aug. 11, herbicide in irrigation conveyance sys- 2006; 74 FR 26534, June 3, 2009; 74 FR 47457, tems and lakes, ponds, reservoirs, or Sept. 16, 2009; 80 FR 37551, July 1, 2015]

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§ 180.1022 Iodine-detergent complex; poultry litter, and storage areas for si- exemption from the requirement of lage and grain. a tolerance. (c) Preharvest and postharvest appli- The aqueous solution of hydriodic cation of propanoic acid (CAS Reg. No. acid and elemental iodine, including 79–09–4), propanioc acid, calcium salt one or both of the surfactants (a) (CAS Reg. No. 4075–81–4), and propanioc polyoxypropylene-polyoxyethylene gly- sodium salt (CAS Reg. No. 137–40–6) are col nomionic block polymers (min- exempted from the requirement of a imum average molecular weight 1,900) tolerance on all crops when used as ei- ther an active or inert ingredient in ac- and (b) a-(p- nonylphenyl)-omega- hydroxypoly (oxyethylene) having a cordance with good agricultural prac- tice in pesticide formulations applied maximum average molecular weight of to growing crops, to raw agricultural 748 and in which the nonyl group is a commodities before and after harvest propylene trimer isomer, is exempted and to animals. from the requirement of a tolerance for residues in egg, and poultry, fat; poul- [69 FR 47025, Aug. 4, 2004, as amended at 74 try, meat; poultry, meat byproducts FR 26534, June 3, 2009] when used as a sanitizer in poultry drinking water. § 180.1025 Xylene; exemption from the requirement of a tolerance. [74 FR 26534, June 3, 2009] Xylene is exempted from the require- ment of a tolerance when used as an § 180.1023 Propanoic acid; exemptions aquatic herbicide applied to irrigation from the requirement of a toler- conveyance systems in accordance with ance. the following conditions: (a) Postharvest application of pro- (a) It is to be used only in programs panoic acid or a mixture of methylene of the Bureau of Reclamation, U.S. De- bispropionate and oxy(bismethylene) partment of Interior, and cooperating bisproprionate when used as a fun- water user organizations. gicide is exempted from the require- (b) It is to be applied as an emulsion ment of a tolerance for residues in or at an initial concentration not to ex- on the following raw agricultural com- ceed 750 parts per million. modities: Alfalfa, forage; alfalfa, hay; (c) It is not to be applied when there alfalfa, seed; barley, grain; is any likelihood that the irrigation Bermudagrass, forage; Bermudagrass, water will be used as a source of raw hay; bluegrass, forage; bluegrass, hay; water for a potable water system or bromegrass, forage; bromegrass, hay; where return flows of such treated irri- clover, forage; clover, hay; corn, field, gation water into receiving rivers and grain; corn, pop, grain; cowpea, hay; streams would contain residues of xy- fescue, forage; fescue, hay; lespedeza, lene in excess of 10 parts per million. forage; lespedeza, hay; lupin; oat, (d) Xylene to be used as an aquatic grain; orchardgrass, forage; herbicide shall meet the requirement orchardgrass, hay; peanut, hay; pea, limiting the presence of a polynuclear field, hay; ryegrass, Italian, hay; sor- aromatic hydrocarbons as listed in 21 ghum, grain, grain; soybean, hay; CFR 172.250. sudangrass, forage; sudangrass, hay; [38 FR 16352, June 22, 1973, as amended at 50 timothy, forage; timothy, hay; vetch, FR 2980, Jan. 3, 1985] forage; vetch, hay; and wheat, grain. (b) Propanoic acid is exempt from the § 180.1027 Nuclear polyhedrosis virus requirement of a tolerance for residues of Heliothis zea; exemption from in or on cattle, meat; cattle, meat by- the requirement of a tolerance. products; goat, meat; goat, meat by- (a) For the purposes of this section, products; hog, meat; hog meat byprod- the viral insecticide must be produced ucts; horse, meat; horse, meat byprod- with an unaltered and unadulterated ucts; sheep, meat; sheep meat byprod- inoculum of the single-embedded ucts; and, poultry, fat; poultry meat; Heliothis zea nuclear polyhedrosis virus poultry meat byproducts; milk, and (HzSNPV). The identity of the seed egg when applied as a bactericide/fun- virus must be assured by periodic gicide to livestock drinking water, checks.

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(b) Each lot of active ingredient of hexaadecenal to disrupt the mating of the viral insecticide shall have the fol- the artichoke plume moth. lowing specifications: [74 FR 26534, June 3, 2009] (1) The level of extraneous bacterial contamination of the final § 180.1040 Ethylene glycol; exemption unformulated viral insecticide should from the requirement of a toler- not exceed 107 colonies per gram as de- ance. termined by an aerobic plate on Ethylene glycol as a component of trypticase soy agar. pesticide formulations is exempt from (2) Human pathogens, e.g., Sal- the requirement of a tolerance when monella, Shigella, or Vibrio, must be used in foliar applications to peanut absent. plants. (3) Safety to mice as determined by an intraperitoneal injection study [43 FR 41393, Sept. 18, 1978] must be demonstrated. (4) Identity of the viral product, as § 180.1041 Nosema locustae; exemption from the requirement of a toler- determined by the most sensitive and ance. standardized analytical technique, e.g., restriction endonuclease and/or SDS- The insecticide Nosema locustae is ex- PAGE analysis, must be demonstrated. empted from the requirement of a tol- (c) Exemptions from the requirement erance for residues in or on all raw ag- of a tolerance are established for the ricultural commodities. residues of the microbial insecticide [47 FR 21537, May 19, 1982] Heliothis zea NPV, as specified in para- graphs (a) and (b) of this section, in or § 180.1043 Gossyplure; exemption from on all agricultural commodities. the requirement of a tolerance. [60 FR 42460, Aug. 16, 1995, as amended at 74 The pheromone gossyplure, a 1:1 mix- FR 26534, June 3, 2009] ture of (Z,Z)- and (Z,E)-7,11- hexadecadien-1-ol acetate) is exempt § 180.1033 Methoprene; exemption from the requirement of a tolerance in from the requirement of a toler- or on the raw agricultural commodity ance. cotton, undelinted seed when applied to Methoprene is exempt from the re- cotton from capillary fibers. quirement of a tolerance in or on all [74 FR 26534, June 3, 2009] food commodities when used to control insect larvae. § 180.1049 Carbon dioxide; exemption [68 FR 34829, June 11, 2003] from the requirement of a toler- ance. § 180.1037 Polybutenes; exemption The insecticide carbon dioxide is ex- from the requirement of a toler- empted from the requirement of a tol- ance. erance when used after harvest in (a) Polybutenes are exempt from the modified atmospheres for stored insect requirement of a tolerance for residues control on food commodities. in or on the raw agricultural com- modity cotton, undelinted seed when [65 FR 33716, May 24, 2000] used as a sticker agent for formula- § 180.1050 Nitrogen; exemption from tions of the attractant gossyplure (1:1 the requirements of a tolerance. mixture of (Z,Z)- and (Z,E)-7,11- hexadecadien-1-ol acetate) to disrupt The insecticide nitrogen is exempted the mating of the pink bollworm. from the requirements of a tolerance (b) Polybutenes are exempt from the when used after harvest in modified requirement of a tolerance for residues atmospheres for stored product insect in or on the raw agricultural com- control on all food commodities. modity artichoke when used as a stick- [65 FR 33716, May 24, 2000] er agent in multi-layered laminted controlled-release dispensers of (Z)-11-

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§ 180.1052 2,2,5-trimethyl-3-dichloro- § 180.1058 Sodium diacetate; exemp- acetyl-1,3-oxazolidine; exemption tion from the requirement of a tol- from the requirement of a toler- erance. ance. Sodium diacetate, when used 2,2,5-trimethyl-3-dichloroacetyl-1,3- postharvest as a fungicide, is exempt oxazolidine is exempted from the re- from the requirement of a tolerance for quirement of a tolerance when used as residues in or on alfalfa, hay; an inert ingredient in formulations of the herbicides S-ethyl Bermudagrass, hay; bluegrass, hay; dipropylthiocarbamate, S-propyl bromegrass, hay; clover,hay; corm, dipropylthiocarbamate, and S-ethyl field, grain; corn, pop, grain; oat, grain; diisobutylthiocarbamate applied to orchardgrass, hay; sorghum, grain, corn fields before the corn plants grain; sudangrass, hay; ryegrass, emerge from the soil with a maximum Italian, hay; timothy, hay. of 0.5 pound of the inert ingredient per [74 FR 26534, June 3, 2009] acre. [45 FR 51201, Aug. 1, 1980] § 180.1064 Tomato pinworm insect pheromone; exemption from the re- § 180.1054 Calcium hypochlorite; ex- quirement of a tolerance. emptions from the requirement of a tolerance. An exemption from the requirement of a tolerance is established for com- (a) Calcium hypochlorite is exempted bined residues of both components of from the requirement of a tolerance the tomato pinworm insect pheromone when used preharvest or postharvest in (E)-4-tridecen-1-yl acetate and (Z)-4- solution on all raw agricultural com- modities. tridecen-1-yl acetate in or on all raw (b) Calcium hypochlorite is exempted agricultural commodities (preharvest) from the requirement of a tolerance in in accordance with the following pre- or on grape when used as a fumigant scribed conditions: postharvest by means of a chlorine (a) Application shall be limited sole- generator pad. ly to point source dispensers or point source chopped fibers containing the [59 FR 59165, Nov. 16, 1994, as amended at 74 FR 26534, June 3, 2009] tomato pinworm insect pheromone. (b) Cumulative yearly application § 180.1056 Boiled linseed oil; exemp- cannot exceed 200 grams of tomato tion from requirement of tolerance. pinworm pheromone per acre. Boiled linseed oil (containing no [58 FR 34376, June 25, 1993] more than 0.33 percent manganese naphthenate and no more than 0.33 per- § 180.1065 2-Amino-4,5-dihydro-6-meth- cent cobalt naphthenate) is exempt yl-4-propyl-s-triazolo(1,5- from the requirement of a tolerance alpha)pyrimidin-5-one; exemption when used as a coating agent for S- from the requirement of a toler- ethyl hexahydro-1H-azepine-1- ance. carbothioate. No more than 15 percent The inert ingredient, 2-amino-4,5- of the pesticide formulation may con- dihydro-6-methyl-4-propyl-s- sist of ‘‘boiled linseed oil.’’ This exemp- tion is limited to use on rice before edi- triazolo(1,5-alpha)pyrimidin-5-one is ble parts form. exempted from the requirement of a tolerance when used as an emetic at [46 FR 33270, June 29, 1981] not more than 0.3 percent in formula- tions of paraquat dichloride. Further § 180.1057 Phytophthora palmivora; exemption from requirement of tol- restrictions on this exemption are that erance. this ingredient may not be advertised Phytophthora palmivora is exempted as an emetic and the paraquat product from the requirement of a tolerance in may not be promoted in any way be- or on the raw agricultural commodity cause of the inclusion of this inert in- fruit, citrus. gredient. [74 FR 26534, June 3, 2009] [70 FR 46431, Aug. 10, 2005]

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§ 180.1067 Methyl eugenol and mala- § 180.1070 Sodium chlorite; exemption thion combination; exemption from from the requirement of a toler- the requirement of a tolerance. ance. The insect attractant methyl eugenol Sodium chlorite is exempted from and the insecticide malathion are ex- the requirement of a tolerance for resi- empt from the requirement of toler- dues when used in accordance with ances on all raw agricultural commod- good agricultural practice as a seed- ities when used in combination in Ori- soak treatment in the growing of the ental fruit fly eradication programs raw agricultural commodities vege- under the authority of the U.S. Depart- table, brassica, leafy, group 5 and rad- ment of Agriculture, in accordance ish, roots and radish, tops. with the following directions and speci- [74 FR 26534, June 3, 2009] fications: (a) The combination shall be at the § 180.1071 Peanuts, Tree Nuts, Milk, ratio of three parts methyl eugenol to Soybeans, Eggs, Fish, Crustacea, one part technical malathion (3:1). and Wheat; exemption from the re- quirement of a tolerance. (b) This combination is to be impreg- nated on a carrier (cigarette filter tips (a) General. Residues resulting from (cellulose acetate); cotton strings; fi- the following uses of the food com- berboard squares) or mixed with a jel modity forms of peanuts, tree nuts, cleared under 40 CFR 180.920 or 180.950. milk, soybeans, eggs (including putres- (c) The maximum actual dosage per cent eggs), fish, crustacea, and wheat application per acre shall be 28.35 are exempted from the requirement of grams (one ounce avoirdupois) methyl a tolerance in or on all food commod- ities under FFDCA section 408 (when eugenol and 9.45 grams (one-third (0.33) used as either an inert or an active in- ounce avoirdupois) technical mala- gredient in a pesticide formulation), if thion. such use is in accordance with good ag- [47 FR 9002, Mar. 3, 1982, as amended at 69 FR ricultural practices: 23142, Apr. 28, 2004] (1) Use in pesticide products intended to treat seeds. § 180.1068 C 12-C 18 fatty acid potassium (2) Use in nursery and greenhouse op- salts; exemption from the require- erations, as defined in 40 CFR 170.3, ment of a tolerance. which includes seeding, potting and C12-C18 fatty acids (saturated and un- transplanting activities. saturated) potassium salts are exempt- (3) Pre-plant and at-transplant appli- ed from the requirement of a tolerance cations. for residues in or on all raw agricul- (4) Incorporation into seedling and tural commodities when used in ac- planting beds. cordance with good agricultural prac- (5) Applications to cuttings and bare tice. roots. [60 FR 34871, July 5, 1995] (6) Applications to the field that occur after the harvested crop has been § 180.1069 (Z)-11-Hexadecenal; exemp- removed. tion from the requirement of a tol- (7) Soil-directed applications around erance. and adjacent to all plants. An exemption from the requirement (8) Applications to rangelands, which of a tolerance is established for resi- is land, mostly grasslands, whose dues of the biological insecticide plants can provide food (i.e., forage) for grazing or browsing animals. (pheromone) (Z)-11-hexadecenal when used as a sex attractant on artichoke (9) Use in chemigation and irrigation plants to control the artichoke plume systems (via flood, drip, or furrow ap- plication with no overhead spray appli- moth. cations). [47 FR 14906, Apr. 7, 1982] (10) Application as part of a dry fer- tilizer on which an active ingredient is impregnated.

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(11) Aerial and ground applications tolerance in or on all the raw agricul- that occur when no above-ground har- tural commodities (food and feed) in- vestable food commodities are present cluding, peach; quince; nectarine; and (usually pre-bloom). nut, macadamia when used in orchards (12) Application as part of an animal with encapsulated polyethylene tubing feed-through product. to control oriental fruit moth. (13) Applications as gel and solid (non-liquid/non-spray) crack and crev- [74 FR 26534, June 3, 2009] ice treatments that place the gel or § 180.1074 F.D.&C. Blue No. 1; exemp- bait directly into or on top of the tion from the requirement of a tol- cracks and crevices via a mechanism erance. such as a syringe. F.D.&C. Blue No. 1 is exempted from (14) Applications to the same crop the requirement of a tolerance when from which the food commodity is de- used as an aquatic plant control agent. rived, whether the plant fraction(s) in- tended for harvest are present or not, [47 FR 25963, June 16, 1982] e.g., applications of peanut meal when applied to peanut plants. § 180.1075 Colletotrichum (b) Specific chemical substances. Resi- gloeosporioides f. sp. aeschynomene; dues resulting from the use of the fol- exemption from the requirement of a tolerance. lowing substances as either an inert or an active ingredient in a pesticide for- An exemption from the requirement mulation are exempted from the re- of a tolerance is established for resi- quirement of a tolerance under FFDCA dues of the mycoherbicide section 408, if such use is in accordance Colletotrichum gloeosporioides f. sp. with good agricultural practices and aeschynomene in or on the following such use is included in paragraph (a): raw agricultural commodities:

Chemical Substance CAS No. COMMODITY

Caseins ...... 9000–71–9 Aspirated grain fractions Caseins, ammonium complexes ...... 9005–42–9 Rice, grain Caseins, hydrolyzates ...... 65072–00–6 Soybean, forage Caseins, potassium complexes ...... 68131–54–4 Soybean, hay Caseins, sodium complexes ...... 9005–46–3 Soybean, seed [47 FR 25742, June 15, 1982, as amended at 74 [70 FR 1360, Jan. 7, 2005] FR 26534, June 3, 2009]

§ 180.1072 Poly-D-glucosamine § 180.1076 Viable spores of the micro- (chitosan); exemption from the re- organism Bacillus popilliae; exemp- quirement of a tolerance. tion from the requirement of a tol- (a) An exemption from the require- erance. ment of a tolerance is established for (a) For the purposes of this section residues of the biological plant growth the microbial insecticide for which ex- regulator poly-D-glucosamine when emption from the requirement of a tol- used as a seed treatment in or on bar- erance is being established shall have ley, beans, oats, peas, rice, and wheat. the following specifications: (b) An exemption from the require- (1) The microorganism shall be an au- ment of a tolerance is established for thentic strain of Bacillus popilliae con- residues of the biological plant growth forming to the morphological and bio- regulator poly-D-glucosamine when chemical characteristics of Bacillus used as a pesticide in the production popilliae as described in Bergey’s Man- any raw agricultural commodity. ual of Determinative Bacteriology, [60 FR 19524, Apr. 19, 1995] Eighth Edition. (2) Spore preparations of Bacillus § 180.1073 Isomate-M; exemption from popilliae shall be produced by an ex- the requirement of a tolerance. traction process from diseased Japa- The oriental fruit moth pheromone nese beetles, and may contain a small (Isomate-M) (Z-8-dodecen-l-yl acetate, percentage of the naturally occurring E-8-dodecen-l-yl acetate, Z-8-dodecen-l- milky disease bacterium Bacillus ol) is exempt from the requirement of a lentimorbus.

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(3) Each lot of spore preparation, Pea, dry, seed prior to the addition of other mate- Pea, succulent rials, shall be tested by subcutaneous [48 FR 54819, Dec. 7, 1983, as amended at 74 injection of at least 1 million spores FR 26535, June 3, 2009] into each of five laboratory test mice weighing 17 grams to 23 grams. Such § 180.1084 Monocarbamide dihydrogen test shall show no evidence of infection sulfate; exemption from the require- ment of a tolerance. of injury in the test animals when ob- served for 7 days following injection. Monocarbamide dihydrogen sulfate is (b) Exemption from the requirement exempted from the requirement of a of a tolerance is established for resi- tolerance when used as a herbicide or dues of the microbial insecticide Bacil- desiccant in or on all raw agricultural lus popilliae, as specified in paragraph commodities. (a) of this section in or on grass, pas- [53 FR 12152, Apr. 13, 1988] ture, forage and grass, rangeland, for- age when it is applied to growing crops § 180.1086 3,7,11-Trimethyl-1,6,10- in accordance with good agricultural dodecatriene-1-ol and 3,7,11- practices. trimethyl-2,6,10-dodecatriene-3-ol; exemption from the requirement of [47 FR 38535, Sept. 1, 1982, as amended at 74 a tolerance. FR 26535, June 3, 2009] The insect pheromone containing the active ingredients 3,7,11-trimethyl- § 180.1080 Plant volatiles and 1,6,10-dodecatriene-1-ol and 3,7,11- pheromone; exemptions from the trimethyl-2,6,10-dodecatriene-3-ol is ex- requirement of a tolerance. empted from the requirement of a tol- An exemption from the requirement erance in or on all raw agricultural of a tolerance is established for resi- commodities. dues of the plant volatiles cyclic decadiene, cyclic decene, cyclic [52 FR 12165, Apr. 15, 1987; 52 FR 29014, Aug. 5, 1987] pentadecatriene, and decatriene and the pheromone Z-2-isopropenyl-1- § 180.1087 Sesame stalks; exemption methylcyclobutaneethanol; Z-3,3-di- from the requirement of a toler- methyl-D1,b-cyclohexaneethanol; Z-3,3- ance. dimethyl-D1,a-cyclohexaneethanal; E- An exemption from the requirement 3,3-dimethyl-D1,a-cyclohexaneethanal of a tolerance is established for resi- combination when applied to cotton in dues of the biorational nematicide ses- hollow synthetic fibers. ame stalk in or on the following raw [48 FR 28442, June 22, 1983] agricultural commodities: Almond; al- mond, hulls; cotton, undelinted seed; § 180.1083 Dimethyl sulfoxide; exemp- cotton, gin byproducts; soybean, seed; tion from the requirement of a tol- soybean, forage; soybean, hay; aspi- erance. rated grain fractions; potato; beet, Dimethyl sulfoxide (DMSO) [CAS sugar, roots; beet, sugar, tops; tomato; Registry Number 67–68–5] is exempted pepper, bell; squash; strawberry; egg- from the requirement of a tolerance plant; cucumber; carrot, roots; radish, when used as an inert solvent or cosol- roots; radish, top; turnip, roots; turnip, vent in formulations with the following tops; onion; pea, dry; pea, succulent; pesticides when used in accordance melon; grape; walnut; orange; grape- with good agricultural practices in or fruit; mulberry; peach; apple; apricot; on the following raw agricultural com- blackberry; loganberry; pecan; cherry; modities: plum, and cranberry. (a) Carbaryl (1-naphthyl methyl-car- [74 FR 26535, June 3, 2009] bamate) § 180.1089 Poly-N-acetyl-D-glu- Pea, dry, seed cosamine; exemption from the re- Pea, succulent quirement of tolerance. (b) O-O-Diethyl O-(2-isopropyl-6- An exemption from the requirement methyl-4-pyrimidinyl) of a tolerance is established for resi- phosphorothioate dues of the biochemical nematicide

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poly-N-acetyl-D-glucosamine on a vari- from the requirement of a tolerance in ety of agricultural crops. or on the raw agricultural commodity grape when used in orchards with en- [53 FR 10249, Mar. 30, 1988] capsulated polyethylene tubing to con- § 180.1090 Lactic acid; exemption from trol grape berry moth. the requirement of a tolerance. [74 FR 26535, June 3, 2009] Lactic acid (2-hydroxypropanoic acid) is exempted from the requirement § 180.1098 Gibberellins [Gibberellic Acids (GA3 and GA4 + GA7), and So- of a tolerance when used as a plant dium or Potassium Gibberellate]; growth regulator in or on all raw agri- exemption from the requirement of cultural commodities. a tolerance. [53 FR 15286, May 4, 1988] An exemption from the requirement of a tolerance is established for resi- § 180.1091 Aluminum isopropoxide and dues of gibberellins [gibberellic acids aluminum secondary butoxide; ex- (GA3 and GA4 + GA7), and sodium or emption from the requirement of a potassium gibberellate] in or on all tolerance. food commodities when used as plant Aluminum isopropoxide (CAS Reg. regulators on plants, seeds, or cuttings No. 555–31–7) and aluminum secondary and on all food commodities after har- butoxide (CAS Reg. No. 2269–22–9) are vest in accordance with good agricul- exempted from the requirement of a tural practices. tolerance when used in accordance [64 FR 31505, June 11, 1999] with good agricultural practices as sta- bilizers in formulations of the insecti- § 180.1100 Gliocladium virens isolate cide amitraz [N′-(2,4-dimethylphenyl)- GL-21; exemption from the require- N-[[(2,4-dimethylphenyl)imino]-N- ment of a tolerance. methylmethanimidamide] applied to An exemption from the requirement growing crops or animals. of a tolerance is established for resi- [53 FR 34509, Sept. 7, 1988; 53 FR 36696, Sept. dues of the biofungicide Gliocladium 21, 1988] virens GL-21 in or on all raw agricul- tural commodities when used either as § 180.1092 Menthol; exemption from a fungicide for inoculation of plant the requirement of a tolerance. growth media in greenhouses or on ter- An exemption from the requirement restrial food crops grown outdoors in of a tolerance is established for resi- accordance with good agricultural dues of the pesticidal chemical men- practices. thol in or on honey and honeycomb [60 FR 48659, Sept. 20, 1995; 60 FR 52248, Oct. when used in accordance with good ag- 5, 1995] ricultural practice in over-wintering bee hives. § 180.1101 Parasitic (parasitoid) and predatory insects; exemption from [74 FR 26535, June 3, 2009] the requirement of a tolerance. § 180.1095 Chlorine gas; exemptions Parasitic (parasitoid) and predatory from the requirement of a toler- insects are exempted from the require- ance. ment of a tolerance for residues when Chlorine gas is exempted from the re- they are used in accordance with good agricultural and practices quirement of a tolerance when used to control insect pests of stored raw preharvest or postharvest in solution whole grains such as corn, small on all raw agricultural commodities. grains, rice, soybeans, peanuts, and [56 FR 21309, May 8, 1991] other legumes either bulk or warehoused in bags. For the purposes § 180.1097 GBM-ROPE; exemption from of this rule, the parasites (parasitoids) the requirement of a tolerance. and predators are considered to be spe- The grape berry moth pheromone cies of Hymenoptera in the genera (GBM-ROPE) containing the active in- Trichogramma, Trichogrammatidae; gredients (Z)-9-dedecenyl acetate and Bracon, Braconidae; Venturia, (Z)-11-tetradecenyl acetate is exempt Mesostenus, Ichneumonidae;

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Anisopteromalus, Choetospila, fluorescens is exempt from the require- Lariophagus, Dibrachys, Habrocytus, ments of a tolerance in or on all raw Pteromalus, Pteromalidae; agricultural commodities. Cephalonomia, Holepyris, Laelius, [56 FR 28326, June 20, 1991] Bethylidae; and of Hemiptera in the genera Xylocoris, Lyctocoris, and § 180.1110 3-Carbamyl-2,4,5-trichloro- Dufouriellus, Anthocoridae. Whole in- benzoic acid; exemption from the sects, fragments, parts, and other resi- requirement of a tolerance. dues of these parasites and predators An exemption from the requirement remain subject to 21 U.S.C. 342(a)(3). of a tolerance is established for the res- [57 FR 14646, Apr. 22, 1992] idues of 3-carbamyl-2,4,5- trichlorobenzoic acid in or on all raw § 180.1102 Trichoderma harzianum agricultural commodities which occur KRL-AG2 (ATCC #20847) strain T– from the direct application of 22; exemption from requirement of chlorothalonil to crops in § 180.275 (a) a tolerance. and (b) and/or as an inadvertent residue An exemption from the requirement resulting from the soil of of a tolerance is established for resi- chlorothalonil when applied to crops in dues of the biofungicide Trichoderma § 180.275 (a) and (b), and subsequent up- harzianum KRL-AG2 (ATCC #20847); take by rotated crops when used ac- also known as strain T-22 when applied cording to approved agricultural prac- in/or on all food commodities. tices. [64 FR 16860, Apr. 7, 1999] [57 FR 24552, June 10, 1992]

§ 180.1103 Isomate-C; exemption from § 180.1111 Bacillus subtilis GB03; ex- the requirement of a tolerance. emption from the requirement of a The codling moth pheromone tolerance. (Isomate-C) E,E-8,10-dodecenyl alcohol, The biofungicide Bacillus subtilis GB03 dodecanol, tetradecanol is exempt from is exempted from the requirement of a the requirements of a tolerance in or tolerance in or on all raw agricultural on all raw agricultural commodities commodities when used in accordance when formulated in polyethylene with good agricultural practices. pheromone dispensers for use in or- [73 FR 50556, Aug. 27, 2008] chards with encapsulated polyethylene tubing to control codling moth. § 180.1113 Lagenidium giganteum; ex- emption from the requirement of a [74 FR 26535, June 3, 2009] tolerance. § 180.1107 Delta endotoxin of Bacillus Lagenidium giganteum (a fungal orga- thuringiensis variety kurstaki en- nism) is exempt from the requirement capsulated into killed Pseudomonas of a tolerance in or on the raw agricul- fluorescens; exemption from the re- tural commodities aspirated grain frac- quirement of a tolerance. tions; grass, forage; grass, hay; rice, The delta endotoxin of Bacillus grain; rice, straw; soybean, seed; soy- thuringiensis variety kurstaki encap- bean, forage; soybean, hay; rice, wild, sulated into killed Pseudomonas grain. fluorescens is exempt from the require- [74 FR 26535, June 3, 2009] ments of a tolerance in or on all raw agricultural commodities. § 180.1114 Pseudomonas fluorescens [56 FR 28328, June 20, 1991] A506, Pseudomonas fluorescens 1629RS, and Pseudomonas syringae § 180.1108 Delta endotoxin of Bacillus 742RS; exemptions from the re- thuringiensis variety San Diego en- quirement of a tolerance. capsulated into killed Pseudomonas The biological pesticides fluorescens; exemption from the re- Pseudomonas fluorescens A506, quirement of a tolerance. Pseudomonas fluorescens 1629RS, and The delta endotoxin of Bacillus Pseudomonas syringae 742RS are ex- thuringiensis variety San Diego encap- empted from the requirement of a tol- sulated into killed Pseudomonas erance in or on all raw agricultural

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commodities when applied as a frost modities when used as an active ingre- protection agent or biological control dient in , herbicides, or fun- agent to growing agricultural crops in gicides preharvest or postharvest in ac- accordance with good agricultural cordance with good agricultural prac- practices. tices. [57 FR 42700, Sept. 16, 1992] [58 FR 44283, Aug. 20, 1993]

§ 180.1118 Spodoptera exigua nuclear § 180.1122 Inert ingredients of polyhedrosis virus; exemption from semiochemical dispensers; exemp- the requirement of a tolerance. tions from the requirement of a tol- An exemption from the requirement erance. of a tolerance is established for the mi- (a) All inert ingredients of crobial pest control agent Spodoptera semiochemical dispenser products for- exigua nuclear polyhedrosis virus when mulated with, and/or contained in, dis- used as a pesticide control agent on all pensers made of polymeric matrix ma- raw agricultural commodities. terials (including the monomers, plas- [58 FR 25784, Apr. 28, 1993] ticizers, dispersing agents, anti- oxidants, UV protectants, stabilizers, § 180.1119 Azadirachtin; exemption and other inert ingredients) are ex- from the requirement of a toler- ance. empted from the requirement of a tol- erance when used as carriers in pes- An exemption from the requirement ticide formulations for application to of a tolerance is established for the bio- growing crops only. These dispensers chemical azadirachtin, which is iso- shall conform to the following speci- lated from the berries of the Neem tree fications: (Azadirachta indica), when used as a pesticide at 20 grams or less per acre on (1) Exposure must be limited to inad- all raw agricultural commodities. vertent physical contact only. The de- sign of the dispenser must be such as to [58 FR 8696, Feb. 17, 1993] preclude any contamination by its components of the raw agricultural § 180.1120 Streptomyces sp. strain K61; exemption from the requirement of commodity (RAC) or processed foods/ a tolerance. feeds derived from the commodity by virtue of its proximity to the RAC or The biological pesticide Streptomyces as a result of its physical size. sp. strain K61 is exempted from the re- quirement of a tolerance in or on all (2) The dispensers must be applied raw agricultural commodities when discretely. This exemption does not used as a fungicide for the treatment of apply to components of semiochemical seeds, cuttings, transplants, and plants formulations applied in a broadcast of agricultural crops in accordance manner either to a crop field plot or to with good agricultural practices. individual plants. (b) A semiochemical dispenser is a [58 FR 21403, Apr. 21, 1993] single enclosed or semi-enclosed unit § 180.1121 Boric acid and its salts, that releases semiochemical(s) into the borax (sodium borate decahydrate), surrounding atmosphere via volatiliza- disodium octaborate tetrahydrate, tion and is applied in a manner to pro- boric oxide (boric anhydride), so- vide discrete application of the dium borate and sodium metabo- semiochemical(s) into the environ- rate; exemptions from the require- ment. ment of a tolerance. (c) Semiochemicals are chemicals An exemption from the requirement that are emitted by plants or animals of a tolerance is established for resi- and modify the behavior of receiving dues of the pesticidal chemical boric organisms. These chemicals must be acid and its salts, borax (sodium borate naturally occurring or substantially decahydrate), disodium octaborate tet- identical to naturally occurring rahydrate, boric oxide (boric anhy- semiochemicals. dride), sodium borate and sodium met- aborate, in or on raw agricultural com- [58 FR 64494, Dec. 8, 1993]

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§ 180.1124 Arthropod pheromones; ex- § 180.1127 Biochemical pesticide plant emption from the requirement of a floral volatile attractant com- tolerance. pounds: cinnamaldehyde, cinnamyl Arthropod pheromones, as described alcohol, 4-methoxy cinnamaldehyde, 3-phenyl propanol, 4-methoxy in § 152.25(b) of this chapter, when used phenethyl alcohol, indole, and 1,2,4- in retrievably sized polymeric matrix trimethoxybenzene; exemptions dispensers are exempt from the re- from the requirement of a toler- quirement of a tolerance in or on all ance. raw agricultural commodities when ap- Residues of the biochemical pesticide plied to growing crops only at a rate plant floral volatile attractant com- not to exceed 150 grams active ingre- pounds: cinnamaldehyde, cinnamyl al- dient/acre/year in accordance with good agricultural practices. cohol, 4-methoxy cinnamaldehyde, 3- phenyl propanol, 4-methoxy phenethyl [59 FR 14759, Mar. 30, 1994] alcohol, indole, and 1,2,4- trimethoxybenzene are exempt from § 180.1126 Codlure, (E,E)-8,10- the requirement of a tolerance in or on Dodecadien-1-ol; exemption from the following raw agricultural com- the requirement of a tolerance. modities: the following field crops—al- An exemption from the requirement falfa, clover, cotton, dandelion, pea- of a tolerance is established for the in- nuts (including hay), rice, sorghum sect pheromone codlure, (E,E)-8,10- (milo), soybeans, sunflower, sweet po- dodecadien-1-ol, on all raw agricultural tatoes, and wheat; the following vege- commodities in accordance with the table crops—asparagus, beans (includ- following prescribed conditions: ing forage hay), beets, carrots, celery, (a) Application shall be limited sole- cole crops (cabbage, broccoli, brussels ly to codlure dispensers that conform sprouts, cauliflower), collards (kale, to the following specifications: mustard greens, turnip greens, kohl- (1) Commodity exposure must be lim- rabi), corn, fresh (field, sweet, pop, ited to inadvertent physical contact. seed), corn fodder and forage, chinese The design of the dispenser must be cabbage, cowpeas, cucurbitis (cucum- such as to preclude any exposure of its bers, squash, pumpkin), egg plant, en- components to the raw agricultural dive (escarole), horseradish (radish, ru- commodity (RAC) or processed foods/ tabagas, turnip roots), leafy greens feeds derived from the commodity due (spinach, swiss chard), lettuce (head to its proximity to the RAC or as a re- leaf), okra, parsley, parsnip, peas, peas sult of its physical size. Dispensers with pods, peppers, potatoes, sugar must be of such size and construction that they are readily recognized post- beets, tomatoes; the following tree application. fruit, berry and nut crops—almonds, apples, apricots, berries (blackberry, (2) The dispensers must be applied discretely, i.e., placed in the field in boysenberry, dewberry, loganberry, easily perceived distinct locations in a raspberry), blueberry, cherry, citrus manner that does not prevent later re- (grapefruit, kumquat, lemon, lime, or- trieval. This exemption does not apply ange, tangelo, and tangerine) cran- to codlure applied in a broadcast man- berry, grapes, melons, (watermelon, ner either to a crop field plot or to in- honeydew, crenshaw, cantaloupe, ca- dividual plants. saba, persian), nectarines, pears, pe- (b) A codlure dispenser is a single en- cans, peaches, and strawberry as dis- closed or semi-enclosed unit that re- persed from the end-use product Corn ® leases codlure into the surrounding at- Rootworm Bait , a pesticidal bait, in mosphere via volatilization and is ap- accordance with the prescribed condi- plied in a manner to provide discrete tions in paragraph (a) of this section. application (i.e., in easily perceived dis- (a) Cumulative yearly application tinct locations in a manner that does cannot exceed 20 grams of each floral not prevent later retrieval) of the attractant/acre/application. codlure into the environment. (b) [Reserved] [59 FR 9931, Mar. 2, 1994] [59 FR 15857, Apr. 5, 1994]

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§ 180.1128 Bacillus subtilis MBI 600; § 180.1139 Sodium 5-nitroguaiacolate; exemption from the requirement of exemption from the requirement of a tolerance. a tolerance. An exemption from the requirement The biochemical sodium 5- of a tolerance is established for resi- nitroguiacolate is exempted from the dues of the biofungicide Bacillus subtilis requirement of a tolerance when used MBI 600 in or on all food commodities, as a plant growth regulator in end-use including residues resulting from post- products at a concentration of 0.1% by harvest uses, when applied or used in weight and applied at an application accordance with good agricultural rate of 20 g of a.i. per acre or less per practices. application, in or on all food commod- ities. [74 FR 15869, Apr. 8, 2009] [65 FR 66181, Nov. 3, 2000] § 180.1130 N-(n-octyl)-2-pyrrolidone and N-(n-dodecyl)-2-pyrrolidone; ex- § 180.1140 Sodium o-nitrophenolate; emptions from the requirement of a exemption from the requirement of tolerance. a tolerance. (a) N-(n-octyl)-2-pyrrolidone and N- The biochemical sodium o- (n-dodecyl)-2-pyrrolidone are exempt nitrophenolate is exempted from the from the requirement of a tolerance requirement of a tolerance when used when used as solvents in cotton defo- as a plant growth regulator in end-use liant formulations containing products at a concentration of 0.2% by thidiazuron and diuron as active ingre- weight and applied at an application dients. rate of 20 g of a.i. per acre or less per (b) N-(n-octyl)-2-pyrrolidone is ex- application, in or on all food commod- empt from the requirement of a toler- ities. ance when used as a solvent in formu- lations containing pyraflufen-ethyl as [65 FR 66181, Nov. 3, 2000] an active ingredient at a concentration § 180.1141 Sodium p-nitrophenolate; not to exceed 20% by weight. exemption from the requirement of [79 FR 10682, Feb. 26, 2014] a tolerance. The biochemical sodium p- § 180.1131 Ampelomyces quisqualis iso- nitrophenolate is exempted from the late M10; exemption from the re- requirement of a tolerance when used quirement of a tolerance. as a plant growth regulator in end-use The biological fungicide Ampelomyces product at a concentration of 0.3% by quisqualis isolate M10 is exempted from weight and applied at an application the requirement of a tolerance in or on rate of 20 g of a.i. per acre or less per all raw agricultural commodities when application, in or on all food commod- used as a fungicide on agricultural ities. crops in accordance with good agricul- tural practices. [65 FR 66181, Nov. 3, 2000] [59 FR 33437, June 29, 1994] § 180.1142 1,4-Dimethylnaphthalene; exemption from the requirement of § 180.1135 Pasteuria penetrans; exemp- a tolerance. tion from the requirement of a tol- erance. An exemption from the requirement of a tolerance is established for the res- The biological nematicide Pasteuria idues of the plant growth regulator, penetrans is exempted from the require- 1,4-dimethylnaphthalene (1,4-DMN), ment of a tolerance in or on all raw ag- when applied postharvest to all sprout- ricultural commodities, except roots ing root, tuber, and bulb crops in ac- and tubers, when used as a nematicide cordance with good agricultural prac- in the production of fruits and vegeta- tices. bles in greenhouses. [77 FR 68697, Nov. 16, 2012] [59 FR 66741, Dec. 28, 1994]

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§ 180.1143 Methyl anthranilate; exemp- § 180.1149 Inclusion bodies of the tion from the requirement of a tol- multi-nuclear polyhedrosis virus of erance. Anagrapha falcifera; exemption Residues of methyl anthranilate, a from the requirement of a toler- ance. biochemical pesticide, are exempt from the requirement of a tolerance in or on The microbial pest control agent in- all food commodities, when used in ac- clusion bodies of the multi-nuclear cordance with good agricultural prac- polyhedrosis virus of Anagrapha tices. falcifera is exempted from the require- ment of a tolerance in or on all raw ag- [67 FR 51088, Aug. 7, 2002] ricultural commodities when used to control certain lepidopteran pest spe- § 180.1144 Candida oleophila isolate I- 182; exemption from the require- cies. ment of a tolerance. [60 FR 37020, July 19, 1995] Candida oleophila isolate I-182, when used as a post-harvest biological fun- § 180.1150 6-Benzyladenine; exemption gicide, is exempted from the require- from the requirement of a toler- ance. ment of a tolerance in or on all raw ag- ricultural commodities. The biochemical plant regulator 6- benzyladenine (6–BA) is exempt from [60 FR 11033, Mar. 1, 1995] the requirement of a tolerance in or on apple and pear when applied at a rate § 180.1145 Pseudomonas syringae; ex- ≤ emption from the requirement of a of 182 grams of active ingredient per tolerance. acre per season, and in or on pistachio when applied at a rate of ≤60 grams of Pseudomonas syringae is exempted active ingredient per acre per season. from the requirement of a tolerance on all raw agricultural commodities when [72 FR 13179, Mar. 21, 2007] applied postharvest according to good agricultural practices. § 180.1153 Lepidopteran pheromones; exemption from the requirement of [60 FR 12703, Mar. 8, 1995] a tolerance. Lepidopteran pheromones that are § 180.1146 Beauveria bassiana Strain GHA; exemption from the require- naturally occurring compounds, or ment of a tolerance. identical or substantially similar syn- thetic compounds, designated by an Beauveria bassiana Strain GHA is ex- unbranched aliphatic chain (between 9 empted from the requirement of a tol- and 18 carbons) ending in an alcohol, erance in or on all raw agricultural aldehyde or acetate functional group commodities when applied to growing and containing up to 3 double bonds in crops according to good agricultural the aliphatic backbone, are exempt practices. from the requirement of a tolerance in [60 FR 18547, Apr. 12, 1995] or on all raw agricultural commodities. This exemption only pertains to those § 180.1148 Occlusion Bodies of the situations when the pheromone is: Ap- Granulosis Virus of Cydia plied to growing crops at a rate not to pomenella; tolerance exemption. exceed 150 grams active ingredient/ An exemption from the requirement acre/year in accordance with good agri- of a tolerance is established for resi- cultural practices; and applied as a dues of the microbial pest control post-harvest treatment to stored food agent Occlusion Bodies of the commodities at a rate not to exceed 3.5 Granulosis Virus of Cydia pomonella grams active ingredient/1,000 ft2/year (codling moth) in or on all raw agricul- (equivalent to 150 grams active ingre- tural commodities. dient/acre/year) in accordance with good agricultural practices. [60 FR 42450, Aug. 16, 1995] [71 FR 45399, Aug. 9, 2006]

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§ 180.1154 CryIA(c) and CryIC derived § 180.1159 Pelargonic acid; exemption delta-endotoxins of Bacillus from the requirement of tolerances. thuringiensis var. kurstaki encap- (a) An exemption from the require- sulated in killed Pseudomonas fluorescens, and the expression ment of a tolerance is established for plasmid and cloning vector genetic residues of pelargonic acid in or on all constructs. food commodities when used as a plant regulator on plants, seeds, or cuttings CryIA(c) and CryIC derived delta- and on all food commodities after har- endotoxins of Bacillus thuringiensis var. vest in accordance with good agricul- kurstaki encapsulated in killed tural practices. Pseudomonas fluorescens and the expres- (b) Pelargonic acid when used as an sion plasmid and cloning vector ge- herbicide is exempt from the require- netic constructs are exempt from the ment of a tolerance on all plant food requirement of a tolerance when used commodities provided that: in or on all raw agricultural commod- (1) Applications are not made di- ities. rectly to the food commodity except [60 FR 47489, Sept. 13, 1995] when used as a harvest aid or desiccant to: any root and tuber vegetable, bulb § 180.1156 Cinnamaldehyde; exemption vegetable or cotton. from the requirement of a toler- (2) When pelargonic acid is used as a ance. harvest aid or desiccant, applications Cinnamaldehyde (3-phenyl-2- must be made no later than 24 hours propenal) is exempted from the re- prior to harvest. quirement of a tolerance in or on all (c) An exemption from the require- food commodities, when used as a fun- ment of a tolerance is established for gicide, insecticide, and algaecide in ac- residues of pelargonic acid in or on all cordance with good agricultual prac- raw agricultural commodities and in tices. processed commodities, when such resi- dues result from the use of pelargonic [64 FR 7804, Feb. 17, 1999; 64 FR 14099, Mar. 24, acid as an antimicrobial treatment in 1999] solutions containing a diluted end-use § 180.1157 Cytokinins; exemption from concentration of pelargonic acid up to the requirement of a tolerance. 170 ppm per application on food contact surfaces such as equipment, pipelines, An exemption from the requirement tanks, vats, fillers, evaporators, of a tolerance is established for resi- pasteurizers and aseptic equipment in dues of cytokinins (specifically: aque- restaurants, food service operations, ous extract of seaweed meal and dairies, breweries, wineries, beverage kinetin) in or on all food commodities and food processing plants. when used as plant regulators on plants, seeds, or cuttings and on all [62 FR 28364, May 23, 1997, as amended at 64 food commodities after harvest in ac- FR 31505, June 11, 1999; 68 FR 7935, Feb. 19, cordance with good agricultural prac- 2003] tices. § 180.1160 Jojoba oil; exemption from [64 FR 31505, June 11, 1999] the requirement of a tolerance. The insecticide and spray tank adju- § 180.1158 Auxins; exemption from the vant jojoba oil is exempted from the requirement of a tolerance. requirement of a tolerance in or on all An exemption from the requirement raw agricultural commodities when ap- of a tolerance is established for resi- plied at the rate of 1.0% or less of the dues of auxins (specifically: indole-3- final spray in accordance with good ag- acetic acid and indole-3-butyric acid) ricultural practices, provided the in or on all food commodities when jojoba oil does not contain used as plant regulators on plants, simmondsin, simmondsin-2-ferulate, seeds, or cuttings and on all food com- and related conjugated organonitriles modities after harvest in accordance including demethyl simmondsin and with good agricultural practices. didemethylsimmondsin. [64 FR 31505, June 11, 1999] [61 FR 2121, Jan. 25, 1996]

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§ 180.1161 Clarified hydrophobic ex- § 180.1163 Killed Myrothecium tract of neem oil; exemption from verrucaria; exemption from the re- the requirement of a tolerance. quirement of a tolerance. Clarified hydrophobic extract of Killed Myrothecium verrucaria is ex- neem oil is exempt from the require- empted from the requirement of a tol- ment of a tolerance on all food com- erance in or on all raw agricultural modities when used as a botanical fun- commodities when applied as a pre- gicide/insecticide/miticide. seed or pre- or post-planting soil treat- ment alone or mixed with water and [67 FR 43552, June 28, 2002] the mixed suspension be applied through drip or border irrigation sys- § 180.1162 Acrylate polymers and co- tems and the indicator mycotoxin lev- polymers; exemption from the re- quirement of a tolerance. els do not exceed 15 ppm. (a) Acrylate polymers and copoly- [61 FR 11315, Mar. 20, 1996, as amended at 61 mers are exempt from the requirement FR 58332, Nov. 14, 1996] of a tolerance when used as inert ingre- § 180.1165 Capsaicin; exemption from dients in pesticidal formulations ap- the requirement of a tolerance. plied to growing, raw agricultural com- modities. This tolerance exemption Capsaicin is exempt from the require- covers the acrylate polymers/copoly- ment of a tolerance in or on all food mers that are intrinsically safe and al- commodities when used in accordance ready listed in TSCA inventory or will with approved label rates and good ag- meet the polymer tolerance exemption ricultural practice. from requirements of [63 FR 39521, July 23, 1998] premanufacturing notification under 40 CFR 723.250. Polymers exempted can be § 180.1167 Allyl isothiocyanate as a used as dispensers, resins, fibers, and component of food grade oil of mus- beads, as long as the fibers, beads and tard; exemption from the require- resins particle sizes are greater than 10 ment of a tolerance. microns and insoluble in water. This The insecticide and repellent Allyl exemption pertains to the acrylate isothiocyanate is exempt from the re- polymers/copolymers used as inert in- quirement of a tolerance for residues gredients for sprayable and dispenser when used as a component of food pesticide formulations that are applied grade oil of mustard, in or on all raw on food crops. Any acrylate polymers/ agricultural commodities, when ap- copolymers used for encapsulating ma- plied according to approved labeling. terial must be cleared as an inert in- [61 FR 24894, May 17, 1996] gredient when used in pesticide formu- lation applied on food crops. § 180.1176 Sodium bicarbonate; exemp- (b) For the purposes of this exemp- tion from the requirement of a tol- tion, acrylate polymers/copolymers erance. used as inert ingredients in an end-use The biochemical pesticide sodium bi- formulation must meet the definition carbonate is exempted from the re- for a polymer as given in 40 CFR quirement of a tolerance in or on all 723.250(b), are not automatically ex- raw agricultural commodities when ap- cluded by 40 723.250(d), and meet the plied as a fungicide or post-harvest fun- tolerance exemption criteria in 40 CFR gicide in accordance with good agricul- 723.250(e)(1), 40 CFR 723.250 (e)(2) or 40 tural practices. CFR 723.250(e)(3). Therefore, acrylate polymers and copolymers that are al- [61 FR 67473, Dec. 23, 1996] ready listed in the TSCA inventory or § 180.1177 Potassium bicarbonate; ex- will meet the polymer tolerance ex- emption from the requirement of a emption under 40 CFR 723.250 as tolerance. amended on March 29, 1995 are covered The biochemical pesticide potassium by this exemption. bicarbonate is exempted from the re- [61 FR 6551, Feb. 21, 1996] quirement of a tolerance in or on all

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raw agricultural commodities when ap- (FIFRA), as amended (7 U.S.C. 136). plied as a fungicide or post-harvest fun- This temporary exemption from the re- gicide in accordance with good agricul- quirement of a tolerance expires and is tural practices. revoked December 31, 1999. This tem- porary exemption from the require- [61 FR 67473, Dec. 23, 1996] ment of a tolerance may be revoked at § 180.1178 Formic acid; exemption any time if the experimental use per- from the requirement of a toler- mit is revoked or if any experience ance. with or scientific data on this pesticide The pesticide formic acid is exempted indicate that the tolerance is not safe. (b) Kaolin is exempted from the re- from the requirement of a tolerance in quirement of a tolerance for residues or on honey and honeycomb when used when used on or in food commodities to to control tracheal mites and suppress aid in the control of insects, fungi, and varroa mites in bee colonies, and ap- bacteria (food/feed use). plied in accordance with label use di- rections. [62 FR 19685, Apr. 23, 1997, as amended at 63 FR 9430, Feb. 25, 1998] [74 FR 26535, June 3, 2009] § 180.1181 Bacillus cereus strain BPO1; § 180.1179 Plant extract derived from exemption from the requirement of Opuntia lindheimeri, Quercus a tolerance. falcata, Rhus aromatica, and Rhizophoria mangle; exemption An exemption from the requirement from the requirement of a toler- of a tolerance for residues of the Bacil- ance. lus cereus strain BPO1 in or on all raw The biochemical pesticide plant ex- agricultural commodities when ap- tract derived from Opuntia lindheimeri, plied/used in accordance with label di- Quercus falcata, Rhus aromatica, and rections. Rhizophoria mangle is exempted from [67 FR 70017, Nov. 20, 2002] the requirement of a tolerance in or on all raw agricultural commodities when § 180.1187 L-glutamic acid; exemption applied as a nematicide/plant regulator from the requirement of a toler- in accordance with good agricultural ance. practices. L-glutamic acid is exempt from the requirement of a tolerance on all food [62 FR 24842, May 7, 1997] commodities when used in accordance § 180.1180 Kaolin; exemption from the with good agricultural practices. requirement of a tolerance. [66 FR 33198, June 21, 2001] (a) The biochemical pesticide kaolin is temporarily exempted from the re- § 180.1188 Gamma aminobutyric acid; exemption from the requirement of quirement of a tolerance for residues of a tolerance. the insecticide Kaolin, when used on crops (apples, apricots, bananas, beans, Gamma aminobutyric acid is exempt cane berries, citrus fruits, corn, cotton, from the requirement of a tolerance on cranberries, cucurbits, grapes, melons, all food commodities when used in ac- nuts, ornamentals, peaches, peanuts, cordance with good agricultural prac- pears, peppers, plums, potatoes, seed tices. crops, small grains, soybeans, straw- [66 FR 33198, June 21, 2001] berries, sugar beets, and tomatoes) to control certain insect, fungus, and bac- § 180.1189 Methyl salicylate; exemption terial damage to plants. This tem- from the requirement of a toler- porary exemption from the require- ance. ment of a tolerance will permit the The biochemical pesticide methyl sa- marketing of the food commodities in licylate is exempt from the require- this paragraph when treated in accord- ment of a tolerance for residues in or ance with the provisions of experi- on food or feed when used as an insect mental use permit 70060–EUP–1, which repellant in food packaging and animal is being issued under the Federal Insec- feed packaging at an application rate ticide, Fungicide, and Rodenticide Act that does not exceed 0.2 mg of methyl

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salicylate per square inch of packaging luted end-use concentration of peroxy- materials. acetic acid up to 500 ppm, and applied [62 FR 61639, Nov. 19, 1997] to tableware, utensils, dishes, pipe- lines, tanks, vats, fillers, evaporators, § 180.1191 Ferric phosphate; exemp- pasteurizers, aseptic equipment, milk- tion from the requirement of a tol- ing equipment, and other food proc- erance. essing equipment in food handling es- An exemption from the requirement tablishments including, but not limited of a tolerance is established for resi- to dairies, dairy barns, restaurants, dues of the biochemical pesticide, fer- food service operations, breweries, ric phosphate (FePO4, CAS No. 11045– wineries, and beverage and food proc- 86–0) in or on all food commodities. essing plants. [62 FR 56105, Oct. 29, 1997] (c) An exemption from the require- ment of a tolerance is established for § 180.1193 Potassium dihydrogen phos- residues of the biochemical pesticide phate; exemption from the require- peroxyacetic acid and its metabolites ment of a tolerance. and degradates, including hydrogen Potassium dihydrogen phosphate is peroxide and acetic acid, in or on all exempted from the requirement of a food commodities, when used in ac- tolerance in or on all food commodities cordance with good agricultural prac- when applied as a fungicide in accord- tices. ance with good agricultural practices. [74 FR 26535, June 3, 2009, as amended at 76 [63 FR 43085, Aug. 12, 1998] FR 11969, Mar. 4, 2011]

§ 180.1195 Titanium dioxide. § 180.1197 Hydrogen peroxide; exemp- Titanium dioxide (CAS Reg. No. tion from the requirement of a tol- 13463–67–7) is exempted from the re- erance. quirement of a tolerance for residues in An exemption from the requirement or on growing crops, when used as an of a tolerance is established for resi- inert ingredient (UV protectant) in dues of hydrogen peroxide in or on all microencapsulated formulations of the food commodities at the rate of ≤1% insecticide lambda cyhalothrin at no hydrogen peroxide per application on more than 3.0% by weight of the formu- growing and postharvest crops. lation and as an inert ingredient (UV- stabilizer) at no more than 5% in pes- [67 FR 41844, June 20, 2002] ticide formulations containing the ac- tive ingredient napropamide. § 180.1198 Gliocladium catenulatum strain J1446; exemption from the [77 FR 44155, July 27, 2012] requirement of a tolerance. § 180.1196 Peroxyacetic acid; exemp- An exemption from the requirement tion from the requirement of a tol- of a tolerance is established for resi- erance. dues of the microbial pesticide, (a) An exemption from the require- Gliocladium catenulatum strain J1446 ment of a tolerance is established for when used in or on all food commod- residues of peroxyacetic acid in or on ities. all food commodities, when such resi- [63 FR 37288, July 10, 1998] dues result from the use of peroxy- acetic acid as an antimicrobial treat- § 180.1199 ment in solutions containing a diluted Lysophosphatidylethanolamine end use concentration of peroxyacetic (LPE); exemption from the require- acid up to 100 ppm per application on ment of a tolerance. fruits, vegetables, tree nuts, cereal An exemption from the requirement grains, herbs, and spices. of a tolerance is established for resi- (b) An exemption from the require- dues of the biochemical pesticide ment of a tolerance is established for lysophosphatidylethanolamine in or on residues of peroxyacetic acid, in or on all food commodities. all food commodities when used in sanitizing solutions containing a di- [67 FR 17636, Apr. 11, 2002]

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§ 180.1200 Pseudomonas fluorescens (d) Possesses a common secondary strain PRA–25; temporary exemp- structure consisting of a and b units tion from the requirement of a tol- that form an HR domain. erance. (e) Is heat stable (retains HR activity A temporary exemption from the re- when heated to 65 °C for 20 minutes). quirement of a tolerance is established (f) Is readily degraded by a proteinase for residues of the microbial pesticide, representative of environmental condi- pseudomonas fluorescens strain PRA–25 tions (no protein fragments >3.5 kD when used on peas, snap beans and after 15 minutes degradation with sweet corn and will expire July 31, 2001. Subtilisin A). [63 FR 38498, July 17, 1998] (g) Exhibits a rat acute oral toxicity (LD50) of greater than 5,000 mg product/ § 180.1201 Trichoderma harzianum kg body weight. strain T-39; exemption from the re- quirement of a tolerance. [69 FR 24996, May 5, 2004] Trichoderma harzianum strain T-39 is § 180.1205 Beauveria bassiana ATCC exempt from the requirement of a tol- #74040; exemption from the require- erance on all food commodities. ments of a tolerance. [65 FR 38757, June 22, 2000] An exemption from the requirement of a tolerance is established for resi- § 180.1202 Bacillus sphaericus; exemp- dues of the insecticide Beauveria tion from the requirement of a tol- erance. bassiana (ATCC #74040) in or on all food commodities when applied or used as An exemption from the requirement ground and aerial foliar sprays for use of a tolerance is established for resi- only on terrestrial crops. dues of the microbial pesticides, Bacil- lus sphaericus when used in or on all [64 FR 22796, Apr. 28, 1999] food crops. § 180.1206 Aspergillus flavus AF36; ex- [63 FR 48597, Sept. 11, 1998] emption from the requirement of a tolerance. § 180.1204 Harpin protein; exemption from the requirement of a toler- (a) An exemption from the require- ance. ment of a tolerance is established for An exemption from the requirement residues of the microbial pesticide As- of a tolerance is established for resi- pergillus flavus AF36 in or on cotton, dues of individual harpin proteins that gin byproducts; cotton, hulls; cotton, meet specified physiochemical and tox- meal; cotton, refined oil; cotton, icological criteria when used as bio- undelinted seed. chemical pesticides on all food com- (b) An exemption from the require- modities to enhance plant growth, ment of a tolerance is established for quality and yield, to improve overall residues of Aspergillus flavus AF36 in or plant health, and to aid in pest man- on pistachio when applied as an agement. The physiochemical and toxi- antifungal agent and used in accord- cological criteria identifying harpin ance with good agricultural practices. proteins are as follows: (c) An exemption from the require- (a) Consists of a protein less than 100 ment of a tolerance is established for kD in size, that is acidic (pI<7.0), gly- residues of Aspergillus flavus AF36 in or cine rich (>10%), and contains no more on corn, field, forage; corn, field, grain; than one cystine residue. corn, field, stover; corn, field, aspirated (b) The source(s) of genetic material grain fractions; corn, sweet, kernel encoding the protein are bacterial plus cob with husk removed; corn, plant pathogens not known to be mam- sweet, forage; corn, sweet, stover; corn, malian pathogens. pop, grain; and corn, pop, stover, when (c) Elicits the hypersensitive re- applied/used as an antifungal agent. sponse (HR) which is characterized as [68 FR 41541, July 14, 2003, as amended at 72 rapid, localized cell death in plant tis- FR 28871, May 23, 2007; 72 FR 72965, Dec. 26, sue after infiltration of harpin into the 2007; 74 FR 26535, 26546, June 3, 2009; 76 FR intercellular spaces of plant leaves. 16301, Mar. 23, 2011; 77 FR 14291, Mar. 9, 2012]

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§ 180.1207 N-acyl sarcosines and so- Pseudomonas chlororaphis Strain 63–28 dium N-acyl sarcosinates; exemp- in or on all food commodities. tion from the requirement of a tol- erance. [66 FR 53346, Oct. 22, 2001] An exemption from the requirement § 180.1213 Coniothyrium minitans of a tolerance is established for resi- strain CON/M/91–08; exemption dues of the following substances when from the requirement of a toler- used as inert ingredients (surfactants) ance. at levels not to exceed 10% in pesticide An exemption from the requirement formulations containing glyphosate: of a tolerance is established for resi- dues of the microbial pesticide Name CAS Reg. No. Coniothyrium minitans strain CON/M/91– N-acyl sarcosines. 08 when used in or on all food commod- N-cocoyl sarcosine mixture ...... 68411-97-2 ities. N-lauroyl sarcosine ...... 97-78-9 N-myristoyl sarcosine ...... 52558-73-3 [66 FR 16874, Mar. 28, 2001] N-oleoyl sarcosine ...... 110-25-8 N-stearoyl sarcosine ...... 142-48-3 § 180.1218 Indian Meal Moth Sodium N-acyl sarcosinates. Granulosis Virus; exemption from N-cocoyl sarcosine sodium salt mixture ...... 61791-59-1 the requirement of a tolerance. N-methyl-N-(1-oxo-9-octodecenyl) glycine .... 3624-77-9 N-methyl-N-(1-oxododecyl) glycine ...... 137-16-6 An exemption from the requirement N-methyl-N-(1-oxooctadecyl) glycine ...... 5136-55-0 of a tolerance is established for resi- N-methyl-N-(1-oxotetradecyl glycine ...... 30364-51-3 dues of the microbial pesticide Indian Meal Moth Granulosis Virus when used [64 FR 68046, Dec. 6, 1999] in or on all food commodities. § 180.1209 Bacillus subtilis strain QST [68 FR 55875, Sept. 29, 2003] 713 and strain QST 713 variant soil; exemption from the requirement of § 180.1219 Foramsulfuron; exemption a tolerance. from the requirement of a toler- An exemption from the requirement ance. of a tolerance is established for resi- The pesticide foramsulfuron is ex- dues of the microbial pesticides Bacil- empted from the requirement of a tol- lus subtilis strain QST 713 and strain erance in corn, field, grain/corn, field, QST 713 variant soil when used in or on forage/ corn, field, stover/corn, pop, all food commodities. grain/corn, pop, forage/corn, pop, sto- [77 FR 73937, Dec. 12, 2012] ver; corn, sweet, forage; corn, sweet, kernel plus cob with husks removed; § 180.1210 Phosphorous acid; exemp- corn, sweet, stover when applied as a tion from the requirement of a tol- erance. herbicide in accordance with good agri- cultural practices. An exemption from the requirement of a tolerance is established for resi- [74 FR 26535, June 3, 2009] dues of phosphorous acid and its am- monium, sodium, and potassium salts § 180.1220 1-Methylcyclopropene; ex- in or on all food commodities when emption from the requirement of a used as an agricultural fungicide and in tolerance. or on potatoes when applied as a post- An exemption from the requirement harvest treatment at 35,600 ppm or less of a tolerance is established for resi- phosphorous acid. dues of the 1-Methylcyclopropene in or [71 FR 49373, Aug. 23, 2006] on fruits and vegetables when: (a) Used as a post harvest plant § 180.1212 Pseudomonas chlororaphis growth regulator, i.e., for the purpose Strain 63–28; exemption from the of inhibiting the effects of ethylene. requirement of a tolerance. (b) Applied or used outdoors for pre- An exemption from the requirement harvest treatments. of a tolerance is established for resi- dues of the microbial pesticide [73 FR 19150, Apr. 9, 2008]

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§ 180.1221 Pseudozyma flocculosa tions containing a diluted end-use con- strain PF-A22 UL; exemption from centration of decanoic acid (up to 170 the requirement of a tolerance. ppm per application) on food contact An exemption from the requirement surfaces such as equipment, pipelines, of a tolerance is established for resi- tanks, vats, fillers, evaporators, dues of Pseudozyma flocculosa strain pasteurizers and aseptic equipment in PF-A22 UL in or on all food commod- restaurants, food service operations, ities. dairies, breweries, wineries, beverage [67 FR 60966, Sept. 27, 2002] and food processing plants. [68 FR 7939, Feb. 19, 2003; 68 FR 17308, Apr. 9, § 180.1222 Sucrose octanoate esters; 2003] exemption from the requirement of a tolerance. § 180.1226 Bacillus pumilus strain An exemption from the requirement QST2808; temporary exemption of a tolerance is established for resi- from the requirement of a toler- dues of sucrose octanoate esters [(a-D- ance. glucopyranosyl-b-D-fructofuranosyl-oc- A temporary exemption from the re- tanoate), mono-, di-, and triesters of quirement of a tolerance is established sucrose octanoate] in or on all food for residues of the microbial pesticide commodities when used in accordance Bacillus pumilus strain QST2808 when with good agricultural practices. used in or on all agricultural commod- [67 FR 60152, Sept. 25, 2002] ities when applied/used in accordance with label directions. § 180.1223 Imazamox; exemption from the requirement of a tolerance. [68 FR 36480, June 18, 2003] The herbicide imazamox, (±) 2, -[4,5- § 180.1228 Diallyl sulfides; exemption dihydro-4-methyl-4-(1-methylethyl)-5- from the requirement of a toler- oxo-1H-imidazol-2-yl]-5- ance. (methoxymethyl)-3-pyridinecarboxylic acid, is exempt from the requirement An exemption from the requirement of a tolerance on all food commodities of a tolerance is established for resi- when applied as a herbicide in accord- dues of diallyl sulfides when used in/on ance with good agricultural practices. garlic, leeks, onions, and shallots. [68 FR 7433, Feb. 14, 2003] [68 FR 40808, July 9, 2003]

§ 180.1224 Bacillus pumilus GB34; ex- § 180.1230 Ferrous sulfate; exemption emption from the requirement of a from the requirement of a toler- tolerance. ance. An exemption from the requirement An exemption from the requirement of a tolerance is established for resi- of a tolerance is established for resi- dues of the microbial pesticide Bacillus dues of ferrous sulfate. pumilus GB34 when used as a seed treat- ment in or on all food commodities. An [70 FR 33363, June 8, 2005] exemption is also granted for such resi- dues on treated but unplanted soybean § 180.1231 Lime; exemption from the seeds. requirement of a tolerance. An exemption from the requirement [69 FR 76625, Dec. 22, 2004] of a tolerance is established for resi- § 180.1225 Decanoic acid; exemption dues of lime. from the requirement of a toler- ance. [70 FR 33363, June 8, 2005] An exemption from the requirement § 180.1232 Lime-sulfur; exemption from of a tolerance is established for resi- the requirement of a tolerance. dues of decanoic acid in or on all raw An exemption from the requirement agricultural commodities and in proc- of a tolerance is established for resi- essed commodities, when such residues dues of lime-sulfur. result from the use of decanoic acid as an antimicrobial treatment in solu- [70 FR 33363, June 8, 2005]

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§ 180.1233 Potassium sorbate; exemp- § 180.1240 Thymol; exemption from the tion from the requirement of a tol- requirement of a tolerance. erance. (a) Time-limited exemptions from An exemption from the requirement the requirement of a tolerance are es- of a tolerance is established for resi- tablished for residues of thymol on dues of potassium sorbate. honey and honeycomb in connection with use of the pesticide under section [70 FR 33363, June 8, 2005] 18 emergency exemptions granted by the EPA. These time-limited exemp- § 180.1234 Sodium carbonate; exemp- tion from the requirement of a tol- tions from the requirement of a toler- erance. ance for residues of thymol will expire and are revoked on June 30, 2007. An exemption from the requirement (b) An exemption from the require- of a tolerance is established for resi- ment of a tolerance for residues of the dues of sodium carbonate. thymol (as present in thyme oil) in or [70 FR 33363, June 8, 2005] on food commodities when applied/used in/on public eating places, dairy proc- § 180.1235 Sodium hypochlorite; ex- essing equipment, and/or food proc- emption from the requirement of a essing equipment and utensils. tolerance. [70 FR 37696, June 30, 2005, as amended at 71 An exemption from the requirement FR 2895, Jan. 18, 2006; 74 FR 12617, Mar. 25, of a tolerance is established for resi- 2009] dues of sodium hypochlorite. § 180.1241 Eucalyptus oil; exemption [70 FR 33363, June 8, 2005] from the requirement of a toler- ance. § 180.1236 Sulfur; exemption from the Time-limited exemptions from the requirement of a tolerance. requirement of a tolerance are estab- An exemption from the requirement lished for residues of eucalyptus oil on of a tolerance is established for resi- honey and honeycomb in connection dues of sulfur. with use of the pesticide under section 18 emergency exemptions granted by [70 FR 33363, June 8, 2005] the EPA. These time-limited exemp- § 180.1237 Sodium metasilicate; exemp- tions from the requirement of a toler- tion from the requirement of a tol- ance for residues of eucalyptus oil will erance. expire and are revoked on June 30, 2007. (a) An exemption from the require- [70 FR 37696, June 30, 2005] ment of a tolerance is established for residues of sodium metasilicate in or § 180.1243 Bacillus subtilis var. amyloliquefaciens strain FZB24; ex- on all food commodities when used in emption from the requirement of a accordance with approved label rates tolerance. and good agricultural practices as a plant desiccant, so long as the sodium An exemption from the requirement of a tolerance for residues of the Bacil- metasilicate does not exceed 4% by lus subtilis var. amyloliquefaciens strain weight in aqueous solution. FZB24 in or on all agricultural com- (b) An exemption from the require- modities when applied/used in accord- ment of a tolerance is established for ance with label directions. residues of sodium metasilicate in or on all food commodities when used in [68 FR 44640, July 30, 2003] accordance with approved label rates and good agricultural practices as an § 180.1244 Ammonium bicarbonate; ex- emption from the requirement of a insecticide and fungicide, so long as tolerance. the sodium metasilicate does not ex- ceed 2.41% by weight in aqueous solu- An exemption from the requirement tion. of tolerance is established for residues of ammonium bicarbonate used in or [71 FR 19441, Apr. 14, 2006] on all food commodities when used in

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accordance with good agricultural § 180.1251 Geraniol; exemption from practices. the requirement of a tolerance. [69 FR 13745, Mar. 24, 2004] An exemption from the requirement of a tolerance is established for resi- § 180.1245 Rhamnolipid biosurfactant; dues of the biochemical pesticide gera- exemption from the requirement of niol in or on all food commodities. a tolerance. [69 FR 23151, Apr. 28, 2004] An exemption from the requirement of a tolerance is established for resi- § 180.1253 Streptomyces lydicus WYEC 108; exemption from the require- dues of rhamnolipid biosurfactant ment of a tolerance. when used in accordance with good ag- ricultural practices as a fungicide in or An exemption from the requirement on all food commodities. of a tolerance is established for resi- dues of the microbial pesticide [69 FR 16800, Mar. 31, 2004] Streptomyces lydicus WYEC 108 when used in or on all agricultural commod- § 180.1246 Yeast Extract Hydrolysate ities when applied/used in accordance from Saccharomyces cerevisiae: ex- with label directions. emption from the requirement of a tolerance. [69 FR 31301, June 3, 2004] This regulation establishes an ex- § 180.1254 Aspergillus flavus NRRL emption from the requirement of a tol- 21882; exemption from the require- erance for residues of the biochemical ment of a tolerance. pesticide Yeast Extract Hydrolysate (a) An exemption from the require- from Saccharomyces cerevisiae on all ment of a tolerance is established for food commodities when applied/used residues of Aspergillus flavus NRRL for the management of plant diseases. 21882 on peanut; peanut, hay; peanut, meal; and peanut, refined oil. [69 FR 9958, Mar. 3, 2004] (b) An exemption from the require- ment of a tolerance is established for § 180.1248 Exemption of citronellol residues of Aspergillus flavus NRRL from the requirement of a toler- ance. 21882 on corn, field, forage; corn, field, grain; corn, field, stover; corn, field, as- An exemption from the requirement pirated grain fractions; corn, sweet, of a tolerance is established for resi- kernel plus cob with husk removed; dues of the biochemical pesticide corn, sweet, forage; corn, sweet, stover; citronellol in or on all food commod- corn, pop, grain; and corn, pop, stover. ities. [75 FR 6576, Feb. 10, 2010] [69 FR 23146, Apr. 28, 2004] § 180.1255 Bacillus pumilus strain QST § 180.1250 C8, C10, and C12 fatty acid 2808; exemption from the require- monoesters of glycerol and pro- ment of a tolerance. pylene glycol; exemption from the An exemption from the requirement requirement of a tolerance. of a tolerance is established for resi- The C8, C10, and C12 straight-chain dues of the microbial pesticide Bacillus fatty acid monoesters of glycerol (glyc- pumilus strain QST 2808 when used in or erol monocaprylate, glycerol on all agricultural commodities when applied/used in accordance with label monocaprate, and glycerol directions. monolaurate) and propylene glycol (propylene glycol monocaprylate, pro- [69 FR 63954, Nov. 3, 2004] pylene glycol monocaprate, and pro- pylene glycol monolaurate) are exempt § 180.1256 Alternaria destruens strain 059; exemption from the require- from the requirement of a tolerance in ment of a tolerance. or on all food commodities when used in accordance with approved label rates An exemption from the requirement of a tolerance is established for resi- and good agricultural practice. dues of the microbial pesticide [69 FR 34944, June 23, 2004] Alternaria destruens Strain 059 when

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used in or on all raw agricultural com- § 180.1260 Muscodor albus QST 20799 modities when applied/used in accord- and the volatiles produced on re- ance with label directions. hydration; exemption from the re- quirement of a tolerance. [70 FR 28459, May 18, 2005] An exemption from the requirement § 180.1257 Paecilomyces lilacinus of a tolerance is established on all food/ strain 251; exemption from the re- feed commodities, for residues of quirement of a tolerance. Muscodor albus QST 20799, and the An exemption from the requirement volatiles produced on its rehydration, of a tolerance is established for resi- when the pesticide is used for all agri- dues of the microbial pesticide cultural applications, including seed, Paecilomyces lilacinus strain 251 when propagule and post harvest treatments. used in or on all agricultural commod- [70 FR 56576, Sept. 28, 2005] ities when applied/used in accordance with label directions. § 180.1261 Xanthomonas campestris pv. vesicatoria and Pseudomonas [70 FR 19283, Apr. 13, 2005] syringae pv. tomato specific Bacteriophages. § 180.1258 Acetic acid; exemption from the requirement of a tolerance. An exemption from the requirement of a tolerance is established for resi- (a) An exemption from the require- dues of Xanthomonas campestris pv. ment of a tolerance is established for vesicatoria and Pseudomonas syringae pv. residues of the biochemical pesticide tomato specific bacteriophages in or on acetic acid when used as a preservative pepper and tomato. on post-harvest agricultural commod- ities intended for animal feed, includ- [74 FR 26536, June 3, 2009] ing Alfalfa, seed; alfalfa, hay; barley, grain; bermudagrass, hay; bluegrass, § 180.1262 Sorbitol octanoate; exemp- hay; bromegrass, hay; clover, hay; tion from the requirement of a tol- corn, field, grain; corn, pop, grain; erance. cowpea, hay; fescue, hay; lespedeza, An exemption from the requirement hay; lupin; oat, grain; orchardgrass, of a tolerance is established for resi- hay; peanut, hay; timothy, hay; vetch, dues of sorbitol octanoate in or on all hay; and wheat, grain, or commodities food commodities when used in accord- described as grain or hay. ance with label directions. (b) An exemption from the require- [71 FR 4518, Jan. 27, 2006] ment of a tolerance is established for residues of acetic acid in or on all food § 180.1263 Tetrahydrofurfuryl alcohol; crops resulting from unintentional exemption from the requirement of spray and drift to non-target vegeta- a tolerance. tion including non-food, food and feed Tetrahydrofurfuryl alcohol (THFA, crops when used as a non-selective con- CAS Reg. No. 97–99–4) is exempt from tact herbicide spray. the requirement of a tolerance in or on [75 FR 40741, July 14, 2010] all raw agricultural commodities when used in accordance with good agricul- § 180.1259 Reynoutria sachalinensis ex- tural practices as an inert ingredient tract; exemption from the require- applied only: ment of a tolerance. (a) For use as a seed treatment. Residues of the biochemical pesticide (b) For applications prior to planting Reynoutria sachalinensis extract, when and at the time of planting. derived from the whole plant extract, (c) For use on cotton. are exempt from the requirement of a (d) For use in herbicides with one ap- tolerance in or on all food commod- plication to wheat and barley prior to ities. the pre-boot stage, and two applica- tions to canola and soybeans pre- [70 FR 55277, Sept. 21, 2005] bloom.

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(e) For use in herbicides with two ap- eycomb, and honeycomb with honey plications to field corn up to 24 inches when used at 2g or less eucalyptus oil tall (V 5 stage). per hive, where the eucalyptus oil con- tains 80% or more eucalyptol. [71 FR 45415, Aug. 9, 2006] [71 FR 53979, Sept. 13, 2006] § 180.1267 Pantoea agglomerans strain C9–1; exemption from the require- § 180.1272 Pantoea agglomerans strain ment of a tolerance. E325; exemption from the require- An exemption from the requirement ment of a tolerance. of a tolerance is established for resi- An exemption from the requirement dues of Pantoea agglomerans strain C9–1 of a tolerance is established for resi- when used on apples and pears. dues of Pantoea agglomerans strain E325 when used on apples and pears. [71 FR 24596, Apr. 26, 2006] [71 FR 54933, Sept. 20, 2006] § 180.1268 Potassium silicate; exemp- tion from the requirement of a tol- § 180.1273 Beauveria bassiana HF23; erance. exemption from the requirement of a tolerance. Potassium silicate is exempt from the requirement of a tolerance in or on Residues of Beauveria bassiana HF23 all food commodities so long as the po- are exempt from the requirement of a tassium silicate is not applied at rates tolerance on all food/feed commodities, exceeding 1% by weight in aqueous so- when the pesticide is used for the lution and when used in accordance treatment of chicken and livestock fa- with good agricultural practices. cilities, including the treatment of chicken and livestock manure. [71 FR 34272, June 14, 2006] [75 FR 10190, Mar. 5, 2010] § 180.1269 Bacillus mycoides isolate J; exemption from the requirement of § 180.1274 Tris (2-ethylhexyl) phos- a tolerance. phate; exemption from the require- ment of a tolerance. Bacillus mycoides isolate J is tempo- rarily exempt from the requirement of Tris (2-ethylhexyl) phosphate (TEHP, a tolerance when used as a fungicide on CAS Reg. No. 78–42–2) is exempt from potatoes in accordance with a valid the requirement of a tolerance for resi- Federal Insecticide, Fungicide, and dues in grain, aspirated fractions; bar- Rodenticide Act (FIFRA) section 18 ley, grain, barley, hay, barley, straw; emergency exemption. This temporary wheat, grain; wheat, forage; wheat, exemption from the requirement of a hay; wheat, straw when used under the tolerance expires and is revoked on De- following conditions: cember 31, 2015. (a) The use is in accordance with good agricultural practices; [78 FR 24353, Apr. 25, 2013] (b) Tris (2-ethylhexyl) phosphate is used as an inert ingredient in pesticide § 180.1270 Isophorone; exemption from formulations with the active ingredi- the requirement of a tolerance. ents pinoxaden, clodinafop-propargyl, Isophorone (CAS Reg. No. 78–59–1) is and tralkoxydium; exempt from the requirement of a tol- (c) Tris (2-ethylhexyl) phosphate is erance when used as an inert ingre- applied no more than twice per season; dient in pesticide formulations applied and to beets, ginseng, rice, spinach, sugar (d) The applications occur no later beets, and Swiss chard. than the pre-boot stage (prior to for- [71 FR 45408, Aug. 9, 2006] mation of edible grain). [72 FR 5624, Feb. 7, 2007, as amended at 74 FR § 180.1271 Eucalyptus oil; exemption 26536, June 3, 2009] from the requirement of a toler- ance. § 180.1275 Pythium; exception from the An exemption from the requirement requirement of a tolerance. of tolerance is established for residues An exemption from the requirement of eucalyptus oil in or on honey, hon- of tolerance is established on all food/

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feed commodities, for residues of § 180.1280 pythium oligandrum DV 74 when the pes- Poly(hexamethylenebiguanide) hy- ticide is used on food crops. drochloride (PHMB); exemption from the requirement of a toler- [72 FR 27452, May 16, 2007] ance. § 180.1276 Tobacco mild green mosaic Poly(hexamethylenebiguanide) hy- tobamovirus strain U2; exemption drochloride (PHMB)(CAS Reg. No. from the requirement of a toler- 32289–58–0) is exempt from the require- ance. ment of a tolerance for residues of the An exemption from the requirement antimicrobial in or on all food com- of a tolerance is established for resi- modities when the residues are the re- dues of Tobacco mild green mosaic sult of the lawful application of a food tobamovirus strain U2 in or on all com- contact surface sanitizer containing modities of crop groups 17 and 18 when PHMB at 550 parts per million (ppm). applied as a post-emergent herbicide [73 FR 1517, Jan. 9, 2008] and used in accordance with label di- rections and good agricultural prac- § 180.1281 S-Abscisic Acid, (S)-5-(1-hy- tices. droxy-2,6,6-trimethyl-4-oxo-1- cyclohex-2-enyl)-3-methyl-penta- [79 FR 75756, Dec. 19, 2014] (2Z,4E)-dienoic Acid; exemption from the requirement of a toler- § 180.1277 Dibasic esters; exemption ance. from the requirement of a toler- ance. An exemption from the requirement of a tolerance is established for resi- Dibasic esters (CAS Reg. No. 95481–62– dues of S-Abscisic Acid in or on all food 2) is exempted from the requirement of commodities when applied or used a tolerance for residues when used as preharvest as a plant regulator. an inert ingredient (solvent and/or anti-freeze) at 10% W/W or less in [75 FR 11744, Mar. 12, 2010] microencapsulated pesticide formula- tions with the active ingredient § 180.1282 Bacillus firmus I-1582; ex- cyfluthrin. emption from the requirement of a tolerance. [73 FR 10398, Feb. 27, 2008] An exemption from the requirement of a tolerance is established in/on all § 180.1278 Quillaja saponaria extract (saponins); exemption from the re- food/feed commodities, for residues of quirement of a tolerance. Bacillus firmus I-1582 when used as a soil application or seed treatment. Residues of the biochemical pesticide Quillaja saponaria extract (saponins) [73 FR 25528, May 7, 2008] are exempt from the requirement of a tolerance in or on all food commod- § 180.1283 (Z)-7,8-epoxy-2- ities. methyloctadecane (Disparlure); ex- emption from the requirement of a [72 FR 41935, Aug. 1, 2007] tolerance. An exemption from the requirement § 180.1279 Zucchini yellow mosaic of a tolerance is established for resi- virus—weak strain; exemption from the requirement of a tolerance. dues of (Z)-7,8-epoxy-2- methyloctadecane on all food and feed An exemption from the requirement crops that occur when it is used to of a tolerance for residues of the treat trees, shrubs, and pastures and ZYMV–WK strain in or on all raw such use results in unintentional spray cucurbit when applied/used in accord- and drift to non-target vegetation in- ance with label directions. cluding non-food, food, and feed crops. [74 FR 26536, June 3, 2009] This active ingredient is also known as Disparlure. [73 FR 33714, June 13, 2008]

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§ 180.1284 Ammonium salts of higher § 180.1289 Candida oleophila Strain O; fatty acids (C 8-C 18 saturated; C 8-C 12 exemption from the requirement of unsaturated); exemption from the a tolerance. requirement of a tolerance. An exemption from the requirement Ammonium salts of C8-C18 saturated of a tolerance is established for the res- and C8-C12 unsaturated higher fatty idues of the microbial pesticide, acids are exempted from the require- Candida oleophila Strain O, on apples ment of a tolerance for residues in or and pears when applied/used as a post- on all food commodities when used in harvest biofungicide. accordance with good agricultural practice. [74 FR 22464, May 13, 2009] [74 FR 47457, Sept. 16, 2009] § 180.1290 Pasteuria usgae; exemption from the requirement of a toler- § 180.1285 Polyoxin D zinc salt; exemp- ance. tion from the requirement of a tol- erance. An exemption from the requirement of a tolerance is established for resi- An exemption from the requirement dues of Pasteuria usgae in or on all food of a tolerance is established for the res- commodities when applied preharvest idues of polyoxin D zinc salt in or on all food commodities when applied as a and used as a nematicide in accordance fungicide and used in accordance with with good agricultural practices. good agricultural practices. [75 FR 37737, June 30, 2010] [77 FR 56133, Sept. 12, 2012] § 180.1291 Cold pressed neem oil; ex- § 180.1287 Extract of Chenopodium emption from the requirement of a ambrosioides near ambrosioides; ex- tolerance. emption from the requirement of a Residues of the biochemical pesticide tolerance. cold pressed neem oil are exempt from An exemption from the requirement the requirement of a tolerance in or on of a tolerance is established for the res- all food commodities. idues of Extract of Chenopodium [74 FR 55463, Oct. 28, 2009] ambrosioides near ambrosioides when used as an insecticide/acaricide on all § 180.1292 Ulocladium oudemansii (U3 food commodities. Strain); exemption from the re- [74 FR 634, Jan. 7, 2009] quirement of a tolerance. An exemption from the requirement § 180.1288 Tristyrylphenol ethoxylates; of a tolerance is established in/on all exemption from the requirement of food commodities for residues of a tolerance. Ulocladium oudemansii (U3 Strain), An exemption from the requirement when applied or used pre-harvest-only, of a tolerance is established for resi- excluding applications made post-har- dues of poly(oxy-1,2-ethanediyl), a- vest or to processed commodities, as a [2,4,6-tris(1-phenylethyl)phenyl]-w-hy- microbial fungicide in accordance with droxy-, (CAS Reg. No. 70559–25–0) and good agricultural practices. poly(oxy-1,2-ethanediyl), a-[tris(1- phenylethyl)phenyl]-w-hydroxy-, (CAS [74 FR 55458, Oct. 28, 2009] Reg. No. 99734–09–5) on citrus crops, group 10, when used as inert ingredi- § 180.1293 Trichoderma gamsii strain ents under the following conditions: ICC 080; exemption from the re- (a) They are applied post-harvest; quirement of a tolerance. (b) They are used as inert ingredients Trichoderma gamsii strain ICC 080 is in pesticide formulations with exempted from the requirement of a azoxystrobin and fludioxonil; and tolerance in or on all food and feed (c) They constitute no more than commodities when applied preharvest 10.0% of the formulated pesticide prod- and used in accordance with good agri- uct. cultural practices. [74 FR 12625, Mar. 25, 2009] [75 FR 8507, Feb. 25, 2010]

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§ 180.1294 Trichoderma asperellum plied as a fungicide and used in accord- strain ICC 012; exemption from the ance with good agricultural practices. requirement of a tolerance. [75 FR 43076, July 23, 2010] Trichoderma asperellum strain ICC 012 is exempted from the requirement of a § 180.1299 Prohydrojasmon; exemption tolerance in or on all food and feed from the requirement of a toler- commodities when applied pre-harvest ance. and used in accordance with good agri- An exemption from the requirement cultural practices. of a tolerance is established for resi- [75 FR 9530, Mar. 3, 2010] dues of the biochemical pesticide prohydrojasmon (PDJ), propyl-3-oxo-2- § 180.1295 Laminarin; exemption from pentylcyclo-pentylacetate, when used the requirement of a tolerance. as a plant growth regulator in or on apple and grape pre-harvest, in accord- An exemption from the requirement ance with label directions and good ag- of a tolerance is established for resi- ricultural practices. dues of laminarin in or on all food com- modities when laminarin is applied [78 FR 75257, Dec. 11, 2013] preharvest. § 180.1300 Potassium hypochlorite; ex- [75 FR 8256, Feb. 24, 2010] emption from the requirement of a tolerance. § 180.1296 Terpene Constituents α-ter- pinene, d-limonene and p-cymene, An exemption from the requirement of the Extract of Chenopodium of a tolerance is established for resi- ambrosioides near ambrosioides as dues of potassium hypochlorite in or on Synthetically Manufactured; exemp- all commodities. tion from the requirement of a tol- erance. [76 FR 11343, Mar. 2, 2011] An exemption from the requirement § 180.1301 Escherichia coli O157:H7 of a tolerance is established for the res- specific bacteriophages; temporary idues of the biochemical pesticide Ter- exemption from the requirement of pene Constituents a-terpinene, d-limo- a tolerance. nene and p-cymene, of the Extract of A temporary exemption from the re- Chenopodium ambrosioides near quirement of a tolerance is established ambrosioides as Synthetically Manufac- for residues of lytic bacteriophages tured when used as an insecticide/acar- that are specific to Escherichia coli icide in or on all food commodities. O157:H7, sequence negative for shiga [75 FR 39455, July 9, 2010] toxins I and II, and grown on atoxigenic host bacteria when used/ap- § 180.1297 Homobrassinolide; exemp- plied on food contact surfaces in food tion from the requirement of a tol- processing plants in accordance with erance. the terms of Experimental Use Permit An exemption from the requirement (EUP) No. 74234–EUP–2. This temporary of a tolerance is established for the res- exemption expires on April 1, 2013. idues of homobrassinolide in or on all [76 FR 20546, Apr. 13, 2011] food commodities when applied/used as a plant growth regulator in accordance § 180.1302 Sodium Ferric Ethylene- with good agricultural practices. diaminetetraacetate (EDTA); ex- emption from the requirement of a [75 FR 39459, July 9, 2010] tolerance. § 180.1298 Trichoderma hamatum iso- An exemption from the requirement late 382; exemption from the re- of a tolerance is established for resi- quirement of a tolerance. dues of sodium ferric EDTA in or on all food commodities when applied as a An exemption from the requirement molluscicide and used in accordance of a tolerance is established for resi- with good agricultural practices. dues of Trichoderma hamatum isolate 382 in or on all food commodities when ap- [76 FR 17561, Mar. 30, 2011]

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§ 180.1303 Metarhizium anisopliae michiganensis produced in Clavibacter strain F52; exemption from the re- michiganensis subspecies quirement of a tolerance. michiganensis in or on tomato when An exemption from the requirement applied as a bactericide in accordance of a tolerance is established for resi- with good agricultural practices. dues of Metarhizium anisopliae strain [76 FR 66192, Oct. 26, 2011] F52 in or on all food commodities when applied as an insecticide, miticide, or § 180.1308 Bacillus amyloliquefaciens ixodicide and used in accordance with strain D747; exemption from the re- good agricultural practices. quirement of a tolerance. [76 FR 26198, May 6, 2011] An exemption from the requirement of a tolerance is established for resi- § 180.1304 Pseudomonas fluorescens strain CL145A; exemption from the dues of the microbial pesticide, Bacillus requirement of a tolerance. amyloliquefaciens strain D747 in or on all food commodities when used in ac- An exemption from the requirement of a tolerance is established for resi- cordance with good agricultural prac- dues of Pseudomonas fluorescens strain tices. CL145A in or on all food commodities [77 FR 749, Jan. 6, 2012. Redesignated at 77 when applied as a molluscicide. FR 2911, Jan. 20, 2012] [76 FR 52875, Aug. 24, 2011] § 180.1309 Bacillus subtilis strain CX– § 180.1305 Chromobacterium 9060; exemption from the require- subtsugae strain PRAA4–1T; exemp- ment of a tolerance. tion from the requirement of a tol- An exemption from the requirement erance. of a tolerance is established for resi- An exemption from the requirement dues of the microbial pesticide Bacillus of a tolerance is established for resi- subtilis strain CX–9060, in or on all food dues of Chromobacterium subtsugae commodities, when applied or used in strain PRAA4–1T in or on all food com- accordance with good agricultural modities when applied as an insecticide practices. or miticide and used in accordance with good agricultural practices. [77 FR 1637, Jan. 11, 2012] [76 FR 55272, Sept. 7, 2011] § 180.1310 Trichoderma virens strain G–41; exemption from the require- § 180.1306 Isaria fumosorosea (for- ment of a tolerance. merly Paecilomyces fumosoroseus) Apopka strain 97; exemption from An exemption from the requirement the requirement of a tolerance. of a tolerance is established for resi- An exemption from the requirement dues of Trichoderma virens strain G–41, of a tolerance is established for resi- in or on all food commodities, when ap- dues of Isaria fumosorosea (formerly plied as a fungicide and used in accord- Paecilomyces fumosoroseus) Apopka ance with good agricultural practices. strain 97 in or on all food commodities when applied as an insecticide or [77 FR 4908, Feb. 1, 2012] miticide and used in accordance with § 180.1311 Pasteuria nishizawae—Pn1; good agricultural practices. exemption from the requirement of [76 FR 59905, Sept. 28, 2011] a tolerance. An exemption from the requirement § 180.1307 Bacteriophage of Clavibacter michiganensis sub- of a tolerance is established for resi- species michiganensis; exemption dues of Pasteuria nishizawae—Pn1 in or from the requirement of a toler- on all food commodities when applied ance. as a nematicide and used in accordance An exemption from the requirement with good agricultural practices. of a tolerance is established for resi- [77 FR 8741, Feb. 15, 2012] dues of lytic bacteriophage of Clavibacter michiganensis subspecies

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§ 180.1312 Aureobasidium pullulans § 180.1316 Pasteuria spp. strains DSM 14940 and DSM 14941; (Rotylenchulus reniformis nema- exemption from the requirement of tode)—Pr3; exemption from the re- a tolerance. quirement of a tolerance. An exemption from the requirement An exemption from the requirement of a tolerance is established for resi- of a tolerance is established for resi- dues of the microbial pesticides, dues of Pasteuria spp. (Rotylenchulus Aureobasidium pullulans strains DSM reniformis nematode)—Pr3 in or on all 14940 and DSM 14941 in or on all food food commodities when applied as a commodities when applied preharvest nematicide and used in accordance and used in accordance with good agri- with label directions and good agricul- cultural practices. tural practices. [77 FR 8736, Feb. 15, 2012] [77 FR 40276, July 9, 2012]

§ 180.1313 Bacillus pumilus strain § 180.1317 Pesticide chemicals; exemp- GHA 180; exemption from the re- tion from the requirements of a tol- quirement of a tolerance. erance. An exemption from the requirement An exemption from the requirement of a tolerance is established for resi- of a tolerance is established for resi- dues of Bacillus pumilus strain GHA 180 dues of Didecyl dimethyl ammonium in or on all food commodities when chloride in or on broccoli resulting used in accordance with good agricul- from the use of Didecyl dimethyl am- tural practices. monium chloride as a seed treatment at a treatment concentration of 1200 [77 FR 19112, Mar. 30, 2012] ppm prior to planting by immersion. § 180.1314 Killed, nonviable [77 FR 47296, Aug. 8, 2012] Streptomyces acidiscabies strain RL–110T; exemption from the re- § 180.1318 3-decen-2-one; exemption quirement of a tolerance. from the requirement of a toler- An exemption from the requirement ance. of a tolerance is established for resi- An exemption from the requirement dues of killed, nonviable Streptomyces of a tolerance is established for resi- acidiscabies strain RL–110T in or on all dues of the biochemical pesticide, 3- food commodities when applied as a decen-2-one, in or on potatoes when ap- pre- or post-emergent herbicide and plied as a potato sprout inhibitor and used in accordance with good agricul- used in accordance with label direc- tural practices. tions and good agricultural practices. [77 FR 35295, June 13, 2012] [78 FR 11766, Feb. 20, 2013]

§ 180.1315 Natamycin; exemption from § 180.1319 Banda de Lupinus albus the requirement of a tolerance. doce (BLAD); exemption from the An exemption from the requirement requirement of a tolerance. of a tolerance is established for resi- An exemption from the requirement dues of natamycin in or on mushrooms of a tolerance is established for the res- when applied as a fungistat to prevent idues of Banda de Lupinus albus doce the germination of fungal spores on (BLAD), a naturally occurring mushrooms produced in enclosed mush- polypeptide from the catabolism of a room production facilities, and in or on seed storage protein (b-conglutin) of pineapples when applied as a fungistat sweet lupines (Lupinus albus), in or on in accordance with label directions and all food commodities when applied as a good agricultural practices. fungicide and used in accordance with label directions and good agricultural [79 FR 75068, Dec. 17, 2014] practices. [78 FR 17604, Mar. 22, 2013]

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§ 180.1320 Methyl jasmonate; exemp- ance with label directions and good ag- tion from the requirement of a tol- ricultural practices. erance. [79 FR 10685, Feb. 26, 2014] An exemption from the requirement of a tolerance is established for resi- § 180.1325 Heat-killed Burkholderia dues of methyl jasmonate in or on all spp. strain A396 cells and spent fer- mentation media exemption from food commodities when methyl the requirement of a tolerance. jasmonate is applied pre-harvest. An exemption from the requirement [78 FR 22794, Apr. 17, 2013] of a tolerance is established for resi- dues of heat-killed Burkholderia spp. § 180.1321 Complex Polymeric strain A396 cells and spent fermenta- Polyhydroxy Acids; exemption from tion media in or on all food commod- the requirement of a tolerance. ities when applied as a biological insec- An exemption from the requirement ticide to agricultural crops and used in of a tolerance is established for the res- accordance with label directions and idues of complex polymeric good agricultural practices. polyhydroxy acids in or on all food [79 FR 15704, Mar. 21, 2014] commodities when applied as a plant growth regulator and used in accord- § 180.1326 Pseudomonas fluorescens ance with good agricultural practices. strain D7; exemption from the re- quirement of a tolerance. [78 FR 46267, July 31, 2013] An exemption from the requirement of a tolerance is established for resi- § 180.1322 Bacillus pumilus strain BU dues of Pseudomonas fluorescens strain F–33; exemption from the require- D7 in or on all food commodities when ment of a tolerance. used in accordance with label direc- An exemption from the requirement tions and good agricultural practices. of a tolerance is established for resi- dues of Bacillus pumilus strain BU F–33 [79 FR 60750, Oct. 8, 2014] in or on all food commodities when ap- § 180.1327 Tetraacetylethylenediamine plied to elicit induced systemic resist- (TAED) and its metabolite ance in plants and used in accordance Diacetylethylenediamine (DAED); with label directions and good agricul- exemption from the requirement of tural practices. a tolerance. An exemption from the requirement [78 FR 35149, June 12, 2013] of a tolerance is established for resi- dues of the pesticide, § 180.1323 Ethyl-2E,4Z-decadienoate (Pear Ester); exemption from the tetraacetylethylenediamine (TAED), requirement of a tolerance. and its metabolite diacetylethylenediamine (DAED), in or An exemption from the requirement on rice and strawberries, when used as of a tolerance is established for resi- a fungicide and bactericide in accord- dues of the biochemical pesticide, ance with label directions and good ag- ethyl-2E,4Z-decadienoate (pear ester), ricultural practices. in or on all food commodities, when used in accordance with label direc- [79 FR 59121, Oct. 1, 2014] tions and good agricultural practices. § 180.1328 Beauveria bassiana strain [78 FR 53054, Aug. 28, 2013] ANT–03; exemption from the re- quirement of a tolerance. § 180.1324 GS-omega/kappa-Hxtx-Hv1a; An exemption from the requirement exemption from the requirement of of a tolerance is established for resi- a tolerance. dues of Beauveria bassiana strain ANT– An exemption from the requirement 03 in or on all food commodities, when of a tolerance is established for resi- applied as a microbial insecticide and dues of the pesticide GS-omega/kappa- used in accordance with label direc- Hxtx-Hv1a in or on all food commod- tions and good agricultural practices. ities when applied or used in accord- [79 FR 77396, Dec. 24, 2014]

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§ 180.1329 Bacillus subtilis strain IAB/ Subpart E—Pesticide Chemicals BS03, exemption from the require- Not Requiring a Tolerance or ment of a tolerance. an Exemption From a Toler- An exemption from the requirement ance of a tolerance is established for resi- dues of Bacillus subtilis strain IAB/BS03 SOURCE: 66 FR 66772, Dec. 27, 2001, unless in or on all food commodities when otherwise noted. used in accordance with label direc- tions and good agricultural practices. § 180.2000 Scope. [80 FR 9217, Feb. 20, 2015] This subpart sets forth the pesticide chemicals for use in agricultural or § 180.1330 1-Octanol; exemption from other food-related settings for which the requirement of a tolerance. neither a tolerance nor an exemption is deemed to be needed by EPA. An exemption from the requirement of a tolerance is established for resi- § 180.2003 Definitions. dues of 1-octanol in or on root and (a) Food uses are the uses of a pes- tuber vegetables when applied as a ticide chemical that are likely to yield plant growth regulator in accordance residues in food or feed crops, meat, with label directions and good agricul- milk, poultry or egg. tural practices. (b) Non-food uses are those uses that [80 FR 25953, May 6, 2015] are not likely to yield residues in food or feed crops, meat, milk, poultry or § 180.1331 Trichoderma asperelloides egg. strain JM41R; exemption from the [66 FR 66772, Dec. 27, 2001, as amended at 73 requirement of a tolerance. FR 60158, Oct. 10, 2008] An exemption from the requirement of a tolerance is established for resi- § 180.2010 Threshold of regulation de- terminations. dues of Trichoderma asperelloides strain JM41R in or on all food commodities The following pesticide chemical uses when used in accordance with label di- on food or feed, or food or feed crops, rections and good agricultural prac- do not need a tolerance or exemption tices. from the requirement of a tolerance, and may be registered under the Fed- [80 FR 28203, May 18, 2015] eral Insecticide, Fungicide, and Rodenticide Act, 7 U.S.C. 136 et seq., without obtaining such tolerance or ex- emption, based on EPA’s determina- tion that the uses are below the thresh- old of regulation.

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Pesticide Chemical CAS Reg. No. Use/Limits Analytical Method

Thiabendazole 148–79–8 As a seed treatment for dry pea (including field pea, pigeon High Perform- pea, chickpea or lentil), using a maximum application rate of ance Liquid 0.075 pounds of active ingredient per 100 pounds of seed. Chroma- Vines or hay grown from treated seed may not be fed to live- tography/Flo- stock.. rescence De- tector method 1; Modification of Ion-Pairing Liq- uid Chromatograp- hic Determina- tion of Benz- imidazole Fun- gicides in Foods, Gilvydis and Walters, JAOAC, vol. 73, no. 5, 1990. 1Available from: Chief, Analytical Chemistry Branch, Environmental Science Center, 701 Mapes Rd., Ft. Meade, MD 20755– 5350; telephone number: (410) 305–2905; e-mail address: [email protected]

[73 FR 1978, Jan. 11, 2008]

§ 180.2020 Non-food determinations. from the requirement of a tolerance based on EPA’s determination that The following pesticide chemical uses they are not likely to result in residues do not need a tolerance or exemption in or on food.

Pesticide Chemical CAS Reg. No. Limits Uses

Methyl bromide 74–83–9 When applied as a pre-plant soil fumigant All pre-plant soil uses Potassium 12298–68–9 When applied to growing crops in foreign countries Bananas, grapes, triiodide (KI3) and melons Rhodamine B 81–88–9 Not to exceed 2% by weight of the formulated product and 60 ppm on Dye for seed treat- the treated seed ment

[66 FR 66772, Dec. 27, 2001, as amended at 70 FR 40201, July 13, 2005; 71 FR 45402, Aug. 9, 2006]

PARTS 181–189 [RESERVED]

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