388 Subpart G—Judicial Review PART 180—TOLERANCES and EX

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§ 179.125 40 CFR Ch. I (7–1–14 Edition)

or case to the Administrator when ap- Rulemaking, and the information sub- propriate. mitted as part of the comments, the Administrator’s response to comments [55 FR 50293, Dec. 5, 1990, as amended at 57 FR 28087, June 24, 1992; 77 FR 46292, Aug. 3, and the documents or information re- 2012] lied on by the Administrator in issuing the regulation or order. Subpart G—Judicial Review (5) All other documents or information submitted to the docket for the § 179.125 Judicial review. rulemaking in question under parts 177 or part 180 of this chapter. (a) The Administrator’s final decision (6) The Notice of Hearing published is final agency action reviewable in the under § 179.20. courts as provided by FFDCA section (7) All notices of participation filed 408(h), as of the date of publication of under § 179.42. the order in the FEDERAL REGISTER. (8) Any FEDERAL REGISTER notice The failure of a person to file a petition issued under this part that pertains to for judicial review within the period the proceeding. ending on the 60th day after the date of (9) All submissions filed under the publication of the order constitutes § 179.80. a waiver under FFDCA section 408(h) of (10) Any document of which official the right to judicial review of the order notice was taken under § 179.95. and of any regulation promulgated by (b) The record of the administrative the order. proceeding is closed: (b) The record for judicial review of a (1) With respect to the taking of evi- final decision under this part consists dence, when specified by the presiding of the record described in § 179.130. officer. [55 FR 50293, Dec. 5, 1990, as amended at 70 (2) With respect to pleadings, at the FR 33360, June 8, 2005] time specified in § 179.98(a) for the filing of briefs. § 179.130 Administrative record. (c) The presiding officer may reopen (a) For purposes of judicial review, the record to receive further evidence the record of a hearing that culminates at any time before the filing of the ini- in a final decision of the Administrator tial decision. under § 179.105(d) or § 179.112(c) ruling on [55 FR 50293, Dec. 5, 1990, as amended at 70 an objection shall consist of: FR 33360, June 8, 2005] (1) The objection ruled on (and any request for hearing that was included PART 180—TOLERANCES AND EX- with the objection). (2) Any order issued under § 180.7(g) of EMPTIONS FOR PESTICIDE CHEM- this chapter to which the objection re- ICAL RESIDUES IN FOOD lated, and: (i) The regulation or petition denial Subpart A—Definitions and Interpretative that was the subject of that order. Regulations (ii) The petition to which such order Sec. responded. 180.1 Definitions and interpretations. (iii) Any amendment or supplement 180.3 Tolerances for related pesticide chemi- of the petition. cals. (iv) The data and information sub- 180.4 Exceptions. mitted in support of the petition. 180.5 Zero tolerances. 180.6 Pesticide tolerances regarding milk, (v) The notice of filing of the peti- eggs, meat, and/or poultry; statement of tion. policy. (3) Any order issued under § 180.29(f) of this chapter to which the objection Subpart B—Procedural Regulations related, the regulation that was the subject of that order, and each related 180.7 Petitions proposing tolerances or exemptions for pesticide residues in or on Notice of Proposed Rulemaking. raw agricultural commodities or proc- (4) The comments submitted by mem- essed foods. bers of the public in response to the 180.8 Withdrawal of petitions without preju- Notice of Filing or Notice of Proposed dice.

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180.9 Substantive amendments to petitions. 180.183 Disulfoton; tolerances for residues. 180.29 Establishment, modification, and rev- 180.184 Linuron; tolerances for residues. ocation of tolerance on initiative of Ad- 180.185 DCPA; tolerances for residues. ministrator. 180.189 Coumaphos; tolerances for residues. 180.30 Judicial review. 180.190 Diphenylamine; tolerances for resi- 180.31 Temporary tolerances. dues. 180.32 Procedure for modifying and revoking 180.191 Folpet; tolerances for residues. tolerances or exemptions from toler- 180.198 Trichlorfon; tolerances for residues. ances. 180.200 Dicloran; tolerances for residues. 180.33 Fees. 180.202 p-Chlorophenoxyacetic acid; toler- 180.34 Tests on the amount of residue re- ances for residues. maining. 180.204 Dimethoate; tolerances for residues. 180.35 Tests for potentiation. 180.205 Paraquat; tolerances for residues. 180.40 Tolerances for crop groups. 180.206 Phorate; tolerances for residues. 180.41 Crop group tables. 180.207 Trifluralin; tolerances for residues. 180.208 Benfluralin; tolerances for residues. Subpart C—Specific Tolerances 180.209 Terbacil; tolerances for residues. 180.210 Bromacil; tolerances for residues. 180.101 Specific tolerances; general provi- 180.211 Propachlor; tolerances for residues. sions. 180.212 S-Ethyl cyclohexylethylthiocarba- 180.103 Captan; tolerances for residues. mate; tolerances for residues. 180.106 Diuron; tolerances for residues. 180.213 Simazine; tolerances for residues. 180.108 Acephate; tolerances for residues. 180.215 Naled; tolerances for residues. 180.110 Maneb; tolerances for residues. 180.217 Metiram; tolerances for residues. 180.111 Malathion; tolerances for residues. 180.220 Atrazine; tolerances for residues. 180.114 Ferbam; tolerances for residues. 180.222 Prometryn; tolerances for residues. 180.116 Ziram; tolerances for residues. 180.225 Phosphine; tolerances for residues. 180.117 S-Ethyl dipropylthiocarbamate; tol- 180.226 Diquat; tolerances for residues. erances for residues. 180.227 Dicamba; tolerances for residues. 180.121 Methyl parathion; tolerances for res- 180.229 Fluometuron; tolerances for resi- idues. dues. 180.123 Inorganic bromide residues resulting 180.231 Dichlobenil; tolerances for residues. from fumigation with methyl bromide; 180.232 Butylate; tolerances for residues. tolerances for residues. 180.235 Dichlorvos; tolerances for residues. 180.123a Inorganic bromide residues in pea- 180.236 Triphenyltin hydroxide; tolerances nut hay and peanut hulls; statement of for residues. policy. 180.241 Bensulide; tolerances for residues. 180.124 Methyl bromide; tolerances for resi- 180.242 Thiabendazole; tolerances for residues. dues. 180.127 Piperonyl butoxide; tolerances for 180.243 Propazine; tolerances for residues. residues. 180.245 Streptomycin; tolerances for resi- 180.128 Pyrethrins; tolerances for residues. dues. 180.129 o-Phenylphenol and its sodium salt; 180.249 Alachlor; tolerances for residues. tolerances for residues. 180.252 Tetrachlorvinphos; tolerances for 180.130 Hydrogen Cyanide; tolerances for residues. residues. 180.253 Methomyl; tolerances for residues. 180.132 Thiram; tolerances for residues. 180.254 Carbofuran; tolerances for residues. 180.142 2,4-D; tolerances for residues. 180.257 Chloroneb; tolerances for residues. 180.145 Fluorine compounds; tolerances for 180.258 Ametryn; tolerances for residues. residues. 180.259 Propargite; tolerances for residues. 180.151 Ethylene oxide; tolerances for resi- 180.261 Phosmet; tolerances for residues. dues. 180.262 Ethoprop; tolerances for residues. 180.153 Diazinon; tolerances for residues. 180.263 Phosalone; tolerances for residues. 180.154 Azinphos-methyl; tolerances for resi- 180.269 Aldicarb; tolerances for residues. dues. 180.272 Tribuphos; tolerances for residues. 180.155 1-Naphthaleneacetic acid; tolerances 180.274 Propanil; tolerances for residues. for residues. 180.275 Chlorothalonil; tolerances for resi- 180.163 Dicofol; tolerances for residues. dues. 180.169 Carbaryl; tolerances for residues. 180.276 Formetanate hydrochloride; toler- 180.172 Dodine; tolerances for residues. ances for residues. 180.175 Maleic hydrazide; tolerances for resi- 180.278 Phenmedipham; tolerances for residues. dues. 180.176 Mancozeb; tolerances for residues. 180.284 Zinc phosphide; tolerances for resi- 180.178 Ethoxyquin; tolerances for residues. dues. 180.181 Chlorpropham; tolerances for resi- 180.287 Amitraz; tolerances for residues. dues. 180.288 2-(Thiocyanomethylthio) 180.182 Endosulfan; tolerances for residues. benzothiazole; tolerances for residues.

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180.289 Methanearsonic acid; tolerances for 180.377 Diflubenzuron; tolerances for resi- residues. dues. 180.291 Pentachloronitrobenzene; tolerance 180.378 Permethrin; tolerances for residues. for residues. 180.380 Vinclozolin; tolerances for residues. 180.292 Picloram; tolerances for residues. 180.381 Oxyfluorfen; tolerances for residues. 180.293 Endothall; tolerances for residues. 180.383 Sodium salt of acifluorfen; toler- 180.297 N-1-Naphthyl phthalamic acid; tolerances for residues. ances for residues. 180.384 Mepiquat (N,N-dimethylpiperidin- 180.298 Methidathion; tolerances for resi- ium); tolerances for residues. dues. 180.385 Diclofop-methyl; tolerances for resi- 180.299 Dicrotophos; tolerances for residues. dues. 180.300 Ethephon; tolerances for residues. 180.388–180.389 [Reserved] 180.301 Carboxin; tolerances for residues. 180.390 Tebuthiuron; tolerances for residues. 180.303 Oxamyl; tolerances for residues. 180.395 Hydramethylnon; tolerances for resi- 180.304 Oryzalin; tolerances for residues. dues. 180.311 Cacodylic acid; tolerances for resi- 180.396 Hexazinone; tolerances for residues. dues. 180.399 Iprodione; tolerances for residues. 180.314 Triallate; tolerances for residues. 180.401 Thiobencarb; tolerances for residues. 180.315 Methamidophos; tolerances for resi- 180.403 Thidiazuron; tolerances for residues. dues. 180.404 Profenofos; tolerances for residues. 180.316 Pyrazon; tolerances for residues. 180.405 Chlorsulfuron; tolerances for resi- 180.317 Propyzamide; tolerances for residues. dues. 180.407 Thiodicarb; tolerances for residues. 180.318 4-(2-Methyl-4-chlorophenoxy) bu- 180.408 Metalaxyl; tolerances for residues. tyric acid; tolerance for residues. 180.409 Pirimiphos-methyl; tolerances for 180.319 Interim tolerances. residues. 180.324 Bromoxynil; tolerances for residues. 180.410 Triadimefon; tolerances for residues. 180.328 Napropamide; tolerances for resi- 180.411 Fluazifop-P-butyl; tolerances for res- dues. idues. 180.330 S-(2-(Ethylsulfinyl)ethyl) O,O-di- 180.412 Sethoxydim; tolerances for residues. methyl phosphorothioate; tolerances for 180.413 Imazalil; tolerances for residues. residues. 180.414 Cyromazine; tolerances for residues. 180.331 4-(2,4-Dichlorophenoxy) butyric acid; 180.415 Aluminum tris (O-ethylphospho- tolerances for residues. nate); tolerances for residues. 180.332 Metribuzin; tolerances for residues. 180.416 Ethalfluralin; tolerances for resi- 180.337 Oxytetracycline; tolerances for residues. dues. 180.417 Triclopyr; tolerances for residues. 180.339 MCPA; tolerances for residues. 180.418 Cypermethrin and an isomer zeta- 180.341 2,4-Dinitro-6-octylphenyl crotonate cypermethrin; tolerances for residues. and 2,6-dinitro-4-octylphenyl crotonate; 180.419 Chlorpyrifos-methyl; tolerances for tolerances for residues. residues. 180.342 Chlorpyrifos; tolerances for residues. 180.420 Fluridone; tolerances for residues. 180.345 Ethofumesate; tolerances for resi- 180.421 Fenarimol; tolerances for residues. dues. 180.422 Tralomethrin; tolerances for resi- 180.349 Fenamiphos; tolerances for residues. dues. 180.350 Nitrapyrin; tolerances for residues. 180.425 Clomazone; tolerances for residues. 180.352 Terbufos; tolerances for residues. 180.426 2-[4,5-Dihydro-4-methyl-4-(1- 180.353 Desmedipham; tolerances for resi- methylethyl)-5-oxo-1H-imidazol-2-yl]-3- dues. quinoline carboxylic acid; tolerance for 180.355 Bentazon; tolerances for residues. residues. 180.356 Norflurazon; tolerances for residues. 180.427 Tau-Fluvalinate; tolerances for resi- 180.360 Asulam; tolerance for residues. dues. 180.361 Pendimethalin; tolerances for resi- 180.428 Metsulfuron methyl; tolerances for dues. residues. 180.362 Fenbutatin-oxide; tolerances for res- 180.429 Chlorimuron ethyl; tolerances for idues. residues. 180.364 Glyphosate; tolerances for residues. 180.430 Fenoxaprop-ethyl; tolerances for res- 180.367 n-Octyl bicycloheptenedicarbox- idues. imide; tolerances for residues. 180.431 Clopyralid; tolerances for residues. 180.368 Metolachlor; tolerances for residues. 180.432 Lactofen; tolerances for residues. 180.370 5-Ethoxy-3-(trichloromethyl)-1, 2, 4- 180.433 Fomesafen; tolerances for residues. thiadiazole; tolerances for residues. 180.434 Propiconazole; tolerances for resi- 180.371 Thiophanate-methyl; tolerances for dues. residues. 180.435 Deltamethrin; tolerances for resi- 180.372 2,6-Dimethyl-4-tridecylmorpholine; dues. tolerances for residues. 180.436 Cyfluthrin and the isomer beta- 180.373 [Reserved] cyfluthrin; tolerances for residues.

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180.437 Methyl 2-(4-isopropyl-4-methyl-5- 180.478 Rimsulfuron; tolerances for residues. oxo-2-imidazolin-2-yl)-p-toluate and 180.479 Halosulfuron-methyl; tolerances for methyl 6-(4-isopropyl-4-methyl-5-oxo-2- residues. imidazolin-2-yl)-m-toluate; tolerances for 180.480 Fenbuconazole; tolerances for resi- residues. dues. 180.438 Lambda-cyhalothrin and an isomer 180.481 Prosulfuron; tolerances for residues. gamma-cyhalothrin; tolerances for resi- 180.482 Tebufenozide; tolerances for residues. dues. 180.439 Thifensulfuron methyl; tolerances 180.484 Flutolanil; tolerances for residues. for residues. 180.485 Cyproconazole; tolerances for resi- 180.440 Tefluthrin; tolerances for residues. dues. 180.441 Quizalofop ethyl; tolerances for resi- 180.486 Chlorethoxyfos; tolerances for residues. dues. 180.442 Bifenthrin; tolerances for residues. 180.487 Pyrithiobac sodium; tolerances for 180.443 Myclobutanil; tolerances for resi- residues. dues. 180.490 Imazapic; tolerances for residues. 180.444 Sulfur dioxide; tolerances for resi- 180.491 Propylene oxide; tolerances for residues. dues. 180.445 Bensulfuron methyl; tolerances for 180.492 Triflusulfuron-methyl; tolerances residues. for residues. 180.446 Clofentezine; tolerances for residues. 180.493 Dimethomorph; tolerances for resi- 180.447 Imazethapyr; tolerances for residues. dues. 180.448 Hexythiazox; tolerance for residues. 180.494 Pyridaben; tolerance for residues. 180.449 Avermectin B1 and its delta-8,9-iso- 180.495 Spinosad; tolerances for residues. mer; tolerances for residues. 180.496 Thiazopyr; tolerances for residues. 180.450 Beta-(4-Chlorophenoxy)-alpha-(1,1- 180.497 Clofencet; tolerances for residues. dimethylethyl)-1H-1,2,4-triazole-1-eth- 180.498 Sulfentrazone; tolerances for resi- anol; tolerances for residues. dues. 180.451 Tribenuron methyl; tolerances for 180.499 Propamocarb; tolerances for resi- residues. dues. 180.452 Primisulfuron-methyl; tolerances for 180.500 Imazapyr; tolerances for residues. residues. 180.501 Hydroprene; tolerances for residues. 180.454 Nicosulfuron; tolerances for resi- 180.502 Aminoethoxyvinylglycine hydro- dues. chloride (aviglycine HCl); tolerances for 180.455 Procymidone; tolerances for resi- residues. dues. 180.503 Cymoxanil, tolerance for residues. 180.457 Bitertanol; tolerances for residues. 180.504 [Reserved] 180.458 Clethodim; tolerances for residues. 180.505 Emamectin; tolerances for residues. 180.459 Triasulfuron; tolerances for residues. 180.506 Cyclanilide; tolerances for residues. 180.460 Benoxacor; tolerances for residues. 180.507 Azoxystrobin; tolerances for resi- 180.461 Cadusafos; tolerances for residues. dues. 180.462 Pyridate; tolerances for residues. 180.509 Mefenpyr-diethyl; tolerance for resi- 180.463 Quinclorac; tolerances for residues. dues. 180.464 Dimethenamid; tolerances for resi- 180.510 Pyriproxyfen; tolerances for residues. dues. 180.465 4-(Dichloroacetyl)-1-oxa-4- 180.511 Buprofezin; tolerances for residues. azaspiro[4.5]decane. 180.512 [Reserved] 180.466 Fenpropathrin; tolerances for resi- 180.513 Chlorfenapyr; tolerances for residues. dues. 180.467 Carbon disulfide; tolerances for resi- 180.514 Cloransulam-methyl; tolerances for dues. residues. 180.468 Flumetsulam; tolerances for resi- 180.515 Carfentrazone-ethyl; tolerances for dues. residues. 180.469 Dichlormid; tolerances for residues. 180.516 Fludioxonil; tolerances for residues. 180.470 Acetochlor; tolerances for residues. 180.517 Fipronil; tolerances for residues. 180.471 Furilazole; tolerances for residues. 180.518 Pyrimethanil; tolerances for resi- 180.472 Imidacloprid; tolerances for residues. dues. 180.519 Bromide ion and residual bromine; 180.473 Glufosinate ammonium; tolerances tolerances for residues. for residues. 180.521 Fumigants for grain-mill machinery; 180.474 Tebuconazole; tolerances for resi- tolerances for residues. dues. 180.522 Fumigants for processed grains used 180.475 Difenoconazole; tolerances for resi- in production of fermented malt bev- dues. erage; tolerances for residues. 180.476 Triflumizole; tolerances for residues. 180.523 Metaldehyde; tolerances for resi- 180.477 Flumiclorac pentyl; tolerances for dues. residues. 180.525 Resmethrin; tolerances for residues.

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180.526 Synthetic isoparaffinic petroleum 180.569 Forchlorfenuron; tolerances for resi- hydrocarbons; tolerances for residues. dues. 180.527 Flufenacet, N-(4-fluorophenyl)-N-(1- 180.570 Isoxadifen-ethyl; tolerances for resi- methylethyl)-2-[[5-(trifluoromethyl)-1, 3, dues. 4-thiadiazol-2-yl] oxy]acetamide and its 180.571 Mesotrione; tolerances for residues. metabolites containing the 4-fluoro-N- 180.572 Bifenazate; tolerance for residues. methylethyl benzenamine tolerances for 180.573 Tepraloxydim; tolerances for resi- residues. dues. 180.530 2,2-Dimethyl-1,3-benzodioxol-4-ol 180.574 Fluazinam; tolerances for residues. methylcarbamate; tolerances for resi- 180.575 Sulfuryl fluoride; tolerances for residues. dues. 180.532 Cyprodinil; tolerances for residues. 180.576 Cyhalofop-butyl; tolerances for resi- 180.533 Esfenvalerate; tolerances for residues. dues. 180.577 Bispyribac-sodium; tolerances for 180.535 Fluroxypyr 1-methylheptyl ester; residues. tolerances for residues. 180.578 Acetamiprid; tolerances for residues. 180.537 Isoxaflutole; tolerances for residues. 180.579 Fenamidone; tolerances for residues. 180.539 d-Limonene; tolerances for residues. 180.580 Iodosulfuron-Methyl-Sodium; toler- 180.540 Fenitrothion; tolerances for resi- ances for residues. dues. 180.581 Iprovalicarb; tolerances for residues. 180.541 Propetamphos; tolerances for resi- 180.582 Pyraclostrobin; tolerances for residues. dues. 180.543 Diclosulam; tolerances for residues. 180.583 Triticonazole; tolerances for resi- 180.544 Methoxyfenozide; tolerances for residues. dues. 180.584 Tolylfluanid; tolerances for residues. 180.545 Prallethrin (RS)-2-methyl-4-oxo-3-(2- 180.585 Pyraflufen-ethyl; tolerances for resi- propynyl)cyclopent-2-enyl (1RS)-cis, dues. 180.586 Clothianidin; tolerances for residues. trans-chrysanthemate; tolerances for res- 180.587 Famoxadone; tolerance for residues. idues. 180.588 Quinoxyfen; tolerances for residues. 180.546 Mefenoxam; tolerances for residues. 180.589 Boscalid; tolerances for residues. 180.547 Prohexadione calcium; tolerances 180.590 2, 6-Diisopropylnaphthalene (2, 6- for residues. DIPN); tolerances for residues. 180.548 Tralkoxydim; tolerances for resi- 180.591 Trifloxysulfuron; tolerances for residues. dues. 180.549 Diflufenzopyr; tolerances for resi- 180.592 Butafenacil; tolerances for residues. dues. 180.593 Etoxazole; tolerances for residues. 180.551 Fluthiacet-methyl; tolerances for 180.594 Thiacloprid; tolerances for residues. residues. 180.595 Flufenpyr-ethyl; tolerances for resi- 180.552 Sulfosulfuron; tolerances for residues. dues. 180.596 Fosthiazate; tolerances for residues. 180.553 Fenhexamid; tolerances for residues. 180.597 Mesosulfuron-methyl; tolerances for 180.554 Kresoxim-methyl; tolerances for res- residues. idues. 180.598 Novaluron; tolerances for residues. 180.555 Trifloxystrobin; tolerances for resi- 180.599 Acequinocyl; tolerances for residues. dues. 180.600 Propoxycarbazone; tolerances for 180.556 Pymetrozine; tolerances for resi- residues dues. 180.601 Cyazofamid; tolerances for residues. 180.557 Tetraconazole; tolerances for resi- 180.602 Spiroxamine; tolerances for residues. dues. 180.603 Dinotefuran; tolerances for residues. 180.559 Clodinafop-propargyl; tolerances for 180.604 Mepanipyrim; tolerances for resi- residues. dues. 180.560 Cloquintocet-mexyl; tolerances for 180.605 Penoxsulam; tolerances for residues. residues. 180.607 Spiromesifen; tolerances for resi- 180.561 Acibenzolar-S-methyl; tolerances for dues. residues. 180.608 Spirodiclofen; tolerances for resi- 180.562 Flucarbazone-sodium; tolerances for dues. residues. 180.609 Fluoxastrobin; tolerances for resi- 180.563 Ethametsulfuron-methyl; tolerances dues. for residues. 180.610 Aminopyralid; tolerances for resi- 180.564 Indoxacarb; tolerances for residues. dues. 180.565 Thiamethoxam; tolerances for resi- 180.611 Pinoxaden; tolerances for residues. dues. 180.612 Topramezone; tolerances for resi- 180.566 Fenpyroximate; tolerances for residues. dues. 180.613 Flonicamid; tolerances for residues. 180.567 Zoxamide; tolerances for residues. 180.614 Kasugamycin; tolerances for resi- 180.568 Flumioxazin; tolerances for residues. dues.

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180.615 Amicarbazone; tolerances for resi- 180.659 Pyroxasulfone; tolerances for residues. dues. 180.616 Fenpropimorph; tolerances for resi- 180.660 Pyriofenone; tolerances for residues. dues. 180.661 Fluopyram; tolerances for residues. 180.617 Metconazole; tolerances for residues. 180.662 Trinexapac-ethyl; tolerances for res- 180.618 Benthiavalicarb-isopropyl; tolerance idues. for residues. 180.663 Ametoctradin; tolerances for resi- 180.619 Epoxiconazole; tolerances for residues. dues. 180.664 Penflufen; tolerances for residues. 180.620 Etofenprox; tolerances for residues. 180.665 Sedaxane; tolerances for residues. 180.621 Dithianon; tolerances for residues. 180.666 Fluxapyroxad; tolerances for resi- 180.622 Ethaboxam; tolerances for residues. dues. 180.623 Flufenoxuron; tolerances for resi- 180.667 Cyflufenamid, tolerance for residues. dues. 180.668 Sulfoxaflor; tolerances for residues. 180.624 Metrafenone; tolerances for residues. 180.669 Picoxystrobin; tolerances for resi- 180.625 Orthosulfamuron; tolerances for res- dues. idues. 180.671 Fenpyrazamine; tolerances for resi- 180.626 Prothioconazole; tolerances for residues. dues. 180.672 Cyantraniliprole; tolerances for resi- 180.627 Fluopicolide; tolerances for residues. dues. 180.628 Chlorantraniliprole; tolerances for residues. 180.673 Triforine; tolerances for residues. 180.629 Flutriafol; tolerances for residues. 180.674 Proquinazid; tolerances for residues. 180.630 Flusilazole; tolerances for residues. 180.675 Tolfenpyrad; tolerances for residues. 180.631 Pyrasulfotole; tolerances for resi- 180.676 Fenpropidin; tolerances for residues. dues. 180.677 Cyflumetofen; tolerances for resi- 180.632 Fenazaquin; import tolerances for dues. residues. 180.678 Tricyclazole; tolerances for residues. 180.633 Florasulam; tolerances for residues. 180.634 Tembotrione; tolerances for resi- Subpart D—Exemptions From Tolerances dues. 180.900 Exemptions from the requirement of 180.635 Spinetoram; tolerances for residues. a tolerance. 180.636 1,3-dichloropropene; tolerances for 180.905 Pesticide chemicals; exemptions residues. 180.637 Mandipropamid; tolerances for resi- from the requirement of a tolerance. dues. 180.910 Inert ingredients used pre- and post- 180.638 Pyroxsulam; tolerances for residues. harvest; exemptions from the require- 180.639 Flubendiamide; tolerances for resi- ment of a tolerance. dues. 180.920 Inert ingredients used pre-harvest; 180.640 Pyridalyl; tolerances for residues. exemptions from the requirement of a 180.641 Spirotetramat; tolerances for resi- tolerance. dues. 180.930 Inert ingredients applied to animals; 180.642 Gentamicin; tolerances for residues. exemptions from the requirement of a 180.643 Uniconazole; tolerances for residues. tolerance. 180.644 Cyprosulfamide; tolerances for resi- 180.940 Tolerance exemptions for active and dues. inert ingredients for use in antimicrobial 180.645 Thiencarbazone-methyl; tolerances formulations (Food-contact surface sani- for residues. tizing solutions). 180.646 Ipconazole; tolerances for residues. 180.950 Tolerance exemptions for minimal 180.647 d-Phenothrin; tolerances for resi- risk active and inert ingredients. dues. 180.960 Polymers; exemptions from the re- 180.648 Meptyldinocap; tolerances for resi- quirement of a tolerance. dues. 180.1011 Viable spores of the microorganism 180.649 Saflufenacil; tolerances for residues. Bacillus thuringiensis Berliner; exemption 180.650 Isoxaben; tolerances for residues. from the requirement of a tolerance. 180.651 Imazosulfuron; tolerances for resi- 180.1016 Ethylene; exemption from the re- dues. quirement of a tolerance. 180.652 Ethiprole; tolerances for residues. 180.1017 Diatomaceous earth; exemption 180.653 Indaziflam; tolerances for residues. from the requirement of a tolerance. 180.654 Isopyrazam; tolerances for residues. 180.1019 Sulfuric acid; exemption from the 180.655 Flazasulfuron; tolerances for resi- requirement of a tolerance. dues. 180.1020 Sodium chlorate; exemption from 180.656 Amisulbrom; tolerances for residues. the requirement of a tolerance. 180.657 Metaflumizone; tolerances for resi- 180.1021 Copper; exemption from the re- dues. quirement of a tolerance. 180.658 Penthiopyrad; tolerances for resi- 180.1022 Iodine-detergent complex; exemp- dues. tion from the requirement of a tolerance.

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180.1023 Propanoic acid; exemptions from 180.1080 Plant volatiles and pheromone; ex- the requirement of a tolerance. emptions from the requirement of a tol- 180.1025 Xylene; exemption from the re- erance. quirement of a tolerance. 180.1083 Dimethyl sulfoxide; exemption 180.1027 Nuclear polyhedrosis virus of from the requirement of a tolerance. Heliothis zea; exemption from the re- 180.1084 Monocarbamide dihydrogen sulfate; quirement of a tolerance. exemption from the requirement of a tol- 180.1033 Methoprene; exemption from the re- erance. quirement of a tolerance. 180.1086 3,7,11-Trimethyl-1,6,10-dodecatriene- 180.1037 Polybutenes; exemption from the 1-ol and 3,7,11-trimethyl-2,6,10- requirement of a tolerance. dodecatriene-3-ol; exemption from the re- 180.1040 Ethylene glycol; exemption from quirement of a tolerance. the requirement of a tolerance. 180.1087 Sesame stalks; exemption from the 180.1041 Nosema locustae; exemption from requirement of a tolerance. the requirement of a tolerance. 180.1089 Poly-N-acetyl-D-glucosamine; ex- 180.1043 Gossyplure; exemption from the re- emption from the requirement of a toler- quirement of a tolerance. ance. 180.1049 Carbon dioxide; exemption from the 180.1090 Lactic acid; exemption from the re- requirement of a tolerance. quirement of a tolerance. 180.1050 Nitrogen; exemption from the re- 180.1091 Aluminum isopropoxide and alu- quirements of a tolerance. minum secondary butoxide; exemption 180.1052 2,2,5-trimethyl-3-dichloroacetyl-1,3- from the requirement of a tolerance. 180.1092 Menthol; exemption from the re- oxazolidine; exemption from the require- quirement of a tolerance. ment of a tolerance. 180.1095 Chlorine gas; exemptions from the 180.1054 Calcium hypochlorite; exemptions requirement of a tolerance. from the requirement of a tolerance. 180.1097 GBM-ROPE; exemption from the re- 180.1056 Boiled linseed oil; exemption from quirement of a tolerance. requirement of tolerance. 180.1098 Gibberellins [Gibberellic Acids (GA3 180.1057 Phytophthora palmivora; exemp- and GA4 + GA7), and Sodium or Potas- tion from requirement of tolerance. sium Gibberellate]; exemption from the 180.1058 Sodium diacetate; exemption from requirement of a tolerance. the requirement of a tolerance. 180.1100 Gliocladium virens isolate GL-21; ex- 180.1064 Tomato pinworm insect pheromone; emption from the requirement of a toler- exemption from the requirement of a tol- ance. erance. 180.1101 Parasitic (parasitoid) and predatory 180.1065 2-Amino-4,5-dihydro-6-methyl-4- insects; exemption from the requirement propyl-s-triazolo(1,5-alpha)pyrimidin-5- of a tolerance. one; exemption from the requirement of 180.1102 Trichoderma harzianum KRL-AG2 a tolerance. (ATCC #20847) strain T–22; exemption 180.1067 Methyl eugenol and malathion com- from requirement of a tolerance. bination; exemption from the require- 180.1103 Isomate-C; exemption from the re- ment of a tolerance. quirement of a tolerance. 180.1068 C12-C18 fatty acid potassium salts; 180.1107 Delta endotoxin of Bacillus exemption from the requirement of a tol- thuringiensis variety kurstaki encap- erance. sulated into killed Pseudomonas 180.1069 (Z)-11-Hexadecenal; exemption from fluorescens; exemption from the require- the requirement of a tolerance. ment of a tolerance. 180.1070 Sodium chlorite; exemption from 180.1108 Delta endotoxin of Bacillus the requirement of a tolerance. thuringiensis variety San Diego encap- 180.1071 Peanuts, Tree Nuts, Milk, Soy- sulated into killed Pseudomonas beans, Eggs, Fish, Crustacea, and Wheat; fluorescens; exemption from the require- exemption from the requirement of a tol- ment of a tolerance. erance. 180.1110 3-Carbamyl-2,4,5-trichlorobenzoic 180.1072 Poly-D-glucosamine (chitosan); ex- acid; exemption from the requirement of emption from the requirement of a toler- a tolerance. ance. 180.1111 Bacillus subtilis GB03; exemption 180.1073 Isomate-M; exemption from the re- from the requirement of a tolerance. quirement of a tolerance. 180.1113 Lagenidium giganteum; exemption 180.1074 F.D.&C. Blue No. 1; exemption from from the requirement of a tolerance. the requirement of a tolerance. 180.1114 Pseudomonas fluorescens A506, 180.1075 Colletotrichum gloeosporioides f. sp. Pseudomonas fluorescens 1629RS, and aeschynomene; exemption from the re- Pseudomonas syringae 742RS; exemptions quirement of a tolerance. from the requirement of a tolerance. 180.1076 Viable spores of the microorganism 180.1118 Spodoptera exigua nuclear poly- Bacillus popilliae; exemption from the re- hedrosis virus; exemption from the requirement of a tolerance. quirement of a tolerance.

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180.1119 Azadirachtin; exemption from the Pseudomonas fluorescens, and the expres- requirement of a tolerance. sion plasmid and cloning vector genetic 180.1120 Streptomyces sp. strain K61; exemp- constructs. tion from the requirement of a tolerance. 180.1156 Cinnamaldehyde; exemption from 180.1121 Boric acid and its salts, borax (so- the requirement of a tolerance. dium borate decahydrate), disodium 180.1157 Cytokinins; exemption from the re- octaborate tetrahydrate, boric oxide quirement of a tolerance. (boric anhydride), sodium borate and so- 180.1158 Auxins; exemption from the re- dium metaborate; exemptions from the quirement of a tolerance. requirement of a tolerance. 180.1159 Pelargonic acid; exemption from 180.1122 Inert ingredients of semiochemical the requirement of tolerances. dispensers; exemptions from the require- 180.1160 Jojoba oil; exemption from the re- ment of a tolerance. quirement of a tolerance. 180.1124 Arthropod pheromones; exemption 180.1161 Clarified hydrophobic extract of from the requirement of a tolerance. neem oil; exemption from the require- 180.1126 Codlure, (E,E)-8,10-Dodecadien-1-ol; ment of a tolerance. exemption from the requirement of a tol- 180.1162 Acrylate polymers and copolymers; erance. exemption from the requirement of a tol- 180.1127 Biochemical pesticide plant floral erance. volatile attractant compounds: cinna- 180.1163 Killed Myrothecium verrucaria; ex- maldehyde, cinnamyl alcohol, 4-methoxy emption from the requirement of a toler- cinnamaldehyde, 3-phenyl propanol, 4- ance. methoxy phenethyl alcohol, indole, and 180.1165 Capsaicin; exemption from the re- 1,2,4-trimethoxybenzene; exemptions quirement of a tolerance. from the requirement of a tolerance. 180.1167 Allyl isothiocyanate as a compo- 180.1128 Bacillus subtilis MBI 600; exemption nent of food grade oil of mustard; exemp- from the requirement of a tolerance. tion from the requirement of a tolerance. 180.1130 N-(n-octyl)-2-pyrrolidone and N-(n- 180.1176 Sodium bicarbonate; exemption dodecyl)-2-pyrrolidone; exemptions from from the requirement of a tolerance. the requirement of a tolerance. 180.1177 Potassium bicarbonate; exemption 180.1131 Ampelomyces quisqualis isolate M10; from the requirement of a tolerance. exemption from the requirement of a tol- 180.1178 Formic acid; exemption from the erance. requirement of a tolerance. 180.1135 Pasteuria penetrans; exemption from 180.1179 Plant extract derived from Opuntia the requirement of a tolerance. lindheimeri, Quercus falcata, Rhus 180.1139 Sodium 5-nitroguaiacolate; exemp- aromatica, and Rhizophoria mangle; ex- tion from the requirement of a tolerance. emption from the requirement of a toler- 180.1140 Sodium o-nitrophenolate; exemp- ance. tion from the requirement of a tolerance. 180.1180 Kaolin; exemption from the require- 180.1141 Sodium p-nitrophenolate; exemp- ment of a tolerance. tion from the requirement of a tolerance. 180.1181 Bacillus cereus strain BPO1; exemp- 180.1142 1,4-Dimethylnaphthalene; exemption from the requirement of a tolerance. tion from the requirement of a tolerance. 180.1187 L-glutamic acid; exemption from 180.1143 Methyl anthranilate; exemption the requirement of a tolerance. from the requirement of a tolerance. 180.1188 Gamma aminobutyric acid; exemp- 180.1144 Candida oleophila isolate I-182; ex- tion from the requirement of a tolerance. emption from the requirement of a toler- 180.1189 Methyl salicylate; exemption from ance. the requirement of a tolerance. 180.1145 Pseudomonas syringae; exemption 180.1191 Ferric phosphate; exemption from from the requirement of a tolerance. the requirement of a tolerance. 180.1146 Beauveria bassiana Strain GHA; ex- 180.1193 Potassium dihydrogen phosphate; emption from the requirement of a toler- exemption from the requirement of a tol- ance. erance. 180.1148 Occlusion Bodies of the Granulosis 180.1195 Titanium dioxide. Virus of Cydia pomenella; tolerance ex- 180.1196 Peroxyacetic acid; exemption from emption. the requirement of a tolerance. 180.1149 Inclusion bodies of the multi-nu- 180.1197 Hydrogen peroxide; exemption from clear polyhedrosis virus of Anagrapha the requirement of a tolerance. falcifera; exemption from the require- 180.1198 Gliocladium catenulatum strain ment of a tolerance. J1446; exemption from the requirement of 180.1150 6-Benzyladenine; exemption from a tolerance. the requirement of a tolerance. 180.1199 Lysophosphatidylethanolamine 180.1153 Lepidopteran pheromones; exemp- (LPE); exemption from the requirement tion from the requirement of a tolerance. of a tolerance. 180.1154 CryIA(c) and CryIC derived delta- 180.1200 Pseudomonas fluorescens strain endotoxins of Bacillus thuringiensis var. PRA–25; temporary exemption from the kurstaki encapsulated in killed requirement of a tolerance.

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180.1201 Trichoderma harzianum strain T-39; 180.1241 Eucalyptus oil; exemption from the exemption from the requirement of a tol- requirement of a tolerance. erance. 180.1243 Bacillus subtilis var. amylolique- 180.1202 Bacillus sphaericus; exemption from faciens strain FZB24; exemption from the the requirement of a tolerance. requirement of a tolerance. 180.1204 Harpin protein; exemption from the 180.1244 Ammonium bicarbonate; exemption requirement of a tolerance. from the requirement of a tolerance. 180.1205 Beauveria bassiana ATCC #74040; ex- 180.1245 Rhamnolipid biosurfactant; exemp- emption from the requirements of a tol- tion from the requirement of a tolerance. erance. 180.1246 Yeast Extract Hydrolysate from 180.1206 Aspergillus flavus AF36; exemption Saccharomyces cerevisiae: exemption from from the requirement of a tolerance. the requirement of a tolerance. 180.1207 N-acyl sarcosines and sodium N- 180.1248 Exemption of citronellol from the acyl sarcosinates; exemption from the re- requirement of a tolerance. quirement of a tolerance. 180.1250 C8, C10, and C12 fatty acid mono- 180.1209 Bacillus subtilis strain QST 713 and esters of glycerol and propylene glycol; strain QST 713 variant soil; exemption exemption from the requirement of a tol- from the requirement of a tolerance. erance. 180.1210 Phosphorous acid; exemption from 180.1251 Geraniol; exemption from the re- the requirement of a tolerance. quirement of a tolerance. 180.1212 Pseudomonas chlororaphis Strain 63– 180.1253 Streptomyces lydicus WYEC 108; ex- 28; exemption from the requirement of a emption from the requirement of a toler- tolerance. ance. 180.1213 Coniothyrium minitans strain CON/ 180.1254 Aspergillus flavus NRRL 21882; ex- M/91–08; exemption from the requirement emption from the requirement of a toler- of a tolerance. ance. 180.1218 Indian Meal Moth Granulosis Virus; 180.1255 Bacillus pumilus strain QST 2808; ex- exemption from the requirement of a tol- emption from the requirement of a toler- erance. ance. 180.1219 Foramsulfuron; exemption from the 180.1256 Alternaria destruens strain 059; ex- requirement of a tolerance. emption from the requirement of a toler- 180.1220 1-Methylcyclopropene; exemption ance. from the requirement of a tolerance. 180.1257 Paecilomyces lilacinus strain 251; ex- 180.1221 Pseudozyma flocculosa strain PF-A22 emption from the requirement of a toler- UL; exemption from the requirement of a ance. tolerance. 180.1258 Acetic acid; exemption from the re- 180.1222 Sucrose octanoate esters; exemp- quirement of a tolerance. tion from the requirement of a tolerance. 180.1259 Reynoutria sachalinensis extract; ex- 180.1223 Imazamox; exemption from the re- emption from the requirement of a toler- quirement of a tolerance. ance. 180.1224 Bacillus pumilus GB34; exemption 180.1260 Muscodor albus QST 20799 and the from the requirement of a tolerance. volatiles produced on rehydration; ex- 180.1225 Decanoic acid; exemption from the emption from the requirement of a toler- requirement of a tolerance. ance. 180.1226 Bacillus pumilus strain QST2808; 180.1261 Xanthomonas campestris pv. temporary exemption from the require- vesicatoria and Pseudomonas syringae pv. ment of a tolerance. tomato specific Bacteriophages. 180.1228 Diallyl sulfides; exemption from the 180.1262 Sorbitol octanoate; exemption from requirement of a tolerance. the requirement of a tolerance. 180.1230 Ferrous sulfate; exemption from 180.1263 Tetrahydrofurfuryl alcohol; exemp- the requirement of a tolerance. tion from the requirement of a tolerance. 180.1231 Lime; exemption from the require- 180.1267 Pantoea agglomerans strain C9–1; ex- ment of a tolerance. emption from the requirement of a toler- 180.1232 Lime-sulfur; exemption from the re- ance. quirement of a tolerance. 180.1268 Potassium silicate; exemption from 180.1233 Potassium sorbate; exemption from the requirement of a tolerance. the requirement of a tolerance. 180.1269 Bacillus mycoides isolate J; exemp- 180.1234 Sodium carbonate; exemption from tion from the requirement of a tolerance. the requirement of a tolerance. 180.1270 Isophorone; exemption from the re- 180.1235 Sodium hypochlorite; exemption quirement of a tolerance. from the requirement of a tolerance. 180.1271 Eucalyptus oil; exemption from the 180.1236 Sulfur; exemption from the require- requirement of a tolerance. ment of a tolerance. 180.1272 Pantoea agglomerans strain E325; ex- 180.1237 Sodium metasilicate; exemption emption from the requirement of a toler- from the requirement of a tolerance. ance. 180.1240 Thymol; exemption from the re- 180.1273 Beauveria bassiana HF23; exemp- quirement of a tolerance. tion from the requirement of a tolerance.

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180.1274 Tris (2-ethylhexyl) phosphate; ex- 180.1298 Trichoderma hamatum isolate 382; emption from the requirement of a toler- exemption from the requirement of a tol- ance. erance. 180.1275 Pythium; exception from the re- 180.1299 Prohydrojasmon; exemption from quirement of a tolerance. the requirement of a tolerance. 180.1276 Tobacco mild green mosaic 180.1300 Potassium hypochlorite; exemption tobamovirus (TMGMV); temporary ex- from the requirement of a tolerance. emption from the requirement of a toler- 180.1301 Escherichia coli O157:H7 specific ance. bacteriophages; temporary exemption 180.1277 Dibasic esters; exemption from the from the requirement of a tolerance. requirement of a tolerance. 180.1302 Sodium Ferric Ethylenediamine- 180.1278 Quillaja saponaria extract tetraacetate (EDTA); exemption from (saponins); exemption from the require- the requirement of a tolerance. ment of a tolerance. 180.1303 Metarhizium anisopliae strain F52; 180.1279 Zucchini yellow mosaic virus— exemption from the requirement of a tol- weak strain; exemption from the require- erance. ment of a tolerance. 180.1304 Pseudomonas fluorescens strain 180.1280 Poly(hexamethylenebiguanide) hy- CL145A; exemption from the requirement drochloride (PHMB); exemption from the of a tolerance. requirement of a tolerance. 180.1305 Chromobacterium subtsugae strain 180.1281 S-Abscisic Acid, (S)-5-(1-hydroxy- PRAA4–1T; exemption from the require- 2,6,6-trimethyl-4-oxo-1-cyclohex-2-enyl)- ment of a tolerance. 3-methyl-penta-(2Z,4E)-dienoic Acid; ex- 180.1306 Isaria fumosorosea (formerly emption from the requirement of a toler- Paecilomyces fumosoroseus) Apopka ance. strain 97; exemption from the require- 180.1282 Bacillus firmus I-1582; exemption ment of a tolerance. from the requirement of a tolerance. 180.1307 Bacteriophage of Clavibacter 180.1283 (Z)-7,8-epoxy-2-methyloctadecane michiganensis subspecies michiganensis; (Disparlure); exemption from the re- exemption from the requirement of a tol- quirement of a tolerance. erance. 180.1284 Ammonium salts of higher fatty 180.1308 Bacillus amyloliquefaciens strain acids (C8-C18 saturated; C8-C12 unsatu- D747; exemption from the requirement of rated); exemption from the requirement a tolerance. of a tolerance. 180.1309 Bacillus subtilis strain CX–9060; ex- 180.1285 Polyoxin D zinc salt; exemption emption from the requirement of a toler- from the requirement of a tolerance. ance. 180.1287 Extract of Chenopodium ambrosioides 180.1310 Trichoderma virens strain G–41; ex- near ambrosioides; exemption from the re- emption from the requirement of a toler- quirement of a tolerance. ance. 180.1288 Tristyrylphenol ethoxylates; ex- 180.1311 Pasteuria nishizawae—Pn1; exemp- emption from the requirement of a toler- tion from the requirement of a tolerance. ance. 180.1312 Aureobasidium pullulans strains 180.1289 Candida oleophila Strain O; exemp- DSM 14940 and DSM 14941; exemption tion from the requirement of a tolerance. from the requirement of a tolerance. 180.1290 Pasteuria usgae; exemption from the 180.1313 Bacillus pumilus strain GHA 180; ex- requirement of a tolerance. emption from the requirement of a toler- 180.1291 Cold pressed neem oil; exemption ance. from the requirement of a tolerance. 180.1314 Killed, nonviable Streptomyces 180.1292 Ulocladium oudemansii (U3 Strain); acidiscabies strain RL–110T; exemption exemption from the requirement of a tol- from the requirement of a tolerance. erance. 180.1315 Natamycin; exemption from the re- 180.1293 Trichoderma gamsii strain ICC 080; quirement of a tolerance. exemption from the requirement of a tol- 180.1316 Pasteuria spp. (Rotylenchulus erance. reniformis nematode)—Pr3; exemption 180.1294 Trichoderma asperellum strain ICC from the requirement of a tolerance. 012; exemption from the requirement of a 180.1317 Pesticide chemicals; exemption tolerance. from the requirements of a tolerance. 180.1295 Laminarin; exemption from the re- 180.1318 3-decen-2-one; exemption from the quirement of a tolerance. requirement of a tolerance. 180.1296 Terpene Constituents a-terpinene, 180.1319 Banda de Lupinus albus doce d-limonene and p-cymene, of the Extract (BLAD); exemption from the requirement of Chenopodium ambrosioides near of a tolerance. ambrosioides as Synthetically Manufac- 180.1320 Methyl jasmonate; exemption from tured; exemption from the requirement the requirement of a tolerance. of a tolerance. 180.1321 Complex Polymeric Polyhydroxy 180.1297 Homobrassinolide; exemption from Acids; exemption from the requirement the requirement of a tolerance. of a tolerance.

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180.1322 Bacillus pumilus strain BU F–33; ex- Subpart A—Definitions and emption from the requirement of a tolerance. Interpretative Regulations 180.1323 Ethyl-2E,4Z-decadienoate (Pear Ester); exemption from the requirement § 180.1 Definitions and interpretations. of a tolerance. (a) Administrator, without qualifica- 180.1324 GS-omega/kappa-Hxtx-Hv1a; ex- tion, means the Administrator of the emption from the requirement of a toler- Environmental Protection Agency. ance. (b) Agency, without qualification, 180.1325 Heat-killed Burkholderia spp. strain means the Environmental Protection A396 cells and spent fermentation media Agency. exemption from the requirement of a tol- (c) FFDCA means the Federal Food, erance. Drug, and Cosmetic Act, as amended, Subpart E—Pesticide Chemicals Not Re- 21 U.S.C. 301–392. quiring a Tolerance or an Exemption (d) Raw agricultural commodities in- from a Tolerance clude, among other things, fresh fruits, whether or not they have been washed 180.2000 Scope. and colored or otherwise treated in 180.2003 Definitions. their unpeeled natural form; vegetables 180.2010 Threshold of regulation determina- in their raw or natural state, whether tions. or not they have been stripped of their 180.2020 Non-food determinations. outer leaves, waxed, prepared into AUTHORITY: 21 U.S.C. 321(q), 346a and 371. fresh green salads, etc.; grains, nuts, eggs, raw milk, meats, and similar ag- SOURCE: 36 FR 22540, Nov. 25, 1971, unless ricultural produce. It does not include otherwise noted. foods that have been processed, fab- EDITORIAL NOTE: Nomenclature changes to ricated, or manufactured by cooking, part 180 appear at 62 FR 66023, Dec. 17, 1997. freezing, dehydrating, or milling. (e) Where a raw agricultural com- GLOSSARY modity bearing a pesticide chemical NOTE: The items in this glossary were com- residue that has been exempted from piled as an aid to the users of the Code of the requirement of a tolerance, or Federal Regulations. Inclusion or exclusion which is within a tolerance permitted from this glossary has no legal significance. under FFDCA section 408, is used in APPLI = APPLICATION C-I MET = CHOLINESTERASE-INHIBITING preparing a processed food, the proc- METABOLITES essed food will not be considered unsafe CARB = CARBAMATES within the meaning of FFDCA sections EPWRR = EDIBLE PORTION WITH RIND 402 and 408(a), despite the lack of a tol- REMOVED erance or exemption for the pesticide EXC = EXCEPT chemical residue in the processed food, I (IN PPM COLUMN) = INTERIM TOLER- if: ANCE (1) The pesticide chemical has been INC = INCLUDING used in or on the raw agricultural com- K=CWHR = KERNEL PLUS COB WITH modity in conformity with a tolerance HUSK REMOVED under this section; MBYP = MEAT BYPRODUCTS (2) The pesticide chemical residue MIN = MINIMUM has been removed to the extent pos- N (IN PPM COLUMN) = NEGLIGIBLE RESI- DUES sible in good manufacturing practice; NMT = NOT MORE THAN and NON-PER BAG/PKGD RAC = NON-PERISH- (3) The concentration of the pesticide ABLE PACKAGED OR BAGGED RAW AG- chemical residue in the processed food RICULTURAL COMMODITY is not greater than the tolerance pre- PPM = PART(S) PER MILLION scribed for the pesticide chemical res- POST-H = POSTHARVEST APPLICATION idue on the raw agricultural com- PRE-H = PREHARVEST APPLICATION modity. PRE-S = PRESLAUGHTER APPLICATION (f) For the purpose of computing fees PRODS = PRODUCTS rollert as required by § 180.33, each group of re- T (IN PPM COLUMN) = TEMPORARY TOL- lated crops listed in § 180.34(e) and each ERANCE crop group or subgroup listed in § 180.41 [41 FR 4537, Jan. 30, 1976] is counted as a single raw agricultural

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commodity in a petition or request for apply to the corresponding specific raw tolerances or exemption from the re- agricultural commodities listed in col- quirement of a tolerance. umn B. However, a tolerance or exemp- (g) Tolerances and exemptions estab- tion for a specific commodity in col- lished for pesticide chemicals in or on umn B does not apply to the general the general category of raw agricul- category in column A. tural commodities listed in column A

A B

Alfalfa Medicago sativa L. Subsp. sativa, (alfalfa, lucerne); Onobrychis viciifolia Scop. (sainfoin, holy clover, esparcet); and Lotus corniculatus L. (trefoil); and varieties and/or hybrids of these.

Banana Banana, plantain.

Bean Cicer arietinum (chickpea, garbanzo bean); Lupinus spp. (including sweet lupine, white sweet lupine, white lupine, and grain lupine). Phaseolus spp. (including kidney bean, lima bean, mung bean, navy bean, pinto bean, snap bean, and waxbean; Vicia faba (broad bean, fava bean); Vigna spp. (including asparagus bean, blackeyed pea and cowpea).

Bean, dry All beans above in dry form only.

Bean, succulent All beans above in succulent form only.

Blackberry Rubus eubatus (including bingleberry, black satin berry, boysenberry Cherokee blackberry, Chesterberry, Cheyenne blackberry, coryberry, darrowberry, dewberry, Dirksen thornless berry, Himalayaberry, hullberry, Lavacaberry, lowberry, Lucretiaberry, mammoth blackberry, marionberry, nectarberry, olallieberry, Oregon evergreen berry, phenomenalberry, rangerberry, ravenberry, rossberry, Shawnee blackberry, and varieties and/or hybrids of these).

Broccoli Broccoli, chinese broccoli (gia lon, white flowering broccoli).

Cabbage Cabbage, Chinese cabbage (tight-heading varieties only).

Caneberry Rubus spp. (including blackberry); Rubus caesius (youngberry); Rubus loganbaccus (loganberry); Rubus idaeus (red and black raspberry); cultivars, varieties, and/or hybrids of these.

Celery Celery, Florence fennel (sweet anise, sweet fennel, finochio) (fresh leaves and stalks only).

Cherry Cherry, sweet, and cherry, tart.

Endive Endive, escarole.

Fruit, citrus Grapefruit, lemon, lime, orange, tangelo, tangerine, citrus citron, kumquat, and hybrids of these.

Garlic Garlic, great headed; garlic, and serpent garlic.

Lettuce Lettuce, head; and lettuce, leaf

Lettuce, head Lettuce, head; crisphead varieties only

Lettuce, leaf Lettuce, leaf; cos (romaine), butterhead varieties

Marjoram Origanum spp. (includes sweet or annual marjoram, wild marjoram or oregano, and pot marjoram).

Melon Muskmelon, including hybrids and/or varieties of Cucumis melo (including true cantaloupe, cantaloupe, casaba, Santa Claus melon, crenshaw melon, honeydew melon, honey balls, Persian melon, golden pershaw melon, mango melon, pineapple melon, snake melon); and watermelon, including hybrids and/or varieties of (Citrullus spp.).

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A B

Muskmelon Cucumis melo (includes true cantaloupe, cantaloupe, casaba, Santa Claus melon, crenshaw melon, honeydew melon, honey balls, Per- sian melon, golden pershaw melon, mango melon, pineapple melon, snake melon, and other varieties and/or hybrids of these.)

Onion Bulb onion; green onion; and garlic.

Onion, bulb Bulb onion; garlic; great headed garlic; serpent garlic; Chinese onion; pearl onion; potato onion; and shallot, bulb.

Onion, green Green onion; lady’s leek; leek; wild leek; Beltsville bunching onion; fresh onion; tree onion, tops; Welsh onion; and shallot, fresh leaves.

Peach Peach, nectarine

Pea Cajanus cajan (includes pigeon pea); Cicer spp. (includes chickpea and garbanzo bean); Lens culinaris (lentil); Pisum spp. (includes dwarf pea, garden pea, green pea, English pea, field pea, and edible pod pea). [Note: A variety of pesticide tolerances have been previously established for pea and/or bean. Chickpea/garbanzo bean is now classified in both the bean and the pea categories. For garbanzo bean/chickpea only, the highest established pea or bean tolerance will apply to pesticide residues found in this commodity.]

Pea, dry All peas in dry form only.

Pea, succulent All peas in succulent form only.

Pepper All varieties of pepper including pimento and bell, hot, and sweet pepper.

Radish, oriental, roots Raphanus sativus var. longipinnatus (roots and tops), including Chi- nese or Japanese radish (both white and red), winter radish, daikon, lobok, lo pak, and other cultivars and/or hybrids of these.

Radish, oriental, tops) Raphanus sativus var. longipinnatus (roots and tops), including Chi- nese or Japanese radish (both white and red), winter radish, daikon, lobok, lo pak, and other cultivars and/or hybrids of these.

Rapeseed Brassica napus, B. campestris, and Crambe abyssinica (oilseed-producing varieties only which include canola and crambe.)

Raspberry Rubus spp. (including bababerry; black raspberry; blackcap; caneberry; framboise; frambueso; himbeere; keriberry; mayberry; red raspberry; thimbleberry; tulameen; yellow raspberry; and cultivars, varieties, and/or hybrids of these).

Sorghum, grain, grain Sorghum spp. [sorghum, grain, sudangrass (seed crop), and hybrids of these grown for its seed].

Sorghum, forage, stover Sorghum spp. [sorghum, forage; sorghum, stover; sudangrass, and hybrids of these grown for forage and/or stover.

Squash Pumpkin, summer squash, and winter squash.

Sugar apple Annona squamosa L. (sugar apple, sweetsop, anon), and its hybrid A. squamosa L. x A. cherimoya M. (atemoya). Also A. reticulata L. (true custard apple).

Squash, summer Fruits of the gourd (Cucurbitaceae) family that are consumed when immature, 100% of the fruit is edible either cooked or raw, once picked it cannot be stored, has a soft rind which is easily penetrated, and if seeds were harvested they would not germinate; e.g., Cucurbita pepo (i.e., crookneck squash, straightneck squash, scallop squash, and vegetable marrow); Lagenaria spp. (i.e., spaghetti squash, hyotan, cucuzza); Luffa spp. (i.e., hechima, Chinese okra); Momordica spp. (i.e., bitter melon, balsam pear, balsam apple, Chi- nese cucumber); Sechium edule (chayote); and other cultivars and/or hybrids of these.

Sweet potato Sweet potato, yam.

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A B

Tangerine Tangerine (mandarin or mandarin orange); clementine; Mediterranean mandarin; satsuma mandarin; tangelo; tangor; cultivars, varieties, and/or hybrids of these.

Tomato Tomato, tomatillo.

Turnip tops or turnip greens Broccoli raab (raab, raab salad), hanover salad, turnip tops (turnip greens).

Wheat Wheat, triticale.

(h) Unless otherwise specified in this (10) For processed foods consisting paragraph or in tolerance regulations primarily of one ingredient and sold in prescribed in this part for specific pes- a form requiring further preparation ticide chemicals, the raw agricultural prior to consumption (e.g., fruit juice commodity or processed food to be ex- concentrates, dehydrated vegetables, amined for pesticide residues, shall and powdered potatoes), the processed consist of the whole raw agricultural food to be examined for residues shall commodity or processed food. be the whole processed commodity (1) The raw agricultural commodity after compensating for or reconsti- bananas, when examined for pesticide tuting to the commodity’s normal residues, shall not include any crown moisture content, unless a tolerance tissue or stalk. for the concentrated or dehydrated (2) Shell shall be removed and dis- food form is included in this part. If carded from nuts before examination there exists a tolerance for a specific for pesticide residues. pesticide on the processed food in its (3) Caps (hulls) shall be removed and concentrated or dehydrated food form, discarded from strawberries before ex- for the purpose of determining whether amination for pesticide residues. the food is in compliance with that tol- (4) Stems shall be removed and dis- erance, the processed food to be exam- carded from melons before examination ined for residues shall be the whole for pesticide residues. processed commodity on an ‘‘as is’’ (5) Roots, stems, and outer sheaths basis. (or husks) shall be removed and dis- (i) The term pesticide chemical shall carded from garlic bulbs and dry bulb have the meaning specified in FFDCA onions, and only the garlic cloves and section 201(q)(1), as amended, except as onion bulbs shall be examined for pes- provided in § 180.4. ticide residues. (j) The term negligible residue means (6) Where a tolerance is established any amount of a pesticide chemical re- on a root vegetable including tops and/ maining in or on a raw agricultural or with tops, and the tops and the roots commodity or group of raw agricul- are marketed together, they shall be tural commodities that would result in analyzed separately and neither the a daily intake regarded as pesticide residue on the roots nor the toxicologically insignificant on the pesticide residue on the tops shall ex- basis of scientific judgment of ade- ceed the tolerance level, except that in quate safety data. Ordinarily this will the case of carrots, parsnips, and ruta- add to the diet an amount which will bagas, the tops shall be removed and be less than 1/2,000th of the amount discarded before analyzing roots for that has been demonstrated to have no pesticide residues. effect from feeding studies on the most (7) The crowns (leaves at the top of sensitive animal species tested. Such the fruit) shall be removed and dis- toxicity studies shall usually include carded from pineapples before examina- at least 90-day feeding studies in two tion for pesticide residues. species of mammals. (8) The term lima beans means the (k) The term nonperishable raw agri- beans and the pod. cultural commodity means any raw agri- (9) The term peanuts means the pea- cultural commodity not subject to nut meat after removal of the hulls. rapid decay or deterioration that would

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render it unfit for consumption. Exam- cological effects: Chlorinated organic ples are cocoa beans, coffee beans, pesticides, arsenic-containing chemi- field-dried beans, field-dried peas, cals, metallic dithiocarbamates, cho- grains, and nuts. Not included are eggs, linesterase-inhibiting pesticides.) milk, meat, poultry, fresh fruits, and (b) Tolerances established for such vegetables such as onions, parsnips, po- related pesticide chemicals may limit tatoes, and carrots. the amount of a common component (l) The term tolerance with regional (such as As2O3) that may be present, or registration means any tolerance which may limit the amount of biological ac- is established for pesticide residues re- tivity (such as cholinesterase inhibi- sulting from the use of the pesticide tion) that may be present, or may limit pursuant to a regional registration. the total amount of related pesticide Such a tolerance is supported by res- chemicals (such as chlorinated organic idue data from specific growing regions pesticides) that may be present. for a raw agricultural commodity. Indi- (c)(1) Where tolerances for inorganic vidual tolerances with regional reg- bromide in or on the same raw agricul- istration are designated in separate tural commodity are set in two or subsections in 40 CFR 180.101 through more sections in this part (example: 180.999, as appropriate. Additional res- §§ 180.123 and 180.199), the overall quan- idue data which are representative of tity of inorganic bromide to be toler- the proposed use area are required to ated from use of the same pesticide in expand the geographical area of usage different modes of application or from of a pesticide on a raw agricultural two or more pesticide chemicals for commodity having an established ‘‘tol- which tolerances are established is the erance with regional registration.’’ highest of the separate applicable tol- Persons seeking geographically broad- erances. For example, where the bro- er registration of a crop having a ‘‘tol- mide tolerance on asparagus from erance with regional registration’’ methyl bromide commodity fumigation should contact the appropriate EPA is 100 parts per million (40 CFR 180.123) product manager concerning additional and on asparagus from methyl bromide residue data required to expand the use soil treatment is 300 parts per million area. (40 CFR 180.199), the overall inorganic (m) The term pesticide chemical res- bromide tolerance for asparagus grown idue shall have the meaning specified on methyl bromide-treated soil and in FFDCA section 201(q)(2), as amend- also fumigated with methyl bromide ed, except as provided in § 180.4. after harvest is 300 parts per million. (n) The term food commodity means: (2) Where tolerances are established (1) Any raw agricultural commodity in terms of inorganic bromide residues (food or feed) as defined in section only from use of organic bromide fumi- 201(r) of the Federal Food, Drug, and gants on raw agricutural commodities, Cosmetic Act (FFDCA); and such tolerances are sufficient to pro- (2) Any processed food or feed as detect the public health, and no addi- fined in section 201(gg) of the FFDCA. tional concurrent tolerances for the or- [36 FR 22540, Nov. 25, 1971] ganic pesticide chemicals from such use are necessary. This conclusion is EDITORIAL NOTE: For FEDERAL REGISTER citations affecting § 180.1, see the List of CFR based on evidence of the dissipation of Sections Affected, which appears in the the organic pesticide or its conversion Finding Aids section of the printed volume to inorganic bromide residues in the and at www.fdsys.gov. food when ready to eat. (d)(1) Where tolerances are estab- § 180.3 Tolerances for related pesticide lished for both calcium cyanide and hy- chemicals. drogen cyanide on the same raw agri- (a) Pesticide chemicals that cause re- cultural commodity, the total amount lated pharmacological effects will be of such pesticides shall not yield more regarded, in the absence of evidence to residue than that permitted by the the contrary, as having an additive del- larger of the two tolerances, calculated eterious action. (For example, many as hydrogen cyanide. pesticide chemicals within each of the (2) Where tolerances are established following groups have related pharma- for residues of both O,O-diethyl S-[2-

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(ethylthio)ethyl] phosphorodithioate more residue than that permitted by and demeton (a mixture of O,O-diethyl the higher of the two tolerances. O-(and S-) [2-(ethylthio)ethyl] (8) Where a tolerance is established phosphorothioates) on the same raw for more than one pesticide having the agricultural commodity, the total metabolites 1-(3,4-dichlorophenyl)-3- amount of such pesticides shall not methylurea (DCPMU) and 3,4- yield more residue than that permitted dichlorophenylurea (DCPU) found in or by the larger of the two tolerances, cal- on a raw agricultural commodity, the culated as demeton. total amount of such residues shall not (3) Where tolerances are established exceed the highest established toler- for both terpene polychlorinates ance for a pesticide having these me- (chlorinated mixture of camphene, pi- tabolites. nene, and related terpenes, containing (9) Where a tolerance is established 65–66 percent chlorine) and toxaphene for more than one pesticide having as (chlorinated camphene containing 67–69 metabolites compounds containing the percent chlorine) on the same raw agri- benzimidazole moiety found in or on a cultural commodities, the total raw agricultural commodity, the total amount of such pesticides shall not amount of such residues shall not ex- yield more residue than that permitted ceed the highest established tolerance by the larger of the two tolerances, cal- for a pesticide having these metabo- culated as a chlorinated terpene of mo- lites. lecular weight 396.6 containing 67 per- (10) Where a tolerance is established cent chlorine. for triclopyr, chloropyrifos, and (4) Where a tolerance is established chlorpyrifos-methyl having the com- for more than one pesticide containing mon metabolite 3,5,6-trichloro-2- arsenic found in, or on a raw agricul- pyridinol on the same raw agricultural tural commodity, the total amount of commodity, the total amount of such such pesticide shall not exceed the residues shall not exceed the highest highest established tolerance cal- established tolerance for any of the culated as As2O3. (5) Where tolerances are established pesticides having the metabolites. for more than one member of the class (11) Where tolerances are established of dithiocarbamates listed in para- for more than one pesticide having the graph (e)(3) of this section on the same metabolite 3,5,6-trichloro-2-pyridinol raw agricultural commodity, the total found in or on the raw agricultural residue of such pesticides shall not ex- commodity, the total amount of such ceed that permitted by the highest tol- residues shall not exceed the highest erance established for any one member established tolerance for a pesticide of the class, calculated as zinc having this metabolite. ethylenebisdithiocarbamate. (12) Where tolerances are established (6) Where tolerances are established for residues of methomyl, resulting for residues of both S,S,S-tributyl from the use of thiodicarb and/or phosphorotrithioate and tributyl methomyl on the same raw agricul- phosphorotrithioite in or on the same tural commodity, the total amount of raw agricultural commodity, the total methomyl shall not yield more residue amount of such pesticides shall not than that permitted by the higher of yield more residue than that permitted the two tolerances. by the higher of the two tolerances, (e) Except as noted in paragraphs calculated as S,S,S-tributyl (e)(1) and (2) of this section, where resi- phosphorotrithioate. dues from two or more chemicals in the (7) Where tolerances are established same class are present in or on a raw for residues of O,S-dimethyl agricultural commodity the tolerance phosphoramidothioate, resulting from for the total of such residues shall be the use of acephate (O,S-dimethyl the same as that for the chemical hav- acetylphos-phoramidothioate) and/or ing the lowest numerical tolerance in O,S - dimethylphosphoramidothioate this class, unless a higher tolerance on the same agricultural commodity, level is specifically provided for the the total amount of O,S-dimethyl- combined residues by a regulation in phosphoramidothioate shall not yield this part.

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(1) Where residues from two or more A mixture of 5.2 parts by weight of ammoni- chemicals in the same class are present ates of [ethylenebis (dithiocarbamato)] in or on a raw agricultural commodity zinc with 1 part by weight ethylenebis and there are available methods that [dithiocarbamic acid] bimolecular and trimolecular cyclic anhydrosulfides and permit quantitative determination of disulfides. each residue, the quantity of combined 2-Chloroallyl diethyldithiocarbamate. residues that are within the tolerance Coordination product of zinc ion and maneb may be determined as follows: containing 20 percent manganese, 2.5 per- (i) Determine the quantity of each cent zinc, and 77.5 percent residue present. ethylenebisdithiocarbamate. Ferbam. (ii) Divide the quantity of each res- Maneb. idue by the tolerance that would apply Manganous dimethyldithiocarbamate. if it occurred alone, and multiply by Sodium dimethyldithiocarbamate. 100 to determine the percentage of the Thiram. permitted amount of residue present. Zineb. Ziram. (iii) Add the percentages so obtained for all residues present. (4) The following are members of the (iv) The sum of the percentages shall class of chlorinated organic pesticides: not exceed 100 percent. Aldrin. (2) Where residues from two or more BHC (benzene hexachloride). chemicals in the same class are present 1,1-Bis(p-chlorophenyl)-2,2,2- in or on a raw agricultural commodity trichloroethanol. and there are available methods that Chlorbenside (p-chlorobenzyl p-chlorophenyl permit quantitative determinations of sulfide). Chlordane. one or more, but not all, of the resi- Chlorobenzilate (ethyl 4,4′- dues, the amounts of such residues as dichlorobenzilate). may be determinable shall be deducted p-Chlorophenoxyacetic acid. from the total amount of residues p-Chlorophenyl-2,4,5-trichlorophenyl sulfide. present and the remainder shall have 2,4-D (2,4-dichlorophenoxyacetic acid). the same tolerance as that for the DDD (TDE). DDT. chemical having the lowest numerical 1,1-Dichloro-2,2-bis(p-ethylphenyl) ethane. tolerance in that class. The quantity of 2,6-Dichloro-4-nitroaniline. combined residues that are within the 2,4-Dichlorophenyl p-nitrophenyl ether. tolerance may be determined as fol- Dieldrin. lows: Dodecachlorooctahydro-1,3,4-metheno-2H- (i) Determine the quantity of each cyclobuta[cd]pentalene. Endosulfan (6,7,8,9,10,10-hexachloro-1,5,5a, determinable residue present. 6,9,9a-hexahydro-6,9-methano-2,4,3- (ii) Deduct the amounts of such resi- benzodioxathiepin-3-oxide). dues from the total amount of residues Endosulfan sulfate (6,7,8,9,10,10-hexachloro- present and consider the remainder to 1,5,5a,6,9,9a-hexahydro-6,9-methano-2,4,3- have the same tolerance as that for the benzodioxathiepin-3,3-dioxide). chemical having the lowest numerical Heptachlor (1,4,5,6,7,8,8-heptachlor-3a,4,7, 7a- tolerance in that class. tetrahydro-4,7-methanoindene). Heptachlor epoxide (1,4,5,6,7,8,8-heptachloro- (iii) Divide the quantity of each de- 2,3-epoxy-2,3,3a,4,7,7a-hexahydro-4,7- terminable residue by the tolerance methanoindene). that would apply if it occurred alone Hexachlorophene (2,2′-methylenebis(3,4,6- and the quantity of the remaining res- trichlorophenol) and its monosodium salt. idue by the tolerance for the chemical Isopropyl 4,4′-dichlorobenzilate. having the lowest numerical tolerance Lindane. Methoxychlor. in that class and multiply by 100 to de- Ovex (p-chlorophenyl p- termine the percentage of the per- chlorobenzenesulfonate). mitted amount of residue present. Sesone (sodium 2,4-dichlorophenoxyethyl (iv) Add the percentages so obtained sulfate, SES). for all residues present. Sodium 2,4-dichlorophenoxyacetate. (v) The sum of the percentages shall Sodium trichloroacetate. Sulphenone (p-chlorophenyl phenyl sulfone). not exceed 100 percent. Terpene polychlorinates (chlorinated mix- (3) The following pesticides are mem- ture of camphene, pinene, and related bers of the class of dithiocarbamates: terpenes 65-66 percent chlorine).

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2,3,5,6-Tetrachloronitrobenzene. O,O-Diethyl O-(2-isoprophyl-4-methyl-6- Tetradifon (2,4,5,4′-tetrachlorodiphenyl pyrimidinyl) phosphorothioate. sulfone). O,O-Diethyl O-[p-(methylsulfinyl)phenyl] Toxaphene (chlorinated camphene). phosphorothioate and its cholinesterase-in- Trichlorobenzoic acid. hibiting metabolites. Trichlorobenzyl chloride. Diethyl 2-pyrazinyl phosphate. (5) The following are members of the O,O-Diethyl O-2-pyrazinyl phosphorothioate. class of cholinesterase-inhibiting pes- S-(O,O-Diisopropyl phosphorodithioate) of N- ticides: (2-mercaptoethyl) benzenesulfonamide S-(O,O-Diisopropyl phosphorodithioate) of N- Acephate (O,S-dimethyl acetyl- (2-mercaptoethyl) benzenesulfonamide phosphoramidothioate) and its cholin- 2-(Dimethylamino)-5.6-dimethyl-4- esterase-inhibiting metabolite O,S-di- pyrimidinyl dimethylcarbamate and its methyl phosphoramidothioate. metabolites 5,6-dimethyl-2- Aldicarb (2-methyl-2-(methylthio) (formylmethylamino)-4-pyrimidinyl propionaldehyde O- dimethylcarbamate and 5,6-dimethyl-2- (methylcarbamoyl)oxime) and its (methylamino)-4-pyrimidinyl chlorinesterase-inhibiting metabolites 2- dimethylcarbamate (both calculated as methyl-2-(methylsulfinyl)propionaldehyde parent). O-(methycarbamoyl) oxime and 2-methyl- Dimethoate (O,O-dimethyl S-(N-methyl- 2-(methylsulfonyl)propionaldehyde O- carbamoylmethyl) phosphorodithioate). (methylcarbamoyl)oxime. Dimethoate oxygen analog (O,O-dimethyl S- 4-tert-Butyl-2-chlorophenyl methyl methyl (N-methylcarbamoylmethyl) phosphoramidate. phosphorothioate). S-[(tert-Butylthio)methyl] O,O-diethyl O,O-Dimethyl O-p-(dimethylsulfamoyl) phosphorodithioate and its cholinesterase- phenyl phosphate. inhibiting metabolites. O,O-Dimethyl O-p-(dimethylsulfamoyl) Carbaryl (1-naphthyl N-methylcarbamate). phenyl phosphorothioate. Carbofuran (2,3,-dihydro-2,2-dimethyl-7- 3,5-Dimethyl-4-(methylthio) phenyl benzofuranyl-N-methylcarbamate). Carbofuran metabolite (2,3-dihydro-2,2-dimethylcarbamate. methyl-3-hydroxy-7-benofuranyl N- O,O-Dimethyl S-[4-oxo-1,2,3-benzotriazin-3- methylcarbamate). (4H)-ylmethyl] phosphorodithioate. Carbophenothion (S-[(p-chlorophenyl) Dimethyl phosphate of 3-hydroxy-N,N-di- thiolmethyl] O,O-diethyl methyl-cis-crotonamide. phosphorodithioate) and its cholinesterase- Dimethyl phosphate of 3-hydroxy-N-methyl- inhibiting metabolites. cis-crotonamide. Chlorpyrifos (O,O-diethyl O-(3,5,6-trichloro- Dimethyl phosphate of a-methylbenzyl 3-hy- 2-pyridyl)phosphorothioate). droxy-cis-crotonate. Chlorpyrifos-methyl (O,O-dimethyl-O-(3,5,6- O,O-Dimethyl 2,2,2-trichloro-1-hydroxyethyl trichloro-2-pyridyl) phosphorothioate. phosphonate. 2-Chloro-1-(2,4,5-trichlorophenyl)vinyl di- O,O-Dimethyl phosphorodithioate, S-ester methyl phosphate. with 4-(mercaptomethyl)-2-methozy-D2- 2-Chloro-1-(2,4-dichlorophenyl) vinyl diethyl 1,3,4-thiadiazolin-5-one. phosphate. Dioxathion (2,3-p-dioxanedithiol S,S-bis (O,O- Coumaphos (O,O-diethyl O-3-chloro-4-meth- diethylphosphorodithioate)) containing ap- yl-2-oxo-2H-1-benzopyran-7-yl phosran-7-yl proximately 70 percent cis and trans iso- phosphate). mers and approximately 30 percent related Coumaphos oxygen analog (O,O-diethyl O-3- compounds. chloro-4-methyl-2-oxo-2H-1- EPN. benzopyphorothioate). Ethephon ((2- - chloroethyl) phosphonic Dialifor (S-(2-chloro-1-phthalimidoethyl) acid). O,O-diethyl phosphorodithioate). Ethion. Dialifor oxygen analog (S-(2-chloro-1- Ethion oxygen analog (S- phthalimidoethyl) O,O-diethyl [[(diethoxyphosphinothioyl)thio] methyl] phosphorothioate). O,O-diethyl phosphorothioate). Demeton (a mixture of O,O-diethyl O-(and S) [2-ethylthio)ethyl] phosphorothioates). O- Ethyl O-[4-(methylthio) phenyl] S-propyl Ethiolate (S-ethyl diethylthiocarbamate). phosphorodithioate and its cholinesterase- 2,2-Dichlorovinyl dimethyl phosphate. inhibiting metabolites. O,O-Diethyl S-[2-(ethylthio)ethyl] O-Ethyl S,S-dipropylphosphorodithioate. phosphorodithioate and its cholinesterase- Ethyl 3-methyl-4-(methylthio)phenyl (1- inhibiting metabolites. methylethyl) phosphoramidate and its cho- O,O-Diethyl O-(2-diethylamino-6-methyl-4- linesterase-inhibiting metabolites. pyrimidinyl) phosphorothioate and its oxy- O-Ethyl S-phenyl ethylphosphonodithioate. gen analog diethyl 2-diethylamino-6-meth- O-Ethyl S-phenyl ethylphosphonothiolate. yl-4-pyrimidinyl phosphate. m-(1-Ethylpropyl)phenyl methylcarbamate.

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S-[2-Ethylsulfinyl)ethyl] O,O-dimethyl EFFECTIVE DATE NOTE: At 79 FR 27501, May phosphorothioate and its cholinesterase-in- 14, 2014, § 180.3 was amended by revising para- hibiting metabolites, (primarily S-[2- graph (d)(5), effective Nov. 14, 2014. For the (ethyl-sulfonyl)ethyl] O,O-dimethyl convenience of the user, the revised text is phosphorothioate). set forth as follows: Fenthion (O,O-dimethyl O-[3-methyl-4- (methylthio)phenyl]phosphorothioate and § 180.3 Tolerances for related pesticide its cholinesterase-inhibiting metabolites. chemicals. Malathion. N-(Mercaptomethyl)phthalimide S-(O,O-di- * * * * * methyl phosphorodithioate). N-(Mercaptomethyl)phthalimide S-(O,O-di- (d) * * * methyl phosphorothioate). (5) Where tolerances are established for Methomyl (S-methyl N- more than one member of the class of [(methylcarbamoyl)oxy]thioacetimidate). dithiocarbamates listed in paragraph (e)(3) of 1-Methoxycarbonyl-1-propen-2-yl dimethyl this section on the same raw agricultural phosphate and its beta isomer. commodity, the total residue of such pes- m-(1-Methylbutyl)phenyl methylcarbamate. ticides shall not exceed that permitted by Methyl parathion. the highest tolerance established for any one Naled (1,2-dibromo-2,2-dichloroethyl di- member of the class, calculated both as zinc methyl phosphate). ethylenebisdithiocarbamate and carbon di- Oxamyl (methyl N′,N′-dimethyl-N- sulfide. The tolerance based on zinc [(methylcarbamoyl)oxy]-1- ethylenebisdithiocarbamate shall first be thiooxamimidate) multiplied by 0.6 to convert it to the equiva- Parathion. lent carbon disulfide tolerance, and then the Phorate (O,O-diethyl S-(ethylthio)methyl carbon disulfide tolerance levels will be com- phosphorodithioate) and its cholinesterase- pared to determine the highest tolerance inhibiting metabolites. level per raw agricultural commodity. Phosalone (S-(6-chloro-3-mercaptomethyl)-2- benzoxazolinone) O,O-diethyl phosphorodithioate). * * * * * Phosphamidon (2-chloro-2-diethylcarbamoyl- 1-methylvinyl dimethyl phosphate) includ- § 180.4 Exceptions. ing all of its related cholinesterase-inhibiting compounds. The substances listed in this section Pirimiphos-methyl O-[2-diethylamino-6- are excepted from the definitions of methyl-pyrimidinyl) O,O-dimethyl ‘‘pesticide chemical’’ and ‘‘pesticide phosphorothioate chemical residue’’ under FFDCA sec- Ronnel. tion 201(q)(3) and are therefore exempt Schradan (octamethylpyrophosphoramide). from regulation under FFDCA section Tetraethyl pyrophosphate. O,O,O′,O′-Tetramethyl O,O′-sulfinyldi-p- 402(a)(2)(B) and 408. These substances phenylene phosphorothioate. are subject to regulation by the Food O,O,O′,O′-Tetramethyl O,O′-thiodi-p-phen- and Drug Administration as food addi- ylene phosphorothioate. tives under FFDCA section 409. Tributyl phosphorotritlioite. (a) Inert ingredients in food pack- S,S,S-Tributyl phosphorothrithioate. aging treated with a pesticide, when 3,4,5-Trimethylphenyl methylcarbamate and such inert ingredients are the compo- its isomer 2,3,5-trimethylphenyl methylcarbamate. nents of the food packaging material (e.g. paper and paperboard, coatings, (6) The following pesticides are mem- adhesives, and polymers). bers of the class of dinitrophenols: (b) [Reserved] 2,4-Dinitro-6-octylphenyl crotonate and 2,6- [63 FR 10720, Mar. 4, 1998, as amended at 73 dinitro-4-octylphenyl crotonate, mixture FR 54976, Sept. 24, 2008] of. 4,6-Dinitro-o-cresol and its sodium salt. Dinoseb (2-sec-butyl-4,6-dinitrophenol) and § 180.5 Zero tolerances. its alkanolamine, ammonium, and sodium A zero tolerance means that no salts. amount of the pesticide chemical may [41 FR 8969, Mar. 2, 1976] remain on the raw agricultural commodity when it is offered for shipment. EDITORIAL NOTE: For FEDERAL REGISTER citations affecting § 180.3, see the List of CFR A zero tolerance for a pesticide chem- Sections Affected, which appears in the ical in or on a raw agricultural com- Finding Aids section of the printed volume modity may be established because, and at www.fdsys.gov. among other reasons:

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(a) A safe level of the pesticide chem- milk, eggs, meat, and/or poultry. When ical in the diet of two different species it is not possible to determine with cer- of warm-blooded animals has not been tainty whether finite residues will be reliably determined. incurred in milk, eggs, meat, and/or (b) The chemical is carcinogenic to poultry but there is a reasonable expec- or has other alarming physiological ef- tation of finite residues in light of data fects upon one or more of the species of reflecting exaggerated pesticides levels the test animals used, when fed in the in feeding studies, a tolerance will be diet of such animals. established on the raw agricultural (c) The pesticide chemical is toxic, commodity provided that appropriate but is normally used at times when, or tolerances can be established at the in such manner that, fruit, vegetables, same time, on the basis of the toxi- or other raw agricultural commodities cological and other data available, for will not bear or contain it. the finite residues likely to be incurred (d) All residue of the pesticide chem- in these foods through the feed use of ical is normally removed through good the raw agricultural commodity or its agricultural practice such as washing byproducts. When it is not possible to or brushing or through weathering or determine with certainty whether fi- other changes in the chemical itself, nite residues will be incurred in milk, prior to introduction of the raw agri- eggs, meat, and/or poultry but there is cultural commodity into interstate no reasonable expectation of finite res- commerce. idues in light of data such as those re- § 180.6 Pesticide tolerances regarding flecting exaggerated pesticide levels in milk, eggs, meat, and/or poultry; feeding studies and those elucidating statement of policy. the biochemistry of the pesticide chemical in the animal, a tolerance (a) When establishing tolerances for may be established on the raw agricul- pesticide residues in or on raw agricultural commodities, consideration is al- tural commodity without the necessity ways given to possible residues of those of a tolerance on food products derived pesticide chemicals or their conversion from the animal. products entering the diet of man (c) The principles outlined in para- through the ingestion of milk, eggs, graphs (a) and (b) of this section will meat, and/or poultry produced by ani- also be followed with respect to toler- mals fed agricultural products bearing ances for residues which will actually such pesticide residues. In each in- be incurred or are reasonably to be ex- stance an evaluation of all available pected in milk, eggs, meat, and/or poul- data will result in a conclusion either: try by the use of pesticides directly on (1) That finite residues will actually the animal or administered purposely be incurred in these foods from feed use in the feed or drinking water. of the raw agricultural commodity in- (d) Tolerances contemplated by para- cluding its byproducts; or graphs (a) and (b) of this section will in (2) That it is not possible to establish addition to toxicological consider- with certainty whether finite residues ations be conditioned on the avail- will be incurred, but there is a reason- ability of a practicable analytical able expectation of finite residues; or method to determine the pesticide res- (3) That it is not possible to establish idue; that is, the method must be sen- with certainty whether finite residues sitive and reliable at the tolerance will be incurred, but there is no reason- level or in special cases at a higher able expectation of finite residues. level where such level is deemed satis- (b) When the data show that finite factory and safe in light of the toxicity residues will actually be incurred in of the pesticide residue and of the un- milk, eggs, meat, and/or poultry, a tol- likelihood of such residue exceeding erance will be established on the raw the tolerance. The analytical methods agricultural commodity used as feed to be used for enforcement purposes provided that tolerances can be estab- will be those set forth in the ‘‘Pesticide lished at the same time, on the basis of Analytical Manual’’ (see § 180.101(c)). the toxicological and other data avail- The sensitivities of these methods are able, for the finite residues incurred in expressed in that manual.

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Subpart B—Procedural (6) Full reports of tests and inves- Regulations tigations made with respect to the na- ture and amount of the pesticide chem- § 180.7 Petitions proposing tolerances ical residue that is likely to remain in or exemptions for pesticide resi- or on the food, including a description dues in or on raw agricultural com- of the analytical methods used. (See modities or processed foods. § 180.34 for further information about (a) Petitions to be filed with the residue tests.) Agency under the provisions of FFDCA (7) Proposed tolerances for the pes- section 408(d) shall be submitted in du- ticide chemical residue if tolerances plicate. If any part of the material sub- are proposed. mitted is in a foreign language, it shall (8) Practicable methods for removing be accompanied by an accurate and any amount of the residue that would complete English translation. The peti- exceed any proposed tolerance. tion shall be accompanied by an ad- (9) A practical method for detecting vance deposit for fees described in and measuring the levels of the pes- § 180.33. The petition shall state the pe- ticide chemical residue in or on the titioner’s mail address to which notice food, or for exemptions, a statement of objection under FFDCA section why such a method is not needed. 408(g)(2) may be sent. The petition (10) If the petition relates to a toler- must be signed by the petitioner or by ance for a processed food, reports of in- his attorney or agent, or (if a corpora- vestigations conducted using the proc- tion) by an authorized official. essing method(s) used to produce that (b) Petitions shall include the fol- food. lowing information: (11) Such information as the Admin- (1) An informative summary of the istrator may require to make the de- petition and of the data, information, termination under FFDCA section and arguments submitted or cited in 408(b)(2)(C). support of the petition. Both a paper (12) Such information as the Admin- and electronic copy of the summary istrator may require on whether the should be submitted. The electronic pesticide chemical may have an effect copy should be formatted according to in humans that is similar to an effect the Office of Pesticide Programs’ cur- produced by a naturally occurring es- rent standard for electronic data sub- trogen or other endocrine effects. mission as specified at http:// (13) Information regarding exposure www.epa.gov/pesticides/regulating/reg- to the pesticide chemical residue due istering/submissions/index.htm. to any tolerance or exemption already (2) A statement that the petitioner granted for such residue. agrees that such summary or any in- (14) Information concerning any max- formation it contains may be published imum residue level established by the as a part of the notice of filing of the Codex Alimentarius Commission for petition to be published under FFDCA the pesticide chemical residue ad- section 408(d)(3) and as a part of a pro- dressed in the petition. If a Codex max- posed or final regulation issued under imum residue level has been estab- FFDCA section 408. lished for the pesticide chemical res- (3) The name, chemical identity, and idue and the petitioner does not pro- composition of the pesticide chemical pose that this level be adopted, a state- residue and of the pesticide chemical ment explaining the reasons for this that produces the residue. departure from the Codex level. (4) Data showing the recommended (15) Such other data and information amount, frequency, method, and time as the Administrator requires by regu- of application of the pesticide chem- lation to support the petition. ical. (16) Reasonable grounds in support of (5) Full reports of tests and inves- the petition. tigations made with respect to the (c) The data specified under para- safety of the pesticide chemical, in- graphs (b)(1) through (b)(16) of this sec- cluding full information as to the tion should be on separate sheets or methods and controls used in con- sets of sheets, suitably identified. If ducting those tests and investigations. such data have already been submitted

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with an earlier application, the present The full text of the summary may be petition may incorporate it by ref- omitted from the notice. erence to the earlier one. (g) The Administrator may request a (d) Except as noted in paragraph (e) sample of the pesticide chemical at any of this section, a petition shall not be time while a petition is under consider- accepted for filing if any of the data ation. The Administrator shall specify prescribed by FFDCA section 408(d) are in its request for a sample of the pes- lacking or are not set forth so as to be ticide chemical, a quantity which it readily understood. The availability to deems adequate to permit tests of ana- the public of information provided to, lytical methods used to determine resi- or otherwise obtained by, the Agency dues of the pesticide chemical and of under this part shall be governed by methods proposed by the petitioner for part 2 of this chapter. The Adminis- removing any residues of the chemical trator shall make the full text of the that exceed the tolerance proposed. summary referenced in paragraph (b)(1) of this section available to the public (h) The Administrator shall deter- in the public docket at http:// mine, in accordance with the Act, www.regulations.gov no later than pub- whether to issue an order that establishes, modifies, or revokes a tolerance lication in the FEDERAL REGISTER of the notice of the petition filing. regulation (whether or not in accord (e) The Administrator shall notify with the action proposed by the peti- the petitioner within 15 days after its tioner), whether to publish a proposed receipt of acceptance or nonacceptance tolerance regulation and request public of a petition, and if not accepted the comment thereon under § 180.29, or reasons therefor. If petitioner desires, whether to deny the petition. The Ad- the petitioner may supplement a defi- ministrator shall publish in the FED- cient petition after notification as to ERAL REGISTER such order or proposed deficiencies. If the petitioner does not regulation. After receiving comments wish to supplement or explain the peti- on any proposed regulation, the Ad- tion and requests in writing that it be ministrator may issue an order that es- filed as submitted, the petition shall be tablishes, modifies, or revokes a toler- filed and the petitioner so notified. ance regulation. An order published (f) A notice of the filing of a petition under this section shall describe briefly for a pesticide chemical residue toler- how to submit objections and requests ance that the Administrator deter- for a hearing under part 178 of this mines has met the requirements of chapter. A regulation issued under this paragraph (b) of this section shall be section shall be effective on the date of published in the FEDERAL REGISTER by publication in the FEDERAL REGISTER the Administrator within 30 days after unless otherwise provided in the regu- such determination. The notice shall lation. state the name of the pesticide chemical residue and the commodities for [70 FR 33360, June 8, 2005, as amended at 73 which a tolerance is sought and an- FR 75600, Dec. 12, 2008] nounce the availability of a description § 180.8 Withdrawal of petitions with- of the analytical methods available to out prejudice. the Administrator for the detection and measurement of the pesticide In some cases the Administrator will chemical residue with respect to which notify the petitioner that the petition, the petition is filed or shall set forth while technically complete, is inad- the petitioner’s statement of why such equate to justify the establishment of a a method is not needed. The notice tolerance or the tolerance requested by shall explicitly reference the specific petitioner. This may be due to the fact docket identification number in the that the data are not sufficiently clear public docket at http:// or complete. In such cases, the peti- www.regulations.gov where the full text tioner may withdraw the petition pend- of the summary required in paragraph ing its clarification or the obtaining of (b) of this section is located, and refer additional data. This withdrawal may interested parties to this document for be without prejudice to a future filing. further information on the petition. A deposit for fees as specified in § 180.33

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shall accompany the resubmission of (1) Regulations establishing general the petition. procedures and requirements under FFDCA section 408(e)(1)(C). [70 FR 33361, June 8, 2005] (2) Orders issued under FFDCA section 408(f)(1)(C) requiring the submis- § 180.9 Substantive amendments to petitions. sion of data. (3) Orders issued under FFDCA sec- After a petition has been filed, the tion 408(g)(2)(C) ruling on objections to petitioner may submit additional in- establishment, modification, or revoca- formation or data in support thereof, tion of a tolerance or exemption under but in such cases the petition will be FFDCA section 408(d)(4), or any regula- given a new filing date. tion that is the subject of such an [70 FR 33361, June 8, 2005] order. The underlying action here is Agency disposition of a petition seek- § 180.29 Establishment, modification, ing the establishment, modification, or and revocation of tolerance on ini- revocation of a tolerance or exemption. tiative of Administrator. (4) Orders issued under FFDCA section 408(g)(2)(C) ruling on objections to (a) Upon the Administrator’s own ini- the denial of a petition under FFDCA tiative, the Administrator may pro- section 408(d)(4). pose, under FFDCA section 408(e), the (5) Orders issued under FFDCA sec- issuance of a regulation establishing a tion 408(g)(2)(C) ruling on objections to tolerance for a pesticide chemical or the establishment, modification, sus- exempting it from the necessity of a pension, or revocation of a tolerance or tolerance, or a regulation modifying or exemption under FFDCA section revoking an existing tolerance or ex- 408(e)(1)(A) or (e)(1)(B). The underlying emption. action here is the establishment, modi- (b) The Administrator shall provide a fication, suspension, or revocation of a period of not less than 60 days for per- tolerance or exemption upon the initia- sons to comment on the proposed regu- tive of EPA including EPA actions pur- lation, except that a shorter period for suant to FFDCA sections comment may be provided if the Ad- 408(b)(2)(B)(v), 408(b)(2)(E)(ii), ministrator for good cause finds that it 408(d)(4)(C)(ii), 408(l)(4), and 408(q)(1). would be in the public interest to do so (6) Orders issued under FFDCA sec- and states the reasons for the finding tion 408(g)(2)(C) ruling on objections to in the notice of proposed rulemaking. the revocation or modification of a tol- (c) After reviewing any timely com- erance or exemption under FFDCA sec- ments received, the Administrator may tion 408(f)(2) for noncompliance with by order establish, modify, or revoke a requirements for the submission of tolerance regulation, which order and data. regulation shall be published in the (7) Orders issued under FFDCA sec- FEDERAL REGISTER. An order published tion 408(g)(2)(C) ruling on objections to under this section shall state that per- rules issued under FFDCA sections sons may submit objections and re- 408(n)(3) and 408(d) or (e) regarding de- quests for a hearing in the manner determinations pertaining to State au- scribed in part 178 of this chapter. thority to establish regulatory limits (d) Any final regulation issued under on pesticide chemical residues. this section shall be effective on the (8) Orders issued under FFDCA sec- date of publication in the FEDERAL tion 408(g)(2)(C) ruling on objections to REGISTER unless otherwise provided in orders issued under FFDCA section the regulation. 408(n)(5)(C) authorizing States to establish regulatory limits not identical to [70 FR 33361, June 8, 2005] certain tolerances or exemptions. (b) Any issue as to which review is or § 180.30 Judicial review. was obtainable under paragraph (a) of (a) Under FFDCA section 408(h), judi- this section shall not be the subject of cial review is available in the United judicial review under any other provi- States Courts of Appeal as to the fol- sion of law. In part, this means that, lowing actions: for the Agency actions subject to the

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objection procedure in FFDCA section (e) Conditions under which a tem- 408(g)(2), judicial review is not avail- porary tolerance is established shall in- able unless an adversely affected party clude: exhausts these objection procedures, (1) A limitation on the amount of the and any petition procedures prelimi- chemical to be used on the designated nary thereto. crops permitted under the experimental permit. [70 FR 33362, June 8, 2005] (2) A limitation for the use of the chemical on the designated crops to § 180.31 Temporary tolerances. bona fide experimental use by qualified (a) A temporary tolerance (or exemp- persons as indicated in the experi- tion from a tolerance) established mental permit. under the authority of FFDCA section (3) A requirement that the person or 408(r) shall be deemed to be a tolerance firm which obtains the experimental (or exemption from the requirement of permit for which the temporary toler- a tolerance) for the purposes of FFDCA ance is established will immediately section 408(a)(1) or (a)(2) and for the inform the Environmental Protection purposes of § 180.30. Agency of any reports on findings from (b) A request for a temporary toler- the experimental use that have a bear- ance or a temporary exemption from a ing on safety. (4) A requirement that the person or tolerance by a person who has obtained firm which obtained the experimental or is seeking an experimental permit permit for which the temporary toler- for a pesticide chemical under the Fed- ance is established will keep records of eral Insecticide, Fungicide, and production, distribution, and perform- Rodenticide Act shall be accompanied ance for a period of 2 years and, on re- by such data as are available on sub- quest, at any reasonable time, make jects outlined in § 180.7(b) and an ad- these records available to any author- vance deposit to cover fees as provided ized officer or employee of the Environ- in § 180.33. mental Protection Agency. (c) To obtain a temporary tolerance, a requestor must comply with the peti- [70 FR 33362, June 8, 2005] tion procedures specified in FFDCA § 180.32 Procedure for modifying and section 408(d) and § 180.7 except as pro- revoking tolerances or exemptions vided in this section. from tolerances. (d) A temporary tolerance or exemp- (a) The Administrator on his/her own tion from a tolerance may be issued for initiative may propose the issuance of a period designed to allow the orderly a regulation modifying or revoking a marketing of the raw agricultural com- tolerance for a pesticide chemical res- modities produced while testing a pes- idue on raw agricultural commodities ticide chemical under an experimental or processed foods or modifying or re- permit issued under authority of the voking an exemption from tolerance Federal Insecticide, Fungicide, and for such residue. Rodenticide Act if the Administrator (b) Any person may file with the Ad- concludes that the safety standard in ministrator a petition proposing the FFDCA section 408(b)(2) or (c), as appli- issuance of a regulation modifying or cable, is met. Subject to the require- revoking a tolerance or exemption ments of FFDCA section 408(e), a tem- from a tolerance for a pesticide chem- porary tolerance or exemption from a ical residue. The petition shall furnish tolerance may be revoked if the experi- reasonable grounds for the action mental permit is revoked, or may be sought. Reasonable grounds shall in- revoked at any time if it develops that clude an explanation showing wherein the application for a temporary toler- the person has a substantial interest in ance contains a misstatement of a ma- such tolerance or exemption from tol- terial fact or that new scientific data erance and an assertion of facts (sup- or experience with the pesticide chem- ported by data if available) showing ical indicates that it does not meet the that new uses for the pesticide chem- safety standard in FFDCA section ical have been developed or old uses 408(b)(2) or (c), as applicable. abandoned, that new data are available

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as to toxicity of the chemical, or that tion shall be accompanied by a fee of experience with the application of the $4,600. tolerance or exemption from tolerance (e) A petition or request for a tem- may justify its modification or revoca- porary tolerance for a pesticide chem- tion. Evidence that a person has reg- ical which has a tolerance for other istered or has submitted an application uses at the same numerical level or a for the registration of a pesticide under higher numerical level shall be accom- the Federal Insecticide, Fungicide, and panied by a fee of $16,075, plus $1,225 for Rodenticide Act will be regarded as each raw agricultural commodity on evidence that the person has a substan- which the temporary tolerance is tial interest in a tolerance or exemp- sought. tion from the requirement of a toler- (f) Each petition for revocation of a ance for a pesticide chemical that con- tolerance shall be accompanied by a fee sists in whole or in part of the pes- of $10,125. Such fee is not required ticide. New data should be furnished in when, in connection with the change the form specified in § 180.7(b) for sub- sought under this paragraph, a petition mitting petitions, as applicable. is filed for the establishment of new (c) The procedures for completing ac- tolerances to take the place of those tion on an Administrator initiated pro- sought to be revoked and a fee is paid posal or a petition shall be those speci- as required by paragraph (a) of this sec- fied in §§ 180.29 and 180.7, as applicable. tion. [70 FR 33362, June 8, 2005] (g) If a petition or a request is not accepted for processing because it is § 180.33 Fees. technically incomplete, the fee, less (a) Each petition for the establish- $2,025 for handling and initial review, ment of a new tolerance or a tolerance shall be returned. If a petition is with- higher than already established, shall drawn by the petitioner after initial be accompanied by a fee of $80,950, plus processing, but before significant Agen- $2,025 for each raw agricultural com- cy scientific review has begun, the fee, modity more than nine on which the less $2,025 for handling and initial re- establishment of a tolerance is review, shall be returned. If an unaccept- quested, except as provided in para- able or withdrawn petition is resub- graphs (b), (d), and (h) of this section. mitted, it shall be accompanied by the (b) Each petition for the establish- fee that would be required if it were ment of a tolerance at a lower numer- being submitted for the first time. ical level or levels than a tolerance al- (h) Each petition for a crop group tol- ready established for the same pes- erance, regardless of the number of raw ticide chemical, or for the establish- agricultural commodities involved, ment of a tolerance on additional raw shall be accompanied by a fee equal to agricultural commodities at the same the fee required by the analogous cat- numerical level as a tolerance already egory for a single tolerance that is not established for the same pesticide a crop group tolerance, i.e., paragraphs chemical, shall be accompanied by a (a) through (f) of this section, without fee of $18,500 plus $1,225 for each raw a charge for each commodity where agricultural commodity on which a tol- that would otherwise apply. erance is requested. (i) Objections under section 408(d)(5) (c) Each petition for an exemption of the Act shall be accompanied by a from the requirement of a tolerance or filing fee of $4,050. repeal of an exemption shall be accom- (j) The person who files a petition for panied by a fee of $14,925. judicial review of an order under sec- (d) Each petition or request for a tion 408(h) of the Act shall pay the temporary tolerance or a temporary costs of preparing the record on which exemption from the requirement of a the order is based unless the person has tolerance shall be accompanied by a fee no financial interest in the petition for of $32,325 except as provided in para- judicial review. graph (e) of this section. A petition or (k) No fee under this section will be request to renew or extend such tem- imposed on the Interregional Research porary tolerance or temporary exemp- Project Number 4 (IR-4 Program).

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(l) The Administrator may waive or Schedule (GS) pay scale. In addition, refund part or all of any fee imposed by processing costs and fees will periodi- this section if the Administrator deter- cally be reviewed and changes will be mines in his or her sole discretion that made to the schedule as necessary. such a waiver or refund will promote When automatic adjustments are made the public interest or that payment of based on the GS pay scale, the new fee the fee would work an unreasonable schedule will be published in the FED- hardship on the person on whom the ERAL REGISTER as a final rule to be- fee is imposed. A request for waiver or come effective 30 days or more after refund of a fee shall be submitted to publication, as specified in the rule. the Office of Pesticide Programs’ Docu- When changes are made based on peri- ment Processing Desk at the appro- odic reviews, the changes will be sub- priate address as set forth in 40 CFR ject to public comment. 150.17(a) or (b). A fee of $2,025 shall ac- (o) No fee required by this section company every request for a waiver or shall be levied during the period begin- refund, as specified in paragraph (m) of ning on October 1, 2003, and ending Sep- this section, except that the fee under tember 30, 2008. this paragraph shall not be imposed on any person who has no financial inter- [68 FR 24371, May 7, 2003, as amended at 69 est in any action requested by such FR 12544, Mar. 17, 2004; 70 FR 33363, June 8, person under paragraphs (a) through (j) 2005; 71 FR 35547, June 21, 2006] of this section. The fee for requesting a § 180.34 Tests on the amount of res- waiver or refund shall be refunded if idue remaining. the request is granted. (m) All deposits and fees required by (a) Data in a petition on the amount the regulations in this part shall be of residue remaining in or on a raw ag- paid by money order, bank draft, or ricultural commodity should establish certified check drawn to the order of the residue that may remain when the the Environmental Protection Agency. pesticide chemical is applied according All deposits and fees shall be forwarded to directions registered under the Fed- to the Environmental Protection Agen- eral Insecticide, Fungicide, and cy, Headquarters Accounting Oper- Rodenticide Act, or according to direc- ations Branch, Office of Pesticide Pro- tions contained in an application for grams (Tolerance Fees), P.O. Box registration. These data should estab- 360277M, Pittsburgh, PA 15251. The pay- lish the residues that may remain ments should be specifically labeled under conditions most likely to result ‘‘Tolerance Petition Fees’’ and should in high residues on the commodity. be accompanied only by a copy of the (b) The petition should establish the letter or petition requesting the toler- reliability of the residue data reported ance. The actual letter or petition, in it. Sufficient information should be along with supporting data, shall be submitted about the analytical method forwarded within 30 days of payment to to permit competent analysts to apply the Office of Pesticide Programs’ Docu- it successfully. ment Processing Desk at the appro- (c) If the pesticide chemical is ab- priate address as set forth in 40 CFR sorbed into a living plant or animal 150.17(a) or (b). A petition will not be when applied (is systemic), residue accepted for processing until the re- data may be needed on each plant or quired fees have been submitted. A pe- animal on which a tolerance or exemp- tition for which a waiver of fees has tion is requested. been requested will not be accepted for (d) If the pesticide chemical is not processing until the fee has been absorbed into the living plant or ani- waived or, if the waiver has been de- mal when applied (is not systemic), it nied, the proper fee is submitted after may be possible to make a reliable es- notice of denial. A request for waiver timate of the residues to be expected or refund will not be accepted after sci- on each commodity in a group of re- entific review has begun on a petition. lated commodities on the basis of less (n) This fee schedule will be changed data than would be required for each annually by the same percentage as the commodity in the group, considered percent change in the Federal General separately.

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(e) Each of the following groups of grass, soybean hay, sudan grass, tim- crops lists raw agricultural commod- othy, and vetch. ities that are considered to be related (26) Corn forage, sorghum forage. for the purpose of paragraph (d) of this (27) Sugarcane, cane sorghum. section. Commodities not listed in this paragraph are not considered to be re- [36 FR 22540, Nov. 25, 1971, as amended at 39 lated for the purpose of paragraph (d) FR 28286, Aug. 6, 1974; 39 FR 28977, Aug. 13, 1974; 40 FR 6972, Feb. 18, 1975; 45 FR 82928, of this section. Dec. 17, 1980; 48 FR 29860, June 29, 1983; 60 FR (1) Apples, crabapples, pears, quinces. 26635, May 17, 1995; 73 FR 75600, Dec. 12, 2008] (2) Avocados, papayas. (3) Blackberries, boysenberries, § 180.35 Tests for potentiation. dewberries, loganberries, raspberries. Experiments have shown that certain (4) Blueberries, currants, goose- cholinesterase-inhibiting pesticides berries, huckleberries. when fed together to test animals are (5) Cherries, plums, prunes. more toxic than the sum of their indi- (6) Oranges, citrus citron, grapefruit, vidual toxicities when fed separately. kumquats, lemons, limes, tangelos, One substance potentiates the toxicity tangerines. of the other. Important toxicological (7) Mangoes, persimmons. interactions also have been observed (8) Peaches, apricots, nectarines. between pesticides and other sub- (9) Beans, peas, soybeans (each in dry stances. Wherever there is reason to form). believe that a pesticide chemical for (10) Beans, peas, soybeans (each in which a tolerance is proposed may succulent form). interact with other pesticide chemicals (11) Broccoli, brussels sprouts, cauli- or other substances to which man is ex- flower, kohlrabi. posed, it may be necessary to require (12) Cantaloups, honeydew melons, special experimental data regarding muskmelons, pumpkins, watermelons, potentiation capacities to evaluate the winter squash. safety of the proposed tolerance. This (13) Carrots, garden beets, sugar necessarily will be determined on a beets, horseradish, parsnips, radishes, case-by-case basis. rutabagas, salsify roots, turnips. (14) Celery, fennel. § 180.40 Tolerances for crop groups. (15) Cucumbers, summer squash. (16) Lettuce, endive (escarole), Chi- (a) Group or subgroup tolerances may nese cabbage, salsify tops. be established as a result of: (17) Onions, garlic, leeks, shallots (1) A petition from a person who has (green, or in dry bulb form). submitted an application for the reg- (18) Potatoes, Jerusalem-artichokes, istration of a pesticide under the Fed- sweetpotatoes, yams. eral Insecticide, Fungicide, and (19) Spinach, beet tops, collards, dan- Rodenticide Act. delion, kale, mustard greens, parsley, (2) On the initiative of the Adminis- Swiss chard, turnip tops, watercress. trator. (20) Tomatoes, eggplants, peppers, pi- (3) A petition by an interested per- mentos. son. (21) Pecans, almonds, brazil nuts, (b) The tables in § 180.41 are to be bush nuts, butternuts, chestnuts, fil- used in conjunction with this section berts, hazelnuts, hickory nuts, wal- for the establishment of crop group tol- nuts. erances. Each table in § 180.41 lists a (22) Field corn, popcorn, sweet corn group of raw agricultural commodities (each in grain form). that are considered to be related for (23) Milo, sorghum (each in grain the purposes of this section. Refer also form). to § 180.1(g) for a listing of commodities (24) Wheat, barley, oats, rice, rye for which established tolerances may (each in grain form). be applied to certain other related and (25) Alfalfa, Bermuda grass, blue- similar commodities. grass, brome grass, clovers, cowpea (c) When there is an established or hay, fescue, lespedeza, lupines, orchard proposed tolerance for all of the rep- grass, peanut hay, peavine hay, rye resentative commodities for a specific

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group or subgroup of related commod- rather than group tolerances, will nor- ities, a tolerance may be established mally be established. for all commodities in the associated (h) Alternatively, a commodity with group or subgroup. Tolerances may be a residue level significantly higher or established for a crop group or, alter- lower than the other commodities in a natively, tolerances may be established group may be excluded from the group for one or more of the subgroups of a tolerance (e.g., cereal grains, except crop group. corn). In this case an individual toler- (d) The representative crops are ance at the appropriate level for the given as an indication of the minimum unique commodity would be estab- residue chemistry data base acceptable lished, if necessary. The alternative ap- to the Agency for the purposes of es- proach of excluding a commodity with tablishing a group tolerance. The a significantly higher or lower residue Agency may, at its discretion, allow level will not be used to establish a tol- group tolerances when data on suitable erance for a commodity subgroup. Most substitutes for the representative crops subgroups have only two representa- are available (e.g., limes instead of tive commodities; to exclude one such lemons). commodity and its related residue data (e) Since a group tolerance reflects would likely provide insufficient res- maximum residues likely to occur on idue information to support the re- all individual crops within a group, the mainder of the subgroup. Residue data proposed or registered patterns of use from crops additional to those rep- for all crops in the group or subgroup resentative crops in a grouping may be must be similar before a group toler- required for systemic pesticides. ance is established. The pattern of use consists of the amount of pesticide ap- (i) The commodities included in the plied, the number of times applied, the groups will be updated periodically ei- timing of the first application, the in- ther at the initiative of the Agency or terval between applications, and the at the request of an interested party. interval between the last application Persons interested in updating this sec- and harvest. The pattern of use will tion should contact the Registration also include the type of application; for Division of the Office of Pesticide Pro- example, soil or foliar application, or grams. application by ground or aerial equip- (j) When EPA amends a crop group in ment. a manner that expands or contracts the (f) When the crop grouping contains commodities that are covered by the commodities or byproducts that are group, EPA will initially retain the utilized for animal feed, any needed pre-existing as well as the revised crop tolerance or exemption from a toler- group in the CFR. The revised crop ance for the pesticide in meat, milk, group will have the same number as poultry and/or eggs must be established the pre-existing crop group; however, before a tolerance will be granted for the revised crop group number will be the group as a whole. The representa- followed by a hyphen and the final two tive crops include all crops in the digits of the year in which it was estab- group that could be processed such lished (e.g., if Crop Group 1 is amended that residues may concentrate in proc- in 2007, the revised group will be des- essed food and/or feed. Processing data ignated as Crop Group 1-07). If the pre- will be required prior to establishment existing crop group had crop sub- of a group tolerance. Tolerances will groups, these subgroups will be num- not be granted on a group basis as to bered in a similar fashion in the re- processed foods prepared from crops vised crop group. The name of the re- covered by the group tolerance. vised crop group will not be changed (g) If maximum residues (tolerances) from the pre-existing crop group unless for the representative crops vary by the revision so changes the composi- more than a factor of 5 from the max- tion of the crop group that the pre-ex- imum value observed for any crop in isting name is no longer accurate. Once the group, a group or subgroup toler- a revised crop group is established, ance will ordinarily not be established. EPA will no longer establish tolerances In this case individual crop tolerances, under the pre-existing crop group. At

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appropriate times, EPA will amend tol- dividual tolerances must be estab- erances for crop groups that have been lished. Miscellaneous commodities in- superseded by revised crop groups to tentionally not included in any group conform the pre-existing crop group to include asparagus, avocado, banana, the revised crop group. Once all of the fig, globe artichoke, hops, mango, pa- tolerances for the pre-existing crop paya, pawpaw, peanut, persimmon, group have been updated, the pre-exist- pineapple, water chestnut, and water- ing crop group will be removed from cress. the CFR. (c) Each group is identified by a (k) Establishment of a tolerance does group name and consists of a list of not substitute for the additional need representative commodities followed to register the pesticide under a com- panion law, the Federal Insecticide, by a list of all commodity members for Fungicide, and Rodenticide Act. The the group. If the group includes sub- Registration Division of the Office of groups, each subgroup lists the sub- Pesticide Programs should be con- group name, the representative com- tacted concerning procedures for reg- modity or commodities, and the mem- istration of new uses of a pesticide. ber commodities for the subgroup. Sub- groups, which are a subset of their as- [60 FR 26635, May 17, 1995, as amended at 70 sociated crop group, are established for FR 33363, June 8, 2005; 72 FR 69155, Dec. 7, 2007; 75 FR 56014, Sept. 15, 2010] some but not all crops groups. (1) Crop Group 1: Root and Tuber § 180.41 Crop group tables. Vegetables Group. (a) The tables in this section are to (i) Representative commodities. Carrot, be used in conjunction with § 180.40 to potato, radish, and sugar beet. establish crop group tolerances. (ii) Table. The following table 1 lists (b) Commodities not listed are not all the commodities included in Crop considered as included in the groups for Group 1 and identifies the related crop the purposes of this paragraph, and in- subgroups.

TABLE 1—CROP GROUP 1: ROOT AND TUBER VEGETABLES

Related crop Commodities subgroups

Arracacha (Arracacia xanthorrhiza) ...... 1C, 1D Arrowroot (Maranta arundinacea) ...... 1C, 1D Artichoke, Chinese (Stachys affinis) ...... 1C, 1D Artichoke, Jerusalem (Helianthus tuberosus) ...... 1C, 1D Beet, garden (Beta vulgaris) ...... 1A, 1B Beet, sugar (Beta vulgaris) ...... 1A Burdock, edible (Arctium lappa) ...... 1A, 1B Canna, edible (Queensland arrowroot) (Canna indica) ...... 1C, 1D Carrot (Daucus carota) ...... 1A, 1B Cassava, bitter and sweet (Manihot esculenta) ...... 1C, 1D Celeriac (celery root) (Apium graveolens var. rapaceum) ...... 1A, 1B Chayote (root) (Sechium edule) ...... 1C, 1D Chervil, turnip-rooted (Chaerophyllum bulbosum)...... 1A, 1B Chicory (Cichorium intybus) ...... 1A, 1B Chufa (Cyperus esculentus) ...... 1C, 1D Dasheen (taro) (Colocasia esculenta) ...... 1C, 1D Ginger (Zingiber officinale) ...... 1C, 1D Ginseng (Panax quinquefolius) ...... 1A, 1B Horseradish (Armoracia rusticana) ...... 1A, 1B Leren (Calathea allouia) ...... 1C, 1D Parsley, turnip-rooted (Petroselinum crispum var. tuberosum) ...... 1A, 1B Parsnip (Pastinaca sativa) ...... 1A, 1B Potato (Solanum tuberosum) ...... 1C Radish (Raphanus sativus) ...... 1A, 1B Radish, oriental (daikon) (Raphanus sativus subvar. longipinnatus) ...... 1A, 1B Rutabaga (Brassica campestris var. napobrassica) ...... 1A, 1B Salsify (oyster plant) (Tragopogon porrifolius)...... 1A, 1B Salsify, black (Scorzonera hispanica) ...... 1A, 1B Salsify, Spanish (Scolymus hispanicus) ...... 1A, 1B Skirret (Sium sisarum) ...... 1A, 1B Sweet potato (Ipomoea batatas) ...... 1C, 1D Tanier (cocoyam) (Xanthosoma sagittifolium) ...... 1C, 1D Turmeric (Curcuma longa) ...... 1C, 1D

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TABLE 1—CROP GROUP 1: ROOT AND TUBER VEGETABLES—Continued

Related crop Commodities subgroups

Turnip (Brassica rapa var. rapa) ...... 1A, 1B Yam bean (jicama, manoic pea) (Pachyrhizus spp.) ...... 1C, 1D Yam, true (Dioscorea spp.) ...... 1C, 1D

(iii) Table. The following table 2 iden- commodity(ies) for each subgroup, and tifies the crop subgroups for Crop lists all the commodities included in Group 1, specifies the representative each subgroup.

TABLE 2—CROP GROUP 1 SUBGROUP LISTING

Representative commodities Commodities

Crop Subgroup 1A. Root vegetables subgroup. Carrot, radish, and sugar beet...... Beet, garden; beet, sugar; burdock, edible; carrot; celeriac; chervil, turnip-rooted; chicory; ginseng; horseradish; parsley, turnip-rooted; parsnip; radish; radish, oriental; rutabaga; salsify; salsify, black; salsify, Spanish; skirret; turnip. Crop Subgroup 1B. Root vegetables (except sugar beet) subgroup. Carrot and radish...... Beet, garden; burdock, edible; carrot; celeriac; chervil, turnip-rooted; chicory; ginseng; horseradish; parsley, turnip-rooted; parsnip; radish; radish, oriental; rutabaga; salsify; salsify, black; salsify, Spanish; skirret; turnip. Crop Subgroup 1C. Tuberous and corm vegetables subgroup. Potato...... Arracacha; arrowroot; artichoke, Chinese; artichoke, Jerusalem; canna, edible; cassava, bitter and sweet; chayote (root); chufa; dasheen; ginger; leren; potato; sweet potato; tanier; turmeric; yam bean; yam, true. Crop Subgroup 1D. Tuberous and corm vegetables (except potato) subgroup. Sweet potato...... Arracacha; arrowroot; artichoke, Chinese; artichoke, Jerusalem; canna, edible; cassava, bitter and sweet; chayote (root); chufa; dasheen; ginger; leren; sweet potato; tanier; turmeric; yam bean; yam, true.

(2) Crop Group 2. Leaves of Root and Radish, oriental (daikon) (Raphanus sativus Tuber Vegetables (Human Food or Ani- subvar. longipinnatus) mal Feed) Group (Human Food or Ani- Rutabaga (Brassica campestris var. mal Feed) Group. napobrassica) (i) Representative commodities. Turnip Salsify, black (Scorzonera hispanica) and garden beet or sugar beet. Sweet potato (Ipomoea batatas) Tanier (cocoyam) (Xanthosoma sagittifolium) (ii) Commodities. The following is a Turnip (Brassica rapa var. rapa) list of all the commodities included in Yam, true (Dioscorea spp.) Crop Group 2: (3) Crop Group 3. Bulb Vegetables CROP GROUP 2: LEAVES OF ROOT AND TUBER (Allium spp.) Group. VEGETABLES (HUMAN FOOD OR ANIMAL FEED) GROUP—COMMODITIES (i) Representative commodities. Onion, green; and onion, dry bulb. Beet, garden (Beta vulgaris) (ii) Commodities. The following is a Beet, sugar (Beta vulgaris) list of all the commodities in Crop Burdock, edible (Arctium lappa) Group 3. Carrot (Daucus carota) Cassava, bitter and sweet (Manihot esculenta) CROP GROUP 3: BULB VEGETABLE (Allium SPP.) Celeriac (celery root) (Apium graveolens var. GROUP—COMMODITIES rapaceum) Chervil, turnip-rooted (Chaerophyllum Garlic, bulb (Allium sativum) bulbosum) Garlic, great headed, (elephant) (Allium ampeloprasum var. ampeloprasum) Chicory (Cichorium intybus) Leek (Allium ampeloprasum, A. porrum, A. tricoccum) Dasheen (taro) (Colocasia esculenta) Onion, dry bulb and green (Allium cepa, A. fistulosum) Parsnip (Pastinaca sativa) Onion, Welsh, (Allium fistulosum) Radish (Raphanus sativus) Shallot (Allium cepa var. cepa)

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(4) Crop Group 3-07. Bulb Vegetable (ii) Table. The following Table 1 lists Group. all the commodities listed in Crop (i) Representative Commodities. Onion, Group 3-07 and identifies the related bulb and onion, green. crop subgroups.

TABLE 1—CROP GROUP 3-07: BULB VEGETABLE GROUP

Commodities Related crop subgroups

Chive, fresh leaves (Allium schoenoprasum L.) ...... 3-07B Chive, Chinese, fresh leaves (Allium tuberosum Rottler ex Spreng) ...... 3-07B Daylily, bulb (Hemerocallis fulva (L.) L. var. fulva) ...... 3-07A Elegans hosta (Hosta Sieboldiana (Hook.) Engl) ...... 3-07B Fritillaria, bulb (Fritillaria L. fritillary) ...... 3-07A Fritillaria, leaves (Fritillaria L. fritillary) ...... 3-07B Garlic, bulb (Allium sativum L. var. sativum) (A. sativum Common Garlic Group) ...... 3-07A Garlic, great headed, bulb (Allium ampeloprasum L. var. ampeloprasum) (A. ampeloprasum Great Headed Garlic Group) ...... 3-07A Garlic, Serpent, bulb (Allium sativum var. ophioscorodon or A. sativum Ophioscorodon Group) ...... 3-07A Kurrat (Allium kurrat Schweinf. Ex. K. Krause or A. ampeloprasum Kurrat Group) ...... 3-07B Lady’s leek (Allium cernuum Roth) ...... 3-07B Leek Allium porrum L. (syn: A. ampeloprasum L. var. porrum (L.) J. Gay) (A.ampeloprasum Leek Group) ...... 3-07B Leek, wild (Allium tricoccum Aiton) ...... 3-07B Lily, bulb (Lilium spp. (Lilium Leichtlinii var. maximowiczii, Lilium lancifolium)) ...... 3-07A Onion, Beltsville bunching (Allium x proliferum (Moench) Schrad.) (syn: Allium fistulosum L. x A. cepa L.) ...... 3-07B Onion, bulb (Allium cepa L. var. cepa) (A. cepa Common Onion Group) ...... 3-07A Onion, Chinese, bulb (Allium chinense G. Don.) (syn: A. bakeri Regel) ...... 3-07A Onion, fresh (Allium fistulosum L. var. caespitosum Makino) ...... 3-07B Onion, green (Allium cepa L. var. cepa) (A. cepa Common Onion Group) ...... 3-07B Onion, macrostem (Allium macrostemom Bunge) ...... 3-07B Onion, pearl (Allium porrum var. sectivum or A. ampeloprasum Pearl Onion Group) ...... 3-07A Onion, potato, bulb (Allium cepa L. var. aggregatum G. Don.) (A. cepa Aggregatum Group) ...... 3-07A Onion, tree, tops (Allium x proliferum (Moench) Schrad. ex Willd.) (syn: A. cepa var. proliferum (Moench) Regel; A. cepa L. var. bulbiferum L.H. Bailey; A. cepa L. var. viviparum (Metz.) Alef.) ...... 3-07B Onion, Welsh, tops (Allium fistulosum L.) ...... 3-07B Shallot, bulb (Allium cepa var. aggregatum G. Don.) ...... 3-07A Shallot, fresh leaves (Allium cepa var. aggregatum G. Don.) ...... 3-07B Cultivars, varieties, and/or hybrids of these......

(iii) Table. The following Table 2 commodities for each subgroup and identifies the crop subgroups for Crop lists all the commodities included in Group 3-07, specifies the representative each subgroup.

TABLE 2—CROP GROUP 3-07: SUBGROUP LISTING

Representative commodities Commodities

Crop subgroup 3-07A. Onion, bulb, sub- Daylily, bulb; fritillaria, bulb; garlic, bulb; garlic, great-headed, bulb; garlic, serpent, group. bulb; lily, bulb; onion, bulb; onion, Chinese, bulb; onion, pearl; onion, potato, Onion, bulb...... bulb; shallot, bulb; cultivars, varieties, and/or hybrids of these. Crop subgroup 3-07B. Onion, green, sub- Chive, fresh leaves; chive, Chinese, fresh leaves; elegans hosta; fritillaria, leaves; group. kurrat; lady’s leek; leek; leek, wild; Onion, Beltsville bunching; onion, fresh; Onion, green...... onion, green; onion, macrostem; onion, tree, tops; onion, Welsh, tops; shallot, fresh leaves; cultivars, varieties, and/or hybrids of these.

(5) Crop Group 4. Leafy Vegetables (ii) Table. The following table 1 lists (Except Brassica Vegetables) Group. all the commodities included in Crop (i) Representative commodities. Celery, Group 4 and identifies the related crop head lettuce, leaf lettuce, and spinach subgroups. (Spinacia oleracea).

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TABLE 1—CROP GROUP 4: LEAFY VEGETABLES (EXCEPT BRASSICA VEGETABLES) GROUP

Related crop Commodities subgroups

Amaranth (leafy amaranth, Chinese spinach, tampala) (Amaranthus spp.) ...... 4A Arugula (Roquette) (Eruca sativa) ...... 4A Cardoon (Cynara cardunculus) ...... 4B Celery (Apium graveolens var. dulce) ...... 4B Celery, Chinese (Apium graveolens var. secalinum) ...... 4B Celtuce (Lactuca sativa var. angustana) ...... 4B Chervil (Anthriscus cerefolium) ...... 4A Chrysanthemum, edible-leaved (Chrysanthemum coronarium var. coronarium) ...... 4A Chrysanthemum, garland (Chrysanthemum coronarium var. spatiosum) ...... 4A Corn salad (Valerianella locusta) ...... 4A Cress, garden (Lepidium sativum) ...... 4A Cress, upland (yellow rocket, winter cress) (Barbarea vulgaris) ...... 4A Dandelion (Taraxacum officinale) ...... 4A Dock (sorrel) (Rumex spp.) ...... 4A Endive (escarole) (Cichorium endivia) ...... 4A Fennel, Florence (finochio) (Foeniculum vulgare Azoricum Group) ...... 4B Lettuce, head and leaf (Lactuca sativa) ...... 4A Orach (Atriplex hortensis) ...... 4A Parsley (Petroselinum crispum) ...... 4A Purslane, garden (Portulaca oleracea) ...... 4A Purslane, winter (Montia perfoliata) ...... 4A Radicchio (red chicory) (Cichorium intybus) ...... 4A Rhubarb (Rheum rhabarbarum) ...... 4B Spinach (Spinacia oleracea) ...... 4A Spinach, New Zealand (Tetragonia tetragonioides, T. expansa) ...... 4A Spinach, vine (Malabar spinach, Indian spinach) (Basella alba) ...... 4A Swiss chard (Beta vulgaris var. cicla) ...... 4B

(iii) Table. The following table 2 iden- commodities for each subgroup, and tifies the crop subgroups for Crop lists all the commodities included in Group 4, specifies the representative each subgroup.

TABLE 2—CROP GROUP 4 SUBGROUP LISTING

Representative commodities Commodities

Crop Subgroup 4A. Leafy greens subgroup. Head lettuce and leaf lettuce, and spinach Amaranth; arugula; chervil; chrysanthemum, edible-leaved; chrysanthemum, (Spinacia oleracea). garland; corn salad; cress, garden; cress, upland; dandelion; dock; endive; lettuce; orach; parsley; purslane, garden; purslane, winter; radicchio (red chicory); spinach; spinach, New Zealand; spinach, vine. Crop Subgroup 4B. Leaf petioles subgroup. Celery...... Cardoon; celery; celery, Chinese; celtuce; fennel, Florence; rhubarb; Swiss chard.

(6) Crop Group 5. Brassica (Cole) Leafy (ii) Table. The following table 1 lists Vegetables Group. all the commodities included in Crop (i) Representative commodities. Broc- Group 5 and identifies the related crop coli or cauliflower; cabbage; and mus- subgroups. tard greens.

TABLE 1—CROP GROUP 5: Brassica (COLE) LEAFY VEGETABLES

Related crop Commodities subgroups

Broccoli (Brassica oleracea var. botrytis) ...... 5A Broccoli, Chinese (gai lon) (Brassica alboglabra) ...... 5A Broccoli raab (rapini) (Brassica campestris) ...... 5B Brussels sprouts (Brassica oleracea var. gemmifera) ...... 5A Cabbage (Brassica oleracea) ...... 5A Cabbage, Chinese (bok choy) (Brassica chinensis) ...... 5B Cabbage, Chinese (napa) (Brassica pekinensis) ...... 5A Cabbage, Chinese mustard (gai choy) (Brassica campestris) ...... 5A

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TABLE 1—CROP GROUP 5: Brassica (COLE) LEAFY VEGETABLES—Continued

Related crop Commodities subgroups

Cauliflower (Brassica oleracea var. botrytis) ...... 5A Cavalo broccolo (Brassica oleracea var. botrytis) ...... 5A Collards (Brassica oleracea var. acephala) ...... 5B Kale (Brassica oleracea var. acephala) ...... 5B Kohlrabi (Brassica oleracea var. gongylodes) ...... 5A Mizuna (Brassica rapa Japonica Group) ...... 5B Mustard greens (Brassica juncea) ...... 5B Mustard spinach (Brassica rapa Perviridis Group) ...... 5B Rape greens (Brassica napus) ...... 5B

(iii) Table. The following table 2 iden- commodity(ies) for each subgroup, and tifies the crop subgroups for Crop lists all the commodities included in Group 5, specifies the representative each subgroup.

TABLE 2—CROP GROUP 5 SUBGROUP LISTING

Representative commodities Commodities

Crop Subgroup 5A. Head and stem Brassica subgroup Broccoli or cauliflower; and cabbage ...... Broccoli; broccoli, Chinese; brussels sprouts; cabbage; cabbage, Chinese (napa); cabbage, Chinese mustard; cauliflower; cavalo broccolo; kohlrabi Crop Subgroup 5B. Leafy Brassica greens subgroup. Mustard greens ...... Broccoli raab; cabbage, Chinese (bok choy); collards; kale; mizuna; mustard greens; mustard spinach; rape greens

(7) Crop Group 6. Legume Vegetables one succulent cultivar and one dried (Succulent or Dried) Group. cultivar); and soybean. (i) Representative commodities. Bean (ii) Table. The following table 1 lists (Phaseolus spp.; one succulent cultivar all the commodities included in Crop and one dried cultivar); pea (Pisum spp.; Group 6 and identifies the related crop subgroups.

TABLE 1—CROP GROUP 6: LEGUME VEGETABLES (SUCCULENT OR DRIED)

Related crop Commodities subgroups

Bean (Lupinus spp.) (includes grain lupin, sweet lupin, white lupin, and white sweet lupin) ...... 6C Bean (Phaseolus spp.) (includes field bean, kidney bean, lima bean, navy bean, pinto bean, runner bean, snap bean, tepary bean, wax bean) ...... 6A, 6B, 6C Bean (Vigna spp.) (includes adzuki bean, asparagus bean, blackeyed pea, catjang, Chinese longbean, cowpea, Crowder pea, moth bean, mung bean, rice bean, southern pea, urd bean, yardlong bean) ...... 6A, 6B, 6C Broad bean (fava bean) (Vicia faba) ...... 6B, 6C Chickpea (garbanzo bean) (Cicer arietinum) ...... 6C Guar (Cyamopsis tetragonoloba) ...... 6C Jackbean (Canavalia ensiformis) ...... 6A Lablab bean (hyacinth bean) (Lablab purpureus) ...... 6C Lentil (Lens esculenta) ...... 6C Pea (Pisum spp.) (includes dwarf pea, edible-pod pea, En glish pea, field pea, garden pea, green pea, snow pea, sugar snap pea) ...... 6A, 6B, 6C Pigeon pea (Cajanus cajan) ...... 6A, 6B, 6C Soybean (Glycine max) ...... N/A Soybean (immature seed) (Glycine max) ...... 6A Sword bean (Canavalia gladiata) ...... 6A

(iii) Table. The following table 2 iden- commodities for each subgroup, and tifies the crop subgroups for Crop lists all the commodities included in Group 6, specifies the representative each subgroup.

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TABLE 2—CROP GROUP 6 SUBGROUP LISTING

Representative commodities Commodities

Crop Subgroup 6A. Edible-podded legume vegetables subgroup. Any one succulent cultivar of edible-podded Bean (Phaseolus spp.) (includes runner bean, snap bean, wax bean); bean bean (Phaseolus spp.) and any one suc- (Vigna spp.) (includes asparagus bean, Chinese longbean, moth bean, culent cultivar of edible-podded pea (Pisum yardlong bean); jackbean; pea (Pisum spp.) (includes dwarf pea, edible-pod spp.).. pea, snow pea, sugar snap pea); pigeon pea; soybean (immature seed); sword bean. Crop Subgroup 6B. Succulent shelled pea and bean subgroup. Any succulent shelled cultivar of bean Bean (Phaseolus spp.) (includes lima bean (green)); broad bean (succulent); (Phaseolus spp.) and garden pea (Pisum bean (Vigna spp.) (includes blackeyed pea, cowpea, southern pea); pea spp.).. (Pisum spp.) (includes English pea, garden pea, green pea); pigeon pea. Crop Subgroup 6C. Dried shelled pea and bean (except soybean) subgroup Any one dried cultivar of bean (Phaseolus Dried cultivars of bean (Lupinus spp.) (includes grain lupin, sweet lupin, white spp.); and any one dried cultivar of pea lupin, and white sweet lupin); (Phaseolus spp.) (includes field bean, kidney (Pisum spp.). bean, lima bean (dry), navy bean, pinto bean; tepary bean; bean (Vigna spp.) (includes adzuki bean, blackeyed pea, catjang, cowpea, Crowder pea, moth bean, mung bean, rice bean, southern pea, urd bean); broad bean (dry); chickpea; guar; lablab bean; lentil; pea (Pisum spp.) (includes field pea); pigeon pea.

(8) Crop Group 7. Foliage of Legume (ii) Table. The following table 1 lists Vegetables Group. the commodities included in Crop (i) Representative commodities. Any Group 7. cultivar of bean (Phaseolus spp.), field pea (Pisum spp.), and soybean.

TABLE 1—CROP GROUP 7: FOLIAGE OF LEGUME VEGETABLES GROUP

Representative commodities Commodities

Any cultivar of bean (Phaseolus spp.) and field Plant parts of any legume vegetable included in the legume vegetables that will pea (Pisum spp.), and soybean (Glycine be used as animal feed. max).

(iii) Table. The following table 2 iden- modities for the subgroup, and lists all tifies the crop subgroup for Crop Group the commodities included in the sub- 7 and specifies the representative com- group.

TABLE 2—CROP GROUP 7 SUBGROUP LISTING

Representative commodities Commodities

Crop Subgroup 7A. Foliage of legume vegetables (except soybeans) subgroup Any cultivar of bean (Phaseolus spp.), and Plant parts of any legume vegetable (except soybeans) included in the legume field pea (Pisum spp.). vegetables group that will be used as animal feed.

(9) Crop Group 8. Fruiting Vegetables CROP GROUP 8: FRUITING VEGETABLES Group. (EXCEPT CUCURBITS)—COMMODITIES (i) Representative commodities. To- Eggplant (Solanum melongena) mato, bell pepper, and one cultivar of Groundcherry (Physalis spp.) non-bell pepper. Pepino (Solanum muricatum) (ii) Commodities. The following is a Pepper (Capsicum spp.) (includes bell pepper, list of all the commodities included in chili pepper, cooking pepper, pimento, Crop Group 8: sweet pepper) Tomatillo (Physalis ixocarpa) Tomato (Lycopersicon esculentum)

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(10) Crop Group 8–10. Fruiting Vege- small tomato; bell pepper and one table Group. cultivar of small nonbell pepper. (i) Representative commodities. To- (ii) Commodities. The following is a mato, standard size, and one cultivar of list of all commodities included in the Crop group 8–10.

TABLE 1—CROP GROUP 8–10: FRUITING VEGETABLE GROUP

Related crop sub- Commodities groups

African eggplant, Solanum macrocarpon L ...... 8–10B, 8–10C Bush tomato, Solanum centrale J.M. Black ...... 8–10A Cocona, Solanum sessiliflorum Dunal ...... 8–10A Currant tomato, Lycopersicon pimpinellifolium L ...... 8–10A Eggplant, Solanum melongena L ...... 8–10B, 8–10C Garden huckleberry, Solanum scabrum Mill ...... 8–10A Goji berry, Lycium barbarum L ...... 8–10A Groundcherry, Physalis alkekengi L., P. grisea (Waterf.) M. Martinez, P. peruviana L., P. pubescens L .. 8–10A Martynia, Proboscidea louisianica (Mill.) Thell ...... 8–10B, 8–10C Naranjilla, Solanum quitoense Lam ...... 8–10A Okra, Abelmoschus esculentus (L.) Moench ...... 8–10B, 8–10C Pea eggplant, Solanum torvum Sw...... 8–10B, 8–10C Pepino, Solanum muricatum Aiton ...... 8–10B, 8–10C Pepper, bell, Capsicum annuum L. var. annuum, Capsicum spp ...... 8–10B Pepper, nonbell, Capsicum chinese Jacq., C. annuum L. var. annuum, C. frutescens L., C. baccatum L., 8–10B, 8–10C C. pubescens Ruiz & Pav., Capsicum spp. Roselle, Hibiscus sabdariffa L ...... 8–10B, 8–10C Scarlet eggplant, Solanum aethiopicum L ...... 8–10B, 8–10C Sunberry, Solanum retroflexum Dunal ...... 8–10A Tomatillo, Physalis philadelphica Lam ...... 8–10A Tomato, Solanum lycopersicum L., Solanum lycopersicum L. var. lycopersicum ...... 8–10A Tree tomato, Solanum betaceum Cav ...... 8–10A Cultivars, varieties and/or hybrids of these ......

(iii) Table. The following Table 2 commodities for each subgroup and identifies the crop subgroups for Crop lists all the commodities included in Group 8–10, specifies the representative each subgroup.

TABLE 2—CROP GROUP 8–10. SUBGROUP LISTING

Representative commodities Commodities

Crop subgroup 8–10A. Tomato subgroup Tomato, standard size, and one cultivar of small tomato ...... Bush tomato; cocona; currant tomato; garden huckleberry; goji berry; groundcherry; naranjilla; sunberry; tomatillo; tomato; tree tomato; cultivars, varieties, and/or hybrids of these. Crop subgroup 8–10B. Pepper/Eggplant subgroup Bell pepper and one cultivar of small nonbell pepper ...... African eggplant; bell pepper; eggplant; Martynia; nonbell pepper; okra; pea eggplant; pepino; roselle; scarlet eggplant; cultivars, varieties, and/or hybrids of these. Crop subgroup 8–10C. Nonbell pepper/Eggplant subgroup One cultivar of small nonbell pepper or one cultivar of small African eggplant; eggplant; martynia; nonbell pepper; okra; pea eggplant. eggplant; pepino; roselle; scarlet eggplant; cultivars, varieties, and/or hybrids of these.

(11) Crop Group 9. Cucurbit Vegeta- (ii) Table. The following table 1 lists bles Group. all the commodities included in Crop (i) Representative commodities. Cucum- Group 9 and identifies the related sub- ber, muskmelon, and summer squash. groups.

TABLE 1—CROP GROUP 9: CUCURBIT VEGETABLES

Related crop Commodities subgroups

Chayote (fruit) (Sechium edule) ...... 9B

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TABLE 1—CROP GROUP 9: CUCURBIT VEGETABLES—Continued

Related crop Commodities subgroups

Chinese waxgourd (Chinese preserving melon) (Benincasa hispida) ...... 9B Citron melon (Citrullus lanatus var. citroides) ...... 9A Cucumber (Cucumis sativus) ...... 9B Gherkin (Cucumis anguria) ...... 9B Gourd, edible (Lagenaria spp.) (includes hyotan, cucuzza); (Luffa acutangula, L. cylindrica) (includes hechima, Chinese okra) ...... 9B Momordica spp. (includes balsam apple, balsam pear, bitter melon, Chinese cucumber) ...... 9B Muskmelon (hybrids and/or cultivars of Cucumis melo) (includes true cantaloupe, cantaloupe, casaba, crenshaw melon, golden pershaw melon, honeydew melon, honey balls, mango melon, Persian melon, pineapple melon, Santa Claus melon, and snake melon) ...... 9A Pumpkin (Cucurbita spp.) ...... 9B Squash, summer (Cucurbita pepo var. melopepo) (includes crookneck squash, scallop squash, straightneck squash, vegetable marrow, zucchini) ...... 9B Squash, winter (Cucurbita maxima; C. moschata) (includes butternut squash, calabaza, hubbard squash); (C. mixta; C. pepo) (includes acorn squash, spaghetti squash) ...... 9B Watermelon (includes hybrids and/or varieties of Citrullus lanatus) ...... 9A

(iii) Table. The following table 2 iden- commodities for each subgroup, and tifies the crop subgroups for Crop lists all the commodities included in Group 9, specifies the representative each subgroup.

TABLE 2—CROP GROUP 9 SUBGROUP LISTING

Representative commodities Commodities

Crop Subgroup 9A. Melon subgroup Cantaloupes ...... Citron melon; muskmelon; watermelon Crop Subgroup 9B. Squash/cucumber subgroup One cultivar of summer squash and cucumber. Chayote (fruit); Chinese waxgourd; cucumber; gherkin; gourd, edible; Momordica spp.; pumpkin; squash, summer; squash, winter.

(12) Crop Group 10. Citrus Fruit Lemon (Citrus jambhiri, Citrus limon) Group. Lime (Citrus aurantiifolia) (i) Representative commodities. Sweet Mandarin (tangerine) (Citrus reticulata) orange; lemon and grapefruit. Orange, sour (Citrus aurantium) (ii) Commodities. The following is a Orange, sweet (Citrus sinensis) list of all the commodities in Crop Pummelo (Citrus grandis, Citrus maxima) Group 10: Satsuma mandarin (Citrus unshiu) (13) Crop Group 10–10. Citrus Fruit CROP GROUP 10: CITRUS FRUITS (CITRUS SPP., Group. FORTUNELLA SPP.) GROUP—COMMODITIES (i) Representative commodities. Orange Calamondin (Citrus mitis×Citrofortunella mitis) or Tangerine/Mandarin, Lemon or Citrus citron (Citrus medica) Citrus hybrids (Citrus spp.) (includes Lime, and Grapefruit. chironja, tangelo, tangor) (ii) Commodities. The following is a Grapefruit (Citrus paradisi) list of all the commodities in Crop Kumquat (Fortunella spp.) Group 10–10.

TABLE 1—CROP GROUP 10–10: CITRUS FRUIT GROUP

Related crop sub- Commodities groups

Australian desert lime, Eremocitrus glauca (Lindl.) Swingle ...... 10–10B Australian finger lime, Microcitrus australasica (F. Muell.) Swingle ...... 10–10B Australian round lime, Microcitrus australis (A. Cunn. Ex Mudie) Swingle ...... 10–10B Brown River finger lime, Microcitrus papuana Winters ...... 10–10B Calamondin, Citrofortunella microcarpa (Bunge) Wijnands ...... 10–10A Citron, Citrus medica L ...... 10–10A Citrus hybrids, Citrus spp. Eremocitrus spp., Fortunella spp., Microcitrus spp., and Poncirus spp ...... 10–10A Grapefruit, Citrus paradisi Macfad ...... 10–10C

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TABLE 1—CROP GROUP 10–10: CITRUS FRUIT GROUP—Continued

Related crop sub- Commodities groups

Japanese summer grapefruit, Citrus natsudaidai Hayata ...... 10–10C Kumquat, Fortunella spp ...... 10–10B Lemon, Citrus limon (L.) Burm. f ...... 10–10B Lime, Citrus aurantiifolia (Christm.) Swingle ...... 10–10B Mediterranean mandarin, Citrus deliciosa Ten ...... 10–10A Mount White lime, Microcitrus garrowayae (F.M. Bailey) Swingle ...... 10–10B New Guinea wild lime, Microcitrus warburgiana (F.M. Bailey) Tanaka ...... 10–10B Orange, sour, Citrus aurantium L ...... 10–10A Orange, sweet, Citrus sinensis (L.) Osbeck ...... 10–10A Pummelo, Citrus maxima (Burm.) Merr ...... 10–10C Russell River lime, Microcitrus inodora (F.M. Bailey) Swingle ...... 10–10B Satsuma mandarin, Citrus unshiu Marcow ...... 10–10A Sweet lime, Citrus limetta Risso ...... 10–10B Tachibana orange, Citrus tachibana (Makino) Tanaka ...... 10–10A Tahiti lime, Citrus latifolia (Yu. Tanaka) Tanaka ...... 10–10B Tangelo, Citrus xtangelo J.W. Ingram & H.E. Moore ...... 10–10A, 10–10C Tangerine (Mandarin), Citrus reticulata Blanco ...... 10–10A Tangor, Citrus nobilis Lour ...... 10–10A Trifoliate orange, Poncirus trifoliata (L.) Raf ...... 10–10A Uniq fruit, Citrus aurantium Tangelo group ...... 10–10C Cultivars, varieties and/or hybrids of these.

(iii) Table. The following Table 2 tive commodities for each subgroup identifies the crop subgroups for Crop and lists all the commodities included Group 10–10, specifies the representa- in each subgroup.

TABLE 2—CROP GROUP 10–10: SUBGROUP LISTING

Representative commodities Commodities

Crop Subgroup 10–10A. Orange subgroup Orange or tangerine/mandarin ...... Calamondin; citron; citrus hybrids; mediterranean mandarin; orange, sour; orange, sweet; satsuma mandarin; tachibana orange; tangerine (mandarin); tangelo; tangor; trifoliate orange; cultivars, varieties, and/or hybrids of these. Crop Subgroup 10–10B. Lemon/Lime subgroup Lemon or lime ...... Australian desert lime; Australian finger lime; Australian round lime; brown river finger lime; kumquat; lemon; lime; mount white lime; New Guinea wild lime; Russell River lime; sweet lime; Tahiti lime; cultivars , varieties, and/or hybrids of these. Crop Subgroup 10–10C. Grapefruit subgroup Grapefruit ...... Grapefruit; Japanese summer grapefruit; pummelo; tangelo; uniq fruit; cultivars, varieties, and/or hybrids of these.

(14) Crop Group 11: Pome Fruits Quince (Cydonia oblonga) Group. (15) Crop group 11–10. Pome Fruit (i) Representative commodities. Apple Group. and pear. (i) Representative commodities. Apple (ii) Commodities. The following is a and Pear list of all the commodities included in (ii) Commodities. The following is a Crop Group 11: list of all the commodities in Crop CROP GROUP 11: POME FRUITS GROUP— Group 11–10. COMMODITIES CROP GROUP 11–10: POME FRUIT GROUP— Apple (Malus domestica) COMMODITIES Crabapple (Malus spp.) Loquat (Eriobotrya japonica) Apple, Malus domestica Borkh. Mayhaw (Crataegus aestivalis, C. opaca, and C. Azarole, Crataegus azarolus L. rufula) Crabapple, Malus sylvestris (L.) Mill., M. Pear (Pyrus communis) prunifolia (Willd.) Borkh. Pear, oriental (Pyrus pyrifolia) Loquat, Eriobotrya japonica (Thunb.) Lindl.

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Mayhaw, Crataegus aestivalis (Walter) Torr. & CROP GROUP 12: STONE FRUITS GROUP— A. Gray, C. opaca COMMODITIES Hook. & Arn., and C. rufula Sarg. Medlar, Mespilus germanica L. Apricot (Prunus armeniaca) Pear, Pyrus communis L. Cherry, sweet (Prunus avium), Pear, Asian, Pyrus pyrifolia (Burm. f.) Nakai Cherry, tart (Prunus cerasus) var. culta (Makino) Nakai Nectarine (Prunus persica) Pseudocydonia sinensis (Thouin) C.K. Schneid. Peach (Prunus persica) Quince, Cydonia oblonga Mill. Plum (Prunus domestica, Prunus spp.) Quince, Chinese, Chaenomeles speciosa Plum, Chickasaw (Prunus angustifolia) (Sweet) Nakai, Plum, Damson (Prunus domestica spp. Quince, Japanese, Chaenomeles japonica insititia) (Thunb.) Lindl. ex Spach Tejocote, Crataegus mexicana DC. Plum, Japanese (Prunus salicina) Cultivars, varieties and/or hybrids of these. Plumcot (Prunus. armeniaca×P. domestica) Prune (fresh) (Prunus domestica, Prunus spp.) (16) Crop Group 12. Stone Fruits Group. (17) Crop Group 12–12: Stone Fruit (i) Representative commodities. Sweet Group. cherry or tart cherry; peach; and plum (i) Representative commodities. Sweet or fresh prune (Prunus domestica, cherry or Tart cherry; Peach; and Prunus spp.) Plum or Prune plum. (ii) Commodities. The following is a (ii) Commodities. The following Table list of all the commodities included in 1 is a list of all commodities included Crop Group 12: in Crop Group 12–12.

TABLE 1—CROP GROUP 12–12: STONE FRUIT GROUP

Related crop Commodities subgroup

Apricot (Prunus armeniaca L.) ...... 12–12C Apricot, Japanese (Prunus mume Siebold & Zucc.) ...... 12–12C Capulin (Prunus serotina Ehrh. var. salicifolia (Kunth) Koehne) ...... 12–12A Cherry, black (Prunus serotina Ehrh.) ...... 12–12A Cherry, Nanking (Prunus tomentosa Thunb.) ...... 12–12A Cherry, sweet (Prunus avium (L.) L.) ...... 12–12A Cherry, tart (Prunus cerasus L.) ...... 12–12A Jujube, Chinese (Ziziphus jujuba Mill.) ...... 12–12C Nectarine (Prunuspersica (L.) Batsch var. nucipersica (Suckow) C.K. Schneid) ...... 12–12B Peach (Prunus persica (L.) Batsch var. persica) ...... 12–12B Plum (Prunus domestica L. subsp. domestica) ...... 12–12C Plum, American (Prunus americana Marshall) ...... 12–12C Plum, beach (Prunus maritima Marshall) ...... 12–12C Plum, Canada (Prunus nigra Aiton) ...... 12–12C Plum, cherry (Prunus cerasifera Ehrh.) ...... 12–12C Plum, Chickasaw (Prunus angustifolia Marshall) ...... 12–12C Plum, Damson (Prunus domestica L. subsp. insititia (L.) C.K. Schneid.) ...... 12–12C Plum, Japanese (Prunus salicina Lindl.; P. salicina Lindl. var. salicina) ...... 12–12C Plum, Klamath (Prunus subcordata Benth.) ...... 12–12C Plum, prune (Prunus domestica L. subsp. domestica) ...... 12–12C Plumcot (Prunus hybr.) ...... 12–12C Sloe (Prunus spinosa L.) ...... 12–12C Cultivars, varieties, and/or hybrids of these.

(iii) Crop subgroups. The following resentative commodities for each sub- Table 2 identifies the crop subgroups group, and lists all the commodities in- for Crop Group 12–12, specifies the rep- cluded in each subgroup.

TABLE 2—CROP GROUP 12–12: SUBGROUP LISTING

Representative commodities Commodities

Crop subgroup 12–12A. Cherry subgroup

Cherry, sweet or Cherry, tart .... Capulin; Cherry, black; Cherry, Nanking; Cherry, sweet; Cherry, tart; cultivars, varieties, and/or hybrids of these.

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TABLE 2—CROP GROUP 12–12: SUBGROUP LISTING—Continued

Representative commodities Commodities

Crop subgroup 12–12B. Peach subgroup

Peach ...... Peach; Nectarine; cultivars, varieties, and/or hybrids of these.

Crop subgroup 12–12C. Plum subgroup

Plum or Prune plum ...... Apricot; Apricot, Japanese; Jujube, Chinese; Plum; Plum, American; Plum, beach; Plum, Can- ada; Plum, cherry; Plum, Chickasaw; Plum, Damson; Plum, Japanese; Plum, Klamath; Plumcot; Plum, prune; Sloe; cultivars, varieties, and/or hybrids of these.

(18) Crop Group 13. Berries Group. (ii) Table. The following table 1 lists (i) Representative commodities. Any all the commodities included in Crop one blackberry or any one raspberry; Group 13 and identifies the related sub- and blueberry. groups.

TABLE 1—CROP GROUP 13: BERRIES GROUP

Related crop Commodities subgroups

Blackberry (Rubus eubatus) (including bingleberry, black satin berry, boysenberry, Cherokee blackberry, Chesterberry, Cheyenne blackberry, coryberry, darrowberry, dewberry, Dirksen thornless berry, Himalayaberry, hullberry, Lavacaberry, lowberry, Lucretiaberry, mammoth blackberry, marionberry, nectarberry, olallieberry, Oregon evergreen berry, phenomenalberry, rangeberry, ravenberry, rossberry, Shawnee blackberry, youngberry, and varieties and/or hybrids of these) ...... 13A Blueberry (Vaccinium spp.) ...... 13B Currant (Ribes spp.) ...... 13B Elderberry (Sambucus spp.) ...... 13B Gooseberry (Ribes spp.) ...... 13B Huckleberry (Gaylussacia spp.) ...... 13B Loganberry (Rubus loganobaccus) ...... 13A Raspberry, black and red (Rubus occidentalis, Rubus strigosus, Rubus idaeus) ...... 13A

(iii) Table. The following table 2 iden- commodities for each subgroup, and tifies the crop subgroups for Crop lists all the commodities included in Group 13, specifies the representative each subgroup.

TABLE 2—CROP GROUP 13 SUBGROUPS LISTING

Representative commodities Commodities

Crop Subgroup 13A. Caneberry (blackberry and raspberry) subgroup. Any one blackberry or any one raspberry...... Blackberry; loganberry; red and black raspberry; cultivars and/or hybrids of these. Crop Subgroup 13B. Bushberry subgroup.. Blueberry, highbush...... Blueberry, highbush and lowbush; currant; elderberry; gooseberry; huckleberry.

(19) Crop Group 13-07. Berry and Small berry; grape; fuzzy kiwifruit, and Fruit Crop Group strawberry. (i) Representative commodities. Any (ii) Table. The following Table 1 lists one blackberry or any one raspberry; all the commodities listed in Crop highbush blueberry; elderberry or mul- Group 13-07 and identifies the related crop subgroups.

TABLE 1—CROP GROUP 13-07: BERRY AND SMALL FRUIT CROP GROUP

Commodities Related crop subgroups

Amur river grape (Vitis amurensis Rupr) ...... 13-07D, 13-07E, 13-07F Aronia berry (Aronia spp.) ...... 13-07B Bayberry (Myrica spp.) ...... 13-07C

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TABLE 1—CROP GROUP 13-07: BERRY AND SMALL FRUIT CROP GROUP—Continued

Commodities Related crop subgroups

Bearberry (Arctostaphylos uva-ursi) ...... 13-07G, 13-07H Bilberry (Vaccinium myrtillus L.) ...... 13-07G, 13-07H Blackberry (Rubus spp.) (including Andean blackberry, arctic blackberry, bingleberry, black satin berry, boysenberry, brombeere, California blackberry, Chesterberry, Cherokee blackberry, Chey- enne blackberry, common blackberry, coryberry, darrowberry, dewberry, Dirksen thornless berry, evergreen blackberry, Himalayaberry, hullberry, lavacaberry, loganberry, lowberry, Lucretiaberry, mammoth blackberry, marionberry, mora, mures deronce, nectarberry, Northern dewberry, olallieberry, Oregon evergreen berry, phenomenalberry, rangeberry, ravenberry, rossberry, Shaw- nee blackberry, Southern dewberry, tayberry, youngberry, zarzamora, and cultivars, varieties and/or hybrids of these.) ...... 13-07A Blueberry, highbush (Vaccinium spp.) ...... 13-07B Blueberry, lowbush (Vaccinium angustifolium Aiton) ...... 13-07B Buffalo currant (Ribes aureum Pursh) ...... 13-07B Buffaloberry (Shepherdia argentea (Pursh) Nutt.) ...... 13-07C Che (Cudrania tricuspidata Bur. Ex Lavallee) ...... 13-07C Chilean guava (Myrtus ugni Mol.) ...... 13-07B Chokecherry (Prunus virginiana L.) ...... 13-07C Cloudberry (Rubus chamaemorus L.) ...... 13-07G, 13-07H Cranberry (Vaccinium macrocarpon Aiton) ...... 13-07G, 13-07H Currant, black (Ribes nigrum L.) ...... 13-07B Currant, red (Ribes rubrum L.) ...... 13-07B Elderberry (Sambucus spp.) ...... 13-07B, 13-07C European barberry (Berberis vulgaris L.) ...... 13-07B Gooseberry (Ribes spp.) ...... 13-07B, 13-07D, 13- 07E, 13-07F Grape (Vitis spp.) ...... 13-07D, 13-07F Highbush cranberry (Viburnum opulus L. var. Americanum Aiton) ...... 13-07B Honeysuckle, edible (Lonicera caerula L. var. emphyllocalyx Nakai, Lonicera caerula L var . edulis Turcz. ex herder) ...... 13-07B Huckleberry (Gaylussacia spp.) ...... 13-07B Jostaberry (Ribes x nidigrolaria Rud. Bauer and A. Bauer) ...... 13-07B Juneberry (Saskatoon berry) (Amelanchier spp.) ...... 13-07B, 13-07C Kiwifruit, fuzzy (Actinidia deliciosa A. Chev.) (C.F. Liang and A.R. Fergusons, Actinida chinensis Planch.) ...... 13-07D, 13-07E Kiwifruit, hardy (Actinidia arguta (Siebold and Zucc.) Planch. ex Miq) ...... 13-07D, 13-07E, 13-07F Lingonberry (Vaccinium vitis-idaea L.) ...... 13-07B, 13-07G 13-07H Maypop (Passiflora incarnata L.) ...... 13-07E, 13-07F Mountain pepper berries (Tasmannia lanceolata)(Poir.) A.C.Sm...... 13-07C Mulberry (Morus spp.) ...... 13-07C Muntries (Kunzea pomifera F. Muell.) ...... 13-07G, 13-07H Native currant (Acrotriche depressa R. BR.) ...... 13-07B Partridgeberry (Mitchella repens L.) ...... 13-07G, 13-07H Phalsa (Grewia subinaequalis DC.) ...... 13-07C Pincherry (Prunus pensylvanica L.f.) ...... 13-07C Raspberry, black and red (Rubus spp.) ...... 13-07A Riberry (Syzygium luehmannii) ...... 13-07C Salal (Gaultheria shallon Pursh.) ...... 13-07B, 13-07C Schisandra berry (Schisandra chinensis (Turcz.) Baill.) ...... 13-07D, 13-07E, 13-07F Sea buckthorn (Hippophae rhamnoides L.) ...... 13-07B Serviceberry (Sorbus spp.) ...... 13-07C Strawberry (Fragaria x ananassa Duchesne) ...... 13-07G Wild raspberry (Rubus muelleri Lefevre ex P.J. Mull) ...... 13-07A Cultivars, varieties, and/or hybrids of these......

(iii) Table. The following Table 2 tive commodities for each subgroup identifies the crop subgroups for Crop and lists all the commodities included Group 13-07, specifies the representa- in each subgroup.

TABLE 2—CROP GROUP 13-07: SUBGROUP LISTING

Representative commodities Commodities

Crop Subgroup 13-07A. Caneberry subgroup Any one blackberry or any one rasp- Blackberry; loganberry; raspberry, red and black; wild raspberry; cultivars, vari- berry.. eties, and/or hybrids of these. Crop Subgroup 13-07B. Bushberry subgroup.

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TABLE 2—CROP GROUP 13-07: SUBGROUP LISTING—Continued

Representative commodities Commodities

Blueberry, highbush...... Aronia berry; blueberry, highbush; blueberry, lowbush; buffalo currant; Chilean guava; currant, black; currant, red; elderberry; European, barberry; gooseberry; cranberry, highbush; honeysuckle, edible; huckleberry; jostaberry; Juneberry; lingonberry; native currant; salal; sea buckthorn; cultivars, varieties, and/or hybrids of these. Crop Subgroup 13-07C. Large shrub/tree berry subgroup. Elderberry or mulberry...... Bayberry; buffaloberry; che; chokecherry; elderberry; Juneberry; mountain pepper berries; mulberry; phalsa; pincherry; riberry; salal; serviceberry; cultivars, varieties, and/or hybrids of these. Crop Subgroup 13-07D. Small fruit vine climbing subgroup. Grape and fuzzy kiwifruit...... Amur river grape; gooseberry; grape; kiwifruit, fuzzy; kiwifruit, hardy; Maypop; schisandra berry; cultivars, varieties, and /or hybrids of these. Crop Subgroup 13-07E. Small fruit vine climbing subgroup, except grape. Fuzzy kiwifruit...... Amur river grape; gooseberry; kiwifruit, fuzzy; kiwifruit, hardy; Maypop; schisandra berry; cultivars, varieties, and/or hybrids of these. Crop Subgroup 13-07F. Small fruit vine climbing subgroup except fuzzy kiwifruit. Grape...... Amur river grape; gooseberry; grape; kiwifruit, hardy; Maypop; schisandra berry; cultivars varieties, and/or hybrids of these. Crop Subgroup 13-07G. Low growing berry subgroup. Strawberry...... Bearberry; bilberry; blueberry, lowbush; cloudberry; cranberry; lingonberry; muntries; partridgeberry; strawberry; cultivars, varieties, and/or hybrids of these. Crop Subgroup 13-07H. Low growing berry subgroup, except strawberry. Cranberry ...... Bearberry; bilberry; blueberry, lowbush; cloudberry; cranberry; lingonberry; muntries; partridgeberry; cultivars, varieties, and/or cultivars of these.

(20) Crop Group 14. Tree Nuts Group. CROP GROUP 14–12: TREE NUT GROUP (i) Representative commodities. Almond African nut-tree (Ricinodendron heudelotii and pecan. (Baill.) Heckel) (ii) Commodities. The following is a Almond (Prunus dulcis (Mill.) D.A. Webb) list of all the commodities included in Beechnut (Fagus grandifolia Ehrh.; F. Crop Group 14: sylvatica L.) Brazil nut (Bertholletia excelsa Humb. & CROP GROUP 14: TREE NUTS—COMMODITIES Bonpl.) Brazilian pine (Araucaria angustifolia Almond (Prunus dulcis) (Bertol.) Kuntze) Beech nut (Fagus spp.) Bunya (Araucaria bidwillii Hook.) Brazil nut (Bertholletia excelsa) Bur oak (Quercus macrocarpa Michx.) Butternut (Juglans cinerea) Butternut (Juglans cinerea L.) Cashew (Anacardium occidentale) Cajou nut (Anacardium giganteum Hance ex Chestnut (Castanea spp.) Engl.) Chinquapin (Castanea pumila) Candlenut (Aleurites moluccanus (L.) Willd.) Cashew (Anacardium occidentale L.) Filbert (hazelnut) (Corylus spp.) Chestnut (Castanea crenata Siebold & Zucc.; Hickory nut (Carya spp.) C. dentata (Marshall) Borkh.; C. mollissima Macadamia nut (bush nut) (Macadamia spp.) Blume; C. sativa Mill.) Pecan (Carya illinoensis) Chinquapin (Castaneapumila (L.) Mill.) Walnut, black and English (Persian) (Juglans Coconut (Cocos nucifera L.) spp.) Coquito nut (Jubaea chilensis (Molina) Baill.) Dika nut (Irvingia gabonensis (Aubry- (21) Crop Group 14–12. Tree Nut Group. Lecomte ex O’Rorke) Baill.) (i) Representative commodities. Almond Ginkgo (Ginkgo biloba L.) and Pecan. Guiana chestnut (Pachira aquatica Aubl.) (ii) Commodities. The following is a Hazelnut (Filbert) (Corylus americana Mar- list of all commodities included in Crop shall; C. avellana L.; C. californica (A. DC.) Group 14–12. Rose; C. chinensis Franch.) Heartnut (Juglans ailantifolia Carrie`re var. cordiformis (Makino) Rehder)

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Hickory nut (Carya cathayensis Sarg.; C. (i) Representative commodities. Corn, glabra (Mill.) Sweet; C. laciniosa (F. Michx.) wheat, and any other cereal grain crop. W. P. C. Barton; C. myristiciformis (F. (ii) Commodities. The commodities in- Michx.) Elliott; C. ovata (Mill.) K. Koch; C. cluded in Crop Group 16 are: Forage, tomentosa (Lam.) Nutt.) Japanese horse-chestnut (Aesculus turbinate fodder, and straw of all commodities Blume) included in the group cereal grains Macadamia nut (Macadamia integrifolia Maid- group. en & Betche; M. tetraphylla L.A.S. John- (24) Crop Group 17. Grass Forage, Fod- son) der, and Hay Group. Mongongo nut (Schinziophyton rautanenii (i) Representative commodities. Ber- (Schinz) Radcl.-Sm.) muda grass; bluegrass; and bromegrass Monkey-pot (Lecythis pisonis Cambess.) or fescue. Monkey puzzle nut (Araucaria araucana (Molina) K. Koch) (ii) Commodities. The commodities in- Okari nut (Terminalia kaernbachii Warb.) cluded in Crop Group 17 are: Any grass, Pachira nut (Pachira insignis (Sw.) Savigny) Gramineae family (either green or Peach palm nut (Bactris gasipaes Kunth var. cured) except sugarcane and those in- gasipaes) cluded in the cereal grains group, that Pecan (Carya illinoinensis (Wangenh.) K. will be fed to or grazed by livestock, all Koch) pasture and range grasses and grasses Pequi (Caryocar brasiliense Cambess.; C. villosum (Aubl.) Pers; C. nuciferum L.) grown for hay or silage. Pili nut (Canarium ovatum Engl.; C. vulgare (25) Crop Group 18. Nongrass Animal Leenh.) Feeds (Forage, Fodder, Straw, and Pine nut (Pinus edulis Engelm.; P. koraiensis Hay) Group. Siebold & Zucc.; P. sibirica Du Tour; P. (i) Representative commodities. Alfalfa pumila (Pall.) Regel; P. gerardiana Wall. ex and clover (Trifolium spp.) D. Don; P. monophylla Torr. & Fre´m.; P. (ii) Commodities. The following is a quadrifolia Parl. ex Sudw.; P. pinea L.) list of all the commodities included in Pistachio (Pistacia vera L.) Sapucaia nut (Lecythis zabucaja Aubl.) Crop Group 18: Tropical almond (Terminalia catappa L.) CROP GROUP 18: NONGRASS ANIMAL FEEDS Walnut, black (Juglans nigra L.; J. hindsii (FORAGE, FODDER, STRAW, AND HAY) Jeps. ex R. E. Sm.; J. microcarpa Berland.) GROUP—COMMODITIES Walnut, English (Juglans regia L.) Yellowhorn (Xanthoceras sorbifolium Bunge) Alfalfa (Medicago sativa subsp. sativa) Cultivars, varieties, and/or hybrids of these Bean, velvet (Mucuna pruriens var. utilis) (22) Crop Group 15. Cereal Grains Clover (Trifolium spp., Melilotus spp.) Group. Kudzu (Pueraria lobata) Lespedeza (Lespedeza spp.) (i) Representative commodities. Corn Lupin (Lupinus spp.) (fresh sweet corn and dried field corn), Sainfoin (Onobrychis viciifolia); rice, sorghum, and wheat. Trefoil (Lotus spp.) (ii) Commodities. The following is a Vetch (Vicia spp.) list of all the commodities included in Vetch, crown (Coronilla varia) Crop Group 15: Vetch, milk (Astragalus spp). (26) Crop Group 19. Herbs and Spices CROP GROUP 15: CEREAL GRAINS— COMMODITIES Group. (i) Representative commodities. Basil Barley (Hordeum spp.) (fresh and dried); black pepper; chive; Buckwheat (Fagopyrum esculentum) and celery seed or dill seed. Corn (Zea mays) Millet, pearl (Pennisetum glaucum) (ii) Table. The following table 1 lists Millet, proso (Panicum milliaceum) all the commodities included in Crop Oats (Avena spp.) Group 19 and identifies the related sub- Popcorn (Zea mays var. everta) groups. Rice (Oryza sativa) Rye (Secale cereale) TABLE 1—CROP GROUP 19: HERBS AND SPICES Sorghum (milo) (Sorghum spp.) GROUP Teosinte (Euchlaena mexicana) Triticale (Triticum-Secale hybrids) Related Wheat (Triticum spp.) crop Commodities sub- Wild rice (Zizania aquatica) groups

(23) Crop Group 16. Forage, Fodder Allspice (Pimenta dioica) ...... 19B and Straw of Cereal Grains Group. Angelica (Angelica archangelica) ...... 19A

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TABLE 1—CROP GROUP 19: HERBS AND SPICES TABLE 1—CROP GROUP 19: HERBS AND SPICES GROUP—Continued GROUP—Continued

Related Related Commodities crop crop sub- Commodities subgroups groups

Anise (anise seed) (Pimpinella anisum) ...... 19B Lavender (Lavandula officinalis) ...... 19A Anise, star (Illicium verum) ...... 19B Lemongrass (Cymbopogon citratus) ...... 19A Annatto (seed) ...... 19B Lovage (leaf) (Levisticum officinale) ...... 19A Balm (lemon balm) (Melissa officinalis) ...... 19A Lovage (seed) (Levisticum officinale) ...... 19B Basil (Ocimum basilicum) ...... 19A Mace (Myristica fragrans) ...... 19B Borage (Borago officinalis) ...... 19A Marigold (Calendula officinalis) ...... 19A Burnet (Sanguisorba minor) ...... 19A Marjoram (Origanum spp.) (includes sweet or an- Camomile (Anthemis nobilis) ...... 19A nual marjoram, wild marjoram or oregano, and Caper buds (Capparis spinosa) ...... 19B pot marjoram) ...... 19A Caraway (Carum carvi) ...... 19B Mustard (seed) (Brassica juncea, B. hirta, B. nigra) 19B Caraway, black (Nigella sativa) ...... 19B Nasturtium (Tropaeolum majus) ...... 19A Cardamom (Elettaria cardamomum) ...... 19B Nutmeg (Myristica fragrans) ...... 19B Cassia bark (Cinnamomum aromaticum) ...... 19B Parsley (dried) (Petroselinum crispum) ...... 19A Cassia buds (Cinnamomum aromaticum) ...... 19B Catnip (Nepeta cataria) ...... 19A Pennyroyal (Mentha pulegium) ...... 19A Celery seed (Apicum graveolens) ...... 19B Pepper, black (Piper nigrum) ...... 19B Chervil (dried) (Anthriscus cerefolium) ...... 19A Pepper, white ...... 19B Chive (Allium schoenoprasum) ...... 19A Poppy (seed) (Papaver somniferum) ...... 19B Chive, Chinese (Allium tuberosum) ...... 19A Rosemary (Rosemarinus officinalis) ...... 19A Cinnamon (Cinnamomum verum) ...... 19B Rue (Ruta graveolens) ...... 19A Clary (Salvia sclarea) ...... 19A Saffron (Crocus sativus) ...... 19B Clove buds (Eugenia caryophyllata) ...... 19B Sage (Salvia officinalis) ...... 19A Coriander (cilantro or Chinese parsley) (leaf) Savory, summer and winter (Satureja spp.) ...... 19A (Coriandrum sativum) ...... 19A Sweet bay (bay leaf) (Laurus nobilis) ...... 19A Coriander (cilantro) (seed) (Coriandrum sativum) ... 19B Tansy (Tanacetum vulgare) ...... 19A Costmary (Chrysanthemum balsamita) ...... 19A Tarragon (Artemisia dracunculus) ...... 19A Culantro (leaf) (Eryngium foetidum) ...... 19A Thyme (Thymus spp.) ...... 19A Culantro (seed) (Eryngium foetidum) ...... 19B Vanilla (Vanilla planifolia) ...... 19B Cumin (Cuminum cyminum) ...... 19B Wintergreen (Gaultheria procumbens) ...... 19A Curry (leaf) (Murraya koenigii) ...... 19A Woodruff (Galium odorata) ...... 19A Dill (dillweed) (Anethum graveolens) ...... 19A Wormwood (Artemisia absinthium) ...... 19A Dill (seed) (Anethum graveolens) ...... 19B Fennel (common) (Foeniculum vulgare) ...... 19B (iii) Table. The following table 2 iden- Fennel, Florence (seed) (Foeniculum vulgare Azoricum Group) ...... 19B tifies the crop subgroups for Crop Fenugreek (Trigonella foenumgraecum) ...... 19B Group 19, specifies the representative Grains of paradise (Aframomum melegueta) ...... 19B commodities for each subgroup, and Horehound (Marrubium vulgare) ...... 19A Hyssop (Hyssopus officinalis) ...... 19A lists all the commodities included in Juniper berry (Juniperus communis) ...... 19B each subgroup.

TABLE 2—CROP GROUP 19 SUBGROUPS

Representative commodities Commodities

Crop Subgroup 19A. Herb subgroup. Basil (fresh and dried) and chive...... Angelica; balm; basil; borage; burnet; camomile; catnip; chervil (dried); chive; chive, Chinese, clary; coriander (leaf); costmary; culantro (leaf); curry (leaf); dillweed; horehound; hyssop; lavender; lemongrass; lovage (leaf); marigold; marjoram (Origanum spp.); nasturtium; parsley (dried); pennyroyal; rosemary; rue; sage; savory, summer and winter; sweet bay; tansy; tarragon; thyme; wintergreen; woodruff; and wormwood. Crop Subgroup 19B. Spice subgroup. Black pepper; and celery seed or dill seed...... Allspice; anise (seed); anise, star; annatto (seed); caper (buds); caraway; caraway, black; cardamom; cassia (buds); celery (seed); cinnamon; clove (buds); coriander (seed); culantro (seed); cumin; dill (seed); fennel, common; fennel, Florence (seed); fenugreek; grains of paradise; juniper (berry); lovage (seed); mace; mustard (seed); nutmeg; pepper, black; pepper, white; poppy (seed); saffron; and vanilla.

(27) Crop Group 20. Oilseed Group. (ii) Table. The following Table 1 lists (i) Representative commodities. all the commodities listed in Crop Rapeseed (canola varieties only); sun- Group 20 and identifies the related crop flower, seed and cottonseed.

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subgroups and includes cultivars and/or varieties of these commodities.

TABLE 1—CROP GROUP 20: OILSEED GROUP

Related crop Commodities subgroups

Borage, Borago officinalis L ...... 20A Calendula, Calendula officinalis L ...... 20B Castor oil plant, Ricinus communis L ...... 20B Chinese tallowtree, Triadica sebifera (L.) Small ...... 20B Cottonseed, Gossypium hirsutum L. Gossypium spp ...... 20C Crambe, Crambe hispanica L.; C. abyssinica Hochst. ex R.E. Fr ...... 20A Cuphea, Cuphea hyssopifolia Kunth ...... 20A Echium, Echium plantagineum L ...... 20A Euphorbia, Euphorbia esula L ...... 20B Evening primrose, Oenothera biennis L ...... 20B Flax seed, Linum usitatissimum L ...... 20A Gold of pleasure, Camelina sativa (L.) Crantz ...... 20A Hare’s ear mustard, Conringia orientalis (L.) Dumort ...... 20A Jojoba, Simmondsia chinensis (Link) C.K. Schneid ...... 20B Lesquerella, Lesquerella recurvata (Engelm. ex A. Gray) S. Watson ...... 20A Lunaria, Lunaria annua L ...... 20A Meadowfoam, Limnanthes alba Hartw. ex Benth ...... 20A Milkweed, Asclepias spp ...... 20A Mustard seed, Brassica hirta Moench, Sinapis alba L. subsp. Alba...... 20A Niger seed, Guizotia abyssinica (L.f.) Cass ...... 20B Oil radish, Raphanus sativus L. var. oleiformis Pers ...... 20A Poppy seed, Papaver somniferum L. subsp. Somniferum ...... 20A Rapeseed, Brassica spp.; B. napus L ...... 20A Rose hip, Rosa rubiginosa L ...... 20B Safflower, Carthamus tinctorious L ...... 20B Sesame, Sesamum indicum L., S. radiatum Schumach. & honn ...... 20A Stokes aster, Stokesia laevis (Hill) Greene ...... 20B Sunflower, Helianthus annuus L ...... 20B Sweet rocket, Hesperis matronalis L ...... 20A Tallowwood, Ximenia americana L ...... 20B Tea oil plant, Camellia oleifera C. Abel ...... 20B Vernonia, Vernonia galamensis (Cass.) Less ...... 20B Cultivars, varieties, and/or hybrids of these.

(iii) Table. The following Table 2 commodities for each subgroup and identifies the crop subgroups for Crop lists all the commodities included in Group 20, specifies the representative each subgroup.

TABLE 2—CROP GROUP 20: SUBGROUP LISTING

Representative commodities Commodities

Crop subgroup 20A. Rapeseed subgroup Rapeseed, canola varieties only ...... Borage; crambe; cuphea; echium; flax seed; gold of pleasure; hare’s ear mustard; lesquerella; lunaria; meadowfoam; milkweed; mustard seed; oil radish; poppy seed; rapeseed; sesame; sweet rocket cultivars, varieties, and/or hybrids of these. Crop subgroup 20B. Sunflower subgroup Sunflower, seed...... Calendula; castor oil plant; chinese tallowtree; euphorbia; evening primrose; jojoba; niger seed; rose hip; safflower; stokes aster; sunflower; tallowwood; tea oil plant; vernonia; cultivars, varieties, and/or hybrids of these. Crop subgroup 20C. Cottonseed subgroup Cottonseed ...... Cottonseed; cultivars, varieties, and/or hybrids of these.

(28) Crop Group 21. Edible fungi (i) Representative commodities. White Group. button mushroom and any one oyster mushroom or any Shiitake mushroom.

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(ii) Table. The following is a list of all in compliance with the tolerances es- the commodities in Crop Group 21. tablished in this part 180 are identified There are no related subgroups. among the methods contained or referenced in the Food and Drug Adminis- CROP GROUP 21—EDIBLE FUNGI GROUP— tration’s ‘‘Pesticide Analytical Man- COMMODITIES ual’’ which is available from the Food Blewitt (Lepista nuda) and Drug Administration, Department Bunashimeji (Hypsizygus marrmoreus) Chinese mushroom (Volvariella volvacea) (Bull.) Singer of Health, Education, and Welfare, 200 Enoki (Flammulina velutipes) (Curt.) Singer C Street SW., Washington, DC 20204. Hime-Matsutake (Agaricus blazei) Murill Hirmeola (Auricularia auricular) § 180.103 Captan; tolerances for resi- Maitake (Grifola frondosa) dues. Morel (Morchella spp.) Nameko (Pholiota nameko) (a)(1) General. Tolerances are estab- Net Bearing (Dictyophora) lished for residues of the fungicide, Oyster mushroom (Pleurotus spp.) Pom Pom (Hericium erinaceus) captan (N-trichloromethylthio-4- Reishi mushroom (Ganoderma lucidum (Leyss. Fr.) Karst.) cyclohexene-1,2-dicarboximide) in or on Rodman’s agaricus (Agaricus bitorquis) (Quel.) Saccardo the following commodities: Shiitake mushroom (Lentinula edodes (Berk.) Pegl.) Shimeji (Tricholoma conglobatum) Parts per Stropharia (Stropharia spp.) Commodity million Truffle (Tuber spp.) White button mushroom (Agaricus bisporous (Lange) Almond ...... 0.25 Imbach) Almond, hulls ...... 75 .0 White Jelly Fungi (Tremella fuciformis) Animal feed, nongrass, group 18 ...... 0 .05 Apple ...... 25.0 [60 FR 26635, May 17, 1995, as amended at 72 Apricot ...... 10 .0 FR 69156, 69157, Dec. 7, 2007; 73 FR 52, Jan. 2, Blueberry ...... 20 .0 2008; 75 FR 76289, Dec. 8, 2010; 77 FR 50620, Caneberry, subgroup 13A ...... 25.0 Cherry, sweet ...... 50 .0 Aug. 22, 2012] Cherry, tart ...... 50.0 Cotton, undelinted seed ...... 0 .05 Dill, seed ...... 0 .05 Subpart C—Specific Tolerances Flax, seed ...... 0 .05 Grape ...... 25 .0 Grain, cereal, forage, fodder and straw, group EDITORIAL NOTE: Nomenclature changes to 16 ...... 0 .05 subpart C of part 180 appear at 67 FR 41803– Grain, cereal, group 15 ...... 0.05 41808, June 19, 2002; 67 FR 42393–42397, June Grass, forage ...... 0 .05 21, 2002; 68 FR 39430–39435, July 1, 2003; 71 FR Grass, hay ...... 0 .05 74804–74812, Dec. 13, 2006; 72 FR 53137–53151, Nectarine ...... 25 .0 Sept. 18, 2007; 72 FR 61536, Oct. 31, 2007; 73 FR Okra ...... 0.05 Peach ...... 15 .0 60155–60157, Oct. 10, 2008; 75 FR 56014, Sept. 15, Peanut ...... 0 .05 2010; and 76 FR 34885, June 15, 2011. Peanut, hay ...... 0.05 Pear ...... 25 .0 § 180.101 Specific tolerances; general Plum, prune, fresh ...... 10.0 provisions. Rapeseed, forage ...... 0 .05 Rapeseed, seed ...... 0 .05 (a) The tolerances established for Safflower, seed ...... 0 .05 pesticide chemicals in this subpart C Sesame, seed ...... 0 .05 Strawberry ...... 20.0 apply to residues resulting from their Sunflower, seed ...... 0.05 application prior to harvest or slaugh- Vegetable, brassica leafy, group 5 ...... 0 .05 ter, unless otherwise stated. Toler- Vegetable, bulb, group 3 ...... 0 .05 Vegetable, cucurbit, group 9 ...... 0.05 ances are expressed in terms of parts Vegetable, foliage of legume, group 7 ...... 0 .05 by weight of the pesticide chemical per Vegetable, fruiting, group 8 ...... 0.05 one million parts by weight of the raw Vegetable, leafy, except brassica, group 4 ...... 0 .05 Vegetable, leaves of root and tuber, group 2 ..... 0 .05 agricultural commodity. Vegetable, legume, group 6 ...... 0 .05 (b) The poisonous and deleterious Vegetable, root and tuber, group 1 ...... 0 .05 substances for which tolerances are established by the regulations in this (2) Tolerances are established for the subpart C are named by their common combined residues of the fungicide, names wherever practicable, otherwise captan (N-trichloromethylthio-4- by their chemical names. cyclohexene-1,2-dicarboximide) and its (c) The analytical methods to be used metabolite 1,2,3,6- for determining whether pesticide resi- tetrahydrophthalimide (THPI), meas- dues, including negligible residues, in ured at THPI, in or on the following or on raw agricultural commodities are commodities:

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Parts per Parts per Commodity million Commodity million

Cattle, fat ...... 0.15 Lemon ...... 0.5 Cattle, meat ...... 0 .20 Nut, macadamia ...... 0.05 Cattle, meat byproducts ...... 0.30 Olive ...... 1 Goat, fat ...... 0 .15 Papaya ...... 0 .5 Goat, meat ...... 0.20 Peach ...... 0 .1 Goat, meat byproducts ...... 0 .30 Hog, fat ...... 0 .15 Pear ...... 1 Hog, meat ...... 0 .20 Pea, field, seed ...... 0 .1 Hog, meat byproducts ...... 0 .30 Pea, field, vines ...... 2 Horse, fat ...... 0 .15 Pea, field, hay ...... 2 Horse, meat ...... 0 .20 Pecan ...... 0 .05 Horse, meat byproducts ...... 0 .30 Peppermint, tops ...... 1 .5 Milk ...... 0.10 Pineapple ...... 0.1 Sheep, fat ...... 0 .15 Sheep, meat ...... 0.20 Pineapple, process residue ...... 0 .4 Sheep, meat byproducts ...... 0 .30 Sheep, fat ...... 1 Sheep, meat ...... 1 (b) Section 18 emergency exemptions. Sheep, meat byproducts ...... 1 [Reserved] Sorghum, grain, forage ...... 2 Sorghum, grain, grain ...... 0 .5 (c) Tolerances with regional registra- Sorghum, grain, stover ...... 2 tions. [Reserved] Spearmint, tops ...... 1 .5 (d) Indirect or inadvertent residues. Sugarcane, cane ...... 0.2 [Reserved] Sugarcane, molasses ...... 0 .7 Walnut ...... 0 .05 [72 FR 52016, Sept. 12, 2007] Wheat, bran ...... 0.7 Wheat, forage ...... 2 § 180.106 Diuron; tolerances for resi- Wheat, grain ...... 0 .5 dues. Wheat, hay ...... 2 (a) General. Tolerances are estab- Wheat, straw ...... 1 .5 lished for the combined residues of the herbicide diuron, 3-(3,4- (b) Section 18 emergency exemptions. dichlorophenyl)-1,1-dimethylurea and [Reserved] its metabolites convertible to 3,4- (c) Tolerances with regional registra- dichloroaniline in or on food commod- tions. Tolerances with a regional reg- ities, as follows: istration as defined in § 180.1(l) are established for the combined residues of Parts per Commodity million the herbicide diuron (3-(3,4- dichlorophenyl)-1,1-dimethylurea and Alfalfa, forage ...... 3.0 its metabolites convertible to 3,4- Alfalfa, hay ...... 2.0 Apple ...... 0.1 dichloroaniline) in or on the raw agri- Artichoke, globe ...... 1 cultural commodities: Asparagus ...... 7 Banana ...... 0.1 Parts per Berry group 13 ...... 0 .1 Commodity million Cattle, fat ...... 1 Cattle, meat ...... 1 Barley, bran ...... 0 .7 Cattle, meat byproducts ...... 1 Barley, grain ...... 0 .2 Citrus, oil ...... 3.0 Barley, hay ...... 2 Corn, field, grain ...... 0 .1 Corn, pop, grain ...... 0.1 Barley, straw ...... 1 .5 Cotton, undelinted seed ...... 0 .2 Cactus ...... 0 .05 Fish – freshwater finfish, farm raised ...... 2 .0 Clover, forage ...... 0.1 Fruit, citrus, group 10, except lemon ...... 0 .05 Clover, hay ...... 1.0 Goat, fat ...... 1 Oat, forage ...... 2 Goat, meat ...... 1 Oat, grain ...... 0 .1 Goat, meat byproducts ...... 1 Oat, hay ...... 2 Grain, aspirated fractions ...... 5 .0 Oat, straw ...... 1.5 Grape ...... 0 .05 Grass, forage, except bermudagrass ...... 2 Trefoil, forage ...... 0 .1 Grass, hay, except bermudagrass ...... 2 Trefoil, hay ...... 1 .5 Hazelnut ...... 0 .1 Vetch, forage ...... 0 .1 Hog, fat ...... 1 Vetch, hay ...... 1 .5 Hog, meat ...... 1 Hog, meat byproducts ...... 1 Horse, fat ...... 1 Horse, meat ...... 1 Horse, meat byproducts ...... 1

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(d) Indirect or inadvertent residues. methyl acetyl phosphoramidothioate, [Reserved] including its metabolites and degradates other than methamidophos, [63 FR 2164, Jan. 14, 1998, as amended at 63 FR 57072, Oct. 26, 1998; 64 FR 41305, July 30, in or on all food items (other than 1999; 66 FR 28671, May 24, 2001; 67 FR 46883, those already covered by a higher tol- July 17, 2002; 69 FR 71717, Dec. 10, 2004; 72 FR erance as a result of use on growing 32540, June 13, 2007; 72 FR 35666, June 29, 2007; crops) in food handling establishments 73 FR 54958, Sept. 24, 2008; 76 FR 34885, June where food and food products are held, 15, 2011] processed, prepared and served, including food service, manufacturing and § 180.108 Acephate; tolerances for resi- processing establishments, such as res- dues. taurants, cafeterias, supermarkets, (a) General. (1) Tolerances are estab- bakeries, breweries, dairies, meat lished for residues of acephate, O,S-di- slaughtering and packing plants, and methyl acetyl phosphoramidothioate, canneries, where application of including its metabolites and acephate shall be limited solely to spot degradates other than methamidophos, and/or crack and crevice treatment (a in or on the commodities in the fol- coarse, low-pressure spray shall be used lowing table. Compliance with the tol- to avoid atomization or splashing of erance levels specified in this para- the spray for spot treatments; equip- graph is to be determined by measuring ment capable of delivering a pin- only acephate, O,S-dimethyl acetyl stream of insecticide shall be used for phosphoramidothioate, in or on the crack and crevice treatments). Spray commodity. concentration shall be limited to a maximum of 1.0 percent active ingre- 1 Parts per Commodity million dient. Contamination of food or food- contact surfaces shall be avoided. Com- Bean, dry, seed ...... 3 .0 Bean, succulent ...... 3 .0 pliance with the tolerance levels speci- Brussels sprouts ...... 3 .0 fied in this paragraph is to be deter- Cattle, fat ...... 0.1 mined by measuring only acephate, Cattle, meat ...... 0 .1 Cattle, meat byproducts ...... 0.1 O,S-dimethyl acetyl Cauliflower ...... 2 .0 phosphoramidothioate, in or on the Celery ...... 10 commodity. Cotton, hulls ...... 1 .0 Cotton, meal ...... 1 .0 (3) Tolerances are established for res- Cotton, undelinted seed ...... 0 .5 idues of methamidophos, O,S-dimethyl Cranberry ...... 0 .5 phosphoramidothioate, including its Egg ...... 0 .1 Goat, fat ...... 0 .1 metabolites and degradates, in or on Goat, meat ...... 0.1 the commodities in the following table Goat, meat byproducts ...... 0 .1 as a result of the application of Hog, fat ...... 0 .1 Hog, meat ...... 0 .1 acephate. Compliance with the toler- Hog, meat byproducts ...... 0 .1 ance levels specified in this paragraph Horse, fat ...... 0 .1 is to be determined by measuring only Horse, meat ...... 0 .1 Horse, meat byproducts ...... 0 .1 methamidophos, O,S-dimethyl Lettuce, head ...... 10 phosphoramidothioate, in or on the Milk ...... 0.1 commodity. Peanut ...... 0 .2 Pepper ...... 4 .0 Parts per Peppermint, tops ...... 27 Commodity million Poultry, fat ...... 0.1 Poultry, meat ...... 0 .1 Bean, dry, seed ...... 1 Poultry, meat byproducts ...... 0.1 Bean, succulent ...... 1 Sheep, fat ...... 0 .1 Brussels sprouts ...... 0 .5 Sheep, meat ...... 0.1 Cauliflower ...... 0 .5 Sheep, meat byproducts ...... 0 .1 Celery ...... 1 Spearmint, tops ...... 27 Cranberry ...... 0 .1 Soybean, seed ...... 1 .0 Lettuce, head ...... 1 1 Where there is a direct use of methamidophos on the Pepper ...... 1 commodity, residues of methamidophos resulting from Peppermint, tops ...... 1 methamidophos application are regulated under 40 CFR Spearmint, tops ...... 1 180.315. (2) A tolerance of 0.02 ppm is estab- (b) Section 18 emergency exemptions. lished for residues of acephate, O,S-di- [Reserved]

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(c) Tolerances with regional registra- Parts per Expiration/ tions. A tolerance with a regional reg- Commodity revocation million date istration is established for residues of acephate, O,S-dimethyl acetyl Grape ...... 7 12/31/12 phosphoramidothioate, including its Kale ...... 10 12/31/12 Kohlrabi ...... 10 12/31/12 metabolites and degradates other than Lettuce ...... 10 12/31/12 methamidophos, in or on the com- Melon ...... 4 12/31/12 modity in the following table. Compli- Mustard greens ...... 10 12/31/12 Nectarine ...... 10 12/31/12 ance with the tolerance level specified Onion ...... 7 12/31/12 in this paragraph is to be determined Papaya ...... 10 12/31/12 by measuring only acephate, O,S-di- Peach ...... 10 12/31/12 Pepper ...... 7 12/31/12 methyl acetyl phosphoramidothioate, Potato ...... 0.1 12/31/12 in or on the commodity. Pumpkin ...... 7 12/31/12 Squash, summer ...... 4 12/31/12 Parts per Commodity1 Squash, winter ...... 4 12/31/12 million Tomato ...... 4 12/31/12 Turnip, greens ...... 10 12/31/12 Nut, macadamia ...... 0.05 Turnip, roots ...... 7 12/31/12 1 Where there is a direct use of methamidophos on the commodity, residues of methamidophos resulting from (b) Section 18 emergency exemptions. methamidophos application are regulated under 40 CFR 180.315. [Reserved] (c) Tolerances with regional registra- (d) Indirect or inadvertent residues. tions. [Reserved] [Reserved] (d) Indirect or inadvertent residues. [63 FR 13542, Mar. 20, 1998, as amended at 67 [Reserved] FR 49615, July 31, 2002; 73 FR 5108, Jan. 29, 2008; 75 FR 60237, Sept. 29, 2010] [62 FR 49924, Sept. 24, 1997, as amended at 63 FR 57072, Oct. 26, 1998; 64 FR 13103, Mar. 17, § 180.110 Maneb; tolerances for resi- 1999; 64 FR 72284, Dec. 27, 1999; 66 FR 64773, dues. Dec. 14, 2001; 68 FR 37764, June 25, 2003; 70 FR 37696, June 30, 2005; 70 FR 75739, Dec. 21, 2005; (a) General. Tolerances for residues of 74 FR 636, Jan. 7, 2009; 74 FR 46371, Sept. 9, the fungicide maneb (manganous 2009; 76 FR 34885, June 15, 2011; 76 FR 40814, ethylenebisdithiocarbamate), cal- July 12, 2011] culated as zinc EFFECTIVE DATE NOTE: At 79 FR 27501, May ethylenebisdithiocarbamate, are estab- 14, 2014, § 180.110 was removed, effective Nov. lished in or on raw agricultural com- 14, 2014. modities in the following table: § 180.111 Malathion; tolerances for res- Expiration/ idues. Commodity Parts per revocation million date (a) General. (1) Tolerances are estab- Almond ...... 0.1 12/31/12 lished for residues of the insecticide Apple ...... 2 12/31/12 malathion (O,O-dimethyl Apricot ...... 10 12/31/12 dithiophosphate of diethyl Banana (not more than 0.5 part per million shall be in the pulp after mercaptosuccinate) in or on the fol- peel is removed and discarded lowing food commodities: (preharvest application only)) ...... 4 12/31/12 Bean, dry, seed ...... 7 12/31/12 Commodity Parts per Bean, succulent ...... 10 12/31/12 million Beet, sugar, tops ...... 45 12/31/12 Broccoli ...... 10 12/31/12 Alfalfa, forage ...... 135 Brussels sprouts ...... 10 12/31/12 Alfalfa, hay ...... 135 Cabbage ...... 10 12/31/12 Almond, hulls ...... 50 Cabbage, Chinese, bok choy ...... 10 12/31/12 Almond, postharvest ...... 8 Cabbage, Chinese, napa ...... 10 12/31/12 Apple ...... 8 Carrot, roots ...... 7 12/31/12 Apricot ...... 8 Cauliflower ...... 10 12/31/12 Asparagus ...... 8 Celery ...... 5 12/31/12 Avocado ...... 8 Collards ...... 10 12/31/12 Barley, grain, postharvest ...... 8 Corn, sweet, kernel plus cob with Bean, dry, seed ...... 8 husks removed ...... 5 12/31/12 Bean, succulent ...... 8 Cranberry ...... 7 12/31/12 Beet, garden, roots ...... 8 Cucumber ...... 4 12/31/12 Beet, garden, tops ...... 8 Eggplant ...... 7 12/31/12 Beet, sugar, roots ...... 1 Endive ...... 10 12/31/12 Beet, sugar, tops ...... 8 Fig ...... 7 12/31/12 Blackberry ...... 8

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Parts per Parts per Commodity million Commodity million

Blueberry ...... 8 Rice, wild ...... 8 Boysenberry ...... 8 Rutabaga ...... 8 Carrot, roots ...... 8 Rye, grain, postharvest ...... 8 Chayote, fruit ...... 8 Safflower, seed ...... 0 .2 Chayote, roots ...... 8 Salsify, roots ...... 8 Cherry ...... 8 Salsify, tops ...... 8 Chestnut ...... 1 Shallot, bulb ...... 8 Clover, forage ...... 135 Sorghum, grain, forage ...... 8 Clover, hay ...... 135 Sorghum, grain, grain, postharvest ...... 8 Corn, field, forage ...... 8 Soybean, forage ...... 135 Corn, field, grain, postharvest ...... 8 Soybean, hay ...... 135 Corn, pop, grain, postharvest ...... 8 Soybean, seed ...... 8 Corn, sweet, forage ...... 8 Soybean, vegetable, succulent ...... 8 Corn, sweet, kernel plus cob with husks re- Spearmint, tops ...... 8 moved ...... 2 Squash, summer ...... 8 Cowpea, forage ...... 135 Squash, winter ...... 8 Cowpea, hay ...... 135 Strawberry ...... 8 Cranberry ...... 8 Sunflower, seed, postharvest ...... 8 Cucumber ...... 8 Sweet potato, roots ...... 1 Currant ...... 8 Tangerine ...... 8 Date, dried fruit ...... 8 Tomato ...... 8 Dewberry ...... 8 Trefoil, forage ...... 135 Eggplant ...... 8 Trefoil, hay ...... 135 Fig ...... 8 Turnip, greens ...... 8 Flax, seed ...... 0 .1 Turnip, roots ...... 8 Garlic, bulb ...... 8 Vegetable, brassica, leafy, group 5 ...... 8 Gooseberry ...... 8 Vegetable, leafy, except brassica, group 4 ...... 8 Grape ...... 8 Vetch, hay ...... 135 Grapefruit ...... 8 Walnut ...... 8 Guava ...... 8 Wheat, grain, postharvest ...... 8 Hazelnut ...... 1 Hop, dried cones ...... 1 (2) Tolerances are established for the Horseradish ...... 8 combined residues of the insecticide Kumquat ...... 8 Leek ...... 8 malathion (O,O-dimethyl Lemon ...... 8 dithiophosphate of diethyl Lentil, seed ...... 8 mercaptosuccinate) and its metabolite, Lespedeza, hay ...... 135 malaoxon (O,O-dimethyl thiophosphate Lime ...... 8 Loganberry ...... 8 of diethyl mercaptosuccinate), in or on Lupin, seed ...... 8 the following food commodities: Mango ...... 8 Melon ...... 8 Commodity Parts per Mushroom ...... 8 million Nectarine ...... 8 Nut, macadamia ...... 1 Barley, straw ...... 50 Oat, grain, postharvest ...... 8 Corn, field, stover ...... 30 .0 Okra ...... 8 Cotton, undelinted seed ...... 20 .0 Onion, bulb ...... 8 Grass, forage ...... 200 Onion, green ...... 8 Grass, hay ...... 270 Orange ...... 8 Oat, forage ...... 4 .0 Papaya ...... 1 Oat, straw ...... 50 Parsnip ...... 8 Rye, forage ...... 4 .0 Passionfruit ...... 8 Rye, straw ...... 50 Pea ...... 8 Watercress ...... 0 .2 Pea, field, hay ...... 8 Wheat, forage ...... 4 .0 Pea, field, vines ...... 8 Wheat, straw ...... 50 Peach ...... 8 Peanut, hay ...... 135 (3) Tolerances are established for res- Peanut, postharvest ...... 8 idues of the insecticide malathion Pear ...... 8 Pecan ...... 8 (O,O-dimethyl dithiophosphate of Pepper ...... 8 diethyl mercaptosuccinate), in or on Peppermint, tops ...... 8 the following food commodities: Pineapple ...... 8 Plum ...... 8 Commodity Parts per Plum, prune ...... 8 million Potato ...... 8 Pumpkin ...... 8 Cattle, fat ...... 4 Quince ...... 8 Cattle, meat1 ...... 4 Radish ...... 8 Cattle, meat byproducts1 ...... 4 Raspberry ...... 8 Egg ...... 0 .1 Rice, grain, postharvest ...... 8 Goat, fat ...... 4

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dried pulp shall not exceed 50 parts per Commodity Parts per million million. Goat, meat1 ...... 4 (ii) A tolerance of 10 parts per million Goat, meat byproducts1 ...... 4 is established for malathion in non- Hog, fat ...... 4 medicated cattle feed concentrate Hog, meat1 ...... 4 blocks resulting from its application as Hog, meat byproducts1 ...... 4 Horse, fat ...... 4 a pesticide to paper used in packaging Horse, meat1 ...... 4 the nonmedicated cattle feed con- Horse, meat byproducts1 ...... 4 centrate blocks. Milk, fat ...... 0 .5 (b) Section 18 emergency exemptions. Poultry, fat ...... 4 [Reserved] Poultry, meat1 ...... 4 Poultry, meat byproducts1 ...... 4 (c) Tolerances with regional registra- Sheep, fat ...... 4 tions. [Reserved] Sheep, meat1 ...... 4 (d) Indirect or inadvertent residues. Sheep, meat byproducts1 ...... 4 [Reserved] 1 The tolerance level shall not be exceeded in any cut of meat or in any meat byproducts from cattle, goat, hog, horse, [43 FR 22974, May 30, 1978, as amended at 43 poultry, or sheep. FR 45584, Oct. 3, 1978; 44 FR 38844, July 3, (4) Malathion may be safely used in 1979; 45 FR 76145, Nov. 18, 1980; 47 FR 42738, Sept. 29, 1982; 47 FR 55226, Dec. 8, 1982; 52 FR accordance with the following condi- 45183, Nov. 25, 1987; 62 FR 66023, 66025, Dec. 17, tions: 1997; 65 FR 33694, May 24, 2000; 72 FR 35665, (i) It is incorporated into paper trays June 29, 2007; 73 FR 54959, Sept. 24, 2008; 74 FR in amounts not exceeding 100 milli- 47455, Sept. 16, 2009; 75 FR 60238, Sept. 29, grams per square foot. 2010] (ii) Treated paper trays are intended for use only in the drying of grape (rai- § 180.114 Ferbam; tolerances for resi- sins). dues. (iii) Total residues of malathion re- (a) General. Tolerances are estab- sulting from drying of grape on treated lished for residues of the fungicide trays and from application to grape be- ferbam (ferric fore harvest shall not exceed 12 parts dimethyldithiocarbamate), calculated per million on processed ready-to-eat as carbon disulfide, in or on the fol- raisins. lowing food commodities: (5) Residues of malathion in saf- Expiration/ flower, refined oil from application to Parts per Commodity million Revocation the growing safflower plant shall not Date exceed 0.6 parts per million. Apple ...... 4.0 1 None (6) Malathion may be safely used for Bean ...... 7.0 1 10/27/07 the control of insects during the drying Cabbage ...... 7.0 1 10/27/07 of grape (raisins) in compliance with Cherry ...... 4.0 1 None Cranberry ...... 4.0 1 None paragraph (a)(4) of this section by in- Fruit, citrus, group 10 ...... 4.0 1 None corporation into paper trays in Grape ...... 4.0 1 None amounts not exceeding 100 milligrams Lettuce ...... 7.0 1 10/27/07 per square foot. Nectarine ...... 4.0 1 None Peach ...... 4.0 1 None (7) Malathion (O,O-dimethyl Pear ...... 4.0 1 None dithiophosphate of diethyl Raspberry ...... 7.0 1 10/27/07 mercaptosuccinate) may be safely used 1Some of these tolerances were established on the basis of in feed in accordance with the fol- data acquired at the public hearings held in 1950 (formerly § 180.101) and the remainder were established on the basis lowing conditions. of pesticide petitions presented under the procedure specified (i) A tolerance of 50 parts per million in the amendment to the Federal Food, Drug, and Cosmetic is established for residues of malathion Act by Pub. L. 518, 83d Congress (68 Stat. 511) in citrus, dried pulp for cattle feed, (b) Section 18 emergency exemptions. when present as the result of the appli- [Reserved] cation of the pesticide to bagged citrus (c) Tolerances with regional registra- pulp during storage. Whether or not tions. Tolerances with regional reg- tolerances for residues of malathion on istrations, as defined in § 180.1(l), are the fresh fruit have been established established for residues of the fun- under section 408 of the Act, the total gicide ferbam (ferric residue of malathion in the citrus, dimethyldithiocarbamate), calculated

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as carbon disulfide, in or on the fol- ethyl dipropylthiocarbamate, including lowing food commodities: its metabolites and degradates, in or on the commodities in the following Parts per mil- Commodity lion table. Compliance with the tolerance levels specified in this paragraph is to Mango ...... 4.0 1 be determined by measuring only the 1 This tolerance was established on the basis of data ac- sum of S-ethyl dipropylthiocarbamate, quired at the public hearings held in 1950 (formerly § 180.101) and the remainder was established on the basis of pesticide S-ethyl (2- petitions presented under the procedure specified in the hydroxypropyl)propylcarbamothioate, amendment to the Federal Food, Drug, and Cosmetic Act by Pub. L. 518, 83d Congress (68 Stat. 511) S-(2-hydroxyethyl)dipropylcarbamothioate, and S- (d) Indirect or inadvertent residues. ethyl (3- [Reserved] hydroxypropyl)propylcarbamothioate, [63 FR 57072, Oct. 26, 1998, as amended at 72 calculated as the stoichiometric equiv- FR 53453, Sept. 19, 2007] alent of S-ethyl dipropylthiocarbamate, in or on the § 180.116 Ziram; tolerances for resi- commodity. dues. (a) General. Tolerances are estab- Parts per Commodity million lished for residues of the fungicide ziram (zinc dimethyldithiocarbamate), Alfalfa, forage ...... 0.2 calculated as zinc Alfalfa, hay ...... 0.6 Almond ...... 0.08 ethylenebisdithiocarbamate, in or on Almond, hulls ...... 0 .08 the following food commodities: Bean, dry, seed ...... 0 .08 Bean, succulent ...... 0 .08 Beet, garden, tops ...... 0 .5 Parts per Expiration/ Commodity million revocation Beet, sugar, molasses ...... 0 .4 date Beet, sugar, tops ...... 0.5 Clover, forage ...... 0.1 1 Almond ...... 0.1 None Clover, hay ...... 0.1 1 Apple ...... 7.0 None Corn, field, forage ...... 0 .08 1 Apricot ...... 7.0 None Corn, field, grain ...... 0 .08 1 Blackberry ...... 7.0 5/11/13 Corn, field, stover ...... 0 .08 Blueberry ...... 1 7.0 None Corn, pop, grain ...... 0.08 Cherry, sweet ...... 1 7.0 None Corn, pop, stover ...... 0.08 Cherry, tart ...... 1 7.0 None Corn, sweet, forage ...... 0 .08 Grape ...... 7.0 None Corn, sweet, kernel plus cob with husks re- Huckleberry ...... 7.0 None moved ...... 0 .08 Peach ...... 7.0 None Corn, sweet, stover ...... 0 .08 Pear ...... 1 7.0 None Pecan ...... 0.1 None Cotton, gin byproducts ...... 0 .20 Quince ...... 1 7.0 None Cotton, undelinted seed ...... 0 .08 Strawberry ...... 7.0 None Fruit, citrus, group 10 ...... 0 .1 Tomato ...... 1 7.0 None Lespedeza, forage ...... 0 .1 Lespedeza, hay ...... 0.1 1 Some of these tolerances were established on the basis of Pea, succulent ...... 0 .08 data acquired at the public hearings held in 1950 (formerly Safflower, seed ...... 0 .08 § 180.101) and the remainder were established on the basis Sunflower, seed ...... 0.08 of pesticide petitions presented under the procedure specified in the amendment to the Federal Food, Drug, and Cosmetic Tomato ...... 0.08 Act by Public Law 518, 83d Congress (68 Stat. 511). Trefoil, forage ...... 0 .1 Trefoil, hay ...... 0 .1 (b) Section 18 emergency exemptions. Vegetable, root ...... 0 .1 [Reserved] Walnut ...... 0 .08 (c) Tolerances with regional registrations. [Reserved] (b) Section 18 emergency exemptions. (d) Indirect or inadvertent residues. [Reserved] [Reserved] (c) Tolerances with regional registrations. [Reserved] [68 FR 39437, July 1, 2003, as amended at 71 (d) Indirect or inadvertent residues. FR 54432, Sept. 15, 2006; 73 FR 54959, Sept. 24, [Reserved] 2008; 77 FR 59123, Sept. 26, 2012] [75 FR 60239, Sept. 29, 2010] § 180.117 S-Ethyl dipropylthiocarbamate; tolerances § 180.121 Methyl parathion; tolerances for residues. for residues. (a) General. Tolerances are estab- (a) General. Tolerances are established for residues of the herbicide S- lished for residues of the insecticide

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methyl parathion, including its me- Parts per Expiration/ tabolites and degradates, in or on the Commodity Revocation million Date commodities in the table in this paragraph. Compliance with the tolerance Alfalfa, hay, postharvest ...... 50.0 10/31/11 levels specified in this paragraph is to Almond, postharvest ...... 200.0 None Apple, postharvest ...... 5.0 None be determined by measuring only Apricot, postharvest ...... 20.0 None methyl parathion, O,O-dimethyl O-(4- Artichoke, jerusalem, postharvest ... 30.0 None nitrophenyl) phosphorothioate, in or Asparagus, postharvest ...... 100.0 None Avocado, postharvest ...... 75.0 None on the commodity. Barley, grain, postharvest ...... 50.0 None Bean, lima, postharvest ...... 50.0 None Parts per Expiration/ Bean, postharvest ...... 50.0 None Commodity million Revocation Bean, snap, succulent, postharvest 50.0 None date Bean, succulent, postharvest ...... 50.0 None Beet, garden, roots, postharvest ..... 30.0 None Alfalfa, forage ...... 1.25 12/31/13 Beet, sugar, roots, postharvest ...... 30.0 None Alfalfa, hay ...... 5.0 12/31/13 Blueberry, postharvest ...... 20.0 None Almond ...... 0.1 12/31/13 Butternut, postharvest ...... 200.0 None Almond, hulls ...... 3.0 12/31/13 Cabbage, postharvest ...... 50.0 None Barley ...... 1.0 12/31/13 Cacao bean, roasted bean, Corn, field, forage ...... 1.0 12/31/13 postharvest ...... 50.0 None Corn, field, grain ...... 1.0 12/31/13 Cantaloupe, postharvest ...... 20.0 None Corn, pop, grain ...... 1.0 12/31/13 Carrot, roots, postharvest ...... 30.0 None Corn, sweet, forage ...... 1.0 12/31/13 Cashew, postharvest ...... 200.0 None Cherry, sweet, postharvest ...... 20.0 None Corn, sweet, kernel plus cob with Cherry, tart, postharvest ...... 20 None husks removed ...... 1.0 12/31/13 Chestnut, postharvest ...... 200.0 None Cotton, undelinted seed ...... 0.75 12/31/13 Cippolini, bulb, postharvest ...... 50.0 None Grass, forage ...... 1.0 12/31/13 Citron, citrus, postharvest ...... 30.0 None Oat ...... 1.0 12/31/13 Coconut, copra, postharvest ...... 100.0 None Onion ...... 1.0 12/31/13 Coffee, bean, green, postharvest .... 75.0 None Pea, field, vines ...... 1.0 12/31/13 Corn, field, grain, postharvest ...... 50.0 None Potato ...... 0.1 12/31/13 Corn, pop, postharvest ...... 240.0 None Rapeseed, seed ...... 0.2 12/31/13 Corn, sweet, kernel plus cob with Rice, grain ...... 1.0 12/31/13 husks removed, postharvest ...... 50.0 None Soybean, hay ...... 1.0 12/31/13 Cotton, undelinted seed, Soybean, seed ...... 0.1 12/31/13 postharvest ...... 200.0 10/31/11 Cucumber, postharvest ...... 30.0 None Sunflower, seed ...... 0.2 12/31/13 Cumin, seed, postharvest ...... 100.0 None Sweet potato, roots ...... 0.1 12/31/13 Eggplant, postharvest ...... 20.0 None Walnut ...... 0.1 12/31/13 Garlic, postharvest ...... 50.0 None Wheat ...... 1.0 12/31/13 Ginger, postharvest ...... 100.0 None Grape, postharvest ...... 20.0 None (b) Section 18 emergency exemptions. Grapefruit, postharvest ...... 30.0 None [Reserved] Hazelnut, postharvest ...... 200.0 None Horseradish, postharvest ...... 30.0 None (c) Tolerances with regional registra- Kumquat, postharvest ...... 30.0 None tions. [Reserved] Lemon, postharvest ...... 30.0 None Lime, postharvest ...... 30.0 None (d) Indirect or inadvertent residues. Melon, honeydew, postharvest ...... 20.0 None [Reserved] Muskmelon, postharvest ...... 20.0 None Nectarine, postharvest ...... 20.0 None [66 FR 1245, Jan. 5, 2001, as amended at 66 FR Nut, brazil, postharvest ...... 200.0 None 38955, July 26, 2001; 67 FR 38603, June 5, 2002; Nut, hickory, postharvest ...... 200.0 None 72 FR 35666, June 29, 2007; 73 FR 54959, Sept. Nut, macadamia, postharvest ...... 200.0 None 24, 2008; 74 FR 46372, Sept. 9, 2009; 76 FR 56652, Oat, postharvest ...... 50.0 None Sept. 14, 2011; 78 FR 60721, Oct. 2, 2013] Okra, postharvest ...... 30.0 None Onion, bulb, postharvest ...... 20.0 None Onion, green, postharvest ...... 20.0 None § 180.123 Inorganic bromide residues Orange, postharvest ...... 30.0 None resulting from fumigation with Parsnip, roots, postharvest ...... 30.0 None methyl bromide; tolerances for resi- Peach, postharvest ...... 20.0 None dues. Peanut, postharvest ...... 200.0 None Pear, postharvest ...... 5.0 None (a) General. (1) Tolerances are estab- Pea, blackeyed, postharvest ...... 50.0 None lished for residues of inorganic bro- Pea, postharvest ...... 50.0 None mides (calculated as Br) in or on the Pecan, postharvest ...... 200.0 None Pepper, postharvest ...... 30.0 None following food commodities which have Pimento, postharvest ...... 30.0 None been fumigated with the antimicrobial Pineapple, postharvest ...... 20.0 None agent and insecticide methyl bromide Pistachio, postharvest ...... 200.0 None Plum, postharvest ...... 20.0 None after harvest (with the exception of Pomegranate, postharvest ...... 100.0 None strawberry): Potato, postharvest ...... 75.0 None

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tion, unless a higher level is estab- Parts per Expiration/ Commodity Revocation lished elsewhere in this part. million Date (3) Tolerances are established for res- Pumpkin, postharvest ...... 20.0 None idues of inorganic bromides (calculated Quince, postharvest ...... 5.0 None as Br) as follows: Radish, postharvest ...... 30.0 None Rice, grain, postharvest ...... 50.0 None (i) 400 parts per million for residues Rutabaga, roots, postharvest ...... 30.0 None in or on dog food, resulting from fumi- Rutabaga, tops, postharvest ...... 30.0 None gation with methyl bromide. Rye, grain, postharvest ...... 50.0 None Salsify, roots, postharvest ...... 30.0 None (ii) 125 parts per million for residues Sorghum, grain, grain, postharvest 50.0 None in or on processed commodities for ani- Soybean, postharvest ...... 200.0 None mal feedstuffs from barley, corn, grain Squash, summer, postharvest ...... 30.0 None Squash, winter, postharvest ...... 20.0 None sorghum, oat, rice, rye and wheat, re- Squash, zucchini, postharvest ...... 20.0 None sulting directly from fumigation with Strawberry, postharvest ...... 60.0 None methyl bromide or from carryover and Sweet potato, postharvest ...... 75.0 None concentration of residues of inorganic Tangerine, postharvest ...... 30.0 None Timothy, hay, postharvest ...... 50.0 10/19/10 bromides from fumigation of the grains Tomato, postharvest ...... 20.0 None with methyl bromide. Turnip, roots, postharvest ...... 30.0 None (b) Section 18 emergency exemptions. Walnut, postharvest ...... 200.0 None Watermelon, postharvest ...... 20.0 None [Reserved] Wheat ...... 50.0 None (c) Tolerances with regional registrations. A tolerance with regional reg- (2) Inorganic bromide may be present istration, as defined in § 180.1(l), is es- as a residue in certain processed food tablished for residues of inorganic bro- in accordance with the following condi- mides (calculated as Br) in or on the tions: following food commodity grown in (i) When inorganic bromide residues soil fumigated with methyl bromide. are present as a result of fumigation of the processed food with methyl bro- Parts per Commodity million mide or from such fumigation in addition to the authorized use of methyl Ginger, postharvest ...... 100 bromide on the source raw agricultural commodity, as provided for in this (d) Indirect or inadvertent residues. part, the total residues of inorganic [Reserved] bromides (calculated as Br) shall not [71 FR 74812, Dec. 13, 2006, as amended at 75 exceed the following levels: FR 60239, Sept. 29, 2010] (A) 400 parts per million in or on egg, dried and herb, processed and spice. § 180.123a Inorganic bromide residues (B) 325 parts per million in or on in peanut hay and peanut hulls; cheese, parmesan and cheese, roquefort statement of policy. cheese. (a) Investigations by the Food and (C) 250 parts per million in or on to- Drug Administration show that peanut mato, concentrated products and fig, hay and peanut shells have been used dried fruit. as feed for meat and dairy animals. (D) 125 parts per million in or on While many growers now harvest pea- processed food other than those listed nuts with combines and leave the hay above. on the ground to be incorporated into (ii) When inorganic bromide residues the soil, some growers follow the prac- are present in malt beverage, fer- tice of curing peanuts on the vines in a mented in accordance with 21 CFR stack and save the hay for animal feed. 172.730(a)(2), the amount shall not ex- Peanut shells or hulls have been used ceed 25 parts per million (calculated as to a minor extent as roughage for cat- Br). tle feed. It has been established that (iii) Where tolerances are established the feeding to cattle of peanut hay and on both the raw agricultural commod- peanut hulls containing residues of in- ities and processed food made there- organic bromides will contribute con- from, the total residues of inorganic siderable residues of inorganic bro- bromides in or on the processed food mides to the meat and milk. shall not be greater than those des- (b) There are no tolerances for inor- ignated in paragraph (a)(2) of this sec- ganic bromides in meat and milk to

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cover residues from use of such peanut Commodity Parts per hulls as animal feed. Peanut hulls con- million taining residues of inorganic bromides Currant, postharvest ...... 8 from the use of methyl bromide are un- Dewberry, postharvest ...... 8 suitable as an ingredient in the feed of Egg ...... 1 meat and dairy animals and should not Fig, postharvest ...... 8 Flax, seed, postharvest ...... 8 be represented, sold, or used for that Goat, fat ...... 0 .1 purpose. Goat, meat ...... 0.1 Goat, meat byproducts ...... 0 .1 [58 FR 65555, Dec. 15, 1993] Gooseberry, postharvest ...... 8 Grape, postharvest ...... 8 § 180.124 Methyl bromide; tolerances Guava, postharvest ...... 8 for residues. Hog, fat ...... 0 .1 Hog, meat ...... 0 .1 (a) General. A tolerance is established Hog, meat byproducts ...... 0 .1 for residues of the fumigant methyl Horse, fat ...... 0 .1 bromide, including metabolites and Horse, meat ...... 0 .1 degradates, in or on the commodity in Horse, meat byproducts ...... 0 .1 the table below. Compliance with the Loganberry, postharvest ...... 8 Mango, postharvest ...... 8 tolerance level specified below is to be Milk, fat ...... 0 .25 determined by measuring only methyl Muskmelon, postharvest ...... 8 bromide. Oat, postharvest ...... 8 Orange, postharvest ...... 8 Parts per Peach, postharvest ...... 8 Commodity million Peanut, postharvest ...... 8 Pea, postharvest ...... 8 Cotton, undelinted seed ...... 150 Pear, postharvest ...... 8 Pineapple, postharvest ...... 8 (b) Section 18 emergency exemptions. Plum, prune, fresh, postharvest ...... 8 [Reserved] Potato, postharvest ...... 0 .25 Poultry, fat ...... 3 (c) Tolerances with regional registra- Poultry, meat ...... 3 tions. [Reserved] Poultry, meat byproducts ...... 3 (d) Indirect or inadvertent residues. Raspberry, postharvest ...... 8 [Reserved] Rice, postharvest ...... 20 Rye, postharvest ...... 20 [77 FR 35298, June 13, 2012] Sheep, fat ...... 0 .1 Sheep, meat ...... 0.1 § 180.127 Piperonyl butoxide; toler- Sheep, meat byproducts ...... 0 .1 ances for residues. Sorghum, grain, postharvest ...... 8 Sweet potato, postharvest ...... 0 .25 (a) General. (1) Tolerances for resi- Tomato, postharvest ...... 8 dues of the insecticide piperonyl Walnut, postharvest ...... 8 butoxide [(butyl carbityl)(6-propyl Wheat, postharvest ...... 20 piperonyl)ether] are established in or (2) Piperonyl butoxide may be safely on the following food commodities: used in accordance with the following prescribed conditions: Commodity Parts per million (i) It is used or intended for use in Almond, postharvest ...... 8 combination with pyrethrins for con- Apple, postharvest ...... 8 trol of insects: Barley, postharvest ...... 20 (A) In cereal grain mills and in stor- Bean, postharvest ...... 8 Birdseed, mixtures, postharvest ...... 20 age areas for milled cereal grain prod- Blackberry, postharvest ...... 8 ucts, whereby the amount of piperonyl Blueberry, postharvest ...... 8 butoxide is at least equal to but not Boysenberry, postharvest ...... 8 more than 10 times the amount of Buckwheat, grain, postharvest ...... 20 Cattle, fat ...... 0.1 pyrethrins in the formulation. Cattle, meat ...... 0 .1 (B) On the outer ply of multiwall Cattle, meat byproducts ...... 0.1 paper bags of 50 pounds or more capac- Cherry, sweet, postharvest ...... 8 Cherry, tart, postharvest ...... 8 ity in amounts not exceeding 60 milli- Cacoa bean, roasted bean, postharvest ...... 8 grams per square foot, whereby the Coconut, copra, postharvest ...... 8 amount of piperonyl butoxide is equal Corn, field, grain, postharvest ...... 20 to 10 times the amount of pyrethrins in Corn, pop, postharvest ...... 20 Cotton, undelinted seed, postharvest ...... 8 the formulation. Such treated bags are Crabapple, postharvest ...... 8 to be used only for food, dried.

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(C) On cotton bags of 50 pounds or it shall be used in accordance with more capacity in amounts not exceed- such label and labeling. ing 55 milligrams per square foot of (v) Where tolerances are established cloth, whereby the amount of piperonyl on both raw agricultural commodities butoxide is equal to 10 times the and processed food made therefrom, the amount of pyrethrins in the formula- total residues of piperonyl butoxide in tion. Such treated bags are constructed or on the processed food shall not be with waxed paper liners and are to be greater than that permitted by the used only for food, dried that contain 4 larger of the two tolerances. percent fat or less. (3) Piperonyl butoxide may be safely (D) In two-ply bags consisting of cel- used in accordance with the following lophane/polyolefin sheets bound to- prescribed conditions: gether by an adhesive layer when it is (i) It is used or intended for use in incorporated in the adhesive. The combination with pyrethrins for con- treated sheets shall contain not more trol of insects: than 50 milligrams of piperonyl (A) On the outer ply of multiwall butoxide per square foot (538 milli- paper bags of 50 pounds or more capac- grams per square meter). Such treated ity in amounts not exceeding 60 milli- bags are to be used only for packaging grams per square foot. plum, prune, dried; grape, raisin; and (B) On cotton bags of 50 pounds or other fruit, dried and are to have a more capacity in amounts not exceed- maximum ratio of 3.12 milligrams of ing 55 milligrams per square foot of piperonyl butoxide per ounce of fruit cloth. Such treated bags are con- (0.10 milligram of piperonyl butoxide structed with waxed paper liners and per gram of product). are to be used only for feed, dried that (E) In food processing and food stor- contain 4 percent fat or less. age areas: Provided, That the food is (ii) It is used in combination with removed or covered prior to such use. pyrethrins, whereby the amount of (ii) It is used or intended for use in piperonyl butoxide is equal to 10 times combination with pyrethrins and N- the amount of pyrethrins in the formu- octylbicycloheptene dicarboximide for lation. Such treated bags are to be used insect control in accordance with 21 only for feed, dried. CFR 178.3730. (iii) A tolerance of 10 parts per mil- (iii) A tolerance of 10 parts per million is established for residues of lion is established for residues of piperonyl butoxide in or on: piperonyl butoxide when present as the (A) Grain, cereal, milled fractions result of migration: when present therein as a result of its (A) In or on feed, dried from its use use in cereal grain mills and in storage on the outer ply of multiwall paper areas for milled cereal grain products. bags of 50 pounds or more capacity. (B) Food, dried when present as a re- (B) In or on feed, dried that contain sult of migration from its use on the 4 percent fat, or less, from its use on outer ply of multiwall paper bags of 50 cotton bags of 50 pounds or more capac- pounds or more capacity. ity constructed with waxed paper lin- (C) Food treated in accordance with ers. 21 CFR 178.3730. (iv) To assure safe use of the pes- (D) Food, dried that contain 4 per- ticide, its label and labeling shall con- cent fat, or less, when present as a re- form to that registered with the U.S. sult of migration from its use on the Environmental Protection Agency. cloth of cotton bags of 50 pounds or (v) Where tolerances are established more capacity constructed with waxed on both the raw agricultural commod- paper liners. ities and food, processed made there- (E) Food treated in accordance with from, the total residues of piperonyl paragraph (a)(2)(i)(D) and (E) of this butoxide in or on the processed food section. shall not be greater than that per- (iv) To assure safe use of the pes- mitted by the larger of the two toler- ticide, its label and labeling shall con- ances. form to that registered with the U.S. (b) Section 18 emergency exemptions. Environmental Protection Agency, and [Reserved]

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(c) Tolerances with regional registra- Commodity Parts per tions. [Reserved] million (d) Indirect or inadvertent residues. Cotton, undelinted seed, postharvest ...... 1.0 [Reserved] Crabapple, postharvest ...... 1 .0 Currant, postharvest ...... 1 .0 [71 FR 74813, Dec. 13, 2006] Dewberry, postharvest ...... 1 .0 Fig, postharvest ...... 1 .0 § 180.128 Pyrethrins; tolerances for Flax, seed, postharvest ...... 1 .0 residues. Goat, fat ...... 1 .0 Goat, meat ...... 0.05 (a) General. (1) Tolerances for resi- Goat, meat byproducts ...... 0 .05 dues of the insecticide pyrethrins ((1S)- Gooseberry, postharvest ...... 1 .0 Grape, postharvest ...... 1 .0 2-methyl-4-oxo-3-(2Z)-2,4- Guava, postharvest ...... 1 .0 pentadienylcyclopenten-1-yl (1R,3R)- Hog, fat ...... 1 .0 2,2-dimethyl-3-(2-methyl-1-pro- Hog, meat ...... 0 .05 Hog, meat byproducts ...... 0 .05 penyl)cyclopropanecarboxylate (pyre- Horse, fat ...... 1 .0 thrin 1), (1S)-2-methyl-4-oxo-3-(2Z)-2,4- Horse, meat ...... 0 .05 pentadienyl-2-cyclopenten-1-yl (1R,3R)- Horse, meat byproducts ...... 0 .05 Loganberry, postharvest ...... 1 .0 3-[(1E)-3-methoxy-2-methyl-3-oxo-1-pro- Mango, postharvest ...... 1 .0 penyl]-2,2-dimethylcyclopropane- Milk, fat (reflecting negligible residues in milk) ... 0 .05 carboxylate (pyrethrin 2), (1S)-3-(2Z)-2- Muskmelon, postharvest ...... 1.0 Oat, grain, postharvest ...... 1 .0 butenyl-2-methyl-4-oxo-2-cyclopenten- Orange, postharvest ...... 1.0 1-yl (1R,3R)-2,2-dimethyl-3-(2-methyl-1- Pea, dry, seed, postharvest ...... 1 .0 propenyl)cyclopropanecarboxylate Peach, postharvest ...... 1.0 Peanut, postharvest ...... 1 .0 (cinerin 1), (1S)-3-(2Z)-2-butenyl-2- Pear, postharvest ...... 1.0 methyl-4-oxo-2-cyclopenten-1-yl Pineapple, postharvest ...... 1 .0 (1R,3R)-3-[(1E)-3-methoxy-2-methyl-3- Plum, prune, fresh, postharvest ...... 1 .0 Potato, postharvest ...... 0 .05 oxo-1-propenyl]-2,2- Raspberry, postharvest ...... 1.0 dimethylcyclopropanecarboxylate Rice, grain, postharvest ...... 3 .0 (cinerin 2), (1S)-2-methyl-4-oxo-3-(2Z)-2- Rye, grain, postharvest ...... 3 .0 Sheep, fat ...... 1 .0 pentenyl-2-cyclopenten-1-yl (1R, 3R)- Sheep, meat ...... 0.05 2,2-dimethyl-3-(2-methyl-1-pro- Sheep, meat byproducts ...... 0 .05 penyl)cyclopropanecarboxylate Sorghum, grain, grain, postharvest ...... 1.0 Sweet potato, postharvest ...... 0 .05 (jasmolin 1), and (1S)-2-methyl-4-oxo-3- Tomato, postharvest ...... 1 .0 (2Z)-pentenyl-2-cyclopenten-1-yl Walnut, postharvest ...... 1.0 (1R,3R)-3-[(1E)-3-methoxy-2-methyl-3- Wheat, grain, postharvest ...... 3 .0 oxo-1-propenyl]-2,2- dimethylcyclopropanecarboxylate (2) A tolerance of 1.0 ppm is estab- (jasmolin 2)), the insecticidally active lished for residues of the insecticide principles of Chrysanthemum pyrethrins in or on milled fractions de- cinerariaefolium, which are measured rived from grain, cereal when present as cumulative residues of pyrethrin 1, as a result of its use in cereal grain cinerin 1, and jasmolin 1 are not to ex- mills and in storage areas for milled ceed the following: cereal grain products. (3) A tolerance of 1.0 ppm is estab- Commodity Parts per lished for residues of the insecticide million pyrethrins in or on all food items in Almond, postharvest ...... 1 .0 food handling establishments where Apple, postharvest ...... 1 .0 food and food products are held, proc- Barley, grain, postharvest ...... 3 .0 Bean, succulent, postharvest ...... 1.0 essed, prepared and/or served. Food Birdseed, mixtures, postharvest ...... 3 .0 must be removed or covered prior to Blackberry, postharvest ...... 1 .0 use. Blueberry, postharvest ...... 1 .0 Boysenberry, postharvest ...... 1 .0 (4) Where tolerances are established Buckwheat, grain, postharvest ...... 3 .0 on both the raw agricultural commod- Cacao bean, roasted bean, postharvest ...... 1.0 ities and processed foods made there- Cattle, fat ...... 1.0 from, the total residues of pyrethrins Cattle, meat ...... 0 .05 Cattle, meat byproducts ...... 0.05 in or on the processed food shall not be Cherry, sweet, postharvest ...... 1 .0 greater than that permitted by the Cherry, tart, postharvest ...... 1 .0 larger of the two tolerances. Coconut, copra, postharvest ...... 1 .0 Corn, field, grain, postharvest ...... 3 .0 (b) Section 18 emergency exemptions. Corn, pop, grain, postharvest ...... 3 .0 [Reserved]

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(c) Tolerances with regional registra- § 180.132 Thiram; tolerances for resi- tions. [Reserved] dues. (d) Indirect or inadvertent residues. (a) General. Tolerances for residues of [Reserved] the fungicide thiram (tetramethyl [71 FR 74814, Dec. 13, 2006, as amended at 73 thiuram disulfide), including its me- FR 5108, Jan. 29, 2008] tabolites and degradates, in or on the commodities in the table below. Com- § 180.129 o-Phenylphenol and its so- pliance with the tolerance levels speci- dium salt; tolerances for residues. fied is to be determined by measuring (a) General. Tolerances are estab- only thiram. lished for combined residues of the fun- Parts per Expiration/ gicide o-phenylphenol and sodium o- Commodity million revocation phenylphenate, each expressed as o- date phenylphenol, from postharvest appli- Apple ...... 7.0 None cation of either in or on the following Banana1 ...... 0.80 3/31/15 Peach ...... 7.0 None food commodities: Strawberry ...... 20 None Parts per 1 No U.S. registrations as of September 23, 2009. Commodity million (b) Section 18 emergency exemptions. Apple ...... 25 [Reserved] Cantaloupe (NMT 10 ppm in edible portion) ...... 125 (c) Tolerances with regional registra- Carrot, roots ...... 20 tions. [Reserved] Cherry ...... 5 Citrus fruits ...... 10 (d) Indirect or inadvertent residues. Cucumber ...... 10 [Reserved] Lemon ...... 10 [67 FR 49615, July 31, 2002, as amended at 74 Nectarine ...... 5 FR 48391, Sept. 23, 2009; 79 FR 8301, Feb. 12, Orange ...... 10 2014; 79 FR 18822, Apr. 4, 2014] Pepper, bell ...... 10 Peach ...... 20 Pear ...... 25 .0 § 180.142 2,4-D; tolerances for residues. Pineapple ...... 10 (a) General. Tolerances are estab- Plum, prune, fresh ...... 20 lished for residues of the herbicide, Sweet potato, roots ...... 15 plant regulator, and fungicide 2,4-D, in- Tomato ...... 10 cluding its metabolites and degradates, (b) Section 18 emergency exemptions. in or on the commodities in the table [Reserved] below. Compliance with the tolerance levels is to be determined by meas- (c) Tolerances with regional registra- uring residues of 2,4-D (2,4- tions. [Reserved] dichlorophenoxyacetic acid), both free (d) Indirect or inadvertent residues. and conjugated, determined as the [Reserved] acid, in or on the following commod- [73 FR 54960, Sept. 24, 2008] ities:

Parts per § 180.130 Hydrogen Cyanide; toler- Commodity million ances for residues. Almond hulls ...... 0 .1 (a) General. A tolerance for residues Asparagus ...... 5.0 of the insecticide hydrogen cyanide Barley, bran ...... 4 .0 from postharvest fumigation as a re- Barley, grain ...... 2 .0 sult of application of sodium cyanide is Barley, straw ...... 50 Berry, group 13 ...... 0 .2 established as follows: 50 parts per mil- Cattle, fat ...... 0.3 lion in or on Fruit, citrus. Cattle, kidney ...... 4 .0 (b) Section 18 emergency exemptions. Cattle, meat ...... 0 .3 Cattle, meat byproducts, except kidney ...... 0.3 [Reserved] Corn, field, forage ...... 6 .0 (c) Tolerances with regional registra- Corn, field, grain ...... 0 .05 tions. [Reserved] Corn, field, stover ...... 50 Corn, pop, grain ...... 0.05 (d) Indirect or inadvertent residues. Corn, pop, stover ...... 50 [Reserved] Corn, sweet, forage ...... 6 .0 Corn, sweet, kernel plus cob with husks re- [64 FR 39077, July 21, 1999] moved ...... 0 .05

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below. Compliance with the tolerance Commodity Parts per million levels is to be determined by meas- Corn, sweet, stover ...... 50 uring residues of 2,4-D (2,4- Cranberry ...... 0 .5 dichlorophenoxyacetic acid), both free Fish ...... 0 .1 and conjugated, determined as the Fruit, citrus, group 10 ...... 3 .0 Fruit, pome, group 11 ...... 0.05 acid, in or on the follow commodities: Fruit, stone, group 12 ...... 0 .05 Goat, fat ...... 0 .3 Commodity Parts per Goat, kidney ...... 4 .0 million Goat, meat ...... 0.3 Rice, wild, grain ...... 0.05 Goat, meat byproducts, except kidney ...... 0 .3 Grain, aspirated fractions ...... 40 Grape ...... 0 .05 (d) Indirect or inadvertent residues. Grass, forage ...... 360 Tolerances are established for indirect Grass, hay ...... 300 Hop, dried cones ...... 0 .2 or inadvertent residues of the herbi- Horse, fat ...... 0 .3 cide, plant regulator, and fungicide 2,4- Horse, kidney ...... 4 .0 D, including its metabolites and Horse, meat ...... 0 .3 degradates, in or on the commodities Horse, meat byproducts, except kidney ...... 0 .3 Millet, forage ...... 25 in the table below. Compliance with Millet, grain ...... 2 .0 the tolerances levels is to be deter- Millet, straw ...... 50 mined by measuring residues of 2,4-D Milk ...... 0.05 Nut, tree, group 14 ...... 0 .2 (2,4-dichlorophenoxyacetic acid), both Oat, forage ...... 25 free and conjugated, determined as the Oat, grain ...... 2 .0 acid, in or on the following commod- Oat, straw ...... 50 Pistachio ...... 0.05 ities: Potato ...... 0 .4 Rice, grain ...... 0 .5 Parts per Commodity million Rice, hulls ...... 2 .0 Rice, straw ...... 10 Animal feed, nongrass, group 18 ...... 0 .2 Rye, bran ...... 4 .0 Avocado ...... 0 .05 Rye, forage ...... 25 Cotton, undelinted seed ...... 0 .05 Rye, grain ...... 2.0 Dill, seed ...... 0 .05 Rye, straw ...... 50 Okra ...... 0.05 Sheep, fat ...... 0 .3 Vegetable, brassica leafy, group 5 ...... 0 .4 Sheep, kidney ...... 4.0 Vegetable, bulb, group 3 ...... 0 .05 Sheep, meat ...... 0.3 Vegetable, cucurbit, group 9 ...... 0.05 Sheep, meat byproducts, except kidney ...... 0 .3 Vegetable, foliage of legume, group 7 ...... 0 .2 Shellfish ...... 1 .0 Vegetable, fruiting, group 8 ...... 0.05 Sorghum, grain, forage ...... 0.2 Vegetable, leafy, except brassica, group 4 ...... 0 .4 Sorghum, grain, grain ...... 0 .2 Vegetable, legume, group 6 ...... 0 .05 Sorghum, grain, stover ...... 0 .2 Soybean, forage ...... 0 .02 Soybean, hay ...... 2 .0 [72 FR 52017, Sept. 12, 2007, as amended at 73 Soybean, seed ...... 0 .02 FR 53737, Sept. 17, 2008; 74 FR 48411, Sept. 23, Strawberry ...... 0 .05 2009; 76 FR 55817, Sept. 9, 2011] Sugarcane, cane ...... 0.05 Sugarcane, molasses ...... 0 .2 Teff, bran ...... 4.0 § 180.145 Fluorine compounds; toler- Teff, forage ...... 25.0 ances for residues. Teff, grain ...... 2 .0 Teff, straw ...... 50 .0 (a) General. (1) Tolerances are estab- Vegetable, leaves of root and tuber, group 2 ..... 0 .1 lished for combined residues of the in- Vegetable, root and tuber, except potato, group secticidal fluorine compounds cryolite 1 ...... 0 .1 and synthetic cryolite (sodium alu- Wheat, bran ...... 4.0 Wheat, forage ...... 25 minum fluoride) in or on the following Wheat, grain ...... 2 .0 agricultural commodities: Wheat, straw ...... 50 Commodity Parts per (b) Section 18 emergency exemptions. million [Reserved] Apricot ...... 7 (c) Tolerances with regional registra- Blackberry ...... 7 tions. Tolerances with regional reg- Blueberry ...... 7 Boysenberry ...... 7 istration, as defined in § 180.1(l), are es- Broccoli ...... 7 tablished for residues of the herbicide, Brussels sprouts ...... 7 plant regulator, and fungicide 2,4-D, in- Cabbage ...... 7 Cauliflower ...... 7 cluding its metabolites and degradates, Collards ...... 7 in or on the commodities in the table Cranberry ...... 7

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Parts per Parts per Commodity million Commodity million

Cucumber ...... 7 Triticale, grain, postharvest ...... 40.0 Dewberry ...... 7 Vegetable, legume, group 6, postharvest ...... 70 Eggplant ...... 7 Wheat, bran, postharvest ...... 40 .0 Fruit, citrus ...... 7 Wheat, flour, postharvest ...... 125 .0 Grape ...... 7 Wheat, germ, postharvest ...... 130 .0 Kale ...... 7 Wheat, grain, postharvest ...... 40.0 Kohlrabi ...... 7 Wheat, milled byproducts, postharvest ...... 130.0 Lettuce, head ...... 7 Wheat, shorts, postharvest ...... 40.0 Lettuce, leaf ...... 7 Loganberry ...... 7 (b) Section 18 emergency exemptions. Melon ...... 7 Nectarine ...... 7 [Reserved] Peach ...... 7 (c) Tolerances with regional registra- Pepper ...... 7 tions. Tolerances with regional reg- Plum, prune, fresh ...... 7 istration, as defined by § 180.1(l), are es- Pumpkin ...... 7 Raspberry ...... 7 tablished for the combined residues of Squash, summer ...... 7 the insecticidal fluorine compounds, Squash, winter ...... 7 cryolite and synthetic cryolite (sodium Strawberry ...... 7 Tomato ...... 7 aluminum fluoride), in or on the fol- Youngberry ...... 7 lowing raw agricultural commodities:

Parts per (2) Tolerances are established for res- Commodity million idues of fluoride in or on the following commodities from the postharvest fu- Kiwifruit ...... 15 migation with sulfuryl fluoride for the control of insects: (d) Indirect or inadvertent residues. [Reserved] Parts per Commodity million [71 FR 74815, Dec. 13, 2006, as amended at 76 FR 34885, June 15, 2011] All processed food commodities not otherwise listed ...... 70 § 180.151 Ethylene oxide; tolerances Barley, bran, postharvest ...... 45 .0 for residues. Barley, flour, postharvest ...... 45.0 Barley, grain, postharvest ...... 15 .0 (a) General. (1) Tolerances are estab- Barley, pearled barley, postharvest ...... 45.0 lished for residues of the antimicrobial Cattle, meat, dried ...... 40 Cheese ...... 5 .0 agent and insecticide ethylene oxide, Cacao bean, roasted bean, postharvest ...... 20 when used as a postharvest fumigant in Coconut, postharvest ...... 40 or on the following food commodities: Coffee, bean, green, postharvest ...... 15 Corn, field, flour, postharvest ...... 35 .0 Parts per Corn, field, grain, postharvest ...... 10.0 Commodity million Corn, field, grits, postharvest ...... 10.0 Corn, field, meal, postharvest ...... 30 .0 Herb and spice, group 19, dried, except basil .... 7 Corn, pop, grain, postharvest ...... 10 .0 Licorice, roots ...... 7 Cotton, undelinted seed, postharvest ...... 70 Peppermint, tops, dried ...... 7 Egg, dried ...... 900 Sesame, seed ...... 7 Fruit, dried, except grape, raisin, postharvest ..... 3 .0 Spearmint, tops, dried ...... 7 Ginger, postharvest ...... 70 Vegetable, dried ...... 7 Grain, aspirated fractions, postharvest ...... 55 .0 Walnut ...... 50 Grape, raisin, postharvest ...... 7 .0 Hog, meat ...... 20 Herbs and spices group 19, postharvest ...... 70 (2) Tolerances are established for res- Milk, powdered ...... 5 .0 idues of the ethylene oxide reaction Millet, grain, postharvest ...... 40.0 product, 2-chloroethanol, commonly Nut, pine, postharvest ...... 20 referred to as ethylene chlorohydrin, Nut, tree, Group 14, postharvest ...... 10 .0 Oat, flour, postharvest ...... 75 .0 when ethylene oxide is used as a Oat, grain, postharvest ...... 25 .0 postharvest fumigant in or on food Oat, groats/rolled oats ...... 75 .0 commodities as follows: Peanut, postharvest ...... 15 Pistachio, postharvest ...... 10 .0 Commodity Parts per Rice, bran, postharvest ...... 31 .0 million Rice, flour, postharvest ...... 45 Rice, grain, postharvest ...... 12.0 Herb and spice, group 19, dried, except basil .... 940 Rice, hulls, postharvest ...... 35.0 Licorice, roots ...... 940 Rice, polished rice, postharvest ...... 25.0 Peppermint, tops, dried ...... 940 Rice, wild, grain, postharvest ...... 25 .0 Sesame, seed ...... 940 Sorghum, grain, postharvest ...... 40.0 Spearmint, tops, dried ...... 940

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(b) Section 18 emergency exemptions. Commodity Parts per million [Reserved] Vegetable, dried ...... 940 (c) Tolerances with regional registrations. Tolerances with regional reg- (b) Section 18 emergency exemptions. istration, as defined in § 180.1(l), are es- [Reserved] tablished for residues of the insecticide (c) Tolerances with regional registra- diazinon, O, O-diethyl O-[6-methyl-2-(1- tions. [Reserved] methylethyl)-4-pyrimidinyl]- (d) Indirect or inadvertent residues. phosphorothioate (CAS No. 333–41–5), in [Reserved] or on the following food commodities:

[65 FR 33695, May 24, 2000, as amended at 74 Commodity Parts per FR 46696, Sept. 11, 2009] million Almond ...... 0.50 § 180.153 Diazinon; tolerances for resi- Banana ...... 0.20 dues. Celery ...... 0 .70 Cucumber ...... 0 .75 (a) General. Tolerances are estab- Parsley, leaves ...... 0.75 lished for residues of the insecticide Parsnip ...... 0.50 diazinon, O,O-diethyl O-[6-methyl-2-(1- Pepper ...... 0 .5 Potato ...... 0 .10 methylethyl)-4- Squash, summer ...... 0 .50 pyrimidinyl]phosphorothioate (CAS Squash, winter ...... 0 .75 No. 333–41–5), in or on the following Sweet potato, roots ...... 0 .10 Swiss chard ...... 0.70 food commodities: Turnip, roots ...... 0 .50 Turnip, tops ...... 0.75 Parts per mil- Commodity lion (d) Indirect or inadvertent residues. Almond, hulls ...... 3 .0 [Reserved] Apple ...... 0.50 Apricot ...... 0 .20 [47 FR 42738, Sept. 29, 1982] Bean, lima ...... 0 .50 EDITORIAL NOTE: For FEDERAL REGISTER ci- Bean, snap, succulent ...... 0 .50 Beet, garden, roots ...... 0 .75 tations affecting § 180.153, see the List of CFR Beet, garden, tops ...... 0 .70 Sections Affected, which appears in the Blueberry ...... 0 .50 Finding Aids section of the printed volume Caneberry subgroup 13-07A ...... 0.75 and at www.fdsys.gov. Carrot, roots ...... 0.75 Cattle, fat ...... 0.50 § 180.154 Azinphos-methyl; tolerances Cherry, sweet ...... 0 .20 for residues. Cherry, tart ...... 0 .20 Cranberry ...... 0 .50 (a) General. Tolerances for residues of Endive ...... 0.70 the insecticide O,O-dimethyl S-[(4-oxo- Fig ...... 0 .50 1,2,3-benzotriazin-3(4H)- Ginseng ...... 0 .75 Grape ...... 0 .75 2 yl)methyl]phosphorodithioate in or on Hazelnut ...... 0 .50 the following raw agricultural com- Kiwifruit 1 ...... 0.75 modities: Lettuce ...... 0.70 Melon ...... 0 .75 Expiration/ 2 Parts per Mushroom ...... 0 .75 Commodity million Revocation Nectarine ...... 0 .20 Date Onion, bulb ...... 0 .75 1 Onion, green ...... 0 .75 Almond ...... 0.2 None 1 Pea, succulent ...... 0 .50 Almond, hulls ...... 5.0 None Apple2 ...... 1.5 None Peach ...... 0 .20 Blackberry3 ...... 2.0 None Pear ...... 0 .50 Blueberry2 ...... 5.0 None Pineapple ...... 0.50 Boysenberry3 ...... 2.0 None Plum, prune, fresh ...... 0.20 Brussels sprouts4 ...... 2.0 None Radish ...... 0 .50 Cherry2 ...... 2.0 None Rutabaga ...... 0 .75 Crabapple2 ...... 1.5 None Spinach ...... 0 .70 Cranberry3 ...... 0.5 12/31/12 Strawberry ...... 0 .50 Loganberry3 ...... 2.0 None Tomato ...... 0.75 Parsley, leaves2 ...... 5.0 None Vegetable, brassica, leafy, group 5 ...... 0.70 Parsley, turnip rooted, roots2 ...... 2.0 None Watercress ...... 0 .05 Peach3 ...... 2.0 None 2 1There are no domestic registrations for kiwifruit as of Pear ...... 1.5 None March 6, 2002. Pistachio1 ...... 0.3 None 2The expiration/revocation date for this tolerance is 9/10/ Plum, prune5 ...... 2.0 None 2010. Quince5 ...... 1.5 None

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Expiration/ § 180.163 Dicofol; tolerances for resi- Commodity Parts per Revocation million Date dues. (a) General. (1) Tolerances are estab- Raspberry3 ...... 2.0 None Walnut1 ...... 0.3 None lished for residues of the insecticide dicofol, including its metabolites and 1There are no U.S. registrations as of degradates, in or on the commodities October 30, 2009. in the table in this paragraph. Compli- 2There are no U.S. registrations as of ance with the tolerance levels specified September 30, 2012. in this paragraph is to be determined 3There are no U.S. registrations since by measuring only dicofol as the sum September 30, 2006. of its p,p-dicofol and o,p-dicofol iso- 4There are no U.S. registrations since mers: 4-chloro-a-(4-chlorophenyl)-a- September 30, 2008. (trichloromethyl)benzenemethanol and 5There are no U.S. registrations since 2-chloro-a-(4-chlorophenyl)-a- December 28, 2005. (trichloromethyl)benzenemethanol, in (b) Section 18 emergency exemptions. or on the commodity. [Reserved] Expiration/ (c) Tolerances with regional registra- Commodity Parts per revocation tions. [Reserved] million date (d) Indirect or inadvertent residues. Apple, wet pomace ...... 38.0 10/31/16 [Reserved] Bean, dry, seed ...... 0.5 10/31/16 Bean, succulent ...... 3.0 10/31/16 [65 FR 38752, June 22, 2000, as amended at 74 Butternut ...... 0.1 10/31/16 FR 46697, Sept. 11, 2009] Caneberry subgroup 13A ...... 5.0 10/31/16 Chestnut ...... 0.1 10/31/16 § 180.155 1-Naphthaleneacetic acid; tol- Citrus, dried pulp ...... 12.0 10/31/16 erances for residues. Citrus oil ...... 200.0 10/31/16 Cotton, refined oil ...... 0.5 10/31/16 (a) General. Tolerances are estab- Cotton, undelinted seed ...... 0.1 10/31/16 lished for the residues of 1- Fruit, citrus, group 10 ...... 6.0 10/31/16 Fruit, pome, group 11 ...... 10.0 10/31/16 naphthaleneacetic acid, including its Fruit, stone, group 12 ...... 5.0 10/31/16 metabolites and degradates in or on Grape ...... 5.0 10/31/16 the commodities in the following table. Grape, raisin ...... 20.0 10/31/16 Compliance with the tolerance levels Hazelnut ...... 0.1 10/31/16 Hop, dried cones ...... 65.0 10/31/16 specified is to be determined by meas- Nut, hickory ...... 0.1 10/31/16 uring only 1-naphthaleneacetic acid Nut, macadamia ...... 0.1 10/31/16 and its conjugates, calculated as the Pecan ...... 0.1 10/31/16 Peppermint, oil ...... 30.0 10/31/16 Stoichiometric equivalent of 1- Peppermint, tops ...... 25.0 10/31/16 naphthaleneacetic acid, in or on the Spearmint, oil ...... 30.0 10/31/16 commodity. Spearmint, tops ...... 25.0 10/31/16 Strawberry ...... 10.0 10/31/16 Parts per Tea, dried ...... 50.0 None Commodity million Tea, plucked leaves ...... 30.0 None Vegetable, cucurbit, group 9 ...... 2.0 10/31/16 Avocado ...... 0 .05 Vegetable, fruiting, group 8 ...... 2.0 10/31/16 Cherry, sweet ...... 0 .1 Walnut ...... 0.1 10/31/16 Fruit, pome, group 11–10 ...... 0 .15 Mango ...... 0.05 Olive ...... 0 .7 (2) Tolerances are established for res- Orange ...... 0 .1 idues of the insecticide dicofol, includ- Pineapple1 ...... 0 .05 ing its metabolites and degradates, in Potato ...... 0 .01 or on the commodities in the table in Rambutan ...... 2 .0 Sapote, mamey ...... 0 .05 this paragraph. Compliance with the Tangerine ...... 0 .1 tolerance levels specified in this para- 1 There are no U.S. registrations since 1988. graph is to be determined by measuring only the sum of p,p-dicofol, 4-chloro-a- (b) Section 18 emergency exemptions. (4-chlorophenyl)-a- [Reserved] (trichloromethyl)benzenemethanol, its (c) Tolerances with regional registra- isomer o,p-dicofol, 2-chloro-a-(4- tions. [Reserved] chlorophenyl)-a- (d) Indirect or inadvertent residues. (trichloromethyl)benzenemethanol, [Reserved] and its metabolites 4-chloro-a-(4- [78 FR 30218, May 22, 2013] chlorophenyl)-a- 448

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(dichloromethyl)benzenemethanol and Parts per Expiration/ 2-chloro- -(4-chlorophenyl)- - Commodity revocation a a million date (dichloromethyl)benzenemethanol, calculated as the stoichiometric equiva- Asparagus ...... 15 None lent of p,p-dicofol, 4-chloro- -(4- Banana ...... 5.0 None a Beet, sugar, roots ...... 0.5 None chlorophenyl)-a- Beet, sugar, tops ...... 25 None (trichloromethyl)benzenemethanol, in Bushberry subgroup 13-07B ...... 3.0 None or on the commodity. Cabbage ...... 21 None Cactus, fruit ...... 5.0 None Cactus, pads ...... 12 None Expiration/ Commodity Parts per Revocation Caneberry subgroup 13-07A ...... 12.0 None million Date Citrus, oil ...... 20 None Clover, forage ...... 50 None Cattle, fat ...... 50.0 10/31/16 Clover, hay ...... 70 None Cattle, liver ...... 5.0 10/31/16 Corn, field, forage ...... 30 None Cattle, meat ...... 3.0 10/31/16 Corn, field, grain ...... 0.02 None Cattle, meat byproducts, except Corn, field, stover ...... 20 None liver ...... 3.0 10/31/16 Corn, pop, grain ...... 0.02 None Egg ...... 0.05 10/31/16 Corn, pop, stover ...... 20 None Goat, fat ...... 50.0 10/31/16 Corn, sweet, forage ...... 185 None Goat, liver ...... 5.0 10/31/16 Corn, sweet, kernel plus cob with Goat, meat ...... 3.0 10/31/16 husks removed ...... 0.1 None Goat, meat byproducts, except liver 3.0 10/31/16 Corn, sweet, stover ...... 215 None Hog, fat ...... 50.0 10/31/16 Cotton, undelinted seed ...... 5.0 10/31/09 Hog, liver ...... 5.0 10/31/16 Cranberry ...... 3.0 None Hog, meat ...... 3.0 10/31/16 Dandelion, leaves ...... 22 None Hog, meat byproducts, except liver 3.0 10/31/16 Endive ...... 10 None Horse, fat ...... 50.0 10/31/16 Flax, seed ...... 0.5 None Horse, liver ...... 5.0 10/31/16 Fruit, citrus, group 10 ...... 10 None Horse, meat ...... 3.0 10/31/16 Fruit, pome, group 11 ...... 12 None Horse, meat byproducts, except Fruit, stone, group 12 ...... 10 None liver ...... 3.0 10/31/16 Grain, aspirated fractions ...... 70 None Milk, fat (reflecting 0.75 ppm in Grape ...... 10 None whole milk) ...... 22.0 10/31/16 Grape, raisin ...... 12 None Poultry, fat ...... 0.1 10/31/16 Grass, forage ...... 100 None Poultry, meat ...... 0.1 10/31/16 Grass, hay ...... 15 None Poultry, meat byproducts ...... 0.1 10/31/16 Leaf petiole subgroup 4B ...... 3.0 None Sheep, fat ...... 50.0 10/31/16 Lettuce ...... 10 None Sheep, liver ...... 5.0 10/31/16 Millet, proso, grain ...... 1.0 None Sheep, meat ...... 3.0 10/31/16 Millet, proso, straw ...... 20 None Sheep, meat byproducts, except Nut, tree group 14, except walnut ... 0.1 None liver ...... 3.0 10/31/16 Okra ...... 4.0 None Olive ...... 10 None (b) Section 18 emergency exemptions. Oyster ...... 0.25 None Parsley, leaves ...... 22 None [Reserved] Pea and bean, dried shelled, except (c) Tolerances with regional registra- soybean, subgroup 6C ...... 1.0 None tions. [Reserved] Peanut ...... 0.05 None Peanut, hay ...... 20 None (d) Indirect or inadvertent residues. Pineapple ...... 2.0 None [Reserved] Pistachio ...... 0.1 None Rice, grain ...... 15 None [63 FR 34826, June 26, 1998, as amended at 72 Rice, hulls ...... 30 None FR 35665, June 29, 2007; 72 FR 41928, Aug. 1, Rice, straw ...... 60 None 2007; 77 FR 59124, Sept. 26, 2012] Sorghum grain, forage ...... 30 None Sorghum grain, grain ...... 10 None § 180.169 Carbaryl; tolerances for resi- Sorghum grain, stover ...... 30 None dues. Soybean, forage ...... 15 None Soybean, hay ...... 15 None (a) General. (1) Tolerances are estab- Soybean, seed ...... 0.5 None lished for residues of the insecticide Spinach ...... 22 None Strawberry ...... 4.0 None carbaryl, 1-naphthyl N- Sunflower, seed ...... 0.5 None methylcarbamate per se, in or on the Sweet potato, roots ...... 0.2 None following food commodities: Trefoil, forage ...... 15 None Trefoil, hay ...... 25 None Vegetable, brassica, leafy, group 5, Parts per Expiration/ Commodity revocation except cabbage ...... 10 None million date Vegetable, cucurbit, group 9 ...... 3.0 None Vegetable, foliage of legume, sub- Alfalfa, forage ...... 50 None group 7A, except soybean ...... 60 None Alfalfa, hay ...... 75 None Vegetable, fruiting, group 8 ...... 5.0 None Almond, hulls ...... 50 None Vegetable, leaves of root and tuber, Apple, wet pomace ...... 15 None group 2, except sugar beet tops 75 None

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(d) Indirect or inadvertent residues. Parts per Expiration/ Commodity revocation [Reserved] million date [65 FR 33695, May 24, 2000, as amended at 66 Vegetable, legume, edible podded, subgroup 6A ...... 10 None FR 38955, July 26, 2001; 67 FR 49615, July 31, Vegetable, root and tuber, group 1, 2002; 70 FR 44492, Aug. 3, 2005; 73 FR 52611, except sugar beet and sweet po- Sept. 10, 2008; 74 FR 10490, Mar. 11, 2009] tato ...... 2.0 None Walnut ...... 1.0 None § 180.172 Dodine; tolerances for resi- Wheat, forage ...... 30 None dues. Wheat, grain ...... 1.0 None Wheat, hay ...... 30 None (a) General. Tolerances are estab- Wheat, straw ...... 20 None lished for residues of the fungicide dodine, including its metabolites and (2) Tolerances are established for res- degradates, in or on the commodities idues of the insecticide carbaryl, 1- listed in the table below. Compliance naphthyl N-methylcarbamate, includ- with the tolerance levels specified in ing its metabolites: 1-naphthol the table is to be determined by meas- (naphthyl-sulfate); 5,6- uring only dodine, N-dodecylguanidine dihydrodihydroxycarbaryl; and 5,6- acetate; in or on the following com- dihydrodihydroxy naphthol, calculated modities. as 1-naphthyl N-methylcarbamate and Parts per the free and conjugated residues of Commodity million carbaryl: 5,6-dihydro-5,6-dihydroxy carbaryl and 5-methoxy-6-hydroxy Almond, hull ...... 30 .0 carbaryl, in or on the following food Apple ...... 5.0 Apple, wet pomace ...... 15.0 commodities: Banana ...... 0.50 Fruit, stone, crop group 12 ...... 5 .0 Parts per Expiration/ Nuts, tree, crop group 14 ...... 0 .3 Commodity revocation Peanut ...... 0 .013 million date Pear ...... 5 .0 Strawberry ...... 5 .0 Cattle, fat ...... 0.5 None Cattle, meat ...... 1.0 None Cattle, meat byproducts ...... 3.0 None (b) Section 18 emergency exemptions. Egg ...... 0.5 10/31/09 [Reserved] Goat, fat ...... 0.5 None (c) Tolerances with regional registra- Goat, meat ...... 1.0 None tions. [Reserved] Goat, meat byproducts ...... 3.0 None Hog, fat ...... 0.5 None (d) Indirect or inadvertent residues. Hog, meat ...... 1.0 None [Reserved] Hog, meat byproducts ...... 3.0 None Horse, fat ...... 0.5 None [72 FR 52017, Sept. 12, 2007, as amended at 73 Horse, meat ...... 1.0 None FR 45634, Aug. 6, 2008; 77 FR 72237, Dec. 5, Horse, meat byproducts ...... 3.0 None 2012] Milk ...... 1.0 None Poultry, fat ...... 5.0 10/31/09 § 180.175 Maleic hydrazide; tolerances Poultry, meat ...... 5.0 10/31/09 for residues. Sheep, fat ...... 0.5 None Sheep, meat ...... 1.0 None (a) General. (1) Tolerances for resi- Sheep, meat byproducts ...... 3.0 None dues of the herbicide and plant regulator maleic hydrazide (1,2-dihydro-3,6- (b) Section 18 emergency exemptions. pyridazinedione) are established in or [Reserved] on the following raw agricultural com- (c) Tolerances with regional registra- modities: tions. Tolerances with regional reg- Parts per istrations, as defined in § 180.1(l), are Commodity million established for residues of the insecticide carbaryl, 1-naphthyl N- Onion, bulb ...... 15.0 Potato ...... 50.0 methylcarbamate per se, in or on the following food commodities: (2) A food additive known as maleic Parts per hydrazide (1,2-dihydro-3,6- Commodity million pyridazinedione) may be present in potato, chips when used in accordance Dillweed, fresh leaves ...... 0 .2 with the following conditions:

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(i) The food additive is present as a Commodity Parts per result of the application of a pesticide million formulation containing maleic hydra- Cherimoya ...... 3 .0 zide to the growing potato plant in ac- Corn, field, forage ...... 5 cordance with directions registered by Corn, field, grain ...... 0 .1 Corn, field, stover ...... 5 the U.S. Environmental Protection Corn, pop, grain ...... 0.5 Agency. Corn, pop, stover ...... 5 (ii) The label of the pesticide formu- Corn, sweet, forage ...... 5 Corn, sweet, kernel plus cob with husks re- lation containing the food additive moved ...... 0 .5 conforms to labeling registered by the Corn, sweet, stover ...... 5 U.S. Environmental Protection Agen- Cotton, undelinted seed ...... 0 .5 Crabapple ...... 10 cy. Cranberry ...... 7 (iii) The food additive is present in an Custard apple ...... 3 .0 amount not to exceed 160 parts per mil- Fennel ...... 10 lion by weight of the finished food. Ginseng ...... 1 .2 Goat, kidney ...... 0 .5 (b) Section 18 emergency exemptions. Goat, liver ...... 0.5 [Reserved] Grape ...... 7 (c) Tolerances with regional registra- Hog, kidney ...... 0.5 Hog, liver ...... 0 .5 tions. [Reserved] Horse, kidney ...... 0 .5 (d) Indirect or inadvertent residues. Horse, liver ...... 0 .5 [Reserved] Lettuce, head ...... 3.5 Lettuce, leaf ...... 18 [62 FR 64293, Dec. 5, 1997, as amended at 64 Mango ...... 15.0 FR 11792, Mar. 10, 1999; 67 FR 35048, May 17, Oat, bran ...... 20 2002] Oat, flour ...... 20 Oat, grain ...... 5 Oat, groats/rolled oats ...... 20 § 180.176 Mancozeb; tolerances for res- Oat, straw ...... 25 idues. Onion, bulb ...... 0 .5 (a) General. Tolerances are estab- Papaya (whole fruit with no residue present in the edible pulp after the peel is removed and lished for residues of mancozeb (a co- discarded) ...... 10 ordination product of zinc ion and Peanut ...... 0 .5 maneb (manganese Peanut, hay ...... 65 Pear ...... 10 ethylenebisdithiocarbamate)), includ- Pepper ...... 12 ing its metabolites and degradates, in Poultry, kidney ...... 0 .5 or on the commodities in the following Poultry, liver ...... 0 .5 Quince ...... 10 table. Compliance with the tolerance Rye, bran ...... 20 levels specified in this paragraph is to Rye, grain ...... 5 be determined by measuring only those Rye, straw ...... 25 mancozeb residues convertible to and Sapodilla ...... 15 .0 Sapote, mamey ...... 15 .0 expressed in terms of the degradate Sapote, white ...... 15 .0 carbon disulfide. Sheep, kidney ...... 0.5 Sheep, liver ...... 0.5 Parts per Star apple ...... 15 .0 Commodity million Sugar apple ...... 3 .0 Tangerine1 ...... 10 Almond ...... 0.1 Tomato ...... 4 Almond, hulls ...... 4 Vegetable, cucurbit, group 9 ...... 2.0 Apple ...... 7 Walnut ...... 0 .70 Asparagus (negligible residue) ...... 0 .1 Wheat, bran ...... 20 Atemoya ...... 3 .0 Wheat, flour ...... 20 Banana ...... 4.0 Wheat, germ ...... 20 Banana, pulp ...... 0 .5 Wheat, grain ...... 5 Barley, bran ...... 20 Wheat, middlings ...... 20 Barley, flour ...... 20 Wheat, shorts ...... 20 Barley, grain ...... 5 Wheat, straw ...... 25 Barley, pearled barley ...... 20 Barley, straw ...... 25 1 There are no U.S. registrations for use of mancozeb on Beet, sugar, roots ...... 2 tangerine. Beet, sugar, tops ...... 65 (b) Section 18 emergency exemptions. Broccoli ...... 7 Cabbage ...... 9 Time limited tolerances are estab- Canistel ...... 15 .0 lished in connection with use of the Carrot, roots ...... 2 pesticide under a section 18 emergency Cattle, kidney ...... 0 .5 Cattle, liver ...... 0 .5 exemption granted by EPA for residues Celery ...... 5 of mancozeb (a coordination product of

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zinc ion and maneb (manganese Commodity Parts per ethylenebisdithiocarbamate)), includ- million ing its metabolites and degradates, in Corn, sweet, forage ...... 70 or on the commodities in the following Corn, sweet, kernel plus cob with husks re- table. Compliance with the tolerance moved ...... 0 .1 Corn, sweet, stover ...... 40 levels specified in this paragraph is to Cotton, undelinted seed ...... 0 .5 be determined by measuring only those Crabapple ...... 0 .6 mancozeb residues convertible to and Cranberry ...... 5 Custard apple ...... 3 .0 expressed in terms of the degradate Fennel ...... 2.5 carbon disulfide. The tolerances will Flax, seed ...... 0 .15 expire and are revoked on the dates Ginseng ...... 1 .2 specified in the following table. Goat, kidney ...... 0 .5 Goat, liver ...... 0.5 Grape ...... 1 .5 Expiration/ Commodity Parts per Revocation Hog, kidney ...... 0.5 million Date Hog, liver ...... 0 .5 Horse, kidney ...... 0 .5 Ginseng ...... 2.0 12/31/10 Horse, liver ...... 0 .5 Walnut ...... 0.015 12/31/13 Lettuce, head ...... 3.5 Lettuce, leaf ...... 18 Mango ...... 15.0 (c) Tolerances with regional registra- Oat, flour ...... 20 tions. [Reserved] Oat, grain ...... 5 (d) Indirect or inadvertent residues. Oat, groats/rolled oats ...... 20 [Reserved] Oat, straw ...... 25 Onion, bulb ...... 1 .5 [65 FR 33708, May 24, 2000, as amended at 65 Papaya ...... 10 FR 49924, Aug. 16, 2000; 66 FR 64773, Dec. 14, Peanut ...... 0 .1 Peanut, hay ...... 65 2001; 68 FR 2247, Jan. 16, 2003; 69 FR 29458, Pear ...... 0 .6 May 24, 2004; 71 FR 76199, Dec. 20, 2006; 74 FR Pepper ...... 12 46372, Sept. 9, 2009; 75 FR 770, Jan. 6, 2010; 75 Potato ...... 0 .2 FR 50913, Aug. 18, 2010; 76 FR 18915, Apr. 6, Poultry, kidney ...... 0 .5 2011; 78 FR 44455, July 24, 2013] Poultry, liver ...... 0 .5 Quince ...... 0 .6 EFFECTIVE DATE NOTE: At 79 FR 27501, May Rice, grain ...... 0 .06 14, 2014, § 180.176 was amended by revising the Rye, bran ...... 20 table in paragraph (a) and revising para- Rye, grain ...... 5 graphs (b) and (c), effective Nov. 14, 2014. For Rye, straw ...... 25 Sapodilla ...... 15 .0 the convenience of the user, the revised text Sapote, mamey ...... 15 .0 is set forth as follows: Sapote, white ...... 15 .0 Sheep, kidney ...... 0.5 § 180.176 Mancozeb; tolerances for residues. Sheep, liver ...... 0.5 (a) * * * Sorghum, grain, forage ...... 0.15 Sorghum, grain, grain ...... 0 .25 Parts per Sorghum, grain, stover ...... 0 .15 Commodity million Star apple ...... 15 .0 Sugar apple ...... 3 .0 Almond ...... 0.1 Tangerine 1 ...... 10 Almond, hulls ...... 4 Tomato ...... 2.5 Apple ...... 0.6 Vegetable, cucurbit, group 9 ...... 2.0 Asparagus ...... 0.1 Walnut ...... 0 .70 Atemoya ...... 3 .0 Wheat, bran ...... 20 Banana ...... 2 Wheat, flour ...... 20 Barley, bran ...... 20 Wheat, germ ...... 20 Barley, flour ...... 20 Wheat, grain ...... 5 Barley, grain ...... 5 Wheat, middlings ...... 20 Barley, pearled barley ...... 20 Wheat, shorts ...... 20 Barley, straw ...... 25 Wheat, straw ...... 25 Beet, sugar, dried pulp ...... 3 .0 Beet, sugar, roots ...... 1 .2 1 There are no U.S. registrations for use of mancozeb on Beet, sugar, tops ...... 60 tangerine. Broccoli ...... 7 Cabbage ...... 9 (b) Section 18 emergency exemptions. [Re- Canistel ...... 15 .0 served] Cattle, kidney ...... 0 .5 (c) Tolerances with regional registrations. A Cattle, liver ...... 0 .5 tolerance with regional registrations, as de- Cherimoya ...... 3 .0 fined in § 180.1(l), is established for residues Corn, field, forage ...... 40 of the fungicide mancozeb, (a coordination Corn, field, grain ...... 0 .1 Corn, field, stover ...... 15 product of zinc ion and maneb (manganese Corn, pop, grain ...... 0.1 ethylenebisdithiocarbamate)), including its Corn, pop, stover ...... 40 metabolites and degradates, in or on the

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commodity in the following table in this Parts per paragraph. Compliance with the tolerance Commodity million levels specified in this paragraph is to be determined by measuring only those mancozeb Goat, fat ...... 0 .20 Goat, kidney ...... 0 .30 residues convertible to and expressed in Goat, meat ...... 0.06 terms of the degradate carbon disulfide. Goat, meat byproducts except kidney ...... 0 .06 Hog, fat ...... 0 .20 Commodity Parts per Hog, kidney ...... 0.30 million Hog, meat ...... 0 .06 Hog, meat byproducts except kidney ...... 0 .06 Carrot, roots ...... 1 Horse, fat ...... 0 .20 Horse, kidney ...... 0 .30 Horse, meat ...... 0 .06 * * * * * Horse, meat byproducts except kidney ...... 0.06 Milk ...... 0.30 Sheep, fat ...... 0 .20 § 180.178 Ethoxyquin; tolerances for Sheep, kidney ...... 0.30 residues. Sheep, meat ...... 0.06 (a) General. A tolerance is established Sheep, meat byproducts except kidney ...... 0 .06 for residues of the plant regulator (b) Section 18 emergency exemptions. ethoxyquin (1,2-dihydro-6-ethoxy-2,2,4- [Reserved] trimethylquinoline) from preharvest or (c) Tolerances with regional registra- postharvest use in or on the following tions. [Reserved] commodity: (d) Indirect or inadvertent residues. Parts per [Reserved] Commodity million [43 FR 52487, Nov. 13, 1978, as amended at 63 Pear ...... 3 FR 57073, Oct. 26, 1998; 72 FR 37653, July 11, 2007] (b) Section 18 emergency exemptions. [Reserved] § 180.182 Endosulfan; tolerances for (c) Tolerances with regional registra- residues. tions. [Reserved] (a)(1) General. Tolerances are estab- (d) Indirect or inadvertent residues. lished for residues of the insecticide [Reserved] endosulfan, including its metabolites [63 FR 57073, Oct. 26, 1998] and degradates, in or on the commodities in the table in this paragraph. § 180.181 Chlorpropham; tolerances for Compliance with the tolerance levels residues. specified in this paragraph is to be de- (a) General. (1) Tolerances are estab- termined by measuring only the sum of lished for residues of the plant regu- endosulfan, 6,7,8,9,10,10-hexachloro- lator and herbicide chlorpropham (iso- 1,5,5a,6,9,9a-hexahydro-6,9-methano- propyl m-chlorocarbanilate (CIPC) in 2,4,3-benzodioxathiepin 3-oxide (alpha or on the following food commodities: and beta isomers), and its metabolite endosulfan sulfate, 6,7,8,9,10,10- Commodity Parts per hexachloro-1,5,5a,6,9,9a-hexahydro-6,9- million methano-2,4,3-benzodioxathiepin-3,3-di- Potato ...... 30 oxide, calculated as the stoichiometric Potato, wet peel ...... 40 equivalent of endosulfan, in or on the commodity. (2) Tolerances are established for the combined residues of the plant regu- Expiration/ Commodity Parts per revocation lator and herbicide chlorpropham (iso- million date propyl m-chlorocarbanilate (CIPC) and its metabolite 4-hydroxychlorpropham- Almond ...... 0.3 7/31/12 Almond, hulls ...... 1.0 7/31/12 O-sulfonic acid (4-HSA) in or on the fol- Apricot ...... 2.0 7/31/12 lowing food commodities: Bean ...... 2.0 7/31/12 Broccoli ...... 3.0 7/31/12 Brussels sprouts ...... 2.0 7/31/12 Commodity Parts per million Cabbage ...... 4.0 7/31/12 Cantaloupe ...... 1.0 7/31/12 Cattle, fat ...... 0.20 Carrot, roots ...... 0.2 7/31/12 Cattle, kidney ...... 0 .30 Cattle, fat ...... 13.0 7/31/16 Cattle, meat ...... 0 .06 Cattle, liver ...... 5.0 7/31/16 Cattle, meat byproducts except kidney ...... 0 .06 Cattle, meat ...... 2.0 7/31/16

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Expiration/ Expiration/ Commodity Parts per revocation Commodity Parts per revocation million date million date

Cattle, meat byproducts, except Nut, macadamia ...... 0.2 7/31/12 liver ...... 1.0 7/31/16 Peach ...... 2.0 7/31/12 Cauliflower ...... 2.0 7/31/12 Pear ...... 2.0 7/31/13 Celery ...... 8.0 7/31/12 Pineapple ...... 1.0 7/31/16 Cherry, sweet ...... 2.0 7/31/12 Pineapple, process residue ...... 20.0 7/31/16 Cherry, tart ...... 2.0 7/31/12 Plum ...... 2.0 7/31/12 Collards ...... 2.0 7/31/12 Plum, prune ...... 2.0 7/31/12 Cotton, gin byproducts ...... 30.0 7/31/12 Sheep, fat ...... 13.0 7/31/16 Cotton, undelinted seed ...... 1.0 7/31/12 Sheep, liver ...... 5.0 7/31/16 Cucumber ...... 1.0 7/31/12 Sheep, meat ...... 2.0 7/31/16 Eggplant ...... 1.0 7/31/12 Sheep, meat byproducts, except Goat, fat ...... 13.0 7/31/16 liver ...... 1.0 7/31/16 Goat, liver ...... 5.0 7/31/16 Squash, summer ...... 1.0 7/31/12 Goat, meat ...... 2.0 7/31/16 Strawberry ...... 2.0 7/31/16 Goat, meat byproducts, except liver 1.0 7/31/16 Sweet potato, roots ...... 0.15 7/31/12 Hazelnut ...... 0.2 7/31/12 Walnut ...... 0.2 7/31/12 Hog, fat ...... 13.0 7/31/16 Watermelon ...... 1.0 7/31/12 Hog, liver ...... 5.0 7/31/16 Hog, meat ...... 2.0 7/31/16 Hog, meat byproducts, except liver 1.0 7/31/16 (2) A tolerance is established for the Horse, fat ...... 13.0 7/31/16 combined residues of the insecticide Horse, liver ...... 5.0 7/31/16 Horse, meat ...... 2.0 7/31/16 endosulfan, 6,7,8,9,10,10-hexachloro- Horse, meat byproducts, except 1,5,5a,6,9,9a-hexahydro-6,9-methano-2, liver ...... 1.0 7/31/16 4,3-benzodioxathiepin-3-oxide (alpha Kale ...... 2.0 7/31/12 and beta isomers), and its metabolite Lettuce, head ...... 11.0 7/31/12 Lettuce, leaf ...... 6.0 7/31/12 endosulfan sulfate, 6,7,8,9,10,10- Milk, fat ...... 2.0 7/31/16 hexachloro-1,5,5a,6,9,9a-hexahydro-6,9- Muskmelon ...... 1.0 7/31/12 methano-2, 4,3-benzodioxathiepin-3,3- Mustard greens ...... 2.0 7/31/12 Mustard, seed ...... 0.2 7/31/12 dioxide in or on the commodity in the Nectarine ...... 2.0 7/31/12 following table:

Expiration/ Commodity Parts per million revocation date

Tea, dried ...... 24 (reflecting less than 0.1 ppm in beverage tea) resulting from application of the insecticide 7/31/16 to growing tea.

(b) Section 18 emergency exemptions. lent of endosulfan, in or on the com- [Reserved] modity. (c) Tolerances with regional registra- Expiration/ tions. (1) Tolerances with regional reg- Parts per Commodity million revocation istration, as defined in § 180.1(l), are es- date tablished for residues of the insecticide Apple ...... 1.0 12/31/14 endosulfan, including its metabolites Apple, wet pomace ...... 5.0 12/31/14 and degradates, in or on the commod- Blueberry ...... 0.3 12/31/14 Corn, sweet, forage ...... 12.0 12/31/14 ities in the table in this paragraph, Corn, sweet, kernel plus cob with when endosulfan is used in the state of husks removed ...... 0.2 12/31/14 Florida. Compliance with the tolerance Corn, sweet, stover ...... 14.0 12/31/14 Pepper ...... 2.0 12/31/14 levels specified in this paragraph is to Potato ...... 0.2 12/31/14 be determined by measuring only the Pumpkin ...... 1.0 12/31/14 sum of endosulfan, 6,7,8,9,10,10- Squash, winter ...... 1.0 12/31/14 hexachloro-1,5,5a,6,9,9a-hexahydro-6,9- Tomato ...... 1.0 12/31/14 methano-2,4,3-benzodioxathiepin 3- (2) Tolerances with regional registra- oxide (alpha and beta isomers), and its tions. Tolerances with regional reg- metabolite endosulfan sulfate, istration, as defined in § 180.1(l), are es- 6,7,8,9,10,10-hexachloro-1,5,5a,6,9,9a- tablished for residues of the insecticide hexahydro-6,9-methano-2,4,3- endosulfan, including its metabolites benzodioxathiepin-3,3-dioxide, cal- and degradates, in or on the commod- culated as the stoichiometric equiva- ities in the table in this paragraph,

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when endosulfan is used in the United ygen analog sulfone, O,O-diethyl S-(2- States (except Florida). Compliance (ethylsulfonyl)ethyl) with the tolerance levels specified in phosphorothioate; calculated as the this paragraph is to be determined by stoichiometric equivalent of measuring only the sum of endosulfan, disulfoton, in or on the commodity. 6,7,8,9,10,10-hexachloro-1,5,5a,6,9,9a- hexahydro-6,9-methano-2,4,3- Expiration/ Commodity Parts per Revocation benzodioxathiepin 3-oxide (alpha and million Date beta isomers), and its metabolite endosulfan sulfate, 6,7,8,9,10,10- Bean, lima ...... 0.75 12/31/13 hexachloro-1,5,5a,6,9,9a-hexahydro-6,9- Bean, snap, succulent ...... 0.75 12/31/13 methano-2,4,3-benzodioxathiepin-3,3-di- Broccoli ...... 0.75 12/31/13 Brussels sprouts ...... 0.75 12/31/13 oxide, calculated as the stoichiometric Cabbage ...... 0.75 12/31/13 equivalent of endosulfan, in or on the Cauliflower ...... 0.75 12/31/13 commodity. Coffee, green bean ...... 0.2 6/30/14 Cotton, undelinted seed ...... 0.75 12/31/13 Parts per Expiration/ Lettuce, head ...... 0.75 12/31/14 Commodity revocation Lettuce, leaf ...... 2 12/31/14 million date Apple ...... 1.0 7/31/15 (b) Section 18 emergency exemptions. Apple, wet pomace ...... 5.0 7/31/15 Blueberry ...... 0.3 7/31/15 [Reserved] Corn, sweet, forage ...... 12.0 7/31/15 (c) Tolerances with regional registra- Corn, sweet, kernel plus cob with tions. A tolerance with regional reg- husks removed ...... 0.2 7/31/15 Corn, sweet, stover ...... 14.0 7/31/15 istration is established for residues of Pepper ...... 2.0 7/31/15 the insecticide disulfoton, O,O-diethyl Potato ...... 0.2 7/31/15 S-(2-(ethylthio)ethyl) Pumpkin ...... 1.0 7/31/15 Squash, winter ...... 1.0 7/31/15 phosphorodithioate, including its me- Tomato ...... 1.0 7/31/15 tabolites and degradates, in or on the commodity in the following table. (d) Indirect or inadvertent residues. Compliance with the tolerance levels [Reserved] specified in this paragraph is to be de- [65 FR 33696, May 24, 2000, as amended at 71 termined by measuring only the sum of FR 54433, Sept. 15, 2006; 76 FR 56653, Sept. 14, disulfoton, O,O-diethyl S-(2- 2011; 78 FR 8409, Feb. 6, 2013] (ethylthio)ethyl) phosphorodithioate, and its metabolites demeton-S, O,O- § 180.183 Disulfoton; tolerances for residues. diethyl S-(2-(ethylthio)ethyl) phosphorothioate; disulfoton sulfoxide, (a) General. Tolerances are estab- O,O-diethyl S-(2-(ethylsulfinyl)ethyl) lished for residues of the insecticide phosphorodithioate; disulfoton oxygen disulfoton, O,O-diethyl S-(2- analog sulfoxide, O,O-diethyl S-(2- (ethylthio)ethyl) phosphorodithioate, (ethylsulfinyl)ethyl) phosphorothioate, including its metabolites and degradates, in or on the commodities disulfoton sulfone, O,O-diethyl S-(2- in the following table. Compliance with (ethylsulfonyl)ethyl) the tolerance levels specified in this phosphorodithioate; and disulfoton ox- paragraph is to be determined by meas- ygen analog sulfone, O,O-diethyl S-(2- uring only the sum of disulfoton, O,O- (ethylsulfonyl)ethyl) diethyl S-(2-(ethylthio)ethyl) phosphorothioate; calculated as the phosphorodithioate, and its metabo- stoichiometric equivalent of lites demeton-S, O,O-diethyl S-(2- disulfoton, in or on the commodity. (ethylthio)ethyl) phosphorothioate; Expiration/ disulfoton sulfoxide, O,O-diethyl S-(2- Commodity Parts per Revocation (ethylsulfinyl)ethyl) million Date phosphorodithioate; disulfoton oxygen analog sulfoxide, O,O-diethyl S-(2- Asparagus ...... 0.1 12/31/13 (ethylsulfinyl)ethyl) phosphorothioate, disulfoton sulfone, O,O-diethyl S-(2- (ethylsulfonyl)ethyl) phosphorodithioate; and disulfoton ox-

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(d) Indirect or inadvertent residues. Commodity Parts per [Reserved] million [63 FR 2165, Jan. 14, 1998, as amended at 63 Parsnip, tops ...... 0 .05 FR 57073, Oct. 26, 1998; 66 FR 38955, July 26, Pea, dry, seed ...... 0 .09 2001; 67 FR 41806, June 19, 2002; 67 FR 49615, Rhubarb ...... 0 .5 Sheep, fat ...... 0 .2 July 31, 2002; 70 FR 44492, Aug. 3, 2005; 73 FR Sheep, kidney ...... 2.0 54960, Sept. 24, 2008; 74 FR 46697, Sept. 11, Sheep, liver ...... 2.0 2009; 75 FR 60240, Sept. 29, 2010] Sheep, meat ...... 0.1 Sheep, meat byproducts except kidney and liver 0 .1 § 180.184 Linuron; tolerances for resi- Sorghum, grain, forage ...... 1.0 dues. Sorghum, grain, grain ...... 0 .25 Sorghum, grain, stover ...... 1 .0 (a) General. Tolerances are estab- Soybean, seed ...... 1 .0 lished for residues of the herbicide Soybean, vegetable ...... 1 .0 linuron (3-(3,4-dichlorophenyl)-1- methoxy-1-methylurea), including its (b) Section 18 emergency exemptions. metabolites and degradates, in or on Time-limited tolerances are estab- the commodities in the table below. lished for residues of the herbicide Compliance with the tolerance levels linuron [3-(3,4-dichlorophenyl)-1- specified below is to be determined by methoxy-1-methylurea], including its measuring only those linuron residues metabolites and degradates, in or on convertible to 3,4-dichloroaniline, cal- the commodities in the table below, re- culated as the stoichiometric equiva- sulting from use of the pesticide pursu- lent of linuron, in or on the com- ant to FIFRA section 18 emergency ex- modity: emptions. Compliance with the tolerance levels specified below is to be de- Parts per termined by measuring only those Commodity million linuron residues convertible to 3.4- Asparagus ...... 7.0 dichloroaniline, calculated as the stoi- Carrot, roots ...... 1.0 chiometric equivalent of linuron, in or Cattle, fat ...... 0.2 Cattle, kidney ...... 2 .0 on the commodity. The tolerance ex- Cattle, liver ...... 2 .0 pires and is revoked on the date speci- Cattle, meat ...... 0 .1 fied in the table. Cattle, meat byproducts except kidney and liver 0 .1 Celeriac ...... 1.0 Expiration/ Cilantro, dried leaves ...... 10 Commodity Parts per revocation Cilantro, fresh leaves ...... 3 .0 million date Coriander, seed ...... 0 .01 Corn, field, forage ...... 1 .0 Lentil ...... 0.1 12/31/14 Corn, field, grain ...... 0 .1 Corn, field, stover ...... 6 .0 Corn, sweet, forage ...... 1 .0 (c) Tolerances with regional registra- Corn, sweet, kernel plus cob with husks re- tions. Tolerances with regional reg- moved ...... 0 .25 istrations, as defined in § 180.1(l), are Corn, sweet, stover ...... 6 .0 Cotton, gin byproducts ...... 5 .0 established for residues of the herbi- Cotton, undelinted seed ...... 0 .25 cide linuron (3-(3,4-dichlorophenyl)-1- Dill, oil ...... 2 .0 methoxy-1-methylurea), including its Dill, seed ...... 0 .5 metabolites and degradates, in or on Dillweed, dried leaves ...... 5 .0 Dillweed, fresh leaves ...... 1 .5 the commodities in the table below. Goat, fat ...... 0 .2 Compliance with the tolerance levels Goat, kidney ...... 2 .0 specified below is to be determined by Goat, liver ...... 2.0 Goat, meat ...... 0.1 measuring only those linuron residues Goat, meat byproducts except kidney and liver .. 0 .1 convertible to 3,4-dichloroaniline, cal- Hog, fat ...... 0 .05 culated as the stoichiometric equiva- Hog, meat ...... 0 .05 Hog, meat byproducts ...... 0 .1 lent of linuron, in or on the com- Horse, fat ...... 0 .2 modity. Horse, kidney ...... 2 .0 Horse, liver ...... 2 .0 Commodity Parts per Horse, meat ...... 0 .1 million Horse, meat byproducts except kidney and liver 0 .1 Horseradish ...... 0.05 Celery ...... 0 .5 Milk ...... 0.05 Potato ...... 0 .2 Parsley, dried leaves ...... 9 .0 Wheat, forage ...... 0 .5 Parsley, leaves ...... 4.0 Wheat, grain ...... 0 .05 Parsnip, roots ...... 0 .05 Wheat, hay ...... 0 .5

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its metabolites monomethyl Commodity Parts per million tetrachloroterephthalate acid (MTP) Wheat, straw ...... 2 .0 and terachlorophthalic acid (TCP) (calculated as DCPA) in or on the fol- (d) Indirect or inadvertent residues. lowing food commodities: [Reserved] Commodity Parts per [64 FR 41822, Aug. 2, 1999, as amended at 72 million FR 37653, July 11, 2007; 73 FR 51727, Sept. 5, Basil, dried leaves ...... 20.0 2008; 76 FR 81396, Dec. 28, 2011; 79 FR 8307, Basil, fresh leaves ...... 5 .0 Feb. 12, 2014] Bean, dry ...... 2.0 Bean, mung, seed ...... 2 .0 § 180.185 DCPA; tolerances for resi- Bean, snap, succulent ...... 2 .0 Celeriac ...... 2.0 dues. Chicory, roots ...... 2 .0 (a) General. Tolerances for the com- Chicory, tops ...... 5 .0 Chive ...... 5 .0 bined residues of the herbicide di- Coriander, leaves ...... 5 .0 methyl tetrachloroterephthalate Corn, field, forage ...... 0 .4 (DCPA) and its metabolites Corn, field, grain ...... 0 .05 Corn, field, stover ...... 0 .4 monomethyltetrachloroterephthalate Corn, pop, forage ...... 0 .4 (MTP) and tetrachloroterephthalic Corn, pop, grain ...... 0.05 acid (TCP) (calculated as dimethyl Corn, pop, stover ...... 0.4 Corn, sweet, forage ...... 0 .4 tetrachloroterephthalate) are estab- Corn, sweet, kernel plus cob with husks re- lished in or on the following food com- moved ...... 0 .05 modities: Corn, sweet, stover ...... 0 .4 Cotton, undelinted seed ...... 0 .2 Parts per Cucumber ...... 1 .0 Commodity million Dill ...... 5 .0 Eggplant ...... 1.0 Cantaloupe ...... 1 .0 Lettuce ...... 2.0 Garlic ...... 1 .0 Marjoram ...... 5 .0 Ginseng ...... 2 .0 Parsley, dried leaves ...... 20.0 Horseradish ...... 2.0 Parsley, leaves ...... 5.0 Muskmelon ...... 1 .0 Pea, blackeyed, seed ...... 2 .0 Onion, bulb ...... 1 .0 Pepper ...... 2 .0 Onion, green ...... 1 .0 Pimento ...... 2 .0 Strawberry ...... 2 .0 Potato ...... 2 .0 Tomato ...... 1.0 Radicchio ...... 5.0 Vegetable, brassica, leafy, group 5 ...... 5.0 Radish, oriental, roots ...... 2 .0 Watermelon ...... 1.0 Radish, oriental, tops ...... 2 .0 Rutabaga ...... 2 .0 Soybean ...... 2.0 (b) Section 18 emergency exemptions. Squash, summer ...... 1 .0 [Reserved] Squash, winter ...... 1 .0 (c) Tolerances with regional registra- Sweet potato ...... 2.0 Turnip, roots ...... 2 .0 tions. Tolerances with regional reg- Turnip, tops ...... 5.0 istration, as defined in § 180.1(l), are es- Yam, true, tuber ...... 2.0 tablished for the combined inadvertent residues of the herbicide dimethyl [72 FR 52018, Sept. 12, 2007, as amended at 73 tetrachloroterephthalate (DCPA) and FR 53737, Sept. 17, 2008; 73 FR 80302, Dec. 31, its metabolites monomethyl 2008; 74 FR 14744, Apr. 1, 2009] tetrachloroterephthalate acid (MTP) and terachlorophthalic acid (TCP) (cal- § 180.189 Coumaphos; tolerances for culated as DCPA) in or on the fol- residues. lowing food commodities: (a) General. Tolerances for residues of the insecticide coumaphos (O,O-diethyl Commodity Parts per O-3-chloro-4-methyl-2-oxo-2H-1- million benzopyran-7-yl phosphorothioate and Radish, roots ...... 2 .0 its oxygen analog (O,O-diethyl O-3- Radish, tops ...... 15 .0 chloro-4-methyl-2-oxo-2H-1- benzopyran-7-yl phosphate) in or on (d) Indirect or inadvertent residues. food commodities as follows: Tolerances are established for the combined indirect or inadvertent residues Commodity Parts per of the herbicide dimethyl million tetrachloroterephthalate (DCPA) and Cattle, fat ...... 1.0

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(d) Indirect or inadvertent residues. Commodity Parts per million [Reserved] Cattle, meat ...... 1 .0 [64 FR 25848, May 13, 1999, as amended at 66 Cattle, meat byproducts ...... 1.0 FR 63198, Dec. 5, 2001; 72 FR 16283, Apr. 4, Goat, fat ...... 1 .0 2007; 76 FR 34885, June 15, 2011] Goat, meat ...... 1.0 Goat, meat byproducts ...... 1 .0 Hog, fat ...... 1 .0 § 180.191 Folpet; tolerances for resi- Hog, meat ...... 1 .0 dues. Hog, meat byproducts ...... 1 .0 Honey ...... 0.15 (a) General. Tolerances are estab- Honeycomb ...... 45 .0 lished for the fungicide folpet (N- Horse, fat ...... 1 .0 (trichloromethylthio)phthalimide) in Horse, meat ...... 1 .0 or on raw agricultural commodities as Horse, meat byproducts ...... 1 .0 Milk, fat (=n in whole milk) ...... 0.5 follows: Sheep, fat ...... 1 .0 Sheep, meat ...... 1.0 Parts per Commodity million Sheep, meat byproducts ...... 1 .0 Apple 1 ...... 5.0 (b) Section 18 emergency exemptions. Cranberry 1 ...... 15 .0 [Reserved] Cucumber 1 ...... 2 .0 (c) Tolerances with regional registra- Grape 1 ...... 50 .0 Grape, raisin 1 ...... 80.0 tions. [Reserved] Hop, dried cones ...... 120 .0 (d) Indirect or inadvertent residues. Lettuce 1 ...... 50.0 [Reserved] Melon 1 ...... 3 .0 Onion,bulb 1 ...... 2 .0 [64 FR 39077, July 21, 1999, as amended at 65 Strawberry 1 ...... 5 .0 FR 49936, Aug. 16, 2000; 67 FR 46883, July 17, Tomato 1 ...... 25.0 2002; 69 FR 29458, May 24, 2004; 72 FR 28876, 1 No U.S. registrations. May 23, 2007] (b) Section 18 emergency exemptions. § 180.190 Diphenylamine; tolerances [Reserved] for residues. (c) Tolerances with regional registra- (a) General. Tolerances for residues of tions. Tolerances with regional reg- the plant regulator diphenylamine are istrations as defined in § 180.1(l) are es- established in or on the following com- tablished for the fungicide folpet (N- modities: (trichloromethylthio)phthalimide) in or on the following raw agricultural Parts per Commodity million commodity:

Apple, wet pomace ...... 30.0 Commodity Parts per Apple from preharvest or postharvest use, in- million cluding use of impregnated wraps ...... 10.0 Avocado ...... 25.0 Cattle, fat ...... 0.01 Cattle, liver ...... 0 .1 Cattle, meat byproducts, except liver ...... 0 .01 (d) Indirect or inadvertent residues. Cattle, meat ...... 0 .01 [Reserved] Goat, fat ...... 0 .01 Goat, liver ...... 0.1 [61 FR 37222, July 17, 1996, as amended at 68 Goat, meat byproducts, except liver ...... 0 .01 FR 10388, Mar. 5, 2003; 69 FR 52192, Aug. 25, Goat, meat ...... 0.01 2004; 72 FR 41928, Aug. 1, 2007] Horse, fat ...... 0 .01 Horse, liver ...... 0 .1 Horse, meat byproducts, except liver ...... 0 .01 § 180.198 Trichlorfon; tolerances for Horse, meat ...... 0 .01 residues. Milk ...... 0.01 (a) General. Tolerances are estab- Pear (post harvest) ...... 5 .0 Sheep, fat ...... 0 .01 lished for residues of the insecticide Sheep, liver ...... 0.1 trichlorfon (dimethyl (2,2,2-trichloro-1- Sheep, meat byproducts, except liver ...... 0 .01 hydroxyethyl) phosphonate) in or on Sheep, meat ...... 0.01 the following food commodities: (b) Section 18 emergency exemptions. Commodity Parts per [Reserved] million (c) Tolerances with regional registra- Cattle, fat 1 ...... 0.5 tions. [Reserved] Cattle, meat 1 ...... 0 .2

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inhibit embryonic root development in Commodity Parts per million or on the following food commodity: Cattle, meat byproducts 1 ...... 0.1 Commodity Parts per 1 There are no U.S. registrations for cattle commodities as million of June 24, 1999. Bean, mung, sprouts ...... 0.2 (b) Section 18 emergency exemptions. [Reserved] (b) Section 18 emergency exemptions. (c) Tolerances with regional registra- [Reserved] tions. [Reserved] (c) Tolerances with regional registra- (d) Indirect or inadvertent residues. tions. [Reserved] [Reserved] (d) Indirect or inadvertent residues. [72 FR 54578, Sept. 26, 2007] [Reserved] [68 FR 39439, July 1, 2003, as amended at 71 § 180.200 Dicloran; tolerances for resi- FR 56398, Sept. 27, 2006] dues. (a) General. Tolerances are estab- § 180.204 Dimethoate; tolerances for lished for residues of the fungicide residues. dicloran, including its metabolites and (a) General. Tolerances are estab- degradates, in or on the commodities lished for total residues of the insecti- in the table in this paragraph. Compli- cide dimethoate (O,O-dimethyl S-(N- ance with the tolerance levels specified methylcarbamoylmethyl) in this paragraph is to be determined phosphorodithioate) including its oxy- by measuring only dicloran, 2,6- gen analog (O,O-dimethyl S-(N- dichloro-4-nitroaniline, in or on the methylcarbamoylmethyl) commodity. phosphorothioate) in or on the following food commodities: Parts per Expiration/ Commodity million revocation Parts per date Commodity million

Apricot ...... 20 None Alfalfa, forage ...... 2.0 Bean, snap, succulent ...... 20 None Alfalfa, hay ...... 2.0 Carrot, roots ...... 10 11/2/11 Bean, dry, seed ...... 2 .0 Celery ...... 15 None Bean, lima ...... 2 .0 Cherry, sweet ...... 20 None Bean, snap, succulent ...... 2 .0 Cucumber ...... 5 None Blueberry 1 ...... 1 .0 Endive ...... 10 None Broccoli ...... 2 .0 Garlic ...... 5 None Cattle, meat byproducts ...... 0.02 Grape ...... 10 None Cauliflower ...... 2 .0 Lettuce ...... 10 None Celery ...... 2 .0 Nectarine ...... 20 None Citrus, dried pulp ...... 5 .0 Onion ...... 10 None Corn, field, forage ...... 1 .0 Peach ...... 20 None Corn, field, grain ...... 0 .1 Plum, prune, fresh ...... 15 None Corn, field, stover ...... 1 .0 Potato ...... 0.25 12/31/14 Corn, pop, grain ...... 0.1 Rhubarb ...... 10 None Corn, pop, stover ...... 1.0 Sweet potato, roots ...... 10 None Corn, sweet, forage ...... 1 .0 Tomato ...... 5 None Cotton, undelinted seed ...... 0 .1 Egg ...... 0 .02 (b) Section 18 emergency exemptions. Endive ...... 2.0 Goat, meat byproducts ...... 0 .02 [Reserved] Grapefruit ...... 2 .0 (c) Tolerances with regional registra- Hog, meat byproducts ...... 0 .02 tions. [Reserved] Horse, meat byproducts ...... 0 .02 Kale ...... 2 .0 (d) Indirect or inadvertent residues. Lemon ...... 2.0 [Reserved] Lettuce, leaf ...... 2 .0 Melon ...... 1 .0 [77 FR 40815, July 11, 2012] Milk ...... 0.002 Mustard greens ...... 2.0 § 180.202 p-Chlorophenoxyacetic acid; Orange ...... 2 .0 tolerances for residues. Pea ...... 2 .0 Pear ...... 2 .0 (a) General. A tolerance is established Pecan ...... 0 .1 for the combined residues of the plant Pepper ...... 2 .0 Potato ...... 0 .2 regulator p-chlorophenoxyacetic acid Poultry, meat byproducts ...... 0.02 and its metabolite p-chlorophenol to Safflower, seed ...... 0 .1

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Parts per Parts per Commodity million Commodity million

Sheep, meat byproducts ...... 0 .02 Barley, hay ...... 3 .5 Sorghum, grain, forage ...... 0.1 Barley, straw ...... 1 .0 Sorghum, grain, grain ...... 0 .1 Beet, sugar, roots ...... 0 .5 Sorghum, grain, stover ...... 0 .1 Beet, sugar, tops ...... 0.05 Soybean, forage ...... 2 .0 Berry group 13 ...... 0 .05 Soybean, hay ...... 2 .0 Biriba ...... 0 .05 Soybean, seed ...... 0 .05 Cacao bean, bean ...... 0 .05 Swiss chard ...... 2.0 Canistel ...... 0 .05 Tangerine ...... 2 .0 Carrot, roots ...... 0.05 Tomato ...... 2.0 Cattle, fat ...... 0.05 Turnip, roots ...... 0 .2 Cattle, kidney ...... 0 .5 Turnip, tops ...... 2.0 Cattle, meat ...... 0 .05 Wheat, forage ...... 2 .0 Cattle, meat byproducts, except kidney ...... 0.05 Wheat, grain ...... 0 .04 Cherimoya ...... 0 .05 Wheat, hay ...... 2 .0 Coffee, bean, green ...... 0 .05 Wheat, straw ...... 2 .0 Corn, field, forage ...... 3 .0 Corn, field, grain ...... 0 .1 1 There are U.S. registrations as of August 16, 1996. Corn, field, stover ...... 10 .0 Corn, pop, grain ...... 0.1 (b) Section 18 emergency exemptions. Corn, pop, stover ...... 10.0 [Reserved] Corn, sweet, kernel plus cob with husks re- (c) Tolerances with regional registra- moved ...... 0 .05 tions. Tolerances with regional reg- Cotton, gin byproducts ...... 110.0 Cotton, undelinted seed ...... 3 .5 istration, as defined in § 180.1(l), are es- Cowpea, forage ...... 0 .1 tablished for total residues of Cowpea, hay ...... 0 .4 dimethoate including its oxygen analog Cranberry ...... 0 .05 Custard apple ...... 0 .05 in or on the following food commod- Egg ...... 0 .01 ities: Endive ...... 0.05 Feijoa ...... 0 .05 Fig ...... 0 .05 Commodity Parts per million Fruit, citrus, group 10 ...... 0 .05 Fruit, pome, group 11 ...... 0.05 Asparagus ...... 0.15 Fruit, stone, group 12 ...... 0 .05 Brussels sprouts ...... 5 .0 Ginger ...... 0 .1 Cherry, sweet ...... 2 .0 Goat, fat ...... 0 .05 Cherry, tart ...... 2 .0 Goat, kidney ...... 0 .5 Goat, meat ...... 0.05 (d) Indirect or inadvertent residues. Goat, meat byproducts, except kidney ...... 0 .05 Grain, aspirated fractions ...... 65.0 [Reserved] Grape ...... 0 .05 [65 FR 33697, May 24, 2000, as amended at 69 Grass, forage ...... 90 .0 Grass, hay ...... 40 .0 FR 6567, Feb. 11, 2004; 73 FR 53737, Sept. 17, Guar, seed ...... 0.5 2008] Guava ...... 0 .05 Hog, fat ...... 0 .05 § 180.205 Paraquat; tolerances for resi- Hog, kidney ...... 0.5 dues. Hog, meat ...... 0 .05 Hog, meat byproducts, except kidney ...... 0 .05 (a) General. Tolerances are estab- Hop, dried cones ...... 0 .5 lished for residues of the desiccant, de- Horse, fat ...... 0 .05 ′ Horse, kidney ...... 0 .5 foliant, and herbicide paraquat (1,1 -di- Horse, meat ...... 0 .05 methyl-4,4′-bipyridinium-ion) derived Horse, meat byproducts, except kidney ...... 0 .05 from application of either the Ilama ...... 0 .05 bis(methyl sulfate) or the dichloride Jaboticaba ...... 0 .05 Kiwifruit ...... 0.05 salt (both calculated as the cation) in Lentil, seed ...... 0 .3 or on the following food commodities: Lettuce ...... 0.05 Longan ...... 0 .05 Parts per Lychee ...... 0 .05 Commodity million Mango ...... 0.05 Milk ...... 0.01 Acerola ...... 0.05 Nut, tree, group 14 ...... 0 .05 Almond, hulls ...... 0 .5 Okra ...... 0.05 Animal feed, nongrass, group 18, forage ...... 75 .0 Olive ...... 0 .05 Animal feed, nongrass, group 18, hay ...... 210.0 Onion, bulb ...... 0 .1 Artichoke, globe ...... 0.05 Onion, green ...... 0 .05 Asparagus ...... 0.5 Papaya ...... 0 .05 Atemoya ...... 0 .05 Passionfruit ...... 0 .2 Avocado ...... 0 .05 Pawpaw ...... 0 .05 Banana ...... 0.05 Pea and bean, dried shelled, except soybean, Barley, grain ...... 0 .05 subgroup 6C, except guar bean ...... 0 .3

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Parts per Parts per Commodity million Commodity million

Pea and bean, succulent shelled, subgroup 6B 0 .05 Cassava ...... 0.05 Pea, field, hay ...... 0.8 Pea, pigeon, seed ...... 0 .05 Pea, field, vines ...... 0 .2 Tanier ...... 0 .05 Peanut ...... 0 .05 Taro, corm ...... 0 .1 Peanut, hay ...... 0.5 Tyfon ...... 0 .05 Peppermint, tops ...... 0 .5 Yam, true, tuber ...... 0.05 Persimmon ...... 0 .05 Pineapple ...... 0.05 Pineapple, process residue ...... 0 .25 (d) Indirect or inadvertent residues. Pistachio ...... 0.05 [Reserved] Pomegranate ...... 0 .05 Potato ...... 0 .5 [46 FR 51614, Oct. 21, 1981] Pulasan ...... 0 .05 Rambutan ...... 0 .05 EDITORIAL NOTE: For FEDERAL REGISTER ci- Rhubarb ...... 0 .05 tations affecting § 180.205, see the List of CFR Rice, grain ...... 0 .05 Sections Affected, which appears in the Rice, straw ...... 0 .06 Finding Aids section of the printed volume Safflower, seed ...... 0 .05 and at www.fdsys.gov. Sapodilla ...... 0 .05 Sapote, black ...... 0 .05 Sapote, mamey ...... 0 .05 § 180.206 Phorate; tolerances for resi- Sapote, white ...... 0 .05 dues. Sheep, fat ...... 0 .05 (a) General. Tolerances are estab- Sheep, kidney ...... 0.5 Sheep, meat ...... 0.05 lished for the combined residues of the Sheep, meat byproducts, except kidney ...... 0 .05 insecticide phorate (O,O-diethyl S Sorghum, forage, forage ...... 0 .1 (ethylthio) meth- Sorghum, grain, forage ...... 0.1 yl]phosphorodithioate), phorate sulf- Sorghum, grain, grain ...... 0 .05 oxide, phorate sulfone, phorate oxygen Soursop ...... 0 .05 Soybean, forage ...... 0 .4 analog, phorate oxygen analog sulf- Soybean, hay ...... 10 .0 oxide, and phorate oxygen analog Soybean, hulls ...... 4 .5 sulfone in or on the following food Soybean, seed ...... 0 .7 commodities: Spanish lime ...... 0 .05 Spearmint, tops ...... 0 .5 Parts per Star apple ...... 0 .05 Commodity million Starfruit ...... 0 .05 Strawberry ...... 0 .25 Bean, dry, seed ...... 0 .05 Sugar apple ...... 0 .05 Bean, succulent ...... 0 .05 Sugarcane, cane ...... 0.5 Beet, sugar, roots ...... 0 .3 Sugarcane, molasses ...... 3 .0 Beet, sugar, tops ...... 3.0 Sunflower, seed ...... 2.0 1 Turnip, greens ...... 0.05 Coffee, green bean ...... 0 .02 Turnip, roots ...... 0 .05 Corn, field, forage ...... 0 .5 Vegetable, brassica, leafy, group 5 ...... 0.05 Corn, field, grain ...... 0 .05 Vegetable, cucurbit, group 9 ...... 0.05 Corn, sweet, forage ...... 0 .5 Vegetable, fruiting, group 8 ...... 0.05 Corn, sweet, kernel plus cob with husks re- Vegetable, legume, edible podded, subgroup 6A 0 .05 moved ...... 0 .05 Wax jambu ...... 0 .05 Cotton, undelinted seed ...... 0 .05 Wheat, forage ...... 0 .5 Hop, dried cones ...... 2 .0 Wheat, grain ...... 1 .1 Peanut ...... 0 .1 Wheat, hay ...... 3 .5 Potato ...... 0 .2 Wheat, straw ...... 50 .0 Sorghum, grain, grain ...... 0 .05 Sorghum, grain, stover ...... 0 .1 (b) Section 18 emergency exemptions. Soybean, seed ...... 0 .05 [Reserved] Sugarcane, cane ...... 0.05 (c) Tolerances with regional registra- Wheat, forage ...... 1 .5 tions. Tolerances with regional reg- Wheat, grain ...... 0 .05 istration as defined in § 180.1(l), are es- Wheat, hay ...... 1 .5 Wheat, straw ...... 0 .05 tablished for residues of the pesticide paraquat (1,1′-dimethyl-4,4′ 1 There are no U.S. registrations as of September 1, 1993 for the use of phorate on the growing crop, coffee. bipyridinium ion) derived from application of either the bis(methyl sulfate) or (b) Section 18 emergency exemptions. the dichloride salt (both calculated as [Reserved] the cation) in or on the following food (c) Tolerances with regional registra- commodities: tions. [Reserved]

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(d) Indirect or inadvertent residues. (c) Tolerances with regional registra- [Reserved] tions. [Reserved] (d) Indirect or inadvertent residues. [58 FR 62038, Nov. 24, 1993, as amended at 63 FR 2165, Jan. 14, 1998; 63 FR 57074, Oct. 26, [Reserved] 1998; 66 FR 50833, Oct. 5, 2001; 67 FR 49616, [45 FR 42619, June 25, 1980, as amended at 45 July 31, 2002; 71 FR 74816, Dec. 13, 2006; 73 FR FR 56346, Aug. 25, 1980; 45 FR 86493, Dec. 31, 53738, Sept. 17, 2008] 1980; 46 FR 37250, July 20, 1981; 47 FR 13524, Mar. 31, 1982; 47 FR 20309, May 12, 1982; 63 FR § 180.207 Trifluralin; tolerances for 57074, Oct. 26, 1998; 64 FR 39082, July 21, 1999; residues. 70 FR 21643, Apr. 27, 2005; 71 FR 54433, Sept. (a) General. Tolerances are estab- 15, 2006; 78 FR 46274, July 31, 2013] lished for residues of trifluralin, including its metabolites and degradates, § 180.208 Benfluralin; tolerances for residues. in or on the commodities in the following table. Compliance with the tol- (a) General. Tolerances are estab- erance levels specified in the following lished for residues of the herbicide table is to be determined by only benfluralin, N-butyl-N-ethyl-aaa- trifluralin a,a,a-trifluoro-2,6-dinitro- trifluoro-2,6-dinitro-p-toluidine, in or N,N-dipropyl-p-toluidine, in or on the on the following food commodities: commodity. Parts per Commodity million Commodity Parts per million Alfalfa, forage ...... 0.05 Alfalfa, hay ...... 0.05 Alfalfa, forage ...... 3.0 Clover, forage ...... 0.05 Alfalfa, hay ...... 2.0 Clover, hay ...... 0.05 Almond, hulls ...... 0 .05 Lettuce ...... 0.05 Asparagus ...... 0.05 Trefoil, forage ...... 0 .05 Barley, grain ...... 0 .05 Trefoil, hay ...... 0 .05 Barley, hay ...... 0 .05 Barley, straw ...... 0 .05 Bean, mung, sprouts ...... 2.0 (b) Section 18 emergency exemptions. Carrot, roots ...... 1.0 [Reserved] Celery ...... 0 .05 Corn, field, forage ...... 0 .05 (c) Tolerances with regional registra- Corn, field, grain ...... 0 .05 tions. [Reserved] Corn, field, stover ...... 0 .05 (d) Indirect or inadvertent residues. Cotton, gin byproducts ...... 0 .05 [Reserved] Endive ...... 0.05 Fruit, citrus, group 10 ...... 0 .05 [68 FR 39439, July 1, 2003, as amended at 73 Fruit, stone, group 12 ...... 0 .05 FR 52613, Sept. 10, 2008] Grape ...... 0 .05 Hop, dried cones ...... 0 .05 Nut, tree, group 14 ...... 0 .05 § 180.209 Terbacil; tolerances for resi- Oilseed, crop group 20 ...... 0 .05 dues. Okra ...... 0.05 Peanut ...... 0 .05 (a) General. Tolerances are estab- Peanut, hay ...... 0.05 lished for combined residues of the her- Peppermint, oil ...... 2 .0 bicide terbacil, (3-tert-butyl-5-chloro-6- Peppermint, tops ...... 0 .05 Sorghum, grain, forage ...... 0.05 methyluracil) and its metabolites [3- Sorghum, grain, grain ...... 0 .05 tert-butyl-5-chloro-6- Sorghum, grain, stover ...... 0 .05 hydroxymethyluracil], [6-chloro-2,3- Spearmint, oil ...... 2 .0 dihydro-7-hydroxymethyl 3,3-dimethyl- Spearmint, tops ...... 0 .05 Sugarcane, cane ...... 0.05 5H-oxazolo(3,2-a) pyrimidin-5-one], and Vegetable, brassica, leafy group 5 ...... 0 .05 [6-chloro-2,3-dihydro-3,3,7-trimethyl- Vegetable, bulb, group 3 ...... 0 .05 5H-oxazolo(3,2-a) pyrimidin-5-one], cal- Vegetable, cucurbit, group 9 ...... 0.05 Vegetable, foliage of legume, group 7 ...... 0 .05 culated as terbacil, in or on the fol- Vegetable, fruiting, group 8 ...... 0.05 lowing raw agricultural commodities: Vegetable, leaves of root and tuber, group 2 ..... 0 .05 Vegetable, legume, group 6 ...... 0 .05 Commodity Parts per Vegetable, root and tuber, group 1, except car- million rot ...... 0 .05 Wheat, grain ...... 0 .05 Alfalfa, forage ...... 1.0 Wheat, straw ...... 0 .05 Alfalfa, hay ...... 2.0 Apple ...... 0.3 Asparagus ...... 0.4 (b) Section 18 emergency exemptions. Blueberry ...... 0 .2 [Reserved] Caneberry subgroup 13A ...... 0 .2

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Parts per Parts per Commodity million Commodity million

Peach ...... 0 .2 Hog, fat ...... 0 .02 Peppermint, tops ...... 2 .0 Hog, meat ...... 0 .02 Spearmint, tops ...... 2 .0 Hog, meat byproducts ...... 0 .02 Strawberry ...... 0 .1 Horse, fat ...... 0 .05 Sugarcane, cane ...... 0.4 Horse, kidney ...... 0 .2 Watermelon ...... 1.0 Horse, meat ...... 0 .02 Horse, meat byproducts, except kidney ...... 0 .05 (b) Section 18 emergency exemptions. Milk ...... 0.02 [Reserved] Sheep, fat ...... 0 .05 (c) Tolerances with regional registra- Sheep, kidney ...... 0.2 Sheep, meat ...... 0.02 tions. [Reserved] Sheep, meat byproducts, except kidney ...... 0 .05 (d) Indirect or inadvertent residues. Sorghum, forage, forage ...... 8 .0 [Reserved] Sorghum, grain, forage ...... 8.0 Sorghum, grain, grain ...... 0 .25 [71 FR 30818, May 31, 2006] Sorghum, grain, stover ...... 12 .0

§ 180.210 Bromacil; tolerances for resi- (b) Section 18 emergency exemptions. dues. [Reserved] (a) General. Tolerances are estab- (c) Tolerances with regional registra- lished for residues of the herbicide tions. [Reserved] bromacil (5-bromo-3-sec-butyl-6- (d) Indirect or inadvertent residues. methyluracil) in or on the following [Reserved] food commodities: [47 FR 25959, June 16, 1982, as amended at 47 FR 28381, June 30, 1982; 47 FR 28626, July 1, Commodity Parts per million 1982; 47 FR 46701, Oct. 20, 1982; 63 FR 57074, Oct. 26, 1998; 72 FR 53454, Sept. 19, 2007] Fruit, citrus ...... 0 .1 Pineapple ...... 0.1 § 180.212 S-Ethyl cyclohexylethylthio- (b) Section 18 emergency exemptions. carbamate; tolerances for residues. [Reserved] (a) General. Tolerances are estab- (c) Tolerances with regional registra- lished for residues of the herbicide S- tions. [Reserved] ethyl cyclohexylethylthiocarbamate in (d) Indirect or inadvertent residues. or on the following food commodities: [Reserved] Commodity Parts per [68 FR 39439, July 1, 2003] million

§ 180.211 Propachlor; tolerances for Beet, garden, roots ...... 0 .05(N) Beet, garden, tops ...... 0 .05(N) residues. Beet, sugar, roots ...... 0 .05(N) (a) General. Tolerances are estab- Beet, sugar, tops ...... 0.05(N) lished for the combined residues of the Spinach ...... 0 .05(N) herbicide propachlor (2-chloro-N- (b) isopropylacetanilide) and its metabo- Section 18 emergency exemptions. [Reserved] lites containing the N-isopropylaniline moiety, calculated as 2-chloro-N- (c) Tolerances with regional registra- isopropylacetanilide, in or on the fol- tions. [Reserved] lowing raw agricultural commodities: (d) Indirect or inadvertent residues. [Reserved] Parts per Commodity million [68 FR 39439, July 1, 2003] Cattle, fat ...... 0.05 § 180.213 Simazine; tolerances for resi- Cattle, kidney ...... 0 .2 dues. Cattle, meat ...... 0 .02 Cattle, meat byproducts, except kidney ...... 0.05 (a) General. Tolerances are estab- Corn, field, forage ...... 3 .0 lished for the combined residues of the Corn, field, grain ...... 0 .2 Corn, field, stover ...... 1 .0 herbicide simazine (2-chloro-4,6- Corn, sweet, forage ...... 3 .0 bis(ethylamino)-s-triazine) and its two Goat, fat ...... 0 .05 chlorinated degradates (2-amino-4- Goat, kidney ...... 0 .2 Goat, meat ...... 0.02 chloro-6-ethylamino-s-triazine and 2,4- Goat, meat byproducts, except kidney ...... 0 .05 diamino-6-chloro-s-triazine), the total

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residue to be measured in or on the fol- application to livestock and poultry, in lowing food commodities: or on the following raw agricultural commodities: Commodity Parts per million Parts per Commodity million Almond ...... 0.25 Almond, hulls ...... 0 .25 Almond, hulls ...... 0 .5 Apple ...... 0.20 Almond ...... 0.5 Avocado ...... 0 .20 Bean, dry, seed ...... 0 .5 Blackberry ...... 0 .20 Bean, succulent ...... 0 .5 Blueberry ...... 0 .20 Beet, sugar, roots ...... 0 .5 Cattle, meat ...... 0 .03 Beet, sugar, tops ...... 0.5 Cattle, meat byproducts ...... 0.03 Broccoli ...... 1 Cherry ...... 0.25 Brussels sprouts ...... 1 Corn, field, forage ...... 0 .20 Cabbage ...... 1 Corn, field, grain ...... 0 .20 Cauliflower ...... 1 Corn, field, stover ...... 0 .25 Celery ...... 3 Corn, pop, grain ...... 0.20 Collards ...... 3 Corn, pop, stover ...... 0.25 Cotton, undelinted seed ...... 0 .5 Corn, sweet, forage ...... 0 .20 Cucumber ...... 0 .5 Corn, sweet, kernel plus cob with husks re- Eggplant ...... 0.5 moved ...... 0 .25 Grape ...... 0 .5 Corn, sweet, stover ...... 0 .25 Grapefruit ...... 3 Cranberry ...... 0 .25 Grass, forage ...... 10 Currant ...... 0 .25 Hop, dried cones ...... 0 .5 Egg ...... 0 .03 Kale ...... 3 Goat, meat ...... 0.03 Legume, forage ...... 10 Goat, meat byproducts ...... 0 .03 Lemon ...... 3 Grape ...... 0 .20 Melon ...... 0 .5 Grapefruit ...... 0 .25 Orange, sweet ...... 3 Hazelnut ...... 0 .20 Peach ...... 0 .5 Horse, meat ...... 0 .03 Pea, succulent ...... 0 .5 Horse, meat byproducts ...... 0 .03 Pepper ...... 0 .5 Lemon ...... 0.25 Pumpkin ...... 0.5 Loganberry ...... 0 .20 Safflower, seed ...... 0 .5 Milk ...... 0.03 Spinach ...... 3 Nut, macadamia ...... 0.25 Squash, summer ...... 0 .5 Olive ...... 0 .20 Squash, winter ...... 0 .5 Orange ...... 0 .25 Strawberry ...... 1 Peach ...... 0 .20 Swiss chard ...... 3 Pear ...... 0 .25 Tangerine ...... 3 Pecan ...... 0 .20 Tomato ...... 0.5 Plum ...... 0 .20 Turnip, greens ...... 3 Raspberry ...... 0 .20 Walnut ...... 0 .5 Sheep, meat ...... 0.03 Sheep, meat byproducts ...... 0 .03 Strawberry ...... 0 .25 (2) A tolerance of 0.5 part per million Walnut ...... 0 .2 is established for the pesticide naled in or on all raw agricultural commodities, (b) Section 18 emergency exemptions. except those otherwise listed in this [Reserved] section, from use of the pesticide for (c) Tolerances with regional registra- area pest (mosquito and fly) control. tions. [Reserved] (b) Section 18 emergency exemptions. (d) Indirect or inadvertent residues. [Reserved] [Reserved] (c) Tolerances with regional registra- [63 FR 2165, Jan. 14, 1998, as amended at 63 tions. [Reserved] FR 57074, Oct. 26, 1998; 72 FR 35665, June 29, (d) Indirect or inadvertent residues. 2007; 72 FR 53454, Sept. 19, 2007] [Reserved]

§ 180.215 Naled; tolerances for resi- [42 FR 46304, Sept. 15, 1977, as amended at 54 dues. FR 20125, May 10, 1989; 63 FR 57074, Oct. 26, 1998; 66 FR 50833, Oct. 5, 2001; 77 FR 59124, (a) General. (1) Tolerances are estab- Sept. 26, 2012] lished for residues of the insecticide naled (1,2-dibromo-2,2-dichloro-ethyl § 180.217 Metiram; tolerances for resi- dimethyl phosphate) and its conversion dues. product 2,2-dichlorovinyl dimethyl (a) General. Tolerances are estab- phosphate, expressed as naled, result- lished for residues of a metiram (a mix- ing from the application of the pes- ture of 5.2 parts by weight of ammoni- ticide to growing crops or from direct ates of [ethylenebis (dithiocarbamato)]

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zinc with 1 part by weight ethylenebis Commodity Parts per [dithiocarbamic acid] bimolecular and million trimolecular cyclic anhydrosulfides Guava ...... 0 .05 and disulfides), including its metabo- Horse, fat ...... 0 .02 lites and degradates, in or on the com- Horse, meat ...... 0 .02 Horse, meat byproducts ...... 0 .02 modities in the following table. Com- Milk ...... 0.02 pliance with the tolerance levels speci- Nut, macadamia ...... 0.20 fied in this paragraph is to be deter- Sheep, fat ...... 0 .02 Sheep, meat ...... 0.02 mined by measuring only those Sheep, meat byproducts ...... 0 .02 metiram residues convertible to and Sorghum, forage, forage ...... 0 .25 expressed in terms of the degradate Sorghum, grain, forage ...... 0.25 Sorghum, grain, grain ...... 0 .20 carbon disulfide. Sorghum, grain, stover ...... 0 .50 Sugarcane, cane ...... 0.20 Commodity Parts per Wheat, forage ...... 1 .5 million Wheat, grain ...... 0 .10 Wheat, hay ...... 5 .0 Apple ...... 0.5 Wheat, straw ...... 0 .50 Apple, pomace, wet ...... 2 Banana 1 ...... 3 Grape, wine 1 ...... 5 (b) Section 18 emergency exemptions. Potato ...... 0 .2 [Reserved] 1 There are no U.S. registrations on bananas and grape, (c) Tolerances with regional registra- wine as of April 29, 2011. tions. [Reserved] (b) Section 18 emergency exemptions. (d) Indirect or inadvertent residues. [Reserved] Tolerances are established for indirect (c) Tolerances with regional registra- or inadvertant residues of atrazine, 2- tions. [Reserved] chloro-4-ethylamino-6-isopropylamino- (d) Indirect or inadvertent residues. s-triazine, in or on the following raw [Reserved] agricultural commodity when present [63 FR 57074, Oct. 26, 1998, as amended at 76 therein as a result of application of FR 23891, Apr. 29, 2011] atrazine to the growing crops in paragraph (a) of this section: § 180.220 Atrazine; tolerances for resi- Parts per dues. Commodity million (a) General. Tolerances are established for the combined residues of the Vegetable, leafy, except brassica, group 4 ...... 0 .25 herbicide atrazine (2-chloro-4- ethylamino-6-isopropylamino-s-tri- [43 FR 29121, July 6, 1978, as amended at 44 azine) and its chlorinated metabolites FR 67116, Nov. 23, 1979; 47 FR 3771, Jan. 27, 1982; 47 FR 8012, Feb. 24, 1982; 63 FR 57075, 2-amino-4-chloro-6-isopropylamino-s- Oct. 26, 1998; 67 FR 46893, July 17, 2002; 69 FR triazine, 2-amino-4-chloro-6- 6567, Feb. 11, 2004; 72 FR 35666, June 29, 2007; ethylamino-s-triazine, and 2,4-diamino- 72 FR 53454, Sept. 19, 2007; 73 FR 37852, July 6-chloro-s-triazine, in or on the fol- 2, 2008; 76 FR 56654, Sept. 14, 2011] lowing food commodities: § 180.222 Prometryn; tolerances for Parts per residues. Commodity million (a) General. Tolerances are estab- Cattle, fat ...... 0.02 lished for residues of the herbicide Cattle, meat ...... 0 .02 Cattle, meat byproducts ...... 0.02 prometryn, including its metabolites Corn, field, forage ...... 1 .5 and degradates, in or on the commod- Corn, field, grain ...... 0 .20 ities in the following table. Compliance Corn, field, stover ...... 0 .5 Corn, pop, forage ...... 1 .5 with the tolerance levels specified in Corn, pop, grain ...... 0.20 the following table is to be determined Corn, pop, stover ...... 0.5 by measuring only prometryn, 2,4- Corn, sweet, forage ...... 15 bis(isopropylamino)-6-methylthio-s-tri- Corn, sweet, kernel plus cob with husks removed ...... 0 .20 azine, in or on the following raw agri- Corn, sweet, stover ...... 2 .0 cultural commodities: Goat, fat ...... 0 .02 Goat, meat ...... 0.02 Parts per Goat, meat byproducts ...... 0 .02 Commodity million Grass, forage ...... 4 .0 Grass, hay ...... 4 .0 Bean, snap, succulent ...... 0 .05

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modities (RACs) resulting from post- Commodity Parts per million harvest fumigation for the control of Carrot, roots ...... 0.45 insects with phosphine gas or Celeriac, roots ...... 0 .05 phosphide compounds that produce Celeriac, tops ...... 0 .20 phosphine gas. Cilantro, leaves ...... 3 .5 Coriander, dried leaves ...... 9.0 Parts per Cotton, gin byproducts ...... 1 .0 Commodity million Cotton, undelinted seed ...... 0 .25 Dill, oil ...... 1 .3 Almond ...... 0.1 Dillweed, dried leaves ...... 1 .1 Avocado ...... 0 .01 Dillweed, fresh leaves ...... 0 .30 Banana ...... 0.01 Leaf petioles subgroup 4B ...... 0 .50 Barley, grain ...... 0 .1 Okra ...... 0.05 Cabbage, Chinese, bok choy ...... 0.01 Parsley, dried leaves ...... 1 .5 Cabbage, Chinese, napa ...... 0 .01 Parsley, leaves ...... 0.60 Cacao bean, dried bean ...... 0 .1 Pea, pigeon, seed ...... 0 .25 Cashew ...... 0 .1 Citron, citrus ...... 0 .01 (b) Section 18 emergency exemptions. Coffee, bean, green ...... 0 .1 [Reserved] Corn, field, grain ...... 0 .1 (c) Tolerances with regional exemptions. Corn, pop, grain ...... 0.1 Cotton, undelinted seed ...... 0 .1 [Reserved] Date, dried fruit ...... 0 .1 (d) Indirect or inadvertent residues. Dill, seed ...... 0 .01 Tolerances are established for indirect Eggplant ...... 0.01 or inadvertent residues of the herbicide Endive ...... 0.01 Grapefruit ...... 0 .01 prometryn, including its metabolites Hazelnut ...... 0 .1 and degradates, in or on the commod- Kumquat ...... 0 .01 ities in the following table. Compliance Lemon ...... 0.01 Lettuce ...... 0.01 with the tolerance levels specified in Lime ...... 0.01 the following table is to be determined Mango ...... 0.01 by measuring only prometryn, 2,4- Millet, grain ...... 0 .1 bis(isopropylamino)-6-methylthio-s-tri- Mushroom ...... 0 .01 Nut, brazil ...... 0 .1 azine, in or on the following raw agri- Oat, grain ...... 0 .1 cultural commodities. Okra ...... 0.01 Orange, sweet ...... 0 .01 Commodity Parts per Papaya ...... 0 .01 million Peanut ...... 0 .1 Pecan ...... 0 .1 Barley, forage ...... 0 .3 Pepper ...... 0 .01 Barley, hay ...... 1 .0 Persimmon ...... 0 .01 Barley, straw ...... 0 .3 Pistachio ...... 0.1 Oat, forage ...... 0 .3 Rice, grain ...... 0 .1 Oat, hay ...... 1.0 Rye, grain ...... 0.1 Oat, straw ...... 0.3 Safflower, seed ...... 0 .1 Rye, forage ...... 0 .3 Salsify, tops ...... 0 .01 Rye, hay ...... 1 .0 Sesame, seed ...... 0 .1 Rye, straw ...... 0 .3 Sorghum, grain ...... 0 .1 Triticale, forage ...... 0 .3 Soybean, seed ...... 0 .1 Triticale, hay ...... 1 .0 Sunflower, seed ...... 0.1 Triticale, straw ...... 0 .3 Sweet potato, roots ...... 0 .01 Wheat, forage ...... 0 .3 Tangelo ...... 0 .01 Wheat, hay ...... 1 .0 Tangerine ...... 0 .01 Wheat, straw ...... 0 .3 Tomato ...... 0.01 Vegetable, legume, group 6, except soybean .... 0 .01 [43 FR 29121, July 6, 1978, as amended at 45 Walnut ...... 0 .1 FR 51782, Aug. 5, 1980; 54 FR 6918, Feb. 15, Wheat, grain ...... 0 .1 1989; 60 FR 20434, Apr. 26, 1995; 63 FR 17692, Apr. 10, 1998; 63 FR 57075, Oct. 26, 1998; 64 FR (2) Tolerances are established for res- 39082, July 21, 1999; 74 FR 47456, Sept. 16, 2009; idues of the fumigant in or on all RACs 74 FR 67108, Dec. 18, 2009; 76 FR 34885, June resulting from preharvest treatment of 15, 2011; 78 FR 55640, Sept. 11, 2013] pest burrows in agricultural and non- crop land areas. § 180.225 Phosphine; tolerances for residues. Parts per Commodity million (a) General. (1) Tolerances are established for residues of phosphine in or All raw agricultural commodities resulting from on the following raw agricultural com- preharvest treatment of pest burrows ...... 0 .01

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(3) Residues resulting from fumiga- Commodity Parts per tion of processed food: million Canola, seed ...... 2 .0 Parts per Commodity million Egg ...... 0 .05 Goat, fat ...... 0 .05 Processed food ...... 0 .01 Goat, meat ...... 0.05 Goat, meat byproducts ...... 0 .05 Hog, fat ...... 0 .05 (4) Residues resulting from fumigation Hog, meat ...... 0 .05 of animal feed: Hog, meat byproducts ...... 0 .05 Horse, fat ...... 0 .05 Horse, meat ...... 0 .05 Commodity Parts per million Horse, meat byproducts ...... 0 .05 Milk ...... 0.02 Animal feed ...... 0.1 Potato ...... 0 .1 Poultry, fat ...... 0.05 (5) To assure safe use of this pes- Poultry, meat ...... 0 .05 Poultry, meat byproducts ...... 0.05 ticide, it must be used in compliance Sheep, fat ...... 0 .05 with the labeling conforming to that Sheep, meat ...... 0.05 registered by the U.S. Environmental Sheep, meat byproducts ...... 0 .05 Protection Agency (EPA) under FIFRA. Labeling shall bear a restric- (2)(i) Tolerances are established for tion to aerate the finished food/feed for residues of the herbicide diquat (6,7 48 hours before it is offered to the con- dihydrodipyrido(1,2-a:2’1’- sumer, unless EPA specifically deter- c)pyrazinediium) (calculated as the mines that a different time period is cation) derived from the application of appropriate. Where appropriate, a the dibromide salt to ponds, lakes, res- warning shall state that under no con- ervoirs, marshes, drainage ditches, ca- dition should any formulation con- nals, streams, and rivers which are taining aluminum or magnesium slow-moving or quiescent in programs phosphide be used so that it will come of the Corp of Engineers or other Fed- in contact with any processed food, ex- eral or State public agencies and to cept processed brewer’s rice, malt, and ponds, lakes and drainage ditches only corn grits stored in breweries for use in where there is little or no outflow of the manufacture of beer. water and which are totally under the (b) Section 18 emergency exemptions. control of the user, in or on the fol- [Reserved] lowing food commodities: (c) Tolerances with regional registra- Parts per tions. [Reserved] Commodity million (d) Indirect or inadvertant residues. Avocado ...... 0 .2 [Reserved] Berry group 13 ...... 0 .05 [64 FR 72950, Dec. 29, 1999, as amended at 71 Cotton, undelinted seed ...... 0 .2 Cranberry ...... 0 .05 FR 74816, Dec. 13, 2006; 72 FR 41929, Aug. 1, Fish ...... 2 .0 2007; 74 FR 46372, Sept. 9, 2009] Fruit, citrus, group 10 ...... 0 .05 Fruit, pome, group 11 ...... 0.02 § 180.226 Diquat; tolerances for resi- Fruit, stone, group 12 ...... 0 .02 dues. Grain, cereal, forage, fodder and straw, group 16 ...... 0 .02 (a) General. (1) Tolerances are estab- Grain, cereal, group 15 ...... 0.02 lished for residues of the plant growth Grape ...... 0 .05 Grass, forage, fodder and hay, group 17 ...... 0 .2 regulator and herbicide diquat, (6,7- Hop, dried cones ...... 0 .2 dihydrodipyrido (1,2-a:2′1′- Nut, tree, group 14 ...... 0 .02 c)pyrazinediium) derived from applica- Shellfish ...... 20 .0 tion of the dibromide salt and cal- Strawberry ...... 0 .05 Sugarcane, cane ...... 0.2 culated as the cation in or on the fol- Vegetable, brassica, leafy, group 5 ...... 0.05 lowing food commodities: Vegetable, cucurbit, group 9 ...... 0.02 Vegetable, foliage of legume, group 7 ...... 0 .2 Vegetable, fruiting, group 8 ...... 0.05 Commodity Parts per million Vegetable, leafy, except brassica, group 4 ...... 0 .05 Vegetable, root and tuber, group 1 ...... 0 .02 Alfalfa, seed ...... 3 .0 Vegetable, seed and pod ...... 0 .05 Cattle, fat ...... 0.05 Cattle, meat ...... 0 .05 Cattle, meat byproducts ...... 0.05 (ii) Where tolerances are established Canola, meal ...... 6 .0 at higher levels from other uses of

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diquat on the subject crops, the higher Commodity Parts per tolerances applies also to residues of million the aquatic uses cited in this para- Cotton, undelinted seed ...... 0 .2 graph. Grass, forage, fodder and hay, group 17, forage 125 .0 (3) Tolerances are established for the Grass, forage, fodder and hay, group 17, hay .... 200 .0 plant growth regulator diquat (6,7 Millet, proso, forage ...... 90.0 Millet, proso, grain ...... 2 .0 dihydrodipyrido(1,2-a:2’1’- Millet, proso, hay ...... 40 .0 c)pyrazinediium) derived from applica- Millet, proso, straw ...... 30 .0 tion of the dibromide salt and cal- Oat, forage ...... 90 .0 culated as the cation in or on the fol- Oat, grain ...... 2 .0 Oat, hay ...... 40.0 lowing food commodites: Oat, straw ...... 30.0 Rye, forage ...... 90 .0 Parts per Rye, grain ...... 2.0 Commodity million Rye, straw ...... 30 .0 Banana1 ...... 0 .05 Sorghum, grain, forage ...... 3.0 Coffee, bean, green1 ...... 0 .05 Sorghum, grain, grain ...... 4 .0 Soybean, hulls ...... 0 .6 Sorghum, grain, stover ...... 10 .0 Sugarcane, cane ...... 0.3 1There are no U.S. registrations as of May 26, 2010. Sugarcane, molasses ...... 5 .0 (4) A tolerance of 0.5 part per million Teff, forage ...... 90.0 Teff, grain ...... 6 .0 is established for residues of diquat in Teff, hay ...... 40.0 potato, granules/flakes and potato, Teff, straw ...... 30 .0 chips. Wheat, forage ...... 90.0 (b) Section 18 emergency exemptions. Wheat, grain ...... 2 .0 Wheat, hay ...... 40 .0 [Reserved] Wheat, straw ...... 30 .0 (c) Tolerances with regional registrations. [Reserved] (2) Tolerances are established for res- (d) Indirect or inadvertent residues. idues of the herbicide dicamba, 3,6- [Reserved] dichloro-o-anisic acid, including its [65 FR 33709, May 24, 2000, as amended at 72 metabolites and degradates, in or on FR 41929, Aug. 1, 2007; 75 FR 29441, May 26, the commodities in the table below. 2010; 75 FR 60241, Sept. 29, 2010] Compliance with the tolerance levels is to be determined by measuring only § 180.227 Dicamba; tolerances for resi- the residues of dicamba (3,6-dichloro-o- dues. anisic acid) and its metabolite, 3,6- (a) General. (1) Tolerances are estab- dichloro-2-hydroxybenzoic acid, cal- lished for the residues of the herbicide culated as the stoichiometric equiva- dicamba (3,6-dichloro-o-anisic acid), in- lent of dicamba, in or on the following cluding its metabolites and degradates, commodities: in or on the commodities in the table Parts per below. Compliance with the tolerance Commodity million levels is to be determined by measuring only the sum of the residues of Asparagus ...... 4.0 dicamba (3,6-dichloro-o-anisic acid) and Cattle, fat ...... 0.3 Cattle, kidney ...... 25 .0 its metabolite, 3,6-dichloro-5-hydroxy- Cattle, meat ...... 0 .25 o-anisic acid, calculated as the stoi- Cattle, meat byproducts, except kidney ...... 3.0 chiometric equivalent of dicamba, in or Goat, fat ...... 0 .3 on the following commodities: Goat, kidney ...... 25.0 Goat, meat ...... 0.25 Goat, meat byproducts, except kidney ...... 3 .0 Parts per Commodity million Hog, fat ...... 0 .3 Hog, kidney ...... 25.0 Barley, grain ...... 6 .0 Hog, meat ...... 0 .25 Barley, hay ...... 2 .0 Hog, meat byproducts, except kidney ...... 3 .0 Barley, straw ...... 15 .0 Horse, fat ...... 0 .3 Corn, field, forage ...... 3 .0 Horse, kidney ...... 25 .0 Corn, field, grain ...... 0 .1 Horse, meat ...... 0 .25 Corn, field, stover ...... 3 .0 Horse, meat byproducts, except kidney ...... 3 .0 Corn, pop, grain ...... 0.1 Milk ...... 0.2 Corn, pop, stover ...... 3.0 Sheep, fat ...... 0 .3 Corn, sweet, forage ...... 0 .50 Sheep, kidney ...... 25.0 Corn, sweet, kernel plus cob with husks re- Sheep, meat ...... 0.25 moved ...... 0 .04 Sheep, meat byproducts, except kidney ...... 3 .0 Corn, sweet, stover ...... 0 .50

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(3) Tolerances are established for res- Commodity Parts per idues of the herbicide dicamba, 3,6- million dichloro-o-anisic acid, including its Cattle, meat byproducts ...... 0.1 metabolites and degradates, in or on Egg ...... 0 .1 the commodities in the table below. Goat, meat byproducts ...... 0 .1 Hog, meat byproducts ...... 0 .1 Compliance with the tolerance levels is Horse, meat byproducts ...... 0 .1 to be determined by measuring only Milk ...... 0.02 the residues of dicamba, 3,6-dichloro-o- Poultry, fat ...... 0.1 anisic acid, and its metabolites, 3,6- Poultry, meat ...... 0 .1 Poultry, meat byproducts ...... 0.1 dichloro-5-hydroxy-o-anisic acid, and Sheep, meat byproducts ...... 0 .1 3,6-dichloro-2-hydroxybenzoic acid, calculated as the stoichiometric equiva- (b) Section 18 emergency exemptions. lent of dicamba, in or on the following [Reserved] commodities: (c) Tolerances with regional registrations. [Reserved] Parts per Commodity million (d) Indirect or inadvertent residues. Tolerances are established for the com- Grain, aspirated fractions ...... 1000 bined residues of the herbicide Soybean, hulls ...... 30 .0 Soybean, seed ...... 10.0 fluometuron, N, N-dimethyl-N’-[3- (trifluoromethyl)phenyl]urea, and its (b) Section 18 emergency exemptions. metabolite, trifluoromethylaniline [Reserved] (TFMA) determined as TFMA, in or on (c) Tolerances with regional registra- the following food commodities. tions. [Reserved] Parts per (d) Indirect or inadvertent residues. Commodity million [Reserved] Grain, cereal, forage, fodder, and straw group [65 FR 33709, May 24, 2000, as amended at 72 16, forage ...... 3 .0 FR 35665, June 29, 2007; 73 FR 17918, Apr. 2, Grain, cereal, forage, fodder, and straw, group 2008; 73 FR 54960, Sept. 24, 2008; 75 FR 60241, 16, stover ...... 6 .0 Sept. 29, 2010; 76 FR 55806, Sept. 9, 2011] Grain, cereal, group 15 ...... 0.5 Peanut ...... 0 .1 Peanut, hay ...... 4.0 § 180.229 Fluometuron; tolerances for Peanut, meal ...... 0 .2 residues. Soybean, forage ...... 3 .0 Soybean, hay ...... 3 .0 (a) General. (1) Tolerances are estab- Soybean, seed ...... 2 .0 lished for the combined residues of the Rice, hulls ...... 1 .0 herbicide fluometuron, N, N-dimethyl- Wheat, milled byproducts ...... 1 .0 N’-[3-(trifluoromethyl)phenyl]urea, and its metabolite, trifluoromethylaniline [73 FR 52613, Sept. 10, 2008] (TFMA) determined as TFMA, in or on the following food commodities: § 180.231 Dichlobenil; tolerances for residues. Parts per Commodity million (a) General. Tolerances are established for the combined residues of the Cotton, gin byproducts ...... 3 .5 herbicide dichlobenil (2,6- Cotton, undelinted seed ...... 1 .0 dichlorobenzonitrile) and its metabo- (2) Tolerances are established for the lite 2,6-dichlorobenzamide in or on the combined residues of the herbicide following raw agricultural commodities: fluometuron, N,N-dimethyl-N’-[3- (trifluoromethyl)phenyl]urea, and its Parts per metabolites determined as TFMA and Commodity million the hydroxylated metabolites: CGA- Apple ...... 0.5 236431, 1-(4-hydroxy-3- Bushberry subgroup 13–07B ...... 0 .15 trifluoromethylphenyl)urea; CGA- Caneberry subgroup 13–07A ...... 0.10 236432, 1-methyl-3-(4-hydroxy-3- Cranberry ...... 0 .1 Fruit, stone, group 12 ...... 0 .15 trifluoromethylphenyl)urea; and CGA- Grape ...... 0 .15 13211, 1,1-dimethyl-3-(4-hydroxy-3- Hazelnut ...... 0 .1 trifluoromethylphenyl)urea, in or on Pear ...... 0 .5 the following food commodities: Rhubarb ...... 0 .06

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(b) Section 18 emergency exemptions. Commodity Parts per [Reserved] million (c) Tolerances with regional registra- Horse, meat byproducts ...... 0 .02(N) tion. [Reserved] Milk ...... 0.02(N) (d) Indirect or inadvertent residues. Mushroom (residues expressed as naled) ...... 0 .5 Poultry, fat ...... 0.05(N) [Reserved] Poultry, meat ...... 0 .05(N) Poultry, meat byproducts ...... 0.05(N) [36 FR 22540, Nov. 25, 1971, as amended at 63 Raw agricultural commodities, nonperishable, FR 57075, Oct. 26, 1998; 66 FR 63198, Dec. 5, bulk stored regardless of fat content, 2001; 73 FR 50570, Aug. 27, 2008] postharvest ...... 0.5 Raw agricultural commodities nonperishable, § 180.232 Butylate; tolerances for resi- packaged or bagged, containing 6 percent fat dues. or less, postharvest ...... 0.5 Raw agricultural commodities, nonperishable, (a) General. Tolerances are estab- packaged or bagged, containing more than 6 lished for residues of the herbicide percent fat, postharvest ...... 2 Sheep, fat ...... 0 .02(N) butylate, including its metabolites and Sheep, meat ...... 0.02(N) degradates, in or on the commodities Sheep, meat byproducts ...... 0 .02(N) in the table in this paragraph. Compli- ance with the tolerance levels specified (2) The tolerance of 0.1 part per mil- in this paragraph is to be determined lion prescribed by 21 CFR 556.180 for by measuring only butylate, S-ethyl bis negligible residues of 2,2-dichlorovinyl (2-methylpropyl) carbamothioate, in or dimethyl phosphate in hog, fat; hog, on the commodity. meat; hog, meat byproducts; and hog, skin covers both its use as an anthel- Expiration/ mintic in swine feed and as an insecti- Commodity Parts per revocation million date cide applied directly to swine. (3) Dichlorvos may be present as a Corn, field, forage ...... 0.1 3/23/13 Corn, field, grain ...... 0.1 3/23/13 residue from application as an insecti- Corn, field, stover ...... 0.1 3/23/13 cide on packaged or bagged nonperish- Corn, pop, grain ...... 0.1 3/23/13 able processed food (see: 21 CFR Corn, pop, stover ...... 0.1 3/23/13 Corn, sweet, forage ...... 0.1 3/23/13 170.3(j)) in an amount in such food not Corn, sweet, kernel plus cob with in excess of 0.5 part per million (ppm). husks removed ...... 0.1 3/23/13 To assure safe use of the insecticide, its label and labeling shall conform to (b) Section 18 emergency exemptions. the label and labeling registered by the [Reserved] U.S. Environmental Protection Agen- (c) Tolerances with regional registra- cy, and the usage employed shall con- tions. [Reserved] form with such label or labeling. (d) Indirect or inadvertent residues. (b) Section 18 emergency exemptions. [Reserved] [Reserved] [68 FR 39439, July 1, 2003, as amended at 76 (c) Tolerances with regional registra- FR 23493, Apr. 27, 2011; 77 FR 59125, Sept. 26, tions. [Reserved] 2012] (d) Indirect or inadvertent residues. [Reserved] § 180.235 Dichlorvos; tolerances for residues. [47 FR 55223, Dec. 8, 1982, as amended at 55 FR 26440, June 28, 1990; 56 FR 29183, June 26, (a) General. (1) Tolerances for resi- 1991; 63 FR 57075, Oct. 26, 1998; 65 FR 33697, dues of the insecticide 2,2-dichlorovinyl May 24, 2000; 74 FR 46373, Sept. 9, 2009; 77 FR dimethyl phosphate are established as 59125, Sept. 26, 2012] follows: § 180.236 Triphenyltin hydroxide; tol- Parts per erances for residues. Commodity million (a) General. Tolerances are estab- Cattle, fat ...... 0.02(N) lished for the combined residues of the Cattle, meat ...... 0 .02(N) Cattle, meat byproducts ...... 0.02(N) fungicide triphenyltin hydroxide Egg ...... 0 .05(N) (TPTH) and its monophenyltin (MPTH) Goat, fat ...... 0 .02(N) and diphenyltin (DPTH) hydroxide and Goat, meat ...... 0.02(N) oxide metabolites, expressed in terms Goat, meat byproducts ...... 0 .02(N) Horse, fat ...... 0 .02(N) of parent TPTH, in or on the following Horse, meat ...... 0 .02(N) raw agricultural commodities:

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mercaptoethyl) benzenesulfonamide in Commodity Parts per million or on the following food commodities: Beet, sugar, roots ...... 0 .05 Parts per Beet, sugar, tops ...... 10.0 Commodity million Cattle, fat ...... 0.2 Cattle, kidney ...... 2 .0 Carrot, roots ...... 0.10 Cattle, liver ...... 4 .0 Cattle, meat ...... 0 .5 (d) Indirect or inadvertent residues. Goat, fat ...... 0 .2 Goat, kidney ...... 2 .0 [Reserved] Goat, liver ...... 4.0 [68 FR 39440, July 1, 2003, as amended at 73 Goat, meat ...... 0.5 Hog, fat ...... 0 .3 FR 53738, Sept. 17, 2008] Hog, meat ...... 0 .06 Hog, meat byproducts ...... 0 .3 § 180.242 Thiabendazole; tolerances for Horse, fat ...... 0 .2 residues. Horse, kidney ...... 2 .0 Horse, liver ...... 4 .0 (a) General. (1) Tolerances are estab- Horse, meat ...... 0 .5 lished for the combined residues of the Milk ...... 0.06 fungicide thiabendazole (2-(4- Pecan ...... 0 .05 thiazolyl)benzimidazole) and its me- Potato ...... 0 .05 Sheep, fat ...... 0 .2 tabolite benzimidazole (free and con- Sheep, kidney ...... 2.0 jugated) in or on the following food Sheep, liver ...... 4.0 commodities: Sheep, meat ...... 0.5 Expiration/ Commodity Parts per Revocation (b) Section 18 emergency exemptions. million Date [Reserved] (c) Tolerances with regional registra- Apple, wet pomace ...... 12.0 None Avocado1 ...... 10.0 None tions. [Reserved] Banana, postharvest ...... 3.0 None (d) Indirect or inadvertent residues. Bean, dry, seed ...... 0.1 None [Reserved] Beet, sugar, dried pulp ...... 3.5 12/25/10 Beet, sugar, roots ...... 0.25 12/25/10 [72 FR 41929, Aug. 1, 2007] Beet, sugar, tops ...... 10.0 12/25/10 Cantaloupe1 ...... 15.0 None Carrot, roots, postharvest ...... 10.0 None § 180.241 Bensulide; tolerances for res- Citrus, oil ...... 15.0 None idues. Corn, field, forage ...... 0.01 None (a) General. Tolerances are estab- Corn, field, grain ...... 0.01 None Corn, field, stover ...... 0.01 None lished for the residues of S-(O,O- Corn, pop, forage ...... 0.01 None diisopropyl phosphorodithioate) of N- Corn, pop, grain ...... 0.01 None (2-mercaptoethyl) benzenesulfonamide Corn, pop, stover ...... 0.01 None Corn, sweet, forage ...... 0.01 None including its oxygen analog S-(O,O- Corn, sweet, kernels plus cop with diisopropyl phosphorothioate) of N-(2- husks removed ...... 0.01 None mercaptoethyl) benzenesulfonamide in Corn, sweet, stover ...... 0.01 None or on the following food commodities: Fruit, citrus, group 10, postharvest 10.0 None Fruit, pome, group 11, postharvest 5.0 None Mango ...... 10.0 None Parts per Commodity million Mushroom ...... 40.0 None Papaya, postharvest ...... 5.0 None Onion, bulb ...... 0 .10 Potato, postharvest ...... 10.0 None Vegetable, brassica, leafy group 5 ...... 0 .15 Soybean ...... 0.1 None 1 Vegetable, cucurbits group 9 ...... 0 .15 Strawberry ...... 5.0 None Vegetable, fruiting group 8 ...... 0 .10 Sweet potato (postharvest to sweet Vegetable, leafy except brassica group 4 ...... 0 .15 potato intended only for use as seed) ...... 0.05 None Wheat, grain ...... 1.0 None (b) Section 18 emergency exemptions. Wheat, straw ...... 1.0 None [Reserved] (c) Tolerances with regional registra- 1There are no U.S. registrations on tions. Tolerances with regional reg- the indicated commodity. istration, as defined in § 180.1(l), are es- (2) Tolerances are established for the tablished for the residues of S-(O,O- combined residues of thiabendazole (2- diisopropyl phosphorodithioate) of N- (4-thiazolyl)benzimidazole) and its me- (2-mercaptoethyl) benzenesulfonamide tabolites 5-hydroxythiabendazole (free including its oxygen analog S-(O,O- and conjugated) and benzimidazole in diisopropyl phosphorothioate) of N-(2- or on the following food commodities:

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streptomycin in or on food commod- Commodity Parts per million ities as follows: Cattle, meat ...... 0 .1 Cattle, meat byproducts ...... 0.4 Commodity Parts per Goat, meat byproducts ...... 0 .4 million Hog, meat byproducts ...... 0 .3 Horse, meat byproducts ...... 0 .4 Bean, dry, seed ...... 0 .5 Milk ...... 0.1 Bean, succulent ...... 0 .5 Sheep, meat byproducts ...... 0 .4 Fruit, pome, group 11 ...... 0.25

(b) Section 18 emergency exemptions. (2) Tolerances are established for res- [Reserved] idues of the fungicide streptomycin (c) Tolerances with regional exemptions. from treatment of seedling plants be- [Reserved] fore transplanting in or on the fol- (d) Indirect or inadvertent residues. lowing food commodities: [Reserved] Parts per [42 FR 32783, June 28, 1977] Commodity million EDITORIAL NOTE: For FEDERAL REGISTER citations affecting § 180.242, see the List of CFR Celery ...... 0 .25 Sections Affected, which appears in the Pepper ...... 0 .25 Finding Aids section of the printed volume Tomato ...... 0.25 and at www.fdsys.gov. (3) Tolerances are established for res- § 180.243 Propazine; tolerances for residues of the fungicide streptomycin idues. from treatment of seed pieces in or on (a) General. Tolerances are estab- the following food commodity: lished for residues of the herbicide Parts per propazine, 2-chloro-4,6- Commodity million bis(isopropylamino)-s-triazine, including its metabolites and degradates, in Potato ...... 0 .25 or on the commodities in the following table. Compliance with the tolerance (b) Section 18 emergency exemptions. levels specified in this paragraph is to Time-limited tolerances are estab- be determined by measuring only the lished for residues of streptomycin, in sum of propazine, 2-chloro-4,6- or on the agricultural commodities, as bis(isopropylamino)-s-triazine, and its specified in the following table, result- two chlorinated degradates, 2-amino-4- ing from use of the pesticide pursuant chloro-6-isopropylamino-s-triazine and to FIFRA section 18 emergency exemp- 2,4-diamino-6-chloro-s-triazine, cal- tions. Compliance with the tolerance culated as the stoichiometric equiva- levels listed in the following table is to lent of propazine, in or on the com- be determined by measuring the levels modity. of streptomycin only, in or on the commodities listed in the table. The toler- Commodity Parts per million ances expire on the dates specified in Sorghum, grain, forage ...... 0.25 the table. Sorghum, grain, grain ...... 0 .25 Sorghum, grain, stover ...... 0 .25 Parts per Expiration Commodity million date (b) Section 18 emergency exemptions. Grapefruit ...... 0.15 12/31/2015 [Reserved] Grapefruit, dried pulp ...... 0.40 12/31/2015 (c) Tolerances with regional registrations. [Reserved] (c) Tolerances with regional registra- (d) Indirect or inadvertent residues. tions. [Reserved] [Reserved] (d) Indirect or inadvertent residues. [75 FR 60242, Sept. 29, 2010] [Reserved] § 180.245 Streptomycin; tolerances for [68 FR 39440, July 1, 2003, as amended at 73 residues. FR 54960, Sept. 24, 2008; 78 FR 29055, May 17, 2013] (a) General. (1) Tolerances are established for residues of the fungicide

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§ 180.249 Alachlor; tolerances for resi- basic hydrolysis, calculated as dues. alachlor, in or on the following raw ag- (a) General. Tolerances are estab- ricultural commodities when present lished for combined residues of therein as a result of the application of alachlor (2-chloro-2’,6’-diethyl-N- alachlor to the growing crops in para- (methoxymethyl)acetanilide) and its graph (a) of this section: metabolites which can be converted to Parts per 2,6-diethylaniline (DEA) or 2-ethyl-6-(1- Commodity million hydroxyethyl)aniline (1-HEEA) upon Animal feed, nongrass, group 18, forage ...... 1 .4 basic hydrolysis, calculated as alachlor Animal feed, nongrass, group 18, hay ...... 1.2 in or on the following raw agricultural Grain, cereal, forage, and straw, group 16 ex- commodities. cept corn, sorghum, rice, straw ...... 0 .8 Grain, cereal, forage, fodder and straw, group 16 except corn, sorghum, rice, forage ...... 0 .6 Parts per Commodity million Grain, cereal, forage, fodder, and straw, group 16 except for corn, sorghum, rice, hay ...... 0 .8 Beans, dry ...... 0.1 Grain, cereal, group 15 except corn, sorghum, Beans, succulent lima ...... 0 .1 rice ...... 0 .05 Cattle, fat ...... 0.02 Cattle, meat byproducts ...... 0.02 Cattle, meat ...... 0 .02 [72 FR 54584, Sept. 26, 2007] Corn, field, forage ...... 2 .0 Corn, field, grain ...... 0 .2 § 180.252 Tetrachlorvinphos; toler- Corn, field, pop ...... 0 .2 ances for residues. Corn, field, stover ...... 2 .0 Corn, pop, stover ...... 2.0 (a) General. Tolerances are estab- Corn, sweet (K+CWHR) ...... 0.05 lished for the combined residues of the Corn, sweet, stover ...... 2 .0 insecticide tetrachlorvinphos [(Z)-2- Cotton, gin byproducts ...... 0 .7 Cotton, undelinted seed ...... 0 .03 chloro-1-(2,4,5-trichlorophenyl) vinyl Cowpea, forage ...... 5 .0 dimethyl phosphate], including its me- Cowpea, hay ...... 5 .0 tabolites, 1-(2,4,5-trichlorophenyl)-eth- Egg ...... 0 .02 Goat, fat ...... 0 .02 anol (free and conjugated forms), 2,4,5- Goat, meat byproducts ...... 0 .02 trichloroacetophenone, and 1-(2,4,5- Goat, meat ...... 0.02 trichlorophenyl)-ethanediol, in or on Hog, fat ...... 0 .02 the following commodities: Hog meat byproducts ...... 0 .02 Hog, meat ...... 0 .02 Parts per Horse, fat ...... 0 .02 Commodity million Horse, meat byproducts ...... 0 .02 Horse, meat ...... 0 .02 Cattle, fat (of which no more than 0.1 ppm is Milk ...... 0.02 tetrachlorvinphos per se) ...... 0 .2 Peanut ...... 0 .5 Cattle, kidney (of which no more than 0.05 Poultry, fat ...... 0.02 ppm is tetrachlorvinphos per se) ...... 1 .0 Poultry, meat byproducts ...... 0.02 Cattle, liver (of which no more than 0.05 ppm Poultry, meat ...... 0 .02 is tetrachlorvinphos per se) ...... 0 .5 Sheep, fat ...... 0 .02 Cattle, meat (of which no more than 2.0 ppm is Sheep, meat byproducts ...... 0 .02 tetrachlorvinphos per se) ...... 2 .0 Sheep, meat ...... 0.02 Cattle, meat byproducts, except kidney and Sorghum grain, forage ...... 2 .0 liver ...... 1 .0 Sorghum, grain, grain ...... 0 .1 Egg (of which no more than 0.05 ppm is Sorghum, grain, stover ...... 1 .0 tetrachlorvinphos per se) ...... 0 .2 Soybeans, seed ...... 1 .0 Hog, fat (of which no more than 0.1 ppm is Sunflower, meal ...... 3 .4 tetrachlorvinphos per se) ...... 0 .2 Sunflower, seed ...... 2.5 Hog, kidney (of which no more than 0.05 ppm is tetrachlorvinphos per se) ...... 1.0 (b) Section 18 emergency exemptions. Hog, liver (of which no more than 0.05 ppm is tetrachlorvinphos per se) ...... 0 .5 [Reserved] Hog, meat (of which no more than 2.0 ppm is (c) Tolerances with regional registra- tetrachlorvinphos per se) ...... 2.0 tions. [Reserved] Hog, meat byproducts, except kidney and liver 1 .0 Milk, fat (reflecting negligible residues in whole (d) Indirect or inadvertent residues. milk and of which no more than 0.05 ppm is Tolerances are established for indirect tetrachlorvinphos per se) ...... 0 .05 or inadvertent residues of alachlor (2- Poultry, fat (of which no more than 7.0 ppm is chloro-2’,6’-diethyl-N- tetrachlorvinphos per se) ...... 7 .0 Poultry, liver (of which no more than 0.05 ppm (methoxymethyl)acetanilide) and its is tetrachlorvinphos per se) ...... 2 .0 metabolites which can be converted to Poultry, meat (of which no more than 3.0 ppm 2,6-diethylaniline (DEA) or 2-ethyl-6-(1- is tetrachlorvinphos per se) ...... 3 .0 hydroxyethyl)aniline (1-HEEA) upon Poultry, meat byproducts, except liver ...... 2 .0

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(b) Section 18 emergency exemptions. Parts per Expiration/ [Reserved] Commodity revocation million date (c) Tolerances with regional registrations. [Reserved] Mustard greens ...... 6 None (d) Indirect or inadvertent residues. Nectarine ...... 5 None [Reserved] Oat, forage ...... 10 None Oat, grain ...... 1 None [76 FR 57659, Sept. 16, 2011, as amended at 78 Oat, hay ...... 10 None FR 15882, Mar. 13, 2013; 78 FR 53684, Aug. 30, Oat, straw ...... 10 None 2013] Onion, green ...... 3 None Orange ...... 2 None § 180.253 Methomyl; tolerances for res- Parsley, leaves ...... 6 None idues. Pea ...... 5 None Pea, field, vines ...... 10 None (a) General. Tolerances are estab- Peach ...... 5 None lished for residues of the insecticide Peanut ...... 0.1 None methomyl, including its metabolites Pecan ...... 0.1 None and degradates, in or on the commod- Pepper, bell ...... 2 None ities in the table in this paragraph. Pepper, nonbell ...... 2 None Compliance with the tolerance levels Peppermint, tops ...... 2 None Pomegranate ...... 0.2 None specified in this paragraph is to be de- Rye, forage ...... 10 None termined by measuring only Rye, grain ...... 1 None methomyl, methyl N-[[(methylamino) Rye, straw ...... 10 None carbonyl]oxy]ethanimidothioate, in or Sorghum, grain, forage ...... 1 None on the commodity. Sorghum, grain, grain ...... 0.2 None Soybean, forage ...... 10 None Soybean, seed ...... 0.2 None Parts per Expiration/ Commodity million revocation Spearmint, tops ...... 2 None date Spinach ...... 6 None Alfalfa, forage ...... 10 None Swiss chard ...... 6 None Alfalfa, hay ...... 10 None Tangerine ...... 2 None Apple ...... 1 None Tomato ...... 1 None Asparagus ...... 2 None Turnip, greens ...... 6 None Avocado ...... 2 None Vegetable, brassica, leafy, group 5 6.0 None Barley, grain ...... 1 None Vegetable, cucurbit, group 9 ...... 0.2 None Barley, hay ...... 10 None Vegetable, fruiting, group 8 ...... 0.2 None Barley, straw ...... 10 None Vegetables, leafy 2 ...... 0.2 None Bean, dry, seed ...... 0.1 None Bean, forage ...... 10 None Vegetable, root and tuber, group 1 0.2 None Bean, succulent ...... 2 None Wheat, forage ...... 10 None Beet, garden, tops ...... 6 None Wheat, grain ...... 1 None Bermudagrass, forage ...... 10 None Wheat, hay ...... 10 None Bermudagrass, hay ...... 40 None Wheat, straw ...... 10 None Blueberry ...... 6 None Broccoli ...... 3 None 1 There are no U.S. registrations for use of methomyl on Brussels sprouts ...... 2 None hop, dried cone, as of February 14, 1990. Cabbage ...... 5 None 2 Except for Beet (tops), broccoli, Brussels sprouts, cab- Cabbage, Chinese, bok choy ...... 5 None bage, cabbage, Chinese, cauliflower, celery, collards, dan- delions, endive (escarole), kale, lettuce, mustard greens, pars- Cabbage, Chinese, napa ...... 5 None ley, spinach, Swiss chard, turnip, greens (tops), and Cauliflower ...... 2 None watercress. Celery ...... 3 None Collards ...... 6 None (b) Section 18 emergency exemptions. Corn, field, forage ...... 10 None Corn, field, grain ...... 0.1 None [Reserved] Corn, field, stover ...... 10 None (c) Tolerances with regional registra- Corn, pop, grain ...... 0.1 None tions. A tolerance with regional reg- Corn, pop, stover ...... 10 None Corn, sweet, forage ...... 10 None istration, as defined in § 180.1(l), is es- Corn, sweet, kernel plus cob with tablished for residues of the insecticide husks removed ...... 0.1 None methomyl, including its metabolites Corn, sweet, stover ...... 10 None Cotton, undelinted seed ...... 0.1 None and degradates, in or on the com- Dandelion, leaves ...... 6 None modity in the table in this paragraph. Endive ...... 5 None Compliance with the tolerance level Grape ...... 5 12/31/16 Grapefruit ...... 2 None specified in this paragraph is to be de- Hop, dried cones 1 ...... 12 None termined by measuring only Kale ...... 6 None methomyl, methyl N-[[(methylamino) Lemon ...... 2 None Lentil, seed ...... 0.1 None carbonyl]oxy]ethanimidothioate, in or Lettuce ...... 5 None on the commodity.

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(d) Indirect or inadvertent residues. Parts per Expiration/ [Reserved] Commodity million Revocation (ppm) date [65 FR 33697, May 24, 2000, as amended at 72 Grape (of which no more than 0.2 FR 35666, June 29, 2007; 74 FR 46373, Sept. 9, ppm is carbamates) ...... 0.4 12/31/09 2009; 75 FR 60242, Sept. 29, 2010; 76 FR 34885, Grape, raisin (of which no more June 15, 2011; 77 FR 59125, Sept. 26, 2012] than 1.0 ppm is carbamate ...... 2.0 12/31/09 Grape, raisin, waste (of which no § 180.254 Carbofuran; tolerances for more than 3.0 ppm is carbamates 6.0 12/31/09 residues. Melon (of which not more than 0.2 ppm is carbamates) ...... 0.4 12/31/09 (a) General. Tolerances are estab- Milk (of which no more than 0.02 lished for the combined residues of the ppm is carbamates) ...... 0.1 12/31/09 insecticide carbofuran (2,3-dihydro-2,2- Oat, grain (of which not more than 0.1 ppm is carbamates) ...... 0.2 12/31/09 dimethyl-7-benzofuranyl-N- Oat, straw (of which not more than methylcarbamate), its carbamate me- 1.0 ppm is carbamates) ...... 5.0 12/31/09 tabolite-2,3-dihydro-2,2-dimethyl-3-hy- Pepper (of which no more than 0.2 droxy-7-benzofuranyl-N- ppm is carbamates) ...... 1 12/31/09 Potato (of which no more than 1 methylcarbamate, and its phenolic me- ppm is carbamates) ...... 2 12/31/09 tabolites 2,3-dihydro-2,2-dimethyl-7- Pumpkin (of which not more than benzofuranol, 2,3-dihydro-2,2-dimethyl- 0.6 ppm is carbamates) ...... 0.8 12/31/09 3,-oxo-7-benzofuranol and 2,3-dihydro- Rice, grain ...... 0.2 12/31/09 2,2-dimethyl-3,7-benzofurandiol in or on Rice, straw (of which no more than 0.2 ppm is carbamates) ...... 1 12/31/09 the following raw agricultural com- Sorghum, forage (of which no more modities: than 0.5 ppm is carbamates) ...... 3 12/31/09 Sorghum, grain, grain ...... 0.1 12/31/09 Parts per Expiration/ Sorghum, grain, stover (of which no Commodity million Revocation more than 0.5 ppm is (ppm) date carbamates) ...... 3 12/31/09 Strawberry (of which no more than Alfalfa, forage (of which no more 0.2 ppm is carbamates) ...... 0.5 12/31/09 than 5 ppm are carbamates) ...... 10 12/31/09 Soybean (of which not more than Alfalfa, hay (of which no more than 0.2 ppm is carbamates) ...... 1.0 12/31/09 20 ppm are carbamates) ...... 40 12/31/09 Soybean, forage (of which not more Banana ...... 0.1 12/31/09 than 20.0 ppm are carbamates) .. 35.0 12/31/09 Barley, grain (of which not more Soybean, hay (of which not more than 0.1 ppm is carbamates) ...... 0.2 12/31/09 than 20.0 ppm are carbamates) .. 35.0 12/31/09 Barley, straw (of which no more Squash (of which not more than 0.6 than 1.0 ppm is carbamates) ...... 5.0 12/31/09 ppm is carbamates) ...... 0.8 12/31/09 Beet, sugar, roots ...... 0.1 12/31/09 Sugarcane, cane ...... 0.1 12/31/09 Beet, sugar, tops (of which no more than 1 ppm is carbamates) ...... 2 12/31/09 Sunflower, seed (of which not more Coffee, bean, green ...... 0.1 12/31/09 than 0.5 ppm is carbamates) ...... 1.0 12/31/09 Corn, field, forage (of which no Wheat, grain (of which not more more than 5 ppm are than 0.1 ppm is carbamates) ...... 0.2 12/31/09 carbamates) ...... 25 12/31/09 Wheat, straw (of which not more Corn, field, grain (of which no more than 1.0 ppm is carbamates) ...... 5.0 12/31/09 than 0.1 ppm is carbamates) ...... 0.2 12/31/09 Corn, field, stover (of which no (b) Section 18 emergency exemptions. more than 5 ppm are [Reserved] carbamates) ...... 25 12/31/09 Corn, pop, grain (of which no more (c) Tolerances with regional registra- than 0.1 ppm is carbamates) ...... 0.2 12/31/09 tion. Tolerances with regional registra- Corn, pop, stover (of which no more tion, as defined in § 180.1(m), are estab- than 5 ppm are carbamates) ...... 25 12/31/09 Corn, sweet, forage (of which no lished for the combined residues of the more than 5 ppm are insecticide carbofuran (2,3-dihydro-2,2- carbamates) ...... 25 12/31/09 dimethyl-7-benzofuranyl-N- Corn, sweet, kernel plus cob with methylcarbamate), its carbamate me- husks removed (of which no more than 0.2 ppm is tabolite 2,3-dihydro-2,2-dimethyl-3-hy- carbamates) ...... 1.0 12/31/09 droxy-7-benzofuranyl-N- Corn, sweet, stover (of which no methylcarbamate, and its phenolic me- more than 5 ppm is carbamates) 25 12/31/09 Cotton, undelinted seed (of which tabolites 2,3-dihydro-2,2-dimethyl-7- no more than 0.2 ppm is benzofuranol, 2,3-dihydro-2,2-dimethyl- carbamates) ...... 1.0 12/31/09 3-oxo-7-benzofuranol, and 2,3-dihydro- Cranberry (of which no more than 2,2-dimethyl-3,7-benzofurandiol in or on 0.3 ppm is carbamates) ...... 0.5 12/31/09 Cucumber (of which not more than the following raw agricultural com- 0.2 ppm is carbamates) ...... 0.4 12/31/09 modity:

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Parts per Expiration/ (c) Tolerances with regional registra- Commodity million Revocation tions. [Reserved] (ppm) date (d) Indirect or inadvertent residues. Artichoke, globe (of which not more [Reserved] than 0.2 ppm is carbamates) ...... 0.4 12/31/09 [68 FR 39440, July 1, 2003, as amended at 72 (d) Indirect or inadvertent residues. FR 53460, Sept. 19, 2007; 76 FR 56654, Sept. 14, [Reserved] 2011] [39 FR 20597, June 12, 1974] § 180.258 Ametryn; tolerances for residues. EDITORIAL NOTE: For FEDERAL REGISTER citations affecting § 180.254, see the List of CFR (a) General. Tolerances are estab- Sections Affected, which appears in the lished for residues of the desiccant and Finding Aids section of the printed volume herbicide (2-ethylamino)-4- and at www.fdsys.gov. (isopropylamino)-6-(methylthio)-s-triazine in or on the following raw agri- § 180.257 Chloroneb; tolerances for res- cultural commodities: idues. (a) General. Tolerances are estab- Expiration/ Commodity Parts per Revocation lished for residues of the fungicide million Date chloroneb, including its metabolites Banana ...... 0.25 6/16/10 and degradates, in or on the commod- Corn, field, forage ...... 0.1 None ities in the table in this paragraph. Corn, field, grain ...... 0.05 None Compliance with the tolerance levels Corn, field, stover ...... 0.05 None specified in this paragraph is to be de- Corn, pop, grain ...... 0.05 None Corn, pop, stover ...... 0.05 None termined by measuring only the sum of Corn, sweet, forage ...... 0.5 6/16/10 chloroneb, 1,4-dichloro-2,5- Corn, sweet, kernel plus cob with dimethoxybenzene, and its metabolite husks removed ...... 0.25 6/16/10 Corn, sweet, stover ...... 0.5 6/16/10 2,5-dichloro-4-methoxyphenol (free and Pineapple ...... 0.05 None conjugated), calculated as the stoichio- Sugarcane, cane ...... 0.05 None metric equivalent of chloroneb, in or on the commodity. (b) Section 18 emergency exemptions. [Reserved] Expiration/ Commodity Parts per revocation (c) Tolerances with regional registra- million date tions. [Reserved] (d) Indirect or inadvertent residues. Bean, dry, seed ...... 0.2 4/16/12 Bean, succulent ...... 0.2 4/16/12 [Reserved] Beet, sugar, roots ...... 0.2 4/16/12 [43 FR 29121, July 6, 1978, as amended at 48 Beet, sugar, tops ...... 0.2 4/16/12 Cowpea, forage ...... 2.0 4/16/12 FR 13175, Mar. 30, 1983; 48 FR 21132, May 11, Cowpea, hay ...... 2.0 4/16/12 1983; 52 FR 33237, Sept. 2, 1987; 63 FR 57075, Cattle, fat ...... 0.2 4/16/12 Oct. 26, 1998; 73 FR 54961, Sept. 24, 2008; 74 FR Cattle, meat ...... 0.2 4/16/12 47456, Sept. 16, 2009] Cattle, meat byproducts ...... 0.2 4/16/12 Cotton, gin byproducts ...... 1.0 4/16/12 § 180.259 Propargite; tolerances for Cotton, undelinted seed ...... 0.2 4/16/12 residues. Goat, fat ...... 0.2 4/16/12 Goat, meat ...... 0.2 4/16/12 (a) General. Tolerances are estab- Goat, meat byproducts ...... 0.2 4/16/12 lished for residues of the pesticide Hog, fat ...... 0.2 4/16/12 Hog, meat ...... 0.2 4/16/12 propargite (2-(p-tert-butylphenoxy) Hog, meat byproducts ...... 0.2 4/16/12 cyclohexyl 2-propynyl sulfite) in or on Horse, fat ...... 0.2 4/16/12 the following food commodities. Horse, meat ...... 0.2 4/16/12 Horse, meat byproducts ...... 0.2 4/16/12 Commodity Parts per Milk ...... 0.05 4/16/12 million Sheep, fat ...... 0.2 4/16/12 Sheep, meat ...... 0.2 4/16/12 Almond ...... 0.1 Sheep, meat byproducts ...... 0.2 4/16/12 Almond, hulls ...... 55 .0 Soybean, forage ...... 2.0 4/16/12 Bean, dry, seed ...... 0 .2 Soybean, hay ...... 2.0 4/16/12 Cattle, fat ...... 0.1 Soybean, seed ...... 0.2 4/16/12 Cattle, meat ...... 0 .1 Cattle, meat byproducts ...... 0.1 Citrus, oil ...... 30.0 (b) Section 18 emergency exemptions. Corn, field, forage ...... 10 .0 [Reserved] Corn, field, grain ...... 0 .1

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commodities in the following table. Commodity Parts per million Compliance with the tolerance levels Corn, field, stover ...... 10 .0 specified in this paragraph is to be de- Corn, pop, grain ...... 0.1 termined by measuring only the sum of Corn, pop, stover ...... 10.0 phosmet, N-(mercaptomethyl) phthal- Corn, sweet, forage ...... 10 .0 Corn, sweet, stover ...... 10.0 imide S-(O,O-dimethyl Cotton, undelinted seed ...... 0 .1 phosphorodithioate), and its oxygen Egg ...... 0 .1 analog, N-(mercaptomethyl) phthal- Goat, fat ...... 0 .1 Goat, meat ...... 0.1 imide S-(O,O-dimethyl Goat, meat byproducts ...... 0 .1 phosphorothioate, calculated as the Grain, aspirated fractions ...... 0 .4 stoichiometric equivalent of phosmet, Grape ...... 10 .0 Grapefruit ...... 5 .0 in or on the commodity. Hog, fat ...... 0 .1 Hog, meat ...... 0 .1 Commodity Parts per Hog, meat byproducts ...... 0 .1 million Hop, dried cones ...... 100 .0 Horse, fat ...... 0 .1 Alfalfa, forage ...... 20 Horse, meat ...... 0 .1 Alfalfa, hay ...... 40 Horse, meat byproducts ...... 0 .1 Almond, hulls ...... 10 Lemon ...... 5.0 Apple ...... 10 Milk, fat (0.08 ppm in milk) ...... 2 .0 Apricot ...... 5 Nectarine ...... 4 .0 Blueberry ...... 10 Orange ...... 10 .0 Cattle, fat ...... 0.2 Peanut ...... 0 .1 Cattle, meat ...... 0 .1 Peppermint, tops ...... 50 .0 Cattle, meat byproducts ...... 0.1 Poultry, fat ...... 0.1 Cherry ...... 10 Potato ...... 0 .1 Cranberry ...... 10 Sheep, fat ...... 0 .1 Fruit, citrus, group 10 ...... 5 Sheep, meat ...... 0.1 Goat, fat ...... 0 .1 Sheep, meat byproducts ...... 0 .1 Goat, meat ...... 0.1 Sorghum, grain, forage ...... 10.0 Goat, meat byproducts ...... 0 .1 Sorghum, grain, grain ...... 5 .0 Grape ...... 10 Sorghum, grain, stover ...... 10 .0 Hog, fat ...... 0 .2 Spearmint, tops ...... 50 .0 Hog, meat ...... 0 .04 Tea, dried ...... 10 .0 Hog, meat byproducts ...... 0 .04 Walnut ...... 0 .1 Horse, fat ...... 0 .1 Horse, meat ...... 0 .1 Horse, meat byproducts ...... 0 .1 (b) Section 18 emergency exemptions. Kiwifruit ...... 25 [Reserved] Milk ...... 0.1 (c) Tolerances with regional registra- Nectarine ...... 5 Nut, tree, group 14 ...... 0 .1 tions. Tolerances with regional reg- Pea, dry, seed ...... 0 .5 istration, as defined in § 180.1(l), are es- Pea, field, hay ...... 20 tablished for residues of propargite in Pea, field, vines ...... 10 Pea, succulent ...... 1 or on the following raw agricultural Peach ...... 10 commodities: Pear ...... 10 Plum, prune, fresh ...... 5 Commodity Parts per Potato ...... 0 .1 million Sheep, fat ...... 0 .1 Sheep, meat ...... 0.1 Corn, sweet, kernel plus cob with husks re- Sheep, meat byproducts ...... 0 .1 moved ...... 0 .1 Sweet potato, roots ...... 12

(d) Indirect or inadvertent residues. (b) Section 18 emergency exemptions. [Reserved] [Reserved] [65 FR 33710, May 24, 2000, as amended at 72 (c) Tolerances with regional registra- FR 41930, Aug. 1, 2007; 73 FR 54961, Sept. 24, tions. Tolerances with regional reg- 2008; 76 FR 34885, June 15, 2011] istration are established for residues of the insecticide phosmet, N- § 180.261 Phosmet; tolerances for resi- (mercaptomethyl) phthalimide S-(O,O- dues. dimethyl phosphorodithioate), includ- (a) General. Tolerances are estab- ing its metabolites and degradates, in lished for residues of the insecticide or on the commodities in the following phosmet, N-(mercaptomethyl) phthal- table. Compliance with the tolerance imide S-(O,O-dimethyl levels specified in this paragraph is to phosphorodithioate), including its me- be determined by measuring only the tabolites and degradates, in or on the sum of phosmet, N-(mercaptomethyl)

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phthalimide S-(O,O-dimethyl Commodity Parts per phosphorodithioate), and its oxygen million analog, N-(mercaptomethyl) phthal- Sweet potato, roots ...... 0 .02 imide S-(O,O-dimethyl 1 There are no U.S. registrations as of July 23, 2009, except phosphorothioate, calculated as the for existing stocks bearing old labeling whose sale, distribution, and use is allowed, provided it is consistent with the stoichiometric equivalent of phosmet, terms of the cancellation order of July 9, 2009; i.e., the EPA in or on the commodity. will allow the technical registrant to continue to sell and dis- tribute existing stocks of the amended registered product bearing old labeling for use on pineapple for 18 months (until Commodity Parts per January 9, 2011) and persons other than the registrant may million continue to sell and/or use existing stocks of product bearing the old labeling until such stocks are exhausted, provided that Crabapple ...... 20 such use is consistent with the terms of the previously ap- Pistachio ...... 0.1 proved labeling on, or that accompanied, the modified product. (d) Indirect or inadvertent residues. (b) Section 18 emergency exemptions. [Reserved] [Reserved] (c) Tolerances with regional registra- [43 FR 46538, Oct. 10, 1978, as amended at 45 tions. [Reserved] FR 8981, Feb. 11, 1980; 48 FR 37213, Aug. 17, (d) Indirect or inadvertent residues. 1983; 52 FR 48539, Dec. 23, 1987; 53 FR 657, Jan. [Reserved] 11, 1988; 53 FR 39090, Oct. 5, 1988; 63 FR 57075, Oct. 26, 1998; 67 FR 49616, July 31, 2002; 74 FR [47 FR 53004, Nov. 24, 1982, as amended at 48 46698, Sept. 11, 2009; 75 FR 60242, Sept. 29, FR 51485, Nov. 9, 1983; 52 FR 33237, Sept. 2, 2010] 1987; 53 FR 30053, Aug. 10, 1988; 63 FR 57075, Oct. 26, 1998; 64 FR 39078, July 21, 1999; 66 FR § 180.262 Ethoprop; tolerances for resi- 38955, July 26, 2001; 67 FR 49616, July 31, 2002; dues. 73 FR 53731, Sept. 17, 2008; 73 FR 54961, Sept. 24, 2008; 74 FR 46373, Sept. 9, 2009; 75 FR 60242, (a) General. Tolerances are estab- Sept. 29, 2010] lished for residues of the nematocide and insecticide ethoprop, O-ethyl S,S- § 180.263 Phosalone; tolerances for res- dipropyl phosphorodithioate, including idues. its metabolites and degradates, in or (a) General. Tolerances are estab- on the commodities in the following lished for residues of the insecticide table. Compliance with the tolerance phosalone, S-(6-chloro-3- levels specified in this paragraph is to (mercaptomethyl)-2-benzoxazolinone) be determined by measuring only O,O-diethyl phosphorodithioate, in or ethoprop, O-ethyl S,S-dipropyl on the following food commodities: phosphorodithioate, in or on the com- Expiration/ modity. Commodity Parts per Revocation million Date

Parts per 1 Commodity million Apple ...... 10.0 9/30/13 Cherry1 ...... 15.0 9/30/13 Grape1 ...... 10.0 9/30/13 Banana ...... 0.02 Peach1 ...... 15.0 9/30/13 Bean, lima ...... 0 .02 Pear1 ...... 10.0 9/30/13 Bean, snap, succulent ...... 0 .02 Plum, prune, fresh1 ...... 15.0 9/30/13 Cabbage ...... 0 .02 1 Corn, field, forage ...... 0 .02 There are no U.S. registrations since 1992. Corn, field, grain ...... 0 .02 (b) Section 18 emergency exemptions. Corn, field, stover ...... 0 .02 [Reserved] Corn, sweet, forage ...... 0 .02 Corn, sweet, kernel plus cob with husks re- (c) Tolerances with regional registra- moved ...... 0 .02 tions. [Reserved] Corn, sweet, stover ...... 0 .02 (d) Indirect or inadvertent residues. Cucumber ...... 0 .02 [Reserved] Hop, dried cones ...... 0 .02 Peppermint, tops ...... 0 .02 [74 FR 46698, Sept. 11, 2009] Pineapple1 ...... 0 .02 Potato ...... 0 .02 § 180.269 Aldicarb; tolerances for resi- Spearmint, tops ...... 0 .02 dues. Sugarcane, cane ...... 0.02 (a) General. Tolerances are established for combined residues of the insecticide and nematocide aldicarb (2-

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methyl-2-(methylthio)propionaldehyde Commodity Parts per O-(methylcarbamoyl) oxime and its million cholinesterase-inhibiting metabolites Milk ...... 0.01 2-methyl 2-(methylsulfinyl) Sheep, fat ...... 0 .15 propionaldehyde O-(methylcarbamoyl) Sheep, meat ...... 0.02 oxime and 2-methyl-2-(methylsulfonyl) Sheep, meat byproducts ...... 0 .02 propionaldehyde O-(methylcarbamoyl) oxime in or on the following food com- (b) Section 18 emergency exemptions. modities: [Reserved] (c) Tolerances with regional registra- Commodity Parts per tions. [Reserved] million (d) Indirect or inadvertent residues. Bean, dry, seed ...... 0 .1 [Reserved] Beet, sugar, roots ...... 0 .05 Beet, sugar, tops ...... 1 [65 FR 33698, May 24, 2000, as amended at 67 Citrus, dried pulp ...... 0 .6 FR 49616, July 31, 2002; 72 FR 53460, Sept. 19, Coffee, bean, green ...... 0 .1 2007] Cotton, undelinted seed ...... 0 .1 Cotton, hulls ...... 0 .3 Grapefruit ...... 0 .3 § 180.274 Propanil; tolerances for resi- Lemon ...... 0.3 dues. Lime ...... 0.3 Orange, sweet ...... 0 .3 (a) General. Tolerances are estab- Peanut ...... 0 .05 lished for the combined residues of the Pecan ...... 0 .5 herbicide propanil (3′, 4′- Potato ...... 1 dichloropropionanilide) and its me- Sorghum, grain, bran ...... 0 .5 Sorghum, grain, grain ...... 0 .2 tabolites convertible to 3, 4- Sorghum, grain, stover ...... 0 .5 dichloroaniline (3, 4-DCA) in or on the Soybean ...... 0.02 following food commodities: Sugarcane, cane ...... 0.02 Sweet potato, roots ...... 0 .1 Parts per Commodity million (b) Section 18 emergency exemptions. [Reserved] Cattle, fat ...... 0.10 (c) Tolerances with regional registra- Cattle, meat ...... 0 .05 Cattle, meat byproducts ...... 1.0 tions. [Reserved] Crayfish ...... 0.05 (d) Indirect or inadvertent residues. Egg ...... 0 .30 [Reserved] Goat, fat ...... 0 .10 Goat, meat ...... 0.05 [65 FR 33710, May 24, 2000, as amended at 69 Goat, meat byproducts ...... 1 .0 FR 6567, Feb. 11, 2004; 73 FR 54961, Sept. 24, Hog, fat ...... 0 .10 2008] Hog, meat ...... 0 .05 Hog, meat byproducts ...... 1 .0 § 180.272 Tribuphos; tolerances for res- Horse, fat ...... 0 .10 idues. Horse, meat ...... 0 .05 Horse, meat byproducts ...... 1 .0 (a) General. Tolerances are estab- Milk ...... 0.05 lished for residues of the defoliant Poultry, fat ...... 0.05 tribuphos (S,S,S-tributyl Poultry, meat ...... 0 .10 phosphorotrithioate) in or on food com- Poultry, meat byproducts ...... 0.50 Rice, bran ...... 40 modities as follows: Rice, grain ...... 10 Rice, hulls ...... 30 Parts per Rice, straw ...... 75 Commodity million Sheep, fat ...... 0 .10 Cattle, fat ...... 0.15 Sheep, meat ...... 0.05 Cattle, meat ...... 0 .02 Sheep, meat byproducts ...... 1 .0 Cattle, meat byproducts ...... 0.02 Cotton, gin byproducts ...... 40 .0 (b) Section 18 emergency exemptions. Cotton, undelinted seed ...... 4 .0 Goat, fat ...... 0 .15 [Reserved] Goat, meat ...... 0.02 (c) Tolerances with regional registra- Goat, meat byproducts ...... 0 .02 tions. [Reserved] Hog, fat ...... 0 .15 Hog, meat ...... 0 .02 (d) Indirect or inadvertent residues. Hog, meat byproducts ...... 0 .02 [Reserved] Horse, fat ...... 0 .15 Horse, meat ...... 0 .02 [63 FR 34827, June 26, 1998, as amended at 72 Horse, meat byproducts ...... 0 .02 FR 28888, May 23, 2007]

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§ 180.275 Chlorothalonil; tolerances for Commodity Parts per residues. million (a) General. (1) Tolerances are estab- Goat, meat ...... 0.03 lished for the fungicide chlorothalonil Hog, fat ...... 0 .1 Hog, kidney ...... 0.5 (tetrachloroisophthalonitrile) and its Hog, meat byproducts, except kidney ...... 0 .05 metabolite 4-hydroxy-2,5,6- Hog, meat ...... 0 .03 trichloroisophthalonitrile in or on the Horse, fat ...... 0 .1 Horse, kidney ...... 0 .5 following food commodities. Horse, meat byproducts, except kidney ...... 0 .05 Horse, meat ...... 0 .03 Commodity Parts per Milk ...... 0.1 million Sheep, fat ...... 0 .1 Sheep, kidney ...... 0.5 Almond ...... 0.05 Sheep, meat byproducts, except kidney ...... 0 .05 Almond, hulls ...... 1 .0 Sheep, meat ...... 0.03 Apricot ...... 0 .5 Asparagus ...... 0.1 Banana (NMT 0.05 ppm in edible pulp) ...... 0 .5 (b) Section 18 emergency exemptions. Bean, dry, seed ...... 0 .1 [Reserved] Bean, snap, succulent ...... 5 (c) Tolerances with regional registra- Blueberry ...... 1 .0 Brassica, head and stem, subgroup 5A ...... 5 .0 tions. Tolerances with regional reg- Carrot, roots ...... 1 istration, as defined in § 180.1(l), are es- Celery ...... 15 tablished for the combined residues of Cherry, sweet ...... 0 .5 chlorothalonil and its metabolite in or Cherry, tart ...... 0 .5 Cocoa bean, dried bean ...... 0 .05 on the following raw agricultural com- Coffee, bean, green ...... 0 .20 modities: Corn, sweet, kernel plus cob with husks removed ...... 1 Parts per Cranberry ...... 5 .0 Commodity million Ginseng ...... 4 .0 Horseradish ...... 4.0 Hazelnut ...... 0 .1 Lentil ...... 0.10 Peppermint, tops ...... 2 Lychee ...... 15 Persimmon ...... 1 .5 Mango ...... 1.0 Spearmint, tops ...... 2 Mushroom ...... 1 .0 Nectarine ...... 0 .5 (d) Indirect or inadvertent residues. Okra ...... 6.0 Onion, bulb ...... 0 .5 [Reserved] Onion, green ...... 5 Papaya ...... 15 [42 FR 56114, Oct. 21, 1977] Parsnip, roots ...... 1 EDITORIAL NOTE: For FEDERAL REGISTER ci- Passionfruit ...... 3 tations affecting § 180.275, see the List of CFR Pea, edible podded ...... 5 Peach ...... 0 .5 Sections Affected, which appears in the Peanut ...... 0 .3 Finding Aids section of the printed volume Pistachio ...... 0.2 and at www.fdsys.gov. Plum ...... 0 .2 Plum, prune ...... 0 .2 § 180.276 Formetanate hydrochloride; Potato ...... 0 .1 tolerances for residues. Rhubarb ...... 4 .0 Soybean ...... 0.2 (a) General. Tolerances are estab- Starfruit ...... 3 .0 lished for residues of the insecticide Tomato ...... 5 Vegetable, cucurbit, group 9 ...... 5.0 formetanate hydrochloride, including Vegetable, fruiting, group 8, except tomato ...... 6 .0 its metabolites and degradates, in or Yam, true ...... 0 .10 on the commodities in the table in this paragraph. Compliance with the toler- (2) Tolerances are established for the ance levels specified in this paragraph metabolite 4-hydroxy-2,5,6- is to be determined by measuring only trichloroisophthalonitrile in or on the formetanate hydrochloride, N,N-di- following food commodities. methyl-N’-[3-[(methylamino)carbonyl] Parts per oxy]phenyl]methanimidamide hydro- Commodity million chloride, in or on the commodity.

Cattle, fat ...... 0.1 Expiration/ Cattle, kidney ...... 0 .5 Commodity Parts per revocation Cattle, meat byproducts, except kidney ...... 0.05 million date Cattle, meat ...... 0 .03 Goat, fat ...... 0 .1 Apple ...... 0.50 12/31/13 Goat, kidney ...... 0 .5 Apple, wet pomace ...... 1.5 12/31/13 Goat, meat byproducts, except kidney ...... 0 .05 Grapefruit ...... 1.5 None

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Expiration/ Parts per Commodity Parts per revocation Commodity million million date Beet, sugar, roots ...... 0 .05 Lemon ...... 0.60 None Beet, sugar, tops ...... 0.2 Lime ...... 0.03 None Grape ...... 0 .01 Nectarine ...... 0.40 None Grass, rangeland, forage ...... 0 .1 Orange ...... 1.5 None Peach ...... 0.40 12/31/13 Grass, rangeland, hay ...... 0 .1 Pear ...... 0.50 12/31/13 Potato ...... 0 .05 Tangelo ...... 0.03 None Sugarcane, cane ...... 0.01 Tangerine ...... 0.03 None Timothy, hay ...... 0 .5 Timothy, forage ...... 0.5 (b) Section 18 emergency exemptions. Wheat, forage ...... 0 .05 [Reserved] Wheat, grain ...... 0 .05 (c) Tolerances with regional registra- Wheat, hay ...... 0 .05 tions. [Reserved] Wheat, straw ...... 0 .05 (d) Indirect or inadvertent residues. (b) Section 18 emergency exemptions. [Reserved] [Reserved] [77 FR 40815, July 11, 2012] (c) Tolerances with regional registrations. Tolerances with regional reg- § 180.278 Phenmedipham; tolerances istration, as defined in § 180.1(l), are es- for residues. tablished for residues of phosphine re- (a) General. Tolerances are estab- sulting from the use of the rodenticide lished for the combined residues of the zinc phosphide in or on the following herbicide phenmedipham (3- raw agricultural commodities as fol- ′ methoxycarbonylaminophenyl-3 - lows: methylcarbanilate) in or on the following food commodities: Parts per Commodity million Parts per Commodity million Artichoke, globe ...... 0.01 Beet, sugar, roots ...... 0 .04 Beet, garden, roots ...... 0 .2 Beet, sugar, tops ...... 0.02 Beet, garden, tops ...... 0 .2 Beet, sugar, dried pulp ...... 0 .5 Beet, sugar, molasses ...... 0 .2 (d) Indirect or inadvertent residues. Beet, sugar, roots ...... 0 .1 [Reserved] Beet, sugar, tops ...... 0.1 Spinach ...... 4 .0 [63 FR 45182, Aug. 25, 1998, as amended at 63 FR 67799, Dec. 9, 1998; 64 FR 40772, July 28, (b) Section 18 emergency exemptions. 1999; 64 FR 61791, Nov. 15, 1999; 65 FR 8874, [Reserved] Feb. 23, 2000; 65 FR 49941, Aug. 16, 2000; 65 FR (c) Tolerances with regional registra- 62634, Oct. 19, 2000; 66 FR 64773, Dec. 14, 2001; tions. [Reserved] 68 FR 2247, Jan. 16, 2003; 68 FR 56195, Sept. 30, (d) Indirect or inadvertent residues. 2003; 70 FR 7046, Feb. 10, 2005; 74 FR 46373, [Reserved] Sept. 9, 2009; 76 FR 34885, June 15, 2011] [72 FR 28888, May 23, 2007] § 180.287 Amitraz; tolerances for residues. § 180.284 Zinc phosphide; tolerances for residues. (a) General. Tolerances are established for residues of the insecticide (a) General. Tolerances are estab- amitraz (N’-[2,4-dimethylphenyl]-N- lished for residues of the phosphine re- [[(2,4-dimethylphenyl)imino]methyl]]- sulting from the use of the rodenticide N-methylmethanimidamide), including zinc phosphide in or on the raw agricul- its metabolites and degradates, in or tural commodities as follows: on the commodities in the following table. Compliance with the tolerance Commodity Parts per million levels specified is to be determined by Alfalfa, forage ...... 0.2 measuring amitraz residues convertible Alfalfa, hay ...... 0.2 to 2,4-dimethylaniline, expressed as the Barley, grain ...... 0 .05 stoichiometric equivalent of amitraz, Barley, hay ...... 0 .2 Barley, straw ...... 0 .2 in or on the following raw agricultural Bean, dry, seed ...... 0 .05 commodities:

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(b) Section 18 emergency exemptions. Commodity Parts per million [Reserved] Cattle, fat ...... 0.1 (c) Tolerances with regional registra- Cattle, meat ...... 0 .02 tions. [Reserved] Cattle, meat byproducts ...... 0.2 (d) Indirect or inadvertent residues. Cotton, undelinted seed 1 ...... 1 .0 [Reserved] Hog, fat ...... 0 .1 Hog, kidney ...... 0.1 [68 FR 39440, July 1, 2003, as amended at 74 Hog, liver ...... 0 .1 FR 46374, Sept. 9, 2009] Hog, meat ...... 0 .05 Hog, meat byproducts ...... 0 .3 Honey ...... 0.2 § 180.289 Methanearsonic acid; toler- Honeycomb ...... 9 ances for residues. Milk ...... 0.03 (a) General. Tolerances are estab- Milk, fat ...... 0 .2 lished for residues of the herbicide 1There are no U.S. registrations on cottonseed as of May 3, methanearsonic acid, including its me- 2006. tabolites and degradates, in or on the (b) Section 18 emergency exemptions. commodities in the table in this para- [Reserved] graph. Compliance with the tolerance (c) Tolerances with regional registra- levels specified in this paragraph is to tions. [Reserved] be determined by measuring only (d) Indirect or inadvertent residues. methanearsonic acid, from application [Reserved] of the disodium and monosodium salts [44 FR 70145, Dec. 6, 1979, as amended at 51 of methanearsonic acid, calculated as FR 16846, May 7, 1986; 52 FR 5767, Feb. 26, the stoichiometric equivalent of As2O3, 1987; 57 FR 53568, Nov. 12, 1992; 58 FR 14316, in or on the commodity. Mar. 17, 1993; 60 FR 12704, Mar. 8, 1995; 67 FR 49616, July 31, 2002; 72 FR 53454, Sept. 19, 2007; Expiration/ Commodity Parts per Revocation 74 FR 47456, Sept. 16, 2009; 78 FR 17133, Mar. million Date 20, 2013] Cotton, undelinted seed ...... 0.7 None § 180.288 2-(Thiocyanomethyl- Cotton, hulls ...... 0.9 None thio)benzothiazole; tolerances for Fruit, citrus ...... 0.35 12/31/12 residues. (b) Section 18 emergency exemptions. (a) General. Tolerances are estab- [Reserved] lished for residues of the fungicide 2- (c) Tolerances with regional registra- (thiocyanomethylthio)benzothiazole in tions. [Reserved] or on the following food commodities: (d) Indirect or inadvertent residues. [Reserved] Commodity Parts per million [63 FR 34828, June 26, 1998, as amended at 77 Barley, grain ...... 0 .1(N) FR 59126, Sept. 26, 2012] Barley, straw ...... 0 .1(N) Beet, sugar, roots ...... 0 .1(N) § 180.291 Pentachloronitrobenzene; tol- Beet, sugar, tops ...... 0.1(N) erance for residues. Corn, field, forage ...... 0 .1(N) Corn, field, grain ...... 0 .1 (a) General. Tolerances are estab- Corn, field, stover ...... 0 .1 lished for the combined residues of the Corn, pop, grain ...... 0.1 fungicide pentachloronitrobenzene Corn, pop, stover ...... 0.1 (PCNB) and its metabolites Cotton, forage ...... 0.1(N) Cotton, undelinted seed ...... 0 .1(N) pentachloroaniline (PCA), and Oat, forage ...... 0 .1(N) pentachlorothioanisole (PCTA), in or Oat, grain ...... 0 .1(N) on the following food commodities: Oat, hay ...... 0.1(N) Oat, straw ...... 0.1(N) Parts per Rice, grain ...... 0 .1(N) Commodity million Rice, straw ...... 0 .1(N) Safflower, seed ...... 0 .1(N) Bean ...... 0 .1 Sorghum, grain, forage ...... 0.1(N) Brassica, head and stem, subgroup 5A ...... 0 .1 Sorghum, grain, grain ...... 0 .1(N) Cotton, undelinted seed ...... 0 .1 Sorghum, grain, stover ...... 0 .1(N) Garlic, bulb ...... 0.1 Wheat, forage ...... 0 .1(N) Peanut ...... 1 .0 Wheat, grain ...... 0 .1(N) Potato ...... 0 .1 Wheat, hay ...... 0 .1(N) Soybean, forage ...... 0 .02 Wheat, straw ...... 0 .1(N) Soybean, hay ...... 0 .02 Soybean, seed ...... 0 .02

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Parts per Parts per Commodity million Commodity million

Vegetable, fruiting, group 8 ...... 0.1 Milk ...... 0.25 Oat, forage ...... 1 .0 (b) Section 18 emergency exemptions. Oat, grain ...... 0 .5 Oat, groats/rolled oats ...... 3 .0 [Reserved] Oat, straw ...... 1.0 (c) Tolerances with regional registra- Poultry, fat ...... 0.05 tions. Tolerances with regional reg- Poultry, meat ...... 0 .05 Poultry, meat byproducts ...... 0.05 istrations, as defined in § 180.1(l), are Sheep, fat ...... 0 .4 established for the combined residues Sheep, meat ...... 0.4 of the fungicide Sheep, meat byproducts ...... 15 Wheat, bran ...... 3.0 pentachloronitrobenzene (PCNB) and Wheat, forage ...... 1 .0 its metabolites pentachloroaniline Wheat, germ ...... 3 .0 (PCA), and pentachlorothioanisole Wheat, grain ...... 0 .5 Wheat, middlings ...... 3 .0 (PCTA), in or on the following food Wheat, shorts ...... 3 .0 commodities: Wheat, straw ...... 1 .0

Parts per (b) Section 18 emergency exemptions. Commodity million [Reserved] Collards ...... 0.2 (c) Tolerances with regional registra- Kale ...... 0 .2 Mustard, greens ...... 0 .2 tions. [Reserved] (d) Indirect or inadvertent residues. (d) Indirect or inadvertent residues. [Reserved] [Reserved] [41 FR 19221, May 11, 1976, as amended at 47 [74 FR 47456, Sept. 16, 2009] FR 53005, Nov. 24, 1982; 64 FR 425, Jan. 5, 1999; 64 FR 39082, July 21, 1999; 72 FR 41930, Aug. 1, § 180.292 Picloram; tolerances for resi- 2007; 75 FR 60243, Sept. 29, 2010] dues. § 180.293 Endothall; tolerances for res- (a) General. Tolerances are estab- idues. lished for residues of the herbicide (a) General. (1) Tolerances are estab- picloram, 4-amino-3,5,6- lished for the residues of endothall, in- trichloropicolinic acid, including its cluding its metabolites and degradates, metabolites and degradates, in or on in or on the commodities in the table, the commodities in the following table below. Compliance with the tolerance from its application in the acid form or levels specified, below, is to be deter- in the form of its salts. Compliance mined by measuring only endothall (7- with the tolerance levels specified in oxabicylco [2.2.1] heptanes-2,3- this paragraph is to be determined by dicarboxylic acid) and its mono-methyl measuring only picloram, 4-amino- ester. 3,5,6-trichloropicolinic acid, in or on the commodity. Parts per Commodity million Parts per Commodity million Apple ...... 0.05 Apple, wet pomace ...... 0 .15 Barley, grain ...... 0 .5 Cotton, undelinted seed ...... 0 .1 Barley, pearled barley ...... 3 .0 Fish ...... 0 .1 Barley, straw ...... 1 .0 Hop, dried cones ...... 0 .1 Cattle, fat ...... 0.4 Potato ...... 0 .1 Cattle, meat ...... 0 .4 Rice, grain ...... 0 .05 Cattle, meat byproducts ...... 15 Rice, straw ...... 0 .05 Egg ...... 0 .05 Goat, fat ...... 0 .4 Goat, meat ...... 0.4 (2) An interim tolerance of 0.2 parts Goat, meat byproducts ...... 15 per million is established for residues Grain, aspirated fractions ...... 4 .0 of the herbicide endothall (7 - Grass, forage ...... 400 oxabicyclo[2.2.1] heptane-2,3- Grass, hay ...... 225 Hog, fat ...... 0 .05 dicarboxylic acid) in water, potable Hog, meat ...... 0 .05 from use of its potassium, sodium, di- Hog, meat byproducts ...... 0 .05 N, N-dimethylalkylamine, and mono-N- Horse, fat ...... 0 .4 Horse, meat ...... 0 .4 N,-dimethylalkylamine salts as Horse, meat byproducts ...... 15 algicides or herbicides to control

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aquatic plants in canals, lakes, ponds, Commodity Parts per and other potential sources of water, million potable. Pea and bean, succulent shelled, subgroup 6B 2 .0 (b) Section 18 emergency exemptions. Peppermint, tops ...... 5 .0 [Reserved] Pistachio ...... 0.05 (c) Tolerances with regional registra- Poultry, fat ...... 0.015 tions. [Reserved] Poultry, liver ...... 0 .05 (d) Indirect or inadvertent residues. Poultry, meat ...... 0 .015 Poultry, meat byproducts ...... 0.20 Tolerances are established for the indi- Rice, hulls ...... 8 .0 rect or inadvertent combined residues Sheep, fat ...... 0 .005 of the herbicide, endothall (7 - Sheep, kidney ...... 0.15 oxabicyclo[2.2.1] heptane-2,3- Sheep, liver ...... 0.05 dicarboxylic acid) in potable water Sheep, meat ...... 0.015 from use of its potassium, sodium, di- Soybean, hulls ...... 0 .5 N, N -dimethylalkylamine, and mono- Soybean, seed ...... 0 .2 Spearmint, tops ...... 5 .0 N-N, -dimethylalkylamine salts as Tomato, paste ...... 0 .1 algicides or herbicides to control Tomato, puree ...... 0 .1 aquatic plants in canals, lakes, ponds, Vegetable, bulb, group 3-07 ...... 0 .5 and other potable water sources that Vegetable, cucurbit, group 9 ...... 1.5 may lead to endothall residues in or on Vegetable, foliage of legume, group 7 ...... 4 .0 the following commodities: Vegetable, fruiting, group 8 ...... 0.05 Vegetable, leafy, except brassica, group 4 ...... 2 .0 Parts per Vegetable, leaves of root and tuber, group 2 ... 3 .0 Commodity million Vegetable, legume, edible, podded, subgroup 6A ...... 2 .0 Almond, hulls ...... 15 .0 Vegetable, root and tuber, group 1 ...... 1 .0 Animal feed, nongrass, group 18, forage ...... 4 .0 Wheat, milled byproducts ...... 5 .0 Animal feed, nongrass, group 18, hay ...... 10 Apple, wet pomace ...... 0 .15 Beet, sugar, molasses ...... 1 .5 [41 FR 23717, June 11, 1976, as amended at 51 Brassica, head and stem subgroup 5A ...... 0 .1 Brassica, leafy, subgroup 5B ...... 2 .0 FR 4498, Feb. 5, 1986; 62 FR 49931, Sept. 24, Bushberry subgroup 13-07B ...... 0 .6 1997; 63 FR 42249, Aug. 7, 1998; 67 FR 35048, Caneberry subgroup 13-07A ...... 0.6 May 17, 2002; 71 FR 47106, Aug. 16, 2006; 71 FR Cattle, fat ...... 0.01 74816, Dec. 13, 2006; 72 FR 52018, Sept. 12, 2007; Cattle, kidney ...... 0 .20 74 FR 67097, Dec. 18, 2009; 78 FR 76566, Dec. 18, Cattle, liver ...... 0 .10 Cattle, meat ...... 0 .03 2013] Corn, field, grain ...... 0 .07 Corn, pop, grain ...... 0.07 § 180.297 N-1-Naphthyl phthalamic Corn, sweet, kernel plus cob with husks re- acid; tolerances for residues. moved ...... 0 .3 Citrus, dried pulp ...... 0 .1 (a) General. Tolerances are estab- Egg ...... 0 .05 lished for residues of the herbicide N-1- Feed commodities not otherwise listed ...... 10 .0 Food commodities not otherwise listed ...... 5 .0 naphthyl phthalamic acid from appli- Fruit, citrus group 10 ...... 0.05 cation of its sodium salt in or on the Fruit, pome, group 11 ...... 0.05 following raw agricultural commod- Fruit, stone, group 12 ...... 0 .3 Goat, fat ...... 0 .005 ities: Goat, kidney ...... 0 .15 Goat, liver ...... 0.05 Commodity Parts per Goat, meat ...... 0.015 million Grain, aspirated fractions ...... 35.0 Grain cereal, forage, fodder and straw, group Cantaloupe ...... 0 .1(N) 16 ...... 10 .0 Cucumber ...... 0 .1(N) Grain, cereal, group 15, except corn ...... 4 .0 Muskmelon ...... 0 .1(N) Grape ...... 1 .0 Watermelon ...... 0.1(N) Grape, raisin ...... 5 .0 Grass, forage, fodder, and hay group 17, forage ...... 3 .5 (b) Section 18 emergency exemptions. Grass, forage, fodder, and hay group 17, hay .. 18 .0 [Reserved] Herb and spice, group 19 ...... 5 .0 Hog, fat ...... 0 .005 (c) Tolerances with regional registra- Hog, kidney ...... 0.10 tions. [Reserved] Hog, liver ...... 0 .05 (d) Indirect or inadvertent residues. Hog, meat ...... 0 .01 Milk ...... 0.03 [Reserved] Nut, tree, group 14 ...... 0 .05 Okra ...... 0.05 [45 FR 32306, May 16, 1980, as amended at 63 Pea and bean, dried shelled, subgroup 6C ...... 0 .2 FR 57075, Oct. 26, 1998]

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§ 180.298 Methidathion; tolerances for (d) Indirect or inadvertent residues. residues. [Reserved] (a) General. Tolerances are estab- [43 FR 44845, Sept. 29, 1978] lished for residues of the insecticide EDITORIAL NOTE: For FEDERAL REGISTER ci- methidathion, including its metabo- tations affecting § 180.298, see the List of CFR lites and degradates, in or on the com- Sections Affected, which appears in the modities in the table in this paragraph. Finding Aids section of the printed volume Compliance with the tolerance levels and at www.fdsys.gov. specified in this paragraph is to be de- § 180.299 Dicrotophos; tolerances for termined by measuring only residues. methidathion, S-[(5-methoxy-2-oxo- 1,3,4-thiadiazol-3(2H)-yl)methyl] O,O- (a) General. Tolerances are estab- dimethyl phosphorodithioate, in or on lished for residues of the insecticide the commodity. dicrotophos, dimethyl phosphate of 3- hydroxy-N,N-dimethyl-cis- crotonamide, in or on the following Parts per Expiration/ Commodity revocation food commodities: million date Parts per Almond, hulls ...... 6.0 12/31/16 Commodity million Artichoke, globe ...... 0.05 12/31/16 Citrus, oil ...... 420.0 12/31/16 Cotton, gin byproducts ...... 2 .0 Cotton, undelinted seed ...... 0.2 12/31/16 Cotton, undelinted seed ...... 0 .2 Fruit, citrus, group 10, except tangerine ...... 4.0 12/31/16 (b) Section 18 emergency exemptions. Fruit, pome, group 11 ...... 0.05 12/31/16 [Reserved] Fruit, stone, group 12 ...... 0.05 12/31/16 (c) Tolerances with regional registra- Mango ...... 0.05 12/31/16 Nut, tree, group 14 ...... 0.05 12/31/16 tions. [Reserved] Olive ...... 0.05 12/31/16 (d) Indirect or inadvertent residues. Safflower, seed ...... 0.5 12/31/16 [Reserved] Sorghum, forage, forage ...... 2.0 12/31/16 Sorghum, grain, forage ...... 2.0 12/31/16 [73 FR 52613, Sept. 10, 2008] Sorghum, grain, grain ...... 0.2 12/31/16 Sorghum, grain, stover ...... 2.0 12/31/16 § 180.300 Ethephon; tolerances for resi- Sunflower, seed ...... 0.5 12/31/16 dues. Tangerine ...... 6.0 12/31/16 (a) General. Tolerances are established for residues of the plant regu- (b) Section 18 emergency exemptions. lator ethephon [(2-chloroethyl) phos- [Reserved] phonic acid] in or on food commodities (c) Tolerances with regional registra- as follows: tions. Tolerances with regional reg- Parts per istration, as defined in § 180.1(l), are es- Commodity million tablished for residues of the insecticide methidathion, including its metabo- Apple ...... 5.0 Apple, juice ...... 10 .0 lites and degradates, in or on the com- Barley, bran ...... 5 .0 modities in the table in this paragraph. Barley, grain ...... 2 .0 Compliance with the tolerance levels Barley, straw ...... 10 .0 Blackberry ...... 30 .0 specified in this paragraph is to be de- Blueberry ...... 20 .0 termined by measuring only Cantaloupe ...... 2 .0 methidathion, S-[(5-methoxy-2-oxo- Cattle, fat ...... 0.02 1,3,4-thiadiazol-3(2H)-yl)methyl] O,O- Cattle, kidney ...... 1 .0 Cattle, meat ...... 0 .02 dimethyl phosphorodithioate, in or on Cattle, meat byproducts, except kidney ...... 0.2 the commodity. Cherry ...... 10.0 Coffee, bean, green ...... 0 .5 Expiration/ Cotton, gin byproducts ...... 180.0 Parts per Cotton, undelinted seed ...... 6 .0 Commodity million revocation date Cucumber ...... 0 .1 Egg ...... 0 .002 Kiwifruit ...... 0.1 12/31/16 Goat, fat ...... 0 .02 Longan ...... 0.1 12/31/16 Goat, kidney ...... 1 .0 Starfruit ...... 0.1 12/31/16 Goat, meat ...... 0.02 Sugar apple ...... 0.2 12/31/16 Goat, meat byproducts, except kidney ...... 0 .2 Grape ...... 2 .0

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Parts per Parts per Commodity million Commodity million

Grape, raisin ...... 12.0 Cattle, meat byproducts ...... 0.1 Hazelnut ...... 0 .80 Cattle, meat ...... 0 .05 Hog, fat ...... 0 .02 Corn, field, forage ...... 0 .2 Hog, kidney ...... 1.0 Corn, field, grain ...... 0 .2 Hog, meat ...... 0 .02 Corn, field, stover ...... 0 .2 Hog, meat byproducts, except kidney ...... 0 .2 Corn, pop, grain ...... 0.2 Horse, fat ...... 0 .02 Corn, pop, stover ...... 0.2 Horse, kidney ...... 1 .0 Corn, sweet, forage ...... 0 .2 Horse, meat ...... 0 .02 Corn, sweet, kernel plus cob with husks re- Horse, meat byproducts, except kidney ...... 0 .2 moved ...... 0 .2 Milk ...... 0.01 Corn, sweet, stover ...... 0 .2 Nut, macadamia ...... 0.5 Cotton, undelinted seed ...... 0 .2 Pepper ...... 30.0 Egg ...... 0 .05 Pineapple ...... 2.0 Goat, fat ...... 0 .05 Poultry, fat ...... 0.02 Goat, meat byproducts ...... 0 .1 Poultry, liver ...... 0 .05 Goat, meat ...... 0.05 Poultry, meat ...... 0 .01 Hog, fat ...... 0 .05 Poultry, meat byproducts, except liver ...... 0 .01 Hog, meat byproducts ...... 0 .1 Sheep, fat ...... 0 .02 Hog, meat ...... 0 .05 Sheep, kidney ...... 1.0 Horse, fat ...... 0 .05 Sheep, meat ...... 0.02 Horse, meat byproducts ...... 0 .1 Sheep, meat byproducts, except kidney ...... 0 .2 Horse, meat ...... 0 .05 Sugarcane, molasses ...... 1 .5 Milk ...... 0.05 Tomato ...... 2.0 Oat, forage ...... 0 .5 Walnut ...... 0 .5 Oat, grain ...... 0 .2 Wheat, bran ...... 5.0 Oat, straw ...... 0.2 Wheat, germ ...... 5 .0 Onion, bulb ...... 0 .2 Wheat, grain ...... 2 .0 Peanut ...... 0 .2 Wheat, middlings ...... 5 .0 Peanut, hay ...... 0.2 Wheat, shorts ...... 5 .0 Poultry, fat ...... 0.1 Poultry, meat byproducts ...... 0.1 Wheat, straw ...... 10 .0 Poultry, meat ...... 0 .1 Rice, grain ...... 0 .2 (b) Section 18 emergency exemptions. Rice, straw ...... 0 .2 [Reserved] Safflower, seed ...... 0 .2 Sheep, fat ...... 0 .05 (c) Tolerances with regional registra- Sheep, meat byproducts ...... 0 .1 tions. A tolerance with regional reg- Sheep, meat ...... 0.05 istration, as defined in § 180.1(m), of 0.1 Soybean, seed ...... 0 .2 part per million is established for resi- Wheat, forage ...... 0 .5 Wheat, grain ...... 0 .2 dues of the plant regulator ethephon Wheat, straw ...... 0 .2 [(2-chloroethyl)phosphonic acid] in or on the food commodity sugarcane. (b) Section 18 emergency exemptions. (d) Indirect or inadvertent residues. [Reserved] [Reserved] (c) Tolerances with regional registrations. [Reserved] [65 FR 33710, May 24, 2000, as amended at 72 FR 53455, Sept. 19, 2007; 75 FR 56015, Sept. 15, (d) Indirect or inadvertent residues. 2010] [Reserved] [47 FR 55222, Dec. 8, 1982, as amended at 50 § 180.301 Carboxin; tolerances for resi- FR 81, Jan. 2, 1985; 62 FR 4915, Feb. 3, 1997; 63 dues. FR 4586, Jan. 30, 1998; 64 FR 11801, Mar. 10, (a) General. Tolerances are estab- 1999; 66 FR 9773, Feb. 12, 2001; 66 FR 64773, lished for the combined residues of the Dec. 14, 2001; 67 FR 40218, June 12, 2002; 67 FR fungicide carboxin (5,6-dihydro-2-meth- 72853, Dec. 9, 2002; 71 FR 56383, Sept. 27, 2006] yl-1,4-oxathiin-3-carboxanilide) and its § 180.303 Oxamyl; tolerances for resi- metabolites determined as aniline and dues. expressed as parent compound, in or on food commodities as follows: (a) General. Tolerances are established for the combined residues of the Commodity Parts per insecticide oxamyl, methyl N,N-di- million methyl-N-[(methylcarbamoyl)-oxy]-1- Barley, grain ...... 0 .2 thiooxamimidate, and its oxime me- Barley, straw ...... 0 .2 tabolite methyl N,N-dimethyl-N-hy- Bean, dry, seed ...... 0 .2 droxy-1-thiooxamimidate calculated as Bean, succulent ...... 0 .2 Canola, seed ...... 0 .03 oxamyl in or on the following food Cattle, fat ...... 0.05 commodities:

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istration, as defined in § 180.1(l), are es- Commodity Parts per million tablished for residues of oryzalin, 3,5- Apple ...... 2 dinitro-N4,N4-dipropylsulfanilamide, in Banana ...... 0.3 or on the following raw agricultural Cantaloupe ...... 2 .0 commodities: Carrot ...... 0 .1 Celery ...... 10 .0 Cotton, undelinted seed ...... 0 .2 Parts per Commodity million Cucumber ...... 2 .0 Eggplant ...... 2.0 Fruit, citrus, group 10 ...... 3 Guava ...... 0 .05 Garlic, bulb ...... 0.2 Papaya ...... 0 .05 Melon, honeydew ...... 2.0 Onion, bulb ...... 0 .2 (d) Indirect or inadvertent residues. Peanut ...... 0 .05 Peanut, hay ...... 2.0 [Reserved] Pear ...... 2 .0 Peppermint, tops ...... 10 .0 [71 FR 54434, Sept. 15, 2006, as amended at 76 Pepper, bell ...... 2 .0 FR 34885, June 15, 2011] Pepper, nonbell ...... 5 .0 Pineapple ...... 1 § 180.311 Cacodylic acid; tolerances for Pineapple, process residue ...... 2 .0 Pumpkin ...... 2.0 residues. Soybean, seed ...... 0 .1 (a) General. A tolerance is established Spearmint, tops ...... 10 .0 Squash, summer ...... 2 .0 for residues of the defoliant cacodylic Squash, winter ...... 2 .0 acid, dimethylarsinic acid, including Tomato ...... 2 its metabolites and degradates, in or Vegetable, tuberous and corm, subgroup 1C ..... 0.1 Watermelon ...... 2.0 on the commodity in the following table. Compliance with the tolerance (b) Section 18 emergency exemptions. level specified in this paragraph is to [Reserved] be determined by measuring only those (c) Tolerances with regional registra- cacodylic acid residues convertible to tions. [Reserved] As2O3, expressed as the stoichiometric (d) Indirect or inadvertent residues. equivalent of cacodylic acid, in or on [Reserved] the commodity. [73 FR 54961, Sept. 24, 2008] Parts per Expiration/ Commodity million Revocation § 180.304 Oryzalin; tolerances for resi- Date dues. Cotton, undelinted seed ...... 2.8 1/1/12 (a) General. Tolerances are established for residues of the herbicide (b) Section 18 emergency exemptions. oryzalin, 3,5-dinitro-N4,N4- [Reserved] dipropylsulfanilamide, in or on the fol- (c) Tolerances with regional registra- lowing raw agricultural commodities: tions. [Reserved]

Parts per (d) Indirect or inadvertent residues. Commodity million [Reserved]

Almond, hulls ...... 0 .05 [69 FR 6567, Feb. 11, 2004, as amended at 75 Avocado ...... 0 .05 FR 60243, Sept. 29, 2010] Berry group 13 ...... 0 .05 Cranberry ...... 0 .05 Fig ...... 0 .05 § 180.314 Triallate; tolerances for resi- Fruit, citrus, group 10 ...... 0 .05 dues. Fruit, pome, group 11 ...... 0.05 Fruit, stone, group 12 ...... 0 .05 (a) General. Tolerances are estab- Grape ...... 0 .05 lished for residues of triallate, S-2,3,4- Kiwifruit ...... 0.05 trichloroallyl Nut, tree, group 14 ...... 0 .05 Olive ...... 0 .05 diisopropylthiocarbamate and its me- Pistachio ...... 0.05 tabolite 2,3,3-trichloroprop-2- Pomegranate ...... 0 .05 enesulfonic acid (TCPSA) in or on the Strawberry ...... 0 .05 following food commodity:

(b) Section 18 emergency exemptions. Parts per [Reserved] Commodity million (c) Tolerances with regional registrations. Tolerances with regional reg- Bermudagrass, hay ...... 0.3

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(b) Section 18 emergency exemptions. istration is established for residues of [Reserved] methamidophos, O,S-dimethyl (c) Tolerances with regional registra- phosphoramidothioate, including its tions. Tolerances with a regional reg- metabolites and degradates, in or on istration, as defined in 180.1(l),are es- the commodity in the following table tablished for residues of the herbicide as a result of the application of (S-2, 3, 4-trichloroallyl methamidophos. Compliance with the diisopropylthiocarbamate) and its me- tolerance levels specified in this para- tabolite 2, 3, 3-trichloroprop-2- graph is to be determined by measuring enesulfonic acid (TCPSA) in or on the only methamidophos, O,S-dimethyl following food commodities: phosphoramidothioate, in or on the commodity. Parts per Commodity million Expiration/ Commodity Parts per Revocation Barley, grain ...... 0 .05 million Date Barley, hay ...... 1 .0 Barley, straw ...... 0 .3 Tomato ...... 2.0 12/31/13 Beet, sugar, dried pulp ...... 0 .2 Beet, sugar, roots ...... 0 .1 Beet, sugar, tops ...... 0.5 (d) Indirect or inadvertent residues. Pea, dry ...... 0 .2 [Reserved] Pea, field, hay ...... 1.0 Pea, field, vines ...... 0 .5 [75 FR 60243, Sept. 29, 2010] Pea, succulent ...... 0 .2 Wheat, forage ...... 0 .5 § 180.316 Pyrazon; tolerances for resi- Wheat, grain ...... 0 .05 dues. Wheat, hay ...... 1 .0 Wheat, straw ...... 1 .0 (a) General. Tolerances are established for combined residues of the her- (d) Indirect or inadvertent residues. bicide pyrazon (5-amino-4-chloro-2- [Reserved] phenyl-3(2H)-pyridazinone) and its me- [72 FR 28888, May 23, 2007, as amended at 73 tabolites (calculated as pyrazon) in or FR 5109, Jan. 29, 2008; 73 FR 53738, Sept. 17, on the following food commodities: 2008; 74 FR 29963, June 24, 2009] Parts per Commodity million § 180.315 Methamidophos; tolerances for residues. Beet, garden, roots ...... 0 .9 Beet, garden, tops ...... 7 .0 (a) General. Tolerances are estab- Beet, sugar, molasses ...... 1 .5 lished for residues of methamidophos, Beet, sugar, roots ...... 0 .2 O,S-dimethyl phosphoramidothioate, Beet, sugar, tops ...... 3.0 including its metabolites and Cattle, fat ...... 0.10 Cattle, liver ...... 0 .15 degradates, in or on the commodities Cattle, meat ...... 0 .10 in the following table as a result of the Cattle, meat byproducts, except liver ...... 0 .10 application of methamidophos. Compli- Goat, fat ...... 0 .10 ance with the tolerance levels specified Goat, liver ...... 0.15 Goat, meat ...... 0.10 in this paragraph is to be determined Goat, meat byproducts, except liver ...... 0 .10 by measuring only methamidophos, Horse, fat ...... 0 .10 O,S-dimethyl phosphoramidothioate, in Horse, liver ...... 0 .15 Horse, meat ...... 0 .10 or on the commodity. Horse, meat byproducts, except liver ...... 0 .10 Milk ...... 0.02 Expiration/ Sheep, fat ...... 0 .10 Commodity Parts per Revocation million Date Sheep, liver ...... 0.15 Sheep, meat ...... 0.10 Broccoli1 ...... 1.0 12/31/12 Sheep, meat byproducts, except liver ...... 0 .10 Cabbage2 ...... 1.0 12/31/12 Cotton, undelinted seed ...... 0.1 12/31/13 (b) Section 18 emergency exemptions. Potato ...... 0.1 12/31/13 [Reserved] 1 There are no U.S. registrations since 1989. (c) Tolerances with regional registra- 2 There are no U.S. registrations since 2001. tions. [Reserved] (b) Section 18 emergency exemptions. (d) Indirect or inadvertent residues. [Reserved] Tolerances are established for com- (c) Tolerances with regional registra- bined residues of the herbicide pyrazon, tions. A tolerance with a regional reg- 5-amino-4-chloro-2-phenyl-3(2H)-

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pyridazinone, and its metabolites (cal- Commodity Parts per culated as pyrazon), in or on the fol- million lowing food commodities: Milk ...... 0.02 Pear ...... 0 .1 Parts per Poultry, fat ...... 0.02 Commodity million Poultry, liver ...... 0 .2 Corn, field, forage ...... 0 .5 Poultry, meat ...... 0 .02 Corn, field, stover ...... 0 .5 Poultry, meat byproducts, except liver ...... 0 .02 Soybean, forage ...... 0 .5 Radicchio ...... 2.0 Soybean, hay ...... 0 .5 Raspberry ...... 0 .05 Wheat, forage ...... 0 .3 Sheep, fat ...... 0 .2 Wheat, hay ...... 0 .2 Sheep, kidney ...... 0.4 Wheat, straw ...... 0 .1 Sheep, liver ...... 0.4 Sheep, meat ...... 0.02 Sheep, meat byproducts, except kidney and [68 FR 39441, July 1, 2003, as amended at 73 liver ...... 0 .02 FR 52614, Sept. 10, 2008] (b) Section 18 emergency exemptions. § 180.317 Propyzamide; tolerances for [Reserved] residues. (c) Tolerances with regional registra- (a) General. Tolerances are estab- tions. Tolerances with regional reg- lished for residues of the herbicide istration, as defined in § 180.1(l), are es- propyzamide, including its metabolites tablished for residues of the herbicide and degradates, in or on the commod- propyzamide, including its metabolites ities in the table in this paragraph. and degradates, in or on the commod- Compliance with the tolerance levels ities in the table in this paragraph. specified in this paragraph is to be de- Compliance with the tolerance levels termined by measuring only those specified in this paragraph is to be de- propyzamide residues convertible to termined by measuring only those methyl 3,5-dichlorobenzoate, expressed propyzamide residues convertible to as the stoichiometric equivalent of methyl 3,5-dichlorobenzoate, expressed propyzamide, 3,5-dichloro-N-(1,1-di- as the stoichiometric equivalent of methyl-2-propynyl)benzamide, in or on propyzamide, 3,5-dichloro-N-(1,1-di- the commodity. methyl-2-propynyl)benzamide, in or on the commodity. Parts per Commodity million Commodity Parts per Alfalfa, seed ...... 10 .0 million Animal feed, nongrass, group 18 ...... 10 .0 Apple ...... 0.1 Pea, field, seed ...... 0 .05 Artichoke, globe ...... 0.01 Rhubarb ...... 0 .1 Blackberry ...... 0 .05 Blueberry ...... 0 .05 (d) Indirect or inadvertent residues. Boysenberry ...... 0 .05 Tolerances are established for indirect Cattle, fat ...... 0.2 Cattle, kidney ...... 0 .4 or inadvertent residues of the herbicide Cattle, liver ...... 0 .4 propyzamide, including its metabolites Cattle, meat ...... 0 .02 and degradates, in or on the commod- Cattle, meat byproducts, except kidney and liver 0.02 Egg ...... 0 .02 ities in the table in this paragraph. Endive ...... 1.0 Compliance with the tolerance levels Fruit, stone, group 12 ...... 0 .1 specified in this paragraph is to be de- Goat, fat ...... 0 .2 Goat, kidney ...... 0 .4 termined by measuring only those Goat, liver ...... 0.4 propyzamide residues convertible to Goat, meat ...... 0.02 methyl 3,5-dichlorobenzoate, expressed Goat, meat byproducts, except kidney and liver 0 .02 as the stoichiometric equivalent of Grape ...... 0 .1 Hog, fat ...... 0 .2 propyzamide, 3,5-dichloro-N-(1,1-di- Hog, kidney ...... 0.4 methyl-2-propynyl)benzamide, in or on Hog, liver ...... 0 .4 the commodity. Hog, meat ...... 0 .02 Hog, meat byproducts, except kidney and liver .. 0 .02 Parts per Horse, fat ...... 0 .2 Commodity million Horse, kidney ...... 0 .4 Horse, liver ...... 0 .4 Grain, cereal, forage, group 16 ...... 0 .6 Horse, meat ...... 0 .02 Grain, cereal, hay, group 16 ...... 0 .2 Horse, meat byproducts, except kidney and liver 0 .02 Grain, cereal, straw, group 16 ...... 0 .3 Lettuce, head ...... 1.0

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[72 FR 52018, Sept. 12, 2007, as amended at 76 Commodity Parts per FR 23493, Apr. 27, 2011] million

Peppermint, tops ...... 0 .20 § 180.318 4-(2-Methyl-4-chlorophenoxy) Spearmint, tops ...... 0 .20 butyric acid; tolerance for residues. (a) General. (1) A tolerance is estab- (b) Section 18 emergency exemptions. lished for the herbicide 4-(2-methyl-4- [Reserved] chlorophenoxy) butyric acid in or on (c) Tolerances with regional registra- the following food commodity: tions. [Reserved] (d) Indirect or inadvertent residues. Parts per [Reserved] Commodity million [68 FR 39441, July 1, 2003, as amended at 73 Pea ...... 0 .1(N) FR 66785, Nov. 12, 2008]

(2) Tolerances are established for the § 180.319 Interim tolerances. combined residues, free and con- (a) General. While petitions for toler- jugated, of the herbicide MCPB, 4-(4- ances for negligible residues are pend- chloro-2-methylphenoxy)butanoic acid, ing and until action is completed on and its metabolite MCPA, (4-chloro-2- these petitions, interim tolerances are methylphenoxy)acetic acid, in or on established for residues of the listed the following food commodities: pesticide chemicals in or on the following raw agricultural commodities:

Raw Expiration/ Substances Uses Tolerance in parts per million agricultural revocation commodity date

Coordination product of zinc ion Fungicide ...... 1.0 (Calculated as zinc ethylene- Potato ...... None and maneb. bisdithio-carbamate). Endothall (7-oxabicyclo- Herbicide ...... 0.2 ...... Beet, sugar ...... None (2,2,1)heptane 2,3-dicarboxylic acid. Methyl parathion ...... Herbicide ...... 0.5 ...... Rye ...... 12/31/13

(b) Section 18 emergency exemptions. Commodity Parts per [Reserved] million (c) Tolerances with regional registra- Alfalfa, forage ...... 0.1 tions. [Reserved] Alfalfa, hay ...... 0.5 (d) Indirect or inadvertent residues. Barley, grain ...... 0 .05 Barley, hay ...... 9 .0 [Reserved] Barley, straw ...... 4 .0 [77 FR 59126, Sept. 26, 2012] Corn, field, forage ...... 0 .3 Corn, field, grain ...... 0 .05 EFFECTIVE DATE NOTE: At 79 FR 27502, May Corn, field, stover ...... 0 .2 14, 2014, § 180.319 was amended by removing Corn, pop, grain ...... 0.05 Corn, pop, stover ...... 0.2 the entry for ‘‘Coordination product of zinc Flax, seed ...... 0 .1 ion and maneb’’ from the table in paragraph Garlic ...... 0 .1 (a), effective Nov. 14, 2014. Grain, aspirated fractions ...... 1 .2 Grass, forage ...... 18 § 180.324 Bromoxynil; tolerances for Grass, hay ...... 5 .0 residues. Oat, forage ...... 0 .3 Oat, grain ...... 0 .05 (a) General. (1) Tolerances are estab- Oat, hay ...... 9.0 lished for residues of the herbicide Oat, straw ...... 4.0 Onion, bulb ...... 0 .1 bromoxynil, including its metabolites Peppermint, hay ...... 0 .1 and degradates, in or on the commod- Rye, forage ...... 1 .0 ities in the table below. Compliance Rye, grain ...... 0.05 Rye, straw ...... 2 .0 with the tolerance levels is to be deter- Sorghum, grain, forage ...... 0.8 mined by measuring only bromoxynil, Sorghum, grain, grain ...... 0 .2 3,5-dibromo-4-hydroxybenzonitrile, re- Sorghum, grain, stover ...... 0 .2 sulting from application of its octanoic Spearmint, hay ...... 0 .1 Wheat, forage ...... 1 .0 and/or heptanoic acid ester, in or on Wheat, grain ...... 0 .05 the commodities. Wheat, hay ...... 4 .0

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Parts per Expiration/ Commodity million Commodity Parts per revocation million date Wheat, straw ...... 2 .0 Almond, hulls ...... 0.1 None Asparagus ...... 0.1 None (2) Tolerances are established for res- Basil ...... 0.1 None idues of the herbicide bromoxynil, 3,5- Berry group 13 ...... 0.1 None dibromo-4-hydroxybenzonitrile, includ- Coffee, green bean ...... 0.1 None Cranberry ...... 0.1 None ing its metabolites and degradates, in Grape ...... 0.1 None or on the commodities in the table Kiwifruit ...... 0.1 None below. Compliance with the tolerance Marjoram ...... 0.1 None Nut, tree, group 14 ...... 0.1 None levels is to be determined by meas- Peppermint, tops ...... 0.1 None uring only bromoxynil and its metabo- Persimmon ...... 0.1 None lite, 3,5-dibromo-4-hydroxybenzoic acid Rhubarb ...... 0.1 None Rosemary ...... 0.1 None (DBHA), resulting from application of Savory, summer ...... 0.1 None its octanoic and/or heptanoic acid Savory, winter ...... 0.1 None ester, in or on the commodities. Spearmint, tops ...... 0.1 None Strawberry ...... 0.1 None Parts per Sweet potato, roots ...... 0.1 None Commodity million Vegetable, brassica, leafy, group 5 0.1 None Vegetable, fruiting, group 8 ...... 0.1 None Cattle, fat ...... 1 Cattle, meat byproducts ...... 3.5 (b) Section 18 emergency exemptions. Cattle, meat ...... 0 .5 [Reserved] Cotton, gin byproducts ...... 7 .0 (c) Tolerances with regional registra- Cotton, hulls ...... 5 .0 Cotton, undelinted seed ...... 1 .5 tions. [Reserved] Egg ...... 0 .05 (d) Indirect or inadvertent residues. Goat, fat ...... 1 [Reserved] Goat, meat byproducts ...... 3 .5 Goat, meat ...... 0.5 [73 FR 52614, Sept. 10, 2008, as amended at 76 Hog, fat ...... 1 FR 34885, June 15, 2011] Hog, meat byproducts ...... 3 .5 Hog, meat ...... 0 .5 § 180.330 S-(2-(Ethylsulfinyl)ethyl) O,O- Horse, fat ...... 1 dimethyl phosphorothioate; toler- Horse, meat byproducts ...... 3 .5 ances for residues. Horse, meat ...... 0 .5 (a) General. (1) Tolerances are estab- Milk ...... 0.4 Poultry, fat ...... 0.05 lished for the combined residues of the Poultry, meat byproducts ...... 0.3 insecticide oxydemeton-methyl (S-(2- Poultry, meat ...... 0 .05 (ethylsulfinyl)ethyl) O,O-dimethyl Sheep, fat ...... 1 phosphorothioate) and its metabolite Sheep, meat byproducts ...... 3 .5 oxydemeton-methyl sulfone in or on Sheep, meat ...... 0.5 the following food commodities: (b) Section 18 emergency exemptions. Commodity Parts per [Reserved] million (c) Tolerances with regional registra- Alfalfa, forage ...... 5.0 tions. [Reserved] Alfalfa, hay ...... 11.0 (d) Indirect or inadvertent residues. Bean, lima ...... 0 .2 Beet, sugar, roots ...... 0 .3 [Reserved] Beet, sugar, tops ...... 0.5 Broccoli ...... 1 .0 [62 FR 33023, June 18, 1997, as amended at 63 Brussels sprouts ...... 1 .0 FR 26480, May 13, 1998; 66 FR 47402, Sept. 12, Cabbage ...... 2 .0 2001; 70 FR 7046, Feb. 10, 2005; 72 FR 35666, Cauliflower ...... 1 .0 June 29, 2007; 72 FR 41930, Aug. 1, 2007; 76 FR Clover, forage ...... 5.0 31491, June 1, 2011] Clover, hay ...... 10.0 Corn, sweet, forage ...... 1 .0 Corn, sweet, kernel plus cob with husks re- § 180.328 Napropamide; tolerances for moved ...... 0 .5 residues. Corn, sweet, stover ...... 3 .0 Cotton, undelinted seed ...... 0 .02 (a) General. Tolerances are estab- Cucumber ...... 1 .0 lished for residues of the herbicide Eggplant ...... 1.0 napropamide, N,N-diethyl-2-(1- Grapefruit ...... 1 .0 Hazelnut ...... 0 .05 napthalenyloxy) propionamide, in or on Lemon ...... 1.0 the following food commodities: Lettuce, head ...... 2.0

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Commodity Parts per § 180.331 4-(2,4-Dichlorophenoxy) bu- million tyric acid; tolerances for residues. Melon ...... 0 .2 (a) General. Tolerances are estab- Onion, bulb ...... 0 .05 lished for residues of the herbicide 4- Orange ...... 1 .0 Pepper ...... 0 .75 (2,4-dichlorophenoxy) butyric acid (2,4- Peppermint, tops ...... 12 .5 DB), both free and conjugated, deter- Pumpkin ...... 0.2 mined as the acid, in or on food com- Safflower, seed ...... 1 .0 Sorghum, forage, forage ...... 2 .0 modities, as follows: Sorghum, grain, forage ...... 2.0 Sorghum, grain, grain ...... 0 .75 Commodity Parts per Spearmint, tops ...... 12 .5 million Squash, summer ...... 1 .0 Squash, winter ...... 0 .3 Alfalfa, forage ...... 0.7 Strawberry ...... 2 .0 Alfalfa, hay ...... 2.0 Walnut ...... 0 .05 Cattle, meat byproducts ...... 0.05 Clover, forage ...... 0.2 Clover, hay ...... 0.2 (2) Tolerances are established for the Goat, meat byproducts ...... 0 .05 combined residues of the insecticide Hog, meat byproducts ...... 0 .05 oxydemeton-methyl (S-(2- Horse, meat byproducts ...... 0 .05 Peanut ...... 0 .2 (ethylsulfinyl)ethyl) O,O-dimethyl Peppermint, tops ...... 0 .2 phosphorothioate) and its cholin- Sheep, meat byproducts ...... 0 .05 esterase-inhibiting metabolites in or Soybean, forage ...... 0 .7 Soybean, hay ...... 2 .0 on the following food commodities: Soybean, seed ...... 0 .5 Spearmint, tops ...... 0 .2 Commodity Parts per Trefoil, forage ...... 0 .7 million Trefoil, hay ...... 2 .0 Cattle, fat ...... 0.01 Cattle, meat ...... 0 .01 (b) Section 18 emergency exemptions. Cattle, meat byproducts ...... 0.01 [Reserved] Egg ...... 0 .01 (c) Tolerances with regional registra- Goat, fat ...... 0 .01 Goat, meat ...... 0.01 tions. [Reserved] Goat, meat byproducts ...... 0 .01 (d) Indirect or inadvertent residues. Hog, fat ...... 0 .01 [Reserved] Hog, meat ...... 0 .01 Hog, meat byproducts ...... 0 .01 [73 FR 54961, Sept. 24, 2008, as amended at 74 Horse, fat ...... 0 .01 FR 46374, Sept. 9, 2009] Horse, meat ...... 0 .01 Horse, meat byproducts ...... 0 .01 Milk ...... 0.01 § 180.332 Metribuzin; tolerances for Poultry, fat ...... 0.01 residues. Poultry, meat ...... 0 .01 Poultry, meat byproducts ...... 0.01 (a) General. Tolerances are estab- Sheep, fat ...... 0 .01 lished for combined residues of the her- Sheep, meat ...... 0.01 bicide metribuzin (4-amino-6-(1,1- Sheep, meat byproducts ...... 0 .01 dimethylethyl)-3-(methylthio)-;1,2,4- (b) Section 18 emergency exemptions. triazin-5(4H)-one) and its triazinone [Reserved] metabolites in or on food commodities: (c) Tolerances with regional registra- Parts per tions. Tolerances with regional reg- Commodity million istrations, as defined in § 180.1(l), are Alfalfa, forage ...... 2.0 established for the combined residues Alfalfa, hay ...... 7.0 of the insecticide oxydemeton-methyl Asparagus ...... 0.1 (S-(2-(ethylsulfinyl)-ethyl) O,O-di- Barley, grain ...... 0 .75 Barley, hay ...... 7 .0 methyl phosphorothioate) and its me- Barley, pearled barley ...... 3 .0 tabolite oxydemeton-methyl sulfone in Barley, straw ...... 1 .0 or on the following food commodities: Carrot, roots ...... 0.3 Cattle, fat ...... 0.7 Commodity Parts per million Cattle, meat ...... 0 .7 Cattle, meat byproducts ...... 0.7 Broccoli raab ...... 2 .0 Corn, field, forage ...... 0 .1 Corn, field, grain ...... 0 .05 Corn, field, stover ...... 0 .1 (d) Indirect or inadvertent residues. Corn, pop, grain ...... 0.05 [Reserved] Corn, sweet, forage ...... 0 .1 Corn, sweet, kernel plus cob with husks re- [72 FR 54578, Sept. 26, 2007] moved ...... 0 .05

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ance levels specified in this paragraph Commodity Parts per million is to be determined by measuring only Corn, sweet, stover ...... 0 .1 oxytetracycline, Egg ...... 0 .01 (4S,4aR,5S,5aR,6S,12aS)-4- Goat, fat ...... 0 .7 (dimethylamino)-1,4,4a,5,5a,6,11,12a- Goat, meat ...... 0.7 Goat, meat byproducts ...... 0 .7 octahydro-3,5,6,10,12,12a-hexahydroxy- Grass, forage ...... 2 .0 6-methyl-1,11-dioxo-2- Grass, hay ...... 7 .0 naphthacenecarboxamide, in or on the Hog, fat ...... 0 .7 Hog, meat ...... 0 .7 commodity. Hog, meat byproducts ...... 0 .7 Horse, fat ...... 0 .7 Parts per Commodity million Horse, meat ...... 0 .7 Horse, meat byproducts ...... 0 .7 Apple ...... 0.35 Lentil ...... 0.05 Peach ...... 0 .35 Milk ...... 0.05 Pear ...... 0 .35 Pea, dry, seed ...... 0 .05 Pea, field, hay ...... 4.0 Pea, field, vines ...... 0 .5 (b) Section 18 emergency exemptions. Pea, succulent ...... 0 .1 [Reserved] Potato ...... 0 .6 (c) Tolerances with regional registra- Potato, chips ...... 3 .0 Potato, processed potato waste ...... 3 .0 tions. [Reserved] Poultry, fat ...... 0.7 (d) Indirect or inadvertent residues. Poultry, meat ...... 0 .7 [Reserved] Poultry, meat byproducts ...... 0.7 Sainfoin, forage ...... 2 .0 [76 FR 23493, Apr. 27, 2011] Sainfoin, hay ...... 7 .0 Sheep, fat ...... 0 .7 Sheep, meat ...... 0.7 § 180.339 MCPA; tolerances for resi- Sheep, meat byproducts ...... 0 .7 dues. Soybean, seed ...... 0 .3 (a) General. (1) Tolerances are estab- Soybean, forage ...... 4 .0 Soybean, hay ...... 4 .0 lished for residues of the herbicide Sugarcane, cane ...... 0.1 MCPA ((4-chloro-2- Sugarcane, molasses ...... 2 .0 methylphenoxy)acetic acid), both free Tomato ...... 0.1 Wheat, bran ...... 3.0 and conjugated, resulting from the di- Wheat, forage ...... 2 .0 rect application of MCPA or its sodium Wheat, germ ...... 3 .0 or dimethylamine salts, or its 2- Wheat, grain ...... 0 .75 ethylhexyl ester in or on the following Wheat, hay ...... 7 .0 Wheat, middlings ...... 3 .0 food commodities: Wheat, shorts ...... 3 .0 Wheat, straw ...... 1 .0 Parts per Commodity million

(b) Section 18 emergency exemptions. Alfalfa, forage ...... 0.5 [Reserved] Alfalfa, hay ...... 2.0 Barley, grain ...... 1 .0 (c) Tolerances with regional registra- Barley, hay ...... 40 tions. [Reserved] Barley, straw ...... 25 (d) Indirect or inadvertent residues. Clover, forage ...... 0.5 [Reserved] Clover, hay ...... 2.0 Flax, seed ...... 0 .1 [42 FR 62913, Dec. 14, 1977, as amended at 43 Grain, aspirated fractions ...... 3 .0 FR 41396, Sept. 18, 1978; 44 FR 26744, May 7, Grass, forage ...... 300 Grass, hay ...... 20 1979; 44 FR 45387, Aug. 2, 1979; 52 FR 23654, Lespedeza, forage ...... 0 .5 June 24, 1987; 55 FR 26440, June 28, 1990; 62 FR Lespedeza, hay ...... 2.0 66024, 66025, Dec. 17, 1997; 65 FR 33698, May 24, Oat, forage ...... 20 2000; 66 FR 63198, Dec. 5, 2001; 67 FR 49617, Oat, grain ...... 1 .0 July 31, 2002] Oat, hay ...... 115 Oat, straw ...... 25 Pea, dry ...... 0 .1 § 180.337 Oxytetracycline; tolerances Pea, field, hay ...... 0.1 for residues. Pea, succulent ...... 0 .1 (a) General. Tolerances are estab- Pea, field, vines ...... 0 .1 Rye, forage ...... 20 lished for residues of the fungicide/ Rye, grain ...... 1.0 bactericide oxytetracycline, including Rye, straw ...... 25 its metabolites and degradates, in or Trefoil, forage ...... 0 .5 Trefoil, hay ...... 2 .0 on the commodities in the table in this Vetch, forage ...... 0 .5 paragraph. Compliance with the toler- Vetch, hay ...... 2 .0

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(d) Indirect or inadvertent residues. Commodity Parts per million [Reserved] Wheat, forage ...... 20 [40 FR 29715, July 15, 1975, as amended at 63 Wheat, grain ...... 1 .0 FR 57076, Oct. 26, 1998; 69 FR 43924, July 23, Wheat, hay ...... 115 Wheat, straw ...... 25 2004]

(2) Tolerances are established for res- § 180.342 Chlorpyrifos; tolerances for idues of the herbicide MCPA ((4-chloro- residues. 2-methylphenoxy)acetic acid) resulting (a) General. (1) Tolerances are estab- from the direct application of MCPA or lished for residues of the pesticide its sodium or dimethylamine salts, or chlorpyrifos per se (O,O-diethyl-O- its 2-ethylhexyl ester in or on the fol- (3,5,6-trichloro-2-pyridyl) lowing food commodities: phosphorothioate) in or on the following food commodities: Commodity Parts per million Parts per Commodity million Cattle, fat ...... 0.1 Cattle, meat ...... 0 .1 Alfalfa, forage ...... 3.0 Cattle, meat byproducts ...... 0.1 Alfalfa, hay ...... 13 Goat, fat ...... 0 .1 Almond ...... 0.2 Goat, meat ...... 0.1 Almond, hulls ...... 12 Goat, meat byproducts ...... 0 .1 Apple ...... 0.01 Hog, fat ...... 0 .1 Apple, wet pomace ...... 0 .02 Hog, meat ...... 0 .1 Banana ...... 0.1 Hog, meat byproducts ...... 0 .1 Beet, sugar, dried pulp ...... 5 .0 Horse, fat ...... 0 .1 Beet, sugar, molasses ...... 15 Horse, meat ...... 0 .1 Beet, sugar, roots ...... 1 .0 Horse, meat byproducts ...... 0 .1 Beet, sugar, tops ...... 8.0 Milk ...... 0.1 Cattle, fat ...... 0.3 Sheep, fat ...... 0 .1 Cattle, meat ...... 0 .05 Sheep meat ...... 0 .1 Cattle, meat byproducts ...... 0.05 Sheep meat byproducts ...... 0 .1 Cherry, sweet ...... 1 .0 Cherry, tart ...... 1 .0 (b) Section 18 emergency exemptions. Citrus, dried pulp ...... 5 .0 [Reserved] Citrus, oil ...... 20 (c) Tolerances with regional registra- Corn, field, forage ...... 8 .0 Corn, field, grain ...... 0 .05 tions. [Reserved] Corn, field, refined oil ...... 0 .25 (d) Indirect or inadvertent residues. Corn, field, stover ...... 8 .0 [Reserved] Corn, sweet, forage ...... 8 .0 Corn, sweet, kernel plus cob with husk removed 0.05 [72 FR 28888, May 23, 2007, as amended at 73 Corn, sweet, stover ...... 8 .0 FR 5109, Jan. 29, 2008] Cotton, undelinted seed ...... 0 .2 Cranberry ...... 1 .0 § 180.341 2,4-Dinitro-6-octylphenyl cro- Cucumber ...... 0 .05 Egg ...... 0 .01 tonate and 2,6-dinitro-4-octylphenyl Fig ...... 0 .01 crotonate; tolerances for residues. Fruit, citrus, group 10 ...... 1 .0 (a) General. Tolerances are estab- Goat, fat ...... 0 .2 Goat, meat ...... 0.05 lished for combined negligible residues Goat, meat byproducts ...... 0 .05 of a fungicide and insecticide that is a Hazelnut ...... 0 .2 mixture of 2,4-dinitro-6-octylphenyl Hog, fat ...... 0 .2 Hog, meat ...... 0 .05 crotonate and 2,6-dinitro-4-octylphenyl Hog, meat byproducts ...... 0 .05 crotonate in or on raw agricultural Horse, fat ...... 0 .25 commodities as follows: Horse, meat ...... 0 .25 Horse, meat byproducts ...... 0 .25 Kiwifruit ...... 2.0 Commodity Parts per million Milk, fat (Reflecting 0.01 ppm in whole milk) ...... 0 .25 Nectarine ...... 0 .05 Apple 1 ...... 0.1 Onion, bulb ...... 0 .5 Grape 1 ...... 0 .1 Peach ...... 0 .05 1 There are no U.S. registrations on apple and grape as of Peanut ...... 0 .2 October 24, 2002. Peanut, refined oil ...... 0.2 Pear ...... 0 .05 (b) Section 18 emergency exemptions. Pecan ...... 0 .2 [Reserved] Pepper ...... 1 .0 Peppermint, tops ...... 0 .8 (c) Tolerances with regional registra- Peppermint, oil ...... 8 .0 tions. [Reserved] Plum, prune, fresh ...... 0.05

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are not to be placed in exposed areas Commodity Parts per million where direct contact with food, uten- Poultry, fat ...... 0.1 sils, and food-contact surfaces would be Poultry, meat ...... 0 .1 likely to occur. Poultry, meat byproducts ...... 0.1 (vi) To assure safe use of the insecti- Pumpkin ...... 0.05 Radish ...... 2 .0 cide, its label and labeling shall con- Rutabaga ...... 0 .5 form to that registered by the U.S. En- Sheep, fat ...... 0 .2 vironmental Protection Agency, and it Sheep, meat ...... 0.05 Sheep, meat byproducts ...... 0 .05 shall be used in accordance with such Spearmint, tops ...... 0 .8 label and labeling. Spearmint, oil ...... 8 .0 (3) A tolerance of 0.1 part per million Sorghum, grain, forage ...... 0.5 is established for residues of Sorghum, grain, grain ...... 0 .5 Sorghum, grain, stover ...... 2 .0 chlorpyrifos, per se, in or on food com- Soybean, seed ...... 0 .3 modities (other than those already cov- Strawberry ...... 0 .2 ered by a higher tolerance as a result Sunflower, seed ...... 0.1 Sweet potato, roots ...... 0 .05 of use on growing crops) in food service Turnip, roots ...... 1 .0 establishments where food and food Turnip, tops ...... 0.3 products are prepared and served, as a Vegetable, brassica, leafy, group 5 ...... 1.0 Vegetable, legume, group 6. except soybean .... 0 .05 result of the application of chlorpyrifos Walnut ...... 0 .2 in microencapsulated form. Wheat, forage ...... 3 .0 (i) Application of a microencap- Wheat, grain ...... 0 .5 sulated product shall be limited solely Wheat, straw ...... 6 .0 to spot and/or crack and crevice treat- (2) Chlorpyrifos [O,O-diethyl O-(3,5,6- ment in food handling establishments trichloro-2-pyridyl) phosphorothioate] where food and food products are pre- may be safely used in accordance with pared and served. All treatments shall the following prescribed conditions. be applied in such a manner as to avoid (i) Application shall be limited solely contamination of food or food contact to spot and/or crack and crevice treat- surfaces. ment in food handling establishments (ii) Spray concentrations shall be where food and food products are held, limited to a maximum of 0.5 percent of processed, prepared or served. Contami- the active ingredient by weight. nation of food or food contact surfaces (iii) For crack and crevice treatment, shall be avoided. Food must be re- equipment capable of delivering a pin stream of spray directly into cracks moved or covered during treatment. and crevices or capable of applying (ii) Spray concentration for spot small amounts of insecticide into treatment shall be limited to a max- cracks and crevices shall be used. imum of 0.5 percent of the active ingre- (iv) For spot treatment, an individual dient by weight. A course, low-pressure spot shall not exceed 2 square feet. spray shall be used to avoid atomiza- (v) To assure safe use of the insecti- tion or splashing of the spray. cide, its label and labeling shall con- (iii) Paint-on application for spot form to that registered by the U.S. En- treatment shall be limited to a max- vironmental Protection Agency, and it imum of 2 percent of the active ingre- shall be used in accordance with such dient by weight. label and labeling. (iv) Crack and crevice treatment (b) Section 18 emergency exemptions. shall be limited to a maximum of 2 per- [Reserved] cent of the active ingredient by weight. (c) Tolerances with regional registra- Equipment capable of delivering a pin- tions. Tolerances with regional reg- stream of insecticide shall be used. istration, as defined in 180.1(l), are es- (v) Application via adhesive strips tablished for residues of the pesticide shall contain a maximum of 10% by chlorpyrifos per se (O,O-diethyl- O- weight of the controlled-release prod- (3,5,6-trichloro-2-pyridyl) uct in food-handling establishments phosphorothioate) in or on the fol- where food and food products are held, lowing food commodities: processed, prepared, or served. A maximum of 36 strips (or 5.15 grams of Commodity Parts per chlorpyrifos) is to be used per 100 million square feet of floor space. The strips Asparagus ...... 5.0

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calculated as the parent compound) in Commodity Parts per million or on the raw agricultural commod- Grape ...... 0 .01 ities:

(d) Indirect or inadvertent residues. Parts per Commodity million [Reserved] Carrot, roots ...... 7.0 [65 FR 33711, May 24, 2000, as amended at 67 FR 49617, July 31, 2002; 71 FR 74817, Dec. 13, 2006; 73 FR 53739, Sept. 17, 2008; 76 FR 56656, (d) Indirect or inadvertent residues. Sept. 14, 2011] [Reserved]

§ 180.345 Ethofumesate; tolerances for [63 FR 34828, June 26, 1998, as amended at 71 residues. FR 51516, Aug. 30, 2006; 72 FR 52019, Sept. 12, 2007] (a) General. Tolerances for the combined residues of the herbicide § 180.349 Fenamiphos; tolerances for ethofumesate (2-ethoxy-2,3-dihydro-3,3- residues. dimethyl-5-benzofuranyl (a) General. Tolerances are estab- methanesulfonate) and its metabolites lished for residues of the nematicide/in- 2-hydroxy-2,3-dihydro-3,3-dimethyl-5- secticide fenamiphos, ethyl 3-methyl-4- benzofuranyl methanesulfonate and 2,3- dihydro-3,3-dimethyl-2-oxo-5- (methylthio)phenyl 1- benzofuranyl methanesulfonate both (methylethyl)phosphoramidate, includ- calculated as parent compound in or on ing its metabolites and degradates, in the following food commodities: or on the commodities in the following table. Compliance with the tolerance Parts per levels specified in this paragraph is to Commodity million be determined by measuring only the Beet, garden, roots ...... 0 .5 sum of fenamiphos, ethyl 3-methyl-4- Beet, garden, tops ...... 5 .0 Beet, sugar, molasses ...... 0 .5 (methylthio)phenyl 1- Beet, sugar, refined sugar ...... 0 .2 (methylethyl)phosphoramidate, and its Beet, sugar, roots ...... 0 .3 cholinesterase inhibiting metabolites Beet, sugar, tops ...... 4.0 Cattle, fat ...... 0.05 ethyl 3-methyl-4- Cattle, meat ...... 0 .05 (methylsulfinyl)phenyl 1- Cattle, meat byproducts ...... 0.05 (methylethyl)phosphoramidate and Garlic ...... 0 .25 Goat, fat ...... 0 .05 ethyl 3-methyl-4- Goat, meat ...... 0.05 (methylsulfonyl)phenyl 1- Goat, meat byproducts ...... 0 .05 (methylethyl)phosphoramidate, cal- Grass, straw ...... 1 .0 Horse, fat ...... 0 .05 culated as the stoichiometric equiva- Horse, meat ...... 0 .05 lent of fenamiphos, in or on the com- Horse, meat byproducts ...... 0 .05 modity. Onion, bulb ...... 0 .25 Shallot, bulb ...... 0 .25 Parts per Shallot, fresh leaves ...... 0 .25 Commodity million Sheep, fat ...... 0 .05 Sheep, meat ...... 0.05 Banana1 ...... 0 .1 Sheep, meat byproducts ...... 0 .05 Grape1 ...... 0 .1 Grape, raisin1 ...... 0 .3 (b) Section 18 emergency exemptions. Pineapple1 ...... 0 .3 [Reserved] 1 (c) Tolerances with regional registra- There are no U.S. registrations as of May 31, 2007. tion. Tolerances with regional registra- (b) Section 18 emergency exemptions. tion as defined in 40 CFR 180.1(l) are es- [Reserved] tablished for the combined residues of (c) Tolerances with regional registra- ethofumesate,(2-ethoxy -2, 3-dihydro-3, tions. [Reserved] 3-dimethyl-5-benzofuranyl (d) Indirect or inadvertent residues. methanesulfonate) and its metabolites [Reserved] 2-hydroxy-2,3-dihydro-3,3-dimethyl-5- benzofuranyl methanesulfonate and 2,3- [65 FR 33712, May 24, 2000, as amended at 73 dihydro-3,3-dimethyl-2-oxo-5- FR 53739, Sept. 17, 2008; 75 FR 60243, Sept. 29, benzofuranyl methanesulfonate (both 2010]

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§ 180.350 Nitrapyrin; tolerances for Commodity Parts per residues. million (a) General. Tolerances are estab- Banana ...... 0.025 Beet, sugar, roots ...... 0 .05 lished for the combined residues of the Beet, sugar, tops ...... 0.1 soil microbiocide nitrapyrin [2-chloro- Coffee, green bean 1 ...... 0 .05 6-(trichloromethyl) pyridine] and its Corn, field, forage ...... 0 .5 metabolite, 6-chloropicolinic acid in or Corn, field, grain ...... 0 .5 Corn, field, stover ...... 0 .5 on the following raw agricultural com- Corn, pop, grain ...... 0.5 modities: Corn, pop, stover ...... 0.5 Corn, sweet, kernel plus cob with husks removed ...... 0 .05 Commodity Parts per million Corn, sweet, forage ...... 0 .5 Corn, sweet, stover ...... 0 .5 Corn, field, forage ...... 1 .0 Sorghum, grain, forage ...... 0.5 Corn, field, grain ...... 0 .1 Sorghum, grain, grain ...... 0 .05 Corn, field, milled byproducts ...... 0 .2 Sorghum, grain, stover ...... 0 .5 Corn, field, stover ...... 1 .0 1 There are no U. S. registrations as of August 2, 1995, for Corn, pop, grain ...... 0.1 the use of terbufos on the growing crop, coffee. Corn, pop, stover ...... 1.0 Corn, sweet, forage ...... 1 .0 (b) Section 18 emergency exemptions. Corn, sweet, kernel plus cob with husks re- [Reserved] moved ...... 0 .1 (c) Tolerances with regional registra- Corn, sweet, stover ...... 1 .0 Sorghum, forage, forage ...... 0 .5 tions. [Reserved] Sorghum, grain, forage ...... 0.5 (d) Indirect or inadvertent residues. Sorghum, grain, grain ...... 0 .1 [Reserved] Sorghum, grain, stover ...... 0 .5 Wheat, bran ...... 3.0 [73 FR 53740, Sept. 17, 2008] Wheat, forage ...... 2 .0 Wheat, grain ...... 0 .5 § 180.353 Desmedipham; tolerances for Wheat, milled byproducts, except flour ...... 2 .0 residues. Wheat, straw ...... 6 .0 (a) General. Tolerances are estab- (b) Section 18 emergency exemptions. lished for residues of the herbicide [Reserved] desmedipham, (ethyl-m- (c) Tolerances with regional registra- hydroxycarbanilate carbanilate) in or tions. [Reserved] on the following raw agricultural com- (d) Indirect or inadvertent residues. modities in the table that follows: [Reserved] Parts per Commodity million [46 FR 58315, Dec. 1, 1981, as amended at 47 FR 22957, May 26, 1982; 52 FR 33238, Sept. 2, Beet, garden, roots ...... 0 .05 1987; 58 FR 32304, June 9, 1993; 63 FR 57076, Beet, garden, tops ...... 1 .0 Oct. 26, 1998; 72 FR 53461, Sept. 19, 2007] Beet, sugar, roots ...... 0 .1 Beet, sugar, tops ...... 5.0 § 180.352 Terbufos; tolerances for resi- Spinach ...... 6 .0 dues. (b) Section 18 emergency exemptions. (a) General. Tolerances are estab- [Reserved] lished for the combined residues of the (c) Tolerances with regional registra- insecticide terbufos (phosphorodithioic tions. [Reserved] acid, S-(t-butylthio)methyl O,O-diethyl (d) Indirect or inadvertent residues. ester) and its phosphorylated (cholin- [Reserved] esterase-inhibiting) metabolites (phosphorothioic acid, S-(t- [40 FR 4658, Jan. 31, 1975, as amended at 62 butylthio)methyl O,O-diethyl ester; FR 45747, Aug. 29, 1997; 63 FR 49472, Sept. 16, 1998; 64 FR 46292, Aug. 25, 1999; 65 FR 82293, phosphorothioic acid, S-(t- Dec. 28, 2000; 66 FR 64773, Dec. 14, 2001; 68 FR butylsulfinyl)methyl O,O-diethyl ester; 37764, June 25, 2003; 69 FR 71717, Dec. 10, 2004; phosphorothioic acid, S-(t- 72 FR 53449, Sept. 19, 2007; 73 FR 53740, Sept. butylsulfonyl)methyl O,O-diethyl 17, 2008] ester; phosphorodithioic acid, S-(t- butylsulfinyl)methyl O,O-diethyl ester; § 180.355 Bentazon; tolerances for resi- and phosphorodithioic acid, S-(t- dues. butylsulfonyl)methyl O,O-diethyl (a) General. (1) Tolerances are estab- ester) in or on food commodities: lished for the combined residues of the

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herbicide bentazon (3-isopropyl-1H- istration as defined in § 180.1(m), are es- 2,1,3-benzothiadiazin-4(3H)-one-2,2-diox- tablished for combined residues of the ide) and its 6- and 8-hydroxy metabo- herbicide, bentazon (3-isopropyl-1H-2, lites in or on the following food com- 1,3-benzothiadiazin-4(3H)-one-2,2-diox- modities: ide) and its 6- and 8-hydroxy metabolites in or on the following food com- Parts per Commodity million modities:

Bean, dry, seed ...... 0 .05 Commodity Parts per Bean, succulent ...... 0 .5 million Corn, field, forage ...... 3 .0 Corn, field, grain ...... 0 .05 Clover, forage ...... 1.0 Corn, field, stover ...... 3 .0 Clover, hay ...... 2.0 Corn, pop, grain ...... 0.05 Corn, sweet, kernel plus cob with husks re- (d) Indirect or inadvertent residues. moved ...... 0 .05 [Reserved] Cowpea, forage ...... 10 .0 Cowpea, hay ...... 3 .0 [42 FR 26979, May 26, 1977] Flax, seed ...... 1 .0 Pea, dry, seed ...... 1 .0 EDITORIAL NOTE: For FEDERAL REGISTER ci- Pea, field, hay ...... 8.0 tations affecting § 180.355, see the List of CFR Pea, field, vines ...... 3 .0 Sections Affected, which appears in the Pea, succulent ...... 3 .0 Finding Aids section of the printed volume Peanut ...... 0 .05 Peanut, hay ...... 3.0 and at www.fdsys.gov. Pepper, nonbell ...... 0 .05 Peppermint, tops ...... 1 .0 § 180.356 Norflurazon; tolerances for Rice, grain ...... 0 .05 residues. Rice, hulls ...... 0 .25 Rice, straw ...... 3 .0 (a) General. Tolerances are estab- Sorghum, forage ...... 0 .20 lished for the combined residues of the Sorghum, grain, grain ...... 0 .05 herbicide norflurazon (4-chloro-5- Sorghum, grain, stover ...... 0 .05 Soybean, forage ...... 8 .0 (methylamino)-2-(alpha, alpha, alpha- Soybean, hay ...... 8 .0 trifluoro-m-tolyl)-3-(2H)-pyridazinone) Soybean, seed ...... 0 .05 and its desmethyl metabolite 4-chloro- Spearmint, tops ...... 1 .0 5-(amino)-2-alpha, alpha, alpha- (2) Tolerances are established for the trifluoro-m-tolyl)-3(2H)-pyridazinone in combined residues of the herbicide or on the following raw agricultural bentazon (3-isopropyl-1H-2,1,3- commodities: benzothiadiazin-4(3H)-one-2,2-dioxide) Parts per and its metabolite 2-amino-N-isopropyl Commodity million benzamide (AIBA) in or on the fol- Alfalfa, forage ...... 3.0 lowing food commodities: Alfalfa, hay ...... 5.0 Alfalfa, seed ...... 0 .1 Commodity Parts per Almond, hulls ...... 1 .0 million Almond ...... 0.1 Apple ...... 0.1 Cattle, fat ...... 0.05 Apricot ...... 0 .1 Cattle, meat byproducts ...... 0.05 Asparagus ...... 0.05 Cattle, meat ...... 0 .05 Avocado ...... 0 .20 Egg ...... 0 .05 Blackberry ...... 0 .1 Goat, fat ...... 0 .05 Blueberry ...... 0 .2 Goat, meat byproducts ...... 0 .05 Cattle, fat ...... 0.1 Goat, meat ...... 0.05 Cattle, liver ...... 0 .50 Hog, fat ...... 0 .05 Cattle, meat ...... 0 .1 Hog, meat byproducts ...... 0 .05 Cattle, meat byproducts, except liver ...... 0 .1 Hog, meat ...... 0 .05 Cherry ...... 0.1 Milk ...... 0.02 Citrus, dried pulp ...... 0 .4 Poultry, fat ...... 0.05 Citrus, molasses ...... 1.0 Poultry, meat byproducts ...... 0.05 Cotton, undelinted seed ...... 0 .1 Poultry, meat ...... 0 .05 Cranberry ...... 0 .1 Sheep, fat ...... 0 .05 Fruit, citrus ...... 0 .2 Sheep, meat byproducts ...... 0 .05 Goat, fat ...... 0 .1 Sheep, meat ...... 0.05 Goat, liver ...... 0.50 Goat, meat ...... 0.1 (b) Section 18 emergency exemptions. Goat, meat byproducts, except liver ...... 0 .1 [Reserved] Grape ...... 0 .1 Hazelnut ...... 0 .1 (c) Tolerances with regional registra- Hog, fat ...... 0 .1 tions. Tolerances with regional reg- Hog, liver ...... 0 .50

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Parts per Parts per Commodity million Commodity million

Hog, meat ...... 0 .1 Milk ...... 0.05 Hog, meat byproducts, except liver ...... 0 .1 Sheep, fat ...... 0 .05 Hop, dried cones ...... 3 .0 Sheep, meat ...... 0.05 Hop, vines ...... 1 .0 Sheep, meat byproducts ...... 0 .2 Horse, fat ...... 0 .1 Sugarcane, cane ...... 1.0 Horse, liver ...... 0 .50 Sugarcane, molasses ...... 30 Horse, meat ...... 0 .1 Horse, meat byproducts, except liver ...... 0 .1 (b) Section 18 emergency exemptions. Milk ...... 0.1 Nectarine ...... 0 .1 [Reserved] Peach ...... 0 .1 (c) Tolerances with regional registra- Peanut ...... 0 .05 tions. [Reserved] Peanut, hay ...... 5.50 (d) Indirect or inadvertent residues. Peanut, hay ...... 1.5 Pear ...... 0 .1 [Reserved] Pecan ...... 0 .1 Plum, prune, fresh ...... 0.1 [68 FR 39441, July 1, 2003, as amended at 72 Poultry, fat ...... 0.1 FR 37654, July 11, 2007] Poultry, meat ...... 0 .1 Poultry, meat byproducts ...... 0.1 § 180.361 Pendimethalin; tolerances for Raspberry ...... 0 .2 residues. Sheep, fat ...... 0 .1 Sheep, liver ...... 0.50 (a) General. Tolerances are estab- Sheep, meat ...... 0.1 lished for residues of the herbicide Sheep, meat byproducts, except liver ...... 0 .1 Soybean ...... 0.1 pendimethalin, including its metabo- Soybean, forage ...... 1 .0 lites and degradates, in or on the com- Soybean, hay ...... 1 .0 modities. Compliance with the toler- Walnut ...... 0 .1 ance levels specified in the following table below is to be determined by (b) Section 18 emergency exemptions. measuring only pendimethalin, [N- (1- [Reserved] ethylpropyl)-3,4-dimethyl-2,6- (c) Tolerances with regional registra- dinitrobenzenamine], and its metabo- tion. [Reserved] lite, 4-[(1-ethylpropyl)amino]-2-methyl- (d) Indirect or inadvertent residues. 3,5-dinitrobenzyl alcohol, calculated as [Reserved] the stoichiometric equivalent of [47 FR 14909, Apr. 7, 1982] pendimethalin, in or on the following EDITORIAL NOTE: For FEDERAL REGISTER ci- commodities: tations affecting § 180.356, see the List of CFR Parts per Sections Affected, which appears in the Commodity million Finding Aids section of the printed volume and at www.fdsys.gov. Alfalfa, forage ...... 3.5 Alfalfa, hay ...... 4.0 § 180.360 Asulam; tolerance for resi- Alfalfa, seed ...... 0 .10 Almond, hulls ...... 6 .0 dues. Apple, wet pomace ...... 0 .20 (a) General. Tolerances are estab- Artichoke, globe ...... 0.1 Asparagus ...... 0.15 lished for the combined residues of Beans ...... 0 .10 asulam (methyl sulfanilylcarbamate) Beans, forage ...... 0 .10 and its sulfanilamide containing me- Beans, hay ...... 0 .10 Brassica head and stem, subgroup 5-A ...... 0 .1 tabolites in or on the following food Brassica, leafy greens, subgroup 5B ...... 0 .20 commodities: Carrot ...... 0 .5 Citrus, oil ...... 0.5 Corn, field, forage ...... 0 .1 Commodity Parts per million Corn, field, grain ...... 0 .1 Corn, field, stover ...... 0 .1 Cattle, fat ...... 0.05 Corn, pop, grain ...... 0.1 Cattle, meat ...... 0 .05 Corn, sweet, forage ...... 0 .1 Cattle, meat byproducts ...... 0.2 Corn, sweet, kernel plus cob with husks re- Goat, fat ...... 0 .05 moved ...... 0 .1 Goat, meat ...... 0.05 Corn, sweet, stover ...... 0 .1 Goat, meat byproducts ...... 0 .2 Cotton, gin byproducts ...... 3 .0 Hog, fat ...... 0 .05 Cotton, undelinted seed ...... 0 .1 Hog, meat ...... 0 .05 Crayfish ...... 0.05 Hog, meat byproducts ...... 0 .2 Fruit, citrus, group 10 ...... 0 .1 Horse, fat ...... 0 .05 Fruit, pome, group 11 ...... 0.10 Horse, meat ...... 0 .05 Fruit, small vine climbing, except grape, sub- Horse, meat byproducts ...... 0 .2 group 13–07E ...... 0.10

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Parts per Expiration/ Commodity million Commodity Parts per revocation million date Fruit, stone, group 12 ...... 0 .10 Garlic ...... 0 .1 Bermuda grass, hay ...... 60 12/31/10 Grape ...... 0 .1 Grass forage, fodder, and hay crop group 17, (c) Tolerances with regional registra- forage ...... 20 Grass forage, fodder, and hay crop group 17, tions. [Reserved] hay ...... 13 (d) Indirect or inadvertent residues. Grass forage, fodder, and hay crop group 17, [Reserved] straw ...... 4.0 Juneberry ...... 0 .10 [49 FR 15293, Apr. 18, 1984] Leek ...... 0 .20 Lettuce, leaf ...... 4 .0 EDITORIAL NOTE: For FEDERAL REGISTER ci- Melon subgroup 9A ...... 0 .10 tations affecting § 180.361, see the List of CFR Nut, tree, group 14 ...... 0 .1 Sections Affected, which appears in the Olive ...... 0 .1 Finding Aids section of the printed volume Onion, bulb ...... 0 .1 Onion, green ...... 0 .20 and at www.fdsys.gov. Onion, welsh ...... 0.20 Peanut ...... 0 .1 § 180.362 Fenbutatin-oxide; tolerances Peanut, hay ...... 0.1 for residues. Peas (except field peas) ...... 0.10 Peppermint, oil ...... 1 .0 (a) General. (1) Tolerances are estab- Peppermint, tops ...... 0 .2 lished for residues of the miticide/acar- Pistachio ...... 0.1 icide fenbutatin-oxide, including its Pomegranate ...... 0 .10 Potato ...... 0 .1 metabolites and degradates, in or on Rice, grain ...... 0 .1 the plant commodities in the table in Rice, straw ...... 0 .1 this paragraph. Compliance with the Shallot ...... 0.2 Sorghum, forage ...... 0 .1 tolerance levels specified in this para- Sorghum, grain, grain ...... 0 .1 graph is to be determined by measuring Sorghum, grain, stover ...... 0 .1 only fenbutatin-oxide, hexakis (2-meth- Soybean, forage ...... 0 .1 Soybean, hay ...... 0 .1 yl-2-phenylpropyl) distannoxane, in or Soybean, seed ...... 0 .1 on the commodity. Spearmint, oil ...... 1 .0 Spearmint, tops ...... 0 .2 Commodity Parts per Strawberry ...... 0 .10 million Sugarcane, cane ...... 0.1 Sunflower, seed ...... 0.1 Almond, hulls ...... 80 .0 Turnip greens ...... 0 .20 Apple ...... 15.0 Vegetable, fruiting, group 8 ...... 0.10 Apple, wet pomace ...... 100.0 Vegetable, soybean, succulent ...... 0 .10 Cherry, sweet ...... 6 .0 Wheat, grain ...... 0 .10 Cherry, tart ...... 6 .0 Wheat, forage ...... 3 .0 Citrus, dried pulp ...... 100.0 Wheat, hay ...... 0 .60 Citrus, oil ...... 140.0 Wheat, straw ...... 0 .30 Cucumber ...... 4 .0 Eggplant ...... 6.0 (b) Section 18 emergency exemptions. Fruit, citrus, group 10 ...... 20 .0 Grape ...... 5 .0 Time-limited tolerances specified in Grape, raisin ...... 20.0 the following table are established for Nut, tree, group 14 ...... 0 .5 combined residues of the herbicide Papaya ...... 2 .0 Peach ...... 10 .0 pendimethalin, [N-(1-ethylpropyl)-3,4- Pear ...... 15 .0 dimethyl-2,6-dinitrobenzenamine], and Pistachio ...... 0.5 its metabolite 4-[(1- Plum, prune, fresh ...... 4.0 ethylpropyl)amino]-2-methyl-3,5- Plum, prune, dried ...... 20.0 dinitrobenzyl alcohol, in or on the Strawberry ...... 10.0 specified agricultural commodities, re- (2) Tolerances are established for res- sulting from use of the pesticide pursu- idues of the miticide/acaricide ant to FIFRA section 18 emergency ex- fenbutatin-oxide, including its metabo- emptions. The tolerances expire and lites and degradates, in or on the ani- are revoked on the date specified in the mal commodities in the table in this table. paragraph. Compliance with the tolerance levels specified in this paragraph Parts per Expiration/ Commodity million revocation is to be determined by measuring only date the sum of fenbutatin-oxide, hexakis Bermuda grass, forage ...... 25 12/31/10 (2-methyl-2-phenylpropyl)

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distannoxane, and its organotin me- glyphosate, the isopropylamine salt of tabolites, dihydroxybis(2-methyl-2- glyphosate, the ethanolamine salt of phenylpropyl) stannane and 2-methyl- glyphosate, the dimethylamine salt of 2-phenylpropylstannoic acid, cal- glyphosate, the ammonium salt of culated as the stoichiometric equiva- glyphosate, and the potassium salt of lent of fenbutatin-oxide, in or on the glyphosate. Compliance with the fol- commodity. lowing tolerance levels is to be determined by measuring only glyphosate Parts per Commodity million (N-(phosphonomethyl)glycine).

Cattle, fat ...... 0.5 Commodity Parts per Cattle, meat ...... 0 .5 million Cattle, meat byproducts ...... 0.5 Egg ...... 0 .1 Acerola ...... 0.2 Goat, fat ...... 0 .5 Alfalfa, seed ...... 0 .5 Goat, meat ...... 0.5 Almond, hulls ...... 25 Goat, meat byproducts ...... 0 .5 Aloe vera ...... 0 .5 Hog, fat ...... 0 .5 Ambarella ...... 0 .2 Hog, meat ...... 0 .5 Animal feed, nongrass, group 18 ...... 400 Hog, meat byproducts ...... 0 .5 Artichoke, globe ...... 0.2 Horse, fat ...... 0 .5 Asparagus ...... 0.5 Horse, meat ...... 0 .5 Atemoya ...... 0 .2 Horse, meat byproducts ...... 0 .5 Avocado ...... 0 .2 Milk, fat ...... 0 .1 Bamboo, shoots ...... 0 .2 Poultry, fat ...... 0.1 Banana ...... 0.2 Poultry, meat ...... 0 .1 Barley, bran ...... 30 Poultry, meat byproducts ...... 0.1 Beet, sugar, dried pulp ...... 25 Sheep, fat ...... 0 .5 Beet, sugar, roots ...... 10 Sheep, meat ...... 0.5 Beet, sugar, tops ...... 10 Sheep, meat byproducts ...... 0 .5 Berry and small fruit, group 13–07 ...... 0 .20 Betelnut ...... 1 .0 Biriba ...... 0 .2 (b) Section 18 emergency exemptions. Blimbe ...... 0 .2 [Reserved] Breadfruit ...... 0 .2 (c) Tolerances with regional registra- Cacao bean, bean ...... 0 .2 Cactus, fruit ...... 0 .5 tions. A tolerance with regional reg- Cactus, pads ...... 0 .5 istration, as defined in § 180.1(l), is es- Canistel ...... 0 .2 tablished for residues of the miticide/ Carrot ...... 5 .0 Chaya ...... 1.0 acaricide fenbutatin-oxide, including Cherimoya ...... 0 .2 its metabolites and degradates, in or Citrus, dried pulp ...... 1 .5 on the plant commodity in the table in Coconut ...... 0 .1 Coffee, bean, green ...... 1 .0 this paragraph. Compliance with the Corn, pop, grain ...... 0.1 tolerance level specified in this para- Corn, sweet, kernel plus cob with husk removed 3.5 graph is to be determined by measuring Cotton, gin byproducts ...... 210 only fenbutatin-oxide, hexakis (2-meth- Custard apple ...... 0 .2 Date, dried fruit ...... 0 .2 yl-2-phenylpropyl) distannoxane, in or Dokudami ...... 2 .0 on the commodity. Durian ...... 0 .2 Epazote ...... 1 .3 Feijoa ...... 0 .2 Commodity Parts per million Fig ...... 0 .2 Fish ...... 0 .25 Raspberry ...... 10 .0 Fruit, citrus, group 10–10 ...... 0 .50 Fruit, pome, group 11–10 ...... 0 .20 (d) Indirect or inadvertent residues. Fruit, stone, group 12 ...... 0 .2 [Reserved] Galangal, roots ...... 0 .2 Ginger, white, flower ...... 0 .2 [65 FR 33713, May 24, 2000, as amended at 72 Gourd, buffalo, seed ...... 0 .1 FR 41930, Aug. 1, 2007; 73 FR 5109, Jan. 29, Governor’s plum ...... 0 .2 Gow kee, leaves ...... 0 .2 2008; 76 FR 23494, Apr. 27, 2011] Grain, cereal, forage, fodder and straw, group 16, except field corn, forage and field corn, § 180.364 Glyphosate; tolerances for stover ...... 100 residues. Grain, cereal, group 15 except field corn, popcorn, rice, sweet corn, and wild rice ...... 30 (a) General. (1) Tolerances are estab- Grass, forage, fodder and hay, group 17 ...... 300 lished for residues of glyphosate, in- Guava ...... 0 .2 cluding its metabolites and degradates, Herbs subgroup 19A ...... 0 .2 Hop, dried cones ...... 7 .0 in or on the commodities listed below Ilama ...... 0 .2 resulting from the application of Imbe ...... 0 .2

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Parts per Parts per Commodity million Commodity million

Imbu ...... 0 .2 Vegetable, fruiting, group 8–10 (except okra) ..... 0 .10 Jaboticaba ...... 0 .2 Vegetable, leafy, brassica, group 5 ...... 0.2 Jackfruit ...... 0 .2 Vegetable, leafy, except brassica, group 4 ...... 0 .2 Kava, roots ...... 0 .2 Vegetable, leaves of root and tuber, group 2, Kenaf, forage ...... 200 except sugar beet tops ...... 0 .2 Leucaena, forage ...... 200 Vegetable, legume, group 6 except soybean Longan ...... 0 .2 and dry pea ...... 5 .0 Lychee ...... 0 .2 Vegetables, root and tuber, group 1, except car- Mamey apple ...... 0 .2 rot, sweet potato, and sugar beet ...... 0 .20 Mango ...... 0.2 Wasabi, roots ...... 0 .2 Mangosteen ...... 0 .2 Water spinach, tops ...... 0.2 Marmaladebox ...... 0 .2 Watercress, upland ...... 0 .2 Mioga, flower ...... 0 .2 Wax jambu ...... 0 .2 Noni ...... 0 .20 Yacon, tuber ...... 0.2 Nut, pine ...... 1 .0 Nut, tree, group 14 ...... 1 .0 Oilseeds, group 20, except canola ...... 40 (2) Tolerances are established for res- Okra ...... 0.5 idues of glyphosate, including its me- Olive ...... 0 .2 tabolites and degradates, in or on the Oregano, Mexican, leaves ...... 2 .0 commodities listed below resulting Palm heart ...... 0 .2 Palm heart, leaves ...... 0 .2 from the application of glyphosate, the Palm, oil ...... 0 .1 isopropylamine salt of glyphosate, the Papaya ...... 0 .2 ethanolamine salt of glyphosate, the Papaya, mountain ...... 0.2 Passionfruit ...... 0 .2 dimethylamine salt of glyphosate, the Pawpaw ...... 0 .2 ammonium salt of glyphosate, and the Pea, dry ...... 8 .0 potassium salt of glyphosate. Compli- Peanut ...... 0 .1 ance with the following tolerance lev- Peanut, hay ...... 0.5 Pepper leaf, fresh leaves ...... 0 .2 els is to be determined by measuring Peppermint, tops ...... 200 only glyphosate (N- Perilla, tops ...... 1 .8 (phosphonomethyl)glycine) and its me- Persimmon ...... 0 .2 Pineapple ...... 0.1 tabolite N-acetyl-glyphosate (N-acetyl- Pistachio ...... 1.0 N-(phosphonomethyl)glycine; cal- Pomegranate ...... 0 .2 culated as the stoichiometric equiva- Pulasan ...... 0 .2 lent of glyphosate). Quinoa, grain ...... 5 .0 Rambutan ...... 0 .2 Rice, grain ...... 0 .1 Parts per Commodity Million Rice, wild, grain ...... 0.1 Rose apple ...... 0 .2 Canola, seed ...... 20 Sapodilla ...... 0 .2 Cattle, meat byproducts ...... 5.0 Sapote, black ...... 0 .2 Corn, field, forage ...... 13 Sapote, mamey ...... 0 .2 Corn, field, grain ...... 5 .0 Sapote, white ...... 0 .2 Corn, field, stover ...... 100 Shellfish ...... 3 .0 Egg ...... 0 .05 Soursop ...... 0 .2 Goat, meat byproducts ...... 5 .0 Spanish lime ...... 0 .2 Grain aspirated fractions ...... 310 .0 Spearmint, tops ...... 200 Hog, meat byproducts ...... 5 .0 Spice subgroup 19B ...... 7 .0 Horse, meat byproducts ...... 5 .0 Star apple ...... 0 .2 Poultry, meat ...... 0 .10 Starfruit ...... 0 .2 Poultry, meat byproducts ...... 1.0 Stevia, dried leaves ...... 1 .0 Sheep, meat byproducts ...... 5 .0 Sugar apple ...... 0 .2 Soybean, forage ...... 100.0 Sugarcane, cane ...... 2.0 Soybean, hay ...... 200.0 Sugarcane, molasses ...... 30 Soybean, hulls ...... 120 .0 Surinam cherry ...... 0 .2 Soybean, seed ...... 20.0 Sweet potato ...... 3.0 Tamarind ...... 0 .2 Tea, dried ...... 1 .0 (b) Section 18 emergency exemptions. Tea, instant ...... 7 .0 [Reserved] Teff, forage ...... 100 (c) Tolerances with regional registra- Teff, grain ...... 5 .0 Teff, hay ...... 100 tions. [Reserved] Ti, leaves ...... 0 .2 (d) Indirect or inadvertent residues. Ti, roots ...... 0 .2 [Reserved] Ugli fruit ...... 0.5 Vegetable, bulb, group 3–07 ...... 0 .20 [45 FR 64911, Oct. 1, 1980] Vegetable, cucurbit, group 9 ...... 0.5 Vegetable, foliage of legume, subgroup 7A, ex- EDITORIAL NOTE: For FEDERAL REGISTER ci- cept soybean ...... 0 .2 tations affecting § 180.364, see the List of CFR

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Sections Affected, which appears in the Parts per Finding Aids section of the printed volume Commodity million and at www.fdsys.gov. Corn, field, forage ...... 6 .0 Corn, field, grain ...... 0 .10 § 180.367 n-Octyl bicycloheptenedi- Corn, field, stover ...... 6 .0 carboximide; tolerances for resi- Corn, pop, grain ...... 0.10 dues. Corn, pop, stover ...... 6.0 (a) General. A tolerance of 5 parts per Corn, sweet, forage ...... 6 .0 Corn, sweet, kernel plus cob with husks re- million is established for residues of moved ...... 0 .10 the insecticide synergist N-octyl Corn, sweet, stover ...... 6 .0 bicycloheptene dicarboximide, includ- Cotton, gin byproducts ...... 4 .0 ing its metabolites and degradates, in Cotton, undelinted seed ...... 0 .10 or on all food items in food handling Dillweed ...... 0 .50 Egg ...... 0 .02 establishments where food and food Goat, fat ...... 0 .02 products are held, processed, prepared Goat, kidney ...... 0 .20 and/or served, provided that the food is Goat, liver ...... 0.05 removed or covered prior to such use, Goat, meat ...... 0.02 Goat, meat byproducts, except kidney and liver 0 .04 except for bagged food in warehouse Grass, forage ...... 10 storage which need not be removed or Grass, hay ...... 0 .20 covered prior to applications of formu- Horse, fat ...... 0 .02 lations containing N-octyl Horse, kidney ...... 0 .20 Horse, liver ...... 0 .05 bicycloheptene dicarboximide. Compli- Horse, meat ...... 0 .02 ance with the tolerance level specified Horse, meat byproducts, except kidney and liver 0 .04 in this paragraph is to be determined Milk ...... 0.02 by measuring only N-octyl Nut, tree, group 14 ...... 0 .10 Okra ...... 0.50 bicycloheptene dicarboximide, in or on Peanut ...... 0 .20 the commodity. Peanut, hay ...... 20 (b) Section 18 emergency exemptions. Peanut, meal ...... 0 .40 [Reserved] Potato ...... 0 .20 Poultry, fat ...... 0.02 (c) Tolerances with regional registra- Poultry, meat ...... 0 .02 tions. [Reserved] Poultry, meat byproducts ...... 0.05 (d) Indirect or inadvertent residues. Safflower, seed ...... 0 .10 [Reserved] Sheep, fat ...... 0 .02 Sheep, kidney ...... 0.20 [65 FR 33713, May 24, 2000, as amended at 75 Sheep, liver ...... 0.05 FR 60243, Sept. 29, 2010] Sheep, meat ...... 0.02 Sheep, meat byproducts, except kidney and liver ...... 0 .04 § 180.368 Metolachlor; tolerances for Sorghum, grain, forage ...... 1.0 residues. Sorghum, grain, grain ...... 0 .30 (a) General. (1) Tolerances are estab- Sorghum, grain, stover ...... 4 .0 lished for the combined residues (free Soybean, forage ...... 5 .0 Soybean, hay ...... 8 .0 and bound) of the herbicide Soybean, seed ...... 0 .20 metolachlor, 2-chloro-N-(2- ethyl-6- Tomato ...... 0.10 methylphenyl)-N-(2-methoxy-1- Vegetable, foliage of legume, subgroup 7A, except soybean ...... 15.0 methylethyl)acetamide, and its me- Vegetable, legume, group 6 ...... 0 .30 tabolites, determined as the derivatives, 2- [(2-ethyl-6- (2) Tolerances are established for res- methylphenyl)amino]-1-propanol and 4- idues of S-metolachlor, including its (2-ethyl-6-methylphenyl)-2- hydroxy-5- metabolites and degradates, in or on methyl-3-morpholinone, each expressed the commodity(s), as defined. Compli- as the parent compound in the fol- ance with the tolerance levels specified lowing raw agricultural commodities: in the following table below is to be de- Parts per termined by measuring only the sum of Commodity million free and bound S-metolachlor, S-2- chloro-N-(2-ethyl-6-methylphenyl)-N- Almond, hulls ...... 0 .30 Animal feed, nongrass, group 18 ...... 1 .0 (2-methoxy-1-methylethyl)acetamide, Cattle, fat ...... 0.02 its R-enantiomer, and its metabolites, Cattle, kidney ...... 0 .20 determined as the derivatives, 2-(2- Cattle, liver ...... 0 .05 Cattle, meat ...... 0 .02 ethyl-6-methylphenyl)amino-1-pro- Cattle, meat byproducts, except kidney and liver 0.04 panol and 4-(2-ethyl-6-methylphenyl)-2-

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hydroxy-5-methyl-3-morpholinone, cal- Commodity Parts per culated as the stoichiometric equiva- million lent of S-metolachlor, in or on the Sorghum, sweet, stalk ...... 4.0 commodity. Soybean, forage ...... 5 .0 Soybean, hay ...... 8 .0 Soybean, seed ...... 0 .20 Commodity Parts per million Spinach ...... 0 .50 Squash, winter ...... 0 .10 Asparagus ...... 0.10 Sunflower, seed ...... 0.50 Beet, garden, leaves ...... 1 .8 Sunflower, meal ...... 1 .0 Beet, sugar, molasses ...... 2 .0 Tomato, paste ...... 0 .30 Beet, sugar, roots ...... 0 .5 Turnip, greens ...... 1.8 Beet, sugar, tops ...... 15.0 Vegetable, foliage of legume, except soybean, Brassica, head and stem, subgroup 5A ...... 0 .60 subgroup 7A ...... 15 .0 Brassica, leafy greens, subgroup 5B ...... 1 .8 Vegetable, fruiting, group 8, except tabasco Bushberry subgroup 13-07B ...... 0 .15 pepper ...... 0 .10 Caneberry subgroup 13-07A ...... 0.10 Vegetable, legume, group 6 ...... 0 .30 Carrot, roots ...... 0.40 Vegetable, root, except sugar beet, subgroup Cattle, fat ...... 0.02 1B, except carrot ...... 0 .30 Cattle, kidney ...... 0 .20 Vegetable, tuberous and corm, subgroup 1C ..... 0.20 Cattle, liver ...... 0 .05 Cattle, meat ...... 0 .02 Cattle, meat byproducts, except kidney and liver 0.04 (b) Section 18 emergency exemptions. Cilantro, leaves ...... 8 .0 [Reserved] Coriander, seed ...... 0 .13 (c) Tolerances with regional registra- Corn, field, forage ...... 40 tions. (1) Tolerances with regional reg- Corn, field, grain ...... 0 .10 Corn, field, stover ...... 40 istration as defined in 180.1(l) are es- Corn, pop, grain ...... 0.10 tablished for the combined residues Corn, pop, stover ...... 40 (free and bound) of the herbicide Corn, sweet, forage ...... 40 Corn, sweet, kernel plus cob with husks re- metolachlor [2-chloro-N-(2-ethyl-6- moved ...... 0 .10 methylphenyl)-N-(2-methoxy-1- Corn, sweet, stover ...... 40 methylethyl)acetamide] and its me- Cotton, gin byproducts ...... 4 .0 tabolites, determined as the deriva- Cotton, undelinted seed ...... 0 .10 Cucumber ...... 0 .13 tives, 2-[2-ethyl-6- Egg ...... 0 .02 methylphenyl)amino]-1-propanol and 4- Grain, aspirated fractions ...... 0 .70 (2-ethyl-6-methylphenyl)-2-hydroxy-5- Goat, fat ...... 0 .02 Goat, kidney ...... 0 .20 methyl-3-morpholinone, each expressed Goat, liver ...... 0.05 as the parent compound, in or on the Goat, meat ...... 0.02 following raw agricultural commod- Goat, meat byproducts, except kidney and liver 0 .04 ities: Grass, forage ...... 10 .0 Grass, hay ...... 0 .20 Horse, fat ...... 0 .02 Parts per Commodity million Horse, kidney ...... 0 .20 Horse, liver ...... 0 .05 Pepper, nonbell ...... 0 .50 Horse, meat ...... 0 .02 Horse, meat byproducts, except kidney and liver 0 .04 Leaf petioles, subgroup 4B ...... 0 .10 (2) Tolerances with regional registra- Melon, subgroup 9A ...... 0 .10 tion are established for residues of S- Milk ...... 0.02 metolachlor, including its metabolites Okra ...... 0.10 Onion, bulb, subgroup 3-07A ...... 0 .10 and degradates, in or on the commod- Onion, green, subgroup 3-07B ...... 2 .0 ities identified in the following table Peanut ...... 0 .20 below. Compliance with the tolerance Peanut, hay ...... 20.0 levels specified in the following table Peanut, meal ...... 0 .40 Poultry, fat ...... 0.02 below is to be determined by measuring Poultry, meat ...... 0 .02 only the sum of free and bound S- Poultry, meat byproducts ...... 0.05 metolachlor, S-2-chloro-N-(2-ethyl-6- Pumpkin ...... 0.10 Safflower, seed ...... 0 .10 methylphenyl)-N-(2-methoxy-1- Sesame, seed ...... 0 .13 methylethyl)acetamide, its R- Sheep, fat ...... 0 .02 enantiomer, and its metabolites, deter- Sheep, kidney ...... 0.20 mined as the derivatives, 2-(2-ethyl-6- Sheep, liver ...... 0.05 Sheep, meat ...... 0.02 methylphenyl)amino-1-propanol and 4- Sheep, meat byproducts, except kidney and (2-ethyl-6-methylphenyl)-2-hydroxy-5- liver ...... 0 .04 methyl-3-morpholinone, calculated as Sorghum, grain, forage ...... 1.0 Sorghum, grain, grain ...... 0 .3 the stoichiometric equivalent of S- Sorghum, grain, stover ...... 4 .0 metolachlor, in or on the commodity.

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Parts per Parts per Commodity million Commodity million

Pepper, tabasco ...... 0 .50 Animal feed, nongrass, group 18 ...... 1 .0 Barley, grain ...... 0 .10 (d) Indirect or inadvertent residues. (1) Barley, hay ...... 0 .50 Barley, straw ...... 0 .50 Tolerances are established for the indi- Buckwheat, grain ...... 0.10 rect or inadvertent combined residues Millet, forage ...... 0 .50 (free and bound) of the herbicide Millet, grain ...... 0 .10 metolachlor, 2-chloro-N-(2-ethyl-6- Millet, hay ...... 0 .50 Millet, straw ...... 0 .50 methylphenyl)-N-(2-methoxy-1- Oat, forage ...... 0 .50 methylethyl)acetamide, and its me- Oat, grain ...... 0 .10 tabolites, determined as the deriva- Oat, hay ...... 0.50 tives, 2-[(2-ethyl-6- Oat, straw ...... 0.50 Rice, grain ...... 0 .10 methylphenyl)amino]-1-propanol and 4- Rye, forage ...... 0 .50 (2-ethyl-6-methylphenyl)-2- hydroxy-5- Rye, grain ...... 0.10 methyl-3-morpholinone, each expressed Rye, straw ...... 0 .50 as the parent compound in the fol- Wheat, forage ...... 0 .50 Wheat, grain ...... 0 .10 lowing raw agricultural commodities: Wheat, hay ...... 0 .50 Wheat, straw ...... 0 .50 Parts per Commodity million [73 FR 53740, Sept. 17, 2008, as amended at 74 Animal feed, nongrass, group 18 ...... 1 .0 FR 48412, Sept. 23, 2009; 75 FR 56903, Sept. 17, Barley, grain ...... 0 .10 2010; 77 FR 48906, Aug. 15, 2012; 77 FR 59127, Barley, hay ...... 0 .80 Sept. 26, 2012; 79 FR 17441, Mar. 28, 2014] Barley, straw ...... 0 .80 Buckwheat, grain ...... 0.10 Millet, forage ...... 0 .50 § 180.370 5-Ethoxy-3-(trichloromethyl)- Millet, grain ...... 0 .10 1,2,4-thiadiazole; tolerances for resi- Millet, hay ...... 0 .80 dues. Millet, straw ...... 0 .80 (a) General. Tolerances are estab- Oat, forage ...... 0 .50 lished for residues of the fungicide 5- Oat, grain ...... 0 .10 Oat, hay ...... 0.80 ethoxy-3-(trichloromethyl)-1,2,4- Oat, straw ...... 0.80 thiadiazole and its monoacid metabo- Rice, grain ...... 0 .10 lite 3-carboxy-5-ethoxy-1,2,4- Rye, forage ...... 0 .50 thiadiazole in or on the following raw Rye, grain ...... 0.10 agricultural commodities: Rye, straw ...... 0 .80 Wheat, forage ...... 0 .50 Parts per Wheat, grain ...... 0 .10 Commodity million Wheat, hay ...... 0 .80 Wheat, straw ...... 0 .80 Barley, grain ...... 0 .1 Barley, hay ...... 0 .1 Corn, field, forage ...... 0 .1 (2) Tolerances for are established for Corn, field, grain ...... 0 .1 the indirect or inadvertent residues of Corn, field, stover ...... 0 .1 S-metolachlor, including its metabo- Corn, sweet, forage ...... 0 .1 lites and degradates, in or on the com- Corn, sweet, stover ...... 0 .1 Cotton, gin byproducts ...... 0 .1 modities identified in the following Cotton, undelinted seed ...... 0 .1 table below. Compliance with the toler- Peanut ...... 0 .1 ance levels specified in the following Peanut, hay ...... 0.1 table below is to be determined by Safflower, seed ...... 0 .1 Sorghum, grain, forage ...... 0.1 measuring only the sum of free and Sorghum, grain, grain ...... 0 .1 bound S-metolachlor, S-2-chloro-N-(2- Tomato ...... 0.15 ethyl-6-methylphenyl)-N-(2-methoxy-1- Vegetable, foliage of legume, group 7 ...... 0 .1 methylethyl)acetamide, its R- Vegetable, legume, group 6 ...... 0 .1 Wheat, forage ...... 0 .1 enantiomer, and its metabolites, deter- Wheat, grain ...... 0 .1 mined as the derivatives, 2-(2-ethyl-6- Wheat, straw ...... 0 .1 methylphenyl)amino-1-propanol and 4- (2-ethyl-6-methylphenyl)-2-hydroxy-5- (b) Section 18 emergency exemptions. methyl-3-morpholinone, calculated as [Reserved] the stoichiometric equivalent of S- (c) Tolerances with regional registra- metolachlor, in or on the commodity. tions. [Reserved]

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(d) Indirect or inadvertent residues. phenylene) bis(iminocarbonothioyl)) [Reserved] bis(carbamate), including its metabo- [47 FR 49845, Nov. 3, 1982, as amended at 48 lites and degradates, in or on the com- FR 12088, Mar. 23, 1983; 63 FR 57076, Oct. 26, modity in the following table. Compli- 1998; 72 FR 41931, Aug. 1, 2007; 73 FR 54961, ance with the tolerance level specified Sept. 24, 2008] in this paragraph is to be determined by measuring only the sum of § 180.371 Thiophanate-methyl; toler- thiophanate-methyl, dimethyl ((1,2- ances for residues. phenylene) bis (iminocarbonothioyl)) (a) General. Tolerances are estab- bis(carbamate), and its metabolite, lished for residues of thiophanate- methyl 2-benzimidazoyl carbamate methyl, dimethyl ((1,2-phenylene) bis (MBC), calculated as the stoichio- (iminocarbonothioyl)) bis(carbamate), metric equivalent of thiophanate- including its metabolites and methyl, in or on the commodity. degradates, in or on the commodities in the following table. Compliance with Commodity Parts per the tolerance levels specified in this million paragraph is to be determined by meas- Canola, seed ...... 0 .1 uring only the sum of thiophanate- methyl, dimethyl ((1,2-phenylene) bis (d) Indirect or inadvertent residues. (iminocarbonothioyl)) bis(carbamate), [Reserved] and its metabolite, methyl 2- benzimidazoyl carbamate (MBC), cal- [75 FR 60244, Sept. 29, 2010] culated as the stoichiometric equivalent of thiophanate-methyl, in or on § 180.372 2,6-Dimethyl-4- the commodity. tridecylmorpholine; tolerances for residues. Parts per Commodity million (a) General. A tolerance is established for residues of the fungicide 2,6-di- Almond ...... 0.1 methyl-4-tridecylmorpholine in or on Almond, hulls ...... 0 .5 Apple ...... 2.0 the following food commodity: Apricot ...... 15 .0 Banana ...... 2.0 Commodity Parts per Bean, dry, seed ...... 0 .2 million Bean, snap, succulent ...... 2 .0 Beet, sugar, roots ...... 0 .2 Banana 1 ...... 1.0 Cherry, sweet ...... 20 .0 1 Cherry, tart ...... 20.0 There are no U.S. registrations. Grain, aspirated fractions ...... 12 Grape ...... 5 .0 (b) Section 18 emergency exemptions. Onion, bulb ...... 0 .5 [Reserved] Onion, green ...... 3 .0 (c) Tolerances with regional registra- Peach ...... 3 .0 Peanut ...... 0 .1 tions. [Reserved] Peanut, hay ...... 5.0 (d) Indirect or inadvertent residues. Pear ...... 3 .0 [Reserved] Pecan ...... 0 .1 Pistachio ...... 0.1 [73 FR 54961, Sept. 24, 2008] Plum ...... 0 .5 Potato ...... 0 .1 Soybean, hulls ...... 1 .5 § 180.373 [Reserved] Soybean, seed ...... 0 .2 Strawberry ...... 7 .0 § 180.377 Diflubenzuron; tolerances for Vegetable, cucurbit, group 9 ...... 1.0 residues. Wheat, forage ...... 1 .1 Wheat, grain ...... 0 .1 (a) General. (1) Tolerances are estab- Wheat, hay ...... 0 .1 Wheat, straw ...... 0 .1 lished for residues of diflubenzuron, including its metabolites and degradates, (b) Section 18 emergency exemptions. in or on the commodities in the table [Reserved] below. Compliance with the tolerance (c) Tolerances with regional registra- levels specified below is to be deter- tions. A tolerance with a regional reg- mined by measuring only diflubenzuron istration is established for residues of (N-[[(4-chlorophenyl)amino]carbonyl]- thiophanate-methyl, dimethyl ((1,2- 2,6-difluorobenzamide).

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Parts per Parts per Commodity million Commodity million

Artichoke, globe ...... 6.0 Wheat, grain ...... 0 .06 Cattle, fat ...... 0.05 Wheat, hay ...... 6 .0 Cattle, meat ...... 0 .05 Wheat, straw ...... 3 .5 Cotton, undelinted seed ...... 0 .2 Egg ...... 0 .05 Goat, fat ...... 0 .05 (b) Section 18 emergency exemptions. Goat, meat ...... 0.05 Time-limited tolerances are estab- Hog, fat ...... 0 .05 Hog, meat ...... 0 .05 lished for residues of the insecticide Horse, fat ...... 0 .05 diflubenzuron (N-[[(4- Horse, meat ...... 0 .05 chlorophenyl)amino]carbonyl]-2,6- Milk ...... 0.05 Mushroom ...... 0 .2 difluorobenzamide) and its metabo- Poultry, fat ...... 0.05 lites, in connection with use of the pes- Poultry, meat byproducts ...... 0.05 ticide under section 18 emergency ex- Poultry, meat ...... 0 .05 Sheep, fat ...... 0 .05 emptions granted by EPA. Compliance Sheep, meat ...... 0.05 with the tolerance levels specified Soybean ...... 0.05 below is to be determined by measuring Soybean, hulls ...... 0 .5 only the sum of diflubenzuron (N-[[(4- (2) Tolerances are established for res- chlorophenyl)amino]carbonyl]-2,6- idues of the insecticide diflubenzuron difluorobenzamide), 4- (N-[[(4-chlorophenyl)amino]carbonyl]- chlorophenylyurea and 4-chloroaniline, 2,6-difluorobenzamide), in or on the calculated as the stoichiometric equiv- commodities in the table below. Com- alent of diflubenzuron, in or on the pliance with the tolerance levels speci- commodity. The tolerances are specified below is to be determined by meas- fied in the following table, and will ex- uring only the sum of diflubenzuron (N- pire and are revoked on the dates speci- [[(4-chlorophenyl)amino]carbonyl]-2,6- fied. difluorobenzamide), 4- Expiration/ chlorophenylyurea and 4-chloroaniline, Commodity Parts per revocation calculated as the stoichiometric equiv- million date alent of diflubenzuron, in or on the Alfalfa, forage ...... 6.0 12/31/14 commodity. Alfalfa, hay ...... 6.0 12/31/14 Lemon ...... 0.8 12/31/10 Parts per Commodity million (c) Tolerances with regional registra- Almond, hulls ...... 6 .0 tions. [Reserved] Barley, grain ...... 0 .06 Barley, hay ...... 3 .0 (d) Indirect or inadvertent residues. Barley, straw ...... 1 .8 [Reserved] Brassica, leafy greens, subgroup 5B ...... 9 .0 Cattle, meat byproducts ...... 0.15 [65 FR 33699, May 24, 2000] Citrus, oil ...... 32 Fruit, citrus, group 10–10 ...... 3 .0 EDITORIAL NOTE: For FEDERAL REGISTER ci- Fruit, stone, group 12, except cherry ...... 0 .07 tations affecting § 180.377, see the List of CFR Goat, meat byproducts ...... 0 .15 Sections Affected, which appears in the Grain, aspirated fractions ...... 11 Grass, forage, fodder, and hay, group 17 ...... 6 .0 Finding Aids section of the printed volume Hog, meat byproducts ...... 0 .15 and at www.fdsys.gov. Horse, meat byproducts ...... 0 .15 Nut, tree, group 14 ...... 0 .06 § 180.378 Permethrin; tolerances for Oat, forage ...... 7 .0 residues. Oat, grain ...... 0 .06 Oat, hay ...... 6.0 (a) General. Tolerances are estab- Oat, straw ...... 3.5 lished for the combined residues of the Peanut ...... 0 .10 Peanut, hay ...... 55 insecticide cis- and trans-permethrin Peanut, refined oil ...... 0.20 isomers [cis-(3-phenoxyphenyl)methyl Pear ...... 0 .50 3-(2,2-dichloroethenyl)-2,2- Pepper ...... 1 .0 Pistachio ...... 0.06 dimethylcyclopropane carboxylate] Rice, grain ...... 0 .02 and [trans-(3-phenoxyphenyl)methyl 3- Rice, straw ...... 0 .8 (2,2-dichloroethenyl)-2,2- Sheep, meat byproducts ...... 0 .15 Turnip greens ...... 9 .0 dimethylcyclopropane carboxylate] in/ Wheat, forage ...... 7 .0 on the following food commodities:

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the insecticide cis- and trans- Commodity Parts per million permethrin isomers [cis-(3- Alfalfa, forage ...... 20 phenoxyphenyl)methyl 3-(2,2- Alfalfa, hay ...... 45 dichloroethenyl)-2,2- Almond ...... 0.05 dimethylcyclopropane carboxylate] Almond, hulls ...... 20 Artichoke, globe ...... 5.0 and [trans-(3-phenoxyphenyl)methyl 3- Asparagus ...... 2.0 (2,2-dichloroethenyl)-2,2- Avocado ...... 1 .0 dimethylcyclopropane carboxylate] in/ Broccoli ...... 2 .0 on the following food commodities: Brussels sprouts ...... 1 .0 Cabbage ...... 6 .0 Parts per Cattle, fat ...... 1.5 Commodity million Cattle, meat ...... 0 .10 Cattle, meat byproducts ...... 0.10 Collards ...... 15 Cauliflower ...... 0 .5 Grass, forage ...... 15 Cherry, sweet ...... 4 .0 Grass, hay ...... 15 Cherry, tart ...... 4 .0 Papaya ...... 1 .0 Corn, field, forage ...... 50 Turnip, tops ...... 10 Corn, field, grain ...... 0 .05 Turnip, roots ...... 0 .20 Corn, field, stover ...... 30 Corn, pop, grain ...... 0.05 (d) Indirect or inadvertent residues. Corn, pop, stover ...... 30 Corn, sweet, forage ...... 50 [Reserved] Corn, sweet, kernel plus cob with husks removed ...... 0 .10 [72 FR 52019, Sept. 12, 2007] Corn, sweet, stover ...... 30 Egg ...... 0 .10 § 180.380 Vinclozolin; tolerances for Eggplant ...... 0.50 residues. Fruit, pome, group 11 ...... 0.05 Garlic, bulb ...... 0.10 (a) General. Tolerances are estab- Grain, aspirated fractions ...... 0 .50 lished for the combined residues of the Goat, fat ...... 1 .5 fungicide vinclozolin (3-(3,5- Goat, meat ...... 0.10 dichlorophenyl)-5-ethenyl-5-methyl-2,4- Goat, meat byproducts ...... 0 .10 Hazelnut ...... 0 .05 oxazolidinedione) and its metabolites Hog, fat ...... 0 .05 containing the 3,5-dichloroaniline moi- Hog, meat ...... 0 .05 ety in or on the food commodities in Hog, meat byproducts ...... 0 .05 Horse, fat ...... 1 .5 the table below. There are no U.S. reg- Horse, meat ...... 0 .10 istrations for grape (wine) as of July Horse, meat byproducts ...... 0 .10 30, 1997. Horseradish ...... 0.50 Kiwifruit ...... 2.0 Expiration/ Leaf petioles subgroup 4B ...... 5 .0 Parts per Commodity million Revocation Leafy greens subgroup 4A ...... 20 Date Lettuce, head ...... 20 Milk, fat (reflecting 0.88 ppm in whole milk) ...... 3 .0 Bean, succulent ...... 2.0 11/30/05 Mushroom ...... 5 .0 Canola, seed ...... 1.0 11/30/08 Onion, bulb ...... 0 .10 Cattle, fat ...... 0.05 11/30/08 Peach ...... 1 .0 Cattle, meat ...... 0.05 11/30/08 Pepper, bell ...... 0 .50 Cattle, meat byproducts ...... 0.05 11/30/08 Pistachio ...... 0.10 Egg ...... 0.05 11/30/08 Potato ...... 0 .05 Goat, fat ...... 0.05 11/30/08 Poultry, fat ...... 0.15 Goat, meat ...... 0.05 11/30/08 Poultry, meat ...... 0 .05 Goat, meat byproducts ...... 0.05 11/30/08 Grape, wine ...... 6. 0 None Poultry, meat byproducts ...... 0.05 Hog, fat ...... 0.05 11/30/08 Sheep, fat ...... 1 .5 Hog, meat ...... 0.05 11/30/08 Sheep, meat ...... 0.10 Hog, meat byproducts ...... 0.05 11/30/08 Sheep, meat byproducts ...... 0 .10 Horse, fat ...... 0.05 11/30/08 Soybean, seed ...... 0 .05 Horse, meat ...... 0.05 11/30/08 Spinach ...... 20 Horse, meat byproducts ...... 0.05 11/30/08 Tomato ...... 2.0 Lettuce, head ...... 10.0 11/30/05 Vegetable, cucurbit, group 9 ...... 1.5 Lettuce, leaf ...... 10.0 11/30/05 Walnut ...... 0 .05 Milk ...... 0.05 11/30/08 Watercress ...... 5 .0 Poultry, fat ...... 0.1 11/30/08 Poultry, meat ...... 0.1 11/30/08 (b) Section 18 emergency exemptions. Poultry, meat byproducts ...... 0.1 11/30/08 Sheep, fat ...... 0.05 11/30/08 [Reserved] Sheep, meat ...... 0.05 11/30/08 (c) Tolerances with regional registra- Sheep, meat byproducts ...... 0.05 11/30/08 tions. Tolerances with regional registration, as defined in § 180.1(l) are es- (b) Section 18 emergency exemptions. tablished for the combined residues of [Reserved]

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(c) Tolerances with regional registra- Commodity Parts per tions. [Reserved] million (d) Indirect or inadvertent residues. Milk ...... 0.01 [Reserved] Nut, tree, group 14 ...... 0 .05 (e) Revoked tolerances subject to the Olive ...... 0 .05 channel of trade provisions. The fol- Onion, bulb ...... 0 .05 lowing table lists commodities with Peppermint, tops ...... 0 .05 Persimmon ...... 0 .05 residues of vinclozolin resulting from Pistachio ...... 0.05 lawful use are subject to the channels Pomegranate ...... 0 .05 of trade provisions of section 408(l)(5) Poultry, fat ...... 0.2 of the FFDCA: Poultry, meat ...... 0 .01 Poultry, meat byproducts ...... 0.01 Sheep, fat ...... 0 .01 Commodity Parts per million Sheep, meat ...... 0.01 Sheep, meat byproducts ...... 0 .01 Cucumber ...... 1 .0 Soybean ...... 0.05 Fruit, stone, except plum, prune, fresh ...... 25.0 Pepper, bell ...... 3 .0 Spearmint, tops ...... 0 .05 Strawberry ...... 10.0 (b) Section 18 emergency exemptions. [62 FR 38474, July 18, 1997, as amended at 63 [Reserved] FR 7308, Feb. 13, 1998; 65 FR 44468, July 18, (c) Tolerances with regional registra- 2000; 67 FR 40189, June 12, 2002; 68 FR 56189, tions. Tolerances with regional reg- Sept. 30, 2003; 68 FR 69323, Dec. 12, 2003; 70 FR istration are established for residues of 55268, Sept. 21, 2005] the herbicide oxyfluorfen [2-chloro-1-(3- ethoxy-4-nitrophenoxy)-4- § 180.381 Oxyfluorfen; tolerances for (trifluoromethyl)benzene] in or on the residues. following food commodities: (a) General. Tolerances are established for residues of the herbicide Commodity Parts per oxyfluorfen [2-chloro-1-(3-ethoxy-4- million nitrophenoxy)-4- Blackberry ...... 0 .05 (trifluoromethyl)benzene] in or on the Chickpea, seed ...... 0 .05 following food commodities: Grass, forage ...... 0 .05 Grass, hay ...... 0 .05 Grass, seed screenings ...... 0 .05 Commodity Parts per million Guava ...... 0 .05 Papaya ...... 0 .05 Almond, hulls ...... 0 .1 Raspberry ...... 0 .05 Artichoke, globe ...... 0.05 Avocado ...... 0 .05 Taro, corm ...... 0 .05 Banana ...... 0.05 Taro, leaves ...... 0 .05 Broccoli ...... 0 .05 Cabbage ...... 0 .05 (d) Indirect or inadvertent residues. Cacao bean, dried bean ...... 0 .05 Cattle, fat ...... 0.01 [Reserved] Cattle, meat ...... 0 .01 Cattle, meat byproducts ...... 0.01 [45 FR 85022, Dec. 24, 1980] Cauliflower ...... 0 .05 EDITORIAL NOTE: For FEDERAL REGISTER ci- Coffee, bean, green ...... 0 .05 Corn, field, grain ...... 0 .05 tations affecting § 180.381, see the List of CFR Cotton, undelinted seed ...... 0 .05 Sections Affected, which appears in the Date, dried fruit ...... 0 .05 Finding Aids section of the printed volume Egg ...... 0 .03 and at www.fdsys.gov. Feijoa ...... 0 .05 Fig ...... 0 .05 Fruit, pome, group 11 ...... 0.05 § 180.383 Sodium salt of acifluorfen; Fruit, stone, group 12 ...... 0 .05 tolerances for residues. Goat, fat ...... 0 .01 (a) General. Tolerances are estab- Goat, meat ...... 0.01 Goat, meat byproducts ...... 0 .01 lished for combined residues of the her- Grape ...... 0 .05 bicide sodium salt of acifluorfen, so- Hog, fat ...... 0 .01 dium 5-[2-chloro-4- Hog, meat ...... 0 .01 Hog, meat byproducts ...... 0 .01 (trifluoromethyl)phenoxy]-2- Horse, fat ...... 0 .01 nitrobenzoate, and its metabolites (the Horse, meat ...... 0 .01 corresponding acid, methyl ester, and Horse, meat byproducts ...... 0 .01 Horseradish ...... 0.05 amino analogues) in or on the fol- Kiwifruit ...... 0.05 lowing raw agricultural commodities:

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(d) Indirect or inadvertent residues. Commodity Parts per million [Reserved] Peanut ...... 0 .1 [67 FR 3118, Jan. 23, 2002] Rice, grain ...... 0 .1 Rice, straw ...... 0 .2 § 180.385 Diclofop-methyl; tolerances Soybean, seed ...... 0 .1 for residues. Strawberry ...... 0 .05 (a) General. Tolerances are estab- (b) Section 18 emergency exemptions. lished for the combined residues of the [Reserved] herbicide diclofop-methyl (methyl 2-[4- (c) Tolerances with regional restric- (2,4- tions. [Reserved] dichlorophenoxy)phenoxy]propanoate) (d) Indirect or inadvertent residues. and its metabolites, 2-[4-(2,4- [Reserved] dichlorophenoxy)phenoxy]propanoic acid and 2-[4-(2,4-dichloro-5- [45 FR 24877, Apr. 11, 1980, as amended at 46 hydroxyphenoxy)phenoxy]propanoic FR 61272, Dec. 16, 1981; 47 FR 39490, Sept. 8, acid, in or on the following raw agri- 1982; 61 FR 30165, June 14, 1996; 62 FR 39974, cultural commodities: July 25, 1997; 67 FR 35048, May 17, 2002; 69 FR 6567, Feb. 11, 2004; 71 FR 54434, Sept. 15, 2006] Parts per Commodity million § 180.384 Mepiquat (N,N-dimethylpiperidinium); tolerances for residues. Barley, grain ...... 0 .1 Barley, straw ...... 0 .1 (a) General. (1) Tolerances are estab- Wheat, grain ...... 0 .1 lished for residues of the plant growth Wheat, straw ...... 0 .1 regulator mepiquat (N,N- (b) Section 18 emergency exemptions. dimethylpiperidinium) in or on the fol- [Reserved] lowing commodities: (c) Tolerances with regional registra- Parts per tions. [Reserved] Commodity million (d) Indirect or inadvertent residues. [Reserved] Cattle, meat byproducts ...... 0.1 Cotton, gin byproducts ...... 6 .0 [45 FR 23425, Apr. 7, 1980, as amended at 50 Cotton, undelinted seed ...... 2 .0 FR 20211, May 15, 1985; 51 FR 3599, Jan. 29, Goat, meat byproducts ...... 0 .1 1986; 51 FR 19176, May 28, 1986; 63 FR 57077, Hog, meat byproducts ...... 0 .1 Oct. 26, 1998; 72 FR 41931, Aug. 1, 2007] Horse, meat byproducts ...... 0 .1 Sheep, meat byproducts ...... 0 .1 §§ 180.388–180.389 [Reserved] (2) Tolerances are established for res- § 180.390 Tebuthiuron; tolerances for idues of the plant growth regulator residues. mepiquat chloride (N,N- (a) General. (1) Tolerances are estab- dimethylpiperidinium chloride) in or lished for the combined residues of the on the following commodities: herbicide tebuthiuron (N-(5-(1,1- dimethylethyl)-1,3,4-thiadiazol-2-yl)- Commodity Parts per million N,N’-dimethylurea) and its metabolites Cattle, fat ...... 0.1 N-(5-(2-hydroxy-1,1-dimethylethyl)- Cattle, meat ...... 0 .1 1,3,4-thiadiazol-2-yl)-N,N’- Goat, fat ...... 0 .1 dimethylurea, N-(5-(1,1-dimethylethyl)- Goat, meat ...... 0.1 1,3,4-thiadiazol-2-yl)-N-methylurea, and Grape ...... 1 .0 N-(5-(1,1-dimethylethyl)-1,3,4- Grape, raisin ...... 5 .0 Hog, fat ...... 0 .1 thiadiazol-2-yl)-N’-hydroxymethyl-N- Hog, meat ...... 0 .1 methylurea in or on the following raw Horse, fat ...... 0 .1 agricultural commodities: Horse, meat ...... 0 .1 Sheep, fat ...... 0 .1 Commodity Parts per Sheep, meat ...... 0.1 million

Grass, forage ...... 10 .0 (b) Section 18 emergency exemptions. Grass, hay ...... 10 .0 [Reserved] (c) Tolerances with regional registra- (2) Tolerances are established for the tions. [Reserved] combined residues of the herbicide

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tebuthiuron (N-(5-(1,1-dimethylethyl)- pyrimidinone(3-(4- 1,3,4-thiadiazol-2-yl)-N,N’- (trifluoromethyl)phenyl)-1-(2-(4- dimethylurea) and its metabolites N-(5- (trifluoromethyl)phenyl)ethenyl)-2- (1,1-dimethylethyl)-1,3,4-thiadiazol-2- propenylidene)hydrazone in or on the yl)-N-methylurea, N-(5-(1,1- following raw agricultural commod- dimethylethyl)-1,3,4-thiadiazol-2- ities: yl)urea, 2-dimethylethyl-5-amino-1,3,4- Parts per thiadiazole, and N-(5-(1,1- Commodity million dimethylethyl)-1,3,4-thiadiazol-2-yl)-N’- hydroxymethyl-N-methylurea in or on Grass, forage ...... 2 .0 Grass, hay ...... 2 .0 the following raw agricultural com- Pineapple ...... 0.05 modities: (b) Section 18 emergency exemptions. Parts per Commodity million [Reserved] (c) Tolerances with regional registra- Cattle, fat ...... 1.0 tions. [Reserved] Cattle, meat ...... 1 .0 Cattle, meat byproducts ...... 5.0 (d) Indirect or inadvertent residues. Goat, fat ...... 1 .0 [Reserved] Goat, meat ...... 1.0 Goat, meat byproducts ...... 5 .0 [45 FR 55198, Aug. 19, 1980, as amended at 63 Horse, fat ...... 1 .0 FR 10543, Mar. 4, 1998; 63 FR 65073, Nov. 25, Horse, meat ...... 1 .0 1998; 66 FR 28672, May 24, 2001; 68 FR 37764, Horse, meat byproducts ...... 5 .0 June 25, 2003; 68 FR 48312, Aug. 13, 2003; 72 FR Sheep, fat ...... 1 .0 41931, Aug. 1, 2007] Sheep, meat ...... 1.0 Sheep, meat byproducts ...... 5 .0 § 180.396 Hexazinone; tolerances for (3) A tolerance is established for the residues. combined residues of the herbicide (a) General. (1) Tolerances are estab- tebuthiuron (N-(5-(1,1-dimethylethyl)- lished for residues of the herbicide 1,3,4-thiadiazol-2-yl)-N,N’- hexazinone, 3-cyclohexyl-6- dimethylurea) and its metabolites N-(5- (dimethylamino)-1-methyl-1,3,5-tri- (1,1-dimethylethyl)-1,3,4-thiadiazol-2- azine-2,4-(1H, 3H)-dione, including its yl)-N-methylurea, N-(5-(2-hydroxy-1,1- metabolites and degradates, in or on dimethylethyl)-1,3,4-thiadiazol-2-yl)-N- the commodities in the following table. methylurea, N-(5-(1,1-dimethylethyl)- Compliance with the tolerance levels 1,3,4-thiadiazol-2-yl)urea, N-(5-(1,1- specified in this paragraph is to be de- dimethylethyl)-1,3,4-thiadiazol-2-yl)-N’- termined by measuring only the sum of hydroxymethyl-N-methylurea, and N- hexazinone, 3-cyclohexyl-6- (5-(2-hydroxy-1,1-dimethylethyl)-1,3,4- (dimethylamino)-1-methyl-1,3,5-tri- thiadiazol-2-yl)-N’-hydroxymethyl-N- azine-2,4-(1H, 3H)-dione, and its plant methylurea in or on the following raw metabolites: metabolite A, 3-(4- agricultural commodities: hydroxycyclohexyl)-6- (dimethylamino)-1-methyl-1,3,5-tri- Commodity Parts per azine-2,4-(1H, 3H)-dione, metabolite B, million 3-cyclohexyl-6-(methylamino)-1-meth- Milk ...... 0.8 yl-1,3,5-triazine-2,4-(1H, 3H)-dione, metabolite C, 3-(4-hydroxycyclohexyl)-6- (b) Section 18 emergency exemptions. (methylamino)-1-methyl-1,3,5-triazine- [Reserved] 2,4-(1H, 3H)-dione, metabolite D, 3- (c) Tolerances with regional registra- cyclohexyl-1-methyl-1,3,5-triazine-2,4,6- tions. [Reserved] (1H, 3H, 5H)-trione, and metabolite E, (d) Indirect or inadvertent residues. 3-(4-hydroxycyclohexyl)-1-methyl-1,3,5- [Reserved] triazine-2,4,6-(1H, 3H, 5H)-trione, calculated as the stoichiometric equiva- [72 FR 53461, Sept. 19, 2007] lent of hexazinone, in or on the com- § 180.395 Hydramethylnon; tolerances modity. for residues. Parts per (a) General. Tolerances are estab- Commodity million lished for residues of the insecticide Alfalfa, forage ...... 2.0 tetrahydro-5,5-dimethyl-2(1H)- Alfalfa, hay ...... 4.0

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hydroxycyclohexyl)-6-(methylamino)-1- Commodity Parts per million methyl-1,3,5-triazine-2,4-(1H, 3H)-dione, Alfalfa, seed ...... 2 .0 metabolite C-2, 3-(3- Blueberry ...... 0 .6 hydroxycyclohexyl)-6-(methylamino)-1- Grass, forage ...... 250 methyl-1,3,5-triazine-2,4-(1H, 3H)-dione, Grass, hay ...... 230 Pineapple ...... 0.6 and metabolite F, 3-cyclohexyl-6- Sugarcane, cane ...... 0.6 amino-1-methyl-1,3,5-triazine-2,4-(1H, Sugarcane, molasses ...... 4 .0 3H)-dione, calculated as the stoichiometric equivalent of hexazinone, in or (2) Tolerances are established for res- on the commodity. idues of the herbicide hexazinone, 3- cyclohexyl-6-(dimethylamino)-1-meth- Commodity Parts per yl-1,3,5-triazine-2,4-(1H, 3H)-dione, in- million cluding its metabolites and degradates, Milk ...... 11 in or on the commodities in the following table. Compliance with the tol- (b) Section 18 emergency exemptions. erance levels specified in this para- [Reserved] graph is to be determined by measuring (c) Tolerances with regional registra- only the sum of hexazinone, 3- tions. [Reserved] cyclohexyl-6-(dimethylamino)-1-meth- (d) Indirect or inadvertent residues. yl-1,3,5-triazine-2,4-(1H, 3H)-dione, and [Reserved] its animal tissue metabolites: metabo- [65 FR 33713, May 24, 2000, as amended at 71 lite B, 3-cyclohexyl-6-(methylamino)-1- FR 56399, Sept. 27, 2006; 75 FR 60244, Sept. 29, methyl-1,3,5-triazine-2,4-(1H, 3H)-dione, 2010] and metabolite F, 3-cyclohexyl-6- amino-1-methyl-1,3,5-triazine-2,4-(1H, § 180.399 Iprodione; tolerances for res- 3H)-dione, calculated as the stoichio- idues. metric equivalent of hexazinone, in or (a) General. (1) Tolerances are estab- on the commodity. lished for the combined residues of the fungicide iprodione [3-(3,5- Parts per Commodity million dichlorophenyl)-N-(1-methylethyl)-2,4- dioxo-1-imidazolidinecarboxamide], its Cattle, fat ...... 0.1 isomer 3-(1-methylethyl)-N-(3,5- Cattle, meat ...... 0 .5 Cattle, meat byproducts ...... 4.0 dichlorophenyl)-2,4-dioxo-1- Goat, fat ...... 0 .1 imidazolidinecarboxamide, and its me- Goat, meat ...... 0.5 tabolite 3-(3,5-dichlorophenyl)-2,4- Goat, meat byproducts ...... 4 .0 Hog, fat ...... 0 .1 dioxo-1-imidazolidine-carboxamide in Hog, meat ...... 0 .5 or on the following food commodities: Hog, meat byproducts ...... 4 .0 Horse, fat ...... 0 .1 Commodity Parts per Horse, meat ...... 0 .5 million Horse, meat byproducts ...... 4 .0 Sheep, fat ...... 0 .1 Almond, hulls ...... 2 .0 Sheep, meat ...... 0.5 Almond ...... 0.3 Sheep, meat byproducts ...... 4 .0 Apricot ...... 20 .0 Bean, dry, seed ...... 2 .0 Bean, forage ...... 90 .0 (3) A tolerance is established for resi- Bean, succulent ...... 2 .0 dues of the herbicide hexazinone, 3- Blueberry ...... 15 .0 cyclohexyl-6-(dimethylamino)-1-meth- Boysenberry ...... 15 .0 Broccoli ...... 25 .0 yl-1,3,5-triazine-2,4-(1H, 3H)-dione, in- Caneberry subgroup 13A ...... 25 .0 cluding its metabolites and degradates, Carrot, roots ...... 5.0 in or on the commodity in the fol- Cherry, sweet, postharvest ...... 20 .0 lowing table. Compliance with the tol- Cherry, tart ...... 20.0 Cotton, undelinted seed ...... 0 .10 erance level specified in this paragraph Cowpea, hay ...... 90 .0 is to be determined by measuring only Currant ...... 15.0 the sum of hexazinone, 3-cyclohexyl-6- Garlic ...... 0 .1 Ginseng ...... 2 .0 (dimethylamino)-1-methyl-1,3,5-tri- Ginseng, dried root ...... 4 .0 azine-2,4-(1H, 3H)-dione, and its me- Grape ...... 60 .0 tabolites: metabolite B, 3-cyclohexyl-6- Grape, raisin ...... 300 Kiwifruit ...... 10.0 (methylamino)-1-methyl-1,3,5-triazine- Lettuce ...... 25.0 2,4-(1H, 3H)-dione, metabolite C, 3-(4- Nectarine, postharvest ...... 20.0

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(c) Tolerances with regional registra- Commodity Parts per million tions. Tolerances with regional reg- Onion, bulb ...... 0 .5 istration, as defined in § 180.1(l), are es- Peach, postharvest ...... 20.0 tablished for the combined residues of Peanut ...... 0 .5 the fungicide iprodione [3-(3,5- Peanut, hay ...... 150.0 dichlorophenyl)-N-(1-methylethyl)-2,4- Plum, postharvest ...... 20 .0 Plum, prune ...... 20.0 dioxo-1-imidazolidinecarboxamide], its Potato ...... 0 .5 isomer [3-(1-methylethyl)-N-(3,5- Raspberry ...... 15 .0 dichlorophenyl)-2,4-dioxo-1- Rice, bran ...... 30.0 imidazolidinecarboxamide], and its me- Rice, grain ...... 10 .0 Rice, hulls ...... 50 .0 tabolite [3-(3,5-dichlorophenyl)-2,4- Rice, straw ...... 20 .0 dioxo-1-imidazolidinecarboxamide] in Strawberry ...... 15.0 or on the following food commodity:

(2) Tolerances are established for the Commodity Parts per combined residues of iprodione [3-(3,5- million dichlorophenyl)-N-(1-methylethyl)-2,4- Mustard greens ...... 15.0 dioxo-1-imidazolidinecarboxamide], its isomer [3-(1-methylethyl)-N-(3,5- (d) Indirect or inadvertent residues. dichlorophenyl)-2,4-dioxo-1- [Reserved] imidazolidinecarboxamide, and its metabolites [3-(3,5-dichlorophenyl)-2,4- [48 FR 40385, Sept. 7, 1983] dioxo-1-imidazolidine-carboxamide] EDITORIAL NOTE: For FEDERAL REGISTER ci- and [N-(3,5-dichloro-4-hydroxyphenyl)- tations affecting § 180.399, see the List of CFR ureido-carboxamide], all expressed as Sections Affected, which appears in the iprodione equivalents in or on the fol- Finding Aids section of the printed volume lowing food commodities of animal ori- and at www.fdsys.gov. gin: § 180.401 Thiobencarb; tolerances for residues. Commodity Parts per million (a) General. Tolerances are estab- Cattle, fat ...... 0.5 lished for the combined residues of the Cattle, kidney ...... 3 .0 herbicide thiobencarb (S-[(4- Cattle, liver ...... 3 .0 chlorophenyl)methyl]diethyl- Cattle, meat ...... 0 .5 Cattle, meat byproducts, except kidney and liver 0.5 carbamothioate) and its chlorobenzyl Egg ...... 1 .5 and chlorophenyl moiety-containing Goat, fat ...... 0 .5 metabolites in or on the following raw Goat, kidney ...... 3 .0 agricultural commodities: Goat, liver ...... 3.0 Goat, meat ...... 0.5 Part per Goat, meat byproducts, except kidney and liver 0 .5 Commodity million Hog, fat ...... 0 .5 Hog, kidney ...... 3.0 Cattle, fat ...... 0.2 Hog, liver ...... 3 .0 Cattle, meat byproducts ...... 0.2 Hog, meat ...... 0 .5 Cattle, meat ...... 0 .2 Hog, meat byproducts, except kidney and liver .. 0 .5 Egg ...... 0 .2 Horse, fat ...... 0 .5 Goat, fat ...... 0 .2 Horse, kidney ...... 3 .0 Goat, meat byproducts ...... 0 .2 Horse, liver ...... 3 .0 Goat, meat ...... 0.2 Horse, meat ...... 0 .5 Hog, fat ...... 0 .2 Horse, meat byproducts, except kidney and liver 0 .5 Hog, meat byproducts ...... 0 .2 Milk ...... 0.5 Poultry, fat ...... 3.5 Hog, meat ...... 0 .2 Poultry, liver ...... 5 .0 Horse, fat ...... 0 .2 Poultry, meat ...... 1 .0 Horse, meat byproducts ...... 0 .2 Poultry, meat byproducts, except liver ...... 1 .0 Horse, meat ...... 0 .2 Sheep, fat ...... 0 .5 Milk ...... 0.05 Sheep, kidney ...... 3.0 Poultry, fat ...... 0.2 Sheep, liver ...... 3.0 Poultry, meat byproducts ...... 0.2 Sheep, meat ...... 0.5 Poultry, meat ...... 0 .2 Sheep, meat byproducts, except kidney and Rice, grain ...... 0 .2 liver ...... 0 .5 Rice, straw ...... 1 .0 Sheep, fat ...... 0 .2 (b) Section 18 emergency exemptions. Sheep, meat byproducts ...... 0 .2 [Reserved] Sheep, meat ...... 0.2

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(b) Section 18 emergency exemptions. § 180.404 Profenofos; tolerances for [Reserved] residues. (c) Tolerances with regional registra- (a) General. Tolerances are estab- tions. Tolerances with regional reg- lished for residues of the insecticide istration, as defined in § 180.1(l), are es- profenofos (O-(4-bromo-2- tablished for residues of the herbicide chlorophenyl)-O-ethyl-S-propyl thiobencarb (S-[(4-chloro- phosphorothioate) in or on the fol- phenyl)methyl]diethylcarbamothioate) lowing food commodities: and its chlorobenzyl and chlorophenyl moiety-containing metabolites in or on Commodity Parts per the following raw agricultural com- million modities: Cattle, fat ...... 0.05 Cattle, meat ...... 0 .05 Cattle, meat byproducts ...... 0.05 Commodity Parts per million Cotton, gin byproducts ...... 55 .0 Cotton, undelinted seed ...... 2 .0 Celery ...... 0 .2 Goat, fat ...... 0 .05 Endive ...... 0.2 Goat, meat ...... 0.05 Lettuce ...... 0.2 Goat, meat byproducts ...... 0 .05 Horse, fat ...... 0 .05 (d) Indirect or inadvertent residues. Horse, meat ...... 0 .05 Horse, meat byproducts ...... 0 .05 [Reserved] Milk ...... 0.01 Sheep, fat ...... 0 .05 [47 FR 6833, Feb. 17, 1982, as amended at 56 Sheep, meat ...... 0.05 FR 2440, Jan. 23, 1991; 76 FR 34885, June 15, Sheep, meat byproducts ...... 0 .05 2011] (b) Section 18 emergency exemptions. § 180.403 Thidiazuron; tolerances for [Reserved] residues. (c) Tolerances with regional registra- (a) General. Tolerances are estab- tions. [Reserved] lished for the combined residues of the (d) Indirect or inadvertent residues. defoliant thidiazuron (N-phenyl-N-1,2,3- [Reserved] thiadiazol-5-ylurea) and its aniline containing metabolites in or on the fol- [65 FR 33700, May 24, 2000, as amended at 66 FR 50833, Oct. 5, 2001; 67 FR 49617, July 31, lowing food commodities: 2002; 72 FR 54579, Sept. 26, 2007] Parts per Commodity million § 180.405 Chlorsulfuron; tolerances for residues. Cattle, fat ...... 0.4 Cattle, meat ...... 0 .4 (a) General. (1) Tolerances are estab- Cattle, meat byproducts ...... 0.4 lished for the combined residues of Cotton, gin byproducts ...... 24 .0 chlorsulfuron (2-chloro-N-[(4-methoxy- Cotton, undelinted seed ...... 0 .3 6-methyl-1,3,5-triazin-2- Goat, fat ...... 0 .4 Goat, meat ...... 0.4 yl)aminocarbonyl]benzenesulfonamide) Goat, meat byproducts ...... 0 .4 and its metabolite, 2-chloro-5-hydroxy- Hog, fat ...... 0 .4 N-[(4-methoxy-6-methyl-1,3,5-triazin-2- Hog, meat ...... 0 .4 Hog, meat byproducts ...... 0 .4 yl)aminocarbonyl] benzenesulfonamide Horse, fat ...... 0 .4 in or on the following raw agricultural Horse, meat ...... 0 .4 commodities: Horse, meat byproducts ...... 0 .4 Milk ...... 0.05 Parts per Sheep, fat ...... 0 .4 Commodity million Sheep, meat ...... 0.4 Sheep, meat byproducts ...... 0 .4 Barley, grain ...... 0 .1 Barley, straw ...... 0 .5 Oat, forage ...... 20 .0 (b) Section 18 emergency exemptions. Oat, grain ...... 0 .1 [Reserved] Oat, straw ...... 0.5 (c) Tolerances with regional registra- Wheat, forage ...... 20.0 tions. [Reserved] Wheat, grain ...... 0 .1 Wheat, straw ...... 0 .5 (d) Indirect or inadvertent residues. [Reserved] (2) Tolerances are established for res- [65 FR 33700, May 24, 2000, as amended at 72 idues of chlorsulfuron (2-chloro-N-[(4- FR 53462, Sept. 19, 2007] methoxy-6-methyl-1,3,5-triazin-2-

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yl)aminocarbonyl] (d) Indirect or inadvertent residues. benzenesulfonamide) in or on the fol- [Reserved] lowing raw agricultural commodities. [62 FR 44595, Aug. 22, 1997, as amended at 75 Parts per FR 60245, Sept. 29, 2010] Commodity million § 180.408 Metalaxyl; tolerances for res- Cattle, fat ...... 0.3 idues. Cattle, meat ...... 0 .3 Cattle, meat byproducts ...... 0.3 (a) General. Tolerances are estab- Goat, fat ...... 0 .3 lished for the combined residues of the Goat, meat ...... 0.3 Goat, meat byproducts ...... 0 .3 fungicide metalaxyl [N-(2,6- Grass, forage ...... 11 .0 dmethylphyenyl)-N-(methoxyacetyl) Grass, hay ...... 19 .0 alanine methylester] and its metabo- Hog, fat ...... 0 .3 Hog, meat ...... 0 .3 lites containing the 2,6- Hog, meat byproducts ...... 0 .3 dimethylaniline moiety, and N-(2-hy- Horse, fat ...... 0 .3 droxy methyl-6-methylphenyl)-N- Horse, meat ...... 0 .3 Horse, meat byproducts ...... 0 .3 (methoxyacetyl)-alanine methyl ester, Milk ...... 0.1 each expressed as metalaxyl equiva- Sheep, fat ...... 0 .3 lents, in or on the following food com- Sheep, meat ...... 0.3 Sheep, meat byproducts ...... 0 .3 modities: Parts per (b) Section 18 emergency exemptions. Commodity million [Reserved] Alfalfa, forage ...... 6.0 (c) Tolerances with regional registra- Alfalfa, hay ...... 20.0 tions. [Reserved] Almond ...... 0.5 (d) Indirect or inadvertent residues. Almond, hulls ...... 10 .0 [Reserved] Apple ...... 0.2 Apple, wet pomace ...... 0 .4 [67 FR 52873, Aug. 14, 2002] Apricot, dried ...... 4 .0 Asparagus ...... 7.0 Avocado ...... 4 .0 § 180.407 Thiodicarb; tolerances for Beet, garden, roots ...... 0 .1 residues. Beet, garden, tops ...... 0 .1 (a) General. Tolerances are estab- Beet, sugar ...... 0 .1 Beet, sugar, molasses ...... 1 .0 lished for the combined residues of the Beet, sugar, roots ...... 0 .5 insecticide thiodicarb (dimethyl N,N′- Beet, sugar, tops ...... 10.0 [thiobis[[(methylimino)carbonyloxy]] Blueberry ...... 2 .0 Broccoli ...... 2 .0 bis[ethanimidothioate]) and its me- Brussels sprouts ...... 2 .0 tabolite methomyl (S-methyl N- Cabbage ...... 1 .0 [(methylcarbamoyl) Cattle, fat ...... 0.4 Cattle, kidney ...... 0 .4 oxy]thioacetimidate) in or on the fol- Cattle, liver ...... 0 .4 lowing food commodities or groups. Cattle, meat ...... 0 .05 The time-limited tolerances expire and Cattle, meat byproducts, except kidney and liver 0.05 are revoked on the dates listed in the Cauliflower ...... 1 .0 Citrus, oil ...... 7.0 following table: Citrus, dried pulp ...... 7 .0 Clover, forage ...... 1.0 Parts per Expiration/ Clover, hay ...... 2.5 Commodity million revocation Cotton, undelinted seed ...... 0 .1 date Cranberry ...... 4 .0 Egg ...... 0 .05 Broccoli ...... 7.0 None Fruit, citrus ...... 1 .0 Cabbage ...... 7.0 None Fruit, stone, group 12 ...... 1 .0 Cauliflower ...... 7.0 None Ginseng ...... 3 .0 Corn, sweet, kernel plus cob with Goat, fat ...... 0 .4 husks removed ...... 2.0 None Goat, kidney ...... 0 .4 Cotton, undelinted seed ...... 0.4 None Goat, liver ...... 0.4 Soybean, hulls ...... 0.8 None Goat, meat ...... 0.05 Soybean ...... 0.2 None Goat, meat byproducts, except kidney and liver 0 .05 Vegetable, leafy, except brassica, Grain, cereal, group 15, except barley, oat and group 4 ...... 35 None wheat ...... 0.1 Grain, crop ...... 0 .1 (b) Section 18 emergency exemptions. Grape ...... 2 .0 [Reserved] Grape, raisin ...... 6 .0 Grass, forage ...... 10 .0 (c) Tolerances with regional registra- Grass, hay ...... 25 .0 tions. [Reserved] Hog, fat ...... 0 .4

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fungicide metalaxyl [N-(2,6- Commodity Parts per million dimethylphenyl)-N-(methoxyacetyl) al- Hog, kidney ...... 0.4 anine methyl ester] and its metabolites Hog, liver ...... 0 .4 containing the 2,6-dimethylaniline Hog, meat ...... 0 .05 moiety, and N-(2-hydroxy methyl-6- Hog, meat byproducts, except kidney and liver .. 0 .05 Hop, dried cones ...... 20 methyl)-N-(methoxyacetyl)-alanine Hop, vines ...... 2 .0 methylester, each expressed as Horse, fat ...... 0 .4 metalaxyl, in or on the following raw Horse, kidney ...... 0 .4 Horse, liver ...... 0 .4 agricultural commodity: Horse, meat ...... 0 .05 Horse, meat byproducts, except kidney and liver 0 .05 Commodity Parts per Lettuce, head ...... 5.0 million Milk ...... 0.02 Mustard greens ...... 5.0 Papaya ...... 0 .1 Onion, bulb ...... 3 .0 Onion, green ...... 10.0 (d) Indirect or inadvertent tolerances. Peanut ...... 0 .2 Tolerances are established for indirect Peanut, hay ...... 20.0 Peanut, meal ...... 1 .0 or inadvertent residues of metalaxyl in Peanut, hulls ...... 2 .0 or on the food commodities when Pineapple ...... 0.1 present therein as a result of the appli- Pineapple, fodder ...... 0 .1 Pineapple, forage ...... 0 .1 cation of metalaxyl to growing crops Plum, prune, dried ...... 4.0 listed in paragraph (a) of this section Potato, chips ...... 4 .0 and other non-food crops to read as fol- Potato, granules, flakes ...... 4.0 lows: Potato, processed potato waste ...... 4 .0 Potato, wet peel ...... 4 .0 Part per Poultry, fat ...... 0.4 Commodity million Poultry, kidney ...... 0 .4 Poultry, liver ...... 0 .4 Barley, bran ...... 1 .0 Poultry, meat ...... 0 .05 Barley, flour ...... 1 .0 Poultry, meat byproducts, except kidney and Barley, grain ...... 0 .2 liver ...... 0 .05 Potato ...... 0 .5 Barley, pearled barley ...... 1 .0 Raspberry ...... 0 .5 Barley, straw ...... 2 .0 Sheep, fat ...... 0 .4 Grain, cereal, forage, fodder and straw, group Sheep, kidney ...... 0.4 16, except barley, oat, and wheat; forage ...... 1 .0 Sheep, liver ...... 0.4 Grain, cereal, forage, fodder and straw, group Sheep, meat ...... 0.05 16, except barley, oat, and wheat; stover ...... 1 .0 Sheep, meat byproducts, except kidney and Grain, cereal, forage, fodder and straw, group liver ...... 0 .05 16, except barley, oat, and wheat; straw ...... 1 .0 Soybean, hulls ...... 2 .0 Oat, flour ...... 1 .0 Soybean, meal ...... 2.0 Oat, forage ...... 2 .0 Soybean, seed ...... 1 .0 Oat, grain ...... 0 .2 Spinach ...... 10 .0 Oat, groats, rolled oats ...... 1 .0 Strawberry ...... 10.0 Oat, straw ...... 2.0 Sunflower, seed ...... 0.1 Wheat, bran ...... 1.0 Sunflower, forage ...... 0.1 Wheat, flour ...... 1 .0 Tomato, paste ...... 3 .0 Wheat, forage ...... 2 .0 Tomato, puree ...... 3 .0 Vegetable, brassica, leafy, group 5, except broc- Wheat, germ ...... 1 .0 coli, cabbage, cauliflower, brussels sprouts, Wheat, grain ...... 0 .2 and mustard greens ...... 0 .1 Wheat, middlings ...... 1 .0 Vegetable, cucurbit, group 9 ...... 1.0 Wheat, shorts ...... 1 .0 Vegetable, foilage of legume, group 7 ...... 8 .0 Wheat, straw ...... 2 .0 Vegetable, fruiting, group 8 ...... 1.0 Vegetable, leafy, except brassica, group 4, except spinach ...... 5 .0 [65 FR 33700, May 24, 2000, as amended at 72 Vegetable, leaves of root and tuber, group 2 ..... 15 .0 FR 35666, June 29, 2007; 74 FR 46374, Sept. 9, Vegetable, legume, cannery waste ...... 5 .0 2009; 75 FR 56015, Sept. 15, 2010] Vegetable, legume, group 6 ...... 0 .2 Vegetable, root and tuber, group 1 ...... 0 .5 § 180.409 Pirimiphos-methyl; toler- Walnut ...... 0 .5 ances for residues. (b) Section 18 emergency exemptions. (a) General. Tolerances are estab- [Reserved] lished for residues of the insecticide (c) Tolerances with regional registra- pirimiphos-methyl (O-(2-diethylamino- tions. Tolerances with regional reg- 6-methyl-4-pyrimidinyl) O,O-dimethyl istration (refer to § 180.1(m)) are estab- phosphorothioate) in or on the fol- lished for the combined residues of the lowing raw agricultural commodities:

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specified in the table below is to be de- Commodity Parts per million termined by measuring only the sum of Cattle, fat ...... 0.02 fluazifop-P-butyl, butyl(R)-2-[4-[[5- Cattle, meat byproducts ...... 0.02 (trifluoromethyl)-2- Corn, field, grain ...... 8 .0 pyridinyl]oxy]phenoxy]propanoate, and Corn, pop, grain ...... 8.0 Goat, fat ...... 0 .02 the free and conjugated forms of the re- Goat, meat byproducts ...... 0 .02 solved isomer of fluazifop, (R)-2-[4-[[5- Grain, aspirated fractions ...... 20.0 (trifluoromethyl)-2- Hog, fat ...... 0 .02 Hog, meat byproducts ...... 0 .02 pyridinyl]oxy]phenoxy]propanoic acid, Horse, fat ...... 0 .02 calculated as the stoichiometric equiv- Horse, meat byproducts ...... 0 .02 alent of fluazifop, in or on the com- Poultry, fat ...... 0.02 Sheep, fat ...... 0 .02 modity. Sheep, meat byproducts ...... 0 .02 Sorghum, grain, grain ...... 8 .0 Parts per Commodity million

(b) Section 18 emergency exemptions. Banana ...... 0.01 [Reserved] Beans, dry, seed ...... 50 (c) Tolerances with regional registra- Beet, sugar, dried pulp ...... 1 .0 Beet, sugar, molasses ...... 3 .5 tions. [Reserved] Beet, sugar, roots ...... 0 .25 (d) Indirect or inadvertent residues. Carrot, roots ...... 2.0 [Reserved] Cattle, fat ...... 0.05 Cattle, meat ...... 0 .05 [65 FR 33714, May 24, 2000, as amended at 67 Cattle, meat byproducts ...... 0.05 FR 41807, June 19, 2002; 67 FR 49617, July 31, Citrus, dried pulp ...... 0 .40 2002; 70 FR 44492, Aug. 3, 2005; 72 FR 53462, Citrus, juice ...... 0 .06 Citrus, oil ...... 30.0 Sept. 19, 2007] Cotton, gin byproducts ...... 1 .5 Cotton, refined oil ...... 1.3 § 180.410 Triadimefon; tolerances for Cotton, undelinted seed ...... 1 .0 residues. Egg ...... 0 .05 Endive ...... 6.0 (a) General. Tolerances are estab- Fruit, citrus, group 10 ...... 0 .03 lished for the combined residues of the Fruit, stone ...... 0 .05 fungicide triadimefon, 1-(4- Goat, fat ...... 0 .05 Goat, meat ...... 0.05 chlorophenoxy)-3,3-dimethyl-1-(1H- Goat, meat byproducts ...... 0 .05 1,2,4-triazol-1-yl)-2-butanone, and Grape ...... 0 .01 triadimenol, b-(4-chlorophenoxy)-a-(1,1- Hog, fat ...... 0 .05 dimethylethyl)-1H-1,2,4-triazole-1-eth- Hog, meat ...... 0 .05 Hog, meat byproducts ...... 0 .05 anol, expressed as triadimefon, in or on Horse, fat ...... 0 .05 the following food commodities: Horse, meat ...... 0 .05 Horse, meat byproducts ...... 0 .05 Milk ...... 0.05 Parts per Expiration/ Commodity million Revocation Nut, macadamia ...... 0.1 Date Onion, bulb ...... 0 .5 Peanut ...... 1 .5 Pineapple ...... 2.0 None Peanut, meal ...... 2 .2 Pecans ...... 0 .05 (b) Section 18 emergency exemptions. Poultry, fat ...... 0.05 [Reserved] Poultry, meat ...... 0 .05 Poultry, meat byproducts ...... 0.05 (c) Tolerances with regional registra- Potato1 ...... 1 .0 tions. [Reserved] Potato, chips1 ...... 2 .0 (d) Indirect or inadvertent residues. Potato, granules/flakes1 ...... 4 .0 Sheep, fat ...... 0 .05 [Reserved] Sheep, meat ...... 0.05 [73 FR 54962, Sept. 24, 2008, as amended at 76 Sheep, meat byproducts ...... 0 .05 Soybean, seed ...... 2 .5 FR 34885, June 15, 2011] Sweet potato, roots ...... 0 .05 § 180.411 Fluazifop-P-butyl; tolerances 1 No U.S. registrations. for residues. (b) Section 18 emergency exemptions. (a) General. Tolerances are estab- [Reserved] lished for residues of the herbicide (c) Tolerances with regional registra- fluazifop-P-butyl, including its me- tions. Tolerances with regional reg- tabolites and degradates, in or on the istrations are established for residues following commodities in the table. of the herbicide fluazifop-P-butyl, in- Compliance with the tolerance levels cluding its metabolites and degradates,

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in or on the following commodities in Commodity Parts per the table. Compliance with the toler- million ance levels specified in the table below Citrus, dried pulp ...... 1 .5 is to be determined by measuring only Clover, forage ...... 35 the sum of fluazifop-P-butyl, butyl(R)- Clover, hay ...... 55 Coriander, leaves ...... 4 .0 2-[4-[[5-(trifluoromethyl)-2- Corn, field, forage ...... 2 .0 pyridinyl]oxy]phenoxy]propanoate, and Corn, field, grain ...... 0 .5 the free and conjugated forms of the re- Corn, field, stover ...... 2 .5 Corn, sweet, forage ...... 3 .0 solved isomer of fluazifop, (R)-2-[4-[[5- Corn, sweet, kernel plus cob with husk removed 0.4 (trifluoromethyl)-2- Corn, sweet, stover ...... 3 .5 pyridinyl]oxy]phenoxy]propanoic acid, Cotton, undelinted seed ...... 5 .0 calculated as the stoichiometric equiv- Cowpea, forage ...... 15 Cowpea, hay ...... 50 alent of fluazifop, in or on the com- Crambe, meal ...... 40 .0 modity. Crambe, seed ...... 35.0 Cranberry ...... 2 .5 Parts per Cuphea, seed ...... 35 .0 Commodity million Dillweed, fresh leaves ...... 10 Echium, seed ...... 35 .0 Asparagus ...... 3.0 Egg ...... 2 .0 Coffee, bean ...... 0 .1 Flax, seed ...... 5 .0 Pepper, tabasco ...... 1 .0 Fruit, citrus, group 10 ...... 0 .5 Rhubarb ...... 0 .5 Fruit, pome, group 11 ...... 0.2 Goat, fat ...... 0 .2 (d) Indirect or inadvertent residues. Goat, meat ...... 0.2 Goat, meat byproducts ...... 1 .0 [Reserved] Gold of pleasure, meal ...... 40.0 [65 FR 33714, May 24, 2000, as amended at 74 Gold of pleasure, seed ...... 35.0 Grape ...... 1 .0 FR 9372, Mar. 4, 2009; 74 FR 46374, Sept. 9, Grape, raisin ...... 2 .0 2009; 74 FR 47457, Sept. 16, 2009; 76 FR 5703, Hare’s ear mustard, seed ...... 35 .0 Feb. 2, 2011; 76 FR 59908, Sept. 28, 2011] Hog, fat ...... 0 .2 Hog, meat ...... 0 .2 § 180.412 Sethoxydim; tolerances for Hog, meat byproducts ...... 1 .0 residues. Horse, fat ...... 0 .2 Horse, meat ...... 0 .2 (a) General. Tolerances are estab- Horse, meat byproducts ...... 1 .0 lished for combined residues of the her- Juneberry ...... 5 .0 Lesquerella, seed ...... 35 .0 bicide 2-[1-(ethoxyimino)butyl]-5-[2- Lingonberry ...... 5.0 (ethylthio)propyl]-3-hydroxy-2-cyclo- Lunaria, seed ...... 35 .0 hexen-1-one (CAS Reg. No. 74051–80–2) Meadowfoam, seed ...... 35 .0 and its metabolites containing the 2- Milk ...... 0.5 Milkweed, seed ...... 35.0 cyclohexen-1-one moiety (calculated as Mustard, seed ...... 35 .0 the herbicide) in or on the following Nectarine ...... 0 .2 commodities: Nut, tree, group 14 ...... 0 .2 Oil radish, seed ...... 35.0 Parts per Okra ...... 2.5 Commodity million Pea and bean, dried shelled, except soybean, subgroup 6C ...... 25 Alfalfa, forage ...... 40 Pea, field, hay ...... 40 Alfalfa, hay ...... 40 Pea, field, vines ...... 20 Almond, hulls ...... 2 .0 Pea, succulent ...... 10 Apricot ...... 0 .2 Peach ...... 0 .2 Apple, wet pomace ...... 0 .8 Peanut ...... 25 Asparagus ...... 4.0 Peppermint, tops ...... 30 Bean, succulent ...... 15 Pistachio ...... 0.2 Beet, sugar, molasses ...... 10 Poppy, seed ...... 35 .0 Beet, sugar, tops ...... 3.0 Potato granules/flakes ...... 8 .0 Blueberry ...... 4 .0 Potato waste, processed ...... 8.0 Borage, meal ...... 10 Poultry, fat ...... 0.2 Borage, seed ...... 6 .0 Poultry, meat ...... 0 .2 Buckwheat, flour ...... 25 Poultry, meat byproducts ...... 2.0 Buckwheat, grain ...... 19 Radish, tops ...... 4 .5 Caneberry subgroup 13 A ...... 5.0 Rapeseed, meal ...... 40 Canola, meal ...... 40 Rapeseed, seed ...... 35 Canola, seed ...... 35 Safflower, seed ...... 15 Cattle, fat ...... 0.2 Salal ...... 5 .0 Cattle, meat ...... 0 .2 Sesame, seed ...... 35 .0 Cattle, meat byproducts ...... 1.0 Sheep, fat ...... 0 .2 Cherry, sweet ...... 0 .2 Sheep, meat ...... 0.2 Cherry, tart ...... 0 .2 Sheep, meat byproducts ...... 1 .0

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Parts per Parts per Commodity million Commodity million

Soybean, hay ...... 10 Fruit, citrus, postharvest ...... 10.0 Soybean, seed ...... 16 Wheat, forage ...... 0 .5 Spearmint, tops ...... 30 Wheat, grain ...... 0 .1 Strawberry ...... 10 Wheat, hay ...... 0 .5 Sunflower, meal ...... 20 Wheat, straw ...... 0 .5 Sunflower, seed ...... 7.0 Sweet rocket, seed ...... 35.0 (2) Tolerances are established for the Turnip, tops ...... 5.0 Vegetable, brassica, leafy, group 5 ...... 5.0 combined residues of the fungicide Vegetable, bulb, group 3 ...... 1 .0 imazalil, 1-[2-(2,4-dichlorophenyl)-2-(2- Vegetable, cucurbit, group 9 ...... 4.0 propenyloxy)ethyl]-1H-imidazole, and Vegetable, fruiting, group 8 ...... 4.0 Vegetable, leafy, except brassica, group 4 ...... 4 .0 its metabolites, 3-[2-(2,4- Vegetable, root and tuber, group 1 ...... 4 .0 dichlorophenyl)-2-(2,3- dihydroxypropoxy)ethyl]-2,4- (b) Section 18 emergency exemptions. imidazolidinedione (FK772) and 3-[2- [Reserved] (2,4-dichlorophenyl)-2-(hydroxy)]-2,4- (c) Tolerances with regional registra- imidazolidinedione (FK284), in or on tion. Tolerances with regional registra- the following food commodities: tion, as defined in § 180.1(l), are established for the combined residues of the Parts per Commodity million herbicide 2-[1-(ethoxyimino)butyl]-5-[2- (ethylthio)propyl]-3-hydroxy-2-cyclo- Cattle, fat ...... 0.01 hexen-1-one) and its metabolites con- Cattle, meat ...... 0 .01 Cattle, meat byproducts ...... 0.2 taining the 2-cyclohexen-1-one moiety Goat, fat ...... 0 .01 (calculated as the herbicide) in or on Goat, meat ...... 0.01 the following commodities: Goat, meat byproducts ...... 0 .2 Horse, fat ...... 0 .01 Horse, meat ...... 0 .01 Expiration/ Commodity Parts per Revocation Horse, meat byproducts ...... 0 .2 million Date Milk ...... 0.02 Sheep, fat ...... 0 .01 Artichoke, globe ...... 5.0 None Sheep, meat ...... 0.01 Rhubarb ...... 0.3 None Sheep, meat byproducts ...... 0 .2

(d) Indirect and inadvertent residues. (b) Section 18 emergency exemptions. [Reserved] [Reserved] (c) Tolerances with regional registra- [62 FR 17740, Apr. 11, 1997] tions. [Reserved] EDITORIAL NOTE: For FEDERAL REGISTER ci- (d) Indirect or inadvertent residues. tations affecting § 180.412, see the List of CFR [Reserved] Sections Affected, which appears in the Finding Aids section of the printed volume [65 FR 33715, May 24, 2000, as amended at 67 and at www.fdsys.gov. FR 46893, July 17, 2002; 71 FR 54434, Sept. 15, 2006] § 180.413 Imazalil; tolerances for residues. § 180.414 Cyromazine; tolerances for (a) General. (1) Tolerances are estab- residues. lished for the combined residues of the (a) General. (1) Tolerances are estab- fungicide imazalil, 1-[2-(2,4- lished for residues of the insecticide dichlorophenyl)-2-(2- cyromazine, including its metabolites propenyloxy)ethyl]-1H-imidazole, and and degradates, in or on the commod- its metabolite, 1-(2,4-dichlorophenyl)-2- ities in the table in this paragraph. (1H-imidazole-1-yl)-1-ethanol, in or on Compliance with the tolerance levels the following food commodities: specified in this paragraph is to be determined by measuring only Parts per cyromazine, N-cyclopropyl-1,3,5-tri- Commodity million azine-2,4,6-triamine, in or on the com- Banana ...... 3.0 modity. Barley, grain ...... 0 .1 Barley, hay ...... 0 .5 Parts per Barley, straw ...... 0 .5 Commodity million Citrus, dried pulp ...... 25 .0 Citrus, oil ...... 200.0 Bean, dry, except cowpea ...... 3 .0

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cyromazine-treated feed must stop at Commodity Parts per million least 3 days (72 hours) before slaughter. Bean, lima ...... 1 .0 If the feed is formulated by any person Bean, succulent ...... 2 .0 other than the end user, the formulator Broccoli ...... 1 .0 must inform the end user, in writing, Cabbage, abyssinian ...... 10 .0 Cabbage, seakale ...... 10.0 of the 3-day (72 hours) pre-slaughter in- Cattle, fat ...... 0.05 terval. Compliance with the tolerance Cattle, kidney ...... 0 .2 level specified in this paragraph is to Cattle, meat ...... 0 .05 Cattle, meat byproducts, except kidney ...... 0.05 be determined by measuring only Egg ...... 0 .25 cyromazine, N-cyclopropyl-1,3,5-tri- Garlic ...... 0 .2 azine-2,4,6-triamine, in or on the com- Garlic, great-headed, bulb ...... 0 .2 modity. Goat, fat ...... 0 .05 Goat, kidney ...... 0 .2 (b) Section 18 emergency exemptions. Goat, meat ...... 0.05 [Reserved] Goat, meat byproducts, except kidney ...... 0 .05 (c) Tolerances with regional registra- Hanover salad, leaves ...... 10 .0 Hog, fat ...... 0 .05 tions. [Reserved] Hog, kidney ...... 0.2 (d) Indirect or inadvertent residues. Hog, meat ...... 0 .05 Tolerances are established for indirect Hog, meat byproducts, except kidney ...... 0 .05 Horse, fat ...... 0 .05 or inadvertent residues of the insecti- Horse, kidney ...... 0 .2 cide cyromazine, including its metabo- Horse, meat ...... 0 .05 lites and degradates, in or on the com- Horse, meat byproducts, except kidney ...... 0 .05 modities in the table in this paragraph Leek ...... 3 .0 Mango 1 ...... 0.3 when present therein as a result of the Milk ...... 0.05 application of cyromazine to growing Mushroom ...... 1 .0 crops listed in paragraph (a)(1) of this Onion, bulb ...... 0 .2 Onion, green ...... 3 .0 section. Compliance with the tolerance Onion, potato ...... 3 .0 levels specified in this paragraph is to Onion, tree ...... 3.0 be determined by measuring only Onion, welsh ...... 3.0 Pepper ...... 1 .0 cyromazine, N-cyclopropyl-1,3,5-tri- Potato ...... 0 .8 azine-2,4,6-triamine, in or on the com- Poultry, fat (from chicken layer hens and chick- modity. en breeder hens only) ...... 0 .05 Poultry, meat (from chicken layer hens and Parts per chicken breeder hens only) ...... 0 .05 Commodity million Poultry, meat byproducts (from chicken layer hens and chicken breeder hens only) ...... 0 .05 Cotton, undelinted seed ...... 0 .1 Rakkyo, bulb ...... 0.2 Corn, sweet, kernel plus cob with husks re- Shallot, bulb ...... 0 .2 moved ...... 0 .5 Shallot, fresh leaves ...... 3 .0 Corn, sweet, forage ...... 0 .5 Sheep, fat ...... 0 .05 Corn, sweet, stover ...... 0 .5 Sheep, kidney ...... 0.2 Radish, roots ...... 0 .5 Sheep, meat ...... 0.05 Radish, tops ...... 0 .5 Sheep, meat byproducts, except kidney ...... 0 .05 Tomato ...... 0.5 Turnip, greens ...... 10.0 [65 FR 25860, May 4, 2000, as amended at 67 Vegetable, brassica, leafy, group 5, except broc- FR 72593, Dec. 6, 2002; 68 FR 55269, Sept. 24, coli ...... 10 .0 2003; 75 FR 22256, Apr. 28, 2010; 76 FR 23494, Vegetable, leafy, except brassica, group 4 ...... 7 .0 Apr. 27, 2011] Vegetable, cucurbit, group 9 ...... 1.0 1There are no U.S. registrations on mango as of May 4, § 180.415 Aluminum tris (O- 2000. ethylphosphonate); tolerances for (2) A tolerance of 5.0 parts per mil- residues. lion is established for residues of the (a) General. Tolerances are estab- insecticide cyromazine, including its lished for residues of the fungicide alu- metabolites and degradates, in or on minum tris (O-ethylphosphonate), in- poultry feed when used as a feed addi- cluding its metabolites and degradates, tive only in feed for chicken layer hens in or on the commodities in the table and chicken breeder hens at the rate of in this paragraph. Compliance with the not more than 0.01 pound of tolerance levels specified in this para- cyromazine per ton of poultry feed for graph is to be determined by measuring control of flies in manure of treated only aluminum tris (O- chicken layer hens and chicken breeder ethylphosphonate), in or on the com- hens, provided the feeding of modity.

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by measuring only the residues of Commodity Parts per million ethalfluralin, N-ethyl-N-(2-methyl-2- Avocado ...... 25 propenyl)-2,6-dinitro-4- Banana ...... 3.0 (trifluoromethyl)benzenamine. Bushberry subgroup 13B ...... 40 Caneberry subgroup 13A ...... 0 .1 Parts per Cranberry ...... 0 .5 Commodity million Fruit, citrus, group 10 ...... 5 .0 Fruit, pome, group 11 ...... 10 Bean, dry, seed ...... 0 .05 Ginseng ...... 0 .1 Dill, dried leaves ...... 0 .05 Hop, dried cones ...... 45 Dill, fresh leaves ...... 0 .05 Juneberry ...... 40 Peanut ...... 0 .05 Lingonberry ...... 40 Pea, dry, seed ...... 0 .05 Nut, macadamia ...... 0.20 Potato ...... 0 .05 Onion, bulb ...... 0 .5 Rapeseed subgroup 20A ...... 0 .05 Onion, green ...... 10.0 Soybean ...... 0.05 Pea, succulent ...... 0 .3 Sunflower subgroup 20B ...... 0.05 Pineapple ...... 0.1 Vegetable, cucurbit, group 9 ...... 0.05 Salal ...... 40 Strawberry ...... 75 (b) Section 18 emergency exemptions. Tomato ...... 3 Turnip, greens ...... 40 [Reserved] Turnip, roots ...... 15 (c) Tolerances with regional registra- Vegetable, brassica, leafy, group 5 ...... 60 tions. [Reserved] Vegetable, cucurbit, group 9 ...... 15 (d) Indirect or inadvertent residues. Vegetable, leafy, except brassica, group 4 ...... 100 [Reserved] (b) Section 18 emergency exemptions. [49 FR 391, Jan. 4, 1984, as amended at 50 FR [Reserved] 4976, Feb. 5, 1985; 52 FR 11262, Apr. 8, 1987; 62 (c) Tolerances with regional registra- FR 66014, Dec. 17, 1997; 64 FR 5191, Feb. 3, tions. Tolerances with regional reg- 1999; 64 FR 54782, Oct. 8, 1999; 66 FR 37598, istration, as defined in § 180.1(l), are es- July 19, 2001; 66 FR 41454, Aug. 8, 2001; 67 FR 2342, Jan. 17, 2002; 67 FR 49617, July 31, 2002; tablished for residues of the fungicide 72 FR 68534, Dec. 5, 2007; 78 FR 40020, July 3, aluminum tris (O-ethylphosphonate), 2013] including its metabolites and degradates, in or on the commodities § 180.417 Triclopyr; tolerances for resi- in the table in this paragraph. Compli- dues. ance with the tolerance levels specified (a) General. (1) Tolerances for resi- in this paragraph is to be determined dues of the herbicide triclopyr per se, by measuring only aluminum tris (O- as a result of the application/use of ethylphosphonate), in or on the com- butoxyethyl ester of triclopyr and modity. triethyylamine salt of triclopyr, are established in or on the following raw ag- Parts per Commodity million ricultural commodities:

Asparagus ...... 0.1 Commodity Parts per Grape ...... 10 million

Egg ...... 0 .05 (d) Indirect or inadvertent residues. Fish ...... 3 .0 [Reserved] Grass, forage ...... 700.0 Grass, hay ...... 200.0 [64 FR 36801, July 8, 1999, as amended at 64 Milk ...... 0.01 FR 37875, July 14, 1999; 65 FR 50438, Aug. 18, Poultry, fat ...... 0.1 2000; 67 FR 55346, Aug. 29, 2002; 68 FR 11335, Poultry, meat ...... 0 .1 Mar. 10, 2003; 70 FR 7047, Feb. 10, 2005; 76 FR Poultry, meat byproducts, except kidney ...... 0.1 23494, Apr. 27, 2011] Rice, grain ...... 0 .3 Rice, straw ...... 10 .0 Shellfish ...... 3 .5 § 180.416 Ethalfluralin; tolerances for residues. (2) Tolerances for the combined resi- (a) General. Tolerances are estab- dues of the herbicide triclopyr ((3,5,6- lished for residues of the herbicide trichloro-2-pyridinyl)oxy) acetic acid ethalfluralin, including its metabolites and its metabolite 3,5,6-trichloro-2- and degradates, in or on the commod- pyridinol (TCP), as a result of the ap- ities in the following table. Compliance plication/use of butoxyethyl ester of with the tolerance levels specified in triclopyr or the triethylamine salt of the following table is to be determined triclopyr, are established in or on the

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following raw agricultural commod- Commodity Parts per ities: million Hog, fat ...... 0 .1 Parts per Commodity million Hog, meat ...... 0 .05 Horse, fat ...... 1 .0 Cattle, fat ...... 0.05 Horse, meat ...... 0 .2 Cattle, kidney ...... 0 .5 Horse, meat byproducts ...... 0 .05 Cattle, liver ...... 0 .5 Lettuce, head ...... 4.0 Cattle, meat ...... 0 .05 Milk, fat (reflecting 0.10 in whole milk) ...... 2 .5 Cattle, meat byproducts, except kidney and liver 0.05 Onion, bulb ...... 0 .1 Goat, fat ...... 0 .05 Onion, green ...... 6 .0 Goat, kidney ...... 0 .5 Pecan ...... 0 .05 Goat, liver ...... 0.5 Poultry, fat ...... 0.05 Goat, meat ...... 0.05 Poultry, meat ...... 0 .05 Goat, meat byproducts, except kidney and liver 0 .05 Sheep, fat ...... 1 .0 Hog, fat ...... 0 .05 Sheep, meat ...... 0.2 Hog, kidney ...... 0.5 Sheep, meat byproducts ...... 0 .05 Hog, liver ...... 0 .5 Hog, meat ...... 0 .05 (2) Tolerances are established for res- Hog, meat byproducts, except kidney and liver .. 0 .05 idues of zeta-cypermethrin, (S-cyano(3- Horse, fat ...... 0 .05 Horse, kidney ...... 0 .5 phenoxyphenyl) methyl (±))(cis-trans 3- Horse, liver ...... 0 .5 (2,2-dichloroethenyl)-2,2 Horse, meat ...... 0 .05 dimethylcyclopropanecarboxylate), in- Horse, meat byproducts, except kidney and liver 0 .05 Sheep, fat ...... 0 .05 cluding its metabolites and degradates, Sheep, kidney ...... 0.5 in or on the commodities in the fol- Sheep, liver ...... 0.5 lowing table. Compliance with the tol- Sheep, meat ...... 0.05 Sheep, meat byproducts, except kidney and erance levels specified in the following liver ...... 0 .05 table is to be determined by measuring only total cypermethrin, cyano(3- (b) Section 18 emergency exemptions. phenoxyphenyl)methyl 3-(2,2- [Reserved] dichloroethenyl)-2,2- (c) Tolerances with regional registra- dimethylcyclopropane carboxylate, in tions. [Reserved] or on the commodity. (d) Indirect or inadvertent residues. Parts per [Reserved] Commodity million [50 FR 18486, May 1, 1985, as amended at 55 Alfalfa, hay ...... 15.00 FR 26440, June 28, 1990; 60 FR 4095, Jan. 20, Alfalfa, forage ...... 5.00 1995; 62 FR 46894, Sept. 5, 1997; 63 FR 45406, Alfalfa, seed ...... 0 .50 Aug. 26, 1998; 67 FR 35048, May 17, 2002; 67 FR Almond, hulls ...... 6 58725, Sept. 18, 2002; 72 FR 41931, Aug. 1, 2007] Animal feed, nongrass, group 18, forage ...... 8 Animal feed, nongrass, group 18, hay ...... 40 § 180.418 Cypermethrin and an isomer Artichoke, globe ...... 0.60 Avocado ...... 0 .50 zeta-cypermethrin; tolerances for Barley, grain ...... 3 .0 residues. Barley, hay ...... 6 .0 (a) General. (1) Tolerances are estab- Barley, straw ...... 20 .0 Beet, sugar, roots ...... 0 .05 lished for residues of the insecticide Beet, sugar, tops ...... 0.20 cypermethrin (±)alpha cyano-(3- Berry group 13 ...... 0 .8 phenoxyphenyl)methyl(±)cis,trans- Borage, seed ...... 0 .2 Brassica, head and stem, subgroup 5A ...... 2 .00 3(2,2-dichloroethenyl-2,2- Brassica, leafy greens, subgroup 5B ...... 14 .00 dimethylcyclopropanecarboxylate in or Buckwheat, grain ...... 3.0 on the following commodities: Buckwheat, hay ...... 6 .0 Buckwheat, straw ...... 20 .0 Parts per Cabbage ...... 2 .00 Commodity million Canistel ...... 0 .50 Castor oil plant, refined oil ...... 0.4 Brassica, head and stem, subgroup 5A ...... 2 .0 Castor oil plant, seed ...... 0 .2 Brassica, leafy greens, subgroup 5B ...... 14 .0 Cattle, fat ...... 1.00 Cattle, fat ...... 1.0 Cattle, meat ...... 0 .2 Cattle, meat ...... 0 .2 Cattle, meat byproducts ...... 0.05 Cattle, meat byproducts ...... 0.05 Chinese tallowtree, refined oil ...... 0 .4 Cotton, gin byproducts ...... 11 .0 Chinese tallowtree, seed ...... 0 .2 Cotton, undelinted seed ...... 0 .5 Cilantro, leaves ...... 10 Egg ...... 0 .05 Citrus, dried pulp ...... 1 .8 Goat, fat ...... 1 .0 Citrus, oil ...... 4.0 Goat, meat ...... 0.2 Corn, field, forage ...... 0 .20 Goat, meat byproducts ...... 0 .05 Corn, field, grain ...... 0 .05

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Parts per Parts per Commodity million Commodity million

Corn, field, stover ...... 3 .00 Rose hip, refined oil ...... 0.4 Corn, pop, grain ...... 0.05 Rose hip, seed ...... 0.2 Corn, pop, stover ...... 3.00 Rye, grain ...... 3.0 Corn, sweet, forage ...... 15 .00 Rye, hay ...... 6 .0 Corn, sweet, kernel plus cob with husks re- Rye, straw ...... 20 .0 moved ...... 0 .05 Safflower, seed ...... 0 .2 Corn, sweet, stover ...... 15.00 Sapodilla ...... 0 .50 Cotton, undelinted seed ...... 0 .5 Sapote, black ...... 0 .50 Crambe, seed ...... 0.2 Sapote, mamey ...... 0 .50 Cuphea, seed ...... 0 .2 Sesame, seed ...... 0 .2 Echium, seed ...... 0 .2 Sheep, fat ...... 1 .00 Egg ...... 0 .05 Sheep, meat ...... 0.2 Euphorbia, refined oil ...... 0 .4 Sheep, meat byproducts ...... 0 .05 Euphorbia, seed ...... 0 .2 Sorghum, grain, forage ...... 0.1 Evening primrose, refined oil ...... 0 .4 Sorghum, grain, grain ...... 0 .5 Evening primrose, seed ...... 0 .2 Sorghum, grain, stover ...... 5 .0 Flax, seed ...... 0 .2 Soybean, seed ...... 0 .05 Food commodities/feed commodities (other than Star apple ...... 0 .50 those covered by a higher tolerance as a re- Stokes aster, refined oil ...... 0 .4 sult of use on growing crops) in food/feed Stokes aster, seed ...... 0 .2 handling establishments ...... 0 .05 Sugarcane, cane ...... 0.60 Fruit, citrus, group 10 ...... 0 .35 Sunflower, refined oil ...... 0.5 Fruit, pome, group 11 ...... 2 Sunflower, seed ...... 0.2 Fruit, stone, group 12 ...... 1 Sweet rocket, seed ...... 0 .2 Goat, fat ...... 1 .00 Tallowwood, refined oil ...... 0.4 Goat, meat ...... 0.2 Tallowwood, seed ...... 0 .2 Goat, meat byproducts ...... 0 .05 Tea oil plant, refined oil ...... 0 .4 Gold of pleasure, seed ...... 0 .2 Tea oil plant, seed ...... 0 .2 Grain, aspirated fractions ...... 10.0 Turnip, greens ...... 14 Grape ...... 2 Vegetable, cucurbit, group 9 ...... 0.2 Grass, forage, fodder, and hay, group 17, for- Vegetable, fruiting, group 8 ...... 0.2 age ...... 10 Vegetable, leafy, except brassica, group 4 ...... 10.00 Grass, forage, fodder and hay, group 17, hay .... 35 Vegetable, legume, edible podded, subgroup 6A 0 .5 Hare’s-ear mustard, seed ...... 0 .2 Vegetable, root and tuber, group 1, except Hog, fat ...... 0 .1 sugar beet ...... 0 .1 Hog, meat ...... 0 .05 Vernonia, refined oil ...... 0 .4 Horse, fat ...... 1 .00 Vernonia, seed ...... 0 .2 Horse, meat ...... 0 .2 Wheat, forage ...... 3 .0 Horse, meat byproducts ...... 0 .05 Wheat, grain ...... 0 .2 Jojoba, refined oil ...... 0.4 Wheat, hay ...... 6 .0 Wheat, straw ...... 7 .0 Jojoba, seed ...... 0.2 Lesquerella, seed ...... 0 .2 Lunaria, seed ...... 0 .2 (3) Tolerances are established for res- Mango ...... 0.70 idues of the insecticide, alpha- Meadowfoam, seed ...... 0 .2 Milk, fat (reflecting 0.10 in whole milk) ...... 2 .50 cypermethrin, (R)-cyano(3- Milkweed, seed ...... 0 .2 phenoxyphenyl)methyl (1S,3S)-rel-3- Mustard, seed ...... 0 .2 (2,2-dichloroethenyl)-2,2- Niger seed, refined oil ...... 0 .4 dimethylcyclopropane carboxylate, in- Niger seed, seed ...... 0 .2 Nut, tree, group 14 ...... 0 .05 cluding its metabolites and degradates, Oat, grain ...... 3 .0 in or on the commodities in the table Oat, hay ...... 6.0 below. Compliance with the tolerance Oat, straw ...... 20.0 Oil radish, seed ...... 0.2 levels specified below is to be deter- Okra ...... 0.2 mined by measuring only total Onion, bulb ...... 0 .10 cypermethrin, cyano(3- Onion, green ...... 3 .00 phenoxyphenyl)methyl 3-(2,2- Papaya ...... 0 .50 Pea and bean, dried shelled, except soybean, dichloroethenyl)-2,2- subgroup 6C ...... 0 .05 dimethylcyclopropane carboxylate, in Pea and bean, succulent shelled, subgroup 6B 0 .1 or on the commodity. Peanut ...... 0 .05 Pecan ...... 0 .05 Parts per Pistachio ...... 0.05 Commodity million Poppy, seed ...... 0 .2 Poultry, fat ...... 0.05 Alfalfa, hay ...... 15 Poultry, meat ...... 0 .05 Beet, sugar, roots ...... 0 .05 Rapeseed ...... 0 .2 Beet, sugar, tops ...... 0.20 Rice, grain ...... 1 .50 Brassica, head and stem, subgroup 5A ...... 2 .0 Rice, hulls ...... 6 .00 Cattle, fat ...... 1.0 Rice, straw ...... 2 .00 Cattle, meat ...... 0 .20 Rice, wild, grain ...... 1.5 Cattle, meat byproducts ...... 0.05

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Parts per Parts per Commodity million Commodity million

Citrus, dried pulp ...... 1 .8 Cattle, fat ...... 0.5 Citrus, oil ...... 4.0 Cattle, meat ...... 0 .5 Corn, field, grain ...... 0 .05 Cattle, meat byproducts ...... 0.5 Corn, pop, grain ...... 0.05 Egg ...... 0 .1 Corn, sweet, kernel plus cob with husks re- Goat, fat ...... 0 .5 moved ...... 0 .05 Goat, meat ...... 0.5 Cotton, undelinted seed ...... 0 .50 Goat, meat byproducts ...... 0 .5 Egg ...... 0 .05 Hog, fat ...... 0 .5 Fruit, citrus, group 10–10 ...... 10 Hog, meat ...... 0 .5 Goat, fat ...... 1 .0 Hog, meat byproducts ...... 0 .5 Goat, meat ...... 0.20 Horse, fat ...... 0 .5 Goat, meat byproducts ...... 0 .05 Horse, meat ...... 0 .5 Hog, fat ...... 1 .0 Horse, meat byproducts ...... 0 .5 Hog, meat ...... 0 .05 Milk, fat (0.05 ppm (N) in whole milk ...... 1 .25 Horse, fat ...... 1 .0 Oat, grain ...... 6 .0 Horse, meat ...... 0 .20 Poultry, fat ...... 0.5 Horse, meat byproducts ...... 0 .05 Poultry, meat ...... 5 Milk, fat, reflecting 0.10 ppm in whole milk ...... 2 .5 Poultry, meat byproducts ...... 5 Nut, tree, group 14–12 ...... 0 .05 Rice, grain ...... 6 .0 Pea and bean, dried shelled, except soybean, Sheep, fat ...... 0 .5 subgroup 6C ...... 0 .05 Sheep, meat ...... 0.5 Pea and bean, succulent shelled, subgroup 6B 0 .10 Sheep, meat byproducts ...... 0 .5 Poultry, fat ...... 0.05 Sorghum, grain ...... 6 .0 Poultry, meat ...... 0 .05 Wheat, grain ...... 6 .0 Rice, grain ...... 1 .5 Sheep, fat ...... 1 .0 Sheep, meat ...... 0.20 (2) Tolerances are established for the Sheep, meat byproducts ...... 0 .05 combined residues of the insecticide Sorghum, grain, grain ...... 0 .50 chlorpyrifos-methyl (O,-O- dimethyl-O- Soybean, seed ...... 0 .05 Vegetable, cucurbit, group 9 ...... 0.20 (3,5,6-trichloro-2-pyridyl) Vegetable, fruiting, group 8–10 ...... 0 .20 phosphorothioate and its metabolite Vegetable, leafy, group 4 ...... 10 (3,5,6-trichloro-2-pyridinol) in or on the Vegetable, legume, edible podded, subgroup 6A 0 .50 Vegetable, root and tuber, group 1, except following food commodities when sugar beet ...... 0 .10 present therein as a result of applica- Wheat, grain ...... 0 .20 tion to stored grains:

(b) Section 18 emergency exemptions. Commodity Parts per [Reserved] million (c) Tolerances with regional registra- Barley, bran ...... 90 tions. [Reserved] Barley, pearled barley ...... 90 (d) Indirect or inadvertent residues. Rice, bran ...... 30 Rice, hulls ...... 30 [Reserved] Rice, polished rice ...... 30 Sorghum, grain, bran ...... 90 [62 FR 63235, 63243, Nov. 26, 1997, as amended Wheat, bran ...... 30 at 63 FR 48586, Sept. 11, 1998; 66 FR 47993, Wheat, germ ...... 30 Sept. 17, 2001; 67 FR 6430, Feb. 12, 2002; 67 FR Wheat, middlings ...... 30 56495, Sept. 4, 2002; 69 FR 71717, Dec. 10, 2004; Wheat, shorts ...... 30 71 FR 78382, Dec. 29, 2006; 72 FR 53462, Sept. 19, 2007; 72 FR 71801, Dec. 19, 2007; 73 FR 1525, (b) Section 18 emergency exemptions. Jan. 9, 2008; 77 FR 72984, Dec. 7, 2012; 78 FR [Reserved] 7275, Feb. 1, 2013] (c) Tolerances with regional registrations. [Reserved] § 180.419 Chlorpyrifos-methyl; tolerances for residues. (d) Indirect or inadvertent residues. [Reserved] (a) General. (1) Tolerances are established for the combined residues of the [65 FR 33715, May 24, 2000, as amended at 74 insecticide chlorpyrifos-methyl [O,-O,- FR 46374, Sept. 9, 2009] dimethyl O-(3,5,6-trichloro-2-pyridyl)] § 180.420 Fluridone; tolerances for res- phosphorothioate and its metabolite idues. (3,5,6-trichloro-2-pyridinol) in or on the following food commodities: (a) General. (1) Tolerances are established for residues of the herbicide Commodity Parts per fluridone, including its metabolites million and degradates, in or on the commod- Barley, grain ...... 6 .0 ities in the table in this paragraph.

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Compliance with the tolerance levels pyridinone, including its metabolites specified in this paragraph is to be de- and degradates in or on the specified termined by measuring only the sum of agricultural commodities, resulting fluridone, 1-methyl-3-phenyl-5-(3- from use of the pesticide pursuant to (trifluoromethyl)phenyl)-4(1H)- the Federal Insecticide, Fungicide, and pyridinone, and its bound residues, cal- Rodenticide Act (FIFRA) section 18 culated as the stoichiometric equiva- emergency exemptions. Compliance lent of fluridone, in or on the com- with the tolerance levels specified modity. below is to be determined by measuring only fluridone. The tolerances expire Parts per on the date specified in the table. Commodity million

Crayfish ...... 0.5 Parts per Expiration Commodity million date Fish ...... 0 .5 Cotton, undelinted seed ...... 0.1 12/31/14 (2) Tolerances are established for residues of the herbicide fluridone, includ- (c) Tolerances with regional registra- ing its metabolites and degradates, in tions. [Reserved] or on the commodities in the table in (d) Indirect or inadvertent residues. this paragraph. Compliance with the Tolerances are established for indirect tolerance levels specified in this para- or inadvertent residues of the herbicide graph is to be determined by measuring fluridone, including its metabolites only fluridone, 1-methyl-3-phenyl-5-(3- and degradates, in or on the irrigated (trifluoromethyl)phenyl)-4(1H)- crop commodities and crop groupings pyridinone, in or on the commodity. in the table in this paragraph, resulting from use of irrigation water con- Parts per Commodity million taining residues of 0.15 parts per million following applications of fluridone Cattle, fat ...... 0.05 on or around aquatic sites. Where tol- Cattle, kidney ...... 0 .1 Cattle, liver ...... 0 .1 erances are established at higher levels Cattle, meat ...... 0 .05 from other uses of fluridone on the Cattle, meat byproducts ...... 0.05 crops in the table in this paragraph, Egg ...... 0 .05 Goat, fat ...... 0 .05 the higher tolerance also applies to res- Goat, kidney ...... 0 .1 idues in or on the irrigated commodity. Goat, liver ...... 0.1 Compliance with the tolerance levels Goat, meat ...... 0.05 specified in this paragraph is to be de- Goat, meat byproducts ...... 0 .05 Hog, fat ...... 0 .05 termined by measuring only fluridone, Hog, kidney ...... 0.1 1-methyl-3-phenyl-5-(3- Hog, liver ...... 0 .1 (trifluoromethyl)phenyl)-4(1H)- Hog, meat ...... 0 .05 Hog, meat byproducts ...... 0 .05 pyridinone, in or on the commodity. Horse, fat ...... 0 .05 Horse, kidney ...... 0 .1 Commodity Parts per Horse, liver ...... 0 .1 million Horse, meat ...... 0 .05 Animal feed, nongrass, group 18 ...... 0 .15 Horse, meat byproducts ...... 0 .05 Avocado ...... 0 .1 Milk ...... 0.05 Berry, group 13 ...... 0 .1 Poultry, fat ...... 0.05 Cotton, undelinted seed ...... 0 .1 Poultry, kidney ...... 0 .01 Cranberry ...... 0 .1 Poultry, liver ...... 0 .01 Fruit, citrus, group 10 ...... 0 .1 Poultry, meat ...... 0 .05 Fruit, pome, group 11 ...... 0.1 Poultry, meat byproducts ...... 0.05 Fruit, stone, group 12 ...... 0 .1 Sheep, fat ...... 0 .05 Grain, cereal, forage, fodder and straw, group Sheep, kidney ...... 0.1 16 ...... 0 .1 Sheep, liver ...... 0.1 Grain, cereal, group 15 ...... 0.1 Sheep, meat ...... 0.05 Grape ...... 0 .1 Sheep, meat byproducts ...... 0 .05 Grass, forage ...... 0 .15 Hop, dried cones ...... 0 .1 (b) Section 18 emergency exemptions. Nut, tree, group 14 ...... 0 .1 Okra ...... 0.1 Time-limited tolerances specified in Strawberry ...... 0 .1 the following table are established for Vegetable, brassica, leafy, group 5 ...... 0.1 residues of the herbicide fluridone, 1- Vegetable, cucurbit, group 9 ...... 0.1 Vegetable, fruiting, group 8 ...... 0.1 methyl-3-phenyl-5-(3- Vegetable, leafy, except brassica, group 4 ...... 0 .1 (trifluoromethyl)phenyl)-4(1H)- Vegetable, leaves of root and tuber, group 2 ..... 0 .1

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(d) Indirect or inadvertent residues. Commodity Parts per million [Reserved] Vegetable, legume, group 6 ...... 0 .1 [51 FR 39662, Oct. 30, 1986, as amended at 53 Vegetable, root and tuber, group 1 ...... 0 .1 FR 27349, July 20, 1988; 53 FR 44403, Nov. 3, 1988; 54 FR 45734, Oct. 31, 1989; 60 FR 33354, [76 FR 23495, Apr. 27, 2011, as amended at 77 June 28, 1995; 62 FR 49937, Sept. 24, 1997; 62 FR FR 66720, Nov. 7, 2012] 61447, Nov. 18, 1997; 67 FR 35048, May 17, 2002; 67 FR 41807, June 19, 2002; 69 FR 6567, Feb. 11, 2004; 71 FR 32846, June 7, 2006; 71 FR 54434, § 180.421 Fenarimol; tolerances for res- Sept. 15, 2006; 74 FR 68173, Dec. 23, 2009; 75 FR idues. 56897, Sept. 17, 2010] (a) General. Tolerances are established for residues of fenarimol, includ- § 180.422 Tralomethrin; tolerances for residues. ing its metabolites and degradates, in or on the commodities in the following (a) General. (1) Tolerances are estab- table. Compliance with the tolerance lished for residues of the insecticide levels specified in the following table is tralomethrin, including its metabolites to be determined by measuring only and degradates, in or on the commodities in the table in this paragraph. fenarimol alpha-(2 chlorophenyl)- Compliance with the tolerance levels alpha-(4-chlorophenyl)-5- specified in this paragraph is to be de- pyrimidinemethanol. termined by measuring only the sum of Parts per tralomethrin, (S)-cyano(3- Commodity million phenoxyphenyl)methyl (1R,3S)-2,2-dimethyl-3-(1,2,2,2- Apple ...... 0.3 tetrabromoethyl) Apple, wet pomace ...... 0 .3 Banana ...... 0.25 cyclopropanecarboxylate, and its me- Cattle, fat ...... 0.01 tabolites (S)-cyano(3- Cattle, kidney ...... 0 .01 phenoxyphenyl)methyl (1R,3R)-3-(2,2- Cattle, meat ...... 0 .01 dibromoethenyl)-2,2- Cattle, meat byproducts, except kidney ...... 0.05 dimethylcyclopropanecarboxylate and Cherry, sweet ...... 1 .0 (S)-cyano(3-phenoxyphenyl)methyl Cherry, tart ...... 1 .0 (1S,3R)-3-(2,2-dibromoethenyl)-2,2- Goat, fat ...... 0 .01 Goat, kidney ...... 0 .01 dimethylcyclopropanecarboxylate, cal- Goat, meat ...... 0.01 culated as the stoichiometric equiva- Goat, meat byproducts, except kidney ...... 0 .05 lent of tralomethrin, in or on the com- Grape ...... 0 .1. modity. Hazelnut ...... 0 .02 Hop, dried cones ...... 5 .0 Parts per Expiration/ Horse, fat ...... 0 .01 Commodity revocation million date Horse, kidney ...... 0 .01 Horse, meat ...... 0 .01 Broccoli ...... 0.5 7/9/13 Horse, meat byproducts, except kidney ...... 0 .05 Cotton, undelinted seed ...... 0.02 7/9/13 Pear ...... 0 .1 Cotton, oil ...... 0.20 7/9/13 Pecan ...... 0 .02 Lettuce, head ...... 1.00 7/9/13 Sheep, fat ...... 0 .01 Lettuce, leaf ...... 3.00 7/9/13 Soybean, seed ...... 0.05 7/9/13 Sheep, kidney ...... 0.01 Sunflower, seed ...... 0.05 7/9/13 Sheep, meat ...... 0.01 Sheep, meat byproducts, except kidney ...... 0 .05 (2) A tolerance of 0.02 part per mil- Vegetable, cucurbit, group 9* ...... 0 .20 lion with an expiration/revocation date *There are no U.S. registrations as of August 27, 2010. of July 9, 2013 is established for resi- (b) Section 18 emergency exemptions. dues of the insecticide tralomethrin, [Reserved] including its metabolites and (c) Tolerances with regional registra- degradates, in or on food commodities tions. [Reserved] (other than those covered by a higher tolerance as a result of use on growing crops) in food-handling establishments. Compliance with the tolerance level specified in this paragraph is to be determined by measuring only the sum of tralomethrin, (S)-cyano(3-

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phenoxyphenyl)methyl (1R,3S)-2,2-di- tralomethrin, (S)-cyano(3- methyl-3-(1,2,2,2- phenoxyphenyl)methyl (1R,3S)-2,2-di- tetrabromoethyl) methyl-3-(1,2,2,2- cyclopropanecarboxylate, and its me- tetrabromoethyl) tabolites (S)-cyano(3- cyclopropanecarboxylate, and its me- phenoxyphenyl)methyl (1R,3R)-3-(2,2- tabolites (S)-cyano(3- dibromoethenyl)-2,2- phenoxyphenyl)methyl (1R,3R)-3-(2,2- dimethylcyclopropanecarboxylate and dibromoethenyl)-2,2- (S)-cyano(3-phenoxyphenyl)methyl dimethylcyclopropanecarboxylate and (1S,3R)-3-(2,2-dibromoethenyl)-2,2- (S)-cyano(3-phenoxyphenyl)methyl dimethylcyclopropanecarboxylate, cal- (1S,3R)-3-(2,2-dibromoethenyl)-2,2- culated as the stoichiometric equiva- dimethylcyclopropanecarboxylate, cal- lent of tralomethrin, in or on the com- culated as the stoichiometric equiva- modity. lent of tralomethrin, in or on the com- (i) The insecticide may be present as modity. a residue from application of (i) The insecticide may be present as tralomethrin in food-handling estab- a residue from application of lishments, including food service, man- tralomethrin in feed-handling estab- ufacturing, and processing establish- lishments, including feed manufac- ments, such as restaurants, cafeterias, turing and processing establishments. supermarkets, bakeries, breweries, (ii) The application shall be made in dairies, meat slaughtering and packing accordance with the following pre- plants, and canneries. scribed conditions: Application shall be (ii) The application shall be made in limited to a general surface and spot accordance with the following pre- and/or crack and crevice treatment in scribed conditions: Application shall be feed-handling establishments where limited to a general surface and spot feed and feed products are held or proc- and/or crack and crevice treatment in essed. General surface application may food-handling establishments where be used only when the facility is not in food and food products are held, proc- operation provided exposed feed has essed, prepared, and served. General been covered or removed from the area surface application may be used only being treated. All feed-contact surfaces when the facility is not in operation and equipment must be thoroughly provided exposed food has been covered cleaned after general surface applica- or removed from the area being treat- tions. Spot and/or crack and crevice ap- ed. All food-contact surfaces and equip- plication may be used while the facil- ment must be thoroughly cleaned after ity is in operation provided exposed general surface applications. Spot and/ feed is covered or removed from the or crack and crevice application may area being treated prior to application. be used while the facility is in oper- Spray concentration shall be limited to ation provided exposed food is covered a maximum of 0.06 percent active in- or removed from the area being treated gredient. Contamination of feed and prior to application. Spray concentra- feed-contact surfaces shall be avoided. tion shall be limited to a maximum of (b) Section 18 emergency exemptions. 0.06 percent active ingredient. Con- [Reserved] tamination of food and food-contact (c) Tolerances with regional registra- surfaces shall be avoided. tions. [Reserved] (3) A tolerance of 0.02 part per mil- (d) Indirect or inadvertent residues. lion with an expiration/revocation date [Reserved] of July 9, 2013 is established for resi- [62 FR 63001, Nov. 26, 1997, as amended at 62 dues of the insecticide tralomethrin, FR 66025, Dec. 17, 1997; 65 FR 33701, May 24, including its metabolites and 2000; 71 FR 74817, Dec. 13, 2006; 77 FR 59127, degradates, in or on feed commodities Sept. 26, 2012] (other than those covered by a higher tolerance as a result of use on growing § 180.425 Clomazone; tolerances for crops) in feed-handling establishments. residues. Compliance with the tolerance level (a) General. Tolerances are estab- specified in this paragraph is to be de- lished for residues of the herbicide termined by measuring only the sum of clomazone, including its metabolites

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and degradates, in or on the commod- § 180.427 Tau-Fluvalinate; tolerances ities in the table in this paragraph. for residues. Compliance with the tolerance levels (a) General. Tolerances are estab- specified in this paragraph is to be de- lished for residues of the insecticide termined by measuring only tau-fluvalinate, cyano-(3- clomazone, 2-[(2-chlorophenyl)methyl]- phenoxyphenyl)methyl N-[2-chloro-4- 4,4-dimethyl-3-isoxazolidinone, in or on (trifluoromethyl)phenyl]-D-valinate, in the commodity. or on the following food commodities: Parts per Commodity million Parts per Commodity million Bean, snap, succulent ...... 0 .05 Honey ...... 0.02 Brassica, head and stem, subgroup 5A ...... 0 .10 Cotton, undelinted seed ...... 0 .05 Cowpea, forage ...... 0 .05 (b) Section 18 emergency exemptions. Cowpea, hay ...... 0 .05 [Reserved] Cucumber ...... 0 .1 (c) Tolerances with regional registra- Pea, southern, dry seed ...... 0.05 tions. [Reserved] Pea, southern, succulent seed ...... 0 .05 (d) Indirect and inadvertent residues. Pea, succulent ...... 0 .05 Pepper ...... 0 .05 [Reserved] Peppermint, tops ...... 0 .05 [65 FR 33701, May 24, 2000, as amended at 67 Pumpkin ...... 0.1 FR 49617, July 31, 2002; 73 FR 52616, Sept. 10, Rhubarb ...... 0 .30 2008] Rice, grain ...... 0 .02 Rice, straw ...... 0 .02 Soybean ...... 0.05 § 180.428 Metsulfuron methyl; toler- Spearmint, tops ...... 0 .05 ances for residues. Squash, summer ...... 0 .1 (a) General. (1) Tolerances are estab- Squash, winter ...... 0 .1 lished for the combined residues of the Sugarcane, cane ...... 0.05 Sweet potato, roots ...... 0 .05 herbicide metsulfuron methyl (methyl Vegetable, cucurbit, group 9 ...... 0.05 2-[[[[(4-methoxy-6-methyl-1,3,5- triazin- Vegetable, tuberous and corm, except potato, 2-yl)amino]carbonyl]amino] sulfonyl] subgroup 1D ...... 0 .05 benzoate) and its metabolite methyl 2- [[[[(4-methoxy-6-methyl-1-,3,5- triazin- (b) Section 18 emergency exemptions. 2-yl)amino]carbonyl]amino] sulfonyl]- [Reserved] 4-hydroxybenzoate in or on the fol- (c) Tolerances with regional registra- lowing raw material agricultural com- tions. [Reserved] modities: (d) Indirect or inadvertent residues. Parts per [Reserved] Commodity million

[51 FR 9446, Mar. 19, 1986] Barley, grain ...... 0 .1 EDITORIAL NOTE: For FEDERAL REGISTER ci- Barley, hay ...... 20 .0 tations affecting § 180.425, see the List of CFR Barley, straw ...... 0 .3 Sections Affected, which appears in the Grass, forage ...... 15 .0 Finding Aids section of the printed volume Grass, hay ...... 15 .0 and at www.fdsys.gov. Grass, straw ...... 15 .0 Sorghum, grain, forage ...... 0.2 Sorghum, grain, grain ...... 0 .1 § 180.426 2-[4,5-Dihydro-4-methyl-4-(1- Sorghum, grain, stover ...... 0 .2 methylethyl)-5-oxo-1H-imidazol-2- Sugarcane, cane ...... 0.05 yl]-3-quinoline carboxylic acid; tol- Wheat, forage ...... 5 .0 erance for residues. Wheat, grain ...... 0 .1 A tolerance is established for resi- Wheat, hay ...... 20 .0 dues of the herbicide 2-[4,5-dihydro-4- Wheat, straw ...... 0 .3 methyl-4-(1-methylethyl)-5-oxo-1H- (2) Tolerances are established for res- imidazol-2-yl]-3-quinoline carboxylic idues of metsulfuron methyl (methyl- acid, in or on the raw agricultural com- 2[[[[(4-methoxy- 6-methyl-1,3,5-triazin- modity soybean at 0.05 part per mil- 2- yl)amino]carbonyl]amino] sulfonyl] lion. benzoate) in or on the following raw [51 FR 13309, Apr. 2, 1986] agricultural commodities:

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(d) Indirect or inadvertent residues. Commodity Parts per million [Reserved] Cattle, fat ...... 0.1 [74 FR 10494, Mar. 11, 2009, as amended at 74 Cattle, kidney ...... 0 .5 FR 67087, Dec. 18, 2009] Cattle, meat ...... 0 .1 Cattle, meat byproducts ...... 0.1 Goat, fat ...... 0 .1 § 180.430 Fenoxaprop-ethyl; tolerances Goat, kidney ...... 0 .5 for residues. Goat, meat ...... 0.1 Goat, meat byproducts ...... 0 .1 (a) General. Tolerances are estab- Hog, fat ...... 0 .1 lished for residues of the herbicide Hog, kidney ...... 0.5 fenoxaprop-ethyl, including its me- Hog, meat ...... 0 .1 Hog, meat byproducts ...... 0 .1 tabolites and degradates, in or on the Horse, fat ...... 0 .1 commodities in the table in this para- Horse, kidney ...... 0 .5 graph. Compliance with the tolerance Horse, meat ...... 0 .1 Horse, meat byproducts ...... 0 .1 levels specified in this paragraph is to Milk ...... 0.05 be determined by measuring only the Sheep, fat ...... 0 .1 sum of fenoxaprop-ethyl, (±)-ethyl 2-[4- Sheep, kidney ...... 0.5 Sheep, meat ...... 0.1 [(6-chloro-2- Sheep, meat byproducts ...... 0 .1 benzoxazolyl)oxy]phenoxy]propanoate, and its metabolites, 2-[4-[(6-chloro-2- (b) Section 18 emergency exemptions. benzoxazolyl)oxy]phenoxy]propanoic [Reserved] acid and 6-chloro-2,3- (c) Tolerances with regional registra- dihydrobenzoxazol-2-one, calculated as tions. [Reserved] the stoichiometric equivalent of (d) Indirect or inadvertent residues. fenoxaprop-ethyl, in or on the com- [Reserved] modity.

[64 FR 70191, Dec. 16, 1999, as amended at 66 Parts per FR 64773, Dec. 14, 2001; 67 FR 51097, Aug. 7, Commodity million 2002] Barley, grain ...... 0 .05 Barley, straw ...... 0 .1 § 180.429 Chlorimuron ethyl; toler- Cattle, fat ...... 0.05 ances for residues. Cattle, meat byproducts ...... 0.05 Cattle, meat ...... 0 .05 (a) General. Tolerances are estab- Cotton, undelinted seed ...... 0 .05 lished for residues of the herbicide Goat, fat ...... 0 .05 chlorimuron ethyl, including its me- Goat, meat byproducts ...... 0 .05 Goat, meat ...... 0.05 tabolites and degradates, in or on the Hog, fat ...... 0 .05 commodities in the table below. Com- Hog, meat byproducts ...... 0 .05 pliance with the tolerance levels speci- Hog, meat ...... 0 .05 Horse, fat ...... 0 .05 fied in the following table is to be de- Horse, meat byproducts ...... 0 .05 termined by measuring only Horse, meat ...... 0 .05 chlorimuron ethyl, ethyl 2-[[[[(4- Milk ...... 0.02 chloro-6-methoxypyrimidin- Peanut ...... 0 .05 Peanut, hulls ...... 0 .05 2yl)amino]carbonyl]sulfonyl]benzoate] Rice, grain ...... 0 .05 in or on the following commodities: Sheep, fat ...... 0 .05 Sheep, meat byproducts ...... 0 .05 Parts per Sheep, meat ...... 0.05 Commodity million Soybean ...... 0.05 Wheat, grain ...... 0 .05 Berry, low growing, except strawberry, subgroup Wheat, straw ...... 0 .50 13–07H ...... 0 .02 Corn, field, forage ...... 0 .5 (b) Section 18 emergency exemptions. Corn, field, grain ...... 0 .01 Corn, field, stover ...... 2 .0 Time-limited tolerances are estab- Grain, aspirated fractions ...... 3 .0 lished for residues of the herbicide Peanut ...... 0 .02 fenoxaprop-ethyl, including its me- Soybean, forage ...... 0 .45 Soybean, hay ...... 1 .8 tabolites and degradates, in or on the Soybean, seed ...... 0 .05 commodities in the table in this paragraph in connection with use of (b) Section 18 emergency exemptions. fenoxaprop-ethyl under section 18 [Reserved] emergency exemptions granted by (c) Tolerances with regional registra- EPA. Compliance with the tolerance tions. [Reserved] levels specified in this paragraph is to

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be determined by measuring only the and degradates, in or on the commod- sum of fenoxaprop-ethyl, (±)-ethyl 2-[4- ities in the table below from its appli- [(6-chloro-2- cation in the acid form or in the form benzoxazolyl)oxy]phenoxy]propanoate, of its salts. Compliance with the toler- and its metabolites, 2-[4-[(6-chloro-2- ance levels specified below is to be de- benzoxazolyl)oxy]phenoxy]propanoic termined by measuring only clopyralid, acid and 6-chloro-2,3- (3,6-dichloro-2-pyridinecarboxylic acid), dihydrobenzoxazol-2-one, calculated as in or on the following commodities: the stoichiometric equivalent of Parts per fenoxaprop-ethyl, in or on the com- Commodity million modity. The tolerances expire and are revoked on the dates specified in the Apple ...... 0.05 Asparagus ...... 1.0 table in this paragraph. Barley, bran ...... 12 Barley, grain ...... 3 .0 Parts per Expiration/ Barley, hay ...... 9 .0 Commodity million revocation Barley, pearled barley ...... 12 date Barley, straw ...... 9 .0 Beet, garden, tops ...... 3 .0 Grass, forage ...... 0.05 12/31/16 Beet, garden, roots ...... 4 .0 Grass, hay ...... 0.05 12/31/16 Beet, sugar, molasses ...... 10 Beet, sugar, roots ...... 2 .0 (c) Tolerances with regional registra- Beet, sugar, tops ...... 3.0 Brassica, head and stem, subgroup 5A ...... 2 .0 tions. Tolerances with regional reg- Brassica, leafy greens, subgroup 5B ...... 5 .0 istration, as defined in § 180.1(l), are es- Bushberry subgroup 13-07B ...... 0 .50 tablished for residues of the herbicide Canola, meal ...... 6 .0 fenoxaprop-ethyl, including its me- Canola, seed ...... 3 .0 Cattle, fat ...... 1.0 tabolites and degradates, in or on the Cattle, liver ...... 3 .0 commodities in the table in this para- Cattle, meat ...... 1 .0 graph when fenoxaprop-ethyl is used in Cattle, meat byproducts, except liver ...... 36 .0 Corn, field, forage ...... 3 .0 the states of Oregon, Washington, and Corn, field, grain ...... 1 .0 Utah. Compliance with the tolerance Corn, field, milled byproducts ...... 1 .5 levels specified in this paragraph is to Corn, field, stover ...... 10 .0 Corn, pop, grain ...... 1.0 be determined by measuring only the Corn, pop, stover ...... 10.0 sum of fenoxaprop-ethyl, (±)-ethyl 2-[4- Corn, sweet, forage ...... 7 .0 [(6-chloro-2- Corn, sweet, kernel plus cob with husks removed ...... 1 .0 benzoxazolyl)oxy]phenoxy]propanoate, Corn, sweet, stover ...... 10.0 and its metabolites, 2-[4-[(6-chloro-2- Cranberry ...... 4 .0 benzoxazolyl)oxy]phenoxy]propanoic Egg ...... 0 .1 Flax, meal ...... 6 .0 acid and 6-chloro-2,3- Fruit, stone, group 12 ...... 0 .5 dihydrobenzoxazol-2-one, calculated as Goat, fat ...... 1 .0 the stoichiometric equivalent of Goat, liver ...... 3.0 fenoxaprop-ethyl, in or on the com- Goat, meat ...... 1.0 Goat, meat byproducts, except liver ...... 36 .0 modity Grass, forage ...... 500.0 Grass, hay ...... 500.0 Commodity Parts per Hog, fat ...... 0 .2 million Hog, meat ...... 0 .2 Hog, meat byproducts ...... 0 .2 Grass, hay ...... 0 .09 Hop, dried cones ...... 5 .0 Horse, fat ...... 1 .0 (d) Indirect or inadvertent residues. Horse, liver ...... 3 .0 [Reserved] Horse, meat ...... 1 .0 Horse, meat byproducts, except liver ...... 36 .0 [63 FR 1377, Jan. 9, 1998, as amended at 63 FR Milk ...... 0.2 Oat, forage ...... 9 .0 19837, Apr. 22, 1998; 73 FR 33718, June 13, 2008; Oat, grain ...... 3 .0 75 FR 80346, Dec. 22, 2010; 76 FR 23495, Apr. 27, Oat, groats/rolled oats ...... 12 2011; 78 FR 78748, Dec. 27, 2013; 79 FR 26164, Oat, straw ...... 9.0 May 7, 2014] Peppermint, tops ...... 3 .0 Plum, prune, dried ...... 1.5 § 180.431 Clopyralid; tolerances for Poultry, fat ...... 0.2 Poultry, meat ...... 0 .2 residues. Poultry, meat byproducts ...... 0.2 (a) General. Tolerances are estab- Rapeseed, forage ...... 3 .0 Rapeseed, meal ...... 6 .0 lished for residues of the herbicide Rapeseed, subgroup 20A, except gold of pleas- clopyralid, including its metabolites ure ...... 3 .0

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lactofen, including its metabolites and Commodity Parts per million degradates, in or on the commodities Sheep, fat ...... 1 .0 in the table in this paragraph. Compli- Sheep, liver ...... 3.0 ance with the tolerance levels specified Sheep, meat ...... 1.0 Sheep, meat byproducts, except liver ...... 36 .0 in this paragraph is to be determined Spearmint, tops ...... 3 .0 by measuring only lactofen, 2-ethoxy-1- Spinach ...... 5 .0 methyl-2-oxoethyl 5-[2-chloro-4- Strawberry ...... 4 .0 Swiss chard ...... 3.0 (trifluoromethyl)phenoxy]-2- Teff, forage ...... 9 .0 nitrobenzoate, in or on the commodity. Teff, grain ...... 3 .0 Teff, hay ...... 9 .0 Commodity Parts per Teff, straw ...... 9 .0 million Turnip, greens ...... 4.0 Turnip, roots ...... 1 .0 Okra ...... 0.02 Wheat, bran ...... 12 Vegetables, fruiting, group 08 ...... 0 .02 Wheat, forage ...... 9 .0 Wheat, germ ...... 12 Wheat, grain ...... 3 .0 (d) Indirect or inadvertent residues. Wheat, middling ...... 12 [Reserved] Wheat, shorts ...... 12 Wheat, straw ...... 9 .0 [69 FR 57216, Sept. 24, 2004, as amended at 72 FR 33906, June 20, 2007; 76 FR 23496, Apr. 27, (b) Section 18 emergency exemptions. 2011] [Reserved] (c) Tolerances with regional registra- § 180.433 Fomesafen; tolerances for tions. [Reserved] residues. (d) Indirect or inadvertent residues. [Reserved] (a) General. Tolerances are established for residues of the herbicide [52 FR 10566, Apr. 2, 1987] fomesafen, including its metabolites EDITORIAL NOTE: For FEDERAL REGISTER ci- and degradates, in or on the following tations affecting § 180.431, see the List of CFR commodities. Compliance with the tol- Sections Affected, which appears in the erance levels specified in the following Finding Aids section of the printed volume and at www.fdsys.gov. table below is to be determined by measuring only fomesafen, 5-[2-chloro- § 180.432 Lactofen; tolerances for resi- 4-(trifluoromethyl)phenoxy]-N- dues. (methylsulfonyl)-2-nitrobenzamide, in (a) General. Tolerances are estab- or on the commodity. lished for residues of the herbicide Parts per lactofen, including its metabolites and Commodity million degradates, in or on the commodities in the table in this paragraph. Compli- Bean, dry ...... 0.05 ance with the tolerance levels specified Bean, lima, succulent ...... 0.05 in this paragraph is to be determined Bean, snap, succulent ...... 0.05 Cantaloupe ...... 0.025 by measuring only lactofen, 2-ethoxy-1- Cotton, gin byproducts ...... 0.025 methyl-2-oxoethyl 5-[2-chloro-4- Cotton, undelinted seed ...... 0.025 (trifluoromethyl)phenoxy]-2- Cucumber ...... 0.025 nitrobenzoate, in or on the commodity. Pea, succulent ...... 0.025 Pepper, bell ...... 0.025 Commodity Parts per Pepper, non-bell ...... 0.025 million Potato ...... 0.025 Pumpkin ...... 0.025 Beans, snap, succulent, except lima bean ...... 0 .01 Cotton, gin byproducts ...... 0 .02 Soybean ...... 0.05 Cotton, undelinted seed ...... 0 .01 Soybean, vegetable, succulent ...... 0.05 Peanut ...... 0 .01 Squash, summer ...... 0.025 Soybean, seed ...... 0 .01 Squash, winter ...... 0.025 Tomato ...... 0.025 (b) Section 18 emergency exemptions. [Reserved] (b) Section 18 emergency exemptions. (c) Tolerances with regional registra- [Reserved] tions. Tolerances with regional reg- (c) Tolerances with regional registra- istration, as defined in § 180.1(l), are es- tions. [Reserved] tablished for residues of the herbicide

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(d) Indirect or inadvertent residues. Commodity Parts per [Reserved] million [71 FR 25951, May 3, 2006, as amended at 72 Horse, fat ...... 0 .05 FR 52020, Sept. 12, 2007; 76 FR 12882, Mar. 9, Horse, kidney ...... 2 .0 Horse, liver ...... 2 .0 2011; 78 FR 65570, Nov. 1, 2013] Horse, meat ...... 0 .05 Horse, meat byproducts, except liver and kidney 0 .05 § 180.434 Propiconazole; tolerances for Leaf petioles subgroup 4B ...... 5 .0 residues. Low growing berry subgroup 13–07G, except cranberry ...... 1 .3 (a) General. Tolerances are estab- Milk ...... 0.05 lished for residues of propiconazole, in- Mushroom ...... 0 .1 cluding its metabolites and degradates, Nut, tree, group 14 ...... 0 .1 Oat, forage ...... 4 .0 in or on the commodities in the table Oat, grain ...... 3 .0 below. Compliance with the tolerance Oat, hay ...... 15 levels specified below is to be deter- Oat, straw ...... 10 Onion, bulb subgroup 3–07A ...... 0.2 mined by measuring only those Onion, green, subgroup 3–07B ...... 9 .0 propiconazole residues convertible to Parsley, fresh leaves ...... 13 2,4-dichlorobenzoic acid (2,4–DCBA), ex- Parsley, dried leaves ...... 35 Peanut ...... 0 .2 pressed as the stoichiometric equiva- Peanut, hay ...... 20 lent of propiconazole, in or on the com- Peppermint, tops ...... 10 .0 modity in the table below: Pineapple ...... 4.5 Pineapple, process residue ...... 7 .0 Pistachio ...... 0.1 Parts per Commodity million Plum ...... 0 .60 Rapeseed subgroup 20A ...... 0 .30 Almond, hulls ...... 7 .0 Rice, bran ...... 15 Banana ...... 0.2 Rice, grain ...... 7 .0 Barley, bran ...... 6 .0 Rice, hulls ...... 20 Barley, grain ...... 3 .0 Rice, straw ...... 18 Barley, hay ...... 30 Rye, bran ...... 0 .6 Barley, straw ...... 20 Rye, forage ...... 9 .0 Bean, dry seed ...... 0 .40 Rye, grain ...... 0.3 Bean, snap ...... 0 .70 Rye, straw ...... 10 Bean, succulent shelled ...... 0 .10 Sheep, fat ...... 0 .05 Beet, garden, roots ...... 0 .30 Sheep, kidney ...... 2.0 Beet, garden, tops ...... 5 .5 Sheep, liver ...... 2.0 Beet, sugar, dried pulp ...... 1 .0 Sheep, meat ...... 0.05 Beet, sugar, molasses ...... 1 .5 Sheep, meat byproducts, except liver and kid- Beet, sugar, roots ...... 0 .3 ney ...... 0.05 Beet, sugar, tops ...... 10 Sorghum, grain, forage ...... 12 Bushberry, subgroup 13–07B ...... 1.0 Sorghum, grain, grain ...... 3 .5 Caneberry, subgroup 13–07A ...... 1 .0 Sorghum, grain, stover ...... 15 Carrot, roots ...... 0.25 Soybean, forage ...... 11 Cattle, fat ...... 0.05 Soybean, hay ...... 30 Cattle, kidney ...... 2 .0 Soybean, seed ...... 2 .0 Cattle, liver ...... 2 .0 Spearmint, tops ...... 10 .0 Cattle, meat ...... 0 .05 Sugarcane, cane ...... 0.4 Cattle, meat byproducts, except liver and kidney 0.05 Tomato ...... 3.0 Cilantro, leaves ...... 13 Vegetable, foliage of legume, group 7 ...... 30 Citrus, oil ...... 1000 Wheat, bran ...... 0.6 Corn, field, forage ...... 12 Wheat, forage ...... 15 Corn, field, grain ...... 0 .2 Wheat, grain ...... 0 .3 Corn, field, stover ...... 30 Wheat, hay ...... 30 Corn, pop, grain ...... 0.2 Wheat, straw ...... 20 Corn, pop, stover ...... 30 Corn, sweet, forage ...... 6 .0 (b) Section 18 emergency exemptions. Corn, sweet, kernel plus cob with husks removed ...... 0 .1 Time-limited tolerances are estab- Corn, sweet, stover ...... 30 lished for residues of propiconazole (1- Fruit, citrus, group 10–10 ...... 8 .0 [[2-(2,4-dichlorophenyl)-4-propyl-1,3- Fruit, stone, group 12, except plum ...... 4 .0 dioxolan-2-yl] methyl]-1H-1,2,4-triazole) Goat, fat ...... 0 .05 Goat, kidney ...... 2 .0 and its metabolites determined as 2,4- Goat, liver ...... 2.0 dichlorobenzoic acid and expressed as Goat, meat ...... 0.05 parent compound, in connection with Goat, meat byproducts, except liver and kidney 0 .05 Grain, aspirated fractions ...... 110 use of the pesticide under section 18 Grass, forage ...... 0 .5 emergency exemptions granted by Grass, hay ...... 0 .5 EPA. The tolerances will expire and Grass, straw ...... 40 Hog, kidney ...... 0.2 are revoked on the dates specified in Hog, liver ...... 0 .2 the following table:

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dimethylcyclopropanecarboxylate] and Parts per Expiration/ Commodity revocation alpha-R-deltamethrin [(R)-alpha-cyano- million date m-phenoxybenzyl-(1R,3R)-3-(2,2- Avocado ...... 10 12/31/16 dibromovinyl)-2,2- Nectarine ...... 2.0 12/31/13 dimethylcyclopropanecarboxylate] in Peach ...... 2.0 12/31/13 or on the following agricultural com- (c) Tolerances with regional registra- modities: tions. A tolerance with regional reg- Parts per istration, as defined in § 180.1(l), is es- Commodity million tablished for residues of 1-[[2-(2,4- Almond, hulls ...... 2 .5 dichlorophenyl)-4-propyl-1,3-dioxolan-2- Apple, wet pomace ...... 1 .0 yl]methyl]-1H-1,2,4-triazole and its me- Artichoke, globe ...... 0.5 tabolites determined as 2,4- Barley, bran ...... 5 .0 Cattle, fat ...... 0.05 dichlorobenzoic acid and expressed as Cattle, meat ...... 0 .02 parent compound, in or on the fol- Cattle, meat byproducts ...... 0.05 lowing commodities: Corn, field, forage ...... 0 .7 Corn, field, refined oil ...... 2 .5 Parts per Corn, field, stover ...... 5 .0 Commodity million Corn, pop, stover ...... 5.0 Corn, sweet, forage ...... 10 Cranberry ...... 1 .0 Corn, sweet, kernel plus cob with husks re- Rice, wild, grain ...... 0.5 moved ...... 0 .03 Corn, sweet, stover ...... 15 Cotton, refined oil ...... 0.2 (d) Indirect or inadvertent residues. Cotton, undelinted seed ...... 0 .04 Tolerances are established for the com- Egg ...... 0 .02 bined residues of the fungicide 1-[[2- Fruit, pome, Group 11 ...... 0 .2 Goat, fat ...... 0 .05 (2,4-dichlorophenyl)-4-propyl-1,3- Goat, meat ...... 0.02 dioxolan-2-yl] methyl]-1H-1,2,4-triazole Goat, meat byproducts ...... 0 .05 and its metabolites determined as 2,4- Grain, aspirated fractions ...... 65 Grain, cereal, Group 15, except sweet corn ...... 1 .0 dichlorobenzoic acid and expressed as Hog, fat ...... 0 .05 parent compound in or on the following Horse, fat ...... 0 .05 commodities when present therein as a Horse, meat ...... 0 .02 result of application of propiconazole Horse, meat byproducts ...... 0 .05 Lychee* ...... 0 .2 to growing crops in paragraphs (a) and Milk, fat (reflecting 0.02 ppm in whole milk) ...... 0 .1 (c) of this section: Nut, tree, Group 14 ...... 0.1 Onion, bulb ...... 0 .1 Parts per Onion, green ...... 1 .5 Commodity million Poultry, fat ...... 0.05 Poultry, meat ...... 0 .02 Alfalfa, forage ...... 0.1 Poultry, meat byproducts ...... 0.02 Alfalfa, hay ...... 0.1 Radish, tops ...... 4 .0 Rapeseed ...... 0 .2 Rice, hulls ...... 2 .5 [71 FR 55306, Sept. 22, 2006, as amended at 72 Rye, bran ...... 5 .0 FR 20439, Apr. 25, 2007; 74 FR 12613, Mar. 25, Sheep, fat ...... 0 .05 2009; 75 FR 80346, Dec. 22, 2010; 76 FR 27268, Sheep, meat ...... 0.02 May 11, 2011; 77 FR 38204, June 27, 2012; 77 FR Sheep, meat byproducts ...... 0 .05 Sorghum, grain, forage ...... 0.5 75044, Dec. 19, 2012; 78 FR 23503, Apr. 19, 2013; Sorghum, grain, stover ...... 1 .0 78 FR 78748, Dec. 27, 2013; 79 FR 18467, Apr. 2, Soybean, seed ...... 0 .1 2014] Soybean, hulls ...... 0 .2 Starfruit* ...... 0.2 § 180.435 Deltamethrin; tolerances for Sunflower, seed ...... 0.1 residues. Tomato ...... 0.2 Tomato, paste ...... 1 .0 (a) General. (1) Tolerances are estab- Tomato, puree ...... 1 .0 lished for the combined residues of the Vegetable, cucurbit, Group 9 ...... 0 .2 Vegetable, fruiting, Group 8 ...... 0 .3 pesticide chemical deltamethrin Vegetable, root, except sugar beet, Subgroup IB 0 .2 [(1R,3R)-3-(2,2-dibromovinyl)-2,2- Vegetable, tuberous and corm, Subgroup IC ..... 0 .04 dimethylcyclopropanecarboxylic acid Wheat, bran ...... 5.0 (S)-alpha-cyano-3-phenoxybenzyl ester *There are no U.S. registrations for use of deltamethrin on and its major metabolites, trans starfruit and lychee. deltamethrin [(S)-alpha-cyano-m- (2) A tolerance of 0.05 ppm is estab- phenoxybenzyl(1R,3S)-3-(2,2- lished for residues of the insecticide dibromovinyl)-2,2- deltamethrin (1R,3R)-3-(2,2-

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dibromovinyl)-2,2- (c) Tolerances with regional registra- dimethylcyclopropanecarboxylic acid tions. [Reserved] (S)-alpha-cyano-3-phenoxybenzyl ester (d) Indirect or inadvertent residues. and its major metabolites, trans [Reserved] deltamethrin (S)-alpha-cyano-m- [62 FR 63001, Nov. 26, 1997, as amended at 63 phenoxybenzyl-(1R,3R)-3-(2,2- FR 45414, Aug. 26, 1998; 69 FR 62614, Oct. 27, dibromovinyl)-2,2- 2004; 74 FR 46375, Sept. 9, 2009; 76 FR 34885, dimethylcyclopropanecarboxylate and June 15, 2011] alpha-R-deltamethrin[(R)-alpha-cyano- m-phenoxybenzyl-(1R,3R)-3-(2,2- § 180.436 Cyfluthrin and the isomer dibromovinyl)-2,2- beta-cyfluthrin; tolerances for resi- dimethylcyclopropanecarboxylate] as dues. follows: (a) General. (1) Tolerances are estab- (i) In or on all food/feed items (other lished for residues of the insecticide than those covered by a higher toler- cyfluthrin (cyano(4-fluoro-3- ance as a result of use on growing phenoxyphenyl)methyl-3-(2,2- crops) in food/feed handling establish- dichloroethenyl)-2,2dimethyl- ments. cyclopropane-carboxylate; CAS No. (ii) The insecticide may be present as 68359–37–5) in or on the following raw a residue from application of agricultural commodities: deltamethrin in food handling estab- Parts per lishments, including food service, man- Commodity million ufacturing and processing establishments, such as restaurants, cafeterias, Alfalfa ...... 5 .0 Alfalfa, forage ...... 5.0 supermarkets, bakeries, breweries, Alfalfa, hay ...... 13 dairies, meat slaughtering and packing Almond, hulls ...... 0 .5 plants, and canneries, feed handling es- Barley, bran ...... 0 .5 Barley, grain ...... 0 .15 tablishments including feed manufac- Beet, sugar, dried pulp ...... 1 .0 turing and processing establishments, Beet, sugar, roots ...... 0 .10 in accordance with the following pre- Brassica, head and stem, subgroup 5A ...... 2 .5 Brassica, leafy greens, subgroup 5B ...... 7 .0 scribed conditions: Buckwheat, grain ...... 0.15 (A) Application shall be limited to Carrot, roots ...... 0.20 general surface and spot and/or crack Cattle, fat ...... 2.0 and crevice treatment in food/feed han- Cattle, meat ...... 0 .10 Cattle, meat byproducts ...... 0.10 dling establishments where food/feed Citrus, dried pulp ...... 0 .3 and food/feed products are held, proc- Citrus, oil ...... 0.3 essed, prepared and served. General Corn, field, grain ...... 0 .05 Corn, pop, grain ...... 0.05 surface application may be used only Corn, sweet, kernel plus cob with husks re- when the facility is not in operation moved ...... 0 .05 provided exposed food/feed has been Cotton, hulls ...... 2 .0 Cotton, refined oil ...... 2.0 covered or removed from the area Cotton, undelinted seed ...... 1 .0 being treated. Spot and/or crack and Egg ...... 0 .01 crevice application may be used while Fruit, citrus, group 10 ...... 0 .2 the facility is in operation provided ex- Fruit, pome, group 11 ...... 0.5 Fruit, stone, group 12 ...... 0 .3 posed food/feed is covered or removed Goat, fat ...... 2 .0 from the area being treated prior to ap- Goat, meat ...... 0.05 plication. Spray concentration shall be Goat, meat byproducts ...... 0 .05 Grain, aspirated fractions ...... 150 limited to a maximum of 0.06 percent Grain, cereal, forage, fodder and hay, group 16, active ingredient. Contamination of forage, except rice ...... 25 food/feed or food/feed contact surfaces Grain, cereal, forage, fodder and hay, group 16, hay, except rice ...... 6 .0 shall be avoided. Grain, cereal, forage, fodder and hay, group 16, (B) To assure safe use of the insecti- stover, except rice ...... 30 cide, its label and labeling shall con- Grain, cereal, forage, fodder and hay, group 16, form to that registered with the U.S. straw, except rice ...... 7 .0 Grape ...... 1 .0 Environmental Protection Agency and Grape, raisin ...... 3 .5 shall be used in accordance with such Grass, forage, fodder and hay, group 17, forage 12 label and labeling. Grass, forage, fodder and hay, group 17, hay .... 50 Hog, fat ...... 0 .5 (b) Section 18 emergency exemptions. Hog, meat ...... 0 .01 [Reserved] Hog, meat byproducts ...... 0 .01

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(i) General surface treatments shall Commodity Parts per million be limited to a maximum of 3.8 grams Hop, dried cones ...... 20 .0 of active ingredient per 1,000 square Hop, vines ...... 4 .0 feet, applying to walls, floors, and ceil- Horse, fat ...... 2 .0 ings with a low-pressure system. Cover Horse, meat ...... 0 .05 Horse, meat byproducts ...... 0 .05 or remove all food processing and/or Lettuce, head ...... 2.0 handling equipment during applica- Lettuce, leaf ...... 3 .0 tion. Do not apply directly to food Milk ...... 0.2 products. Reapplications may be made Milk, fat ...... 5 .0 Millet, grain ...... 0 .15 at 10-day intervals. Mustard greens ...... 7.0 (ii) Crack and crevice or spot treat- Nut, tree, group 14 ...... 0 .01 ments shall be limited to a maximum Oat, bran ...... 0 .5 of 0.1 percent of the active ingredient Oat, grain ...... 0 .15 Pea and bean, dried shelled, except soybean, weight, applied with a low-pressure subgroup 6C ...... 0 .15 system with a pinpoint or variable-pat- Pea, dry, seed ...... 0 .15 tern nozzle. Dust formulation shall be Pea, southern, succulent ...... 0 .25 limited to a maximum of 0.1 percent of Peanut ...... 0 .01 Peanut, hay ...... 6.0 the active ingredient by weight, ap- Pepper ...... 0 .50 plied using a hand duster, power dust- Pistachio ...... 0.01 er, or other equipment capable of ap- Poultry, fat ...... 0.01 Poultry, meat ...... 0 .01 plying dust insecticide directly into Poultry, meat byproducts ...... 0.01 voids and cracks and crevices. Dust ap- Radish, roots ...... 1 .0 plications should be made in a manner Rye, bran ...... 0 .5 to avoid deposits on exposed surfaces Rye, grain ...... 0.15 Sheep, fat ...... 2 .0 or introducing the material into the Sheep, meat ...... 0.05 air. Cover exposed food or remove food Sheep, meat byproducts ...... 0 .05 from premises. Do not apply directly to Sorghum, grain, grain ...... 3 .5 food. Reapplications may be made at Soybean, forage ...... 8 .0 Soybean, hay ...... 4 .0 10-day intervals. Soybean, seed ...... 0 .03 (iii) To ensure safe use of the insecti- Sugarcane, cane ...... 0.05 cide, its label and labeling shall con- Sugarcane, molasses ...... 0 .20 form to that registered by the Environ- Sunflower, forage ...... 5.0 Sunflower, seed ...... 0.02 mental Protection Agency, and it shall Teosinte, grain ...... 0 .05 be used in accordance with such label Tomato ...... 0.20 and labeling. Tomato, dry pomace ...... 5.0 Tomato, paste ...... 0 .5 (3) A tolerance of 0.05 part per mil- Tomato, wet pomace ...... 5.0 lion is established for residues of the Triticale, grain ...... 0 .15 insecticide cyfluthrin (cyano(4-fluoro- Turnip, greens ...... 7.0 3-phenoxyphenyl)methyl-3-(2,2- Vegetable, cucurbit, group 9 ...... 0.1 Vegetable, fruiting, group 8 ...... 0.5 dichloroethenyl)-2,2- Vegetable, leafy, except brassica, group 4 ...... 6 .0 dimethylcyclopropanecarboxylate; Vegetable, tuberous and corm, subgroup 1C ..... 0.01 CAS Reg. No. 68359–37–5) in feed com- Wheat, bran ...... 0.5 Wheat, grain ...... 0 .15 modities exposed to the insecticide Wheat, shorts ...... 0 .5 during treatment of feed-handling establishments where feed and feed prod- (2) A tolerance of 0.05 ppm is estab- ucts are held, processed, prepared, or lished for residues of the insecticide served. Treatments may be made by cyfluthrin (cyano(4-fluoro-3- general surface, spot, and/or crack and phenoxyphenyl)methyl-3-(2,2- crevice applications. dichloroethenyl)-2,2- (i) General surface tratments shall be dimethylcyclopropanecarboxylate; limited to a maximum of 3.8 grams of CAS Reg. No. 69359–37–5) in food com- active ingredient per 1,000 square feet, modities exposed to the insecticide applying to walls, floors, and ceilings during treatment of food-handling es- with a low-pressure system. Cover or tablishments where food and food prod- remove all feed processing and/or han- ucts are held, processed, prepared, or dling equipment during application. Do served. Treatments may be made by not apply directly to feed products. Re- general surface, spot, and/or crack and applications may be made at 10-day in- crevice applications. tervals.

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(ii) Crack and crevice or spot treat- Commodity Parts per ments shall be limited to a maximum million of 0.1 percent of the active ingredient Cattle, meat ...... 0 .10 by weight, applied with a low-pressure Cattle, meat byproducts ...... 0.10 system with a pinpoint or variable-pat- Citrus, dried pulp ...... 0 .3 Citrus, oil ...... 0.3 tern nozzle. Dust formulation shall be Corn, field, grain ...... 0 .05 limited to a maximum of 0.1 percent of Corn, pop, grain ...... 0.05 the active ingredient by weight, ap- Corn, sweet, kernel plus cob with husks removed ...... 0 .05 plied using a hand duster, power dust- Cotton, hulls ...... 2 .0 er, or other equipment capable of ap- Cotton, refined oil ...... 2.0 plying dust insecticide directly into Cotton, undelinted seed ...... 1 .0 voids and cracks and crevices. Dust ap- Egg ...... 0 .01 Fruit, citrus, group 10 ...... 0 .2 plications should be made in a manner Fruit, pome, group 11 ...... 0.5 to avoid deposits on exposed surfaces Fruit, stone, group 12 ...... 0 .3 or introducing the material into the Goat, fat ...... 2 .0 Goat, meat ...... 0.05 air. Cover exposed feed or remove feed Goat, meat byproducts ...... 0 .05 from premises. Do not apply directly to Grain, aspirated fractions ...... 150 feed. Reapplications may be made at Grain, cereal, forage, fodder and hay, group 16, forage, except rice ...... 25 10-day intervals. Grain, cereal, forage, fodder and hay, group 16, (iii) To ensure safe use of the insecti- hay, except rice ...... 6 .0 cide, its label and labeling shall con- Grain, cereal, forage, fodder and hay, group 16, form to that registered by EPA, and it stover, except rice ...... 30 Grain, cereal, forage, fodder and hay, group 16, shall be used in accordance with such straw, except rice ...... 7 .0 label and labeling. Grape ...... 1 .0 (4) Tolerances are established for res- Grape, raisin ...... 3 .5 Grass, forage, fodder and hay, group 17, forage 12 idues of the isomer, beta-cyfluthrin, Grass, forage, fodder and hay, group 17, hay .... 50 cyano(4-fluoro-3- Hog, fat ...... 0 .5 phenoxyphenyl)methyl-3-(2,2- Hog, meat ...... 0 .01 dichloroethenyl)-2,2-dimethyl- Hog, meat byproducts ...... 0 .01 Hop, dried cones ...... 20 .0 cyclopropanecarboxylate [mixture Hop, vines ...... 4 .0 comprising the enantiomeric pair (R)- Horse, fat ...... 2 .0 a-cyano-4-fluoro-3-phenoxybenzyl Horse, meat ...... 0 .05 Horse, meat byproducts ...... 0 .05 (1S,3S)-3-(2,2-dichlorovinyl)-2,2- Lettuce, head ...... 2.0 dimethylcyclopropanecarboxylate and Lettuce, leaf ...... 3 .0 (S)-a-cyano-4-fluoro-3-phenoxybenzyl Milk ...... 0.2 (1R,3R)-3-(2,2-dichlorovinyl)-2,2- Milk, fat ...... 5 .0 Millet, grain ...... 0 .15 dimethylcyclopropanecarboxylate with Mustard greens ...... 7.0 the enantiomeric pair (R)-a-cyano-4- Nut, tree, group 14 ...... 0 .01 fluoro-3-phenoxybenzyl (1S,3R)-3-(2,2- Oat, bran ...... 0 .5 Oat, grain ...... 0 .15 dichlorovinyl)-2,2- Pea and bean, dried shelled, except soybean, dimethylcyclopropanecarboxylate and subgroup 6C ...... 0 .15 (S)-a-cyano-4-fluoro-3-phenoxybenzyl Pea, dry, seed ...... 0 .15 (1R,3S)-3-(2,2-dichlorovinyl)-2,2- Pea, southern, succulent ...... 0 .25 Peanut ...... 0 .01 dimethylcyclopropanecarboxylate], in Peanut, hay ...... 6.0 or on the following raw agricultural Pepper ...... 0 .50 commodities: Pistachio ...... 0.01 Poultry, fat ...... 0.01 Parts per Poultry, meat ...... 0 .01 Commodity million Poultry, meat byproducts ...... 0.01 Radish, roots ...... 1 .0 Alfalfa ...... 5 .0 Rye, bran ...... 0 .5 Alfalfa, forage ...... 5.0 Rye, grain ...... 0.15 Alfalfa, hay ...... 13 Sheep, fat ...... 2 .0 Almond, hulls ...... 0 .5 Sheep, meat ...... 0.05 Barley, bran ...... 0 .5 Sheep, meat byproducts ...... 0 .05 Barley, grain ...... 0 .15 Sorghum, grain, grain ...... 3 .5 Beet, sugar, dried pulp ...... 1 .0 Soybean, forage ...... 8 .0 Beet, sugar, roots ...... 0 .10 Soybean, hay ...... 4 .0 Brassica, head and stem, subgroup 5A ...... 2 .5 Soybean, seed ...... 0 .03 Brassica, leafy greens, subgroup 5B ...... 7 .0 Sugarcane, cane ...... 0.05 Buckwheat, grain ...... 0.15 Sugarcane, molasses ...... 0 .20 Carrot, roots ...... 0.20 Sunflower, forage ...... 5.0 Cattle, fat ...... 2.0 Sunflower, seed ...... 0.02

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dimethylcyclopropanecarboxylate and Commodity Parts per million (R)-a-cyano-3-phenoxybenzyl-(Z)- Teosinte, grain ...... 0 .05 (1S,3S)-3-(2-chloro-3,3,3-trifluoroprop-1- Tomato ...... 0.20 enyl)-2,2- Tomato, paste ...... 0 .5 dimethylcyclopropanecarboxylate and Tomato, pomace ...... 5 .0 Triticale, grain ...... 0 .15 its epimer expressed as epimer of lamb- Turnip, greens ...... 7.0 da-cyhalothrin, a 1:1 mixture of (S)-a- Vegetable, cucurbit, group 9 ...... 0.1 cyano-3-phenoxybenzyl-(Z)-(1S,3S)-3-(2- Vegetable, fruiting, group 8 ...... 0.5 Vegetable, leafy greens, except Brassica, group chloro-3,3,3-trifluoroprop-1-enyl)-2,2- 4 ...... 6 .0 dimethylcyclopropanecarboxylate and Vegetable, tuberous and corm, subgroup 1C ..... 0.01 (R)-a-cyano-3-phenoxybenzyl-(Z)- Wheat, bran ...... 0.5 (1R,3R)-3-(2-chloro-3,3,3-trifluoroprop-1- Wheat, grain ...... 0 .15 Wheat, shorts ...... 0 .5 enyl)-2,2- dimethylcyclopropanecarboxylate, on (b) Section 18 emergency exemptions. plants and livestocks, as indicated in [Reserved] the following table. (c) Tolerances with regional registra- Parts per tions. [Reserved] Commodity million (d) Indirect or inadvertent residues. [Reserved] Alfalfa, forage ...... 5.0 Alfalfa, hay ...... 6.0 [53 FR 1924, Jan. 25, 1988] Almond, hulls ...... 1 .5 Apple, wet pomace ...... 2 .50 EDITORIAL NOTE: For FEDERAL REGISTER ci- Avocado, imported ...... 0.20 tations affecting § 180.436, see the List of CFR Barley, bran ...... 0 .2 Sections Affected, which appears in the Barley, grain ...... 0 .05 Finding Aids section of the printed volume Barley, hay ...... 2 .0 Barley, straw ...... 2 .0 and at www.fdsys.gov. Brassica, head and stem, subgroup 5A ...... 0 .4 Buckwheat, grain ...... 0.05 § 180.437 Methyl 2-(4-isopropyl-4-meth- Canola, refined oil ...... 2 .0 yl-5-oxo-2-imidazolin-2-yl)-p-toluate Canola, seed ...... 1 .0 and methyl 6-(4-isopropyl-4-methyl- Cattle, fat ...... 3.0 5-oxo-2-imidazolin-2-yl)-m-toluate; Cattle, meat ...... 0 .2 Cattle, meat byproducts ...... 0.2 tolerances for residues. Corn, field, flour ...... 0 .15 Tolerances are established for the Corn, field, forage ...... 6 .0 Corn, field, grain ...... 0 .05 combined residues of the herbicide Corn, field, stover ...... 1 .0 methyl 2-(4-isopropyl-4-methyl-5-oxo-2- Corn, pop, grain ...... 0.05 imidazolin-2-yl)-p-toluate and methyl Corn, pop, grain, flour ...... 0 .05 6-(4-isopropyl-4-methyl-5-oxo-2- Corn, pop, stover ...... 1.0 Corn, sweet, forage ...... 6 .0 imidazolin-2-yl)-m-toluate in or on the Corn, sweet, stover ...... 1 .0 following raw agricultural commod- Corn, sweet, kernel plus cob with husks re- ities: moved ...... 0 .05 Cotton, undelinted seed ...... 0 .05 Egg ...... 0 .01 Parts per Commodity million Fruit, pome, group 11 ...... 0.30 Fruit, stone, group 12 ...... 0 .50 Barley, grain ...... 0 .10 Garlic ...... 0 .1 Barley, straw ...... 2 .00 Goat, fat ...... 3 .0 Sunflower, seed ...... 0.10 Goat, meat ...... 0.2 Wheat, grain ...... 0 .10 Goat, meat byproducts ...... 0 .2 Wheat, straw ...... 2 .00 Grain, aspirated fractions ...... 2 .0 Grass, forage, fodder and hay, group 17 ...... 7 .0 Hog, fat ...... 0 .2 [53 FR 24069, June 27, 1988] Hog, meat ...... 0 .01 Hog, meat byproducts ...... 0 .02 Hop, dried cones ...... 10 .0 § 180.438 Lambda-cyhalothrin and an Horse, fat ...... 3 .0 isomer gamma-cyhalothrin; toler- Horse, meat ...... 0 .2 ances for residues. Horse, meat byproducts ...... 0 .2 (a) General. (1) Tolerances are estab- Lettuce, head ...... 2.0 Lettuce, leaf ...... 2 .0 lished for the combined residues of the Milk, fat (reflecting 0.4 ppm in whole milk) ...... 10 .0 pyrethroid lambda-cyhalothrin, 1:1 Nut, tree, group 14 ...... 0 .05 mixture of (S)-a-cyano-3- Oat, grain ...... 0 .05 Oat, forage ...... 2 .0 phenoxybenzyl-(Z)-(1R,3R)-3-(2-chloro- Oat, hay ...... 2.0 3,3,3-trifluoroprop-1-enyl)-2,2- Oat, straw ...... 2.0

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Parts per Parts per Commodity million Commodity million

Onion, bulb ...... 0 .1 Corn, field, flour ...... 0 .15 Pea and bean, dried shelled, except soybean, Corn, field, forage ...... 6 .0 subgroup 6C ...... 0 .10 Corn, field, grain ...... 0 .05 Pea and bean, succulent shelled, subgroup 6B 0 .01 Corn, field, stover ...... 1 .0 Peanut ...... 0 .05 Corn, pop, grain ...... 0.05 Peanut, hay ...... 3.0 Corn, pop, stover ...... 1.0 Pistachio ...... 0.05 Corn, sweet, forage ...... 6 .0 Poultry, fat ...... 0.03 Corn, sweet, kernel plus cob with husks re- Poultry, meat ...... 0 .01 moved ...... 0 .05 Poultry, meat byproducts ...... 0.01 Corn, sweet, stover ...... 1 .0 Rice, grain ...... 1 .0 Cotton, undelinted seed ...... 0 .05 Rice, hulls ...... 5 .0 Egg ...... 0 .01 Rice, straw ...... 1 .8 Fruit, pome, group 11 ...... 0.30 Rice, wild, grain ...... 1.0 Fruit, stone, group 12 ...... 0 .50 Rye, bran ...... 0 .2 Garlic ...... 0 .10 Rye, grain ...... 0.05 Goat, fat ...... 3 .0 Rye, forage ...... 2 .0 Goat, meat ...... 0.2 Rye, straw ...... 2 .0 Goat, meat byproducts ...... 0 .2 Sheep, fat ...... 3 .0 Grain, aspirated fractions ...... 2 .0 Sheep, meat ...... 0.2 Hog, fat ...... 3 .0 Sheep, meat byproducts ...... 0 .2 Hog, meat ...... 0 .2 Soybean ...... 0.01 Hog, meat byproducts ...... 0 .2 Sorghum, grain, grain ...... 0 .2 Horse, fat ...... 3 .0 Sorghum, grain, forage ...... 0.30 Horse, meat ...... 0 .2 Sorghum, grain, stover ...... 0 .50 Horse, meat byproducts ...... 0 .2 Sugarcane, cane ...... 0.05 Lettuce, head ...... 2.0 Sunflower, forage ...... 0.2 Lettuce, leaf ...... 2 .0 Sunflower, seed, hulls ...... 0 .50 Milk, fat (reflecting 0.20 ppm in whole milk) ...... 5 .0 Sunflower, refined oil ...... 0.30 Nut, tree, group 14 ...... 0 .05 Sunflower, seed ...... 0.2 Okra ...... 0.20 Tomato ...... 0.1 Onion, bulb ...... 0 .1 Tomato, dry pomace ...... 6.0 Pea and bean, dried shelled, except soybean, Tomato, wet pomace ...... 6.0 subgroup 6C ...... 0 .10 Vegetable, cucurbit, group 9 ...... 0.05 Pea and bean, succulent shelled, subgroup 6B 0 .01 Vegetable, fruiting, group 8 ...... 0.20 Peanut ...... 0 .05 Vegetable, legume, edible podded, subgroup 6A 0 .20 Peanut, hay ...... 3.0 Vegetable, tuberous and corm, subgroup 1C ..... 0.02 Pistachio ...... 0.05 Wheat, grain ...... 0 .05 Poultry, fat ...... 0.03 Wheat, forage ...... 2 .0 Poultry, meat ...... 0 .01 Wheat, hay ...... 2 .0 Poultry, meat byproducts ...... 0.01 Wheat, straw ...... 2 .0 Rice, grain ...... 1 .0 Wheat, bran ...... 0.2 Rice, hulls ...... 5 .0 Rice, straw ...... 1 .8 1 Sheep, fat ...... 3 .0 (2) Tolerances are established for Sheep, meat ...... 0.2 the combined residues of the Sheep, meat byproducts ...... 0 .2 pyrethroid [gamma-cyhalothrin (the Sorghum, grain, forage ...... 0.30 isolated active isomer of lambda- Sorghum, grain, grain ...... 0 .20 Sorghum, grain, stover ...... 0 .50 cyhalothrin) (S)-′-cyano-3- Soybean ...... 0.01 phenoxybenzyl (Z)-(1R,3R)-3-(2-chloro- Sugarcane ...... 0 .05 3,3,3-trifluoroprop-1-enyl)-2,2- Sunflower, forage ...... 0.20 Sunflower, refined oil ...... 0.30 dimethylcyclopropanecarboxylate)) Sunflower, seed ...... 0.20 and its epimer (R)-′-cyano-3- Sunflower, seed, hulls ...... 0 .50 phenoxybenzyl (Z)-(1R,3R)-3-(2-chloro- Tomato ...... 0.10 Tomato, dry pomace ...... 6.0 3,3,3-trifluoroprop-1-enyl)-2,2- Tomato, wet pomace ...... 6.0 dimethylcyclopropanecarboxylate in/ Vegetables, fruiting, group 8 ...... 0.20 on the following commodities: Vegetable, legume, edible podded, subgroup 6A 0 .20 Wheat, bran ...... 2.0 Parts per Wheat, forage ...... 2 .0 Commodity million Wheat, grain ...... 0 .05 Wheat, hay ...... 2 .0 Alfalfa, forage ...... 5 Wheat, straw ...... 2 .0 Alfalfa, hay ...... 6 1 The analytical enforcement methods for lambda- Almond, hulls ...... 1 .5 cyhalothrin are applicable for determination of gamma- Apple, pomace, wet ...... 2 .50 cyhalothrin residues in plant and animal commodities. Avocado, imported ...... 0.20 Brassica, head and stem, subgroup 5A ...... 0 .4 (3) A tolerance of 0.01 part per mil- Canola, seed ...... 0 .15 lion is established for residues of the Cattle, fat ...... 3 Cattle, meat ...... 0 .2 insecticide lamba-cyhalothrin and an Cattle, meat byproducts ...... 0.2 isomer gamma-cyhalothrin in or on all

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food commodities (other than those al- cluding its metabolites and degradates, ready covered by a higher tolerance as in or on the commodities listed in the a result of use on growing crops) in following table [below]. Compliance food-handling establishments where with the tolerance levels specified in food products are held, processed, or the following table [below] is to be de- prepared. termined by measuring only (b) Section 18 emergency exemptions. thifensulfuron methyl (methyl 3-[[[[(4- [Reserved] methoxy-6-methyl-1,3,5-triazin-2- (c) Tolerances with regional registra- yl)amino]carbonyl]amino] sulfonyl]-2- tions. [Reserved] thiophenecarboxylate). (d) Indirect or inadvertent residues. Parts per [Reserved] Commodity million

[71 FR 74817, Dec. 13, 2006, as amended at 72 Safflower, seed ...... 0 .05 FR 45663, Aug. 15, 2007; 73 FR 39264, July 9, 2008; 76 FR 34885, June 15, 2011] (d) Indirect or inadvertent residues. § 180.439 Thifensulfuron methyl; toler- [Reserved] ances for residues. [69 FR 55982, Sept. 17, 2004, as amended at 69 (a) General. Tolerances are estab- FR 63957, Nov. 3, 2004; 72 FR 13184, Mar. 21, lished for residues of thifensulfuron 2007; 73 FR 47075, Aug. 13, 2008; 75 FR 19277, methyl, including its metabolites and Apr. 14, 2010; 77 FR 52240, Aug. 29, 2012] degradates, in or on the commodities § 180.440 Tefluthrin; tolerances for res- listed in the following table [below]. idues. Compliance with the tolerance levels specified in the following table [below] (a) General. Tolerances are estab- is to be determined by measuring only lished for the combined residues of the thifensulfuron methyl (methyl 3-[[[[(4- insecticide tefluthrin (2,3,5,6 methoxy-6-methyl-1,3,5-triazin-2- tetrafluroro-4-methylphenyl)methyl-(1 ± yl)amino]carbonyl]amino] sulfonyl]-2- alpha, 3 alpha)-(Z)-( )-3(2-chloro-3,3,3- thiophenecarboxylate). trifluoro-1-propenyl)-2,2- diemthylcyclopropanecarboxylate) and Commodity Parts per its metabolite (Z)-3-(2-chloro-3,3,3- million trifluroro-1-propenyl)-2,2- Barley, grain ...... 0 .05 dimethylcyclopropanecarboxylic acid Barley, hay ...... 0 .8 in or on the following commodities: Barley, straw ...... 0 .10 Canola, seed ...... 0 .02 Parts per Chicory, roots ...... 0 .01 Commodity million Chicory, tops ...... 0 .01 Corn, field, forage ...... 0 .10 Corn, field, forage ...... 0 .06 Corn, field, grain ...... 0 .05 Corn, field, grain ...... 0 .06 Corn, field, stover ...... 0 .10 Corn, field, stover ...... 0 .06 Cotton, gin byproducts ...... 0 .02 Corn, pop, grain ...... 0.06 Cotton, undelinted seed ...... 0 .02 Corn, pop, stover ...... 0.06 Flax, seed ...... 0 .02 Corn, sweet, forage ...... 0 .06 Oat, forage ...... 0 .2 Corn, sweet, kernel plus cob with husks re- Oat, grain ...... 0 .05 moved ...... 0 .06 Oat, hay ...... 0.05 Corn, sweet, stover ...... 0 .06 Oat, straw ...... 0.10 Rice, grain ...... 0 .05 Rice, straw ...... 0 .05 (b) Section 18 emergency exemptions. Sorghum, grain, forage...... 0 .05 [Reserved] Sorghum, grain, grain ...... 0 .05 (c) Tolerances with regional registra- Sorghum, grain, stover ...... 0 .05 tions. [Reserved] Soybean ...... 0.10 Wheat, forage ...... 2 .5 (d) Indirect or inadvertent residues. Wheat, grain ...... 0 .05 [Reserved] Wheat, hay ...... 0 .7 Wheat, straw ...... 0 .10 [62 FR 62961, Nov. 26, 1997, as amended at 74 FR 46375, Sept. 9, 2009] (b) Section 18 emergency exemptions. [Reserved] § 180.441 Quizalofop ethyl; tolerances (c) Tolerances with regional registra- for residues. tions. Tolerances are established for (a) General. (1) Tolerances are estab- residues of thifensulfuron methyl, in- lished for residues of the herbicide

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quizalofop ethyl, including its metabo- Commodity Parts per lites and degradates, in or on the com- million modities in the following table. Com- Cattle, meat ...... 0 .02 pliance with the tolerance levels speci- Cattle, meat byproducts ...... 0.05 fied in the following table is to be de- Egg ...... 0 .02 Goat, fat ...... 0 .05 termined by measuring only those Goat, meat ...... 0.02 quizalofop ethyl residues convertible to Goat, meat byproducts ...... 0 .05 2-methoxy-6-chloroquinoxaline, ex- Hog, fat ...... 0 .05 Hog, meat ...... 0 .02 pressed as the stoichiometric equiva- Hog, meat byproducts ...... 0 .05 lent of quizalofop ethyl, in or on the Horse, fat ...... 0 .05 commodity. Horse, meat ...... 0 .02 Horse, meat byproducts ...... 0 .05 Milk ...... 0.01 Parts per Commodity million Milk, fat ...... 0 .25 Poultry, fat ...... 0.05 Barley, grain ...... 0 .05 Poultry, meat ...... 0 .02 Barley, hay ...... 0 .05 Poultry, meat byproducts ...... 0.05 Barley, straw ...... 0 .05 Sheep, fat ...... 0 .05 Bean, dry, seed ...... 0 .4 Sheep, meat ...... 0.02 Bean, succulent ...... 0 .25 Sheep, meat byproducts ...... 0 .05 Beet, sugar, molasses ...... 0 .2 Beet, sugar, roots ...... 0 .1 (b) Section 18 emergency exemptions. Beet, sugar, tops ...... 0.5 [Reserved] Cotton, undelinted seed ...... 0 .1 Cowpea, forage ...... 3 .0 (c) Tolerances with regional registra- Cowpea, hay ...... 3 .0 tions. Tolerances with regional reg- Crambe, meal ...... 2 .0 istration are established for residues of Flax, seed ...... 0 .05 Gold of pleasure, meal ...... 2.0 the herbicide quizalofop ethyl, includ- Lentil, seed ...... 0 .05 ing its metabolites and degradates, in Pea, dry ...... 0 .25 or on the commodities in the following Pea, field, hay ...... 3.0 table. Compliance with the tolerance Pea, field, vines ...... 3 .0 Pea, succulent ...... 0 .3 levels specified in the following table is Peppermint, tops ...... 2 .0 to be determined by measuring only Rapeseed, meal ...... 2 .0 those quizalofop ethyl residues con- Rapeseed subgroup 20A, except flax, seed ...... 1 .5 Sorghum, grain, aspirated grain fractions ...... 1 .0 vertible to 2-methoxy-6- Sorghum, grain, forage ...... 0.20 chloroquinoxaline, expressed as the Sorghum, grain, grain ...... 0 .20 stoichiometric equivalent of quizalofop Sorghum, grain, stover ...... 0 .30 Soybean, flour ...... 0 .5 ethyl, in or on the commodity. Soybean, hulls ...... 0 .02 Soybean, meal ...... 0.5 Parts per Commodity million Soybean, seed ...... 0 .05 Soybean, soapstock ...... 1 .0 Pineapple ...... 0.1 Spearmint, tops ...... 2 .0 Sunflower, seed ...... 1.9 Wheat, forage ...... 0 .05 (d) Indirect or inadvertent residues. Wheat, grain ...... 0 .05 [Reserved] Wheat, hay ...... 0 .05 Wheat, straw ...... 0 .05 [63 FR 32759, June 16, 1998, as amended at 70 FR 7870, Feb. 16, 2005; 71 FR 56378, Sept. 27, (2) Tolerances are established for res- 2006; 76 FR 56045, Sept. 15, 2010; 77 FR 23630, idues of the herbicide quizalofop ethyl, Apr. 20, 2012] including its metabolites and degradates, in or on the commodities § 180.442 Bifenthrin; tolerances for residues. in the following table. Compliance with the tolerance levels specified in the fol- (a) General. (1) Tolerances are estab- lowing table is to be determined by lished for residues of the insecticide measuring only those quizalofop ethyl bifenthrin, including its metabolites residues convertible to quizalofop (2-[4- and degradates, in or on the commod- (6-chloroquinoxalin-2-yl- ities in the table below. Compliance oxy)phenoxy]propanoic acid), expressed with the tolerance levels specified as quizalofop, in or on the commodity. below is to be determined by measuring only bifenthrin, (2-methyl [1,1′- Commodity Parts per biphenyl]-3-yl) methyl-3-(2-chloro- million 3,3,3,-trifluoro-1-propenyl)-2,2- Cattle, fat ...... 0.05 dimethylcyclopropanecarboxylate.

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Parts per Parts per Commodity million Commodity million

Almond, hulls ...... 2 .0 Turnip, greens ...... 3.5 Artichoke, globe ...... 1.0 Vegetable, cucurbit, group 9 ...... 0.4 Banana 1 ...... 0.1 Vegetable, legume, edible podded, subgroup 6A 0 .6 Beet, garden, roots ...... 0 .45 Vegetable, root, subgroup 1B except sugar beet Beet, garden, tops ...... 15 and garden beet ...... 0 .10 Brassica, head and stem, subgroup 5A, except Vegetable, tuberous and corm, subgroup 1C ..... 0.05 cabbage ...... 0 .6 Brassica, leafy greens, subgroup 5B ...... 3 .5 1 There are no U.S. registrations. Bushberry subgroup 13-07B ...... 1 .8 Cabbage ...... 4 .0 (2) A tolerance of 0.05 ppm is estab- Caneberry subgroup 13A ...... 1 .0 lished for residues of the insecticide Cattle, fat ...... 1.0 bifenthrin, (2-methyl[1,1′-biphenyl]-3- Cattle, meat byproducts ...... 0.10 Cattle, meat ...... 0 .5 yl)methyl-3-(2-chloro-3,3,3-trifluoro-1- Coriander, dried leaves ...... 25 propenyl)-2,2-dimethylcyclopropane- Coriander, leaves ...... 6 .0 carboxylate, as follows: Coriander, seed ...... 5 .0 Corn, field, forage ...... 3 .0 (i) In or on all food/feed items (other Corn, field, grain ...... 0 .05 than those covered by a higher toler- Corn, field, stover ...... 5 .0 ance as a result of use on growing Corn, pop, grain ...... 0.05 crops) in food/feed handling establish- Corn, pop, stover ...... 5.0 Corn, sweet, forage ...... 3 .0 ments. Corn, sweet, kernel plus cob with husk removed 0.05 (ii) The insecticide may be present as Corn, sweet, stover ...... 5 .0 a residue from application of bifenthrin Cotton, undelinted seed ...... 0 .5 Eggplant ...... 0.05 in food handling establishments, in- Egg ...... 0 .05 cluding food service, manufacturing Fruit, citrus, group 10 ...... 0 .05 and processing establishments, such as Goat, fat ...... 1 .0 restaurants, cafeterias, supermarkets, Goat, meat byproducts ...... 0 .10 Goat, meat ...... 0.5 bakeries, breweries, dairies, meat Grain, aspirated fractions ...... 70 slaughtering and packing plants, and Grape ...... 0 .2 canneries, feed handling establish- Groundcherry ...... 0 .5 Herb subgroup 19A ...... 0 .05 ments including feed manufacturing Hog, fat ...... 1 .0 and processing establishments, in ac- Hog, meat byproducts ...... 0 .10 cordance with the following prescribed Hog, meat ...... 0 .5 conditions: Hop, dried cones ...... 10 .0 Horse, fat ...... 1 .0 (A) Application shall be limited to Horse, meat byproducts ...... 0 .10 general surface and spot and/or crack Horse, meat ...... 0 .5 and crevice treatment in food/feed han- Leafy petioles subgroup 4B ...... 3 .0 Lettuce, head ...... 3.0 dling establishments where food/feed Mayhaw ...... 1 .4 and food/feed products are held, proc- Milk, fat (reflecting 0.1 ppm in whole milk) ...... 1 .0 essed, prepared and served. General Nut, tree, group 14 ...... 0 .05 surface application may be used only Okra ...... 0.50 Pea and bean, dried shelled, expect soybean, when the facility is not in operation subgroup 6C ...... 0 .15 provided exposed food/feed has been Pea and bean, succulent shelled, subgroup 6B 0 .05 covered or removed from the area Peanut ...... 0 .05 Pear ...... 0 .5 being treated. Spot and/or crack and Pepino ...... 0 .5 crevice application may be used while Pepper, bell ...... 0 .5 the facility is in operation provided ex- Pepper, nonbell ...... 0 .5 posed food/feed is covered or removed Pistachio ...... 0.05 Poultry, fat ...... 0.05 from the area being treated prior to ap- Poultry, meat byproducts ...... 0.05 plication. Spray concentration shall be Poultry, meat ...... 0 .05 limited to a maximum of 0.06 percent Radish, tops ...... 4 .5 Rapeseed, seed ...... 0 .05 active ingredient. Contamination of Sheep, fat ...... 1 .0 food/feed or food/feed contact surfaces Sheep, meat byproducts ...... 0 .1 shall be avoided. Sheep, meat ...... 0.5 (B) To assure safe use of the insecti- Soybean, hulls ...... 0 .50 Soybean, refined oil ...... 0 .30 cide, its label and labeling shall con- Soybean, seed ...... 0 .2 form to that registered with the U.S. Spinach ...... 0 .2 Environmental Protection Agency and Strawberry ...... 3 .0 Tea, dried 1 ...... 30 shall be used in accordance with such Tomato ...... 0.15 label and labeling.

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(b) Section 18 emergency exemptions. propanenitrile (free and bound), in or Time-limited tolerances are estab- on the following food commodities: lished for residues of the insecticide Parts per bifenthrin, including its metabolites Commodity million and degradates, in connection with use of the pesticide under a Section 18 Almond ...... 0.1 Almond, hulls ...... 2 .0 emergency exemption granted by EPA. Apple ...... 0.5 Compliance with the tolerance levels Apple, dry pomace ...... 5.0 specified below is to be determined by Apple, wet pomace ...... 5 .0 Artichoke, globe ...... 0.90 measuring only bifenthrin, (2-methyl Asparagus ...... 0.02 [1,1′-biphenyl]-3-yl) methyl-3-(2-chloro- Banana, postharvest ...... 4 .0 3,3,3,-trifluoro-1-propenyl)-2,2- Bean, snap, succulent ...... 1 .0 dimethylcyclopropanecarboxylate. Caneberry subgroup 13A ...... 2 .0 Canistel ...... 3 .0 These tolerances will expire and are re- Cattle, fat ...... 0.05 voked on the dates specified in the fol- Cattle, liver ...... 1 .0 lowing table: Cattle, meat ...... 0 .1 Cattle, meat byproducts, except liver ...... 0 .2 Cherry, sweet ...... 5 .0 Expiration/ Commodity Parts per revocation Cherry, tart ...... 5 .0 million date Cilantro, leaves ...... 9 .0 Cotton, undelinted seed ...... 0 .02 Apple ...... 0.5 12/31/15 Currant ...... 3 .0 Nectarine ...... 0.5 12/31/15 Egg ...... 0 .02 Peach ...... 0.5 12/31/15 Fruit, stone, except cherry ...... 2.0 Goat, fat ...... 0 .05 Goat, liver ...... 1.0 (c) Tolerances with regional registra- Goat, meat ...... 0.1 tions. Tolerances with regional reg- Goat, meat byproducts, except liver ...... 0 .2 istrations are established for residues Gooseberry ...... 2 .0 Grain, aspirated fractions ...... 35 of the insecticide bifenthrin, including Grape ...... 1 .0 its metabolites and degradates, in or Grape, dried pomace ...... 10 .0 on the commodities in the table below. Grape, raisin ...... 10.0 Grape, raisin, waste ...... 25 .0 Compliance with the tolerance levels Grape, wet pomace ...... 10 .0 specified below is to be determined by Hog, fat ...... 0 .05 measuring only bifenthrin, (2-methyl Hog, liver ...... 1 .0 ′ Hog, meat ...... 0 .1 [1,1 -biphenyl]-3-yl) methyl-3-(2-chloro- Hog, meat byproducts, except liver ...... 0 .2 3,3,3,-trifluoro-1-propenyl)-2,2- Hop, dried cones ...... 10 dimethylcyclopropanecarboxylate. Horse, fat ...... 0 .05 Horse, liver ...... 1 .0 Parts per Horse, meat ...... 0 .1 Commodity million Horse, meat byproducts, except liver ...... 0 .2 Leafy greens, subgroup 4A, except spinach ...... 9 .0 Grass, forage ...... 4 .0 Mango ...... 3.0 Grass, hay ...... 15 Mayhaw ...... 0 .70 Milk ...... 0.2 (d) Indirect or inadvertent residues. Okra ...... 4.0 Papaya ...... 3 .0 [Reserved] Peppermint, tops ...... 3 .0 Plum, prune, dried ...... 8.0 [62 FR 31002, June 6, 1997] Poultry, fat ...... 0.02 Poultry, meat ...... 0 .02 EDITORIAL NOTE: For FEDERAL REGISTER ci- Poultry, meat byproducts ...... 0.02 tations affecting § 180.442, see the List of CFR Sapodilla ...... 3 .0 Sections Affected, which appears in the Sapote, black ...... 3 .0 Finding Aids section of the printed volume Sapote, mamey ...... 3 .0 and at www.fdsys.gov. Sheep, fat ...... 0 .05 Sheep, liver ...... 1.0 § 180.443 Myclobutanil; tolerances for Sheep, meat ...... 0.1 residues. Sheep, meat byproducts, except liver ...... 0 .2 Soybean, forage ...... 3 .5 (a) General. Tolerances are estab- Soybean, hay ...... 15 lished for combined residues of the fun- Soybean, refined oil ...... 0 .40 Soybean, seed ...... 0 .25 gicide myclobutanil alpha-butyl-alpha- Spearmint, tops ...... 3 .0 (4-chlorophenyl)-1H-1,2,4-triazole-1- Star apple ...... 3 .0 propanenitrile and its alcohol metabo- Strawberry ...... 0 .50 Tomato ...... 0.30 lite (alpha-(3-hydroxybutyl)-alpha-(4- Tomato, puree ...... 0 .50 chlorophenyl)-1H-1,2,4-triazole-1- Tomato, paste ...... 1 .0

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Parts per Expiration/ Commodity million Commodity Parts per revocation million date Vegetable, cucurbit, group 9 ...... 0.20 Vegetable, fruiting, group 8, except tomato ...... 4 .0 Fig ...... 10 12/31/14

(b) Section 18 emergency exemptions. (c) Tolerances with regional registra- [Reserved] tions. [Reserved] (c) Tolerances with regional registra- (d) Indirect or inadvertent residues. tions. [Reserved] [Reserved] (d) Indirect or inadvertent residues. [54 FR 20126, May 10, 1989, as amended at 76 Tolerances are established for residues FR 56648, Sept. 14, 2011] of the fungicide myclobutanil alpha- butyl-alpha-(4-chlorophenyl)-1H-1,2,4- § 180.445 Bensulfuron methyl; toler- triazole-1-propanenitrile in or on the ances for residues. following food commodities: (a) General. Tolerances are established for residues of the herbicide Parts per Commodity million bensulfuron methyl (methyl-2[[[[[(4,6- dimethoxy-pyrimidin-2-yl) amino] car- Animal feed, nongrass, group 18 ...... 0 .03 Grain, cereal, forage, fodder and straw, group bonyl] amino] sulfonyl] methyl] ben- 16 ...... 0 .03 zoate) in or on the following raw agri- Grain, cereal, group 15 ...... 0.03 cultural commodities: Vegetable, brassica, leafy, group 5 ...... 0.03 Vegetable, foliage of legume, group 7 ...... 0 .03 Parts per Vegetable, fruiting, group 8 ...... 0.03 Commodity million Vegetable, leafy, except brassica, group 4 ...... 0 .03 Vegetable, leaves of root and tuber, group 2 ..... 0 .03 Crayfish ...... 0.05 Vegetable, legume, group 6 ...... 0 .03 Rice, grain ...... 0 .02 Vegetable, root and tuber, group 1 ...... 0 .03 Rice, straw ...... 0 .3

[54 FR 6131, Feb. 8, 1989] (b) Section 18 emergency exemptions. [Reserved] EDITORIAL NOTE: For FEDERAL REGISTER ci- (c) Tolerances with regional registra- tations affecting § 180.443, see the List of CFR tions. [Reserved] Sections Affected, which appears in the (d) Indirect or inadvertent residues. Finding Aids section of the printed volume and at www.fdsys.gov. [Reserved] [63 FR 9435, Feb. 25, 1998] § 180.444 Sulfur dioxide; tolerances for residues. § 180.446 Clofentezine; tolerances for (a) General. A tolerance is established residues. as follows for sulfite residues of the (a) General. (1) Tolerances are estab- fungicide sulfur dioxide (determined as lished for residues of the insecticide (SO2)) in or on the following raw agri- clofentezine, including its metabolites cultural commodity(ies): and degradates, in or on the commodities in the table in this paragraph. Parts per Commodity million Compliance with the tolerance levels specified in this paragraph is to be de- Grape, postharvest ...... 10.0 termined by measuring only clofentezine, 3,6-bis(2-chlorophenyl)- (b) Section 18 emergency exemptions. 1,2,4,5-tetrazine, in or on the com- Time-limited tolerances specified in modity. the following table are established for residues of sulfur dioxide, including its Commodity Parts per metabolites and degradates in or on million the specified agricultural commodities, Almond, hulls ...... 5 .0 resulting from use of the pesticide pur- Almond ...... 0.5 suant to FFIFRA section 18 emergency Apple ...... 0.5 Apple, dry pomace ...... 3.0 exemptions. Compliance with the toler- Apple, wet pomace ...... 3 .0 ance levels specified below is to be de- Apricot ...... 1 .0 termined by measuring only sulfur di- Cherry ...... 1.0 Grape ...... 1 .0 oxide (SO2). The tolerances expire on Nectarine ...... 1 .0 the date specified in the table. Peach ...... 1 .0

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applied as its acid or ammonium salt, Commodity Parts per million in or on the following raw agricultural Pear ...... 0 .5 commodities: Persimmon ...... 0 .05 Walnut ...... 0 .02 Parts per Commodity million

(2) Tolerances are established for res- Canola, seed 1 ...... 0 .10 idues of the insecticide clofentezine, Soybean ...... 0.1 including its metabolites and Vegetable, legume, group 6 ...... 0 .1 degradates, in or on the commodities 1 There are no U.S. registrations for canola as of March in the table in this paragraph. Compli- 21, 2003. ance with the tolerance levels specified (2) Tolerances are established for the in this paragraph is to be determined sum of the residues of the herbicide by measuring only the sum of imazethapyr, 2-[4,5-dihydro-4-methyl-4- clofentezine, 3,6-bis(2-chlorophenyl)- (1-methylethyl)-5-oxo- 1H-imidazol-2- 1,2,4,5-tetrazine, and its metabolite, 3- yl]-5-ethyl-3-pyridine carboxylic acid; (2-chloro-4-hydroxyphenyl)-6-(2- its metabolite CL 288511, 2-[4,5-dihydro- chlorophenyl)-1,2,4,5-tetrazine, cal- 4-methyl-4-(1-methylethyl)-5-oxo-1H- culated as the stoichiometric equiva- imidazol-2-yl]-5-(1-hydroxyethyl)-3-pyr- lent of clofentezine, in or on com- idine carboxylic acid; and its metabo- modity. lite CL 182704, 5-[1-(beta-D- Parts per glucopyranosyloxy)ethyl]-2-[4,5- Commodity million dihydro-4-methyl-4-(1-methylethyl)-5- Cattle, fat ...... 0.05 oxo-1H-imidazol-2-yl]-3- Cattle, liver ...... 0 .4 pyridinecarboxylic acid, applied as its Cattle, meat ...... 0 .05 acid or ammonium salt, in or on the Cattle, meat byproducts, except liver ...... 0 .05 Goat, fat ...... 0 .05 following commodities: Goat, liver ...... 0.4 Goat, meat ...... 0.05 Commodity Parts per Goat, meat byproducts, except liver ...... 0 .05 million Hog, fat ...... 0 .05 Hog, liver ...... 0 .4 Alfalfa, seed ...... 0 .15 Hog, meat ...... 0 .05 Alfalfa, seed screenings ...... 0 .15 Hog, meat byproducts, except liver ...... 0 .05 Animal feed, nongrass, group 18, forage ...... 3 .0 Horse, fat ...... 0 .05 Animal feed, nongrass, group 18, hay ...... 5.5 Horse, liver ...... 0 .4 Peanut ...... 0 .1 Horse, meat ...... 0 .05 Rice, bran ...... 1.2 Horse, meat byproducts, except liver ...... 0 .05 Rice, grain ...... 0 .3 Milk ...... 0.01 Rice, straw ...... 0 .4 Sheep, fat ...... 0 .05 Sheep, liver ...... 0.4 Sheep, meat ...... 0.05 (3) A tolerance is established for the Sheep, meat byproducts, except liver ...... 0 .05 sum of residues of the herbicide imazethapyr, 2-[4,5-dihydro-4-methyl-4- (b) Section 18 emergency exemptions. (1-methylethyl)-5-oxo- 1H-imidazol-2- [Reserved] yl]-5-ethyl-3-pyridine carboxylic acid, (c) Tolerances with regional registra- and its metabolite CL 288511, 2-[4,5- tions. [Reserved] dihydro-4-methyl-4-(1-methylethyl)-5- (d) Indirect or inadvertent residues. oxo-1H-imidazol-2-yl]-5-(1-hydroxy- [Reserved] ethyl)-3-pyridine carboxylic acid, ap- [56 FR 15503, Apr. 17, 1991, as amended at 56 plied as its acid or ammonium salt, in FR 22335, May 15, 1991; 59 FR 26947, May 25, or on the following commodities: 1994; 60 FR 12709, Mar. 8, 1995; 64 FR 19050, Apr. 19, 1999; 70 FR 11572, Mar. 9, 2005; 74 FR Parts per Commodity million 46375, Sept. 9, 2009; 76 FR 23496, Apr. 27, 2011] Cattle, meat byproducts ...... 0.10 § 180.447 Imazethapyr; tolerances for Corn, field, forage ...... 0 .1 residues. Corn, field, grain ...... 0 .1 Corn, field, stover ...... 0 .1 (a) General. (1) Tolerances are estab- Crayfish ...... 0.15 lished for residues of the herbicide Goat, meat byproducts ...... 0 .10 imazethapyr, 2-[4,5-dihydro-4-methyl-4- Hog, meat byproducts ...... 0 .10 (1-methylethyl)-5-oxo- 1H-imidazol-2- Horse, meat byproducts ...... 0 .10 yl]-5-ethyl-3-pyridine carboxylic acid, Sheep, meat byproducts ...... 0 .10

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(b) Section 18 emergency exemptions. Commodity Parts per [Reserved] million (c) Tolerances with regional registra- Fruit, stone, group 12 ...... 1 .0 tions. Tolerances with regional reg- Goat, fat ...... 0 .05 istration, as defined in § 180.1(l) of this Goat, meat byproducts ...... 0 .5 chapter, are established for the sum of Grain, aspirated fractions ...... 5 residues of the herbicide imazethapyr, Hog, fat ...... 0 .02 Hog, meat byproducts ...... 0 .05 2- [4,5-dihydro-4-methyl-4-(1- Hop, dried cones ...... 2 .0 methylethyl)-5-oxo-1H-imidazol-2-yl]-5- Horse, fat ...... 0 .05 ethyl- 3-pyridine carboxylic acid, as its Horse, meat byproducts ...... 0 .5 ammonium salt, and its metabolite, 2- Milk ...... 0.05 [4,5-dihydro-4-methyl-4-(1- Nut, tree, group 14 ...... 0 .30 methylethyl)-5-oxo-1H-imidazol-2-yl]-5- Pepper/eggplant subgroup 8–10B ...... 1 .5 Peppermint, tops ...... 2 .0 (1- hydroxyethyl)-3-pyridine carboxylic Pistachio ...... 0.30 acid, both free and conjugated, applied Plum, prune, dried ...... 1.3 as its acid or ammonium salt, in or on Poultry, fat ...... 0.05 the following raw agricultural com- Poultry, meat byproducts ...... 0.05 modities: Sheep, fat ...... 0 .05 Sheep, meat byproducts ...... 0 .5 Spearmint, tops ...... 2 .0 Commodity Parts per million Tomato ...... 0.50

Endive ...... 0.1 Lettuce, head ...... 0.1 (b) Section 18 emergency exemptions. Lettuce, leaf ...... 0 .1 Time-limited tolerances are established for residues of hexythiazox, in- (d) Indirect or inadvertent residues. cluding its metabolites and degradates, [Reserved] in connection with use of the pesticide [67 FR 55331, Aug. 29, 2002, as amended at 68 under section 18 emergency exemptions FR 13849, Mar. 21, 2003; 71 FR 6359, Feb. 8, granted by EPA. Compliance with the 2006; 76 FR 34885, June 15, 2011] tolerance levels specified below is to be determined by measuring only § 180.448 Hexythiazox; tolerance for hexythiazox and its metabolites con- residues. taining the (4-chlorophenyl)-4-methyl- (a) General. Tolerances are estab- 2-oxo-3-thiazolidine moiety, calculated lished for residues of hexythiazox, in- as the stoichiometric equivalent of cluding its metabolites and degradates, hexythiazox. These tolerances will ex- in or on the commodities in the table pire and are revoked on the dates speci- below. Compliance with the tolerance fied in the following table: levels specified below is to be determined by measuring only hexythiazox Expiration/ Commodity Parts per revocation and its metabolites containing the (4- million date chlorophenyl)-4-methyl-2-oxo-3- thiazolidine moiety, calculated as the Corn, sweet, plus cobs with husks removed (K+CWHR) ...... 0.02 12/31/12 stoichiometric equivalent of Corn, sweet, forage ...... 6.0 12/31/12 hexythiazox. Corn, sweet, stover ...... 2.5 12/31/12

Parts per Commodity million (c) Tolerances with regional registrations. Tolerances with regional reg- Almond, hulls ...... 10 istrations as defined by § 180.1(l), are es- Apple, wet pomace ...... 0 .40 Berry, low growing, subgroup 13–07G ...... 6 tablished for residues of hexythiazox, Caneberry subgroup 13–07A ...... 1 including its metabolites and Cattle, fat ...... 0.05 degradates, in or on the commodities Cattle, meat byproducts ...... 0.5 Citrus, dried pulp ...... 0 .60 in the table below. Compliance with Citrus, oil ...... 24 the tolerance levels specified below is Corn, field, forage ...... 3 .0 to be determined by measuring only Corn, field, grain ...... 0 .02 Corn, field, stover ...... 7 .0 hexythiazox and its metabolites con- Date, dried fruit ...... 1 .0 taining the (4-chlorophenyl)-4-methyl- Egg ...... 0 .05 2-oxo-3-thiazolidine moiety, calculated Fruit, pome, group 11–10 ...... 0 .4 Fruit, small, vine climbing, subgroup 13–07F, as the stoichiometric equivalent of except fuzzy kiwifruit ...... 1 hexythiazox.

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Parts per Parts per Commodity million Commodity million

Alfalfa, forage (EPA Regions 9–11 only) ...... 15 Citrus ...... 0 .02 Alfalfa, hay (EPA Regions 9–11 only) ...... 30 Cotton, gin byproducts ...... 1 .0 Bean, dried, seed (EPA Regions 7–12 only) ...... 0 .4 Cotton, undelinted seed ...... 0 .02 Bean, succulent (EPA Regions 7–12 only) ...... 0.3 Food products in food handling establishments Corn, field, forage ...... 6 .0 (other than those already covered by higher Corn, field, grain ...... 0 .02 tolerances as a result of use on growing Corn, field, stover ...... 2 .5 crops, and other than those already covered Corn, sweet, forage (EPA Regions 7–12 only) ... 4 .0 by tolerances on milk, meat, and meat by- Corn, sweet, kernel plus cob with husks re- products) ...... 0.01 moved (EPA Regions 7–12 only) ...... 0 .1 Fruit, stone, group 12 ...... 0 .09 Cotton, gin byproducts, CA and AZ only ...... 3 .0 Goat, fat ...... 0 .01 Cotton, undelinted seed, CA and AZ only ...... 0 .20 Goat, meat ...... 0.02 Fruit, citrus group 10 (CA, AZ, TX only) ...... 0 .35 Goat, meat byproducts ...... 0 .02 Potato ...... 0 .02 Grape ...... 0 .02 Sorghum, grain, forage (EPA Regions 6–8 only) 5 Herb subgroup 19A, except chive ...... 0 .030 Sorghum, grain, grain (EPA Regions 6–8 only) .. 3 Hog, fat ...... 0 .01 Sorghum, grain, stover (EPA Regions 6–8 only) 6 Hog, meat ...... 0 .02 Timothy, forage (EPA Regions 9–11 only) ...... 40 Hog, meat byproducts ...... 0 .02 Timothy, hay (EPA Regions 9–11 only) ...... 40 Hop, dried cones ...... 0 .20 Horse, fat ...... 0 .01 (d) Indirect or inadvertent residues. Horse, meat ...... 0 .02 [Reserved] Horse, meat byproducts ...... 0 .02 Milk ...... 0.005 [54 FR 17948, Apr. 26, 1989] Nut, tree, group 14 ...... 0 .01 Onion, bulb, subgroup 3–07A ...... 0 .01 EDITORIAL NOTE: For FEDERAL REGISTER ci- Pear ...... 0 .02 tations affecting § 180.448, see the List of CFR Peppermint, tops ...... 0 .010 Sections Affected, which appears in the Pistachio ...... 0.01 Finding Aids section of the printed volume Plum, prune, dried ...... 0.025 and at www.fdsys.gov. Poultry, meat ...... 0 .02 Poultry, meat byproducts ...... 0.02 § 180.449 Avermectin B and its delta- Sheep, fat ...... 0 .01 1 Sheep, meat ...... 0.02 8,9-isomer; tolerances for residues. Sheep, meat byproducts ...... 0 .02 (a) General. Tolerances are estab- Spearmint, tops ...... 0 .010 lished for residues of abamectin, in- Strawberry ...... 0 .05 Vegetable, cucurbit, group 9 ...... 0.005 cluding its metabolites and degradates, Vegetable, fruiting, group 8 ...... 0.020 in or on the commodities in the fol- Vegetable, leafy, except brassica, group 4 ...... 0 .10 lowing table. Compliance with the tol- Vegetable, tuberous and corm, subgroup 01C 0 .01 erance levels specified in the following table is to be determined by measuring (b) Section 18 emergency exemptions. only avermectin B1 a mixture of [Reserved] avermectins containing greater than or (c) Tolerances with regional registra- equal to 80% avermectin B1 a (5-O- tions. [Reserved] demethyl avermectin A1) and less than (d) Indirect or inadvertent residues. or equal to 20% avermectin B1b (5-O- [Reserved] demethyl-25-de(1-methylpropyl)-25-(1- [62 FR 44095, Aug. 19, 1997] methylethyl) avermectin A1) and its EDITORIAL NOTE: For FEDERAL REGISTER ci- delta-8,9-isomer in or on the following tations affecting § 180.449, see the List of CFR commodities: Sections Affected, which appears in the Finding Aids section of the printed volume Parts per Commodity million and at www.fdsys.gov. Almond, hulls ...... 0 .10 § 180.450 Beta-(4-Chlorophenoxy)- Apple ...... 0.020 alpha-(1,1-dimethylethyl)-1H-1,2,4- Apple, wet pomace ...... 0 .10 triazole-1-ethanol; tolerances for Avocado ...... 0 .020 Bean, dry, seed ...... 0 .01 residues. Cattle, fat ...... 0.03 (a) General. Tolerances are estab- Cattle, meat ...... 0 .02 Cattle, meat byproducts ...... 0.06 lished for the combined residues of the Celeriac, roots ...... 0 .05 fungicide b-(4-chlorophenoxy)-a-(1,1- Celeriac, tops ...... 0 .05 dimethylethyl)-1H-1,2,4-triazole-1-eth- Chive, dried leaves ...... 0 .02 anol (triadimenol) and its butanediol Chive, fresh leaves ...... 0 .01 Citrus, dried pulp ...... 0 .10 metabolite, 4-(4-chlorophenoxy)-2,2-di- Citrus, oil ...... 0.10 methyl-4-(1H-1,2,4-triazol-l-yl)-1,3-

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butanediol, calculated as triadimenol, Commodity Parts per in or on the following commodities: million Flax, seed ...... 0 .02 Expiration/ Commodity Parts per Revocation Grain, aspirated fractions ...... 1 .5 million Date Oat, forage ...... 0 .05 Oat, grain ...... 0 .05 Banana 1 ...... 0.2 None Oat, hay ...... 0.05 Barley, grain ...... 0.05 None Oat, straw ...... 0.10 Barley, straw ...... 0.2 None Rice, grain ...... 0 .05 Corn, field, forage ...... 0.05 None Rice, straw ...... 0 .05 Corn, field, grain ...... 0.05 None Sorghum, grain, forage ...... 0.05 Corn, field, stover ...... 0.05 None Sorghum, grain, grain ...... 0 .05 Corn, pop, grain ...... 0.05 None Sorghum, grain, stover ...... 0 .05 Corn, pop, stover ...... 0.05 None Soybean, forage ...... 0 .07 Corn, sweet, forage ...... 0.05 None Soybean, hay ...... 0 .35 Corn, sweet, kernel plus cob with Soybean, hulls ...... 0 .04 husks removed ...... 0.05 None Soybean, seed ...... 0 .01 Corn, sweet, stover ...... 0.05 None Sunflower, seed ...... 0.05 Cotton, undelinted seed ...... 0.02 None Wheat, forage ...... 0 .3 Oat, forage ...... 2.5 None Wheat, grain ...... 0 .05 Oat, grain ...... 0.05 None Wheat, hay ...... 0 .5 Oat, straw ...... 0.2 None Wheat, straw ...... 0 .10 Rye, forage ...... 2.5 None Rye, grain ...... 0.05 None (b) Section 18 emergency exemptions. Rye, straw ...... 0.1 None Wheat, forage ...... 2.5 None [Reserved] Wheat, grain ...... 0.05 None (c) Tolerances with regional registra- Wheat, straw ...... 0.2 None tions. Tolerances with regional reg- 1 There are no U.S. registrations for banana (whole) as of istration, as defined in § 180.1(l) are es- September 22, 1993. tablished for residues of the herbicide (b) Section 18 emergency exemptions. tribenuron methyl (methyl-2-[[[[N-(4- [Reserved] methoxy-6-methyl-1,3,5-triazin-2-yl) (c) Tolerances with regional registra- methylamino] car- tions. [Reserved] bonyl]amino]sulfonyl] benzoate) in or (d) Indirect or inadvertent residues. on the following raw agricultural com- [Reserved] modities:

[73 FR 54962, Sept. 24, 2008, as amended at 74 Commodity Parts per FR 47457, Sept. 16, 2009; 76 FR 34885, June 15, million 2011] Grass, forage, fodder and hay, group 17, except bermudagrass; forage ...... 0 .10 § 180.451 Tribenuron methyl; toler- Grass, forage, fodder and hay, group 17, ex- ances for residues. cept bermudagrass; hay ...... 0 .10 (a) General. Tolerances are estab- (d) Indirect or inadvertent residues. lished for residues of the herbicide [Reserved] tribenuron methyl and its metabolites and degradates in or on the commod- [69 FR 56718, Sept. 22, 2004, as amended at 72 ities in the following table. Compliance FR 11789, Mar. 14, 2007; 73 FR 47065, Aug. 13, with the tolerance levels specified 2008; 74 FR 67128, Dec. 18, 2009; 76 FR 34885, below is to be determined by measuring June 15, 2011] only tribenuron methyl, methyl-2- § 180.452 Primisulfuron-methyl; toler- [[[[N-(4-methoxy-6-methyl-1,3,5-triazin- ances for residues. 2-yl) methylamino] carbonyl] amino] sulfonyl] benzoate, in or on the fol- (a) General. Tolerances are estab- lowing commodities: lished for residues of primisulfuron- methyl (3-[4,6-bis-(difluoromethoxy)- Commodity Parts per pyrimidin-2-yl]-1-(2- million methoxycarbonylphenylsulfonyl) urea) Barley, grain ...... 0 .05 in or on the following raw agricultural Barley, hay ...... 0 .4 commodities. Barley, straw ...... 0 .10 Canola, seed ...... 0 .02 Parts per Corn, field, forage ...... 0 .15 Commodity million Corn, field, grain ...... 0 .01 Corn, field, stover ...... 1 .1 Cattle, fat ...... 0.10 Cotton, gin byproducts ...... 0 .02 Cattle, meat ...... 0 .10 Cotton, undelinted seed ...... 0 .02 Cattle, meat byproducts ...... 0.10

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Parts per Parts per Commodity million Commodity million

Corn, field, forage ...... 0 .10 Goat, meat ...... 0.01 Corn, field, grain ...... 0 .02 Goat, meat byproducts ...... 0 .05 Corn, field, stover ...... 0 .10 Grass, forage ...... 9 .0 Corn, pop, grain ...... 0.02 Grass, hay ...... 25 .0 Corn, pop, stover ...... 0.10 Horse, fat ...... 0 .01 Egg ...... 0 .10 Horse, meat ...... 0 .01 Goat, fat ...... 0 .10 Horse, meat byproducts ...... 0 .05 Goat, meat ...... 0.10 Milk ...... 0.01 Goat, meat byproducts ...... 0 .10 Sheep, fat ...... 0 .01 Hog, fat ...... 0 .10 Sheep, meat ...... 0.01 Hog, meat ...... 0 .10 Sheep, meat byproducts ...... 0 .05 Hog, meat byproducts ...... 0 .10 Horse, fat ...... 0 .10 (b) Section 18 emergency exemptions. Horse, meat ...... 0 .10 Horse, meat byproducts ...... 0 .10 Time-limited tolerances specified in Milk ...... 0.02 the following table [below] are estab- Poultry, fat ...... 0.10 lished for residues of the herbicide Poultry, meat ...... 0 .10 Poultry, meat byproducts ...... 0.10 nicosulfuron, 3-Pyridinecarboxamide, Sheep, fat ...... 0 .10 2-[[[[(4,6-dimethoxy-2- Sheep, meat ...... 0.10 pyrimidinyl)amino] car- Sheep, meat byproducts ...... 0 .10 bonyl]amino]sulfonyl]-N,N-dimethyl-, in or on the specified agricultural com- (b) Section 18 emergency exemptions. modities, resulting from use of the pes- [Reserved] ticide pursuant to FFIFRA section 18 (c) Tolerances with regional registra- emergency exemptions. The tolerances tions. [Reserved] expire and are revoked on the date (d) Indirect or inadvertent residues. specified in the table. [Reserved] [55 FR 21548, May 25, 1990, as amended at 62 Expiration/ Commodity Parts per Revokation FR 66020, Dec. 17, 1997; 63 FR 66458, Dec. 2, million Date 1998; 67 FR 35049, May 17, 2002; 74 FR 46375, Sept. 9, 2009; 74 FR 46699, Sept. 11, 2009; 77 FR Bermuda grass, forage ...... 10 12/31/11 59128, Sept. 26, 2012] Bermuda grass, hay ...... 25 12/31/11

§ 180.454 Nicosulfuron; tolerances for (c) Tolerances with regional registra- residues. tions. [Reserved] (d) Indirect or inadvertent residues. (a) General. Tolerances are estab- [Reserved] lished for residues of the herbicide nicosulfuron, including its metabolites [75 FR 17578, Apr. 7, 2010] and degradates, in or on the commodities in the following table [below]. § 180.455 Procymidone; tolerances for Compliance with the tolerance levels residues. specified in the following table [below] A tolerance is established for the res- is to be determined by measuring only idues of the fungicide procymidone, N- nicosulfuron, 3-Pyridinecarboxamide, (3,5-dichlorophenyl)-1,2- 2-[[[[(4,6-dimethoxy-2- dimethylcyclopropane-1,2 pyrimidinyl)amino] car- dicarboximide, in or on the following bonyl]amino]sulfonyl]-N,N-dimethyl-. raw agricultural commodity:

Parts per Commodity Parts per Commodity million million

Cattle, fat ...... 0.01 Grape, wine ...... 5 .0 Cattle, meat ...... 0 .01 Cattle, meat byproducts ...... 0.05 Corn, field, forage ...... 0 .1 [59 FR 42514, Aug. 18, 1994] Corn, field, grain ...... 0 .1 Corn, field, stover ...... 0 .1 § 180.457 Bitertanol; tolerances for res- Corn, pop, grain ...... 0.1 idues. Corn, pop, stover ...... 0.1 Corn, sweet, forage ...... 0 .1 (a) General. A tolerance is established Corn, sweet, kernel plus cob with husks re- for the residues of the fungicide moved ...... 0 .1 ′ Corn, sweet, stover ...... 0 .1 bitertanol, b-([1,1 -biphenyl]-4-yloxy)-a- Goat, fat ...... 0 .01 (1,1-dimethylethyl)-1H-1,2,4-triazole-1-

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ethanol, in or on the following raw ag- Commodity Parts per ricultural commodity: million Cranberry ...... 0 .50 Parts per Commodity million Egg ...... 0 .2 Flax, meal ...... 1 .0 Banana 1 ...... 0.5 Flax, seed ...... 0 .6 Goat, fat ...... 0 .2 1 There are no U.S. registrations as of April 1, 1992. Goat, meat ...... 0.2 Goat, meat byproducts ...... 0 .2 (b) Section 18 emergency exemptions. Herb subgroup 19A ...... 12.0 [Reserved] Hog, fat ...... 0 .2 (c) Tolerances with regional registra- Hog, meat ...... 0 .2 Hog, meat byproducts ...... 0 .2 tions. [Reserved] Hop, dried cones ...... 0 .5 (d) Indirect or inadvertent residues. Horse, fat ...... 0 .2 [Reserved] Horse, meat ...... 0 .2 Horse, meat byproducts ...... 0 .2 [74 FR 47457, Sept. 16, 2009] Leaf petioles subgroup 4B ...... 0 .60 Leafy greens subgroup 4A ...... 2 .0 § 180.458 Clethodim; tolerances for res- Melon subgroup 9A ...... 2 .0 idues. Milk ...... 0.05 Mustard, seed ...... 0 .50 (a) General. Tolerances are estab- Onion, bulb ...... 0 .20 lished for residues of the herbicide Onion, green ...... 2 .0 Peach ...... 0 .20 clethodim, including its metabolites Peanut ...... 3 .0 and degradates, in or on the commod- Peanut, hay ...... 3.0 ities in the table in this paragraph. Peanut, meal ...... 5 .0 Peppermint, tops ...... 5 .0 Compliance with the tolerance levels Potato ...... 0 .5 specified in this paragraph is to be de- Potato, granules/flakes ...... 2 .0 termined by measuring only the sum of Poultry, fat ...... 0.2 Poultry, meat ...... 0 .2 clethodim, 2-[(1E)-1-[[[(2E)-3-chloro-2- Poultry, meat byproducts ...... 0.2 propenyl]oxy]imino]propyl]-5-[2- Radish, tops ...... 0 .70 (ethylthio)propyl]-3-hydroxy-2-cyclo- Safflower, meal ...... 10.0 hexen-1-one, and its metabolites con- Safflower, seed ...... 5 .0 Sesame, seed ...... 0 .35 taining the 5-(2- Sheep, fat ...... 0 .2 ethylthiopropyl)cyclohexene-3-one and Sheep, meat ...... 0.2 5-(2-ethylthiopropyl)-5- Sheep, meat byproducts ...... 0 .2 Soybean ...... 10.0 hydroxycyclohexene-3-one moieties Spearmint, tops ...... 5 .0 and their sulphoxides and sulphones, Squash/cucumber subgroup 9B ...... 0.50 calculated as the stoichiometric equiv- Strawberry ...... 3 .0 alent of clethodim, in or on the com- Sunflower, meal ...... 10 .0 Sunflower, seed ...... 5.0 modity. Turnip, greens ...... 3.0 Vegetable, fruiting group 8 ...... 1 .0 Commodity Parts per Vegetable, legume, group 6, except soybean .... 3 .5 million Vegetable, root, except sugar beet, subgroup 1B ...... 1 .0 Alfalfa, forage ...... 6.0 Vegetable, tuberous and corm, subgroup 1C ..... 1.0 Alfalfa, hay ...... 10 Artichoke, globe ...... 1.2 Asparagus ...... 1.7 (b) Section 18 emergency exemptions. Bean, dry, seed ...... 2 .5 [Reserved] Beet, sugar, molasses ...... 1 .0 Beet, sugar, roots ...... 0 .20 (c) Tolerances with regional registra- Beet, sugar, tops ...... 1.0 tions. [Reserved] Brassica, head and stem, subgroup 5A ...... 3 .0 (d) Indirect or inadvertent residues. Brassica, leafy greens, subgroup 5B ...... 3 .0 [Reserved] Bushberry subgroup 13–07B ...... 0 .20 Caneberry subgroup 13–07A ...... 0.30 [76 FR 23496, Apr. 27, 2011, as amended at 77 Canola, meal ...... 1 .0 Canola, seed ...... 0 .50 FR 59128, Sept. 26, 2012] Cattle, fat ...... 0.2 Cattle, meat ...... 0 .2 § 180.459 Triasulfuron; tolerances for Cattle, meat byproducts ...... 0.2 residues. Clover, forage ...... 10.0 Clover, hay ...... 20.0 (a) General. Tolerances are estab- Corn, field, forage ...... 0 .2 lished for residues of the herbicide Corn, field, grain ...... 0 .2 triasulfuron [3-(6-methoxy-4-methyl- Corn, field, stover ...... 0 .2 Cotton, meal ...... 2 .0 1,3,5-triazin-2-yl)-1-(2-(2- Cotton, undelinted seed ...... 1 .0 chloroethoxy)phenylsulfonyl)urea] in

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or on the following raw agricultural § 180.461 Cadusafos; tolerances for res- commodities: idues.

Parts per A tolerance is established for the res- Commodity million idues of the nematicide/insecticide cadusafos, O-ethyl S,S-di-sec-butyl Barley, grain ...... 0 .02 Barley, straw ...... 2 .0 phosphorodithioate, in or on the fol- Cattle, fat ...... 0.1 lowing raw agricultural commodity: Cattle, kidney ...... 0 .5 Cattle, meat byproducts, except kidney ...... 0.1 Commodity Parts per Cattle, meat ...... 0 .1 million Goat, fat ...... 0 .1 Goat, kidney ...... 0 .5 Banana ...... 0.01 Goat, meat byproducts, except kidney ...... 0 .1 Goat, meat ...... 0.1 Grass, forage ...... 7 .0 There are no U.S. registrations as of Grass, hay ...... 2 .0 May 10, 1994, for the nematicide/ Hog, fat ...... 0 .1 insecticid cadusafos. Hog, kidney ...... 0.5 Hog, meat byproducts ...... 0 .1 [59 FR 39467, Aug. 3, 1994] Hog, meat ...... 0 .1 Horse, fat ...... 0 .1 § 180.462 Pyridate; tolerances for resi- Horse, kidney ...... 0 .5 dues. Horse, meat byproducts, except kidney ...... 0 .1 Horse, meat ...... 0 .1 (a) General. Tolerances are estab- Milk ...... 0.02 lished for residues of the herbicide Sheep, fat ...... 0 .1 pyridate, including its metabolites and Sheep, kidney ...... 0.5 Sheep, meat byproducts, except kidney ...... 0 .1 degradates, in or on the commodities Sheep, meat ...... 0.1 in the table in this paragraph. Compli- Wheat, forage ...... 5 .0 ance with the tolerance levels specified Wheat, grain ...... 0 .02 Wheat, straw ...... 2 .0 in this paragraph is to be determined by measuring only the sum of pyridate, (b) Section 18 emergency exemptions. O-(6-chloro-3-phenyl-4-pyridazinyl)-S- [Reserved] octyl-carbonothioate, and its metabo- (c) Tolerances with regional registra- lites, 6-chloro-3-phenyl-pyridazine-4-ol tions. [Reserved] and conjugates of 6-chloro-3-phenyl-py- (d) Indirect or inadvertent residues. ridazine-4-ol, calculated as the stoi- [Reserved] chiometric equivalent of pyridate, in or on the commodity. [60 FR 36731, July 18, 1995, as amended at 63 FR 44152, Aug. 18, 1998; 63 FR 66449, Dec. 2, Commodity Parts per 1998] million Brassica, head and stem, subgroup 5A ...... 0 .03 § 180.460 Benoxacor; tolerances for Cabbage ...... 0 .03 residues. Chickpea, seed ...... 0 .1 Collards ...... 0.03 (a) General. Tolerances are estab- Corn, field, forage ...... 0 .03 lished for residues of the inert ingre- Corn, field, grain ...... 0 .03 dient (safener) benoxacor (4- Corn, field, stover ...... 0 .03 Corn, pop, grain ...... 0.03 (dichloroacetyl)-3,4-dihydro-3-methyl- Corn, pop, stover ...... 0.03 2H-1, 4-benzoxazine) at 0.01 parts per Peanut ...... 0 .03 million (ppm) when used in pesticide Peppermint, tops ...... 0 .20 formulations containing metolachlor Spearmint, tops ...... 0 .20 or S-metolachlor in or on raw agricul- (b) Section 18 emergency exemptions. tural commodities for which tolerances [Reserved] have been established for metolachlor (c) Tolerances with regional registra- or S-metolachlor. tions. [Reserved] (b) Section 18 energency exemptions. (d) Indirect or inadvertent residues. [Reserved] [Reserved] (c) Tolerances with regional registrations. [Reserved] [57 FR 54303, Nov. 18, 1992, as amended at 62 (d) Indirect or inadvertent residues. FR 44558, Aug. 22, 1997; 63 FR 53844, Oct. 7, [Reserved] 1998; 64 FR 46298, Aug. 25, 1999; 65 FR 25652, May 3, 2000; 67 FR 35049, May 17, 2002; 72 FR [63 FR 7305, Feb. 13, 1998, as amended at 70 35665, June 29, 2007; 74 FR 46376, Sept. 9, 2009; FR 21631, Apr. 27, 2005] 76 FR 23496, Apr. 27, 2011]

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§ 180.463 Quinclorac; tolerances for OMMODITY residues. Parts per (a)(1) General. Tolerances are estab- Commodity million lished for residues of the herbicide Rapeseed, subgroup 20A 1 ...... 1.5 quinclorac, including its metabolites and degradates, in or on the commod- 1 There are no U.S. Registrations. ities in the table in this paragraph. (b) Section 18 emergency exemptions. Compliance with the tolerance levels Time-limited tolerances are estab- specified in this paragraph is to be de- lished for residues of the herbicide termined by measuring only quinclorac, including its metabolites quinclorac, 3,7-dichloro-8- and degradates, in or on the com- quinolinecarboxylic acid, in or on the modity in the table in this paragraph. commodity. Compliance with the tolerance level specified in this paragraph is to be de- Parts per Commodity million termined by measuring only quinclorac, 3,7-dichloro-8- Barley, grain ...... 2 .0 quinolinecarboxylic acid, in or on the Berry, low growing, except strawberry, subgroup 13–07H ...... 1.5 commodity. The tolerance expires and Cattle, fat ...... 0.7 is revoked on the date specified in the Cattle, meat byproducts ...... 1.5 table in this paragraph. Cattle, meat ...... 0 .05 Egg ...... 0 .05 Expiration/ Goat, fat ...... 0 .7 Commodity Parts per revocation Goat, meat byproducts ...... 1 .5 million date Goat, meat ...... 0.05 Grain, aspirated fractions ...... 1200 Cranberry ...... 15.0 12/31/12 Grass, forage ...... 150 Grass, hay ...... 130 Hog, fat ...... 0 .7 (c) Tolerances with regional registra- Hog, meat byproducts ...... 1 .5 tions. [Reserved] Hog, meat ...... 0 .05 (d) Indirect or inadvertent residues. Horse, fat ...... 0 .7 Horse, meat byproducts ...... 1 .5 [Reserved] Horse, meat ...... 0 .05 Milk ...... 0.05 [57 FR 47996, Oct. 21, 1992, as amended at 64 Poultry, fat ...... 0.05 FR 6548, 6549, Feb. 10, 1999; 64 FR 14632, Mar. Poultry, meat byproducts ...... 0.1 26, 1999; 65 FR 33701, May 24, 2000; 67 FR 35049, Poultry, meat ...... 0 .05 May 17, 2002; 72 FR 55073, Sept. 28, 2007; 74 FR Rhubarb ...... 0 .5 51490, Oct. 7, 2009; 74 FR 67090, Dec. 18, 2009; Rice, bran ...... 15.0 76 FR 23497, Apr. 27, 2011; 77 FR 75566, Dec. 21, Rice, grain ...... 5 .0 Rice, straw ...... 12 .0 2012; 78 FR 71528, Nov. 29, 2013] Sheep, fat ...... 0 .7 Sheep, meat byproducts ...... 1 .5 § 180.464 Dimethenamid; tolerances for Sheep, meat ...... 0.05 residues. Sorghum, grain, forage ...... 3.0 Sorghum, grain, grain ...... 6 .0 (a) General. Tolerances are estab- Sorghum, grain, stover ...... 1 .0 lished for residues of the herbicide Wheat, forage ...... 1 .0 dimethenamid, 1(R,S)-2-chloro-N-[(1- Wheat, germ ...... 0 .75 Wheat, grain ...... 0 .5 methyl-2-methoxy)ethyl]-N-(2,4- Wheat, hay ...... 0 .5 dimethylthien-3-yl)-acetamide, applied Wheat, straw ...... 0 .1 as either the 90:10 or 50:50 S:R isomers, in or on the following food commod- (2) Tolerances are established for res- ities: idues of the herbicide quinclorac, including its metabolites and degradates, Commodity Parts per in or on the commodity in the fol- million lowing table. Compliance with the tol- Bean, dry, seed ...... 0 .01 erance levels specified in this para- Beet, garden, roots ...... 0 .01 graph is to be determined by measuring Beet, garden, tops ...... 0 .01 Beet, sugar, dried pulp ...... 0 .01 only quinclorac, 3,7-dichloro-8- Beet, sugar, molasses ...... 0 .01 quinolinecarboxylic acid, and its meth- Beet, sugar, roots ...... 0 .01 yl ester, methyl-3,7-dichloro-8- Beet, sugar, tops ...... 0.01 quinolinecarboxylate, calculated as the Corn, field, forage ...... 0 .01 Corn, field, grain ...... 0 .01 stoichiometric equivalent of Corn, field, stover ...... 0 .01 quinclorac, in or on the commodity. Corn, pop, forage ...... 0 .01

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3) when used as an inert ingredient Commodity Parts per million (safener) in or on the following raw ag- Corn, pop, grain ...... 0.01 ricultural commodities: Corn, pop, stover ...... 0.01 Parts per mil- Corn, sweet, forage ...... 0 .01 Commodity 1 Corn, sweet, kernel plus cob with husks re- lion moved ...... 0 .01 Corn, sweet, stover ...... 0 .01 Corn, field, forage ...... 0.005 Corn, field, grain ...... 0.005 Garlic ...... 0 .01 Corn, field, stover ...... 0.005 Grass, forage ...... 0 .15 Corn, pop, grain ...... 0.005 Grass, hay ...... 2 .5 Corn, pop, stover ...... 0.005 Grass, seed screenings ...... 0 .01 Grass, straw ...... 0 .01 1There are no U.S. registered products containing 4- Hop, dried cones ...... 0 .05 (dichloroacetyl)-1-oxa-4-azaspiro[4.5]decane as of June 17, Horseradish ...... 0.01 2002. Leek ...... 0 .01 Onion, bulb ...... 0 .01 (b) Section 18 emergency exemptions. Onion, green ...... 0 .01 [Reserved] Onion, Welsh ...... 0 .01 (c) Tolerances with regional registra- Peanut ...... 0 .01 tions. [Reserved] Peanut, hay ...... 0.01 Radish, roots ...... 0 .01 (d) Indirect or inadvertent residues. Radish, tops ...... 0 .01 [Reserved] Rutabaga, roots ...... 0 .01 Rutabaga, tops ...... 0 .1 [68 FR 4392, Jan. 29, 2003] Shallot, bulb ...... 0 .01 Shallot, fresh leaves ...... 0 .01 § 180.466 Fenpropathrin; tolerances for Sorghum, grain, forage ...... 0.01 residues. Sorghum, grain, grain ...... 0 .01 Sorghum, grain, stover ...... 0 .01 (a) General. Tolerances are estab- Soybean, seed ...... 0 .01 lished for residues of fenpropathrin, in- Turnip, greens ...... 0.1 Turnip, roots ...... 0 .01 cluding its metabolites and degradates, Turnip, tops ...... 0.1 in or on the commodities in the fol- Vegetable, tuberous and corm, subgroup 1C ... 0.01 lowing table. Compliance with the tolerance levels specified below is to be (b) Section 18 emergency exemptions. determined by measuring only [Reserved] fenpropathrin (alpha-cyano-3-phenoxy- (c) Tolerances with regional registra- benzyl 2,2,3,3 tions. Tolerances with regional reg- tetramethylcyclopropanecarboxylate). istration are established for residues of dimethenamid, 1 (R,S)-2-chloro-N-[(1- Commodity Parts per methyl-2-methoxy) ethyl]-N-(2,4- million dimethylthien-3-yl)-acetamide) in or Acerola ...... 3.0 on the following raw agricultural com- Almond, hulls ...... 4 .5 modities: Atemoya ...... 1 .5 Avocado ...... 1 .0 Barley, grain ...... 0 .04 Parts per Barley, hay ...... 3 .0 Commodity million Barley, straw ...... 2 .0 Pumpkin ...... 0.01 Berry, low growing, subgroup 13–07G ...... 2 .0 Squash, winter ...... 0 .01 Biriba ...... 1 .5 Brassica, head and stem, subgroup 5A ...... 3 .0 Bushberry subgroup 13–07B ...... 3 .0 (d) Indirect or inadvertent residues. Caneberry subgroup 13-07A ...... 12 [Reserved] Canistel ...... 1 .0 Cattle, fat ...... 1.0 [65 FR 51551, Aug. 24, 2000, as amended at 67 Cattle, meat byproducts ...... 0.1 FR 46884, July 17, 2002; 69 FR 29459, May 24, Cattle, meat ...... 0 .1 2004; 69 FR 57207, Sept. 24, 2004; 70 FR 24712, Cherimoya ...... 1 .5 May 11, 2005; 71 FR 25942, May 3, 2006; 71 FR Cherry, sweet ...... 5 .0 Cherry, tart ...... 5 .0 49354, Aug. 23, 2006; 72 FR 44388, Aug. 8, 2007; Citrus, dried pulp ...... 4 .0 72 FR 73630, Dec. 28, 2007] Citrus, oil ...... 75 Cotton, refined oil ...... 3.0 § 180.465 4-(Dichloroacetyl)-1-oxa-4- Cotton, undelinted seed ...... 1 .0 azaspiro[4.5]decane. Custard apple ...... 1 .5 Egg ...... 0 .05 (a) General. Tolerances are estab- Feijoa ...... 3 .0 lished for the residues of 4- Fruit, citrus, group 10–10 ...... 2 .0 Fruit, pome, group 11–10 ...... 5 .0 (dichloroacetyl)-1-oxa-4- Fruit, small vine climbing, except fuzzy azaspiro[4.5]decane, (CAS No. 71526–07– kiwifruit, subgroup 13–07F ...... 5.0

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carbon disulfide, from the application Commodity Parts per million of sodium tetrathiocarbonate, in or on Fruit, stone, crop group 12, except cherry ...... 1 .4 the following raw agricultural com- Goat, fat ...... 1 .0 modities: Goat, meat byproducts ...... 0 .1 Goat, meat ...... 0.1 Parts per Grape, raisin ...... 10.0 Commodity million Guava ...... 3 .0 Hog, fat ...... 1 .0 Almond ...... 0.1 Hog, meat byproducts ...... 0 .1 Almond, hulls ...... 0 .1 Hog, meat ...... 0 .1 Grape ...... 0 .1 Horse, fat ...... 1 .0 Grapefruit ...... 0 .1 Horse, meat byproducts ...... 0 .1 Lemon ...... 0.1 Horse, meat ...... 0 .1 Orange, sweet ...... 0 .1 Ilama ...... 1 .5 Peach ...... 0 .1 Jaboticaba ...... 3 .0 Plum, prune, fresh ...... 0.1 Longan ...... 7 .0 Lychee ...... 7 .0 Mango ...... 1.0 [58 FR 33771, June 21, 1993, as amended at 62 Melon subgroup 9A ...... 0 .5 FR 26949, May 16, 1997] Milk, fat (reflecting 0.08 ppm in whole milk) ..... 2 .0 Nut, tree, crop group 14 ...... 0 .10 § 180.468 Flumetsulam; tolerances for Olive ...... 5 .0 Papaya ...... 1 .0 residues. Passionfruit ...... 3 .0 (a) General. Tolerances are estab- Pea, succulent ...... 0 .02 Peanut, hay ...... 20.0 lished for residues of the herbicide Peanut ...... 0 .01 flumetsulam, including its metabolites Pistachio ...... 0.10 and degradates, in or on the commod- Poultry, fat ...... 0.05 Poultry, meat byproducts ...... 0.05 ities in the table in this paragraph. Poultry, meat ...... 0 .05 Compliance with the tolerance levels Pulasan ...... 7 .0 specified in this paragraph is to be de- Rambutan ...... 7 .0 Sapodilla ...... 1 .0 termined by measuring only Sapote, black ...... 1 .0 flumetsulam, N-(2,6-difluorophenyl)-5- Sapote, mamey ...... 1 .0 methyl-(1,2,4)-triazolo-(1,5a)-pyrimi- Sheep, fat ...... 1 .0 dine-2-sulfonamide, in or on the com- Sheep, meat byproducts ...... 0 .1 Sheep, meat ...... 0.1 modity. Soursop ...... 1 .5 Spanish lime ...... 7 .0 Commodity Parts per Squash/Cucumber subgroup 9B ...... 0 .5 million Star apple ...... 1 .0 Starfruit ...... 3 .0 Bean, dry, seed ...... 0 .05 Sugar apple ...... 1 .5 Corn, field, forage ...... 0 .05 Tea, dried 1 ...... 2 .0 Corn, field, grain ...... 0 .05 Vegetable, fruiting, group 8–10 ...... 1 .0 Corn, field, stover ...... 0 .05 Wax jambu ...... 3 .0 Soybean, seed ...... 0 .05 1 There are no U.S. registrations as of November 28, 2012, for the use of fenpropathrin on tea, dried. (b) Section 18 emergency exemptions. [Reserved] (b) Section 18 emergency exemptions. (c) Tolerances with regional registra- [Reserved] tions. [Reserved] (c) Tolerances with regional registra- (d) Indirect or inadvertent residues. tions. [Reserved] [Reserved] (d) Indirect or inadvertent residues. [Reserved] [76 FR 23497, Apr. 27, 2011] [62 FR 63034, Nov. 26, 1997, as amended at 63 § 180.469 Dichlormid; tolerances for FR 48116, Sept. 9, 1998; 64 FR 3009, Jan. 20, residues. 1999; 65 FR 11242, Mar. 2, 2000; 65 FR 24397, (a) General. Tolerances are estab- Apr. 26, 2000; 65 FR 48620, Aug. 9, 2000; 66 FR 64774, Dec. 14, 2001; 67 FR 35049, May 17, 2002; lished for residues of dichlormid, in- 70 FR 38789, July 6, 2005; 70 FR 55747, Sept. 23, cluding its metabolites and degradates, 2005; 74 FR 12606, Mar. 25, 2009; 77 FR 70908, when used as an inert ingredient (her- Nov. 28, 2012; 78 FR 69569, Nov. 20, 2013] bicide safener) in pesticide formulations, in or on the commodities in the § 180.467 Carbon disulfide; tolerances following table. Compliance with the for residues. tolerances is to be determined by meas- Tolerances are established for the uring only dichlormid (2,2-dichloro- nematicide, insecticide, and fungicide N,N-di-2-propenylacetamide).

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Parts per Parts per Commodity million Commodity million

Corn, field, forage ...... 0 .05 Sorghum, grain, forage ...... 1.6 Corn, field, grain ...... 0 .05 Sorghum, grain, grain ...... 0 .05 Corn, field, stover ...... 0 .05 Sorghum, grain, stover ...... 1 .7 Corn, pop, grain ...... 0.05 Soybean, meal ...... 1.2 Corn, pop, stover ...... 0.05 Soybean, seed ...... 1 .0 Corn, sweet, forage ...... 0 .05 Corn, sweet, kernel plus cob with husks removed ...... 0 .05 (b) Section 18 emergency exemptions. Corn, sweet, stover ...... 0 .05 [Reserved] (c) Tolerances with regional registra- (b) Section 18 emergency exemptions. tions. [Reserved] [Reserved] (d) Indirect or inadvertent residues. (c) Tolerances with regional registra- Tolerances are established for indirect tions. [Reserved] or inadvertent residues of acetochlor, (d) Indirect or inadvertent residues. including its metabolites and [Reserved] degradates, in or on the raw agricul- [65 FR 16149, Mar. 27, 2000, as amended at 67 tural commodities in the table to this FR 51105, Aug. 7, 2002; 69 FR 58290, Sept. 30, paragraph when present therein as a 2004; 70 FR 76699, Dec. 28, 2005; 74 FR 37623, result of application of acetochlor to July 29, 2009; 76 FR 16310, Mar. 23, 2011] the growing crops in the table to paragraph (a) of this section. Compliance § 180.470 Acetochlor; tolerances for with the tolerance levels specified residues. below is to be determined by measuring (a) General. Tolerances are estab- only acetochlor, 2-chloro-2’-methyl-6- lished for residues of acetochlor, in- ethyl-N-ethoxymethylacetanilide, and cluding its metabolites and degradates, its metabolites containing the ethyl in or on the commodities in the table methyl aniline (EMA) moiety and the below. Compliance with the tolerance hydroxyethyl methyl aniline (HEMA) levels specified below is to be deter- moiety. Both parent and the named mined by measuring only acetochlor, 2- metabolites shall be determined as chloro-2’-methyl-6-ethyl-N- ethyl methyl aniline (EMA) and hy- ethoxymethylacetanilide, and its me- droxyethyl methyl aniline (HEMA), tabolites containing the ethyl methyl and calculated as the stoichiometric aniline (EMA) moiety and the hydroxy- equivalents of acetochlor, in or on the ethyl methyl aniline (HEMA) moiety. following commodities. Both parent and the named metabo- Parts per lites shall be determined as ethyl Commodity million methyl aniline (EMA) and hydroxyethyl methyl aniline (HEMA), and cal- Animal feed, nongrass, group 18, forage ...... 1 .3 culated as the stoichiometric equiva- Animal feed, nongrass, group 18, hay ...... 3.5 Grain, cereal, forage, fodder and straw, group lents of acetochlor, in or on the fol- 16, except corn, grain sorghum, rice and lowing commodities: wheat, forage ...... 0 .5 Grain, cereal, forage, fodder and straw, group 16, except corn, grain sorghum, rice and Commodity Parts per million wheat, hay ...... 2 .0 Grain, cereal, forage, fodder and straw, group Beet, sugar, dried pulp ...... 0 .50 16, except corn, grain sorghum, rice and Beet, sugar, molasses ...... 0 .80 wheat, stover ...... 0 .1 Beet, sugar, roots ...... 0 .30 Grain, cereal, forage, fodder and straw, group Beet, sugar, tops ...... 0.70 16, except corn, grain sorghum, and wheat, Corn, field, forage ...... 4 .5 straw ...... 0 .3 Corn, field, grain ...... 0 .05 Grain, cereal, group 15, except corn, grain sor- Corn, field, stover ...... 2 .5 ghum, and wheat, grain ...... 0.05 Corn, pop, grain ...... 0.05 Pea and bean, dried shelled, except soybean, Corn, pop, stover ...... 2.5 subgroup 6C ...... 0 .05 Corn, sweet, forage ...... 1 .5 Potato ...... 0 .05 Corn, sweet, kernels plus cob with husks re- Soybean, forage ...... 0 .7 moved ...... 0 .05 Soybean, hay ...... 1 .0 Corn, sweet, stover ...... 1 .0 Sunflower, seed ...... 0.05 Cotton, gin byproducts ...... 4 .0 Wheat, forage ...... 0 .5 Cotton, undelinted seed ...... 0 .6 Wheat, grain ...... 0 .02 Peanut ...... 0 .20 Wheat, hay ...... 2 .0 Peanut, hay ...... 7.0 Wheat, straw ...... 0 .1 Peanut, meal ...... 0 .25

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[72 FR 27468, May 16, 2007, as amended at 74 Parts per FR 29969, June 24, 2009; 74 FR 47450, Sept. 16, Commodity million 2009; 78 FR 13268, Feb. 27, 2013; 79 FR 3517, Jan. 22, 2014] Avocado ...... 1 .0 Banana ...... 0.50 Beet, sugar, molasses ...... 0 .30 § 180.471 Furilazole; tolerances for res- Beet, sugar, roots ...... 0 .05 idues. Beet, sugar, tops ...... 0.50 Biriba ...... 0 .30 (a) General. Tolerances are estab- Blueberry ...... 3 .5 lished for residues of furilazole; 3- Borage, seed ...... 0 .05 dichloroacetyl-5-(2-furanyl)-2, 2- Caneberry, subgroup 13-A ...... 2 .5 Canistel ...... 1 .0 dimethyloxazolidine (CAS Reg. No. Canola, seed ...... 0 .05 121776–33–8) when used as an inert in- Cattle, fat ...... 0.30 gredient (safener) in pesticide formula- Cattle, meat ...... 0 .30 tions in or on the following raw agri- Cattle, meat byproducts ...... 0.30 Cherimoya ...... 0 .30 cultural commodities: Citrus, dried pulp ...... 5 .0 Coffee, bean, green ...... 0 .80 Commodity Parts per Cotton, gin byproducts ...... 4 .0 million Cotton, meal ...... 8 .0 Cotton, undelinted seed ...... 6 .0 Corn, field, forage ...... 0 .01 Crambe, seed ...... 0.05 Corn, field, grain ...... 0 .01 Cranberry ...... 0 .05 Corn, field, stover ...... 0 .01 Currant ...... 3 .5 Corn, pop, grain ...... 0.01 Custard apple ...... 0 .30 Corn, pop, stover ...... 0.01 Egg ...... 0 .02 Sorghum, forage ...... 0 .01 Elderberry ...... 3 .5 Sorghum, grain ...... 0 .01 Feijoa ...... 1 .0 Sorghum, stover ...... 0 .01 Fish ...... 0 .05 Fish-shellfish, mollusc ...... 0 .05 (b) Section 18 emergency exemptions. Flax, seed ...... 0 .05 [Reserved] Fruit, citrus, group 10 ...... 0 .70 (c) Tolerances with regional registra- Fruit, pome, group 11 ...... 0.6 Fruit, stone, group 12 ...... 3 .0 tions. [Reserved] Goat, fat ...... 0 .30 (d) Indirect or inadvertent residues. Goat, meat ...... 0.30 [Reserved] Goat, meat byproducts ...... 0 .30 Gooseberry ...... 3 .5 [65 FR 8867, Feb. 23, 2000, as amended at 67 Grain, cereal, forage, fodder and straw, group FR 15735, Apr. 3, 2002; 72 FR 57492, Oct. 10, 16, forage, except rice ...... 7 .0 2007] Grain, cereal, forage, fodder and straw, group 16, hay, except rice ...... 6 .0 Grain, cereal, forage, fodder and straw, group § 180.472 Imidacloprid; tolerances for 16, stover, except rice ...... 0 .30 residues. Grain, cereal, forage, fodder and straw, group 16, straw, except rice ...... 3.0 (a) General. Tolerances are estab- Grain, cereal, group 15, except rice ...... 0 .05 lished for residues of the insecticide Grape ...... 1 .0 imidacloprid, including its metabolites Grape, juice ...... 1 .5 and degradates, in or on the commod- Grape, raisin ...... 1 .5 Guava ...... 1 .0 ities in the table below. Compliance Herbs subgroup 19A, dried herbs ...... 48 with the tolerance levels specified Herbs subgroup 19-A, fresh herbs ...... 8 .0 below is to be determined by measuring Hog, fat ...... 0 .30 Hog, meat ...... 0 .30 only the sum of imidacloprid (1-[6- Hog, meat byproducts ...... 0 .30 chloro-3-pyridinyl) methyl]-N-nitro-2- Hop, dried cones ...... 6 .0 imidazolidinimine) and its metabolites Horse, fat ...... 0 .30 containing the 6-chloropyridinyl moi- Horse, meat ...... 0 .30 Horse, meat byproducts ...... 0 .30 ety, calculated as the stoichiometric Huckleberry ...... 3 .5 equivalent of imidacloprid, in or on the Ilama ...... 0 .30 following commodities: Jaboticaba ...... 1 .0 Juneberry ...... 3 .5 Parts per Kava, leaves ...... 4 .0 Commodity million Kava, roots ...... 0 .40 Leaf petioles subgroup 4B ...... 6 .0 Acerola ...... 1.0 Leafy greens subgroup 4A ...... 3 .5 Almond, hulls ...... 4 .0 Lettuce, head ...... 3.5 Apple ...... 0.5 Lettuce, leaf ...... 3 .5 Apple, wet pomace ...... 3 .0 Lingonberry ...... 3.5 Artichoke, globe ...... 2.5 Longan ...... 3 .0 Aspirated grain fractions ...... 240 Lychee ...... 3 .0 Atemoya ...... 0 .30 Mango ...... 1.0

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imidacloprid (1-[6-chloro-3- Commodity Parts per million pyridinyl)methyl]-N-nitro-2- Milk ...... 0.10 imidazolidinimine) and its metabolites Mustard, black, seed ...... 0 .05 containing the 6-chloropyridinyl moi- Mustard, field, seed ...... 0 .05 ety, calculated as the stoichiometric Mustard, Indian, seed ...... 0 .05 Mustard, rapeseed, seed ...... 0 .05 equivalent of imidacloprid. These tol- Mustard, seed ...... 0 .05 erances will expire and are revoked on Nut, tree, group 14 ...... 0 .05 the dates specified in the following Okra ...... 1.0 table: Onion, dry bulbs, subgroup 3-07A ...... 0 .15 Onion, green, subgroup 3-07B ...... 2 .5 Expiration/ Papaya ...... 1 .0 Parts per Commodity million revocation Passionfruit ...... 1 .0 date Peanut ...... 0 .45 Peanut, hay ...... 35 Sugarcane, cane ...... 6.0 12/31/15 Peanut, meal ...... 0 .75 Sugarcane, molasses ...... 50 12/31/15 Pecan ...... 0 .05 Persimmon ...... 3 .0 Pistachio ...... 0.05 (c) Tolerances with regional registra- Pomegranate ...... 0 .90 tions. [Reserved] Potato, chip ...... 0 .40 (d) Indirect or inadvertent residues. Potato, processed potato waste ...... 0 .90 Tolerances are established for indirect Poultry, fat ...... 0.05 Poultry, meat ...... 0 .05 or inadvertent residues of the insecti- Poultry, meat byproducts ...... 0.05 cide imidacloprid, including its me- Pulasan ...... 3 .0 tabolites and degradates, in or on the Rambutan ...... 3 .0 commodities in the table below. Com- Rapeseed, seed ...... 0 .05 Raspberry, wild ...... 2.5 pliance with the tolerance levels speci- Safflower, seed ...... 0 .05 fied below is to be determined by meas- Salal ...... 3 .5 uring only the sum of imidacloprid (1- Sapodilla ...... 1 .0 Sapote, black ...... 1 .0 [6-chloro-3-pyridinyl) methyl]-N-nitro- Sapote, mamey ...... 1 .0 2-imidazolidinimine) and its metabo- Sheep, fat ...... 0 .30 lites containing the 6-chloropyridinyl Sheep, meat ...... 0.30 moiety, calculated as the stoichio- Sheep, meat byproducts ...... 0 .30 Soursop ...... 0 .30 metric equivalent of imidacloprid, in Soybean, forage ...... 8 .0 or on the following commodities, when Soybean, hay ...... 35 present therein as a result of the appli- Soybean, meal ...... 4.0 cation of the pesticide to growing crops Soybean, seed ...... 3 .5 Spanish lime ...... 3 .0 listed in this section and other non- Star apple ...... 1 .0 food crops as follows: Starfruit ...... 1 .0 Strawberry ...... 0 .50 Commodity Parts per Sugar apple ...... 0 .30 million Sunflower, seed ...... 0.05 Tomato, paste ...... 6 .0 Rice, grain ...... 0 .05 Tomato, puree ...... 3 .0 Vegetable, foliage of legume, group 7 ...... 2 .5 Vegetable, brassica leafy, group 5 ...... 3 .5 Vegetable, legume, group 6 ...... 0 .3 Vegetable, cucurbit, group 9 ...... 0.5 Vegetable, fruiting, group 8 ...... 1.0 Vegetable, leaves of root and tuber, group 2 ..... 4 .0 [75 FR 22251, Apr. 28, 2010, as amended at 78 Vegetable, legume, group 6, except soybean .... 4 .0 FR 33743, June 5, 2013] Vegetable, root and tuber, group 1, except sugar beet ...... 0 .40 § 180.473 Glufosinate ammonium; tol- Watercress ...... 3 .5 erances for residues. Watercress, upland ...... 3 .5 Wax jambu ...... 1 .0 (a) General. Tolerances are established for residues of the herbicide (b) Section 18 emergency exemptions. glufosinate ammonium, including its Time-limited tolerances are estab- metabolites and degradates, in or on lished for residues of the insecticide the commodities in the table below. imidacloprid, including its metabolites Compliance with the tolerance levels and degradates in connection with use specified below is to be determined by of the pesticide under a Section 18 measuring the sum of glufosinate am- emergency exemption granted by EPA. monium, butanoic acid, 2-amino-4- Compliance with the tolerance levels (hydroxymethylphosphinyl) specified below is to be determined by monoammonium salt, and its metabo- measuring only the sum of lites, 2-(acetylamino)-4-

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(hydroxymethyl phosphinyl)butanoic (d) Indirect or inadvertent residues. acid, and 3- Tolerances are established for indirect (hydroxymethylphosphinyl)propanoic or inadvertent residues of glufosinate acid, expressed as 2-amino-4- ammonium, including its metabolites (hydroxymethylphosphinyl)butanoic and degradates, in or on the commod- acid equivalents: ities in the table below, as a result of the application of glufosinate ammo- Parts per Commodity million nium to crops listed in paragraph (a) of this section. Compliance with the tol- Almond, hulls ...... 0 .50 erance levels specified below is to be Apple ...... 0.05 determined by measuring the sum of Banana ...... 0.30 Banana, pulp ...... 0 .20 glufosinate ammonium, butanoic acid, Beet, sugar, molasses ...... 5 .0 2-amino-4-(hydroxymethylphosphinyl) Beet, sugar, roots ...... 0 .9 monoammonium salt, and its metabo- Beet, sugar, tops (leaves) ...... 1 .5 Bushberry subgroup 13B ...... 0 .15 lite, 3-(hydroxymethylphosphinyl) pro- Canola, meal ...... 1 .1 panoic acid, expressed as 2-amino-4- Canola, seed ...... 0 .40 (hydroxymethylphosphinyl)butanoic Cattle, fat ...... 0.40 acid equivalents. Cattle, meat ...... 0 .15 Cattle, meat byproducts ...... 6.0 Parts per Corn, field forage ...... 4.0 Commodity million Corn, field, grain ...... 0 .20 Corn, field, stover ...... 6 .0 Barley, hay ...... 0 .40 Corn, sweet, forage ...... 1 .5 Barley, straw ...... 0 .40 Corn, sweet, kernels plus cob with husks re- Buckwheat, fodder ...... 0 .40 moved ...... 0 .30 Buckwheat, forage ...... 0 .40 Corn, sweet, stover ...... 6 .0 Oat, forage ...... 0 .40 Cotton, gin byproducts ...... 15 Oat, hay ...... 0.40 Cotton, undelinted seed ...... 4 .0 Oat, straw ...... 0.40 Egg ...... 0 .15 Rye, forage ...... 0 .40 Fruit, citrus, group 10–10 ...... 0 .15 Rye, straw ...... 0 .40 Fruit, pome, group 11–10 ...... 0 .25 Teosinte ...... 0 .40 Fruit, stone, group 12–12 ...... 0 .25 Triticale ...... 0.40 Goat, fat ...... 0 .40 Wheat, forage ...... 0 .40 Goat, meat ...... 0.15 Wheat, hay ...... 0 .40 Goat, meat byproducts ...... 6 .0 Wheat, straw ...... 0 .40 Grain aspirated fractions ...... 25 Grape ...... 0 .05 Hog, fat ...... 0 .40 [68 FR 55849, Sept. 29, 2003, as amended at 71 Hog, meat ...... 0 .15 FR 25945, May 3, 2006; 72 FR 72625, Dec. 21, Hog, meat byproducts ...... 6 .0 2007; 76 FR 23497, Apr. 27, 2011; 77 FR 59113, Horse, fat ...... 0 .40 Sept. 26, 2012] Horse, meat ...... 0 .15 Horse, meat byproducts ...... 6 .0 § 180.474 Tebuconazole; tolerances for Juneberry ...... 0 .10 Lingonberry ...... 0.10 residues. Milk ...... 0.15 (a) General. (1) Tolerances are estab- Nut, tree, group 14 ...... 0 .10 lished for residues of tebuconazole, Olive ...... 0 .15 Pistachio ...... 0.10 alpha-[2-(4-chlorophenyl)ethyl]-alpha- Potato ...... 0 .80 (1,1-dimethylethyl)-1H-1,2,4-triazole-1- Potato, chips ...... 1 .6 ethanol, including its metabolites and Potato granules/flakes ...... 2 .0 Poultry, fat ...... 0.15 degradates, in or on the commodities Poultry, meat ...... 0 .15 in the table below. Compliance with Poultry, meat byproducts ...... 0.60 the tolerance levels specified below is Rice, grain ...... 1 .0 to be determined by measuring only Rice, hull ...... 2 .0 Rice, straw ...... 2 .0 tebuconazole [a-[2-(4-chlorophenyl) Salal ...... 0 .10 ethyl]-a-(1,1-dimethylethyl)-1H-1,2,4- Sheep, fat ...... 0 .40 triazole-1-ethanol], in or on the com- Sheep, meat ...... 0.15 Sheep, meat byproducts ...... 6 .0 modity. Soybean ...... 2.0 Soybean, hulls ...... 5 .0 Commodity Parts per million

(b) Section 18 emergency exemptions. Almond, hulls ...... 6 .0 [Reserved] Apple, wet pomace ...... 0 .1 Asparagus ...... 0.05 (c) Tolerances with regional restric- Banana ...... 0.05 tions. [Reserved] Barley, grain ...... 0 .3

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dimethylethyl)-1H-1,2,4-triazole-1-eth- Commodity Parts per million anol) and its diol metabolite (1-(4- Barley, hay ...... 7 .0 chlorophenyl)-4,4-dimethyl-3-(1H -1,2,4- Barley, straw ...... 3 .5 triazole-1-yl-methyl)-pentane-3,5-diol), Bean, dry seed ...... 0 .1 calculated as the stoichiometric equiv- Bean, succulent ...... 0 .1 Beet, garden, roots ...... 0 .70 alent of tebuconzole, in or on the com- Beet, garden, tops ...... 7 .0 modity. Brassica, leafy greens, subgroup 5B ...... 2 .5 Cherry, sweet, pre- and post-harvest ...... 5 .0 Parts per Cherry, tart, pre- and post-harvest ...... 5 .0 Commodity million Coffee, green bean 1 ...... 0 .15 Coffee, roasted bean 1 ...... 0 .3 Cattle, meat byproducts ...... 0.2 Corn, field, forage ...... 4 .0 Goat, meat byproducts ...... 0 .2 Corn, field, grain ...... 0 .05 Horse, meat byproducts ...... 0 .2 Corn, field, stover ...... 3 .5 Corn, pop, grain ...... 0.05 Milk ...... 0.1 Corn, pop, stover ...... 3.5 Sheep, meat byproducts ...... 0 .2 Corn, sweet, forage ...... 7 .0 Corn, sweet, kernel plus cob with husks re- (b) Section 18 emergency exemptions. moved ...... 0 .5 Corn, sweet, stover ...... 6 .0 [Reserved] Cotton, gin byproducts ...... 25 .0 (c) Tolerances with regional registra- Cotton, undelinted seed ...... 2 .0 tions. Tolerances are established for Fruit, pome, group 11 ...... 0.05 Fruit, stone, group 12, except cherry ...... 1 .0 residues of the fungicide tebuconazole, Grain, aspirated fractions ...... 16.0 including its metabolites and Grape ...... 5 .0 degradates, in or on the commodities Grass, forage ...... 8 .0 Grass, hay ...... 25 .0 in the following table. Compliance with Grass, seed screenings ...... 55.0 the tolerance levels specified below is Grass, straw ...... 30 .0 to be determined by measuring only Hop, dried cones ...... 35 .0 tebuconazole, alpha-[2-(4- Lychee ...... 1 .6 Mango, postharvest ...... 0 .15 chlorophenyl)ethyl]-alpha-(1,1- Nut, tree, group 14 ...... 0 .05 dimethylethyl)-1H-1,2,4-triazole-1-eth- Oat, forage ...... 0 .10 anol, in or on the commodity. Oat, grain ...... 0 .15 Oat, hay ...... 0.10 Oat, straw ...... 0.10 Parts per Commodity million Onion, bulb, subgroup 3-07A ...... 0 .2 Onion, green, subgroup 3-07B ...... 1 .3 Turnip, roots ...... 0 .5 Orange 1 ...... 1 .0 Orange, oil 1 ...... 10 Turnip, tops ...... 7.0 Peach ...... 1 .0 Peanut ...... 0 .1 (d) Indirect or inadvertent residues. Pistachio ...... 0.05 [Reserved] Plum, pre- and post-harvest ...... 1 .0 Soybean, forage ...... 25 [59 FR 39464, Aug. 3, 1994] Soybean, hay ...... 50 Soybean, seed ...... 0 .08 EDITORIAL NOTE: For FEDERAL REGISTER ci- Sunflower, seed ...... 0.05 tations affecting § 180.474, see the List of CFR Sunflower, meal ...... 0 .2 Sunflower, refined oil ...... 0.2 Sections Affected, which appears in the Vegetable, cucurbit, group 9 ...... 0.4 Finding Aids section of the printed volume Vegetable, fruiting, group 8–10 ...... 1 .3 and at www.fdsys.gov. Wheat, forage ...... 3 .0 Wheat, germ ...... 0 .20 § 180.475 Difenoconazole; tolerances Wheat, grain ...... 0 .15 Wheat, hay ...... 7 .0 for residues. Wheat, shorts ...... 0 .20 (a) General. (1) Tolerances are estab- Wheat, straw ...... 1 .5 lished for residues of difenoconazole, 1There are no U.S. registrations. including its metabolites and (2) Tolerances are established for res- degradates, in or on the commodities idues of the fungicide tebuconazole, in- in the following table. Compliance with cluding its metabolites and degradates, the tolerance levels specified below is in or on the commodities in the fol- to be determined by measuring only lowing table. Compliance with the tol- difenoconazole, 1-[2-[2-chloro-4-(4- erance levels specified in the following chlorophenoxy)phenyl]-4-methyl-1,3- table is to be determined by measuring dioxolan-2-ylmethyl]-1H-1,2,4-triazole, only the sum of tebuconazole (alpha-[2- in or on the following raw agricultural (4-chlorophenyl)ethyl]-alpha-(1,1- commodities:

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metric equivalent of difenoconazole, in Commodity Parts per million the following commodities: Almond, hulls ...... 7 .0 Parts per Apple, wet pomace ...... 4 .5 Commodity million Aspirated grain fractions ...... 95 Banana1 ...... 0 .2 Cattle, fat ...... 0.10 Barley, grain ...... 0 .1 Cattle, liver ...... 0 .40 Barley, hay ...... 0 .05 Cattle, meat ...... 0 .05 Barley, straw ...... 0 .05 Cattle, meat byproduct (except liver) ...... 0 .10 Beet, sugar ...... 0 .3 Egg ...... 0 .02 Beet, sugar, dried pulp ...... 1 .9 Goat, fat ...... 0 .10 Berry, low growing, subgroup 13–07G, except Goat, liver ...... 0.40 cranberry ...... 2.5 Goat, meat ...... 0.05 Brassica, head and stem, subgroup 5A ...... 1 .9 Goat, meat byproduct (except liver) ...... 0.10 Brassica, leafy green, subgroup 5B ...... 35 Hog, fat ...... 0 .10 Canola, seed ...... 0 .01 Hog, liver ...... 0 .40 Carrot ...... 0 .50 Hog, meat ...... 0 .05 Chickpea ...... 0 .08 Hog, meat byproduct (except liver) ...... 0 .10 Citrus, dried pulp ...... 2 .0 Horse, fat ...... 0 .10 Citrus, oil ...... 25 Horse, liver ...... 0 .40 Corn, sweet, forage ...... 0 .01 Horse, meat ...... 0 .05 Corn, sweet, kernel plus cob with husks re- Horse, meat byproduct (except liver) ...... 0 .10 moved ...... 0 .01 Milk ...... 0.01 Corn, sweet, stover ...... 0 .01 Sheep, fat ...... 0 .10 Cotton, gin byproducts ...... 0 .05 Sheep, liver ...... 0.40 Cotton, undelinted seed ...... 0 .05 Sheep, meat ...... 0.05 Fruit, citrus, group 10–10 ...... 0 .60 Sheep, meat byproduct (except liver) ...... 0.10 Fruit, pome, group 11–10 ...... 1 .0 Fruits, stone, group 12 ...... 2 .5 (b) Section 18 emergency exemptions. Grape ...... 4 .0 Grape, raisin ...... 6 .0 [Reserved] Mango 1 ...... 0.07 (c) Tolerances with regional registra- Nut, tree, group 14 ...... 0 .03 tions. [Reserved] Oat, forage ...... 0 .15 Oat, grain ...... 0 .01 (d) Indirect or inadvertent residues. Oat, hay ...... 0.05 [Reserved] Oat, straw ...... 0.05 Onion, bulb, subgroup 3-07A ...... 0 .20 [64 FR 36254, July 6, 1999] Onion, green, subgroup 3-07B ...... 6 .0 EDITORIAL NOTE: For FEDERAL REGISTER ci- 1 Papaya ...... 0 .30 tations affecting § 180.475, see the List of CFR Pistachio ...... 0.03 Potato, wet peel ...... 7 .3 Sections Affected, which appears in the Rye, forage ...... 0 .15 Finding Aids section of the printed volume Rye, grain ...... 0.01 and at www.fdsys.gov. Rye, straw ...... 0 .05 Soybean, hulls ...... 0 .20 § 180.476 Triflumizole; tolerances for Soybean, seed ...... 0 .15 residues. Turnip, greens ...... 35 Vegetable, cucurbit, group 9 ...... 0.70 (a) General. (1) Tolerances are estab- Vegetable, fruiting, group 8–10 ...... 0 .60 lished for residues of the fungicide Vegetable, tuberous and corm, subgroup 1C ..... 4.0 Wax jambu 1 ...... 1 .5 triflumizole, including its metabolites Wheat, forage ...... 0 .1 and degradates, in or on the commod- Wheat, grain ...... 0 .1 ities listed in the table below. Compli- Wheat, hay ...... 0 .05 ance with the tolerance levels specified Wheat, straw ...... 0 .1 below is to be determined by measuring 1There are no U.S. registrations. only the parent compound triflumizole, (2) Tolerances are established for res- 1-(1-((4-chloro-2- idues of difenoconazole, including its (trifluoromethyl)phenyl)imino)-2- metabolites and degradates, in the propoxyethyl)-1 H -imidazole, and its commodities in the table below. Com- metabolites containing the 4-chloro-2- pliance with the tolerance levels speci- trifluoromethylaniline moiety, cal- fied below is to be determined by meas- culated as stoichiometric equivalent of uring the sum of difenoconazole, 1-[2- the parent compound. [2-chloro-4-(4-chlorophenoxy)phenyl]-4- Parts per methyl-1,3-dioxolan-2-ylmethyl]-1H- Commodity million 1,2,4-triazole, and its metabolite, CGA– 205375, 1-[2-chloro-4-(4-chloro- Apple, dry pomace ...... 2.0 Apple, wet pomace ...... 2 .0 phenoxy)phenyl]-2-[1,2,4]triazol-1-yl- Berry, low growing, subgroup 13–07G, except ethanol, calculated as the stoichio- cranberry ...... 2.0

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(b) Section 18 emergency exemptions. Commodity Parts per million [Reserved] Brassica, head and stem, subgroup 5A ...... 8 .0 (c) Tolerances with regional registra- Brassica, leafy greens, subgroup 5B ...... 40 tions. [Reserved] Canistel ...... 2 .5 (d) Indirect or inadvertent residues. Cherry, sweet ...... 1 .5 Cherry, tart ...... 1 .5 [Reserved] Cilantro, leaves ...... 35 [65 FR 33702, May 24, 2000, as amended at 67 Fruit, pome, group 11–10 ...... 0 .50 Fruit, small, vine climbing, except fuzzy FR 40228, June 12, 2002; 67 FR 54587, Aug. 23, kiwifruit, subgroup 13–07F ...... 2 .5 2002; 70 FR 7047, Feb. 10, 2005; 70 FR 17915, Grape, dried pomace ...... 15 .0 Apr. 8, 2005; 71 FR 13279, Mar. 15, 2006; 71 FR Grape, raisin, waste ...... 10 .0 49358, Aug. 23, 2006; 74 FR 26543, June 3, 2009; Grape, wet pomace ...... 15 .0 74 FR 46376, Sept. 9, 2009; 76 FR 34885, June 15, Hazelnut ...... 0 .05 2011; 79 FR 12408, Mar. 5, 2014] Hop, dried cones ...... 50 Leafy greens subgroup 4A, except spinach ...... 35 Mango ...... 2.5 § 180.477 Flumiclorac pentyl; toler- Papaya ...... 2 .5 ances for residues. Pineapple ...... 4.0 Sapodilla ...... 2 .5 (a) General. Tolerances are estab- Sapote, black ...... 2 .5 lished for residues of the herbicide Sapote, mamey ...... 2 .5 flumiclorac pentyl, including its me- Star apple ...... 2 .5 Swiss chard ...... 18 tabolites and degradates, in or on the Tomato ...... 1.5 commodities in the table in this para- Turnip, greens ...... 40 graph. Compliance with the tolerance Vegetable, cucurbit, Group 9 ...... 0 .5 levels specified in this paragraph is to be determined by measuring only (2) Tolerances are established for res- flumiclorac pentyl, pentyl(2-chloro-4- idues of the fungicide triflumizole, in- fluoro-5-(1,3,4,5,6,7-hexahydro-1,3-dioxo- cluding its metabolites and degradates, 2H-isoindol-2-yl)phenoxy)acetate, in or in or on the commodities of animal ori- on the commodity. gin listed in the table below. Compli- ance with the tolerance levels specified Commodity Parts per below is to be determined by measuring million only the parent compound triflumizole, Corn, field, forage ...... 0 .01 1-(1-((4-chloro-2- Corn, field, grain ...... 0 .01 (trifluoromethyl)phenyl)imino)-2- Corn, field, stover ...... 0 .01 Cotton, gin byproducts ...... 3 .0 propoxyethyl)-1 H -imidazole, the me- Cotton, undelinted seed ...... 0 .2 tabolite 4-chloro-2-hydroxy-6- Soybean, hulls ...... 0 .02 trifluoromethylaniline sulfate, and Soybean, seed ...... 0 .01 other metabolites containing the 4- chloro-2-trifluoromethylaniline moi- (b) Section 18 emergency exemptions. ety, calculated as the parent com- [Reserved] pound. (c) Tolerances with regional registrations. [Reserved] Commodity Parts per (d) Indirect or inadvertent residues. million [Reserved] Cattle, fat ...... 0.5 [65 FR 33702, May 24, 2000, as amended at 71 Cattle, meat ...... 0 .05 FR 11533, Mar. 8, 2006; 76 FR 23497, Apr. 27, Cattle, meat byproducts ...... 0.5 Egg ...... 0 .05 2011] Goat, fat ...... 0 .5 Goat, meat ...... 0.05 § 180.478 Rimsulfuron; tolerances for Goat, meat byproducts ...... 0 .5 residues. Hog, fat ...... 0 .5 Hog, meat ...... 0 .05 (a) General. Tolerances are estab- Hog, meat byproducts ...... 0 .5 lished for residues of the herbicide Horse, fat ...... 0 .5 rimsulfuron, including its metabolites Horse, meat ...... 0 .05 Horse, meat byproducts ...... 0 .5 and degradates, in or on the commod- Milk ...... 0.05 ities in the table below. Compliance Poultry, fat ...... 0.05 with the tolerance levels specified Poultry, meat ...... 0 .05 Poultry, meat byproducts ...... 0.1 below is to be determined by measuring Sheep, fat ...... 0 .5 only rimsulfuron, N-((4,6- Sheep, meat ...... 0.05 dimethoxypyrimidin-2- Sheep, meat byproducts ...... 0 .5 yl)aminocarbonyl)-3-(ethylsulfonyl)-2-

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pyridinesulfonamide), in or on the Commodity Parts per commodities. million Goat, meat byproducts ...... 1 .0 Parts per Commodity million Hog, meat byproducts ...... 0 .1 Horse, fat ...... 0 .05 Almond, hulls ...... 0 .09 Horse, meat ...... 0 .05 Bushberry, subgroup 13–07B ...... 0.01 Horse, meat byproducts ...... 1 .0 Caneberry, subgroup 13–07A ...... 0 .01 Milk ...... 0.05 Chicory, roots ...... 0 .01 Sheep, fat ...... 0 .05 Chicory, tops ...... 0 .01 Sheep, meat ...... 0.05 Corn, field, forage ...... 0 .4 Sheep, meat byproducts ...... 1 .0 Corn, field, grain ...... 0 .1 Corn, field, stover ...... 2 .5 (2) Tolerances are established for res- Fruit, citrus, group 10 ...... 0 .01 idues of the herbicide halosulfuron- Fruit, pome, group 11 ...... 0.01 Fruit, stone, group 12 ...... 0 .01 methyl, methyl 5-[(4,6-dimethoxy-2- Grain, aspirated fractions ...... 4 .5 pyrimidiny)amino]carbonylamino Grape ...... 0 .01 sulfonyl]-3-chloro-1-methyl-1H-pyr- Nut, tree, group 14 ...... 0 .01 Pistachio ...... 0.01 azole-4-carboxylate, including its me- Potato ...... 0 .1 tabolites and degradates, in or on the Soybean, forage ...... 0 .25 commodities in the following table. Soybean, hay ...... 1 .2 Compliance with the tolerance levels Soybean, hulls ...... 0 .04 Soybean, seed ...... 0 .01 specified in the following table is to be Tomato ...... 0.05 determined by measuring only halosulfuron-methyl. (b) Section 18 emergency exemptions. Parts per [Reserved] Commodity million (c) Tolerances with regional registrations. [Reserved] Alfalfa, forage ...... 1.0 Alfalfa, hay ...... 2.0 (d) Indirect or inadvertent residues. Almond, hulls ...... 0 .2 [Reserved] Apple ...... 0.05 Artichoke ...... 0 .05 [63 FR 16696, Apr. 6, 1998, as amended at 72 Asparagus ...... 0.8 FR 41913, Aug. 1, 2007; 74 FR 67137, Dec. 18, Bean, dry, seed ...... 0 .05 2009; 77 FR 3625, Jan. 25, 2012; 77 FR 46306, Bushberry, subgroup 13-07B ...... 0 .05 Aug. 3, 2012] Caneberry subgroup 13–07A ...... 0.05 Corn, field, forage ...... 0 .2 Corn, field, grain ...... 0 .05 § 180.479 Halosulfuron-methyl; toler- Corn, field, stover ...... 0 .8 ances for residues. Corn, pop, grain ...... 0.05 Corn, pop, stover ...... 0.8 (a) General. (1) Tolerances are estab- Corn, sweet, forage ...... 0 .2 lished for residues of the herbicide Corn, sweet, kernel plus cob with husks re- halosulfuron-methyl, methyl 5-[(4,6- moved ...... 0 .05 Corn, sweet, stover ...... 0 .8 dimethoxy-2-pyrimidiny)amino] Cotton, gin byproducts ...... 0 .05 carbonylaminosulfonyl]-3-chloro-1- Cotton, undelinted seed ...... 0 .05 methyl-1H-pyrazole-4-carboxylate, in- Grass, forage, fodder, and hay, group 17, forage ...... 20 cluding its metabolites and degradates, Grass, forage, fodder, and hay, group 17, hay 0 .5 in or on the commodities in the fol- Melon subgroup 9A ...... 0 .1 lowing table. Compliance with the tol- Millet, proso, forage ...... 10 erance levels specified in the following Millet, proso, grain ...... 0 .01 Millet, proso, hay ...... 0 .01 table is to be determined by measuring Millet, proso, straw ...... 0 .01 only those halosulfuron-methyl resi- Nut, tree, group 14 ...... 0 .05 dues containing the 3- Okra ...... 0.05 Pea and bean, succulent shelled, subgroup 6 .. 0 .05 chlorosulfonamide (3-CSA) moiety, ex- Pea and bean, succulent shelled, subgroup 6B 0 .05 pressed as the stoichiometric equiva- Pistachio ...... 0.05 lent of halosulfuron-methyl, in or on Rhubarb ...... 0 .05 Rice, grain ...... 0 .05 the commodity. Rice, straw ...... 0 .2 Sorghum, grain, forage ...... 0.05 Commodity Parts per Sorghum, grain, grain ...... 0 .05 million Sorghum, grain, stover ...... 0 .1 Soybean, seed ...... 0 .05 Cattle, fat ...... 0.05 Squash/Cucumber subgroup 9B ...... 0 .5 Cattle, meat ...... 0 .05 Sugarcane, cane ...... 0.05 Cattle, meat byproducts ...... 1.0 Vegetable, fruiting, group 8 ...... 0.05 Goat, fat ...... 0 .05 Vegetable, tuberous and corm, subgroup 1C ... 0.05 Goat, meat ...... 0.05

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(b) Section 18 emergency exemptions. Commodity Parts per [Reserved] million (c) Tolerances with regional registra- Wheat, grain ...... 0 .1 tions. [Reserved] Wheat, hay ...... 8 .0 (d) Indirect or inadvertent residues. Wheat, straw ...... 8 .0 [Reserved] 1There are no United States registrations for grape as of August 2006. [64 FR 25448, May 12, 1999, as amended at 65 FR 58433, Sept. 29, 2000; 66 FR 66340, Dec. 26, (b) Section 18 emergency exemptions. 2001; 66 FR 66786, Dec. 27, 2001; 67 FR 45649, [Reserved] July 10, 2002; 67 FR 59192, Sept. 20, 2002; 70 FR (c) Tolerances with regional registra- 51622, Aug. 31, 2005; 72 FR 8927, Feb. 28, 2007; tions. [Reserved] 74 FR 48401, Sept. 23, 2009; 75 FR 46853, Aug. (d) Indirect or inadvertent residues. 4, 2010; 76 FR 34886, June 15, 2011; 77 FR 71561, [Reserved] Dec. 3, 2012; 78 FR 53051, Aug. 28, 2013] [60 FR 11032, Mar. 1, 1995] § 180.480 Fenbuconazole; tolerances EDITORIAL NOTE: For FEDERAL REGISTER ci- for residues. tations affecting § 180.480, see the List of CFR (a) Tolerances are established for res- Sections Affected, which appears in the idues of the fungicide fenbuconazole, Finding Aids section of the printed volume including its metabolites and and at www.fdsys.gov. degradates, in or on the commodities § 180.481 Prosulfuron; tolerances for in the table below. Compliance with residues. the tolerance levels specified below is (a) General. Tolerances are estab- to be determined by measuring only lished for residues of the herbicide the sum of fenbuconazole, alpha-[2-(4- prosulfuron and its metabolites and chlorophenyl)-ethyl]-alpha-phenyl-3- degradates in or on the commodities in (1H-1,2,4-triazole)-1-propanenitrile, and the table below. Compliance with the its metabolites RH-9129, cis-5-(4- tolerance levels specified in the table chlorophenyl)-dihydro-3-phenyl-3-(1H- below is to be determined by measuring 1,2,4-triazole-1-ylmethyl)-2-3 H- only prosulfuron, 1-(4-methoxy-6-meth- furanone, and RH-9130, trans-5-(4- yl-triazin-2-yl)-3-[2-(3,3,3- chlorophenyl)-dihydro-3-phenyl-3-(1H- trifluoropropyl)-phenylsulfonyl]-urea, 1,2,4-triazole-1-ylmethyl)-2-3 H- in or on the commodity. furanone, calculated as the stoichiometric equivalent of fenbuconazole, in Commodity Parts per or on the following agricultural com- million modities. Grain, cereal, forage, fodder, and straw, group 16, except rice, fodder ...... 0 .01 Commodity Parts per Grain, cereal, forage, fodder, and straw, group million 16, except rice, forage ...... 0 .10 Grain, cereal, forage, fodder, and straw, group Almond ...... 0.05 16, except rice, hay ...... 0 .20 Almond, hulls ...... 1 .0 Grain, cereal, forage, fodder, and straw, group Apple ...... 0.4 16, except rice, straw ...... 0 .02 Apple, wet pomace ...... 1 .0 Grain, cereal, group 15, except rice ...... 0 .01 Banana ...... 0.3 Beet, sugar, dried pulp ...... 1 .0 Beet, sugar, molasses ...... 0 .4 (b) Section 18 emergency exemptions. Beet, sugar, roots ...... 0 .3 [Reserved] Beet, sugar, tops ...... 9.0 (c) Tolerances with regional registra- Bushberry subgroup 13B ...... 0 .3 tion. [Reserved] Cattle, meat byproducts ...... 0.05 Citrus, dried pulp ...... 5 .0 (d) Indirect or inadvertent residues. Citrus, oil ...... 40.0 [Reserved] Cranberry ...... 0 .5 Fruit, citrus, group 10 ...... 1 .0 [74 FR 67118, Dec. 18, 2009] Fruit, stone, group 12 ...... 1 .0 Goat, meat byproducts ...... 0 .05 § 180.482 Tebufenozide; tolerances for Grain, aspirated fractions ...... 6 .0 residues. Grape 1 ...... 1 .0 Horse, meat byproducts ...... 0 .05 (a) General. (1) Tolerances are estab- Peanut ...... 0 .1 lished for residues of the insecticide Pecan ...... 0 .05 tebufenozide, including its metabolites Pepper ...... 1 .0 Sheep, meat byproducts ...... 0 .05 and degradates, in or on the commod- Wheat, forage ...... 4 .0 ities in the table in this paragraph.

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Compliance with the tolerance levels the stoichiometric equivalent of specified in this paragraph is to be de- tebufenozide, in or on the commodity. termined by measuring only Parts per tebufenozide, 3,5-dimethylbenzoic acid Commodity million 1-(1,1-dimethylethyl)-2-(4- ethylbenzoyl)hydrazide, in or on the Cattle, fat ...... 0.1 commodity. Cattle, meat ...... 0 .08 Cattle, meat byproducts ...... 0.08 Parts per Goat, fat ...... 0 .1 Commodity million Goat, meat ...... 0.08 Goat, meat byproducts ...... 0 .08 Almond, hulls ...... 25 Hog, fat ...... 0 .1 Apple ...... 1.0 Hog, meat ...... 0 .08 Apple, dry pomace ...... 3.0 Hog, meat byproducts ...... 0 .08 Apple, wet pomace ...... 3 .0 Horse, fat ...... 0 .1 Berry group 13 ...... 3 .0 Horse, meat ...... 0 .08 Brassica, head and stem, subgroup 5A ...... 5 .0 Brassica, leafy greens, subgroup 5B ...... 10 .0 Horse, meat byproducts ...... 0 .08 Canola, refined oil ...... 4 .0 Milk ...... 0.04 Canola, seed ...... 2 .0 Sheep, fat ...... 0 .1 Citrus, oil ...... 15.0 Sheep, meat ...... 0.08 Cotton ...... 1 .5 Sheep, meat byproducts ...... 0 .08 Cotton, gin byproducts ...... 30 Cranberry ...... 1 .0 (b) Section 18 emergency exemptions. Fruit, citrus, group 10 ...... 0 .80 Fruit, pome ...... 1.5 [Reserved] Grape ...... 3 .0 (c) Tolerances with regional registra- Kiwifruit 1 ...... 0.5 tions. [Reserved] Leaf petioles subgroup 4B ...... 2 .0 Leafy greens subgroup 4A ...... 10 .0 (d) Indirect or inadvertent residues. Nut, tree, group 14 ...... 0 .1 Tolerances are established for indirect Peppermint, tops ...... 10 .0 or inadvertent residues of the insecti- Pistachio ...... 0.1 cide tebufenozide, including its me- Spearmint, tops ...... 10 .0 Turnip, greens ...... 9.0 tabolites and degradates, in or on the Turnip, roots ...... 0 .3 commodities in the table in this para- Vegetable, fruiting, group 8 ...... 1.0 graph when present therein as a result Vegetable, tuberous and corm, except potato, subgroup 1D ...... 0 .015 of the application of tebufenozide to Walnut ...... 0 .1 growing crops listed in the table to 1There are no U.S. registrations on kiwifruit as of June 15, paragraph (a)(1) of this section. Com- 1999. pliance with the tolerance levels speci- (2) Tolerances are established for res- fied in this paragraph is to be deter- idues of the insecticide tebufenozide, mined by measuring only the sum of including its metabolites and tebufenozide, 3,5-dimethylbenzoic acid degradates, in or on the commodities 1-(1,1-dimethylethyl)-2-(4- in the table in this paragraph. Compli- ethylbenzoyl)hydrazide, and its me- ance with the tolerance levels specified tabolite, 3,5-dimethylbenzoic acid 1- in this paragraph is to be determined (1,1-dimethylethyl)-2-(4-(1-hydroxy- by measuring only the sum of ethyl)benzoyl)hydrazide, calculated as tebufenozide, 3,5-dimethylbenzoic acid the stoichiometric equivalent of 1-(1,1-dimethylethyl)-2-(4- tebufenozide, in or on the commodity. ethylbenzoyl)hydrazide, and its me- Parts per tabolites, 3,5-dimethylbenzoic acid 1- Commodity million (1,1-dimethylethyl)-2-((4- Animal feed, nongrass, group 18 ...... 1 .0 carboxymethyl)benzoyl)hydrazide, 3- Grain, cereal, forage, fodder and straw, group hydroxymethyl-5-methylbenzoic acid 1- 16 ...... 1 .0 (1,1-dimethylethyl)-2-(4- Grass, forage, fodder and hay, group 17 ...... 1 .0 ethylbenzoyl)hydrazide, stearic acid Vegetable, foliage of legume, group 7 ...... 0 .20 conjugate of 3-hydroxymethyl-5- methylbenzoic acid 1-(1,1- [60 FR 29347, May 31, 1995] dimethylethyl)-2-(4- EDITORIAL NOTE: For FEDERAL REGISTER ci- ethylbenzoyl)hydrazide, and 3- tations affecting § 180.482, see the List of CFR hydroxymethyl-5-methylbenzoic acid 1- Sections Affected, which appears in the (1,1-dimethylethyl)-2-(4-(1-hydroxy- Finding Aids section of the printed volume ethyl)benzoyl)hydrazide, calculated as and at www.fdsys.gov.

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§ 180.484 Flutolanil; tolerances for res- (d) Indirect or inadvertent residues. idues. Tolerances are established for the indi- (a) General. Tolerances are estab- rect or inadvertent residues of lished for residues of flutolanil, N-(3-(1- flutolanil, N-(3-(1- methylethoxy) phenyl)-2- methylethoxy)phenyl)-2- (trifluoromethyl)benzamide, including (trifluoromethyl)benzamide, including its metabolites and degradates, in or its metabolites and degradates, in or on the commodities in the table below. on the commodities in the table below. Compliance with the tolerance levels Compliance with the tolerance levels specified below is to be determined by specified below is to be determined by measuring only flutolanil and its me- measuring only flutolanil and its metabolites converted to 2- tabolites converted to 2- (trifluoromethyl) benzoic acid and cal- (trifluoromethyl) benzoic acid and calculated as flutolanil, in or on the fol- culated as flutolanil, in or on the following commodities. lowing commodities: Parts per Parts per Commodity million Commodity million Wheat, bran ...... 0.20 Cattle, fat ...... 0.10 Wheat, forage ...... 2 .5 Cattle, kidney ...... 1 .00 Wheat, grain ...... 0 .05 Cattle, liver ...... 2 .00 Wheat, hay ...... 1 .2 Cattle, meat byproducts ...... 0.05 Wheat, straw ...... 0 .20 Cattle, meat ...... 0 .05 Cotton, gin byproducts ...... 0 .20 Cotton, undelinted seed ...... 0 .20 [60 FR 42458, Aug. 16, 1995, as amended at 61 Egg ...... 0 .05 FR 33044, June 26, 1996; 63 FR 42256, 42257, Goat, fat ...... 0 .10 Aug. 7, 1998; 66 FR 10825, Feb. 20, 2001; 71 FR Goat, kidney ...... 1 .00 74818, Dec. 13, 2006; 72 FR 35665, June 29, 2007; Goat, liver ...... 2.00 Goat, meat byproducts ...... 0 .05 73 FR 33017, June 11, 2008; 75 FR 17570, Apr. 7, Goat, meat ...... 0.05 2010; 75 FR 80350, Dec. 22, 2010] Hog, fat ...... 0 .10 Hog, kidney ...... 1.00 § 180.485 Cyproconazole; tolerances for Hog, liver ...... 2 .00 residues. Hog, meat byproducts ...... 0 .05 Hog, meat ...... 0 .05 (a) General. (1) Tolerances are estab- Horse, fat ...... 0 .10 lished for residues of the free and con- Horse, kidney ...... 1 .00 jugated forms of the fungicide Horse, liver ...... 2 .00 Horse, meat byproducts ...... 0 .05 cyproconazole, including its metabo- Horse, meat ...... 0 .05 lites and degradates, in or on the com- Milk ...... 0.05 modities in the table below. Compli- Peanut ...... 0 .5 Peanut, hay ...... 15.0 ance with the proposed tolerance levels Peanut, meal ...... 1 .0 specified below is to be determined by Potato ...... 0 .20 measuring only cyproconazole (a-(4- Potato, wet peel ...... 0 .30 chlorophenyl)-a-(1-cyclopropylethyl)- Poultry, fat ...... 0.05 Poultry, meat ...... 0 .05 1H-1,2,4-triazole-1-ethanol) in or on the Poultry, meat byproducts ...... 0.05 following commodities: Rice, bran ...... 10.0 Rice, grain ...... 7 .0 Commodity Parts per Rice, hulls ...... 25 .0 million Rice, straw ...... 10 .0 Sheep, fat ...... 0 .10 Aspirated grain fractions ...... 2 .5 Sheep, kidney ...... 1.00 Cattle, fat ...... 0.01 Sheep, liver ...... 2.00 Cattle, meat byproducts (except liver) ...... 0 .01 1 Sheep, meat ...... 0.05 Coffee bean, green (Imported) ...... 0 .1 Sheep, meat byproducts ...... 0 .05 Corn, field, forage ...... 0 .60 Soybean, forage ...... 8 .0 Corn, field, grain ...... 0 .01 Soybean, hay ...... 2 .5 Corn, field, stover ...... 1 .2 Goat, fat ...... 0 .01 Soybean, seed ...... 0 .20 Goat, meat byproducts (except liver) ...... 0.01 Turnip, greens ...... 0.1 Horse, fat ...... 0 .01 Vegetable, brassica, leafy, group 5 ...... 0.1 Horse, meat byproducts (except liver) ...... 0 .01 Peanut ...... 0 .01 (b) Section 18 emergency exemptions. Peanut, hay ...... 6.0 [Reserved] Sheep, fat ...... 0 .01 Sheep, meat byproducts (except liver) ...... 0.01 (c) Tolerances with regional registra- Soybean, forage ...... 1 .0 tions. [Reserved] Soybean, hay ...... 3 .0

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(d) Indirect or inadvertent residues. Commodity Parts per million [Reserved] Soybean, oil ...... 0 .10 [63 FR 53835, Oct. 7, 1998, as amended at 71 FR Soybean, seed ...... 0 .05 Wheat, forage ...... 0 .80 71058, Dec. 8, 2006; 73 FR 27760, May 14, 2008; Wheat, grain ...... 0 .05 78 FR 37473, June 21, 2013] Wheat, grain, milled byproducts ...... 0 .10 Wheat, hay ...... 1 .3 § 180.486 Chlorethoxyfos; tolerances Wheat, straw ...... 0 .90 for residues. 1There are no U.S. registrations as of February 15, 2008 for use on coffee bean. (a) General. Tolerances are established for residues of the insecticide (2) A tolerance is established for the chlorethoxyfos, including its metabo- combined residues of the free and con- lites and degradates, in or on the com- jugated forms of the fungicide modities in the table in this paragraph. cyproconazole, including its metabo- Compliance with the tolerance levels lites and degradates, in or on the commodity in the table below. Compliance specified in this paragraph is to be de- with the tolerance level specified below termined by measuring only is to be determined by measuring only chlorethoxyfos, O,O-diethyl O-(1,2,2,2- tetrachloroethyl) phosphorothioate, in the sum of cyproconazole (a-(4- or on the commodity. chlorophenyl)-a-(1-cyclopropylethyl)- 1H-1,2,4-triazole-1-ethanol) and its me- Parts per tabolite d-(4-chlorophenyl)-b,d- Commodity million dihydroxy-g-methyl-1H-1,2,4-triazole-1- hexenoic acid, calculated as the stoi- Corn, field, forage ...... 0 .01 Corn, field, grain ...... 0 .01 chiometric equivalent of Corn, field, stover ...... 0 .01 cyproconazole, in or on the following Corn, pop, grain ...... 0.01 commodity: Corn, pop, stover ...... 0.01 Corn, sweet, forage ...... 0 .01 Parts per Corn, sweet, kernel plus cob with husks re- Commodity million moved ...... 0 .01 Milk ...... 0.02 Corn, sweet, stover ...... 0 .01

(3) Tolerances are established for the (b) Section 18 emergency exemptions. combined residues of the free and con- [Reserved] jugated forms of the fungicide (c) Tolerances with regional registra- cyproconazole, including its metabo- tions. [Reserved] lites and degradates, in or on the com- (d) Indirect or inadvertent residues. modities in the table below. Compli- [Reserved] ance with the tolerance level specified below is to be determined by measuring [76 FR 23498, Apr. 27, 2011] only the sum of cyproconazole (a-(4- § 180.487 Pyrithiobac sodium; toler- chlorophenyl)-a-(1-cyclopropylethyl)- ances for residues. 1H-1,2,4-triazole-1-ethanol) and its metabolite 2-(4-chlorophenyl)-3- (a) General. Tolerances are estab- cyclopropyl-1-[1,2,4]triazol-1-yl-butane- lished for residues of the herbicide, 2,3-diol, calculated as the stoichio- pyrithiobac sodium, (sodium 2-chloro- metric equivalent of cyproconazole, in 6-[(4,6-dimethoxypyrimidin-2- or on the following commodities: yl)thio]benzoate), resulting from the application of the pesticide chemical in Parts per or on the following foods/feeds: Commodity million

Cattle, liver ...... 0 .50 Commodity Parts per Goat, liver ...... 0.50 million Hog, liver ...... 0 .01 Horse, liver ...... 0 .50 Cotton, gin byproducts ...... 0 .15 Sheep, liver ...... 0.50 Cotton, undelinted seed ...... 0 .02

(b) Section 18 emergency exemptions. (b) Section 18 emergency exemptions. [Reserved] [Reserved] (c) Tolerances with regional registra- (c) Tolerances with regional registrations. [Reserved] tions. [Reserved]

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(d) Indirect or inadvertent residues. Commodity Parts per [Reserved] million [62 FR 54783, Oct. 22, 1997, as amended at 64 Goat, fat ...... 0 .1 FR 56469, Oct. 20, 1999; 67 FR 72110, Dec. 4, Goat, kidney ...... 1 .0 Goat, meat byproducts, except kidney ...... 0 .1 2002] Goat, meat ...... 0.1 Horse, fat ...... 0 .1 § 180.490 Imazapic; tolerances for resi- Horse, kidney ...... 1 .0 dues. Horse, meat byproducts, except kidney ...... 0 .1 Horse, meat ...... 0 .1 (a) General. (1) Tolerances are estab- Milk ...... 0.1 lished for residues of the herbicide Sheep, fat ...... 0 .1 imazapic, including its metabolites and Sheep, kidney ...... 1.0 Sheep, meat byproducts, except kidney ...... 0 .1 degradates, in or on the commodities Sheep, meat ...... 0.1 listed in the following table. Compli- ance with the tolerance levels specified (b) Section 18 emergency exemptions. is to be determined by measuring the [Reserved] sum of imazapic (2-[4,5-dihydro-4-meth- (c) Tolerances with regional registra- yl-4-(1-methylethyl)-5-oxo-1H-imidazol- tions. [Reserved] 2-yl]-5-methyl-3-pyridinecarboxylic (d) Indirect or inadvertent residues. acid) and its metabolites (±)-2-[4,5- [Reserved] dihydro-4-methyl-4-(1-methylethyl)-5- [64 FR 54224, Oct. 6, 1999, as amended at 66 FR oxo-1H-imidazol-2-yl]-5- 64774, Dec. 14, 2001; 66 FR 66332, Dec. 26, 2001; hydroxymethyl-3-pyridinecarboxylic 78 FR 49932, Aug. 16, 2013; 79 FR 18818, Apr. 4, acid and (±)-2-[4,5-dihydro-4-methyl-4- 2014; 79 FR 32170, June 4, 2014] (1-methylethyl)-5-oxo-1H-imidazol-2- yl]-5-(b-D-glucopyranosyloxy)methyl-3- § 180.491 Propylene oxide; tolerances pyridinecarboxylic acid, calculated as for residues. the stoichiometric equivalent of (a) General. (1) Tolerances are estab- imazapic. lished for residues of the fumigant propylene oxide, including its metabolites Parts per Commodity million and degradates, in or on the commodities in the table in this paragraph. Grass, forage ...... 15 Compliance with the tolerance levels Grass, hay ...... 30 Peanut ...... 0 .1 specified in this paragraph is to be de- Soybean, seed 1 ...... 0 .40 termined by measuring only propylene Sugarcane, cane 2 ...... 0.03 oxide, when used as a postharvest fumi- 1 There are no US registrations as of April 4, 2014. gant, in or on the commodity. 2 There are no U.S. registrations as of June 4, 2014. Parts per (2) Tolerances are established for res- Commodity million idues of the herbicide imazapic, including its metabolites and degradates, in Cacao bean, cocoa powder ...... 200 Cacao bean, dried bean ...... 200 or on the commodities listed in the fol- Fig ...... 3 .0 lowing table. Compliance with the tol- Garlic, dried ...... 300 erance levels specified is to be deter- Grape, raisin ...... 1 .0 Herbs and spices, group 19, dried ...... 300 mined by measuring the sum of Nut, pine ...... 300 imazapic (2-[4,5-dihydro-4-methyl-4-(1- Nut, tree, group 14 ...... 300 methylethyl)-5-oxo-1H-imidazol-2-yl]-5- Nutmeat, processed, except peanuts ...... 300 Onion, dried ...... 300 methyl-3-pyridinecarboxylic acid) and Pistachio ...... 300 its metabolite (±)-2-[4,5-dihydro-4- Plum, prune, dried ...... 2.0 methyl-4-(1-methylethyl)-5-oxo-1H- imidazol-2-yl]-5-hydroxymethyl-3- (2) Tolerances are established for res- pyridinecarboxylic acid, calculated as idues of the reaction product, pro- the stoichiometric equivalent of pylene chlorohydrin, including its me- imazapic. tabolites and degradates, in or on the commodities in the table in this para- Parts per Commodity million graph. Compliance with the tolerance levels specified in this paragraph is to Cattle, fat ...... 0.10 be determined by measuring only the Cattle, kidney ...... 1 .0 Cattle, meat byproducts, except kidney ...... 0.1 sum of propylene chlorohydrin (1- Cattle, meat ...... 0 .1 chloro-2-propanol), and its isomer 2-

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chloro-1-propanol, calculated as the (d) Indirect or inadvertent residues. stoichiometric equivalent of propylene [Reserved] chlorohydrin (1-chloro-2-propanol), [67 FR 40196, June 12, 2002, as amended at 76 that results from the use of propylene FR 22625, Apr. 22, 2011] oxide as a postharvest fumigant, in or on the commodity. § 180.493 Dimethomorph; tolerances for residues. Parts per Commodity million (a) General. Tolerances are established for the residues of the fungicide Basil, dried leaves ...... 6000 Cacao bean, cocoa powder ...... 20 .0 dimethomorph, (E,Z) 4-[3-(4- Cacao bean, dried bean ...... 20 .0 chlorophenyl)-3-(3,4-dimethoxyphenyl)- Fig ...... 3 .0 1-oxo-2-propenyl]morpholine, in or on Garlic, dried ...... 6000 the following commodities: Grape, raisin ...... 4 .0 Herbs and spices, group 19, dried, except basil 1500 Parts per Nut, pine ...... 10 .0 Commodity million Nut, tree, group 14 ...... 10 .0 Nutmeat, processed, except peanuts ...... 10 .0 Brassica, head and stem, subgroup 5A ...... 6 .0 Onion, dried ...... 6000 Brassica, leafy greens, subgroup 5B ...... 30 .0 Pistachio ...... 10.0 Ginseng ...... 0 .90 Plum, prune, dried ...... 2.0 Grape ...... 3 .0 Grape, raisin ...... 7 .0 Hop, dried cones ...... 60 (b) Section 18 emergency exemptions. Lettuce, head ...... 10 [Reserved] Lettuce, leaf ...... 10 (c) Tolerances with regional registra- Onion, bulb, subgroup 3–07A ...... 0 .6 Onion, green, subgroup 3–07B ...... 15 .0 tions. [Reserved] Potato ...... 0 .05 (d) Indirect or inadvertent residues. Potato, wet peel ...... 0 .20 [Reserved] Taro, corm ...... 0 .5 Taro, leaves ...... 6 .0 [65 FR 33702, May 24, 2000, as amended at 68 Turnip, greens ...... 20.0 FR 39430, July 1, 2003; 72 FR 49651, Aug. 29, Vegetable, cucurbit, group 9 ...... 0.5 2007; 73 FR 54963, Sept. 24, 2008; 76 FR 38037, Vegetable, fruiting, group 8 ...... 1.5 Vegetable, leafy (except Brassica) group 4 ...... 30 .0 June 29, 2011; 77 FR 28495, May 15, 2012]

§ 180.492 Triflusulfuron-methyl; toler- (b) Section 18 emergency exemptions. ances for residues. [Reserved] (c) Tolerances with regional registra- (a) General. Tolerances are estab- tions. Tolerances with regional reg- lished for residues of triflusulfuron- istrations are established for residues methyl, including its metabolites and of the fungicide dimethomorph, (E,Z) 4- degradates, in or on the commodities [3-(4-chlorophenyl)-3-(3,4- listed in the table below. Compliance dimethoxyphenyl)-1-oxo-2-pro- with the tolerance levels specified penyl]morpholine, in or on the fol- below is to be determined by measuring lowing commodities: only triflusulfuron-methyl (methyl 2- [[[[[4-(dimethylamino)-6-(2,2,2- Commodity Parts per trifluoroethoxy)-1,3,5-triazin-2- million yl]amino]carbonyl]amino]sulfonyl]-3- Bean, lima, succulent ...... 0 .60 methylbenzoate) in or on the following commodities: (d) Indirect or inadvertent residues. Tolerances are established for the indi- Parts per Commodity million rect or inadvertent residues of the fungicide dimethomorph, in or on the Beet, garden, roots ...... 0 .01 commodities in the following table. Beet, garden, tops ...... 0 .02 Compliance with the following toler- Beet, sugar, roots ...... 0 .05 Beet, sugar, tops ...... 0.05 ance levels specified in the following Chicory, roots ...... 0 .05 table is to be determined by measuring only dimethomorph (E,Z)-4-[3-(4- (b) Section 18 emergency exemptions. chlorophenyl)-3-(3,4- [Reserved] dimethoxyphenyl)acryloyl]morpholine (c) Tolerances with regional registra- calculated in or on the following com- tions. [Reserved] modities:

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Parts per Revoca- Commodity million Commodity Parts per tion/expira- million tion date Wheat, forage ...... 0 .15 Wheat, hay ...... 0 .15 Strawberry ...... 2.5 None Wheat, straw ...... 0 .4 Tomato ...... 0.15 None

[62 FR 26416, May 14, 1997] (b) Section 18 emergency exemptions. [Reserved] EDITORIAL NOTE: For FEDERAL REGISTER ci- (c) Tolerances with regional registra- tations affecting § 180.493, see the List of CFR tions. Tolerances with regional reg- Sections Affected, which appears in the Finding Aids section of the printed volume istration, as defined in § 180.1(m) are es- and at www.fdsys.gov. tablished for residues of the insecticide pyridaben [2-tert-butyl-5(4-tert- § 180.494 Pyridaben; tolerance for resi- butylbenzylthio)-4-chloropyridazin- dues. 3(2H)-one] in or on the following raw (a) General. Tolerances are estab- agricultural commodity: lished for residues of the insecticide Parts per Expiration pyridaben [2-tert-butyl-5-(4-tert- Commodity million Date butylbenzylthio)-4-chloropyridazin- Cranberry ...... 0.5 None 3(2H)-one] on the following plants, and of the insecticide pyridaben and its me- (d) Indirect or inadvertent residues. tabolites (2-tert-butyl-5-(4-(1-carboxy-1- [Reserved] methylethyl)benzylthio)-4- chloropyridazin-3(2H)-one] and (2-tert- [65 FR 43712, July 14, 2000, as amended at 66 butyl-5-[4(-1,1-dimethyl-2- FR 33199, June 21, 2001; 70 FR 55769, Sept. 23, hypdroxyethyl)benzylthio-4- 2005; 76 FR 56015, Sept. 15, 2010] chloropyridazinn-3(2H)-one) on ani- § 180.495 Spinosad; tolerances for resi- mals, as indicated in the following dues. table. (a) General. Tolerances are established for residues of the insecticide Parts per Revoca- Commodity tion/expira- spinosad in or on the food commodities million tion date in the table to this paragraph. Almond, hulls ...... 4.0 None Spinosad is a fermentation product of Apple ...... 0.5 None Saccharopolyspora spinosa. The product Apple, wet pomace ...... 0.75 None Canistel ...... 0.10 None consists of two related active ingredi- Cattle, fat ...... 0.05 None ents: Spinosyn A (Factor A: CAS # Cattle, meat ...... 0.05 None 131929–60–7) or 2-[(6-deoxy-2,3,4-tri-O Cattle, meat byproducts ...... 0.05 None Citrus ...... 0.5 None -methyl-a-L-manno-pyranosyl)oxy]-13- Citrus, dried pulp ...... 1.5 None [[5-(dimethylamino)-tetrahydro-6- Citrus, oil ...... 10.0 None methyl-2H-pyran-2-yl]oxy]-9-ethyl- Fruit, stone, group 12 ...... 2.5 None Goat, fat ...... 0.0 None 2,3,3a,5a,5b,6,9,10,11,12,13,14,16a,16b- Goat, meat ...... 0.05 None tetradecahydro-14-methyl-1H-as- Goat, meat byproducts ...... 0.05 None Indaceno[3,2-d]oxacyclododecin-7,15- Grape ...... 1.5 None Hog, fat ...... 0.05 None dione; and Spinosyn D (Factor D; CAS Hog, meat ...... 0.05 None # 131929–63–0) or 2-[(6-deoxy-2,3,4-tri-O- Hog, meat byproducts ...... 0.05 None methyl-a-L-manno-pyranosyl)oxy]-13- Hop, dried cones ...... 10.0 None Horse, fat ...... 0.05 None [[5-(dimethyl-amino)-tetrahydro-6- Horse, meat ...... 0.05 None methyl-2H-pyran-2-yl]oxy]-9-ethyl- Horse, meat byproducts ...... 0.05 None 2,3,3a,5a,5b,6,9,10,11,12,13,14,16a,16b- Mango ...... 0.10 None Milk ...... 0.01 None tetradecahydro-4,14-methyl-1H-as- Nut, tree, group 14 ...... 0.05 None Indaceno[3,2-d]oxacyclododecin-7,15- Papaya ...... 0.10 None dione. Pear ...... 0.75 None Pistachio ...... 0.05 None Parts per mil- Sapodilla ...... 0.10 None Commodity lion Sapote, black ...... 0.10 None Sapote, mamey ...... 0.10 None Acerola ...... 1.5 Sheep, fat ...... 0.05 None Alfalfa, seed ...... 0 .15 Sheep, meat ...... 0.05 None Alfalfa, seed screenings ...... 2 .0 Sheep, meat byproduct ...... 0.05 None Almond, hulls ...... 19 Star apple ...... 0.10 None Amaranth, grain, grain ...... 1 .0

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Parts per mil- Parts per mil- Commodity lion Commodity lion

Amaranth, grain, stover ...... 10 Longan ...... 0 .3 Animal feed, nongrass, group, 18 ...... 0.02 Lychee ...... 0 .3 Animal feed, nongrass, group, 18, forage ...... 35.0 Mango ...... 0.3 Animal feed, nongrass, group, 18, hay ...... 30 .0 Milk ...... 7.0 Apple, dry pomace ...... 0.5 Milk, fat ...... 85 Apple, wet pomace ...... 0 .5 Nut, tree, group 14 ...... 0 .10 Artichoke, globe ...... 0.3 Okra ...... 0.40 Asparagus ...... 0.2 Onion, green ...... 2 .0 Atemoya ...... 0 .3 Avocado ...... 0 .3 Papaya ...... 0 .3 Banana ...... 0.25 Passionfruit ...... 0 .3 Beet, sugar, molasses ...... 0 .75 Pea and bean, dried shelled, except soybean, Biriba ...... 0 .3 subgroup 6C ...... 0 .02 Brassica, head and stem, subgroup 5A ...... 2 .0 Pea and bean, succulent shelled, subgroup Brassica, leafy greens, subgroup 5B ...... 10 .0 6B ...... 0 .02 Bushberry subgroup 13B ...... 0 .250 Peanut ...... 0 .02 Caneberry subgroup 13A ...... 0 .7 Peanut, hay ...... 11.0 Canistel ...... 0 .3 Peppermint, tops ...... 3 .5 Cattle, fat ...... 50 Pineapple ...... 0.02 Cattle, liver ...... 10 Pineapple, process residue ...... 0 .08 Cattle, meat ...... 2 .0 Pistachio ...... 0.10 Cattle, meat byproducts, except liver ...... 5 .0 Pomegranate ...... 0 .30 Cherimoya ...... 0 .3 Poultry, fat ...... 1.3 Citrus, oil ...... 3.0 Poultry, meat ...... 0 .10 Citrus, dried pulp ...... 0 .5 Poultry, meat byproducts ...... 0.20 Coriander, leaves ...... 8 .0 Pulasan ...... 0 .3 Corn, sweet, kernel plus cob with husks re- Rambutan ...... 0 .3 moved ...... 0 .02 Rice, hulls ...... 4 .0 Cotton, gin byproducts ...... 1 .5 Cotton, undelinted seed ...... 0 .02 Salal ...... 0 .250 Cranberry ...... 0 .01 Sapodilla ...... 0 .3 Custard apple ...... 0 .3 Sapote, black ...... 0 .3 Date ...... 0 .10 Sapote, mamey ...... 0 .3 Egg ...... 0 .30 Sapote, white ...... 0 .3 Feijoa ...... 05 Sheep, fat ...... 50 Fig ...... 0 .10 Sheep, liver ...... 10 Fish ...... 4 .0 Sheep, meat ...... 2.0 Fish-shellfish, crustacean ...... 4 .0 Sheep, meat byproducts, except liver ...... 5 .0 Fish-shellfish, mollusc ...... 4 .0 Soursop ...... 0 .3 Food commodities ...... 0 .02 Soybean ...... 0.02 Fruit, citrus, group 10 ...... 0 .3 Spanish lime ...... 0 .3 Fruit, pome, group 11 ...... 0.20 Spearmint, tops ...... 3 .5 Fruit, stone, group 12 ...... 0 .20 Spice, subgroup 19B, except black pepper .... 1 .7 Goat, fat ...... 50 Star apple ...... 0 .3 Goat, liver ...... 10 Starfruit ...... 0 .3 Goat, meat ...... 2.0 Strawberry ...... 1 .0 Goat, meat byproducts, except liver ...... 5 .0 Sugar apple ...... 0 .3 Grain, aspirated fractions ...... 200 Ti, leaves ...... 10 .0 Grain, cereal, group 15 ...... 1.5 Vegetable, bulb, group 3, except green onion 0.10 Grain, cereal, group 16, forage, except rice ... 2 .5 Vegetable, cucurbit, group 9 ...... 0.3 Grain, cereal, group 16, hay, except rice ...... 10 .0 Vegetable, foliage of legume, group 7 ...... 8 .0 Grain, cereal, group, 16, stover, except rice ... 10 .0 Vegetable, fruiting, group 8 ...... 0.4 Grain, cereal, group, 16, straw, except rice .... 1 .0 Grape ...... 0 .50 Vegetable, leafy, except brassica, group 4 ..... 8 .0 Grape, raisin ...... 0 .70 Vegetable, leaves of root and tuber, group 2 10 .0 Grass, forage, fodder and hay, group 17, for- Vegetable, legume, edible podded, subgroup age ...... 10 .0 6A ...... 0 .30 Grass, forage, fodder and hay, group 17, hay 5 .0 Vegetable, root and tuber, group 1 ...... 0 .10 Guava ...... 0 .3 Watercress ...... 8 .0 Herb subgroup 19A, dried ...... 22 Wax jambu ...... 0 .3 Herb subgroup 19A, fresh ...... 3.0 Hog, fat ...... 5 .0 (b) Section 18 emergency exemptions. Hog, meat ...... 0 .50 Hog, meat byproducts ...... 2 .0 [Reserved] Hop, dried cones ...... 22 (c) Tolerances with regional registra- Horse, fat ...... 50 tions. [Reserved] Horse, liver ...... 10 (d) Indirect or inadvertant residues. Horse, meat ...... 2 .0 Horse, meat byproducts, except liver ...... 5 .0 [Reserved] Ilama ...... 0 .3 Jaboticaba ...... 0 .3 [72 FR 68540, Dec. 5, 2007, as amended at 74 Juneberry ...... 0 .25 FR 46376, Sept. 9, 2009; 74 FR 48408, Sept. 23, Lingonberry ...... 0.250 2009; 75 FR 60327, Sept. 30, 2010]

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§ 180.496 Thiazopyr; tolerances for res- Expiration/ Commodity Parts per revocation idues. million date Tolerances are established for combined residues of the herbicide Poultry, meat byproducts ...... 0.20 7/14/12 Sheep, fat ...... 0.04 7/14/12 thiazopyr (3-pyridinecaroxylic acid, 2- Sheep, kidney ...... 10.0 7/14/12 (difluoromethyl)-5-(4,5-dihydro-2- Sheep, meat ...... 0.15 7/14/12 thiazolyl)-4-(2-methylpropyl)-6- Sheep, meat byproducts, except (trifluoromethyl)-, methyl ester) and kidney ...... 0.5 7/14/12 its metabolites determined as 2- Wheat, forage ...... 10.0 7/14/12 (difluoromethyl)-6-(trifluoromethyl)- Wheat, grain ...... 250.0 7/14/12 Wheat, hay ...... 40.0 7/14/12 3,4,5-pyridinetricarboxylic acid, all ex- Wheat, straw ...... 50.0 7/14/12 pressed as the parent equivalents in or on the following raw agricultural com- (b) Section 18 emergency exemptions. modities: [Reserved] Parts per (c) Tolerances with regional registra- Commodities million tions. [Reserved] Grapefruit ...... 0 .05 (d) Indirect or inadvertent residues. Orange, sweet ...... 0 .05 Tolerances are established for indirect or inadvertent residues of the plant [62 FR 9978, Mar. 5, 1997] growth regulator (hybridizing agent) clofencet, including its metabolites § 180.497 Clofencet; tolerances for resi- and degradates, in or on the commod- dues. ities in the table in this paragraph. (a) General. Tolerances are estab- Compliance with the tolerance levels lished for residues of the plant growth specified in this paragraph is to be de- regulator (hybridizing agent) clofencet, termined by measuring only clofencet, including its metabolites and potassium 2-(4-chlorophenyl)-3-ethyl- degradates, in or on the commodities 2,5-dihydro-5-oxo-4- in the table in this paragraph. Compli- pyridazinecarboxylate, expressed as the ance with the tolerance levels specified free acid, in or on the commodity when in this paragraph is to be determined present therein as a result of the appli- by measuring only clofencet, potas- cation of clofencet to the growing sium 2-(4-chlorophenyl)-3-ethyl-2,5- dihydro-5-oxo-4-pyridazinecarboxylate, crops in paragraph (a) of this section. expressed as the free acid, in or on the Expiration/ commodity. Commodity Parts per revocation million date Expiration/ Parts per Grain, cereal, forage, fodder and Commodity million revocation date straw, group 16, except rice, sweet corn, wheat, and wild rice; Cattle, fat ...... 0.04 7/14/12 forage ...... 4.0 7/14/12 Cattle, kidney ...... 10.0 7/14/12 Grain, cereal, forage, fodder and Cattle, meat ...... 0.15 7/14/12 straw, group 16, except rice, Cattle, meat byproducts, except kid- sweet corn, wheat, and wild rice; ney ...... 0.5 7/14/12 hay ...... 15.0 7/14/12 Egg ...... 1.0 7/14/12 Grain, cereal, forage, fodder and Goat, fat ...... 0.04 7/14/12 straw, group 16, except rice, Goat, kidney ...... 10.0 7/14/12 sweet corn, wheat, and wild rice; Goat, meat ...... 0.15 7/14/12 stover ...... 1.0 7/14/12 Goat, meat byproducts, except kidney ...... 0.5 7/14/12 Grain, cereal, forage, fodder and Hog, fat ...... 0.04 7/14/12 straw, group 16, except rice, Hog, kidney ...... 10.0 7/14/12 sweet corn, wheat, and wild rice; Hog, meat ...... 0.15 7/14/12 straw ...... 4.0 7/14/12 Hog, meat byproducts, except kid- Grain, cereal group 15, except rice, ney ...... 0.5 7/14/12 sweet corn, wheat, and wild rice 20.0 7/14/12 Horse, fat ...... 0.04 7/14/12 Soybean ...... 30.0 7/14/12 Horse, kidney ...... 10.0 7/14/12 Soybean, forage ...... 10.0 7/14/12 Horse, meat ...... 0.15 7/14/12 Soybean, hay ...... 10.0 7/14/12 Horse, meat byproducts, except kidney ...... 0.5 7/14/12 Milk ...... 0.02 7/14/12 [76 FR 56656, Sept. 14, 2011] Poultry, fat ...... 0.04 7/14/12 Poultry, meat ...... 0.15 7/14/12

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§ 180.498 Sulfentrazone; tolerances for Commodity Parts per residues. million (a)(1) General. Tolerances are estab- Melon, subgroup 9A ...... 0 .15 lished for the combined residues of the Nut, tree, group 14 ...... 0 .15 Pea and bean, dried shelled, except soybean, free and conjugated forms of subgroup 6C ...... 0 .15 sulfentrazone, including its metabo- Pea, succulent ...... 0 .15 lites and degradates, in or on the com- Peanut ...... 0 .20 modities in the table below. Compli- Peanut, meal ...... 0 .40 ance with the tolerance levels specified Peppermint, tops ...... 0 .30 below is to be determined by measuring Pistachio ...... 0.15 Rhubarb ...... 0 .15 only the sum of sulfentrazone (N-[2,4- Spearmint, tops ...... 0 .30 dichloro-5-[4-(difluoromethyl)-4,5- Sugarcane, cane ...... 0.15 dihydro-3-methyl-5-oxo-1H-1,2,4-triazol- Sugarcane, molasses ...... 0 .20 1-yl]phenyl]methanesulfonamide) and Sunflower subgroup 20B ...... 0.20 its metabolite HMS (N-(2,4-dichloro-5- Turnip, roots ...... 0 .15 Turnip, tops ...... 0.60 (4-(difluoromethyl)-4,5-dihydro-3- Vegetable, fruiting, group 8–10 ...... 0 .15 hydroxymethyl-5-oxo-1H-1,2,4-triazol-1- Vegetable, soybean, succulent ...... 0 .15 yl)phenyl)methanesulfonamide, cal- Vegetable, tuberous and corm, subgroup 1C ... 0.15 culated as the stoichiometric equivalent of sulfentrazone in or on the fol- (b) Section 18 emergency exemptions. lowing commodities. [Reserved] (c) Tolerances with regional registra- Parts per Commodity million tions. Tolerances with regional registration are established for the com- Soybean, seed ...... 0 .05 bined residues of the free and conjugated forms of sulfentrazone, includ- (2) Tolerances are established for the ing its metabolites and degradates, in combined residues of the free and con- or on the commodities in the table jugated forms of sulfentrazone, includ- below. Compliance with the tolerance ing its metabolites and degradates, in levels specified below is to be deter- or on the commodities in the table mined by measuring only the sum of below. Compliance with the tolerance sulfentrazone (N-[2,4-dichloro-5-[4- levels specified below is to be deter- (difluoromethyl)-4,5-dihydro-3-methyl- mined by measuring only the sum of 5-oxo-1H-1,2,4-triazol-1- sulfentrazone (N-[2,4-dichloro-5-[4- yl]phenyl]methanesulfonamide) and its (difluoromethyl)-4,5-dihydro-3-methyl- metabolites HMS (N-(2,4-dichloro-5-(4- 5-oxo-1H-1,2,4-triazol-1- (difluoromethyl)-4,5-dihydro-3- yl]phenyl]methanesulfonamide) and its hydroxymethyl-5-oxo-1H-1,2,4-triazol-1- metabolites HMS (N-(2,4-dichloro-5-(4- yl)phenyl)methanesulfonamide) and (difluoromethyl)-4,5-dihydro-3- DMS (N-(2,4-dichloro-5-(4- hydroxymethyl-5-oxo-1H-1,2,4-triazol-1- yl)phenyl)methanesulfonamide) and (difluoromethyl)-4,5-dihydro-5-oxo-1H- DMS (N-(2,4-dichloro-5-(4- 1,2,4-triazol-1- (difluoromethyl)-4,5-dihydro-5-oxo-1H- yl)phenyl)methanesulfonamide, cal- 1,2,4-triazol-1- culated as the stoichiometric equiva- yl)phenyl)methanesulfonamide, cal- lent of sulfentrazone in or on the fol- culated as the stoichiometric equiva- lowing commodities. lent of sulfentrazone in or on the fol- Parts per lowing commodities. Commodity million

Bean, lima, succulent ...... 0 .15 Commodity Parts per million Cowpea, succulent ...... 0 .15 Wheat, forage ...... 0 .50 Asparagus ...... 0.15 Wheat, grain ...... 0 .15 Berry and small fruit, group 13–07 ...... 0 .15 Wheat, hay ...... 0 .30 Brassica, head and stem, subgroup 5A ...... 0 .20 Wheat, straw ...... 1 .5 Brassica, leafy greens, subgroup 5B ...... 0 .40 Corn, field, forage ...... 0 .20 Corn, field, grain ...... 0 .15 (d) Indirect or inadvertent residues. Corn, field, stover ...... 0 .30 Tolerances are established for inad- Flax ...... 0 .15 Fruit, citrus, group 10–10 ...... 0 .15 vertent and indirect combined residues Horseradish ...... 0.20 of the free and conjugated forms of

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sulfentrazone, including its metabo- Commodity Parts per lites and degradates, in or on the com- million modities in the table below. Compli- Lettuce, leaf ...... 90 ance with the tolerance levels specified Potato ...... 0 .06 below is to be determined by measuring Tomato, paste ...... 5 .0 Vegetable, cucurbit, group 9 ...... 1.5 only the sum of sulfentrazone (N-[2,4- Vegetable, fruiting, group 8 ...... 2.0 dichloro-5-[4-(difluoromethyl)-4,5- dihydro-3-methyl-5-oxo-1H-1,2,4-triazol- (b) Section 18 emergency exemptions. 1-yl]phenyl]methanesulfonamide) and [Reserved] its metabolites HMS (N-(2,4-dichloro-5- (c) Tolerance with regional registra- (4-(difluoromethyl)-4,5-dihydro-3- tions. Tolerances with regional reg- hydroxymethyl-5-oxo-1H-1,2,4-triazol-1- istrations are established for the resi- yl)phenyl)methanesulfonamide) and dues of propamocarb, including its me- DMS (N-(2,4-dichloro-5-(4- tabolites and degradates, in or on the (difluoromethyl)-4,5-dihydro-5-oxo-1H- commodities specified in the following 1,2,4-triazol-1- table resulting from the application of yl)phenyl)methanesulfonamide, cal- the hydrochloride salt of propamocarb. culated as the stoichiometric equiva- Compliance with the following toler- lent of sulfentrazone in or on the fol- ance levels is to be determined by lowing commodities when present measuring only propamocarb (propyl therein as a result of the application of N-[3- sulfentrazone to growing crops. (dimethylamino)propyl]carbamate):

Parts per Commodity Parts per Commodity million million

Grain, cereal (excluding sweet corn), Hulls ...... 0 .30 Bean, lima, succulent ...... 2 .0 Grain, cereal, forage, fodder and straw, group 16, except sweet corn; forage ...... 0.2 (d) Indirect or inadvertent residues. Grain, cereal, forage, fodder and straw, group 16, except sweet corn; hay ...... 0.2 [Reserved] Grain, cereal, forage, fodder and straw, group [62 FR 15620, Apr. 2, 1997, as amended at 62 16, except sweet corn; stover ...... 0 .1 Grain, cereal, forage, fodder and straw, group FR 26966, May 16, 1997; 63 FR 32136, June 12, 16, except sweet corn; straw ...... 0 .6 1998; 64 FR 16843, Apr. 7, 1999; 65 FR 58399, Grain, cereal, group 15, except sweet corn ...... 0 .1 Sept. 29, 2000; 66 FR 37598, July 19, 2001; 66 FR Grain, cereal, group 15, except sweet corn; 48585, Sept. 21, 2001; 67 FR 35049, May 17, 2002; bran ...... 0 .15 69 FR 47022, Aug. 4, 2004; 70 FR 7047, Feb. 10, 2005; 78 FR 33736, June 5, 2013] [62 FR 10708, Mar. 10, 1997] § 180.500 Imazapyr; tolerances for resi- EDITORIAL NOTE: For FEDERAL REGISTER ci- dues. tations affecting § 180.498, see the List of CFR Sections Affected, which appears in the (a) General. Tolerances are estab- Finding Aids section of the printed volume lished for residues of the herbicide, and at www.fdsys.gov. imazapyr, including its metabolites and degradates, in or on the commod- § 180.499 Propamocarb; tolerances for ities in the following table. Compliance residues. with the tolerance levels specified in (a) General. Tolerances are estab- the following table is to be determined lished for the residues of propamocarb, by measuring only the residues of including its metabolites and imazapyr [2-[4,5-dihydro-4-methyl-4-(1- degradates, in or on the commodities methylethyl)-5-oxo-1H-imidazol-2-yl]-3- specified in the following table result- pyridinecarboxylic acid]. ing from the application of the hydro- Parts per chloride salt of propamocarb. Compli- Commodity million ance with the following tolerance levels is to be determined by measuring Cattle, fat ...... 0.05 Cattle, kidney ...... 0 .20 only propamocarb (propyl N-[3- Cattle, meat ...... 0 .05 (dimethylamino)propyl]carbamate): Cattle, meat byproducts, except kidney ...... 0.05 Corn, field, forage ...... 0 .05 Parts per Corn, field, grain ...... 0 .05 Commodity million Corn, field, stover ...... 0 .05 Fish ...... 1 .0 Lettuce, head ...... 50 Goat, fat ...... 0 .05

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minimum distance of 3 feet from ex- Commodity Parts per million posed foods. Goat, kidney ...... 0 .20 (2) To assure safe use of the insect Goat, meat ...... 0.05 growth regulator, the label and label- Goats, meat byproducts, except kidney ...... 0 .05 ing shall conform to that registered by Grass, forage ...... 100 Grass, hay ...... 30 the U.S. Environmental Protection Horse, fat ...... 0 .05 Agency, and it shall be used in accord- Horse, kidney ...... 0 .20 ance with such label and labeling. Horse, meat ...... 0 .05 Horse, meat byproducts, except kidney ...... 0 .05 (b) Section 18 emergency exemptions. Lentil 1 ...... 0.2 [Reserved] Milk ...... 0.01 (c) Tolerances with regional registra- Rapeseed subgroup 20A 1 ...... 0 .05 Sheep, fat ...... 0 .05 tions. [Reserved] Sheep, kidney ...... 0.20 (d) Indirect or inadvertent residues. Sheep, meat ...... 0.05 [Reserved] Sheep, meat byproducts, except kidney ...... 0 .05 Shellfish ...... 0 .10 [62 FR 61647, Nov. 19, 1997, as amended at 71 Soybean, meal 1 ...... 4.5 FR 74818, Dec. 13, 2006] Soybean, seed 1 ...... 4 .0 1 Sunflower subgroup 20B ...... 0.05 § 180.502 Aminoethoxyvinylglycine hy- 1 There are no U.S. Registrations. drochloride (aviglycine HCl); toler- (b) Section 18 emergency exemptions. ances for residues. [Reserved] (a) General. Tolerances are estab- (c) Tolerances with regional registra- lished for residues of tions. [Reserved] aminoethoxyvinylglycine hydro- (d) Indirect or inadvertent residues. chloride (aviglycine HCl) in or on the [Reserved] following food commodities:

[68 FR 55484, Sept. 26, 2003, as amended at 78 Parts per FR 66653, Nov. 6, 2013; 79 FR 19487, Apr. 9, Commodity million 2014] Apple ...... 0.08 Fruit, stone, group 12, except cherry ...... 0 .170 § 180.501 Hydroprene; tolerances for Pear ...... 0 .08 residues. (a) General. A tolerance of 0.2 part per (b) Section 18 emergency exemptions. million is established for residues of [Reserved] hydroprene [(S)-(Ethyl (2E,4E,7S)- (c) Tolerances with regional registra- 3,7,11-trimrthyl-2,4-dodecadienoate)], tions. [Reserved] (CAS Reg. No. 65733–18–8) on food com- (d) Indirect or inadvertent residues. modities in food-handling establish- [Reserved] ments in accordance with the following [62 FR 24838, May 7, 1997, as amended at 64 prescribed conditions: FR 31129, June 10, 1999; 66 FR 36481, 36484, (1) Application shall be limited to July 12, 2001; 69 FR 7606, Feb. 18, 2004] spot, crack and crevice, perimeter and ultra low volume (ULV) fogging treat- § 180.503 Cymoxanil, tolerance for resi- ment in food storage or food-handling dues. establishments, including warehouses, (a) General. Tolerances are estab- food service, manufacturing, and proc- lished for residues of the fungicide, essing establishments such as res- cymoxanil, 2-cyano -N- taurants, cafeterias, supermarkets, [(ethylamino)carbonyl]-2- bakeries, breweries, dairies, meat (methoxyimino) acetamide, in or on slaughtering and packing plants, and the following food commodities: canneries where food and food products are held, processed, and served: Pro- Commodity Parts per vided that the food is removed or cov- million ered prior to such use, and food-proc- Caneberry, subgroup 13A-07 ...... 4 .0 essing surfaces are covered during Cilantro, leaves ...... 19 Hop, dried cones ...... 7 .0 treatment or thoroughly cleaned before Leafy greens, subgroup 4A ...... 19 using, or in the case of point-source de- Leaf petioles, subgroup 4B ...... 6 .0 vice treatments, devices must not Lychee 1 ...... 1 .0 Onion, bulb, subgroup 3-07A ...... 0 .05 come into direct contact with food Onion, green, subgroup 3-07B ...... 1 .1 preparation surfaces and must be in a Potato ...... 0 .05

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Parts per Parts per Commodity million Commodity million

Vegetable, cucurbit, group 9 ...... 0.05 Almond, hulls ...... 0 .20 Vegetable, fruiting, group 8 ...... 0.2 Apple, wet pomace ...... 0 .075 Cotton, gin byproducts ...... 0 .050 1 There is no U.S. registration for lychee. Cotton, undelinted seed ...... 0 .025 Fruit, pome, group 11 ...... 0.025 (b) Section 18 emergency exemptions. Grape, wine 1 ...... 0 .03 [Reserved] Nut, tree, group 14 ...... 0 .02 Pistachio ...... 0.02 (c) Tolerances with a regional registra- Tomato, paste ...... 0 .150 tion. Tolerances with a regional reg- Turnip, greens ...... 0.050 istration as defined in § 180.1(l) are es- Vegetable, Brassica, leafy, group 5 ...... 0 .050 Vegetable, cucurbit, group 9 ...... 0.02 tablished for the residues of the fun- Vegetable, fruiting, group 8 ...... 0.020 gicide cymoxanil, 2-cyano -N- Vegetable, leafy, except Brassica, group 4 ...... 0 .100 [(ethylamino)carbonyl]-2- 1 There are no U.S. registrations for use of emamectin on (methoxyimino) acetamide) in or on grape, wine. the raw agricultural commodities: (2) Tolerances are established for emamectin, including its metabolites Parts per Commodity million and degradates, in or on the commodities in the following table. Compliance Grape ...... 0 .10 with the tolerance levels specified in the following table is to be determined (d) Indirect or inadvertent residues. by measuring only the sum of [Reserved] emamectin (MAB1a + MAB1b isomers) and the associated 8,9-Z isomers (8,9- [62 FR 26411, May 14, 1997, as amended at 62 ZB and 8,9-ZB ). FR 39956, July 25, 1997; 63 FR 24949, May 6, 1a 1b 1998; 63 FR 66464, Dec. 2, 1998; 64 FR 6539, Feb. Parts per 10, 1999; 64 FR 47689, Sept. 1, 1999; 66 FR 37598, Commodity million July 19, 2001; 67 FR 35049, May 17, 2002; 68 FR Cattle, fat ...... 0.010 41936, July 16, 2003; 70 FR 7047, Feb. 10, 2005; Cattle, liver ...... 0 .050 72 FR 37646, July 11, 2007; 73 FR 58885, Oct. 8, Cattle, meat ...... 0 .003 2008; 76 FR 34885, June 15, 2011] Cattle, meat byproducts, except liver ...... 0 .020 Goat, fat ...... 0 .010 Goat, liver ...... 0.050 § 180.504 [Reserved] Goat, meat ...... 0.003 Goat, meat byproducts, except liver ...... 0 .020 § 180.505 Emamectin; tolerances for Hog, fat ...... 0 .003 residues. Hog, liver ...... 0 .020 Hog, meat ...... 0 .002 (a) General. (1) Tolerances are estab- Hog, meat byproducts (except liver) ...... 0 .005 lished for emamectin, including its me- Horse, fat ...... 0 .010 Horse, liver ...... 0 .050 tabolites and degradates, in or on the Horse, meat ...... 0 .003 commodities in the table below. Com- Horse, meat byproducts, except liver ...... 0 .020 Milk ...... 0.003 pliance with the tolerance levels speci- Sheep, fat ...... 0 .010 fied below is to be determined by meas- Sheep, liver ...... 0.050 uring only the sum of emamectin (a Sheep, meat ...... 0.003 mixture of a minimum of 90% 4′-epi- Sheep, meat byproducts, except liver ...... 0 .020 ′ methylamino-4 -deoxyavermectin B1a (b) Section 18 emergency exemptions. and maximum of 10% 4′-epi- [Reserved] ′ methylamino-4 -deoxyavermectin B1b) (c) Tolerances with regional registra- and its metabolites 8,9-isomer of the tions. [Reserved] B1a and B1b component of the parent (d) Indirect and inadvertant residues. (8,9-ZMA), or 4′-deoxy-4′-epi-amino- [Reserved] avermectin B1a and 4’-deoxy-4’-epi- ′ ′ [71 FR 18649, Apr. 12, 2006, as amended at 74 amino-avermectin B1b; 4 -deoxy-4 -epi- FR 2873, Jan. 16, 2009; 78 FR 18511, Mar. 27, amino avermectin B1a (AB1a); 4′-deoxy- 2013; 78 FR 49939, Aug. 16, 2013] 4′-epi-(N-formyl-N-methyl)amino- avermectin (MFB1a); and 4′-deoxy-4′- § 180.506 Cyclanilide; tolerances for residues. epi-(N-formyl)amino-avermectin B1a (FAB1a), calculated as the stoichio- (a) General. Tolerances are estab- metric equivalent of emamectin. lished for residues of the plant growth

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regulator, cyclanilide, [1-(2,4- Parts per dichlorophenylaminocarbonyl)- Commodity million cyclopropane carboxylic acid] determined as 2,4-dichloroaniline (cal- Almond, hulls ...... 4 .0 culated as cyclanilide) in or on the fol- Animal feed, nongrass, group 18, forage ...... 45 lowing food commodities and processed Animal feed, nongrass, group 18, hay 120 feed: Artichoke, globe ...... 4 .0 Asparagus ...... 0.04 Parts Per Commodity Million Atemoya ...... 2.0 Avocado ...... 2 .0 Cattle, fat ...... 0.10 Banana ...... * Cattle, meat ...... 0 .02 Barley, bran ...... 6 .0 Cattle, meat byproducts, except kidney ...... 0.2 Barley, forage ...... 25 Cattle, kidney ...... 2 .0 Barley, grain ...... 3 .0 Cotton, undelinted seed ...... 0 .60 Cotton, gin byproducts ...... 25 .0 Barley, hay ...... 10.0 Goat, fat ...... 0 .10 Barley, straw ...... 15.0 Goat, meat ...... 0.02 Berry, low growing, subgroup 13–07G, Goat, meat byproducts, except kidney ...... 0 .20 except cranberry ...... 10.0 Goat, kidney ...... 2 .0 Biriba ...... 2 .0 Horse, fat ...... 0 .10 Brassica, head and stem, subgroup Horse, meat ...... 0 .02 Horse, meat byproducts, except kidney ...... 0 .20 5A ...... 3 .0 Horse, kidney ...... 2 .0 Brassica, leafy greens, subgroup 5B .. 25 Hog, fat ...... 0 .10 Bushberry subgroup 13–07B ...... 5.0 Hog, meat ...... 0 .02 Caneberry subgroup 13–07A ...... 5.0 Hog, meat byproducts, except kidney ...... 0 .20 Canistel ...... 2.0 Hog, kidney ...... 2.0 Cherimoya ...... 2 .0 Milk ...... 0.04 Cilantro, leaves ...... 30 .0 Sheep, fat ...... 0 .10 Sheep, meat ...... 0.20 Citrus, dried pulp ...... 20.0 Sheep, meat byproducts, except kidney ...... 0 .20 Citrus, oil ...... 40.0 Sheep, kidney ...... 2.0 Corn, field, forage ...... 12 .0 Corn, field, grain ...... 0 .05 (b) Section 18 emergency exemptions. Corn, field, refined oil ...... 0 .3 [Reserved] Corn, field, stover ...... 25.0 (c) Tolerances with regional registra- Corn, pop, grain ...... 0 .05 Corn, pop, stover ...... 25.0 tions. [Reserved] Corn, sweet, forage ...... 12.0 (d) Indirect or inadvertent residues. Corn, sweet, kernel plus cob with [Reserved] husks removed ...... 0.05 Corn, sweet, stover ...... 25 .0 [62 FR 28355, May 23, 1997; 62 FR 34182, June Cotton, gin byproducts ...... 45 25, 1997] Cottonseed subgroup 20C ...... 0 .7 Cranberry ...... 0 .50 § 180.507 Azoxystrobin; tolerances for Custard apple ...... 2 .0 residues. Dragon fruit ...... 2 .0 (a) General. (1) Tolerances are estab- Feijoa ...... 2.0 lished for residues of the fungicide, Fruit, citrus, group 10–10 ...... 15.0 azoxystrobin, including its metabolites Fruit, small vine climbing, except and degradates, in or on the commod- fuzzy kiwifruit, subgroup 13–07F ..... 2 .0 Fruit, stone, group 12 ...... 1 .5 ities in the following table. Compliance Ginseng 1 ...... 0 .5 with the tolerance levels specified in Grain, aspirated fractions ...... 420 the table is to be determined by meas- Grass, forage ...... 15 uring only the sum of azoxystrobin, Grass, hay ...... 20 [methyl(E)-2-(2-(6-(2-cyanophenoxy) Guava ...... 2.0 pyrimidin-4-yloxy)phenyl)-3- Herb Subgroup 19A, dried leaves ...... 260 methoxyacrylate], and the Z-isomer of Herb Subgroup 19A, fresh leaves ...... 50 Hop, dried cones ...... 20.0 azoxystrobin [methyl(Z)-2-(2-(6-(2- Ilama ...... 2 .0 cyanophenoxy)pyrimidin-4- Jaboticaba ...... 2 .0 yloxy)phenyl)-3 methoxyacrylate] in or Jackfruit ...... 2.0 on the commodity. Longan ...... 2 .0 Loquat ...... 2.0 Parts per Lychee ...... 2 .0 Commodity million Mango ...... 2 .0 Nut, tree, group 14 ...... 0.02 Acerola ...... 2 .0 Oats, forage ...... 5.0

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Parts per Parts per Commodity million Commodity million

Oats, grain ...... 1 .5 Wasabi, dry ...... 260 Oats, hay ...... 10.0 Wasabi, fresh ...... 50 Oats, straw ...... 3 .0 Watercress ...... 3 .0 Onion, bulb, subgroup 3–07A ...... 1 .0 Wax jambu ...... 2.0 Onion, green, subgroup 3–07B ...... 7.5 Wheat, forage ...... 15.0 Papaya ...... 2 .0 Wheat, grain ...... 0.2 Passionfruit ...... 2 .0 Wheat, hay ...... 30.0 Pawpaw ...... 2 .0 Wheat, straw ...... 10.0 Pea and bean, dried shelled, except soybean, subgroup 6C ...... 0 .5 * 2.0 (of which not more than 0.1 is contained in Pea and bean, succulent shelled, sub- the pulp) 1 group 6B ...... 0.5 There are no United States registrations for use of azoxystrobin on ginseng. Peanut ...... 0.2 Peanut, hay ...... 15 .0 (2) Tolerances are established for res- Peanut, refined oil ...... 0.6 idues of the fungicide, azoxystrobin, in- Pepper/eggplant subgroup 8–10B ...... 3 .0 cluding its metabolites and degradates, Peppermint, tops ...... 30 Persimmon ...... 2 .0 in or on the commodities in the fol- Pistachio ...... 0 .50 lowing table. Compliance with the tol- Pulasan ...... 2 .0 erance levels specified in the table is to Rambutan ...... 2 .0 be determined by measuring only Rapeseed subgroup 20A ...... 1 .0 azoxystrobin, [methyl(E)-2-(2-(6-(2- Rice, grain ...... 5 .0 cyanophenoxy) pyrimidin-4- Rice, hulls ...... 20 yloxy)phenyl)-3-methoxyacrylate] in or Rice, straw ...... 12 on the commodity. Rice, wild, grain ...... 5 .0 Rye, forage ...... 7.0 Parts per Rye, grain ...... 0 .2 Commodity million Rye, straw ...... 1.5 Sapodilla ...... 2 .0 Cattle, fat ...... 0.03 Sapote, black ...... 2 .0 Cattle, meat ...... 0 .01 Sapote, mamey ...... 2.0 Cattle, meat byproducts ...... 0.07 Goat, fat ...... 0 .03 Sapote, white ...... 2 .0 Goat, meat ...... 0.01 Sorghum, grain, forage ...... 25 Goat, meat byproducts ...... 0 .07 Sorghum, grain, grain ...... 11 Hog, fat ...... 0 .010 Sorghum, grain, stover ...... 40 Hog, meat ...... 0 .01 Soursop ...... 2 .0 Hog, meat byproducts ...... 0 .010 Soybean, hay ...... 55.0 Horse, fat ...... 0 .03 Soybean, hulls ...... 1 .0 Horse, meat ...... 0 .01 Soybean, seed ...... 0 .5 Horse, meat byproducts ...... 0 .07 Spanish lime ...... 2 .0 Milk...... 0 .006 Sheep, fat ...... 0 .03 Spearmint, tops ...... 30 Sheep, meat ...... 0.01 Spice Subgroup 19B, except black Sheep, meat byproducts ...... 0 .07 pepper ...... 38 Star apple ...... 2.0 (b) Section 18 emergency exemptions. Starfruit ...... 2.0 [Reserved] Sugar apple ...... 2.0 Sugarcane, cane ...... 0.2 (c) Tolerances with regional registra- Sunflower subgroup 20B ...... 0 .5 tion. [Reserved] Tamarind ...... 2.0 (d) Indirect or inadvertent residues. Tomato, paste ...... 0.6 [Reserved] Tomato subgroup 8–10A ...... 0.2 Turnip, greens ...... 25 [62 FR 32235, June 13, 1997] Vegetable, cucurbit, group 9 ...... 0 .3 EDITORIAL NOTE: For FEDERAL REGISTER ci- Vegetable, foliage of legume, group 7 30.0 tations affecting § 180.507, see the List of CFR Vegetable, leafy, except brassica, Sections Affected, which appears in the group 4 ...... 30.0 Finding Aids section of the printed volume Vegetable, leaves of root and tuber, and at www.fdsys.gov. group 2 ...... 50 .0 Vegetable, legume, edible podded, § 180.509 Mefenpyr-diethyl; tolerance subgroup 6A, except soybean ...... 3 .0 for residues. Vegetable, root, subgroup 1A ...... 0 .5 Vegetable, tuberous and corm, sub- (a) General. Tolerances are estab- group 1C ...... 8.0 lished for residues of the safener,

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mefenpyr-diethyl, including its me- Commodity Parts per tabolites and degradates, when applied million at a rate no greater than 0.053 pound Soybean, forage ...... 0 .1 safener per acre per growing season in Soybean, hay ...... 0 .1 or on the commodities in the table Soybean, seed ...... 0 .02 below. Compliance with the tolerance levels specified below is to be deter- [73 FR 74977, Dec. 10, 2008, as amended at 76 mined by measuring only the sum of FR 23903, Apr. 29, 2011] mefenpyr-diethyl (1-(2,4- dichlorophenyl)-4,5-dihydro-5-methyl- § 180.510 Pyriproxyfen; tolerances for 1H-pyrazole-3,5-dicarboxylic acid, residues. diethyl ester) and its 2,4- (a) General. (1) Tolerances are estab- dichlorophenyl-pyrazoline metabolites, lished for residues of pyriproxyfen, in- calculated as the stoichiometric equiv- cluding its metabolites and degradates, alent of mefenpyr-diethyl, in or on the in or on the commodities in the fol- commodity. lowing table. Compliance with the tolerance levels specified is determined by Parts per Commodity million measuring only pyriproxyfen, 2-[1- methyl-2-(4-phenoxyphenoxy) Barley, grain ...... 0 .05 ethoxy]pyridine, in or on the com- Barley, hay ...... 0 .2 Barley, straw ...... 0 .5 modity. Cattle, meat byproducts ...... 0.1 Goat, meat byproducts ...... 0 .1 Commodity Parts per Grass, forage ...... 1 .6 million Grass, hay ...... 0 .2 Acerola ...... 0.10 Hog, meat byproducts ...... 0 .1 Almond, hulls ...... 2 .0 Horse, meat byproducts ...... 0 .1 Animal feed, nongrass, group 18, forage ...... 0 .70 Sheep, meat byproducts ...... 0 .1 Animal feed, nongrass, group 18, hay ...... 1.1 Sorghum, grain, forage ...... 0.4 Animal feed, nongrass, group 18, seed ...... 2 .0 Sorghum, grain, grain ...... 0 .04 Apple, wet pomace ...... 0 .8 Sorghum, grain, stover ...... 0 .2 Wheat, forage ...... 0 .2 Artichoke, globe ...... 2.0 Wheat, grain ...... 0 .05 Asparagus ...... 2.0 Wheat, hay ...... 0 .2 Atemoya ...... 0 .20 Wheat, straw ...... 0 .5 Avocado ...... 1 .0 Banana ...... 0.20 Beet, sugar, dried pulp ...... 3 .0 (b) Section 18 emergency exemptions. Berry, low growing, except strawberry, sub- [Reserved] group 13–07H ...... 1.0 (c) Tolerances with regional registra- Biriba ...... 0 .20 Brassica, head and stem, subgroup 5A ...... 0 .70 tions. [Reserved] Brassica, leafy greens, subgroup 5B ...... 2 .0 (d) Indirect or inadvertent residues. Bushberry subgroup 13–07B ...... 1 .0 Tolerances are established for the indi- Cacao bean, dried ...... 0 .02 rect or inadvertent residues of Caneberry subgroup 13–07A ...... 1.0 Canistel ...... 1 .0 mefenpyr-diethyl, including its me- Canola, seed ...... 0 .20 tabolites and degradates, when applied Cherimoya ...... 0 .20 at a rate no greater than 0.053 pound Citrus, oil ...... 20 Citrus, dried pulp ...... 2 .0 safener per acre per growing season in Coffee, instant ...... 0 .10 or on the commodities identified in the Coffee, green bean ...... 0 .02 table below. Compliance with the toler- Cotton, gin byproducts ...... 2 .0 Cotton, undelinted seed ...... 0 .05 ance levels specified below is to be de- Custard apple ...... 0 .20 termined by measuring only the sum of Date ...... 0 .30 mefenpyr-diethyl (1-(2,4- Feijoa ...... 0 .10 dichlorophenyl)-4,5-dihydro-5-methyl- Fig ...... 0 .30 Fig, dried fruit ...... 1 .0 1H-pyrazole-3,5-dicarboxylic acid, Fruit, citrus, group 10–10 ...... 0 .50 diethyl ester) and its 2,4- Fruit, pome, group 11–10 ...... 0 .20 dichlorophenyl-pyrazoline metabolites, Fruit, small, vine climbing, except grape, subgroup 13–07E ...... 0 .35 calculated as the stoichiometric equiv- Fruit, stone, group 12 ...... 1 .0 alent of mefenpyr-diethyl, in or on the Grain, cereal, group 15 ...... 1.1 commodity. Grain, cereal, forage, fodder and straw, group 16 ...... 1 .1 Parts per Grape ...... 2 .5 Commodity million Grass, forage, fodder, and hay, group 17, forage ...... 0 .70 Canola, seed ...... 0 .02 Grass, forage, fodder, and hay, group 17, hay 1 .1

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covered or removed from the area Commodity Parts per million being treated prior to application. Guava ...... 0 .10 Food contact surfaces should be thor- Herb subgroup 19A ...... 100 oughly washed with an effective clean- Ilama ...... 0 .20 ing compound and rinced with potable Jaboticaba ...... 0 .10 Lychee ...... 0 .30 water after use of the product. To as- Mango ...... 1.0 sure safe use of this additive, its label Nut, tree, group 14 ...... 0 .02 and labeling shall conform to that reg- Olive ...... 1 .0 Olive, oil ...... 2 .0 istered with the U.S. Environmental Papaya ...... 1 .0 Protection Agency, and shall be used in Passionfruit ...... 0 .10 accordance with such label and label- Pawpaw ...... 1 .0 Peanut ...... 0 .20 ing. Pineapple ...... 0.30 (b) Section 18 emergency exemptions. Pineapple, process residue ...... 1 .1 [Reserved] Pistachio ...... 0.02 Pomegranate ...... 0 .20 (c) Tolerances with regional registra- Potato, chips ...... 0 .75 tions. [Reserved] Potato, granules/flakes ...... 0 .75 (d) Indirect or inadvertent residues. Potato, wet peel ...... 0 .75 [Reserved] Pulasan ...... 0 .30 Rambutan ...... 0 .30 [64 FR 10233, Mar. 3, 1999] Rice, hulls ...... 5 .5 Safflower, seed ...... 0 .20 EDITORIAL NOTE: For FEDERAL REGISTER ci- Sapodilla ...... 1 .0 tations affecting § 180.510, see the List of CFR Sapote, black ...... 1 .0 Sections Affected, which appears in the Sapote, mamey ...... 1 .0 Finding Aids section of the printed volume Sapote, white ...... 0 .30 Sesame, seed ...... 0 .02 and at www.fdsys.gov. Soursop ...... 0 .20 Spanish lime ...... 0 .30 § 180.511 Buprofezin; tolerances for Star apple ...... 1 .0 residues. Starfruit ...... 0 .10 Strawberry ...... 0 .30 (a) General. Tolerances are estab- Sugar apple ...... 0 .20 lished for residues of buprofezin, in- Sugarcane ...... 1 .1 cluding its metabolites and degradates Tea ...... 0 .02 Vegetable, bulb, group 3–07 ...... 0 .70 in or on the commodities in the table Vegetable, cucurbit, group 9 ...... 0.10 below. Compliance with the tolerance Vegetable, foliage of legume, group 7 ...... 2 .0 levels specified below is to be deter- Vegetable, fruiting, group 8–10 ...... 0 .80 Vegetable, leafy, except Brassica, group 4 ...... 3 .0 mined by measuring only the Vegetable, leaves of root and tuber, group 2 ... 2 .0 buprofezin, 2-[(1,1- Vegetable, legume, group 6 ...... 0 .20 dimethylethyl)imino]tetrahydro-3(1- Vegetable, root and tuber, group 1 ...... 0 .15 Walnut ...... 0 .02 methylethyl)-5-phenyl-4H-1,3,5- Watercress ...... 2 .0 thiadiazin-4-one, in the commodity. Wax jambu ...... 0 .10 Commodity Parts per (2) A tolerance of 0.10 parts per mil- million lion is established for all food commod- Acerola ...... 0.30 ities as a result of the proposed use of Almond, hulls ...... 2 .0 Apricot ...... 9 .0 NYLAR in food handling establish- Atemoya ...... 0 .30 ments where food and food products are Avocado ...... 0 .30 held, prepared, processed or served. Ap- Banana ...... 0.20 plication is limited to space, general Bean, snap, succulent ...... 0 .02 Bean, succulent ...... 0 .02 surface, spot, and/or crack and crevice Berry, low growing, subgroup 13-07G ...... 2 .5 treatment in food handling establish- Birida ...... 0 .30 ments where food and food products are Brassica, head and stem, subgroup 5A ...... 12.0 Brassica, leafy greens, subgroup 5B ...... 60 held, processed, prepared and served. Canistel ...... 0 .90 Space and general surface application Cattle, fat ...... 0.05 may be used only when the facility is Cattle, kidney ...... 0 .05 not in operation provided exposed food Cattle, liver ...... 0 .05 Cattle, meat ...... 0 .05 is covered or removed from the area Cattle, meat byproducts ...... 0.05 being treated prior to application. Cherimoya ...... 0 .30 Spot, and/or crack and crevice treat- Citrus, dried pulp ...... 7 .5 Citrus, oil ...... 80 ment may be used while the facility is Coffee, green bean ...... 0 .35 in operation provided exposed food is Cotton, gin byproducts ...... 20 .0

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(d) Indirect or inadvertent residues. Commodity Parts per million [Reserved] Cotton, undelinted seed ...... 0 .35 [62 FR 40741, July 30, 1997] Custard apple ...... 0 .30 Feijoa ...... 0 .30 EDITORIAL NOTE: For FEDERAL REGISTER ci- Fruit, citrus, group 10 ...... 2 .5 Fruit, pome, group 11–10, except pear and tations affecting § 180.511, see the List of CFR pear, Asian ...... 3 .0 Sections Affected, which appears in the Fruit, stone, group 12, except apricot and Finding Aids section of the printed volume peach ...... 1 .9 and at www.fdsys.gov. Goat, fat ...... 0 .05 Goat, kidney ...... 0 .05 Goat, liver ...... 0.05 § 180.512 [Reserved] Goat, meat ...... 0.05 Goat, meat byproducts ...... 0 .05 § 180.513 Chlorfenapyr; tolerances for Grape ...... 2 .5 residues. Guava ...... 0 .3 Hog, fat ...... 0 .05 (a) General. (1) Tolerances are estab- Hog, kidney ...... 0.05 lished for residues of the insecticide Hog, liver ...... 0 .05 Hog, meat ...... 0 .05 chlorfenapyr [4-bromo-2-(4- Hog, meat byproducts ...... 0 .05 chlorophenyl)-1-(ethoxymethyl)-5- Horse, fat ...... 0 .05 Horse, kidney ...... 0 .05 (trifluoromethyl)-1H-pyrrole-3- Horse, liver ...... 0 .05 carbonitrile] in or on the following raw Horse, meat ...... 0 .05 agricultural commodities: Horse, meat byproducts ...... 0 .05 Ilama ...... 0 .30 Parts per Jaboticaba ...... 0 .30 Commodity million Lettuce, head ...... 6.0 Longan ...... 0 .30 Vegetable, fruiting, group 8 ...... 1.0 Lychee ...... 0 .30 Mango ...... 0.90 Milk ...... 0.01 (2) A tolerance of 0.01 parts per mil- Nut, tree group 14 ...... 0.05 lion is established for residues of Olive ...... 3 .5 Olive, oil ...... 4 .8 chlorfenapyr in or on all food commod- Papaya ...... 0 .90 ities (other than those covered by a Passionfruit ...... 0 .30 higher tolerance as a result of use on Peach ...... 9 .0 Pear ...... 6 .0 growing crops) in food/feed handling Pear, Asian ...... 6 .0 areas where food/feed products are pre- Persimmon ...... 1 .9 Pistachio ...... 0.05 pared, held, processed, or served and in Pomegranate ...... 1 .9 accordance with the following pre- Pulasan ...... 0 .30 scribed conditions: Radicchio ...... 6.0 Rambutan ...... 0 .30 (i) Application shall be no greater Sapodilla ...... 0 .90 than a 0.5% active ingredient solution Sapote, black ...... 0 .90 for spot crack and crevice use in food/ Sapote, mamey ...... 0 .90 Sheep, fat ...... 0 .05 feed handling establishments, where Sheep, kidney ...... 0.05 food and food products are held, proc- Sheep, liver ...... 0.05 essed, prepared and/or served. Sheep, meat ...... 0.05 Sheep, meat byproducts ...... 0 .05 (ii) Application may only be under- Soursop ...... 0 .30 taken when the facility is not in oper- Spanish lime ...... 0 .30 ation, and provided exposed food has Star apple ...... 0 .90 Starfruit ...... 0 .30 been covered, or removed from the area Sugar apple ...... 0 .30 being treated prior to application. Tea1 ...... 20 (iii) Food contact surfaces and equip- Turnip, greens ...... 60 Vegetable, cucurbit, group 9 ...... 0.50 ment should be throughly washed with Vegetable, fruiting, group 8–10 ...... 2 .0 an effective cleaning compound, and Vegetable, leafy, except Brassica, group 4, except head lettuce and radicchio ...... 35 rinsed with potable water after each Wax jambu ...... 0 .30 use of the product. 1 There are no U.S. registrations at this time. (iv) Contamination of food or food contact surfaces shall be avoided. Ap- (b) Section 18 emergency exemption. plication excludes any direct applica- [Reserved] tion to any food, food packaging, or (c) Tolerances with regional registra- any food contact surfaces. tions. [Reserved]

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(v) To assure safe use, the label and oxo-1H-1,2,4-triazol-1-yl]-4- labeling shall conform to that reg- fluorobenzenepropanoic acid), cal- istered by the U.S. Environmental Pro- culated as the stoichiometric equiva- tection Agency, and it shall be used in lent of carfentrazone-ethyl, in or on accordance with such label and label- the following commodities: ing. Parts per (b) Section 18 emergency exemptions. Commodity million [Reserved] (c) Tolerances with regional registra- Acerola ...... 0.10 Almond, hulls ...... 0 .20 tions. [Reserved] Animal feed, nongrass, crop group 18, forage 2 .0 (d) Indirect or inadvertent residues. Animal feed, nongrass, crop group 18, hay ...... 5 .0 [Reserved] Animal feed, nongrass, crop group 18, seed .... 15 .0 Atemoya ...... 0 .10 [68 FR 55527, Sept. 26, 2003, as amended at 70 Avocado ...... 0 .10 FR 3654, Jan. 26, 2005] Banana ...... 0.20 Barley, bran ...... 0 .80 Barley, flour ...... 0 .80 § 180.514 Cloransulam-methyl; toler- Berry group 13 ...... 0 .10 ances for residues. Birida ...... 0 .10 Borage ...... 0 .10 (a) General. Tolerances are estab- Cacao bean, bean ...... 0 .10 lished for residues of the herbicide, Cactus ...... 0 .10 cloransulam-methyl, N-(2- Caneberry subgroup 13A ...... 0 .1 carboxymethyl-6-chlorophenyl)-5- Canistel ...... 0 .10 Canola ...... 0 .10 ethoxy-7-fluoro-(1,2,4)-triazolo[1,5c]-py- Cattle, fat ...... 0.10 rimidine-2-sulfonamide, plus its acid, Cattle, meat ...... 0 .10 cloransulam, calculated as parent ester Cattle, meat byproducts ...... 0.10 Cherimoya ...... 0 .10 in or on the following raw agricultural Coconut ...... 0 .10 commodities: Coffee, bean, green ...... 0 .10 Corn, field, forage ...... 0 .20 Corn, sweet, forage ...... 0 .20 Commodity Parts per million Corn, sweet, kernel plus cob with husk removed ...... 0 .10 Soybean, forage ...... 0 .1 Cotton, gin byproducts ...... 10 Soybean, hay ...... 0 .2 Cotton, undelinted seed ...... 0 .20 Soybean, seed ...... 0 .02 Cotton, hulls ...... 0 .60 Cotton, meal ...... 0 .35 (b) Section 18 emergency exemptions. Cotton, refined oil ...... 1.0 [Reserved] Crambe, seed ...... 0.10 Custard apple ...... 0 .10 (c) Tolerances with regional registra- Date, dried fruit ...... 0 .10 tions. [Reserved] Feijoa ...... 0 .10 (d) Indirect or inadvertent residues. Fig ...... 0 .10 Fish ...... 0 .30 [Reserved] Flax, seed ...... 0 .10 [62 FR 49163, Sept. 19, 1997] Fruit, citrus, group 10 ...... 0 .10 Fruit, pome, group 11 ...... 0.10 Fruit, stone, group 12 ...... 0 .10 § 180.515 Carfentrazone-ethyl; toler- Goat, fat ...... 0 .10 ances for residues. Goat, meat ...... 0.10 Goat, meat byproducts ...... 0 .10 (a) General. Tolerances are estab- Grain, aspirated grain fractions ...... 1 .8 lished for residues of the herbicide Grain, cereal, forage, fodder and straw group carfentrazone-ethyl, including its me- 16, except corn and sorghum; forage ...... 1 .0 tabolites and degradates, in or on the Grain, cereal, forage, fodder and straw, group 16, hay ...... 0 .30 commodities listed in the following Grain, cereal, forage, fodder and straw, group table. Compliance with the following 16, stover ...... 0 .30 tolerance levels is to be determined by Grain, cereal, forage, fodder and straw, group 16, except rice; straw ...... 0.10 measuring only the sum of Grain, cereal, group 15 ...... 0.10 carfentrazone-ethyl (ethyl-alpha-2- Grain, cereal, group 15 (except rice grain and dichloro-5-[-4-(difluoromethyl)-4,5- sorghum grain) ...... 0 .10 dihydro-3-methyl-5-oxo-1H -1,2,4- Grain, cereal, stover ...... 0 .80 Grain, cereal, straw ...... 3 .0 triazol-1-yl]-4- Grape ...... 0 .10 fluorobenzenepropanoate) and its me- Grass, forage ...... 5 .0 tabolite carfentrazone-chloropropionic Grass, hay ...... 8 .0 Guava ...... 0 .10 acid (alpha, 2-dichloro-5-[-4- Herbs and spices group 19 ...... 2.0 difluoromethyl)-4,5-dihydro-3-methyl-5- Hog, fat ...... 0 .10

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Parts per Parts per Commodity million Commodity million

Hog, meat ...... 0 .10 Vegetable, bulb, group 3 ...... 0 .10 Hog, meat byproducts ...... 0 .10 Vegetable, cucurbit, group 9 ...... 0.10 Hop, dried cones ...... 0 .10 Vegetable, foliage of legume, except soybean, Horse, fat ...... 0 .10 subgroup 7A ...... 0 .10 Horse, meat ...... 0 .10 Vegetable, fruiting, group 8 ...... 0.10 Horse, meat byproducts ...... 0 .10 Vegetable, leafy, except brassica, group 4 ...... 0 .10 Horseradish ...... 0.10 Vegetable, leaves of root and tuber, group 2 ... 0 .10 Ilama ...... 0 .10 Vegetable, legume, group 6 ...... 0 .10 Jaboticaba ...... 0 .10 Vegetable, root and tuber, group 1 ...... 0 .10 Juneberry ...... 0 .10 Wasaba, roots ...... 0.10 Kava, roots ...... 0 .10 Wax jambu ...... 0 .10 Kiwifruit ...... 0.10 Wheat, bran ...... 0.80 Lingonberry ...... 0.10 Wheat, flour ...... 0 .80 Longan ...... 0 .10 Wheat, germ ...... 0 .80 Lychee ...... 0 .10 Wheat, middlings ...... 0 .80 Mango ...... 0.10 Wheat, shorts ...... 0 .80 Milk ...... 0.05 Millet, flour ...... 0 .80 (b) Section 18 emergency exemptions. Mustard, seed ...... 0 .10 [Reserved] Noni ...... 0 .10 Nut, tree, group 14 ...... 0 .10 (c) Tolerances with regional registra- Oat, flour ...... 0 .80 tions. [Reserved] Okra ...... 0.10 (d) Indirect or inadvertent residues. Olive ...... 0 .10 Palm heart ...... 0 .10 [Reserved] Palm heart, leaves ...... 0 .10 [63 FR 52180, Sept. 30, 1998] Papaya ...... 0 .10 Passionfruit ...... 0 .10 EDITORIAL NOTE: For FEDERAL REGISTER ci- Pawpaw ...... 0 .10 tations affecting § 180.515, see the List of CFR Peanut ...... 0 .10 Sections Affected, which appears in the Peanut, hay ...... 0.10 Persimmon ...... 0 .10 Finding Aids section of the printed volume Pistachio ...... 0.10 and at www.fdsys.gov. Pomegranate ...... 0 .10 Poultry, meat byproducts ...... 0.10 § 180.516 Fludioxonil; tolerances for Pulasan ...... 0 .10 residues. Pummelo ...... 0 .10 Rambutan ...... 0 .10 (a) General. (1) Tolerances are estab- Rapeseed, forage ...... 0 .10 lished for residues of the fungicide Rapeseed, seed ...... 0 .10 fludioxonil, including its metabolites Rice, grain ...... 1 .3 Rice, hulls ...... 3 .5 and degradates, in or on the commod- Rice, straw ...... 1 .0 ities in the following table. Compliance Rye, bran ...... 0 .80 with the tolerance levels specified in Rye, flour ...... 0 .80 Safflower, seed ...... 0 .10 the following table is to be determined Salal ...... 0 .10 by measuring only fludioxonil, 4-(2,2- Sapodilla ...... 0 .10 difluoro-1,3-benzodioxol-4-yl)-1-H- Sapote, black ...... 0 .10 pyrrole-3-carbonitrile). Sapote, mamey ...... 0 .10 Sheep, fat ...... 0 .10 Parts per Sheep, meat ...... 0.10 Commodity million Sheep, meat byproducts ...... 0 .10 Shellfish ...... 0 .30 Acerola ...... 5.0 Sorghum, forage ...... 0 .20 Animal feed, nongrass, group 18 ...... 0 .01 Sorghum, grain ...... 0 .25 Atemoya ...... 20 Sorghum, sweet ...... 0 .10 Avocado ...... 5 .0 Soursop ...... 0 .10 Bean, dry ...... 0.4 Soybean, seed ...... 0 .10 Bean, succulent ...... 0 .4 Spanish lime ...... 0 .10 Beet, sugar, roots ...... 0 .02 Star apple ...... 0 .10 Berry, low growing, subgroup 13–07G, except Starfruit ...... 0 .10 cranberry ...... 3.0 Stevia ...... 0 .10 Biriba ...... 20 Strawberry ...... 0 .10 Brassica, head and stem, subgroup 5A ...... 2 .0 Strawberrypear ...... 0 .10 Brassica, leafy greens, subgroup 5B ...... 10 Sugar apple ...... 0 .10 Bushberry subgroup 13–07B ...... 2 .0 Sugarcane ...... 0 .15 Caneberry subgroup 13–07A ...... 5.0 Sunflower, seed ...... 0.10 Canistel ...... 5 .0 Tea, dried ...... 0 .10 Cherimoya ...... 20 Ti, leaves ...... 0 .10 Citrus, oil ...... 500 Ti, roots ...... 0 .10 Cotton, gin byproducts ...... 0 .05 Vanilla ...... 0 .10 Cotton, undelinted seed ...... 0 .05 Vegetable, brassica, leafy, group 5 ...... 0.10 Custard apple ...... 20

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difluoro-1,3-benzodioxol-4-yl)-1-H- Commodity Parts per million pyrrole-3-carbonitrile), and its metabo- Dragon fruit ...... 1 .0 lites converted to 2,2-difluoro-l,3- Feijoa ...... 5 .0 benzodioxole-4-carboxylic acid, cal- Flax, seed ...... 0 .05 culated as the stoichiometric equiva- Fruit, citrus, group 10–10 ...... 10 Fruit, pome, group 11–10 ...... 5 .0 lent of fludioxonil. Fruit, small vine climbing, except fuzzy kiwifruit, subgroup 13–07F ...... 2 .0 Commodity Parts per Fruit, stone, group 12 ...... 5 .0 million Ginseng ...... 4 .0 Cattle, fat ...... 0.05 Grain, cereal, group 15 ...... 0.02 Cattle, meat ...... 0 .01 Grain, cereal, forage, fodder, and straw, group Cattle, meat byproducts ...... 0.05 16 ...... 0 .01 Goat, fat ...... 0 .05 Grass, forage, fodder and hay, group 17 ...... 0 .01 Goat, meat ...... 0.01 Guava ...... 5 .0 Goat, meat byproducts ...... 0 .05 Herb subgroup 19A, dried leaves ...... 65 Horse, fat ...... 0 .05 Herb subgroup 19A, fresh leaves ...... 10 Horse, meat ...... 0 .01 Ilama ...... 20 Horse, meat byproducts ...... 0 .05 Jaboticaba ...... 5 .0 Milk ...... 0.01 Kiwifruit, fuzzy ...... 20 Sheep, fat ...... 0 .05 Leaf petioles subgroup 4B ...... 15 Sheep, meat ...... 0.01 Leafy greens subgroup 4A ...... 30 Sheep, meat byproducts ...... 0 .05 Longan ...... 20 Lychee ...... 20 Mango ...... 5.0 (b) Section 18 emergency exemptions. Melon subgroup 9A ...... 0 .03 [Reserved] Onion, bulb, subgroup 3–07A ...... 0 .50 (c) Tolerances with regional registra- Onion, green, subgroup 3–07B ...... 7 .0 Papaya ...... 5 .0 tions. [Reserved] Passionfruit ...... 5 .0 (d) Indirect or inadvertent residues. Peanut ...... 0 .01 [Reserved] Peanut, hay ...... 0.01 Pineapple ...... 20 [62 FR 56082, Oct. 29, 1997] Pistachio ...... 0.10 Pomegranate ...... 5 .0 EDITORIAL NOTE: For FEDERAL REGISTER ci- Pulasan ...... 20 tations affecting § 180.516, see the List of CFR Rambutan ...... 20 Sections Affected, which appears in the Rapeseed, forage ...... 0 .01 Finding Aids section of the printed volume Rapeseed, seed ...... 0 .01 and at www.fdsys.gov. Safflower, seed ...... 0 .01 Sapodilla ...... 5 .0 Sapote, black ...... 5 .0 § 180.517 Fipronil; tolerances for resi- Sapote, mamey ...... 5 .0 dues. Soursop ...... 20 Spanish lime ...... 20 (a) General. Therefore, tolerances are Spice subgroup 19B ...... 0 .02 established for combined residues of Star apple ...... 5 .0 the insecticide fipronil (5-amino-1-[2,6- Starfruit ...... 5 .0 Sugar apple ...... 20 dichloro-4-(trifluoromethyl)phenyl]-4- Sunflower, seed ...... 0.01 [(1R,S)-(trifluoromethyl)sulfinyl]-1H- Tomato ...... 5.0 pyrazole-3-carbonitrile) and its me- Turnip, greens ...... 10 tabolites 5-amino-1-[2,6-dichloro-4- Vegetable, cucurbit, group 9 ...... 0.45 Vegetable, foliage of legume, group 7 ...... 0 .01 (trifluoromethyl)phenyl]-4- Vegetable, fruiting, group 8–10, except tomato .. 0 .50 [(trifluoromethyl) sulfonyl]-1H-pyr- Vegetable, leaves of root and tuber, group 2 ..... 30 azole-3-carbonitrile and 5-amino-1-[2,6- Vegetable, legume, group 6 ...... 0 .01 Vegetable, root, except sugar beet, subgroup dichloro-4-(trifluoromethyl) phenyl]-4- 1B ...... 0 .75 [(trifluoromethyl)thio]-1H-pyrazole-3- Vegetable, tuberous and corm, subgroup 1C ..... 6.0 carbonitrile and its photodegradate 5- Watercress ...... 7 .0 Wax jambu ...... 5 .0 amino-1-(2,6-dichloro-4- Yam, true, tuber ...... 8.0 (trifluoromethyl)phenyl]-4-[(1R,S)- (trifluoromethyl)]-1H-pyrazole-3- (2) Tolerances are established for res- carbonitrile in or on the following idues of the fungicide fludioxonil, in- items at the levels specified: cluding its metabolites and degradates, Parts per in or on the commodities in the fol- Commodity million lowing table. Compliance with the tolerance levels specified in the following Cattle, fat ...... 0.40 Cattle, liver ...... 0 .10 table is to be determined by measuring Cattle, meat ...... 0 .04 only the sum of fludioxonil, 4-(2,2- Cattle, meat byproducts, except liver ...... 0 .04

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(d) Indirect or inadvertent residues. Commodity Parts per million Tolerances are established for com- Corn, field, grain ...... 0 .02 bined indirect or inadvertent residues Corn, field, stover ...... 0 .30 of the insecticide fipronil and its me- Corn, field, forage ...... 0 .15 tabolites and photodegradate in or on Egg ...... 0 .03 food commodities when present therein Goat, fat ...... 0 .40 Goat, liver ...... 0.10 as a result of the application of fipronil Goat, meat ...... 0.04 to growing crops listed in paragraphs Goat, meat byproducts, except liver ...... 0 .04 (a) and (b) of this section and other Hog, fat ...... 0 .04 nonfood crops to read as follows: Hog, liver ...... 0 .02 Hog, meat ...... 0 .01 Parts per Hog, meat byproducts, except liver ...... 0 .01 Commodity million Horse, fat ...... 0 .40 Horse, liver ...... 0 .10 Wheat, forage ...... 0 .02 Horse, meat ...... 0 .04 Wheat, grain ...... 0 .005 Horse, meat byproducts, except liver ...... 0 .04 Wheat, hay ...... 0 .03 Milk, fat (reflecting 0.05 ppm in whole milk) ..... 1 .50 Wheat, straw ...... 0 .03 Potato ...... 0 .03 Potato, wet peel ...... 0 .10 Poultry, fat ...... 0.05 [62 FR 62979, Nov. 26, 1997, as amended at 63 Poultry, meat ...... 0 .02 FR 38495, July 17, 1998; 72 FR 46913, Aug. 22, Poultry, meat byproducts ...... 0.02 2007; 74 FR 46377, Sept. 9, 2009; 75 FR 80346, Rice, grain ...... 0 .04 Dec. 22, 2010; 78 FR 78748, Dec. 27, 2013] Rice, straw ...... 0 .10 Sheep, fat ...... 0 .40 § 180.518 Pyrimethanil; tolerances for Sheep, liver ...... 0.10 residues. Sheep, meat ...... 0.04 Sheep, meat byproducts, except liver ...... 0 .04 (a) General. (1) Tolerances are established for residues of the fungicide (b) Section 18 emergency exemptions.. pyrimethanil, including its metabolites Time-limited tolerances are estab- and degradates, in or on the commod- lished for combined residues of the in- ities in the following table Compliance secticide, fipronil, 5-amino-1-(2,6- with the tolerance levels specified in dichloro-4-(trifluoromethyl) phenyl)-4- the following table is to be determined ((1,R,S)-trifluoromethyl)sulfinyl)-1-H- by measuring only pyrimethanil (4,6-di- pyrazole-3-carbonitrile and its 2 me- methyl-N-phenyl-2-pyrimidinamine). tabolites MB45950 (5-amino-1-(2,6- dichloro-4-(trifluoromethyl)phenyl)-4- Parts per Commodity million [(trifluoromethyl)thio]-1H-pyrazole-3- carbonitrile) and MB46136 (5-amino-1- Almond ...... 0.20 (2,6-dichloro-4- Almond, hulls ...... 12 Apple, wet pomace ...... 40 (trifluoromethyl)phenyl)-4- Banana ...... 0.10 [(trifluoromethyl)sulfonyl]-1H-pyr- Berry, low growing, subgroup 13–07G ...... 3 .0 azole-3-carbonitrile) and its Citrus, oil ...... 150 Fruit, citrus, group 10, except lemon, photodegradate MB46513 (5-amino-1- postharvest ...... 10 (2,6-dichloro-4- Fruit, pome, group 11 (pre-harvest and post- (trifluoromethyl)phenyl]-4-[(1R,S)- harvest) ...... 14 Fruit, small, vine climbing, subgroup 13–07F, (trifluoromethyl)]-1H-pyrazole-3- except fuzzy kiwifruit ...... 5 .0 carbonitrile), in connection with use of Fruit, stone, group 12 ...... 10 the pesticide under Section 18 emer- Ginseng ...... 1 .5 gency exemptions granted by EPA. The Grape, raisin ...... 8 .0 Lemon, preharvest and postharvest ...... 11 tolerances expire and are revoked on Onion, bulb, subgroup 3–07A ...... 2 .0 the dates specified in the table for this Onion, green, subgroup 3–07B ...... 3 .0 paragraph. Pistachio ...... 0.20 Tomato ...... 0.50 Vegetable, tuberous and corm, subgroup 1C ... 0.05 Parts per Expiration/ Commodity million revocation date (2) Tolerances are established for res- Rutabaga ...... 1.0 12/31/16 idues of the fungicide pyrimethanil, in- Turnip ...... 1.0 12/31/16 cluding its metabolites and degradates, in or on the commodities in the fol- (c) Tolerances with regional registra- lowing table. Compliance with the tol- tions. [Reserved] erance levels specified in the following

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table is to be determined by measuring resin (as a source of bromine) under the only the sum of pyrimethanil and its supervision of trained personnel. metabolite 4-[4,6-dimethyl-2- (2) Residual bromine levels are con- pyrimidinyl)amino]phenol, calculated trolled to not exceed 1.0 part per mil- as the stoichiometric equivalent of lion (ppm) in the final treated water. pyrimethanil. Control is effected using calibrated re- Parts per circulating or proportioning bromine Commodity million feeder equipment and periodic checks

Cattle, fat ...... 0.01 of residual bromine using a bromine Cattle, kidney ...... 2 .5 test kit. To assure safe use of the addi- Cattle, meat ...... 0 .01 tives, the label and labeling of the dis- Cattle, meat byproducts, except kidney ...... 0.01 Goat, fat ...... 0 .01 infectant formulation containing the Goat, kidney ...... 2 .5 food additives shall conform to the Goat, meat ...... 0.01 label and labeling registered by the Goat, meat byproducts, except kidney ...... 0 .01 Horse, fat ...... 0 .01 U.S. Environmental Protection Agen- Horse, kidney ...... 2 .5 cy. Horse, meat ...... 0 .01 (3) No tolerance is established for Horse, meat byproducts, except kidney ...... 0 .01 Sheep, fat ...... 0 .01 bromide ion levels. Sheep, kidney ...... 2.5 (b) Section 18 emergency exemptions. Sheep, meat ...... 0.01 Sheep, meat byproducts, except kidney ...... 0 .01 [Reserved] (c) Tolerances with regional registra- (3) Tolerances are established for res- tions. [Reserved] idues of the fungicide pyrimethanil, in- (d) Indirect or inadvertent residues. cluding its metabolites and degradates, [Reserved] in or on the commodities in the following table. Compliance with the tol- [41 FR 17893, Apr. 29, 1976. Redesignated at 41 erance levels specified in the following FR 26568, June 28, 1976, and at 53 FR 24667, June 29, 1988. Redesignated and amended at table is to be determined by measuring 63 FR 34319, June 24, 1998; 71 FR 74818, Dec. only the sum of pyrimethanil and its 13, 2006] metabolite 4,6-dimethyl-2- (phenylamino)-5-pyrimidinol, cal- § 180.521 Fumigants for grain-mill ma- culated as the stoichiometric equiva- chinery; tolerances for residues. lent of pyrimethanil. (a) General. Fumigants may be safely

Commodity Parts per used in or on grain-mill machinery in million accordance with the following pre- Milk ...... 0.05 scribed conditions: (1) The fumigants consist of methyl (b) Section 18 emergency exemptions. bromide. [Reserved] (2) To assure safe use of the fumi- (c) Tolerances with regional registra- gant, its label and labeling shall con- tions. [Reserved] form to the label and labeling reg- (d) Indirect or inadvertent residues. istered by the U.S. Environmental Pro- [Reserved] tection Agency. [62 FR 63669, Dec. 2, 1997, as amended at 69 (3) Residues of inorganic bromides FR 52443, Aug. 26, 2004; 73 FR 64251, Oct. 29, (calculated as Br) in milled fractions 2008; 74 FR 32448, July 8, 2009; 77 FR 45503, derived from cereal grain from all fu- Aug. 1, 2012] migation sources, including fumigation § 180.519 Bromide ion and residual of grain-mill machinery, shall not ex- bromine; tolerances for residues. ceed 125 parts per million. (a) General. The food additives, bro- (b) Section 18 emergency exemptions. mide ion and residual bromine, may be [Reserved] present in water, potable in accordance (c) Tolerances with regional registra- with the following conditions: tions. [Reserved] (1) The food additives are present as a result of treating water aboard ships with a polybrominated ion-exchange

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(d) Indirect or inadvertent residues. uring only metaldehyde, 2,4,6,8- [Reserved] tetramethyl-1,3,5,7-tetroxocane, in or on the commodity. [40 FR 14156, Mar. 28, 1975. Redesignated at 41 FR 26568, June 28, 1976, as amended at 49 FR Parts per 44459, Nov. 7, 1984. Further redesignated at 53 Commodity million FR 24667, June 29, 1988, as amended at 54 FR 6130, Feb. 8, 1989. Further redesignated and Artichoke, globe ...... 0.07 amended at 63 FR 34319, June 24, 1998] Berry, low growing, subgroup 13–07G ...... 6 .25 Bushberry subgroup 13–07B ...... 0 .15 Cactus ...... 0 .07 § 180.522 Fumigants for processed Caneberry subgroup 13–07A ...... 0.15 grains used in production of fer- Corn, field, forage ...... 0 .30 mented malt beverage; tolerances Corn, field, grain ...... 0 .05 for residues. Corn, field, stover ...... 0 .10 Corn, sweet, forage ...... 0 .30 (a) General. Fumigants for processed Corn, sweet, kernel plus cob with husks re- grain may be safely used, in accordance moved ...... 0 .05 Corn, sweet, stover ...... 0 .10 with the following conditions. Fruit, citrus, group 10 ...... 0 .26 (1) Methyl bromide. Total residues of Grass, forage ...... 2 .0 inorganic bromides (calculated as Br) Grass, hay ...... 2 .0 from the use of this fumigant shall not Leaf petioles subgroup 4B ...... 0 .50 Lettuce ...... 1.73 exceed 125 parts per milion. Peppermint, oil ...... 12 (2) Methyl bromide is used to fumi- Peppermint, tops ...... 4 .0 gate corn grits and cracked rice in the Spearmint, oil ...... 12 Spearmint, tops ...... 4 .0 production of fermented malt beverage. Taro, corm ...... 0 .15 (3) To assure safe use of the fumi- Taro, leaves ...... 1 .0 gant, its label and labeling shall con- Tomato ...... 0.24 form to the label and labeling reg- Vegetable, brassica, leafy, group 5 ...... 2.5 istered by the U.S. Environmental Pro- Watercress ...... 3 .2 tection Agency, and the usage em- (b) Section 18 emergency exemptions. ployed should conform with such label [Reserved] or labeling. (c) Tolerances with regional registra- (4) The total residue of inorganic bro- tions. Tolerances with a regional reg- mides in fermented malt beverage, re- istration as defined in § 180.1(l) are es- sulting from the use of corn grits and tablished for residues of the cracked rice fumigated with the fumi- molluscicide metaldehyde, including gant described in paragraph (a)(2) of its metabolites and degradates, in or this section plus additional residues of on the following commodities. Compli- inorganic bromides that may be ance with the specified tolerance level present from uses in accordance with is to be determined by measuring only other regulations in this chapter pro- metaldehyde, 2,4,6,8-tetramethyl- mulgated under section 408 and/or 409 1,3,5,7-tetroxocane, in or on the com- of the Act, does not exceed 25 parts per modity. million bromide (calculated as Br). (b) Section 18 emergency exemptions. Commodity Parts per [Reserved] million (c) Tolerances with regional registra- Soybean, seed ...... 0.05 tions. [Reserved] (d) Indirect or inadvertent residues. (d) Indirect or inadvertent residues. [Reserved] [Reserved] [71 FR 74818, Dec. 13, 2006] [73 FR 54963, Sept. 24, 2008, as amended at 78 FR 70869, Nov. 27, 2013] § 180.523 Metaldehyde; tolerances for residues. § 180.525 Resmethrin; tolerances for (a) General. Tolerances are estab- residues. lished for residues of the molluscicide (a) General. Tolerances are estab- metaldehyde, including its metabolites lished for residues of the insecticide and degradates, in or on the commod- resmethrin [5-(phenylmethyl)-3- ities listed in the following table. Com- furanyl] methyl 2,2-dimethyl-3-(2- pliance with the specified tolerance methyl-1-propenyl) levels is to be determined by meas- cyclopropanecarboxylate in or on food

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commodities at 3.0 ppm resulting from § 180.527 Flufenacet, N-(4- use of the insecticide in food handling fluorophenyl)-N-(1-methylethyl)-2- and storage areas as a space concentra- [[5-(trifluoromethyl)-1, 3, 4- tion for spot/or crack and crevice treat- thiadiazol-2-yl] oxy]acetamide and its metabolites containing the 4- ment and shall be limited to a max- fluoro-N-methylethyl benzenamine imum of 3.00 percent of the active in- tolerances for residues. gredient by weight, and as a space (a) General. Tolerances are estab- treatment shall be limited to a max- lished for the combined residues of the imum of 0.5 fluid ounce of 3.0 percent herbicide flufenacet, N-(4- active ingredient by weight per 1000 fluorophenyl)-N-(1-methylethyl)-2-[[5- cubic feet of space provided that the (trifluoromethyl)-1, 3, 4-thiadiazol-2-yl] food is removed or covered prior to oxy]acetamide and its metabolites con- such use. To assure safe use of the ad- taining the 4-fluoro-N-methylethyl ditive, its label and labeling shall con- benzenamine moiety in or on the fol- form to that registered with the U.S. lowing commodities. Environmental Protection Agency, and Parts per shall be used in accordance with such Commodity million label and labeling. (b) Section 18 emergency exemptions. Cattle, kidney ...... 0 .05 Corn, field, forage ...... 0 .4 [Reserved] Corn, field, grain ...... 0 .05 (c) Tolerances with regional registra- Corn, field, stover ...... 0 .4 Corn, sweet, forage ...... 0 .45 tions. [Reserved] Corn, sweet, kernel plus cob with husks re- (d) Indirect or inadvertent residues. moved ...... 0 .05 [Reserved] Corn, sweet, stover ...... 0 .30 Goat, kidney ...... 0 .05 [71 FR 74819, Dec. 13, 2006] Hog, kidney ...... 0.05 Horse, kidney ...... 0 .05 Sheep, kidney ...... 0.05 § 180.526 Synthetic isoparaffinic petro- Soybean, seed ...... 0 .1 leum hydrocarbons; tolerances for Wheat, bran ...... 0.80 residues. Wheat, forage ...... 6 .0 Wheat, grain ...... 0 .60 (a) General. Synthetic isoparaffinic Wheat, hay ...... 1 .2 petroleum hydrocarbons complying Wheat, straw ...... 0 .35 with 21 CFR 172.882 (a) and (b) may be (b) Section 18 emergency exemptions. safely used as a component of insecti- [Reserved] cide formulations for use on animal (c) Tolerances with regional registra- feed in an amount no greater than rea- tions. Tolerances are established for sonably required to accomplish its in- combined residues of flufenacet, N-(4- tended effect as an adjuvant in the in- fluorophenyl)-N-(1-methylethyl)-2-[[5- secticide formulation and shall not be (trifluoromethyl)-1, 3, 4-thiadiazol-2-yl] intended to accomplish any effect in oxy]acetamide, and its metabolites animal feed. It is used or intended for containing the 4-fluoro-N-methylethyl use as a component of insecticide for- benzenamine moiety, with regional mulations used in compliance with reg- registration. ulations issued in 40 CFR part 180 and Parts per in this part. Commodity million (b) Section 18 emergency exemptions. [Reserved] Grass, forage ...... 7 .0 Grass, hay ...... 0 .4 (c) Tolerances with regional registrations. [Reserved] (d) Indirect or inadvertent residues. (d) Indirect or inadvertent residues. Tolerances are established for indirect [Reserved] or inadvertent residues of the herbicide flufenacet, N-(4-fluorophenyl)-N-(1- [40 FR 14161, Mar. 28, 1975, as amended at 50 FR 2959, Jan. 23, 1985, and amended at 53 FR methylethyl)-2-[[5-(trifluoromethyl)- 24668, 24669, June 29, 1988. Redesignated and 1,3,4-thiadiazol-2-yl]oxy]acetamide and amended at 63 FR 34319, June 24, 1998] its metabolites containing the 4-fluoro- N-methylethyl benzenamine moiety in or on the following raw agricultural

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commodities when present therein as a (d) Indirect or inadvertent residues. result of application of flufenacet to [Reserved] the growing crops in paragraph (a) of [63 FR 34828, June 26, 1998, as amended at 69 this section. FR 58083, Sept. 29, 2004]

Parts per Commodity million § 180.532 Cyprodinil; tolerances for residues. Alfalfa, forage ...... 0.1 (a) General. (1) Tolerances are estab- Alfalfa, hay ...... 0.1 lished for residues of the fungicide Alfalfa, seed ...... 0 .1 Clover, forage ...... 0.1 cyprodinil, including its metabolites Clover, hay ...... 0.1 and degradates, in or on the commod- Grain, cereal, group 15, except rice ...... 0 .1 ities in the table below. Compliance Grain, cereal, forage, fodder, and straw, group with the tolerance levels specified 16, except rice ...... 0 .1 below is to be determined by measuring Grass, forage, fodder, and hay, group 17 ...... 0 .1 only cyprodinil 4-cyclopropyl-6-methyl-N-phenyl-2-pyrimidinamine. [63 FR 26473, May 13, 1998, as amended at 63 FR 50791, Sept. 23, 1998; 64 FR 42846, Aug. 6, Commodity Parts per 1999; 65 FR 64366, Oct. 27, 2000; 68 FR 2247, million Jan. 16, 2003; 68 FR 37759, June 25, 2003; 70 FR Almond ...... 0.02 37696, June 30, 2005; 71 FR 76200, Dec. 20, 2006; Almond, hulls ...... 8 .0 72 FR 26310, May 9, 2007] Apple, wet pomace ...... 4 .6 Avocado ...... 1 .2 Bean, dry ...... 0.6 § 180.530 2,2-Dimethyl-1,3-benzodioxol- Bean, succulent ...... 0 .6 4-ol methylcarbamate; tolerances Berry, low growing, subgroup 13–07G, except for residues. cranberry ...... 5.0 Brassica, head and stem, subgroup 5A ...... 1 .0 (a) General. (1) The insecticide 2,2-di- Brassica, leafy greens, subgroup 5B ...... 10 .0 methyl-1,3-benzodioxol-4-yl Bushberry subgroup 13–07B ...... 3 .0 methylcarbamate may be safely used Caneberry subgroup 13–07A ...... 10 Canistel ...... 1 .2 in spot and/or crack and crevice treat- Canola, seed 1 ...... 0 .03 ments in animal feed handling estab- Citrus, dried pulp ...... 8 .0 lishments, including feed manufac- Citrus, oil ...... 60 Dragon fruit ...... 2 .0 turing and processing establishments, Fruit, pome, group 11–10 ...... 1 .7 such as stores, supermarkets, dairies, Fruit, small vine climbing, except fuzzy kiwifruit, meat slaughtering and packing plants, subgroup 13–07F ...... 3 .0 Fruit, stone, group 12 ...... 2 .0 and canneries until the tolerance expi- Grape, raisin ...... 5 .0 ration/revocation date of April 26, 2005. Herb subgroup 19A, dried, except parsley ...... 15 .0 (2) The insecticide 2,2-dimethyl-1,3- Herb subgroup 19A, fresh, except parsley ...... 3 .0 Kiwifruit ...... 1.8 benzodioxol-4-yl methylcarbamate may Leaf petioles subgroup 4B ...... 30 be safely used in spot and/or crack and Leafy greens subgroup 4A ...... 50 crevice treatments in food handling es- Lemon ...... 0.60 Lime ...... 0.60 tablishments, including food service, Longan ...... 2 .0 manufacturing and processing estab- Lychee ...... 2 .0 lishments, such as restaurants, cafe- Mango ...... 1.2 Onion, bulb, subgroup 3–07A ...... 0 .6 terias, supermarkets, bakeries, brew- Onion, green, subgroup 3–07B ...... 4 .0 eries, dairies, meat slaughtering and Papaya ...... 1 .2 packing plants, and canneries until the Parsley, dried leaves ...... 170 Parsley, leaves ...... 35 tolerance expiration/revocation date of Pistachio ...... 0.10 April 26, 2005. Pulasan ...... 2 .0 (3) To ensure safe use of the additive, Rambutan ...... 2 .0 Sapodilla ...... 1 .2 its label and labeling shall conform to Sapote, black ...... 1 .2 that registered with the U.S. Environ- Sapote, mamey ...... 1 .2 mental Protection Agency and it shall Spanish lime ...... 2 .0 Star apple ...... 1 .2 be used in accordance with such label Turnip, greens ...... 10.0 and labeling. Vegetable, cucurbit, group 9 ...... 0.70 (b) Section 18 emergency exemptions. Vegetable, fruiting, group 8–10 ...... 1 .5 Vegetable, leaves of root and tuber, group 2 ..... 10 [Reserved] Vegetable, root, except sugarbeet, subgroup 1B 0 .75 (c) Tolerances with regional registra- Watercress ...... 20 tions. [Reserved] 1 Import only.

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(2) Tolerances are established for res- Commodity Parts per idues of the fungicide cyprodinil, in- million cluding its metabolites and degradates, Blueberry ...... 1 .0 in the commodities in the table below. Broccoli ...... 1 .0 Compliance with the tolerance levels Cabbage, except Chinese cabbage ...... 3.0 Caneberry subgroup 13A ...... 1 .0 specified below is to be determined by Cantaloupe ...... 0 .5 measuring only the sum of cyprodinil Carrot, roots ...... 0.5 4-cyclopropyl-6-methyl-N-phenyl-2- Cattle, fat ...... 1.5 pyrimidinamine and free and con- Cattle, meat ...... 1 .5 Cattle, meat byproducts ...... 1.5 jugated CGA–304075 4-(4-cyclopropyl-6- Cauliflower ...... 0 .5 methyl-pyrimidin-2-ylamino)-phenol, Collards ...... 3.0 calculated as the stoichiometric equiv- Corn, field, forage ...... 15 .0 Corn, field, grain ...... 0 .02 alent of cyprodinil. Corn, field, stover ...... 15 .0 Corn, pop, grain ...... 0.02 Commodity Parts per Corn, pop, stover ...... 15.0 million Corn, sweet, forage ...... 15 .0 Corn, sweet, kernel plus cob with husks re- Cattle, meat byproducts ...... 0.02 moved ...... 0 .1 Goat, meat byproducts ...... 0 .02 Corn, sweet, stover ...... 15.0 Horse, meat byproducts ...... 0 .02 Cotton, undelinted seed ...... 0 .2 Sheep, meat byproducts ...... 0 .02 Cucumber ...... 0 .5 Egg ...... 0 .03 (b) Section 18 emergency exemptions. Eggplant ...... 0.5 [Reserved] Elderberry ...... 1 .0 (c) Tolerances with regional registra- Fruit, stone, group 12 ...... 3 .0 Goat, fat ...... 1 .5 tions. [Reserved] Goat, meat ...... 1.5 (d) Indirect or inadvertent residues. Goat, meat byproducts ...... 1 .5 [Reserved] Gooseberry ...... 1 .0 Hazelnut ...... 0 .2 [63 FR 17706, Apr. 10, 1998] Hog, fat ...... 1 .5 Hog, meat ...... 1 .5 EDITORIAL NOTE: For FEDERAL REGISTER ci- Hog, meat byproducts ...... 1 .5 tations affecting § 180.532, see the List of CFR Horse, fat ...... 1 .5 Sections Affected, which appears in the Horse, meat ...... 1 .5 Finding Aids section of the printed volume Horse, meat byproducts ...... 1 .5 and at www.fdsys.gov. Kiwifruit ...... 0.5 Lentil, seed ...... 0 .25 Melon, honeydew ...... 0.5 § 180.533 Esfenvalerate; tolerances for Milk ...... 0.3 residues. Milk, fat ...... 7 .0 (a) General. (1) Tolerances are estab- Muskmelon ...... 0 .5 Mustard greens ...... 5.0 lished for the combined residues of the Okra ...... 0.5 insecticide esfenvalerate, (S)-cyano(3- Pea, dry, seed ...... 0 .25 phenoxyphenyl)methyl-(S)-4-chloro-a- Pea, succulent ...... 0 .5 Peanut ...... 0 .02 (1-methylethyl)benzeneacetate, its Pear ...... 1 .0 non-racemic isomer, (R)-cyano(3- Pecan ...... 0 .2 phenoxyphenyl)methyl-(R)-4-chloro-a- Pepper ...... 0 .5 (1-methylethyl)benzeneacetate and its Potato ...... 0 .02 Poultry, fat ...... 0.3 diastereomers (S)-cyano(3- Poultry, liver ...... 0 .03 phenoxyphenyl)methyl-(R)-4-chloro-a- Poultry, meat ...... 0 .03 (1-methylethyl)benzeneacetate and (R)- Poultry, meat byproducts, except liver ...... 0 .3 Pumpkin ...... 0.5 cyano(3-phenoxyphenyl)methyl-(S)-4- Radish, roots ...... 0 .3 chloro-a-(1- Radish, tops ...... 3 .0 methylethyl)benzeneacetate, in or on Sheep, fat ...... 1 .5 food commodities as follows: Sheep, meat ...... 1.5 Sheep, meat byproducts ...... 1 .5 Parts per Sorghum, grain, forage ...... 10.0 Commodity million Sorghum, grain, grain ...... 5 .0 Sorghum, grain, stover ...... 10 .0 Almond ...... 0.2 Soybean, hulls ...... 0 .5 Almond, hulls ...... 5 .0 Soybean, seed ...... 0 .05 Apple ...... 1.0 Squash, summer ...... 0 .5 Artichoke, globe ...... 1.0 Squash, winter ...... 0 .5 Bean, dry, seed ...... 0 .25 Sugarcane, cane ...... 1.0 Bean, snap, succulent ...... 1 .0 Sunflower, seed ...... 0.5 Beet, sugar, roots ...... 0 .05 Sweet potato, roots ...... 0 .05 Beet, sugar, tops ...... 5.0 Tomato ...... 0.5

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Commodity Parts per § 180.535 Fluroxypyr 1-methylheptyl million ester; tolerances for residues. Turnip, greens ...... 7.0 (a) General. Tolerances are estab- Turnip, roots ...... 0 .5 lished for combined residues of Walnut ...... 0 .2 fluroxypyr 1-methylheptyl ester [1- Watermelon ...... 0.5 methylheptyl ((4-amino-3,5-dichloro-6- fluoro-2-pyridinyl)oxy)acetate] and its (2) A tolerance of 0.05 ppm on raw ag- metabolite fluroxypyr [((4-amino-3,5- ricultural food commodities (other dichloro-6-fluoro-2-pyridinyl)oxy)acetic than those food commodities already acid] in or on the following raw agri- covered by a higher tolerance as a re- cultural commodities. Compliance with sult of use on growing crops) is estab- the established tolerance levels is de- lished for the combined residues of the termined by measuring only the sum of insecticide esfenvalerate, (S)-cyano(3- fluroxypyr 1-methylheptyl ester [1- phenoxyphenyl)methyl-(S)-4-chloro-a- methylheptyl ((4-amino-3, 5-dichloro-6- (1-methylethyl)benzeneacetate, its fluoro-2-pyridinyl)oxy)acetate] and its non-racemic isomer, (R)-cyano(3- metabolite fluroxypyr [((4-amino-3,5- phenoxyphenyl)methyl-(R)-4-chloro-a- dichloro-6-fluoro-2-pyridinyl)oxy)acetic (1-methylethyl)benzeneacetate and its acid] calculated as the stoichiometric diastereomers (S)-cyano(3- equivalent of fluroxypyr. phenoxyphenyl)methyl-(R)-4-chloro-a- Parts per (1-methylethyl)benzeneacetate and (R)- Commodity million cyano(3-phenoxyphenyl)methyl-(S)-4- chloro-a-(1- Barley, grain ...... 0 .5 Barley, hay ...... 12 .0 methylethyl)benzeneacetate as a result Barley, hay ...... 20 .0 of the use of esfenvalerate in food-han- Barley, straw ...... 12 .0 dling establishments. Cattle, fat ...... 0.1 Cattle, kidney ...... 1 .5 (b) Section 18 emergency exemptions. Cattle, meat ...... 0 .1 [Reserved] Cattle, meat byproducts ...... 0.1 (c) Tolerances with regional registra- Corn, field, forage ...... 1 .0 Corn, field, grain ...... 0 .02 tions. Tolerances with regional reg- Corn, field, stover ...... 0 .5 istration are established for the com- Corn, sweet, forage ...... 1 .0 bined residues of the insecticide Corn, sweet, kernel plus cob with husks removed ...... 0 .02 esfenvalerate, (S)-cyano(3- Corn, sweet, stover ...... 2 .0 phenoxyphenyl)methyl-(S)-4-chloro-a- Fruit, pome, group 11 ...... 0.02 (1-methylethyl)benzeneacetate, its Garlic, bulb ...... 0.03 Goat, fat ...... 0 .1 non-racemic isomer, (R)-cyano(3- Goat, kidney ...... 1 .5 phenoxyphenyl)methyl-(R)-4-chloro-a- Goat, meat ...... 0.1 (1-methylethyl)benzeneacetate and its Goat, meat byproducts ...... 0 .1 Grain, aspirated fractions ...... 0 .6 diastereomers (S)-cyano(3- Grass, forage ...... 120 phenoxyphenyl)methyl-(R)-4-chloro-a- Grass, hay ...... 160 (1-methylethyl)benzeneacetate and (R)- Hog, fat ...... 0 .1 cyano(3-phenoxyphenyl)methyl-(S)-4- Hog, kidney ...... 1.5 Hog, meat ...... 0 .1 chloro-a-(1- Hog, meat byproducts ...... 0 .1 methylethyl)benzeneacetate, in or on Horse, fat ...... 0 .1 food commodities as follows: Horse, kidney ...... 1 .5 Horse, meat ...... 0 .1 Horse, meat byproducts ...... 0 .1 Parts per Milk ...... 0.3 Commodity million Millet, forage ...... 12.0 Millet, grain ...... 0 .5 Cabbage, chinese, bok choy ...... 1 .0 Millet, hay ...... 20.0 Kohlrabi ...... 2 .0 Millet, proso, straw ...... 12 .0 Lettuce, head ...... 5.0 Oat, forage ...... 12 .0 Oat, grain ...... 0 .5 (d) Indirect or inadvertent residues. Oat, hay ...... 20.0 Oat, straw ...... 12.0 [Reserved] Onion, bulb ...... 0 .03 Rice, bran ...... 3.0 [63 FR 23401, Apr. 29, 1998, as amended at 63 Rice, grain ...... 1 .5 FR 48615, Sept. 11, 1998; 74 FR 46699, Sept. 11, Shallot, bulb ...... 0 .03 2009] Sheep, fat ...... 0 .1

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(d) Indirect or inadvertent residues. Commodity Parts per million [Reserved] Sheep, kidney ...... 1.5 [63 FR 50784, Sept. 23, 1998, as amended at 73 Sheep, meat ...... 0.1 FR 75608, Dec. 12, 2008; 76 FR 76314, Dec. 7, Sheep, meat byproducts ...... 0 .1 2011] Sorghum, grain, forage ...... 2.0 Sorghum, grain, grain ...... 0 .02 § 180.539 d-Limonene; tolerances for Sorghum, grain, stover ...... 4 .0 residues. Wheat, forage ...... 12.0 Wheat, grain ...... 0 .5 (a) General. (1) The insecticide d-lim- Wheat, hay ...... 20 .0 onene may be safely used in insect-re- Wheat, straw ...... 12 .0 pellent tablecloths and in insect-repellent strips used in food- or feed-han- (b) Section 18 emergency exemptions. dling establishments. [Reserved] (2) To assure safe use of the insect re- (c) Tolerances with regional registra- pellent, its label and labeling shall con- tions. [Reserved] form to that registered by the U.S. En- (d) Indirect or inadvertent residues. vironmental Protection Agency, and it [Reserved] shall be used in accordance with such label and labeling. [63 FR 52169, Sept. 30, 1998, as amended at 64 (b) Section 18 emergency exemptions. FR 22799, Apr. 28, 1999; 66 FR 37598, July 19, 2001; 66 FR 47971, Sept. 17, 2001; 67 FR 46884, [Reserved] July 17, 2002; 67 FR 60146, Sept. 25, 2002; 68 FR (c) Tolerances with regional registra- 75438, Dec. 31, 2003; 69 FR 2074, Jan. 14, 2004; tions. [Reserved] 70 FR 3649, Jan. 26, 2005; 70 FR 7047, Feb. 10, (d) Indirect or inadvertent residues. 2005; 71 FR 76204, Dec. 20, 2006; 72 FR 73635, [Reserved] Dec. 28, 2007; 78 FR 3333, Jan. 16, 2013] [65 FR 33715, May 24, 2000, as amended at 70 FR 55268, Sept. 21, 2005] § 180.537 Isoxaflutole; tolerances for residues. § 180.540 Fenitrothion; tolerances for (a) General. Tolerances are estab- residues. lished for residues of the herbicide, (a) General. Tolerances are estab- isoxaflutole, including its metabolites lished for residues of the insecticide and degradates, in or on the commod- fenitrothion, O,O-dimethyl O-(4-nitro- ities in the table below. Compliance m-tolyl) phosphorothioate, from the with the tolerance levels specified postharvest application of the insecti- below is to be determined by measuring cide to stored wheat in Australia, in or only the sum of isoxaflutole ((5- on the following food commodity: cyclopropyl-4-isoxazolyl) [2- Parts per (methylsulfonyl)-4- Commodity million (trifluoromethyl)phenyl] methanone) and its metabolite 1-(2-methylsulfonyl- Wheat, gluten 1 ...... 3.0 4-trifluoromethylphenyl)-2-cyano-3- 1 There are no U.S. registrations on food commodities since cyclopropyl propan-1,3-dione (RPA 1987. 202248), calculated as the stoichio- (b) Section 18 emergency exemptions. metric equivalent of isoxaflutole, in or [Reserved] on the commodity: (c) Tolerances with regional registrations. [Reserved] Parts per Commodity million (d) Indirect or inadvertent residues. [Reserved] Corn, field, forage ...... 0 .04 Corn, field, grain ...... 0 .02 [73 FR 54963, Sept. 24, 2008] Corn, field, stover ...... 0 .02 Grain, aspirated fractions ...... 0 .30 § 180.541 Propetamphos; tolerances for Soybean, seed ...... 0 .05 residues. (a) General. A tolerance of 0.1 part per (b) Section 18 emergency exemptions. million is established for residues of [Reserved] the insecticide propetamphos, includ- (c) Tolerances with regional registra- ing its metabolites and degradates, in tions. [Reserved] or on food or feed commodities when

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present therein as a result of the treat- § 180.544 Methoxyfenozide; tolerances ment of food- or feed-handling estab- for residues. lishments with propetamphos. Direct (a) General. (1) Tolerances are estab- application shall be limited solely to lished for residues of the insecticide spot and/or crack and crevice treat- methoxyfenozide, including its metabo- ment in food- or feed-handling estab- lites and degradates, in or on the com- lishments where food or feed and food modities listed in the following table. or feed products are held, processed, Compliance with the tolerance levels prepared, served, or sold. Spray and specified in the following table is to be dust concentrations shall be limited to determined by measuring only a maximum of 1 percent active ingre- methoxyfenozide (3-methoxy-2- dient. For crack and crevice treatment, methylbenzoic acid 2-(3,5- equipment capable of delivering a dust dimethylbenzoyl)-2-(1,1-dimethylethyl) or a pin-stream of spray directly into hydrazide) in or on the commodity. cracks and crevices shall be used. For Parts per spot treatment, a coarse, low-pressure Commodity million spray shall be used to avoid contamination of food, feed, or food-contact/feed- Acerola ...... 0.4 Almond, hulls ...... 25 contact surfaces. Compliance with the Animal feed, nongrass, group 18, forage ...... 50 .0 tolerance level specified in this para- Animal feed, nongrass, group 18, hay ...... 150.0 graph is to be determined by measuring Apple, wet pomace ...... 7 .0 Artichoke, globe ...... 3.0 only propetamphos, 1-methylethyl- Atemoya ...... 0 .60 (2E)-3- Avocado ...... 0 .6 ((ethylamino)methoxyphosphinothioyl) Beet, sugar, roots ...... 0 .50 Berry, low growing, subgroup 13–07G, except oxy)-2-butenoate, in or on the com- cranberry ...... 2.0 modity. Biriba ...... 0 .60 (b) Section 18 emergency exemptions. Brassica, head and stem, subgroup 5A ...... 7 .0 Brassica, leafy greens, subgroup 5B ...... 30 [Reserved] Bushberry subgroup 13-07B ...... 3 .0 (c) Tolerances with regional registra- Caneberry subgroup 13–07A ...... 6.0 tions. [Reserved] Canistel ...... 0 .6 Cattle, fat ...... 0.50 (d) Indirect or inadvertent residues. Cattle, meat ...... 0 .02 [Reserved] Cherimoya ...... 0 .60 Citrus, oil ...... 100 [65 FR 33716, May 24, 2000, as amended at 76 Corn, field, forage ...... 15 FR 23498, Apr. 27, 2011] Corn, field, grain ...... 0 .05 Corn, field, refined oil ...... 0 .20 Corn, field, stover ...... 125 § 180.543 Diclosulam; tolerances for Corn, pop, grain ...... 0.05 residues. Corn, pop, stover ...... 125 Corn, sweet, forage ...... 30 (a) General. Tolerances are estab- Corn, sweet, kernel plus cob with husks re- lished for residues of the herbicide moved ...... 0 .05 diclosulam [N-(2,6-dichlorophenyl)-5- Corn, sweet, stover ...... 60 Cotton, gin byproducts ...... 35 ethoxy-7-fluoro[1,2,4] triazolo[1,5- Cotton, undelinted seed ...... 2 .0 c]pyrimidine-2-sulfonamide] in or on Cranberry ...... 0 .5 the following raw agricultural com- Custard apple ...... 0 .60 Date ...... 8 .0 modities as follows: Feijoa ...... 0 .4 Fruit, citrus, group 10–10 ...... 3 .0 Commodity Parts per Fruit, pome, group 11–10 ...... 2 .0 million Fruit, small, vine climbing, except fuzzy kiwifruit, subgroup 13–07F ...... 1 .0 Peanut ...... 0 .020 Fruit, stone, group 12, except plum, prune, Soybean, seed ...... 0 .020 fresh ...... 3 .0 Goat, fat ...... 0 .50 (b) Section 18 emergency exemptions. Goat, meat ...... 0.02 Grain, aspirated grain fractions ...... 120 [Reserved] Grape, raisin ...... 1 .5 (c) Tolerances with regional registra- Grass, forage, fodder and hay, group 17, for- tions. [Reserved] age ...... 18 .0 Grass, forage, fodder and hay, group 17, hay .. 30 .0 (d) Indirect or inadvertent residues. Guava ...... 0 .4 [Reserved] Herb subgroup 19A, except chive ...... 400 Hog, fat ...... 0 .1 [65 FR 12134, Mar. 8, 2000] Hog, meat ...... 0 .02

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modities in the following table. Com- Commodity Parts per million pliance with the tolerance levels speci- Horse, fat ...... 0 .50 fied in the following table is to be de- Horse, meat ...... 0 .02 termined by measuring only the sum of Ilama ...... 0 .60 methoxyfenozide [3-methoxy-2- Jaboticaba ...... 0 .4 Leaf petioles subgroup 4B ...... 25 methylbenzoic acid 2-(3,5- Leafy greens subgroup 4A ...... 30 dimethylbenzoyl)-2-(1,1-dimethylethyl) Longan ...... 2 .0 hydrazide] and its glucuronide metabo- Lychee ...... 2 .0 Mango ...... 0.6 lite (b-D-Glucopyranuronic acid, 3-[[2- Milk ...... 0.10 (1,1-dimethylethyl)-2-(3,5- Nut, tree, group 14 ...... 0 .10 dimethylbenzoyl)-hydrazino]carbonyl]- Onion, green, subgroup 3-07B ...... 5 .0 2-methylphenyl-), calculated as the Papaya ...... 0 .6 Passionfruit ...... 0 .4 stoichiometric equivalent of Pea and bean, dried shelled, except soybean, methoxyfenozide. subgroup 6C, except pea, blackeyed, seed and pea, southern, seed ...... 0.50 Parts per Pea and bean, succulent shelled, subgroup 6B 0 .2 Commodity million Pea, blackeyed, seed ...... 4 .0 Pea, southern, seed ...... 4.0 Cattle, liver ...... 0 .40 Peanut ...... 0 .02 Cattle, meat byproducts, except liver ...... 0 .10 Peanut, hay ...... 55.0 Egg ...... 0 .02 Peanut, oil ...... 0 .04 Goat, liver ...... 0.40 Peppermint, tops ...... 7 .0 Goat, meat byproducts, except liver ...... 0 .10 Pistachio ...... 0.10 Hog, liver ...... 0 .1 Plum, prune, fresh ...... 0.30 Hog, meat byproducts, except liver ...... 0 .02 Pomegranate ...... 0 .6 Horse, liver ...... 0 .40 Poultry, fat ...... 0.02 Horse, meat byproducts, except liver ...... 0 .10 Poultry, meat ...... 0 .02 Poultry, liver ...... 0 .10 Pulasan ...... 2 .0 Poultry, meat byproducts, except liver ...... 0 .02 Rambutan ...... 2 .0 Sheep, liver ...... 0.40 Sapodilla ...... 0 .6 Sheep, meat byproducts, except liver ...... 0 .10 Sapote, black ...... 0 .6 Sapote, mamey ...... 0 .6 (b) Section 18 emergency exemptions. Sheep, fat ...... 0 .50 [Reserved] Sheep, meat ...... 0.02 Sorghum, grain, forage ...... 15 (c) Tolerances with regional registra- Sorghum, grain, grain ...... 6 .0 tions. [Reserved] Sorghum, grain, stover ...... 20 (d) Indirect or inadvertent tolerances. Sorghum, sweet, forage ...... 15 Sorghum, sweet, grain ...... 6 .0 (1) Tolerances are established for the Sorghum, sweet, stalk ...... 15 indirect or inadvertent residues of the Sorghum, sweet, stover ...... 20 insecticide methoxyfenozide, including Soursop ...... 0 .60 its metabolites and degradates, in or Soybean, aspirated grain fractions ...... 160 Soybean, forage ...... 30 on the raw agricultural commodities in Soybean, hay ...... 80 the following table, when present Soybean, hulls ...... 2 .0 therein as a result of the application of Soybean, seed ...... 1 .0 Spanish lime ...... 2 .0 methoxyfenozide to growing crops as Spearmint, tops ...... 7 .0 listed in paragraph (a) of this section. Star apple ...... 0 .6 Compliance with the tolerance levels Starfruit ...... 0 .4 specified in the following table is to be Sugar apple ...... 0 .60 Turnip, greens ...... 30 determined by measuring only Vegetable, cucurbit, group 9 ...... 0.3 methoxyfenozide [3-methoxy-2- Vegetable, foliage of legume, except soybean, methylbenzoic acid 2-(3,5- subgroup 7A ...... 35 Vegetable, fruiting, group 8–10 ...... 2 .0 dimethylbenzoyl)-2-(1,1-dimethylethyl) Vegetable, leaves of root and tuber, group 2 ... 30 hydrazide]. Vegetable, legume, edible podded, subgroup 6A ...... 1 .5 Commodity Parts per Vegetable, root, except sugar beet, Subgroup million 1B ...... 0 .90 Vegetable, tuberous and corm, except potato, Onion, bulb, subgroup 3–07A ...... 0 .10 subgroup 1D ...... 0 .02 Potato ...... 0 .02 Wax jambu ...... 0 .4 (2) Tolerances are established for the (2) Tolerances are established for res- indirect or inadvertent residues of the idues of the insecticide insecticide methoxyfenozide, including methoxyfenozide, including its metabo- its metabolites and degradates, in or lites and degradates, in or on the com- on the raw agricultural commodities in

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the following table, when present handling establishments where food therein as a result of the application of and food products are held, processed, methoxyfenozide to growing crops as prepared and/or served. General surface listed in paragraph (a) of this section. or space spray applications may be Compliance with the tolerance levels used only when the facility is not in specified in the following table is to be operation provided exposed food has determined by measuring only the sum been covered or removed from the area of methoxyfenozide [3-methoxy-2- being treated prior to application. Spot methylbenzoic acid, 2-(3,5- and/or crack and crevice application dimethylbenzoyl)-2-(1,1-dimethylethyl) may be used while the facility is in op- hydrazide] and the following metabo- eration provided exposed food is cov- lites (all calculated as the stoichio- ered or removed from the area being metric equivalent of methoxyfenozide): treated prior to application. Spray con- free phenol of methoxyfenozide [3,5- centrate shall be limited to a max- dimethylbenzoic acid N-tert-butyl-N′- imum of 2.0% active ingredient. Con- (3-hydroxy-2-methylbenzoyl) hydra- tamination of food or food contact sur- zide], the glucose conjugate of the phe- faces shall be avoided. Food contact nol [3,5-dimethyl benzoic acid N-tert- surfaces and equipment should be butyl-N′-[3 (b-D-glucopyranosyloxy)-2- throughly washed with an effective methylbenzoyl]-hydrazide] and the cleaning compound and rinsed with po- malonylglycosyl conjugate of the phe- table water after use of the product. nol [3,5-dimethyl benzoic acid N-tert- (4) To assure safe use of the additive, butyl-N′-[3 (b-D-6-malonyl- its label and labeling shall conform to glucopyranosyl-1-oxy)-2- that registered with the U.S. Environ- methylbenzoyl]-hydrazide]. mental Protection Agency, and it shall be used in accordance with such label Parts per Commodity million and labeling. (b) Section 18 emergency exemptions. Animal feed, nongrass, group 18, straw ...... 8.0 [Reserved] Chive ...... 4 .5 Grain, cereal, forage, fodder and straw group (c) Tolerances with regional registra- 16, except corn ...... 6 .0 tions. [Reserved] Rapeseed subgroup 20A ...... 1 .0 (d) Indirect or inadvertent residues. Spice subgroup 19B ...... 4 .5 Sunflower subgroup 20B ...... 1.0 [Reserved] [65 FR 39313, June 26, 2000, as amended at 71 [67 FR 59203, Sept. 20, 2002, as amended at 68 FR 74819, Dec. 13, 2006] FR 32389, May 30, 2003; 68 FR 37765, June 25, 2003; 69 FR 58097, Sept. 29, 2004; 70 FR 7047, § 180.546 Mefenoxam; tolerances for Feb. 10, 2005; 70 FR 51604, Aug. 31, 2005; 70 FR residues. 75739, Dec. 21, 2005; 71 FR 32853, June 7, 2006; (a) General. Tolerances are estab- 73 FR 11826, Mar. 5, 2008; 74 FR 22468, May 13, lished for residues of mefenoxam, in- 2009; 74 FR 45335, Sept. 2, 2009; 76 FR 34886, June 15, 2011; 77 FR 40812, July 11, 2012; 78 FR cluding its metabolites and degradates, 60714, Oct. 2, 2013] in or on the commodities in the table below. Compliance with the tolerance § 180.545 Prallethrin (RS)-2-methyl-4- levels specified below is to be deter- oxo-3-(2-propynyl)cyclopent-2-enyl mined by measuring only metalaxyl (1RS)-cis, trans-chrysanthemate; (methyl N-(2,6-dimethylphenyl)-N- tolerances for residues. (methoxyacetyl)-DL-alaninate). (a) General. (1) A tolerance of 1.0 ppm Parts per is established for residues of the insec- Commodity million ticide prallethrin (RS)-2-methyl-4-oxo- 3-(2-propynyl)cyclopent-2-enyl (1RS)- Artichoke, globe ...... 0.05 Atemoya ...... 0 .20 cis, trans-chrysanthemate as follows: Bean, snap, succulent ...... 0 .20 (2) In or on food commodities in food Bushberry subgroup 13–07B ...... 2 .0 handling establishments where food Caneberry subgroup 13–07A ...... 0.70 Canistel ...... 0 .40 and food products are held, processed, Custard apple ...... 0 .20 prepared and/or served. Herbs, dried ...... 55 (3) Application shall be limited to Herbs, fresh ...... 8 .0 Kiwifruit ...... 0.10 space, general surface, and spot and/or Mango ...... 0.40 crack and crevice treatment in food Onion, bulb, subgroup 3–07A ...... 3 .0

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(d) Indirect or inadvertent residues. Commodity Parts per million [Reserved] Onion, green, subgroup 3–07B ...... 10 [65 FR 25660, May 3, 2000, as amended at 66 Papaya ...... 0 .40 FR 29712, June 1, 2001; 76 FR 71464, Nov. 18, Sapodilla ...... 0 .40 2011] Sapote, black ...... 0 .40 Sapote, mamey ...... 0 .40 § 180.548 Tralkoxydim; tolerances for Spinach ...... 10 residues. Star apple ...... 0 .40 Starfruit ...... 0 .20 (a) General. Tolerances are estab- Sugar apple ...... 0 .20 lished for residues of the herbicide, tralkoxydim, 2-Cyclohexen-1-one, 2-[1- (b) Section 18 emergency exemptions. (ethoxyimino)propyl]-3-hydroxy-5- [Reserved] (2,4,6-trimethylphenyl)-(9Cl) in or on (c) Tolerances with regional registra- the raw agricultural commodities: tions. [Reserved] (d) Indirect or inadvertant residues. Parts per Commodity million [Reserved] Barley, grain ...... 0 .02 [65 FR 57556, Sept. 25, 2000, as amended at 66 Barley, hay ...... 0 .02 FR 48003, Sept. 17, 2001; 67 FR 35050, May 17, Barley, straw ...... 0 .05 2002; 76 FR 4548, Jan. 26, 2011] Wheat, forage ...... 0 .05 Wheat, grain ...... 0 .02 § 180.547 Prohexadione calcium; toler- Wheat, hay ...... 0 .02 ances for residues. Wheat, straw ...... 0 .05 (a) General. Tolerances are estab- (b) Section 18 emergency exemptions. lished for residues of the growth regu- [Reserved] lator, prohexadione calcium, including (c) Tolerances with regional registra- its metabolites and degradates, in or tions. [Reserved] on the commodities in the table below. (d) Indirect or inadvertent residues. Compliance with the tolerance levels [Reserved] specified below is to be determined by measuring only prohexadione calcium [63 FR 69199, Dec. 16, 1998, as amended at 68 FR 48302, Aug. 13, 2003; 70 FR 70739, Nov. 23, (calcium 3-oxido-5-oxo-4- 2005] propionylcyclohex-3-enecarboxylate)’’ in or on the following commodities. § 180.549 Diflufenzopyr; tolerances for residues. Parts per Commodity million (a) General. Tolerances are established for combined residues of Cattle, kidney ...... 0 .10 diflufenzopyr, 2-(1-[([3,5- Cattle, meat byproducts, except kidney ...... 0.05 Cherry, sweet ...... 0 .40 difluorophenylamino] car- Fruit, pome, group 11 ...... 3.0 bonyl)hydrazono]ethyl)-3- Goat, kidney ...... 0 .10 pyridinecarboxylic acid, and its me- Goat, meat byproducts, except kidney ...... 0 .05 tabolites convertible to 8- Grass, forage 1 ...... 0 .10 methylpyrido[2,3-d]pyridazin-5(6H)-one, 1 Grass, hay ...... 0 .10 expressed as diflufenzopyr, in or on the Grass, seed screenings 1 ...... 3 .5 Grass, straw 1 ...... 1 .2 following raw agricultural commod- Hog, kidney ...... 0.10 ities: Hog, meat byproducts, except kidney ...... 0 .05 Horse, kidney ...... 0 .10 Parts per Commodity million Horse, meat byproducts, except kidney ...... 0 .05 Peanut ...... 1 .0 Corn, field, forage ...... 0 .05 Peanut, hay ...... 0.60 Corn, field, grain ...... 0 .05 Sheep, kidney ...... 0.10 Corn, field, stover ...... 0 .05 Sheep, meat byproducts, except kidney ...... 0 .05 Corn, pop, grain ...... 0.05 Corn, pop, stover ...... 0.05 1 Registration is limited to grass grown for seed. Corn, sweet, forage ...... 0 .05 Corn, sweet, kernel plus cob with husks re- (b) Section 18 emergency exemptions. moved ...... 0 .05 [Reserved] Corn, sweet, stover ...... 0 .05 (c) Tolerances with regional registra- Grass, forage ...... 22 .0 tions. [Reserved] Grass, hay ...... 7 .0

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(b) Section 18 emergency exemptions. § 180.552 Sulfosulfuron; tolerances for [Reserved] residues. (c) Tolerances with regional registra- (a) General. Tolerances are estab- tions. [Reserved] lished for residues of the herbicide (d) Indirect or inadvertent residues. sulfosulfuron, 1–(4,6- [Reserved] dimethoxypyrimidin-2-yl)-3-[(2- [64 FR 4308, Jan. 28, 1999, as amended at 67 ethanesulfonyl-imidazo[1,2-a]pyridine- FR 55338, Aug. 29, 2002; 76 FR 34886, June 15, 3-yl) sulfonyl]urea and its metabolites 2011] converted to 2-(ethylsulfonyl)- imidazo[1,2-a]pyridine and calculated § 180.551 Fluthiacet-methyl; tolerances as sulfosulfuron in or on the raw agri- for residues. cultural commodities. (a) General. (1) A tolerance is estab- Parts per lished for residues of the herbicide, Commodity million fluthiacet-methyl, acetic acid [[2- chloro-4-fluoro-5-[(tetrahydro-3-oxo- Cattle, fat ...... 0.02 Cattle, meat ...... 0 .01 1H,3H-[1,3,4]thiadiazolo[3,4-a]pyridazin- Cattle, meat byproducts ...... 0.3 1-ylidene)amino]phenyl]thio]-methyl Goat, fat ...... 0 .02 ester, in or on the food commodity: Goat, meat ...... 0.01 Goat, meat byproducts ...... 0 .3 Parts per Grass, forage, fodder and hay, group 17, for- Commodity million age ...... 14 Grass, forage, fodder and hay, group 17, hay .. 25 Corn, field, forage ...... 0 .050 Hog, fat ...... 0 .005 Corn, field, grain ...... 0 .010 Hog, meat ...... 0 .005 Corn, field, stover ...... 0 .050 Hog, meat byproducts ...... 0 .05 Corn, pop, grain ...... 0.010 Horse, fat ...... 0 .02 Corn, pop, stover ...... 0.050 Horse, meat ...... 0 .01 Corn, sweet, forage ...... 0 .050 Horse, meat byproducts ...... 0 .3 Milk ...... 0.02 Corn, sweet, kernel plus cob with husks re- Sheep, fat ...... 0 .02 moved ...... 0 .010 Sheep, meat ...... 0.01 Corn, sweet, stover ...... 0 .050 Sheep, meat byproducts ...... 0 .3 Soybean, seed ...... 0 .01 Wheat, forage ...... 4 .0 Wheat, grain ...... 0 .02 (2) A tolerance is established for the Wheat, hay ...... 0 .3 combined residues of the herbicide Wheat, straw ...... 0 .1 fluthiacet-methyland its acid metabolite: acetic acid, [[2-chloro-4-fluoro-5- (b) Section 18 emergency exemptions. [tetrahydro-3-oxo-1H,3H- [Reserved] [1,3,4]thiadiazolo[3,4-a]pyridazin-1- (c) Tolerances with regional registra- ylidene)amino]phenyl]thio]-methyl tions. [Reserved] ester, and its acid metabolite, acetic (d) Indirect or inadvertent residues. acid, [[2-chloro-4-fluoro-5-[(tetrahydro- [Reserved] 3-oxo-1H,3H-[1,3,4]thiadiazolo[3,4- [64 FR 27192, May 19, 1999, as amended at 70 a]pyridazin-1- FR 69464, Nov. 16, 2005; 72 FR 54574, Sept. 26, ylidene)amino]phenyl]thio]- , in or on 2007] the following food commodities: § 180.553 Fenhexamid; tolerances for Parts per residues. Commodity million (a) General. Tolerances are estab- Cotton, gin byproducts ...... 0 .20 lished for the residues of the fungicide Cotton, undelinted seed ...... 0 .020 fenhexamid (N-2,3-dichloro-4- hydroxyphenyl)-1-methyl (b) Section 18 emergency exemptions. cyclohexanecarboxamide) in or on the [Reserved] following commodities: (c) Tolerances with regional registrations. [Reserved] Commodity Parts per (d) Indirect or inadvertent residues. million [Reserved] Almond, hulls ...... 2 .0 Almond ...... 0.02 [64 FR 18357, Apr. 14, 1999, as amended at 66 Asparagus ...... 0.02 FR 65850, Dec. 21, 2001; 71 FR 77625, Dec. 27, Bushberry subgroup 13B ...... 5 .0 2006] Caneberry subgroup 13A ...... 20 .0

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(2) Tolerances are established in or Commodity Parts per million on the following commodities for the Cilantro, leaves ...... 30.0 residues of the metabolite (E)-2-[2-(2- Cucumber ...... 2 .0 methylphenoxy)methyl]-phenyl-2- Fruit, stone, group 12, except plum, prune, (methoxyimido)acetic acid resulting fresh, postharvest ...... 10.0 from the use of the fungicide kresoxim- Ginseng ...... 0 .3 Grape ...... 4 .0 methyl: Grape, raisin ...... 6 .0 Juneberry ...... 5 .0 Commodity Parts per Kiwifruit, postharvest ...... 15 .0 million Leafy greens subgroup 4A, except spinach ...... 30 .0 Cattle, meat byproducts ...... 0.01 Lingonberry ...... 5.0 Goat, meat byproducts ...... 0 .01 Pear ...... 10 Sheep, meat byproducts ...... 0 .01 Pepper, nonbell ...... 0 .02 Pistachio ...... 0.02 Plum, prune, dried ...... 2.5 (b) Section 18 emergency exemptions. Plum, prune, fresh ...... 1.5 [Reserved] Pomegranate ...... 2 .0 (c) Tolerances with regional registra- Salal ...... 5 .0 tions. [Reserved] Strawberry ...... 3 .0 Vegetable, fruiting, group 8, except nonbell (d) Indirect or inadvertent residues. pepper ...... 2 .0 [Reserved] [64 FR 31136, June 10, 1999, as amended at 71 (b) Section 18 emergency exemptions. FR 50359, Aug. 25, 2006; 74 FR 46377, Sept. 9, [Reserved] 2009] (c) Tolerances with regional registrations. [Reserved] § 180.555 Trifloxystrobin; tolerances (d) Indirect or inadvertent residues. for residues. [Reserved] (a) General. Tolerances are estab- [64 FR 28924, May 28, 1999, as amended at 65 lished for residues of trifloxystrobin, FR 19849, Apr. 13, 2000; 65 FR 69883, Nov. 21, including its metabolites and 2000; 67 FR 19120, Apr. 18, 2002; 68 FR 2247, degradates, in or on the commodities Jan. 16, 2003; 68 FR 55519, Sept. 26, 2003; 71 FR in the table below. Compliance with 15617, Mar. 29, 2006; 71 FR 43664, Aug. 2, 2006; the tolerance levels specified below is 73 FR 19154, Apr. 9, 2008] to be determined by measuring only the sum of trifloxystrobin, § 180.554 Kresoxim-methyl; tolerances for residues. benzeneacetic acid, (E,E)-a- (methoxyimino)-2-[[[[1-[3- (a) General. (1) Tolerances are estab- (trifluoromethyl) phenyl]ethylidene] lished for the combined residues of the amino]oxy]methyl]-, methyl ester, and fungicide kresoxim-methyl (methyl the free form of its acid metabolite (E)-2-[2-(2-methylphenoxy)-meth- CGA–321113, (E,E)-methoxyimino-[2-[1- yl]phenyl-2-(methoxyimido)acetate) (3-trifluoromethyl-phenyl)- and its metabolites as follows: (E)-2-[2- ethylideneaminooxymethyl]- (2-methylphenoxy)methyl]-phenyl-2- phenyl]acetic acid, calculated as the (methoxyimido)acetic acid; (E)-2-[2-(2- stoichiometric equivalent of hydroxymethylphenoxy)methyl]- trifloxystrobin, in or on the com- phenyl-2-(methoxyimido)acetic acid modity. (free and glucose conjugated); and (E)- 2-[2-(4-hydroxy-2-methylphenoxy)- Commodity Parts per methyl]phenyl-2-(methoxyimido)acetic million acid (free and glucose conjugated) in or Alfalfa, forage ...... 0.01 on the following commodities: Alfalfa, hay ...... 0.01 Almond, hulls ...... 9 .0 Parts per Apple, wet pomace ...... 5 .0 Commodity million Artichoke, globe ...... 1.0 Asparagus ...... 0.07 Apple, dry pomace ...... 1.0 Banana 1 ...... 0.10 Apple, wet pomace ...... 1 .0 Barley, grain ...... 0 .05 Fruit, pome ...... 0.5 Barley, hay ...... 0 .3 Grape ...... 1 .0 Barley, straw ...... 5 .0 Grape, raisin ...... 1 .5 Beet, sugar, dried pulp ...... 0 .4 Pecan ...... 0 .15 Beet, sugar, molasses ...... 0 .2 Vegetable, cucurbit, group 9 ...... 0.40 Beet, sugar, roots ...... 0 .1 Beet, sugar, tops ...... 4.0

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Parts per Parts per Commodity million Commodity million

Canistel ...... 0 .7 Wheat, forage ...... 0 .3 Cattle, fat ...... 0.1 Wheat, grain ...... 0 .05 Cattle, meat ...... 0 .1 Wheat, hay ...... 0 .2 Cattle, meat byproducts ...... 0.1 Wheat, straw ...... 5 .0 Citrus, dried pulp ...... 1 .0 Citrus, oil ...... 38 1 There are no U.S. registrations as of September 27, 1999 Coffee, green bean 2 ...... 0 .02 for use on banana. 2 There are no U.S. registrations as of January 18, 2012 for Corn, field, forage ...... 6 .0 use on coffee, green bean. Corn, field, grain ...... 0 .05 Corn, field, stover ...... 7 (b) Section 18 emergency exemptions. Corn, field, refined oil ...... 0 .1 [Reserved] Corn, pop, grain ...... 0.05 Corn, pop, stover ...... 7 (c) Tolerances with regional registra- Corn, sweet, cannery waste ...... 0 .6 tions. [Reserved] Corn, sweet, forage ...... 7 .0 (d) Indirect or inadvertent residues. Corn, sweet, kernel plus cob with husks removed ...... 0 .04 [Reserved] Corn, sweet, stover ...... 4 .0 Egg ...... 0 .04 [64 FR 51907, Sept. 27, 1999] Fruit, citrus, group 10 ...... 0 .6 EDITORIAL NOTE: For FEDERAL REGISTER ci- Fruit, pome ...... 0.5 tations affecting § 180.555, see the List of CFR Fruit, stone, group 12 ...... 2 Goat, fat ...... 0 .1 Sections Affected, which appears in the Goat, meat ...... 0.1 Finding Aids section of the printed volume Goat, meat byproducts ...... 0 .1 and at www.fdsys.gov. Grain, aspirated fractions ...... 5 .0 Grape ...... 2 .0 § 180.556 Pymetrozine; tolerances for Grape, raisin ...... 5 .0 residues. Grass, forage ...... 12 Grass, hay ...... 17 (a) General. Tolerances are estab- Hog, fat ...... 0 .05 lished for residues of the insecticide Hog, meat ...... 0 .05 Hog, meat byproducts ...... 0 .05 pymetrozine 1,2,4-triazin-3(2H)-one,4,5- Hop, dried cones ...... 11 .0 dihydro-6-methyl-4-[(3- Horse, fat ...... 0 .1 pyridinylmethylene) amino] in or on Horse, meat ...... 0 .1 the following raw agricultural com- Horse, meat byproducts ...... 0 .1 Leaf petioles subgroup 4B ...... 3 .5 modities. The tolerance level for each Mango ...... 0.7 commodity is expressed in terms of the Milk ...... 0.02 parent insecticide only, which serves as Nut, tree, group 14 ...... 0 .04 Oat, forage ...... 0 .3 an indicator of the use of pymetrozine Oat, grain ...... 0 .05 on these raw agricultural commodities. Oat, hay ...... 0.3 Oat, straw ...... 5.0 Commodity Parts per Papaya ...... 0 .7 million Peanut, hay ...... 4.0 Peanut ...... 0 .05 Asparagus ...... 0.04 Pistachio ...... 0.04 Brassica, head and stem, subgroup 5A ...... 0 .5 Potato ...... 0 .04 Brassica, leafy greens, subgroup 5B ...... 0 .25 Poultry, fat ...... 0.04 Cotton, gin byproducts ...... 2 .0 Poultry, meat ...... 0 .04 Cotton, undelinted seed ...... 0 .3 Poultry, meat byproducts ...... 0.04 Hop, dried cones ...... 6 .0 Radish, tops ...... 10 Pecan ...... 0 .02 Rice, grain ...... 3 .5 Turnip, greens ...... 0.25 Rice, hulls ...... 8 Vegetable, fruiting, group 8 ...... 0.2 Rice, straw ...... 7 .5 Vegetable, cucurbit, group 9 ...... 0.1 Sapodilla ...... 0 .7 Vegetable, leafy, execpt brassica, group 4 ...... 0 .6 Sapote, black ...... 0 .7 Vegetable, tuberous and corm, subgroup 1C ... 0.02 Sapote, mamey ...... 0 .7 Sheep, fat ...... 0 .1 (b) Section 18 emergency exemptions. Sheep, meat ...... 0.1 [Reserved] Sheep, meat byproducts ...... 0 .1 Soybean, forage ...... 10 .0 (c) Tolerances with regional registra- Soybean, hay ...... 25 .0 tions. [Reserved] Soybean, seed ...... 0 .08 (d) Indirect or inadvertent residues. Star apple ...... 0 .7 Strawberry ...... 1 .1 [Reserved] Vegetable, cucurbit, group 9 ...... 0.50 [65 FR 48634, Aug. 9, 2000, as amended at 66 Vegetable, fruiting ...... 0.5 Vegetable, root, except sugar beet, subgroup FR 14846, Mar. 14, 2001; 66 FR 66794, Dec. 27, 1B ...... 0 .1 2001; 70 FR 7047, Feb. 10, 2005; 70 FR 43298, Wheat, bran ...... 0.15 July 27, 2005]

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§ 180.557 Tetraconazole; tolerances for (d) Indirect or inadvertent residues. residues. [Reserved] (a) General. Tolerances are estab- [70 FR 20830, Apr. 22, 2005, as amended at 70 lished for residues of tetraconazole, in- FR 31359, June 1, 2005; 72 FR 18134, Apr. 11, cluding its metabolites and degradates, 2007; 73 FR 67406, Nov. 14, 2008; 76 FR 53648, in or on the commodities listed below. Aug. 29, 2011] Compliance with the following tolerance levels is to be determined by § 180.559 Clodinafop-propargyl; toler- measuring only tetraconazole (1-[2-(2,4- ances for residues. dichlorophenyl)-3-(1,1,2,2- (a) General. Tolerances are estab- tetrafluoroethoxy)propyl]-1H-1,2,4-tri- lished for clodinafop-propargyl, includ- azole), in or on the following commod- ing its metabolites and degradates, in ities. or on the commodities in the following

Parts per table. Compliance with the tolerance Commodity million levels specified in the following table is to be determined by measuring only Aspirated grain fractions ...... 1 .0 Beet sugar, dried pulp ...... 0 .15 clodinafop-propargyl [(2R)-2-[4-[(5- Beet sugar, molasses ...... 0 .15 chloro-3-fluoro-2- Beet sugar, root ...... 0 .05 pyridinyl)oxy]phenoxy]propanoic acid, Cattle, fat ...... 0.15 2-propynyl ester] and its metabolite Cattle, liver ...... 1 .50 clodinafop [(2R)-2-[4-[(5-chloro-3-fluoro- Cattle, meat ...... 0 .01 Cattle, meat byproducts (except liver) ...... 0 .15 2- pyridinyl)oxy]phenoxy]propanoic Corn, field, forage ...... 1 .1 acid]. Corn, field, grain ...... 0 .01 Corn, field, stover ...... 1 .7 Commodity Parts per Corn, pop, grain ...... 0.01 million Corn, pop, stover ...... 1.7 Wheat, forage ...... 0 .1 Eggs ...... 0 .02 Wheat, grain ...... 0 .02 Goat, fat ...... 0 .15 Wheat, hay ...... 0 .1 Goat, liver ...... 1.50 Wheat, straw ...... 0 .5 Goat, meat ...... 0.01 Goat, meat byproducts (except liver) ...... 0.15 Hog, fat ...... 0 .01 (b) Section 18 emergency exemptions. Hog, liver ...... 0 .05 [Reserved] Hog, meat ...... 0 .01 (c) Tolerances with regional registra- Hog, meat byproducts (except liver) ...... 0 .01 tions. [Reserved] Horse, fat ...... 0 .15 Horse, liver ...... 1 .50 (d) Indirect or inadvertent residues. Horse, meat ...... 0 .01 [Reserved] Horse, meat byproducts (except liver) ...... 0 .15 Low growing berry subgroup 13–07G, except [65 FR 38774, June 22, 2000, as amended at 77 cranberry ...... 0 .25 FR 72226, Dec. 5, 2012] Milk ...... 0.03 Milk, fat ...... 0 .75 § 180.560 Cloquintocet-mexyl; toler- Peanut ...... 0 .03 ances for residues. Peanut, oil ...... 0 .10 Pecan ...... 0 .04 (a) General. Tolerances are estab- Poultry, fat ...... 0.05 lished for the combined residues of Poultry, meat ...... 0 .01 cloquintocet-mexyl, (acetic acid [(5- Poultry meat byproducts ...... 0 .05 chloro-8-quinolinyl)oxy]-,1- Sheep, fat ...... 0 .15 Sheep, liver ...... 1.50 methylhexyl ester; CAS Reg. No. 99607– Sheep, meat ...... 0.01 70–2) and its acid metabolite (5-chloro- Sheep, meat byproducts (except liver) ...... 0.15 8-quinolinoxyacetic acid), when used as Small fruit vine climbing, except fuzzy kiwifruit, an inert ingredient (safener) in pes- subgroup 13–07F ...... 0.20 Soybean, refined oil ...... 0 .80 ticide formulations containing the ac- Soybean, seed ...... 0 .15 tive ingredients clodinafop-propargyl (wheat only), dicamba (wheat only), (b) Section 18 emergency exemptions. flucarbazone-sodium (wheat only), [Reserved] pinoxaden (wheat or barley), or (c) Tolerances with regional registra- pyroxsulum (wheat only) in or on the tions. [Reserved] following food commodities:

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acid (CGA–210007), expressed as the Commodity Parts per million Stoichiometric equivalent of Barley, grain ...... 0 .1 acibenzolar- S -methyl, in or on the fol- Barley, hay ...... 0 .1 lowing raw agricultural commodities. Barley, straw ...... 0 .1 Wheat, forage ...... 0 .2 Expiration/ Wheat, grain ...... 0 .1 Commodity Parts per revocation Wheat, hay ...... 0 .5 million date Wheat, straw ...... 0 .1 Apple ...... 0.05 12/31/15 (b) Section 18 emergency exemptions. Grapefruit ...... 0.05 12/31/15 [Reserved] Pear ...... 0.05 12/31/15 (c) Tolerances with regional registra- (b) Section 18 emergency exemptions. tions. [Reserved] [Reserved] (d) Indirect or inadvertent residues. (c) Tolerances with regional registra- [Reserved] tions. [Reserved] [65 FR 38764, June 22, 2000, as amended at 70 (d) Indirect or inadvertent residues. FR 74688, Dec. 16, 2005; 73 FR 11820, Mar. 5, [Reserved] 2008; 75 FR 16020, Mar. 31, 2010; 76 FR 38035, June 29, 2011] [65 FR 50446, Aug. 18, 2000, as amended at 70 FR 7861, Feb. 16, 2005; 71 FR 76200, Dec. 20, § 180.561 Acibenzolar-S-methyl; toler- 2006; 74 FR 24710, May 26, 2009; 76 FR 34886, ances for residues. June 15, 2011; 77 FR 21676, Apr. 11, 2012; 77 FR 30406, May 23, 2012] (a) General. (1) Tolerances are established for residues of acibenzolar-S- § 180.562 Flucarbazone-sodium; toler- methyl, benzo(1,2,3)thiadiazole-7- ances for residues. carbothioic acid-S-methyl ester, in- (a) General. Tolerances are estab- cluding its metabolites and degradates, lished for combined residues of the her- in or on the commodities in the table bicide flucarbazone-sodium, 4,5- below. Compliance with the tolerance dihydro-3-methoxy-4-methyl-5-oxo-N- levels specified below is to be deter- [[2(trifluoromethoxy)phenyl] sulfonyl]- mined by measuring only those 1H-1,2,4-triazole 1-carboxamide, sodium acibenzolar-S-methyl residues convert- salt) and its N-desmethyl metabolite; ible to benzo(1,2,3)thiadiazole-7-car- and its metabolites converted to 2- boxylic acid (CGA–210007), expressed as (trifluoromethoxy)benzene sulfonamide the stoichiometric equivalent of and calculated as flucarbazone-sodium acibenzolar-S-methyl, in or on the fol- in or on the following food commod- lowing raw agricultural commodities. ities: Parts per Commodity million Parts per Commodity million Banana 1 ...... 0.1 Berry, low growing, subgroup 13–07G ...... 0 .15 Cattle, liver ...... 1 .50 Onion, bulb, subgroup 3–07A ...... 0 .1 Cattle, meat ...... 0 .01 Spinach ...... 1 .0 Cattle, meat byproducts, except liver ...... 0 .01 Tomato, paste ...... 3 .0 Goat, liver ...... 1.50 Vegetable, brassica, leafy, group 5 ...... 1.0 Goat, meat ...... 0.01 Vegetable, cucurbit, group 9 ...... 2.0 Goat, meat byproducts, except liver ...... 0 .01 Vegetable, fruiting, group 8 ...... 1.0 Hog, liver ...... 1 .50 Vegetable, leafy, group 4 ...... 0 .25 Hog, meat ...... 0 .01 1 There are no United States registrations for banana. Hog, meat byproducts, except liver ...... 0 .01 Horse, liver ...... 1 .50 (2) Tolerances are established for res- Horse, meat ...... 0 .01 idues of acibenzolar- S -methyl, Horse, meat byproducts, except liver ...... 0 .01 Milk ...... 0.005 benzo(1,2,3)thiadiazole-7-carbothioic Sheep, liver ...... 1.50 acid- S -methyl ester, including its me- Sheep, meat ...... 0.01 tabolites and degradates, in or on the Sheep, meat byproducts, except liver ...... 0 .01 commodities in the table below. Com- Wheat, forage ...... 0 .30 Wheat, grain ...... 0 .01 pliance with the tolerance levels speci- Wheat, hay ...... 0 .10 fied below is to be determined by meas- Wheat, straw ...... 0 .05 uring only those acibenzolar- S -methyl residues convertible to (b) Section 18 emergency exemptions. benzo(1,2,3)thiadiazole-7-carboxylic [Reserved]

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(c) Tolerances with regional registra- Commodity Parts per tions. [Reserved] million (d) Indirect or inadvertant residues. Berry, low growing, except strawberry, subgroup [Reserved] 13–07H ...... 1 Bushberry subgroup 13–07B ...... 1 .5 [70 FR 67915, Nov. 9, 2005, as amended at 71 Cattle, fat ...... 1.5 FR 76931, Dec. 22, 2006] Cattle, meat ...... 0 .05 Cattle, meat byproducts ...... 0.03 § 180.563 Ethametsulfuron-methyl; tol- Corn, sweet, forage ...... 10 Corn, sweet, kernel plus cob with husk removed 0.02 erances for residues. Corn, sweet, stover ...... 15 (a) General. A tolerance is established Cotton, gin byproducts ...... 15 Cotton, undelinted seed ...... 2 .0 for residues of ethametsulfuron methyl Cowpea, forage ...... 50 (methyl 2- ((((4-ethoxy-6- Cowpea, hay ...... 100 (methylamino)-1,3,5- triazin-2-yl) Fruit, pome, except pear, group 11 ...... 1 .0 amino) carbonyl) amino) sulfonyl) ben- Fruit, small vine climbing, except fuzzy kiwifruit, subgroup 13–07F ...... 2 zoate) in or on the following raw agri- Fruit, stone, group 12 ...... 0 .90 cultural commodities. Goat, fat ...... 1 .5 Goat, meat ...... 0.05 Parts per Goat, meat byproducts ...... 0 .03 Commodity million Grain, aspirated fractions ...... 45 Grape, raisin ...... 5 .0 Canola, seed ...... 0 .02 Hog, fat ...... 1 .5 Crambe, seed ...... 0.02 Hog, meat ...... 0 .05 Rapeseed, seed ...... 0 .02 Hog, meat byproducts ...... 0 .03 Horse, fat ...... 1 .5 (b) Section 18 emergency exemptions. Horse, meat ...... 0 .05 Horse, meat byproducts ...... 0 .03 [Reserved] Milk ...... 0.15 (c) Tolerances with regional registra- Milk, fat ...... 4 .0 tions. [Reserved] Okra ...... 0.50 Pea, southern, seed ...... 0.10 (d) Indirect of inadvertent residues. Peanut ...... 0 .01 [Reserved] Peanut, hay ...... 40 Pear ...... 0 .20 [65 FR 57972, Sept. 27, 2000, as amended at 66 Pear, oriental ...... 0.20 FR 18207, Apr. 6, 2001; 67 FR 35050, May 17, Peppermint, tops ...... 11 2002] Sheep, fat ...... 1 .5 Sheep, meat ...... 0.05 § 180.564 Indoxacarb; tolerances for Sheep, meat byproducts ...... 0 .03 Soybean, hulls ...... 4 .0 residues. Soybean, seed ...... 0 .80 (a) General. (1) Tolerances are estab- Spearmint, tops ...... 11 lished for residues of indoxacarb, in- Turnip, greens ...... 12 Vegetable, Brassica, leafy, group 5 ...... 12 cluding its metabolites and degradates, Vegetable, cucurbit, group 9 ...... 0.60 in or on the commodities in the table Vegetable, fruiting, group 8 ...... 0.50 below. Compliance with the tolerance Vegetable, leafy, except Brassica, group 4 ...... 14 levels specified below is to be deter- Vegetable, tuberous and corm, subgroup 1-C .... 0.01 mined by measuring only indoxacarb, (2) Tolerances are established for res- (S)-methyl 7-chloro-2,5-dihydro-2-[[(me- idues of indoxacarb, including its methoxycarbonyl)[4-(trifluoromethoxy) tabolites and degradates, in or on the phenyl]amino]carbonyl]indeno[1,2-e] commodities in the table below. Com- [1,3,4][oxadiazine-4a(3H)-carboxylate, pliance with the tolerance levels speci- and its R-enantiomer, (R)-methyl 7- fied below is to be determined by meas- chloro-2,5-dihydro-2-[[(methoxycar- uring only the sum of indoxacarb, (S)- bonyl)[4-(trifluoromethoxy)phenyl] methyl-7-chloro-2,5-dihydro-2-[[(me- amino]carbonyl]indeno[1,2-e][1,3,4] thoxycarbonyl)[4-(trifluoromethoxy)- [oxadiazine-4a(3H)-carboxylate. phenyl]amino]carbonyl]indeno[1,2e] Parts per [1,3,4]oxadiazine-4a(3H)-carboxylate, its Commodity million R-enantiomer, (R)-methyl 7-chloro-2,5- Apple, wet pomace ...... 3 .0 dihydro-2-[[(methoxycarbonyl)[4- Alfalfa, forage ...... 10 (trifluoromethoxy) Alfalfa, hay ...... 50 phenyl]amino]carbonyl]indeno [1,2-e] Bean, dry, seed ...... 0 .2 [1,3,4] oxadiazine-4a(3H)-carboxylate, Bean, succulent ...... 0 .9 Beet, garden, roots ...... 0 .30 and the metabolites: IN–JT333, methyl Beet, garden, tops ...... 6 .0 7-chloro-2,5-dihydro-2-[[[4-

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(trifluoromethoxy)phenyl]- Commodity Parts per amino]carbonyl]indeno[1,2- million e][1,3,4]oxadiazine-4a(3H)-carboxylate; Alfalfa, forage ...... 0.05 IN–KT319, (E)-methyl 5-chloro-2,3,- Alfalfa, hay ...... 0.12 dihydro-2-hydroxy-1-[[[(methoxycar- Almond, hulls ...... 1 .2 Artichoke, globe ...... 0.45 bonyl)[4- Avocado ...... 0 .40 (trifluoromethoxy)phenyl]amino]-car- Barley, grain ...... 0 .4 bonyl]hydrazono]-1H-indene-2- Barley, hay ...... 0 .40 carboxylate; IN–JU873, methyl 5- Barley, straw ...... 0 .40 Bean, succulent ...... 0 .02 chloro-2,3-dihydro-2-hydroxy-1-[[[[4- Berry, low growing, subgroup 13–07G, except (triflurormethoxy)- cranberry ...... 0.30 phenyl]amino]carbonyl]hydrazono]-1H- Borage, seed ...... 0 .02 Brassica, head and stem, subgroup 5–A ...... 4.5 indene-2-carboxylate; IN–KG433, meth- Brassica, leafy greens, subgroup 5–B ...... 3 .0 yl 5-chloro-2,3,-dihydro-2-hydroxy-1- Buckwheat, forage ...... 0 .50 [[[(methoxycarbonyl)[4- Buckwheat, hay ...... 0 .02 (trifluoromethoxy)phenyl] Buckwheat, straw ...... 0 .02 Bushberry subgroup 13–07B, except lingonberry amino]carbonyl]-hydrazono]-1H-indene- and blueberry, lowbush ...... 0 .20 2-carboxylate; and IN–KB687, methyl Caneberry subgroup 13–07A ...... 0.35 [4- Canistel ...... 0 .40 Canola, seed ...... 0 .02 (trifluoromethoxy)phenyl]carbamate, Cattle, meat ...... 0 .02 calculated as the stoichiometric equiv- Cattle, meat byproducts ...... 0.04 alent of indoxacarb in the commodity. Citrus, dried pulp ...... 0 .60 Coffee, green, bean 1 ...... 0 .20 Parts per Corn, field, forage ...... 0 .10 Commodity million Corn, field, stover ...... 0 .05 Corn, pop, forage ...... 0 .10 Egg ...... 0 .20 Corn, pop, stover ...... 0.05 Poultry, fat ...... 0.20 Corn, sweet, forage ...... 0 .10 Poultry, meat ...... 0 .06 Corn, sweet, kernel plus cob with husks re- Poultry, meat byproducts ...... 0.06 moved ...... 0 .02 Corn, sweet, stover ...... 0 .05 (c) Tolerances with regional registra- Cotton, gin byproducts ...... 1 .5 tions. [Reserved] Cotton, undelinted seed ...... 0 .10 Crambe, seed ...... 0.02 (d) Indirect or inadvertent residues. Cranberry ...... 0 .02 [Reserved] Flax, seed ...... 0 .02 Food commodities and feed commodities (other [65 FR 58424, Sept. 29, 2000, as amended at 67 than those covered by a higher tolerance as a FR 41807, June 19, 2002; 67 FR 47309, July 18, result of use on growing crops) in food/feed 2002; 67 FR 58730, Sept. 18, 2002; 68 FR 25830, handling establishments ...... 0 .02 May 14, 2003; 68 FR 27746, May 21, 2003; 69 FR Fruit, citrus, group 10 ...... 0 .40 28842, May 19, 2004; 69 FR 29459, May 24, 2004; Fruit, pome, group 11 ...... 0.2 69 FR 32282, June 9, 2004; 72 FR 37641, July 11, Fruit, small, vine climbing, subgroup 13–07F, except fuzzy kiwifruit ...... 0 .20 2007; 74 FR 33165, July 10, 2009; 77 FR 8749, Fruit, stone, group 12 ...... 0 .5 Feb. 15, 2012; 78 FR 78738, Dec. 27, 2013] Goat, meat ...... 0.02 Goat, meat byproducts ...... 0 .04 § 180.565 Thiamethoxam; tolerances Grain, aspirated fractions ...... 2 .0 for residues. Grain, cereal, group 15, except barley ...... 0.02 Grape, raisin ...... 0 .30 (a) General. Tolerances are estab- Hog, meat ...... 0 .02 lished for residues of the insecticide Hog, meat byproducts ...... 0 .02 thiamethoxam, including its metabo- Hop, dried cones ...... 0 .10 Horse, meat ...... 0 .02 lites and degradates, in or on the fol- Horse, meat byproducts ...... 0 .04 lowing commodities. Compliance with Mango ...... 0.40 the tolerance levels specified below is Milk ...... 0.02 to be determined by measuring only Millet, pearl, forage ...... 0 .02 Millet, pearl, stover ...... 0 .02 thiamethoxam 3-[(2-chloro-5- Millet, proso, forage ...... 0 .02 thiazolyl)methyl]tetrahydro-5-methyl- Millet, proso, stover ...... 0 .02 N-nitro-4H-1,3,5-oxadiazin-4-imine and Millet, proso, straw ...... 0 .02 its metabolite CGA–322704 N-[(2-chloro- Mustard, seed ...... 0 .02 Nut, tree, group 14 ...... 0 .02 thiazol-5-yl)methyl]-N′-methyl-N″- Oat, forage ...... 0 .50 nitro-guanidine, calculated as the stoi- Oat, hay ...... 0.02 chiometric equivalent of Oat, straw ...... 0.02 Onion, dry bulb ...... 0 .03 thiamethoxam, in or on the following Papaya ...... 0 .40 commodities: Peanut ...... 0 .05

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amino]oxy]methyl]benzoate, calculated Commodity Parts per million as the stoichiometric equivalent of Peanut, hay ...... 0.25 fenpyroximate. Peanut, meal ...... 0 .15 Peppermint, tops ...... 1 .5 Commodity Parts per Pistachio ...... 0.02 million Potato ...... 0 .25 Radish, tops ...... 0 .80 Almond, hulls ...... 3 .0 Avocado ...... 0 .15 Rapeseed, seed ...... 0 .02 Bean, snap, succulent ...... 0 .40 Rye, forage ...... 0 .50 Berry, low growing, subgroup 13–07G ...... 1 .0 Rye, straw ...... 0 .02 Canistel ...... 0 .15 Safflower, seed ...... 0 .02 Citrus, dried pulp ...... 2 .5 Sapodilla ...... 0 .40 Citrus, oil ...... 10 Sapote, black ...... 0 .40 Corn, field, forage ...... 2 .0 Sapote, mamey ...... 0 .40 Corn, field, grain ...... 0 .02 Sheep, meat ...... 0.02 Corn, field, refined oil ...... 0 .05 Sheep, meat byproducts ...... 0 .04 Corn, field, stover ...... 7 .0 Sorghum, forage ...... 0 .02 Corn, pop, forage ...... 2 .0 Sorghum, grain, stover ...... 0 .02 Corn, pop, grain ...... 0.02 Soybean, hulls ...... 0 .08 Corn, pop, stover ...... 7.0 Spearmint, tops ...... 1 .5 Cotton, gin byproducts ...... 10 Star apple ...... 0 .40 Cotton, undelinted seed ...... 0 .10 Sunflower ...... 0 .02 Cucumber ...... 0 .40 Tea, dried 1 ...... 20 Fruit, citrus, group 10–10 ...... 0 .50 Tomato, paste ...... 0 .80 Fruit, pome, group 11–10 ...... 0 .30 Vegetable, cucurbit, group 9 ...... 0.2 Fruit, small, vine climbing, except fuzzy Vegetable, fruiting, group 8 ...... 0.25 kiwifruit, subgroup 13–07F ...... 1 .0 Vegetable, leafy, except brassica, group 4 ...... 4 .0 Fruit, stone, group 12–12 ...... 2 .0 Vegetable, legume, group 6 ...... 0 .02 Grain, aspirated fractions ...... 0 .40 Vegetable, root, subgroup 1A ...... 0 .05 Hop, dried cones ...... 10 Vegetable, tuberous and corm, except potato, Mango ...... 0.15 subgroup 1D ...... 0 .02 Melon subgroup 9A ...... 0 .10 Wheat, forage ...... 0 .50 Nut, tree, group 14 ...... 0 .10 Wheat, hay ...... 0 .02 Papaya ...... 0 .15 Wheat, straw ...... 0 .02 Peppermint, tops ...... 7 .0 Pistachio ...... 0.10 1 There are no U.S. registrations as of March 27, 2013. Sapodilla ...... 0 .15 Sapote, black ...... 0 .15 (b) Section 18 emergency exemptions. Sapote, mamey ...... 0 .15 [Reserved] Spearmint, tops ...... 7 .0 (c) Tolerances with regional registra- Star, apple ...... 0 .15 Tea, dried 1 ...... 20 tions. [Reserved] Vegetable, fruiting, group 8–10 ...... 0 .20 (d) Indirect or inadvertent residues. Vegetable, tuberous and corm, subgroup 1C ... 0.10 [Reserved] 1 There are no U.S. Registrations. [65 FR 79762, Dec. 20, 2000] (2) Tolerances are established for res- EDITORIAL NOTE: For FEDERAL REGISTER ci- idues of the insecticide fenpyroximate, tations affecting § 180.565, see the List of CFR including its metabolites and Sections Affected, which appears in the degradates, in or on the commodities Finding Aids section of the printed volume in the table below. Compliance with and at www.fdsys.gov. the tolerance levels specified in the table is to be determined by measuring § 180.566 Fenpyroximate; tolerances for residues. only the sum of fenpyroximate, (E)-1,1- dimethylethyl 4-[[[[(1,3-dimethyl-5- (a) General. (1) Tolerances are estab- phenoxy-1H-pyrazol-4-yl)methylene] lished for residues of the insecticide amino]oxy]methyl]benzoate and its fenpyroximate, including its metabo- metabolites (E)-4-[(1,3-dimethyl-5- lites and degradates, in or on the com- phenoxypyrazol-4-yl)-methyleneamino modities in the table below. Compli- oxymethyl]benzoic acid and (E)-1,1- ance with the tolerance levels specified dimethylethyl-2-hydroxyethyl 4-[[[[(1,3- in the table is to be determined by dimethyl-5-phenoxy-1H-pyrazol-4-yl) measuring only the sum of methylene]amino]oxy]methyl]ben- fenpyroximate, (E)-1,1-dimethylethyl 4- zoate, calculated as the stoichiometric [[[[(1,3-dimethyl-5-phenoxy-1H-pyrazol- equivalent of fenpyroximate. 4-yl)methylene]amino]oxy]methyl]benzoate and its Z-isomer, (Z)-1,1- Commodity Parts per dimethylethyl 4-[[[[(1,3-dimethyl-5- million phenoxy-1H-pyrazol-4-yl)methylene] Cattle, fat ...... 0.03

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Parts per Expiration/revoca- Commodity million Commodity Parts per million tion date

Cattle, meat ...... 0 .03 Honey ...... 0.10 12/31/13 Cattle, meat byproducts, except kidney and liver ...... 0 .03 Goat, fat ...... 0 .03 (c) Tolerances with regional registra- Goat, meat ...... 0.03 tions. [Reserved] Goat, meat byproducts, except kidney and liver 0 .03 (d) Indirect or inadvertent residues. Horse, fat ...... 0 .03 [Reserved] Horse, meat ...... 0 .03 Horse, meat byproducts, except kidney and [66 FR 18568, Apr. 10, 2001, as amended at 69 liver ...... 0 .03 Milk ...... 0.015 FR 32464, June 10, 2004; 71 FR 49368, Aug. 23, Sheep, fat ...... 0 .03 2006; 72 FR 26321, May 9, 2007; 74 FR 37617, Sheep, meat ...... 0.03 July 29, 2009; 74 FR 63079, Dec. 2, 2009; 75 FR Sheep, meat byproducts, except kidney and 80346, Dec. 22, 2010; 77 FR 73951, Dec. 12, 2012; liver ...... 0 .03 78 FR 36097, June 17, 2013]

(3) Tolerances are established for res- § 180.567 Zoxamide; tolerances for resi- idues of the insecticide fenpyroximate, dues. including its metabolites and (a) General. (1) Tolerances are estab- degradates, in or on the commodities lished for residues of zoxamide (3,5- in the table below. Compliance with dichloro-N-(3-chloro-1-ethyl-1-methyl- the tolerance levels specified in the 2-oxopropyl)-4-methylbenzamide) in or table is to be determined by measuring on the following commodities: only the sum of fenpyroximate, (E)-1,1- dimethylethyl 4-[[[[(1,3-dimethyl-5- Commodity Parts per phenoxy-1H-pyrazol-4-yl)methylene] million amino]oxy]methyl]benzoate and its Grape ...... 3 .0 metabolite (E)-4-[(1,3-dimethyl-5- Grape, raisin ...... 15.0 phenoxypyrazol-4-yl)-methyleneamino Tomato ...... 2.0 oxymethyl]benzoic acid, calculated as Vegetable, cucurbit, group 9 ...... 1.0 the stoichiometric equivalent of (2) Tolerances are established for the fenpyroximate. combined residues of zoxamide and its metabolites 3,5-dichloro-1,4- Commodity Parts per million benzenedicarboxylic acid (RH–1455 and Cattle, kidney ...... 0 .25 RH–141455) and 3,5-dichloro-4- Cattle, liver ...... 0 .25 hydroxymethylbenzoic acid (RH–1452 Goat, kidney ...... 0 .25 and RH–141452) in or on the following Goat, liver ...... 0.25 commodities: Horse, kidney ...... 0 .25 Horse, liver ...... 0 .25 Sheep, kidney ...... 0.25 Parts per Commodity million Sheep, liver ...... 0.25 Potato ...... 0 .060 (b) Section 18 emergency exemptions. Potato, granules/flakes ...... 0 .30 Time-limited tolerances are estab- Potato, wet peel ...... 0 .10 lished for residues of the insecticide fenpyroximate, including its metabo- (b) Section 18 emergency exemptions. A lites and degradates in or on the com- time-limited tolerance is established modities in the table below. Compli- for residues of the fungicide zoxamide ance with the tolerance levels specified (3,5-dichloro-N-(3-chloro-1-ethyl-1- in the table is to be determined by methyl-2-oxopropyl)-4- measuring only the sum of methylbenzamide) in connection with fenpyroximate, (E)-1,1-dimethylethyl 4- use of the pesticide under a section 18 [[[[(1,3-dimethyl-5-phenoxy-1H-pyrazol- emergency exemption granted by EPA. 4-yl) meth- The tolerance will expire and is re- ylene]amino]oxy]methyl]benzoate and voked on the date specified in the fol- its Z-isomer, (Z)-1,1-dimethylethyl 4- lowing table. [[[[(1,3-dimethyl-5-phenoxy-1H-pyrazol- Parts per Revocation 4-yl)methylene]amino]oxy]methyl]ben- Commodity million date zoate, calculated as the stoichiometric equivalent of fenpyroximate. Ginseng ...... 0.06 12/31/10

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(c) Tolerances with regional registra- Commodity Parts per tions. [Reserved] million (d) Indirect or inadvertent residues. Wheat, grain ...... 0 .40 [Reserved] Wheat, hay ...... 0 .02 Wheat, straw ...... 6 .0 [66 FR 18733, Apr. 11, 2001, as amended at 66 FR 49118, Sept. 26, 2001; 69 FR 16805, Mar. 31, (b) Section 18 emergency exemptions. 2004; 71 FR 31104, June 1, 2006; 71 FR 76200, [Reserved] Dec. 20, 2006; 75 FR 770, Jan. 6, 2010] (c) Tolerances with regional registra- § 180.568 Flumioxazin; tolerances for tions. [Reserved] residues. (d) Indirect or inadvertent residues. [Reserved] (a) General. Tolerances are established for residues of flumioxazin, 2-[7- [66 FR 19878, Apr. 18, 2001, as amended at 68 fluoro-3,4-dihydro-3-oxo-4-(2-propynyl)- FR 51471, Aug. 27, 2003; 69 FR 16831, Mar. 31, 2H-1,4-benzoxazin-6-yl]-4,5,6,7- 2004; 69 FR 52198, Aug. 25, 2004; 71 FR 25956, tetrahydro-1H-isoindole-1,3(2H)-dione, May 3, 2006; 71 FR 61413, Oct. 18, 2006; 73 FR 11831, Mar. 5, 2008; 73 FR 39251, July 9, 2008; 75 including its metabolites and FR 8265, Feb. 24, 2010; 75 FR 69009, Nov. 10, degradates, in or on the commodities 2010; 77 FR 58499, Sept. 21, 2012; 78 FR 20466, in the table below. Compliance with Apr. 5, 2013] the tolerance levels specified below is to be determined by measuring only § 180.569 Forchlorfenuron; tolerances flumioxazin. for residues. (a) General. (1) Tolerances are estab- Parts per Commodity million lished for residues of forchlorfenuron, including its metabolites and Alfalfa, forage ...... 3.0 degradates, in or on the commodities Alfalfa, hay ...... 8.0 Almond, hulls ...... 0 .70 in the table below. Compliance with Artichoke, globe ...... 0.02 the tolerance levels specified below is Asparagus ...... 0.02 to be determined by measuring only Bushberry subgroup 13–07B ...... 0 .02 Cabbage ...... 0 .02 forchlorfenuron (N-(2-chloro-4- Cabbage, Chinese, napa ...... 0 .02 pyridinyl)-N-phenylurea). Corn, field, forage ...... 0 .02 Corn, field, grain ...... 0 .02 Commodity Parts per Corn, field, stover ...... 0 .02 million Cotton, gin byproducts ...... 0 .60 Cotton, undelinted seed ...... 0 .02 Almond ...... 0.01 Fish, freshwater ...... 1 .5 Almond, hulls ...... 0 .15 Fruit, pome, group 11 ...... 0.02 Bushberry subgroup 13–07B ...... 0 .01 Fruit, stone, group 12 ...... 0 .02 Cherry, sweet ...... 0 .01 Garlic ...... 0 .02 Fig ...... 0 .01 Grain, aspirated fractions ...... 100 Grape ...... 0 .03 Grape ...... 0 .02 Grape, raisin ...... 0 .06 Hop, dried cones ...... 0 .05 Kiwifruit ...... 0.04 Leaf petioles subgroup 4B ...... 0 .02 Pear ...... 0 .01 Nut, tree, group 14 ...... 0 .02 Pistachio ...... 0.01 Okra ...... 0.02 Plum, prune, fresh ...... 0.01 Olive ...... 0 .02 Onion, bulb ...... 0 .02 (2) Temporary tolerances are estab- Pea and bean, dried shelled, except soybean, lished for residues of forchlorfenuron, subgroup 6C ...... 0 .07 Peanut ...... 0 .02 including its metabolites and Peppermint, tops ...... 0 .04 degradates, in or on the commodities Pistachio ...... 0.02 in the table below. Compliance with Pomegranate ...... 0 .02 the tolerance levels specified below is Prickly pear, fruit ...... 0 .07 Prickly pear, pads ...... 0.06 to be determined by measuring on Rapeseed subgroup 20A ...... 0 .40 forchlorfenuron (N-(2-chloro-4- Shallot, bulb ...... 0 .02 pyridinyl)-N′-phenylurea). Soybean, seed ...... 0 .02 Spearmint, tops ...... 0 .04 Parts per Expiration/ Strawberry ...... 0 .07 Commodity revocation Sugarcane, cane ...... 0.20 million date Sunflower subgroup 20B ...... 0.50 Vegetable, cucurbit, group 9 ...... 0.03 Almond ...... 0.01 12/31/15 Vegetable, fruiting, group 8 ...... 0.02 Almond, hulls ...... 0.15 12/31/15 Vegetable, tuberous and corm, subgroup 1C ..... 0.02 Cherry, sweet ...... 0.01 12/31/15 Wheat, forage ...... 0 .02 Fig ...... 0.01 12/31/15

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(c) Tolerances with regional registra- Parts per Expiration/ Commodity revocation tions. [Reserved] million date (d) Indirect or inadvertent residues. Pear ...... 0.01 12/31/15 [Reserved] Pistachio ...... 0.01 12/31/15 Plum, prune, fresh ...... 0.01 12/31/15 [66 FR 33187, June 21, 2001, as amended at 66 FR 40141, Aug. 2, 2001; 67 FR 12878, Mar. 20, (b) Section 18 emergency exemptions. 2002; 69 FR 29890, May 26, 2004; 72 FR 63997, [Reserved] Nov. 14, 2007] (c) Tolerances with regional restrictions. [Reserved] § 180.571 Mesotrione; tolerances for (d) Indirect or inadvertent residues. residues. [Reserved] (a) General. Tolerances are established for residues of the herbicide [66 FR 22936, May 7, 2001, as amended at 69 FR 48805, Aug. 11, 2004; 69 FR 58322, Sept. 30, mesotrione, including its metabolites 2004; 73 FR 47846, Aug. 15, 2008; 78 FR 46283, and degradates, in or on the commod- July 31, 2013; 79 FR 18471, Apr. 2, 2014] ities in the table below. Compliance with the tolerance levels specified § 180.570 Isoxadifen-ethyl; tolerances below is to be determined by measuring for residues. only mesotrione, 2-[4-(methylsulfonyl)- (a) General. (1) Tolerances are estab- 2-nitrobenzoyl]-1,3-cyclohexanedione, lished for residues of isoxadifen-ethyl in or on the following raw agricultural (ethyl 5,5-diphenyl-2-isoxazoline-3- commodities: carboxylate, (CAS No. 163520–33–0), and Parts per its metabolite: 4,5-dihydro-5,5-di- Commodity million phenyl-3-isoxazolecarboxylic acid, when used as an inert ingredient Asparagus ...... 0.01 Berry, group 13 ...... 0 .01 (safener) in or on the following raw ag- Corn, field, forage ...... 0 .01 ricultural commodities: Corn, field, grain ...... 0 .01 Corn, field, stover ...... 0 .01 Parts per Corn, pop, grain ...... 0.01 Commodity million Corn, pop, stover ...... 0.01 Corn, field, forage ...... 0 .20 Corn, sweet, forage ...... 0 .5 Corn, field, grain ...... 0 .08 Corn, sweet, kernel plus cob with husks re- Corn, field, stover ...... 0 .40 moved ...... 0 .01 Corn, oil ...... 0 .50 Corn, sweet, stover ...... 1 .5 Corn, pop, grain ...... 0.04 Cranberry ...... 0 .02 Corn, pop, stover ...... 0.25 Flax, seed ...... 0 .01 Corn, sweet, forage ...... 0 .30 Grass, forage ...... 0 .01 Corn, sweet, kernel plus cob with husk removed 0.04 Grass, hay ...... 0 .01 Corn, sweet, stover ...... 0 .45 Grass, seed screenings ...... 0 .10 Grass, straw ...... 0 .10 (2) Tolerances are established for the Lingonberry ...... 0.01 residues of isoxadifen-ethyl (3- Millet, forage ...... 0 .01 isoxazolecarboxylic acid, 4,5-dihydro- Millet, grain ...... 0 .01 Millet, hay ...... 0 .02 5,5-diphenyl-, ethyl ester (CAS No. Millet, straw ...... 0 .02 164520–33–0)), and its metabolites 4,5- Oat, forage ...... 0 .01 dihydro-5,5-diphenyl-3- Oat, grain ...... 0 .01 isoxazolecarboxylic acid and b-hy- Oat, hay ...... 0.01 droxy-b-benzenepropanenitrile when Oat, straw ...... 0.01 Okra ...... 0.01 used as an inert ingredient (safener) in Rhubarb ...... 0 .01 or on the following raw agricultural Sorghum, grain, forage ...... 0.01 commodities: Sorghum, grain, grain ...... 0 .01 Sorghum, grain, stover ...... 0 .01 Commodity Parts per Sorghum, sweet ...... 0 .01 million Soybean, seed ...... 0 .01 Sugarcane, cane ...... 0.01 Rice, grain ...... 0 .10 Rice, hulls ...... 0 .50 Rice, straw ...... 0 .25 (b) Section 18 emergency exemptions. [Reserved] (b) Section 18 emergency exemptions. (c) Tolerances with regional registra- [Reserved] tions. [Reserved]

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(d) Indirect or inadvertent residues. Commodity Parts per [Reserved] million [66 FR 33195, June 21, 2001, as amended at 67 Pistachio ...... 0.20 FR 45656, July 10, 2002; 68 FR 273, Jan. 3, 2003; Plum ...... 0 .20 Pulasan ...... 5 .0 69 FR 58310, Sept. 30, 2004; 70 FR 14551, Mar. Rambutan ...... 5 .0 23, 2005; 72 FR 71802, Dec. 19, 2007; 73 FR 1512, Sapodilla ...... 7 .0 Jan. 9, 2008; 73 FR 9226, Feb. 20, 2008; 74 FR Sapote, mamey ...... 7 .0 67123, Dec. 18, 2009; 76 FR 34886, June 15, 2011] Sheep, fat ...... 0 .10 Soursop ...... 1 .6 § 180.572 Bifenazate; tolerance for resi- Soybean, succulent shelled ...... 0 .70 Spanish lime ...... 5 .0 dues. Spearmint, tops ...... 25 (a) General. (1) Tolerances are estab- Star apple ...... 7 .0 Starfruit ...... 0 .90 lished for residues of bifenazate (1- Strawberry ...... 1 .5 methylethyl 2-(4-methoxy[1,1′- Sugar apple ...... 1 .6 biphenyl]-3-yl)hydrazinecarboxylate) Vegetable, cucurbit, group 9 ...... 0.75 including its metabolites and Vegetable, fruiting, group 8 ...... 2.0 Vegetable, legume, edible-podded, subgroup 6A 6.0 degradates, in or on the commodities Vegetable, tuberous and corm, subgroup 1C ..... 0.10 listed in the following table. Compli- Wax jambu ...... 0 .90 ance with the tolerance levels specified are to be determined by measuring (2) Tolerances are established for res- only the sum of bifenazate and its me- idues of bifenazate (1-methylethyl 2-(4- tabolite diazinecarboxylic acid, 2-(4- methoxy[1,1′-biphenyl]-3-yl) methoxy-[1,1′-biphenyl]-3-yl), 1- hydrazinecarboxylate) including its methylethyl ester (expressed as metabolites and degradates, in or on bifenazate) in or on the following food the commodities listed in the following commodities: table. Compliance with the tolerance levels specified are to be determined by Commodity Parts per measuring only the sum of bifenazate million and its metabolites diazinecarboxylic Acerola ...... 0.90 acid, 2-(4-methoxy-[1,1′-biphenyl]-3-yl), Almond, hulls ...... 15 1-methylethyl ester (expressed as Apple, wet pomace ...... 1 .2 ′ ′ Atemoya ...... 1 .6 bifenazate); 1,1 -biphenyl, 4-ol; and 1,1 - Avocado ...... 7 .0 biphenyl, 4-oxysulfonic acid (expressed Bean, dry seed ...... 0 .60 as 1,1′-biphenyl, 4-ol) in or on the fol- Berry, low-growing subgroup 13–07G ...... 1 .5 Biriba ...... 1 .6 lowing food commodities: Black sapote ...... 7 .0 Caneberry subgroup 13-07A ...... 5.0 Parts per mil- Commodity lion Canistel ...... 7 .0 Cattle, fat ...... 0.10 Cattle, meat ...... 0.02 Cherimoya ...... 1 .6 Cattle, meat byproducts ...... 0.02 Cotton, gin byproducts ...... 35 Goat, meat ...... 0.02 Cotton, undelinted seed ...... 0 .75 Goat, meat byproducts ...... 0.02 Custard apple ...... 1 .6 Hog, meat ...... 0.02 Feijoa ...... 0 .90 Hog, meat byproducts ...... 0.02 Fruit, pome, group 11 ...... 0.75 Horse, meat ...... 0.02 Fruit, small, vine climbing subgroup 13–07F, ex- Horse, meat byproducts ...... 0.02 cept fuzzy kiwifruit ...... 1 .0 Milk ...... 0.02 Fruit, stone, group 12, except plum ...... 2 .5 Sheep, meat ...... 0.02 Goat, fat ...... 0 .10 Sheep, meat byproducts ...... 0.02 Grape ...... 0 .75 Grape, raisin ...... 1 .2 Guava ...... 0 .9 (b) Section 18 emergency exemptions. Hog, fat ...... 0 .10 Time-limited tolerances are estab- Hop, dried cones ...... 15 lished for residues of bifenazate (1- Horse, fat ...... 0 .10 ′ Jaboticaba ...... 0 .90 methylethyl 2-(4-methoxy[1,1 - Ilama ...... 1 .6 biphenyl]-3-yl)hydrazinecarboxylate) Longan ...... 5 .0 including its metabolites and Lychee ...... 5 .0 degradates in connection with use of Mango ...... 7.0 Nut, tree, group 14 ...... 0 .20 the pesticide under section 18 emer- Okra ...... 2.0 gency exemptions granted by EPA. Papaya ...... 7 .0 Compliance with the tolerance levels Passionfruit ...... 0 .90 Pea and bean, succulent shelled, subgroup 6B 0 .70 specified in the following table are to Peppermint, tops ...... 25 be determined by measuring only the

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sum of bifenazate and its metabolite Compliance with the tolerance levels diazinecarboxylic acid, 2-(4-methoxy- specified below is to be determined by [1,1′-biphenyl]-3-yl), 1-methylethyl measuring only the combined residues ester (expressed as bifenazate). The tol- of tepraloxydim (2-[1-[[[(2E)-3-chloro-2- erances will expire and are revoked on propen-1-yl]oxy]imino]propyl]-3-hy- the dates specified in the following droxy-5-(tetrahydro-2H-pyran-4-yl)-2- table. cyclohexen-1-one) and its metabolites convertible to GP (3-(tetrahydropyran- Expiration/ Commodity Parts per Revocation 4-yl)pentane-1,5-dioic acid), OH–GP (3- million Date hydroxy-3-(tetrahydropyran-4- Timothy, forage ...... 50 12/31/16 yl)pentane-1,5-dioic acid), and GL (3-(2- Timothy, hay ...... 150 12/31/16 oxotetrahydropyran-4-yl)-1,5-dioic acid), calculated as tepraloxydim, in or (c) Tolerances with regional registra- on the commodities. tions. [Reserved] (d) Indirect or inadvertent residues. Parts per Commodity million [Reserved] Cattle, fat ...... 0.15 [66 FR 34569, June 29, 2001] Cattle, kidney ...... 0 .50 EDITORIAL NOTE: For FEDERAL REGISTER ci- Cattle, meat ...... 0 .20 tations affecting § 180.572, see the List of CFR Cattle, meat byproducts, except kidney ...... 0.20 Sections Affected, which appears in the Egg ...... 0 .20 Finding Aids section of the printed volume Goat, fat ...... 0 .15 Goat, kidney ...... 0 .50 and at www.fdsys.gov. Goat, meat ...... 0.20 Goat, meat byproducts, except kidney ...... 0 .20 § 180.573 Tepraloxydim; tolerances for Hog, fat ...... 0 .15 residues. Hog, kidney ...... 0.50 (a) General. (1) Tolerances are estab- Hog, meat ...... 0 .20 Hog, meat byproducts, except kidney ...... 0 .20 lished for residues of tepraloxydim, in- Horse, fat ...... 0 .15 cluding its metabolites and degradates, Horse, kidney ...... 0 .50 in or on the commodities in the table Horse, meat ...... 0 .20 below. Compliance with the tolerance Horse, meat byproducts, except kidney ...... 0 .20 levels specified below is to be deter- Milk ...... 0.10 Poultry, fat ...... 0.30 mined by measuring only the combined Poultry, liver ...... 1 .00 residues of tepraloxydim, (2-[1-[[[(2E)-3- Poultry, meat ...... 0 .20 chloro-2-propen-1-yl]oxy]imino]propyl]- Poultry, meat byproducts, except liver ...... 0 .20 3-hydroxy-5-(tetrahydro-2H-pyran-4-yl)- Sheep, fat ...... 0 .15 Sheep, kidney ...... 0.50 2-cyclohexen-1-one) and its metabolites Sheep, meat ...... 0.20 convertible to GP (3-(tetrahydropyran- Sheep, meat byproducts, except kidney ...... 0 .20 4-yl)pentane-1,5-dioic acid) and OH–GP (3-hydroxy-3-(tetrahydropyran-4- (b) Section 18 emergency exemptions. yl)pentane-1,5-dioic acid), calculated as [Reserved] tepraloxydim, in or on the commod- (c) Tolerances with regional registra- ities. tions. A tolerance with regional registration, as defined in § 180.1(l), is es- Parts per Commodity million tablished for residues of tepraloxydim, including its metabolites and Cotton, undelinted seed ...... 0 .2 degradates, in or on the commodities Cotton, gin byproducts ...... 3 .0 Flax, seed ...... 0 .10 in the table below. Compliance with Grain, aspirated fraction ...... 1200.0 the tolerance levels specified below is Pea and bean, dried shelled, except soybean, to be determined by measuring only subgroup 6C 1 ...... 0 .10 Soybean, seed ...... 6 .0 the combined residues of tepraloxydim Soybean, hulls ...... 8 .0 (2-[1-[[[(2E)-3-chloro-2-propen-1- Sunflower subgroup 20B 1 ...... 0.20 yl]oxy]imino]propyl]-3-hydroxy-5- 1 There are no U.S. registrations for commodities in this (tetrahydro-2H-pyran-4-yl)-2-cyclo- subgroup. hexen-1-one) and its metabolites con- (2) Tolerances are established for res- vertible to GP (3-(tetrahydropyran-4- idues of tepraloxydim, including its yl)pentane-1,5-dioic acid) and OH–GP metabolites and degradates, in or on (3-hydroxy-3-(tetrahydropyran-4- the commodities in the table below. yl)pentane-1,5-dioic acid), calculated as

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tepraloxydim, in or on the commod- Commodity Parts per ities. million Grape, wine 1 ...... 3 .0 Commodity Parts per million 1 No US registration as of March 15, 2002.

Canola, seed ...... 0 .50 (3) Tolerances are established for residues of fluazinam (3-chloro-N-[3- (d) Indirect or inadvertent residues. chloro-2,6-dinitro-4- [Reserved] (trifluoromethyl)phenyl]-5- (trifluoromethyl)-2-pyridinamine), in- [66 FR 40150, Aug. 2, 2001 as amended at 72 FR 54588, Sept. 26, 2007; 76 FR 34885, June 15, 2011; cluding its metabolites and degradates, 76 FR 82152, Dec. 30, 2011] in or on the commodities in the table below. Compliance with the tolerance § 180.574 Fluazinam; tolerances for levels specified below is to be deter- residues. mined by measuring only fluazinam, (a) General. (1) Tolerances are estab- AMPA (2-(6-amino-3-chloro-a,a,a- lished for residues of fluazinam (3- trifluoro-2-nitro-p-toluidino)-3-chloro- chloro-N-[3-chloro-2,6-dinitro-4- 5-(trifluoromethyl) pyridine), DAPA (3- (trifluoromethyl)phenyl]-5- chloro-2-(2,6-diamino-3-chloro-a,a,a.- (trifluoromethyl)-2-pyridinamine), in- trifluoro-p-toluidino)-5- cluding its metabolites and degradates, (trifluoromethyl)pyridine), and their in or on the commodities in the table sulfamate conjugates. below. Compliance with the tolerance Parts per levels specified below is to be deter- Commodity million mined by measuring only fluazinam. Cattle, fat ...... 0.05 Cattle, meat byproducts ...... 0.05 Commodity Parts per Goat, fat ...... 0 .05 million Goat, meat byproducts ...... 0 .05 Horse, fat ...... 0 .05 Apple ...... 2.0 Horse, meat byproducts ...... 0 .05 Apple, wet pomace ...... 5 .0 Sheep, fat ...... 0 .05 Bushberry subgroup 13-07B ...... 7 .0 Sheep, meat byproducts ...... 0 .05 Carrot, roots ...... 0.70 Ginseng ...... 4 .5 (b) Section 18 emergency exemptions. Lettuce, head ...... 0.02 Lettuce, leaf ...... 2 .0 [Reserved] Melon subgroup 9A ...... 0 .07 (c) Tolerances with regional registra- Onion, bulb, subgroup 3-07A ...... 0 .20 tions. [Reserved] Pea and bean, dried shelled, except soybean, (d) Indirect or inadvertent residues. subgroup 6C, except pea ...... 0.02 [Reserved] Pea and bean, succulent shelled, subgroup 6B, except pea ...... 0 .04 [66 FR 46738, Sept. 7, 2001, as amended at 67 Peanut ...... 0 .02 FR 19130, Apr. 18, 2002; 72 FR 60260, Oct. 24, Pepper/eggplant subgroup 8–10B ...... 0 .09 2007; 75 FR 26667, May 12, 2010; 76 FR 3029, Potato ...... 0 .02 Soybean, seed ...... 0 .01 Jan. 19, 2011; 77 FR 66729, Nov. 7, 2012] Soybean, hulls ...... 0 .05 Turnip, greens ...... 0.01 § 180.575 Sulfuryl fluoride; tolerances Vegetable, Brassica leafy, group 5 ...... 0.01 for residues. Vegetable, legume, edible-podded, subgroup (a)(1) General. Tolerances are estab- 6A, except pea ...... 0.10 lished for residues of sulfuryl fluoride (2) Tolerances are established for resin or on the following commodities idues of fluazinam, including its me- from the postharvest fumigation with tabolites and degradates, in or on the sulfuryl fluoride for the control of in- commodities in the table below. Com- sects: pliance with the tolerance levels speci- Parts per fied below is to be determined by meas- Commodity million uring only fluazinam and its metabo- All processed food commodities not otherwise lite AMGT (3-[[4-amino-3-[[3-chloro-5- listed ...... 2 .0 (trifluoromethyl)-2-pyridinyl]amino]-2- Barley, bran, postharvest ...... 0 .05 nitro-6-(trifluoromethyl) phenyl]thio]- Barley, flour, postharvest ...... 0.05 Barley, grain, postharvest ...... 0 .1 2-(beta-D-glucopyranosyloxy) propionic Barley, pearled barley, postharvest ...... 0 .05 acid). Cacao bean, roasted bean, postharvest ...... 0.2

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[R-(+)-2-(4(4-cyano-2-fluorophenoxy)- Commodity Parts per million phenoxy)propionic acid], and the di- Cattle, meat, dried ...... 0.01 acid metabolite [(2R)-4-(4-(1- Cheese ...... 2 .0 carboxyethoxy)phenoxy)-3- Coconut, postharvest ...... 1 .0 fluorobenzoic acid]. Coffee, bean, roasted bean, postharvest ...... 1 .0 Corn, field, flour, postharvest ...... 0 .01 Parts per Corn, field, grain, postharvest ...... 0 .05 Commodity million Corn, field, grits, postharvest ...... 15.0 Corn, field, meal, postharvest ...... 0 .01 Rice, grain ...... 0 .40 Corn, pop, grain, postharvest ...... 0 .05 Wild rice, grain ...... 0 .40 Cotton, undelinted seed, postharvest ...... 0.5 Egg, dried ...... 1 .0 Fruit, dried, postharvest ...... 0 .05 (b) Section 18 emergency exemptions. Ginger, postharvest ...... 0 .5 [Reserved] Grain, aspirated fractions, postharvest ...... 0 .05 (c) Tolerances with regional registra- Herbs and spices group 19, postharvest ...... 0 .5 Hog, meat ...... 0 .02 tions. [Reserved] Milk, powdered ...... 2 .0 (d) Indirect or inadvertent residues. Millet, grain, postharvest ...... 0.1 [Reserved] Nut, pine, postharvest ...... 0.2 Nut, tree, Group 14, postharvest ...... 3 .0 [67 FR 43256, June 27, 2002, as amended at 74 Oat, flour, postharvest ...... 0 .05 FR 15880, Apr. 8, 2009; 76 FR 82157, Dec. 30, Oat, grain, postharvest ...... 0 .1 Oat, groats/rolled oats, postharvest ...... 0 .1 2011] Peanut, postharvest ...... 0 .5 Pistachio, postharvest ...... 3 .0 § 180.577 Bispyribac-sodium; toler- Rice, bran, postharvest ...... 0 .01 ances for residues. Rice, flour, postharvest ...... 0 .05 Rice, grain, postharvest ...... 0 .04 (a) General. Tolerances are estab- Rice, hulls, postharvest ...... 0.1 lished for residues of the herbicide Rice, polished rice, postharvest ...... 0 .01 bispyribac-sodium, including its me- Rice, wild, grain, postharvest ...... 0 .05 Sorghum, grain, grain, postharvest ...... 0.1 tabolites and degradates, in or on the Triticale, grain, postharvest ...... 0 .1 commodity listed below. Compliance Vegetable, legume, group 6, postharvest ...... 0.5 with the tolerance level specified below Wheat, bran, postharvest ...... 0 .05 Wheat, flour, postharvest ...... 0 .05 is to be determined by measuring only Wheat, germ, postharvest ...... 0 .02 bispyribac-sodium, (2,6-bis[(4,6- Wheat, grain, postharvest ...... 0 .1 dimethoxy-2-pyrimidinyl)oxy]benzoic Wheat, milled byproducts, postharvest ...... 0 .05 Wheat, shorts, postharvest ...... 0 .05 acid, sodium salt), in or on the following raw agricultural commodities: (2) To assure safe use of this pesticide Parts per commodities treated with sulfuryl flu- Commodity million oride must be aerated for at least 24 Fish, freshwater ...... 0 .01 hours prior to entering commerce. Rice, grain ...... 0 .02 (b) Section 18 emergency exemptions. Rice, straw ...... 0 .02 [Reserved] (c) Tolerances with regional registra- (b) Section 18 emergency exemptions. tion. [Reserved] [Reserved] (d) Indirect or inadvertant residues. (c) Tolerances with regional registra- [Reserved] tions. [Reserved] (d) Indirect or inadvertent residues. [67 FR 5740, Feb. 7, 2002, as amended at 69 FR 3257, Jan. 23, 2004; 70 FR 40908, July 15, 2005] [Reserved] [66 FR 48097, Sept. 18, 2001, as amended at 76 § 180.576 Cyhalofop-butyl; tolerances FR 5716, Feb. 2, 2011] for residues. (a) General. Tolerances are estab- § 180.578 Acetamiprid; tolerances for lished for residues of cyhalofop-butyl, residues. including its metabolites and (a) General. (1) Tolerances are estab- degradates, in or on the commodities lished for residues of the insecticide listed in the table below. Compliance acetamiprid (1E)-N-[(6-chloro-3- with the tolerance levels specified pyridinyl)methyl]-N’-cyano-N- below is to be determined by measuring methylethanimidamide, including its cyhalofop butyl [R-(+)-n-butyl-2-(4(4- metabolites and degradates, in or on cyano-2-fluorophenoxy)- the commodities in the table below as phenoxy)propionate], cyhalofop acid a result of the application of

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acetamiprid. Compliance with the tol- Commodity Parts per erance levels specified below is to be million determined by measuring only Cattle, meat ...... 0 .30 acetamiprid in or on the following Cattle, meat byproducts ...... 0.70 commodities. Egg ...... 0 .010 Goat, fat ...... 0 .20 Commodity Parts per Goat, meat ...... 0.30 million Goat, meat byproducts ...... 0 .70 Almond, hulls ...... 5 .0 Hog, fat ...... 0 .10 Asparagus ...... 0.80 Hog, meat ...... 0 .10 Berry, low growing subgroups 13–07G ...... 0.60 Hog, meat byproducts ...... 0 .20 Brassica, head and stem, subgroup 5A ...... 1 .20 Horse, fat ...... 0 .20 Brassica, leafy greens, subgroup 5B ...... 15 Horse, meat ...... 0 .30 Bushberry subgroup 13–07B ...... 1 .6 Horse, meat byproducts ...... 0 .70 Caneberry subgroup 13–07A ...... 1.6 Milk ...... 0.30 Canola, seed ...... 0 .010 Poultry, fat ...... 0.010 Citrus, dried pulp ...... 1 .20 Corn, sweet, forage ...... 15 Poultry, liver ...... 0 .050 Corn, sweet, kernel plus cob with husks re- Poultry, meat ...... 0 .010 moved ...... 0 .01 Sheep, fat ...... 0 .20 Corn, sweet, stover ...... 30 Sheep, meat ...... 0.30 Cotton, gin byproducts ...... 20 .0 Sheep, meat byproducts ...... 0 .70 Cotton, undelinted seed ...... 0 .60 Fruit, citrus, group 10–10 ...... 1 .0 Fruit, pome, group 11–10 ...... 1 .0 (3) A tolerances of 0.01 ppm is estab- Fruit, small, vine climbing, except fuzzy lished for residues of the insecticide kiwifruit, subgroup 13-07F ...... 0 .35 acetamiprid, including its metabolites Fruit, stone, group 12, except plum, prune ...... 1 .20 Grain, aspirated fractions ...... 5 .0 and degradates, in or on all food/feed Mustard, seed ...... 0 .010 items (other than those covered by a Nut, tree, group 14 ...... 0 .10 higher tolerance in paragraph (a)(1) or Onion, bulb, subgroup 3–07A ...... 0 .02 Onion, green, subgroup 3–07B ...... 4 .5 (a)(2) of this section as a result of the Pea and bean, succulent shelled, subgroup 6B 0 .40 use on growing crops) as a result of the Pistachio ...... 0.10 application of acetamiprid in food/feed Plum, prune, dried ...... 0.40 Plum, prune, fresh ...... 0.20 handling establishments. Compliance Soybean, hulls ...... 0 .04 with the 0.01 ppm tolerance level is to Soybean, seed ...... 0 .03 be determined by measuring only Tea, dried1 ...... 50.0 Tomato, paste ...... 0 .40 acetamiprid (1E)-N-[(6-chloro-3- Turnip greens ...... 15 pyridinyl)methyl]-N′-cyano-N- Vegetable, cucurbit, group 9 ...... 0.50 methylethanimidamide in or on the Vegetable, fruiting, group 8–10 ...... 0 .20 Vegetable, leafy, except brassica, group 4 ...... 3 .00 commodities. Vegetable, legume, edible podded, subgroup (b) Section 18 emergency exemptions. 6A ...... 0 .60 Vegetable, tuberous and corm, group 1 ...... 0 .01 [Reserved] (c) Tolerances with regional registra- 1There are no U.S. registrations as of February 10, 2010, for the use of acetamiprid on dried tea. tions. Tolerances with regional registrations are established for residues (2) Tolerances are established for residues of the insecticide acetamiprid of the insecticide acetamiprid (1E)-N- ′ (1E)-N-[(6-chloro-3-pyridinyl)methyl]- [(6-chloro-3-pyridinyl)methyl]-N - N′-cyano-N-methylethanimidamide, in- cyano-N-methylethanimidamide, including its metabolites and degradates, cluding its metabolites and degradates, in or on the commodities in the table in or on the commodities in the table below as a result of the application of below as a result of the application of acetamiprid. Compliance with the tol- acetamiprid. Compliance with the tolerance levels specified below is to be erance levels specified below is to be determined by measuring acetamiprid determined by measuring only and (1E)-N-[(6-chloro-3- acetamiprid in or on the following pyridinyl)methyl]-N′-cyano-N- commodities. ethanimidamide in or on the following commodities. Parts per Commodity million Parts per Commodity million Clover, forage ...... 0.10 Clover, hay ...... 0.01 Cattle, fat ...... 0.20

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(d) Indirect or inadvertent residues. Commodity Parts per [Reserved] million [67 FR 14659, Mar. 27, 2002, as amended at 68 Goat, fat ...... 0 .10 FR 52352, Sept. 3, 2003; 70 FR 19293, Apr. 13, Goat, meat ...... 0.10 Goat, meat byproducts ...... 0 .10 2005; 72 FR 67262, Nov. 28, 2007; 73 FR 2811, Milk ...... 0.02 Jan. 16, 2008; 75 FR 6582, Feb. 10, 2010; 77 FR Sheep, fat ...... 0 .10 18716, Mar. 28, 2012; 77 FR 43529, July 25, 2012; Sheep, meat ...... 0.10 78 FR 36676, June 19, 2013] Sheep, meat byproducts ...... 0 .10

§ 180.579 Fenamidone; tolerances for (b) Section 18 emergency exemptions. residues. [Reserved] (a) General. (1) Tolerances are estab- (c) Tolerances with regional registra- lished for residues of the fungicide, tions. A tolerance with regional reg- fenamidone, including its metabolites istration as defined in § 180.1(l) is estab- and degradates, in or on the following lished for residues of the fungicide commodities. Compliance with the tol- fenamidone, including its metabolites erance levels is to be determined by and degradates, in or on the following measuring only fenamidone (4H- commodities. Compliance with the tol- Imidazol-4-one, 3,5-dihydro-5-methyl-2- erance levels is to be determined by (methylthio)-5-phenyl-3 (phenylamino)- measuring only fenamidone (4H- ,(S)-), in or on the commodities: Imidazol-4-one, 3,5-dihydro-5-methyl-2- (methylthio)-5-phenyl-3 (phenylam- Parts per ino)-,(S)-), in or on the commodity: Commodity million Parts per Bean, succulent, except cowpea ...... 0 .80 Commodity million Brassica, head and stem, subgroup 5A ...... 5 .0 Brassica, leafy greens, subgroup 5B ...... 55 Grape1 ...... 1 .0 Cilantro, leaves ...... 60 Cotton, gin byproducts ...... 0 .02 1 Applicable to grapes grown East of the Rocky Mountains. Cotton, undelinted seed ...... 0 .02 Ginseng ...... 0 .80 (d) Indirect or inadvertent residues. Okra ...... 3.5 Tolerances are established for residues Onion, bulb, subgroup 3–07A ...... 0 .20 of the fungicide fenamidone, including Onion, green, subgroup 3–07B ...... 1 .5 Pepper, nonbell ...... 3 .5 its metabolites and degradates, in or Sunflower ...... 0 .02 on the following commodities. Compli- Tomato, paste ...... 2 .2 ance with the tolerance levels is to be Tomato, puree ...... 2 .0 determined by measuring fenamidone Turnip, greens ...... 55 Vegetable, cucurbit, group 9 ...... 0.15 (4H-Imidazol-4-one, 3,5-dihydro-5-meth- Vegetable, fruiting, group 8, except nonbell pep- yl-2-(methylthio)-5-phenyl-3 per ...... 1 .0 (phenylamino)-,(S)-), and its metabo- Vegetable, leafy, except Brassica, group 4 ...... 60 Vegetable, root, except sugar beet, subgroup lite RPA 717879 (2,4-imidazolidinedione, 1B, except radish ...... 0 .15 5-methyl-5-phenyl), in or on the fol- Vegetable, tuberous and corm, subgroup 1C ..... 0.02 lowing commodities when present therein as a result of application of (2) Tolerances are established for res- fenamidone to the crops in paragraph idues of the fungicide fenamidone, in- (a)(1). cluding its metabolites and degradates, in or on the following commodities. Commodity Parts per Compliance with the tolerance levels is million to be determined by measuring Grain, cereal, group 15, except rice ...... 0 .1 fenamidone (4H-Imidazol-4-one, 3,5- Grain, cereal, forage, fodder and straw, group 16, except rice ...... 0 .5 dihydro-5-methyl-2-(methylthio)-5- Soybean, forage ...... 0 .15 phenyl-3 (phenylamino)-,(S)-), and its Soybean, hay ...... 0 .25 metabolite RPA 717879 (2,4- Soybean, seed ...... 0 .02 imidazolidinedione, 5-methyl-5-phenyl), Strawberry ...... 0 .02 in or on the commodities: [67 FR 60976, Sept. 27, 2002, as amended at 69 Commodity Parts per FR 58066, Sept. 29, 2004; 71 FR 55293, Sept. 22, million 2006; 72 FR 60272, Oct. 24, 2007; 74 FR 34257, Cattle, fat ...... 0.10 July 15, 2009; 76 FR 34885, June 15, 2011; 76 FR Cattle, meat ...... 0 .10 70895, Nov. 16, 2011; 77 FR 32401, June 1, 2012; Cattle, meat byproducts ...... 0.10 79 FR 13882, Mar. 12, 2014]

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§ 180.580 Iodosulfuron-Methyl-Sodium; below is to be determined by measuring tolerances for residues. only the sum of pyraclostrobin (car- (a) General. Tolerances are estab- bamic acid, [2-[[[ 1-(4-chlorophenyl)-1H- lished for residues of the herbicide pyrazol-3-yl]oxy] meth- Iodosulfuron-Methyl-Sodium (methyl 4- yl]phenyl]methoxy-, methyl ester) and iodo-2-[3-(4-methoxy-6-methyl-1,3,5 its desmethoxy metabolite (methyl-N- triazin-2-yl)ureidosulfonyl]benzoate, so- [[[1-(4-chlorophenyl)-1H-pyrazol-3- dium salt) in or on the following com- yl]oxy]methyl] phenylcarbamate), cal- modities: culated as the stoichiometric equivalent of pyraclostrobin, in or on the Parts per commodity. Commodity million Parts per Corn, field, forage ...... 0 .05 Commodity million Corn, field, grain ...... 0 .03 Corn, field, stover ...... 0 .05 Alfalfa, forage ...... 10 Wheat, forage ...... 0 .10 Alfalfa, hay ...... 30 Wheat, grain ...... 0 .02 Almond, hulls ...... 7 .0 Wheat, hay ...... 0 .05 Apple, wet pomace ...... 8 .0 Wheat, straw ...... 0 .05 Artichoke, globe ...... 3.0 Avocado ...... 0 .6 (b) Section 18 emergency exemptions. Banana ...... 0.04 [Reserved] Barley, grain ...... 1 .4 Barley, hay ...... 25 (c) Tolerances with regional registra- Barley, straw ...... 6 .0 tions. [Reserved] Bean, succulent shelled ...... 0 .5 (d) Indirect or inadvertent residues. Beet, sugar, dried pulp ...... 1 .0 [Reserved] Beet, sugar, roots ...... 0 .2 Beet, sugar, tops ...... 8.0 [67 FR 57532, Sept. 11, 2002, as amended at 74 Berry, low growing, subgroup 13–07G, except FR 23644, May 20, 2009] cranberry ...... 1.2 Brassica, head and stem, subgroup 5A ...... 5 .0 Brassica, leafy greens, subgroup 5B ...... 16 .0 § 180.581 Iprovalicarb; tolerances for Bushberry subgroup 13–07B ...... 4 .0 residues. Caneberry subgroup 13–07A ...... 4.0 (a) General. Tolerances are estab- Canistel ...... 0 .6 Citrus, dried pulp ...... 12 .5 lished for residues of iprovalicarb, [2- Citrus, oil ...... 9.0 methyl-1[[[(1S)-(4-methylphenyl) ethyl] Coffee, green bean ...... 1 0 .3 amino]carbonyl] propyl]carbamic acid Corn, field, forage ...... 5 .0 Corn, field, grain ...... 0 .1 methylethylester, in or on the fol- Corn, field, refined oil ...... 0 .2 lowing commodities. Corn, field, stover ...... 17 .0 Corn, pop, grain ...... 0.1 Commodity Parts per Corn, pop, stover ...... 17.0 million Corn, sweet, forage ...... 5 .0 Corn, sweet, kernel plus cob with husks re- Grape 1 ...... 2 .0 moved ...... 0 .04 1 Tomato ...... 1.0 Corn, sweet, stover ...... 23.0 1There is no U.S. registration as of September 1, 2005. Cotton, gin byproducts ...... 30 Endive, belgium ...... 4 .0 (b) Section 18 emergency exemptions. Fruit, citrus, group 10–10 ...... 2 .0 [Reserved] Fruit, pome, group 11–10 ...... 1 .5 Fruit, small vine climbing, except fuzzy (c) Tolerances with regional registra- kiwifruit, subgroup 13–07F ...... 2.0 tions. [Reserved] Fruit, stone, group 12 ...... 2 .5 (d) Indirect or inadvertent residues. Grain, aspirated fractions ...... 2 .5 [Reserved] Grape, raisin ...... 7 .0 Grass, forage ...... 10 [67 FR 54359, Aug. 22, 2002, as amended at 70 Grass, hay ...... 4 .5 FR 55281, Sept. 21, 2005] Grass, seed screenings ...... 27 Grass, straw ...... 14 Hop, dried cones ...... 23 .0 § 180.582 Pyraclostrobin; tolerances Mango ...... 0.6 for residues. Nut, tree, group 14 ...... 0 .04 (a) General. (1) Tolerances are estab- Oat, grain ...... 1 .2 Oat, hay ...... 18 lished for residues of the fungicide Oat, straw ...... 15 pyradostrobin, including its metabo- Oilseed group 20 ...... 0 .45 lites and degradates, in or on the com- Papaya ...... 0 .6 Pea, succulent ...... 0 .2 modities in the table below. Compli- Pea and bean, dried shelled, except soybean, ance with the tolerance levels specified subgroup 6C ...... 0 .5

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Parts per Parts per Commodity million Commodity million

Peanut ...... 0 .05 Milk ...... 0.1 Peanut, refined oil ...... 0.1 Poultry, eggs ...... 0 .10 Peppermint, tops ...... 8 .0 Poultry, fat ...... 0.10 Persimmon ...... 3 .0 Poultry, meat ...... 0 .10 Pistachio ...... 0.7 Poultry, meat byproducts ...... 0.10 Radish, tops ...... 16 Sheep, fat ...... 0 .1 Rye, grain ...... 0.04 Sheep, liver ...... 1.5 Rye, straw ...... 0 .5 Sheep, meat ...... 0.1 Sapodilla ...... 0 .6 Sheep, meat byproducts, except liver ...... 0 .2 Sapote, black ...... 0 .6 Sapote, mamey ...... 0 .6 (b) Section 18 emergency exemptions. A Sorghum, grain, forage ...... 5.0 Sorghum, grain, grain ...... 0 .60 time-limited tolerance is established Sorghum, grain, stover ...... 0 .80 for combined residues of the fungicide Soybean, forage ...... 11 pyraclostrobin, (carbamic acid, [2-[[[1- Soybean, hay ...... 14 (4-chlorophenyl)-1H-pyrazol-3- Soybean, hulls ...... 0 .06 Soybean, seed ...... 0 .04 yl]oxy]methyl] phenyl]methoxy-, Spearmint, tops ...... 8 .0 methyl ester) and its desmethoxy me- Star apple ...... 0 .6 tabolite (methyl-N-[[[1-(4- Sugarcane, cane ...... 0.20 Vegetable, bulb, group 3–07 ...... 0 .9 chlorophenyl) pyrazol-3-yl]oxy]o- Vegetable, cucurbit, group 9 ...... 0.5 tolyl]carbamate) in connection with Vegetable, foliage of legume, except soybean, use of the pesticide under section 18 subgroup 7A ...... 25 .0 emergency exemptions granted by Vegetable, fruiting, group 8–10 ...... 1 .4 Vegetable, leafy, except brassica, group 4 ...... 29.0 EPA. The time-limited tolerance will Vegetable, leaves of root and tuber, group 2, expire and is revoked on the date speci- except sugar beet ...... 16 .0 fied in the following table. Vegetable, legume, edible podded, subgroup 6A ...... 0 .5 Expiration/ Vegetable, root, except sugar beet, subgroup Commodity Parts per revocation 1B ...... 0 .4 million date Vegetable, tuberous and corm, subgroup 1C ... 0.04 Vegetables, foliage of legume, group 7 ...... 25 Endive, belgium ...... 11.0 12/31/13 Wheat, grain ...... 0 .02 Wheat, hay ...... 6 .0 (c) Tolerances with regional registra- Wheat, straw ...... 8 .5 tions. [Reserved] (2) Tolerances are established for (d) Indirect or inadvertent residues. combined residues of the fungicide [Reserved] pyraclostrobin carbamic acid, [2-[[[1-(4- [67 FR 60901, Sept. 27, 2002, as amended at 69 chlorophenyl)-1H-pyrazol-3- FR 63100, Oct. 29, 2004; 71 FR 17021, Apr. 5, yl]oxy]methyl]phenyl]methoxy-, meth- 2006; 72 FR 54569, Sept. 26, 2007; 73 FR 15431, yl ester and its metabolites convertible Mar. 24, 2008; 73 FR 21842, Apr. 23, 2008; 73 FR 44167, July 30, 2008; 74 FR 11499, Mar. 18, 2009; to 1-(4-chlorophenyl)-1H-pyrazol-3-ol 74 FR 51496, Oct. 7, 2009; 75 FR 770, Jan. 6, and 1-(4-chloro-2-hydroxyphenyl)-1H- 2010; 75 FR 42329, July 21, 2010; 75 FR 80346, pyrazol-3-ol, expressed as parent com- Dec. 22, 2010; 76 FR 81396, Dec. 28, 2011; 78 FR pound, in or on the following raw agri- 53046, Aug. 28, 2013] cultural commodities. § 180.583 Triticonazole; tolerances for Parts per residues. Commodity million (a) General. Tolerances are estab- Cattle, fat ...... 0.1 lished for residues of the fungicide Cattle, liver ...... 1 .5 Cattle, meat ...... 0 .1 triticonazole, (1RS)-(E)-5-[(4- Cattle, meat byproducts, except liver ...... 0 .2 chlorophenyl)methylene]-2,2-dimethyl- Goat, fat ...... 0 .1 1-(1H-1,2,4-triazol-1- Goat, liver ...... 1.5 ylmethyl)cyclopentanol, from the Goat, meat ...... 0.1 Goat, meat byproducts, except liver ...... 0 .2 treatment of seed prior to planting in Hog, fat ...... 0 .1 or on raw agricultural commodities as Hog, liver ...... 1 .5 follows: Hog, meat ...... 0 .1 Hog, meat byproducts, except liver ...... 0 .2 Parts per Horse, fat ...... 0 .1 Commodity million Horse, liver ...... 0 .1 Horse, meat ...... 0 .1 Grain, cereal, forage, fodder and straw, group Horse, meat byproducts, except liver ...... 0 .2 16, except rice ...... 0 .10

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measuring only the sum of the parent Commodity Parts per million pyraflufen-ethyl, ethyl 2-[2-chloro-5-(4- Grain, cereal, group 15, except rice ...... 0 .01 chloro-5-difluoromethoxy)-1-methyl- 1H-pyrazol-3-yl]-4-fluorophenoxy] ace- (b) Section 18 emergency exemptions. tate and its acid metabolites: E–1, 2- [Reserved] chloro-5-(4-chloro-5-difluoromethoxy-1- (c) Tolerances with regional registra- methyl-1H-pyrazol-3-yl)-4- tions. [Reserved] fluorophenoxyacetic acid, and E–9, 2- (d) Indirect or inadvertent residues. chloro-5-(4-chloro-5-difluoromethoxy- [Reserved] 1H-pyrazol-3-yl)-4-fluorophenoxyacetic [67 FR 60959, Sept. 27, 2002, as amended at 75 acid, both calculated as the stoichio- FR 4288, Jan. 27, 2010] metric equivalent of pyraflufen-ethyl in or on the commodity. § 180.584 Tolylfluanid; tolerances for Parts per residues. Commodity million (a) General. Tolerances are established for residues of tolylfluanid, 1,1- Almond, hulls ...... 0 .02 Cattle, fat ...... 0.03 dichloro-N-[(dimethylamino)-sulfonyl]- Cattle, meat ...... 0 .03 1-fluoro-N-(4- Cattle, meat byproducts ...... 0.03 methylphenyl)methanesulfenamide in Corn, field, forage ...... 0 .01 or on the following commodities. Corn, field, grain ...... 0 .01 Corn, field, stover ...... 0 .01 Parts per Cotton, gin byproducts ...... 1 .5 Commodity million Cotton, undelinted seed ...... 0 .04 Fruit, pome, group 11–10 ...... 0 .01 Apple 1 ...... 5.0 Fruit, stone, group 12 ...... 0 .01 1 Grape ...... 11 Goat, fat ...... 0 .03 1 Hop, dried cones ...... 30 Goat, meat ...... 0.03 Tomato 1 ...... 2.0 Goat, meat byproducts ...... 0 .03 1 No U.S. registration as of August 31, 2002. Grape ...... 0 .01 Grass, forage, group 17 ...... 1 .0 (b) Section 18 emergency exemptions. Grass, hay, group 17 ...... 1 .4 [Reserved] Horse, fat ...... 0 .03 (c) Tolerances with regional registra- Horse, meat ...... 0 .03 tions. [Reserved] Horse, meat byproducts ...... 0 .03 Milk ...... 0.03 (d) Indirect or inadvertent residues. Nut, tree, group 14 ...... 0 .01 [Reserved] Olive ...... 0 .01 Peanut ...... 0 .01 [67 FR 60141, Sept. 25, 2002] Peanut, hay ...... 0.07 Pistachio ...... 0.01 § 180.585 Pyraflufen-ethyl; tolerances Pomegranate ...... 0 .01 for residues. Potato ...... 0 .02 (a) General. Tolerances are estab- Sheep, fat ...... 0 .03 Sheep, meat ...... 0.03 lished for residues of the herbicide, Sheep, meat byproducts ...... 0 .03 pyraflufen-ethyl, including its metabo- Soybean, forage ...... 0 .05 lites and degradates, in the commod- Soybean, hay ...... 0 .10 ities in the table below. Compliance Soybean, seed ...... 0 .01 Wheat, forage ...... 0 .02 with the plant commodity tolerance Wheat, grain ...... 0 .01 levels specified in the table is to be de- Wheat, hay ...... 0 .01 termined by measuring only the sum of Wheat, straw ...... 0 .01 the parent pyraflufen-ethyl, ethyl 2-[2- chloro-5-(4-chloro-5-difluoromethoxy)- (b) Section 18 emergency exemptions. 1-methyl-1H-pyrazol-3-yl]-4- [Reserved] fluorophenoxy] acetate, and its acid (c) Tolerances with regional registra- metabolite, E–1, 2-chloro-5-(4-chloro-5- tions. [Reserved] difluoromethoxy-1-methyl-1H-pyrazol- (d) Indirect or inadvertent residues. 3-yl)-4-fluorophenoxyacetic acid, cal- [Reserved] culated as the stoichiometric equiva- [68 FR 23055, Apr. 30, 2003, as amended at 68 lent of pyraflufen-ethyl in or on the FR 27739, May 21, 2003; 69 FR 26312, May 12, commodity. Compliance with the live- 2004; 73 FR 51743, Sept. 5, 2008; 76 FR 31484, stock commodity tolerance levels spec- June 11, 2011; 77 FR 75861, Dec. 26, 2012; 78 FR ified in the table is to be determined by 13263, Feb. 27, 2013]

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§ 180.586 Clothianidin; tolerances for Expiration/ Commodity Parts per revocation residues. million date (a) General. (1) Tolerances are estab- Rice, seed ...... 0.01 6/23/12 lished for residues of the insecticide clothianidin, including its metabolites (b) Section 18 emergency exemptions. and degradates. Compliance with the [Reserved] tolerance levels specified below is to be (c) Tolerances with regional registra- determined by measuring only tions. [Reserved] clothianidin, (E)-N-[(2-Chloro-5- (d) Indirect and inadvertant residues. thiazolyl)methyl]-N′ -methyl-N″ Tolerances are established for the indi- -nitroguanidine, in or on the following rect or inadvertent residues of the in- raw agricultural commodities: secticide clothianidin, including its metabolites and degradates. Compli- Parts per Commodity million ance with the tolerance levels specified below is to be determined by measuring Almond, hulls ...... 1 .5 only clothianidin, (E)-1-(2-chloro-1,3- Beet, sugar, dried pulp ...... 0 .03 Beet, sugar, molasses ...... 0 .05 thiazol-5-ylmethyl)-3-methyl-2- Beet, sugar, roots ...... 0 .02 nitroguanidine, in or on the following Berry, low-growing, subgroup 13-07H, except raw agricultural commodities when strawberry ...... 0.01 present therein as a result of the appli- Canola, seed ...... 0 .01 Cotton, gin byproducts ...... 4 .5 cation of clothianidin to crops listed in Cotton, undelinted seed ...... 0 .20 paragraph (a) of this section: Fig ...... 0 .05 Fruit, pome ...... 1.0 Commodity Parts per Grain, cereal, forage, fodder and straw, group million 16, except rice, forage ...... 0 .35 Grain, cereal, forage, fodder and straw, group Animal feed, nongrass, group 18 ...... 0 .02 16, except rice, hay ...... 0 .07 Grass, forage, fodder and hay, group 17 ...... 0 .02 Soybean, forage ...... 0 .02 Grain, cereal, forage, fodder and straw, group Soybean, hay ...... 0 .02 16, except rice, stover ...... 0 .1 Grain, cereal, forage, fodder and straw, group 16, except rice, straw ...... 0.05 [74 FR 65028, Dec. 9, 2009, as amended at 76 Grain, cereal, group 15, except rice ...... 0 .01 FR 7718, Feb. 11, 2011; 76 FR 25246, May 4, Grape ...... 0 .60 2011; 76 FR 34886, June 15, 2011; 77 FR 52252, Milk ...... 0.01 Mustard, seed ...... 0 .01 Aug. 29, 2012; 78 FR 19136, Mar. 29, 2013] Nut, tree, group 14 ...... 0 .01 Peach ...... 0 .80 § 180.587 Famoxadone; tolerance for Pepper ...... 0 .80 residues. Pomegranate ...... 0 .20 Potato, chips ...... 0 .6 (a) General. Tolerances are estab- Potato, granules/flakes ...... 1 .5 lished for residues of the fungicide Rice, grain ...... 0 .01 famoxadone (3-anilino-5-methyl-5-(4- Soybean, seed ...... 0 .02 phenoxyphenyl)-1,3-oxazolidine-2,4- Tea, dried 1 ...... 70 Vegetable, brassica, leafy, group 5 ...... 1.9 dione) in or on the following commod- Vegetable, bulb, group 3-07 ...... 0 .45 ities: Vegetable, cucurbit, group 9 ...... 0.06 Vegetable, fruiting, group 8, except pepper ...... 0.20 Commodity Parts per Vegetable, leafy, except brassica, group 4 ...... 3 .0 million Vegetable, root, except sugar beet, subgroup Caneberry subgroup 13–07A ...... 10 1B ...... 0 .8 Cattle, fat ...... 0.02 Vegetable, tuberous and corm, subgroup 1C ..... 0.3 Cattle, liver ...... 0 .05 1 No U.S. registrations. Cilantro, leaves ...... 25 Goat, fat ...... 0 .02 (2) Time-limited tolerances are estab- Goat, liver ...... 0.05 lished for residues of the insecticide Grape, raisin 1 ...... 4 .0 Hop, dried cone ...... 80 clothianidin, including its metabolites Horse, fat ...... 0 .02 and degradates. Compliance with the Horse, liver ...... 0 .05 tolerance levels specified below is to be Milk, fat (reflecting negligible residues in whole milk) ...... 0 .06 determined by measuring only Onion, bulb, subgroup 3–07A ...... 0 .45 clothianidin, (E)-1-(2-chloro-1,3-thiazol- Onion, green, subgroup 3–07B ...... 40 5-ylmethyl)-3-methyl-2-nitroguanidine, Potato ...... 0 .02 Sheep, fat ...... 0 .02 in or on the following raw agricultural Sheep, liver ...... 0.05 commodity: Spinach ...... 50

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(d) Indirect or inadvertent residues. Commodity Parts per million [Reserved] Tomato ...... 1.0 [68 FR 55858, Sept. 29, 2003, as amended at 70 Vegetable, cucurbit, group 9 ...... 0.30 FR 4032, Jan. 28, 2005; 71 FR 50354, Aug. 25, Vegetable, fruiting, group 8, except tomato ...... 4 .0 2006; 74 FR 14743, Apr. 1, 2009; 78 FR 57280, Vegetable, leafy, except Brassica, group 4, except spinach ...... 25 Sept. 18, 2013] 1 There are no U.S. registrations as of May 15, 2003. § 180.589 Boscalid; tolerances for resi- (b) Section 18 emergency exemptions. dues. [Reserved] (a) General. (1) Tolerances are estab- (c) Tolerances with a regional registra- lished for residues of the fungicide tions. Tolerances with a regional reg- boscalid, including its metabolites and istration as defined in § 180.1(l) are es- degradates, in or on the commodities tablished for the residues of the fun- listed below. Compliance with the tol- gicide famoxadone, 3-anilino-5-methyl- erance levels specified below is to be 5-(4-phenoxyphenyl)-1,3-oxazolidine-2,4- determined by measuring only dione) in or on the raw agricultural boscalid, 3-pyridinecarboxamide, 2- commodities: chloro-N-(4′-chloro[1,1’-biphenyl]-2-yl), in or on the following raw agricultural Parts per commodities: Commodity million Parts per Grape ...... 2 .5 Commodity million (d) Indirect or inadvertant residues. Alfalfa, forage ...... 30.0 Alfalfa, hay ...... 65.0 [Reserved] Almond, hulls ...... 17 Apple, wet pomace ...... 10 [68 FR 39471, July 2, 2003, as amended at 72 Artichoke, globe ...... 6.0 FR 28881, May 23, 2007; 74 FR 9364, Mar. 4, Avocado ...... 1 .5 2009; 76 FR 34885, June 15, 2011] Banana, import 1 ...... 0 .40 Berry, low growing, subgroup 13–07G, except § 180.588 Quinoxyfen; tolerances for cranberry ...... 4.5 Brassica, head and stem, subgroup 5A ...... 3 .0 residues. Brassica, leafy greens, subgroup 5B ...... 18 .0 (a) General. Tolerances are estab- Bushberry subgroup 13–07B ...... 13 .0 Caneberry subgroup 13–07A ...... 10.0 lished for residues of the fungicide Canistel ...... 1 .5 quinoxyfen, including its metabolites Canola, refined oil ...... 5 .0 and degradates, in or on the commod- Citrus, dried pulp ...... 4 .5 ities in the following table. Compliance Citrus, oil ...... 85.0 Coffee, green bean, import 1 ...... 0 .05 with the tolerance levels specified in Cotton, gin byproducts ...... 55 .0 the following table is to be determined Cucumber ...... 0 .5 by measuring only quinoxyfen (5,7- Endive, Belgium ...... 6 .0 Fruit, citrus, group 10–10 ...... 2 .0 dichloro-4-(4-fluorophenoxy)quinoline). Fruit, pome, group 11–10 ...... 3 .0 Fruit, small vine climbing, except fuzzy kiwifruit, Commodity Parts per subgroup 13–07F ...... 5 .0 million Fruit, stone, group 12 ...... 3 .5 Grain, aspirated fractions ...... 3 .0 Artichoke, globe ...... 1.4 Grape, raisin ...... 8 .5 Berry, low growing, subgroup 13–07G ...... 1 .0 Hop, dried cones ...... 35 Fruit, small vine climbing, except fuzzy kiwifruit, Leaf petioles subgroup 4B ...... 45 subgroup 13–07F ...... 2 .0 Leafy greens subgroup 4A, except head lettuce Fruit, stone, group 12 ...... 0 .70 and leaf lettuce ...... 60 Hop, dried cones ...... 3 .0 Lettuce, head ...... 6.5 Gourd, edible ...... 0 .20 Lettuce, leaf ...... 11 .0 Lettuce, head ...... 7.0 Mango ...... 1.5 Lettuce, leaf ...... 19 Nut, tree, group 14 ...... 0 .70 Melon, subgroup 9A ...... 0 .08 Oilseed group 20 ...... 3 .5 Pumpkin ...... 0.20 Papya ...... 1 .5 Squash, winter ...... 0 .20 Pea and bean, dried shelled, except soybean, Vegetable, fruiting, group 8–10 ...... 1 .7 subgroup 6C, except cowpea, field pea and grain lupin ...... 2 .5 Pea and bean, succulent shelled, subgroup 6B, (b) Section 18 emergency exemptions. except cowpea ...... 0 .6 [Reserved] Peanut ...... 0 .05 Peanut, meal ...... 0 .15 (c) Tolerances with regional registra- Peanut, refined oil ...... 0.15 tions. [Reserved] Peppermint, tops ...... 30 .0

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gency exemptions granted by EPA. Commodity Parts per million Compliance with the tolerance level Persimmon ...... 8 .0 specified below is to be determined by Pistachio ...... 0.70 measuring only boscalid, 3- Sapodilla ...... 1 .5 ′ Sapote, black ...... 1 .5 pyridinecarboxamide, 2-chloro-N-(4 - Sapote, mamey ...... 1 .5 chloro[1,1’-biphenyl]-2-yl). This toler- Soybean, hulls ...... 0 .2 ance will expire and is revoked on the Soybean, seed ...... 0 .1 Soybean, vegetable ...... 2 .0 date specified in the following table: Spearmint, tops ...... 30 .0 Star apple ...... 1 .5 Parts per Expiration/ Turnip, greens ...... 40.0 Commodity million revocation Vegetable, bulb, group 3–07 ...... 5 .0 date Vegetable, cucurbit, group 9, except cucumber 1.6 Vegetable, fruiting, group 8–10 ...... 3 .0 Endive, Belgian ...... 16 12/31/13 Vegetable, legume, edible podded, subgroup 6A 1 .6 Vegetable, root, subgroup 1A, except sugar (c) Tolerances with regional registra- beet, garden beet, radish, and turnip ...... 1.0 Vegetable, tuberous and corm, subgroup 1C ..... 0.05 tion. [Reserved] 1No US registrations as of September 16, 2009. (d) Indirect or inadvertent residues. Tolerances are established for the indi- (2) Tolerances are established for res- rect or inadvertent residues of the fun- idues of the fungicide boscalid, includ- gicide boscalid, including its metabo- ing its metabolites and degradates, in lites and degradates, in or on the com- or on the commodities listed below. modities listed below. Compliance with Compliance with the tolerance levels the tolerance levels specified below is specified below is to be determined by measuring only the sum of boscalid, 3- to be determined by measuring only pyridinecarboxamide, 2-chloro-N-(4’- boscalid, 3-pyridinecarboxamide, 2- ′ chloro[1,1’-biphenyl]-2-yl), and metabo- chloro-N-(4 -chloro[1,1’-biphenyl]-2-yl), lites 2-chloro-N-(4’-chloro-5-hydroxy- in or on the following commodities: biphenyl-2-yl) nicotinamide and glucu- Parts per ronic acid conjugate of 2-chloro-N-(4′- Commodity million chloro-5-hydroxy-biphenyl-2-yl) nicotinamide, calculated as the stoichio- Animal feed, nongrass, group 18, forage, except alfalfa ...... 1.0 metric equivalent of boscalid in or on Animal feed, nongrass, group 18, hay, except the following food commodities: alfalfa ...... 2.0 Animal feed, nongrass, group 18, seed ...... 0 .05 Parts per Beet, garden, roots ...... 0 .1 Commodity million Beet, sugar, roots ...... 0 .1 Cattle, fat ...... 0.30 Cowpea, seed ...... 0 .1 Cattle, meat ...... 0 .10 Grain, cereal, forage, fodder and straw, group Cattle, meat byproducts ...... 0.35 16, forage ...... 2 .0 Egg ...... 0 .02 Grain, cereal, forage, fodder and straw, group Goat, fat ...... 0 .30 16, stover ...... 1 .5 Goat, meat ...... 0.10 Grain, cereal, forage, fodder and straw, group Goat, meat byproducts ...... 0 .35 16, straw ...... 3 .0 Hog, fat ...... 0 .20 Grain, cereal, group 15 ...... 0.20 Hog, meat ...... 0 .05 Grass, forage, fodder, and hay, group 17, for- Hog, meat byproducts ...... 0 .10 age ...... 2 .0 Horse, fat ...... 0 .30 Grass, forage, fodder, and hay, group 17, hay ... 8 .0 Horse, meat ...... 0 .10 Horse, meat byproducts ...... 0 .35 Grass, forage, fodder, and hay, group 17, seed Milk ...... 0.10 screenings ...... 0 .20 Poultry, fat ...... 0.20 Grass, forage, fodder, and hay, group 17, straw 0 .30 Poultry, meat ...... 0 .05 Lupin, grain, grain ...... 0 .1 Poultry, meat byproducts ...... 0.20 Pea, field, seed ...... 0 .1 Sheep, fat ...... 0 .30 Radish, roots ...... 0 .1 Sheep, meat ...... 0.10 Rice, hulls ...... 0 .50 Sheep, meat byproducts ...... 0 .35 Turnip, roots ...... 0 .1 Vegetable, foliage of legume, group 7, forage .... 1 .5 (b) Section 18 emergency exemptions. Vegetable, foliage of legume, group 7, hay ...... 2 .0 Time-limited tolerances are estab- Vegetable, foliage of legume, group 7, vines ..... 0 .05 lished for residues of the fungicide Vegetable, leafy, except brassica, group 4, ex- boscalid, including its metabolites and cept celery, lettuce and spinach ...... 1 .0 degradates, in connection with use of Vegetable, leaves of root and tuber, group 2 ..... 0 .1 the pesticide under section 18 emer-

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[68 FR 44651, July 30, 2003, as amended at 69 Parts per FR 19774, Apr. 14, 2004; 70 FR 55293, Sept. 21, Commodity million 2005; 71 FR 6364, Feb. 8, 2006; 71 FR 25961, May 3, 2006; 71 FR 76190, Dec. 20, 2006; 73 FR 16558, Fruit, citrus, Group 10 ...... 0.03 Mar. 28, 2008; 74 FR 47445, Sept. 16, 2009; 75 FR Cotton, undelinted seed ...... 0 .05 Cotton, gin byproducts ...... 1 .0 770, Jan. 6, 2010; 75 FR 29907, May 28, 2010; 75 Sugarcane ...... 0 .01 FR 80346, Dec. 22, 2010; 78 FR 67048, Nov. 8, Tomato ...... 0.01 2013] (b) Section 18 emergency exemptions. § 180.590 2, 6-Diisopropylnaphthalene (2, 6-DIPN); tolerances for residues. [Reserved] (c) Tolerances with regional registra- (a) General. Tolerances are estab- tions. [Reserved] lished for residues of the growth inhib- (d) Indirect or inadvertent residues. itor 2,6-DIPN, including its metabolites [Reserved] and degradates, in or on the commodities in the following table. Compliance [68 FR 54386, Sept. 17, 2003] with the tolerance levels specified in the following table is to be determined § 180.592 Butafenacil; tolerances for by measuring only 2,6- residues. Diisopropylnaphthalene. (a) General. (1) Tolerances are established for residues of the herbicide Parts per Commodity million butafenacil, (1,1-dimethyl-2-oxo-2-(2- propenyloxy)ethyl 2-chloro-5-[3,6- Cattle, fat ...... 0.2 dihydro-3-methyl-2,6-dioxo-4- Cattle, meat ...... 0 .02 Cattle, meat byproducts, except fat ...... 0 .02 (trifluoromethyl)-1(2H)-pyrimidinyl] Goat, fat ...... 0 .2 benzoate) in or on the following raw Goat, meat ...... 0.02 agricultural commodities: Goat, meat byproducts, except fat ...... 0 .02 Horse, fat ...... 0 .2 Parts per Horse, meat ...... 0 .02 Commodity million Horse, meat byproducts, except fat ...... 0.02 Milk, fat ...... 0 .02 Cotton, gin byproducts ...... 10 Potato, granules/flakes ...... 5 .5 Cotton, undelinted seed ...... 0 .50 Potato, wet peel ...... 6 .0 Potato, whole ...... 2 .0 Sheep, fat ...... 0 .2 (2) Tolerances are established for res- Sheep, meat ...... 0.02 idues of the herbicide butafenacil, (1,1- Sheep, meat byproducts, except fat ...... 0 .02 dimethyl-2-oxo-2-(2-propenyloxy)ethyl 2-chloro-5-[3,6-dihydro-3-methyl-2,6- (b) Section 18 emergency exemptions. dioxo-4-(trifluoromethyl)-1(2H)- [Reserved] pyrimidinyl] benzoate) and its metabo- (c) Tolerances with regional registra- lite CGA-293731 (1-carboxy-1- tions. [Reserved] methylethyl 2-chloro-5-[3,6-dihydro-3- (d) Indirect or inadvertent residues. methyl-2,6-dioxo-4-(trifluoromethyl)- [Reserved] 1(2H)-pyrimidinyl] benzoate), in or on [71 FR 52011, Sept. 1, 2006, as amended at 74 the following livestock commodities: FR 66579, Dec. 16, 2009; 77 FR 32406, June 1, 2012] Parts per Commodity million

§ 180.591 Trifloxysulfuron; tolerances Cattle, kidney ...... 0 .05 for residues. Cattle, liver ...... 0 .50 (a) General. Tolerances are estab- Goat, kidney ...... 0 .05 lished for residues of the herbicide Goat, liver ...... 0.50 Hog, kidney ...... 0.05 trifloxysulfuron, N-[[(4,6-dimethoxy-2- Hog, liver ...... 0 .50 pyrimidinyl)amino]carbonyl]-3-(2,2,2- Horse, kidney ...... 0 .05 trifluoroethoxy)-2-pyridinesulfonamide Horse, liver ...... 0 .50 in or on the following raw agricultural Sheep, kidney ...... 0.05 commodities. Sheep, liver ...... 0.50

Parts per (b) Section 18 emergency exemptions. Commodity million [Reserved] Almond ...... 0.02 (c) Tolerances with regional registra- Almond, hulls ...... 0 .01 tions. [Reserved]

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(d) Indirect and inadvertant residues. Commodity Parts per [Reserved] million [68 FR 54827, Sept. 19, 2003] Tomato ...... 0.20 1There are no U.S. registrations for use of etoxazole on § 180.593 Etoxazole; tolerances for resi- tangerines as of September 26, 2003. * There are currently no U.S. registrations for tea as of April dues. 13, 2011. (a) General. Tolerances are estab- (b) Section 18 emergency exemptions. lished for residues of etoxazole, includ- [Reserved] ing its metabolites and degradates, in (c) Tolerances with regional registra- or on the commodities in the table tions. [Reserved] below. Compliance with the tolerance (d) Indirect and inadvertant residues. levels specified below is to be deter- [Reserved] mined by measuring only etoxazole (2- (2,6-difluorophenyl)-4-[4-(1,1- [68 FR 55493, Sept. 26, 2003, as amended at 70 dimethylethyl)-2-ethoxyphenyl]-4,5- FR 41625, July 20, 2005; 72 FR 72963, Dec. 26, 2007; 74 FR 25160, May 27, 2009; 76 FR 20542, dihydrooxazole) in or on the com- Apr. 13, 2011; 77 FR 3621, Jan. 25, 2012] modity. § 180.594 Thiacloprid; tolerances for Parts per Commodity million residues. (a) General. Tolerances are estab- Almond, hulls ...... 2 .0 Apple, wet pomace ...... 0 .50 lished for residues of the insecticide Avocado ...... 0 .20 thiacloprid, including its metabolites Berry, low growing, subgroup 13–07G ...... 0 .50 and degradates in or on the commod- Caneberry subgroup 13–07A ...... 1.5 ities in the following table. Compliance Canistel ...... 0 .20 with the tolerance levels specified in Cattle, fat ...... 0.02 Cattle, liver ...... 0 .01 the following table is to be determined Corn, field, forage ...... 0 .80 by measuring only thiacloprid ([3-[(6- Corn, field, grain ...... 0 .01 chloro-3-pyridinyl)methyl]-2- Corn, field, refined oil ...... 0 .03 thiazolidinylidene] cyanamide) in or on Corn, field, stover ...... 4 .0 Corn, pop, grain ...... 0.01 the commodity. Corn, pop, stover ...... 4.0 Cotton, gin byproducts ...... 1 .0 Commodity Parts per Cotton, undelinted seed ...... 0 .05 million Fruit, pome, group 11 ...... 0.20 Apple, wet pomace ...... 0 .60 Fruit, small vine climbing, except fuzzy kiwifruit, Cattle, fat ...... 0.020 subgroup 13–07F ...... 0 .50 Cattle, kidney ...... 0 .050 Fruit, stone, group 12, except plum ...... 1 .0 Cattle, liver ...... 0 .15 Goat, fat ...... 0 .02 Cattle, meat ...... 0 .030 Goat, liver ...... 0.01 Cattle, meat byproducts ...... 0.050 Grape, raisin ...... 1 .5 Cherry subgroup 12–12A ...... 0 .5 Hop, dried cones ...... 7 .0 Cotton, gin byproducts ...... 11 .0 Horse, fat ...... 0 .02 Cotton, undelinted seed ...... 0 .020 Horse, liver ...... 0 .01 Fruit, pome, group 11 ...... 0.30 Mango ...... 0.20 Goat, fat ...... 0 .020 Melon subgroup 9A ...... 0 .20 Goat, kidney ...... 0 .050 Milk, fat ...... 0 .01 Goat, liver ...... 0.15 Nut, tree, group 14 ...... 0 .01 Goat, meat ...... 0.030 Papaya ...... 0 .20 Goat, meat byproducts ...... 0 .050 Pepper/eggplant subgroup 8–10B ...... 0 .20 Horse, fat ...... 0 .020 Peppermint, oil ...... 20 Horse, kidney ...... 0 .050 Peppermint, tops ...... 10 Horse, liver ...... 0 .15 Pistachio ...... 0.01 Horse, meat ...... 0 .030 Plum ...... 0 .15 Horse, meat byproducts ...... 0 .050 Plum, prune, dried ...... 0.30 Milk ...... 0.030 Sapodilla ...... 0 .20 Peach subgroup 12–12B ...... 0.5 Pepper ...... 1 .0 Sapote, black ...... 0 .20 Plum subgroup 12–12C ...... 0 .05 Sapote, mamey ...... 0 .20 Sheep, fat ...... 0 .020 Sheep, fat ...... 0 .02 Sheep, kidney ...... 0.050 Sheep, liver ...... 0.01 Sheep, liver ...... 0.15 Spearmint, oil ...... 20 Sheep, meat ...... 0.030 Spearmint, tops ...... 10 Sheep, meat byproducts ...... 0 .050 Squash/cucumber subgroup 9B ...... 0.02 Star apple ...... 0 .20 Tangerine 1 ...... 0 .10 (b) Section 18 emergency exemptions. Tea, dried * ...... 15 [Reserved]

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(c) Tolerances with regional registra- thiazolidinyl)phosphonothioate, and its tions. [Reserved] metabolite, O-ethyl S-(1- (d) Indirect or inadvertent residues. methylpropyl)(2- [Reserved] (methylsulfonyl)ethyl) [68 FR 55512, Sept. 26, 2003, as amended at 78 phosphoramidothioate, calculated as FR 8416, Feb. 6, 2013] the stoichiometric equivalent of fosthiazate, in or on the commodity. § 180.595 Flufenpyr-ethyl; tolerances Parts per for residues. Commodity million (a) General. (1) Tolerances are established for residues of the herbicide, Tomato ...... 0.02 flufenpyr-ethyl; acetic acid, [2-chloro- (b) Section 18 emergency exemptions. 4-fluoro-5-[5-methyl-6-oxo-4- [Reserved] (trifluoromethyl)-1-(6H)-pyridazinyl]- (c) Tolerances with regional registra- phenoxy]-ethyl ester], in or on the fol- tions. [Reserved] lowing commodities: (d) Indirect or inadvertent residues. Parts per [Reserved] Commodity million [69 FR 18275, Apr. 7, 2004, as amended at 76 Corn, field, grain ...... 0 .01 FR 23498, Apr. 27, 2011] Soybean, seed ...... 0 .01 Sugarcane, cane ...... 0.01 § 180.597 Mesosulfuron-methyl; tolerances for residues. (2) Tolerances are established for residues of the herbicide flufenpyr-ethyl; (a) General. Tolerances are estab- acetic acid, [2-chloro-4-fluoro-5-[5- lished for residues of the herbicide methyl-6-oxo-4-(trifluoromethyl)-1- mesosulfuron-methyl, (methyl 2- (6H)-pyridazinyl]-phenoxy]-ethyl [[[[(4,6-dimethoxy-2-pyrimidinyl) ester], and its metabolite, S-3153 acid- amino]carbonyl]amino]sulfonyl] -4- 4-OH; [2-chloro-4-hydroxy-5-[5-methyl- [[(methylsulfonyl)amino] meth- 6- oxo-4-(trifluoromethyl)-1-(6H)- yl]benzoate]) in or on the following raw pyridazinyl]-phenoxy]-acetic acid, free agricultural commodities: and conjugated, in or on the following Parts per commodities: Commodity million

Parts per Cattle, meat byproducts ...... 0.01 Commodity million Goat, meat byproducts ...... 0 .01 Grain, aspirated fractions ...... 0 .60 Corn, field, forage ...... 0 .05 Horse, meat byproducts ...... 0 .01 Corn, field, stover ...... 0 .05 Sheep, meat byproducts ...... 0 .01 Wheat, forage ...... 0 .60 (b) Section 18 emergency exemptions. Wheat, germ ...... 0 .10 Wheat, grain ...... 0 .03 [Reserved] Wheat, hay ...... 0 .06 (c) Tolerances with regional registra- Wheat, straw ...... 0 .30 tions. [Reserved] (d) Indirect or inadvertent residues. (b) Section 18 emergency exemptions. [Reserved] [Reserved] (c) Tolerances with regional registra- [68 FR 54842, Sept. 19, 2003] tions. [Reserved] § 180.596 Fosthiazate; tolerances for (d) Indirect or inadvertent residues. residues. [Reserved] (a) General. A tolerance is established [69 FR 18263, Apr. 7, 2004] for residues of the insecticide fosthiazate, including its metabolites § 180.598 Novaluron; tolerances for and degradates, in or on the com- residues. modity in the table in this paragraph. (a) General. Tolerances are estab- Compliance with the tolerance level lished for residues of the insecticide specified in this paragraph is to be de- novaluron, including its metabolites termined by measuring only the sum of and degradates, in or on the following fosthiazate, O-ethyl S-(1- commodities. Compliance with the tol- methylpropyl)(2-oxo-3- erance levels specified in the following

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table is to be determined by measuring Commodity Parts per only novaluron, (N-[[[3-chloro-4-[1,1,2- million trifluoro-2- (trifluoromethoxy)ethoxy] Sheep, liver ...... 1.0 phenyl]amino]carbonyl]-2,6- Sheep, meat ...... 0.60 difluorobenzamide), in or on the fol- Sheep, meat byproducts, except kidney and liver ...... 11 lowing raw agricultural commodities: Sorghum, grain, forage ...... 6.0 Sorghum, grain, grain ...... 3 .0 Commodity Parts per Sorghum, grain, stover ...... 40 million Soybean, seed ...... 0 .07 Sugarcane, cane ...... 0.50 Apple, wet pomace ...... 8 .0 Sunberry ...... 1.0 Bean, dry, seed ...... 0 .30 Swiss chard ...... 12 Bean, snap, succulent ...... 0 .60 Tomato, bush ...... 1 .0 Berry, low growing, subgroup 13-07G, except Tomato, currant ...... 1 .0 lowbush blueberry ...... 0 .45 Tomato, tree ...... 1 .0 Brassica, head and stem, subgroup 5A ...... 0 .50 Turnip, greens ...... 25 Brassica, leafy greens, subgroup 5B ...... 25 Vegetable, cucurbit, group 9 ...... 0.15 Bushberry subgroup 13-07B ...... 7 .0 Vegetable, fruiting, group 8 ...... 1.0 Cattle, fat ...... 11 Vegetable, tuberous and corm, subgroup 1C ..... 0.05 Cattle, kidney ...... 1 .0 Cattle, liver ...... 1 .0 Cattle, meat ...... 0 .60 (b) Section 18 emergency exemptions. Cattle, meat byproducts, except kidney and liver 11 [Reserved] Cherry ...... 8.0 Cocona ...... 1 .0 (c) Tolerances with regional registra- Corn, sweet, forage ...... 16 tions. [Reserved] Corn, sweet, kernel plus cob with husks re- (d) Indirect or inadvertant residues. moved ...... 0 .05 [Reserved] Corn, sweet, stover ...... 50 Cotton, gin byproducts ...... 30 [69 FR 31021, June 2, 2004, as amended at 71 Cotton, undelinted seed ...... 0 .60 FR 17014, Apr. 5, 2006; 71 FR 61911, Oct. 20, Egg ...... 1 .5 Eggplant, African ...... 1 .0 2006; 73 FR 74982, Dec. 10, 2008; 74 FR 637, Jan. Eggplant, pea ...... 1 .0 7, 2009; 74 FR 20891, May 6, 2009; 74 FR 65033, Eggplant, scarlet ...... 1 .0 Dec. 9, 2009; 75 FR 4278, Jan. 27, 2010; 75 FR Food commodities and feed commodities (other 29447, May 26, 2010; 76 FR 55814, Sept. 9, 2011; than those covered by a higher tolerance as a 78 FR 40033, July 3, 2013] result of use on growing crops) in food and feed handling establishments ...... 0 .01 Fruit, pome, group 11 ...... 2.0 § 180.599 Acequinocyl; tolerances for Fruit, stone, group 12, except cherry ...... 1 .9 residues. Goat, fat ...... 11 (a) General. Tolerances are estab- Goat, kidney ...... 1 .0 Goat, liver ...... 1.0 lished for residues of acequinocyl, in- Goat, meat ...... 0.60 cluding its metabolites and degradates, Goat, meat byproducts, except kidney and liver 11 in or on the commodities in the table Goji berry ...... 1 .0 Grain, aspirated fractions ...... 25 below. Compliance with the tolerance Hog, fat ...... 1 .5 levels specified below is to be deter- Hog, kidney ...... 0.10 mined by measuring only the sum of Hog, liver ...... 0 .10 Hog, meat ...... 0 .07 acequinocyl [2-(acetyloxy)-3-dodecyl- Hog, meat byproducts, except kidney and liver .. 1 .5 1,4-naphthalenedione] and its metabo- Horse, fat ...... 11 lite, 2-dodecyl-3-hydroxy-1,4- Horse, kidney ...... 1 .0 naphthoquinone, calculated as the stoi- Horse, liver ...... 1 .0 Horse, meat ...... 0 .60 chiometric equivalent of acequinocyl, Horse, meat byproducts, except kidney and liver 11 in or on the commodity. Huckleberry, garden ...... 1 .0 Martynia ...... 1 .0 Parts per Milk ...... 1.0 Commodity million Milk, fat ...... 20 Naranjilla ...... 1.0 Almond, hulls ...... 2 .0 Okra ...... 1.0 Apple, wet pomace ...... 1 .0 Peanut ...... 0 .01 Bean, edible podded ...... 0 .25 Plum, prune, dried ...... 2.6 Bean, succulent shelled ...... 0 .30 Poultry, fat ...... 7.0 Berry, low growing, subgroup 13–07G ...... 0 .50 Poultry, kidney ...... 0 .80 Caneberry subgroup 13–07A ...... 4.0 Poultry, liver ...... 0 .80 Cattle, fat ...... 0.02 Poultry, meat ...... 0 .40 Cattle, meat byproducts ...... 0.02 Poultry, meat byproducts, except kidney and Cherry, sweet ...... 0 .50 liver ...... 7 .0 Cherry, tart ...... 1 .0 Roselle ...... 1 .0 Citrus, oil ...... 30 Sheep, fat ...... 11 Cowpea, forage ...... 6 .0 Sheep, kidney ...... 1.0 Cowpea, hay ...... 18

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Parts per Parts per Commodity million Commodity million

Cucumber ...... 0 .15 Cattle, meat ...... 0 .05 Fruit, citrus, group 10 ...... 0 .20 Cattle, meat byproducts ...... 0.3 Fruit, pome, group 11 ...... 0.40 Goat, meat ...... 0.05 Fruit, small vine climbing, except fuzzy kiwifruit, Goat, meat byproducts ...... 0 .3 subgroup 13–07F ...... 1 .6 Horse, meat ...... 0 .05 Goat, fat ...... 0 .02 Horse, meat byproducts ...... 0 .3 Goat, meat byproducts ...... 0 .02 Milk ...... 0.03 Sheep, meat ...... 0.05 Hop, dried cones ...... 4 .0 Sheep, meat byproducts ...... 0 .3 Horse, fat ...... 0 .02 Horse, meat byproducts ...... 0 .02 Melon subgroup 9A ...... 0 .15 (b) Section 18 emergency exemptions. Nut, tree, group 14 ...... 0 .02 [Reserved] Okra ...... 0.70 (c) Tolerances with regional registra- Pistachio ...... 0.02 tions. [Reserved] Sheep, fat ...... 0 .02 Sheep, meat byproducts ...... 0 .02 (d) Indirect or inadvertent residues. Soybean, vegetable, succulent ...... 0 .25 [Reserved] Vegetable, fruiting, group 8 ...... 0.70 [69 FR 40781, July 7, 2004, as amended at 71 FR 52487, Sept. 6, 2006; 74 FR 9377, Mar. 4, (b) Section 18 emergency exemptions. 2009] [Reserved] (c) Tolerances with regional registra- § 180.601 Cyazofamid; tolerances for tions. [Reserved] residues. (d) Indirect or inadvertent residues. (a) General. Tolerances are estab- [Reserved] lished for residues of the fungicide [69 FR 43533, July 21, 2004, as amended at 73 cyazofamid, including its metabolites FR 17910, Apr. 2, 2008; 75 FR 70148, Nov. 17, and degradates, in or on the commod- 2010; 77 FR 25909, May 2, 2012] ities in the following table. Compliance with the tolerance levels specified in § 180.600 Propoxycarbazone; toler- the following table is to be determined ances for residues. by measuring only the sum of 4-chloro- (a) General. (1) Tolerances are estab- 2-cyano-N,N-dimethyl-5-(4- lished for combined residues of the her- methylphenyl)-1H-imidazole-1-sul- bicide propoxycarbazone methyl 2- fonamide and its metabolite, 4-chloro- [[[(4,5-dihydro-4-methyl-5-oxo-3- 5-(4-methylphenyl)-1H-imidazole-2- propoxy-1H-1,2,4-triazol-1- carbonitrile, calculated as the stoichio- yl)carbonyl]amino]sulfonyl]benzoate metric equivalent of cyazofamid, in or and its metabolite methyl 2-[[[(4,5- on the following commodities: dihydro-3-(2-hydroxypropoxy)-4-meth- Parts per yl-5-oxo-1H-1,2,4-triazol-1- Commodity million yl)carbonyl]amino]sulfonyl]benzoate in/on the following raw agricultural Basil, dried leaves ...... 90 Basil, fresh leaves ...... 30 commodities: Bean, succulent ...... 0 .5 Bean, succulent shelled ...... 0 .08 Commodity Parts per Brassica, head and stem, subgroup 5A ...... 1 .2 million Brassica, leafy greens, subgroup 5B ...... 12 .0 Carrot, roots ...... 0.09 Grass, forage ...... 20 Hop dried cones ...... 10.0 Grass, hay ...... 25 Leafy greens subgroup 4A ...... 10 Wheat, forage ...... 17 Turnip, greens ...... 12.0 Wheat, grain ...... 0 .02 Vegetable, cucurbit, group 9 ...... 0.10 Wheat, hay ...... 0 .15 Vegetable, fruiting, group 8–10 ...... 0 .9 Wheat, straw ...... 0 .05 Vegetable, tuberous and corm, subgroup 1C ..... 0.02

(2) Tolerances are established for res- (b) Section 18 emergency exemptions. idues of the herbicide Time-limited tolerances are estab- propoxycarbazone methyl 2-[[[(4,5- lished for residues of the fungicide dihydro-4-methyl-5-oxo-3-propoxy-1H- cyazofamid, including its metabolites 1,2,4-triazol-1- and degradates, in or on the commod- yl)carbonyl]amino]sulfonyl]benzoate ities in the following table. Compliance in/on the following raw agricultural with the tolerance levels specified in commodities: the following table is to be determined

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by measuring only the sum of methanamine) in or on the commod- cyazofamid, 4-chloro-2-cyano-N,N-di- ities. methyl-5-(4-methylphenyl)-1H-imid- Parts per azole-1-sulfonamide and its metabolite Commodity million CCIM, 4-chloro-5-(4-methylphenyl)-1H- imidazole-2-carbonitrile, calculated as Artichoke, globe, import 1 ...... 0 .7 Asparagus 1 ...... 0.05 the stoichiometric equivalent of Banana (import) ...... 3 .0 cyazofamid, resulting from use of the Grape (import) ...... 1 .0 pesticide under FIFRA section 18 emer- Hop, dried cones ...... 50 Vegetable, fruiting , crop group 8 1 ...... 1 .2 gency exemptions. The tolerances expire and are revoked on the date speci- 1 No U.S. registration as of December 1, 2010. fied in the table. (b) Section 18 emergency exemptions. [Reserved] Expiration/ (c) Tolerances with regional registra- Commodity Parts per revocation million date tions. [Reserved] (d) Indirect or inadvertent residues. Basil, dried ...... 144 12/31/14 [Reserved] (c) Tolerances with regional registra- [69 FR 42570, July 16, 2004, as amended at 75 tions. Tolerances with regional reg- FR 74640, Dec. 1, 2010] istrations are established for residues § 180.603 Dinotefuran; tolerances for of the fungicide cyazofamid, including residues. its metabolites and degradates, in or on the commodities in the following (a) General. (1) Tolerances are estab- table. Compliance with the tolerance lished for residues of dinotefuran, (RS)- levels specified in the following table is 1-methyl-2-nitro-3-((tetrahydro-3- to be determined by measuring only furanyl)methyl)guanidine, including the sum of 4-chloro-2-cyano-N,N-di- its metabolites and degradates, in or methyl-5-(4-methylphenyl)-1H-imid- on the commodities listed in the fol- azole-1-sulfonamide and its metabolite, lowing table. Compliance with the tol- 4-chloro-5-(4-methylphenyl)-1H-imid- erance levels specified below is to be azole-2-carbonitrile, calculated as the determined by measuring only the sum stoichiometric equivalent of of dinotefuran and its metabolites DN, cyazofamid, in or on the following 1-methyl-3-(tetrahydro-3- commodities: furylmethyl)guanidine, and UF, 1- methyl-3-(tetrahydro-3- furylmethyl)urea, calculated as the Commodity Parts per million stoichiometric equivalent of Grape ...... 1 .5 dinotefuran, in or on the commodities listed in the table below:

(d) Indirect or inadvertent residues. Parts per [Reserved] Commodity million [69 FR 58299, Sept. 30, 2004, as amended at 73 Berry, low growing, except strawberry, subgroup FR 21839, Apr. 23, 2008; 74 FR 32453, July 8, 13–07H ...... 0 .2 2009; 75 FR 40751, July 14, 2010; 77 FR 4252, Brassica, head and stem, subgroup 5A ...... 1 .4 Brassica, leafy greens, subgroup 5B ...... 15 .0 Jan. 27, 2012; 77 FR 59119, Sept. 26, 2012] Cotton, undelinted seed ...... 0 .4 Cotton, gin byproducts ...... 8 .0 § 180.602 Spiroxamine; tolerances for Fruit, small vine climbing, except fuzzy kiwifruit, residues. subgroup 13–07F ...... 0 .9 Grape, raisin ...... 2 .5 (a) General. Tolerances are estab- Onion, bulb, subgroup 3–07A ...... 0 .15 lished for residues of the fungicide Onion, green, subgroup 3–07B ...... 5 .0 Peach ...... 1 .0 spiroxamine, including its metabolites Potato, chips ...... 0 .1 and degradates, in or on the commod- Potato, granules/flakes ...... 0 .15 ities in the table below. Compliance Rice, grain ...... 9 .0 Tea, dried1 ...... 50 with the tolerance levels specified in Tomato, paste ...... 1 .0 the following table is to be determined Turnip, greens ...... 15.0 by measuring only spiroxamine, [(8- Vegetable, fruiting, group 8 ...... 0.7 Vegetable, cucurbit, group 9 ...... 0.5 (1,1-dimethylethyl)-N-ethyl-N-propyl- Vegetable, leafy, except Brassica, group 4 ...... 5 .0 1,4-dioxaspiro[4,5]decane-2- Vegetable, tuberous and corm, subgroup 1C ..... 0.05

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resulting from use of the pesticide pur- Commodity Parts per million suant to FIFRA section 18 emergency Watercress ...... 8 .0 exemptions. Compliance with the tolerance levels specified below is to be de- 1 There are no U.S. registrations for tea. termined by measuring only the sum of (2) Tolerances are established for res- dinotefuran and its metabolites DN, 1- idues of dinotefuran, (RS)-1-methyl-2- methyl-3-(tetrahydro-3- nitro-3-((tetrahydro-3- furylmethyl)guanidine, and UF, 1- furanyl)methyl)guanidine, including methyl-3-(tetrahydro-3- its metabolites and degradates, in or furylmethyl)urea, calculated as the on the commodities listed in the fol- stoichiometric equivalent of lowing table. Compliance with the tol- dinotefuran, in or on the commodities erance levels specified below is to be listed in the table below. The toler- determined by measuring only the sum ances expire and are revoked on the of dinotefuran, (RS)-1-methyl-2-nitro-3- dates specified in the table. ((tetrahydro-3- furanyl)methyl)guanidine in or on the Expiration/ Commodity Parts per revocation commodities listed in the table below: million date

Commodity Parts per Fruit, pome, Group 11 ...... 2.0 12/31/15 million Fruit, stone, Group 12 ...... 2.0 12/31/15 Cattle, fat ...... 0.05 Cattle, meat ...... 0 .05 (c) Tolerances with regional registra- Cattle, meat byproducts ...... 0.05 tions. [Reserved] Egg ...... 0 .01 (d) Indirect or inadvertent residues. Goat, fat ...... 0 .05 Goat, meat ...... 0.05 [Reserved] Goat, meat byproducts ...... 0 .05 Hog, fat ...... 0 .05 [70 FR 14546, Mar. 23, 2005, as amended at 74 Hog, meat ...... 0 .05 FR 12601, Mar. 25, 2009; 74 FR 67104, Dec. 18, Hog, meat byproducts ...... 0 .05 2009; 75 FR 770, Jan. 6, 2010; 77 FR 56138, Sept. Horse, fat ...... 0 .05 12, 2012; 77 FR 67285, Nov. 9, 2012; 77 FR 70913, Horse, meat ...... 0 .05 Nov. 28, 2012; 78 FR 21272, Apr. 10, 2013; 78 FR Horse, meat byproducts ...... 0 .05 Milk ...... 0.05 24683, Apr. 26, 2013; 79 FR 3512, Jan. 22, 2014] Poultry, meat byproducts ...... 0.01 Sheep, fat ...... 0 .05 § 180.604 Mepanipyrim; tolerances for Sheep, meat ...... 0.05 residues. Sheep, meat byproducts ...... 0 .05 (a) General. [Reserved] (3) A tolerance of 0.01 parts per mil- (b) Section 18 emergency exemptions. lion is established for residues of the [Reserved] insecticide dinotefuran, (RS)-1-methyl- (c) Tolerances with regional registra- 2-nitro-3-((tetrahydro-3- tions. [Reserved] furanyl)methyl)guanidine, including (d) Indirect of inadvertent residues. its metabolites and degradates, in or [Reserved] on all food and/or feed commodities (e) Revoked tolerances subject to the (other than those covered by a higher channel of trade provisions. [Reserved] tolerance as a result of use on growing (f) Import tolerances. Tolerances are crops or inadvertent residues) when established for the combined residues residues result from application of of mepanipyrim, 4-methyl-N-phenyl-6- dinotefuran in food and/or feed han- (1-propynyl)-2-pyrimidinamine, and its dling establishments where food and/or metabolite, 4-methyl-N-phenyl-6-(2- feed products are held, stored, proc- hydroxypropylk)-2-pyrimidinamine, essed, prepared, or served. Compliance both free and conjugated in or on the with the tolerance level is to be deter- following commodities: mined by measuring only dinotefuran. Parts per (b) Section 18 emergency exemptions. Commodity million Time-limited tolerances are estab- Grape ...... 1 .5 lished for residues of dinotefuran, (RS)- Grape, raisin ...... 3 .0 1-methyl-2-nitro-3-((tetrahydro-3- Strawberry ...... 1 .5 furanyl)methyl)guanidine, including Tomato ...... 0.5 its metabolites and degradates, in or on the commodities in the table below [68 FR 60827, Oct. 13, 2004]

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§ 180.605 Penoxsulam; tolerances for Commodity Parts per residues. million (a) General. Tolerances are estab- Corn, field, stover ...... 8 .0 lished for the herbicide, penoxsulam (2- Corn, pop, grain ...... 0.02 Corn, pop, stover ...... 4.0 (2,2-difluoroethoxy)-N-(5,8- Corn, sweet, forage ...... 17 dimethoxy[1,2,4] triazolo[1,5- Corn, sweet, kernel plus cob with husks re- c]pyrimidin-2-yl)-6- moved ...... 0 .02 (trifluoromethyl)benzenesulfonamide) Corn, sweet, stover ...... 12 Cotton, gin byproducts ...... 15 in/on the following raw agricultural Cotton, undelinted seed ...... 0 .50 commodities: Cowpea, forage ...... 30 Cowpea, hay ...... 86 Commodity Parts per Leaf petiole subgroup 4B ...... 6 .0 million Leafy greens subgroup 4A ...... 12 Pea, dry, seed ...... 0 .20 Almond, hulls ...... 0 .01 Peppermint, tops ...... 45 Fish ...... 0 .01 Spearmint, tops ...... 45 Fish, shellfish, crustacean ...... 0 .01 Fish, shellfish, mollusc ...... 0 .02 Tea, dry ...... 40 Grape ...... 0 .01 Tomato, paste ...... 0 .80 Nut, tree, group 14 ...... 0 .01 Vegetable, cucurbit, group 9 ...... 0.10 Pistachio ...... 0.01 Vegetable, fruiting, group 8 ...... 0.45 Rice, grain ...... 0 .02 Vegetable, tuberous and corm, subgroup 1C ..... 0.02 Rice, straw ...... 0 .50 (2) Tolerances are established for res- (b) Section 18 emergency exemptions. idues of the insecticide/miticide [Reserved] spiromesifen, including its metabolites (c) Tolerances with regional registra- and degradates, in or on the commod- tions. [Reserved] ities listed below. Compliance with the (d) Indirect or inadvertent residues. tolerance levels specified below is to be [Reserved] determined by measuring only the sum [69 FR 57197, Sept. 24, 2004, as amended at 72 of spiromesifen [2-oxo-3-(2,4,6- FR 40763, July 25, 2007; 74 FR 18648, Apr. 24, trimethylphenyl)-1-oxaspiro[4.4]non-3- 2009] en-4-yl 3,3-dimethylbutanoate] and its metabolites containing the 4-hydroxy- § 180.607 Spiromesifen; tolerances for 3-(2,4,6-trimethylphenyl)-1- residues. oxaspiro[4.4]non-3-en-2-one and 4-hy- (a) General. (1) Tolerances are estab- droxy-3-[4-(hydroxymethyl)-2,6- lished for residues of the insecticide/ dimethylphenyl]-1-oxaspiro[4.4]non-3- miticide spiromesifen, including its en-2-one moieties, calculated as the metabolites and degradates, in or on stoichiometric equivalent of the commodities listed below. Compli- spiromesifen, in the following livestock ance with the tolerance levels specified commodities: below is to be determined by measuring Parts per only the sum of spiromesifen [2-oxo-3- Commodity million (2,4,6-trimethylphenyl)-1- oxaspiro[4.4]non-3-en-4-yl 3,3- Cattle, fat ...... 0.10 Cattle, meat ...... 0 .02 dimethylbutanoate] and 4-hydroxy-3- Cattle, meat byproducts ...... 0.20 (2,4,6-trimethylphenyl)-1- Goat, fat ...... 0 .10 oxaspiro[4.4]non-3-en-2-one, calculated Goat, meat ...... 0.02 as the stoichiometric equivalent of Goat, meat byproducts ...... 0 .20 Horse, fat ...... 0 .10 spiromesifen, in or on the following Horse, meat ...... 0 .02 primary crop commodities: Horse, meat byproducts ...... 0 .20 Milk ...... 0.01 Milk, fat ...... 0 .25 Commodity Parts per million Sheep, fat ...... 0 .10 Sheep, meat ...... 0.02 Bean, dry ...... 0.02 Sheep, meat byproducts ...... 0 .20 Bean, edible podded ...... 0 .80 Bean, succulent ...... 0 .10 Berry and small fruit, low growing berry, sub- (b) Section 18 emergency exemptions. group 13-07G ...... 2 .0 Time-limited tolerances specified in Brassica, head and stem, subgroup 5A ...... 2 .0 the following table are established for Brassica, leafy greens, subgroup 5B ...... 12 Corn, field, forage ...... 5 .0 residues of the insecticide/miticide Corn, field, grain ...... 0 .02 spiromesifen, including its metabolites

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and degradates, in or on the commod- Commodity Parts per ities listed below. Compliance with the million tolerance levels specified below is to be Wheat, straw ...... 0 .25 determined by measuring only the sum of spiromesifen [2-oxo-3-(2,4,6- trimethylphenyl)-1-oxaspiro[4.4]non-3- [70 FR 43283, July 27, 2005, as amended at 72 FR 3079, Jan. 24, 2007; 73 FR 13140, Mar. 12, en-4-yl 3,3-dimethylbutanoate] and 4- 2008; 73 FR 52606, Sept. 10, 2008; 74 FR 8492, hydroxy-3-(2,4,6-trimethylphenyl)-1- Feb. 25, 2009; 74 FR 15886, Apr. 8, 2009; 75 FR oxaspiro[4.4]non-3-en-2-one, calculated 5526, Feb. 3, 2010; 75 FR 53586, Sept. 1, 2010; 76 as the stoichiometric equivalent of FR 81396, Dec. 28, 2011; 78 FR 3337, Jan. 16, spiromesifen, in or on the specified ag- 2013] ricultural commodities, resulting from use of the pesticide pursuant to FIFRA § 180.608 Spirodiclofen; tolerances for section 18 emergency exemptions. The residues. tolerances expire and are revoked on (a) General. (1) Tolerances are estab- the date specified in the table. lished for residues of spirodiclofen, including its metabolites and degradates, Parts per Expiration/ Commodity million revocation in or on the commodities listed below. date Compliance with the following toler- Soybean, forage ...... 30 12/31/14 ance levels is to be determined by Soybean, hay ...... 86 12/31/14 measuring only spirodiclofen (3-(2,4- Soybean, seed ...... 0.02 12/31/14 dichlorophenyl)-2-oxo-1- (c) Tolerances with regional registra- oxaspiro[4.5]dec-3-en-4-yl 2,2- tions. [Reserved] dimethylbutanoate). (d) Indirect or inadvertent residues. Parts per Tolerances are established for the inad- Commodity million vertent or indirect residues of the insecticide/miticide spiromesifen, includ- Almond, hulls ...... 20 .0 Apple, wet pomace ...... 2 .4 ing its metabolites and degradates, in Avocado ...... 1 .0 or on the commodities listed below. Black sapote ...... 1 .0 Compliance with the tolerance levels Canistel ...... 1 .0 specified below is to be determined by Citrus, juice ...... 0 .60 measuring only the sum of Citrus, oil ...... 35 spiromesifen [2-oxo-3-(2,4,6- Fruit, citrus, group 10 ...... 0 .50 trimethylphenyl)-1-oxaspiro[4.4]non-3- Fruit, pome, group 11 ...... 0.80 Fruit, stone, group 12 ...... 1 .0 en-4-yl 3,3-dimethylbutanoate], 4-hy- Grape ...... 2 .0 droxy-3-(2,4,6-trimethylphenyl)-1- Grape, raisin ...... 6 .0 oxaspiro[4.4]non-3-en-2-one, and its me- Hop, dried cones ...... 30 tabolites containing the 4-hydroxy-3-[4- Mamey sapote ...... 1 .0 (hydroxymethyl)-2,6-dimethylphenyl]- Mango ...... 1.0 1-oxaspiro[4.4]non-3-en-2-one moiety, Nut, tree, group 14 ...... 0 .10 Papaya ...... 1 .0 calculated as the stoichiometric equiv- Pistachio ...... 0.10 alent of spiromesifen, in the following Sapodilla ...... 1 .0 rotational crop commodities: Star apple ...... 1 .0

Parts per Commodity million (2) Tolerances are established for residues of spirodiclofen, including its me- Alfalfa, forage ...... 1.5 tabolites and degradates, in or on the Alfalfa, hay ...... 3.0 Barley, grain ...... 0 .03 commodities listed below. Compliance Barley, hay ...... 0 .25 with the following tolerance levels is Barley, straw ...... 0 .15 Beet, sugar, roots ...... 0 .03 to be determined by measuring only Beet, sugar, tops ...... 0.20 spirodiclofen (3-(2,4-dichlorophenyl)-2- Oat, forage ...... 0 .20 oxo-1-oxaspiro[4.5]dec-3-en-4-yl 2,2- Oat, grain ...... 0 .03 Oat, hay ...... 0.25 dimethylbutanoate) and its metabolite Oat, straw ...... 0.25 3-(2,4-dichlorophenyl)-4-hydroxy-1- Vegetable, bulb, group 3-07 ...... 0 .09 oxaspiro[4,5] dec-3-en-2-one, calculated Wheat, forage ...... 0 .20 Wheat, grain ...... 0 .03 as the stoichiometric equivalent of Wheat, hay ...... 0 .15 spirodiclofen.

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Parts per Parts per Commodity million Commodity million

Cattle, fat ...... 0.02 Soybean, hulls ...... 0 .20 Cattle, meat byproducts ...... 0.10 Soybean, seed ...... 0 .05 Cattle, meat ...... 0 .02 Squash/cucumber subgroup 9B ...... 0.50 Goat, fat ...... 0 .02 Tomato, paste ...... 1 .5 Goat, meat byproducts ...... 0 .1 Vegetable, fruiting, group 8 ...... 1.0 Goat, meat ...... 0.02 Vegetable, tuberous and corm, subgroup 1C ... 0.010 Horse, fat ...... 0 .02 Wheat, forage ...... 7 .0 Horse, meat byproducts ...... 0 .1 Wheat, grain ...... 0 .15 Horse, meat ...... 0 .02 Milk ...... 0.01 Wheat, hay ...... 17 Milk, fat ...... 0 .03 Wheat, straw ...... 11 Sheep, fat ...... 0 .02 Sheep. meat byproducts ...... 0 .1 (2) Tolerances are established for res- Sheep. meat ...... 0.02 idues of fluoxastrobin, including its metabolites and degradates, in or on (b) Section 18 emergency exemptions. the commodities in the table below. [Reserved] Compliance with the tolerance levels (c) Tolerances with regional registra- specified below is to be determined by tions. [Reserved] measuring only fluoxastrobin, (1E)-[2- (d) Indirect or inadvertent residues. [[6-(2-chlorophenoxy)-5-fluoro-4- [Reserved] pyrimidinyl]oxy]phenyl](5,6-dihydro- [70 FR 40211, July 13, 2005, as amended at 73 1,4,2-dioxazin-3-yl)methanone O- FR 25539, May 7, 2008; 75 FR 24434, May 5, methyloxime, its Z isomer, (1Z)-[2-[[6- 2010; 77 FR 73939, Dec. 12, 2012; 79 FR 33464, (2-chlorophenoxy)-5-fluoro-4- June 11, 2014] pyrimidinyl]oxy]phenyl](5,6-dihydro- § 180.609 Fluoxastrobin; tolerances for 1,4,2-dioxazin-3-yl)methanone O- residues. methyloxime, and its phenoxy- hydroxypyrimidine, 6-(2- (a) General. (1) Tolerances are estab- chlorophenoxy)-5-fluoro-4-pyrimidinol, lished for residues of fluoxastrobin, in- calculated as the stoichiometric equiv- cluding its metabolites and degradates, alent of fluoxastrobin. in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be deter- Parts per mined by measuring only Commodity million fluoxastrobin, (1E)-[2-[[6-(2- Cattle, fat ...... 0.10 chlorophenoxy)-5-fluoro-4- Cattle, meat ...... 0 .05 pyrimidinyl]oxy]phenyl](5,6-dihydro- Cattle, meat byproducts ...... 0.20 1,4,2-dioxazin-3-yl)methanone O- Goat, fat ...... 0 .10 Goat, meat ...... 0.05 methyloxime and its Z isomer, (1Z)-[2- Goat, meat byproducts ...... 0 .20 [[6-(2-chlorophenoxy)-5-fluoro-4- Hog, fat ...... 0 .03 pyrimidinyl]oxy]phenyl](5,6-dihydro- Hog, meat byproducts ...... 0 .06 1,4,2-dioxazin-3-yl)methanone O- Horse, fat ...... 0 .10 Horse, meat ...... 0 .05 methyloxime, calculated as the stoi- Horse, meat byproducts ...... 0 .20 chiometric equivalent of fluoxastrobin. Milk ...... 0.03 Milk, fat ...... 0 .75 Commodity Parts per Poultry, liver ...... 0 .06 million Sheep, fat ...... 0 .10 Sheep, meat ...... 0.05 Berry, low growing, subgroup 13-07G ...... 1 .9 Corn, field, forage ...... 3 .0 Sheep, meat byproducts ...... 0 .20 Corn, field, grain ...... 0 .02 Corn, field, stover ...... 4 .5 (b) Section 18 emergency exemptions. Corn, sweet, forage ...... 13 [Reserved] Corn, sweet, kernel plus cob with husks removed ...... 0 .01 (c) Tolerances with regional registra- Corn, sweet, stover ...... 10 tions. [Reserved] Grain, aspirated grain fractions ...... 60 (d) Indirect or inadvertent residues. Leaf petioles subgroup 4B ...... 4 .0 Peanut ...... 0 .02 Tolerances are established for the indi- Peanut, hay ...... 20.0 rect or inadvertent residues of Peanut, refined oil ...... 0.06 fluoxastrobin, including its metabo- Rice, grain ...... 4 .0 Soybean, forage ...... 9 .0 lites and degradates, in or on the com- Soybean, hay ...... 1 .2 modities in the table below, when

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present therein as a result of the appli- metabolites and degradates, in or on cation of fluoxastrobin to the growing the commodities in the table below. crops listed in paragraph (a)(1) of this Compliance with the tolerance levels section. Compliance with the tolerance specified below is to be determined by levels specified below is to be deter- measuring only aminopyralid. mined by measuring only Parts per fluoxastrobin, (1E)-[2-[[6-(2- Commodity million chlorophenoxy)-5-fluoro-4- pyrimidinyl]oxy]phenyl](5,6-dihydro- Cattle, fat ...... 0.02 Cattle, kidney ...... 0 .3 1,4,2-dioxazin-3-yl)methanone O- Cattle, meat ...... 0 .02 methyloxime and its Z isomer, (1Z)-[2- Cattle, meat byproducts, except kidney ...... 0.02 [[6-(2-chlorophenoxy)-5-fluoro-4- Goat, fat ...... 0 .02 Goat, kidney ...... 0 .3 pyrimidinyl]oxy]phenyl](5,6-dihydro- Goat, meat ...... 0.02 1,4,2-dioxazin-3-yl)methanone O- Goat, meat byproducts, except kidney ...... 0 .02 methyloxime, calculated as the stoi- Horse, fat ...... 0 .02 Horse, kidney ...... 0 .3 chiometric equivalent of fluoxastrobin. Horse, meat ...... 0 .02 Horse, meat byproducts, except kidney ...... 0 .02 Commodity Parts per Milk ...... 0.03 million Sheep, fat ...... 0 .02 Sheep, kidney ...... 0.3 Alfalfa, forage ...... 0.050 Sheep, meat ...... 0.02 Alfalfa, hay ...... 0.10 Sheep, meat byproducts, except kidney ...... 0 .02 Cotton, gin byproducts ...... 0 .020 Grain, cereal, forage, fodder, and straw, group 16, except corn ...... 0.10 (b) Section 18 emergency exemptions. Grass, forage ...... 0 .10 [Reserved] Grass, hay ...... 0 .50 Vegetable, foliage of legume, group 7 ...... 0 .050 (c) Tolerances with regional registrations. [Reserved] (d) Indirect or inadvertent residues. [74 FR 67113, Dec. 18, 2009, as amended at 75 [Reserved] FR 60333, Sept. 30, 2010; 76 FR 50898, Aug. 17, 2011; 77 FR 26471, May 4, 2012; 77 FR 64915, [70 FR 46428, Aug. 10, 2005, as amended at 75 Oct. 24, 2012; 79 FR 20105, Apr. 11, 2014] FR 17584, Apr. 7, 2010]

§ 180.610 Aminopyralid; tolerances for § 180.611 Pinoxaden; tolerances for residues. residues. (a) General. (1) Tolerances are estab- (a) General. (1) Tolerances are established for residues of the herbicide lished for the combined residues of aminopyralid, 4-amino-3,6-dichloro-2- pinoxaden (8-(2,6-diethyl-4- pyridinecarboxylic acid, including its methylphenyl)-1,2,4,5-tetrahydro-7-oxo- metabolites and degradates, in or on 7H-pyrazolo[1,2-d][1,4,5] oxadiazepin-9- the commodities in the table below. yl 2,2-dimethylpropanoate), and its me- Compliance with the tolerance levels tabolites 8-(2,6-diethyl-4-methyl- specified below is to be determined by phenyl)-tetrahydro-pyrazolo[1,2- measuring only free and conjugated d][1,4,5]oxadiazepine-7,9-dione (M2), and aminopyralid. free and conjugated forms of 8-(2,6- diethyl-4-hydroxymethyl-phenyl)- Parts per Commodity million tetrahydro-pyrazolo[1,2-d][1,4,5] oxadiazepine-7,9-dione (M4), and 4-(7,9- Corn, field, forage ...... 0 .30 dioxo-hexahydro-pyrazolo[1,2-d] Corn, field, grain ...... 0 .20 Corn, field, stover ...... 0 .20 [1,4,5]oxadiazepin-8-yl)-3,5-diethyl-ben- Grain, aspirated fractions ...... 0 .2 zoic acid (M6), calculated as pinoxaden, Grass, forage ...... 25 in/on the following commodities: Grass, hay ...... 50 Wheat, bran ...... 0.1 Parts per Wheat, forage ...... 2 .0 Commodity million Wheat, grain ...... 0 .04 Wheat, hay ...... 4 .0 Barley, bran ...... 1 .6 Wheat, straw ...... 0 .25 Barley, grain ...... 0 .9 Barley, hay ...... 1 .5 (2) Tolerances are established for res- Barley, straw ...... 1 .0 idues of the herbicide aminopyralid, 4- Egg ...... 0 .06 Poultry, fat ...... 0.06 amino-3,6-dichloro-2- Poultry, meat ...... 0 .06 pyridinecarboxylic acid, including its Poultry, meat byproducts ...... 0.06

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Parts per Parts per Commodity million Commodity million

Wheat, bran ...... 3.0 Corn, sweet, stover ...... 0 .05 Wheat, forage ...... 3 .5 Fish-freshwater finfish ...... 0.05 Wheat, grain ...... 1 .3 Fish-saltwater finfish ...... 0 .05 Wheat, hay ...... 2 .0 Fish-shellfish, crustacean ...... 0 .05 Wheat, straw ...... 1 .5 Fish-shellfish, mollusk ...... 0 .05 Goat, meat byproducts ...... 0 .80 (2) For the combined residues of Hog, meat byproducts ...... 0 .40 Horse, meat byproducts ...... 0 .80 pinoxaden, 8-(2,6-diethyl-4- Poultry, meat byproducts ...... 0.02 methylphenyl)-1,2,4,5-tetrahydro-7-oxo- Sheep, meat byproducts ...... 0 .80 7H-pyrazolo[1,2-d][1,4,5] oxadiazepin-9- yl 2,2-dimethylpropanoate), and its me- (b) Section 18 emergency exemptions. tabolites M2, 8-(2,6-diethyl-4-methyl- [Reserved] phenyl)-tetrahydro-pyrazolo[1,2- (c) Tolerances with regional registra- d][1,4,5]oxadiazepine-7,9-dione, and free tions. [Reserved] and conjugated forms of M4, 8-(2,6- (d) Indirect or inadvertent residues. diethyl-4-hydroxymethyl-phenyl)- [Reserved] tetrahydro-pyrazolo[1,2-d][1,4,5] [78 FR 48074, Aug. 7, 2013] oxadiazepine-7,9-dione, calculated as pinoxaden, in/on the following com- § 180.613 Flonicamid; tolerances for modities: residues. (a) General. (1) Tolerances are estab- Parts per Commodity million lished for the residues of the insecticide flonicamid, including its metabo- Cattle, fat ...... 0.04 Cattle, meat ...... 0 .04 lites and degradates, in or on the com- Cattle, meat byproducts ...... 0.04 modities in the table below. Compli- Milk ...... 0.02 ance with the tolerance levels specified below is to be determined by measuring (b) Section 18 emergency exemptions. only the sum of flonicamid, N- [Reserved] (cyanomethyl)-4-(trifluoromethyl)-3- (c) Tolerances with regional registra- pyridinecarboxamide, and its metabo- tions. [Reserved] lites, TFNA (4- (d) Indirect or inadvertent residues. trifluoromethylnicotinic acid), TFNA– [Reserved] AM (4-trifluoromethylnicotinamide), [70 FR 43322, July 27, 2005] and TFNG, N-(4- trifluoromethylnicotinoyl)glycine, cal- § 180.612 Topramezone; tolerances for culated as the stoichiometric equiva- residues. lent of flonicamid, in or on the fol- (a) General. Tolerances are estab- lowing commodities. lished for residues of the herbicide Parts per topramezone, including its metabolites Commodity million and degradates, in or on the following commodities. Compliance with the fol- Alfalfa, forage ...... 10.0 Alfalfa, hay ...... 1.0 lowing tolerance levels is to be deter- Alfalfa, seed ...... 1 .5 mined by measuring only topramezone Almond, hulls ...... 9 .0 ([3-(4,5-dihydro-3-isoxazolyl)-2-methyl- Berry, low growing, subgroup 13–07G ...... 1 .5 Brassica, head and stem, subgroup 5A ...... 1 .5 4-(methylsulfonyl)phenyl](5-hydroxy-1- Brassica, leafy greens, subgroup 5B ...... 16 methyl-1H-pyrazol-4-yl)methanone) in Cotton, gin byproducts ...... 6 .0 or on the following commodities: Cotton, hulls ...... 2 .0 Cotton, meal ...... 1 .0 Parts per Cotton, undelinted seed ...... 0 .50 Commodity million Cucumber ...... 1 .5 Fruit, pome, group 11–10 ...... 0 .20 Cattle, meat byproducts ...... 0.80 Fruit, stone, group 12–12 ...... 0 .60 Corn, field, forage ...... 0 .05 Hop, dried cones ...... 7 .0 Corn, field, grain ...... 0 .01 Nut, tree, group 14–12 ...... 0 .15 Corn, field, stover ...... 0 .05 Okra ...... 0.40 Corn, pop, grain ...... 0.01 Peppermint, tops ...... 7 .0 Corn, pop, stover ...... 0.05 Potato, granules/flakes ...... 0 .40 Corn, sweet, forage ...... 0 .05 Radish, tops ...... 16 Corn, sweet, kernel plus cob with husks re- Rapeseed subgroup 20A ...... 1 .5 moved ...... 0 .01 Spearmint, tops ...... 7 .0

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Parts per Parts per Commodity million Commodity million

Spinach ...... 9 .0 Sheep, meat ...... 0.08 Tomato, paste ...... 2 .0 Sheep, meat byproducts ...... 0 .08 Tomato, puree ...... 0 .50 Turnip, greens ...... 16 Vegetable, cucurbit, group 9 ...... 1.5 (b) Section 18 emergency exemptions. Vegetable, fruiting, group 8–10 ...... 0 .40 [Reserved] Vegetable, leafy, except brassica, group 4, ex- (c) Tolerances with regional registra- cept spinach ...... 4 .0 Vegetable, root, except sugar beet, subgroup tions. [Reserved] 1B ...... 0 .60 (d) Indirect or inadvertent residues. Vegetable, tuberous and corm, subgroup 1C ..... 0.20 [Reserved] (2) Tolerances are established for the [70 FR 51614, Aug. 31, 2005, as amended at 71 residues of the insecticide flonicamid, FR 15608, Mar. 29, 2006; 73 FR 17923, Apr. 2, including its metabolites and 2008; 77 FR 67776, Nov. 14, 2012; 78 FR 75266, degradates, in or on the commodities Dec. 11, 2013] in the table below. Compliance with the tolerance levels specified below is § 180.614 Kasugamycin; tolerances for residues. to be determined by measuring only the sum of flonicamid, N- (a) General. Tolerances are estab- (cyanomethyl)-4-(trifluoromethyl)-3- lished for residues of kasugamycin, 3- pyridinecarboxamide, and its metabo- O-[2-amino-4- lites, TFNA (4- [(carboxyiminomethyl)amino]-2,3,4,6- trifluoromethylnicotinic acid), and tetradeoxy-a-D-arabino- TFNA–AM (4- hexopyranosyl]-D-chiro-inositol in or trifluoromethylnicotinamide), cal- on the following raw agricultural com- culated as the Stoichiometric equiva- modity: lent of flonicamid, in or on the fol- Parts per lowing commodities. Commodity million

Parts per Vegetable, fruiting, group 8 1 ...... 0.04 Commodity million 1There is no U.S. registration as of September 1, 2005. Cattle, fat ...... 0.03 Cattle, meat ...... 0 .08 (b) Section 18 emergency exemptions. Cattle, meat byproducts ...... 0.08 Time-limited tolerances specified in Egg ...... 0 .04 Goat, fat ...... 0 .03 the following table are established for Goat, meat ...... 0.08 residues of kasugamycin, 3-O-[2-amino- Goat, meat byproducts ...... 0 .08 4-[(carboxyiminomethyl)amino]-2,3,4,6- Hog, fat ...... 0 .03 Hog, meat ...... 0 .03 tetradeoxy-a-D-arabino- Hog, meat byproducts ...... 0 .03 hexopyranosyl]-D-chiro-inositol in or Horse, fat ...... 0 .03 on the specified agricultural commod- Horse, meat ...... 0 .08 Horse, meat byproducts ...... 0 .08 ities, resulting from use of the pes- Milk ...... 0.05 ticide pursuant to FFIFRA section 18 Poultry, fat ...... 0.03 emergency exemptions. The tolerances Poultry, meat ...... 0 .03 Poultry, meat byproducts ...... 0.03 expire and are revoked on the date Sheep, fat ...... 0 .03 specified in the table.

Parts per Expiration/revocation Commodity million date

Apple ...... 0.05 12/31/15

(c) Tolerances with regional registra- § 180.615 Amicarbazone; tolerances for tions. [Reserved] residues. (d) Indirect or inadvertent residues. (a) General. Tolerances are estab- [Reserved] lished for combined residues of the her- [70 FR 55752, Sept. 23, 2005, as amended at 75 bicide, amicarbazone [4-amino-4, 5- FR 19272, Apr. 14, 2010; 77 FR 74119, Dec. 13, dihydro- N-(1,1-dimethylethyl)-3-(1- 2012] methylethyl)-5-oxo-1H-1,2,4-triazole-1-

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carboxamide] and its metabolites DA Commodity Parts per amicarbazone [N-(1,1-dimethylethyl)- million 4,5-dihydro-3-(1-methylethyl)-5-oxo-1H- Alfalfa, forage ...... 0.05 1,2,4-triazole-1-carboxamide] and iPr-2- Alfalfa, hay ...... 0.10 OH DA amicarbazone [N-(1,1- Cotton, gin byproducts ...... 0 .30 Cotton, undelinted seed ...... 0 .07 dimethylethyl)-4,5-dihydro-3-(1-hy- Soybean, forage ...... 1 .50 droxy-1-methylethyl)-5-oxo-1H-1,2,4-tri- Soybean, hay ...... 5 .0 azole-1-carboxamide], calculated as Soybean, seed ...... 0 .80 Wheat, bran ...... 0.15 parent equivalents, in or on the fol- Wheat, flour ...... 0 .15 lowing commodities: Wheat, forage ...... 0 .50 Wheat, germ ...... 0 .15 Parts per Wheat, grain ...... 0 .10 Commodity million Wheat, hay ...... 1 .0 Wheat, middlings, ...... 0.15 Cattle, fat ...... 0.01 Wheat, shorts ...... 0 .15 Wheat, straw ...... 0 .50 Cattle, liver ...... 1 .0 Cattle, meat ...... 0 .01 Cattle, meat byproducts, except liver ...... 0 .10 [70 FR 55760, Sept. 23, 2005, as amended at 74 Corn, field, forage ...... 0 .80 FR 46377, Sept. 9, 2009] Corn, field, grain ...... 0 .05 Corn, field, stover ...... 1 .0 § 180.616 Fenpropimorph; tolerances Goat, fat ...... 0 .01 for residues. Goat, liver ...... 1.0 Goat, meat ...... 0.01 Tolerances are established for the Goat, meat byproducts, except liver ...... 0 .10 residues of the fungicide Hog, fat ...... 0 .01 fenpropimorph (rel-(2R,6S)-4-[3-[4-(1,1- Hog, liver ...... 0 .10 dimethylethyl)phenyl]-2- Hog, meat ...... 0 .01 methylpropyl]-2,6-dimethylmorpholine) Hog, meat byproducts, except liver ...... 0 .01 in or on the following commodity: Horse, fat ...... 0 .01 Horse, liver ...... 1 .0 Parts per Horse, meat ...... 0 .01 Commodity million Horse, meat byproducts, except liver ...... 0 .10 Milk ...... 0.01 Banana* ...... 2 .0 Sheep, fat ...... 0 .01 *No U.S. registration as of February 10, 2006. Sheep, liver ...... 1.0 Sheep, meat ...... 0.01 (b) Section 18 emergency exemptions. Sheep, meat byproducts, except liver ...... 0 .10 [Reserved] Poultry, liver ...... 0 .10 (c) Tolerances with regional registrations. [Reserved] (b) Section 18 emergency exemptions. (d) Indirect or inadvertent residues. [Reserved] [Reserved] (c) Tolerances with regional registra- [71 FR 15612, Mar. 29, 2006] tions. [Reserved] (d) Indirect or inadvertent residues. § 180.617 Metconazole; tolerances for Tolerances are established for the indi- residues. rect or inadvertent residues of (a) General. Tolerances are estab- amicarbazone [4-amino-4, 5-dihydro-N- lished for residues of metconazole, in- (1,1-dimethylethyl)-3-(1-methylethyl)-5- cluding its metabolites and degradates, oxo-1H-1,2,4-triazole-1-carboxamide] in or on the commodities in the fol- and its metabolites DA amicarbazone lowing table. Compliance with the tol- [N-(1,1-dimethylethyl)-4,5-dihydro-3-(1- erance levels specified below is to be methylethyl)-5-oxo-1H-1,2,4-triazole-1- determined by measuring only carboxamide] and iPr-2-OH DA metconazole [5-[(4- amicarbazone [N-(1,1-dimethylethyl)- chlorophenyl)methyl]-2,2-dimethyl-1- 4,5-dihydro-3-(1-hydroxy-1- (1H-1,2,4-triazol-1- methylethyl)-5-oxo-1H-1,2,4-triazole-1- ylmethyl)cyclopentanol] as the sum of carboxamide], calculated as parent its cis- and trans-isomers in or on the equivalents, in or on the following following commodities: commodities when present therein as a result of application of amicarbazone Commodity Parts per to the growing crops in paragraph (a) million of this section: Almond, hulls ...... 4 .0

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Parts per Expiration/ Commodity million Commodity Parts per revocation million date Banana 1 ...... 0.1 Barley, grain ...... 2 .5 Sugarcane, cane ...... 1.6 12/31/14 Barley, hay ...... 7 .0 Sugarcane, molasses ...... 3.2 12/31/14 Barley, straw ...... 7 .0 Beet, sugar, dried pulp ...... 0 .70 (c) Tolerances with regional registra- Beet, sugar, molasses ...... 0 .08 tions. [Reserved] Beet, sugar, roots ...... 0 .07 Bushberry subgroup 13–07B ...... 0 .40 (d) Indirect or inadvertent residues. Canola seed ...... 0 .04 [Reserved] Cattle, meat byproducts ...... 0.04 Corn, field, forage ...... 3 .0 [71 FR 56388, Sept. 27, 2006, as amended at 71 Corn, field, grain ...... 0 .02 FR 76196, Dec. 20, 2006; 73 FR 22828, Apr. 28, Corn, field, stover ...... 30 2008; 74 FR 21266, May 7, 2009; 76 FR 50904, Corn, pop, grain ...... 0.02 Aug. 17, 2011; 76 FR 81396, Dec. 28, 2011; 77 FR Corn, pop, stover ...... 30 26456, May 4, 2012; 77 FR 66723, Nov. 7, 2012; 79 Corn, sweet, forage ...... 3 .0 FR 12411, Mar. 5, 2014] Corn, sweet, kernel plus cob with husks removed ...... 0 .01 Corn, sweet, stover ...... 30.0 § 180.618 Benthiavalicarb-isopropyl; Cotton, gin byproducts ...... 8 .0 tolerance for residues. Cotton, undelinted seed ...... 0 .25 (a) General. Tolerances are estab- Egg ...... 0 .04 Fruit, stone, group 12 ...... 0 .20 lished for the combined residues of Goat, meat byproducts ...... 0 .04 benthiavalicarb-isopropyl, Grain, aspirated grain fractions ...... 7 .0 isopropyl[(S)-1-[[[(1R)-1-(6-fluoro-2- Horse, meat byproducts ...... 0 .04 benzothiazolyl)ethyl]amino] carbonyl]- Nut, tree, group 14 ...... 0 .04 Oat, grain ...... 1 .0 2-methylpropyl]carbamate and Oat, hay ...... 17 isopropyl[(S)-1-[[[(1S)-1-(6-fluoro-2- Oat, straw ...... 6.0 benzothiazolyl)ethyl]amino] carbonyl]- Peanut ...... 0 .04 Peanut, refined oil ...... 0.05 2-methylpropyl]carbamate, in or on the Pistachio ...... 0.04 following raw agricultural commod- Rye, grain ...... 0.25 ities: Rye, straw ...... 14 Sheep, meat byproducts ...... 0 .04 Parts per Soybean, forage ...... 3 .0 Commodity million Soybean, hay ...... 6 .0 Soybean, hulls ...... 0 .08 Grape, imported ...... 0 .25 Soybean, seed ...... 0 .05 Grape, raisin ...... 1 .0 Sugarcane, cane ...... 0.06 Tomato ...... 0.45 Vegetable, tuberous and corn, subgroup 1C ...... 0.04 Note: There are no U.S. registrations as of July 30, 2006. Wheat, grain ...... 0 .15 Wheat, hay ...... 16 (b) Section 18 emergency exemptions. Wheat, milled byproducts ...... 0 .20 [Reserved] Wheat, straw ...... 18 (c) Tolerances with regional registra- 1 No U.S. registration as of August 30, 2006. tions. [Reserved] (b) Section 18 emergency exemptions. (d) Indirect of inadvertent residues. Time-limited tolerances are estab- [Reserved] lished for the residues of the fungicide [71 FR 52003, Sept. 1, 2006] metconazole, including its metabolites and degradates, in or on the commod- § 180.619 Epoxiconazole; tolerances for ities listed in the following table in residues. connection with the use of the pes- (a) General. Tolerances are estab- ticide under section 18 emergency ex- lished for the residues of the fungicide emptions granted by EPA. The toler- epoxiconazole [(rel-1-[[(2R,3S)-3-(2- ances expire and are revoked on the chlorophenyl)-2-(4- dates specified in the following table. fluorophenyl)oxiranyl]methyl]-1H-1,2,4- Compliance with the tolerance levels triazole]) in or on the following com- specified below is to be determined by modities: measuring only metconazole (5-[(4- chlorophenyl)-methyl]-2,2-dimethyl-1- Commodity Parts per (1H-1,2,4-triazol-1- million ylmethyl)cyclopentanol) as the sum of Banana* ...... 0 .5 its cis- and trans-isomers in or on the Coffee* ...... 0 .05 following commodities: *No U.S. Registration as of August 4, 2006

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(b) Section 18 emergency exemptions. levels specified below is to be deter- [Reserved] mined by measuring only dithianon, 5, (c) Tolerances with regional Registra- 10-dihydro-5,10-dioxonaphtho(2,3-b)-1,4- tions. [Reserved] dithiin-2,3-dicarbonitrile. (d) Indirect or inadvertent residues. Parts per [Reserved] Commodity million

[71 FR 53989, Sept. 13, 2006] Fruit, pome, group 111 ...... 5 Grape 2 ...... 3 § 180.620 Etofenprox; tolerances for Hop, dried cones1 ...... 100 residues. 1No U.S. registration as of September 5, 2006. (a) General. A tolerance is established 2No U.S. registration as of January 29, 2010. for residues of the insecticide (b) Section 18 emergency exemptions. etofenprox, including its metabolites [Reserved] and degradates, in or on the com- (c) Tolerances with regional registra- modity in the table in this paragraph. tions. [Reserved] Compliance with the tolerance level (d) Indirect or inadvertent residues. specified in this paragraph is to be de- [Reserved] termined by measuring only [75 FR 5522, Feb. 3, 2010] etofenprox, 2-(4-ethoxyphenyl)-2- methylpropyl 3-phenoxybenzyl ether, § 180.622 Ethaboxam; tolerances for in or on the commodity. residues. (a) General. Tolerances are estab- Commodity Parts per million lished for residues of ethaboxam, N- Cattle, fat ...... 10.0 (cyano-2-thienylmethyl)-4-ethyl-2- Cattle, meat ...... 0 .40 (ethlyamino)-5-thiazolecarboxamide in Cattle, meat byproducts ...... 10.0 or on the following commodity: Egg ...... 0 .40 All food commodities (including feed commod- Parts per ities) not otherwise listed in this subsection .... 5 .0 Commodity million Goat, fat ...... 10 .0 Goat, meat ...... 0.40 Grape 1 ...... 6 .0 Goat, meat byproducts ...... 10 .0 Hog, fat ...... 4 .0 1 There is no U.S. registration as of September 27, 2006 Hog, meat ...... 0 .20 Hog, meat byproducts ...... 4 .0 (b) Section 18 emergency exemptions. Horse, fat ...... 10 .0 [Reserved] Horse, meat ...... 0 .40 (c) Tolerances with regional registra- Horse, meat byproducts ...... 10 .0 tions. [Reserved] Milk ...... 0.60 Poultry, fat ...... 1.0 (d) Indirect or inadvertent residues. Poultry, meat ...... 0 .01 [Reserved] Poultry, meat byproducts ...... 1.0 Rice, grain ...... 0 .01 [71 FR 56392, Sept. 27, 2006] Sheep, fat ...... 10 .0 Sheep, meat ...... 0.40 § 180.623 Flufenoxuron; tolerances for Sheep, meat byproducts ...... 10 .0 residues. (b) Section 18 emergency exemptions. (a) General. Tolerances are estab- [Reserved] lished for residues of the insecticide, (c) Tolerances with regional registra- flufenoxuron, 1-[4-(2-chloro-a,a,a- tions. [Reserved] trifluoro-p-tolyloxy)-2-fluorophenyl]-3- (d) Indirect or inadvertent residues. (2,6-difluorobenzoyl)urea, in or on the [Reserved] following food commodities.

[76 FR 23498, Apr. 27, 2011, as amended at 78 Commodity Parts per FR 70877, Nov. 27, 2013] million Apple 1 ...... 0.50 § 180.621 Dithianon; tolerances for res- Cattle, fat 1 ...... 4.5 idues. Cattle, meat 1 ...... 0 .10 Cattle, meat byproducts 1 ...... 0.50 (a) General. Tolerances are estab- Goat, fat 1 ...... 4 .5 lished for residues of dithianon, includ- Goat, meat 1 ...... 0.10 ing its metabolites and degradates, in Goat, meat byproducts 1 ...... 0 .50 Grape 1 ...... 0 .70 or on the commodities in the table Grape, raisin 1 ...... 2 .0 below. Compliance with the tolerance Horse, fat 1 ...... 4 .5

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Parts per Parts per Commodity million Commodity million

Horse, meat 1 ...... 0 .10 Rice, grain ...... 0 .05 Horse, meat byproducts 1 ...... 0 .50 Rice, straw ...... 0 .05 Milk ...... 0.20 Milk, fat 1 ...... 4 .0 (b) Section 18 emergency exemptions. Orange 1 ...... 0 .30 [Reserved] Orange, oil 1 ...... 60 (c) Tolerances with regional registra- 1 Pear ...... 0 .50 tions. [Reserved] Sheep, fat 1 ...... 4 .5 Sheep, meat 1 ...... 0.10 (d) Indirect and inadvertant residues. Sheep, meat byproducts 1 ...... 0 .50 [Reserved] 1There are no U.S. registrations as of September 30, 2006. [72 FR 8931, Feb. 28, 2007] (b) Section 18 emergency exemptions. § 180.626 Prothioconazole; tolerances [Reserved] for residues. (c) Tolerances with regional restric- (a) General. (1) Tolerances are estab- tions. [Reserved] lished for residues of prothioconazole, (d) Indirect or inadvertent residues. 2-[2-(1-chlorocylcopropyl)-3-(2- [Reserved] chlorophenyl)-2-hydroxypropyl]-1,2- [71 FR 57436, Sept. 29, 2006] dihydro-3H-1,2,4-triazole-3-thion, including its metabolites and degradates, § 180.624 Metrafenone; tolerances for in or on the commodities in the table residues. below. Compliance with the tolerance levels specified below is to be deter- (a) General. Tolerances are estab- mined by measuring only lished for residues of the fungicide prothioconazole and its metabolite metrafenone, including its metabolites prothioconazole-desthio, or -(1- and degradates, in or on the commod- a chlorocyclopropyl)- -[(2- ities in the table below. Compliance a chlorophenyl)methyl]-1H-1,2,4-triazole- with the tolerance levels specified in 1-ethanol, calculated as parent in or on the following table is to be determined the commodity. by measuring only metrafenone (3- bromo-6-methoxy-2- Commodity Parts per methylphenyl)(2,3,4-trimethoxy-6- million methylphenyl)methanone in or on the Alfalfa, forage ...... 0.02 following commodities: Alfalfa, hay ...... 0.02 Beet, sugar, roots ...... 0 .25 Parts per Berry, low growing, except strawberry, subgroup Commodity million 13–07H ...... 0 .20 Bushberry, subgroup 13–07B ...... 2.0 Grape ...... 4 .5 Corn, sweet kernel plus cob with husks re- Grape, raisin ...... 17 moved ...... 0 .04 Grain, aspirated grain fractions ...... 11 Grain, cereal, forage, fodder and straw, group (b) Section 18 emergency exemption. 16, except sorghum, and rice; forage ...... 8 .0 [Reserved] Grain, cereal, forage, fodder and straw, group 16, except sorghum, and rice; hay ...... 7 .0 (c) Tolerances with regional registra- Grain, cereal, forage, fodder and straw, group tions. [Reserved] 16, except sorghum, and rice; stover ...... 10 (d) Indirect or inadvertent residues. Grain, cereal, forage, fodder and straw, group 16, except sorghum, straw ...... 5 .0 [Reserved] Grain, cereal, group 15, except sweet corn and sorghum ...... 0 .35 [71 FR 54917, Sept. 20, 2006, as amended at 75 Pea and bean, dried shelled, except soybean, FR 75393, Dec. 3, 2010] subgroup 6C ...... 0 .9 Peanut ...... 0 .02 § 180.625 Orthosulfamuron; tolerances Potato ...... 0 .02 for residues. Rapeseed, seed ...... 0 .15 Rice, hulls ...... 0 .90 (a) General. Tolerances are estab- Soybean, forage ...... 4 .5 lished for residues of orthosulfamuron Soybean, hay ...... 17 Soybean, seed ...... 0 .15 1-(4,6-dimethoxypyrimidin-2-yl)-3-[2- Vegetable, cucurbit, crop group 9 ...... 0.30 (dimethylcarbamoyl)- phenylsulfamoyl] urea) per se in or on (2) Tolerances are established for res- the following commodities: idues of prothioconazole, 2-[2-(1-

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chlorocylcopropyl)-3-(2-chlorophenyl)- Commodity Parts per 2-hydroxypropyl]-1,2-dihydro-3H-1,2,4- million triazole-3-thion, including its metabo- Brassica, head and stem, subgroup 5A ...... 5 .0 lites and degradates, in or on the com- Grape ...... 2 .0 modities in the table below. Compli- Grape, raisin ...... 6 .0 Potato, processed waste ...... 0.05 ance with the tolerance levels specified Vegetable, brassica (cole) leafy subgroup 5B .... 18 below is to be determined by measuring Vegetable, bulb, crop group 3–07 ...... 7.0 only prothioconazole and its metabo- Vegetable, cucurbit, group 9 ...... 0.50 Vegetable, fruiting, group 8 ...... 1.60 lites prothioconazole-desthio, or a-(1- Vegetable, leafy, except brassica, group 4 ...... 25 chlorocyclopropyl)-a-[(2- Vegetable, leaves of root and tuber, group 2 ..... 15 .0 chlorophenyl)methyl]-1H-1,2,4-triazole- Vegetable root, subgroup 1A ...... 0.15 1-ethanol, and conjugates that can be Vegetable, tuberous and corm subgroup 1C ...... 0 .02 converted to these two compounds by (b) Section 18 emergency exemptions. acid hydrolysis, calculated as parent in [Reserved] or on the commodity. (c) Tolerances with regional registra- Parts per tions. [Reserved] Commodity million (d) Indirect or inadvertent residues. Tolerances are established for residues Cattle, fat ...... 0.1 Cattle, meat ...... 0 .02 of the fungicide fluopicolide [2,6- Cattle, meat byproducts ...... 0.2 dichloro-N-[[3-chloro-5- Goat, fat ...... 0 .1 (trifluoromethyl)-2- Goat, meat ...... 0.02 pyridinyl]methyl]benzamide], includ- Goat, meat byproducts ...... 0 .2 Hog, meat byproducts ...... 0 .05 ing its metabolites and degradates, in Horse, fat ...... 0 .1 or on the commodities in the table in Horse, meat ...... 0 .02 this paragraph. Compliance with the Horse, meat byproducts ...... 0 .2 tolerance levels specified below is to be Milk ...... 0.02 Poultry liver ...... 0 .02 determined by measuring only Sheep, fat ...... 0 .1 fluopicolide [2,6-dichloro-N-[[3-chloro-5- Sheep, meat ...... 0.02 (trifluoromethyl)-2- Sheep, meat byproducts ...... 0 .2 pyridinyl]methyl]benzamide] in or on the commodity. (b) Section 18 emergency exemptions. [Reserved] Commodity Parts per (c) Tolerances with regional registra- million tions. [Reserved] Corn, field, forage ...... 0 .08 (d) Indirect or inadvertent residues. Corn, field, grain ...... 0 .01 Corn, field, stover ...... 0 .20 [Reserved] Wheat, aspirated grain fractions ...... 0.07 [72 FR 11783, Mar. 14, 2007, as amended at 73 Wheat, forage ...... 0 .20 Wheat, grain ...... 0 .02 FR 14719, Mar. 19, 2008; 74 FR 14749, Apr. 1, Wheat, hay ...... 0 .50 2009; 74 FR 46699, Sept. 11, 2009; 75 FR 29914, Wheat, milled byproducts ...... 0 .07 May 28, 2010; 76 FR 61592, Oct. 5, 2011; 78 FR Wheat, straw ...... 0 .50 67052, Nov. 8, 2013] [72 FR 14447, Mar. 28, 2007, as amended at 73 § 180.627 Fluopicolide; tolerances for FR 5455, Jan. 30, 2008; 73 FR 30498, May 28, residues. 2008; 76 FR 22054, Apr. 20, 2011; 79 FR 12401, (a) General. Tolerances are estab- Mar. 5, 2014] lished for residues of the fungicide fluopicolide [2,6-dichloro-N-[[3-chloro-5- § 180.628 Chlorantraniliprole; toler- (trifluoromethyl)-2- ances for residues. pyridinyl]methyl]benzamide], includ- (a) General. Tolerances are estab- ing its metabolites and degradates, in lished for residues of the insecticide or on the commodities in the table in chlorantraniliprole, including its me- this paragraph. Compliance with the tabolites and degradates, in or on the tolerance levels specified below is to be commodities in the table below. Com- determined by measuring only pliance with the tolerance levels speci- fluopicolide [2,6-dichloro-N-[[3-chloro-5- fied below is to be determined by meas- (trifluoromethyl)-2- uring only chlorantraniliprole, 3- pyridinyl]methyl]benzamide] in or on bromo-N-[4-chloro-2-methyl-6- the commodity. [(methylamino)carbonyl]phenyl]-1-(3-

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chloro-2-pyridinyl)-1H-pyrazole-5- Commodity Parts per carboxamide. million Horse, meat byproducts ...... 0 .5 Parts per Commodity million Ilama ...... 4 .0 Jaboticaba ...... 2 .0 Acerola ...... 2.0 Longan ...... 4 .0 Alfalfa, seed ...... 7 .0 Lychee ...... 2 .0 Almond, hulls ...... 5 .0 Mango ...... 4.0 Animal feed, nongrass, group 18, forage ...... 25 Milk ...... 0.1 Animal feed, nongrass, group 18, hay ...... 90 Apple, wet pomace ...... 2 .5 Nut, tree, group 14 ...... 0 .04 Artichoke, globe ...... 4.0 Olive ...... 4 .0 Asparagus ...... 13 Olive, oil ...... 40 Atemoya ...... 4 .0 Onion, bulb, subgroup 3–07A ...... 0 .30 Avocado ...... 4 .0 Onion, green, subgroup 3–07B ...... 3 .0 Banana ...... 4.0 Papaya ...... 4 .0 Beet, sugar, molasses ...... 9 .0 Passionfruit ...... 4 .0 Berry, large shrub/tree, subgroup 13–07C ...... 2 .5 Peanut ...... 0 .06 Berry, low growing, subgroup 13–07G ...... 1 .0 Biriba ...... 4 .0 Peanut, hay ...... 90 Brassica, head and stem, subgroup 5A ...... 4 .0 Peppermint, tops ...... 9 .0 Brassica, leafy greens, subgroup 5B ...... 11 Persimmon ...... 4 .0 Bushberry, subgroup 13–07B ...... 2.5 Pineapple ...... 1.5 Cacao bean ...... 0 .08 Pineapple, process residue ...... 3 .0 Cacao bean, chocolate ...... 1 .5 Pistachio ...... 0.04 Cacao bean, cocoa powder ...... 1 .5 Plum, chickasaw ...... 2 .0 Cacao bean, roasted bean ...... 0 .8 Cactus ...... 13 Plum, damson ...... 2 .0 Canistel ...... 4 .0 Pomegranate ...... 4 .0 Cattle, fat ...... 0.5 Poultry, fat ...... 0.2 Cattle, meat ...... 0 .1 Poultry, meat ...... 0 .05 Cattle, meat byproducts ...... 0.5 Poultry, meat byproducts ...... 0.2 Cherimoya ...... 4 .0 Pulasan ...... 4 .0 Cherry, sweet ...... 2 .0 Rambutan ...... 4 .0 Cherry, tart ...... 2 .0 Rapeseed subgroup 20A ...... 2 .0 Citrus, dried pulp ...... 14 Rice, grain ...... 0 .15 Coffee, green bean ...... 0 .4 Coffee, instant ...... 2 .0 Rice, hulls ...... 0 .4 Corn, field, grain ...... 0 .04 Sapodilla ...... 4 .0 Corn, field, milled byproducts ...... 0 .1 Sapote, black ...... 4 .0 Corn, pop, grain ...... 0.04 Sapote, mamey ...... 4 .0 Corn, sweet, kernel plus cobs with husk re- Sapote, white ...... 4 .0 moved ...... 0 .02 Sheep, fat ...... 0 .5 Cotton, gin byproduct ...... 30 Sheep, meat ...... 0.1 Cotton, hulls ...... 0 .40 Sheep meat byproducts ...... 0 .5 Cottonseed subgroup 20C ...... 0 .3 Soursop ...... 4 .0 Crayfish ...... 8.0 Custard apple ...... 4 .0 Spanish lime ...... 4 .0 Egg ...... 0 .2 Spearmint, tops ...... 9 .0 Feijoa ...... 4 .0 Spice, subgroup 19B ...... 90 Fig ...... 4 .0 Star apple ...... 4 .0 Fruit, caneberry, subgroup 13–07A ...... 1 .8 Starfruit ...... 4 .0 Fruit, citrus, group 10–10 ...... 1 .4 Sugar apple ...... 4 .0 Fruit, pome, group 11–10 ...... 1 .2 Sugarcane, cane ...... 14 Fruit, small vine climbing, subgroup 13–07F ...... 2.5 Sugarcane, molasses ...... 420 Fruit, stone, group 12–12, except cherry, chicka- Sunflower subgroup 20B ...... 2.0 saw plum, and damson plum ...... 4 .0 Tea, dried ...... 50 .0 Goat, fat ...... 0 .5 Ti, leaves ...... 13 .0 Goat, meat ...... 0.1 Goat, meat byproducts ...... 0 .5 Ti, root ...... 0 .3 Grain, aspirated grain fractions ...... 640 Vegetable, cucurbit, group 9 ...... 0.5 Grain, cereal, except rice and corn, group 15 .... 6.0 Vegetable, foliage of legume, group 7 ...... 90 Grain, cereal, forage, fodder and straw, group Vegetable, fruiting, group 8–10 ...... 1 .4 16 ...... 40 Vegetable, leafy, except brassica, group 4 ...... 13 Grape, raisin ...... 5 .0 Vegetable, leaves of root and tuber, group 2 ..... 40 .0 Grass forage, fodder and hay, group 17 ...... 90 Vegetable, legume, group 6 ...... 2 .0 Guava ...... 4 .0 Vegetable, root and tuber, group 1 ...... 0 .30 Herb subgroup 19A, dried leaves ...... 90 Wax jambu ...... 4 .0 Herb subgroup 19A, fresh leaves ...... 25 Hog, fat ...... 0 .05 Hog, meat ...... 0 .02 (b) Section 18 emergency exemptions. Hog, meat byproducts ...... 0 .05 [Reserved] Hop, dried cones ...... 90 Horse, fat ...... 0 .5 (c) Tolerances with regional registra- Horse, meat ...... 0 .1 tions. [Reserved]

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(d) Indirect or inadvertent residues. Commodity Parts per [Reserved] million [75 FR 5532, Feb. 3, 2010, as amended at 75 FR Horse, liver ...... 0 .80 17566, Apr. 7, 2010; 76 FR 44821, July 27, 2011; Horse, meat byproducts, except liver ...... 0 .05 Horse, muscle ...... 0.05 76 FR 59909, Sept. 28, 2011; 77 FR 60315, Oct. 3, Japanese horse-chestnut ...... 0 .02 2012; 77 FR 75561, Dec. 21, 2012; 78 FR 57285, Macadamia nut ...... 0 .02 Sept. 18, 2013; 79 FR 7401, Feb. 7, 2014] Milk ...... 0.01 Mongongo nut ...... 0 .02 EDITORIAL NOTE: At 78 FR 57285, Sept. 18, Monkey-pot ...... 0 .02 2013, § 180.628 was amended by revising the Pachira nut ...... 0 .02 commodity ‘‘Egg’’ in the table in paragraph Peanut ...... 0 .09 (a); however, no revised text was provided, so Peanut, hay ...... 15 the amendment could not be incorporated. Pecan ...... 0 .02 Sapucaia nut ...... 0.02 Sheep, fat ...... 0 .05 § 180.629 Flutriafol; tolerances for resi- Sheep, liver ...... 0.80 dues. Sheep, meat byproducts, except liver ...... 0 .05 (a) General. Tolerances are estab- Sheep, muscle ...... 0 .05 Soybean, seed ...... 0 .35 lished for the residues of flutriafol, Strawberry ...... 1 .5 [(±)-a-(2-fluorophenyl)-a-(4- Tomato, paste ...... 1 .5 fluorophenyl)-1H-1,2,4-triazole-1-eth- Vegetable, cucurbit, group 9 ...... 0.30 Vegetable, fruiting, group 8–10 ...... 1 .0 anol], including its metabolites and Walnut, black ...... 0 .02 degradates in or on the following com- Walnut, English ...... 0.02 modities. Compliance with the fol- Wheat, bran ...... 0.30 Wheat, forage ...... 30 lowing tolerances is to be determined Wheat, germ ...... 0 .25 by measuring flutriafol only. Wheat, grain ...... 0 .15 Wheat, hay ...... 15 Parts per Wheat, straw ...... 9 .0 Commodity million 1 There are no U.S. registrations as of October 22, 2013. African tree nut ...... 0 .02 Almond ...... 0.60 (b) Section 18 emergency exemptions. Almond, hull ...... 15 Time-limited tolerances specified in Banana 1 ...... 0.30 the following table are established for Beet sugar ...... 0 .08 ± Brazil nut ...... 0 .02 residues of flutriafol, [( )-a-(2- Bur oak ...... 0 .02 fluorophenyl)-a-(4-fluorophenyl)-1 H Butternut ...... 0 .02 -1,2,4-triazole-1-ethanol], including its Cajou ...... 0 .02 metabolites and degradates in or on Cashew ...... 0 .02 Castanha-do-maranhao ...... 0.02 the specified agricultural commodities, Cattle, fat ...... 0.05 resulting from use of the pesticide pur- Cattle, liver ...... 0 .80 suant to FIFRA section 18 emergency Cattle, meat byproducts, except liver ...... 0 .05 Cattle, muscle ...... 0 .05 exemptions. The tolerances expire on Coconut ...... 0 .02 the date specified in the table. Coffee, green, bean 1 ...... 0 .15 Coffee, instant 1 ...... 0 .30 Commodity Parts per Expiration Coquito nut ...... 0 .02 million date Corn, field, forage ...... 5 .0 Corn, field, grain ...... 0 .01 Cotton, gin byproducts ...... 0.5 12/31/14 Corn, field, refined oil ...... 0 .02 Cotton, meal ...... 0.5 12/31/14 Corn, field, stover ...... 15 Cotton, refined oil ...... 0.5 12/31/14 Corn, pop ...... 0 .01 Cotton, undelinted seed ...... 0.35 12/31/14 Corn, pop, stover ...... 15 Dika nut ...... 0 .02 (c) Tolerances with regional registra- Fruit, pome, group 11–09 ...... 0 .40 Fruit, stone, group 12–10 ...... 1 .5 tions [Reserved] Goat, fat ...... 0 .05 (d) Indirect or inadvertent residues. Goat, liver ...... 0.80 Tolerances are established for the indi- Goat, meat byproducts, except liver ...... 0 .05 rect or inadvertent residues of the fun- Goat, muscle ...... 0 .05 Grain, aspirated fractions ...... 2 .2 gicide flutriafol, including its metabo- Grape ...... 1 .5 lites and degradates, in or on the com- Grape, raisin ...... 2 .4 modities in the table below when Guiana chestnut ...... 0 .02 Hazelnut ...... 0 .02 present therein as a result of the appli- Heartnut ...... 0 .02 cation of flutriafol to the growing Hickory nut ...... 0 .02 crops listed in the table to paragraph Hog, fat ...... 0 .01 Hog, muscle ...... 0.01 (a) of this section. Compliance with the Horse, fat ...... 0 .05 following tolerance levels specified

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below is to be determined by measuring droxy-3-methyl-1H-pyrazol-4-yl)[2- only flutriafol ((±)-a-(2-fluorophenyl)-a- (methylsulfonyl)-4- (4-fluorophenyl)-1H-1,2,4-triazole-1-eth- (trifluoromethyl)phenyl]methanone), anol) in or on the following commod- calculated as the stoichiometric equiv- ities: alent of pyrasulfotole, in or on the commodities: Commodity Parts per million Parts per Commodity million Corn, sweet, forage ...... 0 .09 Corn, sweet, kernel plus cob with husk removed 0.01 Aspirated grain fractions ...... 0 .40 Corn, sweet, stover ...... 0 .07 Barley, grain ...... 0 .02 Cotton, gin byproducts ...... 0 .02 Barley, hay ...... 0 .30 Cotton, undelinted seed ...... 0 .01 Barley, straw ...... 0 .20 Cattle, fat ...... 0.03 Cattle, liver ...... 3 .0 [75 FR 26673, May 12, 2010, as amended at 76 Cattle, meat ...... 0 .02 FR 69647, Nov. 9, 2011; 77 FR 47301, Aug. 8, Cattle, meat byproducts, except liver ...... 0 .70 2012; 77 FR 48901, Aug. 15, 2012; 78 FR 75262, Eggs ...... 0 .02 Dec. 11, 2013; 79 FR 32673, June 6, 2014] Goat, fat ...... 0 .03 Goat, liver ...... 3.0 § 180.630 Flusilazole; tolerances for Goat, meat ...... 0.02 Goat, meat byproducts, except liver ...... 0 .70 residues. Grass, forage ...... 25 (a) General. [Reserved] Grass, hay ...... 3 .5 Hog, fat ...... 0 .02 (b) Section 18 emergency exemptions. Hog, liver ...... 0 .30 Time-limited tolerances are estab- Hog, meat ...... 0 .02 lished for residues of the fungicide, Hog, meat byproducts, except liver ...... 0 .05 flusilazole, (1-[[bis(4- Horse, fat ...... 0 .03 Horse, liver ...... 3 .0 fluorophenyl)methylsilyl]methyl]-1H- Horse, meat ...... 0 .02 1,2,4-triazole) in connection with use of Horse, meat byproducts, except liver ...... 0 .70 the pesticide under Section 18 emer- Milk ...... 0.03 Oat, forage ...... 0 .10 gency exemptions granted by EPA. The Oat, grain ...... 0 .08 tolerances expire and are revoked on Oat, hay ...... 0.50 the dates specified in the following Oat, straw ...... 0.20 table. Poultry, fat ...... 0.02 Poultry, meat ...... 0 .02 Poultry, meat byproducts ...... 0.20 Expiration/ Commodity Parts per revocation Rye, forage ...... 0 .20 million date Rye, grain ...... 0.02 Rye, straw ...... 0 .20 Soybean, aspirated grain fractions 2.6 12/31/10 Sheep, fat ...... 0 .03 Soybean, seed ...... 0.04 12/31/10 Sheep, liver ...... 3.0 Soybean, oil ...... 0.10 12/31/10 Sheep, meat ...... 0.02 Sheep, meat byproducts, except liver ...... 0 .70 (c) Tolerances with regional registra- Sorghum, grain, forage ...... 1.5 Sorghum, grain, grain ...... 0 .70 tions. [Reserved] Sorghum, grain, stover ...... 0 .80 (d) Indirect or inadvertant residues. Wheat, forage ...... 0 .20 [Reserved] Wheat, grain ...... 0 .02 Wheat, hay ...... 0 .80 [72 FR 49660, Aug. 29, 2007] Wheat, straw ...... 0 .20

§ 180.631 Pyrasulfotole; tolerances for (b) Section 18 emergency exemptions. residues. [Reserved] (a) General. Tolerances are estab- (c) Tolerances with regional registra- lished for residues of the herbicide tions. [Reserved] pyrasulfotole, including its metabo- (d) Indirect or inadvertent residues. lites and degradates, in or on the com- [Reserved] modities in the table below. Compli- [72 FR 45649, Aug. 15, 2007, as amended at 76 ance with the tolerance levels specified FR 23898, Apr. 29, 2011] below is to be determined by measuring only the sum of pyrasulfotole ((5-hy- § 180.632 Fenazaquin; import toler- droxy-1,3-dimethyl-1H-pyrazol-4-yl)[2- ances for residues. (methylsulfonyl)-4- (a) General. Import tolerances are es- (trifluoromethyl)phenyl]methanone) tablished for residues of the insecticide and its desmethyl metabolite (5-hy- and miticide, fenazaquin, 4-tert-

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butylphenethyl quinazolin-4-yl ether, tembotrione, 2-[2-chloro-4- in or on raw agricultural commodities (methylsulfonyl)-3-[(2,2,2- as follows: trifluoroethoxy)methyl]benzoyl]-1,3- cyclohexanedione and its metabolite, 2- Parts per Commodity million [2-chloro-4-(methylsulfonyl)-3-[(2,2,2- trifluoroethoxy) methyl]benzoyl]-4,6- Apple ...... 0.2 dihydroxy-1,3-cyclohexanedione, cal- Citrus Oil ...... 10 Fruit, Citrus, Group 10, except Grapefruit ...... 0 .5 culated as the stoichiometric equiva- Pear ...... 0 .2 lent of tembotrione, in or on the following commodities. (b) Section is emergency exempotions. [Reserved] Parts per Commodity million (c) Tolerances with regional registration. [Reserved] Cattle, liver ...... 0 .40 (d) Indirect or inadvertent residues. Cattle, meat byproducts, except liver ...... 0 .07 Corn, field, forage ...... 0 .60 [Reserved] Corn, field, grain ...... 0 .02 Corn, field, stover ...... 0 .45 [72 FR 44393, Aug. 8, 2007] Corn, pop, grain ...... 0.02 Corn, pop, stover ...... 0.35 § 180.633 Florasulam; tolerances for Corn, sweet, forage ...... 0 .35 residues. Corn, sweet, stover ...... 0 .60 Goat, liver ...... 0.40 (a) General. Tolerances are estab- Goat, meat byproducts, except liver ...... 0 .07 lished for residues of the herbicide Horse, liver ...... 0 .40 florasulam N-(2,6-difluorophenyl)-8- Horse, meat byproducts, except liver ...... 0 .07 Poultry, liver ...... 0 .07 fluoro-5-methoxy(1,2,4)triazolo(1,5- Sheep, liver ...... 0.40 c)pyrimidine-2-sulfonamide in or on Sheep, meat byproducts, except liver ...... 0 .07 the following commodities: (2) Tolerances are established for res- Parts per Commodity million idues of the herbicide tembotrione, including its metabolites and degradates, Barley, grain ...... 0 .01 in or on the commodities listed in the Barley, hay ...... 0 .05 Barley, straw ...... 0 .05 table to this paragraph. Compliance Oat, forage ...... 0 .05 with the tolerance levels specified Oat, grain ...... 0 .01 below is to be determined by measuring Oat, hay ...... 0.05 Oat, straw ...... 0.05 only tembotrione, 2-[2-chloro-4- Rye, forage ...... 0 .05 (methylsulfonyl)-3-[(2,2,2- Rye, grain ...... 0.01 trifluoroethoxy)methyl]benzoyl]-1,3- Rye, straw ...... 0 .05 Wheat, forage ...... 0 .05 cyclohexanedione in or on the fol- Wheat, grain ...... 0 .01 lowing commodities. Wheat, hay ...... 0 .05 Wheat, straw ...... 0 .05 Parts per Commodity million (b) Section 18 emergency exemptions. Corn, sweet, kernel plus cob with husks re- [Reserved] moved ...... 0 .01 (c) Tolerances with regional registrations. [Reserved] (b) Section 18 emergency exemptions. (d) Indirect or inadvertent residues. [Reserved] [Reserved] (c) Tolerances with regional registra- [72 FR 55077, Sept. 28, 2007] tions. [Reserved] (d) Indirect or inadvertent residues. § 180.634 Tembotrione; tolerances for [Reserved] residues. [72 FR 55085, Sept. 28, 2007, as amended at 74 (a) General. (1) Tolerances are estab- FR 47894, Sept. 18, 2009] lished for residues of the herbicide tembotrione, including its metabolites § 180.635 Spinetoram; tolerances for and degradates, in or on the commod- residues. ities listed in the table to this para- (a) General. Tolerances are estab- graph. Compliance with the tolerance lished for the combined residues of the levels specified below is to be deter- insecticide spinetoram, expressed as a mined by measuring only the sum of combination of XDE-175-J: 1-H-as-

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indaceno[3,2-d]oxacyclododecin-7,15- Commodity Parts per dione, 2-[(6-deoxy-3-O-ethyl-2,4-di-O- million methyl-a-L-mannopyranosyl) oxy]-13- Corn, sweet, kernel plus cob with husks re- [[(2R,5S,6R)-5- moved ...... 0 .04 (dimethylamino)tetrahydro-6-methyl- Cotton, gin byproducts ...... 1 .5 Cotton, undelinted seed ...... 0 .04 2H-pyran-2-yl] oxy]-9-ethyl- Cranberry ...... 0 .04 2,3,3a,4,5,5a,5b,6,9, 10,11,12,13,14,16a,16b- Custard apple ...... 0 .30 hexadecahydro 14-methyl-, Date ...... 0 .10 Egg ...... 0 .04 (2R,3aR,5aR,5bS,9S, 13S,14R,16aS,16bR); Feijoa ...... 0 .30 XDE-175-L: 1H-as-indaceno[3,2- Fig ...... 0 .10 d]oxacyclododecin-7,15-dione, 2-[(6- Fruit, citrus, group 10 ...... 0 .30 deoxy-3-O- ethyl-2,4-di-O-methyl-a-L- Fruit, pome, group 11 ...... 0.20 Fruit, stone, group 12 ...... 0 .20 mannopyranosyl)oxy]-13-[[(2R,5S,6R)-5- Goat, fat ...... 5 .5 (dimethylamino)tetrahydro-6-methyl- Goat, liver ...... 0.85 2H-pyran-2-yl]oxy]-9-ethyl- Goat, meat ...... 0.20 Goat, meat byproducts (except liver) ...... 0.60 2,3,3a,5a,5b,6,9, 10,11,12,13,14,16a,16b- Grain, aspirated fractions ...... 20 tetradecahydro-4,14-dimethyl-, Grain, cereal, group 15, except rice, sorghum, (2S,3aR,5aS,5bS,9S, 13S,14R,16aS,16bS); pearl millet and proso millet ...... 0 .04 Grain, cereal, group 16, forage ...... 3 .5 ND-J: (2R,3aR,5aR,5bS,9S, Grain, cereal, group 16, hay ...... 10 13S,14R,16aS,16bR)-9-ethyl-14-methyl- Grain, cereal, group 16, stover ...... 10 13-[[(2S,5S,6R)-6- methyl-5- Grain, cereal, straw, group 16, except rice ...... 1 .0 (methylamino)tetrahydro- 2H-pyran-2- Grape ...... 0 .50 Grape, raisin ...... 0 .70 yl]oxy]-7,15-dioxo-2,3,3a,4,5,5a,5b,6,7,9, Guava ...... 0 .30 10,11,12,13,14,15,16a,16b- octadecahydro- Herb, dried, subgroup 19A ...... 22 1H-as- indaceno[3,2-d]oxacyclododecin- Herb, fresh, subgroup 19A ...... 3 .0 Hog, fat ...... 0 .40 2-yl 6-deoxy-3-O-ethyl-2,4-di-O-methyl- Hog, meat ...... 0 .04 alpha-L-mannopyranoside; and NF-J: Hog, meat byproducts ...... 0 .04 (2R,3S,6S)-6-([(2R,3aR,5aR,5bS,9S, Hop, dried cones ...... 22 13S,14R,16aS,16bR)- 2-[(6-deoxy-3-O- Horse, fat ...... 5 .5 Horse, liver ...... 0 .85 ethyl-2,4-di-O- methyl-alpha-L- Horse, meat ...... 0 .20 mannopyranosyl) oxy]-9-ethyl-14-meth- Horse, meat byproducts (except liver) ...... 0 .60 yl-7,15-dioxo-2, 3,3a,4,5,5a,5b,6,7,9, Ilama ...... 0 .30 Jaboticaba ...... 0 .30 10,11,12,13,14,15,16a,16b- octadecahydro- Juneberry ...... 0 .25 1H-as- indaceno[3,2-d]oxacyclododecin- Lingonberry ...... 0.25 13-yl] oxy)-2-methyltetrahydro- 2H- Longan ...... 0 .30 pyran-3-yl(methyl)formamide, in or on Lychee ...... 0 .30 Mango ...... 0.30 the following raw agricultural com- Milk ...... 0.30 modities: Milk, fat ...... 7 .5 Millet, pearl, grain ...... 1 .0 Millet, proso, grain ...... 1 .0 Commodity Parts per million Nut, tree, group 14 ...... 0 .10 Okra ...... 0.40 Acerola ...... 0.30 Onion, green ...... 2 .0 Almond, hulls ...... 19 Papaya ...... 0 .30 Amaranth grain, grain ...... 1 .0 Passionfruit ...... 0 .30 Apple, wet pomace ...... 0 .50 Pea and bean, dried shelled, except soybean, Artichoke, globe ...... 0.30 subgroup 6C ...... 0 .04 Asparagus ...... 0.04 Pea and bean, succulent shelled, subgroup 6B 0 .04 Atemoya ...... 0 .30 Peanut ...... 0 .04 Avocado ...... 0 .30 Peanut, hay ...... 11 Banana ...... 0.25 Peppermint, tops ...... 3 .5 Beet, sugar, molasses ...... 0 .75 Pineapple ...... 0.04 Biriba ...... 0 .30 Pineapple, processed residue ...... 0 .15 Brassica, head and stem, subgroup 5A ...... 2 .0 Pistachio ...... 0.10 Brassica, leafy greens, subgroup 5B ...... 10 Pomegranate ...... 0 .30 Bushberry, subgroup 13B ...... 0 .25 Poultry, fat ...... 0.10 Caneberry, subgroup 13A ...... 0.70 Poultry, meat ...... 0 .04 Canistel ...... 0 .30 Poultry, meat byproducts ...... 0.04 Cattle, fat ...... 5.5 Pulasan ...... 0 .30 Cattle, liver ...... 0 .85 Rambutan ...... 0 .30 Cattle, meat ...... 0 .20 Salal ...... 0 .25 Cattle, meat byproducts (except liver) ...... 0 .60 Sapodilla ...... 0 .30 Cherimoya ...... 0 .30 Sapote, black ...... 0 .30 Citrus, dried pulp ...... 0 .50 Sapote, mamey ...... 0 .30 Citrus, oil ...... 3.0 Sapote, white ...... 0 .30

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(d) Indirect or inadvertent residues. Commodity Parts per million [Reserved] Sheep, fat ...... 5 .5 [73 FR 8218, Feb. 13, 2008] Sheep, liver ...... 0.85 Sheep, meat ...... 0.20 § 180.637 Mandipropamid; tolerances Sheep, meat products (except liver) ...... 0 .60 for residues. Sorghum, grain, grain ...... 1 .0 Soursop ...... 0 .30 (a) General. Tolerances are estab- Soybean, seed ...... 0 .04 lished for residues of mandipropamid, Spanish lime ...... 0 .30 including its metabolites and Spearmint, tops ...... 3 .5 Spice, subgroup 19B, except black pepper ...... 1 .7 degradates, in or on the commodities Star apple ...... 0 .30 listed in the table below. Compliance Star fruit ...... 0 .30 with the tolerance levels specified Strawberry ...... 1 .0 below is to be determined by measuring Sugar apple ...... 0 .30 only mandipropamid (4-chloro-N-[2-[3- Ti, leaves ...... 10 Vegetable, bulb, group 3, except green onion .... 0.10 methoxy-4-(2- Vegetable, cucurbit, group 9 ...... 0.30 propynyloxy)phenyl]ethyl]-a-(2- Vegetable, foliage of legume, group 7 ...... 8 .0 propynyloxy)benzeneacetamide) in or Vegetable, fruiting, group 8 ...... 0.40 on the commodity. Vegetable, leafy, except Brassica, group 4 ...... 8 .0 Vegetable, leaves of root and tuber, group 2 ..... 10 Parts per Vegetable, legume, edible podded, subgroup 6A 0 .30 Commodity million Vegetable, root and tuber, group 1 ...... 0 .10 Watercress ...... 8 .0 Basil, dried leaves ...... 200 Wax jambu ...... 0 .30 Basil, fresh leaves ...... 30 Bean, snap ...... 0 .90 Brassica, head and stem, subgroup 5A ...... 3 (b) Section 18 emergency exemptions. Brassica, leafy greens, subgroup 5B ...... 25 [Reserved] Fruit, small vine climbing, except fuzzy kiwifruit, (c) Tolerances with regional registra- subgroup 13–07F ...... 1 .4 Ginseng ...... 0 .30 tion. [Reserved] Grape, raisin ...... 3 .0 (d) Indirect and invertent residues. [Re- Hop, dried cones ...... 50 served] Onion, bulb, subgroup 3–07A ...... 0 .05 Onion, green, subgroup 3–07B ...... 4 .0 [72 FR 57499, Oct. 10, 2007, as amended at 73 Potato, wet peel ...... 0 .03 FR 14714, Mar. 19, 2008; 74 FR 40759, Aug. 13, Vegetable, cucurbit, group 9 ...... 0.6 Vegetable, fruiting, group 8–10 ...... 1 .0 2009] Vegetable, leafy except Brassica, group 4 ...... 20 Vegetable, tuberous and corm, subgroup 1C ..... 0.01 § 180.636 1,3-dichloropropene; tolerances for residues. (b) Section 18 emergency exemptions. (a) General. Tolerances are estab- Time-limited tolerances are established for the combined residues of the lished for residues of mandipropamid, fungicide cis- and trans-1,3- including its metabolites and dichloropropene and its metabolites degradates, in or on the commodities cis- and trans-3-chloroacrylic acid, and listed in the table below resulting from cis- and trans-3-chloroallyl alcohol in or use of the pesticide pursuant to on the following commodities. FFIFRA section 18 emergency exemptions. Compliance with the tolerance Parts per levels specified below is to be deter- Commodity million mined by measuring only Grape ...... 0.018 mandipropamid (4-chloro-N-[2-[3- methoxy-4-(2- (b) Section 18 emergency exemptions. propynyloxy)phenyl]ethyl]-a-(2- [Reserved] propynyloxy)benzeneacetamide) in or (c) Tolerances with regional registra- on the commodity. The tolerances ex- tions. [Reserved] pire on the date specified in the table.

Parts per Expiration/revocation Commodity million date

Basil, dried ...... 240 12/31/15

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(c) Tolerances with regional registra- Commodity Parts per tions. [Reserved] million (d) Indirect or inadvertent tolerances. Corn, sweet, kernel plus cob with husks re- [Reserved] moved ...... 0 .01 Corn, sweet, stover ...... 25 [73 FR 2816, Jan. 16, 2008, as amended at 74 Cotton gin byproducts ...... 60 FR 33169, July 10, 2009; 76 FR 55804, Sept. 9, Cotton, undelinted seed ...... 0 .90 2011; 77 FR 74119, Dec. 13, 2012; 78 FR 76992, Fruit, pome, group 11 ...... 1.5 Dec. 20, 2013] Fruit, stone, group 12 ...... 1 .6 Grape ...... 1 .4 Nut, tree, group 14 ...... 0 .06 § 180.638 Pyroxsulam; tolerances for Okra ...... 0.30 residues. Vegetable, cucurbit, group 9 ...... 0.20 Vegetable, fruiting, group 8 ...... 0.60 (a) General. Tolerances are estab- Vegetable, leafy, except Brassica, group 4 ...... 11 lished for residues of the herbicide pyroxsulam, N-(5,7- (2) Tolerances are established for res- dimethoxy[1,2,4]triazolo[1,5- idues of flubendiamide, including its a]pyrimidin-2-yl)-2-methoxy-4- metabolites and degradates, in or on (trifluoromethyl)-3- the commodities in the table below. pyridinesulfonamide in or on the raw Compliance with the tolerance levels agricultural commodities: specified in the table is to be determined by measuring only Parts per 2 Commodity million flubendiamide N -[1,1-dimethyl-2- (methylsulfonyl)ethyl]-3-iodo-N1-[2- Wheat, forage ...... 0 .06 methyl-4-[1,2,2,2-tetrafluoro-1- Wheat, grain ...... 0 .01 Wheat, hay ...... 0 .01 (trifluoromethyl)ethyl]phenyl]-1,2- Wheat, straw ...... 0 .03 benzenedicarboxamide, in or on the following commodities: (b) Section 18 emergency exemptions. Parts per [Reserved] Commodity million (c) Tolerances with regional registrations. [Reserved] Alfalfa, forage ...... 25 Alfalfa, hay ...... 65 (d) Indirect or inadvertent residues. Artichoke, globe ...... 1.6 [Reserved] Berry, low growing, subgroup 13–07G, except cranberry ...... 1.5 [73 FR 10402, Feb. 27, 2008] Brassica, head and stem, subgroup 5A ...... 3 .0 Brassica, leafy greens, subgroup 5B ...... 25 § 180.639 Flubendiamide; tolerances Cattle, fat ...... 0.70 Cattle, meat ...... 0 .08 for residues. Cattle, meat byproducts ...... 0.60 (a) General. (1) Tolerances are estab- Egg ...... 0 .40 Fruit, small fruit vine climbing except fuzzy lished for residues of flubendiamide, in- kiwifruit, subgroup 13–07F ...... 1 .4 cluding its metabolites and degradates, Goat, fat ...... 0 .70 in or on the commodities in the table Goat, meat ...... 0.08 below. Compliance with the tolerance Goat, meat byproducts ...... 0 .60 Grain, aspirated grain fractions ...... 153 levels specified in the table is to be de- Hog, fat ...... 0 .15 termined by measuring only Hog, meat ...... 0 .03 flubendiamide N2-[1, 1-dimethyl-2- Hog, meat byproducts ...... 0 .15 1 Horse, fat ...... 0 .70 (methylsulfonyl)ethyl]-3-iodo-N -[2- Horse, meat ...... 0 .08 methyl-4- [1,2,2,2-tetrafluoro-1- Horse, meat byproducts ...... 0 .60 (trifluoromethyl)ethyl]phenyl]-1,2- Milk ...... 0.15 Milk, fat ...... 1 .0 benzenedicarboxamide, in or on the fol- Pea and bean, dried shelled, except soybean, lowing commodities: subgroup 6C ...... 0 .60 Pea and bean, succulent shelled, subgroup 6B 0 .05 Commodity Parts per Peanut, hay ...... 60 million Peanut, meal ...... 0 .03 Peanut, nutmeat ...... 0 .02 Almond, hulls ...... 9 .0 Peanut, refined oil ...... 0.03 Apple, wet pomace ...... 5 .0 Pistachio ...... 0.06 Corn, field, forage ...... 8 .0 Poultry, fat ...... 3.0 Corn, field, grain ...... 0 .03 Poultry, liver ...... 0 .60 Corn, field, stover ...... 15 Poultry, meat ...... 0 .10 Corn, pop, grain ...... 0.02 Rice, grain 1 ...... 0 .50 Corn, pop, stover ...... 15 Safflower, seed ...... 5 .0 Corn, sweet, forage ...... 9 .0 Sheep, fat ...... 0 .70

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Parts per [76 FR 16307, Mar. 23, 2011, as amended at 76 Commodity million FR 55273, Sept. 7, 2011; 77 FR 73945, Dec. 12, 2012] Sheep, meat ...... 0.08 Sheep, meat byproducts ...... 0 .60 Sorghum, grain, forage ...... 12 § 180.640 Pyridalyl; tolerances for resi- Sorghum, grain, grain ...... 5 .0 dues. Sorghum, grain, stover ...... 14 (a) General. Tolerances are estab- Soybean, forage ...... 18 lished for residues of pyridalyl, pyri- Soybean, hay ...... 60 Soybean, hulls ...... 0 .80 dine,2-[3-[2,6-dichloro-4-[(3,3-dichloro-2- Soybean, seed ...... 0 .25 propenyl)oxy]phenoxy]propoxy]-5- Sugarcane, cane ...... 0.30 (trifluoromethyl, in or on the following Sunflower, seed ...... 5.0 raw agricultural commodities:) Turnip, greens ...... 25 Vegetable, foliage of legume, except soybean, Parts per subgroup 7A ...... 35 Commodity million Vegetable, legume, edible podded, subgroup 6A ...... 0 .50 Brassica, head and stem, subgroup 5A ...... 3 .5 Mustard greens ...... 30 1 There are no U.S. registrations for rice, grain. Turnip greens ...... 30 (b) Section 18 emergency exemptions. Vegetable, fruiting, group 8 ...... 1.0 Vegetables, leafy, except Brassica, group 4 ...... 20 [Reserved] (c) Tolerances with regional registra- (b) Section 18 emergency exemptions. tions. [Reserved] [Reserved] (d) Indirect or inadvertent residues. (c) Tolerances with regional registra- Tolerances are established for residues tions. [Reserved] of flubendiamide, including its metabo- (d) Indirect or inadvertent residues. lites and degradates, in or on the com- [Reserved] modities in the table below. Compli- ance with the tolerance levels specified [73 FR 25533, May 7, 2008] in the table is to be determined by § 180.641 Spirotetramat; tolerances for measuring only flubendiamide N2-[1, 1- residues. dimethyl-2-(methylsulfonyl)ethyl]-3- (a) General. (1) Tolerances are estab- iodo-N1-[2-methyl-4- [1,2,2,2- lished for residues of the insecticide tetrafluoro-1- spirotetramat, including its metabo- (trifluoromethyl)ethyl]phenyl]-1, 2- lites and degradates, in or on the com- benzenedicarboxamide, in or on the fol- modities in the table below. Compli- lowing commodities: ance with the tolerance levels specified Parts per below is to be determined by measuring Commodity million only the sum of spirotetramat (cis-3- Barley, hay ...... 0 .04 (2,5-dimethlyphenyl)-8-methoxy-2-oxo- Barley, straw ...... 0 .07 1-azaspiro[4.5]dec-3-en-4-yl-ethyl car- Buckwheat ...... 0 .07 bonate) and its metabolites cis-3-(2,5- Clover, forage ...... 0.15 dimethylphenyl)-4-hydroxy-8-methoxy- Clover, hay ...... 0.04 1-azaspiro[4.5]dec-3-en-2-one, cis-3-(2,5- Grass, forage ...... 0 .15 Grass, hay ...... 0 .04 dimethylphenyl)-3-hydroxy-8-methoxy- Millet, pearl, forage ...... 0 .15 1-azaspiro[4.5]decane-2,4-dione, cis-3- Millet, pearl, hay ...... 0.04 (2,5-dimethylphenyl)-8-methoxy-2-oxo- Millet, proso, forage ...... 0 .15 1-azaspiro[4.5]dec-3-en-4-yl beta-D-glu- Millet, proso, hay ...... 0 .04 Millet, proso, straw ...... 0 .07 copyranoside, and cis-3-(2,5- Oats, forage ...... 0 .15 dimethylphenyl)-4-hydroxy-8-methoxy- Oats, hay ...... 0.04 1-azaspiro[4.5]decan-2-one, calculated Oats, straw ...... 0.07 Rye, forage ...... 0 .15 as the stoichiometric equivalent of Rye, straw ...... 0 .07 spirotetramat, in or on the following Teosinte, forage ...... 0 .15 commodities. Teosinte, hay ...... 0 .04 Teosinte, straw ...... 0.07 Commodity Parts per Triticale, forage ...... 0 .15 million Triticale, hay ...... 0 .04 Triticale, straw ...... 0 .07 Acerola ...... 2.5 Wheat, forage ...... 0 .15 Almond, hulls ...... 9 .0 Wheat, hay ...... 0 .03 Artichoke, globe ...... 1.5 Wheat, straw ...... 0 .03 Aspirated grain fractions ...... 10 .0 Avocado ...... 0 .60

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bonate]) and its metabolite cis-3-(2,5- Commodity Parts per million dimethylphenyl)-4-hydroxy-8-methoxy- Berry, low growing, except strawberry, subgroup 1-azaspiro[4.5]dec-3-en-2-one, calculated 13–07H ...... 0 .30 as the stoichiometric equivalent of Black sapote ...... 0 .60 Brassica, head and stem, subgroup 5A ...... 2 .5 spirotetramat, in or on the following Brassica, leafy, subgroup 5B ...... 8 .0 commodities: Bushberry subgroup 13–07B ...... 3 .0 Canistel ...... 0 .60 Parts per Citrus, oil ...... 6.0 Commodity million Coffee, green bean ...... 0 .20 Coffee, instant ...... 0 .50 Cattle, fat ...... 0.02 Corn, sweet, kernel plus cob with husks re- Cattle, meat ...... 0 .02 moved ...... 1 .5 Cattle, meat byproducts ...... 0.20 Cotton gin byproducts1 ...... 10 .0 Cotton, undelinted seed1 ...... 0 .30 Eggs ...... 0 .02 Feijoa ...... 2 .5 Goat, fat ...... 0 .02 Fruit, citrus, group 10–10 ...... 0 .60 Goat, meat ...... 0.02 Fruit, pome, group 11–10 ...... 0 .70 Goat, meat byproducts ...... 0 .20 Fruit, stone, group 12 ...... 4 .5 Hog, meat byproducts ...... 0 .02 Grape, raisin ...... 3 .0 Horse, fat ...... 0 .02 Guava ...... 2 .5 Horse, meat ...... 0 .02 Hop, dried cones ...... 10 .0 Jaboticaba ...... 2 .5 Horse, meat byproducts ...... 0 .20 Longan ...... 13 .0 Milk ...... 0.01 Lychee ...... 13.0 Poultry, meat byproducts ...... 0.02 Mamey sapote ...... 0 .60 Sheep, fat ...... 0 .02 Mango ...... 0.60 Sheep, meat ...... 0.02 Nut, tree, group 14 ...... 0 .25 Sheep, meat byproducts ...... 0 .20 Papaya ...... 0 .40 Passionfruit ...... 2 .5 Persimmon ...... 2 .5 (b) Section 18 emergency exemptions. Pineapple ...... 0.30 [Reserved] Pistachio ...... 0.25 Pomegranate ...... 0 .50 (c) Tolerances with regional registra- Potato, flakes ...... 1 .6 tions. Tolerances with regional reg- Pulasan ...... 13 .0 istrations are established for residues Rambutan ...... 13 .0 Sapodilla ...... 0 .60 of the insecticide spirotetramat, in- Small fruit vine climbing subgroup, except fuzzy cluding its metabolites and degradates, kiwifruit, subgroup 13–07F ...... 1.3 in or on the commodities in the table Soybean forage ...... 8.0 Soybean hay ...... 16.0 below. Compliance with the tolerance Soybean seed ...... 5 .0 levels specified below is to be deter- Spanish lime ...... 13 Star apple ...... 0 .60 mined by measuring only the sum of Starfruit ...... 2 .5 spirotetramat (cis-3-(2,5- Strawberry1 ...... 0 .40 dimethlyphenyl)-8-methoxy-2-oxo-1- Taro, leaves ...... 9 .0 Vegetable, bulb, group 3–07 ...... 0 .80 azaspiro[4.5]dec-3-en-4-yl-ethyl car- Vegetable, cucurbit, group 9 ...... 0.30 bonate) and its metabolites cis-3-(2,5- Vegetable, foliage of legume, except soybean, dimethylphenyl)-4-hydroxy-8-methoxy- subgroup 07A ...... 7 .0 Vegetable, fruiting, group 8–10 ...... 2 .5 1-azaspiro[4.5]dec-3-en-2-one, cis-3-(2,5- Vegetable, leafy, except brassica, group 4 ...... 9 .0 dimethylphenyl)-3-hydroxy-8-methoxy- Vegetable, legume, group 06, except soybean .. 2 .5 1-azaspiro[4.5]decane-2,4-dione, cis-3- Vegetable, tuberous and corm, subgroup 1C ..... 0.60 Watercress ...... 2 .0 (2,5-dimethylphenyl)-8-methoxy-2-oxo- Wax jambu ...... 2 .5 1-azaspiro[4.5]dec-3-en-4-yl beta-D-glu- White sapote ...... 0 .60 copyranoside, and cis-3-(2,5- 1 Import tolerance only. There are no U.S. registrations for dimethylphenyl)-4-hydroxy-8-methoxy- cotton or strawberry. 1-azaspiro[4.5]decan-2-one, calculated (2) Tolerances are also established for as the stoichiometric equivalent of residues of the insecticide spirotetramat, in or on the following spirotetramat, including its metabo- commodities. lites and degradates, in or on the commodities in the table below. Compli- Parts per Commodity ance with the tolerance levels specified million below is to be determined by measuring Banana ...... 4.0 only the sum of spirotetramat (cis-3- (2,5-dimethlyphenyl)-8-methoxy-2-oxo- 1-azaspiro[4.5]dec-3-en-4-yl-ethyl car-

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(d) Indirect or inadvertant residues. safener cyprosulfamide, N-[[4- [Reserved] [(cyclopropylamino)carbonyl] phenyl]sulfonyl]-2-methoxybenzamide, [73 FR 39256, July 9, 2008, as amended at 76 FR 28681, May 18, 2011; 77 FR 8746, Feb. 15, in or on the following raw agricultural 2012; 77 FR 75859, Dec. 26, 2012; 78 FR 28512, commodities: May 15, 2013; 78 FR 66651, Nov. 6, 2013] Parts per Commodity million § 180.642 Gentamicin; tolerances for residues. Corn, field, forage ...... 0 .20 Corn, field, grain ...... 0 .01 (a) General. [Reserved] Corn, field, stover ...... 0 .20 (b) Section 18 emergency exemptions. Corn, pop, grain ...... 0.01 Time-limited tolerances specified in Corn, pop, stover ...... 0.20 Corn, sweet, forage ...... 0 .40 the following table are established for Corn, sweet, kernel plus cob with husks re- residues of gentamicin in or on the moved ...... 0 .01 specified agricultural commodities, re- Corn, sweet, stover ...... 0 .35 sulting from use of the pesticide pursu- (2) Tolerances are established for res- ant to FIFRA section 18 emergency ex- idues of the herbicide safener emptions. The tolerances expire and cyprosulfamide, N-[[4- are revoked on the date specified in the [(cyclopropylamino)carbonyl] following table. phenyl]sulfonyl]-2-methoxybenzamide, and its metabolite 4-(aminosulfonyl)-N- Parts per Expiration/ Commodity revocation cyclopropylbenzamide, calculated as million date cyprosulfamide, in or on the following Apple ...... 0.10 12/31/10 raw agricultural commodities:

(c) Tolerance with regional restrictions. Parts per Commodity million [Reserved] (d) Indirect or inadvertant residues. Cattle, meat byproducts ...... 0.02 [Reserved] Goat, meat byproducts ...... 0 .02 Horse, meat byproducts ...... 0 .02 [73 FR 44162, July 30, 2008] Sheep, meat byproducts ...... 0 .02

§ 180.643 Uniconazole; tolerances for (b) Section 18 emergency exemptions. residues. [Reserved] (a) General. Tolerances are estab- (c) Tolerances with regional registra- lished for residues of the fungicide/ tions. [Reserved] plant growth regulator uniconazole-P, (d) Indirect or inadvertant residues. (E)-(S)-1-(4-chlorophenyl)-4,4-dimethyl- [Reserved] 2-(1H-1,2,4-triazol-1-yl)pent-1-en-3-ol, [73 FR 60974, Oct. 15, 2008] its R-enantiomer and its Z-isomer in or on the following raw agricultural com- § 180.645 Thiencarbazone-methyl; tol- modities: erances for residues. (a) General. (1) Tolerances are estab- Parts per Commodity million lished for residues of thiencarbazone- methyl [methyl 4-[[[(4,5-dihydro-3- Vegetable, fruiting, group 8 ...... 0.01 methoxy-4-methyl-5-oxo-1H-1,2,4- triazol-1-yl)-carbonyl]amino]sulfonyl]- (b) Section 18 emergency exemptions. 5-methyl-3-thiophenecarboxylate], per [Reserved] se, in or on the following food and feed (c) Tolerances with regional registra- commodities: tions. [Reserved] (d) Indirect or inadvertant residues. Commodity Parts per [Reserved] million [73 FR 51736, Sept. 5, 2008] Corn, field, forage ...... 0 .04 Corn, field, grain ...... 0 .01 Corn, field, stover ...... 0 .02 § 180.644 Cyprosulfamide; tolerances Corn, pop, grain ...... 0.01 for residues. Corn, pop, stover ...... 0.01 Corn, sweet, forage ...... 0 .05 (a) General. (1) Tolerances are estab- Corn, sweet, kernel plus cob with husks re- lished for residues of the herbicide moved ...... 0 .01

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ylmethyl)cyclopentanol) in or on the Commodity Parts per million commodity. Corn, sweet, stover ...... 0 .05 Parts per Wheat, forage ...... 0 .10 Commodity million Wheat, grain ...... 0 .01 Wheat, hay ...... 0 .01 Cotton, gin byproducts ...... 0 .01 Wheat, straw ...... 0 .01 Cotton, undelinted seed ...... 0 .01 Grain, cereal, forage, fodder and straw, group (2) Tolerances are established for 16, except rice ...... 0 .01 Grain, cereal group 15, except rice ...... 0.01 combined residues of thiencarbazone- Peanut ...... 0 .01 methyl and its metabolite BYH 18636- Soybean, forage ...... 0 .01 MMT [5-methoxy-4-methyl-2,4-dihydro- Vegetable, legume, group 6 ...... 0 .01 3H-1,2,4-triazol-3-one], calculated as the parent compound, in or on the fol- (b) Section 18 emergency exemptions. lowing food commodities of animal ori- [Reserved] gin: (c) Tolerances with regional registrations. [Reserved] Commodity Parts per (d) Indirect or inadvertent residues. million [Reserved] Cattle, meat ...... 0 .02 [73 FR 69559, Nov. 19, 2008, as amended at 79 Cattle, meat byproducts ...... 0.02 FR 15240, Mar. 19, 2014] Goat, meat ...... 0.02 Goat, meat byproducts ...... 0 .02 Horse, meat ...... 0 .02 § 180.647 d-Phenothrin; tolerances for Horse, meat byproducts ...... 0 .02 residues. Milk ...... 0.02 (a) General. A tolerance of 0.01 parts Sheep, meat ...... 0.02 per million is established for residues Sheep, meat byproducts ...... 0 .02 of the insecticide d-phenothrin in or on (b) Section 18 emergency exemptions. all food/feed crops following wide-area [Reserved] mosquito adulticide applications. (c) Tolerances with regional registra- (b) Section 18 emergency exemptions. tions. [Reserved] [Reserved] (c) Tolerances with regional registra- (d) Indirect or inadvertent residues. tions. [Reserved] Tolerances are established for indirect (d) Indirect or inadvertent residues. or inadvertent combined residues of [Reserved] thiencarbazone-methyl and its metabolite BYH 18636-MMT-glucoside [2- [74 FR 32443, July 8, 2009] hexopyranosyl-5-methoxy-4-methyl-2,4- dihydro-3H-1,2,4-triazol-3-one], cal- § 180.648 Meptyldinocap; tolerances culated as the parent compound, in or for residues. on the following food commodities: (a) General. Tolerances are established for the combined residues of the Parts per Commodity million fungicide meptyldinocap, 2-(1- methylheptyl)-4,6-dinitrophenyl (2E)-2- Soybean, forage ...... 0 .04 butenoate and 2,4-DNOP, 2,4-dinitro-6- Soybean, hay ...... 0 .15 (1-methylheptyl)phenol expressed as meptyldinocap in or on the following [73 FR 60968, Oct. 15, 2008] commodities:

§ 180.646 Ipconazole; tolerances for Commodity Parts Per Mil- residues. lion (a) General. Tolerances are estab- Grape ...... 0.20 lished for residues of ipconazole, including its metabolites and degradates, (b) Section 18 emergency exemptions. in or on the commodities listed in the [Reserved] table below. Compliance with the toler- (c) Tolerances with regional registra- ance levels specified below is to be de- tions. [Reserved] termined by measuring only ipconazole (d) Indirect or inadvertent residues. (2-[(4-chlorophenyl)methyl]-5-(1- [Reserved] methylethyl)-1-(1H-1,2,4-triazol-1- [74 FR 48396, Sept. 23, 2009]

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§ 180.649 Saflufenacil; tolerances for fluoro-N-[[methyl(1-methylethyl) residues. amino]sulfonyl]benzamide, in or on the (a) General. (1) Tolerances are estab- commodities. lished for residues of saflufenacil, in- Parts per cluding its metabolites and degradates, Commodity million in or on the commodities in the table Cattle, fat ...... 0.01 below. Compliance with the tolerance Cattle, liver ...... 2 .5 levels specified below is to be deter- Cattle, meat ...... 0 .01 mined by measuring only the sum of Cattle, meat byproducts, except liver ...... 0 .05 Fish-freshwater finfish ...... 0.01 saflufenacil, 2-chloro-5-[3,6-dihydro-3- Fish-shellfish, crustacean ...... 0 .01 methyl-2,6-dioxo-4-(trifluoromethyl)- Goat, fat ...... 0 .01 1(2H)-pyrimidinyl]-4-fluoro-N-[[methyl Goat, liver ...... 2.5 (1-methylethyl)amino]sulfonyl]benz- Goat, meat ...... 0.01 Goat, meat byproducts, except liver ...... 0 .05 amide, and its metabolites N-[2-chloro- Hog, fat ...... 0 .01 5-(2,6-dioxo-4-(trifluoromethyl)-3,6- Hog, liver ...... 0 .80 dihydro-1(2H)-pyrimidinyl)-4- Hog, meat ...... 0 .01 ′ Hog, meat byproducts, except liver ...... 0 .02 fluorobenzoyl]-N -isopropylsulfamide Horse, fat ...... 0 .01 and N-[4-chloro-2-fluoro-5- Horse, liver ...... 2 .5 ({[(isopropylamino)sulfonyl] Horse, meat ...... 0 .01 amino}carbonyl)phenyl]urea, cal- Horse, meat byproducts, except liver ...... 0 .05 Milk ...... 0.01 culated as the stoichiometric equiva- Sheep, fat ...... 0 .01 lent of saflufenacil, in or on the com- Sheep, liver ...... 2.5 modities. Sheep, meat ...... 0.01 Sheep, meat byproducts, except liver ...... 0 .05 Parts per Commodity million (b) Section 18 emergency exemptions. Almond, hulls ...... 0 .10 [Reserved] Banana 1 ...... 0.03 (c) Tolerances with regional registra- Coffee, green bean 1 ...... 0 .03 tions. [Reserved] Cotton, gin byproducts ...... 0 .45 Cottonseed subgroup 20C ...... 0 .20 (d) Indirect or inadvertent residues. Fruit, citrus, group 10 ...... 0 .03 [Reserved] Fruit, pome, group 11 ...... 0.03 Fruit, stone, group 12 ...... 0 .03 [74 FR 46689, Sept. 11, 2009, as amended at 76 Grain, aspirated fractions ...... 10 FR 27261, May 11, 2011; 76 FR 76309, Dec. 7, Grain, cereal, forage, fodder and straw group 16 0 .10 2011; 79 FR 9866, Feb. 21, 2014] Grain, cereal, group 15 ...... 0.03 Grape ...... 0 .03 § 180.650 Isoxaben; tolerances for resi- Mango 1 ...... 0.03 Nut, tree, group 14 ...... 0 .03 dues. Pea and bean, dried shelled, except soybean, (a) General. Tolerances are estab- subgroup 6C ...... 0 .30 Pea and bean, succulent shelled, subgroup 6B 0 .03 lished for residues of the herbicide Pea, hay ...... 17 isoxaben, including its metabolites and Pistachio ...... 0.03 degradates, in or on the commodities Rapeseed subgroup 20A ...... 0 .45 Soybean, hulls ...... 0 .50 in the table below. Compliance with Soybean, seed ...... 0 .10 the tolerance levels specified below is Sugarcane, cane 2 ...... 0.05 to be determined by measuring only Sugarcane, molasses 2 ...... 0 .08 isoxaben, N-[3-(1-ethyl-1- Sunflower subgroup 20B ...... 1.0 Vegetable, foliage of legume, group 7 (except methylpropyl)-5-isoxazolyl]-2, 6- pea, hay) ...... 0.10 dimethoxybenzamide, in or on the com- Vegetable, legume, edible podded, subgroup 6A 0 .03 modity. 1 No U.S. registration as of December 7, 2011. 2 No U.S. registration as of February 21, 2014. Parts per Commodity million (2) Tolerances are established for residues of saflufenacil, including its me- Almond, hulls ...... 0 .40 Grape ...... 0 .01 tabolites and degradates, in or on the Nut, tree, Group 14 ...... 0.02 commodities in the table below. Com- Pistachio ...... 0.02 pliance with the tolerance levels specified below is to be determined by meas- (b) Section 18 emergency exemptions. uring only saflufenacil, 2-chloro-5-[3,6- [Reserved] dihydro-3-methyl-2,6-dioxo-4- (c) Tolerances with regional registra- (trifluoromethyl)-1(2H)-pyrimidinyl]-4- tions. [Reserved]

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(d) Indirect or inadvertent residues. (c) Tolerances with regional registra- [Reserved] tions. [Reserved] (d) Indirect or inadvertent residues. [75 FR 69360, Nov. 12, 2010] [Reserved] § 180.651 Imazosulfuron; tolerances for [76 FR 18921, Apr. 6, 2011] residues. (a) General. Tolerances are estab- § 180.653 Indaziflam; tolerances for lished for residues of the herbicide residues. imazosulfuron, including its metabo- (a) General. Tolerances are estab- lites and degradates, in or on the fol- lished for residues of the herbicide lowing commodities. Compliance with indaziflam, N-[(1R,2S)-2,3-dihydro-2,6- the tolerance levels specified in the fol- dimethyl-1H-inden-1-yl]-6-(1- lowing table below is to be determined fluoroethyl)-1,3,5-triazine-2,4-diamine, by measuring only imazosulfuron, 2- including its metabolites and chloro-N-[[(4,6-dimethoxy-2- degradates, in or on the commodities pyrimidinyl)amino]carbonyl]imidazo- in the following table. Compliance with [1,2-a]pyridine-3-sulfonamide, in or on the tolerance levels specified in the the commodity. table below is to be determined by measuring only indaziflam, in or on the Parts per commodity. Commodity million Parts per Melon subgroup 9A ...... 0 .02 Commodity million Pepper, bell ...... 0 .02 Pepper, non-bell ...... 0.02 Almond, hulls ...... 0 .15 Rice, grain ...... 0 .02 Banana 1 ...... 0.01 Tomato ...... 0.02 Coffee, green bean 1 ...... 0 .01 Vegetable, tuberous and corm, subgroup 1C ..... 0.02 Fruit, citrus, group 10–10 ...... 0 .01 Fruit, pome, group 11–10 ...... 0 .01 (b) Section 18 emergency exemptions. Fruit, stone, group 12 ...... 0 .01 Grape ...... 0 .01 [Reserved] Nut, tree, group 14 ...... 0 .01 (c) Tolerances with regional registra- Olive ...... 0 .01 tions. [Reserved] Palm, oil 1 ...... 0 .03 Pistachio ...... 0.01 (d) Indirect or inadvertent residues. Sugarcane, refined sugar 1 ...... 0 .01 [Reserved] 1 No U.S. Registrations as of 12/02/2013. 2 Tolerance without a corresponding U.S. registration. [75 FR 81884, Dec. 29, 2010, as amended at 78 FR 44444, July 24, 2013] (b) Section 18 emergency exemptions. [Reserved] § 180.652 Ethiprole; tolerances for resi- (c) Tolerances with regional registra- dues. tions. [Reserved] (a) General. Tolerances (without U.S. (d) Indirect or inadvertent residues. registrations) are established for resi- [Reserved] dues of the insecticide ethiprole, in- [76 FR 18905, Apr. 6, 2011, as amended at 79 cluding its metabolites and degradate, FR 4630, Jan. 29, 2014] in or on the following commodities listed in the table. Compliance with § 180.654 Isopyrazam; tolerances for the tolerance levels specified in the residues. table is to be determined by measuring (a) General. Tolerances are estab- only ethiprole [5-amino-1-[2,6-dichloro- lished for residues of the fungicide 4-(trifluoromethyl)phenyl]-4-[(ethyl)- isopyrazam, including its metabolites sulfinyl]-1H-pyrazole-3-carbonitrile], in and degradates, in or on the commod- or on the following commodities: ities listed in the following table. Com- Parts per pliance with the tolerance levels speci- Commodity million fied in the following table is to be determined by measuring only Rice, grain 1 ...... 1 .7 Tea, dried 1 ...... 30 isopyrazam (3-(difluoromethyl)-1-methyl-N-[1,2,3,4-tetrahydro-9-(1- 1 There are no U.S. registrations for rice and tea. methylethyl)-1,4-methano-naphthalen- (b) Section 18 emergency exemptions. 5-yl]-1H-pyrazole-4-carboxamide), as [Reserved] the sum of its syn-isomer (3-

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(difluoromethyl)-1-methyl-N-[(1RS, and degradates, in or on the commod- 4SR, 9RS)-1,2,3,4-tetrahydro-9-(1- ities listed below. Compliance with the methylethyl)-1,4-methanonaphthalen- tolerance levels is to be determined by 5-yl]-1H-pyrazole-4-carboxamide) and measuring only amisulbrom, 3-[(3- anti-isomer (3-(difluoromethyl)-1-meth- bromo-6-fluoro-2-methyl-1H-indole-1- yl-N-[(1RS, 4SR, 9SR)-1,2,3,4- yl) sulfonyl]-N, N-dimethyl-1H-1, 2, 4- tetrahydro-9-(1-methylethyl)-1,4- triazole-1-sulfonamide]. methano-naphthalen-5-yl]-1H-pyrazole- Parts per 4-carboxamide) in or on the com- 1 Commodity million modity. Grape ...... 0 .40 Commodity Parts per Grape, raisin ...... 1 .0 million Tomato ...... 0.50 Tomato, paste ...... 1 .2 Apple1 ...... 0 .70 Banana1 ...... 0 .05 1 There is no U.S. registration for use of amisulbrom on Peanut1 ...... 0 .01 grape or tomato. 1 There are no U.S. registrations for use of isopyrazam on (b) Section 18 emergency exemptions. apple, banana, or peanut. [Reserved] (b) Section 18 emergency exemptions. (c) Tolerances with regional registra- [Reserved] tions. [Reserved] (c) Tolerances with regional registra- (d) Indirect or inadvertent residues. tions. [Reserved] [Reserved] (d) Indirect or inadvertent residues. [Reserved] [76 FR 59914, Sept. 28, 2011] [76 FR 61596, Oct. 5, 2011, as amended at 78 FR § 180.657 Metaflumizone; tolerances 78745, Dec. 27, 2013] for residues. § 180.655 Flazasulfuron; tolerances for (a) General. Tolerances are estab- residues. lished for residues of the insecticide metaflumizone, including its metabo- (a) General. Tolerances are estab- lites and degradates, in or on the com- lished for residues of flazasulfuron, in- modities listed in the following table. cluding its metabolites and degradates, Compliance with the tolerance levels in or on the commodities in the table specified in the following table is to be below. Compliance with the tolerance determined by measuring only the sum levels specified below is to be deter- of metaflumizone (E and Z isomers; 2- mined by measuring only flazasulfuron [2-(4-cyanophenyl)-1-[3- ( -[[(4,6-dimethoxy-2- N (trifluoromethyl) phenyl]ethylidene]- pyrimidinyl)amino]carbonyl]-3- N-[4-(trifluoromethoxy)phenyl] (trifluoromethyl)-2- hydrazinecarboxamide) and its metabo- pyridinesulfonamide). lite 4-{2-oxo-2-[3-(trifluoromethyl) phenyl]ethyl}-benzonitrile, calculated Commodity Parts per million as the stoichiometric equivalent of Fruit, citrus, group 10–10 ...... 0 .01 metaflumizone, in or on the following Grape ...... 0 .01 commodities: Sugarcane ...... 0 .01 Commodity Parts per (b) Section 18 emergency exemptions. million [Reserved] Almond, hulls ...... 0 .04 (c) Tolerances with regional registra- Eggplant 1 ...... 1.5 tions. [Reserved] Fruit, citrus, group 10 ...... 0 .04 Grape ...... 0 .04 (d) Indirect or inadvertent residues. Nut, tree, group 14 ...... 0 .04 [Reserved] Pepper 1 ...... 1 .5 Tomato 1 ...... 0.60 [77 FR 10968, Feb. 24, 2012] Tomato, paste 1 ...... 1 .2 § 180.656 Amisulbrom; tolerances for 1 There are no U.S. registrations as of April 4, 2014. residues. (b) Section 18 emergency exemptions. (a) General. Tolerances are estab- [Reserved] lished for residues of the fungicide (c) Tolerances with regional registra- amisulbrom, including its metabolites tions. [Reserved]

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(d) Indirect or inadvertent residues. Commodity Parts per [Reserved] million [77 FR 10386, Feb. 22, 2012, as amended at 79 Triticale, forage ...... 40 FR 18810, Apr. 4, 2014] Triticale, grain ...... 0 .15 Triticale, hay ...... 80 Triticale, straw ...... 1 .0 § 180.658 Penthiopyrad; tolerances for Vegetable, bulb, group 3–07 ...... 3 .0 residues. Vegetable, cucurbit, group 9 ...... 0.60 (a) General. (1) Tolerances are estab- Vegetable, foliage of legume, group 7, hay ...... 200 lished for residues of penthiopyrad, in- Vegetable, foliage of legume, group 7, vines/forage ...... 50 cluding its metabolites and degradates, Vegetable, fruiting, group 8–10 ...... 3 .0 in or on the commodities in the table Vegetable, leafy, except brassica, group 4 ...... 30 below. Compliance with the tolerance Vegetable, leaves of root and tuber, group 2 ..... 50 levels specified below is to be deter- Vegetable, legume, edible podded, subgroup 6A 4 .0 Vegetable, legume, succulent shelled, subgroup mined by measuring only penthiopyrad 6B ...... 0 .40 (N-[2-(1,3-dimethylbutyl)-3-thienyl]-1- Vegetable, root, subgroup 1B, except sugar methyl-3-(trifluoromethyl)-1H-pyr- beet ...... 3 .0 azole-4-carboxamide). Vegetable, tuber and corm, subgroup 1C ...... 0 .06 Wheat, forage ...... 40 Parts per Wheat, grain ...... 0 .15 Commodity million Wheat, hay ...... 80 Wheat, milled byproducts ...... 0 .30 Alfalfa, forage ...... 7.0 Wheat, straw ...... 1 .0 Alfalfa, hay ...... 20 Almond, hulls ...... 6 .0 (2) Tolerances are established for res- Apple, wet pomace ...... 1 .5 Barley, grain ...... 0 .15 idues of penthiopyrad, including its Barley, hay ...... 80 metabolites and degradates, in or on Barley, milled byproducts ...... 0.90 the commodities in the table below. Barley, straw ...... 1 .0 Beet, sugar, dried pulp ...... 1 .5 Compliance with the tolerance levels Beet, sugar, roots ...... 0 .5 specified below is to be determined by Berry, low growing, subgroup 13–07G ...... 3 .0 measuring only the sum of Brassica, head and stem, subgroup 5A ...... 5 .0 Brassica, leafy greens, subgroup 5B ...... 50 penthiopyrad (N-[2-(1,3-dimethylbutyl)- Buckwheat, grain ...... 0.15 3-thienyl]-1-methyl-3- Canola ...... 1 .5 (trifluoromethyl)-1H-pyrazole-4- Corn, field, forage ...... 40 carboxamide) and its metabolite (1- Corn, field, grain ...... 0 .01 Corn, field, refined oil ...... 0 .05 methyl-3-trifluoromethyl-1H-pyrazole- Corn, field, stover ...... 15 4-carboxamide), calculated as the stoi- Corn, pop, grain ...... 0.01 chiometric equivalent of penthiopyrad, Corn, sweet, kernel plus cob with husks removed ...... 0 .01 in or on the commodity. Cotton, seed ...... 1.5 Cotton, gin byproducts ...... 15 Parts per Commodity million Fruit, pome, group 11–10 ...... 0 .50 Fruit, stone, group 12 ...... 4 .0 Cattle, fat ...... 0.03 Grain, aspirated fractions ...... 30 Cattle, meat ...... 0 .03 Millet, spp...... 0 .80 Nut, tree, group 14 ...... 0 .06 Cattle, meat byproducts ...... 0.09 Oat, forage ...... 40 Goat, fat ...... 0 .03 Oat, grain ...... 0 .15 Goat, meat ...... 0.03 Oat, hay ...... 80 Goat, meat byproducts ...... 0 .09 Oat, straw ...... 1.0 Horse, fat ...... 0 .03 Pea and bean, dried shelled, except soybean, Horse, meat ...... 0 .03 subgroup 6C ...... 0 .40 Horse, meat byproducts ...... 0 .09 Peanut ...... 0 .04 Milk ...... 0.02 Peanut, hay ...... 30 Sheep, fat ...... 0 .03 Peanut, refined oil ...... 0.06 Sheep, meat ...... 0.03 Pistachio ...... 0.06 Sheep, meat byproducts ...... 0 .09 Potato, processed potato waste ...... 0 .20 Rye, forage ...... 40 (b) Section 18 emergency exemptions. Rye, grain ...... 0.15 Rye, straw ...... 1 .0 [Reserved] Sorghum, forage ...... 40 (c) Tolerances with regional registra- Sorghum, grain, grain ...... 0 .80 tions. [Reserved] Sorghum, stover ...... 15 Soybean, seed ...... 0 .40 (d) Indirect or inadvertent residues. Sunflower, seed ...... 1.5 [Reserved] Teosinte, grain ...... 0 .15 Tomato, paste ...... 3 .5 [77 FR 14297, Mar. 9, 2012]

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§ 180.659 Pyroxasulfone; tolerances for Commodity Parts per residues. million (a) General. (1) Tolerances are estab- Soybean, hay ...... 2 .0 lished for residues of the herbicide Wheat, forage ...... 6 .0 Wheat, hay ...... 1 .0 pyroxasulfone, including its metabo- Wheat, straw ...... 0 .60 lites and degradates, in or on the commodities in the table below. Compli- (3) Tolerances are established for res- ance with the tolerance levels specified idues of the herbicide pyroxasulfone, below is to be determined by measuring including its metabolites and only the sum of pyroxasulfone, 3-[[[5- degradates, in or on the commodities (difluoromethoxy)-1-methyl-3- in the table below. Compliance with (trifluoromethyl)-1H-pyrazol-4- the tolerance levels specified below is yl]methyl]sulfonyl]-4,5-dihydro-5,5- to be determined by measuring only dimethylisoxazole, and its metabolite, the sum of pyroxasulfone, 3-[[[5- 5-(difluoromethoxy)-1-methyl-3- (difluoromethoxy)-1-methyl-3- (trifluoromethyl)-1H-pyrazol-4-car- (trifluoromethyl)-1H-pyrazol-4- boxylic acid (M-3), calculated as the yl]methyl]sulfonyl]-4,5-dihydro-5,5- stoichiometric equivalent of dimethylisoxazole, and its metabolites, pyroxasulfone, in or on the commodity. 5-(difluoromethoxy)-1-methyl-3- (trifluoromethyl)-1H-pyrazol-4-car- Parts per boxylic acid (M–3); [5- Commodity million (difluoromethoxy)-3-(trifluoromethyl)- Corn, field, grain ...... 0 .02 1H-pyrazol-4-yl]methanesulfonic acid Corn, pop, grain ...... 0.015 Corn, sweet, kernel plus cob with husks re- (M–25); and 3-[1-carboxy-2-(5,5-di- moved ...... 0 .015 methyl-4,5-dihydroisoxazol-3- Cotton, undelinted seed ...... 0 .04 ylthio)ethylamino]-3-oxopropanoic acid Wheat, grain ...... 0 .03 (M–28), calculated as the stoichiometric equivalent of pyroxasulfone, in (2) Tolerances are established for res- or on the commodity. idues of the herbicide pyroxasulfone, including its metabolites and Commodity Parts per degradates, in or on the commodities million in the table below. Compliance with Soybean, seed ...... 0 .06 the tolerance levels specified below is to be determined by measuring only (4) Tolerances are established for res- the sum of pyroxasulfone, 3-[[[5- idues of the herbicide pyroxasulfone, (difluoromethoxy)-1-methyl-3- including its metabolites and (trifluoromethyl)-1H-pyrazol-4- degradates, in or on the commodities yl]methyl]sulfonyl]-4,5-dihydro-5,5- in the following table. Compliance with dimethylisoxazole, and its metabolites, the tolerance levels specified in the fol- 5-(difluoromethoxy)-1-methyl-3- lowing table is to be determined by (trifluoromethyl)-1H-pyrazol-4- measuring only the sum of yl]methanesulfonic acid (M–1); 5- pyroxasulfone [3-[[[5- (difluoromethoxy)-1-methyl-3- (difluoromethoxy)-1-methyl-3- (trifluoromethyl)-1H-pyrazol-4-car- (trifluoromethyl)-1H-pyrazol-4- boxylic acid (M-3); and [5- yl]methyl]sulfonyl]-4,5-dihydro-5,5- (difluoromethoxy)-3-(trifluoromethyl)- dimethylisoxazole] and its metabolites 1H-pyrazol-4-yl]methanesulfonic acid [5-(difluoromethoxy)-1-methyl-3- (M-25), calculated as the stoichiometric (trifluoromethyl)-1H-pyrazol-4- equivalent of pyroxasulfone, in or on yl]methanesulfonic acid (M–1) and 5- the commodity. (difluoromethoxy)-1-methyl-3- (trifluoromethyl)-1H-pyrazol-4-car- Parts per Commodity million boxylic acid (M–3), calculated as the stoichiometric equivalent of Corn, field, forage ...... 0 .09 pyroxasulfone, in or on the commodity. Corn, field, stover ...... 0 .15 Corn, pop, stover ...... 0.15 Parts per Corn, sweet, forage ...... 0 .10 Commodity million Corn, sweet, stover ...... 0 .15 Cotton, gin byproducts ...... 0 .20 Milk ...... 0.003 Soybean, forage ...... 1 .0

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(b) Section 18 emergency exemptions. Commodity Parts [Reserved] per million (c) Tolerances with regional registra- Beet, sugar, root ...... 0 .04 tions. [Reserved] Cherry ...... 0.60 (d) Indirect or inadvertent residues. Grape, wine ...... 2 .0 [Reserved] Nut, tree, group 14 ...... 0 .05 Peanut ...... 0 .02 [77 FR 12213, Feb. 29, 2012, as amended at 78 Pistachio ...... 0.05 FR 13257, Feb. 27, 2013; 78 FR 46279, July 31, Potato ...... 0 .02 2013; 79 FR 34633, June 18, 2014] Potato, processed potato waste ...... 0 .08 Strawberry ...... 1 .5 Watermelon ...... 1.0 § 180.660 Pyriofenone; tolerances for residues. 1 There are no U.S. registrations. (a) General. Tolerances are estab- (2) Tolerances are established for res- lished for residues of the fungicide idues of the fungicide fluopyram, N-[2- pyriofenone, including its metabolites [3-chloro-5-(trifluoromethyl)-2- and degradates, in or on the following pyridinyl]ethyl]-2- commodities listed in the table. Com- (trifluoromethyl)benzamide, including pliance with the tolerance levels speci- its metabolites and degradates. Com- fied in the table is to be determined by pliance with the tolerance levels speci- measuring only pyriofenone, (5-chloro- fied in the table below is to be deter- 2-methoxy-4-methyl-3-pyridinyl)(2,3,4- mined by measuring only the sum of trimethoxy-6-methylphenyl) fluopyram and its metabolite, 2- methanone, in or on the following com- (trifluoromethyl)benzamide, calculated modities: as the stoichiometric equivalent of fluopyram, in or on the commodity. Parts per Commodity million Parts per Commodity million Grape 1 ...... 0 .30 1 Grape, raisin ...... 0 .50 Cattle, fat ...... 0.11 1 There are no U.S. registrations for grape and grape, Cattle, meat ...... 0 .15 raisin. Cattle, meat byproducts ...... 1.1 Egg ...... 0 .25 (b) Section 18 emergency exemptions. Goat, fat ...... 0 .11 [Reserved] Goat, meat ...... 0.15 (c) Tolerances with regional registra- Goat, meat byproducts ...... 1 .1 tions. [Reserved] Hog, fat ...... 0 .05 Hog, meat ...... 0 .05 (d) Indirect or inadvertent residues. Hog, meat byproducts ...... 0 .70 [Reserved] Horse, fat ...... 0 .11 Horse, meat ...... 0 .15 [77 FR 13506, Mar. 7, 2012] Horse, meat byproducts ...... 1 .1 Milk ...... 0.07 § 180.661 Fluopyram; tolerances for Poultry, fat ...... 0.20 residues. Poultry, meat ...... 0 .15 Poultry, meat byproducts ...... 0.60 (a) General. (1) Tolerances are estab- Sheep, fat ...... 0 .11 lished for residues of the fungicide Sheep, meat ...... 0.15 Fluopyram, N-[2-[3-chloro-5- Sheep, meat byproducts ...... 1 .1 (trifluoromethyl)-2-pyridinyl]ethyl]-2- (trifluoromethyl)benzamide, including (b) Section 18 emergency exemptions. its metabolites and degradates in or on [Reserved] the commodities in the table below. (c) Tolerances with regional registra- Compliance with the tolerance levels tions. [Reserved] specified in the table is to be deter- (d) Indirect or inadvertent residues. It mined by measuring only fluopyram in is recommended that tolerances be es- or on the commodity. tablished for indirect or inadvertent residues of fungicide fluopyram, N-[2- Commodity Parts [3-chloro-5-(trifluoromethyl)-2- per million pyridinyl]ethyl]-2- Almond, hull ...... 8 .0 (trifluoromethyl)benzamide, including Apple ...... 0.30 its metabolites and degradates, in or Apple, wet pomace ...... 0 .60 Banana 1 ...... 1.0 on the commodities in the table below. Bean, dry ...... 0.09 Compliance with the tolerance levels

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specified in the table is to be deter- Commodity Parts per mined by measuring only fluopyram in million or on the commodity. Sheep, meat ...... 0.02 Sheep, meat byproducts ...... 0 .04 Commodity Parts per Sugarcane, cane ...... 0.8 million Sugarcane, molasses ...... 2 .5 Wheat, bran ...... 6.0 Alfalfa, forage ...... 0.45 Wheat, forage ...... 1 .0 Alfalfa, hay ...... 1.1 Wheat, grain ...... 4 .0 Canola, seed ...... 1 .8 Wheat, hay ...... 1 .5 Cotton, gin byproducts ...... 0 .05 Wheat, middlings ...... 10 .5 Cotton, undelinted seed ...... 0 .01 Wheat, straw ...... 0 .9 Grain, cereal, forage, fodder and straw, group 16, except rice; forage ...... 4 .0 Grain, cereal, forage, fodder and straw, group (b) Section 18 emergency exemptions. 16, except rice; hay, straw and stover ...... 7 .0 [Reserved] Grain, cereal, group 15, except rice ...... 1 .5 (c) Tolerances with regional registra- Soybean, forage ...... 4 .0 Soybean, hay ...... 15 tions. [Reserved] Soybean, seed ...... 0 .10 (d) Indirect or inadvertent residues. [Reserved] [77 FR 10975, Feb. 24, 2012] [77 FR 12745, Mar. 2, 2012, as amended at 77 FR 60919, Oct. 3, 2012] § 180.662 Trinexapac-ethyl; tolerances for residues. § 180.663 Ametoctradin; tolerances for (a) General. Tolerances are estab- residues. lished for residues of the plant growth (a) General. Tolerances are estab- inhibitor, trinexapac-ethyl, including lished for residues of the fungicide its metabolites and degradates, in or ametoctradin, including its metabo- on the commodities in the table below. lites and degradates, in or on the com- Compliance with the tolerance levels modities in the following table. Com- specified below is to be determined by pliance with the tolerance levels speci- measuring both trinexapac-ethyl, ethyl fied in the following table is to be de- 4-(cyclopropylhydroxymethylene)-3,5- termined by measuring only dioxocyclohexanecarboxylate and the ametoctradin (5-ethyl-6- associated metabolite, trinexpac, 4- octyl[1,2,4]triazolo[1,5-a]pyrimidin-7- (cyclopropylhydroxymethylene)-3,5- amine). dioxocyclohexanecarboxylic acid, cal- Parts per culated as the stoichiometric equiva- Commodity million lent of trinexapac-ethyl, in or on the commodity. Brassica, head and stem, subgroup 5A ...... 9 .0 Brassica, leafy greens, subgroup 5B ...... 50 Grape ...... 4 .0 Parts per Commodity million Grape, raisin ...... 8 .0 Hop, dried cones ...... 10 .0 Barley, bran ...... 2 .5 Onion, bulb, subgroup 3–07A ...... 1 .5 Barley, grain ...... 2 .0 Onion, green, subgroup 3–07B ...... 20 .0 Barley, hay ...... 0 .8 Spinach ...... 50 .0 Barley, straw ...... 0 .4 Vegetable, cucurbit, group 9 ...... 3.0 Cattle, fat ...... 0.02 Vegetable, fruiting, group 8–10 ...... 1 .5 Cattle, meat ...... 0 .02 Vegetable, leafy, except Brassica, group 4, ex- Cattle, meat byproducts ...... 0.04 cept spinach ...... 40 .0 Goat, fat ...... 0 .02 Vegetable, tuberous and corm, subgroup 1C ..... 0.05 Goat, meat ...... 0.02 Goat, meat byproducts ...... 0 .04 (b) Section 18 emergency exemptions. Grass, forage ...... 1 .5 [Reserved] Grass, hay ...... 4 .0 Grass, seed screenings ...... 40.0 (c) Tolerances with regional registra- Grass, straw ...... 10 .0 tions. [Reserved] Hog, fat ...... 0 .02 (d) Indirect or inadvertent residues. Hog, meat ...... 0 .02 Hog, meat by-products ...... 0 .03 [Reserved] Horse, fat ...... 0 .02 [77 FR 21734, May 9, 2012] Horse, meat ...... 0 .02 Horse, meat byproducts ...... 0 .04 Oat, forage ...... 1 .0 § 180.664 Penflufen; tolerances for resi- Oat, grain ...... 4 .0 dues. Oat, hay ...... 1.5 Oat, straw ...... 0.9 (a) General. Tolerances are estab- Sheep, fat ...... 0 .02 lished for residues of the fungicide

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penflufen, including its metabolites Commodity Parts per and degradates, in or on the following million commodities listed in the table. Com- Oat, straw ...... 0.01 pliance with the tolerance levels speci- Pea and bean, dried shelled, except soybean, fied in the table is to be determined by subgroup 6C ...... 0 .01 Potato ...... 0 .02 measuring only penflufen N-[2-(1,3- Potato, wet peel ...... 0 .075 dimethylbutyl)phenyl]-5-fluoro-1,3-di- Rapeseed, subgroup 20A ...... 0.01 methyl-1H-pyrazole-4-carboxamide, in Rye, forage ...... 0 .015 Rye, grain ...... 0.01 or on the following commodities. Rye, straw ...... 0 .01 Sorghum, grain, forage ...... 0.01 Parts per Sorghum, grain, grain ...... 0 .01 Commodity million Sorghum, grain, stover ...... 0 .01 Alfalfa, forage ...... 0.01 Soybean, forage ...... 0 .05 Alfalfa, hay ...... 0.01 Soybean, hay ...... 0 .04 Cotton, gin by-products ...... 0 .01 Soybean, seed ...... 0 .01 Grain cereal, forage, fodder and straw, group Vegetable, foliage of legume, except soybean, 16 ...... 0 .01 subgroup 7A ...... 0 .01 Grain, cereal, group 15 ...... 0.01 Wheat, forage ...... 0 .015 Oilseed, group 20 ...... 0 .01 Wheat, grain ...... 0 .01 Vegetable, foliage of legume, group 7 ...... 0 .01 Wheat, hay ...... 0 .06 Vegetable, legume, group 6 ...... 0 .01 Wheat, straw ...... 0 .01 Vegetable, tuberous and corm subgroup 1C .... 0 .01 (b) Section 18 emergency exemptions. (b) Section 18 emergency exemptions. [Reserved] [Reserved] (c) Tolerances with regional registra- (c) Tolerances with regional registrations. [Reserved] tions. [Reserved] (d) Indirect inadvertent residues. [Re- (d) Indirect or inadvertent residues. served] [Reserved] [77 FR 36924, June 20, 2012, as amended at 78 [77 FR 28281, May 14, 2012] FR 33748, June 5, 2013; 78 FR 60719, Oct. 2, 2013] § 180.665 Sedaxane; tolerances for residues. § 180.666 Fluxapyroxad; tolerances for (a) General. Tolerances are estab- residues. lished for residues of the fungicide (a) General. Tolerances are estab- sedaxane, including its metabolites and lished for residues of the fungicide degradates, in or on the commodities fluxapyroxad, including its metabolites in the following table. Compliance with and degradates, in or on the commod- the tolerance levels specified in the fol- ities listed in the table below. Compli- lowing table is to be determined by ance with the tolerance levels specified measuring only sedaxane, N-[2-[1,1′- below is to be determined by measuring bicyclopropyl]-2-ylphenyl]-3- only fluxapyroxad, 3-(difluoromethyl)- (difluoromethyl)-1-methyl-1H-pyrazole- 1-methyl-N-(3′,4′,5′-trifluoro[1,1′- 4-carboxamide, as the sum of its cis- biphenyl]-2-yl)-1H-pyrazole-4- and trans-isomers in or on the com- carboxamide in or on the commodity. modity. Commodity Parts per Parts per million Commodity million Almond, hulls ...... 4 .0 Barley, grain ...... 0 .01 Apple, wet pomace ...... 2 .0 Barley, hay ...... 0 .04 Beet, sugar ...... 0 .1 Barley, straw ...... 0 .01 Beet, sugar, dried pulp ...... 0 .1 Canola, seed ...... 0 .01 Beet, sugar, tops ...... 7.0 Corn, field, forage ...... 0 .01 Berry, low growing, subgroup 13–07G ...... 4 .0 Corn, field, grain ...... 0 .01 Bushberry, subgroup 13–07B ...... 7.0 Corn, field, stover ...... 0 .01 Caneberry, subgroup 13–07A ...... 5 .0 Corn, pop, grain ...... 0.01 Cattle, fat ...... 0.05 Corn, pop, stover ...... 0.01 Cattle, meat ...... 0 .01 Corn, sweet, forage ...... 0 .01 Cattle, meat byproducts ...... 0.03 Corn, sweet, kernel plus cob with husks re- Corn, field, grain ...... 0 .01 moved ...... 0 .01 Corn, oil ...... 0 .03 Corn, sweet, stover ...... 0 .01 Corn, pop, grain ...... 0.01 Oat, forage ...... 0 .015 Corn, sweet, kernels plus cobs with husks re- Oat, grain ...... 0 .01 moved ...... 0 .15 Oat, hay ...... 0.06 Cotton, gin byproducts ...... 0 .01

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termined by measuring only Commodity Parts per million fluxapyroxad, 3-(difluoromethyl)-1- Cotton, undelinted seed ...... 0 .01 methyl-N-(3′,4′,5′-trifluoro[1,1′- Egg ...... 0 .002 biphenyl]-2-yl)-1H-pyrazole-4- Fish-freshwater finfish ...... 0.01 carboxamide in or on the commodity. Fish-shellfish, crustacean ...... 0 .01 Fruit, pome, group 11 ...... 0.8 Parts per Fruit, small, vine climbing, except fuzzy Commodity million kiwifruit, subgroup 13–07F ...... 2 .0 Fruit, stone, group 12–12 ...... 3 .0 Nongrass animal feeds, group18 ...... 0 .30 Goat, fat ...... 0 .05 Peppermint, tops ...... 0 .01 Goat, meat ...... 0.01 Spearmint, tops ...... 0 .01 Goat, meat byproducts ...... 0 .03 Grain, aspirated fractions ...... 20.0 Grain, cereal, forage, fodder and straw, group [77 FR 28275, May 14, 2012, as amended at 77 16 ...... 20 FR 46307, Aug. 3, 2012; 79 FR 10677, Feb. 26, Grain, cereal, group 15, (except corn, field, grain; except corn, pop, grain; except corn, 2014] kernels plus cobs with husks removed; except rice; except wheat ...... 3 .0 § 180.667 Cyflufenamid, tolerance for Grape, raisin ...... 5 .7 residues. Hog, meat byproducts ...... 0 .01 Horse, fat ...... 0 .05 (a) General. Tolerances are estab- Horse, meat ...... 0 .01 lished for residues of the fungicide Horse, meat byproducts ...... 0 .03 cyflufenamid, including its metabolites Milk ...... 0.005 Nut, tree, group 14–12 ...... 0 .06 and degradates, in or on the commod- Oilseeds, group 20 (except cottonseed) ...... 0 .9 ities in the table below. Compliance Pea and bean, dried shelled except soybean, with the tolerance levels specified subgroup 6C ...... 0 .4 Pea and bean, succulent shelled, subgroup 6B 0 .5 below is to be determined by measuring Peanut ...... 0 .01 only cyflufenamid, [N(Z)]-N- Peanut, refined oil ...... 0.02 [[(cyclopropylmethoxy)amino][2,3- Plum, prune, dried ...... 3.0 Potato, wet peel ...... 0 .1 difluoro-6-(trifluoromethyl)phenyl] Rice, bran ...... 4.5 methylene]benzeneacetamide. Rice, bran ...... 8.5 Rice, grain ...... 5 .0 Commodity Parts per Rice, hulls ...... 8 .0 million Rice, hulls ...... 15 .0 Sheep, fat ...... 0 .05 Apple, wet pomace ...... 0.10 Sheep, meat ...... 0.01 Berry, low growing, subgroup 13–07G, except Sheep, meat byproducts ...... 0 .03 cranberry ...... 0.20 Soybean, hulls ...... 0 .3 Fruit, pome, group 11 ...... 0.06 Soybean, seed ...... 0 .15 Fruit, small vine climbing, except fuzzy kiwifruit, Sugarcane, cane ...... 3.0 subgroup 13–07F ...... 0.15 Vegetable, brassica leafy, group 5 ...... 4 .0 Grape, raisin ...... 0.30 Vegetable, bulb, group 3–07 ...... 1 .5 Vegetable, cucurbit, group 9 ...... 0.07 Vegetable, cucurbit, group 9 ...... 0.50 Vegetable, foliage of legume, group 7 ...... 30 (b) Section 18 emergency exemptions. Vegetables, fruiting, group 8 ...... 0.7 Vegetable, leafy, except brassica, group 4 ...... 30 [Reserved] Vegetable, legume, edible podded, subgroup (c) Tolerances with regional registra- 6A ...... 2 .0 tions. [Reserved] Vegetable, root, except sugarbeet, subgroup 1B ...... 0.90 (d) Indirect or inadvertent residues. Vegetable, tuberous and corm, subgroup 1C ... 0.02 [Reserved] Wheat, bran ...... 0.6 Wheat, grain ...... 0 .3 [77 FR 38210, June 27, 2012]

(b) Section 18 emergency exemptions. § 180.668 Sulfoxaflor; tolerances for [Reserved] residues. (c) Tolerances with regional registra- (a) General. Tolerances are estab- tions. [Reserved] lished for residues of the insecticide (d) Indirect or inadvertent residues. sulfoxaflor, including its metabolites Tolerances are established for the com- and degradates, in or on the commod- bined indirect or inadvertent residues ities in the table. Compliance with the of the fungicide fluxapyroxad, includ- tolerance levels specified is to be deter- ing its metabolites and degradates, in mined by measuring only sulfoxaflor or on the commodities listed in the (N-[methyloxido[1-[6-(trifluoromethyl)- table below. Compliance with the toler- 3-pyridinyl]ethyl]-g4-sulfanylidene]cy- ance levels specified below is to be de- anamide).

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(d) Indirect or inadvertent residues. Commodity Parts per million [Reserved] Almond, hulls ...... 6 .0 [77 FR 59565, Sept. 28, 2012, as amended at 78 Barley, grain ...... 0 .40 FR 38227, June 26, 2013] Barley, hay ...... 1 .0 Barley, straw ...... 2 .0 Bean, dry seed ...... 0 .20 § 180.669 Picoxystrobin; tolerances for Bean, succulent ...... 4 .0 residues. Beet, sugar, dried pulp ...... 0 .07 (a) General. Tolerances are estab- Beet, sugar, molasses ...... 0 .25 Berry, low growing, subgroup 13–7G ...... 0 .70 lished for residues of the fungicide Cattle, fat ...... 0.10 picoxystrobin, including its metabo- Cattle, meat ...... 0 .15 lites and degradates, in or on the com- Cattle, meat byproducts ...... 0.40 modities listed below. Compliance with Cauliflower ...... 0 .08 the tolerance levels specified below is Citrus, dried pulp ...... 3 .6 Cotton, gin byproducts ...... 6 .0 to be determined by measuring only Cotton, hulls ...... 0 .35 picoxystrobin, methyl (aE)-a- Cottonseed subgroup 20C ...... 0 .20 (methoxymethylene)-2-[[[6- Fruit, citrus, group 10–10 ...... 0 .70 (trifluoromethyl)-2-pyridinyl]oxy] Fruit, pome, group 11–10 ...... 0 .50 Fruit, small, vine climbing, subgroup 13–07F, methyl]benzeneacetate. except fuzzy kiwi fruit ...... 2.0 Fruit, stone, group 12 ...... 3 .0 Parts per Commodity million Goat, fat ...... 0 .10 Goat, meat ...... 0.15 Barley, bran ...... 0 .5 Goat, meat byproducts ...... 0 .40 Barley, grain ...... 0 .3 Grain, aspirated fractions ...... 20.0 Cattle, fat ...... 0.01 Grape, raisin ...... 6 .0 Cattle, meat ...... 0 .01 Hog, fat ...... 0 .01 Cattle, meat byproducts ...... 0.01 Hog, meat ...... 0 .01 Corn, field, refined oil ...... 0 .07 Hog, meat byproducts ...... 0 .01 Eggs ...... 0 .01 Horse, fat ...... 0 .10 Goat, fat ...... 0 .01 Horse, meat ...... 0 .15 Goat, meat ...... 0.01 Horse, meat byproducts ...... 0 .40 Goat, meat byproducts ...... 0 .01 Leafy greens, subgroup 4A ...... 6.0 Grain, aspirated grain fractions ...... 10 Leafy petiole, subgroup 4B ...... 2 .0 Grain, cereal, forage, fodder, and straw, group Milk ...... 0.15 16, forage ...... 15 Nuts, tree, group 14 ...... 0 .015 Grain, cereal, forage, fodder, and straw, group Onion, bulb, subgroup 3–07A ...... 0 .01 16, hay ...... 5 Onion, green, subgroup 3–07B ...... 0 .70 Grain, cereal, forage, fodder, and straw, group Pistachio ...... 0.015 16, stover ...... 10 Poultry, eggs ...... 0 .01 Grain, cereal, forage, fodder, and straw, group Poultry, fat ...... 0.01 16, straw ...... 2 Poultry, meat ...... 0 .01 Grain, cereal, group 15, except rice and barley 0 .04 Poultry, meat byproducts ...... 0.01 Hog, fat ...... 0 .01 Rapeseed, meal ...... 0 .50 Hog, meat ...... 0 .01 Rapeseed subgroup 20A ...... 0 .40 Hog, meat byproducts ...... 0 .01 Sheep, fat ...... 0 .10 Horse, fat ...... 0 .01 Sheep, meat ...... 0.15 Horse, meat ...... 0 .01 Sheep, meat byproducts ...... 0 .40 Horse, meat byproducts ...... 0 .01 Soybean, seed ...... 0 .20 Milk ...... 0.01 Tomato, paste ...... 2 .60 Pea and bean, dried shelled, except soybean, Tomato, puree ...... 1 .20 subgroup 6C ...... 0 .06 Vegetable, brassica, leafy, group 5, except Poultry, fat ...... 0.01 cauliflower ...... 2 .0 Poultry, meat ...... 0 .01 Vegetable, cucurbit, group 9 ...... 0.40 Poultry, meat byproducts ...... 0.01 Vegetable, fruiting, group 8–10 ...... 0 .70 Rapeseed subgroup 20A ...... 0 .08 Vegetable, leaves of root and tuber, group 2 ... 3 .0 Sheep, fat ...... 0 .01 Vegetable, legume, foliage, group 7 ...... 3.0 Sheep, meat ...... 0.01 Vegetable, root and tuber, group 1 ...... 0 .05 Sheep, meat byproducts ...... 0 .01 Watercress ...... 6 .0 Soybean, forage ...... 1 Wheat, forage ...... 1 .0 Soybean, hay ...... 3 Wheat, grain ...... 0 .08 Soybean, hulls ...... 0 .2 Wheat, hay ...... 1 .5 Soybean, seed ...... 0 .05 Wheat, straw ...... 2 .0 Vegetable, foliage of legume, except soybean, subgroup 7A ...... 40 Wheat, bran ...... 0.06 (b) Section 18 emergency exemptions. Wheat, germ ...... 0 .09 [Reserved] (c) Tolerances with regional registra- (b) Section 18 emergency exemptions. tions. [Reserved] [Reserved]

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(c) Tolerances with regional registra- Commodity Parts per tions. [Reserved] million (d) Indirect or inadvertent residues. Brassica leafy vegetables (subgroup 5B) ...... 30 [Reserved] Bushberry (subgroup 13–07B) ...... 4 .0 Cattle, fat ...... 0.01 [77 FR 72231, Dec. 5, 2012] Cattle, meat ...... 0 .01 Cattle, meat byproducts ...... 0.01 § 180.671 Fenpyrazamine; tolerances Cherry (subgroup 12–12A) ...... 6 .0 for residues. Citrus, oil ...... 2.4 (a) General. Tolerances are estab- Cotton, gin byproducts ...... 10 lished for residues of the fungicide Fruit, citrus (group 10–10) ...... 0 .70 Fruit, pome (group 11–10) ...... 1 .5 fenpyrazamine, in or on the following Goat, fat ...... 0 .01 commodities. Compliance with the tol- Goat, meat ...... 0.01 erance levels specified in the following Goat, meat byproducts ...... 0 .01 table is to be determined by measuring Horse, fat ...... 0 .01 only fenpyrazamine S-allyl 5-amino-2- Horse, meat ...... 0 .01 Horse, meat byproducts ...... 0 .01 isopropyl-4-(2-methylphenyl)-3-oxo-2,3- Milk ...... 0.01 dihydropyrazole-1-carbothioate, in or Nut, tree (group 14–12) ...... 0 .04 on the following commodities: Oilseed (group 20) ...... 1 .5 Onion, bulb (subgroup 3–07A) ...... 0 .04 Commodity Parts per Onion, green (subgroup 3–07B) ...... 8 .0 million Peach (subgroup 12–12B) ...... 1 .5 Plum (subgroup 12–12C) ...... 0 .50 Almond ...... 0.02 Sheep, fat ...... 0 .01 Almond, hulls ...... 1 .5 Berry, low growing, subgroup 13–07G ...... 3 Sheep, meat ...... 0.01 Bushberry subgroup 13–07B ...... 5 Sheep, meat byproducts ...... 0 .01 Caneberry subgroup 13–07A ...... 5 Vegetable, cucurbit (group 9) ...... 0 .40 Fruit, small vine climbing, except fuzzy kiwifruit, Vegetable, fruiting (group 8–10) ...... 2 .0 subgroup 13–07F ...... 3 Vegetable, leafy (except Brassica) (group 4) ...... 20 Ginseng ...... 0 .7 Vegetable, tuberous and corm (subgroup 1C) .... 0 .15 Grape, juice ...... 4 Lettuce, head ...... 1.5 Lettuce, leaf ...... 2 (b) Section 18 emergency exemptions. Pistachio ...... 0.02 [Reserved] (c) Tolerances with regional registra- (b) Section 18 emergency exemptions. tions. [Reserved] [Reserved] (d) Indirect or inadvertent residues. (c) Tolerances with regional registra- Tolerances are established for indirect tions. [Reserved] or inadvertent tolerances for residues (d) Indirect or inadvertent residues. of cyantraniliprole, 3-bromo-1-(3- [Reserved] chloro-2-pyridinyl)-N-[4-cyano-2-meth- [78 FR 14465, Mar. 6, 2013] yl-6-[(methylamino)carbonyl]phenyl]- 1H-pyrazole-5-carboxamide, including § 180.672 Cyantraniliprole; tolerances its metabolites and degradates, in or for residues. on commodities in the following table. (a) General. Tolerances are estab- Compliance with the tolerance levels lished for the combined residues of the specified in the following table is to be insecticide cyantraniliprole, 3-bromo-1- determined by measuring only (3-chloro-2-pyridinyl)-N-[4-cyano-2- cyantraniliprole in or on the com- methyl-6-[(methylamino)carbonyl] modity. phenyl]-1H-pyrazole-5-carboxamide, in- Parts per cluding its metabolites and degradates, Commodity million in or on commodities in the following table. Compliance with the tolerance Animal feed, nongrass (group 18) ...... 0.20 Grain, cereal, forage, fodder and straw (group levels specified in the following table is 16) ...... 0 .50 to be determined by measuring only Grass forage, fodder and hay (group 17) ...... 0 .50 cyantraniliprole in or on the com- Peanut, hay ...... 0.01 modity. Vegetable, foliage of legume (group 7) ...... 0 .70 Vegetable, leaves of root and tuber vegetables Parts per (group 2) ...... 0 .04 Commodity million Vegetable, root (subgroup 1A) ...... 0 .02

Almond, hulls ...... 8 .0 Brassica head and stem (subgroup 5A) ...... 3 .0 [79 FR 6833, Feb. 5, 2014]

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§ 180.673 Triforine; tolerances for resi- and degradates, in or on the commod- dues. ities in the table below. Compliance (a) General. Tolerances are estab- with the tolerance levels specified lished for residues of triforine, includ- below is to be determined by measuring ing its metabolites and degradates. only tolfenpyrad, 4-chloro-3-ethyl-1- Compliance with the tolerance levels methyl-N-[4-(p-tolyloxy)benzyl]pyr- specified in the following table is to be azole-5-carboxamide. determined by measuring only triforine Parts per (N,N′-[1,2-piperazinediylbis(2,2,2- Commodity million trichloroehylidene)]bis[formamide]), in Almond hulls ...... 6 .0 or on the following commodities. Citrus, dried pulp ...... 8 .0 Citrus, oil ...... 70.0 Parts per Cotton, gin byproducts ...... 15 .0 Commodity million Cotton, undelinted seed ...... 0 .70 Blueberry 1 ...... 1 .0 Fruit, stone, group 12–12 ...... 2 .0 Tomato 1 ...... 0.5 Fruits, citrus, group 10–10 ...... 1 .5 Grape ...... 2 .0 1 There are no U.S. registrations for blueberry and tomato. Grape, raisin ...... 6 .0 Nuts, tree, group 14–12 ...... 0 .05 (b) Section 18 emergency exemptions. Persimmon ...... 2 .0 [Reserved] Plum, prune ...... 3 .0 (c) Tolerances with regional registra- Pomegranate ...... 2 .0 tions. [Reserved] Potato ...... 0 .01 Tea ...... 30 .0 (d) Indirect or inadvertent residues. Vegetable, leafy, except Brassica, group 4 ...... 30 .0 [Reserved] [78 FR 32151, May 29, 2013. Redesignated at 78 (2) Tolerances are established for res- FR 36677, June 19, 2013] idues of the insecticide tolfenpyrad, including its metabolites and degradates, § 180.674 Proquinazid; tolerances for in or on the commodities in the fol- residues. lowing table. Compliance with the tol- (a) General. Tolerances are estab- erance levels specified below is to be lished for residues of the fungicide, determined by measuring only the sum proquinazid, including its metabolites of tolfenpyrad, 4-chloro-3-ethyl-1-meth- and degradates, in or on the commod- yl-N-[4-(p-tolyloxy)benzyl]pyrazole-5- ities listed in the following table. Com- carboxamide, and its metabolite 4-[4- pliance with the tolerance levels speci- [(4-chloro-3-ethyl-1-methylpyrazol-5- fied in the following table is to be de- yl)carbonylamino-methyl]phenoxy]- termined by measuring only benzoic acid, calculated as the stoi- proquinazid, [6-Iodo-2-propoxy-3- chiometric equivalent of tolfenpyrad. propyl-3H-quinazolin-4-one), in or on Parts per the following commodities: Commodity million

Commodity Parts per Cattle, fat ...... 0.01 million Cattle, meat ...... 0 .01 Cattle, meat byproducts ...... 0.35 Grape 1 ...... 0 .50 Goat, fat ...... 0 .01 Grape, raisin 1 ...... 1 .0 Goat, meat ...... 0.01 1 No U.S. registrations for Proquinazid. Goat, meat byproducts ...... 0 .35 Horse, fat ...... 0 .01 (b) Section 18 emergency exemptions. Horse, meat ...... 0 .01 [Reserved] Horse, meat byproducts ...... 0 .35 (c) Tolerances with regional registra- Milk ...... 0.03 Sheep, fat ...... 0 .01 tions. [Reserved] Sheep, meat ...... 0.01 (d) Indirect or inadvertent residues. Sheep, meat byproducts ...... 0 .35 [Reserved] (b) Section 18 emergency exemptions. [79 FR 18815, Apr. 4, 2014] [Reserved] § 180.675 Tolfenpyrad; tolerances for (c) Tolerances with regional registra- residues. tion. [Reserved] (d) Indirect or inadvertent residues. (a) General. (1) Tolerances are estab- [Reserved] lished for residues of the insecticide tolfenpyrad, including its metabolites [79 FR 1605, Jan. 9, 2014]

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§ 180.676 Fenpropidin; tolerances for § 180.678 Tricyclazole; tolerances for residues. residues. (a) General. Tolerances are estab- (a) General. (1) Tolerances are established for the residues of fenpropidin, lished for residues of the fungicide including its metabolites and tricyclazole, including its metabolites degradates, in or on the commodities and degradates, in or on the commod- in the table below. Compliance with ities in the table below. Compliance the tolerance levels specified below is with the tolerance levels specified to be determined by measuring only below is to be determined by measuring fenpropidin (1-[3-[4-(1,1-dimethylethyl) only tricyclazole (5-methyl-1,2,4- triazolo[3,4-b ]benzothiazole). phenyl]-2-methylpropyl]piperidine). Parts Parts per Commodity per million Commodity million Rice, grain 1 ...... 3 .0 Banana 1 ...... 10 1 There are no U.S. Registrations on Rice as of June 11, 1 There are no U.S. registrations as of December 13, 2013. 2014. (b) Section 18 tolerance. [Reserved] (b) Section 18 emergency exemptions. (c) Tolerances with regional registra- [Reserved] tions. [Reserved] (c) Tolerances with regional registra- (d) Indirect or inadvertent residues. tions. [Reserved] [Reserved] (d) Indirect or inadvertent residues. [Reserved] [79 FR 8096, Feb. 11, 2014] [79 FR 33468, June 11, 2014] § 180.677 Cyflumetofen; tolerances for residues. Subpart D—Exemptions From (a) Genera2l. Tolerances are estab- Tolerances lished for residues of the insecticide cyflumetofen, including its metabolites § 180.900 Exemptions from the requirement of a tolerance. and degradates, in or on the commodities in the table below. Compliance An exemption from a tolerance shall with the tolerance levels for be granted when it appears that the cyflumetofen is to be determined by total quantity of the pesticide chem- measuring only cyflumetofen, 2- ical in or on all raw agricultural commodities for which it is useful under methoxyethyl -cyano- -[4-(1,1- a a conditions of use currently prevailing dimethylethyl)phenyl]- -oxo-2- b or proposed will involve no hazard to (trifluoromethyl)benzenepropanoate, in the public health. or on the commodity. [69 FR 23117, Apr. 28, 2004] Commodity Parts per million § 180.905 Pesticide chemicals; exemp- Almond, hulls ...... 4 .0 tions from the requirement of a tol- Citrus, oil ...... 16 erance. Fruit, citrus, group 10–10 ...... 0 .30 (a) When applied to growing crops, in Fruit, pome, group 11–10 ...... 0 .30 accordance with good agricultural Grape ...... 0 .60 practice, the following pesticide chemi- Nut, tree, group 14–12 ...... 0 .01 Strawberry ...... 0 .60 cals are exempt from the requirement Tomato ...... 0.40 of a tolerance: (1) Petroleum oils. (b) Section 18 emergency exemptions. (2) Piperonyl butoxide. [Reserved] (3) Pyrethrins. (c) Tolerances with regional registra- (4) Sabadilla. tions. [Reserved] (b) When applied to growing crops, in (d) Indirect or inadvertent residues. accordance with good agricultural [Reserved] practice, the pesticides rotenone or derris or cube roots are exempt from [79 FR 29108, May 21, 2014] the requirement of a tolerance. There

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are no U.S. registrations for use of ro- § 180.910 Inert ingredients used pre- tenone, derris, or cube roots on food and post-harvest; exemptions from commodities as of March 23, 2011. the requirement of a tolerance. (c) These pesticides are not exempted Residues of the following materials from the requirement of a tolerance are exempted from the requirement of when applied to a crop at the time of or a tolerance when used in accordance after harvest. with good agricultural practice as inert (or occasionally active) ingredients in [77 FR 59128, Sept. 26, 2012] pesticide formulations applied to growing crops or to raw agricultural commodities after harvest:

Inert ingredients Limits Uses

Acetic acid ...... Catalyst Acetic anhydride ...... Solvent, cosolvent Acetone ...... Do. Alkanoic and alkenoic acids, mono- and diesters ...... Emulsifiers of a-hydro-w-hydroxypoly (oxyethylene) with molecular weight (in amu) range of 200 to 6,000.

Alkyl (C8-C24) benzenesulfonic acid and its am- ...... Surfactants, related adjuvants of surfactants monium, calcium, magnesium, potassium, sodium, and zinc salts.

C10-C18-Alkyl dimethyl amine oxides (CAS Reg. 15% by weight in pesticide Surfactant Nos. 1643–20–5, 2571–88–2, 2605–79–0, formulation. 3332–27–2, 61788–90–7, 68955–55–5, 70592–80–2, 7128–91–8, 85408–48–6, and 85408–49–7).

a-Alkyl(C6-C15)-w- Not to exceed 30% of pes- Surfactants, related adjuvants of surfactants hydroxypoly(oxyethylene)sulfate, and its am- ticide formulation. monium, calcium, magnesium, potassium, sodium, and zinc salts, poly(oxyethylene) content averages 2–4 moles (CAS Reg. Nos. 3088–31–1, 9004–82–4, 9004–84–6, 9021– 91–4, 13150–00–0, 25446–78–0, 26183–44– 8, 27140–00–7, 27731–61–9, 27731–62–0, 32612–48–9, 34431–25–9, 35015–74–8, 50602–06–7, 52286–18–7, 52286–19–8, 54116–08–4, 61702–79–2, 62755–21–9, 63428–86–4, 63428–87–5, 65086–57–9, 65086–79–5, 67674–66–2, 67845–82–3, 67845–83–4, 68037–05–8, 68037–06–9, 68171–41–5, 68424–50–0, 68511–39–7, 68585–34–2, 68610–66–2, 68611–55–2, 68649–53–6, 68890–88–0, 68891–29–2, 68891–30–5, 68891–38–3, 69011–37–6, 73665–22–2, 75422–21–8, 78330–16–2, 78330–17–3, 78330–25–3, 78330–26–4, 78330–27–5, 78330–28–6, 78330–29–7, 78330–30–0, 96130–61–9, 106597–03–9, 110392–50–2, 125301–88–4, 125301–89–5, 125301–92–0, 125736–54–1, 157707–85–2, 160104–51–8, 160901–27–9, 160901–28–0, 160901–29–1, 160901–30–4, 161025–28–1, 161074–79–9, 162063–19–6).

a-alkyl (C12-C15)-w-hydroxypoly (oxypropylene) Not more than 20% of pes- Surfactant poly (oxyethylene) copolymers (where the ticide formulations. poly (oxypropylene) content is 3–60 moles and the poly (oxyethylene) content is 5–80 moles).

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Inert ingredients Limits Uses

a-alkyl-w-hydroxypoly (oxypropylene) and/or ...... Surfactants, related adjuvants of poly (oxyethylene) polymers where the alkyl surfactants. chain contains a minimum of six carbons (CAS Reg. No.: 9002–92–0; 9004–95–9; 9004–98–2; 9005–00–9; 9035–85–2; 9038– 29–3; 9038–43–1; 9040–05–5; 9043–30–5; 9087–53–0; 25190–05–0; 24938–91–8; 25231–21–4; 26183–52–8; 26468–86–0; 26636–39–5; 27252–75–1; 27306–79–2; 31726–34–8; 34398–01–1; 34398–05–5; 37251–67–5; 37311–00–5; 37311–01–6; 37311–02–7; 37311–04–9; 39587–22–9; 50861–66–0; 52232–09–4; 52292–17–8; 52609–19–5; 57679–21–7; 59112–62–8; 60828–78–6; 61702–78–1; 61725–89–1; 61791–13–7; 61791–20–6; 61791–28–4; 61804–34–0; 61827–42–7; 61827–84–7; 62648–50–4; 63303–01–5; 63658–45–7; 63793–60–2; 64366–70–7; 64415–24–3; 64415–25–4; 64425–86–1; 65104–72–5; 65150–81–4; 66455–14–9: 66455–15–0; 67254–71–1; 67763–08–0; 68002–96–0; 68002–97–1; 68131–39–5; 68131–40–8; 68154–96–1; 68154–97–2; 68154–98–3; 68155–01–1; 68213–23–0; 68213–24–1; 68238–81–3; 68238–82–4; 68409–58–5; 68409–59–6; 68439–30–5; 68439–45–2; 68439–46–3; 68439–48–5; 68439–49–6; 68439–50–9; 68439–51–0; 68439–53–2; 68439–54–3; 68458–88–8; 68526–94–3; 68526–95–4; 68551–12–2; 68551–13–3; 68551–14–4; 68603–20–3; 68603–25–8; 68920–66–1; 68920–69–4; 68937–66–6; 68951–67–7; 68954–94–9; 68987–81–5; 68991–48–0; 69011–36–5; 69013–18–9; 69013–19–0; 69227–20–9; 69227–21–0; 69227–22–1; 69364–63–2; 70750–27–5; 70879–83–3; 70955–07–6; 71011–10–4; 71060–57–6; 71243–46–4; 72066–65–0; 72108–90–8; 72484–69–6; 72854–13–8; 72905–87–4; 73018–31–2; 73049–34–0; 74432–13–6; 74499–34–6; 78330–19–5; 78330–20–8; 78330–21–9; 78330–23–1; 79771–03–2; 84133–50–6; 85422–93–1; 97043–91–9; 97953–22–5; 102782–43–4; 103331–86–8; 103657–84–7; 103657–85–8; 103818–93–5; 103819–03–0; 106232–83–1; 111905–54–5; 116810–31–2; 116810–32–3; 116810–33–4; 120313–48–6; 120944–68–5; 121617–09–2; 126646–02–4; 126950–62–7; 127036–24–2; 139626–71–4; 152231–44– 2; 154518–36–2; 157627–86–6; 157627–88– 8; 157707–41–0; 157707–43–2; 159653–49– 3; 160875–66–1; 160901–20–2; 160901–09– 7; 160901–19–9; 161025–21–4; 161025–22– 5; 166736–08–9; 169107–21–5; 172588–43– 1; 176022–76–7; 196823–11–7; 287935–46– 0; 288260–45–7; 303176–75–2; 954108–36– 2).

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Inert ingredients Limits Uses

a-alkyl (minimum C6 linear, branched, saturated Not to exceed 30% of pes- Surfactants, related adjuvants of surfactants and/or unsaturated)-w-hydroxypolyoxyethylene ticide formulation. polymer with or without polyoxypropylene, mixture of di- and monohydrogen phosphate esters and the corresponding ammonium, calcium, magnesium, monoethanolamine, potassium, sodium and zinc salts of the phosphate esters; minimum oxyethylene content averages 2 moles; minimum oxypropylene content is 0 moles (CAS Reg. Nos. 9004–80–2, 9046–01–9, 26982–05–8, 31800–89–2, 37280–82–3, 39464–66–9, 39341–09–8, 39341–65–6, 39464–69–2, 42612–52–2, 50643–20–4, 50668–50–3, 51884–64–1, 52019–36–0, 57486–09–6, 58318–92–6, 59112–71–9, 60267–55–2, 61837–79–4, 62362–49–6, 63747–86–4, 63887–55–8, 66272–25–1, 67711–84–6, 67786–06–5, 67989–06–4, 68070–99–5, 68071–17–0, 68071–35–2, 68071–37–4, 68130–44–9, 68130–45–0, 68130–46–1, 68130–47–2, 68186–29–8, 68186–36–7, 68186–34–5, 68186–37–8, 68238–84–6, 68311–02–4, 68311–04–6, 68389–72–0, 68413–78–5, 68425–73–0, 68425–75–2, 68439–39–4, 68458–48–0, 68511–15–9, 68511–36–4, 68511–37–5, 68551–05–3, 68585–15–9, 68585–16–0, 68585–17–1, 68585–36–4, 68585–39–7, 68603–24–7, 68607–14–7, 68610–64–0, 68610–65–1, 68649–29–6, 68649–30–9, 68650–84–0, 68815–11–2, 68855–46–9, 68856–03–1, 68890–90–4, 68890–91–5, 68891–12–3, 68891–13–4, 68891–26–9, 68908–64–5, 68909–65–9, 68909–67–1, 68909–69–3, 68921–24–4, 68921–60–8, 68954–87–0, 68954–88–1, 68954–92–7, 68987–35–9, 69029–43–2, 69980–69–4, 70247–99–3, 70248–14–5, 70903–63–8, 71965–23–6, 71965–24–7, 72480–27–4, 72623–67–7, 72623–68–8, 72828–56–9, 72828–57–0, 73018–34–5, 73038–25–2, 73050–08–5, 73050–09–6, 73361–29–2, 73378–71–9, 73378–72–0, 73559–42–9, 73559–43–0, 73559–44–1, 73559–45–2, 74499–76–6, 76930–25–1, 78330–22–0, 78330–24–2, 91254–26–1, 93925–54–3, 96416–89–6, 103170–31–6, 103170–32–7, 106233–09–4, 106233–10–7, 108818–88–8, 110392–49–9, 111798–26–6, 111905–50–1, 116671–23–9, 117584–36–8, 119415–05–3, 121158–61–0, 121158–63–2, 125139–13–1, 125301–86–2, 125301–87–3, 126646–03–5, 129870–77–5, 129870–80–0, 130354–37–9, 136504–88–6, 143372–50–3, 143372–51–4, 154518–39–5, 154518–40–8, 155240–11–2, 160498–49–7, 160611–24–5, 171543–66–1, 210493–60–0, 246159–55–7, 251298–11–0, 261627–68–3, 317833–96–8, 422563–19–7, 873662–29–4, 936100–29–7, 936100–30–0, 1072943–56–6, 1187742–89– 7, 1187743–35–6). N-alkyl (C8-C18) primary amines and their ace- Concentration in formulated Surfactants, related adjuvants of surfactants tate salts where the alkyl group is linear and end-use products not to may be saturated and/or unsaturated (CAS exceed 10% by weight in Reg. Nos. 61790–57–6, 61790–58–7, 61790– herbicide products, 4% 59–8, 61790–60–1, 61788–46–3, 61790–33– by weight in insecticide 8, 68155–38–4). products, and 4% by weight in fungicide products.

Alkyl (C8-C18) sulfate and its ammonium, cal- ...... Surfactants. cium, isopropylamine, magnesium, potassium, sodium, and zinc salts. Aluminum hydroxide ...... Diluent, carrier

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Inert ingredients Limits Uses

Aluminum oxide ...... Diluent Aluminum stearate ...... Surfactant Amides, C5-C9, N-[3-(dimethylamino) propyl] ...... Surfactant (CAS Reg. No. 1044764–00–2). Amides, C6-C12, N-[3-(dimethylamino) propyl] ...... Surfactant (CAS Reg. No. 1044764–06–8). Ammonium bicarbonate ...... Surfactant, suspending agent, dispersing agent Ammonium carbamate ...... Synergist in aluminum phosphide formulations Ammonium chloride ...... Intensifier when used with ammonium nitrate as a dessicant or defoliant. Fire suppressant in aluminum phosphide and magnesium phosphide formulations Ammonium hydroxide...... Solvent, cosolvent, neutralizer, solubilizing agent Ammonium salts of fatty acids (C8-C18 satu- ...... Surfactant rated) (CAS Reg. No. 5972–76–9, 63718–65– 0, 16530–70–4, 32582–95–9, 2437–23–2, 191799–95–8, 16530–71–5, 93917–76–1, 5297–93–8, 94266–36–1, 1002–89–7). Ammonium stearate ...... Surfactant Ammonium sulfate ...... Solid diluent, carrier Ammonium thiosulfate ...... Intensifier when used with ammonium nitrate as desiccant or defoliant Amyl acetate ...... Solvent, cosolvent, attractant Ascorbyl palmitate ...... Preservative Attapulgite-type clay ...... Solid diluent, carrier, thickener Bacillus thuringiensis fermentation solids and/or ...... Diluent, carrier solubles. Bentonite ...... Solid diluent, carrier Benzoic acid ...... Preservative for formulation Bicyclo[3.1.1]hept–2–ene, 2,6,6–trimethyl–, ...... Surfactants, related adjuvants of surfactants homopolymer (Alpha-pinene, homopolymer)(CAS Reg. No. 25766–18–1). Bicyclo[3.1.1]heptane, 6,6–dimethyl–2–meth- ...... Surfactants, related adjuvants of surfactants ylene–, homopolymer (Beta-pinene, homopolymer) (CAS Reg. No. 25719–60–2). Bicyclo[3.1.1]hept–2–ene, 2,6,6–trimethyl–, poly- ...... Surfactants, related adjuvants of surfactants mer with 6,6– dimethyl–2– methylenebicyclo [3.1.1] heptane (Copolymer of alpha- and beta-pinene) (CAS Reg. No. 31393–98–3). 2-Bromo-2-nitro-1,3-propanediol (CAS Reg. No. 0.04% or less by weight of In-can preservative 52–51–7). the total pesticide formulation. Butane ...... Propellant n-Butanol (CAS Reg. No. 71–36–3) ...... Solvent, cosolvent Butylated hydroxyanisole ...... Antioxidant Butylated hydroxytoluene ...... Do. Calcareous shale ...... Solid diluent carrier Calcite ...... Do. Calcium carbonate ...... Do. Calcium chloride ...... Stabilizer Calcium phosphate ...... Solid diluent, carrier Calcium hydroxide ...... Do. Calcium hypochlorite ...... Sanitizing and bleaching agent Calcium lactate pentahydrate (CAS Reg. No...... Nutrient, stabilizer 5743–47–5). Calcium oxide ...... Solid diluent, carrier Calcium salt of partially dimerized rosin, con- ...... Coating agent forming to 21 CFR 172.210. Calcium silicate ...... Solid diluent, carrier Calcium stearate ...... Do. Carbon Dioxide (CAS Reg. No. 124–38–9) ...... None ...... Propellant Carrageenan, conforming to 21 CFR 172.620 .... Minimum molecular weight Thickener (in amu): 100,000. Cetyl alcohol (CAS Reg. No. 36653–82–4) ...... Not more than 5.0% of pes- Evaporation retardant ticide formulation. Charcoal, activated ...... Meets specifications in the Carrier Food Chemical Codex. Coconut shells ...... Solid diluent and carrier Cod liver oil ...... Solvent, cosolvent Croscarmellose sodium (CAS Reg. No. 74811– ...... Disintegrant, solid diluent, carrier, and thick- 65–7). ener n-Decyl alcohol (CAS Reg. No. 112–30–1) ...... Solvent or co-solvent

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Inert ingredients Limits Uses

Dialkyl (C8-C18) dimethyl ammonium chloride ..... Not more than 0.2% in sili- Flocculating agent in the manufacture of silica, ca, hydrated silica. hydrated silica for use as a solid diluent, carrier Diatomite (diatomaceous earth) ...... Solid diluent carrier Diethylaminoethanol, ethoxylated, propoxylated, ...... Surfactant reaction products with fatty acid dimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173188–75–4). Diethylaminoethanol, ethoxylated, propoxylated, ...... Surfactant reaction products with fatty acid trimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173188–83–4). Diethylaminoethanol, ethoxylated, reaction prod- ...... Surfactant uct with fatty acid dimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173188–72–1). Diethylaminoethanol, ethoxylated, reaction prod- ...... Surfactant ucts with fatty acid trimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173188–81–2). Diethylene glycol abietate ...... Surfactants, related adjuvants of surfactants 1,1-Difluoroethane (CAS Reg. No. 75–37–6) ..... For aerosol pesticide formu- Aerosol propellant lations used for insect control in food- and feed- handling establishments and animals. 1,2-Dihydro-6-ethoxy-2,2,4-trimethylquinolene .... Not more than 0.02% of Antioxidant pesticide formulation. Diisopropyl adipate (CAS Reg. No. 6938–94–9) 40% in mosquito control Solvent, co-solvent. formulations. Dimethyl adipate (CAS no. 627–93–0) ...... None ...... Solvent/co-solvent Dimethylaminoethanol, ethoxylated, ...... Surfactant propoxylated, reaction products with fatty acid dimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173188–42–5). Dimethylaminoethanol, ethoxylated, ...... Surfactant propoxylated, reaction products with fatty acid trimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173188–67–4). Dimethylaminoethanol, ethoxylated, reaction ...... Surfactant products with fatty acid dimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173188–38–9). Dimethylaminoethanol, ethoxylated, reaction ...... Surfactant products with fatty acid trimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173188–49–2). Dimethyl ether (methane, oxybis-) (CAS Reg...... Propellant No. 115–10–6). Dimethyl glutarate (CAS no. 1119–40–0) ...... None ...... Solvent/co-solvent 3,6-Dimethyl-4-octyn-3,6-diol ...... Not more than 2.5% of pes- Surfactants, related adjuvants of surfactants ticide formulation. Dimethyl succinate (CAS no. 106–65–0) ...... None ...... Solvent/co-solvent Dipropylene glycol ...... Solvent, cosolvent Disodium phosphate ...... Anticaking agent, conditioning agent Disodium zinc ethylenediaminetetraacetate ...... Sequestrant dihydride. Dolomite ...... Solid diluent, carrier Epoxidized linseed oil ...... Surfactants, related adjuvants of surfactants Epoxidized soybean oil ...... Do. Ethyl acetate ...... Solvent, cosolvent Ethyl alcohol ...... Do. Ethyl esters of fatty acids derived from edible ...... Solvent, cosolvent fats and oils. Ethyl maltol (CAS Reg. No.4940–11–8) ...... Not more than 0.2 % of the Odor masking agent pesticide formulation. Ethylene glycol (CAS Reg. No. 107–21–1) ...... Without limitation ...... Encapsulating agent for pesticides being applied post-harvest as residual, and crack and crevice sprays in and around food and nonfood areas of residential and nonresiden- tial structures, including food handling establishments

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Inert ingredients Limits Uses

Ethylene oxide adducts of 2,4,7,9-tetramethyl-5- ...... Surfactants, related adjuvants of surfactants decynediol, the ethylene oxide content averages 3.5, 10 or 30 moles (CAS Reg. No. 9014–85–1). (S,S)-Ethylenediamine disuccinic acid trisodium ...... Sequestrant or chelating agent salt (CAS Reg. No. 178949–82–1). Ethylenediaminetetraacetic acid ...... 3% of pesticide formulation Sequestrant Ethylenediaminetetraacetic acid, tetrasodium 5% of pesticide formulation Sequestrant salt. 2–Ethyl-1-hexanol (CAS Reg. No. 104–76–7) .... Not more than 10% of pes- Solvent, adjuvant of surfactants ticide. Fatty acids, conforming to 21 CFR 172.860 ...... Binder, defoaming agent, lubricant FD&C Blue No. 1 ...... Not more than 0.2% of pes- Dye ticide formulation. FD&C Red No. 40 (CAS Reg. No. 25956–17–6) Not to exceed 0.002% by Dye, coloring agent conforming to 21 CFR 74.340. weight of pesticide formulation. Ferric Citrate (CAS Reg. No. 2338–05–8) ...... Stabilizer Ferric sulfate ...... Solid diluent, carrier Furcelleran ...... Thickener D-glucopyranose, oligomeric, C10–16-alkyl ...... Surfactant glycosides (CAS Reg. No. 110615–47–9). Glycerides, edible fats and oils derived from ...... Emulsifier, dispersing agent plants and animals, reaction products with sucrose (CAS Reg. Nos. 100403–38–1, 100403–41–6, 100403–39–2, 100403–40–5). Glycerol mono-, di-, and triacetate ...... Solvent, cosolvent Glyceryl monostearate ...... Emulsifier Granite ...... Do. Graphite ...... Solid diluent, carrier Gum arabic (acacia) ...... Surfactant, suspending agent, dispersing agent Gypsum ...... Solid diluent, carrier Hexamethylenetetramine ...... For use in citrus washing Preservative solutions only at not more than 1%. 3-hexen-1-ol, (3Z)- (CAS Reg. No. 928-96-1) ..... Not more than 0.4% of the Odorant, alerting agent pesticide formulation. n-Hexyl alcohol (CAS Reg. No. 111–27–3) ...... Solvent, cosolvent C9 rich aromatic hydrocarbons (CAS Reg. No...... Solvent 64742–95–6). C10–11 rich aromatic hydrocarbons (CAS Reg...... Solvent No. 64742–94–5). C11–12 rich aromatic hydrocarbons (CAS Reg...... Solvent No. 64742–94–5). Hydrochloric acid ...... Solvent, neutralizer Hydroxyethylmorpholine, ethoxylated, ...... Surfactant propoxylated, reaction products with fatty acid dimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173189–06–4). Hydroxyethylmorpholine, ethoxylated, ...... Surfactant propoxylated, reaction products with fatty acid trimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173189–17–7). Hydroxyethylmorpholine, ethoxylated, reaction ...... Surfactant products with fatty acid dimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173189–00–8). Hydroxyethylmorpholine, ethoxylated, reaction ...... Surfactant products with fatty acid trimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173189–09–7). Hydroxyethylpiperidine, ethoxylated, ...... Surfactant propoxylated, reaction products with fatty acid dimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173189–22–4. Hydroxyethylpiperidine, ethoxylated, ...... Surfactant propoxylated, reaction products with fatty acid trimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173189–28–0).

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Inert ingredients Limits Uses

Hydroxyethylpiperidine, ethoxylated, reaction ...... Surfactant products with fatty acid dimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173189–20–2). Hydroxyethylpiperidine, ethoxylated, reaction ...... Surfactant products with fatty acid trimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173189–25–7). Hydroxyethylidine diphosphonic acid (HEDP) For use in antimicrobial Stabilizer, chelator (CAS Reg. No. 2809–21–4). pesticide formulations at not more than 1 percent. Iron oxide ...... Solid diluent, carrier Isobutane (CAS Reg. No. 75–28–5) ...... None ...... Propellant Isopropyl myristate (CAS Reg. No. 110–27–0) ...... Solvent Kaolinite-type clay ...... Solid diluent, carrier Lactic acid ...... Solvent Lactic acid, 2-ethylhexyl ester (CAS Reg. No...... Solvent 6283–86–9). Lactic acid, 2-ethylhexyl ester, (2S)- (CAS Reg...... Solvent No. 186817–80–1). Lactic acid, n-propyl ester, (S); (CAS Reg. No...... Solvent 53651–69–7). Lauryl alcohol ...... Surfactant Lignin (CAS Reg. No. 9005–53–2) ...... Surfactant, related adjuvants of surfactants Lignin, alkali (CAS Reg. No. 8068–05–1) ...... Do. Lignin, alkali, oxidized, sodium salt (CAS Reg...... Do. No. 68201–23–0). Lignin alkali reaction products with disodium sul- ...... Do. fite and formaldehyde (CAS Reg. No. 105859–97–0). Lignin alkali reaction products with formaldehyde ...... Do. and sodium bisulfite (CAS Reg. No. 68512– 35–6). Lignosulfonic acid (CAS Reg. No. 8062–15–5) ...... Do. Lignosulfonic acid, ammonium calcium salt ...... Do. (CAS Reg. No. 12710–04–2). Lignosulfonic acid, ammonium magnesium salt ...... Do. (CAS Reg. No. 123175–37–1). Lignosulfonic acid, ammonium salt (CAS Reg...... Do. No. 8061–53–8). Lignosulfonic acid, ammonium sodium salt (CAS ...... Do. Reg. No. 166798–73–8). Lignosulfonic acid, calcium magnesium salt ...... Do. (CAS Reg. No. 55598–86–2). Lignosulfonic acid, calcium salt (CAS Reg. No...... Do. 8061–52–7). Lignosulfonic acid, calcium sodium salt (CAS ...... Do. Reg. No. 37325–33–0). Lignosulfonic acid, ethoxylated, sodium salt ...... Do. (CAS Reg. No. 68611–14–3). Lignosulfonic acid, magnesium salt (CAS Reg...... Do. No. 8061–54–9). Lignosulfonic acid, potassium salt (CAS Reg...... Do. No. 37314–65–1). Lignosulfonic acid, sodium salt (CAS Reg. No...... Do. 8061–51–6). Lignosulfonic acid, sodium salt, oxidized (CAS ...... Do. Reg. No. 68855–41–4). Lignosulfonic acid, sodium salt, polymer with ...... Do. formaldehyde and phenol (CAS Reg. No. 37207–89–9). Lignosulfonic acid, sodium salt, sulfomethylated ...... Do. (CAS Reg. No. 68512–34–5). Lignosulfonic acid, zinc salt (CAS Reg. No...... Do. 57866–49–6). d-Limonene (CAS Reg. No. 5989–27–5) ...... Solvent, fragrance Magnesium carbonate ...... Anticaking agent, conditioning agent Magnesium chloride ...... Safener Magnesium lime ...... Solid diluent, carrier Magnesium oxide ...... Do. Magnesium silicate ...... Do. Magnesium stearate ...... Surfactant Magnesium sulfate ...... Solid diluent, carrier, safener Methyl alcohol ...... Solvent

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Inert ingredients Limits Uses

Methyl n-amyl ketone (CAS Reg. No. 110–43–0) ...... Solvent, cosolvent Methyl 5-(dimethylamino)-2-methyl-5- ...... Solvent oxopentanoate (1174627–68–9). Methyl esters of fatty acids derived from edible ...... Solvent, cosolvent fats and oils. Methyl esters of higher fatty acids conforming to ...... Antidusting agent, surfactant 21 CFR 573.640. Methyl isobutyl ketone ...... Solvent 2-methyl-2,4-pentanediol (CAS Reg. No. 107– Without limitation ...... Growing crops and food animals 41–5). 2-methyl-1,3-propanediol (CAS Reg. No. 2163– ...... Solvent, surfactant 42–0). Methylated silicones ...... Antifoaming agent Mono-, di-, and trimethylnapthalenesulfonic ...... Surfactants, related adjuvants of surfactants acids and napthalenesulfonic acids formaldehyde condensates, ammonium and sodium salts (CAS Reg. Nos 9008–63–3, 9069–80–1, 9084–06–4, 36290–04–7, 91078–68–1, 141959–43–5, 68425–94–5). Mica ...... Solid diluent, carrier Mineral oil, U.S.P., or conforming to 21 CFR ...... Diluent, carrier, and solvent 172.878 or 178.3620(a) (CAS Reg. No. 8012– 95–1). Monoammonium phosphate ...... No more than 3.75% by Postharvest fumigation in formulation with alu- weight in formulation. minum phosphide

Mono- and diglycerides of C 8-C18 fatty acids ...... Surfactants, related adjuvants of surfactants Montmorillonite-type clay ...... Solid diluent, carrier Nonyl, decyl, and undecyl glycoside mixture with ...... Surfactant. a mixture of nonyl, decyl, and undecyl oligosaccharides and related reaction products (primarily decanol and undecanol) produced as an aqueous-based liquid (50 to 65% solids) from the reaction of primary alcohols (containing 15 to 20% secondary alcohol isomers) in a ratio of 20% C9, 40% C10, and 40% C11 with carbohydrates (average glucose to alkyl chain ratio 1.3 to 1.8). a-(p-Nonylphenol)-w-hydroxypoly(oxyethylene) Not to exceed 7% of pes- Surfactants, related adjuvants of surfactants mixture of dihydrogen phosphate and ticide formulation. monohydrogen phosphate esters and the corresponding ammonium, calcium, magnesium, potassium, sodium, and zinc salts of the phosphate esters; the nonyl group is a propylene trimer isomer and the poly(oxyethylene) content averages 4–14 or 30 moles (CAS Reg. Nos. 51811–79–1, 59139–23–0, 67922–57–0, 68412–53–3, 68553–97–9, 68954–84–7, 99821–14–4, 152143–22–1, 51609–41–7, 37340–60–6, 106151–63–7, 68584–47–4, 52503–15–8, 68458–49–1). a-(p-Nonylphenyl)-w-hydroxypoly(oxyethylene) ...... Surfactants, related adjuvants of surfactants produced by the condensation of 1 mole of nonylphenol (nonyl group is a propylene trimer isomer) with an average of 4-14 or 30- 90 moles of ethylene oxide; if a blend of products is used, the average number of moles of ethylene oxide reacted to produce any product that is a component of the blend shall be in the range of 4-14 or 30-90. a-(p-Nonylphenol)-w-hydroxypoly(oxyethylene) Not to exceed 7% of pes- Surfactants, related adjuvants of surfactants sulfate, ammonium, calcium, magnesium, po- ticide formulation. tassium, sodium, and zinc salts the nonyl group is propylene trimer isomer and the poly(oxyethylene) content averages 4 moles (CAS Reg. Nos. 9014–90–8, 9051–57–4, 9081–17–8, 68649–55–8, 68891–33–8. 1-Octanal (CAS Reg. No. 124–13–0) ...... Not more than 0.2% of the Odor masking agent pesticide formulation. n-Octyl alcohol (CAS Reg. No. 111–87–5) ...... Solvent or co-solvent

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Inert ingredients Limits Uses

Octyl and decyl glucosides mixture with a mix- ...... Surfactants, related adjuvants of surfactants ture of octyl and decyloligosaccharides and related reaction products (primarily n- decanol) produced as an aqueous-based liquid (68-72% solids) from the reaction of straight chain alcohols (C8(45%), C10 (55%)) with anhydrous glucose. Oleic acid ...... Diluent Oleic acid diester of a-hydro-w-hydroxypoly ...... Surfactants, related adjuvants of surfactants (oxyethylene); the poly(oxyethylene) having average molecular weight (in amu) 400. a-Oleoyl-w-hydroxypoly(oxyethylene), average ...... Emulsifier molecular weight (in amu) of 600. Oleyl alcohol (CAS Reg. No. 143–28–2 ...... 15% ...... Cosolvent Oxalic acid ...... No more oxalic acid should Calcium chelating hard water inhibitor be used than is necessary to chelate calcium and in no case should more than 2 lb oxalic acid per acre be used. Palmitic acid ...... Diluent Pentaerythritol ester of maleic anhydride modi- ...... Plasticizer fied wood rosin. Petrolatum, conforming to 21 CFR 172.880 ...... Coating agent Petroleum hydrocarbons, light odorless con- ...... Solvent, diluent. forming to 21 CFR 172.884. Petroleum hydrocarbons, synthetic isoparaffinic, ...... Do. conforming to 21 CFR 172.882. Petroleum naphtha, conforming to 21 CFR ...... Component of coating agent 172.250(d). Petroleum wax, conforming to 21 CFR ...... Coating agent 172.886(d). Phosphoric acid ...... Buffer Polyethylene, conforming to 21 CFR ...... Binder, carrier, and coating agent 177.1520(c). Polyethylene glycol[a-hydro-w- ...... Surfactants, related adjuvants of surfactants hydroxypoly(oxyethylene)]; mean molecular weight (in amu) 194 to 9,500 conforms to 21 CFR 178.3750. Polyglycerol esters of fatty acids conforming to ...... Surfactants, related adjuvants of surfactants 21 CFR 172.854. Polyglyceryl phthalate ester of coconut oil fatty None ...... Surfactants, related adjuvants of surfactants acids, including fatty acid coco polymers with glyceryl and phthalic anhydride (CAS No. 67746–02–5) and coconut oil polymer with glyceryl and phthalic anhydride (CAS No. 66070–87–9). Poly(oxy-1,2-ethanediyl), a-(carboxymethyl)-w- ...... Surfactant (nonylphenoxy) produced by the condensation of 1 mole of nonylphenol (nonyl group is a propylene trimer isomer) with an average of 4- 14 or 30-90 moles of ethylene oxide. The molecular weight (in amu) ranges are 454-894 and 1598-4238. Poly(oxy-1,2-ethanediyl), a-[tris(1- For use in post-harvest ap- Surfactants phenylethyl)phenyl]-w-hydroxy-, (CAS Reg. plications; not to exceed No. 99734–09–5). 15% by weight in pesticide formulations. Polyoxyethylene (20) sorbitan monostearate ...... Surfactants, related adjuvants of surfactants [Poly[oxy(methyl-1,2-ethanediyl)], a-[2-bis(2-hy- Not to exceed 15% in the Surfactant droxyethyl)amino]propyl]-w-hydroxy,-ether with formulated product; only a-hydro-w-hydroxypoly(oxy-1,2-ethanediyl) for use with glyphosate. (1:2), mono-C12–16 alkyl ethers, (CAS Reg. No. 176022–82–5). Polysorbate 65, conforming to 21 CFR 172.838 ...... Emulsifier Potassium aluminum silicate ...... Solid diluent, carrier Potassium benzoate (Cas No. 582–25–2) ...... None ...... Preservative Potassium hydroxide ...... Neutralizer Potassium phosphate ...... Buffer Potassium sulfate ...... Solid diluent Propane ...... Propellant 1,3-Propanediol (CAS Reg. No. 504–63–2) ...... Solvent, co-solvent, diluent, or freeze-point de- pressant

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Inert ingredients Limits Uses

2-Propanol, 1,1′,1″-nitrilotris- (CAS No. 122–20– Without limitation ...... Neutralizer 3). n-Propanol ...... Solvent, cosolvent 2-Propenoic acid, 2-methyl-, polymer with ethyl ...... Encapsulating agent, dispensers, resins, fibers 2-propenoate and methyl 2-methyl-2- and beads propenoate, ammonium salt (CAS Registra- tion No. 55989–05–4), minimum number average molecular weight (in amu), 18,900.. Propylene glycol ...... Solvent, cosolvent. Propylene glycol alginate (as defined in 21 CFR ...... Defoaming agent 172.858). Propyl gallate ...... Antioxidant Propyl p-hydroxybenzoate ...... Preservative for formulations Pyrophyllite ...... Solid diluent, carrier Rhizobium inoculants (e.g. Sinorhizobium, ...... All leguminous food commodities Bradyrhizobium & Rhizobium). Rosin, partially dimerized (as defined in 21 CFR ...... Surfactants, related adjuvants of surfactants 172.615). Rosin, partially hydrogenated (as defined in 21 ...... Do. CFR 172.615). Rosin, wood ...... Do. Salts of fatty acids, conforming to 21 CFR ...... Binder, emulsifier, anticaking agent 172.863. Sand ...... Solid diluent, carrier Shellac, bleached; refined, food grade, arsenic ...... Coating agent and rosin-free. Silver nitrate (Cas Reg. No. 7761–88–8) ...... For use on potatoes as Stabilizer post-harvest treatment to control sprouting at no more than 0.06% by weight in pesticide formulations. Soapstone ...... Solid diluent Sodium acid pyrophosphate ...... Surfactant, suspending agent, dispersing agent, buffer Sodium alkyl naphthalenesulfonates (CAS Reg. Limited to no more than Surfactants, related adjuvants of surfactants Nos. 68909–83–1, 68909–84–2, 68909–82–0, 30% by weight in pes- 27213–90–7, 26264–58–4, 27178–87–6, ticide end-use products. 111163–74–7, 908356–16–1, 25417–20–3, 25638–17–9, 145578–88–7, 1322–93–6, 1323–19–9, 7403–47–6, 68442–09–1, 127646–44–0, 908356–18–3). Sodium aluminum silicate ...... Solid diluent, carrier Sodium dioctylsulfosuccinate ...... Surfactants, related adjuvants of surfactants Sodium 1,4-dihexyl sulfosuccinate (CAS Reg...... Surfactants, related adjuvants of surfactants No. 3006–15–3). Sodium 1,4-diisobutyl sulfosuccinate (CAS Reg...... Surfactants, related adjuvants of surfactants No. 127–39–9). Sodium 1,4-dipentyl sulfosuccinate (CAS Reg...... Surfactants, related adjuvants of surfactants No. 922–80–5). Sodium hexametaphosphate...... Surfactant, emulsifier, wetting agent, suspending agent, dispersing agent, buffer Sodium hydroxide ...... Neutralizer Sodium metasilicate ...... Surfactants, emulsifiers, wetting agents, dispersing agents, buffer Sodium monoalkyl and dialkyl (C6-C16) Not to exceed 20% in pes- Surfactants, related adjuvants of surfactants phenoxy benzenedisulfonates and related ticide formulations. acids (CAS Reg. Nos. 147732–59–0, 147732– 60–3, 169662–22–0, 70191–75–2, 36445–71– 3, 39354–74–0, 70146–13–3, 119345–03–8, 149119–20–0, 149119–19–7, 119345–04–9, 28519–02–0, 25167–32–2, 30260–73–2, 65143–89–7, 70191–76–3). Sodium a-olefinsulfonate (sodium C14-C16) ...... Surfactants, related adjuvants of surfactants (Olefin sulfonate). SodiumN-oleoyl- N-methyl taurine (CAS Reg...... Surfactants, related adjuvants of surfactants No. 137–20–2). Sodium and potassium salts of N-alkyl (C8–C18)- Concentration in formulated Surfactants, related adjuvants of surfactants beta-iminodipropionic acid where the C8–C18 end-use products not to is linear and may be saturated and/or unsatu- exceed 30% by weight in rated (CAS Reg. Nos. 110676–19–2, 3655– pesticide formulations. 00–3, 61791–56–8, 14960–06–6, 26256–79– 1, 90170–43–7, 91696–17–2, 97862–48–1). Sodium salt of sulfated oleic acid ...... Surfactants, related adjuvants of surfactants

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Inert ingredients Limits Uses

Sodium silicate ...... Surfactant, emulsifier, wetting agent, stabilizer, inhibitor Sodium starch glycolate (CAS Reg. No. 9063– Granular and tableted prod- Disintegrant 38–1). ucts only; not to exceed 8% of the formulated product. Sodium sulfate ...... Solid diluent, carrier Sodium tripolyphosphate...... Buffer, surfactant, suspending agent, dispersing agent, anticaking agent, conditioning agent Sorbic acid (CAS Reg. No. 110–44–1) ...... Preservative for formulations Sorbitan fatty acid esters (fatty acids limited to ...... Surfactants, related adjuvants or surfactants. C12, C14, C16, and C18 containing minor amounts of associated fatty acids) and their derivatives; the poly(oxyethylene) content averages 5-20 moles. Soybean flour ...... Expires May 24, 2005...... Surfactant Soybean oil-derived fatty acids ...... Solvent, cosolvent Stearic acid ...... Diluent a-Stearoyl-w-hydroxypoly(oxyethylene), average ...... Emulsifier molecular weight (in amu) of 600. a-Stearoyl-w-hydroxypoly(oxyethylene); the ...... Surfactants, related adjuvants of surfactants poly(oxyethylene) content averages either 8, 9, or 40 moles; if a blend of products is used, the average number of moles ethylene oxide reacted to produce any product that is a component of the blend shall be either 8, 9, or 40. Sucrose octaacetate ...... Adhesive Sulfite liquors and cooking liquors, spent, ...... Surfactant, related adjuvants of surfactants oxidized (CAS Reg. No. 68514–09–0). Sulfuric acid (CAS Reg. No.7664–93–9) ...... Not to exceed 10% of the pH Control agent pesticide formulation; non-aerosol formulations only. Synthetic paraffin and its succinic derivatives ...... Carrier, binder, and carrying agent conforming to 21 CFR 172.275. Synthetic petroleum wax, conforming to 21 CFR ...... Binder, carrier, and coating agent 172.888. Talc ...... Solid diluent, carriers Tall oil; fatty acids not less than 58%, rosin ...... Surfactants, related adjuvants of surfactants acids not more than 44%, unsaponifiables not more than 8%. Tartrazine ...... Dye Terpenes and terpenoids, turpentine oil, alpha- ...... Surfactants, related adjuvants of surfactants pinene fraction, polymd. (CAS Reg. No. 70750–57–1). 1,1,1,2-Tetrafluoroethane, (CAS Reg. No. 811– ...... Aerosol propellant 97–2). Tetrahydrofurfuryl alcohol (THFA) (CAS Reg. No Expires February 9, 2008 ... Solvent/cosolvent 97–99–4). N,N,N′,N″,-tetrakis-(2-hydroxypropyl) ethylene- Concentration in formulated Stabilizer for formulation. diamine (CAS Reg. No. 102–60–3). end-use products not to exceed 20% by weight in pesticide formulations. a-[p-(1,1,3,3-tetramethylbutyl)phenyl]-w- Not to exceed 7% of pes- Surfactants related adjuvants of surfactants hydroxypoly(oxyethylene) produced by the ticide formulation. condensation of 1 mole of p-(1,1,3,3- tetramethylbutyl)phenol with a range of 1–14 or 30–70 moles of ethylene oxide: If a blend of products is used, the average range number of moles of ethylene oxide reacted to produce any product that is a component of the blend shall be in the range of 1–14 or 30– 70 (CAS Reg. Nos. 9036–19–5, 9002–93–1). 2,4,7,9-Tetramethyl-5-decyn-4, 7-diol ...... Not more than 2.5% of pes- Surfactants, related adjuvants of surfactants ticide formulation. Tetrasodium pyrophosphate ...... Anticaking agent, conditioning agent Thiosulfuric acid, disodium salt, anhydrous...... Dechlorinator, reducing agent (CAS Reg. No 7772–98–7). Thiosulfuric acid, disodium salt, pentahydrate...... Do. (CAS Reg. No. 10102–17–7). d-Alpha tocopherol (CAS Reg. No. 9–02–9 ...... None ...... Safener d-Alpha tocopheryl acetate (CAS Reg. No. 58– None ...... Do. 95–7).

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Inert ingredients Limits Uses

dl-Alpha tocopherol (CAS Reg. No.10191–41–0) None ...... Do. dl-Alpha tocopheryl acetate (CAS Reg. No. None ...... Do. 7695–91–2). Tricalcium phosphate ...... Surfactant, suspending agent, dispersing agent, anticaking agent, conditioning agent Trisodium phosphate ...... Surfactant, emulsifier, wetting agent Vermiculite ...... Solid diluent, carrier. Vitamin E (CAS Reg. No. 1406–18–4) ...... None ...... Safener Walnut shells ...... Leaching inhibitor, binder for water-dispersible aggregates, sticker and suspension stabilizer Wintergreen oil ...... Attractant Wood flour ...... Derived from wood free of Solid diluent and carrier chemical preservatives. Xanthan gum-modified, produced by the reac- Not more than 0.5% of pes- Surfactant tion of xanthan gum and glyoxal (maximum ticide formulation. 0.3% by weight). Xylene meeting the specifications listed in 21 In pesticide formulations for Solvent, cosolvent CFR 172.884(b)(4). grain storage only. Zeolite (hydrated alkali aluminum silicate) ...... Solid diluent, carrier Zinc oxide ...... Coating agent Zinc sulfate (basic and monohydrate) ...... Do. Zinc sulfate (basic and monohydrate) ...... Solid diluent, carrier

[69 FR 23117, Apr. 28, 2004]

EDITORIAL NOTE: For FEDERAL REGISTER citations affecting § 180.910, see the List of CFR Sections Affected, which appears in the Finding Aids section of the printed volume and at www.fdsys.gov.

§ 180.920 Inert ingredients used pre- when used in accordance with good ag- harvest; exemptions from the re- ricultural practice as inert (or occa- quirement of a tolerance. sionally active) ingredients in pesticide The following materials are exempt- formulations applied to growing crops ed from the requirement of a tolerance only:

Inert ingredients Limits Uses

Acetophenone ...... Attractant Adenosine (CAS Reg. No. 58–61–7) ...... Maximum of 0.5% of formu- Synergist lation. Alder bark ...... Seed germination stimulator

Alkyl (C12-C16) dimethyl ammonio acetate (CAS 20% by weight in pesticide Surfactant Reg. Nos. 683–10–3, 2601–33–4 and 693– formulation. 33–4.

a-Alkyl (minimum C6 linear, branched, saturated Not to exceed 30% of pes- Surfactants, related adjuvants of surfactants and/or unsaturated)-w-hydroxypolyoxyethylene ticide formulation. polymer with or without polyoxypropylene, mixture of di- and monohydrogen phosphate esters and the corresponding ammonium, calcium, magnesium, monoethanolamine, potassium, sodium, and zinc salts of the phosphate esters; minimum oxyethylene content is 2 moles; minimum oxypropylene content is 0 moles (CAS Reg. Nos. 9046–01–9, 37280– 82–3, 39464–66–9, 42612–52–2, 50643–20– 4, 52019–36–0, 58318–92–6, 60267–55–2, 61837–79–4, 67711–84–6, 68070–99–5, 68071–35–2, 68071–17–0, 68130–47–2, 68186–37–8, 68186–36–7, 68311–02–4, 68425–73–0, 68458–48–0, 68511–37–5, 68610–65–1, 68585–36–4, 68649–29–6, 68815–11–2, 68908–64–5, 68891–13–4, 73038–25–2, 78330–24–2, 108818–88–8, 154518–39–5, 317833–96–8, 873662–29–4, 936100–29–7, 936100–30–0).

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Inert ingredients Limits Uses

N-alkyl(C8-C18) dimethylamidopropylamines Not to exceed 20% by Surfactants, related adjuvants of surfactants where the alkyl group is linear and may be weight in herbicide formu- saturated and/or unsaturated (CAS Reg. Nos. lations. 109–28–4, 3179–80–4, 7651–02–7, 22890– 10–4, 22890–11–5, 39669–97–1, 45267–19– 4, 68140–01–2, 1147459–12–8, 146987–98– 6). N-alkyl (C8-C18) primary amines and their ace- Concentration in formulated Surfactants, related adjuvants of surfactants tate salts where the alkyl group is linear and end-use products not to may be saturated and/or unsaturated (CAS exceed 10% by weight in Reg. Nos. 61790–57–6, 61790–58–7, 61790– herbicide products, 4% 59–8, 61790–60–1, 61788–46–3, 61790–33– by weight in insecticide 8, 68155–38–4). products, and 4% by weight in fungicide products. N,N-Bis-a-ethyl-w-hydroxypoly(oxy-1,2- Not to exceed 25% in herbi- Surfactants, related adjuvants of surfactants ethanediyl) C8–C18 saturated and unsatu- cide formulations and rated alkylamines; the poly(oxy-1,2-ethanediyl) 10% in insecticide and content is 2–60 moles (CAS Reg. Nos. fungicide formulations. 10213–78–2, 25307–17–9, 26635–92–7, 26635–93–8, 288259–52–9, 58253–49–9, 61790–82–7, 61791–14–8, 61791–24–0, 61791–26–2, 61791–31–9, 61791–44–4, 68155–33–9, 68155–39–5, 68155–40– 8,70955–14–5, 73246–96–5, 1266162–49–5). N,N–Bis-a-ethyl-w-hydroxypoly(oxy-1,2- Not to exceed 25% in herbi- Surfactants, related adjuvants of surfactants ethanediyl/oxy(methyl-1,2-ethanediyl) C8-C18 cide formulations and saturated and unsaturated alkylamines; the 10% in insecticide and poly(oxy-1,2-ethanediyl/oxy(methyl-1,2- fungicide formulations. ethanediyl) content is 2–60 moles (CAS Reg. Nos. 68213–26–3, 68153–97–9, 75601–76–2). Aluminum sulfate ...... Safener adjuvant Ammonium chloride (CAS Reg. No. 12125–02– ...... Carrier/nutrient 9). Ammonium formate (CAS Reg. No. 540–69–2) ...... Complexing or fixing agent Ammonium nitrate (CAS Reg. No. 6484–52–2) ...... Adjuvant/ intensifier for herbicides Ammonium polyphosphate (CAS Reg. No...... Sequestrant, buffer, or surfactant 68333–79–9). Barium sulfate ...... Carrier 1,4-Benzenedicarboxylic acid, dimethyl ester, For use in honeybee hive Component of controlled release agent polymer with 1,4-butanediol, adipic acid, and miticide formulations. hexamethylene diisocyanate, minimum number average molecular weight (in amu) 30,000 (CAS Reg. No. 55231–08–8). 1,2-Benzisothiazolin-3-one ...... Not more than 0.1% of for- Preservative/stabilizer mulation. Not more than 0.02 lb to be applied per acre. Boric acid ...... Sequestrant Buffalo gourd root powder (Cucurbita No more than 2.5 lbs/acre/ Gustatory stimulant foetidissima root powder); or, Zucchini juice season (3.4 gm/acre/sea- (Cucurbita pepo juice) or Hawkesbury melon son of Cucurbitacin). Citrullus lanatus.. Butyl stearate ...... Defoamer g-Butyrolactone ...... Solvent C.I. Pigment Blue #15 (CAS Reg. No. 147–14– For seed treament use only Dye, coloring agent 8; containing no more than 50 ppm poly- chlorinated biphenyls (PCBs)). C.I. Pigment Green #7 (CAS Reg. No. 1328– For seed treatment use Dye, coloring agent 53–6; containing no more than 50 ppm poly- only. chlorinated biphenyls (PCBs)). C.I. Pigment Violet #23 (CAS Reg. No. 6358– For seed treatment use Dye, coloring agent 30–1; containing no more than 20 ppb of poly- only. chlorinated dibenzo-p-dioxins and/or poly- chlorinated dibenzofurans). Calcium gluconate (CAS Reg. No. 299–28–5) ...... Sequestrant Camphor (CAS Reg. No. 76–22–2) ...... Not more than 5% weight to Deodorant, melting point adjustment weight (w/w) of pesticide formulations. Carbon Black (CAS Reg. No. 1333–86–4) ...... For seed treatment use Colorant only. Carbonic acid, dipotassium salt (CAS Reg. No...... Buffering agent 584–08–7).

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Inert ingredients Limits Uses

Carbonic acid, dipotassium salt, trihydrate (CAS ...... Buffering agent Reg. No. 18662–52–7). Carboxymethyl guar gum sodium salt (CAS Without limitation ...... Thicker/drift reduction agent Reg. No. 39346–76–4). Carboxymethyl-hydroxypropyl guar (CAS Reg. Without limitation ...... Thicker/drift reduction agent No. 68130–15–4). Carous chloride ...... 10 ppm in formulation ...... Tagging agent Carrageenan, conforming to 21 CFR 172.260 .... Not more than 0.15% of Thickener and stabilizer for pesticide formula- pesticide formulation. tions applied to seeds before planting Chlorobenzene ...... Contains not more than 1% Solvent, cosolvent impurities. Not for use after edible parts of plant begin to form. Do not graze livestock in treated areas within 48 hours after application. 5-Chloro-2-methyl-4-isothiazolin-3-one (in com- Not more than 0.0022% Preservative bination with 2-methyl-4-isothiazolin-3-one). (22.5 ppm) in the formulation; 0.00022% (or 2.25 ppm) in the final solution applied to growing crops. Choline chloride (CAS Reg. No. 67–48–1) ...... As a solvent Choline hydroxide (CAS Reg No. 123–41–1) ..... Without limitation ...... Neutralizer Cis-isomer of 1-(3-chloroallyl)-3,5,7-triaza-1- Maximum of 0.14% by Preservative azoniaadamantane chloride (CAS Reg. No. weight of formulation. 51229–78–8). Copper naphthenate ...... Not more than 2.5% of for- Mercaptan scavenger in technical pesticide mulation; application limited to before edible por- tions of plants begin to form. Cyclohexane ...... Solvent, cosolvent Cyclohexanone ...... Do. Cysteine (CAS Reg. No. 52–90–4) ...... Maximum of 0.5% of formu- Synergist lation. D&C Green No. 6 ...... Dye D&C Red No. 17, technical grade ...... Dye D&C Red No. 33 (CAS Reg. No. 3567–66–6); ...... Dye meeting the specifications listed in 21 CFR 74.1333. D&C Violet No. 2, technical grade ...... Not more than 0.005% of Dye pesticide formulation. Decanamide, N,N-dimethyl (CAS Reg. No...... Emulsifier, solvent, cosolvent 14433–76–2). Diammonium phosphate (CAS Reg. No. 7783– ...... Buffer, surfactant 28–0). dibenzylidene sorbitol (32647–67–9) ...... Thinning agent Diethanolamine ...... Stabilizer, inhibitor for formulations used before crop emerges from soil

Diethanolamine salts of alkyl (C8-C24) Not to exceed 7% of pes- Surfactants, related adjuvants of surfactants. benzenesulfonic acid (CAS Reg. Nos. 26545– ticide formulation. 53–9, 67815–95–6, 67889–94–5, 67889–95– 6, 68259–34–7, 68478–47–7, 68567–68–0, 68815–34–9, 68815–37–2, 68891–02–1, 68953–97–9, 84989–15–1, 85338–09–6, 90194–39–1, 90194–40–4, 90218–08–9). Diethylene glycol ...... Deactivator, adjuvant for formulations used before crop emerges from soil Diethylene Glycol (CAS No. 111–46–6) ...... Without limitation ...... Solvent, stabilizer and/or antifreeze Diethylene glycol and diethylene glycol ...... Deactivator for formulations used before crop monobutyl, monoethyl, and monomethyl emerges from soil, stabilizer ethers. Diethylene glycol mono butyl ether (CAS Reg. Without limitation ...... Pesticide inert ingredient as a solvent, sta- No. 112–34–5). bilizer and/or antifreeze Diethylene Glycol MonoEthyl Ether (CAS Reg. Without limitation ...... Solvent, stabilizer and/or antifreeze No. 111–90–0).

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Inert ingredients Limits Uses

Dimethylaminopropylamine, isopropylamine, eth- ...... Surfactants, related adjuvants of surfactants. anolamine, and triethanolamine salts of alkyl (C8-C24) benzenesulfonic acid (CAS Reg. Nos. 3088–30–0, 12068–12–1, 26264–05–1, 26836–07–7, 27323–41–7, 55470–69–4, 58089–99–9, 61886–59–7, 61931–76–8, 67924–05–4, 68110–32–7, 68259–35–8, 68411–31–4, 68442–72–8, 68567–69–1, 68584–24–7, 68584–25–8, 68648–81–7, 68648–96–4, 68649–00–3, 68815–30–5, 68815–35–0, 68910–32–7, 68953–93–5, 68953–98–0, 70528–84–6, 72391–21–0, 84961–74–0, 85480–55–3, 85480–56–4, 85995–82–0, 90194–42–6, 90194–53–9, 90194–54–0, 90194–55–1, 90218–09–0, 90218–11–4, 90218–35–2, 96687–54–6, 99924–49–9, 121617–08–1, 157966–96–6, 193562–36–6, 319926–68–6, 877677–48–0, 1093628–27–3). 3,6-Dimethyl-4-octyn-3,6-diol ...... In pesticide formulations, Surfactants, related adjuvants of surfactants for soil prior to planting or to plants before edible parts form. Dimethyl sulfoxide ...... Solvent or cosolvent for formulations used before crop emerges from soil or prior to formation of edible parts of food plants Dipotassium hydrogen phosphate ...... Buffering agent Dipropylene glycol monomethyl ether ...... Stabilizer Douglas-fir bark, ground ...... Solid diluent, carrier Dysprosium chloride ...... 10 ppm in formulation ...... Tagging agent 1,2-ethanediamine,N,N,N″, N″-tetramethyl-, poly- For use in pesticide formu- Adjuvant or water conditioner mer with 1,1′-oxybis[2-chloroethane] (CAS lations applied to cotton Reg. No. 31075–24–8). or wheat only. (S,S)–Ethylenediaminedisuccinic acid (CAS ...... Sequestrant or chelating agent Reg. No. 20846–91–7). Ethylene glycol ...... Antifreeze, deactivator for all pesticides used before crop emerges from soil and in herbicides before or after crop emerges Ethylene glycol (CAS Reg. No. 107–21–1) ...... Without limitation ...... Pesticide inert ingredient as a solvent, stabilizer and/or antifreeze. Ethylene glycol monobutyl ether ...... 2-Ethylhexanol ...... Cosolvent, defoamer, solvent for all pesticides used before crop emerges from soil and in herbicides before or after crop emerges Europic chloride ...... 10 ppm in formulation ...... Tagging agent FD&C Blue No. 1 (CAS Reg. No. 3844–45–9) ... For seed treatment use Dye, coloring agent only. FD&C Blue No. 1, methyl-polyethylene glycol For seed treatment use Dye, coloring agent derivative (CAS Reg. No. 9079–34–9). only; Number average molecular weight (in amu) is greater than 1,000; Not to exceed 5% of the formulated pesticide product. FD&C Blue No. 1, polyethylene glycol derivative For seed treatment use Dye, coloring agent (CAS Reg. No. 9079–33–8). only; Number average molecular weight (in amu) is greater than 1,000; Not to exceed 5% of the formulated pesticide product. FD&C Red No. 40 (CAS Reg. No. 25956–17–6) For seed treatment use Dye, coloring agent only. Not to exceed 2% by weight of the pesticide formulation. Ferric chloride ...... Not greater than 2% of suspending, dispersing agent, pesticide formulation Fluoroapatite ...... Solid diluent, carrier Folic acid (CAS Reg. No. 59–30–3) ...... Maximum of 0.5% of formu- Synergist lation. Gluconic acid (and sodium salt) ...... Sequestrant l-Glutamic acid (C5 H9 NO4´ CAS Reg. No. 56– Seet treatment use only ..... Plant nutrient 86–0). [alpha]-D-glucopyranoside, 2-ethylhexyl 6-O- ...... Surfactant [alpha]-D glucopyranosyl- (CAS Reg. No. 330980–61–5).

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Inert ingredients Limits Uses

[alpha]-D-glucopyranoside, 2-ethylhexyl (CAS ...... Surfactant Reg. No. 125590–73–0). Glutamine (CAS Reg. No. 56–85–9) ...... Maximum of 0.5% of formu- Synergist lation. Glycerol—propylene oxide polymer (CAS Reg...... Component in water-soluble film No. 25791–96–2). Glyceryl triacetate ...... Stabilizer Glyceryl tris-12-hydroxystearate ...... Flow control agent Graphite ...... Treatment aid for seeds Guar hydroxypropyltrimethylammonium chloride ...... Thickener/drift reduction agent (CAS Reg. No. 71329–50–5). Hexamethylenetetramine ...... Stabilizer for carriers in solid pesticide formulations 2-(2’-hydroxy-3’,5’-di-tert-amylphenyl) Maximum concentration of Ultraviolet (UV) stabilizer benzotriazole (CAS Reg. No. 25973–55–1). 0.6% in insecticide formulations applied to adzuki beans, canola, chickpeas, cotton, faba beans, field peas, lentils, linola, linseed, lucerne, lupins, mung beans, navy beans, pigeon peas, safflower, sunflower, and vetch. 2-Hydroxy-4-n-octoxybenzophenone (CAS Reg. Not more than 0.2 pt of Light stabilizer No. 1843–05–6). pesticide formulation. Hydroxypropyl guar gum ...... Thickener Isobornyl acetate ...... Solvent Isobutyl alcohol ...... Do. Isobutylene-butene copolymers ...... For soil application only ...... Binder Isooctadecanol ...... Not more than 2% of pes- Defoaming agent ticide formulation. Lanthanum chloride ...... 10 ppm in formulation ...... Tagging agent. Magnesium nitrate (in combination with 2-meth- None ...... Preservation yl-4-isothiazolin-3-one and 5-chloro-2-methyl- 4-isothiazolin-3-one). Maleic acid and maleic anhydride ...... For pesticide formulations Stabilizer applied to apples with a minimum preharvest interval of 21 days. Manganese carbonate ...... Plant nutrient D-mannose (CAS Reg. No. 3458–28–4) ...... Sequestrant, binder, filler Mesityl oxide ...... Not for use after edible Solvent, cosolvent parts of plant begin to form. Do not graze livestock in treated areas within 48 hours after application. Methionine (CAS Reg. No. 59–51–8) ...... Maximum of 0.5% of formu- Synergist lation. Methyl alcohol ...... Do. Methyl ethyl ketone ...... Surfactant Methyl p- hydroxybenzoate ...... Preservative for formulations Methyl isobutyl ketone ...... Solvent, cosolvent 2-Methyl-4-isothiazolin-3-one (in combination Not more than 0.0022% Preservative with 5-chloro-2-methyl-4-isothiazolin-3-one). (22.5 ppm) in the formulation; 0.00022% (or 2.25 ppm) in the final solution applied to growing crops. Mono-, di-, and trimethylnapthalenesulfonic ...... Surfactants, related adjuvants of surfactants acids and napthalenesulfonic acids formaldehyde condensates, ammonium and sodium salts (CAS Reg. Nos. 9008–63–3, 9069–80–1, 9084–06–4, 36290–04–7, 91078–68–1, 141959–43–5, 68425–94–5). Methyl oleate ...... Surfactant 2-Methyl-2,4-pentanediol ...... Solvent for formulations used before crop emerges from soil

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Inert ingredients Limits Uses

Methyl poly(oxyethylene)C8–C18 alkylammonium Concentration in formulated Surfactants, related adjuvants of surfactants chlorides where the poly(oxyethylene) content end use products not to is n=2–15 and where C8–C18 alkyl is linear exceed 10% by weight in and may be saturated or unsaturated (CAS herbicide products and Reg. Nos. 3010–24–0, 18448–65–2, 70750– 5% by weight in all other 47–9, 22340–01–8, 67784–77–4, 64755–05– pesticide products. 1, 61791–10–4, 28724–32–5, 28880–55–9, 68187–69–9, 68607–27–2, 60687–90–3. N-Methylpyrrolidone (CAS Reg. No. 872-504) ...... Solvent, cosolvent Mixed phytosterols (consisting of campesterol, ...... Surfactant sitosterol and stigmasterol, with minor amounts of associated plant sterols) derived from edible vegetable oils. Mono- and bis-(1H, 1H, 2H, 2H-perfluoroalkyl) Not more than 0.5% of pes- Surfactant, related adjvants of surfactants phosphates where the alkyl group is even ticide formulation. Expires numbered and in the C6-C12 range. February 9, 2008. Mono- and dialkyl (C8-C18) methylated ammo- ...... Surfactants, related adjuvants of surfactants nium chloride compounds, where the alkyl group(s) (C8-C18) are derived from coconut, cottonseed, soya, tallow, or hogfat fatty acids. Morpholine 4-C6-12 Acyl Derivatives (CAS Reg...... As a solvent No. 887947–29–7). Nicotinamide (CAS Reg. No. 98–92–0) ...... Maximum of 0.5% of formu- Synergist lation. a-(p-Nonylphenyl)-w-hydroxypoly(oxyethylene); ...... Surfactant produced by the condensation of 1 mole of nonylphenol (nonyl group is a propylene trimer isomer) with an average of 4-14 or 30- 100 moles of ethylene oxide; if a blend of products is used, the average number of moles of ethylene oxide reacted to produce any product that is a component of the blend shall be in the range 4-14 or 30-100. Octanamide, N,N-dimethyl (CAS Reg. No...... Emulsifier, solvent, cosolvent 1118–92–9). a-Oleoyl-w-(oleoyloxy) poly(oxyethylene) derived ...... Component of defoamers from a-hydro-w-hydroxypoly(oxyethylene) (molecular weight 600 amu). Oxo-decyl acetate (CAS reg. No. 108419–33–6) ...... Solvent Oxo-heptyl acetate (CAS Reg. No. 90438–79–2) ...... Solvent Oxo-hexyl acetate (CAS Reg. No. 88230–35–7) ...... Solvent Oxo-nonyl acetate (CAS Reg. No. 108419–34– ...... Solvent 7). Oxo-octyl acetate (CAS Reg. No. 108419–32–5) ...... Solvent Oxo-tridecyl acetate (CAS Reg. No. 108419– ...... Solvent 35–8). Phenol ...... Solvent, cosolvent Phenol, 2-(2H-benzotriazole-2-yl)-6-dodecyl-4- Maximum concentration of Ultraviolet (UV) stabilizer methyl; (CAS Reg. No. 23328–53–2). 0.6% in insecticide formulations applied to adzuki beans, canola, chickpeas, cotton, faba beans, field peas, lentils, linola, linseed, lucerne, lupins, mung beans, navy beans, pigeon peas, safflower, sunflower, and vetch. Phenolsulfonic acid—formaldehyde—urea con- Applied to growing plants Dispersant surfactant densate and its sodium salt. only. (Phthalocyaninato (2)) copper; (C.I. pigment When used as a colorant in Coloring agent, pigment blue No. 15). low-density plastic films. Pigment red 48 ...... For seed treatment use Dye only. a-Pinene ...... Not more than 2% of formu- Stabilizer lation by weight. Poly(oxy-1,2-ethanediyl), a-isotridecyl-w- At a maximum of 10% in Surfactant methoxy (CAS Reg. No. 345642–79–7). formulation. Poly(oxyethylene) adducts of mixed phytosterols ...... Surfactant, related adjuvants (such sterols to consist of campesterol, stigmasterol and sitosterol with minor amounts of associated plant sterols) derived from edible vegetable oils; polyoxyethylene content averaging 5-26 moles.

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Inert ingredients Limits Uses

Polyoxyethylene polyoxypropylene mono(di-sec- Limited to herbicide formu- Surfactants, related adjuvants of surfactants butylphenyl) ether (CAS Reg. No. 69029–39– lations only, and to no 6). more than 30% by weight in herbicide formulations intended for application to turf. Poly(oxyethylene) (5) sorbitan monooleate ...... Surfactants, related adjuvants of surfactants Polysorbate 60, conforming to 21 CFR 172.836 ...... Surfactant Potassium dihydrogen phosphate ...... Buffering agent 2-Propanamine, compound with a-phosphono-w- Not more than 15% in the Surfactant butoxypoly (oxy-1,2-ethanediyl) (2:1) (CAS formulated product. Reg. No. 431040–31–2). 2-Propanamine, compounds with polyethylene Not more than 15% in the Surfactant glycol dihydrogen phosphate C8– 10- alkyl formulated product. ether (2:1) (CAS Reg. No. 431062–72–5). Propylene glycol monomethyl ether ...... Solvent Pyridoxine (CAS Reg. No. 65–23–6) ...... Maximum of 0.5% of formu- Synergist lation. Rosin, dark wood (as defined in 21 CFR ...... Surfactants, related adjuvants of surfactants 178.3870(a)(1)(v)). Rosin, gum ...... Do. Rosin, tall oil ...... Do. Scandium chloride ...... 10 ppm in formulation ...... Tagging agent Sodium bisulfate (CAS Reg. No. 7681–38–1) ...... Acidifying/buffering agent Sodium 1,4-dicyclohexyl sulfosuccinate ...... Surfactants, related adjuvants of surfactants Sodium 1,4-dihexyl sulfosuccinate (CAS Reg...... Surfactants, related adjuvants of surfactants No. 3006–15–3). Sodium dihydrogen phosphate (CAS Reg. No...... Buffering agent 7558–80–7) conforming to 21 CFR 182.6778. Sodium 1,4-diisobutyl sulfosuccinate (CAS Reg...... Surfactants, related adjuvants of surfactants No. 127–39–9). Sodium 1,4-dipentyl sulfosuccinate (CAS Reg...... Surfactants, related adjuvants of surfactants No. 922–80–5). Sodium metaborate ...... Sequestrant Sodium molybdate ...... Plant nutrient Sodium nitrate ...... Solid diluent Sodium nitrite ...... Not more than 3% of pes- Stabilizer, inhibitor. ticide formulation. Sodium o-phenylphenate ...... Not more than 0.1% of pes- Preservative for formulation ticide formulation. Sodium salt of the insoluble fraction of rosin ...... Surfactants, related adjuvants of surfactants Sodium salts of N-alkyl (C8-C18)-beta- Concentration in formulated Surfactants, related adjuvants of surfactants iminodipropionic acid where the C8-C18 is lin- end-use products not to ear and may be saturated and/or unsaturated exceed 30% by weight in (CAS Reg. Nos. 3655-00-3, 61791-56-8, pesticide formulations. 14960-06-6, 26256-79-1, 90170-43-7, 91696- 17-2, 97862-48-1). Sodium tetraborate ...... Not more than 2% of pes- Buffering agent; corrosion inhibitor ticide formulation. Tallowamine, ethoxylated, mixture of dihydrogen Not to exceed 20% of pes- Surfactants, related adjuvants of surfactants phosphate and monohydrogen phosphate ticide formulation. esters and the corresponding ammonium, calcium, potassium, and sodium salts of the phosphate esters, where the poly(oxyethylene) content averages 2–20 moles (CAS Reg. No. 68308–48–5). Tannin ...... Dispersing agent Tertiary butylhydroquinone ...... Antioxidant 1-Tetradecanamine, N,N-dimethyl-, N-oxide ...... Component in water-soluble film (CAS Reg. No. 3332–27–2). N,N,N′,N″-Tetrakis-(2-hydroxypropyl) ethylene- Concentration in formulated Stabilizer for formulations diamine (CAS Reg. No. 102–60–3). end-use products not to exceed 20% by weight in pesticide formulations. 2,4,7,9-Tetramethyl-5-decyne 4,7-diol ...... In pesticide formulations, Surfactants, related adjuvants of surfactants for application to soil prior to planting or to plants before edible parts form. Tetrapotassium pyrophosphate (CAS Reg. No. Not to exceed 10% of for- Sequestrant, anticaking agent, conditioning 7320–345). mulation. agent Titanium dioxide (CAS Reg. No. 13463–67–7) ...... Pigment/coloring agent in plastic bags used to wrap growing banana (preharvest), colorant on seeds for planting

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Inert ingredients Limits Uses

Toluenesulfonic acid and its ammonium, cal- ...... Solvent, cosolvent cium, magnesium, potassium, sodium, and zinc salts. Triethanolamine ...... Stabilizer, inhibitor for formulations used before crop emerges from soil Triethanolamine (CAS Reg. No. 102–71–6) ...... Stabilizer, inhibitor Triethylene glycol ...... Deactivator Triethyl phosphate ...... Stabilizer for formulations used before crop emerges from soil Trimethylolpropane (CAS Reg. No. 77–99–6) .... Not to exceed 15% by Component in water-soluble film weight of the film. a-[2,4,6-Tris[1-(phenyl)ethyl]phenyl]-w-hydroxy Not more than 15% of the Surfactant. poly(oxyethylene), the poly(oxyethylene) con- formulation. tent averages 4-150 moles). a-[2,4,6-Tris[1-(phenyl)ethyl]phenyl]-w-hydroxy Not more than 15% of the Do. poly(oxyethylene); mixture of monohydrogen formulation. and dihydrogen phosphate esters and the corresponding ammonium, calcium, magnesium, potassium, sodium, and zinc salts, the poly(oxyethylene) content averages 4-150 moles). a-[2,4,6-Tris[1-(phenyl)ethyl]phenyl]-w-hydroxy Not more than 15% of the Do. poly(oxyethylene) sulfate, and the cor- pesticide formulation. responding ammonium, calcium, magnesium, potassium, sodium, and zinc salts, the poly(oxyethylene) content averages 4-150 moles. Tryptophan (CAS Reg. No. 73–22–3) ...... Maximum of 0.5% of formu- Synergist lation. Valeric acid, normal ...... Not more than 2% in pes- Stenching agent or odorant ticide formulations. Xylene ...... Solvent, cosolvent Xylenesulfonic acid its ammonium calcium, mag- ...... Surfactants, related adjuvants of surfactants nesium, potassium, sodium, and zinc salts. Yucca extract from Yucca schidigera ...... Wetting agent Ytterbium chloride ...... 10 ppm in formulation ...... Tagging agent Yttrium chloride ...... 10 ppm in formulation ...... Tagging agent Zinc orthophosphate ...... Plant nutrient and safener Zinc stearate, conforming to 21 CFR 182.5994 ...... Flow control agent and 582.5994.

[69 FR 23124, Apr. 28, 2004]

EDITORIAL NOTE: For FEDERAL REGISTER citations affecting § 180.920, see the List of CFR Sections Affected, which appears in the Finding Aids section of the printed volume and at www.fdsys.gov.

§ 180.930 Inert ingredients applied to when used in accordance with good ag- animals; exemptions from the re- ricultural practice as inert (or occa- quirement of a tolerance. sionally active) ingredients in pesticide The following materials are exempt- formulations applied to animals: ed from the requirement of a tolerance

Inert ingredients Limits Uses

Acetic acid (CAS Reg. No. 64–19–7) ...... Not more than 0.5% of pes- Catalyst ticide formulation. Acetic anhydride ...... Solvent, cosolvent, stabilizer Acetone (Cas Reg. No. 67–64–1) ...... Solvent or cosolvent Alkanoic and alkenoic acids, mono- and ...... Emulsifiers diesters of a-hydro-w- hydroxypoly(oxyethylene) with molecular weight (in amu) range of 200 to 6,000.

Alkyl (C8-C24) benzenesulfonic acid and its am- ...... Surfactants, emulsifier, related adjuvants of monium, calcium, magnesium, potassium, so- surfactants dium, and zinc salts.

Alkyl (C12-C16) dimethyl ammonio acetate (CAS 20% by weight in pesticide Surfactant Reg. Nos. 683–10–3, 2601–33–4 and 693– formulation. 33–4.

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Inert ingredients Limits Uses

a-alkyl (C12-C15)-w-hydroxypoly Not to exceed 20% of pes- Surfactant (oxypropylene)poly (oxyethylene)copolymers ticide formulations. (where the poly(oxypropylene) content is 3-60 moles and the poly(oxyethylene) content is 5- 80 moles), the resulting ethoxylated propoxylated (C12-C15) alcohols having a minimum molecular weight (in amu) of 1,500, CAS Reg. No. 68551–13–3.

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Inert ingredients Limits Uses

a-alkyl-w-hydroxypoly (oxypropylene) and/or ...... Surfactants, related adjuvants of surfactants. poly (oxyethylene) polymers where the alkyl chain contains a minimum of six carbons (CAS Reg. No.: 9002–92–0; 9004–95–9; 9004–98–2; 9005–00–9; 9035–85–2; 9038– 29–3; 9038–43–1; 9040–05–5; 9043–30–5; 9087–53–0; 25190–05–0; 24938–91–8; 25231–21–4; 26183–52–8; 26468–86–0; 26636–39–5; 27252–75–1; 27306–79–2; 31726–34–8; 34398–01–1; 34398–05–5; 37251–67–5; 37311–00–5; 37311–01–6; 37311–02–7; 37311–04–9; 39587–22–9; 50861–66–0; 52232–09–4; 52292–17–8; 52609–19–5; 57679–21–7; 59112–62–8; 60828–78–6; 61702–78–1; 61725–89–1; 61791–13–7; 61791–20–6; 61791–28–4; 61804–34–0; 61827–42–7; 61827–84–7; 62648–50–4; 63303–01–5; 63658–45–7; 63793–60–2; 64366–70–7; 64415–24–3; 64415–25–4; 64425–86–1; 65104–72–5; 65150–81–4; 66455–14–9: 66455–15–0; 67254–71–1; 67763–08–0; 68002–96–0; 68002–97–1; 68131–39–5; 68131–40–8; 68154–96–1; 68154–97–2; 68154–98–3; 68155–01–1; 68213–23–0; 68213–24–1; 68238–81–3; 68238–82–4; 68409–58–5; 68409–59–6; 68439–30–5; 68439–45–2; 68439–46–3; 68439–48–5; 68439–49–6; 68439–50–9; 68439–51–0; 68439–53–2; 68439–54–3; 68458–88–8; 68526–94–3; 68526–95–4; 68551–12–2; 68551–13–3; 68551–14–4; 68603–20–3; 68603–25–8; 68920–66–1; 68920–69–4; 68937–66–6; 68951–67–7; 68954–94–9; 68987–81–5; 68991–48–0; 69011–36–5; 69013–18–9; 69013–19–0; 69227–20–9; 69227–21–0; 69227–22–1; 69364–63–2; 70750–27–5; 70879–83–3; 70955–07–6; 71011–10–4; 71060–57–6; 71243–46–4; 72066–65–0; 72108–90–8; 72484–69–6; 72854–13–8; 72905–87–4; 73018–31–2; 73049–34–0; 74432–13–6; 74499–34–6; 78330–19–5; 78330–20–8; 78330–21–9; 78330–23–1; 79771–03–2; 84133–50–6; 85422–93–1; 97043–91–9; 97953–22–5; 102782–43–4; 103331–86–8; 103657–84–7; 103657–85–8; 103818–93–5; 103819–03–0; 106232–83–1; 111905–54–5; 116810–31–2; 116810–32–3; 116810–33–4; 120313–48–6; 120944–68–5; 121617–09–2; 126646–02–4; 126950–62–7; 127036–24–2; 139626–71–4; 152231–44–2; 154518–36–2; 157627–86–6; 157627–88–8; 157707–41–0; 157707–43–2; 159653–49–3; 160875–66–1; 160901–20–2; 160901–09–7; 160901–19–9; 161025–21–4; 161025–22–5; 166736–08–9; 169107–21–5; 172588–43–1; 176022–76–7; 196823–11–7; 287935–46–0; 288260–45–7; 303176–75–2; 954108–36–2).

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Inert ingredients Limits Uses

a-alkyl (minimum C6 linear, branched, saturated Not to exceed 30% of pes- Surfactants, related adjuvants of surfactants and/or unsaturated)-w- ticide formulation. hydroxypolyoxyethylene polymer with or without polyoxypropylene, mixture of di- and monohydrogen phosphate esters and the corresponding ammonium, calcium, magnesium, monoethanolamine, potassium, sodium and zinc salts of the phosphate esters; minimum oxyethylene content averages 2 moles; minimum oxypropylene content is 0 moles (CAS Reg. Nos. 9004–80–2, 9046–01–9, 26982– 05–8, 31800–89–2, 37280–82–3, 39464–66– 9, 39341–09–8, 39341–65–6, 39464–69–2, 42612–52–2, 50643–20–4, 50668–50–3, 51884–64–1, 52019–36–0, 57486–09–6, 58318–92–6, 59112–71–9, 60267–55–2, 61837–79–4, 62362–49–6, 63747–86–4, 63887–55–8, 66272–25–1, 67711–84–6, 67786–06–5, 67989–06–4, 68070–99–5, 68071–17–0, 68071–35–2, 68071–37–4, 68130–44–9, 68130–45–0, 68130–46–1, 68130–47–2, 68186–29–8, 68186–36–7, 68186–34–5, 68186–37–8, 68238–84–6, 68311–02–4, 68311–04–6, 68389–72–0, 68413–78–5, 68425–73–0, 68425–75–2, 68439–39–4, 68458–48–0, 68511–15–9, 68511–36–4, 68511–37–5, 68551–05–3, 68585–15–9, 68585–16–0, 68585–17–1, 68585–36–4, 68585–39–7, 68603–24–7, 68607–14–7, 68610–64–0, 68610–65–1, 68649–29–6, 68649–30–9, 68650–84–0, 68815–11–2, 68855–46–9, 68856–03–1, 68890–90–4, 68890–91–5, 68891–12–3, 68891–13–4, 68891–26–9, 68908–64–5, 68909–65–9, 68909–67–1, 68909–69–3, 68921–24–4, 68921–60–8, 68954–87–0, 68954–88–1, 68954–92–7, 68987–35–9, 69029–43–2, 69980–69–4, 70247–99–3, 70248–14–5, 70903–63–8, 71965–23–6, 71965–24–7, 72480–27–4, 72623–67–7, 72623–68–8, 72828–56–9, 72828–57–0, 73018–34–5, 73038–25–2, 73050–08–5, 73050–09–6, 73361–29–2, 73378–71–9, 73378–72–0, 73559–42–9, 73559–43–0, 73559–44–1, 73559–45–2, 74499–76–6, 76930–25–1, 78330–22–0, 78330–24–2, 91254–26–1, 93925–54–3, 96416–89–6, 103170–31–6, 103170–32–7, 106233–09–4, 106233–10–7, 108818–88–8, 110392–49–9, 111798–26–6, 111905–50–1, 116671–23–9, 117584–36–8, 119415–05–3, 121158–61–0, 121158–63–2, 125139–13–1, 125301–86–2, 125301–87–3, 126646–03–5, 129870–77–5, 129870–80–0, 130354–37–9, 136504–88–6, 143372–50–3, 143372–51–4, 154518–39–5, 154518–40–8, 155240–11–2, 160498–49–7, 160611–24–5, 171543–66–1, 210493–60–0, 246159–55–7, 251298–11–0, 261627–68–3, 317833–96–8, 422563–19–7, 873662–29–4, 936100–29–7, 936100–30–0, 1072943–56–6, 1187742–89–7, 1187743–35–6). N-alkyl (C8-C18) primary amines and their ace- Concentration in formulated Surfactants, related adjuvants of surfactants tate salts where the alkyl group is linear and end-use products not to ex- may be saturated and/or unsaturated (CAS ceed 10% by weight in her- Reg. Nos. 61790–57–6, 61790–58–7, 61790– bicide products, 4% by 59–8, 61790–60–1, 61788–46–3, 61790–33– weight in insecticide prod- 8, 68155–38–4). ucts, and 4% by weight in fungicide products.

Alkyl (C8-C18) sulfate and its ammonium, cal- ...... Surfactant cium, magnesium, potassium, sodium, and zinc salts.

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Inert ingredients Limits Uses

N,N-Bis-a-ethyl-w-hydroxypoly(oxy-1,2- Not to exceed 25% in herbi- Surfactants, related adjuvants of surfactants ethanediyl) C8–C18 saturated and unsatu- cide formulations and 10% rated alkylamines; the poly(oxy-1,2- in insecticide and fungicide ethanediyl) content is 2–60 moles (CAS Reg. formulations. Nos. 10213–78–2, 25307–17–9, 26635–92–7, 26635–93–8, 288259–52–9, 58253–49–9, 61790–82–7, 61791–14–8, 61791–24–0, 61791–26–2, 61791–31–9, 61791–44–4, 68155–33–9, 68155–39–5, 68155–40– 8,70955–14–5, 73246–96–5, 1266162–49–5). N,N-Bis-a-ethyl-w-hydroxypoly(oxy-1,2- Not to exceed 25% in herbi- Surfactants, related adjuvants of surfactants ethanediyl/oxy(methyl-1,2-ethanediyl) C8-C18 cide formulations and 10% saturated and unsaturated alkylamines; the in insecticide and fungicide poly(oxy-1,2-ethanediyl/oxy(methyl-1,2- formulations. ethanediyl) content is 2–60 moles (CAS Reg. Nos. 68213–26–3, 68153–97–9, 75601–76– 2). Ascorbyl palmitate ...... Preservative Attapulgite-type clay ...... Solid diluent, carrier Barium sulfate (CAS Reg. No. 7727–43–7) ...... Carrier, density control agent Benzoic acid ...... Preservative for formulations 2-Bromo-2-nitro-1,3-propanediol (CAS Reg. No. 0.04% or less by weight of In-can preservative 52–51–7). the total pesticide formulation. Butane ...... Propellant n-Butanol (CAS Reg. No. 71–36–3) ...... Solvent for blended emulsifiers Butylated hydroxyanisole ...... Antioxidant Butylated hydroxytoluene ...... Do. Calcium carbonate ...... Solid diluent, carrier Calcium chloride ...... Stabilizer Calcium silicate, hydrated calcium silicate ...... Anticaking agent, solid diluent, carrier Calcium stearate (CAS Reg. No. 1592–23–0) ...... Stabilizer, component of plastic animal tag Calcium sulfate ...... Solid diluent, carrier Carbon black (CAS Reg. No. 1333–86–4) ...... Colorant/pigment in animal tag Carbon Dioxide (CAS Reg. No. 124–38–9) ...... None ...... Propellant Carrageenan, conforming to 21 CFR 172.620 ... Minimum molecular weight (in Thickener amu): 100,000. Cyclohexanone ...... Solvent, cosolvent D&C Green No. 6 ...... Dye, coloring agent D&C Red No. 17 ...... Do. D&C Violet No. 2 ...... Do. Dialkyl (C8-C18) dimethylammonium chloride ..... Not more than 0.2% in silica Flocculating agent in the manufacture of silica hydrated silica. hydrated silica for use as a solid diluent, carrier Diatomite (diatomaceous earth) ...... Solid diluent, carrier Diethanolamine salts of alkyl (C8-C24) Not to exceed 7% of pesticide Surfactants, related adjuvants of surfactants. benzenesulfonic acid (CAS Reg. Nos. formulation. 26545–53–9, 67815–95–6, 67889–94–5, 67889–95–6, 68259–34–7, 68478–47–7, 68567–68–0, 68815–34–9, 68815–37–2, 68891–02–1, 68953–97–9, 84989–15–1, 85338–09–6, 90194–39–1, 90194–40–4, 90218–08–9). Diethylaminoethanol, ethoxylated, propoxylated, ...... Surfactant reaction products with fatty acid dimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173188–75–4). Diethylaminoethanol, ethoxylated, propoxylated, ...... Surfactant reaction products with fatty acid trimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173188–83–4). Diethylaminoethanol, ethoxylated, reaction ...... Surfactant products with acid trimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173188–81–2). Diethylaminoethanol, ethoxylated, reaction ...... Surfactant product with fatty acid dimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173188–72–1). Diethylphthalate ...... Solvent, cosolvent 1,1-Difluoroethane (CAS Reg. No. 75–37–6) ..... For aerosol pesticide formula- Aerosol propellant tions used for insect control in food- and feed-handling establishments and animals.

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Inert ingredients Limits Uses

Dimethyl ether (CAS Reg. No. 115–10–6) ...... Propellant Dimethylaminoethanol, ethoxylated, ...... Surfactant propoxylated, reaction products with fatty acid dimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173188–42–5). Dimethylaminoethanol, ethoxylated, ...... Surfactant propoxylated reaction products with fatty acid trimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173188–67–4). Dimethylaminoethanol, ethoxylated, reaction ...... Surfactant products with fatty acid trimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173188–38–9). Dimethylaminoethanol, ethoxylated, reaction ...... Surfactant products with fatty acid trimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173188–49–2). Dimethylaminopropylamine, isopropylamine, ...... Surfactants, related adjuvants of surfactants. ethanolamine, and triethanolamine salts of alkyl (C8-C24) benzenesulfonic acid (CAS Reg. Nos. 3088–30–0, 12068–12–1, 26264– 05–1, 26836–07–7, 27323–41–7, 55470–69– 4, 58089–99–9, 61886–59–7, 61931–76–8, 67924–05–4, 68110–32–7, 68259–35–8, 68411–31–4, 68442–72–8, 68567–69–1, 68584–24–7, 68584–25–8, 68648–81–7, 68648–96–4, 68649–00–3, 68815–30–5, 68815–35–0, 68910–32–7 68953–93–5, 68953–98–0, 70528–84–6, 72391–21–0, 84961–74–0, 85480–55–3, 85480–56–4, 85995–82–0, 90194–42–6, 90194–53–9, 90194–54–0, 90194–55–1, 90218–09–0, 90218–11–4, 90218–35–2, 96687–54–6, 99924–49–9, 121617–08–1, 157966–96–6, 193562–36–6, 319926–68–6, 877677–48–0, 1093628–27–3).. 3,6-Dimethyl-4-octyne-3,6-diol ...... Not more than 2.5% of pes- Surfactants, related adjuvants of surfactants ticide formulation. Dimethylpolysiloxane (CAS Reg. No. 9016–00– ...... Defoaming agent 6). Dipropylene glycol monomethyl ether ...... Surfactants, related adjuvants of surfactants Epoxidized soybean oil (CAS Reg. No. 8013– ...... Stabilizer, plasticizer, component animal tag 07–8). Ethyl alcohol ...... Solvent, cosolvent Ethyl maltol (CAS Reg. No.4940–11–8) ...... Not more than 0.2 % of the Odor masking agent pesticide formulation. Ethylene oxide adducts of 2,4,7,9-tetramethyl-5- ...... Surfactants, related adjuvants of surfactants decynediol, the ethylene oxide content averages 3.5, 10 or 30 moles (CAS Reg. No. 9014–85–1). 2-Ethyl-1-hexanol (CAS Reg. No. 104–76–7) .... Not more than 10% of pes- Solvent, adjuvant of surfactants ticide. FD&C Blue No. 1 ...... Dye, coloring agent FD&C Yellow No. 6 Aluminum Lake (CAS Reg. Not more than 2% by weight Pigment in animal tag and similar slow-re- No. 15790–07–5). of pesticide formulation. lease devices D-glucopyranose, oligomeric, C10–16-alkyl ...... Surfactant glycosides (CAS Reg. No. 110615–47–9). Glycerol monooleate ...... Surfactants, related adjuvants of surfactants Glyceryl monostearate ...... Emulsifier Glyceryl tris-12-hydroxystearate ...... Flow control agent Graphite ...... Solid diluent, carrier n-Hexyl alcohol (CAS Reg. No. 111–27–3) ...... Solvent, cosolvent Hydroxyethylmorpholine, ethoxylated, ...... Surfactant propoxylated, reaction products with fatty acid dimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173189–06–4). Hydroxyethylmorpholine, ethoxylated, ...... Surfactant propoxylated, reaction products with fatty acid trimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173188–67–4).

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Inert ingredients Limits Uses

Hydroxyethylmorpholine, ethoxylated, reaction ...... Surfactant products with fatty acid dimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173189–00–8). Hydroxyethylmorpholine, ethoxylated, reaction ...... Surfactant products with fatty acid trimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173189–09–7). Hydroxyethylpiperidine, ethoxylated, ...... Surfactant propoxylated, reaction products with fatty acid dimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173189–22–4). Hydroxyethylpiperidine, ethoxylated, ...... Surfactant propoxylated, reaction products with fatty acid trimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173189–28–0). Hydroxyethylpiperidine, ethoxylated, reaction ...... Surfactant products with fatty acid dimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173189–20–2). Hydroxyethylpiperidine, ethoxylated, reaction ...... Surfactant products with fatty acid trimers, minimum number average molecular weight (in amu), 1,200 (CAS Reg. No. 1173189–25–7). 2-(2′-Hydroxy-5′-methylphenyl)benzotriazole Not more than 0.5% by Ultraviolet light absorber/stabilizer in animal (CAS Reg. No. 2440–22–4). weight of pesticide formula- tag and similar slow-release devices tion. Iron oxide (CAS Reg. No. 1309–37–1) ...... Colorant in pesticide formulations for animal tags Isobutane (CAS Reg. No. 75–28–5) ...... None ...... Propellant Isopropyl myristate, CAS Reg. No. 110–27–0 ...... Solvent Kaolinite-type clay ...... Solid diluent, carrier Kerosene, U.S.P. reagent ...... Solvent, cosolvent Lactic acid ...... Solvent Lactic acid, 2-ethylhexyl ester (CAS Reg. No...... Solvent 6283–86–9). Lactic acid, 2-ethylhexyl ester, (2S)- (CAS Reg...... Solvent No. 186817–80–1). Lactic acid, n-propyl ester, (S); (CAS Reg. No...... Solvent 53651–69–7). Lignin (CAS Reg. No. 9005–53–2) ...... Surfactant, related adjuvants of surfactants Lignin, alkali (CAS Reg. No. 8068–05–1) ...... Do. Lignin, alkali, oxidized, sodium salt (CAS Reg...... Do. No. 68201–23–0). Lignin alkali reaction products with disodium ...... Do. sulfite and formaldehyde (CAS Reg. No. 105859–97–0). Lignin alkali reaction products with formalde- ...... Do. hyde and sodium bisulfite (CAS Reg. No. 68512–35–6). Lignosulfonic acid (CAS Reg. No. 8062–15–5) ...... Do. Lignosulfonic acid, ammonium calcium salt ...... Do. (CAS Reg. No. 12710–04–2). Lignosulfonic acid, ammonium magnesium salt ...... Do. (CAS Reg. No. 123175–37–1). Lignosulfonic acid, ammonium salt (CAS Reg...... Do. No. 8061–53–8). Lignosulfonic acid, ammonium sodium salt ...... Do. (CAS Reg. No. 166798–73–8). Lignosulfonic acid, calcium magnesium salt ...... Do. (CAS Reg. No. 55598–86–2). Lignosulfonic acid, calcium salt (CAS Reg. No...... Do. 8061–52–7). Lignosulfonic acid, calcium sodium salt (CAS ...... Do. Reg. No. 37325–33–0). Lignosulfonic acid, ethoxylated, sodium salt ...... Do. (CAS Reg. No. 68611–14–3). Lignosulfonic acid, magnesium salt (CAS Reg...... Do. No. 8061–54–9). Lignosulfonic acid, potassium salt (CAS Reg...... Do. No. 37314–65–1).

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Inert ingredients Limits Uses

Lignosulfonic acid, sodium salt (CAS Reg. No...... Do. 8061–51–6). Lignosulfonic acid, sodium salt, oxidized (CAS ...... Do. Reg. No. 68855–41–4). Lignosulfonic acid, sodium salt, polymer with ...... Do. formaldehyde and phenol (CAS Reg. No. 37207–89–9). Lignosulfonic acid, sodium salt, sulfomethylated ...... Do. (CAS Reg. No. 68512–34–5). Lignosulfonic acid, zinc salt (CAS Reg. No...... Do. 57866–49–6). d-Limonene (CAS Reg. No. 5989–27–5) ...... Solvent, fragrance Magnesium carbonate ...... Solid diluent, carrier Magnesium silicate, hydrated magnesium sili- ...... Do. cate. Methyl alcohol ...... Solvent, cosolvent Methyl n-amyl ketone (CAS Reg. No. 110–43– ...... Solvent, cosolvent 0). Methyl esters of higher fatty acids conforming ...... Antidusting agent to 21 CFR 573.640. Methyl-p-hydroxybenzoate (Methyl paraben) ..... Meets specifications of Food Preservative Chemicals Codex; not to exceed 0.1% in formulations. Methyl isobutyl ketone ...... Solvent, cosolvent 2-methyl-2,4-pentanediol (CAS Reg. No.–107– Without limitation ...... Growing crops and food animals 41–5). 2-methyl-1,3-propanediol (CAS Reg. No. 2163– ...... Solvent, surfactant 42–0). Mineral oil, U.S.P., or conforming to 21 CFR ...... Solvent, diluent 172.878 or 178.3620(a), (b). Montmorillonite-type clay ...... Solid diluent, carrier Nonyl, decyl, and undecyl glycoside mixture ...... Surfactant with a mixture of nonyl, decyl, and undecyl oligosaccharides and related reaction products (primarily decanol and undecanol) produced as an aqueous-based liquid (50 to 65% solids) from the reaction of primary alcohols (containing 15 to 20% secondary alcohol isomers) in a ratio of 20% C9, 40% C10, and 40% C11 with carbohydrates (average glucose to alkyl chain ratio 1.3 to 1.8). a-(p-Nonylphenol)-w-hydroxypoly(oxyethylene) Not to exceed 7% of pesticide Surfactants, related adjuvants of surfactants mixture of dihydrogen phosphate and formulation. monohydrogen phosphate esters and the corresponding ammonium, calcium, magnesium, potassium, sodium, and zinc salts of the phosphate esters; the nonyl group is a propylene trimer isomer and the poly(oxyethylene) content averages 4–14 or 30 moles (CAS Reg. Nos. 51811–79–1, 59139–23–0, 67922–57–0, 68412–53–3, 68553–97–9, 68954–84–7, 99821–14–4, 152143–22–1, 51609–41–7, 37340–60–6, 106151–63–7, 68584–47–4, 52503–15–8, 68458–49–1). a-(p-Nonylphenol)-w-hydroxypoly(oxyethylene) Not to exceed 7% of pesticide Surfactants, related adjuvants of surfactants sulfate, ammonium, calcium, magnesium, po- formulation. tassium, sodium, and zinc salts the nonyl group is propylene trimer isomer and the poly(oxyethylene) content averages 4 moles (CAS Reg. Nos. 9014–90–8, 9051–57–4, 9081–17–8, 68649–55–8, 68891–33–8. a-(p-Nonylphenyl)-w-hydroxypoly(oxyethylene) ...... Surfactants, emulsifier, related adjuvants of produced by the condensation of 1 mole of surfactants. nonylphenol (nonyl group is a propylene trimer isomer) with an average of 4-15 or 30- 90 moles of ethylene oxide; if a blend of products is used, the average number of moles of ethylene oxide reacted to produce any product that is a component of the blend shall be in the range of 4-15 or 30-90 moles.

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Inert ingredients Limits Uses

Octadecyl 3,5-di-tert-butyl-4-hydroxyhydro Not more than 0.5% by Thermal stabilizer/antioxidant in animal tag cinnamate (CAS Reg. No. 2082–79–3). weight of pesticide formula- and similar slow-release devices tion. 1-Octanal (CAS Reg. No. 124–13–0) ...... Not more than 0.2% of the Odor masking agent pesticide formulation. Octyl and decyl glucosides mixture with a mix- ...... Thermal stabilizer/antioxidant in animal tag ture of octyl and decyl oligosaccharides and and similar slow-release devices related reaction products (primarily n- decanol) produced as an aqueous-based liquid (68-72% solids) from the reaction of straight chain alcohols (C8(45%), C10) with anhydrous glucose. Octyl epoxytallate (CAS Reg. No. 61788–72–5) ...... Plasticizer, component animal tag Oleic acid, conforming to 21 CFR 172.862 ...... Defoaming agent (CAS Reg. No. 112–80–1). a-Oleoyl-w-hydroxypoly(oxyethylene), average ...... Emulsifier molecular weight (in amu) of 600. a-Oleoyl-w-(oleyloxy)poly(oxyethylene) derived ...... Emulsifier, defoaming agent from a-hydro-w-hydroxypoly(oxyethylene), molecular weight (in amu) 600. Petroleum hydrocarbons, light, odorless, con- ...... Solvent, diluent forming to 21 CFR 172.884 or 178.3650. Petroleum hydrocarbons, synthetic isoparaffinic, ...... Do. conforming to 21 CFR 172.882 or 178.3530. Phenol ...... Solvent, cosolvent a-Pinene ...... Not more than 2% of formula- Stabilizer tion by weight. Polyethylene (CAS Reg. No. 9002–88–4) con- ...... Component of plastic slow release tag forming to 21 CFR 172.615. Polyethylene glycol [a-hydro-w- ...... Surfactants, related adjuvants of surfactants hydroxypoly(oxyethylene)]; mean molecular weight (in amu) 194 to 9,500 conforms to 21 CFR 178.3750. Potassium benzoate (Cas No. 582–25–2) ...... None ...... Preservative Potassium hydroxide ...... Meeting Food Chemicals, Neutralizer Codex specifications. Propane ...... Propellant 1,2,3-Propanetriol, homopolymer ...... Emulsifier diisooctadecanoate (CAS Reg. No. 63705– 03–3). n-Propanol ...... Solvent, for blended emulsifiers 2-Propenoic acid, 2-methyl-, polymer with ethyl ...... Encapsulating agent,dispensers, resins, fibers 2-propenoate and methyl 2-methyl-2- and beads propenoate, ammonium salt (CAS Registra- tion No. 55989–05–4), minimum number average molecular weight (in amu), 18,900.. Propylene glycol ...... Solvent, cosolvent Propylene glycol monomethyl ether ...... Deactivator, emmolient Propyl gallate ...... Antioxidant Propyl p-hydroxybenzoate (Propyl paraben) ...... Meets specifications of Food Preservative Chemicals Codex; not to exceed 0.1% in formulations. Pyrophylite ...... Solid diluent, carrier Silica, hydrated silica ...... Anticaking agent, solid diluent, carrier Silica aerogel (finely powdered microcellular sili- ...... Component of antifoaming agent ca foam having a minimum silica content of 89.5%). Soapstone ...... Solid diluent Sodium alkyl naphthalenesulfonates (CAS Reg. Limited to no more than 30% Surfactants, related adjuvants of surfactants Nos. 68909–83–1, 68909–84–2, 68909–82–0, by weight in pesticide end- 27213–90–7, 26264–58–4, 27178–87–6, use products. 111163–74–7, 908356–16–1, 25417–20–3, 25638–17–9, 145578–88–7, 1322–93–6, 1323–19–9, 7403–47–6, 68442–09–1, 127646–44–0, 908356–18–3). Sodium 1,4-dihexyl sulfosuccinate (CAS Reg...... Surfactants, related adjuvants of surfactants No. 3006–15–3). Sodium 1,4-diisobutyl sulfosuccinate (CAS Reg...... Surfactants, related adjuvants of surfactants No. 127–39–9). Sodium dioctylsulfosuccinate ...... Surfactants, related adjuvants of surfactants Sodium 1,4-dipentyl sulfosuccinate (CAS Reg...... Surfactants, related adjuvants of surfactants No. 922–80–5). Sodium hydroxide ...... Neutralizer

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Inert ingredients Limits Uses

Sodium monoalkyl and dialkyl (C6-C16) Not to exceed 20% in pes- Surfactants, related adjuvants of surfactants phenoxy benzenedisulfonates and related ticide formulations. acids (CAS Reg. Nos. 147732–59–0, 147732–60–3, 169662–22–0, 70191–75–2, 36445–71–3, 39354–74–0, 70146–13–3, 119345–03–8, 149119–20–0, 149119–19–7, 119345–04–9, 28519–02–0, 25167–32–2, 30260–73–2, 65143–89–7, 70191–76–3). Sodium N-oleoyl-N-methyl taurine (CAS Reg...... Surfactants, related adjuvants of surfactants No. 137–20–2).

Sodium and potassium salts of N-alkyl (C8– Concentration in formulated Surfactants, related adjuvants of surfactants C18)-beta-iminodipropionic acid where the end-use products not to ex- C8–C18 is linear and may be saturated and/or ceed 30% by weight in pes- unsaturated (CAS Reg. Nos. 110676–19–2, ticide formulations. 3655–00–3, 61791–56–8, 14960–06–6, 26256–79–1, 90170–43–7, 91696–17–2, 97862–48–1). Sodium starch glycolate (CAS Reg. No. 9063– Granular and tableted prod- Disintegrant 38–1). ucts only; not to exceed 8% of the formulated product. Sodium sulfate ...... Solid diluent, carrier Sorbitan fatty acid esters (fatty acids limited to ...... Buffering agent; corrosion inhibition C12, C14, C16, and C18 containing minor amounts of associated fatty acids) and poly(oxyethylene) derivatives of sorbitan fatty acid esters; the poly(oxyethylene) content averages 16-20 moles. Sorbitol ...... Antidusting agent. Stearic acid (CAS Reg. No. 57–11–4) ...... Lubricant, component animal tag a-Stearoyl-w-hydroxypoly(oxyethylene), average ...... Emulsifier molecular weight (in amu) of 600. a-Stearoyl-w-hydroxypoly(oxyethylene); the ...... Surfactants; related adjuvants of surfactants poly(oxyethylene) content averages 8, 9, or 40 moles; if a blend of products is used, the average number of moles of ethylene oxide reacted to produce any product that is a component of the blend shall be 8, 9, or 40. Sulfite liquors and cooking liquors, spent, ...... Surfactant, related adjuvants of surfactants oxidized (CAS Reg. No. 68514–09–0). Sulfur (CAS Reg. No. 7704–34–9) ...... Stabilizer Talc ...... Do. Tall oil; fatty acids not less than 58%, rosin ...... Surfactants, related adjuvants of surfactants acids not more than 44%, unsaponifiables not more than 8%. Tartrazine ...... Dye, coloring agent N,N,N′,N″,-tetrakis-(2-hydroxypropyl) ethylene- Concentration in formulated Stabilizer for formulation. diamine (CAS Reg. No. 102–60–3). end-use products not to exceed 20% by weight in pesticide formulations. 2,4,7,9-Tetramethyl-5-decyne-4.7-diol ...... Not more than 2.5% of pes- Surfactants, related adjuvants of surfactants ticide formulation. Titanium dioxide (CAS Reg. No. 13463–67–7) ...... Pigment/colorant in pesticide formulations for animal tag Toluenesulfonic acid and its ammonium, cal- ...... Do. cium, magnesium, potassium, sodium, and zinc salts. Triacetin (glyceryl triacetate) ...... Solvent, cosolvent Trisodium phosphate ...... Precipitant, buffer, filler Xylene ...... Solvent, cosolvent Xylenesulfonic acid and its ammonium, calcium, ...... Surfactants, related adjuvants of surfactants magnesium, potassium, sodium, and zinc salts. Zinc oxide ...... Solid diluent, carrier Zinc stearate, conforming to 21 CFR 182.5994 ...... Water repellant, dessicant, and coating agent. and 582.5994. Zinc stearate (CAS Reg. No. 557–05–1) ...... Water repellant, desiccant, and coating agent; stabilizer, component of plastic animal tag Zinc sulfate (basic and monohydrate) ...... Water repellant, dessicant, and coating agent

[69 FR 23130, Apr. 28, 2004]

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EDITORIAL NOTE: For FEDERAL REGISTER citations affecting § 180.930, see the List of CFR Sections Affected, which appears in the Finding Aids section of the printed volume and at www.fdsys.gov.

§ 180.940 Tolerance exemptions for ac- semi-permanent or permanent food- tive and inert ingredients for use in contact surface (other than being ap- antimicrobial formulations (Food- plied on food packaging) with adequate contact surface sanitizing solu- draining before contact with food. tions). (a) The following chemical sub- Residues of the following chemical stances when used as ingredients in an substances are exempted from the re- antimicrobial pesticide formulation quirement of a tolerance when used in may be applied to: Food-contact sur- accordance with good manufacturing faces in public eating places, dairy- practice as ingredients in an anti- processing equipment, and food-proc- microbial pesticide formulation, provided that the substance is applied on a essing equipment and utensils.

Pesticide Chemical CAS Reg. No. Limits

Acetic acid 64–19–7 When ready for use, the end-use concentration is not to exceed 290 ppm a-alkyl-w-hydroxypoly (oxypropylene) and/or 9002–92–0; 9004–95–9; poly (oxyethylene) polymers where the alkyl 9004–98–2; 9005–00–9; chain contains a minimum of six carbons. 9035–85–2; 9038–29–3; 9038–43–1; 9040–05–5; 9043–30–5; 9087–53–0; 25190–05–0; 24938–91–8; 25231–21–4; 26183–52–8; 26468–86–0; 26636–39–5; 27252–75–1; 27306–79–2; 31726–34–8; 34398–01–1; 34398–05–5; 37251–67–5; 37311–00–5; 37311–01–6; 37311–02–7; 37311–04–9; 39587–22–9; 50861–66–0; 52232–09–4; 52292–17–8; 52609–19–5; 57679–21–7; 59112–62–8; 60828–78– 6; 61702–78–1; 61725– 89–1;.

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Pesticide Chemical CAS Reg. No. Limits

...... 61791–13–7; 61791–20–6; 61791–28–4; 61804–34–0; 61827–42–7; 61827–84–7; 62648–50–4; 63303–01–5; 63658–45–7; 63793–60–2; 64366–70–7; 64415–24–3; 64415–25–4; 64425– 86–1; 65104–72–5; 65150–81–4; 66455–14–9: 66455–15–0; 67254–71–1; 67763–08–0; 68002–96–0; 68002–97–1; 68131–39–5; 68131–40–8; 68154–96–1; 68154–97–2; 68154–98–3; 68155–01–1; 68213–23–0; 68213–24–1; 68238–81–3; 68238–82–4; 68409–58–5; 68409–59–6; 68439–30–5; 68439–45–2; 68439–46–3; 68439–48–5; 68439–49–6; 68439–50–9; 68439–51–0; 68439–53–2; 68439–54–3; 68458–88–8; 68526–94–3; 68526–95– 4; 68551–12–2; 68551– 13–3; 68551–14–4; 68603– 20–3; 68603–25–8; 68920– 66–1; 68920–69–4; 68937– 66–6; 68951–67–7; 68954– 94–9; 68987–81–5; 68991– 48–0; 69011–36–5; 69013– 18–9; 69013–19–0; 69227– 20–9; 69227–21–0; 69227– 22–1; 69364–63–2; 70750– 27–5; 70879–83–3; 70955–07–6; 71011–10–4; 71060–57–6; 71243–46–4; 72066–65–0; 72108–90–8; 72484–69–6; 72854–13–8; 72905–87–4; 73018–31–2; 73049–34–0; 74432–13–6; 74499–34–6; 78330–19–5; 78330–20–8; 78330–21–9; 78330–23–1; 79771–03–2; 84133–50–6; 85422–93–1; 97043–91–9; 97953–22–5; 102782–43–4; 103331–86– 8; 103657–84–7; 103657– 85–8; 103818–93–5; 103819–03–0; 106232–83– 1; 111905–54–5; 116810– 31–2; 116810–32–3; 116810–33–4; 120313–48– 6; 120944–68–5; 121617– 09–2; 126646–02–4; 126950–62–7; 127036–24– 2; 139626–71–4; 152231– 44–2; 154518–36–2; 157627–86–6; 157627–88– 8; 157707–41–0; 157707– 43–2; 159653–49–3; 160875–66–1; 160901–20– 2; 160901–09–7; 160901– 19–9; 161025–21–4; 161025–22–5; 166736–08– 9; 169107–21–5; 172588– 43–1; 176022–76–7; 196823–11–7; 287935–46– 0; 288260–45–7; 303176– 75–2; 954108–36–2. Ammonium chloride 12125–02–9 When ready for use, the end-use concentration is not to exceed 48 ppm Amylopectin, acid-hydrolyzed, 1- 113894–85–2 None oxtenylbutanedioate

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Pesticide Chemical CAS Reg. No. Limits

Amylopectin, hydrogen 1- 125109–81–1 None octadecenylbutanedioate Copper sulfate pentahydrate 7758–99–8 When ready for use, the end-use concentration is not to exceed 80 ppm D-Glucopyranose, oligomeric, decyl octyl 68515–73–1 None glycosides Ethanol 64–17–5 None Ethylenediamine- tetraacetic acid (EDTA), 64–02–8 None tetrasodium salt FD&C Green No. 3 CAS Reg. No. 2353–45–9 None FD&C Yellow No. 5 1934–21–0 When ready for use, the end-use concentration is not to exceed 1000 ppm Hydrogen peroxide 7722–84–1 When ready for use, the end-use concentration is not to exceed 91 ppm Hypochlorous acid, sodium salt 7681–52–9 When ready for use, the end-use concentration of all hypochlorous acid chemicals in the solution is not to exceed 200 ppm determined as total available chlorine Iodine 7553–56–2 When ready for use, the total end-use concentration of all iodide-producing chemicals in the solution is not to exceed 25 ppm of titratable iodine Lipase, triacylglycerol 9001–62–1 When ready for use, the end-use concentration is not to exceed 500 ppm Magnesium oxide 1309–48–4 None Methylene blue 61–73–4 When ready for use, the end-use concentration is not to exceed 0.4 ppm 2-Methyl-1,3-propanediol 2163–42–0 None Nitric acid 7697–37–2 When ready for use, the end-use concentration is not to exceed 1,000 ppm a-(p-Nonylphenyl)-w-hydroxypoly (oxyethylene) None None average poly(oxyethylene) content 11 moles) Octadecanoic acid, calcium salt 1592–23–0 None 1-Octanesulfonic acid, sodium salt 5324–84–5 When ready for use, the end-use concentration is not to exceed 46 ppm Octanoic acid 124–07–2 When ready for use, the end-use concentration is not to exceed 52 ppm Oxirane, methyl-, polymer with oxirane, min- 9003–11–6 None imum molecular weight (in amu), 1900 Peroxyacetic acid 79–21–0 When ready for use, the end-use concentration is not to exceed 58 ppm Peroxyoctanoic acid 33734–57–5 When ready for use, the end-use concentration is not to exceed 52 ppm Phosphonic acid, (1-hydroxyethylidene)bis- 2809–21–4 When ready for use, the end-use concentration is not to exceed 14 ppm Phosphoric acid, trisodium salt 7601–54–9 When ready for use, the end-use concentration is not to exceed 5916 ppm Potassium bromide 7758–02–3 When ready for use, the end-use concentration is not to exceed 46 ppm total available halogen Potassium iodide 7681–11–0 When ready for use, the total end-use concentration of all iodide-producing chemicals in the solution is not to exceed 25 ppm of titratable iodine 1,3-Propanediol 504–63–2 None Propylene glycol 57–55–6 None Quaternary ammonium compounds, alkyl (C12- 8001–54–5 When ready for use, the end-use concentra- C18) benzyldimethyl, chlorides tion of all quaternary chemicals in the solution is not to exceed 200 ppm of active quaternary compound Quaternary ammonium compounds: n-alkyl 68424–85–1 When ready for use, the end-use concentra- (C12-18) dimethyl benzyl ammonium chloride tion of all quaternary chemicals in solution is not to exceed 400 ppm of active quaternary compound Quaternary Ammonium Compounds: n-alkyl (C 85409–23–0 When ready for use, the end-use concentra- 12-14) dimethyl ethylbenzyl ammonium chlo- tion of all quaternary chemicals in solution ride, average molecular weight (in amu), 377 is not to exceed 400 ppm of active quater- to 384 nary compound. Quaternary ammonium compounds n-alkyl (C12- None When ready for use, the end-use concentra- C18) dimethyl ethylbenzyl ammonium chloride tion of all quaternary chemicals in the solu- average molecular weight (in amu) 384 tion is not to exceed 200 ppm of active quaternary compound

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Pesticide Chemical CAS Reg. No. Limits

Quaternary ammonium compounds, Di-n-Alkyl None When ready for use, the end-use concentra- (C8-10) dimethyl ammonium chloride, average tion of these specific in quaternary ammo- molecular weight (in amu) 332 to 361 nium compounds is not to exceed 240 ppm of active quaternary ammonium compound; the end-use concentration of all quaternary chemicals in the solution is not to exceed 400 ppm of active quaternary compound Quaternary ammonium compounds, didecyl di- 148788–55–0/148812–654–1 When ready for use, the end-use concentra- methyl ammonium carbonate/didecyl dimethyl tion of these specific ammonium com- ammonium bicarbonate pounds is not to exceed 400 ppm of active quaternary ammonium compound Silver ions resulting from the use of electro- 14701–21–4 When ready for use, the end-use concentra- lytically-generated silver ions stabilized in cit- tion of silver ions is not to exceed 50 ppm ric acid as silver dihydrogen citrate (does not of active silver include metallic silver) Sodium bisulfate 7681–38–1 When ready for use, the end-use concentration is not to exceed 2,000 ppm. Sorbitan, mono-9-octadecenoate, poly(oxy-1,2- 9005–65–6 None ethanediyl) derivs., (Z)- Sulfuric acid monododecyl ester, sodium salt 151–21–3 When ready for use, the end-use concentra- (sodium lauryl sulfate) tion is not to exceed 350 ppm 1,3,5-Triazine-2,4,6(1H,3H,5H)-trione, 1,3- 2893–78–9 When ready for use, the end-use concentra- dichloro-, sodium salt tion of all di- or trichloroisocyanuric acid chemicals in the solution is not to exceed 100 ppm determined as total available chlorine Xylenesulfonic acid, sodium salt 1300–72–7 When ready for use, the end-use concentration is not to exceed 500 ppm

(b) The following chemical sub- may be applied to: Dairy processing stances when used as ingredients in an equipment, and food-processing equip- antimicrobial pesticide formulation ment and utensils.

Pesticide Chemical CAS Reg. No. Limits

Acetic acid 64–19–7 When ready for use, the end-use concentration is not to exceed 686 ppm Acetic acid, chloro-, sodium salt, reaction prod- 68608–66–2 When ready for use, the end-use concentra- ucts with 4,5-dihydro-2-undecyl-1H-imidazole- tion is not to exceed 42 ppm chloroacetic 1-ethanol and sodium hydroxide acid Benzenesulfonic acid, dodecyl- 27176–87–0 When ready for use, the end-use concentration is not to exceed 5.5 ppm Butanedioic acid, octenyl- 28805–58–5 When ready for use, the end-use concentration is not to exceed 156 ppm Butoxy monoether of mixed (ethylene-pro- None None pylene) polyalkylene glycol, minimum average molecular weight (in amu), 2400 Calcium chloride 10043–52–4 When ready for use, the end-use concentration is not to exceed 17 ppm n-Carboxylic acids (C6-C12), consisting of a mix- None When ready for use, the end-use concentra- ture of not less than 56% octanoic acid and tion is not to exceed 39 ppm not less than 40% decanoic acid Decanoic acid 334–48–5 When ready for use, the end-use concentration is not to exceed 90 ppm Ethanesulfonic acid, 2-[cyclohexyl (1- 132–43–4 When ready for use, the end-use concentra- oxohexadecyl) amino]-, sodium salt tion is not to exceed 237 ppm Ethylenediaminetetraacetic acid (EDTA), diso- 139–33–3 When ready for use, the end-use concentra- dium salt tion is not to exceed 1400 ppm FD&C Yellow No. 5 (Tartrazine) (conforming to 1934–21–0 None 21 CFR 74.705) D-Gluconic acid, monosodium salt 527–07–1 When ready for use, the end-use concentration is not to exceed 760 ppm Hydriodic acid 10034–85–2 When ready for use, the total end-use concentration of all iodide-producing chemicals is not to exceed 25 ppm of titratable iodine Hydrogen peroxide 7722–84–1 When ready for use, the end-use concentration is not to exceed 465 ppm Hypochlorous acid 7790–92–3 When ready for use, the end-use concentration of all hypochlorous acid chemicals in the solution is not to exceed 200 ppm determined as total available chlorine

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Pesticide Chemical CAS Reg. No. Limits

Iodine 7553–56–2 When ready for use, the total end-use concentration of all iodide-producing chemicals in the solution is not to exceed 25 ppm of titratable iodine Lactic acid 50–21–5 When ready for use, the end-use concentration is not to exceed 138 ppm Nonanoic acid 112–05–0 When ready for use, the end-use concentration is not to exceed 90 ppm 1-Octanamine, N,N-dimethyl- 7378–99–6 When ready for use, the end-use concentration is not to exceed 113 ppm 1,2-Octanedisulfonic acid 113669–58–2 When ready for use, the end-use concentration is not to exceed 102 ppm 1-Octanesulfonic acid 3944–72–7 When ready for use, the end-use concentration is not to exceed 172 ppm 1-Octanesulfonic acid, sodium salt 5324–84–5 When ready for use, the end-use concentration is not to exceed 297 ppm 1-Octanesulfonic acid, 2-sulfino- 113652–56–5 When ready for use, the end-use concentration is not to exceed 102 ppm Octanoic acid 124–07–2 When ready for use, the end-use concentration is not to exceed 176 ppm Oxychloro species (including chlorine dioxide) None When ready for use, the end-use concentra- generated by acidification of an aqueous so- tion is not to exceed 200 ppm of chlorine lution of sodium chlorite dioxide as determined by the method titled, Iodometric Method for the Determination of Available Chlorine Dioxide (50-250 ppm available chlorine dioxide) Peroxyacetic acid 79–21–0 When ready for use, the end-use concentration is not to exceed 315 ppm Peroxyoctanoic acid 33734–57–5 When ready for use, the end-use concentration is not to exceed 122 ppm Phosphonic acid, (1-hydroxyethylidene)bis- 2809–21–4 When ready for use, the end-use concentration is not to exceed 34 ppm Phosphoric acid 7664–38–2 None Phosphoric acid, monosodium salt 7558–80–7 When ready for use, the end-use concentration is not to exceed 350 ppm Potassium iodide 7681–11–0 When ready for use, the total end-use concentration of all iodide-producing chemicals in the solution is not to exceed 25 ppm of titratable iodine Propanoic acid 79–09–4 When ready for use, the end-use concentration is not to exceed 297 ppm 2,6-Pyridinedicarboxylic acid 499–83–2 When ready for use, the end-use concentration is not to exceed 1.2 ppm Sulfuric acid 7664–93–9 When ready for use, the end-use concentration is not to exceed 288 ppm Sulfuric acid monododecyl ester, sodium salt 151–21–3 When ready for use, the end-use concentra- (sodium lauryl sulfate) tion is not to exceed 350 ppm

(c) The following chemical sub- may be applied to: Food-processing stances when used as ingredients in an equipment and utensils. antimicrobial pesticide formulation

Pesticide Chemical CAS Reg. No. Limits

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Pesticide Chemical CAS Reg. No. Limits

Butanedioic acid, sulfo-, 1,4-dioctyl ester, so- 1639–66–3 None dium salt Butoxy monoether of mixed (ethylene-pro- None None pylene) polyalkylene glycol, cloudpoint of 90 - 100oC in 0.5 aqueous solution, average molecular weight (in amu), 3300 Butoxy monoether of mixed (ethylene-pro- None None pylene) polyalkylene glycol, minimum average molecular weight (in amu), 2400 Calcium chloride 10043–52–4 When ready for use, the end-use concentration is not to exceed 17 ppm n-Carboxylic acids (C6-C12), consisting of a mix- None When ready for use, the end-use concentra- ture of not less than 56% octanoic acid and tion is not to exceed 39 ppm not less than 40% decanoic acid 3-Cyclohexene-1-methanol,a,a,4-trimethyl- 98–55–5 None 1-Decanaminium, N-decyl-N, N-dimethyl-, chlo- 7173–51–5 When ready for use, the end-use concentra- ride tion is not to exceed 200 ppm of active quaternary compound Decanoic acid 3347–48–5 When ready for use, the end-use concentration is not to exceed 234 ppm Ethanesulfonic acid, 2-[cyclohexyl (1- 132–43–4 When ready for use, the end-use concentra- oxohexadecyl) amino]-, sodium salt tion is not to exceed 237 ppm Ethanol 64–17–5 None Ethanol, 2 butoxy- 111–76–2 None Ethanol, 2-(2-ethoxyethoxy)- 111–90–0 None Ethylenediaminetetraacetic acid (EDTA), diso- 139–33–3 When ready for use, the end-use concentra- dium salt tion is not to exceed 1400 ppm Ethylenediaminetetraacetic acid (EDTA), 64–02–8 None tetrasodium salt Fatty acids, coco, potassium salts 61789–30–8 None Fatty acids, tall-oil, sulfonated, sodium salts 68309–27–3 When ready for use, the end-use concentration is not to exceed 66 ppm FD&C Yellow No. 5 (Tartrazine) (conforming to 1934–21–0 None 21 CFR 74.705) D-Gluconic acid, monosodium salt 527–07–1 When ready for use, the end-use concentration is not to exceed 760 ppm Hydriodic acid 10034–85–2 When ready for use, the total end-use concentration of all iodide-producing chemicals in the solution is not to exceed 25 ppm of titratable iodine Hydrogen peroxide 7722–84–1 When ready for use, the end-use concentration is not to exceed 1100 ppm Hypochlorous acid 7790–92–3 When ready for use, the end-use concentration of all hypochlorous acid chemicals in the solution is not to exceed 200 ppm determined as total available chlorine Hypochlorous acid, calcium salt 7778–54–3 When ready for use, the end-use concentration of all hypochlorous acid chemicals in the solution is not to exceed 200 ppm determined as total available chlorine Hypochlorous acid, lithium salt 13840–33–0 When ready for use, the end-use concentration of all hypochlorous acid chemicals in the solution is not to exceed 200 ppm determined as total available chlorine and 30 ppm lithium Hypochlorous acid, potassium salt 7778–66–7 When ready for use, the end-use concentration of all hypochlorous acid chemicals in the solution is not to exceed 200 ppm determined as total available chlorine Hypochlorous acid, sodium salt 7681–52–9 When ready for use, the end-use concentration of all hypochlorous acid chemicals in the solution is not to exceed 200 ppm determined as total available chlorine Iodine 7553–56–2 When ready for use, the total end-use concentration of all iodide-producing chemicals in the solution is not to exceed 25 ppm of titratable iodine Lactic acid 50–21–5 None Magnesium oxide 1309–48–4 None Methylene blue 61–73–4 When ready for use, the end-use concentration is not to exceed 0.4 ppm Neodecanoic acid 26896–20–8 When ready for use, the end-use concentration is not to exceed 174 ppm

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Pesticide Chemical CAS Reg. No. Limits

Nonanoic acid 112–05–0 When ready for use, the end-use concentration is not to exceed 90 ppm a-(p-Nonylphenyl)-w-hydroxypoly (oxyethylene) None None maximum average molecular weight (in amu), 748 a-(p-Nonylphenol)-w-hydroxypoly (oxyethylene) None None average poly(oxyethylene) content 11 moles a-(p-Nonylphenyl)-w-hydroxypoly (oxyethylene) None None produced by the condensation of 1 mole p- nonylphenol with 9 to 12 moles ethylene oxide a-(p-Nonylphenyl)-w-hydroxypoly (oxyethylene), None None 9 to 13 moles ethylene oxide Octadecanoic acid, calcium salt 1592–23–0 None 9-Octadecenoic acid (9Z)-, sulfonated 68988–76–1 When ready for use, the end-use concentration is not to exceed 312 ppm 9-Octadecenoic acid (9Z)-sulfonated, sodium 68443–05–0 When ready for use, the end-use concentra- salts tion is not to exceed 200 ppm 1-Octanamine, N,N-dimethyl- 7378–99–6 When ready for use, the end-use concentration is not to exceed 113 ppm 1,2-Octanedisulfonic acid 113669–58–2 When ready for use, the end-use concentration is not to exceed 102 ppm 1-Octanesulfonic acid 3944–72–7 When ready for use, the end-use concentration is not to exceed 172 ppm 1-Octanesulfonic acid, sodium salt 5324–84–5 When ready for use, the end-use concentration is not to exceed 312 ppm 1-Octanesulfonic acid, 2-sulfino- 113652–56–5 When ready for use, the end-use concentration is not to exceed 102 ppm Octanoic acid 124–07–2 When ready for use, the end-use concentration is not to exceed 234 ppm Oxirane, methyl-, polymer with oxirane, min- 9003–11–6 None imum molecular weight (in amu), 1900 Oxirane, methyl-, polymer with oxirane, block, 106392–12–5 None average molecular weight (in amu), 1900 Oxirane, methyl-, polymer with oxirane, block, None None minimum average molecular weight (in amu), 2000 Oxirane, methyl-, polymer with oxirane, block, None None 27 to 31 moles of polyoxypropylene, average molecular weight (in amu) 2000 Oxychloro species (predominantly chlorite, chlo- None When ready for use, the end-use concentra- rate and chlorine dioxide in an equilibrium tion is not to exceed 200 ppm of chlorine mixture) generated either (i) by directly me- dioxide as determined by the method titled, tering a concentrated chlorine dioxide solu- ‘‘Iodometric Method for the Determination of tion prepared just prior to use, into potable Available Chlorine Dioxide (50-250 ppm water, or (ii) by acidification of an aqueous al- available chlorine dioxide)’’ kaline solution of oxychloro species (predomi- nately chlorite and chlorate) followed by dilu- tion with potable water Oxychloro species (including chlorine dioxide) None When ready for use, the end-use concentra- generated by acidification of an aqueous so- tion is not to exceed 200 ppm of chlorine lution of sodium chlorite dioxide as determined by the method titled, ‘‘Iodometric Method for the Determination of Available Chlorine Dioxide (50-250 ppm available chlorine dioxide)’’ 2,4-Pentanediol, 2-methyl- 107–41–5 None Peroxyacetic acid 79–21–0 When ready for use, the end-use concentration is not to exceed 315 ppm Peroxyoctanoic acid 33734–57–5 When ready for use, the end-use concentration is not to exceed 122 ppm Phenol, 4-chloro-2-(phenylmethyl)- 120–32–1 When ready for use, the end-use concentration is not to exceed 320 ppm Phenol, 4-(1,1-dimethylpropyl)- 80–46–6 When ready for use, the end-use concentration is not to exceed 80 ppm Phosphonic acid, (1-hydroxyethylidene)bis- 2809–21–4 When ready for use, the end-use concentration is not to exceed 34 ppm Phosphoric acid 7664–38–2 None Phosphoric acid, monosodium salt 7558–80–7 When ready for use, the end-use concentration is not to exceed 350 ppm Phosphoric acid, trisodium salt 7601–54–9 When ready for use, the end-use concentration is not to exceed 5916 ppm

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Pesticide Chemical CAS Reg. No. Limits

Poly(oxy-1,2-ethanediyl), a-[(1,1,3,3- None None tetramethylbutyl) phenyl]-w-hydroxy-, produced with one mole of the phenol and 4 to 14 moles ethylene oxide Potassium bromide 7758–02–3 When ready for use, the end-use concentration of all bromide-producing chemicals in the solution is not to exceed 200 ppm total available halogen Potassium iodide 7681–11–0 When ready for use, the total end-use concentration of all iodide-producing chemicals in the solution is not to exceed 25 ppm of titratable iodine Propanoic acid 79–09–4 When ready for use, the end-use concentration is not to exceed 297 ppm 2,6-Pyridinedicarboxylic acid 499–83–2 When ready for use, the end-use concentration is not to exceed 1.2 ppm

Quaternary ammonium compounds, alkyl (C12- 8001–54–5 When ready for use, the end-use concentra- C18) benzyldimethyl, chlorides tion of this specific quaternary compound is not to exceed 200 ppm within the end-use total concentration that is not to exceed 400 ppm active quaternary compound Quaternary ammonium compounds, n-alkyl None When ready for use, the end-use concentra- (C12-C14) dimethyl ethylbenzyl ammonium tion of this specific quaternary compound is chloride, average molecular weight (in amu), not to exceed 200 ppm within the end-use 377 to 384 total concentration that is not to exceed 400 ppm active quaternary compound Quaternary ammonium compounds, n-alkyl None When ready for use, the end-use concentra- (C12-C18) dimethyl ethylbenzyl ammonium tion of this specific quaternary compound is chloride average molecular weight (in amu) not to exceed 200 ppm within the end-use 384 total concentration that is not to exceed 400 ppm active quaternary compound Quaternary ammonium compounds, di-n-Alkyl None When ready for use, the end-use concentra- (C8-C10) dimethyl ammonium chloride, aver- tion of this specific quaternary compound is age molecular weight (in amu), 332 to 361 not to exceed 240 ppm within the end-use total concentration that is not to exceed 400 ppm active quaternary compound

Sodium-a-alkyl(C12-C15)-w-hydroxypoly (oxy- None None ethylene) sulfate with the poly(oxyethylene) content averaging one mole Sodium bromide 7647–15–6 When ready for use, the end-use concentration of all bromide-producing chemicals in the solution is not to exceed 200 ppm total available halogen Sodium iodide 7681–82–5 When ready for use, the total end-use concentration of all iodide-producing chemicals in the solution is not to exceed 25 ppm of titratable iodine Sulfuric acid 7664–93–9 When ready for use, the end-use concentration is not to exceed 228 ppm Sulfuric acid monododecyl ester, sodium salt 151–21–3 None (sodium lauryl sulfate) 1,3,5-Triazine-2,4,6(1H,3H,5H)-trione, 1,3- 2782–57–2 When ready for use, the end-use concentra- dichloro- tion of all di- or trichloroisocyanuric acid chemicals in the solution is not to exceed 100 ppm determined as total available chlorine 1,3,5-Triazine-2,4,6(1H,3H,5H)-trione, 1,3- 2244–21–5 When ready for use, the end-use concentra- dichloro-, potassium salt tion of all di- or trichloroisocyanuric acid chemicals in the solution is not to exceed 100 ppm determined as total available chlorine 1,3,5-Triazine-2,4,6(1H,3H,5H)-trione, 1,3- 2893–78–9 When ready for use, the end-use concentra- dichloro-, sodium salt tion of all di- or trichloroisocyanuric acid chemicals in the solution is not to exceed 100 ppm determined as total available chlorine 1,3,5-Triazine-2,4,6(1H,3H,5H)-trione, 1,3,5- 87–90–1 When ready for use, the end-use concentra- trichloro- tion of all di- or trichloroisocyanuric acid chemicals in the solution is not to exceed 100 ppm determined as total available chlorine

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Pesticide Chemical CAS Reg. No. Limits

1,3,5-Triazine, N,N′,N″-trichloro-2,4,6-triamino- 7673–09–8 When ready for use, the end-use concentration of all di- or trichloroisocyanuric acid chemicals in the solution is not to exceed 200 ppm determined as total available chlorine

[69 FR 23136, Apr. 28, 2004, as amended at 71 FR 30811, May 31, 2006; 71 FR 45423, Aug. 9, 2006; 71 FR 46125, Aug. 11, 2006; 72 FR 51186, Sept. 6, 2007; 73 FR 37858, July 2, 2008; 73 FR 49107, Aug. 20, 2008; 73 FR 53725, Sept. 17, 2008; 74 FR 27454, June 10, 2009; 74 FR 38944, Aug. 5, 2009; 74 FR 40509, Aug. 12, 2009; 75 FR 40735, July 14, 2010; 76 FR 55267, Sept. 7, 2011; 77 FR 45498, Aug. 1, 2012; 77 FR 50617, Aug. 22, 2012; 77 FR 53150, Aug. 31, 2012; 77 FR 68692, Nov. 16, 2012; 78 FR 35147, June 12, 2013; 78 FR 46264, July 31, 2013; 78 FR 48621, Aug. 9, 2013; 78 FR 59269, Sept. 26, 2013; 78 FR 65565, Nov. 1, 2013; 78 FR 67042, Nov. 8, 2013; 78 FR 78731, Dec. 27, 2013; 79 FR 6096, Feb. 3, 2014; 79 FR 26152, May 7, 2014; 79 FR 32666, June 6, 2014; 79 FR 33473, June 11, 2014]

§ 180.950 Tolerance exemptions for (b) Animal feed items. Animal feed minimal risk active and inert ingre- items means meat meal and all items dients. derived from field crops that are fed to Unless specifically excluded, residues livestock excluding both the raw and resulting from the use of the following processed forms of peanuts, tree nuts, substances as either an inert or an ac- milk, soybeans, eggs, fish, crustacea, tive ingredient in a pesticide chemical and wheat. Meat meal is an animal feed formulation, including antimicrobial composed of dried animal fat and pro- pesticide chemicals, are exempted from tein that has been sterilized. Other the requirement of a tolerance under than meat meal, the term animal feed FFDCA section 408, if such use is in ac- item does not extend to any item de- cordance with good agricultural or signed to be fed to animals that con- manufacturing practices. tains, to any extent, components of (a) Commonly consumed food commod- animals. Included within the term ani- ities. Commonly consumed food com- mal feed items are: modities means foods that are com- (1) The hulls and shells of the commonly consumed for their nutrient modities specified in paragraph properties. The term commonly con- (a)(2)(ii) of this section, and cocoa sumed food commodities shall only bean. apply to food commodities (whether a (2) Bird feed such as canary seed. raw agricultural commodity or a proc- (3) Any feed component of a medi- essed commodity) in the form the com- cated feed meeting the definition of an modity is sold or distributed to the animal feed item. public for consumption. (c) Edible fats and oils. Edible fats and oils means all edible (food or feed) fats (1) Included within the term com- and oils, derived from either plants or monly consumed food commodities are: animals, whether or not commonly (i) Sugars such as sucrose, lactose, consumed, including products derived dextrose and fructose, and invert sugar from hydrogenating (food or feed) oils, and syrup. or liquefying (food or feed) fats. (ii) Spices such as cinnamon, cloves, (1) Included within the term edible and red pepper. fats and oils are oils (such as soybean (iii) Herbs such as basil, anise, or oil) that are derived from the commod- fenugreek. ities specified in paragraph (a)(2)(ii) of (2) Excluded from the term com- this section when such oils are highly monly consumed food commodities are: refined via a solvent extraction proce- (i) Any food commodity that is adul- dure. terated under 21 U.S.C. 342. (2) Excluded from the term edible (ii) Both the raw and processed forms fats and oils are plant oils used in the of peanuts, tree nuts, milk, soybeans, pesticide chemical formulation specifi- eggs, fish, crustacea, and wheat. cally to impart their characteristic (iii) Alcoholic beverages. fragrance and/or flavoring. (iv) Dietary supplements. (d) [Reserved]

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(e) Specific chemical substances. Resi- microbial pesticide chemicals, are ex- dues resulting from the use of the fol- empted from the requirement of a tol- lowing substances as either an inert or erance under FFDCA section 408, if an active ingredient in a pesticide such use is in accordance with good ag- chemical formulation, including anti- ricultural or manufacturing practices.

Chemical CAS No.

Acetic acid, sodium salt ...... 127–09–3 Alpha-cyclodextrin ...... 10016–20–3 Amylopectin, acid-hydrolyzed, 1-octenylbutanedioate ...... 113894–85–2 Amylopectin, hydrogen 1-octadecenylbutanedioate ...... 125109–81–1 Animal glue ...... None Ascorbic acid (vitamin C) ...... 50–81–7 Beeswax ...... 8012–89–3 Benzoic acid, sodium salt ...... 532–32–1 Beta-cyclodextrin ...... 7585–39–9 Carbonic acid, monopotassium salt ...... 298–14–6 Carbonic acid, monosodium salt (sodium bicarbonate) ...... 144–55–8 Carnauba wax ...... 8015–86–9 Carob gum (locust bean gum) ...... 9000–40–2 Castor oil ...... 8001–79–4 Castor oil, hydrogenated ...... 8001–78–3 Cellulose ...... 9004–34–6 Cellulose acetate ...... 9004–35–7 Cellulose, carboxy methyl ether, sodium salt ...... 9004–32–4 Cellulose, 2-hydroxyethyl ether ...... 9004–62–0 Cellulose, 2-hydroxypropyl ether ...... 9004–64–2 Cellulose, 2-hydroxypropyl methyl ether ...... 9004–65–3 Cellulose, methyl ether ...... 9004–67–5 Cellulose, mixture with cellulose carboxymethyl ether, sodium salt ...... 51395–75–6 Cellulose, pulp ...... 65996–61–4 Cellulose, regenerated ...... 68442–85–3 Citric acid ...... 77–92–9 Citric acid, 2-(acetyloxy)-, tributyl ester ...... 77–90–7 Citric acid, calcium salt ...... 7693–13–2 Citric acid, calcium salt (2:3) ...... 813–94–5 Citric acid, dipotassium salt ...... 3609–96–9 Citric acid, disodium salt ...... 144–33–2 Citric acid, monohydrate ...... 5949–29–1 Citric acid, monopotassium salt ...... 866–83–1 Citric acid, monosodium salt ...... 18996–35–5 Citric acid, potassium salt ...... 7778–49–6 Citric acid, triethyl ester ...... 77–93–0 Citric acid, tripotassium salt ...... 866–84–2 Citric acid, tripotassium salt, monohydrate ...... 6100–05–6 Citric acid, sodium salt ...... 994–36–5 Citric acid, trisodium salt ...... 68–04–2 Citric acid, trisodium salt, dihydrate ...... 6132–04–3 Citric acid, trisodium salt, pentahydrate ...... 6858–44–2 Coffee grounds ...... 68916–18–7 Dextrins ...... 9004–53–9 1,3-Dioxolan-2-one, 4-methyl-(propylene carbonate) ...... 108–32–7 Fumaric acid ...... 110–17–8 Gamma-cyclodextrin ...... 17465–86–0 Gellan gum ...... 71010–52–1 D-Glucitol (sorbitol) ...... 50–70–4 Glycerol (glycerin) (1,2,3-propanetriol) ...... 56–81–5 Guar gum ...... 9000–30–0 Humic acid ...... 1413–93–6 Humic acid, potassium salt ...... 68514–28–3 Humic acid, sodium salt ...... 68131–04–4 Lactic acid, n-butyl ester ...... 138–22–7 Lactic acid, n-butyl ester, (S) ...... 34451–19–9 Lactic acid, ethyl ester ...... 97–64–3 Lactic acid, ethyl ester,(S) ...... 687–47–8 Lanolin ...... 8006–54–0 Lecithins ...... 8002–43–5 Lecithins, soya ...... 8030–76–0 Licorice Extract ...... 68916–91–6 Maltodextrin ...... 9050–36–6 Paper ...... None Potassium chloride ...... 7447–40–7 2-Propanol (isopropyl alcohol) ...... 67–63–0 Red cabbage color, expressed from edible red cabbage heads via a pressing process using only acidi- None fied water.

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Chemical CAS No.

Silica, amorphous, fumed (crystalline free) ...... 112945–52–5 Silica, amorphous, precipitated and gel ...... 7699–41–4 Silica gel ...... 63231–67–4 Silica gel, precipitated, crystalline-free ...... 112926–00–8 Silica, hydrate ...... 10279–57–9 Silica, vitreous ...... 60676–86–0 Soap (The water soluble sodium or potassium salts of fatty acids produced by either the saponification None of fats and oils, or the neutralization of fatty acid). Sorbic acid, potassium salt ...... 24634–61–5 Soapbark (Quillaja saponin) ...... 1393–03–9 Sodium alginate ...... 9005–38–3 Sodium chloride ...... 7647–14–5 Syrups, hydrolyzed starch, hydrogenated ...... 68425–17–2 Ultramarine blue (C.I. Pigment Blue 29) ...... 57455–37–5 Urea ...... 57–13–6 Vanillin ...... 121–33–5 Xanthan gum ...... 11138–66–2

[67 FR 36537, May 24, 2002] definition of a polymer and the criteria EDITORIAL NOTE: For FEDERAL REGISTER ci- specified for defining a low-risk poly- tations affecting § 180.950, see the List of CFR mer in 40 CFR 723.250, as an inert ingre- Sections Affected, which appears in the dient in a pesticide chemical formula- Finding Aids section of the printed volume tion, including antimicrobial pesticide and at www.fdsys.gov. chemical formulations, are exempted § 180.960 Polymers; exemptions from from the requirement of a tolerance the requirement of a tolerance. under FFDCA section 408, if such use is Residues resulting from the use of in accordance with good agricultural or the following substances, that meet the manufacturing practices.

Polymer CAS No.

Acetic acid ethenyl ester, polymer with ethenol and (a)-2-propenyl-(w)- 137091–12–4 hydroxypoly (oxy-1,2-ethanediyl) minimum number average molecular weight (in amu), 15,000

Acetic acid ethenyl ester, polymer with 1-ethenyl-2-pyrrolidinone 25086–89–9

Acetic acid ethenyl ester, polymer with oxirane, minimum number av- 25820–49–9 erage molecular weight (in amu), 17,000

Acetic acid ethenyl ester, polymer with sodium 2-methyl-2-[(1-oxo-2- 924892–37–5 propen-1-yl)amino]-1-propanesulfonate (1:1), hydrolyzed, minimum number average molecular weight (in amu), 61,000

Acrylic acid-benzyl methacrylate-1-propanesulfonic acid, 2-methyl-2- 1152297–42–1 [(1-oxo-2-propenyl)amino]-, monosodium salt, minimum number average molecular weight (in amu), 1500

Acrylic acid, polymerized, and its ethyl and methyl esters None

Acrylic acid-sodium acrylate-sodium-2-methylpropanesulfonate copoly- 97953–25–8 mer, minimum average molecular weight (in amu), 4,500

Acrylic acid-stearyl methacrylate copolymer, minimum number average 27756–15–6 molecular weight (in amu), 2,500

Acrylic acid, styrene, a-methyl styrene copolymer, ammonium salt, 89678–90–0 minimum number average molecular weight (in amu), 1,250

Acrylic acid terpolymer, partial sodium salt, minimum number average 151006–66–5 molecular weight (in amu), 2,400

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Polymer CAS No.

Acrylic polymers composed of one or more of the following monomers: None Acrylic acid, methyl acrylate, ethyl acrylate, butyl acrylate, hydroxyethyl acrylate, hydroxypropyl acrylate, hydroxybutyl acrylate, carboxyethyl acrylate, methacrylic acid, methyl methacrylate, ethyl methacrylate, butyl methacrylate, isobutyl methacrylate, hydroxyethyl methacrylate, hydroxypropyl methacrylate, hydroxybutyl methacrylate, lauryl methacrylate, and stearyl methacrylate; with none and/or one or more of the following monomers: Acrylamide, N-methyl acrylamide, N,N-dimethyl acrylamide, N-octylacrylamide, maleic anhydride, maleic acid, monoethyl maleate, diethyl maleate, monooctyl maleate, dioctyl maleate; and their corresponding sodium, potassium, ammonium, isopropylamine, triethylamine, monoethanolamine, and/or triethanolamine salts; the resulting polymer having a minimum number average molecular weight (in amu), 1,200

Acrylonitrile-butadiene copolymer conforming to 21 CFR 180.22, min- 9003–18–3 imum average molecular weight (in amu), 1,000

Acrylonitrile-styrene-hydroxypropyl methacrylate copolymer, minimum None number average molecular weight (in amu), 447,000

a-alkyl (C12–C15) - w- hydroxypoly(oxypropylene)poly(oxyethylene)co- 68551–13–3 polymers (where the poly(oxypropylene) content is 3–60 moles and the poly(oxyethylene) content is 5–80 moles), the resulting ethoxylated propoxylated (C12–C15) alcohols having a minimum molecular weight (in amu), 1,500

a-alkyl-w-hydroxypoly (oxypropylene) and/or poly (oxyethylene) poly- 9002–92–0; 9004–95–9; 9004–98–2; 9005–00–9; mers where the alkyl chain contains a minimum of six carbons and 9035–85–2; 9038–29–3; 9038–43–1; 9040–05–5; a minimum number average molecular weight (in amu) 1,100 9043–30–5; 9087–53–0; 25190–05–0; 24938–91–8; 25231–21–4; 26183–52–8; 26468–86–0; 26636–39– 5; 27252–75–1; 27306–79–2; 31726–34–8; 34398– 01–1; 34398–05–5; 37251–67–5; 37311–00–5; 37311–01–6; 37311–02–7; 37311–04–9; 39587–22– 9; 50861–66–0; 52232–09–4; 52292–17–8; 52609– 19–5; 57679–21–7; 59112–62–8; 60828–78–6; 61702–78–1; 61725–89–1; 61791–13–7; 61791–20– 6; 61791–28–4; 61804–34–0; 61827–42–7; 61827– 84–7; 62648–50–4; 63303–01–5; 63658–45–7; 63793–60–2; 64366–70–7; 64415–24–3; 64415–25– 4; 64425–86–1; 65104–72–5; 65150–81–4; 66455– 14–9: 66455–15–0; 67254–71–1; 67763–08– 0; 68002–96–0; 68002–97–1; 68131–39–5; 68131– 40–8; 68154–96–1; 68154–97–2; 68154–98–3; 68155–01–1; 68213–23–0; 68213–24–1; 68238–81– 3; 68238–82–4; 68409–58–5; 68409–59–6; 68439– 30–5; 68439–45–2; 68439–46–3; 68439–48–5; 68439–49–6; 68439–50–9; 68439–51–0; 68439–53– 2; 68439–54–3; 68458–88–8; 68526–94–3; 68526– 95–4; 68551–12–2; 68551–13–3; 68551–14–4; 68603–20–3; 68603–25–8; 68920–66–1; 68920–69– 4; 68937–66–6; 68951–67–7; 68954–94–9; 68987– 81–5; 68991–48–0; 69011–36–5; 69013–18–9; 69013–19–0; 69227–20–9; 69227–21–0; 69227–22– 1; 69364–63–2; 70750–27–5; 70879–83–3; 70955– 07–6; 71011–10–4; 71060–57–6; 71243–46–4; 72066–65–0; 72108–90–8; 72484–69–6; 72854–13– 8; 72905–87–4; 73018–31–2; 73049–34–0; 74432– 13–6; 74499–34–6; 78330–19–5; 78330–20–8; 78330–21–9; 78330–23–1; 79771–03–2; 84133–50– 6; 85422–93–1; 97043–91–9; 97953–22–5; 102782– 43–4; 103331–86–8; 103657–84–7; 103657–85–8; 103818–93–5; 103819–03–0; 106232–83– 1; 111905–54–5; 116810–31–2; 116810–32–3; 116810–33–4; 120313–48–6; 120944–68–5; 121617–09–2; 126646–02–4; 126950–62–7; 127036–24–2; 139626–71–4; 152231–44–2; 154518– 36–2; 157627–86–6; 157627–88–8; 157707–41–0; 157707–43–2; 159653–49–3; 160875–66–1; 160901– 20–2; 160901–09–7; 160901–19–9; 161025–21–4; 161025–22–5; 166736–08–9; 169107–21–5; 172588– 43–1; 176022–76–7; 196823–11–7; 287935–46–0; 288260–45–7; 303176–75–2; 954108–36–2

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Polymer CAS No.

Alkyl (C12–C20) methacrylate-methacrylic acid copolymer, minimum None molecular weight (in amu), 11,900

2H-Azepin-2-one, 1-ethenylhexahydro-, homopolymer 25189–83–7

1,3 Benzene dicarboxylic acid, 5-sulfo-, 1,3-dimethyl ester, sodium 212842–88–1 salt, polymer with 1,3-benzene dicarboxylic acid, 1,4-benzene dicarboxylic acid, dimethyl 1,4-benzene dicarboxylate and 1,2- ethanediol, minimum number average molecular weight (in amu), 2,580

3,5-Bis(6-isocyanatohexyl)-2H-1,3,5-oxadiazine-2,4,6-(3H,5H)-trione, 87823–33–4 polymer with diethylenetriamine, minimum number average molecular weight (in amu), 1,000,000

Polymer of one or more diglycidyl ethers of bisphenol A, resorcinol, None glycerol, cyclohexanedimethanol, neopentyl glycol, and polyethylene glycol with one or more of the following: Polyoxypropylene diamine, polyoxypropylene triamine, N-aminoethyl-piperazine, trimethyl-1,6- hexanediamine isophorone diamine, N,N-dimethyl-1,3- diaminopropane, nadic methyl anhydride, 1,2-cyclohexane- dicarboxylic anhydride and 1,2,3,6-tetrahydrophthalic anhydride, minimum number average molecular weight (in amu), 400,000

Butadiene-styrene copolymer None

1,4-Butanediol-methylenebis(4-phenylisocyanate)-poly(tetramethylene 9018– 04–6 glycol) copolymer, minimum molecular weight (in amu) 158,000

Butene, homopolymer 9003–29–6

2-butenedioic acid (2Z)-, monobutyl ester, polymer with 205193–99–3 methoxyethene, sodium salt, minimum number average molecular weight (in amu), 18,200

2-Butenedioic acid (Z)-, polymer with ethenol and ethenyl acetate, so- 139871–83–3 dium salt, minimum number average molecular weight (in amu), 75,000

Butyl acrylate-vinyl acetate-acrylic acid copolymer, minimum number 65405–40–5 average molecular weight (in amu), 18,000

Carbonic acid, diethyl ester, polymer with a-hydro-w- 1147260–65–8 hydroxypoly[oxy(methyl-1,2-ethanediyl)] ether with 2-ethyl-2- (hydroxymethyl)-1,3-propanediol (3:1), ester with a-[[[[5- (carboxyamino)-1,3,3-trimethylcyclohexyl]methyl]amino]carbonyl]-w- methoxypoly(oxy-1,2-ethanediyl), minimum number average molecular weight (in amu), 1,900

Castor oil, ethoxylated, dioleate, minimum number average molecular 110531–96–9 weight (in amu), 1260.

Castor oil, ethoxylated, oleate, minimum number average molecular 220037–02–5 weight (in amu), 1,600

Castor oil, polymer with adipic acid, linoleic acid, oleic acid and ricin- 1357486–09–9 oleic acid, minimum number average molecular weight (in amu), 3,500

Castor oil, polyoxyethylated; the poly(oxyethylene) content averages None 5–54 moles

Chlorinated polyethylene 64754–90–1

Cross-linked nylon-type polymer formed by the reaction of a mixture of None sebacoyl chloride and polymethylene polyphenylisocycanate with a mixture of ethylenediamine and diethylenetriamine

Cross-linked polyurea-type encapsulating polymer None

Dimethylpolysiloxane minimum number average molecular weight (in 63148–62–9 amu), 6,800

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Polymer CAS No.

Dimethyl silicone polymer with silica, minimum number average molec- 67762–90–7 ular weight (in amu), 1,100,000

a-(o,p-Dinonylphenyl)-w-hydroxypoly(oxyethylene) produced by con- 9014–93–1 densation of 1 mole of dinonylphenol (nonyl group is a propylene trimer isomer) with an average of 140-160 moles of ethylene oxide

Docosyl methacrylate-acrylic acid copolymer, or docosyl methacrylate- None octadecyl methacrylate-acrylic acid copolymer, minimum number average molecular weight (in amu), 3,000

1,12-Dodecanediol dimethacrylate polymer, minimum molecular weight None (in amu), 100,000

a-(p-Dodecylphenyl)-w-hydroxypoly(oxyethylene) produced by the con- 9014–92–0 densation of 1 mole of dodecylphenol (dodecyl group is a propylene 26401–47–8 tetramer isomer) with an average of 30-70 moles of ethylene oxide

1,2-Ethanediamine, N1-(2-aminoethyl)-, polymer with 2,4-diisocyanato- 35297–61–1 1-methylbenzene, minimum number average molecular weight (in amu), one million

1, 2-Ethanediamine, polymer with methyl oxirane and oxirane, min- 26316–40–5 imum number average molecular weight (in amu), 1,100

Ethylene glycol dimethyacrylate-lauryl methacrylate copolymer, min- None imum molecular weight (in amu), 100,000

Ethylene glycol dimethacrylate polymer, minimum molecular weight (in None amu), 100,000

Fatty acids, tall-oil, ethoxylated propoxylated, minimum number aver- 67784–86–5 age molecular weight (in amu), 2,009

Formaldehyde, polymer with a-[bis(1-phenylethyl)phenyl]-w- 157291–93–5 hydroxypoly(oxy-1,2-ethanediyl), number average molecular weight (in amu), 1,803

Formaldehyde, polymer with 2-methyloxirane and 4-nonylphenol, min- 37523–33–4 imum number average molecular weight (in amu), 4,000

Fumaric acid-isophthalic acid-styrene-ethylene/propylene glycol co- None polymer, minimum average molecular weight (in amu), 1×1018

2,5-Furandione, polymer with ethenylbenzene, hydrolyzed, 3- 1062609–13–5 (dimethylamino)propyl imide, imide with polyethylene-polypropylene glycol 2-aminopropyl me ether, 2,2′-(1,2-diazenediyl)bis[2- methylbutanenitrile]-initiated, minimum number average molecular weight (in amu), 5,816

2,5-Furandione, polymer with ethenylbenzene, reaction products with 162568–32–3 polyethylene-polypropylene glycol 2-aminopropyl Me ether; minimum number average molecular weight (in amu), 14,000

Hexadecyl acrylate-acrylic acid copolymer, hexadecyl acrylate-butyl None acrylate-acrylic acid copolymer, or hexadecyl acrylate-dodecyl acrylate-acrylic acid copolymer, minimum number average molecular weight (in amu), 3,000

Hexamethyl disilizane, reaction product with silica, minimum number 68909–20–6 average molecular weight (in amu), 645,000

1,6-Hexanediol dimethyacrylate polymer, minimum molecular weight None (in amu), 100,000

a-Hydro-w-hydroxy-poly(oxyethylene) C8 alkyl ether citrates, 330977–00–9 poly(oxyethylene) content is 4–12 moles, minimum number average molecular weight (in amu) 1,300

a-Hydro-w-hydroxy-poly(oxyethylene) C10–C16-alkyl ether citrates, 330985–58–5 poly(oxyethylene) content is 4–12 moles, minimum number average molecular weight (in amu) 1,100

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Polymer CAS No.

a-Hydro-w-hydroxy-poly(oxyethylene) C16–C18-alkyl ether citrates, 330985–61–0 poly(oxyethylene) content is 4–12 moles, minimum number average molecular weight (in amu) 1,300

a-Hydro-w-hydroxypoly(oxyethylene), minimum number average mo- 25322–68–3 lecular weight (in amu), 17,000

a-Hydro-w-hydroxypoly(oxyethylene)poly (oxypropylene) None poly(oxyethylene) block copolymer; the minimum poly(oxypropylene) content is 27 moles and the minimum molecular weight (in amu) is 1,900

a-Hydro-w-hydroxypoly(oxypropylene); minimum molecular weight (in None amu) 2,000

12-Hydroxystearic acid-polyethylene glycol copolymer, minimum num- 70142–34–6 ber average molecular weight (in amu), 3,690

Isodecyl alcohol ethoxylated (2–8 moles) polymer with chloromethyl None oxirane, minimum number average molecular weight (in amu) 2,500

Lauryl methacrylate-1,6-hexanediol dimethacrylate copolymer, min- None imum molecular weight (in amu), 100,000

Maleic acid-butadiene copolymer None

Maleic acid monobutyl ester-vinyl methyl ether copolymer, minimum 25119–68–0 average molecular weight (in amu), 52,000

Maleic acid monoethyl ester-vinyl methyl ether copolymer, minimum 25087–06–3 average molecular weight (in amu), 46,000

Maleic acid monoisopropyl ester-vinyl methyl ether copolymer, min- 31307–95–6 imum average molecular weight (in amu), 49,000

Maleic anhydride-diisobutylene copolymer, sodium salt, minimum num- 37199–81–8 ber average molecular weight (in amu) 5,0007–18,000

Maleic anhydride-methylstyrene copolymer sodium salt, minimum 60092–15–1 number average molecular weight (in amu), 15,000

Maleic anhydride-methyl vinyl ether, copolymer, average molecular None weight (in amu), 250,000

Methacrylic acid-methyl methacrylate-polyethylene glycol methyl ether 100934–04–1 methacrylate copolymer, minimum number averge molecular weight (in amu), 3,700

Methacrylic acid-methyl methacrylate-polyethylene glycol monomethyl 111740–36–4 ether methacrylate graft copolymer, minimum number average molecular weight (in amu), 1,800

Methacrylic copolymer, minimum number average molecular weight (in 63150–03–8 amu), 15,000

Methyl methacrylate-methacrylic acid-monomethoxypolyethylene glycol 119724–54–8 methacrylate copolymer,) minimum number average molecular weight (in amu), 2,730

Methyl methacrylate-2-sulfoethyl methacrylate- None dimethylaminoethylmethacrylate-glycidyl methacrylate-styrene-2- ethylhexyl acrylate graft copolymer, minimum average molecular weight (in amu), 9,600

Methyl vinyl ether-maleic acid copolymer), minimum number average 25153–40–6 molecular weight (in amu), 75,000

Methyl vinyl ether-maleic acid copolymer, calcium sodium salt, min- 62386–95–2 imum number average molecular weight (in amu), 900,000

Monophosphate ester of the block copolymer a-hydro-w- None hydroxypoly(oxyethylene) poly(oxypropylene) poly(oxyethylene); the poly(oxypropylene) content averages 37–41 moles, average molecular weight (in amu), 8,000

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Polymer CAS No.

a-(p-Nonylphenyl)-w-hydroxypoly(oxyethylene) mixture of dihydrogen None phosphate and monohydrogen phosphate esters and the corresponding ammonium, calcium, magnesium, monoethanolamine, potassium, sodium, and zinc salts of the phosphate esters; the nonyl group is a propylene trimer isomer and the poly(oxyethylene) content averages 30 moles

a-(p-Nonylphenyl)-w-hydroxypoly(oxyethylene) sulfate, and its ammo- None nium, calcium, magnesium, monoethanolamine, potassium, sodium, and zinc salts; the nonyl group is a propylene trimer isomer and the poly(oxyethylene) content averages 30-90 moles of ethylene oxide

a-(p-Nonylphenyl-w-hydroxypoly(oxypropylene) block polymer with None poly(oxyethylene); polyoxypropylene content of 10–60 moles; polyoxyethylene content of 10–80 moles; molecular weight (in amu), 1,200–7,100.

a-(r-Nonylphenyl)poly(oxypropylene) block polymer with poly(oxy- 37251–69–7 ethylene); poly oxyethylene content 30 to 90 moles; minimum number average molecular weight (in amu), 1,889

Octadecanoic Acid, 12-Hydroxy-, Homopolymer Ester with 2- 1373125–59–7 Methylloxirane Polymer with Oxirane monobutyl Ether, minimum number average molecular weight (in amu), 4,500

Octadecanoic acid, 12-hydroxy-, homopolymer, octadecanoate min- 58128–22–6) imum number average molecular weight (in amu), 1,370

a-cis-9-Octadecenyl-w-hydroxypoly(oxyethylene); the octadecenyl None group is derived from oleyl alcohol and the poly(oxyethylene) content averages 20 moles

Octadecyl acrylate-acrylic acid copolymer, octadecyl acrylate-dodecyl None acrylate-acrylic acid copolymer, octadecyl methacrylate-butyl acrylate-acrylic acid copolymer, octadecyl methacrylate-hexyl acrylate- acrylic acid copolymer, octadecyl methacrylate-dodecyl acrylate- acrylic acid copolymer, or octadecyl methacrylate-dodecyl methacrylate-acrylic acid copolymer, minimum number average molecular weight (in amu) 3,000

Oleic acid diester of a-hydro-w-hydroxypoly(oxyethylene); the None poly(oxyethylene), average molecular weight (in amu), 2,300

2-oxepanone, homopolymer, minimum number average molecular 24980–41–4 weight (in amu) 52,000

Oxirane, decyl-, reaction products with polyethylene-polypropylene gly- 903890–89–1 col ether with trimethylolpropane (3:1)

Oxirane, hexadecyl-, reaction products with polyethylene-poly- 893427–80–0 propylene glycol ether with trimethylolpropane (3:1)

Oxirane, 2-methyl-, polymer with oxirane, dimethyl ether, minimum 61419–46–3 number average molecular weight (in amu), 2,800

Oxirane, methyl-, polymer with oxirane, ether with 2-ethyl-2- 903890–90–4 (hydroxymethyl) – 1,3 - propanediol (3:1), reaction products with tetradecyloxirane

Oxirane, methyl-, polymer with oxirane, mono[2-(2-butoxyethoxy) ethyl] 85637–75–8 ether, minimum number average molecular weight (in amu), 2,500

Oxirane, methyl-, polymer with Oxirane, Monobutyl Ether 9038–95–3

Oxirane, 2-methyl-, polymer with oxirane, minimum number average 9003–11–6 molecular weight (in amu), 1,100

Oxirane, 2-methyl-, polymer with oxirane, mono [2-[2-(2- 926031–36–9 butoxymethylethoxy)methylethoxy]methylethyl] ether, minimum number average molecular weight (in amu), 3,000

Polyamide polymer derived from sebacic acid, vegetable oil acids with None or without dimerization, terephthalic acid and/or ethylenediamine

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Polymer CAS No.

Polyethylene glycol-polyisobutenyl anhydride-tall oil fatty acid copoly- 68650–28–2 mer, minimum number average molecular weight (in amu), 2,960

Polyethylene, oxidized, minimum number average molecular weight (in None amu), 1,200

Polymers produced by the reaction of either 1,6-hexanediisocyanate; 2,4,4-trimethyl-1,6-hexanediisocyanate; 5-isocyanato-1- (isocyanatomethyl)-fxsp0;1,3,3fxsp0;-trimethyIcyclohexane (isophoronediisocyanate); 4,4′-methylene-bis-1,1′- cyclohexanediisocyanate; 4,4′-methylene-bis-1,1′ benzyldiisocyanate; or 1,3-bis-(2-isocyanatopropan-2-yl)benzene with polyethylene glycol and end-capped with one or a mixture of more than one of octanol, decanol, dodecanol, tetradecanol, hexadecanol, octadecanol, and octadec-9-enol or polyethyleneglycol ethers of octanol, decanol, dodecanol, tetradecanol, hexadecanol, octadecanol, and octadec-9-enol, minimum number average molecular weight (in amu), 20,000

1161844–26–3, 1161844–30–9, 1161844–43–4, 1161844–51–4, 1161844–53–6, 693252–31–2, 162993–60–4, 630102–86–2. Polymethylene polyphenylisocyanate, polymer with ethylene diamine, None diethylene triamine and sebacoyl chloride, cross-linked; minimum number average molecular weight (in amu), 100,000

Polyoxyalkylated glycerol fatty acid esters; the mono-, di-, or 61791–23–9, 68201–46–7, 68440–49–3, 68458–88–8, triglyceride mixtures of C8 through C22, primarily C8 through C18 68606–12–2, 68648–38–4, 70377–91–2, 70914–02– saturated and unsaturated, fatty acids containing up to 15% water 2, 72245–12–6, 72698–41–3, 180254–52–8, by weight reacted with a minimum of three moles of either ethylene 248273–72–5, 308063–50–5, 952722–33–7 oxide or propylene oxide; the resulting polyoxyalkylated glycerol ester polymer minimum number average molecular weight (in amu), 1,500

Poly(oxy-1,2-ethanediyl), a-hydro-w-hydroxy-, polymer with 1, 1′-meth- 39444–87–6 ylene-bis-[4-isocyanatocyclohexane], minimum number average molecular weight (in amu), 1800

Polyoxyethylated primary amine (C14–C18); the fatty amine is derived None from an animal source and contains 3% water; the poly(oxyethylene) content averages 20 moles

Polyoxyethylated sorbitol fatty acid esters; the polyoxyethylated sor- None bitol solution containing 15% water is reacted with fatty acids limited to C12, C14, C16, and C18, containing minor amounts of associated fatty acids; the poly(oxyethylene) content averages 30 moles.

Polyoxyethylated sorbitol fatty acid esters; the sorbitol solution con- None taining up to 15% water is reacted with 20–50 moles of ethylene oxide and aliphatic alkanoic and/or alkenoic fatty acids C8 through C22 with minor amounts of associated fatty acids; the resulting polyoxyethylene sorbitol ester having a minimum molecular weight (in amu), 1,300

Poly(oxyethylene/oxypropylene) monoalkyl (C6–C10) ether sodium fu- 102900–02–7 marate adduct, minimum number average molecular weight (in amu), 1,900

Polyoxymethylene copolymer, minimum number average molecular None weight (in amu), 15,000

Poly(oxypropylene) block polymer with poly(oxyethylene), molecular None weight (in amu), 1,800–16,000

Poly(phenylhexylurea), cross-linked, minimum average molecular None weight (in amu), 36,000

Polypropylene 9003–07–0

Polystyrene, minimum number average molecular weight (in amu), 9003–53–6 50,000

Polytetrafluoroethylene 9002–84–0

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Polymer CAS No.

Polyvinyl acetate, copolymer with maleic anhydride, partially None hydrolyzed, sodium salt, minimum number average molecular weight (in amu), 53,000

Polyvinylpyrrolidone butylated polymer, minimum number average mo- 26160–96–3 lecular weight (in amu), 9,500

Polyvinyl acetate, minimum molecular weight (in amu), 2,000 None

Polyvinyl acetate—polyvinyl alcohol copolymer, minimum number av- 25213–24–5 erage molecular weight (in amu), 50,000

Polyvinyl alcohol 9002–89–5

Polyvinyl chloride None

Polyvinyl chloride, minimum number average molecular weight (in 9002–86–2 amu), 29,000

Poly(vinylpyrrolidone), minimum number average molecular weight (in 9003–39–8 amu), 4,000

Poly(vinylpyrrolidone-1-eicosene), minimum average molecular weight 28211–18–9 (in amu), 3,000

Poly(vinylpyrrolidone-1-hexadecene), minimum average molecular 63231–81–2 weight (in amu), 4,700

1-propanesulfonic acid, 2-methyl-2-[(1-oxo-2-propenyl)amino]-, mono- 107568–12–7 sodium salt, polymer with ethenol and ethenyl acetate, minimum number average molecular weight (in amu) 50,000

2-Propene-1-sulfonic acid sodium salt, polymer with ethenol and eth- None enyl acetate, number average molecular weight (in amu) 6,000– 12,000

2-propenoic acid, butyl ester, polymer with ethenylbenzene, methyl 2- 27306–39–4 methyl-2-propenoate and 2-propenoic acid (in amu), 1900.

2-Propenoic acid, butyl ester, polymer with ethyl 2-propenoate and N- 33438–19–6 (hydroxymethyl)-2-propenamide, minimum number average molecular weight (in amu), 30,000

2-Propenoic acid, 2-ethylhexyl ester, polymer with ethenylbenzene 25153–46–2 14,000 daltons

2-Propenoic acid, 2-ethylhexyl ester, polymer with ethenylbenzene and 68240–06–2 2-methylpropyl 2-methyl-2-propenoate, minimum number average molecular weight (in amu), 18,000

2-Propenoic acid, 2-hydroxyethyl ester, polymer with a-[4- 1007234–89–0 (ethenyloxy)butyl]-w-hydroxypoly (oxy-1,2-ethanediyl), minimum number average molecular weight (in amu), 17,000

[2-propenoic acid, 2-methyl-, C12-16-alkyl esters, telomers with 1- 950207–35–9 dodecanethiol, polyethylene-polypropylene glycol ether with propylene glycol monomethacrylate (1:1), and styrene 2,2’-(1,2- diazenediyl)bis[2-methylbutanenitrile]-initiated, minimum number average molecular weight (in amu), 4,000

2-Propenoic acid, methyl ester, polymer with ethenyl acetate, 886993–11–9 hydrolyzed, sodium salts

2-Propenoic acid, 2-methyl-, 2-ethylhexyl ester, telomer with 1- 1283712–50–4 dodecanethiol, ethenylbenzene and 2-methyloxirane polymer with oxirane monoether with 1,2-propanediol mono(2-methyl-2- propenoate), hydrogen 2-sulfobutanedioate, sodium salt, 2, 2′-(1,2- diazenediyl)bis[2-methylpropanenitrile]-initiated, minimum number average molecular weight (in amu), 1,200

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Polymer CAS No.

2-Propenoic acid, 2-methyl-, phenylmethyl ester, polymer with 2-prope- CASRN 1246766–57–3 noic acid and sodium 2-methyl-2-[(1-oxo-2-propen-1-yl)amino]-1- propanesulfonate (1:1), peroxydisulfuric acid ([HO)S(O)2]202) sodium salt (1:2)-initiated minimum number average molecular weight >1,000 Daltons; maximum number average molecular weight 10,000 Daltons

2-Propenoic acid, 2-methyl-, polymer with butyl 2-propenoate and 25036–16–2 ethenylbenzene, minimum number average molecular weight (in amu), 17,000

2-Propenoic acid, 2-Methyl-, Polymer with Butyl 2-Propenoate, Methyl 153163–36–1 2-Methyl-2-Propenoate, Methyl 2-Propenoate and 2-Propenoic Acid, graft, Compound with 2-Amino-2-Methyl-1-Propanol

2-Propenoic Acid, 2-Methyl-, Polymer with Ethenylbenzene, 2- 146753–99–3 Ethylhexyl 2-Propenoate, 2-Hydroxyethyl 2-Propenoate, N- (Hydroxymethyl) -2-Methyl-2-Propenamide and Methyl 2-Methyl-2- Propenoate, Ammonium Salt

2-Propenoic acid, 2-methyl-, polymers with Bu acrylate, Et acrylate, 890051–63–5 Me methacrylate and polyethylene glycol methacrylate C16-18-alkyl ethers, minimum number average molecular weight (in amu), 13,000

2-Propenoic acid, 2-methyl-, telomer with 2-ethylhexyl 2-propenoate, 1260001–65–7 2-propanol and sodium 2-methyl-2-[(1-oxo-2-propen-1-yl) amino]-1- propanesulfonate (1:1), sodium salt, minimum number average molecular weight (in amu): 2,900

2-Propenoic acid, monoester with 1,2-propanediol, polymer with a-[4- 955015–23–3 (ethenyloxy) butyl]-w-hydroxypoly (oxy-1,2-ethanediyl) and 2,5- furandione, minimum number average molecular weight (in amu), 25,000

2-propenoic acid polymer, with 1,3-butadiene and ethenylbenzene, 25085–39–6 minimum number average molecular weight (in amu), 9400

2-Propenoic acid, polymer with ethenylbenzene and (1-methylethenyl) 129811–24–1 benzene, sodium salt, minimum number average molecular weight (in amu), 2,800

2-Propenoic acid, polymer with a-[4-(ethenyloxy) butyl]-w-hydroxypoly 251479–97–7 (oxy-1,2-ethanediyl) and 2,5-furandione, sodium salt, minimum number average molecular weight (in amu), 25,000

2-Propenoic acid, polymer with a-[4-(ethenyloxy) butyl]-w-hydroxypoly 518026–64–7 (oxy-1,2-ethanediyl) and 1,2-propanediol mono-2-propenoate, potassium sodium salt, minimum number average molecular weight (in amu), 16,000

2-Propenoic acid, polymer with a-[4-(ethenyloxy) butyl]-w-hydroxypoly 250591–84–5 (oxy-1, 2-ethanediyl), sodium salt, minimum number average molecular weight (in amu), 24,000

2-Propenoic acid, polymer with 2-propenamide, sodium salt, minimum 25085–02–3 number average molecular weight (in amu), 18,000

2-Propenoic acid, sodium salt, polymer with 2-propenamide, minimum 25987–30–8 number average molecular weight (in amu), 18,000

2-Propenoic, 2-methyl-, polymers with ethyl acrylate and polyethylene 888969–14–0 glycol methylacrylate C18-22 alkyl ethers

2-Pyrrolidone, 1-ethenyl-, polymer with ethenol, minimum number av- 26008–54–8 erage molecular weight (in amu), 23,000

Silane, dichloromethyl- reaction product with silica minimum number 68611–44–9 average molecular weight (in amu), 3,340,000

Silane, trimethoxy[3-(oxiranylmethoxy)propyl]-, hydrolysis products with 68584–82–7 silica, minimum number average molecular weight (in amu), 640,000

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Polymer CAS No.

Silicic acid, sodium salt, reaction products with chlorotrimethylsilane None and iso-propyl alcohol, reaction with poly(oxypropylene)- poly(oxyethylene) glycol, minimum number average molecular weight (in amu), 75,000

Sodium polyflavinoidsulfonate, consisting chiefly of the copolymer of None catechin and leucocyanidin

Soybean oil, ethoxylated; the poly(oxyethylene) content averages 10 61791–23–9 moles or greater

Starch, oxidized, polymers with Bu acrylate, tert-Bu acrylate and sty- 204142–80–3 rene, minimum number average molecular weight (in amu), 10,000

Stearyl methacrylate-1,6-hexanediol dimethacrylate copolymer, min- None imum molecular weight (in amu), 100,000

Styrene, copolymers with acrylic acid and/or methacrylic acid, with None none and/or one or more of the following monomers: Acrylamidopropyl methyl sulfonic acid, methallyl sulfonic acid, 3- sulfopropyl acrylate, 3-sulfopropyl methacrylate, hydroxypropyl methacrylate, hydroxypropyl acrylate, hydroxyethyl methacrylate, hydroxyethyl acrylate, and/or lauryl methacrylate; and its sodium, potassium, ammonium, monoethanolamine, and triethanolamine salts; the resulting polymer having a minimum number average molecular weight (in amu), 1200

Styrene-ethylene-propylene block copolymer, minimum number aver- 108388–87–0 age molecular weight (in amu), 125,000

Styrene, 2-ethylhexyl acrylate, butyl acrylate copolymer, minimum 30795–23–4 number average molecular weight (in amu), 4,200

Styrene-2-ethylhexyl acrylate-glycidyl methacrylate-2-acrylamido-2- None methylpropanesulfonic acid graft copolymer, minimum number average molecular weight (in amu), 12,500

Styrene-maleic anhydride copolymer None

Styrene-maleic anhydride copolymer, ester derivative None

Tall oil, polymer with polyethylene glycol and succinic anhydride 1398573–80–2 monopolyisobutylene derivs., minimum number average molecular weight (in amu), 1,200

Tetradecyl acrylate-acrylic acid copolymer, minimum number average None molecular weight (in amu), 3,000

Tetraethoxysilane, polymer with hexamethyldisiloxane, minimum num- 104133–09–7 ber average molecular weight (in amu), 2,500

Tetraethoxysilane, polymer with hexamethyldisiloxane, minimum num- 104133–09–7 ber average molecular weight (in amu), 6,500

a-[p-(1,1,3,3-Tetramethylbutyl)phenyl]-w-hydroxypoly(oxyethylene) pro- 9036–19–5 duced by the condensation of 1 mole of p-(1,1,3,3- 9002–93–1 tetramethylbutyl)phenol with a range of 30-70 moles of ethylene oxide

a-[p-(1,1,3,3-Tetramethylbutyl)phenyl] poly(oxypropylene) block poly- None mer with poly(oxyethylene); the poly(oxypropylene) content averages 25 moles, the poly(oxyethylene) content averages 40 moles, the molecular weight (in amu) averages 3,400

a-[2,4,6-Tris[1-(phenyl)ethyl]phenyl]-w-hydroxy poly(oxyethylene) None poly(oxypropylene) copolymer, the poly(oxypropylene) content averages 2–8 moles, the poly(oxyethylene) content averages 16– 30moles, average molecular weight (in amu), 1,500

Urea-formaldehyde copolymer, minimum average molecular weight (in 9011–05–6 amu), 30,000

Vinyl acetate-allyl acetate-monomethyl maleate copolymer, minimum None average molecular weight (in amu), 20,000

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Polymer CAS No.

Vinyl acetate-ethylene copolymer, minimum number average molec- 24937–78–8 ular weight (in amu), 69,000

Vinyl acetate polymer with none and/or one or more of the following None monomers: Ethylene, propylene, N-methyl acrylamide, acrylamide, monoethyl maleate, diethyl maleate, monooctyl maleate, dioctyl maleate, maleic anhydride, maleic acid, octyl acrylate, butyl acrylate, ethyl acrylate, methyl acrylate, acrylic acid, octyl methacrylate, butyl methacrylate, ethyl methacrylate, methyl methacrylate, methacrylic acid, carboxyethyl acrylate, and diallyl phthalate; and their corresponding sodium, potassium, ammonium, isopropylamine, triethylamine, monoethanolamine and/or triethanolamine salts; the resulting polymer having a minimum number average molecular weight (in amu), 1,200

Vinyl acetate-vinyl alcohol-alkyl lactone copolymer, minimum number None average molecular weight (in amu), 40,000; minimum viscosity of 18 centipoise

Vinyl alcohol-disodium itaconate copolymer, minimum average molec- None ular weight (in amu), 50,290

Vinyl alcohol-vinyl acetate copolymer, benzaldehyde-o-sodium None sulfonate condensate, minimum number average molecular weight (in amu), 20,000

Vinyl alcohol-vinyl acetate-monomethyl maleate, sodium salt-maleic None acid, disodium salt-g-butyrolactone acetic acid, sodium salt copolymer, minimum number average molecular weight (in amu), 20,000

Vinyl chloride-vinyl acetate copolymers None

Vinyl pyrrolidone-acrylic acid copolymer, minimum number average 28062–44–4 molecular weight (in amu), 6,000

Vinyl pyrrolidone-dimethylaminoethylmethacrylate copolymer, minimum 30581–59–0 number average molecular weight (in amu), 20,000

Vinyl pyrrolidone-styrene copolymer 25086–29–7

[67 FR 36528, May 24, 2002] (2) Spore preparations of Bacillus EDITORIAL NOTE: For FEDERAL REGISTER ci- thuringiensis Berliner shall be produced tations affecting § 180.960, see the List of CFR by pure culture fermentation proce- Sections Affected, which appears in the dures with adequate control measures Finding Aids section of the printed volume during production to detect any and at www.fdsys.gov. changes from the characteristics of the parent strain or contamination by § 180.1011 Viable spores of the micro- other microorganisms. organism Bacillus thuringiensis (3) Each lot of spore preparation, Berliner; exemption from the re- prior to the addition of other mate- quirement of a tolerance. rials, shall be tested by subcutaneous (a) For the purposes of this section injection of at least 1 million spores the microbial insecticide for which ex- into each of five laboratory test mice emption from the requirement of a tol- weighing 17 grams to 23 grams. Such erance is being established shall have test shall show no evidence of infection the following specifications: or injury in the test animals when ob- (1) The microorganism shall be an au- served for 7 days following injection. thentic strain of Bacillus thuringiensis (4) Spore preparations shall be free of Berliner conforming to the morpho- the Bacillus thuringiensis b-exotoxin logical and biochemical characteristics when tested with the fly larvae tox- of Bacillus thuringiensis as described in icity test (‘‘Microbial Control of In- Bergey’s Manual of Determinative Bac- sects and Mites,’’ R.P.M. Bond et al., p. teriology, Eighth Edition. 280 ff., 1971). This specification can be satisfied either by determining that

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each master seed lot brought into pro- to food commodities after harvest, and duction is a Bacillus thuringiensis strain to animals. which does not produce b-exotoxin (b) Diatomaceous earth may be safely under standard manufacturing condi- used in accordance with the following tions or by periodically determining conditions. Application shall be lim- that b-exotoxin synthesized during ited solely to spot and/or crack and spore production is eliminated by the crevice treatments in food or feed proc- subsequent spore-harvesting procedure. essing and food or feed storage areas in (b) Exemption from the requirement accordane with the precribed condi- of a tolerance is established for resi- tions: dues of the microbial insecticide Bacil- (1) It is used or intended for use for lus thuringiensis Berliner, as specified control of insects in food or feed proc- in paragraph (a) of this section, in or essing and food or feed storage areas: on honey and honeycomb and all other Provided, That the food or feed is re- raw agricultural commodities when it moved or covered prior to such use. is applied either to growing crops, or (2) To assure safe use of the insecti- when it is applied after harvest in ac- cide, its label and labeling shall con- cordance with good agricultural prac- form to that registered by the U.S. En- tices. vironmental Protection Agency, and it shall be used in accordance with such [36 FR 22540, Nov. 25, 1971, as amended at 38 label and labeling. FR 19045, July 17, 1973; 42 FR 28540, June 3, 1977; 45 FR 43721, June 30, 1980; 45 FR 56347, [65 FR 33716, May 24, 2000] Aug. 25, 1980; 74 FR 26533, June 3, 2009] § 180.1019 Sulfuric acid; exemption § 180.1016 Ethylene; exemption from from the requirement of a toler- the requirement of a tolerance. ance. (a) Residues of sulfuric acid are ex- Ethylene is exempted from the re- empted from the requirement of a tol- quirement of a tolerance for residues erance when used in accordance with when: good agricultural practice when used (a) For all food commodities, it is as a herbicide in the production of gar- used as a plant regulator on plants, lic and onions, and as a potato vine seeds, or cuttings and on all food com- dessicant in the production of potatoes. modities after harvest and when ap- (b) Residues of sulfuric acid are ex- plied in accordance with good agricul- empted from the requirement of a tol- tural practices. erance in cattle, meat; goat, meat; hog, (b) Injected into the soil to cause pre- meat; horse, meat; sheep, meat; poul- mature germination of witchweed in try, fat; poultry, meat; poultry, meat, bean (lima and string), cabbage, canta- byproducts; egg; milk; fish, shellfish, loupe, collard, corn, cotton, cucumber, and irrigated crops when it results eggplant, okra, onion, pasture grass, from the use of sulfuric acid as an inert pea (field and sweet), peanut, pepper, ingredient in a pesticide product used potato, sweet potato, sorghum, soy- in irrigation conveyance systems and bean, squash, tomato, turnip, and wa- lakes, ponds, reservoirs, or bodies of termelon fields as part of the U.S. De- water in which fish or shellfish are cul- partment of Agriculture witchweed tivated. The sulfuric acid is not to ex- control program. ceed 10% of the pesticide formulation [39 FR 33315, Sept. 17, 1974, as amended at 40 (non-aerosol formulations only). FR 19477, May 5, 1975; 64 FR 31505, June 11, [69 FR 40787, July 7, 2004, as amended at 74 1999] FR 26533, June 3, 2009]

§ 180.1017 Diatomaceous earth; exemp- § 180.1020 Sodium chlorate; exemption tion from the requirement of a tol- from the requirement of a toler- erance. ance. (a) Diatomaceous earth is exempted Sodium chlorate is exempted from from the requirement of a tolerance for the requirement of a tolerance for resi- residues when used in accordance with dues when used as a defoliant or des- good agricultural practice in pesticide iccant in accordance with good agricul- formulations applied to growing crops, tural practice on the following crops:

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Bean, dry, seed Copper compounds CAS Reg. No. Corn, field, forage Corn, field, grain Basic copper carbonate (mala- Corn, field, stover chite) ...... 1184–64–1 Corn, pop, grain Copper ammonia complex ...... 16828–95–8 Copper ethylenediamine complex 13426–91–0 Corn, pop, stover Copper hydroxide ...... 20427–59–2 Corn, sweet, forage Copper octanoate ...... 20543–04–8 Corn, sweet, stover Copper oxychloride ...... 1332–65–6 Cotton, undelinted seed Copper oxychloride sulfate ...... 8012–69–9 Flax, seed Copper salts of fatty and rosin Grain, aspirated fractions acids ...... 9007–39–0 Guar, seed Copper sulfate basic ...... 1344–73–6 Pea, southern Copper sulfate pentahydrate ...... 7758–99–8 Pepper, nonbell Cuprous oxide ...... 1317–19–1 Potato Rice, grain (c) Copper sulfate pentahydrate (CAS Rice, straw Reg. No. 7758–99–8) is exempt from the Safflower, seed requirement of a tolerance when ap- Sorghum, forage, forage plied as a fungicide to growing crops or Sorghum, grain, forage to raw agricultural commodities after Sorghum, grain, grain harvest, and as a bactericide/fungicide Sorghum, grain, stover in or on meat, fat and meat by-prod- Soybean, forage Soybean, hay ucts of cattle, sheep, hogs, goats, Soybean, seed horses and poultry, milk and eggs when Sunflower, seed applied as a bactericide/fungicide to Wheat, grain animal premises and bedding. [74 FR 47457, Sept. 16, 2009] (d) Copper (II) hydroxide (CAS Reg. No. 20427–59–2) is exempt from the re- § 180.1021 Copper; exemption from the quirement of a tolerance when applied requirement of a tolerance. to growing crops or to raw agricultural (a) Copper is exempted from the re- commodities as an inert ingredient (for quirement of a tolerance in cattle, pH control) in pesticide products. meat; goat, meat; hog, meat; horse, [65 FR 68912, Nov. 15, 2000, as amended at 69 meat; sheep, meat; milk, poultry, fat; FR 4069, Jan. 28, 2004; 71 FR 46110, Aug. 11, poultry, meat; poultry, meat byprod- 2006; 74 FR 26534, June 3, 2009; 74 FR 47457, ucts; egg, fish, shellfish, and irrigated Sept. 16, 2009] crops when it results from the use of: (1) Copper sulfate as an algicide or § 180.1022 Iodine-detergent complex; herbicide in irrigation conveyance sys- exemption from the requirement of tems and lakes, ponds, reservoirs, or a tolerance. bodies of water in which fish or shell- The aqueous solution of hydriodic fish are cultivated. acid and elemental iodine, including (2) Basic copper carbonate (mala- one or both of the surfactants (a) chite) as an algicide or herbicide in im- polyoxypropylene-polyoxyethylene gly- pounded and stagnant bodies of water col nomionic block polymers (min- (3) Copper triethanolamine and cop- imum average molecular weight 1,900) per monoethanolamine as an algicide and (b) a-(p- nonylphenyl)-omega- or herbicide in fish hatcheries, lakes, hydroxypoly (oxyethylene) having a ponds, and reservoirs maximum average molecular weight of (4) Cuprous oxide bearing antifouling 748 and in which the nonyl group is a coatings for control of algae or other propylene trimer isomer, is exempted coatings for control of algae or other organisms on submerged concrete or from the requirement of a tolerance for other (irrigation) structures. residues in egg, and poultry, fat; poul- (b) The following copper compounds try, meat; poultry, meat byproducts are exempt from the requirement of a when used as a sanitizer in poultry tolerance when applied (primarily) as a drinking water. fungicide to growing crops using good [74 FR 26534, June 3, 2009] agricultural practices:

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§ 180.1023 Propanoic acid; exemptions aquatic herbicide applied to irrigation from the requirement of a toler- conveyance systems in accordance with ance. the following conditions: (a) Postharvest application of pro- (a) It is to be used only in programs panoic acid or a mixture of methylene of the Bureau of Reclamation, U.S. De- bispropionate and oxy(bismethylene) partment of Interior, and cooperating bisproprionate when used as a fun- water user organizations. gicide is exempted from the require- (b) It is to be applied as an emulsion ment of a tolerance for residues in or at an initial concentration not to ex- on the following raw agricultural com- ceed 750 parts per million. modities: Alfalfa, forage; alfalfa, hay; (c) It is not to be applied when there alfalfa, seed; barley, grain; is any likelihood that the irrigation Bermudagrass, forage; Bermudagrass, water will be used as a source of raw hay; bluegrass, forage; bluegrass, hay; water for a potable water system or bromegrass, forage; bromegrass, hay; where return flows of such treated irri- clover, forage; clover, hay; corn, field, gation water into receiving rivers and grain; corn, pop, grain; cowpea, hay; streams would contain residues of xy- fescue, forage; fescue, hay; lespedeza, lene in excess of 10 parts per million. forage; lespedeza, hay; lupin; oat, (d) Xylene to be used as an aquatic grain; orchardgrass, forage; herbicide shall meet the requirement orchardgrass, hay; peanut, hay; pea, limiting the presence of a polynuclear field, hay; ryegrass, Italian, hay; sor- aromatic hydrocarbons as listed in 21 ghum, grain, grain; soybean, hay; CFR 172.250. sudangrass, forage; sudangrass, hay; [38 FR 16352, June 22, 1973, as amended at 50 timothy, forage; timothy, hay; vetch, FR 2980, Jan. 3, 1985] forage; vetch, hay; and wheat, grain. (b) Propanoic acid is exempt from the § 180.1027 Nuclear polyhedrosis virus requirement of a tolerance for residues of Heliothis zea; exemption from in or on cattle, meat; cattle, meat by- the requirement of a tolerance. products; goat, meat; goat, meat by- (a) For the purposes of this section, products; hog, meat; hog meat byprod- the viral insecticide must be produced ucts; horse, meat; horse, meat byprod- with an unaltered and unadulterated ucts; sheep, meat; sheep meat byprod- inoculum of the single-embedded ucts; and, poultry, fat; poultry meat; Heliothis zea nuclear polyhedrosis virus poultry meat byproducts; milk, and (HzSNPV). The identity of the seed egg when applied as a bactericide/fun- virus must be assured by periodic gicide to livestock drinking water, checks. poultry litter, and storage areas for si- (b) Each lot of active ingredient of lage and grain. the viral insecticide shall have the fol- (c) Preharvest and postharvest appli- lowing specifications: cation of propanoic acid (CAS Reg. No. (1) The level of extraneous bacterial 79–09–4), propanioc acid, calcium salt contamination of the final (CAS Reg. No. 4075–81–4), and propanioc unformulated viral insecticide should sodium salt (CAS Reg. No. 137–40–6) are not exceed 107 colonies per gram as de- exempted from the requirement of a termined by an aerobic plate on tolerance on all crops when used as ei- trypticase soy agar. ther an active or inert ingredient in ac- (2) Human pathogens, e.g., Sal- cordance with good agricultural prac- monella, Shigella, or Vibrio, must be tice in pesticide formulations applied absent. to growing crops, to raw agricultural (3) Safety to mice as determined by commodities before and after harvest an intraperitoneal injection study and to animals. must be demonstrated. [69 FR 47025, Aug. 4, 2004, as amended at 74 (4) Identity of the viral product, as FR 26534, June 3, 2009] determined by the most sensitive and standardized analytical technique, e.g., § 180.1025 Xylene; exemption from the restriction endonuclease and/or SDS- requirement of a tolerance. PAGE analysis, must be demonstrated. Xylene is exempted from the require- (c) Exemptions from the requirement ment of a tolerance when used as an of a tolerance are established for the

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residues of the microbial insecticide § 180.1043 Gossyplure; exemption from Heliothis zea NPV, as specified in para- the requirement of a tolerance. graphs (a) and (b) of this section, in or The pheromone gossyplure, a 1:1 mix- on all agricultural commodities. ture of (Z,Z)- and (Z,E)-7,11- [60 FR 42460, Aug. 16, 1995, as amended at 74 hexadecadien-1-ol acetate) is exempt FR 26534, June 3, 2009] from the requirement of a tolerance in or on the raw agricultural commodity § 180.1033 Methoprene; exemption cotton, undelinted seed when applied to from the requirement of a toler- cotton from capillary fibers. ance. [74 FR 26534, June 3, 2009] Methoprene is exempt from the requirement of a tolerance in or on all § 180.1049 Carbon dioxide; exemption food commodities when used to control from the requirement of a toler- insect larvae. ance. The insecticide carbon dioxide is ex- [68 FR 34829, June 11, 2003] empted from the requirement of a tolerance when used after harvest in § 180.1037 Polybutenes; exemption modified atmospheres for stored insect from the requirement of a tolerance. control on food commodities. (a) Polybutenes are exempt from the [65 FR 33716, May 24, 2000] requirement of a tolerance for residues § 180.1050 Nitrogen; exemption from in or on the raw agricultural com- the requirements of a tolerance. modity cotton, undelinted seed when used as a sticker agent for formula- The insecticide nitrogen is exempted tions of the attractant gossyplure (1:1 from the requirements of a tolerance mixture of (Z,Z)- and (Z,E)-7,11- when used after harvest in modified hexadecadien-1-ol acetate) to disrupt atmospheres for stored product insect the mating of the pink bollworm. control on all food commodities. (b) Polybutenes are exempt from the [65 FR 33716, May 24, 2000] requirement of a tolerance for residues in or on the raw agricultural com- § 180.1052 2,2,5-trimethyl-3-dichloro- modity artichoke when used as a stick- acetyl-1,3-oxazolidine; exemption from the requirement of a toler- er agent in multi-layered laminted ance. controlled-release dispensers of (Z)-11- hexaadecenal to disrupt the mating of 2,2,5-trimethyl-3-dichloroacetyl-1,3- the artichoke plume moth. oxazolidine is exempted from the requirement of a tolerance when used as [74 FR 26534, June 3, 2009] an inert ingredient in formulations of the herbicides S-ethyl § 180.1040 Ethylene glycol; exemption dipropylthiocarbamate, S-propyl from the requirement of a toler- dipropylthiocarbamate, and S-ethyl ance. diisobutylthiocarbamate applied to Ethylene glycol as a component of corn fields before the corn plants pesticide formulations is exempt from emerge from the soil with a maximum the requirement of a tolerance when of 0.5 pound of the inert ingredient per used in foliar applications to peanut acre. plants. [45 FR 51201, Aug. 1, 1980] [43 FR 41393, Sept. 18, 1978] § 180.1054 Calcium hypochlorite; exemptions from the requirement of a § 180.1041 Nosema locustae; exemption tolerance. from the requirement of a tolerance. (a) Calcium hypochlorite is exempted from the requirement of a tolerance The insecticide Nosema locustae is ex- when used preharvest or postharvest in empted from the requirement of a tol- solution on all raw agricultural com- erance for residues in or on all raw ag- modities. ricultural commodities. (b) Calcium hypochlorite is exempted [47 FR 21537, May 19, 1982] from the requirement of a tolerance in

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or on grape when used as a fumigant (a) Application shall be limited sole- postharvest by means of a chlorine ly to point source dispensers or point generator pad. source chopped fibers containing the [59 FR 59165, Nov. 16, 1994, as amended at 74 tomato pinworm insect pheromone. FR 26534, June 3, 2009] (b) Cumulative yearly application cannot exceed 200 grams of tomato § 180.1056 Boiled linseed oil; exemp- pinworm pheromone per acre. tion from requirement of tolerance. [58 FR 34376, June 25, 1993] Boiled linseed oil (containing no more than 0.33 percent manganese § 180.1065 2-Amino-4,5-dihydro-6-meth- naphthenate and no more than 0.33 per- yl-4-propyl-s-triazolo(1,5- cent cobalt naphthenate) is exempt alpha)pyrimidin-5-one; exemption from the requirement of a tolerance from the requirement of a toler- when used as a coating agent for S- ance. ethyl hexahydro-1H-azepine-1- The inert ingredient, 2-amino-4,5- carbothioate. No more than 15 percent dihydro-6-methyl-4-propyl-s- of the pesticide formulation may con- triazolo(1,5-alpha)pyrimidin-5-one is sist of ‘‘boiled linseed oil.’’ This exemp- exempted from the requirement of a tion is limited to use on rice before edi- tolerance when used as an emetic at ble parts form. not more than 0.3 percent in formulations of paraquat dichloride. Further [46 FR 33270, June 29, 1981] restrictions on this exemption are that § 180.1057 Phytophthora palmivora; this ingredient may not be advertised exemption from requirement of tol- as an emetic and the paraquat product erance. may not be promoted in any way be- Phytophthora palmivora is exempted cause of the inclusion of this inert in- from the requirement of a tolerance in gredient. or on the raw agricultural commodity [70 FR 46431, Aug. 10, 2005] fruit, citrus. [74 FR 26534, June 3, 2009] § 180.1067 Methyl eugenol and malathion combination; exemption from § 180.1058 Sodium diacetate; exemp- the requirement of a tolerance. tion from the requirement of a tol- The insect attractant methyl eugenol erance. and the insecticide malathion are ex- Sodium diacetate, when used empt from the requirement of toler- postharvest as a fungicide, is exempt ances on all raw agricultural commod- from the requirement of a tolerance for ities when used in combination in Ori- residues in or on alfalfa, hay; ental fruit fly eradication programs Bermudagrass, hay; bluegrass, hay; under the authority of the U.S. Depart- bromegrass, hay; clover,hay; corm, ment of Agriculture, in accordance field, grain; corn, pop, grain; oat, grain; with the following directions and speci- orchardgrass, hay; sorghum, grain, fications: grain; sudangrass, hay; ryegrass, (a) The combination shall be at the Italian, hay; timothy, hay. ratio of three parts methyl eugenol to one part technical malathion (3:1). [74 FR 26534, June 3, 2009] (b) This combination is to be impreg- § 180.1064 Tomato pinworm insect nated on a carrier (cigarette filter tips pheromone; exemption from the re- (cellulose acetate); cotton strings; fi- quirement of a tolerance. berboard squares) or mixed with a jel An exemption from the requirement cleared under 40 CFR 180.920 or 180.950. of a tolerance is established for com- (c) The maximum actual dosage per bined residues of both components of application per acre shall be 28.35 the tomato pinworm insect pheromone grams (one ounce avoirdupois) methyl (E)-4-tridecen-1-yl acetate and (Z)-4- eugenol and 9.45 grams (one-third (0.33) tridecen-1-yl acetate in or on all raw ounce avoirdupois) technical mala- agricultural commodities (preharvest) thion. in accordance with the following pre- [47 FR 9002, Mar. 3, 1982, as amended at 69 FR scribed conditions: 23142, Apr. 28, 2004]

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§ 180.1068 C12-C18 fatty acid potassium which includes seeding, potting and salts; exemption from the require- transplanting activities. ment of a tolerance. (3) Pre-plant and at-transplant applications. C12-C18 fatty acids (saturated and unsaturated) potassium salts are exempt- (4) Incorporation into seedling and ed from the requirement of a tolerance planting beds. for residues in or on all raw agricul- (5) Applications to cuttings and bare tural commodities when used in ac- roots. cordance with good agricultural prac- (6) Applications to the field that tice. occur after the harvested crop has been removed. [60 FR 34871, July 5, 1995] (7) Soil-directed applications around and adjacent to all plants. § 180.1069 (Z)-11-Hexadecenal; exemp- (8) Applications to rangelands, which tion from the requirement of a tol- is land, mostly grasslands, whose erance. plants can provide food (i.e., forage) for An exemption from the requirement grazing or browsing animals. of a tolerance is established for resi- (9) Use in chemigation and irrigation dues of the biological insecticide systems (via flood, drip, or furrow ap- (pheromone) (Z)-11-hexadecenal when plication with no overhead spray appli- used as a sex attractant on artichoke cations). plants to control the artichoke plume (10) Application as part of a dry fer- moth. tilizer on which an active ingredient is impregnated. [47 FR 14906, Apr. 7, 1982] (11) Aerial and ground applications that occur when no above-ground har- § 180.1070 Sodium chlorite; exemption from the requirement of a toler- vestable food commodities are present ance. (usually pre-bloom). (12) Application as part of an animal Sodium chlorite is exempted from feed-through product. the requirement of a tolerance for resi- (13) Applications as gel and solid dues when used in accordance with (non-liquid/non-spray) crack and crev- good agricultural practice as a seed- ice treatments that place the gel or soak treatment in the growing of the bait directly into or on top of the raw agricultural commodities vege- cracks and crevices via a mechanism table, brassica, leafy, group 5 and rad- such as a syringe. ish, roots and radish, tops. (14) Applications to the same crop [74 FR 26534, June 3, 2009] from which the food commodity is derived, whether the plant fraction(s) in- § 180.1071 Peanuts, Tree Nuts, Milk, tended for harvest are present or not, Soybeans, Eggs, Fish, Crustacea, e.g., applications of peanut meal when and Wheat; exemption from the re- applied to peanut plants. quirement of a tolerance. (b) Specific chemical substances. Resi- (a) General. Residues resulting from dues resulting from the use of the fol- the following uses of the food com- lowing substances as either an inert or modity forms of peanuts, tree nuts, an active ingredient in a pesticide for- milk, soybeans, eggs (including putres- mulation are exempted from the re- cent eggs), fish, crustacea, and wheat quirement of a tolerance under FFDCA are exempted from the requirement of section 408, if such use is in accordance a tolerance in or on all food commod- with good agricultural practices and ities under FFDCA section 408 (when such use is included in paragraph (a): used as either an inert or an active in- Chemical Substance CAS No. gredient in a pesticide formulation), if such use is in accordance with good ag- Caseins ...... 9000–71–9 ricultural practices: Caseins, ammonium complexes ...... 9005–42–9 Caseins, hydrolyzates ...... 65072–00–6 (1) Use in pesticide products intended Caseins, potassium complexes ...... 68131–54–4 to treat seeds. Caseins, sodium complexes ...... 9005–46–3 (2) Use in nursery and greenhouse operations, as defined in 40 CFR 170.3, [70 FR 1360, Jan. 7, 2005]

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§ 180.1072 Poly-D-glucosamine § 180.1076 Viable spores of the micro- (chitosan); exemption from the re- organism Bacillus popilliae; exemp- quirement of a tolerance. tion from the requirement of a tol- (a) An exemption from the require- erance. ment of a tolerance is established for (a) For the purposes of this section residues of the biological plant growth the microbial insecticide for which ex- regulator poly-D-glucosamine when emption from the requirement of a tol- used as a seed treatment in or on bar- erance is being established shall have ley, beans, oats, peas, rice, and wheat. the following specifications: (b) An exemption from the require- (1) The microorganism shall be an au- ment of a tolerance is established for thentic strain of Bacillus popilliae con- residues of the biological plant growth forming to the morphological and bio- regulator poly-D-glucosamine when chemical characteristics of Bacillus used as a pesticide in the production popilliae as described in Bergey’s Man- any raw agricultural commodity. ual of Determinative Bacteriology, [60 FR 19524, Apr. 19, 1995] Eighth Edition. (2) Spore preparations of Bacillus § 180.1073 Isomate-M; exemption from popilliae shall be produced by an ex- the requirement of a tolerance. traction process from diseased Japa- The oriental fruit moth pheromone nese beetles, and may contain a small (Isomate-M) (Z-8-dodecen-l-yl acetate, percentage of the naturally occurring E-8-dodecen-l-yl acetate, Z-8-dodecen-l- milky disease bacterium Bacillus ol) is exempt from the requirement of a lentimorbus. tolerance in or on all the raw agricul- (3) Each lot of spore preparation, tural commodities (food and feed) in- prior to the addition of other mate- cluding, peach; quince; nectarine; and rials, shall be tested by subcutaneous nut, macadamia when used in orchards injection of at least 1 million spores with encapsulated polyethylene tubing into each of five laboratory test mice to control oriental fruit moth. weighing 17 grams to 23 grams. Such [74 FR 26534, June 3, 2009] test shall show no evidence of infection of injury in the test animals when ob- § 180.1074 F.D.&C. Blue No. 1; exemp- served for 7 days following injection. tion from the requirement of a tol- (b) Exemption from the requirement erance. of a tolerance is established for resi- F.D.&C. Blue No. 1 is exempted from dues of the microbial insecticide Bacil- the requirement of a tolerance when lus popilliae, as specified in paragraph used as an aquatic plant control agent. (a) of this section in or on grass, pas- [47 FR 25963, June 16, 1982] ture, forage and grass, rangeland, forage when it is applied to growing crops § 180.1075 Colletotrichum in accordance with good agricultural gloeosporioides f. sp. aeschynomene; practices. exemption from the requirement of a tolerance. [47 FR 38535, Sept. 1, 1982, as amended at 74 FR 26535, June 3, 2009] An exemption from the requirement of a tolerance is established for resi- § 180.1080 Plant volatiles and dues of the mycoherbicide pheromone; exemptions from the Colletotrichum gloeosporioides f. sp. requirement of a tolerance. aeschynomene in or on the following An exemption from the requirement raw agricultural commodities: of a tolerance is established for resi- COMMODITY dues of the plant volatiles cyclic Aspirated grain fractions decadiene, cyclic decene, cyclic Rice, grain pentadecatriene, and decatriene and Soybean, forage the pheromone Z-2-isopropenyl-1- Soybean, hay methylcyclobutaneethanol; Z-3,3-di- Soybean, seed methyl-D1,b-cyclohexaneethanol; Z-3,3- [47 FR 25742, June 15, 1982, as amended at 74 dimethyl-D1,a-cyclohexaneethanal; E- FR 26534, June 3, 2009] 3,3-dimethyl-D1,a-cyclohexaneethanal 715

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combination when applied to cotton in § 180.1087 Sesame stalks; exemption hollow synthetic fibers. from the requirement of a tolerance. [48 FR 28442, June 22, 1983] An exemption from the requirement § 180.1083 Dimethyl sulfoxide; exemp- of a tolerance is established for resi- tion from the requirement of a tol- dues of the biorational nematicide ses- erance. ame stalk in or on the following raw Dimethyl sulfoxide (DMSO) [CAS agricultural commodities: Almond; al- Registry Number 67–68–5] is exempted mond, hulls; cotton, undelinted seed; from the requirement of a tolerance cotton, gin byproducts; soybean, seed; when used as an inert solvent or cosol- soybean, forage; soybean, hay; aspi- vent in formulations with the following rated grain fractions; potato; beet, pesticides when used in accordance sugar, roots; beet, sugar, tops; tomato; with good agricultural practices in or pepper, bell; squash; strawberry; egg- on the following raw agricultural com- plant; cucumber; carrot, roots; radish, modities: roots; radish, top; turnip, roots; turnip, (a) Carbaryl (1-naphthyl methyl-car- tops; onion; pea, dry; pea, succulent; bamate) melon; grape; walnut; orange; grapefruit; mulberry; peach; apple; apricot; Pea, dry, seed blackberry; loganberry; pecan; cherry; Pea, succulent plum, and cranberry. (b) O-O-Diethyl O-(2-isopropyl-6- [74 FR 26535, June 3, 2009] methyl-4-pyrimidinyl) phosphorothioate § 180.1089 Poly-N-acetyl-D-glu- Pea, dry, seed cosamine; exemption from the re- Pea, succulent quirement of tolerance. An exemption from the requirement [48 FR 54819, Dec. 7, 1983, as amended at 74 FR 26535, June 3, 2009] of a tolerance is established for residues of the biochemical nematicide § 180.1084 Monocarbamide dihydrogen poly-N-acetyl-D-glucosamine on a vari- sulfate; exemption from the require- ety of agricultural crops. ment of a tolerance. [53 FR 10249, Mar. 30, 1988] Monocarbamide dihydrogen sulfate is exempted from the requirement of a § 180.1090 Lactic acid; exemption from tolerance when used as a herbicide or the requirement of a tolerance. desiccant in or on all raw agricultural Lactic acid (2-hydroxypropanoic commodities. acid) is exempted from the requirement [53 FR 12152, Apr. 13, 1988] of a tolerance when used as a plant growth regulator in or on all raw agri- § 180.1086 3,7,11-Trimethyl-1,6,10- cultural commodities. dodecatriene-1-ol and 3,7,11- trimethyl-2,6,10-dodecatriene-3-ol; [53 FR 15286, May 4, 1988] exemption from the requirement of a tolerance. § 180.1091 Aluminum isopropoxide and aluminum secondary butoxide; ex- The insect pheromone containing the emption from the requirement of a active ingredients 3,7,11-trimethyl- tolerance. 1,6,10-dodecatriene-1-ol and 3,7,11- Aluminum isopropoxide (CAS Reg. trimethyl-2,6,10-dodecatriene-3-ol is ex- No. 555–31–7) and aluminum secondary empted from the requirement of a tol- butoxide (CAS Reg. No. 2269–22–9) are erance in or on all raw agricultural exempted from the requirement of a commodities. tolerance when used in accordance [52 FR 12165, Apr. 15, 1987; 52 FR 29014, Aug. with good agricultural practices as sta- 5, 1987] bilizers in formulations of the insecticide amitraz [N′-(2,4-dimethylphenyl)- N-[[(2,4-dimethylphenyl)imino]-N-

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methylmethanimidamide] applied to § 180.1100 Gliocladium virens isolate growing crops or animals. GL-21; exemption from the requirement of a tolerance. [53 FR 34509, Sept. 7, 1988; 53 FR 36696, Sept. 21, 1988] An exemption from the requirement of a tolerance is established for resi- § 180.1092 Menthol; exemption from dues of the biofungicide Gliocladium the requirement of a tolerance. virens GL-21 in or on all raw agricultural commodities when used either as An exemption from the requirement a fungicide for inoculation of plant of a tolerance is established for resi- growth media in greenhouses or on ter- dues of the pesticidal chemical men- restrial food crops grown outdoors in thol in or on honey and honeycomb accordance with good agricultural when used in accordance with good ag- practices. ricultural practice in over-wintering bee hives. [60 FR 48659, Sept. 20, 1995; 60 FR 52248, Oct. 5, 1995] [74 FR 26535, June 3, 2009] § 180.1101 Parasitic (parasitoid) and § 180.1095 Chlorine gas; exemptions predatory insects; exemption from from the requirement of a toler- the requirement of a tolerance. ance. Parasitic (parasitoid) and predatory Chlorine gas is exempted from the re- insects are exempted from the require- quirement of a tolerance when used ment of a tolerance for residues when preharvest or postharvest in solution they are used in accordance with good on all raw agricultural commodities. agricultural and pest control practices to control insect pests of stored raw [56 FR 21309, May 8, 1991] whole grains such as corn, small grains, rice, soybeans, peanuts, and § 180.1097 GBM-ROPE; exemption from other legumes either bulk or the requirement of a tolerance. warehoused in bags. For the purposes The grape berry moth pheromone of this rule, the parasites (parasitoids) (GBM-ROPE) containing the active in- and predators are considered to be spe- gredients (Z)-9-dedecenyl acetate and cies of Hymenoptera in the genera (Z)-11-tetradecenyl acetate is exempt Trichogramma, Trichogrammatidae; from the requirement of a tolerance in Bracon, Braconidae; Venturia, or on the raw agricultural commodity Mesostenus, Ichneumonidae; Anisopteromalus, Choetospila, grape when used in orchards with en- Lariophagus, Dibrachys, Habrocytus, capsulated polyethylene tubing to con- Pteromalus, Pteromalidae; trol grape berry moth. Cephalonomia, Holepyris, Laelius, [74 FR 26535, June 3, 2009] Bethylidae; and of Hemiptera in the genera Xylocoris, Lyctocoris, and § 180.1098 Gibberellins [Gibberellic Dufouriellus, Anthocoridae. Whole in- Acids (GA3 and GA4 + GA7), and So- sects, fragments, parts, and other resi- dium or Potassium Gibberellate]; dues of these parasites and predators exemption from the requirement of remain subject to 21 U.S.C. 342(a)(3). a tolerance. [57 FR 14646, Apr. 22, 1992] An exemption from the requirement of a tolerance is established for resi- § 180.1102 Trichoderma harzianum dues of gibberellins [gibberellic acids KRL-AG2 (ATCC #20847) strain T– (GA3 and GA4 + GA7), and sodium or 22; exemption from requirement of potassium gibberellate] in or on all a tolerance. food commodities when used as plant An exemption from the requirement regulators on plants, seeds, or cuttings of a tolerance is established for resi- and on all food commodities after har- dues of the biofungicide Trichoderma vest in accordance with good agricul- harzianum KRL-AG2 (ATCC #20847); tural practices. also known as strain T-22 when applied in/or on all food commodities. [64 FR 31505, June 11, 1999] [64 FR 16860, Apr. 7, 1999]

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§ 180.1103 Isomate-C; exemption from § 180.1111 Bacillus subtilis GB03; ex- the requirement of a tolerance. emption from the requirement of a The codling moth pheromone tolerance. (Isomate-C) E,E-8,10-dodecenyl alcohol, The biofungicide Bacillus subtilis GB03 dodecanol, tetradecanol is exempt from is exempted from the requirement of a the requirements of a tolerance in or tolerance in or on all raw agricultural on all raw agricultural commodities commodities when used in accordance when formulated in polyethylene with good agricultural practices. pheromone dispensers for use in orchards with encapsulated polyethylene [73 FR 50556, Aug. 27, 2008] tubing to control codling moth. § 180.1113 Lagenidium giganteum; ex- [74 FR 26535, June 3, 2009] emption from the requirement of a tolerance. § 180.1107 Delta endotoxin of Bacillus thuringiensis variety kurstaki en- Lagenidium giganteum (a fungal orga- capsulated into killed Pseudomonas nism) is exempt from the requirement fluorescens; exemption from the re- of a tolerance in or on the raw agricul- quirement of a tolerance. tural commodities aspirated grain frac- The delta endotoxin of Bacillus tions; grass, forage; grass, hay; rice, thuringiensis variety kurstaki encap- grain; rice, straw; soybean, seed; soy- sulated into killed Pseudomonas bean, forage; soybean, hay; rice, wild, fluorescens is exempt from the require- grain. ments of a tolerance in or on all raw [74 FR 26535, June 3, 2009] agricultural commodities. [56 FR 28328, June 20, 1991] § 180.1114 Pseudomonas fluorescens A506, Pseudomonas fluorescens § 180.1108 Delta endotoxin of Bacillus 1629RS, and Pseudomonas syringae thuringiensis variety San Diego en- 742RS; exemptions from the re- capsulated into killed Pseudomonas quirement of a tolerance. fluorescens; exemption from the re- The biological pesticides quirement of a tolerance. Pseudomonas fluorescens A506, The delta endotoxin of Bacillus Pseudomonas fluorescens 1629RS, and thuringiensis variety San Diego encap- Pseudomonas syringae 742RS are ex- sulated into killed Pseudomonas empted from the requirement of a tol- fluorescens is exempt from the require- erance in or on all raw agricultural ments of a tolerance in or on all raw commodities when applied as a frost agricultural commodities. protection agent or biological control [56 FR 28326, June 20, 1991] agent to growing agricultural crops in accordance with good agricultural § 180.1110 3-Carbamyl-2,4,5-trichloro- practices. benzoic acid; exemption from the requirement of a tolerance. [57 FR 42700, Sept. 16, 1992] An exemption from the requirement § 180.1118 Spodoptera exigua nuclear of a tolerance is established for the res- polyhedrosis virus; exemption from idues of 3-carbamyl-2,4,5- the requirement of a tolerance. trichlorobenzoic acid in or on all raw agricultural commodities which occur An exemption from the requirement from the direct application of of a tolerance is established for the mi- chlorothalonil to crops in § 180.275 (a) crobial pest control agent Spodoptera and (b) and/or as an inadvertent residue exigua nuclear polyhedrosis virus when resulting from the soil metabolism of used as a pesticide control agent on all chlorothalonil when applied to crops in raw agricultural commodities. § 180.275 (a) and (b), and subsequent up- take by rotated crops when used ac- [58 FR 25784, Apr. 28, 1993] cording to approved agricultural practices. [57 FR 24552, June 10, 1992]

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§ 180.1119 Azadirachtin; exemption empted from the requirement of a tol- from the requirement of a toler- erance when used as carriers in pes- ance. ticide formulations for application to An exemption from the requirement growing crops only. These dispensers of a tolerance is established for the bio- shall conform to the following speci- chemical azadirachtin, which is iso- fications: lated from the berries of the Neem tree (1) Exposure must be limited to inad- (Azadirachta indica), when used as a vertent physical contact only. The de- pesticide at 20 grams or less per acre on sign of the dispenser must be such as to all raw agricultural commodities. preclude any contamination by its components of the raw agricultural [58 FR 8696, Feb. 17, 1993] commodity (RAC) or processed foods/ feeds derived from the commodity by § 180.1120 Streptomyces sp. strain K61; exemption from the requirement of virtue of its proximity to the RAC or a tolerance. as a result of its physical size. (2) The dispensers must be applied The biological pesticide Streptomyces discretely. This exemption does not sp. strain K61 is exempted from the re- apply to components of semiochemical quirement of a tolerance in or on all formulations applied in a broadcast raw agricultural commodities when manner either to a crop field plot or to used as a fungicide for the treatment of individual plants. seeds, cuttings, transplants, and plants (b) A semiochemical dispenser is a of agricultural crops in accordance single enclosed or semi-enclosed unit with good agricultural practices. that releases semiochemical(s) into the [58 FR 21403, Apr. 21, 1993] surrounding atmosphere via volatilization and is applied in a manner to pro- § 180.1121 Boric acid and its salts, vide discrete application of the borax (sodium borate decahydrate), semiochemical(s) into the environ- disodium octaborate tetrahydrate, ment. boric oxide (boric anhydride), sodium borate and sodium metabo- (c) Semiochemicals are chemicals rate; exemptions from the require- that are emitted by plants or animals ment of a tolerance. and modify the behavior of receiving An exemption from the requirement organisms. These chemicals must be of a tolerance is established for resi- naturally occurring or substantially dues of the pesticidal chemical boric identical to naturally occurring acid and its salts, borax (sodium borate semiochemicals. decahydrate), disodium octaborate tet- [58 FR 64494, Dec. 8, 1993] rahydrate, boric oxide (boric anhydride), sodium borate and sodium met- § 180.1124 Arthropod pheromones; ex- aborate, in or on raw agricultural com- emption from the requirement of a modities when used as an active ingre- tolerance. dient in insecticides, herbicides, or fun- Arthropod pheromones, as described gicides preharvest or postharvest in ac- in § 152.25(b) of this chapter, when used cordance with good agricultural prac- in retrievably sized polymeric matrix tices. dispensers are exempt from the requirement of a tolerance in or on all [58 FR 44283, Aug. 20, 1993] raw agricultural commodities when ap- § 180.1122 Inert ingredients of plied to growing crops only at a rate semiochemical dispensers; exemp- not to exceed 150 grams active ingre- tions from the requirement of a tol- dient/acre/year in accordance with good erance. agricultural practices. (a) All inert ingredients of [59 FR 14759, Mar. 30, 1994] semiochemical dispenser products formulated with, and/or contained in, dis- § 180.1126 Codlure, (E,E)-8,10- pensers made of polymeric matrix ma- Dodecadien-1-ol; exemption from terials (including the monomers, plas- the requirement of a tolerance. ticizers, dispersing agents, anti- An exemption from the requirement oxidants, UV protectants, stabilizers, of a tolerance is established for the in- and other inert ingredients) are ex- sect pheromone codlure, (E,E)-8,10-

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dodecadien-1-ol, on all raw agricultural table crops—asparagus, beans (includ- commodities in accordance with the ing forage hay), beets, carrots, celery, following prescribed conditions: cole crops (cabbage, broccoli, brussels (a) Application shall be limited sole- sprouts, cauliflower), collards (kale, ly to codlure dispensers that conform mustard greens, turnip greens, kohl- to the following specifications: rabi), corn, fresh (field, sweet, pop, (1) Commodity exposure must be lim- seed), corn fodder and forage, chinese ited to inadvertent physical contact. cabbage, cowpeas, cucurbitis (cucum- The design of the dispenser must be bers, squash, pumpkin), egg plant, en- such as to preclude any exposure of its dive (escarole), horseradish (radish, ru- components to the raw agricultural tabagas, turnip roots), leafy greens commodity (RAC) or processed foods/ (spinach, swiss chard), lettuce (head feeds derived from the commodity due leaf), okra, parsley, parsnip, peas, peas to its proximity to the RAC or as a re- with pods, peppers, potatoes, sugar sult of its physical size. Dispensers beets, tomatoes; the following tree must be of such size and construction fruit, berry and nut crops—almonds, that they are readily recognized post- apples, apricots, berries (blackberry, application. boysenberry, dewberry, loganberry, (2) The dispensers must be applied raspberry), blueberry, cherry, citrus discretely, i.e., placed in the field in (grapefruit, kumquat, lemon, lime, or- easily perceived distinct locations in a ange, tangelo, and tangerine) cran- manner that does not prevent later re- berry, grapes, melons, (watermelon, trieval. This exemption does not apply honeydew, crenshaw, cantaloupe, ca- to codlure applied in a broadcast man- saba, persian), nectarines, pears, pe- ner either to a crop field plot or to in- cans, peaches, and strawberry as dis- dividual plants. persed from the end-use product Corn (b) A codlure dispenser is a single en- Rootworm Bait ®, a pesticidal bait, in closed or semi-enclosed unit that re- accordance with the prescribed condi- leases codlure into the surrounding at- tions in paragraph (a) of this section. mosphere via volatilization and is ap- (a) Cumulative yearly application plied in a manner to provide discrete cannot exceed 20 grams of each floral application (i.e., in easily perceived dis- attractant/acre/application. tinct locations in a manner that does (b) [Reserved] not prevent later retrieval) of the [59 FR 15857, Apr. 5, 1994] codlure into the environment. [59 FR 9931, Mar. 2, 1994] § 180.1128 Bacillus subtilis MBI 600; exemption from the requirement of § 180.1127 Biochemical pesticide plant a tolerance. floral volatile attractant com- An exemption from the requirement pounds: cinnamaldehyde, cinnamyl of a tolerance is established for resi- alcohol, 4-methoxy cinnamaldehyde, dues of the biofungicide Bacillus subtilis 3-phenyl propanol, 4-methoxy phenethyl alcohol, indole, and 1,2,4- MBI 600 in or on all food commodities, trimethoxybenzene; exemptions including residues resulting from post- from the requirement of a toler- harvest uses, when applied or used in ance. accordance with good agricultural Residues of the biochemical pesticide practices. plant floral volatile attractant com- [74 FR 15869, Apr. 8, 2009] pounds: cinnamaldehyde, cinnamyl alcohol, 4-methoxy cinnamaldehyde, 3- § 180.1130 N-(n-octyl)-2-pyrrolidone phenyl propanol, 4-methoxy phenethyl and N-(n-dodecyl)-2-pyrrolidone; ex- alcohol, indole, and 1,2,4- emptions from the requirement of a trimethoxybenzene are exempt from tolerance. the requirement of a tolerance in or on (a) N-(n-octyl)-2-pyrrolidone and N- the following raw agricultural com- (n-dodecyl)-2-pyrrolidone are exempt modities: the following field crops—al- from the requirement of a tolerance falfa, clover, cotton, dandelion, pea- when used as solvents in cotton defo- nuts (including hay), rice, sorghum liant formulations containing (milo), soybeans, sunflower, sweet po- thidiazuron and diuron as active ingre- tatoes, and wheat; the following vege- dients.

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(b) N-(n-octyl)-2-pyrrolidone is ex- application, in or on all food commod- empt from the requirement of a toler- ities. ance when used as a solvent in formu- [65 FR 66181, Nov. 3, 2000] lations containing pyraflufen-ethyl as an active ingredient at a concentration § 180.1141 Sodium p-nitrophenolate; not to exceed 20% by weight. exemption from the requirement of a tolerance. [79 FR 10682, Feb. 26, 2014] The biochemical sodium p- § 180.1131 Ampelomyces quisqualis iso- nitrophenolate is exempted from the late M10; exemption from the re- requirement of a tolerance when used quirement of a tolerance. as a plant growth regulator in end-use product at a concentration of 0.3% by The biological fungicide Ampelomyces weight and applied at an application quisqualis isolate M10 is exempted from rate of 20 g of a.i. per acre or less per the requirement of a tolerance in or on application, in or on all food commod- all raw agricultural commodities when ities. used as a fungicide on agricultural crops in accordance with good agricul- [65 FR 66181, Nov. 3, 2000] tural practices. § 180.1142 1,4-Dimethylnaphthalene; [59 FR 33437, June 29, 1994] exemption from the requirement of a tolerance. § 180.1135 Pasteuria penetrans; exemp- An exemption from the requirement tion from the requirement of a tol- of a tolerance is established for the res- erance. idues of the plant growth regulator, The biological nematicide Pasteuria 1,4-dimethylnaphthalene (1,4-DMN), penetrans is exempted from the require- when applied postharvest to all sprout- ment of a tolerance in or on all raw aging root, tuber, and bulb crops in ac- ricultural commodities, except roots cordance with good agricultural prac- and tubers, when used as a nematicide tices. in the production of fruits and vegeta- [77 FR 68697, Nov. 16, 2012] bles in greenhouses. § 180.1143 Methyl anthranilate; exemp- [59 FR 66741, Dec. 28, 1994] tion from the requirement of a tolerance. § 180.1139 Sodium 5-nitroguaiacolate; exemption from the requirement of Residues of methyl anthranilate, a a tolerance. biochemical pesticide, are exempt from the requirement of a tolerance in or on The biochemical sodium 5- all food commodities, when used in ac- nitroguiacolate is exempted from the cordance with good agricultural prac- requirement of a tolerance when used tices. as a plant growth regulator in end-use products at a concentration of 0.1% by [67 FR 51088, Aug. 7, 2002] weight and applied at an application § 180.1144 Candida oleophila isolate I- rate of 20 g of a.i. per acre or less per 182; exemption from the require- application, in or on all food commod- ment of a tolerance. ities. Candida oleophila isolate I-182, when [65 FR 66181, Nov. 3, 2000] used as a post-harvest biological fungicide, is exempted from the require- § 180.1140 Sodium o-nitrophenolate; ment of a tolerance in or on all raw ag- exemption from the requirement of ricultural commodities. a tolerance. [60 FR 11033, Mar. 1, 1995] The biochemical sodium o- nitrophenolate is exempted from the § 180.1145 Pseudomonas syringae; ex- requirement of a tolerance when used emption from the requirement of a as a plant growth regulator in end-use tolerance. products at a concentration of 0.2% by Pseudomonas syringae is exempted weight and applied at an application from the requirement of a tolerance on rate of 20 g of a.i. per acre or less per all raw agricultural commodities when

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applied postharvest according to good § 180.1153 Lepidopteran pheromones; agricultural practices. exemption from the requirement of a tolerance. [60 FR 12703, Mar. 8, 1995] Lepidopteran pheromones that are § 180.1146 Beauveria bassiana Strain naturally occurring compounds, or GHA; exemption from the require- identical or substantially similar syn- ment of a tolerance. thetic compounds, designated by an unbranched aliphatic chain (between 9 Beauveria bassiana Strain GHA is ex- and 18 carbons) ending in an alcohol, empted from the requirement of a tol- aldehyde or acetate functional group erance in or on all raw agricultural and containing up to 3 double bonds in commodities when applied to growing the aliphatic backbone, are exempt crops according to good agricultural from the requirement of a tolerance in practices. or on all raw agricultural commodities. [60 FR 18547, Apr. 12, 1995] This exemption only pertains to those situations when the pheromone is: Ap- § 180.1148 Occlusion Bodies of the plied to growing crops at a rate not to Granulosis Virus of Cydia exceed 150 grams active ingredient/ pomenella; tolerance exemption. acre/year in accordance with good agri- An exemption from the requirement cultural practices; and applied as a of a tolerance is established for resi- post-harvest treatment to stored food commodities at a rate not to exceed 3.5 dues of the microbial pest control grams active ingredient/1,000 ft2/year agent Occlusion Bodies of the (equivalent to 150 grams active ingre- Granulosis Virus of Cydia pomonella dient/acre/year) in accordance with (codling moth) in or on all raw agricul- good agricultural practices. tural commodities. [71 FR 45399, Aug. 9, 2006] [60 FR 42450, Aug. 16, 1995] § 180.1154 CryIA(c) and CryIC derived § 180.1149 Inclusion bodies of the delta-endotoxins of Bacillus multi-nuclear polyhedrosis virus of thuringiensis var. kurstaki encap- Anagrapha falcifera; exemption sulated in killed Pseudomonas from the requirement of a toler- fluorescens, and the expression ance. plasmid and cloning vector genetic constructs. The microbial pest control agent inclusion bodies of the multi-nuclear CryIA(c) and CryIC derived delta- polyhedrosis virus of Anagrapha endotoxins of Bacillus thuringiensis var. falcifera is exempted from the require- kurstaki encapsulated in killed ment of a tolerance in or on all raw ag- Pseudomonas fluorescens and the expres- ricultural commodities when used to sion plasmid and cloning vector genetic constructs are exempt from the control certain lepidopteran pest spe- requirement of a tolerance when used cies. in or on all raw agricultural commod- [60 FR 37020, July 19, 1995] ities. [60 FR 47489, Sept. 13, 1995] § 180.1150 6-Benzyladenine; exemption from the requirement of a toler- § 180.1156 Cinnamaldehyde; exemption ance. from the requirement of a toler- The biochemical plant regulator 6- ance. benzyladenine (6–BA) is exempt from Cinnamaldehyde (3-phenyl-2- the requirement of a tolerance in or on propenal) is exempted from the re- apple and pear when applied at a rate quirement of a tolerance in or on all of ≤182 grams of active ingredient per food commodities, when used as a fun- acre per season, and in or on pistachio gicide, insecticide, and algaecide in ac- when applied at a rate of ≤60 grams of cordance with good agricultual prac- active ingredient per acre per season. tices. [72 FR 13179, Mar. 21, 2007] [64 FR 7804, Feb. 17, 1999; 64 FR 14099, Mar. 24, 1999]

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§ 180.1157 Cytokinins; exemption from concentration of pelargonic acid up to the requirement of a tolerance. 170 ppm per application on food contact An exemption from the requirement surfaces such as equipment, pipelines, of a tolerance is established for resi- tanks, vats, fillers, evaporators, dues of cytokinins (specifically: aque- pasteurizers and aseptic equipment in ous extract of seaweed meal and restaurants, food service operations, kinetin) in or on all food commodities dairies, breweries, wineries, beverage when used as plant regulators on and food processing plants. plants, seeds, or cuttings and on all [62 FR 28364, May 23, 1997, as amended at 64 food commodities after harvest in ac- FR 31505, June 11, 1999; 68 FR 7935, Feb. 19, cordance with good agricultural prac- 2003] tices. § 180.1160 Jojoba oil; exemption from [64 FR 31505, June 11, 1999] the requirement of a tolerance. § 180.1158 Auxins; exemption from the The insecticide and spray tank adju- requirement of a tolerance. vant jojoba oil is exempted from the An exemption from the requirement requirement of a tolerance in or on all of a tolerance is established for resi- raw agricultural commodities when ap- dues of auxins (specifically: indole-3- plied at the rate of 1.0% or less of the acetic acid and indole-3-butyric acid) final spray in accordance with good ag- in or on all food commodities when ricultural practices, provided the used as plant regulators on plants, jojoba oil does not contain seeds, or cuttings and on all food com- simmondsin, simmondsin-2-ferulate, modities after harvest in accordance and related conjugated organonitriles with good agricultural practices. including demethyl simmondsin and didemethylsimmondsin. [64 FR 31505, June 11, 1999] [61 FR 2121, Jan. 25, 1996] § 180.1159 Pelargonic acid; exemption from the requirement of tolerances. § 180.1161 Clarified hydrophobic extract of neem oil; exemption from (a) An exemption from the require- the requirement of a tolerance. ment of a tolerance is established for residues of pelargonic acid in or on all Clarified hydrophobic extract of food commodities when used as a plant neem oil is exempt from the require- regulator on plants, seeds, or cuttings ment of a tolerance on all food com- and on all food commodities after har- modities when used as a botanical fun- vest in accordance with good agricul- gicide/insecticide/miticide. tural practices. [67 FR 43552, June 28, 2002] (b) Pelargonic acid when used as an herbicide is exempt from the require- § 180.1162 Acrylate polymers and co- ment of a tolerance on all plant food polymers; exemption from the re- commodities provided that: quirement of a tolerance. (1) Applications are not made di- (a) Acrylate polymers and copoly- rectly to the food commodity except mers are exempt from the requirement when used as a harvest aid or desiccant of a tolerance when used as inert ingre- to: any root and tuber vegetable, bulb dients in pesticidal formulations ap- vegetable or cotton. plied to growing, raw agricultural com- (2) When pelargonic acid is used as a modities. This tolerance exemption harvest aid or desiccant, applications covers the acrylate polymers/copoly- must be made no later than 24 hours mers that are intrinsically safe and al- prior to harvest. ready listed in TSCA inventory or will (c) An exemption from the require- meet the polymer tolerance exemption ment of a tolerance is established for from requirements of residues of pelargonic acid in or on all premanufacturing notification under 40 raw agricultural commodities and in CFR 723.250. Polymers exempted can be processed commodities, when such resi- used as dispensers, resins, fibers, and dues result from the use of pelargonic beads, as long as the fibers, beads and acid as an antimicrobial treatment in resins particle sizes are greater than 10 solutions containing a diluted end-use microns and insoluble in water. This

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exemption pertains to the acrylate quirement of a tolerance for residues polymers/copolymers used as inert in- when used as a component of food gredients for sprayable and dispenser grade oil of mustard, in or on all raw pesticide formulations that are applied agricultural commodities, when ap- on food crops. Any acrylate polymers/ plied according to approved labeling. copolymers used for encapsulating material must be cleared as an inert in- [61 FR 24894, May 17, 1996] gredient when used in pesticide formulation applied on food crops. § 180.1176 Sodium bicarbonate; exemption from the requirement of a tol- (b) For the purposes of this exemp- erance. tion, acrylate polymers/copolymers used as inert ingredients in an end-use The biochemical pesticide sodium bi- formulation must meet the definition carbonate is exempted from the re- for a polymer as given in 40 CFR quirement of a tolerance in or on all 723.250(b), are not automatically ex- raw agricultural commodities when ap- cluded by 40 723.250(d), and meet the plied as a fungicide or post-harvest fun- tolerance exemption criteria in 40 CFR gicide in accordance with good agricul- 723.250(e)(1), 40 CFR 723.250 (e)(2) or 40 tural practices. CFR 723.250(e)(3). Therefore, acrylate [61 FR 67473, Dec. 23, 1996] polymers and copolymers that are already listed in the TSCA inventory or § 180.1177 Potassium bicarbonate; ex- will meet the polymer tolerance exemption from the requirement of a emption under 40 CFR 723.250 as tolerance. amended on March 29, 1995 are covered by this exemption. The biochemical pesticide potassium bicarbonate is exempted from the re- [61 FR 6551, Feb. 21, 1996] quirement of a tolerance in or on all raw agricultural commodities when ap- § 180.1163 Killed Myrothecium plied as a fungicide or post-harvest fun- verrucaria; exemption from the requirement of a tolerance. gicide in accordance with good agricultural practices. Killed Myrothecium verrucaria is exempted from the requirement of a tol- [61 FR 67473, Dec. 23, 1996] erance in or on all raw agricultural commodities when applied as a pre- § 180.1178 Formic acid; exemption seed or pre- or post-planting soil treat- from the requirement of a toler- ment alone or mixed with water and ance. the mixed suspension be applied The pesticide formic acid is exempted through drip or border irrigation sys- from the requirement of a tolerance in tems and the indicator mycotoxin lev- or on honey and honeycomb when used els do not exceed 15 ppm. to control tracheal mites and suppress [61 FR 11315, Mar. 20, 1996, as amended at 61 varroa mites in bee colonies, and ap- FR 58332, Nov. 14, 1996] plied in accordance with label use directions. § 180.1165 Capsaicin; exemption from the requirement of a tolerance. [74 FR 26535, June 3, 2009] Capsaicin is exempt from the require- § 180.1179 Plant extract derived from ment of a tolerance in or on all food Opuntia lindheimeri, Quercus commodities when used in accordance falcata, Rhus aromatica, and with approved label rates and good ag- Rhizophoria mangle; exemption ricultural practice. from the requirement of a tolerance. [63 FR 39521, July 23, 1998] The biochemical pesticide plant ex- § 180.1167 Allyl isothiocyanate as a tract derived from Opuntia lindheimeri, component of food grade oil of mus- Quercus falcata, Rhus aromatica, and tard; exemption from the require- Rhizophoria mangle is exempted from ment of a tolerance. the requirement of a tolerance in or on The insecticide and repellent Allyl all raw agricultural commodities when isothiocyanate is exempt from the re- applied as a nematicide/plant regulator

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in accordance with good agricultural § 180.1187 L-glutamic acid; exemption practices. from the requirement of a tolerance. [62 FR 24842, May 7, 1997] L-glutamic acid is exempt from the § 180.1180 Kaolin; exemption from the requirement of a tolerance on all food requirement of a tolerance. commodities when used in accordance with good agricultural practices. (a) The biochemical pesticide kaolin is temporarily exempted from the re- [66 FR 33198, June 21, 2001] quirement of a tolerance for residues of § 180.1188 Gamma aminobutyric acid; the insecticide Kaolin, when used on exemption from the requirement of crops (apples, apricots, bananas, beans, a tolerance. cane berries, citrus fruits, corn, cotton, Gamma aminobutyric acid is exempt cranberries, cucurbits, grapes, melons, from the requirement of a tolerance on nuts, ornamentals, peaches, peanuts, all food commodities when used in ac- pears, peppers, plums, potatoes, seed cordance with good agricultural prac- crops, small grains, soybeans, straw- tices. berries, sugar beets, and tomatoes) to control certain insect, fungus, and bac- [66 FR 33198, June 21, 2001] terial damage to plants. This tem- § 180.1189 Methyl salicylate; exemption porary exemption from the require- from the requirement of a toler- ment of a tolerance will permit the ance. marketing of the food commodities in The biochemical pesticide methyl sa- this paragraph when treated in accord- licylate is exempt from the require- ance with the provisions of experi- ment of a tolerance for residues in or mental use permit 70060–EUP–1, which on food or feed when used as an insect is being issued under the Federal Insec- repellant in food packaging and animal ticide, Fungicide, and Rodenticide Act feed packaging at an application rate (FIFRA), as amended (7 U.S.C. 136). that does not exceed 0.2 mg of methyl This temporary exemption from the re- salicylate per square inch of packaging quirement of a tolerance expires and is materials. revoked December 31, 1999. This tem- [62 FR 61639, Nov. 19, 1997] porary exemption from the requirement of a tolerance may be revoked at § 180.1191 Ferric phosphate; exemp- any time if the experimental use per- tion from the requirement of a tol- mit is revoked or if any experience erance. with or scientific data on this pesticide An exemption from the requirement indicate that the tolerance is not safe. of a tolerance is established for resi- (b) Kaolin is exempted from the re- dues of the biochemical pesticide, fer- quirement of a tolerance for residues ric phosphate (FePO4, CAS No. 11045– when used on or in food commodities to 86–0) in or on all food commodities. aid in the control of insects, fungi, and [62 FR 56105, Oct. 29, 1997] bacteria (food/feed use). § 180.1193 Potassium dihydrogen phos- [62 FR 19685, Apr. 23, 1997, as amended at 63 phate; exemption from the require- FR 9430, Feb. 25, 1998] ment of a tolerance. § 180.1181 Bacillus cereus strain BPO1; Potassium dihydrogen phosphate is exemption from the requirement of exempted from the requirement of a a tolerance. tolerance in or on all food commodities when applied as a fungicide in accord- An exemption from the requirement ance with good agricultural practices. of a tolerance for residues of the Bacil- lus cereus strain BPO1 in or on all raw [63 FR 43085, Aug. 12, 1998] agricultural commodities when ap- § 180.1195 Titanium dioxide. plied/used in accordance with label directions. Titanium dioxide (CAS Reg. No. 13463–67–7) is exempted from the re- [67 FR 70017, Nov. 20, 2002] quirement of a tolerance for residues in

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or on growing crops, when used as an dues of hydrogen peroxide in or on all inert ingredient (UV protectant) in food commodities at the rate of ≤1% microencapsulated formulations of the hydrogen peroxide per application on insecticide lambda cyhalothrin at no growing and postharvest crops. more than 3.0% by weight of the formu- [67 FR 41844, June 20, 2002] lation and as an inert ingredient (UV- stabilizer) at no more than 5% in pes- § 180.1198 Gliocladium catenulatum ticide formulations containing the ac- strain J1446; exemption from the tive ingredient napropamide. requirement of a tolerance. [77 FR 44155, July 27, 2012] An exemption from the requirement of a tolerance is established for resi- § 180.1196 Peroxyacetic acid; exemp- dues of the microbial pesticide, tion from the requirement of a tol- Gliocladium catenulatum strain J1446 erance. when used in or on all food commod- (a) An exemption from the require- ities. ment of a tolerance is established for residues of peroxyacetic acid in or on [63 FR 37288, July 10, 1998] all food commodities, when such resi- § 180.1199 dues result from the use of peroxy- Lysophosphatidylethanolamine acetic acid as an antimicrobial treat- (LPE); exemption from the requirement in solutions containing a diluted ment of a tolerance. end use concentration of peroxyacetic acid up to 100 ppm per application on An exemption from the requirement fruits, vegetables, tree nuts, cereal of a tolerance is established for resi- grains, herbs, and spices. dues of the biochemical pesticide (b) An exemption from the require- lysophosphatidylethanolamine in or on ment of a tolerance is established for all food commodities. residues of peroxyacetic acid, in or on [67 FR 17636, Apr. 11, 2002] all food commodities when used in sanitizing solutions containing a di- § 180.1200 Pseudomonas fluorescens luted end-use concentration of peroxy- strain PRA–25; temporary exemp- acetic acid up to 500 ppm, and applied tion from the requirement of a tol- to tableware, utensils, dishes, pipe- erance. lines, tanks, vats, fillers, evaporators, A temporary exemption from the re- pasteurizers, aseptic equipment, milk- quirement of a tolerance is established ing equipment, and other food proc- for residues of the microbial pesticide, essing equipment in food handling es- pseudomonas fluorescens strain PRA–25 tablishments including, but not limited when used on peas, snap beans and to dairies, dairy barns, restaurants, sweet corn and will expire July 31, 2001. food service operations, breweries, [63 FR 38498, July 17, 1998] wineries, and beverage and food processing plants. § 180.1201 Trichoderma harzianum (c) An exemption from the require- strain T-39; exemption from the re- ment of a tolerance is established for quirement of a tolerance. residues of the biochemical pesticide Trichoderma harzianum strain T-39 is peroxyacetic acid and its metabolites exempt from the requirement of a tol- and degradates, including hydrogen erance on all food commodities. peroxide and acetic acid, in or on all food commodities, when used in ac- [65 FR 38757, June 22, 2000] cordance with good agricultural practices. § 180.1202 Bacillus sphaericus; exemption from the requirement of a tol- [74 FR 26535, June 3, 2009, as amended at 76 erance. FR 11969, Mar. 4, 2011] An exemption from the requirement § 180.1197 Hydrogen peroxide; exemp- of a tolerance is established for resi- tion from the requirement of a tol- dues of the microbial pesticides, Bacil- erance. lus sphaericus when used in or on all food crops. An exemption from the requirement of a tolerance is established for resi- [63 FR 48597, Sept. 11, 1998]

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§ 180.1204 Harpin protein; exemption § 180.1206 Aspergillus flavus AF36; ex- from the requirement of a toler- emption from the requirement of a ance. tolerance. An exemption from the requirement (a) An exemption from the require- of a tolerance is established for resi- ment of a tolerance is established for dues of individual harpin proteins that residues of the microbial pesticide As- meet specified physiochemical and tox- pergillus flavus AF36 in or on cotton, icological criteria when used as bio- gin byproducts; cotton, hulls; cotton, chemical pesticides on all food com- meal; cotton, refined oil; cotton, modities to enhance plant growth, undelinted seed. quality and yield, to improve overall (b) An exemption from the require- plant health, and to aid in pest man- ment of a tolerance is established for agement. The physiochemical and toxi- residues of Aspergillus flavus AF36 in or cological criteria identifying harpin on pistachio when applied as an proteins are as follows: antifungal agent and used in accord- (a) Consists of a protein less than 100 ance with good agricultural practices. kD in size, that is acidic (pI<7.0), gly- (c) An exemption from the require- cine rich (>10%), and contains no more ment of a tolerance is established for than one cystine residue. residues of Aspergillus flavus AF36 in or (b) The source(s) of genetic material on corn, field, forage; corn, field, grain; encoding the protein are bacterial corn, field, stover; corn, field, aspirated plant pathogens not known to be mam- grain fractions; corn, sweet, kernel malian pathogens. plus cob with husk removed; corn, (c) Elicits the hypersensitive re- sweet, forage; corn, sweet, stover; corn, sponse (HR) which is characterized as pop, grain; and corn, pop, stover, when rapid, localized cell death in plant tis- applied/used as an antifungal agent. sue after infiltration of harpin into the [68 FR 41541, July 14, 2003, as amended at 72 intercellular spaces of plant leaves. FR 28871, May 23, 2007; 72 FR 72965, Dec. 26, (d) Possesses a common secondary 2007; 74 FR 26535, 26546, June 3, 2009; 76 FR structure consisting of a and b units 16301, Mar. 23, 2011; 77 FR 14291, Mar. 9, 2012] that form an HR domain. (e) Is heat stable (retains HR activity § 180.1207 N-acyl sarcosines and so- when heated to 65 °C for 20 minutes). dium N-acyl sarcosinates; exemp- (f) Is readily degraded by a proteinase tion from the requirement of a tolerance. representative of environmental conditions (no protein fragments >3.5 kD An exemption from the requirement after 15 minutes degradation with of a tolerance is established for resi- Subtilisin A). dues of the following substances when (g) Exhibits a rat acute oral toxicity used as inert ingredients (surfactants) at levels not to exceed 10% in pesticide (LD50) of greater than 5,000 mg product/ kg body weight. formulations containing glyphosate: [69 FR 24996, May 5, 2004] CAS Reg. Name No.

§ 180.1205 Beauveria bassiana ATCC N-acyl sarcosines. #74040; exemption from the require- N-cocoyl sarcosine mixture ...... 68411-97-2 ments of a tolerance. N-lauroyl sarcosine ...... 97-78-9 An exemption from the requirement N-myristoyl sarcosine ...... 52558-73-3 N-oleoyl sarcosine ...... 110-25-8 of a tolerance is established for resi- N-stearoyl sarcosine ...... 142-48-3 dues of the insecticide Beauveria Sodium N-acyl sarcosinates. bassiana (ATCC #74040) in or on all food N-cocoyl sarcosine sodium salt mixture ...... 61791-59-1 commodities when applied or used as N-methyl-N-(1-oxo-9-octodecenyl) glycine .... 3624-77-9 ground and aerial foliar sprays for use N-methyl-N-(1-oxododecyl) glycine ...... 137-16-6 N-methyl-N-(1-oxooctadecyl) glycine ...... 5136-55-0 only on terrestrial crops. N-methyl-N-(1-oxotetradecyl glycine ...... 30364-51-3 [64 FR 22796, Apr. 28, 1999] [64 FR 68046, Dec. 6, 1999]

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§ 180.1209 Bacillus subtilis strain QST § 180.1219 Foramsulfuron; exemption 713 and strain QST 713 variant soil; from the requirement of a toler- exemption from the requirement of ance. a tolerance. The pesticide foramsulfuron is ex- An exemption from the requirement empted from the requirement of a tol- of a tolerance is established for resi- erance in corn, field, grain/corn, field, dues of the microbial pesticides Bacil- forage/ corn, field, stover/corn, pop, lus subtilis strain QST 713 and strain grain/corn, pop, forage/corn, pop, sto- QST 713 variant soil when used in or on ver; corn, sweet, forage; corn, sweet, all food commodities. kernel plus cob with husks removed; corn, sweet, stover when applied as a [77 FR 73937, Dec. 12, 2012] herbicide in accordance with good agri- § 180.1210 Phosphorous acid; exemp- cultural practices. tion from the requirement of a tol- [74 FR 26535, June 3, 2009] erance. An exemption from the requirement § 180.1220 1-Methylcyclopropene; ex- of a tolerance is established for resi- emption from the requirement of a tolerance. dues of phosphorous acid and its ammonium, sodium, and potassium salts An exemption from the requirement in or on all food commodities when of a tolerance is established for resi- used as an agricultural fungicide and in dues of the 1-Methylcyclopropene in or or on potatoes when applied as a post- on fruits and vegetables when: harvest treatment at 35,600 ppm or less (a) Used as a post harvest plant phosphorous acid. growth regulator, i.e., for the purpose of inhibiting the effects of ethylene. [71 FR 49373, Aug. 23, 2006] (b) Applied or used outdoors for preharvest treatments. § 180.1212 Pseudomonas chlororaphis Strain 63–28; exemption from the [73 FR 19150, Apr. 9, 2008] requirement of a tolerance. § 180.1221 Pseudozyma flocculosa An exemption from the requirement strain PF-A22 UL; exemption from of a tolerance is established for resi- the requirement of a tolerance. dues of the microbial pesticide An exemption from the requirement Pseudomonas chlororaphis Strain 63–28 of a tolerance is established for resi- in or on all food commodities. dues of Pseudozyma flocculosa strain [66 FR 53346, Oct. 22, 2001] PF-A22 UL in or on all food commodities. § 180.1213 Coniothyrium minitans strain CON/M/91–08; exemption [67 FR 60966, Sept. 27, 2002] from the requirement of a tolerance. § 180.1222 Sucrose octanoate esters; exemption from the requirement of An exemption from the requirement a tolerance. of a tolerance is established for resi- An exemption from the requirement dues of the microbial pesticide of a tolerance is established for resi- Coniothyrium minitans strain CON/M/91– dues of sucrose octanoate esters [(a-D- 08 when used in or on all food commod- glucopyranosyl-b-D-fructofuranosyl-oc- ities. tanoate), mono-, di-, and triesters of [66 FR 16874, Mar. 28, 2001] sucrose octanoate] in or on all food commodities when used in accordance § 180.1218 Indian Meal Moth with good agricultural practices. Granulosis Virus; exemption from the requirement of a tolerance. [67 FR 60152, Sept. 25, 2002] An exemption from the requirement § 180.1223 Imazamox; exemption from of a tolerance is established for resi- the requirement of a tolerance. dues of the microbial pesticide Indian The herbicide imazamox, (±) 2, -[4,5- Meal Moth Granulosis Virus when used dihydro-4-methyl-4-(1-methylethyl)-5- in or on all food commodities. oxo-1H-imidazol-2-yl]-5- [68 FR 55875, Sept. 29, 2003] (methoxymethyl)-3-pyridinecarboxylic

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acid, is exempt from the requirement § 180.1228 Diallyl sulfides; exemption of a tolerance on all food commodities from the requirement of a toler- when applied as a herbicide in accordance. ance with good agricultural practices. An exemption from the requirement [68 FR 7433, Feb. 14, 2003] of a tolerance is established for residues of diallyl sulfides when used in/on § 180.1224 Bacillus pumilus GB34; ex- garlic, leeks, onions, and shallots. emption from the requirement of a [68 FR 40808, July 9, 2003] tolerance. An exemption from the requirement § 180.1230 Ferrous sulfate; exemption of a tolerance is established for resi- from the requirement of a toler- dues of the microbial pesticide Bacillus ance. pumilus GB34 when used as a seed treat- An exemption from the requirement ment in or on all food commodities. An of a tolerance is established for resi- exemption is also granted for such residues of ferrous sulfate. dues on treated but unplanted soybean [70 FR 33363, June 8, 2005] seeds. [69 FR 76625, Dec. 22, 2004] § 180.1231 Lime; exemption from the requirement of a tolerance. § 180.1225 Decanoic acid; exemption An exemption from the requirement from the requirement of a toler- of a tolerance is established for resi- ance. dues of lime. An exemption from the requirement [70 FR 33363, June 8, 2005] of a tolerance is established for residues of decanoic acid in or on all raw § 180.1232 Lime-sulfur; exemption from agricultural commodities and in proc- the requirement of a tolerance. essed commodities, when such residues An exemption from the requirement result from the use of decanoic acid as of a tolerance is established for resi- an antimicrobial treatment in solu- dues of lime-sulfur. tions containing a diluted end-use concentration of decanoic acid (up to 170 [70 FR 33363, June 8, 2005] ppm per application) on food contact surfaces such as equipment, pipelines, § 180.1233 Potassium sorbate; exemp- tanks, vats, fillers, evaporators, tion from the requirement of a tolerance. pasteurizers and aseptic equipment in restaurants, food service operations, An exemption from the requirement dairies, breweries, wineries, beverage of a tolerance is established for resi- and food processing plants. dues of potassium sorbate. [68 FR 7939, Feb. 19, 2003; 68 FR 17308, Apr. 9, [70 FR 33363, June 8, 2005] 2003] § 180.1234 Sodium carbonate; exemp- § 180.1226 Bacillus pumilus strain tion from the requirement of a tol- QST2808; temporary exemption erance. from the requirement of a toler- An exemption from the requirement ance. of a tolerance is established for resi- A temporary exemption from the re- dues of sodium carbonate. quirement of a tolerance is established [70 FR 33363, June 8, 2005] for residues of the microbial pesticide Bacillus pumilus strain QST2808 when § 180.1235 Sodium hypochlorite; ex- used in or on all agricultural commod- emption from the requirement of a ities when applied/used in accordance tolerance. with label directions. An exemption from the requirement [68 FR 36480, June 18, 2003] of a tolerance is established for residues of sodium hypochlorite. [70 FR 33363, June 8, 2005]

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§ 180.1236 Sulfur; exemption from the § 180.1241 Eucalyptus oil; exemption requirement of a tolerance. from the requirement of a tolerance. An exemption from the requirement of a tolerance is established for resi- Time-limited exemptions from the dues of sulfur. requirement of a tolerance are established for residues of eucalyptus oil on [70 FR 33363, June 8, 2005] honey and honeycomb in connection with use of the pesticide under section § 180.1237 Sodium metasilicate; exemp- 18 emergency exemptions granted by tion from the requirement of a tol- the EPA. These time-limited exemp- erance. tions from the requirement of a toler- (a) An exemption from the require- ance for residues of eucalyptus oil will ment of a tolerance is established for expire and are revoked on June 30, 2007. residues of sodium metasilicate in or [70 FR 37696, June 30, 2005] on all food commodities when used in accordance with approved label rates § 180.1243 Bacillus subtilis var. and good agricultural practices as a amyloliquefaciens strain FZB24; ex- plant desiccant, so long as the sodium emption from the requirement of a tolerance. metasilicate does not exceed 4% by weight in aqueous solution. An exemption from the requirement (b) An exemption from the require- of a tolerance for residues of the Bacil- ment of a tolerance is established for lus subtilis var. amyloliquefaciens strain FZB24 in or on all agricultural com- residues of sodium metasilicate in or modities when applied/used in accord- on all food commodities when used in ance with label directions. accordance with approved label rates and good agricultural practices as an [68 FR 44640, July 30, 2003] insecticide and fungicide, so long as § 180.1244 Ammonium bicarbonate; ex- the sodium metasilicate does not exemption from the requirement of a ceed 2.41% by weight in aqueous solu- tolerance. tion. An exemption from the requirement [71 FR 19441, Apr. 14, 2006] of tolerance is established for residues of ammonium bicarbonate used in or § 180.1240 Thymol; exemption from the on all food commodities when used in requirement of a tolerance. accordance with good agricultural (a) Time-limited exemptions from practices. the requirement of a tolerance are es- [69 FR 13745, Mar. 24, 2004] tablished for residues of thymol on honey and honeycomb in connection § 180.1245 Rhamnolipid biosurfactant; with use of the pesticide under section exemption from the requirement of a tolerance. 18 emergency exemptions granted by the EPA. These time-limited exemp- An exemption from the requirement tions from the requirement of a toler- of a tolerance is established for resi- ance for residues of thymol will expire dues of rhamnolipid biosurfactant and are revoked on June 30, 2007. when used in accordance with good agricultural practices as a fungicide in or (b) An exemption from the require- on all food commodities. ment of a tolerance for residues of the thymol (as present in thyme oil) in or [69 FR 16800, Mar. 31, 2004] on food commodities when applied/used in/on public eating places, dairy proc- § 180.1246 Yeast Extract Hydrolysate from Saccharomyces cerevisiae: ex- essing equipment, and/or food proc- emption from the requirement of a essing equipment and utensils. tolerance. [70 FR 37696, June 30, 2005, as amended at 71 This regulation establishes an ex- FR 2895, Jan. 18, 2006; 74 FR 12617, Mar. 25, emption from the requirement of a tol- 2009] erance for residues of the biochemical pesticide Yeast Extract Hydrolysate from Saccharomyces cerevisiae on all

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food commodities when applied/used 21882 on peanut; peanut, hay; peanut, for the management of plant diseases. meal; and peanut, refined oil. (b) An exemption from the require- [69 FR 9958, Mar. 3, 2004] ment of a tolerance is established for § 180.1248 Exemption of citronellol residues of Aspergillus flavus NRRL from the requirement of a toler- 21882 on corn, field, forage; corn, field, ance. grain; corn, field, stover; corn, field, as- An exemption from the requirement pirated grain fractions; corn, sweet, of a tolerance is established for resi- kernel plus cob with husk removed; dues of the biochemical pesticide corn, sweet, forage; corn, sweet, stover; citronellol in or on all food commod- corn, pop, grain; and corn, pop, stover. ities. [75 FR 6576, Feb. 10, 2010] [69 FR 23146, Apr. 28, 2004] § 180.1255 Bacillus pumilus strain QST § 180.1250 C8, C10, and C12 fatty acid 2808; exemption from the require- monoesters of glycerol and pro- ment of a tolerance. pylene glycol; exemption from the An exemption from the requirement requirement of a tolerance. of a tolerance is established for resi- The C8, C10, and C12 straight-chain dues of the microbial pesticide Bacillus fatty acid monoesters of glycerol (glyc- pumilus strain QST 2808 when used in or erol monocaprylate, glycerol on all agricultural commodities when monocaprate, and glycerol applied/used in accordance with label monolaurate) and propylene glycol directions. (propylene glycol monocaprylate, pro- [69 FR 63954, Nov. 3, 2004] pylene glycol monocaprate, and propylene glycol monolaurate) are exempt § 180.1256 Alternaria destruens strain from the requirement of a tolerance in 059; exemption from the require- or on all food commodities when used ment of a tolerance. in accordance with approved label rates An exemption from the requirement and good agricultural practice. of a tolerance is established for resi- [69 FR 34944, June 23, 2004] dues of the microbial pesticide Alternaria destruens Strain 059 when § 180.1251 Geraniol; exemption from used in or on all raw agricultural com- the requirement of a tolerance. modities when applied/used in accord- An exemption from the requirement ance with label directions. of a tolerance is established for resi- [70 FR 28459, May 18, 2005] dues of the biochemical pesticide geraniol in or on all food commodities. § 180.1257 Paecilomyces lilacinus strain 251; exemption from the re- [69 FR 23151, Apr. 28, 2004] quirement of a tolerance. § 180.1253 Streptomyces lydicus WYEC An exemption from the requirement 108; exemption from the require- of a tolerance is established for resi- ment of a tolerance. dues of the microbial pesticide An exemption from the requirement Paecilomyces lilacinus strain 251 when of a tolerance is established for resi- used in or on all agricultural commod- dues of the microbial pesticide ities when applied/used in accordance Streptomyces lydicus WYEC 108 when with label directions. used in or on all agricultural commod- [70 FR 19283, Apr. 13, 2005] ities when applied/used in accordance with label directions. § 180.1258 Acetic acid; exemption from the requirement of a tolerance. [69 FR 31301, June 3, 2004] (a) An exemption from the require- § 180.1254 Aspergillus flavus NRRL ment of a tolerance is established for 21882; exemption from the require- residues of the biochemical pesticide ment of a tolerance. acetic acid when used as a preservative (a) An exemption from the require- on post-harvest agricultural commod- ment of a tolerance is established for ities intended for animal feed, includ- residues of Aspergillus flavus NRRL ing Alfalfa, seed; alfalfa, hay; barley,

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grain; bermudagrass, hay; bluegrass, § 180.1262 Sorbitol octanoate; exemp- hay; bromegrass, hay; clover, hay; tion from the requirement of a tol- corn, field, grain; corn, pop, grain; erance. cowpea, hay; fescue, hay; lespedeza, An exemption from the requirement hay; lupin; oat, grain; orchardgrass, of a tolerance is established for resi- hay; peanut, hay; timothy, hay; vetch, dues of sorbitol octanoate in or on all hay; and wheat, grain, or commodities food commodities when used in accord- described as grain or hay. ance with label directions. (b) An exemption from the requirement of a tolerance is established for [71 FR 4518, Jan. 27, 2006] residues of acetic acid in or on all food § 180.1263 Tetrahydrofurfuryl alcohol; crops resulting from unintentional exemption from the requirement of spray and drift to non-target vegeta- a tolerance. tion including non-food, food and feed crops when used as a non-selective con- Tetrahydrofurfuryl alcohol (THFA, tact herbicide spray. CAS Reg. No. 97–99–4) is exempt from the requirement of a tolerance in or on [75 FR 40741, July 14, 2010] all raw agricultural commodities when used in accordance with good agricul- § 180.1259 Reynoutria sachalinensis ex- tural practices as an inert ingredient tract; exemption from the require- applied only: ment of a tolerance. (a) For use as a seed treatment. Residues of the biochemical pesticide (b) For applications prior to planting Reynoutria sachalinensis extract, when and at the time of planting. derived from the whole plant extract, (c) For use on cotton. are exempt from the requirement of a (d) For use in herbicides with one ap- tolerance in or on all food commod- plication to wheat and barley prior to ities. the pre-boot stage, and two applica- [70 FR 55277, Sept. 21, 2005] tions to canola and soybeans pre- bloom. § 180.1260 Muscodor albus QST 20799 (e) For use in herbicides with two ap- and the volatiles produced on re- plications to field corn up to 24 inches hydration; exemption from the re- tall (V 5 stage). quirement of a tolerance. An exemption from the requirement [71 FR 45415, Aug. 9, 2006] of a tolerance is established on all food/ § 180.1267 Pantoea agglomerans strain feed commodities, for residues of C9–1; exemption from the require- Muscodor albus QST 20799, and the ment of a tolerance. volatiles produced on its rehydration, An exemption from the requirement when the pesticide is used for all agri- of a tolerance is established for resi- cultural applications, including seed, dues of Pantoea agglomerans strain C9–1 propagule and post harvest treatments. when used on apples and pears. [70 FR 56576, Sept. 28, 2005] [71 FR 24596, Apr. 26, 2006] § 180.1261 Xanthomonas campestris pv. vesicatoria and Pseudomonas § 180.1268 Potassium silicate; exemp- syringae pv. tomato specific tion from the requirement of a tol- Bacteriophages. erance. An exemption from the requirement Potassium silicate is exempt from of a tolerance is established for resi- the requirement of a tolerance in or on dues of Xanthomonas campestris pv. all food commodities so long as the po- vesicatoria and Pseudomonas syringae pv. tassium silicate is not applied at rates tomato specific bacteriophages in or on exceeding 1% by weight in aqueous so- pepper and tomato. lution and when used in accordance with good agricultural practices. [74 FR 26536, June 3, 2009] [71 FR 34272, June 14, 2006]

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§ 180.1269 Bacillus mycoides isolate J; § 180.1274 Tris (2-ethylhexyl) phos- exemption from the requirement of phate; exemption from the require- a tolerance. ment of a tolerance. Bacillus mycoides isolate J is tempo- Tris (2-ethylhexyl) phosphate (TEHP, rarily exempt from the requirement of CAS Reg. No. 78–42–2) is exempt from a tolerance when used as a fungicide on the requirement of a tolerance for resi- potatoes in accordance with a valid dues in grain, aspirated fractions; bar- Federal Insecticide, Fungicide, and ley, grain, barley, hay, barley, straw; Rodenticide Act (FIFRA) section 18 wheat, grain; wheat, forage; wheat, emergency exemption. This temporary hay; wheat, straw when used under the exemption from the requirement of a following conditions: tolerance expires and is revoked on De- cember 31, 2015. (a) The use is in accordance with good agricultural practices; [78 FR 24353, Apr. 25, 2013] (b) Tris (2-ethylhexyl) phosphate is used as an inert ingredient in pesticide § 180.1270 Isophorone; exemption from the requirement of a tolerance. formulations with the active ingredients pinoxaden, clodinafop-propargyl, Isophorone (CAS Reg. No. 78–59–1) is and tralkoxydium; exempt from the requirement of a tolerance when used as an inert ingre- (c) Tris (2-ethylhexyl) phosphate is dient in pesticide formulations applied applied no more than twice per season; to beets, ginseng, rice, spinach, sugar and beets, and Swiss chard. (d) The applications occur no later than the pre-boot stage (prior to for- [71 FR 45408, Aug. 9, 2006] mation of edible grain). § 180.1271 Eucalyptus oil; exemption [72 FR 5624, Feb. 7, 2007, as amended at 74 FR from the requirement of a toler- 26536, June 3, 2009] ance. An exemption from the requirement § 180.1275 Pythium; exception from the of tolerance is established for residues requirement of a tolerance. of eucalyptus oil in or on honey, hon- An exemption from the requirement eycomb, and honeycomb with honey of tolerance is established on all food/ when used at 2g or less eucalyptus oil feed commodities, for residues of per hive, where the eucalyptus oil con- pythium oligandrum DV 74 when the pes- tains 80% or more eucalyptol. ticide is used on food crops. [71 FR 53979, Sept. 13, 2006] [72 FR 27452, May 16, 2007] § 180.1272 Pantoea agglomerans strain E325; exemption from the require- § 180.1276 Tobacco mild green mosaic ment of a tolerance. tobamovirus (TMGMV); temporary exemption from the requirement of An exemption from the requirement a tolerance. of a tolerance is established for residues of Pantoea agglomerans strain E325 A temporary exemption from the re- when used on apples and pears. quirement of a tolerance is established for residues of tobacco mild green mo- [71 FR 54933, Sept. 20, 2006] saic tobamovirus in or on all grass, for- § 180.1273 Beauveria bassiana HF23; age and grass, hay. exemption from the requirement of [74 FR 26536, June 3, 2009] a tolerance. Residues of Beauveria bassiana HF23 § 180.1277 Dibasic esters; exemption are exempt from the requirement of a from the requirement of a toler- tolerance on all food/feed commodities, ance. when the pesticide is used for the Dibasic esters (CAS Reg. No. 95481–62– treatment of chicken and livestock fa- 2) is exempted from the requirement of cilities, including the treatment of a tolerance for residues when used as chicken and livestock manure. an inert ingredient (solvent and/or [75 FR 10190, Mar. 5, 2010] anti-freeze) at 10% W/W or less in

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microencapsulated pesticide formula- § 180.1282 Bacillus firmus I-1582; ex- tions with the active ingredient emption from the requirement of a cyfluthrin. tolerance. An exemption from the requirement [73 FR 10398, Feb. 27, 2008] of a tolerance is established in/on all § 180.1278 Quillaja saponaria extract food/feed commodities, for residues of (saponins); exemption from the re- Bacillus firmus I-1582 when used as a soil quirement of a tolerance. application or seed treatment. Residues of the biochemical pesticide [73 FR 25528, May 7, 2008] Quillaja saponaria extract (saponins) are exempt from the requirement of a § 180.1283 (Z)-7,8-epoxy-2- methyloctadecane (Disparlure); ex- tolerance in or on all food commod- emption from the requirement of a ities. tolerance. [72 FR 41935, Aug. 1, 2007] An exemption from the requirement of a tolerance is established for resi- § 180.1279 Zucchini yellow mosaic dues of (Z)-7,8-epoxy-2- virus—weak strain; exemption from methyloctadecane on all food and feed the requirement of a tolerance. crops that occur when it is used to An exemption from the requirement treat trees, shrubs, and pastures and of a tolerance for residues of the such use results in unintentional spray ZYMV–WK strain in or on all raw and drift to non-target vegetation in- cucurbit when applied/used in accord- cluding non-food, food, and feed crops. This active ingredient is also known as ance with label directions. Disparlure. [74 FR 26536, June 3, 2009] [73 FR 33714, June 13, 2008]

§ 180.1280 § 180.1284 Ammonium salts of higher Poly(hexamethylenebiguanide) hy- fatty acids (C8-C18 saturated; C8-C12 drochloride (PHMB); exemption unsaturated); exemption from the from the requirement of a toler- requirement of a tolerance. ance. Ammonium salts of C8-C18 saturated Poly(hexamethylenebiguanide) hy- and C8-C12 unsaturated higher fatty drochloride (PHMB)(CAS Reg. No. acids are exempted from the require- 32289–58–0) is exempt from the requirement of a tolerance for residues in or ment of a tolerance for residues of the on all food commodities when used in antimicrobial in or on all food com- accordance with good agricultural modities when the residues are the re- practice. sult of the lawful application of a food [74 FR 47457, Sept. 16, 2009] contact surface sanitizer containing PHMB at 550 parts per million (ppm). § 180.1285 Polyoxin D zinc salt; exemption from the requirement of a tol- [73 FR 1517, Jan. 9, 2008] erance. § 180.1281 S-Abscisic Acid, (S)-5-(1-hy- An exemption from the requirement droxy-2,6,6-trimethyl-4-oxo-1- of a tolerance is established for the res- cyclohex-2-enyl)-3-methyl-penta- idues of polyoxin D zinc salt in or on (2Z,4E)-dienoic Acid; exemption all food commodities when applied as a from the requirement of a toler- fungicide and used in accordance with ance. good agricultural practices. An exemption from the requirement [77 FR 56133, Sept. 12, 2012] of a tolerance is established for residues of S-Abscisic Acid in or on all food § 180.1287 Extract of Chenopodium commodities when applied or used ambrosioides near ambrosioides; exemption from the requirement of a preharvest as a plant regulator. tolerance. [75 FR 11744, Mar. 12, 2010] An exemption from the requirement of a tolerance is established for the residues of Extract of Chenopodium

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ambrosioides near ambrosioides when § 180.1292 Ulocladium oudemansii (U3 used as an insecticide/acaricide on all Strain); exemption from the re- food commodities. quirement of a tolerance. [74 FR 634, Jan. 7, 2009] An exemption from the requirement of a tolerance is established in/on all § 180.1288 Tristyrylphenol ethoxylates; food commodities for residues of exemption from the requirement of Ulocladium oudemansii (U3 Strain), a tolerance. when applied or used pre-harvest-only, An exemption from the requirement excluding applications made post-har- of a tolerance is established for resi- vest or to processed commodities, as a dues of poly(oxy-1,2-ethanediyl), a- microbial fungicide in accordance with [2,4,6-tris(1-phenylethyl)phenyl]-w-hy- good agricultural practices. droxy-, (CAS Reg. No. 70559–25–0) and [74 FR 55458, Oct. 28, 2009] poly(oxy-1,2-ethanediyl), a-[tris(1- phenylethyl)phenyl]-w-hydroxy-, (CAS § 180.1293 Trichoderma gamsii strain Reg. No. 99734–09–5) on citrus crops, ICC 080; exemption from the re- group 10, when used as inert ingredi- quirement of a tolerance. ents under the following conditions: Trichoderma gamsii strain ICC 080 is (a) They are applied post-harvest; exempted from the requirement of a (b) They are used as inert ingredients tolerance in or on all food and feed in pesticide formulations with commodities when applied preharvest azoxystrobin and fludioxonil; and and used in accordance with good agri- (c) They constitute no more than cultural practices. 10.0% of the formulated pesticide prod- [75 FR 8507, Feb. 25, 2010] uct. [74 FR 12625, Mar. 25, 2009] § 180.1294 Trichoderma asperellum strain ICC 012; exemption from the § 180.1289 Candida oleophila Strain O; requirement of a tolerance. exemption from the requirement of Trichoderma asperellum strain ICC 012 a tolerance. is exempted from the requirement of a An exemption from the requirement tolerance in or on all food and feed of a tolerance is established for the res- commodities when applied pre-harvest idues of the microbial pesticide, and used in accordance with good agri- Candida oleophila Strain O, on apples cultural practices. and pears when applied/used as a post- [75 FR 9530, Mar. 3, 2010] harvest biofungicide. [74 FR 22464, May 13, 2009] § 180.1295 Laminarin; exemption from the requirement of a tolerance. § 180.1290 Pasteuria usgae; exemption An exemption from the requirement from the requirement of a toler- of a tolerance is established for resi- ance. dues of laminarin in or on all food com- An exemption from the requirement modities when laminarin is applied of a tolerance is established for resi- preharvest. dues of Pasteuria usgae in or on all food [75 FR 8256, Feb. 24, 2010] commodities when applied preharvest and used as a nematicide in accordance § 180.1296 Terpene Constituents α-ter- with good agricultural practices. pinene, d-limonene and p-cymene, of the Extract of Chenopodium [75 FR 37737, June 30, 2010] ambrosioides near ambrosioides as Synthetically Manufactured; exemp- § 180.1291 Cold pressed neem oil; ex- tion from the requirement of a tol- emption from the requirement of a erance. tolerance. An exemption from the requirement Residues of the biochemical pesticide of a tolerance is established for the res- cold pressed neem oil are exempt from idues of the biochemical pesticide Ter- the requirement of a tolerance in or on pene Constituents a-terpinene, d-limo- all food commodities. nene and p-cymene, of the Extract of [74 FR 55463, Oct. 28, 2009] Chenopodium ambrosioides near

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ambrosioides as Synthetically Manufac- O157:H7, sequence negative for shiga tured when used as an insecticide/acar- toxins I and II, and grown on icide in or on all food commodities. atoxigenic host bacteria when used/ap- [75 FR 39455, July 9, 2010] plied on food contact surfaces in food processing plants in accordance with § 180.1297 Homobrassinolide; exemp- the terms of Experimental Use Permit tion from the requirement of a tol- (EUP) No. 74234–EUP–2. This temporary erance. exemption expires on April 1, 2013. An exemption from the requirement [76 FR 20546, Apr. 13, 2011] of a tolerance is established for the residues of homobrassinolide in or on all § 180.1302 Sodium Ferric Ethylene- food commodities when applied/used as diaminetetraacetate (EDTA); ex- a plant growth regulator in accordance emption from the requirement of a with good agricultural practices. tolerance. [75 FR 39459, July 9, 2010] An exemption from the requirement of a tolerance is established for resi- § 180.1298 Trichoderma hamatum iso- dues of sodium ferric EDTA in or on all late 382; exemption from the re- food commodities when applied as a quirement of a tolerance. molluscicide and used in accordance An exemption from the requirement with good agricultural practices. of a tolerance is established for residues of Trichoderma hamatum isolate 382 [76 FR 17561, Mar. 30, 2011] in or on all food commodities when applied as a fungicide and used in accord- § 180.1303 Metarhizium anisopliae ance with good agricultural practices. strain F52; exemption from the requirement of a tolerance. [75 FR 43076, July 23, 2010] An exemption from the requirement § 180.1299 Prohydrojasmon; exemption of a tolerance is established for resi- from the requirement of a toler- dues of Metarhizium anisopliae strain ance. F52 in or on all food commodities when An exemption from the requirement applied as an insecticide, miticide, or of a tolerance is established for resi- ixodicide and used in accordance with dues of the biochemical pesticide good agricultural practices. prohydrojasmon (PDJ), propyl-3-oxo-2- [76 FR 26198, May 6, 2011] pentylcyclo-pentylacetate, when used as a plant growth regulator in or on § 180.1304 Pseudomonas fluorescens apple and grape pre-harvest, in accord- strain CL145A; exemption from the ance with label directions and good ag- requirement of a tolerance. ricultural practices. An exemption from the requirement [78 FR 75257, Dec. 11, 2013] of a tolerance is established for residues of Pseudomonas fluorescens strain § 180.1300 Potassium hypochlorite; ex- CL145A in or on all food commodities emption from the requirement of a when applied as a molluscicide. tolerance. An exemption from the requirement [76 FR 52875, Aug. 24, 2011] of a tolerance is established for residues of potassium hypochlorite in or on § 180.1305 Chromobacterium subtsugae strain PRAA4–1T; exemp- all commodities. tion from the requirement of a tol- [76 FR 11343, Mar. 2, 2011] erance. An exemption from the requirement § 180.1301 Escherichia coli O157:H7 of a tolerance is established for resi- specific bacteriophages; temporary exemption from the requirement of dues of Chromobacterium subtsugae a tolerance. strain PRAA4–1T in or on all food commodities when applied as an insecticide A temporary exemption from the re- or miticide and used in accordance quirement of a tolerance is established with good agricultural practices. for residues of lytic bacteriophages that are specific to Escherichia coli [76 FR 55272, Sept. 7, 2011]

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§ 180.1306 Isaria fumosorosea (for- § 180.1310 Trichoderma virens strain merly Paecilomyces fumosoroseus) G–41; exemption from the require- Apopka strain 97; exemption from ment of a tolerance. the requirement of a tolerance. An exemption from the requirement An exemption from the requirement of a tolerance is established for resi- of a tolerance is established for residues of Trichoderma virens strain G–41, dues of Isaria fumosorosea (formerly in or on all food commodities, when ap- Paecilomyces fumosoroseus) Apopka plied as a fungicide and used in accord- strain 97 in or on all food commodities ance with good agricultural practices. when applied as an insecticide or [77 FR 4908, Feb. 1, 2012] miticide and used in accordance with good agricultural practices. § 180.1311 Pasteuria nishizawae—Pn1; exemption from the requirement of [76 FR 59905, Sept. 28, 2011] a tolerance. § 180.1307 Bacteriophage of An exemption from the requirement Clavibacter michiganensis sub- of a tolerance is established for resi- species michiganensis; exemption dues of Pasteuria nishizawae—Pn1 in or from the requirement of a toler- on all food commodities when applied ance. as a nematicide and used in accordance An exemption from the requirement with good agricultural practices. of a tolerance is established for resi- [77 FR 8741, Feb. 15, 2012] dues of lytic bacteriophage of Clavibacter michiganensis subspecies § 180.1312 Aureobasidium pullulans michiganensis produced in Clavibacter strains DSM 14940 and DSM 14941; exemption from the requirement of michiganensis subspecies a tolerance. michiganensis in or on tomato when applied as a bactericide in accordance An exemption from the requirement with good agricultural practices. of a tolerance is established for residues of the microbial pesticides, [76 FR 66192, Oct. 26, 2011] Aureobasidium pullulans strains DSM 14940 and DSM 14941 in or on all food § 180.1308 Bacillus amyloliquefaciens commodities when applied preharvest strain D747; exemption from the re- and used in accordance with good agri- quirement of a tolerance. cultural practices. An exemption from the requirement [77 FR 8736, Feb. 15, 2012] of a tolerance is established for residues of the microbial pesticide, Bacillus § 180.1313 Bacillus pumilus strain amyloliquefaciens strain D747 in or on GHA 180; exemption from the re- all food commodities when used in ac- quirement of a tolerance. cordance with good agricultural prac- An exemption from the requirement tices. of a tolerance is established for resi- [77 FR 749, Jan. 6, 2012. Redesignated at 77 dues of Bacillus pumilus strain GHA 180 FR 2911, Jan. 20, 2012] in or on all food commodities when used in accordance with good agricul- § 180.1309 Bacillus subtilis strain CX– tural practices. 9060; exemption from the require- [77 FR 19112, Mar. 30, 2012] ment of a tolerance. An exemption from the requirement § 180.1314 Killed, nonviable of a tolerance is established for resi- Streptomyces acidiscabies strain T dues of the microbial pesticide Bacillus RL–110 ; exemption from the requirement of a tolerance. subtilis strain CX–9060, in or on all food commodities, when applied or used in An exemption from the requirement accordance with good agricultural of a tolerance is established for resi- practices. dues of killed, nonviable Streptomyces acidiscabies strain RL–110T in or on all [77 FR 1637, Jan. 11, 2012] food commodities when applied as a pre- or post-emergent herbicide and

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used in accordance with good agricul- § 180.1319 Banda de Lupinus albus tural practices. doce (BLAD); exemption from the requirement of a tolerance. [77 FR 35295, June 13, 2012] An exemption from the requirement § 180.1315 Natamycin; exemption from of a tolerance is established for the res- the requirement of a tolerance. idues of Banda de Lupinus albus doce (BLAD), a naturally occurring An exemption from the requirement polypeptide from the catabolism of a of a tolerance is established for resi- seed storage protein (b-conglutin) of dues of natamycin in or on mushrooms sweet lupines (Lupinus albus), in or on when applied as a fungistat to prevent all food commodities when applied as a the germination of fungal spores on fungicide and used in accordance with mushrooms produced in enclosed mush- label directions and good agricultural room production facilities. practices. [77 FR 29548, May 18, 2012] [78 FR 17604, Mar. 22, 2013]

§ 180.1316 Pasteuria spp. § 180.1320 Methyl jasmonate; exemp- (Rotylenchulus reniformis nema- tion from the requirement of a tol- tode)—Pr3; exemption from the re- erance. quirement of a tolerance. An exemption from the requirement An exemption from the requirement of a tolerance is established for resi- of a tolerance is established for residues of methyl jasmonate in or on all food commodities when methyl dues of Pasteuria spp. (Rotylenchulus jasmonate is applied pre-harvest. reniformis nematode)—Pr3 in or on all food commodities when applied as a [78 FR 22794, Apr. 17, 2013] nematicide and used in accordance § 180.1321 Complex Polymeric with label directions and good agricul- Polyhydroxy Acids; exemption from tural practices. the requirement of a tolerance. [77 FR 40276, July 9, 2012] An exemption from the requirement of a tolerance is established for the res- § 180.1317 Pesticide chemicals; exemp- idues of complex polymeric tion from the requirements of a tol- polyhydroxy acids in or on all food erance. commodities when applied as a plant An exemption from the requirement growth regulator and used in accord- of a tolerance is established for resi- ance with good agricultural practices. dues of Didecyl dimethyl ammonium [78 FR 46267, July 31, 2013] chloride in or on broccoli resulting from the use of Didecyl dimethyl am- § 180.1322 Bacillus pumilus strain BU monium chloride as a seed treatment F–33; exemption from the requirement of a tolerance. at a treatment concentration of 1200 ppm prior to planting by immersion. An exemption from the requirement of a tolerance is established for resi- [77 FR 47296, Aug. 8, 2012] dues of Bacillus pumilus strain BU F–33 in or on all food commodities when ap- § 180.1318 3-decen-2-one; exemption plied to elicit induced systemic resist- from the requirement of a tolerance in plants and used in accordance ance. with label directions and good agricul- An exemption from the requirement tural practices. of a tolerance is established for resi- [78 FR 35149, June 12, 2013] dues of the biochemical pesticide, 3- decen-2-one, in or on potatoes when ap- § 180.1323 Ethyl-2E,4Z-decadienoate plied as a potato sprout inhibitor and (Pear Ester); exemption from the used in accordance with label direc- requirement of a tolerance. tions and good agricultural practices. An exemption from the requirement of a tolerance is established for resi- [78 FR 11766, Feb. 20, 2013] dues of the biochemical pesticide, ethyl-2E,4Z-decadienoate (pear ester),

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in or on all food commodities, when § 180.2000 Scope. used in accordance with label directions and good agricultural practices. This subpart sets forth the pesticide chemicals for use in agricultural or [78 FR 53054, Aug. 28, 2013] other food-related settings for which neither a tolerance nor an exemption is § 180.1324 GS-omega/kappa-Hxtx-Hv1a; exemption from the requirement of deemed to be needed by EPA. a tolerance. § 180.2003 Definitions. An exemption from the requirement of a tolerance is established for resi- (a) Food uses are the uses of a pes- dues of the pesticide GS-omega/kappa- ticide chemical that are likely to yield Hxtx-Hv1a in or on all food commod- residues in food or feed crops, meat, ities when applied or used in accord- milk, poultry or egg. ance with label directions and good ag- (b) Non-food uses are those uses that ricultural practices. are not likely to yield residues in food [79 FR 10685, Feb. 26, 2014] or feed crops, meat, milk, poultry or egg. § 180.1325 Heat-killed Burkholderia spp. strain A396 cells and spent fer- [66 FR 66772, Dec. 27, 2001, as amended at 73 mentation media exemption from FR 60158, Oct. 10, 2008] the requirement of a tolerance. § 180.2010 Threshold of regulation de- An exemption from the requirement terminations. of a tolerance is established for residues of heat-killed Burkholderia spp. The following pesticide chemical uses strain A396 cells and spent fermenta- on food or feed, or food or feed crops, tion media in or on all food commod- do not need a tolerance or exemption ities when applied as a biological insec- from the requirement of a tolerance, ticide to agricultural crops and used in and may be registered under the Fed- accordance with label directions and eral Insecticide, Fungicide, and good agricultural practices. Rodenticide Act, 7 U.S.C. 136 et seq., [79 FR 15704, Mar. 21, 2014] without obtaining such tolerance or exemption, based on EPA’s determina- Subpart E—Pesticide Chemicals tion that the uses are below the thresh- Not Requiring a Tolerance or old of regulation. an Exemption From a Toler- ance

SOURCE: 66 FR 66772, Dec. 27, 2001, unless otherwise noted.

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Pesticide Chemical CAS Reg. No. Use/Limits Analytical Method

Thiabendazole 148–79–8 As a seed treatment for dry pea (including field pea, pigeon High Perform- pea, chickpea or lentil), using a maximum application rate of ance Liquid 0.075 pounds of active ingredient per 100 pounds of seed. Chroma- Vines or hay grown from treated seed may not be fed to live- tography/Flo- stock.. rescence De- tector method 1; Modification of Ion-Pairing Liq- uid Chromatograp- hic Determina- tion of Benz- imidazole Fun- gicides in Foods, Gilvydis and Walters, JAOAC, vol. 73, no. 5, 1990. 1Available from: Chief, Analytical Chemistry Branch, Environmental Science Center, 701 Mapes Rd., Ft. Meade, MD 20755– 5350; telephone number: (410) 305–2905; e-mail address: [email protected]

[73 FR 1978, Jan. 11, 2008]

§ 180.2020 Non-food determinations. from the requirement of a tolerance based on EPA’s determination that The following pesticide chemical uses they are not likely to result in residues do not need a tolerance or exemption in or on food.

Pesticide Chemical CAS Reg. No. Limits Uses

Methyl bromide 74–83–9 When applied as a pre-plant soil fumigant All pre-plant soil uses Potassium 12298–68–9 When applied to growing crops in foreign countries Bananas, grapes, triiodide (KI3) and melons Rhodamine B 81–88–9 Not to exceed 2% by weight of the formulated product and 60 ppm on Dye for seed treat- the treated seed ment

[66 FR 66772, Dec. 27, 2001, as amended at 70 FR 40201, July 13, 2005; 71 FR 45402, Aug. 9, 2006]

PARTS 181–189 [RESERVED]

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