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Environmental Protection Agency Pt. 180

(2) Any order issued under § 180.7(g) of PART 180—TOLERANCES AND EX- this chapter to which the objection re- EMPTIONS FROM TOLERANCES lated, and: FOR PESTICIDE CHEMICALS IN (i) The regulation or petition denial FOOD that was the subject of that order. (ii) The petition to which such order responded. EDITORIAL NOTE: An alphabetical listing of pesticide chemicals appears at the end of (iii) Any amendment or supplement this table of contents. of the petition. (iv) The data and information sub- Subpart A—Definitions and Interpretative mitted in support of the petition. Regulations

(v) The notice of filing of the peti- DEFINITIONS AND INTERPRETATIONS tion. Sec. (3) Any order issued under § 180.29(f) 180.1 Definitions and interpretations. of this chapter to which the objection 180.3 Tolerances for related pesticide chemi- related, the regulation that was the cals. subject of that order, and each related 180.4 Exceptions. Notice of Proposed Rulemaking. 180.5 Zero tolerances. 180.6 Pesticide tolerances regarding milk, (4) The comments submitted by mem- eggs, meat, and/or poultry; statement of bers of the public in response to the policy. Notice of Filing or Notice of Proposed Rulemaking, and the information sub- Subpart B—Procedural Regulations mitted as part of the comments, the PROCEDURE FOR FILING PETITIONS SEEKING Administrator’s response to comments THE ESTABLISHMENT, MODIFICATION, OR and the documents or information re- REVOCATION OF TOLERANCES OR EXEMP- lied on by the Administrator in issuing TIONS the regulation or order. 180.7 Petitions proposing tolerances or ex- (5) All other documents or informa- emptions for pesticide residues in or on tion submitted to the docket for the raw agricultural commodities or proc- rulemaking in question under parts 177 essed foods. or part 180 of this chapter. 180.8 Withdrawal of petitions without preju- dice. (6) The Notice of Hearing published 180.9 Substantive amendments to petitions. under § 179.20. (7) All notices of participation filed ADVISORY COMMITTEES under § 179.42. ESTABLISHMENT, MODIFICATION, AND REVOCA- (8) Any FEDERAL REGISTER notice TION OF TOLERANCE ON INITIATIVE OF AD- issued under this part that pertains to MINISTRATOR; JUDICIAL REVIEW; TEMPORARY the proceeding. TOLERANCES; MODIFICATION AND REVOCA- TION OF TOLERANCES; FEES (9) All submissions filed under § 179.80. 180.29 Establishment, modification, and rev- (10) Any document of which official ocation of tolerance on initiative of Ad- ministrator. notice was taken under § 179.95. 180.30 Judicial review. (b) The record of the administrative 180.31 Temporary tolerances. proceeding is closed: 180.32 Procedure for modifying and revoking (1) With respect to the taking of evi- tolerances or exemptions from toler- dence, when specified by the presiding ances. 180.33 Fees. officer. 180.34 Tests on the amount of residue re- (2) With respect to pleadings, at the maining. time specified in § 179.98(a) for the fil- 180.35 Tests for potentiation. ing of briefs. 180.40 Tolerances for crop groups. (c) The presiding officer may reopen 180.41 Crop group tables. the record to receive further evidence Subpart C—Specific Tolerances at any time before the filing of the ini- tial decision. 180.101 Specific tolerances; general provi- sions. [55 FR 50293, Dec. 5, 1990, as amended at 70 180.103 Captan; tolerances for residues. FR 33360, June 8, 2005] 180.106 Diuron; tolerances for residues.

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180.108 ; tolerances for residues. 180.190 Diphenylamine; tolerances for resi- 180.110 Maneb; tolerances for residues. dues. 180.111 ; tolerances for residues. 180.191 Folpet; tolerances for residues. 180.114 Ferbam; tolerances for residues. 180.198 Trichlorfon; tolerances for residues. 180.116 Ziram; tolerances for residues. 180.200 Dicloran; tolerances for residues. 180.117 S-Ethyl dipropylthiocarbamate; tol- 180.202 p-Chlorophenoxyacetic acid; toler- erances for residues. ances for residues. 180.121 Methyl ; tolerances for res- 180.204 including its oxygen idues. analog; tolerances for residues. 180.122 Parathion; tolerances for residues. 180.205 ; tolerances for residues. 180.123 Inorganic bromide residues resulting 180.206 ; tolerances for residues. from fumigation with methyl bromide; 180.207 ; tolerances for residues. tolerances for residues. 180.208 N-Butyl-N-ethyl-a·a·a-trifluoro-2,6- 180.123a Inorganic bromide residues in pea- dinitro-p-toluidine; tolerances for resi- nut hay and peanut hulls; statement of dues. policy. 180.209 Terbacil; tolerances for residues. 180.127 Piperonyl butoxide; tolerances for 180.210 Bromacil; tolerances for residues. residues. 180.211 2-Chloro-N-isopropylacetanilide; tol- 180.128 ; tolerances for residues. erances for residues. 180.129 o-Phenylphenol and its sodium salt; 180.212 S-Ethyl cyclohexylethylthiocarba- tolerances for residues. mate; tolerances for residues. 180.130 Hydrogen Cyanide; tolerances for 180.213 ; tolerances for residues. residues. 180.214 ; tolerances for residues. 180.215 ; tolerances for residues. 180.132 Thiram; tolerances for residues. 180.217 Ammoniates for [ethylenebis- 180.133 ; tolerances for residues. (dithiocarbamato)] zinc and ethylenebis 180.136 Basic copper carbonate; tolerance [dithiocarbamic acid] bimolecular and for residues. trimolecular cyclic anhydrosulfides and 180.142 2,4-D; tolerances for residues. disulfides; tolerances for residues. 180.144 Cyhexatin; tolerances for residues. 180.220 ; tolerances for residues. 180.145 Fluorine compounds; tolerances for 180.221 O-Ethyl S-phenyl ethylphosphonodi- residues. thioate; tolerances for residues. 180.149 Mineral oil; tolerances for residues. 180.222 Prometryn; tolerances for residues. 180.151 Ethylene oxide; tolerances for resi- 180.225 Phosphine; tolerances for residues. dues. 180.226 ; tolerances for residues. 180.153 ; tolerances for residues. 180.227 ; tolerances for residues. 180.154 O,O-Dimethyl S-[(4-oxo-1,2,3-benzo- 180.228 S-Ethyl hexahydro-1H-azepine-1- triazin-3(4H)- carbothioate; tolerances for residues. yl)methyl]phosphorodithioate; toler- 180.229 Fluometuron; tolerances for resi- ances for residues. dues. 180.155 1-Naphthaleneacetic acid; tolerances 180.231 Dichlobenil; tolerances for residues. for residues. 180.232 Butylate; tolerances for residues. 180.157 Methyl 3-[(dimethoxyphosphinyl) 180.235 ; tolerances for residues. oxy]butenoate, alpha and beta isomers; 180.236 Triphenyltin hydroxide; tolerances tolerances for residues. for residues. 180.163 1,1-Bis(p-chlorophenyl)-2,2,2- 180.238 S-Propyl butylethylthiocarbamate; trichloroethanol; tolerances for residues. tolerances for residues. 180.167 Nicotine-containing compounds; tol- 180.239 ; tolerances for resi- erances for residues. dues. 180.169 ; tolerances for residues. 180.241 S-(O,O-Diisopropyl phosphorodi- 180.172 Dodine; tolerances for residues. thioate) of N-(2-mercaptoethyl) benzene- 180.173 ; tolerances for residues. sulfonamide; tolerances for residues. 180.175 Maleic hydrazide; tolerances for resi- 180.242 Thiabendazole; tolerances for resi- dues. dues. 180.176 Mancozeb; tolerances for residues. 180.243 Propazine; tolerances for residues. 180.178 Ethoxyquin; tolerances for residues. 180.245 Streptomycin; tolerances for resi- 180.180 Orthoarsenic acid; tolerance for resi- dues. dues. 180.249 ; tolerances for residues. 180.181 CIPC; tolerances for residues. 180.252 ; tolerances for 180.182 ; tolerances for residues. residues. 180.183 O,O-Diethyl S-[2-(ethylthio)ethyl] 180.253 ; tolerances for residues. phosphorodithioate; tolerances for resi- 180.254 ; tolerances for residues. dues. 180.257 Chloroneb; tolerances for residues. 180.184 ; tolerances for residues. 180.258 Ametryn; tolerances for residues. 180.185 Dimethyl tetrachloroterephthalate; 180.259 Propargite; tolerances for residues. tolerances for residues. 180.261 N-(Mercaptomethyl) phthalimide S- 180.189 ; tolerances for residues. (O,O-dimethyl phosphorodithioate) and

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its oxygen analog; tolerances for resi- 180.339 MCPA; tolerances for residues. dues. 180.341 2,4-Dinitro-6-octylphenyl crotonate 180.262 Ethoprop; tolerances for residues. and 2,6-dinitro-4-octylphenyl crotonate; 180.263 ; tolerances for residues. tolerances for residues. 180.269 ; tolerances for residues. 180.342 ; tolerances for residues. 180.272 Tribuphos; tolerances for residues. 180.345 Ethofumesate; tolerances for resi- 180.274 ; tolerances for residues. dues. 180.275 Chlorothalonil; tolerances for resi- 180.349 ; tolerances for residues. dues. 180.350 Nitrapyrin; tolerances for residues. 180.276 hydrochloride; toler- 180.352 ; tolerances for residues. ances for residues. 180.353 Desmedipham; tolerances for resi- 180.278 Phenmedipham; tolerances for resi- dues. dues. 180.355 ; tolerances for residues. 180.284 Zinc phosphide; tolerances for resi- 180.356 Norflurazon; tolerances for residues. dues. 180.360 ; tolerance for residues. 180.287 ; tolerances for residues. 180.361 ; tolerances for resi- 180.288 2-(Thiocyanomethylthio) dues. benzothiazole; tolerances for residues. 180.362 Hexakis (2-methyl-2-phenyl- 180.289 Methanearsonic acid; tolerances for propyl)distannoxane; tolerances for resi- residues. dues. 180.291 Pentachloronitrobenzene; tolerance 180.364 ; tolerances for residues. for residues. 180.368 ; tolerances for residues. 180.292 ; tolerances for residues. 180.367 n-Octyl bicycloheptenedicarbox- 180.293 ; tolerances for residues. imide; tolerances for residues. 180.294 Benomyl; tolerances for residues. 180.369 Difenzoquat; tolerances for residues. 180.296 Dimethyl phosphate of 3-hydroxy-N- 180.370 5-Ethoxy-3-(trichloromethyl)-1, 2, 4- methyl-cis-crotonamide; tolerances for thiadiazole; tolerances for residues. residues. 180.371 Thiophanate-methyl; tolerances for 180.297 N-1-Naphthyl phthalamic acid; toler- residues. ances for residues. 180.372 2, 6-dimethyl-4-tridecylmorpholine; 180.298 ; tolerances for resi- tolerances for residues. dues. 180.373 [Reserved] 180.299 Dimethyl phosphate of 3-hydroxy- 180.377 ; tolerances for resi- N,N-dimethyl-cis-crotonamide; tolerances dues. for residues. 180.378 ; tolerances for residues. 180.300 ; tolerances for residues. 180.379 Cyano(3-phenoxyphenyl)methyl-4- 180.301 Carboxin; tolerances for residues. chloro-a-(1-methylethyl) benzeneacetate; 180.303 ; tolerances for residues. tolerances for residues. 180.304 Oryzalin; tolerances for residues. 180.380 Vinclozolin; tolerances for residues. 180.309 a-Naphthaleneacetamide; tolerances 180.381 Oxyfluorfen; tolerances for residues. for residues. 180.383 Sodium salt of ; toler- 180.311 ; tolerances for resi- ances for residues. dues. 180.384 Mepiquat (N,N-dimethylpiperidin- 180.312 4-Aminopyridine; tolerances for resi- ium); tolerances for residues. dues. 180.385 Diclofop-methyl; tolerances for resi- 180.314 Triallate; tolerances for residues. dues. 180.315 ; tolerances for resi- 180.388–180.389 [Reserved] dues. 180.390 ; tolerances for residues. 180.316 Pyrazon; tolerances for residues. 180.395 ; tolerances for resi- 180.317 Propyzamide; tolerances for resi- dues. dues. 180.396 ; tolerances for residues. 180.318 4-(2-Methyl-4-chlorophenoxy) bu- 180.399 Iprodione; tolerances for residues. tyric acid; tolerance for residues. 180.401 Thiobencarb; tolerances for residues. 180.319 Interim tolerances. 180.403 Thidiazuron; tolerances for residues. 180.324 ; tolerances for residues. 180.404 ; tolerances for residues. 180.325 2-(m-Chlorophenoxy) propionic acid; 180.405 Chlorsulfuron; tolerances for resi- tolerances for residues. dues. 180.328 N,N-Diethyl-2-(1-naphthalenyloxy) 180.406 Dimethipin; tolerances for residues. propionamide; tolerances for residues. 180.407 Thiodicarb; tolerances for residues. 180.330 S-[2-(Ethylsulfinyl) ethyl] O,O-di- 180.408 Metalaxyl; tolerances for residues. methyl phosphorothioate; tolerances for 180.409 Pirimiphos-methyl; tolerances for residues. residues. 180.331 4-(2,4-Dichlorophenoxy) butyric acid; 180.410 Triadimefon; tolerances for residues. tolerances for residues. 180.411 -butyl; tolerances for resi- 180.332 ; tolerances for residues. dues. 180.337 Oxytetracycline; tolerance for resi- 180.412 ; tolerances for residues. dues. 180.413 Imazalil; tolerances for residues.

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180.414 ; tolerances for residues. 180.454 Nicosulfuron, [3-pyridinecarbox- 180.415 Aluminum tris (O-ethylphospho- amide, 2-((((4,6-dimethoxypyrimidin-2- nate); tolerances for residues. yl)aminocarbonyl)aminosulfonyl))-N,N- 180.416 Ethalfluralin; tolerances for resi- dimethyl]; tolerances for residues. dues. 180.455 Procymidone; tolerances for resi- 180.417 ; tolerances for residues. dues. 180.418 and an isomer zeta- 180.456 Oxadixyl; tolerances for residues. cypermethrin; tolerances for residues. 180.457 Beta-([1,1′-biphenyl]-4-yloxy)-alpha- 180.419 Chlorpyrifos-methyl; tolerances for (1,1-dimethylethyl)-1H-1,2,4-triazole-1- residues. ethanol; tolerances for residues. 180.420 Fluridone; tolerances for residues. 180.458 Clethodim; tolerances for residues. 180.421 Fenarimol; tolerances for residues. 180.459 Triasulfuron; tolerances for residues. 180.422 ; tolerances for resi- 180.460 Benoxacor; tolerances for residues. dues. 180.461 Cadusafos; tolerances for residues. 180.425 ; tolerances for residues. 180.462 Pyridate; tolerances for residues. 180.426 2-[4,5-Dihydro-4-methyl-4-(1- 180.463 ; tolerances for residues. methylethyl)-5-oxo-1H-imidazol-2-yl]-3- 180.464 Dimethenamid; tolerances for resi- quinoline carboxylic acid; tolerance for dues. residues. 180.465 4-(Dichloroacetyl)-1-oxa-4- 180.427 Fluvalinate; tolerances for residues. azaspiro[4.5]decane. 180.428 Metsulfuron methyl; tolerances for 180.466 ; tolerances for resi- residues. dues. 180.429 Chlorimuron ethyl; tolerance for res- 180.467 Carbon disulfide; tolerances for resi- idues. dues. 180.430 Fenoxaprop-ethyl; tolerances for res- 180.468 Flumetsulam; tolerances for resi- idues. dues. 180.431 ; tolerances for residues. 180.469 Dichlormid; tolerances for residues. 180.432 ; tolerances for residues. 180.470 ; tolerances for residues. 180.433 ; tolerances for residues. 180.471 Furilazole; tolerances for residues. 180.434 Propiconazole; tolerances for resi- 180.472 ; tolerances for resi- dues. dues. 180.435 ; tolerances for resi- 180.473 ammonium; tolerances dues. for residues. 180.436 ; tolerances for residues. 180.474 Tebuconazole; tolerances for resi- 180.437 Methyl 2-(4-isopropyl-4-methyl-5- dues. oxo-2-imidazolin-2-yl)-p-toluate and 180.475 Difenoconazole; tolerances for resi- methyl 6-(4-isopropyl-4-methyl-5-oxo-2- dues. imidazolin-2-yl)-m-toluate; tolerances for 180.476 Triflumizole; tolerances for residues. residues. 180.477 Flumiclorac pentyl; tolerances for 180.438 Lambda- and an isomer residues. gamma-cyhalothrin; tolerances for resi- 180.478 Rimsulfuron; tolerances for residues. dues. 180.479 Halosulfuron-methyl; tolerances for 180.439 Thifensulfuron methyl; tolerances residues. for residues. 180.480 Fenbuconazole; tolerances for resi- 180.440 ; tolerances for residues. dues. 180.441 Quizalofop ethyl; tolerances for resi- 180.481 Prosulfuron; tolerances for residues. dues. 180.482 ; tolerances for resi- 180.442 ; tolerances for residues. dues. 180.443 Myclobutanil; tolerances for resi- 180.483 O-[2-(1,1-Dimethylethyl)-5-pyri- dues. midinyl] O-ethyl-O-(1-methylethyl) 180.444 Sulfur dioxide; tolerances for resi- phosphorothioate; tolerances for resi- dues. dues. 180.445 Bensulfuron methyl; tolerances for 180.484 Flutolanil (N-(3-(1-methyl- residues. ethoxy)phenyl)-2- 180.446 Clofentezine; tolerances for residues. (trifluoromethyl)benzamide); tolerances 180.447 Imazethapyr; tolerances for residues. for residues. 180.448 Hexythiazox; tolerance for residues. 180.485 Cyproconazole; tolerances for resi- 180.449 Avermectin B1 and its delta-8,9-iso- dues. mer; tolerances for residues. 180.486 Phosphorothioic acid, 0,0-diethyl 0- 180.450 Beta-(4-Chlorophenoxy)-alpha-(1,1- (1,2,2,2-tetrachloroethyl) ester; toler- dimethylethyl)-1H-1,2,4-triazole-1-eth- ances for residues. anol; tolerances for residues. 180.487 Pyrithiobac sodium; tolerances for 180.451 Tribenuron methyl; tolerances for residues. residues. 180.489 Sulfosate (Sulfonium, trimethyl-salt 180.452 Primisulfuron-methyl; tolerances for with N-(phosphonomethyl)glycine (1:1)); residues. tolerances for residues.

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180.490 -ammonium; tolerances for 180.535 1-methylheptyl ester; residues. tolerances for residues. 180.491 Propylene oxide; tolerances for resi- 180.536 Triazamate; tolerances for residues. dues. 180.537 Isoxaflutole; tolerances for residues. 180.492 Triflusulfuron methyl; tolerances for 180.538 Copper; tolerances for residues. residues 180.539 d-; tolerances for residues. 180.493 Dimethomorph; tolerances for resi- 180.540 ; tolerances for resi- dues. dues. 180.494 Pyridaben; tolerance for residues. 180.541 Propetamphos; tolerances for resi- 180.495 ; tolerances for residues. dues. 180.496 Thiazopyr; tolerances for residues. 180.543 Diclosulam; tolerances for residues. 180.497 Clofencet; tolerances for residues. 180.544 Methoxyfenozide; tolerances for resi- 180.498 ; tolerances for resi- dues. dues. 180.545 (RS)-2-methyl-4-oxo-3-(2- 180.499 Propamocarb hydrochloride, toler- propynyl)cyclopent-2-enyl (1RS)-cis, ances for residues. trans-chrysanthemate; tolerances for res- 180.500 ; tolerances for residues. idues. 180.501 ; tolerances for residues. 180.546 Mefenoxam; tolerances for residues. 180.502 Aminoethoxyvinylglycine hydro- 180.547 Prohexadione calcium; tolerances chloride (aviglycine HCl); tolerances for for residues. residues. 180.548 Tralkoxydim; tolerances for resi- 180.503 Cymoxanil, tolerance for residues. dues. 180.504 [Reserved] 180.549 Diflufenzopyr; tolerances for resi- 180.505 Emamectin; tolerances for residues. dues. 180.506 Cyclanilide; tolerances for residues. 180.550 Arsanilic acid [(4-aminophenyl) 180.507 Azoxystrobin; tolerances for resi- arsonic acid]; tolerances for residues. dues. 180.551 Fluthiacet-methyl; tolerances for 180.509 Mefenpyr-diethyl; tolerance for resi- residues. dues. 180.552 Sulfosulfuron; tolerances for resi- 180.510 ; tolerances for resi- dues. dues. 180.553 Fenhexamid; tolerances for residues. 180.511 ; tolerances for residues. 180.554 Kresoxim-methyl; tolerances for res- 180.512 [Reserved] idues. 180.513 ; tolerances for resi- 180.555 Trifloxystrobin; tolerances for resi- dues. dues. 180.514 Cloransulam-methyl; tolerances for 180.556 Pymetrozine; tolerances for resi- residues. dues. 180.515 Carfentrazone-ethyl; tolerances for 180.557 Tetraconazole; tolerances for resi- residues. dues. 180.516 Fludioxonil; tolerances for residues. 180.558 N,N-diethyl-2-(4-methylbenzyl- 180.517 ; tolerances for residues. oxy)ethylamine hydrochloride; toler- 180.518 Pyrimethanil; tolerances for resi- ances for residues. dues. 180.559 Clodinafop-propargyl; tolerances for 180.519 Bromide ion and residual bromine; residues. tolerances for residues. 180.560 Cloquintocet-mexyl; tolerances for 180.521 Fumigants for grain-mill machinery; residues. tolerances for residues. 180.561 Acibenzolar-S-methyl; tolerances for 180.522 Fumigants for processed grains used residues. in production of fermented malt bev- 180.562 Flucarbazone-sodium; tolerances for erage; tolerances for residues. residues. 180.523 Metaldehyde; tolerances for resi- 180.563 Ethametsulfuron-methyl; tolerances dues. for residues. 180.525 ; tolerances for residues. 180.564 ; tolerances for residues. 180.526 Synthetic isoparaffinic petroleum 180.565 ; tolerances for resi- hydrocarbons; tolerances for residues. dues. 180.527 Flufenacet, N-(4-fluorophenyl)-N-(1- 180.566 Fenpyroximate; tolerances for resi- methylethyl)-2-[[5-(trifluoromethyl)-1, 3, dues. 4-thiadiazol-2-yl] oxy]acetamide and its 180.567 Zoxamide; tolerances for residues. metabolites containing the 4-fluoro-N- 180.568 Flumioxazin; tolerances for residues. methylethyl benzenamine tolerances for 180.569 Forchlorfenuron; tolerances for resi- residues. dues. 180.530 2,2-Dimethyl-1,3-benzodioxol-4-ol 180.570 Isoxadifen-ethyl; tolerances for resi- methylcarbamate; tolerances for resi- dues. dues. 180.571 ; tolerances for residues. 180.532 Cyprodinil; tolerances for residues. 180.572 Bifenazate; tolerance for residues. 180.533 ; tolerances for resi- 180.573 Tepraloxydim; tolerances for resi- dues. dues.

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180.574 Fluazinam; tolerances for residues. 180.619 Epoxiconazole; tolerances for resi- 180.575 Sulfuryl fluoride; tolerances for resi- dues. dues. 180.620 ; tolerances for residues. 180.576 Cyhalofop-butyl; tolerances for resi- 180.621 Dithianon; tolerances for residues. dues. 180.622 Ethaboxam; tolerances for residues. 180.577 Bispyribac-sodium; tolerances for 180.623 ; tolerances for resi- residues. dues. 180.578 ; tolerances for residues. 180.624 Metrafenone; tolerances for residues. 180.579 Fenamidone; tolerances for residues. 180.625 Orthosulfamuron; tolerances for res- 180.580 Iodosulfuron-Methyl-Sodium; toler- idues. ances for residues. 180.626 Prothioconazole; tolerances for resi- 180.581 Iprovalicarb; tolerances for residues. dues. 180.582 Pyraclostrobin; tolerances for resi- 180.627 Fluopicolide; tolerances for residues. dues. 180.628 ; tolerances for 180.583 Triticonazole; tolerances for resi- residues. dues. 180.584 Tolylfluanid; tolerances for residues. Subpart D—Exemptions From Tolerances 180.585 Pyraflufen-ethyl; tolerances for resi- 180.900 Exemptions from the requirement of dues. a tolerance. 180.586 ; tolerances for residues. 180.905 Pesticide chemicals; exemptions 180.587 Famoxadone; tolerance for residues. from the requirement of a tolerance. 180.588 Quinoxyfen; tolerances for residues. 180.910 Inert ingredients used pre- and post- 180.589 Boscalid; tolerances for residues. harvest; exemptions from the require- 180.590 2, 6-Diisopropylnaphthalene (2, 6- ment of a tolerance. DIPN); tolerances for residues. 180.920 Inert ingredients used pre-harvest; 180.591 Trifloxysulfuron; tolerances for resi- exemptions from the requirement of a dues. tolerance. 180.592 ; tolerances for residues. 180.930 Inert ingredients applied to animals; 180.593 Etoxazole; tolerances for residues. exemptions from the requirement of a 180.594 ; tolerances for residues. tolerance. 180.595 Flufenpyr-ethyl; tolerances for resi- 180.940 Tolerance exemptions for active and dues. inert ingredients for use in antimicrobial 180.596 Fosthiazate; tolerances for residues. formulations (Food-contact surface sani- 180.597 Mesosulfuron-methyl; tolerances for tizing solutions). residues. 180.950 Tolerance exemptions for minimal 180.598 Novaluron; tolerances for residues. risk active and inert ingredients. 180.599 Acequinocyl; tolerances for residues. 180.960 Polymers; exemptions from the re- 180.600 Propoxycarbazone; tolerances for quirement of a tolerance. residues 180.1011 Viable spores of the microorganism 180.601 Cyazofamid; tolerances for residues. Berliner; exemption 180.602 Spiroxamine; tolerances for residues. from the requirement of a tolerance. 180.603 ; tolerances for residues. 180.1016 Ethylene; exemption from the re- 180.604 Mepanipyrim; tolerances for resi- quirement of a tolerance. dues. 180.1017 Diatomaceous earth; exemption 180.605 Penoxsulam; tolerances for residues. from the requirement of a tolerance. 180.607 Spiromesifen; tolerances for resi- 180.1019 Sulfuric acid; exemption from the dues. requirement of a tolerance. 180.608 Spirodiclofen; tolerances for resi- 180.1020 Sodium chlorate; exemption from dues. the requirement of a tolerance. 180.609 Fluoxastrobin; tolerances for resi- 180.1021 Copper; exemption from the re- dues. quirement of a tolerance. 180.610 ; tolerances for resi- 180.1022 Iodine-detergent complex; exemp- dues. tion from the requirement of a tolerance. 180.611 Pinoxaden; tolerances for residues. 180.1023 Propanoic acid; exemptions from 180.612 Topramezone; tolerances for resi- the requirement of a tolerance. dues. 180.1025 Xylene; exemption from the re- 180.613 Flonicamid; tolerances for residues. quirement of a tolerance. 180.614 Kasugamycin; tolerances for resi- 180.1027 Nuclear polyhedrosis virus of dues. Heliothis zea; exemption from the re- 180.615 Amicarbazone; tolerances for resi- quirement of a tolerance. dues. 180.1033 ; exemption from the re- 180.616 Fenpropimorph; tolerances for resi- quirement of a tolerance. dues. 180.1035 Pine oil; exemption from the re- 180.617 Metconazole; tolerances for residues. quirement of a tolerance. 180.618 Benthiavalicarb-isopropyl; tolerance 180.1037 Polybutenes; exemption from the for residues. requirement of a tolerance.

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180.1040 Ethylene glycol; exemption from 180.1087 Sesame stalks; exemption from the the requirement of a tolerance. requirement of a tolerance. 180.1041 Nosema locustae; exemption from 180.1089 Poly-N-acetyl-D-glucosamine; ex- the requirement of a tolerance. emption from the requirement of a toler- 180.1043 Gossyplure; exemption from the re- ance. quirement of a tolerance. 180.1090 Lactic acid; exemption from the re- 180.1049 Carbon dioxide; exemption from the quirement of a tolerance. requirement of a tolerance. 180.1091 Aluminum isopropoxide and alu- 180.1050 Nitrogen; exemption from the re- minum secondary butoxide; exemption quirements of a tolerance. from the requirement of a tolerance. 180.1052 2,2,5-trimethyl-3-dichloroacetyl-1,3- 180.1092 Menthol; exemption from the re- oxazolidine; exemption from the require- quirement of a tolerance. ment of a tolerance. 180.1095 Chlorine gas; exemptions from the 180.1054 Calcium hypochlorite; exemptions requirement of a tolerance. from the requirement of a tolerance. 180.1056 Boiled linseed oil; exemption from 180.1097 GBM-ROPE; exemption from the re- requirement of tolerance. quirement of a tolerance. 180.1057 Phytophthora palmivora; exemption 180.1098 Gibberellins [Gibberellic Acids (GA3 from requirement of tolerance. and GA4 + GA7), and Sodium or Potas- 180.1058 Sodium diacetate; exemption from sium Gibberellate]; exemption from the the requirement of a tolerance. requirement of a tolerance. 180.1064 Tomato pinworm insect pheromone; 180.1100 Gliocladium virens isolate GL-21; ex- exemption from the requirement of a tol- emption from the requirement of a toler- erance. ance. 180.1065 2-Amino-4,5-dihydro-6-methyl-4- 180.1101 Parasitic (parasitoid) and predatory propyl-s-triazolo(1,5-alpha)pyrimidin-5- insects; exemption from the requirement one; exemption from the requirement of of a tolerance. a tolerance. 180.1102 Trichoderma harzianum KRL-AG2 180.1067 Methyl eugenol and malathion com- (ATCC #20847) strain T–22; exemption bination; exemption from the require- from requirement of a tolerance. ment of a tolerance. 180.1103 Isomate-C; exemption from the re- 180.1068 C12-C18 fatty acid potassium salts; quirement of a tolerance. exemption from the requirement of a tol- 180.1107 Delta endotoxin of Bacillus erance. thuringiensis variety kurstaki encap- 180.1069 (Z)-11-Hexadecenal; exemption from sulated into killed Pseudomonas the requirement of a tolerance. fluorescens; exemption from the require- 180.1070 Sodium chlorite; exemption from ment of a tolerance. the requirement of a tolerance. 180.1108 Delta endotoxin of Bacillus 180.1071 Peanuts, Tree Nuts, Milk, Soy- thuringiensis variety San Diego encap- beans, Eggs, Fish, Crustacea, and Wheat; sulated into killed Pseudomonas exemption from the requirement of a tol- fluorescens; exemption from the require- erance. ment of a tolerance. 180.1072 Poly-D-glucosamine (chitosan); ex- 180.1110 3-Carbamyl-2,4,5-trichlorobenzoic emption from the requirement of a toler- acid; exemption from the requirement of ance. a tolerance. 180.1073 Isomate-M; exemption from the re- 180.1111 Bacillus subtilis GB03; exemption quirement of a tolerance. from the requirement of a tolerance. 180.1074 F.D.&C. Blue No. 1; exemption from 180.1113 Lagenidium giganteum; exemption the requirement of a tolerance. 180.1075 Colletotrichum gloeosporioides f. sp. from the requirement of a tolerance. aeschynomene; exemption from the re- 180.1114 Pseudomonas fluorescens A506, quirement of a tolerance. Pseudomonas fluorescens 1629RS, and 180.1076 Viable spores of the microorganism Pseudomonas syringae 742RS; exemptions Bacillus popilliae; exemption from the re- from the requirement of a tolerance. quirement of a tolerance. 180.1118 Spodoptera exigua nuclear poly- 180.1080 volatiles and pheromone; ex- hedrosis virus; exemption from the re- emptions from the requirement of a tol- quirement of a tolerance. erance. 180.1119 ; exemption from the 180.1083 Dimethyl sulfoxide; exemption requirement of a tolerance. from the requirement of a tolerance. 180.1120 Streptomyces sp. strain K61; exemp- 180.1084 Monocarbamide dihydrogen sulfate; tion from the requirement of a tolerance. exemption from the requirement of a tol- 180.1121 and its salts, borax (so- erance. dium borate decahydrate), disodium 180.1086 3,7,11-Trimethyl-1,6,10-dodecatriene- octaborate tetrahydrate, boric oxide 1-ol and 3,7,11-trimethyl-2,6,10- (boric anhydride), sodium borate and so- dodecatriene-3-ol; exemption from the re- dium metaborate; exemptions from the quirement of a tolerance. requirement of a tolerance.

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180.1122 Inert ingredients of semiochemical 180.1154 CryIA(c) and CryIC derived delta- dispensers; exemptions from the require- endotoxins of Bacillus thuringiensis var. ment of a tolerance. kurstaki encapsulated in killed 180.1124 Arthropod pheromones; exemption Pseudomonas fluorescens, and the expres- from the requirement of a tolerance. sion plasmid and cloning vector genetic 180.1126 Codlure, (E,E)-8,10-Dodecadien-1-ol; constructs. exemption from the requirement of a tol- 180.1155 Bacillus thuringiensis subspecies erance. Kurstaki CryIA(c) and the genetic mate- 180.1127 Biochemical pesticide plant floral rial necessary for its production in all volatile attractant compounds: cinna- ; exemption from the requirement maldehyde, cinnamyl alcohol, 4-methoxy of a tolerance. cinnamaldehyde, 3-phenyl propanol, 4- 180.1156 Cinnamaldehyde; exemption from methoxy phenethyl alcohol, indole, and the requirement of a tolerance. 1,2,4-trimethoxybenzene; exemptions 180.1157 Cytokinins; exemption from the re- from the requirement of a tolerance. quirement of a tolerance. 180.1128 Bacillus subtilis MBI 600; exemption 180.1158 ; exemption from the re- from the requirement of a tolerance. quirement of a tolerance. 180.1130 N-(n-octyl)-2-pyrrolidone and N-(n- 180.1159 Pelargonic acid; exemption from dodecyl)-2-pyrrolidone; exemptions from the requirement of tolerances. the requirement of a tolerance. 180.1160 Jojoba oil; exemption from the re- 180.1131 Ampelomyces quisqualis isolate M10; quirement of a tolerance. exemption from the requirement of a tol- 180.1161 Clarified hydrophobic extract of erance. neem oil; exemption from the require- 180.1134 Neomycin phosphotransferase II ment of a tolerance. and genetic material necessary for its 180.1162 Acrylate polymers and copolymers; production; exemption from the require- exemption from the requirement of a tol- ment of a tolerance. erance. 180.1135 Pasteuria penetrans; exemption from 180.1163 Killed Myrothecium verrucaria; ex- the requirement of a tolerance. emption from the requirement of a toler- 180.1139 Sodium 5-nitroguaiacolate; exemp- ance. tion from the requirement of a tolerance. 180.1165 Capsaicin; exemption from the re- 180.1140 Sodium o-nitrophenolate; exemp- quirement of a tolerance. tion from the requirement of a tolerance. 180.1167 Allyl isothiocyanate as a compo- 180.1141 Sodium p-nitrophenolate; exemp- nent of food grade oil of mustard; exemp- tion from the requirement of a tolerance. tion from the requirement of a tolerance. 180.1142 1,4-Dimethylnaphthalene; exemp- 180.1173 Bacillus thuringiensis CryIA(b) delta- tion from the requirement of a tolerance. endotoxin and the genetic material nec- 180.1143 Methyl anthranilate; exemption essary for its production in all plants. from the requirement of a tolerance. 180.1174 CP4 Enolpyruvylshikimate-3-phos- 180.1144 Candida oleophila isolate I-182; ex- phate (CP4 EPSPS) and the genetic ma- emption from the requirement of a toler- terial necessary for its production in all ance. plants. 180.1145 Pseudomonas syringae; exemption 180.1176 Sodium bicarbonate; exemption from the requirement of a tolerance. from the requirement of a tolerance. 180.1146 Beauveria bassiana Strain GHA; ex- 180.1177 Potassium bicarbonate; exemption emption from the requirement of a toler- from the requirement of a tolerance. ance. 180.1178 Formic acid; exemption from the 180.1147 Bacillus thuringiensis CryIIIA delta- requirement of a tolerance. endotoxin and the genetic material nec- 180.1179 Plant extract derived from Opuntia essary for its production. lindheimeri, Quercus falcata, Rhus 180.1148 Occlusion Bodies of the Granulosis aromatica, and Rhizophoria mangle; ex- Virus of Cydia pomenella; tolerance ex- emption from the requirement of a toler- emption. ance. 180.1149 Inclusion bodies of the multi-nu- 180.1180 Kaolin; exemption from the require- clear polyhedrosis virus of Anagrapha ment of a tolerance. falcifera; exemption from the require- 180.1181 Bacillus cereus strain BPO1; exemp- ment of a tolerance. tion from the requirement of a tolerance. 180.1150 6-Benzyladenine; exemption from 180.1182 Coat Protein of Virus Y and the requirement of a tolerance. the genetic material necessary for its 180.1151 Phosphinothricin Acetyltransferase production; exemption from the require- (PAT) and the genetic material nec- ment of a tolerance. essary for its production all plants; ex- 180.1183 Potato Roll Virus Resistance emption from the requirement of a toler- Gene (also known as orf1/orf2 gene) and ance. the genetic material necessary for it’s 180.1153 Lepidopteran pheromones; exemp- production; Exemption from the require- tion from the requirement of a tolerance. ment of a tolerance.

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180.1184 Coat Protein of Watermelon Mosaic 180.1210 Phosphorous acid; exemption from Virus-2 and Zucchini Yellow Mosaic the requirement of a tolerance. Virus and the genetic material necessary 180.1212 Pseudomonas chlororaphis Strain 63– for its production; exemption from the 28; exemption from the requirement of a requirement of a tolerance. tolerance. 180.1185 Coat Protein of Papaya Ringspot 180.1213 Coniothyrium minitans strain CON/ Virus and the genetic material necessary M/91–08; exemption from the requirement for its production; exemption from the of a tolerance. requirement of a tolerance. 180.1214 Bacillus thuringiensis Cry3Bb1 pro- 180.1186 Coat protein of cucumber mosaic tein and the genetic material necessary virus and the genetic material necessary for its production in corn; exemption for its production; exemption from the from the requirement of a tolerance. requirement of a tolerance. 180.1215 Bacillus thuringiensis Cry2Ab2 pro- 180.1187 L-glutamic acid; exemption from tein and the genetic material necessary the requirement of a tolerance. for its production in cotton; exemption 180.1188 Gamma aminobutyric acid; exemp- from the requirement of a tolerance. tion from the requirement of a tolerance. 180.1216 B-D-glucuronidase from E. coli and 180.1189 Methyl salicylate; exemption from the genetic material necessary for its the requirement of a tolerance. production as a plant-pesticide inert in- 180.1190 Glyphosate Oxidoreductase [GOX or gredient; exemption from the require- GOXv247] and the genetic material nec- ment of a tolerance. essary for its production in all plants; ex- 180.1217 Bacillus thuringiensis Cry1F protein emption from the requirement of a toler- and the genetic material necessary for ance. its production in corn; exemption from 180.1191 Ferric phosphate; exemption from the requirement of a tolerance. the requirement of a tolerance. 180.1218 Indian Meal Moth Granulosis Virus; 180.1192 Bacillus thuringiensis subspecies exemption from the requirement of a tol- tolwothi Cry9C protein and the genetic erance. material necessary for its production in 180.1219 Foramsulfuron; exemption from the corn; exemption from the requirement of requirement of a tolerance. a tolerance. 180.1220 1-Methylcyclopropene; exemption 180.1193 Potassium dihydrogen phosphate; from the requirement of a tolerance. exemption from the requirement of a tol- 180.1221 Pseudozyma flocculosa strain PF-A22 erance. UL; exemption from the requirement of a 180.1195 Titanium dioxide; exemption from tolerance. the requirement of a tolerance. 180.1222 Sucrose octanoate esters; exemp- 180.1196 Peroxyacetic acid; exemption from tion from the requirement of a tolerance. the requirement of a tolerance. 180.1223 Imazamox; exemption from the re- 180.1197 Hydrogen peroxide; exemption from quirement of a tolerance. the requirement of a tolerance. 180.1224 Bacillus pumilus GB34; exemption 180.1198 Gliocladium catenulatum strain from the requirement of a tolerance. J1446; exemption from the requirement of 180.1225 Decanoic acid; exemption from the a tolerance. requirement of a tolerance. 180.1199 Lysophosphatidylethanolamine 180.1226 Bacillus pumilus strain QST2808; (LPE); exemption from the requirement temporary exemption from the require- of a tolerance. ment of a tolerance. 180.1200 Pseudomonas fluorescens strain 180.1227 Bacillus thuringiensis Cry1F protein PRA–25; temporary exemption from the and it genetic material necessary for its requirement of a tolerance. production in or on cotton; temporary 180.1201 Trichoderma harzianum strain T-39; exemption from the requirement of a tol- exemption from the requirement of a tol- erance. erance. 180.1228 Diallyl sulfides; exemption from the 180.1202 Bacillus sphaericus; exemption from requirement of a tolerance. the requirement of a tolerance. 180.1230 Ferrous sulfate; exemption from 180.1204 Harpin protein; exemption from the the requirement of a tolerance. requirement of a tolerance. 180.1231 Lime; exemption from the require- 180.1205 Beauveria bassiana ATCC #74040; ex- ment of a tolerance. emption from the requirements of a tol- 180.1232 Lime-sulfur; exemption from the re- erance. quirement of a tolerance. 180.1206 Aspergillus flavus AF36; exemption 180.1233 Potassium sorbate; exemption from from the requirement of a tolerance. the requirement of a tolerance. 180.1207 N-acyl sarcosines and sodium N- 180.1234 Sodium carbonate; exemption from acyl sarcosinates; exemption from the re- the requirement of a tolerance. quirement of a tolerance. 180.1235 Sodium hypochlorite; exemption 180.1209 Bacillus subtilis strain QST 713; ex- from the requirement of a tolerance. emption from the requirement of a toler- 180.1236 Sulfur; exemption from the require- ance. ment of a tolerance.

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180.1237 Sodium metasilicate; exemption 180.1263 Tetrahydrofurfuryl alcohol; exemp- from the requirement of a tolerance. tion from the requirement of a tolerance. 180.1240 Thymol; exemption from the re- 180.1267 Pantoea agglomerans strain C9–1; quirement of a tolerance. exemption from the requirement of a tol- 180.1241 Eucalyptus oil; exemption from the erance. requirement of a tolerance. 180.1268 Potassium silicate; exemption from 180.1242 Bacillus thuringiensis Cry34Ab1 and the requirement of a tolerance. Cry35Ab1 proteins and the genetic mate- 180.1269 Bacillus mycoides Isolate J on rial necessary for their production in sugar beets: exemption from the require- corn; temporary exemption from the re- ment of a tolerance. quirement of a tolerance. 180.1270 Isophorone; exemption from the re- 180.1243 Bacillus subtilis var. amylolique- quirement of a tolerance. faciens strain FZB24; exemption from the 180.1271 Eucalyptus oil; exemption from the requirement of a tolerance. requirement of a tolerance. 180.1244 Ammonium bicarbonate; exemption 180.1272 Pantoea agglomerans strain E325; from the requirement of a tolerance. exemption from the requirement of a tol- 180.1245 Rhamnolipid biosurfactant; exemp- erance. tion from the requirement of a tolerance. 180.1273 Beauveria bassiana HF23; exemp- 180.1246 Yeast Extract Hydrolysate from tion from the requirement of a tolerance. Saccharomyces cerevisiae: exemption from 180.1274 Tris (2-ethylhexyl) phosphate; ex- the requirement of a tolerance. emption from the requirement of a toler- 180.1248 Exemption of citronellol from the ance. requirement of a tolerance. 180.1275 Pythium; exception from the re- 180.1249 Hygromycin B phosphotransferase quirement of a tolerance. (APH4) marker protein and the genetic 180.1276 Tobacco mild green mosaic material necessary for its production in tobamovirus (TMGMV); temporary ex- all plants; exemption from the require- emption from the requirement of a toler- ment of a tolerance. ance. 180.1250 C8, C10, and C12 fatty acid mono- esters of glycerol and propylene glycol; Subpart E—Pesticide Chemicals Not Re- exemption from the requirement of a tol- quiring a Tolerance or an Exemption erance. from a Tolerance 180.1251 Geraniol; exemption from the re- quirement of a tolerance. 180.2000 Scope. 180.1252 Phosphomannose isomerase and the 180.2003 Definitions. genetic material necessary for its pro- 180.2010 Threshold of regulation determina- duction in all plants; exemption from the tions. [Reserved] requirement of a tolerance. 180.2020 Non-food determinations. 180.1253 Streptomyces lydicus WYEC 108; ex- AUTHORITY: 21 U.S.C. 321(q), 346a and 371. emption from the requirement of a toler- ance. SOURCE: 36 FR 22540, Nov. 25, 1971, unless 180.1254 Aspergillus flavus NRRL 21882 on otherwise noted. peanut; exemption from requirement of a EDITORIAL NOTE: Nomenclature changes to tolerance. part 180 appear at 62 FR 66023, Dec. 17, 1997. 180.1255 Bacillus pumilus strain QST 2808; ex- emption from the requirement of a toler- ALPHABETICAL LISTING OF PESTICIDE CHEMICALS ance. 180.1256 Alternaria destruens strain 059; ex- emption from the requirement of a toler- Section Name Number ance. 180.1257 Paecilomyces lilacinus strain 251; ex- ACEPHATE ...... 180.108 emption from the requirement of a toler- ACETAMIPRID ...... 180.578 ance. ACETIC ACID ...... 180.1258 180.1258 Acetic acid; exemption from the re- ACETOCHLOR ...... 180.470 quirement of a tolerance. ACEQUINOCYL ...... 180.599 180.1259 Reynoutria sachalinensis extract; ex- ACIBENZOLAR-S-METHYL ...... 180.561 ACRYLATE POLYMERS AND CO- emption from the requirement of a toler- POLYMERS ...... 180.1162 ance. ACRYLIC AC-STEARYL METHACRY- 180.1260 Muscodor albus QST 20799 and the LATE COPOLYMER ...... 180.1109 volatiles produced on rehydration; ex- ACTIVE AND INERT INGREDIENTS emption from the requirement of a toler- FOR USE IN ANTIMICROBIAL ance. FORMULATIONS (FOOD-CON- 180.1261 Xanthomonas campestris pv. TACT SURFACE SANITIZING SO- LUTIONS) ...... 180.940 vesicatoria and Pseudomonas syringae pv. N-ACYL SARCOSINES AND SO- tomato specific Bacteriophages. DIUM N-SARCOSINATE ...... 180.1207 180.1262 Sorbitol octanoate; exemption from ALACHLOR ...... 180.249 the requirement of a tolerance. ALDICARB ...... 180.269

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ALPHABETICAL LISTING OF PESTICIDE ALPHABETICAL LISTING OF PESTICIDE CHEMICALS—Continued CHEMICALS—Continued

Name Section Section Number Name Number

ALLYL ISOTHIOCYANATE AS A BACILLUS THURINGIENSIS COMPONENT OF FOOD GRADE CRY3Bb1 PROTEIN AND THE GE- OIL OF MUSTARD ...... 180.1167 NETIC MATERIAL NECESSARY ALTERNARIA DESTRUENS STRAIN FOR ITS PRODUCTION IN CORN 180.1214 059 ...... 180.1256 BACILLUS THURINGIENSIS ALUMINUM ISOPROPOXIDE AND CRY34Ab1 and CRY35Ab1 PRO- ALUMINUM SECONDARY TEINS AND THE GENETIC MATE- BUTOXIDE ...... 180.1091 RIAL NECESSARY FOR THEIR ALUMINUM TRIS PRODUCTION IN CORN ...... 180.1242 (O,ETHYLPHOSPHONATE) ...... 180.415 BACILLUS THURINGIENSIS AMETRYN ...... 180.258 CRYIA(B) DELTA-ENDOTOXIN AMICARBAZONE ...... 180.615 AND THE GENETIC MATERIAL 2-AMINO-4,5-DIHYDRO-6-METHYL- NECESSARY FOR ITS PRODUC- 4-PROPYL-S-TRIAZOLO(1,5- TION (PLASMID VECTOR ALPHA)PYRIMIDIN-5-ONE ...... 180.1065 PCIB4431) IN CORN ...... 180.1152 AMINOETHOXYVINYLGLYCINE HY- DROCHLORIDE (AVIGLYCINE BACILLUS THURINGIENSIS CRYIIIA HCI) ...... 180.502 DELTA-ENDOTOXIN AND THE AMINOPYRALID ...... 180.610 GENETIC MATERIAL NECESSARY 4-AMINOPYRIDINE ...... 180.312 FOR ITS PRODUCTION ...... 180.1147 AMITRAZ ...... 180.287 BACILLUS THURINGIENSIS CRY1F AMMONIATES OF [ETHYLENEBIS PROTEIN AND ITS GENETIC MA- (DITHIOCARBAMATO)] ZINC AND TERIAL NECESSARY FOR ITS ETHYLENEBIS (DITHIOCARBAMIC PRODUCTION IN OR ON COTTON 180.1227 ACID) BIMOLECULAR AND BACILLUS THURINGIENSIS SUB- TRIMOLECULAR CYCLIC SPECIES KURSTAKI CRYIA(C) ANHYDROSULFIDES AND AND THE GENETIC MATERIAL DISULFIDES ...... 180.217 NECESSARY FOR ITS PRODUC- AMMONIUM BICARBONATE ...... 180.1244 TION IN ALL PLANTS ...... 180.1155 AMPELOMYCES QUISQUALIS ISO- BACILLUS THURINGIENSIS SUB- LATE M10 ...... 180.1131 SPECIES TOLWORTHI CRY9C ANTHROPOD PHEROMONES ...... 180.1124 PROTEIN AND THE GENETIC MA- ARSANILIC ACID [(4- TERIAL NECESSARY FOR ITS AMINOPHENYL) ARSONIC ACID] 180.550 PRODUCTION IN CORN ...... 180.1192 ASPERGILLUS FLAVUS AF36 ...... 180.1206 BACILLUS SUBTILIS VAR. ASPERGILLUS FLAVUS NRRL AMYLOLIQUEFACIENS STRAIN 21882 ON PEANUT ...... 180.1254 FZB24 ...... 180.1243 ASULAM ...... 180.360 BEAUVERIA BASSIANA ATCC ATRAZINE ...... 180.220 #74040 ...... 180.1205 AUXINS ...... 180.1158 BEAUVERIA BASSIANA STRAIN AVERMECTIN B1 AND ITS DELTA- GHA ...... 180.1146 8,9-ISOMER ...... 180.449 BENOMYL ...... 180.294 AZADIRACHTIN ...... 180.1119 AZOXYSTROBIN ...... 180.507 BENOXACOR ...... 180.460 BACILLUS CEREUS STRAIN BP01 ... 180.1181 BENSULFURON METHYL ESTER .... 180.445 BACILLUS MYCOIDES ISOLATE J BENTAZON ...... 180.355 ON SUGAR BEETS ...... 180.1269 Benthiavalicarb-isopropyl ...... 180.618 BACILLUS POPILLIAE, VIABLE 6-BENZYLADENINE ...... 180.1150 SPORES ...... 180.1076 BETA-([1,1′-BIPHENYL]-4-YLOXY)- BACILLUS PUMILUS GB 34 ...... 180.1224 ALPHA-(1,1-DIMETHYLETHYL)-1H- BACILLUS PUMILUS STRAIN QST 1,2,4-TRIAZOLE-1-ETHANOL ...... 180.457 2808 ...... 180.1255 BIFENTHRIN ...... 180.442 BACILLUS SPHAERICUS ...... 180.1202 BIFENAZATE ...... 180.572 BACILLUS SUBTILIS STRAIN QST BIOCHEMICAL PESTICIDE PLANT 713 ...... 180.1209 FLORAL VOLATILE ATTRACTANT BACILLUS SUBTILLIS GB03 ...... 180.1111 COMPOUNDS: BACILLUS SUBTILLIS MBI 600 ...... 180.1128 CINNAMALDEHYDE, CINNAMYL BACILLUS THURINGIENSIS BER- ALCOHOL, 4-METHOXY LINER, VIABLE SPORES ...... 180.1011 CINNAMALDEHYDE, 3-PHENYL BACILLUS THURINGIENSIS PROPANOL, 4-METHOXY CRYIA(b) DELTA-ENDOTOXIN PHENETHYL ALCOHOL, INDOLE, AND THE GENETIC MATERIAL AND 1,2,4-TRIMETHOXY BEN- NECESSARY FOR ITS PRODUC- ZENE ...... 180.1127 TION IN ALL PLANT ...... 180.1173 BACILLUS THURINGIENSIS 1,1-BIS(P-CHLOROPHENYL)-2,2,2- CRY2Ab2 PROTEIN AND THE GE- TRICHLOROETHANOL ...... 180.163 NETIC MATERIAL NECESSARY BISPYRIBAC-SODIUM ...... 180.577 FOR ITS PRODUCTION IN CORN OR COTTON ...... 180.1215

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ALPHABETICAL LISTING OF PESTICIDE ALPHABETICAL LISTING OF PESTICIDE CHEMICALS—Continued CHEMICALS—Continued

Name Section Section Number Name Number

BORIC ACID AND ITS SALTS, CLODINAFOP-PROPARGYL ...... 180.559 BORAX (SODIUM BORATE DECA- CLOFENCET ...... 180.497 HYDRATE), DISODIUM CLOFENTEZINE ...... 180.446 OCTABORATE TETRAHYDRATE, CLOPYRALID ...... 180.431 BORIC OXIDE (BORIC ANHY- CLOQUINTOCET-METHYL ...... 180.560 DRIDE), SODIUM BORATE, AND COAT PROTEIN OF CUCUMBER SODIUM METABORATE ...... 180.1121 MOSAIC VIRUS AND THE GE- BOSCALID ...... 180.589 NETIC MATERIAL NECESSARY BROMACIL ...... 180.210 FOR ITS PRODUCTION ...... 180.1186 BROMIDE ION AND RESIDUAL COAT PROTEIN OF PAPAYA BROMINE ...... 180.519 RINGSPOT VIRUS AND THE GE- BROMOXYNIL ...... 180.324 NETIC MATERIAL NECESSARY BUPROFEZIN ...... 180.511 FOR ITS PRODUCTION ...... 180.1185 BUTAFENACIL ...... 180.592 COAT PROTEIN OF POTATO VIRUS N-BUTYL-N-ETHYL-A,A,A- Y AND THE GENETIC MATERIAL TRIFLUORO-2,6-DINITRO-P-TOLU- NECESSARY FOR ITS PRODUC- IDINE ...... 180.208 TION ...... 180.1182 CACODYLIC ACID ...... 180.311 COAT PROTEIN OF WATERMELON CADUSAFOS ...... 180.461 MOSAIC VIRUS-2 AND ZUCCHINI CALCIUM HYPOCHLORITE ...... 180.1054 YELLOW MOSAIC VIRUS AND CANDIDA OLEOPHILA ISOLATE I- THE GENETIC MATERIAL NEC- 182 ...... 180.1144 ESSARY FOR ITS PRODUCTION 180.1184 CAPSAICIN ...... 180.1165 CODLURE, (E,E)-8,10- CAPTAN ...... 180.103 DODECADIEN-1-01 ...... 180.1126 3-CARBAMYL-2,4,5- CONIOTHYRIUM MINITANS STRAIN TRICHLORBENZOIC ACID ...... 180.1110 CON/M/91-08 ...... 180.1213 CARBARYL ...... 180.169 COORDINATION PRODUCT OF CARBARYL (1-NAPHTHYL N- ZINC ION AND MANEB ...... 180.319 METHYLCARBAMATE AND ITS METABOLITE 1-NAPHTHOL, CAL- COPPER ...... 180.538 CULATED AS CARBARYL ...... 180.319 ...... 180.1021 CARBOFURAN ...... 180.254 COPPER CARBONATE, BASIC ...... 180.136 CARBON DIOXIDE ...... 180.1049 COUMAPHOS ...... 180.189 CARBON DISULFIDE ...... 180.467 CRYIA(C) AND CRYIC DERIVED ...... 180.1005 DELTA-ENDOTOXINS OF BACIL- ...... 180.156 LUS THURINGIENSIS VAR. CARBOXIN ...... 180.301 KURSTAKI ENCAPSULATED IN CARFENTRAZONE-ETHYL ...... 180.515 KILLED PSEUDOMONAS CHLORANTRANILIPROLE ...... 180.628 FLUORESCENS, AND THE EX- CHLORFENAPYR ...... 180.513 PRESSION PLASMID AND ...... 180.285 CLONING VECTOR GENETIC CHLORIMURON ETHYL ...... 180.429 CONSTRUCTS ...... 180.1154 CHLORINE GAS ...... 180.1095 CYANO(3- 2-CHLORO-N- PHENOXYPHENYL)METHYL-4- ISOPROPYLACETANILIDE ...... 180.211 CHLORO-A-(1-METHYLETHYL) CHLORONEB ...... 180.257 BENZENACETATE ...... 180.379 P-CHLOROPHENOXYACETIC ACID 180.202 CYAZOFAMID ...... 180.601 BETA-(4-CHLOROPHENOXY)- CYCLANILIDE ...... 180.506 ALPHA-(1,1-DIMETHYLETHYL)-1H- CYFLUTHRIN ...... 180.436 1,2,4-TRIAZOLE-1-1-ETHANOL ..... 180.450 CYHALOFOP-BUTYL ...... 180.576 1-(4-CHLOROPHENOXY)-3,3- CYHEXATIN ...... 180.144 DIMETHYL- (1H-1,2,4-TRIAZOL-1- CYMOXANIL ...... 180.503 YL)-2-BUTANONE ...... 180.410 CYPERMETHRIN AND AN ISOMER 2-(M- ZETA-CYPERMETHRIN ...... 180.418 CHLOROPHENOXY)PROPIONIC CYPROCONAZOLE ...... 180.485 ACID ...... 180.325 CYPRODINIL ...... 180.532 CHLOROTHALONIL ...... 180.275 CYROMAZINE ...... 180.414 CHLOROPYRIFOS ...... 180.342 CYTOKININS ...... 180.1157 CHLORPYRIFOS-METHYL ...... 180.419 2,4-D ...... 180.142 CHLORSULFURON ...... 180.405 DAMINOZIDE ...... 180.246 CINNAMALEDHYDE ...... 180.1156 DECANOIC ACID ...... 180.1225 CIPC ...... 180.181 (Z)-9-DEDECENYL ACETATE AND CITRONELLOL ...... 180.1248 (Z)-11-TETRADECENYL ACETATE CLARIFIED HYDROPHOBIC EX- (GBM-ROPE) ...... 180.1097 TRACT OF NEEM OIL ...... 180.1161 DELTA ENDOTOXIN OF BACILLUS CLOMAZONE ...... 180.425 THURINGIENSIS VARIETY CLORANSULAM-METHYL ...... 180.514 KURSTAKI ENCAPSULATED INTO CLOTHIANIDIN ...... 180.586 KILLED PSEUDOMONAS CLETHODIM ...... 180.458 FLUORESCENS ...... 180.1107

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DELTA ENDOTOXIN OF BACILLUS DIMETHYL PHOSPHATE OF 3-HY- THURINGIENSIS VARIETY SAN DROXY-N,N-DIMETHYL CIS- DIEGO ENCAPSULATED INTO CROTONAMIDE ...... 180.299 KILLED PSEUDOMONAS DIMETHYL PHOSPHATE OF 3-HY- FLUORESCENS ...... 180.1108 DROXY-N-METHYL-CIS- DELTAMETHRIN ...... 180.435 CROTONAMIDE ...... 180.296 DESMEDIPHAM ...... 180.353 DIMETHYL DIALLYL SULFIDES ...... 180.1228 TETRACHLOROTEREPHTHALATE 180.185 DICHLORMID ...... 180.469 DIMETHYLFORMAMIDE ...... 180.1046 DIMETHYL SULFOXIDE ...... 180.1083 DIATOMACEOUS EARTH ...... 180.1017 2,6-DIMETHYL-4- DIAZINON ...... 180.153 TRIDECYLMORPHOLINE ...... 180.372 DICAMBA ...... 180.227 2,4-DINITRO-6-OCTYLPHENYL CRO- DICHLOBENIL ...... 180.231 TONATE AND 2,6-DINITRO-4- 4-(DICHLOROACETYL)-1-OXA-4- OCTYLPHENYL CROTONATE ...... 180.341 AZASPIRO[4.5]DECANE ...... 180.465 DINOTEFURAN ...... 180.603 3,5-DICHLORO-N-(1,1-DIMETHYL-2- DIPHENYLAMINE ...... 180.190 PROPYNYL) BENZAMINE ...... 180.317 DIPROPETRYN ...... 180.329 4-(2,4-DICHLOROPHENOXY) BU- DIQUAT ...... 180.226 TYRIC ACID ...... 180.331 DITHIANON ...... 180.621 DICHLORVOS ...... 180.235 DIURON ...... 180.106 DICLOFOP-METHYL ...... 180.385 DODINE ...... 180.172 DICLOSULAM ...... 180.543 EGG SOLIDS (WHOLE) ...... 180.1071 O,O-DIETHYL S-(2- EMAMECTIN ...... 180.505 (ETHYLTHIO)ETHYL ENDOSULFAN ...... 180.182 PHOSPHORODITHIOATE ...... 180.183 ENDOTHALL ...... 180.293 ENDOTHALL (7-OXABICYCLO-(2,2,1) N,N-DIETHYL-2-(4- HEPTANE 2,3-DICARBOXYLIC METHYLBENZYLOX- ACID) ...... 180.319 Y)ETHYLAMINE HYDRO- CP4 ENOLPYRUVYLSHIKIMATE-3- CHLORIDE ...... 180.558 PHOSPHATE (CP4 EPSPS) AND N,N-DIETHYL-2-(1- THE GENETIC MATERIAL NEC- NAPHTHALENYLOX- ESSARY FOR ITS PRODUCTION Y)PROPIONAMIDE ...... 180.328 IN ALL PLANTS ...... 180.1174 DIFENOCONAZOLE ...... 180.475 Epoxiconazole ...... 180.619 DIFENZOQUAT ...... 180.369 ESFENVALERATE ...... 180.533 DIFLUFENZOPYR ...... 180.549 ETHABOXAM ...... 180.622 DIFLUBENZURON ...... 180.377 ETHALFLURALIN ...... 180.416 DIHYDROAZADIRACHTIN ...... 180.1169 ETHAMETSULFURON-METHYL ...... 180.563 2-[4,5-DIHYDRO-4-METHYL-4(1- ETHEPHON ...... 180.300 METHYLETHYL)-5-OXO-1H- ETHION ...... 180.173 IMIDAZOL-2-YL]-3-QUINOLINE ETHOPROP ...... 180.262 CARBOXYLIC ACID ...... 180.426 ETHOFUMESATE ...... 180.345 2,6-DIISOPROPYLNAPHTHALENE ETHOXYQUIN ...... 180.178 (2,6-DIPN)180.590. 5-ETHOXY-3-TRICHLOROMETHYL- S-(O,O-DIISOPROPYL 1,2,4-THIADIAZOLE ...... 180.370 PHOSPHORODITHIOATE) OF N- S-ETHYL (2-MERCAPTOETHYL) CYCLOHEXYLETHYLTHIOCARBA- BENZENESULFONAMIDE ...... 180.241 MATE ...... 180.212 DIMETHENAMID ...... 180.464 S-ETHYL DIISOBUTYLTHIOCARBAMATE .... 180.232 DIMETHIPIN ...... 180.406 S-ETHYL DIMETHOATE INCLUDING ITS OXY- DIPROPYLTHIOCARBAMATE ...... 180.117 GEN ANALOG ...... 180.204 S-ETHYL HEXAHYDRO-1H- DIMETHOMORPH ...... 180.493 AZEPINE-1-CARBOTHIOATE ...... 180.228 2,2-DIMETHYL-1,3-BENZODIOXOL-4- O-ETHYL S-PHENYL OL METHYLCARBAMATE ...... 180.530 ETHYLPHOSPHONODITHIOATE ... 180.221 O,O-DIMETHYL S-[4-OXO-1,2,3- ETHYLENE ...... 180.1016 BENZOTRIAZIN-3 (4H)- ETHYLENE GLYCOL ...... 180.1040 YLMETHY- ETHYLENE OXIDE ...... 180.151 L]PHOSPHORODITHIOATE ...... 180.531 S-(2-(ETHYLSULFINYL)ETHYL) O,O- O-[2-(1,1-DIMETHYLETHYL)-5- DIMETHYL PHOSPHOROTHIOATE 180.330 PYRIMIDNYL] O-EThYL-O-(1- ETOFENPROX ...... 180.620 METHYLETHY- ETOXAZOLE ...... 180.593 L)PHOSPHOROTHIOATE ...... 180.483 EXEMPTIONS FROM THE RE- 1,4-DIMETHYLNAPHTHALENE ...... 180.1142 QUIREMENT OF A TOLERANCE .. 180.900 O,O-DIMETHYL S-[(4-OXO-1,2,3- FAMOXADONE ...... 180.587 BENZOTRIAZIN-3(4H)- C8, C10, and C12 FATTY ACID YL)METHYL] MONOESTERS OF GLYCEROL PHOSPHORODITHIOATE ...... 180.154 AND PROPYLENE GLYCOL ...... 180.1250

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F.D.&C. BLUE NO. 1 ...... 180.1074 GLUFOSINATE AMMONIUM ...... 180.473 FENAMIDONE ...... 180.579 GLUTAMIC ACID ...... 180.1187 FENAMIPHOS ...... 180.349 GLYPHOSATE ...... 180.364 FENARIMOL ...... 180.421 GLYPHOSATE OXIDOREDUCTASE FENBUCONAZOLE ...... 180.480 [GOX OR GOXV247] AND THE FENHEXAMID ...... 180.553 GENETIC MATERIAL NECESSARY FENITROTHION ...... 180.540 FOR ITS PRODUCTION ...... 180.1190 FENOXAPROP-ETHYL ...... 180.430 GOSSYPLURE ...... 180.1043 FENPROPATHRIN ...... 180.466 HALOSULFURON-METHYL ...... 180.479 FENPROPIMORPH ...... 180.616 HARPIN PROTEIN ...... 180.1204 FENPYROXIMATE ...... 180.566 (Z)-11-HEXADECENAL ...... 180.1069 FENTHION ...... 180.214 HEXAKIS(2-METHYL-2- FERBAM ...... 180.114 PHENYLPROPYL)DISTANNOXANE 180.362 FERRIC PHOSPHATE ...... 180.1191 HEXAZINONE ...... 180.396 FERROUS SULFATE ...... 180.1230 HEXYTHIAZOX ...... 180.448 FIPRONIL ...... 180.517 HYDROGEN CYANIDE ...... 180.130 FLONICAMID ...... 180.613 HYDROGEN PEROXIDE ...... 180.1197 FLUAZIFOP-BUTYL ...... 180.411 HYDROPRENE ...... 180.501 FLUAZINAM ...... 180.574 HYGROMYCIN B FLUCARBAZONE-SODIUM ...... 180.562 PHOSPHOTRANSFERASE (APH4) FLUDIOXONIL ...... 180.516 MARKER PROTEIN AND THE GE- FLUFENOXURON ...... 180.623 FLUFENPYR-ETHYL ...... 180.595 NETIC MATERIAL NECESSARY FLUMETSULAM ...... 180.468 FOR ITS PRODUCTION IN ALL FLUMICLORAC PENTYL ...... 180.477 PLANTS ...... 180.1249 FLUMIOXAZIN ...... 180.568 IMAZALIL ...... 180.413 FLUODMETURON ...... 180.229 IMAZAMOX ...... 180.1223 FLUOPICOLIDE ...... 180.627 IMAZAPIC-AMMONIUM ...... 180.490 FLUORINE COMPOUNDS ...... 180.145 IMAZAPYR ...... 180.500 N-(4-FLUOROPHENYL)-N-(1- IMAZETHAPYR ...... 180.447 METHYLETHYL)-2-[[5- IMIDACLOPRID ...... 180.472 TRIFLUOROMETHYL)-1,3,4- INCLUSION BODIES OF THE MULTI- THIADIAZOL-2- NUCLEAR POLYHEDROSIS YL]OXY]ACETAMIDE ...... 180.527 VIRUS OF ANAGRAPH FLUOXASTROBIN ...... 180.609 FALCIFERA ...... 180.1149 FLURIDONE ...... 180.420 INDIAN MEAL MOTH GRANULOSIS FLUROXYPYR 1-METHYLHEPTYL VIRUS ...... 180.1218 ESTER ...... 180.535 INDOXACARB ...... 180.564 FLUTHIACET-METHYL ...... 180.551 INERT INGREDIENTS APPLIED TO FLUTOLANIL (N-(3-(1- ANIMALS ...... 180.930 METHYLETHOXY)PHENYL)-2- INERT INGREDITENTS OF (TRIFLUOROMETHY- SEMIOCHEMICAL DISPENSERS .. 180.1122 L)BENZAMIDE) ...... 180.484 INERT INGREDIENTS USED PRE- FLUVALINATE ...... 180.427 AND POST-HARVEST ...... 180.910 FOOD-CONTACT SURFACE SANI- INERT INGREDIENTS USED PRE- TIZING SOLUTIONS ...... 180.940 HARVEST ...... 180.920 FOLPET ...... 180.191 INORGANIC BROMIDE RESIDUES FORAMSULFURON ...... 180.1219 IN PEANUT HAY AND PEANUT FORCHLORFENURON ...... 180.569 HULLS ...... 180.123A FORMETANATE HYDROCHLORIDE 180.276 INORGANIC BROMIDE RESIDUES FORMIC ACID ...... 180.1178 RESULTING FROM FUMIGATION FOSTHIAZATE ...... 180.596 WITH METHYL BROMIDE ...... 180.123 FUMIGANTS FOR GRAIN MILL MA- INTERIM TOLERANCES ...... 180.319 CHINERY ...... 180.521 IODINE-DETERGENT COMPLEX ...... 180.1022 FUMIGANTS FOR PROCESSED IODOSULFURON-METHYL-SODIUM 180.580 GRAINS USED IN PRODUCTION IPRODIONE ...... 180.399 OF FERMENTED MALT BEV- IPROVALICARB ...... 180.581 ERAGES ...... 180.522 ISOMATE-C ...... 180.1103 FURILAZOLE ...... 180.471 ISOMATE-M ...... 180.1073 GAMMA AMINOBUTYRIC ACID ...... 180.1188 ISOPROPYL M- GERANIOL ...... 180.1251 CHLOROCARBANILATE (CIPC) .... 180.319 GIBBERELLINS (GA3) ...... 180.1098 ISOPROPYL CARBANILATE (IPC) .... 180.319 GLIOCLADIUM CATENULATUM ISOXAFLUTOLE ...... 180.537 STRAIN J1446 ...... 180.1198 JOJOBA OIL ...... 180.1160 GLIOCLADIUM VIRENS GL-21 ...... 180.1100 KAOLIN ...... 180.1180 B-D-GLUCURONIDASE FROM E. KILLED MYROTHECIUM COLI AND THE GENETIC MATE- VERRUCARIA ...... 180.1163 RIAL NECESSARY FOR ITS PRO- KONTROL H.V...... 180.1063 DUCTION AS A PLANT-PES- KRESOXIM-METHYL ...... 180.554 TICIDE INERT INGREDIENT ...... 180.1216 KASUGAMYCIN ...... 180.614

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LACTIC ACID ...... 180.1090 N-1-NAPHTHYL PHTHALAMIC ACID 180.297 LACTOFEN ...... 180.432 NEOMYCIN LAGENIDIUM GIGANTEUM ...... 180.1113 PHOSPHOTRANSFERASE II AND LAMBDA-CYHALOTHRIN ...... 180.438 THE GENETIC MATERIAL NEC- LEPIDOPTERAN PHEROMONES ...... 180.1153 ESSARY FOR ITS PRODUCTION 180.1134 LIME ...... 180.1231 NICOSULFURON [3- D-LIMONENE ...... 180.539 PYRIDINECARBOXAMIDE, 2- LIME-SULFUR ...... 180.1232 ((((4,6-DIMETHOXYPYRIMIDIN-2- LINDANE ...... 180.133 YL)AMINOCARBONYL) LINURON ...... 180.184 AMINOSULFONYL))-N, N-DI- LINSEED OIL, BOILED ...... 180.1056 METHYL] ...... 180.454 LYSOPHOSPHATIDYLETHANOLAMI- NICOTINE-CONTAINING COM- NE (LPE) ...... 180.1199 POUNDS ...... 180.167 MALATHION ...... 180.111 NITROGEN ...... 180.1050 MALEIC HYDRAZIDE ...... 180.175 NORFLURAZON ...... 180.356 MANCOZEB ...... 180.176 MANEB ...... 180.110 NOSEMA LOCUSTAE ...... 180.1041 MCPA ...... 180.339 NOVALURON ...... 180.598 MEFENOXAM ...... 180.546 NUCLEAR POLYHEDROSIS VIRUS MEFENPYR-DIETHYL ...... 180.509 OF HELIOTHIS ZEA ...... 180.1027 MENTHOL ...... 180.1092 OCCULSION BODIES OF THE MEPANIPYRIM ...... 180.604 GRANULOSIS VIRUS OF CYDIA MEPIQUAT (N,N- POMENELLA ...... 180.1148 DIMETHYLPIPERIDINIUM) ...... 180.384 N-OCTYL N-(MERCAPTOMETHYL) PHTHAL- BICYCLOHEPTENEDICARBOXIMI- IMIDE S-(O,O-DIMETHYL DE ...... 180.367 PHOSPHORODITHIOATE) AND N-(N-OCTYL)-2-PYRROLIDONE AND ITS OXYGEN ANALOG ...... 180.261 N-(N-DODECYL)-2-PYRROLIDONE 180.1130 MESOSULFURON-METHYL ...... 180.597 ORTHOARSENIC ACID ...... 180.180 METALAXYL ...... 180.408 ORTHOSULFAMURON ...... 180.625 METALDEHYDE ...... 180.523 ORYZALIN ...... 180.304 METARHIZIUM ANISOPLIAE STRAIN OXADIXYL ...... 180.456 ESF1 ...... 180.1116 OXAMYL ...... 180.303 METHAMIDOPHOS ...... 180.315 OXYFLUORFEN ...... 180.381 METHANEARSONIC ACID ...... 180.289 OXYTETRACYCLINE ...... 180.337 METHIDATHION ...... 180.298 PAECILOMYCES LILACINUS METHOMYL ...... 180.253 STRAIN 251; ...... 180.1257 METHOPRENE ...... 180.1033 PANTOEA AGGLOMERANS STRAIN METHOXYFENOZIDE ...... 180.544 C9-1 ...... 180.1267 METHYL ANTHRANILATE ...... 180.1143 PARAQUAT ...... 180.205 4-(2-METHYL-4-CHLOROPHENOXY) PARASITIC (PARASITOID) AND BUTYRIC ACID ...... 180.318 PREDATORY INSECTS ...... 180.1101 1-METHYLCYCLOPROPENE ...... 180.1220 PARATHION ...... 180.122 METHYL 3- PARATHION (O,O,DIETHYL-O-P- ((DIMETHOXYPHOSPHINYL)OXY) NITROPHENYLTHIOPHOSPHATE) BUTENOATE, A AND B ISOMERS 180.157 OR ITS METHYL HOMOLOG ...... 180.319 METHYL EUGENOL/MALATHION PASTEURIA PENETRANS ...... 180.1135 COMBINATION ...... 180.1067 PELARGONIC ACID ...... 180.1159 METHYL 2-(4-ISOPROPYL-4-METH- PENDIMETHALIN ...... 180.361 YL-5-OXO-2-IMIDAZOLIN-2-YL)-P- PENOXSULAM ...... 180.605 TOLUATE AND METHYL 6-(4-ISO- PENTACHLORONITROBENZENE ..... 180.291 PROPYL-4-METHYL-5-OXO-2- IMIDAZOLIN-2-YL)-M-TOLUATE .... 180.437 PENTACHLORONITROBENZENE ..... 180.319 METHYL PARATHION ...... 180.121 PENTANE ...... 180.1014 METHYL SALICYLATE ...... 180.1189 PERMETHRIN ...... 180.378 METOLACHLOR ...... 180.368 PEROXYACETIC ACID ...... 180.1196 METRAFENONE ...... 180.624 PESTICIDE CHEMICALS ...... 180.905 METRIBUZIN ...... 180.332 PHENMEDIPHAM ...... 180.278 METSULFURON METHYL ...... 180.428 O-PHENYLPHENOL AND ITS SO- MINERAL OIL ...... 180.149 DIUM SALT ...... 180.129 MONOCARBAMIDE DIHYDROGEN PHORATE ...... 180.206 SULFATE ...... 180.1084 PHOSALONE ...... 180.263 MUSCODOR ALBUS QST 20799 PHOSPHAMIDON ...... 180.239 AND THE VOLATILES PRODUCED PHOSPHINE ...... 180.225 ON REHYDRATION ...... 180.1260 PHOSPHINOTHRICIN MYCLOBUTANIL ...... 180.443 ACETYLTRANSFERASE (PAT) NALED ...... 180.215 AND THE GENETIC MATERIAL A-NAPHTHALENEACETAMIDE ...... 180.309 NECESSARY FOR ITS PRODUC- 1-NAPHTHALENEACETIC ACID ...... 180.155 TION ALL PLANTS ...... 180.1151

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Section Section Name Number Name Number

PHOSPHOMANNOSE ISOMERASE PSEUDOMONAS CHLORORAPHIS AND THE GENETIC MATERIAL STRAIN 63-28 ...... 180.1212 NECESSARY FOR ITS PRODUC- PSEUDOMONAS FLUORESCENS TION IN ALL PLANTS ...... 180.1252 A506, 1629RS, 742RS ...... 180.1114 PHOSPHOROUS ACID ...... 180.1210 PSEUDOMONAS FLUORESCENS E- PHOSPHOROTHIOIC ACID, O,O- 1053 ...... 180.1088 DIETHYL O-(1,2,2,2- PSEUDOMONAS FLUORESCENS TETRACHLOROETHYL)ESTER ..... 180.486 STRAIN PRA-25 ...... 180.1200 PHYTOPHTHORA PALMIVORA ...... 180.1057 PSEUDOMONAS FLUORESCENS PICLORAM ...... 180.292 STRAIN NCIB 12089 ...... 180.1129 PINE OIL ...... 180.1035 PSEUDOMONAS SYRINGAE ...... 180.1145 PINOXADEN ...... 180.611 PSEUDOZYMA FLOCCULOSA PIPERONYL BUTOXIDE ...... 180.127 STRAIN PF-A22 UL ...... 180.1221 PIRIMIPHOS-METHYL ...... 180.409 PUCCINIA CANALICULATA (ATCC PLANT EXTRACT DERIVED FROM 40199) ...... 180.1123 OPUNTIA LINDHEIMERI, PYMETROZINE ...... 180.556 QUERCUS FALCATA, RHUS PYRACLOSTROBIN ...... 180.582 AROMATICA, AND RHIZOPHORIA PYRAFLUFEN-ETHYL ...... 180.585 MANGLE ...... 180.1179 PYRAZON ...... 180.316 PLANT VOLATILES/PHEROMONE .... 180.1080 PYRETHRINS ...... 180.128 POLY-N-ACETYL-D-GLUCOSAMINE 180.1089 PYRIDABEN ...... 180.494 POLYBUTENES ...... 180.1037 PYRIDATE ...... 180.462 POLY-D-GLUCOSAMINE ...... 180.1072 PYRIMETHANIL ...... 180.518 POLYHEDRAL OCCLUSION BODIES PYRITHIOBAC SODIUM ...... 180.487 OF AUTOGRAPHA CALIFORNICA PYRIPOXYFEN ...... 180.510 NUCLEAR POLYHEDROSIS QUINCLORAC ...... 180.463 VIRUS ...... 180.1125 QUINOXYFEN ...... 180.588 POLYMERS. QUIZALOFOP-ETHYL ...... 180.441 POLY(VINYLPYRROLIDONE/1- RESMETHRIN ...... 180.525 EICOSENE) ...... 180.1104 REYNOUTRIA SACHALINENSIS EX- POLY(VINYLPYRROLIDONE/1- TRACT ...... 180.1259 HEXADECENE) ...... 180.1105 RIMSULFURON ...... 180.478 POTASSIUM BICARBONATE ...... 180.1177 RHAMNOLIPID BIOSURFACTANT .... 180.1245 POTASSIUM DIHYDROGEN PHOS- SETHOXYDIM ...... 180.412 PHATE ...... 180.1193 SIMAZINE (2-CHLORO-4,6- POTASSIUM OLEATE AND RE- BIS(ETHYLAMINO)-S-TRIAZINE) ... 180.213 LATED C12-C18 FATTY ACID PO- SODIUM BICARBONATE ...... 180.1176 TASSIUM SALTS ...... 180.1068 SODIUM CARBONATE ...... 180.1234 POTASSIUM SILICATE ...... 180.1268 SODIUM CHLORATE ...... 180.1020 POTASSIUM SORBATE ...... 180.1233 SODIUM CHLORITE ...... 180.1070 POTATO LEAF ROLL VIRUS RE- SODIUM DIACETATE ...... 180.1058 SISTANCE GENE (ALSO KNOWN SODIUM HYPOCHLORITE ...... 180.1235 AS ORF1/ORF2 GENE) AND THE SODIUM METASILICATE ...... 180.1237 GENETIC MATERIAL NECESSARY SODIUM 5-NITROGUAIACOLATE ..... 180.1139 FOR IT’S PRODUCTION ...... 180.1183 SODIUM O-NITROPHENOLATE ...... 180.1140 PRALLETHRIN (RS)-2-METHYL-4- SODIUM P-NITROPHENOLATE ...... 180.1141 OXO-3-(2- SODIUM SALT OF ACIFLUORFEN ... 180.383 PROPYNYL)CYCLOPENT-2-ENYL SODIUM SALT OF FOMESAFEN ...... 180.433 (1RS)-CIS, TRANS- SORBITOL OCTANOATE ...... 180.1262 CHRYSANTHEMATE ...... 180.545 SPINOSAD ...... 180.495 PRIMISULFURON-METHYL ...... 180.452 SPIRODICLOFEN ...... 180.608 PROCYMIDONE ...... 180.455 SPIROMESIFEN ...... 180.607 PROFENOFOS ...... 180.404 SPIROXAMINE ...... 180.602 PROHEXADIONE CALCIUM ...... 180.547 SPODOPTERA EXIGUA NUCLEAR PROMETRYN ...... 180.222 POLYHEDROSIS VIRUS ...... 180.1118 PROPAMOCARB ...... 180.499 STREPTOMYCES LYDICUS WYEC PROPANIL ...... 180.274 108 ...... 180.1253 PROPARGITE ...... 180.259 STREPTOMYCES SP. STRAIN K61 .. 180.1120 PROPAZINE ...... 180.243 STREPTOMYCIN ...... 180.245 PROPETAMPHOS ...... 180.541 SUCROSE OCTANOATE ESTERS .... 180.1222 PROPICONAZOLE ...... 180.434 SULFENTRAZONE ...... 180.498 PROPIONIC ACID ...... 180.1023 SULFOSATE (SULFONIUM, PROPOXYCARBAZONE ...... 180.600 TRIMETHYL-SALT WITH N- S-PROPYL (PHOSPHONOMETHYL)GLYCINE BUTYLETHYLTHIOCARBAMATE ... 180.238 (1:1)) ...... 180.489 PROPYLENE OXIDE ...... 180.491 SULFOSULFURON ...... 180.552 PROPYZAMIDE ...... 180.317 SULFUR ...... 180.1236 PROSULFURON ...... 180.481 SULFUR DIOXIDE ...... 180.444, PROTHIOCONAZOLE ...... 180.626 SULFURIC ACID ...... 180.1019

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ALPHABETICAL LISTING OF PESTICIDE ALPHABETICAL LISTING OF PESTICIDE CHEMICALS—Continued CHEMICALS—Continued

Name Section Section Number Name Number

SULFURYL FLUORIDE ...... 180.575 3,7,11-TRIMETHYL-1,6,10- SULPROFOS ...... 180.542 DODECATRIENE-1-OL AND SYNTHETIC ISOPARAFFINIC PE- 3,7,11-TRIMETHYL-2,6,10- TROLEUM HYDROCARBONS ...... 180.526 DODECATRIENE-3-OL ...... 180.1086 TEBUTHIURON ...... 180.390 TRIPHENYLTIN HYDROXIDE ...... 180.236 TEFLUTHRIN ...... 180.440 TRISULFURON ...... 180.459 TERBACIL ...... 180.209 TRITICONAZOLE ...... 180.583 TEBUCONAZOLE ...... 180.474 VINCLOZOLIN ...... 180.380 TEBUFENOZIDE ...... 180.482 XANTHOMONAS CAMPESTRIS PV. TEPRALOXYDIM ...... 180.573 VESICATORIA AND TERBUFOS ...... 180.352 PSEUDOMONAS SYRINGAE PV. TETRACHLOVINPHOS ...... 180.252 TOMATO SPECIFIC 1,2,4,5-TETRACHLORO-3- BACTERIOPHAGES ...... 180.1261 NITROBENZENE ...... 180.203 XYLENE ...... 180.1025 TETRACONAZOLE ...... 180.557 YEAST EXTRACT HYDROLYSATE TETRAHYDRO-5,5-DIMETHYL-2(1H)- FROM SACCHAROMYCES PYRIMIDINONE (3-(4-TRIFLUOR CEREVISIAE ...... 180.1246 OMETHYL)PHENYL)-1-(2-4- ZINC PHOSPHIDE ...... 180.284 (TRIFLUOROMETHYL)PHENYL) ZIRAM ...... 180.116 ETHENYL)2-PROPENYLIDENE) ZOXAMIDE ...... 180.567 HYDRAZONE ...... 180.395 THIABENDAZOLE ...... 180.242 NOTE: The Alphabetical Listing of Pesticide Chemi- THIACLOPRID ...... 180.594 cals is a finding aid intended for the convenience of THIAMETHOXAM ...... 180.565 the reader. This list is compiled and kept up to date THIAZOPYR ...... 180.498 by the Environmental Protection Agency and is re- THIDIAZURON ...... 180.403 vised through July 1, 2007. THIFENSULFURON METHYL ...... 180.439 THIOBENCARB ...... 180.401 GLOSSARY 2-(THIOCYANOMETHYLTHIO) BENZOTHIAZOLE ...... 180.288 NOTE: The items in this glossary were com- THIODICARB ...... 180.407 piled as an aid to the users of the Code of THIOPHANATE-METHYL ...... 180.371 Federal Regulations. Inclusion or exclusion THIRAM ...... 180.132 from this glossary has no legal significance. THYMOL ...... 180.1240 APPLI = APPLICATION TITANIUM DIOXIDE ...... 180.1195 TOBACCO MILD GREEN MOSAIC C-I MET = CHOLINESTERASE-INHIBITING TOBAMOVIRUS (TMGMV) ...... 180.1276 METABOLITES TOLERANCE EXEMPTIONS FOR CARB = MINIMAL RISK ACTIVE AND EPWRR = EDIBLE PORTION WITH RIND INERT INGREDIENTS ...... 180.950 REMOVED TOLYLFLUANID ...... 180.584 TOMATO PINWORM INSECT EXC = EXCEPT PHEROMONE ...... 180.1064 I (IN PPM COLUMN) = INTERIM TOLER- TOPRAMEZONE ...... 180.612 ANCE TRALOMETHRIN ...... 180.422 INC = INCLUDING TRALKOXYDIM ...... 180.548 K=CWHR = KERNEL PLUS COB WITH TRIASULFURON ...... 180.459 HUSK REMOVED TRIAZAMATE ...... 180.536 TRIBENURON METHYL ...... 180.451 MBYP = MEAT BYPRODUCTS TRIBUPHOS ...... 180.272 MIN = MINIMUM TRIBUTYLPHOSPHOROTRITHIOITE 180.186 N (IN PPM COLUMN) = NEGLIGIBLE RESI- S-2,3,3-TRICHLOROALLYL DUES DIISOPROPYLTHIOCARBAMATE 180.314 NMT = NOT MORE THAN TRICHLORFON ...... 180.198 TRICHODERMA HARZIANUM KRL- NON-PER BAG/PKGD RAC = NON-PERISH- AG2 (ATCC #20847) STRAIN T-22 180.1102 ABLE PACKAGED OR BAGGED RAW TRICHODERMA HARZIANUM AGRICULTURAL COMMODITY STRAIN T-39 ...... 180.1201 PPM = PART(S) PER MILLION TRICLOPYR ...... 180.417 POST-H = POSTHARVEST APPLICATION TRIFLOXYSTROBIN ...... 180.555 PRE-H = PREHARVEST APPLICATION TRIFLOXYSULFURON ...... 180.591 TRIFLUMIZOLE ...... 180.476 PRE-S = PRESLAUGHTER APPLICATION TRIFLURALIN ...... 180.207 PRODS = PRODUCTS rollert TRIFLUSULFURON METHYL ...... 180.492 T (IN PPM COLUMN) = TEMPORARY TOL- 2,2,5-TRIMETHYL-3- ERANCE DICHLOROACETYL-1,3-OXAZOLI- DINE ...... 180.1052 [41 FR 4537, Jan. 30, 1976]

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Subpart A—Definitions and within the meaning of FFDCA sections Interpretative Regulations 402 and 408(a), despite the lack of a tol- erance or exemption for the pesticide DEFINITIONS AND INTERPRETATIONS chemical residue in the processed food, if: § 180.1 Definitions and interpretations. (1) The pesticide chemical has been (a) Administrator, without qualifica- used in or on the raw agricultural com- tion, means the Administrator of the modity in conformity with a tolerance Environmental Protection Agency. under this section; (b) Agency, without qualification, (2) The pesticide chemical residue means the Environmental Protection has been removed to the extent pos- Agency. sible in good manufacturing practice; (c) FFDCA means the Federal Food, and Drug, and Cosmetic Act, as amended, (3) The concentration of the pesticide 21 U.S.C. 301–392. chemical residue in the processed food (d) Raw agricultural commodities in- is not greater than the tolerance pre- clude, among other things, fresh fruits, scribed for the pesticide chemical res- whether or not they have been washed idue on the raw agricultural com- and colored or otherwise treated in modity. their unpeeled natural form; vegetables (f) For the purpose of computing fees in their raw or natural state, whether as required by § 180.33, each group of re- or not they have been stripped of their lated crops listed in § 180.34(e) and each outer , waxed, prepared into crop group or subgroup listed in § 180.41 fresh green salads, etc.; grains, nuts, is counted as a single raw agricultural eggs, raw milk, meats, and similar ag- commodity in a petition or request for ricultural produce. It does not include tolerances or exemption from the re- foods that have been processed, fab- quirement of a tolerance. ricated, or manufactured by cooking, (g) Tolerances and exemptions estab- freezing, dehydrating, or milling. lished for pesticide chemicals in or on (e) Where a raw agricultural com- the general category of raw agricul- modity bearing a pesticide chemical tural commodities listed in column A residue that has been exempted from apply to the corresponding specific raw the requirement of a tolerance, or agricultural commodities listed in col- which is within a tolerance permitted umn B. However, a tolerance or exemp- under FFDCA section 408, is used in tion for a specific commodity in col- preparing a processed food, the proc- umn B does not apply to the general essed food will not be considered unsafe category in column A.

A B

Alfalfa ...... Medicago sativa, (alfalfa, lucerne); Onobrychio viciaefolia (sainfoin, holy clover, esparcet); and Lotus corniculatus (birdsfoot trefoil); and varieties and/or hybrids of these. Bananas ...... Bananas, plantains. Beans ...... Cicer arietinum (chick peas, garbanzo beans); Lupinus spp. (including sweet lupine, white sweet lupine, white lupine, and grain lupine). Phaseolus spp. (including kidney beans, lima beans, mung beans, navy beans, pinto beans, snap beans, and waxbeans); Vicia faba (broad beans, fava beans); Vigna spp. (including asparagus beans, blackeyed peas and cowpeas). Beans (dry) ...... All beans above in dry form only. Beans (succulent) ...... All beans above in succulent form only. Blackberries ...... Rubus eubatus (including bingleberries, black satin berries, boysenberries, Cherokee blackberries, Chesterberries, Cheyenne blackberries, coryberries, darrowberries, dewberries, Dirksen thorn- less berries, Himalayaberries, hullberries, Lavacaberries, lowberries, Lucretiaberries, mammoth blackberries, marionberries, nectarberries, olallieberries, Oregon evergreen berries, phenomenalberries, rangerberries, ravenberries, rossberries, Shawnee blackberries, and vari- eties and/or hybrids of these). Broccoli ...... Broccoli, chinese broccoli (gia lon, white flowering broccoli). Cabbage ...... Cabbage, Chinese cabbage (tight-heading varieties only). Caneberries ...... Rubus spp. (including blackberries; Rubus caesius (youngberry); Rubus loganbaccus (loganberry); Rubus occidentalis, idaeus, and strigosus (red and black raspberries); and varieties and/or hy- brids of these. ...... Celery, Florence (sweet , sweet fennel, finochio) (fresh leaves and stalks only). Cherries ...... Sour cherries, sweet cherries. Citrus fruits ...... Grapefruit, lemons, limes, oranges, tangelos, tangerines, citrus citron, kumquats, and hybrids of these. Endive ...... Endive, escarole.

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A B

Lettuce ...... Lettuce, head; and lettuce, leaf Lettuce, head ...... Lettuce, head; crisphead varieties only Lettuce, leaf ...... Lettuce, leaf; cos (romaine), butterhead varieties Marjoram ...... Origanum spp. (includes sweet or annual marjoram, wild marjoram or oregano, and pot marjoram). Melons ...... Muskmelons, including hybrids and/or varieties of Cucumis melo (including true cantaloupe, canta- loupe, casaba, Santa Claus melon, crenshaw melon, honeydew melon, honey balls, Persian melon, golden pershaw melon, mango melon, pineapple melon, snake melon); and watermelons, including hybrids and/or varieties of (Citrullus spp.). Muskmelons ...... Cucumis melo (includes true cantaloupe, cantaloupe, casaba, Santa Claus melon, crenshaw melon, honeydew melon, honey balls, Persian melon, golden pershaw melon, mango melon, pineapple melon, snake melon, and other varieties and/or hybrids of these.) Onions ...... Dry bulb onions, green onions, and garlic. Onions (dry bulbs only) ..... Garlic, onions (dry bulbs only), shallots (dry bulbs only). Onions, green ...... Green onions, leeks, spring onions or scallions, Japanese bunching onions, green shallots, or green eschalots. Oriental radish (root and Raphanus sativus var. longipinnatus (root and tops), including Chinese or Japanese radish (both tops). white and red), winter radish, daikon, lobok, lo pak, and other cultivars and/or hybrids of these. Peaches ...... Peaches, nectarines Peas ...... Cajanus cajan (includes pigeon peas); Cicer spp. (includes chick peas and garbanzo beans); Lens culinaris (lentils); Pisum spp. (includes dwarf peas, garden peas, green peas, English peas, field peas, and edible pod peas). [Note: A variety of pesticide tolerances have been previously estab- lished for peas and/or beans. Chick peas/garbanzo beans are now classified in both the bean and the pea categories. For garbanzo beans/chick peas ONLY, the highest established pea or bean tolerance will apply to pesticide residues found in this commodity.] Peas (dry) ...... All peas in dry form only. Peas (succulent) ...... All peas in succulent form only. Peppers ...... All varieties of peppers including pimentos and bell, hot, and sweet peppers. Rapeseed ...... Brassica napus, B. campestris, and Crambe abyssinica (oilseed-producing varieties only which in- clude canola and crambe.) Sorghum (grain) ...... Sorghum spp. [sorghum (grain), sudangrass (seed crop), and hybrids of these grown for its seed]. Sorghum (fodder, forage) .. Sorghum ssp. [(sorghum (fodder, forage), sudangrass, and hybrids of these grown for fodder and/ or forage)]. Squash ...... Pumpkins, summer, and winter squash. Sugar apple ...... Annona squamosa L. (sugar apple, sweetsop, anon), and its hybrid A. squamosa L.×A. cherimoya M. (atemoya). Also A. reticulata L. (true custard apple). Summer squash ...... Fruits of the gourd (Cucurbitaceae) family that are consumed when immature, 100% of the fruit is edible either cooked or raw, once picked it cannot be stored, has a soft rind which is easily pen- etrated, and if seeds were harvested they would not germinate; e.g., Cucurbita pepo (i.e., crookneck squash, straightneck squash, scallop squash, and vegetable marrow); Lagenaria spp. (i.e., spaghetti squash, hyotan, cucuzza); Luffa spp. (i.e., hechima, Chinese okra); Momordica spp. (i.e., bitter melon, balsam pear, balsam apple, Chinese cucumber); Sechium edule (chayote); and other cultivars and/or hybrids of these. Sweet potatoes ...... Sweet potatoes, yams. Tangerines ...... Tangerines (mandarins or mandarin oranges); tangelos, tangors, and other hybrids of tangerine with other citrus. Tomatoes ...... Tomatoes, tomatillos. Turnip tops or turnip Broccoli raab (raab, raab salad), hanover salad, turnip tops (turnip greens). greens. Wheat ...... Wheat, triticale.

(h) Unless otherwise specified, toler- residues, shall not include any crown ances and exemptions established tissue or stalk. under the regulations in this part (2) Shell shall be removed and dis- apply to residues from only preharvest carded from nuts before examination application of the chemical. for pesticide residues. (i) Unless otherwise specified in this (3) Caps (hulls) shall be removed and paragraph or in tolerance regulations discarded from strawberries before ex- amination for pesticide residues. prescribed in this part for specific pes- (4) Stems shall be removed and dis- ticide chemicals, the raw agricultural carded from melons before examination commodity or processed food to be ex- for pesticide residues. amined for pesticide residues, shall (5) Roots, stems, and outer sheaths consist of the whole raw agricultural (or husks) shall be removed and dis- commodity or processed food. carded from garlic bulbs and dry bulb (1) The raw agricultural commodity onions, and only the garlic cloves and bananas, when examined for pesticide onion bulbs shall be examined for pes- ticide residues.

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(6) Where a tolerance is established sensitive animal species tested. Such on a root vegetable including tops and/ toxicity studies shall usually include or with tops, and the tops and the roots at least 90-day feeding studies in two are marketed together, they shall be species of mammals. analyzed separately and neither the (l) The term nonperishable raw agri- pesticide residue on the roots nor the cultural commodity means any raw agri- pesticide residue on the tops shall ex- cultural commodity not subject to ceed the tolerance level, except that in rapid decay or deterioration that would the case of , , and ruta- render it unfit for consumption. Exam- bagas, the tops shall be removed and ples are cocoa beans, coffee beans, discarded before analyzing roots for field-dried beans, field-dried peas, pesticide residues. grains, and nuts. Not included are eggs, (7) The crowns (leaves at the top of milk, meat, poultry, fresh fruits, and the fruit) shall be removed and dis- vegetables such as onions, parsnips, po- carded from pineapples before examina- tatoes, and carrots. tion for pesticide residues. (m) The term tolerance with regional (8) The term lima beans means the registration means any tolerance which beans and the pod. is established for pesticide residues re- (9) The term peanuts means the pea- sulting from the use of the pesticide nut meat after removal of the hulls. pursuant to a regional registration. (10) For processed foods consisting primarily of one ingredient and sold in Such a tolerance is supported by res- a form requiring further preparation idue data from specific growing regions prior to consumption (e.g., fruit juice for a raw agricultural commodity. Indi- concentrates, dehydrated vegetables, vidual tolerances with regional reg- and powdered potatoes), the processed istration are designated in separate food to be examined for residues shall subsections in 40 CFR 180.101 through be the whole processed commodity 180.999, as appropriate. Additional res- after compensating for or reconsti- idue data which are representative of tuting to the commodity’s normal the proposed use area are required to moisture content, unless a tolerance expand the geographical area of usage for the concentrated or dehydrated of a pesticide on a raw agricultural food form is included in this part. If commodity having an established ‘‘tol- there exists a tolerance for a specific erance with regional registration.’’ pesticide on the processed food in its Persons seeking geographically broad- concentrated or dehydrated food form, er registration of a crop having a ‘‘tol- for the purpose of determining whether erance with regional registration’’ the food is in compliance with that tol- should contact the appropriate EPA erance, the processed food to be exam- product manager concerning additional ined for residues shall be the whole residue data required to expand the use processed commodity on an ‘‘as is’’ area. basis. (n) The term pesticide chemical residue (j) The term pesticide chemical shall shall have the meaning specified in have the meaning specified in FFDCA FFDCA section 201(q)(2), as amended, section 201(q)(1), as amended, except as except as provided in § 180.4. provided in § 180.4. (o) The term food commodity means: (k) The term negligible residue means (1) Any raw agricultural commodity any amount of a pesticide chemical re- (food or feed) as defined in section maining in or on a raw agricultural 201(r) of the Federal Food, Drug, and commodity or group of raw agricul- Cosmetic Act (FFDCA); and tural commodities that would result in (2) Any processed food or feed as de- a daily intake regarded as fined in section 201(gg) of the FFDCA. toxicologically insignificant on the basis of scientific judgment of ade- [36 FR 22540, Nov. 25, 1971] quate safety data. Ordinarily this will EDITORIAL NOTE: For FEDERAL REGISTER ci- add to the diet an amount which will tations affecting § 180.1, see the List of CFR be less than 1/2,000th of the amount Sections Affected, which appears in the that has been demonstrated to have no Finding Aids section of the printed volume effect from feeding studies on the most and on GPO Access.

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§ 180.3 Tolerances for related pesticide (d)(1) Where tolerances are estab- chemicals. lished for both calcium cyanide and hy- (a) Pesticide chemicals that cause re- drogen cyanide on the same raw agri- lated pharmacological effects will be cultural commodity, the total amount regarded, in the absence of evidence to of such pesticides shall not yield more the contrary, as having an additive del- residue than that permitted by the eterious action. (For example, many larger of the two tolerances, calculated pesticide chemicals within each of the as hydrogen cyanide. following groups have related pharma- (2) Where tolerances are established cological effects: Chlorinated organic for residues of both O,O-diethyl S-[2- pesticides, -containing chemi- (ethylthio)ethyl] phosphorodithioate cals, metallic dithiocarbamates, cho- and demeton (a mixture of O,O-diethyl linesterase-inhibiting pesticides.) O-(and S-) [2-(ethylthio)ethyl] (b) Tolerances established for such phosphorothioates) on the same raw related pesticide chemicals may limit agricultural commodity, the total the amount of a common component amount of such pesticides shall not yield more residue than that permitted (such as As2O3) that may be present, or may limit the amount of biological ac- by the larger of the two tolerances, cal- tivity (such as cholinesterase inhibi- culated as demeton. tion) that may be present, or may limit (3) Where tolerances are established the total amount of related pesticide for both terpene polychlorinates chemicals (such as chlorinated organic (chlorinated mixture of camphene, pi- pesticides) that may be present. nene, and related terpenes, containing (c)(1) Where tolerances for inorganic 65–66 percent chlorine) and bromide in or on the same raw agricul- (chlorinated camphene containing 67–69 tural commodity are set in two or percent chlorine) on the same raw agri- more sections in this part (example: cultural commodities, the total §§ 180.123 and 180.199), the overall quan- amount of such pesticides shall not tity of inorganic bromide to be toler- yield more residue than that permitted ated from use of the same pesticide in by the larger of the two tolerances, cal- different modes of application or from culated as a chlorinated terpene of mo- two or more pesticide chemicals for lecular weight 396.6 containing 67 per- which tolerances are established is the cent chlorine. highest of the separate applicable tol- (4) Where a tolerance is established erances. For example, where the bro- for more than one pesticide containing mide tolerance on asparagus from arsenic found in, or on a raw agricul- methyl bromide commodity fumigation tural commodity, the total amount of is 100 parts per million (40 CFR 180.123) such pesticide shall not exceed the and on asparagus from methyl bromide highest established tolerance cal- soil treatment is 300 parts per million culated as As2O3. (40 CFR 180.199), the overall inorganic (5) Where tolerances are established bromide tolerance for asparagus grown for more than one member of the class on methyl bromide-treated soil and of dithiocarbamates listed in para- also fumigated with methyl bromide graph (e)(3) of this section on the same after harvest is 300 parts per million. raw agricultural commodity, the total (2) Where tolerances are established residue of such pesticides shall not ex- in terms of inorganic bromide residues ceed that permitted by the highest tol- only from use of organic bromide fumi- erance established for any one member gants on raw agricutural commodities, of the class, calculated as zinc such tolerances are sufficient to pro- ethylenebisdithiocarbamate. tect the public health, and no addi- (6) Where tolerances are established tional concurrent tolerances for the or- for residues of both S,S,S-tributyl ganic pesticide chemicals from such phosphorotrithioate and tributyl use are necessary. This conclusion is phosphorotrithioite in or on the same based on evidence of the dissipation of raw agricultural commodity, the total the organic pesticide or its conversion amount of such pesticides shall not to inorganic bromide residues in the yield more residue than that permitted food when ready to eat. by the higher of the two tolerances,

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calculated as S,S,S-tributyl (13) Where tolerances are established phosphorotrithioate. for residues of both 1-(4- (7) Where tolerances are established chlorophenoxy)-3,3-dimethyl-1-(1H- for residues of a-naphthaleneacetamide 1,2,4-triazol-1-yl)-2-butanone and/or a-naphthaleneacetic acid in or (triadimefon) and beta-(4- on the same raw agricultural com- chlorophenoxy)-alpha-(1,1- modity, the total amount of such pes- dimethylethyl)-1H-1,2,4-triazole-1-eth- ticides shall not yield more residue anol (triadimenol) including its than that permitted by the higher of butanediol metabolite, 4-(4- the two tolerances, calculated as a- chlorophenoxy)-2,2-dimethyl-4-(1H- naphthaleneacetic acid. 1,2,4-triazol-1-yl)-1,3-butanediol, in or (8) Where tolerances are established on the same raw agricultural com- for residues of O,S-dimethyl modity and its products thereof, the phosphoramidothioate, resulting from total amount of such residues shall not the use of acephate (O,S-dimethyl yield more residue than that permitted acetylphos-phoramidothioate) and/or by the higher of the two tolerances. O,S - dimethylphosphoramidothioate on (14) Where tolerances are established the same agricultural commodity, the for residues of methomyl, resulting total amount of O,S-dimethyl- from the use of thiodicarb and/or phosphoramidothioate shall not yield methomyl on the same raw agricul- more residue than that permitted by tural commodity, the total amount of the higher of the two tolerances. methomyl shall not yield more residue than that permitted by the higher of (9) Where a tolerance is established the two tolerances. for more than one pesticide having the (e) Except as noted in paragraphs metabolites 1-(3,4-dichlorophenyl)-3- (e)(1) and (2) of this section, where resi- methylurea (DCPMU) and 3,4- dues from two or more chemicals in the dichlorophenylurea (DCPU) found in or same class are present in or on a raw on a raw agricultural commodity, the agricultural commodity the tolerance total amount of such residues shall not for the total of such residues shall be exceed the highest established toler- the same as that for the chemical hav- ance for a pesticide having these me- ing the lowest numerical tolerance in tabolites. this class, unless a higher tolerance (10) Where a tolerance is established level is specifically provided for the for more than one pesticide having as combined residues by a regulation in metabolites compounds containing the this part. benzimidazole moiety found in or on a (1) Where residues from two or more raw agricultural commodity, the total chemicals in the same class are present amount of such residues shall not ex- in or on a raw agricultural commodity ceed the highest established tolerance and there are available methods that for a pesticide having these metabo- permit quantitative determination of lites. each residue, the quantity of combined (11) Where a tolerance is established residues that are within the tolerance for triclopyr, chloropyrifos, and may be determined as follows: chlorpyrifos-methyl having the com- (i) Determine the quantity of each mon metabolite 3,5,6-trichloro-2- residue present. pyridinol on the same raw agricultural (ii) Divide the quantity of each res- commodity, the total amount of such idue by the tolerance that would apply residues shall not exceed the highest if it occurred alone, and multiply by established tolerance for any of the 100 to determine the percentage of the pesticides having the metabolites. permitted amount of residue present. (12) Where tolerances are established (iii) Add the percentages so obtained for more than one pesticide having the for all residues present. metabolite 3,5,6-trichloro-2-pyridinol (iv) The sum of the percentages shall found in or on the raw agricultural not exceed 100 percent. commodity, the total amount of such (2) Where residues from two or more residues shall not exceed the highest chemicals in the same class are present established tolerance for a pesticide in or on a raw agricultural commodity having this metabolite. and there are available methods that

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permit quantitative determinations of . one or more, but not all, of the resi- Chlorobenzilate (ethyl 4,4′- dues, the amounts of such residues as dichlorobenzilate). p-Chlorophenoxyacetic acid. may be determinable shall be deducted p-Chlorophenyl-2,4,5-trichlorophenyl sulfide. from the total amount of residues 2,4-D (2,4-dichlorophenoxyacetic acid). present and the remainder shall have DDD (TDE). the same tolerance as that for the DDT. chemical having the lowest numerical 1,1-Dichloro-2,2-bis(p-ethylphenyl) ethane. tolerance in that class. The quantity of 2,6-Dichloro-4-nitroaniline. combined residues that are within the 2,4-Dichlorophenyl p-nitrophenyl ether. tolerance may be determined as fol- . Dodecachlorooctahydro-1,3,4-metheno-2H- lows: cyclobuta[cd]pentalene. (i) Determine the quantity of each Endosulfan (6,7,8,9,10,10-hexachloro-1,5,5a, determinable residue present. 6,9,9a-hexahydro-6,9-methano-2,4,3- (ii) Deduct the amounts of such resi- benzodioxathiepin-3-oxide). dues from the total amount of residues Endosulfan sulfate (6,7,8,9,10,10-hexachloro- present and consider the remainder to 1,5,5a,6,9,9a-hexahydro-6,9-methano-2,4,3- have the same tolerance as that for the benzodioxathiepin-3,3-dioxide). (1,4,5,6,7,8,8-heptachlor-3a,4,7, 7a- chemical having the lowest numerical tetrahydro-4,7-methanoindene). tolerance in that class. Heptachlor epoxide (1,4,5,6,7,8,8-heptachloro- (iii) Divide the quantity of each de- 2,3-epoxy-2,3,3a,4,7,7a-hexahydro-4,7- terminable residue by the tolerance methanoindene). that would apply if it occurred alone Hexachlorophene (2,2′-methylenebis(3,4,6- and the quantity of the remaining res- trichlorophenol) and its monosodium salt. idue by the tolerance for the chemical Isopropyl 4,4′-dichlorobenzilate. having the lowest numerical tolerance Lindane. . in that class and multiply by 100 to de- Ovex (p-chlorophenyl p- termine the percentage of the per- chlorobenzenesulfonate). mitted amount of residue present. Sesone (sodium 2,4-dichlorophenoxyethyl (iv) Add the percentages so obtained sulfate, SES). for all residues present. Sodium 2,4-dichlorophenoxyacetate. (v) The sum of the percentages shall Sodium trichloroacetate. not exceed 100 percent. Sulphenone (p-chlorophenyl phenyl sulfone). Terpene polychlorinates (chlorinated mix- (3) The following pesticides are mem- ture of camphene, pinene, and related bers of the class of dithiocarbamates: terpenes 65-66 percent chlorine). A mixture of 5.2 parts by weight of ammoni- 2,3,5,6-Tetrachloronitrobenzene. ′ ates of [ethylenebis (dithiocarbamato)] (2,4,5,4 -tetrachlorodiphenyl zinc with 1 part by weight ethylenebis sulfone). [dithiocarbamic acid] bimolecular and Toxaphene (chlorinated camphene). trimolecular cyclic anhydrosulfides and Trichlorobenzoic acid. disulfides. Trichlorobenzyl chloride. 2-Chloroallyl diethyldithiocarbamate. (5) The following are members of the Coordination product of zinc ion and maneb class of cholinesterase-inhibiting pes- containing 20 percent manganese, 2.5 per- cent zinc, and 77.5 percent ticides: ethylenebisdithiocarbamate. Acephate (O,S-dimethyl acetyl- Ferbam. phosphoramidothioate) and its cholin- Maneb. esterase-inhibiting metabolite O,S-di- Manganous dimethyldithiocarbamate. methyl phosphoramidothioate. Sodium dimethyldithiocarbamate. Aldicarb (2-methyl-2-(methylthio) Thiram. propionaldehyde O- Zineb. (methylcarbamoyl)oxime) and its Ziram. chlorinesterase-inhibiting metabolites 2- (4) The following are members of the methyl-2-(methylsulfinyl)propionaldehyde class of chlorinated organic pesticides: O-(methycarbamoyl) oxime and 2-methyl- 2-(methylsulfonyl)propionaldehyde O- . (methylcarbamoyl)oxime. BHC (benzene hexachloride). 4-tert-Butyl-2-chlorophenyl methyl methyl 1,1-Bis(p-chlorophenyl)-2,2,2- phosphoramidate. trichloroethanol. S-[(tert-Butylthio)methyl] O,O-diethyl Chlorbenside (p-chlorobenzyl p-chlorophenyl phosphorodithioate and its cholinesterase- sulfide). inhibiting metabolites.

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Carbaryl (1-naphthyl N-methylcarbamate). O,O-Dimethyl O-p-(dimethylsulfamoyl) Carbofuran (2,3,-dihydro-2,2-dimethyl-7- phenyl phosphorothioate. benzofuranyl-N-methylcarbamate). 3,5-Dimethyl-4-(methylthio) phenyl Carbofuran metabolite (2,3-dihydro-2,2-di- methylcarbamate. methyl-3-hydroxy-7-benofuranyl N- O,O-Dimethyl S-[4-oxo-1,2,3-benzotriazin-3- methylcarbamate). (4H)-ylmethyl] phosphorodithioate. Carbophenothion (S-[(p-chlorophenyl) Dimethyl phosphate of 3-hydroxy-N,N-di- thiolmethyl] O,O-diethyl methyl-cis-crotonamide. phosphorodithioate) and its cholinesterase- Dimethyl phosphate of 3-hydroxy-N-methyl- inhibiting metabolites. cis-crotonamide. Chlorpyrifos (O,O-diethyl O-(3,5,6-trichloro- Dimethyl phosphate of a-methylbenzyl 3-hy- 2-pyridyl)phosphorothioate). droxy-cis-crotonate. Chlorpyrifos-methyl (O,O-dimethyl-O-(3,5,6- O,O-Dimethyl 2,2,2-trichloro-1-hydroxyethyl trichloro-2-pyridyl) phosphorothioate. phosphonate. 2-Chloro-1-(2,4,5-trichlorophenyl)vinyl di- O,O-Dimethyl phosphorodithioate, S-ester methyl phosphate. with 4-(mercaptomethyl)-2-methozy-D2- 2-Chloro-1-(2,4-dichlorophenyl) vinyl diethyl 1,3,4-thiadiazolin-5-one. phosphate. (2,3-p-dioxanedithiol S,S-bis (O,O- Coumaphos (O,O-diethyl O-3-chloro-4-meth- diethylphosphorodithioate)) containing ap- yl-2-oxo-2H-1-benzopyran-7-yl phosran-7-yl proximately 70 percent cis and trans iso- phosphate). mers and approximately 30 percent related Coumaphos oxygen analog (O,O-diethyl O-3- compounds. chloro-4-methyl-2-oxo-2H-1- EPN. benzopyphorothioate). Ethephon ((2- - chloroethyl) phosphonic (S-(2-chloro-1-phthalimidoethyl) acid). Ethion. O,O-diethyl phosphorodithioate). Ethion oxygen analog (S- Dialifor oxygen analog (S-(2-chloro-1- [[(diethoxyphosphinothioyl)thio] methyl] phthalimidoethyl) O,O-diethyl O,O-diethyl phosphorothioate). phosphorothioate). O- Ethyl O-[4-(methylthio) phenyl] S-propyl Demeton (a mixture of O,O-diethyl O-(and S) phosphorodithioate and its cholinesterase- [2-ethylthio)ethyl] phosphorothioates). inhibiting metabolites. Ethiolate (S-ethyl diethylthiocarbamate). O-Ethyl S,S-dipropylphosphorodithioate. 2,2-Dichlorovinyl dimethyl phosphate. Ethyl 3-methyl-4-(methylthio)phenyl (1- O,O-Diethyl S-[2-(ethylthio)ethyl] methylethyl) phosphoramidate and its cho- phosphorodithioate and its cholinesterase- linesterase-inhibiting metabolites. inhibiting metabolites. O-Ethyl S-phenyl ethylphosphonodithioate. O,O-Diethyl O-(2-diethylamino-6-methyl-4- O-Ethyl S-phenyl ethylphosphonothiolate. pyrimidinyl) phosphorothioate and its oxy- m-(1-Ethylpropyl)phenyl methylcarbamate. gen analog diethyl 2-diethylamino-6-meth- S-[2-Ethylsulfinyl)ethyl] O,O-dimethyl yl-4-pyrimidinyl phosphate. phosphorothioate and its cholinesterase-in- O,O-Diethyl O-(2-isoprophyl-4-methyl-6- hibiting metabolites, (primarily S-[2- pyrimidinyl) phosphorothioate. (ethyl-sulfonyl)ethyl] O,O-dimethyl O,O-Diethyl O-[p-(methylsulfinyl)phenyl] phosphorothioate). phosphorothioate and its cholinesterase-in- Fenthion (O,O-dimethyl O-[3-methyl-4- hibiting metabolites. (methylthio)phenyl]phosphorothioate and Diethyl 2-pyrazinyl phosphate. its cholinesterase-inhibiting metabolites. O,O-Diethyl O-2-pyrazinyl phosphorothioate. Malathion. S-(O,O-Diisopropyl phosphorodithioate) of N- N-(Mercaptomethyl)phthalimide S-(O,O-di- (2-mercaptoethyl) benzenesulfonamide methyl phosphorodithioate). S-(O,O-Diisopropyl phosphorodithioate) of N- N-(Mercaptomethyl)phthalimide S-(O,O-di- (2-mercaptoethyl) benzenesulfonamide methyl phosphorothioate). 2-(Dimethylamino)-5.6-dimethyl-4- Methomyl (S-methyl N- pyrimidinyl dimethylcarbamate and its [(methylcarbamoyl)oxy]thioacetimidate). metabolites 5,6-dimethyl-2- 1-Methoxycarbonyl-1-propen-2-yl dimethyl (formylmethylamino)-4-pyrimidinyl phosphate and its beta isomer. dimethylcarbamate and 5,6-dimethyl-2- m-(1-Methylbutyl)phenyl methylcarbamate. (methylamino)-4-pyrimidinyl Methyl parathion. dimethylcarbamate (both calculated as Naled (1,2-dibromo-2,2-dichloroethyl di- parent). methyl phosphate). Dimethoate (O,O-dimethyl S-(N-methyl- Oxamyl (methyl N′,N′-dimethyl-N- carbamoylmethyl) phosphorodithioate). [(methylcarbamoyl)oxy]-1- Dimethoate oxygen analog (O,O-dimethyl S- thiooxamimidate) (N-methylcarbamoylmethyl) Parathion. phosphorothioate). Phorate (O,O-diethyl S-(ethylthio)methyl O,O-Dimethyl O-p-(dimethylsulfamoyl) phosphorodithioate) and its cholinesterase- phenyl phosphate. inhibiting metabolites.

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Phosalone (S-(6-chloro-3-mercaptomethyl)-2- § 180.5 Zero tolerances. benzoxazolinone) O,O-diethyl phosphorodithioate). A zero tolerance means that no Phosphamidon (2-chloro-2-diethylcarbamoyl- amount of the pesticide chemical may 1-methylvinyl dimethyl phosphate) includ- remain on the raw agricultural com- ing all of its related cholinesterase-inhib- modity when it is offered for shipment. iting compounds. A zero tolerance for a pesticide chem- Pirimiphos-methyl O-[2-diethylamino-6- ical in or on a raw agricultural com- methyl-pyrimidinyl) O,O-dimethyl modity may be established because, phosphorothioate among other reasons: Ronnel. (a) A safe level of the pesticide chem- (octamethylpyrophosphoramide). ical in the diet of two different species Tetraethyl pyrophosphate. of warm-blooded animals has not been ′ ′ ′ O,O,O ,O -Tetramethyl O,O -sulfinyldi-p- reliably determined. phenylene phosphorothioate. (b) The chemical is carcinogenic to O,O,O′,O′-Tetramethyl O,O′-thiodi-p-phen- ylene phosphorothioate. or has other alarming physiological ef- Tributyl phosphorotritlioite. fects upon one or more of the species of S,S,S-Tributyl phosphorothrithioate. the test animals used, when fed in the 3,4,5-Trimethylphenyl methylcarbamate and diet of such animals. its isomer 2,3,5-trimethylphenyl (c) The pesticide chemical is toxic, methylcarbamate. but is normally used at times when, or in such manner that, fruit, vegetables, (6) The following pesticides are mem- or other raw agricultural commodities bers of the class of dinitrophenols: will not bear or contain it. 2,4-Dinitro-6-octylphenyl crotonate and 2,6- (d) All residue of the pesticide chem- dinitro-4-octylphenyl crotonate, mixture ical is normally removed through good of. agricultural practice such as washing 4,6-Dinitro-o-cresol and its sodium salt. or brushing or through weathering or (2-sec-butyl-4,6-dinitrophenol) and other changes in the chemical itself, its alkanolamine, ammonium, and sodium prior to introduction of the raw agri- salts. cultural commodity into interstate [41 FR 8969, Mar. 2, 1976, as amended at 41 FR commerce. 10605, Mar. 12, 1976; 41 FR 20660, May 20, 1976; 41 FR 51401, Nov. 22, 1976; 42 FR 6582, Feb. 3, § 180.6 Pesticide tolerances regarding 1977; 43 FR 12682, Mar. 27, 1978; 49 FR 44465, milk, eggs, meat, and/or poultry; Nov. 7, 1984; 49 FR 45852, Nov. 21, 1984; 50 FR statement of policy. 18485, May 1, 1985; 50 FR 26684, June 27, 1985; 51 FR 28228, Aug. 6, 1986; 54 FR 31835, Aug. 2, (a) When establishing tolerances for 1989; 57 FR 1649, Jan. 15, 1992; 58 FR 65555, pesticide residues in or on raw agricul- Dec. 15, 1993] tural commodities, consideration is al- ways given to possible residues of those § 180.4 Exceptions. pesticide chemicals or their conversion The substances listed in this section products entering the diet of man are excepted from the definitions of through the ingestion of milk, eggs, ‘‘pesticide chemical’’ and ‘‘pesticide meat, and/or poultry produced by ani- chemical residue’’ under FFDCA sec- mals fed agricultural products bearing tion 201(q)(3) and are therefore exempt such pesticide residues. In each in- from regulation under FFDCA section stance an evaluation of all available 402(a)(2)(B) and 408. These substances data will result in a conclusion either: are subject to regulation by the Food (1) That finite residues will actually and Drug Administration as food addi- be incurred in these foods from feed use tives under FFDCA section 409. of the raw agricultural commodity in- (a) Inert ingredients in food pack- cluding its byproducts; or aging impregnated with an insect re- (2) That it is not possible to establish pellent when such inert ingredients are with certainty whether finite residues the components of the food packaging will be incurred, but there is a reason- material (e.g., paper and paperboard, able expectation of finite residues; or coatings, adhesives, and polymers). (3) That it is not possible to establish with certainty whether finite residues (b) [Reserved] will be incurred, but there is no reason- [63 FR 10720, Mar. 4, 1998] able expectation of finite residues.

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(b) When the data show that finite of the pesticide residue and of the un- residues will actually be incurred in likelihood of such residue exceeding milk, eggs, meat, and/or poultry, a tol- the tolerance. The analytical methods erance will be established on the raw to be used for enforcement purposes agricultural commodity used as feed will be those set forth in the ‘‘Pesticide provided that tolerances can be estab- Analytical Manual’’ (see § 180.101(c)). lished at the same time, on the basis of The sensitivities of these methods are the toxicological and other data avail- expressed in that manual. able, for the finite residues incurred in milk, eggs, meat, and/or poultry. When Subpart B—Procedural it is not possible to determine with cer- tainty whether finite residues will be Regulations incurred in milk, eggs, meat, and/or PROCEDURE FOR FILING PETITIONS SEEK- poultry but there is a reasonable expec- ING THE ESTABLISHMENT, MODIFICA- tation of finite residues in light of data TION, OR REVOCATION OF TOLERANCES reflecting exaggerated pesticides levels OR EXEMPTIONS in feeding studies, a tolerance will be established on the raw agricultural § 180.7 Petitions proposing tolerances commodity provided that appropriate or exemptions for pesticide resi- tolerances can be established at the dues in or on raw agricultural com- same time, on the basis of the toxi- modities or processed foods. cological and other data available, for (a) Petitions to be filed with the the finite residues likely to be incurred Agency under the provisions of FFDCA in these foods through the feed use of section 408(d) shall be submitted in du- the raw agricultural commodity or its plicate. If any part of the material sub- byproducts. When it is not possible to mitted is in a foreign language, it shall determine with certainty whether fi- be accompanied by an accurate and nite residues will be incurred in milk, complete English translation. The peti- eggs, meat, and/or poultry but there is tion shall be accompanied by an ad- no reasonable expectation of finite res- vance deposit for fees described in idues in light of data such as those re- § 180.33. The petition shall state the pe- flecting exaggerated pesticide levels in titioner’s mail address to which notice feeding studies and those elucidating of objection under FFDCA section the biochemistry of the pesticide 408(g)(2) may be sent. The petition chemical in the animal, a tolerance must be signed by the petitioner or by may be established on the raw agricul- tural commodity without the necessity his attorney or agent, or (if a corpora- of a tolerance on food products derived tion) by an authorized official. from the animal. (b) Petitions shall include the fol- (c) The principles outlined in para- lowing information: graphs (a) and (b) of this section will (1) An informative summary of the also be followed with respect to toler- petition and of the data, information, ances for residues which will actually and arguments submitted or cited in be incurred or are reasonably to be ex- support of the petition. Both a paper pected in milk, eggs, meat, and/or poul- and electronic copy of the summary try by the use of pesticides directly on should be submitted. The electronic the animal or administered purposely copy should be formatted according to in the feed or drinking water. the Office of Pesticide Programs’ cur- (d) Tolerances contemplated by para- rent standard for electronic data sub- graphs (a) and (b) of this section will in mission as specified at http:// addition to toxicological consider- www.epa.gov/oppfead1/eds/edsgoals.htm. ations be conditioned on the avail- (2) A statement that the petitioner ability of a practicable analytical agrees that such summary or any in- method to determine the pesticide res- formation it contains may be published idue; that is, the method must be sen- as a part of the notice of filing of the sitive and reliable at the tolerance petition to be published under FFDCA level or in special cases at a higher section 408(d)(3) and as a part of a pro- level where such level is deemed satis- posed or final regulation issued under factory and safe in light of the toxicity FFDCA section 408.

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(3) The name, chemical identity, and idue and the petitioner does not pro- composition of the pesticide chemical pose that this level be adopted, a state- residue and of the pesticide chemical ment explaining the reasons for this that produces the residue. departure from the Codex level. (4) Data showing the recommended (15) Such other data and information amount, frequency, method, and time as the Administrator requires by regu- of application of the pesticide chem- lation to support the petition. ical. (16) Reasonable grounds in support of (5) Full reports of tests and inves- the petition. tigations made with respect to the (c) The data specified under para- safety of the pesticide chemical, in- graphs (b)(1) through (b)(16) of this sec- cluding full information as to the tion should be on separate sheets or methods and controls used in con- sets of sheets, suitably identified. If ducting those tests and investigations. such data have already been submitted (6) Full reports of tests and inves- with an earlier application, the present tigations made with respect to the na- petition may incorporate it by ref- ture and amount of the pesticide chem- erence to the earlier one. ical residue that is likely to remain in (d) Except as noted in paragraph (e) or on the food, including a description of this section, a petition shall not be of the analytical methods used. (See accepted for filing if any of the data § 180.34 for further information about prescribed by FFDCA section 408(d) are residue tests.) lacking or are not set forth so as to be (7) Proposed tolerances for the pes- readily understood. The availability to ticide chemical residue if tolerances the public of information provided to, are proposed. or otherwise obtained by, the Agency (8) Practicable methods for removing under this part shall be governed by any amount of the residue that would part 2 of this chapter. The Adminis- exceed any proposed tolerance. trator shall make the full text of the (9) A practical method for detecting summary referenced in paragraph (b)(1) and measuring the levels of the pes- of this section available to the public ticide chemical residue in or on the in the Environmental Protection Agen- food, or for exemptions, a statement cy Electronic Docket at http:// why such a method is not needed. www.epa.gov/edocket no later than pub- (10) If the petition relates to a toler- lication in the FEDERAL REGISTER of ance for a processed food, reports of in- the notice of the petition filing. vestigations conducted using the proc- (e) The Administrator shall notify essing method(s) used to produce that the petitioner within 15 days after its food. receipt of acceptance or nonacceptance (11) Such information as the Admin- of a petition, and if not accepted the istrator may require to make the de- reasons therefor. If petitioner desires, termination under FFDCA section the petitioner may supplement a defi- 408(b)(2)(C). cient petition after notification as to (12) Such information as the Admin- deficiencies. If the petitioner does not istrator may require on whether the wish to supplement or explain the peti- pesticide chemical may have an effect tion and requests in writing that it be in humans that is similar to an effect filed as submitted, the petition shall be produced by a naturally occurring es- filed and the petitioner so notified. trogen or other endocrine effects. (f) A notice of the filing of a petition (13) Information regarding exposure for a pesticide chemical residue toler- to the pesticide chemical residue due ance that the Administrator deter- to any tolerance or exemption already mines has met the requirements of granted for such residue. paragraph (b) of this section shall be (14) Information concerning any max- published in the FEDERAL REGISTER by imum residue level established by the the Administrator within 30 days after Codex Alimentarius Commission for such determination. The notice shall the pesticide chemical residue ad- state the name of the pesticide chem- dressed in the petition. If a Codex max- ical residue and the commodities for imum residue level has been estab- which a tolerance is sought and an- lished for the pesticide chemical res- nounce the availability of a description

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of the analytical methods available to while technically complete, is inad- the Administrator for the detection equate to justify the establishment of a and measurement of the pesticide tolerance or the tolerance requested by chemical residue with respect to which petitioner. This may be due to the fact the petition is filed or shall set forth that the data are not sufficiently clear the petitioner’s statement of why such or complete. In such cases, the peti- a method is not needed. The notice tioner may withdraw the petition pend- shall explicitly reference the specific ing its clarification or the obtaining of address in the Agency’s Electronic additional data. This withdrawal may Docket (http://www.epa.gov/edocket) be without prejudice to a future filing. where the full text of the summary re- A deposit for fees as specified in § 180.33 quired in paragraph (b) of this section shall accompany the resubmission of and refer interested parties to this doc- the petition. ument for further information on the [70 FR 33361, June 8, 2005] petition. The full text of the summary may be omitted from the notice. § 180.9 Substantive amendments to pe- (g) The Administrator may request a titions. sample of the pesticide chemical at any After a petition has been filed, the time while a petition is under consider- petitioner may submit additional in- ation. The Administrator shall specify formation or data in support thereof, in its request for a sample of the pes- but in such cases the petition will be ticide chemical, a quantity which it given a new filing date. deems adequate to permit tests of ana- lytical methods used to determine resi- [70 FR 33361, June 8, 2005] dues of the pesticide chemical and of methods proposed by the petitioner for ADVISORY COMMITTEES removing any residues of the chemical ESTABLISHMENT, MODIFICATION, AND that exceed the tolerance proposed. REVOCATION OF TOLERANCE ON INITIA- (h) The Administrator shall deter- TIVE OF ADMINISTRATOR; JUDICIAL RE- mine, in accordance with the Act, VIEW; TEMPORARY TOLERANCES; MODI- whether to issue an order that estab- lishes, modifies, or revokes a tolerance FICATION AND REVOCATION OF TOLER- regulation (whether or not in accord ANCES; FEES with the action proposed by the peti- § 180.29 Establishment, modification, tioner), whether to publish a proposed and revocation of tolerance on ini- tolerance regulation and request public tiative of Administrator. comment thereon under § 180.29, or (a) Upon the Administrator’s own ini- whether to deny the petition. The Ad- tiative, the Administrator may pro- ministrator shall publish in the FED- pose, under FFDCA section 408(e), the ERAL REGISTER such order or proposed issuance of a regulation establishing a regulation. After receiving comments tolerance for a pesticide chemical or on any proposed regulation, the Ad- exempting it from the necessity of a ministrator may issue an order that es- tolerance, or a regulation modifying or tablishes, modifies, or revokes a toler- revoking an existing tolerance or ex- ance regulation. An order published emption. under this section shall describe briefly (b) The Administrator shall provide a how to submit objections and requests period of not less than 60 days for per- for a hearing under part 178 of this sons to comment on the proposed regu- chapter. A regulation issued under this lation, except that a shorter period for section shall be effective on the date of comment may be provided if the Ad- publication in the FEDERAL REGISTER ministrator for good cause finds that it unless otherwise provided in the regu- would be in the public interest to do so lation. and states the reasons for the finding [70 FR 33360, June 8, 2005] in the notice of proposed rulemaking. (c) After reviewing any timely com- § 180.8 Withdrawal of petitions with- ments received, the Administrator may out prejudice. by order establish, modify, or revoke a In some cases the Administrator will tolerance regulation, which order and notify the petitioner that the petition, regulation shall be published in the

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FEDERAL REGISTER. An order published rules issued under FFDCA sections under this section shall state that per- 408(n)(3) and 408(d) or (e) regarding de- sons may submit objections and re- terminations pertaining to State au- quests for a hearing in the manner de- thority to establish regulatory limits scribed in part 178 of this chapter. on pesticide chemical residues. (d) Any final regulation issued under (8) Orders issued under FFDCA sec- this section shall be effective on the tion 408(g)(2)(C) ruling on objections to date of publication in the FEDERAL orders issued under FFDCA section REGISTER unless otherwise provided in 408(n)(5)(C) authorizing States to estab- the regulation. lish regulatory limits not identical to certain tolerances or exemptions. [70 FR 33361, June 8, 2005] (b) Any issue as to which review is or § 180.30 Judicial review. was obtainable under paragraph (a) of this section shall not be the subject of (a) Under FFDCA section 408(h), judi- judicial review under any other provi- cial review is available in the United sion of law. In part, this means that, States Courts of Appeal as to the fol- for the Agency actions subject to the lowing actions: objection procedure in FFDCA section (1) Regulations establishing general 408(g)(2), judicial review is not avail- procedures and requirements under able unless an adversely affected party FFDCA section 408(e)(1)(C). exhausts these objection procedures, (2) Orders issued under FFDCA sec- and any petition procedures prelimi- tion 408(f)(1)(C) requiring the submis- nary thereto. sion of data. (3) Orders issued under FFDCA sec- [70 FR 33362, June 8, 2005] tion 408(g)(2)(C) ruling on objections to establishment, modification, or revoca- § 180.31 Temporary tolerances. tion of a tolerance or exemption under (a) A temporary tolerance (or exemp- FFDCA section 408(d)(4), or any regula- tion from a tolerance) established tion that is the subject of such an under the authority of FFDCA section order. The underlying action here is 408(r) shall be deemed to be a tolerance Agency disposition of a petition seek- (or exemption from the requirement of ing the establishment, modification, or a tolerance) for the purposes of FFDCA revocation of a tolerance or exemption. section 408(a)(1) or (a)(2) and for the (4) Orders issued under FFDCA sec- purposes of § 180.30. tion 408(g)(2)(C) ruling on objections to (b) A request for a temporary toler- the denial of a petition under FFDCA ance or a temporary exemption from a section 408(d)(4). tolerance by a person who has obtained (5) Orders issued under FFDCA sec- or is seeking an experimental permit tion 408(g)(2)(C) ruling on objections to for a pesticide chemical under the Fed- the establishment, modification, sus- eral , Fungicide, and pension, or revocation of a tolerance or Rodenticide Act shall be accompanied exemption under FFDCA section by such data as are available on sub- 408(e)(1)(A) or (e)(1)(B). The underlying jects outlined in § 180.7(b) and an ad- action here is the establishment, modi- vance deposit to cover fees as provided fication, suspension, or revocation of a in § 180.33. tolerance or exemption upon the initia- (c) To obtain a temporary tolerance, tive of EPA including EPA actions pur- a requestor must comply with the peti- suant to FFDCA sections tion procedures specified in FFDCA 408(b)(2)(B)(v), 408(b)(2)(E)(ii), section 408(d) and § 180.7 except as pro- 408(d)(4)(C)(ii), 408(l)(4), and 408(q)(1). vided in this section. (6) Orders issued under FFDCA sec- (d) A temporary tolerance or exemp- tion 408(g)(2)(C) ruling on objections to tion from a tolerance may be issued for the revocation or modification of a tol- a period designed to allow the orderly erance or exemption under FFDCA sec- marketing of the raw agricultural com- tion 408(f)(2) for noncompliance with modities produced while testing a pes- requirements for the submission of ticide chemical under an experimental data. permit issued under authority of the (7) Orders issued under FFDCA sec- Federal Insecticide, Fungicide, and tion 408(g)(2)(C) ruling on objections to Rodenticide Act if the Administrator

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concludes that the safety standard in (b) Any person may file with the Ad- FFDCA section 408(b)(2) or (c), as appli- ministrator a petition proposing the cable, is met. Subject to the require- issuance of a regulation modifying or ments of FFDCA section 408(e), a tem- revoking a tolerance or exemption porary tolerance or exemption from a from a tolerance for a pesticide chem- tolerance may be revoked if the experi- ical residue. The petition shall furnish mental permit is revoked, or may be reasonable grounds for the action revoked at any time if it develops that sought. Reasonable grounds shall in- the application for a temporary toler- clude an explanation showing wherein ance contains a misstatement of a ma- the person has a substantial interest in terial fact or that new scientific data such tolerance or exemption from tol- or experience with the pesticide chem- erance and an assertion of facts (sup- ical indicates that it does not meet the ported by data if available) showing safety standard in FFDCA section that new uses for the pesticide chem- 408(b)(2) or (c), as applicable. ical have been developed or old uses (e) Conditions under which a tem- abandoned, that new data are available porary tolerance is established shall in- as to toxicity of the chemical, or that clude: experience with the application of the (1) A limitation on the amount of the tolerance or exemption from tolerance chemical to be used on the designated may justify its modification or revoca- crops permitted under the experi- tion. Evidence that a person has reg- mental permit. istered or has submitted an application for the registration of a pesticide under (2) A limitation for the use of the the Federal Insecticide, Fungicide, and chemical on the designated crops to Rodenticide Act will be regarded as bona fide experimental use by qualified evidence that the person has a substan- persons as indicated in the experi- tial interest in a tolerance or exemp- mental permit. tion from the requirement of a toler- (3) A requirement that the person or ance for a pesticide chemical that con- firm which obtains the experimental sists in whole or in part of the pes- permit for which the temporary toler- ticide. New data should be furnished in ance is established will immediately the form specified in § 180.7(b) for sub- inform the Environmental Protection mitting petitions, as applicable. Agency of any reports on findings from (c) The procedures for completing ac- the experimental use that have a bear- tion on an Administrator initiated pro- ing on safety. posal or a petition shall be those speci- (4) A requirement that the person or fied in §§ 180.29 and 180.7, as applicable. firm which obtained the experimental permit for which the temporary toler- [70 FR 33362, June 8, 2005] ance is established will keep records of § 180.33 Fees. production, distribution, and perform- ance for a period of 2 years and, on re- (a) Each petition for the establish- quest, at any reasonable time, make ment of a new tolerance or a tolerance these records available to any author- higher than already established, shall ized officer or employee of the Environ- be accompanied by a fee of $80,950, plus mental Protection Agency. $2,025 for each raw agricultural com- modity more than nine on which the [70 FR 33362, June 8, 2005] establishment of a tolerance is re- quested, except as provided in para- § 180.32 Procedure for modifying and graphs (b), (d), and (h) of this section. revoking tolerances or exemptions (b) Each petition for the establish- from tolerances. ment of a tolerance at a lower numer- (a) The Administrator on his/her own ical level or levels than a tolerance al- initiative may propose the issuance of ready established for the same pes- a regulation modifying or revoking a ticide chemical, or for the establish- tolerance for a pesticide chemical res- ment of a tolerance on additional raw idue on raw agricultural commodities agricultural commodities at the same or processed foods or modifying or re- numerical level as a tolerance already voking an exemption from tolerance established for the same pesticide for such residue. chemical, shall be accompanied by a

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fee of $18,500 plus $1,225 for each raw a charge for each commodity where agricultural commodity on which a tol- that would otherwise apply. erance is requested. (i) Objections under section 408(d)(5) (c) Each petition for an exemption of the Act shall be accompanied by a from the requirement of a tolerance or filing fee of $4,050. repeal of an exemption shall be accom- (j) The person who files a petition for panied by a fee of $14,925. judicial review of an order under sec- (d) Each petition or request for a tion 408(h) of the Act shall pay the temporary tolerance or a temporary costs of preparing the record on which exemption from the requirement of a the order is based unless the person has tolerance shall be accompanied by a fee no financial interest in the petition for of $32,325 except as provided in para- judicial review. graph (e) of this section. A petition or (k) No fee under this section will be request to renew or extend such tem- imposed on the Interregional Research porary tolerance or temporary exemp- Project Number 4 (IR-4 Program). tion shall be accompanied by a fee of (l) The Administrator may waive or $4,600. refund part or all of any fee imposed by (e) A petition or request for a tem- this section if the Administrator deter- porary tolerance for a pesticide chem- mines in his or her sole discretion that ical which has a tolerance for other such a waiver or refund will promote uses at the same numerical level or a the public interest or that payment of higher numerical level shall be accom- the fee would work an unreasonable panied by a fee of $16,075, plus $1,225 for hardship on the person on whom the each raw agricultural commodity on fee is imposed. A request for waiver or which the temporary tolerance is refund of a fee shall be submitted to sought. the Office of Pesticide Programs’ Docu- (f) Each petition for revocation of a ment Processing Desk at the appro- tolerance shall be accompanied by a fee priate address as set forth in 40 CFR of $10,125. Such fee is not required 150.17(a) or (b). A fee of $2,025 shall ac- when, in connection with the change company every request for a waiver or sought under this paragraph, a petition is filed for the establishment of new refund, as specified in paragraph (m) of tolerances to take the place of those this section, except that the fee under sought to be revoked and a fee is paid this paragraph shall not be imposed on as required by paragraph (a) of this sec- any person who has no financial inter- tion. est in any action requested by such (g) If a petition or a request is not ac- person under paragraphs (a) through (j) cepted for processing because it is of this section. The fee for requesting a technically incomplete, the fee, less waiver or refund shall be refunded if $2,025 for handling and initial review, the request is granted. shall be returned. If a petition is with- (m) All deposits and fees required by drawn by the petitioner after initial the regulations in this part shall be processing, but before significant Agen- paid by money order, bank draft, or cy scientific review has begun, the fee, certified check drawn to the order of less $2,025 for handling and initial re- the Environmental Protection Agency. view, shall be returned. If an unaccept- All deposits and fees shall be forwarded able or withdrawn petition is resub- to the Environmental Protection Agen- mitted, it shall be accompanied by the cy, Headquarters Accounting Oper- fee that would be required if it were ations Branch, Office of Pesticide Pro- being submitted for the first time. grams (Tolerance Fees), P.O. Box (h) Each petition for a crop group tol- 360277M, Pittsburgh, PA 15251. The pay- erance, regardless of the number of raw ments should be specifically labeled agricultural commodities involved, ‘‘Tolerance Petition Fees’’ and should shall be accompanied by a fee equal to be accompanied only by a copy of the the fee required by the analogous cat- letter or petition requesting the toler- egory for a single tolerance that is not ance. The actual letter or petition, a crop group tolerance, i.e., paragraphs along with supporting data, shall be (a) through (f) of this section, without forwarded within 30 days of payment to

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the Office of Pesticide Programs’ Docu- (c) If the pesticide chemical is ab- ment Processing Desk at the appro- sorbed into a living plant or animal priate address as set forth in 40 CFR when applied (is systemic), residue 150.17(a) or (b). A petition will not be data may be needed on each plant or accepted for processing until the re- animal on which a tolerance or exemp- quired fees have been submitted. A pe- tion is requested. tition for which a waiver of fees has (d) If the pesticide chemical is not been requested will not be accepted for absorbed into the living plant or ani- processing until the fee has been mal when applied (is not systemic), it waived or, if the waiver has been de- may be possible to make a reliable es- nied, the proper fee is submitted after timate of the residues to be expected notice of denial. A request for waiver on each commodity in a group of re- or refund will not be accepted after sci- lated commodities on the basis of less entific review has begun on a petition. data than would be required for each (n) This fee schedule will be changed commodity in the group, considered annually by the same percentage as the separately. percent change in the Federal General (e) Each of the following groups of Schedule (GS) pay scale. In addition, crops lists raw agricultural commod- processing costs and fees will periodi- ities that are considered to be related cally be reviewed and changes will be for the purpose of paragraph (d) of this made to the schedule as necessary. section. Commodities not listed in this When automatic adjustments are made paragraph are not considered as related based on the GS pay scale, the new fee for the purpose of paragraph (d) of this schedule will be published in the FED- section. This grouping of crops does ERAL REGISTER as a final rule to be- not affect the certification of useful- come effective 30 days or more after ness by the Administrator as con- publication, as specified in the rule. templated by section 408(l) of the act. When changes are made based on peri- (1) Apples, crabapples, pears, quinces. odic reviews, the changes will be sub- (2) Avocados, papayas. ject to public comment. (3) Blackberries, boysenberries, (o) No fee required by this section dewberries, loganberries, raspberries. shall be levied during the period begin- (4) Blueberries, currants, goose- ning on October 1, 2003, and ending Sep- berries, huckleberries. tember 30, 2008. (5) Cherries, plums, prunes. [68 FR 24371, May 7, 2003, as amended at 69 (6) Oranges, citrus citron, grapefruit, FR 12544, Mar. 17, 2004; 70 FR 33363, June 8, kumquats, lemons, limes, tangelos, 2005; 71 FR 35547, June 21, 2006] tangerines. (7) Mangoes, persimmons. § 180.34 Tests on the amount of res- (8) Peaches, apricots, nectarines. idue remaining. (9) Beans, peas, soybeans (each in dry (a) Data in a petition on the amount form). of residue remaining in or on a raw ag- (10) Beans, peas, soybeans (each in ricultural commodity should establish succulent form). the residue that may remain when the (11) Broccoli, brussels sprouts, cauli- pesticide chemical is applied according , kohlrabi. to directions registered under the Fed- (12) Cantaloups, honeydew melons, eral Insecticide, Fungicide, and muskmelons, pumpkins, watermelons, Rodenticide Act, or according to direc- winter squash. tions contained in an application for (13) Carrots, garden beets, sugar registration. These data should estab- beets, horseradish, parsnips, radishes, lish the residues that may remain rutabagas, salsify roots, turnips. under conditions most likely to result (14) Celery, fennel. in high residues on the commodity. (15) Cucumbers, summer squash. (b) The petition should establish the (16) Lettuce, endive (escarole), Chi- reliability of the residue data reported nese cabbage, salsify tops. in it. Sufficient information should be (17) Onions, garlic, leeks, shallots submitted about the analytical method (green, or in dry bulb form). to permit competent analysts to apply (18) Potatoes, Jerusalem-artichokes, it successfully. sweetpotatoes, yams.

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(19) Spinach, beet tops, collards, dan- (2) On the initiative of the Adminis- delion, kale, mustard greens, , trator. Swiss chard, turnip tops, watercress. (3) A petition by an interested per- (20) Tomatoes, eggplants, peppers, pi- son. mentos. (b) The tables in § 180.41 are to be (21) Pecans, almonds, brazil nuts, used in conjunction with this section bush nuts, butternuts, , fil- for the establishment of crop group tol- berts, hazelnuts, hickory nuts, wal- erances. Each table in § 180.41 lists a nuts. group of raw agricultural commodities (22) Field corn, popcorn, sweet corn that are considered to be related for (each in grain form). the purposes of this section. Refer also (23) Milo, sorghum (each in grain to § 180.1(h) for a listing of commodities form). for which established tolerances may (24) Wheat, barley, oats, rice, rye be applied to certain other related and (each in grain form). similar commodities. (25) Alfalfa, Bermuda grass, blue- (c) When there is an established or grass, brome grass, clovers, cowpea proposed tolerance for all of the rep- hay, fescue, lespedeza, lupines, orchard resentative commodities for a specific grass, peanut hay, peavine hay, rye group or subgroup of related commod- grass, soybean hay, sudan grass, tim- ities, a tolerance may be established othy, and vetch. for all commodities in the associated (26) Corn forage, sorghum forage. group or subgroup. Tolerances may be (27) Sugarcane, cane sorghum. established for a crop group or, alter- [36 FR 22540, Nov. 25, 1971, as amended at 39 natively, tolerances may be established FR 28286, Aug. 6, 1974; 39 FR 28977, Aug. 13, for one or more of the subgroups of a 1974; 40 FR 6972, Feb. 18, 1975; 45 FR 82928, crop group. Dec. 17, 1980; 48 FR 29860, June 29, 1983; 60 FR (d) The representative crops are 26635, May 17, 1995] given as an indication of the minimum residue chemistry data base acceptable § 180.35 Tests for potentiation. to the Agency for the purposes of es- Experiments have shown that certain tablishing a group tolerance. The cholinesterase-inhibiting pesticides Agency may, at its discretion, allow when fed together to test animals are group tolerances when data on suitable more toxic than the sum of their indi- substitutes for the representative crops vidual toxicities when fed separately. are available (e.g., limes instead of One substance potentiates the toxicity lemons). of the other. Important toxicological (e) Since a group tolerance reflects interactions also have been observed maximum residues likely to occur on between pesticides and other sub- all individual crops within a group, the stances. Wherever there is reason to proposed or registered patterns of use believe that a pesticide chemical for for all crops in the group or subgroup which a tolerance is proposed may must be similar before a group toler- interact with other pesticide chemicals ance is established. The pattern of use or other substances to which man is ex- consists of the amount of pesticide ap- posed, it may be necessary to require plied, the number of times applied, the special experimental data regarding timing of the first application, the in- potentiation capacities to evaluate the terval between applications, and the safety of the proposed tolerance. This interval between the last application necessarily will be determined on a and harvest. The pattern of use will case-by-case basis. also include the type of application; for example, soil or foliar application, or § 180.40 Tolerances for crop groups. application by ground or aerial equip- (a) Group or subgroup tolerances may ment. be established as a result of: (f) When the crop grouping contains (1) A petition from a person who has commodities or byproducts that are submitted an application for the reg- utilized for animal feed, any needed istration of a pesticide under the Fed- tolerance or exemption from a toler- eral Insecticide, Fungicide, and ance for the pesticide in meat, milk, Rodenticide Act. poultry and/or eggs must be established

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before a tolerance will be granted for (j) Establishment of a tolerance does the group as a whole. The representa- not substitute for the additional need tive crops include all crops in the to register the pesticide under a com- group that could be processed such panion law, the Federal Insecticide, that residues may concentrate in proc- Fungicide, and Rodenticide Act. The essed food and/or feed. Processing data Registration Division of the Office of will be required prior to establishment Pesticide Programs should be con- of a group tolerance. Tolerances will tacted concerning procedures for reg- not be granted on a group basis as to istration of new uses of a pesticide. processed foods prepared from crops covered by the group tolerance. [60 FR 26635, May 17, 1995, as amended at 70 (g) If maximum residues (tolerances) FR 33363, June 8, 2005] for the representative crops vary by more than a factor of 5 from the max- § 180.41 Crop group tables. imum value observed for any crop in (a) The tables in this section are to the group, a group or subgroup toler- be used in conjunction with § 180.40 to ance will ordinarily not be established. establish crop group tolerances. In this case individual crop tolerances, (b) Commodities not listed are not rather than group tolerances, will nor- considered as included in the groups for mally be established. the purposes of this paragraph, and in- (h) Alternatively, a commodity with dividual tolerances must be estab- a residue level significantly higher or lished. Miscellaneous commodities in- lower than the other commodities in a tentionally not included in any group group may be excluded from the group include asparagus, avocado, banana, tolerance (e.g., cereal grains, except cranberry, fig, globe artichoke, grape, corn). In this case an individual toler- hops, kiwifruit, mango, mushroom, ance at the appropriate level for the okra, papaya, pawpaw, peanut, per- unique commodity would be estab- simmon, pineapple, strawberry, water lished, if necessary. The alternative ap- , and watercress. proach of excluding a commodity with (c) Each group is identified by a a significantly higher or lower residue group name and consists of a list of level will not be used to establish a tol- representative commodities followed erance for a commodity subgroup. Most subgroups have only two representa- by a list of all commodity members for tive commodities; to exclude one such the group. If the group includes sub- commodity and its related residue data groups, each subgroup lists the sub- would likely provide insufficient res- group name, the representative com- idue information to support the re- modity or commodities, and the mem- mainder of the subgroup. Residue data ber commodities for the subgroup. Sub- from crops additional to those rep- groups, which are a subset of their as- resentative crops in a grouping may be sociated crop group, are established for required for systemic pesticides. some but not all crops groups. (i) The commodities included in the (1) Crop Group 1: Root and Tuber groups will be updated periodically ei- Vegetables Group. ther at the initiative of the Agency or (i) Representative commodities. , at the request of an interested party. potato, radish, and sugar beet. Persons interested in updating this sec- (ii) Table. The following table 1 lists tion should contact the Registration all the commodities included in Crop Division of the Office of Pesticide Pro- Group 1 and identifies the related crop grams. subgroups.

TABLE 1—CROP GROUP 1: ROOT AND TUBER VEGETABLES

Related crop Commodities subgroups

Arracacha (Arracacia xanthorrhiza) ...... 1–C, 1–D Arrowroot (Maranta arundinacea) ...... 1–C, 1–D Artichoke, Chinese (Stachys affinis) ...... 1–C, 1–D Artichoke, Jerusalem (Helianthus tuberosus) ...... 1–C, 1–D Beet, garden (Beta vulgaris) ...... 1–A, 1–B Beet, sugar (Beta vulgaris) ...... 1–A

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TABLE 1—CROP GROUP 1: ROOT AND TUBER VEGETABLES—Continued

Related crop Commodities subgroups

Burdock, edible (Arctium lappa) ...... 1–A, 1–B Canna, edible (Queensland arrowroot) (Canna indica) ...... 1–C, 1–D Carrot (Daucus carota) ...... 1–A, 1–B Cassava, bitter and sweet (Manihot esculenta) ...... 1–C, 1–D (celery root) (Apium graveolens var. rapaceum) ...... 1–A, 1–B Chayote (root) (Sechium edule) ...... 1–C, 1–D , turnip-rooted ( bulbosum)...... 1–A, 1–B Chicory (Cichorium intybus) ...... 1–A, 1–B Chufa (Cyperus esculentus) ...... 1–C, 1–D Dasheen (taro) (Colocasia esculenta) ...... 1–C, 1–D Ginger (Zingiber officinale) ...... 1–C, 1–D Ginseng (Panax quinquefolius) ...... 1–A, 1–B Horseradish (Armoracia rusticana) ...... 1–A, 1–B Leren (Calathea allouia) ...... 1–C, 1–D Parsley, turnip-rooted (Petroselinum crispum var. tuberosum) ...... 1–A, 1–B (Pastinaca sativa) ...... 1–A, 1–B Potato (Solanum tuberosum) ...... 1–C Radish (Raphanus sativus) ...... 1–A, 1–B Radish, oriental (daikon) (Raphanus sativus subvar. longipinnatus) ...... 1–A, 1–B Rutabaga (Brassica campestris var. napobrassica) ...... 1–A, 1–B Salsify (oyster plant) (Tragopogon porrifolius)...... 1–A, 1–B Salsify, black (Scorzonera hispanica) ...... 1–A, 1–B Salsify, Spanish (Scolymus hispanicus) ...... 1–A, 1–B Skirret () ...... 1–A, 1–B Sweet potato (Ipomoea batatas) ...... 1–C, 1–D Tanier (cocoyam) (Xanthosoma sagittifolium) ...... 1–C, 1–D Turmeric (Curcuma longa) ...... 1–C, 1–D Turnip (Brassica rapa var. rapa) ...... 1–A, 1–B Yam bean (jicama, manoic pea) (Pachyrhizus spp.) ...... 1–C, 1–D Yam, true (Dioscorea spp.) ...... 1–C, 1–D

(iii) Table. The following table 2 iden- commodity(ies) for each subgroup, and tifies the crop subgroups for Crop lists all the commodities included in Group 1, specifies the representative each subgroup.

TABLE 2—CROP GROUP 1 SUBGROUP LISTING

Representative commodities Commodities

Crop Subgroup 1–A. Root vegetables subgroup. Carrot, radish, and sugar beet...... Beet, garden; beet, sugar; burdock, edible; carrot; celeriac; chervil, turnip-root- ed; chicory; ginseng; horseradish; parsley, turnip-rooted; parsnip; radish; rad- ish, oriental; rutabaga; salsify; salsify, black; salsify, Spanish; skirret; turnip. Crop Subgroup 1–B. Root vegetables (except sugar beet) subgroup. Carrot and radish...... Beet, garden; burdock, edible; carrot; celeriac; chervil, turnip-rooted; chicory; ginseng; horseradish; parsley, turnip-rooted; parsnip; radish; radish, oriental; rutabaga; salsify; salsify, black; salsify, Spanish; skirret; turnip. Crop Subgroup 1–C. Tuberous and corm vegetables subgroup. Potato...... ; arrowroot; artichoke, Chinese; artichoke, Jerusalem; canna, edible; cassava, bitter and sweet; chayote (root); chufa; dasheen; ginger; leren; po- tato; sweet potato; tanier; turmeric; yam bean; yam, true. Crop Subgroup 1–D. Tuberous and corm vegetables (except potato) subgroup. Sweet potato...... Arracacha; arrowroot; artichoke, Chinese; artichoke, Jerusalem; canna, edible; cassava, bitter and sweet; chayote (root); chufa; dasheen; ginger; leren; sweet potato; tanier; turmeric; yam bean; yam, true.

(2) Crop Group 2. Leaves of Root and (i) Representative commodities. Turnip Tuber Vegetables (Human Food or Ani- and garden beet or sugar beet. mal Feed) Group (Human Food or Ani- mal Feed) Group.

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(ii) Commodities. The following is a (3) Crop Group 3. Bulb Vegetables list of all the commodities included in (Allium spp.) Group. Crop Group 2: (i) Representative commodities. Onion, green; and onion, dry bulb. CROP GROUP 2: LEAVES OF ROOT AND TUBER (ii) Commodities. The following is a VEGETABLES (HUMAN FOOD OR ANIMAL list of all the commodities in Crop FEED) GROUP—COMMODITIES Group 3: Beet, garden (Beta vulgaris) Beet, sugar (Beta vulgaris) CROP GROUP 3: BULB VEGETABLES (ALLIUM Burdock, edible (Arctium lappa) SPP.) GROUP—COMMODITIES Carrot (Daucus carota) Garlic (Allium sativum) Cassava, bitter and sweet (Manihot esculenta) Garlic, great-headed (elephant) (Allium Celeriac (celery root) (Apium graveolens var. ampeloprasum var. ampeloprasum) rapaceum) Leek (Allium ampeloprasum, A. porrum, A. Chervil, turnip-rooted (Chaerophyllum tricoccum) bulbosum) Onion, dry bulb and green (Allium cepa, A. Chicory (Cichorium intybus) fistulosum) Dasheen (taro) (Colocasia esculenta) Onion, Welch (Allium fistulosum) Parsnip (Pastinaca sativa) Shallot (Allium cepa var. cepa) Radish (Raphanus sativus) (4) Crop Group 4. Leafy Vegetables Radish, oriental (daikon) (Raphanus sativus (Except Brassica Vegetables) Group. subvar. longipinnatus) (i) Representative commodities. Celery, Rutabaga (Brassica campestris var. napobrassica) head lettuce, leaf lettuce, and spinach Salsify, black (Scorzonera hispanica) (Spinacia oleracea). Sweet potato (Ipomoea batatas) (ii) Table. The following table 1 lists Tanier (cocoyam) (Xanthosoma sagittifolium) all the commodities included in Crop Turnip (Brassica rapa var. rapa) Group 4 and identifies the related crop Yam, true (Dioscorea spp.) subgroups.

TABLE 1—CROP GROUP 4: LEAFY VEGETABLES (EXCEPT BRASSICA VEGETABLES) GROUP

Related crop Commodities subgroups

Amaranth (leafy amaranth, Chinese spinach, tampala) (Amaranthus spp.) ...... 4–A Arugula (Roquette) (Eruca sativa) ...... 4–A Cardoon (Cynara cardunculus) ...... 4–B Celery (Apium graveolens var. dulce) ...... 4–B Celery, Chinese (Apium graveolens var. secalinum) ...... 4–B Celtuce (Lactuca sativa var. angustana) ...... 4–B Chervil (Anthriscus cerefolium) ...... 4–A Chrysanthemum, edible-leaved (Chrysanthemum coronarium var. coronarium) ...... 4–A Chrysanthemum, garland (Chrysanthemum coronarium var. spatiosum) ...... 4–A Corn salad (Valerianella locusta) ...... 4–A Cress, garden (Lepidium sativum) ...... 4–A Cress, upland (yellow rocket, winter cress) (Barbarea vulgaris) ...... 4–A Dandelion (Taraxacum officinale) ...... 4–A Dock (sorrel) (Rumex spp.) ...... 4–A Endive (escarole) (Cichorium endivia) ...... 4–A Fennel, Florence (finochio) (Foeniculum vulgare Azoricum Group) ...... 4–B Lettuce, head and leaf (Lactuca sativa) ...... 4–A Orach (Atriplex hortensis) ...... 4–A Parsley (Petroselinum crispum) ...... 4–A Purslane, garden (Portulaca oleracea) ...... 4–A Purslane, winter (Montia perfoliata) ...... 4–A Radicchio (red chicory) (Cichorium intybus) ...... 4–A Rhubarb (Rheum rhabarbarum) ...... 4–B Spinach (Spinacia oleracea) ...... 4–A Spinach, New Zealand (Tetragonia tetragonioides, T. expansa) ...... 4–A Spinach, vine (Malabar spinach, Indian spinach) (Basella alba) ...... 4–A Swiss chard (Beta vulgaris var. cicla) ...... 4–B

(iii) Table. The following table 2 iden- commodities for each subgroup, and tifies the crop subgroups for Crop lists all the commodities included in Group 4, specifies the representative each subgroup.

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TABLE 2—CROP GROUP 4 SUBGROUP LISTING

Representative commodities Commodities

Crop Subgroup 4–A. Leafy greens subgroup. Head lettuce and leaf lettuce, and spinach Amaranth; arugula; chervil; chrysanthemum, edible-leaved; chrysanthemum, (Spinacia oleracea). garland; corn salad; cress, garden; cress, upland; dandelion; dock; endive; lettuce; orach; parsley; purslane, garden; purslane, winter; radicchio (red chicory); spinach; spinach, New Zealand; spinach, vine. Crop Subgroup 4–B. Leaf petioles subgroup. Celery...... Cardoon; celery; celery, Chinese; celtuce; fennel, Florence; rhubarb; Swiss chard.

(5) Crop Group 5. Brassica (Cole) Leafy (ii) Table. The following table 1 lists Vegetables Group. all the commodities included in Crop (i) Representative commodities. Broc- Group 5 and identifies the related crop coli or cauliflower; cabbage; and mus- subgroups. tard greens.

TABLE 1—CROP GROUP 5: Brassica (COLE) LEAFY VEGETABLES

Related crop Commodities subgroups

Broccoli (Brassica oleracea var. botrytis) ...... 5–A Broccoli, Chinese (gai lon) (Brassica alboglabra) ...... 5–A Broccoli raab (rapini) (Brassica campestris) ...... 5–B Brussels sprouts (Brassica oleracea var. gemmifera) ...... 5–A Cabbage (Brassica oleracea) ...... 5–A Cabbage, Chinese (bok choy) (Brassica chinensis ) ...... 5–B Cabbage, Chinese (napa) (Brassica pekinensis) ...... 5–A Cabbage, Chinese mustard (gai choy) (Brassica campestris) ...... 5–A Cauliflower (Brassica oleracea var. botrytis) ...... 5–A Cavalo broccolo (Brassica oleracea var. botrytis) ...... 5–A Collards (Brassica oleracea var. acephala) ...... 5–B Kale (Brassica oleracea var. acephala) ...... 5–B Kohlrabi (Brassica oleracea var. gongylodes) ...... 5–A Mizuna (Brassica rapa Japonica Group) ...... 5–B Mustard greens (Brassica juncea) ...... 5–B Mustard spinach (Brassica rapa Perviridis Group) ...... 5–B Rape greens (Brassica napus) ...... 5–B

(iii) Table. The following table 2 iden- commodity(ies) for each subgroup, and tifies the crop subgroups for Crop lists all the commodities included in Group 5, specifies the representative each subgroup.

TABLE 2—CROP GROUP 5 SUBGROUP LISTING

Representative commodities Commodities

Crop Subgroup 5–A. Head and stem Brassica subgroup Broccoli or cauliflower; and cabbage ...... Broccoli; broccoli, Chinese; brussels sprouts; cabbage; cabbage, Chinese (napa); cabbage, Chinese mustard; cauliflower; cavalo broccolo; kohlrabi Crop Subgroup 5–B. Leafy Brassica greens subgroup. Mustard greens ...... Broccoli raab; cabbage, Chinese (bok choy); collards; kale; mizuna; mustard greens; mustard spinach; rape greens

(6) Crop Group 6. Legume Vegetables and one dried cultivar); pea (Pisum spp.; (Succulent or Dried) Group. (i) Representative commodities. Bean (Phaseolus spp.; one succulent cultivar

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one succulent cultivar and one dried Group 6 and identifies the related crop cultivar); and soybean. subgroups. (ii) Table. The following table 1 lists all the commodities included in Crop

TABLE 1—CROP GROUP 6: LEGUME VEGETABLES (SUCCULENT OR DRIED)

Related crop Commodities subgroups

Bean (Lupinus spp.) (includes grain lupin, sweet lupin, white lupin, and white sweet lupin) ...... 6–C Bean (Phaseolus spp.) (includes field bean, kidney bean, lima bean, navy bean, pinto bean, runner bean, snap bean, tepary bean, wax bean) ...... 6–A, 6–B, 6–C Bean (Vigna spp.) (includes adzuki bean, asparagus bean, blackeyed pea, catjang, Chinese longbean, cowpea, Crowder pea, moth bean, mung bean, rice bean, southern pea, urd bean, yardlong bean) ...... 6–A, 6–B, 6–C Broad bean (fava bean) (Vicia faba) ...... 6–B, 6–C Chickpea (garbanzo bean) (Cicer arietinum) ...... 6–C Guar (Cyamopsis tetragonoloba) ...... 6–C Jackbean (Canavalia ensiformis) ...... 6–A Lablab bean (hyacinth bean) (Lablab purpureus) ...... 6–C Lentil (Lens esculenta) ...... 6–C Pea (Pisum spp.) (includes dwarf pea, edible-pod pea, English pea, field pea, garden pea, green pea, snow pea, sugar snap pea) ...... 6–A, 6–B, 6–C Pigeon pea (Cajanus cajan) ...... 6–A, 6–B, 6–C Soybean (Glycine max) ...... N/A Soybean (immature seed) (Glycine max) ...... 6–A Sword bean (Canavalia gladiata) ...... 6–A

(iii) Table. The following table 2 iden- commodities for each subgroup, and tifies the crop subgroups for Crop lists all the commodities included in Group 6, specifies the representative each subgroup.

TABLE 2—CROP GROUP 6 SUBGROUP LISTING

Representative commodities Commodities

Crop Subgroup 6–A. Edible-podded legume vegetables subgroup. Any one succulent cultivar of edible-podded Bean (Phaseolus spp.) (includes runner bean, snap bean, wax bean); bean bean (Phaseolus spp.) and any one suc- (Vigna spp.) (includes asparagus bean, Chinese longbean, moth bean, culent cultivar of edible-podded pea (Pisum yardlong bean); jackbean; pea (Pisum spp.) (includes dwarf pea, edible-pod spp.).. pea, snow pea, sugar snap pea); pigeon pea; soybean (immature seed); sword bean. Crop Subgroup 6–B. Succulent shelled pea and bean subgroup. Any succulent shelled cultivar of bean Bean (Phaseolus spp.) (includes lima bean (green)); broad bean (succulent); (Phaseolus spp.) and garden pea (Pisum bean (Vigna spp.) (includes blackeyed pea, cowpea, southern pea); pea spp.).. (Pisum spp.) (includes English pea, garden pea, green pea); pigeon pea. Crop Subgroup 6–C. Dried shelled pea and bean (except soybean) subgroup Any one dried cultivar of bean (Phaseolus Dried cultivars of bean (Lupinus spp.) (includes grain lupin, sweet lupin, white spp.); and any one dried cultivar of pea lupin, and white sweet lupin); (Phaseolus spp.) (includes field bean, kidney (Pisum spp.). bean, lima bean (dry), navy bean, pinto bean; tepary bean; bean (Vigna spp.) (includes adzuki bean, blackeyed pea, catjang, cowpea, Crowder pea, moth bean, mung bean, rice bean, southern pea, urd bean); broad bean (dry); chickpea; guar; lablab bean; lentil; pea (Pisum spp.) (includes field pea); pigeon pea.

(7) Crop Group 7. Foliage of Legume (ii) Table. The following table 1 lists Vegetables Group. the commodities included in Crop (i) Representative commodities. Any Group 7. cultivar of bean (Phaseolus spp.), field pea (Pisum spp.), and soybean.

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TABLE 1—CROP GROUP 7: FOLIAGE OF LEGUME VEGETABLES GROUP

Representative commodities Commodities

Any cultivar of bean (Phaseolus spp.) and field Plant parts of any legume vegetable included in the legume vegetables that will pea (Pisum spp.), and soybean ( Glycine be used as animal feed. max).

(iii) Table. The following table 2 iden- modities for the subgroup, and lists all tifies the crop subgroup for Crop Group the commodities included in the sub- 7 and specifies the representative com- group.

TABLE 2—CROP GROUP 7 SUBGROUP LISTING

Representative commodities Commodities

Crop Subgroup 7–A. Foliage of legume vegetables (except soybeans) subgroup Any cultivar of bean (Phaseolus spp.), and Plant parts of any legume vegetable (except soybeans) included in the legume field pea (Pisum spp.). vegetables group that will be used as animal feed.

(8) Crop Group 8. Fruiting Vegetables Pepper (Capsicum spp.) (includes bell pepper, (Except Cucurbits) Group. chili pepper, cooking pepper, pimento, (i) Representative commodities. To- sweet pepper) mato, bell pepper, and one cultivar of Tomatillo (Physalis ixocarpa) non-bell pepper. Tomato (Lycopersicon esculentum) (ii) Commodities. The following is a (9) Crop Group 9. Cucurbit Vegetables list of all the commodities included in Group. Crop Group 8: (i) Representative commodities. Cucum- CROP GROUP 8: FRUITING VEGETABLES ber, muskmelon, and summer squash. (EXCEPT CUCURBITS)—COMMODITIES (ii) Table. The following table 1 lists Eggplant (Solanum melongena) all the commodities included in Crop Groundcherry (Physalis spp.) Group 9 and identifies the related sub- Pepino (Solanum muricatum) groups.

TABLE 1—CROP GROUP 9: CUCURBIT VEGETABLES

Related crop Commodities subgroups

Chayote (fruit) (Sechium edule) ...... 9–B Chinese waxgourd (Chinese preserving melon) (Benincasa hispida) ...... 9–B Citron melon (Citrullus lanatus var. citroides) ...... 9–A Cucumber (Cucumis sativus) ...... 9–B Gherkin (Cucumis anguria) ...... 9–B Gourd, edible (Lagenaria spp.) (includes hyotan, cucuzza); (Luffa acutangula, L. cylindrica) (includes hechima, Chinese okra) ...... 9–B Momordica spp. (includes balsam apple, balsam pear, bitter melon, Chinese cucumber) ...... 9–B Muskmelon (hybrids and/or cultivars of Cucumis melo) (includes true cantaloupe, cantaloupe, casaba, crenshaw melon, golden pershaw melon, honeydew melon, honey balls, mango melon, Persian melon, pineapple melon, Santa Claus melon, and snake melon) ...... 9–A Pumpkin (Cucurbita spp.) ...... 9–B Squash, summer (Cucurbita pepo var. melopepo) (includes crookneck squash, scallop squash, straightneck squash, vegetable marrow, zucchini) ...... 9–B Squash, winter (Cucurbita maxima; C. moschata) (includes butternut squash, calabaza, hubbard squash); (C. mixta; C. pepo) (includes acorn squash, spaghetti squash) ...... 9–B Watermelon (includes hybrids and/or varieties of Citrullus lanatus) ...... 9–A

(iii) Table. The following table 2 iden- lists all the commodities included in tifies the crop subgroups for Crop each subgroup. Group 9, specifies the representative commodities for each subgroup, and

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TABLE 2—CROP GROUP 9 SUBGROUP LISTING

Representative commodities Commodities

Crop Subgroup 9–A. Melon subgroup Cantaloupes ...... Citron melon; muskmelon; watermelon Crop Subgroup 9–B. Squash/cucumber subgroup One cultivar of summer squash and cucumber. Chayote (fruit); Chinese waxgourd; cucumber; gherkin; gourd, edible; Momordica spp.; pumpkin; squash, summer; squash, winter.

(10) Crop Group 10. Citrus Fruits Pear (Pyrus communis) (Citrus spp., Fortunella spp.) Group. Pear, oriental (Pyrus pyrifolia) (i) Representative commodities. Sweet Quince (Cydonia oblonga) orange; lemon and grapefruit. (12) Crop Group 12. Stone Fruits (ii) Commodities. The following is a Group. list of all the commodities in Crop (i) Representative commodities. Sweet Group 10: cherry or tart cherry; peach; and plum CROP GROUP 10: CITRUS FRUITS (CITRUS SPP., or fresh prune (Prunus domestica, FORTUNELLA SPP.) GROUP—COMMODITIES Prunus spp.) Calamondin (Citrus mitis×Citrofortunella mitis) (ii) Commodities. The following is a Citrus citron (Citrus medica) list of all the commodities included in Citrus hybrids (Citrus spp.) (includes Crop Group 12: chironja, tangelo, tangor) Grapefruit (Citrus paradisi) CROP GROUP 12: STONE FRUITS GROUP— Kumquat (Fortunella spp.) COMMODITIES Lemon (Citrus jambhiri, Citrus limon) Lime (Citrus aurantiifolia) Apricot (Prunus armeniaca) Mandarin (tangerine) (Citrus reticulata) Cherry, sweet (Prunus avium), Orange, sour (Citrus aurantium) Cherry, tart (Prunus cerasus) Orange, sweet (Citrus sinensis) Nectarine (Prunus persica) Pummelo (Citrus grandis, Citrus maxima) Peach (Prunus persica) Satsuma mandarin (Citrus unshiu) Plum (Prunus domestica, Prunus spp.) (11) Crop Group 11: Pome Fruits Plum, Chickasaw (Prunus angustifolia) Group. Plum, Damson (Prunus domestica spp. (i) Representative commodities. Apple insititia) and pear. Plum, Japanese (Prunus salicina) × (ii) Commodities. The following is a Plumcot (Prunus. armeniaca P. domestica) list of all the commodities included in Prune (fresh) (Prunus domestica, Prunus spp.) Crop Group 11: (13) Crop Group 13. Berries Group. (i) Representative commodities. Any CROP GROUP 11: POME FRUITS GROUP— COMMODITIES one blackberry or any one raspberry; and blueberry. Apple (Malus domestica) Crabapple (Malus spp.) (ii) Table. The following table 1 lists Loquat (Eriobotrya japonica) all the commodities included in Crop Mayhaw (Crataegus aestivalis, C. opaca, and C. Group 13 and identifies the related sub- rufula) groups.

TABLE 1—CROP GROUP 13: BERRIES GROUP

Related crop Commodities subgroups

Blackberry (Rubus eubatus) (including bingleberry, black satin berry, boysenberry, Cherokee blackberry, Chesterberry, Cheyenne blackberry, coryberry, darrowberry, dewberry, Dirksen thornless berry, Himalayaberry, hullberry, Lavacaberry, lowberry, Lucretiaberry, mammoth blackberry, marionberry, nectarberry, olallieberry, Oregon evergreen berry, phenomenalberry, rangeberry, ravenberry, rossberry, Shawnee blackberry, youngberry, and varieties and/or hybrids of these) ...... 13–A Blueberry (Vaccinium spp.) ...... 13–B Currant (Ribes spp.) ...... 13–B Elderberry (Sambucus spp.) ...... 13–B Gooseberry (Ribes spp.) ...... 13–B Huckleberry (Gaylussacia spp.) ...... 13–B Loganberry (Rubus loganobaccus) ...... 13–A

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TABLE 1—CROP GROUP 13: BERRIES GROUP—Continued

Related crop Commodities subgroups

Raspberry, black and red (Rubus occidentalis, Rubus strigosus, Rubus idaeus) ...... 13–A

(iii) Table. The following table 2 iden- commodities for each subgroup, and tifies the crop subgroups for Crop lists all the commodities included in Group 13, specifies the representative each subgroup.

TABLE 2—CROP GROUP 13 SUBGROUPS LISTING

Representative commodities Commodities

Crop Subgroup 13–A. Caneberry (blackberry and raspberry) subgroup. Any one blackberry or any one raspberry...... Blackberry; loganberry; red and black raspberry; cultivars and/or hybrids of these. Crop Subgroup 13–B. Bushberry subgroup.. Blueberry, highbush...... Blueberry, highbush and lowbush; currant; elderberry; gooseberry; huckleberry.

(14) Crop Group 14. Tree Nuts Group. Rye (Secale cereale) (i) Representative commodities. Almond Sorghum (milo) (Sorghum spp.) and pecan. Teosinte (Euchlaena mexicana) (ii) Commodities. The following is a Triticale (Triticum-Secale hybrids) list of all the commodities included in Wheat (Triticum spp.) Crop Group 14: Wild rice (Zizania aquatica)

CROP GROUP 14: TREE NUTS—COMMODITIES (16) Crop Group 16. Forage, Fodder and Straw of Cereal Grains Group. Almond (Prunus dulcis) Beech nut (Fagus spp.) (i) Representative commodities. Corn, Brazil nut (Bertholletia excelsa) wheat, and any other cereal grain crop. Butternut (Juglans cinerea) (ii) Commodities. The commodities in- Cashew (Anacardium occidentale) cluded in Crop Group 16 are: Forage, Chestnut (Castanea spp.) fodder, and straw of all commodities Chinquapin (Castanea pumila) Filbert (hazelnut) (Corylus spp.) included in the group cereal grains Hickory nut (Carya spp.) group. Macadamia nut (bush nut) (Macadamia spp.) (17) Crop Group 17. Grass Forage, Fod- Pecan (Carya illinoensis) der, and Hay Group. Walnut, black and English (Persian) (Juglans (i) Representative commodities. Ber- spp.) muda grass; bluegrass; and bromegrass (15) Crop Group 15. Cereal Grains or fescue. Group. (ii) Commodities. The commodities in- (i) Representative commodities. Corn cluded in Crop Group 17 are: Any grass, (fresh sweet corn and dried field corn), Gramineae family (either green or rice, sorghum, and wheat. cured) except sugarcane and those in- (ii) Commodities. The following is a cluded in the cereal grains group, that list of all the commodities included in will be fed to or grazed by livestock, all Crop Group 15: pasture and range grasses and grasses CROP GROUP 15: CEREAL GRAINS— grown for hay or silage. COMMODITIES (18) Crop Group 18. Nongrass Animal Barley (Hordeum spp.) Feeds (Forage, Fodder, Straw, and Buckwheat (Fagopyrum esculentum) Hay) Group. Corn (Zea mays) (i) Representative commodities. Alfalfa Millet, pearl (Pennisetum glaucum) and clover (Trifolium spp.) Millet, proso (Panicum milliaceum) Oats (Avena spp.) (ii) Commodities. The following is a Popcorn (Zea mays var. everta) list of all the commodities included in Rice (Oryza sativa) Crop Group 18:

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CROP GROUP 18: NONGRASS ANIMAL FEEDS Vetch, crown (Coronilla varia) (FORAGE, FODDER, STRAW, AND HAY) Vetch, milk (Astragalus spp). GROUP—COMMODITIES (19) Crop Group 19. Herbs and Spices Alfalfa (Medicago sativa subsp. sativa) Group. Bean, velvet (Mucuna pruriens var. utilis) (i) Representative commodities. Basil Clover (Trifolium spp., Melilotus spp.) (fresh and dried); black pepper; chive; Kudzu (Pueraria lobata) Lespedeza (Lespedeza spp.) and celery seed or seed. Lupin (Lupinus spp.) (ii) Table. The following table 1 lists Sainfoin (Onobrychis viciifolia); all the commodities included in Crop Trefoil (Lotus spp.) Group 19 and identifies the related sub- Vetch (Vicia spp.) groups.

TABLE 1—CROP GROUP 19: HERBS AND SPICES GROUP

Related crop Commodities subgroups

Allspice (Pimenta dioica) ...... 19–B Angelica () ...... 19–A Anise (anise seed) (Pimpinella anisum) ...... 19–B Anise, star (Illicium verum) ...... 19–B Annatto (seed) ...... 19–B Balm (lemon balm) (Melissa officinalis) ...... 19–A Basil (Ocimum basilicum) ...... 19–A Borage (Borago officinalis) ...... 19–A Burnet (Sanguisorba minor) ...... 19–A Camomile (Anthemis nobilis) ...... 19–A Caper buds (Capparis spinosa) ...... 19–B (Carum carvi) ...... 19–B Caraway, black (Nigella sativa) ...... 19–B Cardamom (Elettaria cardamomum) ...... 19–B Cassia bark (Cinnamomum aromaticum) ...... 19–B Cassia buds (Cinnamomum aromaticum) ...... 19–B Catnip (Nepeta cataria) ...... 19–A Celery seed (Apicum graveolens) ...... 19–B Chervil (dried) (Anthriscus cerefolium) ...... 19–A Chive (Allium schoenoprasum) ...... 19–A Chive, Chinese (Allium tuberosum) ...... 19–A Cinnamon (Cinnamomum verum) ...... 19–B Clary (Salvia sclarea) ...... 19–A Clove buds (Eugenia caryophyllata) ...... 19–B (cilantro or Chinese parsley) (leaf) (Coriandrum sativum) ...... 19–A Coriander (cilantro) (seed) (Coriandrum sativum) ...... 19–B Costmary (Chrysanthemum balsamita) ...... 19–A Culantro (leaf) () ...... 19–A Culantro (seed) (Eryngium foetidum) ...... 19–B (Cuminum cyminum) ...... 19–B Curry (leaf) (Murraya koenigii) ...... 19–A Dill (dillweed) (Anethum graveolens) ...... 19–A Dill (seed) (Anethum graveolens) ...... 19–B Fennel (common) (Foeniculum vulgare) ...... 19–B Fennel, Florence (seed) (Foeniculum vulgare Azoricum Group) ...... 19–B Fenugreek (Trigonella foenumgraecum) ...... 19–B Grains of paradise (Aframomum melegueta) ...... 19–B Horehound (Marrubium vulgare) ...... 19–A Hyssop (Hyssopus officinalis) ...... 19–A Juniper berry (Juniperus communis) ...... 19–B Lavender (Lavandula officinalis) ...... 19–A Lemongrass (Cymbopogon citratus) ...... 19–A (leaf) (Levisticum officinale) ...... 19–A Lovage (seed) (Levisticum officinale) ...... 19–B Mace (Myristica fragrans) ...... 19–B Marigold (Calendula officinalis) ...... 19–A Marjoram (Origanum spp.) (includes sweet or annual marjoram, wild marjoram or oregano, and pot marjoram) 19–A Mustard (seed) (Brassica juncea, B. hirta, B. nigra) ...... 19–B Nasturtium (Tropaeolum majus) ...... 19–A Nutmeg (Myristica fragrans) ...... 19–B Parsley (dried) (Petroselinum crispum) ...... 19–A Pennyroyal (Mentha pulegium) ...... 19–A Pepper, black (Piper nigrum) ...... 19–B Pepper, white ...... 19–B Poppy (seed) (Papaver somniferum ) ...... 19–B Rosemary (Rosemarinus officinalis) ...... 19–A

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TABLE 1—CROP GROUP 19: HERBS AND SPICES GROUP—Continued

Related crop Commodities subgroups

Rue (Ruta graveolens) ...... 19–A Saffron (Crocus sativus) ...... 19–B Sage (Salvia officinalis) ...... 19–A Savory, summer and winter (Satureja spp.) ...... 19–A Sweet bay (bay leaf) (Laurus nobilis) ...... 19–A Tansy (Tanacetum vulgare) ...... 19–A Tarragon (Artemisia dracunculus) ...... 19–A Thyme (Thymus spp.) ...... 19–A Vanilla (Vanilla planifolia) ...... 19–B Wintergreen (Gaultheria procumbens) ...... 19–A Woodruff (Galium odorata) ...... 19–A Wormwood (Artemisia absinthium) ...... 19–A

(iii) Table. The following table 2 iden- commodities for each subgroup, and tifies the crop subgroups for Crop lists all the commodities included in Group 19, specifies the representative each subgroup.

TABLE 2—CROP GROUP 19 SUBGROUPS

Representative commodities Commodities

Crop Subgroup 19–A. Herb subgroup. Basil (fresh and dried) and chive...... Angelica; balm; basil; borage; burnet; camomile; catnip; chervil (dried); chive; chive, Chinese, clary; coriander (leaf); costmary; culantro (leaf); curry (leaf); dillweed; horehound; hyssop; lavender; lemongrass; lovage (leaf); marigold; marjoram (Origanum spp.); nasturtium; parsley (dried); pennyroyal; rose- mary; rue; sage; savory, summer and winter; sweet bay; tansy; tarragon; thyme; wintergreen; woodruff; and wormwood. Crop Subgroup 19–B. Spice subgroup. Black pepper; and celery seed or dill seed...... Allspice; anise (seed); anise, star; annatto (seed); caper (buds); caraway; cara- way, black; cardamom; cassia (buds); celery (seed); cinnamon; clove (buds); coriander (seed); culantro (seed); cumin; dill (seed); fennel, common; fennel, Florence (seed); fenugreek; grains of paradise; juniper (berry); lovage (seed); mace; mustard (seed); nutmeg; pepper, black; pepper, white; poppy (seed); saffron; and vanilla.

[60 FR 26635, May 17, 1995]

Subpart C—Specific Tolerances tablished by the regulations in this subpart C are named by their common

EDITORIAL NOTE: Nomenclature changes to names wherever practicable, otherwise subpart C appear at 67 FR 41803–41808, June by their chemical names. 19, 2002; 67 FR 42393–42397, June 21, 2002; 68 FR (c) The analytical methods to be used 39430–39435, July 1, 2003; and 71 FR 74804– for determining whether pesticide resi- 74812, Dec. 13, 2006. dues, including negligible residues, in or on raw agricultural commodities are § 180.101 Specific tolerances; general provisions. in compliance with the tolerances es- tablished in this part 180 are identified (a) The tolerances established for among the methods contained or ref- pesticide chemicals in this subpart C apply to residues resulting from their erenced in the Food and Drug Adminis- application prior to harvest or slaugh- tration’s ‘‘Pesticide Analytical Man- ter, unless otherwise stated. Toler- ual’’ which is available from the Food ances are expressed in terms of parts and Drug Administration, Department by weight of the pesticide chemical per of Health, Education, and Welfare, 200 one million parts by weight of the raw C Street SW., Washington, DC 20204. agricultural commodity. (b) The poisonous and deleterious substances for which tolerances are es-

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§ 180.103 Captan; tolerances for resi- captan under the Rebuttable Presump- dues. tion Against Registration (RPAR) re- (a) Tolerances are established for res- view on the transmission of residues to idues of the fungicide captan (N- meat, milk, and egg from feeding cat- trichloromethylthio-4-cyclohexene-1,2- tle or poultry with raw agricultural dicarboximide) from preharvest and commodities or their byproducts when postharvest uses or combinations of such commodities have been treated such uses in or on the following raw ag- with captan: ricultural commodities: Parts per Commodity million Commodity Parts per million Almond ...... 2 Almond, hulls ...... 100 Apple ...... 25 Bean, dry, seed ...... 25 Apricot ...... 50 Bean, succulent ...... 25 Beet, garden, roots ...... 2 Potato ...... 25 Beet, garden, tops ...... 100 Blackberry ...... 25 Blueberry ...... 25 [46 FR 55114, Nov. 6, 1981, as amended at 49 Broccoli ...... 2 FR 17760, Sept. 28, 1983; 57 FR 36005, Aug. 12, Brussels sprouts ...... 2 Cabbage ...... 2 1992; 63 FR 57072, Oct. 26, 1998] Cantaloupe ...... 25 Carrot, roots ...... 2 § 180.106 Diuron; tolerances for resi- Cattle, fat ...... 0.05 dues. Cattle, meat ...... 0 .05 Cattle, meat byproducts ...... 0.05 (a)(1) General. Tolerances for residues Cauliflower ...... 2 of the diuron (3-(3,4- Celery ...... 50 dichlorophenyl)-1,1-dimethylurea) in or Cherry ...... 100 Collards ...... 2 on food commodities are established as Corn, sweet, kernel plus cob with husks re- follows: moved ...... 2 Cotton, undelinted seed ...... 2 Commodity Parts per Cucumber ...... 25 million Dewberry ...... 25 Eggplant ...... 25 Alfalfa ...... 2 Grape ...... 50 Apple ...... 1 Hog, fat ...... 0 .05 Artichoke, globe ...... 1 Hog, meat ...... 0 .05 Asparagus ...... 7 Hog, meat byproducts ...... 0 .05 Banana ...... 0.1 Kale ...... 2 Barley, grain ...... 1 Lettuce ...... 100 Barley, hay ...... 2 Mango ...... 50 Blackberry ...... 1 Melon, honeydew ...... 25 Blueberry ...... 1 Muskmelon ...... 25 Boysenberry ...... 1 Mustard greens ...... 2 Cattle, fat ...... 1 Nectarine ...... 50 Cattle, meat ...... 1 Onion, bulb ...... 25 Cattle, meat byproducts ...... 1 Onion, green ...... 50 Citrus, dried pulp ...... 4 Peach ...... 50 Clover, forage ...... 2 Pear ...... 25 Clover, hay ...... 2 Pea, dry, seed ...... 2 Corn in grain or ear form (including sweet corn, Pea, succulent ...... 2 field corn, popcorn) ...... 1 Plum, prune, fresh ...... 100 Corn, sweet, forage ...... 2 Pepper ...... 25 Corn, sweet, stover ...... 2 Pumpkin ...... 25 Cotton, undelinted seed ...... 1 Raspberry ...... 25 Currant ...... 1 Rutabagas (roots) ...... 2 Dewberry ...... 1 Soybean, dry ...... 2 Fruit, citrus, ...... 1 Soybean, succulent ...... 2 Goat, fat ...... 1 Spinach ...... 100 Goat, meat ...... 1 Squash, summer ...... 25 Goat, meat byproducts ...... 1 Squash, winter ...... 25 Gooseberry ...... 1 Strawberry ...... 25 Grape ...... 1 Tomato ...... 25 Grass crops (other than Bermuda grass) ...... 2 Turnip, greens ...... 2.0 Grass, hay (other than Bermudagrass, hay) ...... 2 Turnip, roots ...... 2 .0 Hog, fat ...... 1 Watermelon ...... 25.0 Hog, meat ...... 1 Hog, meat byproducts ...... 1 (b) The following tolerances for resi- Horse, fat ...... 1 Horse, meat ...... 1 dues of captan are established on an in- Horse, meat byproducts ...... 1 terim basis pending evaluation of Huckleberry ...... 1

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(c) Tolerances with regional registra- Commodity Parts per million tions. Tolerances with a regional reg- Loganberry ...... 1 istration as defined in § 180.1(n) are es- Nut ...... 0 .1 tablished for the combined residues of Oat, forage ...... 2 the herbicide diuron (3-(3,4- Oat, grain ...... 1 Oat, hay ...... 2 dichlorophenyl)-1,1-dimethylurea and Oat, straw ...... 2 its metabolites convertible to 3,4- Olive ...... 1 dichloroaniline) in or on the raw agri- Papaya ...... 0 .5 Peach ...... 0 .1 cultural commodities: Pear ...... 1 Pea ...... 1 Parts per Commodity million Pea, field, vines ...... 2 Pea, field, hay ...... 2 Cactus ...... 0 .05 Peppermint, tops ...... 2 Pineapple ...... 1 Potato ...... 1 (d) Indirect or inadvertent residues. Raspberry ...... 1 [Reserved] Rye, forage ...... 2 Rye, grain ...... 1 [63 FR 2164, Jan. 14, 1998, as amended at 63 Rye, straw ...... 2 FR 57072, Oct. 26, 1998; 64 FR 41305, July 30, Sheep, fat ...... 1 1999; 66 FR 28671, May 24, 2001; 67 FR 46883, Sheep, meat ...... 1 July 17, 2002; 69 FR 71717, Dec. 10, 2004; 72 FR Sheep, meat byproducts ...... 1 Sorghum, forage ...... 2 32540, June 13, 2007; 72 FR 35666, June 29, 2007] Sorghum, grain ...... 1 Sorghum, grain, stover ...... 2 § 180.108 Acephate; tolerances for resi- Sugarcane, cane ...... 1 dues. Trefoil, forage ...... 2 Trefoil, hay ...... 2 (a) General. (1) Tolerances are estab- Wheat, forage ...... 2 lished for combined residues of Wheat, grain ...... 1 acephate (O,S-dimethyl Wheat, hay ...... 2 Wheat, straw ...... 2 acetylphosphoramidothioate) and its Vetch, forage ...... 2 cholinesterase-inhibiting metabolite Vetch, hay ...... 2 O,S-dimethylphosphura-midothioate in Vetch, seed ...... 1 or on raw agricultural commodities as (2) Tolerances are established for the follows: combined residues of the herbicide Parts per diuron (3-(3,4-dichlorophenyl)-1,1- Commodity million dimethylurea and its metabolites con- Bean (succulent and dry form, of which no more vertible to 3,4-dichloroaniline, in or on than 1 ppm is O,S-dimethyl the following raw agricultural com- phosphoramidothioate) ...... 3 modities: Brussels sprouts (of which no more than 0.5 is O, S-dimethyl phosphoramido-thioate) ...... 3 .0 Cattle, fat ...... 0.1 Parts per Cattle, meat byproducts ...... 0.1 Commodity million Cattle, meat ...... 0 .1 Fish - freshwater finfish, farm raised ...... 2 .0 Cauliflower (of which no more than 0.5 is O, S- Peppermint, tops ...... 1 .5 dimethyl phosphoramido-thioate) ...... 2 .0 Spearmint, tops ...... 1 .5 Celery (of which no more than 1 ppm is O,S-di- methyl phosphoramidothioate) ...... 10 Cotton, undelinted seed ...... 2 (b) Section 18 emergency exemptions. Cotton, hulls ...... 4 Time-limited tolerances are estab- Cotton, meal ...... 8 lished for combined residues of the her- Cranberry (of which no more than 0.1 ppm is 0,S-dimethyl phosphoramidothioate) ...... 0.5 bicide diuron and its metabolites con- Egg ...... 0 .1 vertible to 3,4-dichloroaniline in con- Goat, fat ...... 0 .1 nection with use of the pesticide under Goat, meat byproducts ...... 0 .1 Goat, meat ...... 0.1 section 18 emergency exemptions Hog, fat ...... 0 .1 granted by EPA. These tolerances will Hog, meat byproducts ...... 0 .1 expire and are revoked on the dates Hog, meat ...... 0 .1 Horse, fat ...... 0 .1 specified in the following table. Horse, meat byproducts ...... 0 .1 Horse, meat ...... 0 .1 Expiration/ Lettuce, head (of which no more than 1 ppm is Commodity Parts per Revocation million date O,S-dimethyl phosphoramidothioate) ...... 10 Milk ...... 0.1 Catfish fillets ...... 2.0 06/30/08 Mint hay (of which no more than 1 ppm is O,S- dimethyl phosphoramidothioate) ...... 15.0

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acephate and its cholinesterase-inhib- Commodity Parts per million iting metabolite in or on the following Peanut ...... 0 .2 raw agricultural commodities: Pepper (of which no more than 1 ppm is O, S- Parts per dimethyl phosphoroamidothioate) ...... 4.0 Commodity million Poultry, fat ...... 0.1 Poultry, meat byproducts ...... 0.1 Nut, macadamia ...... 0.05 Poultry, meat ...... 0 .1 Sheep, fat ...... 0 .1 Sheep, meat byproducts ...... 0 .1 (d) Indirect or inadvertent residues. Sheep, meat ...... 0.1 [Reserved] Soybean, meal ...... 4 Soybean ...... 1 [63 FR 13542, Mar. 20, 1998, as amended at 67 FR 49615, July 31, 2002] (2) A food additive tolerance of 0.02 ppm is established for the combined § 180.110 Maneb; tolerances for resi- residues of acephate (O,S-dimethyl dues. acetylphosphoramidothioate) and its (a) General. Tolerances for residues of cholinesterase-inhibiting metabolite, the fungicide maneb (manganous methamidophos as follows: ethylenebisdithiocarbamate), cal- (i) In or on all food items (other than culated as zinc those already covered by a higher tol- ethylenebisdithiocarbamate, are estab- erance as a result of use on growing lished in or on raw agricultural com- crops) in food handling establishments. modities in the following table: (ii) The acephate may be present as a Expiration/ residue from applications of acephate Commodity Parts per Revocation in food handling establishments, in- million Date cluding food service, manufacturing Almond ...... 0.1 None and processing establishments, such as Apple ...... 2 None restaurants, cafeterias, supermarkets, Apricot ...... 10 None Banana (not more than 0.5 part per bakeries, breweries, dairies, meat million) shall be in the pulp after slaughtering and packing plants, and peel is removed and discarded canneries in accordance with the fol- (preharvest application only) ...... 4 None lowing prescribed conditions: Bean, dry, seed ...... 7 None Bean, succulent ...... 10 None (A) Application shall be limited sole- Beet, sugar, tops ...... 45 None ly to spot and/or crack and crevice Broccoli ...... 10 None treatment in food handling establish- Brussels sprouts ...... 10 None Cabbage ...... 10 None ments where food and food products are Cabbage, chinese ...... 10 None held, processed, prepared and served. Carrot,roots ...... 7 None Spray concentration shall be limited to Cauliflower ...... 10 None Celery ...... 5 None a maximum of 1.0 percent active ingre- Collards ...... 10 None dient. For crack and crevice treat- Corn, sweet, kernel plus cob with ments, equipment capable of delivering husks removed ...... 5 None a pin-stream of insecticide shall be Cranberry ...... 7 None Cucumber ...... 4 None used. For spot treatments, a coarse, Eggplant ...... 7 None low-pressure spray shall be used to Endive ...... 10 None avoid atomization or splashing of the Fig ...... 7 None Grape ...... 7 None spray. Contamination of food or food- Kale ...... 10 None contact surfaces shall be avoided. Kohlrabi ...... 10 None (B) To assure safe use of the insecti- Lettuce ...... 10 None Melon ...... 4 None cide, its label and labeling shall con- Mustard greens ...... 10 None form to that registered by the U.S. En- Nectarine ...... 10 None vironmental Protection Agency, and it Onion ...... 7 None shall be used in accordance with such Papaya ...... 10 None Peach ...... 10 None label and labeling. Pepper ...... 7 None (b) Section 18 emergency exemptions. Potato ...... 0.1 None [Reserved] Pumpkin ...... 7 None Squash, summer ...... 4 None (c) Tolerances with regional registra- Squash, winter ...... 4 None tion. Tolerances with regional registra- Tomato ...... 4 None tion, as defined in § 180.1(n), are estab- Turnip, greens ...... 10 None lished for the combined residues of Turnip, roots ...... 7 None

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(b) Section 18 emergency exemptions. A Commodity Parts per time-limited tolerance is established million for residues of the fungicide maneb Corn, fresh (including sweet, kernel plus cob (manganous with husks removed) ...... 2 ethylenebisdithiocarbamate), cal- Corn, grain, postharvest ...... 8 Cotton, undelinted seed ...... 2 culated as zinc Cowpea, forage ...... 135 ethylenebisdithiocarbamate, and its Cowpea, hay ...... 135 metabolite ethylenethiourea in connec- Cranberry ...... 8 Cucumber ...... 8 tion with use of the pesticide under a Currant ...... 8 section 18 emergency exemption grant- Date ...... 8 ed by EPA. The tolerance will expire Dewberry ...... 8 and is revoked on the date specified in Eggplant ...... 8 Egg (from application to poultry) ...... 0 .1 the following table: Fig ...... 8 Filbert ...... 1 Parts per Expiration/ Flax, seed ...... 0 .1 Commodity million revocation Flax, straw ...... 1 date Garlic ...... 8 Goat, fat (PRE-S) ...... 4 Walnut ...... 0.05 12/31/08 Goat, meat byproducts 1 (PRE-S) ...... 4 Goat, meat 1 (PRE-S) ...... 4 (c) Tolerances with regional registra- Gooseberry ...... 8 tions. [Reserved] Grapefruit ...... 8 Grape ...... 8 (d) Indirect or inadvertent residues. Grass ...... 135 [Reserved] Grass, hay ...... 135 Guava ...... 8 [62 FR 49924, Sept. 24, 1997, as amended at 63 Hog, fat (PRE-S) ...... 4 FR 57072, Oct. 26, 1998; 64 FR 13103, Mar. 17, Hog, meat byproducts 1 (PRE-S) ...... 4 1999; 64 FR 72284, Dec. 27, 1999; 66 FR 64773, Hog, meat 1 (PRE-S) ...... 4 Dec. 14, 2001; 68 FR 37764, June 25, 2003; 70 FR Hop ...... 1 37696, June 30, 2005; 70 FR 75739, Dec. 21, 2005] Horseradish ...... 8 Horse, fat (PRE-S) ...... 4 Horse, meat byproducts 1 (PRE-S) ...... 4 § 180.111 Malathion; tolerances for res- Horse, meat 1 (PRE-S) ...... 4 idues. Kumquat ...... 8 (a) General. (1) Tolerances are estab- Leek ...... 8 Lemon ...... 8 lished for residues of the insecticide Lentil, seed ...... 8 malathion (O,O-dimethyl Lespedeza, hay ...... 135 dithiophosphate of diethyl Lespedeza, seed ...... 8 Lespedeza, straw ...... 135 mercaptosuccinate) in or on the fol- Lime ...... 8 lowing food commodities: Loganberry ...... 8 Lupine, seed ...... 8 Commodity Parts per Mango ...... 8 million Melon ...... 8 Milk, fat (from application to dairy cows) ...... 0.5 Alfalfa ...... 135 Mushroom ...... 8 Almond, hulls ...... 50 Nectarine ...... 8 Almond, postharvest ...... 8 Nut, macadamia ...... 1 Apple ...... 8 Oat, grain, postharvest ...... 8 Apricot ...... 8 Okra ...... 8 Asparagus ...... 8 Onion (including green onion) ...... 8 Avocado ...... 8 Orange, sweet ...... 8 Barley, grain, postharvest ...... 8 Papaya ...... 1 Bean ...... 8 Parsnip ...... 8 Beet (including tops) ...... 8 Passionfruit ...... 8 Beet, sugar, roots ...... 1 Peach ...... 8 Beet, sugar, tops ...... 8 Peanut, hay ...... 135 Blackberry ...... 8 Peanut, postharvest ...... 8 Blueberry ...... 8 Pear ...... 8 Boysenberry ...... 8 Pea ...... 8 Carrot, roots ...... 8 Pea, field, vines ...... 8 Cattle, fat (PRE-S) ...... 4 Peavine, hay ...... 8 Cattle, meat byproducts 1 (PRE-S) ...... 4 Pecan ...... 8 Cattle, meat 1 (PRE-S) ...... 4 Peppermint ...... 8 Chayote fruit ...... 8 Pepper ...... 8 Chayote roots ...... 8 Pineapple ...... 8 Cherry ...... 8 Plum ...... 8 Chestnut ...... 1 Potato ...... 8 Clover ...... 135 Poultry, fat (PRE-S) ...... 4 Corn, forage ...... 8 Poultry, meat byproducts 1 (PRE-S) ...... 4

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amounts not exceeding 100 milligrams Commodity Parts per million per square foot. Poultry, meat 1 (PRE-S) ...... 4 (5) Malathion (O,O-dimethyl Plum, prune ...... 8 dithiophosphate of diethyl Pumpkin ...... 8 mercaptosuccinate) may be safely used Quince ...... 8 Radish ...... 8 in feed in accordance with the fol- Raspberry ...... 8 lowing conditions. Rice, grain, postharvest ...... 8 (i) A tolerance of 50 parts per million Rice, wild ...... 8 is established for residues of malathion Rutabagas ...... 8 Rye, grain, postharvest ...... 8 in dehydrated citrus pulp for cattle Safflower, seed ...... 0 .2 feed, when present as the result of the Salsify (including tops) ...... 8 application of the pesticide to bagged Shallots ...... 8 citrus pulp during storage. Whether or Sheep, fat (PRE-S) ...... 4 Sheep, meat byproducts 1 (PRE-S) ...... 4 not tolerances for residues of mala- Sheep, meat 1 (PRE-S) ...... 4 thion on the fresh fruit have been es- Sorghum, forage ...... 8 tablished under section 408 of the Act, Sorghum, grain, postharvest ...... 8 Soybean (dry and succulent) ...... 8 the total residue of malathion in the Soybean, forage ...... 135 dried citrus pulp shall not exceed 50 Soybean, hay ...... 135 parts per million. Spearmint, tops ...... 8 (ii) A tolerance of 10 parts per million Squash, summer and winter ...... 8 Strawberry ...... 8 is established for malathion in non- Sunflower, seed (Post-H) ...... 8 medicated cattle feed concentrate Sweet potato, roots ...... 1 blocks resulting from its application as Tangerine ...... 8 Tomato ...... 8 a pesticide to paper used in packaging Trefoil, forage ...... 135 the nonmedicated cattle feed con- Trefoil, hay ...... 135 centrate blocks. Turnip (including tops) ...... 8 (b) Section 18 emergency exemptions. Vegetable, brassica, leafy, group 5 ...... 8 Vegetables, leafy (except Brassica) ...... 8 [Reserved] Vetch, hay ...... 135 (c) Tolerances with regional registra- Vetch, seed ...... 8 tions. [Reserved] Vetch, straw ...... 135 Walnut ...... 8 (d) Indirect or inadvertent residues. Wheat, grain, postharvest ...... 8 [Reserved] 1 The tolerance level shall not be exceeded in any cut of [43 FR 22974, May 30, 1978, as amended at 43 meat or in any meat byproducts from cattle, goat, hog, horse, FR 45584, Oct. 3, 1978; 44 FR 38844, July 3, poultry, or sheep. 1979; 45 FR 76145, Nov. 18, 1980; 47 FR 42738, (2) Malathion may be safely used in Sept. 29, 1982; 47 FR 55226, Dec. 8, 1982; 52 FR accordance with the following condi- 45183, Nov. 25, 1987; 62 FR 66023, 66025, Dec. 17, tions: 1997; 65 FR 33694, May 24, 2000; 72 FR 35665, (i) It is incorporated into paper trays June 29, 2007] in amounts not exceeding 100 milli- § 180.114 Ferbam; tolerances for resi- grams per square foot. dues. (ii) Treated paper trays are intended for use only in the drying of grape (rai- (a) General. Tolerances for residues of sins). the fungicide ferbam (ferric dimethyl- (iii) Total residues of malathion re- dithiocarbamate), calculated as zinc sulting from drying of grape on treated ethylenebisdithiocarbamate, in or on trays and from application to grape be- raw agricultural commodities are es- fore harvest shall not exceed 12 parts tablished as follows: per million on processed ready-to-eat Parts per raisins. Commodity million (3) Residues of malathion in refined Apple ...... 71 safflower oil from application to the Apricot ...... 71 growing safflower plant shall not ex- Asparagus ...... 71 ceed 0.6 parts per million. Bean ...... 71 Blackberry ...... 71 (4) Malathion may be safely used for Blueberry ...... 71 the control of insects during the drying Boysenberry ...... 71 of grape (raisins) in compliance with Cabbage ...... 71 Cherry ...... 71 paragraph (a)(2) of this section by in- Cranberry ...... 71 corporation into paper trays in Cucumber ...... 71

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(c) Tolerances with regional registra- Commodity Parts per million tions. [Reserved] Dewberry ...... 71 (d) Indirect or inadvertent residues. Fruit, citrus ...... 71 [Reserved] Grape ...... 71 Guava ...... 71 [68 FR 39437, July 1, 2003, as amended at 71 Lettuce ...... 71 FR 54432, Sept. 15, 2006] Loganberry ...... 71 Mango ...... 71 § 180.117 S-Ethyl dipropylthiocarba- Nectarine ...... 71 Papaya ...... 71 mate; tolerances for residues. Peach ...... 71 Tolerances are established for neg- Pear ...... 71 Pea ...... 71 ligible residues (N) of the herbicide S- Raspberry ...... 71 ethyl dipropylthiocarbamate in or on Squash ...... 71 the following raw agricultural com- Tomato ...... 71 Youngberry ...... 71 modities:

1 Some of these tolerances were established on the basis of Parts per data acquired at the public hearings held in 1950 (formerly Commodity million § 180.101) and the remainder were established on the basis of pesticide petitions presented under the procedure specified Almond, hulls ...... 0 .1(N) in the amendment to the Federal Food, Drug, and Cosmetic Act by Pub. L. 518, 83d Congress (68 Stat. 511). Asparagus ...... 0.1(N) Bean, castor ...... 0 .1(N) (b) Section 18 emergency exemptions. Cotton, forage ...... 0.1(N) [Reserved] Cotton, undelinted seed ...... 0 .1(N) Flax, seed ...... 0 .1(N) (c) Tolerances with regional registra- Fruit, citrus ...... 0 .1(N) tions. [Reserved] Fruit, small ...... 0 .1(N) (d) Indirect or inadvertent residues. Grain, crop ...... 0 .1(N) Grass, forage ...... 0 .1(N) [Reserved] Legume, forage ...... 0 .1(N) [63 FR 57072, Oct. 26, 1998] Nut ...... 0 .1(N) Pineapple ...... 0.1(N) Safflower, seed ...... 0 .1(N) § 180.116 Ziram; tolerances for resi- Strawberry ...... 0 .1(N) dues. Sunflower, seed ...... 0.1(N) Vegetable, fruiting ...... 0.1(N) (a) General. Tolerances are estab- Vegetable, leafy ...... 0 .1(N) lished for residues of the fungicide Vegetable, root ...... 0 .1(N) ziram (zinc dimethyldithiocarbamate), Vegetable, seed and pod ...... 0 .1(N) calculated as zinc ethylenebisdithiocarbamate, in or on [42 FR 9178, Feb. 15, 1977] the following food commodities: § 180.121 Methyl parathion; tolerances Expiration/ for residues. Commodity Parts per Revocation million Date (a) General. Tolerances are estab- lished for residues of the insecticide Almond ...... 0.1 1 None Apple ...... 7.0 1 None parathion O, O-Dimethyl-O-p- Apricot ...... 7.0 1 None nitrophenyl thiophosphate (the methyl Beet, garden, roots ...... 7.0 1 1/15/07 homolog of parathion) in or on the fol- Beet, garden, tops ...... 7.0 1 1/15/07 Blackberry ...... 7.0 1 None lowing raw agricultural commodities: Blueberry ...... 7.0 1 None Cabbage ...... 7.0 1/15/07 Commodity Parts per Cauliflower ...... 7.0 1/15/07 million Cherry, sweet ...... 7.0 1 None Cherry, tart ...... 7.0 1 None Alfalfa, forage ...... 1.25 Grape ...... 7.0 None Alfalfa, hay ...... 5.0 Huckleberry ...... 7.0 None Almond ...... 0.1 Melon ...... 7.0 None Almond, hulls ...... 3 .0 Onion ...... 7.0 None Barley ...... 1 .0 Peach ...... 7.0 None Bean, dry, seed ...... 1 .0 Pear ...... 7.0 1 None Beet, sugar ...... 0 .1 Pecan ...... 0.1 None Beet, sugar, top ...... 0.1 Quince ...... 7.0 1 None Cabbage ...... 1 .0 Strawberry ...... 7.0 None Corn ...... 1.0 Tomato ...... 7.0 1 None Corn, forage ...... 1 .0 Cotton, undelinted seed ...... 0 .75 1 See footnote to § 180.114. Grass, forage ...... 1 .0 Hop ...... 1 .0 (b) Section 18 emergency exemptions. Oat ...... 1 .0 [Reserved] Onion ...... 1 .0

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Commodity Parts per § 180.122 Parathion; tolerances for res- million idues. Peanut ...... 1 .0 (a) General. Tolerances are estab- Pea, dry, seed ...... 1 .0 lished for residues of the insecticide Pea, field, vines ...... 1 .0 Pecan ...... 0 .1 parathion (O, O-Diethyl-O-p- Potato ...... 0 .1 nitrophenyl thiophosphate) in or on Rapeseed, seed ...... 0 .2 the following raw agricultural com- Rice, grain ...... 1 .0 Soybean ...... 0.1 modities: Soybean, hay ...... 1 .0 Sunflower, seed ...... 0.2 Parts per Expiration/ Sweet potato, roots ...... 0 .1 Commodity million Revocation Walnut ...... 0 .1 Date Wheat ...... 1.0 Alfalfa, forage ...... 1.25 12/31/05 Alfalfa, hay ...... 5.0 12/31/05 (b) Section 18 emergency exemptions. Barley ...... 1.0 12/31/05 [Reserved] Corn ...... 1.0 12/31/05 (c) Tolerances with regional registra- Corn, forage ...... 1.0 12/31/05 Cotton, undelinted seed ...... 0.75 12/31/05 tions. [Reserved] Rapeseed, seed ...... 0.2 12/31/05 (d) Indirect or inadvertent residues. Sorghum ...... 0.1 12/31/05 [Reserved] Sorghum, forage ...... 3.0 12/31/05 Sorghum, grain, stover ...... 3.0 12/31/05 (e) Revoked tolerances subject to the Soybean ...... 0.1 12/31/05 channel of trade provisions. The fol- Soybean, hay ...... 1.0 12/31/05 lowing table lists commodities for Sunflower, seed ...... 0.2 12/31/05 which methyl parathion use was un- Wheat ...... 1.0 12/31/05 lawful after December 31, 1999, and the (b) Section 18 emergency exemptions. revoked tolerances. Commodities with [Reserved] residues of methyl parathion resulting (c) Tolerances with regional registra- from lawful use are subject to the tions. [Reserved] channels of trade provisions of section (d) Indirect or inadvertent residues. 408(1)(5) of the FFDCA. [Reserved] Parts per Commodity million [67 FR 38603, June 5, 2002]

Apple ...... 1 § 180.123 Inorganic bromide residues Artichoke, globe ...... 1 resulting from fumigation with Beet, garden, tops ...... 1 methyl bromide; tolerances for resi- Beet (with or without tops) ...... 1 Broccoli ...... 1 dues. Brussels sprouts ...... 1 (a) General. (1) Tolerances are estab- Carrot, roots ...... 1 Cauliflower ...... 1 lished for residues of inorganic bro- Celery ...... 1 mides (calculated as Br) in or on the Cherry ...... 1 following food commodities which have Collards ...... 1 been fumigated with the antimicrobial Grape ...... 1 Kale ...... 1 agent and insecticide methyl bromide Kohlrabi ...... 1 after harvest (with the exception of Lettuce ...... 1 strawberry): Mustard greens ...... 1 Nectarine ...... 1 Parts per Peach ...... 1 Commodity million Pear ...... 1 Plum, prune, fresh ...... 1 Alfalfa, hay, postharvest ...... 50 .0 Rutabagas (with or without tops) ...... 1 Almond, postharvest ...... 200.0 Rutabaga tops ...... 1 Apple, postharvest ...... 5 .0 Spinach ...... 1 Apricot, postharvest ...... 20.0 Tomato ...... 1 Artichoke, jerusalem, postharvest ...... 30 .0 Trefoil, forage ...... 1.25 Asparagus, postharvest ...... 100.0 Trefoil, hay ...... 5 Avocado, postharvest ...... 75 .0 Turnip (with or without tops) ...... 1 Barley, grain, postharvest ...... 50 .0 Turnip, greens ...... 1 Bean, lima, postharvest ...... 50 .0 Vegetable, brassica, leafy, group 5 ...... 1 Bean, postharvest ...... 50.0 Vetch ...... 1 Bean, snap, succulent, postharvest ...... 50.0 Bean, succulent, postharvest ...... 50.0 Beet, garden, roots, postharvest ...... 30.0 [66 FR 1245, Jan. 5, 2001, as amended at 66 FR Beet, sugar, roots, postharvest ...... 30 .0 38955, July 26, 2001; 67 FR 38603, June 5, 2002; Blueberry, postharvest ...... 20.0 72 FR 35666, June 29, 2007] Butternut, postharvest ...... 200 .0

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Parts per Parts per Commodity million Commodity million

Cabbage, postharvest ...... 50 .0 Tomato, postharvest ...... 20 .0 Cantaloupe, postharvest ...... 20 .0 Turnip, roots, postharvest ...... 30 .0 Carrot, roots, postharvest ...... 30 .0 Walnut, postharvest ...... 200.0 Cashew, postharvest ...... 200.0 Watermelon, postharvest ...... 20 .0 Cherry, sweet, postharvest ...... 20 .0 Wheat ...... 50.0 Cherry, tart, postharvest ...... 20 Chestnut, postharvest ...... 200.0 (2) Inorganic bromide may be present Cippolini, bulb, postharvest ...... 50 .0 Citron, citrus, postharvest ...... 30.0 as a residue in certain processed food Cacao bean, roasted bean, postharvest ...... 50.0 in accordance with the following condi- Coconut, copra, postharvest ...... 100 .0 tions: Coffee, bean, green, postharvest ...... 75.0 Corn, field, grain, postharvest ...... 50.0 (i) When inorganic bromide residues Corn, pop, postharvest ...... 240 .0 are present as a result of fumigation of Corn, sweet, kernel plus cob with husks re- the processed food with methyl bro- moved, postharvest ...... 50.0 mide or from such fumigation in addi- Cotton, undelinted seed, postharvest ...... 200.0 Cucumber, postharvest ...... 30.0 tion to the authorized use of methyl Cumin, seed, postharvest ...... 100.0 bromide on the source raw agricultural Eggplant, postharvest ...... 20 .0 commodity, as provided for in this Garlic, postharvest ...... 50 .0 Ginger, roots, postharvest ...... 100.0 part, the total residues of inorganic Grapefruit, postharvest ...... 30.0 bromides (calculated as Br) shall not Grape, postharvest ...... 20.0 exceed the following levels: Hazelnut, postharvest ...... 200.0 (A) 400 parts per million in or on egg, Horseradish, postharvest ...... 30 .0 Kumquat, postharvest ...... 30.0 dried and herb, processed and spice. Lemon, postharvest ...... 30 .0 (B) 325 parts per million in or on Lime, postharvest ...... 30 .0 cheese, parmesan and cheese, roquefort Mango, postharvest ...... 20 .0 Melon, honeydew, postharvest ...... 20 .0 cheese. Muskmelon, postharvest ...... 20.0 (C) 250 parts per million in or on to- Nectarine, postharvest ...... 20.0 mato, concentrated products and fig, Nut, brazil, postharvest ...... 200 .0 dried fruit. Nut, hickory, postharvest ...... 200.0 Nut, macadamia, postharvest ...... 200.0 (D) 125 parts per million in or on Oat, postharvest ...... 50.0 processed food other than those listed Okra, postharvest ...... 30 .0 above. Onion, bulb, postharvest ...... 20 .0 Onion, green, postharvest ...... 20 .0 (ii) When inorganic bromide residues Orange, postharvest ...... 30.0 are present in malt beverage, fer- Papaya, postharvest ...... 20 .0 mented in accordance with 21 CFR Parsnip, roots, postharvest ...... 30.0 172.730(a)(2), the amount shall not ex- Peach, postharvest ...... 20.0 Peanut, postharvest ...... 200.0 ceed 25 parts per million (calculated as Pear, postharvest ...... 5.0 Br). Pea, blackeyed, postharvest ...... 50 .0 (iii) Where tolerances are established Pea, postharvest ...... 50.0 Pecan, postharvest ...... 200.0 on both the raw agricultural commod- Pepper, postharvest ...... 30 .0 ities and processed food made there- Pimento, postharvest ...... 30 .0 from, the total residues of inorganic Pineapple, postharvest ...... 20 .0 bromides in or on the processed food Pistachio, postharvest ...... 200 .0 Plum, postharvest ...... 20 .0 shall not be greater than those des- Pomegranate, postharvest ...... 100.0 ignated in paragraph (a)(2) of this sec- Potato, postharvest ...... 75 .0 tion, unless a higher level is estab- Pumpkin, postharvest ...... 20 .0 Quince, postharvest ...... 5 .0 lished elsewhere in this part. Radish, postharvest ...... 30.0 (3) Tolerances are established for res- Rice, grain, postharvest ...... 50.0 idues of inorganic bromides (calculated Rutabaga, roots, postharvest ...... 30.0 as Br) as follows: Rutabaga, tops, postharvest ...... 30.0 Rye, grain, postharvest ...... 50 .0 (i) 400 parts per million for residues Salsify, roots, postharvest ...... 30 .0 in or on dog food, resulting from fumi- Sorghum, grain, grain, postharvest ...... 50.0 gation with methyl bromide. Soybean, postharvest ...... 200 .0 (ii) 125 parts per million for residues Squash, summer, postharvest ...... 30 .0 Squash, winter, postharvest ...... 20 .0 in or on processed commodities for ani- Squash, zucchini, postharvest ...... 20.0 mal feedstuffs from barley, corn, grain Strawberry, postharvest ...... 60 .0 sorghum, oat, rice, rye and wheat, re- Sweet potato, postharvest ...... 75 .0 Tangerine, postharvest ...... 30.0 sulting directly from fumigation with Timothy, hay, postharvest ...... 50 .0 methyl bromide or from carryover and

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concentration of residues of inorganic piperonyl)ether] are established in or bromides from fumigation of the grains on the following food commodities: with methyl bromide. Parts per (b) Section 18 emergency exemptions. Commodity million [Reserved] (c) Tolerances with regional registra- Almond, postharvest ...... 8 tions. A tolerance with regional reg- Apple, postharvest ...... 8 Barley, postharvest ...... 20 istration, as defined in § 180.1(n), is es- Bean, postharvest ...... 8 tablished for residues of inorganic bro- Birdseed, mixtures, postharvest ...... 20 mides (calculated as Br) in or on the Blackberry, postharvest ...... 8 following food commodity grown in Blueberry, postharvest ...... 8 Boysenberry, postharvest ...... 8 soil fumigated with methyl bromide. Buckwheat, grain, postharvest ...... 20 Cattle, fat ...... 0.1 Parts per Cattle, meat byproducts ...... 0.1 Commodity million Cattle, meat ...... 0 .1 Ginger, roots, postharvest ...... 100 Cherry, sweet, postharvest ...... 8 Cherry, tart, postharvest ...... 8 Cacoa bean, roasted bean, postharvest ...... 8 (d) Indirect or inadvertent residues. Coconut, copra, postharvest ...... 8 [Reserved] Corn, field, grain, postharvest ...... 20 Corn, pop, postharvest ...... 20 [71 FR 74812, Dec. 13, 2006] Cotton, undelinted seed, postharvest ...... 8 Crabapple, postharvest ...... 8 § 180.123a Inorganic bromide residues Currant, postharvest ...... 8 in peanut hay and peanut hulls; Dewberry, postharvest ...... 8 statement of policy. Egg ...... 1 Fig, postharvest ...... 8 (a) Investigations by the Food and Flax, seed, postharvest ...... 8 Drug Administration show that peanut Goat, fat ...... 0 .1 hay and peanut shells have been used Goat, meat byproducts ...... 0 .1 Goat, meat ...... 0.1 as feed for meat and dairy animals. Gooseberry, postharvest ...... 8 While many growers now harvest pea- Grape, postharvest ...... 8 nuts with combines and leave the hay Guava, postharvest ...... 8 Hog, fat ...... 0 .1 on the ground to be incorporated into Hog, meat byproducts ...... 0 .1 the soil, some growers follow the prac- Hog, meat ...... 0 .1 tice of curing peanuts on the vines in a Horse, fat ...... 0 .1 stack and save the hay for animal feed. Horse, meat byproducts ...... 0 .1 Horse, meat ...... 0 .1 Peanut shells or hulls have been used Loganberry, postharvest ...... 8 to a minor extent as roughage for cat- Mango, postharvest ...... 8 tle feed. It has been established that Milk, fat ...... 0 .25 Muskmelon, postharvest ...... 8 the feeding to cattle of peanut hay and Oat, postharvest ...... 8 peanut hulls containing residues of in- Orange, postharvest ...... 8 organic bromides will contribute con- Peach, postharvest ...... 8 siderable residues of inorganic bro- Peanut, postharvest ...... 8 Pea, postharvest ...... 8 mides to the meat and milk. Pear, postharvest ...... 8 (b) There are no tolerances for inor- Pineapple, postharvest ...... 8 ganic bromides in meat and milk to Plum, prune, fresh, postharvest ...... 8 cover residues from use of such peanut Potato, postharvest ...... 0 .25 Poultry, fat ...... 3 hulls as animal feed. Peanut hulls con- Poultry, meat byproducts ...... 3 taining residues of inorganic bromides Poultry, meat ...... 3 from the use of methyl bromide are un- Raspberry, postharvest ...... 8 Rice, postharvest ...... 20 suitable as an ingredient in the feed of Rye, postharvest ...... 20 meat and dairy animals and should not Sheep, fat ...... 0 .1 be represented, sold, or used for that Sheep, meat byproducts ...... 0 .1 purpose. Sheep, meat ...... 0.1 Sorghum, grain, postharvest ...... 8 [58 FR 65555, Dec. 15, 1993] Sweet potato, postharvest ...... 0 .25 Tomato, postharvest ...... 8 Walnut, postharvest ...... 8 § 180.127 Piperonyl butoxide; toler- Wheat, postharvest ...... 20 ances for residues. (a) General. (1) Tolerances for resi- (2) Piperonyl butoxide may be safely dues of the insecticide piperonyl used in accordance with the following butoxide [(butyl carbityl)(6-propyl prescribed conditions:

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(i) It is used or intended for use in outer ply of multiwall paper bags of 50 combination with pyrethrins for con- pounds or more capacity. trol of insects: (C) Food treated in accordance with (A) In cereal grain mills and in stor- 21 CFR 178.3730. age areas for milled cereal grain prod- (D) Food, dried that contain 4 per- ucts, whereby the amount of piperonyl cent fat, or less, when present as a re- butoxide is at least equal to but not sult of migration from its use on the more than 10 times the amount of cloth of cotton bags of 50 pounds or pyrethrins in the formulation. more capacity constructed with waxed (B) On the outer ply of multiwall paper liners. paper bags of 50 pounds or more capac- (E) Food treated in accordance with ity in amounts not exceeding 60 milli- paragraph (a)(2)(i)(D) and (E) of this grams per square foot, whereby the section. amount of piperonyl butoxide is equal (iv) To assure safe use of the pes- to 10 times the amount of pyrethrins in ticide, its label and labeling shall con- the formulation. Such treated bags are form to that registered with the U.S. to be used only for food, dried. Environmental Protection Agency, and (C) On cotton bags of 50 pounds or it shall be used in accordance with more capacity in amounts not exceed- such label and labeling. ing 55 milligrams per square foot of (v) Where tolerances are established cloth, whereby the amount of piperonyl on both raw agricultural commodities butoxide is equal to 10 times the and processed food made therefrom, the amount of pyrethrins in the formula- total residues of piperonyl butoxide in tion. Such treated bags are constructed or on the processed food shall not be with waxed paper liners and are to be greater than that permitted by the used only for food, dried that contain 4 larger of the two tolerances. percent fat or less. (3) Piperonyl butoxide may be safely (D) In two-ply bags consisting of cel- used in accordance with the following lophane/polyolefin sheets bound to- prescribed conditions: gether by an adhesive layer when it is (i) It is used or intended for use in incorporated in the adhesive. The combination with pyrethrins for con- treated sheets shall contain not more trol of insects: than 50 milligrams of piperonyl butoxide per square foot (538 milli- (A) On the outer ply of multiwall grams per square meter). Such treated paper bags of 50 pounds or more capac- bags are to be used only for packaging ity in amounts not exceeding 60 milli- plum, prune, dried; grape, raisin; and grams per square foot. other fruit, dried and are to have a (B) On cotton bags of 50 pounds or maximum ratio of 3.12 milligrams of more capacity in amounts not exceed- piperonyl butoxide per ounce of fruit ing 55 milligrams per square foot of (0.10 milligram of piperonyl butoxide cloth. Such treated bags are con- per gram of product). structed with waxed paper liners and (E) In food processing and food stor- are to be used only for feed, dried that age areas: Provided, That the food is contain 4 percent fat or less. removed or covered prior to such use. (ii) It is used in combination with (ii) It is used or intended for use in pyrethrins, whereby the amount of combination with pyrethrins and N- piperonyl butoxide is equal to 10 times octylbicycloheptene dicarboximide for the amount of pyrethrins in the formu- insect control in accordance with 21 lation. Such treated bags are to be used CFR 178.3730. only for feed, dried. (iii) A tolerance of 10 parts per mil- (iii) A tolerance of 10 parts per mil- lion is established for residues of lion is established for residues of piperonyl butoxide in or on: piperonyl butoxide when present as the (A) Grain, cereal, milled fractions result of migration: when present therein as a result of its (A) In or on feed, dried from its use use in cereal grain mills and in storage on the outer ply of multiwall paper areas for milled cereal grain products. bags of 50 pounds or more capacity. (B) Food, dried when present as a re- (B) In or on feed, dried that contain sult of migration from its use on the 4 percent fat, or less, from its use on

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cotton bags of 50 pounds or more capac- Commodity Parts per ity constructed with waxed paper lin- million ers. Hog, meat byproducts ...... 0.1(N) (iv) To assure safe use of the pes- Hog, meat ...... 0.1(N) ticide, its label and labeling shall con- Horse, fat ...... 0.1(N) Horse, meat byproducts ...... 0.1(N) form to that registered with the U.S. Horse, meat ...... 0.1(N) Environmental Protection Agency. Loganberry, postharvest ...... 1 (v) Where tolerances are established Mango, postharvest ...... 1 Milk, fat ...... 0.5 on both the raw agricultural commod- Muskmelon, postharvest ...... 1 ities and food, processed made there- Oat, grain, postharvest ...... 1 from, the total residues of piperonyl Orange, postharvest ...... 1 butoxide in or on the processed food Peach, postharvest ...... 1 Peanut, postharvest ...... 1 shall not be greater than that per- Pea, postharvest ...... 1 mitted by the larger of the two toler- Pear, postharvest ...... 1 ances. Pineapple, postharvest ...... 1 Plum, prune, fresh, postharvest ...... 1 (b) Section 18 emergency exemptions. Potato, postharvest ...... 0.05 [Reserved] Poultry, fat ...... 0.2 (c) Tolerances with regional registra- Poultry, meat byproducts ...... 0.2 Poultry, meat ...... 0.2 tions. [Reserved] Raspberry, postharvest ...... 1 (d) Indirect or inadvertent residues. Rice, grain, postharvest ...... 3 [Reserved] Rye, postharvest ...... 3 Sheep, fat ...... 0.1(N) [71 FR 74813, Dec. 13, 2006] Sheep, meat byproducts ...... 0.1(N) Sheep, meat ...... 0.1(N) § 180.128 Pyrethrins; tolerances for Sorghum, grain, grain, postharvest ...... 1 residues. Sweet potato, postharvest ...... 0.05 Tomato, postharvest ...... 1 (a) General. (1) Tolerances for resi- Walnut, postharvest ...... 1 dues of the insecticide pyrethrins Wheat, postharvest ...... 3 (insecticidally active principles of Chrysanthemum cinerariaefolium) are es- (2) Pyrethrins may be safely used in tablished in or on the following food accordance with the following pre- commodities: scribed conditions: (i) It is used or intended for use in Commodity Parts per combination with piperonyl butoxide million for control of insects: Almond, postharvest ...... 1 (A) In cereal grain mills and in stor- Apple, postharvest ...... 1 age areas for milled cereal grain prod- Barley, postharvest ...... 3 ucts, whereby the amount of Bean, postharvest ...... 1 Birdseed, mixtures, postharvest ...... 3 pyrethrins is from 10 percent to 100 per- Blackberry, postharvest ...... 1 cent of the amount of piperonyl Blueberry, postharvest ...... 1 butoxide in the formulation. Boysenberry, postharvest ...... 1 Buckwheat, grain, postharvest ...... 3 (B) On the outer ply of multiwall Cattle, fat ...... 0.1(N) paper bags of 50 pounds or more capac- Cattle, meat byproducts ...... 0.1(N) ity in amounts not exceeding 6 milli- Cattle, meat ...... 0.1(N) Cherry, sweet, postharvest ...... 1 grams per square foot, whereby the Cherry, tart, postharvest ...... 1 amount of pyrethrins is equal to 10 per- Cacao bean, roasted bean, postharvest ...... 1 cent of the amount of piperonyl Coconut, copra, postharvest ...... 1 butoxide in the formulation. Such Corn, field, grain, postharvest ...... 3 Corn, pop, grain, postharvest ...... 3 treated bags are to be used only for Cotton, undelinted seed, postharvest ...... 1 food, dried. Crabapple, postharvest ...... 1 (C) On cotton bags of 50 pounds or Currant, postharvest ...... 1 Dewberry, postharvest ...... 1 more capacity in amounts not exceed- Egg ...... 0.1(N) ing 5.5 milligrams per square foot of Fig, postharvest ...... 1 cloth, whereby the amount of Flax, seed, postharvest ...... 1 pyrethrins is equal to 10 percent of the Goat, fat ...... 0.1(N) Goat, meat byproducts ...... 0.1(N) amount of piperonyl butoxide in the Goat, meat ...... 0.1(N) formulation. Such treated bags are Gooseberry, postharvest ...... 1 constructed with waxed paper liners Grape, postharvest ...... 1 Guava, postharvest ...... 1 and are to be used only for food, dried Hog, fat ...... 0.1(N) that contain 4 percent fat or less.

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(D) In two-ply bags consisting of cel- (3) Pyrethrins may be safely used in lophane/polyolefin sheets bound to- accordance with the following pre- gether by an adhesive layer when it is scribed conditions: incorporated in the adhesive. The (i) It is used or intended for use in treated sheets shall contain not more combination with piperonyl butoxide than 10 milligrams of pyrethrins per for control of insects: square foot (107.6 milligrams per square (A) On the outer ply of multiwall meter). Such treated bags are to be paper bags of 50 pounds or more capac- used only for packaging plum, prune, ity in amounts not exceeding 6 milli- dried; grape, raisin; and other fruit, grams per square foot. dried, and are to have a maximum (B) On cotton bags of 50 pounds or ratio of 0.31 milligram of pyrethrins more capacity in amounts not exceed- per ounce of fruit (0.01 milligram of ing 5.5 milligrams per square foot of pyrethrins per gram of product). cloth. Such treated bags are con- (E) In food processing areas and food structed with waxed paper liners and storage areas: Provided, That the food are to be used only for feed, dried that is removed or covered prior to such contain 4 percent fat or less. use. (ii) It is used in combination with piperonyl butoxide, whereby the (ii) It is used or intended for use in amount of pyrethrins is equal to 10 per- combination with piperonyl butoxide cent of the amount of piperonyl and N-octylbicycloheptene butoxide in the formulation. Such dicarboximide for insect control in ac- treated bags are to be used only for cordance with § 180.367(a)(2). feed, dried. (iii) A tolerance of 1 part per million (iii) A tolerance of 1 part per million is established for residues of pyrethrins is established for residues of pyrethrins in or on: when present as the result of migra- (A) Grain, cereal, milled fractions tion: when present as a result of its use in (A) In or on feed, dried from its use cereal grain mills and in storage areas on the outer ply of multiwall paper for grain, cereal, milled products. bags of 50 pounds or more capacity. (B) Food, dried when present as the (B) In or on feed, dried that contain result of migration from its use on the 4 percent fat, or less, from its use on outer ply of multiwall paper bags of 50 cotton bags of 50 pounds or more capac- pounds or more capacity. ity constructed with waxed paper lin- (C) Food treated in accordance with ers. § 180.367(a)(2). (iv) To assure safe use of the pes- (D) Food, dried that contain 4 per- ticide, its label and labeling shall con- cent fat, or less, when present as a re- form to that registered with the U.S. sult of migration from its use on the Environmental Protection Agency. cloth of cotton bags of 50 pounds or (v) Where tolerances are established more capacity constructed with waxed on both raw agricultural commodities paper liners. and food, processed made therefrom, (E) Food treated in accordance with the total residues of pyrethrins in or paragraphs (a)(2)(i)(D) and (a)(2)(i)(E)) on the food, processed shall not be of this section. greater than that permitted by the (iv) To assure safe use of the pes- larger of the two tolerances. ticide, its label and labeling shall con- (b) Section 18 emergency exemptions. form to that registered with the U.S. [Reserved] Environmental Protection Agency, and (c) Tolerances with regional registra- it shall be used in accordance with tions. [Reserved] such label and labeling. (d) Indirect or inadvertent residues. (v) Where tolerances are established [Reserved] on both the raw agricultural commod- [71 FR 74814, Dec. 13, 2006] ities and food, processed made there- from, the total residues of pyrethrins § 180.129 o-Phenylphenol and its so- in or on the food, processed shall not be dium salt; tolerances for residue. greater than that permitted by the Tolerances are established for com- larger of the two tolerances. bined residues of the fungicide o-

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phenylphenol and sodium o- (b) Section 18 emergency exemptions. phenylphenate, each expressed as o- [Reserved] phenylphenol, from postharvest appli- (c) Tolerances with regional registra- cation of either in or on the following tions. [Reserved] raw agricultural commodities: (d) Indirect or inadvertent residues. [Reserved] Parts per Commodity million [67 FR 49615, July 31, 2002]

Apple ...... 25 § 180.133 Lindane; tolerances for resi- Cantaloupe (NMT 10 ppm in edible portion) ...... 125 Carrot, roots ...... 20 dues. Cherry ...... 5 (a) General. Tolerances are estab- Citrus ...... 10 lished for residues of the insecticide Citron ...... 10 Cucumber ...... 10 lindane (gamma isomer of 1,2,3,4,5,6- Grapefruit ...... 10 hexachlorocyclohexane) in or on raw Kiwifruit ...... 20 agricultural commodities as follows: Kumquat ...... 10 Lemon ...... 10 Parts per Expiration/ Lime ...... 10 Commodity million Revocation Nectarine ...... 5 Date Orange, sweet ...... 10 Pepper, bell ...... 10 Broccoli ...... 1.0 4/26/07 Peach ...... 20 Brussels sprouts ...... 1.0 4/26/07 Pear ...... 25 .0 Cabbage ...... 1.0 4/26/07 Cattle, fat ...... 7.0 None Pineapple ...... 10 Cauliflower ...... 1.0 4/26/07 Plum, prune, fresh ...... 20 Goat, fat ...... 7.0 None Sweet potato, roots ...... 15 Hog, fat ...... 4.0 None Tangerine ...... 10 Horse, fat ...... 7.0 None Tomato ...... 10 Sheep, fat ...... 7.0 None

[46 FR 27938, May 22, 1981, as amended at 48 (b) Section 18 emergency exemptions. FR 32015, July 13, 1983] [Reserved] (c) Tolerances with regional registra- § 180.130 Hydrogen Cyanide; toler- tions. [Reserved] ances for residues. (d) Indirect or inadvertent residues. (a) General. A tolerance for residues [Reserved] of the insecticide hydrogen cyanide [68 FR 39438, July 1, 2003, as amended at 70 from postharvest fumigation as a re- FR 55286, Sept. 21, 2005] sult of application of sodium cyanide is established as follows: 50 parts per mil- § 180.136 Basic copper carbonate; tol- lion in or on Fruit, citrus. erance for residues. (b) Section 18 emergency exemptions. The tolerance for residues of the fun- [Reserved] gicide basic copper carbonate in or on (c) Tolerances with regional registra- pear from postharvest use of the chem- tions. [Reserved] ical is 3 parts per million of combined (d) Indirect or inadvertent residues. copper. [Reserved] § 180.142 2,4-D; tolerances for residues. [64 FR 39077, July 21, 1999] (a) General. (1) Tolerances are estab- § 180.132 Thiram; tolerances for resi- lished for residues of the herbicide, dues. plant regulator, and fungicide 2,4-D (a) General. Tolerances for residues of (2,4-dichlorophenoxyacetic acid) in or the fungicide thiram (tetramethyl on raw agricultural commodities as thiuram disulfide) in or on raw agricul- follows: tural commodities are established as Parts per follows: Commodity million

Apple ...... 5 Commodity Parts per million Apricot ...... 5 Fruit, citrus ...... 5 Apple ...... 7.0 Pear ...... 5 Peach ...... 7 .0 Potato ...... 0 .2 Strawberry ...... 7 .0 Quince ...... 5

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(i) The tolerance on apricot also in- ethylamine, heptylamine, cludes residues of 2,4-D (2,4- isopropanolamine, isopropylamine, dichlorophenoxyacetic acid) from the linoleylamine, methylamine, morpho- preharvest application of 2,4-D di- line, octylamine, oleylamine, N-oleyl- methylamine salt to apricot. 1,3-propylenediamine, propylamine, tri- (ii) The tolerance on Fruit, citrus ethanolamine, triethylamine, also includes residues 2,4-D from the triisopropanolamine, and preharvest application of 2,4-D iso- trimethyamine. propyl ester and 2,4-D butoxyethyl (ii) Esters. Residues on all the above ester and from the postharvest applica- may result from application of 2,4-D in tion of 2,4-D alkanolamine salts and acid form, or in the form of one or 2,4-D isopropyl ester to Fruit, citrus. more of the following esters: amyl (2) Tolerances are established for res- (pentyl), butoxyethoxypropyl, idues of 2,4-D at: butoxyethyl, butoxypolythylene glycol butyl ether, butoxypropyl, butyl, Parts per dipropylene glycol isobutyl ether, Commodity million ethoxyethoxyethyl, Barley, grain ...... 0 .5 ethoxyethoxypropyl, ethyl, Blueberry ...... 0 .1 ethoxypropyl, isobutyl, isooctyl (in- Corn, forage ...... 20 Corn, fresh, sweet, kernel plus cob with husks cluding, but not limited to, 2- removed ...... 0 .5 ethylhexyl, 2-ethyl-4-methylpentyl, Corn, grain ...... 0 .5 and 2-octyl), isopropyl, methyl, poly- Corn, stover ...... 20 Cranberry ...... 0 .5 ethylene glycol 200, polypropoxybutyl, Fruit, stone ...... 0 .2 polypropylene glycol, propylene glycol, Grape ...... 0 .5 propylene glycol butyl ether, propylene Grass hay ...... 300 Grass, pasture ...... 1,000 glycol isobutyl ether, Grass, rangeland ...... 1,000 tetrahydrofurfuryl, and tripropylene Hop ...... 0 .05 glycol isobutyl ether. Millet, forage ...... 20 (3) Tolerances are established for Millet, grain ...... 0 .5 Millet, straw ...... 20 negligible residues of 2,4-D from appli- Nut ...... 0 .2 cation of its dimethylamine salt to ir- Oat, forage ...... 20 rigation ditch banks in the Western Oat, grain ...... 0 .5 Pistachio ...... 0.2 United States in programs of the Bu- Rice, grain ...... 0 .1 reau of Reclamation, U.S. Department Rice, straw ...... 20 of Interior; cooperating water user or- Rice, wild ...... 0 .1 Rye, forage ...... 20 ganizations; the Bureau of Sport Fish- Rye, grain ...... 0.5 eries, U.S. Department of Interior; Ag- Sorghum, forage ...... 20 ricultural Research Service, U.S. De- Sorghum, grain ...... 0 .5 partment of Agriculture; and the Corps Sorghum, grain, stover ...... 20 Soybean ...... 0.02 of Engineers, U.S. Department of De- Sugarcane, cane ...... 2 fense. Where tolerances are established Sugarcane, forage ...... 20 at higher levels from other uses of 2,4- Wheat, forage ...... 20 Wheat, grain ...... 0 .5 D on the following crops, the higher tolerance applies also to residues from (i) Salts. Residues on all the above the irrigation ditch bank use cited in may result from application of 2,4-D in this paragraph. acid form, or in the form of one or The established tolerances follow: more of the following salts: Parts per (A) The inorganic salts: Ammonium, Commodity million lithium, potassium, and sodium. (B) The amine salts: Alkanolamines Avocado ...... 0 .1(N) Cotton, undelinted seed ...... 0 .1(N) of the ethanol and isopropanol series, Cucurbits ...... 0 .1(N) alkyl (C-12), alkylk (C-13), alkyl (C-14), Fruit, citrus ...... 0 .1(N) alkylamines derived from tall oil, Fruit, pome ...... 0.1(N) Fruit, small ...... 0 .1(N) amylamine, diethanolamine, Fruit, stone ...... 0 .1(N) diethylamine, diisopropanolamine, di- Grain, crop ...... 0 .1(N) methylamine, N,N-dimethyl- Grass, forage ...... 0 .1(N) Hop ...... 0 .1(N) linoleylamine, N,N- Legume, forage ...... 0 .1(N) dimethyloleyamine, ethanolamine, Nut ...... 0 .1(N)

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Parts per Parts per Commodity million Commodity million

Vegetable, fruiting ...... 0.1(N) Cattle, kidney ...... 2 Vegetable, leafy ...... 0 .1(N) Cattle, meat ...... 0 .2 Vegetable, root ...... 0 .1(N) Cattle, meat byproducts, except kidney ...... 0.2 Vegetable, seed and pod ...... 0 .1(N) Egg ...... 0 .05 Goat, fat ...... 0 .2 (4) A tolerance is established for resi- Goat, kidney ...... 2 dues of 2,4-D sodium salt and Goat, meat ...... 0.2 Goat, meat byproducts, except kidney ...... 0 .2 alkanolamine salts (of the ethanol and Hog, fat ...... 0 .2 isopropanol series), calculated as 2,4-D Hog, kidney ...... 2 (2,4-dichlorophenoxyacetic acid) as fol- Hog, meat ...... 0 .2 lows: Hog, meat byproducts, except kidney ...... 0 .2 Horse, fat ...... 0 .2 Horse, kidney ...... 2 Parts per Commodity million Horse, meat ...... 0 .2 Horse, meat byproducts, except kidney ...... 0 .2 Asparagus ...... 5 Milk ...... 0.1 Poultry ...... 0 .05 Sheep, fat ...... 0 .2 (5) A tolerance is established for resi- Sheep, kidney ...... 2 dues of 2,4-D from application of its Sheep, meat ...... 0.2 alkanolamine salts (of the ethanol and Sheep, meat byproducts, except kidney ...... 0 .2 isopropanol series) as follows: (9) A tolerance is established for resi- Parts per dues of 2,4-D from applications of its Commodity million dimethylamine salt or its Strawberry ...... 0 .05 butoxyethanol ester for Eurasian Watermilfoil control in programs con- (6) Tolerances are established for res- ducted by the Tennessee Valley Au- idues of 2,4-D from application of its di- thority in dams and reservoirs of the methylamine salt for water hyacinth TVA system as follows: control in ponds, lakes, reservoirs, marshes, bayous, drainage ditches, ca- Commodity Parts per nals, rivers and streams that are quies- million cent or slow moving in programs con- Fish ...... 1 .0 ducted by the Corps of Engineers or other Federal, State, or local public (10) A tolerance with regional reg- agencies. Where tolerances are estab- istration as defined in § 180.1(n) is es- lished at higher levels from other uses tablished for the residues of 2,4-D (2,4- of the dimethylamine salt of 2,4-D on dichlorophenoxyacetic acid). The toler- crops included within these commodity ance includes residues from the appli- groups, the higher tolerances also cation of 2,4-D and its N-oleyl-1,3- apply to residues from the aquatic uses propylenediamine salt on the following cited in this paragraph. The estab- raw agricultural commodity: lished tolerances follow: Parts per Commodity million Parts per Commodity million Raspberry ...... 0 .1 Crops in paragraph (c) of this section ...... 1 .0 Crop groupings in paragraph (c) of this section 1 .0 (11) [Reserved] Fish ...... 1 .0 (12) The following tolerances are es- Shellfish ...... 1 .0 tablished for residues of 2,4-D (2,4- (7) [Reserved] dichloro-phenoxyacetic acid) in the fol- (8) Tolerances are established for res- lowing processed feeds. Such residues idues of 2,4-dichlorophenoxyacetic acid may be present therein only as a result (2,4-d) and/or its metabolite, 2,4- of application to the growing crop of dichlorophenol (2,4-DCP) in food prod- the identified in this sec- ucts of animal origin as follows. tion: (i) 5 parts per million in sugarcane Commodity Parts per bagasse and sugarcane, molasses. million (ii) 2 parts per million in the milled Cattle, fat ...... 0.2 fractions derived from barley, oats,

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rye, and wheat to be ingested as animal Expiration/ Commodity Parts per Revocation feed or converted into animal feed. million Date (13) Tolerances are established for residues of the herbicide 2,4-D (2,4- Rice, wild, grain ...... 0.1 12/31/05 dichlorophenoxyacetic acid) as follows: (c) Tolerances with regional registra- (i) 5 ppm in sugarcane, molasses, re- tions. [Reserved] sulting from application of the herbi- (d) Indirect or inadvertent residues. cide to sugarcane fields. [Reserved] (ii) 2 ppm in the milled fractions (ex- cept flour) derived from barley, oats, [47 FR 620, Jan. 6, 1982, as amended at 48 FR 2323, Jan 19, 1983; 55 FR 39408, Sept. 27, 1990; rye, and wheat to be ingested as food or 61 FR 13429, Mar. 27, 1996; 62 FR 46907, Sept. to be converted to food. Such residues 5, 1997; 63 FR 34829, June 26, 1998; 64 FR 11799, may be present therein only as a result Mar. 10, 1999; 64 FR 69409, Dec. 13, 1999; 65 FR of application to the growing crop of 82940, Dec. 29, 2000; 67 FR 10631, Mar. 8, 2002; the herbicides identified in 40 CFR 68 FR 2247, Jan. 16, 2003; 70 FR 43309, July 27, 180.142. 2005] (iii) 0.1 ppm (negligible residue) in § 180.144 Cyhexatin; tolerances for res- water, potable. Such residues may be idues. present therein only: (a) General. Tolerances are estab- (A) As a result of the application of lished for combined residues of the pes- the dimethylamine salt of 2,4-D to irri- ticide cyhexatin gation ditch banks in the Western (tricyclohexylhydroxystannane; CAS United States in programs of the Bu- Reg. No. 13121–70–5) and its organotin reau of Reclamation; cooperating metabolites (calculated as cyhexatin) water user organizations; the Bureau of in or on the following food commod- Sport Fisheries, U.S. Department of ities: the Interior; Agricultural Research Expiration/ Service, U.S. Department of Agri- Parts per Commodity million Revocation culture; and the Corps of Engineers, Date U.S. Department of Defense. Orange, juice ...... 0.1 6/13/09 (B) As a result of the application of the dimethylamine salt of 2,4-D for (b) Section 18 emergency exemptions. water hyacinth control in ponds, lakes, [Reserved] reservoirs, marshes, bayous, drainage (c) Tolerances with regional registra- ditches, canals, rivers and streams that tions. [Reserved] are quiescent or slow moving in pro- (d) Indirect or inadvertent residues. grams of the Corps of Engineers or [Reserved] other Federal, State, or local public [65 FR 33708, May 24, 2000, as amended at 70 agencies. FR 55272, Sept. 21, 2005] (C) As a result of application of its dimethylamine salt or is § 180.145 Fluorine compounds; toler- ances for residues. butoxyethanol ester for Eurasian watermilfoil control in programs con- (a) General. (1) Tolerances are estab- ducted by the Tennessee Valley Au- lished for combined residues of the in- thority in dams and reservoirs of the secticidal fluorine compounds cryolite and synthetic cryolite (sodium alu- TVA system. minum fluoride) in or on the following (b) Section 18 emergency exemptions. A agricultural commodities: time-limited tolerance is established for 2,4-dichlorophenoxyacetic acid (2,4- Commodity Parts per D) in or on rice, wild, grain in connec- million tion with use of the pesticide under a Apricot ...... 7 section 18 emergency exemption grant- Blackberry ...... 7 Blueberry ...... 7 ed by EPA. The tolerance will expire Boysenberry ...... 7 on the dates specified in the following Broccoli ...... 7 table. Brussels sprouts ...... 7 Cabbage ...... 7 Cauliflower ...... 7

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Parts per Parts per Commodity million Commodity million

Collards ...... 7 Hog, meat ...... 20 Cranberry ...... 7 Herbs and spices group 19, postharvest ...... 70 Cucumber ...... 7 Milk, powdered ...... 5 .0 Dewberry ...... 7 Millet, grain, postharvest ...... 40.0 Eggplant ...... 7 Nut, pine, postharvest ...... 20 Fruit, citrus ...... 7 Nut, tree, Group 14, postharvest ...... 10 .0 Grape ...... 7 Oat, flour, postharvest ...... 75 .0 Kale ...... 7 Oat, grain, postharvest ...... 25 .0 Kohlrabi ...... 7 Oat, groats/rolled oats ...... 75 .0 Lettuce, head ...... 7 Peanut, postharvest ...... 15 Lettuce, leaf ...... 7 Pistachio, postharvest ...... 10 .0 Loganberry ...... 7 Rice, bran, postharvest ...... 31 .0 Melon ...... 7 Rice, flour, postharvest ...... 45 Nectarine ...... 7 Rice, grain, postharvest ...... 12.0 Peach ...... 7 Rice, hulls, postharvest ...... 35.0 Pepper ...... 7 Rice, polished rice, postharvest ...... 25.0 Plum, prune, fresh ...... 7 Rice, wild, grain, postharvest ...... 25 .0 Pumpkin ...... 7 Sorghum, grain, postharvest ...... 40.0 Raspberry ...... 7 Triticale, grain, postharvest ...... 40.0 Squash, summer ...... 7 Vegetable, legume, group 6, postharvest ...... 70 Squash, winter ...... 7 Wheat, bran, postharvest ...... 40 .0 Strawberry ...... 7 Wheat, flour, postharvest ...... 125 .0 Tomato ...... 7 Wheat, germ, postharvest ...... 130 .0 Youngberry ...... 7 Wheat, grain, postharvest ...... 40.0 Wheat, milled byproducts, postharvest ...... 130.0 Wheat, shorts, postharvest ...... 40.0 (2) Time-limited tolerances are estab- lished for residues of the insecticidal (b) Section 18 emergency exemptions. fluorine compounds cryolite and syn- [Reserved] thetic cryolite (sodium aluminum fluo- (c) Tolerances with regional registra- ride) in or on the commodities as fol- tions. Tolerances with regional reg- lows: istration, as defined by § 180.1(n), are established for the combined residues Expiration/ Parts per of the insecticidal fluorine compounds, Commodity million revocation date cryolite and synthetic cryolite (sodium Potato ...... 2.0 11/21/2001 aluminum fluoride), in or on the fol- Potato, processed potato waste ...... 22.0 11/21/2001 lowing raw agricultural commodities:

(3) Tolerances are established for res- Parts per Commodity million idues of fluoride in or on the following commodities from the postharvest fu- Kiwifruit ...... 15 migation with sulfuryl fluoride for the control of insects: (d) Indirect or inadvertent residues. [Reserved] Parts per Commodity million [71 FR 74815, Dec. 13, 2006] All processed food commodities not otherwise § 180.149 Mineral oil; tolerances for listed ...... 70 residues. Barley, bran, postharvest ...... 45 .0 Barley, flour, postharvest ...... 45.0 (a) General. (1) For the purposes of Barley, grain, postharvest ...... 15 .0 this section, the insecticide mineral oil Barley, pearled barley, postharvest ...... 45.0 Cattle, meat, dried ...... 40 is defined as the refined petroleum Cheese ...... 5 .0 fraction having the following charac- Cacao bean, roasted bean, postharvest ...... 20 teristics: Coconut, postharvest ...... 40 (i) Minimum flashpoint of 300 °F. Coffee, bean, green, postharvest ...... 15 Corn, field, flour, postharvest ...... 35 .0 (ii) Gravity of 27 to 34 by the Amer- Corn, field, grain, postharvest ...... 10.0 ican Petroleum Institute standard Corn, field, grits, postharvest ...... 10.0 method. Corn, field, meal, postharvest ...... 30 .0 ° Corn, pop, grain, postharvest ...... 10 .0 (iii) Pour point of 30 F maximum. Cotton, undelinted seed, postharvest ...... 70 (iv) Color 2 maximum by standards of Egg, dried ...... 900 the American Society for Testing Ma- Fruit, dried , postharvest (other than raisin) ...... 3 .0 terials. Ginger, postharvest ...... 70 Grain, aspirated fractions, postharvest ...... 55 .0 (v) Boiling point between 480 °F and Grape, raisin, postharvest ...... 7 .0 960 °F.

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(vi) Viscosity at 100 °F of 100 to 200 Environmental Protection Agency and seconds Saybolt. it shall be used in accordance with (vii) Unsulfonated residue of 90 per- such label or labeling. cent minimum. (iii) Residues of ethylene oxide in (viii) No sulfur compounds according ground spices from both postharvest to the United States Pharmacopeia application to whole spices and appli- test under Liquid Petrolatum. cation to the ground spices shall not (2) Tolerances for residues of mineral exceed the established tolerance of 50 oil as specified in paragraph (a)(1) of parts per million for residues in whole this section are established in or on the spices in paragraph (a)(1) of this sec- following food commodities: tion. (b) Section 18 emergency exemptions. Parts per Commodity million [Reserved] (c) Tolerances with regional registra- Corn, grain, postharvest ...... 200 tions. [Reserved] Sorghum, grain, grain, postharvest ...... 200 (d) Indirect or inadvertent residues. (b) Section 18 emergency exemptions. [Reserved] [Reserved] [65 FR 33695, May 24, 2000] (c) Tolerances with regional registra- tions. [Reserved] § 180.153 Diazinon; tolerances for resi- (d) Indirect or inadvertent residues. dues. [Reserved] (a) General. (1) Tolerances are estab- [68 FR 39438, July 1, 2003] lished for residues of the insecticide diazinon (O,O-diethyl O-[6-methyl-2-(1- § 180.151 Ethylene oxide; tolerances methylethyl)-4- for residues. pyrimidinyl]phosphorothioate; CAS (a) General. (1) Tolerances are estab- Reg. No. 333–41–5) in or on the following lished for residues of the antimicrobial raw agricultural commodities: agent and insecticide ethylene oxide, Parts per when used as a postharvest fumigant in Commodity million or on the following food commodities: Almond ...... 0.5 Almond, hulls ...... 3 .0 Parts per Apple ...... 0.5 Commodity million Apricot ...... 0 .5 Coconut, copra ...... 50 Banana ...... 0.2 Bean, lima ...... 0 .5 Spices, whole ...... 50 Bean, snap, succulent ...... 0 .5 Walnut, black ...... 50 Beet, garden, roots ...... 0 .75 Beet, garden, tops ...... 0 .7 (2) Ethylene oxide may be safely used Beet, sugar, roots ...... 0 .5 as a fumigant for the control of micro- Beet, sugar, tops ...... 10.0 Blackberry ...... 0 .5 organisms and insect infestation in Blueberry ...... 0 .5 ground spices and other processed nat- Carrot, roots ...... 0.75 ural seasoning materials, except mix- Cattle, fat ...... 0.7 tures to which salt has been added, in Celery ...... 0 .7 Cherry ...... 0.75 accordance with the following pre- Citrus ...... 0 .7 scribed conditions: Corn, field, forage ...... 40 .0 (i) Ethylene oxide, either alone or Corn, sweet, forage ...... 40 .0 Corn, sweet, kernel plus cob with husks re- admixed with carbon dioxide or dichlo- moved ...... 0 .7 rodifluoromethane, shall be used in Cranberry ...... 0 .5 amounts not to exceed that required to Cucumber ...... 0 .75 Endive ...... 0.7 accomplish the intended technical ef- Fig ...... 0 .5 fects. If used with dichlorodifluoro- Filbert ...... 0 .5 methane, the dichlorodifluoromethane Ginseng, roots ...... 0 .75 shall conform with the requirements Grape ...... 0 .75 Hop, dried cones ...... 0 .75 prescribed by 21 CFR 173.355 of this Kiwifruit ...... 0.75 chapter. Lettuce ...... 0.7 (ii) To assure safe use of the fumi- Loganberry ...... 0 .75 Melon ...... 0 .75 gant, its label and labeling shall con- Mushroom ...... 0 .75 form to that registered with the U.S. Nectarine ...... 0 .5

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(B) Application to areas, surfaces, or Commodity Parts per million utensils contacted by food, contamina- Olive ...... 1 . 0 tion of food and food contact surfaces, Onion, dry bulb ...... 0 .75 and the introduction of spray or dust Onion, green ...... 0 .75 into the air is to be avoided. Parsley, leaves ...... 0.75 Parsnip ...... 0.5 (C) For spot treatment, a coarse, low Peach ...... 0 .7 pressure spray shall be used. Applica- Pear ...... 0 .5 tion is limited to floor surfaces only Pea, field, hay ...... 10.0 and to 20 percent of the surface area. Pea, field, vines ...... 25 .0 Pea, succulent ...... 0 .5 Any individual spot treatment shall Pepper ...... 0 .5 not exceed 2 square feet. Pineapple ...... 0.5 (D) For crack and crevice treatment, Plum, prune, fresh ...... 0.5 Potato ...... 0 .1 equipment capable of delivering dust or Potato, sweet ...... 0 .1 a pin stream of spray directly into the Radicchio ...... 0.7 cracks and crevices shall be used. Radish ...... 0 .5 (ii) To assure safe use of the insecti- Raspberry ...... 0 .5 Rutabaga ...... 0 .75 cide, its label and labeling shall con- Sheep, fat ...... 0 .7 form to that registered by the U.S. En- Sheep, meat (fat basis) ...... 0 .7 vironmental Protection Agency, and it Sheep, meat byproducts (fat basis) ...... 0.7 Spinach ...... 0 .7 shall be used in accordance with such Squash, summer ...... 0 .5 label and labeling. Squash, winter ...... 0 .75 (3) A regulation is established per- Strawberry ...... 0 .5 mitting the use of the insecticide Swiss chard ...... 0.7 Tomato ...... 0.75 diazinon (O,O-diethyl O-[6-methyl-2-(1- Turnip, greens ...... 0.75 methylethyl)-4-pyrimidinyl] Turnip, roots ...... 0 .5 phosphorothioate; CAS Reg. No. 333–41– Vegetable, brassica, leafy, group 5 ...... 0.7 Walnut ...... 0 .5 5) in animal feed-handling establish- Watercress ...... 0 .7 ments in accordance with the following prescribed conditions: (2) A regulation is established per- (i) Application shall be limited solely mitting the use of the insecticide to spot and/or crack and crevice treat- diazinon (O, O-diethyl O-[6-methyl-2-(1- ment in animal feed handling estab- methylethyl)-4-pyrimidinyl] lishments, including feed manufac- phosphorothioate; CAS Reg. No. 333–41– turing and processing establishments 5) in food-handling establishments in such as stores, supermarkets, dairies, accordance with the following pre- meat slaughtering and packing plants, scribed conditions: and canneries, where feed and feed (i) Application shall be limited solely products are held, processed, and sold. to spot and/or crack and crevice treat- (A) Spray and dust concentrations ment in food-handling establishments, shall be limited to a maximum of 1 per- including food service, manufacturing, cent and 2 percent, respectively, of ac- and processing establishments, such as tive ingredient by weight. The spray restaurants, cafeterias, supermarkets, concentration limit of 1 percent shall bakeries, breweries, dairies, meat include, but not be limited to, encap- slaughtering and packing plants, and sulated formulations of the additive canneries where food and food products utilizing the encapsulating polymer are held, processed, and served. formed from the reaction of sebacoyl (A) Spray and dust concentrations chloride, polymethylene shall be limited to a maximum of 1 per- polyphenylisocyanate, ethylene- cent and 2 percent, respectively, of ac- diamine and/or diethylenetriamine. tive ingredient by weight. The spray (B) Application to areas, surfaces, or concentration limit of 1 percent shall utensils contacted by feed, contamina- include, but not be limited to, encap- tion of feed or feed contact surfaces, sulated formulations of the additive and the introduction of spray and dust utilizing the encapsulating polymer into the air is to be avoided. formed from the reaction of sebacoyl (C) For spot treatment, a coarse, low- chloride, polymethylene pressure spray shall be used. Applica- polyphenylisocyanate, ethylene- tion is limited to floor surfaces only diamine and/or diethylenetriamine. and to 20 percent of the surface area.

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Any individual spot treatment shall Parts per Expiration/ not exceed 2 square feet. Commodity Revocation million Date (D) For crack and crevice treatment, equipment capable of delivering dust or Boysenberry ...... 2.0 None a pin stream directly into cracks and Broccoli ...... 2.0 None Brussels sprouts ...... 2.0 None crevices shall be used. Cabbage ...... 2.0 None (ii) To assure safe use of the insecti- Cauliflower ...... 2.0 None cide, its label and labeling shall con- Celery ...... 2.0 None Cherry ...... 2.0 None form to that registered by the U.S. En- Clover ...... 2.0 None vironmental Protection Agency, and Clover, hay ...... 5.0 None shall be used in accordance with that Cotton, undelinted seed ...... 0.5 None Crabapple ...... 1.5 None label and labeling. Cranberry ...... 0.5 None (b) Section 18 emergency exemptions. Cucumber ...... 2.0 None [Reserved] Eggplant ...... 0.3 None Filbert ...... 0.3 None (c) Tolerances with regional registra- Fruit, citrus, group 10 ...... 2.0 None tions. Tolerances with regional reg- Grape ...... 4.0 None istration, as defined in § 180.1(n), are es- Loganberry ...... 2.0 None Melon ...... 2.0 None tablished for residues of the insecticide Onion ...... 2.0 None diazinon (O,O- diethyl O-(6-methyl-2-(1- Parsley, leaves ...... 5.0 None methylethyl)-4-pyrimidinyl]- Parsley, turnip rooted, roots ...... 2.0 None phosphorothioate; CAS Reg. No. 33–41– Peach ...... 2.0 None Pear ...... 1.5 None 5) in or on the following raw agricul- Pecan ...... 0.3 None tural commodities: Pepper ...... 0.3 None Pistachio ...... 0.3 None Parts per Plum, prune ...... 2.0 None Commodity million Potato ...... 0.2 None Quince ...... 1.5 None Radish, Chinese (roots) ...... 0 .1 Raspberry ...... 2.0 None Radish, Chinese (tops) ...... 0.1 Spinach ...... 2.0 None Strawberry ...... 2.0 None (d) Indirect or inadvertent residues. Sugarcane, cane ...... 0.3 6/30/00 Tomato, postharvest ...... 2.0 None [Reserved] Trefoil, hay ...... 5.0 None Walnut ...... 0.3 None [47 FR 42738, Sept. 29, 1982, as amended at 48 FR 14896, Apr. 6, 1983; 49 FR 37758, Sept. 26, (b) Section 18 emergency exemptions. 1984; 49 FR 47494, Dec. 5, 1984; 51 FR 46858, Dec. 29, 1986; 52 FR 32306, Aug. 27, 1987; 53 FR [Reserved] 23395, June 22, 1988; 53 FR 48260, Nov. 30, 1988; (c) Tolerances with regional registra- 63 FR 2165, 2167, Jan. 14, 1998; 66 FR 38955, tions. [Reserved] July 26, 2001; 69 FR 6567, Feb. 11, 2004; 70 FR (d) Indirect or inadvertent residues. 55267, Sept. 21, 2005] [Reserved] § 180.154 O,O-Dimethyl S-[(4-oxo-1,2,3- [65 FR 38752, June 22, 2000] benzotriazin-3(4H)- yl)methyl]phosphorodithioate; tol- § 180.155 1-Naphthaleneacetic acid; tol- erances for residues. erances for residues. (a) General. Tolerances for residues of (a) Tolerances are established for res- the insecticide O,O-dimethyl S-[(4-oxo- idues of the plant growth regulator 1- 1,2,3-benzotriazin-3(4H)- naphthaleneacetic acid in or on the fol- yl)methyl]phosphorodithioate in or on lowing raw agricultural commodities: the following raw agricultural com- Parts per modities: Commodity million

Expiration/ Apple ...... 1 Commodity Parts per Revocation Cherry, sweet ...... 0 .1 million Date Olive ...... 0 .1(N) Orange, sweet ...... 0 .1 Alfalfa ...... 2.0 None Pear ...... 1 Alfalfa, hay ...... 5.0 None Pineapple (from the application of the sodium Almond ...... 0.2 None salt to the growing crop) ...... 0 .05 Almond, hulls ...... 5.0 None Quince ...... 1 Apple ...... 1.5 None Tangerine ...... 0 .1 Bean, snap, succulent ...... 2.0 None Birdfoot trefoil ...... 2.0 None Blackberry ...... 2.0 None (b) Tolerances are established for res- Blueberry ...... 5.0 None idues of the ethyl ester of 1-

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naphthaleneacetic acid in or on the fol- Commodity Parts per lowing raw agricultural commodities: million Apple ...... 5 Parts per Apricot ...... 10 Commodity million Bean, dry, seed ...... 5 Bean, lima, succulent ...... 5 Apple ...... 1 Bean, snap, succulent ...... 5 Pear ...... 1 Blackberry ...... 5 Olive ...... 0 .1 Boysenberry ...... 5 Butternut ...... 5 Cantaloupe ...... 5 [46 FR 23238, Apr. 24, 1981, as amended at 47 Cherry ...... 5 FR 33692, Aug. 4, 1982; 48 FR 20054, May 4, Chestnut ...... 5 1983] Cotton, undelinted seed ...... 0 .1 Crabapple ...... 5 Cucumber ...... 5 § 180.157 Methyl 3-[(dimethoxyphos- Dewberry ...... 5 phinyl) oxy]butenoate, alpha and Eggplant ...... 5 beta isomers; tolerances for resi- Fig ...... 5 dues. Filbert ...... 5 Grapefruit ...... 10 (a) General. Tolerances are estab- Grape ...... 5 lished for residues of the insecticide Hay, peppermint ...... 25 Hazelnuts ...... 5 methyl 3- Hop ...... 30 [(dimethoxyphosphinyl)oxy]butenoate, Kumquat ...... 10 alpha and beta isomers, in or on the Lemon ...... 10 following raw agricultural commod- Lime ...... 10 Loganberry ...... 5 ities: Melon ...... 5 Muskmelon ...... 5 Commodity Parts per Nectarine ...... 10 million Nut, hickory ...... 5 Nut, macadamia ...... 5 Broccoli ...... 1 .0 Orange, sweet ...... 10 Cabbage ...... 1 .0 Peach ...... 10 Cauliflower ...... 1 .0 Pear ...... 5 Celery ...... 1 .0 Pecan ...... 5 Cucumber ...... 0 .2 Pepper ...... 5 Grape ...... 0 .5 Pimento ...... 5 Plum, prune, fresh ...... 5 Lettuce ...... 0.5 Pumpkin ...... 5 Melon (incl. Cantaloupe, Melon, honeydew, and Quince ...... 5 muskmelon, determined on the edible portion Raspberry ...... 5 with rind removed) ...... 0 .5 Spearmint, tops ...... 25 Pea ...... 0 .25 Squash, summer ...... 5 Pepper ...... 0 .25 Squash, winter ...... 5 Spinach ...... 1 .0 Strawberry ...... 5 Squash, summer ...... 0 .25 Tangerine ...... 10 Strawberry ...... 1 .0 Tea, dried ...... 45 Tomato ...... 0.2 Tomato ...... 5 Watermelon ...... 0.5 Walnut ...... 5 Watermelon ...... 5

(b) Section 18 emergency exemptions. (b) Section 18 emergency exemptions. [Reserved] [Reserved] (c) Tolerances with regional registra- (c) Tolerances with regional registra- tions. [Reserved] tions. [Reserved] (d) Indirect or inadvertent residues. (d) Indirect or inadvertent residues. [Reserved] [Reserved] [64 FR 41822, Aug. 2, 1999] [63 FR 34826, June 26, 1998, as amended at 72 FR 35665, June 29, 2007] § 180.163 1,1-Bis(p-chlorophenyl)-2,2,2- trichloroethanol; tolerances for res- § 180.167 Nicotine-containing com- idues. pounds; tolerances for residues. (a) General. Tolerances for residues of (a) General. Tolerances are estab- the insecticide 1,1-bis(p-chlorophenyl)- lished for residues of nicotine- con- 2,2,2-trichloroethanol in or on raw agri- taining compounds used as cultural commodities are established in or on the following raw agricultural as follows: commodities:

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Expiration/ Parts per Commodity Parts per Revocation Commodity million million Date Flax, seed ...... 5 Cucumber ...... 2.0 12/4/05 Fruit, citrus ...... 10 Lettuce ...... 2.0 12/4/05 Grape ...... 10 Tomato ...... 2.0 12/4/05 Grass ...... 100 Grass, hay ...... 100 (b) Section 18 emergency exemptions. Horseradish ...... 5 Kale ...... 12 [Reserved] Kohlrabi ...... 10 (c) Tolerances with regional registra- Lentil, seed ...... 10 tions. [Reserved] Lettuce ...... 10 (d) Indirect or inadvertent residues. Loganberry ...... 12 Melon ...... 10 [Reserved] Millet, proso, grain ...... 3 Millet, proso, straw ...... 100 [67 FR 35915, May 22, 2002, as amended at 69 Mustard greens ...... 12 FR 43924, July 23, 2004] Nectarine ...... 10 Okra ...... 10 § 180.169 Carbaryl; tolerances for resi- Olive ...... 10 dues. Oyster ...... 0.25 Parsley, leaves ...... 12 (a) General. (1) Tolerances are estab- Parsnip ...... 5 lished for residues of the insecticide Peach ...... 10 carbaryl (1-naphthyl N- Peanut ...... 5 Peanut, hay ...... 100 methylcarbamate), including its hy- Pea (with pods) ...... 10 drolysis product 1-naphthol, calculated Pea, field, vines ...... 100 as 1-naphthyl N-methylcarbamate, in Pecan ...... 1 Pepper ...... 10 or on the following food commodities: Pistachio ...... 1 Plum, prune, fresh ...... 10 Parts per Poultry, fat ...... 5 Commodity million Poultry, meat ...... 5 Alfalfa ...... 100 Potato ...... 0.2(N) Alfalfa, hay ...... 100 Prickly pear cactus, fruit ...... 12.0 Almond ...... 1 Prickly pear cactus, pads ...... 12.0 Almond, hulls ...... 40 Pumpkin ...... 10 Apricot ...... 10 Radish ...... 5 Asparagus ...... 10 Raspberry ...... 12 Banana ...... 10 Rice, grain ...... 5 Bean ...... 10 Rice, straw ...... 100 Beet, garden, roots ...... 5 Rutabagas ...... 5 Beet, garden, tops ...... 12 Salsify (roots) ...... 5 Beet, sugar, tops ...... 100 Salsify, tops ...... 10 Blackberry ...... 12 Sorghum, forage ...... 100 Blueberry ...... 10 Sorghum, grain ...... 10 Boysenberry ...... 12 Soybean ...... 5 Broccoli ...... 10 Soybean, forage ...... 100 Brussels sprouts ...... 10 Soybean, hay ...... 100 Cabbage ...... 10 Spinach ...... 12 Cabbage, chinese ...... 10 Squash, summer ...... 10 Carrot, roots ...... 10 Squash, winter ...... 10 Cauliflower ...... 10 Strawberry ...... 10 Celery ...... 10 Sunflower, seed ...... 1 Cherry ...... 10 Sweet potato, roots ...... 0.2 Chestnut ...... 1 Swiss chard ...... 12 Clover ...... 100 Tomato ...... 10 Clover, hay ...... 100 Trefoil, forage ...... 100.0 Collards ...... 12 Trefoil, hay ...... 100.0 Corn, sweet, kernel plus cob with husks re- Turnip, greens ...... 12 moved ...... 5 Turnip, roots ...... 5 Corn, forage ...... 100 Walnut ...... 1 Corn, stover ...... 100 Wheat, grain ...... 3 Cotton, undelinted seed ...... 5 Wheat, hay ...... 100 Cowpea ...... 5 Wheat, straw ...... 100 Cowpea, forage ...... 100 Cowpea, hay ...... 100 (2) Tolerances are established for res- Cranberry ...... 10 Cucumber ...... 10 idues of the insecticide carbaryl (1- Dandelion, leaves ...... 12 naphthyl N-methylcarbamate) includ- Dewberry ...... 12 ing its metabolites 1-naphthol Eggplant ...... 10 Endive ...... 10 (naphthyl-sulfate), 5,6- Filbert (hazelnuts) ...... 1 dihydrodihydroxycarbaryl, and 5,6-

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dihydrodihydroxy naphthol, calculated (d) Indirect or inadvertent residues. as 1-naphthyl N-methylcarbamate in or [Reserved] on the following food commodities: [65 FR 33695, May 24, 2000, as amended at 66 FR 38955, July 26, 2001; 67 FR 49615, July 31, Part per Commodity million 2002; 70 FR 44492, Aug. 3, 2005]

Cattle, fat ...... 0.1 § 180.172 Dodine; tolerances for resi- Cattle, kidney ...... 1 dues. Cattle, liver ...... 1 Cattle, meat ...... 0 .1 (a) Tolerances are established for res- Cattle, meat byproducts ...... 0.1 idues of the fungicide dodine (n- Goat, fat ...... 0 .1 dodecylguanidine acetate) in or on the Goat, kidney ...... 1 following raw agricultural commod- Goat, liver ...... 1 ities. Goat, meat ...... 0.1 Goat, meat byproducts ...... 0 .1 Parts per Hog, fat ...... 0 .1 Commodity million Hog, kidney ...... 1 Hog, liver ...... 1 Apple ...... 5.0 Hog, meat ...... 0 .1 Cherry, sweet ...... 5 .0 Hog, meat byproducts ...... 0 .1 Cherry, tart ...... 5 .0 Horse, fat ...... 0 .1 Meat ...... 0 Milk ...... 0 Horse, kidney ...... 1 Peach ...... 5 .0 Horse, liver ...... 1 Pear ...... 5 .0 Horse, meat ...... 0 .1 Pecan ...... 0 .3 Horse, meat byproducts ...... 0 .1 Strawberry ...... 5 .0 Sheep, fat ...... 0 .1 Walnut ...... 0 .3 Sheep, kidney ...... 1 Sheep, liver ...... 1 (b) Tolerances with regional registra- Sheep, meat ...... 0.1 Sheep, meat byproducts ...... 0 .1 tion, as defined in § 180.1(n), are estab- lished for residues of dodine in or on (3) A tolerance is established for resi- the following raw agricultural com- dues of the insecticide carbaryl (1- modities: naphthyl N-methylcarbamate), includ- Parts per ing its metabolites 1-naphthol Commodity million (naphthyl sulfate), 5,6-dihydro- dihydroxycarbaryl and 5-methoxy-6- Spinach ...... 12 .0 hydroxycarbaryl, calculated as 1- naphthyl N-methylcarbamate in or on [48 FR 37211, Aug. 17, 1983, as amended at 52 the food commodity milk at 0.3 ppm. FR 33236, Sept. 2, 1987] (4) Tolerances are established for res- § 180.173 Ethion; tolerances for resi- idues of the insecticide carbaryl (1- dues. naphthyl N-methylcarbamate) in or on (a) General. Tolerances are estab- the following food commodities: lished for residues of the insecticide Parts per ethion (O,O,O′,O′-tetraethyl S,S′-meth- Commodity million ylene bisphosphorodithioate) including Fruit, pome ...... 10.0 its oxygen analog (S- Pineapple ...... 2.0 [[(diethoxyphosphinothioyl)thio] meth- yl] O,O- diethyl phosphorothioate) in (b) Section 18 emergency exemptions. or on the following raw agricultural [Reserved] commodities: (c) Tolerances with regional registra- Expiration/ tions. Tolerances with regional reg- Parts per Commodity million Revocation istration are established for the insec- Date ticide carbaryl (1-napthyl N- Cattle, fat ...... 0.2 10/1/08 methylcarbamate) in or on the fol- Cattle, meat (fat basis) ...... 0.2 10/1/08 lowing food commodities. Cattle, meat byproducts ...... 0.2 10/1/08 Citrus, dried pulp ...... 25.0 10/1/08 Fruit, citrus, group 10 ...... 5.0 10/1/08 Parts per Commodity million Goat, fat ...... 0.2 10/1/08 Goat, meat ...... 0.2 10/1/08 Dill, fresh ...... 0.2 Goat, meat byproducts ...... 0.2 10/1/08 Hog, fat ...... 0.2 10/1/08

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(c) Tolerances with regional registra- Parts per Expiration/ Commodity Revocation tions. [Reserved] million Date (d) Indirect or inadvertent residues. Hog, meat ...... 0.2 10/1/08 [Reserved] Hog, meat byproducts ...... 0.2 10/1/08 Horse, fat ...... 0.2 10/1/08 [62 FR 64293, Dec. 5, 1997, as amended at 64 Horse, meat ...... 0.2 10/1/08 FR 11792, Mar. 10, 1999; 67 FR 35048, May 17, Horse, meat byproducts ...... 0.2 10/1/08 2002] Milk, fat, reflecting negligible resi- dues in milk ...... 0.5 10/1/08 § 180.176 Mancozeb; tolerances for res- Sheep, fat ...... 0.2 10/1/08 idues. Sheep, meat ...... 0.2 10/1/08 Sheep, meat byproducts ...... 0.2 10/1/08 (a) General. Tolerances for residues of a fungicide which is a coordination (b) Section 18 emergency exemptions. product of zinc ion and maneb (man- [Reserved] ganous ethylene-bisdithiocarbamate) (c) Tolerances with regional registra- containing 20 percent manganese, 2.5 tions.[Reserved] percent zinc, and 77.5 percent ethylene- (d) Indirect or inadvertent residues. bisdithiocarbamate (the whole product [Reserved] calculated as zinc ethylenebisdithiocarbamate), are es- [47 FR 42739, Sept. 29, 1982, as amended at 63 FR 2165, Jan. 14, 1998; 63 FR 57073, Oct. 26, tablished as follows: 1998; 67 FR 49615, July 31, 2002; 69 FR 43924, Parts per July 23, 2004] Commodity million § 180.175 Maleic hydrazide; tolerances Apple ...... 7 for residues. Asparagus (negligible residue) ...... 0 .1 Banana ...... 4.0 (a) General. (1) Tolerances for resi- Banana, pulp (no peel) ...... 0.5 dues of the herbicide and plant regu- Barley, grain ...... 5 Barley, milled feed fractions ...... 20 lator maleic hydrazide (1,2-dihydro-3,6- Barley, straw ...... 25 pyridazinedione) are established in or Beet, sugar ...... 2 on the following raw agricultural com- Beet, sugar, tops ...... 65 Carrot, roots ...... 2 modities: Celery ...... 5 Corn, forage ...... 5 Commodity Parts per Corn grain (except popcorn grain) ...... 0.1 million Corn, stover ...... 5 Cotton, undelinted seed ...... 0 .5 Onion, dry bulb ...... 15.0 Crabapple ...... 10 Potato ...... 50.0 Cranberry ...... 7 Cucumber ...... 4 (2) A food additive known as maleic Fennel ...... 10 hydrazide (1,2-dihydro-3,6- Fresh corn (including sweet corn, kernels plus cob with husk removed) ...... 0 .5 pyridazinedione) may be present in po- Grape ...... 7 tato, chips when used in accordance Kidney ...... 0.5 with the following conditions: Liver ...... 0.5 Melon ...... 4 (i) The food additive is present as a Oat, bran ...... 20 result of the application of a pesticide Oat, grain ...... 5 formulation containing maleic hydra- Oat, milled feed fractions ...... 20 Oat, straw ...... 25 zide to the growing potato plant in ac- Onion, dry bulb ...... 0 .5 cordance with directions registered by Papaya (whole fruit with no residue present in the U.S. Environmental Protection the edible pulp after the peel is removed and Agency. discarded) ...... 10 Peanut ...... 0 .5 (ii) The label of the pesticide formu- Peanut vine hay ...... 65 lation containing the food additive Pear ...... 10 conforms to labeling registered by the Popcorn grain ...... 0 .5 Quince ...... 10 U.S. Environmental Protection Agen- Rye, grain ...... 5 cy. Rye, milled feed fractions ...... 20 (iii) The food additive is present in an Rye, straw ...... 25 Squash, summer ...... 4 amount not to exceed 160 parts per mil- Tomato ...... 4 lion by weight of the finished food. Wheat, grain ...... 5 (b) Section 18 emergency exemptions. Wheat, milled feed fractions ...... 20 [Reserved] Wheat, straw ...... 25

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(b) Section 18 emergency exemptions. A (b) Section 18 emergency exemptions. time-limited tolerance is established [Reserved] for combined residues of the fungicide (c) Tolerances with regional registra- mancozeb, calculated as zinc tions. [Reserved] ethylenebisdithiocarbamate and it’s (d) Indirect or inadvertent residues. metabolite ETU in connection with use [Reserved] of the pesticide under a section 18 [68 FR 39439, July 1, 2003] emergency exemption granted by EPA. The tolerance will expire and is re- § 180.181 CIPC; tolerances for resi- voked on the dates specified in the fol- dues. lowing table. (a) General. Tolerances are estab- lished for residues of the plant regu- Parts per Expiration/ Commodity million Revocation lator and herbicide CIPC (isopropyl m- Date chlorocarbanilate) and its metabolite Ginseng ...... 2.0 12/31/09 1-hydroxy-2-propyl 3′-chlorocarbanilate (calculated as CIPC) in or on the fol- (c) Tolerances with regional registra- lowing raw agricultural commodities: tions. [Reserved] Parts per (d) Indirect or inadvertent residues. Commodity million [Reserved] Potato, postharvest ...... 50 [65 FR 33708, May 24, 2000, as amended at 65 FR 49924, Aug. 16, 2000; 66 FR 64773, Dec. 14, (b) Section 18 emergency exemptions. 2001; 68 FR 2247, Jan. 16, 2003; 69 FR 29458, [Reserved] May 24, 2004; 71 FR 76199, Dec. 20, 2006] (c) Tolerances with regional registra- tions. [Reserved] § 180.178 Ethoxyquin; tolerances for (d) Indirect or inadvertent residues. residues. [Reserved] (a) General. A tolerance is established [43 FR 52487, Nov. 13, 1978, as amended at 63 for residues of the plant regulator FR 57073, Oct. 26, 1998] ethoxyquin (1,2-dihydro-6-ethoxy-2,2,4- trimethylquinoline) from preharvest or § 180.182 Endosulfan; tolerances for postharvest use in or on the following residues. commodity: (a) General. (1) Tolerances are estab- Parts per lished for the combined residues of the Commodity million insecticide endosulfan, 6,7,8,9,10,10- hexachloro-1,5,5a,6,9,9a-hexahydro-6,9- Pear ...... 3 methano-2,4,3-benzodioxathiepin-3- oxide (alpha and beta isomers), and its (b) Section 18 emergency exemptions. metabolite endosulfan sulfate, [Reserved] 6,7,8,9,10,10-hexachloro-1,5,5a,6,9,9a- (c) Tolerances with regional registra- hexahydro-6,9-methano-2,4,3- tions. [Reserved] benzodioxathiepin-3,3-dioxide, in or on (d) Indirect or inadvertent residues. the following food commodities: [Reserved] Parts per [63 FR 57073, Oct. 26, 1998] Commodity million § 180.180 Orthoarsenic acid; tolerance Alfalfa, forage ...... 0.3 for residues. Alfalfa, hay ...... 1.0 Almond ...... 0.3 (a) General. A tolerance that expires Almond, hulls ...... 1 .0 on July 1, 1995, for combined As O is Apple ...... 1.0 2 3 Apple, wet pomace ...... 5 .0 established for residues of the defoliant Apricot ...... 2 .0 orthoarsenic acid in or on the following Barley, grain ...... 0 .3 food commodity: Barley, straw ...... 0 .4 Bean ...... 2 .0 Blueberry ...... 0 .3 Parts per Commodity million Broccoli ...... 3 .0 Brussels sprouts ...... 2 .0 Cotton, undelinted seed ...... 4 Cabbage ...... 4 .0 Carrot, roots ...... 0.2

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bined residues of the insecticide Commodity Parts per million endosulfan, 6,7,8,9,10,10-hexachloro- Cattle, fat ...... 13.0 1,5,5a,6,9,9a-hexahydro-6,9-methano- Cattle, liver ...... 5 .0 2,4,3-benzodioxathiepin-3-oxide (alpha Cattle, meat ...... 2 .0 and beta isomers), and its metabolite Cattle, meat byproducts, except liver ...... 1 .0 Cauliflower ...... 2 .0 endosulfan sulfate, 6,7,8,9,10,10- Celery ...... 8 .0 hexachloro-1,5,5a,6,9,9a-hexahydro-6,9- Cherry, sweet ...... 2 .0 methano-2,4,3-benzodioxathiepin-3,3-di- Cherry, tart ...... 2 .0 oxide, in or on dried tea (reflecting less Collards ...... 2.0 Corn, sweet, forage ...... 12 .0 than 0.1 ppm residues in beverage tea) Corn, sweet, kernel plus cob with husks re- resulting from application of the insec- moved ...... 0 .2 ticide to growing tea. Corn, sweet, stover ...... 14.0 Cotton, gin byproducts ...... 30 .0 (b) Section 18 emergency exemptions. Cotton, undelinted seed ...... 1 .0 [Reserved] Eggplant ...... 1.0 (c) Tolerances with regional registra- Goat, fat ...... 13 .0 tions. [Reserved] Goat, liver ...... 5.0 Goat, meat ...... 2.0 (d) Indirect or inadvertent residues. Goat, meat byproducts, except liver ...... 1 .0 [Reserved] Grape ...... 2 .0 Hazelnut ...... 0 .2 [65 FR 33696, May 24, 2000, as amended at 71 Hog, fat ...... 13 .0 FR 54433, Sept. 15, 2006] Hog, liver ...... 5 .0 Hog, meat ...... 2 .0 § 180.183 O,O-Diethyl S-[2-(ethyl- Hog, meat byproducts, except liver ...... 1 .0 thio)ethyl] phosphorodithioate; tol- Horse, fat ...... 13 .0 Horse, liver ...... 5 .0 erances for residues. Horse, meat ...... 2 .0 (a) General. Tolerances are estab- Horse, meat byproducts, except liver ...... 1 .0 lished for the combined residues of the Kale ...... 2 .0 Lettuce, head ...... 11.0 insecticide O,O-diethyl S-[2- Lettuce, leaf ...... 6 .0 (ethylthio)ethyl] phosphorodithioate Milk, fat ...... 2 .0 and its cholinesterase-inhibiting me- Mustard greens ...... 2.0 Mustard, seed ...... 0 .2 tabolites, calculated as demeton, in or Nectarine ...... 2 .0 on the following raw agricultural com- Nut, macadamia ...... 0.2 modities: Oat, grain ...... 0 .3 Oat, straw ...... 0.4 Expiration/ Pea, succulent ...... 2 .0 Commodity Parts per Revocation Peach ...... 2 .0 million Date Pear ...... 2 .0 Pecan ...... 0 .2 Barley, grain ...... 0.75 None Pepper ...... 2 .0 Barley, straw ...... 5.0 None Pineapple ...... 1.0 Bean, dry, seed ...... 0.75 None Pineapple, process residue ...... 20.0 Bean, lima ...... 0.75 None Plum ...... 2 .0 Bean, snap, succulent ...... 0.75 None Plum, prune ...... 2 .0 Broccoli ...... 0.75 None Potato ...... 0 .2 Brussels sprouts ...... 0.75 None Rapeseed, seed ...... 0 .2 Cabbage ...... 0.75 None Rye, grain ...... 0.3 Cauliflower ...... 0.75 None Rye, straw ...... 0 .3 Coffee, bean ...... 0.3 None Sheep, fat ...... 13 .0 Corn, field, forage ...... 5.0 12/9/03 Sheep, liver ...... 5.0 Corn, field, grain ...... 0.3 12/9/03 Sheep, meat ...... 2.0 Corn, field, stover ...... 5.0 12/9/03 Sheep, meat byproducts, except liver ...... 1 .0 Corn, pop, forage ...... 5.0 12/9/03 Spinach ...... 2 .0 Corn, pop, grain ...... 0.3 12/9/03 Strawberry ...... 2 .0 Corn, pop, stover ...... 5.0 12/9/03 Sugarcane, cane ...... 0.5 Corn, sweet, forage ...... 5.0 12/9/03 Sweet potato, roots ...... 0 .15 Corn, sweet, kernel plus cob with Tomato ...... 1.0 husks removed ...... 0.3 12/9/03 Turnip, roots ...... 0 .2 Corn, sweet, stover ...... 5.0 12/9/03 Turnip, tops ...... 2.0 Cotton, undelinted seed ...... 0.75 None Vegetable, cucurbit, group 9 ...... 1.0 Lettuce ...... 0.75 None Walnut ...... 0 .2 Oat, grain ...... 0.75 12/9/03 Watercress ...... 2 .0 Oat, hay ...... 5.0 12/9/03 Wheat, grain ...... 0 .3 Oat, straw ...... 5.0 12/9/03 Wheat, straw ...... 0 .4 Peanut ...... 0.75 None Pea ...... 0.75 None Pea, field, vines ...... 5.0 None (2) A tolerances of 24 parts per mil- Pecan ...... 0.75 12/9/03 lion (ppm) is established for the com- Pepper ...... 0.1 None

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Expiration/ Parts per Commodity Parts per Revocation Commodity million million Date Goat, meat ...... 1 Potato ...... 0.75 None Hog, fat ...... 1 Sorghum, forage ...... 5.0 None Hog, meat byproducts ...... 1 Sorghum, grain, grain ...... 0.75 None Hog, meat ...... 1 Sorghum, grain, stover ...... 5.0 None Horse, fat ...... 1 Soybean ...... 0.1 None Horse, meat byproducts ...... 1 Soybean, forage ...... 0.25 None Horse, meat ...... 1 Soybean, hay ...... 0.25 None Parsnip (with or without tops) ...... 0 .5 Spinach ...... 0.75 None Potato ...... 1 Sugarcane, cane ...... 0.3 None Sheep, fat ...... 1 Tomato ...... 0.75 None Sheep, meat byproducts ...... 1 Wheat, hay ...... 5.0 None Sheep, meat ...... 1 Wheat, grain ...... 0.3 None Sorghum, forage ...... 1 Wheat, straw ...... 5.0 None Sorghum, grain, grain ...... 0 .25 Sorghum, grain, stover ...... 1 Soybean, (dry or succulent) ...... 1 (b) Section 18 emergency exemptions. Soybean, forage ...... 1 [Reserved] Soybean, hay ...... 1 (c) Tolerances with regional registra- Wheat, forage ...... 0 .5 tions. Tolerances with regional reg- Wheat, grain ...... 0 .25 Wheat, hay ...... 0 .5 istration, as defined in § 180.1(n), are es- Wheat, straw ...... 0 .5 tablished for the combined residues of O,O-diethyl S-[2-(ethylthio)ethyl] (b) Section 18 emergency exemptions. phosphorodithioate and its cholin- [Reserved] esterase-inhibiting metabolites, cal- (c) Tolerances with regional registra- culated as demeton, in or on the fol- tions. Tolerances with regional reg- lowing raw agricultural commodities: istration, as defined in § 180.1(n), are es- tablished for residues of the herbicide Parts per Commodity million linuron 3-(3,4-dichlorophenyl)-1- methoxy-1-methylurea] in or on the Asparagus ...... 0.1 following food commodity:

(d) Indirect or inadvertent residues. Commodity Parts per [Reserved] million [63 FR 2165, Jan. 14, 1998, as amended at 63 Parsley, leaves ...... 0.25 FR 57073, Oct. 26, 1998; 66 FR 38955, July 26, 2001; 67 FR 41806, June 19, 2002; 67 FR 49615, (d) Indirect or inadvertent residues. July 31, 2002; 70 FR 44492, Aug. 3, 2005] [Reserved] [64 FR 41822, Aug. 2, 1999] § 180.184 Linuron; tolerances for resi- dues. § 180.185 Dimethyl tetrachlorotereph- (a) General. Tolerances are estab- thalate; tolerances for residues. lished for residues of the herbicide (a) General. Tolerances for combined linuron (3-(3,4-dichlorophenyl)-1- residues of the herbicide dimethyl methoxy-1-methylurea) in or on the tetrachlorotereph-thalate and its me- following food commodities: tabolites monomethyl Parts per tetrachloroterephthalate and Commodity million tetrachloroterephthalic acid (cal- culated as dimethyl Asparagus ...... 7.0 Carrot, roots ...... 1 tetrachloroterephthalate) are estab- Cattle, fat ...... 1 lished in or on the following raw agri- Cattle, meat byproducts ...... 1 cultural commodities: Cattle, meat ...... 1 Celery ...... 0 .5 Parts per Corn, field, forage ...... 1 Commodity million Corn, field, stover ...... 1 Corn, fresh (inc. sweet, kernel plus cob with Basil, dried leaves ...... 5 .0 husks removed) ...... 0 .25 Basil, fresh leaves ...... 20.0 Corn, grain (inc. pop) ...... 0 .25 Bean, field dry ...... 2 Corn, sweet, forage ...... 1 Bean, mung, seed ...... 2 Corn, sweet, stover ...... 1 Bean, snap, succulent ...... 2 Cotton, undelinted seed ...... 0 .25 Cantaloupe ...... 1 Goat, fat ...... 1 Celeriac ...... 2.0 Goat, meat byproducts ...... 1 Chicory, roots ...... 2 .0

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Commodity Parts per § 180.189 Coumaphos; tolerances for million residues. Chicory, tops ...... 5 .0 (a) General. Tolerances for residues of Chive ...... 5 .0 the insecticide coumaphos (O,O-diethyl Coriander, leaves ...... 5 .0 Corn, field, forage ...... 0 .4 O-3-chloro-4-methyl-2-oxo-2H-1- Corn, field, stover ...... 0 .4 benzopyran-7-yl phosphorothioate and Corn, grain (including field and pop) ...... 0.05 its oxygen analog (O,O-diethyl O-3- Corn, pop, forage ...... 0 .4 Corn, pop, stover ...... 0.4 chloro-4-methyl-2-oxo-2H-1- Corn, sweet, kernel plus cob with husks re- benzopyran-7-yl phosphate) in or on moved ...... 0 .05 food commodities as follows: Corn, sweet, forage ...... 0 .4 Corn, sweet, stover ...... 0 .4 Parts per Cotton, undelinted seed ...... 0 .2 Commodity million Cress, upland ...... 5 Cucumber ...... 1 Cattle, fat ...... 1.0 Dill ...... 5 .0 Cattle, meat ...... 1 .0 Eggplant ...... 1 Cattle, meat byproducts ...... 1.0 Garlic ...... 1 Goat, fat ...... 1 .0 Ginseng ...... 2 .0 Goat, meat ...... 1.0 Horseradish ...... 2 Goat, meat byproducts ...... 1 .0 Lettuce ...... 2 Hog, fat ...... 1 .0 Marjoram ...... 5 .0 Hog, meat ...... 1 .0 Melon, honeydew ...... 1 Hog, meat byproducts ...... 1 .0 Onion ...... 1 Honey ...... 0.15 Parsley, leaves ...... 5.0 Honeycomb ...... 45 .0 Parsley, dried leaves ...... 20.0 Horse, fat ...... 1 .0 Pea, blackeyed ...... 2 Horse, meat ...... 1 .0 Pepper ...... 2 Horse, meat byproducts ...... 1 .0 Pimento ...... 2 Milk, fat (=n in whole milk) ...... 0.5 Potato ...... 2 Radicchio ...... 5.0 Sheep, fat ...... 1 .0 Radish, oriental ...... 2.0 Sheep, meat ...... 1.0 Rutabagas ...... 2 Sheep, meat byproducts ...... 1 .0 Soybean ...... 2 Squash, summer ...... 1 (b) Section 18 emergency exemptions. Squash, winter ...... 1 [Reserved] Strawberry ...... 2 Sweet potato, roots ...... 2 (c) Tolerances with regional registra- Tomato ...... 1 tions. [Reserved] Turnip ...... 2 (d) Indirect or inadvertent residues. Turnip, greens ...... 5 Vegetable, brassica, leafy, group 5 ...... 5 [Reserved] Watermelon ...... 1 Yam, true, tuber ...... 2 [64 FR 39077, July 21, 1999, as amended at 65 FR 49936, Aug. 16, 2000; 67 FR 46883, July 17, (b) Section 18 emergency exemptions. 2002; 69 FR 29458, May 24, 2004; 72 FR 28876, [Reserved] May 23, 2007] (c) Tolerances with regional registra- § 180.190 Diphenylamine; tolerances tions. Tolerances with regional reg- for residues. istration, as defined in § 180.1(n), are es- tablished for the combined residues of (a) General. Tolerances for residues of dimethyl tetrachloroterephthalate and the plant regulator diphenylamine are its metabolites, calculated as dimethyl established in or on the following com- tetrachloroterephthalate, in or on the modities: following raw agricultural commod- Parts per ities: Commodity million

Parts per Apple, wet pomace ...... 30.0 Commodity million Apple from preharvest or postharvest use, in- cluding use of impregnated wraps ...... 10.0 Radish, roots ...... 2 .0 Cattle, fat ...... 0.01 Radish, tops ...... 15 .0 Cattle, liver ...... 0 .1 Cattle, meat byproducts, except liver ...... 0 .01 (d) Indirect or inadvertent residues. Cattle, meat ...... 0 .01 Goat, fat ...... 0 .01 [Reserved] Goat, liver ...... 0.1 [41 FR 27357, July 2, 1976, as amended at 43 Goat, meat byproducts, except liver ...... 0 .01 Goat, meat ...... 0.01 FR 29294, July 7, 1978; 49 FR 30700, Aug. 1, Horse, fat ...... 0 .01 1984; 52 FR 33237, Sept. 2, 1987; 54 FR 5080, Horse, liver ...... 0 .1 Feb. 1, 1989; 69 FR 51582, Aug. 20, 2004] Horse, meat byproducts, except liver ...... 0 .01

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Commodity Parts per § 180.198 Trichlorfon; tolerances for million residues. Horse, meat ...... 0 .01 Tolerances are established for resi- Milk ...... 0.01 dues of the insecticide dimethyl (2,2,2- Pear (post harvest) ...... 5 .0 trichloro-1-hydroxyethyl) phosphonate Sheep, fat ...... 0 .01 Sheep, liver ...... 0.1 in or on the following raw agricultural Sheep, meat byproducts, except liver ...... 0 .01 commodities: Sheep, meat ...... 0.01 Parts per Commodity million (b) Section 18 emergency exemptions. [Reserved] Cattle, fat ...... 0.1(N) Cattle, meat byproducts ...... 0.1(N) (c) Tolerances with regional registra- Cattle, meat ...... 0 .1(N) tions. [Reserved] (d) Indirect or inadvertent residues. A [45 FR 6104, Jan. 25, 1980, as amended at 47 time-limited tolerance is established FR 56136, Dec. 15, 1982; 63 FR 57073, Oct. 26, for the indirect or inadvertent residues 1998] of diphenylamine in or on the following commodity: § 180.200 Dicloran; tolerances for resi- dues. Expiration/ (a) General. (1) Tolerances are estab- Commodity Parts per Revocation million Date lished for residues of the fungicide 2,6- dichloro-4-nitroaniline in or on the fol- Pear ...... 10 12/1/01 lowing raw agricultural commodities. Unless otherwise specified, these toler- [64 FR 25848, May 13, 1999, as amended at 66 ances prescribed in this paragraph pro- FR 63198, Dec. 5, 2001; 72 FR 16283, Apr. 4, vide for residues from preharvest appli- 2007] cation only.

Parts per § 180.191 Folpet; tolerances for resi- Commodity million dues. Apricot, postharvest ...... 20 (a) General. Tolerances are estab- Bean, snap, succulent ...... 20 lished for the fungicide folpet (N- Carrot, roots, postharvest ...... 10 (trichloromethylthio)phthalimide) in Celery ...... 15 Cherry, sweet, postharvest ...... 20 or on raw agricultural commodities as Cucumber ...... 5 follows: Endive ...... 10 Garlic ...... 5 Parts per Grape ...... 10 Commodity million Lettuce ...... 10 Nectarine, postharvest ...... 20 Apple ...... 25 Onion ...... 10 Avocado ...... 25 Peach, postharvest ...... 20 Plum, prune, fresh, postharvest ...... 15 Cranberry ...... 25 Potato ...... 0.25 Cucumber ...... 15 Rhubarb ...... 10 Grape ...... 25 Sweet potato, postharvest ...... 10 Hop, dried cones ...... 120 Tomato ...... 5 Lettuce ...... 50 Melon ...... 15 (2) Unless otherwise specified, these Onion, dry bulb ...... 15 tolerances prescribed in this section Strawberry ...... 25 provide for residues from preharvest Tomato ...... 25 application only. (b) Section 18 emergency exemptions. (b) Section 18 emergency exemptions. [Reserved] [Reserved] (c) Tolerances with regional registra- (c) Tolerances with regional registra- tions. [Reserved] tions. [Reserved] (d) Indirect or inadvertent residues. (d) Indirect or inadvertent residues. [Reserved] [Reserved] [46 FR 27938, May 22, 1981, as amended at 63 [61 FR 37222, July 17, 1996, as amended at 68 FR 162, Jan. 5, 1998; 63 FR 57073, Oct. 26, 1998; FR 10388, Mar. 5, 2003; 69 FR 52192, Aug. 25, 64 FR 13096, Mar. 17, 1999; 67 FR 35048, May 17, 2004] 2002]

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§ 180.202 p-Chlorophenoxyacetic acid; Commodity Parts per tolerances for residues. million (a) General. A tolerance is established Mustard greens ...... 2 for the combined residues of the plant Orange, sweet ...... 2 Pear ...... 2 regulator p-chlorophenoxyacetic acid Pea ...... 2 and its metabolite p-chlorophenol to Pecan ...... 0.1 inhibit embryonic root development in Pepper ...... 2 Potato ...... 0.2 or on the following food commodity: Poultry, meat byproducts ...... 0.02 Safflower, seed ...... 0.1 Commodity Parts per Sheep, meat byproducts ...... 0.02 million Sorghum, forage ...... 0.2 Sorghum, grain ...... 0.1 Bean, mung, sprouts ...... 0.2 Soybean ...... 0.05 Soybean, forage ...... 2 (b) Section 18 emergency exemptions. Soybean, hay ...... 2 [Reserved] Spinach ...... 2 (c) Tolerances with regional registra- Swiss chard ...... 2 Tangerine ...... 2 tions. [Reserved] Tomato ...... 2 (d) Indirect or inadvertent residues. Turnip, greens ...... 2 [Reserved] Turnip, roots ...... 2 Wheat, grain ...... 0.04 [68 FR 39439, July 1, 2003, as amended at 71 Wheat, hay ...... 2 FR 56398, Sept. 27, 2006] Wheat, straw ...... 2 1There are no U.S. registrations as of August 16, 1995. § 180.204 Dimethoate including its oxy- gen analog; tolerances for residues. (b) Section 18 emergency exemptions. [Reserved] (a) General. Tolerances are estab- (c) Tolerances with regional registra- lished for total residues of the insecti- tions. Tolerances with regional reg- cide dimethoate (O,O-dimethyl S-(N- istration, as defined in § 180.1(n), are es- methylcarbamoylmethyl) tablished for total residues of phosphorodithioate) including its oxy- dimethoate including its oxygen analog gen analog (O,O-dimethyl S-(N- in or on the following food commod- methylcarbamoylmethyl) ities: phosphorothioate) in or on the fol- lowing food commodities: Parts per Commodity million Parts per Commodity million Asparagus ...... 0.15 Brussels sprouts ...... 5 Alfalfa ...... 2 Cherry ...... 2 Apple ...... 2 Bean, dry, seed ...... 2 (d) Indirect or inadvertent residues. Bean, lima ...... 2 Bean, snap, succulent ...... 2 [Reserved] Blueberry1 ...... 1 Broccoli ...... 2 [65 FR 33697, May 24, 2000, as amended at 69 Cabbage ...... 2 FR 6567, Feb. 11, 2004] Cattle, meat byproducts ...... 0.02 Cauliflower ...... 2 § 180.205 Paraquat; tolerances for resi- Celery ...... 2 dues. Citrus, dried pulp ...... 5 Collards ...... 2 (a) General. Tolerances are estab- Corn, forage ...... 1 lished for residues of the desiccant, de- Corn, grain ...... 0.1 foliant, and herbicide paraquat (1,1′-di- Corn, stover ...... 1 Cotton, undelinted seed ...... 0.1 methyl-4,4′-bipyridinium-ion) derived Egg ...... 0.02 from application of either the Endive ...... 2 bis(methyl sulfate) or the dichloride Goat, meat byproducts ...... 0.02 Grapefruit ...... 2 salt (both calculated as the cation) in Grape ...... 1 or on the following food commodities: Hog, meat byproducts ...... 0.02 Horse, meat byproducts ...... 0.02 Commodity Parts per Kale ...... 2 million Lemon ...... 2 Lentil, seed ...... 2.0 Acerola ...... 0.05 Lettuce ...... 2 Alfalfa ...... 5 Melon ...... 1 Almond, hulls ...... 0.5 Milk ...... 0.002 Animal feed, nongrass, group 18, forage ...... 75

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Parts per Parts per Commodity million Commodity million

Animal feed, nongrass, group 18, hay ...... 210 Lettuce ...... 0.05(N) Apple ...... 0.05(N) Milk ...... 0.01(N) Apricot ...... 0.05(N) Mint, hay ...... 0.5 Artichoke, globe ...... 0.05 Mint, hay, spent ...... 3.0 Asparagus ...... 0.5 Nectarine ...... 0.05(N) Avocado ...... 0.05(N) Nut ...... 0.05(N) Banana ...... 0.05(N) Nut, tree, group 14 ...... 0.05 Barley, hay ...... 3.5 Okra ...... 0.05 Barley, grain ...... 0.05(N) Olive ...... 0.05(N) Barley, straw ...... 1.0 Onion, bulb ...... 0.10 Bean, dry, seed ...... 0.3 Onion, green ...... 0.05 Bean, forage ...... 0.1 Papaya ...... 0.05(N) Bean, hay ...... 0.4 Passionfruit ...... 0.2 Bean, lima, succulent ...... 0.05 Pea and bean, dried shelled, except soybean, Bean, snap, succulent ...... 0.05 subgroup 6C, except guar bean ...... 0.30 Beet, sugar ...... 0.5 Pea and bean, succulent shelled, subgroup 6B 0.05 Beet, sugar, tops ...... 0.05 Pea, dry, seed ...... 0.3 Berry group 13 ...... 0.05 Pea, field, vines ...... 0.2 Birdsfoot trefoil ...... 5 Pea, field, hay ...... 0.8 Broccoli ...... 0.05 Pea, succulent ...... 0.05 Cabbage ...... 0.05 Peach ...... 0.05(N) Cabbage, chinese ...... 0.05 Peanut ...... 05 Cacao bean ...... 0.05 Peanut, hay ...... 5 Carrot, roots ...... 0.05 Pear ...... 0.05(N) Cattle, fat ...... 0.05 Persimmon ...... 0.05 Cattle, kidney ...... 0.50 Pineapple ...... 0.05(N) Cattle, meat ...... 0.05 Pistachio ...... 0.05 Cattle, meat byproducts, except kidney ...... 0.05 Plum, prune, fresh ...... 0.05(N) Cauliflower ...... 0.05 Potato ...... 0.5 Cherry ...... 0.05(N) Rhubarb ...... 0.05(N) Clover ...... 5 Rice, grain ...... 0.05 Coffee, bean, green ...... 0.05(N) Rice, straw ...... 0.06 Collards ...... 0.05 Safflower, seed ...... 0.05(N) Corn, field, forage ...... 3.0 Sheep, fat ...... 05 Corn, field, grain ...... 0.1 Sheep, kidney ...... 0.50 Corn, field, stover ...... 10.0 Sheep, meat ...... 05 Corn, fresh (inc sweet corn), kernel plus cob Sheep, meat byproducts, except kidney ...... 05 with husks removed ...... 0.05(N) Pea, succulent ...... 0.05 Corn, pop, grain ...... 0.1 Sorghum, forage, forage ...... 0.10 Corn, pop, stover ...... 10.0 Sorghum, grain ...... 0.05(N) Cotton, gin byproducts ...... 110 Sorghum, grain, forage ...... 0.10 Cotton, undelinted seed ...... 3.5 Soybean ...... 0.05(N) Cranberry ...... 0.05 Soybean, forage ...... 0.40 Cucurbits ...... 0.05 Soybean, hay ...... 10 Egg ...... 0.01(N) Soybean, hulls ...... 4.5 Endive ...... 0.05 Soybean, seed ...... 0.70 Fig ...... 0.05(N) Strawberry ...... 0.25 Fruit, citrus ...... 0.05(N) Sugarcane, cane ...... 0.5(N) Fruit, pome, group 11 ...... 0.05 Sunflower, seed ...... 2 Fruit, small ...... 0.05(N) Turnip, greens ...... 0.05 Fruit, stone, group 12 ...... 0.05 Turnip, roots ...... 0.05 Ginger ...... 0.10 Vegetable, Brassica leafy, group 5 ...... 0.05 Goat, fat ...... 05 Vegetable, cucurbit, group 9 ...... 0.05 Goat, kidney ...... 0.50 Vegetable, fruiting, group 8 ...... 0.05 Goat, meat ...... 05 Vegetable, legume, edible podded, subgroup Goat, meat byproducts, except kidney ...... 05 6A ...... 0.05 Grain, aspirated fractions ...... 65 Wheat, forage ...... 0.50 Grape ...... 0.05 Wheat, grain ...... 1.1 Grass, pasture ...... 5 Wheat, hay ...... 3.5 Grass, range ...... 5 Wheat, straw ...... 50 Guar bean ...... 0.5 Guava ...... 0.05(N) Hog, fat ...... 05 (b) Section 18 emergency exemptions. Hog, kidney ...... 0.50 [Reserved] Hog, meat ...... 05 (c) Tolerances with regional registra- Hog, meat byproducts, except kidney ...... 05 tions. Tolerances with regional reg- Hop, dried cones ...... 0.50 Horse, fat ...... 05 istration as defined in § 180.1(n), are es- Horse, kidney ...... 0.50 tablished for residues of the pesticide Horse, meat ...... 05 paraquat (1,1′-dimethyl-4,4′ Horse, meat byproducts, except kidney ...... 05 Kiwifruit ...... 0.05 bipyridinium ion) derived from applica- Lentil, seed ...... 0.3 tion of either the bis(methyl sulfate) or

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the dichloride salt (both calculated as (d) Indirect or inadvertent residues. the cation) in or on the following food [Reserved] commodities: [58 FR 62038, Nov. 24, 1993, as amended at 63 FR 2165, Jan. 14, 1998; 63 FR 57074, Oct. 26, Parts per Commodity million 1998; 66 FR 50833, Oct. 5, 2001; 67 FR 49616, July 31, 2002; 71 FR 74816, Dec. 13, 2006] Cassava ...... 0.05 Pea, pigeon, seed ...... 0 .05 § 180.207 Trifluralin; tolerances for Tanier ...... 0 .05 residues. Taro, corm ...... 0 .1 (a) General. Tolerances are estab- Tyfon ...... 0 .05 Yam, true, tuber ...... 0.05 lished for residues of the herbicide and plant growth regulator trifluralin, (d) Indirect or inadvertent residues. alpha, alpha, alpha-trifluoro-2,6- [Reserved] dinitro-N,N-dipropyl-p-toluidine, in or on the following raw agricultural com- [46 FR 51614, Oct. 21, 1981] modities: DITORIAL OTE EDERAL EGISTER E N : For F R ci- Parts per tations affecting § 180.205, see the List of CFR Commodity million Sections Affected, which appears in the Finding Aids section of the printed volume Alfalfa, forage ...... 3.0 Alfalfa, hay ...... 2.0 and on GPO Access. Almond, hulls ...... 0 .05 Asparagus ...... 0.05 § 180.206 Phorate; tolerances for resi- Barley, grain ...... 0 .05 dues. Barley, hay ...... 0 .05 Barley, straw ...... 0 .05 (a) General. Tolerances are estab- Bean, mung, sprouts ...... 2.0 lished for combined residues of the in- Carrot, roots ...... 1.0 Celery ...... 0 .05 secticide phorate (O,O-diethyl Corn, field, forage ...... 0 .05 S[(ethylthio) methyl] Corn, field, grain ...... 0 .05 Corn, field, stover ...... 0 .05 phosphorodithioate) and its cholin- Cotton, gin byproducts ...... 0 .05 esterase-inhibiting metabolites in or Cotton, undelinted seed ...... 0 .05 on raw agricultural commodities as Endive ...... 0.05 Flax, seed ...... 0 .05 follows: Fruit, citrus, group 10 ...... 0 .05 Fruit, stone, group 12 ...... 0 .05 Commodity Parts per Grape ...... 0 .05 million Hop, dried cones ...... 0 .05 Mustard, seed ...... 0 .05 Bean ...... 0 .1 Nut, tree, group 14 ...... 0 .05 Beet, sugar, roots ...... 0 .3 Okra ...... 0.05 Beet, sugar, tops ...... 3.0 Peanut ...... 0 .05 Coffee, bean, green1 ...... 0 .02 Peanut, hay ...... 0.05 Corn, forage ...... 0 .5 Peppermint oil ...... 2 .0 Corn, grain ...... 0 .1 Peppermint, tops ...... 0 .05 Rapeseed, seed ...... 0 .05 Corn, sweet, kernel plus cob with husks re- Safflower, seed ...... 0 .05 moved ...... 0 .1 Sorghum, grain, forage ...... 0.05 Cotton, undelinted seed ...... 0 .05 Sorghum, grain, grain ...... 0 .05 Hop ...... 0 .5 Sorghum, grain, stover ...... 0 .05 Peanut ...... 0 .1 Spearmint oil ...... 2 .0 Potato ...... 0 .5 Spearmint, tops ...... 0 .05 Sorghum, grain ...... 0 .1 Sugarcane, cane ...... 0.05 Sorghum, grain, stover ...... 0 .1 Sunflower, seed ...... 0.05 Soybean ...... 0.1 Vegetable, brassica, leafy group 5 ...... 0 .05 Vegetable, bulb, group 3 ...... 0 .05 Sugarcane, cane ...... 0.1 Vegetable, cucurbit, group 9 ...... 0.05 Wheat, grain ...... 0 .05 Vegetable, foliage of legume, group 7 ...... 0 .05 Wheat, hay ...... 1 .5 Vegetable, fruiting, group 8 ...... 0.05 Wheat, straw ...... 0 .05 Vegetable, leaves of root and tuber, group 2 ..... 0 .05 Vegetable, legume, group 6 ...... 0 .05 1There are no U.S. registrations as of September 1, 1993 for coffee, bean, green. Vegetable, root and tuber, group 1, except car- rot ...... 0 .05 (b) Section 18 emergency exemptions. Wheat, grain ...... 0 .05 [Reserved] Wheat, straw ...... 0 .05 (c) Tolerances with regional registra- (b) Section 18 emergency exemptions. tions. [Reserved] [Reserved]

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(c) Tolerances with regional registra- Commodity Parts per tions. [Reserved] million (d) Indirect or inadvertent residues. Canebserry ...... 0 .2 [Reserved] Peach ...... 0 .2 Peppermint, tops ...... 2 .0 [45 FR 42619, June 25, 1980, as amended at 45 Spearmint, tops ...... 2 .0 FR 56346, Aug. 25, 1980; 45 FR 86493, Dec. 31, Strawberry ...... 0 .1 1980; 46 FR 37250, July 20, 1981; 47 FR 13524, Sugarcane, cane ...... 0.4 Mar. 31, 1982; 47 FR 20309, May 12, 1982; 63 FR Watermelon ...... 1.0 57074, Oct. 26, 1998; 64 FR 39082, July 21, 1999; 70 FR 21643, Apr. 27, 2005; 71 FR 54433, Sept. (b) Section 18 emergency exemptions. 15, 2006] [Reserved] (c) Tolerances with regional registra- § 180.208 N-Butyl-N-ethyl-ù·ù·ù-tri- tions. [Reserved] fluoro-2,6-dinitro-p-toluidine; toler- (d) Indirect or inadvertent residues. ances for residues [Reserved] (a) General. Tolerances are estab- [71 FR 30818, May 31, 2006] lished for residues of the herbicide N- butyl-N-ethyl-a·a·a-trifluoro-2,6- § 180.210 Bromacil; tolerances for resi- dinitro-p-toluidine in or on the fol- dues. lowing food commodities: (a) General. Tolerances are estab- Parts per lished for residues of the herbicide Commodity million bromacil (5-bromo-3-sec-butyl-6- Alfalfa, forage ...... 0.05(N) methyluracil) in or on the following Alfalfa, hay ...... 0.05(N) food commodities: Clover, forage ...... 0.05(N) Clover, hay ...... 0.05(N) Commodity Parts per Lettuce ...... 0.05(N) million Peanut ...... 0 .05(N) Trefoil, forage ...... 0 .05(N) Fruit, citrus ...... 0 .1 Trefoil, hay ...... 0 .05(N) Pineapple ...... 0.1

(b) Section 18 emergency exemptions. (b) Section 18 emergency exemptions. [Reserved] [Reserved] (c) Tolerances with regional registra- (c) Tolerances with regional registra- tions. [Reserved] tions. [Reserved] (d) Indirect or inadvertent residues. (d) Indirect or inadvertent residues. [Reserved] [Reserved] [68 FR 39439, July 1, 2003] [68 FR 39439, July 1, 2003]

§ 180.209 Terbacil; tolerances for resi- § 180.211 2-Chloro-N-isopropylacetani- dues. lide; tolerances for residues. (a) General. Tolerances are estab- (a) General. Tolerances are estab- lished for combined residues of the her- lished for residues of the herbicide 2- bicide terbacil, (3-tert-butyl-5-chloro-6- chloro-N- isopropylacetanilide and its methyluracil) and its metabolites [3- metabolites (calculated as 2-chloro-N- tert-butyl-5-chloro-6- isopropylacetanilide) in or on the fol- hydroxymethyluracil], [6-chloro-2,3- lowing raw agricultural commodities: dihydro-7-hydroxymethyl 3,3-dimethyl- Parts per 5H-oxazolo(3,2-a) pyrimidin-5-one], and Commodity million [6-chloro-2,3-dihydro-3,3,7-trimethyl- Cattle, fat ...... 0.02(N) 5H-oxazolo(3,2-a) pyrimidin-5-one], cal- Cattle, meat byproducts ...... 0.02(N) culated as terbacil, in or on the fol- Cattle, meat ...... 0 .02(N) lowing raw agricultural commodities: Corn, forage ...... 1 .5 Corn, grain ...... 0 .1(N) Parts per Egg ...... 0 .02(N) Commodity million Goat, fat ...... 0 .02(N) Goat, meat byproducts ...... 0 .02(N) Alfalfa, forage ...... 1.0 Goat, meat ...... 0.02(N) Alfalfa, hay ...... 2.0 Hog, fat ...... 0 .02(N) Apple ...... 0.3 Hog, meat byproducts ...... 0 .02(N) Asparagus ...... 0.4 Hog, meat ...... 0 .02(N) Blueberry ...... 0 .2 Horse, fat ...... 0 .02(N)

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Parts per Expiration/ Commodity million Commodity Parts per revocation million date Horse, meat byproducts ...... 0 .02(N) Horse, meat ...... 0 .02(N) Apple ...... 0.25 None Milk ...... 0.02(N) Artichoke,globe ...... 0.5 12/31/00 Poultry, fat ...... 0.02(N) Asparagus ...... 10 12/31/00 Poultry, meat byproducts ...... 0.02(N) Avocado ...... 0.25 None Poultry, meat ...... 0 .02(N) Bermudagrass, forage ...... 15 None Sheep, fat ...... 0 .02(N) Bermudagrass, hay ...... 15 None Sheep, meat byproducts ...... 0 .02(N) Blackberry ...... 0.25 None Sheep, meat ...... 0.02(N) Blueberry ...... 0.25 None Sorghum, forage ...... 5 .0 Boysenberry ...... 0.25 None Sorghum, grain ...... 0 .25 Cattle, fat ...... 0.02(N) None Sorghum, grain, stover ...... 5 .0 Cattle, meat byproducts ...... 0.02(N) None Cattle, meat ...... 0.02(N) None Cherry ...... 0.25 None (b) Section 18 emergency exemptions. Corn, forage ...... 0.25 None [Reserved] Corn, sweet, kernel plus cob with (c) Tolerances with regional registra- husks removed ...... 0.25 None tions. [Reserved] Corn, grain ...... 0.25 None Corn, stover ...... 0.25 None (d) Indirect or inadvertent residues. Cranberry ...... 0.25 None [Reserved] Currant ...... 0.25 None Dewberry ...... 0.25 None [47 FR 25959, June 16, 1982, as amended at 47 Egg ...... 0.02(N) None FR 28381, June 30, 1982; 47 FR 28626, July 1, Filbert ...... 0.25 None 1982; 47 FR 46701, Oct. 20, 1982; 63 FR 57074, Goat, fat ...... 0.02(N) None Oct. 26, 1998] Goat, meat byproducts ...... 0.02(N) None Goat, meat ...... 0.02(N) None Grapefruit ...... 0.25 None § 180.212 S-Ethyl cyclohexylethylthio- Grape ...... 0.25 None ; tolerances for residues. Grass, forage ...... 15 None Grass, hay ...... 15 None (a) General. Tolerances are estab- Hog, fat ...... 0.02(N) None lished for residues of the herbicide S- Hog, meat byproducts ...... 0.02(N) None ethyl cyclohexylethylthiocarbamate in Hog, meat ...... 0.02(N) None Horse, fat ...... 0.02(N) None or on the following food commodities: Horse, meat byproducts ...... 0.02(N) None Horse, meat ...... 0.02(N) None Commodity Parts per Lemon ...... 0.25 None million Loganberry ...... 0.25 None Milk ...... 0.02(N) None Beet, garden, roots ...... 0 .05(N) Nut, macadamia ...... 0.25 None Beet, garden, tops ...... 0 .05(N) Olive ...... 0.25 None Beet, sugar, roots ...... 0 .05(N) Orange, sweet ...... 0.25 None Beet, sugar, tops ...... 0.05(N) Peach ...... 0.25 None Spinach ...... 0 .05(N) Pear ...... 0.25 None Pecan ...... 0.1(N) None (b) Section 18 emergency exemptions. Plum ...... 0.25 None [Reserved] Poultry, fat ...... 0.02(N) None Poultry, meat byproducts ...... 0.02(N) None (c) Tolerances with regional registra- Poultry, meat ...... 0.02(N) None tions. [Reserved] Raspberry ...... 0.25 None (d) Indirect or inadvertent residues. Sheep, fat ...... 0.02(N) None [Reserved] Sheep, meat byproducts ...... 0.02(N) None Sheep, meat ...... 0.02(N) None [68 FR 39439, July 1, 2003] Strawberry ...... 0.25 None Sugarcane, cane ...... 0.25 12/31/00 Sugarcane, molasses ...... 1 None § 180.213 Simazine; tolerances for resi- Walnut ...... 0.2 None dues. (a) General. (1) Tolerances are estab- (2) Tolerances are established for the lished for residues of the herbicide combined residues of the herbicide simazine (2-chloro- 4,6-bis(ethylamino)- simazine (2-chloro-4,6-bis(ethylamino)- s-triazine) in or on the following raw s-triazine) and its metabolites 2-amino- agricultural commodities: 4-chloro-6-ethylamino-s-triazine and 2,4-diamino-6-chloro-s-triazine in or on Parts per Expiration/ Commodity revocation raw agricultural commodities as fol- million date lows:

Alfalfa, forage ...... 15 None Parts per Alfalfa, hay ...... 15 None Commodity million Almond ...... 0.25 None Almond, hulls ...... 0.25 None Banana ...... 0.2

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Parts per Parts per Commodity million Commodity million

Fish ...... 12 Almond, hulls ...... 0 .5 Almond ...... 0.5 Bean, dry, seed ...... 0 .5 (b) Section 18 emergency exemptions. Bean, succulent ...... 0 .5 [Reserved] Beet, sugar, roots ...... 0 .5 (c) Tolerances with regional registra- Beet, sugar, tops ...... 0.5 Broccoli ...... 1 tions. [Reserved] Brussels sprouts ...... 1 (d) Indirect or inadvertent residues. Cabbage ...... 1 [Reserved] Cauliflower ...... 1 Celery ...... 3 [63 FR 2165, Jan. 14, 1998, as amended at 63 Collards ...... 3 FR 57074, Oct. 26, 1998; 72 FR 35665, June 29, Cotton, undelinted seed ...... 0 .5 Cucumber ...... 0 .5 2007] Eggplant ...... 0.5 Grapefruit ...... 3 § 180.214 Fenthion; tolerances for resi- Grape ...... 0 .5 dues. Grass, forage ...... 10 Hop ...... 0 .5 (a) General. Tolerances are estab- Kale ...... 3 lished for residues of the insecticide Legume, forage ...... 10 Lemon ...... 3 fenthion (O,O- dimethyl O-[4- Lettuce ...... 1 (methylthio)-m- tolyl] Melon ...... 0 .5 phosphorothioate) and its cholin- Orange, sweet ...... 3 Peach ...... 0 .5 esterase-inhibiting metabolites in or Pea, succulent ...... 0 .5 on the following raw agricultural com- Pepper ...... 0 .5 modities: Pumpkin ...... 0.5 Safflower, seed ...... 0 .5 Expiration/ Spinach ...... 3 Commodity Parts per Revocation Squash, summer ...... 0 .5 million Date Squash, winter ...... 0 .5 Strawberry ...... 1 Cattle, fat ...... 0.1 4/1/06 Swiss chard ...... 3 Cattle, meat ...... 0.1 4/1/06 Tangerine ...... 3 Cattle, meat byproducts ...... 0.1 4/1/06 Tomato ...... 0.5 Turnip, greens ...... 3 Hog, fat ...... 0.1 4/1/03 Walnut ...... 0 .5 Hog, meat ...... 0.1 4/1/03 Hog, meat byproducts ...... 0.1 4/1/03 Milk ...... 0.01 4/1/03 (2) A tolerance of 0.5 part per million is established for the pesticide naled in (b) Section 18 emergency exemptions. or on all raw agricultural commodities, [Reserved] except those otherwise listed in this (c) Tolerances with regional registra- section, from use of the pesticide for tions. [Reserved] area pest (mosquito and ) control. (d) Indirect or inadvertent residues. (b) Section 18 emergency exemptions. [Reserved] [Reserved] (c) Tolerances with regional registra- [45 FR 86492, Dec. 31, 1980, as amended at 63 tions. [Reserved] FR 57074, Oct. 26, 1998; 66 FR 50833, Oct. 5, (d) Indirect or inadvertent residues. 2001; 67 FR 49616, July 31, 2002] [Reserved] § 180.215 Naled; tolerances for resi- [42 FR 46304, Sept. 15, 1977, as amended at 54 dues. FR 20125, May 10, 1989; 63 FR 57074, Oct. 26, 1998; 66 FR 50833, Oct. 5, 2001] (a) General. (1) Tolerances are estab- lished for residues of the insecticide § 180.217 Ammoniates for [ethylenebis- naled (1,2-dibromo-2,2-dichloro-ethyl (dithiocarbamato)] zinc and ethyl- dimethyl phosphate) and its conversion enebis [dithiocarbamic acid] bimo- product 2,2-dichlorovinyl dimethyl lecular and trimolecular cyclic phosphate, expressed as naled, result- anhydrosulfides and disulfides; tol- ing from the application of the pes- erances for residues. ticide to growing crops or from direct (a) General. Tolerances are estab- application to livestock and poultry, in lished for residues of a fungicide that is or on the following raw agricultural a mixture of 5.2 parts by weight of am- commodities: moniates of [ethylenebis

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(dithiocarbamato)] zinc with 1 part by (2) A tolerance is established for com- weight ethylenebis [dithiocarbamic bined residues of the herbicide atrazine acid] bimolecular and trimolecular cy- (2-chloro-4-ethylamino-6- clic anhydrosulfides and disulfides, cal- isopropylamino-s-triazine) and its me- culated as zinc tabolites 2-amino-4-chloro-6- ethylenebisdithiocarbamate, in or on ethylamino-s-triazine, 2-amino-4- the following raw agricultural com- chloro-6-isopropylamino-s-triazine, and modities as follows: 2-chloro-4,6-diamino-s-triazine in or on the following raw agricultural com- Parts per Commodity million modity:

Apple ...... 2.0 Commodity Parts per Potato ...... 0 .5 million Grass, range ...... 4 (b) Section 18 emergency exemptions. [Reserved] (b) Section 18 emergency exemptions. (c) Tolerances with regional registra- [Reserved] tions. [Reserved] (c) Tolerances with regional registra- (d) Indirect or inadvertent residues. tions. [Reserved] [Reserved] (d) Indirect or inadvertent residues. [63 FR 57074, Oct. 26, 1998] [Reserved] [43 FR 29121, July 6, 1978, as amended at 44 § 180.220 Atrazine; tolerances for resi- FR 67116, Nov. 23, 1979; 47 FR 3771, Jan. 27, dues. 1982; 47 FR 8012, Feb. 24, 1982; 63 FR 57075, (a) General. (1) Tolerances are estab- Oct. 26, 1998; 67 FR 46893, July 17, 2002; 69 FR lished for residues of the herbicide 6567, Feb. 11, 2004; 72 FR 35666, June 29, 2007] atrazine (2-chloro-4-ethylamino-6- § 180.221 O-Ethyl S-phenyl ethylphos- isopropylamino-s-triazine) in or on the phonodithioate; tolerances for resi- following raw agricultural commod- dues. ities: (a) General. Time limited tolerances are established for residues of the in- Commodity Parts per million secticide O-Ethyl S- Cattle, fat ...... 0.02 phenylethylphosphonodithioate, in- Cattle, meat byproducts ...... 0.02 cluding its oxygen analog (O-ethyl S- Cattle, meat ...... 0 .02 phenyl ethylphosphonothioate, in or on Corn, field, forage ...... 15 the following food commodities: Corn, fodder, field ...... 15 Corn, grain ...... 0 .25 Expiration/ Corn, pop, forage ...... 15 Commodities Parts per Revocation Corn, pop, stover ...... 15 million date Corn, sweet, forage ...... 15 Corn, sweet, kernel plus cob with husks re- Asparagus ...... 0.5 12/31/02 moved ...... 0 .25 Banana ...... 0.1 Do. Corn, sweet, stover ...... 15 Beet, sugar, tops ...... 0.1 Do. Goat, fat ...... 0 .02 Corn, field, forage ...... 0.1 Do. Goat, meat byproducts ...... 0 .02 Corn, field, grain ...... 0.1 Do. Goat, meat ...... 0.02 Corn, field, stover ...... 0.1 Do. Guava ...... 0 .05 Corn, sweet kernel plus cob with Horse, fat ...... 0 .02 husks removed ...... 0.1 Do. Horse, meat byproducts ...... 0 .02 Corn, pop, grain ...... 0.1 Do. Horse, meat ...... 0 .02 Corn, pop, stover ...... 0.1 Do. Milk ...... 0.02 Corn, sweet, stover ...... 0.1 Do. Nut, macadamia ...... 0.25 Corn, sweet, forage ...... 0.1 Do. Rye grass, perennial ...... 15 Peanut ...... 0.1 Do. Sheep, fat ...... 0 .02 Peanut, hay ...... 0.1 Do. Sheep, meat byproducts ...... 0 .02 Pea, field, hay ...... 0.1 Do. Sheep, meat ...... 0.02 Pea, field, vines ...... 0.1 Do. Sorghum, forage ...... 15 Peppermint, tops ...... 0.1 Do. Sorghum, grain ...... 0 .25 Plantain ...... 0.1 Do. Sorghum, grain, stover ...... 15 Sorghum, grain, stover ...... 0.1 Do. Sugarcane, cane ...... 0.25 Sorghum, grain, forage ...... 0.1 Do. Sugarcane, fodder ...... 0.25 Sorghum, grain, grain ...... 0.1 Do. Sugarcane, forage ...... 0.25 Soybean, forage ...... 0.1 Do. Wheat, grain ...... 0 .25 Soybean, hay ...... 0.1 Do. Wheat, straw ...... 5 Spearmint, tops ...... 0.1 Do. Strawberry ...... 0.1 Do.

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on the following raw agricultural com- Parts per Expiration/ Commodities Revocation modities (RACs) resulting from post- million date harvest fumigation for the control of Sugarcane, cane ...... 0.1 Do. insects with phosphine gas or Vegetable, leafy ...... 0.1 Do. phosphide compounds that produce Vegetable, fruiting, group 8 ...... 0.1 Do. Vegetable, root crop ...... 0.1 Do. phosphine gas. Vegetable, seed and pod ...... 0.1 Do. Parts per Commodity million (b) Section 18 emergency exemptions. [Reserved] Almond ...... 0.1 (c) Tolerances with regional registra- Avocado ...... 0 .01 Banana (includes Plantains) ...... 0.01 tions. [Reserved] Barley, grain ...... 0 .1 (d) Indirect or inadvertent residues. Cabbage, Chinese ...... 0 .01 [Reserved] Cacao bean, dried bean ...... 0 .1 Cashew ...... 0 .1 [64 FR 39077, July 21, 1999] Citron, citrus ...... 0 .01 Coffee, bean, green ...... 0 .1 Corn, field, grain ...... 0 .1 § 180.222 Prometryn; tolerances for Corn, pop, grain ...... 0.1 residues. Cotton, undelinted seed ...... 0 .1 (a) General. Tolerances are estab- Date, dried fruit ...... 0 .1 Dill, seed ...... 0 .01 lished for residues of the herbicide Eggplant ...... 0.01 prometryn (2,4-bis(isopropylamino)-6- Endive ...... 0.01 methylthio-s-triazine) in or on the fol- Filbert ...... 0 .1 Grapefruit ...... 0 .01 lowing raw agricultural commodities: Kumquat ...... 0 .01 Lemon ...... 0.01 Commodity Parts per Lettuce ...... 0.01 million Lime ...... 0.01 Mango ...... 0.01 1 Carrot, roots ...... 0 .1 Millet, grain ...... 0 .1 Celery ...... 0 .5 Mushroom ...... 0 .01 Corn, grain ...... 0 .25 Nut, brazil ...... 0 .1 Cotton, undelinted seed ...... 0 .25 Oat, grain ...... 0 .1 Pea, pigeon, seed ...... 0 .25 Okra ...... 0.01 1There are no U.S. registrations as of April 10, 1998 for use Orange, sweet ...... 0 .01 on carrots. Papaya ...... 0 .01 Peanut ...... 0 .1 (b) Section 18 emergency exemptions. Pecan ...... 0 .1 [Reserved] Pepper ...... 0 .01 Persimmon ...... 0 .01 (c) Tolerances with regional exemptions. Pimento ...... 0 .01 Tolerances with regional registration, Pistachio ...... 0.1 as defined in § 180.1(n), are established Rice, grain ...... 0 .1 for residues of the herbicide prometryn Rye, grain ...... 0.1 Safflower, seed ...... 0 .1 (2,4-bis(isopropylamino-6-methylthio-s- Salsify, tops ...... 0 .01 triazine) in or on the following raw ag- Sesame, seed ...... 0 .1 ricultural commodity: Sorghum, grain ...... 0 .1 Soybean, seed ...... 0 .1 Sunflower, seed ...... 0.1 Parts per Commodity million Sweet potato, roots ...... 0 .01 Tangelo ...... 0 .01 Dill ...... 0 .3 Tangerine ...... 0 .01 Parsley, leaves ...... 0.1 Tomato ...... 0.01 Vegetable, legume, group 6, except soybean .... 0 .01 Walnut ...... 0 .1 (d) Indirect or inadvertent residues. Wheat, grain ...... 0 .1 [Reserved] [43 FR 29121, July 6, 1978, as amended at 45 (2) Tolerances are established for res- FR 51782, Aug. 5, 1980; 54 FR 6918, Feb. 15, idues of the fumigant in or on all RACs 1989; 60 FR 20434, Apr. 26, 1995; 63 FR 17692, resulting from preharvest treatment of Apr. 10, 1998; 63 FR 57075, Oct. 26, 1998; 64 FR pest burrows in agricultural and non- 39082, July 21, 1999] crop land areas.

§ 180.225 Phosphine; tolerances for Commodity Parts per residues. million (a) General. (1) Tolerances are estab- All RACs resulting from preharvest treatment of lished for residues of phosphine in or pest burrows ...... 0 .01

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(3) Residues resulting from fumiga- Commodity Parts per tion of processed food: million Goat, meat ...... 0.02 Parts per Commodity million Hog, fat ...... 0 .02 Hog, meat byproducts ...... 0 .02 Processed food ...... 0 .01 Hog, meat ...... 0 .02 Horse, fat ...... 0 .02 Horse, meat byproducts ...... 0 .02 (4) Residues resulting from fumigation Horse, meat ...... 0 .02 of animal feed: Milk ...... 0.02 Potato ...... 0 .1 Potato, processed potato waste ...... 1 .0 Commodity Parts per million Poultry, fat ...... 0.02 Poultry, meat byproducts ...... 0.02 Animal feed ...... 0.1 Poultry, meat ...... 0 .02 Sheep, fat ...... 0 .02 (5) To assure safe use of this pes- Sheep, meat byproducts ...... 0 .02 ticide, it must be used in compliance Sheep, meat ...... 0.02 with the labeling conforming to that (2)(i) Tolerances are established for registered by the U.S. Environmental residues of the herbicide diquat (6,7- Protection Agency (EPA) under dihydrodipyrido (1,2-a:2,1-c) FIFRA. Labeling shall bear a restric- pyrazinediium) (calculated as the tion to aerate the finished food/feed for cation) derived from the application of 48 hours before it is offered to the con- the dibromide salt to ponds, lakes, res- sumer, unless EPA specifically deter- ervoirs, marshes, drainage ditches, ca- mines that a different time period is nals, streams, and rivers which are appropriate. Where appropriate, a slow-moving or quiescent in programs warning shall state that under no con- of the Corps of Engineers or other Fed- dition should any formulation con- eral or State public agencies and to taining aluminum or magnesium ponds, lakes and drainage ditches only phosphide be used so that it will come where there is little or no outflow of in contact with any processed food, ex- water and which are totally under the cept processed brewer’s rice, malt, and control of the user, in or on the fol- corn grits stored in breweries for use in lowing food commodities: the manufacture of beer. (b) Section 18 emergency exemptions. Commodity Parts per [Reserved] million (c) Tolerances with regional registra- Avocado ...... 0 .02 tions. [Reserved] Cotton, undelinted seed ...... 0 .02 (d) Indirect or inadvertant residues. Fish ...... 0 .1 Fruit, citrus, group 10 ...... 0 .02 [Reserved] Fruit, pome, group 11 ...... 0.02 [64 FR 72950, Dec. 29, 1999, as amended at 71 Fruit, small ...... 0 .02 Fruit, stone, group 12 ...... 0 .02 FR 74816, Dec. 13, 2006] Grain, crop ...... 0 .02 Grass, forage ...... 0 .1 § 180.226 Diquat; tolerances for resi- Hop, dried cones ...... 0 .02 dues. Nut, tree, group 14 ...... 0 .02 Shellfish ...... 0 .1 (a) General. (1) Tolerances are estab- Sugarcane, cane ...... 0.02 lished for residues of the plant growth Vegetable, cucurbit, group 9 ...... 0.02 regulator diquat [6,7-dihydrodipyrido Vegetable, foliage of legume, group 7 ...... 0 .1 Vegetable, fruiting, group 8 ...... 0.02 (1,2-a:2(a) Tolerancprime;,1-c) Vegetable, leafy ...... 0 .02 pyrazinediium] derived from applica- Vegetable, root and tuber, group 1 ...... 0 .02 tion of the dibromide salt and cal- Vegetable, seed and pod ...... 0 .02 culated as the cation in or on the fol- lowing food commodities: (ii) Where tolerances are established at higher levels from other uses of Commodity Parts per diquat on the subject crops, the higher million tolerances applies also to residues of Cattle, fat ...... 0.02 the aquatic uses cited in this para- Cattle, meat byproducts ...... 0.02 graph. Cattle, meat ...... 0 .02 (3) Tolerances are established for the Egg ...... 0 .02 Goat, fat ...... 0 .02 plant growth regulator diquat [6,7- Goat, meat byproducts ...... 0 .02 dihydrodipyrido (1,2-a:21⁄4,11⁄4-c)

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pyrazinediium] derived from applica- Commodity Parts per tion of the dibromide salt and cal- million culated as the cation in or on the fol- Sugarcane, cane ...... 0.1 lowing food commodities: Sugarcane, fodder ...... 0.1 Sugarcane, forage ...... 0.1 Commodity Parts per Sugarcane, molasses ...... 2 .0 million Wheat, forage ...... 80.0 Wheat, grain ...... 2 .0 Banana ...... 0.05 Coffee ...... 0 .05 Wheat, hay ...... 20 .0 Wheat, straw ...... 30 .0 (4) There are no U.S. registrations as of December 6, 1995. (2) Tolerances are established for the (5) A tolerance of 0.5 part per million combined residues of the herbicide is established for residues of diquat in dicamba (3,6-dichloro-o-anisic acid) and potato, granules/flakes and potato, its metabolite 3,6-dichloro-2- chips. hydroxybenzoic acid in or on the food (6) A tolerance regulation of 1.0 part commodities as follows: per million (ppm) is established for res- Parts per idues of the desiccant diquat [6,7- Commodity million dihydrodipyrido (1,2-a:21⁄4,11⁄4-c) Asparagus ...... 4.0 pyrazinediium] derived from applica- Cattle, fat ...... 0.2 tion of the dibromide salt and cal- Cattle, kidney ...... 1 .5 culated as the cation, in processed, Cattle, liver ...... 1 .5 dried potato waste. Cattle, meat byproducts ...... 0.2 (b) Section 18 emergency exemptions. Cattle, meat ...... 0 .2 Goat, fat ...... 0 .2 [Reserved] Goat, kidney ...... 1 .5 (c) Tolerances with regional registra- Goat, liver ...... 1.5 tions. [Reserved] Goat, meat byproducts ...... 0 .2 (d) Indirect or inadvertent residues. Goat, meat ...... 0.2 [Reserved] Hog, fat ...... 0 .2 Hog, kidney ...... 1.5 [65 FR 33709, May 24, 2000] Hog, liver ...... 1 .5 Hog, meat byproducts ...... 0 .2 § 180.227 Dicamba; tolerances for resi- Hog, meat ...... 0 .2 dues. Horse, fat ...... 0 .2 Horse, kidney ...... 1 .5 (a) General. (1) Tolerances are estab- Horse, liver ...... 1 .5 lished for the combined residues of the Horse, meat byproducts ...... 0 .2 herbicide dicamba (3,6-dichloro-o-anisic Horse, meat ...... 0 .2 acid) and its metabolite 3,6-dichloro-5- Milk ...... 0.3 Sheep, fat ...... 0 .2 hydroxy-o- anisic acid in or on the food Sheep, kidney ...... 1.5 commodities as follows: Sheep, liver ...... 1.5 Sheep, meat byproducts ...... 0 .2 Parts per Sheep, meat ...... 0.2 Commodity million

Barley, grain ...... 6 .0 (3) Tolerances are established for the Barley, hay ...... 2 .0 combined residues of dicamba (3,6- Barley, straw ...... 15 .0 Corn, field, forage ...... 3 .0 dichloro-o-anisic and its metablites 3,6- Corn, field, stover ...... 3 .0 dichloro-5-hydroxy-o-anisic acid and Corn, grain ...... 0 .5 3,6-dichloro-2-hydroxybenzoic acid in Corn, pop, stover ...... 3.0 or on the food commodities as follows: Cotton, undelinted seed ...... 5 .0 Cotton, meal ...... 5 .0 Crop Group 17 (grass, forage, fodder and hay). Parts per Commodity million Grass, forage ...... 125.0 Grass, hay ...... 200.0 Grain, aspirated fractions ...... 5100 .0 Millet, proso, grain ...... 0 .5 Soybean, hulls ...... 13 .0 Millet, proso, straw ...... 0 .5 Soybean, seed ...... 10.0 Oat, forage ...... 80 .0 Oat, grain ...... 0 .5 Oat, hay ...... 20.0 (b) Section 18 emergency exemptions. Oat, straw ...... 0.5 [Reserved] Sorghum, forage ...... 3 .0 Sorghum, grain ...... 3 .0 (c) Tolerances with regional registra- Sorghum, grain, stover ...... 3 .0 tions. [Reserved]

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(d) Indirect or inadvertent residues. Commodity Parts per [Reserved] million [65 FR 33709, May 24, 2000, as amended at 72 Apple ...... 0.5 Blackberry ...... 0 .1 FR 35665, June 29, 2007] Blueberry ...... 0 .15 Cranberry ...... 0 .1 § 180.228 S-Ethyl hexahydro-1H-aze- Filbert ...... 0 .1 pine-1-carbothioate; tolerances for Fruit, stone, group 12 ...... 0 .15 residues. Grape ...... 0 .15 Pear ...... 0 .5 (a) General. Tolerances are estab- Raspberry ...... 0 .1 lished for the herbicide S-ethyl hexahydro-11H-azepine-1-carbothioate (b) Section 18 emergency exemptions. in or on the following food commod- [Reserved] ities: (c) Tolerances with regional registra- tion. [Reserved] Expiration/ (d) Indirect or inadvertent residues. Commodity Parts per Revocation million Date [Reserved] [36 FR 22540, Nov. 25, 1971, as amended at 63 Rice, grain ...... 0.1 9/1/09 Rice, straw ...... 0.1 9/1/09 FR 57075, Oct. 26, 1998; 66 FR 63198, Dec. 5, 2001]

(b) Section 18 emergency exemptions. § 180.232 Butylate; tolerances for resi- [Reserved] dues. (c) Tolerances with regional registra- (a) General. Tolerances are estab- tions. [Reserved] lished for the herbicide butylate in or (d) Indirect or inadvertent residues. on the following food commodities: [Reserved] Parts per [68 FR 39439, July 1, 2003, as amended at 69 Commodity million FR 58083, Sept. 29, 2004] Corn, field, forage ...... 0 .1 § 180.229 Fluometuron; tolerances for Corn, field, grain ...... 0 .1 Corn, field, stover ...... 0 .1 residues. Corn, pop, forage ...... 0 .1 (a) General. A tolerance is established Corn, pop, grain ...... 0.1 Corn, sweet, forage ...... 0 .1 for negligible residues of the herbicide Corn, sweet, kernel plus cob with husks re- fluometuron (1,1-dimethyl-3-(a,a,a- moved ...... 0 .1 trifluoro-m-tolyl)) in or on the fol- lowing raw agricultural commodity: (b) Section 18 emergency exemptions. [Reserved] Parts per (c) Tolerances with regional registra- Commodity million tions. [Reserved] Cotton, undelinted seed ...... 0 .1 (d) Indirect or inadvertent residues. [Reserved] (b) Section 18 emergency exemptions. [Reserved] [68 FR 39439, July 1, 2003] (c) Tolerances with regional registra- § 180.235 Dichlorvos; tolerances for tion. [Reserved] residues. (d) Indirect or inadvertent residues. (a) General. (1) Tolerances for resi- [Reserved] dues of the insecticide 2,2-dichlorovinyl [63 FR 57075, Oct. 26, 1998] dimethyl phosphate are established as follows: § 180.231 Dichlobenil; tolerances for residues. Parts per Commodity million (a) General. Tolerances are estab- Cattle, fat ...... 0.02(N) lished for the combined residues of the Cattle, meat ...... 0 .02(N) herbicide dichlobenil (2,6- Cattle, meat byproducts ...... 0.02(N) dichlorobenzonitrile) and its metabo- Egg ...... 0 .05(N) lite 2,6-dichlorobenzamide in or on the Goat, fat ...... 0 .02(N) Goat, meat ...... 0.02(N) following raw agricultural commod- Goat, meat byproducts ...... 0 .02(N) ities: Horse, fat ...... 0 .02(N)

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Parts per Parts per Commodity million Commodity million

Horse, meat ...... 0 .02(N) Cattle, kidney ...... 0 .05 Horse, meat byproducts ...... 0 .02(N) Cattle, liver ...... 0 .05 Milk ...... 0.02(N) Goat, kidney ...... 0 .05 Mushroom (residues expressed as naled) ...... 0 .5 Goat, liver ...... 0.05 Poultry, fat ...... 0.05(N) Poultry, meat ...... 0 .05(N) Hog, kidney ...... 0.05 Poultry, meat byproducts ...... 0.05(N) Hog, liver ...... 0 .05 Raw agricultural commodities, nonperishable, Horse, kidney ...... 0 .05 bulk stored regardless of fat content, Horse, liver ...... 0 .05 postharvest ...... 0.5 Pecan ...... 0 .05 Raw agricultural commodities nonperishable, Potato ...... 0 .05 packaged or bagged, containing 6 percent fat Sheep, kidney ...... 0.05 or less, postharvest ...... 0.5 Sheep, liver ...... 0.05 Raw agricultural commodities, nonperishable, packaged or bagged, containing more than 6 percent fat, postharvest ...... 2 [61 FR 36299, July 10, 1996, as amended at 67 Sheep, fat ...... 0 .02(N) Sheep, meat ...... 0.02(N) FR 41806, June 19, 2002] Sheep, meat byproducts ...... 0 .02(N) Tomato, postharvest (residues expressed as § 180.238 S-Propyl butylethylthiocarba- naled) ...... 0 .05 mate; tolerances for residues. (2) The tolerance of 0.1 part per mil- (a) General. Tolerances are estab- lion prescribed by 21 CFR 556.180 for lished for residues of the herbicide S- negligible residues of 2,2-dichlorovinyl propyl butylethylthiocarbamate in or dimethyl phosphate in the edible tissue on the following food commodities: of swine covers both its use as an ant- Parts per helmintic in swine feed and as an insec- Commodity million ticide applied directly to swine. (3) Dichlorvos may be present as a Beet, sugar, roots ...... 0 .1(N) residue from application as an insecti- Beet, sugar, tops ...... 0.1(N) Tomato ...... 0.1(N) cide on packaged or bagged nonperish- able processed food (see: 21 CFR (b) Section 18 emergency exemptions. 170.3(j)) in an amount in such food not [Reserved] in excess of 0.5 part per million (ppm). (c) Tolerances with regional registra- To assure safe use of the insecticide, tions. [Reserved] its label and labeling shall conform to the label and labeling registered by the (d) Indirect or inadvertent residues. U.S. Environmental Protection Agen- [Reserved] cy, and the usage employed shall con- [68 FR 39439, July 1, 2003] form with such label or labeling. (b) Section 18 emergency exemptions. § 180.239 Phosphamidon; tolerances for [Reserved] residues. (c) Tolerances with regional registra- (a) General. Tolerances (expressed as tions. [Reserved] phosphamidon) for residues of the in- (d) Indirect or inadvertent residues. secticide phosphamidon (2-chloro-2- [Reserved] diethylcarbamoyl-1-methylvinyl di- [47 FR 55223, Dec. 8, 1982, as amended at 55 methyl phosphate) including all of its FR 26440, June 28, 1990; 56 FR 29183, June 26, related cholinesterase-inhibiting com- 1991; 63 FR 57075, Oct. 26, 1998; 65 FR 33697, pounds in or on raw agricultural com- May 24, 2000] modities are established as follows:

§ 180.236 Triphenyltin hydroxide; tol- Expira- erances for residues. Parts tion/Rev- Commodity per mil- ocation Tolerances are established for resi- lion Date dues of the fungicide triphenyltin hy- droxide in or on raw agricultural com- Apple ...... 1.0 12/31/02 modities as follows: (b) Section 18 emergency exemptions. Commodity Parts per [Reserved] million (c) Tolerances with regional registra- Beet, sugar, roots ...... 0 .05 tions. [Reserved]

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(d) Indirect or inadvertent residues. Commodity Parts per [Reserved] million [67 FR 46893, July 17, 2002] Rice, rough ...... 3 Rice, straw ...... 10 Soybean ...... 0.1 § 180.241 S-(O,O-Diisopropyl phosphor- Strawberry ...... 5 .0 odithioate) of N-(2-mercaptoethyl) Sweet potato (POST-H to sweet potato intended benzenesulfonamide; tolerances for only for use as seed) ...... 0 .02 residues. Squash, hubbard ...... 1 Wheat, grain ...... 1 .0 (a) General. Tolerances are estab- Wheat, milled fractions (except flour) ...... 3.0 lished for residues of S-(O,O- Wheat, straw ...... 1 diisopropyl phosphorodithioate) of N- (2-mercaptoethyl benzenesulfonamide (2) Tolerances are established for including its oxygen analog S-(O,O- combined residues of thiabendazole and diisopropyl phosphorodithioate) of N- its metabolite 5-hydroxythiabendazole (2-mercaptoethyl) benzenesulfonamide in the following raw agricultural com- in or on the following food commod- modities: ities: Parts per Commodity million Commodity Parts per million Cattle, fat ...... 0.1 Cattle, meat byproducts ...... 0.1 Carrot, roots ...... 0.1(N) Cattle, meat ...... 0 .1 Cucurbits ...... 0 .1(N) Egg ...... 0 .1 Onion, dry bulb ...... 0 .1(N) Poultry ...... 0 .1 Vegetable, fruiting ...... 0.1(N) Poultry, meat byproducts ...... 0.1 Vegetable, leafy ...... 0 .1(N) Poultry, meat ...... 0 .1 Goat, fat ...... 0 .1 (b) Section 18 emergency exemptions. Goat, meat byproducts ...... 0 .1 Goat, meat ...... 0.1 [Reserved] Hog, fat ...... 0 .1 (c) Tolerances with regional registra- Hog, meat byproducts ...... 0 .1 tions. [Reserved] Hog, meat ...... 0 .1 Horse, fat ...... 0 .1 (d) Indirect or inadvertent residues. Horse, meat byproducts ...... 0 .1 [Reserved] Horse, meat ...... 0 .1 Milk ...... 0.4 [68 FR 39440, July 1, 2003] Sheep, fat ...... 0 .1 Sheep, meat byproducts ...... 0 .1 § 180.242 Thiabendazole; tolerances for Sheep, meat ...... 0.1 residues. (b) Section 18 emergency exemptions. (a) General. (1) Tolerances are estab- Time-limited tolerances are estab- lished for residues of the fungicide lished for the residues of thiabendazole, thiabendazole (2-(4- in connection with use of the pesticide thiazolyl)benzimidazole) in or on the under section 18 emergency exemptions following raw agricultural commod- granted by EPA. The tolerances are ities: specified in the following table. The tolerances will expire on the dates Commodity Parts per million specified in the table. Apple, postharvest ...... 10 Expiration/ Avocado ...... 10 Commodity Parts per Revocation Banana, postharvest ...... 3 million Date Banana, pulp, postharvest ...... 0 .4 Bean, dry, seed ...... 0 .1 Brussels sprout ...... 0.05 12/31/09 Beet, sugar, dried pulp ...... 3 .5 Cabbage ...... 0.05 12/31/09 Beet, sugar, roots ...... 0 .25 Cauliflower ...... 0.05 12/31/09 Beet, sugar, tops ...... 10 Lentil, seed ...... 0.1 12/31/07 Cantaloupe ...... 15.0 Carrot, roots, postharvest ...... 10 (c) Tolerances with regional exemptions. Citrus, dried pulp, postharvest ...... 35 Fruit, citrus, postharvest ...... 10 [Reserved] Mango ...... 10 (d) Indirect or inadvertent residues. Mushroom ...... 40 .0 [Reserved] Papaya, postharvest ...... 5 Pear, postharvest ...... 10 [42 FR 32783, June 28, 1977] Potato processing waste (PRE- & POST-H) ...... 30 Potato, postharvest ...... 10 .0 EDITORIAL NOTE: For FEDERAL REGISTER ci- Rice, hulls ...... 8 tations affecting § 180.242, see the List of CFR

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Sections Affected, which appears in the § 180.249 Alachlor; tolerances for resi- Finding Aids section of the printed volume dues. and on GPO Access. Tolerances are established for the § 180.243 Propazine; tolerances for res- combined residues of the herbicide idues. alachlor (2-chloro-2′,6′-diethyl-N- Tolerances are established for neg- (methoxymethyl) acetanilide) and its ligible residues (N) of the herbicide metabolites (calculated as alachlor) in propazine (2-chloro-4,6- or on the following raw agricultural bis(isopropylamino)-s-triazine in or on commodities: the following raw agricultural com- Parts per modities: Commodity million

Parts per Bean, dry, seed ...... 0 .1 Commodity million Bean, forage ...... 0 .2 Bean, hay ...... 0 .2 Sorghum, forage ...... 0 .25(N) Bean, lima, succulent ...... 0 .1 Sorghum, grain ...... 0 .25(N) Cattle, fat ...... 0.02 Sorghum, grain, stover ...... 0 .25(N) Cattle, meat byproducts ...... 0.02 Sorghum, sweet ...... 0 .25(N) Cattle, meat ...... 0 .02 Corn, forage ...... 0 .2 Corn, grain ...... 0 .2 [43 FR 29121, July 6, 1978] Corn, stover ...... 0 .2 Corn, sweet, kernel plus cob with husks re- § 180.245 Streptomycin; tolerances for moved ...... 0 .05 Egg ...... 0 .02 residues. Goat, fat ...... 0 .02 (a) General. (1) Tolerances are estab- Goat, meat byproducts ...... 0 .02 Goat, meat ...... 0.02 lished for residues of the fungicide Hog, fat ...... 0 .02 streptomycin in or on the following Hog, meat byproducts ...... 0 .02 food commodity: Hog, meat ...... 0 .02 Horse, fat ...... 0 .02 Parts per Horse, meat byproducts ...... 0 .02 Commodity million Horse, meat ...... 0 .02 Milk ...... 0.02 Pome, fruit ...... 0 .25 Peanut ...... 0 .05 Poultry, fat ...... 0.02 Poultry, meat byproducts ...... 0.02 (2) Tolerances are established for res- Poultry, meat ...... 0 .02 idues of the fungicide streptomycin Sheep, fat ...... 0 .02 from treatment of seedling plants be- Sheep, meat byproducts ...... 0 .02 fore transplanting in or on the fol- Sheep, meat ...... 0.02 Sorghum, forage ...... 2 .0 lowing food commodities: Sorghum, grain (milo) ...... 0 .1 Sorghum, grain, stover ...... 1 .0 Parts per Soybean ...... 0.2 Commodity million

Celery ...... 0 .25 [48 FR 5921, Feb. 9, 1983, as amended at 54 FR Pepper ...... 0 .25 20125, May 10, 1989; 59 FR 39466, Aug. 3, 1994; Tomato ...... 0.25 60 FR 28345, May 31, 1995; 70 FR 44492, Aug. 3, 2005] (3) Tolerances are established for res- idues of the fungicide streptomycin § 180.252 Tetrachlorvinphos; toler- from treatment of seed pieces in or on ances for residues. the following food commodity: (a) General. (1) Tolerances are estab- Parts per lished for residues of the insecticide Commodity million tetrachlorvinphos (2-chloro-1-(2,4,5- Potato ...... 0 .25 trichlorophenyl) vinyl dimethyl phos- phate) in or on the following food com- (b) Section 18 emergency exemptions. modities: [Reserved] Commodity Parts per (c) Tolerances with regional registra- million tions. [Reserved] Cattle, fat ...... 1.5 (d) Indirect or inadvertent residues. Egg ...... 0 .1 [Reserved] Goat, fat ...... 0 .5 Hog, fat ...... 1 .5 [68 FR 39440, July 1, 2003] Horse, fat ...... 0 .5

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Parts per Parts per Commodity million Commodity million

Milk, fat (reflecting negligible residues in whole Corn, fresh (inc sweet, kernel plus cob with milk) ...... 0 .5 husks removed) ...... 0 .1(N) Poultry, fat ...... 0.75 Corn, grain (inc pop) ...... 0 .1(N) Corn, stover ...... 10 (2) Tetrachlorvinphos may be safely Cotton, undelinted seed ...... 0 .1(N) Cucurbits ...... 0 .2(N) used in accordance with the following Dandelion, leaves ...... 6 prescribed conditions: Endive ...... 5 (i) It is used in the feed of beef, dairy Grapefruit ...... 2 Grape ...... 5 cattle, and horse at a rate of 0.00015 Grass, Bermuda ...... 10 pound (0.07 gram) and swine at the rate Grass, Bermuda, hay (dried and dehydrated) .... 40 of 0.00011 pound (0.05 gram) per 100 Hop, dried cones1 ...... 12 Kale ...... 6 pounds of body weight per day. Leek ...... 3 .0 (ii) It is used for control of fecal Lemon ...... 2 in manure of treated cattle, horse, and Lentil, seed ...... 0 .1 Lettuce ...... 5 swine. Mint, hay ...... 2 (iii) To assure safe use of the pes- Mustard greens ...... 6 ticide, the label and labeling of the pes- Nectarine ...... 5 Oat, forage ...... 10 ticide formulation shall conform to the Oat, grain ...... 1 label and labeling registered by the Oat, hay ...... 10 United States Environmental Protec- Oat, straw ...... 10 Onion, green ...... 3 tion Agency. Orange, sweet ...... 2 (b) Section 18 emergency exemptions. Parsley, leaves ...... 6 [Reserved] Peach ...... 5 (c) Tolerances with regional registra- Peanut ...... 0 .1(N) Pea ...... 5 tions. [Reserved] Pea, vines ...... 10 (d) Indirect or inadvertent residues. Pecan ...... 0 .1 [Reserved] Pepper ...... 2 Pomegranate ...... 0 .2(N) [64 FR 39053, July 21, 1999, as amended at 65 Rye, forage ...... 10 FR 33697, May 24, 2000; 67 FR 49616, July 31, Rye, grain ...... 1 Rye, straw ...... 10 2002] Sorghum, forage ...... 1 Sorghum, grain ...... 0 .2(N) § 180.253 Methomyl; tolerances for res- Soybean ...... 0.2(N) idues. Soybean, forage ...... 10 Spinach ...... 6 (a) General. Tolerances are estab- Strawberry ...... 2 lished for residues of the insecticide Swiss chard ...... 6 methomyl (S-methyl N- Tangerine ...... 2 Tomato ...... 1 [(methylcarbamoyl)oxy] Turnip, greens ...... 6 thioacetimidate) in or on the food com- Vegetable, brassica, leafy, group 5 ...... 6.0 modities as follows: Vegetable, fruiting ...... 0.2(N) Vegetables, leafy [exc. beet (tops), broccoli, Parts per Brussels sprouts, cabbage, cabbage, Chi- Commodity million nese, cauliflower, celery, collards, dandelions, endive (escarole), kale, lettuce, mustard Alfalfa ...... 10 greens, parsley, spinach, Swiss chard, turnip, Apple ...... 1 greens (tops), and watercress] ...... 0.2(N) Asparagus ...... 2 Vegetable, root ...... 0 .2(N) Avocado ...... 2 Watercress ...... 6 Barley, grain ...... 1 Wheat, forage ...... 10 Barley, hay ...... 10 Wheat, grain ...... 1 Barley, straw ...... 10 Wheat, hay ...... 10 Bean, dry, seed ...... 0 .1(N) Wheat, straw ...... 10 Bean, forage ...... 10 1There are no U.S. registrations for use of methomyl on Bean, succulent ...... 2 hop, dried cone, as of February 14, 1990. Beet, garden, tops ...... 6 Blueberry ...... 6 (b) Section 18 emergency exemptions. Broccoli ...... 3 [Reserved] Brussels sprouts ...... 2 Cabbage ...... 5 (c) Tolerances with regional registra- Cabbage, chinese ...... 5 tions. Tolerances with regional reg- Cauliflower ...... 2 istration, as defined in § 180.1(n), are es- Celery ...... 3 Collards ...... 6 tablished for residues of methomyl in Corn, forage ...... 10 or on the following food commodities:

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Parts per Parts per Commodity million Commodity million (ppm) Pear ...... 4 Oat, straw (of which not more than 1.0 ppm is (d) Indirect or inadvertent residues. carbamates) ...... 5 .0 Pepper (of which no more than 0.2 ppm is [Reserved] carbamates) ...... 1 Potato (of which no more than 1 ppm is [65 FR 33697, May 24, 2000, as amended at 72 carbamates) ...... 2 FR 35666, June 29, 2007] Pumpkin (of which not more than 0.6 ppm is carbamates) ...... 0 .8 § 180.254 Carbofuran; tolerances for Raisins, waste (of which no more than 3.0 ppm residues. is carbamate ...... 6.0 (a) General. Tolerances are estab- Rice, grain ...... 0 .2 Rice, straw (of which no more than 0.2 ppm is lished for the combined residues of the carbamates) ...... 1 insecticide carbofuran (2,3-dihydro-2,2- Sorghum, fodder (of which no more than 0.5 dimethyl-7-benzofuranyl-N- ppm is carbamates) ...... 3 methylcarbamate), its carbamate me- Sorghum, forage (of which no more than 0.5 ppm is carbamates) ...... 3 tabolite-2,3-dihydro-2,2-dimethyl-3-hy- Sorghum, grain ...... 0 .1 droxy-7-benzofuranyl-N- Strawberry (of which no more than 0.2 ppm is methylcarbamate, and its phenolic me- carbamates) ...... 0 .5 tabolites 2,3-dihydro-2,2-dimethyl-7- Soybean (of which not more than 0.2 ppm is benzofuranol, 2,3-dihydro-2,2-dimethyl- carbamates) ...... 1 .0 Soybean, forage (of which not more than 20.0 3,-oxo-7-benzofuranol and 2,3-dihydro- ppm are carbamates) ...... 35 .0 2,2-dimethyl-3,7-benzofurandiol in or on Soybean, hay (of which not more than 20.0 ppm the following raw agricultural com- are carbamates) ...... 35 .0 modities: Squash (of which not more than 0.6 ppm is carbamates) ...... 0 .8 Parts per Sugarcane, cane ...... 0.1 Commodity million Sunflower, seed (of which not more than 0.5 (ppm) ppm is carbamates) ...... 1 .0 Wheat, grain (of which not more than 0.1 ppm is Alfalfa, forage (of which no more than 5 ppm carbamates) ...... 0 .2 are carbamates) ...... 10 Wheat, straw (of which not more than 1.0 ppm Alfalfa, hay (of which no more than 20 ppm are is carbamates) ...... 5.0 carbamates) ...... 40 Banana ...... 0.1 Barley, grain (of which not more than 0.1 ppm is (b) Section 18 emergency exemptions. carbamates) ...... 0 .2 [Reserved] Barley, straw (of which not more than 1.0 ppm is carbamates) ...... 5 .0 (c) Tolerances with regional registra- Beet, sugar ...... 0 .1 tion. Tolerances with regional registra- Beet, sugar, tops (of which no more than 1 ppm tion, as defined in § 180.1(n), are estab- is carbamates) ...... 2 Coffee, bean, green ...... 0 .1 lished for the combined residues of the Corn, forage (of which no more than 5 ppm are insecticide carbofuran (2,3-dihydro-2,2- carbamates) ...... 25 dimethyl-7-benzofuranyl-N- Corn, fresh (including sweet corn), kernel plus cob with husks removed (of which not more methylcarbamate), its carbamate me- than 0.2 ppm is carbamates) ...... 1 .0 tabolite 2,3-dihydro-2,2-dimethyl-3-hy- Corn, grain (including popcorn) (of which no droxy-7-benzofuranyl-N- more than 0.1 ppm is carbamates) ...... 0 .2 Corn, stover (of which no more than 5 ppm are methylcarbamate, and its phenolic me- carbamates) ...... 25 tabolites 2,3-dihydro-2,2-dimethyl-7- Cotton, undelinted seed (of which no more than benzofuranol, 2,3-dihydro-2,2-dimethyl- 0.2 ppm is carbamates) ...... 1 .0 3-oxo-7-benzofuranol, and 2,3-dihydro- Cranberry (of which no more than 0.3 ppm is carbamates) ...... 0 .5 2,2-dimethyl-3,7-benzofurandiol in or on Cucumber (of which not more than 0.2 ppm is the following raw agricultural com- carbamates) ...... 0.4 modity: Grape (of which no more than 0.2 ppm is carbamates) ...... 0 .4 Grape, raisin (of which no more than 1.0 ppm is Parts per Expiration/ Commodity million Revocation carbamate ...... 2 .0 date Melon (of which not more than 0.2 ppm is carbamates) ...... 0 .4 Artichoke, globe (of which not more Milk (of which no more than 0.02 ppm is than 0.2 ppm is carbamates) ...... 0.4 None carbamates) ...... 0.1 Canola, seed (of which no more Oat, grain (of which not more than 0.1 ppm is than 0.2 ppm is carbamate) ...... 1.0 2/22/98 carbamates) ...... 0 .2

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(d) Indirect or inadvertent residues. Commodity Parts per [Reserved] million [39 FR 20597, June 12, 1974] Banana ...... 0.25 Corn, forage ...... 0 .5 EDITORIAL NOTE: For FEDERAL REGISTER ci- Corn, grain ...... 0 .25 tations affecting § 180.254, see the List of CFR Corn, stover ...... 0 .5 Corn, sweet, kernel plus cob with husks re- Sections Affected, which appears in the moved ...... 0 .25 Finding Aids section of the printed volume Pineapple ...... 0.25 and on GPO Access. Pineapple, fodder ...... 0 .25 Pineapple, forage ...... 0 .25 § 180.257 Chloroneb; tolerances for res- Sugarcane, cane ...... 0.25 Sugarcane, fodder ...... 0.25 idues. Sugarcane, forage ...... 0.25 (a) General. Tolerances are estab- Tanier ...... 0 .25 lished for residues of the fungicide Yam, true, tuber ...... 0.25 chloroneb (1,4-dichloro-2,5- (b) Section 18 emergency exemptions. dimethoxybenzene) and its metabolite [Reserved] 2,5-dichloro-4-methoxyphenol (cal- (c) Tolerances with regional registra- culated as chloroneb) in or on the fol- tions. Tolerances with regional reg- lowing food commodities: istration, as defined in § l80.1(n), are es- Parts per tablished for the residues of ametryn in Commodity million or on the following raw agricultural commodities: Bean ...... 0 .1(N) Bean, forage ...... 2 Parts per Beet, sugar, roots ...... 0 .1(N) Commodity million Beet, sugar, tops ...... 0.1(N) Cattle, fat ...... 0.2 Cassava, root ...... 0 .1 Cattle, meat ...... 0 .2 Cattle, meat byproducts ...... 0.2 (d) Indirect or inadvertent residues. Cotton, forage ...... 2 [Reserved] Cotton, undelinted seed ...... 0 .1(N) Goat, fat ...... 0 .2 [43 FR 29121, July 6, 1978, as amended at 48 Goat, meat ...... 0.2 FR 13175, Mar. 30, 1983; 48 FR 21132, May 11, Goat, meat byproducts ...... 0 .2 1983; 52 FR 33237, Sept. 2, 1987; 63 FR 57075, Hog, fat ...... 0 .2 Oct. 26, 1998] Hog, meat ...... 0 .2 Hog, meat byproducts ...... 0 .2 Horse, fat ...... 0 .2 § 180.259 Propargite; tolerances for Horse, meat ...... 0 .2 residues. Horse, meat byproducts ...... 0 .2 (a) General. Tolerances are estab- Milk ...... 0.05(N) lished for residues of the pesticide Sheep, fat ...... 0 .2 Sheep, meat ...... 0.2 propargite (2-(p-tert-butylphenoxy) Sheep, meat byproducts ...... 0 .2 cyclohexyl 2-propynyl sulfite) in or on Soybean ...... 0.1(N) the following food commodities. Soybean, forage ...... 2 Commodity Parts per (b) Section 18 emergency exemptions. million [Reserved] Almond ...... 0.1 (c) Tolerances with regional registra- Almond, hulls ...... 55 Bean, dry, seed ...... 0 .2 tions. [Reserved] Cattle, fat ...... 0.1 (d) Indirect or inadvertent residues. Cattle, meat byproducts ...... 0.1 [Reserved] Cattle, meat ...... 0 .1 Citrus, dried pulp ...... 40 [68 FR 39440, July 1, 2003] Corn, forage ...... 10 Corn, grain ...... 0 .1 Corn, stover ...... 10 § 180.258 Ametryn; tolerances for resi- Cotton, undelinted seed ...... 0 .1 dues. Egg ...... 0 .1 (a) General. Tolerances are estab- Goat, fat ...... 0 .1 Goat, meat byproducts ...... 0 .1 lished for residues of the desiccant and Goat, meat ...... 0.1 herbicide (2-ethylamino)-4- Grapefruit ...... 5 (isopropylamino)-6-(methylthio)-s-tri- Grape ...... 10 Hog, fat ...... 0 .1 azine in or on the following raw agri- Hog, meat byproducts ...... 0 .1 cultural commodities: Hog, meat ...... 0 .1

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Parts per Parts per Commodity million Commodity million

Hop ...... 15 Blueberry ...... 10 Hop, dried cones ...... 30 Cattle, fat ...... 0.2 Horse, fat ...... 0 .1 Cattle, meat ...... 0.2 Horse, meat byproducts ...... 0 .1 Cattle, mby ...... 0.2 Horse, meat ...... 0 .1 Cherry ...... 10 Lemon ...... 5 Cotton, undelinted seed ...... 0.1 Milk, fat (0.08 ppm in milk) ...... 2 Cranberry ...... 10 Mint ...... 50 Fruit, citrus ...... 5 Nectarine ...... 4 Goat, fat ...... 0.2 Orange, sweet ...... 5 Goat, meat byproducts ...... 0.2 Peanut ...... 0 .1 Goat, meat ...... 0.2 Peanut, hay ...... 10 Grape ...... 10 Peanut, hulls ...... 10 Hog, fat ...... 0.2 Poultry, fat ...... 0.1 Hog, meat byproducts ...... 0.2 Poultry, meat byproducts ...... 0.1 Hog, meat ...... 0.2 Poultry, meat ...... 0 .1 Horse, fat ...... 0.2 Potato ...... 0 .1 Horse, meat byproducts ...... 0.2 Sheep, fat ...... 0 .1 Horse, meat ...... 0.2 Sheep, meat byproducts ...... 0 .1 Kiwifruit ...... 25 Sheep, meat ...... 0.1 Nectarine ...... 5 Sorghum, forage ...... 10 Nut ...... 0.1(N) Sorghum, grain ...... 10 Peach ...... 10 Sorghum, grain, stover ...... 10 Pear ...... 10 Tea, dried ...... 10 Pea ...... 0.5 Walnut ...... 0 .1 Pea, field, vines ...... 10 Pea, field, hay ...... 10 Plum, prune, fresh ...... 5 (b) Section 18 emergency exemptions. Potato ...... 0.1 [Reserved] Sheep, fat ...... 0.2 (c) Tolerances with regional registra- Sheep, meat byproducts ...... 0.2 tions. Tolerances with regional reg- Sheep, meat ...... 0.2 Sweet potato, roots ...... 10 istration, as defined in § 180.1(n), are es- tablished for residues of propargite in (b) Section 18 emergency exemptions. or on the following raw agricultural [Reserved] commodities: (c) Tolerances with regional registra- Parts per tions. Tolerances with regional reg- Commodity million istration, as defined in § 180.1(n), are es- tablished for the sum of the residue for Corn, sweet, kernel plus cob with husks re- moved ...... 0 .1 the insecticide N-(mercaptomethyl) phthalimide S-(O,O-dimethyl (d) Indirect or inadvertent residues. phosphorodithioate) and its oxygen [Reserved] analog N-(mercaptomethyl) phthal- imide S-(O,O-dimethyl [65 FR 33710, May 24, 2000] phosphorothioate) in or on the fol- § 180.261 N-(Mercaptomethyl) phthali- lowing raw agricultural commodity: mide S-(O,O-dimethyl phosphoro- Parts per dithioate) and its oxygen analog; Commodity million tolerances for residues. Crabapple ...... 20 (a) General. Tolerances are estab- Pistachio ...... 0.1 lished for the sum of the residues for the insecticide N-(mercaptomethyl) (d) Indirect or inadvertent residues. phthalimide S-(O,O-dimethyl [Reserved] phosphorodithioate) and its oxygen [43 FR 46538, Oct. 10, 1978, as amended at 45 analog N-(mercaptomethyl) phthal- FR 8981, Feb. 11, 1980; 48 FR 37213, Aug. 17, imide S-(O,O-dimethyl 1983; 52 FR 48539, Dec. 23, 1987; 53 FR 657, Jan. phosphorothioate) in or on the fol- 11, 1988; 53 FR 39090, Oct. 5, 1988; 63 FR 57075, lowing raw agricultural commodities: Oct. 26, 1998; 67 FR 49616, July 31, 2002]

Commodity Parts per § 180.262 Ethoprop; tolerances for resi- million dues. Alfalfa ...... 40 (a) General. Tolerances are estab- Almond, hulls ...... 10 Apple ...... 10 lished for residues of the nematocide Apricot ...... 5 and insecticide ethoprop (O-ethyl S,S-

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dipropyl phosphorodithioate) in or on O-(methylcarbamoyl) oxime and its the following raw agricultural com- cholinesterase-inhibiting metabolites modities: 2-methyl 2-(methylsulfinyl) propionaldehyde O-(methylcarbamoyl) Parts per Commodity million oxime and 2-methyl-2-(methylsulfonyl) propionaldehyde O-(methylcarbamoyl) Banana ...... 0.02 oxime in or on the following food com- Bean, lima ...... 0 .02 Bean, snap, succulent ...... 0 .02 modities: Cabbage ...... 0 .02 Corn, forage ...... 0 .02 Commodity Parts per Corn, grain ...... 0 .02 million Corn, stover ...... 0 .02 Corn, sweet, kernel plus cob with husks re- Bean, dry, seed ...... 0 .1 moved ...... 0 .02 Beet, sugar ...... 0 .05 Cucumber ...... 0 .02 Beet, sugar, tops ...... 1 Peanut ...... 0 .02 Citrus, dried pulp ...... 0 .6 Peanut, hay ...... 0.02 Coffee, bean, green ...... 0 .1 Pineapple ...... 0.02 Cotton, undelinted seed ...... 0 .1 Potato ...... 0 .02 Cotton, hulls ...... 0 .3 Sugarcane, cane ...... 0.02 Grapefruit ...... 0 .3 Sweet potato, roots ...... 0 .02 Lemon ...... 0.3 Lime ...... 0.3 Orange, sweet ...... 0 .3 (b) Section 18 emergency exemptions. Peanut ...... 0 .05 [Reserved] Pecan ...... 0 .5 Potato ...... 1 (c) Tolerances with regional registra- Sorghum, grain ...... 0 .2 tions. [Reserved] Sorghum, grain, bran ...... 0 .5 (d) Indirect or inadvertent residues. Sorghum, grain, stover ...... 0 .5 [Reserved] Soybean ...... 0.02 Sugarcane, cane ...... 0.02 [47 FR 53004, Nov. 24, 1982, as amended at 48 Sugarcane, fodder ...... 0.1 Sugarcane, forage ...... 0.1 FR 51485, Nov. 9, 1983; 52 FR 33237, Sept. 2, Sweet potato, roots ...... 0 .1 1987; 53 FR 30053, Aug. 10, 1988; 63 FR 57075, Oct. 26, 1998; 64 FR 39078, July 21, 1999; 66 FR (b) Section 18 emergency exemptions. 38955, July 26, 2001; 67 FR 49616, July 31, 2002] [Reserved] § 180.263 Phosalone; tolerances for res- (c) Tolerances with regional registra- idues. tions. [Reserved] (d) Indirect or inadvertent residues. Tolerances are established for resi- [Reserved] dues of the insecticide phosalone (S-(6- chloro-3-(mercaptomethyl)-2- [65 FR 33710, May 24, 2000, as amended at 69 benzoxazolinone)O,O,-diethyl FR 6567, Feb. 11, 2004] phosphorodithioate) in or on the fol- lowing raw agricultural commodities: § 180.272 Tribuphos; tolerances for res- idues. Parts per (a) General. Tolerances are estab- Commodity million lished for residues of the defoliant Almond ...... 0.1 tribuphos (S,S,S-tributyl Apple ...... 10.0 phosphorotrithioate) in or on food com- Apricot ...... 15 .0 Cherry ...... 15.0 modities as follows: Grape ...... 10 .0 Peach ...... 15 .0 Commodity Parts per Pear ...... 10 .0 million Plum, prune, fresh ...... 15.0 Cattle, fat (negligible residue) ...... 0 .02 Cattle, meat byproducts (negligible residue) ...... 0 .02 [47 FR 42740, Sept. 29, 1982, as amended at 63 Cattle, meat (negligible residue) ...... 0 .02 FR 57066, Oct. 26, 1998; 64 FR 3428, Jan. 22, Cotton, undelinted seed ...... 4 Goat, fat (negligible residue) ...... 0 .02 1999; 67 FR 49616, July 31, 2002] Goat, meat byproducts (negligible residue) ...... 0 .02 Goat, meat (negligible residue) ...... 0 .02 § 180.269 Aldicarb; tolerances for resi- Milk (negligible residue) ...... 0 .002 dues. Sheep, fat (negligible residue) ...... 0 .02 Sheep, meat byproducts (negligible residue) ...... 0 .02 (a) General. Tolerances are estab- Sheep, meat (negligible residue) ...... 0 .02 lished for combined residues of the in- secticide and nematocide aldicarb (2- (b) Section 18 emergency exemptions. methyl-2-(methylthio)propionaldehyde [Reserved]

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(c) Tolerances with regional registra- Commodity Parts per tions. [Reserved] million (d) Indirect or inadvertent residues. Almond ...... 0.05 [Reserved] Almond, hulls ...... 1 .0 Apricot ...... 0 .5 [65 FR 33698, May 24, 2000, as amended at 67 Asparagus ...... 0.1 FR 49616, July 31, 2002] Banana (NMT 0.05 ppm in edible pulp) ...... 0 .5 Bean, dry, seed ...... 0 .1 Bean, snap, succulent ...... 5 § 180.274 Propanil; tolerances for resi- Blueberry ...... 1 .0 dues. Broccoli ...... 5 Brussels sprouts ...... 5 (a) General. Tolerances are estab- Cabbage ...... 5 lished for the combined residues of the Carrot, roots ...... 1 herbicide propanil (3′, 4′- Cauliflower ...... 5 Celery ...... 15 dichloropropionanilide) and its me- Cherry, sweet ...... 0 .5 tabolites convertible to 3, 4- Cherry, tart ...... 0 .5 dichloroaniline (3, 4-DCA) in or on the Cocoa bean, dried bean ...... 0 .05 following food commodities: Coffee, bean, green ...... 0 .20 Corn, sweet, kernel plus cob with husks re- moved ...... 1 Parts per Cranberry ...... 5 .0 Commodity million Cucumber ...... 5 Mango ...... 1.0 Cattle, fat ...... 0.10 Melon ...... 5 Cattle, meat ...... 0 .05 Mushroom ...... 1 .0 Cattle, meat byproducts ...... 1.0 Nectarine ...... 0 .5 Crayfish ...... 0.05 Onion, dry bulb ...... 0 .5 Egg ...... 0 .30 Onion, green ...... 5 Goat, fat ...... 0 .10 Papaya ...... 15 Goat, meat ...... 0.05 Parsnip, roots ...... 1 Goat, meat byproducts ...... 1 .0 Passionfruit ...... 3 Hog, fat ...... 0 .10 Peach ...... 0 .5 Hog, meat ...... 0 .05 Peanut ...... 0 .3 Hog, meat byproducts ...... 1 .0 Pepper, nonbell1) ...... 5 Horse, fat ...... 0 .10 Pistachio ...... 0.2 Horse, meat ...... 0 .05 Plum ...... 0 .2 Horse, meat byproducts ...... 1 .0 Plum, prune ...... 0 .2 Potato ...... 0 .1 Milk ...... 0.05 Pumpkin ...... 5 Poultry, fat ...... 0.05 Soybean ...... 0.2 Poultry, meat ...... 0 .10 Squash, summer ...... 5 Poultry, meat byproducts ...... 0.50 Squash, winter ...... 5 Rice, bran ...... 40 Tomato ...... 5 Rice, grain ...... 10 1 Rice, hulls ...... 30 There are no U.S. registrations as of January, 2001. Rice, straw ...... 75 (2) Tolerances are established for the Sheep, fat ...... 0 .10 Sheep, meat ...... 0.05 metabolite 4-hydroxy-2,5,6- Sheep, meat byproducts ...... 1 .0 trichloroisophthalonitrile in or on the following food commodities. (b) Section 18 emergency exemptions. Parts per [Reserved] Commodity million (c) Tolerances with regional registra- Cattle, fat ...... 0.1 tions. [Reserved] Cattle, kidney ...... 0 .5 (d) Indirect or inadvertent residues. Cattle, meat byproducts, except kidney ...... 0.05 [Reserved] Cattle, meat ...... 0 .03 Goat, fat ...... 0 .1 [63 FR 34827, June 26, 1998, as amended at 72 Goat, kidney ...... 0 .5 FR 28888, May 23, 2007] Goat, meat byproducts, except kidney ...... 0 .05 Goat, meat ...... 0.03 Hog, fat ...... 0 .1 § 180.275 Chlorothalonil; tolerances for Hog, kidney ...... 0.5 residues. Hog, meat byproducts, except kidney ...... 0 .05 Hog, meat ...... 0 .03 (a) General. (1) Tolerances are estab- Horse, fat ...... 0 .1 lished for the fungicide chlorothalonil Horse, kidney ...... 0 .5 (tetrachloroisophthalonitrile) and its Horse, meat byproducts, except kidney ...... 0 .05 metabolite 4-hydroxy-2,5,6- Horse, meat ...... 0 .03 Milk ...... 0.1 trichloroisophthalonitrile in or on the Sheep, fat ...... 0 .1 following food commodities. Sheep, kidney ...... 0.5

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Parts per Parts per Commodity million Commodity million

Sheep, meat byproducts, except kidney ...... 0 .05 Lemon ...... 4.0 Sheep, meat ...... 0.03 Lime ...... 4.0 Nectarine ...... 4 .0 (b) Section 18 emergency exemptions. Orange, sweet ...... 4 .0 Peach ...... 5 .0 Time-limited tolerances are estab- Pear ...... 3 .0 lished for chlorothalonil and its me- Tangerine ...... 4 .0 tabolite 4-hydroxy-2,5,6- trichloroisophthalonitrile (expresed as (b) Section 18 emergency exemptions. chlorothalonil) in connection with use [Reserved] of the pesticide under the section 18 (c) Tolerances with regional registra- emergency exemptions granted by tions. [Reserved] EPA. The tolerances will expire and (d) Indirect or inadvertent residues. are revoked on the dates specified in [Reserved] the following table: [63 FR 34827, June 26, 1998, as amended at 69 Expiration/ FR 43924, July 23, 2004] Commodity Parts per revocation million date § 180.278 Phenmedipham; tolerances for residues. Ginseng ...... 0.10 12/31/07 (a) General. Tolerances are estab- (c) Tolerances with regional registra- lished for the combined residues of the tions. Tolerances with regional reg- herbicide phenmedipham (3- istration, as defined in § 180.1(n), are es- methoxycarbonylaminophenyl-3′- tablished for the combined residues of methylcarbanilate) in or on the fol- chlorothalonil and its metabolite in or lowing food commodities: on the following raw agricultural com- Parts per modities: Commodity million

Commodity Parts per Beet, garden, roots ...... 0 .2 million Beet, garden, tops ...... 0 .2 Beet, sugar, dried pulp ...... 0 .5 Filbert ...... 0 .1 Beet, sugar, molasses ...... 0 .2 Mint hay ...... 2 Beet, sugar, roots ...... 0 .1 Beet, sugar, tops ...... 0.1 (d) Indirect or inadvertent residues. Spinach ...... 4 .0 [Reserved] (b) Section 18 emergency exemptions. [42 FR 56114, Oct. 21, 1977, as amended at 43 FR 22725, May 26, 1978; 46 FR 30500, June 9, [Reserved] 1981; 46 FR 48931, Oct. 5, 1981; 47 FR 23934, (c) Tolerances with regional registra- June 2, 1982; 47 FR 25741, June 15, 1982; 47 FR tions. [Reserved] 42741, Sept. 29, 1982; 49 FR 45852, Nov. 21, 1984; (d) Indirect or inadvertent residues. 50 FR 30172, July 24, 1985; 52 FR 33237, Sept. [Reserved] 2, 1987; 61 FR 10282, Mar. 13, 1996; 62 FR 65376, Dec. 12, 1997; 66 FR 14342, Mar. 12, 2001; 66 FR [72 FR 28888, May 23, 2007] 56245, Nov. 7, 2001; 67 FR 42397, June 21, 2002; 70 FR 708, Jan. 5, 2005] § 180.284 Zinc phosphide; tolerances for residues. § 180.276 Formetanate hydrochloride; (a) General. Tolerances are estab- tolerances for residues. lished for residues of the phosphine re- (a) General. Tolerances are estab- sulting from the use of the rodenticide lished for residues of the insecticide zinc phosphide in or on the raw agricul- formetanate hydrochloride (m- tural commodities as follows: [[(dimethylamino)methylene]amino Parts per ]phenyl methylcarbamate hydro- Commodity million chloride) in or on raw agricultural commodities as follows: Alfalfa, forage ...... 0.2 Alfalfa, hay ...... 0.2 Parts per Barley, grain ...... 0 .05 Commodity million Barley, hay ...... 0 .2 Barley, straw ...... 0 .2 Apple ...... 3.0 Bean, dry, seed ...... 0 .05 Grapefruit ...... 4 .0 Beet, sugar, roots ...... 0 .05

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[[(2,4-dimethylphenyl)imino] methyl]]- Commodity Parts per million N-methylmethanimidamide) and its Beet, sugar, tops ...... 0.2 metabolites N-(2,4-dimethylphenyl)-N- Grape ...... 0 .01 methyl formamide and N-(2,4- Grass (rangeland) ...... 0 .1 dimethylphenyl)-N- Potato ...... 0 .05 Sugarcane, cane ...... 0.01 methylmethanimidamide (both cal- Timothy, hay ...... 0 .5 culated as the parent) in or on the fol- Timothy, forage ...... 0.5 lowing raw agricultural commodities Wheat, forage ...... 0 .05 Wheat, grain ...... 0 .05 (RAC) at the following levels: Wheat, hay ...... 0 .05 Wheat, straw ...... 0 .05 Parts per Commodity million

(b) Section 18 emergency exemptions. Cattle, fat ...... 0.1 Time-limited tolerances are estab- Cattle, meat byproducts ...... 0.3 Cattle, meat ...... 0 .05 lished for residues of phosphine result- Cotton, undelinted seed ...... 1 .0 ing from the use of the rodenticide zinc Egg ...... 0 .01 phosphide in connection with use of the Goat, fat ...... 0 Goat, meat byproducts ...... 0 pesticide under FIFRA section 18 emer- Goat, meat ...... 0 gency exemptions granted by EPA. The Hog, fat ...... 0 .1 tolerances are specified in the fol- Hog, kidney ...... 0.2 Hog, liver ...... 0 .2 lowing table. The tolerances expire on Hog, meat byproducts ...... 0 .3 the date specified in the table. Hog, meat ...... 0 .05 Honey ...... 1.0 Honeycomb ...... 6 .0 Parts per Expiration/ Commodity million Revocation Hop, dried cones ...... 60 .0 Date Milk ...... 0.03 Milk, fat ...... 0 .3 Alfalfa, forage ...... 1.0 12/31/05 Pear ...... 3 Alfalfa, hay ...... 1.0 12/31/05 Poultry fat/meat ...... 0 .01 Clover, forage ...... 0.1 12/31/05 Poultry, meat byproducts ...... 0.05 Clover, hay ...... 0.1 12/31/05 Sheep, fat ...... 0 Timothy, seed ...... 0.1 12/31/05 Sheep, meat byproducts ...... 0 Sheep, meat ...... 0 (c) Tolerances with regional registra- tions. Tolerances with regional reg- (b) Section 18 emergency exemptions. istration, as defined in § 180.1(n), are es- [Reserved] tablished for residues of phosphine re- (c) Tolerances with regional registra- sulting from the use of the rodenticide tions. [Reserved] zinc phosphide in or on the following (d) Indirect or inadvertent residues. raw agricultural commodities as fol- [Reserved] lows: [44 FR 70145, Dec. 6, 1979, as amended at 51 Parts per FR 16846, May 7, 1986; 52 FR 5767, Feb. 26, Commodity million 1987; 57 FR 53568, Nov. 12, 1992; 58 FR 14316, Mar. 17, 1993; 60 FR 12704, Mar. 8, 1995; 67 FR Artichoke, globe ...... 0.01 49616, July 31, 2002] Beet, sugar, roots ...... 0 .04 Beet, sugar, tops ...... 0.02 § 180.288 2-(Thiocyanomethyl- (d) Indirect or inadvertent residues. thio)benzothiazole; tolerances for residues. [Reserved] (a) General. Tolerances are estab- [63 FR 45182, Aug. 25, 1998, as amended at 63 lished for residues of the fungicide 2- FR 67799, Dec. 9, 1998; 64 FR 40772, July 28, (thiocyanomethylthio)benzothiazole in 1999; 64 FR 61791, Nov. 15, 1999; 65 FR 8874, Feb. 23, 2000; 65 FR 49941, Aug. 16, 2000; 65 FR or on the following food commodities: 62634, Oct. 19, 2000; 66 FR 64773, Dec. 14, 2001; Parts per 68 FR 2247, Jan. 16, 2003; 68 FR 56195, Sept. 30, Commodity million 2003; 70 FR 7046, Feb. 10, 2005] Barley, grain ...... 0 .1(N) § 180.287 Amitraz; tolerances for resi- Barley, straw ...... 0 .1(N) Beet, sugar, roots ...... 0 .1(N) dues. Beet, sugar, tops ...... 0.1(N) (a) General. Tolerances are estab- Corn, grain ...... 0 .1(N) Corn, forage ...... 0 .1(N) lished for residues of the insecticide Corn, stover ...... 0 .1(N) amitraz (N′-[2,4-dimethylphenyl]-N- Cotton, forage ...... 0.1(N)

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pentachloroaniline (PCA) and methyl Commodity Parts per million pentachlorophenyl sulfide (MPCPS) in Cotton, undelinted seed ...... 0 .1(N) or on the following raw agricultural Oat, forage ...... 0 .1(N) commodities: Oat, grain ...... 0 .1(N) Oat, hay ...... 0.1(N) Commodity Parts per Oat, straw ...... 0.1(N) million Rice, grain ...... 0 .1(N) Rice, straw ...... 0 .1(N) Collards ...... 0.2 Safflower, seed ...... 0 .1(N) Kale ...... 0 .2 Sorghum, grain, forage ...... 0.1(N) Mustard greens ...... 0.2 Sorghum, grain, grain ...... 0 .1(N) Sorghum, grain, stover ...... 0 .1(N) Wheat, forage ...... 0 .1(N) [36 FR 22540, Nov. 25, 1971, as amended at 53 Wheat, grain ...... 0 .1(N) FR 9443, Mar. 23, 1988; 71 FR 74816, Dec. 13, Wheat, hay ...... 0 .1(N) 2006] Wheat, straw ...... 0 .1(N) § 180.292 Picloram; tolerances for resi- (b) Section 18 emergency exemptions. dues. [Reserved] (a) General. (1) Tolerances are estab- (c) Tolerances with regional registra- lished for residues of the pesticide tions. [Reserved] picloram (4-amino-3,5,6- (d) Indirect or inadvertent residues. trichloropicolinic acid) from its appli- [Reserved] cation in the acid form or in the form [68 FR 39440, July 1, 2003] of its potassium, triethylamine, or triisopropanolamine salts expressed as § 180.289 Methanearsonic acid; toler- picloram in or on the following raw ag- ances for residues. ricultural commodities: (a) General. Tolerances are estab- Parts per lished for residues of the herbicide Commodity million methanearsonic acid (calculated as As2 Barley, grain ...... 0 .5 O3) from application of the disodium Barley, straw ...... 1 and monosodium salts of Cattle, fat ...... 0.2 methanearsonic acid in or on raw agri- Cattle, kidney ...... 5 Cattle, liver ...... 0 .5 cultural commodities as follows: Cattle, meat ...... 0 .2 Cattle, meat byproducts, except kidney and liver 0.2 Commodity Parts per Egg ...... 0 .05 million Goat, fat ...... 0 .2 Goat, meat ...... 0.2 Cotton, undelinted seed ...... 0 .7 Goat, meat byproducts, except kidney and liver 0 .2 Cotton, hulls ...... 0 .9 Goat, kidney ...... 5 Fruit, citrus ...... 0 .35 Goat, liver ...... 0.5 Grass, forage ...... 80 (b) Section 18 emergency exemptions. Hog, meat byproducts, except kidney and liver .. 0 .2 [Reserved] Hog, fat ...... 0 .2 Hog, kidney ...... 5 (c) Tolerances with regional registra- Hog, liver ...... 0 .5 tions. [Reserved] Hog, meat ...... 0 .2 (d) Indirect or inadvertent residues. Horse, meat byproducts, except kidney and liver 0 .2 Horse, fat ...... 0 .2 [Reserved] Horse, kidney ...... 5 Horse, liver ...... 0 .5 [63 FR 34828, June 26, 1998] Horse, meat ...... 0 .2 Milk ...... 0.05 § 180.291 Pentachloronitrobenzene; tol- Oat, forage ...... 1 erance for residues. Oat, grain ...... 0 .5 Oat, straw ...... 1 (a) A tolerance of 0.1 part per million Poultry, fat ...... 0.05 is established for negligible residues of Poultry, meat byproducts ...... 0.05 the fungicide pentachloronitrobenzene Poultry, meat ...... 0 .05 Sheep, fat ...... 0 .2 in or on the raw agricultural com- Sheep, kidney ...... 5 modity cotton, undelinted seed. Sheep, liver ...... 0.5 (b) Tolerances with regional registra- Sheep, meat ...... 0.2 Sheep, meat byproducts, except kidney and tion (refer to § 180.1 (n)) are established liver ...... 0 .2 for the combined residues of the fun- Wheat, grain ...... 0 .5 gicides pentachloronitrobenzene Wheat, forage ...... 1 (PCNB) and its metabolites Wheat, straw ...... 1

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(2) Tolerances are established for res- Commodity Parts per idues of picloram [4-amino-3,5,6- million trichloropicolinic acid] resulting from Hop ...... 0 .1 the application of the pesticide to Potato ...... 0 .1 growing crops in the following: Rice, grain ...... 0 .05(N) Rice, straw ...... 0 .05(N) Parts per Food million (2) An interim tolerance of 0.2 parts Barley, milled fractions (exc flour) ...... 3 per million is established for residues Oat, groats/rolled oats ...... 3 of the herbicide endothall (7 - Wheat, milled fractions (exc flour) ...... 3 oxabicyclo[2.2.1] heptane-2,3- dicarboxylic acid) in water, potable (3) Tolerances are established for res- from use of its potassium, sodium, di- idues of picloram [4-amino-3,5,6- N, N-dimethylalkylamine, and mono-N- trichloro-picolinic acid] resulting from N,-dimethylalkylamine salts as the application of the pesticide to algicides or herbicides to control growing crops in the following: aquatic plants in canals, lakes, ponds, Parts per and other potential sources of water, Food million potable. (b) Section 18 emergency exemptions. Barley, milled fractions (exc flour) ...... 3 Oat, groats/rolled oats ...... 3 [Reserved] Wheat, milled fractions (exc flour) ...... 3 (c) Tolerances with regional registra- tions. [Reserved] (b) Section 18 emergency exemptions. (d) Indirect or inadvertent residues. [Reserved] [Reserved] (c) Tolerances with regional registra- [41 FR 23717, June 11, 1976, as amended at 51 tions. [Reserved] FR 4498, Feb. 5, 1986; 62 FR 49931, Sept. 24, (d) Indirect or inadvertent residues. 1997; 63 FR 42249, Aug. 7, 1998; 67 FR 35048, Tolerances are established for indirect May 17, 2002; 71 FR 47106, Aug. 16, 2006; 71 FR or indadvertent residues of the herbi- 74816, Dec. 13, 2006] cide picloram, 4-amino-3,5,6- trichloropicolinic acid, from applica- § 180.294 Benomyl; tolerances for resi- tion of its potassium form on barley, dues. fallow cropland, oats, and wheat in or (a) General. Tolerances are estab- on the following raw agricultural com- lished for the combined residues of the modities: fungicide benomyl (methyl 1- (butylcarbamoyl)-2- Expiration/ Parts per benzimidazolecarbamate) and its me- Commodity million Revocation Date tabolites containing the benzimidazole Grain, aspirated fractions ...... 4.0 12/31/00 moiety (calculated as benomyl) in or Sorghum, grain ...... 0.3 12/31/00 on the following raw agricultural com- Sorghum grain, forage ...... 0.2 12/31/00 modities: Sorghum grain, stover ...... 0.5 12/31/00 Expira- Parts tion/Rev- [41 FR 19221, May 11, 1976, as amended at 47 Commodity per mil- ocation FR 53005, Nov. 24, 1982; 64 FR 425, Jan. 5, 1999; lion Date 64 FR 39082, July 21, 1999] Almond, hulls ...... 1.0 1/1/07 Apple, postharvest ...... 7.0 1/1/08 § 180.293 Endothall; tolerances for res- Apricot, postharvest ...... 15.0 1/1/08 idues. Banana, postharvest, not more than (a) General. (1) Tolerances are estab- 0.2 ppm shall be present in the pulp after peel is removed and discarded 1.0 1/1/08 lished for combined residues of Barley, grain ...... 0.2 1/1/08 Endothall, 7-oxabicyclo [2, 2, 1] Barley, straw ...... 0.2 1/1/08 heptane-2, 3-dicarboxylic acid and its Bean ...... 2.0 1/1/07 Beet, sugar, roots ...... 0.2 1/1/07 monomethyl ester in or on the fol- Beet, sugar, tops ...... 15.0 1/1/07 lowing raw agricultural commodities: Blackberry ...... 7.0 1/1/08 Blueberry ...... 7.0 1/1/08 Boysenberry ...... 7.0 1/1/08 Commodity Parts per million Broccoli ...... 0.2 1/1/06 Brussels sprouts ...... 15.0 1/1/06 Cotton, undelinted seed ...... 0 .1 Cabbage ...... 0.2 1/1/06 Fish ...... 0 .1 Cabbage, chinese, bok choy ...... 10.0 1/1/06

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Expira- Expira- Parts tion/Rev- Parts tion/Rev- Commodity per mil- ocation Commodity per mil- ocation lion Date lion Date

Cabbage, chinese, napa ...... 10.0 1/1/06 Strawberry ...... 5.0 1/1/08 Carrot, roots ...... 0.2 1/1/07 Sweet potato, roots ...... 0.2 1/1/07 Cattle, fat ...... 0.1 1/1/08 Tomato ...... 5.0 1/1/09 Cattle, meat ...... 0.1 1/1/08 Tomato, concentrated products ...... 50.0 1/1/09 Cattle, meat byproducts ...... 0.1 1/1/08 Turnip, roots ...... 0.2 1/1/07 Cauliflower ...... 0.2 1/1/06 Wheat, grain ...... 0.2 1/1/08 Celery ...... 3.0 1/1/07 Wheat, straw ...... 15.0 1/1/08 Cherry, postharvest ...... 15.0 1/1/08 Citrus, dried pulp ...... 50.0 1/1/08 Collards ...... 0.2 1/1/06 (b) Section 18 emergency exemptions. Corn, sweet, forage ...... 0.2 1/1/08 [Reserved] Corn, sweet, kernel plus cob with (c) Tolerances with regional registra- husks removed ...... 0.2 1/1/08 Corn, sweet, stover ...... 0.2 1/1/08 tions. Tolerances with regional reg- Cucumber ...... 1.0 1/1/07 istration, as defined in § 180.1(n), are es- Currant ...... 7.0 1/1/08 tablished for residues of the fungicide Dewberry ...... 7.0 1/1/08 Egg ...... 0.1 1/1/08 benomyl (methyl 1-[butylcarbamoyl]-2- Eggplant ...... 0.2 1/1/09 benzimidazolecarbamate) and its me- Fruit, citrus, postharvest ...... 10.0 1/1/08 tabolites containing the benzimidazole Garlic ...... 0.2 1/1/06 Goat, fat ...... 0.1 1/1/08 moiety (calculated as benomyl) in or Goat, meat ...... 0.1 1/1/08 on the raw agricultural commodities. Goat, meat byproducts ...... 0.1 1/1/08 Grape ...... 10.0 1/1/08 Parts Expira- Grape, raisin ...... 50.0 1/1/08 Commodity per mil- tion/Rev- Hog, fat ...... 0.1 1/1/08 lion ocation Hog, meat ...... 0.1 1/1/08 Date Hog, meat byproducts ...... 0.1 1/1/08 Horse, fat ...... 0.1 1/1/08 Avocado ...... 3.0 1/1/08 Horse, meat ...... 0.1 1/1/08 Dandelion, leaves ...... 10.0 1/1/07 Horse, meat byproducts ...... 0.1 1/1/08 Papaya ...... 3.0 1/1/08 Kale ...... 0.2 1/1/06 Pistachio ...... 0.2 1/1/07 Kohlrabi ...... 0.2 1/1/06 Turnip, greens ...... 6.0 1/1/07 Loganberry ...... 7.0 1/1/08 Watercress ...... 10.0 1/1/07 Mango ...... 3.0 1/1/08 Melon ...... 1.0 1/1/07 (d) Indirect or inadvertent residues. Milk ...... 0.1 1/1/08 Mushroom, postharvest ...... 10.0 1/1/08 [Reserved] Mustard greens ...... 0.2 1/1/06 Nectarine, postharvest ...... 15.0 1/1/08 [52 FR 58536, Dec. 23, 1987, as amended at 52 Nut ...... 0.2 1/1/07 FR 58538, Dec. 23, 2987; 53 FR 9024, Mar. 18, Oat, grain ...... 0.2 1/1/08 1988; 59 FR 46354, Sept. 8, 1994; 63 FR 2167, Oat, straw ...... 0.2 1/1/08 Jan. 14, 1998; 67 FR 46905, July 17, 2002] Peach, postharvest ...... 15.0 1/1/08 Peanut ...... 0.2 1/1/08 Peanut, hay ...... 15.0 1/1/08 § 180.296 Dimethyl phosphate of 3-hy- Pear, postharvest ...... 7.0 1/1/08 droxy-N-methyl-cis-crotonamide; Pepper ...... 0.2 1/1/09 tolerances for residues. Pineapple, postharvest ...... 35.0 1/1/08 Pistachio ...... 0.2 1/1/07 (a) General. Tolerances are estab- Plum, postharvest ...... 15.0 1/1/08 lished for residues of the insecticide Plum, prune, fresh, postharvest ...... 15.0 1/1/08 Dimethyl phosphate of 3-hydroxy-N- Poultry, fat ...... 0.1 1/1/08 methyl-cis-crotonamide in or on the Poultry, liver ...... 0.2 1/1/08 Poultry, meat ...... 0.1 1/1/08 following raw agricultural commod- Poultry, meat byproducts, except liver 0.1 1/1/08 ities: Pumpkin ...... 1.0 1/1/07 Raspberry ...... 7.0 1/1/08 Expiration/ Rice, grain ...... 5.0 1/1/08 Parts per Commodity million Revocation Rice, hulls ...... 20.0 1/1/08 date Rice, straw ...... 15.0 1/1/08 Rutabaga ...... 0.2 1/1/07 Cotton, undelinted seed ...... 0.1 12/31/00 Rye, grain ...... 0.2 1/1/08 Peanut ...... 0.05 12/31/00 Rye, straw ...... 0.2 1/1/08 Potato ...... 0.1 12/31/00 Sheep, fat ...... 0.1 1/1/08 Sugarcane, cane ...... 0.1 12/31/00 Sheep, meat ...... 0.1 1/1/08 Tomato ...... 0.5 12/31/00 Sheep, meat byproducts ...... 0.1 1/1/08 Tomato, concentrated products ...... 2.0 12/31/00 Soybean ...... 0.2 1/1/07 Spinach ...... 0.2 1/1/07 Squash, summer ...... 1.0 1/1/07 (b) Section 18 emergency exemptions. Squash, winter ...... 1.0 1/1/07 [Reserved]

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(c) Tolerances with regional registra- Commodity Parts per tions. [Reserved] million (d) Indirect or inadvertent residues. Walnut ...... 0 .05 [Reserved] [64 FR 19492, Apr. 21, 1999] (b) Section 18 emergency exemptions. [Reserved] § 180.297 N-1-Naphthyl phtha- (c) Tolerances with regional registra- lamic acid; tolerances for residues. tions. Tolerances with regional reg- (a) General. Tolerances are estab- istration, as defined in § 180.1(n), are es- lished for residues of the herbicide N-1- tablished for residues of the insecticide naphthyl phthalamic acid from appli- methidathion (O,O-dimethyl cation of its sodium salt in or on the phosphorodithioate, S-ester with 4- following raw agricultural commod- (mercaptomethyl-2-methoxy-1,3,4- ities: thiadiazolin-5-one), in or on the fol- lowing raw agricultural commodity: Parts per Commodity million Parts per Commodity million Cantaloupe ...... 0 .1(N) Cucumber ...... 0 .1(N) Kiwifruit ...... 0.1 Muskmelon ...... 0 .1(N) Longan ...... 0 .1 Watermelon ...... 0.1(N) Starfruit ...... 0 .1 Sugar apple ...... 0 .2 (b) Section 18 emergency exemptions. (d) Indirect or inadvertent residues. [Reserved] [Reserved] (c) Tolerances with regional registra- tions. [Reserved] [43 FR 44845, Sept. 29, 1978, as amended at 43 (d) Indirect or inadvertent residues. FR 45363, Oct. 2, 1978; 46 FR 18314, Mar. 24, [Reserved] 1981; 50 FR 1054, Jan. 9, 1985; 50 FR 5070, Feb. 6, 1985; 53 FR 23391, June 22, 1988; 54 FR 20125, [45 FR 32306, May 16, 1980, as amended at 63 May 10, 1989; 55 FR 2377, Jan. 24, 1990; 55 FR FR 57075, Oct. 26, 1998] 24083, June 14, 1990; 55 FR 49389, Nov. 28, 1990; 57 FR 31325, July 15, 1992; 63 FR 57075, Oct. 26, § 180.298 Methidathion; tolerances for 1998; 66 FR 50833, Oct. 5, 2001] residues. (a) General. Tolerances are estab- § 180.299 Dimethyl phosphate of 3-hy- droxy-N,N-dimethyl-cis-crotona- lished for residues of the insecticide mide; tolerances for residues. methidathion (O,O-dimethyl phosphorodithioate, S-ester with 4- Tolerances are established for resi- (mercaptomethyl-2-methoxy-1,3,4- dues of the insecticide dimethyl phos- thiadiazolin-5-one) in or on the fol- phate of 3-hydroxy-N,N-dimethyl-cis- lowing raw agricultural commodities: crotonamide in or on the following raw agricultural commodities: Commodity Parts per million Parts per Commodity million Alfalfa ...... 12 Alfalfa, hay ...... 12 Cotton, undelinted seed ...... 0 .05(N) Almond, hulls ...... 6 Artichoke, globe ...... 0.05 Cotton, undelinted seed ...... 0 .2 [47 FR 55224, Dec. 8, 1982, as amended at 64 Fruit, citrus (except mandarins) ...... 2 .0 FR 39082, July 21, 1999] Fruit, pome ...... 0.05 Fruit, stone ...... 0 .05 § 180.300 Ethephon; tolerances for resi- Grass ...... 12 dues. Grass, hay ...... 12 Mango ...... 0.05 (a) General. Tolerances are estab- Nut ...... 0 .05 lished for residues of the plant regu- Olive ...... 0 .05 Peach ...... 0 .05 lator ethephon [(2-chloroethyl) phos- Pecan ...... 0 .05 phonic acid] in or on food commodities Safflower, seed ...... 0 .5 as follows: Sorghum, forage ...... 2 Sorghum, grain ...... 0 .2 Parts per Sorghum, grain, stover ...... 2 Commodity million Sunflower, seed ...... 0.5 Tangerine ...... 6 .0 Apple ...... 5

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Parts per Parts per Commodity million Commodity million

Barley, bran ...... 5 .0 Barley, grain ...... 0 .2 Barley, grain ...... 2 .0 Barley, straw ...... 0 .2 Barley, pearled barley ...... 5 .0 Bean, dry, seed ...... 0 .2 Barley, straw ...... 10 .0 Bean, succulent ...... 0 .2 Blackberry ...... 30 Canola, seed ...... 0 .03 Blueberry ...... 20 Cattle, fat ...... 0.05 Cantaloupe ...... 2 Cattle, meat byproducts ...... 0.1 Cattle, fat ...... 0.1 Cattle, meat ...... 0 .05 Cattle, meat byproducts ...... 0.1 Corn, field, forage ...... 0 .2 Cattle, meat ...... 0 .1 Corn, field, grain ...... 0 .2 Cherry ...... 10 Corn, field, stover ...... 0 .2 Coffee, bean, green ...... 0 .1(N) Corn, pop, grain ...... 0.2 Cotton, undelinted seed ...... 2 .0 Corn, pop, stover ...... 0.2 Cranberry ...... 5 Corn, sweet, forage ...... 0 .2 Cucumber ...... 0 .1 Corn, sweet, kernel plus cob with husks re- Fig ...... 5 moved ...... 0 .2 Goat, fat ...... 0 .1 Corn, sweet, stover ...... 0 .2 Goat, meat byproducts ...... 0 .1 Cotton, undelinted seed ...... 0 .2 Goat, meat ...... 0.1 Egg ...... 0 .05 Grape ...... 2 .0 Goat, fat ...... 0 .05 Grape, raisin ...... 12 Goat, meat byproducts ...... 0 .1 Hog, fat ...... 0 .1 Goat, meat ...... 0.05 Hog, meat byproducts ...... 0 .1 Hog, fat ...... 0 .05 Hog, meat ...... 0 .1 Hog, meat byproducts ...... 0 .1 Horse, fat ...... 0 .1 Hog, meat ...... 0 .05 Horse, meat byproducts ...... 0 .1 Horse, fat ...... 0 .05 Horse, meat ...... 0 .1 Horse, meat byproducts ...... 0 .1 Milk ...... 0.1 Horse, meat ...... 0 .05 Nut, macadamia ...... 0.5 Milk ...... 0.05 Pepper ...... 30 Oat, forage ...... 0 .5 Pineapple ...... 2 Oat, grain ...... 0 .2 Pumpkin ...... 0.1 Oat, straw ...... 0.2 Sheep, fat ...... 0 .1 Onion, bulb ...... 0 .2 Sheep, meat byproducts ...... 0 .1 Peanut ...... 0 .2 Sheep, meat ...... 0.1 Peanut, hay ...... 0.2 Sugarcane, molasses ...... 1 .5 Poultry, fat ...... 0.1 Tomato ...... 2 Poultry, meat byproducts ...... 0.1 Walnut ...... 0 .5 Poultry, meat ...... 0 .1 Wheat, bran ...... 5.0 Rice, grain ...... 0 .2 Wheat, grain ...... 2 .0 Rice, straw ...... 0 .2 Wheat, middlings ...... 5 .0 Safflower, seed ...... 0 .2 Wheat, shorts ...... 5 .0 Sheep, fat ...... 0 .05 Wheat, straw ...... 10 .0 Sheep, meat byproducts ...... 0 .1 Sheep, meat ...... 0.05 Soybean, seed ...... 0 .2 (b) Section 18 emergency exemptions. Wheat, forage ...... 0 .5 [Reserved] Wheat, grain ...... 0 .2 (c) Tolerances with regional registra- Wheat, straw ...... 0 .2 tions. A tolerance with regional reg- istration, as defined in § 180.1(n), of 0.1 (b) Section 18 emergency exemptions. part per million is established for resi- [Reserved] dues of the plant regulator ethephon (c) Tolerances with regional registra- [(2-chloroethyl)phosphonic acid] in or tions. [Reserved] on the food commodity sugarcane. (d) Indirect or inadvertent residues. [Reserved] (d) Indirect or inadvertent residues. [Reserved] [47 FR 55222, Dec. 8, 1982, as amended at 50 FR 81, Jan. 2, 1985; 62 FR 4915, Feb. 3, 1997; 63 [65 FR 33710, May 24, 2000] FR 4586, Jan. 30, 1998; 64 FR 11801, Mar. 10, 1999; 66 FR 9773, Feb. 12, 2001; 66 FR 64773, § 180.301 Carboxin; tolerances for resi- Dec. 14, 2001; 67 FR 40218, June 12, 2002; 67 FR dues. 72853, Dec. 9, 2002; 71 FR 56383, Sept. 27, 2006] (a) General. Tolerances are estab- lished for the combined residues of the § 180.303 Oxamyl; tolerances for resi- fungicide carboxin (5,6-dihydro-2-meth- dues. yl-1,4-oxathiin-3-carboxanilide) and its (a) General. (1) Tolerances are estab- metabolites determined as and lished for the sum of the residues of the expressed as parent compound, in or on insecticide oxamyl (methyl N-N-di- food commodities as follows: methyl-N-[(methylcarbamoyl)-oxy]-1-

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thiooxamimidate) and its oxime me- Commodity Parts per tabolite N,N-dimethyl-N-hydroxy-1- million thiooxamimidate calculated as oxamyl Berry, group 13 ...... 0 .05 in or on the following food commod- Cranberry ...... 0 .05 ities: Fig ...... 0 .05 Fruit, citrus, group 10 ...... 0 .05 Parts per Fruit, pome, group 11 ...... 0.05 Commodity million Fruit, stone, group 12 ...... 0 .05 Apple ...... 2 Grape ...... 0 .05 Banana ...... 0.3 Kiwifruit ...... 0.05 Cantaloupe ...... 2 .0 Nut, tree, group 14 ...... 0 .05 Celery ...... 3 Olive ...... 0 .05 Cotton, undelinted seed ...... 0 .2 Pistachio ...... 0.05 Cucumber ...... 2 .0 Pomegranate ...... 0 .05 Eggplant ...... 2.0 Strawberry ...... 0 .05 Fruit, citrus ...... 3 Melon, honeydew ...... 2.0 Peanut ...... 0 .2 (b) Section 18 emergency exemptions. Peanut, hay ...... 2.0 [Reserved] Pear ...... 2 .0 Peppermint, tops ...... 10 .0 (c) Tolerances with regional registra- Pepper, bell ...... 3 tions. Tolerances with regional reg- Pepper, nonbell ...... 5 .0 istration, as defined in § 180.1(n), are es- Pineapple ...... 1 tablished for residues of oryzalin, 3,5- Potato ...... 0 .1 Pumpkin ...... 2.0 dinitro-N4,N4-dipropylsulfanilamide, in Soybean ...... 0.2 or on the following raw agricultural Spearmint, tops ...... 10 .0 commodities: Squash, summer ...... 2 .0 Squash, winter ...... 2 .0 Parts per Tomato ...... 2 Commodity million Vegetable, root ...... 0 .1 Watermelon ...... 2.0 Guava ...... 0 .05 Papaya ...... 0 .05 (2) A tolerance of 6 parts per million is established for residues of the insec- (d) Indirect or inadvertent residues. ticide oxamyl (methyl N,N-dimethyl-N- [Reserved] [(methylcarbamoyl)oxy]-1- thiooxamimidate) in pineapple, bran as [71 FR 54434, Sept. 15, 2006] a result of application of the insecti- cide to growing pineapple. § 180.309 ù-Naphthaleneacetamide; tol- erances for residues. (b) Section 18 emergency exemptions. [Reserved] (a) General. Tolerances are estab- (c) Tolerances with regional registra- lished for combined negligible residues tions. [Reserved] of the plant regulatora- (d) Indirect or inadvertent residues. naphthaleneacetamide and its metabo- [Reserved] lite a-naphthaleneacetic acid (cal- [65 FR 33698, May 24, 2000, as amended at 67 culated asa-naphthaleneacetic acid) in FR 41807, June 19, 2002; 67 FR 49617, July 31, or on the following food commodities: 2002] Parts per Commodity million § 180.304 Oryzalin; tolerances for resi- dues. Apple ...... 0.1 (a) General. Tolerances are estab- Pear ...... 0 .1 lished for residues of the herbicide (b) Section 18 emergency exemptions. oryzalin, 3,5-dinitro-N4,N4- dipropylsulfanilamide, in or on the fol- [Reserved] lowing raw agricultural commodities: (c) Tolerances with regional registra- tions. [Reserved] Parts per Commodity million (d) Indirect or inadvertent residues. [Reserved] Almond, hulls ...... 0 .05 Avocado ...... 0 .05 [68 FR 39440, July 1, 2003]

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§ 180.311 Cacodylic acid; tolerances for tabolite 2, 3, 3-trichloroprop-2- residues. enesulfonic acid (TCPSA) in or on the (a) General. Tolerances are estab- following food commodities: lished for residues of the defoliant cac- Parts per odylic acid (dimethylarsinic acid), ex- Commodity million pressed as As2O3, in or on the following raw agricultural commodity as follows: Barley, grain ...... 0 .05 Barley, hay ...... 1 .0 Barley, straw ...... 0 .3 Commodity Parts per million Beet, sugar, dried pulp ...... 0 .2 Beet, sugar, roots ...... 0 .1 Cotton, undelinted seed ...... 2 .8 Beet, sugar, tops ...... 0.5 Pea, dry ...... 0 .2 (b) Section 18 emergency exemptions. Pea, field, hay ...... 1.0 [Reserved] Pea, field, vines ...... 0 .5 (c) Tolerances with regional registra- Pea, succulent ...... 0 .2 tions. [Reserved] Wheat, grain ...... 0 .05 (d) Indirect or inadvertent residues. Wheat, hay ...... 1 .0 [Reserved] Wheat, straw ...... 1 .0 [69 FR 6567, Feb. 11, 2004] (d) Indirect or inadvertent residues. [Reserved] § 180.312 4-Aminopyridine; tolerances for residues. [72 FR 28888, May 23, 2007] (a) General. Tolerances are estab- lished for residues of the bird repellent § 180.315 Methamidophos; tolerances for residues. 4-aminopyridine in or on the following food commodities: (a) Tolerances are established for res- idues of the insecticide methamidophos Expiration/ Commodity Parts per Revocation (O,S-dimethyl phosphoramidothioate) million Date in or on the following raw agricultural

Corn, field, forage ...... 0.1 1/15/06 commodities: Corn, field, grain ...... 0.1 1/15/06 Corn, field, stover ...... 0.1 1/15/06 Commodity Parts per Corn, pop, grain ...... 0.1 1/15/06 million Corn, pop, stover ...... 0.1 1/15/06 Corn, sweet, forage ...... 0.1 1/15/06 Broccoli ...... 1 .0 Corn, sweet, kernel plus cob with Brussels sprouts ...... 1 .0 husks removed ...... 0.1 1/15/06 Cabbage ...... 1 .0 Corn, sweet, stover ...... 0.1 1/15/06 Cauliflower ...... 1 .0 Sunflower, seed ...... 0.1 1/15/06 Cotton, undelinted seed ...... 0 .1 Cucumber ...... 1 .0 (b) Section 18 emergency exemptions. Eggplant ...... 1.0 [Reserved] Lettuce ...... 1.0 (c) Tolerances with regional registra- Melon ...... 0 .5 Pepper ...... 1 .0 tions. [Reserved] Potato ...... 0 .1 (d) Indirect or inadvertent residues. Tomato ...... 1.0 [Reserved] [68 FR 39441, July 1, 2003, as amended at 70 (b) Tolerances with regional registra- FR 55268, Sept. 21, 2005] tion, as defined in § 180.1(n), are estab- lished for residues of methamidophos § 180.314 Triallate; tolerances for resi- in or on the following raw agricultural dues. commodities: (a) General. [Reserved] (b) Section 18 emergency exemptions. Parts per Commodity million [Reserved] (c) Tolerances with regional registra- Celery ...... 1 tions. Tolerances with a regional reg- istration, as defined in 180.1(m),are es- [47 FR 13525, Mar. 31, 1982, as amended at 48 tablished for residues of the herbicide FR 44537, Sept. 29, 1983; 52 FR 33238, Sept. 2, (S-2, 3, 4-trichloroallyl 1987; 67 FR 49617, July 31, 2002] diisopropylthiocarbamate) and its me-

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§ 180.316 Pyrazon; tolerances for resi- Commodity Parts per dues. million (a) General. Tolerances are estab- Horse, meat ...... 0 .02 lished for combined residues of the her- Lettuce ...... 1.0 Milk ...... 0.02 bicide pyrazon (5-amino-4-chloro-2- Nongrass animal feed ...... 10 .0 phenyl-3(2H)-pyridazinone) and its me- Pear ...... 0 .1 tabolites (calculated as pyrazon) in or Poultry, fat ...... 0.02 Poultry, kidney ...... 0 .2 on the following food commodities: Poultry, liver ...... 0 .2 Poultry, meat byproductsidney, liver ...... 0 .02 Commodity Parts per Poultry, meat ...... 0 .02 million Radicchio, greens (tops) ...... 2.0 Raspberry ...... 0 .05 Beet, garden, roots ...... 0 .1(N) Sheep, fat ...... 0 .02 Beet, garden, tops ...... 1 Sheep, kidney ...... 0.4 Beet, sugar, roots ...... 0 .1(N) Sheep, liver ...... 0.4 Beet, sugar, tops ...... 1 Sheep, meat byproducts, except kidney, liver .... 0 .02 Milk ...... 0.01(N) Sheep, meat ...... 0.02

(b) Section 18 emergency exemptions. (b) Section 18 emergency exemptions. [Reserved] Time-limited tolerances are estab- (c) Tolerances with regional registra- lished for the residues of propyzamide, tions. [Reserved] in connection with use of the pesticide (d) Indirect or inadvertent residues. under section 18 emergency exemptions [Reserved] granted by EPA. The tolerances will [68 FR 39441, July 1, 2003] expire on the dates specified in the fol- lowing table. § 180.317 Propyzamide; tolerances for residues. Expiration/ Commodity Parts per Revocation (a) General. Tolerances are estab- million Date lished for combined residues of the her- Cranberry ...... 0.05 12/31/09 bicide propyzamide and its metabolites (containing the 3,5-dichlorobenzoyl (c) Tolerances with regional registra- moiety and calculated as 3,5-dichloro- tions. Tolerances with regional reg- N-(1,1-dimethyl-2-propynyl)benzamide) istration are established for the com- in or on the following raw agricultural bined residues of the herbicide commodities: propyzamide and its metabolites (con- taining the 3,5-dichlorobenzoyl moiety Parts per Commodity million and calculated as 3,5-dichloro-N-(1,1-di- methyl-2-propynyl)benzamide) in or on Apple ...... 0.1 Artichoke, globe ...... 0.1 the following raw agricultural com- Blackberry ...... 0 .05 modities: Blueberry ...... 0 .05 Boysenberry ...... 0 .05 Commodity Parts per Cattle, fat ...... 0.02 million Cattle, kidney ...... 0 .4 Cattle, liver ...... 0 .4 Pea, dried (winter) ...... 0 .05 Cattle, meat byproducts, except kidney, liver ..... 0 .02 Rhubarb ...... 0 .1 Cattle, meat ...... 0 .02 Egg ...... 0 .02 (d) Indirect or inadvertent residues. Endive ...... 1.0 [Reserved] Fruit, stone ...... 0 .1 Goat, fat ...... 0 .02 [61 FR 10284, Mar. 13, 1996, as amended at 63 Goat, kidney ...... 0 .4 FR 49486, Sept. 16, 1998; 64 FR 6532, Feb. 10, Goat, liver ...... 0.4 Goat, meat byproducts, except kidney, liver ...... 0 .02 1999; 66 FR 64773, Dec. 14, 2001; 67 FR 35048, Goat, meat ...... 0.02 May 17, 2002; 69 FR 2073, Jan. 14, 2004; 71 FR Grape ...... 0 .1 76199, Dec. 20, 2006] Hog, fat ...... 0 .02 Hog, kidney ...... 0.4 § 180.318 4-(2-Methyl-4-chlorophenoxy) Hog, liver ...... 0 .4 butyric acid; tolerance for residues. Hog, meat byproducts, except kidney, liver ...... 0 .02 Hog, meat ...... 0 .02 (a) General. A tolerance is established Horse, fat ...... 0 .02 for the herbicide 4-(2-methyl-4- Horse, kidney ...... 0 .4 Horse, liver ...... 0 .4 chlorophenoxy) butyric acid in or on Horse, meat byproducts, except kidney, liver ..... 0 .02 the following food commodity:

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Parts per § 180.319 Interim tolerances. Commodity million While petitions for tolerances for Pea ...... 0 .1(N) negligible residues are pending and (b) Section 18 emergency exemptions. until action is completed on these peti- [Reserved] tions, interim tolerances are estab- (c)Tolerances with regional registra- lished for residues of the listed pes- tions. [Reserved] ticide chemicals in or on the following (d) Indirect or inadvertent residues. raw agricultural commodities: [Reserved] [68 FR 39441, July 1, 2003]

Tolerance in parts Substances Uses per million Raw agricultural commodity

Carbaryl (1-naphthyl N-methylcarbamate Insecticide 0.5 ...... Egg and its metabolite 1-naphthol, cal- culated as carbaryl. Coordination product of zinc ion and Fungicide 1.0 (Calculated as Potato maneb. zinc ethylenebisdithio- carbamate) Endothall (7-oxabicyclo-(2,2,1) heptane Herbicide 0.2 ...... Beet, sugar 2,3- dicarboxylic acid). Isopropyl carbanilate (IPC) ...... Herbicide 5.0 ...... Alfalfa, hay; clover, hay; and grass, hay ...... 2.0 ...... Alfalfa, forage; clover, forage; and grass, forage ...... 0.1 ...... Flax, seed; lentil; lettuce, head and let- tuce, leaf; pea; safflower, seed; spin- ach; and beet, sugar, roots and beet, sugar, tops ...... 0.5 ...... Egg; cattle, fat; cattle meat; cattle, meat byproducts; goat, fat; goat, meat; goat, meat byproducts; hog, fat; hog, meat; hog, meat byproducts; horse, fat; horse, meat; horse, meat byprod- ucts; milk; sheep, fat; sheep meat; sheep, meat byproducts; poultry, fat; poultry, meat; poultry, meat byprod- ucts Isopropyl m-chlorocarbanilate (CIPC)...... Herbicide 0.05 ...... Milk; cattle, fat; cattle, meat; cattle, meat byproducts; goat, fat; goat, meat; goat, meat byproducts; hog, fat; hog, meat; hog, meat byproducts; horse, fat; horse, meat; horse, meat byprod- ucts; sheep, fat; sheep meat; sheep, meat byproducts Parathion (O,O-diethyl-O-p- Herbicide 0.5 ...... Rye nitrophenythiophosphate) or its methyl homolog. Pentachloronitrobenzene ...... Fungicide 1.0 ...... Peanut 0.1 Bean, broccoli, Brussels sprouts, cab- bage, cauliflower, garlic, pepper, po- tato, and tomato

[71 FR 74816, Dec. 13, 2006]

§ 180.324 Bromoxynil; tolerances for Commodity Parts per residues. million (a) General. (1) Tolerances are estab- Alfalfa, seeding ...... 0.1 Barley, grain ...... 0 .1 lished for residues of the herbicide Barley, straw ...... 0 .1 bromoxynil (3,5-dibromo-4- Canarygrass, annual, hay ...... 0 .1 hydroxybenzonitrile) resulting from Canarygrass, annual, seed ...... 0.1 Corn, field, stover ...... 0 .1 application of its octanoic and/or Corn, fodder (green) ...... 0 .1 heptanoic acid ester in or on the fol- Corn, grain ...... 0 .1 Corn, grain, field ...... 0 .1 lowing commodities: Corn, stover ...... 0 .1

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Commodity Parts per § 180.325 2-(m-Chlorophenoxy) propi- million onic acid; tolerances for residues. Flax, seed ...... 0 .1 (a) General. A tolerance is established Flax, straw ...... 0 .1 for negligible residues of the plant reg- Garlic ...... 0 .1 ulator 2-(m-chlorophenoxy) propionic Mint hay ...... 0 .1 Oat, forage ...... 0 .1 acid from application of the acid or of Oat, grain ...... 0 .1 2-(m-chlorophenoxy)propionamide in or Oat, straw ...... 0.1 on the following raw agricultural com- Onion, dry bulb ...... 0 .1 modity: Rye, forage ...... 0 .1 Rye, grain ...... 0.1 Parts per Expiration/ Rye, straw ...... 0 .1 Commodity million Revocation Sorghum, forage ...... 0 .1 Date Sorghum, grain ...... 0 .1 Pineapple ...... 0.3 2/1/07 Sorghum, grain, stover ...... 0 .1 Wheat, forage ...... 0 .1 Wheat, grain ...... 0 .1 (b) Section 18 emergency exemptions. Wheat, straw ...... 0 .1 [Reserved] (c) Tolerances with regional registra- (2) Tolerances are established for res- tions. [Reserved] idues of the herbicide bromoxynil (3,5- (d) Indirect or inadvertent residues. dibromo-4-hydroxybenzonitrile) and its [Reserved] metabolite 3,5-dibromo-4- [69 FR 43924, July 23, 2004] hydroxybenzoic acid (DBHA) resulting from application of its octanoic and/or § 180.328 N,N-Diethyl-2-(1-naphthale- heptanoic acid ester in or on the fol- nyloxy)propionamide; tolerances lowing commodities: for residues.

Parts per (a) Tolerances are established for Commodity million negligible residues (N) of the herbicide N,N--Diethyl-2-(1-napthalenyloxy) Cattle, fat ...... 1 Cattle, meat byproducts ...... 3.5 propionamide in or on the following Cattle, meat ...... 0 .5 raw agricultural commodities: Cotton, gin byproducts ...... 7 .0 Cotton, hulls ...... 5 .0 Parts per Commodity million Cotton, undelinted seed ...... 1 .5 Egg ...... 0 .05 Almond, hulls ...... 0 .1(N) Goat, fat ...... 1 Artichoke, globe ...... 0.1 Goat, meat byproducts ...... 3 .5 Asparagus ...... 0.1 Goat, meat ...... 0.5 Avocado ...... 0 .1 Hog, fat ...... 1 Basil ...... 0.1 Hog, meat byproducts ...... 3 .5 Coffee, bean, green ...... 0 .1(N) Hog, meat ...... 0 .5 Fig ...... 0 .1(N) Horse, fat ...... 1 Fruit, citrus ...... 0 .1(N) Horse, meat byproducts ...... 3 .5 Fruit, pome ...... 0.1(N) Horse, meat ...... 0 .5 Fruit, small ...... 0 .1(N) Milk ...... 0.1 Fruit, stone ...... 0 .1(N) Kiwifruit ...... 0.1 Poultry, fat ...... 0.05 Marjoram ...... 0 .1 Poultry, meat byproducts ...... 0.3 Mint ...... 0 .1 Poultry, meat ...... 0 .05 Nut ...... 0 .1(N) Sheep, fat ...... 1 Olive ...... 0 .1 Sheep, meat byproducts ...... 3 .5 Persimmon ...... 0 .1 Sheep, meat ...... 0.5 Pistachio ...... 0.1 Rhubarb ...... 0 .1 (b) Section 18 emergency exemptions. Rosemary ...... 0 .1 Savory, Summer ...... 0 .1 [Reserved] Savory, winter ...... 0 .1 (c) Tolerances with regional registra- Sweet potato, roots ...... 0 .1 tions. [Reserved] Vegetable, brassica, leafy, group 5 ...... 0.1 Vegetable, cucurbit, group 9 ...... 0.1 (d) Indirect or inadvertent residues. Vegetable, fruiting ...... 0.1(N) [Reserved] [62 FR 33023, June 18, 1997, as amended at 63 (b) Tolerances with regional registra- FR 26480, May 13, 1998; 66 FR 47402, Sept. 12, tion are established for residues of the 2001; 70 FR 7046, Feb. 10, 2005; 72 FR 35666, herbicide N,N-diethyl-2-(1- June 29, 2007] naphthalenyloxy) propionamide in or

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on the following raw agricultural com- Commodity Parts per modities: million Melon ...... 0 .3 Parts per Commodity million Milk ...... 0.01 Mint, hay ...... 12.5 Pomegranate ...... 0 .1 Onion, dry bulb ...... 0 .05 Orange, sweet ...... 1 Pear ...... 0 .3 [42 FR 17443, Apr. 1, 1977, as amended at 45 Pepper ...... 0 .75 FR 64579, Sept. 30, 1980; 46 FR 39828, Aug. 5, Plum, prune, fresh ...... 1 1981; 46 FR 47548, Sept. 29, 1981; 47 FR 39490, Pumpkin ...... 0.3 Safflower, seed ...... 1 .0 Sept. 8, 1982; 48 FR 13175, Mar. 30, 1983; 48 FR Sheep, fat ...... 0 .01 46310, Oct. 12, 1983; 48 FR 50317, Nov. 1, 1983; Sheep, meat byproducts ...... 0 .01 48 FR 51487, Nov. 9, 1983; 50 FR 45113, Oct. 30, Sheep, meat ...... 0.01 1985; 58 FR 34914, June 30, 1993] Sorghum, forage ...... 2 .0 Sorghum, grain ...... 0 .75 § 180.330 S-[2-(Ethylsulfinyl)ethyl] O,O- Sorghum milled fractions (except flour) ...... 2 .0 Squash, summer ...... 1 dimethyl phosphorothioate; toler- Squash, winter ...... 0 .3 ances for residues. Strawberry ...... 2 (a) General. Tolerances are estab- Turnip ...... 0 .3 Turnip, greens ...... 2 lished for residues of the pesticide S-[2- Walnut ...... 0 .3 (ethylsulfinyl)-ethyl] O,O-dimethyl phosphorothioate and its cholin- (b) Section 18 emergency exemptions. esterase-inhibiting metabolites on the [Reserved] following raw agricultural commod- (c) Tolerances with regional registra- ities. tions. Tolerances with regional reg- istration, as defined in § 180.1(n), are es- Parts per Commodity million tablished for residues of S-[2-(ethyl-sul- finyl)ethyl] O,O-dimethyl Alfalfa, green ...... 5 phosphorothioate and its cholin- Alfalfa, hay, grown for seed ...... 11 Apple ...... 1 esterase-inhibiting metabolites in or Bean, lima ...... 0 .5 on the following raw agricultural com- Bean, lima, forage ...... 2 modities: Bean, snap, succulent ...... 0 .5 Bean, snap, forage ...... 2 Parts per Beet, sugar ...... 0 .3 Commodity million Beet, sugar, tops ...... 0.5 Broccoli ...... 1 Apricot ...... 0 .5 Brussels sprouts ...... 1 Cabbage ...... 1 Cattle, fat ...... 0.01 (d) Indirect or inadvertent residues. Cattle, meat byproducts ...... 0.01 [Reserved] Cattle, meat ...... 0 .01 Cauliflower ...... 1 [41 FR 28791, July 13, 1976; 41 FR 29681, July Clover, forage ...... 5 19, 1976, as amended at 41 FR 34629, Aug. 16, Clover, hay, grown for seed ...... 11 1976; 41 FR 41693, Sept. 23, 1976; 49 FR 4737, Clover, seed screenings ...... 11 Feb. 8, 1984; 52 FR 33238, Sept. 2, 1987; 62 FR Corn, forage ...... 3 66024, Dec. 17, 1997; 63 FR 57076, Oct. 26, 1998] Corn, grain ...... 0 .5 Corn, stover ...... 3 Corn, sweet, kernel plus cob with husks re- § 180.331 4-(2,4-Dichlorophenoxy) bu- moved ...... 0 .5 tyric acid; tolerances for residues. Cotton, undelinted seed ...... 0 .1 Tolerances are established for the Cucumber ...... 1 Eggplant ...... 1 combined residues of the herbicide 4- Filbert ...... 0 .05 (2,4-dichlorophenoxy) butyric acid and Goat, fat ...... 0 .01 its metabolite 2,4- Goat, meat byproducts ...... 0 .01 Goat, meat ...... 0.01 dichlorophenoxyacetic acid in or on the Grapefruit ...... 1 following raw agricultural commod- Grape ...... 0 .1 ities: Hog, fat ...... 0 .01 Hog, meat byproducts ...... 0 .01 Parts per Hog, meat ...... 0 .01 Commodity million Horse, fat ...... 0 .01 Horse, meat byproducts ...... 0 .01 Alfalfa ...... 0 .2(N) Horse, meat ...... 0 .01 Clover ...... 0 .2(N) Lemon ...... 1 Mint, hay ...... 0.2 Lettuce, head ...... 2 Peanut ...... 0 .2(N)

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Parts per Parts per Commodity million Commodity million

Soybean ...... 0.2(N) Sugarcane, molasses ...... 2 .0 Soybean, hay ...... 0 .2(N) Tomato ...... 0.1 Trefoil, birdsfoot ...... 0 .2(N) Wheat, bran ...... 3.0 Wheat, forage ...... 2 .0 Wheat, germ ...... 3 .0 [48 FR 19026, Apr. 27, 1983] Wheat, grain ...... 0 .75 Wheat, hay ...... 7 .0 § 180.332 Metribuzin; tolerances for Wheat, middlings ...... 3 .0 Wheat, shorts ...... 3 .0 residues. Wheat, straw ...... 1 .0 (a) General. Tolerances are estab- lished for combined residues of the her- (b) Section 18 emergency exemptions. bicide metribuzin (4-amino-6-(1,1- [Reserved] dimethyl- ethyl)-3-(methylthio)-;1,2,4- (c) Tolerances with regional registra- triazin-5(4H)-one) and its triazinone tions. [Reserved] metabolites in or on food commodities: (d) Indirect or inadvertent residues. [Reserved] Parts per Commodity million [42 FR 62913, Dec. 14, 1977, as amended at 43 FR 41396, Sept. 18, 1978; 44 FR 26744, May 7, Alfalfa, forage ...... 2.0 1979; 44 FR 45387, Aug. 2, 1979; 52 FR 23654, Alfalfa, hay ...... 7.0 Asparagus ...... 0.1 June 24, 1987; 55 FR 26440, June 28, 1990; 62 FR Barley, grain ...... 0 .75 66024, 66025, Dec. 17, 1997; 65 FR 33698, May 24, Barley, hay ...... 7 .0 2000; 66 FR 63198, Dec. 5, 2001; 67 FR 49617, Barley, pearled barley ...... 3 .0 July 31, 2002] Barley, straw ...... 1 .0 Carrot, roots ...... 0.3 § 180.337 Oxytetracycline; tolerance Cattle, fat ...... 0.7 Cattle, meat ...... 0 .7 for residues. Cattle, meat byproducts ...... 0.7 Tolerances are established for resi- Corn, field, forage ...... 0 .1 Corn, field, grain ...... 0 .05 dues of the pesticide oxytetracycline in Corn, field, stover ...... 0 .1 or on the following raw agricultural Corn, pop, grain ...... 0.05 commodities: Corn, sweet, forage ...... 0 .1 Corn, sweet, kernel plus cob with husks re- Parts per moved ...... 0 .05 Commodity million Corn, sweet, stover ...... 0 .1 Egg ...... 0 .01 Peach ...... 0 .35 Goat, fat ...... 0 .7 Pear ...... 0 .35 Goat, meat ...... 0.7 Goat, meat byproducts ...... 0 .7 Grass, forage ...... 2 .0 [60 FR 34871, July 5, 1995] Grass, hay ...... 7 .0 Hog, fat ...... 0 .7 § 180.339 MCPA; tolerances for resi- Hog, meat ...... 0 .7 dues. Hog, meat byproducts ...... 0 .7 Horse, fat ...... 0 .7 (a) General. (1) Tolerances are estab- Horse, meat ...... 0 .7 lished for residues of the herbicide Horse, meat byproducts ...... 0 .7 Lentil ...... 0.05 MCPA ((4-chloro-2- Milk ...... 0.05 methylphenoxy)acetic acid), both free Pea, dry, seed ...... 0 .05 and conjugated, resulting from the di- Pea, field, hay ...... 4.0 rect application of MCPA or its sodium Pea, field, vines ...... 0 .5 Pea, succulent ...... 0 .1 or dimethylamine salts, or its 2- Potato ...... 0 .6 ethylhexyl ester in or on the following Potato, chips ...... 3 .0 food commodities: Potato, processed potato waste ...... 3 .0 Poultry, fat ...... 0.7 Parts per Poultry, meat ...... 0 .7 Commodity million Poultry, meat byproducts ...... 0.7 Sainfoin, forage ...... 2 .0 Alfalfa, forage ...... 0.5 Sainfoin, hay ...... 7 .0 Alfalfa, hay ...... 2.0 Sheep, fat ...... 0 .7 Barley, grain ...... 1 .0 Sheep, meat ...... 0.7 Barley, hay ...... 40 Sheep, meat byproducts ...... 0 .7 Barley, straw ...... 25 Soybean, seed ...... 0 .3 Clover, forage ...... 0.5 Soybean, forage ...... 4 .0 Clover, hay ...... 2.0 Soybean, hay ...... 4 .0 Flax, seed ...... 0 .1 Sugarcane, cane ...... 0.1 Grass, forage ...... 300

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crotonate and 2,6-dinitro-4-octylphenyl Commodity Parts per million crotonate in or on raw agricultural Grass, hay ...... 20 commodities as follows: Lespedeza, forage ...... 0 .5 Lespedeza, hay ...... 2.0 Commodity Parts per Oat, forage ...... 20 million Oat, grain ...... 1 .0 1 Oat, hay ...... 115 Apple ...... 0 .1 Oat, straw ...... 25 Grape1 ...... 0 .1 Pea, dry ...... 0 .1 1There are no U.S. registrations on apple and grape as of Pea, field, hay ...... 0.1 October 24, 2002. Pea, succulent ...... 0 .1 Pea, field, vines ...... 0 .1 (b) Section 18 emergency exemptions. Rye, forage ...... 20 [Reserved] Rye, grain ...... 1.0 Rye, straw ...... 25 (c) Tolerances with regional registra- Trefoil, forage ...... 0 .5 tions. [Reserved] Trefoil, hay ...... 2 .0 (d) Indirect or inadvertent residues. Vetch, forage ...... 0 .5 Vetch, hay ...... 2 .0 [Reserved] Wheat, forage ...... 20 [40 FR 29715, July 15, 1975, as amended at 63 Wheat, grain ...... 1 .0 Wheat, hay ...... 115 FR 57076, Oct. 26, 1998; 69 FR 43924, July 23, Wheat, straw ...... 25 2004]

(2) Tolerances are established for res- § 180.342 Chlorpyrifos; tolerances for idues of the herbicide MCPA ((4-chloro- residues. 2-methylphenoxy)acetic acid) resulting (a) General. (1) Tolerances are estab- from the direct application of MCPA or lished for combined residues of the pes- its sodium or dimethylamine salts, or ticide chlorpyrifos (O,O-diethyl O- its 2-ethylhexyl ester in or on the fol- (3,5,6-trichloro-2-pyridyl) lowing food commodities: phosphorothioate and its metabolite 3,5,6-trichloro-2-pyridinol in or on the Parts per Commodity million following food commodities:

Cattle, fat ...... 0.1 Commodity Parts per Cattle, meat ...... 0 .1 million Cattle, meat byproducts ...... 0.1 Goat, fat ...... 0 .1 Almond ...... 0.2 Goat, meat ...... 0.1 Almond, hulls ...... 12 .0 Goat, meat byproducts ...... 0 .1 Apple ...... 1.5 Hog, fat ...... 0 .1 Bean, lima ...... 0 .05 Hog, meat ...... 0 .1 Bean, snap, succulent ...... 0 .05 Hog, meat byproducts ...... 0 .1 Beet, sugar, molasses ...... 15 .0 Horse, fat ...... 0 .1 Beet, sugar, dried pulp ...... 5 .0 Horse, meat ...... 0 .1 Beet, sugar, roots ...... 1 .0 Horse, meat byproducts ...... 0 .1 Beet, sugar, tops ...... 8.0 Milk ...... 0.1 Blueberry ...... 2 ppm Sheep, fat ...... 0 .1 (of which no more than 1 ppm is chlorpyrifos) Sheep meat ...... 0 .1 Citrus, dried pulp ...... 5 .0 Sheep meat byproducts ...... 0 .1 Citrus, oil ...... 25.0 Corn, field, refined oil ...... 3 .0 (b) Section 18 emergency exemptions. Corn, sweet, kernel plus cob with husks re- moved ...... 0 .1 [Reserved] Cranberry ...... 1 .0 (c) Tolerances with regional registra- Fruit, citrus ...... 1 .0 tions. [Reserved] Kiwifruit ...... 2.0 Nut, tree, group 14 ...... 0 .2 (d) Indirect or inadvertent residues. Onion, dry bulb ...... 0 .5 [Reserved] Pepper ...... 1 .0 Sorghum, forage ...... 1 .5 [72 FR 28888, May 23, 2007] Sorghum, grain, grain ...... 0 .75 Sorghum, grain, stover ...... 6 .0 § 180.341 2,4-Dinitro-6-octylphenyl cro- Sunflower, seed ...... 0.25 tonate and 2,6-dinitro-4-octylphenyl Tomato ...... 0.5 crotonate; tolerances for residues. Vegetable, brassica, leafy, group 5 ...... 12.0 Walnut ...... 0 .2 (a) General. Tolerances are estab- 1 lished for combined negligible residues Of which no more than 1.0 ppm is chlorpyrifos. of a fungicide and insecticide that is a (2) Tolerances are established for res- mixture of 2,4-dinitro-6-octylphenyl idues of the pesticide chlorpyrifos

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(O,O-diethyl O-(3,5,6-trichloro-2-pyr- (ii) Spray concentration for spot idyl) phosphorothioate in or on the fol- treatment shall be limited to a max- lowing food commodities: imum of 0.5 percent of the active ingre- dient by weight. A course, low-pressure Parts per Commodity million spray shall be used to avoid atomiza- tion or splashing of the spray. Alfalfa, forage ...... 3 (iii) Paint-on application for spot Alfalfa, hay ...... 13 Banana ...... 0.1 treatment shall be limited to a max- Banana, pulp ...... 0 .01 imum of 2 percent of the active ingre- Broccoli ...... 1 dient by weight. Brussels sprouts ...... 1 Cabbage ...... 1 (iv) Crack and crevice treatment Cabbage, chinese ...... 1 shall be limited to a maximum of 2 per- Cattle, fat ...... 0.3 cent of the active ingredient by weight. Cattle, meat and meat byproducts ...... 0.05 Equipment capable of delivering a pin- Cauliflower ...... 1 Cherry ...... 1 stream of insecticide shall be used. Corn, field, grain ...... 0 .05 (v) Application via adhesive strips Corn, forage and fodder ...... 8 shall contain a maximum of 10% by Cotton, undelinted seed ...... 0 .2 Cucumber ...... 0 .05 weight of the controlled-release prod- Egg ...... 0 .01 uct in food-handling establishments Fig ...... 0 .01 where food and food products are held, Goat, fat ...... 0 .2 Goat, meat and meat byproducts ...... 0 .05 processed, prepared, or served. A max- Hog, fat ...... 0 .2 imum of 36 strips (or 5.15 grams of Hog, meat and meat byproducts ...... 0 .05 chlorpyrifos) is to be used per 100 Horse, meat, fat, and meat byproducts ...... 0 .25 Legume vegetables, succulent or dried (except square feet of floor space. The strips soybean) ...... 0 .05 are not to be placed in exposed areas Milk, fat ...... 0 .25 where direct contact with food, uten- Milk, whole ...... 0 .01 sils, and food-contact surfaces would be Milling fractions (except flour) of wheat ...... 1 .5 Mint, hay ...... 0.8 likely to occur. Mint oil ...... 8 (vi) To assure safe use of the insecti- Nectarine ...... 0 .05 cide, its label and labeling shall con- Peach ...... 0 .05 Peanut oil ...... 0.4 form to that registered by the U.S. En- Peanut ...... 0 .2 vironmental Protection Agency, and it Pear ...... 0 .05 shall be used in accordance with such Plum ...... 0 .05 label and labeling. Poultry, meat, fat, and meat byproducts (inc. tur- keys) ...... 0 .1 (4) A tolerance of 0.1 part per million Pumpkin ...... 0.05 is established for residues of Radish ...... 2 chlorpyrifos, per se, in or on food com- Rutabagas ...... 0 .5 Sheep, fat ...... 0 .2 modities (other than those already cov- Sheep, meat and meat byproducts ...... 0 .05 ered by a higher tolerance as a result Soybean, forage ...... 0 .7 of use on growing crops) in food service Soybean, seed ...... 0 .3 establishments where food and food Strawberry ...... 0 .2 Sweet potato, roots ...... 0 .05 products are prepared and served, as a Turnip, greens ...... 0.3 result of the application of chlorpyrifos Turnip ...... 1 in microencapsulated form. Wheat, grain ...... 0 .5 Wheat, straw ...... 6 (i) Application of a microencap- Wheat, forage ...... 3 sulated product shall be limited solely to spot and/or crack and crevice treat- (3) Chlorpyrifos [O,O-diethyl O-(3,5,6- ment in food handling establishments trichloro-2-pyridyl) phosphorothioate] where food and food products are pre- may be safely used in accordance with pared and served. All treatments shall the following prescribed conditions. be applied in such a manner as to avoid (i) Application shall be limited solely contamination of food or food contact to spot and/or crack and crevice treat- surfaces. ment in food handling establishments (ii) Spray concentrations shall be where food and food products are held, limited to a maximum of 0.5 percent of processed, prepared or served. Contami- the active ingredient by weight. nation of food or food contact surfaces (iii) For crack and crevice treatment, shall be avoided. Food must be re- equipment capable of delivering a pin moved or covered during treatment. stream of spray directly into cracks

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and crevices or capable of applying or on the following raw agricultural small amounts of insecticide into commodities: cracks and crevices shall be used. Parts per (iv) For spot treatment, an individual Commodity million spot shall not exceed 2 square feet. (v) To assure safe use of the insecti- Beet, garden, roots ...... 0 .5 Beet, garden, tops ...... 4 .0 cide, its label and labeling shall con- Beet, sugar, roots ...... 0 .1 form to that registered by the U.S. En- Beet, sugar, tops ...... 1.00 vironmental Protection Agency, and it Cattle, fat ...... 0.05 Cattle, meat byproducts ...... 0.05 shall be used in accordance with such Cattle, meat ...... 0 .05 label and labeling. Garlic, bulb ...... 0.25 (b) Section 18 emergency exemptions. Goat, fat ...... 0 .05 Goat, meat byproducts ...... 0 .05 [Reserved] Goat, meat ...... 0.05 (c) Tolerances with regional registra- Grass, straw ...... 1 tions. (1) Tolerances with regional reg- Hog, fat ...... 0 .05 Hog, meat byproducts ...... 0 .05 istration, as defined in § 180.1(n), are es- Hog, meat ...... 0 .05 tablished for the combined residues of Horse, fat ...... 0 .05 chlorpyrifos and its metabolite 3,5,6- Horse, meat byproducts ...... 0 .05 trichloro-2-pyridinol in or on the fol- Horse, meat ...... 0 .05 Onion, bulb ...... 0 .25 lowing food commodities: Shallot, bulb ...... 0 .25 Shallot, fresh leaves ...... 0 .25 Commodity Parts per Sheep, fat ...... 0 .05 million Sheep, meat byproducts ...... 0 .05 Sheep, meat ...... 0.05 Asparagus ...... 5.0 Grape ...... 0 .5 Leek (of which no more than 0.2 ppm is (2) Tolerances are established for chlorpyrifos) ...... 0 .5 combined residues of the herbicide ethofumesate (2-ethoxy-2,3-dihydro-3,3- (2) Tolerances with regional registra- dimethyl-5-benzofuranyl tion, as defined in § 180.1(n), are estab- methanesulfonate; CAS Reg. No. 26225– lished for residues of the pesticide 79–6) and its metabolites 2-hydroxy-2,3- chlorpyrifos (O,O-diethyl O-(3,5,6- dihydro-3,3-dimethyl-5-benzofuranyl trichloro-2-pyridyl)phosphorothioate) methanesulfonate and 2,3-dihydro-3,3- in or on the following food commod- dimethyl-2-oxo-5-benzofuranyl ities: methanesulfonate, (both calculated as the parent compound) in or on the fol- Parts per Commodity million lowing processed feeds when present therein as a result of application of the Cherimoya ...... 0 .05 herbicide to the growing crops: Feijoa (pineapple guava) ...... 0 .05 Sapote ...... 0 .05 Parts per Commodity million (d) Indirect or inadvertent residues. Sugar beet molasses ...... 0 .5 [Reserved] [65 FR 33711, May 24, 2000, as amended at 67 (b) Section 18 emergency exemptions. FR 49617, July 31, 2002; 71 FR 74817, Dec. 13, [Reserved] 2006] (c) Tolerances with regional registra- tion. Tolerances with regional registra- § 180.345 Ethofumesate; tolerances for tion as defined in 40 CFR 180.1(m) are residues. established for the combined residues (a) General. (1) Tolerances are estab- of ethofumesate,(2-ethoxy -2, 3-dihydro- lished for combined residues of the her- 3, 3-dimethyl-5-benzofuranyl bicide ethofumesate (2-ethoxy-2,3- methanesulfonate) and its metabolites dihydro-3,3-dimethyl-5-benzofuranyl 2-hydroxy-2,3-dihydro-3,3-dimethyl-5- methanesulfonate) and its metabolites benzofuranyl methanesulfonate and 2,3- 2-hydroxy-2,3-dihydro-3,3-dimethyl-5- dihydro-3,3-dimethyl-2-oxo-5- benzofuranyl methanesulfonate and 2,3- benzofuranyl methanesulfonate (both dihydro-3,3-dimethyl-2-oxo-5- calculated as the parent compound) in benzofuranyl methanesulfonate (both or on the raw agricultural commod- calculated as the parent compound) in ities:

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phosphoramidate, ethyl-4- Commodity Parts per million (methylsulfinyl)phenyl Carrot, roots ...... 7.0 phosphoramidate, and ethyl 3-methyl- 4-(methyl-sulfonyl)phenyl (d) Indirect or inadvertent residues. phosphoramidate in or on the following [Reserved] raw agricultural meat commodities: [63 FR 34828, June 26, 1998, as amended at 71 Commodity Parts per FR 51516, Aug. 30, 2006] million Cattle, fat ...... 0.05 § 180.349 Fenamiphos; tolerances for Cattle, meat ...... 0 .05 residues. Cattle, meat byproducts ...... 0.05 (a) General. (1) Tolerances are estab- Goat, fat ...... 0 .05 Goat, meat ...... 0.05 lished for the combined residues of the Goat, meat byproducts ...... 0 .05 nematocide Fenamiphos (ethyl 3-meth- Hog, fat ...... 0 .05 yl-4-(methylthio)phenyl (1- Hog, meat ...... 0 .05 Hog, meat byproducts ...... 0 .05 methylethyl) phosphoramidate) and its Horse, fat ...... 0 .05 cholinesterase inhibiting metabolites Horse, meat ...... 0 .05 ethyl 3-methyl-4- Horse, meat byproducts ...... 0 .05 Milk ...... 0.01 (methylsulfinyl)phenyl (1- Sheep, fat ...... 0 .05 methylethyl)phosphoramidate and Sheep, meat ...... 0.05 ethyl 3-methyl-4- Sheep, meat byproducts ...... 0 .05 (methylsulfonyl)phenyl (1- methylethyl) phosphoramidate in or on (b) Section 18 emergency exemptions. the following food commodities: [Reserved] (c) Tolerances with regional registra- Commodity Parts per tions. Tolerances with regional reg- million istration, as defined in § 180.1(n), are es- Apple ...... 0.25 tablished for the combined residues of Banana ...... 0.10 Fenamiphos (ethyl 3-methyl-4- Brussels sprouts ...... 0 .10 (methylthio)phenyl (1-methylethyl) Cabbage ...... 0 .10 Cherry ...... 0.25 phosphoramidate) and its cholin- Citrus, oil ...... 25.0 esterase-inhibiting metabolites ethyl 3- Citrus, dried pulp ...... 2 .5 methyl-4-(methylsulfinyl)phenyl (1- Cotton, undelinted seed ...... 0 .05 Eggplant ...... 0.1 methylethyl) phosphoramidate and Garlic ...... 0 .50 ethyl 3-methyl-4- Grapefruit ...... 0 .60 (methylsulfonyl)phenyl (1- Grape ...... 0 .10 methylethyl) phosphoramidate in or on Grape, raisins ...... 0 .3 Lemon ...... 0.60 the following raw agricultural com- Lime ...... 0.60 modities: Okra ...... 0.30 Orange, sweet ...... 0 .60 Commodity Parts per Peach ...... 0 .25 million Peanut ...... 0 .02 Pineapple ...... 0.30 Asparagus ...... 0.02 Pineapple, bran ...... 10.0 Beet, garden, roots ...... 1 .5 Raspberry ...... 0 .1 Beet, garden, tops ...... 1 .0 Strawberry ...... 0 .6 Bok choy ...... 0 .5 Tangerine ...... 0 .60 Kiwifruit ...... 0.1 Pepper, nonbell ...... 0 .6 (2) Tolerances are established for the combined residues of the nematocide (d) Indirect or inadvertent residues. Fenamiphos (ethyl 3-methyl-4- [Reserved] (methylthio)phenyl (1- [65 FR 33712, May 24, 2000] methylethyl)phosphoramidate) and its cholinesterase-inhibiting metabolites § 180.350 Nitrapyrin; tolerances ethyl 3-methyl-4- for residues. (methylsulfinyl)phenyl (1- (a) General. Tolerances are estab- methylethyl)phosphoramidate, ethyl 3- lished for the combined residues of the methyl-4-(methylsulfonyl)phenyl (1- soil microbiocide nitrapyrin [2-chloro- methylethyl)phosphoramidate, ethyl 3- 6-(trichloromethyl) ] and its methyl-4-(methylthio)phenyl metabolite, 6-chloropicolinic acid in or

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on the following raw agricultural com- Commodity Parts per modities: million Corn, sweet, forage ...... 0 .5 Parts per Commodity million Corn, sweet, stover ...... 0 .5 Sorghum, forage ...... 0 .5 Cattle, fat ...... 0.05(N) Sorghum, grain ...... 0 .05 Cattle, meat byproducts ...... 0.05(N) Sorghum, grain, stover ...... 0 .5 Cattle, meat ...... 0 .05(N) Corn, forage ...... 1 .0 Corn, grain ...... 0 .1(N) (b) A time-limited tolerance to expire Corn, stover ...... 1 .0 December 15, 1997 is established for Corn, sweet, kernel plus cob with husks re- combined residues of the insecticide/ moved ...... 0 .1(N) Goat, fat ...... 0 .05(N) nematicide terbufos (S-[[1,1-di- Goat, meat byproducts ...... 0 .05(N) methyl)thio] methyl] O,O-diethyl Goat, meat ...... 0.05(N) Hog, fat ...... 0 .05(N) phosphorodithioate) and its cholin- Hog, meat byproducts ...... 0 .05(N) esterase-inhibiting metabolites in or Hog, meat ...... 0 .05(N) on the following raw agricultural com- Horse, fat ...... 0 .05(N) Horse, meat byproducts ...... 0 .05(N) modity: Horse, meat ...... 0 .05(N) Poultry, fat ...... 0.05(N) Commodity Parts per Poultry, meat byproducts ...... 0.05(N) million Poultry, meat ...... 0 .05(N) Sheep, fat ...... 0 .05(N) Coffee bean, green1 ...... 0 .05 Sheep, meat byproducts ...... 0 .05(N) 1There are no U.S. registrations as of August 2, 1995, for Sheep, meat ...... 0.05(N) the use of terbufos on the growing crop, coffee. Sorghum, forage ...... 0 .1(N) Sorghum, grain ...... 0 .1(N) Sorghum, grain, stover ...... 0 .5 [41 FR 16462, Apr. 19, 1976, as amended at 45 Wheat, forage ...... 0 .5 FR 8012, Feb. 6, 1980; 47 FR 17059, Apr. 21, Wheat, grain ...... 0 .1(N) 1982; 53 FR 15041, Apr. 27, 1988; 54 FR 48745, Wheat, straw ...... 0 .5 Nov. 27, 1989; 58 FR 29119, May 19, 1993; 58 FR 30220, May 26, 1993; 60 FR 63954, Dec. 13, 1995] (b) Section 18 emergency exemptions. [Reserved] § 180.353 Desmedipham; tolerances for (c) Tolerances with regional registra- residues. tions. [Reserved] (d) Indirect or inadvertent residues. (a) General. A tolerance of 0.2 part per [Reserved] million is established for negligible residues of the herbicide desmedipham [46 FR 58315, Dec. 1, 1981, as amended at 47 (ethyl-m-hydroxycarbanilate FR 22957, May 26, 1982; 52 FR 33238, Sept. 2, carbanilate) in or on the raw agricul- 1987; 58 FR 32304, June 9, 1993; 63 FR 57076, Oct. 26, 1998] tural commodity sugar beet (roots and tops). § 180.352 Terbufos; tolerances for resi- (b) Section 18 emergency exemptions. dues. Time-limited tolerances are estab- (a) Tolerances are established for lished for residues of the herbicide combined residues of the insecticide desmedipham in connection with use of terbufos (S-[[1,1-dimethyl)thio]methyl] the pesticide under section 18 emer- O,O-diethyl phosphorodithioate and its gency exemptions granted by EPA. The cholinesterase-inhibiting metabolites tolerances will expire and are revoked in or on the following raw agricultural on the date specified in the following commodities. table:

Commodity Parts per Expiration/ million Commodity Parts per Revocation million Date Banana ...... 0.025 Beet, sugar, roots ...... 0 .05(N) Red beet roots ...... 0.2 6/30/08 Beet, sugar, tops ...... 0.1 Red beet tops ...... 15 6/30/08 Corn, field, forage ...... 0 .5 Corn, field, stover ...... 0 .5 Corn, pop, forage ...... 0 .5 (c) Tolerances with regional registra- Corn, pop, stover ...... 0.5 tions. [Reserved] Corn, grain ...... 0 .05(N) Corn, sweet, kernel plus cob with husks re- moved ...... 0 .05(N)

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(d) Indirect or inadvertent residues. Commodity Parts per [Reserved] million [40 FR 4658, Jan. 31, 1975, as amended at 62 Hog, meat byproducts ...... 0 .05 FR 45747, Aug. 29, 1997; 63 FR 49472, Sept. 16, Hog, meat ...... 0 .05 Milk ...... 0.02 1998; 64 FR 46292, Aug. 25, 1999; 65 FR 82293, Poultry, fat ...... 0.05 Dec. 28, 2000; 66 FR 64773, Dec. 14, 2001; 68 FR Poultry, meat byproducts ...... 0.05 37764, June 25, 2003; 69 FR 71717, Dec. 10, 2004] Poultry, meat ...... 0 .05 Sheep, fat ...... 0 .05 § 180.355 Bentazon; tolerances for resi- Sheep, meat byproducts ...... 0 .05 dues. Sheep, meat ...... 0.05 (a) General. (1) Tolerances are estab- (b) Section 18 emergency exemptions. lished for the combined residues of the [Reserved] herbicide bentazon (3-isopropyl-1H- (c) Tolerances with regional registra- 2,1,3-benzothiadiazin-4(3H)-one-2,2-diox- tions. Tolerances with regional reg- ide) and its 6- and 8-hydroxy metabo- istration as defined in § 180.1(n), are es- lites in or on the following food com- tablished for combined residues of the modities: herbicide, bentazon (3-isopropyl-1H-2, 1,3-benzothiadiazin-4(3H)-one-2,2-diox- Parts per Commodity million ide) and its 6- and 8-hydroxy metabo- lites in or on the following food com- Bean, dry, seed ...... 0 .05 modities: Bean, succulent ...... 0 .5 Corn, field, forage ...... 3 .0 Parts per Corn, field, grain ...... 0 .05 Commodity million Corn, field, stover ...... 3 .0 Corn, pop, grain ...... 0.05 Clover, forage ...... 1.0 Corn, sweet, kernel plus cob with husks re- Clover, hay ...... 2.0 moved ...... 0 .05 Cowpea, forage ...... 10 .0 Cowpea, hay ...... 3 .0 (d) Indirect or inadvertent residues. Flax, seed ...... 1 .0 [Reserved] Pea, dry, seed ...... 1 .0 Pea, field, hay ...... 8.0 [42 FR 26979, May 26, 1977; as amended at 42 Pea, field, vines ...... 3 .0 FR 39978, Aug. 8, 1977; 43 FR 14020, Apr. 4, Pea, succulent ...... 3 .0 1978; 43 FR 35698, Aug. 11, 1978; 43 FR 44844, Peanut ...... 0 .05 Sept. 29, 1978; 44 FR 37919, June 29, 1979; 46 FR Peanut, hay ...... 3.0 Pepper, nonbell ...... 0 .05 32441, June 23, 1981; 49 FR 11836, Mar. 28, 1984; Peppermint, tops ...... 1 .0 62 FR 33569, June 20, 1997; 63 FR 25777, May Rice, grain ...... 0 .05 11, 1998; 64 FR 37863, July 14, 1999; 64 FR 39083, Rice, hulls ...... 0 .25 July 21, 1999; 65 FR 12129, Mar. 8, 2000; 66 FR Rice, straw ...... 3 .0 48011, Sept. 17, 2001; 67 FR 5749, Feb. 7, 2002; Sorghum, forage ...... 0 .20 67 FR 35048, May 17, 2002; 71 FR 56383, Sept. Sorghum, grain ...... 0 .05 27, 2006] Sorghum, grain, stover ...... 0 .05 Soybean, forage ...... 8 .0 Soybean, hay ...... 8 .0 § 180.356 Norflurazon; tolerances for Soybean, seed ...... 0 .05 residues. Spearmint, tops ...... 1 .0 (a) General. Tolerances are estab- (2) Tolerances are established for the lished for the combined residues of the combined residues of the herbicide herbicide norflurazon (4-chloro-5- bentazon (3-isopropyl-1H-2,1,3- (methylamino)-2-(alpha, alpha, alpha- benzothiadiazin-4(3H)-one-2,2-dioxide) trifluoro-m-tolyl)-3-(2H)-pyridazinone) and its metabolite 2-amino-N-isopropyl and its desmethyl metabolite 4-chloro- benzamide (AIBA) in or on the fol- 5-(amino)-2-alpha, alpha, alpha- lowing food commodities: trifluoro-m-tolyl)-3(2H)-pyridazinone in or on the following raw agricultural Parts per commodities: Commodity million Parts per Cattle, fat ...... 0.05 Commodity million Cattle, meat byproducts ...... 0.05 Cattle, meat ...... 0 .05 Alfalfa, forage ...... 3.0 Egg ...... 0 .05 Alfalfa, hay ...... 5.0 Goat, fat ...... 0 .05 Alfalfa, seed ...... 0 .1 Goat, meat byproducts ...... 0 .05 Almond, hulls ...... 1 .0 Goat, meat ...... 0.05 Almond ...... 0.1 Hog, fat ...... 0 .05 Apple ...... 0.1

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Commodity Parts per § 180.360 Asulam; tolerance for resi- million dues. Apricot ...... 0 .1 (a) General. A tolerance is established Asparagus ...... 0.05 for residues of the herbicide asulam Avocado ...... 0 .20 (methyl sulfanilylcarbamate) in or on Blackberry ...... 0 .1 Blueberry ...... 0 .2 the following food commodity: Cattle, fat ...... 0.1 Cattle, liver ...... 0 .25 Parts per Commodity million Cattle, meat ...... 0 .1 Cattle, mbyb, except liver ...... 0 .1 Sugarcane, cane ...... 0.1(N) Cherry ...... 0.1 Citrus, dried pulp ...... 0 .4 (b) Section 18 emergency exemptions. Citrus, molasses ...... 1.0 Cotton, undelinted seed ...... 0 .1 [Reserved] Cranberry ...... 0 .1 (c) Tolerances with regional registra- Filbert ...... 0 .1 tions. [Reserved] Fruit, citrus ...... 0 .2 (d) Indirect or inadvertent residues. Goat, fat ...... 0 .1 [Reserved] Goat, liver ...... 0.25 Goat, meat ...... 0.1 [68 FR 39441, July 1, 2003] Goat, mbyb, except liver ...... 0 .1 Grape ...... 0 .1 § 180.361 Pendimethalin; tolerances for Hog, fat ...... 0 .1 residues. Hog, liver ...... 0 .25 Hog, meat ...... 0 .1 (a) General. Tolerances are estab- Hog, mbyb, except liver ...... 0 .1 lished for the combined residues of the Hop, dried cones ...... 3 .0 herbicide pendimethalin [N-(1- Hop, vines ...... 1 .0 ethylpropyl)-3,4-dimethyl-2,6- Horse, fat ...... 0 .1 Horse, liver ...... 0 .25 dinitrobenzenamine] and its metabolite Horse, meat ...... 0 .1 4-[(1-ethylpropyl)amino]-2-methyl-3,5- Horse, mbyb, except liver ...... 0 .1 dinitrobenzyl alcohol in or on the fol- Milk ...... 0.1 lowing raw agricultural commodities: Nectarine ...... 0 .1 Pecan ...... 0 .1 Commodity Parts per Peach ...... 0 .1 million Peanut ...... 0 .05 Peanut, hay ...... 5.50 Alfalfa, Forage ...... 3 .0 Alfalfa, Hay ...... 4 .0 Peanut, hay ...... 1.5 Alfalfa, Seed ...... 0.10 Pear ...... 0 .1 Almond, hulls ...... 0 .4 Plum, prune, fresh ...... 0.1 Apple, wet pomace ...... 0 .20 Poultry, fat ...... 0.1 Bean, lima, seed ...... 0 .1 Poultry, meat ...... 0 .1 Bean, lima, succulent ...... 0 .1 Poultry, meat byproducts ...... 0.1 Bean, forage ...... 0 .1 Raspberry ...... 0 .2 Bean, hay ...... 0 .1 Sheep, fat ...... 0 .1 Carrots ...... 0 .5 Sheep, liver ...... 0.25 Citrus, oil ...... 0.5 Sheep, meat ...... 0.1 Corn, field, forage ...... 0 .1 Sheep, mbyb, except liver ...... 0 .1 Corn, field, grain ...... 0 .1 Soybean ...... 0.1 Corn, field, stover ...... 0 .1 Soybean, forage ...... 1 .0 Corn, pop, grain ...... 0.1 Soybean, hay ...... 1 .0 Corn, sweet, forage ...... 0 .1 Corn, sweet, kernel plus cob with husks re- Walnut ...... 0 .1 moved ...... 0 .1 Corn, sweet, stover ...... 0 .1 (b) Section 18 emergency exemptions. Cotton, undelinted seed ...... 0 .1 [Reserved] Fruit, citrus, group 10 ...... 0 .1 Fruit, pome, group 11 ...... 0.10 (c) Tolerances with regional registra- Fruit, stone, group 12 ...... 0 .10 tion. [Reserved] Garlic ...... 0 .1 (d) Indirect or inadvertent residues. Juneberry ...... 0 .10 Leek ...... 0 .20 [Reserved] Nut, tree, group 14 ...... 0 .1 Onion, dry bulb ...... 0 .1 [47 FR 14909, Apr. 7, 1982] Onion, green ...... 0 .20 EDITORIAL NOTE: For FEDERAL REGISTER ci- Onion, welsh ...... 0.20 tations affecting § 180.356, see the List of CFR Pea, succulent ...... 0 .1 Peanut ...... 0 .1 Sections Affected, which appears in the Peanut, hay ...... 0.1 Finding Aids section of the printed volume Peppermint, oil ...... 1 .0 and on GPO Access. Peppermint, tops ...... 0 .2

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insecticide hexakis[2-methyl-2- Commodity Parts per million phenylpropyl] distannoxane and its Pistachio ...... 0.1 organotin metabolites calculated as Pomegranate ...... 0 .10 hexakis[2-methyl-2-phenylpropyl] Potato ...... 0 .1 distannoxane in or on the following Rice, grain ...... 0 .1 Rice, straw ...... 0 .1 food commodities: Shallot ...... 0.2 Sorghum, forage ...... 0 .1 Commodity Parts per Sorghum, grain, grain ...... 0 .1 million Sorghum, grain, stover ...... 0 .1 Soybean, forage ...... 0 .1 Almond ...... 0.5 Soybean, hay ...... 0 .1 Almond, hulls ...... 80 .0 Soybean, seed ...... 0 .1 Apple ...... 15.0 Spearmint, oil ...... 1 .0 Cattle, fat ...... 0.5 Spearmint, tops ...... 0 .2 Cattle, meat byproducts ...... 0.5 Strawberry ...... 0 .10 Cattle, meat ...... 0 .5 Sugarcane, cane ...... 0.1 Cherry, sweet ...... 6 .0 Sunflower, seed ...... 0.1 Cherry, tart ...... 6 .0 Vegetable, fruiting, group 8 ...... 0.10 Citrus, oil ...... 140.0 Wheat, grain ...... 0 .10 Wheat, forage ...... 3 .0 Citrus, dried pulp ...... 100.0 Wheat, hay ...... 0 .60 Cucumber ...... 4 .0 Wheat, straw ...... 0 .30 Eggplant ...... 6.0 Egg ...... 0 .1 (b) Section 18 emergency exemptions. Fruit, citrus ...... 20 .0 Goat, fat ...... 0 .5 Time-limited tolerances are estab- Goat, meat byproducts ...... 0 .5 lished for residues of the herbicide Goat, meat ...... 0.5 pendimethalin in connection with use Grape ...... 5 .0 of the pesticide under section 18 emer- Grape, raisin ...... 20.0 gency exemptions granted by EPA. The Hog, fat ...... 0 .5 Hog, meat byproducts ...... 0 .5 tolerances will expire and are revoked Hog, meat ...... 0 .5 on the dates specified in the following Horse, fat ...... 0 .5 table: Horse, meat byproducts ...... 0 .5 Horse, meat ...... 0 .5 Milk, fat ...... 0 .1 Parts per Expiration/ Commodity million Revocation Papaya ...... 2 .0 Date Pecan ...... 0 .5 Peach ...... 10 .0 Mint hay, fresh ...... 0.1 6/30/05 Mint oil ...... 5.0 6/30/05 Pear ...... 15 .0 Plum ...... 4 .0 Plum, prune ...... 4 .0 (c) Tolerances with regional registra- Plum, prune, dried ...... 20.0 tions. [Reserved] Poultry, fat ...... 0.1 (d) Indirect or inadvertent residues. Poultry, meat byproducts ...... 0.1 [Reserved] Poultry, meat ...... 0 .1 Sheep, fat ...... 0 .5 [49 FR 15293, Apr. 18, 1984, as amended at 53 Sheep, meat byproducts ...... 0 .5 FR 3024, Feb. 3, 1988; 54 FR 13688, Apr. 5, 1989; Sheep, meat ...... 0.5 55 FR 26440, June 28, 1990; 58 FR 11379, Feb. Strawberry ...... 10.0 25, 1993; 58 FR 33772, June 21, 1993; 60 FR Walnut ...... 0 .5 48660, Sept. 20, 1995; 62 FR 28361, May 23, 1997; 63 FR 10547, Mar. 4, 1998; 64 FR 13088, Mar. 17, (b) Section 18 emergency exemptions. 1999; 65 FR 44696, July 19, 2000; 66 FR 11112, [Reserved] Feb. 22, 2001; 66 FR 63199, Dec. 5, 2001; 67 FR (c) Tolerances with regional registra- 46883, July 17, 2002; 71 FR 18635, Apr. 12, 2006; tions. Tolerances with regional reg- 71 FR 32849, June 7, 2006; 71 FR 56374, Sept. 27, istration are established for residues of 2006] the insecticide hexakis [2-methyl-2- EDITORIAL NOTE: At 72 FR 27460, May 16, phenylpropyl] distannoxane and its 2007, § 180.361 was amended; however, the organotin metabolites calculated as amendment could not be incorporated due to hexakis [2-methyl-2-phenylpropyl] inaccurate amendatory instruction. distannoxane in or on the food com- § 180.362 Hexakis (2-methyl-2-phenyl- modities: propyl)distannoxane; tolerances for Parts per residues. Commodity million (a) General. Tolerances are estab- lished for the combined residues of the Raspberry ...... 10 .0

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(d) Indirect or inadvertent residues. Commodity Parts per [Reserved] million [65 FR 33713, May 24, 2000] Flax, meal ...... 8 .0 Flax, seed ...... 4 .0 Fruit, citrus, group 10 ...... 0 .5 § 180.364 Glyphosate; tolerances for Fruit, pome, group 11 ...... 0.2 residues. Fruit, stone, group 12 ...... 0 .2 (a) General. Tolerances are estab- Galangal, root ...... 0 .2 Ginger, white, flower ...... 0 .2 lished for residues of glyphosate N- Goat, kidney ...... 4 .0 (phosphonomethyl)glycine resulting Goat, liver ...... 0.5 from the application of glyphosate, the Gourd, buffalo, seed ...... 0 .1 Governor’s plum ...... 0 .2 isopropylamine salt of glyphosate, the Gow kee, leaves ...... 0 .2 ethanolamine salt of glyphosate, the Grain, aspirated fractions ...... 100 dimethylamine salt of glyphosate, the Grain, cereal, forage, fodder and straw, group 16, except corn forage ...... 100 ammonium salt of glyphosate, and the Grain, cereal, group 15, except barley, field potassium salt of glyphosate in or on corn, grain sorghum, oat and wheat ...... 0.1 the following food commodities: Grape ...... 0 .2 Grass, forage, fodder and hay, group 17 ...... 300 Parts per Guava ...... 0 .2 Commodity million Herbs subgroup 19A ...... 0 .2 Hog, kidney ...... 4.0 Acerola ...... 0.2 Hog, liver ...... 0 .5 Alfalfa, seed ...... 0 .5 Hop, dried cones ...... 7 .0 Almond, hulls ...... 25 Horse, kidney ...... 4 .0 Aloe vera ...... 0 .5 Horse, liver ...... 0 .5 Ambarella ...... 0 .2 Ilama ...... 0 .2 Animal feed, nongrass, group 18 ...... 400 Imbe ...... 0 .2 Artichoke, globe ...... 0.2 Imbu ...... 0 .2 Asparagus ...... 0.5 Jackfruit ...... 0 .2 Atemoya ...... 0 .2 Jaboticaba ...... 0 .2 Avocado ...... 0 .2 Jojoba, seed ...... 0.1 Bamboo, shoots ...... 0 .2 Juneberry ...... 0 .2 Banana ...... 0.2 Kava, roots ...... 0 .2 Barley, bran ...... 30 Kenaf, forage ...... 200 Barley, grain ...... 20 Kiwifruit ...... 0.2 Beet, sugar, dried pulp ...... 25 Lesquerella, seed ...... 0 .1 Beet, sugar, roots ...... 10 Leucaena, forage ...... 200 Beet, sugar, tops ...... 10 Lingonberry ...... 0.2 Berry, group 13 ...... 0 .2 Longan ...... 0 .2 Betelnut ...... 1 .0 Lychee ...... 0 .2 Biriba ...... 0 .2 Mamey apple ...... 0 .2 Blimbe ...... 0 .2 Mango ...... 0.2 Borage, seed ...... 0 .1 Mangosteen ...... 0 .2 Breadfruit ...... 0 .2 Marmaladebox ...... 0 .2 Cacao bean ...... 0 .2 Meadowfoam, seed ...... 0 .1 Cactus, fruit ...... 0 .5 Mioga, flower ...... 0 .2 Cactus, pads ...... 0 .5 Mustard, seed ...... 0 .1 Canistel ...... 0 .2 Noni ...... 0 .20 Canola, meal ...... 15 Nut, pine ...... 1 .0 Canola, seed ...... 10 Nut, tree, group 14 ...... 1 .0 Cattle, kidney ...... 4 .0 Oat, grain ...... 20 Cattle, liver ...... 0 .5 Okra ...... 0.5 Chaya ...... 1.0 Olive ...... 0 .2 Cherimoya ...... 0 .2 Oregano, Mexican, leaves ...... 2 .0 Citrus, dried pulp ...... 1 .5 Palm heart ...... 0 .2 Coconut ...... 0 .1 Palm heart, leaves ...... 0 .2 Coffee, bean ...... 1 .0 Palm, oil ...... 0 .1 Corn, field, forage ...... 6 .0 Papaya ...... 0 .2 Corn, field, grain ...... 1 .0 Papaya, mountain ...... 0.2 Cotton, gin byproducts ...... 175 Passionfruit ...... 0 .2 Cotton, undelinted seed ...... 35 Pawpaw ...... 0 .2 Cranberry ...... 0 .2 Pea, dry ...... 8 .0 Crambe, seed ...... 0.1 Peanut ...... 0 .1 Custard apple ...... 0 .2 Peanut, hay ...... 0.5 Date ...... 0 .2 Pepper leaf, fresh leaves ...... 0 .2 Dokudami ...... 2 .0 Peppermint, tops ...... 200 Durian ...... 0 .2 Perilla, tops ...... 1 .8 Egg ...... 0 .05 Persimmon ...... 0 .2 Epazote ...... 1 .3 Pineapple ...... 0.1 Feijoa ...... 0 .2 Pistachio ...... 1.0 Fig ...... 0 .2 Pomegranate ...... 0 .2 Fish ...... 0 .25 Poultry, meat ...... 0 .1

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(d) Indirect or inadvertent residues. Commodity Parts per million [Reserved] Poultry, meat byproducts ...... 1.0 [45 FR 64911, Oct. 1, 1980] Pulasan ...... 0 .2 Quinoa, grain ...... 5 .0 EDITORIAL NOTE: For FEDERAL REGISTER ci- Rambutan ...... 0 .2 Rapeseed, meal ...... 15 tations affecting § 180.364, see the List of CFR Rapeseed, seed ...... 10 Sections Affected, which appears in the Rose apple ...... 0 .2 Finding Aids section of the printed volume Safflower ...... 85 and on GPO Access. Safflower, seed ...... 0 .1 Salal ...... 0 .2 Sapodilla ...... 0 .2 § 180.367 n-Octyl bicycloheptenedi- Sapote, black ...... 0 .2 carboximide; tolerances for resi- Sapote, mamey ...... 0 .2 dues. Sapote, white ...... 0 .2 Sesame, seed ...... 0 .1 (a) General. (1) Tolerances are estab- Sheep, kidney ...... 4.0 lished for residues of the insecticide n- Sheep, liver ...... 0.5 Shellfish ...... 3 .0 octyl bicycloheptene-dicarboximide, Sorghum, grain, grain ...... 15 resulting from dermal application, in Soursop ...... 0 .2 food commodities as follows: Soybean, forage ...... 100 Soybean, hay ...... 200 Parts per Soybean, hulls ...... 100 Commodity million Soybean, seed ...... 20 Spanish lime ...... 0 .2 Cattle, fat ...... 0.3 Spearmint, tops ...... 200 Goat, fat ...... 0 .3 Spice subgroup 19B ...... 7 .0 Star apple ...... 0 .2 Hog, fat ...... 0 .3 Starfruit ...... 0 .2 Horse, fat ...... 0 .3 Stevia, dried leaves ...... 1 .0 Milk, fat ...... 0 .3 Strawberry ...... 0 .2 Sheep, fat ...... 0 .3 Sugar apple ...... 0 .2 Sugarcane, cane ...... 2.0 Sugarcane, molasses ...... 30 (2) N-octylbicycloheptene Sunflower ...... 85 dicarboximide may be safely used in Sunflower, seed ...... 0.1 accordance with the following pre- Surinam cherry ...... 0 .2 Tamarind ...... 0 .2 scribed conditions: Tea, dried ...... 1 .0 (i) It is used in combination with Tea, instant ...... 7 .0 piperonyl butoxide and pyrethrins for Teff, grain ...... 5 .0 Ti, leaves ...... 0 .2 insect control in food-processing and Ti, roots ...... 0 .2 food-storage areas, provided that the Ugli fruit ...... 0.5 food is removed or covered prior to Vegetable, leafy, brassica, group 5 ...... 0.2 Vegetable, bulb, group 3 ...... 0 .2 such use. Vegetable, cucurbit, group 9 ...... 0.5 (ii) Residues in food resulting from Vegetable, foliage of legume, subgroup 7A, ex- the use described in paragraph (a)(2)(i) cept soybean ...... 0 .2 Vegetable, fruiting, group 8 ...... 0.1 of this section shall not exceed 10 parts Vegetable, leafy, group 4 ...... 0 .2 per million of N- octylbicycloheptene Vegetable, leaves of root and tuber, group 2, dicarboximide, 10 parts per million of except sugar beet tops ...... 0 .2 Vegetable, legume, group 6, except soybean .... 5 .0 piperonyl butoxide, and 1 part per mil- Vegetable, legume, group 6 except soybean lion of pyrethrins. and pea,dry ...... 5 .0 (iii) To assure safe use of the pes- Vegetable, root and tuber, group 1, except sugar beet ...... 0 .2 ticide, its label and labeling shall con- Wasabi, roots ...... 0 .2 form to that registered with the U.S. Water spinach, tops ...... 0.2 Environmental Protection Agency and Watercress, upland ...... 0 .2 Wax jambu ...... 0 .2 it shall be used in accordance with Wheat, bran ...... 20 such label and labeling. Wheat, grain ...... 5 .0 Wheat, middlings ...... 20 (b) Section 18 emergency exemptions. Wheat, shorts ...... 20 [Reserved] Yacon, tuber ...... 0.2 (c) Tolerances with regional registra- tions. [Reserved] (b) Section 18 emergency exemptions. (d) Indirect or inadvertent residues. [Reserved] [Reserved] (c) Tolerances with regional registra- tions. [Reserved] [65 FR 33713, May 24, 2000]

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§ 180.368 Metolachlor; tolerances for Commodity Parts per residues. million (a) General. (1) Tolerances are estab- Rye, grain ...... 0.1 lished for the combined residues (free Rye, straw ...... 0 .5 Safflower, seed ...... 0 .1 and bound) of the herbicide Seed and pod vegetables (except soybean) ...... 0 .3 metolachlor [2-chloro-N-(2-ethyl-6- Sheep, fat ...... 0 .02 methylphenyl)-N-(2-methoxy-1- Sheep, kidney ...... 0.2 Sheep, liver ...... 0.05 methylethyl)acetamide] and its me- Sheep, meat ...... 0.02 tabolites, determined as the deriva- Sheep, meat byproducts, except kidney and tives, 2-[(2-ethyl-6- liver ...... 0 .02 Sorghum, forage and fodder ...... 2.0 methylphenyl)amino]-1-propanol and 4- Sorghum, grain ...... 0 .3 (2-ethyl-6-methylphenyl)-2-hydroxy-5- Soybean ...... 0.2 methyl-3-morpholinone, each expressed Soybean, forage and hay ...... 8 .0 as the parent compound, in or on the Vegetable, foliage of legume, except soybean, subgroup 7A ...... 15 .0 raw agricultural commodities. Wheat, forage ...... 0 .5 Wheat, grain ...... 0 .1 Parts per Wheat, straw ...... 0 .5 Commodity million

Almond, hulls ...... 0 .3 (2) Tolerances are established for Barley, grain ...... 0 .1 combined residues of the herbicide S- Barley, straw ...... 0 .5 metolachlor acetamid, 2-chloro-N-(2- Buckwheat, grain ...... 0.1 Cabbage ...... 1 .0 ethyl-6-methylphenyl)-N-(2-methoxy-1- Cattle, fat ...... 0.02 methylethyl)-, (S) and its metabolites, Cattle, kidney ...... 0 .2 determined as the derivatives, 2-(2- Cattle, liver ...... 0 .05 Cattle, meat ...... 0 .02 ethyl-6-methylphenyl)amino-1-pro- Cattle, meat byproducts, except kidney and liver 0.02 panol and 4-(2-ethyl-6-methylphenyl)-2- Celery ...... 0 .1 hydroxy-5-methyl-3-morpholinone, Corn, forage and fodder ...... 8.0 Corn, grain ...... 0 .1 each expressed as the parent compound Corn, sweet, kernel plus cob with husks re- S-metolachlor in or on the following moved ...... 0 .1 raw agricultural commodities: Cotton, undelinted seed ...... 0 .1 Egg ...... 0 .02 Parts per Fruit, stone, group 12 ...... 0 .1 Commodity million Goat, fat ...... 0 .02 Goat, kidney ...... 0 .2 Asparagus ...... 0.10 Goat, liver ...... 0.05 Beet, sugar, molasses ...... 2 .0 Goat, meat ...... 0.02 Beet, sugar, roots ...... 0 .5 Goat, meat byproducts, except kidney and liver 0 .02 Beet, sugar, tops ...... 15.0 Horse, fat ...... 0 .02 Grass, forage ...... 10 .0 Horse, kidney ...... 0 .2 Grass, hay ...... 0 .2 Horse, liver ...... 0 .05 Spinach ...... 0 .5 Horse, meat ...... 0 .02 Sunflower, seed ...... 0.5 Horse, meat byproducts, except kidney and liver 0 .02 Sunflower, meal ...... 1 .0 Milk ...... 0.02 Millet, fodder ...... 0 .5 (3) Tolerances are established for the Millet, forage ...... 0 .5 Millet, grain ...... 0 .1 combined residues (free and bound) of Milo, fodder ...... 0 .5 the herbicide S-metolachlor [S-2- Milo, forage ...... 0 .5 chloro-N-(2-ethyl-6-methylphenyl)-N-(2- Milo, grain ...... 0 .1 Nongrass animal feed (forage, fodder, straw, methoxy-1-methylethyl)acetamide], its and hay) group ...... 3 .0 R-enantiomer, and its metabolites, de- Nut, tree, group 14 ...... 0 .1 termined as the derivatives, 2-[2-ethyl- Oat, forage ...... 0 .5 Oat, grain ...... 0 .1 6-methylphenyl)amino]-1-propanol and Oat, straw ...... 0.5 4-(2-ethyl-6-methylphenyl)-2-hydroxy-5- Peanut ...... 0 .5 methyl-3-morpholinone, each expressed Peanut, forage and hay ...... 30 .0 as the parent compound, in or on the Pepper, bell ...... 0 .1 Potato ...... 0 .2 following raw agricultural commod- Poultry, fat ...... 0.02 ities: Poultry, liver ...... 0 .05 Poultry, meat ...... 0 .02 Parts per Poultry, meat byproducts, except liver ...... 0 .02 Commodity million Rice, forage ...... 0 .5 Rice, straw ...... 0 .5 Brassica, head and stem, subgroup 5A ...... 0 .6 Rice, grain ...... 0 .1 Cattle, fat ...... 0.04 Rye, forage ...... 0 .5 Cattle, kidney ...... 0 .2

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(free and bound) of the herbicide Commodity Parts per million metolachlor [2-chloro-N-(2-ethyl-6- Cattle, liver ...... 0 .1 methylphenyl)-N-(2-methoxy-1- Cattle, meat ...... 0 .04 methylethyl)acetamide] and its me- Cattle, meat byproducts, except kidney and liver 0.04 tabolites, determined as the deriva- Corn, field, stover ...... 6 .0 Corn, pop, stover ...... 6.0 tives, 2-[(2-ethyl-6- Corn, sweet, stover ...... 6 .0 methylphenyl)amino]-1-propanol and 4- Corn, field, forage ...... 6 .0 (2-ethyl-6-methylphenyl)-2-hydroxy-5- Corn, sweet, forage ...... 6 .0 methyl-3-morpholinone, each expressed Corn, sweet, kernel plus cob with husks re- moved ...... 0 .1 as the parent compound, in or on the Corn, field, grain ...... 0 .1 following raw agricultural commod- Corn, pop, grain ...... 0.1 ities: Cotton, gin byproducts ...... 4 .0 Cotton, undelinted seed ...... 0 .1 Parts per Egg ...... 0 .04 Commodity million Garlic, bulb ...... 0.1 Goat, fat ...... 0 .04 Onion, dry bulb ...... 1 .0 Goat, kidney ...... 0 .2 Pepper, chili ...... 0 .5 Goat, liver ...... 0.1 Pepper, cubanelle ...... 0.1 Goat, meat ...... 0.04 Pepper, tabasco ...... 5 Goat, meat byproducts, except kidney and liver 0 .04 Horse, fat ...... 0 .04 (2) Tolerances with regional registra- Horse, kidney ...... 0 .2 Horse, liver ...... 0 .1 tion as defined in § 180.1(n) are estab- Horse, meat ...... 0 .04 lished for the combined residues (free Horse, meat byproducts, except, kidney and and bound) of the herbicide S- liver ...... 0 .04 metolachlor [S-2-chloro-N-(2-ethyl-6- Milk ...... 0.02 Onion, dry bulb ...... 0 .1 methylphenyl)-N-(2-methoxy-1- Onion, green ...... 2 .0 methylethyl)acetamide], its R- Peanut ...... 0 .2 enantiomer, and its metabolites, deter- Peanut, hay ...... 20.0 Peanut, meal ...... 0 .4 mined as the derivatives, 2-[2-ethyl-6- Poultry, fat ...... 0.04 methylphenyl)amino]-1-propanol and 4- Poultry, meat ...... 0 .04 (2-ethyl-6-methylphenyl)-2-hydroxy-5- Poultry, meat byproducts ...... 0.04 methyl-3-morpholinone, each expressed Pumpkin ...... 0.1 Safflower, seed ...... 0 .1 as the parent compound, in or on the Shallot, bulb ...... 0 .1 following raw agricultural commod- Sheep, fat ...... 0 .04 ities: Sheep, kidney ...... 0.2 Sheep, liver ...... 0.1 Parts per Sheep, meat ...... 0.04 Commodity million Sheep, meat byproducts, except kidney and liver ...... 0 .04 Pepper, tabasco ...... 0 .5 Sorghum, grain, forage ...... 1.0 Sorghum, grain, stover ...... 4 .0 (d) Indirect or inadvertent residues. Sorghum, grain, grain ...... 0 .3 Soybean, forage ...... 5 .0 Tolerances are established for the indi- Soybean, hay ...... 8 .0 rect or inadvertent combined residues Soybean, seed ...... 0 .2 (free and bound) of the herbicide S- Squash, winter ...... 0 .1 metolachlor [S-2-chloro-N-(2-ethyl-6- Tomato, paste ...... 0 .3 Vegetable, foliage of legume, except soybean, methylphenyl)-N-(2-methoxy-1- subgroup 7A ...... 15 .0 methylethyl)acetamide], its R- Vegetable, fruiting group 8, (except tabasco enantiomer, and its metabolites, deter- pepper) ...... 0.1 mined as the derivatives, 2-[2-ethyl-6- Vegetable, leaf petioles, subgroup 4B ...... 0 .1 Vegetable, legume, edible podded, subgroup 6A 0 .5 methylphenyl)amino]-1-propanol and 4- Vegetable, legume, pea and bean, dried (2-ethyl-6-methylphenyl)-2-hydroxy-5- shelled, (except soybean) subgroup 6C ...... 0 .1 methyl-3-morpholinone, each expressed Vegetable, root, (except sugar beet) subgroup 1B ...... 0 .3 as the parent compound, in or on the Vegetables, tuberous and corm, subgroup 1C ... 0.2 following raw agricultural commod- ities: (b) Section 18 emergency exemptions. Parts per [Reserved] Commodity million (c) Tolerances with regional registra- tions. (1) Tolerances with regional reg- Barley, grain ...... 0 .1 Barley, hay ...... 1 .0 istration as defined in § 180.1(n) are es- Barley, straw ...... 0 .5 tablished for the combined residues Buckwheat, grain ...... 0.1

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(d) Indirect or inadvertent residues. Commodity Parts per million [Reserved] Nongrass, animal feed (forage, fodder, straw, [71 FR 56399, Sept. 27, 2006] hay) group 18 ...... 1 .0 Oat, forage ...... 0 .5 Oat, grain ...... 0 .1 § 180.370 5-Ethoxy-3-(trichloromethyl)- Oat, hay ...... 1.0 1,2,4-thiadiazole; tolerances for resi- Oat, straw ...... 0.5 dues. Rice, grain ...... 0 .1 (a) General. Tolerances are estab- Rice, straw ...... 0 .5 Rye, forage ...... 0 .5 lished for residues of the fungicide 5- Rye, grain ...... 0.1 ethoxy-3-(trichloromethyl)-1,2,4- Rye, straw ...... 0 .5 thiadiazole and its monoacid metabo- Wheat, forage ...... 0 .5 Wheat, grain ...... 0 .1 lite 3-carboxy-5-ethoxy-1,2,4- Wheat, hay ...... 1 .0 thiadiazole in or on the following raw Wheat, straw ...... 0 .5 agricultural commodities:

Parts per [44 FR 10385, Feb. 20, 1979] Commodity million

EDITORIAL NOTE: For FEDERAL REGISTER ci- Cattle, fat ...... 10 tations affecting § 180.368, see the List of Sec- Cattle, meat byproducts ...... 10 tions Affected, which appears in the Finding Cattle, meat ...... 10 Aids section of the printed volume and on Corn, field, grain ...... 05 GPO Access. Corn, forage ...... 10 Corn, stover ...... 10 Cotton, undelinted seed ...... 20 § 180.369 Difenzoquat; tolerances for Egg ...... 05 residues. Goat, fat ...... 10 (a) General. Tolerances are estab- Goat, meat byproducts ...... 10 Goat, meat ...... 10 lished for residues of difenzoquat (1,2- Hog, fat ...... 10 dimethyl-3,5-diphenyl-1H-pyrazolium Hog, meat byproducts ...... 10 ion), derived from application of the Hog, meat ...... 10 methyl sulfate salt and calculated as Horse, fat ...... 10 Horse, meat byproducts ...... 10 the cation, in or on the following raw Horse, meat ...... 10 agricultural commodities: Milk ...... 05 Poultry, fat ...... 10 Parts per Poultry, meat byproducts ...... 10 Commodity million Poultry, meat ...... 10 Sheep, fat ...... 10 Barley, bran ...... 0 .25 Sheep, meat byproducts ...... 10 Barley, grain ...... 0 .05 Sheep, meat ...... 10 Barley, straw ...... 5 .0 Strawberry ...... 20 Cattle, fat ...... 0.05 Tomato ...... 15 Cattle, meat ...... 0 .05 Wheat, forage ...... 10 Cattle, meat byproducts ...... 0.05 Wheat, grain ...... 05 Goat, fat ...... 0 .05 Wheat, straw ...... 10 Goat, meat ...... 0.05 Goat, meat byproducts ...... 0 .05 (b) Section 18 emergency exemptions. Hog, fat ...... 0 .05 Hog, meat ...... 0 .05 [Reserved] Hog, meat byproducts ...... 0 .05 (c) Tolerances with regional registra- Horse, fat ...... 0 .05 tions. [Reserved] Horse, meat ...... 0 .05 (d) Indirect or inadvertent residues. Horse, meat byproducts ...... 0 .05 Poultry, fat ...... 0.05 [Reserved] Poultry, meat ...... 0 .05 [47 FR 49845, Nov. 3, 1982, as amended at 48 Poultry, meat byproducts ...... 0.05 Sheep, fat ...... 0 .05 FR 12088, Mar. 23, 1983; 63 FR 57076, Oct. 26, Sheep, meat ...... 0.05 1998] Sheep, meat byproducts ...... 0 .05 Wheat, bran ...... 0.25 § 180.371 Thiophanate-methyl; toler- Wheat, grain ...... 0 .05 ances for residues. Wheat, shorts ...... 0 .25 Wheat, straw ...... 5 .0 (a) General. Tolerances are estab- lished for residues of the fungicide (b) Section 18 emergency exemptions. thiophanate-methyl (dimethyl [(1,2- [Reserved] phenylene)-bis(iminocarbonothioyl)] (c) Tolerances with regional registra- bis[carbamate]), its oxygen analogue tions. [Reserved] dimethyl-4,4-o-phenylene

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bis(allophonate), and its benzimid- under section 18 emergency exemptions azole-containing metabolites (cal- granted by EPA. The tolerances are culated as thiophanate-methyl) in or specified in the following table, and on the following food commodities: will expire and are revoked on the dates specified. Parts per Commodity million Expiration/ Commodity Parts per revocation Almond ...... 0.2(N) million date Almond, hulls ...... 1 .0 Apple, dry pomace ...... 40.0 Blueberry ...... 1.5 12/31/09 Apple, postharvest ...... 7 .0 Citrus ...... 0.5 12/31/09 Apricot, postharvest ...... 15.0 Cotton ...... 0.05 12/31/07 Banana ...... 2.0 Cotton, gin byproducts ...... 5.0 12/31/07 Banana, pulp ...... 0 .2 Mushroom ...... 0.01 12/31/07 Bean (snap and dry) ...... 2.0 Vegetable, fruiting, group 8 ...... 0.5 12/31/08 Bean (forage and hay) ...... 50.0 Cattle, fat ...... 0.1 Cattle, kidney ...... 0 .2(N) (c) Tolerances with regional registra- Cattle, liver ...... 2 .5 tions. Tolerances with regional reg- Cattle, meat byproducts, except kidney and liver 0.1(N) istration, as defined in § 180.1(n), are es- Cattle, meat ...... 0 .1(N) Celery ...... 3 .0 tablished for the residues of Cherry, postharvest ...... 15 .0 thiophanate-methyl and its metabolite Cucumber ...... 1 .0 (methyl 2-benzimidazolyl carbamate Egg ...... 0 .1(N) Goat, fat ...... 0 .1(N) (MBC)), expressed as thiophanate- Goat, kidney ...... 0 .2 methyl in or on the following raw agri- Goat, liver ...... 2.5 cultural commodity: Goat, meat byproducts, except kidney and liver 0 .1(N) Goat, meat ...... 0.1(N) Parts per Grape ...... 5 .0 Commodity million Horse, fat ...... 0 .1(N) Horse, liver ...... 1 .0 Canola, seed ...... 0 .1 Horse, meat byproducts, except liver ...... 0 .1(N) Horse, meat ...... 0 .1(N) Melon ...... 1 .0 (d) Indirect or inadvertent residues. Milk ...... 1.0 [Reserved] Nectarine, postharvest ...... 15.0 Onion, dry ...... 3 .00 [65 FR 33699, May 24, 2000, as amended at 67 Onion, green ...... 3 .00 FR 55150, Aug. 28, 2002; 67 FR 57753, Sept. 12, Pear ...... 3 .0 2002; 68 FR 5852, Feb. 5, 2003; 68 FR 43470, July Peach, postharvest ...... 15.0 23, 2003; 69 FR 6567, Feb. 11, 2004; 69 FR 29459, Peanut ...... 0 .2(N) May 24, 2004; 70 FR 14555, Mar. 23, 2005; 70 FR Peanut (forage and hay) ...... 15.0 75739, Dec. 21, 2005; 71 FR 76200, Dec. 20, 2006] Pecan ...... 0 .2 Pistachio ...... 0.1 Plum, postharvest ...... 15 .0 § 180.372 2,6-dimethyl-4- Plum, prune, postharvest ...... 15 .0 tridecylmorpholine; tolerances for Potato ...... 0 .1 residues. Pumpkin ...... 1.0 Sheep, fat ...... 0 .1(N) A tolerance is established for resi- Sheep, kidney ...... 0.2 dues of the fungicide 2,6-dimethyl-4- Sheep, liver ...... 2.5 tridecylmorpholine in or on the fol- Sheep, meat byproducts, except kidney and liver ...... 0 .1(N) lowing raw agricultural commodity: Sheep, meat ...... 0.1(N) Soybean ...... 0.2 Commodity Parts per Squash ...... 1 .0 million Strawberry ...... 5 .0 Banana ...... 0.1 Sugar beet, roots ...... 0 .2 Sugar beet, tops ...... 15 .0 Sugarcane, seed piece treatment PRE-H ...... 0 .1(N) [43 FR 50176, Oct. 27, 1978] Wheat, grain ...... 0 .05 Wheat, hay ...... 0 .10 Wheat, straw ...... 0 .10 § 180.373 [Reserved]

(b) Section 18 emergency exemptions. § 180.377 Diflubenzuron; tolerances for Time-limited tolerances are estab- residues. lished for the residues of thiophanate- (a) General. (1) Tolerances are estab- methyl and its metabolite (methyl 2- lished for residues of the insecticide benzimidazoyl carbamate (MBC)) in diflubenzuron (N-[[(4- connection with use of the pesticide chlorophenyl)amino]carbonyl]-2,6-

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difluorobenzamide) in or on the fol- (b) Section 18 emergency exemptions. lowing food commodities: Time-limited tolerances are estab- lished for the residues of diflubenzuron Parts per Commodity million and its metabolites PCA (p- chloroaniline) and CPU (p- Artichoke, globe ...... 6.0 chlorophenylurea), expressed as the Cattle, fat ...... 0.05 parent diflubenzuron, in connection Cattle, meat ...... 0 .05 Cotton, undelinted seed ...... 0 .2 with use of the pesticide under section Egg ...... 0 .05 18 emergency exemptions granted by Goat, fat ...... 0 .05 EPA. The tolerances are specified in Goat, meat ...... 0.05 the following table, and will expire and Grapefruit ...... 0 .5 Hog, fat ...... 0 .05 are revoked on the dates specified. Hog, meat ...... 0 .05 Horse, fat ...... 0 .05 Parts per Expiration/ Horse, meat ...... 0 .05 Commodity revocation million date Milk ...... 0.05 Mushroom ...... 0 .2 Alfalfa, forage ...... 6.0 6/30/07 Orange, sweet ...... 0 .5 Alfalfa, hay ...... 6.0 6/30/07 Poultry, fat ...... 0.05 Poultry, meat byproducts ...... 0.05 Wheat, aspirated grain fractions ..... 30 12/31/08 Poultry, meat ...... 0 .05 Wheat, milled byproducts ...... 0.10 12/31/08 Sheep, fat ...... 0 .05 Sheep, meat ...... 0.05 (c) Tolerances with regional registra- Soybean ...... 0.05 tions. [Reserved] Soybean, hulls ...... 0 .5 Tangerine ...... 0 .5 (d) Indirect or inadvertent residues. [Reserved] (2) Tolerances are established for [65 FR 33699, May 24, 2000, as amended at 65 combined residues of the insecticide FR 47882, Aug. 4, 2000; 66 FR 16144, Mar. 23, diflubenzuron and its metabolites 4- 2001; 67 FR 7092, Feb. 15, 2002; 67 FR 35048, chlorophenlyurea and 4-chloroaniline May 17, 2002; 67 FR 59017, Sept. 19, 2002; 67 FR in or on the following food commod- 59181, Sept. 20, 2002; 68 FR 51484, Aug. 27, 2003; ities: 69 FR 29459, May 24, 2004; 70 FR 75739, Dec. 21, 2005; 71 FR 69033, Nov. 29, 2006] Commodity Parts per million § 180.378 Permethrin; tolerances for Almond , hulls ...... 6.0 residues. Barley, grain ...... 0 .06 (a) Tolerances, to expire on Novem- Barley, hay ...... 3 .0 Barley, straw ...... 1 .8 ber 15, 1997, are established for residues Brassica, leafy greens, subgroup 5B ...... 9 .0 of the insecticide permethrin [(3- Cattle, meat byproducts ...... 0.15 pheoxyphenyl)methyl 3-(2,2- Fruit, stone, group 12, except cherry ...... 0 .07 dichloroethenyl)-2,2- Goat, meat byproducts ...... 0 .15 Grain, aspirated fractions ...... 11 dimethylcyclopropane carboxylate] in Grass, forage, fodder, and hay, group 17 ...... 6 .0 or on the following raw agricultural Hog, meat byproducts ...... 0 .15 commodities: Horse, meat byproducts ...... 0 .15 Nut, tree, group 14 ...... 0 .06 Parts per Oat, forage ...... 7 .0 Commodity million Oat, grain ...... 0 .06 Oat, hay ...... 6.0 Cotton, undelinted seed ...... 0 .5 Oat, straw ...... 3.5 Peanut ...... 0 .10 Peanut, hay ...... 55 (b) Tolerances are established for res- Peanut, refined oil ...... 0.20 idues of the insecticide permethrin [(3- Pear ...... 0 .50 phenoxyphenyl)methyl 3-(2,2- Pepper ...... 1 .0 dichloroethenyl)-2,2- Pistachio ...... 0.06 Pummelo ...... 0 .50 dimethylcyclopropane carboxylate] Rice, grain ...... 0 .02 and the sum of its metabolites 3-(2,2- Rice, straw ...... 0 .8 dichloroethenyl)-2,2- Sheep, meat byproducts ...... 0 .15 dimethylcyclopropane carboxylic acid Turnip greens ...... 9 .0 Wheat, forage ...... 7 .0 (DCVA) and (3- Wheat, grain ...... 0 .06 phenoxyphenyl)methanol (3-PBA) in or Wheat, hay ...... 6 .0 on the following raw agricultural com- Wheat, straw ...... 3 .5 modities:

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Parts per Parts per Commodity million Commodity million

Alfalfa, forage ...... 25.0 Sheep, fat ...... 3 .0 Alfalfa, hay ...... 55.0 Sheep, meat ...... 0.25 Almond ...... 0.05 Sheep, meat byproducts ...... 2 .0 Almond, hulls ...... 20 .0 Apple ...... 0.05 (d) Tolerances with regional registra- Artichoke, globe ...... 10.0 Asparagus ...... 1.0 tion, as defined in § 180.1(n), are estab- Avocado ...... 1 .0 lished for residues of permethrin [(3- Broccoli ...... 1 .0 phenoxyphenyl)methyl-3-(2,2- Brussels sprouts ...... 1 .0 Cabbage ...... 6 .0 dichloroethenyl)-2,2- Celery ...... 5 .0 dimethylcyclopropane carboxylate] Cauliflower ...... 1 .0 and the sum of its metabolites 3-(2,2- Cherry ...... 3.0 Corn, forage ...... 60 .0 dichloroethenyl(-2,2- Corn grain (field and pop) ...... 0 .05 dimethylcyclopropane carboxylic acid Corn, stover ...... 60 .0 (DCVA) and (3- Corn, sweet, kernel plus cob with husks re- phenoxyphenyl)methanol (3-PBA) in or moved ...... 0 .1 Eggplant ...... 1.0 on the following raw agricultural com- Filbert ...... 0 .05 modities: Garlic ...... 0 .1 Grass, range ...... 15.0 Parts per Horseradish ...... 1.0 Commodity million Kiwifruit ...... 2.0 Lettuce, head ...... 20.0 Collards ...... 20 Mushroom ...... 6 .0 Papaya ...... 1 .0 Onion, dry bulb ...... 0 .1 Turnip, greens ...... 20 Peach ...... 5 .0 Turnip, roots ...... 1 Pear ...... 3 .0 Pepper, bell ...... 1 .0 Pistachio ...... 0.1 [47 FR 45010, Oct. 13, 1982] Potato ...... 0 .05 Soybean ...... 0.05 EDITORIAL NOTE: For FEDERAL REGISTER ci- Spinach ...... 20 .0 tations affecting § 180.378, see the List of CFR Tomato ...... 2 Sections Affected, which appears in the Vegetable, cucurbit, group 9 ...... 3.0 Finding Aids section of the printed volume Vegetable, leafy, except brassica, group 4 ...... 20.0 and on GPO Access. Walnut ...... 0 .05 Watercress ...... 5 .0 § 180.379 Cyano(3-phenoxy- phenyl)methyl-4-chloro-ù-(1-methy- (c) Tolerances are established for res- lethyl) benzeneacetate; tolerances idues of permethrin and the sum total for residues. of its metabolites 3-(2,2- dichloroethenyl)-2,2- (a) General. (1) Tolerances are estab- dimethylcyclopropane carboxylic acid lished for residues of the insecticide (DCVA) and (3- Cyano(3-phenoxyphenyl)methyl-4- phenoxyphenyl(methanol (3-PBA) and chloro-a-(1- 3-phenoxybenzoic acid in or on the fol- methylethyl)benzeneacetate in or on lowing animal commodities. the following raw agricultural com- modities: Parts per Commodity million Parts per Commodity million Cattle, fat ...... 3.0 Cattle, meat ...... 0 .25 Almond, hulls ...... 15 .0 Cattle, meat byproducts ...... 2.0 Almond ...... 0.2 Egg ...... 1 .0 Apple ...... 2.0 Goat, fat ...... 3 .0 Artichoke, globe ...... 0.2 Goat, meat ...... 0.25 Bean, dry, seed ...... 0 .25 Goat, meat byproducts ...... 2 .0 Bean, snap, succulent ...... 2 .0 Hog, fat ...... 3 .0 Broccoli ...... 2 .0 Hog, meat ...... 0 .25 Blueberry ...... 3 .0 Hog, meat byproducts ...... 3 .0 Cabbage ...... 10 .0 Horse, fat ...... 3 .0 Caneberry subgroup 13A ...... 3 .0 Horse, meat ...... 0 .25 Cantaloupe ...... 1 .0 Horse, meat byproducts ...... 2 .0 Carrot, roots ...... 0.5 Milk, fat (reflecting 0.25 ppm in whole milk) ...... 6 .25 Cattle, fat ...... 1.5 Poultry, fat ...... 0.15 Cattle, meat byproducts ...... 1.5 Poultry, meat ...... 0 .05 Cattle, meat ...... 1 .5 Poultry, meat byproducts ...... 0.25 Cauliflower ...... 0 .5

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(1-methylethyl)benzeneacetate shall be Commodity Parts per million limited to space treatment with a max- Collards ...... 10.0 imum of 0.5 fluid ounce of a 0.05-per- Corn, grain ...... 0 .02 cent active ingredient solution per Corn, forage ...... 50 .0 1,000 cubic feet of space, or as a contact Corn, stover ...... 50 .0 Corn, sweet, kernels and cobs ...... 0.1 spray applied as a coarse wet spray at Cotton, undelinted seed ...... 0 .2 a maximum of 1 gallon of a 0.2-percent Cucumber ...... 0 .5 active ingredient solution per 1,000 Currant ...... 3 .0 Eggplant ...... 1.0 square feet of surface. Food must be re- Elderberry ...... 3 .0 moved or covered during treatment. English walnut ...... 0.2 Spray should not be applied directly to Filbert ...... 0 .2 surfaces or utensils that may come Fruit, stone ...... 10 .0 Goat, fat ...... 1 .5 into contact with food. Food-contact Goat, meat byproducts ...... 1 .5 surfaces and equipment should be thor- Goat, meat ...... 1.5 oughly cleaned with an effective clean- Gooseberry ...... 3 .0 Hog, fat ...... 1 .5 ing compound and rinsed with potable Hog, meat byproducts ...... 1 .5 water before using. Hog, meat ...... 1 .5 (iii) Application of (S)-cyano(3- Horse, fat ...... 1 .5 Horse, meat byproducts ...... 1 .5 phenoxyphenyl) methyl-(S)-4-chloro- Horse, meat ...... 1 .5 alpha-(1-methylethyl)benzeneacetate Huckleberry ...... 3 .0 shall be limited to space treatment Melon, honeydew ...... 1.0 Milk ...... 0.3 with a maximum of 1.0 fluid ounce of a Milk, fat ...... 7 .0 0.25-percent active ingredient solution Muskmelon ...... 1 .0 per 1,000 cubic feet of space, or as a Peanut ...... 0 .02 contact spray applied as a coarse wet Pear ...... 2 .0 Pea ...... 1 .0 spray at a maximum of 1 gallon of a Pea, dry, seed ...... 0 .25 0.05-percent active ingredient solution Pecan ...... 0 .2 per 1,000 square feet of surface, or as a Pepper ...... 1 .0 Potato ...... 0 .02 pressurized spot/crack and crevice Pumpkin ...... 1.0 spray of a 0.25-percent solution. Food Radish, roots ...... 0 .3 must be removed or covered during Radish, tops ...... 8 .0 Sheep, fat ...... 1 .5 treatment. Spray should not be applied Sheep, meat byproducts ...... 1 .5 directly to surfaces or utensils that Sheep, meat ...... 1.5 may come into contact with food. Soybean ...... 0.05 Squash, summer ...... 0 .5 Food-contact surfaces and equipment Squash, winter ...... 1 .0 should be thoroughly cleaned with an Sugarcane, cane ...... 2.0 effective cleaning compound and rinsed Sunflower, seed ...... 1.0 with potable water before using. Tomato ...... 1.0 Turnip, greens ...... 20.0 (iv) To assure safe use of the addi- Turnip, roots ...... 0 .5 tive, its label and labeling shall con- Watermelon ...... 1.0 form to that registered with the U.S. Environmental Protection Agency, and (2) A food additive tolerance of 0.05 it shall be used in accordance with parts per million is established for resi- such label and labeling. dues of the insecticide (3) A regulation is established per- cyano(37phenoxyphenyl)methyl-4- mitting residues of the insecticide 4- chloro-alpha-(1- cyano(3-phenoxyphenyl)methyl 4- methylethyl)benzeneacetate and an chloro-alpha-(1- isomer, (S)-cyano(3- methylethyl)benzeneacetate in or on phenoxyphenyl)methyl-(S)-4-chloro- the following commodities: alpha-(1-methylethyl)-benzeneacetate, as follows: Commodity Parts per (i) In or on food commodities (other million than those already covered by a higher Soybean hulls ...... 1 .0 tolerance as a result of use on growing crops) in food-handling establishments (b) Section 18 emergency exemptions. where food products are held, proc- [Reserved] essed, or prepared. (c) Tolerances with regional registra- (ii) Application of cyano(3- tions. Tolerances with regional reg- phenoxyphenyl)methyl-4-chloro-alpha- istration are established for residues of

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the insecticide cyano(3- (c) Tolerances with regional registra- phenoxyphenyl)methyl-4-chloro-alpha- tions. [Reserved] (1-methylethyl)benzeneacetate in or on (d) Indirect or inadvertent residues. the following raw agricultural com- [Reserved] modities: (e) Revoked tolerances subject to the channel of trade provisions. The fol- Parts per Commodity million lowing table lists commodities with residues of vinclozolin resulting from Okra ...... 0.1 lawful use are subject to the channels of trade provisions of section 408(l)(5) (d) Indirect or inadvertent residues. of the FFDCA: [Reserved] Parts per [44 FR 6099, Jan. 31, 1979. Redesignated and Commodity million amended at 44 FR 37919, June 29, 1979; further amended at 55 FR 26440, June 28, 1990] Cucumber ...... 1 .0 Fruit, stone, except plum, prune, fresh ...... 25.0 EDITORIAL NOTE: For FEDERAL REGISTER ci- Pepper, bell ...... 3 .0 tations affecting § 180.379, see the List of CFR Strawberry ...... 10.0 Sections Affected, which appears in the Finding Aids section of the printed volume [62 FR 38474, July 18, 1997, as amended at 63 and on GPO Access. FR 7308, Feb. 13, 1998; 65 FR 44468, July 18, 2000; 67 FR 40189, June 12, 2002; 68 FR 56189, § 180.380 Vinclozolin; tolerances for Sept. 30, 2003; 68 FR 69323, Dec. 12, 2003; 70 FR residues. 55268, Sept. 21, 2005] (a) General. Tolerances are estab- lished for the combined residues of the § 180.381 Oxyfluorfen; tolerances for residues. fungicide vinclozolin (3-(3,5- dichlorophenyl)-5-ethenyl-5-methyl-2,4- (a) General. Tolerances are estab- oxazolidinedione) and its metabolites lished for residues of the herbicide containing the 3,5-dichloroaniline moi- oxyfluorfen [2-chloro-1-(3-ethoxy-4- ety in or on the food commodities in nitrophenoxy)-4- the table below. There are no U.S. reg- (trifluoromethyl)benzene] in or on the istrations for grape (wine) as of July following food commodities: 30, 1997. Parts per Commodity million Parts per Expiration/ Commodity million Revocation Almond, hulls ...... 0 .1 Date Artichoke, globe ...... 0.05 Avocado ...... 0 .05 Bean, succulent ...... 2.0 11/30/05 Banana (including plantain) ...... 0.05 Canola, seed ...... 1.0 11/30/08 Broccoli ...... 0 .05 Cattle, fat ...... 0.05 11/30/08 Cabbage ...... 0 .05 Cattle, meat ...... 0.05 11/30/08 Cattle, fat ...... 0.05 Cattle, meat byproducts ...... 0.05 11/30/08 Cattle, meat byproducts ...... 0.05 Egg ...... 0.05 11/30/08 Cattle, meat ...... 0 .05 Goat, fat ...... 0.05 11/30/08 Cauliflower ...... 0 .05 Goat, meat ...... 0.05 11/30/08 Cocoa bean, dried bean ...... 0 .05 Goat, meat byproducts ...... 0.05 11/30/08 Coffee, bean ...... 0 .05 Grape, wine ...... 6. 0 None Corn, grain ...... 0 .05 Hog, fat ...... 0.05 11/30/08 Cotton, undelinted seed ...... 0 .05 Hog, meat ...... 0.05 11/30/08 Date ...... 0 .05 Hog, meat byproducts ...... 0.05 11/30/08 Egg ...... 0 .05 Horse, fat ...... 0.05 11/30/08 Feijoa ...... 0 .05 Horse, meat ...... 0.05 11/30/08 Fig ...... 05 Horse, meat byproducts ...... 0.05 11/30/08 Fruit, pome, group 11 ...... 0.05 Lettuce, head ...... 10.0 11/30/05 Fruit, stone, group 12 ...... 0 .05 Lettuce, leaf ...... 10.0 11/30/05 Goat, fat ...... 0 .05 Milk ...... 0.05 11/30/08 Goat, meat byproducts ...... 0 .05 Poultry, fat ...... 0.1 11/30/08 Goat, meat ...... 0.05 Poultry, meat ...... 0.1 11/30/08 Grape ...... 0 .05 Poultry, meat byproducts ...... 0.1 11/30/08 Hog, fat ...... 0 .05 Sheep, fat ...... 0.05 11/30/08 Hog, meat byproducts ...... 0 .05 Sheep, meat ...... 0.05 11/30/08 Hog, meat ...... 0 .05 Sheep, meat byproducts ...... 0.05 11/30/08 Horseradish ...... 0.05 Horse, fat ...... 0 .05 Horse, meat byproducts ...... 0 .05 (b) Section 18 emergency exemptions. Horse, meat ...... 0 .05 [Reserved] Kiwifruit ...... 0.05

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Parts per Parts per Commodity million Commodity million

Nut, tree, group 14 ...... 0 .05 Strawberry ...... 0 .05 Olive ...... 0 .05 Onion, dry bulb ...... 0 .05 (b) Section 18 emergency exemptions. Milk ...... 0.05 Mint hay (peppermint and spearmint) ...... 0 .1 [Reserved] Persimmon ...... 0 .05 (c) Tolerances with regional restric- Pistachio ...... 0.05 tions. [Reserved] Pomegranate ...... 0 .05 Poultry, fat ...... 0.05 (d) Indirect or inadvertent residues. Poultry, meat byproducts ...... 0.05 [Reserved] Poultry, meat ...... 0 .05 Sheep, fat ...... 0 .05 [45 FR 24877, Apr. 11, 1980, as amended at 46 Sheep, meat byproducts ...... 0 .05 FR 61272, Dec. 16, 1981; 47 FR 39490, Sept. 8, Sheep, meat ...... 0.05 1982; 61 FR 30165, June 14, 1996; 62 FR 39974, Soybean ...... 0.05 July 25, 1997; 67 FR 35048, May 17, 2002; 69 FR 6567, Feb. 11, 2004; 71 FR 54434, Sept. 15, 2006] (b) Section 18 emergency exemptions. [Reserved] § 180.384 Mepiquat (N,N-dimethylpip- (c) Tolerances with regional registra- eridinium); tolerances for residues. tions. Tolerances with regional reg- (a) General. (1) Tolerances are estab- istration are established for residues of lished for residues of the plant growth the herbicide oxyfluorfen [2-chloro-1-(3- regulator mepiquat (N,N- ethoxy-4-nitrophenoxy)-4- dimethylpiperidinium) in or on the fol- (trifluoromethyl)benzene] in or on the lowing commodities: following food commodities: Commodity Parts per Parts per million Commodity million Cattle, meat byproducts ...... 0.1 Blackberry ...... 0 .05 Cotton, gin byproducts ...... 6 .0 Chickpea, seed ...... 0 .05 Cotton, undelinted seed ...... 2 .0 Guava ...... 0 .05 Goat, meat byproducts ...... 0 .1 Papaya ...... 0 .05 Hog, meat byproducts ...... 0 .1 Raspberry ...... 0 .05 Horse, meat byproducts ...... 0 .1 Taro, corm and leaves ...... 0 .05 Sheep, meat byproducts ...... 0 .1

(d) Indirect or inadvertent residues. (2) Tolerances are established for res- [Reserved] idues of the plant growth regulator [45 FR 85022, Dec. 24, 1980] mepiquat chloride (N,N- dimethylpiperidinium chloride) in or EDITORIAL NOTE: For FEDERAL REGISTER ci- tations affecting § 180.381, see the List of CFR on the following commodities: Sections Affected, which appears in the Parts per Finding Aids section of the printed volume Commodity million and on GPO Access. Cattle, fat ...... 0.1 § 180.383 Sodium salt of acifluorfen; Cattle, meat ...... 0 .1 tolerances for residues. Goat, fat ...... 0 .1 Goat, meat ...... 0.1 (a) General. Tolerances are estab- Grape ...... 1 .0 lished for combined residues of the her- Grape, raisin ...... 5 .0 bicide sodium salt of acifluorfen, so- Hog, fat ...... 0 .1 Hog, meat ...... 0 .1 dium 5-[2-chloro-4- Horse, fat ...... 0 .1 (trifluoromethyl)phenoxy]-2- Horse, meat ...... 0 .1 nitrobenzoate, and its metabolites (the Sheep, fat ...... 0 .1 corresponding acid, methyl ester, and Sheep, meat ...... 0.1 amino analogues) in or on the fol- (b) Section 18 emergency exemptions. lowing raw agricultural commodities: [Reserved] (c) Tolerances with regional registra- Commodity Parts per million tions. [Reserved] Peanut ...... 0 .1 (d) Indirect or inadvertent residues. Rice, grain ...... 0 .1 [Reserved] Rice, straw ...... 0 .2 Soybean, seed ...... 0 .1 [67 FR 3118, Jan. 23, 2002]

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§ 180.385 Diclofop-methyl; tolerances [44 FR 75639, Dec. 21, 1979; 45 FR 17147, Mar. for residues. 18, 1980, as amended at 48 FR 32014, July 13, 1983; 61 FR 19849, May 3, 1996] (a) General. Tolerances are estab- lished for the combined residues of the § 180.395 Hydramethylnon; tolerances herbicide diclofop-methyl (methyl 2-[4- for residues. (2,4- (a) General. Tolerances are estab- dichlorophenoxy)phenoxy]propanoate) lished for residues of the insecticide and its metabolites, 2-[4-(2,4- tetrahydro-5,5-dimethyl-2(1H)- dichlorophenoxy)phenoxy]propanoic pyrimidinone(3-(4- acid and 2-[4-(2,4-dichloro-5- (trifluoromethyl)phenyl)-1-(2-(4- hydroxyphenoxy)phenoxy]propanoic (trifluoromethyl)phenyl)ethenyl)-2- acid, in or on the following raw agri- propenylidene)hydrazone in or on the cultural commodities: following raw agricultural commod- Parts per ities: Commodity million Commodity Parts per Barley, grain ...... 0 .1 million Barley, straw ...... 0 .1 Grass (pasture and rangeland) ...... 0.05 Lentil, seed ...... 0 .1 Grass hay (pasture and rangeland) ...... 0.05 Pea seeds (dry) ...... 0 .1 Pineapple ...... 0.05 Wheat, grain ...... 0 .1 Wheat, straw ...... 0 .1 (b) Section 18 emergency exemptions. (b) Section 18 emergency exemptions. Time-limited tolerances are estab- [Reserved] lished for residues of the insecticide (c) Tolerances with regional registra- hydramethylnon; tetrahydro-5,5-di- tions. [Reserved] methyl-2-(1H)-pyrimidinoine(3-(4- (d) Indirect or inadvertent residues. trifluoromethyl)phenyl)-1-[2- [Reserved] [4(trifluoromethly)phenyl]ethenyl)-2- propenylidene) hydrazone in connec- [45 FR 23425, Apr. 7, 1980, as amended at 50 tion with the use of the pesticides FR 20211, May 15, 1985; 51 FR 3599, Jan. 29, under section 18 emergency exemptions 1986; 51 FR 19176, May 28, 1986; 63 FR 57077, Oct. 26, 1998] granted by EPA. The tolerance will ex- pire and is revoked on the date speci- §§ 180.388–180.389 [Reserved] fied in the following table. Expiration/ § 180.390 Tebuthiuron; tolerances for Commodity Parts per Revocation residues. million Date

Tolerances are established for resi- Pineapple ...... 0.05 6/30/05 dues of the herbicide tebuthiuron (N-[5- 1,1-dimethylethyl)-1,3,4-thiadiazol-2- (c) Tolerances with regional registra- yl]-N,N′-dimethylurea) and its metabo- tions. [Reserved] lites containing the dimethylethyl (d) Indirect or inadvertent residues. thiadiazole moiety in or on the fol- [Reserved] lowing raw agricultural commodities: [45 FR 55198, Aug. 19, 1980, as amended at 63 Parts per FR 10543, Mar. 4, 1998; 63 FR 65073, Nov. 25, Commodity million 1998; 66 FR 28672, May 24, 2001; 68 FR 37764, June 25, 2003; 68 FR 48312, Aug. 13, 2003] Cattle, fat ...... 2 Cattle, meat byproducts ...... 2 § 180.396 Hexazinone; tolerances for Cattle, meat ...... 2 Goat, fat ...... 2 residues. Goat, meat byproducts ...... 2 (a) General. (1) Tolerances are estab- Goat, meat ...... 2 Grass, forage ...... 10 .0 lished for the combined residues of Grass, hay ...... 10 .0 hexazinone (3-cyclohexyl-6- Horse, fat ...... 2 (dimethylamino)-1-methyl-1,3,5-tri- Horse, meat byproducts ...... 2 azine-2,4-(1H,3H)-dione) and its plant Horse, meat ...... 2 Milk ...... 0.3 metabolites; A [3-(4- Sheep, fat ...... 2 hydroxycyclohexyl)-6- Sheep, meat byproducts ...... 2 (dimethylamino)-1-methyl-1,3,5-tri- Sheep, meat ...... 2 azine-2,4-(1H,3H)-dione], B [3-

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cyclohexyl-6-(methylamino)-1-methyl- (1H,3H)-dione) (calculated as 1,3,5-triazine-2,4-(1H,3H)-dione], C [3-(4- hexazinone) in milk: hydroxycyclohexyl)-6-(methylamino)-1- Parts per methyl-1,3,5-triazine-2,4-(1H,3H)-dione], Commodity million D [3-cyclohexyl)-1-methyl-1,3,5-tri- azine-2,4,6-(1H,3H,5H)-trione], and E [3- Milk ...... 0.2 (4-hydroxycyclohexyl)-1-methyl-1,3,5- triazine-2,4,6-(1H,3H,5H)-trione] (cal- (b) Section 18 emergency exemptions. culated as hexazinone) in the following [Reserved] (c) Tolerances with regional registra- commodities: tions. Tolerances with regional reg- istration, as defined in § 180.1(n) and Commodity Parts per million which excludes use of hexazinone on Alfalfa, forage ...... 2.0 sugarcane in Florida, are established Alfalfa, hay ...... 8.0 for the combined residues of Alfalfa, seed ...... 2 .0 hexazinone (3-cyclohexyl-6- Blueberry ...... 0 .6 (dimethylamino)-1-methyl-1,3,5-tri- Grass, forage ...... 10 .0 azine-2,4-(1H,3H)-dione and its plant Pineapple ...... 0.6 metabolites; A [3-(4- (2) Tolerances are established for the hydroxycyclohexyl)-6- combined residues of hexazinone (3- (dimethylamino)-1-methyl-1,3,5-tri- cyclohexyl-6-(dimethylamino)-1-meth- azine-2,4(1H,3H)-dione], B [3- yl-1,3,5-triazine-2,4-(1H,3H)-dione) and cyclohexyl-6-(methylamino)-1-methyl- its animal tissue metabolites; B [3- 1,3,5-triazine-2,4-(1H,3H)-dione], C [3-(4- cyclohexyl-6-(methylamino)-1-methyl- hydroxycyclohexyl)-6-(methylamino)-1- 1,3,5-triazine-2,4-(1H,3H)-dione], and F methyl-1,3,5-triazine-2,4-(1H,3H)-dione], (3-cyclohexyl-6-amino-1-methyl-1,3,5- D [(3-cyclohexyl)-1-methyl-1,3,5-tri- triazine-2,4-(1H,3H)-dione) (calculated azine-2,4,6-(1H,3H,5H)-trione], and E [3- as hexazinone) in the following food (4-hydroxycyclohexyl)-1-methyl-1,3,5- commodities: triazine-2,4,6-(1H,3H,5H)-trione] (cal- culated as hexazinone) in the following Parts per commodities: Commodity million Parts per Cattle, fat ...... 0.1 Commodity milliom Cattle, meat ...... 0 .1 Cattle, meat byproducts ...... 0.1 Sugarcane, cane ...... 0.6 Goat, fat ...... 0 .1 Sugarcane, molasses ...... 4 .0 Goat, meat ...... 0.1 Goat, meat byproducts ...... 0 .1 (d) Indirect or inadvertent residues. Hog, fat ...... 0 .1 [Reserved] Hog, meat ...... 0 .1 Hog, meat byproducts ...... 0 .1 [65 FR 33713, May 24, 2000, as amended at 71 Horse, fat ...... 0 .1 FR 56399, Sept. 27, 2006] Horse, meat ...... 0 .1 Horse, meat byproducts ...... 0 .1 Sheep, fat ...... 0 .1 § 180.399 Iprodione; tolerances for res- Sheep, meat ...... 0.1 idues. Sheep, meat byproducts ...... 0 .1 (a) General. (1) Tolerances are estab- lished for the combined residues of the (3) Tolerances are established for the fungicide iprodione [3-(3,5- combined residues of hexazinone (3- dichlorophenyl)-N-(1-methylethyl)-2,4- cyclohexyl-6-(dimethylamino)-1-meth- dioxo-1-imidazolidinecarboxamide], its yl-1,3,5-triazine-2,4-(1H,3H)-dione) and isomer 3-(1-methylethyl)-N-(3,5- its metabolites; B [3-cyclohexyl-6- dichlorophenyl)-2,4-dioxo-1- (methylamino)-1-methyl-1,3,5-triazine- imidazolidinecarboxamide, and its me- 2,4-(1H,3H)-dione], C [3-(4- tabolite 3-(3,5-dichlorophenyl)-2,4- hydroxycyclohexyl)-6-(methylamino)-1- dioxo-1-imidazolidine-carboxamide in methyl-1,3,5-triazine-2,4-(1H,3H)-dione], or on the following food commodities: C-2 [3-(3-hydroxycyclohexyl)-6- (methylamino)-1-methyl-1,3,5-triazine- Commodity Parts per 2,4-(1H,3H)-dione] and F (3-cyclohexyl- million 6-amino-1-methyl-1,3,5-triazine-2,4- Almond, hulls ...... 2 .0

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Parts per Parts per Commodity million Commodity million

Almond ...... 0.3 Hog, meat ...... 0 .5 Apricot ...... 20 .0 Hog, meat byproducts, except kidney and liver .. 0 .5 Bean, dried, vine hay ...... 90.0 Horse, fat ...... 0 .5 Bean, dry, seed ...... 2 .0 Horse, kidney ...... 3 .0 Bean, forage ...... 90 .0 Horse, liver ...... 3 .0 Bean, succulent ...... 2 .0 Blueberry ...... 15 .0 Horse, meat ...... 0 .5 Boysenberry ...... 15 .0 Horse, meat byproducts, except kidney and liver 0 .5 Broccoli ...... 25 .0 Milk ...... 0.5 Caneberry subgroup 13A ...... 25 .0 Poultry, fat ...... 3.5 Carrot, roots ...... 5.0 Poultry, liver ...... 5 .0 Cherry (sweet), postharvest ...... 20.0 Poultry, meat ...... 1 .0 Cherry, tart ...... 20.0 Poultry, meat byproducts, except liver ...... 1 .0 Cotton, undelinted seed ...... 0 .10 Currant ...... 15.0 Sheep, fat ...... 0 .5 Garlic ...... 0 .1 Sheep, kidney ...... 3.0 Ginseng ...... 2 .0 Sheep, liver ...... 3.0 Ginseng, dried root ...... 4 .0 Sheep, meat ...... 0.5 Grape ...... 60 .0 Sheep, meat byproducts, except kidney and Grape, raisin ...... 300 liver ...... 0 .5 Kiwifruit ...... 10.0 Lettuce ...... 25.0 Nectarine, postharvest ...... 20.0 (b) Section 18 emergency exemptions. Onion, dry bulb ...... 0 .5 [Reserved] Peach, postharvest ...... 20.0 (c) Tolerances with regional registra- Peanut ...... 0 .5 Peanut, hay ...... 150.0 tions. Tolerances with regional reg- Plum, postharvest ...... 20 .0 istration, as defined in § 180.1(n), are es- Plum, prune ...... 20.0 tablished for the combined residues of Potato ...... 0 .5 Raspberry ...... 15 .0 the fungicide iprodione [3-(3,5- Rice, bran ...... 30.0 dichlorophenyl)-N-(1-methylethyl)-2,4- Rice, grain ...... 10 .0 dioxo-1-imidazolidinecarboxamide], its Rice, hulls ...... 50 .0 isomer [3-(1-methylethyl)-N-(3,5- Rice, straw ...... 20 .0 Strawberry ...... 15.0 dichlorophenyl)-2,4-dioxo-1- imidazolidinecarboxamide], and its me- (2) Tolerances are established for the tabolite [3-(3,5-dichlorophenyl)-2,4- combined residues of iprodione [3-(3,5- dioxo-1-imidazolidinecarboxamide] in dichlorophenyl)-N-(1-methylethyl)-2,4- or on the following food commodity: dioxo-1-imidazolidinecarboxamide], its isomer [3-(1-methylethyl)-N-(3,5- Parts per Commodity million dichlorophenyl)-2,4-dioxo-1- imidazolidinecarboxamide, and its me- Chinese mustard ...... 15 .0 tabolites [3-(3,5-dichlorophenyl)-2,4- dioxo-1-imidazolidine-carboxamide] (d) Indirect or inadvertent residues. and [N-(3,5-dichloro-4-hydroxyphenyl)- [Reserved] ureido-carboxamide], all expressed as iprodione equivalents in or on the fol- [48 FR 40385, Sept. 7, 1983] lowing food commodities of animal ori- EDITORIAL NOTE: For FEDERAL REGISTER ci- gin: tations affecting § 180.399, see the List of Sec- tions Affected, which appears in the Finding Commodity Parts per Aids section of the printed volume and on million GPO Access. Cattle, fat ...... 0.5 Cattle, kidney ...... 3 .0 § 180.401 Thiobencarb; tolerances for Cattle, liver ...... 3 .0 residues. Cattle, meat ...... 0 .5 Cattle, meat byproducts, except kidney and liver 0.5 (a) Tolerances are established for the Egg ...... 1 .5 combined residues of the herbicide Goat, fat ...... 0 .5 thiobencarb (S-[(4- Goat, kidney ...... 3 .0 Goat, liver ...... 3.0 chlorophenyl)methyl]diethyl- Goat, meat ...... 0.5 carbamothioate) and its chlorobenzyl Goat, meat byproducts, except kidney and liver 0 .5 and chlorophenyl moiety-containing Hog, fat ...... 0 .5 Hog, kidney ...... 3.0 metabolites in or on the following raw Hog, liver ...... 3 .0 agricultural commodities:

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Part per Parts per Commodity million Commodity million

Cattle, fat ...... 0.2 Horse, fat ...... 0 .2 Cattle, meat byproducts ...... 0.2 Horse, meat ...... 0 .2 Cattle, meat ...... 0 .2 Horse, meat byproducts ...... 0 .2 Egg ...... 0 .2 Milk ...... 0.05 Goat, fat ...... 0 .2 Poultry, fat ...... 0.2 Goat, meat byproducts ...... 0 .2 Poultry, meat ...... 0 .2 Goat, meat ...... 0.2 Poultry, meat byproducts ...... 0.2 Hog, fat ...... 0 .2 Sheep, fat ...... 0 .2 Hog, meat byproducts ...... 0 .2 Sheep, meat ...... 0.2 Hog, meat ...... 0 .2 Sheep, meat byproducts ...... 0 .2 Horse, fat ...... 0 .2 Horse, meat byproducts ...... 0 .2 (b) Section 18 emergency exemptions. Horse, meat ...... 0 .2 Milk ...... 0.05 [Reserved] Poultry, fat ...... 0.2 (c) Tolerances with regional registra- Poultry, meat byproducts ...... 0.2 tions. [Reserved] Poultry, meat ...... 0 .2 (d) Indirect or inadvertent residues. Rice, grain ...... 0 .2 Rice, straw ...... 1 .0 [Reserved] Sheep, fat ...... 0 .2 Sheep, meat byproducts ...... 0 .2 [65 FR 33700, May 24, 2000] Sheep, meat ...... 0.2 § 180.404 Profenofos; tolerances for (b) Tolerances with regional registra- residues. tion, as defined in § 180.1(n), are estab- (a) General. Tolerances are estab- lished for residues of the herbicide lished for combined residues of the in- thiobencarb (S-[(4-chloro- secticide profenofos [O-(4-bromo-2- phenyl)methyl]diethylcarbamothioate) chlorophenyl)-0-ethyl-S-propyl and its chlorobenzyl and chlorophenyl phosphorothioate and its metabolites moiety-containing metabolites in or on converted to 4-bromo-2-chlorophenyl the following raw agricultural com- and calculated as profenofos in or on modities: the following food commodities:

Parts per Commodity Parts per Commodity million million

Celery ...... 0 .2 Cattle, fat ...... 0.05 Endive ...... 0.2 Cattle, meat byproducts ...... 0.05 Lettuce ...... 0.2 Cattle, meat ...... 0 .05 Cotton, undelinted seed ...... 3 .0 Goat, fat ...... 0 .05 [47 FR 6833, Feb. 17, 1982, as amended at 56 Goat, meat byproducts ...... 0 .05 FR 2440, Jan. 23, 1991] Goat, meat ...... 0.05 Horse, fat ...... 0 .05 § 180.403 Thidiazuron; tolerances for Horse, meat byproducts ...... 0 .05 Horse, meat ...... 0 .05 residues. Milk ...... 0.01 (a) General. Tolerances are estab- Sheep, fat ...... 0 .05 Sheep, meat byproducts ...... 0 .05 lished for the combined residues of the Sheep, meat ...... 0.05 defoliant thidiazuron (N-phenyl-N-1,2,3- thiadiazol-5-ylurea) and its aniline con- (b) Section 18 emergency exemptions. taining metabolites in or on the fol- [Reserved] lowing food commodities: (c) Tolerances with regional registra- tions. [Reserved] Parts per Commodity million (d) Indirect or inadvertent residues. [Reserved] Cattle, fat ...... 0.2 Cattle, meat ...... 0 .2 [65 FR 33700, May 24, 2000, as amended at 66 Cattle, meat byproducts ...... 0.2 FR 50833, Oct. 5, 2001; 67 FR 49617, July 31, Cotton, undelinted seed ...... 0 .4 2002] Cotton, hulls ...... 0 .8 Egg ...... 0 .1 Goat, fat ...... 0 .2 § 180.405 Chlorsulfuron; tolerances for Goat, meat ...... 0.2 residues. Goat, meat byproducts ...... 0 .2 (a) General. (1) Tolerances are estab- Hog, fat ...... 0 .2 Hog, meat ...... 0 .2 lished for the combined residues of Hog, meat byproducts ...... 0 .2 chlorsulfuron (2-chloro-N-[(4-methoxy-

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6-methyl-1,3,5-triazin-2- Commodity Parts per yl)aminocarbonyl]benzenesulfonamide) million and its metabolite, 2-chloro-5-hydroxy- Cotton, undelinted seed ...... 0 .5 N-[(4-methoxy-6-methyl-1,3,5-triazin-2- Cotton, hulls ...... 0 .7 yl)aminocarbonyl] benzenesulfonamide Cattle, fat ...... 0.02 Cattle, meat ...... 0 .02 in or on the following raw agricultural Cattle, meat byproducts ...... 0.02 commodities: Goat, fat ...... 0 .02 Goat, meat ...... 0.02 Parts per Goat, meat byproducts ...... 0 .02 Commodity million Hog, fat ...... 0 .02 Hog, meat ...... 0 .02 Barley, grain ...... 0 .1 Hog, meat byproducts ...... 0 .02 Barley, straw ...... 0 .5 Horse, fat ...... 0 .02 Oat, forage ...... 20 .0 Horse, meat ...... 0 .02 Oat, grain ...... 0 .1 Horse, meat byproducts ...... 0 .02 Sheep, fat ...... 0 .02 Oat, straw ...... 0.5 Sheep, meat ...... 0.02 Wheat, forage ...... 20.0 Sheep, meat byproducts ...... 0 .02 Wheat, grain ...... 0 .1 Wheat, straw ...... 0 .5 (b) Section 18 emergency exemptions. (2) Tolerances are established for res- [Reserved] idues of chlorsulfuron (2-chloro-N-[(4- (c) Tolerances with regional registra- methoxy-6-methyl-1,3,5-triazin-2- tions. [Reserved] yl)aminocarbonyl] (d) Indirect or inadvertent residues. benzenesulfonamide) in or on the fol- [Reserved] lowing raw agricultural commodities. [65 FR 33700, May 24, 2000]

Commodity Parts per § 180.407 Thiodicarb; tolerances for million residues. Cattle, fat ...... 0.3 (a) General. Tolerances are estab- Cattle, meat ...... 0 .3 lished for the combined residues of the Cattle, meat byproducts ...... 0.3 ′ Goat, fat ...... 0 .3 insecticide thiodicarb (dimethyl N,N - Goat, meat ...... 0.3 [thiobis[[(methylimino)carbonyloxy]] Goat, meat byproducts ...... 0 .3 bis[ethanimidothioate]) and its me- Grass, forage ...... 11 .0 tabolite methomyl (S-methyl N- Grass, hay ...... 19 .0 [(methylcarbamoyl) Hog, fat ...... 0 .3 Hog, meat ...... 0 .3 oxy]thioacetimidate) in or on the fol- Hog, meat byproducts ...... 0 .3 lowing food commodities or groups. Horse, fat ...... 0 .3 The time-limited tolerances expire and Horse, meat ...... 0 .3 are revoked on the dates listed in the Horse, meat byproducts ...... 0 .3 Milk ...... 0.1 following table: Sheep, fat ...... 0 .3 Expiration/ Sheep, meat ...... 0.3 Commodity Parts per revocation Sheep, meat byproducts ...... 0 .3 million date

(b) Section 18 emergency exemptions. Broccoli ...... 7.0 None Cabbage ...... 7.0 None [Reserved] Cauliflower ...... 7.0 None (c) Tolerances with regional registra- Corn, sweet grain, kernel plus cob tions. [Reserved] with husks removed ...... 2.0 None Cotton, undelinted seed ...... 0.4 None (d) Indirect or inadvertent residues. Cotton, hulls ...... 0.8 None [Reserved] Leafy vegetables (except Brassica vegetables) ...... 35 None [67 FR 52873, Aug. 14, 2002] Soybean, hulls ...... 0.8 None Soybean ...... 0.2 None § 180.406 Dimethipin; tolerances for residues. (b) Section 18 emergency exemptions. (a) General. Tolerances are estab- [Reserved] lished for residues of the harvest (c) Tolerances with regional registra- growth regulant dimethipin (2,3- tions. [Reserved] dihydro-5,6-dimethyl-1,4-dithiin 1,1,4,4- (d) Indirect or inadvertent residues. tetraoxide; CAS Reg. No. 55290–64–7) in [Reserved] or on the following food commodities: [62 FR 44595, Aug. 22, 1997]

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§ 180.408 Metalaxyl; tolerances for res- Commodity Parts per idues. million (a) General. Tolerances are estab- Horse, kidney ...... 0 .4 lished for the combined residues of the Horse, liver ...... 0 .4 Horse, meat ...... 0 .05 fungicide metalaxyl [N-(2,6- Horse, meat byproducts, except kidney and liver 0 .05 dmethylphyenyl)-N-(methoxyacetyl) Lettuce, head ...... 5.0 alanine methylester] and its metabo- Milk ...... 0.02 lites containing the 2,6- Mustard greens ...... 5.0 Onion, dry bulb ...... 3 .0 dimethylaniline moiety, and N-(2-hy- Onion, green ...... 10.0 droxy methyl-6-methylphenyl)-N- Peanut, hay ...... 20.0 (methoxyacetyl)-alanine methyl ester, Peanut, meal ...... 1 .0 each expressed as metalaxyl equiva- Peanut, nut ...... 0 .2 Peanut, hulls ...... 2 .0 lents, in or on the following food com- Pineapple ...... 0.1 modities: Pineapple, fodder ...... 0 .1 Pineapple, forage ...... 0 .1 Commodity Parts per Plum, prune, dried ...... 4.0 million Potato waste, dried, processed ...... 4 .0 Potato, processed (including potato, chips) ...... 4 .0 Alfalfa, forage ...... 6.0 Poultry, fat ...... 0.4 Alfalfa, hay ...... 20.0 Poultry, kidney ...... 0 .4 Almond ...... 0.5 Poultry, liver ...... 0 .4 Almond, hulls ...... 10 .0 Poultry, meat ...... 0 .05 Apple ...... 0.2 Poultry, meat byproducts, except kidney and Apple, wet pomace ...... 0 .4 liver ...... 0 .05 Apricot (dried) ...... 4 .0 Potato ...... 0 .5 Asparagus ...... 7.0 Raspberry ...... 0 .5 Avocado ...... 4 .0 Sheep, fat ...... 0 .4 Beet, garden ...... 0 .1 Sheep, kidney ...... 0.4 Beet, sugar ...... 0 .1 Beet, sugar, molasses ...... 1 .0 Sheep, liver ...... 0.4 Beet, sugar, roots ...... 0 .5 Sheep, meat ...... 0.05 Beet, sugar, tops ...... 10.0 Sheep, meat byproducts, except kidney and Beet, garden, tops ...... 0 .1 liver ...... 0 .05 Blueberry ...... 2 .0 Soybean, hulls ...... 2 .0 Broccoli ...... 2 .0 Soybean, meal ...... 2.0 Brussels sprouts ...... 2 .0 Soybean, seed ...... 1 .0 Cabbage ...... 1 .0 Spinach ...... 10 .0 Cattle, fat ...... 0.4 Strawberry ...... 10.0 Cattle, kidney ...... 0 .4 Sunflower, seed ...... 0.1 Cattle, liver ...... 0 .4 Sunflower, forage ...... 0.1 Cattle, meat ...... 0 .05 Tomato, processed ...... 3 .0 Cattle, meat byproducts, except kidney and liver 0.05 Vegetable, brassica, leafy, group 5, except broc- Cauliflower ...... 1 .0 coli, cabbage, cauliflower, brussels sprouts, Citrus, oil ...... 7.0 and mustard greens ...... 0 .1 Citrus, dried pulp ...... 7 .0 Vegetable, cucurbit, group 9 ...... 1.0 Clover, forage ...... 1.0 Vegetable, fruiting, group 8 ...... 1.0 Clover, hay ...... 2.5 Vegetable, leafy, except brassica, group 4, ex- Cotton, undelinted seed ...... 0 .1 cept spinach ...... 5 .0 Cranberry ...... 4 .0 Vegetable, leaves of root and tuber, group 2 ..... 15 .0 Egg ...... 0 .05 Vegetable, legume, cannery waste ...... 5 .0 Fruit, citrus ...... 1 .0 Vegetable, legume, foliage ...... 8.0 Fruit, stone, group 12 ...... 1 .0 Vegetable, legume, group 6 ...... 0 .2 Ginseng ...... 3 .0 Vegetable, root and tuber, group 1 ...... 0 .5 Goat, fat ...... 0 .4 Walnut ...... 0 .5 Goat, kidney ...... 0 .4 Goat, liver ...... 0.4 (b) Section 18 emergency exemptions. Goat, meat ...... 0.05 Goat, meat byproducts, except kidney and liver 0 .05 [Reserved] Grain, cereal (except wheat, barley, and oats) ... 0 .1 (c) Tolerances with regional registra- Grain, crop ...... 0 .1 tions. Tolerances with regional reg- Grape ...... 2 .0 Grape, raisin ...... 6 .0 istration (refer to § 180.1(n)) are estab- Grass, forage ...... 10 .0 lished for the combined residues of the Grass, hay ...... 25 .0 fungicide metalaxyl [N-(2,6- Hog, fat ...... 0 .4 dimethylphenyl)-N-(methoxyacetyl) al- Hog, kidney ...... 0.4 Hog, liver ...... 0 .4 anine methyl ester] and its metabolites Hog, meat ...... 0 .05 containing the 2,6-dimethylaniline Hog, meat byproducts, except kidney and liver .. 0 .05 moiety, and N-(2-hydroxy methyl-6- Hop, dried cones ...... 20 Hop, vines ...... 2 .0 methyl)-N-(methoxyacetyl)-alanine Horse, fat ...... 0 .4 methylester, each expressed as

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metalaxyl, in or on the following raw Commodity Parts per agricultural commodity: million Goat, kidney ...... 2 .0 Parts per Commodity million Goat, liver ...... 2.0 Goat, meat byproducts ...... 0 .2 Papaya ...... 0 .1 Hog, fat ...... 0 .2 Hog, kidney ...... 2.0 Hog, liver ...... 2 .0 (d) Indirect or inadvertent tolerances. Hog, meat byproducts ...... 0 .2 Tolerances are established for indirect Horse, fat ...... 0 .2 or inadvertent residues of metalaxyl in Horse, kidney ...... 2 .0 Horse, liver ...... 2 .0 or on the food commodities when Horse, meat byproducts ...... 0 .2 present therein as a result of the appli- Poultry, fat ...... 0.2 cation of metalaxyl to growing crops Sheep, fat ...... 0 .2 Sheep, kidney ...... 2.0 listed in paragraph (a) of this section Sheep, liver ...... 2.0 and other non-food crops to read as fol- Sheep, meat byproducts ...... 0 .2 lows: Sorghum, grain, grain ...... 8 .0

Commodity Part per (b) Section 18 emergency exemptions. million [Reserved] Barley, grain ...... 0 .2 (c) Tolerances with regional registra- Barley, milling fractions ...... 1.0 tions. [Reserved] Barley, straw ...... 2 .0 Grain, cereal group (except wheat, barley, and (d) Indirect or inadvertent residues. oats), fodder ...... 1 .0 [Reserved] Grain, cereal group (except wheat, barley, and oats), forage ...... 1 .0 [65 FR 33714, May 24, 2000, as amended at 67 Grain, cereal group (except wheat, barley, and FR 41807, June 19, 2002; 67 FR 49617, July 31, oats), straw ...... 1 .0 2002; 70 FR 44492, Aug. 3, 2005] Oat, forage ...... 2 .0 Oat, grain ...... 0 .2 § 180.410 Triadimefon; tolerances for Oat milling fractions ...... 1.0 Oat, straw ...... 2.0 residues. Wheat, forage ...... 2 .0 (a) General. Tolerances are estab- Wheat, grain ...... 0 .2 Wheat, milling fractions ...... 1 .0 lished for the combined residues of the Wheat, straw ...... 2 .0 fungicide 1-(4-chlorophenoxy)-3,3-di- methyl-1(1H-1,2,4-triazol-1-yl)-2-buta- [65 FR 33700, May 24, 2000, as amended at 72 none and its metabolites containing FR 35666, June 29, 2007] chlorophenoxy and triazole moieties (expressed as the fungicide) in or on § 180.409 Pirimiphos-methyl; toler- the following raw agricultural com- ances for residues. modities: (a) General. Tolerances are estab- Parts per lished for the combined residues of the Commodity million insecticide pirimiphos-methyl, O-[2- diethylamino-6-methyl-4-pyrimidinyl) Apple ...... 1.0 Apple, dry pomace ...... 4.0 O,O-dimethyl phosphorothioate, the Apple, wet pomace ...... 4 .0 metabolite O-[2-ethylamino-6-methyl- Barley, milled fractions (except flour) ...... 4 .0 pyrimidin-4-yl) O,O-dimethyl Beet, sugar ...... 0 .5 Beet, sugar, tops ...... 3.0 phosphorothioate and, in free and con- Cattle, fat ...... 1.0 jugated form, the metabolites 2- Cattle, meat ...... 1 .0 diethylamino-6-methyl-pyrimidin-4-ol), Cattle, meat byproducts ...... 1.0 Chickpea, seed ...... 0 .1 2-ethylamino-6-methyl-pyrimidin-4-ol, Cucurbits ...... 0 .3 and 2-amino-6-methyl-pyrimidin-4-ol in Egg ...... 0 .04 or on the following food commodities: Grape ...... 1 .0 Goat, fat ...... 1 .0 Parts per Goat, meat ...... 1.0 Commodity million Goat, meat byproducts ...... 1 .0 Grape pomace (wet and dry) ...... 3.0 Cattle, fat ...... 0.2 Grape, raisin, waste ...... 7 .0 Cattle, kidney ...... 2 .0 Grass, forage ...... 0 .2 Cattle, liver ...... 2 .0 Grass, seed screenings ...... 145.0 Cattle, meat ...... 0 .2 Grass, straw, grown for seed ...... 105 .0 Cattle, meat byproducts ...... 0.2 Hog, fat ...... 0 .04 Corn ...... 8.0 Hog, meat ...... 0 .04 Goat, fat ...... 0 .2 Hog, meat byproducts ...... 0 .04

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Parts per Parts per Commodity million Commodity million

Horse, fat ...... 1 .0 Cattle, meat byproducts ...... 05 Horse, meat ...... 1 .0 Cotton, undelinted seed ...... 1 Horse, meat byproducts ...... 1 .0 Cotton, oil ...... 0 .2 Milk ...... 0.04 Egg ...... 05 Nectarine ...... 4 .0 Pear ...... 1 .0 Goat, fat ...... 05 Pineapple, fresh ...... 3 .0 Goat, meat ...... 05 Poultry, fat ...... 0.04 Goat, meat byproducts ...... 05 Poultry, meat ...... 0 .04 Hog, fat ...... 05 Poultry, meat byproducts ...... 0.04 Hog, meat ...... 05 Sheep, fat ...... 1 .0 Hog, meat byproducts ...... 05 Sheep, meat ...... 1.0 Horse, fat ...... 05 Sheep, meat byproducts ...... 1 .0 Horse, meat ...... 05 Wheat, forage ...... 15.0 Wheat, grain ...... 1 .0 Horse, meat byproducts ...... 05 Wheat, milled fractions (except flour) ...... 4.0 Milk ...... 05 Wheat, straw ...... 5 .0 Poultry, fat ...... 05 Poultry, meat ...... 05 (b) Section 18 emergency exemptions. Poultry, meat byproducts ...... 05 [Reserved] Sheep, fat ...... 05 Sheep, meat ...... 05 (c) Tolerances with regional registra- Sheep, meat byproducts ...... 05 tions. Tolerances with regional reg- Soybean ...... 1.0 istration are established for the com- Soybean, meal ...... 2.0 bined residues of the fungicide 1-(4- Soybean, refined oil ...... 2 .0 chlorophenoxy)-3,3-dimethyl-1(1H-1,2,4- triazol-l-yl)-2-butanone and its metabo- (2) Tolerances are established for res- lites containing chlorophenoxy and tri- idues of the resolved isomer of azole moieties (expressed as the fun- fluazifop, (R)-2-[4-[[5-(trifluoromethyl)- gicide) in or on the following raw agri- 2-pyridinyl]oxy]phenoxy]propanoic cultural commodities: acid, both free and conjugated and of fluazifop-P-butyl, butyl(R)-2-[4-[[5- Parts per Commodity million (trifluoromethyl)-2- pyridinyl]oxy]phenoxy]propanoate, all Raspberry ...... 2 .0 expressed as fluazifop, in or on the food commodity: (d) Indirect or inadvertent residues. [Reserved] Parts per Commodity million [49 FR 10548, Mar. 21, 1984; 49 FR 19654, May 9, 1984, as amended at 50 FR 1052, Jan. 9, 1985; Carrot, roots ...... 2.0 51 FR 15324, Apr. 23, 1986; 61 FR 39541, July 29, Endive ...... 6.0 1996; 61 FR 63725, Dec. 2, 1996; 62 FR 47568, Fruit, stone ...... 0 .05 Sept. 10, 1997; 64 FR 5191, Feb. 3, 1999; 67 FR Nut, macadamia ...... 0.1 35048, May 17, 2002; 67 FR 41807, June 19, 2002] Onion (bulb) ...... 0 .5 Pecan ...... 0 .05 § 180.411 Fluazifop-butyl; tolerances Spinach ...... 6 .0 for residues. Sweet potato, roots ...... 0 .5 (a) General. (1) Tolerances are estab- (b) Section 18 emergency exemptions. lished for residues of the herbicide [Reserved] fluazifop-butyl (#)-2-[4-[5- (c) Tolerances with regional registra- (trifluoromethyl)-2- tions. (1) Tolerances with regional reg- pyridinyl]oxy]phenoxy propanoic acid istration are established for residues of (fluazifop), both free and conjugated fluazifop-butyl (#)-2-[4-[5- and of (#)-2-[4-[5-(trifluoromethyl)-2- (trifluoromethyl)-2- pyridinyl]oxy]phenoxy propanoate pyridinyl]oxy]phenoxy propanoic acid (fluazifop-butyl), all expressed as (fluazifop), both free and conjugated fluazifop, in or on the following food and of (#)-butyl-2-[4-[5- commodities: (trifluoromethyl)-2- pyridinyl]oxy]phenoxy propanoate Commodity Parts per million (fluazifop-butyl), all expressed as Cattle, fat ...... 0.05 fluazifop, in or on the following food Cattle, meat ...... 05 commodities:

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Parts per Expiration/ Commodity million Commodity Parts per Revocation million Date Pepper, tabasco ...... 1 .0 Citrus, dried pulp ...... 1.5 None Clover, forage ...... 35.0 None (2) Tolerances with regional registra- Clover, hay ...... 50.0 None tion, see § 180.1(n), are established for Coriander ...... 4.0 None residues of the resolved isomer of the Corn, field, grain ...... 0.5 None Corn fodder ...... 2.5 None herbicide fluazifop, (R)-2-[4-[[5- Corn forage ...... 2.0 None (trifluoromethyl)-2-pyridinyl]- Corn, sweet, forage ...... 3.0 None oxy]phenoxy] propanoic acid, both free Corn, sweet, kernel plus cob with and conjugated and of fluazifop-P- husks removed ...... 0.4 None Corn, sweet stover ...... 3.5 None butyl, butyl[R]-2-[4-[[5- Cotton, seed, soapstock ...... 15 None (trifluoromethyl)-2- Cotton, undelinted seed ...... 5.0 None pyridinyl]oxy]phenoxy] propanoate, all Cranberry ...... 2.0 None Egg ...... 2.0 None expressed as fluazifop, in or on the food Flax, meal ...... 7 None commodities: Flax, seed ...... 5.0 None Flax, straw ...... 2.0 None Parts per Fruit, citrus ...... 0.5 None Commodity million Fruit, pome ...... 0.2 None Goat, fat ...... 0.2 None Asparagus ...... 3.0 Goat, meat byproducts ...... 1.0 None Coffee, bean ...... 0 .1 Goat, meat ...... 0.2 None Rhubarb ...... 0 .5 Grape ...... 1.0 None Grape, raisin ...... 2.0 None Hog, fat ...... 0.2 None (d) Indirect or inadvertent residues. Hog, meat byproducts ...... 1.0 None [Reserved] Hog, meat ...... 0.2 None Horse, fat ...... 0.2 None [65 FR 33714, May 24, 2000] Horse, meat byproducts ...... 1.0 None Horse, meat ...... 0.2 None § 180.412 Sethoxydim; tolerances for Juneberry ...... 5.0 None residues. Lentil, seed ...... 30.0 None Lingonberry ...... 5.0 None (a) General. Tolerances are estab- Milk ...... 0.5 None lished for combined residues of the her- Nectarine ...... 0.2 None Nut, tree, group 14 ...... 0.2 None bicide 2-[1-(ethoxyimino)butyl]-5-[2- Peach ...... 0.2 None (ethylthio)propyl]-3-hydroxy-2-cyclo- Peanut ...... 25.0 None hexen-1-one (CAS Reg. No. 74051–80–2) Peanut, soapstock ...... 75.0 None Pea, dry, seed ...... 40.0 None and its metabolites containing the 2- Pea, field, vines ...... 20.0 None cyclohexen-1-one moiety (calculated as Pea, field, hay ...... 40.0 None the herbicide) in or on the following Pea, succulent ...... 10.0 None Peppermint, tops (stems and commodities: leaves) ...... 30.0 None Pistachio ...... 0.2 None Parts per Expiration/ Potato flakes ...... 8.0 None Commodity Revocation Potato granules ...... 8.0 None million Date Potato waste, processed (wet and Alfalfa, forage ...... 40.0 None dry) ...... 8.0 None Alfalfa, hay ...... 40.0 None Poultry, fat ...... 0.2 None Almond, hulls ...... 2.0 None Poultry, meat byproducts ...... 2.0 None Apple, dry pomace ...... 0.8 None Poultry, meat ...... 0.2 None Salal ...... 5.0 None Apple, wet pomace ...... 0.8 None Safflower ...... 15.0 None Apricot ...... 0.2 None Sheep, fat ...... 0.2 None Asparagus ...... 4.0 None Sheep, meat byproducts ...... 1.0 None Bean, dry, seed ...... 20.0 None Sheep, meat ...... 0.2 None Bean, forage ...... 15.0 None Soybean, hay ...... 10.0 None Bean, hay ...... 50.0 None Soybean ...... 16.0 None Bean, succulent ...... 15.0 None Spearmint, tops (stems and leaves) 30.0 None Beet, sugar, molasses ...... 10.0 None Strawberry ...... 10.0 None Beet, sugar, tops ...... 3.0 None Sunflower meal ...... 20.0 None Blueberry ...... 4.0 None Sunflower, seed ...... 7.0 None Caneberry subgroup 13A ...... 5.0 None Tomato, concentrated products ...... 24 None Canola/rapeseed ...... 35.0 None Tomato, dry pomace ...... 12.0 None Canola/rapeseed, meal ...... 40.0 None Vegetable, brassica, leafy, group 5 5.0 None Cattle, fat ...... 0.2 None Vegetable, bulb, group 3 ...... 1.0 None Cattle, meat byproducts ...... 1.0 None Vegetable, cucurbit, group 9 ...... 4.0 None Cattle, meat ...... 0.2 None Vegetable, fruiting ...... 4.0 None Cherry, sweet ...... 0.2 None Vegetable, leafy, except brassica, Cherry, tart ...... 0.2 None group 4 ...... 4.0 None Citrus, molasses ...... 1.5 None

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(b) Section 18 emergency exemptions. its metabolites, 3-[2-(2,4- (c) Tolerances with regional registra- dichlorophenyl)-2-(2,3- tion. Tolerances with regional registra- dihydroxypropoxy)ethyl]-2,4- tion, as defined in § 180.1(n), are estab- imidazolidinedione (FK772) and 3-[2- lished for the combined residues of the (2,4-dichlorophenyl)-2-(hydroxy)]-2,4- herbicide 2-[1-(ethoxyimino)butyl]-5-[2- imidazolidinedione (FK284), in or on (ethylthio)propyl]-3-hydroxy-2-cyclo- the following food commodities: hexen-1-one) and its metabolites con- Parts per taining the 2-cyclohexen-1-one moiety Commodity million (calculated as the herbicide) in or on the following commodities: Cattle, fat ...... 0.01 Cattle, meat ...... 0 .01 Expiration/ Cattle, meat byproducts ...... 0.2 Commodity Parts per Revocation Goat, fat ...... 0 .01 million Date Goat, meat ...... 0.01 Goat, meat byproducts ...... 0 .2 Artichoke, globe ...... 5.0 None Horse, fat ...... 0 .01 Rhubarb ...... 0.3 None Horse, meat ...... 0 .01 Horse, meat byproducts ...... 0 .2 (d) Indirect and inadvertent residues. Milk ...... 0.02 Sheep, fat ...... 0 .01 [Reserved] Sheep, meat ...... 0.01 Sheep, meat byproducts ...... 0 .2 [62 FR 17740, Apr. 11, 1997, as amended at 62 FR 44565, Aug. 22, 1997; 63 FR 54073, Oct. 8, 1998; 64 FR 32196, June 16, 1999; 64 FR 56703, (b) Section 18 emergency exemptions. Oct. 21, 1999; 66 FR 51594, Oct. 10, 2001; 66 FR [Reserved] 65452, Dec. 19, 2001; 67 FR 35048, May 17, 2002; (c) Tolerances with regional registra- 67 FR 41807, June 19, 2002; 67 FR 42397, June tions. [Reserved] 21, 2002; 68 FR 55869, Sept. 29, 2003; 72 FR 8922, (d) Indirect or inadvertent residues. Feb. 28, 2007] [Reserved] EDITORIAL NOTE: At 72 FR 8922, Feb. 28, [65 FR 33715, May 24, 2000, as amended at 67 2007, in § 180.412, commodities were added to FR 46893, July 17, 2002; 71 FR 54434, Sept. 15, the table in paragraph (a), however, the 2006] amendment could not be done due to insuffi- cient data. § 180.414 Cyromazine; tolerances for residues. § 180.413 Imazalil; tolerances for resi- dues. (a) General. (1) Tolerances are estab- (a) General. (1) Tolerances are estab- lished for residues of the insecticide lished for the combined residues of the cyromazine (N-cyclopropyl-1,3,5-tri- fungicide imazalil, 1-[2-(2,4- azine-2,4,6-triamine) in or on the fol- dichlorophenyl)-2-(2- lowing raw agricultural commodities: propenyloxy)ethyl]-1H-imidazole, and Parts per its metabolite, 1-(2,4-dichlorophenyl)-2- Commodity million (1H-imidazole-1-yl)-1-ethanol, in or on Bean, dry, except cowpea ...... 3 .0 the following food commodities: Bean, lima ...... 1 .0 Broccoli ...... 1 .0 Commodity Parts per Cabbage, abyssinian ...... 10 .0 million Cabbage, seakale ...... 10.0 Cattle, fat ...... 0.05 Banana ...... 3.0 Cattle, kidney ...... 0 .2 Barley, grain ...... 0 .1 Cattle, meat ...... 0 .05 Barley, hay ...... 0 .5 Cattle, meat byproducts, except kidney ...... 0.05 Barley, straw ...... 0 .5 Egg ...... 0 .25 Citrus, dried pulp ...... 25 .0 Garlic, bulb ...... 0.2 Citrus, oil ...... 200 .0 Garlic, great-headed, bulb ...... 0 .2 Fruit, citrus, postharvest ...... 10.0 Goat, fat ...... 0 .05 Wheat, forage ...... 0 .5 Goat, kidney ...... 0 .2 Wheat, grain ...... 0 .1 Goat, meat ...... 0.05 Wheat, hay ...... 0 .5 Goat, meat byproducts, except kidney ...... 0 .05 Wheat, straw ...... 0 .5 Hanover salad, leaves ...... 10 .0 Hog, fat ...... 0 .05 (2) Tolerances are established for the Hog, kidney ...... 0.2 combined residues of the fungicide Hog, meat ...... 0 .05 Hog, meat byproducts, except kidney ...... 0 .05 imazalil, 1-[2-(2,4-dichlorophenyl)-2-(2- Horse, fat ...... 0 .05 propenyloxy)ethyl]-1H-imidazole, and Horse, kidney ...... 0 .2

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(v) Residues of cyromazine are not to Commodity Parts per million exceed 5.0 parts per million (ppm) in Horse, meat ...... 0 .05 poultry feed. Horse, meat byproducts, except kidney ...... 0 .05 (b) Section 18 emergency exemptions. Leek ...... 3 .0 [Reserved] Mango1 ...... 0 .3 (c) Tolerances with regional registra- Milk ...... 0.05 Mushroom ...... 1 .0 tions. [Reserved] Onion, dry bulb ...... 0 .2 (d) Indirect or inadvertent residues. Onion, green ...... 3 .0 Tolerances are established for the indi- Onion, potato ...... 3 .0 rect or inadvertent residues of Onion, tree ...... 3.0 cyromazine (N-cyclopropyl-1,3,5-tri- Onion, welsh ...... 3.0 Pepper ...... 1 .0 azine-2,4,6-triamine), in or on the raw Potato ...... 0 .8 agricultural commodities when present Poultry, fat (from chicken layer hens and chick- therein as a result of the application of en breeder hens only) ...... 0 .05 cyromazine to growing crops listed in Poultry, meat (from chicken layer hens and chicken breeder hens only) ...... 0 .05 paragraph (a)(1) of this section. Poultry, meat byproducts (from chicken layer hens and chicken breeder hens only) ...... 0 .05 Parts per Commodity million Rakkyo, bulb ...... 0.2 Shallot, bulb ...... 0 .2 Cotton, undelinted seed ...... 0 .1 Shallot, fresh leaves ...... 3 .0 Corn, sweet, kernel plus cob with husks re- Sheep, fat ...... 0 .05 moved ...... 0 .5 Sheep, kidney ...... 0.2 Corn, sweet, forage ...... 0 .5 Sheep, meat ...... 0.05 Corn, sweet, stover ...... 0 .5 Sheep, meat byproducts, except kidney ...... 0 .05 Radish, root ...... 0 .5 Tomato ...... 0.5 Radish, tops (leaves) ...... 0 .5 Turnip, greens ...... 10.0 Vegetable, brassica, leafy, group 5, except broc- coli ...... 10 .0 [65 FR 25860, May 4, 2000, as amended at 67 Vegetable, leafy, except brassica, group 4 ...... 7 .0 FR 72593, Dec. 6, 2002; 68 FR 55269, Sept. 24, Vegetable, cucurbit, group 9 ...... 1.0 2003] 1There are no U.S. registrations on mango as of May 4, 2000. § 180.415 Aluminum tris (O- ethylphosphonate); tolerances for (2) The additive cyromazine (N- residues. cyclopropyl-1,3,5-triazine-2,4,6-tri- (a) General. Tolerances are estab- amine) may be safely used in accord- lished for residues of the fungicide alu- ance with the following prescribed con- minum tris(O-ethylphosphonate) in or ditions: on the following food commodities: (i) It is used as a feed additive only in feed for chicken layer hens and chicken Expiration/ Commodity Parts per Revocation breeder hens at the rate of not more million Date than 0.01 pound of cyromazine per ton of poultry feed. Avocado ...... 25 None Banana ...... 3.0 None (ii) It is used for control of flies in Blueberry ...... 40 12/31/00 manure of treated chicken layer hens Bushberry subgroup 13B ...... 40 None and chicken breeder hens. Caneberry subgroup 13A ...... 0.1 None Cranberry ...... 0.5 None (iii) Feeding of cyromazine-treated Fruit, citrus, group 10 ...... 5.0 None feed must stop at least 3 days (72 Fruit, pome ...... 10 None hours) before slaughter. If the feed is Ginseng ...... 0.1 None Hop, dried cones ...... 45 None formulated by any person other than Juneberry ...... 40 None the end user, the formulator must in- Leafy vegetables (except brassica form the end user, in writing, of the 3– vegetables) group ...... 100 None Lingonberry ...... 40 None day (72 hours) preslaughter interval. Nut, macadamia ...... 0.20 None (iv) To ensure safe use of the addi- Onion, green ...... 10.0 None tive, the labeling of the pesticide for- Pea, succulent ...... 0.3 None mulation containing the feed additive Pineapple ...... 0.1 None Pineapple, fodder ...... 0.1 None shall conform to the labeling which is Pineapple, forage ...... 0.1 None registered by the U.S. Environmental Onion, dry bulb ...... 0.5 None Protection Agency, and the additive Salal ...... 40 None Strawberry ...... 75 None shall be used in accordance with this Tomato ...... 3 None registered labeling. Turnip, greens ...... 40 None

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Expiration/ § 180.417 Triclopyr; tolerances for resi- Commodity Parts per Revocation million Date dues. (a) General. (1) Tolerances are estab- Turnip, roots ...... 15 None Vegetable, brassica, leafy, group 5 60 None lished for the combined residues of the Vegetable, cucurbit, group 9 ...... 15 None herbicide triclopyr ((3,5,6-trichloro-2- pyridinyl)oxy)acetic acid and its me- (b) Section 18 emergency exemptions. tabolites 3,5,6-trichloro-2-pyridinol and [Reserved] 2-methoxy-3,5,6-trichloropyridine in or (c) Tolerances with regional registra- on the following raw agricultural com- tions. Tolerances with regional reg- modities: istration, as defined in § 180.1(n), are es- Parts per tablished for residues of the fungicide Commodity million aluminum tris (O-ethylphosphonate) in or on the following raw agricultural Fish ...... 3 .0 commodities: Grass, forage ...... 500 Grass, forage, hay ...... 500 Shellfish ...... 3 .5 Parts per Commodity million (2) Tolerances are established for the Asparagus ...... 0.1 combined residues of the herbicide Grape ...... 10 triclopyr ((3,5,6-trichloro-2- (d) Indirect or inadvertent residues. pyridinyl)oxy)acetic acid and its me- [Reserved] tabolite 3,5,6-trichloro-2-pyridinol in or on the following raw agricultural com- [64 FR 36801, July 8, 1999, as amended at 64 modities: FR 37875, July 14, 1999; 65 FR 50438, Aug. 18, 2000; 67 FR 55346, Aug. 29, 2002; 68 FR 11335, Commodity Parts per Mar. 10, 2003; 70 FR 7047, Feb. 10, 2005] million Egg ...... 0 .05 § 180.416 Ethalfluralin; tolerances for Meat, fat, and meat byproducts, except kidney residues. and liver, of cattle, goat, hog, horse, and (a) General. Tolerances are estab- sheep ...... 0 .05 Meat, fat, and meat byproducts, except kidney, lished for residues of the herbicide of poultry ...... 0 .1 ethalfluralin [N-ethyl-N-(2-methyl-2- Milk ...... 0.01 propenyl)-2,6-dinitro-4- Liver and kidney of cattle, goat, hog, horse, and (trifluoromethyl)benzenamine] in or on sheep ...... 0 .5 Rice, grain ...... 0 .3 the following raw agricultural com- Rice, straw ...... 10 .0 modities: (b) Section 18 emergency exemptions. Parts per Commodity million [Reserved] (c) Tolerances with regional registra- Bean, dry, seed ...... 0 .05 tions. [Reserved] Canola, seed ...... 0 .05 Peanut ...... 0 .05 (d) Indirect or inadvertent residues. Pea, dry, seed ...... 0 .05 [Reserved] Safflower, seed ...... 0 .05 Soybean ...... 0.05 [50 FR 18486, May 1, 1985, as amended at 55 Sunflower, seed ...... 0.05 FR 26440, June 28, 1990; 60 FR 4095, Jan. 20, Vegetable, cucurbit, group 9 ...... 0.05 1995; 62 FR 46894, Sept. 5, 1997; 63 FR 45406, Aug. 26, 1998; 67 FR 35048, May 17, 2002; 67 FR (b) Section 18 emergency exemptions. 58725, Sept. 18, 2002] [Reserved] (c) Tolerances with regional registra- § 180.418 Cypermethrin and an isomer tions. [Reserved] zeta-cypermethrin; tolerances for (d) Indirect or inadvertent residues. residues. [Reserved] (a) General. (1) Tolerances are estab- lished for residues of the insecticide [49 FR 391, Jan. 4, 1984, as amended at 50 FR cypermethrin (±)alpha cyano-(3- 4976, Feb. 5, 1985; 52 FR 11262, Apr. 8, 1987; 62 ± FR 66014, Dec. 17, 1997; 64 FR 5191, Feb. 3, phenoxyphenyl)methyl( )cis,trans- 1999; 64 FR 54782, Oct. 8, 1999; 66 FR 37598, 3(2,2-dichloroethenyl-2,2- July 19, 2001; 66 FR 41454, Aug. 8, 2001; 67 FR dimethylcyclopropanecarboxylate in or 2342, Jan. 17, 2002; 67 FR 49617, July 31, 2002] on the following commodities:

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Parts per Parts per Commodity million Commodity million

Brassica, head and stem, subgroup 5A ...... 2 .0 Goat, meat byproducts ...... 0 .05 Cattle, fat ...... 0.05 Goat, meat ...... 0.2 Cattle, meat byproducts ...... 0.05 Grain, aspirated fractions ...... 10.0 Cattle, meat ...... 0 .05 Grape ...... 2 Cotton, undelinted seed ...... 0 .5 Grass, forage, group 17 ...... 10 Goat, fat ...... 0 .05 Grass, hay, group 17 ...... 35 Goat, meat byproducts ...... 0 .05 Hog, fat ...... 1 .00 Goat, meat ...... 0.05 Hog, meat byproducts ...... 0 .05 Hog, fat ...... 0 .05 Hog, meat ...... 0 .2 Hog, meat byproducts ...... 0 .05 Horse, fat ...... 1 .00 Hog, meat ...... 0 .05 Horse, meat byproducts ...... 0 .05 Horse, fat ...... 0 .05 Horse, meat ...... 0 .2 Horse, meat byproducts ...... 0 .05 Leafy vegetables except, Brassica ...... 10.00 Horse, meat ...... 0 .05 Lettuce, head ...... 10.00 Lettuce, head ...... 10.0 Milk, fat (reflecting 0.10 in whole milk) ...... 2 .50 Milk ...... 0.05 Nut, tree, group 14 ...... 0 .05 Onion, dry bulb ...... 0 .10 Onion, dry bulb ...... 0 .10 Onion, green ...... 6 .0 Onion, green ...... 3 .00 Pecan ...... 0 .05 Peanut ...... 0 .05 Sheep, fat ...... 0 .05 Pecan ...... 0 .05 Sheep, meat byproducts ...... 0 .05 Poultry, fat ...... 0.05 Sheep, meat ...... 0.05 Poultry, meat byproducts ...... 0.05 Vegetable, brassica, leafy group 5 ...... 14 .0 Poultry, meat ...... 0 .05 Rapeseed ...... 0 .2 (2) Tolerances are established for res- Rice, grain ...... 1 .50 Rice, hulls ...... 6 .00 idues of the insecticide Z-cypermethrin Rice, straw ...... 2 .00 (S-cyano(3-phenoxyphenyl) methyl Sheep, fat ...... 1 .00 (±))(cis-trans 3-(2,2-dichloroethenyl)-2,2 Sheep, meat byproducts ...... 0 .05 Sheep, meat ...... 0.2 dimethylcyclopropanecarboxylate and Sorghum, forage ...... 0 .1 its inactive R-isomers in or on the fol- Sorghum, grain ...... 0 .5 lowing raw agricultural commodities: Sorghum, grain, stover ...... 5 .0 Soybean, seed ...... 0 .05 Parts per Succulent, shelled pea and bean (Crop sub- Commodity million group 6B) ...... 0 .1 Sugarcane, cane ...... 0.60 Alfalfa, hay ...... 15.00 Sunflower ...... 0 .2 Alfalfa, forage ...... 5.00 Sunflower, refined oil ...... 0.5 Alfalfa, seed ...... 0 .50 Turnip, greens ...... 14 Almond, hulls ...... 6 Vegetable, brassica, leafy group 5 ...... 14 .00 Animal feed, nongrass, group 18, forage ...... 8 Vegetable, cucurbit, group 9 ...... 0.2 Animal feed, nongrass, group 18, hay ...... 40 Vegetable, fruiting, except cucurbits (Crop Beet, sugar, roots ...... 0 .05 Group 8) ...... 0 .2 Beet, sugar, tops ...... 0.20 Vegetable, root and tuber, group 1, except Berry, group 13 ...... 0 .8 sugar beet ...... 0 .1 Brassica, head and stem, subgroup 5A ...... 2 .00 Wheat, forage ...... 3 .0 Cabbage ...... 2 .00 Wheat, grain ...... 0 .2 Cattle, fat ...... 1.00 Wheat, hay ...... 6 .0 Cattle, meat byproducts ...... 0.05 Wheat, straw ...... 7 .0 Cattle, meat ...... 0 .2 Cilantro, leaves ...... 10 (b) Section 18 emergency exemptions. Corn, field, grain ...... 0 .05 Corn, pop, grain ...... 0.05 Time-limited tolerances are estab- Corn, field, forage ...... 0 .20 lished for combined residues of zeta- Corn, field, stover ...... 3 .00 cypermethin, methyl(E)-2-(2-(6-(2- Corn, pop, stover ...... 3.00 Corn, sweet, kernel plus cob with husks re- cyanophenoxy)pyrimidin-4- moved ...... 0 .05 yloxy)phenyl)-3-methoxyacrylate a and Corn, sweet, forage ...... 15 .00 the Z isomer of zeta-cypermethin, Corn, sweet, stover ...... 15.00 methyl (Z)-2-(2-(6-(2- Cotton, undelinted seed ...... 0 .5 Dried, shelled pea and bean, except soybean cyanophenoxy)pyrimidin-4- (Crop subgroup 6C) ...... 0 .05 yloxy)phenyl)-3-methoxyacrlate in con- Edible podded legume vegetables (Crop sub- nection with the use of the pesticide group 6A) ...... 0.5 Egg ...... 0 .05 under section 18 emergency exemptions Food/feed items (other than those covered by a granted by EPA in or on the food com- higher tolerance as a result of use on growing modities in the following table. The crops) in food/feed handling establishments ... 0.05 tolerances expire and will be revoked Fruit, pome, group 11 ...... 2 Fruit, stone, group 12 ...... 1 by EPA on the date specified in the Goat, fat ...... 1 .00 table.

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Expiration/ Parts per Commodity Parts per revocation Food million million date Barley milling fractions (except flour) ...... 90 Flax, meal ...... 0.2 6/30/2008 Oat milling fractions (except flour) ...... 130 Flax, seed ...... 0.2 6/30/2008 Rice milling fractions (except flour) ...... 30 Mustard, seed ...... 1.0 6/30/2005 Sorghum, grain, bran ...... 90 Wheat milling fractions (except flour) ...... 30 (c) Tolerances with regional registra- tions. [Reserved] (b) Section 18 emergency exemptions. (d) Indirect or inadvertent residues. [Reserved] [Reserved] (c) Tolerances with regional registra- tions. [Reserved] [62 FR 63235, 63243, Nov. 26, 1997, as amended (d) Indirect or inadvertent residues. at 63 FR 48586, Sept. 11, 1998; 66 FR 47993, [Reserved] Sept. 17, 2001; 67 FR 6430, Feb. 12, 2002; 67 FR 56495, Sept. 4, 2002; 69 FR 71717, Dec. 10, 2004; [65 FR 33715, May 24, 2000] 71 FR 78382, Dec. 29, 2006] § 180.420 Fluridone; tolerances for res- § 180.419 Chlorpyrifos-methyl; toler- idues. ances for residues. (a) Tolerances are established for the (a) General. (1) Tolerances are estab- combined residues (free and bound) of lished for the combined residues of the the herbicide fluridone (1-methyl-3- insecticide chlorpyrifos-methyl [O,-O,- phenyl-5-[3-trifluoromethyl)phenyl]- dimethyl O-(3,5,6-trichloro-2-pyridyl)] 4(1H)-5-[3-(trifluoromethyl)phenyl]- phosphorothioate and its metabolite 4(1H)-pyridinone) in fish and crayfish (3,5,6-trichloro-2-pyridinol) in or on the at 0.5 part per million. following food commodities: (b) Tolerances are established for res- idues of the herbicide fluridone in the Parts per following raw agricultural commod- Commodity million ities: Barley, grain ...... 6 .0 Cattle, fat ...... 0.5 Parts per Commodity million Cattle, meat ...... 0 .5 Cattle, meat byproducts ...... 0.5 Cattle, fat ...... 0.05 Egg ...... 0 .1 Cattle, kidney ...... 1 Goat, fat ...... 0 .5 Cattle, liver ...... 1 Goat, meat ...... 0.5 Cattle, meat, except kidney and liver ...... 05 Goat, meat byproducts ...... 0 .5 Cattle, meat byproducts ...... 05 Hog, fat ...... 0 .5 Egg ...... 05 Hog, meat ...... 0 .5 Goat, fat ...... 05 Hog, meat byproducts ...... 0 .5 Goat, kidney ...... 1 Horse, fat ...... 0 .5 Goat, liver ...... 1 Horse, meat ...... 0 .5 Goat, meat, except kidney and liver ...... 05 Horse, meat byproducts ...... 0 .5 Goat, meat byproducts ...... 05 Milk, fat (0.05 ppm (N) in whole milk ...... 1 .25 Hog, fat ...... 05 Oat, grain ...... 6 .0 Hog, kidney ...... 1 Poultry, fat ...... 0.5 Hog, liver ...... 1 Hog, meat, except kidney and liver ...... 05 Poultry, meat ...... 5 Hog, meat byproducts ...... 05 Poultry, meat byproducts ...... 5 Horse, fat ...... 05 Rice, grain ...... 6 .0 Horse, kidney ...... 1 Sheep, fat ...... 0 .5 Horse, liver ...... 1 Sheep, meat ...... 0.5 Horse, meat, except kidney and liver ...... 05 Sheep, meat byproducts ...... 0 .5 Horse, meat byproducts ...... 05 Sorghum, grain ...... 6 .0 Milk ...... 05 Wheat, grain ...... 6 .0 Poultry, fat ...... 05 Poultry, kidney ...... 01 (2) Tolerances are established for the Poultry liver ...... 01 Poultry, meat, except kidney and liver ...... 05 combined residues of the insecticide Poultry, meat byproducts ...... 05 chlorpyrifos-methyl (O,-O- dimethyl-O- Sheep, fat ...... 05 (3,5,6-trichloro-2-pyridyl) Sheep, kidney ...... 1 Sheep, liver ...... 1 phosphorothioate and its metabolite Sheep, meat, except kidney and liver ...... 05 (3,5,6-trichloro-2-pyridinol) in or on the Sheep, meat byproducts ...... 05 following food commodities when present therein as a result of applica- (c) Tolerances are established in the tion to stored grains: following irrigated crops and crop

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groupings for residues of the herbicide Commodity Parts per fluridone resulting from use of irriga- million tion water containing residues of 0.15 Sheep, meat byproducts, except kidney ...... 0 .05 ppm following applications on or around aquatic sites. Where tolerances (b) Section 18 emergency exemptions. are established at higher levels from [Reserved] other uses of fluridone on the following (c) Tolerances with regional registra- crops, the higher tolerance also applies tions. [Reserved] to residues in the irrigated commodity. (d) Indirect or inadvertent residues. The tolerances follow: [Reserved] [51 FR 39662, Oct. 30, 1986, as amended at 53 Commodity Parts per million FR 27349, July 20, 1988; 53 FR 44403, Nov. 3, 1988; 54 FR 45734, Oct. 31, 1989; 60 FR 33354, Avocado ...... 0 .1 Citrus ...... 1 June 28, 1995; 62 FR 49937, Sept. 24, 1997; 62 FR Cotton, undelinted seed ...... 1 61447, Nov. 18, 1997; 67 FR 35048, May 17, 2002; Cucurbits ...... 1 67 FR 41807, June 19, 2002; 69 FR 6567, Feb. 11, Fruit, pome ...... 1 2004; 71 FR 32846, June 7, 2006; 71 FR 54434, Fruit, small ...... 1 Sept. 15, 2006] Fruit, stone ...... 1 Grain, crop ...... 1 Grass, forage ...... 15 § 180.422 Tralomethrin; tolerances for Hop ...... 1 residues. Legume, forage ...... 15 (a) General. (1) Tolerances are estab- Nut ...... 1 Root crops, vegetables ...... 1 lished for the combined residues of the Vegetable, fruiting ...... 1 pesticide chemical tralomethrin ((S)- Vegetable, leafy ...... 1 alpha-cyano-3-phenoxybenzyl (1R,3S)- Vegetable, seed and pod ...... 1 2,2-dimethyl-3-[(RS)-1,2,2,2- tetrabromoethyl]- [51 FR 12146, Apr. 9, 1986, as amended at 55 cyclopropanecarboxylate) and its me- FR 29829, July 20, 1990] tabolites (S)-alpha-cyano-3- phenoxybenzyl (1R,3R)-3(2,2- § 180.421 Fenarimol; tolerances for res- idues. dibromovinyl)-2,2-dimethyl- cyclopropanecarboxylate and (S)-alpha- (a) General. Tolerances are estab- cyano-3-phenoxybenzyl(1S,3R)-3-(2,2- lished for residues of the fungicide dibromovinyl)-2,2-dimethyl- fenarimol, alpha-(2-chlorophenyl)- cyclopropanecarboxylate calculated as alpha-(4-chlorophenyl)-5- the parent in or on the following food pyrimidinemethanol, in or on the fol- commodities: lowing raw agricultural commodities: Commodity Parts per Parts per million Commodity million Broccoli ...... 0 .5 Apple ...... 0.1 Cotton, undelinted seed ...... 0 .02 Apple, wet pomace ...... 0 .3 Cotton, oil ...... 0 .20 Banana ...... 0.25 Lettuce, head ...... 1.00 Cattle, fat ...... 0.01 Lettuce, leaf ...... 3 .00 Cattle, kidney ...... 0 .01 Soybean ...... 0.05 Cattle, meat ...... 0 .01 Sunflower, seed ...... 0.05 Cattle, meat byproducts, except kidney ...... 0.05 Cherry, sweet ...... 1 .0 (2) A tolerance of 0.02 part per mil- Cherry, tart ...... 1 .0 Goat, fat ...... 0 .01 lion is established for the combined Goat, kidney ...... 0 .01 residues of the insecticide Goat, meat ...... 0.01 tralomethrin ((S)-alpha-cyano-3- Goat, meat byproducts, except kidney ...... 0 .05 Grape ...... 0 .1. phenoxybenzyl-(1R,3S)-2,2-dimethyl-3- Hazelnut ...... 0 .02 [(RS)-1,2,2,2-tetrabromoethyl] Horse, fat ...... 0 .01 cyclopropanecarboxylate) and its me- Horse, kidney ...... 0 .01 tabolites cis-deltamethrin [(S-alpha- Horse, meat ...... 0 .01 Horse, meat byproducts, except kidney ...... 0 .05 cyano-3-phenoxybenzyl-(1R,3R)-3-[2,2- Pear ...... 0 .1 dibromovinyl)-2,2- Pecan ...... 0 .02 dimethylcyclopropanecarboxylate] and Sheep, fat ...... 0 .01 Sheep, kidney ...... 0.01 trans-deltamethrin [(S)-alpha-cyano-3- Sheep, meat ...... 0.01 phenoxybenzyl (1S,3R)-3-(2,2-

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dibromovinyl)-2,2- dibromovinyl)-2,2- dimethylcyclopropanecarboxylate] as dimethylcyclopropanecarboxylate as follows: follows: (i) In or on food commodities (other (i) In or on all feed items (other than than those covered by a higher toler- those covered by a higher tolerance as ance as a result of use on growing a result of use on growing crops) in crops) in food-handling establishments. feed-handling establishments. (ii) The insecticide may be present as (ii) The insecticide may be present as a residue from application of a residue from application of tralomethrin in food-handling estab- tralomethrin in feed-handling estab- lishments, including food service, man- lishments, including feed manufac- ufacturing, and processing establish- turing and processing establishments ments, such as restaurants, cafeterias, in accordance with the following pre- supermarkets, bakeries, breweries, scribed conditions: dairies, meat slaughtering and packing (A) Application shall be limited to a plants, and canneries in accordance general surface and spot and/or crack with the following prescribed condi- and crevice treatment in feed-handling tions: establishments where feed and feed (A) Application shall be limited to a products are held or processed. General general surface and spot and/or crack surface application may be used only and crevice treatment in food-handling when the facility is not in operation establishments where food and food provided exposed feed has been covered products are held, processed, prepared, or removed from the area being treat- and served. General surface application ed. All feed-contact surfaces and equip- may be used only when the facility is ment must be thoroughly cleaned after not in operation provided exposed food general surface applications. Spot and/ has been covered or removed from the or crack and crevice application may area being treated. All food-contact be used while the facility is in oper- surfaces and equipment must be thor- ation provided exposed feed is covered oughly cleaned after general surface or removed from the area being treated applications. Spot and/or crack and prior to application. Spray concentra- crevice application may be used while tion shall be limited to a maximum of the facility is in operation provided ex- 0.06 percent active ingredient. Con- posed food is covered or removed from tamination of feed and feed- contact the area being treated prior to applica- surfaces shall be avoided. tion. Spray concentration shall be lim- (B) To assure safe use of the insecti- ited to a maximum of 0.06 percent ac- cide, its label and labelling shall con- tive ingredient. Contamination of food form to that registered with the U.S. and food-contact surfaces shall be Environmental Protection Agency and avoided. shall be used in accordance with such (B) To assure safe use of the insecti- label and labelling. cide, its label and labelling shall con- (b) Section 18 emergency exemptions. form to that registered with the U.S. [Reserved] Environmental Protection Agency and (c) Tolerances with regional registra- shall be used in accordance with such tions. [Reserved] label and labelling. (d) Indirect or inadvertent residues. (3) A tolerance of 0.02 part per mil- [Reserved] lion is established for the combined [62 FR 63001, Nov. 26, 1997, as amended at 62 residues of the insecticide FR 66025, Dec. 17, 1997; 65 FR 33701, May 24, tralomethrin ((S)-alpha-cyano-3- 2000; 71 FR 74817, Dec. 13, 2006] phenoxybenzyl-(1R,3S)-2,2-dimethyl-3- [(RS)-1,2,2,2-tetrabromoethyl] § 180.425 Clomazone; tolerances for cyclopropanecarboxylate) and its me- residues. tabolites cis-deltamethrin [(S)-alpha- (a) General. Tolerances are estab- cyano-3-phenoxybenzyl-(1R,3R)-3-(2,2- lished for residues of the herbicide dibromovinyl)-2,2- clomazone, 2-(2-chlorophenyl)methyl- dimethylcyclopropanecarboxylate] and 4,4-dimethyl-3-isoxazolidinone, in or on trans-deltamethrin [(S)-alpha-cyano-3- the following raw agricultural com- phenoxybenzyl (1S,3R)-3-(2,2- modities:

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Parts per Parts per Commodity million Commodity million

Bean, snap, succulent ...... 0 .05 Honey ...... 0.05 Cabbage ...... 0 .1 Cotton, undelinted seed ...... 0 .05 (b) Section 18 emergency exemptions. Cucumber ...... 0 .1 Pea, succulent ...... 0 .05 [Reserved] Pepper ...... 0 .05 (c) Tolerances with regional registra- Peppermint, tops ...... 0 .05 tions. [Reserved] Pumpkin ...... 0.1 (d) Indirect and inadvertent residues. Rice, grain ...... 0 .02 [Reserved] Rice, straw ...... 0 .02 Soybean ...... 0.05 [65 FR 33701, May 24, 2000, as amended at 67 Spearmint, tops ...... 0 .05 FR 49617, July 31, 2002] Squash, summer ...... 0 .1 Squash, winter ...... 0 .1 Sugarcane, cane ...... 0.05 § 180.428 Metsulfuron methyl; toler- Sweet potato, roots ...... 0 .05 ances for residues. Vegetable, cucurbit, group 9 ...... 0.05 (a) General. (1) Tolerances are estab- Vegetable, tuberous and corm, except potato, subgroup 1D ...... 0 .05 lished for the combined residues of the herbicide metsulfuron methyl (methyl (b) Section 18 emergency exemptions. 2-[[[[(4-methoxy-6-methyl-1,3,5-triazin- [Reserved] 2-yl)amino] car- (c) Tolerances with regional registra- bonyl]amino]sulfonyl]benzoate) and its tions. [Reserved] metabolite methyl 2-[[[[(4-methoxy-6- (d) Indirect or inadvertent residues. methyl-1-,3,5-triazin-2- [Reserved] yl)amino]carbonyl]amino] sulfonyl]-4- hydroxybenzoate in or on the following [51 FR 9446, Mar. 19, 1986, as amended at 53 raw material agricultural commod- FR 3022, Feb. 3, 1988; 53 FR 19907, June 1, 1988; 56 FR 21310, May 8, 1991; 57 FR 59824, Dec. 16, ities: 1992; 58 FR 8697, Feb. 17, 1993; 58 FR 15804, Parts per Mar. 24, 1993; 60 FR 54605, Oct. 25, 1995; 61 FR Commodity million 20745, May 8, 1996; 62 FR 24045, May 2, 1997; 63 FR 13130, Mar. 18, 1998; 64 FR 28377, May 26, Barley, grain ...... 0 .1 1999; 64 FR 69415, Dec. 13, 1999; 65 FR 79769, Barley, hay ...... 20 .0 Barley, straw ...... 0 .3 Dec. 20, 2000; 65 FR 80343, Dec. 21, 2000; 66 FR Grass, fodder ...... 15 .0 10204, Feb. 14, 2001; 66 FR 39675, Aug. 1, 2001; Grass, forage ...... 15 .0 67 FR 35048, May 17, 2002; 67 FR 54124, Aug. 21, Grass, hay ...... 15 .0 2002] Sorghum, grain, forage ...... 0.2 Sorghum, grain, grain ...... 0 .1 § 180.426 2-[4,5-Dihydro-4-methyl-4-(1- Sorghum, grain, stover ...... 0 .2 Sugarcane, cane ...... 0.05 methylethyl)-5-oxo-1H-imidazol-2- Wheat, forage ...... 5 .0 yl]-3-quinoline carboxylic acid; tol- Wheat, grain ...... 0 .1 erance for residues. Wheat, hay ...... 20 .0 A tolerance is established for resi- Wheat, straw ...... 0 .3 dues of the herbicide 2-[4,5-dihydro-4- (2) Tolerances are established for res- methyl-4-(1-methylethyl)-5-oxo-1H- idues of metsulfuron methyl (methyl- imidazol-2-yl]-3-quinoline carboxylic 2[[[[(4-methoxy-6-methyl-1,3,5-triazin-2- acid, in or on the raw agricultural com- yl) amino]carbonyl] modity soybean at 0.05 part per mil- amino]sulfonyl]benzoate) in or on the lion. following raw agricultural commod- [51 FR 13309, Apr. 2, 1986] ities:

§ 180.427 Fluvalinate; tolerances for Commodity Parts per residues. million (a) General. Tolerances are estab- Cattle, fat ...... 0.1 Cattle, kidney ...... 0 .5 lished for residues of the insecticide Cattle, meat ...... 0 .1 (alpha RS,2R)-fluvalinate [(RS)-alpha- Cattle, meat byproducts ...... 0.1 cyano-3-phenoxybenzyl (R)-2-[2-chloro- Goat, fat ...... 0 .1 4-(trifluoromethyl) anilino]-3- Goat, kidney ...... 0 .5 Goat, meat ...... 0.1 methylbutanoate in or on the following Goat, meat byproducts ...... 0 .1 food commodities: Hog, fat ...... 0 .1

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Parts per Parts per Commodity million Commodity million

Hog, kidney ...... 0.5 Cattle, meat ...... 0 .05 Hog, meat ...... 0 .1 Cotton, undelinted seed ...... 0 .05 Hog, meat byproducts ...... 0 .1 Goat, fat ...... 0 .05 Horse, fat ...... 0 .1 Goat, meat byproducts ...... 0 .05 Horse, kidney ...... 0 .5 Goat, meat ...... 0.05 Horse, meat ...... 0 .1 Hog, fat ...... 0 .05 Horse, meat byproducts ...... 0 .1 Hog, meat byproducts ...... 0 .05 Milk ...... 0.05 Hog, meat ...... 0 .05 Sheep, fat ...... 0 .1 Horse, fat ...... 0 .05 Sheep, kidney ...... 0.5 Horse, meat byproducts ...... 0 .05 Sheep, meat ...... 0.1 Horse, meat ...... 0 .05 Sheep, meat byproducts ...... 0 .1 Milk ...... 0.02 Peanut hulls ...... 0 .05 (b) Section 18 emergency exemptions. Peanut ...... 0 .05 Rice, grain ...... 0 .05 [Reserved] Sheep, fat ...... 0 .05 (c) Tolerances with regional registra- Sheep, meat byproducts ...... 0 .05 tions. [Reserved] Sheep, meat ...... 0.05 (d) Indirect or inadvertent residues. Soybean ...... 0.05 Wheat, grain ...... 0 .05 [Reserved] Wheat, straw ...... 0 .50 [64 FR 70191, Dec. 16, 1999, as amended at 66 FR 64773, Dec. 14, 2001; 67 FR 51097, Aug. 7, (b) Section 18 emergency exemptions. 2002] [Reserved] (c) Tolerances with regional registra- § 180.429 Chlorimuron ethyl; tolerance tions. [Reserved] for residues. (d) Indirect or inadvertent residues. A tolerance is established for the res- [Reserved] idues of the herbicide chlorimuron [63 FR 1377, Jan. 9, 1998, as amended at 63 FR ethyl [ethyl 2-[[[[ (4-chloro-6- 19837, Apr. 22, 1998] methoxypyrimidin-2yl) amino]carbonyl] amino]sulfonyl] ben- § 180.431 Clopyralid; tolerances for zoate] in or on the following raw agri- residues. cultural commodities: (a) General. Tolerances are estab- Parts per lished for combined residues of the her- Commodity million bicide clopyralid (3,6-dichloro-2- Peanut ...... 0 .02 pyridinecarboxylic acid) in or on the Soybean ...... 0.05 following commodities:

Parts per [54 FR 27350, June 29, 1989] Commodity million

§ 180.430 Fenoxaprop-ethyl; tolerances Asparagus ...... 1.0 for residues. Barley, grain ...... 3 .0 Barley, hay ...... 9 .0 (a) General. Tolerances are estab- Barley, milled fractions (except flour) ...... 12 lished for the combined residues of the Barley, straw ...... 9 .0 Beet, garden, tops ...... 3 .0 herbicide fenoxaprop-ethyl [(±)-ethyl 2- Beet, garden, roots ...... 4 .0 [4-[(6-chloro-2- Beet, sugar, molasses ...... 10 benzoxazolyl)oxy]phenoxy]propanoate] Beet, sugar, roots ...... 2 .0 Beet, sugar, tops ...... 3.0 and its metabolites [2-[4-](6-chloro-2- Brassica, head and stem, subgroup 5A ...... 2 .0 benzoxazoly)oxy]phenoxy]propanoic Canola, meal ...... 6 .0 acid and 6-chloro- 2,3- Canola, seed ...... 3 .0 dihydrobenzoxazol-2-one], each ex- Cattle, fat ...... 1.0 Cattle, liver ...... 3 .0 pressed as fenoxaprop-ethyl, in or on Cattle, meat ...... 1 .0 the following raw agricultural com- Cattle, meat byproducts, except liver ...... 36 .0 modities: Corn, field, forage ...... 3 .0 Corn, field, stover ...... 10 .0 Parts per Corn, field, grain ...... 1 .0 Commodity million Corn, field, milled byproducts ...... 1 .5 Corn, pop, grain ...... 1.0 Barley, grain ...... 0 .05 Corn, pop, stover ...... 10.0 Barley, straw ...... 0 .1 Corn, sweet, forage ...... 7 .0 Cattle, fat ...... 0.05 Corn, sweet, kernel plus cob with husks re- Cattle, meat byproducts ...... 0.05 moved ...... 1 .0

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nitrobenzoate, in or on the following Commodity Parts per million raw agricultural commodities: Corn, sweet, stover ...... 10.0 Parts per Crambe, seed ...... 3.0 Commodity million Cranberry ...... 4 .0 Egg ...... 0 .1 Beans, snap, succulent (excluding limas) ...... 0 .01 Flax, meal ...... 6 .0 Cotton, gin byproducts ...... 0 .02 Flax, seed ...... 3 .0 Cotton, undelinted seed ...... 0 .01 Fruit, stone, group 12 ...... 0 .5 Peanut ...... 0 .01 Goat, fat ...... 1 .0 Soybean, seed ...... 0 .01 Goat, liver ...... 3.0 Goat, meat ...... 1.0 (b) Section 18 emergency exemptions. Goat, meat byproducts, except liver ...... 36 .0 Grass, forage and hay ...... 500.0 [Reserved] Hog, fat ...... 0 .2 (c) Tolerances with regional registra- Hog, meat ...... 0 .2 tions. Tolerances with regional reg- Hog, meat byproducts ...... 0 .2 istrations, as defined in 180.1(n) are es- Hop, dried cones ...... 5 .0 Horse, fat ...... 1 .0 tablished for residues of the herbicide, Horse, liver ...... 3 .0 lactofen, 1-(carboethoxy)ethyl 5-[2- Horse, meat ...... 1 .0 chloro-4-(trifluoromethyl)phenoxy]-2- Horse, meat byproducts, except liver ...... 36 .0 nitrobenzoate, in or on the following Milk ...... 0.2 Mint, hay ...... 3.0 food commodities: Mustard, greens ...... 5 .0 Mustard, seed ...... 3 .0 Parts per Commodity million Oat, forage ...... 9 .0 Oat, grain ...... 3 .0 Okra ...... 0.02 Oat, milled fractions (except flour) ...... 12 Vegetables, fruiting, group 08 ...... 0 .02 Oat, straw ...... 9.0 Plum, prune, dried ...... 1.5 Poultry, fat ...... 0.2 (d) Indirect or inadvertent residues. Poultry, meat ...... 0 .2 [Reserved] Poultry, meat byproducts ...... 0.2 Rapeseed, seed ...... 3 .0 [69 FR 57216, Sept. 24, 2004, as amended at 72 Rapeseed, forage ...... 3 .0 FR 33906, June 20, 2007] Sheep, fat ...... 1 .0 Sheep, liver ...... 3.0 § 180.433 Fomesafen; tolerances for Sheep, meat ...... 1.0 residues. Sheep, meat byproducts, except liver ...... 36 .0 Spinach ...... 5 .0 (a) General. Tolerances are estab- Strawberry ...... 1 .0 lished for the residues of fomesafen 5- Turnip, greens ...... 4.0 [2-chloro-4-(trifluoromethyl)phenoxy]- Turnip, roots ...... 1 .0 Wheat, forage ...... 9 .0 N-(methylsulfonyl)-2-nitrobenzamide Wheat, grain ...... 3 .0 from the application of its sodium salt Wheat, milled fractions (except flour) ...... 12 in or on the following commodities: Wheat, straw ...... 9 .0 Commodity Parts per (b) Section 18 emergency exemptions. million [Reserved] Bean, dry ...... 0.025 (c) Tolerances with regional registra- Bean, snap, succulent ...... 0.025 Cotton, gin byproducts ...... 0.025 tions. [Reserved] Cotton, undelinted seed ...... 0.025 (d) Indirect or inadvertent residues. Soybean ...... 0.05 [Reserved] (b) Section 18 emergency exemptions. [52 FR 10566, Apr. 2, 1987] [Reserved] EDITORIAL NOTE: For FEDERAL REGISTER ci- (c) Tolerances with regional registra- tations affecting § 180.431, see the List of CFR tions. [Reserved] Sections Affected, which appears in the (d) Indirect or inadvertent residues. Finding Aids section of the printed volume [Reserved] and on GPO Access. [71 FR 25951, May 3, 2006] § 180.432 Lactofen; tolerances for resi- dues. § 180.434 Propiconazole; tolerances for (a) Tolerances are established for res- residues. idues of the herbicide lactofen, 1- (a) General. Tolerances are estab- (carboethoxy)ethyl 5-[2-chloro-4- lished for the combined residues of the (trifluoromethyl)phenoxy]-2- fungicide 1-[[2-(2,4-dichlorophenyl)-4-

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propyl-1,3-dioxolan-2-yl] methyl]-1H- Commodity Parts per 1,2,4-triazole and its metabolites deter- million mined as 2,4-dichlorobenzoic acid and Sheep, fat ...... 0 .05 expressed as parent compound in or on Sheep, kidney ...... 2.0 the following commodities: Sheep, liver ...... 2.0 Sheep, meat ...... 0.05 Sheep, meat byproducts, except liver and kid- Parts per Commodity million ney ...... 0.05 Sorghum, grain, forage ...... 12 Almond, hulls ...... 7 .0 Sorghum, grain, grain ...... 3 .5 Banana ...... 0.2 Sorghum, grain, stover ...... 15 Barley, bran ...... 0 .6 Soybean, forage ...... 11 Barley, grain ...... 0 .3 Soybean, hay ...... 30 Barley, hay ...... 1 .4 Soybean, seed ...... 2 .0 Barley, straw ...... 10 Spearmint, tops ...... 3 .5 Beet, sugar, dried pulp ...... 1 .0 Strawberry ...... 1 .3 Beet, sugar, molasses ...... 1 .5 Wheat, bran ...... 0.6 Beet, sugar, roots ...... 0 .3 Wheat, forage ...... 1 .7 Beet, sugar, tops ...... 10 Wheat, grain ...... 0 .3 Berry, group 13 ...... 1 .0 Wheat, hay ...... 1 .4 Wheat, straw ...... 10 Carrot, roots ...... 0.25 Cattle, fat ...... 0.05 Cattle, kidney ...... 2 .0 (b) Section 18 emergency exemptions. Cattle, liver ...... 2 .0 Time-limited tolerances are estab- Cattle, meat ...... 0 .05 Cattle, meat byproducts, except liver and kidney 0.05 lished for residues of propiconazole (1- Corn, field, forage ...... 12 [[2-(2,4-dichlorophenyl)-4-propyl-1,3- Corn, field, grain ...... 0 .2 dioxolan-2-yl] methyl]-1H-1,2,4-triazole) Corn, field, stover ...... 30 and its metabolites determined as 2,4- Corn, pop, grain ...... 0.2 Corn, pop, stover ...... 30 dichlorobenzoic acid and expressed as Corn, sweet, forage ...... 6 .0 parent compound, in connection with Corn, sweet, kernel plus cob with husks re- use of the pesticide under section 18 moved ...... 0 .1 Corn, sweet, stover ...... 30 emergency exemptions granted by Fruit, stone, group 12 ...... 1 .0 EPA. The tolerances will expire and Goat, fat ...... 0 .05 are revoked on the dates specified in Goat, kidney ...... 2 .0 the following table: Goat, liver ...... 2.0 Goat, meat ...... 0.05 Expiration/ Goat, meat byproducts, except liver and kidney 0 .05 Commodity Parts per revocation Grain, aspirated fractions ...... 30 million date Grass, forage ...... 0 .5 Grass, hay ...... 0 .5 Nectarine ...... 2.0 12/31/2010 Grass, straw ...... 40 Peach ...... 2.0 12/31/2010 Hog, kidney ...... 0.2 Hog, liver ...... 0 .2 (c) Tolerances with regional registra- Horse, fat ...... 0 .05 Horse, kidney ...... 2 .0 tions. A tolerance with regional reg- Horse, liver ...... 2 .0 istration, as defined in §180.1(m), is es- Horse, meat ...... 0 .05 tablished for residues of 1-[[2-(2,4- Horse, meat byproducts, except liver and kidney 0 .05 Leaf petioles, subgroup 4B ...... 5 .0 dichlorophenyl)-4-propyl-1,3-dioxolan-2- Milk ...... 0.05 yl]methyl]-1H-1,2,4-triazole and its me- Mushroom ...... 0 .1 tabolites determined as 2,4- Nut, tree, group 14 ...... 0 .1 dichlorobenzoic acid and expressed as Oat, forage ...... 1 .7 Oat, grain ...... 0 .3 parent compound, in or on the fol- Oat, hay ...... 1.4 lowing commodities: Oat, straw ...... 10 Onion, bulb ...... 0 .2 Commodity Parts per Onion, green ...... 9 .0 million Peanut ...... 0 .2 Peanut, hay ...... 20 Cranberry ...... 1 .0 Peppermint, tops ...... 3 .5 Rice, wild, grain ...... 0.5 Pineapple ...... 0.1 Pistachio ...... 0.1 (d) Indirect or inadvertent residues. Rice, bran ...... 15 Tolerances are established for the com- Rice, grain ...... 7 .0 Rice, hulls ...... 20 bined residues of the fungicide 1-[[2- Rice, straw ...... 18 (2,4-dichlorophenyl)-4-propyl-1,3- Rye, bran ...... 0 .6 dioxolan-2-yl] methyl]-1H-1,2,4-triazole Rye, forage ...... 1 .7 Rye, grain ...... 0.3 and its metabolites determined as 2,4- Rye, straw ...... 10 dichlorobenzoic acid and expressed as

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parent compound in or on the following Commodity Parts per commodities when present therein as a million result of application of propiconazole Onion, dry bulb ...... 0 .1 to growing crops in paragraphs (a) and Onion, green ...... 1 .5 (c) of this section: Poultry, fat ...... 0.05 Poultry, meat ...... 0 .02 Parts per Poultry, meat byproducts ...... 0.02 Commodity million Radish tops ...... 4.0 Rapeseed ...... 0 .2 Alfalfa, forage ...... 0.1 Rice, hulls ...... 2 .5 Alfalfa, hay ...... 0.1 Rye, bran ...... 5 .0 Sheep, fat ...... 0 .05 [71 FR 55306, Sept. 22, 2006, as amended at 72 Sheep, meat ...... 0.02 Sheep, meat byproducts ...... 0 .05 FR 20439, Apr. 25, 2007] Sorghum, grain forage ...... 0 .5 Sorghum, grain stover ...... 1.0 § 180.435 Deltamethrin; tolerances for Soybean, seed ...... 0 .1 residues. Soybean, hulls ...... 0 .2 (a) General. (1) Tolerances are estab- Starfruit* ...... 0.2 Sunflower seed ...... 0 .1 lished for the combined residues of the Tomato ...... 0.2 pesticide chemical deltamethrin Tomato, concentrated products ...... 1.0 [(1R,3R)-3-(2,2-dibromovinyl)-2,2- Vegetable, cucurbit, Group 9 ...... 0 .2 dimethylcyclopropanecarboxylic acid Vegetable, fruiting, Group 8 ...... 0 .3 Vegetable, root, except sugar beet, Subgroup IB 0 .2 (S)-alpha-cyano-3-phenoxybenzyl ester Vegetable, tuberous and corm, Subgroup IC ..... 0 .04 and its major metabolites, trans Wheat, bran ...... 5.0 deltamethrin [(S)-alpha-cyano-m- *There are no U.S. registrations for use of deltamethrin on phenoxybenzyl(1R,3S)-3-(2,2- starfruit and lychee. dibromovinyl)-2,2- (2) A tolerance of 0.05 ppm is estab- dimethylcyclopropanecarboxylate] and lished for residues of the insecticide alpha-R-deltamethrin [(R)-alpha-cyano- deltamethrin (1R,3R)-3-(2,2- m-phenoxybenzyl-(1R,3R)-3-(2,2- dibromovinyl)-2,2- dibromovinyl)-2,2- dimethylcyclopropanecarboxylic acid dimethylcyclopropanecarboxylate] in (S)-alpha-cyano-3-phenoxybenzyl ester or on the following agricultural com- and its major metabolites, trans modities: deltamethrin (S)-alpha-cyano-m- Parts per phenoxybenzyl-(1R,3R)-3-(2,2- Commodity million dibromovinyl)-2,2- Almond, hulls ...... 2 .5 dimethylcyclopropanecarboxylate and Apples, wet pomace ...... 1 .0 alpha-R-deltamethrin[(R)-alpha-cyano- Artichoke, globe ...... 0.5 m-phenoxybenzyl-(1R,3R)-3-(2,2- Barley, bran ...... 5 .0 Cattle, fat ...... 0.05 dibromovinyl)-2,2- Cattle, meat ...... 0 .02 dimethylcyclopropanecarboxylate] as Cattle, meat byproducts ...... 0.05 follows: Corn, field, forage ...... 0 .7 Corn, field, refined oil ...... 2 .5 (i) In or on all food/feed items (other Corn, field, stover ...... 5 .0 than those covered by a higher toler- Corn, pop, stover ...... 5.0 ance as a result of use on growing Corn, sweet, forage ...... 10 Corn, sweet, kernel plus cob with husks re- crops) in food/feed handling establish- moved ...... 0 .03 ments. Corn, sweet, stover ...... 15 (ii) The insecticide may be present as Cotton, undelinted seed ...... 0 .04 Cotton, oil ...... 0 .2 a residue from application of Egg ...... 0 .02 deltamethrin in food handling estab- Fruit, pome, Group 11 ...... 0 .2 lishments, including food service, man- Goat, fat ...... 0 .05 ufacturing and processing establish- Goat, meat ...... 0.02 Goat, meat byproducts ...... 0 .05 ments, such as restaurants, cafeterias, Grain, aspirated fractions ...... 65 supermarkets, bakeries, breweries, Grain, cereal, Group 15, except sweet corn ...... 1 .0 dairies, meat slaughtering and packing Hog, fat ...... 0 .05 Horse, fat ...... 0 .05 plants, and canneries, feed handling es- Horse, meat ...... 0 .02 tablishments including feed manufac- Horse, meat byproducts ...... 0 .05 turing and processing establishments, Lychee* ...... 0 .2 Milk, fat (reflecting 0.02 ppm in whole milk) ...... 0 .1 in accordance with the following pre- Nut, tree, Group 14 ...... 0.1 scribed conditions:

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(A) Application shall be limited to Commodity Parts per general surface and spot and/or crack million and crevice treatment in food/feed han- Corn, field, milled byproducts ...... 7 .0 dling establishments where food/feed Corn, field, refined oil ...... 30 .0 and food/feed products are held, proc- Corn, field, stover ...... 6 .0 Corn, pop, stover ...... 6.0 essed, prepared and served. General Corn, sweet, forage ...... 15 .00 surface application may be used only Corn, sweet, kernel plus cob with husks re- when the facility is not in operation moved ...... 0 .05 Corn, sweet, stover ...... 30.00 provided exposed food/feed has been Cotton, hulls ...... 2 .0 covered or removed from the area Cotton, refined oil ...... 2.0 being treated. Spot and/or crack and Cotton, undelinted seed ...... 1 .0 crevice application may be used while Egg ...... 0 .01 Fruit, citrus, group 10 ...... 0 .2 the facility is in operation provided ex- Fruit, pome, group 11 ...... 0.5 posed food/feed is covered or removed Fruit, stone, group 12 ...... 0 .3 from the area being treated prior to ap- Goat, fat ...... 10 .0 Goat, meat ...... 0.40 plication. Spray concentration shall be Goat, meat byproducts ...... 0 .40 limited to a maximum of 0.06 percent Grain, aspirated fractions ...... 600 active ingredient. Contamination of Grain, cereal, group 15 ...... 4.0 Grape ...... 1 .0 food/feed or food/feed contact surfaces Grape, raisin ...... 3 .5 shall be avoided. Hog, fat ...... 10 .0 (B) To assure safe use of the insecti- Hog, meat ...... 0 .40 cide, its label and labeling shall con- Hog, meat byproducts ...... 0 .40 Hop, dried cones ...... 20 .0 form to that registered with the U.S. Hop, vines ...... 4 .0 Environmental Protection Agency and Horse, fat ...... 10 .0 shall be used in accordance with such Horse, meat ...... 0 .40 Horse, meat byproducts ...... 0 .40 label and labeling. Lettuce, head ...... 2.0 (b) Section 18 emergency exemptions. Lettuce, leaf ...... 3 .0 [Reserved] Milk ...... 1.0 (c) Tolerances with regional registra- Milk, fat ...... 30 .0 Mustard greens ...... 7.0 tions. [Reserved] Nut, tree, group 14 ...... 0 .01 (d) Indirect or inadvertent residues. Oat, bran ...... 5 .0 [Reserved] Pea and bean, dried shelled, except soybean, subgroup 6C ...... 0 .15 [62 FR 63001, Nov. 26, 1997, as amended at 63 Pea, dry, seed ...... 0 .15 FR 45414, Aug. 26, 1998; 69 FR 62614, Oct. 27, Pea, southern, succulent ...... 0 .25 2004] Peanut ...... 0 .01 Peanut, hay ...... 6.0 Pepper ...... 0 .50 § 180.436 Cyfluthrin; tolerances for Pistachio ...... 0.01 residues. Poultry, fat ...... 0.01 (a) General. (1) Tolerances are estab- Poultry, meat ...... 0 .01 Poultry, meat byproducts ...... 0.01 lished for residues of the insecticide Radish, roots ...... 1 .0 cyfluthrin (cyano(4-fluoro-3- Rice, bran ...... 6.0 phenoxyphenyl)methyl-3-(2,2- Rice, hulls ...... 18 .0 dichloroethenyl)-2,2dimethyl- Rye, bran ...... 5 .0 Sheep, fat ...... 10 .0 cyclopropane-carboxylate; CAS No. Sheep, meat ...... 0.40 68359–37–5) in or on the following raw Sheep, meat byproducts ...... 0 .40 agricultural commodities: Sorghum, grain, forage ...... 2.0 Sorghum, grain, stover ...... 5 .0 Soybean, forage ...... 8 .0 Parts per Commodity million Soybean, hay ...... 4 .0 Soybean, seed ...... 0 .03 Alfalfa ...... 5 .0 Sugarcane, cane ...... 0.05 Alfalfa, hay ...... 10.0 Sugarcane, molasses ...... 0 .20 Almond, hulls ...... 0 .5 Sunflower, forage ...... 5.0 Barley, bran ...... 5 .0 Sunflower, seed ...... 0.02 Brassica, head and stem, subgroup 5A ...... 2 .5 Tomato ...... 0.20 Brassica, leafy greens, subgroup 5B ...... 7 .0 Tomato, paste ...... 0 .5 Carrot, roots ...... 0.20 Tomato, pomace ...... 5 .0 Cattle, fat ...... 10.0 Turnips, greens ...... 7.0 Cattle, meat ...... 0 .40 Vegetable, cucurbit, group 9 ...... 0.1 Cattle, meat byproducts ...... 0.40 Vegetable, fruiting, group 8 ...... 0.5 Citrus, dried pulp ...... 0 .3 Vegetable, leafy greens, except Brassica, group Citrus, oil ...... 0.3 4 ...... 6 .0 Corn, field, forage ...... 3 .0 Vegetable, tuberous and corm, subgroup 1C ..... 0.01

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3-phenoxyphenyl)methyl-3-(2,2- Commodity Parts per million dichloroethenyl)-2,2- Wheat, bran ...... 6.5 dimethylcyclopropanecarboxylate; Wheat, forage ...... 5 .0 CAS Reg. No. 68359–37–5) in feed com- Wheat, hay ...... 6 .0 modities exposed to the insecticide Wheat, shorts ...... 11 .0 Wheat, straw ...... 6 .0 during treatment of feed-handling es- tablishments where feed and feed prod- (2) A tolerance of 0.05 ppm is estab- ucts are held, processed, prepared, or lished for residues of the insecticide served. Treatments may be made by cyfluthrin (cyano(4-fluoro-3- general surface, spot, and/or crack and phenoxyphenyl)methyl-3-(2,2- crevice applications. dichloroethenyl)-2,2- (i) General surface tratments shall be dimethylcyclopropanecarboxylate; limited to a maximum of 3.8 grams of CAS Reg. No. 69359–37–5) in food com- active ingredient per 1,000 square feet, modities exposed to the insecticide applying to walls, floors, and ceilings during treatment of food-handling es- with a low-pressure system. Cover or tablishments where food and food prod- remove all feed processing and/or han- ucts are held, processed, prepared, or dling equipment during application. Do served. Treatments may be made by not apply directly to feed products. Re- general surface, spot, and/or crack and applications may be made at 10-day in- crevice applications. tervals. (i) General surface treatments shall (ii) Crack and crevice or spot treat- be limited to a maximum of 3.8 grams ments shall be limited to a maximum of active ingredient per 1,000 square of 0.1 percent of the active ingredient feet, applying to walls, floors, and ceil- by weight, applied with a low-pressure ings with a low-pressure system. Cover system with a pinpoint or variable-pat- or remove all food processing and/or tern nozzle. Dust formulation shall be handling equipment during applica- limited to a maximum of 0.1 percent of tion. Do not apply directly to food the active ingredient by weight, ap- products. Reapplications may be made plied using a hand duster, power dust- at 10-day intervals. er, or other equipment capable of ap- (ii) Crack and crevice or spot treat- plying dust insecticide directly into ments shall be limited to a maximum voids and cracks and crevices. Dust ap- of 0.1 percent of the active ingredient plications should be made in a manner weight, applied with a low-pressure to avoid deposits on exposed surfaces system with a pinpoint or variable-pat- or introducing the material into the tern nozzle. Dust formulation shall be air. Cover exposed feed or remove feed limited to a maximum of 0.1 percent of from premises. Do not apply directly to the active ingredient by weight, ap- feed. Reapplications may be made at plied using a hand duster, power dust- 10-day intervals. er, or other equipment capable of ap- (iii) To ensure safe use of the insecti- plying dust insecticide directly into cide, its label and labeling shall con- voids and cracks and crevices. Dust ap- form to that registered by EPA, and it plications should be made in a manner shall be used in accordance with such to avoid deposits on exposed surfaces label and labeling. or introducing the material into the air. Cover exposed food or remove food (b) Section 18 emergency exemptions. from premises. Do not apply directly to [Reserved] food. Reapplications may be made at (c) Tolerances with regional registra- 10-day intervals. tions. Tolerances with regional reg- (iii) To ensure safe use of the insecti- istration, as defined in § 180.1(n), are es- cide, its label and labeling shall con- tablished for residues of cyfluthrin in form to that registered by the Environ- or on the following raw agricultural mental Protection Agency, and it shall commodities: be used in accordance with such label Parts per and labeling. Commodity million (3) A tolerance of 0.05 part per mil- lion is established for residues of the Grass, forage ...... 6 .0 insecticide cyfluthrin (cyano(4-fluoro- Grass, hay ...... 8 .0

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(d) Indirect or inadvertent residues. plants and livestocks, as indicated in [Reserved] the following table. [53 FR 1924, Jan. 25, 1988, as amended at 54 Commodity Parts per FR 27643, June 30, 1989; 60 FR 28354, May 31, million 1995; 60 FR 33357, June 28, 1995; 60 FR 34876, Alfalfa, forage ...... 5.0 July 5, 1995; 61 FR 10681, Mar. 15, 1996; 61 FR Alfalfa, hay ...... 6.0 39886, July 31, 1996; 62 FR 25523, May 9, 1997; Almond, hulls ...... 1 .5 62 FR 63018, 63019, Nov. 26, 1997; 64 FR 35067, Apple, wet pomace ...... 2 .50 June 30, 1999; 66 FR 27473, May 17, 2001; 67 FR Avocado, imported ...... 0.20 60991, Sept. 27, 2002; 70 FR 7047, Feb. 10, 2005; Brassica, head and stem, subgroup 5A ...... 0 .4 70 FR 53953, Sept. 13, 2005; 71 FR 19442, Apr. Canola, refined oil ...... 2 .0 Canola, seed ...... 1 .0 14, 2006] Cattle, fat ...... 3.0 Cattle, meat ...... 0 .2 § 180.437 Methyl 2-(4-isopropyl-4-meth- Cattle, meat byproducts ...... 0.2 yl-5-oxo-2-imidazolin-2-yl)-p-toluate Corn, field, grain ...... 0 .05 and methyl 6-(4-isopropyl-4-methyl- Corn, field, grain, flour ...... 0.15 5-oxo-2-imidazolin-2-yl)-m-toluate; Corn, field, forage ...... 6 .0 Corn, field, stover ...... 1 .0 tolerances for residues. Corn, pop, grain ...... 0.05 Tolerances are established for the Corn, pop, grain, flour ...... 0 .05 Corn, pop, stover ...... 1.0 combined residues of the herbicide Corn, sweet, forage ...... 6 .0 methyl 2-(4-isopropyl-4-methyl-5-oxo-2- Corn, sweet, stover ...... 1 .0 imidazolin-2-yl)-p-toluate and methyl Corn, sweet, kernel plus cob with husks re- moved ...... 0 .05 6-(4-isopropyl-4-methyl-5-oxo-2- Cotton, undelinted seed ...... 0 .05 imidazolin-2-yl)-m-toluate in or on the Egg ...... 0 .01 following raw agricultural commod- Fruit, pome, group 11 ...... 0.30 Fruit, stone, group 12 ...... 0 .50 ities: Garlic ...... 0 .1 Goat, fat ...... 3 .0 Commodity Parts per Goat, meat ...... 0.2 million Goat, meat byproducts ...... 0 .2 Grain, aspirated fractions ...... 2 .0 Barley, grain ...... 0 .10 Hog, fat ...... 3 .0 Barley, straw ...... 2 .00 Hog, meat ...... 0 .2 Sunflower, seed ...... 0.10 Hog, meat byproducts ...... 0 .2 Wheat, grain ...... 0 .10 Hop, dried cones ...... 10 .0 Wheat, straw ...... 2 .00 Horse, fat ...... 3 .0 Horse, meat ...... 0 .2 Horse, meat byproducts ...... 0 .2 [53 FR 24069, June 27, 1988] Lettuce, head ...... 2.0 Lettuce, leaf ...... 2 .0 § 180.438 Lambda-cyhalothrin and an Milk, fat (reflecting 0.2 ppm in whole milk) ...... 5 .0 Nut, tree, group 14 ...... 0 .05 isomer gamma-cyhalothrin; toler- Onion, bulb ...... 0 .1 ances for residues. Pea and bean, dried shelled, except soybean, (a) General. (1) Tolerances are estab- subgroup 6C ...... 0 .10 Pea and bean, succulent shelled, subgroup 6B 0 .01 lished for the combined residues of the Peanut ...... 0 .05 lambda-cyhalothrin, 1:1 Peanut, hay ...... 3.0 mixture of (S)-a-cyano-3- Poultry, fat ...... 0.03 Poultry, meat ...... 0 .01 phenoxybenzyl-(Z)-(1R,3R)-3-(2-chloro- Poultry, meat byproducts ...... 0.01 3,3,3-trifluoroprop-1-enyl)-2,2- Rice, grain ...... 1 .0 dimethylcyclopropanecarboxylate and Rice, hulls ...... 5 .0 (R)- -cyano-3-phenoxybenzyl-(Z)- Rice, straw ...... 1 .8 a Sheep, fat ...... 3 .0 (1S,3S)-3-(2-chloro-3,3,3-trifluoroprop-1- Sheep, meat ...... 0.2 enyl)-2,2- Sheep, meat byproducts ...... 0 .2 dimethylcyclopropanecarboxylate and Soybean ...... 0.01 Sorghum, grain, grain ...... 0 .2 its epimer expressed as epimer of lamb- Sorghum, grain, forage ...... 0.30 da-cyhalothrin, a 1:1 mixture of (S)-a- Sorghum, grain, stover ...... 0 .50 cyano-3-phenoxybenzyl-(Z)-(1S,3S)-3-(2- Sugarcane, cane ...... 0.05 chloro-3,3,3-trifluoroprop-1-enyl)-2,2- Sunflower, forage ...... 0.2 Sunflower, seed, hulls ...... 0 .50 dimethylcyclopropanecarboxylate and Sunflower, refined oil ...... 0.30 (R)-a-cyano-3-phenoxybenzyl-(Z)- Sunflower, seed ...... 0.2 (1R,3R)-3-(2-chloro-3,3,3-trifluoroprop-1- Tomato ...... 0.1 Tomato, dry pomace ...... 6.0 enyl)-2,2- Tomato, wet pomace ...... 6.0 dimethylcyclopropanecarboxylate, on Vegetables, fruiting, group 8 ...... 0.20

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Parts per Parts per Commodity million Commodity million

Vegetables, legume, edible podded, subgroup Poultry, meat ...... 0 .01 6A ...... 0 .20 Poultry, meat byproducts ...... 0.01 Wheat, grain ...... 0 .05 Rice, grain ...... 1 .0 Wheat, forage ...... 2 .0 Rice, hulls ...... 5 .0 Wheat, hay ...... 2 .0 Rice, straw ...... 1 .8 Wheat, straw ...... 2 .0 Sheep, fat ...... 3 .0 Wheat, bran ...... 0.2 Sheep, meat ...... 0.2 Sheep, meat byproducts ...... 0 .2 (2) Tolerances1 are established for the Sorghum, grain, forage ...... 0.30 combined residues of the pyrethroid Sorghum, grain, grain ...... 0 .20 Sorghum, grain, stover ...... 0 .50 [gamma-cyhalothrin (the isolated ac- Soybean ...... 0.01 tive isomer of lambda-cyhalothrin) (S)- Sugarcane ...... 0 .05 ′-cyano-3-phenoxybenzyl (Z)-(1R,3R)-3- Sunflower, forage ...... 0.20 (2-chloro-3,3,3-trifluoroprop-1-enyl)-2,2- Sunflower, seed hulls ...... 0 .50 Sunflower, refined oil ...... 0.30 dimethylcyclopropanecarboxylate)) Sunflower, seed ...... 0.20 and its epimer (R)-′-cyano-3- Tomato ...... 0.10 phenoxybenzyl (Z)-(1R,3R)-3-(2-chloro- Tomato, dry pomace ...... 6.0 3,3,3-trifluoroprop-1-enyl)-2,2- Tomato, wet pomace ...... 6.0 Vegetables, fruiting, group 8 ...... 0.20 dimethylcyclopropanecarboxylate in/ Vegetable, legume, edible podded, subgroup 6A 0 .20 on the following commodities: Wheat, grain ...... 0 .05 Wheat, forage ...... 2 .0 Commodity Parts per Wheat, hay ...... 2 .0 million Wheat, straw ...... 2 .0 Wheat, bran ...... 2.0 Alfalfa, forage ...... 5 Alfalfa, hay ...... 6 1 The analytical enforcement methods for lambda- Almond, hulls ...... 1 .5 cyhalothrin are applicable for determination of gamma- Apple, wet pomace ...... 2 .50 cyhalothrin residues in plant and animal commodities. Avocado, imported ...... 0.20 Brassica, head and stem, subgroup 5A ...... 0 .4 (3) A food additive tolerance of 0.01 Canola, seed ...... 0 .15 part per million is established for resi- Cattle, fat ...... 3 dues of the insecticide [1a(S*),3a(Z)]- Cattle, meat ...... 0 .2 (±)-cyano(3-phenoxyphenyl)methyl 3-(2- Cattle, meat byproducts ...... 0.2 Corn, field, forage ...... 6 .0 chloro-3,3,3-trifluoro-1-propenyl)-2,2- Corn, field, grain ...... 0 .05 dimethylcyclopropanecarboxylate Corn, field, grain, flour ...... 0.15 (lambda-cyhalothrin) as follows: Corn, field, stover ...... 1 .0 Corn, pop, grain ...... 0.05 (i) In or on all food commodities Corn, pop, stover ...... 1.0 (other than those already covered by a Corn, sweet, forage ...... 6 .0 higher tolerance as a result of use on Corn, sweet, kernel plus cob with husks re- moved ...... 0 .05 growing crops) in food-handling estab- Corn, sweet, stover ...... 1 .0 lishments where food products are Cotton, undelinted seed ...... 0 .05 held, processed, or prepared. Egg ...... 0 .01 Fruit, pome, group 11 ...... 0.30 (ii) Application shall be limited sole- Fruit, stone, group 12 ...... 0 .50 ly to spot and/or crack and crevice Garlic ...... 0 .10 treatment with a spray solution max- Goat, fat ...... 3 .0 imum of a 0.06-percent active ingre- Goat, meat ...... 0.2 Goat, meat byproducts ...... 0 .2 dient by weight. Food must be removed Grain, aspirated fractions ...... 2 .0 or covered during treatment. Spray Hog, fat ...... 3 .0 should not be applied directly to sur- Hog, meat ...... 0 .2 Hog, meat byproducts ...... 0 .2 faces or utensils that may come into Horse, fat ...... 3 .0 contact with food. Food-contact sur- Horse, meat ...... 0 .2 faces and equipment should be thor- Horse, meat byproducts ...... 0 .2 Lettuce, head ...... 2.0 oughly cleaned with an effective clean- Lettuce, leaf ...... 2 .0 ing compound and rinsed with potable Milk, fat (reflecting 0.20 ppm in whole milk ...... 5 .0 water before using. Nut, tree, group 14 ...... 0 .05 Onion, bulb ...... 0 .1 (iii) For spot treatment, a coarse Pea and bean, dried shelled, except soybean, low-pressure spray shall be used. Limit subgroup 6C ...... 0 .10 individual spot treatments to an area Pea and bean, succulent shelled, subgroup 6B 0 .01 no larger than 20 percent of the surface Peanut ...... 0 .05 Peanut, hay ...... 3.0 area. Any individual spot treatment Poultry, fat ...... 0.03 shall not exceed 2 square feet.

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(iv) For crack and crevice treatment, yl)amino] carbonyl] amino] sulfonyl]-2- equipment capable of delivering a pin- thiophene carboxylate) in or on the fol- stream of spray directly into the lowing raw agricultural commodities: cracks and crevices shall be used. Parts per (v) To assure safe use of the additive, Commodity million its label and labeling shall conform to that registered with the U.S. Environ- Barley, grain ...... 0 .05 Barley, straw ...... 0 .10 mental Protection Agency, and it shall Canola, seed ...... 0 .02 be used in accordance with such label Corn, field, forage ...... 0 .10 and labeling. Corn, field, grain ...... 0 .05 Corn, field, stover ...... 0 .10 (b) Section 18 emergency exemptions. Cotton, gin byproducts ...... 0 .02 Time-limited tolerances are estab- Cotton, undelinted seed ...... 0 .02 lished for combined residues of the in- Flax, seed ...... 0 .02 secticide lambda-cyhalothrin (a 1:1 Oat, grain ...... 0 .05 Oat, straw ...... 0.10 mixture of (S)-a-cyano-3- Rice, grain ...... 0 .05 phenoxybenzyl-(Z)-(1R,3R)-3-(2-chloro- Rice, straw ...... 0 .05 3,3,3-trifluoroprop-1-enyl)-2,2- Sorghum, grain, forage...... 0 .05 Sorghum, grain, grain ...... 0 .05 dimethylcyclopropanecarboxylate and Sorghum, grain, stover ...... 0 .05 (R)-a-cyano-3-phenoxybenzyl-(Z)- Soybean ...... 0.10 (1S,3S)-3-(2-chloro-3,3,3-trifluoroprop-1- Wheat, grain ...... 0 .05 enyl)-2,2- Wheat, straw ...... 0 .10 dimethylcyclopropanecarboxylate and (b) Section 18 emergency exemptions. its epimer a 1:1 mixture of (S)-a-cyano- [Reserved] 3-phenoxybenzyl-(Z)-(1S,3S)-3-(2-chloro- (c) Tolerances with regional registra- 3,3,3-trifluoroprop-1-enyl)-2,2- tions. [Reserved] dimethylcyclopropanecarboxylate and (d) Indirect or inadvertent residues. (R)-a-cyano-3-phenoxybenzyl -(Z)- [Reserved] (1R,3R)-3-(2-chloro-3,3,3-trifluoroprop-1- enyl)-2,2-dimethylcyclo- [69 FR 55982, Sept. 17, 2004, as amended at 69 propanecarboxylate in connection with FR 63957, Nov. 3, 2004; 72 FR 13184, Mar. 21, use of the pesticide under section 18 2007] emergency exemptions granted by § 180.440 Tefluthrin; tolerances for res- EPA. The tolerances will expire and idues. are revoked on the dates specified in the following table: (a) General. Tolerances are estab- lished for the combined residues of the insecticide tefluthrin (2,3,5,6 Parts per Expiration/ Commodity revocation tetrafluroro-4-methylphenyl)methyl-(1 million date alpha, 3 alpha)-(Z)-(±)-3(2-chloro-3,3,3- Barley, bran ...... 0.2 12/31/08 trifluoro-1-propenyl)-2,2- Barley, grain ...... 0.05 12/31/08 diemthylcyclopropanecarboxylate) and Barley, hay ...... 2.0 12/31/08 Barley, straw ...... 2.0 12/31/08 its metabolite (Z)-3-(2-chloro-3,3,3- Clover, forage ...... 5.0 12/31/08 trifluroro-1-propenyl)-2,2- Clover, hay ...... 6.0 12/31/08 dimethylcyclopropanecarboxylic acid Grass, forage ...... 5.0 12/31/08 Grass, hay ...... 6.0 12/31/08 in or on the following commodities: Rice, wild, grain ...... 1.0 12/31/08 Parts per Commodity million (c) Tolerances with regional registra- tions. [Reserved] Corn, field, fodder and forage, pop and sweet ... 0.06 Corn, fresh (including sweet K and corn with (d) Indirect or inadvertent residues. husk removed (CWHR) ...... 0.06 [Reserved] Corn, field, grain and pop ...... 0 .06 [71 FR 74817, Dec. 13, 2006] (b) Section 18 emergency exemptions. § 180.439 Thifensulfuron methyl; toler- [Reserved] ances for residues. (c) Tolerances with regional registra- tions. [Reserved] (a) General. Tolerances are estab- (d) Indirect or inadvertent residues. lished for residues of the herbicide [Reserved] thifensulfuron methyl (methyl-3-[[[[(4- methoxy-6-methyl-1,3,5-triazin-2- [62 FR 62961, Nov. 26, 1997]

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§ 180.441 Quizalofop ethyl; tolerances quizalofop-p ethyl ester [ethyl (R)-(2-[4- for residues. ((6-chloroquinoxalin-2- (a) General. (1) Tolerances are estab- yl)oxy)phenoxy)propanoate], and its lished for the combined residues of the acid metabolite quizalofop-p [R-(2-(4- herbicide quizalofop (2-[4-(6- ((6-quinoxalin-2- chloroquinoxalin-2-yl yl)oxy)phenoxy)propanoic acid], and oxy)phenoxy]propanoic acid) and the S enantiomers of both the ester and quizalofop ethyl (ethyl-2-[4-(6- the acid, all expressed as quizalofop-p- chloroquinoxalin-2-yl ethyl ester, in or on the following raw oxy)phenoxy]propanoate), all expressed agricultural commodities; as quizalofop ethyl, in or on the fol- Parts per lowing agricultural commodities: Commodity million

Parts per Barley, grain ...... 0 .05 Commodity million Barley, hay ...... 0 .05 Barley, straw ...... 0 .05 Bean, dry ...... 0.4 Beet, sugar, molasses ...... 0 .2 Bean, succulent ...... 0 .25 Canola, meal ...... 1 .5 Beet, sugar, roots ...... 0 .1 Canola, seed ...... 1 .0 Beet, sugar, tops ...... 0.5 Cotton, undelinted seed ...... 0 .1 Cowpea, forage ...... 3 .0 Flax, seed ...... 0 .05 Cowpea, hay ...... 3 .0 Lentil, seed ...... 0 .05 Pea, dry ...... 0 .25 Peppermint, tops ...... 2 .0 Pea, field, hay ...... 3.0 Spearmint, tops ...... 2 .0 Pea, field, vines ...... 3 .0≤ Sunflower, seed ...... 1.9 Pea, succulent ...... 0 .3 Wheat, forage ...... 0 .05 Soybean flour ...... 0.5 Wheat, grain ...... 0 .05 Soybean, hulls ...... 0 .02 Wheat, hay ...... 0 .05 Soybean, meal ...... 0.5 Wheat, straw ...... 0 .05 Soybean, soapstock ...... 1 .0 Soybean ...... 0.05 (4) Time limited tolerances to expire on June 14, 1999 are established for the (2) Tolerances are established for the combined residues of the herbicide combined residues of the herbicide quizalofop-p ethyl ester (ethyl (R)-(2-(4- quizalofop (2-[4-(6-chloroquinoxalin-2-yl ((6-chloroquinoxalin-2- oxy)phenoxy]propanoic acid), quizalop- yl)oxy)phenoxy)propanoate) and it acid ethyl (ethyl-2-[4-(6-chloroquinoxalin-2- metabolite quizalofop-p [R-(2-(4-((6- yl oxy)phenoxy]propanoate), and chloroquinoxalin-2- quizalofop-methyl (methyl 2-[4-(6- yl)oxy)phenoxy)propanoic acid), and chloroquinoxalin-2-yl- the S enantiomers of both the ester and oxy)phenoxy]propanoate, all expressed the acid, all expressed as quizalofop-p- as quizalofop ethyl, as follows: ethyl ester in or on the following raw Parts per agricultural commodities: Commodity million Commodities Parts per Cattle, fat ...... 0.05 million Cattle, meat ...... 0 .02 Cattle, meat byproducts ...... 0.05 Beet, sugar, molasses ...... 0 .2 Egg ...... 0 .02 Beet, sugar root ...... 0 .1 Goat, fat ...... 0 .05 Beet, sugar, tops ...... 0.5 Goat, meat ...... 0.02 Vegetable, foliage of legume, except soybean, Goat, meat byproducts ...... 0 .05 subgroup 7A ...... 3 .0 Hog, fat ...... 0 .05 Vegetable, legume, group 6 ...... 0 .25 Hog, meat ...... 0 .02 Hog, meat byproducts ...... 0 .05 (b) Section 18 emergency exemptions. Horse, fat ...... 0 .05 Horse, meat ...... 0 .02 [Reserved] Horse, meat byproducts ...... 0 .05 (c) Tolerances with regional registra- Milk ...... 0.01 tions. Tolerances with regional reg- Milk, fat ...... 0 .25 Poultry, fat ...... 0.05 istration, as defined in § 180.1(n), are es- Poultry, meat ...... 0 .02 tablished for the combined residues of Poultry, meat byproducts ...... 0.05 the herbicide quizalofop-p ethyl ester Sheep, fat ...... 0 .05 [ethyl (R)-2-[4-((6-chloroquinoxalin-2- Sheep, meat ...... 0.02 Sheep, meat byproducts ...... 0 .05 yl)oxy)phenoxy] propionate], its acid metabolite quizalofop-p [R-(2-[4-((6- (3) Tolerances are established for the chloroquinoxalin-2-yl)oxy)phenoxy]) combined residues of the herbicide propanoic acid], and the S enantiomers

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of both the ester and the acid, all ex- Commodity Parts per pressed as quizalofop-p ethyl ester, in million or the raw agricultural commodities, Poultry, fat ...... 0.05 as follows: Poultry, meat byproducts ...... 0.05 Poultry, meat ...... 0 .05 Commodity Parts per Pepper, bell ...... 0 .5 million Pepper, nonbell ...... 0 .5 Rapeseed, seed ...... 0 .05 Pineapple ...... 0.1 Sheep, fat ...... 1 .0 Sheep, meat byproducts ...... 0 .1 (d) Indirect or inadvertent residues. Sheep, meat ...... 0.5 [Reserved] Spinach ...... 0 .2 Strawberry ...... 3 .0 [63 FR 32759, June 16, 1998, as amended at 70 Tomato ...... 0.15 FR 7870, Feb. 16, 2005; 71 FR 56378, Sept. 27, Turnip, greens ...... 3.5 2006] Vegetable, cucurbit, group 9 ...... 0.4 Vegetable, legume, edible podded, subgroup 6A 0 .6 § 180.442 Bifenthrin; tolerances for res- Vegetable, tuberous and corm, subgroup 1C ..... 0.05 idues. 1 There are no U.S. registrations as of April 30, 2003. (a) General. (1) Tolerances are estab- (2) A tolerance of 0.05 ppm is estab- lished for residues of the insecticide lished for residues of the insecticide bifenthrin (2-methyl [1,1′-biphenyl]-3- bifenthrin, (2-methyl[1,1′-biphenyl]-3- yl) methyl-3-(2-chloro-3,3,3,-trifluoro-1- yl)methyl-3-(2-chloro-3,3,3-trifluoro-1- propenyl)-2,2- propenyl)-2,2-dimethylcyclopropane- dimethylcyclopropanecarboxylate in or carboxylate, as follows: on the following food commodities: (i) In or on all food/feed items (other than those covered by a higher toler- Parts per Commodity million ance as a result of use on growing crops) in food/feed handling establish- Almond, hulls ...... 2 .0 Artichoke, globe ...... 1.0 ments. Banana1 ...... 0 .1 (ii) The insecticide may be present as Brassica, head and stem, subgroup 5A, except a residue from application of bifenthrin cabbage ...... 0 .6 in food handling establishments, in- Brassica, leafy greens, subgroup 5B ...... 3 .5 Cabbage ...... 4 .0 cluding food service, manufacturing Caneberry subgroup 13A ...... 1 .0 and processing establishments, such as Cattle, fat ...... 1.0 restaurants, cafeterias, supermarkets, Cattle, meat byproducts ...... 0.10 Cattle, meat ...... 0 .5 bakeries, breweries, dairies, meat Coriander, dried leaves ...... 25 slaughtering and packing plants, and Coriander, leaves ...... 6 .0 canneries, feed handling establish- Coriander, seed ...... 5 .0 Corn, forage ...... 3 .0 ments including feed manufacturing Corn, grain (field, seed, and pop) ...... 0 .05 and processing establishments, in ac- Corn, stover ...... 5 .0 cordance with the following prescribed Corn, sweet, kernel plus cob with husk removed 0.05 conditions: Cotton, undelinted seed ...... 0 .5 Eggplant ...... 0.05 (A) Application shall be limited to Egg ...... 0 .05 general surface and spot and/or crack Fruit, citrus, group 10 ...... 0 .05 and crevice treatment in food/feed han- Goat, fat ...... 1 .0 Goat, meat byproducts ...... 0 .10 dling establishments where food/feed Goat, meat ...... 0.5 and food/feed products are held, proc- Grape ...... 0 .2 essed, prepared and served. General Herb subgroup 19A ...... 0 .05 Hog, fat ...... 1 .0 surface application may be used only Hog, meat byproducts ...... 0 .10 when the facility is not in operation Hog, meat ...... 0 .5 provided exposed food/feed has been Hop, dried cones ...... 10 .0 Horse, fat ...... 1 .0 covered or removed from the area Horse, mby ...... 0 .10 being treated. Spot and/or crack and Horse, meat ...... 0 .5 crevice application may be used while Lettuce, head ...... 3.0 the facility is in operation provided ex- Milk, fat (reflecting 0.1 ppm in whole milk) ...... 1 .0 Nut, tree, group 14 ...... 0 .05 posed food/feed is covered or removed Okra ...... 0.50 from the area being treated prior to ap- Pea and bean, dried shelled, expect soybean, plication. Spray concentration shall be subgroup 6C ...... 0 .15 Pea and bean, succulent shelled, subgroup 6B 0 .05 limited to a maximum of 0.06 percent Pear ...... 0 .5 active ingredient. Contamination of

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food/feed or food/feed contact surfaces Commodity Parts per shall be avoided. million (B) To assure safe use of the insecti- Cattle, liver ...... 1 .0 cide, its label and labeling shall con- Cattle, meat ...... 0 .1 form to that registered with the U.S. Cattle, meat byproducts, except liver ...... 0 .2 Cherry, sweet ...... 5 .0 Environmental Protection Agency and Cherry, tart ...... 5 .0 shall be used in accordance with such Cotton, undelinted seed ...... 0 .02 label and labeling. Currant ...... 3 .0 Egg ...... 0 .02 (b) Section 18 emergency exemptions. Fruit, stone (except cherry) ...... 2 .0 Time limited tolerances are estab- Goat, fat ...... 0 .05 lished for residues of the insecticide Goat, liver ...... 1.0 bifenthrin ((2-methyl [1,1′-biphenyl]-3- Goat, meat ...... 0.1 Goat, meat byproducts, except liver ...... 0 .2 yl) methyl-3-(2-chloro-3,3,3,-trifluoro-1- Gooseberry ...... 2 .0 propenyl) -2,2- Grain, aspirated fractions ...... 35 dimethylcyclopropanecarboxylate), in Grape pomace (wet and dry) ...... 10.0 Grape ...... 1 .0 connection with use of the pesticide Grape, raisin ...... 10.0 under section 18 emergency exemptions Grape, raisin, waste ...... 25 .0 granted by EPA. The tolerances will Hog, fat ...... 0 .05 Hog, liver ...... 1 .0 expire and are revoked on the dates Hog, meat ...... 0 .1 specified in the following table. Hog, meat byproducts, except liver ...... 0 .2 Hop, dried cones ...... 10 Parts per Expiration/ Horse, fat ...... 0 .05 Commodity million revocation Horse, liver ...... 1 .0 date Horse, meat ...... 0 .1 Horse, meat byproducts, except liver ...... 0 .2 Orchardgrass, forage ...... 0.05 12/31/09 Mayhaw ...... 0 .70 Orchardgrass, hay ...... 0.05 12/31/09 Milk ...... 0.2 Peppermint, tops ...... 3 .0 (c) Tolerances with regional registra- Plum, prune, dried ...... 8.0 tions. [Reserved] Poultry, fat ...... 0.02 Poultry, meat ...... 0 .02 (d) Indirect or inadvertent residues. Poultry, meat byproducts ...... 0.02 [Reserved] Sheep, fat ...... 0 .05 Sheep, liver ...... 1.0 [62 FR 31002, June 6, 1997] Sheep, meat ...... 0.1 Sheep, meat byproducts, except liver ...... 0 .2 EDITORIAL NOTE: For FEDERAL REGISTER ci- Soybean, forage ...... 3 .5 tations affecting § 180.442, see the List of CFR Soybean, hay ...... 15 Sections Affected, which appears in the Soybean, refined oil ...... 0 .40 Finding Aids section of the printed volume Soybean, seed ...... 0 .25 and on GPO Access. Spearmint, tops ...... 3 .0 Strawberry ...... 0 .50 Tomato ...... 0.30 § 180.443 Myclobutanil; tolerances for Tomato, puree ...... 0 .50 residues. Tomato, paste ...... 1 .0 (a) General. Tolerances are estab- Vegetable, cucurbit, group 9 ...... 0.20 lished for combined residues of the fun- gicide myclobutanil alpha-butyl-alpha- (b) Section 18 emergency exemptions. (4-chlorophenyl)-1H-1,2,4-triazole-1- Time-limited tolerances are estab- propanenitrile and its alcohol metabo- lished for residues of the fungicide lite (alpha-(3-hydroxybutyl)-alpha-(4- myclobutanil in connection with use of chlorophenyl)-1H-1,2,4-triazole-1- the pesticide under section 18 emer- propanenitrile (free and bound), in or gency exemptions granted by EPA. on the following food commodities: These tolerances will expire and are re- voked on the dates specified in the fol- Parts per lowing table. Commodity million Expiration/ Almond ...... 0.1 Commodity Parts per revocation Almond, hulls ...... 2 .0 million date Apple ...... 0.5 Apple, dry pomace ...... 5.0 Artichoke, globe ...... 1.0 12/31/07 Apple, wet pomace ...... 5 .0 Beet, sugar, dried pulp ...... 1.0 12/31/07 Asparagus ...... 0.02 Beet, sugar, molasses ...... 1.0 12/31/07 Banana, postharvest ...... 4 .0 Beet, sugar, refined sugar ...... 0.70 12/31/07 Bean, snap, succulent ...... 1 .0 Beet, sugar, roots ...... 0.05 12/31/07 Caneberry subgroup 13A ...... 2 .0 Beet, sugar, tops ...... 1.0 12/31/07 Cattle, fat ...... 0.05 Pepper ...... 1.0 6/30/08

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Expiration/ Parts per Commodity Parts per revocation Commodity million million date Crayfish ...... 0.05 Vegetable, foliage of legume, group Rice, grain ...... 0 .02 07 ...... 1.0 6/30/09 Rice, straw ...... 0 .3 Vegetable, legume, group 06 ...... 1.0 6/30/09 (b) Section 18 emergency exemptions. (c) Tolerances with regional registra- [Reserved] tions. [Reserved] (c) Tolerances with regional registra- (d) Indirect or inadvertent residues. tions. [Reserved] Tolerances are established for residues (d) Indirect or inadvertent residues. of the fungicide myclobutanil alpha- [Reserved] butyl-alpha-(4-chlorophenyl)-1H-1,2,4- [63 FR 9435, Feb. 25, 1998] triazole-1-propanenitrile in or on the following food commodities: § 180.446 Clofentezine; tolerances for residues. Parts per Commodity million (a) General. (1) Tolerances are estab- lished for residues of the insecticide Animal feed, nongrass, group 18 ...... 0 .03 clofentezine (3,6-bis(2-chlorophenyl)- Grain, cereal, forage, fodder and straw, group 16 ...... 0 .03 1,2,4,5-tetrazine) in or on the following Grain, cereal, group 15 ...... 0.03 raw agricultural commodities: Vegetable, brassica, leafy, group 5 ...... 0.03 Parts per Vegetable, foliage of legume, group 7 ...... 0 .03 Commodity million Vegetable, fruiting, group 8 ...... 0.03 Vegetable, leafy, except brassica, group 4 ...... 0 .03 Almond, hulls ...... 5 .0 Vegetable, leaves of root and tuber, group 2 ..... 0 .03 Almond ...... 0.5 Vegetable, legume, group 6 ...... 0 .03 Apple, pomace ...... 3.0 Vegetable, root and tuber, group 1 ...... 0 .03 Apple ...... 0.5 Apricot ...... 1 .0 Cherry ...... 1.0 [54 FR 6131, Feb. 8, 1989] Grapes ...... 1 .0 Nectarine ...... 1 .0 EDITORIAL NOTE: For FEDERAL REGISTER ci- Peach ...... 1 .0 tations affecting § 180.443, see the List of CFR Pear ...... 0 .5 Persimmons ...... 0 .05 Sections Affected, which appears in the Walnut ...... 0 .02 Finding Aids section of the printed volume and on GPO Access. (2) Tolerances are established for the combined residues of clofentezine and § 180.444 Sulfur dioxide; tolerances for the 3-(2-chloro-4-hydroxyphenyl)-6-(2- residues. chlorophenyl)-1,2,4,5-tetrazine metabo- A tolerance is established as follows lite in or on the following commod- for sulfite residues of the fungicide sul- ities: fur dioxide (determined as (SO2)) in or Parts per on the following raw agricultural com- Commodity million modity(ies): Cattle, fat ...... 0.05 Parts per Cattle, liver ...... 0 .4 Commodity million Cattle, meat ...... 0 .05 Cattle, meat byproducts, except liver ...... 0 .05 Grape, postharvest ...... 10.0 Goat, fat ...... 0 .05 Goat, liver ...... 0.4 Goat, meat ...... 0.05 [54 FR 20126, May 10, 1989] Goat, meat byproducts, except liver ...... 0 .05 Hog, fat ...... 0 .05 Hog, liver ...... 0 .4 § 180.445 Bensulfuron methyl; toler- Hog, meat ...... 0 .05 ances for residues. Hog, meat byproducts, except liver ...... 0 .05 Horse, fat ...... 0 .05 (a) General. Tolerances are estab- Horse, liver ...... 0 .4 lished for residues of the herbicide Horse, meat ...... 0 .05 bensulfuron methyl (methyl-2[[[[[(4,6- Horse, meat byproducts, except liver ...... 0 .05 Milk ...... 0.01 dimethoxy-pyrimidin-2-yl) amino] car- Sheep, fat ...... 0 .05 bonyl] amino] sulfonyl] methyl] ben- Sheep, liver ...... 0.4 zoate) in or on the following raw agri- Sheep, meat ...... 0.05 cultural commodities: Sheep, meat byproducts, except liver ...... 0 .05

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(b) Section 18 emergency exemptions. yl]-5-ethyl-3-pyridine carboxylic acid, [Reserved] and its metabolite CL 288511, 2-[4,5- (c) Tolerances with regional registra- dihydro-4-methyl-4-(1-methylethyl)-5- tions. [Reserved] oxo-1H-imidazol-2-yl]-5-(1-hydroxy- (d) Indirect or inadvertent residues. ethyl)-3-pyridine carboxylic acid, ap- [Reserved] plied as its acid or ammonium salt, in or on the following commodities: [56 FR 15503, Apr. 17, 1991, as amended at 56 FR 22335, May 15, 1991; 59 FR 26947, May 25, Parts per 1994; 60 FR 12709, Mar. 8, 1995; 64 FR 19050, Commodity million Apr. 19, 1999; 70 FR 11572, Mar. 9, 2005] Cattle, meat byproducts ...... 0.10 § 180.447 Imazethapyr; tolerances for Corn, field, forage ...... 0 .1 residues. Corn, field, grain ...... 0 .1 Corn, field, stover ...... 0 .1 (a) General. (1) Tolerances are estab- Crayfish ...... 0.15 lished for residues of the herbicide Goat, meat byproducts ...... 0 .10 Hog, meat byproducts ...... 0 .10 imazethapyr, 2-[4,5-dihydro-4-methyl-4- Horse, meat byproducts ...... 0 .10 (1-methylethyl)-5-oxo- 1H-imidazol-2- Sheep, meat byproducts ...... 0 .10 yl]-5-ethyl-3-pyridine carboxylic acid, applied as its acid or ammonium salt, (b) Section 18 emergency exemptions. in or on the following raw agricultural [Reserved] commodities: (c) Tolerances with regional registra- tions. Tolerances with regional reg- Parts per Commodity million istration, as defined in § 180.1(n) of this chapter, are established for the sum of Canola, seed1 ...... 0 .10 residues of the herbicide imazethapyr, Soybeans ...... 0.1 Vegetable, legume, group 6 ...... 0 .1 2- [4,5-dihydro-4-methyl-4-(1- methylethyl)-5-oxo-1H-imidazol-2-yl]-5- 1 There are no U.S. registrations for canola as of March 21, 2003. ethyl- 3-pyridine carboxylic acid, as its ammonium salt, and its metabolite, 2- (2) Tolerances are established for the [4,5-dihydro-4-methyl-4-(1- sum of the residues of the herbicide methylethyl)-5-oxo-1H-imidazol-2-yl]-5- imazethapyr, 2-[4,5-dihydro-4-methyl-4- (1- hydroxyethyl)-3-pyridine carboxylic (1-methylethyl)-5-oxo- 1H-imidazol-2- acid, both free and conjugated, applied yl]-5-ethyl-3-pyridine carboxylic acid; as its acid or ammonium salt, in or on its metabolite CL 288511, 2-[4,5-dihydro- the following raw agricultural com- 4-methyl-4-(1-methylethyl)-5-oxo-1H- modities: imidazol-2-yl]-5-(1-hydroxyethyl)-3-pyr- idine carboxylic acid; and its metabo- Commodity Parts per lite CL 182704, 5-[1-(beta-D- million glucopyranosyloxy)ethyl]-2-[4,5- Endive (escorole) ...... 0.1 dihydro-4-methyl-4-(1-methylethyl)-5- Lettuce, head ...... 0.1 oxo-1H-imidazol-2-yl]-3- Lettuce, leaf ...... 0 .1 pyridinecarboxylic acid, applied as its acid or ammonium salt, in or on the (d) Indirect or inadvertent residues. following commodities: [Reserved] [67 FR 55331, Aug. 29, 2002, as amended at 68 Parts per Commodity million FR 13849, Mar. 21, 2003; 71 FR 6359, Feb. 8, 2006] Alfalfa, seed ...... 0 .15 Alfalfa, seed screening ...... 0 .15 § 180.448 Hexythiazox; tolerance for Animal feed, nongrass, group, forage ...... 3 .0 Animal feed, nongrass, group, hay ...... 5.5 residues. Peanut ...... 0 .1 (a) General. Tolerances are estab- Rice, bran ...... 1.2 Rice, grain ...... 0 .3 lished for the combined residues of the Rice, straw ...... 0 .4 miticide hexythiazox, trans-5-(4- chlorophenyl)-N-cyclohexyl-4-methyl-2- (3) A tolerance is established for the oxothiazolidine-3-carboxamide and its sum of residues of the herbicide metabolites containing the (4- imazethapyr, 2-[4,5-dihydro-4-methyl-4- chlorophenyl)-4-methyl-2-oxo-3- (1-methylethyl)-5-oxo- 1H-imidazol-2- thiazolidine moiety (expressed as parts

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per million of the parent compound) in ent) in or on the following commod- or on the following commodities: ities:

Parts per Commodity Parts per Commodity million million

Almond, hulls ...... 10 Cotton, gin byproducts, CA only ...... 3 .0 Apple, wet pomace ...... 2 .5 Cotton, undelinted seed, CA only ...... 0 .20 Caneberry subgroup 13A ...... 1 .0 Fruit, citrus group 10 (CA, AZ, TX only) ...... 0 .35 Cattle, fat ...... 0.02 Cattle, meat byproducts ...... 0.12 (d) Indirect or inadvertent residues. Citrus, dried pulp ...... 1 .5 [Reserved] Citrus, oil ...... 0.90 Date, dried fruit ...... 1 .0 [54 FR 17948, Apr. 26, 1989, as amended at 61 Fruit, pome, group 11 ...... 1.7 FR 6554, Feb. 21, 1996; 62 FR 62992, Nov. 26, Fruit, stone, group 12, except plum ...... 1 .0 1997; 62 FR 68216, Dec. 31, 1997; 63 FR 17101, Goat, fat ...... 0 .02 Apr. 8, 1998; 63 FR 54599, Oct. 13, 1998; 63 FR Goat, meat byproducts ...... 0 .12 Grape ...... 0 .75 55547, Oct. 16, 1998; 65 FR 56255, Sept. 18, 2000; Hog, fat ...... 0 .02 65 FR 58450, Sept. 29, 2000; 66 FR 19891, Apr. Hog, meat byproducts ...... 0 .02 18, 2001; 67 FR 46884, July 17, 2002; 68 FR 10376, Hop ...... 2 .0 Mar. 5, 2003; 69 FR 65080, Nov. 10, 2004; 71 FR Horse, fat ...... 0 .02 14411, Mar. 22, 2006] Horse, meat byproducts ...... 0 .12 Milk ...... 0.02 § 180.449 Avermectin B1 and its delta- Nut, tree, group 14 ...... 0 .30 8,9-isomer; tolerances for residues. Peppermint, tops ...... 2 .0 Pistachio ...... 0.30 (a) General. Tolerances are estab- Plum ...... 0 .10 lished for the combined residues of the Plum, prune, dried ...... 0.40 Plum, prune, fresh ...... 0.10 insecticide avermectin B1 (a mixture of Sheep, fat ...... 0 .02 avermectins containing greater than or Sheep, meat byproducts ...... 0 .12 equal to 80% avermectin B1a (5-O- Spearmint, tops ...... 2 .0 demethyl avermectin A ) and less than Strawberry ...... 3 .0 1 or equal to 20% avermectin B1b (5-O- (b) Section 18 emergency exemptions. demethyl-25-de(1-methylpropyl)-25-(1- Time-limited tolerances are estab- methylethyl) avermectin A1)) and its lished for the combined residues of the delta-8,9-isomer in or on the following insecticide hexythiazox and its me- commodities: tabolites containing the (4- Parts per chlorophenyl)-4-methyl-2-oxo-3- Commodity million thiazolidine moiety in connection with Almond ...... 0.005 use of the pesticide under section 18 Almond, hulls ...... 0.10 emergency exemptions granted by Apple ...... 0.020 EPA. These tolerances will expire and Apple, wet pomace ...... 0.10 Avocado ...... 0.020 are revoked on the dates specified in Cattle, fat ...... 0.015 the following table. Cattle, meat byproducts ...... 0.02 Cattle, meat ...... 0.02 Parts per Expiration/ Celeriac, roots ...... 0.05 Commodity million revocation Celeriac, tops ...... 0.05 date Citrus, dried pulp ...... 0.10 Citrus, oil ...... 0.10 Corn, field, grain ...... 0.05 12/31/07 Citrus ...... 0.02 Corn, field, forage ...... 2.0 12/31/07 Cotton, gin byproducts ...... 0.15 Corn, field, stover ...... 2.0 12/31/07 Cotton, undelinted seed ...... 0.005 Cucurbits (cucumber, mellons, and squashes) 0.005 (c) Tolerances with regional registra- Food products in food handling establishments tions. Tolerances with regional reg- (other than those already covered by higher tolerances as a result of use on growing istrations as defined 40 CFR 180.1(n), crops, and other than those already covered are established for the combined resi- by tolerances on milk, meat, and meat by- dues of the ovicide/miticide products) ...... 0.01 hexythiazox (trans-5-(4-chlorophenyl)- Goat, meat ...... 0.02 Goat, meat byproducts ...... 0.02 N-cyclohexyl-4-methyl-2- Grape ...... 0.02 oxothiazolidine-3-carboxamide) and its Herbs, crop subgroup 19A (except chives) ...... 0.030 metabolites containing the (4- Hog, meat ...... 0.02 Hog, meat byproducts ...... 0.02 chlorophenyl)-4-methyl-2-oxo-3- Hop, dried cones ...... 0.20 thiazolidine moiety (expressed as par- Horse, meat ...... 0.02

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Parts per Parts per Commodity million Commodity million

Horse, meat byproducts ...... 0.02 Banana1 ...... 0 .2 Milk ...... 0.005 Barley, grain ...... 0 .05 Mint ...... 0.010 Barley, straw ...... 0 .2 Pear ...... 0.02 Corn, forage ...... 0 .05 Plum ...... 0.010 Corn, grain ...... 0 .05 Plum, prune, dried ...... 0.025 Corn, stover ...... 0 .05 Potato ...... 0.005 Corn, sweet, kernel plus cob with husks re- Poultry, meat ...... 0.02 moved ...... 0 .05 Cotton, forage ...... 0.02 Poultry, meat byproducts ...... 0.02 Cotton, undelinted seed ...... 0 .02 Sheep, meat ...... 0.02 Oat, grain ...... 0 .05 Sheep, meat byproducts ...... 0.02 Oat, forage ...... 2 .5 Strawberry ...... 0.02 Oat, straw ...... 0.2 Vegetable, fruiting, crop group 8 ...... 0.020 Rye, forage ...... 2 .5 Vegetable, leafy, except Brassica, crop group Rye, grain ...... 0.05 4 ...... 0.10 Rye, straw ...... 0 .1 Walnut ...... 0.005 Sorghum, forage, hay ...... 0 .05 Sorghum, grain ...... 0 .01 (b) Section 18 emergency exemptions. Sorghum, grain, stover ...... 0 .01 Wheat, forage ...... 2 .5 Time-limited tolerances are estab- Wheat, grain ...... 0 .05 lished for the residues of avermectin B1 Wheat, straw ...... 0 .2 and it delta-8,9-isomer, in connection 1 There are no U.S. registrations for banana (whole) as of with use of the pesticide under section September 22, 1993. 18 emergency exemptions granted by (b) Tolerances are established for the EPA. The tolerances are specified in combined residues of the fungicide the following table. The tolerances will beta-(4-chlorophenoxy)-alpha-(1,1- expire on the dates specified in the dimethylethyl)-1H-1,2,4-triazole-1-eth- table. anol (triadimenol) and its metabolites containing the chlorophenoxy moiety, Parts per Expiration/ Commodity million revocation calculated as triadimenol, in or on the date following commodities: Onion, bulb ...... 0.005 12/31/09 Parts per Commodity million (c) Tolerances with regional registra- tions. [Reserved] Cattle, fat ...... 0.1 Cattle, meat ...... 0 .1 (d) Indirect or inadvertent residues. Cattle, meat byproducts ...... 0.1 [Reserved] Egg ...... 0 .01 Goat, fat ...... 0 .1 [62 FR 44095, Aug. 19, 1997, as amended at 62 Goat, meat ...... 0.1 FR 56088, Oct. 29, 1997; 63 FR 42248, Aug. 7, Goat, meat byproducts ...... 0 .1 1998; 63 FR 53837, Oct. 7, 1998; 64 FR 16850, Hog, fat ...... 0 .1 Apr. 7, 1999; 64 FR 48560, Sept. 7, 1999; 64 FR Hog, meat ...... 0 .1 Hog, meat byproducts ...... 0 .1 63711, Nov. 22, 1999; 65 FR 47877, Aug. 4, 2000; Horse, fat ...... 0 .1 65 FR 76174, Dec. 6, 2000; 65 FR 80336, 80361, Horse, meat ...... 0 .1 Dec. 21, 2000; 66 FR 37598, July 19, 2001; 66 FR Horse, meat byproducts ...... 0 .1 64774, Dec. 14, 2001; 67 FR 35049, May 17, 2002; Milk ...... 0.01 69 FR 2074, Jan. 14, 2004; 70 FR 7886, Feb. 16, Poultry, fat ...... 0.01 2005; 72 FR 5629, Feb. 7, 2007] Poultry, meat ...... 0 .01 Poultry, meat byproducts ...... 0.01 Sheep, fat ...... 0 .1 § 180.450 Beta-(4-Chlorophenoxy)- Sheep, meat ...... 0.1 alpha-(1,1-dimethylethyl)-1H-1,2,4- Sheep, meat byproducts ...... 0 .1 triazole-1-ethanol; tolerances for residues. [54 FR 31836, Aug. 2, 1989, as amended at 58 (a) Tolerances are established for the FR 46087, Sept. 1, 1993; 58 FR 62039, Nov. 24, combined residues of the fungicide 1993; 59 FR 44935, Aug. 31, 1994] beta-(4-chlorophenoxy)-alpha-(1,1-di- methyl-ethyl)-1H-1,2,4-triazole-1-eth- § 180.451 Tribenuron methyl; toler- anol (triademenol) and its butanediol ances for residues. metabolite, 4-(4-chlorophenoxy)-2,2-di- (a) General. Tolerances are estab- methyl-4-(1H-1,2,4-triazol-l-yl)-1,3- lished for the residues of the herbicide butanediol, calculated as triadimenol, tribenuron methyl (methyl-2-[[[[N-(4- in or on the following commodities: methoxy-6-methyl-1,3,5-triazin-2-yl)

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methylamino] car- Commodity Parts per bonyl]amino]sulfonyl] benzoate) in or million on the following raw agricultural com- Cattle, fat ...... 0.10 modities: Cattle, meat ...... 0 .10 Cattle, meat byproducts ...... 0.10 Corn, forage ...... 0 .10 Commodity Parts per million Corn, fresh (including sweet kernels plus cobs with husks removed) ...... 0 .10 Barley, grain ...... 0 .05 Corn, grain ...... 0 .02 Barley, straw ...... 0 .10 Corn, stover ...... 0 .10 Canola, seed ...... 0 .02 Egg ...... 0 .10 Corn, field, forage ...... 0 .05 Goat, fat ...... 0 .10 Corn, field, grain ...... 0 .05 Goat, meat ...... 0.10 Corn, field, stover ...... 0 .05 Goat, meat byproducts ...... 0 .10 Cotton, gin byproducts ...... 0 .02 Hog, fat ...... 0 .10 Cotton, undelinted seed ...... 0 .02 Hog, meat ...... 0 .10 Flax, seed ...... 0 .02 Hog, meat byproducts ...... 0 .10 Oat, grain ...... 0 .05 Horse, fat ...... 0 .10 Oat, straw ...... 0.10 Horse, meat ...... 0 .10 Rice, grain ...... 0 .05 Horse, meat byproducts ...... 0 .10 Milk ...... 0.02 Rice, straw ...... 0 .05 Poultry, fat ...... 0.10 Sorghum, grain, forage ...... 0.05 Poultry, meat ...... 0 .10 Sorghum, grain, grain ...... 0 .05 Poultry, meat byproducts ...... 0.10 Sorghum, grain, stover ...... 0 .05 Sheep, fat ...... 0 .10 Soybean, seed ...... 0 .05 Sheep, meat ...... 0.10 Sunflower, seed ...... 0.05 Sheep, meat byproducts ...... 0 .10 Wheat, grain ...... 0 .05 Wheat, straw ...... 0 .10 (b) Section 18 emergency exemptions. [Reserved] (b) Section 18 emergency exemptions. (c) Tolerances with regional registra- [Reserved] tions. [Reserved] (c) Tolerances with regional registra- (d) Indirect or inadvertent residues. tions. Tolerances with regional reg- [Reserved] istration, as defined in § 180.1(n) are es- tablished for residues of the herbicide [55 FR 21548, May 25, 1990, as amended at 62 tribenuron methyl (methyl-2-[[[[N-(4- FR 66020, Dec. 17, 1997; 63 FR 66458, Dec. 2, methoxy-6-methyl-1,3,5-triazin-2-yl) 1998; 67 FR 35049, May 17, 2002] methylamino] car- § 180.454 Nicosulfuron, [3-pyridinecar- bonyl]amino]sulfonyl] benzoate) in or boxamide, 2-((((4,6-dimethoxypyri- on the following raw agricultural com- midin-2- modities: yl)aminocarbonyl)aminosulfonyl))- N,N-dimethyl]; tolerances for resi- Parts per dues. Commodity million Tolerances are established for the Grass, forage, fodder and hay, group (except residues of the herbicide nicosulfuron Bermudagrass); forage ...... 0 .10 Grass, forage, fodder and hay, group (except [3-pyridinecarboxamide, 2-((((4,6- Bermudagrass); hay ...... 0 .10 dimethoxypyrimidin-2- yl)aminocarbonyl)aminosulfonyl))-N,N- (d) Indirect or inadvertent residues. dimethyl] in or on the following raw [Reserved] agricultural commodities:

[69 FR 56718, Sept. 22, 2004, as amended at 72 Parts per FR 11789, Mar. 14, 2007] Commodity million

Corn, field, forage ...... 0 .1 § 180.452 Primisulfuron-methyl; toler- Corn, forage ...... 0 .1 ances for residues. Corn, grain ...... 0 .1 (a) General. Tolerances are estab- Corn, stover ...... 0 .1 Corn, sweet, kernel plus cob with husks re- lished for residues of primisulfuron- moved ...... 0 .1 methyl (3-[4,6-bis-(difluoromethoxy)- Corn, sweet, fodder (stover) ...... 0 .1 pyrimidin-2-yl]-1-(2- Corn, sweet, forage ...... 0 .1 methoxycarbonylphenylsulfonyl) urea) in or on the following raw agricultural [55 FR 28621, July 12, 1990, as amended at 61 commodities. FR 7734, Feb. 29, 1996]

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§ 180.455 Procymidone; tolerances for anol in or on the following raw agricul- residues. tural commodity:

A tolerance is established for the res- Parts per idues of the fungicide procymidone, N- Commodity million (3,5-dichlorophenyl)-1,2- dimethylcyclopropane-1,2 Banana ...... 0.2 dicarboximide, in or on the following raw agricultural commodity: There are no U.S. registrations as of April 1, 1992. Parts per Commodity million [57 FR 29032, June 30, 1992] Grape, wine ...... 5 .0 § 180.458 Clethodim; tolerances for res- idues. [59 FR 42514, Aug. 18, 1994] (a) General. (1) Tolerances are estab- lished for the combined residues of the § 180.456 Oxadixyl; tolerances for resi- herbicide clethodim ((E)-(±)-2-[1-[[(3- dues. chloro-2-propenyl)oxy]imino]propyl]-5- (a) General. Tolerances are estab- [2-(ethylthio)propyl]-3-hydroxy-2-cyclo- lished for the combined residues of the hexen-1-one) and its metabolites con- fungicide oxadixyl [2-methoxy-N-(2- taining the 2-cyclohexen-1-one moiety oxo-1,3-oxazolidin-3-yl)-acet-2′,6′- in or on the following raw agricultural xylidide] and its desmethyl (M-3) me- commodities. tabolite (2-hydroxy-N-(2-oxo-1,3- oxazolidin-3-yl)-acet-2′,6′-xylidide), cal- Commodity Parts per culated as oxadixyl in or on the fol- million lowing raw agricultural commodities: Cattle, fat ...... 0.2 Cattle, meat ...... 0 .2 Expiration/ Cattle, meat byproducts ...... 0.2 Commodity Parts per Revocation million Date Cotton, undelinted seed ...... 1 .0 Egg ...... 0 .2 Animal feed, nongrass, group, 18 ... 0.1 9/27/03 Goat, fat ...... 0 .2 Cotton, undelinted seed ...... 0.1 9/27/03 Goat, meat ...... 0.2 Grain, cereal, group 15, except Goat, meat byproducts ...... 0 .2 wheat ...... 0.1 9/27/03 Hog, fat ...... 0 .2 Grass, forage, fodder and hay, Hog, meat ...... 0 .2 group 17 ...... 0.1 9/27/03 Hog, meat byproducts ...... 0 .2 Pea ...... 0.1 9/27/03 Horse, fat ...... 0 .2 Soybean ...... 0.1 9/27/03 Horse, meat ...... 0 .2 Sunflower, seed ...... 0.1 9/27/03 Horse, meat byproducts ...... 0 .2 Vegetable, brassica, leafy, group 5 0.1 9/27/03 Milk ...... 0.05 Vegetable, cucurbit, group 9 ...... 0.1 9/27/03 Vegetable, fruiting, group 8 ...... 0.1 9/27/03 Potato ...... 0 .5 Vegetable, leafy, except brassica, Poultry, fat ...... 0.2 group 4 ...... 0.1 9/27/03 Poultry, meat ...... 0 .2 Vegetable, root and tuber, group 1 0.1 9/27/03 Poultry, meat byproducts ...... 0.2 Sheep, fat ...... 0 .2 (b) Section 18 emergency exemptions. Sheep, meat ...... 0.2 Sheep, meat byproducts ...... 0 .2 [Reserved] Soybean ...... 10.0 (c) Tolerances with regional registra- tions. [Reserved] (2) Time limited tolerances are estab- (d) Indirect or inadvertent residues. lished for the combined residues of [Reserved] clethodim, ((E)-(±)-2-[1-[[(3-chloro-2- [67 FR 45642, July 10, 2002] propenyl)oxy]imino]propyl]-5-[2- ethylthio)propyl]-3-hydroxy-2-cyclo- § 180.457 Beta-([1,1′-biphenyl]-4-yloxy)- hexen-1-one) and its metabolites con- alpha-(1,1-dimethylethyl)-1H-1,2,4- taining the 5-(2- triazole-1-ethanol; tolerances for ethylthiopropyl)cyclohexene-3-one and residues. 5-(2-(ethylthiopropyl)-5- A tolerance is established for the res- hydroxycyclohexene-3-one moieties idues of the fungicide beta-([1,1′- and their sulphoxides and sulphones, biphenyl]-4-yloxy)-alpha-(1,1- expressed as clethodim in or on the fol- dimethylethyl)-1H-1,2,4-triazole-1-eth- lowing raw agricultural commodities:

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(4) Tolerances are established for res- Parts per Expiration/ Commodity Revocation idues of the herbicide clethodim ((E)- million Date (±)-2-[1-[[(3-chloro-2-pro- Tomato, paste ...... 3 4/30/03 penyl)oxy]imino]propyl]-5-[2- Tomato, puree ...... 2 4/30/03 (ethylthio)propyl]-3-hydroxy-2-cyclo- hexen-1-one) and its metabolites con- (3) Tolerances are established for the taining the 2-cyclohexen-1-one moiety combined residues of the herbicide in or on the following feeds. clethodim [(E)-(±)-2-[1-[[(3-chloro-2-pro- penyl)oxy]imino]propyl]-5-[2- Feed Parts per (ethylthio)propyl]-3-hydroxy-2-cyclo- million hexen-1-one] and its metabolites con- Cotton, meal ...... 2 .0 taining the 5-(2- Soybean, soapstock ...... 15 .0 ethylthiopropyl)cyclohexen-3-one and 5-(2-ethylthiopropyl)-5- (b) Section 18 emergency exemptions. hydroxycyclohexen-3-one moieties and [Reserved] their sulphoxides and sulphones, ex- (c) Tolerances with regional registra- pressed as clethodim tolerance residues tions. [Reserved] for the following commodities. (d) Indirect or inadvertent residues. [Reserved] Parts per Commodity million [59 FR 4835, Feb. 2, 1994, as amended at 60 FR 33360, June 28, 1995; 60 FR 40505, Aug. 9, 1995; Alfalfa, forage ...... 6.0 63 FR 17108, Apr. 8, 1998; 66 FR 14837, Mar. 14, Alfalfa, hay ...... 10 2001; 66 FR 30080, June 5, 2001; 66 FR 30333, Asparagus ...... 1.7 June 6, 2001; 66 FR 47979, Sept. 17, 2001; 66 FR Bean, dry, seed ...... 2 .5 Beet, sugar, molasses ...... 1 .0 67493, Dec. 31, 2001; 67 FR 46900, July 17, 2002; Beet, sugar, roots ...... 0 .20 70 FR 7047, Feb. 10, 2005; 72 FR 26316, May 9, Beet, sugar, tops ...... 1.0 2007] Brassica, head and stem, subgroup 5A ...... 3 .0 Brassica, leafy greens, subgroup 5B ...... 3 .0 § 180.459 Triasulfuron; tolerances for Canola, meal ...... 1 .0 residues. Canola, seed ...... 0 .50 Cranberry ...... 0 .50 (a) General. Tolerances are estab- Clover, forage ...... 10.0 lished for residues of the herbicide Clover, hay ...... 20.0 triasulfuron [3-(6-methoxy-4-methyl- Flax, meal ...... 1 .0 Flax, seed ...... 0 .50 1,3,5-triazin-2-yl)-1-(2-(2- Flax seed ...... 0 .6 chloroethoxy)phenylsulfonyl)urea] in Herb subgroup 19A ...... 12.0 or on the following raw agricultural Hop, dried cones ...... 0 .5 commodities: Leaf petioles subgroup 4B ...... 0 .60 Leafy greens subgroup 4A ...... 2 .0 Parts per Lettuce, leaf ...... 2 .0 Commodity million Melon subgroup 9A ...... 2 .0 Mustard, seed ...... 0 .50 Barley, grain ...... 0 .02 Onion, dry bulb ...... 0 .20 Barley, straw ...... 2 .0 Onion, green ...... 2 .0 Cattle, fat ...... 0.1 Peanut ...... 3 .0 Cattle, kidney ...... 0 .5 Peanut, hay ...... 3.0 Cattle, meat byproducts, except kidney ...... 0.1 Peanut, meal ...... 5 .0 Cattle, meat ...... 0 .1 Peppermint, tops ...... 5 .0 Goat, fat ...... 0 .1 Potato, granules/flakes ...... 2 .0 Goat, kidney ...... 0 .5 Radish, tops ...... 0 .70 Goat, meat byproducts, except kidney ...... 0 .1 Safflower, meal ...... 10.0 Goat, meat ...... 0.1 Safflower, seed ...... 5 .0 Grass, forage ...... 7 .0 Sesame, seed ...... 0 .35 Grass, hay ...... 2 .0 Spearmint, tops ...... 5 .0 Hog, fat ...... 0 .1 Spinach ...... 2 .0 Hog, kidney ...... 0.5 Squash/cucumber subgroup 9B ...... 0.50 Hog, meat byproducts ...... 0 .1 Strawberry ...... 3 .0 Hog, meat ...... 0 .1 Sunflower, meal ...... 10 .0 Horse, fat ...... 0 .1 Sunflower, seed ...... 5.0 Horse, kidney ...... 0 .5 Turnip, greens ...... 3.0 Horse, meat byproducts, except kidney ...... 0 .1 Vegetable, fruiting, group 8 ...... 1.0 Horse, meat ...... 0 .1 Vegetable, legume group 6, except soybean ..... 3.5 Milk ...... 0.02 Vegetable, root, except sugar beet, subgroup Sheep, fat ...... 0 .1 1B ...... 1 .0 Sheep, kidney ...... 0.5 Vegetable, tuberous and corm, subgroup 1C ..... 1.0 Sheep, meat byproducts, except kidney ...... 0 .1 Sheep, meat ...... 0.1

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herbicide pyridate (O-(6-chloro-3- Commodity Parts per million phenyl-4-pyridazinyl)-S-octyl- Wheat, forage ...... 5 .0 carbonothioate), the metabolite 6- Wheat, grain ...... 0 .02 chloro-3-phenyl-pyridazine-4-ol and Wheat, straw ...... 2 .0 conjugates of 6-chloro-3-phenyl-pyrid- azine-4-ol, expressed as pyridate, in or (b) Section 18 emergency exemptions. on the following raw agricultural com- [Reserved] modities: (c) Tolerances with regional registra- tions. [Reserved] Commodity Parts per (d) Indirect or inadvertent residues. million [Reserved] Brassica, head and stem, subgroup 5A ...... 0 .03 Cabbage ...... 0 .03 [60 FR 36731, July 18, 1995, as amended at 63 Chickpea, seed ...... 0 .1 FR 44152, Aug. 18, 1998; 63 FR 66449, Dec. 2, Collards ...... 0.03 1998] Corn, field, forage ...... 0 .03 Corn, grain ...... 0 .03 § 180.460 Benoxacor; tolerances for Corn, stover ...... 0 .03 residues. Peanut ...... 0 .03 Peppermint, tops ...... 0 .20 (a) General. Tolerances are estab- Spearmint, tops ...... 0 .20 lished for residues of the inert ingre- dient (safener) benoxacor (4- (b) Section 18 emergency exemptions. (dichloroacetyl)-3,4-dihydro-3-methyl- [Reserved] 2H-1, 4-benzoxazine) at 0.01 parts per (c) Tolerances with regional registra- million (ppm) when used in pesticide tions. [Reserved] formulations containing metolachlor (d) Indirect or inadvertent residues. or S-metolachlor in or on raw agricul- [Reserved] tural commodities for which tolerances [57 FR 54303, Nov. 18, 1992, as amended at 62 have been established for metolachlor FR 44558, Aug. 22, 1997; 63 FR 53844, Oct. 7, or S-metolachlor. 1998; 64 FR 46298, Aug. 25, 1999; 65 FR 25652, (b) Section 18 energency exemptions. May 3, 2000; 67 FR 35049, May 17, 2002; 72 FR [Reserved] 35665, June 29, 2007] (c) Tolerances with regional registra- tions. [Reserved] § 180.463 Quinclorac; tolerances for (d) Indirect or inadvertent residues. residues. [Reserved] (a) General. Tolerances are estab- lished for residues of quinclorac (3,7- [63 FR 7305, Feb. 13, 1998, as amended at 70 dichloro-8-quinoline carboxylic acid) in FR 21631, Apr. 27, 2005] or the following food commodities:

§ 180.461 Cadusafos; tolerances for res- Parts per idues. Commodity million

A tolerance is established for the res- Cattle, fat ...... 0.7 idues of the nematicide/insecticide Cattle, meat byproducts ...... 1.5 cadusafos, O-ethyl S,S-di-sec-butyl Cattle, meat ...... 0 .05 Egg ...... 0 .05 phosphorodithioate, in or on the fol- Goat, fat ...... 0 .7 lowing raw agricultural commodity: Goat, meat byproducts ...... 1 .5 Goat, meat ...... 0.05 Commodity Parts per Grain, aspirated fractions ...... 1200 million Hog, fat ...... 0 .7 Hog, meat byproducts ...... 1 .5 Banana ...... 0.01 Hog, meat ...... 0 .05 Horse, fat ...... 0 .7 There are no U.S. registrations as of Horse, meat byproducts ...... 1 .5 Horse, meat ...... 0 .05 May 10, 1994, for the nematicide/ Milk ...... 0.05 insecticid cadusafos. Poultry, fat ...... 0.05 Poultry, meat byproducts ...... 0.1 [59 FR 39467, Aug. 3, 1994] Poultry, meat ...... 0 .05 Rice, bran ...... 15.0 § 180.462 Pyridate; tolerances for resi- Rice, grain ...... 5 .0 dues. Rice, straw ...... 12 .0 Sheep, fat ...... 0 .7 (a) General. Tolerances are estab- Sheep, meat byproducts ...... 1 .5 lished for the combined residues of the Sheep, meat ...... 0.05

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(b) Section 18 emergency exemptions. A Commodity Parts per million time-limited tolerance is established Sorghum, grain, forage ...... 3.0 for residues of dimethenamid-p, 1-(RS)- Sorghum, grain, grain ...... 6 .0 2-chloro-N-[(1-methyl-2- Sorghum, grain, stover ...... 1 .0 methoxy)ethyl]-N-(2,4-dimethylthien-3- Wheat, forage ...... 1 .0 Wheat, germ ...... 0 .75 yl)-acetamide in or on the following Wheat, grain ...... 0 .5 commodity: Wheat, hay ...... 0 .5 Wheat, straw ...... 0 .1 Expiration/ Commodity Parts per revocation million date (b) Section 18 emergency exemptions. [Reserved] Squash, winter ...... 0.01 06/30/09 (c) Tolerances with regional registra- tions. [Reserved] (c) Tolerances with regional registra- (d) Indirect or inadvertent residues. tions. [Reserved] [Reserved] (d) Indirect or inadvertent residues. [Reserved] [57 FR 47996, Oct. 21, 1992, as amended at 64 FR 6548, 6549, Feb. 10, 1999; 64 FR 14632, Mar. [65 FR 51551, Aug. 24, 2000, as amended at 67 26, 1999; 65 FR 33701, May 24, 2000; 67 FR 35049, FR 46884, July 17, 2002; 69 FR 29459, May 24, May 17, 2002] 2004; 69 FR 57207, Sept. 24, 2004; 70 FR 24712, May 11, 2005; 71 FR 25942, May 3, 2006; 71 FR § 180.464 Dimethenamid; tolerances for 49354, Aug. 23, 2006] residues. (a) General. Tolerances are estab- § 180.465 4-(Dichloroacetyl)-1-oxa-4- azaspiro[4.5]decane. lished for residues of the herbicide dimethenamid, 1(R,S)-2-chloro-N-[(1- (a) General. Tolerances are estab- methyl-2-methoxy)ethyl]-N-(2,4- lished for the residues of 4- dimethylthien-3-yl)-acetamide, applied (dichloroacetyl)-1-oxa-4- as either the 90:10 or 50:50 S:R isomers, azaspiro[4.5]decane, (CAS No. 71526–07– in or on the following food commod- 3) when used as an inert ingredient ities: (safener) in or on the following raw ag- ricultural commodities: Parts per Commodity million 1 Parts per mil- Commodity lion Bean, dry, seed ...... 0 .01 Beet, garden, roots ...... 0 .01 Corn, field, forage ...... 0.005 Beet, garden, tops ...... 0 .01 Corn, field, grain ...... 0.005 Beet, sugar, dried pulp ...... 0 .01 Corn, field, stover ...... 0.005 Beet, sugar, molasses ...... 0 .01 Corn, pop, grain ...... 0.005 Beet, sugar, roots ...... 0 .01 Corn, pop, stover ...... 0.005 Beet, sugar, tops ...... 0.01 Corn, field, forage ...... 0 .01 1There are no U.S. registered products containing 4- Corn, field, grain ...... 0 .01 (dichloroacetyl)-1-oxa-4-azaspiro[4.5]decane as of June 17, 2002. Corn, field, stover ...... 0 .01 Corn, pop, forage ...... 0 .01 (b) Section 18 emergency exemptions. Corn, pop, grain ...... 0.01 Corn, pop, stover ...... 0.01 [Reserved] Corn, sweet, forage ...... 0 .01 (c) Tolerances with regional registra- Corn, sweet, kernel plus cob with husks re- tions. [Reserved] moved ...... 0 .01 (d) Indirect or inadvertent residues. Corn, sweet, stover ...... 0 .01 Garlic ...... 0 .01 [Reserved] Horseradish ...... 0.01 Leek ...... 0 .01 [68 FR 4392, Jan. 29, 2003] Onion, dry bulb ...... 0 .01 Onion, green ...... 0 .01 § 180.466 Fenpropathrin; tolerances for Onion, Welsh ...... 0 .01 residues. Peanut, hay ...... 0.01 Peanut, nutmeat ...... 0 .01 (a) General. Tolerances are estab- Shallot, bulb ...... 0 .01 lished for residues of the pesticide Shallot, fresh leaves ...... 0 .01 chemical fenpropathrin (alpha-cyano-3- Sorghum, grain ...... 0 .01 Sorghum, grain, forage ...... 0.01 phenoxy-benzyl 2,2,3,3- Sorghum, grain, stover ...... 0 .01 tetramethylcyclopropanecarboxylate) Soybean, seed ...... 0 .01 in or on the following agricultural Vegetable, tuberous and corm, subgroup 1C ..... 0.01 commodities:

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Commodity Parts per § 180.467 Carbon disulfide; tolerances million for residues. Brassica, head and stem, subgroup 5A ...... 3 .0 Tolerances are established for the Bushberry subgroup 13B ...... 3 .0 nematicide, insecticide, and fungicide Cattle, fat ...... 1.0 Cattle, meat byproducts ...... 0.1 carbon disulfide, from the application Cattle, meat ...... 0 .1 of sodium tetrathiocarbonate, in or on Citrus, dried pulp ...... 4 .0 the following raw agricultural com- Citrus, oil ...... 75 Cotton, undelinted seed ...... 1 .0 modities: Cotton, oil ...... 3 .0 Egg ...... 0 .05 Commodity Parts per Fruit, citrus, group 10 ...... 2 .0 million Fruit, pome, group 11 ...... 5.0 Goat, fat ...... 1 .0 Almond ...... 0.1 Goat, meat byproducts ...... 0 .1 Almond, hulls ...... 0 .1 Grapefruit ...... 0 .1 Goat, meat ...... 0.1 Grape ...... 0 .1 Grape ...... 5 .0 Lemon ...... 0.1 Grape, raisin ...... 10.0 Orange, sweet ...... 0 .1 Hog, fat ...... 1 .0 Peach ...... 0 .1 Hog, meat byproducts ...... 0 .1 Plum, prune, fresh ...... 0.1 Hog, meat ...... 0 .1 Horse, fat ...... 1 .0 Horse, meat byproducts ...... 0 .1 [58 FR 33771, June 21, 1993, as amended at 62 Horse, meat ...... 0 .1 FR 26949, May 16, 1997] Juneberry ...... 3 .0 Lingonberry ...... 3.0 Melon subgroup 9–A ...... 0.5 § 180.468 Flumetsulam; tolerances for Milkfat (reflecting 0.08 ppm in whole milk) ...... 2 .0 residues. Pea, succulent ...... 0 .02 Peanut, hay ...... 20.0 Tolerances are established for resi- Peanut ...... 0 .01 dues of the herbicide flumetsulam, N- Poultry, fat ...... 0.05 (2,6-difluorophenyl)-5-methyl-(1,2,4)- Poultry, meat byproducts ...... 0.05 Poultry, meat ...... 0 .05 triazolo-[1,5a]-pyrimidine-2-sul- Salal ...... 3 .0 fonamide, in or on the following raw Sheep, fat ...... 1 .0 agricultural commodities: Sheep, meat byproducts ...... 0 .1 Sheep, meat ...... 0.1 Parts per Squash/Cucumber subgroup 9B ...... 0 .5 Commodity million Strawberry ...... 2 .0 Vegetable, fruiting, group 8 ...... 1.0 Beans (dry) ...... 0 .05 Corn, field, grain ...... 0 .05 (b) Section 18 emergency exemptions. Corn, field, forage ...... 0 .05 Corn, field, stover ...... 0 .05 Time-limited tolerances are estab- Soybean ...... 0.05 lished for residues of the herbicide fenpropathrin in connection with use of [58 FR 57967, Oct. 28, 1993, as amended at 71 the pesticide under section 18 emer- FR 58518, Oct. 4, 2006] gency exemptions granted by EPA. The tolerance will expire and is revoked on § 180.469 Dichlormid; tolerances for the date specified in the following residues. table. (a) General. Tolerances are estab- lished for residues of dichormid; (Acet- Parts per Expiration/ Commodity million Revocation amide, 2,2-dichloro-N,N-di-2-propenyl-) Date (CAS Reg. No. 37764–25–3) when used as Currant ...... 15 12/31/08 an inert ingredient (herbicide safener) in pesticide formulations in or on the (c) Tolerances with regional registra- following food commodities: tions. [Reserved] Expiration/ (d) Indirect or inadvertent residues. Commodity Parts per revocation [Reserved] million date [62 FR 63034, Nov. 26, 1997, as amended at 63 Corn, field, forage ...... 0.05 12/31/08 FR 48116, Sept. 9, 1998; 64 FR 3009, Jan. 20, Corn, field, grain ...... 0.05 12/31/08 1999; 65 FR 11242, Mar. 2, 2000; 65 FR 24397, Corn, field, stover ...... 0.05 12/31/08 Apr. 26, 2000; 65 FR 48620, Aug. 9, 2000; 66 FR Corn, pop, grain ...... 0.05 12/31/08 Corn, pop, stover ...... 0.05 12/31/08 64774, Dec. 14, 2001; 67 FR 35049, May 17, 2002; Corn, sweet, forage ...... 0.05 12/31/08 70 FR 38789, July 6, 2005; 70 FR 55747, Sept. 23, Corn, sweet, kernel plus cob with 2005] husks removed ...... 0.05 12/31/08

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growing crops in paragraph (a) of this Parts per Expiration/ Commodity revocation section: million date

Corn, sweet, stover ...... 0.05 12/31/08 Parts per Commodity million

(b) Section 18 emergency exemptions. Animal feed, nongrass, group 18, forage ...... 1 .3 [Reserved] Animal feed, nongrass, group 18, hay ...... 3.5 Beet, sugar, root ...... 0 .05 (c) Tolerances with regional registra- Beet, sugar, tops ...... 0.05 tions. [Reserved] Grain, cereal, forage, fodder and straw, group (d) Indirect or inadvertent residues. 16, except corn, grain sorghum, rice and [Reserved] wheat, forage ...... 0 .5 Grain, cereal, forage, fodder and straw, group [65 FR 16149, Mar. 27, 2000, as amended at 67 16, except corn, grain sorghum, rice and wheat, hay ...... 2 .0 FR 51105, Aug. 7, 2002; 69 FR 58290, Sept. 30, Grain, cereal, forage, fodder and straw, group 2004; 70 FR 76699, Dec. 28, 2005] 16, except corn, grain sorghum, rice and wheat, stover ...... 0 .1 § 180.470 Acetochlor; tolerances for Grain, cereal, forage, fodder and straw, group residues. 16, except corn, grain sorghum, rice and wheat, straw ...... 0 .3 (a) General. Tolerances are estab- Grain, cereal, group 15, except corn, grain sor- lished for residues of acetochlor; 2- ghum, rice, and wheat, grain ...... 0.05 chloro-2’-methyl-6-ethyl-N- Pea and bean, dried shelled, except soybean, subgroup 6C ...... 0 .05 ethoxymethylacetanilide, and its me- Potato ...... 0 .05 tabolites containing the ethyl methyl Soybean, forage ...... 0 .7 aniline (EMA) moiety and the hydroxy- Soybean, hay ...... 1 .0 Soybean, seed ...... 0 .1 ethyl methyl aniline (HEMA) moiety, Sunflower, seed ...... 0.05 to be analyzed as acetochlor and ex- Wheat, forage ...... 0 .5 pressed as acetochlor equivalents, in or Wheat, grain ...... 0 .02 on the following raw agricultural com- Wheat, hay ...... 2 .0 Wheat, straw ...... 0 .1 modities.

Parts per [72 FR 27468, May 16, 2007] Commodity million § 180.471 Furilazole; tolerances for res- Corn, field, forage ...... 3 .0 Corn, field, grain ...... 0 .05 idues. Corn, field, stover ...... 1 .5 (a) General. Tolerances are estab- Corn, pop, grain ...... 0.05 lished for residues of furilazole; 3- Corn, pop, stover ...... 1.5 Corn, sweet, forage ...... 1 .5 dichloroacetyl-5-(2-furanyl)-2, 2- Corn, sweet, kernels plus cob with husks re- dimethyloxazolidine (CAS Reg. No. moved ...... 0 .05 121776–33–8) when used as an inert in- Corn, sweet, stover ...... 1 .0 gredient (safener) in pesticide formula- Sorghum, grain, forage ...... 1.6 Sorghum, grain, grain ...... 0 .05 tions in or on the following raw agri- Sorghum, grain, stover ...... 1 .7 cultural commodities when applied at an annual application rate of 0.1 pound (b) Section 18 emergency exemptions. of safener per acre: [Reserved] Parts per (c) Tolerances with regional registra- Commodity million tions. [Reserved] (d) Indirect or inadvertent residues. Corn, field, forage ...... 0 .01 Corn, field, grain ...... 0 .01 Tolerances are established for indirect Corn, field, stover ...... 0 .01 or inadvertent residues of acetochlor; Corn, pop, grain ...... 0.01 2-chloro-2’-methyl-6-ethyl-N- Corn, pop, stover ...... 0.01 ethoxymethylacetanilide, and its me- tabolites containing the ethyl methyl (b) Section 18 emergency exemptions. aniline (EMA) moiety and the hydroxy- [Reserved] ethyl methyl aniline (HEMA) moiety, (c) Tolerances with regional registra- to be analyzed as acetochlor and ex- tions. [Reserved] pressed as acetochlor equivalents, in or (d) Indirect or inadvertent residues. on the following raw agricultural com- [Reserved] modities when present therein as a re- [65 FR 8867, Feb. 23, 2000, as amended at 67 sult of application of acetochlor to the FR 15735, Apr. 3, 2002]

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§ 180.472 Imidacloprid; tolerances for Commodity Parts Per residues. Million (a) General. Tolerances are estab- Grape, raisin, waste ...... 15 .0 lished permitting the combined resi- Grape ...... 1 .0 Guava ...... 1 .0 dues of the insecticide imidacloprid (1- Herbs subgroup 19A, dried herbs ...... 48 .0 [6-chloro-3-pyridinyl) methyl]-N-nitro- Herbs subgroup 19-A, fresh herbs ...... 8 .0 2-imidazolidinimine) and its metabo- Hog, fat ...... 0 .3 Hog, meat byproducts ...... 0 .3 lites containing the 6-chloropyridinyl Hog, meat ...... 0 .3 moiety, all expressed as 1-[(6-chloro-3- Hop, dried cones ...... 6 .0 pyridinyl)methyl]-N-nitro-2- Horse, fat ...... 0 .3 Horse, meat byproducts ...... 0 .3 imidazolidinimine, in or on the fol- Horse, meat ...... 0 .3 lowing food commodities: Huckleberry ...... 3 .5 Ilama ...... 0 .30 Commodity Parts Per Jaboticaba ...... 1 .0 Million Juneberry ...... 3 .5 Kava, leaves ...... 4 .0 Acerola ...... 1.0 Kava, roots ...... 0 .40 Almond, hulls ...... 4 .0 Leaf petioles subgroup 4B ...... 6 .0 Apple ...... 0.5 Leafy greens subgroup 4A ...... 3 .5 Apple, wet pomace ...... 3 .0 Lettuce, head and leaf ...... 3 .5 Aspirated grain fractions ...... 240 Lingonberry ...... 3.5 Atemoya ...... 0 .30 Longan ...... 3 .0 Artichoke, globe ...... 2.5 Lychee ...... 3 .0 Avocado ...... 1 .0 Mango ...... 1.0 Banana ...... 0.50 Milk ...... 0.1 Barley, grain ...... 0 .05 Millet, pearl, forage ...... 2 .0 Barley, hay ...... 0 .5 Millet, pearl, grain ...... 0 .05 Barley, straw ...... 0 .5 Millet, pearl, hay ...... 6.0 Beet, sugar, roots ...... 0 .05 Millet, pearl, straw ...... 3.0 Beet, sugar, tops ...... 0.5 Millet, proso, forage ...... 2 .0 Beet, sugar, molasses ...... 0 .3 Millet, proso, grain ...... 0 .05 Biriba ...... 0 .30 Millet, proso, hay ...... 6 .0 Blueberry ...... 3 .5 Millet, proso, straw ...... 3 .0 Borage, seed ...... 0 .05 Mustard, black, seed ...... 0 .05 Caneberry, subgroup 13-A ...... 2 .5 Mustard, field, seed ...... 0 .05 Canistel ...... 1 .0 Mustard, Indian, seed ...... 0 .05 Canola, seed ...... 0 .05 Mustard, rapeseed, seed ...... 0 .05 Cattle, fat ...... 0.3 Mustard, seed ...... 0 .05 Cattle, meat byproducts ...... 0.3 Nut, tree, group 14 ...... 0 .05 Cattle, meat ...... 0 .3 Oats, forage ...... 2 .0 Cherimoya ...... 0 .3 Citrus, dried pulp ...... 5 .0 Oats, grain ...... 0 .05 Coffee, green bean ...... 0 .80 Oats, hay ...... 6.0 Corn, field, forage ...... 0 .10 Oats, straw ...... 3.0 Corn, field, grain ...... 0 .05 Okra ...... 1.0 Corn, field, stover ...... 0 .20 Passionfruit ...... 1 .0 Corn, pop, grain ...... 0.05 Papaya ...... 1 .0 Corn, pop, stover ...... 0.20 Peanut ...... 0 .45 Corn, sweet, forage ...... 0 .10 Peanut, hay ...... 35 Corn, sweet, kernel plus cob with husks re- Peanut, meal ...... 0 .75 moved ...... 0 .05 Pecan ...... 0 .05 Corn, sweet, stover ...... 0 .20 Persimmon ...... 3 .0 Cotton, gin byproducts ...... 4 .0 Pistachio ...... 0.05 Cotton, undelinted seed ...... 6 .0 Pomegranate ...... 0 .90 Cotton, meal ...... 8 .0 Potato, chip ...... 0 .4 Crambe, seed ...... 0.05 Potato, waste ...... 0 .9 Cranberry ...... 0 .05 Poultry, fat ...... 0.05 Currant ...... 3 .5 Poultry, meat byproducts ...... 0.05 Custard apple ...... 0 .30 Poultry, meat ...... 0 .05 Egg ...... 0 .02 Pulasan ...... 3 .0 Elderberry ...... 3 .5 Rambutan ...... 3 .0 Feijoa ...... 1 .0 Rapeseed, seed ...... 0 .05 Flax, seed ...... 0 .05 Raspberry, wild ...... 2.5 Fruit, citrus, group 10 ...... 0 .7 Rye, forage ...... 2 .0 Fruit, pome, group 11 ...... 0.6 Rye, grain ...... 0.05 Fruit, stone, group 12 ...... 3 .0 Rye, hay ...... 6 .0 Goat, fat ...... 0 .3 Rye, straw ...... 3 .0 Goat, meat byproducts ...... 0 .3 Safflower, seed ...... 0 .05 Goat, meat ...... 0.3 Salal ...... 3 .5 Gooseberry ...... 3 .5 Sapodilla ...... 1 .0 Grape, juice ...... 1 .5 Sapote, black ...... 1 .0 Grape, pomace (wet or dried) ...... 5.0 Sapote, mamey ...... 1 .0 Grape, raisin ...... 1 .5 Sheep, fat ...... 0 .3

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Parts Per Parts Per Commodity Million Commodity Million

Sheep, meat byproducts ...... 0 .3 Vegetable, legume, crop group 6 ...... 0 .3 Sheep, meat ...... 0.3 Sorghum, forage ...... 0 .10 Sorghum, grain ...... 0 .05 [71 FR 46116, Aug. 11, 2006, as amended at 72 Sorgum, stover ...... 0.10 FR 33912, June 20, 2007] Soursop ...... 0 .30 Soybean, forage ...... 8 .0 § 180.473 Glufosinate ammonium; tol- Soybean, hay ...... 35 Soybean, meal ...... 4.0 erances for residues. Soybean, seed ...... 3 .5 (a) General. (1) Tolerances are estab- Spanish lime ...... 3 .0 Star apple ...... 1 .0 lished for residues of the herbicide Starfruit ...... 1 .0 glufosinate ammonium (butanoic acid, Strawberry ...... 0 .50 2-amino-4-(hydroxymethylphosphinyl)-, Sugar apple ...... 0 .30 monoammonium salt) and its metabo- Sunflower, seed ...... 0.05 Tomato, paste ...... 6 .0 lites, 2-acetamido-4- Tomato, pomace (wet or dried) ...... 4 .O methylphosphinico-butanoic acid and Tomato, puree ...... 3 .0 3-methylphosphinico-propionic acid, Vegetable, brassica leafy, group 5 ...... 3 .5 Vegetable, cucurbit, group 9 ...... 0.5 expressed as 2-amino-4- Vegetable, fruiting, group 8 ...... 1.0 (hydroxymethylphosphinyl)butanoic Vegetable, leaves of root and tuber, group 2 ..... 4 .0 acid equivalents, in or on the following Vegetable, legume, except soybean, group 6 .... 4 .0 Vegetable, root and tuber, group 1, except food commodities: sugar beet ...... 0 .40 Watercress ...... 3 .5 Parts per Commodity million Watercress, upland ...... 3 .5 Wax jambu ...... 1 .0 Almond, hulls ...... 0 .50 Wheat, forage ...... 7 .0 Apple ...... 0.05 Wheat, grain ...... 0 .05 Banana ...... 0.30 Wheat, hay ...... 0 .5 Banana, pulp ...... 0 .20 Wheat, straw ...... 0 .5 Bushberry subgroup 13B ...... 0 .15 Cattle, fat ...... 0.40 (b) Section 18 emergency exemptions. Cattle, meat ...... 0 .15 [Reserved] Cattle, meat byproducts ...... 6.0 Cotton, gin byproducts ...... 15 (c) Tolerances with regional registra- Cotton, undelinted seed ...... 4 .0 tions. [Reserved] Egg ...... 0 .15 (d) Indirect or inadvertent residues. Goat, fat ...... 0 .40 Goat, meat ...... 0.15 Tolerances are established for indirect Goat, meat byproducts ...... 6 .0 or inadvertent combined residues of Grape ...... 0 .05 the insecticide imidacloprid (1-[(6- Hog, fat ...... 0 .40 Hog, meat ...... 0 .15 chloro-3-pyridinyl)methyl]-N-nitro-2- Hog, meat byproducts ...... 6 .0 imidazolidinimine) and its metabolites Horse, fat ...... 0 .40 containing the 6-chloropyridinyl moi- Horse, meat ...... 0 .15 ety, all expressed as 1-[(6-chloro-3- Horse, meat byproducts ...... 6 .0 Juneberry ...... 0 .10 pyridinyl)methyl]-N-nitro-2- Lingonberry ...... 0.10 imidazolidinimine, when present there- Milk ...... 0.15 in as a result of the application of the Nut, tree, group 14 ...... 0 .10 Potato ...... 0 .80 pesticide to growing crops listed in this Potato, chips ...... 1 .60 section and other non-food crops as fol- Potato granules and flakes ...... 2.00 lows: Poultry, fat ...... 0.15 Poultry, meat ...... 0 .15 Parts Per Poultry, meat byproducts ...... 0.60 Commodity Million Salal ...... 0 .10 Sheep, fat ...... 0 .40 Corn, sweet, kernel plus cob with husks re- Sheep, meat ...... 0.15 moved ...... 0 .05 Sheep, meat byproducts ...... 6 .0 Forage, fodder, and straw of Grain, cereal crop group (forage) ...... 2 .0 (2) Tolerances are established for res- Forage, fodder, and straw of Grain, cereal crop idues of the herbicide glufosinate am- group (hay) ...... 6.0 Forage, fodder, and straw of Grain, cereal crop monium (butanoic acid, 2-amino-4- group (stover) ...... 0 .3 (hydroxymethylphosphinyl)-, Forage, fodder, and straw of Grain, cereal crop monoammonium salt) and its metabo- group (straw) ...... 3.0 Grain, cereal, group 15 ...... 0.05 lites, 2-acetamido-4- Vegetable, foliage of legume, group 7 ...... 2 .5 methylphosphinico-butanoic acid and

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3-methylphosphinico-propionic acid, § 180.474 Tebuconazole; tolerances for expressed as 2-amino-4- residues. (hydroxymethylphosphinyl)butanoic (a) General. (1) Tolerances are estab- acid equivalents, in or on the following lished for residues of the fungicide food commodities derived from tebuconazole (alpha-[2-(4- transgenic canola, transgenic cotton, chlorophenyl)-ethyl]-alpha-(1,1- transgenic field corn, transgenic rice, dimethylethyl)-1H-1,2,4-triazole-1-eth- transgenic soybean and transgenic anol) in or on the following raw agri- sugar beet that are tolerant to cultural commodities: glufosinate ammonium: Commodity Parts per Parts per million Commodity million Banana ...... 0.05 Aspirated grain fractions ...... 25 .0 Barley, grain ...... 0 .05 Beet, sugar, molasses ...... 5 .0 Barley, hay ...... 0 .10 Beet, sugar, roots ...... 0 .9 Barley, straw ...... 0 .10 Beet, sugar, tops (leaves) ...... 1 .5 Cherry ...... 4.0 Canola, meal ...... 1 .1 Grape ...... 5 .0 Canola, seed ...... 0 .4 Grass, forage ...... 8 .0 Corn, field, forage ...... 4 .0 Grass, hay ...... 25 .0 Corn, field, grain ...... 0 .2 Grass, seed screenings ...... 55.0 Corn, field, stover ...... 6 .0 Grass, straw ...... 30 .0 Cotton, gin byproducts ...... 15 Oat, forage ...... 0 .10 Cotton, undelinted seed ...... 4 .0 Oat, grain ...... 0 .05 Rice, grain ...... 1 .0 Oat, hay ...... 0.10 Rice, hull ...... 2 .0 Oat, straw ...... 0.10 Rice, straw ...... 2 .0 Peach (includes nectarine) ...... 1 .0 Soybean ...... 2.0 Peanut ...... 0 .1 Soybean, hulls ...... 5 .0 Wheat, forage ...... 0 .10 Wheat, grain ...... 0 .05 Wheat, hay ...... 0 .10 (b) Section 18 emergency exemptions. Wheat, straw ...... 0 .10 [Reserved] (c) Tolerances with regional restric- (2) Tolerances are established for the tions. [Reserved] combined residues of the fungicide, (d) Indirect or inadvertent residues. tebuconazole and its 1-(4- Tolerances are established for indirect chlorophenyl)-4,4-dimethyl-3-(1H-1,2,4- or inadvertent residues of the herbicide triazole-1-yl-methyl)-pentane-3,5-diol glufosinate ammonium, butanoic acid, metabolite. 2-amino-4-(hydroxymethylphosphinyl)-, monoammonium salt and its metabo- Parts per Commodity million lite, 3-methylphosphinicopropionic acid in or on the following raw agricul- Cattle, meat byproducts ...... 0.2 Goat, meat byproducts ...... 0 .2 tural commodities when present there- Horse, meat byproducts ...... 0 .2 in as a result of the application of Milk ...... 0.1 glufosinate ammonium to crops listed Sheep, meat byproducts ...... 0 .2 in paragraph (a) of this section: (b) Section 18 emergency exemptions. (1) Commodity Parts per Time-limited tolerances are estab- million lished for residues of the fungicide Barley, hay ...... 0 .40 tebuconazole (alpha-[2-(4- Barley, straw ...... 0 .40 chlorophenyl)-ethyl]-alpha-(1,1- Buckwheat, fodder ...... 0 .40 Buckwheat, forage ...... 0 .40 dimethylethyl)-1H-1,2,4-triazole-1-eth- Oat, forage ...... 0 .40 anol) in connection with use of the pes- Oat, hay ...... 0.40 ticide under section 18 emergency ex- Oat, straw ...... 0.40 Rye, forage ...... 0 .40 emptions granted by EPA. The toler- Rye, straw ...... 0 .40 ances will expire and are revoked on Teosinte ...... 0 .40 the dates specified in the following Triticale ...... 0.40 table. Wheat, forage ...... 0 .40 Wheat, hay ...... 0 .40 Expiration/ Wheat, straw ...... 0 .40 Commodity Parts per revocation million date

[68 FR 55849, Sept. 29, 2003, as amended at 71 Barley, grain ...... 2.0 6/30/08 FR 25945, May 3, 2006] Barley, hay ...... 20.0 6/30/08

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Expiration/ Parts per Commodity Parts per revocation Commodity million million date Cattle, fat ...... 0.05 Barley, straw ...... 20.0 6/30/08 Cattle, meat ...... 0 .05 Garlic ...... 0.1 12/31/07 Cattle, meat byproducts ...... 0.05 Soybean ...... 0.1 12/31/09 Corn, sweet, forage ...... 0 .01 Sunflower, refined oil ...... 0.4 12/31/07 Corn, sweet, kernel plus cob with husks re- Sunflower, seed ...... 0.2 12/31/07 moved ...... 0 .01 Wheat, hay ...... 15.0 6/30/08 Corn, sweet, stover ...... 0 .01 Wheat, straw ...... 2.0 6/30/08 Cotton, gin byproducts ...... 0 .05 Cotton, undelinted seed ...... 0 .05 (2) Time-limited tolerances are estab- Egg ...... 0 .05 lished for the combined residues of the Fruit, pome, group 113 ...... 0 .10 Goat, fat ...... 0 .05 fungicide tebuconazole (alpha-[2-(4- Goat, meat ...... 0.05 chlorophenyl)-ethyl)-ethyl]-alpha-(1,1- Goat, meat byproducts ...... 0 .05 dimethylethyl)-1H-1,2,4-triazole-1-eth- Grape3 ...... 0 .10 Hog, fat ...... 0 .05 anol) and its 1-(4-chlorophenyl)-4,4-di- Hog, meat ...... 0 .05 methyl-3-(1H-1,2,4-triazole-1-yl-meth- Hog, meat byproducts ...... 0 .05 yl)-pentane-3,5-diol metabolite in con- Horse, fat ...... 0 .05 Horse, meat ...... 0 .05 nection with use of the pesticide under Horse, meat byproducts ...... 0 .05 section 18 emergency exemptions Milk ...... 0.01 granted by EPA. The tolerances will Poultry, fat ...... 0.05 expire and are revoked on the dates Poultry, meat ...... 0 .05 Poultry, meat byproducts ...... 0.05 specified in the following table. Rye, grain1 ...... 0 .1 Sheep, fat ...... 0 .05 Parts per Expiration/ Sheep, meat ...... 0.05 Commodity million revocation Sheep, meat byproducts ...... 0 .05 date Wheat, forage ...... 0 .1 Wheat, grain ...... 0 .1 Egg ...... 0.1 12/31/09 Poultry, fat ...... 0.1 12/31/09 Wheat, straw ...... 0 .1 Poultry, meat ...... 0.1 12/31/09 1There are no U.S. registrations on Barley, grain and Rye, Poultry, meat byproducts ...... 0.1 12/31/09 grain as of April 12, 1995. Hog, fat ...... 0.1 12/31/09 2There are no U.S. registrations on Banana as of June 2, Hog, meat ...... 0.1 12/31/09 1999. Hog, meat byproducts ...... 0.1 12/31/09 3There are no U.S. Registrations on fruit, pome, group 11 or on grapes, as of September 13, 2006. (c) Tolerances with regional registra- (b) Section 18 emergency exemptions. tions. [Reserved] [Reserved] (d) Indirect or inadvertent residues. (c) Tolerances with regional registra- [Reserved] tions. [Reserved] [59 FR 39464, Aug. 3, 1994] (d) Indirect or inadvertent residues. [Reserved] EDITORIAL NOTE: For FEDERAL REGISTER ci- tations affecting § 180.474, see the List of CFR [64 FR 36254, July 6, 1999, as amended at 64 Sections Affected, which appears in the FR 47687, Sept. 1, 1999; 65 FR 55921, Sept. 15, Finding Aids section of the printed volume 2000; 65 FR 82940, Dec. 29, 2000; 66 FR 64774, and on GPO Access. Dec. 14, 2001; 68 FR 37765, June 25, 2003; 70 FR 75739, Dec. 21, 2005; 71 FR 53984, Sept. 13, 2006] § 180.475 Difenoconazole; tolerances for residues. § 180.476 Triflumizole; tolerances for (a) General. Tolerances are estab- residues. lished for residues of the fungicide (a) General. (1) Tolerances are estab- difenoconazole (1-[2-[2-chloro-4-(4- lished for the combined residues of the chlorophenoxy)phenyl]-4-methyl-1,3- fungicide triflumizole, 1-(1-((4-chloro-2- dioxolan-2-ylmethyl]-1H-1,2,4-triazole) (trifluoromethyl)phenyl)imino)-2- in or on the following raw agricultural propoxyethyl)-1H-imidazole, and its commodities. metabolites containing the 4-chloro-2- trifluoromethylaniline moiety, cal- Parts per Commodity million culated as the parent compound, in or on the following food commodities: Banana2 ...... 0 .2 Barley, grain1 ...... 0 .1 Parts per Barley, hay ...... 0 .05 Commodity million Barley, straw ...... 0 .05 Canola, seed ...... 0 .01 Apple, pomace ...... 2.0

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Parts per Expiration/ Commodity million Commodity Parts per revocation million date Apple ...... 0.5 Cherry, sweet ...... 1 .5 Broccoli ...... 1.0 12/31/09 Cherry, tart ...... 1 .5 Cabbage, chinese, napa ...... 20 12/31/09 Collards ...... 20 12/31/09 Filbert ...... 0 .05 Coriander, leaves ...... 20 12/31/09 Grape ...... 2 .5 Dandelion, leaves ...... 7.0 12/31/09 Grape pomace ...... 15.0 Kale ...... 20 12/31/09 Grape, raisin, waste ...... 10 .0 Kohlrabi ...... 20 12/31/09 Pear ...... 0 .5 Mustard, greens ...... 20 12/31/09 Strawberry ...... 2 .0 Parsley, leaves ...... 20 12/31/09 Vegetable, cucurbit, Group 9 ...... 0 .5 Swiss chard ...... 7.0 12/31/09 Turnip, greens ...... 20 12/31/09 (2) Tolerances are established for the (c) Tolerances with regional registra- combined residues of the fungicide tions. [Reserved] triflumizole, 1-(1-((4-chloro-2- (d) Indirect or inadvertent residues. (trifluoromethyl)phenyl)imino)-2- [Reserved] propoxyethyl)-1H-imidazole, the me- tabolite 4-chloro-2-hydroxy-6- [65 FR 33702, May 24, 2000, as amended at 67 trifluoromethylaniline sulfate, and FR 40228, June 12, 2002; 67 FR 54587, Aug. 23, other metabolites containing the 4- 2002; 70 FR 7047, Feb. 10, 2005; 70 FR 17915, chloro-2-trifluoromethylaniline moi- Apr. 8, 2005; 71 FR 13279, Mar. 15, 2006; 71 FR 49358, Aug. 23, 2006] ety, calculated as the parent com- pound, in or on the following food com- § 180.477 Flumiclorac pentyl; toler- modities of animal origin: ances for residues.

Parts per (a) General. Tolerances are estab- Commodity million lished for residues of the herbicide flumiclorac pentyl, [2-chloro-4-fluoro-5- Cattle, fat ...... 0.5 Cattle, meat ...... 0 .05 (1,3,4,5,6,7-hexahydro-1,3-dioxo-2H- Cattle, meat byproducts ...... 0.5 isoindol-2-yl)phenoxy]-acetate, in or on Egg ...... 0 .05 the raw agricultural commodities list- Goat, fat ...... 0 .5 ed below. Goat, meat ...... 0.05 Goat, meat byproducts ...... 0 .5 Commodity Parts per Hog, fat ...... 0 .5 million Hog, meat ...... 0 .05 Corn, field, forage ...... 0 .01 Hog, meat byproducts ...... 0 .5 Corn, field, grain ...... 0 .01 Horse, fat ...... 0 .5 Corn, field, stover ...... 0 .01 Horse, meat ...... 0 .05 Cotton gin by products ...... 3 .0 Horse, meat byproducts ...... 0 .5 Cotton, undelinted seed ...... 0 .2 Milk ...... 0.05 Soybean, hulls ...... 0 .02 Poultry, fat ...... 0.05 Soybean, seed ...... 0 .01 Poultry, meat ...... 0 .05 Poultry, meat byproducts ...... 0.1 (b) Section 18 emergency exemptions. Sheep, fat ...... 0 .5 [Reserved] Sheep, meat ...... 0.05 (c) Tolerances with regional registra- Sheep, meat byproducts ...... 0 .5 tions. [Reserved] (b) Section 18 emergency exemptions. (d) Indirect or inadvertent residues. Time limited tolerances are estab- [Reserved] lished for the residues triflumizole (1- [65 FR 33702, May 24, 2000, as amended at 71 (1-((4-chloro-2- FR 11533, Mar. 8, 2006] (trifluoromethyl)phenyl)imino)-2- propoxyethyl)-1H-imidazole) and its § 180.478 Rimsulfuron; tolerances for metabolites containing the 4-chloro-2- residues trifluoromethylaniline moiety, cal- (a) General. Tolerances are estab- culated as the parent in connection lished for residues of the herbicide with use of the pesticide under section rimsulfuron (N-((4,6- 18 emergency exemptions granted by dimethoxypyrimidin-2- EPA. The tolerances are specified in yl)aminocarbonyl)-3-(ethylsulfonyl)-2- the following table, and will expire and pyridinesulfonamide in or on the fol- are revoked on the dates specified. lowing raw agricultural commodities:

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Parts per Parts per Commodity million Commodity million

Corn, field, forage ...... 0 .1 Corn, sweet, kernel plus cob with husks re- Corn, field, grain ...... 0 .1 moved ...... 0 .05 Corn, field, stover ...... 0 .1 Cotton, gin byproducts ...... 0 .05 Potato ...... 0 .1 Cotton, undelinted seed ...... 0 .05 Tomato ...... 0.05 Melon subgroup 9A ...... 0 .1 Nut, tree, group 14 ...... 0 .05 (b) Section 18 emergency exemptions. Pistachio ...... 0.05 Rice, grain ...... 0 .05 [Reserved] Rice, straw ...... 0 .2 (c) Tolerances with regional registra- Sorghum, grain, fodder/stover ...... 0 .1 tions. [Reserved] Sorghum, grain, forage ...... 0.05 (d) Indirect or inadvertent residues. Sorghum, grain, grain ...... 0 .05 Squash/Cucumber subgroup 9B ...... 0 .5 [Reserved] Sugarcane, cane ...... 0.05 [63 FR 16696, Apr. 6, 1998] Vegetable, fruiting, group 8 ...... 0.05

§ 180.479 Halosulfuron-methyl; toler- (b) Section 18 emergency exemptions. ances for residues. Time-limited tolerances are estab- lished for residues of halosulfuron (a) General. (1) Tolerances are estab- lished for residues of the herbicide methyl, methyl 5-[(4,6-dimethoxy-2- halosulfuron-methyl, methyl 5-[(4,6- pyrimidinyl)amino] dimethoxy-2-pyrimidiny)amino] carbonylaminosulfonyl-3-chloro-1- carbonylaminosulfonyl-3-chloro-1- methyl-1H-pyrazole-4-carboxylate, in connection with use of the pesticide methyl-1H-pyrazole-4-caboxylate, and its metabolites determined as 3-chloro- under FIFRA section 18 emergency ex- 1-methyl-5-sulfamoylpyrazole-4-car- emptions granted by EPA in or on the boxylic acid, expressed as halosulfuron- following commodity: methyl equivalent in or on the raw ag- Parts per Expiration/ ricultural commodities listed in the Commodity million revocation table in this unit. date Sweet potato ...... 1.0 12/31/08 Parts per Commodity million (c) Tolerances with regional registra- Cattle, meat byproducts ...... 0.1 tions. [Reserved] Goat, meat byproducts ...... 0 .1 Hog, meat byproducts ...... 0 .1 (d) Indirect or inadvertent residues. Horse, meat byproducts ...... 0 .1 [Reserved] Sheep, meat byproducts ...... 0 .1 [64 FR 25448, May 12, 1999, as amended at 65 (2) Tolerances are established for res- FR 58433, Sept. 29, 2000; 66 FR 66340, Dec. 26, 2001; 66 FR 66786, Dec. 27, 2001; 67 FR 45649, idues of the herbicide halosulfuron- July 10, 2002; 67 FR 59192, Sept. 20, 2002; 70 FR methyl, methyl 5-[(4,6-dimethoxy-2- 51622, Aug. 31, 2005; 72 FR 8927, Feb. 28, 2007] pyrimidinyl) amino]carbonylaminosulfonyl-3-chloro- § 180.480 Fenbuconazole; tolerances 1-methyl-1H-pyrazole- 4-carboxylate, in for residues. or on the raw agricultural commodities (a) General. (1) Time-limited toler- listed below. ances, to expire on December 31, 2001, are reestablished for combined residues Parts per Commodity million of the fungicide fenbuconazole [alpha- [2-(4-chlorophenyl)-ethyl]-alpha- Alfalfa, forage ...... 1.0 Alfalfa, hay ...... 2.0 phenyl-3-(1H-1,2,4-triazole)-1- Almond, hulls ...... 0 .2 propanenitrile] and its metabolites, cis- Asparagus ...... 0.8 5-(4-chlorophenyl)-dihydro-3-phenyl-3- Bean, dry, seed ...... 0 .05 (1H-1,2,4-triazole-1-ylmethyl)-2-3H- Bean, snap, succulent ...... 0 .05 Corn, field, forage ...... 0 .2 furanone and trans-5-(4- Corn, field, grain ...... 0 .05 chlorophenyl)dihydro-3-phenyl-3-(1H- Corn, field, stover ...... 0 .8 1,2,4-triazole-1-ylmethyl-2-3H-furanone, Corn, pop, grain ...... 0.05 expressed as fenbuconazole, in or on Corn, pop, stover ...... 0.8 Corn, sweet, fodder/stover ...... 0.8 the following raw agricultural com- Corn, sweet, forage ...... 0 .2 modities:

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Parts per Expiration/ Commodity million Commodity Parts per revocation million date Almond ...... 0.05 Almond, hulls ...... 1 .0 Hog, fat ...... 0.01 12/31/08 Apple ...... 0.4 Hog, meat byproducts ...... 0.01 12/31/08 Apple, wet pomace ...... 1 .0 Hog, meat ...... 0.01 12/31/08 Banana ...... 0.3 Horse, fat ...... 0.01 12/31/08 Beet, sugar, dried pulp ...... 1 .0 Horse, meat ...... 0.01 12/31/08 Beet, sugar, molasses ...... 0 .4 Sheep, fat ...... 0.01 12/31/08 Beet, sugar, roots ...... 0 .3 Sheep, meat ...... 0.01 12/31/08 Beet, sugar, tops ...... 9.0 Bushberry subgroup 13B ...... 0 .3 (c) Tolerances with regional registra- Cattle, meat byproducts ...... 0.05 Citrus, dried pulp ...... 5 .0 tions. [Reserved] Citrus, oil ...... 40.0 (d) Indirect or inadvertent residues. Cranberry ...... 0 .5 [Reserved] Fruit, citrus, group 10 ...... 1 .0 Fruit, stone, group 12 ...... 1 .0 [60 FR 11032, Mar. 1, 1995, as amended at 60 Goat, meat byproducts ...... 0 .05 FR 27421, May 24, 1995; 63 FR 31640, June 10, Grain, aspirated fractions ...... 6 .0 1998; 64 FR 4583, Jan. 29, 1999; 64 FR 7801, Feb. Grape1 ...... 1 .0 Horse, meat byproducts ...... 0 .05 17, 1999; 64 FR 15306, Mar. 31, 1999; 65 FR 45922, Peanut ...... 0 .1 July 26, 2000; 65 FR 82940, Dec. 29, 2000; 66 FR Pecan ...... 0 .05 37598, July 19, 2001; 66 FR 64774, Dec. 14, 2001; Sheep, meat byproducts ...... 0 .05 67 FR 1888, Jan. 15, 2002; 67 FR 46884, July 17, Wheat, forage ...... 4 .0 2002; 68 FR 37765, June 25, 2003; 69 FR 29459, Wheat, grain ...... 0 .1 May 24, 2004; 70 FR 11583, Mar. 9, 2005; 70 FR Wheat, hay ...... 8 .0 75739, Dec. 21, 2005; 71 FR 55299, Sept. 22, 2006] Wheat, straw ...... 8 .0 1There are no United States registrations for grape as of § 180.481 Prosulfuron; tolerances for August 2006. residues. (2) Residues in these commodities not Tolerances that expire as indicated in excess of the established tolerance in the table below are established for resulting from the uses described in residues of the herbicide prosulfuron 1- paragraph (a)(1) of this section remain- (4-methoxy-6-methyl-triazin-2-yl)-3-[2- ing after expiration of the time-limited (3,3,3-trifluoropropyl)-phenylsulfonyl]- tolerance will not be considered to be urea in or on the following raw agricul- actionable if the fungicide is applied tural commodities: during the term of and in accordance with the provisions of the above regu- Commodity Parts per Expiration lation. million date (b) Section 18 emergency exemptions. A Cattle, fat ...... 0.05 12/31/99 time-limited tolerance is established Cattle, kidney ...... 0.05 Do. Cattle, liver ...... 0.05 Do. for fenbuconazole (alpha-[2-4- Cattle, meat ...... 0.05 Do. chlorophenyl)-ethyl]alpha-phenyl-3- Cattle, meat byproducts ...... 0.05 Do. (1H-1,2,4-triazole)-1-propanenitrile] and Corn, forage ...... 0.01 Do. its metabolites, cis-5-(4-chlorophenyl)- Corn, grain and fresh (including sweet kernels plus cobs with dihydro-3-phenyl-3-(1H-1,2,4-triazole-1- husks removed) ...... 0.01 Do. ylmethyl)-2-3H-furanone and trans-5-(4- Corn, stover ...... 0.01 Do. chlorophenyl)dihydro-3-phenyl-3-(1H Goat, fat ...... 0.05 Do. Goat, kidney ...... 0.05 Do. 1,2,4-triazole-1-ylmethyl-2-3H-furanone, Goat, liver ...... 0.05 Do. expressed as fenbuconazole in or on Goat, meat ...... 0.05 Do. Blueberry in connection with use of the Goat, meat byproducts ...... 0.05 Do. pesticide under a section 18 exemption Grain, cereal group (except rice and wild rice), fodder ...... 0.01 Do. granted by EPA. The time-limited tol- Grain, cereal group (except rice and erance will expire on the date specified wild rice), forage ...... 0.10 Do. in the following table. Grain, cereal group (except rice and wild rice), grain ...... 0.01 Do. Expiration/ Grain, cereal group (except rice and Commodity Parts per revocation wild rice), hay ...... 0.20 Do. million date Grain, cereal group (except rice and wild rice), straw ...... 0.02 Do. Blueberry ...... 1.0 12/31/07 Hog, fat ...... 0.05 Do. Cattle, fat ...... 0.01 12/31/08 Hog, kidney ...... 0.05 Do. Cattle, meat ...... 0.01 12/31/08 Hog, liver ...... 0.05 Do. Goat, fat ...... 0.01 12/31/08 Hog, meat ...... 0.05 Do. Goat, meat ...... 0.01 12/31/08 Hog, meat byproducts ...... 0.05 Do.

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hydroxymethyl,5-methyl-1-(1,1- Commodity Parts per Expiration million date dimethylethyl)-2-(4- Horse, fat ...... 0.05 Do. ethylbenzoyl)hydrazide and benzoic Horse, kidney ...... 0.05 Do. acid, 3-hydroxymethyl-5-methyl-1-(1,1- Horse, liver ...... 0.05 Do. dimethylethyl)-2-(4-(1-hydroxy- Horse, meat ...... 0.05 Do. Horse, meat byproducts ...... 0.05 Do. ethyl)benzoyl)hydrazide. Milk ...... 0.01 Do. Sheep, fat ...... 0.05 Do. Commodity Parts per Sheep, kidney ...... 0.05 Do. million Sheep, liver ...... 0.05 Do. Fat of cattle, goat, hog, horse, and sheep ...... 0 .1 Sheep, meat ...... 0.05 Do. Meat of cattle, goat, hog, horse and sheep ...... 0 .08 Sheep, meat byproducts ...... 0.05 Do. Meat byproducts of cattle, goat, hog, horse and sheep ...... 0 .08 [61 FR 26842, May 29, 1996, as amended at 61 Milk ...... 0.04 FR 26844, May 29, 1996] (b) Section 18 emergency exemptions. § 180.482 Tebufenozide; tolerances for Time-limited tolerances are estab- residues. lished for residues of the insecticide (a) General. (1) Tolerances are estab- benzoic acid in connection with use of lished for residues of the insecticide the pesticide under section 18 emer- tebufenozide, benzoic acid, 3,5-di- gency exemptions granted by EPA. The methyl-1-(1,1-dimethylethyl)-2-(4- tolerances will expire and are revoked ethylbenzoyl)hydrazide, in or on the on the dates specified in the following following raw agricultural commod- table. ities: Expiration/ Commodity Parts per revocation Parts per million date Commodity million Beet, garden, roots ...... 0.3 12/31/05 Almond, hulls ...... 25 Beet, garden, tops ...... 9.0 12/31/05 Apple, pomace ...... 3.0 Grape ...... 3.0 12/31/05 Apple ...... 1.0 Sweet potato, roots ...... 0.25 12/31/05 Berry group 13 ...... 3.0 Brassica, head and stem, subgroup 5A ...... 5.0 (c) Tolerances with regional registra- Brassica, leafy greens, subgroup 5B ...... 10.0 Canola, refined oil ...... 4.0 tions. [Reserved] Canola, seed ...... 2.0 (d) Indirect or inadvertent residues. Citrus, oil ...... 15.0 Tolerances are established for the indi- Cotton ...... 1.5 Cotton, gin byproducts ...... 30 rect or inadvertent combined residues Cranberry ...... 1.0 of tebufenozide, benzoic acid, 3,5-di- Fruit, citrus, group 10 ...... 0.80 methyl-1-(1,1-dimethylethyl)-2-(4- Fruit, pome ...... 1.5 Grape ...... 3.0 ethylbenzoyl)hydrazide and its metabo- Kiwifruit1 ...... 0.5 lite benzoic acid, 3,5-dimethyl-1- Leaf petioles subgroup 4B ...... 2.0 (1,1dimethylethyl)-2-[4-(1-hydroxy- Leafy greens subgroup 4A ...... 10.0 ethyl)benzoyl]hydrazide in or on the Peppermint, tops ...... 10.0 Spearmint, tops ...... 10.0 raw agricultural commodities when Tree nut crop group including pistachio ...... 0.1 present therein as a result of the appli- Turnip, greens ...... 9.0 cation of tebufenozide to growing crops Turnip, roots ...... 0.3 Vegetable, fruiting (Except cucurbits) ...... 1.0 listed in paragraph (a) of this section Vegetable, tuberous and corm (except potato), to read as follows: subgroup 1D ...... 0.015 Walnut ...... 0.1 Parts per Commodity million 1There are no U.S. registrations on kiwifruit as of June 15, 1999. Forage, fodder, hay and straw of grain, cereal, (2) Tolerances are established for the group 16 ...... 1.0 Forage, fodder, straw and hay of non-grass ani- combined residues of tebufenozide and mal feed, group 18 ...... 1.0 its metabolites benzoic acid, 3,5-di- Grass, forage, fodder and hay, group 17 ...... 1 .0 methyl-1-(1,1-dimethylethyl)-2-((4- Vegetable, foliage of legume, group 7 ...... 0 .20 carboxymethyl)benzoyl)hydrazide), benzoic acid, 3-hydroxymethyl,5-meth- [60 FR 29347, May 31, 1995] yl-1-(1,1-dimethylethyl)-2-(4- EDITORIAL NOTE: For FEDERAL REGISTER ci- ethylbenzoyl)hydrazide, the stearic tations affecting § 180.482, see the List of CFR acid conjugate of benzoic acid, 3- Sections Affected, which appears in the

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Finding Aids section of the printed volume Parts per and on GPO Access. Commodity million

Poultry (including turkeys), fat ...... 0 .05 § 180.483 O-[2-(1,1-Dimethylethyl)-5- Poultry (including turkeys), meat byproducts ...... 0 .05 pyrimidinyl] O-ethyl-O-(1-methyl- Poultry (including turkeys), meat ...... 0 .05 ethyl) phosphorothioate; tolerances Rice, bran ...... 10.0 for residues. Rice, grain ...... 7 .0 Rice, hulls ...... 25 .0 Time-limited tolerances are estab- Rice, straw ...... 10 .0 lished for residues of the insecticide O- Sheep, fat ...... 0 .10 [2-(1,1-dimethylethyl)-5-pyrimidinyl] O- Sheep, kidney ...... 1.00 Sheep, liver ...... 2.00 ethyl-O-(1-methylethyl) Sheep, meat ...... 0.05 phosphorothioate in or on the fol- Sheep, meat byproducts ...... 0 .05 lowing raw agricultural commodities: (2) Time-limited tolerances. Time-lim- Parts per Expiration ited tolerances are established for the Commodity million date residues of the fungicide flutolanil N- Corn, forage and fodder, field, pop, (3-(1-methylethoxy)phenyl)-2- and sweet ...... 0.01 7/6/99 (trifluoromethyl)benzamide and its me- Corn, grain, field and pop ...... 0.01 Do. Corn, sweet, kernel plus cob with tabolites converted to 2- husks removed ...... 0.01 Do. (trifluoromethyl) benzoic acid and cal- culated as flutolanil in or on the fol- [60 FR 34873, July 5, 1995] lowing agricultural commodities:

Expiration/ § 180.484 Flutolanil (N-(3-(1-methyl- Commodity Parts per Revocation ethoxy)phenyl)-2-(trifluorometh- million Date yl)benzamide); tolerances for resi- dues. Rice, grain ...... 2.0 12/31/00 Rice, straw ...... 8.0 12/31/00 (a) General—(1) Permanent tolerances. Rice, bran ...... 3.0 12/31/00 Tolerances are established for residues Rice, hulls ...... 7.0 12/31/00 of flutolanil, N-(3-(1- methylethoxy)phenyl)-2- (b) Section 18 emergency exemptions. (trifluoromethyl)benzamide, and its [Reserved] metabolites converted to 2- (c) Tolerances with regional registra- (trifluoromethyl) benzoic acid and cal- tions. [Reserved] (d) culated as flutolanil in or on the fol- Indirect or inadvertent residues. [Reserved] lowing raw agricultural commodities: [60 FR 42458, Aug. 16, 1995, as amended at 61 Parts per FR 33044, June 26, 1996; 63 FR 42256, 42257, Commodity million Aug. 7, 1998; 66 FR 10825, Feb. 20, 2001; 71 FR Cattle, fat ...... 0.10 74818, Dec. 13, 2006; 72 FR 35665, June 29, 2007] Cattle, kidney ...... 1 .00 Cattle, liver ...... 2 .00 § 180.485 Cyproconazole; tolerances for Cattle, meat byproducts ...... 0.05 residues. Cattle, meat ...... 0 .05 Egg ...... 0 .05 (a) General. A tolerance is established Goat, fat ...... 0 .10 for residues of the fungicide Goat, kidney ...... 1 .00 Goat, liver ...... 2.00 cyproconazole, (2RS,3RS)-2-(4- Goat, meat byproducts ...... 0 .05 chlorophenyl)-3-cyclopropyl-1-(1H-1,2,4- Goat, meat ...... 0.05 triazole-1-yl)butan-2-ol in or on the im- Hog, fat ...... 0 .10 Hog, kidney ...... 1.00 ported agricultural commodity coffee, Hog, liver ...... 2 .00 bean, green at 0.1 ppm. There are no Hog, meat byproducts ...... 0 .05 U.S. registrations as of October 7, 1998, Hog, meat ...... 0 .05 Horse, fat ...... 0 .10 for use on coffee bean. Horse, kidney ...... 1 .00 (b) Section 18 emergency exemptions. A Horse, liver ...... 2 .00 time-limited tolerance is established Horse, meat byproducts ...... 0 .05 for residues of the fungicide Horse, meat ...... 0 .05 Milk ...... 0.05 cyproconazole per se ((2RS,3RS)-2-(4- Peanut ...... 0 .5 chlorophenyl)-3-cyclopropyl-1-(1H Peanut, hay ...... 15.0 -1,2,4- triazole-1-yl)butan-2-ol) in or on Peanut meal ...... 1 .0 Potato ...... 0 .20 soybean seed in connection with the Potato, wet peel ...... 0 .30 use of the pesticide under section 18

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emergency exemptions granted by (d) Indirect or inadvertent residues. EPA. The tolerance will expire and be [Reserved] revoked on the date specified in the [62 FR 54783, Oct. 22, 1997, as amended at 64 following table. FR 56469, Oct. 20, 1999; 67 FR 72110, Dec. 4, 2002] Expiration/ Commodity Parts per Revocation million Date § 180.489 Sulfosate (Sulfonium, tri- methyl-salt with N-(phospho- Soybean, seed ...... 0.10 12/31/09 nomethyl)glycine (1:1)); tolerances for residues. (c) Tolerances with regional registra- (a) General. Tolerances are estab- tions. [Reserved] lished for residues of the herbicide (d) Indirect or inadvertent residues. sulfosate (sulfonium, trimethyl-salt [Reserved] with N-(phosphonomethyl)glycine (1:1)) [63 FR 53835, Oct. 7, 1998, as amended at 71 FR as the sum of the residues of the 71058, Dec. 8, 2006] trimethylsulfonium cation (TSM) and the N-(phosphonomethyl glycine anion § 180.486 Phosphorothioic acid, 0,0- measured separately in or on the fol- diethyl 0-(1,2,2,2-tetrachloroethyl) lowing raw and processed agricultural ester; tolerances for residues. commodities. Tolerances are established permit- Parts per ting the residue of the insecticide Commodity million phosphorothioic acid, 0,0-diethyl 0- Almond, hulls (of which no more than 0.30 ppm (1,2,2,2-tetrachloroethyl) ester in or on is trimethylsulfonium (TMS))...... 1 .00 the following raw agricultural com- Banana (imported only) 1 ...... 0 .05 modities: Cattle, fat ...... 0.5 Cattle, kidney ...... 6 .0 Parts per Cattle, meat byproducts, except kidney ...... 1.5 Commodity million Cattle, meat ...... 1 .0 Corn, field, forage ...... 0 .10 Corn, field, forage ...... 0 .01 Corn, field and pop, grain (of which no more than 0.10 ppm is TMS)...... 0 .20 Corn, field, grain ...... 0 .01 Corn, field and pop, stover (of which no more Corn, field, stover ...... 0 .01 than 0.20 ppm is TMS)...... 0 .30 Corn, pop, grain ...... 0.01 Corn, sweet, forage (of which no more than 5.0 Corn, pop, stover ...... 0.01 ppm is TMS) ...... 20 Corn, sweet, kernel plus cob with husks re- Corn, sweet, kernel plus cob with husks re- moved ...... 0 .01 moved (of which no more than 0.10 ppm is Corn, sweet, forage ...... 0 .01 TMS) ...... 0 .15 Corn, sweet, stover (fodder) ...... 0 .01 Corn, sweet, stover (of which no more than 65 ppm is TMS) ...... 170 Cotton, gin byproducts (of which no more than [60 FR 49792, Sept. 27, 1995] 35 ppm is TMS) ...... 120 Cotton, undelinted seed (of which no more than 10 ppm is TMS) ...... 40 § 180.487 Pyrithiobac sodium; toler- Crop group 2: Leaves of root and tuber vegeta- ances for residues. bles (human food or animal feed (except rad- (a) General. Tolerances are estab- ish) group (of which no more than 0.20 ppm is TSM) ...... 0 .30 lished for residues of the herbicide, Crop group 8: Vegetable, fruiting (except pyrithiobac sodium, (sodium 2-chloro- cucurbits) group ...... 0 .05 6-[(4,6-dimethoxypyrimidin-2- Crop subgroup 1–A: Root vegetables (except radish) subgroup (of which no more than 0.10 yl)thio]benzoate), resulting from the ppm is TSM) ...... 0.15 application of the pesticide chemical in Crop subgroup 1–C: Tuberous and corm vege- or on the following foods/feeds: tables subgroup (of which no more than 0.50 ppm is TSM) ...... 1 Parts per Crop subgroup 6–A: Edible-podded legume Commodity million vegetables subgroup (of which no more than 0.3 ppm is TSM) ...... 0 .5 Cotton, gin byproducts ...... 0 .15 Crop subgroup 6–B: Succulent shelled pea and Cotton, undelinted seed ...... 0 .02 bean subgroup (of which no more than 0.1 ppm is TSM) ...... 0 .20 Crop subgroup 6–C: Dried shelled pea and (b) Section 18 emergency exemptions. bean (except soybean and animal feed) sub- [Reserved] group (of which no more than 1.5 ppm is TSM) ...... 6 .0 (c) Tolerances with regional registra- Egg ...... 0 .05 tions. [Reserved] Fruit, citrus, group 10 ...... 0 .05

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(d) Indirect or inadvertent residues. Commodity Parts per million [Reserved] Fruit, pome, group 11 ...... 0.05 [64 FR 22805, Apr. 28, 1999, as amended at 64 Fruit, stone, group 12 ...... 0 .05 FR 31511, June 11, 1999; 66 FR 48613, Sept. 21, Goat, fat ...... 0 .5 Goat, kidney ...... 6 .0 2001] Goat, meat byproducts, except kidney ...... 1 .5 Goat, meat ...... 1.0 § 180.490 Imazapic-ammonium; toler- Grain, aspirated fractions (of which no more ances for residues. than 720 ppm is TMS) ...... 1,300 Grape ...... 0 .10 (a) General. (1) Tolerances are estab- Grape, raisin (of which no more than 0.05 ppm lished for combined residues of the her- is TMS)...... 0 .20 ± Hog, fat ...... 0 .5 bicide imazapic, ( )-2-[4,5-dihydro-4- Hog, kidney ...... 6.0 methyl-4-(1-methylethyl)-5-oxo-1H- Hog, meat byproducts, except kidney ...... 1 .5 imidazol-2-yl]-5-methyl-3- Hog, meat ...... 1 .0 pyridinecarboxylic acid and its me- Horse, fat ...... 0 .5 Horse, kidney ...... 6 .0 tabolite (±)-2-[4,5-dihydro-4-methyl-4- Horse, meat byproducts, except kidney ...... 1 .5 (1-methylethyl)-5-oxo-1H-imidazol-2- Horse, meat ...... 1 .0 yl]-5-hydroxymethyl-3- Milk ...... 1.5 Nut, tree, group 14 ...... 0 .05 pyridinecarboxylic acid, both free and Pistachio ...... 0.05 conjugated, in or on the following food Poultry, fat ...... 0.05 commodities: Poultry, meat byproducts ...... 0.50 Poultry, meat ...... 0 .05 Parts per Prune (of which no more than 0.05 ppm is Commodity million TMS)...... 0 .20 Radish, roots (of which no more than 15 ppm is Grass, forage ...... 15 TMS) ...... 16 Grass, hay ...... 30 Radish, tops (of which no more than 8.0 ppm is Peanut ...... 0 .1 TMS) ...... 10 Sheep, fat ...... 0 .5 Sheep, kidney ...... 6.0 (2) Tolerances are also established for Sheep, meat byproducts, except kidney ...... 1 .5 the combined residues of the herbicide Sheep, meat ...... 1.0 imazapic, (±)-2-[4,5-dihydro-4-methyl-4- Sorghum, grain, forage (of which no more than 0.10 ppm is TMS) ...... 0.20 (1-methylethyl)-5-oxo-1H-imidazol-2- Sorghum, grain, grain (of which no more than yl]-5-methyl-3-pyridinecarboxylic acid 15 ppm is TMS) ...... 35 and its free metabolite (±)-2-[4,5- Sorghum, grain, stover (of which no more than dihydro-4-methyl-4-(1-methylethyl)-5- 60 ppm is TMS) ...... 140 Soybean, forage (of which no more than 1 ppm oxo-1H-imidazol-2-yl]-5- is TMS)...... 2 .0 hydroxymethyl-3-pyridinecarboxylic Soybean, hay (of which no more than 2 ppm is acid, in or on the following food com- TMS)...... 5 .0 Soybean, hulls (of which no more than 25 ppm modities: is TMS) ...... 45 Soybean, seed (of which no more than 13 ppm Parts per Commodity million is TMS) ...... 21 Wheat, bran (of which no more than 6.0 ppm is Cattle, fat ...... 0.10 TMS) ...... 30 Cattle, kidney ...... 1 .0 Wheat, forage (of which no more than 30 ppm Cattle, meat byproducts, except kidney ...... 0.1 is TMS) ...... 35 Cattle, meat ...... 0 .1 Wheat, grain (of which no more than 2.5 ppm is TMS) ...... 10 Goat, fat ...... 0 .1 Wheat, hay (of which no more than 0.50 ppm is Goat, kidney ...... 1 .0 TMS) ...... 1 .0 Goat, meat byproducts, except kidney ...... 0 .1 Wheat shorts (of which no more than 0.5 ppm is Goat, meat ...... 0.1 TMS) ...... 1 .5 Horse, fat ...... 0 .1 Wheat, shorts (of which no more than 5.0 ppm Horse, kidney ...... 1 .0 is TMS) ...... 20 Horse, meat byproducts, except kidney ...... 0 .1 Wheat, straw (of which no more than 0.5 ppm is Horse, meat ...... 0 .1 TMS) ...... 1 .0 Milk ...... 0.1 Wheat, straw (of which no more than 40 ppm is Sheep, fat ...... 0 .1 TMS) ...... 90 Sheep, kidney ...... 1.0 Sheep, meat byproducts, except kidney ...... 0 .1 1 There are no U.S. registrations as of the date of publica- Sheep, meat ...... 0.1 tion of the tolerance in the FEDERAL REGISTER (b) Section 18 emergency exemptions. (b) Section 18 emergency exemptions. [Reserved] [Reserved] (c) Tolerances with regional registra- (c) Tolerances with reginal registra- tions. [Reserved] tions. [Reserved]

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(d) Indirect or inadvertent residues. § 180.492 Triflusulfuron methyl; toler- [Reserved] ances for residues. [64 FR 54224, Oct. 6, 1999, as amended at 66 FR (a) General. Tolerances are estab- 64774, Dec. 14, 2001; 66 FR 66332, Dec. 26, 2001] lished for residues of the herbicide, triflusulfuron methyl 2-[[[[[4- § 180.491 Propylene oxide; tolerances (dimethylamino)-6-(2,2,2- for residues. trifluoroethoxy)-1,3,5-triazin-2- (a) General. Propylene oxide may be yl]amino]carbonyl]amino]sulfonyl]-3- safely used in or on foods in accordance methylbenzoate in or on the raw agri- with the following prescribed condi- cultural commodities: tions: Parts per (1) It is intended as a fumigant in or Commodity million on bulk quantities of cocoa, gums, processed spices, and processed Beet, sugar, roots ...... 0 .05 Beet, sugar, tops ...... 0.05 nutmeats (except peanuts) when such Chicory, roots ...... 0 .05 bulk foods are to be further processed into a final food form. (b) Section 18 emergency exemptions. (2) It is applied in fumigation cham- [Reserved] bers not more than one time at a tem- (c) Tolerances with regional registra- perature not in excess of 125 °F. The tions. [Reserved] maximum period of fumigation shall (d) Indirect or inadvertent residues. not exceed 4 hours for cocoa, processed [Reserved] nutmeats (except peanuts), and proc- [67 FR 40196, June 12, 2002] essed spices. For edible gums, the max- imum duration shall be 24 hours. § 180.493 Dimethomorph; tolerances (3) When used as described in para- for residues. graphs (a)(1) and (2) of this section, res- (a) General. A tolerance is established idues shall not exceed the following for the residues of the fungicide limitations: dimethomorph, (E,Z) 4-[3-(4- Parts per chlorophenyl)-3-(3,4-dimethoxyphenyl)- Commodity million 1-oxo-2-propenyl]morpholine in or on the following commodity: Cocoa bean, bean ...... 300 Gum, edible ...... 300 Parts per Nutmeat, processed, except peanuts ...... 300 Commodity million Spices, processed ...... 300 Brassica, head and stem, subgroup 5A ...... 2 .0 (4) When used as a mixture with car- Brassica, leafy greens, subgroup 5B ...... 20 .0 bon dioxide (92 parts of carbon dioxide Grape1 ...... 3 .5 Grape, raisin1 ...... 6 .0 to 8 parts of propylene oxide on a Hop, dried cones ...... 60 weight/weight basis), all commodities Lettuce, head ...... 10 listed in paragraph (a)(3) of this section Lettuce, leaf ...... 10 Potato, wet peel ...... 0 .15 may be processed not more than one Taro, corm ...... 0 .5 time for a period not to exceed 48 hours Taro, leaves ...... 6 .0 and at a temperature not to exceed 125 Vegetable, bulb, group 3 ...... 2 .0 °F. Vegetable, cucurbit, group 9 ...... 0.5 Vegetable, fruiting, group 8 ...... 1.5 (5) To assure safe use of the pesticide, 1 There are no U.S. registrations as of August 25, 2000, for the label and labeling of the pesticide the use of dimethomorph on the growing crops, grape, hop, formulation shall conform to the label and raisins. and labeling registered by the U. S. En- (b) Section 18 emergency exemptions. vironmental Protection Agency. [Reserved] (b) Section 18 emergency exemptions. (c) Tolerances with regional registra- [Reserved] tions. [Reserved] (c) Tolerances with regional registra- (d) Indirect or inadvertent residues. tions. [Reserved] Time-limited tolerances are estab- (d) Indirect or inadvertent residues. lished for inadvertent or indirect resi- [Reserved] dues of the fungicide dimethomorph in [65 FR 33702, May 24, 2000, as amended at 68 or on the following raw agricultural FR 39430, July 1, 2003] commodities when present therein as a

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result of the application of Parts per Revoca- dimethomorph to growing crops. The Commodity tion/expira- million tion date tolerances will expire and are revoked on the dates specified in the following Milk ...... 0.01 None table. Nut tree, group 14 ...... 0.05 None Papaya ...... 0.10 None Pear ...... 0.75 None Expiration/ Pistachio ...... 0.05 None Commodity Parts per revocation million date Sapodilla ...... 0.10 None Sapote, black ...... 0.10 None Grain, cereal group, fodder ...... 0.15 5/12/04 Sapote, mamey ...... 0.10 None Grain, cereal group, forage ...... 0.05 5/12/04 Sheep, fat ...... 0.05 None Grain, cereal group, grain ...... 0.05 5/12/04 Sheep, meat ...... 0.05 None Grain, cereal group, hay ...... 0.10 5/12/04 Sheep, meat by-product ...... 0.05 None Grain, cereal group, straw ...... 0.15 5/12/04 Star apple ...... 0.10 None Strawberry ...... 2.5 None Tomato ...... 0.15 None [62 FR 26416, May 14, 1997, as amended at 62 FR 39961, July 25, 1997; 63 FR 8139, Feb. 18, (b) Section 18 emergency exemptions. 1998; 63 FR 32140, June 12, 1998; 64 FR 18369, [Reserved] Apr. 14, 1999; 64 FR 25455, May 12, 1999; 65 FR (c) Tolerances with regional registra- 58390, Sept. 29, 2000; 66 FR 37598, July 19, 2001; tions. Tolerances with regional reg- 67 FR 35049, May 17, 2002; 67 FR 60923, Sept. istration, as defined in § 180.1(n) are es- 27, 2002; 68 FR 55833, Sept. 29, 2003; 70 FR 7047, Feb. 10, 2005; 71 FR 76177, Dec. 20, 2006] tablished for residues of the insecticide pyridaben [2-tert-butyl-5(4-tert- § 180.494 Pyridaben; tolerance for resi- butylbenzylthio)-4-chloropyridazin- dues. 3(2H)-one] in or on the following raw (a) General. Tolerances are estab- agricultural commodity: lished for residues of the insecticide Parts per Expiration pyridaben [2-tert-butyl-5-(4-tert- Commodity million Date butylbenzylthio)-4-chloropyridazin- Cranberry ...... 0.5 None 3(2H)-one] on the following plants, and of the insecticide pyridaben and its me- (d) Indirect or inadvertent residues. tabolites (2-tert-butyl-5-(4-(1-carboxy-1- [Reserved] methylethyl)benzylthio)-4- chloropyridazin-3(2H)-one] and (2-tert- [65 FR 43712, July 14, 2000, as amended at 66 FR 33199, June 21, 2001; 70 FR 55769, Sept. 23, butyl-5-[4(-1,1-dimethyl-2- 2005] hypdroxyethyl)benzylthio-4- chloropyridazinn-3(2H)-one) on ani- § 180.495 Spinosad; tolerances for resi- mals, as indicated in the following dues. table. (a) General. Tolerances are estab- lished for residues of the insecticide Parts per Revoca- Commodity million tion/expira- spinosad in or on the food commodities tion date in the table to this paragraph. Almond, hulls ...... 4.0 None Spinosad is a fermentation product of Apple ...... 0.5 None Saccharopolyspora spinosa. The product Apple, wet pomace ...... 0.75 None Canistel ...... 0.10 None consists of two related active ingredi- Cattle, fat ...... 0.05 None ents: Spinosyn A (Factor A; CAS# Cattle, meat ...... 0.05 None 131929-60-7) or 2-[(6-deoxy-2,3,4-tri-O- Cattle, meat byproducts ...... 0.05 None methyl-a-L-manno-pyranosyl)oxy]-13- Citrus ...... 0.5 None Citrus, dried pulp ...... 1.5 None [[5-(dimethylamino)-tetrahydro-6- Citrus, oil ...... 10.0 None methyl-2H-pyran-2- yl]oxy]-9-ethyl- Fruit, stone, group 12 ...... 2.5 None 2,3,3a,5a,5b,6,9,10,11,12,13,14,16a,16b- Goat, fat ...... 0.0 None Goat, meat ...... 0.05 None tetradecahydro-14-methyl-1H-as- Goat, meat byproducts ...... 0.05 None Indaceno[3,2-d]oxacyclododecin-7,15- Grape ...... 1.5 None dione; and Spinosyn D (Factor D; CAS# Hog, fat ...... 0.05 None 131929-63-0) or 2-[(6-deoxy-2,3,4-tri-O- Hog, meat ...... 0.05 None Hog meat byproducts ...... 0.05 None methyl-a-L-manno-pyranosyl)oxy]-13- Hop, dried cones ...... 10.0 None [[5-(dimethyl-amino)- tetrahydro-6- Horse, fat ...... 0.05 None methyl-2H-pyran-2-yl]oxy]-9-ethyl- Horse meat ...... 0.05 None Horse meat byproducts ...... 0.05 None 2,3,3a,5a,5b,6,9,10,11,12,13,14,16a, 16b- Mango ...... 0.10 None tetradecahydro-4,14-methyl-1H-as-

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Indaceno[3,2-d]oxacyclododecin-7,15- Parts per Expiration/ dione. Typically, the two factors are Commodity Revocation million Date present at an 85:15 (A:D) ratio. Herb, fresh, subgroup ...... 3.0 None Parts per Expiration/ Hog, fat ...... 33 None Commodity million Revocation Hog, meat byproducts ...... 8.0 None Date Hog, meat ...... 1.5 None Hop, dried cones ...... 22 None Acerola ...... 1.5 None Horse, fat ...... 50 None Alfalfa, seed ...... 0.15 None Horse, liver ...... 10 None Alfalfa, seed screenings ...... 2.0 None Horse, meat ...... 2.0 None Almond, hulls ...... 2.0 None Horse, meat byproducts, except Amaranth, grain, grain ...... 1.0 None liver ...... 5.0 None Amaranth, grain, stover ...... 10 None Ilama ...... 0.3 None Animal feed, nongrass, group, 18 ... 0.02 None Jaboticaba ...... 0.3 None Animal feed, nongrass, group, 18, Juneberry ...... 0.25 None forage ...... 35.0 None Leafy vegetables (except Brassica Animal feed, nongrass, group, 18, vegetables group) ...... 8.0 None hay ...... 30.0 None Legume vegetables, edible podded Apple pomace ...... 0.5 None (Crop Subgroup 6A) ...... 0.30 None Artichoke, globe ...... 0.3 None Legume vegetables, dried shell pea Asparagus ...... 0.2 None and bean (Crop Subgroup 6C) .... 0.02 None Atemoya ...... 0.3 None Legume vegetables, succulent Avocado ...... 0.3 None shelled pea and bean (Crop Sub- Banana ...... 0.25 None Beet, sugar, molasses ...... 0.75 None group 6B) ...... 0.02 None Biriba ...... 0.3 None Lingonberry ...... 0.250 None Brassica, head and stem, subgroup Longan ...... 0.3 None 5A ...... 2.0 None Lychee ...... 0.3 None Bushberry subgroup 13B ...... 0.250 None Mango ...... 0.3 None Canistel ...... 0.3 None Milk ...... 7.0 None Cattle, fat ...... 50 None Milk, fat ...... 85 None Cattle, liver ...... 10 None Nut, tree, group 14 ...... 0.02 None Cattle, meat ...... 2.0 None Okra ...... 0.40 None Cattle, meat byproducts, except Onion, green ...... 2.0 None liver ...... 5.0 None Papaya ...... 0.3 None Cherimoya ...... 0.3 None Passionfruit ...... 0.3 None Citrus, oil ...... 3.0 None Peanut ...... 0.02 None Citrus, dried pulp ...... 0.5 None Peanut, hay ...... 11.0 None Coriander, leaves ...... 8.0 None Peppermint, tops ...... 3.5 None Corn, sweet, kernel plus cob with Pistachio ...... 0.020 None husks removed ...... 0.02 None Poultry, fat ...... 1.3 None Cotton, gin byproducts ...... 1.5 None Poultry, meat ...... 0.10 None Cotton, undelinted seed ...... 0.02 None Poultry, meat byproducts ...... 0.10 None Cranberry ...... 0.01 None Pulasan ...... 0.3 None Cranberry subgroup 13A ...... 0.7 None Rambutan ...... 0.3 None Custard apple ...... 0.3 None Rice, hulls ...... 4.0 None Egg ...... 0.30 None Salal ...... 0.250 None Feijoa ...... 05 None Sapodilla ...... 0.3 None Fig ...... 0.10 None Sapote, black ...... 0.3 None Food commodities ...... 0.02 None Sapote, mamey ...... 0.3 None Fruit, citrus, group 10 ...... 0.3 None Sapote, white ...... 0.3 None Fruit, pome, group 11 ...... 0.20 None Sheep, fat ...... 50 None Fruit, stone, group 12 ...... 0.20 None Sheep, liver ...... 10 None Goat, fat ...... 50 None Sheep, meat ...... 2.0 None Goat, liver ...... 10 None Sheep, meat byproducts, except Goat, meat ...... 2.0 None liver ...... 5.0 None Goat, meat byproducts, except liver 5.0 None Soursop ...... 0.3 None Grain, aspirated fractions ...... 200 None Soybean ...... 0.02 None Grain, cereal, group 15 ...... 1.5 None Spanish lime ...... 0.3 None Grain, cereal, group 16, forage, ex- Spearmint, tops ...... 3.5 None cept rice ...... 2.5 None Star apple ...... 0.3 None Grain, cereal, group 16, hay, except Starfruit ...... 0.3 None rice ...... 10.0 None Strawberry ...... 1.0 None Grain, cereal, group, 16, stover, ex- Sugar apple ...... 0.3 None cept rice ...... 10.0 None Ti, leaves ...... 10.0 None Grain, cereal, group, 16, straw, ex- Vegetable, brassica, leafy, group 5 10.0 None cept rice ...... 1.0 None Vegetable, bulb, group 3, except Grape ...... 0.50 None green onion ...... 0.10 None Grape, raisin ...... 0.70 None Vegetable, cucurbit (cucumber, Grass, forage, fodder and hay, melon, squashes), group 9 ...... 0.3 None group 17, forage ...... 10.0 None Vegetable, foliage of legume, group Grass, forage, fodder and hay, 7 ...... 8.0 None group 17, hay ...... 5.0 None Vegetable, fruiting, group 8 ...... 0.4 None Guava ...... 0.3 None Vegetable, leaves of root and tuber, Herb, dried, subgroup ...... 22 None group 2 ...... 10.0 None

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its metabolites determined as 2- Parts per Expiration/ Commodity Revocation (difluoromethyl)-6-(trifluoromethyl)- million Date 3,4,5-pyridinetricarboxylic acid, all ex- Vegetable, root and tuber, group 1 0.10 None pressed as the parent equivalents in or Watercress ...... 8.0 None on the following raw agricultural com- Wax jambu ...... 0.3 None modities:

(b) Section 18 emergency exemptions. Parts per Factor A is 2-[(6-deoxy-2,3,4-tri-O-meth- Commodities million yl-o-L-mannopyranosyl)oxy]-13-[[5- Grapefruit ...... 0 .05 (dimethlamino)- tetrahydro-6-methyl- Orange, sweet ...... 0 .05 2H-pyran-2-yl]oxy]9-ethyl- 2,3,3a,5a,6,9,10,11,12,13,14,16a, [62 FR 9978, Mar. 5, 1997] 6b,tetradecahydro-14-methyl-1H-as- Indaceno[3,2d]oxacyclododecin-7,15- § 180.497 Clofencet; tolerances for resi- dione. Factor D is 2-[6-deoxy-2,3,4-tri-O- dues. methyl-o-L-mannopyranosyl)oxy]13-[[5- (a) Tolerances—general. Tolerances (dimethylamino)-tetrahydri-6-methyl- are established for the plant growth 2H-pyran-2-yl]oxy]-9-ethyl- regulator (hybridizing agent) clofencet, 2,3,3a,5a,5b,6,9,10,11,12,13,14,16a,16b- [2-(4-chlorophenyl)-3-ethyl-2,5 dihydro- tetradecahydro-4,14,dimethyl-1H-as- 5-oxo-4-pyridazinecarboxylic acid, po- Indaceno[3,2d]oxacyclododecin-7,15- tassium salt] expressed as the free acid dione. in or on the following raw agricultural commodities: Parts per Expiration/ Commodity million Revocation date Parts per Commodities million Cattle, fat ...... 15.0 12/31/05 Cattle, meat byproducts ...... 3.50 12/31/05 Cattle, fat ...... 0.04 Cattle, meat ...... 0.60 12/31/05 Cattle, kidney ...... 10 .0 Egg ...... 0.030 12/31/05 Cattle, meat byproducts, except kidney ...... 0.5 Goat, fat ...... 15.0 12/31/05 Cattle, meat ...... 0 .15 Goat, meat byproducts ...... 3.50 12/31/05 Egg ...... 1 .0 Goat, meat ...... 0.60 12/31/05 Goat, fat ...... 0 .04 Hog, fat ...... 15.0 12/31/05 Goat, kidney ...... 10.0 Hog, meat byproducts ...... 3.50 12/31/05 Goat, meat byproducts, except kidney ...... 0 .5 Hog, meat ...... 0.60 12/31/05 Goat, meat ...... 0.15 Horse, fat ...... 15.0 12/31/05 Hog, fat ...... 0 .04 Horse, meat byproducts ...... 3.50 12/31/05 Hog, kidney ...... 10.0 Horse, meat ...... 0.60 12/31/05 Hog, meat byproducts, except kidney ...... 0 .5 Poultry, fat ...... 0.30 12/31/05 Hog, meat ...... 0 .15 Sheep, fat ...... 15.0 12/31/05 Horse, fat ...... 0 .04 Sheep, meat byproducts ...... 3.50 12/31/05 Horse, kidney ...... 10 .0 Sheep, meat ...... 0.60 12/31/05 Horse, meat byproducts, except kidney ...... 0 .5 Horse, meat ...... 0 .15 (c) Tolerances with regional registra- Milk ...... 0.02 tions. [Reserved] Poultry, fat ...... 0.04 Poultry, meat byproducts ...... 0.20 (d) Indirect or inadvertent residues. Poultry, meat ...... 0 .15 [Reserved] Sheep, fat ...... 0 .04 Sheep, kidney ...... 10.0 [62 FR 8631, Feb. 26, 1997] Sheep, meat byproducts, except kidney ...... 0 .5 Sheep, meat ...... 0.15 EDITORIAL NOTE: For FEDERAL REGISTER ci- Wheat, forage ...... 10.0 tations affecting § 180.495, see the List of CFR Wheat, grain ...... 250 .0 Sections Affected, which appears in the Wheat, hay ...... 40 .0 Finding Aids section of the printed volume Wheat, straw ...... 50 .0 and on GPO Access. (b) Tolerances for indirect or inad- § 180.496 Thiazopyr; tolerances for res- vertent residues. Tolerances are estab- idues. lished for indirect or inadvertent resi- Tolerances are established for com- dues of the plant growth regulator bined residues of the herbicide (hybridizing agent) clofencet, [2-(4- thiazopyr (3-pyridinecaroxylic acid, 2- chlorophenyl)-3-ethyl-2,5-dihydro-5- (difluoromethyl)-5-(4,5-dihydro-2- oxo-4-pyridazinecarboxylic acid, potas- thiazolyl)-4-(2-methylpropyl)-6- sium salt] expressed as the free acid in (trifluoromethyl)-, methyl ester) and or on the following raw agricultural

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commodities when present therein as a Commodity Parts per result of the application of clofencet to million the growing crops in paragraph (a) of Horseradish, roots ...... 0 .20 this section: Pea and bean, dried shelled, except soybean, subgroup 6C ...... 0 .15 Parts per Peanut ...... 0 .20 Commodities million Peanut, meal ...... 0 .40 Grain, cereal group (except rice, wild rice, sweet Peppermint, tops ...... 0 .30 corn and wheat), forage ...... 4 .0 Potato ...... 0 .15 Grain, cereal group (except rice, wild rice, sweet Spearmint, tops ...... 0 .30 corn and wheat, grain ...... 20 .0 Sugarcane, cane ...... 0.15 Grain, cereal group (except rice, wild rice, sweet Sugarcane, molasses ...... 0 .20 corn and wheat), hay ...... 15 .0 Sunflower, seed ...... 0.20 Grain, cereal group (except rice, wild rice, sweet corn and wheat), stover (fodder) ...... 1 .0 Grain, cereal group (except rice, wild rice, sweet (b) Section 18 emergency exemptions. corn and wheat), straw ...... 4 .0 Time-limited tolerances are estab- Soybean ...... 30.0 Soybean, forage ...... 10 .0 lished for residues of the herbicide N- Soybean, hay ...... 10 .0 [2,4-dichloro-5-[4- (difluoromethyl)-4,5- dihydro-3-methyl-5-oxo-1H-1,2,4-triazol- [62 FR 9983, Mar. 5, 1997] 1-y-l]phenyl] methanesulfonamide and its metabolites 3-hydroxymethyl § 180.498 Sulfentrazone; tolerances for sulfentrazone and 3-desmethyl residues. sulfentrazone, in connection with use (a)(1) General. A tolerance is estab- of the pesticide under section 18 emer- lished for combined residues of the her- gency exemptions granted by EPA. The bicide sulfentrazone N-[2,4-dichloro-5- tolerance is specified in the following [4-(difluoromethyl)-4,5-dihydro-3-meth- table. The tolerances expire and will be yl-5-oxo-1H-1,2,4-triazol-1- revoked by EPA on the date specified yl]phenyl]methanesulfonamide and its in the table. major metabolite 3-hydroxymethyl sulfentrazone N-[2,4-dichloro-5-[4- Expiration/ Commodity Parts per revocation (difluoromethyl)-4,5-dihydro-3- million date hydroxymethyl-5-oxo-1H-1,2,4-triazol-1- yl]phenyl]methanesulfonamide in or on Bean, succulent seed without pod the following raw agricultural com- (lima bean & cowpea) ...... 0.1 12/31/07 modity: Flax, seed ...... 0.20 12/31/07 Strawberry ...... 0.60 12/31/07 Parts per Commodity million (c) Tolerances with regional registra- Soybean, seed ...... 0 .05 tions. [Reserved] (d) Indirect or inadvertent residues. (2) Tolerances are established for Tolerances are established for inad- combined residues of the herbicide vertent and indirect combined residues sulfentrazone and its metabolites HMS of the herbicide sulfentrazone (N-[2,4- (N-(2,4-dichloro-5-(4-(difluoromethyl)- dichloro-5-[4-(difluoromethyl)-4,5- 4,5-dihydro-3-hydroxymethyl-5-oxo-1H- dihydro-3-methyl-5-oxo-1H-1,2,4-triazol- 1,2,4-triazol- 1- 1-yl]phenyl]methanesulfonamide) and yl)phenyl)methanesulfonamide) and its metabolites 3-hydroxymethyl DMS (N-(2,4-dichloro-5-(4- sulfentrazone (N-[2,4-dichloro-5-[4- (difluoromethyl)-4,5-dihydro-5-oxo-1H- (difluoromethyl)-4,5-dihydro-3- 1,2,4-triazol-1- hydroxymethyl-5-oxo-1H-1,2,4-triazol-1- yl)phenyl)methanesulfonamide in or on yl]phenyl]methanesulfonamide) and 3- the following food commodities: desmethyl sulfentrazone (N-[2,4- Parts per dichloro-5-[4-(difluoromethyl)-4,5- Commodity million dihydro-5-oxo-1H-1,2,4-triazol-l- Asparagus ...... 0.15 yl]phenyl]methanesulfonamide) in or Bean, lima, succulent ...... 0 .15 on the following raw agricultural com- Cabbage ...... 0 .20 modities when present therein as a re- Corn, field, forage ...... 0 .20 Corn, field, grain ...... 0 .15 sult of the application of sulfentrazone Corn, field, stover ...... 0 .30 to growing crops.

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Parts per Parts per Commodity million Commodity million

Grain, cereal (excluding sweet corn), Bran ...... 0 .15 Cattle, fat ...... 0.05 Grain, cereal (excluding sweet corn), Forage ..... 0 .2 Cattle, kidney ...... 0 .20 Grain, cereal (excluding sweet corn), Grain ...... 0 .1 Cattle, meat ...... 0 .05 Grain, cereal (excluding sweet corn), Hay ...... 0 .2 Cattle, meat byproducts (except kidney) ...... 0 .05 Grain, cereal (excluding sweet corn), Hulls ...... 0 .30 Corn, field, forage ...... 0 .05 Grain, cereal (excluding sweet corn), Stover ...... 0 .1 Corn, field, grain ...... 0 .05 Grain, cereal (excluding sweet corn), Straw ...... 0.6 Corn, field, stover ...... 0 .05 Fish ...... 1 .0 Goat, fat ...... 0 .05 [62 FR 10708, Mar. 10, 1997, as amended at 64 Goat, kidney ...... 0 .20 FR 51067, Sept. 21, 1999; 65 FR 67279, Nov. 9, Goat, meat ...... 0.05 Goats, meat byproducts (except kidney) ...... 0 .05 2000; 65 FR 82940, Dec. 29, 2000; 66 FR 39658, Grass, forage ...... 100 Aug. 1, 2001; 67 FR 46884, July 17, 2002; 67 FR Grass, hay ...... 30 54118, Aug. 21, 2002; 68 FR 2247, Jan. 16, 2003; Horse, fat ...... 0 .05 68 FR 55280, Sept. 24, 2003; 69 FR 29459, May Horses, kidney ...... 0 .20 24, 2004; 69 FR 71717, Dec. 10, 2004; 70 FR 7047, Horse, meat ...... 0 .05 Feb. 10, 2005] Horses, meat byproducts (except kidney) ...... 0 .05 Milk ...... 0.01 Sheep, fat ...... 0 .05 § 180.499 Propamocarb hydrochloride, Sheep, kidney ...... 0.20 tolerances for residues. Sheep, meat ...... 0.05 Sheep, meat byproducts (except kidney) ...... 0.05 (a) General. Tolerances are estab- Shellfish ...... 0 .10 lished for the residues of propyl[3- (dimethylamino)propyl]carbamate (b) Section 18 emergency exemptions. monohydrochloride also known as [Reserved] propamocarb hydrochloride in or on (c) Tolerances with regional registra- the following raw agricultural com- tions. [Reserved] modity: (d) Indirect or inadvertent residues. [Reserved] Commodity Parts per million [68 FR 55484, Sept. 26, 2003] Lettuce, head ...... 50 Lettuce, leaf ...... 90 § 180.501 Hydroprene; tolerances for Potato ...... 0 .06 residues. Tomato, paste ...... 5 .0 (a) General. A tolerance of 0.2 part per Vegetable, cucurbit, group 9 ...... 1.5 Vegetable, fruiting, group 8 ...... 2.0 million is established for residues of hydroprene [(S)-(Ethyl (2E,4E,7S)- (b) Section 18 emergency exemptions. 3,7,11-trimrthyl-2,4-dodecadienoate)], [Reserved] (CAS Reg. No. 65733–18–8) on food com- (c) Tolerance with regional registra- modities in food-handling establish- tions. [Reserved] ments in accordance with the following (d) Indirect or inadvertent residues. prescribed conditions: [Reserved] (1) Application shall be limited to spot, crack and crevice, perimeter and [62 FR 15620, Apr. 2, 1997, as amended at 62 ultra low volume (ULV) fogging treat- FR 26966, May 16, 1997; 63 FR 32136, June 12, 1998; 64 FR 16843, Apr. 7, 1999; 65 FR 58399, ment in food storage or food-handling Sept. 29, 2000; 66 FR 37598, July 19, 2001; 66 FR establishments, including warehouses, 48585, Sept. 21, 2001; 67 FR 35049, May 17, 2002; food service, manufacturing, and proc- 69 FR 47022, Aug. 4, 2004; 70 FR 7047, Feb. 10, essing establishments such as res- 2005] taurants, cafeterias, supermarkets, bakeries, breweries, dairies, meat § 180.500 Imazapyr; tolerances for resi- slaughtering and packing plants, and dues. canneries where food and food products (a) General. Tolerances are being es- are held, processed, and served: Pro- tablished for residues of the herbicide vided that the food is removed or cov- imazapyr, [2-[4,5-dihydro-4-methyl-4-(1- ered prior to such use, and food-proc- methylethyl)-5-oxo-1H-imidazol-2-yl]-3- essing surfaces are covered during pyridinecarboxylic acid], applied as the treatment or thoroughly cleaned before acid or ammonium salt, in or on the using, or in the case of point-source de- following raw agricultural commod- vice treatments, devices must not ities: come into direct contact with food

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preparation surfaces and must be in a Commodity Parts per minimum distance of 3 feet from ex- million posed foods. Vegetable, fruiting, group 8 ...... 0.2 (2) To assure safe use of the insect 1There are no U.S. registrations for grape and lychee. growth regulator, the label and label- ing shall conform to that registered by (b) Section 18 emergency exemptions. the U.S. Environmental Protection [Reserved] Agency, and it shall be used in accord- (c) Tolerances with regional registra- ance with such label and labeling. tions. [Reserved] (b) Section 18 emergency exemptions. (d) Indirect or inadvertent residues. [Reserved] [Reserved] (c) Tolerances with regional registra- [62 FR 26411, May 14, 1997, as amended at 62 tions. [Reserved] FR 39956, July 25, 1997; 63 FR 24949, May 6, (d) Indirect or inadvertent residues. 1998; 63 FR 66464, Dec. 2, 1998; 64 FR 6539, Feb. [Reserved] 10, 1999; 64 FR 47689, Sept. 1, 1999; 66 FR 37598, July 19, 2001; 67 FR 35049, May 17, 2002; 68 FR [62 FR 61647, Nov. 19, 1997, as amended at 71 41936, July 16, 2003; 70 FR 7047, Feb. 10, 2005] FR 74818, Dec. 13, 2006] § 180.504 [Reserved] § 180.502 Aminoethoxyvinylglycine hy- drochloride (aviglycine HCl); toler- § 180.505 Emamectin; tolerances for ances for residues. residues. (a) General. Tolerances are estab- (a) General. (1) Tolerances are estab- lished for residues of lished for combined residues of aminoethoxyvinylglycine hydro- emamectin (a mixture of a minimum of chloride (aviglycine HCl) in or on the 90% 4′-epi-methylamino-4′- following food commodities: deoxyavermectin B1a and maximum of 10% 4′-epi-methylamino-4′- Commodity Parts per million deoxyavermectin B1b) and its metabo- lites 8,9-isomer of the B1a and B1b com- Apple ...... 0.08 ′ Fruit, stone, group 12, except cherry ...... 0.170 ponent of the parent (8,9-ZMA), or 4 - Pear ...... 0.08 deoxy-4′-epi-amino-avermectin B1a and 4′-deoxy-4′-epi-amino-avermectin B1b; (b) Section 18 emergency exemptions. 4′-deoxy-4′-epi-amino avermectin B1a [Reserved] (AB1a); 4′-deoxy-4′-epi-(N-formyl-N- (c) Tolerances with regional registra- methyl)amino-avermectin (MFB1a); and tions. [Reserved] 4′-deoxy-4′-epi-(N-formyl)amino- (d) Indirect or inadvertent residues. avermectin B1a (FAB1a) in or on the fol- [Reserved] lowing commodities: [62 FR 24838, May 7, 1997, as amended at 64 Commodity Parts per FR 31129, June 10, 1999; 66 FR 36481, 36484, million July 12, 2001; 69 FR 7606, Feb. 18, 2004] Apple, wet pomace ...... 0.075 Cotton, gin byproducts ...... 0.050 § 180.503 Cymoxanil, tolerance for resi- Cotton, undelinted seed ...... 0.025 dues. Fruit, pome, group 11 ...... 0.025 (a) General. A tolerance is established Tomato, paste ...... 0.150 Turnip, greens ...... 0.050 for residues of the fungicide, Vegetable, Brassica, leafy, group 5 ...... 0.050 cymoxanil, 2-cyano-N- Vegetable, fruiting (except Cucurbits), group 8 .... 0.020 [(ethylamino)carbonyl]-2- Vegetable, leafy, except Brassica, group 4 ...... 0.100 (methoxyimino) acetamide, in or on the following food commodity. (2) Tolerances are also established for combined residues of emamectin Parts per (MAB1a + MAB1b isomers) and the asso- Commodity million ciated 8,9-Z isomers (8,9-ZB1a + 8,9-ZB1b) Grape 1 ...... 0 .1 in/on the following commodities when Hop, dried cones ...... 1 .0 present therein as a result of the appli- Lettuce, head ...... 4.0 cation of emamectin to crops listed in Lychee 1 ...... 1 .0 Potato ...... 0 .05 the table in paragraph (a)(1) of this sec- Vegetable, cucurbit, group 9 ...... 0.05 tion:

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(c) Tolerances with regional registra- Commodity Parts per million tions. [Reserved] Cattle, fat ...... 0.010 (d) Indirect or inadvertent residues. Cattle, liver ...... 0.050 [Reserved] Cattle, meat ...... 0.003 Cattle, meat byproducts, except liver ...... 0.020 [62 FR 28355, May 23, 1997; 62 FR 34182, June Goat, fat ...... 0.010 25, 1997] Goat, liver ...... 0.050 Goat, meat ...... 0.003 Goat, meat byproducts, except liver ...... 0.020 § 180.507 Azoxystrobin; tolerances for Horse, fat ...... 0.010 residues. Horse, liver ...... 0.050 (a) General. (1) Tolerances are estab- Horse, meat ...... 0.003 Horse, meat byproducts, except liver ...... 0.020 lished for residues of the fungicide, Milk ...... 0.003 azoxystrobin, [methyl(E)-2-(2-(6-(2- Sheep, fat ...... 0.010 cyanophenoxy) pyrimidin-4- Sheep, liver ...... 0.050 Sheep, meat ...... 0.003 yloxy)phenyl)-3-methoxyacrylate] and Sheep, meat byproducts, except liver ...... 0.020 the Z-isomer of azoxystrobin, [meth- yl(Z)-2-(2-(6-(2- (b) Section 18 emergency exemptions. cyanophenoxy)pyrimidin-4- [Reserved] yloxy)phenyl)-3 methoxyacrylate] in or (c) Tolerances with regional registra- on the following food commodities and tions. [Reserved] processed food: (d) Indirect and inadvertant residues. [Reserved] Parts per Commodity million [71 FR 18649, Apr. 12, 2006] Acerola ...... 2.0 Almond, hulls ...... 4 .0 § 180.506 Cyclanilide; tolerances for Artichoke, globe ...... 4.0 residues. Asparagus ...... 0.04 (a) General. Tolerances are estab- Atemoya ...... 2 .0 Avocado ...... 2 .0 lished for residues of the plant growth Banana (pre-harvest and post harvest) ...... 2 .0 regulator, cyclanilide, [1-(2,4- (of which not more than 0.1 is contained in the pulp) dichlorophenylaminocarbonyl)- Barley, bran ...... 0 .2 Barley, grain ...... 0 .1 cyclopropane carboxylic acid] deter- Barley, hay ...... 15 .0 mined as 2,4-dichloroaniline (cal- Barley, straw ...... 4 .0 culated as cyclanilide) in or on the fol- Biriba ...... 2 .0 lowing food commodities and processed Brassica, head and stem, subgroup 5A ...... 3 .0 Brassica, leafy greens, subgroup 5B ...... 25 feed: Bushberry subgroup 13B ...... 3 .0 Caneberry subgroup 13A ...... 5 .0 Commodity Parts Per Canistel ...... 2 .0 Million Canola, seed ...... 1 .0 Citrus, dried pulp ...... 20 .0 Cattle, fat ...... 0.10 Citrus, oil ...... 40.0 Cattle, meat ...... 0 .02 Cherimoya ...... 2 .0 Cattle, meat byproducts, except kidney ...... 0.2 Coriander, leaves ...... 30 .0 Cattle, kidney ...... 2 .0 Corn, field, forage ...... 12 .0 Cotton, undelinted seed ...... 0 .60 Corn, field, grain ...... 0 .05 Cotton, gin byproducts ...... 25 .0 Corn, field, refined oil ...... 0 .3 Goat, fat ...... 0 .10 Goat, meat ...... 0.02 Corn, field, stover ...... 25 .0 Goat, meat byproducts, except kidney ...... 0 .20 Corn, pop, grain ...... 0.05 Goat, kidney ...... 2 .0 Corn, pop, stover ...... 25.0 Horse, fat ...... 0 .10 Corn, sweet, forage ...... 12 .0 Horse, meat ...... 0 .02 Corn, sweet, kernel plus cob with husks re- Horse, meat byproducts, except kidney ...... 0 .20 moved ...... 0 .05 Horse, kidney ...... 2 .0 Corn, sweet, stover ...... 25.0 Hog, fat ...... 0 .10 Cotton, gin byproducts ...... 0 .02 Hog, meat ...... 0 .02 Cotton, undelinted seed ...... 0 .02 Hog, meat byproducts, except kidney ...... 0 .20 Crambe, seed ...... 0.5 Hog, kidney ...... 2.0 Cranberry ...... 0 .50 Milk ...... 0.04 Cucurbits ...... 0 .3 Sheep, fat ...... 0 .10 Custard apple ...... 2 .0 Sheep, meat ...... 0.20 Feijoa ...... 2 .0 Sheep, meat byproducts, except kidney ...... 0 .20 Flax, seed ...... 0 .5 Sheep, kidney ...... 2.0 Fruit, citrus, group 10 ...... 10 .0 Fruit, stone ...... 1 .5 Grain, aspirated fractions ...... 10 (b) Section 18 emergency exemptions. Grain, aspirated fractions ...... 30.0 [Reserved] Grape ...... 1 .0

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Parts per Parts per Commodity million Commodity million

Grass, forage 1 ...... 15 Watercress ...... 3 .0 Grass, hay 1 ...... 20 Wax jambu ...... 2 .0 Guava ...... 2 .0 Wheat, bran ...... 0.20 Herb Subgroup 19A, dried leaves ...... 260 Wheat, grain ...... 0 .10 Herb Subgroup 19A, fresh leaves ...... 50 Wheat, hay ...... 15 Hop, dried cones ...... 20 .0 Wheat, straw ...... 4 .0 Ilama ...... 2 .0 Jaboticaba ...... 2 .0 (2) Tolerances are established for res- Jackfruit ...... 2 .0 Juneberry ...... 3 .0 idues of the fungicide, azoxystrobin Lingonberry ...... 3.0 [methyl(E)-2-(2-(6-(2- Longan ...... 2 .0 cyanophenoxy)pyrimidin-4- Loquat ...... 2 .0 Lychee ...... 2 .0 yloxy)phenyl)-3-methoxyacrylate] in or Mango ...... 2.0 on the following food commodities. Mustard, field, seed ...... 0 .5 Mustard, Indian, seed ...... 0 .5 Commodity Parts per Mustard, seed ...... 0 .5 million Nut, tree, group 14 ...... 0 .02 Okra ...... 2.0 Cattle, fat ...... 0.03 Onion, dry bulb ...... 1 .0 Cattle, meat ...... 0 .01 Onion, green ...... 7 .5 Cattle, meat byproducts ...... 0.07 Passionfruit ...... 2 .0 Goat, fat ...... 0 .03 Pawpaw ...... 2 .0 Goat, meat ...... 0.01 Papaya ...... 2 .0 Goat, meat byproducts ...... 0 .07 Pea and bean, dried shelled, except soybean, Hog, fat ...... 0 .010 Hog, meat ...... 0 .01 subgroup 6C ...... 0 .5 Hog, meat byproducts ...... 0 .010 Pea and bean, succulent shelled, subgroup 6B 0 .5 Horse, fat ...... 0 .03 Peanut ...... 0 .2 Horse, meat ...... 0 .01 Peanut, refined oil ...... 0.6 Horse, meat byproducts ...... 0 .07 Peanut, hay ...... 15.0 Milk...... 0 .006 Pecan ...... 0 .01 Sheep, fat ...... 0 .03 Peppermint, tops ...... 30 Sheep, meat ...... 0.01 Persimmon ...... 2 .0 Sheep, meat byproducts ...... 0 .07 Pistachio ...... 0.50 Potato ...... 0 .03 Pulasan ...... 2 .0 (b) Section 18 emergency exemptions. Rambutan ...... 2 .0 Time-limited tolerances are estab- Rapeseed, Indian ...... 0 .5 lished for the combined residues of the Rapeseed, seed ...... 0 .5 Rice, grain ...... 5 .0 fungicide, azoxystrobin, [methyl (E)-2- Rice, hulls ...... 20 (2-(6-(2-cyanophenoxy)pyrimidin-4- Rice, straw ...... 12 yloxy)phenyl)-3-methoxyacrylate) and Safflower, seed ...... 0 .5 Salal ...... 3 .0 the Z isomer of azoxystrobin, [methyl Sapodilla ...... 2 .0 (Z)-2-(2-(6-(2-cyanophenoxy)pyrimidin- Sapote, black ...... 2 .0 4-yloxy)phenyl)-3-methoxyacrylate] in Sapote, mamey ...... 2 .0 connection with use of the pesticide Sapote, white ...... 2 .0 Soursop ...... 2 .0 under section 18 emergency exemptions Soybean, hay ...... 55 .0 granted by EPA. The tolerances are Soybean, hulls ...... 1 .0 specified in the following table. The Soybean, seed ...... 0 .5 Spanish lime ...... 2 .0 tolerances expire and will be revoked Spearmint, tops ...... 30 by EPA on the date specified in the Spice Subgroup 19B, except black pepper ...... 38 table. Star apple ...... 2 .0 Starfruit ...... 2 .0 Expiration/ Strawberry ...... 10 Parts per Commodity million revocation Sugar apple ...... 2 .0 date Sunflower, seed ...... 0.5 Tamarind ...... 2 .0 Brassica, head and stem, subgroup Tomato ...... 0.2 5A ...... 30 12/31/06 Tomato, paste ...... 0 .6 Rice, wild ...... 5.0 12/31/09 Turnip, greens ...... 25 Safflower, seed ...... 1.0 6/30/08 Vegetable, foliage of legume, group 7 ...... 30.0 Vegetable, fruiting, group 8, except tomato ...... 2 .0 (c) Tolerances with regional registra- Vegetable, leafy, except brassica, group 4 ...... 30.0 tion. [Reserved] Vegetable, leaves of root and tuber, group 2 ..... 50 .0 Vegetable, legume, edible podded, subgroup, (d) Indirect or inadvertent residues. except soybean ...... 3.0 [Reserved] Vegetable, root, subgroup 1A ...... 0 .5 Vegetable, tuberous and corm, subgroup 1C ..... 0.03 [62 FR 32235, June 13, 1997]

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EDITORIAL NOTE: For FEDERAL REGISTER ci- Parts per tations affecting § 180.507, see the List of CFR Commodity million Sections Affected, which appears in the Finding Aids section of the printed volume Citrus hybrids ...... 0 .30 Cotton, gin byproducts ...... 2 .0 and on GPO Access. Cotton, undelinted seed ...... 0 .05 Custard apple ...... 0 .20 § 180.509 Mefenpyr-diethyl; tolerance Feijoa ...... 0 .10 for residues. Fig ...... 0 .30 Fig, dried ...... 1 .0 (a) General. Tolerances are estab- Fruit, citrus ...... 0 .3 lished for residues of the herbicide Fruit, pome ...... 0.2 safener mefenpyr-diethyl (1-(2,4- Fruit, stone, group 12 ...... 1 .0 dichlorophenyl)-4,5-dihydro-5-methyl- Grape ...... 2 .5 Grass, forage, fodder, and hay, group 17, for- 1H-pyrazole-3,5-dicarboxylic acid, age ...... 0 .70 diethyl ester) and its 2,4- Grass, forage, fodder, and hay, group 17, hay ... 1 .1 dichlorophenyl-pyrazoline metabolites Guava ...... 0 .10 at a rate of 0.0267 pound safener per Ilama ...... 0 .20 Jaboticaba ...... 0 .10 acre per growing season in or on fol- Juneberry ...... 1 .0 lowing commodities: Lingonberry ...... 1.0 Loganberry ...... 0 .30 Lychee ...... 0 .30 Commodity Parts per million Mango ...... 1.0 Nut, tree, group 14 ...... 0 .02 Barley, grain ...... 0 .05 Okra ...... 0.02 Barley, hay ...... 0 .2 Olive ...... 1 .0 Barley, straw ...... 0 .5 Olive, oil ...... 2 .0 Cattle, meat byproducts ...... 0.1 Onion, dry bulb ...... 0 .15 Goat, meat byproducts ...... 0 .1 Papaya ...... 1 .0 Hog, meat byproducts ...... 0 .1 Passionfruit ...... 0 .10 Horse, meat byproducts ...... 0 .1 Pistachio ...... 0.02 Sheep, meat byproducts ...... 0 .1 Pulasan ...... 0 .30 Wheat, forage ...... 0 .2 Rambutan ...... 0 .30 Wheat, grain ...... 0 .05 Salal ...... 1 .0 Wheat, hay ...... 0 .2 Sapodilla ...... 1 .0 Wheat, straw ...... 0 .5 Sapote, black ...... 1 .0 Sapote, mamey ...... 1 .0 (b) Section 18 emergency exemptions. Soursop ...... 0 .20 [Reserved] Spanish lime ...... 0 .30 (c) Tolerances with regional registra- Star apple ...... 1 .0 Starfruit ...... 0 .10 tions. [Reserved] Strawberry ...... 0 .30 (d) Indirect or inadvertent residues. Sugar apple ...... 0 .20 [Reserved] Vegetable, cucurbit, group 9 ...... 0.10 Vegetable, fruiting, group 8 ...... 0.2 [68 FR 23046, Apr. 30, 2003] Vegetable, legume, group 6 ...... 0 .20 Walnut ...... 0 .02 § 180.510 Pyriproxyfen; tolerances for Wax jambu ...... 0 .10 residues. White sapote ...... 0 .30 (a) General. (1) Tolerances are estab- (2) A tolerance of 0.10 parts per mil- lished for residues of the insecticide lion is established for all foods as a re- pyriproxyfen 2-[1-methyl-2-(4- sult of the proposed use of NYLAR in phenoxyphenoxy)ethoxypyridine in or food handling establishments where on the following food commodities: food and food products are held, pre- pared, processed or served. Application Parts per Commodity million is limited to space, general surface, spot, and/or crack and crevice treat- Acerola ...... 0.10 ment in food handling establishments Almond, hulls ...... 2 .0 Apple, wet pomace ...... 0 .8 where food and food products are held, Atemoya ...... 0 .20 processed, prepared and served. Space Avocado ...... 1 .0 and general surface application may be Biriba ...... 0 .20 Brassica, head and stem, subgroup 5A ...... 0 .70 used only when the facility is not in Brassica, leafy greens, subgroup 5B ...... 2 .0 operation provided exposed food is cov- Bushberry subgroup 13B ...... 1 .0 ered or removed from the area being Canistel ...... 1 .0 treated prior to application. Spot, and/ Cherimoya ...... 0 .20 Citrus, oil ...... 20 or crack and crevice treatment may be Citrus, dried pulp ...... 2 .0 used while the facility is in operation

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provided exposed food is covered or re- Parts per Expiration/ moved from the area being treated Commodity Revocation million Date prior to application. Food contact sur- faces should be thoroughly washed Citrus, dried pulp ...... 7.5 None with an effective cleaning compound Citrus, oil ...... 80 None Cotton, gin byproducts ...... 20.0 None and rinced with potable water after use Cotton seed ...... 0.35 None of the product. To assure safe use of Cotton, undelinted seed ...... 0.40 12/31/05 this additive, its label and labeling Custard, apple ...... 0.30 None Feijoa ...... 0.30 None shall conform to that registered with Fruit, citrus, Group 10 ...... 2.5 None the U.S. Environmental Protection Fruit, pome, group 11 ...... 4.0 None Agency, and shall be used in accord- Goat, fat ...... 0.05 None Goat, kidney ...... 0.05 None ance with such label and labeling. Goat, liver ...... 0.05 None (b) Section 18 emergency exemptions. Goat, meat ...... 0.05 None Time-limited tolerances are estab- Goat, meat byproducts ...... 0.05 None Grape ...... 0.40 None lished for the residues of the insect Guava ...... 0.30 None growth regulator pyriproxyfen, in con- Hog, fat ...... 0.05 None nection with the use of the pesticide Hog, kidney ...... 0.05 None Hog, liver ...... 0.05 None under section 18 emergency exemptions Hog, meat ...... 0.05 None granted by EPA. The tolerances will Hog, meat byproducts ...... 0.05 None expire on the dates specified in the fol- Horse, fat ...... 0.05 None Horse, kidney ...... 0.05 None lowing table. Horse, liver ...... 0.05 None Horse, meat ...... 0.05 None Parts per Expiration/ Horse, meat byproducts ...... 0.05 None Commodity revocation Ilama ...... 0.30 None million date Jaboticaba ...... 0.30 None Lettuce, head ...... 5.0 None Bean, succulent ...... 0.10 6/30/08 Lettuce, leaf ...... 13.0 None Celery ...... 2.50 6/30/07 Loganberry ...... 0.30 None Strawberry ...... 0.30 12/31/07 Lychee ...... 0.30 None Mango ...... 0.30 None (c) Tolerances with regional registra- Milk ...... 0.01 None tions. [Reserved] Papaya ...... 0.30 None Passion fruit ...... 0.30 None (d) Indirect or inadvertent residues. Peach ...... 9.0 None [Reserved] Pistachio ...... 0.05 None Pulasan ...... 0.30 None [64 FR 10233, Mar. 3, 1999] Rambutan ...... 0.30 None Sapodilla ...... 0.30 None EDITORIAL NOTE: For FEDERAL REGISTER ci- Sapote, black ...... 0.30 None tations affecting § 180.510, see the List of CFR Sapote, mamey ...... 0.30 None Sections Affected, which appears in the Sheep, fat ...... 0.05 None Finding Aids section of the printed volume Sheep, kidney ...... 0.05 None and on GPO Access. Sheep, liver ...... 0.05 None Sheep, meat ...... 0.05 None Sheep, meat byproducts ...... 0.05 None § 180.511 Buprofezin; tolerances for Soursop ...... 0.30 None residues. Spanish lime ...... 0.30 None (a) General. Tolerances are estab- Star apple ...... 0.30 None Starfruit ...... 0.30 None lished for residues of buprofezin in or Sugar apple ...... 0.30 None on the following food commodities: Tomato ...... 0.40 None Vegetable, Cucurbit, Group 9 ...... 0.50 None Wax jambu ...... 0.30 None Parts per Expiration/ Commodity million Revocation Date (b) Section 18 emergency exemption. Acerola ...... 0.30 None [Reserved] Almond ...... 0.05 None (c) Tolerances with regional registra- Almond hulls ...... 2.0 None Atemoya ...... 0.30 None tions. [Reserved] Avocado ...... 0.30 None (d) Indirect or inadvertent residues. Banana ...... 0.20 None [Reserved] Bean, snap, succulent ...... 0.02 None Birida ...... 0.30 None [62 FR 40741, July 30, 1997, as amended at 63 Canistel ...... 0.30 None FR 33585, June 19, 1998; 63 FR 41727, Aug. 5, Cattle, fat ...... 0.05 None 1998; 64 FR 45887, Aug. 23, 1999; 64 FR 59655, Cattle, kidney ...... 0.05 None Nov. 3, 1999; 65 FR 52947, Aug. 31, 2000; 66 FR Cattle, liver ...... 0.05 None Cattle, meat ...... 0.05 None 46389, Sept. 5, 2001; 68 FR 37771, June 25, 2003; Cattle, meat byproducts ...... 0.05 None 70 FR 17907, Apr. 8, 2005; 71 FR 55313, Sept. 22, Cherimoya ...... 0.30 None 2006; 72 FR 35187, June 27, 2007]

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EDITORIAL NOTE: At 72 FR 35187, June 27, (b) Section 18 emergency exemptions. 2007, § 180.511 was amended by adding and re- [Reserved] vising entries in the table in paragraph (a); (c) Tolerances with regional registra- however, the amendment could not be done tions. [Reserved] due to insufficient data. (d) Indirect or inadvertent residues. § 180.512 [Reserved] [Reserved] [68 FR 55527, Sept. 26, 2003, as amended at 70 § 180.513 Chlorfenapyr; tolerances for FR 3654, Jan. 26, 2005] residues. (a) General. (1) Tolerances are estab- § 180.514 Cloransulam-methyl; toler- ances for residues. lished for residues of the insecticide chlorfenapyr [4-bromo-2-(4- (a) General. Tolerances are estab- chlorophenyl)-1-(ethoxymethyl)-5- lished for residues of the herbicide, (trifluoromethyl)-1H-pyrrole-3- cloransulam-methyl, N-(2- carbonitrile] in or on the following raw carboxymethyl-6-chlorophenyl)-5- agricultural commodities: ethoxy-7-fluoro-(1,2,4)-triazolo[1,5c]-py- rimidine-2-sulfonamide, plus its acid, Commodity Parts per cloransulam, calculated as parent ester million in or on the following raw agricultural Vegetable, fruiting, group 8 ...... 1.0 commodities: Parts per (2) A tolerance of 0.01 parts per mil- Commodity million lion is established for residues of Soybean, forage ...... 0 .1 chlorfenapyr in or on all food commod- Soybean, hay ...... 0 .2 ities (other than those covered by a Soybean, seed ...... 0 .02 higher tolerance as a result of use on growing crops) in food/feed handling (b) Section 18 emergency exemptions. areas where food/feed products are pre- [Reserved] pared, held, processed, or served and in (c) Tolerances with regional registra- accordance with the following pre- tions. [Reserved] scribed conditions: (d) Indirect or inadvertent residues. (i) Application shall be no greater [Reserved] than a 0.5% active ingredient solution [62 FR 49163, Sept. 19, 1997] for spot crack and crevice use in food/ feed handling establishments, where § 180.515 Carfentrazone-ethyl; toler- food and food products are held, proc- ances for residues. essed, prepared and/or served. (a) General. Tolerances are estab- (ii) Application may only be under- lished for combined residues of the her- taken when the facility is not in oper- bicide carfentrazone-ethyl (ethyl- ation, and provided exposed food has alpha-2-dichloro-5-[-4-(difluoromethyl)- been covered, or removed from the area 4,5-dihydro-3-methyl-5-oxo-1H-1,2,4- being treated prior to application. triazol-1-yl]-4-fluorobenzene (iii) Food contact surfaces and equip- propanoate) and its metabolite: ment should be throughly washed with carfentrazone-chloropropionic acid an effective cleaning compound, and (alpha, 2-dichloro-5-[-4-difluoromethyl)- rinsed with potable water after each 4,5-dihydro-3-methyl-5-oxo-1H-1,2,4- use of the product. triazol-1-yl]-4-fluorobenzenepropanoic (iv) Contamination of food or food acid) in or on the following raw agri- contact surfaces shall be avoided. Ap- cultural commodities: plication excludes any direct applica- Parts per tion to any food, food packaging, or Commodity million any food contact surfaces. Acerola ...... 0.10 (v) To assure safe use, the label and Almond, hulls ...... 0 .20 labeling shall conform to that reg- Atemoya ...... 0 .10 istered by the U.S. Environmental Pro- Avocado ...... 0 .10 tection Agency, and it shall be used in Banana ...... 0.20 Berry, group 13 ...... 0 .10 accordance with such label and label- Birida ...... 0 .10 ing. Borage ...... 0 .10

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Parts per Parts per Commodity million Commodity million

Cacao ...... 0.10 Rice, straw ...... 1 .0 Cactus ...... 0 .10 Safflower, seed ...... 0 .10 Caneberry subgroup 13A ...... 0 .1 Salal ...... 0 .10 Canistel ...... 0 .10 Sapodilla ...... 0 .10 Canola ...... 0 .10 Sapote, black ...... 0 .10 Cherimoya ...... 0 .10 Sapote, mamey ...... 0 .10 Coffee ...... 0 .10 Shellfish ...... 0 .30 Coconut ...... 0 .10 Sorghum, sweet ...... 0 .10 Corn, field, forage ...... 0 .20 Soursop, group ...... 0.10 Corn, sweet, forage ...... 0 .20 Sorghum, forage ...... 0 .20 Corn, sweet, kernel plus cob with husk removed 0.10 Soybean, seed ...... 0 .1 Cotton, gin by products ...... 10 Spanish lime ...... 0 .10 Cotton, undelinted seed ...... 0 .20 Star apple ...... 0 .10 Cotton, hulls ...... 0 .60 Starfruit ...... 0 .10 Cotton, meals ...... 0 .35 Stevia ...... 0 .10 Cotton, refined oil ...... 1.0 Strawberry ...... 0 .10 Crambe, seed ...... 0.10 Strawberrypear ...... 0 .10 Custard apple ...... 0 .10 Sugar, apple ...... 0.10 Date ...... 0 .10 Sugarcane ...... 0 .10 Fat (cattle, goat, horse, and sheep) ...... 0 .10 Sunflower, seed ...... 0.10 Feijoa ...... 0 .10 Tea ...... 0 .10 Fig ...... 0 .10 Ti, leaves ...... 0 .10 Fish ...... 0 .30 Ti, roots ...... 0 .10 Flax, seed ...... 0 .10 Vanilla ...... 0 .10 Vegetable, bulb, group 03 ...... 0 .10 Fruit, citrus, group 10 ...... 0 .10 Vegetable, brassica, leafy, group 05 ...... 0 .10 Fruit, pome, group 11 ...... 0.10 Vegetable, cucurbit, group 9 ...... 0.10 Fruit, stone, group 12 ...... 0 .10 Vegetable, foliage of legume (except soybean), Grain, cereal, forage (excluding corn and sor- group 07 ...... 0.10 ghum) ...... 1.0 Vegetable, fruiting, group 8 ...... 0.10 Grain, cereal, hay ...... 0 .30 Vegetable, legume, group 06 ...... 0 .10 Grain, cereal, group 15 ...... 0.10 Vegetable, leafy, except brassica, group 04 ...... 0.10 Grain, cereal, stover ...... 0 .30 Vegetable, leaves of root and tuber, group 02 ... 0 .10 Grain, cereal, straw (excluding rice) ...... 0 .10 Vegetable, root and tuber, group 01 ...... 0 .10 Grape ...... 0 .10 Wasabia, roots ...... 0 .10 Grass, forage ...... 5 .0 Wax, Jambu ...... 0.10 Grass, hay ...... 8 .0 Guava ...... 0 .10 Herb and Spices, group 19 ...... 2 .0 (b) Section 18 emergency exemptions. Hop, dried cones ...... 0 .10 Time-limited tolerances are estab- Horseradish ...... 0.10 lished for combined residues of the her- Ilama ...... 0 .10 Jaboticaba ...... 0 .10 bicide carfentrazone-ethyl and its Juneberry ...... 0 .10 chloropropionic acid metabolite in con- Kava, Kava ...... 0 .10 nection with use of the pesticide under Kiwi fruit ...... 0 .10 section 18 emergency exemptions Lingonberry ...... 0.10 Longan ...... 0 .10 granted by EPA. These tolerances will Lychee ...... 0 .10 expire and are revoked on the dates Mango ...... 0.10 specified in the following table. Meat, (cattle, goat, horse, and sheep) ...... 0.10 Meat, byproducts, cattle, goat, horse, and Expiration/ sheep) ...... 0 .10 Commodity Parts per Revocation Milk ...... 0.05 million Date Mulberry, Indian ...... 0 .10 Mustard, seed ...... 0 .10 Hop, dried cones ...... 0.30 6/30/05 Nut, tree, group 14 ...... 0 .10 Tomato, paste ...... 0.60 6/30/07 Okra ...... 0.10 Tomato, puree ...... 0.60 6/30/07 Olive ...... 0 .10 Vegetable, fruiting, group 8 ...... 0.10 6/30/07 Palm heart ...... 0 .10 Palm heart, leaves ...... 0 .10 (c) Tolerances with regional registra- Papaya ...... 0 .10 Passionfruit ...... 0 .10 tions. [Reserved] Pawpaw ...... 0 .10 (d) Indirect or inadvertent residues. Peanut ...... 0 .10 [Reserved] Peanut, hay ...... 0.10 Persimmon ...... 0 .10 [63 FR 52180, Sept. 30, 1998, as amended at 63 Pistachio ...... 0.10 FR 65078, Nov. 25, 1998; 64 FR 45890, Aug. 23, Pomegranate ...... 0 .10 1999; 65 FR 48626, Aug. 9, 2000; 66 FR 39647, Pummelo ...... 0 .10 39682, Aug. 1, 2001; 67 FR 35050, May 17, 2002; Pusalan ...... 0 .10 Rambutan ...... 0 .10 67 FR 40211, June 12, 2002; 68 FR 37765, June Rapeseed, forage ...... 0 .10 25, 2003; 69 FR 29459, May 24, 2004; 69 FR 58078, Rapeseed, seed ...... 0 .10 Sept. 29, 2004]

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§ 180.516 Fludioxonil; tolerances for benzodioxol-4-yl)-1H-pyrrole-3- residues. carbonitrile) in connection with use of (a) General. Tolerances are estab- the pesticide under section 18 emer- lished for residues of the fungicide gency exemptions granted by EPA. The fludioxonil (4-(2,2-difluoro-1,3- tolerances will expire and are revoked benzodioxol-4-yl)-1H-pyrrole-3- on the dates specified in the following carbonitrile) in or on the following table: commodities: Parts per Expiration/ Commodity million revocation Parts per date Commodity million Pomegranate ...... 5.0 6/30/06 Bean, dry ...... 0.4 Bean, succulent ...... 0 .4 (c) Tolerances with regional registra- Brassica, head and stem, subgroup 5A ...... 2 .0 Brassica, leafy greens, subgroup 5B ...... 10 tions. [Reserved] Bushberry subgroup 13B ...... 2 .0 (d) Indirect or inadvertent residues. Caneberry subgroup 13A ...... 5 .0 [Reserved] Carrot ...... 0 .75 Citrus, crop group 10 ...... 10 [62 FR 56082, Oct. 29, 1997] Cotton, gin byproducts ...... 0 .05 Cotton, undelinted seed ...... 0 .05 EDITORIAL NOTE: For FEDERAL REGISTER ci- Flax, seed ...... 0 .05 tations affecting § 180.516, see the List of CFR Forage, fodder, and straw of Grain, cereal ...... 0 .01 Sections Affected, which appears in the Fruit, pome, group 11 ...... 5.0 Finding Aids section of the printed volume Fruit, stone, group 12 ...... 5 .0 and on GPO Access. Grain, cereal ...... 0 .02 Grape ...... 1 .0 Grapefruit, oil ...... 500 § 180.517 Fipronil; tolerances for resi- Grass, forage, fodder and hay, group 17 ...... 0 .01 dues. Herb and spicegroup 19 ...... 0 .02 Herb, dried, subgroup 19A ...... 65 (a) General. Therefore, tolerances are Herb, fresh, subgroup 19A ...... 10 established for combined residues of Juneberry ...... 2 .0 the insecticide fipronil (5-amino-1-[2,6- Kiwifruit ...... 20 dichloro-4-(trifluoromethyl)phenyl]-4- Leafy greens subgroup 4A, except spinach ...... 30 Leafy vegetables except Brassica ...... 0 .01 [(1R,S)-(trifluoromethyl)sulfinyl]-1H- Leaves and roots of tuber vegetables ...... 0 .02 pyrazole-3-carbonitrile) and its me- Lingonberry ...... 2.0 tabolites 5-amino-1-[2,6-dichloro-4- Longan ...... 1 .0 Lychee ...... 1 .0 (trifluoromethyl)phenyl]-4- Melon subgroup 9A ...... 0 .03 [(trifluoromethyl) sulfonyl]-1H-pyr- Non-grass animal feed ...... 0 .01 azole-3-carbonitrile and 5-amino-1-[2,6- Onion, dry bulb ...... 0 .20 dichloro-4-(trifluoromethyl) phenyl]-4- Onion, green ...... 7 .0 Peanut, hay ...... 0.01 [(trifluoromethyl)thio]-1H-pyrazole-3- Peanut, meat (hulls removed) ...... 0 .01 carbonitrile and its photodegradate 5- Pistachio ...... 0.10 amino-1-(2,6-dichloro-4- Pomegranate ...... 5 .0 Pulasan ...... 1 .0 (trifluoromethyl)phenyl]-4-[(1R,S)- Rambutan ...... 1 .0 (trifluoromethyl)]-1H-pyrazole-3- Rapeseed, forage ...... 0 .01 carbonitrile in or on the following Rapeseed, seed ...... 0 .01 items at the levels specified: Safflower, seed ...... 0 .01 Salal ...... 2 .0 Parts per Spanish lime ...... 1 .0 Commodity million Strawberry ...... 2 .0 Sunflower, seed ...... 0.01 Corn, field, grain ...... 0 .02 Turnip, greens ...... 10 Corn, field, stover ...... 0 .30 Vegetable, bulb, group 3 ...... 0 .02 Corn, field, forage ...... 0 .15 Vegetable, cucurbit, group 9 ...... 0.01 Egg ...... 0 .03 Vegetable, foliage of legume, group 7 ...... 0 .01 Fat of cattle, goat, horse and sheep ...... 0 .40 Vegetable, fruiting, group 8 ...... 0.01 Hog Fat ...... 0.04 Vegetable, legume, group 6 ...... 0 .01 Hog Liver ...... 0 .02 Vegetable, root and tuber, group 1 ...... 0 .02 Hog, meat ...... 0 .01 Watercress ...... 7 .0 Hog Meat Byproducts, except liver ...... 0 .01 Yam, true ...... 8 .0 Liver of cattle, goat, horse and sheep ...... 0 .10 Milk, fat (reflecting 0.05 ppm in whole milk) ...... 1 .50 (b) Section 18 emergency exemptions. Meat Byproducts, except liver of cattle, goat, Time-limited tolerances are estab- horse and sheep ...... 0 .04 Meat of cattle, goat, horse and sheep ...... 0.04 lished for residues of the fungicide Poultry Fat ...... 0 .05 fludioxonil (4-(2,2-difluoro-1,3- Poultry Meat ...... 0 .02

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Parts per Parts per Commodity million Commodity million

Poultry, meat byproducts ...... 0.02 Sheep, kidney ...... 0.30 Rice, grain ...... 0 .04 Sheep, meat ...... 0.01 Rice, straw ...... 0 .10 Sheep, mbyp (except kidney) ...... 0.01

(b) Section 18 emergency exemptions. (3) Tolerances are established for the [Reserved] combined residues of the fungicide (c) Tolerances with regional registra- pyrimethanil 4,6-dimethyl-N-phenyl-2- tions. [Reserved] pyrimidinamine and its metabolite 4,6- (d) Indirect or inadvertent residues. dimethyl-2-(phenylamino)-5- [Reserved] pyrimidinol in or on the following com- [62 FR 62979, Nov. 26, 1997, as amended at 63 modity: FR 38495, July 17, 1998] Commodity Parts per § 180.518 Pyrimethanil; tolerances for million residues. Milk ...... 0.03 (a) General. (1) Tolerances are estab- lished for the residues of the fungicide (b) Section 18 emergency exemptions. pyrimethanil 4,6-dimethyl-N-phenyl-2- [Reserved] pyrimidinamine in or on the following (c) Tolerances with regional registra- raw agricultural commodities: tions. [Reserved] (d) Indirect or inadvertent residues. Parts per Commodity million [Reserved]

Almond ...... 0.20 [62 FR 63669, Dec. 2, 1997, as amended at 69 Almond, hulls ...... 12 FR 52443, Aug. 26, 2004] Apple, wet pomace ...... 12 Banana ...... 0.10 § 180.519 Bromide ion and residual Citrus, oil ...... 150 Fruit, citrus, group 10 (post-harvest) ...... 10 bromine; tolerances for residues. Fruit, pome, group 11 (pre-harvest and post-har- (a) General. The food additives, bro- vest) ...... 3 .0 Fruit, stone (except cherry), group 12 ...... 3 .0 mide ion and residual bromine, may be Grape ...... 5 .0 present in water, potable in accordance Grape, raisin ...... 8 .0 with the following conditions: Onion, dry bulb ...... 0 .10 Onion, green ...... 2 .0 (1) The food additives are present as Pistachio ...... 0.20 a result of treating water aboard ships Strawberry ...... 3 .0 with a polybrominated ion-exchange Tomato ...... 0.50 Vegetable, tuberous and corm, subgroup 1C ..... 0.05 resin (as a source of bromine) under the supervision of trained personnel. (2) Tolerances are established for the (2) Residual bromine levels are con- combined residues of the fungicide trolled to not exceed 1.0 part per mil- pyrimethanil 4,6-dimethyl-N-phenyl-2- lion (ppm) in the final treated water. pyrimidinamine and its metabolite 4- Control is effected using calibrated re- [4,6-dimethyl-2- circulating or proportioning bromine pyrimidinyl)amino]phenol in or on the feeder equipment and periodic checks following commodities: of residual bromine using a bromine test kit. To assure safe use of the addi- Parts per tives, the label and labeling of the dis- Commodity million infectant formulation containing the Cattle, fat ...... 0.01 food additives shall conform to the Cattle, kidney ...... 0 .30 label and labeling registered by the Cattle, meat ...... 0 .01 Cattle, mbyp (except kidney) ...... 0 .01 U.S. Environmental Protection Agen- Goat, fat ...... 0 .01 cy. Goat, kidney ...... 0 .30 (3) No tolerance is established for Goat, meat ...... 0.01 Goat, mbyp (except kidney) ...... 0.01 bromide ion levels. Horse, fat ...... 0 .01 (b) Section 18 emergency exemptions. Horse, kidney ...... 0 .30 [Reserved] Horse, meat ...... 0 .01 Horse, mbyp (except kidney) ...... 0 .01 (c) Tolerances with regional registra- Sheep, fat ...... 0 .01 tions. [Reserved]

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(d) Indirect or inadvertent residues. ployed should conform with such label [Reserved] or labeling. (4) The total residue of inorganic bro- [41 FR 17893, Apr. 29, 1976. Redesignated at 41 FR 26568, June 28, 1976, and at 53 FR 24667, mides in fermented malt beverage, re- June 29, 1988. Redesignated and amended at sulting from the use of corn grits and 63 FR 34319, June 24, 1998; 71 FR 74818, Dec. cracked rice fumigated with the fumi- 13, 2006] gant described in paragraph (a)(2) of this section plus additional residues of § 180.521 Fumigants for grain-mill ma- inorganic bromides that may be chinery; tolerances for residues. present from uses in accordance with (a) General. Fumigants may be safely other regulations in this chapter pro- used in or on grain-mill machinery in mulgated under section 408 and/or 409 accordance with the following pre- of the Act, does not exceed 25 parts per scribed conditions: million bromide (calculated as Br). (1) The fumigants consist of methyl (b) Section 18 emergency exemptions. bromide. [Reserved] (2) To assure safe use of the fumi- (c) Tolerances with regional registra- gant, its label and labeling shall con- tions. [Reserved] form to the label and labeling reg- (d) Indirect or inadvertent residues. istered by the U.S. Environmental Pro- [Reserved] tection Agency. (3) Residues of inorganic bromides [71 FR 74818, Dec. 13, 2006] (calculated as Br) in milled fractions § 180.523 Metaldehyde; tolerances for derived from cereal grain from all fu- residues. migation sources, including fumigation of grain-mill machinery, shall not ex- (a) General. The food additive metal- ceed 125 parts per million. dehyde may be safely used as a (b) Section 18 emergency exemptions. preharvest spray or dust on strawberry [Reserved] to control slugs and snails, in accord- (c) Tolerances with regional registra- ance with the following prescribed con- tions. [Reserved] ditions: (d) Indirect or inadvertent residues. (1) The food additive is applied as a [Reserved] preharvest spray or dust on growing strawberry at a rate of not more than [40 FR 14156, Mar. 28, 1975. Redesignated at 41 1 pound per acre, calculated as metal- FR 26568, June 28, 1976, and amended at 49 FR dehyde, and applied not later than 14 44459, Nov. 7, 1984. Redesignated at 53 FR days before first picking. 24667, June 29, 1988, and amended at 54 FR 6130, Feb. 8, 1989. Redesignated and amended (2) A tolerance of zero is established at 63 FR 34319, June 24, 1998] for residues of metaldehyde on straw- berry. § 180.522 Fumigants for processed (3) To insure safe usage of the addi- grains used in production of fer- tive: mented malt beverage; tolerances (i) The label of any market package for residues. of the additive shall bear, in addition (a) General. Fumigants for processed to other information required by the grain may be safely used, in accordance act, the name of the additive. with the following conditions. (ii) The label of any prepared mix or (1) Methyl bromide. Total residues of concentrate shall indicate the percent- inorganic bromides (calculated as Br) age by weight of the additive. from the use of this fumigant shall not (iii) The label shall bear adequate di- exceed 125 parts per milion. rections for use, in conformance with (2) Methyl bromide is used to fumi- paragraph (a) of this section and may gate corn grits and cracked rice in the indicate that in the event the metalde- production of fermented malt beverage. hyde is removed by rain an additional (3) To assure safe use of the fumi- application may be made provided such gant, its label and labeling shall con- application is made not less than 14 form to the label and labeling reg- days before first picking. istered by the U.S. Environmental Pro- (b) Section 18 emergency exemptions. tection Agency, and the usage em- [Reserved]

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(c) Tolerances with regional registra- (b) Section 18 emergency exemptions. tions. [Reserved] [Reserved] (d) Indirect or inadvertent residues. (c) Tolerances with regional registra- [Reserved] tions. [Reserved] [40 FR 14156, Mar. 28, 1975. Redesignated and (d) Indirect or inadvertent residues. amended at 63 FR 34319, June 24, 1998] [Reserved] [40 FR 14161, Mar. 28, 1975, as amended at 50 § 180.525 Resmethrin; tolerances for FR 2959, Jan. 23, 1985, and amended at 53 FR residues. 24668, 24669, June 29, 1988. Redesignated and (a) General. Tolerances are estab- amended at 63 FR 34319, June 24, 1998] lished for residues of the insecticide resmethrin [5-(phenylmethyl)-3- § 180.527 Flufenacet, N-(4- furanyl] methyl 2,2-dimethyl-3-(2- fluorophenyl)-N-(1-methylethyl)-2- [[5-(trifluoromethyl)-1, 3, 4- methyl-1-propenyl) thiadiazol-2-yl] oxy]acetamide and cyclopropanecarboxylate in or on food its metabolites containing the 4- commodities at 3.0 ppm resulting from fluoro-N-methylethyl benzenamine use of the insecticide in food handling tolerances for residues. and storage areas as a space concentra- (a) General. Tolerances are estab- tion for spot/or crack and crevice treat- lished for the combined residues of the ment and shall be limited to a max- herbicide flufenacet, N-(4- imum of 3.00 percent of the active in- fluorophenyl)-N-(1-methylethyl)-2-[[5- gredient by weight, and as a space (trifluoromethyl)-1, 3, 4-thiadiazol-2-yl] treatment shall be limited to a max- oxy]acetamide and its metabolites con- imum of 0.5 fluid ounce of 3.0 percent taining the 4-fluoro-N-methylethyl active ingredient by weight per 1000 benzenamine moiety in or on the fol- cubic feet of space provided that the lowing commodities. food is removed or covered prior to such use. To assure safe use of the ad- Commodity Parts per ditive, its label and labeling shall con- million form to that registered with the U.S. Cattle, kidney ...... 0 .05 Environmental Protection Agency, and Corn, field, forage ...... 0 .4 shall be used in accordance with such Corn, field, grain ...... 0 .05 Corn, field, stover ...... 0 .4 label and labeling. Corn, sweet, forage ...... 0 .45 (b) Section 18 emergency exemptions. Corn, sweet, kernel plus cob with husks re- [Reserved] moved ...... 0 .05 (c) Tolerances with regional registra- Corn, sweet, stover ...... 0 .30 Goat, kidney ...... 0 .05 tions. [Reserved] Hog, kidney ...... 0.05 (d) Indirect or inadvertent residues. Horse, kidney ...... 0 .05 [Reserved] Sheep, kidney ...... 0.05 Soybean, seed ...... 0 .1 [71 FR 74819, Dec. 13, 2006] Wheat, bran ...... 0.80 Wheat, forage ...... 6 .0 § 180.526 Synthetic isoparaffinic petro- Wheat, grain ...... 0 .60 leum hydrocarbons; tolerances for Wheat, hay ...... 1 .2 residues. Wheat, straw ...... 0 .35 (a) General. Synthetic isoparaffinic (b) Section 18 emergency exemptions. petroleum hydrocarbons complying [Reserved] with 21 CFR 172.882 (a) and (b) may be (c) Tolerances with regional registra- safely used as a component of insecti- tions. Tolerances are established for cide formulations for use on animal combined residues of flufenacet, N-(4- feed in an amount no greater than rea- fluorophenyl)-N-(1-methylethyl)-2-[[5- sonably required to accomplish its in- (trifluoromethyl)-1, 3, 4-thiadiazol-2-yl] tended effect as an adjuvant in the in- oxy]acetamide, and its metabolites secticide formulation and shall not be containing the 4-fluoro-N-methylethyl intended to accomplish any effect in benzenamine moiety, with regional animal feed. It is used or intended for registration. use as a component of insecticide for- mulations used in compliance with reg- Commodity Parts per ulations issued in 40 CFR part 180 and million in this part. Grass, forage ...... 7 .0

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tolerance expiration/revocation date of Commodity Parts per million April 26, 2005. Grass, hay ...... 0 .4 (3) To ensure safe use of the additive, its label and labeling shall conform to (d) Indirect or inadvertent residues. that registered with the U.S. Environ- Tolerances are established for indirect mental Protection Agency and it shall or inadvertent residues of the herbicide be used in accordance with such label flufenacet, N-(4-fluorophenyl)-N-(1- and labeling. methylethyl)-2-[[5-(trifluoromethyl)- (b) Section 18 emergency exemptions. 1,3,4-thiadiazol-2-yl]oxy]acetamide and [Reserved] its metabolites containing the 4-fluoro- (c) Tolerances with regional registra- N-methylethyl benzenamine moiety in tions. [Reserved] or on the following raw agricultural (d) Indirect or inadvertent residues. commodities when present therein as a [Reserved] result of application of flufenacet to [63 FR 34828, June 26, 1998, as amended at 69 the growing crops in paragraph (a) of FR 58083, Sept. 29, 2004] this section. § 180.532 Cyprodinil; tolerances for Parts per residues. Commodity million (a) General. (1) Tolerances are estab- Alfalfa, forage ...... 0.1 lished for residues of the fungicide Alfalfa, hay ...... 0.1 Alfalfa, seed ...... 0 .1 cyprodinil, 4-cyclopropyl-6-methyl-N- Clover, forage ...... 0.1 phenyl-2-pyrimidinamine in or on the Clover, hay ...... 0.1 following food commodities: Grain, cereal, group 15, except rice ...... 0 .1 Grain, cereal, forage, fodder, and straw, group Parts per 16, except rice ...... 0 .1 Commodity million Grass, forage, fodder, and hay, group 17 ...... 0 .1 Almond, hulls ...... 8 .0 Almond nutmeats ...... 0 .02 [63 FR 26473, May 13, 1998, as amended by 63 Apple, wet pomace ...... 0 .15 FR 50791, Sept. 23, 1998; 64 FR 42846, Aug. 6, Bean, dry ...... 0.6 1999; 65 FR 64366, Oct. 27, 2000; 68 FR 2247, Bean, succulent ...... 0 .6 Jan. 16, 2003; 68 FR 37759, June 25, 2003; 70 FR Brassica, head and stem, subgroup 5A ...... 1 .0 Brassica, leafy greens, subgroup 5B ...... 10 .0 37696, June 30, 2005; 71 FR 76200, Dec. 20, 2006; Bushberry subgroup 13B ...... 3 .0 72 FR 26310, May 9, 2007] Caneberry subgroup 13A ...... 10 Carrot ...... 0 .75 § 180.530 2,2-Dimethyl-1,3-benzodioxol- Fruit, pome ...... 0.1 4-ol methylcarbamate; tolerances Fruit, stone ...... 2 .0 Grape ...... 2 .0 for residues. Grape, raisin ...... 3 .0 (a) General. (1) The insecticide 2,2-di- Herb, subgroup 19A, dried ...... 15 .0 Herb, subgroup 19A, fresh ...... 3 .0 methyl-1,3-benzodioxol-4-yl Juneberry ...... 3 .0 methylcarbamate may be safely used Leafy greens subgroup 4A, except spinach ...... 30 in spot and/or crack and crevice treat- Lingonberry ...... 3.0 ments in animal feed handling estab- Longan ...... 2 .0 Lychee ...... 2 .0 lishments, including feed manufac- Pistachio ...... 0.10 turing and processing establishments, Pulasan ...... 2 .0 such as stores, supermarkets, dairies, Rambutan ...... 2 .0 Salal ...... 3 .0 meat slaughtering and packing plants, Spanish lime ...... 2 .0 and canneries until the tolerance expi- Turnip, greens ...... 10.0 ration/revocation date of April 26, 2005. Watercress ...... 20 (2) The insecticide 2,2-dimethyl-1,3- benzodioxol-4-yl methylcarbamate may (2) Time-limited tolerances are estab- be safely used in spot and/or crack and lished for residues of the fungicide crevice treatments in food handling es- cyprodinil, 4-cyclopropyl-6-methyl-N- tablishments, including food service, phenyl-2-pyrimidinamine in or on the manufacturing and processing estab- following food commodities. lishments, such as restaurants, cafe- Parts per Expiration/ terias, supermarkets, bakeries, brew- Commodity million revocation eries, dairies, meat slaughtering and date packing plants, and canneries until the Onion, dry bulb ...... 0.60 12/31/07

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fluroxypyr 1-methylheptyl ester [1- Parts per Expiration/ Commodity revocation methylheptyl ((4-amino-3,5-dichloro-6- million date fluoro-2-pyridinyl)oxy)acetate] and its Onion, green ...... 4.0 12/31/07 metabolite fluroxypyr [((4-amino-3,5- Strawberry ...... 5.0 12/31/07 dichloro-6-fluoro-2-pyridinyl)oxy)acetic acid] in or on the following raw agri- (b) Section 18 emergency exemptions. cultural commodities. [Reserved] (c) Tolerances with regional registra- Parts per tions. [Reserved] Commodity million (d) Indirect or inadvertent residues. Barley, grain ...... 0 .5 [Reserved] Barley, hay ...... 12 .0 Barley, hay ...... 20 .0 [63 FR 17706, Apr. 10, 1998, as amended at 64 Barley, straw ...... 12 .0 FR 18351, Apr. 14, 1999; 64 FR 35037, June 30, Cattle, fat ...... 0.1 1999; 65 FR 36792, June 12, 2000; 65 FR 82291, Cattle, kidney ...... 1 .5 Dec. 28, 2000; 66 FR 33486, June 22, 2001; 66 FR Cattle, meat ...... 0 .1 64775, Dec. 14, 2001; 67 FR 35050, May 17, 2002; Cattle, meat byproducts ...... 0.1 68 FR 5847, Feb. 5, 2003;68 FR 54817, Sept. 19, Corn, field, forage ...... 1 .0 2003; 68 FR 75442, Dec. 31, 2003; 69 FR 61604, Corn, field, grain ...... 0 .02 Corn, field, stover ...... 0 .5 Oct. 20, 2004; 70 FR 7047, Feb. 10, 2005; 70 FR Corn, sweet, forage ...... 1 .0 37688, June 30, 2005] Corn, sweet, kernel plus cob with husks re- moved ...... 0 .02 § 180.533 Esfenvalerate; tolerances for Corn, sweet, stover ...... 2 .0 residues. Garlic, bulb ...... 0.03 Goat, fat ...... 0 .1 (a) General. Tolerances are estab- Goat, kidney ...... 1 .5 lished for residues of the insecticide Goat, meat ...... 0.1 esfenvalerate, ((S)-cyano-(3- Goat, meat byproducts ...... 0 .1 Grain, aspirated fractions ...... 0 .6 phenoxyphenyl) methyl (S)-4-chloro-a- Grass, forage ...... 120 (1-methylethyl) benzeneacetate in or Grass, hay ...... 160 on the following raw agricultural com- Hog, fat ...... 0 .1 modities: Hog, kidney ...... 1.5 Hog, meat ...... 0 .1 Hog, meat byproducts ...... 0 .1 Parts per Commodity million Horse, fat ...... 0 .1 Horse, kidney ...... 1 .5 Artichoke, globe ...... 1.0 Horse, meat ...... 0 .1 Beet, sugar, dried pulp ...... 2 .5 Horse, meat byproducts ...... 0 .1 Beet, sugar, roots ...... 0 .5 Milk ...... 0.3 Beet, sugar, tops ...... 5.0 Oat, forage ...... 12 .0 Egg ...... 0 .03 Oat, grain ...... 0 .5 Kiwifruit ...... 0.5 Oat, hay ...... 20.0 Kohlrabi ...... 2 .0 Oat, straw ...... 12.0 Lettuce, head ...... 5.0 Onion, bulb ...... 0 .03 Mustard greens ...... 5.0 Shallot, bulb ...... 0 .03 Poultry, fat ...... 0.3 Sheep, fat ...... 0 .1 Poultry, meat ...... 0 .03 Sheep, kidney ...... 1.5 Poultry, meat byproducts, except liver ...... 0 .3 Sheep, meat ...... 0.1 Poultry, liver ...... 0 .03 Sheep, meat byproducts ...... 0 .1 Sorghum, forage ...... 10 .0 Sorghum, grain, forage ...... 2.0 Sorghum, grain ...... 5 .0 Sorghum, grain, grain ...... 0 .02 Sorghum, grain, stover ...... 10 .0 Sorghum, grain, stover ...... 4 .0 Wheat, forage ...... 12.0 (b) Section 18 emergency exemptions. Wheat, grain ...... 0 .5 [Reserved] Wheat, hay ...... 20 .0 Wheat, straw ...... 12 .0 (c) Tolerances with regional registra- tions. [Reserved] (b) Section 18 emergency exemptions. (d) Indirect or inadvertent residues. Time-limited tolerances are estab- [Reserved] lished for the combined residues of [63 FR 23401, Apr. 29, 1998, as amended at 63 fluroxypyr 1-methylheptyl ester and its FR 48615, Sept. 11, 1998] metabolite fluroxypyr, in connection with use of the pesticide under section § 180.535 Fluroxypyr 1-methylheptyl 18 emergency exemptions granted by ester; tolerances for residues. EPA. The tolerances will expire and (a) General. Tolerances are estab- are revoked on the dates specified in lished for combined residues of the following table.

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pound, in or on the following raw agri- Parts per Expiration/ Commodity Revocation cultural commodities: million Date

Corn, field, forage ...... 2.0 12/31/06 Parts per Commodity million Corn, field, grain ...... 0.05 12/31/06 Corn, field, stover ...... 2.5 12/31/06 Corn, field, forage ...... 1 .0 Corn, sweet, forage ...... 2.0 12/31/06 Corn, field, grain ...... 0 .20 Corn, sweet, kernel plus cob with Corn, field, stover ...... 0 .50 husks removed ...... 0.05 12/31/06 Corn, sweet, stover ...... 2.5 12/31/06 Onion ...... 0.02 6/30/07 (2) Tolerances are established for Sorghum, grain, forage ...... 2.0 12/31/05 combined residues of the herbicide Sorghum, grain, grain ...... 0.035 12/31/05 Sorghum, grain, stover ...... 4.0 12/31/05 isoxaflutole [5-cyclopropyl-4-(2- methylsulfonyl-4-trifluoromethyl ben- (c) Tolerances with regional registra- zoyl) isoxazole] and its metabolite 1-(2- tions. [Reserved] methylsulfonyl-4- (d) Indirect or inadvertent residues. trifluoromethylphenyl)-2-cyano-3- [Reserved] cyclopropyl propan-1,3-dione (RPA 202248), calculated as the parent com- [63 FR 52169, Sept. 30, 1998, as amended at 64 pound, in or on the following raw agri- FR 22799, Apr. 28, 1999; 66 FR 37598, July 19, cultural commodities: 2001; 66 FR 47971, Sept. 17, 2001; 67 FR 46884, July 17, 2002; 67 FR 60146, Sept. 25, 2002; 68 FR Parts per 75438, Dec. 31, 2003; 69 FR 2074, Jan. 14, 2004; Commodity million 70 FR 3649, Jan. 26, 2005; 70 FR 7047, Feb. 10, 2005; 71 FR 76204, Dec. 20, 2006] Cattle, fat ...... 0.20 Cattle, liver ...... 0 .50 Cattle, meat ...... 0 .20 § 180.536 Triazamate; tolerances for Cattle, meat byproducts, except liver ...... 0 .10 residues. Egg ...... 0 .01 (a) General. Time-limited tolerances Goat, fat ...... 0 .20 Goat, liver ...... 0.50 are established for the combined resi- Goat, meat ...... 0.20 dues of triazamate (RH-7988) ethyl(3- Goat, meat byproducts, except liver ...... 0 .10 tert-butyl-1-dimethylcarbamoyl-1H- Hog, fat ...... 0 .20 Hog, liver ...... 0 .50 1,2,4-triazol-5-ylthio)acetate and its Hog, meat ...... 0 .20 metabolite (RH0422) in or on the fol- Hog, meat byproducts, except liver ...... 0 .10 lowing commoditie(s): Horse, fat ...... 0 .20 Horse, liver ...... 0 .50 Expiration/ Horse, meat ...... 0 .20 Parts per Horse, meat byproducts, except liver ...... 0 .10 Commodity million Revocation Date Milk ...... 0.02 Poultry, fat ...... 0.20 Apple ...... 0.1 12/31/01 Poultry, liver ...... 0 .30 Poultry, meat ...... 0 .20 (b) Section 18 emergency exemptions. Sheep, fat ...... 0 .20 Sheep, liver ...... 0.50 (c) Tolerances with regional registra- Sheep, meat ...... 0.20 tions. [Reserved] Sheep, meat byproducts, except liver ...... 0 .10 (d) Indirect or inadvertent residues. [Reserved] (b) Section 18 emergency exemptions. [Reserved] [63 FR 71026, Dec. 23, 1998] (c) Tolerances with regional registra- § 180.537 Isoxaflutole; tolerances for tions. [Reserved] residues. (d) Indirect or inadvertent residues. [Reserved] (a) General. (1) Tolerances are estab- lished for combined residues of the her- [63 FR 50784, Sept. 23, 1998] bicide isoxaflutole [5-cyclopropyl-4-(2- methylsulfonyl-4-trifluoromethyl ben- § 180.538 Copper; tolerances for resi- zoyl) isoxazole] and its metabolites 1- dues. (2-methylsulfonyl-4- (a) General. A tolerance of 1 part per trifluoromethylphenyl)-2-cyano-3- million is established in water, potable cyclopropyl propan-1,3-dione (RPA for residues of copper resulting from 202248) and 2-methylsulphonyl-4- the use of the algicides or herbicides trifluoromethyl benzoic acid (RPA basic copper carbonate (malachite), 203328), calculated as the parent com- copper sulfate, copper

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monoethanolamine, and copper tri- § 180.541 Propetamphos; tolerances for ethanolamine to control aquatic plants residues. in reservoirs, lakes, ponds, irrigation (a) A tolerance of 0.1 part per million ditches, and other potential sources of is established for residues of the insec- potable water. ticide propetamphos ([(e)-]- (b) Section 18 emergency exemptions. methylethyl 3-[[(ethylamino) [Reserved] methoxyphosphinothioyl]oxy]-2- (c) Tolerances with regional registra- tions. [Reserved] butenoate]) in food commodities ex- (d) Indirect or inadvertent residues. posed to the insecticide during treat- [Reserved] ment of food- or feed-handling estab- lishments. [71 FR 74819, Dec. 13, 2006] (1) Direct application shall be limited solely to spot and/or crack and crevice § 180.539 d-Limonene; tolerances for residues. treatment in food-handling establish- ments where food and food products are (a) General. (1) The insecticide d-lim- held, processed, prepared, or served. onene may be safely used in insect-re- Spray and dust concentrations shall be pellent tablecloths and in insect-repel- limited to a maximum of 1 percent ac- lent strips used in food- or feed-han- tive ingredient. For crack and crevice dling establishments. treatment, equipment capable of deliv- (2) To assure safe use of the insect re- ering a dust or a pin-stream of spray pellent, its label and labeling shall con- form to that registered by the U.S. En- directly into cracks and crevices shall vironmental Protection Agency, and it be used. For spot treatment, a coarse, shall be used in accordance with such low-pressure spray shall be used to label and labeling. avoid contamination of food or food- (b) Section 18 emergency exemptions. contact surfaces. [Reserved] (2) Direct application shall be limited (c) Tolerances with regional registra- solely to spot and/or crack and crevice tions. [Reserved] treatment in feed-handling establish- (d) Indirect or inadvertent residues. ments where feed and feed products are [Reserved] held, processed, prepared, or sold. Spray and dust concentrations shall be [65 FR 33715, May 24, 2000, as amended at 70 FR 55268, Sept. 21, 2005] limited to a maximum of 1 percent ac- tive ingredient. For crack and crevice § 180.540 Fenitrothion; tolerances for treatment, equipment capable of deliv- residues. ering a dust or a pinstream of spray di- (a) General. A tolerance of 30 parts rectly into cracks and crevices shall be per million, of which no more than 15 used. For spot treatment, a coarse, parts per million is O,O-dimethyl O-(4- low-pressure spray shall be used to nitro-m-tolyl) phosphorothioate or avoid contamination of feed or feed- O,O-dimethyl O-(4-nitro-m-tolyl) phos- contact surfaces. phate, is established for combined resi- (3) To ensure safe use of the insecti- dues of the insecticide O,O-dimethyl O- cide, its label and labeling shall con- (4-nitro-m-tolyl) phosphorothioate and form to that registered by the U.S. En- its metabolites O,O-dimethyl O-(4- vironmental Protection Agency, and it nitro-m-tolyl) phosphate and 3-methyl- shall be used in accordance with such 4- in wheat gluten resulting label and labeling. from postharvest application of the in- (b) Section 18 emergency exemptions. secticide to stored wheat in Australia. [Reserved] (b) Section 18 emergency exemptions. (c) Tolerances with regional registra- [Reserved] tions. [Reserved] (c) Tolerances with regional registra- (d) Indirect or inadvertent residues. tions. [Reserved] [Reserved] (d) Indirect or inadvertent residues. [Reserved] [65 FR 33716, May 24, 2000] [65 FR 33716, May 24, 2000]

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§ 180.543 Diclosulam; tolerances for Commodity Parts per residues. million (a) General. Tolerances are estab- Leaf petioles subgroup ...... 25 lished for residues of the herbicide Leafy greens subgroup 4A ...... 30 Longan ...... 2 .0 diclosulam [N-(2,6-dichlorophenyl)-5- Lychee ...... 2 .0 ethoxy-7-fluoro[1,2,4] triazolo[1,5- Mango ...... 0.5 c]pyrimidine-2-sulfonamide] in or on Milk ...... 0.10 the following raw agricultural com- Nut, tree, group 14 ...... 0 .10 Okra ...... 2.0 modities as follows: Papaya ...... 0 .5 Pea and bean, succulent shelled, subgroup 6B 0 .2 Commodity Parts per Pea, blackeyed, seed ...... 4 .0 million Pea, southern, seed ...... 4.0 Peppermint ...... 7 .0 Peanut ...... 0 .020 Pistachio ...... 0.10 Soybean, seed ...... 0 .020 Plum, prune, fresh ...... 0.30 Poultry, fat ...... 0.02 (b) Section 18 emergency exemptions. Poultry, meat ...... 0 .02 [Reserved] Pulasan ...... 2 .0 (c) Tolerances with regional registra- Rambutan ...... 2 .0 Sapodilla ...... 0 .5 tions. [Reserved] Sapote, black ...... 0 .5 (d) Indirect or inadvertent residues. Sapote, mamey ...... 0 .5 [Reserved] Sheep, fat ...... 0 .50 Sheep, meat ...... 0.02 [65 FR 12134, Mar. 8, 2000] Soybean, aspirated grain fractions ...... 160 Soybean, forage ...... 30 § 180.544 Methoxyfenozide; tolerances Soybean, hay ...... 80 for residues. Soybean, hulls ...... 2 .0 Soybean, seed ...... 1 .0 (a) General. (1) Tolerances are estab- Spanish lime ...... 2 .0 lished for residues of the insecticide Spearmint ...... 7.0 Star apple ...... 0 .5 methoxyfenozide per se; benzoic acid, Strawberries ...... 1 .5 3-methoxy-2-methyl-, 2-(3,5- Turnip, greens ...... 30 dimethylbenzoyl)-2-(1,1-dimethylethyl) Vegetable, cucurbit, group 9 ...... 0.3 Vegetable, foliage of legume, (except soybean) hydrazide in or on the following food subgroup 7A ...... 35 commodities: Vegetable, fruiting, group 8 ...... 2.0 Vegetable, leaves of root and tuber, group 2 ..... 30 Commodity Parts per Vegetable, legume, edible podded, subgroup 6A 1 .5 million Vegetable, root, subgroup 1A ...... 0 .5 Almond, hulls ...... 25 Apple, wet pomace ...... 7 .0 (2) For combined residues of the in- Artichoke, globe ...... 3.0 secticide methoxyfenozide; benzoic Brassica, head and stem, subgroup 5A ...... 7 .0 acid, 3-methoxy-2-methyl-, 2-(3,5- Brassica, leafy greens, subgroup 5B ...... 30 Canistel ...... 0 .5 dimethylbenzoyl)-2-(1,1-dimethylethyl) Cattle, fat ...... 0.50 hydrazide and its glucuronide metabo- Cattle, meat ...... 0 .02 lite RH-141,518; b-D-Glucopyranuronic Coriander, leaves ...... 30 Corn, field, forage ...... 15 acid, 3-[2-(1,1-dimethylethyl)-2-(3,5- Corn, field, grain ...... 0 .05 dimethylbenzoyl)-hydrazino]carbonyl- Corn, field, refined oil ...... 0 .20 2-methylphenyl-] in the following com- Corn, field, stover ...... 125 Corn, sweet, forage ...... 30 modities: Corn, sweet, kernel plus cob with husks re- moved ...... 0 .05 Parts per Commodity million Corn, sweet, stover ...... 60 Cotton, gin byproducts ...... 35 Cattle, liver ...... 0 .40 Cotton, undelinted seed ...... 2 .0 Cattle, meat byproducts, except liver ...... 0 .10 Cranberry ...... 0 .5 Egg ...... 0 .02 Fruit, pome, group 11 ...... 1.5 Goat, liver ...... 0.40 Fruit, stone, group 12, except plum, prune, fresh 3 .0 Goat, meat byproducts, except liver ...... 0 .10 Goat, fat ...... 0 .50 Hog, liver ...... 0 .1 Goat, meat ...... 0.02 Hog, meat byproducts, except liver ...... 0 .02 Grain, aspirated fractions ...... 2 .0 Horse, liver ...... 0 .40 Grape ...... 1 .0 Horse, meat byproducts, except liver ...... 0 .10 Grape, raisin ...... 1 .5 Poultry, liver ...... 0 .10 Hog, fat ...... 0 .1 Poultry, meat byproducts, except liver ...... 0 .02 Hog, meat ...... 0 .02 Sheep, liver ...... 0.40 Horse, fat ...... 0 .50 Sheep, meat byproducts, except liver ...... 0 .10 Horse, meat ...... 0 .02

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(b) Section 18 emergency exemptions. methoxyfenozide to growing crops as Time-limited tolerances are estab- listed in paragraph (a) of this section: lished for the residues of the insecti- cide methoxyfenozide in connection Expiration/ Commodity Parts per Revocation with the use of the pesticide under sec- million Date tion 18 emergency exemption granted by EPA. The tolerances will expire on Animal feed, non-grass, group ...... 10.0 09/30/07 Grain, cereal, forage, fodder and the dates specified in the following ta- straw, group ...... 10.0 09/30/07 bles. Grass, forage, fodder and hay, group 17 ...... 10.0 09/30/07 Parts per Expiration/ Herb and spice, group ...... 10.0 09/30/07 Commodity million revocation Vegetable, legume, group 6 ...... 0.10 09/30/07 date Vegetable, foliage of legume, group Sorghum, grain ...... 0.05 12/31/07 7 ...... 10.0 09/30/07 Sorghum, grain, forage ...... 15 12/31/07 Sorghum, grain, stover ...... 125 12/31/07 Soybean, aspirated grain fractions 20 12/31/07 [67 FR 59203, Sept. 20, 2002, as amended at 68 Soybean, forage ...... 10 12/31/07 FR 32389, May 30, 2003; 68 FR 37765, June 25, Soybean, hay ...... 75 12/31/07 2003; 69 FR 58097, Sept. 29, 2004; 70 FR 7047, Soybean, refined oil ...... 1.0 12/31/07 Feb. 10, 2005; 70 FR 51604, Aug. 31, 2005; 70 FR Soybean, seed ...... 0.04 12/31/07 75739, Dec. 21, 2005; 71 FR 32853, June 7, 2006]

(c) Tolerances with regional registra- § 180.545 Prallethrin (RS)-2-methyl-4- tions. [Reserved] oxo-3-(2-propynyl)cyclopent-2-enyl (d) Indirect or inadvertent residues. (1) (1RS)-cis, trans-chrysanthemate; Tolerances are established for the indi- tolerances for residues. rect or inadvertent residues of the in- (a) General. (1) A tolerance of 1.0 ppm secticide methoxyfenozide per se; ben- is established for residues of the insec- zoic acid, 3-methoxy-2-methyl-, 2-(3,5- ticide prallethrin (RS)-2-methyl-4-oxo- dimethylbenzoyl)-2-(1,1-dimethylethyl) 3-(2-propynyl)cyclopent-2-enyl (1RS)- hydrazide in or on the following raw cis, trans-chrysanthemate as follows: agricultural commodities, when (2) In or on food commodities in food present therein as a result of the appli- handling establishments where food cation of methoxyfenozide to growing and food products are held, processed, crops as listed in paragraph (a) of this prepared and/or served. section: (3) Application shall be limited to space, general surface, and spot and/or Parts per Expiration/ Commodity Revocation crack and crevice treatment in food million Date handling establishments where food Vegetable, bulb, group 3 ...... 0.20 09/30/07 and food products are held, processed, Vegetable, root and tuber, group 1 0.10 09/30/07 prepared and/or served. General surface Vegetable, leaves of root and tuber, group 2 ...... 0.20 09/30/07 or space spray applications may be used only when the facility is not in (2) Tolerances are established for the operation provided exposed food has indirect or inadvertent combined resi- been covered or removed from the area dues of methoxyfenozide; benzoic acid, being treated prior to application. Spot 3-methoxy-2-methyl-, 2-(3,5- and/or crack and crevice application dimethylbenzoyl)-2-(1,1-dimethylethyl) may be used while the facility is in op- hydrazide and its metabolites RH- eration provided exposed food is cov- 117,236 free phenol of methoxyfenozide; ered or removed from the area being 3,5-dimethylbenzoic acid N-tert-butyl- treated prior to application. Spray con- N′-(3-hydroxy-2-methylbenzoyl) hydra- centrate shall be limited to a max- zide, RH-151,055 glucose conjugate of imum of 2.0% active ingredient. Con- RH-117,236; 3,5-dimethyl benzoic acid N- tamination of food or food contact sur- tert-butyl-N-[3 (b-D- faces shall be avoided. Food contact glucopyranosyloxy)-2-methylbenzoyl]- surfaces and equipment should be hydrazide and RH-152,072 the throughly washed with an effective malonylglycosyl conjugate of RH cleaning compound and rinsed with po- 117,236 in or on the following raw agri- table water after use of the product. cultural commodities, when present (4) To assure safe use of the additive, therein as a result of the application of its label and labeling shall conform to

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that registered with the U.S. Environ- or on the following raw agricultural mental Protection Agency, and it shall commodities: be used in accordance with such label and labeling. Parts per Commodity million (b) Section 18 emergency exemptions. [Reserved] Cattle, kidney ...... 0 .10 (c) Tolerances with regional registra- Cattle, meat byproducts, except kidney ...... 0.05 tions. [Reserved] Goat, kidney ...... 0 .10 (d) Indirect or inadvertent residues. Goat, meat byproducts, except kidney ...... 0 .05 1 [Reserved] Grass, forage ...... 0.10 Grass, hay1 ...... 0.10 [65 FR 39313, June 26, 2000, as amended at 71 Grass, seed screenings1 ...... 3 .5 FR 74819, Dec. 13, 2006] Grass, straw1 ...... 1 .2 Hog, kidney ...... 0.10 § 180.546 Mefenoxam; tolerances for Hog, meat byproducts, except kidney ...... 0 .05 residues. Horse, kidney ...... 0 .10 Horse, meat byproducts, except kidney ...... 0 .05 (a) General. Tolerances are estab- Peanut ...... 1 .0 lished for the combined residues of (R)- Peanut, hay ...... 0.60 and (S)-2-[(2,6-dimethyl(phenyl)- Fruit, pome, group 11 ...... 3.0 methoxyacetylamine]-propionic acid Sheep, kidney ...... 0.10 methyl ester, and its metabolites con- Sheep, meat byproducts, except kidney ...... 0 .05 taining the 2,6 dimethylaniline moiety, 1Registration is limited to grass grown for seed. and N-(2-hydroxy methyl-6- methylphenyl)-N-(methoxyacetyl)-ala- (b) Section 18 emergency exemptions. nine methyl ester, each expressed as [Reserved] mefenoxam equivalents, in or on the (c) Tolerances with regional registra- following food commodities: tions. [Reserved] (d) Indirect or inadvertent residues. Parts per [Reserved] Commodity million [65 FR 25660, May 3, 2000, as amended at 66 Artichoke, globe ...... 0.05 Atemoya ...... 0 .20 FR 29712, June 1, 2001] Canistel ...... 0 .40 Custard apple ...... 0 .20 § 180.548 Tralkoxydim; tolerances for Herbs, dried ...... 55 residues. Herbs, fresh ...... 8 .0 Kiwifruit ...... 0.10 (a) General. Tolerances are estab- Lingonberry ...... 2.0 Mango ...... 0.40 lished for residues of the herbicide, Papaya ...... 0 .40 tralkoxydim, 2-Cyclohexen-1-one, 2-[1- Sapodilla ...... 0 .40 (ethoxyimino)propyl]-3-hydroxy-5- Sapote, black ...... 0 .40 (2,4,6-trimethylphenyl)-(9Cl) in or on Sapote, mamey ...... 0 .40 Star apple ...... 0 .40 the raw agricultural commodities: Starfruit ...... 0 .20 Sugar apple ...... 0 .20 Parts per Commodity million (b) Section 18 emergency exemptions. Barley, grain ...... 0 .02 [Reserved] Barley, hay ...... 0 .02 (c) Tolerances with regional registra- Barley, straw ...... 0 .05 tions. [Reserved] Wheat, forage ...... 0 .05 (d) Indirect or inadvertant residues. Wheat, grain ...... 0 .02 [Reserved] Wheat, hay ...... 0 .02 Wheat, straw ...... 0 .05 [65 FR 57556, Sept. 25, 2000, as amended at 66 FR 48003, Sept. 17, 2001; 67 FR 35050, May 17, (b) Section 18 emergency exemptions. 2002] [Reserved] § 180.547 Prohexadione calcium; toler- (c) Tolerances with regional registra- ances for residues. tions. [Reserved] (a) General. Tolerances are estab- (d) Indirect or inadvertent residues. lished for residues of the plant growth [Reserved] regulator, prohexadione calcium (cal- [63 FR 69199, Dec. 16, 1998, as amended at 68 cium 3-oxido-5-oxo-4- FR 48302, Aug. 13, 2003; 70 FR 70739, Nov. 23, propionylcyclohex-3-enecarboxylate) in 2005]

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§ 180.549 Diflufenzopyr; tolerances for Expiration/ Commodity Parts per Revocation residues. million Date (a) General. Tolerances are estab- Sheep, kidney ...... 4.0 7/31/05 lished for combined residues of Sheep, meat ...... 0.60 7/31/05 diflufenzopyr, 2-(1-[([3,5- Sheep, meat byproducts, except difluorophenylamino]car- kidney ...... 0.50 7/31/05 bonyl)hydrazono]ethyl)-3- pyridinecarboxylic acid, and its me- (b) Section 18 emergency exemptions. tabolites convertible to 8- [Reserved] methylpyrido[2,3-d]pyridazin-5(6H)-one, (c) Tolerances with regional registra- expressed as diflufenzopyr, in or on the tions. [Reserved] following raw agricultural commod- (d) Indirect or inadvertent residues. ities: [Reserved] [64 FR 4308, Jan. 28, 1999, as amended at 67 Parts per Commodity million FR 55338, Aug. 29, 2002]

Corn, field, forage ...... 0 .05 § 180.550 Arsanilic acid [(4- Corn, field, grain ...... 0 .05 aminophenyl) arsonic acid]; toler- Corn, field, stover ...... 0 .05 ances for residues. Corn, pop, grain ...... 0.05 Corn, pop, stover ...... 0.05 (a) General. A time-limited tolerance Corn, sweet, forage ...... 0 .05 is established for residues of the plant Corn, sweet, kernel plus cob with husks re- moved ...... 0 .05 growth regulator arsanilic acid [(4- Corn, sweet, stover ...... 0 .05 aminophenyl) arsonic acid], in or on Grass, forage ...... 22 .0 the following food commodities in con- Grass, hay ...... 7 .0 nection with the use of the pesticide (2) Time-limited tolerances are estab- under section 5 experimental use per- lished for combined residues of mit. The tolerance will expire on the diflufenzopyr, 2-(1-[([3,5- date specified in the following table: difluorophenylamino]car- Parts per Expiration/ bonyl)hydrazono]ethyl)-3- Commodity million revocation pyridinecarboxylic acid, its metabo- date lites convertible to 8-methylpyrido[2,3- Grapefruit ...... 2 (not to 2/28/01 d]pyridazin- 5(6H)-one, and free and exceed 0.7 ppm acid-released 8- total hydroxymethylpyrido[2,3-d]pyridazine- arsenic) 2,5(1H,6H)-dione, expressed as diflufenzopyr, in or on the following (b) Section 18 emergency exemptions. raw agricultural commodities: [Reserved] (c) Tolerances with regional registra- Expiration/ Commodity Parts per Revocation tions. [Reserved] million Date (d) Indirect or inadvertent residues. [Reserved] Cattle, fat ...... 0.30 7/31/05 Cattle, kidney ...... 4.0 7/31/05 [64 FR 14639, Mar. 26, 1999] Cattle, meat ...... 0.60 7/31/05 Cattle, meat byproducts, except kid- ney ...... 0.50 7/31/05 § 180.551 Fluthiacet-methyl; tolerances Goat, fat ...... 0.30 7/31/05 for residues. Goat, kidney ...... 4.0 7/31/05 (a) General. (1) A tolerance is estab- Goat, meat ...... 0.60 7/31/05 Goat, meat byproducts, except kid- lished for residues of the herbicide, ney ...... 0.50 7/31/05 fluthiacet-methyl, acetic acid [[2- Hog, fat ...... 0.30 7/31/05 chloro-4-fluoro-5-[(tetrahydro-3-oxo- Hog, kidney ...... 4.0 7/31/05 Hog, meat ...... 0.60 7/31/05 1H,3H-[1,3,4]thiadiazolo[3,4-a]pyridazin- Hog, meat byproducts, except kid- 1-ylidene)amino]phenyl]thio]-methyl ney ...... 0.50 7/31/05 ester, in or on the food commodity: Horse, fat ...... 0.30 7/31/05 Horse, kidney ...... 4.0 7/31/05 Parts per Horse, meat ...... 0.60 7/31/05 Commodity million Horse, meat byproducts, except kid- ney ...... 0.50 7/31/05 Corn, field, forage ...... 0 .050 Milk ...... 3.0 7/31/05 Corn, field, grain ...... 0 .010 Sheep, fat ...... 0.30 7/31/05 Corn, field, stover ...... 0 .050

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Parts per Parts per Commodity million Commodity million

Corn, pop, grain ...... 0.010 Horse, fat ...... 0 .005 Corn, pop, stover ...... 0.050 Horse, meat ...... 0 .005 Corn, sweet, forage ...... 0 .050 Horse, meat byproducts ...... 0 .05 Corn, sweet, kernel plus cob with husks re- Milk ...... 0.006 moved ...... 0 .010 Sheep, fat ...... 0 .005 Corn, sweet, stover ...... 0 .050 Sheep, meat ...... 0.005 Soybean, seed ...... 0 .01 Sheep, meat byproducts ...... 0 .05 Wheat, forage ...... 4 .0 (2) A tolerance is established for the Wheat, grain ...... 0 .02 Wheat, hay ...... 0 .3 combined residues of the herbicide Wheat, straw ...... 0 .1 fluthiacet-methyland its acid metabo- lite: acetic acid, [[2-chloro-4-fluoro-5- (b) Section 18 emergency exemptions. [tetrahydro-3-oxo-1H,3H- Time-limited tolerances are estab- [1,3,4]thiadiazolo[3,4-a]pyridazin-1- lished for the combined residues of the ylidene)amino]phenyl]thio]-methyl herbicide sulfosulfuron, 1-(4,6- ester, and its acid metabolite, acetic dimethoxypyrimidin-2-yl)-3-[(2- acid, [[2-chloro-4-fluoro-5-[(tetrahydro- ethanesulfonyl-imidazo[1,2-a]pyridine- 3-oxo-1H,3H-[1,3,4]thiadiazolo[3,4- 3-yl)sulfonyl]urea and metabolites con- a]pyridazin-1- verted to 2-(ethylsulfonyl)-imidazo[1,2- ylidene)amino]phenyl]thio]- , in or on a]pyridine (calculated as sulfosulfuron) the following food commodities: in connection with use of the pesticide under section 18 emergency exemptions Parts per granted by EPA. The tolerances are Commodity million specified in the following table. The Cotton, gin byproducts ...... 0.20 tolerances will expire on the dates Cotton undelinted seed ...... 0.020 specified in the table. (b) Section 18 emergency exemptions. Parts per Expiration/ [Reserved] Commodity revocation million date (c) Tolerances with regional registra- tions. [Reserved] Bahiagrass, forage ...... 11 12/31/09 (d) Indirect or inadvertent residues. Bahiagrass, hay ...... 40 12/31/09 Bermudagrass, forage ...... 11 12/31/09 [Reserved] Bermudagrass, hay ...... 40 12/31/09 Cattle, fat ...... 0.04 12/31/09 [64 FR 18357, Apr. 14, 1999, as amended at 66 Cattle, meat ...... 0.02 12/31/09 FR 65850, Dec. 21, 2001; 71 FR 77625, Dec. 27, Cattle, meat byproducts ...... 0.50 12/31/09 2006] Goat, fat ...... 0.04 12/31/09 Goat, meat ...... 0.02 12/31/09 § 180.552 Sulfosulfuron; tolerances for Goat, meat byproducts ...... 0.50 12/31/09 Horse, fat ...... 0.04 12/31/09 residues. Horse, meat ...... 0.02 12/31/09 (a) General. Tolerances are estab- Horse, meat byproducts ...... 0.50 12/31/09 Milk ...... 0.02 12/31/09 lished for residues of the herbicide Sheep, fat ...... 0.04 12/31/09 sulfosulfuron, 1–(4,6- Sheep, meat ...... 0.02 12/31/09 dimethoxypyrimidin-2-yl)-3-[(2- Sheep, meat byproducts ...... 0.50 12/31/09 ethanesulfonyl-imidazo[1,2-a]pyridine- 3-yl) sulfonyl]urea and its metabolites (c) Tolerances with regional registra- converted to 2-(ethylsulfonyl)- tions. [Reserved] imidazo[1,2-a]pyridine and calculated (d) Indirect or inadvertent residues. as sulfosulfuron in or on the raw agri- [Reserved] cultural commodities. [64 FR 27192, May 19, 1999, as amended at 70 FR 69464, Nov. 16, 2005] Commodity Parts per million § 180.553 Fenhexamid; tolerances for Cattle, fat ...... 0.005 residues. Cattle, meat ...... 0 .005 Cattle, meat byproducts ...... 0.05 (a) General. Tolerances are estab- Goat, fat ...... 0 .005 lished for the residues of the fungicide Goat, meat ...... 0.005 fenhexamid (N-2,3-dichloro-4- Goat, meat byproducts ...... 0 .05 hydroxyphenyl)-1-methyl Hog, fat ...... 0 .005 Hog, meat ...... 0 .005 cyclohexanecarboxamide) in or on the Hog, meat byproducts ...... 0 .05 following commodities:

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(2) Tolerances are established in or Commodity Parts per million on the following commodities for the Almond, hulls ...... 2 .0 residues of the metabolite (E)-2-[2-(2- Almond ...... 0.02 methylphenoxy)methyl]-phenyl-2- Bushberry subgroup 13B ...... 5 .0 (methoxyimido)acetic acid resulting Caneberry subgroup 13A ...... 20 .0 Cilantro, leaves ...... 30.0 from the use of the fungicide kresoxim- Cucumber ...... 2 .0 methyl: Fruit, stone, group 12, except plum, prune, fresh, postharvest ...... 10.0 Parts per Ginseng ...... 0 .3 Commodity million Grape ...... 4 .0 Grape, raisin ...... 6 .0 Cattle, meat byproducts ...... 0.01 Juneberry ...... 5 .0 Goat, meat byproducts ...... 0 .01 Kiwifruit, postharvest ...... 15 .0 Sheep, meat byproducts ...... 0 .01 Leafy greens, subgroup 4A, except spinach ...... 30 .0 Lingonberry ...... 5.0 (b) Section 18 emergency exemptions. Pear ...... 10 Pepper, nonbell ...... 0 .02 [Reserved] Pistachio ...... 0.02 (c) Tolerances with regional registra- Plum, prune, dried ...... 2.5 tions. [Reserved] Plum, prune, fresh ...... 1.5 Pomegranate ...... 2 .0 (d) Indirect or inadvertent residues. Salal ...... 5 .0 [Reserved] Strawberry ...... 3 .0 Vegetable, fruiting, group 8, except nonbell pep- [64 FR 31136, June 10, 1999, as amended at 71 per ...... 2 .0 FR 50359, Aug. 25, 2006]

(b) Section 18 emergency exemptions. § 180.555 Trifloxystrobin; tolerances [Reserved] for residues. (c) Tolerances with regional registra- (a) General. Tolerances are estab- tions. [Reserved] lished for combined residues of (d) Indirect or inadvertent residues. trifloxystrobin (Benzeneacetic acid, [Reserved] (E,E)-a-(methoxyimino)-2-[[[[1-[3- [64 FR 28924, May 28, 1999, as amended at 65 (trifluoromethyl) FR 19849, Apr. 13, 2000; 65 FR 69883, Nov. 21, phenyl]ethylidene]amino]oxy]methyl]-, 2000; 67 FR 19120, Apr. 18, 2002; 68 FR 2247, methyl ester) and the free form of its Jan. 16, 2003; 68 FR 55519, Sept. 26, 2003; 71 FR acid metabolite CGA–321113 ((E,E)- 15617, Mar. 29, 2006; 71 FR 43664, Aug. 2, 2006] methoxyimino-[2-[1-(3-trifluoromethyl- phenyl)-ethylideneaminooxymethyl]- § 180.554 Kresoxim-methyl; tolerances phenyl]acetic acid in or on the fol- for residues. lowing commodities. (a) General. (1) Tolerances are estab- lished for the combined residues of the Commodity Parts per fungicide kresoxim-methyl (methyl million (E)-2-[2-(2-methylphenoxy)-meth- Almond, hulls ...... 3 .0 yl]phenyl-2-(methoxyimido)acetate) Almond ...... 0.04 Apple, wet pomace ...... 5 .0 and its metabolites as follows: (E)-2-[2- Banana1 ...... 0 .10 (2-methylphenoxy)methyl]-phenyl-2- Barley, grain ...... 0 .05 (methoxyimido)acetic acid; (E)-2-[2-(2- Barley, hay ...... 0 .3 Barley, straw ...... 5 .0 hydroxymethylphenoxy)methyl]- Beet, sugar, dried pulp ...... 0 .4 phenyl-2-(methoxyimido)acetic acid Beet, sugar, molasses ...... 0 .2 (free and glucose conjugated); and (E)- Beet, sugar, roots ...... 0 .1 Beet, sugar, tops ...... 4.0 2-[2-(4-hydroxy-2-methylphenoxy)- Cattle, fat ...... 0.05 methyl]phenyl-2-(methoxyimido)acetic Cattle, meat ...... 0 .05 acid (free and glucose conjugated) in or Cattle, meat byproducts ...... 0.05 Citrus, dried pulp ...... 0 .8 on the following commodities: Citrus, oil ...... 30 Corn, field, forage ...... 0 .2 Parts per Corn, field, grain ...... 0 .05 Commodity million Corn, field, stover ...... 7 Corn, field, refined oil ...... 0 .1 Apple, pomace ...... 1.0 Corn, pop, grain ...... 0.05 Fruit, pome ...... 0.5 Grape ...... 1 .0 Corn, pop, stover ...... 7 Grape, raisin ...... 1 .5 Corn, sweet, cannery waste ...... 0 .6 Pecans ...... 0 .15 Corn, sweet, forage ...... 0 .6 Vegetable, cucurbit, group 9 ...... 0.40 Corn, sweet, kernel plus cob with husks re- moved ...... 0 .04

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expire and are revoked on the date Commodity Parts per million specified in the table in this unit. Corn, sweet, stover ...... 0 .25 Egg ...... 0 .04 Expiration/ Commodity Parts per revocation Fruit, citrus, group 10 ...... 0 .3 million date Fruit, pome ...... 0.5 Fruit, stone, group 12 ...... 2 Soybean, forage ...... 4.0 12/31/09 Goat, fat ...... 0 .05 Soybean, hay ...... 6.5 12/31/09 Goat, meat ...... 0.05 Soybean, seed ...... 0.04 12/31/09 Goat, meat byproducts ...... 0 .05 Grain, aspirated fractions ...... 5 .0 Grape ...... 2 .0 (c) Tolerances with regional registra- Grape, raisin ...... 5 .0 tions. [Reserved] Hog, fat ...... 0 .05 Hog, meat, ...... 0 .05 (d) Indirect or inadvertent residues. Hog, meat byproducts ...... 0 .05 [Reserved] Hop, dried cones ...... 11 .0 Horse, fat ...... 0 .05 [64 FR 51907, Sept. 27, 1999, as amended at 65 Horse, meat ...... 0 .05 FR 44453, July 18, 2000; 67 FR 35924, May 22, Horse, meat byproducts ...... 0 .05 2002; 68 FR 53304, Sept. 10, 2003; 70 FR 36532, Leaf petioles subgroup 4B ...... 3 .5 June 24, 2005; 71 FR 15604, Mar. 29, 2006; 71 FR Milk ...... 0.02 Nut, tree, group 14 ...... 0 .04 55319, Sept. 22, 2006] Oat, forage ...... 0 .3 Oat, grain ...... 0 .05 § 180.556 Pymetrozine; tolerances for Oat, hay ...... 0.3 residues. Oat, straw ...... 5.0 Peanut, hay ...... 4.0 (a) General. Tolerances are estab- Peanut ...... 0 .05 lished for residues of the insecticide Pistachio ...... 0.04 Potato ...... 0 .04 pymetrozine 1,2,4-triazin-3(2H)-one,4,5- Poultry, fat ...... 0.04 dihydro-6-methyl-4-[(3- Poultry, meat ...... 0 .04 pyridinylmethylene) amino] in or on Poultry, meat byproducts ...... 0.04 Rice, grain ...... 3 .5 the following raw agricultural com- Rice, hulls ...... 8 modities. The tolerance level for each Rice, straw ...... 7 .5 commodity is expressed in terms of the Sheep, fat ...... 0 .05 parent insecticide only, which serves as Sheep, meat ...... 0.05 Sheep, meat byproducts ...... 0 .05 an indicator of the use of pymetrozine Soybean, forage ...... 10 .0 on these raw agricultural commodities. Soybean, hay ...... 25 .0 Soybean, seed ...... 0 .08 Parts per Vegetable, cucurbit, group 9 ...... 0.50 Commodity million Vegetable, fruiting ...... 0.5 Vegetable, root, except sugar beet, subgroup Asparagus ...... 0.04 1B, except radish ...... 0 .10 Brassica, head and stem, subgroup 5A ...... 0 .5 Wheat, bran ...... 0.15 Brassica, leafy greens, subgroup 5B ...... 0 .25 Wheat, forage ...... 0 .3 Cotton, gin byproducts ...... 2 .0 Wheat, grain ...... 0 .05 Wheat, hay ...... 0 .2 Cotton, undelinted seed ...... 0 .3 Wheat, straw ...... 5 .0 Hop, dried cones ...... 6 .0 Pecan ...... 0 .02 1 There are no U.S. registrations as of September 27, 1999 Turnip, greens ...... 0.25 for use on banana. Vegetable, fruiting, group 8 ...... 0.2 (b) Section 18 emergency exemptions. Vegetable, cucurbit, group 9 ...... 0.1 Time-limited tolerances are estab- Vegetable, leafy, execpt brassica, group (Crop lished for combined residues of the fun- Group 4) ...... 0 .6 gicide trifloxystrobin, (benzeneacetic Vegetable, tuberous and corm, subgroup 1C ..... 0.02 acid, (E,E)-[alpha]-(methoxyimino)-2- (b) Section 18 emergency exemptions. [[[[1-[3-(trifluoromethyl)phenyl]ethyl- [Reserved] idene]amino]oxy]methyl]-,methylester) and the free form of its acid metabolite (c) Tolerances with regional registra- CGA–321113 ((E,E)-methoxyimino-[2-[1- tions. [Reserved] (3-trifluoromethylphenyl) (d) Indirect or inadvertent residues. ethylideneaminooxymethyl]- [Reserved] phenyl]acetic acid) in connection with [65 FR 48634, Aug. 9, 2000, as amended at 66 the use of the pesticide under FIFRA FR 14846, Mar. 14, 2001; 66 FR 66794, Dec. 27, section 18 emergency exemptions 2001; 70 FR 7047, Feb. 10, 2005; 70 FR 43298, granted by EPA. The tolerances will July 27, 2005]

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§ 180.557 Tetraconazole; tolerances for Commodity Parts per residues. million (a) General. Tolerances are estab- Orange, sweet ...... 0 .01 lished for residues of the fungicide, tetraconazole, 1-[2-(2,4-dichlorophenyl)- (b) Section 18 emergency exemptions. 3-(1,1,2,2-tetrafluoroethoxy)propyl]-1H- [Reserved] 1,2,4-triazole in or on the following (c) Tolerances with regional registra- commodities: tions. [Reserved] (d) Indirect or inadvertent residues. Parts per Commodity million [Reserved]

Aspirated grain fractions ...... 1 .0 [65 FR 1814, Jan. 12, 2000] Beet sugar, dried pulp ...... 0 .15 Beet sugar, molasses ...... 0 .15 § 180.559 Clodinafop-propargyl; toler- Beet sugar, root ...... 0 .05 ances for residues. Cattle, fat ...... 0.02 Cattle, liver ...... 0 .20 (a) General. Tolerances are estab- Cattle, meat ...... 0 .01 lished for combined residues of Cattle, meat byproducts (except liver) ...... 0 .01 Eggs ...... 0 .02 clodinafop-propargyl (propanoic acid, Goat, fat ...... 0 .02 2-[4-(5-chloro-3-fluoro-2- Goat, liver ...... 0.20 pyridinyl)oxy]phenoxy]-,2-propynyl Goat, meat ...... 0.01 Goat, meat byproducts (except liver) ...... 0.01 ester, (2R)-) and its acid metabolite Hog, fat ...... 0 .01 (propanoic acid, 2-[4-[(5-chloro-3-fluoro- Hog, liver ...... 0 .05 2-pyridinyl)oxy]phenoxy]-, (2R)-), in or Hog, meat ...... 0 .01 on wheat, grain at 0.1 ppm ; wheat, for- Hog, meat byproducts (except liver) ...... 0 .01 Horse, fat ...... 0 .02 age at 0.1 ppm; wheat, hay at 0.1 ppm; Horse, liver ...... 0 .20 and wheat, straw at 0.50 ppm. Horse, meat ...... 0 .01 Horse, meat byproducts (except liver) ...... 0 .01 Parts per Milk ...... 0.01 Commodity million Milk, fat ...... 0 .25 Peanut ...... 0 .03 Wheat, forage ...... 0 .1 Peanut, oil ...... 0 .10 Wheat, grain ...... 0 .1 Pecan ...... 0 .04 Wheat, hay ...... 0 .1 Poultry, fat ...... 0.05 Wheat, straw ...... 0 .5 Poultry, meat ...... 0 .01 Poultry meat byproducts ...... 0 .01 Sheep, fat ...... 0 .02 (b) Section 18 emergency exemptions. Sheep, liver ...... 0.20 [Reserved] Sheep, meat ...... 0.01 (c) Tolerances with regional registra- Sheep, meat byproducts (except liver) ...... 0.01 Soybean, refined oil ...... 0 .80 tions. [Reserved] Soybean, seed ...... 0 .15 (d) Indirect or inadvertent residues. [Reserved] (b) Section 18 emergency exemptions. [Reserved] [65 FR 38774, June 22, 2000] (c) Tolerances with regional registra- tions. [Reserved] § 180.560 Cloquintocet-mexyl; toler- (d) Indirect or inadvertent residues. ances for residues. [Reserved] (a) General. Tolerances are estab- lished for the combined residues of [70 FR 20830, Apr. 22, 2005, as amended at 70 FR 31359, June 1, 2005; 72 FR 18134, Apr. 11, cloquintocet-mexyl (acetic acid, [(5- 2007] chloro-8-quniolinyl)oxy]-, 1- methylhexyl ester)(CAS No. 99607–70–2) § 180.558 N,N-diethyl-2-(4-methylbenz- and its acid metabolite (5-chloro-8- yloxy)ethylamine hydrochloride; quinlinoxyacetic acid) when used as an tolerances for residues. inert ingredient (safener) in pesticide (a) General. A tolerance for residues formulations containing the active in- of the plant growth regulator N,N- gredients pinoxaden (wheat or barley) diethyl-2-(4- or clodinafop-propargyl (wheat only) in methylenzyloxy)ethylamine hydro- a 1:4 ratio of safener to active ingre- chloride in or on raw agricultural com- dient in or on the following food com- modities is established as follows: modities:

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Commodity Parts per § 180.562 Flucarbazone-sodium; toler- million ances for residues. Barley, grain ...... 0 .1 (a) General. Tolerances are estab- Barley, hay ...... 0 .1 Barley, straw ...... 0 .1 lished for combined residues of the her- Wheat, forage ...... 0 .1 bicide flucarbazone-sodium, 4,5- Wheat, grain ...... 0 .1 dihydro-3-methoxy-4-methyl-5-oxo-N- Wheat, hay ...... 0 .1 Wheat, straw ...... 0 .1 [[2(trifluoromethoxy)phenyl] sulfonyl]- 1H-1,2,4-triazole 1-carboxamide, sodium (b) Section 18 emergency exemptions. salt) and its N-desmethyl metabolite; [Reserved] and its metabolites converted to 2- (c) Tolerances with regional registra- (trifluoromethoxy)benzene sulfonamide tions. [Reserved] and calculated as flucarbazone-sodium (d) Indirect or inadvertent residues. in or on the following food commod- [Reserved] ities: [65 FR 38764, June 22, 2000, as amended at 70 Commodity Parts per FR 74688, Dec. 16, 2005] million

§ 180.561 Acibenzolar-S-methyl; toler- Cattle, liver ...... 1.50 ances for residues. Cattle, meat ...... 0.01 Cattle, meat byproducts except liver ...... 0.01 (a) General. Tolerances are estab- Goat, liver ...... 1.50 lished for residues of acibenzolar-S- Goat, meat ...... 0.01 methyl, benzo(1,2,3)thiadiazole-7- Goat, meat byproducts except liver ...... 0.01 Hog, liver ...... 1.50 carbothioic acid-S-methyl ester, in or Hog, meat ...... 0.01 on the following raw agricultural com- Hog, meat byproducts except liver ...... 0.01 modities: Horse, liver ...... 1.50 Horse, meat ...... 0.01 Horse, meat by-products except liver ...... 0.01 Commodity Parts per million Milk ...... 0.005 Sheep, liver ...... 1.50 Banana1 ...... 0 .1 Sheep, meat ...... 0.01 Spinach ...... 1 .0 Sheep, meat byproducts except liver ...... 0.01 Tomato, paste ...... 3 .0 Wheat, forage ...... 0.30 Vegetable, brassica, leafy, group 5 ...... 1.0 Wheat, grain ...... 0.01 Vegetable, fruiting ...... 1.0 Vegetable, leafy ...... 0 .25 Wheat, hay ...... 0.10 Wheat, straw ...... 0.05 1 There are no United States registrations for banana. (b) Section 18 emergency exemptions. (b) Section 18 emergency exemptions. Time-limited tolerances are estab- [Reserved] lished for residues of acibenzolar-S- (c) Tolerances with regional registra- methyl, benzo(1,2,3)thiadiazole-7- tions. [Reserved] carbothioic acid-S-methyl ester in con- (d) Indirect or inadvertant residues. nection with use of the pesticide under [Reserved] section 18 emergency exemptions [70 FR 67915, Nov. 9, 2005, as amended at 71 granted by EPA. The time-limited tol- FR 76931, Dec. 22, 2006] erances will expire and are revoked on the date specified in the following § 180.563 Ethametsulfuron-methyl; tol- table: erances for residues. (a) General. A tolerance is established Parts per Expiration/ Commodity million revocation for residues of ethametsulfuron methyl date (methyl 2- ((((4-ethoxy-6- Onion, dry bulb ...... 0.05 12/31/09 (methylamino)-1,3,5- triazin-2-yl) Onion, green ...... 0.05 12/31/09 amino) carbonyl) amino) sulfonyl) ben- zoate) in or on the following raw agri- (c)Tolerances with regional registra- cultural commodities. tions. [Reserved] (d)Indirect or inadvertent residues. [Re- Commodity Parts per served] million [65 FR 50446, Aug. 18, 2000, as amended at 70 Canola, seed ...... 0 .02 FR 7861, Feb. 16, 2005; 71 FR 76200, Dec. 20, Crambe, seed ...... 0.02 2006] Rapeseed, seed ...... 0 .02

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(b) Section 18 emergency exemptions. Commodity Parts per [Reserved] million (c) Tolerances with regional registra- Vegetable, fruiting, group 8 ...... 0.50 tions. [Reserved] (d) Indirect of inadvertent residues. (2) Time-limited tolerances are estab- [Reserved] lished for combined residues of [65 FR 57972, Sept. 27, 2000, as amended at 66 indoxacarb, (S)-methyl 7-chloro-2,5- FR 18207, Apr. 6, 2001; 67 FR 35050, May 17, dihydro-2-[[(methoxycarbonyl) [4- 2002] (trifluoromethoxy) phenyl]amino] car- bonyl] indeno[1,2-e][1,3,4]oxadiazine- § 180.564 Indoxacarb; tolerances for 4a(3H)-carboxylate, and its R- residues. enantiomer, (R)-methyl 7-chloro- 2,5- (a) General. (1) Tolerances are estab- dihydro-2- [[(methoxycarbonyl)[4- lished for the combined residues of the (trifluoromethoxy) phenyl]amino] car- insecticide indoxacarb, (S)-methyl 7- bonyl]indeno[1,2-e] [1,3,4]oxadiazine- chloro-2,5-dihydro-2-[[(methoxycar- 4a(3H)- carboxylate, in connection with bonyl)[4-(trifluoromethoxy)phenyl] use of the pesticide under FIFRA sec- amino]carbonyl]indeno[1,2- tion 5 experimental use permit granted e][1,3,4]oxadiazine-4a(3H)-carboxylate, by EPA. The tolerances are specified in and its R-enantimomer, (R)-methyl 7- the following table, and will expire and chloro-2,5-dihydro-2-[[(methoxycar- are revoked on the dates specified. bonyl)[4- (trifluoromethoxy)phenyl]amino] car- Expiration/ Commodity Parts per revocation bonyl]indeno[1,2-e][1,3,4]oxadiazine- million date 4a(3H)-carboxylate, in or on the fol- lowing raw agricultural commodities: Cherry, sweet ...... 1.0 May 21, 2007 Parts per Cherry, tart ...... 1.0 May 21, Commodity million 2007 Peach ...... 10 May 15, Apple ...... 1.0 2006 Apple, wet pomace ...... 3 .0 Brassica, head and stem, subgroup 5A ...... 5 .0 Alfalfa, forage ...... 10 (b) Time-limited tolerances are es- Alfalfa, hay ...... 50 tablished for the residues of Cattle, fat ...... 1.5 indoxacarb, (S)-methyl 7-chloro-2,5- Cattle, meat ...... 0 .05 dihydro-2-[[(methoxycarbonyl)[4- Cattle, meat byproducts ...... 0.03 Corn, sweet, forage ...... 10 (trifluoromethoxy)phenyl] Corn, sweet, kernel plus cob with husk removed 0.02 amino]carbonyl]indeno [1,2- Corn, sweet, stover ...... 15 e][1,3,4]oxadiazine-4a(3H)-carboxylate, Cotton, gin byproducts ...... 15 and its R-enantiomer, (R)-methyl 7- Cotton, undelinted seed ...... 2 .0 Goat, fat ...... 1 .5 chloro-2,5-dihydro-2-[[(methoxycar- Goat, meat ...... 0.05 bonyl)[4-(trifluoromethoxy)phenyl] Goat, meat byproducts ...... 0 .03 amino]carbonyl]indeno[1,2- Hog, fat ...... 1 .5 Hog, meat ...... 0 .05 e][1,3,4]oxadiazine-4a(3H)-carboxylate, Hog, meat byproducts ...... 0 .03 in connection with use of the pesticide Horse, fat ...... 1 .5 under section 18 emergency exemptions Horse, meat ...... 0 .05 granted by EPA. The tolerances are Horse, meat byproducts ...... 0 .03 Lettuce, head ...... 5.0 specified in the following table, and Lettuce, leaf ...... 10 will expire and are revoked on the Milk ...... 0.15 dates specified. Milk, fat ...... 4 .0 Pear ...... 0 .20 Expiration/ Peanut ...... 0 .01 Commodity Parts per revocation Peanut, hay ...... 40 million date Potato ...... 0 .01 Sheep, fat ...... 1 .5 Collards ...... 3.0 06/30/06 Sheep, meat ...... 0.05 Cranberry ...... 0.50 12/31/07 Sheep, meat byproducts ...... 0 .03 Soybean, aspirated grain fractions ...... 45 Soybean, hulls ...... 4 .0 (c) Tolerances with regional registra- Soybean, seed ...... 0 .80 tions. [Reserved]

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(d) Indirect or inadvertent residues. Commodity Parts per [Reserved] million [65 FR 58424, Sept. 29, 2000, as amended at 67 Potato ...... 0.25 FR 41807, June 19, 2002; 67 FR 47309, July 18, Radish, tops ...... 0.80 Rapeseed, seed ...... 0.02 2002; 67 FR 58730, Sept. 18, 2002; 68 FR 25830, Safflower, seed ...... 0.02 May 14, 2003; 68 FR 27746, May 21, 2003; 69 FR Salal ...... 0.20 28842, May 19, 2004; 69 FR 29459, May 24, 2004; Sheep, meat byproducts ...... 0.02 69 FR 32282, June 9, 2004] Sheep, meat ...... 0.02 Sorghum, forage ...... 0.02 Sorghum, grain ...... 0.02 § 180.565 Thiamethoxam; tolerances Sorghum, grain, stover ...... 0.02 for residues. Spearmint ...... 1.5 (a) General. A tolerance is established Strawberry ...... 0.3 Sunflower ...... 0.02 for the combined residues of the insec- Tomato, paste ...... 0.80 ticide thiamethoxam [3-[(2-chloro-5- Vegetable, cucurbit, group 9 ...... 0.2 thiazolyl)methyl]tetrahydro-5-methyl- Vegetable, fruiting, group 8 ...... 0.25 Vegetable, leafy, except brassica, group 4 ...... 4.0 N-nitro-4H-1,3,5-oxadiazin-4-imine] Vegetable, legume, group 6 ...... 0.02 (CAS Reg. No. 153719–23–4) and its me- Vegetable, root, except sugar beet, subgroup tabolite [N-(2-chloro-thiazol-5- 1B ...... 0.02 ylmethyl)-N′-methyl-N′-nitro-guani- Vegetable, tuberous and corm, except potato, subgroup 1D ...... 0.02 dine] in or on the following raw agri- Wheat, forage ...... 0.50 cultural commodities: Wheat, grain ...... 0.02 Wheat, hay ...... 0.02 Parts per Wheat, straw ...... 0.02 Commodity million 1There are no U.S. registrations as of September 17, 2003. Artichoke, globe ...... 0.45 Barley, grain ...... 0.30 (b) Section 18 emergency exemptions. Barley, hay ...... 0.40 Time-limited tolerances are estab- Barley, straw ...... 0.40 lished for the combined residues of the Bean, succulent ...... 0.02 insecticide thiamethoxam [3-[(2-chloro- Borage, seed ...... 0.02 Brassica, head and stem, subgroup 5-A ...... 4.5 5-thiazolyl)methyl]tetrahydro-5-meth- Brassica, leafy greens, subgroup 5-B ...... 3.0 yl-N-nitro-4H-1,3,5-oxadiazin-4-imine] Bushberry, subgroup 13B ...... 0.20 and its metabolite CGA-322704 in con- Caneberry subgroup 13-A ...... 0.35 Canola, seed ...... 0.02 nection with use of the pesticide under Cattle, meat byproducts ...... 0.02 section 18 emergency exemptions Cattle, meat ...... 0.02 granted by EPA. These tolerances will Coffee 1 ...... 0.05 Corn, field, forage ...... 0.10 expire and are revoked on the dates Corn, field, grain ...... 0.020 specified in the following table: Corn, field, stover ...... 0.05 Corn, pop, forage ...... 0.10 Parts per Expiration/ Corn, pop, grain ...... 0.02 Commodity million revocation Corn, pop, stover ...... 0.05 date Corn, sweet, forage ...... 0.10 Corn, sweet, kernel plus cob with husks re- Cranberry ...... 0.02 12/31/07 moved ...... 0.02 Corn, sweet, stover ...... 0.05 (c) Tolerances with regional registra- Cotton, gin byproducts ...... 1.5 tions. [Reserved] Cotton, undelinted seed ...... 0.10 Crambe, seed ...... 0.02 (d) Indirect or inadvertent residues. Cranberry ...... 0.02 [Reserved] Flax, seed ...... 0.02 Fruit, pome, group 11 ...... 0.2 [65 FR 79762, Dec. 20, 2000, as amended at 65 Fruit, stone, group 12 ...... 0.5 FR 80353, Dec. 21, 2000; 66 FR 28397, May 23, Goat, meat byproducts ...... 0.02 2001; 67 FR 35050, May 17, 2002; 67 FR 66571, Goat, meat ...... 0.02 Nov. 1, 2002; 68 FR 51479, Aug. 27, 2003; 68 FR Grape ...... 0.20 54394, Sept. 17, 2003; 69 FR 55512, Sept. 15, Grape, raisin ...... 0.30 Hog, meat byproducts ...... 0.02 2004; 70 FR 719, Jan. 5, 2005; 70 FR 7182, Feb. Hog, meat ...... 0.02 11, 2005; 72 FR 34409, June 22, 2007] Hop, dried cones ...... 0.10 Horse, meat byproducts ...... 0.02 § 180.566 Fenpyroximate; tolerances Horse, meat ...... 0.02 for residues. Juneberry ...... 0.20 Lingonberry ...... 0.20 (a) General. (1) Tolerances are estab- Milk ...... 0.02 lished for residues of the insecticide Mustard, seed ...... 0.02 Pecan ...... 0.02 fenpyroximate, (E)-1,1-dimethylethyl 4- Peppermint ...... 1.5 [[[[(1,3-dimethyl- 5-phenoxy-1H-

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pyrazol-4-yl) methylene] ylene aminooxymethyl]benzoic acid, amino]oxy]methyl] benzoate and its calculated as the parent compound in Z-isomer, (Z)-1,1-dimethylethyl 4- the following commodities: [[[[(1,3-dimethyl-5- phenoxy-1H- Parts per pyrazol-4-yl)methylene] amino]oxy] Commodity million methyl]benzoate in or on the following commodities: Cattle, kidney ...... 0 .25 Cattle, liver ...... 0 .25 Goat, kidney ...... 0 .25 Commodity Parts per million Goat, liver ...... 0.25 Horse, kidney ...... 0 .25 Almond, hulls ...... 3.0 Horse, liver ...... 0 .25 Citrus, dried pulp ...... 2.5 Sheep, kidney ...... 0.25 Citrus, oil ...... 10 Sheep, liver ...... 0.25 Cotton, gin byproducts ...... 10 Cotton undelinted seed ...... 0.10 Fruit, citrus, group 10 ...... 0.60 (b) Section 18 emergency exemptions. Fruit, pome, group 11 ...... 0.40 Time-limited tolerance is established Grape ...... 1.0 Hop, dried cones ...... 10 for the combined residues of Nut, tree, group 14 ...... 0.10 fenpyroximate, (E)-1,1-dimethylethyl 4- Peppermint, tops ...... 7.0 [[[(E)-[(1,3-dimethyl-5-phenoxy-1H- Pistachio ...... 0.10 pyrazol-4-yl) methylene] amino]oxy] Spearmint, tops ...... 7.0 methyl]benzoate in or on honey at 0.10 (2) Tolerances are established for res- ppm. This tolerance expires and is re- idues of the insecticide fenpyroximate, voked on the date specified in the fol- (E)-1,1-dimethylethyl 4-[[[[(1,3-di- lowing table. methyl-5 -phenoxy-1H-pyrazol-4-yl) Expiration/revoca- methylene] amino]oxy]methyl] ben- Commodity Parts per million tion date zoate and its metabolites, (E)-4- [(1,3- dimethyl-5- phenoxypyrazol-4-yl)- Honey ...... 0.10 12/31/10 methylene aminooxymethyl]benzoic (c) Tolerances with regional registra- acid and (E)-1,1-dimethylethyl-2-hy- tions. [Reserved] droxyethyl 4- [[[[(1,3-dimethyl -5- (d) Indirect or inadvertent residues. phenoxy-1H-pyrazol-4-yl) meth- [Reserved] ylene]amino]oxy]methyl] benzoate, calculated as the parent compound in [66 FR 18568, Apr. 10, 2001, as amended at 69 or on the following commodities: FR 32464, June 10, 2004; 71 FR 49368, Aug. 23, 2006; 72 FR 26321, May 9, 2007] Commodity Parts per million § 180.567 Zoxamide; tolerances for resi- Cattle, fat ...... 0.03 dues. Cattle, meat ...... 0.03 (a) General. (1) Tolerances are estab- Cattle, meat byproducts (excluding liver and kidney) ...... 0.03 lished for residues of zoxamide (3,5- Goat, fat ...... 0.03 dichloro-N-(3-chloro-1-ethyl-1-methyl- Goat, meat ...... 0.03 2-oxopropyl)-4-methylbenzamide) in or Goat, meat byproducts (excluding liver and kid- ney ...... 0.03 on the following commodities: Horse, fat ...... 0.03 Horse, meat ...... 0.03 Parts per Commodity million Horse, meat byproducts (excluding liver and kidney) ...... 0.03 Grape ...... 3 .0 Milk ...... 0.015 Grape, raisin ...... 15.0 Sheep, fat ...... 0.03 Sheep, meat ...... 0.03 Tomato ...... 2.0 Sheep, meat byproducts (excluding liver and Vegetable, cucurbit, group 9 ...... 1.0 kidney ...... 0.03 (2) Tolerances are established for the (3) Tolerances are established for res- combined residues of zoxamide and its idues of the insecticide fenpyroximate, metabolites 3,5-dichloro-1,4- (E)-1,1-dimethylethyl 4- [[[[(1,3-di- benzenedicarboxylic acid (RH–1455 and methyl-5-phenoxy-1H-pyrazol-4-yl) RH–141455) and 3,5-dichloro-4- methylene]amino]oxy]methyl] ben- hydroxymethylbenzoic acid (RH–1452 zoate and its metabolite, (E)-4-[(1,3-di- and RH–141452) in or on the following methyl-5-phenoxypyrazol-4-yl)-meth- commodities:

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lished for residues of the herbicide Commodity Parts per million flumioxazin in connection with the use Potato, tuber ...... 0 .060 of the pesticides under section 18 emer- Potato, granule/flakes ...... 0 .30 gency exemptions granted by EPA. The Potato, wet peel ...... 0 .10 tolerances will expire and are revoked (b) Section 18 emergency exemptions. A on the dates specified in the following time-limited tolerance is established table. for residues of the fungicide zoxamide Expiration/ (3,5-dichloro-N-(3-chloro-1-ethyl-1- Parts per Commodity million Revocation methyl-2-oxopropyl)-4- date methylbenzamide) in connection with Alfalfa, forage ...... 0.13 12/31/09 use of the pesticide under a section 18 Alfalfa, hay ...... 0.45 12/31/09 emergency exemption granted by EPA. The tolerance will expire and is re- (c) Tolerances with regional registra- voked on the date specified in the fol- tions. [Reserved] lowing table. (d) Indirect or inadvertent residues. Parts per Revocation [Reserved] Commodity million date [66 FR 19878, Apr. 18, 2001, as amended at 68 Ginseng ...... 0.06 12/31/09 FR 51471, Aug. 27, 2003; 69 FR 16831, Mar. 31, 2004; 69 FR 52198, Aug. 25, 2004; 71 FR 25956, (c) Tolerances with regional registra- May 3, 2006; 71 FR 61413, Oct. 18, 2006] tions. [Reserved] (d) Indirect or inadvertent residues. § 180.569 Forchlorfenuron; tolerances [Reserved] for residues. [66 FR 18733, Apr. 11, 2001, as amended at 66 (a) General. (1) Tolerances are estab- FR 49118, Sept. 26, 2001; 69 FR 16805, Mar. 31, lished for residues of the plant growth 2004; 71 FR 31104, June 1, 2006; 71 FR 76200, regulator forchlorfenuron; N-(2-chloro- Dec. 20, 2006] 4-pyridinyl)-N′phenyl urea in or on the following commodities: § 180.568 Flumioxazin; tolerances for residues. Commodity Parts per (a) General. Tolerances are estab- million lished for residues of flumioxazin, 2-[7- Grape ...... 0 .03 fluoro-3,4-dihydro-3-oxo-4-(2-propynyl)- Grape, raisin ...... 0 .06 2H-1,4-benzoxazin-6-yl]-4,5,6,7- Kiwifruit ...... 0.04 tetrahydro-1H-isoindole-1,3(2H)-dione, in or on the following raw agricultural (2) Time-limited tolerances are estab- commodities: lished for residues of the plant growth regulator forchlorfenuron; N-(2-chloro- Parts per Commodity million 4-pyridinyl)-N ′-phenylurea in or on the food commodities: Almond (hulls) ...... 0.70 Almond (nutmeat) ...... 0.02 Expiration/ Cotton, gin byproducts ...... 0 .60 Commodity Parts per revocation Cotton, undelinted seed ...... 0 .02 million date Fruit, pome, group 11 ...... 0.02 Fruit, stone, group 12 ...... 0 .02 Almond ...... 0.01 05/31/06 Garlic (bulb) ...... 0 .02 Apple ...... 0.01 05/31/06 Grape ...... 0 .02 Blueberry ...... 0.01 05/31/06 Onion (dry bulb) ...... 0 .02 Peanut ...... 0 .02 Cranberry ...... 0.01 05/31/06 Peppermint (tops) ...... 0.04 Fig ...... 0.01 05/31/06 Pistachio ...... 0.02 Olive ...... 0.01 05/31/06 Shallot (bulb) ...... 0 .02 Pear ...... 0.01 05/31/06 Soybean, seed ...... 0 .02 Plum (fresh) ...... 0.01 05/31/06 Spearmint (tops) ...... 0 .04 Strawberry ...... 0 .07 Sugarcane (cane) ...... 0 .20 (b) Section 18 emergency exemptions. Tuberous/corm vegetables (Subgroup 1C) ...... 0 .02 [Reserved] (c) Tolerances with regional restric- (b) Section 18 emergency exemptions. tions. [Reserved] Time-limited tolerances are estab-

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(d) Indirect or inadvertent residues. mesotrione, 2-[4-(methylsulfonyl)-2- [Reserved] nitrobenzoyl]-1,3-cyclohexanedione, in or on the following commodities: [66 FR 22936, May 7, 2001, as amended at 69 FR 48805, Aug. 11, 2004; 69 FR 58322, Sept. 30, Parts per 2004] Commodity million

§ 180.570 Isoxadifen-ethyl; tolerances Corn, field, forage ...... 0 .01 Corn, field, grain ...... 0 .01 for residues. Corn, field, stover ...... 0 .01 (a) General. (1) Tolerances are estab- Corn, pop, grain ...... 0.01 Corn, pop, stover ...... 0.01 lished for residues of isoxadifen-ethyl Corn, sweet, forage ...... 0 .5 (ethyl 5,5-diphenyl-2-isoxazoline-3- Corn, sweet, kernel plus cob with husks re- carboxylate, (CAS No. 163520–33–0), and moved ...... 0 .01 its metabolite: 4,5-dihydro-5,5-di- Corn, sweet, stover ...... 1 .5 phenyl-3-isoxazolecarboxylic acid, (b) Section 18 emergency exemptions. when used as an inert ingredient Time-limited tolerances are estab- (safener) in or on the following raw ag- lished for residues of the herbicide ricultural commodities when applied at mesotrione, 2-[4-(methylsulfonyl)-2- an annual application rate of 0.08 nitrobenzoyl]-1,3-cyclohexanedione, in pound of safener per acre. connection with use of the herbicide Parts per under section 18 emergency exemptions Commodity million granted by EPA. The tolerances are specified in the following table. The Corn, field, grain ...... 0 .10 Corn, field, forage ...... 0 .10 tolerances will expire on the dates Corn, field, stover ...... 0 .20 specified in the table.

Parts per (2) Tolerances are established for the Commodity h million residues of isoxadifen-ethyl (3- isoxazolecarboxylic acid, 4,5-dihydro- Corn, sweet, kernel plus cob with husks removed ...... 0.01 06/30/04 5,5-diphenyl-, ethyl ester (CAS No. Corn, sweet, forage ...... 0.50 06/30/04 163520–33–0)), and its metabolites 4,5- Corn, sweet, stover ...... 2.0 06/30/04 dihydro-5,5-diphenyl-3- Cranberry ...... 0.01 12/31/07 isoxazolecarboxylic acid and b-hy- droxy-b-benezenepropanenitrile when (c) Tolerances with regional registra- used as an inert ingredient (safener) in tions. [Reserved] or on the following raw agricultural (d) Indirect or inadvertent residues. commodities, when applied at an an- [Reserved] nual application rate of 0.17 pounds [66 FR 33195, June 21, 2001, as amended at 67 isoxadifen-ethyl/acre. FR 45656, July 10, 2002; 68 FR 273, Jan. 3, 2003; 69 FR 58310, Sept. 30, 2004; 70 FR 14551, Mar. Parts per 23, 2005] Commodity million

Rice, grain ...... 0 .10 § 180.572 Bifenazate; tolerance for resi- Rice, hulls ...... 0 .50 dues. Rice, straw ...... 0 .25 (a) General. (1) Tolerances are estab- lished for combined residues of (b) Section 18 emergency exemptions. bifenazate (1-methylethyl 2-(4- [Reserved] methoxy[1,1′-biphenyl]-3- (c) Tolerances with regional registra- yl)hydrazinecarboxylate) and tions. [Reserved] diazinecarboxylic acid, 2-(4-methoxy- (d) Indirect or inadvertent residues. [1,1′-biphenyl]-3-yl), 1-methylethyl [Reserved] ester (expressed as bifenazate) in or on [66 FR 33187, June 21, 2001, as amended at 66 the following food commodities: FR 40141, Aug. 2, 2001; 67 FR 12878, Mar. 20, 2002; 69 FR 29890, May 26, 2004] Parts per Commodity million

§ 180.571 Mesotrione; tolerances for Almond, hulls ...... 15 residues. Apple, wet pomace ...... 1 .2 Cattle, fat ...... 0.10 (a) General. Tolerances are estab- Cotton, gin byproducts ...... 35 lished for residues of the herbicide Cotton, undelinted seed ...... 0 .75

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Parts per Expiration/ Commodity million Commodity Parts per Revocation million Date Fruit, pome, group 11 ...... 0.75 Fruit, stone, group 12, except plum ...... 2 .5 Cherry, tart ...... 5.0 12/31/09 Goat, fat ...... 0 .10 Potato ...... 0.05 12/31/06 Grape ...... 0 .75 Soybean, hulls ...... 20 12/31/09 Soybean, meal ...... 3.5 12/31/09 Grape, raisin ...... 1 .2 Soybean, refined oil ...... 20 12/31/09 Hog, fat ...... 0 .10 Soybean, seed ...... 1.5 12/31/09 Hop, dried cones ...... 15 Timothy, forage ...... 50 12/31/07 Horse, fat ...... 0 .10 Timothy, hay ...... 150 12/31/07 Nut, tree, group 14 ...... 0 .20 Okra ...... 2.0 (c) Tolerances with regional registra- Pea, edible podded, succulent ...... 4.0 Pea, garden, succulent ...... 0 .20 tions. [Reserved] Peppermint, tops ...... 25 (d) Indirect or inadvertent residues. Pistachio ...... 0.20 [Reserved] Plum ...... 0 .20 Sheep, fat ...... 0 .10 [66 FR 34569, June 29, 2001, as amended at 66 Spearmint, tops ...... 25 FR 42772, Aug. 15, 2001; 67 FR 4922, Feb. 1, Strawberry ...... 1 .5 2002; 67 FR 46884, July 17, 2002; 68 FR 55502, Vegetable, cucurbit, group 9 ...... 0.75 Sept. 26, 2003; 69 FR 5297, Feb. 4, 2004; 70 FR Vegetable, fruiting, group 8 ...... 2.0 4037, Jan. 28, 2005; 70 FR 74695, Dec. 16, 2005; Vegetable, tuberous and corm, subgroup 1C ..... 0.10 71 FR 51505, Aug. 30, 2006]

(2) Tolerances are established for § 180.573 Tepraloxydim; tolerances for combined residues of bifenazate (1- residues. methylethyl 2-(4-methoxy[1,1′- (a) General. (1) Tolerances are estab- biphenyl]-3-yl) hydrazinecarboxylate); lished for the residues of tepraloxydim diazinecarboxylic acid, 2-(4-methoxy- (2-[1-[[[(2E)-3-chloro-2-pro- [1,1′-biphenyl]-3-yl), 1-methylethyl penyl]oxy]imino]propyl]-3-hydroxy-5- ester (expressed as bifenazate); 1,1′- (tetrahydro-2H-pyran-4-yl)- biphenyl, 4-ol; and 1,1′-biphenyl, 4- cyclohexene-1-one) and its metabolites oxysulfonic acid (expressed as 1,1′- convertible to GP (3-(tetrahydropyran- biphenyl, 4-ol) in or on the following 4-yl)pentane-1,5-dioic acid) and OH-GP food commodities: (3-hydroxy-3-(tetrahydropyran-4- yl)pentane-1,5-dioic acid), calculated as Parts per mil- Commodity lion tepraloxydim in or on the following raw agricultural commodities. Cattle, meat ...... 0.02 Cattle, meat byproducts ...... 0.02 Commodity Parts per Goat, meat ...... 0.02 million Goat, meat byproducts ...... 0.02 Hog, meat ...... 0.02 Cotton, undelinated seed ...... 0 .2 Hog, meat byproducts ...... 0.02 Cotton, gin byproducts ...... 3 .0 Soybean, seed ...... 6 .0 Horse, meat ...... 0.02 Soybean, hulls ...... 8 .0 Horse, meat byproducts ...... 0.02 Soybean, aspirated grain fraction ...... 1200 .0 Milk ...... 0.02 Sheep, meat ...... 0.02 Sheep, meat byproducts ...... 0.02 (2) Tolerances are established for the combined residues of tepraloxydim and (b) Section 18 emergency exemptions. its metabolites convertible to GP, OH- Time-limited tolerances are estab- GP, and GL (3-(2-oxotetrahydropyran-4- lished for combined residues of yl)-1,5-dioic acid), calculated as bifenazate (1-methylethyl 2-(4- tepraloxydim in or on the following methoxy[1,1′-biphenyl]-3- commodities yl)hydrazinecarboxylate) and Parts per diazinecarboxylic acid, 2-(4-methoxy- Commodity million [1,1′-biphenyl]-3-yl), 1-methylethyl Cattle, fat ...... 0.15 ester (expressed as bifenazate) in con- Cattle, kidney ...... 0 .50 nection with use of the pesticide under Cattle, meat ...... 0 .20 section 18 emergency exemptions Cattle, meat byproducts, except kidney ...... 0.20 granted by EPA. The tolerances will Egg ...... 0 .20 Goat, fat ...... 0 .15 expire and are revoked on the dates Goat, kidney ...... 0 .50 specified in the following table. Goat, meat ...... 0.20

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Parts per Parts per Commodity million Commodity million

Goat, meat byproducts, except kidney ...... 0 .20 Wine grape 1 ...... 3 .0 Hog, fat ...... 0 .15 1 No US registration as of March 15, 2002. Hog, kidney ...... 0.50 Hog, meat ...... 0 .20 (b) Section 18 emergency exemptions. Hog, meat byproducts, except kidney ...... 0 .20 [Reserved] Horse, fat ...... 0 .15 Horse, kidney ...... 0 .50 (c) Tolerances with regional registra- Horse, meat ...... 0 .20 tions. [Reserved] Horse, meat byproducts, except kidney ...... 0 .20 (d) Indirect or inadvertent residues. Milk ...... 0.10 [Reserved] Poultry, fat ...... 0.30 Poultry, liver ...... 1 .00 [66 FR 46738, Sept. 7, 2001, as amended at 67 Poultry, meat ...... 0 .20 FR 19130, Apr. 18, 2002] Poultry, meat byproducts, except liver ...... 0 .20 Sheep, fat ...... 0 .15 § 180.575 Sulfuryl fluoride; tolerances Sheep, kidney ...... 0.50 for residues. Sheep, meat ...... 0.20 Sheep, meat byproducts, except kidney ...... 0 .20 (a)(1) General. Tolerances are estab- lished for residues of sulfuryl fluoride (b) Section 18 emergency exemptions. in or on the following commodities [Reserved] from the postharvest fumigation with (c) Tolerances with regional registra- sulfuryl fluoride for the control of in- tions. A tolerance with regional reg- sects: istration, as defined in § 180.1(n) is es- Parts per tablished for the combined residues of Commodity million tepraloxydim and its metabolites con- vertible to GP and OH-GP, calculated All processed food commodities not otherwise listed ...... 2 .0 as tepraloxydim in or on the following Barley, bran, postharvest ...... 0 .05 raw agricultural commodity: Barley, flour, postharvest ...... 0.05 Barley, grain, postharvest ...... 0 .1 Barley, pearled barley, postharvest ...... 0 .05 Commodity Parts per million Cacao bean, roasted bean, postharvest ...... 0.2 Cattle, meat, dried ...... 0.01 Canola, seed ...... 0 .50 Cheese ...... 2 .0 Coconut, postharvest ...... 1 .0 (d) Indirect or inadvertent residues. Coffee, postharvest ...... 1 .0 Corn, field, flour, postharvest ...... 0 .01 [Reserved] Corn, field, grain, postharvest ...... 0 .05 Corn, field, grits, postharvest ...... 15.0 [66 FR 40150, Aug. 2, 2001] Corn, field, meal, postharvest ...... 0 .01 Corn, pop, grain, postharvest ...... 0 .05 § 180.574 Fluazinam; tolerances for Cotton, undelinted seed, postharvest ...... 0.5 residues. Egg, dried ...... 1 .0 Fruit, dried, postharvest ...... 0 .05 (a)(1) General. Tolerances are estab- Ginger, postharvest ...... 0 .5 lished for residues of fluazinam, (3- Grain, aspirated fractions, postharvest ...... 0 .05 Herbs and spices group 19, postharvest ...... 0 .5 chloro-N-[3-chloro-2,6-dinitro-4- Hog, meat ...... 0 .02 (trifluoromethyl) phenyl]-5- Milk, powdered ...... 2 .0 (trifluoromethyl)-2-pyridinamine) in or Millet, grain, postharvest ...... 0.1 on the following commodities: Nut, pine, postharvest ...... 0.2 Nut, tree, Group 14, postharvest ...... 3 .0 Oat, flour, postharvest ...... 0 .05 Parts per Oat, grain, postharvest ...... 0 .1 Commodity million Oat, groats/rolled oats, postharvest ...... 0 .1 Peanut ...... 0 .02 Peanut, postharvest ...... 0 .5 Pistachio, postharvest ...... 3 .0 Potato ...... 0 .02 Rice, bran, postharvest ...... 0 .01 Rice, flour, postharvest ...... 0 .05 (a)(2) Tolerances are established for Rice, grain, postharvest ...... 0 .04 residues of fluazinam and its metabo- Rice, hulls, postharvest ...... 0.1 lite AMGT 3-[[4-amino-3-[[3-chloro-5- Rice, polished rice, postharvest ...... 0 .01 Rice, wild, grain, postharvest ...... 0 .05 (trifloromethyl)-2-pyridinyl]amino]-2- Sorghum, grain, postharvest ...... 0 .1 nitro-6-(trifluoromethyl) phenyl] thio]- Triticale, grain, postharvest ...... 0 .1 2-(beta-D-glucopyranosyloxy) propionic Vegetable, legume, group 6, postharvest ...... 0.5 Wheat, bran, postharvest ...... 0 .05 acid) in or on the following com- Wheat, flour, postharvest ...... 0 .05 modity: Wheat, germ, postharvest ...... 0 .02

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Parts per Parts per Commodity million Commodity million

Wheat, grain, postharvest ...... 0 .1 Rice, grain ...... 0 .02 Wheat, milled byproducts, postharvest ...... 0 .05 Rice, straw ...... 0 .02 Wheat, shorts, postharvest ...... 0 .05 (b) Section 18 emergency exemptions. (2) To assure safe use of this pesticide [Reserved] commodities treated with sulfuryl flu- (c) Tolerances with regional registra- oride must be aerated for at least 24 tions. [Reserved] hours prior to entering commerce. (d) Indirect or inadvertent residues. (b) Section 18 emergency exemptions. [Reserved] [Reserved] [66 FR 48097, Sept. 18, 2001] (c) Tolerances with regional registra- tion. [Reserved] § 180.578 Acetamiprid; tolerances for (d) Indirect or inadvertant residues. residues. [Reserved] (a) General. (1) Tolerances are estab- lished for residues of the insecticide [67 FR 5740, Feb. 7, 2002, as amended at 69 FR acetamiprid N1-[(6-chloro-3-pyr- 3257, Jan. 23, 2004; 70 FR 40908, July 15, 2005] idyl)methyl]-N2-cyano-N1- methylacetamidine in or on the fol- § 180.576 Cyhalofop-butyl; tolerances lowing commodities: for residues. (a) General. Time-limited tolerances Parts per Commodity million are established for combined residues of cyhalofop (cyhalofop-butyl, R-(+)-n- Canola, seed ...... 0.010 Citrus, dried pulp ...... 1.20 butyl-2-(4(4-cyano-2-fluorophenoxy)- Cotton, gin byproducts ...... 20.0 phenoxy)propionate, plus cyhalofop Cotton, undelinted seed ...... 0.60 acid, R-(+)-2-(4(4-cyano-2- Fruit, citrus, group 10 ...... 0.50 Fruit, pome group ...... 1.0 fluorophenoxy)-phenoxy)propionic Grape ...... 0.20 acid) and the di-acid metabolite, (2R)-4- Mustard, seed ...... 0.010 [4-(1-carboxyethoxy)phenoxy]-3- Tomato, paste ...... 0.40 Vegetable, brassica, leafy, group 5 ...... 1.20 fluorobenzoic acid, from the applica- Vegetable, fruiting, group 8 ...... 0.20 tion of the herbicide cyhalofop-butyl in Vegetable, leafy, except brassica, group 4 ...... 3.00 or on the following raw agricultural Vegetable, tuberous and corm, group 1 ...... 0.01 commodities: (2) Tolerances are established for the combined residues of the insecticide Parts per Expiration/ Commodity Revocation acetamiprid N1-[(6-chloro-3-pyr- million Date idyl)methyl]-N2-cyano-N1- Rice, grain ...... 0.03 6/1/2007 methylacetamidine and N1-[(6-chloro-3- Rice, straw ...... 8.0 6/1/2007 pyridyl)methyl]-N2-cyano-acetamidine in or on the following commodities: (b) Section 18 emergency exemptions. [Reserved] Parts per Commodity million (c) Tolerances with regional registra- tions. [Reserved] Cattle, fat ...... 0.10 Cattle, meat ...... 0.10 (d) Indirect or inadvertent residues. Cattle, meat byproducts ...... 0.20 [Reserved] Egg ...... 0.010 Goat, fat ...... 0.10 [67 FR 43256, June 27, 2002] Goat, meat ...... 0.10 Goat, meat byproducts ...... 0.20 § 180.577 Bispyribac-sodium; toler- Hog, fat ...... 0.10 Hog, meat ...... 0.10 ances for residues. Hog, meat byproducts ...... 0.20 (a) General. Tolerances are estab- Horse, fat ...... 0.10 Horse, meat ...... 0.10 lished for residues of bispyribac-so- Horse, meat byproducts ...... 0.20 dium, sodium 2,6-bis[(4,6-dimethoxy- Milk ...... 0.10 pyrimidin-2-yl)oxy]benzoate, in or on Poultry, fat ...... 0.010 Poultry, liver ...... 0.050 the following raw agricultural com- Poultry, meat ...... 0.010 modities: Sheep, fat ...... 0.10

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(b) Section 18 emergency exemptions. A Commodity Parts per million time-limited tolerance is established Sheep, meat ...... 0.10 for residues of the fungicide Sheep, meat byproducts ...... 0.20 fenamidone, (4H-imidazol-4-one, 3,5- dihydro-5-methyl-2-(methylthio)-5- (b) Section 18 emergency exemptions. phenyl-3-(phenylamino), (S)-) in con- [Reserved] nection with use of the pesticide under (c) Tolerances with regional registra- a section 18 emergency exemption tions. [Reserved] granted by EPA. The tolerance will ex- (d) Indirect or inadvertent residues. pire and is revoked on the date speci- [Reserved] fied in the following table:

[67 FR 14659, Mar. 27, 2002, as amended at 68 Expiration/ FR 52352, Sept. 3, 2003; 70 FR 19293, Apr. 13, Parts per Commodity million revocation 2005] date

§ 180.579 Fenamidone; tolerances for Carrot ...... 0.20 12/31/2009 residues. (c) Tolerances with regional registra- (a) General. (1) Tolerances are estab- tions. [Reserved] lished for residues of fenamidone (4H- (d) Indirect or inadvertent residues. Imidazol-4-one, 3,5-dihydro-5-methyl-2- Tolerances are established for residues (methylthio)-5-phenyl-3 (phenylamino)- of the fungicide fenamidone (4-H- , (S)-) from the application of the fun- imidazol-4-one, 3,5-dihydro-5-methyl-2- gicide fenamidone on the following raw (methlthio)-5-phenyl-3-(phenylamino, agricultural commodities: (S)-) and its metabolite RPA 717879 (2,4- imidazolidinedione, 5-methyl-5-phenyl) Parts per Commodity million in or on the following agricultural commodities when present therein as a Garlic, bulb ...... 0.20 result of application of fenamidone to Garlic, great headed ...... 0.20 Grape (imported) ...... 1 .0 the crops in paragraph (a)(1). Leek ...... 1 .5 Lettuce, head ...... 15 Commodity Parts per Lettuce, leaf ...... 20 million Onion, dry bulb ...... 0 .20 Onion, green ...... 1 .5 Wheat, grain ...... 0 .10 Onion, welsh ...... 1.5 Wheat, hay ...... 0 .50 Shallot, bulb ...... 0 .20 Wheat, forage ...... 0 .15 Shallot, fresh leaves ...... 1 .5 Wheat, straw ...... 0 .35 Tomato ...... 1.0 Tomato, paste ...... 2 .2 Tomato, puree ...... 2 .0 [67 FR 60976, Sept. 27, 2002, as amended at 69 Vegetable, cucurbit, group 9 ...... 0.15 FR 58066, Sept. 29, 2004; 71 FR 55293, Sept. 22, Vegetable, tuberous and corm, subgroup 01C ... 0 .02 2006]

(2) Tolerances are established for the § 180.580 Iodosulfuron-Methyl-Sodium; combined residues of fenamidone (4H- tolerances for residues. imidazol-4-one, 3,5-dihydro-5-methyl-2- (a) General. Tolerances are estab- (methylthio)-5-phenyl-3-(phenylamino), lished for residues of the herbicide (S)-) and its metabolite RPA 717879 (2,4- Iodosulfuron-Methyl-Sodium (methyl 4- imidazolidinedione, 5-methyl-5-phenyl), iodo-2-[3-(4-methoxy-6-methyl-1,3,5 expressed as parent compound, in or on triazin-2-yl)ureidosulfonyl]benzoate, so- the following commodities: dium salt) in or on the following com- modities: Commodity Parts per million Parts per Commodity million Beef, fat ...... 0 .10 Beef, meat ...... 0 .10 Corn, field, forage ...... 0 .05 Beef, meat byproducts ...... 0 .10 Corn, field, grain ...... 0 .03 Goat, fat ...... 0 .10 Corn, field, stover ...... 0 .05 Goat, meat ...... 0.10 Goat, meat byproducts ...... 0 .10 Milk ...... 0.02 (b) Section 18 emergency exemptions. Sheep, fat ...... 0 .10 [Reserved] Sheep, meat ...... 0.10 (c) Tolerances with regional registra- Sheep, meat byproduct ...... 0 .10 tions. [Reserved]

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(d) Indirect or inadvertent residues. Commodity Parts per [Reserved] million [67 FR 57532, Sept. 11, 2002] Corn, pop, grain ...... 0.1 Corn, pop, stover ...... 17.0 § 180.581 Iprovalicarb; tolerances for Corn, sweet, forage ...... 5 .0 Corn, sweet, kernel plus cob with husks re- residues. moved ...... 0 .04 (a) General. Tolerances are estab- Corn, sweet, stover ...... 23.0 lished for residues of iprovalicarb, [2- Fruit, citrus, group 10 ...... 2 .0 Fruit, pome, group ...... 1.5 methyl-1[[[(1S)-(4-methylphenyl) ethyl] Fruit, stone, group 12 ...... 0 .9 amino]carbonyl] propyl]carbamic acid Grain, aspirated fractions ...... 2 .5 methylethylester, in or on the fol- Grape ...... 2 .0 lowing commodities. Grape, raisin ...... 7 .0 Grass, forage ...... 10 Grass, hay ...... 4 .5 Commodity Parts per million Grass, seed screenings ...... 27 Grass, straw grown for seed ...... 14 Grape1 ...... 2 .0 Hop, dried cones ...... 23 .0 1 Tomatoes ...... 1 .0 Legume, forage, except peanut and soybean, 1There is no U.S. registration as of September 1, 2005. subgroup ...... 25.0 Mango1 ...... 0 .1 (b) Section 18 emergency exemptions. Nut, tree, group 14 ...... 0 .04 [Reserved] Papaya1 ...... 0 .1 (c) Tolerances with regional registra- Pea, succulent ...... 0 .2 tions. [Reserved] Pea and bean, dried shelled, except soybean, subgroup 6C ...... 0 .5 (d) Indirect or inadvertent residues. Peanut ...... 0 .05 [Reserved] Peanut, refined oil ...... 0.1 Peppermint ...... 8 .0 [67 FR 54359, Aug. 22, 2002, as amended at 70 Pistachio ...... 0.7 FR 55281, Sept. 21, 2005] Radish, tops ...... 16 Rye, grain ...... 0.04 § 180.582 Pyraclostrobin; tolerances Rye, straw ...... 0 .5 for residues. Soybean, forage ...... 5 .0 Soybean, hay ...... 7 .0 (a) General. (1) Tolerances are estab- Soybean, hulls ...... 0 .06 lished for combined residues of the fun- Soybean, seed ...... 0 .04 gicide pyraclostrobin (carbamic acid, Spearmint ...... 8.0 [2-[[[1-(4-chlorophenyl)-1H-pyrazol-3- Strawberry ...... 1 .2 yl]oxy]methyl]phenyl]methoxy-, meth- Sunflower ...... 0 .3 Vegetable, bulb ...... 0 .9 yl ester) and its desmethoxy metabo- Vegetable, cucurbit, group 9 ...... 0.5 lite (methyl-N-[[[1-(4-chlorophenyl)-1H- Vegetables, foliage of legume, group 7 ...... 25 pyrazol-3- Vegetable, fruiting, group 8 ...... 1.4 yl]oxy]methyl]phenylcarbamate), ex- Vegetable, leafy, except brassica, group ...... 29.0 Vegetable, leaves of root and tuber, except pressed as parent compound, in or on sugar beet ...... 16 .0 the following raw agricultural com- Vegetable, legume, edible podded, subgroup .... 0 .5 modities. Vegetable, root, except sugar beet, subgroup 1B ...... 0 .4 Vegetable, tuberous and corm, subgroup 1C ..... 0.04 Commodity Parts per million Wheat, grain ...... 0 .02 Wheat, hay ...... 6 .0 Almond, hulls ...... 7 .0 Wheat, straw ...... 8 .5 Apple, wet pomace ...... 8 .0 Banana ...... 0.04 1 There are no U.S. registrations on mango or papaya as of Barley, grain ...... 0 .4 April 5, 2006. Barley, hay ...... 25 Barley, straw ...... 6 .0 (2) Tolerances are established for Bean, succulent shelled ...... 0 .5 combined residues of the fungicide Beet, sugar, dried pulp ...... 1 .0 pyraclostrobin carbamic acid, [2-[[[1-(4- Beet, sugar, roots ...... 0 .2 Beet, sugar, tops ...... 8.0 chlorophenyl)-1H-pyrazol-3- Berry group 13 ...... 1 .3 yl]oxy]methyl]phenyl]methoxy-, meth- Brassica, head and stem, subgroup ...... 5.0 yl ester and its metabolites convertible Brassica, leafy greens, subgroup ...... 16 .0 Citrus, dried pulp ...... 12 .5 to 1-(4-chlorophenyl)-1H-pyrazol-3-ol Citrus, oil ...... 9.0 and 1-(4-chloro-2-hydroxyphenyl)-1H- Corn, field, forage ...... 5 .0 pyrazol-3-ol, expressed as parent com- Corn, field, grain ...... 0 .1 Corn, field, refined oil ...... 0 .2 pound, in or on the following raw agri- Corn, field, stover ...... 17 .0 cultural commodities.

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Commodity Parts per § 180.584 Tolylfluanid; tolerances for million residues. Cattle, fat ...... 0.1 (a) General. Tolerances are estab- Cattle, liver ...... 1 .5 lished for residues of tolylfluanid, 1,1- Cattle, meat ...... 0 .1 dichloro-N-[(dimethylamino)-sulfonyl]- Cattle, meat byproducts, except liver ...... 0 .2 Goat, fat ...... 0 .1 1-fluoro-N-(4- Goat, liver ...... 1.5 methylphenyl)methanesulfenamide in Goat, meat ...... 0.1 or on the following commodities. Goat, meat byproducts, except liver ...... 0 .2 Hog, fat ...... 0 .1 Commodity Parts per Hog, liver ...... 1 .5 million Hog, meat ...... 0 .1 1 Hog, meat byproducts, except liver ...... 0 .2 Apple ...... 5 .0 1 Horse, fat ...... 0 .1 Grape ...... 11 Hop1 ...... 30 Horse, liver ...... 0 .1 Tomato1 ...... 2 .0 Horse, meat ...... 0 .1 Horse, meat byproducts, except liver ...... 0 .2 1 No U.S. registration as of August 31, 2002. Milk ...... 0.1 Sheep, fat ...... 0 .1 (b) Section 18 emergency exemptions. Sheep, liver ...... 1.5 [Reserved] Sheep, meat ...... 0.1 (c) Tolerances with regional registra- Sheep, meat byproducts, except liver ...... 0 .2 tions. [Reserved] (d) Indirect or inadvertent residues. (b) Section 18 emergency exemptions. [Reserved] [Reserved] (c) Tolerances with regional registra- [67 FR 60141, Sept. 25, 2002] tions. [Reserved] § 180.585 Pyraflufen-ethyl; tolerances (d) Indirect or inadvertent residues. for residues. [Reserved] (a) General. Tolerances are estab- [67 FR 60901, Sept. 27, 2002, as amended at 69 lished for residues of the herbicide FR 63100, Oct. 29, 2004; 71 FR 17021, Apr. 5, pyraflufen-ethyl (ethyl 2-chloro-5-(4- 2006] chloro-5-difluoromethoxy-1-methyl-1H- § 180.583 Triticonazole; tolerances for pyrazol-3-yl)-4-fluorophenoxyacetate) residues. and its acid metabolite, E-1 (2-chloro-5- (4-chloro-5-difluoromethoxy-1-methyl- (a) General. Tolerances are estab- 1H-pyrazol-3-yl)-4- fluorophenoxyacetic lished for residues of the fungicide acid), in or on the following raw agri- triticonazole, (1RS)-(E)-5-[(4- cultural commodities: chlorophenyl)methylene]-2,2-dimethyl- 1-(1H-1,2,4-triazol-1- Commodity Parts per ylmethyl)cyclopentanol, from the million treatment of seed prior to planting in Corn, field, forage ...... 0 .01 or on raw agricultural commodities as Corn, field, grain ...... 0 .01 Corn, field, stover ...... 0 .01 follows: Cotton, gin byproducts ...... 1 .5 Cotton, undelinted seed ...... 0 .04 Commodity Parts per Potato ...... 0 .02 million Soybean, forage ...... 0 .01 Soybean, hay ...... 0 .01 Barley, grain ...... 0 .05 Soybean, seed ...... 0 .01 Barley, hay ...... 0 .05 Wheat, forage ...... 0 .1 Barley, straw ...... 0 .05 Wheat, grain ...... 0 .01 Wheat, forage ...... 0 .05 Wheat, hay ...... 0 .1 Wheat, grain ...... 0 .05 Wheat, straw ...... 0 .01 Wheat, hay ...... 0 .05 Wheat, straw ...... 0 .05 (b) Section 18 emergency exemptions. [Reserved] (b) Section 18 emergency exemptions. (c) Tolerances with regional registra- [Reserved] tions. [Reserved] (c) Tolerances with regional registra- (d) Indirect or inadvertent residues. tions. [Reserved] [Reserved] (d) Indirect or inadvertent residues. [Reserved] [68 FR 23055, Apr. 30, 2003, as amended at 68 FR 27739, May 21, 2003; 69 FR 26312, May 12, [67 FR 60959, Sept. 27, 2002] 2004]

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§ 180.586 Clothianidin; tolerances for Commodity Parts per residues. million (a) General. Tolerances are estab- Grass, forage, fodder and hay, group 17 ...... 0 .02 lished for residues of the insecticide Soybean, forage ...... 0 .02 clothianidin, (E)-1-(2-chloro-1,3-thiazol- Soybean, hay ...... 0 .02 5-ylmethyl)-3-methyl-2-nitroguanidine, in or on the following raw agricultural [68 FR 32399, May 30, 2003, as amended at 70 commodities: FR 7894, Feb. 16, 2005; 71 FR 74801, Dec. 13, 2006] Commodity Parts per million § 180.587 Famoxadone; tolerance for Canola, seed ...... 0 .01 residues. Corn, field, forage ...... 0 .10 Corn, field, grain ...... 0 .01 (a) General. Tolerances are estab- Corn, field, stover ...... 0 .10 lished for residues of the fungicide Corn, pop, grain ...... 0.01 famoxadone (3-anilino-5-methyl-5-(4- Corn, pop, stover ...... 0.10 Corn, sweet, forage ...... 0 .10 phenoxyphenyl)-1,3-oxazolidine-2,4- Corn, sweet, kernel plus cob with husk removed 0.01 dione) in or on the following commod- Corn, sweet, stover ...... 0 .10 ities: Cotton, gin byproducts ...... 0 .01 Cotton, undelinted seed ...... 0 .01 Grape ...... 0 .60 Parts per Commodity million Milk ...... 0.01 Pome fruit ...... 1.0 Caneberry, Subgroup 13A ...... 10 Potato ...... 0 .05 Potato, granules/flakes ...... 0 .08 Cattle, fat ...... 0.02 Sorghum, forage, grain, stover ...... 0 .01 Cattle, liver ...... 0 .05 Goat, fat ...... 0 .02 (b) Section 18 emergency exemptions. Goat, liver ...... 0.05 Grape, raisin1 ...... 4 .0 Time-limited tolerances are estab- Hop, dried cone ...... 80 lished for the residues of the insecti- Horse, fat ...... 0 .02 cide clothianidin, (E)-1-(2-chloro-1,3- Horse, liver ...... 0 .05 thiazol-5-ylmethyl)-3-methyl-2- Lettuce, head ...... 10.0 nitroguanidine, in connection with use Milk, fat (reflecting negligible residues in whole of the pesticide under section 18 emer- milk) ...... 0 .06 Potato ...... 0 .02 gency exemptions granted by EPA. Sheep, fat ...... 0 .02 These tolerances will expire and are re- Sheep, liver ...... 0.05 voked on the dates specified in the fol- Tomato ...... 1.0 lowing table: Vegetable, cucurbits, group 9 ...... 0.30 Vegetable, fruiting, group 8 except tomato ...... 4 .0 Expiration/ Commodity Parts per revocation 1 There are no U.S. registrations as of May 15, 2003. million date (b) Section 18 emergency exemptions. Beet, sugar, roots ...... 0.02 12/31/09 [Reserved] Beet, sugar, tops ...... 0.02 12/31/09 (c) Tolerances with a regional registra- (c) Tolerances with regional registra- tions. Tolerances with a regional reg- tions. [Reserved] istration as defined in Sec. 180.1(n) are (d) Indirect and inadvertant residues. established for the residues of the fun- Tolerances are established for the indi- gicide famoxadone, 3-anilino-5-methyl- rect or inadvertent residues of the in- 5-(4-phenoxyphenyl)-1,3-oxazolidine-2,4- secticide clothianidin, (E)-1-(2-chloro- dione) in or on the raw agricultural 1,3-thiazol-5-ylmethyl)-3-methyl-2- commodities: nitroguanidine, in or on the following Parts per raw agricultural commodities when Commodity million present therein as a result of the appli- cation of clothianidin to crops listed in Grape ...... 2 .5 paragraph (a) of this section: (d) Indirect or inadvertant residues. Parts per Commodity million [Reserved]

Animal feed, nongrass ...... 0 .02 [68 FR 39471, July 2, 2003, as amended at 72 Grain, cereal, forage, fodder and straw ...... 0 .02 FR 28881, May 23, 2007]

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§ 180.588 Quinoxyfen; tolerances for Commodity Parts per residues. million (a) General. Tolerances are estab- Berries, group 13 ...... 3.5 lished for residues of the fungicide Canola, refined oil ...... 5 .0 Canola, seed ...... 3 .5 quinoxyfen, 5,7-dichloro-4-(4- Cucumber ...... 0 .20 fluorophenoxy)quinoline in or on the Fruit, pome, crop group, group 11 ...... 3 .0 following raw agricultural commod- Fruit, stone, group 12 ...... 1 .7 Grape ...... 3 .5 ities: Grape, raisin ...... 8 .5 Hops, cones, dried ...... 35 Parts per Leafy greens, subgroup 4A, except head and Commodity million leaf lettuce ...... 60 Leafy petioles, subgroup 4B ...... 45 Cherry, sweet ...... 0 .30 Lettuce, head ...... 6.5 Cherry, tart ...... 0 .30 Hop, dried cones ...... 3 .0 Lettuce, leaf ...... 11 .0 Grape ...... 0 .60 Nut, tree, group 14 ...... 0 .70 Lettuce, head ...... 7.0 Pea and bean, succulent shelled, subgroup 6B, Lettuce, leaf ...... 19 except cowpea ...... 0 .6 Melon, subgroup 9A ...... 0 .08 Peanut ...... 0 .05 Pepper, bell ...... 0 .35 Peanut, meal ...... 0 .15 Pepper, nonbell ...... 1 .7 Peanut, refined oil ...... 0.15 Strawberry ...... 0 .90 Peppermint, tops ...... 30 .0 Pistachio ...... 0.70 Soybean, hulls ...... 0 .2 (b) Section 18 emergency exemptions. Soybean, seed ...... 0 .1 Time-limited tolerances are estab- Soybean, vegetable ...... 2 .0 lished for residues of the fungicide Spearmint, tops ...... 30 .0 Strawberry ...... 4 .5 quinoxyfen, 5,7-dichloro-4-(4- Sunflower, seed ...... 0.60 fluorophenoxy)quinoline in connection Vegetable, Brassica leafy, head and stem, sub- with use of the pesticide under section group 5A ...... 3 .0 18 emergency exemptions granted by Vegetable, Brassica leafy, leafy greens, sub- group 5B ...... 18 .0 EPA. The time-limited tolerances will Vegetable, bulb, group 3 ...... 3 .0 expire and are revoked on the date Vegetable, cucurbit, group 9, except cucumber 1.6 specified in the following table: Vegetable, fruiting, group 8 ...... 1.2 Vegetable, legume, dried shell pea and bean Expiration/ (except soybean), subgroup 6C, except Commodity Parts per revocation cowpea, field pea, and grain lupin ...... 2 .5 million date Vegetable, legume, edible podded, subgroup 6A 1 .6 Vegetable, root, subgroup 1A , except sugar Pumpkin ...... 0.30 12/31/07 beet, garden beet, radish, and turnip ...... 0 .7 Squash, winter ...... 0.30 12/31/07 Vegetable, tuberous and corm, subgroup 1C ..... 0.05 Vegetable, cucurbit, subgroup 9A ... 0.30 12/31/07 1 No US registration as of January 31, 2006. (c) Tolerances with regional registra- (2) Tolerances are established for the tions. [Reserved] combined residues of the fungicide (d) Indirect or inadvertent residues. boscalid, 3-pyridinecarboxamide, 2- [Reserved] chloro-N-(4′-chloro[1,1′-biphenyl]-2-yl) and metabolites 2-chloro-N-(4′-chloro-5- [68 FR 55858, Sept. 29, 2003, as amended at 70 FR 4032, Jan. 28, 2005; 71 FR 50354, Aug. 25, hydroxy-biphenyl-2-yl)nicotinamide 2006] and glucuronic acid conjugate of 2- chloro-N-(4′-chloro-5-hydroxy-biphenyl- § 180.589 Boscalid; tolerances for resi- 2-yl)nicotinamide in or on the fol- dues. lowing food commodities: (a) General. (1) Tolerances are estab- Parts per lished for residues of the fungicide Commodity million boscalid, 3-pyridinecarboxamide, 2- ′ ′ Cattle, fat ...... 0.30 chloro-N-(4 -chloro[1,1 -biphenyl]-2-yl) Cattle, meat ...... 0 .10 in or on the following raw agricultural Cattle, meat byproducts ...... 0.35 commodities: Egg ...... 0 .02 Goat, fat ...... 0 .30 Parts per Goat, meat ...... 0.10 Commodity million Goat, meat, byproducts ...... 0 .35 Hog, fat ...... 0 .10 Almond, hulls ...... 17 Hog, meat ...... 0 .05 Apple, wet, pomace ...... 10 Hog, meat byproducts ...... 0 .10 Aspirated grain fractions ...... 3 .0 Horse, fat ...... 0 .30 Banana, import1 ...... 0 .20 Horse, meat ...... 0 .10

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Parts per Parts per Commodity million Commodity million

Horse, meat byproducts ...... 0 .35 Rice, hulls ...... 0 .50 Milk ...... 0.10 Turnip, roots ...... 0 .1 Poultry, fat ...... 0.05 Vegetable, leafy, group 4, except lettuce, celery Poultry, meat ...... 0 .05 and spinach ...... 1 .0 Poultry, meat, byproduct ...... 0 .10 Vegetable, legume, foliage, group 7, forage ...... 1 .5 Sheep, fat ...... 0 .30 Vegetable, legume, foliage, group 7, hay ...... 2 .0 Sheep, meat ...... 0.10 Vegetable, legume, foliage, group 7, vines ...... 0.05 Sheep, meat byproducts ...... 0 .35 Vegetable, root and tuber, leaves, Group 2 ...... 0.1

(b) Section 18 emergency exemptions. [68 FR 44651, July 30, 2003, as amended at 69 Time-limited tolerances are estab- FR 19774, Apr. 14, 2004; 70 FR 55293, Sept. 21, lished for residues of the fungicide 2005; 71 FR 6364, Feb. 8, 2006; 71 FR 25961, May boscalid, 3-pyridinecarboxamide, 2- 3, 2006; 71 FR 76190, Dec. 20, 2006] chloro-N-(4′-chloro[1,1′-biphenyl]-2-yl) in connection with use of the pesticide § 180.590 2, 6-Diisopropylnaphthalene under section 18 emergency exemptions (2, 6-DIPN); tolerances for residues. granted by EPA. These tolerances will (a) General. Time-limited tolerances expire and are revoked on the dates are established for residues of 2, 6- specified in the following table: DIPN in or on the following commod- ities resulting from post-harvest appli- Expiration/ Commodity Parts per Revocation cations to potato, when 2, 6-DIPN is million Date used in accordance with good agricul- tural practices: Tangerine ...... 2.0 12/31/08

Parts per Expiration/ (c) Tolerances with regional registra- Commodity million revocation tion. [Reserved] date (d) Indirect or inadvertent residues. Cattle, fat ...... 0.8 8/1/09 Tolerances are established for residues Cattle, liver ...... 0.3 8/1/09 of the fungicide boscalid, 3- Cattle, meat ...... 0.1 8/1/09 Cattle, meat byproducts ...... 0.1 8/1/09 pyridinecarboxamide, 2-chloro-N-(4′- Goat, fat ...... 0.8 8/1/09 chloro[1,1′-biphenyl]-2-yl) in or on the Goat, liver ...... 0.3 8/1/09 following raw agricultural commod- Goat, meat ...... 0.1 8/1/09 Goat, meat byproducts ...... 0.1 8/1/09 ities when present therein as a result Hog, fat ...... 0.8 8/1/09 of application of boscalid to the grow- Hog, liver ...... 0.3 8/1/09 ing crops in paragraph (a)(1) of this sec- Hog, meat ...... 0.1 8/1/09 Hog, meat byproducts ...... 0.1 8/1/09 tion: Horse, fat ...... 0.8 8/1/09 Horse, liver ...... 0.3 8/1/09 Parts per Horse, meat ...... 0.1 8/1/09 Commodity million Horse, meat byproducts ...... 0.1 8/1/09 Milk ...... 0.1 8/1/09 Animal feed, nongrass, group 18, forage ...... 1 .0 Potato ...... 2.0 8/1/09 Animal feed, nongrass, group 18, hay ...... 2.0 Potato, wet peel ...... 6.0 8/1/09 Animal feed, nongrass, group 18, seed ...... 0 .05 Sheep, fat ...... 0.8 8/1/09 Beet, garden, roots ...... 0 .1 Sheep, liver ...... 0.3 8/1/09 Beet, sugar, roots ...... 0 .1 Sheep, meat ...... 0.1 8/1/09 Cotton, gin byproducts ...... 0 .30 Sheep, meat byproducts ...... 0.1 8/1/09 Cotton, undelinted seed ...... 0 .05 Cowpea, seed ...... 0 .1 Flax, seed ...... 3 .5 (b) Section 18 emergency exemptions. Grain, cereal, forage, fodder and straw, group [Reserved] 16, fodder ...... 1 .5 Grain, cereal, forage, fodder and straw, group (c) Tolerances with regional registra- 16, forage ...... 2 .0 tions. [Reserved] Grain, cereal, forage, fodder and straw, group (d) Indirect or inadvertent residues. 16, straw ...... 3 .0 [Reserved] Grain, cereal, group 15 ...... 0.20 Grass, forage, fodder, and hay, group 17, for- [71 FR 52011, Sept. 1, 2006] age ...... 2 .0 Grass, forage, fodder, and hay, group 17, hay ... 8 .0 Grass, forage, fodder, and hay, group 17, seed § 180.591 Trifloxysulfuron; tolerances screenings ...... 0 .20 for residues. Grass, forage, fodder, and hay, group 17, straw 0 .30 (a) General. Tolerances are estab- Lupin, grain, grain ...... 0 .1 Pea, field, seed ...... 0 .1 lished for residues of the herbicide Radish, roots ...... 0 .1 trifloxysulfuron, N-[[(4,6-dimethoxy-2-

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pyrimidinyl)amino]carbonyl]-3-(2,2,2- (b) Section 18 emergency exemptions. trifluoroethoxy)-2-pyridinesulfonamide [Reserved] in or on the following raw agricultural (c) Tolerances with regional registra- commodities. tions. [Reserved] (d) Indirect and inadvertant residues. Parts per Commodity million [Reserved]

Almond ...... 0.02 [68 FR 54827, Sept. 19, 2003] Almond, hulls ...... 0 .01 Fruit, citrus, Group 10 ...... 0.03 § 180.593 Etoxazole; tolerances for resi- Cotton, undelinted seed ...... 0 .05 Cotton, gin byproducts ...... 1 .0 dues. Sugarcane ...... 0 .01 (a) General. Tolerances are estab- Tomato ...... 0.01 lished for residues of the insecticide (b) Section 18 emergency exemptions. etoxazole, 2-(2,6-difluorophenyl)-4-[4- [Reserved] (1,1-dimethylethyl)-2-ethoxyphenyl]- (c) Tolerances with regional registra- 4,5-dihydrooxazole, in or on the fol- tions. [Reserved] lowing raw agricultural commodities: (d) Indirect or inadvertent residues. Parts per [Reserved] Commodity million

[68 FR 54386, Sept. 17, 2003] Almond, hulls ...... 2 .0 Apple, wet pomace ...... 0 .50 § 180.592 Butafenacil; tolerances for Cattle, fat ...... 0.02 residues. Cattle, liver ...... 0 .01 (a) General. (1) Tolerances are estab- Cotton, gin byproducts ...... 1 .0 lished for residues of the herbicide Cotton, undelinted seed ...... 0 .05 Fruit, pome, group 11 ...... 0.20 butafenacil, (1,1-dimethyl-2-oxo-2-(2- Goat, fat ...... 0 .02 propenyloxy)ethyl 2-chloro-5-[3,6- Goat, liver ...... 0.01 dihydro-3-methyl-2,6-dioxo-4- Grape ...... 0 .50 (trifluoromethyl)-1(2H)-pyrimidinyl] Grape, raisin ...... 1 .5 benzoate) in or on the following raw Horse, fat ...... 0 .02 Horse, liver ...... 0 .01 agricultural commodities: Milk, fat ...... 0 .01 Nut, tree, group 14 ...... 0 .01 Parts per Commodity million Pistachio ...... 0.01 Sheep, fat ...... 0 .02 Cotton, gin byproducts ...... 10 Sheep, liver ...... 0.01 Cotton, undelinted seed ...... 0 .50 Strawberry ...... 0 .50 Tangerine1 ...... 0 .10 (2) Tolerances are established for res- 1There are no U.S. registrations for use of etoxazole on idues of the herbicide butafenacil, (1,1- tangerines as of September 26, 2003. dimethyl-2-oxo-2-(2-propenyloxy)ethyl (b) Section 18 emergency exemptions. 2-chloro-5-[3,6-dihydro-3-methyl-2,6- [Reserved] dioxo-4-(trifluoromethyl)-1(2H)- (c) Tolerances with regional registra- pyrimidinyl] benzoate) and its metabo- tions. [Reserved] lite CGA-293731 (1-carboxy-1- methylethyl 2-chloro-5-[3,6-dihydro-3- (d) Indirect and inadvertant residues. methyl-2,6-dioxo-4-(trifluoromethyl)- [Reserved] 1(2H)-pyrimidinyl] benzoate), in or on [68 FR 55493, Sept. 26, 2003, as amended at 70 the following livestock commodities: FR 41625, July 20, 2005]

Commodity Parts per § 180.594 Thiacloprid; tolerances for million residues. Cattle, kidney ...... 0 .05 Cattle, liver ...... 0 .50 (a) General. Tolerances for combined Goat, kidney ...... 0 .05 residues of the insecticide thiacloprid Goat, liver ...... 0.50 ([3-[(6-chloro-3-pyridinyl)methyl]-2- Hog, kidney ...... 0.05 thiazolidinylidene] cyanamide) and me- Hog, liver ...... 0 .50 Horse, kidney ...... 0 .05 tabolites retaining the thiazolidine Horse, liver ...... 0 .50 ring intact, measured and expressed in Sheep, kidney ...... 0.05 terms of thiacloprid, per se, in or on the Sheep, liver ...... 0.50 following commodities:

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Parts per Parts per Commodity million Commodity million

Apple, wet pomace ...... 0.60 Corn, field, forage ...... 0 .05 Cattle, fat ...... 0.020 Corn, field, stover ...... 0 .05 Cattle, kidney ...... 0.050 Cattle, liver ...... 0.15 (b) Section 18 emergency exemptions. Cattle, meat ...... 0.030 Cattle, meat byproducts ...... 0.050 [Reserved] Cotton, gin byproducts ...... 11.0 (c) Tolerances with regional registra- Cotton, undelinted seed ...... 0.020 tions. [Reserved] Fruit, pome, group 11 ...... 0.30 (d) Indirect or inadvertent residues. Goat, fat ...... 0.020 Goat, kidney ...... 0.050 [Reserved] Goat, liver ...... 0.15 [68 FR 54842, Sept. 19, 2003] Goat, meat ...... 0.030 Goat, meat byproducts ...... 0.050 Horse, fat ...... 0.020 § 180.596 Fosthiazate; tolerances for Horse, kidney ...... 0.050 residues. Horse, liver ...... 0.15 (a) General. Tolerances are estab- Horse, meat ...... 0.030 Horse, meat byproducts ...... 0.050 lished for the combined residues of Milk ...... 0.030 Fosthiazate (O-ethyl S-(1- Sheep, fat ...... 0.020 methylpropyl)(2-oxo-3- Sheep, kidney ...... 0.050 thiazolidinyl)phosphonothioate and its Sheep, liver ...... 0.15 metabolite O-ethyl S-(1- Sheep, meat ...... 0.030 Sheep, meat byproducts ...... 0.050 methylpropyl)[2-(methylsulfonyl)ethyl] phosphoramidothioate) (ASC–67131). (b) Section 18 emergency exemptions. Parts per [Reserved] Commodity million (c) Tolerances with regional registra- tions. [Reserved] Tomato ...... 0.02 (d) Indirect or inadvertent residues. [Reserved] (b) Section 18 emergency exemptions. [Reserved] [68 FR 55512, Sept. 26, 2003] (c) Tolerances with regional registra- tions. [Reserved] § 180.595 Flufenpyr-ethyl; tolerances (d) Indirect or inadvertent residues. for residues. [Reserved] (a) General. (1) Tolerances are estab- lished for residues of the herbicide, [69 FR 18275, Apr. 7, 2004] flufenpyr-ethyl; acetic acid, [2-chloro- § 180.597 Mesosulfuron-methyl; toler- 4-fluoro-5-[5-methyl-6-oxo-4- ances for residues. (trifluoromethyl)-1-(6H)-pyridazinyl]- phenoxy]-ethyl ester], in or on the fol- (a) General. Tolerances are estab- lowing commodities: lished for residues of the herbicide mesosulfuron-methyl, (methyl 2-[[[[ Commodity Parts per (4,6-dimethoxy-2-pyrimidinyl) million amino]carbonyl]amino]sulfonyl] -4- Corn, field, grain ...... 0 .01 [[(methylsulfonyl)amino] meth- Soybean, seed ...... 0 .01 yl]benzoate]) in or on the following raw Sugarcane, cane ...... 0.01 agricultural commodities:

(2) Tolerances are established for res- Commodity Parts per idues of the herbicide flufenpyr-ethyl; million acetic acid, [2-chloro-4-fluoro-5-[5- Cattle, meat byproducts ...... 0.01 methyl-6-oxo-4-(trifluoromethyl)-1- Goat, meat byproducts ...... 0 .01 (6H)-pyridazinyl]-phenoxy]-ethyl Grain, aspirated fractions ...... 0 .60 ester], and its metabolite, S-3153 acid- Horse, meat byproducts ...... 0 .01 Sheep, meat byproducts ...... 0 .01 4-OH; [2-chloro-4-hydroxy-5-[5-methyl- Wheat, forage ...... 0 .60 6- oxo-4-(trifluoromethyl)-1-(6H)- Wheat, germ ...... 0 .10 pyridazinyl]-phenoxy]-acetic acid, free Wheat, grain ...... 0 .03 and conjugated, in or on the following Wheat, hay ...... 0 .06 commodities: Wheat, straw ...... 0 .30

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(b) Section 18 emergency exemptions. voked on the date specified in the fol- [Reserved] lowing table: (c) Tolerances with regional registra- Expiration/ tions. [Reserved] Commodity Parts per revocation (d) Indirect or inadvertent residues. million date [Reserved] Sugarcane, cane ...... 0.15 12/31/09 [69 FR 18263, Apr. 7, 2004] (c) Tolerances with regional registra- § 180.598 Novaluron; tolerances for tions. [Reserved] residues. (d) Indirect or inadvertant residues. (a) General. Tolerances are estab- [Reserved] lished for residues of the insecticide [69 FR 31021, June 2, 2004, as amended at 71 novaluron, 1-[3-chloro-4-(1,1,2-trifluoro- FR 17014, Apr. 5, 2006; 71 FR 61911, Oct. 20, 2-trifluoro-methoxyethoxy)phenyl]-3- 2006] (2,6-difluorobenzoyl)urea, in or on the following raw agricultural commod- § 180.599 Acequinocyl; tolerances for ities: residues. (a) General. Tolerances for combined Parts per residues of the insecticide acequinocyl, Commodity million 2-(acetyloxy)-3-dodecyl-1,4- Apple, wet pomace ...... 8 .0 naphthalenedione, and its metabolite, Brassica, head and stem, subgroup 5A ...... 0 .50 2-dodecyl-3-hydroxy-1,4- Cattle, fat ...... 11 Cattle, kidney ...... 1 .0 naphthoquinone, expressed as Cattle, liver ...... 1 .0 acequinocyl equivalents in or on the Cattle, meat ...... 0 .60 following commodities: Cattle, meat byproducts, except liver and kidney 0.60 Cotton, gin byproducts ...... 30 Commodity Parts per Cotton, undelinted seed ...... 0 .60 million Egg ...... 0 .05 Fruit, pome, group 11 ...... 2.0 Almond ...... 0.02 Goat, fat ...... 11 Almond, hulls ...... 2 .0 Goat, kidney ...... 1 .0 Apple, wet pomace ...... 1 .0 Goat, liver ...... 1.0 Cattle, fat ...... 0.02 Goat, meat ...... 0.60 Cattle, liver ...... 0 .02 Goat, meat byproducts except liver and kidney .. 0 .60 Citrus, oil ...... 30 Hog, fat ...... 0 .05 Fruit, citrus, group 10 ...... 0 .20 Fruit, pome, group 11 ...... 0.40 Hog, meat ...... 0 .01 Goat, fat ...... 0 .02 Hog, meat byproducts ...... 0 .01 Goat, liver ...... 0.02 Horse, fat ...... 11 Horse, fat ...... 0 .02 Horse, kidney ...... 1 .0 Horse, liver ...... 0 .02 Horse, liver ...... 1 .0 Pistachio ...... 0.02 Horse, meat ...... 0 .60 Sheep, fat ...... 0 .02 Horse, meat byproducts, except liver and kidney 0 .60 Sheep, liver ...... 0.02 Milk ...... 1.0 Strawberry ...... 0 .40 Milk, fat ...... 20 Poultry, fat ...... 0.40 Poultry, meat ...... 0 .03 (b) Section 18 emergency exemptions. Poultry, meat byproducts ...... 0.04 [Reserved] Sheep, fat ...... 11 (c) Tolerances with regional registra- Sheep, kidney ...... 1.0 tions. [Reserved] Sheep, liver ...... 1.0 Sheep, meat ...... 0.60 (d) Indirect or inadvertent residues. Sheep, meat byproducts, except liver and kid- [Reserved] ney ...... 0.60 Vegetables, tuberous and corn, subgroup 1C .... 0.05 [69 FR 43533, July 21, 2004]

(b) Section 18 emergency exemptions. A § 180.600 Propoxycarbazone; toler- time-limited tolerance is established ances for residues for residues of the fungicide novaluron, (a) General. (1) Tolerances are estab- 1-[3-chloro-4-(1,1,2-trifluoro-2- lished for combined residues of the her- trifluoromethoxyethoxy) phenyl]-3-[2,6- bicide propoxycarbazone methyl 2- diflurobenzoyl]urea in connection with [[[(4,5-dihydro-4-methyl-5-oxo-3- use of the pesticide under a section 18 propoxy-1H-1,2,4-triazol-1- emergency exemption granted by EPA. yl)carbonyl]amino]sulfonyl]benzoate The tolerance will expire and is re- and its metabolite methyl 2-[[[(4,5-

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dihydro-3-(2-hydroxypropoxy)-4-meth- (b) Section 18 emergency exemptions. yl-5-oxo-1H-1,2,4-triazol-1- [Reserved] yl)carbonyl]amino]sulfonyl]benzoate (c) Tolerances with regional registra- in/on the following raw agricultural tions. [Reserved] commodities: (d) Indirect or inadvertent residues. [Reserved] Parts per Commodity million [69 FR 58299, Sept. 30, 2004]

Wheat, forage ...... 17 § 180.602 Spiroxamine; tolerances for Wheat, grain ...... 0 .02 residues. Wheat, hay ...... 0 .15 Wheat, straw ...... 0 .05 (a) General. Tolerances are estab- lished for the combined residues of the (2) Tolerances are established for res- fungicide spiroxamine (8-(1,1- idues of the herbicide dimethylethyl)-N-ethyl-N-propyl-1,4- propoxycarbazone methyl 2-[[[(4,5- dioxaspiro[4,5]decane-2-methanamine) dihydro-4-methyl-5-oxo-3-propoxy-1H- and its metabolites containing the N- 1,2,4-triazol-1- ethyl-N-propyl-1,2-dihydroxy-3- yl)carbonyl]amino]sulfonyl]benzoate aminopropane moiety, calculated as in/on the following raw agricultural parent equivalent, in or on the fol- commodities: lowing raw agricultural commodities:

Commodity Parts per Parts per million Commodity million

Cattle, meat ...... 0 .05 Banana (import) ...... 3 .0 Cattle, meat byproducts ...... 0.3 Grape (import) ...... 1 .0 Goat, meat ...... 0.05 Hop, dried cones ...... 50 Goat, meat byproducts ...... 0 .3 Horse, meat ...... 0 .05 (b) Section 18 emergency exemptions. Horse, meat byproducts ...... 0 .3 [Reserved] Milk ...... 0.03 Sheep, meat ...... 0.05 (c) Tolerances with regional registra- Sheep, meat byproducts ...... 0 .3 tions. [Reserved] (d) Indirect or inadvertent residues. (b) Section 18 emergency exemptions. [Reserved] [Reserved] [69 FR 42570, July 16, 2004] (c) Tolerances with regional registra- tions. [Reserved] § 180.603 Dinotefuran; tolerances for (d) Indirect or inadvertent residues. residues. [Reserved] (a) General. (1) Tolerances are estab- [69 FR 40781, July 7, 2004, as amended at 71 lished for the combined residues of FR 52487, Sept. 6, 2006] Dinotefuran, [N-methyl-N′-nitro-N′′- ((tetrahydro-3- § 180.601 Cyazofamid; tolerances for furanyl)methyl)guanidine] and its me- residues. tabolites DN [1-methyl-3-(tetrahydro-3- (a) General. Tolerances are estab- furylmethyl)guanidine] and UF [1- lished for the combined residues of methyl-3-(tetrahydro-3- cyazofamid, 4-chloro-2-cyano-N,N-di- furylmethyl)urea], expressed as methyl-5-(4-methylphenyl)-1H-imid- dinotefuran. azole-1-sulfonamide, and its metabolite Parts per CCIM, 4-chloro-5-(4-methylphenyl)-1H- Commodity million imidazole-2-carbonitrile, expressed as cyazofamid, in or on the following Brassica, head and stem, subgroup 5A ...... 1 .4 Cotton, undelinted seed ...... 0 .4 commodities: Cotton, gin byproducts ...... 8 .0 Grape ...... 0 .9 Commodity Parts per Grape, raisin ...... 2 .5 million Potato ...... 0 .05 Potato, chips ...... 0 .1 Cucurbit vegetables (Group 9) ...... 0 .10 Potato, granules/flakes ...... 0 .15 Grape, wine,* import ...... 1 .5 Tomato, paste ...... 1 .0 Potato ...... 0 .02 Vegetable, fruiting, group 8 ...... 0.7 Tomato ...... 0.20 Vegetable, cucubit, group 9 ...... 0 .5 Vegetable, leafy, except Brassica, group 4 ...... 5 .0 *No domestic registrations.

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(2) Tolerances are established for res- § 180.605 Penoxsulam; tolerances for idues of dinotefuran N-methyl-N′-nitro- residues. ′′ N -tetrahydro-3- (a) General. Tolerances are estab- furanyl)methyl)guanidine in/on the fol- lished for the herbicide, penoxsulam ( lowing commodities: 2-(2,2-difluoroethoxy)-N-(5,8- Parts per dimethoxy[1,2,4] triazolo[1,5- Commodity million c]pyrimidin-2-yl)-6- (trifluoromethyl)benzenesulfonamide) Cattle, fat ...... 0.05 in/on the following raw agricultural Cattle, mbyp ...... 0 .05 Cattle, meat ...... 0 .05 commodities: Goat, fat ...... 0 .05 Goat, mbyp ...... 0 .05 Parts per Commodity million Goat, meat ...... 0.05 Hog, fat ...... 0 .05 Rice, grain ...... 0 .02 Hog, mbyp ...... 0 .05 Rice, straw ...... 0 .50 Hog, meat ...... 0 .05 Horse, fat ...... 0 .05 (b) Section 18 emergency exemptions. Horse, mbyp ...... 0 .05 Horse, meat ...... 0 .05 [Reserved] Milk ...... 0.05 (c) Tolerances with regional registra- Sheep, fat ...... 0 .05 tions. [Reserved] Sheep, mbyp ...... 0 .05 (d) Indirect or inadvertent residues. Sheep, meat ...... 0.05 [Reserved] (b) Section 18 emergency exemptions. [69 FR 57197, Sept. 24, 2004] [Reserved] (c) Tolerances with regional registra- § 180.607 Spiromesifen; tolerances for residues. tions. [Reserved] (d) Indirect or inadvertent residues. (a) General. (1) Tolerances are estab- [Reserved] lished for the combined residues of spiromesifen (2-oxo-3-(2,4,6- [70 FR 14546, Mar. 23, 2005] trimethylphenyl)-1-oxaspiro[4.4]non-3- en-4-yl 3,3-dimethylbutanoate) and its § 180.604 Mepanipyrim; tolerances for enol metabolite (4-hydroxy-3-(2,4,6- residues. trimethylphenyl)-1-oxaspiro[4.4]non-3- (a) General. [Reserved] en-2-one), calculated as the parent (b) Section 18 emergency exemptions. compound equivalents in or on the fol- [Reserved] lowing primary crop commodities: (c) Tolerances with regional registra- Parts per tions. [Reserved] Commodity million (d) Indirect of inadvertent residues. [Reserved] Brassica, head and stem, subgroup 5A ...... 2 .0 Corn, field, forage ...... 3 .0 (e) Revoked tolerances subject to the Corn, field, grain ...... 0 .02 channel of trade provisions. [Reserved] Corn, field, stover ...... 5 .0 Cotton, gin byproducts ...... 15 (f) Import tolerances. Tolerances are Cotton, undelinted seed ...... 0 .50 established for the combined residues Strawberry ...... 2 .0 of mepanipyrim, 4-methyl-N-phenyl-6- Tomato, paste ...... 0 .60 (1-propynyl)-2-pyrimidinamine, and its Vegetable, brassica, leafy greens, subgroup 5B 12 Vegetable, cucurbit, group 9 ...... 0.10 metabolite, 4-methyl-N-phenyl-6-(2- Vegetable, fruiting, group 8 ...... 0.45 hydroxypropylk)-2-pyrimidinamine, Vegetable, leafy greens, subgroup 4A ...... 12 both free and conjugated in or on the Vegetable, tuberous and corm, subgroup 1C ..... 0.02 following commodities: (2) Tolerances are established for the Commodity Parts per combined residues of spiromesifen (2- million oxo-3-(2,4,6-trimethylphenyl)-1- Grape ...... 1 .5 oxaspiro[4.4]non-3-en-4-yl 3,3- Grape, raisin ...... 3 .0 dimethylbutanoate), and its metabo- Strawberry ...... 1 .5 lites containing the enol (4-hydroxy-3- Tomato ...... 0.5 (2,4,6-trimethylphenyl)-1- oxaspiro[4.4]non-3-en-2-one) and 4- [68 FR 60827, Oct. 13, 2004] hydroxymethyl (4-hydroxy-3-[4-

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(hydroxymethyl)-2,6-dimethylphenyl]- dimethylbutanoate) in or on the fol- 1-oxaspiro[4.4]non-3-en-2-one) moieties, lowing plant commodities: calculated as the parent compound Parts per equivalents in the following livestock Commodity million commodities: Almond, hulls ...... 20 .0 Parts per Apple, wet pomace ...... 2 .0 Commodity million Citrus, juice ...... 0 .60 Citrus, oil ...... 20.0 Cattle, fat ...... 0.05 Fruit, citrus, group 10 ...... 0 .50 Cattle, meat byproducts ...... 0.05 Fruit, pome, group 11 ...... 0.80 Goat, fat ...... 0 .05 Fruit, stone, group 12 ...... 1 .0 Goat, meat byproducts ...... 0 .05 Grape ...... 2 .0 Horse, fat ...... 0 .05 Grape, juice ...... 2 .4 Horse, meat byproducts ...... 0 .05 Grape, raisin ...... 4 .0 Milk, fat ...... 0 .10 Nut, tree, group 14 ...... 0 .10 Sheep, fat ...... 0 .05 Pistachio ...... 0.10 Sheep, meat byproducts ...... 0 .05 (2) Tolerances are established for res- (b) Section 18 emergency exemptions. idues of spirodiclofen (3-(2,4- [Reserved] dichlorophenyl)-2-oxo-1- (c) Tolerances with regional registra- oxaspiro[4.5]dec-3-en-4-yl 2,2- tions. [Reserved] dimethylbutanoate) and its free enol (d) Indirect or inadvertent residues. metabolite BAJ 2510 (3-(2,4- Tolerances are established for the inad- dichlorophenyl)-4-hydroxy-1- vertent or indirect combined residues oxaspiro[4,5]dec-3-en-2-one) in or on the of spiromesifen (2-oxo-3-(2,4,6- following livestock commodities: trimethylphenyl)-1- oxaspiro[4.4]non-3- en-4-yl 3,3-dimethylbutanoate), its enol Commodity Parts per metabolite (4-hydroxy-3-(2,4,6- million trimethylphenyl)-1-oxaspiro[4.4]non-3- Cattle, fat ...... 0.02 en-2-one), and its metabolites con- Cattle, meat byproducts ...... 0.10 taining the 4-hydroxymethyl moiety (4- Cattle, meat ...... 0 .02 Goat, fat ...... 0 .02 hydroxy-3-[4-(hydroxymethyl)-2,6- Goat, meat byproducts ...... 0 .1 dimethylphenyl]-1-oxaspiro[4.4]non-3- Goat, meat ...... 0.02 en-2-one), calculated as the parent Horse, fat ...... 0 .02 Horse, meat byproducts ...... 0 .1 compound equivalents in the following Horse, meat ...... 0 .02 rotational crop commodities: Milk ...... 0.01 Milk, fat ...... 0 .03 Sheep, fat ...... 0 .02 Commodity Parts per million Sheep. meat byproducts ...... 0 .1 Sheep. meat ...... 0.02 Alfalfa, forage ...... 1.5 Alfalfa, hay ...... 3.0 Barley, grain ...... 0 .03 (b) Section 18 emergency exemptions. Barley, hay ...... 0 .25 [Reserved] Barley, straw ...... 0 .15 (c) Tolerances with regional registra- Beet, sugar, roots ...... 0 .03 Beet, sugar, tops ...... 0.20 tions. [Reserved] Oat, forage ...... 0 .20 (d) Indirect or inadvertent residues. Oat, grain ...... 0 .03 [Reserved] Oat, hay ...... 0.25 Oat, straw ...... 0.25 [70 FR 40211, July 13, 2005] Wheat, forage ...... 0 .20 Wheat, grain ...... 0 .03 Wheat, hay ...... 0 .15 § 180.609 Fluoxastrobin; tolerances for Wheat, straw ...... 0 .25 residues. (a) General. (1) Tolerances are estab- [70 FR 43283, July 27, 2005, as amended at 72 lished for the combined residues of FR 3079, Jan. 24, 2007] fluoxastrobin, (1E)-[2-[[6-(2- chlorophenoxy)-5-fluoro-4- § 180.608 Spirodiclofen; tolerances for pyrimydinyl]oxy]phenyl](5,6-dihydro- residues. 1,4,2-dioxazin-3-yl)methanone O- (a) General. (1) Tolerances are estab- methyloxime, and its Z isomer, (1Z)-[2- lished for residues of spirodiclofen per [[6-(2-chlorophenoxy)-5-fluoro-4- se (3-(2,4-dichlorophenyl)-2-oxo-1- pyrimydinyl]oxy]phenyl](5,6-dihydro- oxaspiro[4.5]dec-3-en-4-yl 2,2- 1,4,2-dioxazin-3-yl)methanone O-

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methyloxime, in or on the following crops listed in paragraph (a)(1) of this raw agricultural commodities: section:

Commodity Parts per Parts per million Commodity million

Leaf petioles subgroup 4B ...... 4 .0 Alfalfa, forage ...... 0.050 Peanut ...... 0 .010 Alfalfa, hay ...... 0.10 Peanut, hay ...... 20.0 Cotton, gin byproducts ...... 0 .020 Peanut, refined oil ...... 0.030 Grain, cereal, forage, fodder, and straw, group Tomato, paste ...... 1 .5 16 ...... 0 .10 Vegetable, fruiting, group 8 ...... 1.0 Vegetable, tuberous and corm, subgroup 1C ..... 0.010 Grass, forage ...... 0 .10 Grass, hay ...... 0 .50 (2) Tolerances are established for the Vegetable, foliage of legume, group 7 ...... 0 .050 combined residues of fluoxastrobin, (1E)-[2-[[6-(2-chlorophenoxy)-5-fluoro-4- [70 FR 54650, Sept. 16, 2005] pyrimydinyl]oxy]phenyl](5,6-dihydro- 1,4,2-dioxazin-3-yl)methanone O- § 180.610 Aminopyralid; tolerances for residues. methyloxime, its Z isomer, (1Z)-[2-[[6- (2-chlorophenoxy)-5-fluoro-4- (a) General. (1) Tolerances are estab- pyrimydinyl]oxy]phenyl](5,6-dihydro- lished for free and conjugated residues 1,4,2-dioxazin-3-yl)methanone O- of the herbicide, aminopyralid (2-pyri- methyloxime, and its phenoxy- dine carboxylic acid, 4-amino-3,6- hydroxypyrimidine metabolite, 6-(2- dichloro-) calculated as aminopyralid chlorophenoxy)-5-fluoro-4-pyrimidinol, in or on: in or on the following raw agricultural Parts per commodities: Commodity million

Commodity Parts per Grass, forage ...... 25 million Grass, hay ...... 50 Cattle, fat ...... 0.10 Wheat, bran ...... 0.1 Cattle, meat ...... 0 .05 Wheat, forage ...... 2 .0 Cattle, meat byproducts ...... 0.10 Wheat, grain ...... 0 .04 Goat, fat ...... 0 .10 Wheat, hay ...... 4 .0 Goat, meat ...... 0.05 Wheat, straw ...... 0 .25 Goat, meat byproducts ...... 0 .10 Aspirated grain fractions ...... 0 .2 Horse, fat ...... 0 .10 Horse, meat ...... 0 .05 (2) Tolerances are established for res- Horse, meat byproducts ...... 0 .10 Milk ...... 0.02 idues of the herbicide aminopyralid in Milk, fat ...... 0 .50 or on: Sheep, fat ...... 0 .10 Sheep, meat ...... 0.05 Commodity Parts per Sheep, meat byproducts ...... 0 .10 million

(b) Section 18 emergency exemptions. Cattle, fat ...... 0.02 Cattle, meat ...... 0 .02 [Reserved] Cattle, meat byproducts, excluding kidney ...... 0 .02 (c) Tolerances with regional registra- Cattle, kidney ...... 0 .3 tions. [Reserved] Goat, fat ...... 0 .02 (d) Indirect or inadvertent residues. Goat, meat ...... 0.02 Tolerances are established for the indi- Goat, meat byproducts, excluding kidney ...... 0 .02 Goat, kidney ...... 0 .3 rect or inadvertent combined residues Horse, fat ...... 0 .02 of fluoxastrobin, (1E)-[2-[[6-(2- Horse, meat ...... 0 .02 chlorophenoxy)-5-fluoro-4- Horse, meat byproducts, excluding kidney ...... 0 .02 pyrimydinyl]oxy]phenyl](5,6-dihydro- Horse, kidney ...... 0 .3 1,4,2-dioxazin-3-yl)methanone O- Milk ...... 0.03 Sheep, fat ...... 0 .02 methyloxime, and its Z isomer, (1Z)-[2- Sheep, meat ...... 0.02 [[6-(2-chlorophenoxy)-5-fluoro-4- Sheep, meat byproducts, excluding kidney ...... 0.02 pyrimydinyl]oxy]phenyl](5,6-dihydro- Sheep, kidney ...... 0.3 1,4,2-dioxazin-3-yl)methanone O- methyloxime, in or on the following (b) Section 18 emergency exemptions. raw agricultural commodities when [Reserved] present therein as a result of the appli- (c) Tolerances with regional registra- cation of fluoxastrobin to the growing tions. [Reserved]

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(d) Indirect or inadvertent residues. (b) Section 18 emergency exemptions. [Reserved] [Reserved] (c) Tolerances with regional registra- [70 FR 46428, Aug. 10, 2005] tions. [Reserved] § 180.611 Pinoxaden; tolerances for (d) Indirect or inadvertent residues. residues. [Reserved] (a) General. (1) Tolerances are estab- [70 FR 43322, July 27, 2005] lished for the combined residues of pinoxaden (8-(2,6-diethyl-4- § 180.612 Topramezone; tolerances for methylphenyl)-1,2,4,5-tetrahydro-7-oxo- residues. 7H-pyrazolo[1,2-d][1,4,5] oxadiazepin-9- (a) General. (1) Tolerances are estab- yl 2,2-dimethylpropanoate), and its me- lished for residues of the herbicide tabolites 8-(2,6-diethyl-4-methyl- topramezone, [3-(4,5-dihydro-3- phenyl)-tetrahydro-pyrazolo[1,2- isoxazolyl)-2-methyl-4- d][1,4,5]oxadiazepine-7,9-dione (M2), and (methylsulfonyl)phenyl](5-hydroxy-1- free and conjugated forms of 8-(2,6- methyl-1H-pyrazol-4-yl)methanone, in diethyl-4-hydroxymethyl-phenyl)- or on the following raw agricultural tetrahydro-pyrazolo[1,2-d][1,4,5] commodities: oxadiazepine-7,9-dione (M4), and 4-(7,9- dioxo-hexahydro-pyrazolo[1,2-d] Parts per Commodity million [1,4,5]oxadiazepin-8-yl)-3,5-diethyl-ben- zoic acid (M6), calculated as pinoxaden, Cattle, kidney ...... 0 .05 in/on the following commodities: Cattle, liver ...... 0 .15 Corn, field, forage ...... 0 .05 Parts per Corn, field, grain ...... 0 .01 Commodity million Corn, field, stover ...... 0 .05 Corn, pop, grain ...... 0.01 Barley, bran ...... 1 .6 Corn, pop, stover ...... 0.05 Barley, grain ...... 0 .9 Corn, sweet, forage ...... 0 .05 Barley, hay ...... 1 .5 Corn, sweet, kernel plus cob with husks re- Barley, straw ...... 1 .0 moved ...... 0 .01 Egg ...... 0 .06 Corn, sweet, stover ...... 0 .05 Poultry, fat ...... 0.06 Goat, kidney ...... 0 .05 Poultry, meat ...... 0 .06 Goat, liver ...... 0.15 Poultry, meat byproducts ...... 0.06 Horse, kidney ...... 0 .05 Wheat, bran ...... 3.0 Horse, liver ...... 0 .15 Wheat, forage ...... 3 .5 Sheep, kidney ...... 0.05 Wheat, grain ...... 1 .3 Sheep, liver ...... 0.15 Wheat, hay ...... 2 .0 Wheat, straw ...... 1 .5 (b) Section 18 emergency exemptions. [Reserved] (2) For the combined residues of (c) Tolerances with regional registra- pinoxaden, 8-(2,6-diethyl-4- tions. [Reserved] methylphenyl)-1,2,4,5-tetrahydro-7-oxo- (d) Indirect or inadvertent residues. 7H-pyrazolo[1,2-d][1,4,5] oxadiazepin-9- [Reserved] yl 2,2-dimethylpropanoate), and its me- tabolites M2, 8-(2,6-diethyl-4-methyl- [70 FR 46419, Aug. 10, 2005] phenyl)-tetrahydro-pyrazolo[1,2- § 180.613 Flonicamid; tolerances for d][1,4,5]oxadiazepine-7,9-dione, and free residues. and conjugated forms of M4, 8-(2,6- diethyl-4-hydroxymethyl-phenyl)- (a) General. (1) Tolerances are estab- tetrahydro-pyrazolo[1,2-d][1,4,5] lished for the combined residues of oxadiazepine-7,9-dione, calculated as flonicamid [N-(cyanomethyl)-4- pinoxaden, in/on the following com- (trifluoromethyl)-3- modities: pyridinecarboxamide] and its metabo- lites TFNA [4-trifluoromethylnicotinic Commodity Parts per acid], TFNA-AM [4- million trifluoromethylnicotinamide] TFNG Cattle, fat ...... 0.04 [N-(4- Cattle, meat ...... 0 .04 trifluoromethylnicotinoyl)glycine] in Cattle, meat byproducts ...... 0.04 or on the following raw agricultural Milk ...... 0.02 commodities:

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hexopyranosyl]-D-chiro-inositol in or Commodity Parts per million on the following raw agricultural com- Brassica, head and stem, subgroup 5A ...... 1 .5 modity: Cotton, gin byproducts ...... 6 .0 Cotton, hulls ...... 2 .0 Commodity Parts per Cotton, meal ...... 1 .0 million Cotton, undelinted seed ...... 0 .50 Vegetable, fruiting group 81 ...... 0 .04 Fruit, pome, group 11 ...... 0.20 Fruit, stone, group 12 ...... 0 .60 1There is no U.S. registration as of September 1, 2005. Mustard greens ...... 11 Potato ...... 0 .20 (b) Section 18 emergency exemptions. Potato, granular/flakes ...... 0 .40 [Reserved] Spinach ...... 9 .0 (c) Tolerances with regional registra- Tomato, paste ...... 2 .0 Tomato, puree ...... 0 .50 tions. [Reserved] Vegetable, cucurbit, group ...... 0 .40 (d) Indirect or inadvertent residues. Vegetable, fruiting, group ...... 0 .40 [Reserved] Vegetable, leafy except Brassica group 4, ex- cept spinach ...... 4 .0 [70 FR 55752, Sept. 23, 2005]

(2) Tolerances are established for § 180.615 Amicarbazone; tolerances for combined residues of flonicamid [N- residues. (cyanomethyl)-4-(trifluoromethyl)-3- (a) General. Tolerances are estab- pyridinecarboxamide], and its metabo- lished for combined residues of the her- lites TFNA [4-trifluoromethylnicotinic bicide, amicarbazone [4-amino-4, 5- acid], TFNA-AM [4- dihydro- N-(1,1-dimethylethyl)-3-(1- trifluoromethylnicotinamide] in or on methylethyl)-5-oxo-1H-1,2,4-triazole-1- the following raw agricultural com- carboxamide] and its metabolites DA modities: amicarbazone [N-(1,1-dimethylethyl)- 4,5-dihydro-3-(1-methylethyl)-5-oxo-1H- Parts per Commodity million 1,2,4-triazole-1-carboxamide] and iPr-2- OH DA amicarbazone [N-(1,1- Cattle, fat ...... 0.02 Cattle, meat ...... 0 .05 dimethylethyl)-4,5-dihydro-3-(1-hy- Cattle, meat byproducts ...... 0.08 droxy-1-methylethyl)-5-oxo-1H-1,2,4-tri- Egg ...... 0 .03 azole-1-carboxamide], calculated as Goat, fat ...... 0 .02 parent equivalents, in or on the fol- Goat, meat ...... 0.05 Goat, meat byproducts ...... 0 .08 lowing commodities: Horse, fat ...... 0 .02 Horse, meat ...... 0 .05 Commodity Parts per Horse, meat byproducts ...... 0 .08 million Milk ...... 0.02 Cattle, fat ...... 0.01 Poultry, fat ...... 0.02 Cattle, liver ...... 1 .0 Poultry, meat ...... 0 .02 Cattle, meat ...... 0 .01 Poultry, meat byproducts ...... 0.02 Cattle, meat byproducts, except liver ...... 0 .10 Sheep, fat ...... 0 .02 Corn, field, forage ...... 0 .80 Sheep, meat ...... 0.05 Corn, field, grain ...... 0 .05 Sheep, meat by products ...... 0.08 Corn, field, stover ...... 1 .0 Goat, fat ...... 0 .01 (b) Section 18 emergency exemptions. Goat, liver ...... 1.0 [Reserved] Goat, meat ...... 0.01 Goat, meat byproducts, except liver ...... 0 .10 (c) Tolerances with regional registra- Hog, fat ...... 0 .01 tions. [Reserved] Hog, liver ...... 0 .10 (d) Indirect or inadvertent residues. Hog, meat ...... 0 .01 [Reserved] Hog, meat byproducts, except liver ...... 0 .01 Horse, fat ...... 0 .01 [70 FR 51614, Aug. 31, 2005, as amended at 71 Horse, liver ...... 1 .0 FR 15608, Mar. 29, 2006] Horse, meat ...... 0 .01 Horse, meat byproducts, except liver ...... 0 .10 Milk ...... 0.01 § 180.614 Kasugamycin; tolerances for Sheep, fat ...... 0 .01 residues. Sheep, liver ...... 1.0 Sheep, meat ...... 0.01 (a) General. Tolerances are estab- Sheep, meat byproducts, except liver ...... 0 .10 lished for residues of kasugamycin, 3- Poultry, liver ...... 0 .10 O-[2-amino-4- [(carboxyiminomethyl)amino]-2,3,4,6- (b) Section 18 emergency exemptions. tetradeoxy-a-D-arabino- [Reserved]

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(c) Tolerances with regional registra- § 180.617 Metconazole; tolerances for tions. [Reserved] residues. (d) Indirect or inadvertent residues. (a) General. Tolerances are estab- Tolerances are established for the indi- lished for the residue of the fungicide rect or inadvertent residues of metconazole (5-[(4- amicarbazone [4-amino-4, 5-dihydro-N- chlorophenyl)methyl]-2,2-dimethyl-1- (1,1-dimethylethyl)-3-(1-methylethyl)-5- (1H-1,2,4-triazol-1- oxo-1H-1,2,4-triazole-1-carboxamide] ylmethyl)cyclopentanol) in or on the and its metabolites DA amicarbazone following commodity: [N-(1,1-dimethylethyl)-4,5-dihydro-3-(1- methylethyl)-5-oxo-1H-1,2,4-triazole-1- Commodity Parts per carboxamide] and iPr-2-OH DA million amicarbazone [N-(1,1-dimethylethyl)- Banana1 ...... 0 .1 4,5-dihydro-3-(1-hydroxy-1- 1 No U.S. registration as of August 30, 2006. methylethyl)-5-oxo-1H-1,2,4-triazole-1- carboxamide], calculated as parent (b) Section 18 emergency exemptions. equivalents, in or on the following Time-limited tolerances are estab- commodities when present therein as a lished for residues of the fungicide result of application of amicarbazone metconazole, 5-[(4- to the growing crops in paragraph (a) chlorophenyl)methyl]-2,2-dimethyl-1- of this section: (1H -1,2,4-triazole-1-yl-meth- yl)cyclopentanol in or on aspirated Parts per grain fractions; egg; meat, fat and Commodity million meat by-products of cattle, goat, hog, Alfalfa, forage ...... 0.05 horse, poultry and sheep; milk; soy- Alfalfa, hay ...... 0.10 bean, hulls; soybean, meal; soybean, re- Cotton, gin byproducts ...... 0 .30 fined oil; and soybean, seed in connec- Cotton, undelinted seed ...... 0 .07 tion with the use of the pesticide under Soybean, forage ...... 1 .50 Soybean, hay ...... 5 .0 section 18 emergency exemptions Soybean, seed ...... 0 .80 granted by EPA. The tolerances will Wheat, forage ...... 0 .50 expire and be revoked on the date spec- Wheat, grain ...... 0 .10 ified in the following table. Wheat, grain, milled byproducts ...... 0 .15 Wheat, hay ...... 1 .0 Expiration/ Wheat, straw ...... 0 .50 Commodity Parts per revocation million date

[70 FR 55760, Sept. 23, 2005] Aspirated grain fractions ...... 1.00 12/31/10 Cattle, fat ...... 0.02 12/31/10 § 180.616 Fenpropimorph; tolerances Cattle, meat ...... 0.02 12/31/10 for residues. Cattle, meat byproducts ...... 0.02 12/31/10 Egg ...... 0.02 12/31/10 Tolerances are established for the Goat, fat ...... 0.02 12/31/10 residues of the fungicide Goat, meat ...... 0.02 12/31/10 fenpropimorph (rel-(2R,6S)-4-[3-[4-(1,1- Goat, meat byproducts ...... 0.02 12/31/10 Hog, fat ...... 0.02 12/31/10 dimethylethyl)phenyl]-2- Hog, meat ...... 0.02 12/31/10 methylpropyl]-2,6-dimethylmorpholine) Hog, meat byproducts ...... 0.02 12/31/10 in or on the following commodity: Horse, fat ...... 0.02 12/31/10 Horse, meat ...... 0.02 12/31/10 Parts per Horse, meat byproducts ...... 0.02 12/31/10 Commodity million Milk ...... 0.02 12/31/10 Poultry, fat ...... 0.02 12/31/10 Banana* ...... 2 .0 Poultry, meat ...... 0.02 12/31/10 Poulty, meat byproducts ...... 0.02 12/31/10 *No U.S. registration as of February 10, 2006. Sheep, fat ...... 0.02 12/31/10 (b) Section 18 emergency exemptions. Sheep, meat ...... 0.02 12/31/10 Sheep, meat byproducts ...... 0.02 12/31/10 [Reserved] Soybean, hulls ...... 1.20 12/31/10 (c) Tolerances with regional registra- Soybean, meal ...... 0.25 12/31/10 tions. [Reserved] Soybean, refined oil ...... 1.20 12/31/10 (d) Indirect or inadvertent residues. Soybean, seed ...... 0.10 12/31/10 [Reserved] (c) Tolerances with regional registra- [71 FR 15612, Mar. 29, 2006] tions. [Reserved]

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(d) Indirect or inadvertent residues. § 180.620 Etofenprox; tolerances for [Reserved] residues. [71 FR 56388, Sept. 27, 2006, as amended at 71 (a) General. [Reserved] FR 76196, Dec. 20, 2006] (b) Section 18 emergency exemptions. Time-limited tolerances are estab- § 180.618 Benthiavalicarb-isopropyl; lished for residues of etofenprox (2- tolerance for residues. [ethoxyphenyl]-2-methylpropyl-3- (a) General. Tolerances are estab- phenoxy benzyl ether) in connection lished for the combined residues of with use of the pesticide under section benthiavalicarb-isopropyl, 18 emergency exemptions granted by isopropyl[(S)-1-[[[(1R)-1-(6-fluoro-2- EPA. The tolerances will expire and benzothiazolyl)ethyl]amino] carbonyl]- are revoked on the dates specified in 2-methylpropyl]carbamate and the following table. isopropyl[(S)-1-[[[(1S)-1-(6-fluoro-2- benzothiazolyl)ethyl]amino] carbonyl]- Expiration/ Commodity Parts per revocation 2-methylpropyl]carbamate, in or on the million date following raw agricultural commod- ities: Rice, grain ...... 0.01 12/31/09 Rice, straw ...... 0.02 12/31/09 Parts per Commodity million (c) Tolerances with regional registra- tions. [Reserved] Grape, imported ...... 0 .25 Grape, raisin ...... 1 .0 (d) Indirect or inadvertent residues. Tomato ...... 0.45 [Reserved] Note: There are no U.S. registrations as of July 30, 2006. [71 FR 54928, Sept. 20, 2006] (b) Section 18 emergency exemptions. [Reserved] § 180.621 Dithianon; tolerances for res- idues. (c) Tolerances with regional registra- tions. [Reserved] (a) General. Tolerances are estab- (d) Indirect of inadvertent residues. lished for residues of the fungicide [Reserved] dithianon, (5,10-dihydro-5,10- dioxonaphtho(2,3-b)-1,4-dithiin-2,3- [71 FR 52003, Sept. 1, 2006] dicarbonitrile) in or on the following commodities: § 180.619 Epoxiconazole; tolerances for residues. Commodity Parts per (a) General. Tolerances are estab- million lished for the residues of the fungicide Fruit, pome, group 111 ...... 5 epoxiconazole [(rel-1-[[(2R,3S)-3-(2- Hop, dried cones1 ...... 100 chlorophenyl)-2-(4- 1No U.S. registration as of September 5, 2006. fluorophenyl)oxiranyl]methyl]-1H-1,2,4- triazole]) in or on the following com- (b) Section 18 emergency exemptions. modities: [Reserved] (c) Tolerances with regional registra- Commodity Parts per tions. [Reserved] million (d) Indirect or inadvertent residues. Banana* ...... 0.5 [Reserved] Coffee* ...... 0.05 [71 FR 54922, Sept. 20, 2006] *No U.S. Registration as of August 4, 2006 (b) Section 18 emergency exemptions. § 180.622 Ethaboxam; tolerances for [Reserved] residues. (c) Tolerances with regional Registra- (a) General. Tolerances are estab- tions. [Reserved] lished for residues of ethaboxam, N- (d) Indirect or inadvertent residues. (cyano-2-thienylmethyl)-4-ethyl-2- [Reserved] (ethlyamino)-5-thiazolecarboxamide in or on the following commodity: [71 FR 53989, Sept. 13, 2006]

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Parts per Parts per Commodity million Commodity million

Grape1 ...... 6 .0 Grape ...... 0 .61 1 There is no U.S. registration as of September 27, 2006 1 There is no U.S. registration on grapes as of September 20, 2006. (b) Section 18 emergency exemptions. (b) Section 18 emergency exemption. [Reserved] [Reserved] (c) Tolerances with regional registra- (c) Tolerances with regional registra- . [Reserved] tions tions. [Reserved] (d) Indirect or inadvertent residues. (d) Indirect or inadvertent residues. [Reserved] [Reserved] [71 FR 56392, Sept. 27, 2006] [71 FR 54917, Sept. 20, 2006]

§ 180.623 Flufenoxuron; tolerances for § 180.625 Orthosulfamuron; tolerances residues. for residues. (a) General. Tolerances are estab- (a) General. Tolerances are estab- lished for residues of the insecticide, lished for residues of orthosulfamuron flufenoxuron, 1-[4-(2-chloro-a,a,a- 1-(4,6-dimethoxypyrimidin-2-yl)-3-[2- trifluoro-p-tolyloxy)-2-fluorophenyl]-3- (dimethylcarbamoyl)- (2,6-difluorobenzoyl)urea, in or on the phenylsulfamoyl] urea) per se in or on following food commodities. the following commodities:

Commodity Parts per Parts per million Commodity million

Apple1 ...... 0 .50 Rice, grain ...... 0 .05 Cattle, fat1 ...... 4 .5 Rice, straw ...... 0 .05 Cattle, meat1 ...... 0 .10 Cattle, meat byproducts1 ...... 0 .50 (b) Section 18 emergency exemptions. Goat, fat1 ...... 4 .5 Goat, meat1 ...... 0 .10 [Reserved] Goat, meat byproducts1 ...... 0 .50 (c) Tolerances with regional registra- Grape1 ...... 0 .70 tions. [Reserved] Grape, raisin1 ...... 2 .0 (d) Indirect and inadvertant residues. Horse, fat1 ...... 4.5 Horse, meat1 ...... 0 .10 [Reserved] Horse, meat byproducts1 ...... 0.50 [72 FR 8931, Feb. 28, 2007] Milk ...... 0.20 Milk, fat1 ...... 4.0 Orange1 ...... 0.30 § 180.626 Prothioconazole; tolerances Orange, oil1 ...... 60 for residues. Pear1 ...... 0 .50 (a) General. (1) Tolerances are estab- Sheep, fat1 ...... 4 .5 Sheep, meat1 ...... 0 .10 lished for combined residues of the fun- Sheep, meat byproducts1 ...... 0 .50 gicide prothioconazole, 2-[2-(1- chlorocyclopropyl)-3-(2-chlorophenyl)- 1There are no U.S. registrations as of September 30, 2006. 2-hydroxypropyl]-1,2-dihydro-3H-1,2,4- (b) Section 18 emergency exemptions. triazole-3-thione, and prothioconazole- [Reserved] desthio, a-(1-chlorocyclopropyl)-a-[(2- (c) Tolerances with regional restric- chlorophenyl)methyl]-1H-1,2,4-triazole- tions. [Reserved] 1-ethanol, calculated as parent in or on (d) Indirect or inadvertent residues. the following commodities: [Reserved] Commodity Parts per [71 FR 57436, Sept. 29, 2006] million

Barley, grain ...... 0 .35 § 180.624 Metrafenone; tolerances for Barley, hay ...... 7 .0 residues. Barley, straw ...... 4 .0 (a) General. Tolerances are estab- Grain, aspirated grain fractions ...... 11 Pea and bean, dried shelled, except soybean, lished for residues of metrafenone, (3- subgroup 6C ...... 0 .9 bromo-6-methoxy-2- Peanut ...... 0 .02 methylphenyl)(2,3,4-trimethoxy-6- Peanut, hay ...... 6.0 Rapeseed, seed ...... 0 .15 methylphenyl)methanone, in or on the Wheat, forage ...... 6 .0 following commodities. Wheat, grain ...... 0 .07

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(d) Indirect or inadvertent residues. Commodity Parts per million [Reserved] Wheat, hay ...... 4 .5 [72 FR 14447, Mar. 28, 2007] Wheat, straw ...... 5 .0 § 180.628 Chlorantraniliprole; toler- (2) Tolerances are established for ances for residues. combined residues of the fungicide prothioconazole, 2-[2-(1- (a) Tolerances are established for res- chlorocyclopropyl)-3-(2-chlorophenyl)- idues of the pesticide 2-hydroxypropyl]-1,2-dihydro-3H-1,2,4- chlorantraniliprole (3-bromo-N-[4- triazole-3-thione, and prothioconazole- chloro-2-methyl-6- desthio, a-(1-chlorocyclopropyl)-a-[(2- [(methylamino)carbonyl]phenyl]-1-(3- chlorophenyl)methyl]-1H-1,2,4-triazole- chloro-2-pyridinyl)-1H-pyrazole-5- 1-ethanol, and conjugates that can be carboxamide) in or on the following converted to these two compounds by raw agricultural commodities: acid hydrolysis, calculated as parent in Expiration/ or on the following commodities: Commodity Parts per revocation million date Parts per Commodity million Apple ...... 0.25 05/01/2010 Apple, wet pomace ...... 0.60 05/01/2010 Cattle, fat ...... 0.1 Celery ...... 7.0 05/01/2010 Cattle, meat ...... 0 .02 Cucumber ...... 0.10 05/01/2010 Cattle, meat byproducts ...... 0.2 Lettuce, head ...... 4.0 05/01/2010 Goat, fat ...... 0 .1 Lettuce, leaf ...... 8.0 05/01/2010 Goat, meat ...... 0.02 Pear ...... 0.30 05/01/2010 Goat, meat byproducts ...... 0 .2 Pepper ...... 0.50 05/01/2010 Hog, meat byproducts ...... 0 .05 Spinach ...... 13.0 05/01/2010 Horse, fat ...... 0 .1 Squash ...... 0.40 05/01/2010 Horse, meat ...... 0 .02 Tomato ...... 0.30 05/01/2010 Horse, meat byproducts ...... 0 .2 Milk ...... 0.02 Watermelon ...... 0.20 05/01/2010 Poultry liver ...... 0 .02 Sheep, fat ...... 0 .1 (b) Section 18 emergency exemptions. Sheep, meat ...... 0.02 [Reserved] Sheep, meat byproducts ...... 0 .2 (c) Tolerances with regional registra- (b) Section 18 emergency exemptions. tions. [Reserved] [Reserved] (d) Indirect or inadvertent residues. (c) Tolerances with regional registra- [Reserved] tions. [Reserved] [72 FR 27455, May 16, 2007] (d) Indirect or inadvertent residues. [Reserved] Subpart D—Exemptions From [72 FR 11783, Mar. 14, 2007] Tolerances

§ 180.627 Fluopicolide; tolerances for § 180.900 Exemptions from the require- residues. ment of a tolerance. (a) General. Tolerances are estab- An exemption from a tolerance shall lished for residues of fluopicolide, 2,6- be granted when it appears that the dichloro-N-[[3-chloro-5- total quantity of the pesticide chem- (trifluoromethyl)-2-pyridinyl]methyl] ical in or on all raw agricultural com- benzamide, in or on the following com- modities for which it is useful under modities. conditions of use currently prevailing or proposed will involve no hazard to Parts per mil- Commodity lion the public health.

Grape ...... 2.0 [69 FR 23117, Apr. 28, 2004] Grape, raisin ...... 6.0 § 180.905 Pesticide chemicals; exemp- (b) Section 18 emergency exemptions. tions from the requirement of a tol- [Reserved] erance. (c) Tolerances with regional registra- (a) When applied to growing crops, in tions. [Reserved] accordance with good agricultural

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practice, the following pesticide chemi- when applied to a crop at the time of or cals are exempt from the requirement after harvest. of a tolerance: [69 FR 23117, Apr. 28, 2004] (1) [Reserved] (2) N-Octylbicyclo(2,2,1)-5-heptene- § 180.910 Inert ingredients used pre- 2,3-dicarboximide. and post-harvest; exemptions from (3) Petroleum oils. the requirement of a tolerance. (4) Piperonyl butoxide. Residues of the following materials (5) [Reserved] are exempted from the requirement of (6) and pyrethrins. a tolerance when used in accordance (7) Rotenone or derris or cube roots. with good agricultural practice as inert (or occasionally active) ingredients in (8) Sabadilla. pesticide formulations applied to grow- (b) These pesticides are not exempted ing crops or to raw agricultural com- from the requirement of a tolerance modities after harvest:

Inert ingredients Limits Uses

Acetic acid ...... Catalyst Acetic anhydride ...... Solvent, cosolvent Acetone ...... Do. Alkanoic and alkenoic acids, mono- and diesters ...... Emulsifiers of a-hydro-w-hydroxypoly (oxyethylene) with molecular weight (in amu) range of 200 to 6,000. Alkyl (C8-C24) benzenesulfonic acid and its am- ...... Surfactants, related adjuvants of surfactants monium, calcium, magnesium, potassium, so- dium, and zinc salts. a-Alkyl (C9-C18-w-hydroxypoly(oxyethylene) with ...... Solvent, cosolvent, surfactant, and related ad- poly(oxyethylene) content of 2-30 moles. juvants of surfactants a-(p-Alkylphenyl)-w-hydroxypoly(oxyethylene) ...... Surfactants, related adjuvants of surfactants produced by the condensation of 1 mole of alkylphenol (alkyl is a mixture of propylene tetramer and pentamer isomers and averages C13) with 6 moles of ethylene oxide. a-Alkyl (C6-C14)-w-hydroxypoly(oxypropylene) ...... Do. block copolymer with polyoxyethylene; polyoxypropylene content is 1-3 moles; polyoxyethylene content is 4-12 moles; aver- age molecular weight (in amu) is approxi- mately 635. a-alkyl (C12-C15)-w-hydroxypoly (oxypropylene) Not more than 20% of pes- Surfactant poly (oxyethylene) copolymers (where the ticide formulations poly (oxypropylene) content is 3–60 moles and the poly (oxyethylene) content is 5–80 moles). Alkyl (C8-C18) sulfate and its ammonium, cal- ...... Surfactants. cium, isopropylamine, magnesium, potassium, sodium, and zinc salts. Aluminum hydroxide ...... Diluent, carrier Aluminum oxide ...... Diluent Aluminum stearate ...... Surfactant Ammonium bicarbonate ...... Surfactant, suspending agent, dispersing agent Ammonium carbamate ...... Synergist in aluminum phosphide formulations Ammonium chloride ...... Intensifier when used with ammonium nitrate as a dessicant or defoliant. Fire suppressant in aluminum phosphide and magnesium phosphide formulations Ammonium hydroxide...... Solvent, cosolvent, neutralizer, solubilizing agent Ammonium stearate ...... Surfactant Ammonium sulfate ...... Solid diluent, carrier Ammonium thiosulfate ...... Intensifier when used with ammonium nitrate as desiccant or defoliant Amyl acetate ...... Solvent, cosolvent, attractant Ascorbyl palmitate ...... Preservative Attapulgite-type clay ...... Solid diluent, carrier, thickener Bacillus thuringiensis fermentation solids and/or ...... Diluent, carrier solubles. Bentonite ...... Solid diluent, carrier Benzoic acid ...... Preservative for formulation

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Inert ingredients Limits Uses

Bicyclo[3.1.1]hept–2–ene, 2,6,6–trimethyl–, ...... Surfactants, related adjuvants of surfactants homopolymer (Alpha-pinene, homopolymer )(CAS Reg. No. 25766–18–1). Bicyclo[3.1.1]heptane, 6,6–dimethyl–2–meth- ...... Surfactants, related adjuvants of surfactants ylene–, homopolymer (Beta-pinene, homopolymer) (CAS Reg. No. 25719–60–2). Bicyclo[3.1.1]hept–2–ene, 2,6,6–trimethyl–, poly- ...... Surfactants, related adjuvants of surfactants mer with 6,6– dimethyl–2– methylenebicyclo [3.1.1] heptane (Copolymer of alpha- and beta-pinene) (CAS Reg. No. 31393–98–3). 2-Bromo-2-nitro-1,3-propanediol (CAS Reg. No. 0.04% or less by weight of In-can preservative 52–51–7). the total pesticide formu- lation. Butane ...... Propellant n-Butanol (CAS Reg. No. 71–36–3) ...... Solvent, cosolvent Butylated hydroxyanisole ...... Antioxidant Butylated hydroxytoluene ...... Do. a-(p-tert-Butylphenyl)-w-hydroxypoly (oxy- ...... Surfactants related adjuvants of surfactants ethylene) mixture of dihydrogen phosphate and monohydrogen phosphate esters and the corresponding ammonium calcium, magne- sium, monoethanolamine, potassium, sodium, and zinc salts of the phosphate esters; the poly(oxyethylene) content averages 4-12 moles. Calcareous shale ...... Solid diluent carrier Calcite ...... Do. Calcium carbonate ...... Do. Calcium chloride ...... Stabilizer Calcium phosphate ...... Solid diluent, carrier Calcium hydroxide ...... Do. Calcium hypochlorite ...... Sanitizing and bleaching agent Calcium oxide ...... Solid diluent, carrier Calcium salt of partially dimerized rosin, con- ...... Coating agent forming to 21 CFR 172.210. Calcium silicate ...... Solid diluent, carrier Calcium stearate ...... Do. Carrageenan, conforming to 21 CFR 172.620 .... Minimum molecular weight Thickener (in amu): 100,000. Cetyl alcohol (CAS Reg. No. 36653–82–4) ...... Not more than 5.0% of pes- Evaporation retardant ticide formulation. Charcoal, activated ...... Meets specifications in the Carrier Food Chemical Codex. Coconut shells ...... Solid diluent and carrier Cod liver oil ...... Solvent, cosolvent Croscarmellose sodium (CAS Reg. No. 74811– ...... Disintegrant, solid diluent, carrier, and thick- 65–7). ener Dialkyl (C8-C18) dimethyl ammonium chloride ..... Not more than 0.2% in sili- Flocculating agent in the manufacture of silica, ca, hydrated silica. hydrated silica for use as a solid diluent, car- rier Diatomite (diatomaceous earth) ...... Solid diluent carrier Diethylene glycol abietate ...... Surfactants, related adjuvants of surfactants 1,1-Difluoroethane (CAS Reg. No. 75–37–6) ..... For aerosol pesticide formu- Aerosol propellant lations used for insect control in food- and feed- handling establishments and animals. 1,2-Dihydro-6-ethoxy-2,2,4-trimethylquinolene .... Not more than 0.02% of Antioxidant pesticide formulation. Dimethyl ether (methane, oxybis-) (CAS Reg...... Propellant No. 115–10–6). 3,6-Dimethyl-4-octyn-3,6-diol ...... Not more than 2.5% of pes- Surfactants, related adjuvants of surfactants ticide formulation. a-(o,p-Dinonylphenyl)-w-hydroxypoly (oxy- ...... Surfactants, related adjuvants of surfactants ethylene) mixture of dihydrogen phosphate and monohydrogen phosphate esters and the corresponding ammonium, calcium, magne- sium, monoethanolamine, potassium, sodium, and zinc salts of the phosphate esters; the nonyl group is a propylene trimer isomer and the poly(oxyethylene) content averages 4-14 moles.

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Inert ingredients Limits Uses

a-(o,p-Dinonylphenyl)-w-hydroxypoly (oxy- ...... Do. ethylene) produced by condensation of 1 mole of dinonylphenol (nonyl group is a propylene trimer isomer) with an average of 4-14 or 140- 160 moles of ethylene oxide. Dipropylene glycol ...... Solvent, cosolvent Disodium phosphate ...... Anticaking agent, conditioning agent Disodium zinc ethylenediaminetetraacetate ...... Sequestrant dihydride. Dodecylbenzenesulfonic acid, amine salts ...... Release rate regulator in pheromone formula- tion a-(p-Dodecylphenyl)-w-hydroxypoly (oxy- ...... Surfactants, related, adjuvants of surfactants ethylene) produced by the condensation of 1 mole of dodecylphenol (dodecyl group is a propylene tetramer isomer) with an average of 4-14 or 30-70 moles of ethylene oxide; if a blend of products is used, the average num- ber of moles of ethylene oxide reacted to produce any product that is a component of the blend shall be in the range of 4-14 or 30- 70. Dolomite ...... Solid diluent, carrier Epoxidized linseed oil ...... Surfactants, related adjuvants of surfactants Epoxidized soybean oil ...... Do. Ethyl acetate ...... Solvent, cosolvent Ethyl alcohol ...... Do. Ethyl esters of fatty acids derived from edible ...... Solvent, cosolvent fats and oils. Ethyl maltol (CAS Reg. No.4940–11–8) ...... Not more than 0.2 % of the Odor masking agent pesticide formulation. Ethylene oxide adducts of 2,4,7,9-tetramethyl-5- ...... Surfactants, related adjuvants of surfactants decynediol, the ethylene oxide content aver- ages 3.5, 10, or 30 moles. Ethylenediaminetetraacetic acid ...... 3% of pesticide formulation Sequestrant Ethylenediaminetetraacetic acid, tetrasodium 5% of pesticide formulation Sequestrant salt. 2-Ethyl-1-hexanol ...... Not more than 2.5% of pes- Solvent, adjuvant of surfactants ticide formulation. Fatty acids, conforming to 21 CFR 172.860 ...... Binder, defoaming agent, lubricant FD&C Blue No. 1 ...... Not more than 0.2% of pes- Dye ticide formulation. FD&C Red No. 40 (CAS Reg. No. 25956–17–6) Not to exceed 0.002% by Dye, coloring agent conforming to 21 CFR 74.340. weight of pesticide formu- lation. Ferric sulfate ...... Solid diluent, carrier Furcelleran ...... Thickener D-glucopyranose, oligomeric, C10–16-alkyl ...... Surfactant glycosides (CAS Reg. No. 110615–47–9). Glycerides, edible fats and oils derived from ...... Emulsifier, dispersing agent plants and animals, reaction products with su- crose (CAS Reg. Nos. 100403–38–1, 100403–41–6, 100403–39–2, 100403–40–5). Glycerol mono-, di-, and triacetate ...... Solvent, cosolvent Glyceryl monostearate ...... Emulsifier Granite ...... Do. Graphite ...... Solid diluent, carrier Gum arabic (acacia) ...... Surfactant, suspending agent, dispersing agent Gypsum ...... Solid diluent, carrier Hexamethylenetetramine ...... For use in citrus washing Preservative solutions only at not more than 1%. 3-hexen-1-ol, (3Z)- (CAS Reg. No. 928-96-1) ..... Not more than 0.4% of the Odorant, alerting agent pesticide formulation. n-Hexyl alcohol (CAS Reg. No. 111–27–3) ...... Solvent, cosolvent Hydrochloric acid ...... Solvent, neutralizer Hydroxyethylidine diphosphonic acid (HEDP) For use in antimicrobial Stabilizer, chelator (CAS Reg. No. 2809–21–4). pesticide formulations at not more than 1 percent. Iron oxide ...... Solid diluent, carrier Isopropyl myristate (CAS Reg. No. 110–27–0) ...... Solvent Kaolinite-type clay ...... Solid diluent, carrier Lactic acid ...... Solvent Lactic acid, 2-ethylhexyl ester (CAS Reg. No...... Solvent 6283–86–9).

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Inert ingredients Limits Uses

Lactic acid, 2-ethylhexyl ester, (2S)- (CAS Reg...... Solvent No. 186817–80–1). Lactic acid, n-propyl ester, (S); (CAS Reg. No...... Solvent 53651–69–7). Lauryl alcohol ...... Surfactant a-Lauryl-w-hydroxypoly(oxyethylene), average ...... Emulsifier molecular weight (in amu) of 600. a-Lauryl-w-hydroxypoly(oxyethylene) sulfate, so- ...... Surfactants, related adjuvants of surfactants dium salt; the poly(oxyethylene) content is 3-4 moles. Lignin (CAS Reg. No. 9005–53–2) ...... Surfactant, related adjuvants of surfactants Lignin, alkali (CAS Reg. No. 8068–05–1) ...... Do. Lignin, alkali, oxidized, sodium salt (CAS Reg...... Do. No. 68201–23–0). Lignin alkali reaction products with disodium sul- ...... Do. fite and formaldehyde (CAS Reg. No. 105859–97–0). Lignin alkali reaction products with formaldehyde ...... Do. and sodium bisulfite (CAS Reg. No. 68512– 35–6). Lignosulfonic acid (CAS Reg. No. 8062–15–5) ...... Do. Lignosulfonic acid, ammonium calcium salt ...... Do. (CAS Reg. No. 12710–04–2). Lignosulfonic acid, ammonium magnesium salt ...... Do. (CAS Reg. No. 123175–37–1). Lignosulfonic acid, ammonium salt (CAS Reg...... Do. No. 8061–53–8). Lignosulfonic acid, ammonium sodium salt (CAS ...... Do. Reg. No. 166798–73–8). Lignosulfonic acid, calcium magnesium salt ...... Do. (CAS Reg. No. 55598–86–2). Lignosulfonic acid, calcium salt (CAS Reg. No...... Do. 8061–52–7). Lignosulfonic acid, calcium sodium salt (CAS ...... Do. Reg. No. 37325–33–0). Lignosulfonic acid, ethoxylated, sodium salt ...... Do. (CAS Reg. No. 68611–14–3). Lignosulfonic acid, magnesium salt (CAS Reg...... Do. No. 8061–54–9). Lignosulfonic acid, potassium salt (CAS Reg...... Do. No. 37314–65–1). Lignosulfonic acid, sodium salt (CAS Reg. No...... Do. 8061–51–6). Lignosulfonic acid, sodium salt, oxidized (CAS ...... Do. Reg. No. 68855–41–4). Lignosulfonic acid, sodium salt, polymer with ...... Do. formaldehyde and phenol (CAS Reg. No. 37207–89–9). Lignosulfonic acid, sodium salt, sulfomethylated ...... Do. (CAS Reg. No. 68512–34–5). Lignosulfonic acid, zinc salt (CAS Reg. No...... Do. 57866–49–6). d-Limonene (CAS Reg. No. 5989–27–5) ...... Solvent, fragrance Magnesium carbonate ...... Anticaking agent, conditioning agent Magnesium chloride ...... Safener Magnesium lime ...... Solid diluent, carrier Magnesium oxide ...... Do. Magnesium silicate ...... Do. Magnesium stearate ...... Surfactant Magnesium sulfate ...... Solid diluent, carrier, safener Manganous oxide ...... Solid diluent, carrier Methyl alcohol ...... Solvent Methyl n-amyl ketone (CAS Reg. No. 110–43–0) ...... Solvent, cosolvent Methylated silicones ...... Antifoaming agent Methyl esters of fatty acids derived from edible ...... Solvent, cosolvent fats and oils. Methyl esters of higher fatty acids conforming to ...... Antidusting agent, surfactant 21 CFR 573.640. Methyl isobutyl ketone ...... Solvent Mica ...... Solid diluent, carrier Mineral oil, U.S.P., or conforming to 21 CFR ...... Diluent, carrier, and solvent 172.878 or 178.3620(a) (CAS Reg. No. 8012– 95–1).

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Inert ingredients Limits Uses

Monoammonium phosphate ...... No more than 3.75% by Postharvest fumigation in formulation with alu- weight in formulation. minum phosphide Mono- and diglycerides of C8-C18 fatty acids ...... Surfactants, related adjuvants of surfactants Montmorillonite-type clay ...... Solid diluent, carrier Nonyl, decyl, and undecyl glycoside mixture with ...... Surfactant. a mixture of nonyl, decyl, and undecyl oligosaccharides and related reaction prod- ucts (primarily decanol and undecanol) pro- duced as an aqueous-based liquid (50 to 65% solids) from the reaction of primary alcohols (containing 15 to 20% secondary alcohol iso- mers) in a ratio of 20% C9, 40% C10, and 40% C11 with carbohydrates (average glucose to alkyl chain ratio 1.3 to 1.8). a-(p-Nonylphenyl)-w-hydroxypoly(oxyethylene) ...... Surfactants, related adjuvants of surfactants mixture of dihydrogen phosphate and monohydrogen phosphate esters and the cor- responding ammonium, calcium, magnesium, monoethanolamine, potassium, sodium, and zinc salts of the phosphate esters; the nonyl group is a propylene trimer isomer and the poly(oxyethylene) content averages 4-14 moles or 30 moles. a-(p-Nonylphenyl)-w-hydroxypoly(oxyethylene) ...... Do. produced by the condensation of 1 mole of nonylphenol (nonyl group is a propylene trimer isomer) with an average of 4-14 or 30- 90 moles of ethylene oxide; if a blend of prod- ucts is used, the average number of moles of ethylene oxide reacted to produce any prod- uct that is a component of the blend shall be in the range of 4-14 or 30-90. a-(p-Nonylphenyl)-w-hydroxypoly(oxyethylene) ...... Do. sulfate, ammonium, calcium, magnesium, po- tassium, sodium, and zinc salts; the nonyl group is a propylene trimer isomer and the poly(oxyethylene) content averages 4 moles. 1-Octanal (CAS Reg. No. 124–13–0) ...... Not more than 0.2% of the Odor masking agent pesticide formulation Octyl and decyl glucosides mixture with a mix- ...... Surfactants, related adjuvants of surfactants ture of octyl and decyloligosaccharides and related reaction products (primarily n- decanol) produced as an aqueous-based liq- uid (68-72% solids) from the reaction of straight chain alcohols (C8(45%), C10 (55%)) with anhydrous glucose. Oleic acid ...... Diluent Oleic acid diester of a-hydro-w-hydroxypoly ...... Surfactants, related adjuvants of surfactants (oxyethylene); the poly(oxyethylene) having average molecular weight (in amu) 400. a-Oleoyl-w-hydroxypoly(oxyethylene), average ...... Emulsifier molecular weight (in amu) of 600. Oleyl alcohol (CAS Reg. No. 143–28–2 ...... 15% ...... Cosolvent Oxalic acid ...... No more oxalic acid should Calcium chelating hard water inhibitor be used than is nec- essary to chelate calcium and in no case should more than 2 lb oxalic acid per acre be used. Palmitic acid ...... Diluent Pentaerythritol ester of maleic anhydride modi- ...... Plasticizer fied wood rosin. Petrolatum, conforming to 21 CFR 172.880 ...... Coating agent Petroleum hydrocarbons, light odorless con- ...... Solvent, diluent. forming to 21 CFR 172.884. Petroleum hydrocarbons, synthetic isoparaffinic, ...... Do. conforming to 21 CFR 172.882. Petroleum naphtha, conforming to 21 CFR ...... Component of coating agent 172.250(d). Petroleum wax, conforming to 21 CFR ...... Coating agent 172.886(d). Phosphoric acid ...... Buffer Polyethylene, conforming to 21 CFR ...... Binder, carrier, and coating agent 177.1520(c).

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Inert ingredients Limits Uses

Polyethylene glycol[a-hydro-w- ...... Surfactants, related adjuvants of surfactants hydroxypoly(oxyethylene)]; mean molecular weight (in amu) 194 to 9,500 conforms to 21 CFR 178.3750. Polyglycerol esters of fatty acids conforming to ...... Surfactants, related adjuvants of surfactants 21 CFR 172.854. Polyglyceryl phthalate ester of coconut oil fatty ...... Do. acids. Poly(methylene-p-tert-butylphenoxy)- ...... Coating agent poly(oxyethylene) ethanol; the poly(oxyethylene) content averages 4-12 moles. Poly(methylene-p-nonylphenoxy)poly (oxy- ...... Coating agent ethylene) ethanol; the poly(oxyethylene) con- tent averages 4-12 moles. Poly(oxy-1,2-ethanediyl), a-(carboxymethyl)-w- ...... Surfactant (nonylphenoxy) produced by the condensation of 1 mole of nonylphenol (nonyl group is a propylene trimer isomer) with an average of 4- 14 or 30-90 moles of ethylene oxide. The mo- lecular weight (in amu) ranges are 454-894 and 1598-4238. Polyoxyethylene (20) sorbitan monostearate ...... Surfactants, related adjuvants of surfactants [Poly[oxy(methyl-1,2-ethanediyl)], a-[2-bis(2-hy- Not to exceed 15% in the Surfactant droxyethyl)amino]propyl]-w-hydroxy,-ether with formulated product; only a-hydro-w-hydroxypoly(oxy-1,2-ethanediyl) for use with glyphosate. (1:2), mono-C12–16 alkyl ethers, (CAS Reg. No. 176022–82–5). Polysorbate 65, conforming to 21 CFR 172.838 ...... Emulsifier Potassium aluminum silicate ...... Solid diluent, carrier Potassium hydroxide ...... Neutralizer Potassium phosphate ...... Buffer Potassium sulfate ...... Solid diluent Propane ...... Propellant n-Propanol ...... Solvent, cosolvent 2-Propenoic acid, 2-methyl-, polymer with ethyl ...... Encapsulating agent, dispensers, resins, fibers 2-propenoate and methyl 2-methyl-2- and beads propenoate, ammonium salt (CAS Registra- tion No. 55989–05–4), minimum number aver- age molecular weight (in amu), 18,900. Propylene glycol ...... Solvent, cosolvent. Propylene glycol alginate (as defined in 21 CFR ...... Defoaming agent 172.858). Propyl gallate ...... Antioxidant Propyl p-hydroxybenzoate ...... Preservative for formulations Pyrophyllite ...... Solid diluent, carrier Rhizobium inoculants (e.g. Sinorhizobium, ...... All leguminous food commodities Bradyrhizobium & Rhizobium). Rosin, partially dimerized (as defined in 21 CFR ...... Surfactants, related adjuvants of surfactants 172.615). Rosin, partially hydrogenated (as defined in 21 ...... Do. CFR 172.615). Rosin, wood ...... Do. Salts of fatty acids, conforming to 21 CFR ...... Binder, emulsifier, anticaking agent 172.863. Sand ...... Solid diluent, carrier Secondary alkyl (C11-C15) poly(oxyethylene) ac- ...... Surfactant etate, sodium salt; the ethylene oxide content averages 5 moles. Shellac, bleached; refined, food grade, arsenic ...... Coating agent and rosin-free. Soapstone ...... Solid diluent Sodium acid pyrophosphate ...... Surfactant, suspending agent, dispersing agent, buffer Sodium a-olefinsulfonate (sodium C14-C16) ...... Surfactants, related adjuvants of surfactants (Olefin sulfonate). Sodium aluminum silicate ...... Solid diluent, carrier Sodium diisobutylnaphthalenesulfonate ...... Surfactants, related adjuvants of surfactants Sodium dioctylsulfosuccinate ...... Do. Sodium dodecylphenoxybenzenedisulfonate ...... Do. Sodium hexametaphosphate...... Surfactant, emulsifier, wetting agent, sus- pending agent, dispersing agent, buffer Sodium hydroxide ...... Neutralizer Sodium isopropylisohexylnaphthalenesulfonate ...... Surfactants, related adjuvants of surfactants

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Inert ingredients Limits Uses

Sodium lauryl glyceryl ether sulfonate ...... Do. Sodium metasilicate ...... Surfactants, emulsifiers, wetting agents, dis- persing agents, buffer

Sodium monoalkyl and dialkyl (C8-C16) ...... Surfactants, related adjuvants of surfactants phenoxybenzenedisulfonate mixtures con- taining not less than 70% of the monoalkylated product. Sodium mono- and dimethyl ...... Do. naphthalenesulfonates, molecular weight (in amu) 245-260. Sodium mono-, di-, and tributyl ...... Do. naphthalenesulfonates. Sodium mono-, di-, and triisopropyl ...... Do. naphthalenesulfonate. Sodium N-oleoyl-N-methyltaurine ...... Do. Sodium salt of sulfated oleic acid ...... Surfactants, related adjuvants of surfactants Sodium silicate ...... Surfactant, emulsifier, wetting agent, stabilizer, inhibitor Sodium glycolate (CAS Reg. No. 9063– Granular and tableted prod- Disintegrant 38–1). ucts only; not to exceed 8% of the formulated product. Sodium sulfate ...... Solid diluent, carrier Sodium sulfite ...... Stabilizer Sodium tripolyphosphate...... Buffer, surfactant, suspending agent, dis- persing agent, anticaking agent, conditioning agent Sorbic acid (CAS Reg. No. 110–44–1) ...... Preservative for formulations Sorbitan fatty acid esters (fatty acids limited to ...... Surfactants, related adjuvants or surfactants. C12, C14, C16, and C18 containing minor amounts of associated fatty acids) and their derivatives; the poly(oxyethylene) content averages 5-20 moles. Soybean flour ...... Expires May 24, 2005...... Surfactant Soybean oil-derived fatty acids ...... Solvent, cosolvent Sperm oil conforming to 21 CFR 172.210 ...... Coating agent Stearic acid ...... Diluent a-Stearoyl-w-hydroxypoly(oxyethylene), average ...... Emulsifier molecular weight (in amu) of 600. a-Stearoyl-w-hydroxypoly(oxyethylene); the ...... Surfactants, related adjuvants of surfactants poly(oxyethylene) content averages either 8, 9, or 40 moles; if a blend of products is used, the average number of moles ethylene oxide reacted to produce any product that is a com- ponent of the blend shall be either 8, 9, or 40. Sucrose octaacetate ...... Adhesive Sulfite liquors and cooking liquors, spent, ...... Surfactant, related adjuvants of surfactants oxidized (CAS Reg. No. 68514–09–0). Sulfuric acid (CAS Reg. No.7664–93–9) ...... Not to exceed 10% of the pH Control agent pesticide formulation; non-aerosol formulations only. Synthetic paraffin and its succinic derivatives ...... Carrier, binder, and carrying agent conforming to 21 CFR 172.275. Synthetic petroleum wax, conforming to 21 CFR ...... Binder, carrier, and coating agent 172.888. Talc ...... Solid diluent, carriers Tall oil; fatty acids not less than 58%, rosin ...... Surfactants, related adjuvants of surfactants acids not more than 44%, unsaponifiables not more than 8%. Tartrazine ...... Dye Terpenes and terpenoids, turpentine oil, alpha- ...... Surfactants, related adjuvants of surfactants pinene fraction, polymd. (CAS Reg. No. 70750–57–1). 1,1,1,2-Tetrafluoroethane, (CAS Reg. No. 811– ...... Aerosol propellant 97–2). Tetrahydrofurfuryl alcohol ...... Solvent cosolvent

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Inert ingredients Limits Uses

a-[p-(1,1,3,3-Tetramethylbutyl)phenyl]-w- ...... Surfactants, related adjuvants of surfactants hydroxypoly(oxyethylene) produced by the condensation of 1 mole of p-(1,1,3,3- tetramethylbutyl)phenol with a range of 1-14 or 30-70 moles of ethylene oxide: if a blend of products is used, the average range number of moles of ethylene oxide reacted to produce any product that is a component of the blend shall be in the range of 1-14 or 30-70. 2,4,7,9-Tetramethyl-5-decyn-4, 7-diol ...... Not more than 2.5% of pes- Surfactants, related adjuvants of surfactants ticide formulation. Tetrasodium pyrophosphate ...... Anticaking agent, conditioning agent Thiosulfuric acid, disodium salt, anhydrous...... Dechlorinator, reducing agent (CAS Reg. No 7772–98–7). Thiosulfuric acid, disodium salt, pentahydrate...... Do. (CAS Reg. No. 10102–17–7). Tricalcium phosphate ...... Surfactant, suspending agent, dispersing agent, anticaking agent, conditioning agent Tridecylpoly(oxyethylene) acetate, sodium salt; ...... Surfactants, related adjuvants of surfactants where the ethylene oxide content averages 6- 7 moles. Trisodium phosphate ...... Surfactant, emulsifier, wetting agent Vermiculite ...... Solid diluent, carrier. Walnut shells ...... Leaching inhibitor, binder for water-dispersible aggregates, sticker and suspension stabilizer Wintergreen oil ...... Attractant Wood flour ...... Derived from wood free of Solid diluent and carrier chemical preservatives. Xanthan gum-modified, produced by the reac- Not more than 0.5% of pes- Surfactant tion of xanthan gum and glyoxal (maximum ticide formulation. 0.3% by weight). Xylene meeting the specifications listed in 21 In pesticide formulations for Solvent, cosolvent CFR 172.884(b)(4). grain storage only. Zeolite (hydrated alkali aluminum silicate) ...... Solid diluent, carrier Zinc oxide ...... Coating agent Zinc sulfate (basic and monohydrate) ...... Do. Zinc sulfate (basic and monohydrate) ...... Solid diluent, carrier

[69 FR 23117, Apr. 28, 2004, as amended at 69 FR 33578, June 16, 2004; 69 FR 34949, June 23, 2004; 69 FR 40786, July 7, 2004; 69 FR 47025, Aug. 4, 2004; 69 FR 58304, 58314, Sept. 30, 2004; 70 FR 28443, 28451, May 18, 2005; 70 FR 31364, June 1, 2005; 70 FR 37692, June 30, 2005; 70 FR 38786, July 6, 2005; 70 FR 43311, July 27, 2005; 70 FR 44496, Aug. 3, 2005; 70 FR 51628, Aug. 31, 2005; 70 FR 54286, Sept. 14, 2005; 70 FR 55296, Sept. 21, 2005; 70 FR 55733, Sept. 23, 2005; 70 FR 67910, Nov. 9, 2005; 71 FR 14414, Mar. 22, 2006; 71 FR 30810, May 31, 2006; 71 FR 43660, Aug. 2, 2006; 71 FR 45421, Aug. 9, 2006]

EFFECTIVE DATE NOTE 1: At 71 FR 45414, Aug. 9, 2006, in § 180.910 the table was amended by revising the entry for Tetrahydrofurfuryl alcohol, effective Feb. 9, 2008. For the convenience of the user, the revised text is set forth as follows:

§ 180.910 Inert ingredients used pre- and post-harvest; exemptions from the requirement of a tolerance.

* * * * *

Inert ingredients Limits Uses

*** * * Tetrahydrofurfuryl alcohol (THFA) (CAS Reg. No 97–99–4) Expires February 9, 2008 Solvent/cosolvent *** * *

EFFECTIVE DATE NOTE 2: At 71 FR 45421, Aug. 9, 2006, in § 180.910 the table was amended by removing the following entries, effective Aug. 9, 2008: a. a-Alkyl (C9-C18-w-hydroxypoly(oxyethylene) with poly(oxyethylene) content of 2-30 moles. b. a-(p-Alkylphenyl)-w-hydroxypoly(oxyethylene) produced by the condensation of 1 mole of alkylphenol (alkyl is a mixture of propylene tetramer and pentamer isomers and averages C13) with 6 moles of ethylene oxide.

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c. a-Alkyl (C6-C14)-w-hydroxypoly(oxypropylene) block copolymer with polyoxyethylene; polyoxypropylene content is 1-3 moles; polyoxyethylene content is 4-12 moles; average molec- ular weight (in amu) is approximately 635. d. a-(p-tert-Butylphenyl)-w-hydroxypoly (oxyethylene) mixture of dihydrogen phosphate and monohydrogen phosphate esters and the corresponding ammonium calcium, magnesium, monoethanolamine, potassium, sodium, and zinc salts of the phosphate esters; the poly(oxyethylene) content averages 4-12 moles. e. a-(o,p-Dinonylphenyl)-w-hydroxypoly (oxyethylene) mixture of dihydrogen phosphate and monohydrogen phosphate esters and the corresponding ammonium, calcium, magnesium, monoethanolamine, potassium, sodium, and zinc salts of the phosphate esters; the nonyl group is a propylene trimer isomer and the poly(oxyethylene) content averages 4-14 moles. f. a-(o,p-Dinonylphenyl)-w-hydroxypoly (oxyethylene) produced by condensation of 1 mole of dinonylphenol (nonyl group is a propylene trimer isomer) with an average of 4-14 or 140- 160 moles of ethylene oxide. g. Dodecylbenzenesulfonic acid, amine salts. h. a-(p-Dodecylphenyl)-w-hydroxypoly (oxyethylene) produced by the condensation of 1 mole of dodecylphenol (dodecyl group is a propylene tetramer isomer) with an average of 4- 14 or 30-70 moles of ethylene oxide; if a blend of products is used, the average number of moles of ethylene oxide reacted to produce any product that is a component of the blend shall be in the range of 4-14 or 30-70. i. Ethylene oxide adducts of 2,4,7,9-tetramethyl-5-decynediol, the ethylene oxide content averages 3.5, 10, or 30 moles. j. a-Lauryl-w-hydroxypoly(oxyethylene), average molecular weight (in amu) of 600. k. a-Lauryl-w-hydroxypoly(oxyethylene) sulfate, sodium salt; the poly(oxyethylene) con- tent is 3-4 moles. l. Manganous oxide. m. a-(p-Nonylphenyl)-w-hydroxypoly(oxyethylene) mixture of dihydrogen phosphate and monohydrogen phosphate esters and the corresponding ammonium, calcium, magnesium, monoethanolamine, potassium, sodium, and zinc salts of the phosphate esters; the nonyl group is a propylene trimer isomer and the poly (oxyethylene) content averages 4-14 moles or 30 moles. n. a-(p-Nonylphenyl)-w-hydroxypoly(oxyethylene) sulfate, ammonium, calcium, magne- sium, potassium, sodium, and zinc salts; the nonyl group is a propylene trimer isomer and the poly(oxyethylene) content averages 4 moles. o. Polyglyceryl phthalate ester of coconut oil fatty acids. p. Poly(methylene-p-tert-butylphenoxy)- poly(oxyethylene) ethanol; the poly(oxyethylene) content averages 4-12 moles. q. Poly(methylene-p-nonylphenoxy)poly(oxyethylene) ethanol; the poly(oxyethylene) con- tent averages 4-12 moles.

r. Secondary alkyl (C11-C15) poly(oxyethylene) acetate, sodium salt; the ethylene oxide con- tent averages 5 moles. s. Sodium diisobutylnaphthalenesulfonate. t. Sodium dodecylphenoxybenzenedisulfonate. u. Sodium isopropylisohexylnaphthalenesulfonate. v. Sodium lauryl glyceryl ether sulfonate.

w. Sodium monoalkyl and dialkyl (C8-C16) phenoxybenzenedisulfonate mixtures containing not less than 70% of the monoalkylated product. x. Sodium mono- and dimethylnaphthalenesulfonates, molecular weight (in amu) 245-260. y. Sodium mono-, di-, and tributyl naphthalenesulfonates. z. Sodium mono-, di-, and triisopropyl naphthalenesulfonate. aa. Sodium N-oleoyl-N-methyltaurine. bb. Sodium sulfite. cc. a-[p-(1,1,3,3-Tetramethylbutyl)phenyl]-w-hydroxypoly(oxyethylene) produced by the con- densation of 1 mole of p-(1,1,3,3-tetramethylbutyl)phenol with a range of 1-14 or 30-70 moles of ethylene oxide: if a blend of products is used, the average range number of moles of ethyl- ene oxide reacted to produce any product that is a component of the blend shall be in the range of 1-14 or 30-70. ee. Tridecylpoly(oxyethylene) acetate, sodium salt; where the ethylene oxide content aver- ages 6-7 moles.

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§ 180.920 Inert ingredients used pre- when used in accordance with good ag- harvest; exemptions from the re- ricultural practice as inert (or occa- quirement of a tolerance. sionally active) ingredients in pesticide The following materials are exempt- formulations applied to growing crops ed from the requirement of a tolerance only:

Inert ingredients Limits Uses

Acetophenone ...... Attractant Adenosine (CAS Reg. No. 58–61–7) ...... Maximum of 0.5% of formu- Synergist lation. Alder bark ...... Seed germination stimulator

a-Alkyl (C12-C18)-w-hydroxypoly(oxyethylene) co- ...... Surfactants, related adjuvants of surfactants polymers with poly(oxypropylene); polyoxyethylene content averages 3-12 moles and polyoxypropylene content 2-9 moles.

a-Alkyl (C10-C16)-w-hydroxypoly(oxyethylene) ...... Surfactants, related adjuvants of surfactants mixture of dihydrogen phosphate and monohydrogen phosphate esters and the cor- responding ammonium, calcium, magnesium, monoethanolamine, potassium, sodium, and zinc salts of the phosphate esters; the poly(oxyethylene) content averages 3-20 moles.

a-Alkyl (C12-C15)-w-hydroxypoly(oxyethylene) Not more than 0.2% in the Emulsifiers in pesticide concentrates applied sulfosuccinate, isopropylamine and N-hy- final solution. with liquid fertilizer solutions before crop droxyethyl isopropylamine salts of; the emerges from soil or not later than 4 weeks poly(oxyethylene) content averages 3-12 after planting moles.

a-Alkyl(C10-C12)-w-hydroxpoly(oxyethylene) ...... Surfactants, related adjuvants of surfactants. poly(oxypropylene) copolymer; poly(oxyethylene) content is 11-15 moles; poly(oxyproplene) content is 1-3 moles.

a-Alkyl(C12-C18)-w-hydroxypoly(oxyethylene/ ...... Do. oxypropylene) hetero polymer in which the oxyethylene content averages 13-17 moles and the oxypropylene content averages 2-6 moles.

a-Alkyl (C10-C16)-w-hydroxypoly (oxy- ...... Do. ethylene)poly(oxypropylene) mixture of di- and monohydrogen phosphate esters and the cor- responding ammonium, calcium, magnesium, monoethanolamine, potassium, sodium, and zinc salts of the phosphate esters; the com- bined poly(oxyethylene) poly(oxypropylene) content averages 3-20 moles.

a-Alkyl (C12-C18)-w-hydroxypoly(oxyethylene/ ...... Do. oxypropylene) hetero polymer in which the oxyethylene content is 8-12 moles and the oxypropylene content is 3-7 moles.

a-Alkyl (C12-C15)-w-hydroxypoly(oxyethylene/ ...... Solvent, cosolvent, surfactant, and related ad- oxypropylene) hetero polymer in which the juvants of surfactants oxyethylene content is 8-13 moles and the oxypropylene content is 7-30 moles.

a-Alkyl (C21-C71)-w-hydroxypoly (oxyethylene) in Not to exceed 10% ...... Wetting agent or granule coating which the poly(oxyethylene) content is 2 to 91 moles and molecular weight range from 390 to 5,000.

n-Alkyl(C8-C18)amine acetate ...... Surfactants, related adjuvants of surfactants Aluminum sulfate ...... Safener adjuvant

Amine salts of alkyl(C8-C24) benzenesulfonic ...... Surfactants, related adjuvants of surfactants acid (butylamine, dimethylaminopropylamine, mono- and diisopropylamine, mono-, di-, and triethanolamine). N-(Aminoethyl) ethanolamine salt of For use only in liquid emul- Do. dodecylbenzenesulfonic acid. sifiable herbicide con- centrates. Ammonium nitrate (CAS Reg. No. 6484–52–2) ...... Adjuvant/ intensifier for herbicides Ammonium polyphosphate (CAS Reg. No...... Sequestrant, buffer, or surfactant 68333–79–9). Barium sulfate ...... Carrier

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Inert ingredients Limits Uses

1,2-Benzisothiazolin-3-one ...... Not more than 0.1% of for- Preservative/stabilizer mulation. Not more than 0.02 lb to be applied per acre. N,N-Bis[a-ethyl-w-hydroxypoly(oxyethylene) ...... Surfactants for preemergence use with herbi- alkylamine; the poly(oxyethylene) content cides on sugarcane only averages 3 moles; the alkyl groups (C14-C18) are derived from tallow, or from soybean or cottonseed oil acids. N,N-Bis(2-hydroxyethyl)alkylamine, where the ...... Surfactants, related adjuvants of surfactants alkyl groups (C8-C18) are derived from coco- nut, cottonseed, soya, or tallow acids. N,N-Bis 2-(w-hydroxypolyoxyethylene) ethyl) ...... Do. alkylamine; the reaction product of 1 mole N,N-bis(2-hydroxyethyl)alkylamine and 3-60 moles of ethylene oxide, where the alkyl group (C8-C18) is derived from coconut, cot- tonseed, soya, or tallow acids. N,N-Bis-2-(w-hydroxypolyoxyethylene/ ...... Surfactant, related adjuvants of surfactants polyoxypropylene) ethyl alkylamine; the reac- tion product of 1 mole of N,N-bis(2-hydroxy- ethyl alkylamine) and 3-60 moles of ethylene oxide and propylene oxide, where the alkyl group (C8-C18) is derived from coconut, cot- tonseed, soya, or tallow acids. Boric acid ...... Sequestrant Buffalo gourd root powder (Cucurbita No more than 2.5 lbs/acre/ Gustatory stimulant foetidissima root powder); or, Zucchini juice season (3.4 gm/acre/sea- (Cucurbita pepo juice) or Hawkesbury melon son of Cucurbitacin). Citrullus lanatus.. Butoxytriethylene glycol phosphate ...... Surfactants for arsenical herbicide formulations only Butyl stearate ...... Defoamer g-Butyrolactone ...... Solvent C.I. Pigment Blue #15 (CAS Reg. No. 147–14– For seed treament use only Dye, coloring agent 8; containing no more than 50 ppm poly- chlorinated biphenyls (PCBs)). C.I. Pigment Green #7 (CAS Reg. No. 1328– For seed treatment use Dye, coloring agent 53–6; containing no more than 50 ppm poly- only. chlorinated biphenyls (PCBs)). C.I. Pigment Violet #23 (CAS Reg. No. 6358– For seed treatment use Dye, coloring agent 30–1; containing no more than 20 ppb of poly- only. chlorinated dibenzo-p-dioxins and/or poly- chlorinated dibenzofurans). Camphor (CAS Reg. No. 76–22–2) ...... Not more than 5% weight to Deodorant, melting point adjustment weight (w/w) of pesticide formulations. Carbonic acid, dipotassium salt (CAS Reg. No...... Buffering agent 584–08–7). Carbonic acid, dipotassium salt, trihydrate (CAS ...... Buffering agent Reg. No. 18662–52–7). Carous chloride ...... 10 ppm in formulation ...... Tagging agent Carrageenan, conforming to 21 CFR 172.260 .... Not more than 0.15% of Thickener and stabilizer for pesticide formula- pesticide formulation. tions applied to seeds before planting Chlorobenzene ...... Contains not more than 1% Solvent, cosolvent impurities. Not for use after edible parts of plant begin to form. Do not graze livestock in treated areas within 48 hours after application. 5-Chloro-2-methyl-4-isothiazolin-3-one (in com- Not more than 0.0022% Preservative bination with 2-methyl-4-isothiazolin-3-one). (22.5 ppm) in the formu- lation; 0.00022% (or 2.25 ppm) in the final solution applied to growing crops. Copper naphthenate ...... Not more than 2.5% of for- Mercaptan scavenger in technical pesticide mulation; application lim- ited to before edible por- tions of plants begin to form. Cyclohexane ...... Solvent, cosolvent Cyclohexanol ...... Do. Cyclohexanone ...... Do.

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Inert ingredients Limits Uses

Cysteine (CAS Reg. No. 52–90–4) ...... Maximum of 0.5% of formu- Synergist lation. D&C Green No. 6 ...... Dye D&C Red No. 17, technical grade ...... Dye D&C Red No. 33 (CAS Reg. No. 3567–66–6); ...... Dye meeting the specifications listed in 21 CFR 74.1333. D&C Violet No. 2, technical grade ...... Not more than 0.005% of Dye pesticide formulation. Decanamide, N,N-dimethyl (CAS Reg. No...... Emulsifier, solvent, cosolvent 14433–76–2). n-Decyl alcohol ...... Dye Diammonium phosphate (CAS Reg. No. 7783– ...... Buffer, surfactant 28–0). a-(Di-sec-butyl)phenylpoly(oxypropylene) block ...... Surfactants, related adjuvants of surfactants polymer with poly(oxyethylene); the poly(oxypropylene) content averages 4 moles, the poly(oxyethylene) content averages 5 to 12 moles, the molecular. Diethanolamine ...... Stabilizer, inhibitor for formulations used before crop emerges from soil Diethylene glycol ...... Deactivator, adjuvant for formulations used be- fore crop emerges from soil Diethylene glycol and diethylene glycol ...... Deactivator for formulations used before crop monobutyl, monoethyl, and monomethyl emerges from soil, stabilizer ethers. 3,6-Dimethyl-4-octyn-3,6-diol ...... In pesticide formulations, Surfactants, related adjuvants of surfactants for soil prior to planting or to plants before edible parts form. Dimethyl sulfoxide ...... Solvent or cosolvent for formulations used be- fore crop emerges from soil or prior to forma- tion of edible parts of food plants Dipotassium hydrogen phosphate ...... Buffering agent Dipropylene glycol monomethyl ether ...... Stabilizer Disodium 4-isodecyl sulfosuccinate ...... Surfactants related adjuvants of surfactants. Dodecylphenol ...... Coupling agent in emulsifier a-Dodecylphenol-w-hydroxypoly(oxyethylene/ ...... Surfactants, related adjuvants of surfactants oxypropylene) hetero polymer where ethylene oxide content is 11-13 moles and oxypropylene content is 14-16 moles, molec- ular weight (in amu) averages 600 to 965. Douglas-fir bark, ground ...... Solid diluent, carrier Dysprosium chloride ...... 10 ppm in formulation ...... Tagging agent Ethylene glycol ...... Antifreeze, deactivator for all pesticides used before crop emerges from soil and in herbi- cides before or after crop emerges Ethylene glycol monobutyl ether ...... 2-Ethylhexanol ...... Cosolvent, defoamer, solvent for all pesticides used before crop emerges from soil and in herbicides before or after crop emerges Europic chloride ...... 10 ppm in formulation ...... Tagging agent FD&C Blue No. 1, methyl-polyethylene glycol For seed treatment use Dye, coloring agent derivative (CAS Reg. No. 9079–34–9). only; Number average molecular weight (in amu) is greater than 1,000; Not to exceed 5% of the for- mulated pesticide product. FD&C Blue No. 1, polyethylene glycol derivative For seed treatment use Dye, coloring agent (CAS Reg. No. 9079–33–8). only; Number average molecular weight (in amu) is greater than 1,000; Not to exceed 5% of the for- mulated pesticide product. FD&C Red No. 40 (CAS Reg. No. 25956–17–6) For seed treatment use Dye, coloring agent only. Not to exceed 2% by weight of the pesticide formulation. Ferric chloride ...... Not greater than 2% of suspending, dispersing agent, pesticide formulation Fluoroapatite ...... Solid diluent, carrier Folic acid (CAS Reg. No. 59–30–3) ...... Maximum of 0.5% of formu- Synergist lation. Gluconic acid (and sodium salt) ...... Sequestrant

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Inert ingredients Limits Uses

l-Glutamic acid (C5 H9 NO4´ CAS Reg. No. 56– Seet treatment use only ..... Plant nutrient 86–0). [alpha]-D-glucopyranoside, 2-ethylhexyl 6-O- ...... Surfactant [alpha]-D glucopyranosyl- (CAS Reg. No. 330980–61–5). [alpha]-D-glucopyranoside, 2-ethylhexyl (CAS ...... Surfactant Reg. No. 125590–73–0). Glutamine (CAS Reg. No. 56–85–9) ...... Maximum of 0.5% of formu- Synergist lation. Glycerol—propylene oxide polymer (CAS Reg...... Component in water-soluble film No. 25791-96-2). Glyceryl triacetate ...... Stabilizer Glyceryl tris-12-hydroxystearate ...... Flow control agent Graphite ...... Treatment aid for seeds Hexamethylenetetramine ...... Stabilizer for carriers in solid pesticide formula- tions 2-Hydroxy-4-n-octoxybenzophenone (CAS Reg. Not more than 0.2 pt of Light stabilizer No. 1843–05–6). pesticide formulation. Hydroxypropyl guar gum ...... Thickener Isobornyl acetate ...... Solvent Isobutyl alcohol ...... Do. Isobutylene-butene copolymers ...... For soil application only ...... Binder Isooctadecanol ...... Not more than 2% of pes- Defoaming agent ticide formulation. Isopropylbenzenesulfonic acid and its ammo- ...... Surfactants and related adjuvants of nium, calcium, magnesium, potassium, so- surfactants dium, and zinc salts. Lanthanum chloride ...... 10 ppm in formulation ...... Tagging agent. (3-Lauramidopropyl) trimethylammonium methyl Not more than 2.6% in the Antistatic agent sulfate. formulation. Not to be ap- plied within 7 days of har- vest. Linoleic diethanolamide (CAS Reg. No. 56863– ...... Surfactant 02–6). Magnesium nitrate (in combination with 2-meth- None ...... Preservation yl-4-isothiazolin-3-one and 5-chloro-2-methyl- 4-isothiazolin-3-one). Maleic acid and maleic anhydride ...... For pesticide formulations Stabilizer applied to apples with a minimum preharvest in- terval of 21 days. Manganese carbonate ...... Plant nutrient Mesityl oxide ...... Not for use after edible Solvent, cosolvent parts of plant begin to form. Do not graze live- stock in treated areas within 48 hours after ap- plication. Methionine (CAS Reg. No. 59–51–8) ...... Maximum of 0.5% of formu- Synergist lation. Methyl alcohol ...... Do. Methyl bis(2-hydroxyethyl)alkyl ammonium chlo- ...... Surfactant ride, where the carbon chain (C8-C18) is de- rived from coconut, cottonseed, soya, or tal- low acids. a,a′-[Methylenebis]-4-(1,1,3,3-tetramethylbutyl)- ...... Solvent, cosolvent, surfactant, and related ad- o-phenylene bis[w-hydroxypoly(oxyethylene)] juvants of surfactants having 6-7.5 moles of ethylene oxide per hydroxyl group. Methyl ethyl ketone ...... Surfactant Methyl p- hydroxybenzoate ...... Preservative for formulations Methyl isobutyl ketone ...... Solvent, cosolvent 2-Methyl-4-isothiazolin-3-one (in combination Not more than 0.0022% Preservative with 5-chloro-2-methyl-4-isothiazolin-3-one). (22.5 ppm) in the formu- lation; 0.00022% (or 2.25 ppm) in the final solution applied to growing crops. Methylnaphthalenesulfonic acid—formaldehyde ...... Dispersant condensate, sodium salt. Methyl oleate ...... Surfactant 2-Methyl-2,4-pentanediol ...... Solvent for formulations used before crop emerges from soil

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Inert ingredients Limits Uses

Methyl poly(oxyethylene) alkyl ammonium chlo- ...... Surfactant ride, where the poly(oxyethylene) content is 3- 15 moles and the alkyl group (C8-C18) is de- rived from coconut, cottonseed, soya, or tal- low acids. N-Methylpyrrolidone (CAS Reg. No. 872-504) ...... Solvent, cosolvent Methyl violet 2B ...... Dye Mixed phytosterols (consisting of campesterol, ...... Surfactant. sitosterol and stigmasterol, with minor amounts of associated plant sterols) derived from edible vegetable oils. Mono- and bis-(1H, 1H, 2H, 2H-perfluoroalkyl) Not more than 0.5% of pes- Defoaming agent phosphates where the alkyl group is even ticide formulation. numbered and in the C6-C12 range. Mono- and dialkyl (C8-C18) methylated ammo- ...... Surfactants, related adjuvants of surfactants nium chloride compounds, where the alkyl group(s) (C8-C18) are derived from coconut, cottonseed, soya, tallow, or hogfat fatty acids. Morpholine salt of dodecylbenzenesulfonic acid ...... Do. Naphthalenesulfonic acid-formaldehyde conden- ...... Do. sate, ammonium and sodium salts. Nicotinamide (CAS Reg. No. 98–92–0) ...... Maximum of 0.5% of formu- Synergist lation. a-(p-Nonylphenyl)-w-hydroxypoly(oxyethylene); ...... Surfactant produced by the condensation of 1 mole of nonylphenol (nonyl group is a propylene trimer isomer) with an average of 4-14 or 30- 100 moles of ethylene oxide; if a blend of products is used, the average number of moles of ethylene oxide reacted to produce any product that is a component of the blend shall be in the range 4-14 or 30-100. Octanamide, N,N-dimethyl (CAS Reg. No...... Emulsifier, solvent, cosolvent 1118–92–9). n- Octyl alcohol ...... Solvent, cosolvent a-Oleoyl-w-(oleoyloxy) poly(oxyethylene) derived ...... Component of defoamers from a-hydro-w-hydroxypoly(oxyethylene) (molecular weight 600 amu). Oxo-decyl acetate (CAS reg. No. 108419–33–6) ...... Solvent Oxo-heptyl acetate (CAS Reg. No. 90438–79–2) ...... Solvent Oxo-hexyl acetate (CAS Reg. No. 88230–35–7) ...... Solvent Oxo-nonyl acetate (CAS Reg. No. 108419–34– ...... Solvent 7). Oxo-octyl acetate (CAS Reg. No. 108419–32–5) ...... Solvent Oxo-tridecyl acetate (CAS Reg. No. 108419– ...... Solvent 35–8). Partial sodium salt of N- lauryl-a- Not more than 1% of pes- Surfactants, related adjuvants of surfactants iminodipropionic acid. ticide formulation. Phenol ...... Solvent, cosolvent Phenolsulfonic acid—formaldehyde—urea con- Applied to growing plants Dispersant surfactant densate and its sodium salt. only. (Phthalocyaninato (2)) copper; (C.I. pigment When used as a colorant in Coloring agent, pigment blue No. 15). low-density plastic films. Pigment red 48 ...... For seed treatment use Dye only. a-Pinene ...... Not more than 2% of formu- Stabilizer lation by weight. Poly(methylene-p- ...... Encapsulating agent nonylphenoxy)poly(oxypropylene) propanol; the poly(oxy-propylene) content averages 4- 12 moles. Poly(oxyethylene) adducts of mixed phytosterols ...... Surfactant, related adjuvants (such sterols to consist of campesterol, stig- masterol and sitosterol with minor amounts of associated plant sterols) derived from edible vegetable oils; polyoxyethylene content aver- aging 5-26 moles. Poly(oxyethylene) (5) sorbitan monooleate ...... Surfactants, related adjuvants of surfactants Polysorbate 60, conforming to 21 CFR 172.836 ...... Surfactant Potassium dihydrogen phosphate ...... Buffering agent Primary n-alkylamines, where the alkyl group ...... Surfactant (C8-C18) is derived from coconut, cottonseed, soya, or tallow acids.

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Inert ingredients Limits Uses

2-Propanamine, compound with a-phosphono-w- Not more than 15% in the Surfactant butoxypoly (oxy-1,2-ethanediyl) (2:1) (CAS formulated product. Reg. No. 431040–31–2). 2-Propanamine, compounds with polyethylene Not more than 15% in the Surfactant glycol dihydrogen phosphate C8– 10- alkyl formulated product. ether (2:1) (CAS Reg. No. 431062–72–5). Propylene glycol monomethyl ether ...... Solvent Pyridoxine (CAS Reg. No. 65–23–6) ...... Maximum of 0.5% of formu- Synergist lation. Rosin, dark wood (as defined in 21 CFR ...... Surfactants, related adjuvants of surfactants 178.3870(a)(1)(v)). Rosin, gum ...... Do. Rosin, tall oil ...... Do. Scandium chloride ...... 10 ppm in formulation ...... Tagging agent Sodium bisulfate (CAS Reg. No. 7681–38–1) ...... Acidifying/buffering agent Sodium 1,4-dicyclohexyl sulfosuccinate ...... Surfactants, related adjuvants of surfactants Sodium 1,4-dihexyl sulfosuccinate ...... Do. Sodium dihydrogen phosphate (CAS Reg. No...... Buffering agent 7558–80–7) conforming to 21 CFR 182.6778. Sodium 1,4-diisobutyl sulfosuccinate ...... Surfactants, related adjuvants of surfactants Sodium 1,4-dipentyl sulfosuccinate ...... Do. Sodium 1,4-ditridecyl sulfosuccinate ...... Do. Sodium metaborate ...... Sequestrant Sodium molybdate ...... Plant nutrient Sodium nitrate ...... Solid diluent Sodium nitrite ...... Not more than 3% of pes- Stabilizer, inhibitor. ticide formulation. Sodium o-phenylphenate ...... Not more than 0.1% of pes- Preservative for formulation ticide formulation. Sodium salt of the insoluble fraction of rosin ...... Surfactants, related adjuvants of surfactants Sodium tetraborate ...... Not more than 2% of pes- Buffering agent; corrosion inhibitor ticide formulation. Sulfosuccinic acid ester with N-(2,-hydroxy- Not more than 0.2% in the Emulsifiers in pesticide concentrates applied propyl) oleamide, ammonia and final solution. with liquid fertilizer solutions before crop isopropylamine salts of. emerges from soil or not later than 4 weeks after planting Tall oil diesters with polypropylene glycol (CAS ...... Component in water-soluble film Reg. No. 68648–12–4). Tannin ...... Dispersing agent Tertiary butylhydroquinone ...... Antioxidant 1-Tetradecanamine, N,N-dimethyl-, N-oxide ...... Component in water-soluble film (CAS Reg. No. 3332–27–2). N,N,N′,N″-Tetrakis-(2-hydroxypropyl) ethylene- ...... Stabilizer for formulations used before crop diamine. emerges from soil a-[p-(1,1,3,3-Tetramethylbutyl)phenyl]-w- ...... Surfactants, related adjuvants of surfactants hydroxypoly(oxyethylene) mixture of dihydro- gen phosphate and monohydrogen phosphate esters and the corresponding sodium salts of the phosphate esters; the poly(oxyethylene) content averages 6 to 10 moles. 2,4,7,9-Tetramethyl-5-decyne 4,7-diol ...... In pesticide formulations, Do. for application to soil prior to planting or to plants before edible parts form. Tetrapotassium pyrophosphate (CAS Reg. No. Not to exceed 10% of for- Sequestrant, anticaking agent, conditioning 7320–345). mulation. agent Titanium dioxide (CAS Reg. No. 13463–67–7) ...... Pigment/coloring agent in plastic bags used to wrap growing banana (preharvest), colorant on seeds for planting Toluenesulfonic acid and its ammonium, cal- ...... Solvent, cosolvent cium, magnesium, potassium, sodium, and zinc salts. Triethanolamine ...... Stabilizer, inhibitor for formulations used before crop emerges from soil Triethylene glycol ...... Deactivator Triethyl phosphate ...... Stabilizer for formulations used before crop emerges from soil Trimethylolpropane (CAS Reg. No. 77–99–6) .... Not to exceed 15% by Component in water-soluble film weight of the film. a-[2,4,6-Tris[1-(phenyl)ethyl]phenyl]-w-hydroxy Not more than 15% of the Surfactant. poly(oxyethylene), the poly(oxyethylene) con- formulation. tent averages 4-150 moles).

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Inert ingredients Limits Uses

a-[2,4,6-Tris[1-(phenyl)ethyl]phenyl]-w-hydroxy Not more than 15% of the Do. poly(oxyethylene); mixture of monohydrogen formulation. and dihydrogen phosphate esters and the cor- responding ammonium, calcium, magnesium, potassium, sodium, and zinc salts, the poly(oxyethylene) content averages 4-150 moles). a-[2,4,6-Tris[1-(phenyl)ethyl]phenyl]-w-hydroxy Not more than 15% of the Do. poly(oxyethylene) sulfate, and the cor- pesticide formulation. responding ammonium, calcium, magnesium, potassium, sodium, and zinc salts, the poly(oxyethylene) content averages 4-150 moles. Tryptophan (CAS Reg. No. 73–22–3) ...... Maximum of 0.5% of formu- Synergist lation. Valeric acid, normal ...... Not more than 2% in pes- Stenching agent or odorant ticide formulations. Xylene ...... Solvent, cosolvent Xylenesulfonic acid its ammonium calcium, mag- ...... Surfactants, related adjuvants of surfactants nesium, potassium, sodium, and zinc salts. Yucca extract from Yucca schidigera ...... Wetting agent Ytterbium chloride ...... 10 ppm in formulation ...... Tagging agent Yttrium chloride ...... 10 ppm in formulation ...... Tagging agent Zinc orthophosphate ...... Plant nutrient and safener Zinc stearate, conforming to 21 CFR 182.5994 ...... Flow control agent and 582.5994.

[69 FR 23124, Apr. 28, 2004, as amended at 70 FR 7900, Feb. 16, 2005; 70 FR 31369, June 1, 2005; 70 FR 41619, July 20, 2005; 70 FR 54280, Sept. 14, 2005; 70 FR 55296, Sept. 21, 2005; 70 FR 55733, Sept. 23, 2005; 71 FR 14415, Mar. 22, 2006; 71 FR 18642, Apr. 12, 2006; 71 FR 30811, May 31, 2006; 71 FR 43667, Aug. 2, 2006; 71 FR 45408, 45421, Aug. 9, 2006]

EFFECTIVE DATE NOTE 1: At 71 FR 45411, Aug. 9, 2006, in § 180.920 the table was amended by revising the following inert ingredient, effective Feb. 9, 2008. For the convenience of the user, the revised text is set forth as follows:

§ 180.920 Inert ingredients used pre-harvest; exemptions from the requirement of a tolerance.

* * * * *

Inert ingredients Limits Uses

*** * * Mono- and bis-(1H, 1H, 2H, 2H-perfluoroalkyl) phosphates Not more than 0.5% of pes- Surfactant, related adjvants of where the alkyl group is even numbered and in the C6- ticide formulation. Expires surfactants C12 range. February 9, 2008. *** * *

EFFECTIVE DATE NOTE 2: At 71 FR 45421, Aug. 9, 2006, in § 180.920 the table was amended by removing the following entries, effective Aug. 9, 2008. a. a-Alkyl (C12-C18)-w-hydroxypoly(oxyethylene) copolymers with poly(oxypropylene); polyoxyethylene content averages 3-12 moles and polyoxypropylene content 2-9 moles. b. a-Alkyl (C10-C16)-w-hydroxypoly(oxyethylene) mixture of dihydrogen phosphate and monohydrogen phosphate esters and the corresponding ammonium, calcium, magnesium, monoethanolamine, potassium, sodium, and zinc salts of the phosphate esters; the poly(oxyethylene) content averages 3-20 moles. c. a-Alkyl (C12-C15)-w-hydroxypoly(oxyethylene) sulfosuccinate, isopropylamine and N-hy- droxyethyl isopropylamine salts of; the poly(oxyethylene) content averages 3-12 moles. d. a-Alkyl(C10-12)-w-hydroxpoly(oxyethylene) poly(oxypropylene) copolymer; poly(oxyethylene) content is 11-15 moles; poly(oxyproplene) content is 1-3 moles. e. a-Alkyl(C12-C18)-w-hydroxypoly (oxyethylene/oxypropylene) hetero polymer in which the oxyethylene content averages 13-17 moles and the oxypropylene content averages 2-6 moles. f. a-Alkyl (C10-C16)-w-hydroxypoly(oxyethylene)poly(oxypropylene) mixture of di- and monohydrogen phosphate esters and the corresponding ammonium, calcium, magnesium, monoethanolamine, potassium, sodium, and zinc salts of the phosphate esters; the combined poly(oxyethylene) poly(oxypropylene) content averages 3-20 moles. g. a-Alkyl (C12-C18)-w-hydroxypoly(oxyethylene/oxypropylene) hetero polymer in which the oxyethylene content is 8-12 moles and the oxypropylene content is 3-7 moles.

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h. a-Alkyl (C12-C15)-w-hydroxypoly(oxyethylene/oxypropylene) hetero polymer in which the oxyethylene content is 8-13 moles and the oxypropylene content is 7-30 moles.

i. a-Alkyl (C21-C71)-w-hydroxypoly (oxyethylene) in which the poly(oxyethylene) content is 2 to 91 moles and molecular weight range from 390 to 5,000.

j. n-Alkyl(C8-C18)amine acetate. k. Amine salts of alkyl (C8-C24) benzenesulfonic acid (butylamine, dimethylaminopropylamine, mono- and diisopropylamine, mono- , di- , and triethanolamine). l. N-(Aminoethyl) ethanolamine salt of dodecylbenzenesulfonic acid. m. N,N-Bis[a-ethyl-w-hydroxypoly(oxyethylene) alkylamine; the poly(oxyethylene) content averages 3 moles; the alkyl groups (C14-C18) are derived from tallow, or from soybean or cot- tonseed oil acids.

n. N,N-Bis(2-hydroxyethyl)alkylamine, where the alkyl groups (C8-C18) are derived from co- conut, cottonseed, soya, or tallow acids. o. N,N-Bis 2-(w-hydroxypolyoxyethylene) ethyl) alkylamine; the reaction product of 1 mole N,N-bis(2-hydroxyethyl)alkylamine and 3-60 moles of ethylene oxide, where the alkyl group (C8-C18) is derived from coconut, cottonseed, soya, or tallow acids. p. N,N-Bis-2-(w-hydroxypolyoxyethylene/polyoxypropylene) ethyl alkylamine; the reaction product of 1 mole of N,N-bis(2-hydroxyethyl alkylamine) and 3-60 moles of ethylene oxide and propylene oxide, where the alkyl group (C8-C18) is derived from coconut, cottonseed, soya, or tallow acids. q. Butoxytriethylene glycol phosphate. r. Cyclohexanol. s. a-(Di-sec-butyl)phenylpoly(oxypropylene) block polymer with poly(oxyethylene); the poly(oxypropylene) content averages 4 moles, the poly(oxyethylene) content averages 5 to 12 moles, the molecular. t. Disodium 4-isodecyl sulfosuccinate. u. Dodecylphenol. v. a-Dodecylphenol-w-hydroxypoly(oxyethylene/oxypropylene) hetero polymer where ethyl- ene oxide content is 11-13 moles and oxypropylene content is 14-16 moles, molecular weight (in amu) averages 600 to 965. w. Isopropylbenzenesulfonic acid and its ammonium, calcium, magnesium, potassium, so- dium, and zinc salts. x. (3-Lauramidopropyl) trimethylammonium methyl sulfate. y. Linoleic diethanolamide (CAS Reg. No. 56863–02–6).

z. Methyl bis(2-hydroxyethyl)alkyl ammonium chloride, where the carbon chain (C8-C18) is derived from coconut, cottonseed, soya, or tallow acids. aa. a,a′-[Methylenebis]-4-(1,1,3,3-tetramethylbutyl)-o-phenylene bis[w- hydroxypoly(oxyethylene)] having 6-7.5 moles of ethylene oxide per hydroxyl group. bb. Methylnaphthalenesulfonic acid—formaldehyde condensate, sodium salt. cc. Methyl poly(oxyethylene) alkyl ammonium chloride, where the poly(oxyethylene) con- tent is 3-15 moles and the alkyl group (C8-C18) is derived from coconut, cottonseed, soya, or tallow acids. dd. Methyl violet 2B. ee. Morpholine salt of dodecylbenzenesulfonic acid. ff. Naphthalenesulfonic acid-formaldehyde condensate, ammonium and sodium salts. gg. Partial sodium salt of N-lauryl-a-iminodipropionic acid. hh. Poly(methylene-p-nonylphenoxy)poly(oxypropylene) propanol; the poly(oxy-propylene) content averages 4-12 moles.

ii. Primary n-alkylamines, where the alkyl group (C8-C18) is derived from coconut, cotton- seed, soya, or tallow acids. kk. Sodium 1,4-dicyclohexyl sulfosuccinate. ll. Sodium 1,4-dihexyl sulfosuccinate. mm. Sodium 1,4-diisobutyl sulfosuccinate. nn. Sodium 1,4-dipentyl sulfosuccinate. oo. Sodium 1,4-ditridecyl sulfosuccinate. qq. Sulfosuccinic acid ester with N-(2,-hydroxy-propyl) oleamide, ammonia and isopropylamine salts of. rr. Tall oil diesters with polypropylene glycol (CAS Reg. No. 68648–12–4). ss. N,N,N′,N′′-Tetrakis-(2-hydroxypropyl) ethylenediamine. tt. a-[p-(1,1,3,3-Tetramethylbutyl)phenyl]-w-hydroxypoly(oxyethylene) mixture of dihydro- gen phosphate and monohydrogen phosphate esters and the corresponding sodium salts of the phosphate esters; the poly(oxyethylene) content averages 6 to 10 moles.

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§ 180.930 Inert ingredients applied to when used in accordance with good ag- animals; exemptions from the re- ricultural practice as inert (or occa- quirement of a tolerance. sionally active) ingredients in pesticide The following materials are exempt- formulations applied to animals: ed from the requirement of a tolerance

Inert ingredients Limits Uses

Acetic acid (CAS Reg. No. 64–19–7) ...... Not more than 0.5% of pes- Catalyst ticide formulation. Acetic anhydride ...... Solvent, cosolvent, stabilizer Alkanoic and alkenoic acids, mono- and diesters ...... Emulsifiers of a-hydro-w-hydroxypoly(oxyethylene) with molecular weight (in amu) range of 200 to 6,000. Alkyl (C8-C24) benzenesulfonic acid and its am- ...... Surfactants, emulsifier, related adjuvants of monium, calcium, magnesium, potassium, so- surfactants dium, and zinc salts. a-Alkyl (C9-C18)-w-hydroxy poly(oxyethylene): ...... Solvent, cosolvent, surfactant, and related ad- the poly(oxyethylene) content averages 2-20 juvants of surfactants moles. a-Alkyl (C12- C15)-w-hydroxypoly(oxyethylene/ ...... Solvent, cosolvent, surfactant, and related ad- oxypropylene) hetero polymer in which the juvants of surfactants oxyethylene content is 8-13 moles and the oxypropylene content is 7-30 moles. a-Alkyl (C8-C10) hydroxypoly(oxypropylene) ...... Do. block polymer with polyoxyethylene; polyoxypropylene content averages 3 moles and polyoxyethylene content averages 5-12 moles. a-Alkyl (C6-C14)-w-hydroxypoly(oxypropylene) ...... Surfactants, related adjuvants of surfactants block copolymer with polyoxyethylene; polyoxypropylene content is 1-3 moles; polyoxyethylene content is 7-9 moles; average molecular weight (in amu) approximately 635. a-alkyl (C12-C15)-w-hydroxypoly Not to exceed 20% of pes- Surfactant (oxypropylene)poly (oxyethylene)copolymers ticide formulations (where the poly(oxypropylene) content is 3-60 moles and the poly(oxyethylene) content is 5- 80 moles), the resulting ethoxylated propoxylated (C12-C15) alcohols having a min- imum molecular weight (in amu) of 1,500, CAS Reg. No. 68551–13–3. a-(p- Alkylphenyl)-w-hydroxypoly (oxyethylene) ...... Do. produced by the condensation of 1 mole of alkylphenol (alkyl is a mixture of propylene tetramer and pentamer isomers and averages C13) with 6 moles of ethylene oxide. Alkyl (C8-C18) sulfate and its ammonium, cal- ...... Do. cium, magnesium, potassium, sodium, and zinc salts. Amine salts of alkyl (C8-C24) benzenesulfonic ...... Do. acid (butylamine; dimethylamino propylamine; mono- and diisopropyl- amine; and mono-, di-, and triethanolamine). Ascorbyl palmitate ...... Preservative Attapulgite-type clay ...... Solid diluent, carrier Barium sulfate (CAS Reg. No. 7727–43–7) ...... Carrier, density control agent Benzoic acid ...... Preservative for formulations 2-Bromo-2-nitro-1,3-propanediol (CAS Reg. No. 0.04% or less by weight of In-can preservative 52–51–7). the total pesticide formu- lation. Butane ...... Propellant n-Butanol (CAS Reg. No. 71–36–3) ...... Solvent for blended emulsifiers Butylated hydroxyanisole ...... Antioxidant Butylated hydroxytoluene ...... Do. a-(p-tert- Butylphenyl)-w-hydroxypoly (oxy- ...... Surfactants, related adjuvants of surfactants ethylene) mixture of dihydrogen phosphate and monohydrogen phosphate esters and the corresponding ammonium, calcium, magne- sium, monoethanolamine, potassium, sodium, and zinc salts of the phosphate esters; the poly(oxyethylene) content averages 4-12 moles.

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Inert ingredients Limits Uses

Calcium carbonate ...... Solid diluent, carrier Calcium chloride ...... Stabilizer Calcium silicate, hydrated calcium silicate ...... Anticaking agent, solid diluent, carrier Calcium stearate (CAS Reg. No. 1592–23–0) ...... Stabilizer, component of plastic animal tag Calcium sulfate ...... Solid diluent, carrier Carbon black (CAS Reg. No. 1333–86–4) ...... Colorant/pigment in animal tag Carrageenan, conforming to 21 CFR 172.620 .... Minimum molecular weight Thickener (in amu): 100,000. Cyclohexanone ...... Solvent, cosolvent D&C Green No. 6 ...... Dye, coloring agent D&C Red No. 17 ...... Do. D&C Violet No. 2 ...... Do. Dialkyl (C8-C18) dimethylammonium chloride ...... Not more than 0.2% in sili- Flocculating agent in the manufacture of silica ca hydrated silica. hydrated silica for use as a solid diluent, car- rier Diatomite (diatomaceous earth) ...... Solid diluent, carrier Diethylphthalate ...... Solvent, cosolvent 1,1-Difluoroethane (CAS Reg. No. 75–37–6) ..... For aerosol pesticide formu- Aerosol propellant lations used for insect control in food- and feed- handling establishments and animals. Dimethyl ether (CAS Reg. No. 115–10–6) ...... Propellant 3,6-Dimethyl-4-octyne-3,6-diol ...... Not more than 2.5% of pes- Surfactants, related adjuvants of surfactants ticide formulation. Dimethylpolysiloxane (CAS Reg. No. 9016–00– ...... Defoaming agent 6). a-(o,p-Dinonylphenyl)-w-hydroxypoly (oxy- ...... Surfactants, related adjuvants of surfactants ethylene) mixture of dihydrogen phosphate and monohydrogen phosphate esters and the corresponding ammonium, calcium, magne- sium, monoethanolamine, potassium, sodium, and zinc salts of the phosphate esters; the nonyl group is a propylene trimer isomer and the poly(oxyethylene) content averages 4-14 moles. a-(o,p-Dinonylphenyl)-w-hydroxypoly (oxy- ...... Do. ethylene), produced by the condensation of 1 mole of dinonylphenol (nonyl group is a pro- pylene trimer isomer) with an average of 4-14 moles of ethylene oxide. Dipropylene glycol monomethyl ether ...... Do. Dodecylbenzenesulfonic acid, amine salts ...... Do. a-(p-Dodecylphenyl)-w-hydroxypoly (oxy- ...... Surfactants, emulsifier ethylene) produced by the condensation of 1 mole of dodecylphenol (dodecyl group is a propylene tetramer isomer) with an average of 4-14 or 30-70 moles of ethylene oxide; if a blend of products is used, the average num- ber of moles of ethylene oxide reacted to produce any product that is a component of the blend shall be in the range of 4-14 or 30- 70 moles. Epoxidized soybean oil (CAS Reg. No. 8013– ...... Stabilizer, plasticizer, component animal tag 07–8). Ethyl alcohol ...... Solvent, cosolvent Ethyl maltol (CAS Reg. No.4940–11–8) ...... Not more than 0.2 % of the Odor masking agent pesticide formulation. Ethylene oxide adducts of 2,4,7,9-tetramethyl-5- ...... Surfactants, related adjuvants of surfactants decynediol, the ethylene oxide content aver- ages 3.5, 10, or 30 moles. 2-Ethyl-1-hexanol ...... Not more than 2.5% of pes- Solvent, adjuvant of surfactants ticide formulation. FD&C Blue No. 1 ...... Dye, coloring agent FD&C Yellow No. 6 Aluminum Lake (CAS Reg. Not more than 2% by Pigment in animal tag and similar slow-release No. 15790–07–5). weight of pesticide formu- devices lation. D-glucopyranose, oligomeric, C10–16-alkyl ...... Surfactant glycosides (CAS Reg. No. 110615–47–9). Glycerol monooleate ...... Surfactants, related adjuvants of surfactants Glyceryl monostearate ...... Emulsifier Glyceryl tris-12-hydroxystearate ...... Flow control agent Graphite ...... Solid diluent, carrier n-Hexyl alcohol (CAS Reg. No. 111–27–3) ...... Solvent, cosolvent

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Inert ingredients Limits Uses

2-(2′-Hydroxy-5′-methylphenyl)benzotriazole Not more than 0.5% by Ultraviolet light absorber/stabilizer in animal tag (CAS Reg. No. 2440–22–4). weight of pesticide formu- and similar slow-release devices lation. Iron oxide (CAS Reg. No. 1309–37–1) ...... Colorant in pesticide formulations for animal tags Isopropyl myristate, CAS Reg. No. 110–27–0 ...... Solvent Kaolinite-type clay ...... Solid diluent, carrier Kerosene, U.S.P. reagent ...... Solvent, cosolvent Lactic acid ...... Solvent Lactic acid, 2-ethylhexyl ester (CAS Reg. No...... Solvent 6283–86–9). Lactic acid, 2-ethylhexyl ester, (2S)- (CAS Reg...... Solvent No. 186817–80–1). Lactic acid, n-propyl ester, (S); (CAS Reg. No...... Solvent 53651–69–7). a-Lauryl-w-hydroxypoly(oxyethylene), average ...... Emulsifier molecular weight (in amu) of 600. a-Lauryl-w-hydroxypoly(oxyethylene) sulfate, so- ...... Surfactants, related adjuvants of surfactants dium salt; the poly(oxyethylene) content is 3-4 moles. Lignin (CAS Reg. No. 9005–53–2) ...... Surfactant, related adjuvants of surfactants Lignin, alkali (CAS Reg. No. 8068–05–1) ...... Do. Lignin, alkali, oxidized, sodium salt (CAS Reg...... Do. No. 68201–23–0). Lignin alkali reaction products with disodium sul- ...... Do. fite and formaldehyde (CAS Reg. No. 105859–97–0). Lignin alkali reaction products with formaldehyde ...... Do. and sodium bisulfite (CAS Reg. No. 68512– 35–6). Lignosulfonic acid (CAS Reg. No. 8062–15–5) ...... Do. Lignosulfonic acid, ammonium calcium salt ...... Do. (CAS Reg. No. 12710–04–2). Lignosulfonic acid, ammonium magnesium salt ...... Do. (CAS Reg. No. 123175–37–1). Lignosulfonic acid, ammonium salt (CAS Reg...... Do. No. 8061–53–8). Lignosulfonic acid, ammonium sodium salt (CAS ...... Do. Reg. No. 166798–73–8). Lignosulfonic acid, calcium magnesium salt ...... Do. (CAS Reg. No. 55598–86–2). Lignosulfonic acid, calcium salt (CAS Reg. No...... Do. 8061–52–7). Lignosulfonic acid, calcium sodium salt (CAS ...... Do. Reg. No. 37325–33–0). Lignosulfonic acid, ethoxylated, sodium salt ...... Do. (CAS Reg. No. 68611–14–3). Lignosulfonic acid, magnesium salt (CAS Reg...... Do. No. 8061–54–9). Lignosulfonic acid, potassium salt (CAS Reg...... Do. No. 37314–65–1). Lignosulfonic acid, sodium salt (CAS Reg. No...... Do. 8061–51–6). Lignosulfonic acid, sodium salt, oxidized (CAS ...... Do. Reg. No. 68855–41–4). Lignosulfonic acid, sodium salt, polymer with ...... Do. formaldehyde and phenol (CAS Reg. No. 37207–89–9). Lignosulfonic acid, sodium salt, sulfomethylated ...... Do. (CAS Reg. No. 68512–34–5). Lignosulfonic acid, zinc salt (CAS Reg. No...... Do. 57866–49–6). d-Limonene (CAS Reg. No. 5989–27–5) ...... Solvent, fragrance Magnesium carbonate ...... Solid diluent, carrier Magnesium silicate, hydrated magnesium sili- ...... Do. cate. Manganous oxide ...... Do. Methyl alcohol ...... Solvent, cosolvent Methyl n-amyl ketone (CAS Reg. No. 110–43–0) ...... Solvent, cosolvent Methyl esters of higher fatty acids conforming to ...... Antidusting agent 21 CFR 573.640.

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Inert ingredients Limits Uses

Methyl-p-hydroxybenzoate (Methyl paraben) ...... Meets specifications of Preservative Food Chemicals Codex; not to exceed 0.1% in formulations. Methyl isobutyl ketone ...... Solvent, cosolvent Mineral oil, U.S.P., or conforming to 21 CFR ...... Solvent, diluent 172.878 or 178.3620(a), (b). Mono-, di-, and trimethylnaphthalenesulfonic Not to exceed 0.006% in Dispersing-wetting agent in dip vat operations acids-formaldehyde condensates, sodium final formulation. for large animals, such as cattle salts. Montmorillonite-type clay ...... Solid diluent, carrier Naphthalenesulfonic acid and its sodium salt ...... Surfactants, related adjuvants of surfactants Nonyl, decyl, and undecyl glycoside mixture with ...... Surfactant a mixture of nonyl, decyl, and undecyl oligosaccharides and related reaction prod- ucts (primarily decanol and undecanol) pro- duced as an aqueous-based liquid (50 to 65% solids) from the reaction of primary alcohols (containing 15 to 20% secondary alcohol iso- mers) in a ratio of 20% C9, 40% C10, and 40% C11 with carbohydrates (average glucose to alkyl chain ratio 1.3 to 1.8). a-(p-Nonylphenyl)-w-hydroxypoly(oxyethylene) ...... Surfactants, related adjuvants of surfactants mixture of dihydrogen phosphate and monohydrogen phosphate esters and the cor- responding ammonium, calcium, magnesium, monoethanolamine, potassium, sodium, and zinc salts of the phosphate esters; the nonyl group is a propylene trimer isomer and the poly(oxyethylene) content averages 4-14 moles. a-(p-Nonylphenyl)-w-hydroxypoly(oxyethylene) ...... Surfactants, emulsifier, related adjuvants of produced by the condensation of 1 mole of surfactants. nonylphenol (nonyl group is a propylene trimer isomer) with an average of 4-15 or 30- 90 moles of ethylene oxide; if a blend of prod- ucts is used, the average number of moles of ethylene oxide reacted to produce any prod- uct that is a component of the blend shall be in the range of 4-15 or 30-90 moles. a-(p-Nonylphenyl)-w-hydroxypoly(oxyethylene) ...... Surfactants, related adjuvants of surfactants sulfate, and its ammonium, calcium, magne- sium, potassium, sodium, and zinc salts; the nonyl group is a propylene trimer isomer and the poly(oxyethylene) content averages 4 moles. a-(p-Nonylphenyl)-w-hydroxypoly(oxyethylene) ...... Surfactants, related adjuvants of surfactants sulfate, and its ammonium, calcium, magne- sium, monoethanolamine, potassium, sodium, and zinc salts; the nonyl group is a propylene trimer isomer and the poly(oxyethylene) con- tent averages 4-14 or 30-90 moles of ethyiene oxide. Octadecyl 3,5-di-tert-butyl-4-hydroxyhydro Not more than 0.5% by Thermal stabilizer/antioxidant in animal tag and cinnamate (CAS Reg. No. 2082–79–3). weight of pesticide formu- similar slow-release devices lation. 1-Octanal (CAS Reg. No. 124–13–0) ...... Not more than 0.2% of the Odor masking agent pesticide formulation. Octyl and decyl glucosides mixture with a mix- ...... Thermal stabilizer/antioxidant in animal tag and ture of octyl and decyl oligosaccharides and similar slow-release devices related reaction products (primarily n-decanol) produced as an aqueous-based liquid (68- 72% solids) from the reaction of straight chain alcohols (C8(45%), C10) with anhydrous glu- cose. Octyl epoxytallate (CAS Reg. No. 61788–72–5) ...... Plasticizer, component animal tag Oleic acid, conforming to 21 CFR 172.862 (CAS ...... Defoaming agent Reg. No. 112–80–1). a-Oleoyl-w-hydroxypoly(oxyethylene), average ...... Emulsifier molecular weight (in amu) of 600. a-Oleoyl-w-(oleyloxy)poly(oxyethylene) derived ...... Emulsifier, defoaming agent from a-hydro-w-hydroxypoly(oxyethylene), mo- lecular weight (in amu) 600.

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Inert ingredients Limits Uses

Petroleum hydrocarbons, light, odorless, con- ...... Solvent, diluent forming to 21 CFR 172.884 or 178.3650. Petroleum hydrocarbons, synthetic isoparaffinic, ...... Do. conforming to 21 CFR 172.882 or 178.3530. Phenol ...... Solvent, cosolvent a-Pinene ...... Not more than 2% of formu- Stabilizer lation by weight. Polyethylene (CAS Reg. No. 9002–88–4) con- ...... Component of plastic slow release tag forming to 21 CFR 172.615. Polyethylene glycol [a-hydro-w- ...... Surfactants, related adjuvants of surfactants hydroxypoly(oxyethylene)]; mean molecular weight (in amu) 194 to 9,500 conforms to 21 CFR 178.3750. Polyglyceryl phthalate esters of coconut oil fatty ...... Do. acids. Poly(methylene-p-tert- ...... Do. butylphenoxy)poly(oxyethylene) ethanol; the poly(oxyethylene) content averages 4-12 moles. Poly(methylene-p- ...... Do. nonylphenoxy)poly(oxyethylene) ethanol; the poly(oxyethylene) content averages 4-12 moles. Poly(methylene-p- ...... Do. nonylphenoxy)poly(oxypropylene) propanol; the poly(oxypropylene) content averages 4-12 moles. Potassium hydroxide ...... Meeting Food Chemicals, Neutralizer Codex specifications. Propane ...... Propellant n-Propanol ...... Solvent, for blended emulsifiers 2-Propenoic acid, 2-methyl-, polymer with ethyl ...... Encapsulating agent,dispensers, resins, fibers 2-propenoate and methyl 2-methyl-2- and beads propenoate, ammonium salt (CAS Registra- tion No. 55989–05–4), minimum number aver- age molecular weight (in amu), 18,900. Propylene glycol ...... Solvent, cosolvent Propylene glycol monomethyl ether ...... Deactivator, emmolient Propyl gallate ...... Antioxidant Propyl p-hydroxybenzoate (Propyl paraben) ...... Meets specifications of Preservative Food Chemicals Codex; not to exceed 0.1% in formulations. Pyrophylite ...... Solid diluent, carrier Secondary alkyl (C11-C15) poly(oxyethylene) ac- ...... Surfactant etate, sodium salt; the ethylene oxide content averages 5 moles. Silica, hydrated silica ...... Anticaking agent, solid diluent, carrier Silica aerogel (finely powdered microcellular sili- ...... Component of antifoaming agent ca foam having a minimum silica content of 89.5%). Soapstone ...... Solid diluent Sodium diisobutylnaphthalenesulfonate ...... Surfactants, related adjuvants of surfactants Sodium dioctylsulfosuccinate ...... Do. Sodium hydroxide ...... Neutralizer Sodium isopropylisohexylnaphthalenesulfonate ...... Surfactants, related adjuvants of surfactants Sodium isopropylnaphthalenesulfonate ...... Do. Sodium monoalkyl and diakyl (C8-C13) ...... Do. phenoxybenzenedisulfonate mixtures con- taining not less than 70% of the monoalkylated product. Sodium mono- and ...... Do. dimethylnaphthalenesulfonate, molecular weight (in amu) 245-260. Sodium mono-, di-, and ...... Solvent, cosolvent stabilizer tributylnaphthalenesulfonates. Sodium N-oleoyl-N-methyl taurine ...... Not more than 1% of pes- Surfactant ticide formulations. Sodium starch glycolate (CAS Reg. No. 9063– Granular and tableted prod- Disintegrant 38–1). ucts only; not to exceed 8% of the formulated product. Sodium sulfate ...... Solid diluent, carrier

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Inert ingredients Limits Uses

Sorbitan fatty acid esters (fatty acids limited to ...... Buffering agent; corrosion inhibition C12, C14, C16, and C18 containing minor amounts of associated fatty acids) and poly(oxyethylene) derivatives of sorbitan fatty acid esters; the poly(oxyethylene) content averages 16-20 moles. Sorbitol ...... Antidusting agent. Stearic acid (CAS Reg. No. 57–11–4) ...... Lubricant, component animal tag a-Stearoyl-w-hydroxypoly(oxyethylene), average ...... Emulsifier molecular weight (in amu) of 600. a-Stearoyl-w-hydroxypoly(oxyethylene); the ...... Surfactants; related adjuvants of surfactants poly(oxyethylene) content averages 8, 9, or 40 moles; if a blend of products is used, the average number of moles of ethylene oxide reacted to produce any product that is a com- ponent of the blend shall be 8, 9, or 40. Sulfite liquors and cooking liquors, spent, ...... Surfactant, related adjuvants of surfactants oxidized (CAS Reg. No. 68514–09–0). Sulfur (CAS Reg. No. 7704–34–9) ...... Stabilizer Talc ...... Do. Tall oil; fatty acids not less than 58%, rosin ...... Surfactants, related adjuvants of surfactants acids not more than 44%, unsaponifiables not more than 8%. Tartrazine ...... Dye, coloring agent a-[p-(1,1,3,3-Tetramethylbutyl)phenyl]-w- ...... Surfactants, related adjuvants of surfactants hydroxypoly(oxyethylene) produced by the condensation of 1 mole of p (1,1,3,3- tetramethylbutyl)phenol with a range of 1-14 or 30-70 moles of ethylene oxide: if a blend of products is used, the average range number of moles of ethylene oxide reacted to produce any product that is a component of the blend shall be in the range of 1-14 or 30-70. 2,4,7,9-Tetramethyl-5-decyne-4.7-diol ...... Not more than 2.5% of pes- Surfactants, related adjuvants of surfactants ticide formulation. Titanium dioxide (CAS Reg. No. 13463–67–7) ...... Pigment/colorant in pesticide formulations for animal tag Toluenesulfonic acid and its ammonium, cal- ...... Do. cium, magnesium, potassium, sodium, and zinc salts. Triacetin (glyceryl triacetate) ...... Solvent, cosolvent Tridecylpoly(oxyethylene) acetate sodiums salt; ...... Surfactants, related adjuvants of surfactants where the ethylene oxide content averages 6- 7 moles. Trisodium phosphate ...... Precipitant, buffer, filler Xylene ...... Solvent, cosolvent Xylenesulfonic acid and its ammonium, calcium, ...... Surfactants, related adjuvants of surfactants magnesium, potassium, sodium, and zinc salts. Zinc oxide ...... Solid diluent, carrier Zinc stearate, conforming to 21 CFR 182.5994 ...... Water repellant, dessicant, and coating agent. and 582.5994. Zinc stearate (CAS Reg. No. 557–05–1) ...... Water repellant, desiccant, and coating agent; stabilizer, component of plastic animal tag Zinc sulfate (basic and monohydrate) ...... Water repellant, dessicant, and coating agent

[69 FR 23130, Apr. 28, 2004, as amended at 69 FR 29894, May 26, 2004; 69 FR 34949, June 23, 2004; 69 FR 58070, Sept. 29, 2004; 69 FR 58304, Sept. 30, 2004; 70 FR 37692, June 30, 2005; 70 FR 43312, July 27, 2005; 70 FR 44496, Aug. 3, 2005; 70 FR 51628, Aug. 31, 2005; 70 FR 54286, Sept. 14, 2005; 70 FR 55296, Sept. 21, 2005; 70 FR 67910, Nov. 9, 2005; 70 FR 55733, Sept. 23, 2005; 71 FR 14415, Mar. 22, 2006; 71 FR 30811, May 31, 2006; 71 FR 45422, Aug. 9, 2006]

EFFECTIVE DATE NOTE: At 71 FR 45422, Aug. 9, 2006, in § 180.930, the table was amended by removing the following entries, effective Aug. 9, 2008: a. a-Alkyl (C9-C18)-w-hydroxy poly(oxyethylene): the poly(oxyethylene) content averages 2- 20 moles. b. a-Alkyl (C12-C15)-w-hydroxypoly(oxyethylene/oxypropylene) hetero polymer in which the oxyethylene content is 8-13 moles and the oxypropylene content is 7-30 moles. c. a-Alkyl (C8-C10) hydroxypoly(oxypropylene) block polymer with polyoxyethylene; polyoxypropylene content averages 3 moles and polyoxyethylene content averages 5-12 moles.

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d. a-Alkyl (C6-C14)-w-hydroxypoly(oxypropylene) block copolymer with polyoxyethylene; polyoxypropylene content is 1-3 moles; polyoxyethylene content is 7-9 moles; average molec- ular weight (in amu) approximately 635. e. a-(p-Alkylphenyl)-w-hydroxypoly (oxyethylene) produced by the condensation of 1 mole of alkylphenol (alkyl is a mixture of propylene tetramer and pentamer isomers and averages C13) with 6 moles of ethylene oxide. f. Amine salts of alkyl (C8-C24) benzenesulfonic acid (butylamine; dimethylamino propyl- amine; mono- and diisopropyl- amine; and mono- , di-, and triethanolamine). g. a-(p-tert- Butylphenyl)-w-hydroxypoly(oxyethylene) mixture of dihydrogen phosphate and monohydrogen phosphate esters and the corresponding ammonium, calcium, magnesium, monoethanolamine, potassium, sodium, and zinc salts of the phosphate esters; the poly(oxyethylene) content averages 4-12 moles. h. a-(o,p-Dinonylphenyl)-w-hydroxypoly (oxyethylene) mixture of dihydrogen phosphate and monohydrogen phosphate esters and the corresponding ammonium, calcium, magnesium, monoethanolamine, potassium, sodium, and zinc salts of the phosphate esters; the nonyl group is a propylene trimer isomer and the poly(oxyethylene) content averages 4-14 moles. i. a-(o,p-Dinonylphenyl)-w-hydroxypoly (oxyethylene), produced by the condensation of 1 mole of dinonylphenol (nonyl group is a propylene trimer isomer) with an average of 4-14 moles of ethylene oxide. j. Dodecylbenzenesulfonic acid, amine salts. k. a-(p-Dodecylphenyl)-w-hydroxypoly (oxyethylene) produced by the condensation of 1 mole of dodecylphenol (dodecyl group is a propylene tetramer isomer) with an average of 4- 14 or 30-70 moles of ethylene oxide; if a blend of products is used, the average number of moles of ethylene oxide reacted to produce any product that is a component of the blend shall be in the range of 4-14 or 30-70 moles. l. Ethylene oxide adducts of 2,4,7,9-tetramethyl-5-decynediol, the ethylene oxide content averages 3.5, 10, or 30 moles. n. a-Lauryl-w-hydroxypoly(oxyethylene), average molecular weight (in amu) of 600. o. a-Lauryl-w-hydroxypoly(oxyethylene), sulfate, sodium salt; the poly(oxyethylene) con- tent is 3-4 moles. p. Manganous oxide. r. Mono-, di-, and trimethylnaphthalenesulfonic acids-formaldehyde condensates, sodium salts. s. Naphthalenesulfonic acid and its sodium salt. t. a-(p-Nonylphenyl)-w-hydroxypoly(oxyethylene) mixture of dihydrogen phosphate and monohydrogen phosphate esters and the corresponding ammonium, calcium, magnesium, monoethanolamine, potassium, sodium, and zinc salts of the phosphate esters; the nonyl group is a propylene trimer isomer and the poly(oxyethylene) content averages 4-14 moles. u. a-(p-Nonylphenyl)-w-hydroxypoly(oxyethylene) sulfate, and its ammonium, calcium, magnesium, potassium, sodium, and zinc salts; the nonyl group is a propylene trimer isomer and the poly(oxyethylene) content averages 4 moles. v. a-(p-Nonylphenyl)-w-hydroxypoly(oxyethylene) sulfate, and its ammonium, calcium, magnesium, monoethanolamine, potassium, sodium, and zinc salts; the nonyl group is a pro- pylene trimer isomer and the poly(oxyethylene) content averages 4-14 or 30-90 moles of ethyiene oxide. w. Polyglyceryl phthalate esters of coconut oil fatty acids. x. Poly(methylene-p-tert-butylphenoxy)poly(oxyethylene) ethanol; the poly(oxyethylene) content averages 4-12 moles. y. Poly(methylene-p-nonylphenoxy)poly(oxyethylene) ethanol; the poly(oxyethylene) con- tent averages 4-12 moles. z. Poly(methylene-p-nonylphenoxy)poly(oxypropylene) propanol; the poly(oxypropylene) content averages 4-12 moles. aa. Secondary alkyl (C11-C15) poly(oxyethylene) acetate, sodium salt; the ethylene oxide content averages 5 moles. cc. Sodium diisobutylnaphthalenesulfonate. dd. Sodium isopropylisohexylnaphthalenesulfonate. ee. Sodium isopropylnaphthalenesulfonate. ff. Sodium monoalkyl and diakyl (C8-C13) phenoxybenzenedisulfonate mixtures containing not less than 70% of the monoalkylated product. gg. Sodium mono- and dimethylnaphthalenesulfonate, molecular weight (in amu) 245-260. hh. Sodium mono-, di-, and tributylnaphthalenesulfonates. ii. Sodium N-oleoyl-N-methyl taurine. jj. a-[p-(1,1,3,3-Tetramethylbutyl)phenyl]-w-hydroxypoly(oxyethylene) produced by the con- densation of 1 mole of p (1,1,3,3-tetramethylbutyl)phenol with a range of 1-14 or 30-70 moles of ethylene oxide: if a blend of products is used, the average range number of moles of ethyl- ene oxide reacted to produce any product that is a component of the blend shall be in the range of 1-14 or 30-70.

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ll. Tridecylpoly(oxyethylene) acetate sodiums salt; where the ethylene oxide content aver- ages 6-7 moles.

§ 180.940 Tolerance exemptions for ac- semi-permanent or permanent food- tive and inert ingredients for use in contact surface (other than being ap- antimicrobial formulations (Food- plied on food packaging) with adequate contact surface sanitizing solu- draining before contact with food. tions). (a) The following chemical sub- Residues of the following chemical stances when used as ingredients in an substances are exempted from the re- antimicrobial pesticide formulation quirement of a tolerance when used in may be applied to: Food-contact sur- accordance with good manufacturing faces in public eating places, dairy- practice as ingredients in an anti- processing equipment, and food-proc- microbial pesticide formulation, pro- vided that the substance is applied on a essing equipment and utensils.

Pesticide Chemical CAS Reg. No. Limits

Acetic acid 64–19–7 When ready for use, the end-use concentration is not to exceed 290 ppm

a-Alkyl(C10-C14)-w-hydroxypoly (oxyethylene) None None poly(oxypropylene) average molecular weight (in amu), 768 to 837

a-Alkyl(C12-C18)-w-hydroxypoly (oxyethylene) None None poly(oxypropylene) average molecular weight (in amu), 950 to 1120 Ammonium chloride 12125–02–9 When ready for use, the end-use concentration is not to exceed 48 ppm Ethanol 64–17–5 None Ethylenediaminetetraacetic acid (EDTA), 64–02–8 None tetrasodium salt Hydrogen peroxide 7722–84–1 When ready for use, the end-use concentration is not to exceed 91 ppm Hypochlorous acid, sodium salt 7681–52–9 When ready for use, the end-use concentration of all hypochlorous acid chemicals in the so- lution is not to exceed 200 ppm determined as total available chlorine Iodine 7553–56–2 When ready for use, the total end-use con- centration of all iodide-producing chemicals in the solution is not to exceed 25 ppm of ti- tratable iodine Magnesium oxide 1309–48–4 None Methylene blue 61–73–4 When ready for use, the end-use concentration is not to exceed 0.4 ppm a-(p-Nonylphenyl)-w-hydroxypoly (oxyethylene) None None average poly(oxyethylene) content 11 moles) Octadecanoic acid, calcium salt 1592–23–0 None 1-Octanesulfonic acid, sodium salt 5324–84–5 When ready for use, the end-use concentration is not to exceed 46 ppm Octanoic acid 124–07–2 When ready for use, the end-use concentration is not to exceed 52 ppm Oxirane, methyl-, polymer with oxirane, min- 9003–11–6 None imum molecular weight (in amu), 1900 Peroxyacetic acid 79–21–0 When ready for use, the end-use concentration is not to exceed 58 ppm Peroxyoctanoic acid 33734–57–5 When ready for use, the end-use concentration is not to exceed 52 ppm Phosphonic acid, (1-hydroxyethylidene)bis- 2809–21–4 When ready for use, the end-use concentration is not to exceed 14 ppm Phosphoric acid, trisodium salt 7601–54–9 When ready for use, the end-use concentration is not to exceed 5916 ppm Potassium bromide 7758–02–3 When ready for use, the end-use concentration is not to exceed 46 ppm total available halo- gen Potassium iodide 7681–11–0 When ready for use, the total end-use con- centration of all iodide-producing chemicals in the solution is not to exceed 25 ppm of ti- tratable iodine

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Pesticide Chemical CAS Reg. No. Limits

Quaternary ammonium compounds, alkyl (C12- 8001–54–5 When ready for use, the end-use concentration C18) benzyldimethyl, chlorides of all quaternary chemicals in the solution is not to exceed 200 ppm of active quaternary compound Quaternary ammonium compounds, n-alkyl (C12- None When ready for use, the end-use concentration C14) dimethyl ethylbenzyl ammonium chloride, of all quaternary chemicals in the solution is average molecular weight (in amu), 377 to not to exceed 200 ppm of active quaternary 384 compound Quaternary ammonium compounds n-alkyl (C12- None When ready for use, the end-use concentration C18) dimethyl ethylbenzyl ammonium chloride of all quaternary chemicals in the solution is average molecular weight (in amu) 384 not to exceed 200 ppm of active quaternary compound Quaternary ammonium compounds di-n-alkyl None When ready for use, the end-use concentration (C8-C10) dimethyl ammonium chloride, aver- of this specific quaternary compound is not age molecular weight (in amu), 332 to 361 to exceed 150 ppm of active quaternary compound; the end-use concentration of all quaternary chemicals in the solution is not to exceed 200 ppm of active quaternary com- pound Sulfuric acid monododecyl ester, sodium salt 151–21–3 When ready for use, the end-use concentration (sodium lauryl sulfate) is not to exceed 3 ppm 1,3,5-Triazine-2,4,6(1H,3H,5H)-trione, 1,3- 2893–78–9 When ready for use, the end-use concentration dichloro-, sodium salt of all di- or trichloroisocyanuric acid chemi- cals in the solution is not to exceed 100 ppm determined as total available chlorine

(b) The following chemical sub- may be applied to: Dairy processing stances when used as ingredients in an equipment, and food-processing equip- antimicrobial pesticide formulation ment and utensils.

Pesticide Chemical CAS Reg. No. Limits

Acetic acid 64–19–7 When ready for use, the end-use concentration is not to exceed 686 ppm Acetic acid, chloro-, sodium salt, reaction prod- 68608–66–2 When ready for use, the end-use concentration ucts with 4,5-dihydro-2-undecyl-1H-imidazole- is not to exceed 42 ppm chloroacetic acid 1-ethanol and sodium hydroxide Benzenesulfonic acid, dodecyl- 27176–87–0 When ready for use, the end-use concentration is not to exceed 5.5 ppm Butanedioic acid, octenyl- 28805–58–5 When ready for use, the end-use concentration is not to exceed 156 ppm Butoxy monoether of mixed (ethylene-propylene) None None polyalkylene glycol, minimum average molec- ular weight (in amu), 2400 Calcium chloride 10043–52–4 When ready for use, the end-use concentration is not to exceed 17 ppm

n-Carboxylic acids (C6-C12), consisting of a mix- None When ready for use, the end-use concentration ture of not less than 56% octanoic acid and is not to exceed 39 ppm not less than 40% decanoic acid Decanoic acid 334–48–5 When ready for use, the end-use concentration is not to exceed 90 ppm Ethanesulfonic acid, 2-[cyclohexyl (1- 132–43–4 When ready for use, the end-use concentration oxohexadecyl) amino]-, sodium salt is not to exceed 237 ppm Ethylenediaminetetraacetic acid (EDTA), diso- 139–33–3 When ready for use, the end-use concentration dium salt is not to exceed 1400 ppm FD&C Yellow No. 5 (Tartrazine) (conforming to 1934–21–0 None 21 CFR 74.705) D-Gluconic acid, monosodium salt 527–07–1 When ready for use, the end-use concentration is not to exceed 760 ppm Hydriodic acid 10034–85–2 When ready for use, the total end-use con- centration of all iodide-producing chemicals is not to exceed 25 ppm of titratable iodine Hydrogen peroxide 7722–84–1 When ready for use, the end-use concentration is not to exceed 465 ppm Hypochlorous acid 7790–92–3 When ready for use, the end-use concentration of all hypochlorous acid chemicals in the so- lution is not to exceed 200 ppm determined as total available chlorine

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Pesticide Chemical CAS Reg. No. Limits

Iodine 7553–56–2 When ready for use, the total end-use con- centration of all iodide-producing chemicals in the solution is not to exceed 25 ppm of ti- tratable iodine Lactic acid 50–21–5 When ready for use, the end-use concentration is not to exceed 138 ppm a-Lauroyl-w-hydroxypoly (oxyethylene) with an None None average of 8-9 moles ethylene oxide, average molecular weight (in amu), 400 Nonanoic acid 112–05–0 When ready for use, the end-use concentration is not to exceed 90 ppm 1-Octanamine, N,N-dimethyl- 7378–99–6 When ready for use, the end-use concentration is not to exceed 113 ppm 1,2-Octanedisulfonic acid 113669–58–2 When ready for use, the end-use concentration is not to exceed 102 ppm 1-Octanesulfonic acid 3944–72–7 When ready for use, the end-use concentration is not to exceed 172 ppm 1-Octanesulfonic acid, sodium salt 5324–84–5 When ready for use, the end-use concentration is not to exceed 297 ppm 1-Octanesulfonic acid, 2-sulfino- 113652–56–5 When ready for use, the end-use concentration is not to exceed 102 ppm Octanoic acid 124–07–2 When ready for use, the end-use concentration is not to exceed 176 ppm Oxirane, methyl-, polymer with oxirane, ether 11111–34–5 When ready for use, the end-use concentration with (1,2-ethanediyldinitrilo)tetrakis [propanol] is not to exceed 20 ppm (4:1) Oxychloro species (including chlorine dioxide) None When ready for use, the end-use concentration generated by acidification of an aqueous solu- is not to exceed 200 ppm of chlorine dioxide tion of sodium chlorite as determined by the method titled, Iodometric Method for the Determination of Available Chlorine Dioxide (50-250 ppm available chlorine dioxide) Peroxyacetic acid 79–21–0 When ready for use, the end-use concentration is not to exceed 315 ppm Peroxyoctanoic acid 33734–57–5 When ready for use, the end-use concentration is not to exceed 122 ppm Phosphonic acid, (1-hydroxyethylidene)bis- 2809–21–4 When ready for use, the end-use concentration is not to exceed 34 ppm Phosphoric acid 7664–38–2 None Phosphoric acid, monosodium salt 7558–80–7 When ready for use, the end-use concentration is not to exceed 350 ppm Potassium iodide 7681–11–0 When ready for use, the total end-use con- centration of all iodide-producing chemicals in the solution is not to exceed 25 ppm of ti- tratable iodine Propanoic acid 79–09–4 When ready for use, the end-use concentration is not to exceed 297 ppm 2,6-Pyridinedicarboxylic acid 499–83–2 When ready for use, the end-use concentration is not to exceed 1.2 ppm Sulfuric acid 7664–93–9 When ready for use, the end-use concentration is not to exceed 288 ppm Sulfuric acid monododecyl ester, sodium salt 151–21–3 When ready for use, the end-use concentration (sodium lauryl sulfate) is not to exceed 350 ppm

(c) The following chemical sub- may be applied to: Food-processing stances when used as ingredients in an equipment and utensils. antimicrobial pesticide formulation

Pesticide Chemical CAS Reg. No. Limits

Acetic acid 64–19–7 When ready for use, the end-use concentration is not to exceed 686 ppm Acetic acid, chloro-, sodium salt, reaction prod- 68608–66–2 When ready for use, the end-use concentration ucts with 4,5-dihydro-2-undecyl-1H-imidazole- is not to exceed 42 ppm chloroacetic acid 1-ethanol and sodium hydroxide

a-Alkyl(C10-C14)-w-hydroxypoly (oxyethylene) None None poly (oxypropylene) average molecular weight (in amu), 768 to 837

a-Alkyl(C11-C15)-w-hydroxypoly (oxyethylene) None None with ethylene oxide content 9 to 13 moles

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Pesticide Chemical CAS Reg. No. Limits

a-Alkyl(C12-C15)-w-hydroxypoly (oxyethylene) None None polyoxypropylene, average molecular weight (in amu), 965

a-Alkyl(C12-C18)-w-hydroxypoly (oxyethylene) None None poly(oxypropylene) average molecular weight (in amu), 950 to 1120 Ammonium chloride 12125–02–9 When ready for use, the end-use concentration is not to exceed 48 ppm Benzenesulfonic acid, dodecyl- 27176–87–0 When ready for use, the end-use concentration is not to exceed 400 ppm Benzenesulfonic acid, dodecyl-, sodium salt 25155–30–0 When ready for use, the end-use concentration is not to exceed 430 ppm [1,1′-Biphenyl]-2-ol 90–43–7 When ready for use, the end-use concentration is not to exceed 400 ppm Boric acid, sodium salt 7775–19–1 None Butanedioic acid, octenyl- 28805–58–5 When ready for use, the end-use concentration is not to exceed 156 ppm Butanedioic acid, sulfo-, 1,4-dioctyl ester, so- 1639–66–3 None dium salt Butoxy monoether of mixed (ethylene-propylene) None None polyalkylene glycol, cloudpoint of 90 - 100oC in 0.5 aqueous solution, average molecular weight (in amu), 3300 Butoxy monoether of mixed (ethylene-propylene) None None polyalkylene glycol, minimum average molec- ular weight (in amu), 2400 Calcium chloride 10043–52–4 When ready for use, the end-use concentration is not to exceed 17 ppm

n-Carboxylic acids (C6-C12), consisting of a mix- None When ready for use, the end-use concentration ture of not less than 56% octanoic acid and is not to exceed 39 ppm not less than 40% decanoic acid 3-Cyclohexene-1-methanol,a,a,4-trimethyl- 98–55–5 None 1-Decanaminium, N-decyl-N, N-dimethyl-, chlo- 7173–51–5 When ready for use, the end-use concentration ride is not to exceed 200 ppm of active quater- nary compound Decanoic acid 3347–48–5 When ready for use, the end-use concentration is not to exceed 234 ppm Ethanesulfonic acid, 2-[cyclohexyl (1- 132–43–4 When ready for use, the end-use concentration oxohexadecyl) amino]-, sodium salt is not to exceed 237 ppm Ethanol 64–17–5 None Ethanol, 2 butoxy- 111–76–2 None Ethanol, 2-(2-ethoxyethoxy)- 111–90–0 None Ethylenediaminetetraacetic acid (EDTA), diso- 139–33–3 When ready for use, the end-use concentration dium salt is not to exceed 1400 ppm Ethylenediaminetetraacetic acid (EDTA), 64–02–8 None tetrasodium salt Fatty acids, coco, potassium salts 61789–30–8 None Fatty acids, tall-oil, sulfonated, sodium salts 68309–27–3 When ready for use, the end-use concentration is not to exceed 66 ppm FD&C Yellow No. 5 (Tartrazine) (conforming to 1934–21–0 None 21 CFR 74.705) D-Gluconic acid, monosodium salt 527–07–1 When ready for use, the end-use concentration is not to exceed 760 ppm Hydriodic acid 10034–85–2 When ready for use, the total end-use con- centration of all iodide-producing chemicals in the solution is not to exceed 25 ppm of ti- tratable iodine Hydrogen peroxide 7722–84–1 When ready for use, the end-use concentration is not to exceed 1100 ppm Hypochlorous acid 7790–92–3 When ready for use, the end-use concentration of all hypochlorous acid chemicals in the so- lution is not to exceed 200 ppm determined as total available chlorine Hypochlorous acid, calcium salt 7778–54–3 When ready for use, the end-use concentration of all hypochlorous acid chemicals in the so- lution is not to exceed 200 ppm determined as total available chlorine Hypochlorous acid, lithium salt 13840–33–0 When ready for use, the end-use concentration of all hypochlorous acid chemicals in the so- lution is not to exceed 200 ppm determined as total available chlorine and 30 ppm lithium

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Pesticide Chemical CAS Reg. No. Limits

Hypochlorous acid, potassium salt 7778–66–7 When ready for use, the end-use concentration of all hypochlorous acid chemicals in the so- lution is not to exceed 200 ppm determined as total available chlorine Hypochlorous acid, sodium salt 7681–52–9 When ready for use, the end-use concentration of all hypochlorous acid chemicals in the so- lution is not to exceed 200 ppm determined as total available chlorine Iodine 7553–56–2 When ready for use, the total end-use con- centration of all iodide-producing chemicals in the solution is not to exceed 25 ppm of ti- tratable iodine Lactic acid 50–21–5 None a-Lauroyl-w-hydroxypoly (oxyethylene) with an None None average of 8-9 moles ethylene oxide, average molecular weight (in amu), 400 Magnesium oxide 1309–48–4 None Methylene blue 61–73–4 When ready for use, the end-use concentration is not to exceed 0.4 ppm Naphthalene sulfonic acid, sodium salt 1321–69–3 When ready for use, the end-use concentration of all naphthalene sulfonate chemicals in the solution is not to exceed 332 ppm naph- thalene sulfonates Naphthalene sulfonic acid sodium salt, and its None When ready for use, the end-use concentration methyl, dimethyl and trimethyl derivatives of all naphthalene sulfonate chemicals in the solution is not to exceed 332 ppm naph- thalene sulfonates Naphthalene sulfonic acid sodium salt, and its None When ready for use, the end-use concentration methyl, dimethyl and trimethyl derivatives of naphthalene sulfonate chemicals in the alkylated at 3% by weight with C6-C9 linear solution is not to exceed 332 ppm naph- olefins thalene sulfonates Neodecanoic acid 26896–20–8 When ready for use, the end-use concentration is not to exceed 174 ppm Nonanoic acid 112–05–0 When ready for use, the end-use concentration is not to exceed 90 ppm a-(p-Nonylphenyl)-w-hydroxypoly (oxyethylene) None None maximum average molecular weight (in amu), 748 a-(p-Nonylphenol)-w-hydroxypoly (oxyethylene) None None average poly(oxyethylene) content 11 moles a-(p-Nonylphenyl)-w-hydroxypoly (oxyethylene) None None produced by the condensation of 1 mole p- nonylphenol with 9 to 12 moles ethylene oxide a-(p-Nonylphenyl)-w-hydroxypoly (oxyethylene), None None 9 to 13 moles ethylene oxide Octadecanoic acid, calcium salt 1592–23–0 None 9-Octadecenoic acid (9Z)-, sulfonated 68988–76–1 When ready for use, the end-use concentration is not to exceed 312 ppm 9-Octadecenoic acid (9Z)-sulfonated, sodium 68443–05–0 When ready for use, the end-use concentration salts is not to exceed 200 ppm 1-Octanamine, N,N-dimethyl- 7378–99–6 When ready for use, the end-use concentration is not to exceed 113 ppm 1,2-Octanedisulfonic acid 113669–58–2 When ready for use, the end-use concentration is not to exceed 102 ppm 1-Octanesulfonic acid 3944–72–7 When ready for use, the end-use concentration is not to exceed 172 ppm 1-Octanesulfonic acid, sodium salt 5324–84–5 When ready for use, the end-use concentration is not to exceed 312 ppm 1-Octanesulfonic acid, 2-sulfino- 113652–56–5 When ready for use, the end-use concentration is not to exceed 102 ppm Octanoic acid 124–07–2 When ready for use, the end-use concentration is not to exceed 234 ppm Oxirane, methyl-, polymer with oxirane, min- 9003–11–6 None imum molecular weight (in amu), 1900 Oxirane, methyl-, polymer with oxirane, block, 106392–12–5 None average molecular weight (in amu), 1900 Oxirane, methyl-, polymer with oxirane, block, None None minimum average molecular weight (in amu), 2000 Oxirane, methyl-, polymer with oxirane, block, None None 27 to 31 moles of polyoxypropylene, average molecular weight (in amu) 2000

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Pesticide Chemical CAS Reg. No. Limits

Oxirane, methyl-, polymer with oxirane, ether 11111–34–5 When ready for use, the end-use concentration with (1,2-ethanediyldinitrilo)tetrakis [propanol] is not to exceed 20 ppm (4:1) Oxychloro species (predominantly chlorite, chlo- None When ready for use, the end-use concentration rate and chlorine dioxide in an equilibrium is not to exceed 200 ppm of chlorine dioxide mixture) generated either (i) by directly meter- as determined by the method titled, ing a concentrated chlorine dioxide solution ‘‘Iodometric Method for the Determination of prepared just prior to use, into potable water, Available Chlorine Dioxide (50-250 ppm or (ii) by acidification of an aqueous alkaline available chlorine dioxide)’’ solution of oxychloro species (predominately chlorite and chlorate) followed by dilution with potable water Oxychloro species (including chlorine dioxide) None When ready for use, the end-use concentration generated by acidification of an aqueous solu- is not to exceed 200 ppm of chlorine dioxide tion of sodium chlorite as determined by the method titled, ‘‘Iodometric Method for the Determination of Available Chlorine Dioxide (50-250 ppm available chlorine dioxide)’’ 2,4-Pentanediol, 2-methyl- 107–41–5 None Peroxyacetic acid 79–21–0 When ready for use, the end-use concentration is not to exceed 315 ppm Peroxyoctanoic acid 33734–57–5 When ready for use, the end-use concentration is not to exceed 122 ppm Phenol, 4-chloro-2-(phenylmethyl)- 120–32–1 When ready for use, the end-use concentration is not to exceed 320 ppm Phenol, 4-(1,1-dimethylpropyl)- 80–46–6 When ready for use, the end-use concentration is not to exceed 80 ppm Phosphonic acid, (1-hydroxyethylidene)bis- 2809–21–4 When ready for use, the end-use concentration is not to exceed 34 ppm Phosphoric acid 7664–38–2 None Phosphoric acid, monosodium salt 7558–80–7 When ready for use, the end-use concentration is not to exceed 350 ppm Phosphoric acid, trisodium salt 7601–54–9 When ready for use, the end-use concentration is not to exceed 5916 ppm Poly(oxy-1,2-ethanediyl), a-[(1,1,3,3- None None tetramethylbutyl) phenyl]-w-hydroxy-, pro- duced with one mole of the phenol and 4 to 14 moles ethylene oxide Potassium bromide 7758–02–3 When ready for use, the end-use concentration of all bromide-producing chemicals in the so- lution is not to exceed 200 ppm total avail- able halogen Potassium iodide 7681–11–0 When ready for use, the total end-use con- centration of all iodide-producing chemicals in the solution is not to exceed 25 ppm of ti- tratable iodine Propanoic acid 79–09–4 When ready for use, the end-use concentration is not to exceed 297 ppm 2,6-Pyridinedicarboxylic acid 499–83–2 When ready for use, the end-use concentration is not to exceed 1.2 ppm Quaternary ammonium compounds, alkyl (C12- 8001–54–5 When ready for use, the end-use concentration C18) benzyldimethyl, chlorides of this specific quaternary compound is not to exceed 200 ppm within the end-use total concentration that is not to exceed 400 ppm active quaternary compound Quaternary ammonium compounds, n-alkyl (C12- None When ready for use, the end-use concentration C14) dimethyl ethylbenzyl ammonium chloride, of this specific quaternary compound is not average molecular weight (in amu), 377 to to exceed 200 ppm within the end-use total 384 concentration that is not to exceed 400 ppm active quaternary compound Quaternary ammonium compounds, n-alkyl (C12- None When ready for use, the end-use concentration C18) dimethyl ethylbenzyl ammonium chloride of this specific quaternary compound is not average molecular weight (in amu) 384 to exceed 200 ppm within the end-use total concentration that is not to exceed 400 ppm active quaternary compound Quaternary ammonium compounds, di-n-Alkyl None When ready for use, the end-use concentration (C8-C10) dimethyl ammonium chloride, aver- of this specific quaternary compound is not age molecular weight (in amu), 332 to 361 to exceed 240 ppm within the end-use total concentration that is not to exceed 400 ppm active quaternary compound Sodium-a-alkyl(C12-C15)-w-hydroxypoly (oxy- None None ethylene) sulfate with the poly(oxyethylene) content averaging one mole

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Pesticide Chemical CAS Reg. No. Limits

Sodium bromide 7647–15–6 When ready for use, the end-use concentration of all bromide-producing chemicals in the so- lution is not to exceed 200 ppm total avail- able halogen Sodium iodide 7681–82–5 When ready for use, the total end-use con- centration of all iodide-producing chemicals in the solution is not to exceed 25 ppm of ti- tratable iodine Sulfuric acid 7664–93–9 When ready for use, the end-use concentration is not to exceed 228 ppm Sulfuric acid monododecyl ester, sodium salt 151–21–3 None (sodium lauryl sulfate) 1,3,5-Triazine-2,4,6(1H,3H,5H)-trione, 1,3- 2782–57–2 When ready for use, the end-use concentration dichloro- of all di- or trichloroisocyanuric acid chemi- cals in the solution is not to exceed 100 ppm determined as total available chlorine 1,3,5-Triazine-2,4,6(1H,3H,5H)-trione, 1,3- 2244–21–5 When ready for use, the end-use concentration dichloro-, potassium salt of all di- or trichloroisocyanuric acid chemi- cals in the solution is not to exceed 100 ppm determined as total available chlorine 1,3,5-Triazine-2,4,6(1H,3H,5H)-trione, 1,3- 2893–78–9 When ready for use, the end-use concentration dichloro-, sodium salt of all di- or trichloroisocyanuric acid chemi- cals in the solution is not to exceed 100 ppm determined as total available chlorine 1,3,5-Triazine-2,4,6(1H,3H,5H)-trione, 1,3,5- 87–90–1 When ready for use, the end-use concentration trichloro- of all di- or trichloroisocyanuric acid chemi- cals in the solution is not to exceed 100 ppm determined as total available chlorine 1,3,5-Triazine, N,N′,N″-trichloro-2,4,6-triamino- 7673–09–8 When ready for use, the end-use concentration of all di- or trichloroisocyanuric acid chemi- cals in the solution is not to exceed 200 ppm determined as total available chlorine Xylenesulfonic acid, sodium salt 1300–72–7 When ready for use, the end-use concentration is not to exceed 62 ppm

[69 FR 23136, Apr. 28, 2004, as amended at 71 FR 30811, May 31, 2006; 71 FR 46125, Aug. 11, 2006]

EFFECTIVE DATE NOTE: At 71 FR 45423, Aug. 9, 2006, § 180.940 was amended as follows, effec- tive Aug. 9, 2008: 1. The table in paragraph (a) is amended by removing the following entries:

i. a-Alkyl(C10-C14)-w- hydroxypoly (oxyethylene) poly(oxypropylene) average molecular weight (in amu), 768 to 837.

ii. a-Alkyl(C12-C18)-w hydroxypoly (oxyethylene) poly(oxypropylene) average molecular weight (in amu), 950 to 1120. 2. The table in paragraph (b) is amended by removing the following entries: i. a-Lauroyl-w-hydroxypoly (oxyethylene) with an average of 8-9 moles ethylene oxide, aver- age molecular weight (in amu), 400. ii. Oxirane, methyl-, polymer with oxirane, ether with (1,2-ethanediyldinitrilo)tetrakis [propanol] (4:1). 3. The table in paragraph (c) is amended by removing the following entries:

i. a-Alkyl(C10-C14)-w-hydroxypoly (oxyethylene) poly (oxypropylene) average molecular weight (in amu), 768 to 837.

ii. a-Alkyl(C11-C15)-w-hydroxypoly (oxyethylene) with ethylene oxide content 9 to 13 moles. iii. a-Alkyl(C12-C15)-w-hydroxypoly (oxyethylene) polyoxypropylene, average molecular weight (in amu), 965.

iv. a-Alkyl(C12-C18)-w-hydroxypoly (oxyethylene) poly(oxypropylene) average molecular weight (in amu), 950 to 1120. v. a-Lauroyl-w-hydroxypoly (oxyethylene) with an average of 8-9 moles ethylene oxide, av- erage molecular weight (in amu), 400. vi. Naphthalene sulfonic acid, sodium salt. vii. Naphthalene sulfonic acid sodium salt, and its methyl, dimethyl and trimethyl deriva- tives. viii. Naphthalene sulfonic acid sodium salt, and its methyl, dimethyl and trimethyl deriva- tives alkylated at 3% by weight with C6-C9 linear olefins. ix. Oxirane, methyl-, polymer with oxirane, ether with (1,2-ethanediyldinitrilo)tetrakis [propanol] (4:1).

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§ 180.950 Tolerance exemptions for (a)(2)(ii) of this section, and cocoa minimal risk active and inert ingre- bean. dients. (2) Bird feed such as canary seed. Unless specifically excluded, residues (3) Any feed component of a medi- resulting from the use of the following cated feed meeting the definition of an substances as either an inert or an ac- animal feed item. tive ingredient in a pesticide chemical (c) Edible fats and oils. Edible fats and formulation, including antimicrobial oils means all edible (food or feed) fats pesticide chemicals, are exempted from and oils, derived from either plants or the requirement of a tolerance under animals, whether or not commonly FFDCA section 408, if such use is in ac- consumed, including products derived cordance with good agricultural or from hydrogenating (food or feed) oils, manufacturing practices. or liquefying (food or feed) fats. (a) Commonly consumed food commod- (1) Included within the term edible ities. Commonly consumed food com- fats and oils are oils (such as soybean modities means foods that are com- oil) that are derived from the commod- monly consumed for their nutrient ities specified in paragraph (a)(2)(ii) of properties. The term commonly con- this section when such oils are highly sumed food commodities shall only refined via a solvent extraction proce- apply to food commodities (whether a dure. raw agricultural commodity or a proc- (2) Excluded from the term edible essed commodity) in the form the com- fats and oils are plant oils used in the modity is sold or distributed to the pesticide chemical formulation specifi- public for consumption. cally to impart their characteristic (1) Included within the term com- fragrance and/or flavoring. monly consumed food commodities are: (d) [Reserved] (i) Sugars such as sucrose, lactose, (e) Specific chemical substances. Resi- dextrose and fructose, and invert sugar dues resulting from the use of the fol- and syrup. lowing substances as either an inert or (ii) Spices such as cinnamon, cloves, an active ingredient in a pesticide and red pepper. chemical formulation, including anti- (iii) Herbs such as basil, anise, or microbial pesticide chemicals, are ex- fenugreek. empted from the requirement of a tol- (2) Excluded from the term com- erance under FFDCA section 408, if monly consumed food commodities are: such use is in accordance with good ag- (i) Any food commodity that is adul- ricultural or manufacturing practices. terated under 21 U.S.C. 342. Chemical CAS No. (ii) Both the raw and processed forms of peanuts, tree nuts, milk, soybeans, Acetic acid, sodium salt ...... 127–09–3 eggs, fish, crustacea, and wheat. Alpha-cyclodextrin ...... 10016–20–3 Animal glue ...... None (iii) Alcoholic beverages. Ascorbic acid (vitamin C) ...... 50–81–7 (iv) Dietary supplements. Beeswax ...... 8012–89–3 (b) Animal feed items. Animal feed Benzoic acid, sodium salt ...... 532–32–1 Beta-cyclodextrin ...... 7585–39–9 items means meat meal and all items Carbonic acid, monopotassium salt ...... 298–14–6 derived from field crops that are fed to Carbonic acid, monosodium salt (sodium bicar- livestock excluding both the raw and bonate) ...... 144–55–8 processed forms of peanuts, tree nuts, Carnauba wax ...... 8015–86–9 Carob gum (locust bean gum) ...... 9000–40–2 milk, soybeans, eggs, fish, crustacea, Castor oil ...... 8001–79–4 and wheat. Meat meal is an animal feed Castor oil, hydrogenated ...... 8001–78–3 composed of dried animal fat and pro- Cellulose ...... 9004–34–6 Cellulose acetate ...... 9004–35–7 tein that has been sterilized. Other Cellulose, carboxy methyl ether, sodium salt ... 9004–32–4 than meat meal, the term animal feed Cellulose, 2-hydroxyethyl ether ...... 9004–62–0 item does not extend to any item de- Cellulose, 2-hydroxypropyl ether ...... 9004–64–2 Cellulose, 2-hydroxypropyl methyl ether ...... 9004–65–3 signed to be fed to animals that con- Cellulose, methyl ether ...... 9004–67–5 tains, to any extent, components of Cellulose, mixture with cellulose carboxymethyl animals. Included within the term ani- ether, sodium salt ...... 51395–75–6 mal feed items are: Cellulose, pulp ...... 65996–61–4 Cellulose, regenerated ...... 68442–85–3 (1) The hulls and shells of the com- Citric acid ...... 77–92–9 modities specified in paragraph Citric acid, 2-(acetyloxy)-, tributyl ester ...... 77–90–7

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Chemical CAS No. [67 FR 36537, May 24, 2002, as amended at 67 FR 56229, Sept. 3, 2002; 67 FR 78718, Dec. 26, Citric acid, calcium salt ...... 7693–13–2 2002; 68 FR 16437, Apr. 4, 2003; 68 FR 18552, Citric acid, calcium salt (2:3) ...... 813–94–5 Citric acid, dipotassium salt ...... 3609–96–9 Apr. 16, 2003; 68 FR 52700, Sept. 5, 2003; 69 FR Citric acid, disodium salt ...... 144–33–2 4077, Jan. 28, 2004; 69 FR 9963, Mar. 3, 2004; 69 Citric acid, monohydrate ...... 5949–29–1 FR 29894, May 26, 2004; 69 FR 33578, June 16, Citric acid, monopotassium salt ...... 866–83–1 2004; 69 FR 58070, Sept. 29, 2004; 70 FR 7876, Citric acid, monosodium salt ...... 18996–35–5 Citric acid, potassium salt ...... 7778–49–6 Feb. 16, 2005; 70 FR 28447, May 18, 2005; 70 FR Citric acid, triethyl ester ...... 77–93–0 38785, July 6, 2005; 71 FR 30811, May 31, 2006] Citric acid, tripotassium salt ...... 866–84–2 Citric acid, tripotassium salt, monohydrate ...... 6100–05–6 Citric acid, sodium salt ...... 994–36–5 § 180.960 Polymers; exemptions from Citric acid, trisodium salt ...... 68–04–2 the requirement of a tolerance. Citric acid, trisodium salt, dihydrate ...... 6132–04–3 Citric acid, trisodium salt, pentahydrate ...... 6858–44–2 Residues resulting from the use of Coffee grounds ...... 68916–18–7 the following substances, that meet the Dextrins ...... 9004–53–9 definition of a polymer and the criteria 1,3-Dioxolan-2-one, 4-methyl-(propylene car- bonate) ...... 108–32–7 specified for defining a low-risk poly- Fumaric acid ...... 110–17–8 mer in 40 CFR 723.250, as an inert ingre- Gamma-cyclodextrin ...... 17465–86–0 Gellan gum ...... 71010–52–1 dient in a pesticide chemical formula- D-Glucitol (sorbitol) ...... 50–70–4 tion, including antimicrobial pesticide Glycerol (glycerin) (1,2,3-propanetriol) ...... 56–81–5 Guar gum ...... 9000–30–0 chemical formulations, are exempted Humic acid ...... 1413–93–6 from the requirement of a tolerance Humic acid, potassium salt ...... 68514–28–3 under FFDCA section 408, if such use is Humic acid, sodium salt ...... 68131–04–4 Lactic acid, n-butyl ester ...... 138–22–7 in accordance with good agricultural or Lactic acid, n-butyl ester, (S) ...... 34451–19–9 manufacturing practices. Lactic acid, ethyl ester ...... 97–64–3 Lactic acid, ethyl ester,(S) ...... 687–47–8 Polymer CAS No. Lanolin ...... 8006–54–0 Lecithins ...... 8002–43–5 Lecithins, soya ...... 8030–76–0 Acetic acid ethenyl ester, polymer with ethenol 137091– Licorice Extract ...... 68916–91–6 and (a)-2-propenyl-(w)-hydroxypoly (oxy-1,2- 12–4 Maltodextrin ...... 9050–36–6 ethanediyl) minimum number average molec- Paper ...... None ular weight (in amu), 15,000 Potassium chloride ...... 7447–40–7 2-Propanol (isopropyl alcohol) ...... 67–63–0 Acetic acid ethenyl ester, polymer with 1-eth- 25086–89– Red cabbage color, expressed from edible red enyl-2-pyrrolidinone 9 cabbage heads via a pressing process using only acidified water ...... None Acrylic acid, polymerized, and its ethyl and None Silica, amorphous, fumed (crystalline free) ...... 112945–52– methyl esters 5 Silica, amorphous, precipitated and gel ...... 7699–41–4 Acrylic acid-sodium acrylate-sodium-2- 97953–25– Silica gel ...... 63231–67–4 methylpropanesulfonate copolymer, minimum 8 Silica gel, precipitated, crystalline-free ...... 112926–00– average molecular weight (in amu), 4,500 8 Silica, hydrate ...... 10279–57–9 Acrylic acid-stearyl methacrylate copolymer, 27756–15– Silica, vitreous ...... 60676–86–0 minimum number average molecular weight 6 Soap (The water soluble sodium or potassium (in amu), 2,500 salts of fatty acids produced by either the saponification of fats and oils, or the neutral- Acrylic acid, styrene, a-methyl styrene copoly- 89678–90– ization of fatty acid) ...... None mer, ammonium salt, minimum number aver- 0 Sorbic acid, potassium salt ...... 24634–61–5 age molecular weight (in amu), 1,250 Soapbark (Quillaja saponin) ...... 1393–03–9 Sodium alginate ...... 9005–38–3 Sodium chloride ...... 7647–14–5 Acrylic acid terpolymer, partial sodium salt, 151006– Syrups, hydrolyzed starch, hydrogenated ...... 68425–17–2 minimum number average molecular weight 66–5 Ultramarine blue (C.I. Pigment Blue 29) ...... 57455–37–5 (in amu), 2,400 Urea ...... 57–13–6 Vanillin ...... 121–33–5 Xanthan gum ...... 11138–66–2

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Polymer CAS No. Polymer CAS No.

Acrylic polymers composed of one or more of None Butyl acrylate-vinyl acetate-acrylic acid copoly- 65405–40– the following monomers: Acrylic acid, methyl mer, minimum number average molecular 5 acrylate, ethyl acrylate, butyl acrylate, hy- weight (in amu), 18,000 droxyethyl acrylate, hydroxypropyl acrylate, hydroxybutyl acrylate, carboxyethyl acrylate, Castor oil, polyoxyethylated; the None methacrylic acid, methyl methacrylate, ethyl poly(oxyethylene) content averages 5–54 methacrylate, butyl methacrylate, isobutyl moles methacrylate, hydroxyethyl methacrylate, hydroxypropyl methacrylate, hydroxybutyl Chlorinated polyethylene 64754–90– methacrylate, lauryl methacrylate, and stearyl 1 methacrylate; with none and/or one or more of the following monomers: Acrylamide, N- Cross-linked nylon-type polymer formed by the None methyl acrylamide, N,N-dimethyl acrylamide, reaction of a mixture of sebacoyl chloride N-octylacrylamide, maleic anhydride, maleic and polymethylene polyphenylisocycanate acid, monoethyl maleate, diethyl maleate, with a mixture of ethylenediamine and monooctyl maleate, dioctyl maleate; and their diethylenetriamine corresponding sodium, potassium, ammo- nium, isopropylamine, triethylamine, Cross-linked polyurea-type encapsulating poly- None monoethanolamine, and/or triethanolamine mer salts; the resulting polymer having a min- imum number average molecular weight (in Dimethylpolysiloxane minimum number average 63148–62– amu), 1,200 molecular weight (in amu), 6,800 9

Acrylonitrile-butadiene copolymer conforming to 9003–18–3 Dimethyl silicone polymer with silica, minimum 67762–90– 21 CFR 180.22, minimum average molecular number average molecular weight (in amu), 7 weight (in amu), 1,000. 1,100,000

Acrylonitrile-styrene-hydroxypropyl methacrylate None a-(o,p-Dinonylphenyl)-w- 9014–93–1 copolymer, minimum number average molec- hydroxypoly(oxyethylene) produced by con- ular weight (in amu), 447,000 densation of 1 mole of dinonylphenol (nonyl group is a propylene trimer isomer) with an a-alkyl (C12–C15) - w- 68551–13– average of 140-160 moles of ethylene oxide hydroxypol- 3 y(oxypropylene)poly(oxyethylene)copolymers Docosyl methacrylate-acrylic acid copolymer, or None (where the poly(oxypropylene) content is 3– docosyl methacrylate-octadecyl methacrylate- 60 moles and the poly(oxyethylene) content acrylic acid copolymer, minimum number av- is 5–80 moles), the resulting ethoxylated erage molecular weight (in amu), 3,000 propoxylated (C12–C15) alcohols having a minimum molecular weight (in amu), 1,500 1,12-Dodecanediol dimethacrylate polymer, None minimum molecular weight (in amu), 100,000 Alkyl (C12–C20) methacrylate-methacrylic acid None copolymer, minimum molecular weight (in a-(p-Dodecylphenyl)-w- 9014–92–0 amu), 11,900 hydroxypoly(oxyethylene) produced by the 26401–47– condensation of 1 mole of dodecylphenol 8 2H-Azepin-2-one, 1-ethenylhexahydro-, 25189–83– (dodecyl group is a propylene tetramer iso- homopolymer 7 mer) with an average of 30-70 moles of ethylene oxide 1,3 Benzene dicarboxylic acid, 5-sulfo-, 1,3-di- 212842– methyl ester, sodium salt, polymer with 1,3- 88–1 1, 2-Ethanediamine, polymer with methyl 26316–40– benzene dicarboxylic acid, 1,4-benzene oxirane and oxirane, minimum number aver- 5 dicarboxylic acid, dimethyl 1,4-benzene age molecular weight (in amu), 1,100 dicarboxylate and 1,2-ethanediol, minimum number average molecular weight (in amu), Ethylene glycol dimethyacrylate-lauryl meth- None 2,580 acrylate copolymer, minimum molecular weight (in amu), 100,000 3,5-Bis(6-isocyanatohexyl)-2H-1,3,5-oxadiazine- 87823–33– 2,4,6-(3H,5H)-trione, polymer with 4 Ethylene glycol dimethacrylate polymer, min- None diethylenetriamine, minimum number average imum molecular weight (in amu), 100,000 molecular weight (in amu), 1,000,000 Formaldehyde, polymer with a-[bis(1- 157291– Butadiene-styrene copolymer None phenylethyl)phenyl]-w-hydroxypoly(oxy-1,2- 93–5 ethanediyl), number average molecular 1,4-Butanediol-methylenebis(4- 9018– 04–6 weight (in amu), 1,803 phenylisocyanate)-poly(tetramethylene glycol) copolymer, minimum molecular weight (in Fumaric acid-isophthalic acid-styrene-ethylene/ None amu) 158,000 propylene glycol copolymer, minimum aver- age molecular weight (in amu), 1×1018 Butene, homopolymer 9003–29–6 Hexadecyl acrylate-acrylic acid copolymer, None 2-Butenedioic acid (Z)-, polymer with ethenol 139871– hexadecyl acrylate-butyl acrylate-acrylic acid and ethenyl acetate, sodium salt, minimum 83–3 copolymer, or hexadecyl acrylate-dodecyl ac- number average molecular weight (in amu), rylate-acrylic acid copolymer, minimum num- 75,000 ber average molecular weight (in amu), 3,000 595

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Polymer CAS No. Polymer CAS No.

Hexamethyl disilizane, reaction product with 68909–20– Methacrylic acid-methyl methacrylate-poly- 100934– silica, minimum number average molecular 6 ethylene glycol methyl ether methacrylate co- 04–1 weight (in amu), 645,000 polymer, minimum number averge molecular weight (in amu), 3,700 1,6-Hexanediol dimethyacrylate polymer, min- None imum molecular weight (in amu), 100,000 Methacrylic copolymer, minimum number aver- 63150–03– age molecular weight (in amu), 15,000 8 a-Hydro-w-hydroxy-poly(oxyethylene) C8 alkyl 330977– ether citrates, poly(oxyethylene) content is 4– 00–9 Methyl methacrylate-methacrylic acid- 119724– 12 moles, minimum number average molec- monomethoxypolyethylene glycol methacry- 54–8 ular weight (in amu) 1,300. late copolymer,) minimum number average molecular weight (in amu), 2,730 a-Hydro-w-hydroxy-poly(oxyethylene) C10– 330985– C16-alkyl ether citrates, poly(oxyethylene) 58–5 Methyl methacrylate-2-sulfoethyl methacrylate- None content is 4–12 moles, minimum number av- dimethylaminoethylmethacrylate-glycidyl erage molecular weight (in amu) 1,100. methacrylate-styrene-2-ethylhexyl acrylate graft copolymer, minimum average molecular a-Hydro-w-hydroxy-poly(oxyethylene) C16– 330985– weight (in amu), 9,600 C18-alkyl ether citrates, poly(oxyethylene) 61–0 content is 4–12 moles, minimum number av- Methyl vinyl ether-maleic acid copolymer), min- 25153–40– erage molecular weight (in amu) 1,300. imum number average molecular weight (in 6 amu), 75,000 a-Hydro-w-hydroxypoly(oxyethylene), minimum None molecular weight (in amu), 100,000 Methyl vinyl ether-maleic acid copolymer, cal- 62386–95– cium sodium salt, minimum number average 2 a-Hydro-w-hydroxypoly(oxyethylene)poly None molecular weight (in amu), 900,000 (oxypropylene) poly(oxyethylene) block co- polymer; the minimum poly(oxypropylene) Monophosphate ester of the block copolymer None content is 27 moles and the minimum molec- a-hydro-w-hydroxypoly(oxyethylene) ular weight (in amu) is 1,900 poly(oxypropylene) poly(oxyethylene); the poly(oxypropylene) content averages 37–41 a-Hydro-w-hydroxypoly(oxypropylene); min- None moles, average molecular weight (in amu), imum molecular weight (in amu) 2,000 8,000 12-Hydroxystearic acid-polyethylene glycol co- 70142–34– a-(p-Nonylphenyl)-w-hydroxypoly(oxyethylene) None polymer, minimum number average molec- 6 mixture of dihydrogen phosphate and ular weight (in amu), 3,690 monohydrogen phosphate esters and the corresponding ammonium, calcium, magne- Isodecyl alcohol ethoxylated (2–8 moles) poly- None sium, monoethanolamine, potassium, so- mer with chloromethyl oxirane, minimum dium, and zinc salts of the phosphate esters; number average molecular weight (in amu) the nonyl group is a propylene trimer isomer 2,500 and the poly(oxyethylene) content averages 30 moles Lauryl methacrylate-1,6-hexanediol None dimethacrylate copolymer, minimum molec- a-(p-Nonylphenyl)-w-hydroxypoly(oxyethylene) None ular weight (in amu), 100,000 sulfate, and its ammonium, calcium, magne- sium, monoethanolamine, potassium, so- Maleic acid-butadiene copolymer None dium, and zinc salts; the nonyl group is a propylene trimer isomer and the Maleic acid monobutyl ester-vinyl methyl ether 25119–68– poly(oxyethylene) content averages 30-90 copolymer, minimum average molecular 0 moles of ethylene oxide weight (in amu), 52,000 a-(p-Nonylphenyl-w-hydroxypoly(oxypropylene) None Maleic acid monoethyl ester-vinyl methyl ether 25087–06– block polymer with poly(oxyethylene); copolymer, minimum average molecular 3 polyoxypropylene content of 10–60 moles; weight (in amu), 46,000 polyoxyethylene content of 10–80 moles; mo- lecular weight (in amu), 1,200–7,100. Maleic acid monoisopropyl ester-vinyl methyl 31307–95– ether copolymer, minimum average molec- 6 ular weight (in amu), 49,000 a-(p-Nonylphenyl)poly(oxypropylene) block None polymer with poly(oxyethylene); poly oxy- Maleic anhydride-diisobutylene copolymer, so- 37199–81– ethylene content 30 to 90 moles; molecular dium salt, minimum number average molec- 8 weight (in amu) averages 3,000 ular weight (in amu) 5,0007–18,000 Octadecanoic acid, 12-hydroxy-, homopolymer, 58128–22– Maleic anhydride-methylstyrene copolymer so- 60092–15– octadecanoate minimum number average 6), dium salt, minimum number average molec- 1 molecular weight (in amu), 1,370 ular weight (in amu), 15,000 a-cis-9-Octadecenyl-w- None Maleic anhydride-methyl vinyl ether, copolymer, None hydroxypoly(oxyethylene); the octadecenyl average molecular weight (in amu), 250,000 group is derived from oleyl alcohol and the poly(oxyethylene) content averages 20 moles

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Polymer CAS No. Polymer CAS No.

Octadecyl acrylate-acrylic acid copolymer, octa- None Polyoxyethylated sorbitol fatty acid esters; the None decyl acrylate-dodecyl acrylate-acrylic acid sorbitol solution containing up to 15% water copolymer, octadecyl methacrylate-butyl ac- is reacted with 20–50 moles of ethylene rylate-acrylic acid copolymer, octadecyl meth- oxide and aliphatic alkanoic and/or alkenoic acrylate-hexyl acrylate-acrylic acid copoly- fatty acids C8 through C22 with minor mer, octadecyl methacrylate-dodecyl acry- amounts of associated fatty acids; the result- late-acrylic acid copolymer, or octadecyl ing polyoxyethylene sorbitol ester having a methacrylate-dodecyl methacrylate-acrylic minimum molecular weight (in amu), 1,300 acid copolymer, minimum number average

molecular weight (in amu) 3,000 Poly(oxyethylene/oxypropylene) monoalkyl (C6– 102900– C10) ether sodium fumarate adduct, minimum 02–7 Oleic acid diester of a-hydro-w- None number average molecular weight (in amu), hydroxypoly(oxyethylene); the 1,900 poly(oxyethylene), average molecular weight (in amu), 2,300 Polyoxymethylene copolymer, minimum number None average molecular weight (in amu), 15,000 Oxirane, decyl-, reaction products with poly- 903890– ethylene-polypropylene glycol ether with 89–1 Poly(oxypropylene) block polymer with None trimethylolpropane (3:1) poly(oxyethylene), molecular weight (in amu), 1,800–16,000 Oxirane, hexadecyl-, reaction products with pol- 893427– yethylene-polypropylene glycol ether with 80–0 Poly(phenylhexylurea), cross-linked, minimum None trimethylolpropane (3:1) average molecular weight (in amu), 36,000

Oxirane, methyl-, polymer with oxirane, ether 903890– Polypropylene 9003–07–0 with 2-ethyl-2-(hydroxymethyl) – 1,3 - 90–4 propanediol (3:1), reaction products with Polystyrene, minimum number average molec- 9003–53–6 tetradecyloxirane ular weight (in amu), 50,000

Oxirane, methyl-, polymer with oxirane, 85637–75– Polytetrafluoroethylene 9002–84–0 mono[2-(2-butoxyethoxy) ethyl] ether, min- 8 imum number average molecular weight (in Polyvinyl acetate, copolymer with maleic anhy- None amu), 2,500 dride, partially hydrolyzed, sodium salt, min- imum number average molecular weight (in Oxirane, methyl-, polymer with Oxirane, 9038–95–3 amu), 53,000 Monobutyl Ether Polyvinylpyrrolidone butylated polymer, min- 26160–96– Polyamide polymer derived from sebacic acid, None imum number average molecular weight (in 3 vegetable oil acids with or without amu), 9,500 dimerization, terephthalic acid and/or ethyl- enediamine Polyvinyl acetate, minimum molecular weight None (in amu), 2,000 Polyethylene glycol-polyisobutenyl anhydride- 68650–28– tall oil fatty acid copolymer, minimum number 2 Polyvinyl acetate—polyvinyl alcohol copolymer, 25213–24– average molecular weight (in amu), 2,960 minimum number average molecular weight 5 (in amu), 50,000 Polyethylene, oxidized, minimum number aver- None age molecular weight (in amu), 1,200 Polyvinyl alcohol 9002–89–5

Polymethylene polyphenylisocyanate, polymer None Polyvinyl chloride None with ethylene diamine, diethylene triamine and sebacoyl chloride, cross-linked; minimum Polyvinyl chloride, minimum number average 9002–86–2 number average molecular weight (in amu), molecular weight (in amu), 29,000 100,000 Poly(vinylpyrrolidone), minimum number aver- 9003–39–8 Polyoxyethylated primary amine (C14–C18); the None age molecular weight (in amu), 4,000 fatty amine is derived from an animal source and contains 3% water; the poly(oxyethylene) Poly(vinylpyrrolidone-1-eicosene), minimum av- 28211–18– content averages 20 moles erage molecular weight (in amu), 3,000 9

Polyoxyethylated sorbitol fatty acid esters; the None Poly(vinylpyrrolidone-1-hexadecene), minimum 63231–81– polyoxyethylated sorbitol solution containing average molecular weight (in amu), 4,700 2 15% water is reacted with fatty acids limited to C12, C14, C16, and C18, containing minor 2-Propene-1-sulfonic acid sodium salt, polymer None amounts of associated fatty acids; the with ethenol and ethenyl acetate, number av- poly(oxyethylene) content averages 30 erage molecular weight (in amu) 6,000– moles. 12,000

2-Propenoic acid, methyl ester, polymer with 886993– ethenyl acetate, hydrolyzed, sodium salts. 11–9

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Polymer CAS No. Polymer CAS No.

2-Propenoic acid, 2-Methyl-, Polymer with Butyl 153163– Tetraethoxysilane, polymer with 104133– 2-Propenoate, Methyl 2-Methyl-2-Propenoate, 36–1 hexamethyldisiloxane, minimum number av- 09–7 Methyl 2-Propenoate and 2-Propenoic Acid, erage molecular weight (in amu), 6,500 graft, Compound with 2-Amino-2-Methyl-1- Propanol a-[p-(1,1,3,3-Tetramethylbutyl)phenyl]-w- 9036–19–5 hydroxypoly(oxyethylene) produced by the 9002–93–1 2-Propenoic Acid, 2-Methyl-, Polymer with 146753– condensation of 1 mole of p-(1,1,3,3- Ethenylbenzene, 2-Ethylhexyl 2-Propenoate, 99–3 tetramethylbutyl)phenol with a range of 30-70 2-Hydroxyethyl 2-Propenoate, N- moles of ethylene oxide (Hydroxymethyl) -2-Methyl-2-Propenamide and Methyl 2-Methyl-2-Propenoate, Ammo- a-[p-(1,1,3,3-Tetramethylbutyl)phenyl] None nium Salt poly(oxypropylene) block polymer with poly(oxyethylene); the poly(oxypropylene) 2-Propenoic, 2-methyl-, polymers with ethyl ac- 888969– content averages 25 moles, the rylate and polyethylene glycol methylacrylate 14–0 poly(oxyethylene) content averages 40 C18-22 alkyl ethers moles, the molecular weight (in amu) aver- ages 3,400 2-Propenoic acid, polymer with 2-propenamide, 25085–02– sodium salt, minimum number average mo- 3 a-[2,4,6-Tris[1-(phenyl)ethyl]phenyl]-w-hydroxy None lecular weight (in amu), 18,000 poly(oxyethylene) poly(oxypropylene) copoly- mer, the poly(oxypropylene) content aver- 2-Propenoic acid, sodium salt, polymer with 2- 25987–30– ages 2–8 moles, the poly(oxyethylene) con- propenamide, minimum number average mo- 8 tent averages 16–30moles, average molec- lecular weight (in amu), 18,000 ular weight (in amu), 1,500

Silane, dichloromethyl- reaction product with 68611–44– Urea-formaldehyde copolymer, minimum aver- 9011–05–6 silica minimum number average molecular 9 age molecular weight (in amu), 30,000 weight (in amu), 3,340,000 Vinyl acetate-allyl acetate-monomethyl maleate None Sodium polyflavinoidsulfonate, consisting chief- None copolymer, minimum average molecular ly of the copolymer of catechin and weight (in amu), 20,000 leucocyanidin Vinyl acetate-ethylene copolymer, minimum 24937–78– Soybean oil, ethoxylated; the poly(oxyethylene) 61791–23– number average molecular weight (in amu), 8 content averages 10 moles or greater 9 69,000

Stearyl methacrylate-1,6-hexanediol None Vinyl acetate polymer with none and/or one or None dimethacrylate copolymer, minimum molec- more of the following monomers: Ethylene, ular weight (in amu), 100,000 propylene, N-methyl acrylamide, acrylamide, monoethyl maleate, diethyl maleate, Styrene, copolymers with acrylic acid and/or None monooctyl maleate, dioctyl maleate, maleic methacrylic acid, with none and/or one or anhydride, maleic acid, octyl acrylate, butyl more of the following monomers: acrylate, ethyl acrylate, methyl acrylate, Acrylamidopropyl methyl sulfonic acid, meth- acrylic acid, octyl methacrylate, butyl meth- allyl sulfonic acid, 3-sulfopropyl acrylate, 3- acrylate, ethyl methacrylate, methyl meth- sulfopropyl methacrylate, hydroxypropyl acrylate, methacrylic acid, carboxyethyl acry- methacrylate, hydroxypropyl acrylate, hy- late, and diallyl phthalate; and their cor- droxyethyl methacrylate, and/or hydroxyethyl responding sodium, potassium, ammonium, acrylate; and its sodium, potassium, ammo- isopropylamine, triethylamine, nium, monoethanolamine, and triethanol- monoethanolamine and/or triethanolamine amine salts; the resulting polymer having a salts; the resulting polymer having a min- minimum number average molecular weight imum number average molecular weight (in (in amu), 1,200 amu), 1,200

Styrene, 2-ethylhexyl acrylate, butyl acrylate 30795–23– Vinyl acetate-vinyl alcohol-alkyl lactone copoly- None copolymer, minimum number average molec- 4 mer, minimum number average molecular ular weight (in amu), 4,200 weight (in amu), 40,000; minimum viscosity of 18 centipoise Styrene-2-ethylhexyl acrylate-glycidyl methacry- None late-2-acrylamido-2-methylpropanesulfonic Vinyl alcohol-disodium itaconate copolymer, None acid graft copolymer, minimum number aver- minimum average molecular weight (in amu), age molecular weight (in amu), 12,500 50,290

Styrene-maleic anhydride copolymer None Vinyl alcohol-vinyl acetate copolymer, benz- None aldehyde-o-sodium sulfonate condensate, minimum number average molecular weight Styrene-maleic anhydride copolymer, ester de- None (in amu), 20,000 rivative Vinyl alcohol-vinyl acetate-monomethyl male- None Tetradecyl acrylate-acrylic acid copolymer, min- None ate, sodium salt-maleic acid, disodium salt-g- imum number average molecular weight (in butyrolactone acetic acid, sodium salt copoly- amu), 3,000 mer, minimum number average molecular weight (in amu), 20,000 598

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Polymer CAS No. sects and Mites,’’ R.P.M. Bond et al., p. 280 ff., 1971). This specification can be Vinyl chloride-vinyl acetate copolymers None satisfied either by determining that Vinyl pyrrolidone-acrylic acid copolymer, min- 28062–44– each master seed lot brought into pro- imum number average molecular weight (in 4 duction is a Bacillus thuringiensis strain amu), 6,000 which does not produce b-exotoxin Vinyl pyrrolidone- 30581–59– under standard manufacturing condi- dimethylaminoethylmethacrylate copolymer, 0 tions or by periodically determining minimum number average molecular weight that b-exotoxin synthesized during (in amu), 20,000 spore production is eliminated by the Vinyl pyrrolidone-styrene copolymer 25086–29– subsequent spore-harvesting procedure. 7 (b) Exemption from the requirement of a tolerance is established for resi- [67 FR 36528, May 24, 2002, as amended at 68 dues of the microbial insecticide Bacil- FR 8850, Feb. 26, 2003; 68 FR 10986, Mar. 7, lus thuringiensis Berliner, as specified 2003; 68 FR 15967, Apr. 2, 2003; 68 FR 23072, in paragraph (a) of this section, in or Apr. 30, 2003; 69 FR 4073, Jan. 28, 2004; 69 FR on beeswax and honey and all other 50077, Aug. 13, 2004; 71 FR 42277, 42281, 42285, raw agricultural commodities when it 42288, 42291, 42295, July 26, 2006; 71 FR 45424, Aug. 9, 2006; 71 FR 57439, Sept. 29, 2006; 71 FR is applied either to growing crops, or 58521, Oct. 4, 2006; 72 FR 8916, Feb. 28, 2007; 72 when it is applied after harvest in ac- FR 10077, Mar. 7, 2007] cordance with good agricultural prac- tices. § 180.1011 Viable spores of the micro- organism Bacillus thuringiensis [36 FR 22540, Nov. 25, 1971, as amended at 38 Berliner; exemption from the re- FR 19045, July 17, 1973; 42 FR 28540, June 3, quirement of a tolerance. 1977; 45 FR 43721, June 30, 1980; 45 FR 56347, Aug. 25, 1980] (a) For the purposes of this section the microbial insecticide for which ex- § 180.1016 Ethylene; exemption from emption from the requirement of a tol- the requirement of a tolerance. erance is being established shall have Ethylene is exempted from the re- the following specifications: quirement of a tolerance for residues (1) The microorganism shall be an au- when: thentic strain of Bacillus thuringiensis (a) For all food commodities, it is Berliner conforming to the morpho- used as a plant regulator on plants, logical and biochemical characteristics seeds, or cuttings and on all food com- of Bacillus thuringiensis as described in modities after harvest and when ap- Bergey’s Manual of Determinative Bac- plied in accordance with good agricul- teriology, Eighth Edition. tural practices. (2) Spore preparations of Bacillus (b) Injected into the soil to cause pre- thuringiensis Berliner shall be produced mature germination of witchweed in by pure culture fermentation proce- bean (lima and string), cabbage, canta- dures with adequate control measures loupe, collard, corn, cotton, cucumber, during production to detect any eggplant, okra, onion, pasture grass, changes from the characteristics of the pea (field and sweet), peanut, pepper, parent strain or contamination by potato, sweet potato, sorghum, soy- other microorganisms. bean, squash, tomato, turnip, and wa- (3) Each lot of spore preparation, termelon fields as part of the U.S. De- prior to the addition of other mate- partment of Agriculture witchweed rials, shall be tested by subcutaneous control program. injection of at least 1 million spores into each of five laboratory test mice [39 FR 33315, Sept. 17, 1974, as amended at 40 weighing 17 grams to 23 grams. Such FR 19477, May 5, 1975; 64 FR 31505, June 11, test shall show no evidence of infection 1999] or injury in the test animals when ob- served for 7 days following injection. § 180.1017 Diatomaceous earth; exemp- (4) Spore preparations shall be free of tion from the requirement of a tol- erance. the Bacillus thuringiensis b-exotoxin when tested with the fly larvae tox- (a) Diatomaceous earth is exempted icity test (‘‘Microbial Control of In- from the requirement of a tolerance for residues when used in accordance with

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good agricultural practice in pesticide COMMODITY formulations applied to growing crops, Beans, dry, edible Peppers, chili to food commodities after harvest, and Corn, fodder Potatoes to animals. Corn, forage Rice (b) Diatomaceous earth may be safely Corn, grain Rice, straw used in accordance with the following Cottonseed Safflower, grain Sorghum, grain conditions. Application shall be lim- Flaxseed Sorghum, fodder ited solely to spot and/or crack and Flax, straw crevice treatments in food or feed proc- Sorghum, forage Guar beans Soybeans essing and food or feed storage areas in Peas, southern Sunflower seed accordane with the precribed condi- tions: (b) A time-limited exemption from (1) It is used or intended for use for the requirement of a tolerance is estab- control of insects in food or feed proc- lished for residues of the defoliant/des- essing and food or feed storage areas: iccant in connection with use of the Provided, That the food or feed is re- pesticide under section 18 emergency moved or covered prior to such use. exemptions granted by EPA. The ex- (2) To assure safe use of the insecti- emption will expire and is revoked on cide, its label and labeling shall con- the date specified in the following form to that registered by the U.S. En- table: vironmental Protection Agency, and it Expiration/ shall be used in accordance with such Commodity Parts per revocation label and labeling. million date

[65 FR 33716, May 24, 2000] Wheat ...... NA 12/31/06

§ 180.1019 Sulfuric acid; exemption from the requirement of a toler- [54 FR 9800, Mar. 8, 1989, as amended at 60 FR ance. 4862, Jan. 25, 1995; 62 FR 63863, Dec. 3, 1997; 63 FR 35846, July 1, 1998; 64 FR 42849, Aug. 6, (a) Residues of sulfuric acid are ex- 1999; 65 FR 48639, Aug. 9, 2000; 68 FR 2247, Jan. empted from the requirement of a tol- 16, 2003; 69 FR 71717, Dec. 10, 2004] erance when used in accordance with good agricultural practice when used § 180.1021 Copper; exemption from the as a herbicide in the production of gar- requirement of a tolerance. lic and onions, and as a potato vine (a) Copper is exempted from the re- dessicant in the production of potatoes. quirement of a tolerance in meat, (b) Residues of sulfuric acid are ex- milk, poultry, eggs, fish, shellfish, and empted from the requirement of a tol- irrigated crops when it results from the erance in meat, milk, poultry, eggs, use of: fish, shellfish, and irrigated crops when (1) Copper sulfate as an algicide or it results from the use of sulfuric acid herbicide in irrigation conveyance sys- as an inert ingredient in a pesticide tems and lakes, ponds, reservoirs, or product used in irrigation conveyance bodies of water in which fish or shell- systems and lakes, ponds, reservoirs, or fish are cultivated. bodies of water in which fish or shell- (2) Basic copper carbonate (mala- fish are cultivated. The sulfuric acid is chite) as an algicide or herbicide in im- not to exceed 10% of the pesticide for- pounded and stagnant bodies of water mulation (non-aerosol formulations (3) Copper triethanolamine and cop- only). per monoethanolamine as an algicide [69 FR 40787, July 7, 2004] or herbicide in fish hatcheries, lakes, ponds, and reservoirs § 180.1020 Sodium chlorate; exemption (4) Cuprous oxide bearing antifouling from the requirement of a toler- coatings for control of algae or other ance. coatings for control of algae or other (a) Sodium chlorate is exempted from organisms on submerged concrete or the requirement of a tolerance for resi- other (irrigation) structures. dues in or on the following raw agricul- (b) The following copper compounds tural commodities when used as a defo- are exempt from the requirement of a liant, desiccant, or fungicide in accord- tolerance when applied (primarily) as a ance with good agricultural practice. fungicide to growing crops using good

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agricultural practices: Bordeaux mix- § 180.1023 Propanoic acid; exemptions ture, basic copper carbonate (mala- from the requirement of a toler- chite) (CAS Reg. No. 1184–64–1), copper ance. ethylenediamine complex, copper hy- (a) Postharvest application of pro- droxide (CAS Reg. No. 20427–59–2), cop- panoic acid or a mixture of methylene per lime mixtures, copper linoleate bispropionate and oxy(bismethylene) (CAS Reg. No. 7721–15–5), copper octa- bisproprionate when used as a fun- noate (CAS Reg. No. 20543–04–8), copper gicide is exempted from the require- oleate (CAS Reg. No. 10402–16–1), copper ment of a tolerance for residues in or oxychloride (CAS Reg. No. 1332–40–7), on the following raw agricultural com- copper sulfate basic (CAS Reg. No. modities: Alfalfa, barley grain, Ber- 1344–73–6), cupric oxide (CAS Reg. No. muda grass, bluegrass, brome grass, clover, corn grain, cowpea hay, fescue, 1317–38–0), and cuprous oxide (CAS Reg. lespedeza, lupines, oat grain, orchard No. 1317–19–1). grass, peanut hay, peavine hay, rye (c) Copper sulfate pentahydrate (CAS grass, sorghum grain, soybean hay, Reg. No. 7758–99–8) is exempt from the sudan grass, timothy, vetch, and wheat requirement of a tolerance when ap- grain. plied as a fungicide to growing crops or (b) Propanoic acid is exempt from the to raw agricultural commodities after requirement of a tolerance for residues harvest, and as a bactericide/fungicide in or on meat and meat byproducts of in or on meat, fat and meat by-prod- cattle, sheep, hogs, goats, horses, and ucts of cattle, sheep, hogs, goats, poultry, milk, and eggs when applied as horses and poultry, milk and eggs when a bactericide/fungicide to livestock applied as a bactericide/fungicide to drinking water, poultry litter, and animal premises and bedding. storage areas for silage and grain. (d) Copper (II) hydroxide (CAS Reg. (c) Preharvest and postharvest appli- No. 20427–59–2) is exempt from the re- cation of propanoic acid (CAS Reg. No. quirement of a tolerance when applied 79–09–4), propanioc acid, calcium salt (CAS Reg. No. 4075–81–4), and propanioc to growing crops or to raw agricultural sodium salt (CAS Reg. No. 137–40–6) are commodities as an inert ingredient (for exempted from the requirement of a pH control) in pesticide products. tolerance on all crops when used as ei- [65 FR 68912, Nov. 15, 2000, as amended at 69 ther an active or inert ingredient in ac- FR 4069, Jan. 28, 2004; 71 FR 46110, Aug. 11, cordance with good agricultural prac- 2006] tice in pesticide formulations applied to growing crops, to raw agricultural § 180.1022 Iodine-detergent complex; commodities before and after harvest exemption from the requirement of and to animals. a tolerance. [69 FR 47025, Aug. 4, 2004] The aqueous solution of hydriodic acid and elemental iodine, including § 180.1025 Xylene; exemption from the one or both of the surfactants (a) requirement of a tolerance. polyoxypropylene-polyoxyethylene gly- Xylene is exempted from the require- col nomionic block polymers (min- ment of a tolerance when used as an imum average molecular weight 1,900) aquatic herbicide applied to irrigation and (b) a-(p- nonylphenyl)-omega- conveyance systems in accordance with hydroxypoly (oxyethylene) having a the following conditions: maximum average molecular weight of (a) It is to be used only in programs 748 and in which the nonyl group is a of the Bureau of Reclamation, U.S. De- propylene trimer isomer, is exempted partment of Interior, and cooperating from the requirement of a tolerance for water user organizations. (b) It is to be applied as an emulsion residues in eggs and poultry when used at an initial concentration not to ex- as a sanitizer in poultry drinking ceed 750 parts per million. water. (c) It is not to be applied when there [37 FR 6581, Mar. 31, 1972] is any likelihood that the irrigation water will be used as a source of raw water for a potable water system or

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where return flows of such treated irri- § 180.1033 Methoprene; exemption gation water into receiving rivers and from the requirement of a toler- streams would contain residues of xy- ance. lene in excess of 10 parts per million. Methoprene is exempt from the re- (d) Xylene to be used as an aquatic quirement of a tolerance in or on all herbicide shall meet the requirement food commodities when used to control limiting the presence of a polynuclear insect larvae. aromatic hydrocarbons as listed in 21 CFR 172.250. [68 FR 34829, June 11, 2003] [38 FR 16352, June 22, 1973, as amended at 50 § 180.1035 Pine oil; exemption from the FR 2980, Jan. 3, 1985] requirement of a tolerance. Pine oil is exempted from the re- § 180.1027 Nuclear polyhedrosis virus quirement of a tolerance for residues in of Heliothis zea; exemption from the raw agricultural commodities the requirement of a tolerance. honey and beeswax, when present (a) For the purposes of this section, therein as a result of its use as a deo- the viral insecticide must be produced dorant at no more than 12 percent in with an unaltered and unadulterated formulation with the bee repellent bu- inoculum of the single-embedded tanoic anhydride applied in an absorb- Heliothis zea nuclear polyhedrosis virus ent pad over the hive. (HzSNPV). The identity of the seed virus must be assured by periodic [53 FR 52708, Dec. 29, 1988] checks. § 180.1037 Polybutenes; exemption (b) Each lot of active ingredient of from the requirement of a toler- the viral insecticide shall have the fol- ance. lowing specifications: (a) Polybutenes are exempt from the (1) The level of extraneous bacterial requirement of a tolerance for residues contamination of the final in or on the raw agricultural com- unformulated viral insecticide should modity cottonseed when used as a 7 not exceed 10 colonies per gram as de- sticker agent for formulations of the termined by an aerobic plate on attractant gossyplure (1:1 mixture of trypticase soy agar. (Z,Z)- and (Z,E)-7,11-hexadecadien-1-ol (2) Human pathogens, e.g., Sal- acetate) to disrupt the mating of the monella, Shigella, or Vibrio, must be pink bollworm. absent. (b) Polybutenes are exempt from the (3) Safety to mice as determined by requirement of a tolerance for residues an intraperitoneal injection study in or on the raw agricultural com- must be demonstrated. modity artichokes when used as a (4) Identity of the viral product, as sticker agent in multi-layered lami- determined by the most sensitive and nated controlled-release dispensers of standardized analytical technique, e.g., (Z)-11-hexadecenal to disrupt the mat- restriction endonuclease and/or SDS- ing of the artichoke plume moth. PAGE analysis, must be demonstrated. [42 FR 47205, Sept. 20, 1977; 42 FR 56114, Oct. (c) Exemptions from the requirement 21, 1977, as amended at 48 FR 21133, May 11, of a tolerance are established for the 1983] residues of the microbial insecticide Heliothis zea NPV, as specified in para- § 180.1040 Ethylene glycol; exemption graphs (a) and (b) of this section, in or from the requirement of a toler- on all agricultural commmodities in- ance. cluding: corn, cottonseed, beans, let- Ethylene glycol as a component of tuce, okra, peppers, sorghum, soy- pesticide formulations is exempt from beans, and tomatoes. the requirement of a tolerance when used in foliar applications to peanut [60 FR 42460, Aug. 16, 1995] plants. [43 FR 41393, Sept. 18, 1978]

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§ 180.1041 Nosema locustae; exemption § 180.1054 Calcium hypochlorite; ex- from the requirement of a toler- emptions from the requirement of a ance. tolerance. The insecticide Nosema locustae is ex- (a) Calcium hypochlorite is exempted empted from the requirement of a tol- from the requirement of a tolerance erance for residues in or on all raw ag- when used preharvest or postharvest in ricultural commodities. solution on all raw agricultural com- [47 FR 21537, May 19, 1982] modities. (b) Calcium hypochlorite is exempted § 180.1043 Gossyplure; exemption from from the requirement of a tolerance in the requirement of a tolerance. or on grapes when used as a fumigant The pheromone gossyplure, a 1:1 mix- postharvest by means of a chlorine ture of (Z,Z)- and (Z,E)-7,11- generator pad. hexadecadien-1-ol acetate) is exempt [59 FR 59165, Nov. 16, 1994] from the requirement of a tolerance in or on the raw agricultural commodity § 180.1056 Boiled linseed oil; exemp- cottonseed when applied to cotton from tion from requirement of tolerance. capillary fibers. Boiled linseed oil (containing no [43 FR 20803, May 15, 1978] more than 0.33 percent manganese naphthenate and no more than 0.33 per- § 180.1049 Carbon dioxide; exemption cent cobalt naphthenate) is exempt from the requirement of a toler- ance. from the requirement of a tolerance when used as a coating agent for S- The insecticide carbon dioxide is ex- ethyl hexahydro-1H-azepine-1- empted from the requirement of a tol- carbothioate. No more than 15 percent erance when used after harvest in of the pesticide formulation may con- modified atmospheres for stored insect sist of ‘‘boiled linseed oil.’’ This exemp- control on food commodities. tion is limited to use on rice before edi- [65 FR 33716, May 24, 2000] ble parts form.

§ 180.1050 Nitrogen; exemption from [46 FR 33270, June 29, 1981] the requirements of a tolerance. § 180.1057 Phytophthora palmivora; ex- The insecticide nitrogen is exempted emption from requirement of toler- from the requirements of a tolerance ance. when used after harvest in modified atmospheres for stored product insect Phytophthora palmivora is exempted control on all food commodities. from the requirement of a tolerance in or on the raw agricultural commodity [65 FR 33716, May 24, 2000] citrus fruit. § 180.1052 2,2,5-trimethyl-3-dichloro- [46 FR 18695, Mar. 26, 1981] acetyl-1,3-oxazolidine; exemption from the requirement of a toler- § 180.1058 Sodium diacetate; exemp- ance. tion from the requirement of a tol- 2,2,5-trimethyl-3-dichloroacetyl-1,3- erance. oxazolidine is exempted from the re- Sodium diacetate, when used quirement of a tolerance when used as postharvest as a fungicide, is exempt an inert ingredient in formulations of from the requirement of a tolerance for the herbicides S-ethyl residues in or on alfalfa hay, Bermuda dipropylthiocarbamate, S-propyl grass hay, blue grass hay, brome grass dipropylthiocarbamate, and S-ethyl hay, clover hay, corn grain, oat grain, diisobutylthiocarbamate applied to orchard grass hay, sorghum grain, corn fields before the corn plants sudan grass hay, rye grass hay, and emerge from the soil with a maximum timothy hay. of 0.5 pound of the inert ingredient per acre. [58 FR 47215, Sept. 8, 1993] [45 FR 51201, Aug. 1, 1980]

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§ 180.1064 Tomato pinworm insect (cellulose acetate); cotton strings; fi- pheromone; exemption from the re- berboard squares) or mixed with a jel quirement of a tolerance. cleared under 40 CFR 180.920 or 180.950. An exemption from the requirement (c) The maximum actual dosage per of a tolerance is established for com- application per acre shall be 28.35 bined residues of both components of grams (one ounce avoirdupois) methyl the tomato pinworm insect pheromone eugenol and 9.45 grams (one-third (0.33) (E)-4-tridecen-1-yl acetate and (Z)-4- ounce avoirdupois) technical mala- tridecen-1-yl acetate in or on all raw thion. agricultural commodities (preharvest) [47 FR 9002, Mar. 3, 1982, as amended at 69 FR in accordance with the following pre- 23142, Apr. 28, 2004] scribed conditions: (a) Application shall be limited sole- § 180.1068 C12-C18 fatty acid potassium ly to point source dispensers or point salts; exemption from the require- source chopped fibers containing the ment of a tolerance.

tomato pinworm insect pheromone. C12-C18 fatty acids (saturated and un- (b) Cumulative yearly application saturated) potassium salts are exempt- cannot exceed 200 grams of tomato ed from the requirement of a tolerance pinworm pheromone per acre. for residues in or on all raw agricul- [58 FR 34376, June 25, 1993] tural commodities when used in ac- cordance with good agricultural prac- § 180.1065 2-Amino-4,5-dihydro-6-meth- tice. yl-4-propyl-s-triazolo(1,5- alpha)pyrimidin-5-one; exemption [60 FR 34871, July 5, 1995] from the requirement of a toler- ance. § 180.1069 (Z)-11-Hexadecenal; exemp- tion from the requirement of a tol- The inert ingredient, 2-amino-4,5- erance. dihydro-6-methyl-4-propyl-s- An exemption from the requirement triazolo(1,5-alpha)pyrimidin-5-one is of a tolerance is established for resi- exempted from the requirement of a dues of the biological insecticide tolerance when used as an emetic at (pheromone) (Z)-11-hexadecenal when not more than 0.3 percent in formula- tions of paraquat dichloride. Further used as a sex attractant on artichoke restrictions on this exemption are that plants to control the artichoke plume this ingredient may not be advertised moth. as an emetic and the paraquat product [47 FR 14906, Apr. 7, 1982] may not be promoted in any way be- cause of the inclusion of this inert in- § 180.1070 Sodium chlorite; exemption gredient. from the requirement of a toler- ance. [70 FR 46431, Aug. 10, 2005] Sodium chlorite is exempted from § 180.1067 Methyl eugenol and mala- the requirement of a tolerance for resi- thion combination; exemption from dues when used in accordance with the requirement of a tolerance. good agricultural practice as a seed- The insect attractant methyl eugenol soak treatment in the growing of the and the insecticide malathion are ex- raw agricultural commodities crop empt from the requirement of toler- group Brassica (cole) leafy vegetables ances on all raw agricultural commod- and radishes. ities when used in combination in Ori- [50 FR 51856, Dec. 20, 1985] ental fruit fly eradication programs under the authority of the U.S. Depart- § 180.1071 Peanuts, Tree Nuts, Milk, ment of Agriculture, in accordance Soybeans, Eggs, Fish, Crustacea, with the following directions and speci- and Wheat; exemption from the re- fications: quirement of a tolerance. (a) The combination shall be at the (a) General. Residues resulting from ratio of three parts methyl eugenol to the following uses of the food com- one part technical malathion (3:1). modity forms of peanuts, tree nuts, (b) This combination is to be impreg- milk, soybeans, eggs (including putres- nated on a carrier (cigarette filter tips cent eggs), fish, crustacea, and wheat

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are exempted from the requirement of quirement of a tolerance under FFDCA a tolerance in or on all food commod- section 408, if such use is in accordance ities under FFDCA section 408 (when with good agricultural practices and used as either an inert or an active in- such use is included in paragraph (a): gredient in a pesticide formulation), if such use is in accordance with good ag- Chemical Substance CAS No. ricultural practices: Caseins ...... 9000–71–9 (1) Use in pesticide products intended Caseins, ammonium complexes ...... 9005–42–9 to treat seeds. Caseins, hydrolyzates ...... 65072–00–6 (2) Use in nursery and greenhouse op- Caseins, potassium complexes ...... 68131–54–4 erations, as defined in 40 CFR 170.3, Caseins, sodium complexes ...... 9005–46–3 which includes seeding, potting and transplanting activities. [70 FR 1360, Jan. 7, 2005] (3) Pre-plant and at-transplant appli- cations. § 180.1072 Poly-D-glucosamine (4) Incorporation into seedling and (chitosan); exemption from the re- planting beds. quirement of a tolerance. (5) Applications to cuttings and bare roots. (a) An exemption from the require- (6) Applications to the field that ment of a tolerance is established for occur after the harvested crop has been residues of the biological plant growth removed. regulator poly-D-glucosamine when (7) Soil-directed applications around used as a seed treatment in or on bar- and adjacent to all plants. ley, beans, oats, peas, rice, and wheat. (8) Applications to rangelands, which (b) An exemption from the require- is land, mostly grasslands, whose ment of a tolerance is established for plants can provide food (i.e., forage) for residues of the biological plant growth grazing or browsing animals. regulator poly-D-glucosamine when (9) Use in chemigation and irrigation used as a pesticide in the production systems (via flood, drip, or furrow ap- any raw agricultural commodity. plication with no overhead spray appli- cations). [60 FR 19524, Apr. 19, 1995] (10) Application as part of a dry fer- tilizer on which an active ingredient is § 180.1073 Isomate-M; exemption from impregnated. the requirement of a tolerance. (11) Aerial and ground applications The oriental fruit moth pheromone that occur when no above-ground har- (Isomate-M) (Z-8-dodecen-l-yl acetate, vestable food commodities are present E-8-dodecen-l-yl acetate, Z-8-dodecen-l- (usually pre-bloom). ol) is exempt from the requirement of a (12) Application as part of an animal tolerance in or on all the raw agricul- feed-through product. tural commodities (food and feed) in- (13) Applications as gel and solid cluding peaches, quinces, nectarines, (non-liquid/non-spray) crack and crev- and macadamia nuts when used in or- ice treatments that place the gel or chards with encapsulated polyethylene bait directly into or on top of the tubing to control oriental fruit moth. cracks and crevices via a mechanism such as a syringe. [54 FR 22897, May 30, 1989, as amended at 55 (14) Applications to the same crop FR 23935, June 13, 1990] from which the food commodity is de- rived, whether the plant fraction(s) in- § 180.1074 F.D.&C. Blue No. 1; exemp- tended for harvest are present or not, tion from the requirement of a tol- e.g., applications of peanut meal when erance. applied to peanut plants. F.D.&C. Blue No. 1 is exempted from (b) Specific chemical substances. Resi- the requirement of a tolerance when dues resulting from the use of the fol- used as an aquatic plant control agent. lowing substances as either an inert or an active ingredient in a pesticide for- [47 FR 25963, June 16, 1982] mulation are exempted from the re-

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§ 180.1075 Colletotrichum § 180.1080 Plant volatiles and gloeosporioides f. sp. aeschynomene; pheromone; exemptions from the exemption from the requirement of requirement of a tolerance. a tolerance. An exemption from the requirement An exemption from the requirement of a tolerance is established for resi- of a tolerance is established for resi- dues of the plant volatiles cyclic dues of the mycoherbicide decadiene, cyclic decene, cyclic Colletotrichum gloeosporioides f. sp. pentadecatriene, and decatriene and aeschynomene in or on the following the pheromone Z-2-isopropenyl-1- raw agricultural commodities: methylcyclobutaneethanol; Z-3,3-di- COMMODITY methyl-D1,b-cyclohexaneethanol; Z-3,3- dimethyl-D1,a-cyclohexaneethanal; E- Rice grain 3,3-dimethyl-D1,a-cyclohexaneethanal Soybeans combination when applied to cotton in [47 FR 25742, June 15, 1982] hollow synthetic fibers.

§ 180.1076 Viable spores of the micro- [48 FR 28442, June 22, 1983] organism Bacillus popilliae; exemp- tion from the requirement of a tol- § 180.1083 Dimethyl sulfoxide; exemp- erance. tion from the requirement of a tol- erance. (a) For the purposes of this section the microbial insecticide for which ex- Dimethyl sulfoxide (DMSO) [CAS emption from the requirement of a tol- Registry Number 67–68–5] is exempted erance is being established shall have from the requirement of a tolerance the following specifications: when used as an inert solvent or cosol- (1) The microorganism shall be an au- vent in formulations with the following thentic strain of Bacillus popilliae con- pesticides when used in accordance forming to the morphological and bio- with good agricultural practices in or chemical characteristics of Bacillus on the following raw agricultural com- popilliae as described in Bergey’s Man- modities: ual of Determinative Bacteriology, Com- Eighth Edition. Pesticides modity (2) Spore preparations of Bacillus popilliae shall be produced by an ex- (a) Carbaryl (1-naphthyl methyl-carbamate) ...... Peas traction process from diseased Japa- (b) O-O-Diethyl O-(2-isopropyl-6-methyl-4- Peas pyrimidinyl) phosphorothioate. nese , and may contain a small percentage of the naturally occurring milky disease bacterium Bacillus [48 FR 54819, Dec. 7, 1983]) lentimorbus. § 180.1084 Monocarbamide dihydrogen (3) Each lot of spore preparation, sulfate; exemption from the require- prior to the addition of other mate- ment of a tolerance. rials, shall be tested by subcutaneous injection of at least 1 million spores Monocarbamide dihydrogen sulfate is into each of five laboratory test mice exempted from the requirement of a weighing 17 grams to 23 grams. Such tolerance when used as a herbicide or test shall show no evidence of infection desiccant in or on all raw agricultural of injury in the test animals when ob- commodities. served for 7 days following injection. [53 FR 12152, Apr. 13, 1988] (b) Exemption from the requirement of a tolerance is established for resi- § 180.1086 3,7,11-Trimethyl-1,6,10- dues of the microbial insecticide Bacil- dodecatriene-1-ol and 3,7,11- lus popilliae, as specified in paragraph trimethyl-2,6,10-dodecatriene-3-ol; (a) of this section in or on pasture and exemption from the requirement of rangeland forage when it is applied to a tolerance. growing crops in accordance with good The insect pheromone containing the agricultural practices. active ingredients 3,7,11-trimethyl- [47 FR 38535, Sept. 1, 1982] 1,6,10-dodecatriene-1-ol and 3,7,11-

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trimethyl-2,6,10-dodecatriene-3-ol is ex- methylmethanimidamide] applied to empted from the requirement of a tol- growing crops or animals. erance in or on all raw agricultural commodities. [53 FR 34509, Sept. 7, 1988; 53 FR 36696, Sept. 21, 1988] [52 FR 12165, Apr. 15, 1987; 52 FR 29014, Aug. 5, 1987] § 180.1092 Menthol; exemption from the requirement of a tolerance. § 180.1087 Sesame stalks; exemption An exemption from the requirement from the requirement of a toler- ance. of a tolerance is established for resi- dues of the pesticidal chemical men- An exemption from the requirement thol in or on beeswax and honey when of a tolerance is established for resi- used in accordance with good agricul- dues of the biorational nematicide ses- tural practice in over-wintering bee ame stalk in or on the following raw agricultural commodities: cotton, soy- hives. beans, potatoes, sugarbeets, tomatoes, [53 FR 47811, Nov. 28, 1988] bell peppers, squash, strawberries, egg- plants, cucumbers, carrots, radish, tur- § 180.1095 Chlorine gas; exemptions nips, onions, peas, melons, grapes, wal- from the requirement of a toler- nuts, almond, orange, grapefruit, mul- ance. berry, peach, apple, apricot, black- Chlorine gas is exempted from the re- berry, loganberry, pecan, cherry, plum, quirement of a tolerance when used and cranberry. preharvest or postharvest in solution [53 FR 5379, Feb. 24, 1988] on all raw agricultural commodities.

§ 180.1089 Poly-N-acetyl-D-glu- [56 FR 21309, May 8, 1991] cosamine; exemption from the re- quirement of tolerance. § 180.1097 GBM-ROPE; exemption from the requirement of a tolerance. An exemption from the requirement of a tolerance is established for resi- The grape berry moth pheromone dues of the biochemical nematicide (GBM-ROPE) containing the active in- poly-N-acetyl-D-glucosamine on a vari- gredients (Z)-9-dedecenyl acetate and ety of agricultural crops. (Z)-11-tetradecenyl acetate is exempt from the requirement of a tolerance in [53 FR 10249, Mar. 30, 1988] or on the raw agricultural commodity grapes when used in orchards with en- § 180.1090 Lactic acid; exemption from the requirement of a tolerance. capsulated polyethylene tubing to con- trol grape berry moth. Lactic acid (2-hydroxypropanoic acid) is exempted from the requirement [55 FR 28622, July 12, 1990] of a tolerance when used as a plant growth regulator in or on all raw agri- § 180.1098 Gibberellins [Gibberellic cultural commodities. Acids (GA3 and GA4 + GA7), and So- dium or Potassium Gibberellate]; [53 FR 15286, May 4, 1988] exemption from the requirement of a tolerance. § 180.1091 Aluminum isopropoxide and aluminum secondary butoxide; ex- An exemption from the requirement emption from the requirement of a of a tolerance is established for resi- tolerance. dues of gibberellins [gibberellic acids Aluminum isopropoxide (CAS Reg. (GA3 and GA4 + GA7), and sodium or No. 555–31–7) and aluminum secondary potassium gibberellate] in or on all butoxide (CAS Reg. No. 2269–22–9) are food commodities when used as plant exempted from the requirement of a regulators on plants, seeds, or cuttings tolerance when used in accordance and on all food commodities after har- with good agricultural practices as sta- vest in accordance with good agricul- bilizers in formulations of the insecti- tural practices. cide amitraz [N′-(2,4-dimethylphenyl)- [64 FR 31505, June 11, 1999] N-[[(2,4-dimethylphenyl)imino]-N-

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§ 180.1100 Gliocladium virens isolate § 180.1103 Isomate-C; exemption from GL-21; exemption from the require- the requirement of a tolerance. ment of a tolerance. The pheromone An exemption from the requirement (Isomate-C) E,E-8,10-dodecenyl alcohol, of a tolerance is established for resi- dodecanol, tetradecanol is exempt from dues of the biofungicide Gliocladium the requirements of a tolerance in or virens GL-21 in or on all raw agricul- on all RAC’s when formulated in poly- tural commodities when used either as ethylene pheromone dispensers for use a fungicide for inoculation of plant in orchards with encapsulated poly- growth media in greenhouses or on ter- ethylene tubing to control codling restrial food crops grown outdoors in moth. accordance with good agricultural practices. [56 FR 23523, May 22, 1991] [60 FR 48659, Sept. 20, 1995; 60 FR 52248, Oct. § 180.1107 Delta endotoxin of Bacillus 5, 1995] thuringiensis variety kurstaki en- capsulated into killed Pseudomonas § 180.1101 Parasitic (parasitoid) and fluorescens; exemption from the re- predatory insects; exemption from quirement of a tolerance. the requirement of a tolerance. The delta endotoxin of Bacillus Parasitic (parasitoid) and predatory thuringiensis variety kurstaki encap- insects are exempted from the require- sulated into killed Pseudomonas ment of a tolerance for residues when fluorescens is exempt from the require- they are used in accordance with good ments of a tolerance in or on all raw agricultural and practices agricultural commodities. to control insect pests of stored raw whole grains such as corn, small [56 FR 28328, June 20, 1991] grains, rice, soybeans, peanuts, and other legumes either bulk or § 180.1108 Delta endotoxin of Bacillus warehoused in bags. For the purposes thuringiensis variety San Diego en- capsulated into killed Pseudomonas of this rule, the parasites (parasitoids) fluorescens; exemption from the re- and predators are considered to be spe- quirement of a tolerance. cies of Hymenoptera in the genera Trichogramma, Trichogrammatidae; The delta endotoxin of Bacillus Bracon, Braconidae; Venturia, thuringiensis variety San Diego encap- Mesostenus, Ichneumonidae; sulated into killed Pseudomonas Anisopteromalus, Choetospila, fluorescens is exempt from the require- Lariophagus, Dibrachys, Habrocytus, ments of a tolerance in or on all raw Pteromalus, Pteromalidae; agricultural commodities. Cephalonomia, Holepyris, Laelius, [56 FR 28326, June 20, 1991] Bethylidae; and of Hemiptera in the genera Xylocoris, Lyctocoris, and § 180.1110 3-Carbamyl-2,4,5-trichloro- Dufouriellus, Anthocoridae. Whole in- benzoic acid; exemption from the sects, fragments, parts, and other resi- requirement of a tolerance. dues of these parasites and predators An exemption from the requirement remain subject to 21 U.S.C. 342(a)(3). of a tolerance is established for the res- [57 FR 14646, Apr. 22, 1992] idues of 3-carbamyl-2,4,5- trichlorobenzoic acid in or on all raw § 180.1102 Trichoderma harzianum agricultural commodities which occur KRL-AG2 (ATCC #20847) strain T– from the direct application of 22; exemption from requirement of chlorothalonil to crops in § 180.275 (a) a tolerance. and (b) and/or as an inadvertent residue An exemption from the requirement resulting from the soil metabolism of of a tolerance is established for resi- chlorothalonil when applied to crops in dues of the biofungicide Trichoderma § 180.275 (a) and (b), and subsequent up- harzianum KRL-AG2 (ATCC #20847); take by rotated crops when used ac- also known as strain T-22 when applied cording to approved agricultural prac- in/or on all food commodities. tices. [64 FR 16860, Apr. 7, 1999] [57 FR 24552, June 10, 1992]

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§ 180.1111 Bacillus subtilis GB03; ex- lated from the berries of the Neem tree emption from the requirement of a (Azadirachta indica), when used as a tolerance. pesticide at 20 grams or less per acre on The biofungicide Bacillus subtilis GB03 all raw agricultural commodities. is exempted from the requirement of a [58 FR 8696, Feb. 17, 1993] tolerance in or on all raw agricultural commodities when applied as a seed § 180.1120 Streptomyces sp. strain K61; treatment for growing agricultural exemption from the requirement of crops in accordance with good agricul- a tolerance. tural practices. The biological pesticide Streptomyces [57 FR 29033, June 30, 1992] sp. strain K61 is exempted from the re- quirement of a tolerance in or on all § 180.1113 Lagenidium giganteum; ex- raw agricultural commodities when emption from the requirement of a used as a fungicide for the treatment of tolerance. seeds, cuttings, transplants, and plants Lagenidium giganteum (a fungal orga- of agricultural crops in accordance nism) is exempt from the requirement with good agricultural practices. of a tolerance in or on the raw agricul- [58 FR 21403, Apr. 21, 1993] tural commodities grasses, forage and hay; rice, grain and straw; soybeans; § 180.1121 Boric acid and its salts, soybean, forage and hay; and wild rice. borax (sodium borate decahydrate), disodium octaborate tetrahydrate, [57 FR 53570, Nov. 12, 1992] boric oxide (boric anhydride), so- dium borate and sodium metabo- § 180.1114 Pseudomonas fluorescens rate; exemptions from the require- A506, Pseudomonas fluorescens ment of a tolerance. 1629RS, and Pseudomonas syringae 742RS; exemptions from the re- An exemption from the requirement quirement of a tolerance. of a tolerance is established for resi- dues of the pesticidal chemical boric The biological pesticides acid and its salts, borax (sodium borate Pseudomonas fluorescens A506, decahydrate), disodium octaborate tet- Pseudomonas fluorescens 1629RS, and rahydrate, boric oxide (boric anhy- Pseudomonas syringae 742RS are ex- dride), sodium borate and sodium met- empted from the requirement of a tol- aborate, in or on raw agricultural com- erance in or on all raw agricultural modities when used as an active ingre- commodities when applied as a frost dient in insecticides, herbicides, or fun- protection agent or biological control gicides preharvest or postharvest in ac- agent to growing agricultural crops in cordance with good agricultural prac- accordance with good agricultural tices. practices. [58 FR 44283, Aug. 20, 1993] [57 FR 42700, Sept. 16, 1992] § 180.1122 Inert ingredients of § 180.1118 Spodoptera exigua nuclear semiochemical dispensers; exemp- polyhedrosis virus; exemption from tions from the requirement of a tol- the requirement of a tolerance. erance. An exemption from the requirement (a) All inert ingredients of of a tolerance is established for the mi- semiochemical dispenser products for- crobial pest control agent Spodoptera mulated with, and/or contained in, dis- exigua nuclear polyhedrosis virus when pensers made of polymeric matrix ma- used as a pesticide control agent on all terials (including the monomers, plas- raw agricultural commodities. ticizers, dispersing agents, anti- [58 FR 25784, Apr. 28, 1993] oxidants, UV protectants, stabilizers, and other inert ingredients) are ex- § 180.1119 Azadirachtin; exemption empted from the requirement of a tol- from the requirement of a toler- erance when used as carriers in pes- ance. ticide formulations for application to An exemption from the requirement growing crops only. These dispensers of a tolerance is established for the bio- shall conform to the following speci- chemical azadirachtin, which is iso- fications:

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(1) Exposure must be limited to inad- (1) Commodity exposure must be lim- vertent physical contact only. The de- ited to inadvertent physical contact. sign of the dispenser must be such as to The design of the dispenser must be preclude any contamination by its such as to preclude any exposure of its components of the raw agricultural components to the raw agricultural commodity (RAC) or processed foods/ commodity (RAC) or processed foods/ feeds derived from the commodity by feeds derived from the commodity due virtue of its proximity to the RAC or to its proximity to the RAC or as a re- as a result of its physical size. sult of its physical size. Dispensers (2) The dispensers must be applied must be of such size and construction discretely. This exemption does not that they are readily recognized post- apply to components of semiochemical application. formulations applied in a broadcast (2) The dispensers must be applied manner either to a crop field plot or to discretely, i.e., placed in the field in individual plants. easily perceived distinct locations in a (b) A semiochemical dispenser is a manner that does not prevent later re- single enclosed or semi-enclosed unit trieval. This exemption does not apply that releases semiochemical(s) into the to codlure applied in a broadcast man- surrounding atmosphere via volatiliza- ner either to a crop field plot or to in- tion and is applied in a manner to pro- dividual plants. vide discrete application of the (b) A codlure dispenser is a single en- semiochemical(s) into the environ- closed or semi-enclosed unit that re- ment. leases codlure into the surrounding at- (c) Semiochemicals are chemicals mosphere via volatilization and is ap- that are emitted by plants or animals plied in a manner to provide discrete and modify the behavior of receiving application (i.e., in easily perceived dis- organisms. These chemicals must be tinct locations in a manner that does naturally occurring or substantially not prevent later retrieval) of the identical to naturally occurring codlure into the environment. semiochemicals. [59 FR 9931, Mar. 2, 1994] [58 FR 64494, Dec. 8, 1993] § 180.1127 Biochemical pesticide plant § 180.1124 Arthropod pheromones; ex- floral volatile attractant com- emption from the requirement of a pounds: cinnamaldehyde, cinnamyl tolerance. alcohol, 4-methoxy cinnamaldehyde, 3-phenyl propanol, 4-methoxy Arthropod pheromones, as described phenethyl alcohol, indole, and 1,2,4- in § 152.25(b) of this chapter, when used trimethoxybenzene; exemptions in retrievably sized polymeric matrix from the requirement of a toler- dispensers are exempt from the re- ance. quirement of a tolerance in or on all Residues of the biochemical pesticide raw agricultural commodities when ap- plant floral volatile attractant com- plied to growing crops only at a rate pounds: cinnamaldehyde, cinnamyl al- not to exceed 150 grams active ingre- cohol, 4-methoxy cinnamaldehyde, 3- dient/acre/year in accordance with good phenyl propanol, 4-methoxy phenethyl agricultural practices. alcohol, indole, and 1,2,4- [59 FR 14759, Mar. 30, 1994] trimethoxybenzene are exempt from the requirement of a tolerance in or on § 180.1126 Codlure, (E,E)-8,10- the following raw agricultural com- Dodecadien-1-ol; exemption from modities: the following field crops—al- the requirement of a tolerance. falfa, clover, cotton, dandelion, pea- An exemption from the requirement nuts (including hay), rice, sorghum of a tolerance is established for the in- (milo), soybeans, sunflower, sweet po- sect pheromone codlure, (E,E)-8,10- tatoes, and wheat; the following vege- dodecadien-1-ol, on all raw agricultural table crops—asparagus, beans (includ- commodities in accordance with the ing forage hay), beets, carrots, celery, following prescribed conditions: cole crops (cabbage, broccoli, brussels (a) Application shall be limited sole- sprouts, cauliflower), collards (kale, ly to codlure dispensers that conform mustard greens, turnip greens, kohl- to the following specifications: rabi), corn, fresh (field, sweet, pop,

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seed), corn fodder and forage, chinese the requirement of a tolerance in or on cabbage, cowpeas, cucurbitis (cucum- all raw agricultural commodities when bers, squash, pumpkin), egg plant, en- used as a fungicide on agricultural dive (escarole), horseradish (radish, ru- crops in accordance with good agricul- tabagas, turnip roots), leafy greens tural practices. (spinach, swiss chard), lettuce (head leaf), okra, parsley, parsnip, peas, peas [59 FR 33437, June 29, 1994] with pods, peppers, potatoes, sugar § 180.1134 Neomycin phosphotransfer- beets, tomatoes; the following tree ase II and genetic material nec- fruit, berry and nut crops—almonds, essary for its production; exemp- apples, apricots, berries (blackberry, tion from the requirement of a tol- boysenberry, dewberry, loganberry, erance. raspberry), blueberry, cherry, citrus The neomycin phosphotransferase II (grapefruit, kumquat, lemon, lime, or- ange, tangelo, and tangerine) cran- (NPTII) and the genetic material nec- berry, grapes, melons, (watermelon, essary for the production of this pro- honeydew, crenshaw, cantaloupe, ca- tein are exempted from the require- saba, persian), nectarines, pears, pe- ment of a tolerance in or on all raw ag- cans, peaches, and strawberry as dis- ricultural commodities when used as a persed from the end-use product Corn plant-pesticide inert ingredient.  Rootworm Bait , a pesticidal bait, in [59 FR 49353, Sept. 28, 1994] accordance with the prescribed condi- tions in paragraph (a) of this section. EFFECTIVE DATE NOTE: At 72 FR 20434, (a) Cumulative yearly application 20435, Apr. 25, 2007, § 180.1134 was redesignated as § 174.521 and revised, effective July 24, 2007. cannot exceed 20 grams of each floral For the convenience of the user, the revised attractant/acre/application. text is set forth as follows: (b) [Reserved] § 174.521 Neomycin phosphotransferase II; [59 FR 15857, Apr. 5, 1994] exemption from the requirement of a tol- erance. § 180.1128 Bacillus subtilis MBI 600; Residues of the neomycin exemption from the requirement of phosphotransferase II (NPTII) enzyme are a tolerance. exempted from the requirement of a toler- The biofungicide Bacillus subtilis MBI ance in all food commodities when used as a 600 is exempted from the requirement plant-incorporated protectant inert ingre- of a tolerance in or on all raw agricul- dient. tural commodities when applied as a seed treatment on seeds used for grow- § 180.1135 Pasteuria penetrans; exemp- ing agricultural crops in accordance tion from the requirement of a tol- erance. with good agricultural practices. The biological nematicide Pasteuria [59 FR 29544, June 8, 1994] penetrans is exempted from the require- § 180.1130 N-(n-octyl)-2-pyrrolidone ment of a tolerance in or on all raw ag- and N-(n-dodecyl)-2-pyrrolidone; ex- ricultural commodities, except roots emptions from the requirement of a and tubers, when used as a nematicide tolerance. in the production of fruits and vegeta- N-(n-octyl)-2-pyrrolidone and N-(n- bles in greenhouses. dodecyl)-2-pyrrolidone are exempt from [59 FR 66741, Dec. 28, 1994] the requirement of a tolerance when used as solvents in cotton defoliant for- § 180.1139 Sodium 5-nitroguaiacolate; mulations containing thidiazuron and exemption from the requirement of diuron as active ingredients. a tolerance. [59 FR 32084, June 22, 1994] The biochemical sodium 5- nitroguiacolate is exempted from the § 180.1131 Ampelomyces quisqualis iso- requirement of a tolerance when used late M10; exemption from the re- as a plant growth regulator in end-use quirement of a tolerance. products at a concentration of 0.1% by The biological fungicide Ampelomyces weight and applied at an application quisqualis isolate M10 is exempted from rate of 20 g of a.i. per acre or less per

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application, in or on all food commod- § 180.1144 Candida oleophila isolate I- ities. 182; exemption from the require- ment of a tolerance. [65 FR 66181, Nov. 3, 2000] Candida oleophila isolate I-182, when § 180.1140 Sodium o-nitrophenolate; used as a post-harvest biological fun- exemption from the requirement of gicide, is exempted from the require- a tolerance. ment of a tolerance in or on all raw ag- ricultural commodities. The biochemical sodium o- nitrophenolate is exempted from the [60 FR 11033, Mar. 1, 1995] requirement of a tolerance when used § 180.1145 Pseudomonas syringae; ex- as a plant growth regulator in end-use emption from the requirement of a products at a concentration of 0.2% by tolerance. weight and applied at an application Pseudomonas syringae is exempted rate of 20 g of a.i. per acre or less per from the requirement of a tolerance on application, in or on all food commod- all raw agricultural commodities when ities. applied postharvest according to good [65 FR 66181, Nov. 3, 2000] agricultural practices. [60 FR 12703, Mar. 8, 1995] § 180.1141 Sodium p-nitrophenolate; exemption from the requirement of § 180.1146 Beauveria bassiana Strain a tolerance. GHA; exemption from the require- ment of a tolerance. The biochemical sodium p- nitrophenolate is exempted from the Beauveria bassiana Strain GHA is ex- requirement of a tolerance when used empted from the requirement of a tol- as a plant growth regulator in end-use erance in or on all raw agricultural product at a concentration of 0.3% by commodities when applied to growing crops according to good agricultural weight and applied at an application practices. rate of 20 g of a.i. per acre or less per application, in or on all food commod- [60 FR 18547, Apr. 12, 1995] ities. § 180.1147 Bacillus thuringiensis [65 FR 66181, Nov. 3, 2000] CryIIIA delta-endotoxin and the ge- netic material necessary for its pro- § 180.1142 1,4-Dimethylnaphthalene; duction. exemption from the requirement of Bacillus thuringiensis CryIIIA delta- a tolerance. endotoxin and the genetic material An exemption from the requirement necessary for its production are ex- of a tolerance is established for resi- empted from the requirement of a tol- dues of the plant growth regulator 1,4- erance when used as a plant pesticide dimethylnaphthalene when applied in potatoes. ‘‘Genetic material nec- post harvest to potatoes in accordance essary for its production’’ means the with good agricultural practices. CryIIIA gene and its regulatory re- gions. ‘‘Regulatory regions’’ are the ge- [60 FR 7457, Feb. 8, 1995] netic materials that control the ex- pression of the gene, such as pro- § 180.1143 Methyl anthranilate; exemp- moters, terminators, and enhancers. tion from the requirement of a tol- erance. [60 FR 21728, May 3, 1995] Residues of methyl anthranilate, a EFFECTIVE DATE NOTE: At 72 FR 20434, 20435, Apr. 25, 2007, § 180.1147 was redesignated biochemical pesticide, are exempt from as § 174.509 and revised, effective July 24, 2007. the requirement of a tolerance in or on For the convenience of the user, the revised all food commodities, when used in ac- text is set forth as follows: cordance with good agricultural prac- § 174.509 Bacillus thuringiensis Cry3A pro- tices. tein; exemption from the requirement of a tolerance. [67 FR 51088, Aug. 7, 2002] Residues of Bacillus thuringiensis Cry3A protein are exempted from the requirement

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of a tolerance when used as a plant-incor- gions. ‘‘Regulatory regions’’ are the ge- porated protectant in potatoes. netic material that control the expres- sion of the genetic material encoding § 180.1148 Occlusion Bodies of the Granulosis Virus of Cydia the PAT protein, such as promoters, pomenella; tolerance exemption. terminators, and enhancers. An exemption from the requirement [62 FR 17719, Apr. 11, 1997] of a tolerance is established for resi- EFFECTIVE DATE NOTE: At 72 FR 20434, dues of the microbial pest control 20435, Apr. 25, 2007, § 180.1151 was redesignated agent Occlusion Bodies of the as § 174.522 and revised, effective July 24, 2007. Granulosis Virus of Cydia pomonella For the convenience of the user, the revised (codling moth) in or on all raw agricul- text is set forth as follows: tural commodities. § 174.522 Phosphinothricin [60 FR 42450, Aug. 16, 1995] Acetyltransferase (PAT); exemption from the requirement of a tolerance. § 180.1149 Inclusion bodies of the Residues of the Phosphinothricin multi-nuclear polyhedrosis virus of Acetyltransferase (PAT) enzyme are exempt Anagrapha falcifera; exemption from the requirement of a tolerance when from the requirement of a toler- used as plant-incorporated protectant inert ance. ingredients in all food commodities. The microbial pest control agent in- clusion bodies of the multi-nuclear § 180.1153 Lepidopteran pheromones; polyhedrosis virus of Anagrapha exemption from the requirement of falcifera is exempted from the require- a tolerance. ment of a tolerance in or on all raw ag- Lepidopteran pheromones that are ricultural commodities when used to naturally occurring compounds, or control certain lepidopteran pest spe- identical or substantially similar syn- cies. thetic compounds, designated by an [60 FR 37020, July 19, 1995] unbranched aliphatic chain (between 9 and 18 carbons) ending in an alcohol, § 180.1150 6-Benzyladenine; exemption aldehyde or acetate functional group from the requirement of a toler- and containing up to 3 double bonds in ance. the aliphatic backbone, are exempt The biochemical plant regulator 6- from the requirement of a tolerance in benzyladenine (6–BA) is exempt from or on all raw agricultural commodities. the requirement of a tolerance in or on This exemption only pertains to those apple and pear when applied at a rate situations when the pheromone is: Ap- of ≤182 grams of active ingredient per plied to growing crops at a rate not to acre per season, and in or on pistachio exceed 150 grams active ingredient/ when applied at a rate of ≤60 grams of acre/year in accordance with good agri- active ingredient per acre per season. cultural practices; and applied as a post-harvest treatment to stored food [72 FR 13179, Mar. 21, 2007] commodities at a rate not to exceed 3.5 2 § 180.1151 Phosphinothricin Acetyl- grams active ingredient/1,000 ft /year transferase (PAT) and the genetic (equivalent to 150 grams active ingre- material necessary for its produc- dient/acre/year) in accordance with tion all plants; exemption from the good agricultural practices. requirement of a tolerance. [71 FR 45399, Aug. 9, 2006] Phosphinothricin Acetyltransferase (PAT) and the genetic material nec- § 180.1154 CryIA(c) and CryIC derived essary for its production in all plants delta-endotoxins of Bacillus are exempt from the requirement of a thuringiensis var. kurstaki encap- tolerance when used as plant-pesticide sulated in killed Pseudomonas inert ingredients in all plant raw agri- fluorescens, and the expression cultural commodities. ‘‘Genetic mate- plasmid and cloning vector genetic rial necessary for its production’’ constructs. means the genetic material which com- CryIA(c) and CryIC derived delta- prise genetic material encoding the endotoxins of Bacillus thuringiensis var. PAT protein and its regulatory re- kurstaki encapsulated in killed

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Pseudomonas fluorescens and the expres- § 180.1157 Cytokinins; exemption from sion plasmid and cloning vector ge- the requirement of a tolerance. netic constructs are exempt from the An exemption from the requirement requirement of a tolerance when used of a tolerance is established for resi- in or on all raw agricultural commod- dues of cytokinins (specifically: aque- ities. ous extract of seaweed meal and [60 FR 47489, Sept. 13, 1995] kinetin) in or on all food commodities when used as plant regulators on § 180.1155 Bacillus thuringiensis sub- plants, seeds, or cuttings and on all species Kurstaki CryIA(c) and the food commodities after harvest in ac- genetic material necessary for its cordance with good agricultural prac- production in all plants; exemption tices. from the requirement of a toler- ance. [64 FR 31505, June 11, 1999] Bacillus thuringiensis subspecies § 180.1158 Auxins; exemption from the kurstaki CryIA(c) delta-endotoxin and requirement of a tolerance. the genetic material necessary for its An exemption from the requirement production in all plants are exempt of a tolerance is established for resi- from the requirement of a tolerance dues of auxins (specifically: indole-3- when used as plant-pesticides in all acetic acid and indole-3-butyric acid) plant raw agricultural commodities. in or on all food commodities when ‘‘Genetic material necessary for its used as plant regulators on plants, production’’ means the genetic mate- seeds, or cuttings and on all food com- rial which comprise genetic material modities after harvest in accordance encoding the CryIA(c) delta-endotoxin with good agricultural practices. and its regulatory regions. ‘‘Regu- latory regions’’ are the genetic mate- [64 FR 31505, June 11, 1999] rial that control the expression of the genetic material encoding the CryIA(c) § 180.1159 Pelargonic acid; exemption delta-endotoxin, such as promoters, from the requirement of tolerances. terminators, and enhancers. (a) An exemption from the require- ment of a tolerance is established for [62 FR 17722, Apr. 11, 1997] residues of pelargonic acid in or on all EFFECTIVE DATE NOTE: At 72 FR 20434, food commodities when used as a plant 20435, Apr. 25, 2007, § 180.1155 was redesignated regulator on plants, seeds, or cuttings as § 174.510 and revised, effective July 24, 2007. and on all food commodities after har- For the convenience of the user, the revised vest in accordance with good agricul- text is set forth as follows: tural practices. § 174.510 Bacillus thuringiensis Cry1Ac pro- (b) Pelargonic acid when used as an tein in all plants; exemption from the re- herbicide is exempt from the require- quirement of a tolerance. ment of a tolerance on all plant food Residues of Bacillus thuringiensis Cry1Ac commodities provided that: protein in all plants are exempt from the re- (1) Applications are not made di- quirement of a tolerance when used as plant- rectly to the food commodity except incorporated protectants in all food com- when used as a harvest aid or desiccant modities. to: any root and tuber vegetable, bulb vegetable or cotton. § 180.1156 Cinnamaldehyde; exemption from the requirement of a toler- (2) When pelargonic acid is used as a ance. harvest aid or desiccant, applications must be made no later than 24 hours Cinnamaldehyde (3-phenyl-2- prior to harvest. propenal) is exempted from the re- (c) An exemption from the require- quirement of a tolerance in or on all ment of a tolerance is established for food commodities, when used as a fun- residues of pelargonic acid in or on all gicide, insecticide, and algaecide in ac- raw agricultural commodities and in cordance with good agricultual prac- processed commodities, when such resi- tices. dues result from the use of pelargonic [64 FR 7804, Feb. 17, 1999; 64 FR 14099, Mar. 24, acid as an antimicrobial treatment in 1999] solutions containing a diluted end-use

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concentration of pelargonic acid up to microns and insoluble in water. This 170 ppm per application on food contact exemption pertains to the acrylate surfaces such as equipment, pipelines, polymers/copolymers used as inert in- tanks, vats, fillers, evaporators, gredients for sprayable and dispenser pasteurizers and aseptic equipment in pesticide formulations that are applied restaurants, food service operations, on food crops. Any acrylate polymers/ dairies, breweries, wineries, beverage copolymers used for encapsulating ma- and food processing plants. terial must be cleared as an inert in- [62 FR 28364, May 23, 1997, as amended at 64 gredient when used in pesticide formu- FR 31505, June 11, 1999; 68 FR 7935, Feb. 19, lation applied on food crops. 2003] (b) For the purposes of this exemp- § 180.1160 Jojoba oil; exemption from tion, acrylate polymers/copolymers the requirement of a tolerance. used as inert ingredients in an end-use formulation must meet the definition The insecticide and spray tank adju- for a polymer as given in 40 CFR vant jojoba oil is exempted from the requirement of a tolerance in or on all 723.250(b), are not automatically ex- raw agricultural commodities when ap- cluded by 40 723.250(d), and meet the plied at the rate of 1.0% or less of the tolerance exemption criteria in 40 CFR final spray in accordance with good ag- 723.250(e)(1), 40 CFR 723.250 (e)(2) or 40 ricultural practices, provided the CFR 723.250(e)(3). Therefore, acrylate jojoba oil does not contain polymers and copolymers that are al- simmondsin, simmondsin-2-ferulate, ready listed in the TSCA inventory or and related conjugated organonitriles will meet the polymer tolerance ex- including demethyl simmondsin and emption under 40 CFR 723.250 as didemethylsimmondsin. amended on March 29, 1995 are covered by this exemption. [61 FR 2121, Jan. 25, 1996] [61 FR 6551, Feb. 21, 1996] § 180.1161 Clarified hydrophobic ex- tract of neem oil; exemption from § 180.1163 Killed Myrothecium the requirement of a tolerance. verrucaria; exemption from the re- Clarified hydrophobic extract of quirement of a tolerance. neem oil is exempt from the require- Killed Myrothecium verrucaria is ex- ment of a tolerance on all food com- empted from the requirement of a tol- modities when used as a botanical fun- erance in or on all raw agricultural gicide/insecticide/miticide. commodities when applied as a pre- [67 FR 43552, June 28, 2002] seed or pre- or post-planting soil treat- ment alone or mixed with water and § 180.1162 Acrylate polymers and co- the mixed suspension be applied polymers; exemption from the re- quirement of a tolerance. through drip or border irrigation sys- tems and the indicator mycotoxin lev- (a) Acrylate polymers and copoly- els do not exceed 15 ppm. mers are exempt from the requirement of a tolerance when used as inert ingre- [61 FR 11315, Mar. 20, 1996, as amended at 61 dients in pesticidal formulations ap- FR 58332, Nov. 14, 1996] plied to growing, raw agricultural com- modities. This tolerance exemption § 180.1165 Capsaicin; exemption from covers the acrylate polymers/copoly- the requirement of a tolerance. mers that are intrinsically safe and al- Capsaicin is exempt from the require- ready listed in TSCA inventory or will ment of a tolerance in or on all food meet the polymer tolerance exemption commodities when used in accordance from requirements of with approved label rates and good ag- premanufacturing notification under 40 ricultural practice. CFR 723.250. Polymers exempted can be used as dispensers, resins, fibers, and [63 FR 39521, July 23, 1998] beads, as long as the fibers, beads and resins particle sizes are greater than 10

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§ 180.1167 Allyl isothiocyanate as a netic material necessary for its produc- component of food grade oil of mus- tion’’ means the genetic material tard; exemption from the require- which comprise genetic material en- ment of a tolerance. coding the CP4 EPSPS and its regu- The insecticide and repellent Allyl latory regions. ‘‘Regulatory regions’’ isothiocyanate is exempt from the re- are the genetic material that control quirement of a tolerance for residues the expression of the genetic material when used as a component of food encoding the CP4 EPSPS, such as pro- grade oil of mustard, in or on all raw moters, terminators, and enhancers. agricultural commodities, when ap- plied according to approved labeling. [61 FR 40340, Aug. 2, 1996] [61 FR 24894, May 17, 1996] EFFECTIVE DATE NOTE: At 72 FR 20434, 20435, Apr. 25, 2007, § 180.1174 was redesignated § 180.1173 Bacillus thuringiensis as § 174.523 and revised, effective July 24, 2007. CryIA(b) delta-endotoxin and the For the convenience of the user, the revised genetic material necessary for its text is set forth as follows: production in all plants. § 174.523 CP4 Enolpyruvylshikimate-3-phos- Bacillus thuringiensis CryIA(b) delta- phate (CP4 EPSPS) synthase in all plants; endotoxin and the genetic material exemption from the requirement of a tol- necessary for its production in all erance. plants are exempt from the require- Residues of the CP4 ment of a tolerance when used as plant Enolpyruvylshikimate-3-phosphate (CP4 pesticides in all plant raw agricultural EPSPS) synthase enzyme in all plants are exempt from the requirement of a tolerance commodities. ‘‘Genetic material nec- when used as plant-incorporated protectant essary for its production’’ means the inert ingredients in all food commodities. genetic material which comprise ge- netic material encoding the CryIA(b) § 180.1176 Sodium bicarbonate; exemp- delta-endotoxin and its regulatory re- tion from the requirement of a tol- gions. ‘‘Regulatory regions’’ are the ge- erance. netic material that control the expres- The biochemical pesticide sodium bi- sion of the genetic material encoding carbonate is exempted from the re- the CryIA(b) delta-endotoxin, such as quirement of a tolerance in or on all promoters, terminators, and enhancers. raw agricultural commodities when ap- [61 FR 40343, Aug. 2, 1996] plied as a fungicide or post-harvest fun- EFFECTIVE DATE NOTE: At 72 FR 20434, gicide in accordance with good agricul- 20435, Apr. 25, 2007, § 180.1173 was redesignated tural practices. as § 174.511 and revised, effective July 24, 2007. [61 FR 67473, Dec. 23, 1996] For the convenience of the user, the revised text is set forth as follows: § 180.1177 Potassium bicarbonate; ex- § 174.511 Bacillus thuringiensis Cry1Ab pro- emption from the requirement of a tein in all plants; exemption from the re- tolerance. quirement of a tolerance. The biochemical pesticide potassium Residues of Bacillus thuringiensis Cry1Ab protein in all plants are exempt from the re- bicarbonate is exempted from the re- quirement of a tolerance when used as plant- quirement of a tolerance in or on all incorporated protectants in all food com- raw agricultural commodities when ap- modities. plied as a fungicide or post-harvest fun- gicide in accordance with good agricul- § 180.1174 CP4 Enolpyruvylshikimate- tural practices. 3-phosphate (CP4 EPSPS) and the genetic material necessary for its [61 FR 67473, Dec. 23, 1996] production in all plants. CP4 Enolpyruvylshikimate-3-phos- § 180.1178 Formic acid; exemption phate (CP4 EPSPS) and the genetic from the requirement of a toler- material necessary for its production ance. in all plants are exempt from the re- The pesticide formic acid is exempted quirement of a tolerance when used as from the requirement of a tolerance in plant pesticide inert ingredients in all or on honey and beeswax when used to raw agricultural commodities. ‘‘Ge- control tracheal mites and suppress

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varroa mites in bee colonies, and ap- aid in the control of insects, fungi, and plied in accordance with label use di- bacteria (food/feed use). rections. [62 FR 19685, Apr. 23, 1997, as amended at 63 [64 FR 8529, Feb. 22, 1999] FR 9430, Feb. 25, 1998]

§ 180.1179 Plant extract derived from § 180.1181 Bacillus cereus strain BPO1; Opuntia lindheimeri, Quercus exemption from the requirement of falcata, Rhus aromatica, and a tolerance. Rhizophoria mangle; exemption An exemption from the requirement from the requirement of a toler- of a tolerance for residues of the Bacil- ance. lus cereus strain BPO1 in or on all raw The biochemical pesticide plant ex- agricultural commodities when ap- tract derived from Opuntia lindheimeri, plied/used in accordance with label di- Quercus falcata, Rhus aromatica, and rections. Rhizophoria mangle is exempted from the requirement of a tolerance in or on [67 FR 70017, Nov. 20, 2002] all raw agricultural commodities when § 180.1182 Coat Protein of Potato Virus applied as a nematicide/plant regulator Y and the genetic material nec- in accordance with good agricultural essary for its production; exemp- practices. tion from the requirement of a tol- erance. [62 FR 24842, May 7, 1997] An exemption fron the requirement § 180.1180 Kaolin; exemption from the of a tolerance is established for resi- requirement of a tolerance. dues of the biological plant pesticide (a) The biochemical pesticide kaolin Coat Protein of Potato Virus Y and the is temporarily exempted from the re- genetic material necessary for its pro- quirement of a tolerance for residues of duction in or on all food commodities. the insecticide Kaolin, when used on [62 FR 43657, Aug. 15, 1997] crops (apples, apricots, bananas, beans, EFFECTIVE DATE NOTE: At 72 FR 20434, cane berries, citrus fruits, corn, cotton, 20435, Apr. 25, 2007, § 180.1182 was redesignated cranberries, cucurbits, grapes, melons, as § 174.512 and revised, effective July 24, 2007. nuts, ornamentals, peaches, peanuts, For the convenience of the user, the revised pears, peppers, plums, potatoes, seed text is set forth as follows: crops, small grains, soybeans, straw- § 174.512 Coat Protein of Potato Virus Y; ex- berries, sugar beets, and tomatoes) to emption from the requirement of a toler- control certain insect, fungus, and bac- ance. terial damage to plants. This tem- Residues of Coat Protein of Potato Virus Y porary exemption from the require- are exempt from the requirement of a toler- ment of a tolerance will permit the ance when used as a plant-incorporated pro- marketing of the food commodities in tectant in or on all food commodities. this paragraph when treated in accord- ance with the provisions of experi- § 180.1183 Potato Leaf Roll Virus Re- mental use permit 70060–EUP–1, which sistance Gene (also known as orf1/ orf2 gene) and the genetic material is being issued under the Federal Insec- necessary for it’s production; Ex- ticide, Fungicide, and Rodenticide Act emption from the requirement of a (FIFRA), as amended (7 U.S.C. 136). tolerance. This temporary exemption from the re- An exemption from the requirement quirement of a tolerance expires and is of a tolerance is established for resi- revoked December 31, 1999. This tem- dues of the biological plant pesticide porary exemption from the require- Potato Leaf Roll Virus Resistance ment of a tolerance may be revoked at Gene (also known as orf1/orf2 gene) and any time if the experimental use per- the genetic material necessary for its mit is revoked or if any experience production. with or scientific data on this pesticide indicate that the tolerance is not safe. [64 FR 13080, Mar. 17, 1999] (b) Kaolin is exempted from the re- EFFECTIVE DATE NOTE: At 72 FR 20434, quirement of a tolerance for residues 20435, Apr. 25, 2007, § 180.1183 was redesignated when used on or in food commodities to as § 174.513 and revised, effective July 24, 2007.

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For the convenience of the user, the revised § 174.515 Coat Protein of Papaya Ringspot text is set forth as follows: Virus; exemption from the requirement of a tolerance. § 174.513 Potato Leaf Roll Virus Resistance Residues of Coat Protein of Papaya Gene (also known as orf1/orf2 gene); ex- emption from the requirement of a toler- Ringspot Virus are exempt from the require- ance. ment of a tolerance when used as a plant-in- An exemption from the requirement of a corporated protectant in or on all food com- tolerance is established for residues of the modities. plant-incorporated protectant Potato Leaf Roll Virus Resistance Gene (also known as § 180.1186 Coat protein of cucumber orf1/orf2 gene) in or on all food commodities. mosaic virus and the genetic mate- rial necessary for its production; § 180.1184 Coat Protein of Watermelon exemption from the requirement of Mosaic Virus-2 and Zucchini Yellow a tolerance. Mosaic Virus and the genetic mate- rial necessary for its production; An exemption from the requirement exemption from the requirement of a tolerance is established for resi- for a tolerance. dues of the biological plant pesticide An exemption from the requirement Coat Protein of Cucumber Mosaic of a tolerance is established for resi- Virus and the genetic material nec- dues of the biological plant pesticide essary for its production in or on all Coat Protein of Watermelon Mosaic food commodities. Virus-2 and Zucchini Yellow Mosaic [62 FR 44579, Aug. 22, 1997] Virus and the genetic material nec- essary for its production in or on all EFFECTIVE DATE NOTE: At 72 FR 20434, food commodities. 20435, Apr. 25, 2007, § 180.1186 was redesignated as § 174.516 and revised, effective July 24, 2007. [62 FR 44582, Aug. 22, 1997] For the convenience of the user, the revised text is set forth as follows: EFFECTIVE DATE NOTE: At 72 FR 20434, 20435, Apr. 25, 2007, § 180.1184 was redesignated § 174.516 Coat protein of cucumber mosaic as § 174.514 and revised, effective July 24, 2007. virus; exemption from the requirement of For the convenience of the user, the revised a tolerance. text is set forth as follows: Residues of Coat Protein of Cucumber Mo- § 174.514 Coat Protein of Watermelon Mo- saic Virus are exempt from the requirement saic Virus-2 and Zucchini Yellow Mosaic of a tolerance when used as a plant-incor- Virus; exemption from the requirement porated protectant in or on all food commod- for a tolerance. ities. Residues of Coat Protein of Watermelon Mosaic Virus-2 and Zucchini Yellow Mosaic § 180.1187 L-glutamic acid; exemption Virus are exempt from the requirement of a from the requirement of a toler- tolerance when used as a plant-incorporated ance. protectant in or on all food commodities. L-glutamic acid is exempt from the § 180.1185 Coat Protein of Papaya requirement of a tolerance on all food Ringspot Virus and the genetic ma- commodities when used in accordance terial necessary for its production; with good agricultural practices. exemption from the requirement of a tolerance. [66 FR 33198, June 21, 2001] An exemption from the requirement of a tolerance is established for resi- § 180.1188 Gamma aminobutyric acid; dues of the biological plant pesticide exemption from the requirement of Coat Protein of Papaya Ringspot Virus a tolerance. and the genetic material necessary for Gamma aminobutyric acid is exempt its production in or on all food com- from the requirement of a tolerance on modities. all food commodities when used in ac- [62 FR 44575, Aug. 22, 1997] cordance with good agricultural prac- tices. EFFECTIVE DATE NOTE: At 72 FR 20434, 20435, Apr. 25, 2007, § 180.1185 was redesignated [66 FR 33198, June 21, 2001] as § 174.515 and revised, effective July 24, 2007. For the convenience of the user, the revised text is set forth as follows:

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§ 180.1189 Methyl salicylate; exemption § 180.1192 Bacillus thuringiensis sub- from the requirement of a toler- species tolworthi Cry9C protein and ance. the genetic material necessary for its production in corn; exemption The biochemical pesticide methyl sa- from the requirement of a toler- licylate is exempt from the require- ance. ment of a tolerance for residues in or on food or feed when used as an insect The plant-pesticide Bacillus repellant in food packaging and animal thuringiensis subspecies tolworthi Cry9C and the genetic material necessary for feed packaging at an application rate its production in corn is exempted from that does not exceed 0.2 mg of methyl the requirement of a tolerance for resi- salicylate per square inch of packaging dues, only in corn used for feed; as well materials. as in meat, poultry, milk, or eggs re- [62 FR 61639, Nov. 19, 1997] sulting from animals fed such feed.

§ 180.1190 Glyphosate Oxidoreductase [63 FR 28261, May 22, 1998] [GOX or GOXv247] and the genetic EFFECTIVE DATE NOTE: At 72 FR 20434, material necessary for its produc- 20435, Apr. 25, 2007, § 180.1192 was redesignated tion in all plants; exemption from as § 174.517 and revised, effective July 24, 2007. the requirement of a tolerance. For the convenience of the user, the revised Glyphosate Oxidoreductase [GOX or text is set forth as follows: GOXv247] and the genetic material nec- § 174.517 Bacillus thuringiensis Cry9C pro- essary for its production in all plants tein in corn; exemption from the require- are exempt from the requirement of a ment of a tolerance. tolerance when used as plant-pesticide The plant-incorporated protectant Bacillus inert ingredients in all plant RACs. Ge- thuringiensis Cry9C protein in corn is exempt- ed from the requirement of a tolerance for netic material necessary for its production residues, only in corn used for feed; as well means the genetic material which com- as in meat, poultry, milk, or eggs resulting prise genetic material encoding the from animals fed such feed. GOX proteins and their regulatory re- gions. Regulatory regions are the ge- § 180.1193 Potassium dihydrogen phos- netic material that control the expres- phate; exemption from the require- sion of the genetic material encoding ment of a tolerance. the GOX proteins, such as promoters, Potassium dihydrogen phosphate is terminators, and enhancers. exempted from the requirement of a tolerance in or on all food commodities [62 FR 52509, Oct. 8, 1997] when applied as a fungicide in accord- EFFECTIVE DATE NOTE: At 72 FR 20434, ance with good agricultural practices. 20435, Apr. 25, 2007, § 180.1190 was redesignated as § 174.524 and revised, effective July 24, 2007. [63 FR 43085, Aug. 12, 1998] For the convenience of the user, the revised text is set forth as follows: § 180.1195 Titanium dioxide. Titanium dioxide is exempted from § 174.524 Glyphosate Oxidoreductase GOX the requirement of a tolerance for resi- or GOXv247 in all plants; exemption from the requirement of a tolerance. dues in or on growing crops, when used Residues of the Glyphosate Oxidoreductase as an inert ingredient (UV protectant) GOX or GOXv247 enzyme in all plants are ex- in microencapsulated formulations of empt from the requirement of a tolerance the insecticide lambdacyhalothrin at when used as plant-incorporated protectant no more than 3.0% by weight of the for- inert ingredients in all food commodities. mulation. § 180.1191 Ferric phosphate; exemp- [63 FR 14363, Mar. 25, 1998] tion from the requirement of a tol- erance. § 180.1196 Peroxyacetic acid; exemp- tion from the requirement of a tol- An exemption from the requirement erance. of a tolerance is established for resi- (a) An exemption from the require- dues of the biochemical pesticide, fer- ment of a tolerance is established for ric phosphate (FePO , CAS No. 11045– 4 residues of peroxyacetic acid in or on 86–0) in or on all food commodities. raw agricultural commodities, in proc- [62 FR 56105, Oct. 29, 1997] essed commodities, when such residues

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result from the use of peroxyacetic § 180.1200 Pseudomonas fluorescens acid as an antimicrobial treatment in strain PRA–25; temporary exemp- solutions containing a diluted end use tion from the requirement of a tol- concentration of peroxyacetic acid up erance. to 100 ppm per application on fruits, A temporary exemption from the re- vegetables, tree nuts, cereal grains, quirement of a tolerance is established herbs, and spices. for residues of the microbial pesticide, (b) An exemption from the require- pseudomonas fluorescens strain PRA–25 ment of a tolerance is established for when used on peas, snap beans and residues of peroxyacetic acid, in or on sweet corn and will expire July 31, 2001. all raw and processed food commodities when used in sanitizing solutions con- [63 FR 38498, July 17, 1998] taining a diluted end-use concentration § 180.1201 Trichoderma harzianum of peroxyacetic acid up to 500 ppm, and strain T-39; exemption from the re- applied to tableware, utensils, dishes, quirement of a tolerance. pipelines, tanks, vats, fillers, evapo- Trichoderma harzianum strain T-39 is rators, pasteurizers, aseptic equipment, exempt from the requirement of a tol- milking equipment, and other food erance on all food commodities. processing equipment in food handling establishments including, but not lim- [65 FR 38757, June 22, 2000] ited to dairies, dairy barns, res- taurants, food service operations, brew- § 180.1202 Bacillus sphaericus; exemp- eries, wineries, and beverage and food tion from the requirement of a tol- erance. processing plants. An exemption from the requirement [65 FR 75173, Dec. 1, 2000] of a tolerance is established for resi- § 180.1197 Hydrogen peroxide; exemp- dues of the microbial pesticides, Bacil- tion from the requirement of a tol- lus sphaericus when used in or on all erance. food crops. An exemption from the requirement [63 FR 48597, Sept. 11, 1998] of a tolerance is established for resi- dues of hydrogen peroxide in or on all § 180.1204 Harpin protein; exemption food commodities at the rate of ≤ 1% from the requirement of a toler- hydrogen peroxide per application on ance. growing and postharvest crops. An exemption from the requirement of a tolerance is established for resi- [67 FR 41844, June 20, 2002] dues of individual harpin proteins that § 180.1198 Gliocladium catenulatum meet specified physiochemical and tox- strain J1446; exemption from the icological criteria when used as bio- requirement of a tolerance. chemical pesticides on all food com- An exemption from the requirement modities to enhance plant growth, of a tolerance is established for resi- quality and yield, to improve overall dues of the microbial pesticide, plant health, and to aid in pest man- Gliocladium catenulatum strain J1446 agement. The physiochemical and toxi- when used in or on all food commod- cological criteria identifying harpin ities. proteins are as follows: (a) Consists of a protein less than 100 [63 FR 37288, July 10, 1998] kD in size, that is acidic (pI<7.0), gly- cine rich (>10%), and contains no more § 180.1199 than one cystine residue. Lysophosphatidylethanolamine (LPE); exemption from the require- (b) The source(s) of genetic material ment of a tolerance. encoding the protein are bacterial plant pathogens not known to be mam- An exemption from the requirement malian pathogens. of a tolerance is established for resi- (c) Elicits the hypersensitive re- dues of the biochemical pesticide sponse (HR) which is characterized as lysophosphatidylethanolamine in or on rapid, localized cell death in plant tis- all food commodities. sue after infiltration of harpin into the [67 FR 17636, Apr. 11, 2002] intercellular spaces of plant leaves.

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(d) Possesses a common secondary Name CAS Reg. structure consisting of a and b units No. that form an HR domain. N-cocoyl sarcosine mixture ...... 68411-97-2 (e) Is heat stable (retains HR activity N-lauroyl sarcosine ...... 97-78-9 when heated to 65 °C for 20 minutes). N-myristoyl sarcosine ...... 52558-73-3 (f) Is readily degraded by a proteinase N-oleoyl sarcosine ...... 110-25-8 representative of environmental condi- N-stearoyl sarcosine ...... 142-48-3 tions (no protein fragments >3.5 kD Sodium N-acyl sarcosinates. after 15 minutes degradation with N-cocoyl sarcosine sodium salt mixture ...... 61791-59-1 N-methyl-N-(1-oxo-9-octodecenyl) glycine .... 3624-77-9 Subtilisin A). N-methyl-N-(1-oxododecyl) glycine ...... 137-16-6 (g) Exhibits a rat acute oral toxicity N-methyl-N-(1-oxooctadecyl) glycine ...... 5136-55-0 (LD50) of greater than 5,000 mg product/ N-methyl-N-(1-oxotetradecyl glycine ...... 30364-51-3 kg body weight. [69 FR 24996, May 5, 2004] [64 FR 68046, Dec. 6, 1999]

§ 180.1205 Beauveria bassiana ATCC § 180.1209 Bacillus subtilis strain QST #74040; exemption from the require- 713; exemption from the require- ments of a tolerance. ment of a tolerance. An exemption from the requirement An exemption from the requirement of a tolerance is established for resi- of a tolerance is established for resi- dues of the insecticide Beauveria dues of the microbial pesticide Bacillus bassiana (ATCC #74040) in or on all food subtilis strain QST 713 when used in or commodities when applied or used as on all food commodities. ground and aerial foliar sprays for use only on terrestrial crops. [65 FR 41369, July 5, 2000] [64 FR 22796, Apr. 28, 1999] § 180.1210 Phosphorous acid; exemp- tion from the requirement of a tol- § 180.1206 Aspergillus flavus AF36; ex- erance. emption from the requirement of a tolerance. An exemption from the requirement (a) An exemption from the require- of a tolerance is established for resi- ment of a tolerance is established for dues of phosphorous acid and its am- residues of the microbial pesticide As- monium, sodium, and potassium salts pergillus flavus AF36 in or on cotton and in or on all food commodities when its food/feed commodities. used as an agricultural fungicide and in (b) Apergillus flavus AF36 is tempo- or on potatoes when applied as a post- rarily exempt from the requirement of harvest treatment at 35,600 ppm or less a tolerance on pistachio when used in phosphorous acid. accordance with the Experimental Use [71 FR 49373, Aug. 23, 2006] Permit 71693-EUP-1. This temporary exemption from tolerance will expire § 180.1212 Pseudomonas chlororaphis on May 14, 2010. Strain 63–28; exemption from the requirement of a tolerance. [68 FR 41541, July 14, 2003, as amended at 72 FR 28871, May 23, 2007] An exemption from the requirement of a tolerance is established for resi- § 180.1207 N-acyl sarcosines and so- dues of the microbial pesticide dium N-acyl sarcosinates; exemp- Pseudomonas chlororaphis Strain 63–28 tion from the requirement of a tol- in or on all food commodities. erance. An exemption from the requirement [66 FR 53346, Oct. 22, 2001] of a tolerance is established for resi- dues of the following substances when § 180.1213 Coniothyrium minitans strain CON/M/91–08; exemption used as inert ingredients (surfactants) from the requirement of a toler- at levels not to exceed 10% in pesticide ance. formulations containing glyphosate: An exemption from the requirement Name CAS Reg. of a tolerance is established for resi- No. dues of the microbial pesticide N-acyl sarcosines. Coniothyrium minitans strain CON/M/91–

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08 when used in or on all food commod- gions. Regulatory regions are the ge- ities. netic material, such as promoters, ter- [66 FR 16874, Mar. 28, 2001] minators, and enhancers, that control the expression of the genetic material § 180.1214 Bacillus thuringiensis encoding the Cry2Ab2 protein. Cry3Bb1 protein and the genetic material necessary for its produc- [69 FR 16823, Mar. 31, 2004] tion in corn; exemption from the re- EFFECTIVE DATE NOTE: At 72 FR 20434, quirement of a tolerance. 20435, Apr. 25, 2007, § 180.1215 was redesignated Bacillus thuringiensis Cry3Bb1 protein as § 174.519 and revised, effective July 24, 2007. and the genetic material necessary for For the convenience of the user, the revised its production in corn are exempt from text is set forth as follows: the requirement of a tolerance when § 174.519 Bacillus thuringiensis Cry2Ab2 used as plant-incorporated protectants protein in cotton; exemption from the re- in the food and feed commodities of quirement of a tolerance. field corn, sweet corn and popcorn. Ge- Residues of Bacillus thuringiensis Cry2Ab2 netic material necessary for its produc- protein in cotton is exempt from the require- tion means the genetic material which ment of a tolerance when used as a plant-in- comprise genetic material encoding the corporated protectant in the food and feed Cry3Bb1 protein and its regulatory re- commodities, cotton seed, cotton oil, cotton gions. Regulatory regions are the ge- meal, cotton hay, cotton hulls, cotton for- netic material, such as promoters, ter- age, and cotton gin byproducts. minators, and enhancers, that control the expression of the genetic material § 180.1216 B-D-glucuronidase from E. encoding the Cry3Bb1 protein. coli and the genetic material nec- essary for its production as a plant- [69 FR 16814, Mar. 31, 2004] pesticide inert ingredient; exemp- tion from the requirement of a tol- EFFECTIVE DATE NOTE: At 72 FR 20434, 20435, Apr. 25, 2007, § 180.1214 was redesignated erance. as § 174.518 and revised, effective July 24, 2007. An exemption from the requirement For the convenience of the user, the revised of a tolerance is established for resi- text is set forth as follows: dues of B-D-glucuronidase from E. coli § 174.518 Bacillus thuringiensis Cry3Bb1 and the genetic material necessary for protein in corn; exemption from the re- its production when used as a plant- quirement of a tolerance. pesticide inert ingredient in or on all Residues of Bacillus thuringiensis Cry3Bb1 food commodities. Genetic material protein in corn are exempt from the require- ment of a tolerance when used as plant-in- necessary for the production means corporated protectants in the food and feed both: Genetic material that encodes a commodities of corn; corn, field; corn, sweet; substance or leads to the production of and corn, pop. a substance; and regulatory regions. It does not include non-coding, non-ex- § 180.1215 Bacillus thuringiensis pressed nucleotide sequences. Regu- Cry2Ab2 protein and the genetic material necessary for its produc- latory region means genetic material tion in cotton; exemption from the that controls the expression of the ge- requirement of a tolerance. netic material that encodes a pes- Bacillus thuringiensis Cry2Ab2 protein ticidal substance or leads to the pro- and the genetic material necessary for duction of a pesticidal substance. Ex- its production in cotton is exempt from amples of regulatory regions include, the requirement of a tolerance when but are not limited to, promoters, used as a plant-incorporated protectant enhancers, and terminators. in the food and feed commodities, cot- [66 FR 42961, Aug. 16, 2001] ton seed, cotton oil, cotton meal, cot- ton hay, cotton hulls, cotton forage, EFFECTIVE DATE NOTE: At 72 FR 20434, and cotton gin byproducts. Genetic ma- 20435, Apr. 25, 2007, § 180.1216 was redesignated terial necessary for its production as § 174.525 and revised, effective July 24, 2007. means the genetic material which com- For the convenience of the user, the revised text is set forth as follows: prise genetic material encoding the Cry2Ab2 protein and its regulatory re-

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§ 174.525 E. coli B-D-glucuronidase enzyme § 180.1219 Foramsulfuron; exemption as a plant-incorporated protectant inert from the requirement of a toler- ingredient; exemption from the require- ance. ment of a tolerance. Residues of E. coli B-D-glucuronidase en- The pesticide foramsulfuron (N,N-di- zyme are exempt from the requirement of a methyl-2-[3-(4,6-dimethoxy-pyrimidin- tolerance when used as a plant-incorporated 2- yl)ureidosulfonyl]-4- protectant inert ingredient in all food com- formylaminobenzamide) is exempted modities. from the requirement of a tolerance in corn, field, grain; corn, field, forage; § 180.1217 Bacillus thuringiensis corn, field, stover; corn, sweet Cry1F protein and the genetic ma- (K+CWHR); corn, sweet, forage; corn, terial necessary for its production sweet, stover; corn, pop grain; and in corn; exemption from the re- corn, pop, stover when applied as a her- quirement of a tolerance. bicide in accordance with good agricul- Bacillus thuringiensis Cry1F protein tural practices. and the genetic material necessary for [72 FR 26324, May 9, 2007] its production in corn are exempt from the requirement of a tolerance when § 180.1220 1-Methylcyclopropene; ex- used as plant-pesticides in the food and emption from the requirement of a tolerance. feed commodities of field corn, sweet corn and popcorn. ‘‘Genetic material An exemption from the requirement necessary for its production’’ means of a tolerance is established for resi- the genetic material which comprise: dues of 1-Methylcyclopropene in or on genetic material encoding the Cry1F fruits and vegetables when used as a post harvest plant growth regulator, protein and its regulatory regions. i.e., for the purpose of inhibiting the ef- ‘‘Regulatory regions’’ are the genetic fects of ethylene. material, such as promoters, termi- nators, and enhancers, that control the [67 FR 48800, July 26, 2002] expression of the genetic material en- § 180.1221 Pseudozyma flocculosa coding the Cry1F protein. strain PF-A22 UL; exemption from [66 FR 30325, June 6, 2001] the requirement of a tolerance. An exemption from the requirement EFFECTIVE DATE NOTE: At 72 FR 20434, 20435, Apr. 25, 2007, § 180.1217 was redesignated of a tolerance is established for resi- as § 174.520 and revised, effective July 24, 2007. dues of Pseudozyma flocculosa strain For the convenience of the user, the revised PF-A22 UL in or on all food commod- text is set forth as follows: ities. [67 FR 60966, Sept. 27, 2002] § 174.520 Bacillus thuringiensis Cry1F pro- tein in corn; exemption from the require- ment of a tolerance. § 180.1222 Sucrose octanoate esters; exemption from the requirement of Residues of Bacillus thuringiensis Cry1F a tolerance. protein in corn are exempt from the require- ment of a tolerance when used as plant-in- An exemption from the requirement corporated protectants in the food and feed of a tolerance is established for resi- commodities of corn; corn, field; corn, sweet; dues of sucrose octanoate esters [(a-D- and corn, pop. glucopyranosyl-b-D-fructofuranosyl-oc- tanoate), mono-, di-, and triesters of § 180.1218 Indian Meal Moth sucrose octanoate] in or on all food Granulosis Virus; exemption from commodities when used in accordance the requirement of a tolerance. with good agricultural practices. An exemption from the requirement [67 FR 60152, Sept. 25, 2002] of a tolerance is established for resi- dues of the microbial pesticide Indian § 180.1223 Imazamox; exemption from Meal Moth Granulosis Virus when used the requirement of a tolerance. in or on all food commodities. The herbicide imazamox, (±) 2, -[4,5- dihydro-4-methyl-4-(1-methylethyl)-5- [68 FR 55875, Sept. 29, 2003] oxo-1H-imidazol-2-yl]-5- (methoxymethyl)-3-pyridinecarboxylic

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acid, is exempt from the requirement § 180.1227 Bacillus thuringiensis of a tolerance on all food commodities Cry1F protein and it genetic mate- when applied as a herbicide in accord- rial necessary for its production in ance with good agricultural practices. or on cotton; temporary exemption from the requirement of a toler- [68 FR 7433, Feb. 14, 2003] ance. Bacillus thuringiensis Cry1F protein § 180.1224 Bacillus pumilus GB34; ex- and its genetic material necessary for emption from the requirement of a its production in cotton are exempt tolerance. from the requirement of a tolerance An exemption from the requirement when used as a plant-incorporated pro- of a tolerance is established for resi- tectant in the food and feed commodity dues of the microbial pesticide Bacillus of cotton. This temporary tolerance ex- pumilus GB34 when used as a seed treat- emption expires on May 1, 2005. ment in or on all food commodities. An [69 FR 16819, Mar. 31, 2004] exemption is also granted for such resi- EFFECTIVE DATE NOTE: At 72 FR 20434, Apr. dues on treated but unplanted soybean 25, 2007, § 180.1227 was removed, effective July seeds. 24, 2007. [69 FR 76625, Dec. 22, 2004] § 180.1228 Diallyl sulfides; exemption from the requirement of a toler- § 180.1225 Decanoic acid; exemption ance. from the requirement of a toler- ance. An exemption from the requirement of a tolerance is established for resi- An exemption from the requirement dues of diallyl sulfides when used in/on of a tolerance is established for resi- garlic, leeks, onions, and shallots. dues of decanoic acid in or on all raw agricultural commodities and in proc- [68 FR 40808, July 9, 2003] essed commodities, when such residues § 180.1230 Ferrous sulfate; exemption result from the use of decanoic acid as from the requirement of a toler- an antimicrobial treatment in solu- ance. tions containing a diluted end-use con- An exemption from the requirement centration of decanoic acid (up to 170 of a tolerance is established for resi- ppm per application) on food contact dues of ferrous sulfate. surfaces such as equipment, pipelines, tanks, vats, fillers, evaporators, [70 FR 33363, June 8, 2005] pasteurizers and aseptic equipment in § 180.1231 Lime; exemption from the restaurants, food service operations, requirement of a tolerance. dairies, breweries, wineries, beverage An exemption from the requirement and food processing plants. of a tolerance is established for resi- [68 FR 7939, Feb. 19, 2003; 68 FR 17308, Apr. 9, dues of lime. 2003] [70 FR 33363, June 8, 2005]

§ 180.1226 Bacillus pumilus strain § 180.1232 Lime-sulfur; exemption from QST2808; temporary exemption the requirement of a tolerance. from the requirement of a toler- ance. An exemption from the requirement of a tolerance is established for resi- A temporary exemption from the re- dues of lime-sulfur. quirement of a tolerance is established for residues of the microbial pesticide [70 FR 33363, June 8, 2005] Bacillus pumilus strain QST2808 when § 180.1233 Potassium sorbate; exemp- used in or on all agricultural commod- tion from the requirement of a tol- ities when applied/used in accordance erance. with label directions. An exemption from the requirement [68 FR 36480, June 18, 2003] of a tolerance is established for resi- dues of potassium sorbate. [70 FR 33363, June 8, 2005]

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§ 180.1234 Sodium carbonate; exemp- ance for residues of thymol will expire tion from the requirement of a tol- and are revoked on June 30, 2007. erance. (b) An exemption from the require- An exemption from the requirement ment of tolerance is established for of a tolerance is established for resi- residues of Thymol (5-methyl-2-iso- dues of sodium carbonate. propyl-1-phenol in or on honey, honey- comb, and honeycomb with honey when [70 FR 33363, June 8, 2005] used in accordance with good agricul- § 180.1235 Sodium hypochlorite; ex- tural practices. emption from the requirement of a [70 FR 37696, June 30, 2005, as amended at 71 tolerance. FR 2895, Jan. 18, 2006] An exemption from the requirement of a tolerance is established for resi- § 180.1241 Eucalyptus oil; exemption dues of sodium hypochlorite. from the requirement of a toler- ance. [70 FR 33363, June 8, 2005] Time-limited exemptions from the § 180.1236 Sulfur; exemption from the requirement of a tolerance are estab- requirement of a tolerance. lished for residues of eucalyptus oil on An exemption from the requirement honey and honeycomb in connection of a tolerance is established for resi- with use of the pesticide under section dues of sulfur. 18 emergency exemptions granted by the EPA. These time-limited exemp- [70 FR 33363, June 8, 2005] tions from the requirement of a toler- ance for residues of eucalyptus oil will § 180.1237 Sodium metasilicate; exemp- expire and are revoked on June 30, 2007. tion from the requirement of a tol- erance. [70 FR 37696, June 30, 2005] (a) An exemption from the require- ment of a tolerance is established for § 180.1242 Bacillus thuringiensis residues of sodium metasilicate in or Cry34Ab1 and Cry35Ab1 proteins and the genetic material necessary on all food commodities when used in for their production in corn; tem- accordance with approved label rates porary exemption from the require- and good agricultural practices as a ment of a tolerance. plant desiccant, so long as the sodium Bacillus thuringiensis Cry34Ab1 and metasilicate does not exceed 4% by Cry35Ab1 proteins and the genetic ma- weight in aqueous solution. terial necessary for their production in (b) An exemption from the require- corn are temporarily exempted from ment of a tolerance is established for the requirement of a tolerance when residues of sodium metasilicate in or used as plant-incorporated protectants on all food commodities when used in in the food and feed commodities of accordance with approved label rates field corn, sweet corn and popcorn. and good agricultural practices as an This temporary exemption from the re- insecticide and fungicide, so long as quirement of a tolerance will permit the sodium metasilicate does not ex- the use of the food commodities in this ceed 2.41% by weight in aqueous solu- paragraph when treated in accordance tion. with the provisions of the experimental [71 FR 19441, Apr. 14, 2006] use permits 68467-EUP-3, 68467-EUP-5, 68467-EUP-T(7), 68467-EUP-I(8), 29964- § 180.1240 Thymol; exemption from the EUP-1, 29964-EUP-3, 29964-EUP-U(4), requirement of a tolerance. and 29964-EUP-L(5) which may be (a) Time-limited exemptions from issued and amended/extended under the the requirement of a tolerance are es- Federal Insecticide, Fungicide, and tablished for residues of thymol on Rodenticide Act (FIFRA), as amended honey and honeycomb in connection (7 U.S.C. 136). This temporary exemp- with use of the pesticide under section tion from the requirement of a toler- 18 emergency exemptions granted by ance expires and is revoked April 30, the EPA. These time-limited exemp- 2006. This temporary exemption from tions from the requirement of a toler- the requirement of a tolerance may be

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revoked at any time if the experi- § 180.1248 Exemption of citronellol mental use permit is revoked or if any from the requirement of a toler- experience with or scientific data on ance. this pesticide indicate that the toler- An exemption from the requirement ance is not safe. of a tolerance is established for resi- [68 FR 40183, July 7, 2003] dues of the biochemical pesticide citronellol in or on all food commod- EFFECTIVE DATE NOTE: At 72 FR 20434, Apr. 25, 2007, § 180.1242 was removed, effective July ities. 24, 2007. [69 FR 23146, Apr. 28, 2004]

§ 180.1243 Bacillus subtilis var. § 180.1249 Hygromycin B phospho- amyloliquefaciens strain FZB24; ex- transferase (APH4) marker protein emption from the requirement of a and the genetic material necessary tolerance. for its production in all plants; ex- An exemption from the requirement emption from the requirement of a of a tolerance for residues of the Bacil- tolerance. lus subtilis var. amyloliquefaciens strain Hygromycin B phosphotransferase FZB24 in or on all agricultural com- (APH4) and the genetic material nec- modities when applied/used in accord- essary for its production in all plants ance with label directions. are exempt from the requirement of a [68 FR 44640, July 30, 2003] tolerance when used as a plant-incor- porated protectant inert ingredient in § 180.1244 Ammonium bicarbonate; ex- cotton. ‘‘Genetic material necessary emption from the requirement of a for its production’’ means the genetic tolerance. material which comprise genetic mate- An exemption from the requirement rial encoding the APH4 protein and its of tolerance is established for residues regulatory regions. ‘‘Regulatory re- of ammonium bicarbonate used in or gions’’ are the genetic material that on all food commodities when used in control the expression of the genetic accordance with good agricultural material encoding the APH4 protein, practices. such as promoters, terminators, and enhancers. [69 FR 13745, Mar. 24, 2004] [69 FR 18278, Apr. 7, 2004] § 180.1245 Rhamnolipid biosurfactant; exemption from the requirement of EFFECTIVE DATE NOTE: At 72 FR 20434, a tolerance. 20435, Apr. 25, 2007, § 180.1249 was redesignated as § 174.526 and revised, effective July 24, 2007. An exemption from the requirement For the convenience of the user, the revised of a tolerance is established for resi- text is set forth as follows: dues of rhamnolipid biosurfactant when used in accordance with good ag- § 174.526 Hygromycin B phosphotransferase (APH4) marker protein in all plants; ex- ricultural practices as a fungicide in or emption from the requirement of a toler- on all food commodities. ance. [69 FR 16800, Mar. 31, 2004] Residues of the Hygromycin B phosphotransferase (APH4) enzyme in all § 180.1246 Yeast Extract Hydrolysate plants are exempt from the requirement of a from Saccharomyces cerevisiae: ex- tolerance when used as a plant-incorporated emption from the requirement of a protectant inert ingredient in cotton. tolerance. § 180.1250 C8, C10, and C12 fatty acid This regulation establishes an ex- monoesters of glycerol and pro- emption from the requirement of a tol- pylene glycol; exemption from the erance for residues of the biochemical requirement of a tolerance. pesticide Yeast Extract Hydrolysate The C8, C10, and C12 straight-chain from Saccharomyces cerevisiae on all fatty acid monoesters of glycerol (glyc- food commodities when applied/used erol monocaprylate, glycerol for the management of plant diseases. monocaprate, and glycerol [69 FR 9958, Mar. 3, 2004] monolaurate) and propylene glycol

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(propylene glycol monocaprylate, pro- Streptomyces lydicus WYEC 108 when pylene glycol monocaprate, and pro- used in or on all agricultural commod- pylene glycol monolaurate) are exempt ities when applied/used in accordance from the requirement of a tolerance in with label directions. or on all food commodities when used in accordance with approved label rates [69 FR 31301, June 3, 2004] and good agricultural practice. § 180.1254 Aspergillus flavus NRRL [69 FR 34944, June 23, 2004] 21882 on peanut; exemption from requirement of a tolerance. § 180.1251 Geraniol; exemption from the requirement of a tolerance. (a) An exemption from the require- An exemption from the requirement ment of a tolerance is established for of a tolerance is established for resi- residues of Aspergillus flavus NRRL dues of the biochemical pesticide gera- 21882 on peanut and its food/feed com- niol in or on all food commodities. modities. (b) Aspergillus flavus NRRL 21882 is [69 FR 23151, Apr. 28, 2004] temporarily exempt from the require- § 180.1252 Phosphomannose isomerase ment of a tolerance on corn when used and the genetic material necessary in accordance with the Experimental for its production in all plants; ex- Use Permit 75624–EUP–2. This tem- emption from the requirement of a porary exemption from tolerance will tolerance. expire on May 2, 2009. Phosphomannose isomerase (PMI) protein and the genetic material nec- [69 FR 39350, June 30, 2004, as amended at 72 essary for its production in plants are FR 27463, May 16, 2007] exempt from the requirement of a tol- § 180.1255 Bacillus pumilus strain QST erance when used as plant-incorporated 2808; exemption from the require- protectant inert ingredients in plant ment of a tolerance. commodities. Genetic material nec- essary for its production means the ge- An exemption from the requirement netic material which comprise genetic of a tolerance is established for resi- material encoding the PMI protein and dues of the microbial pesticide Bacillus its regulatory regions. Regulatory re- pumilus strain QST 2808 when used in or gions are the genetic material, such as on all agricultural commodities when promoters, terminators, and enhancers, applied/used in accordance with label that control the expression of the ge- directions. netic material encoding the PMI pro- tein. [69 FR 63954, Nov. 3, 2004] [69 FR 26775, May 14, 2004] § 180.1256 Alternaria destruens strain EFFECTIVE DATE NOTE: At 72 FR 20434, 059; exemption from the require- 20435, Apr. 25, 2007, § 180.1252 was redesignated ment of a tolerance. as § 174.527 and revised, effective July 24, 2007. An exemption from the requirement For the convenience of the user, the revised of a tolerance is established for resi- text is set forth as follows: dues of the microbial pesticide § 174.527 Phosphomannose isomerase in all Alternaria destruens Strain 059 when plants; exemption from the requirement used in or on all raw agricultural com- of a tolerance. modities when applied/used in accord- Residues of the phosphomannose isomerase (PMI) enzyme in plants are exempt from the ance with label directions. requirement of a tolerance when used as [70 FR 28459, May 18, 2005] plant-incorporated protectant inert ingredi- ents in all food commodities. § 180.1257 Paecilomyces lilacinus § 180.1253 Streptomyces lydicus WYEC strain 251; exemption from the re- 108; exemption from the require- quirement of a tolerance. ment of a tolerance. An exemption from the requirement An exemption from the requirement of a tolerance is established for resi- of a tolerance is established for resi- dues of the microbial pesticide dues of the microbial pesticide Paecilomyces lilacinus strain 251 when

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used in or on all agricultural commod- § 180.1262 Sorbitol octanoate; exemp- ities when applied/used in accordance tion from the requirement of a tol- with label directions. erance. [70 FR 19283, Apr. 13, 2005] An exemption from the requirement of a tolerance is established for resi- § 180.1258 Acetic acid; exemption from dues of sorbitol octanoate in or on all the requirement of a tolerance. food commodities when used in accord- An exemption from the requirement ance with label directions. of a tolerance is established for resi- [71 FR 4518, Jan. 27, 2006] dues of the biochemical pesticide ace- tic acid when used as a preservative on § 180.1263 Tetrahydrofurfuryl alcohol; post-harvest agricultural commodities exemption from the requirement of intended for animal feed, including al- a tolerance. falfa, barley grain, Bermuda grass, Tetrahydrofurfuryl alcohol (THFA, bluegrass, brome grass, clover, corn CAS Reg. No. 97–99–4) is exempt from grain, cowpea hay, fescue, lespedeza, the requirement of a tolerance in or on lupines, oat grain, orchard grass, pea- all raw agricultural commodities when nut grass, Timothy, vetch, and wheat used in accordance with good agricul- grain, or commodities described as tural practices as an inert ingredient grain or hay. applied only: [70 FR 44488, Aug. 3, 2005] (a) For use as a seed treatment. (b) For applications prior to planting § 180.1259 Reynoutria sachalinensis ex- and at the time of planting. tract; exemption from the require- (c) For use on cotton. ment of a tolerance. (d) For use in herbicides with one ap- Residues of the biochemical pesticide plication to wheat and barley prior to Reynoutria sachalinensis extract, when the pre-boot stage, and two applica- derived from the whole plant extract, tions to canola and soybeans pre- are exempt from the requirement of a bloom. tolerance in or on all food commod- (e) For use in herbicides with two ap- ities. plications to field corn up to 24 inches [70 FR 55277, Sept. 21, 2005] tall (V 5 stage).

§ 180.1260 Muscodor albus QST 20799 [71 FR 45415, Aug. 9, 2006] and the volatiles produced on re- EFFECTIVE DATE NOTE: At 71 FR 45415, Aug. hydration; exemption from the re- 9, 2006, § 180.1263 was added, effective Feb. 9, quirement of a tolerance. 2008. An exemption from the requirement of a tolerance is established on all food/ § 180.1267 Pantoea agglomerans strain C9–1; exemption from the require- feed commodities, for residues of ment of a tolerance. Muscodor albus QST 20799, and the volatiles produced on its rehydration, An exemption from the requirement when the pesticide is used for all agri- of a tolerance is established for resi- cultural applications, including seed, dues of Pantoea agglomerans strain C9–1 propagule and post harvest treatments. when used on apples and pears. [70 FR 56576, Sept. 28, 2005] [71 FR 24596, Apr. 26, 2006]

§ 180.1261 Xanthomonas campestris pv. § 180.1268 Potassium silicate; exemp- vesicatoria and Pseudomonas tion from the requirement of a tol- syringae pv. tomato specific erance. Bacteriophages. Potassium silicate is exempt from An exemption from the requirement the requirement of a tolerance in or on of a tolerance is established for resi- all food commodities so long as the po- dues of Xanthomonas campestris pv. tassium silicate is not applied at rates vesicatoria and Pseudomonas syringae pv. exceeding 1% by weight in aqueous so- tomato specific bacteriophages in or on lution and when used in accordance tomatoes and peppers. with good agricultural practices. [70 FR 76704, Dec. 28, 2005] [71 FR 34272, June 14, 2006]

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§ 180.1269 Bacillus mycoides Isolate J § 180.1274 Tris (2-ethylhexyl) phos- on sugar beets: exemption from the phate; exemption from the require- requirement of a tolerance. ment of a tolerance. Bacillus mycoides isolate J is tempo- Tris (2-ethylhexyl) phosphate (TEHP, rarily exempt from the requirement of CAS Reg. No. 78–42–2) is exempt from a tolerance when used as a fungicide the requirement of a tolerance for resi- for control of Cercospora Leaf Spot dues in wheat and barley when used (Cercospora beticola) on sugar beets. under the following conditions: This temporary exemption from the re- (a) The use is in accordance with good agricultural practices; quirement of a tolerance expires and is (b) Tris (2-ethylhexyl) phosphate is revoked on December 31, 2007. used as an inert ingredient in pesticide [71 FR 34267, June 14, 2006] formulations with the active ingredi- ents pinoxaden, clodinafop-propargyl, § 180.1270 Isophorone; exemption from and tralkoxydium; the requirement of a tolerance. (c) Tris (2-ethylhexyl) phosphate is Isophorone (CAS Reg. No. 78–59–1) is applied no more than twice per season; exempt from the requirement of a tol- and erance when used as an inert ingre- (d) The applications occur no later dient in pesticide formulations applied than the pre-boot stage (prior to for- mation of edible grain). to beets, ginseng, rice, spinach, sugar beets, and Swiss chard. [72 FR 5624, Feb. 7, 2007] [71 FR 45408, Aug. 9, 2006] § 180.1275 Pythium; exception from the requirement of a tolerance. § 180.1271 Eucalyptus oil; exemption An exemption from the requirement from the requirement of a toler- ance. of tolerance is established on all food/ feed commodities, for residues of An exemption from the requirement pythium oligandrum DV 74 when the pes- of tolerance is established for residues ticide is used on food crops. of eucalyptus oil in or on honey, hon- [72 FR 27452, May 16, 2007] eycomb, and honeycomb with honey when used at 2g or less eucalyptus oil § 180.1276 Tobacco mild green mosaic per hive, where the eucalyptus oil con- tobamovirus (TMGMV); temporary tains 80% or more eucalyptol. exemption from the requirement of a tolerance. [71 FR 53979, Sept. 13, 2006] A temporary exemption from the re- § 180.1272 Pantoea agglomerans strain quirement of a tolerance is established E325; exemption from the require- for residues of tobacco mild green mo- ment of a tolerance. saic tobamovirus in or on all grass and grass hay. An exemption from the requirement of a tolerance is established for resi- [72 FR 35181, June 27, 2007] dues of Pantoea agglomerans strain E325 when used on apples and pears. Subpart E—Pesticide Chemicals [71 FR 54933, Sept. 20, 2006] Not Requiring a Tolerance or an Exemption From a Toler- § 180.1273 Beauveria bassiana HF23; ance exemption from the requirement of a tolerance. SOURCE: 66 FR 66772, Dec. 27, 2001, unless An exemption from the requirement otherwise noted. of a tolerance is established on all food/ § 180.2000 Scope. feed commodities, for residues of Beauveria bassiana HF23 when the pes- This subpart sets forth the pesticide ticide is used for chicken manure chemicals for use in agricultural or treatment. other food-related settings for which neither a tolerance nor an exemption is [72 FR 1183, Jan. 10, 2007] deemed to be needed by EPA.

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§ 180.2003 Definitions. § 180.2010 Threshold of regulation de- terminations. [Reserved] (a) Food uses are the uses of a pes- ticide chemical that are likely to yield § 180.2020 Non-food determinations. residues in food or feed crops, meat, The following pesticide chemical uses milk, poultry or eggs. do not need a tolerance or exemption (b) Non-food uses are those uses that from the requirement of a tolerance are not likely to yield residues in food based on EPA’s determination that or feed crops, meat, milk, poultry or they are not likely to result in residues eggs. in or on food.

Pesticide Chemical CAS Reg. No. Limits Uses

Methyl bromide 74–83–9 When applied as a pre-plant soil fumigant All pre-plant soil uses Potassium 12298–68–9 When applied to growing crops in foreign countries Bananas, grapes, triiodide (KI3) and melons Rhodamine B 81–88–9 Not to exceed 2% by weight of the formulated product and 60 ppm on Dye for seed treat- the treated seed ment

[66 FR 66772, Dec. 27, 2001, as amended at 70 FR 40201, July 13, 2005; 71 FR 45402, Aug. 9, 2006]

PARTS 181–189 [RESERVED]

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