5 Underwood Court, Delran, New Jersey 08075-1229 856-461-4003 • 215-238-0338 • Fax 856-461-4916 SITE ASSESSMENT TECHNICAL ASSISTANCE EPA CONTRACT 68-S5-3002
31 March 2000
Mr. Kevin Boyd (3HS31) TDD No. 0003-06 On-Scene Coordinator DCN £0000163 U.S^ Environmental Protection Agency 1650 Arch Street "' • Philadelphia, PA 19103-2029 Subject: Hilltop Residential Lab Site - Trip Report Dear Mr. Boyd: Enclosed is the Hilltop Residential Lab Site Trip Report for your review. If you have any : questions, please feel free to contact me at (856) 461-4003, Ext. 228. Very truly yours, . ROY F. WESTON, INC.
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cc: TDD File
satazfp.hiltpreslabltr
FEDERA. WestonL PROGRAM, Inc. S DIVISION In Association with Foster Wheeler Environmental Corporation; Resource Applications, Inc.; C.C. Johnson & Malhotra, P.C.; and PRC Environmental Management, Inc. • p I n n ri n O TRIP REPORT
HILLTOP RESIDENTIAL LAB SITE TDD No. 0003-06 UPPER DARBY, DELAWARE COUNTY. PA ' CONTRACT Mo. 68-S5-3002
1.0 INTRODUCTION ,______On 14 March 2000, the Roy F. Weston, Inc. (WESTON*), Site Assessment Technical Assistance (SATA) team was directed by U.S. Environmental Protection Agency (EPA) On-Scene Coordinator (OSC) Kevin Boyd to conduct an emergency assessment at the • Hilltop Residential Lab Site located in Upper Darby, Delaware County, PA.
2.0 BACKGROUND ______2.1 Site Location The Hilltop Residential Lab Site consists of a residential property located at 71 10 Hilltop Road, in Upper Darby, Delaware County, PA as illustrated on Figure 1, Site Location Map. 2.2 Site Description : The site is approximately one acre in size and includes a three story house with a stone exterior, 3 bedrooms, 1.5 baths, a full basement housing a laboratory, and a detached single car garage. The property has a small front yard with a grass lawn that measures approximately 10 feet by 10 feet, and a larger backyard that is \^J . approximately 20 feet by 30 feet.
3.0 SITE ACTIVITIES ______On 15 March 2000, OSC Kevin Boyd initiated an emergency removal of hazardous chemicals at the residence located at 71 10 Hilltop Road. SATA conducted air monitoring, inventoried hazardous chemicals in the basement laboratory, and observed their segregation, packing, and disposal by the Emergency and Rapid Response Services (ERRS) contractor, OHM. 3.1 Site Conditions and Observations The residence on this site has grass in the front and backyards. There were no signs of stressed vegetation or stained grass on the site. The average meteorological conditions during the site activities were partly cloudy skies, a light breeze, and a temperature of 60 °F. 3.2 Site Activities SATA members Ray Moffett, Larry Jiang, and Bruce Elkins met OSC Kevin Boyd on site on 1 5 March 2000. SATA entered the laboratory and conducted air monitoring with an organic vapor analyzer (OVA), photoionization dectector satazip-hilltpitslabtrp-ipt \ J I March 2000 ARIOOOQI* FEDERAL PROGRAMS HILLTOP RESIDENTIAL LAB SITE TDD No. 0003-06 DIVISION UPPER DARBY, DELAWARE CO., PA Contract No. 68-35-3002 MMWRUCOMUlTUnt
FIGURE 1 NOT TO SCALE SITE LOCATION MAP ARI00005 HILLTOP RESIDENTIAL LAB SITE TDD No. 0003-06 UPPER DARBY, DELAWARE COUNTY, PA______CONTRACT No. 68-S5-3002
(PID), Multi-Rae, mercury vapor analyzer (Jerome Meter), and micro R meter. Readings on all instruments were below detection levels. After completion of air ^*J monitoring, and at the OSC's direction, SATA began inventorying the chemicals found in the basement of the residence (see Figure 2, Chemical Inventory Location Map). Two chemical bottles in the laboratory had crystallized and had the potential to be shock sensitive. The bottle's contents were solids, which had sublimed along the cap, but did not contain any hazardous peroxide. If hazardous peroxide had been formed during the degradation of the bottle's contents, long needle like crystals would have been visible in the bottle and around the edges of the lid. The crystals in and around the suspected bottles were not needle-like and the SATA chemist determined that they were not shock sensitive. ERRS removed the items inventoried by SATA from the laboratory and began packing them by compatibility groups into drums and cans. SATA also collected photo documentation of the site (see Attachment 1, Photo Log). The EPA Community Involvement Coordinator distributed a fact sheet to the residents of Hilltop Road to inform them of developments on the site (see Attachment 5, EPA Fact Sheets). The OSC, SATA, and ERRS left the site at 1745 hours. A 24- security service was hired by the EPA to provide security at the site until the :; completion of cleanup operations. SATA returned the morning of 16 March 2000 and completed the chemical inventory. ERRS continued to pack and segregate the items inventoried by SATA into drums and cans. OSC Boyd presented the Upper Darby Police Department .> with a suspected drug related item that had been found during the SATA chemical inventory. Upon completion of the chemical inventory, SATA took some additional photographs of site activities and then departed the site. ERRS continued to remove and pack the inventoried items with OSC supervision. The EPA Community Involvement Coordinator distributed another fact sheet to the residents of Hilltop Road to inform them that the EPA had received access to the site and that removal of the chemicals was continuing (see Attachment 5). SATA returned the morning of 17 March 2000 and observed ERRS packing the remaining inventoried chemicals into drums and cans. SATA took some additional photographs of the site and departed upon completion of ERRS packing activities. SATA and ERRS were directed by the OSC to return to the site the week of 20 March 2000 for transportation and disposal (T&D) of the drums and cans. SATA returned the morning of 23 March 2000, and observed ERRS removing several incorrectly packed items from the drums. These items were then repacked into drums with compatible chemicals. Additionally, a controlled material of interest to the Drug Enforcement Agency (DE A) was removed from a drum by ERRS. The DEA collected the controlled material from OSC Boyd-that same day. SATA took some additional photographs of site activities and then departed the site with ERRS and the OSC. SATA and ERRS were directed by the OSC to return to the site the next day for T&D of the drums and cans. ^^ satthilltpresltbtr-rpt 3 31 March 2000 AR100006 FEDERAL HILLTOP RESIDENTIAL LAB SITE TOO No. 0003-06 PROGRAMS ««*„ ^r.______,! • DIVISION UPPER DARBY, DELAWARE CO., PA Contract No. 68-S5-3002 '-'j
„ . . f~\ Drum Storage Area Backyard ' '- - Entrance cP6b to Basement Rear of House Garage First Floor
I I Bar Are* Ciwlapaog A ConUtnen lend! Debris 1 Filled Room w \ Containers3and4 Bah Room Stairway 5,6, and? | Old Equipment
'Hallway v 1 throug^.h* 6 e bB__^J A Ana j D • • I Basement of House D r « "
Nfiacellaneous Equipment and Debris
Sidewalk
7110 Hilltop Road
Figure 2 Not to i cale Chemical Inventory Location Map
ARI00007 HILLTOP RESIDENTIAL LAB SITE TDD No. 0003-06 UPPER DARBY, DELAWARE COUNTY. PA______CONTRACT No. 68-S5-3002
SATA returned the afternoon of 24"March 2000, met the OSC, and observed ERRS complete the removal of the drums and cans for disposal. SAT A received a copy of the transportation and disposal documentation from ERRS. The security service, was released from service as the cleanup activities at the site were concluded. SATA took some additional photographs of site activities and then departed. On 27 March 2000, the EPA Community Involvement Coordinator distributed another fact sheet to the residents of Hilltop Road to inform them that the EPA had removed the chemicals from the residence and that cleanup actions were completed. 4.0 CHEMICAL INVENTORY RESULTS______The laboratory items inventoried at the site by SATA included approximately 805 chemical bottles of various sizes, and other miscellaneous items. Questionable inventoried items Were presented to the OSC for inspection and determination of final disposal. ERRS categorized and segregated these chemicals into seven 55-gallon drums, six 15-gallon drums, and four 5-gallon cans. ERRS then labeled the drums and cans as containing either hazardous or non-hazardous waste* Six of the 55-gallon drums were labeled as hazardous waste, and one was labeled as non-hazardous waste. The six 15- gallon drums were labeled as hazardous waste, as were the four 5-gallon cans. The contractor (Clean Venture) loaded the drums and cans onto a truck and transported them off the site for proper disposal. The chemicals inventoried by SATA can be found on the tables listed in Attachment 2. The ERRS chemical inventory listing can be found in Attachment 3. Copies of the transportation and disposal documentation (manifests) can be found in Attachment 4.
5.0 FUTURE ACTIONS______
The EPA does not anticipate any further action at this time. ATTACHMENTS: 1 - Photograph Log 2 - SATA Chemical Inventory 3 - ERRS Chemical Inventory 4 - Transportation and Disposal Documentation 5 - EPA Fact Sheets
satahilltpreslabtMpt 5 ""—"12000 ARI00008 Attachment 1 Photograph Log
ARI00009 Photograph Log Hilltop Residential Lab Site Upper Darby, Delaware County, PA
Date Taken: 15 March 2000 Photographer: Region III SATA Description: Facing west towards the Hilltop Residential Lab Site.
Date Taken: 15 March 2000 Photographer: Region III SATA Description: Driveway on southwestern side of the residence.
ARIOOOIO Pb otograph Log Hi ltop Residential Lab Site Ufiper Darby, Delaware County, PA
Date Taken: 15 March 2000 Photographer: Region ID SATA Description: View facing northwest towards other residences on Hilltop Road.
Date Taken: 15 March 2000 Photographer: Region ffl SATA Description: View feeing southwest of other residential homes located on Hilltop Road.
ARIOOOII Photograph Log Hilltop Residential Lab Site Upper Darby, Delaware County, PA
Date Taken: 15 March 2000 Photographer: Region III SATA Description: SATA member preparing to enter basement of residence.
Date Taken: 15 March 2000 Photographer: Region HI SATA Description: SATA member opening basement door for entry into the basement.
ARIOOOI2 Photograph Log Hi top Residential Lab Site Uf per Darby, Delaware County, PA
Date Taken: 15 March 2000 Photographer. Region HI SATA ' Description: SATA member inspecting label of jar found in the basement.
Date Taken: 15 March 2000 Photographer: Region ffl SATA Description: Chemicals inside cabinets 5 and 6 in the basement at the site.
ARIOOOI3 Photograph Log Hilltop Residential Lab Site Upper Darby, Delaware County, PA
Date Taken: 15 March 2000 Photographer: Region III SATA Description: Cabinets 5 and 6 in the basement at the site.
Date Taken: 15 March 2000 Photographer: Region HI SATA Description: Container 2 containing chemicals.
ARIOOOU Photograph Log : ••' Hilltop Residential Lab Site Upper Darby, Delaware County, PA
Date Taken: 15 March 2000 Photographer: Region HI SATA Description: Interior northwest view of the basement laboratory at the site.
Date Taken: 15March2000 Photographer: Region IH SATA Description: View feeing northeast of the basement at the site.
ARiOOOIS Photograph Log Hilltop Residential Lab Site Upper Darby, Delaware County, PA
Date Taken: 15 March 2000 Photographer: Region III SATA Description: Interior northwest view of the debris filled room in the Hill basement.
Date Taken: 15 March 2000 Photographer: Region III SATA Description: View feeing south of the debris and equipment in the basement.
ARIOOOI6 Photograph Log Hi Itop Residential Lab Site Upper Darby, Delaware County, PA
Date Taken: 15 March 2000 Photographer: Region IE SATA Description: View feeing northwest of cabinet 5 in the basement.
Date Taken: 15 March 2000 Photographer: Region HI SATA Description: Drug Enforcement Agency warning posted on the door of the residence.
ARI 000 Photograph Log Hilltop Residential Lab Site Upper Darby, Delaware County, PA
Date Taken: 15 March 2000 Photographer: Region III SATA Description: Upper Darby Township notice of property condemnation posted on the door of the residence.
Date Taken: 15 March 2000 Photographer: Region HI SATA Description: SATA member inventorying chemicals in cabinet 2 in the basement.
ARIOOOI8 Photograph Log f) *• Hilltop Residential Lab Site Upper Darby, Delaware County, PA
Date Taken: 15 March 2000 Photographer: Region HI SAT A Description: West side of basement near stairway to outside entrance.
Date Taken: 15 March 2000 Photographer: Region m SATA Description: SATA members inventorying chemicals in cabinet 3 in the basement.
ARIOOOI9 Photograph Log Hilltop Residential Lab Site Upper Darby, Delaware County, PA
Date Taken: 15 March 2000 Photographer: Region HI SATA Description: SATA members inventorying chemicals in container 4 in the basement.
Date Taken: 15 March 2000 Photographer: Region III SATA Description: Chemicals in cabinet 5 in the basement
ARI00020 Pfc otograph Log Hi Itop Residential Lab Site Upper Darby, Delaware County, PA
Date Taken: 15 March 2000 Photographer: Region HI SAT A Description: Chemicals in cabinet 5 in the basement.
Date Taken: 15 March 2000 Photographer: Region HI SATA Description: Miscellaneous equipment and debris on the southern side of the basement. -
AR100021 Photograph Log Hilltop Residential Lab Site Upper Darby, Delaware County, PA
Date Taken: 15 March 2000 Photographer: Region m SATA Description: Chemicals in cabinet 7 on the western side of the basement.
ARI00022 Pfc otograph Log Hi hop Residential Lab Site U|iper Darby, Delaware County, PA
Date Taken: 15 March 2000 Photographer: Region III SAT A Description: Boxes 1 through 6 containing chemicals located on the western side of the basement.
Date Taken: 15 March 2000 Photographer: Region in SATA Description: Boxes 1 through 6 containing chemicals located on the western side of the basement.
AR100023 Photograph Log Hilltop Residential Lab Site Upper Darby, Delaware County, PA
Date Taken: 16 March 2000 Photographer: Region 01 SAT A Description: SATA member removing box 5 for from the west side of the basement for inventory.
ARI0002U Photograph Log Hi Itop Residential Lab Site U[ per Darby, Delaware County, PA
Date Taken: 15 March 2000 Photographer: Region HI SATA Description: Empty cabinet 5 on the western side of the basement.
Date Taken: 15 March 2000 Photographer: Region m SATA Description: Container 2 on the northeastern side of the basement after removal of chemicals.
ARI00025 Photograph Log Hilltop Residential Lab Site Upper Darby, Delaware County, PA
Date Taken: 16 March 2000 Photographer: Region IU SATA Description: Empty cabinets 5 and 6 on the western side of the basement.
ARI00026 Pb otograph Log Hi top Residential Lab Site Ujiper Darby, Delaware County, PA
Date Taken: 16March2000 Photographer: Region in SATA Description: Empty cabinet 7 on the western side of the basement.
ARI00027 Photograph Log Hilltop Residential Lab Site Upper Darby, Delaware County, PA
Date Taken: 16 March 2000 Photographer: Region ffl SATA Description: Empty cabinet 7 on the western side of the basement.
ARI00028 PI lotograph Log H Itop Residential Lab Site U per Darby, Delaware County, PA
Date Taken: 16 March 2000 Photographer: Region m SATA Description: Empty cabinet 6 on the western side of the basement.
ARI00029 Photograph Log Hilltop Residential Lab Site Upper Darby, Delaware County, PA
Date Taken: 15 March 2000 Photographer: Region HI SATA Description: Area 1 alter removal of chemicals in the basement.
ARI00030 PI iGtograph Log H (top Residential Lab Site Ui per Darby, Delaware County, PA
Date Taken: 16 March 2000 Photographer: Region HI SATA Description: Container 4 in the basement after removal of chemicals.
ARI0003I Photograph Log Hilltop Residential Lab Site Upper Darby, Delaware County, PA
Date Taken: 16 March 2000 Photographer: Region III SAT A Description: Container 1 in the basement after removal of chemicals.
ARI00032 Photograph Log Hilltop Residential Lab Site Ufiper Darby, Delaware County, PA
Date Taken: 16 March 2000 Photographer: Region m SATA Description: Drums filled with chemicals removed from the basement and temporarily staged in the backyard of the residence.
Date Taken: 17 March 2000 Photographer: Region m SATA , Description: t Drums filled with chemicals temporarily staged inthe backyard of the residence.
ARI00033 Photograph Log Hilltop Residential Lab Site Upper Darby, Delaware County, PA
Date Taken: 17 March 2000 Photographer: Region III SATA Description: 5-gallon can containing a mercury filled thermometer and other miscellaneous items removed from the basement laboratory.
Date Taken: 17 March 2000 Photographer: Region m SATA Description: Drums filled with chemicals removed from the she, staged in the backyard of the residence.
ARI00031* PI otograph Log H lltop Residential Lab Site U| >pcr Darby, Delaware County, PA
Date Taken: 23 March 2000 Photographer: Region HI SATA Description: 55-gallon drums containing chemicals opened for removal and segregation of noncompatible items.
Date Taken: 23 March 2000 Photographer: Region HI SATA Description: 55-gallon drums containing chemicals opened for removal and segregation of noncompatible items.
ARI00035 Photograph Log Hilltop Residential Lab Site Upper Darby, Delaware County, PA
Date Taken: 24 March 2000 Photographer: Region HI SATA Description: Drums and cans being labeled and marked for transportation and disposal
Date Taken: 24 March 2000 Photographer: Region ffl SATA Description: Drums property marked and labeled awaiting transportation and disposal
ARI00036 PI otograph Log w H lltop Residential Lab Site Upper Darby, Delaware County, PA
Date Taken: 24 March 2000 Photographer: Region ffl SATA Description: Labels on drums for transportation and disposal
Date Taken: 24 March 2000 Photographer: Region ffl SATA Description: Hazardous waste labels on drums awaiting transportation and disposal.
ARI00037 Photograph Log Hilltop Residential Lab Site Upper Darby, Delaware County, PA
Date Taken: 24 March 2000 Photographer: Region III SATA Description: Hazardous waste labels on drums awaiting transportation and disposal
Date Taken: 24 March 2000 Photographer: Region ffl SATA Description: Hazardous waste labels on drums awaiting transportation and disposal
ARI00038 Photograph Log Hil top Residential Lab Site Up er Darby, Delaware County, PA
Date Taken: 24 March 2000 Photographer: Region ffl SATA Description: Hazardous waste labels on drums awaiting transportation and and disposal.
Date Taken: 24 March 2000 Photographer: Region ffl SATA Description: Truck on site for transportation of drums and cans to disposal facility.
ARI00039 Photograph Log Hilltop Residential Lab Site Upper Darby, Delaware County, PA
Date Taken: 24 March 2000 Photographer: Region III SATA Description: Drums and cans loaded onto truck for transportation to disposal facility.
Date Taken: 24 March 2000 Photographer: Region ffl SATA Description: Drum staging area in backyard of residence following removal of drums for transportation to disposal facility. Pfc otograph Log Hi [top Residential Lab Site Upper Darby, Delaware County, PA
Date Taken: 24 March 2000 Photographer: Region IH SAT A Description: Drum staging area in backyard of residence following removal of drums and cans for transportation of drums to disposal facility.
Date Taken: 24 March 2000 Photographer: Region ffl SATA Description: View of driveway of residence following removal of drums to disposal facility.
ARIOOOM Attachment 2 SATA Chemical Inventory
ARIOOOtZ Hilltop Residential Lab Site SATA Chemical Inventory Area 1 Chemical Name Volume Oxygen bottle 50 pounds? Isopropyl alcohol 1oz Ethylene Glycol 1 liter Methylene Chloride empty Chloroform 10ml Sulfuric Acid empty Glycerin 1/2 gallon Chloroform empty
RRIOOOU3 Hilltop Residential Lab Site SATA Chemical Inventory Boxes 1,2,3,4,5,6 Chemical Name Volume , Box1 1 -2 elhanediyl sodium 5 grams 1,2 propane sultone 25 grams 2 - 6 - dimethylphenol 100 grams 2 - phenoxyethenol 100 grams 2 - phenyl - 2 - propanol 100 grams 2,4 - dinitrobenzolc acid 5 grams 2,4 - dinitrobenzolc acid 5 grams 2,4 - dinitrobenzoic acid 5 grams 2,4 - dinitrobenzoic acid 5 grams 3 - 5 - dimethylphenol 99% lOOjjrams 3-5 dinitrobenzoyl chloride 25 grams 4 - (phenylazo) diphenylamine 5 grams 4 - chtorobenzyl cyanide 100 grams 4 - fluoraniline 100 grams 4 - lodoaniline 98% 25 grams 4 - menthoxybenzyl alcohol 138 grams 4 - methoxyacetophene 100 grams 5 - methyl -2- nitrophenol 100 grams a - methyldnnamaldehyde 146.2 grams Acetyt acetone 4oz Acid sulfosallcyllc 1/4 Ib Anisole 100 grams Benzole chloride 99% 25ml Benzylamine 100 grams c - chtoroacetoplenone, 99% 100 grams Cinchonine alkaloid 50 grams Dimethyl fumarate 25 grams Ethyl acetate 1pint Ethyl benzoyl acetate 100 grams Hydrazine sulfate 100 grams Hydrazine sulfate 100 grams Hydrazine sulfate 1/4 Ib Hydrazine sulfate (crystalline) 100 grams Isopropenyl acetate 99% 100 grams Methylethyl ketone 500ml n - methylformlde 250ml nn - dimethyllndoaniline 1 gram o - anisidine 100 grams o - toluidlne 50 grams p - dimethoxybenzene 100 grams Phenethylamine 270ml Phenyl isocyanate 100 grams poly (ethyleneglycol) 500 grams Semi cartaazide hydrochloride 100 grams Tetra - n - butylammonlum 25 grams Tetra - n - propylammonlum iodide 20 grams retrabutylammonla fluorborate 50 grams Tetrabutylammonlum hydrogen sulfate 25 grams Tetraetnylammonium acetate tetrahydrate 25 grams Tetraphenyl arsonlum chloride 25 grams retrappentylammonia Iodine 25 grams
1014 ARIOOOblf Chemical Name _ #in**Volume Thianaphthene 97% 25 grams Triphenylarsine 97% 25 grams Box 2 15%theedon 20 grams 18k gold platkig solution 1qt Amberllte 1lb Amberiite 1lb Bath oil solution 250ml Dimethyl sllicone fluid 500ml Dimethyl silicons fluid 500ml Dow coming 200 fluid 300ml Florisil 200 grams Ion exchange resin ' 1tb Moth ball 10 oz Ocfoil 100ml Ocfoll 100ml P.M. 4.01 buffersolution empty ph 7.00 buffer solution 800ml Potassium chloride solution 25ml Sllcon oil 250ml Silica gel dessicant 1lb Type SA molecular sieve -their label 3lb Unnamed solid 2lb Box 3 (IKM-MO-camphoysuifuric acfcl ammonium salt 50 grams 2,2'-dibromo-p-xy!ene 100 grams 3,4-dlmethylbenzaldehyde 100 grams 3-lsopropylphenol 100 grams 4'Amnoacetanillde 100 grams 4-phenylphenol 100 grams 4-sec-butylphenol 2lb Benzaldehyde 250 grams Benzylamlne 100 grams Biphenyl 200 grams Ethyl dnnamate 500 grams Hydloxylamlne hydrochloride 1lb Hydroqulnone 1lb Laser dye - their label 500ml Malonatdehyde bls(dimethyl acetal) 100 grams m-Nltroanltlne 1lb n,n' - dlphenyl -1.4-phyenylene-diamlne 25 grams n.rKJImethylformamkte dimethyl acetal 100 grams n .n'-methyleneblsacrylamlde 100 grams p-hydroxybenzaldehyde 200 grams Poly (sodium p-styrenesulfonate) 20% 100 grams Propionlc anhydride 100 grams P-tululcacid 100 grams Tetra-n-propylammonium Iodide 30 grams Urea 1lb Box 4 1.2,4,5-benzene tetramlne tetrahydrochloride 5 grams 1,4-phenylene chiso cyanate 80 grams 1,5 - dlamlnonaphthalene 100 grams 2,5-diamlnotoluene sutfate . 100j[rams 2-4 6 - trlfuoroanlline • 1gram 3.4-dimethylanlline 50 grams
2 of 4 ARIOOOttS Chemical Name Volume 4 - lodoaniline 25 grams 414'-diaminostilbene-2,2'-dislfonicacid 200 grams 4-phenylazophenol 25 grams 7.7.8.8-teracyanoquinodimetthane 5 grams Acetic acid • sodium salt 300 grams B-trichloro borazole 25 grams Caco olylic acid 100 grams Carbomethyl cellulose sodium salt no volume Citric acid 100 grams Cytosine 1 gram D-sortitol 10 grams Gallium (III) acetylacetonate 25 grams Glycine ethyl ester 20 grams Guanidlne hyrdrochloride 1kg L-glutamic acid 200 grams Malachite green base 100 grams Merocyanine 540 1 gram Merocyanine 540 1 gram Morin 1lb Pentadecafluoro octanoic acid 25 grams Poly r- 478 5 grams Poly(ethylene glycol) 250 grams Poly(n-vinylcarbazole) 10 grams Polyethylene 25 grams p-terphenyl 5 grams p-terphenyl 25 grams q ulnallzarin 10 grams Sucdnic acid 300 grams Tetraethylammonlum perchlorate 10 grams Textra-n-butylammonium bromide 5 grams Textra-n-propylammonium iodide 20 grams Trans-stilbene 25 grams Triethylamine hydrochloride 200 grams Uracil 25 grams Urea 500 grams Variamlne blue RT salt 25 grams Box 5 4 ,4'-diami nodi phenyl a mine sulfate 100 grams 5-sulfosalicyllc acid dihydrate 300 grams bis-diphylphosphinoethane 200 grams Carbazole 100 grams Hexamethylene-tetramine 1kg Oxalic acid anydrate 100 grams Poly (acrylic acid) 25% 250 grams Poly(butylmethacrylate) 250 grams Poly(dimethylsllane) 100 grams Poly(ethyl methacrylate) 200 grams Poly(methyl methacrylate-co-ethyl acrylate) 25 grams Poly(sodlum 4-styrenesulfonate) 100 grams ResorcincH 500 grams Sodium methylarsenate 1lb Tetramethylammonium fluoride 20 grams Tetramethylammonium fluoride 20 grams Urea 500 grams Box 6 Activated carbon 1 1 tb
3of4 flRIOOOt*6 Chemical Name Volume Boiling stones 1lb CaSo4 1lb CaSo4 1lb CaSo4 100 grams Charcoal activated 2lb Desslcant 50 grams Filter aid(cellte) - their label 30 grams Liquid rare earth polishing compound no. 85 100ml Molecular sieve 3lb Molecular sieve 500 grams Molecular sieve 500 grams Molecular sieves 2lb Mortonsatt 200 grams Salt * 1lb Unnamed solid 1lb Zeolite 1lb
40M ARIOOOU Hilltop Residential Lab Site SATA Chemical Inventory Cabinet 3 Chemical Name (Volume Shelf A 1 - Brornonaphthalene - their label 20ml 2 Methoxyethanol 200ml 25% Glutaraldehyde 1/2 liter Acetanilide 250 grams Acetemide 1 pound Acetylcholine bromide 10 grams Acrytamide - 30 grams Adipic acid - their label 50 grams Amyl sal? - their label 50ml Aniline hydrochloride 1/2 liter Anisyl alcohol 50ml Anthranilic acid 25 grams Benzaldehyde 40ml Benzaldehyde 1/2 liter Benzanilide 100 grams Benzonic acid 500 grams Benzyl acetate 20ml Butanedial succinate - their label 50 grams Butyric acid 1 liter Butyrolacetone 300ml Caffeine - their label 50 grams Camphor 300 grams Chloroetone 30 grams Chlorohydrate - their label 100 gram Cincho? sulfate 20 grams Citric acid hydrous 16 oz Creosote 500ml Cyranuric add 25 grams Diethylene Glycol 200ml Dimethyl phthalate 1 liter Monochlorobenzehe - their label 100ml Myristic acid 10 grams n,n-Dimethyl formamide 1 liter n.n-Dimethyl formamide 1 liter n-Amyl ether 30ml Super concentrate revitalizer 20ml Unknown clear liquid 300ml Shelf B 1 ,3 Dimethyl • 2 - nitrobenzene 100 grams 1 ,5 Diphenyl carbohydroxide 50 grams 2 - Ethytaniline 200ml 2,4 Dlnitrophenylacetlc acid 50 grams 2,5 Dimethylpyrrote 25 grams 3 - methyl • 6 isopropyl - pyrocatechol - their label 100 grams 3 Ethoxy - 4- hydroxybenzaldehyda 100 grams 4 - Ethoxy 3 mehthoxybenzaldehyde 100 grams
10f4 ARIOOOt»8 Chemical Name Volume 50% DOT -their label 50 grams D • fructose - their label 100 grams D - glucose anhydrous 400 grams Dichlorobenzene , 400 grams Dichlorophenol 3ml Diethanolamine 1 liter Diethylphenylmalonate 100 grams Dimethyl sulfoxide - their label 50ml Dimethylamlne hydrochloride 50 grams Dodecyl sodium sulfate 25 grams EDTA - their Label 100 grams Elon (Developing Agent) their label 200 grams Ethyl 2 benzylacetoacetate 100 grams Ethyl bromide 1/2 liter Ethyt chloroacetate Iliter Ethylamlne hydrochloride - their label 30 grams Ethylene glycol 1/2 liter Ethylenediaminetetroacetlc acid 500 grams Formin 80 grams Fumaric acid 300 grams Glycerin 1 liter Glycerine - their label 50ml Glycerol Iliter Hydroquinone 500 grams lodoform N.F. 100 grams lactic acid 1/2 liter Lactose powder 50 grams m - Tolufc acid 500 grams Malonic add 100 grams Methyl salicylate 200ml n,n Diethylethylenediamine 25 grams n,n Diethylethylenediamine 25 grams trans 4 - hydroxystilbene 100 grams Shelf C l.phenylpyrole 100 grams 2 Methyl 1 propanol 1/2 liter 2 Nitrophenyl acetic add 50 grams 2 Phenoxylaniline 15 grams 2,4 Penanedlone - their label 200ml 3 Nitrosalicylic acid 100 grams Al icy lie acid 500 grams DL mandetic acid - their label 300 grams DL methyl benzyl alcohol 50ml Gelatin granular 1 pound Isopentyl alcohol • their label 200ml Malelc anhydride • their label 150 grams Malic acid 1 pound Menthol 200 grams Menthol -their label • \ 30ml menthysalacyclate - their label 30ml Mesltylene 5ml
2 Of 4 ARIOOOl*9 Chemical Name Volume Mesitylene 50ml Methyl benzoate 1 liter Methyl cinnamate - their label 30 grams Methyl salicylate - their label 150ml Methylanthranilate ' 1/2 liter Methylmandelate 50 grams Morpholine 1/2 liter n - methyjaniline 200ml n - methylsuccinimlde 10 grams n - propyl acetate 100 grams Naphthalene - their label 300 grams Napthol 100 grams Napthol beta 100 grams Nicotine 70ml Nithrophenol 100 grams Nitrolotri acetic acid 100 grams Nitron - their label 50 grams Nitroso-betanaphthol - Merck 4oz Octyl alcohol 1/2 liter Oil of peppermint 10 oz Oleic acid 1/2 liter Oxalic acid, dihyradrate (crystal) 500 grams Perfluorooctanoic 30 grams Phenethyl alcohol 200ml Phenyl hydrazine hydrochloride - their labels 50 grams Phenyl salicylate 10 grams Phenylethylamine - contaminated (their label) 30ml Phloroglucinol dihydrate 200 grams Proptonic anhydride 1/2 liter Pyrogallol 50 grams Toluic acid 60 grams Shelf D 1 ,2,4.5 tetramethylbenzene 100 grams 2,5 xylidine- their label 100ml 5 - phenyltetrazole 200 grams Add sulfanlllc 100 grams dibutyl phttialate 500ml m-trilylurea 50 grams p - phenytenediamine 100 grams p - toluenesulfonic acid 500 grams p - toluenesulfonic acid monohydrate 100 grams Phenol 300 grams Phenol phthalein 30 grams Phenol phthalein - their label 70 grams Phend phthalein 500 grams Phenylhydrazine 150ml Phthalic anhydride 500 grams Potyuinyl alcohol 200 grams Potassium acid phthalate 100 grams Propionic acid 1/2 liter Pthalic Anhydride -their label 200 grams
3of4 ARI00050 Chemical Name Volume Quinn sulfate 100 grams Resorcinal 100 grams Saccharin - their label 200 grams Salicylaldehyde - distilled - their label 1/2 liter Salicylic add - their label 50 grams Stearic acid - their label 200 grams Styrene oxide 100 grams Succinimide 100 grams Sucrose • their label 500 grams Syringic acid 25 grams Tartaric acid 500 grams Tetrabutyfammonium 25 grams Tetrabutylammonium percholate 100 grams Tetradecane 100ml Tetra-n-butylammonlum 50 grams Tetraphenylethylene - their label 15 grams Thiamine hydrodoride 200 grams Thioacetamide 100 grams Thioacetamide 50 grams Thiourea - their label 200 grams Thymol S.P. (crystals) - their label 200 grams Trichloroacetlc acid 200ml Triethanolamine 1/2 liter Triethanolamlne hydrochloride (their label) 100 grams Trimethylamlne hydrochloride 100 grams Triphenylmethanol 20 grams Triphenylmethanol 100 grams Triton X-100 - 1- octylphenoxpolyethoxyethanol 50ml Urea 50 grams
4014 ARI0005I Hilltop Residential Lab Site SATA Chemical Inventory Cabinet 5 Chemical Name Volume Shelf A Copper 5 grams Copper 100 grams Copper 1 1b Copper (1) iodide 250 grams Copper (II) acetate monohydrate 100 grams Copper (II) chloride dihydrate 50 grams Copper (II) oxide 5 grams Copper (II) sulfate pentahydrate 1lb Copper foil 2lb Copper metal - their label 1lb Copper metal - their label 1lb Copper sulfate 5lb Cupric acetate 1lb Cupric bromide 1lb Cupric chloride 1lb Cupric nitrate 50 grams Cupric nitrate trihydrate 100 grams Cupric oxide 1!b Cupric sulfate 20 grams Cuz(l)O 5 grams CyCO3 carbon carbonate - their label 1lb Ferric ammonium sulfate - their label 1lb Ferric chloride 6 - hydrate 200 grams Ferric sulfate 1lb Ferrous ammonium sulfate 500 grams Ferrous chloride 1lb Ferrous sulfate 7 - hydrate granular 500 grams Ferrous sulfide 5lb Gold dust 5 grams Iron (III) chloride hexahydrate 100 grams Iron (III) chloride hexahydrate 100 grams Iron (III) sulfate heptahydrate 300 grams Iron chloride - their label 200 grams Iron filings 500 grams Iron filings 2lb Lithium nitrate 1 1b Lithium nitrate 1 1b Lithium nitrate 1lb Steel acid open hearth 0.4% c 100 grams . Steel basic open hearth oil % 0,24c 50 grams Steel basic open hearth oil % c 1lb Steel manganese 1lb Unknown metal solid 5lb Shelf B Germanium dioxide 50 grams Germanium dioxide 1 gram 10f/ ARionnsi Chemical Name ->^ Volume - Germanium dioxide 1 gram Indium metal 5 grams lodic acid 100 grams lodic acid 100 grams lodic acid 100 grams Iodine - 1lb Iodine 100 grams Iodine 100 grams Iodine 200 grams Lanthanum chloride - hydrate 100 grams Lanthanum oxide 250 grams Lanthanum, oxide 100 grams Lead 1lb Lead acetate 1lb Lead acetate- 0.25m - their label 100ml Lead acetate trihydrate 1lb Lead carbonate 1lb Lead chloride 1lb Lead nitrate 1/2 Ib Lead nitrate 2lb Lead sulfide - their label 400 grams Lead wool - their label 1lb Lithium bromide 100 grams Lithium bromide anhydrous 500 grams Lithium carbonate/lithium perchlorchorate - their label 1lb Lithium chloride 1lb Lithium chloride 500 grams Lithium chloride 200 grams Lithium hexafluoroarsenate 1 gram Lithium hydroxide 300 grams Lithium hydroxide 1lb Lithium nitrate 1lb Lithium nitrate * their label 200 grams Lithium perchlorate 100 grams Lithium perchlorate anhydrous 200 grams lithium sulfate 1lb Mercuric acid 1lb Mercurious chloride 200 grams Mercurious toxlde - their label 300 grams Shelf C M? chloride - unknown 1lb Magnesium tlb Magnesium - their label 100 grams Magnesium - their label 150 grams Magnesium acetate 2oz Magnesium chloride 6 hydrate 100 grams Magnesium hydroxide 1lb Magnesium nitrate 1lb Magnesium oxide . 100 grams Magnesium oxide 100 grams Magnesium oxide - their label 20 grams
20f7 flRI00053 Chemical Name Volume - Magnesium sulfate 50 grams Magnesium sulfate 1lb Magnesium sulfate 1lb Magnesium sulfate anhydrous 100 grams Manganese chloride - their label 1/2 Ib Manganese (IU) oxide 100 grams Manganese dioxide 1/2 Ib Manganese dioxide 1lb Manganous carbonate lib Manganous Sulfate, monohydrate 1lb Mercuric acetate 1lb Mercuric Iodide 1lb Mercuric oxide 100 grams Mercuric oxide - their label 3 IDS Mercuric sulfate 1lb Mercuric sulfate 2 IDS Mercuric sulfide 100 grams Mercurous chloride 1lb Mercurous chloride 1lb Mercurous nitrate 50 grams Mercurous nitrate 50 grams Mercurous nitrate 20 grams Mercury 1lb Mercury II oxide 3lbs Mercury nitrate 100 grams Mercury oxycyanide 1lb Mercury pure 1lb Mercury sulfocyanate 20 grams Mercury sulfocyanate 50 grams mn AC2 - their label 50 grams Nickel (II) Sulfate hexahydrate 1lb Nickelous sulfate 6 hydrate 300 grams Unknown heavy liquid (poly bottle) mercury ? 10-20 Ib Unknown heavy liquid mercury ? 50ml Shelf 0 Moly bdenum Hexacarbonyl 20 grams Moly bdenum Metal 50 grams Moly BDIC Acid 85% 1lb Nickel 2 nitrate 1lb Nickel acetate tetrahydrate 100 grams Nickel chloride hexahydrate 20 grams Nickel perochloride hexahydrate 100 grams Nickelous carbonate 1lb Nickelous chlorate 1lb Potassium biphthalate 1lb Potassium bisulphate 1lb Potassium bisulphate 1lb Potassium bitartrate 1lb Potassium bromate 200 grams Potassium bromide 500 grams Potassium bromide 100 grams
30f7 ARI0005«4 Chemical Name Volume Potassium bromide 1lb ^J Potassium carbonate 500 grams Potassium chlorate 400 grams Potassium chlorate 300 grams Potassium chloride - their label 100 grams Potassium chromate 1lb Potassium chromate 1 1b Potassium cyanate 100 grams Potassium dichromate 1lb Potassium dichromate 200 grams Potassium dichromate 400 grams Potassium fern cyanide 500 grams Potassium ferric cyanide 500 grams Potassium ferricyanide 1lb Potassium ferrocyanide 1lb Potassium fluoride anhydrous 50 grams Potassium hydroxide 1lb Potassium Iodide 100 grams Potassium sodium 100 grams Silica 50% Iliter Tartrate Tetrahydrate 500 grams Shelf E Potassium ferric cyanide • their label 20 grams Potassium hydro oxide 45% 1/2 liter Potassium lodate lib Potassium lodate 100 grams Potassium lodate lOOjjrams Potassium iodide 200 grams Potassium iodide 500 grams Potassium meta-periodate 1lb Potassium nitrate 500 grams Potassium oxalate * their label 100 grams Potassium perliodate 10 grams Potassium permanganate 1lb Potassium phosphate monobasic 1 1b Potassium phosphate monobasic 25 grams Potassium sodium tartrate 50 grams Potassium sodium tartrate 100 grams Potassium thiocyanate 100 grams Potassium thiocyanate 1/2 Ib Potassium thiocyanate 500 grams Potassium tungstrate 20 grams Rubidium chloride 20 grams Rubidium chloride - their label 150 grams Selenium dioxide 100 grams Selenium IV oxide 100 grams Silicic add 1lb Silicic add 25 grams Silicon oxy hydride 100 grams Silver acetate 100 grams Silver acetate - their label 50 grams
40f7 ARI00055 Chemical Name Volume - Silver bromide 100 grams Silver chloride 50 grams Silver chloride 100 grams Silver chloride - their label 100 grams Silver chromate 100 grams Silver chromate 50 grams Silver cyanide 100 grams Silver cyanide 100 grams Silver nitrate 1oz Silver nitrate 1 gram Silver nitrate 100 grams Silver nitrate 100 grams Silver nitrate 100 grams Silver nitrate 100 grams Silver nitrate 20 grams Silver nitrate 50 grams Silver nitrate 50 grams Silver nitrate 25 grams Silver nitrate 20 grams Silver nitrate - their label 20 grams Silver sulfate 100 grams Silver sulfate 100 grams Silver sulfate 100 grams Soda and lime 1lb Sodium bisulphate monohydrate 100 grams Sodium Iodide 1lb Sodium perborate 1/2 Ib Sodium perborate - their label 100 grams Sodium thiocyanate 1lb Stannic iodide 50 grams Stannous Chloride 1lb Stannous Chloride 100 grams Tin . 1lb Tin II Chloride 100 grams Tin II Chloride 100 grams Tin IV Chloride pentahydrate 100 grams Tin metal sticks 2lbs Tin oxide 1lb Shelf F Bisodium hydrogen phosphate - their label 300 grams Sodium acetate 1/2 oz Sodium acetate 1lb Sodium acetate 1lb Sodium acetate • their label 1lb Sodium arsenite 50 grams Sodium bicarbonate 300 grams Sodium bicarbonate 1lb Sodium blsmuthate 1lb Sodium bismuthate 100 grams Sodium bismuthate 200 grams Sodium bisulfide 200 grams
50f7 ARI00056 Chemical Name Volume Sodium borate 1lb Sodium bromate 1lb Sodium bromide 5lbs Sodium bromide - their label 50 grams Sodium chlorate ' - 1lb Sodium chlorate 100 grams Sodium formate 1/2 Ib Sodium formate 100 grams Sodium hydro oxide - their label 1/2 Ib Sodium hypophosphate hydrate 1lb Sodium iodide 200 grams Sodium todkJe 1lb Sodium nitrate 1lb Sodium nitrate 1lb Sodium nitrate 1lb Sodium nitrate • their label 1lb Sodium perborate tetrahydrate 100 grams Sodium phosphate dibasic 1lb Sodium phosphate dibasic 1lb Sodium phosphate monobasic 1lb Sodium stannate 100 grams Sodium sulfate anhydrous 1lb Sodium sulflde. 500 grams Strontium bromide 1/2 Ib Strontium chloride 200 grams Strontium chloride 100 grams Strontium chloride hexahydrate 100 grams Strontium nitrate 1lb Strontium nitrate 1 1b Strontium nitrate 100 grams Strontium nitrate , 20 grams Zinc chloride 1lb Shelf O Sodium (no name) 20 grams Sodium bisulphate 1 Ib Sodium carbonate 1lb Sodium fluoride 500 grams Sodium formate 1/2 Ib Sodium moly bdate 1lb Sodium nitrate 1lb Sodium nitrate 200 grams Sodium perchlorate 400 grams Sodium phosphate tribaslc 1lb Sodium sitico fluoride 200 grams Sodium stannate IV trihydrate 100 grams Sodium sulfate - their label 150 grams Sodium sulftde 1lb Sodium Sulfide 200 grams Sodium sulfide - their label 1lb Sodium sulfide anhydrous 1lb Sodium tellurate 50 grams
60f7 ARJ00057 Chemical Name Volume - Sodium thtophosphate 50 grams Sodium thiosulfate 2lb Sodium thiosulfate 1lb Sodium vannadate 100 grams Sublimed sulfur 30 grams Sublimed sulfur 30 grams Sublimed sulfur 100 grams Sublimed sulfur 100 grams Sulfamic acid - their label 2lbs Sulfur 1/2 Ib Thallium nitrate 500 grams Titanium IV-oxlde 5 grams Tungsten hexocarbonyl 1 gram Vanadium III Chloride 1 gram Zinc 1lb Zinc 5lbs Zinc acetate 1lb Zinc acetate dihydrate 20 grams Zinc chloride 100 grams Zinc dust 1/2 Ib Zinc granular 1 1b Zinc nitrate 1lb Zinc oxide 1lb Zinc silicate 20 grams Zinc stearate- their label 100 grams Zinc sulfate 1lb
70f7 ARI00058 Hilltop Residential Lab Site SATA Chemical Inventory Cabinet 6 Chemical Name (Volume Shelf A Aluminum bromide 1 1b Aluminum chloride 300 grams Aluminum chloride 1lb Aluminum chloride - their label 200 grams Aluminum chloride - their label 100 grams Aluminum hydroxide 100 grams Aluminum metal 300 grams Aluminum oxide 2lbs Aluminum potassium sulfate 300 grams Aluminum powder - their label 400 grams Aluminum sulfide solution 20.6% 500ml Ammonium fluoride 300 grams Ammonium formate 1kg Ammonium perfsulfate 2.5kg Shelf B Adhesive remover 500ml Ammmonium molydate 300 grams Ammonium acetate 1/2 Ib Ammonium acetate 1 tb Ammonium carbonate 100 grams Ammonium chloride 1lb Ammonium chloride * their label 150 grams Ammonium dirchromate 1lb Ammonium dirchromate • their label 200 grams Ammonium dirchromate - their label 150 grams Ammonium nitrate 400 grams Ammonium persulfate 100 grams Ammonium phosphate 300 grams Ammonium potassium sulfate - their label 200 grams Ammonium sulfate 1lb Ammonium vannadate 100 grams Ammonium vannadate 300 grams Arsenic trioxide 300 grams Barium acetate 100 grams Barium chloride dihydrate 100 grams Barium nitrate 300 grams Shelf C Antimony - their label 100 grams Antimony - their label 2 IDS Antimony - their label 200 grams Antimony - trioxide 1lb Arsenic pure - their label 300 grams Arsenic trioxide 300 grams Arsenic trisulfuric - their label 100 grams Barium acetate 1lb Sarium acetate 1lb
1of3 AR100059 Chemical Name Volume Barium chloride 500 grams Barium dioxide 100 Ibs Barium hydro oxide 1lb Barium nitrate 1 1b Barium nitrate 300 grams Barium sulfide 1lb Calciurnhydro oxide 1lb Calcium oxide 1lb Paint and clear finish remover 300 grams Paint remover 200 grams Shelf D Bismuth metal 100 grams Bismuth metal 1lb Bismuth nitrate - their label 1lb Bismuth nitrate - their label 1lb Bismuth trioxide 1lb Boric acid 50 grams Boric acid 1lb Boric acid - their label 1lb Cadmium 200 grams Cadmium acetate dihydrate - their label 1 Ib Cadmium chloride 1lb Cadmium chloride 1lb Cadmium nitrate 1lb Cadmium sulfate 1lb Calcium 1lb Calcium 1oz Calcium carbonate 100 grams Calcium carbonate 1lb Calcium carbonate 1lb Calcium chloride dihydrate 20 grams Sodium hypochloride - their label 1lb Shetf E Calcium fluoride 100 grams Calcium hypochloride 1lb Calcium nitrate 1lb Calcium nitrate 1lb Calcium sulfate anhydrous 1lb Calcium sulfate anhydrous 1lb Ceric sulfate 50 grams Cesium acetate 25 grams Cesium chloride 50 grams Cesium iodide 25 grams Chloroplatinic acid 1 gram Chromium ammonia sulfate - their label 200 grams Chromium chloride 1lb Chromium chromlde 1lb Chromium metal 1oz Chromium potassium sulfate - their label 100 grams Chromium trioxide 1!b Chromium trioxide 1lb 2of3 ARIonnso Chemical Name Volume Chromium trioxide 100 grams Cobalt - their label 200 grams Cobalt chloride 1 Ib Cobalt nitrate 1 Ib Pink powder - no label on bottle 200 grams Shelf F Chromic 2 acetate - their label 1 1b Chromium nitrate 1 1b Chromium sutfate 1 lo Cobalt chloride 1 1b Cobalt nitrate 100 grams
3pf3 ARI0006I Hilltop Residential Lab Site SATA Chemical Inventory Cabinet 7 Chemical Name Volume Shelf A 10 - camphorsulfonic acid 60 grams Adipoyl chloride 100 grams Aniline - 2 - sulfonic acid 25 grams Antimony penta fluoride 100 grams Antimony trichloride solution - their label 100ml Benzene sulfbnyl chloride 40ml Benzene sulfonyl chloride 25 grams Bismuth trichloride solution - their label 100ml Hydrazine hydrate 1/2 liter Hydrazine hydrate 50ml p - toluenesulfonyl chloride 1kg Phosphoric acid 100 grams Phthaloyl chloride 300 grams Polyphosphoric acid 1 kg Sebacyl chloride 30ml Sodium nitroprusside 1lb Unnamed liquid - no label 20ml Unnamed liquid - no label - flammable 50ml White crystal - no label 1/2 Ib White powder - no label 1lb Shelf B Potassium cyanide 1/2 Ib Potassium cyanide 100 grams Potassium cyanide 1tb Potassium cyanide - their label 100 grams Sodium cyanide 100 grams Unnamed metal wool 1/2 Ib Unnamed solid 10 grams Unnamed solid 15 grams Unnamed solid 1lb Unnamed solid 200 grams Shelf C Chlorine water 300ml Copper sulfate solution - their label 100ml H2O2 solution 100ml Manganese - 2 - sulfate solution 200ml Offset fixer 1lb Potassium lodate solution 100 mi Sodium bisulfide 10 grams Sodium hydrazine 20 grams Unnamed solid 200 grams
10f1 ARI00062 » * Hilltop Residential Lab Site *•« 'W SATA Chemical Inventory Containers 1,2 4 - Chemical Name (Volume Container 1 Benzyl peroxide 40 grams Cinnemaldehyde 1/2 liter Diethyl pyrocarbonate 100ml Lead acetate 30 grams No label - clear liquid volume not legible Propylene carbonate 1/2 liter Propylene^oxide 1 liter Pyruvic acid 5 grams Pyruvic acid 25 grams Sassafrass (fragrance) 4-40 ml Tyramine 1 gram Container 2 Shelf A 1-Butanol 1 liter 1,4Dioxane 100ml Acetic Anhydride 1/2 liter Acetic Anhydride 1/2 liter Acetic Anhydride 1/2 liter Acetic Anhydride 100ml Acetonitrile 1 liter Acetonitrile 1 liter Acrylonltrile Iliter Ally Chloride Iliter Allylamine alcohol 200ml Amyl Acetate 1/2 liter Amyl Alcohol 1/2 liter Benzone 1 liter Benzyl Alcohol 1 liter Carbon Disulfide 1/2 liter Carbon Dlsutfide 1/2 liter Cydohexanol 1/2 liter Cydohexanol 1/2 liter Cydohexanone • 1/2 liter Cydohexanone Iliter Cydohexanone 1/2 liter Cyclohexylamine 150ml Cydohexanone 100ml Cydohexane 1/2 liter Cydohexanone .- Iliter Dimethyl Sulfoxide 100ml Dimethyl Sulfoxide 1/2 liter Dimethyl Sulfoxide 1 liter Dimethyl Sulfoxide Iliter Dioxane 1/2 liter isobutylamlne 1/2 liter Llgrone Iliter
10f3 AR 100063 Chemical Name Volume n-hexane 1 liter n-butyl bromide 1/2 liter n-methyl cyclohexyamine 100ml Shelf B 1 ,2 Dichloroethane 1/2 liter 2 Propanol 1/2 liter Bromobenzene 1 liter Bromobenzene 1 liter Cydohexanone 1/2 litre Dimethytsulfoxide 1/2 liter Ethyl acetate 1 liter Ethyl alcohol 35% sodium hydroxide (waste oil?) 1/2 liter Ethyl formate 1/2 liter Ethyl formate 1/2 liter Ethyl iodide 100ml Ethyl malonate 1/2 liter Ethylene dichloride 1/2 liter Formaldehyde solution 37% 1/2 liter Hexane 1/2 liter Isopropyl acetate 1/2 liter Methorcrylate 100ml Methy ethyl ketone 1 liter Methylmorpholine 1/2 liter Mono-bromobenzene 1/2 liter Nitrobenzene 1/2 liter Nitromethane 50ml Nitromethane 1/2 liter Pyradine 1/2 liter Pyradine 200ml Pyradine 1/2 liter Pyradine 1 liter Titanium isopropoxide 1/2 liter Toluene 1/2 liter Triethylamine 1/2 liter Xylene 1/2 liter Shelf C 2- Ethoxyethanol 1 gallon 95% Ethanol- Their Label 1_gallon Acetonitrile 1 gallon Benzene 2 liter Hexane 1 gallon n-propyi alcohol 1 gallon Xylene 1 gallon
RRI0006U Chemical Name (Volume Container #4 (on top of cabinet 3) Acetoacetanilide 200 grams Aminobenzoic 100 grams Aniline 1/2 liter Benzyl chloride -'their label 200ml Glutaric dialdehyde 1 liter Glycerol 1 liter Hydrofluosilicic acid 5ml Matonaldehyde bis(diethyl acetal) 100 grams o - acetoacetotoluidide 200 grams Pale pink powder - unknown 200 grams
3 of 3 ARI00065 Attachment 3 ERRS Chemical Inventory
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DATE: I/// PACKING MATERIAL:_l£:/i SIZE QUANTITY DESCRIPTION STATE TYPE OF CONTAINER EPA# IL fiwi'u* /P/ltl//** ^n//" jfeg7 fool O&i 1, /A M V/4 \J0ol 'K >*M& . 1/4 Ilk ARI00082 OHM CORPORATION _ - __ |'i " -* J J j ^ it A t^ A J 'f? "' " GENERATOR: *>£?% '£W III______DOT SHIPPING NAME: ADDRESS:______USEPAIDft fitDjcfiJ&lfr? HAZARD CLASS: UN/NA: PC- MANIFEST #:______' EPA #S: ______DRUM ;iZE:_£k_/_ DRUM#:JtM.ttr«V^ DATE: .1/u PACKING MATERIAL: i^ft/^ &RI00083 OHM CORPORATION /$6J? GENERATOR: \J&£rA ~ &*&* M/ DOT SHIPPING NAME: ADDRESS:______USEPA ID#: HAZARD CLASS: UN/NA: Pf MANIFEST #:______' EPA #S:. DRUM SlZEuSSoL- QRUM#:JZ/2M"<7J DATE: ?/U PACKING MATERIAL: SIZE QUANTITY DESCRIPTION STATE TYPE OF CONTAINER EPA# 6_i__ c UUf i-JL ** \tfojl ««6 f/Utf/b ffitaw/c rt'fr '"''•1 * * w g/i ARI0008I* OHM CORPORATION 'i.' ---''r'i GENERVTQR: USW1 ' frWW DOT SHIPPING NAME:. ADORE3S:______USEPA o#: /^qpr*py/rfj HAZARD CLASS:____ UN/NA: __ PG: MANIFEST #:______EPA tfS: DRUM DRUMftJZMl^J? DATE: ?/// PACKING MATERIAL:. SIZE QUANTITY DESCRIPTION STATE TYPE OF CONTAINER EPA# > * Ai/Arf o W* / Ji n A ^i' ARI00085 OHM CORPORATION GENERATOR: US£PA- £l/U/J7 DOT SHIPPING NAME: M/*j/< ADDRESS: USEPA ID#: nwrtmytts HAZARD CL^SS: ^. 1 UN/NA: V»IW Pfi- 17 " MANIFESTS: ' EPAtfS: "" '" DRUM SIZE: <_>«/ DRUMftL/Ml^y DATE: J*^ PACKING MATERIAL: A / 4/w A*A ' /A / J,V,_ HJtstt Altfrak. ''i /; A SoJ,\* fl/frol ™. / / /£l Afa. h-l'toL //A I I Ol&{ f/u*i /» ' /^/C /A / >jj . /^ 4 ^ 4^^ //A / 1 //t, / W/w ^)UA III 1 _.6*^Vi Ofo+vk. -jT -1"1' IM n 2 ^_* J llA.lh 1 /suhl nftwwi Afsfatyji Lft n * Sdtiu* jkUji blh n 3 fun* CM*. t/i 1 A fM;*. frfah- k/l> // 2 $Ji»<\ VJoruk %* 1 JUtto* ^'M u ,; L/4 /•/^ //;/^ fcsnuM &M a Ihlr / llh Ht J /14A/U4 '*'' ' */ i Ilk —— l/h / t.^/H.ij/i'Ai fWeJX'vt 'fa< -I/I, /; J* C_>_5_)i/y" /w»7'i//4 '1<>)I> j> y n/tei^ Af7w • &RIQ0086TK" / 2 OHM CORPORATION v<" & ** ++r *<"&• GENERATOR: vjPr'J' F-*K> ffW>f DOT SHIPPING NAME: ADDRESS:______" _ USEPA D#: PWPr£W /Vte HAZARD CLASS:_____ UN/NA: ____ PG: MANIFEST #:______EPA ffS:. DRUM IZE:./^fi DRUM ft £/^*»V DATE: ?/^ PACKING MATERIAL;. SIZE QUANTITY DESCRIPTION STATE TYPE OF CONTAINER EPA # lih JUit (__5',r/n/_f._x* J •'. /Vfi'Af'i*v. Pfff / n /A ink** Cv>* /.L W ^£1 ARI00087 OHM CORPORATION GENERATOR: r ' /M______DOT SHIPPING NAME: ADDRESS: ______USEPAIDfr fyP$P0flF'7ttf HAZARD CLASS: 2 UN/NA: UWW MANIFEST ft ______' EPA tfS: DRUM SIZE:7fr7T DRUM ft 1/01/^3 DATE: S//7 PACKING MATERIAL: SIZE QUANTITY DESCRIPTIOS! N STATE TYPE OF CONTAINER EPA# 2^L Ufa* 0001 2^. if i «* tUb* ywyK j --^ &/&* # fy/ Afr* U (u-IfL A-bui to** to/ ,f^ , J'/y^ \tIQ\ $**! " * 41 I/J/J *: /y/y^^». VyM« V££ ^fi; 1rtlt to* d'fr,. ,0/V AR100089 _ OHM CORPORATION GENERATOR: lA£l* & /______t)OT SHIPPING NAME: ADDRESS: -^x— USEPA ID#: tt»£t dfa WT HAZARD CLASS: UN/NA: PG: MANIFESTO ' EPAtfS: DRUM SIZE: i'CW DRUM ft VM/Wf DATE: J/M PACKING MATERIAL: W* SIZE QUANTITY DESCRIPTION STATE TYPE OF CONTAINER EPA# tytttol V / i, i ___ __hnL — pl — — ^_6l,-tJttj — ^_. ————————————— -^fai- / ftr^/" ^'' -J4i_J / A)/,/ A/^/ too/ J^_ _J_ /.w^ /4^/y 9dt — / —— hd»*l U/ff \ ^ •^ - x flRI00090 J •' fcl*fA OHM CORPORATION GENEF ATOR: Vf£M'£//Uj& - hOT SHIPPING NAME: S/cM /,>„// ADORESS: ^/*<,4| A^c ^ USEPA ID#: PtfmfcWf HAZARD CLASS:_1/ ; UN/NA: UA'^V Pf5- ffT MANIFI ST #• ' EPA #"S' " ' DRUM 3IZE:J^t7 DRUMft^MV^ DATE: .?//7A, PACKING MATERIAL: Wn TZWMr SIZE DESCRIPTION STATE TYPE OF CONTAINER EPA# Ift / JViV-fl fxjhU- v 7 7/yArty tiuiM, V. / |J//wM*y ^»tm •-•i «ftf > ii oi */);^rt/ /)^uJ \ibi 1* — /— :f -AM,;j - V'f^Jt W r-« *• / ^tt- ^l^lif^t^^tf 0<«;f %; jiw-i— fyfatk. .{i/^vA 4 / ft twtoQuh j\fy*JK- v^± / Ifa hvfyl 0*nMw tmwtto - PHfAtlL <4/Mw*A / ^ta^A ^''/ Vtfl ^it / ^^/ wtr V, / ^;i*«- fao %t / CAIwfaiyl tytftt - %b / ///^f/4t bur Vo , i Wny/ liKyaak // I i PLj viw " S*t % i rlufffo ffttlht. —^ ' i Mtrifau* v/or ' -* / —— • |faUq ' '"W rtiilH y 'c — ^ ——————— — 4 / /Vht \IM - % t j Mai;\i», fa;\'0 Drvuti<. ARI0009I toti OHM CORPORATION GENERATOR: l/J/W f-fKi IH DOT SHIPPING NAME: W - ^~^ ^ ARIOOUy.•fc /\ r:t — Sj , OHM CORPORATION ^ GENERATOR: 1/5/A* ' £fl& Iff DOT SHIPPING NAME ADDRESS:______USEPA ID#: ri9W0x> srrj , HAZARD CLASS: MANIFEST #:______EPA tfS: l——,.„—_____„ DRUM !>IZE:^i____ DRUM#:_l^fl.y7 DATE: .3JU* PACKING MATERIAL:. SIZE QUANTITY DESCRIPTION STATE TYPE OF CONTAINER EPA # vffj'Mift'l Dofa faol Owl » fitoi In i, -2 & Sl ?V At/./ I tU. / 3 ///1 />« in f*/ #**>! /\L fool tool Mf**l*L L\L C.!»lt M/J ______I ARI00093 b OHM CORPORATION GENERATOR: WfcrH 'pKui fff______OOT SHIPPING NAME:. ______ADDRESS:______USEPA ID#: fMltft , HAZARD CLASS: / UN/NA: MANIFEST #•______EPA tfS: DRUM SIZE: /^/ DRUM #: ij0Att~0y DATE:_2Z^Z__PACKING MATERIAL: SIZE QUANTITY DESCRIPTION STATE TYPE OF CONTAINER v J/i *'&*. MJ Oc/i? lei- bl foftk Sol* „, 3 J¥L- wt him A*/ <^/t/- sd ^ei?^/ ^ , OHM CORPORATION, .e GENERATOR: £*& W_____ DOT SHIPPING NAME: ADDRESS:______USEPA ID#: WW&00W>. HAZARD CLASS: UN/NA: PG: MANIFEST#: EPAtfS: DRUM;SIZE: JB<*/Mi DRUM* l/A!#Vp DATE: PACKING MATERIAL- • f flRIOOOSS ft OHM CORPORATION GENERATOR: fl' /ff DOT SHIPPING NAME: ADDRESS: USEPA ID# MlfPWO IttS , HAZARD CLASS:_Ir UN/NA: l/^ji)^ PG:_2£_ MANIFEST #• EPA #S: DRUM SIZE--• jtf,,/.,. DRUM*: \jftft •*) h/k 1 /I ltJ*l tfVtf Ir \fltA}Xfir t MH Ilk 1 C/^/^ ^/Wc A/M fall / fvfasfa H^xm vM I t Iff • 1 /k> ///> 1 hit* 1 --V_7/V*i IrfWXifa Mn ///, 1 f '/tfi^-( Chltf'!/* M Iff n ^ ^-^tlant3[\fi #i**t ^p&t^J Iff / IhtfiLlvtot. WFMi .- "^ ARI00096 f* OHM CORPORATION GENERA FOR: \IS£wf£Ukw DOT SHIPPING NAME: We A^ ^yA/, ADDRES • USEPAII #: fWWWMA HAZARD CLASS: ^ UN/NA:V/Wyj~ PG- MANIFE£ T"fc ' EPAtfS: DRUM SI E: /^«/ DRUMtf: UtM'l/ DATE: PACKING MATERIAL: &*rW*S SIZE QUANTITY DESCRIPTIO**-**'**" "'""•N STATE TYPE OF CONTAINER EPA# ' ^f J/ __ /fjA /4^/,/C to*t.i*>*> • •A - t . . - ; . ._ . *_ . .-, *- - . ' , ' I AR 100097 OHM CORPORATION GENERATOR: U&M "£$&$______DOT SHIPPING NAME: 1 \ , A '"^ s ARI00098 OHM CORPORATION t> GENERATOR: \fSfrA' fct&lfl______DOT SHIPPING NAME:. ^ 'ADDRESS:______USEPA ID*: n»&W& /?& , HAZARD CLASS: P UN/NA- l/#*0 PG- yT MANIFEST #: EPAtfS: DRUM iSIZE•: jta - i • . • ARI00099 : — r OHM CORPORATION GENERATOR: l/*£/4 "/'l& )1T______DOT SHIPPING NAME: UW< /%g ' HSEPA 1P«: jtJS 1000 3MT. HAZARD CLASS: f UN/NA: MANIFEST #:______. . „. . EPA DRUM SIZE: _ DRUM tUt' DATE: ______PACKING MATERIAL: SIZE QUANTITY DESCRIPTION STATE TYPE OF CONTAINER EPA# Klb / /•'V-^ flbwy Uisi HM1? flvwy Ulfl -44iL- m 2 — ~TT —— l ——— f ———————————— kjj. ——I—— /Arf/iM*//- tt*\&i*\ hfr^ I//// ~* 1 ^ \ N"g' • x^' f ARIOOIOO OHM CORPORATION GENEF ATOR: lUfP" "£wffl DOT SHIPPING NAME: \M*k A • *>/»/ // £ AuKI (J^vtiL till to**» I VM6 v - • ...... '.... . ;...... *~. t ' .'.. . . . ,. . . ' • . ..',...... • . - -- . . f X1 • i •• -l. AR 100 101 OHM CORPORATION GENERATOR: w'______DOT SHIPPING NAME: ADDRESS: USEPA ID# Yf\0ffatf 1ttS , HAZARD CL ^SS: 6./ UN/NA: UA/)tl/PG: fl MANIFEST g. EPA #*S' DRUM SIZE:: W DRUMS: \JtfW DATE: 3 //I PACKING MATERIAL: !/?/•» SIZE QUANTITY DESCRIPTION STATE TYPE OF CONTAINER EPA# fol / A \ •. _ > . M' f ARIOOIO 2 OHM CORPORATION GENERATOR: UWW'PWML______DOT SHIPPING NAME: ADDRESS:______.._ USEPA 1b*: YflPftstf Htl ' HAZARD CLASS:_J^L_ UN/NA: J/vJ/tf PG G ~ MANIFEBT #: - EPAff'S: DRUMSIZIE: 5«*y DRUM#: UWJHf DATE: llrt PACKING MATERIAL: Vtfi SIZE QUANTITY (DESCRIPTION STATE TYPE OF CONTAINER EPA# r • fa* J b y itoUjI Ptfofh Ab/ s y*. '' 1- h- -- AR 100 103 1 r- \ Attachment 4 Transportation and Disposal Documentation ARIOOIOli -'- *{,. State of New Jersey Department of Environmental Protection Hazardous Waste Regulation Program •' Manifest Section P.O. Box 421, Trenton, NJ 08625-0421 Pom Appro**!. OMB No. 206&4O39. UNIFORM HAZARDOUS MonnBtion In the ihedetflwe* WASTE MANIFEST It not required by Federal Jtw. f fling Addrese* ttiHAiriPitiA, m war 4. GeneratofiPhone(<71 *M *M<- MIH 'f II S. Trancp MftflU TOXIC K* Ift^WMMNIC HOB 10004 DOCO O ?/^•__.^..»^__i_ "^I L".-- .^*«ai» _-.**. i JftL'-,,"1 - *%«m-Ak#r' _- *^-"-^ ^g^MB>tiH!iS^.^fejjg(y^^ b'oortilbAnant tniKily i^AXWwWy' tfncrtmT above 6/piW:«>Jpf*itrnah*and eniH Kffik3<)jwtr5n^tohjahw>»to<^*i^^ ITt^rtdu^^^^^ffi^^^^^S^MS^M tafvo^a^tcnaSf tf futft ^areleiLli^^MT^^ ^ rJ^-j^^ ^ •*w •«-*-.-••/• CycteChem, Inc. ___ Recycling, Treatment & Disposal of Hazardous Waste 217 South First Street Elizabeth, N3 07206 * 908-355-580$ Fax (908) 355-0562 LAND DISPOSAL RJESTRICT7ON NOTIFICATION AND CERnFICATION FORM werator Name: werator EPA ID #: ______anifestf: /V / /*/ ^s*tt & /^ j r£r /anrf disposal restriction (LDR) notification must o* submitted with tfio initial shipment of all new waste reams. Dua to revised LDR notification requirements effective after August 23, 199$, previously approved aste streams witt require re-notification on this form with the first shipment after that date. Subsequent TtiRcation Is not required unless the waste stream changes. ) WASH! STREAM INFORMATION Box As Check this box if this LDR certification has been supplied with a previous shipment Additional Information and certification Is not required on this form. y* •-. •. Box Bs Indicate if waste stream Is a wastewater (WW) or non-wastewater (NWW) (aqueous waste streams containing < 19* total organic carton fJOC) and < IK total suspended solids (TS$} are wastewaters. Aff otherstream s are non-wastewaters). Box CsUstaO&A waste codes and subcategory reference letters (if appffcato reference addtttonai pages (e.g. profiles or tab pack slips) containing required Information. B Una Pnrioustf shipped NWW/WW £PA Waste Codes and tubatagor/refereoee letter (ffapfOcable) LDRonOe tbcategory Reference £e&5n/t£R3 cotes'n&fisl&f here do noti&vesubcategoiles) OOOl DOOM DOO3 0003 0003 Water reaiMvm subcategorr OOO3 Other /e-KfA* subotagor ooot Cidmfutii non-battery DOO6 Cadmium containing batterfoi tubcateoorv 0003 L 0009 L rtirf add butteries tubcateyonr 0009 DOO9 mtegorf (>26O PPM To& Mercury) 0009 Low mercury *ubc*taoorrf< 26O PPM Total Mercury) 0009 Mercury ARI0010& SPENT SOLVENT WASTE CONSTITUENTS Ore/a 4 ppffcab/e waste code(s) and constftuentfs) for each manifest Hoe Item containing EPA spent solvent waste codes rOOl-FOOS. > fr .& \J A* CD, JFOOl A BCD___fOO2 A BCD___FOO3 A BCD___fOO4 ABCD fOOS A BCD. .NK0AMM A BCD______-mthyf ether A 8 CD. .•AOTMM A B CD______-methsnol A BCD. ,-H-butyl mlcofiol / ABCD______-otethytene ctiforitf* A BCD. .4to4utytalcohol A B CD______-mtitfiyf mtfiyf tetone A BCD. .-carfwfl disuttide A B CD______-methyl ttotoityt ketone ABCD______-ctrkon tetnchhride ABCD______-a/trafr A B CD______fiilorob4nzene A B CD ABCD'______-m-cm»o/ ABCD______~t*tnd)loroethyt*ne ABCD. ,-9-€nsol ABCD______-to/uene ABCD. ABCD ABCD. .-cretytic adtt A B CD ABCD. ABCD ABCD. A BCD ______•McMommoaoffaommet&Mae ABCD. ,-ethyi mcetate A B CD ______-l,lJ-trlcMorQ-lJ,2,-tr111uQroett}*n* ABCD. .itttyf benzene ABCD______-xyfenes UNDERLYING HAZARDOUS CONSTITUENTS for characteristically hazardous waste streams (EPA codes DOO1-DO43), phase Sst aff underlying hazardous constituents as defined In 4O CFK 268(2)Q) that are present at concentrations exceeding the universal treatment atandaids Ssted m 4O CFR 268.48 (FQM-FOO5 constituent U-,P-,undDO04~DO43 codes &sted to Secti HOWMSTTHESE WASTE STREAMS BE MANAGED? Foreacti manifest tine ten drde appScable teatmentf&jutzment Far contarnrxted sot}, drdeapp&abfe choice as Mfated. C/ """" ' . This Is an EPA hazardous waste Ihatki^ a o^tamlratedsoS or hazardous c^tris. Waste must be treated to the vent standard satorftti 40 CFRsubpartDftt to land ABCD. Jtfe Is a hazardojs waste contaminated soff.Th&cortta^^ hazardous wastes and doees/does s not (Mm)exhbRtchaivcterttcf hazardous waste and Is subject to/compffes wftfr t***** the tott treatment stano^n^as provided by 268,49(c) or the u^versattreatn^ ABCD. .This Is an EPA hazardous waste that meets a8 applicable treatment standards set fcrth In 40&R268sutpartDi and can be bndfiaed without further treatment I certify uno&per^ of law that I have persoralty examined and am HamOiar wOh the waste througti analysts and tEst^crthorouo^tsiowfedg^c^ the waste to s^cftt^ certiftotto that the waste ccni^ with the treato^ appB&leprohMiorB set torthh 40 CHt 268.32 crRCRAS^ Mu&g theposs&IXyoft One andtoprtson f} CERTIFICATION / X '!j 'eB associated documents Is comphto end accurate to the best of my * Suited Name: f ^Y ARIOOI07 ...... Stale ol New Jersey Y^^ Departmenmentt o off Ekivtraunenta EnvironmentaCl Protection;^ ,; • *. Hazardous Waste Regulation Program * Manifest Section P.OvBox ^Trenton, NJ 08625-0421 ' Pleeee type of prtrt -i btocfc letter*. (Form deelgned for ue» on eOte <12^lteh) typewrHer.fr . ArmApp/ovwL OAW Wa 205tKJO». UNIFORM HAZARDOUS i. uenenuori us tr*A iu NO, hiformatton In the shaded area* WASTE MANIFEST ri d d ri H 1 tj ri ^3! pl^ j i not required by Federal '• • 5. Transporter 1 pornpany Name 6. US EPA ID Number I ri .i A «i «i rt ^fTO*HS* r^wSaeHk^, I.IOUIII M O.9 Fi^nas^^^j^ P^^-^RB^I^^^^ - 1>C CycteChem, Inc. Recycling, Treatment & Disposal of Hazardous Waste 217 Stoith First Street, Etizabeffi, NJ07$06£ 908-355-5800, Fax (908) 355-0562 ND DISPOSAL RESTRICTION NOTIFICATION AND CERTIFICATION FORM mentor Name; '' / —* - 'EPklD*:* / ! tte land disposal restriction (LDR) notification must be submitted with the Initial shipment of all new waste reams. Due to revised LDR not**ication requirements effective after August 23, 1998, previously approved aste streams will require re-notification on this form with the first shipment after that date. Subsequent tiff/cation Is not required unless the waste stream changes. •STREAM INFORMATION Box A: Check this box If this WR certification has been supplied with a previous shipment Additional Information and certification Is not required on this form. BoxB: Indicate If waste stream Is a wastewater (WW) or non-wastewater (NWW) (aqueous waste streams containing <196 total organic carbon (TOC) and < W> total suspended solids (TSS) are wastewaters. All other streams are non-wastewaters). BoxdUstattEPA waste codes and subcategory reference letters (It'applicable). Alternatively, attach and reference additional pages (e.g. profiles orlabpacksffps) containing required Information. Une Prevtoiisty shipped NWW/WW £PA Wafta Codes 9J^subcateg<)rY reference letter Of oppli^ble) B C D tbcategoryl\eference Letters (EPA codes not listed here do not have subcategorfes) DOOl A tgnftable characteristic wastes, except high TOCIgnftabteBaufdssvbcateaory DOOl B fttah TOCO ZO°*)kmftabhli<]ttfdsubcategory 0003 A Reactive tutfde gubcategonr 0003 B Reactive cyanide subcateoory 0003 C Water reactive fubcateootY OO03 0 Other reactive fubcateoorv- 0006 A Cadmium not+fotterytubcategory 0006 B Cadmium containing batteries tubcateoory O008 A Lead non-battery tubcatooory OO08 B Lead add batteries subcateoory O009 A Hf ARIOOI09 SPENT SOLVENT WAST* CONSTITUENTS Cirdu applicable waste codefs) and constituents) for each manifest line item containing EPA spent solvent waste codes F001-FOO5. ABCD_____FOOt *aC0____«W-» ABCQ__2.FOO3 ABCD_____FOO4 ABCD______FOOS A B CD______-JcaftMM A B CD______-etftyf ttfier A B CD______-benzettm A B CD______-metfano/ ABCD______-n-imtyt alcohol ABCD______-methyla* cMorUa A B CD______-iso-butylalcohol A B CD______-mothy* eth#ketonm ABCD______-CMfbom disuifid* ABCD______-methyl isobutrl keton* A B CD.____ -carbon tetntcMoridm A B CD.______-nitrobenzon* A B CD______-chlorobcmene A B CD______-pyridln» A B CD______-nt-crtaol A B CD______-totradttoroethyfone A B CD______-o-cresol A B CD______-toiuen* ABCD______-fi-cntof ABCD______-i^^'MehtoroeUtana ABCD______-cnsyOcadd ABCD______-Iflf2~trifhloroatltaaa ABCD.______-cydohexinon* ABCD, ABCD______-o^flefc/araftaffiaae ABCD.______-trichtoromanoffuoromtOtM* A B CD ______-ftftyffcetMtf A B CD A B CD _____ '*afl benzene A B CD ______-xytene* ) UNDERLYING HAZARDOUS CONSnWENTS For cnaractertstfca/fy hazardous waste streams (SPA codes DOO1-D043), pleas* list aff underlying hazardous constituents at defined In 40 CFR 268(2)0) -&-* are present at concentrations exceeding tfto universal treatment standard Bsted In 40 OK 263.43 (FOO1-FOQ5 constituents ktotfo U-, P-, and DOO4-DQ43 codes listed in Section (1) do not need to be lifted In this section). / _____ . / _____ ; ______t-^None Present None Present HOW MUST THEStWASTZ STREAMS BK MANAGED? For each manifest One fern dBncfa applicable tmaui&j0cqutement ForcontsmftatcdsoU drct* applicable choice as indicated. ABCD ____ This waste to non^ardousp&Wtt 261, and b not rzstrk^ to an EPA hazardous waste that SnM a contamteted set crhaza Waste must be treated to the appropriate treatment standard set forth h 40 CrKsubpartD prior to lard Osposal. ABCD ______Thfs is M hazardous deM$ and is s^ject to the alterrat^t^^ ABCD ____ This Is a hazardous wastocontatitiiatsdsoB. This ccntamteted sot dote/does rrt(^^contah listed hazardous wastes and does/does not (^^e&ii&9charactalsac of hazardous wasted to subject to/compGeswtth (M^ fast* treatment standards as prodded br26&^ standards. ABCD ____ This Is an EPA hazardous yiaste that meeti at appBcabtetrea^^ andean be landfiBod without furtr& treatment I certify under pcr^ of law that I have per^^ am fam^ with the waste through analysis artftestog or ttor^^ cartfitoflfcn that the waste comptfes with the treatment standards specified h 40 O^fW 268 SutspartDar^ appBcableprrttfttos& forth hWCFR 268.32 or RCRASec^ suMtttf to two, accurate and coi&ets. I am aware that t^^ S) CERTIFICATION assocto it** ARIOOIIO :>-.••.. State of New Jersey,. .:>• Department of Environmental Protection ,. .. Hazardous Waste Regulation Program" ' Manifest Section** - J ' * -:'•; P.O. Box 421, Trenton, NJ 08625-0421 Pleeae type or print rn block to««f^ 4. Generator-t Phone( f?inv flt* Transporert Company Name Tranaporer 2 Company Name 8, US EPA ID Number I I I I I I t I I I I I 9. Designated FacAty Name and Site Addreea c*var acn IMC , J 717 GttVW flRBT fit n 12. Containenv I •. * 13», 11. USDOTO&r1ptf{*(>MftJdtyAt)p^ , • jToW . IDNi*ntMftndf>*XingQft>tJp)f • No. Type - Quantity-. It L1UHR MVSIC , INfI«VtfWC H O B 00071 4fl> ''F'i't »' i •'".,»'• ''""''' *f , ... " 2-i> '*(* • - -. • * 1^it«ti4r)t:- * •*, • . \k- '.' . • " ..••••.' • - * f* ..* . •* - • ^T1 »»*•)" - i. -«• • FlflrtlABlf UQU^TOVtO MO t * ifw«%; ^IrT'* -"-01. *• -^j*-^-*- '^ :,' ^A ARIOOIII [I. CycleChem, Inc. ______Recycling, Treatment & Disposal of Hazardous Waste 217 South First Street, Elizabeth, W 07206 * 908-355-5800, Fax (908) 355-0562 LAND DISPOSAL RESTRICTION NOTIFICATION AND CERTIFICATION FORM '•eneratorName: _ 'eneratorEPA ID #; _ fan/fest #; ______ »jfc ^/rrf disposal restriction (LDR) notification must be submitted with the Initial shipment of all new waste treams. Due to revised LDR notification requirements effective after August 23, 1998, previously approveo tasta streams wiff require re-notification on this form with the first shipment after that date. Subsequent -otfflcatton Is not required unless the waste stream changes. t) WASTE STREAM INFORMATION Box A: f^ecM this box if this LDR certification has been supplied with a previous shipment Additional Information and certification la not required on this form. Box B: indicate & waste stream Is a wastewater (WW) or non-wastewater (NWW) (aqueous waste streams containing < l*ft total organic carbon (TOC) and < l*ft total suspended solids (TSS) art wastewaters. Aff other streams are non-wastewaters). BoxCs UstattEPA wastecodesandsubcategory'reference letters(it'applicable}. Alternatively, attach-no reference additional pages (e.g. profiles or lab pack slips) containing required Information. •ubcategory Reference Letters (EPA codes not listed here do not have subcategoHes) DOOM A TonftiMcAArzvferirtfcH^ DOOM B HkATOC(>lO ARIOOII2 SPENT SOL VENT WASTE CONSTITUENTS Orcte applicable waste code(s) and constituents) for each manifest line item containing EPA spent solvent waste "i.'••••'< ' «.•,.:. A 8 CD. A B CD_____fOO2 A B CD___«WJ A B CD fOO4 ABC D___FOO5 A BCD. .-ecetone ABCD______-ethyl ether ABCD. •oonzene A B CO_ ABCD. .-a-buttf alcohol . ABCD_ ABCD. Jio-outyt alcohol ABCD______inethyt ethyf tetooe ABCD. .-carbon duuffide ABCD.______-methyl itobutyt ketooc ABCD. .•carbon tetrachlorlde ABCD,______-altrobojuone ABCD. .-ch/orobenrene A B CD ______•pyrtdfne ABCD. ot AB CD ABCD. ,-o-cresot ABCD______-toluene ABCD. ,-p-tnsof ABCD______-J,_U,--*-AAvwf-A«/j« ABCD. .-cretyticocld A B CXL.______-I,lj-tr1dilon>ethsne ABCD. .'Cydohexanone ABCD______-trfchhroethyfene ABCD. ABCD ABCD. .-ethyl acetate ABCD ABCD. .•ethyl benzene A B CD.______-jrytenes 3) UNDERLYING HAZARDOUS CONSTITUENTS For characteristically hazardous waste streams (EPA codes DQO1-DO43), please Kst aff underlying hazardous constituents as defined In 4O CfR 268(2)@) that are present at concentrations exceeding the universal treatment stands rds isted to 4O CFR 268.48 (FQQ1-F005 constituents Identified to f**tton (2) *Jid sjiee^ fSNon•^"*-e Presen~t \ None Present ~T None Present USNone Present HOW MUSTWESE WASTE STREAMS BE MANAGED? For esci manifest tine tern, drctoaFpfk&tetestmentfequJrementForm ABCD____Thk¥^stelsnon-ha^rdou$pGr40CFR261fandkr^restict^ _Th£banEPAhazaTtowa$tethatlsrKtaeQntantinated Waste must be treated to the appropriate treatment standard s& forth h 40 CrKs&partD pier to land ttisposal. ABCt______Th& is* hazards ctettarti is ttt)jea to the atemattetre^^ ABCC____This to* hazardous waste contaminated soB. This coTtimhated soil tbes/ches not (M™>corteft isttf hazardous wastes and does/doesJw*^"^«dfcW*rtaracte6atofto to/compBeswIth (Mm> the soatreatmert standards as protfded by 268.49(c)c^ standards. . ABCC.______Th& to an EPA hazardous waste that meets an appBcabtetrcatmert standard arri can be lancffiBed without falher treatment I certify uriderpena^ of law that I have personally examined and certftotto that the waste complies wtih the trea^ apptk&lepTVh&tto set 1brlh In W CFR 268.32 crRW sutm/ttecf 6 tv$ accurate ajtfccnip^fm CERTIFICATION raffassoctot*cfctocunmtslscompkteendaccw*tetothetesttf fl?IOOII3 , State of NeW'Jersey * - ^DepartnMntof Ernrlrorttnerrtar Protection, .: -. «-•'.' Hazardous Wast* Regulation Program ' * Manifest Section P.O. Box 421, Trenton, NJ 086254421 Pleaee type or print hi Woe* latter*. (Foon dealqned lor me on elfta qa-pHcfi>typ«rriterj . ... Form Approved CMS Nfc 2050-0039. UNIFORM HAZARDOUS i-ueneraiorausEPAiDNo. , nfHgffjf^ |2. Paae \ - mtom-tton in the ihadad areae WASTE MANIFEST ia not required by Federr' -•* (;A* • ' PA i^ioa 4. Genera**Phone<*iytn» OI4 5. Transporter t Company Name . 6. US EPA 10 Number rfrwi"(rflfter INT. ______I »l'.l A «i 4 '*^-4^^^P^^»¥^^^« i*5Ki: MfiiinslB^WV^W ARIOOIU fC CycteChem, Inc. ______Recycling, Treatment & Disposal of Hazardous Waste • 21%$outo First Street, Elizabeth, NJ 07%06f* 908-355-5800, Fax (908) 355-0562 LAND DISPOSAL RESTRICTION NOTIFICATION AND CERTIFICATION FORM enerator Name; 'eneratorEPA ID #: tariffest*: tote land disposal restriction (LDR) notification must be submitted with the Initial shipment of all new waste beams. Dud to revised LDR notification requirements effective after August 23, 1998, previously approved faste streams will require re-notification on this form wfth the first shipment after that date. Subsequent otificatton Is not required unless the waste stream changes. I) WASn- STREAM INFORMATION Box A: Check this box If this LDR certification has been supplied wfth a previous shipment Additional Information and certification to not required on this form. BoxBi Indicate If waste stream Is a wastewater (WW) or non-wastewater (NWW) (aqueous waste streams containing < 196 total organic carbon (TOC) and < 196 total suspended solids (TSS) are wastewaters. All other streams are non-wastewaters). BoxCi UstattEPA waste codes and subcategory reference letters (If applfcaMe). Alternatively, attach and reference additional pages (e.g. profiles or lab pack slips) containing required Information. A B C Una frovkvsty shipped NWW/WW CPA WiUteCod^sandfubategofynflenaceieUor LDRcnftte f A *\j'L?ALLs (J_//V?/ -» - - - - •* - -v-^ - B 1 rJf?J/+2' ^f'/Gr'r *-£'?£& / sS^te C i /X' (/ (Jfn/ \ ;L/ f>}3/ " D v t/J/f /VA_»rS tybcategory Reference letters (EPA codes not listed here do not have subcategortes) DOOl A Ignftable characteristic wastest, except Maft TOC tonftable Squids subcatetjory DOOl B Hteh TOCO lOM}hnftatoltaufd*ubeateffory DOO3 A R**ctiYe9u9fidesubc»tegotY •-,•'- 0003 B Reactive cyanide subcateoory 0003 C Water reactive subcategofY DO03 D Other reactive subcateaory - DO06 A Cadmium non-batterYfubcatsoorY . D006 B Cadmium containlno batteries subcateooTY DO08 A Lead non-battery tubcateoofY oooa B Lead add batteries fubcategorY DO09 A Hkjh mercury oroa^svbcateoorY(>26OWM Total Mercury) DOO9 B Matt mercwY Inorganic fubcategoryfe 26OPPM Total Mercury) • DO09 C Low merairYsvbcateoorYf<26O PPM Totat Mercury) \fO9 D Mercury wastewater gubcaieoory ARIOOI 15 ) SPENT SOLVENT WASTZ CONSTITUENTS C/rcfe applicable waste code(s) and constituents) for each manifest tin* item containing EPA spent sorvont wastm codes FOO1-FQO5. A BCD _____ F001 ABCD ___ FOO2 A BCD ___ 1.FOO3 A BCD _____ FOO4 ABCD _____ FOOS A B CD ______-acetone A B CD ______-ethyl mther ABCD______~6enon* ABCD______-mettiMnoi A B CD ______it-butyl alcohol A 8 CD ______-metttyfen* cMortoa A B CD ______-bo-outyfalcono/ A B CD ______-methyl e&yf keton* ABCD______-carbom dltutffda ABCD ______-metftyf isotwtyf ketoof ABCD______-carbon tetrachlorUo ABCD.______A B CD ______~chlorobetueno A B CD ______-mrrid/nm A B CD ______-nwr-BM/ A B CD A B CD.______-o-crwo/ 4 ff CP ______-toluene ABCD______-p-ovsQl ABCD______-2,1,1,-oichtomittUM ABCD, ______-aetyffcaoU ABCD. ABCD______-CydofieJUnon* A BCD -trtrhlnmvfhvton* ABCD.______-o-dJcMorobenzen» ABCD. A B CD ______-ethyl acetat* A B CD ______-l/lf2-tr1chlon'^2f2f-triffuoroethanm A B 'CD ______-ethyf benzene A B CD ______-xyienet UNDERLYING HAZARDOUS CONSTITUENTS For cfiaracteristfcaffy hazardous wastm streams (EPA code* DO01-DO43), pieas* list at underlying hazardous constituents at defined in 40 CFX 268(2)(i) that an present at concentrations exceeding tha universal treatment standard listed in 40 Cnt 263.43 (FOOl~fWS cortstituents Identffi^ / ______J^iona Present ~ _No* Present A ______. ______.^ _ ^Nono Present t) HOW MUST THESE WASTZ STREAMS BK MANAGED? For each manifest line ten* circle appBcabto teJtJiiaitfcqutTement Ftircontamtotedso% drda applicable choice as todkatetl. ABCD ______77J&w35m*/roY-22«Kfcur0ar^ This is an EPA hazardous waste tf^ is /^ a contamtTated sot cr Hazardous deMi. Waste must be treated to the appropriate treatment standard set fyrthh^O^sutpartrj prior to land ABCD ______ABCD ______Ttte is a hazardous waste contamhatedscA Tt&cantarnhattf stf does/does not (^^ contain listed hazardous wastes and does to/compttes with f'^'tf^soS treatment stardardsy standards. ABCD ______This & an £PA hazardous waste that meets at applet treatment standards* and can be landfiffed wfthout father treatment I certify txiderperiattr of law ^ am famSlar with the waste tfrvugh anafysto and testtycr thorough Jmwfed&tf cttftottotttt the waste compiles wth the treatment standard *) CERTIFICATION 'certify that aS irtfafm/tio.x n on tnJt afiaj associated docunwts Is conqfotaj^accunt* to thtb^ of my O RR100II* . . State, of New Jersey Department of Environmental Protection Hazardous Waste Regulation Program * Manifest Section P.O. Box 421, Trenton, NJ 086254421 . Ptoaee type or print ft Mocfc htten, (Ponn designed tor yea on elite (12-pHch) typewriter.) Fom ****** OUB No. SQS040&. HAZARDOUS Mbrmatkxt In the shaded areas WASTE MANIFEST Is not required by Federal taw 4. Oenentor's Phone < I'jMM Transpxter t Company Name 0. US EPA 10 Number vnrw IHT l H .1 o <1 •! iLfl_:-L A M Tranap xtor 2 Company Name i 8. i i i USj EPiA IiD Numbei ir 9. Design itegFaciny Name and Site Addreaa ttflfTB « l/AlWTH. Ri I M .itt.d ti ^ a «t IT Daecifflon (fadudng Proper Shipping Marrw AfM> OOO.4NOK ROM) *>-' rr'**- ' '••' ^l^^ ..•Iw^.r?:n-r^^>^ • V->,:. -wft*' A^*:*&t*«fc* ______ ffltfertato opveretf by ttl» manrfast eteept ainofedln Attachment 5 EPA Fact Sheets ARIOOII8 EPA, Region 111 on Scene to Protect the Health and Safety of Tea Residents HILLTOP RESIDENTIAL LAB 7110 Hilltop Upper Darby, PA W<; are contacting neighbors in this area to inform them of the following: On March 13, the United States Drug Enforcement Agency arrested a tenant of the property at 7110 Hilltop aftir finding various laboratory chemicals that could be used in the production of methamphetamines. Fol lowing the arrest, members of Delaware County Emergency Services surveyed the property and after fin Ling various hazardous chemicals, asked for EPA assistance. Th r owner of the property has denied EPA access to the property. At this time, EPA is pursuing legal means to gain access and investigate the chemicals that have been found. Local police are securing the property and EFA will provide 24-hour security starting today. EPA has been unable to access the property at this time and examine the materials found there. Once EPA gains access, we will begin a cleanup of the site. After cleanup begins, we will be better able to inform netghbors of any requirements for fiirther action at the site. Should you require further details please contact: William Hudson Community Involvement Coordinator USEPA Region HI- 1650 Arch St Philadelphia, FA 19103 215-814-5532 [email protected] RIM 00119 EPA Safely Removes Chemicals HILLTOP RESIDENTIAL LAB 7110 Hilltop Upper Darby, PA We are contacting neighbors in this area to inform them of the following: On March 13, the United States Drug Enforcement Agency arrested a tenant of the property at 7110 Hilltop after finding various laboratory chemicals that could be used in the production of methamphetamines. ,,; Following the arrest members of Delaware County Emergency Services surveyed the property and after finding various hazardous chemicals, asked for EPA assistance. On Wednesday March 15, EPA was able to enter the property u> clean up the hazardous chemicals. The materials were packed in approximately ten 55-gallon drums* EPA expects to complete the cleanup by Friday March 17 and will leave the property at that time, however the drums will be placed in the rear yard of the property until arrangements can be made for the off-site disposal of the chemicals. To insure that the drums are not disturbed, EPA will continue to provide 24-hour security at the site until they are removed which is expected to take place by Friday March 24. Reuse of the property after EPA cleanup will depend upon the disposition of restrictions on human habitation placed by the United States Drug Enforcement Agency and the Upper Darby Township Department of Public Health. Should you require rhrther details please contact: William Hudson Community Involvement Coordinator USEPA Region HI 1650 Arch St Philadelphia. PA 19103 215-814-5532 [email protected] TOTflL P. 03 ARIOOI20 EPA Completes Cleanup of Hilltop Residence HILLTOP RESIDENTIAL LAB 7110 Hilltop Upper Darby, PA We are contacting neighbors in this area to inform them of the following: Or March 13. the United States Drug Enforcement Agency arrested a tenant of the property at 7110 Hilltop aftsr finding various laboratory chemicals that could be used in the production of methamphetamines. Fo lowing the arrest, members of Delaware County Emergency Services surveyed the property, found vaj ious hazardous chemicals and asked for EPA assistance. Or Wednesday March 15, EPA was able to enter the property and clean up the hazardous chemicals. The materials were packed in twelve 55-gallon drums. EPA completed the cleanup on Friday, March 17 and left the property at that time. The drums were placed in the rear yard of the property and arrangements were nude for the off-site disposal of the chemicals. The drums were removed from the property on Friday M;irch24. EP A has completed its involvement with the Hillside Residential Lab. Reuse of the property after EPA cleanup will depend upon the disposition of restrictions on human habitation placed by the United States Drug Enforcement Agency and the Upper Darby Township Department of Public Health. Should you require further details please contact William Hudson Community Involvement Coordinator USEPA Region m 1650 Arch St Philadelphia, PA 19103 215-314-5532 [email protected] TOTflL P.02 ARIOOI2I