Part 185—Tolerances for Pesticides in Food

§ 180.1167 40 CFR Ch. I (7–1–96 Edition)

PART 185—TOLERANCES FOR 185.2650 Endothall. 185.2700 Ethephon. PESTICIDES IN FOOD 185.2750 Ethion. 185.2800 2-[1-(Ethoxyimino)butyl]-5-[2- Subpart A—[Reserved] (ethylthio)propyl]-3-hydroxy-2- cyclohexene-1-one. Subpart B—Food Additives Permitted in 185.2850 Ethylene oxide. Food for Human Consumption 185.2900 Ethyl formate. 185.2950 Ethyl 3-methyl-4- Sec. (methylthio)phenyl (1-methylethyl)- 185.100 Acephate. phosphoramidate. 185.150 Aldicarb. 185.3000 O-Ethyl O-[4-(methylthio)phenyl] S- 185.200 Aluminum phosphide. propyl phosphorodithioate. 185.250 4-Amino-6-(1,1-dimethylethyl)-3- 185.3200 Fenarimol. (methylthio)-1,2,4-triazin-5(4H)-one. 185.3225 Fenpropathrin. 185.300 Avermectin B1 and its delta-8,9-iso- 185.3250 Fluazifop-butyl. mer; tolerances for residues. 185.3385 Flutolanil (N-(3-(1- 185.350 Benomyl. methylethoxy)phenyl)-2- 185.410 1,1-Bis(p-chlorophenyl)-2,2,2- (trifluoromethyl)benzamide). trichloroethanol. 185.3450 Formetanate hydrochloride. 185.425 Bromide ion and residual bromine. 185.3475 Fumigants for grain-mill machin- 185.600 Carbofuran; tolerances for residues. ery. 185.650 Carbon dioxide. 185.3480 Fumigants for processed grains 185.800 1-(4-Chlorophenoxy)-3,3-dimethyl-1- used in production of fermented malt [1H-1,2,4-triazol-1-yl]-2-butanone. beverages. 185.900 1-[(6-Chloro-3-pyridinyl)methyl]-N- 185.3500 Glyphosate. nitro-2-imidazolidinimine; tolerances for 185.3550 Hexakis. residues. 185.3575 Hexazinone. 185.1000 Chlorpyrifos. 185.3600 Hydrogen cyanide. 185.1050 Chlorpyrifos-methyl. 185.3625 Hydroprene; tolerances for residues. 185.1075 Clethodim ((E)-(±)-2-[1-[[(3-chloro-2- 185.3650 Imazalil. propenyl)oxy]imino]propyl]-5-[2- 185.3700 Inorganic bromide. (ethylthio)propyl]-3-hydroxy-2- 185.3750 Iprodione. cyclohexen-1-one). 185.3765 Lambda-cyhalothrin. 185.1100 Clopyralid. 185.3775 d-Limonene. 185.1150 Combustion product gas. 185.3800 Magnesium phosphide. 185.1200 Copper. 185.3850 Malathion. 185.1250 Cyfluthrin. 185.3900 Maleic hydrazide. 185.1300 Cyano(3-phenoxyphenyl)methyl-4- 185.4000 Metalaxyl. chloro-alpha-(1– 185.4025 Metaldehyde. methylethyl)benzeneacetate and its S,S 185.4035 Metarhizium anisopliae strain isomer. ESF1. 185.1350 Cyhexatin. 185.4100 Methomyl. 185.1450 2,4-D. 185.4150 Methoprene. 185.1500 Dalapon. 185.4200 1-Methoxycarbonyl-1-propen-2-yl 185.1580 Deltamethrin. dimethylphosphate and its beta isomer. 185.1650 Dialifor. 185.4250 Methyl chloride. 185.1700 Diatomaceous earth. 185.4300 Methyl formate. 185.1750 Diazinon. 185.4350 Myclobutanil. 185.1800 Dicamba. 185.4400 Nitrogen. 185.1850 3-(3,5-Dichlorophenyl)-5-ethenyl-5- 185.4450 Norflurazon. methyl-2,4-oxazolidinedione. 185.4500 N-Octylbicycloheptene 185.1900 2,2-Dichlorovinyl dimethyl phos- dicarboximide. phate. 185.4650 Paraformaldehyde. 185.1975 Dihydro-5-heptyl-2(3H)-furanone. 185.4700 Paraquat. 185.1985 Dihydro-5-pentyl-2(3H)-furanone. 185.4800 Phosalone. 185.2150 2,2-Dimethyl-1,3-benzodioxol-4-ol 185.4850 Picloram. methylcarbamate. 185.4900 Piperonyl butoxide. 185.2200 O,O-Dimethyl O-(4-nitro-m-tolyl) 185.4950 Pirimiphos-methyl. phosphorothioate. 185.5000 Propargite. 185.2225 O,O-Dimethyl S-[(4-oxo-1,2,3- 185.5100 Propetamphos. benzotriazin-3(4H)-ylmethyl] 185.5150 Propylene oxide. phosphorodithioate. 185.5200 Pyrethrins. 185.2250 Dimethyl phosphate of 3-hydroxy- 185.5250 Quizalofop ethyl. N-methyl-cis-crotonamide. 185.5300 Resmethrin. 185.2500 Diquat. 185.5375 Sulfonium, trimethyl-salt with N- 185.2600 Endosulfan. (phosphonomethyl)glycine (1:1).

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185.5450 Tralomethrin. stream of insecticide shall be used. For 185.5475 Tetradifon. spot treatments, a coarse, low-pressure 185.5550 Thiabendazole. spray shall be used to avoid atomiza- 185.5950 Triforine. 185.6300 Zinc ion and maneb coordination tion or splashing of the spray. Con- product. tamination of food or food-contact surfaces shall be avoided. Subpart C—Food Additives Resulting From (ii) To assure safe use of the insecti- Contact With Containers or Equipment cide, its label and labeling shall con- And Food Additives Otherwise Affect- form to that registered by the U.S. En- ing Food vironmental Protection Agency, and it 185.7000 Malathion. shall be used in accordance with such lable and labeling. AUTHORITY: 21 U.S.C. 346a and 348. [47 FR 52995, Nov. 24, 1982. Redesignated at 53 SOURCE: 40 FR 14156, Mar. 28, 1975, unless FR 24667, June 29, 1988] otherwise noted. Redesignated at 41 FR 26568, June 28, 1976, and 53 FR 24667, June 29, 1988. § 185.150 Aldicarb. EDITORIAL NOTE: The text of part 185 set forth below was transferred and recodified at (a) A regulation is established per- 53 FR 24666, June 29, 1988. New part 185 for- mitting the combined residues of the merly appeared in 21 CFR part 193. A Redes- insecticide/nematocide aldicarb 2- ignation Table appears in the Finding Aids methyl-2-(methylthio)propionaldehyde section of this volume. O-(methylcarbamoyl)oxime and its cholinesterase-inhibiting metabolites Subpart A—[Reserved] 2-methyl-2-(methylsulfonyl) propionaldehyde O-(methylcarbamoyl)oxime Subpart B—Food Additives Per- and 2-methyl-2-(methyl- mitted in Food for Human sulfonyl)propionaldehyde O-(methyl- Consumption carbamoyl)oxime in or on the commodity sorghum bran at 0.5 part per mil- § 185.100 Acephate. lion. (a) A food additive tolerance of 0.02 (b) [Reserved] ppm is established for the combined residues of acephate (O,S-dimethyl [47 FR 14894, Apr. 7, 1982, as amended at 53 FR 8874, Mar. 18, 1988. Redesignated at 53 FR acetylphosphoramidothioate) and its 24667, June 29, 1988] cholinesterase-inhibiting metabolite, methamidophos as follows: § 185.200 Aluminum phosphide. (1) In or on all food items (other than those already covered by a higher tol- The food additive aluminum erance as a result of use on growing phosphide may be safely used in ac- crops) in food handling establishments. cordance with the following prescribed (2) The acephate may be present as a conditions: residue from applications of acephate (a) It is used to generate phosphine in in food handling establishments, in- the fumigation of processed foods. cluding food service, manufacturing (b) To assure safe use of the additive, and processing establishments, such as it is used in compliance with label and restaurants, cafeterias, supermarkets, labeling conforming to that registered bakeries, breweries, dairies, meat with the U.S. Environmental Protec- slaughtering and packing plants, and tion Agency. Labeling shall bear a canneries in accordance with the fol- warning to aerate the finished food for lowing prescribed conditions: 48 hours before it is offered to the (i) Application shall be limited solely consumer. A further warning shall to spot and/or crack and crevice treat- state that under no condition should ment in food handling establishments the formulation containing aluminum where food and food products are held, phosphide be used so that it or its processed, prepared and served. Spray unreacted residues will come in con- concentration shall be limited to a tact with any processed food, except maximum of 1.0 percent active ingredi- processed brewer’s rice, malt, and corn ent. For crack and crevice treatments, grits stored in breweries for use in the equipment capable of delivering a pin- manufacture of beer.

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(c) Residues of phosphine in or on sult of application of the fungicide to processed foods do not exceed 0.01 part growing grapes and tomatoes. per million. [59 FR 46769, Sept. 12, 1994] [40 FR 14156, Mar. 28, 1975. Redesignated at 41 FR 26568, June 28, 1976, and amended at 44 FR § 185.410 1,1-Bis(p-chlorophenyl)-2,2,2- 35210, June 19, 1979. Redesignated at 53 FR trichloroethanol. 24667, June 29, 1988] A tolerance of 45 parts per million is § 185.250 4-Amino-6-(1,1- established for residues of the insecti- dimethylethyl)- 3-(methylthio)-1,2,4- cide 1,1-bis(p-chlorophenyl)-2,2,2- triazin-5(4H)-one. trichloroethanol in dried tea when Tolerances are established for com- present therein as a result of its appli- bined residues of the herbicide 4- cation to the growing tea crop. amino-6-(1,1-dimethylethyl)-3-(methyl- [40 FR 14156, Mar. 28, 1975. Redesignated at 41 thio)-1,2,4-triazin-5(4H)-one and its tri- FR 26568, June 28, 1976, and at 53 FR 24667, azinone metabolites in or on the fol- June 29, 1988. Correctly redesignated at 53 FR lowing processed foods when present 28383, July 28, 1988] therein as a result of application of EFFECTIVE DATE NOTE: At 59 FR 10997, Mar. this herbicide to growing crops: 9, 1994, § 185.410 was removed. At 59 FR 23800, May 9, 1994 the effective date of the removal Parts per was stayed until further notice. Food million

Barley, milled fractions (except flour) ...... 3 § 185.425 Bromide ion and residual Potatoes, processed (inc. potato chips) ...... 3 bromine. Sugarcane molasses ...... 2 Wheat milled fractions (except flour) ...... 3 The food additives, bromide ion and residual bromine, may be present in po- [44 FR 40283, July 10, 1979. Redesignated at 53 table water in accordance with the fol- FR 24667, June 29, 1988] lowing conditions: (a) The food additives are present as § 185.300 Avermectin B1 and its delta- a result of treating water aboard ships 8,9-isomer; tolerances for residues. with a polybrominated ion-exchange Tolerances, to expire on April 30, resin (as a source of bromine) under the 1996, are established for the combined supervision of trained personnel. residues of the insecticide avermectin (b) Residual bromine levels are con- B1 and its delta-8,9-isomer (a mixture trolled to not exceed 1.0 part per mil- of avermectins containing ´ 80 percent lion (ppm) in the final treated water. avermectin B1a (5-O-demethyl Control is effected using calibrated re- avermectin B1a) and < 20 percent circulating or proportioning bromine avermectin B1a (5-O-demethyl-25-di (1- feeder equipment and periodic checks methylpropyl)-25-1(1-methylethyl) of residual bromine using a bromine avermectin A 1a) in or on the following test kit. To assure safe use of the addi- commodity: tives, the label and labeling of the dis- infectant formulation containing the Parts per Commodity million food additives shall conform to the label and labeling registered by the Citrus oil ...... 0.10 U.S. Environmental Protection Agen- cy. [59 FR 49826, Sept. 30, 1994] (c) No tolerance is established for bromide ion levels. § 185.350 Benomyl. Tolerances of 50 parts per million are [41 FR 17893, Apr. 29, 1976. Redesignated at 41 established for combined residues of FR 26568, June 28, 1976, and at 53 FR 24667, June 29, 1988] the fungicide benomyl (methyl-1- (butylcarbamoyl)-2- benzimidazolecarbamate) and its § 185.600 Carbofuran; tolerances for metabolites containing the benzimid- residues. azole moiety (calculated as benomyl) A tolerance is established for the in raisins and concentrated tomato combined residues of the insecticide products when present therein as a re- carbofuran (2,3-dihydro-2,2-dimethyl-7-

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benzofuranyl-N-methylcarbamate), its ing food resulting from application of carbamate metabolite 2,3-dihydro-2,2- the insecticide to potatoes: dimethyl-3-hydroxy-7-benzofuranyl-N- Parts per methylcarbamate, and the phenolic Food million metabolites 2,3-dihydro-2,2-dimethyl-7- benzofuranol, 2,3-dihydro-2,2-dimethyl- 7-benzofuranol and 2,3-dihydro-2,2-di- Potato, chip ...... 0.4 methyl-3, 7-benzofurandiol in or on the following food commodity: (b) A food additive regulation is es- Parts per tablished premitting residues of the in- Commodity million secticide 1-[(6-chloro-3- Raisins (of which no more than 1.0 ppm is carba- pyridinyl)methyl]-N-nitro-2- mate) ...... 2.0 imidazolidimine in or on the following food commodities: [46 FR 58487, Dec. 2, 1981. Redesignated at 53 FR 24667, June 29, 1988] Part per mil- Food lion

§ 185.650 Carbon dioxide. Grape, juice ...... 1.5 The food additive carbon dioxide may Grape, raisin ...... 1.5 be safely used after harvest in modified Tomato, paste ...... 6.0 atmospheres for stored product insect Tomato, puree ...... 3.0 control on all processed agricultural commodities. [59 FR 61278, Nov. 30, 1994, as amended at 60 FR 18549, Apr. 12, 1995] [46 FR 32866, June 25, 1981. Redesignated at 53 FR 24667, June 29, 1988] § 185.1000 Chlorpyrifos. § 185.800 1-(4-Chlorophenoxy)-3,3-di- (a) Tolerances are established for the methyl-1-(1H-1,2,4-triazol-1-yl)-2- combined residues of the insecticide butanone. chlorpyrifos [O,O-diethyl O-(3,5,6- Tolerances are established for the trichloro-2-pyridyl) phosphorothioate] combined residues of the fungicide 1-(4- and its metabolite 3,5,6-trichloro-2- chlorophenoxy)-3,3-dimethyl-1-(1H- pyridinol resulting from application of 1,2,4-triazol-1-yl)-2-butanone and its the insecticide to growing crops as fol- metabolite beta-(4-chlorophenoxy)- lows: alpha-(1,1-dimethylethyl)-1H-1,2,4-tri- Parts per azole-1-ethanol in or on the following Foods million food commodities: Citrus oil ...... 25.0 Corn oil ...... 3.0

Parts per Food million (b) The additive chlorpyrifos [O,O- diethyl O-(3,5,6-trichloro-2-pyridyl) Barley, milled fractions (except flour) ...... 4.0 phosphorothioate] may be safely used Wheat, milled fractions (except flour) ...... 4.0 in accordance with the following prescribed conditions. [48 FR 5901, Feb. 9, 1983. Redesignated at 53 (1) Application shall be limited solely FR 24667, June 29, 1988] to spot and/or crack and crevice treatment in food handling establishments § 185.900 1-[(6-Chloro-3- where food and food products are held, pyridinyl)methyl]-N-nitro-2- processed, prepared or served. Contami- imidazolidinimine; tolerances for nation of food or food contact surfaces residues. shall be avoided. Food must be re- (a) A food additive regulation is es- moved or covered during treatment. tablished permitting residues of the in- (2) Spray concentration for spot secticide 1-[(6-chloro-3- treatment shall be limited to a maxi- pyridinyl)methyl]-N-nitro-2- mum of 0.5 percent of the active ingre- imidazolidinimine in or on the follow- dient by weight. A course, low-pressure

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spray shall be used to avoid atomiza- (4) For spot treatment, an individual tion or splashing of the spray. spot shall not exceed 2 square feet. (3) Paint-on application for spot (5) To assure safe use of the insecti- treatment shall be limited to a maxi- cide, its label and labeling shall con- mum of 2 percent of the active ingredi- form to that registered by the U.S. En- ent by weight. vironmental Protection Agency, and it (4) Crack and crevice treatment shall shall be used in accordance with such be limited to a maximum of 2 percent label and labeling. of the active ingredient by weight. (d) Tolerances are established for res- Equipment capable of delivering a pin- idues of the insecticide chlorpyrifos stream of insecticide shall be used. [O,O-diethyl O-(3,5,6-trichloro-2-pyri- (5) Application via adhesive strips dyl) phosphorothioate] resulting from shall contain a maximum of 10% by application of the insecticide to grow- weight of the controlled-release prod- ing crops as follows: uct in food-handling establishments Parts per where food and food products are held, Foods million processed, prepared, or served. A maximum of 36 strips (or 5.15 grams of Milling fractions (except flour) of wheat ...... 1.5 chlorpyrifos) is to be used per 100 Mint oil ...... 8 square feet of floor space. The strips Peanut oil ...... 0.4 are not to be placed in exposed areas where direct contact with food, uten- [47 FR 30478, July 14, 1982, as amended at 53 sils, and food-contact surfaces would be FR 9434, Mar. 23, 1988. Redesignated at 53 FR likely to occur. 24667, June 29, 1988; 57 FR 10293, Mar. 25, 1992; 58 FR 19356, Apr. 14, 1993] (6) To assure safe use of the insecticide, its label and labeling shall con- § 185.1050 Chlorpyrifos-methyl. form to that registered by the U.S. En- vironmental Protection Agency, and it Tolerances are established for the shall be used in accordance with such combined residues of the insecticide label and labeling. chlorpyrifos-methyl (O,-O-dimethyl-O- (3,5,6-trichloro-2-pyridyl) phos- (c) A tolerance of 0.1 part per million phorothioate and its metabolite (3,5,6- is established for residues of trichloro-2-pyridinol) in or on the fol- chlorpyrifos, per se, in or on all food lowing processed feeds when present items (other than those already cov- therein as a result of application to ered by a higher tolerance as a result stored grains: of use on growing crops) in food service establishments where food and food Parts per products are prepared and served, as a Food million result of the application of chlorpyrifos Barley milling fractions (except flour) ...... 90 in microencapsulated form. Oats milling fractions (except flour) ...... 130 (1) Application of a microencap- Sorghum milling fractions (except flour) ...... 90 sulated product shall be limited solely Rice milling fractions (except flour) ...... 30 to spot and/or crack and crevice treat- Wheat milling fractions (except flour) ...... 30 ment in food handling establishments where food and food products are pre- [50 FR 26682, June 27, 1985. Redesignated at 53 pared and served. All treatments shall FR 24667, June 29, 1988] be applied in such a manner as to avoid contamination of food or food contact § 185.1075 Clethodim ((E)-(±)-2-[1-[[(3- surfaces. chloro-2-pro- (2) Spray concentrations shall be lim- penyl)oxy]imino]propyl]-5-[2- ited to a maximum of 0.5 percent of the (ethylthio)propyl]-3-hydroxy-2- active ingredient by weight. cyclohexen-1-one). (3) For crack and crevice treatment, Food additive tolerances are estab- equipment capable of delivering a pin lished for the combined residues of the stream of spray directly into cracks herbicide clethodim ((E)-(±)-2-[1-[[(3- and crevices or capable of applying chloro-2-propenyl)oxy]imino]propyl]-5- small amounts of insecticide into [2-(ethylthio)propyl]-3-hydroxy-2- cracks and crevices shall be used. cyclohexen-1-one) and its metabolites

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containing the 2-cyclohexen-1-one moi- be prevented from reaching the food ety in or on the following processed being treated. foods: (b) The insecticide meets the following specifications: Parts per Food million (1) Carbon monoxide content not to exceed 4.5 percent by volume. Potato flakes1 ...... 1.0 (2) It is used or intended for use to Potato granules1 ...... 1.0 displace or remove oxygen in the storage of food, except fresh meat. 1There are no U.S. registrations as of August 9, 1995. [46 FR 32866, June 25, 1981. Redesignated at 53 [60 FR 40505, Aug. 9, 1995] FR 24667, June 29, 1988]

§ 185.1100 Clopyralid. § 185.1200 Copper. (a) Tolerances are established for res- A tolerance of 1 part per million is idues of the herbicide clopyralid (3,6- established in potable water for resi- dichloro-2-pyridinecarboxylic acid), in dues of copper resulting from the use of or on the following foods: the algicides or herbicides basic copper carbonate (malachite), copper sulfate, Parts per Food million copper monoethanolamine, and copper triethanolamine to control aquatic Barley, milled fractions (except flour) ...... 12.0 Oats, milled fractions (except flour) ...... 12.0 plants in reservoirs, lakes, ponds, irri- Wheat, milled fractions (except flour) ...... 12.0 gation ditches, and other potential sources of potable water. (b) Time-limited tolerances are established as follows for residues of the [45 FR 53459, Aug. 12, 1980. Redesignated at 53 herbicide clopyralid (3,6-dichloro-2-pyr- FR 24667, June 29, 1988] idine carboxylic acid), in or on the following foods: § 185.1250 Cyfluthrin.

Parts per Expiration (a) A time-limited tolerance, to ex- Foods million date pire on November 15, 1997, is established for residues of the insecticide Field corn, milling fractions ...... 1.5 December 31, 1996. cyfluthrin (cyano(4-fluoro-3- phenoxyphenyl)methyl-3-(2,2- [52 FR 10563, Apr. 2, 1987. Redesignated at 53 dichloroethenyl)-2,2- FR 24667, June 29, 1988, and amended at 55 FR dimethylcyclopropanecarboxylate) in 31183, Aug. 1, 1990; 59 FR 19640, Apr. 25, 1994] or on the following food commodities:

Commodity Parts per § 185.1150 Combustion product gas. million Expiration date The food additive combustion product gas may be safely used after har- Cottonseed oil ...... 2.0 Nov. 15, 1997. vest in modified atmospheres for stored Tomato, concentrated 0.5 Do. product insect control on all processed products. agricultural commodities (except fresh meat) with the following prescribed conditions: (b) [Reserved] (a) The combustion product gas is (c) A tolerance of 0.05 ppm is estab- produced by the controlled combustion lished for residues of the insecticide in air of butane, propane, or natural cyfluthrin (cyano(4-fluoro-3-phenoxy- gas. The combustion equipment shall phenyl)methyl-3-(2,2-dichloroethenyl)- be provided with an absorption type fil- 2,2-dimethylcyclopropanecarboxylate; ter capable of removing possible toxic CAS Reg. No. 69359–37–5) in food com- impurities through which all gas used modities exposed to the insecticide in the treatment of food shall pass and during treatment of food-handling es- with suitable controls to insure that tablishments where food and food prod- any combustion products failing to ucts are held, processed, prepared, or meet the specifications provided will served. Treatments may be made by

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general surface, spot, and/or crack and § 185.1300 Cyano(3- crevice applications. phenoxyphenyl)methyl-4-chloro- (1) General surface treatments shall alpha-(1– be limited to a maximum of 3.8 grams methylethyl)benzeneacetate and its S,S isomer. of active ingredient per 1,000 square feet, applying to walls, floors, and ceil- (a) A food additive tolerance of 0.05 ings with a low-pressure system. Cover part per million is established for resi- or remove all food processing and/or dues of the insecticide cyano(3- handling equipment during applica- phenoxyphenyl)methyl-4-chloro–alpha- tion. Do not apply directly to food (1-methylethyl)benzeneacetate and an products. Reapplications may be made isomer, (S)-cyano(3-phenoxyphenyl)methyl-(S)-4-chloro–alpha-(1- at 10-day intervals. methylethyl)-benzeneacetate, as fol- (2) Crack and crevice or spot treat- lows: ments shall be limited to a maximum (1) In or on all food items (other than of 0.1 percent of the active ingredient those already covered by a higher tol- by weight, applied with a low-pressure erance as a result of use on growing system with a pinpoint or variable-pat- crops) in food-handling establishments tern nozzle. Dust formulation shall be where food products are held, proc- limited to a maximum of 0.1 percent of essed, or prepared. the active ingredient by weight, ap- (2) Application of cyano(3-phenoxy- plied using a hand duster, power dust- phenyl)methyl-4-chloro-alpha-(1- er, or other equipment capable of ap- methylethyl)benzeneacetate shall be plying dust insecticide directly into limited to space treatment with a max- voids and cracks and crevices. Dust ap- imum of 0.5 fluid ounce of a 0.05-per- plications should be made in a manner cent active ingredient solution per to avoid deposits on exposed surfaces 1,000 cubic feet of space, or as a contact or introducing the material into the spray applied as a coarse wet spray at air. Cover exposed food or remove food a maximum of 1 gallon of a 0.2-percent from premises. Do not apply directly to active ingredient solution per 1,000 food. Reapplications may be made at square feet of surface. Food must be re- 10-day intervals. moved or covered during treatment. (3) To ensure safe use of the insecti- Spray should not be applied directly to cide, its label and labeling shall con- surfaces or utensils that may come form to that registered by the Environ- into contact with food. Food-contact mental Protection Agency, and it shall surfaces and equipment should be thoroughly cleaned with an effective clean- be used in accordance with such label ing compound and rinsed with potable and labeling. water before using. (d) A tolerance of 20.0 parts per mil- (3) Application of (S)-cyano(3- lion is established for residues of the phenoxyphenyl) methyl-(S)-4-chloro- insecticide cyfluthrin (cyano(4-fluoro- alpha-(1-methylethyl)benzeneacetate 3-phenoxyphenyl)methyl-3-(2,2- shall be limited to space treatment dichloroethenyl)-2,2-dimethyl-cyclo- with a maximum of 1.0 fluid ounce of a propanecarboxylate) in or on dried 0.25-percent active ingredient solution hops resulting from application of the per 1,000 cubic feet of space, or as a insecticide to hops. contact spray applied as a coarse wet [52 FR 29009, Aug. 5, 1987; 52 FR 31846, Aug. 24, spray at a maximum of 1 gallon of a 1987, as amended at 53 FR 1917, Jan. 25, 1988; 0.05-percent active ingredient solution 53 FR 18837, May 25, 1988. Redesignated at 53 per 1,000 square feet of surface, or as a FR 24667, June 29, 1988, and amended at 54 FR pressurized spot/crack and crevice 27643, June 30, 1989; 54 FR 46069, Nov. 1, 1989; spray of a 0.25-percent solution. Food 55 FR 26440, June 28, 1990; 60 FR 28354, May must be removed or covered during 31, 1995; 60 FR 33362, June 28, 1995] treatment. Spray should not be applied

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directly to surfaces or utensils that the Interior; Agricultural Research may come into contact with food. Service, U.S. Department of Agri- Food-contact surfaces and equipment culture; and the Corps of Engineers, should be throroughly cleaned with an U.S. Department of Defense. effective cleaning compound and rinsed (ii) As a result of the application of with potable water before using. the dimethylamine salt of 2,4-D for (4) To assure safe use of the additive, water hyacinth control in ponds, lakes, its label and labeling shall conform to reservoirs, marshes, bayous, drainage that registered with the U.S. Environ- ditches, canals, rivers and streams that mental Protection Agency, and it shall are quiescent or slow moving in pro- be used in accordance with such label grams of the Corps of Engineers or and labeling. other Federal, State, or local public (b) [Reserved] agencies. [55 FR 26442, June 28, 1990] (iii) As a result of application of its dimethylamine salt or is butoxy- § 185.1350 Cyhexatin. ethanol ester for Eurasian watermilfoil Tolerances are established for com- control in programs conducted by the bined residues of the insecticide Tennessee Valley Authority in dams cyhexatin (tricyclohexyl- and reservoirs of the TVA system. hydroxystannane; CAS Reg. No. 13121– (b) [Reserved] 70–5) and its organotin metabolites [53 FR 9434, Mar. 23, 1988. Redesignated at 53 (calculated as cyhexatin) in or on the FR 24667, June 29, 1988] following processed foods when present therein as a result of application of § 185.1500 Dalapon. this insecticide to the growing crops: A tolerance of 0.2 part per million is Parts per Food million established for residues of the herbicide dalapon (2,2-dichloropropionic Hops, dried ...... 90 acid) in potable water when present Prunes, dried ...... 4 therein as a result of the application of [53 FR 23389, June 22, 1988. Redesignated at 53 dalapon sodium-magnesium salt mix- FR 24667, June 29, 1988] tures to irrigation ditch banks in the western United States. § 185.1450 2,4-D. [43 FR 22345, May 25, 1978. Redesignated at 53 (a) Tolerances are established for res- FR 24667, June 29, 1988] idues of the herbicide 2,4-D (2,4- dichlorophenoxyacetic acid) as follows: § 185.1580 Deltamethrin. (1) 5 ppm in sugarcane molasses, re- Tolerances are established for resi- sulting from application of the herbi- dues of the insecticide deltamethrin cide to sugarcane fields. [(S)-alpha-cyano-3-phenoxybenzyl- (2) 2 ppm in the milled fractions (ex- (1R,3R)-3-(2,2-dibromovinyl)-2,2- cept flour) derived from barley, oats, dimethylcyclopropanecarboxylate] and rye, and wheat to be ingested as food or its major metabolites, trans- to be converted to food. Such residues deltamethrin [(S)-alpha-cyano-m- may be present therein only as a result phenoxybenzyl(1R,3S)-3-(2,2- of application to the growing crop of dibromovinyl)-2,2- the herbicides identified in 40 CFR dimethylcyclopropanecarboxylate] and 180.142. alpha-R-deltamethrin [(R)-alpha-cyano- (3) 0.1 ppm (negligible residue) in po- m-phenoxybenzyl-(1R,3R)-3-(2,2- table water. Such residues may be dibromovinyl)-2,2- present therein only: dimethylcyclopropanecarboxylate] in (i) As a result of the application of or on the following food commodities: the dimethylamine salt of 2,4-D to irrigation ditch banks in the Western Parts per Expiration United States in programs of the Bu- Commodity million date reau of Reclamation; cooperating water user organizations; the Bureau of Cottonseed oil ...... 0.2 Nov. 15, Sport Fisheries, U.S. Department of 1997

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dairies, meat slaughtering and packing Commodity Parts per Expiration million date plants, and canneries where food and Tomato (products) concentrated 1.0 None food products are held, processed, and served. [60 FR 42455, Aug. 16, 1995] (1) Spray and dust concentrations shall be limited to a maximum of 1 percent and 2 percent, respectively, of ac- § 185.1650 Dialifor. tive ingredient by weight. The spray A tolerance of 2 parts per million is concentration limit of 1 percent shall established for combined residues of include, but not be limited to, encap- the insecticide dialifor (S-(2-chloro-1- sulated formulations of the additive phthalimidoethyl) O,O-diethyl phos- utilizing the encapsulating polymer phorodithioate) and its oxygen analog formed from the reaction of sebacoyl S-(2-chloro-1-phthalimidoethyl O,O- chloride, polymethylene polyphenyl- diethyl phosphorothioate) in or on rai- isocyanate, ethylenediamine and/or sins from application of the insecticide diethylenetriamine. to the growing raw agricultural com- (2) Application to areas, surfaces, or modity grapes. utensils contacted by food, contamination of food and food contact surfaces, § 185.1700 Diatomaceous earth. and the introduction of spray or dust The food additive diatomaceous into the air is to be avoided. earth may be safely used in accordance (3) For spot treatment, a coarse, low with the following conditions. Applica- pressure spray shall be used. Applica- tion shall be limited solely to spot and/ tion is limited to floor surfaces only or crack and crevice treatments in food and to 20 percent of the surface area. processing and food storage areas in ac- Any individual spot treatment shall cordance with the prescribed condi- not exceed 2 square feet. tions: (4) For crack and crevice treatment, (a) It is used or intended for use for equipment capable of delivering dust or control of insects in food processing a pin stream of spray directly into the and food storage areas: Provided, That cracks and crevices shall be used. the food is removed or covered prior to (b) To assure safe use of the insecti- such use. (b) To assure safe use of the insecticide, its label and labeling shall con- cide, its label and labeling shall conform to that registered by the U.S. En- form to that registered by the U.S. En- vironmental Protection Agency, and it vironmental Protection Agency, and it shall be used in accordance with such shall be used in accordance with such label and labeling. label and labeling. [45 FR 12700, Feb. 18, 1981, as amended at 47 [46 FR 55511, Nov. 10, 1981. Redesignated at 53 FR 25952, June 16, 1982; 52 FR 32293, Aug. 27, FR 24667, June 29, 1988] 1987; 53 FR 23389, June 22, 1988. Redesignated at 53 FR 24667, June 29, 1988] § 185.1750 Diazinon. § 185.1800 Dicamba. A regulation is established permitting the use of the insecticide diazinon Tolerances are established for the (O,O-diethyl O-[6-methyl-2-(1-methyl- combined residues of the herbicide ethyl)-4-pyrimidinyl] phosphoro- dicamba (3,6-dichloro-o-anisic acid) and thioate; CAS Reg. No. 333–41–5) in food- its metabolite 3,6-dichloro-5-hydroxy-o- handling establishments in accordance anisic acid in or on the following proc- with the following prescribed condi- essed foods when present therein as a tions: result of application of this herbicide (a) Application shall be limited sole- to growing crops. ly to spot and/or crack and crevice treatment in food handling establishments, including food service, manu- Parts per facturing, and processing establish- Food million ments, such as restaurants, cafeterias, supermarkets, bakeries, breweries, Sugarcane molasses ...... 2.0

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[48 FR 11114, Mar. 16, 1983. Redesignated at 53 § 185.1900 2,2-Dichlorovinyl dimethyl phos- FR 24667, June 29, 1988] phate. A tolerance that expires on March 10, 1994, § 185.1850 3-(3,5-Dichlorophenyl)-5-eth- is established as follows: The food additive enyl-5-methyl-2,4-oxazolidinedione. 2,2-dichlorovinyl dimethyl phosphate may be (a) Tolerances are established for the present as a residue from application as an insecticide on packaged or bagged nonperish- combined residues of the fungicide 3- able processed food (see: 21 CFR 170.3(j)) in (3,5-dichlorophenyl)-5-ethenyl-5-meth- an amount in such food not in excess of 0.5 yl-2,4-oxazolidinedione and its part per million (ppm). To assure safe use of metabolites containing the 3,5- the insecticide, its label and labeling shall dichloroaniline moiety in or on the fol- conform to the label and labeling registered lowing food commodities: by the U.S.Environmental Protection Agen- cy, and the usage employed shall conform to Parts per such label and labeling. Food million [58 FR 59667, Nov. 10, 1993] Prunes ...... 75

(b) A food additive regulation is es- § 185.1975 Dihydro-5-heptyl-2(3H)- tablished for the combined residues of furanone. the fungicide, 3-(3,5-dichlorophenyl)-5- The food additive dihydro-5-heptyl- ethenyl-5-methyl-2,4-oxazolidinedione, 2(3H)-furanone may be safely used in and its metabolites containing the 3,5- accordance with the following condi- dichloroaniline moiety in or on the fol- tions: lowing processed foods when present (a) It is used in combination with the therein as a result of application to active ingredients d-limonene and grapes: dihydro-5-pentyl-2(3H)-furanone in insect-repellent tablecloths and in insect-repellent strips used in food-han- Parts per dling establishments. Food million (b) To assure safe use of the insecti- Raisins ...... 30 cide, its label and labeling shall conform to that registered by the U.S. En- [51 FR 11437, Apr. 3, 1986, as amended at 52 vironmental Protection Agency, and it FR 17941, May 13, 1987; 53 FR 20308, June 3, 1988. Redesignated at 53 FR 24667, June 29, shall be used in accordance with such 1988] label and labeling. [60 FR 16053, Mar. 29, 1995] § 185.1900 2,2-Dichlorovinyl dimethyl phosphate. § 185.1985 Dihydro-5-pentyl-2(3H)- The food additive 2,2-dichlorovinyl furanone. dimethyl phosphate may be present as The food additive dihydro-5-pentyl- a residue from application as an insec- 2(3H)-furanone may be safely used in ticide on packaged or bagged non- accordance with the following condi- perishable processed food (see: 21 CFR tions: 170.3(j)) in an amount in such food not (a) It is used in combination with the in excess of 0.5 part per million (ppm). active ingredients d-limonene and To assure safe use of the insecticide, dihydro-5-heptyl-2(3H)-furanone in in- its label and labeling shall conform to sect-repellent tablecloths and in in- the label and labeling registered by the sect-repellent strips used in food-han- U.S. Environmental Protection Agen- cy, and the usage employed shall con- dling establishments. form with such label or labeling. (b) To assure safe use of the insecticide, its label and labeling shall con- [56 FR 29183, June 26, 1991] form to that registered by the U.S. EFFECTIVE DATE NOTE: At 58 FR 59667, Nov. Enviornmental Protection Agency, and 10, 1993, § 185.1900 was revised. At 59 FR 11556, it shall be used in accordance with Mar. 11, 1994, the revision was stayed until such label and labeling. further notice. For the convenience of the reader, the revised text is set forth below. [60 FR 16053, Mar. 29, 1995]

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§ 185.2150 2,2-Dimethyl-1,3- § 185.2250 Dimethyl phosphate of 3- benzodioxol-4-ol methylcarbamate. hydroxy-N-methyl-cis-crotonamide. (a) The insecticide 2,2-dimethyl-1,3- A tolerance of 2 parts per million is benzodioxol-4-ol methylcarbamate may established for residues of the insecti- be safely used in spot and/or crack and cide dimethyl phosphate of 3-hydroxy- crevice treatments in food handling es- N-methyl-cis-crotonamide in con- tablishments, including food service, centrated tomato products when manufacturing and processing estab- present therein as a result of applica- lishments, such as restaurants, cafe- tion of the insecticide to growing to- terias, supermarkets, bakeries, brew- matoes. eries, dairies, meat slaughtering and packing plants, and canneries. (Sec. 409(c) (1) & (4), Federal Food, Drug, and Cosmetic Act (21 U.S.C. 348(c) (1) & (4)), (b) To ensure safe use of the additive, transferred to the Administrator EPA in Re- its label and labeling shall conform to organization Plan No. 3 of 1970 (35 FR 15623)) that registered with the U.S. Environ- [40 FR 18168, Apr. 25, 1975. Redesignated at 41 mental Protection Agency and it shall FR 26568, June 28, 1976. Redesignated at 53 be used in accordance with such label FR 24667, June 29, 1988] and labeling. § 185.2500 Diquat. (Sec. 409(c)(1) of the Federal Food, Drug, and Cosmetic Act (21 U.S.C. 348(c)(1) transferred (a) A tolerance of 0.01 ppm is estab- to the Administrator EPA in Reorganization lished for residues of the herbicide Plan No. 3 (35 FR 15623)) diquat (6,7-dihydrodipyrido (1,2-a:2′,1′-c) [40 FR 45163, Oct. 1, 1975. Redesignated at 41 pyrazidiinium) derived from applica- FR 26568, June 28, 1976, and amended at 53 FR tion of the dibromide salt in potable 8874, Mar. 18, 1988. Redesignated at 53 FR water resulting from the application of 24667, June 29, 1988] the pesticide for control of aquatic weeds in ponds, lakes, reservoirs, § 185.2200 O,O-Dimethyl O-(4-nitro-m- marshes, bayous, drainage ditches, ca- tolyl) phosphorothioate. nals, streams, and rivers which are (a) A tolerance of 30 parts per mil- slow-moving or quiescent in programs lion, of which no more than 15 parts of the Corps of Engineers or other Fed- per million is O,O-dimethyl O-(4-nitro- eral or State public agencies. These m-tolyl) phosphorothioate or O,O-di- agencies or contractors or licensees methyl O-(4-nitro-m-tolyl) phosphate, under their direct control will make is established for combined residues of certain that the treated water will not the insecticide O,O-dimethyl O-(4- be used for animal consumption, swim- nitro-m-tolyl) phosphorothioate and its ming, spraying, domestic purposes, or metabolites O,O-dimethyl O-(4-nitro-m- for irrigation for 14 days post-treat- tolyl) phosphate and 3-methyl-4- ment or until approved analysis shows nitrophenol in wheat gluten resulting that the water does not contain more from postharvest application of the in- than 0.01 ppm of diquat (calculated as secticide to stored wheat in Australia. the cation) and that no treatment will (b) [Reserved] be made where commercial processing of fish resulting in the production of [44 FR 40282, July 10, 1979, as amended at 53 fish protein concentrate or fish meal is FR 8874, Mar. 18, 1988. Redesignated at 53 FR practiced. 24667, June 29, 1988] (b) A tolerance of 0.01 ppm is established for residues of the herbicide § 185.2225 O,O-Dimethyl S-[4-oxo-1,2,3- diquat (6,7-dihydrodipyrido (1,2-a:2′,1′-c) benzotriazin-3 (4H)-ylmethyl] pyrazinediium) (calculated as the phosphorodithioate. cation) derived from application of the A tolerance of 1 part per million is dibromide salt in potable water result- established for residues of the insecti- ing from the application of the pes- cide O,O-dimethyl S-[4-oxo-1,2,3-benzo- ticide in ponds, lakes, and drainage triazin-3(4H)-ylmethyl] phosphoro- ditches where there is little or no out- dithioate in soybean oil resulting from flow of water and which are totally application of the insecticide to the under control of the user. The applica- raw agricultural commodity soybeans. tor will make certain that treated

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water will not be used for animal con- [47 FR 20763, June 23, 1982, as amended at 50 sumption, swimming, spraying, irriga- FR 14097, Apr. 10, 1985; 51 FR 31325, Sept. 3, tion, or domestic purposes for 14 days 1986; 53 FR 5367, Feb. 24, 1988. Redesignated post-treatment. For the purposes of at 53 FR 24667, June 29, 1988; 60 FR 32097, June 19, 1995] this paragraph only (§ 185.2500(b)) these applications of diquat are not to be § 185.2750 Ethion. used in aquatic sites in Florida. (c) A food additive regulation of 0.5 Tolerances for residues of the insecti- ′ ′ ′ part per million is established for resi- cide ethion (O,O,O ,O -tetraethyl S,S - dues of diquat in processed potatoes methylene bisphosphorodithioate), in- (includes potato chips). cluding its oxygen analog (S-[[(dieth- oxyphosphinothioyl) thio]methyl]O, O- [46 FR 30339, June 8, 1981, and 47 FR 8007, Feb. diethyl phosphorothioate), when 24, 1982. Redesignated and amended at 53 FR present as a result of its application to 24666, 24668, June 29, 1988; 55 FR 26440, June growing agricultural commodities are 28, 1990] established as follows:

§ 185.2600 Endosulfan. 10 parts per million in dried tea. 4 parts per million in raisins. A tolerance of 24 parts per million is established for combined residues of § 185.2800 2-[1-(Ethoxyimino)butyl]-5- the insecticide endosulfan (6,7,8,9,10,10- [2-(ethylthio)propyl]-3-hydroxy-2- hexachloro-1,5,5a,6,9,9a-hexahydro-6,9- cyclohexene-1-one. methano-2,4,3-benzodioxathiepin-3- oxide) and its metabolite endosulfan A food additive regulation is estab- sulfate (6,7,8,9,10,10-hexachloro- lished to permit the combined residues 1,5,5a,6,9,9a-hexahydro-6,9-methano- of the herbicide 2-[1- 2,4,3-benzodioxathiepin-3,3-dioxide) in (ethoxyimino)butyl]-5-[2-(ethyl- or on dried tea (reflecting less than 0.1 thio)propyl]-3-hydroxy-2-cyclohexene- part per million residues in beverage 1-one and its metabolites on the food tea) resulting from application of the commodity tomato products, con- insecticide to growing tea. centrated, at 24.0 parts per million and the food commodities potato flakes and potato granules, at 8.0 parts per mil- § 185.2650 Endothall. lion, and the commodity raisins at 1.0 An interim tolerance of 0.2 part per part per million. million is established for residues of [53 FR 234, Jan. 6, 1988, as amended at 53 FR the herbicide endothall (7- 23388, June 22, 1988. Redesignated at 53 FR oxabicyclo[2.2.1] heptane-2,3-dicarbox- 24667, June 29, 1988; 54 FR 53068, Dec. 27, 1989] ylic acid) in potable water from use of its potassium, sodium, di-N,N- § 185.2850 Ethylene oxide. dimethylalkylamine, and mono-N-N- dimethylalkylamine salts as algicides Ethylene oxide may be safely used as or herbicides to control aquatic plants a fumigant for the control of micro- in canals, lakes, ponds, and other po- organisms and insect infestation in tential sources of potable water. ground spices and other processed natural seasoning materials, except mix- tures to which salt has been added, in § 185.2700 Ethephon. accordance with the following pre- A food additive regulation is estab- scribed conditions: lished permitting residues of the plant (a) Ethylene oxide, either alone or growth regulator ethephon [(2- admixed with carbon dioxide or dichlo- chloroethyl) phosphonic acid] in or on rodifluoromethane, shall be used in the following food commodities: amounts not to exceed that required to accomplish the intended technical ef- Parts per Food million fects. If used with dichlorodifluoromethane, the dichlorodifluoromethane Barley, milling fractions, except flour ...... 5.0 shall conform with the requirements Sugarcane, molasses ...... 1.5 prescribed by 21 CFR 173.355 of this Wheat, milling fractions, except flour ...... 5.0 chapter.

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(b) To assure safe use of the additive, its label and labeling shall conform to Parts that registered with the U.S. Environ- Food per mil- mental Protection Agency and it shall lion be used in accordance with such label or labeling. Citrus oil ...... 25.0 Raisins ...... 0.3 (c) Residues of ethylene oxide in ground spices from both postharvest application to the raw agricultural [48 FR 29839, June 29, 1983. Redesignated at 53 commodity whole spices and applica- FR 24667, June 29, 1988] tion to the ground spices shall not exceed the established tolerance of 50 § 185.3000 O-Ethyl O-[4-(methylthio) parts per million for residues in whole phenyl] S-propyl phosphorodithio- spices in 40 CFR 180.151. ate. A tolerance of 1 part per million is [40 FR 14156, Mar. 28, 1975. Redesignated at 41 FR 26568, June 28, 1976, and amended at 50 FR established for residues of the insecti- 2958, Jan. 23, 1985. Redesignated and amended cide O-ethyl O-[4-(methylthio)- phenyl] at 53 FR 24666, 24668, June 29, 1988] S-propyl phosphorodithioate and its cholinesterase-inhibiting metabolites EFFECTIVE DATE NOTE: At 61 FR 12009, Mar. 22, 1996, § 185.2850 was removed, effective May in cottonseed oil resulting from appli- 21, 1996. At 61 FR 25154, May 20, 1996, the re- cation of the pesticide to growing cot- moval was stayed indefinitely. ton. [43 FR 32130, July 25, 1978. Redesignated at 53 § 185.2900 Ethyl formate. FR 24667, June 29, 1988] The food additive ethyl formate may be safely used in or on specified dried § 185.3200 Fenarimol. fruits in accordance with the following prescribed conditions: Tolerances are established for combined residues of the fungicide (a) It is used or intended for use in or on raisins and dried Zante currants as fenarimol [alpha-(2-chlorophenyl)- a bulk and package fumigant. alpha-(4-chlorophenyl)-5-pyrimidine- (b) It is used in accordance with di- methanol] and its metabolites, alpha- rections registered with the U.S. Envi- (2-chlorophenyl)-alpha-(4-chloro- ronmental Protection Agency, and so phenyl)-1,4-dihydro-5-pyrimidine- used that the total formic acid present methanol and 5-[(2-chlorophenyl) (4- free and combined, in the finished chlorophenyl)methyl]-3,4-dihydro-4-py- product shall not exceed 250 parts per rimidinol measured as the total of million. fenarimol and 5-[(2-chlorophenyl)-(4- (c) To assure safe use of the additive, chlorophenyl) methyl]pyrimidine (cal- its label and labeling shall conform to culated as fenarimol) in or on the fol- that registered with the U.S. Environ- lowing food additive commodities: mental Protection Agency. Parts per Commodity million § 185.2950 Ethyl 3-methyl-4- (methylthio)phenyl (1-methylethyl)- Grape juice ...... 0.6 phosphoramidate. Raisins ...... 0.6 Tolerances are established for the [53 FR 44403, Nov. 3, 1988] combined residues of the nematocide ethyl 3-methyl-4-(methylthio)phenyl (1-methylethyl)-phosphoramidate and § 185.3225 Fenpropathrin. its cholinesterase-inhibiting A food additive tolerance is estab- metabolites ethyl 3-methyl-4-(methyl- lished for residues of the pesticide sulfinyl)phenyl (1-methylethyl)-phos- chemical fenpropathrin (alpha-cyano-3- phoramidate and ethyl 3-methyl-4- phenoxybenzyl 2,2,3,3-tetramethyl- (methylsulfonyl)-phenyl (1-methyl- cyclopropanecarboxylate) as follows: ethyl) phosphoramidate in or on the following food commodities:

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Parts per Expiration Parts per Commodity million date Commodities million Expiration date

Cottonseed oil ...... 3.0 Nov. 15, Rice, hull ...... 7.0 April 30, 1998. 1997 Rice, bran ...... 3.0 Do.

[58 FR 19358, Apr. 14, 1993, as amended at 60 FR 9785, Feb. 22, 1995] [60 FR 42458, Aug. 16, 1995, as amended at 61 FR 33044, June 26, 1996] § 185.3250 Fluazifop-butyl. Tolerances are established for resi- § 185.3450 Formetanate hydrochloride. dues of (±)-2-[4-[[5-(trifluoromethyl)-2- A tolerance of 8 parts per million is pyridinyl]oxy]phenoxy]propanoic acid established for residues of the insecti- (fluazifop), both free and conjugated, cide formetanate hydrochloride (m- and of (±)-butyl 2[4-[[5-(trifluoro- [(dimethylamino) methylene amino] methyl)-2-pyr- phenyl methyl-carbamate hydro- idinyl]oxy]phenoxy]propanoate chloride) in dried prunes when present (fluazifop-butyl), all expressed as therein as a result of the application of fluazifop, in or on the following foods: the insecticide to growing plums (fresh prunes).

Parts per § 185.3475 Fumigants for grain-mill Food million machinery.

Cottonseed, oil ...... 0.2 Fumigants may be safely used in or Soybean, oil ...... 2.0 on grain-mill machinery in accordance with the following prescribed condi- [48 FR 19023, Apr. 27, 1983. Redesignated at 53 tions: FR 24667, June 29, 1988] (a) The fumigants consist of methyl bromide. (b) To assure safe use of the fumi- § 185.3385 Flutolanil (N-(3-(1- methylethoxy)phenyl)-2- gant, its label and labeling shall con- (trifluoromethyl)benzamide). form to the label and labeling registered by the U.S. Environmental Pro- (a) A food additive regulation is es- tection Agency. tablished permitting the combined res- (c) Residues of inorganic bromides idues of the insecticide flutolanil, N-(3- (calculated as Br) in milled fractions (1-methylethoxy)phenyl)-2- derived from cereal grain from all fu- (trifluoromethyl)benzamide, and its migation sources, including fumigation metabolites converted to 2- of grain-mill machinery, shall not ex- (trifluoromethyl) benzoic acid and cal- ceed 125 parts per million. culated as flutolanil in or on the following processed food commodity: [40 FR 14156, Mar. 28, 1975. Redesignated at 41 FR 26568, June 28, 1976, and amended at 49 FR Parts per 44459, Nov. 7, 1984. Redesignated at 53 FR Commodity million 24667, June 29, 1988, and amended at 54 FR 6130, Feb. 8, 1989]

Peanut meal ...... 1.0 § 185.3480 Fumigants for processed grains used in production of fer- (b) A time-limited food additive regu- mented malt beverages. lation is established permitting the Fumigants for processed grain may combined residues of the fungicide be safely used, in accordance with the flutolanil N-(3-(1- following conditions. methylethoxy)phenyl)-2- (a) Methyl bromide. Total residues of (trifluoromethyl)benzamide and its inorganic bromides (calculated as Br) metabolites converted to 2- from the use of this fumigant shall not (trifluoromethyl) benzoic acid and cal- exceed 125 parts per milion. culated as flutolanil in or on the fol- (b) Methyl bromide is used to fumi- lowing raw processed food commodity: gate corn grits and cracked rice in the

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production of fermented malt bev- salt of glyphosate for herbicidal pur- erages. poses. (c) To assure safe use of the fumi- Parts per gant, its label and labeling shall con- Food million form to the label and labeling registered by the U.S. Environmental Pro- Oil, palm ...... 0.1 tection Agency, and the usage em- Olives, imported ...... 0.1 Tea, dried ...... 1.0 ployed should conform with such label Tea, instant ...... 7.0 or labeling. (d) The total residue of inorganic bro- (3) Glyphosate (N- mides in fermented malt beverages, re- (phosphonomethyl)glycine) resulting sulting from the use of corn grits and from the application of the cracked rice fumigated with the fumi- isopropylamine salt of glyphosate and/ gant described in paragraph (a)(2) of or the monoammonium salt of this section plus additional residues of glyphosate for herbicidal purposes. inorganic bromides that may be present from uses in accordance with Food Parts per other regulations in this chapter pro- million mulgated under section 408 and/or 409 Wheat milling fractions (excluding flour) ...... 20.0 of the Act, does not exceed 25 parts per million bromide (calculated as Br). (b) [Reserved] [40 FR 14156, Mar. 28, 1975. Redesignated at 41 [48 FR 56577, Dec. 22, 1983, as amended at 53 FR 26568, June 28, 1976, and amended at 49 FR FR 9434, Mar. 23, 1988. Redesignated at 53 FR 44459, Nov. 7, 1984. Redesignated at 53 FR 24667, June 29, 1988, and amended at 57 FR 24667, June 29, 1988, and amended at 54 FR 42701, Sept. 16, 1992; 58 FR 36359, July 7, 1993] 6130, Feb. 8, 1989] § 185.3550 Hexakis. § 185.3500 Glyphosate. A regulation is established permit- (a) Tolerances are established for the ting the combined residues of the in- combined residues of the herbicide secticide hexakis (2-methyl-2-phenyl- glyphosate and the metabolites as indi- propyl) distannoxane and its organotin cated when present therein as a result metabolites calculated as hexakis (2- of the herbicide application to the methyl-2-phenylpropyl) distannoxane growing crops. in or on the following food items: (1) Glyphosate [N-(phosphono-meth- [47 FR 21532, May 19, 1982, as amended at 48 yl)glycine] and its metabolite FR 37204, Aug. 17, 1983; 48 FR 39058, Aug. 29, aminomethylphosphonic acid resulting 1983. Redesignated at 53 FR 24667, June 29, from the application of the 1988; 59 FR 5109, Feb. 3, 1994] isopropylamine salt of glyphosate for herbicidal purposes and/or the sodium § 185.3575 Hexazinone. sesqui salt for plant growth regulator purposes. A food additive tolerance with re- gional registration, as defined in Food Parts per § 180.1(n) and which excludes use of million hexazinone on sugarcane in Florida, is Molasses, sugarcane ...... 30.0 established for combined residues of the herbicide hexazinone (3-cyclohexyl- (2) Glyphosate [N-(phosphono-meth- 6-(dimethylamino)-1-methyl-1,3,5-tri- yl)glycine] and its metabolite amino- azine-2,4(1H,3H)-dione) and its methylphosphonic acid resulting from metabolites (calculated as hexazinone) the application of the isopropylamine in or on the following food commodity:

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canneries where food and food products Commodity Parts per million are held, processed, and served: Pro- Sugarcane, molasses ...... 5.0 vided, That the food is removed or covered prior to such use, and food-processing surfaces are covered during [60 FR 42462, Aug. 16, 1995] treatment or thoroughly cleaned before using. § 185.3600 Hydrogen cyanide. (b) To assure safe use of the insect The food additive hydrogen cyanide browth regulator, its label and labeling may be present as a residue in certain shall conform to that registered by the processed foods in accordance with the U.S. Environmental Protection Agen- following prescribed conditions: cy, and it shall be used in accordance (a) The food additive is present as a with such label and labeling. result of its use as a fumigant. (b) The residues of hydrogen cyanide [57 FR 36006, Aug. 12, 1992] shall not exceed the following levels: (1) 125 parts per million in cereal § 185.3650 Imazalil. flours. Tolerances are established for the (2) 90 parts per million in cereals that combined residues of the fungicide are cooked before being eaten. imazalil 1-[2-(2,4-dichlorophenyl)-2-(2- (3) 50 parts per million in uncooked ham, bacon, and sausage. propenyloxy)ethyl]-1H-imidazole and (4) 200 parts per million in cocoa. its metabolite 1-(2,4-dichlorophenyl)-2- (c) Where tolerances are established (1H-imidazole-1-yl)-1-ethanol in or on under both sections 408 and 409 of the the following food commodity: Act on the raw agricultural commodity and on the processed food, respectively, the total residues of hydrogen cyanide Parts in or on the processed food shall not be Food per bonter than that designated in para- million boaph (b) of this section. Citrus oil ...... 25.0 (d) To assure safe use of the additive, the label and labeling of the pesticide formulation containing the food addi- [48 FR 28433, June 22, 1983. Redesignated at 53 FR 24667, June 29, 1988] tive shall conform to the label and labeling registered by the U.S. Environ- § 185.3700 Inorganic bromide. mental Protection Agency. The food additive inorganic bromide § 185.3625 Hydroprene; tolerances for may be present as a residue in certain residues. processed foods in accordance with the following conditions: A tolerance of 0.2 part per million is established for combined residues of (a) When the food additive is present both racemic components of as a result of fumigation of the proc- hydroprene, namely [(R)-(Ethyl essed food with methyl bromide or (2E,4E,)-3,7,11-trimethyl-2,4-d- from such fumigation in addition to odecadienoate)] and [(S)-(Ethyl the authorized use of methyl bromide (2E,4E,)-3,7,11-trimethyl-2,4-do- on the source raw aboicultural com- decadienoate)] on all food items in modity, as provided for in 40 CFR part food-handling establishments in ac- 180, the total residues of inorganic bro- cordance with the following prescribed mides (calculated as Br) shall not ex- conditions: ceed the following levels: (a) Application shall be limited sole- 400 parts per million in or on dried eggs and ly to spot or crack and crevice treat- processed herbs and spices. ment in food-handling establishments, 325 parts per million in or on parmesan including food service, manufacturing, cheese and roquefort cheese. and processing establishments such as 250 parts per million in or on concentrated restaurants, cafeterias, supermarkets, tomato products and dried figs. bakeries, breweries, dairies, meat 125 parts per million in or on processed foods slaughtering and packing plants, and other than those listed above.

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(b) [Reserved] crops) in food-handling establishments (c) When the food additive is present where food products are held, proc- in fermented malt beverages in accord- essed, or prepared. ance with §§ 185.3480 and/or 21 CFR (2) Application shall be limited solely 172.730(a)(2) of this chapter, the amount to spot and/or crack and crevice treat- shall not exceed 25 parts per million ment with a spray solution maximum (calculated as Br). of a 0.06-percent active ingredient by (d)—(v) [Reserved] weight. Food must be removed or cov- (w) Where tolerances are established ered during treatment. Spray should under sections 408 and 409 of the not be applied directly to surfaces or FFDCA on both the raw agricultural utensils that may come into contact commodities and processed foods made with food. Food-contact surfaces and therefrom, the total residues of inor- equipment should be thoroughly ganic bromides in or on the processed cleaned with an effective cleaning food shall not be greater than those compound and rinsed with potable designated in paragraphs (a) of this water before using. section, unless a higher level is established elsewhere in this part or in part (3) For spot treatment, a coarse low- 180. pressure spray shall be used. Limit individual spot treatments to an area no [40 FR 14156, Mar. 28, 1975. Redesignated at 41 larger than 20 percent of the surface FR 26568, June 28, 1976, and amended at 49 FR area. Any individual spot treatment 17149, Apr. 23, 1984; 50 FR 2958, Jan. 23, 1985; shall not exceed 2 square feet. 50 FR 3755, Jan. 28, 1985. Redesignated and amended at 53 FR 24666, 24668, June 29, 1988; (4) For crack and crevice treatment, 53 FR 52709, Dec. 29, 1988] equipment capable of delivering a pin- stream of spray directly into the § 185.3750 Iprodione. cracks and crevices shall be used. (5) To assure safe use of the additive, Tolerances are established for the its label and labeling shall conform to combined residues of the fungicide that registered with the U.S. Environ- iprodione [3–(3,5–dichlorophenyl)–N–(1– mental Protection Agency, and it shall methylethyl)–2,4–dioxo–1–imidaz- be used in accordance with such label olidinecarboxamide], its isomer [3–(1– and labeling. methyl-ethyl)–N–(3,5–dichlorophenyl)– 2,4–dioxo–1–imidazolidinecarboxamide], (b) A food additive tolerance is estab- and its metabolite [3–(3,5–dichloro- lished for residues of the insecticide [1 α α ± phenyl)–2,4–dioxo–1–imidazolidinecar- (S*),3 (Z)]-( )-cyano-(3-phenoxyl- boxamide in or on the following food phenyl)methyl 3-(2-chloro-3,3,3- commodity: trifluoro-1-propenyl)-2,2-dimethylcyclopropanecarboxylate as follows: Food Parts per million Parts per Commodity million Ginseng, dried ...... 4.0 Raisins ...... 300 Hops, dried ...... 10.0

[50 FR 4208, Jan. 30, 1985, as amended at 52 (c) A tolerance, to expire on Novem- FR 10562, Apr. 2, 1987. Redesignated at 53 FR ber 15, 1997, is established for the com- 24667, June 29, 1988] bined residues of the insecticide lambda-cyhalothrin and its epimer ex- § 185.3765 Lambda-cyhalothrin. pressed as lambda-cyhalothrin, a 1:1 (a) A food additive tolerance of 0.01 mixture of (S)-α-cyano-3- part per million is established for resi- phenoxybenzyl-(Z)-(1R,3R)-3-(2-chloro- dues of the insecticide [1α(S*),3α(Z)]- 3,3,3-trifluoroprop-1-enyl)-2,2- (±)-cyano(3-phenoxyphenyl)methyl 3-(2- dimethylcyclopropanecarboxylate and chloro-3,3,3-trifluoro-1-propenyl)-2,2- (R)-α-cyano-3-phenoxybenzyl-(Z)- dimethylcyclopropanecarboxylate (1S,3S)-3-(2-chloro-3,3,3-trifluoroprop-1- (lambdacyhalothrin) as follows: enyl)-2,2- (1) In or on all food items (other than dimethylcyclopropanecarboxylate and those already covered by a higher tol- its epimer of lambda-cyhalothrin, a 1:1 erance as a result of use on growing mixture of (S)-α-cyano-3-

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phenoxybenzyl-(Z)-(1S,3S)-3-(2-chloro- (c) Residues of phosphine in or on 3,3,3-trifluoroprop-1-enyl)-2,2- processed foods do not exceed 0.01 part dimethylcyclopropanecarboxylate and per million. (R)-α-cyano-3-phenoxybenzyl-(Z)- [43 FR 56040, Nov. 30, 1978. Redesignated at 53 (1R,3R)-3-(2-chloro-3,3,3-trifluoroprop-1- FR 24667, June 29, 1988] enyl)-2,2- dimethylcyclopropanecarboxylate in or on the following food commodities: § 185.3850 Malathion. Malathion may be safely used in ac- Parts per cordance with the following conditions: Food million (a)(1) It is incorporated into paper trays in amounts not exceeding 100 Corn, grain flour ...... 0.15 Sunflower, oil ...... 0.30 milligrams per square foot. Wheat, bran ...... 0.2 (2) Treated paper trays are intended for use only in the drying of grapes [56 FR 6988, Feb. 21, 1991, as amended at 57 (raisins). FR 32441, July 22, 1992. Redesignated and (3) Total residues of malathion re- amended at 60 FR 34878, July 5, 1995] sulting from drying of grapes on treated trays and from application to grapes before harvest shall not exceed 12 parts § 185.3775 d-Limonene. per million on processed ready-to-eat The food additive d-limonene may be raisins. safely used in accordance with the fol- (b) Residues of malathion in refined lowing conditions: safflower oil from application to the (a) It is used with the active ingredi- growing safflower plant shall not ex- ents dihydro-5-pentyl-2(3H)-furanone ceed 0.6 part per million. and dihydro-5-heptyl-2(3H)-furanone in insect-repellent tablecloths and in in- § 185.3900 Maleic hydrazide. sect-repellent strips used in food-handling establishments. A food additive known as maleic hy- (b) To assure safe use of the insecti- drazide (1,2-dihydro-3,6-pyrida- cide, its label and labeling shall con- zinedione) may be present in potato form to that registered by the U.S. En- chips when used in accordance with the vironmental Protection Agency, and it following conditions: shall be used in accordance with such (a) The food additive is present as a label and labeling. result of the application of a pesticide formulation containing maleic hydra- [60 FR 16053, Mar. 29, 1995] zide to the growing potato plant in accordance with directions registered by § 185.3800 Magnesium phosphide. the U.S. Environmental Protection The food additive magnesium Agency. phosphide may be safely used in ac- (b) The label of the pesticide formu- cordance with the following prescribed lation containing the food additive conditions: conforms to labeling registered by the U.S. Environmental Protection Agen- (a) It is used to generate phosphine in cy. the fumigation of processed foods. (c) The food additive is present in an (b) To assure safe use of the additive, amount not to exceed 160 parts per mil- it is used in compliance with the label lion by weight of the finished food. and labeling conforming to that registered with the U.S. Environmental Protection Agency. The labeling shall § 185.4000 Metalaxyl. bear a warning to aerate the finished (a) A regulation is established per- food for 48 hours before it is offered to mitting the combined residues of the the consumer. A further warning shall fungicide metalaxyl [N-(2,6-dimethyl- state that under no condition should phenyl)-N-(methoxyacetyl) alanine the formulation containing magnesium methyl ester] and its metabolites con- phosphide be used so that it or its taining the 2,6-dimethylaniline moiety, unreacted residues will come in con- and N-(2-hydroxy methyl-6-methyl)-N- tact with any processed food. methoxyacetyl)-alanine methylester,

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each expressed as metalaxyl, in or on (a) The food additive is applied as a the following food commodities: preharvest spray or dust on growing strawberries at a rate of not more than Parts per Food million 1 pound per acre, calculated as metaldehyde, and applied not later than 14 Apricots (dried) ...... 4.0 days before first picking. Citrus, oil ...... 7.0 (b) A tolerance of zero is established Potatoes, processed (including potato chips) ...... 4.0 Prunes (dried) ...... 4.0 for residues of metaldehyde on straw- Raisins ...... 6.0 berries. Tomatoes, processed ...... 3.0 (c) To insure safe usage of the additive: (b) Indirect or inadvertent tolerances. (1) The label of any market package Tolerances are established for indirect of the additive shall bear, in addition or inadvertent residues of metalaxyl in to other information required by the the food commodities when present act, the name of the additive. therein as a result of the application of (2) The label of any prepared mix or metalaxyl to growing crops listed in 40 concentrate shall indicate the percent- CFR 180.408(a) and other non-food crops age by weight of the additive. as listed below: (3) The label shall bear adequate directions for use, in conformance with Food Parts per million paragraph (a) of this section and may Barley, milling fractions ...... 1.0 indicate that in the event the metalde- Oat milling fractions ...... 1.0 hyde is removed by rain an additional Wheat, milling fractions ...... 1.0 application may be made provided such application is made not less than 14 (c) [Reserved] days before first picking. (d) A food additive regulation is established for residues of the fungicide § 185.4035 Metarhizium anisopliae metalaxyl, [N-(2,6-dimethylphenyl)-N- strain ESF1. (methoxyacetyl)alanine methyl ester], and its metabolites containing the 2,6- A food additive regulation is estab- dimethylaniline moiety, and N-(2- lished allowing the use of the microbial hydroxymethyl-6-methylphenyl)-N- pest-control agent Metarhizium (methoxyacetyl) alanine methyl ester, anisopliae strain ESF1 as follows: each expressed as metalaxyl, in or on (a) Metarhizium anisopliae strain the following processed foods when ESF1 may be present as a residue in present therein as a result of applica- food items as a result of application of tion to growing hops: Metarhizium anisopliae strain ESF1 in food-handling establishments, includ- Food Parts per ing food service, manufacturing, and million processing establishments such as res- Hops, dried ...... 20 taurants, cafeterias, supermarkets, bakeries, breweries, dairies, meat- [48 FR 3587, Jan. 26, 1983, as amended at 50 slaughtering and packing plants, and FR 49688, Dec. 4, 1985; 52 FR 41418, Oct. 28, canneries where food and food products 1987; 52 FR 42760, Nov. 6, 1987; 53 FR 8874, are held, processed, and served. Mar. 18, 1988. Redesignated at 53 FR 24667, June 29, 1988, and amended at 54 FR 12445, (b) Application shall be limited sole- Mar. 27, 1989; 55 FR 14833, Apr. 19, 1990; 55 FR ly to placement of attractant stations 26440, June 28, 1990; 56 FR 2442, Jan. 23, 1991; containing Metarhizium anisopliae 56 FR 65003, Dec. 13, 1991; 58 FR 30123, May 26, strain ESF1 in food-handling establish- 1993] ments. (c) To ensure safe use of the micro- § 185.4025 Metaldehyde. bial pest control agent, its label and la- The food additive metaldehyde may beling shall conform to that registered be safely used as a preharvest spray or by the U.S. Environmental Protection dust on strawberries to control slugs Agency, and it shall be used in accord- and snails, in accordance with the fol- ance with such label and labeling. lowing prescribed conditions: [58 FR 29121, May 19, 1993]

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§ 185.4100 Methomyl. dried fruits in accordance with the following prescribed conditions: A food additive tolerance of 12 parts per million is established for residues (a) It is used or intended for use in or of the insecticide methomyl (S-methyl- on raisins and dried Zante currants as N-[ (methylcarbomyl) a bulk and package fumigant. oxy]thioacetimidate) in or on the proc- (b) It is used in accordance with di- essed commodity dried hops as a result rections registered with the U.S. Envi- of application to the growing hops. ronmental Protection Agency, and so There are no United States registra- used that the total formic acid present, tions for use of methomyl on hops, as free and combined in the finished prod- of February 14, 1990. uct shall not exceed 250 parts per million. [55 FR 5220, Feb. 14, 1990] (c) To assure safe use of the additive, its label and labeling shall conform to § 185.4150 Methoprene. that registered with the U.S. Environ- A tolerance of 10 parts per million is mental Protection Agency. established for residues of isopropyl (E,E)-11-methoxy-3,7,11-trimethyl-2,4- § 185.4350 Myclobutanil. dodecadienoate) in or on the food additive commodity cereal grain milled Tolerances are established for com- fractions (except flour and rice hulls). bined residues of the fungicide myclobutanil [alpha-butyl-alpha-(4- [60 FR 42460, Aug. 16, 1995] chlorophenyl)-1H-1,2,4-triazole-1- propanenitrile] and its metabolite § 185.4200 1-Methoxycarbonyl-1- alpha-(3-hydroxybutyl)-alpha-(4- propen-2-yl dimethylphosphate and chlorophenyl)-1H-1,2,4-triazole-1- its beta isomer. propanenitrile (free and bound) in or on A tolerance of 4 parts per million is the following food additive commodity: established for residues of the insecticide 1-methoxycarbonyl-1-propen-2-yl Commodity Parts per dimethylphosphate and its beta isomer million in dehydrated parsley when present as Plums, dried ...... 8.0 a result of application of the insecti- Raisins ...... 10.0 cide to the growing crop. [54 FR 6131, Feb. 8, 1989, as amended at 60 FR § 185.4250 Methyl chloride. 21739, May 3, 1995] The food additive methyl chloride may be safely used in accordance with § 185.4400 Nitrogen. the following prescribed conditions: The food additive nitrogen may be (a) It is used or intended for use as a safely used after harvest in modified propellant in pesticide formulations in atmospheres for stored product insect an amount not to exceed 30 percent of control on all processed agricultural the finished formulation. commodities. (b) It is used or intended for use in food storage and processing areas [46 FR 32866, June 25, 1981. Redesignated at 53 whereby spray applications do not con- FR 24667, June 29, 1988] tact fatty foods. § 185.4450 Norflurazon. (c) To assure safe use of the additive, the label and labeling of the pesticide A regulation is established for the formulation containing the food addi- combined residues of the herbicide tive shall conform to the label and la- norflurazon (4-chloro-5-(methylamino)- beling registered by the U.S. Environ- 2-(alpha, alpha, alpha-trifluoro-m- mental Protection Agency. tolyl)-3(2H)-pyridazinone) and its desmethyl metabolite (4-chloro-5- § 185.4300 Methyl formate. amino-2-(alpha, alpha, alpha-trifluoro- m-tolyl)-3(2H)-pyridazinone) in dried The food additive methyl formate hops at 3.0 parts per million when may be safely used in or on specified

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present therein as a result of its appli- § 185.4800 Phosalone. cation to the growing crop. Tolerances are established for resi- [47 FR 14896, Apr. 7, 1982. Redesignated at 53 dues of the insecticide phosalone (S-(6- FR 24667, June 29, 1988] chloro-3-(mercaptomethyl)-2-benzoxa- zolinone) O,O-diethyl phosphorodithio- § 185.4500 N-Octylbicycloheptene ate) in or on the following processed dicarboximide. foods when present therein as a result of application of the insecticide to the The food additive N- growing crops: octylbicycloheptene dicarboximide may be safely used in accordance with 40 parts per million in or on dried prunes. the following prescribed conditions: 20 parts per million in or on raisins. 8 parts per million in or on dried tea. (a) It is used in combination with piperonyl butoxide and pyrethrins for insect control in food-processing and § 185.4850 Picloram. food-storage areas, provided that the Tolerances are established for resi- food is removed or covered prior to dues of picloram [4-amino-3,5,6- such use. trichloropicolinic acid] resulting from (b) Residues in food resulting from the application of the pesticide to the use described in paragraph (a) of growing crops in the following: this section shall not exceed 10 parts Parts per per million of N-octylbicycloheptene Food million dicarboximide, 10 parts per million of Barley, milled fractions (exc flour) ...... 3 piperonyl butoxide, and 1 part per mil- Oats, milled fractions (exc flour) ...... 3 lion of pyrethrins. Wheat, milled fractions (exc flour) ...... 3 (c) To assure safe use of the additive, its label and labeling shall conform to [41 FR 19211, May 11, 1976. Redesignated at 41 that registered with the U.S. Environ- FR 26568, June 28, 1976, and at 53 FR 24667, mental Protection Agency and it shall June 29, 1988] be used in accordance with such label and labeling. § 185.4900 Piperonyl butoxide. § 185.4650 Paraformaldehyde. The food additive piperonyl butoxide may be safely used in accordance with The food additive paraformaldehyde the following prescribed conditions: may be safely used in accordance with (a) It is used or intended for use in the following prescribed conditions. combination with pyrethrins for con- (a) It is used to control microbial or trol of insects: fungal growth in maple tree tapholes (1) In cereal grain mills and in stor- (b) It is so used that the maple sirup age areas for milled cereal grain prod- produced from the sap of treated maple ucts, whereby the amount of piperonyl trees does not contain in excess of 2 butoxide is at least equal to but not parts per million of formaldehyde. more than 10 times the amount of pyrethrins in the formulation. § 185.4700 Paraquat. (2) On the outer ply of multiwall paper bags of 50 pounds or more capac- A tolerance of 0.2 part per million is ity in amounts not exceeding 60 milli- established for residues of the defo- grams per square foot, whereby the liant, desiccant, and herbicide amount of piperonyl butoxide is equal paraquat (1,1′-dimethyl-4,4′-bipyridini- to 10 times the amount of pyrethrins in um ion) derived from the application of the formulation. Such treated bags are either the bis (methyl sulfate) or di- to be used only for dried foods. chloride salt (both calculated as the (3) On cotton bags of 50 pounds or cation) in or on dried hops resulting more capacity in amounts not exceed- from application of the pesticide to ing 55 milligrams per square foot of growing hops. cloth, whereby the amount of piperonyl [40 FR 43720, Sept. 23, 1975. Redesignated at butoxide is equal to 10 times the 41 FR 26568, June 28, 1976, and at 53 FR 24667, amount of pyrethrins in the formula- June 29, 1988] tion. Such treated bags are constructed

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with waxed paper liners and are to be or on the processed food shall not be used only for dried foods that contain 4 greater than that permitted by the percent fat or less. larger of the two tolerances. (4) In two-ply bags consisting of cel- [40 FR 14156, Mar. 28, 1975. Redesignated at 41 lophane/polyolefin sheets bound to- FR 26568, June 28, 1976, and amended at 50 FR gether by an adhesive layer when it is 2958, Jan. 23, 1985. Redesignated at 53 FR incorporated in the adhesive. The 24667, June 29, 1988] treated sheets shall contain not more than 50 milligrams of piperonyl § 185.4950 Pirimiphos-methyl. butoxide per square foot (538 milligrams per square meter). Such treated (a) Tolerances are established for the bags are to be used only for packaging combined residues of the insecticide prunes, raisins, and other dried fruits pirimiphos-methyl (O-[2-diethylamino- and are to have a maximum ratio of 6-methyl-4-pyrimidinyl] O,O-dimethyl 3.12 milligrams of piperonyl butoxide phosphorothioate) and its metabolite per ounce of fruit (0.10 milligram of O-(2-ethylamino-6-methyl-pyrimidin-4- piperonyl butoxide per gram of prod- yl) O,O-dimethyl phosphorothioate uct). and, in free and conjugated forms, the (5) In food processing and food stor- metabolites 2-diethylamino-6-methyl- age areas: Provided, That the food is re- pyrimidin-4-ol, 2-ethylamino-6-methyl- moved or covered prior to such use. pyrimidin-4-ol, and 2-amino-6-methyl- (b) It is used or intended for use in pyrimidin-4-ol in or on the following combination with pyrethrins and N- processed foods when present therein octylbicycloheptene dicarboximide for as a result of application to stored insect control in accordance with grains: § 178.3730. Parts (c) A tolerance of 10 parts per million per Food mil- is established for residues of piperonyl lion butoxide in or on: (1) Milled fractions derived from ce- Corn milling fractions (except flour) ...... 40 Corn oil ...... 88 real grains when present therein as a Sorghum milling fractions (except flour) ...... 40 result of its use in cereal grain mills and in storage areas for milled cereal (b) A food additive tolerance of 8.0 grain products. parts per million is established for resi- (2) Dried foods when present as a re- dues of the insecticide pirimiphos- sult of migration from its use on the methyl (0-[2-diethylamino-6-methyl-4- outer ply of multiwall paper bags of 50 pyrimidinyl]0,0-dimethyl phos- pounds or more capacity. phorothioate) and its metabolite 0-(2- (3) Foods treated in accordance with ethylamino-6-methyl-pyrimidine-4- § 178.3730. yl)0,0-dimethylphosphorothioate and, (4) Dried foods that contain 4 percent in free and conjugated forms, the fat, or less, when present as a result of metabolites 2-diethylamino-6-methyl- migration from its use on the cloth of pyrimidin-4-ol,2-ethylamino-6-methyl- cotton bags of 50 pounds or more capac- pyrimidin-4-ol, and 2-amino-6-methyl- ity constructed with waxed paper lin- pyrimidin-4-ol in or on the processed ers. commodity wheat flour as a result of (5) Foods treated in accordance with application to stored wheat grain. paragraph (a)(4) and (5) of this section. There are no United States registra- (d) To assure safe use of the additive, tions for use of pirimiphos-methyl on its label and labeling shall conform to wheat, as of June 12, 1990. that registered with the U.S. Environ- mental Protection Agency, and it shall [53 FR 8874, Mar. 18, 1988. Redesignated at 53 be used in accordance with such label FR 24667, June 29, 1988, and amended at 55 FR 23737, June 12, 1990] and labeling. (e) Where tolerances are established under sections 408 and 409 of the Act on § 185.5000 Propargite. both raw agricultural commodities and Tolerances are established for resi- processed foods made therefrom, the dues of the insecticide propargite (2-(p- total residues of piperonyl butoxide in tert-butylphenoxy)cyclohexyl 2-

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propynyl sulfite) in or on the following (a) It is intended as a fumigant in or processed foods when present therein on bulk quantities of cocoa, gums, as a result of the application of this in- processed spices, and processed secticide to growing crops: nutmeats (except peanuts) when such bulk foods are to be further processed Parts per Food million into a final food form. (b) It is applied in fumigation cham- Figs, dried ...... 9 bers not more than one time at a tem- Hops, dried ...... 30 perature not in excess of 125° F. The Tea, dried ...... 10 maximum period of fumigation shall not exceed 4 hours for cocoa, processed [44 FR 38841, July 3, 1979. Redesignated at 53 nutmeats (except peanuts), and proc- FR 24667, June 29, 1988, as amended at 61 FR essed spices. For edible gums, the max- 12009, Mar. 22, 1996] imum duration shall be 24 hours. EFFECTIVE DATE NOTE: At 61 FR 12009, in (c) When used as described in para- § 185.5000, the entries for ‘‘Figs, dried’’ and graphs (a) and (b) of this section, resi- ‘‘Tea, dried’’were removed from the table, ef- dues shall not exceed the following fective May 21, 1996. At 61 FR 25154, May 21, 1996, the removals were stayed indefinitely. limitations: Food Limitations1 § 185.5100 Propetamphos. Cocoa ...... 300 A tolerance of 0.1 part per million is Gums ...... 300 established for residues of the insecti- Processed nutmeats (except peanuts) ...... 300 Spices, processed ...... 300 cide propetamphos ([(e)-]-methylethyl 3-[[(ethylamino) 1 Expressed as parts per million of propylene oxide. methoxyphosphinothioyl]oxy]-2- (d) When used as a mixture with car- butenoate]) in food commodities ex- bon dioxide (92 parts of carbon dioxide posed to the insecticide during treat- to 8 parts of propylene oxide on a ment of food-handling establishments. weight/weight basis), all commodities (a) Direct application shall be lim- listed in paragraph (c) of this section ited solely to spot and/or crack and may be processed not more than one crevice treatment in food-handling es- time for a period not to exceed 48 hours tablishments where food and food prod- and at a temperature not to exceed 125° ucts are held, processed, prepared, or F. served. Spray and dust concentrations (e) To assure safe use of the additive, shall be limited to a maximum of 1 per- the label and labeling of the pesticide cent active ingredient. For crack and formulation containing the food addi- crevice treatment, equipment capable tive shall conform to the label an la- of delivering a dust or a pin-stream of beling registered by the U. S. Environ- spray directly into cracks and crevices mental Protection Agency. shall be used. For spot treatment, a [40 FR 14156, Mar. 28, 1975, as amended at 41 coarse, low-pressure spray shall be used FR 1589, Jan. 9, 1976. Redesignated at 41 FR to avoid contamination of food or food- 26568, June 28, 1976, and amended at 42 FR contact surfaces. 59852, Nov. 22, 1977. Redesignated at 53 FR (b) To ensure safe use of the insecti- 24667, June 29, 1988, as amended at 61 FR cide, its label and labeling shall con- 12009, Mar. 22, 1996; 61 FR 25154, May 20, 1996] form to that registered by the U.S. En- EFFECTIVE DATE NOTE: At 61 FR 12009, vironmental Protection Agency, and it § 185.5150 was removed, effective May 21, 1996. shall be used in accordance with such At 61 FR 25154, May 20, 1996, the removal of label and labeling. the introductory text, paragraphs (a) through (e), and the entries in the table in [48 FR 52902, Nov. 23, 1983. Redesignated at 53 paragraph (c) for ‘‘Cocoa’’, ‘‘Gums’’, ‘‘Proc- FR 24667, June 29, 1988] essed nutmeats (except peanuts)’’, and ‘‘Spices, processed’’ was stayed indefinitely. § 185.5150 Propylene oxide. The food additive propylene oxide § 185.5200 Pyrethrins. may be safely used in or on foods in ac- The food additive pyrethrins may be cordance with the following prescribed safely used in accordance with the fol- conditions: lowing prescribed conditions:

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(a) It is used or intended for use in (2) Dried foods when present as the combination with piperonyl butoxide result of migration from its use on the for control of insects: outer ply of multiwall paper bags of 50 (1) In cereal grain mills and in stor- pounds or more capacity. age areas for milled cereal grain prod- (3) Foods treated in accordance with ucts, whereby the amount of § 185.4500. pyrethrins is from 10 percent to 100 per- (4) Dried foods that contain 4 percent cent of the amount of piperonyl fat, or less, when present as a result of butoxide in the formulation. migration from its use on the cloth of (2) On the outer ply of multiwall cotton bags of 50 pounds or more capac- paper bags of 50 pounds or more capacity constructed with waxed paper lin- ity in amounts not exceeding 6 milli- ers. grams per square foot, whereby the (5) Foods treated in accordance with amount of pyrethrins is equal to 10 per- paragraphs (a)(4) and (a)(5) of this sec- cent of the amount of piperonyl tion. butoxide in the formulation. Such (d) To assure safe use of the additive, treated bags are to be used only for its label and labeling shall conform to dried foods. that registered with the U.S. Environ- (3) On cotton bags of 50 pounds or mental Protection Agency, and it shall more capacity in amounts not exceed- be used in accordance with such label ing 5.5 milligrams per square foot of and labeling. cloth, whereby the amount of (e) Where tolerances are established pyrethrins is equal to 10 percent of the under sections 408 and 409 of the Act on amount of piperonyl butoxide in the both raw agricultural commodities and formulation. Such treated bags are processed foods made therefrom, the constructed with waxed paper liners total residues of pyrethrins in or on and are to be used only for dried foods the processed food shall not be greater that contain 4 percent fat or less. than that permitted by the larger of (4) In two-ply bags consisting of cel- the two tolerances. lophane/polyolefin sheets bound to- [40 FR 14156, Mar. 28, 1975. Redesignated at 41 gether by an adhesive layer when it is FR 26568, June 28, 1976, and further redesig- incorporated in the adhesive. The nated and amended at 53 FR 24666, 24668, treated sheets shall contain not more June 29, 1988] than 10 milligrams of pyrethrins per square foot (107.6 milligrams per square § 185.5250 Quizalofop ethyl. meter). Such treated bags are to be A food additive regulation is estab- used only for packaging prunes, rai- lished to permit the combined residues sins, and other dried fruits and are to of the herbicide quizalofop (2-[4-(6- have a maximum ratio of 0.31 milli- chloroquinoxalin-2-yl oxy) gram of pyrethrins per ounce of fruit phenoxy]propanoic acid) and quizalofop (0.01 milligram of pyrethrins per gram ethyl (ethyl 2-[4-(6-chloroquinoxalin-2- of product). yl oxy)phenoxy] propanoate, all ex- (5) In food processing areas and food pressed as quizalofop ethyl in or on the storage areas: Provided, That the food food commodity soybean flour at 0.5 is removed or covered prior to such part per million (ppm). use. (b) It is used or intended for use in [53 FR 23387, June 22, 1988. Redesignated at 53 FR 24667, June 29, 1988] combination with piperonyl butoxide and N-octylbicycloheptene dicarboximide for insect control in accordance § 185.5300 Resmethrin. with § 185.4500. Tolerances are established for resi- (c) A tolerance of one part per mil- dues of the insecticide resmethrin [5- lion is established for residues of (phenylmethyl)-3-furanyl] methyl 2,2- pyrethrins in or on: dimethyl-3-(2-methyl-1-propenyl) (1) Milled fractions derived from ce- cyclopropanecarboxylate in or on food real grains when present as a result of items at 3.0 ppm resulting from use of its use in cereal grain mills and in stor- the insecticide in food handling and age areas for milled cereal grain prod- storage areas as a space concentration ucts. for spot/or crack and crevice treatment

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and shall be limited to a maximum of lowing food commodities when present 3.00 percent of the active ingredient by as a result of application of the insecti- weight, and as a space treatment shall cide to the growing crops: be limited to a maximum of 0.5 fluid ounce of 3.0 percent active ingredient Commodity Parts per Expiration date by weight per 1000 cubic feet of space million provided that the food is removed or covered prior to such use. To assure Cottonseed oil ...... 0.20 Nov. 15, 1997. safe use of the additive, its label and labeling shall conform to that registered with the U.S. Environmental (b) A time-limited food additive regu- Protection Agency, and shall be used in lation is established permitting resi- accordance with such label and label- dues of the pesticide tralomethrin ((S)- ing. alpha-cyano-3-phenoxybenzyl-(1R,3S)- [48 FR 36247, Aug. 10, 1983. Redesignated at 53 2,2-dimethyl-3-[(RS)-1,2,2,2- FR 24667, June 29, 1988] tetrabromoethyl]- cyclopropanecarboxylate; CAS Reg. No. § 185.5375 Sulfonium, trimethyl-salt 66841-25-6) and its metabolites (S)- with N-(phosphonomethyl)glycine alpha-cyano-3-phenoxybenzyl (1R,3R)-3- (1:1). (2,2-dibromovinyl)-2,2- (a) Food additive regulation is estab- dimethylcyclopropanecarboxylate and lished for residues of the herbicide sul- (S)-alpha-cyano-3- fonium, trimethyl-salt with N- phenoxybenzyl(1S,3R)-3-(2,2- (phosphonomethyl)glycine (1:1) (for- dibromovinly)-2,2- merly glyphosate-trimesium/sulfosate) dimethylcyclopropanecarboxylate cal- in or on the following processed com- culated as the parent in or on the fol- modities: lowing food commodity resulting from application of the insecticide to toma- Parts per Commodities million toes in accordance with an experimental program (34147-EUP-2). The Prunes (of which no more than 0.05 ppm is conditions set forth in this section trimethylsulfonium) ...... 0.2 shall be met. Raisins (of which no more than 0.05 ppm is trimethylsulfonium) ...... 0.20 Parts per Soybean, hulls (of which no more than 2 ppm Commodity million Expiration date is trimethylsulfonium) ...... 7.0

Tomato puree ...... 1.00 June 1, 1997. (b) [Reserved] [61 FR 9359, Mar. 8, 1996, as amended at 61 FR 15900, Apr. 10, 1996] (1) Residues in the food not in excess of the established tolerance resulting from the use described in paragraph (b) § 185.5450 Tralomethrin. of this section remaining after expira- (a) A time-limited food additive regu- tion of the experimental program will lation is established for the combined not be considered to be actionable if residues of the insecticide the insecticide is applied during the tralomethrin ((S)-alpha-cyano-3- term of and in accordance with the pro- phenoxybenzyl-(1R,3S)-2,2-dimethyl-3- visions of the experimental use pro- [(RS)-1,2,2,2-tetrabromoethyl]- cyclopropanecarboxylate; CAS Reg. No. gram and feed additive regulation. 66841-25-6) and its metabolites (S)- (2) The company concerned shall im- alpha-cyano-3-phenoxybenzyl (1R,3R)-3- mediately notify the Environmental (2,2-dibromovinyl)-2,2- Protection Agency of any findings from dimethylcyclopropanecarboxylate and the experimental use that have a bear- (S)-alpha-cyano-3- ing on safety. The firm shall also keep phenoxybenzyl(1S,3R)-3-(2,2- records of production, distribution, and dibromovinly)-2,2- performance, and on request make the dimethylcyclopropanecarboxylate cal- records available to any authorized of- culated as the parent in or on the fol- ficer or employee of the Environmental

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Protection Agency or the Food and shall be used in accordance with such Drug Administration. label and labelling. (c) A food additive tolerance of 0.02 [60 FR 38265, July 26, 1995, as amended at 60 part per million is established for the FR 54612, Oct. 25, 1995] combined residues of the insecticide tralomethrin ((S)-alpha-cyano-3- phenoxybenzyl-(1R,3S)-2,2-dimethyl-3- § 185.5475 Tetradifon. [(RS)-1,2,2,2-tetrabromoethyl] Tolerances are established for resi- cyclopropanecarboxylate) and its dues of tetradifon (2,4,5,4′-tetrachloro- metabolites cis-deltamethrin [(S-alpha- diphenyl sulfone) when present as a re- cyano-3-phenoxybenzyl-(1R,3R)-3-[2,2- sult of its application as a pesticide dibromovinyl)-2,2- chemical to growing agricultural dimethylcyclopropanecarboxylate] and crops, as follows: trans-deltamethrin [(S)-alpha-cyano-3- 120 parts per million in or on dried hops. phenoxybenzyl (1S,3R)-3-(2,2- 10 parts per million in or on dried figs. dibromovinyl)-2,2- 8 parts per million in or on dried tea. dimethylcyclopropanecarboxylate] as follows: § 185.5550 Thiabendazole. (1) In or on all food items (other than those covered by a higher tolerance as A tolerance of 3 parts per million is a result of use on growing crops) in established for residues of the fun- food-handling establishments. gicide thiabendazole [2-(4-thiazolyl) (2) The insecticide may be present as benzimidazole] in or on wheat milled a residue from application of fractions (except flour) resulting from tralomethrin in food-handling estab- applications of the fungicide to grow- lishments, including food service, man- ing wheat. ufacturing, and processing establish- [50 FR 14098, Apr. 10, 1985. Redesignated at 53 ments, such as restaurants, cafeterias, FR 24667, June 29, 1988] supermarkets, bakeries, breweries, dairies, meat slaughtering and packing § 185.5950 Triforine. plants, and canneries in accordance with the following prescribed condi- A food additive regulation is estab- tions: lished to permit residues of the fun- (i) Application shall be limited to a gicide triforine (N,N-[1,4-pipera- general surface and spot and/or crack zinediylbis(2,2,2-trichloroethylidene)] and crevice treatment in food-handling bis[formamide]) in or on the following establishments where food and food processed foods when present therein products are held, processed, prepared, as a result of application to growing and served. General surface application hops: may be used only when the facility is Parts per not in operation provided exposed food Food million has been covered or removed from the Hops, dried ...... 60 area being treated. All food-contact surfaces and equipment must be thoroughly cleaned after general surface [52 FR 39222, Oct. 21, 1987. Redesignated at 53 applications. Spot and/or crack and FR 24667, June 29, 1988] crevice application may be used while the facility is in operation provided ex- § 185.6300 Zinc ion and maneb coordi- posed food is covered or removed from nation product. the area being treated prior to applica- Tolerances are established for resi- tion. Spray concentration shall be lim- dues of a fungicide which is a coordina- ited to a maximum of 0.06 percent ac- tion product of zinc ion and maneb tive ingredient. Contamination of food (manganous and food-contact surfaces shall be ethylenebisdithiocarbamate) contain- avoided. ing 20 percent manganese, 2.5 percent (ii) To assure safe use of the insecti- zinc, and 77.5 percent cide, its label and labelling shall con- ethylenebisdithiocarbamate (the whole form to that registered with the U.S. product calculated as zinc Environmental Protection Agency and ethylenebisdithiocarbamate) in or on

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the following processed foods, when 186.950 2-Chloro-1-(2,4,5- present therein as a result of the appli- trichlorophenyl)vinyl dimethyl phos- cation of this fungicide to growing phate. 186.1000 Chlorpyrifos. crops: 186.1050 Chlorpyrifos-methyl. 20 parts per million in the bran of oats. 186.1075 Clethodim ((E)-(±)-2-[1-[[(3-chloro-2- propenyl)oxy]imino]propyl]-5-[2- [40 FR 14156, Mar. 28, 1975. Redesignated at 41 (ethylthio)propyl]-3-hydroxy-2- FR 26568, June 28, 1976 and 53 FR 24667, June cyclohexen-1-one). 29, 1988, and amended at 59 FR 33694, 33696, 186.1100 Clopyralid. June 30, 1994; 61 FR 12009, Mar. 22, 1996; 61 FR 186.1250 Cyfluthrin. 25154, May 20, 1996] 186.1300 Cyano(3-phenoxyphenyl)methyl 4- EFFECTIVE DATE NOTE: At 61 FR 12009, Mar. chloro-alpha-(1-methyl- 22, 1996, § 185.6300 was removed, effective May ethyl)benzeneacetate. 21, 1996. At 61 FR 25154, May 20, 1996, the re- 186.1350 Cyhexatin. moval of the introductory text and the entry 186.1400 Cyromazine. for ‘‘bran of oats’’ was stayed indefinitely. 186.1450 2,4-D. 186.1500 Dalapon. 186.1650 Dialifor. Subpart C—Food Additives Result- 186.1700 Diatomaceous earth. ing From Contact With Con- 186.1750 Diazinon. tainers or Equipment and 186.1800 Dicamba. 186.1850 3-(3,5-Dichlorophenyl)-5-ethenyl-5- Food Additives Otherwise Af- methyl-2,4-oxazolidinedione. fecting Food 186.1860 3,7-Dichloro-8-quinoline carboxylic acid. § 185.7000 Malathion. 186.1875 Propanil. 186.1950 O,O-Diethyl S-2(ethylthio)ethyl Malathion may be safely used for the phosphorodithioate. control of insects during the drying of 186.1975 Dihydro-5-heptyl-2(3H)-furanone. grapes (raisins) in compliance with 186.1985 Dihydro-5-pentyl-2(3H)-furanone. § 185.3850 by incorporation into paper 186.2000 Diflubenzuron. trays in amounts not exceeding 100 186.2050 Dimethipin. milligrams per square foot. 186.2100 Dimethoate including its oxygen analog. [40 FR 14156, Mar. 28, 1975. Redesignated at 41 186.2150 2,2-Dimethyl-1,3-benzodioxol-4-o1 FR 26568, June 28, 1976, and amended at 50 FR methylcarbamate. 2958, Jan. 23, 1985. Redesignated and amended 186.2225 O,O-Dimethyl S-[4-oxo-1,2,3-benzo- at 53 FR 24666, 24668, June 29, 1988] triazin-3(4H)-yl methyl]phosphorodithioate. 186.2275 N,N-Dimethylpiperidinium chloride. PART 186—PESTICIDES IN ANIMAL 186.2325 O,O-Dimethyl 2,2,2-trichloro-1- FEED hydroxyethyl phosphonate. 186.2400 2,4-Dinitro-6-octylphenyl crotonate Subpart A—[Reserved] and 2,6-dinitro-4-octylphenyl crotonate. 186.2450 Dioxathion. Subpart B—Feed Additives Permitted in 186.2500 Diquat. Animal Feed 186.2550 Diuron. 186.2700 Ethephon. Sec. 186.2750 Ethion. 186.100 Acephate. 186.2775 Ethofumesate. 186.150 Aldicarb. 186.2800 2-[1-(Ethoxyimino)butyl]-5-[2- 186.200 Aluminum phosphide. (ethylthio)propyl]-3-hydroxy-2- 186.250 4-Amino-6-(1,1-dimethylethyl)-3- cyclohexen-1-one. (methylthio)-1,2,4-triazin-5(4H)-one. 186.2950 Ethyl 3-methyl-4-(methyl- 186.300 Avermectin B1 and its delta-8,9-iso- thio)phenyl (1-methylethyl)-phos- mer; tolerances for residues. phoramidate. 186.350 Benomyl. 186.3000 O-Ethyl O-[4-(methylthio)phenyl] S- 186.375 Bentazon. propyl phosphorodithioate. 186.450 sec-Butylamine. 186.3050 S-[2-(Ethylsulfinyl)ethyl] O,O-di- 186.550 Carbaryl. methyl phosphorothioate. 186.600 Carbofuran. 186.3200 Fenarimol. 186.800 1-(4-Chlorophenoxy)-3,3-dimethyl-1- 186.3225 Fenpropathrin. (1H-1,2,4-triazol-1-yl)-2-butanone. 186.3250 Fluazifop-butyl. 186.850 2-(m-Chlorophenoxy)propionic acid. 186.3325 Flumiclorac pentyl; tolerances for 186.900 1-[(6-Chloro-3-pyridinyl) methyl]-N- residues. nitro-2-imidazolidinimine. 186.3350 Fluometuron.

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