EUPT-FV16 Preliminary Results

30th April 2014

Preliminary Results EUPT-Panel DG SANCO Mrs. Almut Bitterhof Mrs. Veerle Vanheusden ORGANISING GROUP Dr. Amadeo R. Fernández-Alba ADVISORY GROUP Dr. Milagros Mezcua Mr. Octavio Malato Dr. Michelangelo Anastassiades Mrs. Carmen Ferrer Mr. Richard Fussell Dr. Miguel Gamón STATISTICAL GROUP Dr. Magnus Jezussek Dr. Carmelo Rodríguez Dr. André de Kok Mr. Ralf Lippold QUALITY CONTROL GROUP Dr. Sonja Masselter Dr. Tuija Pihlström Dr. Antonio Valverde Dr. Mette Erecius Poulsen Mr. Stewart Reynolds Dr. Darinka Stajnbaher

EUPT-FV16 Preliminary Results 30th April 2014 EUPT-FV16 Preliminary Results

30th April 2014

Participation EUPT-FV16 Preliminary Results

30th April 2014

Country No. of Labs Country No. of Labs Country No. of Labs Austria 2 Hungary 4 Serbia 1

Belgium 3 Iceland 1 Singapore 1 Brazil 2 Ireland 1 Slovakia 2

Bulgaria 2 Israel 1 Slovenia 3

China 2 Italy 23 Spain 32

Croatia 7 Kenya 1 Sweden 2

Cyprus 1 Latvia 1 Switzerland 3

Czech Republic 3 Lithuania 1 Thailand 1

Denmark 2 Luxembourg 1 The Netherlands 4

Egypt 1 Norway 1 Turkey 1

Estonia 2 Peru 1 United Kingdom 4

Finland 2 Poland 10 Uruguay 1

France 8 Portugal 2 Total No. of Labs = 183 Total No. of Non-EU countries Labs = 14 Germany 28 Romania 4 Total No. of Countries = 43

Greece 10 Saudi Arabia 1 EU countries, EFTA countries, 3rd countries Participation

Total No. of Labs = 183 Total No. of Countries = 43 EU/EFTA Labs = 169 EU/EFTA countries = 31 Other countries Labs = 14 Other countries = 12

(28 EU + 3 EFTA + 3 Candidate countries + 9 other countries)

EUPT-FV16 Preliminary Results 30th April 2014 EUPT-FV16 Preliminary Results

30th April 2014

175 pesticides Clofentezine Fenarimol Lambda-Cyhalothrin Phosmet oxon 3-hydroxy-carbofuran Clothianidin Fenazaquin Linuron Phoxim Acephate Cyfluthrin Fenbuconazole Lufenuron Pirimicarb Acetamiprid Cypermethrin Fenhexamid Malaoxon Pirimiphos-methyl Acrinathrin Cyproconazole Fenitrothion Malathion Prochloraz Aldicarb Cyprodinil Fenoxycarb Mepanipyrim Procymidone Aldicarb Sulfone Deltamethrin Fenpropathrin Metaflumizone* Profenofos Aldicarb Sulfoxide Demeton-S-methylsulfone Fenpropimorph Metalaxyl and metalaxyl-M Propargite Amitraz Desmethyl-pirimicarb Fenthion Metconazole Propiconazole Azinphos-methyl Diazinon Fenthion oxon Methamidophos Propyzamide Azoxystrobin Dichlofluanid Fenthion oxon sulfone Methidathion Prothioconazole Benfuracarb Dichlorvos Fenthion oxon sulfoxide Methiocarb Prothiofos Bifenthrin Dicloran Fenthion sulfone Methiocarb sulfone Pyraclostrobin Bitertanol Dicofol Fenthion sulfoxide Methiocarb sulfoxide Pyridaben Boscalid Difenoconazole Fipronil Methomyl Pyrimethanil Bromopropylate Diflubenzuron Fludioxonil Methoxyfenozide Pyriproxyfen Flufenoxuron Monocrotophos Quinoxyfen Bromuconazole Dimethoate Spinosad Fluopicolide* Myclobutanil Bupirimate Dimethomorph Spirodiclofen Thiophanate-me Fluquinconazole Omethoate Buprofezin DMST Spiroxamine Tolclofos-methyl Flusilazole Orthophenylphenol Cadusafos* Diphenylamine Tau-Fluvalinate Tolylfluanid Flutolanil* Oxadixyl Captan DMF Tebuconazole Triadimefon Flutriafol Oxamyl Carbaryl DMPF Tebufenozide Triadimenol Folpet Oxydemeton-methyl Carbendazim Endosulfan alpha Tebufenpyrad Triazophos Fosthiazate Paclobutrazole Carbofuran Endosulfan beta Teflubenzuron Trichlorfon Hexaconazole Paraoxon-methyl Carbosulfan Endosulfan sulfate Tefluthrin Trifloxystrobin Hexythiazox Parathion-ethyl Chlorfenapyr EPN Tetraconazole Triflumuron Imazalil Parathion-methyl Chlorfenvinphos Epoxiconazole Tetradifon Trifluralin Imidacloprid Penconazole Chlorobenzilate* Ethion Thiabendazole Triticonazole Indoxacarb Pencycuron Chlorothalonil Ethoprophos Thiacloprid Vinclozolin Iprodione Pendimethalin Chlorpropham Etofenprox Thiamethoxam Zoxamide Iprovalicarb Phenthoate Chlorpyrifos Fenamiphos Thiodicarb Chlorpyrifos-methyl Fenamiphos sulfone Isofenphos-methyl Phosalone *Not in the coordinated Fenamiphos sulfoxide Kresoxim-methyl Phosmet multiannual control programme EUPT-FV16 Preliminary Results

30th April 2014 Pesticides used for the treatment Acetamiprid Endosulfan beta Acrinathrin Fenamiphos Buprofezin Fenhexamid ALL INCLUDED IN MACP

Captan Fludioxonil COMMISSION IMPLEMENTING REGULATION (EU) No 788/2012 of 31 August 2012 concerning a coordinated multiannual control Chlorothalonil Lambda-Cyhalothrin programme of the Union for 2013, 2014 and 2015 to ensure compliance with maximum residue levels of pesticides and to assess the consumer exposure Chlorpyrifos Methoxyfenozide to pesticide residues in and on food of plant and animal origin . Cypermethrin Pirimicarb Cyprodinil Pyridaben Diazinon Spinosad Difenoconazole Tetraconazole Endosulfan alpha Total: 21 CALENDAR

ACTIVITY DATE

- Publishing the Target Pesticide List, Calendar and Matrix on 15th November 2013 the Web page.

- Receiving Application Form from invited laboratories. 23rd Dec 2013 – 31st Jan 2014

- Specific Protocol published on the Web site. 3rd Feb 2014 at the latest

- Deadline for receiving Laboratory scope: Form 0 3rd-14th February 2014

- Sample distribution. 24th February 2014

- Deadline for receiving sample acceptance: Form 1 28th February 2014

- Deadline for receiving results: Forms 2, 3 and 4 17th March 2014

- Filling in Form 5 24th-28th March 2014

- Preliminary Report: only results, no statistical treatment. End of April 2014

- Final Report distributed to the Laboratories. November 2014

EUPT-FV16 Preliminary Results 30th April 2014 Pepper

EUPT-FV16 Preliminary Results 30th April 2014 Organic peppers were grown in the EURL-FV greenhouse in Almería, Spain.

EUPT-FV16 Preliminary Results 30th April 2014 EUPT-FV16 Preliminary Results 30th April 2014 Before harvest, the peppers were treated with commercial formulations

EUPT-FV16 Preliminary Results 30th April 2014 Commercial products used to treat the sample

Pesticide Type Commercial Product Acetamiprid Commercial Formulation Epik 20SG (20%) Acrinathrin Commercial Formulation Jokari (7.5%) Buprofezin Commercial Formulation Geiser (25%) Captan Commercial Formulation Merpan 50 (50%) Chlorothalonil Commercial Formulation Daconil 50 SC (50%) Chlorpyrifos Commercial Formulation Clorifos 48 EC (48%) Cypermethrin Commercial Formulation Citron (10%) Cyprodinil + Fludioxonil Commercial Formulation Switch (37.5%+25%) Diazinon Commercial Formulation Fegazinogole (60%) Difenoconazole Commercial Formulation Core (25%) Endosulfan α y ß Commercial Formulation Sulfanex 35 EC (35%) Fenamiphos Commercial Formulation Nemacur 40LE (40%) Fenhexamid Commercial Formulation Teldor (50%) Lambda Cyhalothrin Commercial Formulation Karate Zeon (1.5%) Methoxyfenozide Commercial Formulation Runner (24%) Pirimicarb Commercial Formulation Aphox (50%) Pyridaben Commercial Formulation Sanmmite 20% (20%) Spinosad Commercial Formulation Spintor 480 SC (48%) Tetraconazole Commercial Formulation Eminent (10%) EUPT-FV16 Preliminary Results 30th April 2014 Preparation of the test item

EUPT-FV16 Preliminary Results 30th April 2014 Homogeneity

- The homogeneity in the treated sample was studied using the 2006 Harmonised Protocol.

20 extracts

-The sampling standard deviation of all the pesticides must be lower than the critical value.

2 Ssample < c All the pesticides passed the homogeneity test EUPT-FV16 Preliminary Results 30th April 2014 Stability 1st Analysis - prior to the sample shipment

2nd Analysis - after the deadline for reporting results

All the pesticides passed the stability test

EUPT-FV16 Preliminary Results 30th April 2014 Stability

Additionally: 3rd Analysis - reproducing the delivery conditions that the samples experienced during 48 hours

EUPT-FV16 Preliminary Results 30th April 2014 EUPT-FV16 Preliminary Results

30th April 2014

Results Acetamiprid Endosulfan beta Acrinathrin Fenamiphos Buprofezin Fenhexamid Captan Fludioxonil Chlorothalonil Lambda-Cyhalothrin Chlorpyrifos Methoxyfenozide Cypermethrin Pirimicarb Cyprodinil Pyridaben Diazinon Spinosad Difenoconazole Tetraconazole Endosulfan alpha

• Endosulfan sulfate

• Fenamiphos sulfone and Fenamiphos sulfoxide

• Pirimicarb-desmethyl

• Propiconazole

• Tebuconazole

EUPT-FV16 Preliminary Results 30th April 2014 Pesticides Robust mean (mg/kg) Lambda-Cyhalothrin 0,078 Diazinon 0,083 Spinosad 0,098 Tetraconazole 0,105 Fenamiphos sulfone 0,109 Captan 0,132 Pyridaben 0,149 Methoxyfenozide 0,170 Pesticides Robust mean (mg/kg) Endosulfan sulfate 0,011 Fludioxonil 0,244 Propiconazole 0,011 Acrinathrin 0,262 Tebuconazole 0,020 Buprofezin 0,469 Desmethyl-pirimicarb 0,027 Cypermethrin 0,527 Cyprodinil 0,588 Acetamiprid 0,636 Pirimicarb 0,730 Fenhexamid 0,855 Difenoconazole 0,945 Endosulfan beta 0,963 Endosulfan alpha 1,149 Chlorothalonil 2,181 Chlorpyrifos 3,667 Fenamiphos sulfoxide 6,641 Fenamiphos 7,277 EUPT-FV16 Preliminary Results 30th April 2014 Pesticides Robust mean (mg/kg)

Endosulfan sulfate 0,011

Propiconazole 0,011

Tebuconazole 0,020

Desmethyl-pirimicarb 0,027

0.011-0.027 mg/kg

EUPT-FV16 Preliminary Results 30th April 2014 Pesticides Robust mean (mg/kg) Lambda-Cyhalothrin 0,078 Diazinon 0,083 0.078-0.100 mg/kg Spinosad 0,098 Tetraconazole 0,105 Fenamiphos sulfone 0,109 Captan 0,132 Pyridaben 0,149 Methoxyfenozide 0,170 Fludioxonil 0,244 Acrinathrin 0,262 Buprofezin 0,469 Cypermethrin 0,527 Cyprodinil 0,588 Acetamiprid 0,636 Pirimicarb 0,730 Fenhexamid 0,855 Difenoconazole 0,945 Endosulfan beta 0,963 Endosulfan alpha 1,149 Chlorothalonil 2,181 Chlorpyrifos 3,667 Fenamiphos sulfoxide 6,641

EUPT-FV16 Preliminary Results Fenamiphos 7,277 30th April 2014 Pesticides Robust mean (mg/kg) Lambda-Cyhalothrin 0,078 Diazinon 0,083 0.078-0.100 mg/kg Spinosad 0,098 Tetraconazole 0,105 Fenamiphos sulfone 0,109 Captan 0,132 Pyridaben 0,149 0.100-0.500 mg/kg Methoxyfenozide 0,170 Fludioxonil 0,244 Acrinathrin 0,262 Buprofezin 0,469 Cypermethrin 0,527 Cyprodinil 0,588 Acetamiprid 0,636 Pirimicarb 0,730 Fenhexamid 0,855 Difenoconazole 0,945 Endosulfan beta 0,963 Endosulfan alpha 1,149 Chlorothalonil 2,181 Chlorpyrifos 3,667 Fenamiphos sulfoxide 6,641

EUPT-FV16 Preliminary Results Fenamiphos 7,277 30th April 2014 Pesticides Robust mean (mg/kg) Lambda-Cyhalothrin 0,078 Diazinon 0,083 0.078-0.100 mg/kg Spinosad 0,098 Tetraconazole 0,105 Fenamiphos sulfone 0,109 Captan 0,132 Pyridaben 0,149 0.100-0.500 mg/kg Methoxyfenozide 0,170 Fludioxonil 0,244 Acrinathrin 0,262 Buprofezin 0,469 Cypermethrin 0,527 Cyprodinil 0,588 Acetamiprid 0,636 Pirimicarb 0,730 Fenhexamid 0,855 > 0.500 mg/kg Difenoconazole 0,945 Endosulfan beta 0,963 Endosulfan alpha 1,149 Chlorothalonil 2,181 Chlorpyrifos 3,667 Fenamiphos sulfoxide 6,641

EUPT-FV16 Preliminary Results Fenamiphos 7,277 30th April 2014 Distribution of data-Histograms

Acetamiprid Acrinathrin

40 40 Mean: 0.636 mg/kg Mean: 0.262 mg/kg

30 30

20 20

Frequency

Frequency

10 10

0 0 0 0,2 0,4 0,6 0,8 1 0 0,2 0,4 0,6 0,8 mg/kg mg/kg Buprofezin Chlorothalonil

50 50 Mean: 0.469 mg/kg Mean: 2.181 mg/kg 40 40

30 30

20

20 Frequency

Frequency

10 10

0 0 0 0,2 0,4 0,6 0,8 1 -1 1 3 5 7 9 11 mg/kg mg/kg EUPT-FV16 Preliminary Results 30th April 2014 Distribution of data-Histograms

Chlorpyrifos Cypermethrin

40 80 Mean: 3.667 mg/kg Mean: 0.527 mg/kg

30 60

20 40

Frequency

Frequency

10 20

0 0 0 0,5 1 1,5 2 2,5 3 0 2 4 6 8 mg/kg mg/kg Cyprodinil Diazinon

40 80 Mean: 0.588 mg/kg Mean: 0.083 mg/kg

30 60

20 40

Frequency

Frequency

10 20

0 0 0 0,2 0,4 0,6 0,8 1 0 0,1 0,2 0,3 0,4 mg/kg mg/kg

EUPT-FV16 Preliminary Results 30th April 2014 Distribution of data-Histograms

Difenoconazole Endosulfan alpha

30 60 Mean: 0.945 mg/kg Mean: 1.149 mg/kg 25 50

20 40

15 30

Frequency 10 Frequency 20

5 10

0 0 0 0,4 0,8 1,2 1,6 -0,1 0,9 1,9 2,9 3,9 mg/kg mg/kg Endosulfan beta Fenamiphos

80 50 Mean: 0.963 mg/kg Mean: 7.277 mg/kg 40 60

30 40 20

Frequency

Frequency

20 10

0 0 -0,1 0,9 1,9 2,9 3,9 -1 3 7 11 15 19 23 mg/kg mg/kg

EUPT-FV16 Preliminary Results 30th April 2014 Distribution of data-Histograms

Fenamiphos sulfone Fenamiphos sulfoxide

50 30 Mean: 0.109 mg/kg Mean: 6.641mg/kg 25 40

20 30 15 20

Frequency Frequency 10

10 5

0 0 0 0,1 0,2 0,3 0,4 -1 2 5 8 11 14 17 mg/kg mg/kg Fenhexamid Fludioxinil

24 40 Mean: 0.855 mg/kg 20 Mean: 0.244 mg/kg 30 16

12 20

Frequency 8 Frequency 10 4

0 0 0 0,3 0,6 0,9 1,2 1,5 0 0,1 0,2 0,3 0,4 0,5 mg/kg mg/kg

EUPT-FV16 Preliminary Results 30th April 2014 Distribution of data-Histograms

Lambda-cyhalothrin Methoxyfenozide

50 20 Mean: 0.078 mg/kg Mean: 0.170 mg/kg 40 16

30 12

20 8

Frequency

Frequency

10 4

0 0 0 0,04 0,08 0,12 0,16 0,2 0,24 0 0,1 0,2 0,3 0,4 mg/kg mg/kg Pirimicarb Pyridaben

40 20 Mean: 0.730 mg/kg Mean: 0.149 mg/kg 16 30

12

20 8

Frequency

Frequency

10 4

0 0 0 0,3 0,6 0,9 1,2 1,5 0,06 0,09 0,12 0,15 0,18 0,21 0,24 mg/kg mg/kg

EUPT-FV16 Preliminary Results 30th April 2014 Distribution of data-Histograms

Spinosad (sum of spinosyn A and spinosyn D, expr. as spinosad) Tetraconazol

50 60 Mean: 0.105 mg/kg Mean: 0.098 mg/kg 50 40

40 30 30

20

Frequency Frequency 20

10 10

0 0 0 0,1 0,2 0,3 0,4 0 0,1 0,2 0,3 0,4 mg/kg mg/kg

EUPT-FV16 Preliminary Results 30th April 2014 Distribution of data-Histograms (special cases)

Tebuconazole Desmethyl-pirimicarb

40 50 Mean: 0.020 mg/kg Mean: 0.027 mg/kg 40 30

30

20 20

Frequency

Frequency

10 10

0 0 0 0,01 0,02 0,03 0,04 0,05 0 0,03 0,06 0,09 0,12 0,15 mg/kg mg/kg Endosulfan sulfate Propiconazole

40 30 Mean: 0.011 mg/kg Mean: 0.011 mg/kg 25 30 20

15 20

Frequency

Frequency 10

10 5

0 0 0,008 0,01 0,012 0,014 0,016 0,018 0,02 0 0,01 0,02 0,03 0,04 mg/kg mg/kg

EUPT-FV16 Preliminary Results 30th April 2014 Distribution of data-Histograms (special cases)

Captan

20 Mean: 0.132 mg/kg 16

12

8

Frequency

4

0 -0,02 0,18 0,38 0,58 0,78 mg/kg

EUPT-FV16 Preliminary Results 30th April 2014 Pesticides MRRL (mg/kg) Robust mean (mg/kg) CV (%)

Acetamiprid 0.01 0,636 15,89 Acrinathrin 0.01 0,262 18,62 Buprofezin 0.01 0,469 13,61 Captan 0.01 0,132 120,09 Chlorothalonil 0.01 2,181 34,39 Chlorpyrifos 0.01 3,667 20,40 Cypermethrin 0.01 0,527 16,45 Cyprodinil 0.01 0,588 14,63 Desmethyl-pirimicarb 0.01 0,027 20,02 Diazinon 0.01 0,083 16,92 Difenoconazole 0.01 0,945 18,71 Endosulfan alpha 0.01 1,149 17,30 Endosulfan beta 0.01 0,963 18,42 Endosulfan sulfate 0.01 0,011 20,71 Fenamiphos 0.01 7,277 21,03 Fenamiphos sulfone 0.01 0,109 19,33 Fenamiphos sulfoxide 0.01 6,641 23,57 Fenhexamid 0.01 0,855 19,84 Fludioxonil 0.01 0,244 18,96 Lambda-Cyhalothrin 0.01 0,078 19,72 Methoxyfenozide 0.01 0,170 21,15 Pirimicarb 0.01 0,730 14,57 Propiconazole 0.01 0,011 14,27 Pyridaben 0.01 0,149 18,17 Spinosad 0.01 0,098 25,18 Tebuconazole 0.01 0,020 17,50 30th April 2014 TetraconazoleEUPT-FV16 Preliminary Results 0.01 0,105 16,02 Pesticides MRRL (mg/kg) Median (mg/kg) Qn (%)

Acetamiprid 0.01 0,632 15,10 Acrinathrin 0.01 0,261 18,75 Buprofezin 0.01 0,467 13,78 Captan 0.01 0,044 51.03 Chlorothalonil 0.01 2,230 32.25 Chlorpyrifos 0.01 3,680 21,11 Cypermethrin 0.01 0,528 16.81 Cyprodinil 0.01 0,591 15,03 Desmethyl-pirimicarb 0.01 0,027 24.67 Diazinon 0.01 0,084 15.86 Difenoconazole 0.01 0,953 19,33 Endosulfan alpha 0.01 1,160 17.22 Endosulfan beta 0.01 0,975 18,00 Endosulfan sulfate 0.01 0,010 22.20 Fenamiphos 0.01 7,385 21.43 Fenamiphos sulfone 0.01 0,110 20.18 Fenamiphos sulfoxide 0.01 6,635 24.39 Fenhexamid 0.01 0,861 20,37 Fludioxonil 0.01 0,241 18.46 Lambda-Cyhalothrin 0.01 0,077 20.18 Methoxyfenozide 0.01 0,165 22,87 Pirimicarb 0.01 0,731 15,18 Propiconazole 0.01 0,010 22,20 Pyridaben 0.01 0,151 17,70 Spinosad 0.01 0,094 23.62 Tebuconazole 0.01 0,020 22.20 30th April 2014 TetraconazoleEUPT-FV16 Preliminary Results 0.01 0,104 17.08 Dispersion of Results

EUPT-FV16 Preliminary Results 30th April 2014 No. of No. of False No. of Not Percentage of Reported Pesticides Reported Negative Analysed Results Results Results Results (out of 169)

Acetamiprid 129 1 39 76 Acrinathrin 136 5 28 80 Buprofezin 145 3 21 86 Chlorothalonil 139 8 22 82 Chlorpyrifos 167 0 2 99 Cypermethrin 154 1 14 91 Cyprodinil 152 1 16 90 Diazinon 164 1 4 97 Difenoconazole 142 0 27 84 Endosulfan alpha 160 2 7 95 Endosulfan beta 159 2 8 94 Fenamiphos 131 3 35 78 Fenamiphos sulfone 102 7 60 60 Fenamiphos sulfoxide 102 7 60 60 Fenhexamid 143 1 25 85 Fludioxonil 138 5 26 82 Lambda-Cyhalothrin 147 6 16 87 Methoxyfenozide 119 2 48 70 Pirimicarb 154 0 15 91 Pyridaben 138 1 30 82 Spinosad 115 1 53 68 TetraconazoleEUPT-FV16 Preliminary Results 139 1 29 8230th April 2014 EUPT-FV16 Preliminary Results

30th April 2014

z-Scores z-Scores classification

%

Acceptable Questionable Unacceptable EUPT-FV16 Preliminary Results 30th April 2014 Robust Mean % Acceptable % Questionable % Unacceptable Pesticides (mg/kg) z-scores z-scores z-scores

Acetamiprid 0,636 98,5 0,8 0,8 Acrinathrin 0,262 89,4 5,0 5,7 Buprofezin 0,469 95,3 1,4 3,4 Chlorothalonil 2,181 83,0 7,5 9,5 Chlorpyrifos 3,667 91,6 6,6 1,8 Cypermethrin 0,527 96,1 2,6 1,3 Cyprodinil 0,588 98,0 1,3 0,7 Diazinon 0,083 96,4 1,2 2,4 Difenoconazole 0,945 96,5 3,5 0,0 Endosulfan alpha 1,149 90,7 3,7 5,6 Endosulfan beta 0,963 90,7 4,3 5,0 Fenamiphos 7,277 88,1 6,0 6,0 Fenamiphos sulfone 0,109 85,3 3,7 11,0 Fenamiphos sulfoxide 6,641 85,3 5,5 9,2 Fenhexamid 0,855 97,2 2,1 0,7 Fludioxonil 0,244 93,0 2,1 4,9 Lambda-Cyhalothrin 0,078 92,2 2,0 5,9 Methoxyfenozide 0,170 95,0 3,3 1,7 Pirimicarb 0,730 98,1 1,9 0,0 Pyridaben 0,149 97,1 2,2 0,7 Spinosad 0,098 86,2 5,2 8,6 TetraconazoleEUPT-FV16 Preliminary Results 0,105 95,0 1,4 3,630th April 2014 AcetamipridAcetamiprid

5,0 0,636 mg/kg 4,0 98,5 % Acceptable 0,8 % Questionable 3,0 0,8 % Unnacceptable 2,0

1,0

0,0

-1,0

-2,0

-3,0

-4,0 1 False negative

-5,0 Lab098 Lab149 Lab018 Lab095 Lab006 Lab169 Lab069 Lab038 Lab073 Lab174 Lab020 Lab093 Lab134 Lab102 Lab119 Lab163 Lab116 Lab117 Lab123 Lab159 Lab051 Lab147 Lab042 Lab019 Lab157 Lab054 Lab167 Lab164 Lab012 Lab062 Lab160 Lab104 Lab033 Lab103 Lab133 Lab118 Lab145 Lab084 Lab101 Lab078 Lab008 Lab182 Lab007 Lab027 Lab128 Lab171 Lab002 Lab024 Lab053 Lab155 Lab050 Lab015 Lab082 Lab001 Lab059 Lab138 Lab165 Lab060 Lab146 Lab031 Lab072 Lab016 Lab009 Lab021 Lab066 Lab106 Lab136 Lab081 Lab047 Lab097 Lab121 Lab139 Lab029 Lab151 Lab056 Lab055 Lab144 Lab130 Lab076 Lab162 Lab068 Lab153 Lab077 Lab010 Lab011 Lab112 Lab110 Lab126 Lab067 Lab079 Lab065 Lab142 Lab183 Lab004 Lab111 Lab140 Lab173 Lab080 Lab105 Lab061 Lab120 Lab003 Lab114 Lab044 Lab063 Lab075 Lab083 Lab122 Lab141 Lab052 Lab178 Lab166 Lab181 Lab028 Lab057 Lab096 Lab030 Lab032 Lab087 Lab025 Lab046 Lab115 Lab017 Lab040 Lab179 Lab070 Lab049 Lab177 Lab013 Lab137 Lab090 Lab034 Lab100 Lab058 Lab099 Lab127 Lab107 Lab091 Lab085 Lab131 Lab041 Lab172 Lab089

EUPT-FV16 Preliminary Results 30th April 2014 AcrinathrinAcrinathrin

5,0 0,263 mg/kg 4,0 89,4 % Acceptable 5,0 % Questionable 3,0 5,7 % Unnacceptable 2,0

1,0

0,0

-1,0

-2,0

-3,0

-4,0 5 False negatives

-5,0 Lab126 Lab139 Lab111 Lab030 Lab169 Lab102 Lab041 Lab065 Lab142 Lab143 Lab146 Lab148 Lab138 Lab154 Lab025 Lab125 Lab002 Lab117 Lab183 Lab105 Lab158 Lab058 Lab020 Lab073 Lab028 Lab178 Lab046 Lab128 Lab096 Lab103 Lab172 Lab042 Lab078 Lab054 Lab060 Lab053 Lab012 Lab051 Lab068 Lab168 Lab066 Lab110 Lab080 Lab122 Lab033 Lab153 Lab179 Lab130 Lab174 Lab015 Lab062 Lab031 Lab134 Lab057 Lab165 Lab136 Lab090 Lab100 Lab127 Lab115 Lab181 Lab044 Lab017 Lab149 Lab108 Lab010 Lab035 Lab162 Lab082 Lab077 Lab011 Lab081 Lab045 Lab069 Lab119 Lab056 Lab101 Lab113 Lab171 Lab018 Lab151 Lab095 Lab167 Lab072 Lab121 Lab097 Lab055 Lab120 Lab086 Lab089 Lab032 Lab123 Lab016 Lab098 Lab063 Lab067 Lab049 Lab129 Lab131 Lab006 Lab163 Lab052 Lab157 Lab161 Lab099 Lab013 Lab093 Lab064 Lab092 Lab008 Lab177 Lab145 Lab133 Lab061 Lab112 Lab084 Lab182 Lab050 Lab059 Lab075 Lab027 Lab009 Lab173 Lab034 Lab074 Lab114 Lab147 Lab085 Lab083 Lab040 Lab107 Lab003 Lab021 Lab106 Lab038 Lab166 Lab118 Lab164 Lab091 Lab140 Lab036 Lab076 Lab150 Lab019 Lab141 Lab160 Lab079 Lab007 Lab070 Lab104

EUPT-FV16 Preliminary Results 30th April 2014 BuprofezinBuprofezin

5,0 0,469 mg/kg 4,0 95,3 % Acceptable 1,4 % Questionable 3,0 3,4% Unnacceptable 2,0

1,0

0,0

-1,0

-2,0

-3,0

-4,0 3 False negatives

-5,0 Lab059 Lab083 Lab092 Lab170 Lab018 Lab157 Lab024 Lab062 Lab023 Lab102 Lab025 Lab174 Lab009 Lab066 Lab130 Lab131 Lab140 Lab164 Lab016 Lab006 Lab139 Lab169 Lab167 Lab064 Lab093 Lab168 Lab002 Lab104 Lab078 Lab116 Lab134 Lab146 Lab123 Lab014 Lab165 Lab048 Lab155 Lab076 Lab182 Lab128 Lab098 Lab141 Lab142 Lab008 Lab033 Lab081 Lab021 Lab084 Lab158 Lab166 Lab172 Lab072 Lab143 Lab178 Lab077 Lab090 Lab122 Lab163 Lab118 Lab151 Lab007 Lab038 Lab065 Lab111 Lab054 Lab015 Lab050 Lab161 Lab120 Lab138 Lab045 Lab105 Lab028 Lab159 Lab160 Lab171 Lab181 Lab073 Lab031 Lab129 Lab019 Lab097 Lab013 Lab088 Lab027 Lab040 Lab082 Lab060 Lab152 Lab029 Lab133 Lab055 Lab099 Lab101 Lab117 Lab119 Lab149 Lab177 Lab061 Lab095 Lab091 Lab049 Lab063 Lab173 Lab179 Lab126 Lab020 Lab068 Lab085 Lab043 Lab089 Lab107 Lab056 Lab086 Lab162 Lab001 Lab137 Lab053 Lab057 Lab147 Lab136 Lab079 Lab080 Lab042 Lab011 Lab034 Lab114 Lab047 Lab036 Lab110 Lab183 Lab145 Lab103 Lab003 Lab153 Lab017 Lab127 Lab069 Lab044 Lab112 Lab046 Lab109 Lab012 Lab032 Lab070 Lab115 Lab030 Lab100 Lab052 Lab051 Lab106 Lab121 Lab010 Lab075 Lab096 Lab150 Lab058 Lab041 Lab035 Lab148 Lab067

EUPT-FV16 Preliminary Results 30th April 2014 ChlorothalonilChlorothalonil

5,0 2,179 mg/kg 4,0 83,0 % Acceptable 7,5 % Questionable 3,0 9,5 % Unnacceptable 2,0

1,0

0,0

-1,0

-2,0

-3,0

-4,0 8 False negatives

-5,0 Lab028 Lab041 Lab073 Lab095 Lab121 Lab135 Lab146 Lab180 Lab157 Lab037 Lab159 Lab158 Lab098 Lab003 Lab102 Lab184 Lab007 Lab165 Lab124 Lab024 Lab174 Lab106 Lab166 Lab168 Lab138 Lab176 Lab042 Lab151 Lab066 Lab120 Lab114 Lab164 Lab080 Lab100 Lab055 Lab069 Lab019 Lab030 Lab078 Lab136 Lab005 Lab062 Lab011 Lab063 Lab051 Lab143 Lab039 Lab072 Lab162 Lab153 Lab017 Lab097 Lab059 Lab126 Lab009 Lab109 Lab054 Lab025 Lab082 Lab130 Lab161 Lab131 Lab155 Lab101 Lab088 Lab081 Lab090 Lab050 Lab092 Lab077 Lab089 Lab179 Lab021 Lab056 Lab075 Lab160 Lab043 Lab139 Lab110 Lab058 Lab099 Lab140 Lab154 Lab049 Lab085 Lab107 Lab149 Lab014 Lab096 Lab152 Lab046 Lab065 Lab145 Lab076 Lab026 Lab112 Lab104 Lab182 Lab119 Lab178 Lab060 Lab016 Lab108 Lab074 Lab177 Lab032 Lab091 Lab079 Lab094 Lab013 Lab053 Lab010 Lab147 Lab002 Lab064 Lab115 Lab125 Lab171 Lab036 Lab052 Lab070 Lab015 Lab061 Lab133 Lab084 Lab103 Lab111 Lab006 Lab001 Lab068 Lab137 Lab033 Lab128 Lab172 Lab113 Lab018 Lab083 Lab087 Lab181 Lab040 Lab163 Lab123 Lab170 Lab167 Lab012 Lab117 Lab173 Lab048 Lab038 Lab031 Lab044 Lab057 Lab035 Lab122 Lab118 Lab020 Lab105 Lab127

EUPT-FV16 Preliminary Results 30th April 2014 ChlorpyrifosChlorpyrifos

5,0 3,667 mg/kg 4,0 91,6 % Acceptable 6,6 % Questionable 3,0 1,8 % Unnacceptable 2,0

1,0

0,0

-1,0

-2,0

-3,0

-4,0 0 False negatives

-5,0 Lab124 Lab073 Lab170 Lab037 Lab158 Lab010 Lab146 Lab135 Lab005 Lab149 Lab157 Lab167 Lab048 Lab174 Lab025 Lab030 Lab081 Lab116 Lab066 Lab078 Lab062 Lab168 Lab159 Lab139 Lab006 Lab022 Lab064 Lab111 Lab123 Lab140 Lab136 Lab102 Lab097 Lab101 Lab151 Lab130 Lab015 Lab058 Lab077 Lab016 Lab134 Lab075 Lab092 Lab023 Lab076 Lab131 Lab082 Lab166 Lab109 Lab169 Lab184 Lab067 Lab088 Lab104 Lab072 Lab094 Lab145 Lab051 Lab065 Lab162 Lab129 Lab056 Lab161 Lab143 Lab142 Lab008 Lab011 Lab032 Lab021 Lab019 Lab002 Lab132 Lab043 Lab059 Lab106 Lab117 Lab150 Lab175 Lab036 Lab177 Lab137 Lab009 Lab040 Lab093 Lab122 Lab049 Lab182 Lab050 Lab080 Lab017 Lab138 Lab120 Lab128 Lab163 Lab165 Lab012 Lab024 Lab038 Lab063 Lab084 Lab061 Lab126 Lab053 Lab090 Lab087 Lab085 Lab003 Lab013 Lab153 Lab141 Lab014 Lab099 Lab172 Lab001 Lab147 Lab183 Lab068 Lab113 Lab042 Lab107 Lab031 Lab091 Lab108 Lab054 Lab154 Lab171 Lab020 Lab033 Lab027 Lab105 Lab086 Lab029 Lab083 Lab118 Lab178 Lab055 Lab103 Lab079 Lab100 Lab044 Lab119 Lab152 Lab089 Lab133 Lab114 Lab070 Lab057 Lab115 Lab155 Lab179 Lab181 Lab028 Lab018 Lab110 Lab047 Lab060 Lab112 Lab045 Lab173 Lab160 Lab098 Lab125 Lab004 Lab095 Lab074 Lab007 Lab096 Lab046 Lab039 Lab052 Lab127 Lab041 Lab180 Lab035 Lab176 Lab148 Lab069 Lab026 Lab034 Lab121 Lab164

EUPT-FV16 Preliminary Results 30th April 2014 Cypermethrin (cypermethrin incl. otherCypermethrin mixtures of constituent isomers (sum of isomers))

5,0 0,528 mg/kg 4,0 96,1 % Acceptable 2,6 % Questionable 3,0 1,3 % Unnacceptable 2,0

1,0

0,0

-1,0

-2,0

-3,0

-4,0 1 False negative

-5,0 Lab003 Lab184 Lab124 Lab146 Lab023 Lab081 Lab024 Lab121 Lab167 Lab028 Lab064 Lab066 Lab157 Lab009 Lab093 Lab118 Lab090 Lab177 Lab102 Lab006 Lab162 Lab123 Lab049 Lab005 Lab065 Lab161 Lab140 Lab082 Lab178 Lab016 Lab143 Lab091 Lab164 Lab138 Lab017 Lab030 Lab151 Lab031 Lab078 Lab139 Lab158 Lab073 Lab166 Lab018 Lab183 Lab088 Lab145 Lab128 Lab134 Lab008 Lab068 Lab076 Lab169 Lab015 Lab083 Lab098 Lab120 Lab150 Lab062 Lab133 Lab002 Lab019 Lab021 Lab059 Lab077 Lab087 Lab108 Lab117 Lab104 Lab036 Lab053 Lab105 Lab131 Lab051 Lab122 Lab153 Lab045 Lab032 Lab048 Lab103 Lab149 Lab060 Lab014 Lab097 Lab092 Lab086 Lab165 Lab056 Lab043 Lab155 Lab159 Lab172 Lab072 Lab033 Lab085 Lab001 Lab027 Lab055 Lab058 Lab142 Lab154 Lab174 Lab013 Lab050 Lab079 Lab095 Lab067 Lab011 Lab063 Lab099 Lab100 Lab126 Lab182 Lab069 Lab089 Lab010 Lab054 Lab112 Lab115 Lab175 Lab107 Lab101 Lab171 Lab181 Lab070 Lab025 Lab119 Lab144 Lab034 Lab113 Lab125 Lab044 Lab074 Lab075 Lab012 Lab020 Lab057 Lab111 Lab173 Lab179 Lab136 Lab137 Lab041 Lab052 Lab046 Lab038 Lab096 Lab163 Lab040 Lab106 Lab035 Lab084 Lab141 Lab116 Lab129 Lab110 Lab039 Lab061 Lab152 Lab026 Lab147 Lab042 Lab007 Lab114 Lab037 Lab168 Lab160 Lab109 Lab148

EUPT-FV16 Preliminary Results 30th April 2014 CyprodinilCyprodinil 0,588 mg/kg 5,0 98,0 % Acceptable 4,0 1,3 % Questionable 3,0 0,7 % Unnacceptable

2,0

1,0

0,0

-1,0

-2,0

-3,0

-4,0 1 False negative

-5,0 Lab170 Lab124 Lab157 Lab160 Lab048 Lab006 Lab159 Lab025 Lab123 Lab165 Lab168 Lab062 Lab102 Lab078 Lab167 Lab082 Lab183 Lab016 Lab023 Lab120 Lab066 Lab174 Lab097 Lab019 Lab011 Lab090 Lab136 Lab155 Lab146 Lab169 Lab002 Lab007 Lab021 Lab140 Lab141 Lab130 Lab009 Lab058 Lab084 Lab158 Lab086 Lab149 Lab081 Lab064 Lab101 Lab108 Lab161 Lab162 Lab077 Lab015 Lab133 Lab131 Lab099 Lab104 Lab151 Lab059 Lab029 Lab008 Lab038 Lab076 Lab030 Lab065 Lab098 Lab103 Lab106 Lab105 Lab001 Lab178 Lab118 Lab112 Lab172 Lab179 Lab121 Lab126 Lab119 Lab056 Lab122 Lab005 Lab166 Lab027 Lab028 Lab111 Lab049 Lab152 Lab153 Lab036 Lab012 Lab091 Lab129 Lab087 Lab116 Lab128 Lab137 Lab139 Lab181 Lab085 Lab031 Lab044 Lab164 Lab057 Lab018 Lab033 Lab050 Lab150 Lab173 Lab060 Lab072 Lab095 Lab068 Lab177 Lab055 Lab083 Lab109 Lab054 Lab020 Lab079 Lab110 Lab003 Lab061 Lab080 Lab047 Lab073 Lab063 Lab093 Lab138 Lab163 Lab046 Lab014 Lab182 Lab145 Lab017 Lab040 Lab089 Lab117 Lab070 Lab107 Lab053 Lab069 Lab092 Lab004 Lab127 Lab114 Lab100 Lab051 Lab039 Lab115 Lab171 Lab013 Lab032 Lab096 Lab052 Lab147 Lab042 Lab088 Lab045 Lab075 Lab043 Lab041 Lab067 Lab148 Lab026 Lab035 Lab034 Lab010

EUPT-FV16 Preliminary Results 30th April 2014 Diazinon 0,084 mg/kg 5,0

4,0 96,4 % Acceptable 1,2 % Questionable 3,0 2,4 % Unnacceptable 2,0

1,0

0,0

-1,0

-2,0

-3,0

-4,0 1 False negative

-5,0 Lab170 Lab124 Lab146 Lab048 Lab139 Lab184 Lab081 Lab165 Lab051 Lab132 Lab140 Lab158 Lab174 Lab088 Lab178 Lab058 Lab097 Lab133 Lab121 Lab134 Lab002 Lab019 Lab102 Lab078 Lab184 Lab023 Lab030 Lab169 Lab009 Lab047 Lab131 Lab066 Lab077 Lab084 Lab092 Lab098 Lab105 Lab123 Lab142 Lab130 Lab060 Lab003 Lab033 Lab076 Lab094 Lab090 Lab104 Lab073 Lab096 Lab151 Lab054 Lab057 Lab062 Lab164 Lab065 Lab021 Lab063 Lab072 Lab001 Lab036 Lab083 Lab111 Lab116 Lab128 Lab154 Lab168 Lab175 Lab167 Lab037 Lab050 Lab086 Lab099 Lab138 Lab162 Lab014 Lab027 Lab034 Lab053 Lab089 Lab106 Lab163 Lab061 Lab087 Lab103 Lab122 Lab143 Lab180 Lab008 Lab044 Lab064 Lab101 Lab109 Lab148 Lab149 Lab183 Lab011 Lab046 Lab059 Lab160 Lab006 Lab016 Lab049 Lab056 Lab137 Lab159 Lab025 Lab068 Lab145 Lab166 Lab126 Lab017 Lab069 Lab075 Lab129 Lab012 Lab013 Lab020 Lab079 Lab005 Lab024 Lab026 Lab038 Lab041 Lab110 Lab150 Lab157 Lab172 Lab173 Lab181 Lab022 Lab085 Lab114 Lab125 Lab177 Lab052 Lab074 Lab147 Lab153 Lab042 Lab182 Lab107 Lab082 Lab141 Lab152 Lab070 Lab136 Lab119 Lab040 Lab004 Lab031 Lab100 Lab118 Lab007 Lab093 Lab029 Lab045 Lab018 Lab028 Lab032 Lab035 Lab055 Lab091 Lab108 Lab115 Lab155 Lab039 Lab043 Lab067 Lab080 Lab120 Lab179 Lab010 Lab112 Lab117 Lab015 Lab095 Lab171 Lab176 Lab135 Lab161

EUPT-FV16 Preliminary Results 30th April 2014 DifenoconazoleDifenoconazole 0,945 mg/kg 5,0

4,0 96,5 % Acceptable 3,5 % Questionable 3,0 0,0 % Unnacceptable

2,0

1,0

0,0

-1,0

-2,0

-3,0

-4,0 0 False negatives

-5,0 Lab124 Lab098 Lab174 Lab006 Lab160 Lab017 Lab157 Lab149 Lab081 Lab023 Lab078 Lab102 Lab151 Lab019 Lab169 Lab018 Lab002 Lab123 Lab062 Lab111 Lab042 Lab066 Lab076 Lab164 Lab016 Lab136 Lab146 Lab140 Lab155 Lab077 Lab009 Lab024 Lab083 Lab008 Lab007 Lab101 Lab030 Lab165 Lab167 Lab097 Lab047 Lab104 Lab021 Lab049 Lab133 Lab181 Lab001 Lab131 Lab072 Lab073 Lab087 Lab128 Lab139 Lab172 Lab046 Lab120 Lab069 Lab138 Lab065 Lab050 Lab118 Lab025 Lab130 Lab162 Lab028 Lab079 Lab114 Lab179 Lab061 Lab031 Lab064 Lab112 Lab182 Lab082 Lab183 Lab036 Lab052 Lab027 Lab051 Lab013 Lab053 Lab137 Lab095 Lab153 Lab055 Lab080 Lab119 Lab063 Lab084 Lab099 Lab107 Lab091 Lab033 Lab093 Lab126 Lab075 Lab057 Lab161 Lab015 Lab040 Lab054 Lab056 Lab122 Lab085 Lab012 Lab059 Lab103 Lab116 Lab068 Lab058 Lab004 Lab142 Lab163 Lab110 Lab177 Lab145 Lab159 Lab020 Lab060 Lab089 Lab141 Lab152 Lab129 Lab070 Lab178 Lab173 Lab038 Lab044 Lab115 Lab117 Lab125 Lab150 Lab171 Lab180 Lab003 Lab029 Lab096 Lab100 Lab121 Lab166 Lab045 Lab011 Lab041 Lab105 Lab147 Lab088 Lab074 Lab048 Lab106 Lab034 Lab067 Lab090 Lab032 Lab148 Lab108

EUPT-FV16 Preliminary Results 30th April 2014 EndosulfanEndosulfan alpha alpha 1,149 mg/kg 5,0

4,0 90,7 % Acceptable 3,7 % Questionable 3,0 5,6 % Unnacceptable

2,0

1,0

0,0

-1,0

-2,0

-3,0

-4,0 2 False negatives

-5,0 Lab003 Lab041 Lab073 Lab156 Lab170 Lab025 Lab157 Lab062 Lab176 Lab124 Lab135 Lab145 Lab184 Lab023 Lab048 Lab081 Lab006 Lab174 Lab076 Lab090 Lab159 Lab162 Lab031 Lab030 Lab168 Lab049 Lab064 Lab019 Lab002 Lab169 Lab082 Lab038 Lab133 Lab009 Lab102 Lab146 Lab111 Lab180 Lab078 Lab120 Lab150 Lab158 Lab015 Lab149 Lab130 Lab131 Lab026 Lab166 Lab136 Lab016 Lab021 Lab151 Lab001 Lab140 Lab123 Lab128 Lab114 Lab086 Lab033 Lab037 Lab129 Lab032 Lab043 Lab083 Lab084 Lab117 Lab134 Lab080 Lab013 Lab101 Lab104 Lab165 Lab152 Lab058 Lab155 Lab010 Lab060 Lab098 Lab077 Lab097 Lab139 Lab178 Lab177 Lab036 Lab072 Lab028 Lab034 Lab164 Lab163 Lab005 Lab088 Lab017 Lab137 Lab182 Lab094 Lab138 Lab093 Lab126 Lab110 Lab079 Lab122 Lab018 Lab119 Lab035 Lab063 Lab085 Lab112 Lab116 Lab161 Lab171 Lab175 Lab181 Lab167 Lab044 Lab055 Lab056 Lab075 Lab113 Lab068 Lab109 Lab091 Lab095 Lab051 Lab054 Lab053 Lab027 Lab153 Lab050 Lab061 Lab147 Lab057 Lab107 Lab144 Lab173 Lab089 Lab179 Lab022 Lab040 Lab099 Lab103 Lab106 Lab125 Lab142 Lab154 Lab141 Lab143 Lab008 Lab046 Lab020 Lab105 Lab096 Lab012 Lab042 Lab065 Lab011 Lab067 Lab087 Lab100 Lab070 Lab160 Lab074 Lab115 Lab121 Lab045 Lab069 Lab052 Lab148 Lab007 Lab118 Lab172 Lab014 Lab066 Lab108 Lab059

EUPT-FV16 Preliminary Results 30th April 2014 EndosulfanEndosulfan betaBeta 0,964 mg/kg 5,0

4,0 90,7 % Acceptable 4,3 % Questionable 3,0 5,0 % Unnacceptable

2,0

1,0

0,0

-1,0

-2,0

-3,0

-4,0 2 False negatives

-5,0 Lab003 Lab041 Lab073 Lab176 Lab156 Lab170 Lab124 Lab135 Lab157 Lab059 Lab145 Lab184 Lab155 Lab030 Lab025 Lab023 Lab081 Lab174 Lab014 Lab064 Lab066 Lab017 Lab062 Lab006 Lab102 Lab162 Lab172 Lab002 Lab048 Lab076 Lab078 Lab123 Lab139 Lab121 Lab111 Lab058 Lab098 Lab158 Lab151 Lab150 Lab120 Lab082 Lab090 Lab033 Lab057 Lab131 Lab130 Lab072 Lab122 Lab149 Lab136 Lab021 Lab179 Lab038 Lab134 Lab146 Lab001 Lab015 Lab019 Lab056 Lab140 Lab181 Lab129 Lab133 Lab105 Lab104 Lab143 Lab177 Lab138 Lab005 Lab109 Lab028 Lab084 Lab166 Lab083 Lab142 Lab144 Lab077 Lab049 Lab009 Lab088 Lab168 Lab079 Lab097 Lab128 Lab036 Lab152 Lab164 Lab091 Lab027 Lab032 Lab034 Lab114 Lab060 Lab137 Lab022 Lab113 Lab171 Lab094 Lab085 Lab035 Lab063 Lab099 Lab112 Lab141 Lab054 Lab075 Lab126 Lab119 Lab165 Lab016 Lab107 Lab178 Lab013 Lab044 Lab154 Lab159 Lab050 Lab067 Lab093 Lab161 Lab182 Lab042 Lab043 Lab061 Lab080 Lab101 Lab031 Lab055 Lab173 Lab086 Lab068 Lab089 Lab020 Lab070 Lab117 Lab065 Lab026 Lab040 Lab087 Lab103 Lab106 Lab147 Lab153 Lab018 Lab118 Lab095 Lab074 Lab160 Lab096 Lab051 Lab110 Lab012 Lab046 Lab116 Lab011 Lab125 Lab175 Lab008 Lab053 Lab037 Lab167 Lab052 Lab100 Lab169 Lab045 Lab180 Lab007 Lab115 Lab010 Lab069 Lab148 Lab108

EUPT-FV16 Preliminary Results 30th April 2014 FenamiphosFenamiphos 7,297 mg/kg 5,0

4,0 88,1 % Acceptable 6,0 % Questionable 3,0 6,0 % Unnacceptable

2,0

1,0

0,0

-1,0

-2,0

-3,0

-4,0 3 False negatives

-5,0 Lab041 Lab083 Lab146 Lab073 Lab069 Lab120 Lab116 Lab149 Lab010 Lab124 Lab184 Lab151 Lab081 Lab025 Lab170 Lab157 Lab021 Lab003 Lab019 Lab165 Lab179 Lab020 Lab014 Lab137 Lab006 Lab002 Lab007 Lab153 Lab166 Lab173 Lab018 Lab118 Lab082 Lab078 Lab030 Lab051 Lab182 Lab155 Lab169 Lab095 Lab101 Lab174 Lab167 Lab072 Lab140 Lab104 Lab145 Lab108 Lab123 Lab062 Lab066 Lab064 Lab084 Lab111 Lab177 Lab131 Lab139 Lab159 Lab054 Lab097 Lab033 Lab122 Lab161 Lab089 Lab009 Lab164 Lab004 Lab012 Lab126 Lab138 Lab117 Lab147 Lab058 Lab061 Lab049 Lab076 Lab085 Lab011 Lab107 Lab016 Lab052 Lab106 Lab091 Lab032 Lab105 Lab063 Lab065 Lab056 Lab077 Lab178 Lab119 Lab053 Lab088 Lab013 Lab099 Lab047 Lab110 Lab050 Lab008 Lab114 Lab093 Lab171 Lab079 Lab059 Lab128 Lab068 Lab057 Lab080 Lab112 Lab133 Lab162 Lab027 Lab115 Lab046 Lab121 Lab023 Lab103 Lab075 Lab045 Lab141 Lab070 Lab040 Lab067 Lab055 Lab028 Lab042 Lab017 Lab136 Lab031 Lab060 Lab029 Lab098 Lab096 Lab127 Lab100 Lab001 Lab183 Lab035 Lab015 Lab160 Lab090 Lab158 Lab039 Lab026 Lab172 Lab034

EUPT-FV16 Preliminary Results 30th April 2014 FenamiphosFenamiphos sulfone sulfone 0,109 mg/kg 5,0

4,0 85,3 % Acceptable 3,7 % Questionable 3,0 11,0 % Unnacceptable

2,0

1,0

0,0

-1,0

-2,0

-3,0

-4,0 7 False negatives

-5,0 Lab004 Lab012 Lab041 Lab059 Lab083 Lab095 Lab146 Lab097 Lab029 Lab166 Lab051 Lab006 Lab073 Lab020 Lab007 Lab061 Lab107 Lab008 Lab131 Lab089 Lab155 Lab047 Lab042 Lab121 Lab028 Lab157 Lab062 Lab096 Lab002 Lab103 Lab123 Lab077 Lab032 Lab128 Lab145 Lab104 Lab084 Lab027 Lab066 Lab085 Lab101 Lab173 Lab076 Lab122 Lab050 Lab080 Lab133 Lab119 Lab015 Lab018 Lab078 Lab060 Lab079 Lab054 Lab056 Lab138 Lab139 Lab001 Lab009 Lab033 Lab063 Lab093 Lab106 Lab115 Lab140 Lab171 Lab172 Lab081 Lab082 Lab100 Lab049 Lab126 Lab151 Lab091 Lab136 Lab016 Lab178 Lab068 Lab110 Lab052 Lab053 Lab057 Lab065 Lab075 Lab153 Lab118 Lab182 Lab167 Lab031 Lab072 Lab023 Lab046 Lab160 Lab019 Lab105 Lab090 Lab070 Lab011 Lab058 Lab112 Lab147 Lab013 Lab017 Lab040 Lab055 Lab067 Lab174 Lab162 Lab021 Lab141 Lab025 Lab069 Lab034 Lab164

EUPT-FV16 Preliminary Results 30th April 2014 FenamiphosFenamiphos sulfoxide sulfoxide 6,625 mg/kg 5,0

4,0 85,3 % Acceptable 5,5 % Questionable 3,0 9,2% Unnacceptable

2,0

1,0

0,0

-1,0

-2,0

-3,0

-4,0 7 False negatives

-5,0 Lab004 Lab041 Lab059 Lab069 Lab083 Lab146 Lab147 Lab162 Lab073 Lab151 Lab170 Lab025 Lab174 Lab061 Lab153 Lab116 Lab021 Lab131 Lab119 Lab095 Lab085 Lab006 Lab020 Lab123 Lab051 Lab107 Lab128 Lab121 Lab078 Lab171 Lab008 Lab106 Lab066 Lab002 Lab053 Lab042 Lab072 Lab082 Lab062 Lab015 Lab034 Lab032 Lab103 Lab079 Lab101 Lab145 Lab133 Lab049 Lab084 Lab028 Lab104 Lab033 Lab122 Lab046 Lab077 Lab050 Lab080 Lab136 Lab167 Lab019 Lab091 Lab011 Lab076 Lab155 Lab110 Lab058 Lab138 Lab070 Lab089 Lab060 Lab029 Lab027 Lab016 Lab141 Lab017 Lab126 Lab166 Lab173 Lab013 Lab182 Lab055 Lab115 Lab057 Lab096 Lab075 Lab040 Lab023 Lab178 Lab097 Lab018 Lab093 Lab054 Lab007 Lab063 Lab112 Lab047 Lab056 Lab001 Lab100 Lab105 Lab052 Lab009 Lab090 Lab157 Lab067 Lab068 Lab139 Lab172 Lab118 Lab065 Lab160 Lab081 Lab140 Lab031 Lab164

EUPT-FV16 Preliminary Results 30th April 2014 FenhexamidFenhexamid

5,0 0,855 mg/kg 4,0 97,2 % Acceptable 2,1 % Questionable 3,0 0,7 % Unnacceptable

2,0

1,0

0,0

-1,0

-2,0

-3,0

-4,0 1 False negative

-5,0 Lab041 Lab024 Lab157 Lab141 Lab007 Lab030 Lab149 Lab048 Lab009 Lab093 Lab077 Lab006 Lab159 Lab032 Lab146 Lab014 Lab180 Lab069 Lab086 Lab123 Lab167 Lab066 Lab169 Lab164 Lab174 Lab073 Lab078 Lab023 Lab182 Lab091 Lab042 Lab002 Lab129 Lab155 Lab105 Lab081 Lab160 Lab062 Lab092 Lab076 Lab016 Lab043 Lab130 Lab015 Lab153 Lab047 Lab099 Lab102 Lab171 Lab036 Lab133 Lab104 Lab051 Lab101 Lab072 Lab165 Lab126 Lab038 Lab065 Lab137 Lab140 Lab005 Lab114 Lab122 Lab004 Lab019 Lab117 Lab136 Lab049 Lab162 Lab025 Lab131 Lab020 Lab111 Lab138 Lab001 Lab027 Lab161 Lab121 Lab166 Lab053 Lab080 Lab178 Lab060 Lab021 Lab116 Lab061 Lab090 Lab008 Lab034 Lab181 Lab118 Lab050 Lab108 Lab127 Lab179 Lab063 Lab067 Lab056 Lab085 Lab013 Lab147 Lab075 Lab031 Lab163 Lab017 Lab119 Lab074 Lab112 Lab152 Lab079 Lab089 Lab068 Lab145 Lab057 Lab103 Lab125 Lab128 Lab100 Lab173 Lab110 Lab012 Lab011 Lab040 Lab058 Lab044 Lab082 Lab059 Lab087 Lab172 Lab107 Lab046 Lab120 Lab095 Lab033 Lab106 Lab183 Lab018 Lab052 Lab097 Lab029 Lab070 Lab084 Lab096 Lab055 Lab064 Lab115 Lab139 Lab177 Lab028 Lab150 Lab088 Lab054 Lab148 Lab151 Lab083

EUPT-FV16 Preliminary Results 30th April 2014 FludioxonilFludioxonil

5,0 0,245 mg/kg 4,0 93,0 % Acceptable 2,1 % Questionable 3,0 4,9 % Unnacceptable 2,0

1,0

0,0

-1,0

-2,0

-3,0

-4,0 5 False negatives

-5,0 Lab004 Lab034 Lab041 Lab069 Lab164 Lab124 Lab018 Lab134 Lab129 Lab067 Lab088 Lab118 Lab064 Lab174 Lab024 Lab032 Lab048 Lab066 Lab149 Lab062 Lab025 Lab030 Lab006 Lab023 Lab002 Lab146 Lab169 Lab081 Lab077 Lab153 Lab078 Lab007 Lab021 Lab108 Lab140 Lab165 Lab097 Lab054 Lab152 Lab178 Lab095 Lab091 Lab131 Lab027 Lab033 Lab087 Lab123 Lab141 Lab157 Lab120 Lab138 Lab105 Lab073 Lab122 Lab145 Lab076 Lab167 Lab063 Lab082 Lab084 Lab101 Lab102 Lab050 Lab130 Lab151 Lab017 Lab046 Lab045 Lab001 Lab072 Lab104 Lab009 Lab011 Lab053 Lab083 Lab086 Lab111 Lab112 Lab161 Lab121 Lab085 Lab160 Lab061 Lab136 Lab126 Lab068 Lab019 Lab040 Lab055 Lab147 Lab031 Lab060 Lab014 Lab044 Lab075 Lab139 Lab128 Lab012 Lab058 Lab093 Lab158 Lab173 Lab181 Lab057 Lab166 Lab090 Lab182 Lab020 Lab042 Lab089 Lab107 Lab051 Lab110 Lab079 Lab115 Lab163 Lab177 Lab133 Lab056 Lab059 Lab099 Lab103 Lab005 Lab003 Lab114 Lab080 Lab070 Lab100 Lab013 Lab038 Lab098 Lab155 Lab183 Lab039 Lab036 Lab008 Lab010 Lab015 Lab172 Lab179 Lab049 Lab119 Lab052 Lab162 Lab096 Lab035 Lab171 Lab065 Lab016 Lab028 Lab150 Lab026 Lab106

EUPT-FV16 Preliminary Results 30th April 2014 LambdaLambda-Cyhalothrin-Cyhalothrin

5,0 0,078 mg/kg 4,0 92,2 % Acceptable 2,0 % Questionable 3,0 5,9 % Unnacceptable

2,0

1,0

0,0

-1,0

-2,0

-3,0

-4,0 6 False negatives

-5,0 Lab003 Lab124 Lab014 Lab034 Lab103 Lab146 Lab148 Lab024 Lab098 Lab139 Lab023 Lab076 Lab049 Lab184 Lab006 Lab178 Lab078 Lab093 Lab151 Lab025 Lab165 Lab058 Lab174 Lab074 Lab138 Lab066 Lab140 Lab145 Lab157 Lab081 Lab163 Lab134 Lab002 Lab062 Lab128 Lab012 Lab016 Lab027 Lab099 Lab136 Lab171 Lab181 Lab060 Lab065 Lab112 Lab121 Lab137 Lab169 Lab001 Lab088 Lab130 Lab133 Lab045 Lab046 Lab079 Lab102 Lab009 Lab031 Lab032 Lab087 Lab123 Lab131 Lab142 Lab158 Lab017 Lab068 Lab057 Lab101 Lab118 Lab183 Lab019 Lab077 Lab149 Lab161 Lab177 Lab053 Lab059 Lab104 Lab172 Lab082 Lab111 Lab166 Lab011 Lab063 Lab064 Lab070 Lab072 Lab110 Lab008 Lab141 Lab144 Lab100 Lab179 Lab021 Lab085 Lab125 Lab107 Lab075 Lab038 Lab044 Lab048 Lab096 Lab147 Lab154 Lab173 Lab119 Lab164 Lab091 Lab126 Lab005 Lab030 Lab061 Lab020 Lab105 Lab106 Lab143 Lab097 Lab113 Lab167 Lab036 Lab040 Lab152 Lab018 Lab050 Lab069 Lab051 Lab067 Lab095 Lab182 Lab084 Lab115 Lab010 Lab028 Lab035 Lab150 Lab033 Lab052 Lab026 Lab086 Lab092 Lab117 Lab120 Lab122 Lab089 Lab015 Lab056 Lab041 Lab055 Lab108 Lab153 Lab162 Lab039 Lab073 Lab054 Lab013 Lab043 Lab083 Lab116 Lab155 Lab168 Lab129 Lab007 Lab042 Lab114 Lab127 Lab160 Lab090

EUPT-FV16 Preliminary Results 30th April 2014 MethoxyfenozideMethoxyfenozide

5,0 0,170 mg/kg 4,0 95,0 % Acceptable 3,3 % Questionable 3,0 1,7 % Unnacceptable

2,0

1,0

0,0

-1,0

-2,0

-3,0

-4,0 2 False negatives

-5,0 Lab083 Lab164 Lab114 Lab157 Lab006 Lab160 Lab019 Lab089 Lab002 Lab020 Lab093 Lab134 Lab081 Lab062 Lab042 Lab100 Lab104 Lab139 Lab078 Lab172 Lab169 Lab097 Lab001 Lab077 Lab131 Lab178 Lab174 Lab007 Lab033 Lab066 Lab106 Lab123 Lab142 Lab031 Lab151 Lab138 Lab050 Lab167 Lab027 Lab111 Lab180 Lab095 Lab165 Lab051 Lab145 Lab073 Lab076 Lab133 Lab054 Lab146 Lab065 Lab120 Lab136 Lab017 Lab025 Lab072 Lab130 Lab016 Lab166 Lab008 Lab009 Lab021 Lab063 Lab082 Lab101 Lab116 Lab122 Lab128 Lab147 Lab162 Lab080 Lab137 Lab011 Lab118 Lab140 Lab029 Lab126 Lab182 Lab061 Lab068 Lab090 Lab044 Lab047 Lab075 Lab032 Lab053 Lab059 Lab117 Lab079 Lab110 Lab121 Lab046 Lab052 Lab067 Lab049 Lab013 Lab070 Lab091 Lab056 Lab058 Lab099 Lab112 Lab060 Lab003 Lab119 Lab183 Lab105 Lab084 Lab030 Lab085 Lab107 Lab177 Lab096 Lab057 Lab127 Lab171 Lab173 Lab179 Lab159 Lab012 Lab024 Lab040 Lab087 Lab103 Lab115 Lab055 Lab041 Lab155 Lab153 Lab149 Lab163 Lab034 Lab141 Lab015

EUPT-FV16 Preliminary Results 30th April 2014 PirimicarbPirimicarb

5,0 0,730 mg/kg 4,0 98,1 % Acceptable 1,9 % Questionable 3,0 0,0 % Unnacceptable

2,0

1,0

0,0

-1,0

-2,0

-3,0 0 False negatives

-4,0 Lab124 Lab149 Lab018 Lab014 Lab048 Lab026 Lab168 Lab006 Lab025 Lab085 Lab174 Lab044 Lab065 Lab102 Lab084 Lab116 Lab119 Lab012 Lab034 Lab120 Lab123 Lab097 Lab093 Lab163 Lab002 Lab143 Lab160 Lab101 Lab131 Lab078 Lab136 Lab036 Lab107 Lab047 Lab099 Lab035 Lab008 Lab167 Lab164 Lab122 Lab023 Lab118 Lab171 Lab121 Lab128 Lab061 Lab007 Lab016 Lab083 Lab103 Lab062 Lab169 Lab022 Lab140 Lab086 Lab003 Lab051 Lab038 Lab066 Lab108 Lab130 Lab088 Lab114 Lab166 Lab027 Lab053 Lab059 Lab153 Lab076 Lab049 Lab137 Lab009 Lab134 Lab141 Lab155 Lab157 Lab180 Lab109 Lab133 Lab033 Lab072 Lab112 Lab104 Lab126 Lab058 Lab150 Lab138 Lab082 Lab067 Lab146 Lab050 Lab081 Lab079 Lab005 Lab021 Lab161 Lab179 Lab031 Lab054 Lab045 Lab030 Lab077 Lab110 Lab089 Lab177 Lab100 Lab046 Lab019 Lab087 Lab098 Lab117 Lab182 Lab178 Lab015 Lab162 Lab004 Lab013 Lab057 Lab145 Lab183 Lab080 Lab017 Lab011 Lab028 Lab032 Lab055 Lab068 Lab070 Lab029 Lab064 Lab096 Lab056 Lab073 Lab148 Lab001 Lab040 Lab095 Lab111 Lab175 Lab165 Lab158 Lab060 Lab043 Lab075 Lab106 Lab105 Lab173 Lab090 Lab159 Lab181 Lab139 Lab020 Lab039 Lab151 Lab147 Lab074 Lab042 Lab069 Lab010 Lab063 Lab115 Lab041 Lab091 Lab052 Lab172

EUPT-FV16 Preliminary Results 30th April 2014 PyridabenPyridaben

5,0 0,149 mg/kg 4,0 97,1 % Acceptable 2,2 % Questionable 3,0 0,7 % Unnacceptable

2,0

1,0

0,0

-1,0

-2,0

-3,0

-4,0 1 False negative

-5,0 Lab108 Lab027 Lab102 Lab174 Lab064 Lab081 Lab023 Lab062 Lab140 Lab077 Lab139 Lab172 Lab149 Lab143 Lab065 Lab123 Lab006 Lab078 Lab019 Lab136 Lab076 Lab007 Lab021 Lab066 Lab093 Lab101 Lab111 Lab128 Lab088 Lab051 Lab016 Lab046 Lab178 Lab165 Lab002 Lab033 Lab038 Lab106 Lab025 Lab085 Lab015 Lab045 Lab138 Lab091 Lab145 Lab167 Lab054 Lab121 Lab131 Lab146 Lab001 Lab009 Lab130 Lab147 Lab158 Lab164 Lab182 Lab050 Lab018 Lab073 Lab031 Lab169 Lab036 Lab042 Lab049 Lab096 Lab129 Lab029 Lab060 Lab072 Lab095 Lab012 Lab032 Lab059 Lab097 Lab013 Lab020 Lab090 Lab126 Lab008 Lab133 Lab017 Lab067 Lab079 Lab105 Lab151 Lab152 Lab057 Lab089 Lab137 Lab068 Lab010 Lab011 Lab053 Lab055 Lab058 Lab083 Lab112 Lab141 Lab153 Lab161 Lab180 Lab084 Lab104 Lab122 Lab056 Lab179 Lab075 Lab107 Lab163 Lab162 Lab119 Lab082 Lab086 Lab040 Lab044 Lab063 Lab087 Lab103 Lab116 Lab173 Lab110 Lab166 Lab069 Lab100 Lab030 Lab003 Lab177 Lab070 Lab061 Lab099 Lab115 Lab155 Lab047 Lab183 Lab109 Lab028 Lab171 Lab117 Lab118 Lab157 Lab014 Lab052 Lab080 Lab034 Lab160 Lab114 Lab159 Lab035 Lab041

EUPT-FV16 Preliminary Results 30th April 2014 Spinosad (sum of spinosynSpinosad A and spinosyn D, expr. as spinosad) (sum of spinosyn A and spinosyn D, expr. as spinosad) 5,0 0,098 mg/kg 4,0 86,2 % Acceptable 5,2 % Questionable 3,0 8,6 % Unnacceptable

2,0

1,0

0,0

-1,0

-2,0

-3,0

-4,0 1 False negative

-5,0 Lab179 Lab114 Lab134 Lab019 Lab002 Lab047 Lab137 Lab078 Lab095 Lab020 Lab155 Lab030 Lab077 Lab131 Lab010 Lab157 Lab174 Lab169 Lab149 Lab122 Lab165 Lab076 Lab100 Lab119 Lab104 Lab055 Lab058 Lab072 Lab112 Lab138 Lab166 Lab059 Lab061 Lab139 Lab099 Lab015 Lab027 Lab123 Lab130 Lab006 Lab021 Lab046 Lab062 Lab003 Lab110 Lab120 Lab028 Lab042 Lab066 Lab140 Lab167 Lab060 Lab073 Lab118 Lab162 Lab178 Lab107 Lab057 Lab183 Lab133 Lab182 Lab017 Lab025 Lab063 Lab103 Lab126 Lab081 Lab008 Lab029 Lab033 Lab044 Lab082 Lab117 Lab016 Lab031 Lab070 Lab075 Lab106 Lab159 Lab011 Lab053 Lab084 Lab101 Lab177 Lab001 Lab013 Lab090 Lab128 Lab067 Lab079 Lab121 Lab024 Lab034 Lab068 Lab111 Lab115 Lab172 Lab136 Lab056 Lab051 Lab007 Lab093 Lab151 Lab040 Lab096 Lab171 Lab089 Lab050 Lab160 Lab102 Lab054 Lab127 Lab097 Lab145 Lab146 Lab141 Lab173 Lab065 Lab049 Lab105 Lab083 Lab163 Lab012 Lab052 Lab041 Lab032 Lab164

EUPT-FV16 Preliminary Results 30th April 2014 TetraconazoleTetraconazole

5,0 0,105 mg/kg 4,0 95,0 % Acceptable 1,4 % Questionable 3,0 3,6 % Unnacceptable

2,0

1,0

0,0

-1,0

-2,0

-3,0

-4,0 1 False negative

-5,0 Lab035 Lab140 Lab177 Lab139 Lab108 Lab174 Lab146 Lab102 Lab040 Lab048 Lab066 Lab099 Lab179 Lab131 Lab025 Lab027 Lab077 Lab002 Lab018 Lab127 Lab006 Lab033 Lab076 Lab130 Lab009 Lab104 Lab150 Lab123 Lab169 Lab045 Lab073 Lab181 Lab084 Lab167 Lab151 Lab165 Lab078 Lab097 Lab149 Lab152 Lab178 Lab019 Lab136 Lab016 Lab030 Lab129 Lab133 Lab036 Lab070 Lab072 Lab021 Lab081 Lab137 Lab038 Lab041 Lab058 Lab062 Lab087 Lab101 Lab105 Lab111 Lab118 Lab161 Lab164 Lab120 Lab160 Lab003 Lab122 Lab001 Lab050 Lab056 Lab060 Lab138 Lab166 Lab057 Lab089 Lab128 Lab162 Lab054 Lab068 Lab020 Lab015 Lab017 Lab047 Lab031 Lab065 Lab008 Lab028 Lab063 Lab064 Lab069 Lab083 Lab090 Lab093 Lab103 Lab115 Lab145 Lab172 Lab014 Lab088 Lab126 Lab046 Lab061 Lab095 Lab119 Lab080 Lab085 Lab049 Lab051 Lab086 Lab096 Lab079 Lab121 Lab044 Lab034 Lab053 Lab059 Lab110 Lab112 Lab116 Lab125 Lab142 Lab173 Lab082 Lab075 Lab029 Lab159 Lab067 Lab182 Lab055 Lab107 Lab114 Lab052 Lab004 Lab007 Lab011 Lab091 Lab147 Lab155 Lab042 Lab013 Lab163 Lab153 Lab024 Lab012 Lab010 Lab171 Lab183 Lab032 Lab141 Lab100 Lab148 Lab157

EUPT-FV16 Preliminary Results 30th April 2014 Combined z-Scores

EUPT-FV16 Preliminary Results 30th April 2014 Average of Squared z-Scores

nn  Zi Zi AZ2 == i==1 n AZ2  2 Good 2 < AZ2  3 Satisfactory AZ2 > 3 Unsatisfactory

EUPT-FV16 Preliminary Results 30th April 2014 2 NRLs OfLs AZ Representation EU/EFTA Laboratories 92 % Good 5 % Satisfactory 3 % Unsatisfactory

Category A: 59,2 % of the EU/EFTA Laboratories EUPT-FV15: 54% (100 Laboratories out of 169)

EUPT-FV15: 92 % Good 7 % Satisfactory 1 % Unsatisfactory

EUPT-FV16 Preliminary Results 30th April 2014 False Positives

5 different laboratories from EU/EFTA countries reported 5 pesticides as false positives

EUPT-FV16 Preliminary Results 30th April 2014 False Positives

Laboratory Concentration Determination RL MRRL Code Pesticide (mg/kg) Technique (mg/Kg) (mg/Kg)

Lab059 Fenpropathrin 0,980 LC-MS/MS (ESI+) 0.01 0,01

Lab160 Folpet 0,240 GC-MS/MS (EI) 0.02 0.01

Mepanipyrim (only parent Lab172 0,019 LC-MS/MS (ESI+) 0.01 0.01 compound)

Lab024 Metalaxyl and metalaxyl-M 0,010 LC-MS/MS (ESI+) 0.01 0.01

Lab003 Tefluthrin 0,012 GC-ECD 0.01 0.01

EUPT-FV16 Preliminary Results 30th April 2014 False Positives

GC-ECD or GC-MS/MS LC-MS/MS

Folpet Fenpropathrin Tefluthrin Mepanipyrim Metalaxyl and metalaxyl-M

EUPT-FV16 Preliminary Results 30th April 2014 EUPT-FV16 Preliminary Results

30th April 2014