0000033
EMB Sample No. C1688 dO Page of u •01 0523 I TASK VOA/WATERI Analysis Date 2-9-87
Accuracy By: Matrix Spike DI Spike EPA QC SURROGATE RESPONSES Surrogate Solution No. Compounds in Solution \ Recovery PC Limits Bromochloromethane 91 70 - 130 l-bromo-2-chloroethane 98 70 - 130 Toluene, d6 95 70 - 130 1,4-dichlorobutane 98 70 - 130 1,9-decadiene 107 70 - 130
SAMPLE RESULTS
Method Result Replicate Precision Accuracy Blank (ug/1) (ua/1) (% RSD) (% R) ud/1 Acetone <50 <50 Acrolein <20 <20 Acrylonitrile <20 <20 Benzene <2 <2 Bromoforra <2 <2 Bromodichloromethane <2 <2 Bromomethane <2 <2 Carbon Bisulfide <100 <100 Carbon Tetrachloride <2 95 <2 Chlorobenzene <2 <2 Chlorodibromomethane <2 <2 Chloroethane <2 <2 2-Chloroethylvinylether <2 <2 Chloroform <2 120 <2 Chloromethane <2 <2 1,2-Dichlorobenzene <2 <2 1,3-Dichlorobenzene <2 91 <2 1,4-Dichlorobenzene <2 <2 Dichlorodifluoromethane <2 <2 1,1-Dichloroethane (2 <2 1r 2-Dichloroethane <2 <2 1r1-Dichloroethene <2 <2 t-1,2-Dichloroethene <2 <2 1,2-Dichloropropane <2 <2 c-1,2-Dichloropropene <2 <2 t-1,2-Dichloropropene <2 <2
EPA Region 5 Records Ctr,
248173 EMB Sample No. C1688 Page of 01 0524 Continuation of TASK VOA/ WATER
Method Result Replicate Precision Accuracy Blank Parameter (ua/1) (ua/1) (% RSD) (* R) ucr/1 Ethylbenzene <2 <2 Fluorotrichloromethane <2 <2 2-Hexanone Methylene Chloride <2 <2 Methyl Ethyl Ketone <10 Methyl Isobutyl Ketone Paraldehyde <20 <20 Styrene <2 <2 1,1,2,2-Tetrachloroethane <2 <2 Tetrachloroethylene <2 <2 Toluene <2 <2 1,1,1-Trichloroethane <2 <2 1,1,2-Trichloroethane <2 <2 Trichloroethylene <2 82 <2 Vinyl Acetate Vinyl Chloride <2 <2 m-Xylene <2 <2 o-Xylene <2 <2 p-Xylene <2 <2 EMB Sample No. C1689 Page .2 of •01 0525
I TASK VOA/HATER! Analysis Date 2-9-87 Accuracy By: Matrix Spike DI Spike EPA QC
SURROGATE RESPONSES Surrogate Solution No. Compounds in Solution \ Recovery PC Limits . Bromochloromethane 86 70 - 130 . l-bromo-2-chloroethane 94 70 - 130 . Toluene, d6 93 70 - 130 . 1,4-dichlorobutane 95 70 - 130 . 1,9-decadiene 104 70 - 130
SAMPLE RESULTS Method Result Replicate Precision Accuracy Blank . Parameter (uq/1) (\ RSD) (% R) ug/l Acetone <50 <50 Acrolein <20 <20 Acrylonitrile <20 <20 Benzene <2 <2 Bromoform <2 <2 Bromodichloromethane <2 <2 Bromomethane <2 <2 Carbon Bisulfide <100 <100 Carbon Tetrachloride <2 95 <2 Chlorobenzene <2 <2 Chlorodibromomethane <2 <2 Chloroethane <2 <2 2-Chloroethylvinylether <2 <2 Chloroform <2 120 <2 Chloromethane <2 <2 1,2-Dichlorobenzene <2 <2 1,3-Dichlorobenzene <2 91 <2 1,4-Dichlorobenzene <2 <2 Dichlorodifluoromethane <2 <2 1,1-Dichloroethane <2 <2 1,2-Dichloroethane <2 <2 1,1-Dichloroethene <2 <2 t-l,2-Dichloroethene <2 <2 1,2-Dichloropropane <2 <2 c-lr2-Dichloropropene <2 <2 t-l,2-Dichloropropene <2 <2 EMB Sample No. C1669 Page . 3 of Dl 0526 Continuation of TASK VOA/WATER
Method Result Replicate Precision Accuracy Blank Parameter (u
SAMPLE RESULTS Method Result Replicate Precision Accuracy Blank Parameter (ua/1) (utr/1) (% R5D) (% R) uq/1 Acetone <50 <50 Acrolein <20 <20 Acrylonitrile <20 <20 Benzene <2 <2 Bromoform <2 <2 Bromodichloromethane <2 <2 Bromomethane <2 <2 Carbon Disulfide <100 <100 Carbon Tetrachloride <2 95 <2 Chlorobenzene <2 <2 Chlorodibromomethane <2 <2 Chloroethane <2 <2 2-Chloroethylvinylether <2 <2 Chloroform <2 120 <2 Chloromethane <2 <2 1,2-Dichlorobenzene <2 <2 1,3~Dichlorobenzene <2 91 <2 1,4-Dichlorobenzene <2 <2 Dichlorodifluoromethane <2 . <2 1,1-Dichloroethane <2 <2 1,2-Dichloroethane . <2 <2 1,1-Dichloroethene <2 <2 t-l,2-Dichloroethene <2 <2 1,2-Dichloropropane <2 <2 c-l,2-Dichloropropene <2 . ' '- <2 t-l,2-Dichloropropene <2 <2 * Present at 1.2 ug/1 EMB Sample No. C1690 Page of 01 0528 Continuation of TASK VGA/WATER
Method Result Replicate Precision Accuracy Blank Parameter (ug/1) (ug/1) (\ RSD) (* R) ug/1 Ethylbenzene <2 <2 Fluorotrichloromethane <2 <2 2-Hexanone <10 Methylene Chloride <2 <2 Methyl Ethyl Ketone <10 Methyl Isobutyl Ketone <10 Paraldehyde <20 <20 Styrene <2 <2 1,1,2,2-Tetrachloroethane <2 <2 Tetrachloroethylene <2 <2 Toluene <2 <2 1,1,1-Trichloroethane 4.5 <2 1,1,2-Trichloroethane <2 <2 Trichloroethylene 21. 82 <2 Vinyl Acetate <10 Vinyl Chloride <2 <2 m-Xylene <2 <2 o-Xylene <2 <2 p-Xylene <2 <2 EMB Sample No. C1691 Page .2 of 01 0529 I TASK VOA/HATERI Analysis Date 2-9-87
Accuracy By: Matrix Spike DI Spike EPA QC SURROGATE RESPONSES Surrogate Solution No. Compounds in Solution * Recovery QC Limits Bromochloronethane 91 70 - 130 l-bromo-2-chloroethane 98 70 - 130 Toluene, d6 96 70 - 130 1,4-dichlorobutane 95 70 - 130 1,9-decadiene 106 70 - 130
SAMPLE RESULTS Method Result Replicate Precision Accuracy Blank Parameter (U SURROGATE RESPONSES Surrogate Solution No. Compounds in Solution Recovery QC Limits Bromochloromethane 90 / 92 70 - 130 l-bromo-2-chloroethane 95 / 95 70 - 130 Toluene, d6 90 / 93 70 - 130 1,4-dichlorobutane 96 / 97 70 - 130 1,9-decadiene 96 / 111 70 - 130 SAMPLE RESULTS Method Result Replicate Precision Accuracy Blank Parameter (ug/1) (ucr/1) (% RSD) <% R> UQ/1 Acetone <50 <50 0.0 <50 Acrolein <20 <20 0.0 <20 Acrylonitrile <20 <20 0.0 <20 Benzene <2 <2 0.0 <2 Bromoform <2 <2 0.0 <2 Bromodichloromethane <2 <2 0.0 <2 Bromomethane <2 <2 0.0 <2 Carbon Disulfide <100 <100 0.0 <100 Carbon Tetrachloride <2 <2 0.0 95 <2 Chlorobenzene <2 <2 0.0 <2 Chlorodibromomethane <2 <2 0.0 <2 Chloroethane <2 <2 0.0 <2 2-Chloroethylvlnylether <2 <2 0.0 <2 Chloroform <2 <2 0.0 120 <2 Chloromethane <2 <2 0.0 <2 1,2-Dichlorobenzene <2 <2 0.0 <2 .. , 1,3-Dichlorobenzene <2 <2 0.0 91 <2 1,4-Dichlorobenzene <2 <2 0.0 <2 Dichlorodifluoromethane <2 <2 0.0 <2 1,1-Dichloroethane <2 <2 0.0 <2 1,2-Dichloroethane - <2 <2 0.0 <2 1,1-Dichloroethene <2 <2 0.0 <2 t-1,2-Dichloroethene <2 <2 0.0 <2 1,2-Dichloropropane <2 <2 o.o - . •/•-:••.-;/•:;; <2 c-1,2-Dichloropropene <2 <2 0.0S •'" <2 t-1,2-Dichloropropene <2 <2 0.0 <2 f EMB Sample No. C1692 Page .3 of 01 0532 Continuation of TASK VOA/WATER J Method Result Replicate Precision Accuracy Blank Parameter (ua/1) (ug/1) (* R5D) (% R) uq/1 Ethylbenzene <2 <2 0.0 <2 Fluor otrichlorome thane <2 <2 0.0 <2 2-Hexanone <10 <10 0.0 <10 Methylene Chloride <2 <2 0.0 <2 Methyl Ethyl Ketone <10 <10 0.0 <10 Methyl Isobutyl Ketone <10 <10 0.0 <10 Paraldehyde <20 <20 0.0 <20 Styrene <2 <2 0.0 <2 1,1,2, 2-Tet rachloroethane <2 <2 0.0 <2 Tetrachloroethylene <2 <2 0.0 <2 Toluene <2 <2 0.0 <2 1 , 1 , 1-Trichloroethane <2 <2 0.0 <2 1,1 , 2-Tr ichloroethane <2 <2 0.0 <2 Trichloroethylene <2 <2 0.0 82 <2 Vinyl Acetate <10 <10 0.0 <10 Vinyl Chloride <2 <2 0.0 <2 a-Xylene <2 <2 0.0 <2 o-Xylene <2 <2 0.0 <2 p-Xylene <2 <2 0.0 <2 EMB Sample No. C1693 Page of 01 0533 » TASK VOA/HATERI Analysis Date 2-9-87 Accuracy By: Matrix Spike DI Spike EPA QC SURROGATE RESPONSES Surrogate Solution No. Compounds in Solution % Recovery PC Limits Broraochloromethane 87 70 - 130 l-bromo-2-chloroethane 92 70 - 130 Toluene, d6 97 70 - 130 1,4-dichlorobutane 92 70 - 130 1,9-decadiene 113 70 - 130 SAMPLE RESULTS Method Result Replicate Precision Accuracy Blank Parameter (u Acetone <50 <50 Acrolein <20 <20 Acrylonitrile <20 <20 Benzene <2 <2 Bromoform <2 <2 Bromodichloromethane <2 <2 Bromomethane <2 <2 Carbon Bisulfide <100 <100 Carbon Tetrachloride <2 95 <2 Chlorobenzene <2 <2 Chlorodibromomethane <2 <2 Chloroethane <2 <2 2-Chloroethylvinylether <2 <2 Chloroform <2 120 <2 Chloromethane <2 <2 Ir2-Dichlorobenzene <2 <2 1,3-Dichlorobenzene <2 91 <2 1,4-Dichlorobenzene <2 <2 Dichlorodifluoromethane <2 <2 1,1-Dichloroethane <2 <2 1,2-Dichloroethane <2 <2 1,1-Dichloroethene <2 <2 t-l,2-Dichloroethene <2 <2 1,2-Dichloropropane <2 <2 c-l,2-Dichloropropene <2 <2 t-l,2-Dichloropropene <2 <2 EMB Sample No. C1693 Page of Continuation of TASK VOA/WATER 01 0534 Method Result Replicate Precision Accuracy Blank Parameter (ua/1) (ua/1) (% RSD) (\ R) ua/1 Ethylbenzene <2 <2 Fluorotrichlorome thane <2 <2 2-Hexanone <1( Methylene Chloride <2 <2 Methyl Ethyl Ketone Methyl Isobutyl Ketone Paraldehyde <20 <20 Styrene <2 <2 1,1,2,2-Tetrachloroethane <2 <2 Tetrachloroethylene <2 <2 Toluene <2 <2 1,1,1-Trichloroethane <2 <2 1,1,2-Trichloroethane <2 <2 Trichloroethylene <2 82 <2 Vinyl Acetate <10 Vinyl Chloride <2 <2 ra-Xylene <2 <2 o-Xylene <2 <2 p-Xylene <2 <2 EMB Sample No. C1694 Page of 01 0535 I TASK VOA/KATERI Analysis Date 2-9-87 Accuracy By: Matrix Spike DI Spike EPA QC SURROGATE RESPONSES Surrogate Solution No. Compounds In Solution % Recovery PC Limits Bromochloromethane 91 70 - 130 1-bromo-2-chloroethane 94 70 - 130 Toluene, d6 91 70 - 130 1,4-dichlorobutane 95 70 - 130 1,9-decadiene 105 70 - 130 SAMPLE RESULTS Method Result Replicate Precision Accuracy Blank Parameter (uq/1) (ug/l) (% RSD) (» R) utr/1 Acetone <50 <50 Acrolein <20 <20 Acrylonitrile <20 <20 Benzene <2 <2 Bromoform <2 <2 Bromodichloromethane <2 <2 Bromomethane <2 <2 Carbon Bisulfide <100 <100 Carbon Tetrachloride <2 95 <2 Chlorobenzene <2 <2 Chlorodibromomethane <2 <2 Chloroethane <2 <2 2-Chloroethylvinylether <2 <2 Chloroform <2 120 <2 Chloromethane <2 <2 1,2-Dichlorobenzene <2 <2 1,3-Dichlorobenzene <2 91 <2 1,4-Dichlorobenzene <2 <2 Dichlorodifluoromethane <2 <2 lf1-Dichloroethane <2 <2 1,2-Dichloroethane <2 <2 1,1-Dichloroethene <2 <2 t-l,2-Dichloroethene <2 <2 1,2-Dichloropropane <2 <2 c-l,2-Dichloropropene <2 <2 t-lr2-Dichloropropene C2 <2 EMB Sample No. C1694 Page of Continuation of TASK VOA/WATER 01 0536 Method Result Replicate Precision Accuracy Blank Parameter (ua/1) (ug/1) (% RSD) (* R) ug/1 Ethylbenzene <2 <2 Fluorotrichloromethane <2 <2 2-Hexanone <10 <10 Methylene Chloride <2 <2 Methyl Ethyl Ketone Methyl Isobutyl Ketone Paraldehyde <20 <20 Styrene <2 <2 1,1,2,2-Tetrachloroethane <2 <2 Tetrachloroethylene <2 <2 Toluene <2 <2 1,1,1-Trichloroethane <2 <2 1,1,2-Trichloroethane <2 <2 Trichloroethylene <2 82 <2 Vinyl Acetate <10 <10 Vinyl Chloride <2 <2 tn-Xylene <2 <2 o-Xylene <2 <2 p-Xylene <2 <2 <^}L EMB Sample No. C1695 Page .2 of 01 053? I TASK VOA/KATERI Analysis Date 2-9-87 Accuracy By: Matrix Spike DI Spike EPA QC SURROGATE RESPONSES Surrogate Solution No. Compounds in Solution * Recovery PC Limits Bromochloromethane 91 70 - 130 l-bromo-2-chloroethane 94 70 - 130 Toluene, d6 91 70 - 130 1,4-dichlorobutane 94 70 - 130 1,9-decadiene 98 70 - 130 SAMPLE RESULTS Method Result Replicate Precision Accuracy Blank Parameter (u