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Smithsonian Miscellaneous Collections SMITHSONIAN MISCELLANEOUS COLLECTIONS. 288 THE CONSTANTS OF NATURE. SPECIFIC GRAVITIES, BOILING POINTS, AND MELTING POINTS. FIEST SUPPLEMENT TO PART I. COMPILED BY FRANK WIGGLESWORTH CLARKE, S. B. PROFESSOR OF CHEMISTRY AND PHYSICS IN THE UNIVERSITY OF CINCINNATI. WASHINGTON, D. C: PUBLISHED BY THE SMITHSONIAN INSTITUTION. APRIL: 1S7 6. ADVERTISEMENT. The following is a first supplement to Part I. of a general work on the "Constants of Nature," gratuitously prepared for the Smithsonian Institu- tion by Professor F. W. Clarke, and published at the expense of its fund. Part I., on Specific Gravities, Boiling Points and Melting Points, was published in 1873, since which time the new determinations have been made and collected which form this supplement. JOSEPH HENRY, Secrt tary Smithsonian Institution. Washington, April, 1S76. ——————————— CONTENTS. PAGE. 1.—Preface 4 2.—Tables of Specific Gravity, Boiling Point and Melting Point. 5 I.—Elementary Substances 5 II. Fluorides, Chlorides, Bromides, and Iodides 9 III. Oxides' and Sulphides 13 IV. Hydrates 14 V.—Chlorates and Bromates 15 VI.—DlTHIONATES AND SULPHATES 16 VII. Selenates and Chromates IS VIII. Nitrates, Vanadates, Arsenates, and Phosphates 19 IX. Carbonates 20 X.—SlLICOFLUORIDES 21 XL Miscellaneous Inorganic Compounds 21 XII. Metallic Alloys 22 XIII. Hydrocarbons 23 XIV. Compounds containing C, H, and 28 XV. Compounds containing C, H, and N. : . 37 XVI. Compounds containing C, H, N, and 37 XVII. Metallic Salts of Organic Acids 39 XVIII. Compounds containing C, H, and CI -11 XIX. Compounds containing C, H, O, and CI 43 '- 45 XX.—Compounds containing C, H, CI, N, or C, H, CI, N. 0. XXI. Organic Compounds containing Bromine 46 XXII. Organic Compounds containing Iodine 49 XXIII. Organic Compounds containing Sulphur 50 XXIV. Miscellaneous Organic Compounds 53 3 — PREFACE. The following supplement to Part I of the Constants of Nature, eon- tains, in addition to determinations published during the past two years, some materials which were overlooked in compiling the original work. In it data are given for nearly seven hundred substances, of which at least four hundred are new since the publication of Part I. Of course the compiler is anxious that his work should be as thorough as possible, and hence he will be greatly obliged to any person calling his attention to errors or omissions. He would also request investigators having unpublished determinations on hand to favor him with copies of them for use in subsequent supplements or editions. Such material is always wortti saving, even when it is not of sufficient value to warrant publishing lnT itself. Few explanations are needed in this supplement. The arrangement and abbreviations are the same which were originally used, with the excep- tion of a very few new titles for periodicals. These are abbreviated as follows : B. D. C. G. "Berichte der Deutschen Chemischen Gesellschaft." B. II. A. S. F. "Bulletin Hebdomadaire de l'Association Scientillque de France." C. C. or C. Cent. "Chemisches Centralblatt." All references to this periodical apply only to the third or current series. Fortsch. d. Phys. " Fortschritte der Physik." F. W. C. Cincinnati, March 9, 1876. SUPPLEMENT TO TABLES OF SPECIFIC GRAVITY, BOILING POINT AND MELTING POINT. I. Elementary Substances. Name. - " : : "_ : : - - :- - - j 3. : : :zi~ :._-_ - " - - • - ~ - " " mefefoer- 7 *a 7 a eba P- -- n»fMw<r 7 - _ a Wilson. 3 : i - "Sagrs Kan. C.3T. 3L I ATTTT TAB, RITEES i& B. - ' - " R. 78. Pis - p. c. g. ; I s Dev M. - B. 7-482 - - ; _ P. c . I " :ihold. P. A ' - B. F P 7 275 p. c. - ; - B. P 7. 482 p. c. g. - ; SPECIFIC GRA YITY TABLES. Name. SPECIFIC GRAVITY TABLES. II. Fluorides, Chlorides, Bromides, and Iodides. Name. 10 SPECIFIC GRAVITY TABLES. Name. SPECIFIC GRAVITY TABLES. 11 Name. 12 SPECIFIC GRAVITY TABLES. SPECIFIC OKA YITY TABLES. 13 Boiling Melting Name. Formula. Specific Gravity. Point. Point. 1 I Ammonium platiniodide A"m 2 Pt 6 4.610. 2 « Manganese MnPtI6.9H20. 3.604. 3 « Iron FePtI6.9H2 0. 3-455- 4 « 3-6i8. Cobalt CoPtI 6 .9H 2 0. 5 « « CoPtI6.12H20. 3.048. 6 « Nickel NiPtI 6 .6H 2 0. 3-976. 7 <c « NiPtI6.9H 2 0. 3-549- 8 « Zinc ZnPtI 6 .9H,0. 3.689, 9 « Magnesium MgPtI6 .9H 2 0. 3-458- 10 Nickel ammonioiodide m I,. 6 n h" . 2.101. III. Oxides and Sulphides. Name. 14 SPECIFIC GRA VITY TABLES. Name. SPECIFIC GBA VITY TABLES. 15 Name. 16 SPECIFIC GRA VITY TABLES. VI. DlTHIONATES AND SULPHATES. Name. SPECIFIC GRAVITY TABLES. 17 Name. 18 SPECIFIC GRAVITY TABLES. VII. Selenates and Cheomates. Name. SPECIFIC GRA VITY TABLES. 19 Name. 20 SPECIFIC GRA VITY TABLES. Name. SPECIFIC GRAVITY TABLES. 21 X. SlLICOFLUORIDES. Name. 22 SPECIFIC GRAVITY TABLES. Name. SPECIFIC GRAVITY TABLES. 23 XIII. Hydrocarbons. Name. 24 SPECIFIC GRAVITY TABLES. Name. SPECIFIC GRA VITY TABLES. Name. 2G SPECIFIC GRAVITY TABLES. Name. « SPECIFIC GRAVITY TABLES. 27 Boiling Formula. Specific Gravity Name. Point. J Terebenthene. '•-''in -tlifi- 8767. o . 8601. 20°. 40°. .8436. 6°- i 5 S . .8270. 60°. .8105. 8o°. •7939- IOO°. 7 Isoterebenthene. .8586. o°. .8427. 20°.28. .8273. 4o°.i 9 . .8131. 58°-32. .7964. •7793- 13 From cubeb oil. C15 H 21 . .9289. 14 « clove. « .905. 15 « calamus •942. 16 Oil of cedar. .9231. 17 « santal wood. .9190. 18 « vitivert. .9332. 19 Petrolene. S953- .8921. 22 Poplar oil. C H .9002. 20 3 23 Tetraterebenthene. C, n PL 977- 24 Isopropyl acetylene. C5 H g . .652. n°. 25 1 8°. Dipropargyl. C6 H 6 . .81. 26 . o°. Hexhydroisoxylol. C8 H 16 Ill- 9°- "Tetramethyl allene. C H . •95*3- 7 12 28 Tolyl phenyl. 1 .01 5. 27 . 29 . l8°.9. Benzyl ethyl benzol. C 15 H 1B .985. 30 Phenanthrene tetrahy- dride. 1.067. IO°.2. C 14 Hu 28 SPECIFIC GRAVITY TABLES. B ° ilin Melting Name. Formula. Specific Gravity g J Point. Point. 1 . 283°-286°. Phenyl xylene. CX4 Hu 2 1 From benzyl toluol. C21 H 20 . .049. 392°-396°. 3 « . phenylbromethyl. C15 H 16 .98. 278°-28o°. 4 « calamus oil. .8793. o° i58°-i59°- 5 n-1« -M-ia. 1. 08-1. Eetene. 1 3. 98^.5. XIV. Compounds Containing C, H, and O. Name. SPECIFIC GRA VITY TABLES. 29 Name. 30 SPECIFIC GnA YITY TABLES. Name. SPECIFIC GRAVITY TABLES. 31 Name. 32 SPECIFIC GRAVITY TABIES. Name. SPECIFIC GRAVITY TABLES. 33 Name. 34 SPECIFIC GRAVITY TABIES SPECIFIC GRA VITY TABLES. 35 AUTHORITIES. 1 36 SPECIFIC GRAVITY TABLES. Name. SPECIFIC GRA VITY TABLES. XV. Compounds Containing C. H. and N. Name. 38 SPECIFIC GRAVITY TABLES. Name. SPECIFIC GllA YITY TABLES. 39 XVII. Metallic Salts of Organic Acids. Name. 40 SPECIFIC GRAVITY TABLES. Name. SPECIFIC GRAVITY TABLES. 41 XVIII. Compounds Containing C. H. and Cl. Name. 42 SPECIFIC GEA VITY TABLES. Name. SPECIFIC GEA VITY TABLES. 43 XIX. Compounds Containing C. H. O. and Cl. Name. 44 SPECIFIC GRAVITY TABLES. Name. SPECIFIC GRAVITY TABLES. 43 XX. Compounds Containing C. H. CI. K; or C. H. CI. N. O. Name. J 46 SPECIFIC GRAVITY TABLES. XXI. Organic Compounds Containing Bromine. _. ... _, . Melt. Name. Formula. Specific Gravity. Boiling Point. poim> Ethyl bromide. C, Hs Br. 1.4775. 5-io- I 14679- io°-i5°. 1.4582. I5°-20°. j I.385. I5°.l Two 33°-39°- J -" J }• different 1.47- 15°- J samples. 33 .5-39°-5- 6 Butyl ene « C H Br . 1.8503. O . 4 8 2 i64°-i65°. « I.8204. 2 ° C . o°. i7o°-i75°. Amylene « C5 H 10 Br2 1.3443. 1.7087. 178 . « 1.6868. I4°- 11 . o°. Hexylene « C6 H 12 Br2 1.6058. i 9 5°-i97 . « 1.5809. 19 « 1.6497. 0°. i8o°-i90°. 14 Dibromome- thane. C H Br . 2.0844. n°-5. 8o°-82°. 2 2 15 Bromo-cthylene 6°. bromide. C 2 H 3 Br3 . 2.624. 1 191 . 16 « « « 2.65. o°. i84°-i85°. 17 Bromo-propy- a. Br. i °.5. lene, C3 H 5 1.364. 9 48 18 « « /?. (i 1.428. I9°.5. |59°-5-6o. 19 Bromo-/? propy- 8°. 1 lene bromide. C3 H5 Br3 2.356. AUTHORITIES. 1 SPECIFIC GRA VITY TABLES. 47 Name. 48 SPECIFIC GRAVITY TABLES. Name. SPECIFIC GRAVITY TABLES. 49 Melt. Formula. Specific Gravity. Boiling Point. Name. Point. 1 Carbon chloro- bromide. C Cl„ Br. .058. o°. 1 IO4 . 2 « « « .842. IOO°.J 3 « 8°. c Propylene C3 H 6 CI Br. 1.63. I I40°-I4i 21°. 93°-95°. 1.474. 1[ Four 9 I.60. 20 . no . r 120°. XXII. Organic Compounds Containing Iodine. Name. 50 SPECIFIC GRA YITY TABLES. Name. SPECIFIC GRAVITY TABLES. 51 Name. J SPECIFIC GRA VITY TABLES. Boiling Melting Name. Formula. Specific Gravity. Point. Point. 1 Ethyl isosulpho cyanide. C,H,NS I.OI913. I 1.019375. .997525. 2I°4. 133-2. .997235. 22°. .87909. \ I33-2- •3735J3- 'Isopropyl sulpho- i 2 -i53°. cyanide. C H N S. .989. O . 5 4 7 8 5°. « « « •974- 1 9 I97°-I98°. Hexyl « C H N S. -9 2 53- 7 13 10 Amyl isosulpho- 0°. cyanide. C6 Hn N S. .957538- 1S2 . (i .94189. 17 . <( .78749. 1 82 . 13 Allyl sulphocy- 1 .07 1. o°. I48°-I49°. anide. C4 H 3 N S. " « « « 1.056. 15°. 15 Phenyl « S. 1. I7°.5. C7 H 5 N 155. 231 16 « 1. I3i°-i32°. Acetyl C3 H 3 N S. 151. 16 17 Benzoyl « S. 1. 16°. 200r205'invacuo C8 H 5 O N 197. 18 Monochlorallyl 12°. sulphocyanide. C H CI N S. 1.27. 185 . 4 4 ,9 Perchloromethyl . I.712. mercaptan. C S Cl 4 I2°.8. I46.5-I4S 20 Carlionyl sulphe- 6°. 36°- thvl chloride. C, H, CI S 0. 1.
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