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Chemexplained.Com Master Lab Equipment and Supplies List (Through Lab #18)

Chemexplained.Com Master Lab Equipment and Supplies List (Through Lab #18)

ChemExplained.com Master Lab Equipment and Supplies List (Through Lab #18)

Science Supply Companies RECOMMENDED Flinn Scientific Carolina Biological Supply Co. Home Science Tools P.O. Box 219 2700 York Rd 665 Carbon St. Batavia, IL 60510 Burlington, NC 27215-3398 Billings, MT 59102 Ph: 800-452-1261 Ph: 800-334-5551 Ph: 800-860-6272 Website: flinnsci.com carolina.com/chemistry/10148.ct www.homesciencetools.com ——————————————————————————————————————————— ChemExplained.com is working with Home Science Tools (HST) in Billings, Montana to make ordering lab supplies for our experiments quicker and easier for parents. HST has provided two lists, one for ordering the chemicals needed for our experiments and another list for ordering ​ ​ equipment and supplies. (Either click the URL or copy/paste it into your browser). ​ ChemExplained.com Chemical List: ​ ​ https://www.homesciencetools.com/wishlist.php?publicwishlist=bbdd79a3ffdb49bea2f6190f1ed516ca

ChemExplained.com Equipment and Supplies List: ​ ​ https://www.homesciencetools.com/wishlist.php?publicwishlist=58f7c118d539e795af6cac108ed80fca

From the HST staff: “Please note that adding all items in a wish list at once will only add 1 item, please advise parents/students to adjust quantities on the items accordingly.” ——————————————————————————————————————————— Please READ THIS before ordering. A number of ChemExplained.com experiments require heat. ​ The heat source listed below in our Equipment list is a propane or butane torch kit. These may be ​ ​ purchased at Home Depot, Ace Hardware or Mills Fleet Farm stores for ~ $25. The replacement butane or propane gas refill containers for these torches cost ~ $4. When these torches are used ​ in an experiment, they must be “hand-held,” because if they are left upright while lit, they can tip over and cause a fire hazard. Home Science Tools (HST) sells a Portable Micro Lab Burner ​ for ~ $52. Butane fuel refill cartridges cost ~ $6. This burner is “tip-resistant” and provides safe, stable operation during an experiment and is recommended, but it cannot be used for Lab #6. In ​ ​ ​ ​ ​ all of our experiments, no burner of any kind may be used without adult supervision.

Laboratory balances are also required in a number of experiments. Balances accurate to 0.01 g ​ (1/100th of a gram) provide the best results. However, lab balances accurate to 0.1 g (1/10th of a ​ gram) can also be used. Amazon.com sells an AMIR Digital Kitchen Scale for ~ $12 (accurate to 0.01 g). Recommended! HST sells an Economy Pocket Scale for ~ $15 (accurate to 0.1 g) ​ ​

In Lab #9, a Molecular Model kit from HST costs ~$22. A bag of colored marshmallows plus toothpicks can also be used for ~ $4.

Amazon.com (Industrial & Scientific area) has many of our items listed at discount prices. ———————————————————————————————————————————

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The numbers following the items below are the Lab experiments that item is used in. ​ ​ Equipment Supplies 1 - 100 mL - 3, 5, 17, 18 Dawn soap - 3, 4, 5, 12, 13, 14-15, 18 1 - 50 mL graduated cylinder - 3, 10 Food coloring (red, blue and yellow) - 1 1 - 25 mL graduated cylinder - 13, 14-15, 18 Garbage (trash) bag - 18 1 - 10 mL graduated cylinder - 1, 3, 4, 18 Pliers or wire cutter - 3, 5, 14-15 3 - 50 mL beaker - 1, 4 wire or cylinder - 3, 5 2 - 250 mL beaker - 3, 7, 10, 13, 14-15, 17, 18 Aluminum wire or cylinder - 3, 14-15 1 - 800 mL (or 1000 mL) beaker - 12, 16 Toothpicks - 5 ​ ​ 10 - Test tubes (16 x 150 mm, large) - 1, 5, 10, 16 Black marker (Vis-A-Vis) - 1, 7, 13 ​ ​ 1 - (100 mm diameter) - 1, 13, 14-15, 17, 18 Karo syrup - 3 ​ ​ 1 - rack (6 holes) - 1, 5, 10 Sandwich bags (sealable) - 4, 18 ​ ​ 1 - (large) - 3, 4, 5, 13, 14-15, 18 Vinegar - 4, 18 ​ ​ 1 - (or clamp) - 5, 16 Table salt (sodium chloride) - 5, 7, 10, 14-15 ​ ​ ​ ​ 1 - Lab balance - 3, 4, 5, 11, 12, 13, 14-15, 16, 17, 18 Baking soda - 4 10 - Dropper pipet (1 mL) - 1, 3, 4, 5, 10, 12, 18 Wood splints (or toothpicks) - 5 ​ ​ 1 - /Spatula (20 cm) - 4, 5, 7, 11, 12, 13, 14-15, 17, 18 Scissors - 10, 14-15 ​ ​ ​ 1 - Forceps (stainless steel) - 5, 10, 11, 12, 13, 14-15 glass slide - 5, 14-15 ​ ​ 1 - Ring stand/support (4” x 6” base) - 5, 11, 12, 13, 14-15, 16 Pencil (#2) - 8, 10, 13. Ink pen - 6, 18 ​ ​ ​ ​ ​ 1 - Ring clamp (or support) - 5, 11, 12, 13, 14-15, 16 Meter stick (or ruler) - 6, 10, 14-15 ​ ​ 1 - (50 mL, low form) - 5, 11, 12 Labels (any size, we can cut to fit) - 6, 7, 18 ​ ​ 1 - Crucible cover (or lid) - 11 Coffee filters - 10, 13, 14-15 ​ ​ 1 - Clay triangle (2.5” pipe-stems) - 5, 11, 13 Q-tips - 7 ​ ​

1 - “Pocket” microscope (or microviewer) - 5, 14-15 Bottled H2O (or distilled) ​- 7, 10, 13, 14-15, 16, 17, 18 ​ ​ ​ ​ ​ ​ ​ 1 - Propane/butane torch - 6 (Can be used in all micro burner labs) Molecular model kit (or marshmallows) - 9 ​ ​ ​ 6 - Watch glasses (100 mm) - 7 Hot pad holder or gloves - 12, 13, 17 ​ ​ 6 - Glass tubing 6 mm, 24” lengths. (or 5 mm, 12” lengths) - 6 Felt-tipped markers (not permanent) - 10 ​ ​ ​ ​ 1 - (ceramic center) - 12, 13, 14-15, 16 Chromatography paper strips - 10 ​ ​ 1 - (80 mL) - 12, 14-15 Paper towels - 10, 14-15, 18 ​ ​ 1 - Triangular file - 6, 17 Metal cookie sheet, cake pan - 13, 14-15, 17 1 - Wash (squirt bottle) (500 mL) - 13, 14-15 Plastic wrap (or corks) - 10 ​ ​ ​ ​ 1 - 12” (non-mercury) - 16 Saucepan - 16 ​ ​ 1 - Stirring rod (10”) - 17, 18 Copper coated steel BBs - 16 ​ ​ 1 - 250 mL - 18 Styrofoam cup (12 oz.) - 16 1 - Portable micro lab burner - 5, 7, 11, 12, 13, 14-15, 16 Empty soda pop can - 17 ​ (Can be used for all labs that need heat except Lab #6) Long nail (6” - 8”) - 17 ​ ​ 4 - Butane fuel refill containers (for micro lab burner) Scotch tape - 6 ​

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ATTENTION! Before purchasing and using any chemicals, please review recent Safety Data ​ ​ ​ ​ Sheets (SDS) at https://chemical safety.com/sds-search/ for additional safety, handling, and ​ ​ disposal information. The number following the chemical name below, e.g. (5 g or 20 mL) is the ​ approximate amount needed for the experiment; NOT the amount you need to order from a science ​ supply company.

Calcium chloride (5 g) - 7 Copper(II) chloride (5 g) - 7, 17 Hydrochloric Acid, 32-36% (20 mL) - 14-15 Copper(II) sulfate pentahydrate (10 g) - 12, 14-15 ​ ​ Iron(III) chloride (5 g) - 5 Lead nitrate (5 g) - 5, 13 Lithium chloride (5 g) - 7 Silver nitrate (2 g) - 5 Manganese dioxide (10 g) - 11 Potassium chloride (5 g) - 7 Potassium chlorate (10 g) - 11 Potassium chromate (10 g) - 5, 13 Potassium permanganate (5 g) - 5 Potassium thiocyanate (5 g) - 5 Strontium chloride (5 g) - 7 Sodium hydroxide (2 g) - 18 Phenolphthalein solution (2 mL) - 18

Equipment/Supplies Needed for Each Lab Experiment [These are all summarized in the lists above]

LAB #1 6 test tubes small funnel 3 small beakers (50 mL) black marker (or blue 3 dropper pipets graduated cylinder red, blue, yellow marker or pencil) (medicine droppers) (10 mL) food coloring

LAB #2 None

LAB #3 balance 10 mL graduated 50 mL graduated 100 mL graduated (0.01 g) cylinder cylinder cylinder aluminum cylinder copper cylinder or 250 mL beaker Karo syrup (dark) or wire wire test tube brush Dawn soap pliers (if using wire) dropper pipet

* Note - Aluminum and copper wire can also be used in lieu of the cylinders. Depending on the thickness of the wire, wrap a 18-36 inch piece of the wire into a tight shape (with a set of pliers) so the wire fits easily inside the graduated cylinder.

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- Laboratory balances that are accurate to a tenth of a gram (0.1 g) can also be used if your balance doesn’t record to the hundredth of a gram. Mass measurements in this lab will be to the 0.01 g. if possible.

LAB #4 laboratory balance 10 mL graduated sealable plastic 50 mL beaker (0.01 g) or (0.1 g) cylinder sandwich bag dropper pipet baking soda vinegar scoopula test tube brush Dawn soap

* Note - Mass measurements in this lab will be to the nearest 0.01 g. However, lab balances that are accurate to a tenth of a gram (0.1 g) can also be used. This will be the case for all future laboratory experiments.

LAB #5 wood splints (toothpicks) 9 - test tubes test tube holder

propane/butane torch (or micro burner) microscope glass slide clay triangle ​ ​ forceps crucible 6 dropper pipets ring stand - butane lighter spatula (or scoopula) “pocket” microscope ring clamp test tube brush test tube rack pliers or wire cutter 100 mL graduated cylinder Dawn soap potassium chromate potassium permanganate laboratory balance potassium thiocyanate silver nitrate lead nitrate copper wire (or Cu turnings) sodium chloride (table salt) iron(III) chloride

* Note - Toothpicks can be used in place of wood splints and copper wire can be used in place of copper turnings, needing the wire cutter. Ordinary table salt is sodium chloride.

LAB #6 glass tubing (borosilicate 6 mm OD) triangular file butane/propane torch ​ ​ yardstick (or ruler) ​ small white label scotch tape

* Note - The 6 mm OD (outside diameter) borosilicate glass tubing may be purchased at the Amazon.com website. Copy and paste the URL into your browser:

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https://www.amazon.com/Pack-Glass-Tubing-Borosilicate-Diameter/dp/B017DVI4TC/ref=s r_1_sc_3?ie=UTF8&qid=1502152653&sr=8-3-spell&keywords=borosilicaye+glass+ - There is no Data Table, Calculations, or Table of Physical Properties in this lab write-up. - You will need three 12” pieces of glass tubing, but it’s good to have a few extra. ​ ​ - The portable micro lab burner does not produce a hot enough flame to be used in this expt. ​ ​ LAB #7 portable micro lab burner Q-tips 2 - 250 mL beakers

black marker pen 6 - watch glasses spatula (or scoopula) ​ calcium chloride potassium chloride copper chloride sodium chloride strontium chloride lithium chloride labels distilled water * Note +2 +3 - The Ba ​ (barium cation) and the Fe ​ (iron cation) flame test will be performed by the ​ ​ instructor because they produce fumes that are toxic. Please record your observations as you watch the video podcast.

LAB #8 sharp #2 pencil periodic table Chapter 6 notes

LAB #9 molecular model kit Chapter 8 notes periodic table

* Note - Colored marshmallows and toothpicks may be used in lieu of a molecular model kit.

LAB #10 felt-tipped markers 6 - large test tubes chromatography 50 mL graduated (red, orange, yellow, green, blue) Not permanent markers! with corks paper strips cylinder sharpened #2 pencil scissors & ruler forceps any size beaker distilled (or bottled) test tube rack dropper pipet table salt water

* Note - To prepare the 0.1% NaCl solution, add 0.1 g of NaCl (table salt) to 100 mL of water or ​ just shake a salt a couple times into a small amount (25 mL) of water. - A dense paper towel like Bounty can be used in lieu of chromatography paper if it is not available. Coffee filters have also been used when cut to fit.

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- Corks not available? Use toothpicks to connect to the chromatography strips and use plastic wrap to cover the top of the test tube to prevent evaporation of the solvent. - Please follow directions carefully in this experiment. You may have to do it 2-3 times to get good results. Each time you do an experiment, it is called a “trial.” ​ ​ - The felt-tipped markers cannot be permanent markers, they must be water-soluble. ​ ​ - Smaller test tubes may also be used if larger ones are not available. - When inserting the chromatography paper into the test tube, don’t “splash” the solvent up onto the paper strip. The solvent must start out below the dye on the point of origin. ​ ​ ​ ​ - Students can design experiments to identify the dyes in colored food products such as M&Ms or Skittles. Place candy in 5-6 drops of water. Stir until the candy dissolves. Do lab.

LAB #11 potassium chlorate manganese dioxide crucible & cover

propane/butane torch (or micro burner) forceps clay triangle ​ ​ ring stand with ring clamp scoopula or spatula laboratory balance

* Note

- Please be careful in handling the potassium chlorate. Do not grind or crush KClO3 or mix ​ ​ it with other chemicals unless told to do so.

LAB #12 hydrated copper sulfate wire gauze evaporating dish or crucible propane/butane torch (or micro burner) 800 mL beaker (or larger) dropper pipet ​ ​ ring stand scoopula or spatula laboratory balance ring clamp forceps Dawn soap hot pad holder or gloves test tube brush butane fuel refill canister

* Note - Hydrated copper sulfate can also be purchased at Home Depot, Menards, Fleet Farm or in most hardware stores. - Laboratory balances accurate to 0.1 g can also be used. - A crucible may be used in the place of an evaporating dish.

LAB #13 potassium chromate lead nitrate 2 - 250 mL glass beakers

propane/butane torch (or micro burner) test tube brush marker or pencil ​ ​ ring stand scoopula or spatula laboratory balance forceps 25 mL graduated cylinder butane lighter

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hot pad holder or gloves ring clamp bottled water wire gauze coffee filters funnel clay triangle Dawn soap small metal cookie sheet/cake pan ​ washing bottle (squirt bottle) ​

* Note - Use caution in measuring the potassium chromate and lead nitrate. Measure out the amount you need and dissolve the chemicals in water as soon as possible. - Laboratory balances accurate to 0.1 g can also be used. - Do not use a stirring rod in this experiment. Carefully “swirl” the beakers instead to ​ ​ ​ ​ dissolve the contents.

LABS #14 - #15 hydrated copper(II) sulfate aluminum wire 3.0 M hydrochloric acid

propane/butane torch (or micro burner) test tube brush evaporating dish ​ ​ ring stand stirring rod or scoopula laboratory balance 250 mL glass beaker 25 mL graduated cylinder butane lighter washing bottle (squirt bottle) ring clamp bottled water ​ wire gauze coffee filters funnel pocket microscope Dawn soap forceps microscope glass slide paper towels small metal cookie sheet/cake pan scissors or wire cutter 12” ruler sodium chloride, NaCl

* Note - This experiment is performed in parts over three days and counts as two lab experiments. The student may stop and start at any time, however, they should add water (bottled) to any solutions that have evaporated. - “Hydrated copper(II) sulfate” is copper(II) sulfate pentahydrate. - A magnifier (or magnifying glass) may be used instead of a pocket microscope. - Laboratory balances accurate to 0.1 g can also be used. - 32-36% hydrochloric acid may be used in lieu of 3.0 M HCl It is possible to perform this experiment without using the 3.0 M HCl, (3 molar hydro- chloric acid) but it may result in a slightly higher percent error.

LAB #16 18 mm x 150 mm test tube copper coated steel BB’s test tube holder Master Lab Equipment and Supplies List for ChemExplained.com 7

thermometer bottled water (room temp.) 12 oz. styrofoam cup ring stand ring clamp saucepan from kitchen micro lab burner wire gauze kitchen stove 600 mL or 800 mL beaker laboratory balance

* Note - Instead of using a ring stand, ring clamp, wire gauze, 600 mL or 800 mL beaker and propane/butane torch or micro lab burner, this experiment can be done with a saucepan of boiling water on the kitchen stove. - A styrofoam cup is used as the in this experiment. - A laboratory balance accurate to 0.1 gram may be used. - The exact size of the test tube is not critical, one of similar sizes may be used. - Record temperatures to the nearest 0.1°C throughout the experiment. - If your laboratory balance ever gives you an “error”or “overload” message of some kind, measure out smaller amounts of your substance at a time and then add them together.

LAB #17 6 soda pop cans, Al (empty) copper(II) chloride (~3.0 g) funnel and gloves ​ triangular file or long nail 250 mL or 400 mL beaker laboratory balance stirring rod or spatula 100 mL graduated cylinder small cake pan

* Note - Copper(II) chloride, either anhydrous or dihydrate may be used in this experiment. - The student should have their Ch. 9 notes available during this lab activity. - A 250 mL beaker and 50 mL graduated cylinder can be used in lieu of the 400 mL beaker and the 100 mL graduated cylinder. - A long nail (6” to 8”) may be used instead of a triangular file.

LAB #18 4 - beakers (100 mL - 400 mL) sodium hydroxide (2.00 g) vinegar (1 pint or less) ​ 10 mL graduated cylinder phenolphthalein solution laboratory balance 25 mL graduated cylinder 1 - bottled water paper towels 100 mL graduated cylinder small white labels scoopula (or spatula) 2-3 dropper pipets small funnel Dawn soap white plastic trash bag 250 mL Erlenmeyer flask small brush (or scrub pad) (kitchen size is best) (with cork or rubber ) stirring rod ink pen

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* Note - Sodium hydroxide (NaOH), can be purchased from Home Science Tools in a 30.0 gram bottle. The student needs exactly 2.00 grams of NaOH for this experiment. - Any beakers sized 100 mL to 400 mL beakers can be used. - The size of the Erlenmeyer flask must be at least 100 mL in volume. (100 mL to 400 mL) - Review your Ch. 18 notes on Titration (including the diagram) before starting this activity. - If you can’t find a cork, use a baggie and rubber band to cover the top of the Er. flask. - This is a fairly short experiment, but it takes a lot of explanation. Pay attention to details! - Vinegar is composed of acetic acid (HAc) dissolved in water.

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