fl
O
TestAmerica
Xylenes,
Vinyl
Toluene-d8 Vinyl
4-Bromofluorobenzene Trichlorofluoromethane
Trichloroethene
Dibromofluoromethane Tetrachloroethene
1 Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Surrogate
1,1
Analyte
Date
Preparation:
Date Method:
Dilution:
Client
Client
Lab
Client:
,2,3-Trichloropropane
2,2-Tetrachloroethane
Sample
chloride
acetate
Analyzed:
Prepared:
Matrix:
Sample
Total
Hercules
(Surr)
Savannah
ID:
ID:
Inc.
12/04/2007 200
5030B
12/04/2007 8260B
Water
680-32249-22
HER-MWI7-112807
1741
1741
8260B
Analysis
Volatile
Page
Result
Batch:
%Rec
Organic
91
92
103
<400
<200
<400
<200
<200
<200
<200 210
<200 <200
<200
52
(ug/L)
680-92648
Compounds
of
151
by
Qualifier
GC!MS
Final
Lab
Initial
Instrument
File
Date
WeightNolume: Date
WeightlVolume:
ID:
Sampled:
Received:
ID:
Acceptance
75-
75- 75
-
b0463.d
GC/MS
120
121
120
Job
11/29/2007
11/28/2007
Number:
Limits
Volatiles
400
400
200
200
200
200
200
200
200
200
200
RL
5
5
Analytical
mL mL
-
0923
1505
680-32249-1
B Data
U
U
U
O
Q
4-Methyl-2-pentanone
Styrene
Propionitrile
1,1,1 Pentachloroethane Methyl Methylene
Methacrylonitrile 2-Hexanone
TestAmerica lodomethane
lsobutyl Ethyl trans-i
trans-i
cis-i
Ethylbenzene
cis-1
1
trans-i
Dichlorodifluoromethane
1,i-Dichloroethene
1
Dibromomethane
3-Chloro-1-propene 2-Chloro-i,3-butadiene
1,i-Dichloroethane Chlorodibromomethane
Ethylene
1
Chloromethane
Chloroform Chloroethane Carbon
Chlorobenzene
Carbon Acrylonitrile
2-Butanone Bromomethane
Acetone
Acrolein
Benzene Acetonitrile
Bromoform Dichlorobromomethane
Analyte
,2-Dichloropropane Date
Date
Dilution: Method:
Preparation:
Client
Lab
,2-Dibromo-3-Chloropropane Client Client:
2-Dichloroethane
,3-Dichloropropene
,2-Dichloroethene
2-Tetrachloroethane
methacrylate
Sample
Analyzed:
Prepared:
methacrylate
,4-Dichloro-2-butene
3-Dichloropropene
2-Dichloroethene
Matrix:
Sample
alcohol
tetrachlonde
disulfide
Dibromide
Chloride
Hercules
(MEK)
Savannah
ID:
ID:
Inc.
(MIBK)
5030B
500
12/06/2007
8260B
12/06/2007
Water
680-32249-22
HER-MWI7-112807
1232
1232
8260B
Analysis
Run
Volatile
Type:
Page
Result
Batch;
Organic
<10000
<500
<500 <5000
<500
<2500 <2500
<10000
<20000 <2500
<5000
<500
<500 <500
<500
<500
<500
<500
<500
<500
<500
<500 <1000
<500
<500
<500 <500 <500
<500
4100 41000
<500
<500
890
<1000
<5000
<500
<500 3000
<500 <10000
<20000
<10000
<13000
DL
(ug/L)
53
680-92858
Compounds
of
151
by
D
D
D
Qualifier
D
GCIMS
Final
Lab
Initial
Instwment
File
Date
Date
WeightNolume:
WeightNolume:
ID:
Sampled:
Received:
ID:
b0473.d
GC/MS
Job
11/29/2007 11/28/2007
Number
Volatiles
500
2500
500 5000
500
2500
10000 20000 2500
10000 5000
500
500
500
500
500
500 500
500
500
500
500
500
500
500
1000
500
500 500
500
500
500 500
500
5000
1000 500
500 500
500
20000
10000
10000 RL
13000
5
5
Analytical
mL mL
-
0923
1505
680-32249-1
B Data
TestAmerica
Xylenes,
Vinyl
Vinyl
Trichlorofluoromethane
Toluene-d8 4-Bromofluorobenzene
Trichloroethene
Tetrachloroethene
1 Toluene
Dibromofluoromethane
1,1,2-Trichloroethane
1,1,1-Trichloroethane
1,1
Surrogate
Analyte
Date
Date
Dilution:
Preparation:
Method:
Client
Client
Lab
Client:
,2,3-Trichloropropane
2,2-Tetrachloroethane
Sample
chloride
acetate
Analyzed:
Prepared:
Matrix:
Sample
Total
Hercules
(Surr)
Savannah
ID:
ID:
Inc.
12/06/2007 500
12/06/2007 5030B
8260B
Water
680-32249-22
HER-MWI7-112807
1232
1232
8260B
Analysis
Run
Volatile
Type:
Page
Result
Batch:
%Rec
Organic
89
97
101
<1000
<500 <500
<1000
<500
<500
<500
<500
<500 <500
<500
DL
(ug/L)
54
680-92858
Compounds
of
151
by
Qualifier
GCIMS
Final
Lab
Initial
Instrument
File
Date
Date
WeightNolume:
WeightNolume:
ID:
Sampled:
Received:
ID:
Acceptance
75-
75-
75-
b0473.d
GC/MS
120
120
121
Job
11/29/2007
11/2812007
Number:
Limits
Volatiles
500
500
1000
500
1000 500
500
500
500
500
500
RL
5
5
Analytical
mL mL
-
0923
1505
680-32249-1
B Data
7
J
]
O
0
4-Methyl-2-pentanone
Styrene
Propionitrile
1.1,1 Pentachloroethane
Methyl
Methylene
Methacrylonitrile 2-Hexanone
TestAmerica Isobutyl
trans-i
lodomethane Ethyl cis-i3-Dichloropropene
Ethylbenzene
trans-i
cis-12-Dichloroethene
I trans-i
Dichlorodifluoromethane
11-Dichloroethene
12-Dichloroethane Ethylene
11-Dichloroethane Dibromometharie
Chlorodibromomethane 3-Chloro-1-propene
2-Chloro-1
Chloromethane
Chloroethane
Chlorobenzene 2-Butanone
Carbon
Carbon
Acrylonitrile
Bromoform Acetonitrile Acetone
Bromomethane Acrolein
Dichlorobromomethane
Benzene
Analyte
Date
,2-Dichloropropane
Date
Dilution: Method:
Preparation:
Client
,2-Dibromo-3-Chloropropane Lab Client
Client:
,2-Tetrachloroethane
methacrylate
Sample
Analyzed:
Prepared:
methacrylate
,4-Dichloro-2-butene
3-Dichloropropene
2-Dichloroethene
Matrix:
Sample
alcohol
tetrachlonde
disulfide
Dibromide
Chloride
Hercules
3-butadiene
(MEK)
Savannah
ID:
ID:
Inc.
(MIBK)
12/04/2007
5030B
8260B
12/04/2007
1.0
Water
680-32249-23
HER-MWI8-112707
0452
0452
8260B
Analysis
Volatile
Page
Result
Batch:
Organic
<1.0
<1.0
<20
<5.0
<10
<1.0
<5.0
<20
<5.0
<40
<1.0
<10
<1.0
<1.0
<1.0 <1.0
1.2 <1.0
<1.0
<1.0
1.4 <1.0
<2.0
<1.0
<1.0
<1.0
<1.0
<1.0 <1.0
<1.0
<1.0 26
<1.0
<1.0
<2.0 <1.0
<10
<1.0
<1.0
<20
<20
<40
<25
1.2
55
(ug/L)
680-92630
Compounds
of
151
by
Qualifier
GCIMS
Final
Lab
Initial
Instrument
File
Date
Date
WeightNolume:
Weight/Volume:
ID:
Received:
Sampled:
ID:
b0454.d
GC/MS
Job
11/29/2007
11/27/2007
Number:
Volatiles
20
1.0
1.0 5.0 5.0
20
40
10 5.0
1.0
1
10 1.0
1.0
1.0
1.0
1.0
1.0 2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0 1.0
1.0
1.0 2.0
1.0
1.0 1.0
10 20
1.0
1.0 40
1.0 20
25
1.0
RL
5
5
0
Analytical
mL mL
-
0923
1630
680-32249-1
B Data
U
TestAmerica
Xylenes,
Vinyl
Vinyl
Toluene-d8 4-Bromofluoroberizene
Dibromofluoromethane Tnchlorofluoromethane
Trichloroethene
Toluene
1
1,1
Tetrachloroethene
Surrogate 1,1,1-Trichloroethane
1,1
Analyte
Date
Date
Dilution: Method:
Preparation:
Client
Lab
Client Client:
,2,3-Trichloropropane
,2-Trichloroethane
,2,2-Tetrachloroethane
chloride
acetate
Sample
Analyzed:
Prepared:
Matrix:
Sample
Total
Hercules
(Surr)
Savannah
ID:
ID:
Inc.
12/04/2007
5030B
1.0 8260B
12/04/2007
Water
680-32249-23
HER-MWI8-112707
0452
0452
8260B
Analysis
Volatile
Page
Result
Batch:
%Rec
Organic
94
99
91
<2.0
<1.0
<2.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
56
(ugIL)
680-92630
Compounds
of
151
by
Qualifier
GC!MS
Final
Initial
Lab
Instrument
File
Date
Date
WeightNolume:
WeightNolume:
ID:
Received:
Sampled:
ID:
Acceptance
75
75 75-120 -
-
GC/MS
b0454.d
120
121
Job
11/29/2007
11/27/2007
Limits
Number:
Volatiles
2.0
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0 AL
5
5
AnayticaI
mL mL
-
0923
1630
680-32249-1
B Data
J
J fl
O
fl
fl
O
O
0
Styrene
Propionitrile 4-Methyl-2-pentanone
Pentachloroethane
1,1,1 Methyl
Methylene
Methacrylonitrile
TestAmerica 2-Hexanone
Isobutyl
trans-i
lodomethane Ethyl
Ethylbenzene
trans-i
cis-1,3-Dichloropropene
1,2-Dichloropropane cis-i
trans-i
Dichlorodifluoromethane
i,1-Dichloroethene
1
il-Dichloroethane Dibromomethane
Ethylene Chlorodibromomethane
3-Chloro-1-propene
1,2-Dibromo-3-Chloropropane 2-Chloro-1
Chloromethane
Chloroform
Chloroethane
Chlorobenzene
Carbon
Carbon
2-Butanone
Acrylonitrile
Bromomethane Acrolein
Bromoform
Dichlorobromomethane Acetone
Benzene
Acetonitrile
Analyte
,2-Dichloroethane
Date
Date
Method:
Dilution:
Preparation:
Client
Lab
Client
Client:
,2-Tetrachloroethane
,2-Dichloroethene
methacrylate
Sample
Analyzed:
methacrylate
Prepared:
,3-Dichloropropene
2-Dichloroethene
4-Dichloro-2-butene
alcohol
Matrix:
Sample
tetrachloride
disulfide
Dibromide
Chloride
Hercules
,3-butadiene
(MEK)
Savannah
ID:
ID:
Inc.
(MIBK)
12/04/2007
5030B
1.0
12/04/2007
8260B
Water
680-32249-24
HER-MWI9-112807
1525
1525
8260B
Analysis
Volatile
Page
Result
Batch:
<1.0
<10
<5.0 <1.0
<5.0
<20
Organic
<40
<5.0
<10 2.6
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
1,1 <1.0
<1.0 <1.0
<2.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
10 <2.0
<10
<1.0
<1.0 44
<1.0
<20
<20
<25
<40
.0
57
(ug/L)
680-92648
Compounds
of
151
by
Qualifier
GCIMS
Final
Initial
Lab
Instrument
File
Date
Date
WeightNolume:
WeightfVolume:
ID:
Received:
Sampled:
ID:
b0458.d
GC/MS
Job
1112812007
11/29/2007
Number:
Volatiles
20
1,0 5.0
1.0 5.0 40
20
10
1.0
5.0
10
1.0
1.0
1.0
1.0
1.0
1.0
2.0
1.0 1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0 2.0
1.0
1.0
1.0
10
1.0 20
1.0
1.0 20
40
1.0 25
RL
5
5
Analytical
mL mL
-
0923
0830
680-32249-1
B Data
fl
U
TestAmericaSavannah
Xylenes,
Vinyl
Vinyl
Toluene-d8 4-Bromofluorobenzene
Trichloroethene
Trichlorofluoromethane
Dibromofluoromethane
Toluene
123-Trichloropropane Tetrachloroethene
112-Trichloroethane
1,1
Surrogate
1,1
Analyte
Date
Dilution: Method:
Date Preparation:
Client
Client
Lab
Client:
22-Tetrachloroethane
1-Trichloroethane
chloride
acetate
Sample
Analyzed:
Prepared:
Matrix:
Sample
Total
Hercules
(Surr)
ID:
ID:
Inc.
12/04/2007 8260B
12/04/2007 503DB
1.0
Water
680-32249-24
HER-MWI9-112807
1525
1525
8260B
Analysis
Volatile
Page
Result
Batch:
%Rec
Organic
91
94
102
<2.0
<1.0
<2.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
1.4 <1.0
58
(ug/L)
680-92648
Compounds
of
151
by
Qualifier
GC!MS
Final
Initial
Lab
Instrument
File
Date
Weight/Volume: Date
WeightNolume:
ID:
Received:
Sampled:
ID:
Acceptance
75-
75-
75-
GC/MS
b0458.d
120 120
121
Job
1112912007
11/28/2007
Number:
Limits
Volatiles
2.0
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
RL
1.0
5
5
Analytical
mL mL
-
0923
0830
680-32249-1
B Data
U
U U
U Q 4-Methyl-2-pentanone Styrene Propionitrile Pentachloroethane Methylene 2-Hexanone Methacrylonitrile Methyl trans-i i,1,i,2-Tetrachloroethane trans-i Ethyl cis-i Isobutyl Ethylbenzene lodomethane cis-i trans-i TestAmerica Dichlorodifluoromethane 1,2-Dichloropropane i,1-Dichloroethene Chlorodibromomethane Chloromethane Chloroform 1,2-Dichloroethane li-Dichloroethane Dibromomethane 3-Chloro-1-propene Ethylene 1,2-Dibromo-3-Chloropropane 2-Chloro-i,3-butadiene Carbon Carbon Chloroethane Chlorobenzene 2-Butanone Acrylonitrile Acrolein Acetonitrile Acetone Bromomethane Bromoform Dichlorobromomethane Benzene Analyte Date Dilution: Date Method: Preparation: Client Lab Client: Client ,2-Dichloroethene 3-Dichloropropene Sample methacrylate Analyzed: Prepared: ,3-Dichloropropere methacrylate ,4-Dichloro-2-butene Matrix: 2-Dichloroethene Sample tetrachloride alcohol disulfide Dibromide Hercules Chloride (MEK) Savannah ID: ID: Inc. (MIBK) 5030B 12/03/2007 8260B 1.0 12/03/2007 Water 680-32249-25 HER-RSI-112607 1852 1852 8260B Analysis Volatile Page Result Batch: Organic <1.0 <5.0 <1.0 <20 <5.0 <10 <1.0 <20 <40 <1.0 <5.0 <10 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 <1.0 <1.0 <10 <1.0 <1.0 <1.0 <20 <20 <40 <25 (ug/L) 59 680-92536 Compounds of 151 by Qualifier GCIMS Final Instrument Initial Lab File Date Date WeightNolume: WeightNolume: ID: Sampled: Received: ID: GCIMS b0443.d Job 11/29/2007 11126/2007 Number: Volatlles 20 5.0 40 5.0 1.0 20 1.0 10 1.0 5.0 10 1.0 1.0 1.0 1.0 1.0 2,0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 2.0 1.0 1.0 1.0 1.0 1.0 1.0 20 40 1.0 1.0 20 10 25 1.0 1.0 1.0 RL 5
5 Analytical mL mL - 0923 1425 680-32249-1
B Data
U
kj
fl
fl
TestAmerica
Xylenes,
Vinyl
Vinyl
Toluene-d8
Trichlorofluoromethane
4-Bromofluorobenzene Trichloroetherie Tetrachloroethene
Toluene
Dibromofluoromethane
i 1,1,2-Trichloroethane
1,1,1-Trichloroethane
1,1
Surrogate
Analyte
Date
Date Preparation:
Method:
Dilution:
Client
Lab
Client Client:
,2,3-Tnchloropropane
2,2-Tetrachloroethane
Sample
chloride
acetate
Analyzed:
Prepared:
Matrix:
Sample
Total
Hercules
(Surr)
Savannah
ID:
ID:
Inc.
5030B
8260B
12/03/2007
12)03/2007
1.0
Water
680-32249-25
HER-RSI
1852
1852
-112607
8260B
Analysis
Volatile
Page
Result
Batch:
%Rec
Organic
96
99
87 <2.0
<1.0
<1.0
<2.0
<1.0 <1.0
<1.0 6.1 <1.0
<1.0
<1.0
(ug/L)
60
680-92536
Compounds
of
151
by
Qualifier
GCIMS
Final
Lab
Initial
Instrument
File
Date
Date
WeightNolume:
WeightNolume:
ID:
Sampled:
Received:
ID:
Acceptance
75
75- 75-
-
b0443.d
GCIMS
120 121
120
Job
11/29/2007
11126/2007
Number
Limits
Volatiles
2.0
2.0
1.0
1.0
1.0
1.0 1.0
1.0
1.0 5
1.0
1.0 RL
5
AnaIytica
mL mL
-
0923
1425
680-32249-1
B Data
n
J
O
Q
Styrene
4-Methyl-2-pentanone
1,11 Propionitrile
Pentachloroethane Methyl
Methacrylonitrile
TestAmerica Methylene
2-Hexanone
lodomethane Ethyl trans-i
Isobutyl
Ethylbenzene cis-1 trans-i
cis-1
1
1,1-Dichloroethene trans-i
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane Ethylene Chlorodibromomethane
Dibromomethane
3-Chloro-1-propene
2-Chloro-1 Chloroform
1 Chloromethane
Chloroethane Carbon
Chlorobenzene Carbon
2-Butanone
Acrylonitrile
Bromoform Acrolein Acetone
Bromomethane Dichlorobromomethane Acetonitrile
Benzene
Analyte
,2-Dichloropropane
Date
Date
Dilution: Method:
Preparation: Client
,2-Dibromo-3-Chloropropane
Lab Client
Client:
,3-Dichloropropene
2-Tetrachloroethane
2-Dichloroethene
methacrylate
Sample
Analyzed:
Prepared:
methacrylate
,3-Dichloropropene
,2-Dichloroethene
,4-Dichloro-2-butene
Matrix:
alcohol
Sample
tetrachloride
disultide
Dibromide
Chloride
Hercules
3-butadiene
(MEK)
Savannah
ID:
ID:
Inc.
(MIBK)
5030B
12/03/2007 8260B
12/03/2007
1.0
Water
680-32249-26
HER-RS2-1
1920
1920
12707
8260
B
Analysis
Volatile
Page
Result
Batch:
<1.0
<1.0
<5.0
<20 <10 Organic
<1.0
<5.0
<20
<40
<10
<5.0 <1.0
<1.0
<1.0
<1.0
<1.0 <1.0
<1.0 <1.0
<1.0
<1.0
<2.0
<1.0
<1.0
<1.0 <1.0
<1.0
<1.0
<1.0 <1.0
<1.0
<1.0
<1.0
<1.0
<10
<2.0
<1.0
<1.0
<1.0
<1.0
<20
<20
<25
<40
61
(ug/L)
680-92536
Compounds
of
151
by
Qualifier
GC!MS
Final
Initial
Lab
lnstwment
File
Date
Date
WeightNolume:
WeightNolume:
ID:
Received:
Sampled:
ID:
GC/MS
b0444.d
Job
11129/2007
11/27/2007
Number:
Volatiles
20
1
5.0
1.0
40
20
10 5.0
1.0
5.0
10
1.0
1.0
1.0
1.0
1.0 1.0
1.0 1.0
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
2.0
1.0
1.0
1.0
10
1.0 20 40
1.0 20
1.0
25
1.0
RL
5
0 5
Analytical
mL mL
-
0923
0915
680-32249-1
B Data
ri
fJ
TestAmerica
Xylenes,
Vinyl
Vinyl
Toluene-d8
Trichloroethene
4-Bromofluorobenzene Tnchlorofluoromethane
Dibromofluoromethane Toluene
1,2,3-Trichloropropane
Tetrachloroethene
11,1-Trichloroethane
1,12-Trichloroethane
Surrogate 1
Analyte
Date
Date
Dilution:
Preparation:
Method:
Client
Client
Lab
Client:
1
2,2-Tetrachloroethane
chloride
Sample
acetate
Analyzed:
Prepared:
Matrix:
Sample
Total
Hercules
(Surr)
Savannah
ID:
ID:
Inc.
5030B
12)03/2007
12/03/2007
1.0 8260B
Water
680-32249-26
HER-RS2-1
1920
1920
12707
8260B
Analysis
Volatile
Page
Result
Batch:
%Rec
Organic
95
99
86
<1.0
<2.0
<1.0
<2.0 <1.0
<1.0
<1.0 6.8
<1.0
<1.0
<1.0
62
(ug/L)
680-92536
Compounds
of
151
by
Qualifier
GCIMS
Final
Initial
Lab
Instrument
File
Date
Date
WeightNolume:
WeightNolume:
ID:
Received:
Sampled:
ID:
Acceptance
75-
75 75 -
-
b0444.d
GC/MS
121
120
120
Job
11/29/2007
11)27/2007
Number:
Limits
Volatiles
2.0
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0 RL
5
5
Analytical
mL mL
-
0923
0915
680-32249-1
B Data
7
J ‘1
J
U
U
U
fl
O
Q
fl
4-Methyl-2-pentanone
Styrene
Propionitrile
Pentachloroethane Methyl
1ii2-Tetrachloroethane Methylene
TestAmerica Methacrylonitrile
2-Hexanone
lodometharie trans-I
Isobutyl
Ethyl
Ethylbenzene cis-1 trans-12-Dichloroethene
cis-1
1
il-Dichloroethene
trans-i
Dichlorodifluoromethane
il-Dichloroethane
1
Ethylene
Dibromomethane
Chlorodibromomethane
1 2-Chloro-1,3-butadiene
3-Chloro-1-propene
Chloromethane
Chloroform
Chloroethane
Chlorobenzene
Carbon 2-Butanone
Carbon
Bromomethane Acrylonitrile
Dichlorobromomethane
Bromoform Acetonitrile
Acrolein
Benzene Acetone
Analyte
,2-Dichloroethane
Date
Date
2-Dichloropropane Dilution:
Preparation:
Method:
Client
Lab Client
Client:
2-Dibromo-3-Chloropropane
3-Dichloropropene
2-Dichloroethene
methacrylate
Sample
methacrylate
Analyzed:
Prepared:
,4-Dichloro-2-butene
3-Dichloropropene
alcohol
Matrix:
tetrachlonde Sample
disulfide
Dibromide
Chloride
Hercules
(MEK)
Savannah
ID:
ID:
Inc.
(MIBK)
12)04/2007
5030B
12/04/2007 8260B
1.0
Water
680-32249-27
HER-RS3-112807
1901
1901
826DB
Analysis
Volatile
Page
Result
Batch:
<1.0
<1.0
<20 <10
<5.0
<5.0
<1.0 <20
<40
<5.0
<10
<1.0
<1.0
<1.0 Organic
<1.0
<1.0
<1.0
<1.0 <1.0
<1.0
<1.0
<2.0
<1.0
<1.0 <1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<10
<2.0 <1.0
<1.0
<1.0
<20
<1.0
<20
<40
<25
63
(ug/L)
680-92648
Compounds
of
151
by
Qualifier
GC/MS
Final
Lab
Initial
Instrument
File
Date
Date
Weight)Volume:
Weight)Volume:
ID:
Sampled:
Received:
ID:
b0466.d
GC/MS
Job
11/29/2007
11/28/2007
Number:
20
1.0 5.0
1.0
10 5.0 40 Volatiles
20
1.0 5.0
1.0
10
1.0
1.0
1.0
1.0
1.0
1.0
1.0
2.0
1.0
1.0
1.0
1.0
1.0 1.0
1.0
1.0
1.0
1.0
1.0
1.0
2.0
1.0
1.0
1.0
10
20
1.0 40
1.0 20
1.0
25
RL
5
5
Analytical
mL mL
-
0923
0920
680-32249-1
B Data
fl
fl
O
TestAmerica
Xylenes,
Vinyl
Vinyl
Toluene-d8
4-Bromofluorobenzene
Trichlorofluoromethane
Dibromofluoromethane Trichloroethene
1
Toluene
Tetrachloroethene
Surrogate
1,1,2-Trichloroethane
1,1
1,1,2,2-Tetrachloroethane
Analyte
Date
Date
Dilution:
Preparation:
Method:
Client
Lab
Client
Client:
2,3-Trichloropropane
1-Thchloroethane
chloride
acetate
Sample
Analyzed:
Prepared:
Matrix:
Sample
Total
Hercules
(Surr)
Savannah
ID:
ID:
Inc.
5030B
1210412007
12/04/2007
1.0 8260B
Water
680-32249-27
HER-RS3-112807
1901
1901
8260B
Analysis
Volatile
Page
Result
Batch:
%Rec
Organic
91
93
101
<2.0
<1.0
<2.0
<1.0
<1.0
<1.0
<1.0 <1.0
5.5
<1.0
<1.0
64
(ug/L)
680-92648
Compounds
of
151
by
Qualifier
GC/MS
Final
Initial
Lab
Instrument
File
Date
WeightNolume:
Date
WeightNolume:
ID:
Received:
Sampled:
ID:
Acceptance
75-
75-
75-
b0466.d
GC/MS
120
121
120
Job
11/29/2007
11/28/2007
Limits
Number:
Volatiles
2.0
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0 RL
1.0
1.0
5
5
Analytical
mL mL
-
0923
0920
680-32249-1
B Data
fl
J
J
fl
U
fl
fl
Q
O
C
4-Methyl-2-pentanone
Styrene
Propionitrile Methyl
Pentachloroethane Methacrylonitrile
1,1,1 Methylene
2-Hexanone
TestAmerica lodomethane trans-i
Isobutyl Ethyl
trans-i
Ethylbenzene cis-1
cis-1
1
trans-i
1,1-Dichloroethene Dichlorodifluoromethane
1 1,1-Dichloroethane Dibromomethane
Ethylene
2-Chloro-1
Chlorodibromomethane
i 3-Chloro-1-propene
Chloromethane
Chloroform
Chloroethane
Chlorobenzene
Carbon Carbon
2-Butanone
Acrylonitrile
Acrolein
Bromomethane Bromoform Acetonitrile Acetone
Dichlorobromomethane
Benzene
Analyte
,2-Dichloropropane
Date
Date Preparation:
Dilution: Method:
Client
,2-Dibromo-3-Chloroproparie
Lab
Client Client:
2-Dichloroethane
,2-Dichloroethene
2-Tetrachloroethane
3-Dichloropropene
methacrylate
Sample
Analyzed:
Prepared:
methacrylate
,3-Dichloropropene
,2-Dichloroethene
,4-Dichloro-2-butene
Matrix:
alcohol
Sample
tetrachloride
disulfide
Dibromide
Chloride
Hercules
,3-butadiene
(MEK)
Savannah
ID:
ID:
Inc.
(MIBK)
5030B
12/04/2007 8260B
12/04/2007
1.0
Water
680-32249-28
HER-FDI-112707
0519
0519
8260B
Analysis
Volatile
Page
Result
Batch:
Organic
<1.0 <20
<1.0
<10
<5.0
<1.0
<5.0
<20
<40
<10
<1.0
<5.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0 <1.0
<1.0
<2.0
<1.0
<1.0 <1.0
<1.0 <1.0
<1.0
<1.0
<1.0 <1.0
<1.0
<1.0
<2.0
<10
<1.0
<1.0
<1.0
<1.0
<20
<20 <40
<25
65
(ug/L)
680-92630
Compounds
of
151
by
Qualifier
GCIMS
Final
Lab
Initial
Instrument
File
Date
Date
WeightNolume:
Weight/Volume:
ID:
Sampled:
Received:
ID:
b0455.d
GC/MS
Job
11/29/2007 11/27/2007
Number:
Volatiles
20
1.0 5.0
1.0
10 20
40
5.0
1.0
5.0
10
1.0
1,0
1.0 1.0
1.0
1.0
1.0 2.0
1.0
1.0
1.0
1.0
1.0 1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0 1.0 2.0
1.0
10 20
1.0 40
1.0
1.0 20
1.0 25
RL
5
5
Analytical
mL mL
-
0000
0923
680-32249-1
B Data
O
Li fl
U
fl
Q
TestAmerica
Xylenes,
Vinyl
Vinyl
Trichlorofluoromethane
Toluene-d8
4-Bromofiuorobenzene Trichloroethene
Tetrachloroethene
Dibromofluoromethane Toluene
1 1,1
1,1,1-Trichloroethane
Surrogate
1,1
Analyte
Date Preparation:
Date Method:
Dilution:
Client
Lab
Client
Client:
,2,3-Trichloropropane
,2-Trichloroethane
2,2-Tetrachloroethane
Sample
chloride
acetate
Analyzed:
Prepared:
Matrix:
Sample
Total
Hercules
(Sun)
Savannah
ID:
ID:
Inc
5030B
8260B
12104/2007
12)04/2007 1.0
Water
680-32249-28
HER-FDI-112707
0519 0519
.
8260B
Analysis
Volatile
Page
Result
Batch:
%Rec
Organic
94
<2.0 <1.0
101
100
<1.0
<2.0 <1.0
<1.0
<1.0
<1.0
<1.0 <1.0
<1.0
(ug/L)
66
680-92630
Compounds
of
151
by
Qualifier
GC!MS
Final
Lab
Instrument
Initial
File
Date
Date
WeightNolume:
WeightNolume:
ID:
Sampled:
Received:
ID:
Acceptance
75-
75-121
75-
b0455.d
GC/MS
120
120
Job
11/27/2007
11/29/2007
Number:
Limits
Volatiles
2.0
2.0
1.0
1.0
1.0 1.0
1.0
1.0
1.0 RL
1.0 1.0
5
5
Analytical
mL mL
-
0000
0923
680-32249-1
B Data
‘1
J
II
L
fl
Styrene
1,1,1 Propionitrile 4-Methyl-2-pentanone
Pentachloroethane
Methyl Methacrylonitrile
Methylene
TestAmericaSavannah
2-Hexanone
Isobutyl trans-i
lodomethane
Ethyl
Ethylbenzene cis-1 trans-1,2-Dichloroethene
cis-i
I trans-i
1,1-Dichloroethene
Dichlorodifluoromethane
1,1-Dichloroethane
Dibromomethane
1,2-Dichloroethane Chlorodibromomethane
Ethylene
3-Chloro-1-propene
2-Chloro-i,3-butadiene
1,2-Dibromo-3-Chloropropane Chloromethane
Chloroform
Chloroethane
Chlorobenzene
Carbon
Carbon
2-Butanone
Acrolein
Bromomethane Dichlorobromomethane Acrylonitrile
Bromoform Acetone
Acetonitrile
Benzene
Analyte
,2-Dichloropropane
Date
Date
Dilution:
Method:
Preparation: Client
Lab Client
Client:
,3-Dichloropropene
,2-Dichloroethene
2-Tetrachloroethane
methacrylate
Sample
Analyzed:
Prepared:
methacrylate
,3-Dichloropropene
,4-Dichloro-2-butene
Matrix:
alcohol
Sample
tetrachloride
disulfide
Dibromide
Chloride
Hercules
(MEK)
ID:
ID:
Inc.
(MIBK)
5030B
12/04/2007 8260B
12/04/2007
1.0
Water
680-32249-29
HER-FD2-112807
1619
1619
8260B
Analysis
Volatile
Page
Result
Batch:
<1.0
<1.0
<20 Organic
<5.0
<10 <5.0
<1.0
<20 <5.0
<40 <10
<1.0
<1.0
<1.0
<1.0
<1.0 4.1
<1.0 <1.0
<1.0
<1.0
<2.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0 2.1
<1.0
<1.0
<1.0
<1.0
<2.0
<10
<1.0
<1.0
<1.0
9.4
<20
<20
<40
<25
67
(ug/L)
680-92648
Compounds
of
151
by
Qualifier
GC/MS
Final
Initial
Lab
Instrument
File
Date
Date
WeightNolume:
Weight/Volume:
ID:
Received:
Sampled:
ID:
b0460.d
GC/MS
Job
11/29/2007
11/28/2007
Number:
Volatiles
20
1.0 5.0
1.0 5.0 40
20
10 5.0
1.0
10
1.0
1.0
1.0 1.0
1.0
1.0
1.0
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
2.0
1.0
1.0
1.0
1.0
10
1.0
20 40
1.0
20
1.0
1.0 25
RL
5
5
Analytical
mL mL
-
0923
0000
680-32249-1
B Data
U
U
TestAmericaSavannah
Xylenes,
Vinyl
Vinyl
4-Bromofluorobenzene
Toluene-d8
Trichlorofluoromethane
Dibromofluoromethane Tnchloroethene
i Toluene
Tetrachloroethene
Surrogate 11,1-Trichloroethane
1,1,2-Tnchloroethane
11,2,2-Tetrachloroethane
Analyte
Date
Date
Dilution:
Method:
Preparation:
Client
Lab
Client
,2,3-Trichloropropane Client:
chloride
acetate
Sample
Analyzed:
Prepared:
Matrix:
Sample
Total
Hercules
(Surr)
ID:
ID:
Inc.
503DB
12104/2007
12/04/2007
1.0 826DB
Water
680-32249-29
HER-FD2-112807
1619
1619
826DB
Analysis
Volatile
Page
Result
Batch:
%Rec
Organic
91
96
103
<2.0
<1.0
<2.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
1.6
68
(ug/L)
680-92648
Compounds
of
151
by
Qualifier
GC/MS
Final
Initial
Lab
Instwment
File
Date
WeightNolume:
Date
WeightNolume:
ID:
Received:
Sampled:
ID:
Acceptance
75-
75-
75-
b0460.d
GC/MS
121
120
120
Job
11/29/2007
11)28/2007
Limits
Number:
Volatiles
2.0
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0 RL
1.0
5
5
Analytical
mL mL
-
0923
0000
680-32249-1
B Data
U
J
fl
L
O
4-Methyl-2-pentanone
Propionitrile
Styrene Pentachloroethane
1,11
Methyl
Methylene
Methacrylonitrile 2-Hexanone
TestAmerica Isobutanol trans-i
lodomethane
Ethylbenzene
Ethyl
cis-i
trans-i
cis-1,2-Dichloroethene
1 trans-i
1,i-Dichloroethene 1 Dichlorodifluoromethane
i,1-Dichloroethane
Dibromomethane
1 Dibromochloromethane
3-Chloro-1-propene
Chloromethane
Chloroform
1 Chloroethane
Chloroprene
Chlorobenzene
Carbon 2-Butanone
Carbon
Bromomethane Acrylonitrile
Acrolein
Bromodichloromethane Acetonitrile
Benzene Acetone
Bromoform
Analyte
Date
Dilution:
Date Preparation:
Method:
,2-Dibromo-3-Chloropropane Client
Lab
Client
Client:
2-Dichloropropane
2-Dichloroethane
2-Dibromoethane
,2-Tetrachloroethane
3-Dichloropropene
methacrylate
Sample
Analyzed:
Prepared:
methacrylate
,2-Dichloroethene
,4-Dichloro-2-butene
3-Dichloropropene
Matrix:
Sample
tetrachloride
disulfide
Chloride
Hercules
Savannah
ID:
ID:
Inc.
40
5030A
12/07/2007
12/07/2007
8260B
Solid
680-32249-30
HER-DAI-112807
1425
1425
DryWt
Corrected:
8260B
Analysis
Volatile
Y
Page
%
Result
Batch:
Moisture:
Organic
<250
<250 <1200
<4900
<1200 <250
<250 <4900
<9900
<250
<1200 <250
<250
<250
<250
<250
<250
<250
<250
<250
<250
<490
<250 <250 <250
<250
<490
<250
<250
<250
<250
<250
<250
<250
<250 <1200
<250
<250
<250
<250
<4900
<4900
<2500
<9900
69
(ug/Kg)
680-92984
Compounds
of
18.8
151
by
Qualifier
GCIMS
Final
Initial
Lab
Instrument
File
Date
Date
WeighiNolume:
Weight/Volume:
ID:
Sampled:
Received:
ID:
l0014,d
GC/MS
Job
11/29/2007
11)2812007
Number:
Volatiles
250 4900
250
250
250
4900
1200
1200
9900
250
250
1200 250
250
250
250
250
250
250
250 490
250
250
250 490
250
250
250
250
250
250
250
250
250
250
250
250
250
250 4900
1200 4900
2500
9900
RL
5
5
Analytical
g mL
-
0923
1530
680-32249-1
L Data Analytical Data
Client: Hercules Inc. Job Number 680-32249-1
Client Sample ID: HER-DAI-112807
Lab Sample ID: 680-32249-30 Date Sampled: 11/28/2007 1530 Client Matrix: Solid % Moisture: 18.8 Date Received: 11/29/2007 0923
8260B Volatile Organic Compounds by GCIMS
Method: 8260B Analysis Batch: 680-92984 Instrument ID: GC/MS Volatiles - L j Preparation: 5030A Lab File ID: 10014.d Dilution: 40 InitialWeight/Volume: 5 g Date Analyzed: 12/07/2007 1425 Final WeightNolume: 5 mL Date Prepared: 12/07/2007 1425
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier RL <250 250 11,2,2-Tetrachloroethane Tetrachloroethene <250 250 Toluene <250 250 1,1,1-Trichloroethane <250 250 11,2-Trichloroethane J <250 250 Tnchloroethene <250 250 Trichlorofluoromethane <250 250 1,23-Trichloropropane <250 250 Vinyl acetate 3 <490 490 Vinyl chloride <250 250 Xylenes, Total 960 490
Surrogate %Rec Acceptance Limits 4-Bromofluorobenzene 82 65- 124 Dibromofluoromethane 87 65- 124 Toluene-d8 (Surr) 72 65- 132
TestAmerica Savannah Page 70 of 151 Data
L
680-32249-1
1550
0923 -
g mL
Analytical
5 5
120000 RL 61000 120000 240000
6100 6100 6100 6100 31000 6100 6100 6100 6100 6100 12000 6100 6100 6100 12000 6100 6100 6100 6100
6100 6100 6100 6100 6100 6100 6100 6100 6100 31000 6100 120000 6100 240000
120000 6100 6100 31000 31000
Volatiles 6100 6100
Number
11/29/2007 11/28/2007
Job
GC/MS 11835.d
ID:
Received: Sampled:
ID:
Weight/Volume:
WeightNolume: Date Date
File
lnstwment
Lab Initial Final
GC/MS
Qualifier
by
151
18.1
of
Compounds
680-92548
(ug/Kg)
71
<61000
<120000 <240000 <120000 <6100 <6100 <6100
<31000 <6100 <6100 <6100 <6100
<6100 <6100 <6100 <6100 <6100
<6100 <12000 <6100 <6100
<12000 <6100 <6100 <6100 <6100 <6100 <6100 <6100 <6100 Organic <6100 <6100 <31000 <6100 <6100 <240000
<6100 <120000 <6100
<31000 <31000 <6100 <120000 Moisture: <6100
Batch:
Result
%
Page
Y
Volatile
Analysis
8260B
Corrected:
DryWt
1856
1856
HER-DA2-112807
680-32249-31 Solid
1000 11/30/2007 8260B 11/30/2007 5030A
Inc.
ID:
ID:
Savannah
Hercules
Chloride
Sample
disulfide
tetrachloride
Matnx:
4-Dichloro-2-butene
3-Dichloropropene
Prepared:
Analyzed: ,2-Dichloroethene
methacrylate
Sample
methacrylate
,3-Dichloropropene
,2-Tetrachloroethane
1
Client.
Client Lab
Client
Method: Dilution: Preparation: Date
Date
Analyte
1
Acetone Benzene Acrolein Acetonitrile Bromodichloromethane Bromoform Acrylonitrile Bromomethane
Carbon 2-Butanone Carbon Chlorobenzene Chloroethane Chloroprene
Chloroform Chloromethane Dibromochloromethane 3-Chloro-1-propene 1,2-Dibromoethane 1,2-Dibromo-3-Chloropropane Dibromomethane
1,2-Dichloroethane 1,1-Dichloroethane Dichlorodifluoromethane trans-i 1,2-Dichloropropane 1,1-Dichloroethene cis-1,2-Dichloroethene
trans-i cis-1 Ethylbenzene
trans-i Ethyl lodomethane 2-Hexanone lsobutanol
Methacrylonitrile Methylene Methyl TestAmerica
Pentachloroethane Propionitrile Styrene 4-Methyl-2-pentanone
‘Q
J Data
L
680-32249-1
1550
0923 -
g mL
Analytical
5
5
RL
6100 6100
6100 6100 6100 12000 6100 6100 12000 6100 6100
Volatiles
Number: Limits
11/28/2007 11/29/2007
Job
124 124 132
GCIMS 11835.d
65-
65- 65-
Acceptance
ID:
Sampled: Received:
ID:
Weight/Volume:
Weight/Volume: Date Date
File
Instrument Initial Lab
Final
GCIMS
Qualifier
X X X
by
151
18.1
of
Compounds
660-92548
(ug/Kg)
72
<6100 <6100 <6100 <6100 <6100 <6100 <6100 <12000 <6100 <6100 <12000
0 0 0
Organic
Moisture:
%Rec
Batch:
Result
%
Page
Y
Volatile
Analysis
8260B
Corrected:
DryWt
12807
1856 1856
HER-DA2-1
Solid 680-32249-31
1000
8260B 11/30/2007 11/30/2007 5030A
Inc.
ID:
ID:
Savannah
(Surr)
Hercules
Total
Sample
Matnx:
Prepared:
Analyzed:
Sample
acetate chlonde
-Trichloroethane
2,2-Tetrachloroethane
Client:
Client Lab
Client
Preparation: Method: Dilution: Date Date
Analyte
1,1
1,1.1 1,1,2-Trichloroethane Surrogate Tetrachloroethene Toluene
1,2,3-Trichloropropane Trichlorofluoromethane Trichloroethene Dibromofluoromethane 4-Bromofluorobenzene Vinyl Toluene-d8 Vinyl Xylenes,
TestAmerica
J j Data
B
680-32249-1
0000 0923 -
mL mL
Analytical
5 5 RL
1.0 20 1.0 25 20 1.0 40 1.0
10 1.0 1.0 1.0 2.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0
2.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 10
1.0 10 5.0 40 5.0 20 1.0 5.0 1.0 20
Volatiles
Number:
11/28/2007 11/29/2007
Job
b0455.d GC/MS
ID:
Sampled: Received:
ID:
Weight/Volume:
Weight/Volume:
Date Date
File
Instrument Lab Initial Final
GC/MS
Qualifier
by
151
of
Compounds
680-92648
(ug/L)
73
<25 <40 <20 <20 <1.0 <1.0
<1.0 <1.0 <10 <2.0 <1.0 <1.0 <1.0
<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
<1.0 <1.0 <1.0 <1.0 <5.0 <10 <20 <5.0 <40 <10 <1.0 Organic <20 <5.0 <1.0 <1.0
Batch:
Result
Page
Volatile
Analysis
82608
1403
1403
BLANK
TRIP
680-32249-32TB
Water
1.0 5030B 12/04/2007 8260B 12/04/2007
(MIBK)
Inc.
ID:
ID:
Savannah
(MEK)
Hercules
Chloride
Dibromide
disulfide
Sample tetrachlonde
Matrix:
alcohol
3-Dichloropropene
,4-Dichloro-2-butene
,2-Dichloroethene
Prepared:
Analyzed: methacrylate
Sample
methacrylate
,2-Dichloroethene
,2-Tetrachloroethane
2-Dibromo-3-Chloropropane
Client: Client Lab
Client
Preparation: Method: Dilution: Date Date
,2-Dichloroethane
,2-Dichloropropane Analyte
Acetonhtrile Benzene Acetone Dichlorobromomethane Bromomethane Acrylonitrile Acrolein Bromoform
2-Butanone Carbon Carbon Chlorobenzene Chloroethane
Chloromethane Chloroform 3-Chloro-i-propene 1 2-Chloro-i,3-butadiene Chlorodibromomethane Ethylene Dibromomethane 1,1-Dichloroethane 1 1,1-Dichloroethene DicNorodifluoromethane trans-i 1
cis-i trans-i cis-1,3-Dichloropropene Ethylbenzene
trans-i Ethyl lodomethane 2-Hexanone Isobutyl TestAmerica Methacrylonitrile Methylene Methyl Propionitrile Pentachloroethane 1,1,1 4-Methyl-2-pentanone Styrene
( Data
B
680-32249-1
0923 0000 -
mL mL
Analytical
5 5
1.0 RL 1.0 1.0 1.0 1.0 1.0 1.0 1.0
1.0
2.0
2.0
Volatiles
Number:
Limits
11/28/2007
11/29/2007
Job
120
120 121
GC/MS b0455.d -
75 75- 75-
Acceptance
ID:
Sampled: Received:
ID:
WeightNolume:
Date WeightNolume: Date
File
Instrument
Lab Initial Final
GC/MS
Qualifier
by
151
of
Compounds
680-92648
(ug/L)
74
<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 <2.0
106
92
89
Organic
%Rec Batch:
Result
Page
Volatile
Analysis
8260B
1403
1403
BLANK
TRIP
680-32249-32TB
Water
1.0
826DB 12/04/2007
503DB 12/04/2007
Inc.
ID:
ID:
Savannah
(Surr)
Hercules
Total
Sample
Matrix:
Prepared: Analyzed:
Sample
acetate chloride
,1-Tnchloroethane ,2-Trichloroethane
Client: Client Lab
Client
Method: Preparation: Dilution: Date Date
Analyte
1,1,2,2-Tetrachloroethane
1,1 1,1 Tetrachloroethene Toluene Surrogate
Tnchloroethene 1,2,3-Trichloropropane Tnchlorofluoromethane
Dibromofluoromethane Vinyl 4-Bromofluorobenzene Vinyl Xylenes, Toluene-d8
TestAmerica
J j Data
T -
680-32249-1
1530
0923
g
mL
uL
AnaIytcaI
15.04
.5 1
RL
2000
2000 2000 2000 2000 2000 2000 2000 2000 2000 2000 2000 2000 2000 2000 2000 2000 10000 2000 2000 2000 2000 2000 2000 2000 2000 2000 2000 10000 2000 2000 2000 2000 10000 2000 2000 2000 10000 10000 4100 2000
2000 2000 2000
SemiVolatiles
Number:
1112812007 11/29/2007
Job
GC/MS t4269.d
(GC/MS)
ID:
Received: Sampled:
Volume:
ID:
WeightNolume:
Weight/Volume:
Date Date
File
Instrument Lab Initial Final Injection
Spectrometry
Qualifier
151
18.8
of
680-93535
Chromatography/Mass
(ug/Kg)
75
680-92817
<2000 <2000 <2000 <2000 <2000 <2000 <2000 <2000 <2000
Gas <2000 <2000 <2000 <2000
<2000 <2000 <2000 <2000 <2000 <2000 <2000 <10000 <2000 <2000 <2000 <2000 <2000 <2000 <2000 <2000 <2000 <2000 <10000 <2000 <2000 <2000 <2000 <4100 <2000 <10000 <10000 <10000 <2000 <2000 <2000
Moisture:
Batch:
Result
by
%
Page
Batch:
Y
Prep
Analysis
Compounds
Corrected:
DryWt
-112807
Semivolatile
1827
1534
8270C
HER-DAI
Solid 680-32249-30
12)1312007
3550B 8270C 5.0 12/06/2007
ether
Inc.
ID:
none
phenyl
ID:
ui
Savannah
Hercules
phthalate
Sample
Matrix:
Prepared:
Analyzed:
Sample
Methylphenol
4
2,4,5-Tetrachlorobenzene 24-Trichlorobenzerie 2-Dichlorobenzene 3,5-Trinitrobenzene 3-Dichlorobenzene 3-Dinitrobenzene
4-Dichlorobenzene 4-Dioxane 4-Naphthoq
Client:
Client Lab Client
Preparation: Method:
Dilution: Date -Naphthylamine Date
&
Analyte
Acenaphthene 1,1-Biphenyl Thionazin Pyridine 1 Sulfotepp I 1 1 I 1 I I 1
I
2,4,5-Trichlorophenol 234,6-Tetrachlorophenol 2,4,6-Trichlorophenol 2,4-Dichlorophenol 2,4-Dimethylphenol 2,4-Dinitrophenol 2,4-Dinitrotoluene Dimethyl 2,6-Dichlorophenol
2,6-Dinitrotoluene 2-Acetylaminofluorene 2-Chlorophenol 2-Chloronaphthalene 2-Methylnaphthalene 2-Methylphenol 2-Naphthylamine 2-Nitrophenol 2-Nitroaniline 2-Picoline 2-Toluidine 3 3,3-Dichlorobenzidine 33’-Dimethylbenzidine TestAmerica 3-Methylcholanthrene 3-Nitroaniline
4,6-Dinitro-2-methylphenol 4-Aminobiphenyl 4-Bromophenyl
4-Chloro-3-methylphenol
j j 4’ R Data
T -
680-32249-1
1530
0923
g
mL
uL
Analytical
15.04
.5 1
RL 10000 10000 4100 2000
20000 2000 2000 2000
410000 2000 4100 2000 2000 2000 2000 2000 2000 2000 2000 2000 2000 2000 2000 2000 2000 2000 2000 2000 2000 2000 2000 2000 2000 1000000 2000 2000 2000 2000
2000 2000 SemiVolatiles 2000 2000
2000 410000
Number:
11/28/2007 11/29/2007
Job
GCIMS
t4269.d
(GCIMS)
ID:
Sampled:
Received:
Volume: ID:
WeightNolume:
Date Date WeightNolume:
File
Instrument
Initial Lab Injection Final
Spectrometry
Qualifier
151
18.8
of
680-93535
Chromatography/Mass
(ug/Kg)
76
680-92817
<4100
<2000 <10000 <10000
<20000 Gas <2000 <2000 <2000 <410000 <4100 <2000 <2000 <2000 <2000 <2000 <2000 <2000 <2000 14000
<2000 <2000
<2000 <2000 <2000 <2000 <2000 <2000 <2000 <2000 <2000 <2000 3500 <2000 <2000 <2000
<2000 <2000 <1000000
<2000 <2000 <2000 <2000 <410000 <2000
Moisture:
Batch:
Result by
%
Page
Batch:
Y
Analysis Prep
Compounds
Corrected:
Dry’.Nt
Semivolatile
1827 1534
8270C
HER-DAI-112807
680-32249-30 Solid
ether
8270C 12/1312007 355DB 12/06/2007 5.0
phenethylamine
Inc.
-oxide
phthalate
azobenzene
ID:
phenyl
ID:
Savannah
Hercules
phthalate
phthalate
Total
Sample
Matrix:
alcohol
phthalate
Prepared:
Analyzed:
Sample
methanesulfonate
methanesulfonate
2-Dimethylbenz(a)anthracene
Client:
Client Lab
Client
Method: Preparation: Dilution: Date Date
Analyte
4-Chloroaniline 4-Chlorophenyl 4-Nitroanhline 4-Nitrophenol 4-Nitroquinolirie-1 7,1
Acenaphthylene alpha,alpha-Dimethyl Acetophenone Benzo[a]anthracene Aniline Anthracene Benzo[a]pyrene Benzo[b]fluoranthene Aramite, Berizo[g,h,i]perylene Benzo[kjfluoranthene Benzyl Bis(2-chloroethoxy)methane Bis(2chloroethyl)ether Bis(2-ethylhexyl)
Diallate Chrysene Dibenz(a,h)anthracene Dibenzofuran Diethyl Di-n-butyl Dinoseb p-Dimethylamino Di-n-octyl Ethyl Fluoranthene
Fluorene Hexachlorobutadiene Hexachlorobenzene Hexachloroethane Hexachlorocyclopentadiene Hexachlorophene Hexachloropropene TestAmerica lndeno[1,2,3-cd}pyrene Isophorone Isosafrole
Methapyrilene Methyl
Q
j j Data
T -
680-32249-1
1530
0923
g
mL
uL
Analytical
15.04 .5 1
RL
2000 2000 2000 2000
2000 2000 2000 2000 2000 2000 2000 10000 2000 2000 2000 10000 2000 2000 2000 2000 2000 2000 2000 2000 2000 2000 2000 2000 2000 2000 2000
SemiVolatiles
Number:
Limits
11/28/2007 11129/2007
Job
GC/MS
t4269.d 128 110
110
-110 -
36- 10-112
41 44 36- 43-110
Acceptance
(GC/MS)
ID:
Sampled: Received:
Volume: ID:
WeightNolume:
WeightNolume:
Date
Date
File
Instrument Lab Initial Final Injection
Spectrometry
Qualifier
D
0 0
151
18.8
of
680-93535
Chromatography/Mass
(ug/Kg)
77
680-92817
<2000 <2000 <2000 <2000 <2000 <2000 <2000 <2000 <2000 <2000 <2000 <2000 Gas <2000 <2000 <10000 <2000
<2000 4800 <10000 <2000 3400 <2000 7500 <2000 <2000 <2000 <2000 <2000 <2000 <2000 <2000
52 50 0 0 41 0
Moisture:
Batch:
%Rec
Result
by
%
Page
Batch:
Y
Prep
Analysis
Compounds
Corrected:
WI
Dry
Semivolatile
1827
1534
8270C
HER-DAI-112807
Solid 680-32249-30
12/13/2007 8270C
3550B 5.0 12/06/2007
Inc.
ether
ID:
ID:
diamine
Savannah
phthalate
Hercules
Sample Total
Matrix:
parathion
Prepared:
Analyzed:
Sample
Parathion
benzyl
Client: Lab Client
Client
Preparation: Method: Dilution: Date Date
Analyte
Nitrobenzene Naphthalene N-Nitrosodiethylamine N-Nitrosodi-n-butylamine N-Nitrosodimethylamine N-Nitrosodiphenylamine N-Nitrosomethylethylamine N-Nitrosodi-n-propylamine N-Nitrosomorpholine N-Nitrosopiperidine N-Nitrosopyrrolidine N-Nitro-o-toluidine Pentachlorobenzene Pentachlorophenol Pentachloronitrobenzene
Phenacetin Phenanthrene Phenol p-Phenylene Pyrene Pronamide Surrogate Safrole, Ethyl o,o,o-Triethylphosphorothioate Disulfoton Methyl Phorate Famphur Dimethoate Butyl 2,4,6-Tribromophenol Phenol-d5 2-Fluorobiphenyl bis(chloroisopropyl) 2-Fluorophenol Terphenyl-d14 Nitrobenzene-d5 TestAmerica
O
J j Data
T -
680-32249-1
1550
0923
g
mL
uL
Analytical
15.26 1 .5
RL
2000 2000 2000 2000
2000 2000 2000 2000 2000 2000 2000 2000 2000 2000 2000 10000 2000 2000 2000 2000 2000 2000 2000 2000 2000 2000 10000 2000 2000 2000 2000 2000 2000 10000 2000 10000 2000 2000 10000 2000 4000
2000 2000 2000
SemiVolatiles
Number
11/29/2007 11/2812007
Job
GC/MS
t4270.d
(GCIMS)
ID:
Received:
Sampled:
Volume:
ID:
WeightNolume:
WeightNolume:
Date Date
File
Initial Instrument Lab Injection Final
Spectrometry
Qualifier
151
18.1
of
680-93535
Chromatography/Mass
78 (ug/Kg)
680-92817
<2000 <2000 <2000 <2000 <2000 <2000 <2000 <2000 <2000 <2000 <2000 <2000 <2000 Gas <2000 <2000 <2000 <2000 <2000 <2000 <2000 <10000 <2000 <2000
<2000 <2000 <2000 <2000 <2000 <2000 <2000 <2000 <10000 <2000 <2000 <2000 <2000 <4000 <10000 <2000 <10000 <10000 <2000 <2000 <2000
Moisture:
Batch:
Result
by
%
Page
Batch:
Y
Prep
Analysis
Compounds
Corrected:
Drywt
Semivolatile
1534
1849
8270C
HER-DA2-112807
Solid
680-32249-31
8270C 12/13/2007 12/06/2007 5.0 3550B
ether
Inc.
ID:
phenyl
ID:
Savannah
Hercules
phthalate
Sample
Matrix:
Prepared:
Analyzed:
Sample
Methylphenol
4
,2,4,5-Tetrachlorobenzene ,2,4-Tnchlorobenzene ,2-Dichlorobenzene ,3,5-Trinitrobenzene
,3-Dichlorobenzene ,3-Dinitrobenzene ,4-Naphthoquinone ,4-Dichlorobenzene Client: ,4-Dioxane Client Lab Client
& Method: Dilution: Preparation: Date Date
Analyte
1 1,1-Biphenyl Sulfotepp Acenaphthene Thionazin Pyridine 1 1 1 1 1 1 1 1-Naphthylamine 1
2,3,4,6-Tetrachlorophenol 2,4,5-Trichlorophenol 2,4,6-Trichlorophenol 24-Dichlorophenol 24-Dimethylphenol 2,6-Dichlorophenol 2,4-Dinitrophenol Dimethyl 24-Dinitrotoluene 26-Dinitrotoluene 2-Acetylaminofluorene 2-Chlorophenol 2-Methylnaphthalene 2-Chloronaphthalene 2-Methylphenol 2-Naphthylamine 2-Nitroaniline 2-Nitrophenol 3 2-Picoline TestAmerica 2-Totuidine 33-Dichlorobenzidine 33-Dimethylbenzidine 3-Methylcholanthrene 3-Nitroaniline
4,6-Dinitro-2-methylphenol 4-Aminobiphenyl 4-Bromophenyl 4-Chloro-3-methylphenol
J Data
T -
680-32249-1
1550
0923
g
mL
uL
Analytical
15.26
.5 1
RL 10000
10000 4000 2000 20000
2000 2000 2000
2000 400000 4000 2000 2000 2000 2000 2000 2000 2000 2000 2000 2000 2000 2000 2000 2000 2000 2000 2000 2000 2000 2000
2000 2000 2000 2000 2000 1000000
2000 2000 2000 2000 2000 2000
400000
SemiVolatiles
Number:
11/28/2007 11/29/2007
Job
GC/MS
t4270.d
(GC/MS)
ID:
Sampled: Received:
Volume: ID:
Weight/Volume:
Weight/Volume: Date Date
File
Instrument Initial Lab Injection Final
Spectrometry
Qualifier *
151
18.1
of
680-93535
Chromatography/Mass
(ug/Kg)
79
680-92817
<4000 <2000 <10000 <10000 <20000 <2000 <2000 <2000 <4000 <400000 <2000 <2000 <2000 <2000 Gas <2000 <2000 <2000 <2000 <2000 7900 <2000 <2000 <2000 <2000 <2000 <2000 <2000 <2000 <2000 <2000 <2000 <2000 <2000 <2000 <2000 <2000 <2000 <2000 <1000000 <2000 <2000 <2000 <400000 <2000
Moisture:
Batch:
Result
by
%
Page
Batch:
Y
Prep
Analysis
Compounds
Corrected:
DryWt
Semivolatile
1849
1534
8270C
HER-DA2-112807
Solid 680-32249-31
ether
12/13/2007 8270C 3550B 12/06/2007 5.0
phenethylamine
Inc.
-oxide
phthalate azobenzene
ID: phenyl
ID:
Hercules
phthalate
phthalate
Total
,23-cd]pyrene
Sample
Matrix:
alcohol
phthalate
Prepared:
Analyzed:
methanesulfonate
Sample
methanesulfonate
2-Dimethylbenz(a)anthracene
Client:
Lab Client Client
Dilution: Method: Preparation: Date Date
Analyte
4-Chloroaniline 4-Chiorophenyl 4-Nitroaniline 4-Nitroquinoline-1 4-Nitrophenol 7,1 alpha,alpha-Dimethyl Acenaphthylene Acetophenone Benzo[a]anthracene Benzo[ajpyrene Benzo[b]fluoranthene Aniline Benzo[g,hj]perylene Anthracene Aramite, Benzyl Benzo[k]fluoranthene Bis(2-ethylhexyl) Bis(2-chloroethoxy)methane Bis(2-chloroethyl)ether
Diallate Dibenz(a,h)anthracene Chrysene Dibenzofuran Di-n-butyl Diethyl Dinoseb p-Dimethylamino Di-n-octyl Ethyl Fluoranthene Hexachlorobenzene Fluorene Hexachlorocyclopentadiene Hexachloroethane Hexachlorobutadiene TestAmericaSavannah Hexachloropropene lndeno[1 Hexachlorophene Isophorone Isosafrole
Methapyrilene Methyl
J Data
T -
680-32249-1
1550
0923
g
mL
uL
Analytical
1 15.26
.5
RL
2000 2000 2000 2000 2000 2000 2000 2000 2000 2000 10000 2000 2000 2000 10000 2000 2000 2000 2000 2000 2000 2000 2000 2000 2000 2000 2000 2000 2000 2000 2000
SemiVolatiles
Number:
Limits
11/28/2007 11/29/2007
Job
128 110 110
GC/MS t4270.d - -
10-112
36-
41 36 44-110
43-110
Acceptance
(GCIMS)
ID:
Received: Sampled:
Volume:
ID:
WeightNolume:
WeightNolume:
Date Date
File
Instrument Lab Initial Injection Final
Spectrometry
Qualifier
0 D D
151
18.1
of
680-93535
Chromatography/Mass
80
(uglKg)
680-92817
<2000 <2000 <2000 <2000 <2000 <2000 <2000 <2000 <2000 <2000 <2000 <2000 <2000 <2000 <10000 <2000 Gas <2000 <2000 <2000 <10000 <2000 <2000 <2000 <2000 <2000 29000 <2000 <2000 <2000 <2000 <2000
55 52 0 0 58
0
Moisture:
Batch:
%Rec
Result
by
Page
%
Batch:
Y
Prep
Analysis
Compounds
Corrected:
DryWt
Semivolatile
1849 1534
827CC
HER-DA2-112807
680-32249-31 Solid
12)06/2007 8270C 12/13/2007 3550B 5.0
Inc.
ether
amine
mine
ID:
ID:
Savannah
diamine
phthalate
Hercules
Total
Sample
Matrix:
parathion
Prepared:
Analyzed:
Sample
Parathion
benzyl
Client: Lab Client
Client Preparation: Method: Dilution: Date Date
Analyte
Naphthalene Nitrobenzene N-Nitrosodi-n-butylamine N-Nitrosodiethyla N-Nitrosodimethylamine N-Nitrosodi-n-propylamine N-Nitrosodiphenyl N-Nitrosomethylethylamine N-Nitrosomorpholine N-Nitrosopiperidine N-Nitrosopyrrolidine N-Nitro-o-toluidine Pentachlorobenzene Pentachloronitrobenzene Pentachlorophenol
Phenacetin Phenanthrene Phenol Pronamide Surrogate Pyrene p-Phenylene Safrole, Disulfoton Ethyl o,o,o”-Triethylphosphorothioate Phorate Famphur Methyl 2,4,6-Tribromophenol Dimethoate 2-Fluorobiphenyl Phenol-d5 Butyl 2-Fluorophenol Terphenyl-d14 bis(chloroisopropyl) Nitrobenzene-d5 TestAmerica
O
J ) Analytical Data
Client: Hercules Inc. Job Number: 680-32249-1
Client Sample ID: HER-DAI-112807
Lab Sample ID: 680-32249-30 Date Sampled: 11)28/2007 1530 Client Matrix: Solid % Moisture: 18.8 Date Received: 11)29/2007 0923
8081A_8082 Organochiorine Pesticides & Polychlonnated Biphenyls by Gas Chromatography Method: R 8081A_8082 Analysis Batch: 680-92578 Instrument ID: GC SemiVolatiles - M J Preparation: 3550B Prep Batch: 680-92308 Lab File ID: m103013.d Dilution: 10 InitialWeight/Volume: 15.10 g Date Analyzed: 12103/2007 1316 Final WeightNolume: 5 mL Date Prepared: 11/30)2007 1149 Injection Volume: 2 uL Column ID: PRIMARY
Analyte DryWI Corrected: Y Result (ug/Kg) Qualifier RL Aldrin <21 21 alpha-BHC <21 21 Chlordane (technical) <210 210 Chlorobenzilate <210 210 4,4-DDD <40 40 4,4-DDE <40 40 4,4’-DDT <40 40 delta-BHC 22 21 Dieldrin <40 40
Endosulfan I <21 21 Endosulfan II <40 40 Endosulfan sulfate <40 40 O Endnn <40 40 Endrin aldehyde <40 40 Endrin ketone <40 40 gamma-BHC (Lindane) <21 21 Heptachlor <21 21 Heptachlor epoxide <21 21 lsodnn <40 40 Kepone <2100 2100 Methoxychlor <210 210 Toxaphene <2100 2100
Surrogate %Rec Acceptance Limits DCB Decachlorobiphenyl 0 D 50- 129 Tetrachloro-m-xylene 0 D 26 - 140
TestAmerica Savannah Page 81 of 151 Data
M -
680-32249-1
1530
0923
g
uL mL
Analytical
15.10
5
2 RL
210
Number:
11/28/2007 11/29/2007
SemiVolatiles
Job
PRIMARY
mI03016.d GC
ID:
Sampled: Received:
Volume:
ID:
ID:
Chromatography
WeightNolume:
WeightNolume: Date
Date
File
Gas
Instrument Lab Initial
by Final Injection Column
Qualifier
Biphenyls
151
18.8
of
680-92578
(ug/Kg)
82
Polychlorinated
680-92308
&
<210
Moisture:
Batch:
Result
%
Page
Batch:
Y
Pesticides
Prep
Analysis
Corrected:
DryWt
Organochlorine
1414
1149
HER-DAI-112807
680-32249-30 Solid
8081A_8082
100 3550B
8081A_8082 11/30/2007 12/03/2007
Inc.
ID:
ID:
Savannah
Hercules
Sample
Matrix:
Prepared:
Analyzed:
Sample
Client:
Lab Client
Client
Method: Preparation: Dilution: Date Date
Analyte
beta-BHC
TestAmerica Data M - 680-32249-1 1550 0923 g mL uL
Analytical 15.17 5 RL 2 21 21 210 210 40 21 40 21 40 40 40 40 40 21 40 40 2100 21 21 40 210 2100 Limits Number: 11/29/2007 11/28/2007 SemiVolatiles PRIMARY Job 129 140 GC ml03017.d - 50- 26 Acceptance ID: Received: Sampled: Volume: ID: ID: Chromatography Weight/Volume: Weight/Volume: Date Date File Gas Instrument Lab Initial Final Injection by Column Qualifier D D Biphenyls 151 18.1 of 680-92578 83 (ugiKg) Polychlorinated 680-92308 & <21 <21 <210 <210 <40 370 <40 36 <40 <21 <40 <40 <40 <40 <40 <21 <21 <21 <40 <2100 <210 <2100 0 0 Moisture: %Rec Batch: Result Page % Batch: Y Pesticides Prep Analysis Corrected: DryWt Organochlorine 1149 1434 8082 HER-DA2-112807 Solid 680-32249-31 8081A_8082 10 11/30/2007 8081A 12/03)2007 3550B Inc. ID: (Lindane) ID: Savannah I II sulfate epoxide (technical) Hercules Sample Matrix: aldehyde ketone Prepared: Analyzed: Decachlorobiphenyl Sample Client: Client Lab Client Preparation: Method: Date Dilution: Date Analyte Chlorobenzilate alpha-BHC Surrogate Chlordane Aldrin Dieldrin Endosulfan delta-BHC Endosulfan Endosulfan 4,4’-DDD 4,4-DDE Endrin Endrin DCB 4,4-DDT Endrin Isodrin Heptachlor Heptachlor Tetrachloro-m-xylene gamma-BHC Kepone Methoxychlor Toxaphene TestAmerica
J Data
M -
680-32249-1
1550
0923
g
mL uL
Analytical
15.17
5
2 RL
210
Number
11/28/2007
11)29)2007
SemiVolatiles
Job
PRIMARY
CC
m103019.d
ID:
Received: Sampled:
Volume:
ID:
ID:
Chromatography
WeightNolume:
WeightNolume: Date
Date
File
Gas
Instrument by Initial Lab Final Injection
Column
Qualifier
Biphenyls
151
18.1
of
680-92578
(ug/Kg)
84
Polychlorinated
680-92308
&
<210
Moisture:
Batch:
Result
%
Page
Batch:
Y
Pesticides
Prep
Analysis
Corrected:
DryWt
Organochlorine
1513
1149
8082
HER-DA2-112807
Solid 680-32249-31
8081A_8082
8081A 12/03/2007 100
3550B 11)30/2007
Inc.
ID:
ID:
Savannah
Hercules
Sample
Matrix:
Analyzed: Prepared:
Sample
Client: Client Lab
Client
Method: Preparation: Date Dilution:
Date
Analyte
beta-BHC
TestAmerica
J Data
S -
680-32249-1
1530
0923
g
mL
uL
Analytical
10
30.0 1
10 10 RL 10
Limits
Number:
11/29/2007 11/2812007
SemiVolatiles
Job
PRIMARY
110
GC s108008.d -
58
Acceptance
ID:
Received: Sampled:
Volume: ID:
ID:
WeightNolume:
WeightNolume:
Date Date
File
Instrument Lab Initial Final Injection
Column
GC
Qualifier
by
151
18.8
of
Herbicides
680-93032
(uglKg)
85
680-92620
<10 <10 <10
97
%Rec Moisture:
Batch:
Result
%
Chlorinated
Page
Batch:
Y
Prep
Analysis
8151A
Corrected:
DryWt
12807
1031
1339
HER-DAI-1
Solid 680-32249-30
acid
1.0 12/08/2007 8151A 12/04/2007 8151A
Inc.
ID:
ID:
Savannah
Hercules
Sample
Matrix:
(24,5-TP)
Prepared: Analyzed:
Sample
Client:
Lab Client
Client
Method: Preparation: Dilution: Date Date
Analyte
Surrogate
2,4-Dichlorophenylacetic 2,4,5-T Silvex 2,4-D
TestAmerica
] 9 Data
S - 680-32249-1
1550
0923
g
mL
uL
Analytical
10 30.1 I
10 RL 10 10
Limits
Number:
11/28/2007 11/29/2007
SemiVolatiles
Job
PRIMARY
110
GC
s108009.d -
58
Acceptance
ID:
Received: Sampled:
Volume: ID:
ID:
WeightNolume:
Date WeightNolume: Date
File
Instrument Lab Initial
Injection Final
Column
GC
Qualifier
by
151
18.1
Herbicides
of
680-93032
(ug/Kg)
86
680-92620
<10
<10 <10
72
Moisture:
%Rec
Batch:
Result
%
Chlorinated
Page
Batch:
Y
Prep
Analysis
8151A
Corrected:
DryWt
12807
1051 1339
HER.DA2-1
Solid 680-32249-31
acid
1.0 8151A 8151A 12/08/2007
12/04/2007
Inc.
ID:
ID:
Savannah
Hercules
Sample
Matrix:
(2,45-TP)
Prepared:
Analyzed:
Sample
Client:
Client Lab
Client
Preparation: Method:
Dilution: Date Date
Analyte
Surrogate
2,45-T
Silvex 2,4-Dichiorophenylacetic 2,4-D
TestAmerica
J j 680-32249-1
4
Number
is
Job
compounds
therefore, compounds
compounds
dilution
obtained
obtained
obtained
sample
also
also
D. also
D.
D.
not a
not a
a
not
with
with
original with
were
were
were
secondary analysis;
analysis;
analysis;
concentration;
limits
the
for
limits
for
for
in
limits
flagged
flagged
flagged
spike
range,
control
be
be
be
recoveries
recoveries
recoveries
diluted
diluted control
diluted
control
the
present
matrix
may
may
may
the
applicable.
was
was
spike
spike was the
spike
the
calibration
151
not
QUALIFIERS
analyte
exceeds
dilution
dilution
dilution
than matrix
matrix
extract
are
extract matrix
of
extract
a
exceeds a
a
exceeds or
The or
or
at
at
the
at
the
the
87
LCSD
exceeded
limits
MSD
greater
or
MSD:
or
Page
Description
Result
required. Surrogate
because Surrogate analyzed LCS
Surrogate because REPORTING
analyzed MS MS,
control because
times Surrogate analyzed
DATA
Qualifier
E
D
X
* D
F
D
4
Inc.
VOA
Savannah
VOA
Hercules
VOA
Semi
Section
Semi
Client:
Lab
GC/MS
GC/MS
GC
TestAmerica QUALITY CONTROL RESULTS ]
TestAmerica Savannah
Page 88 of 151 Quality Control Results
Client: Hercules Inc. Job Number: 680-32249-1
QC Association Summary Report Lab Sample ID Client Sample ID Basis Client Matrix Method Prep Batch
GCIMS VOA Analysis Batch:680-92512 LCS 680-9251 2/16 Lab Control Spike T Water 8260B MB 680-92512/18 Method Blank T Water 826DB g 680-32249-2 HER-CMO1-112607 T Water 826DB 680-32249-3 HER-CM02-112607 T Water 826DB
Analysis Batch:680-92536 LCS 680-92536/5 Lab Control Spike T Water 8260B LCSD 680-92536/6 Lab Control Spike Duplicate T Water 8260B MB 680-92536/7 Method Blank T Water 826DB 680-32249-10 HER-MWO5-112707 T Water 826DB 680-32249-13 HER-MWO8-1128D7 T Water 82608 680-32249-25 HER-RS1-112607 T Water 826DB 680-32249-26 HER-RS2-1 12707 T Water 826DB
Analysis Batch:680-92548 LCS 680-92548/5 Lab Control Spike T Solid 826DB LCSD 680-92548/6 Lab Control Spike Duplicate T Solid 826DB MB 680-92548/7 Method Blank T Solid 826DB O 680-32249-31 HER-DA2-1 12807 T Solid 82608
Analysis Batch:680-92567 LCS 680-92567/15 Lab Control Spike T Water 8260B MB 680-92567/16 Method Blank T Water 82608 680-32249-1 HER-CMDO-112607 T Water 826DB 680-32249-4 HER-CMD3-112607 T Water 826DB 68D-32249-4MS Matrix Spike T Water 826DB 680-32249-4MSD Matrix Spike Duplicate T Water 826DB 680-32249-5 HER-CMD4-112607 T Water 826DB 680-32249-6 HER-CMD5-112607 T Water 826DB 680-32249-7 HER-MWD2-112707 T Water 826DB 68D-32249-7MS Matrix Spike T Water 826GB 68D-32249-7MSD Matrix Spike Duplicate T Water 826GB 680-32249-8 HER-MWO3-112707 T Water 826DB
TestAmerica Savannah
Page 89 of 151 Quality Control Results
Client: Hercules Inc. Job Number: 680-32249-1
QC Association Summary Report Lab Sample ID Client Sample ID Basis Client Matrix Method Prep Batch
GCIMS VOA Analysis Batch:680-92630 LCS 680-92630/11 Lab Control Spike T Water 826DB MB 680-92630/12 Method Blank T Water 826DB 680-32249-9 HER-MWO4-112707 T Water 826DB 680-32249-11 HER-MWD6-112707 T Water 8260B 680-32249-12 HER-MWD7-1128D7 T Water 826DB 680-32249-14 HER-MWO9-112807 T Water 826DB 680-32249-15 HER-MW1O-112707 T Water 8260B 680-32249-16 HER-MW11-112707 T Water 826DB 680-32249-17 HER-MW12-112707 T Water 826DB 680-32249-18 HER-MW13-112807 T Water 826DB 680-32249-19 HER-MW14-112807 T Water 826DB 680-32249-20 HER-MW15-112807 T Water 8260B 680-32249-21 HER-MW16-1128D7 T Water 826DB 680-32249-23 HER-MW18-112707 T Water 826DB 680-32249-28 HER-FD1-112707 T Water 826DB
Analysis Batch:680-92648 LCS 680-92648/9 Lab Control Spike T Water 826DB LCSD 680-92648/10 Lab Control Spike Duplicate T Water 82606 MB 680-92648/11 Method Blank T Water 826DB 680-32249-12MS Matrix Spike T Water 826DB 68D-32249-12MSD Matrix Spike Duplicate T Water 8260B 680-32249-18DL HER-MW13-1128D7 T Water 82606 680-32249-22 HER-MW17-112807 T Water 826DB 680-32249-24 HER-MW19-112807 T Water 826DB 680-32249-27 HER-RS3-1 12807 T Water 826DB 680-32249-29 HER-FD2-1 12807 T Water 826DB 680-32249-32TB TRIP BLANK T Water 826DB
Analysis Batch:680-92858 LCS 680-92858/8 Lab Control Spike T Water 826DB MB 680-92858/9 Method Blank T Water 826DB 680-32249-22DL HER-MW17-112807 T Water 826DB
Analysis Batch:680-92984 LCS 680-92984/3 Lab Control Spike T Solid 826DB MB 680-92984/5 Method Blank T Solid 826DB 680-32249-30 HER-DA1-112807 1 Solid 826DB epprt Basis T = Total
TestAmerica Savannah
Page 90 of 151 Results
680-32249-1
Batch
Prep
680-92817
680-92817
680-92817 680-92817
Control
Number:
Job
Quality
Method
3550B 3550B
3550B 3550B 8270C
8270C
827CC
827CC
Matrix
Client
Solid Solid Solid
Solid Solid
Solid
Solid Solid
151
Report
Basis
T T T
T T T
T T
of
91
Page
Spike
Spike
12807
ID
12807
Blank
Blank
Control
Control
Sample
Lab Method HER-DA1-112807 HER-DA2-1
Lab Method HER-DA1-112807
HEl-DA2-1
Client
Summary
Inc.
VOA
ID
680-92817
Savannah
Hercules
Batch:680-93126
Batch:680-93535
Semi
Basis
Batch:
Association
Sample
680-92817/7-A
680-9281717-A
680-92817/6-A
680-92817/6-A
Total =
Client:
QC Lab
Prep GCIMS
Analysis
Analysis Report
T LCS MB
680-32249-30 680-32249-31 LCS MB
680-32249-30
680-32249-31
TestAmerica
J Results
680-32249-1
Batch
Prep
680-92308 680-92308 680-92308 680-92308 680-92308 680-92308
680-92620 680-92620 680-92620 680-92620 680-92620 680-92620
Control
Number:
Job
Quality
1A_8082
Method
355DB 3550B 355DB 35508 3550B 35508 8081A_8082 8081A_8082 8081A_8082 808 8081A_8082 8081A_8082
8151A 8151A 8151A 8151A 8151A 8151A
8151A 8151A 8151A 8151A 8151A 8151A
Matrix
Client
Solid Solid Solid Solid Solid Solid Solid Solid Solid Solid Solid
Solid Solid
Solid Solid Solid Solid Solid
Solid Solid Solid Solid Solid
Solid
151
Basis Report
T T T T T T
T T T T T T
T T T T T T
T T T T T T
of
92
Page
Duplicate
Duplicate
Duplicate
Spike
Duplicate
Spike
12807 Spike
ID
Spike
12807
Blank
Blank
Blank
Blank
Spike Spike
Spike Spike
Spike Spike
Spike Spike
Control
Control
Control
Control
Sample
Lab
HER-DA1-112807 Method HER-DA2-1 Matrix Matrix
Lab Method HER-DA1-112807 Matrix Matrix HER-DA2-112807 Lab
Method HER-DA1-112807 HER-DA2-1 Matrix Matrix Lab HER-DA1-112807 HER-DA2-112807 Method Matrix
Matrix
Client
Summary
Inc.
0-A
ID
680-92308
680-92620
Savannah
VOA
Hercules
Batch:680-92578
Is
Batch:680-93032
Baa
Batch:
Association Batch:
Sample
680-92308/10-A
680-92308/1
Semi
680-92620/4-A
680-92620/4-A
680-92308/6-A
680-92308/6-A
680-92620/3-A
680-92620/3-A
Total =
Client:
QC Lab GC
Prep
Analysis
Prep
LCS
MB 680-32249-30 Analysis 680-32249-3OMS 680-32249-3OMSD 680-32249-31 LCS
MB 680-32249-30 680-32249-3OMS Report 680-32249-3OMSD T 680-32249-31 LCS MB
680-32249-31 680-32249-30 680-32249-31MSD LCS 680-32249-31MS
MB 680-32249-30 TestAmerica 680-32249-31MS 680-32249-31 680-32249-3IMSD
O
0
j Results
680-32249-1
Control
Number:
Job
Quality
OX
Limits
72
TOL 92 75
99
100
100
%Rec
151
65-124 65-124 65-132
of
OX
87
98
89
Acceptance
102 107
102
%Rec
DBFM
93
OX
82 BFB Page 90
73
98
94
97
%Rec
GC/MS
by
ID
12807
12807
Sample
Report
Compounds
Client
HER-DA1-1 HER-DA2-1
(Surr)
Inc.
Organic
Recovery
Solid
ID
Dibromofluoromethane
Savannah
Hercules
4-Bromofluorobenzene Toluene-d8
Volatile
=
Matrix:
680-92548/6
680-92548/5
680-92984/3
Sample
680-92548/7 680-92984/5
BFB Surrogate DBFM
TOL
Client:
Surrogate
8260B
Client Lab
680-32249-30 680-32249-31 MB MB LCS LCS LCSD
TestAmerica