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A Simple Spectrophotometric Method for the Determination Of
J Clin Pathol: first published as 10.1136/jcp.14.2.202 on 1 March 1961. Downloaded from 202 Technical methods usual laboratory filters may give falsely increased values.) Of the clear and colourless filtrate 10 ml. is pipetted into A a 25 ml. measuring flask and 10 ml. reagent (3) added. simple spectrophotometric After mixing dilute with distilled water to the mark and method for the determination of renew mixing. After 10 minutes the mixture is ready for reading. The colour is stable, according to Watt and urea in blood and urine Chrisp, for 11 days. READING T. K. WITH, TOVE DREYER PETERSEN, AND BIRGIT PETERSEN From the Central Laboratory, Svend- The reactions are read in a spectrophotometer at 420 nm. borg County Hospital, Denmark with a blank prepared in the same way as the reaction mixture but with 3 ml. of distilled water instead of 3 ml. of blood. The urea standard (reagent 4) is treated in the Several methods for urea in determining blood and urine same way as the blood. Cuvettes of 1 cm. thickness are are in use in clinical laboratories, but none is ideal in suitable. mass routine The analysis. spectrophotometric method If p, s, and b are the extinctions of the the based on a modified Ehrlich sample, reagent proposed by Watt standard, and the blank respectively, the urea concen- and Chrisp (1954) for pure solutions is therefore of tration is interest because it can be modified for use in mass clinical analyses of blood and urine. Brown (1959) has l00(p-b)/(s-b) mg./100 ml. -
I. Direct Titration of Sulfate, II. High Precision Spectrophotometric Analysis Max Quentin Freeland Iowa State College
Iowa State University Capstones, Theses and Retrospective Theses and Dissertations Dissertations 1955 I. Direct titration of sulfate, II. High precision spectrophotometric analysis Max Quentin Freeland Iowa State College Follow this and additional works at: https://lib.dr.iastate.edu/rtd Part of the Analytical Chemistry Commons Recommended Citation Freeland, Max Quentin, "I. Direct titration of sulfate, II. High precision spectrophotometric analysis" (1955). Retrospective Theses and Dissertations. 14746. https://lib.dr.iastate.edu/rtd/14746 This Dissertation is brought to you for free and open access by the Iowa State University Capstones, Theses and Dissertations at Iowa State University Digital Repository. It has been accepted for inclusion in Retrospective Theses and Dissertations by an authorized administrator of Iowa State University Digital Repository. For more information, please contact [email protected]. INFORMATION TO USERS This manuscript has been reproduced from the microfilm master. UMi films the text directly from the original or copy submitted. Thus, some thesis and dissertation copies are in typewriter face, while others may be from any type of computer printer. The quality of this reproduction is dependent upon the quality of the copy submitted. Broken or indistinct print, colored or poor quality illustrations and photographs, print bleedthrough, substandard margins, and improper alignment can adversely affect reproduction. In the unlikely event that the author did not send UMI a complete manuscript and there are missing pages, these will be noted. Also, if unauthorized copyright material had to be removed, a note will indicate the deletion. Oversize materials (e.g., maps, drawings, charts) are reproduced by sectioning the original, beginning at the upper left-hand comer and continuing from left to right in equal sections with small overlaps. -
SPECIAL SCIENTIFIC REPORT-FISHERIES Na 349
349 CHEMICAL ANALYSES OF MARINE AND ESTUARINE WATERS USED BY THE GALVESTON BIOLOGICAL LABORATORY SPECIAL SCIENTIFIC REPORT-FISHERIES Na 349 UNITED STATES DEPARTMENT OF THE INTERIOR FISH AND WILDLIFE SERVICE United States Department of the Interior, Fred A. Seaton, Secretary Fish and Wildlife Service, Arnie J. Suomela, Commissioner Bureau of Commercial Fisheries, Donald L, McKernan, Director CHEMICAL ANALYSES OF MARINE AND ESTUARINE WATERS USED BY THE GALVESTON BIOLOGICAL LABORATORY by Kenneth T. Marvin, Zoula P. Zein-Eldin, Billie Z. May and Larence M. Lansford Chemists Galveston, Texas United States Fish and Wildlife Service Special Scientific Report— Fisheries No. 349 Washington, D. C. June 1960 CONTENTS Introduction 1 Sample treatment prior to analysis 1 Sample storage containers 2 Analytical methods 2 Standard samples 2 Phosphate 3 Inorganic only 3 Total and inorganic 3 Total only 4 Nitrate-nitrite 5 Nitrite 5 Salinity 6 Copper 6 Sulfide 7 Oxygen 7 Total carbon dioxide 8 Ammonia 10 Chlorophyll 10 "Carbohydrates" 11 "Protein" (tyrosine equivalent) 12 Washing procedure for all analytical glassware 12 Literature cited 13 111 CHEMICAL AMLYSES OF MAP.INE AND ESTOARIKE mTERS USED BY TBE GALVESTON BIOLOGICAL lABORATORY by Kenneth T. Marvin, Zoula P. Zein-Eldin, Billie Z. May and Larence M. Lansford ABSTRACT This paper describes the chemical techniques and procedures used hy the Biological lahoratory of the U. S. Bureau of Commercial Jlsherles, Galveston^ Texas, for analyzing samples Involved In the chemical and hlo- logical survey of the marine and estuarlne waters of the Gulf of Mexico and also In the many laboratory and field studies and experiments that have heen made pertaining to the red tide investigation. -
Laboratory Equipment Used in Filtration
KNOW YOUR LAB EQUIPMENTS Test tube A test tube, also known as a sample tube, is a common piece of laboratory glassware consisting of a finger-like length of glass or clear plastic tubing, open at the top and closed at the bottom. Beakers Beakers are used as containers. They are available in a variety of sizes. Although they often possess volume markings, these are only rough estimates of the liquid volume. The markings are not necessarily accurate. Erlenmeyer flask Erlenmeyer flasks are often used as reaction vessels, particularly in titrations. As with beakers, the volume markings should not be considered accurate. Volumetric flask Volumetric flasks are used to measure and store solutions with a high degree of accuracy. These flasks generally possess a marking near the top that indicates the level at which the volume of the liquid is equal to the volume written on the outside of the flask. These devices are often used when solutions containing dissolved solids of known concentration are needed. Graduated cylinder Graduated cylinders are used to transfer liquids with a moderate degree of accuracy. Pipette Pipettes are used for transferring liquids with a fixed volume and quantity of liquid must be known to a high degree of accuracy. Graduated pipette These Pipettes are calibrated in the factory to release the desired quantity of liquid. Disposable pipette Disposable transfer. These Pipettes are made of plastic and are useful for transferring liquids dropwise. Burette Burettes are devices used typically in analytical, quantitative chemistry applications for measuring liquid solution. Differing from a pipette since the sample quantity delivered is changeable, graduated Burettes are used heavily in titration experiments. -
BLAUBRAND® Volumetric Instruments and Density Bottles
BLAUBRAND® Volumetric Instruments and Density Bottles Testing Instructions (SOP) March 2015 1. Introduction The standard DIN EN ISO 4787 describes both the design and the testing of the volumetric instruments of glass. The following Testing Instructions describe how to apply the ISO standard in practice. We recommend a testing every 1-3 years. The interval depends on the using of aggressive media and the cleaning procedure. These Instructions may also be used as a basis for the supervision of testing devices to DIN EN ISO 9001, DIN EN ISO 10012 and DIN EN ISO/IEC 17025. The test of the Density Bottles was effected on the basis of DIN EN ISO 4787. Meniscus adjustment with BLAUBRAND® Volumetric Instruments Meniscus adjustment Meniscus adjustment with ring mark with Schellbach stripe Read at the lowest point of the meniscus. Read at the point where the two arrows touch. Meniscus adjustment reflexion of liquid surface meniscus ring mark dark paper (p.e. black, blue) 2 2. Preparation for testing 2. Clear identification of the volumetric instrument to be tested Batch number, individual serial number, trademark, nominal volume and tolerances are directly printed ⇒ The test starts with a clear identification of the on every BLAUBRAND volumetric instruments. volumetric instrument in the test record. 2.1 Copy Test Record (see page 13) 2.2 Serial number/Identification number ⇒ Enter into Test Record All BLAUBRAND® volumetric instruments always carry a batch number, e.g., 13.04, or an individual serial number in the case of individual certificates, e.g., 13.040371 (year of production 2013, Batch No. -
OHAUS Balances Navigator Range
Catalogue OHAUS Balances Navigator Range Has Landed Page 120 Parafilm M New Frontier Up to 60% Off Page 4 Centrifuges German Made Page 148 Bollé Safety Schott-DURAN Rush Plus Small Has Arrived Youtility B ottles Page 77 A New Age SAVINGS Up to 70% off major brands Bacto Laboratories Nov 2020 BactoIssue Laboratories 15.0 Pty Ltd - Phone (02) 9823-9000Proudly - Email [email protected] Supplying - (prices Science excl GST) Since 1966 1 Contents A Centrifuge 145 Flask, Volumetric Glass 17 Alcohol Wipes 55 Centrifuge Tube, Glass 24 Flask, Volumetric Plastic 29 Analytical Balance 117 Centrifuge Tube, Plastic 44 Forceps 88 Aspirator Bottle, Plastic 42 Chemicals 67 Forceps, Artery 92 Autoclave Indicators 59 Clamps, Bosshead 96 Fridge Thermometers 102 Autoclave Tape 59 Clamps, Burettes 97 Funnel, Glass 15 Autoclave Waste Bags 61 Clamps, Retort 96 Funnel, Plastic 30 Clinical Centrifuge 145 G - H B Coats, Laboratory 74 Gloves, Examination 72 Bacticinerator 82 Cold Bricks 69 Gloves, Safety 71 Bags, Waste 61 Colony Counter 81 Gowns 75 Balance, Moisture 119 Conductivity Meter 109 Hand Wash, Alcohol 55 Balances 116 Conical Measure, Plastic 27 Hand Wash, Cleanser 56 Batteries 102 Contaminated Waste Bags 62 Hand Wash, Sanitiser 55 Beaker, Glass 11 Coplin Jar 53 Hockey Stick 50 Beaker, Plastic 27 Corrosive Cabinets 85 Hotplate 124 Bench Roll 58 Cover Slips, Glass 52 Hotplate Stirrer 124 Biju McCartney Bottle 25 Cryo Vial, Plastic 37 Hygrometers 102 Bins, Broken Glass 61 Culture Media 50 I Bins, Chemotherapy 65 Culture Tube, Glass 24 Incubator 138 Bins, -
Signature Redacted Department of Metallurgy Gau, R E Da Signature of Professor in Charge of Research
THERMODYNAMIC PROPERTIES OF THE GROUP VIa SULFIDES: CrS, Mo2 S3 AND WS2 by JOHN PATRICK HAGER B. S., Montana School of Mines (1958) M. S. , School of Mines and Metallurgy University of Missouri (1960) Submitted in Partial Fulfillment of the Requirements for the Degree of DOCTOR OF SCIENCE at the MASSACHUSETTS INSTITUTE OF TECHNOLOGY August, 1969 Signature of Author Signature redacted Department of Metallurgy gau, r e da Signature of Professor in Charge of Research Signature of Chairman of Departmental Committee Graduate Research nchives Signature redacted INST. 7 DEC 2 1969 4IBRARIES -~ U ii THERMODYNAMIC PROPERTIES OF THE GROUP VIa SULFIDES: CrS, Mo 2S 3 and WS 2 by John Patrick Hager Submitted to the Department of Metallurgy on August 18, 1969, in partial fulfillment of the requirements for the degree of Doctor of Science. ABSTRACT The thermodynamic properties of the metal-saturated phase of the Group VIa sulfides have been determined through a study of the effect of gas composition on the sulfidizing action of (H2S g) + H 2 (g) ) mixtures passed over heated metal samples. The following equations for the standard free energy of formation of CrS (c) ' Mo2S3(c) and WS2(c) were obtained: AFCc) ( 250) = -48,190 ( 760) + 13.27( 0.52)T; cal/l/2 g-mole S2(g) (1375-1570 0 K) AF 0 ( 220) = -41,730( 890) + 17.39( 0.59)1R; cal/l/2 g-mole S2(g) 102S3 (c)2(g (1365-1610 0 K) AF ( 220) = -40,110( 920) + 18.64( 0.63)T; cal/l/2 g-mole S WS 2 (c) 2(g) (1370-15650K) An additional study of the thermodynamic properties of Cu2S ) pro- vided a means of evaluating the experimental technique. -
Laboratory Supplies and Equipment
Laboratory Supplies and Equipment Beakers: 9 - 12 • Beakers with Handles • Printed Square Ratio Beakers • Griffin Style Molded Beakers • Tapered PP, PMP & PTFE Beakers • Heatable PTFE Beakers Bottles: 17 - 32 • Plastic Laboratory Bottles • Rectangular & Square Bottles Heatable PTFE Beakers Page 12 • Tamper Evident Plastic Bottles • Concertina Collapsible Bottle • Plastic Dispensing Bottles NEW Straight-Side Containers • Plastic Wash Bottles PETE with White PP Closures • PTFE Bottle Pourers Page 39 Containers: 38 - 42 • Screw Cap Plastic Jars & Containers • Snap Cap Plastic Jars & Containers • Hinged Lid Plastic Containers • Dispensing Plastic Containers • Graduated Plastic Containers • Disposable Plastic Containers Cylinders: 45 - 48 • Clear Plastic Cylinder, PMP • Translucent Plastic Cylinder, PP • Short Form Plastic Cylinder, PP • Four Liter Plastic Cylinder, PP NEW Polycarbonate Graduated Bottles with PP Closures Page 21 • Certified Plastic Cylinder, PMP • Hydrometer Jar, PP • Conical Shape Plastic Cylinder, PP Disposal Boxes: 54 - 55 • Bio-bin Waste Disposal Containers • Glass Disposal Boxes • Burn-upTM Bins • Plastic Recycling Boxes • Non-Hazardous Disposal Boxes Printed Cylinders Page 47 Drying Racks: 55 - 56 • Kartell Plastic Drying Rack, High Impact PS • Dynalon Mega-Peg Plastic Drying Rack • Azlon Epoxy Coated Drying Rack • Plastic Draining Baskets • Custom Size Drying Racks Available Burn-upTM Bins Page 54 Dynalon® Labware Table of Contents and Introduction ® Dynalon Labware, a leading wholesaler of plastic lab supplies throughout -
Accuracy in Volume Measurements
Activity 1: Accuracy in volume measurements Requirements ● 50 mL burette ● Water ● Burette clamp and stand ● 100 mL graduated cylinder ● Funnel ● 100 mL beaker Health and safety, and outline instructions 1. Set up a burette on a stand assembly (see Figure 1). Figure 1 2. Fill the empty burette with water. Make sure the meniscus of the water in the burette rests on the 0.00 mL line at the top of the burette (see Figure 2). 48 48 48 48 35 35 35 35 49 49 49 49 36 36 36 36 50 50 50 50 0 0 0 0 37 37 37 37 1 1 1 1 38 38 38 38 2 2 2 2 39 39 39 39 3 3 3 3 40 40 40 40 0 0 4 0 4 0 4 4 41 41 41 41 1 1 1 1 2 2 5 2 5 2 5 5 42 42 42 42 3 3 3 3 4 4 6 4 6 4 6 6 43 43 43 43 5 5 5 5 6 6 7 6 7 6 7 7 44 44 44 44 7 7 7 7 8 8 8 8 8 8 8 8 45 45 45 45 9 9 9 9 10 10 9 10 9 10 9 9 46 46 46 46 Figure 2 Closed ClosedClosedClosedClosedClosedOpenClosedOpenClosedClosedOpenClosedOpen Closed Closed 3. Place a 100 mL graduated cylinder beneath the tip of the burette. Open the stopcock and slowly release about 40 mL of water from the burette into the graduated cylinder. Record the exact volume of water dispensed from the burette in the appropriate column of the results table. -
Chemistry Lab Equipment ID Wksht
Chemistry Lab Equipment ID Activity CLASS SET- Do NOT take! Directions: A number of items you will be using in the laboratory are shown below. Use the word bank to correctly identify the lab equipment. Part One: 14. 1. 2. 13. 12. 3. 11. 100ml \ J' 10. ! i 4. 5. 8. t t 6. 7. 9. WORD BANK: graduated cylinder, lab stand, eye dropper/pipette, beaker, triple beam balance, Bunsen burner, goggles, tongs, funnel, striker, ring stand, Erlenmeyer flask, lab coat, test tube CLASS SET- Do NOT take! Available online if you need to finish Chemistry Lab Equipment ID Activity CLASS SET- Do NOT take! Part Two: Directions: Match the correct equipment pictured on the other side to the tasks asked for below. Obj,ect Nlam,e Used For Us,ed to pi,ck up or ho Id hot olbj,ects 1. Pmtects th,e ey,es from flying objects or chemicalll spllashes 2. A wiide-m,outhed container used to transport, heat or store 3. substances A small gll'ass ,container us,ed to view ,chemical! readmns 4. or to heat small amounts ,of a substance A device to m,easure the mass or "mass ,out" and obj:ed or 5. substance. Pmtects the scientist and the sd enti1st's clotlhes fiiom 6. haza~dous or hot ,chemicals Us,ed to dispense a v,ery small amount of a lli:quiid 7. Us,ed to rght a Bunsen burner 8. Attaches to a lalb stand and used to hold a va1riety of llab 9. equiip,ment Us,ed to m,easure vollume v,e1ry prec.lisely 10. -
Toxcity Tests for Freshwater Organisms
DFO - Libra y MPO Biblio hèque III II I 11 1111 1204304311 1111 II Canadian Special Publication of Fisheries and Aquatic Sciences 44 einellme ---.211151m.yeee - 7,11r,r1 ft Perielin e—N Edited by E. Scherer QL 626 C314 no.44 c.2 1979 Government of Canada Gouvernement du Canada Fisheries and Oceans Pêches et Océans CANADIAN SPECIAL PUBLICATION OF FISHERIES AND AQUATIC SCIENCES 44 TOXICITY TESTS FOR FRESHWATER ORGANISMS Edited by E. SCHERER Department of Fisheries and Oceans Freshwater Institute Winnipeg, Manitoba R3T 2N6 DEPARTMENT OF FISHERIES AND OCEANS WINNIPEG, MANITOBA 1979 In addition to the Canadian Special Publications of Fisheries and Aquatic Sciences (formerly Miscellaneous Special Publications), the Department of Fisheries and Oceans publishes the Canadian Journal of Fisheries and Aquatic Sciences (formerly the Journal of the Fisheries Research Board of Canada) in annual volumes of monthly issues,and a Bulletin series. These publications are for sale from the Canadian Government Publishing Centre, Supply and Services Canada, Hull, Quebec, Canada KlA 059. Remittance must be made in advance, payable in Canadian funds, to the order of the Receiver General for Canada. THIS PUBLICATION IS AVAILABLE FREE FROM THE FRESHWATER INSTITUTE ED Minister of Supply and Services Canada 1979 Cat. No. Es 41-31/44 ISSN 0706-6481 Correct citation for this publication: Scherer, E. (ed.) 1979. Toxicity tests for freshwater organisms. Can. Spec. Publ. Fish. Aquat. Sci. 44: 194 p. Cover design by Don i A. Taite CONTENTS Page Preface Acknowledgements ix Abstract Résumé DE MARCH, B.G.E.: Reproduction and growth impairment tests with the amphipod Hyalella azteca . -
Health Sciences Program Facilities and Equipment Guide April 1, 2021
New York State Education Department Career and Technical Education Health Sciences Program Facilities and Equipment Guide April 1, 2021 FOREWORD The basic goals of career and technical education (CTE) stress broad, transferable skills that focus on problem solving and decision making, while maintaining traditional elements of hands-on learning, connections with business and industry, and preparation for post- secondary education or employment. Successful career and technical education programs depend on facilities and equipment related to that which is currently used in business and industry. Consideration should be given to new and emerging technologies when planning and delivering high quality programs. Facilities and equipment are needed that will assist in teaching both broad transferable skills and required industry specific competencies to best prepare students for employment or pursuit of further education in health sciences careers. The following pages present recommendations concerning the type of equipment and facilities that will support instruction in Health Sciences Education programs. 2 Table of Contents Page Introduction............................................................................................................................................ 4 Health Sciences Education Core .......................................................................................................... 5 Dental Chairside Assisting ...................................................................................................................