Process for Purification of Ethylene Compound Having Fluorine-Containing Organic Group
Office europeen des brevets (fi) Publication number : 0 506 374 A1 @ EUROPEAN PATENT APPLICATION @ Application number: 92302586.0 @ Int. CI.5: C07C 17/38, C07C 21/18 (g) Date of filing : 25.03.92 (30) Priority : 26.03.91 JP 86090/91 (72) Inventor : Kishita, Hirofumi 3-19-1, Isobe, Annaka-shi Gunma-ken (JP) (43) Date of publication of application : Inventor : Sato, Shinichi 30.09.92 Bulletin 92/40 3-5-5, Isobe, Annaka-shi Gunma-ken (JP) Inventor : Fujii, Hideki (84) Designated Contracting States : 3-12-37, Isobe, Annaka-shi DE FR GB Gunma-ken (JP) Inventor : Matsuda, Takashi 791 ~4 YdndSG Anri3k3~shi @ Applicant : SHIN-ETSU CHEMICAL CO., LTD. Gunma-ken (JP) 6-1, Ohtemachi 2-chome Chiyoda-ku Tokyo (JP) @) Representative : Votier, Sidney David et al CARPMAELS & RANSFORD 43, Bloomsbury Square London WC1A 2RA (GB) (54) Process for purification of ethylene compound having fluorine-containing organic group. (57) A process for purifying an ethylene compound having a fluorine-containing organic group (fluorine- containing ethylene compound) by mixing the fluorine-containing ethylene compound with an alkali metal or alkaline earth metal reducing agent, and subjecting the resulting mixture to irradiation with ultraviolet radiation, followed by washing with water. The purification process ensures effective removal of iodides which are sources of molecular iodine, from the fluorine-containing ethylene compound. < h- CO CO o 10 o Q_ LU Jouve, 18, rue Saint-Denis, 75001 PARIS EP 0 506 374 A1 BACKGROUND OF THE INVENTION 1. Field of the Invention 5 The present invention relates to a process for purifying an ethylene compound having a fluorine-containing organic group, and more particularly to a purification process by which iodine contained as impurity in an ethylene compound having a fluorine-containing organic group can be removed effectively.
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