Sample Collection Information Document for Pathogens Companion to Selected Analytical Methods for Environmental Remediation and Recovery (SAM) 2017
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EPA/600/R-17/374 September 2017 www.epa.gov/homeland-security-research Sample Collection Information Document for Pathogens Companion to Selected Analytical Methods for Environmental Remediation and Recovery (SAM) 2017 Office of Research and Development SCIENCEHomeland Security Research Program This page left intentionally blank EPA/600/R-17/374 September 2017 Sample Collection Information Document for Pathogens Companion to Selected Analytical Methods for Environmental Remediation and Recovery (SAM) 2017 by Sandip Chattopadhyay, Ph.D. Threat and Consequence Assessment Division National Homeland Security Research Center Cincinnati, OH 45268 U.S. Environmental Protection Agency Office of Research and Development Homeland Security Research Program Cincinnati, OH 45268 Disclaimer The U.S. Environmental Protection Agency (EPA) through its Office of Research and Development funded and managed the research described herein. It has been subjected to the Agency’s review and has been approved for publication. Note that approval does not signify that the contents necessarily reflect the views of the Agency. Any mention of trade names, products, or services does not imply an endorsement by the U.S. Government or EPA. The EPA does not endorse any commercial products, services, or enterprises. Questions concerning this document or its application should be addressed to: Sandip Chattopadhyay, Ph.D. National Homeland Security Research Center Office of Research and Development U.S. Environmental Protection Agency 26 W. Martin Luther King Drive, MS NG16 Cincinnati, OH 45268 Phone: 513-569-7549 Fax: 513-487-2555 E-mail: [email protected] ii Table of Contents DISCLAIMER ................................................................................................................................................ II LIST OF TABLES ........................................................................................................................................ IV LIST OF ATTACHMENTS ........................................................................................................................... IV ACRONYMS AND ABBREVIATIONS ......................................................................................................... V ACKNOWLEDGEMENTS ........................................................................................................................... VII 1.0 BACKGROUND .................................................................................................................................... 1 2.0 SCOPE AND APPLICATION ............................................................................................................... 1 2.1 SAMPLE COLLECTION INFORMATION TABLES ...................................................................................... 3 2.2 DOCUMENT DEVELOPMENT ................................................................................................................. 3 2.3 LIMITATIONS ...................................................................................................................................... 4 3.0 HEALTH AND SAFETY CONSIDERATIONS ...................................................................................... 5 3.1 HEALTH AND SAFETY PLANS .............................................................................................................. 5 3.2 PERSONAL PROTECTIVE EQUIPMENT .................................................................................................. 5 3.3 TRAINING ........................................................................................................................................... 5 4.0 PREPARATION FOR SAMPLE COLLECTION ................................................................................... 6 4.1 FIELD SAMPLING EQUIPMENT AND SUPPLIES ....................................................................................... 6 4.2 FIELD DATA DOCUMENTATION ............................................................................................................ 6 4.3 FIELD SCREENING .............................................................................................................................. 7 4.4 QUALITY ASSURANCE/QUALITY CONTROL .......................................................................................... 7 5.0 SAMPLE HANDLING ........................................................................................................................... 9 6.0 SAMPLE ACCEPTANCE ................................................................................................................... 10 7.0 DEFINITIONS ..................................................................................................................................... 11 8.0 LABORATORY SUPPORT ................................................................................................................ 11 8.1 DEFINING ANALYTICAL SUPPORT REQUIREMENTS: CAPABILITIES AND CAPACITY ............................... 11 8.2 ESTABLISHING ANALYTICAL SUPPORT NETWORKS ............................................................................ 12 8.3 COORDINATING WITH ANALYTICAL SUPPORT NETWORKS ................................................................... 13 8.4 LABORATORY NETWORKS AND ASSOCIATIONS .................................................................................. 13 9.0 TOOLS AND DATABASES ............................................................................................................... 14 10.0 ADDITIONAL RESOURCES .............................................................................................................. 16 iii List of Tables Table 1. Pathogens and Media Addressed in this Sample Collection Information Document .... 2 Table 2. Key Laboratory Networks and Associations................................................................13 Table 3. Representative Tools and Databases .........................................................................15 List of Attachments Attachment A: Sample Collection Information for the Environmental Media (Soil, Surface, Liquid, and Aerosol) Attachment B-1: Sample Collection Information for Pathogens (Bacteria, Viruses, Protozoa, and Helminths) in Solids (Soil, Powder) Attachment B-2: Sample Collection Information for Pathogens (Bacteria, Viruses, Protozoa, and Helminths) in Surfaces (Swab, Wipe, Dust Socks) Attachment B-3: Sample Collection Information for Pathogens (Bacteria, Viruses, Protozoa, and Helminths) in Liquids (Water and Wastewater) Attachment B-4: Sample Collection Information for Pathogens (Bacteria, Viruses, Protozoa, and Helminths) in Aerosols Attachment C: Holding Time, Packaging Requirements, and Shipping Label of Sample iv Acronyms and Abbreviations AAVLD American Association of Veterinary Laboratory Diagnosticians AOAC Association of Official Analytical Chemists APHIS Animal and Plant Health Inspection Service APHL Association of Public Health Laboratories ASM American Society for Microbiology BSL biosafety level CBR chemical, biological, and radiological CDC Centers for Disease Control and Prevention CFR Code of Federal Regulations Ch. Chapter COC chain-of-custody d50 cut-off sizes correspond to 50% particle collection efficiency mark DGR Dangerous Goods Regulations DHS Department of Homeland Security (U.S.) DOL Department of Labor (U.S.) DOT Department of Transportation (U.S.) DQO data quality objectives DWRPTB Drinking Water Utility Response Protocol Toolbox EMAC Emergency Management Assistance Compact EOC EPA Emergency Operations Center EPA U.S. Environmental Protection Agency ERLN EPA's Environmental Response Laboratory Network FBI Federal Bureau of Investigation FDA Food and Drug Administration FERN Food Emergency Response Network g gram(s) GPS Global Positioning System HASP health and safety plan HCV Hepatitis C Virus HEV Hepatitis E virus HFV Hemorrhagic Fever Viruses HSRP Homeland Security Research Program IATA International Air Transportation Association ICLN Integrated Consortium of Laboratory Networks ISO International Organization for Standardization L liter Lab Compendium Compendium of Environmental Testing Laboratories LRN Laboratory Response Network MCE mixed cellulose ester mL Milliliter MS/MSD Matrix Spike/Matrix Spike Duplicates NAHLN National Animal Health Laboratory Network NEMI National Environmental Methods Index NHSRC National Homeland Security Research Center NIFA National Institute of Food and Agriculture NIOSH National Institute for Occupational Safety and Health NIST National Institute of Standards and Technology °C degrees Celsius OSHA Occupational Safety and Health Administration PPE personal protective equipment psi Pound-force per square inch v PTFE Polytetrafluoroethylene (Teflon®) QA quality assurance QC quality control SAM Selected Analytical Methods for Environmental Restoration Following Homeland Security Events SCID sample collection information document spp. species UN United Nations URL uniform resource locator USAMRIID United States Army Medical Research Institute of Infectious Diseases USGS United States Geological Survey VCSB voluntary consensus standards body WCIT Water Contaminant Information Tool WLA Water Laboratory Alliance WWRPTB Wastewater Utility Response Protocol Toolbox vi Acknowledgements The following individuals and organization have been acknowledged for their contributions towards the development and/or review of this document. United States Environmental Protection Agency (EPA) Office of Research and Development, National