North River Wastewater Treatment Plant Permit Renewal Documentation

Attachment A-1 TABLE 1-7 NYCDEP NORTH RIVER WWTP AIR TITLE V COMPLIANCE EMISSION TEST

SUMMARY OF TURGl EMISSION TEST RESULTS (4) FEBRUARY 2017

Parameter Av~. ofTrinlicate Oil-Fired Test Runs

Source Oneratin~ Data: ( I ) Load, KW 900.0 Heat Input Rate, MMBtu/hr 29.94

Exhaust Stack Conditions: Temo., °F 548.1 Vol. Flow Rate: wacfm 67,939.3 dscfm 34,450.7 0 2, o/o vd 18.0 CO2, ¾vd 2.1 H2O, %v 4.4

Emission Rates: (3) PM lb/hr 0.696 lb/MMBtu 0.0226 so,m DDffi vd 0.2 DDm,d (a) \ 5% 0 2 0.4 lb/hr 0.060 lb/MMbtu 0.0020 NO, {2} DDffi vd 59.1 DDffi vd (a) 15% 02 123.5 lb/hr 14.37 lb/MMBtu 0.4801 co (2) DDITI,d 14.7 oomvd (a) 15% 02 30.7 lb/hr 2.174 lb/MMBtu 0.0725

(I) Based on WWTP operating data. (2) lb/hr emissions based on EPA RM 19 volumetric flow rate determinations; Avg. of33,922 dscfm. (3) lb/MM Btu emission rates calculated based on a Fuel "F" Factor of 9,190 dscf/MMBtu@ 0% 0 2. (4) Avg. of triplicate lesl runs.

X :\PROJECTS\DOCUMENT\2301-2375\2302\2302r.doc ATTACHMENT B-1

NOx Emission Factor Sample Calculations North River WWTP

Cogeneration Engines NOx Emission Factor Sample Calculations

Draft Permit (Larger Parameters Engines) Selected Smaller Engines Conversion factors Engine Size (MW) 3.37 3.03 1 kW= 1.34102209 hp Engine EEF (Btu/kW) (DG) 8,066 8,607 9,522 range 1 lb= 453.59 g Engine EEF (Btu/kW) (NG) 8,066 8,440 9,337 range 1MMBtu 1,000,000 Btu Digester Gas HHV (Btu/cf) 850 690 750 range Natural Gas HHV (Btu/cf) 1,050 1,050 Emission Factor (g/bhp-hr) 0.98 0.98 PTE in permit

Equations used for emission factor calculations: Emission factor (lbs/mmbtu): (0.98 g/bhp‐hr) x (1 lb /453.59 g) x (1.34102209 hp/1 kW) / 8,066 Btu/kW) x (1,000,000) = 0.36 lbs/mmbtu Emission factor (lbs/mmcf): 0.36 lbs/MMBtu x 1050 Btu/cf = 306.72 lbs/mmscf

Calculations‐ Current Draft Permit Digester Gas Emission Factor NOx (lbs/MMBtu) 0.36 NOx (lbs/mmcf) 306.72 Emission factor in current draft permit for the cogeneration engines operatng on digester gas

Natural Gas Emission Factor NOx (lbs/MMBtu) 0.36 NOx (lbs/mmcf) 378.895 Emission factor in current draft permit for the cogeneration engines operating on natural gas

Calculations for selected new, smaller engines that demonstartes compliance with the factors in the draft permit Digester Gas Emission Factor Using Lower EEF factor (8,607 Btu/kW) Using Low HHV Using High HHV NOx (lbs/MMBtu) 0.34 NOx (lbs/mmcf) 233.34 253.63 range based on HHV values, much less than the 306.72 lbs/mmcf in the draft permit

Using Higher EEF factor (9,522 Btu/kW) Using Low HHV Using High HHV NOx (lbs/MMBtu) 0.31 NOx (lbs/mmcf) 210.92 229.26 range based on HHV values, much less than the 306.72 lbs/mmcf in the draft permit

Natural Gas Emission Factor Using Lower EEF factor (8,440 Btu/kW) NG HHV NOx (lbs/MMBtu) 0.34 NOx (lbs/mmcf) 362.11 much less than the 378.895 lbs/mmcf in the draft permit

Using higher EEF factor (9,337 Btu/kW) NG HHV NOx (lbs/MMBtu) 0.31 NOx (lbs/mmcf) 327.32 much less than the 378.895 lbs/mmcf in the draft permit ATTACHMENT B-2

Digester Gas Test Results rcEN~~~,!:t!!~~x?i~ES, LLC ' Phone (315) 431-9730 • Emergency 24/7 (315) 416-2752 • NYSDOH ELAP Ccrtificntc No, 11830[r ------, Analytical Report11

Timothy Shadi, P.E. Monday, April 25, 2011 Savin Engineers, P.C. Order No.: Cl 104029 3 Campus Drive Pleasantville, NY 10570

TEL: (914) 769 - 3200 FAX: RE: North River

Dear Timothy Shadi, P.E.:

Centek Laboratories, LLC received 1 sample( s) on 4/18/2011 for the analyses presented in the following report.

I certify that this data package is in compliance with the terms and conditions of the Contract, both technically and for completeness. Release of the data contained in this hard copy data package and/or in the computer readable data submitted has been authorized by the Laboratory Manager or his designee, as verified by the following signature.

Centek Laboratories performs all analyses according to EPA, NIOSH or OSHA-approved analytical methods. Centek Laboratories is dedicated to providing quality analyses and exceptional customer service. All method blanks, laboratory spikes, and/or matrix spikes met quality assurance objective except as indicated in the case narrative. All samples were received and analyzed within the EPA recommended holding times. Test results are not Method Blank (MB) corrected for contanJination.

We do our best to malrn our reporting format clear and understandable and hope you are thoroughly satisfied with our services. Please contact your client service representative at (315) 431-9730 or myself, if you would like any additional information regarding this report.

Thank you for using Centek Laboratories. This report can not be reproduced except in its entirety, without prior written authorization.

Sincerely, A~ jY, Russell J. Pellegrino Technical Director

Disclainrnr: The test results and procedures utilized, and laboratory interpretations of the data obtained by Centek as contained in this report are believed by Centek to be accurate and reliable for sample(s)Page 1 tested.of 23 In accepting this report, the customer agrees that the full extent of any and all liability for actual and consequential damages of Centek for the services performed shall be equal to the fee charged to the customer for the services as liquidated damages.

Centek Laboratories, LLC Terms and Conditions

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Page 3 of 23 ~NTEK LABORATORIES, LLC Date: 06-May-l l

CLIBNT: Savin Engineers, P.C. Project: North River CASE NARRATIVE Lab Order: Cl 104029

All method blanks, laboratory spikes, and/or matrix spikes met quality assurance objective except as indicated in the corrective action report(s). All samples were received and analyzed within the EPA recommended holding times. Test results are not Method Blank (MB) corrected for contamination. Samples were analyzed using the methods outlined in the following references:

Compendium of Methods for the Determination of Toxic Organic Compounds, Compendium Method T0-15, January 1999.

Page 4 of 23 Page I of I lb ,:, tG) · :.,,,_,, ·,·, _ ~ ,.-·.- .. .. 6006 ;· <;J.soff Ec:\1,"',;:,0•·, N ;\/,, Pickup/Drapaff ~ li~:~J~~I~~~ (~ .,,,.-,..~-·"······· ONLY '"·'_....- # RSl.!E,0 UPS USE "'-·~·- X //J!./cJ~9 Order '-,~,.t - LAB •. .,~ . ~ .. FedEx Wark ~ Iloatfer.:nc1 IFor , 1 - I X ,!t;Jt\"'.¥'...-, 7 .. · ,,,." .. c/;1.s/;/ {Vt- .,., 'IDate0'ifnea I I FL C, p_ CL ("':=rv"=--.. 1 .,,..~J,.i1J,.,t-?.;f;,,F._1~,,•.,1~1 . I I I , au,;;;,,vu111 .. 71 f(, ><9.J ' ' 1 ; 1 ~r, ~ - nHvv,\Jcmcru -2"ug •ur~ej,Tu!ii:'""i"''lliti\~iiI;;:!:i,1''"~!RJl;r,r 7-Ja..oo Name: na ,,;...,_Ji~~,.,.,,-'1\ti5ir:.,,,,i:~,,,-;u.J~!ti],c1 · ~ 1- i·g· ,__ 30"ugl ~ Site Project: PO#: " __ i; S I ~ -~/....., : .Nan:re AP's ··"t.:~::.i-,,.,.,_,,~~,~~.-•!iJ..:;t!1!lfir.::Jt?;;~i1filwm1mJ:il,!.,-;:.il,i'i:¢.;;,,w.t\r,t':l: • '- J~s/.s- ,,.,r;:,:_ LEED • • CHAIN ,_ 315-431-9731 ·""·r,: l~Centek "'"'cill.,,,,.111?11. i!#fili!l,m'"'lil~i I l.L"!~.. Fax: < ·- ,_ __ _! Brd~.cs Drive by: ,;,-;,; 13206 by: ·"'" 5pm Noon BUIDL/NG Lab Park Days Days Days Days NY r.•!d,t"'t1!Eiiffi~;\ifiinw'""'Pii."""1Jiml:!t11m::-a£.l1,l.;mr~1illmi~li,~e.,~i1!t!i.!i:Sil by by at 1 by: Custody i1' -""·"•'°·' ,!i/f~lmill!!lih'"'W,~'ilfliliiitiff1eo~l'lli!RusljlilfAtr,"-lH%illll 315-431-9730 Da of Day Day Midler Business Business Business Business GREEN Phone: Syracuse, i.JJrnoarq ,?fitl!l1!1i;,!!' Next Next 143 2 3 5 Same j;'":c'~!:O\!i>!JJ'."> 4 :;,,,.,/r.;,,,~,£!~· COMMENTS: Sampled Received Gnain Page 5 of 23 Relinquished Centek Laboratories, LLC

Sample Receipt Checklist

Client Name SAVIN ENGINEERS, P.C. Date and Time Receive 4/1 B/2011

Work Order Numbe C1104029 Received by JDS

Reviewed by J.c,,,-- ;;;rn,. £_~·~;,._,;

Matrix: Carrier name Courier {Centek)

Shipping co Iner/cooler in good condition? Yes 0 NoD Not Presen D

Custody se s intact on shippping container/cooler? Yes D NoD Not Presen 0 Custody seals intact on sample bottles? Yes D NoD Not Presen 0 Chain of custody present? Yes 0 NoD

Chain of custody signed when relinquished and received? Yes 0 NoD Chain of custody agrees with sample labels? Yes 0 NoD Samples In proper container/bottle? Yes 0 NoD Sample containers intact? Yes 0 NoD Sufficient sample volume for indicated test? Yes 0 NoD All samples received within holding time? Yes 0 NoD Container/Temp Blank temperature in compliance? Yes 0 NoD

Water- VOA vials have zero headspace? No VOA vials submitted ~ Yes @,]. No w1J Water- pH acceptable upon receipt? Yes D No0

Adjusted? Checked b

Any Na and/or NA (not applicable) response must be detailed in the comments section be

Client contacted Date contacted: Person contacted

Contacted by: Regarding:

Comments:

Corrective Action

Page 6 of 23 Date: 06-May-l I (~NTEK LABORATORIES, LLC

CLIENT: Savin Engineers, P.C. Project:' North River Work Order Sample Summary Lab Order: Cl 104029

Lab Sample ID Client Sample ID Tag Number Collection Date Date Received Cl 104029-00IA Biogas-Boiler 3 4/15/201 I 4/18/2011

Page 7 of 23 Page I of I I I Date 4/19/201 4/19/2011 4/19/2011 4119/2011 4/19/201 I of Analysis I Page Date Prep Date 06-May-JJ DATES REPORT TCLP TIC + T0-15 TOl5 3588 by Series Series ASTM Method Series Gas by by Name BTU Fixed Siloxnne Sulfurs LFG Test Air J\fntrix I Dntc 4115/201 Collection P.C. LLC ID 3 River Engineers, Snmplc 104029 CJ Savin North Biogns-Boilcr Client Laboratories, ID Order: 104029-00IA Cl Client: Centek Project: Lab Sample

Page 8 of 23 Centek Laboratories, LLC Date: 06-May-l l

CLIENT: Savin Engineers, P.C. Client Sample ID: Biogas-Boiler 3 Lab Order: Cl 104029 Tag Number: Project: North River Collection Date: 4/15/2011 Lab ID: CI I 04029-00 I A Matrix: AIR

Analyses Result **Limit Qua! Units DF Date Analyzed

BTU BY ASTM 3588 STM [email protected] Analyst: RJP BTU Gross or HHV 690 O BTU/cubic ft 4119/2011 BTU Net or LHV 620 o BTU/cubic ft 4/19/2011

FIXED GAS SERIES EPA METHOD JC Analyst: RJP Carbon dioxide 29.9 1.90 % 4/19/2011 Carbon Monoxide ND 0,880 % 4/19/2011 Methane 67.9 0,580 % 4/19/2011 Nitrogen 1.19 8.30 J % 4/1912011 Oxygen 0.360 0.880 J % 4/19/2011

SILOXANE SERIES T0-15 Analyst: LL Decamethylcyclopentaslloxane-D5 230 25 ppbV 5 4119/2011 Decamethyltetraslloxane-L4 33 25 ppbV 5 4/19/2011 Hexamethyicyciotrlslloxane-D3 140 25 ppbV 5 4/19/2011 Hexamethyidlsiioxane-L2 ND 25 ppbV 5 4/19/2011 Octamethylcyclotetrasiloxane-D4 450 25 ppbV 5 4/19/2011 Octamethyltrislloxane-L3 35 25 ppbV 5 4/19/2011 Surr. Bromof\uorobenzene 131 70-130 s %REC 5 4/19/2011 NOTES: * Based on the chromatographic evidence, It appears that the contamination ls from a fuel. Surrogate recovery reported outside establlshed limits.

SULFURS SERIES BY T0-15 T0-15 Analyst: LL 1-Propanethiol 840 50 ppbV 5 4/19/2011 Carbon disulfide 82 50 ppbV 5 4/19/2011 Carbonyl sulfide 33 50 J ppbV 5 4/19/2011 Dimethyl sulfide ND 50 ppbV 5 4/19/2011 Ethyl mercaptan 140 50 ppbV 5 4/19/2011 Hydrogen Sulfide 4800 50 E ppbV 5 4/19/2011 tsopropyl mercaptan 110 50 ppbV 5 4/19/2011 Methyl mercaptan 330 50 ppbV 5 4/19/2011 Surr. Bromofluorobenzene 131 70-130 s %REC 5 4/19/2011 NOTES: E - Estimated value. The amount exceeds the linear working range of the instrument. * Based on the chromatographic evidence, it appears that the contamination is from a fuel, Surrogate recovery reported outside established limits.

LFG BY METHOD TO15 + TIC TO-15 Analyst: LL 1, 1, 1-Trichloroethane ND 25 ppbV 5 4/1912011 1, 1,2,2-Tetrachloroethane ND 25 ppbV 5 4/19/2011 1, 1,2-Trlchloroethane ND 25 ppbV 5 4/19/2011 1, 1-Dichloroethane ND 25 ppbV 5 4/19/2011

Qunlilicrs: • • Reporting Limit Results reported are not blnnk corrected 8 Analyte detected in the associated Method Blank E Value above quantitation rnnge H Holding times for preparation or onalysis exceeded J Analyte detected nt or below quantitation limits JN Non-routine analyte. Quantitntion estimated. ND Not Detected nt the Reporting Limit of3 Page 9S ofSpike 23 Recovery outside accepted recovery limits Page I Centek Laboratories, LLC Date: 06-May-l l

CLIENT: Savin Engineers, P.C. Client Sample ID: Biagas-Boiler 3 Lab Order: Cl 104029 Tag Number: Project: North River Collection Date: 4/15/2011 Lab ID: Cl 104029-00IA Matrix: AIR

Analyses Result **Limit Qua! Units OF Date Analyzed

LFG BY METHOD T015 + TIC T0-15 Analyst: LL 1, 1-Dlchloroethene 42 25 ppbV 5 4/19/2011 1,2,4-Trlchlorobenzene ND 25 ppbV 5 4/19/2011 1,2,4-Trlmethylbenzene 160 25 ppbV 5 4/19/2011 1,2-Dlbromoethane ND 25 ppbV 5 4/19/2011 1,2-Dlchlorobenzene ND 25 ppbV 5 4/19/2011 1,2-Dichloroethane ND 25 ppbV 5 4/19/2011 1,2-Dichloropropane ND 25 ppbV 5 4/19/2011 1,3,5-Trlmethylbenzene 62 25 ppbV 5 4/19/2011 1,3-butadlene ND 25 ppbV 5 4/19/2011 1,3-Dlchlorobenzene ND 25 ppbV 5 4/19/2011 1,4-Dlchlorobenzene ND 25 ppbV 5 4/19/2011 1,4-Dloxane ND 50 ppbV 5 4/19/2011 2,2,4-trlmethylpentane 26 25 ppbV 5 4/19/2011 4-ethyltoluene 48 25 ppbV 5 4/19/2011 Acetone 280 50 ppbV 5 4/19/2011 Ally! chloride ND 25 ppbV 5 4/19/2011 Benzene 38 25 ppbV 5 4/19/2011 Benzyl chloride ND 25 ppbV 5 4/19/2011 Bromodlchloromethane ND 25 ppbV 5 4/19/2011 Bromoform ND 25 ppbV 5 4/19/2011 Bromomethane ND 25 ppbV 5 4/19/2011 Carbon disulfide 94 25 ppbV 5 4/19/2011 Carbon tetrachloride ND 25 ppbV 5 4/19/2011 Chlorobenzene ND 25 ppbV 5 4/19/2011 Chloroethane ND 25 ppbV 5 4/19/2011 Chloroform ND 25 ppbV 5 4/19/2011 Chloromethane ND 25 ppbV 5 4/19/2011 cls-1,2-Dichloroethene ND 25 ppbV 5 4/19/2011 cis-1,3-Dichloropropene ND 25 ppbV 5 4/19/2011 Cyclohexane 19 25 J ppbV 5 4/19/2011 Dlbromochloromethane ND 25 ppbV 5 4/19/2011 Ethyl acetate ND 50 ppbV 5 4/19/2011 Ethylbenzene 270 25 ppbV 5 4/19/2011 Freon 11 ND 25 ppbV 5 4/19/2011 Freon 113 ND 25 ppbV 5 4/19/2011 Freon 114 ND 25 ppbV 5 4/19/2011 Freon 12 ND 25 ppbV 5 4/19/2011 Heptane 130 25 ppbV 5 4/19/2011 Hexachloro-1,3-butadlene ND 25 ppbV 5 4/19/2011 Hexane 76 25 ppbV 5 4/19/2011

Quolificrs: .. Reporting Limit Results reported nre not blonk corrected B Annlyte detected in the nssocintcd Method Blank E Vnlue obove qunntitntion rnnge H Holding times for prepnrntion or nnnlysis exceedeLI Annlytc detected nt or below quuntitntion limits JN Non-routine nnnlyte. Qunntitntion estimated. ND Not Detected nt the Reporting Limit Page 10S ofSpike 23 Recovery outside accepted recovery limits Page 2 of3 Centek Laboratories, LLC Date: 06-May-11

CLIBNT: Savin Engineers, P.C. Client Sample ID: Biagas-Boiler 3 Lab Order: Cl 104029 Tag Number: Project: North River Collection Date: 4/15/2011 Lab ID: Cl 104029-00IA Matrix: AIR

Analyses Result **Limit Qnal Units DF Date Analyzed

LFG BY METHOD T015 + TIC T0-15 Analyst: LL lsopropyl alcohol ND 25 ppbV 5 4/19/2011 m&p-Xylene 360 50 ppbV 5 4/19/2011 Methyl Butyl Ketone ND 50 ppbV 5 4/19/2011 Methyl Ethyl Ketone 74 50 ppbV 5 4/19/2011 Methyl lsobutyl Ketone ND 50 ppbV 5 4/19/2011 Methyl tert-butyl ether ND 25 ppbV 5 4/19/2011 Methylene chloride 9.0 25 J ppbV 5 4/19/2011 a-Xylene 170 25 ppbV 5 4/19/2011 Propylene 540 25 ppbV 5 4/19/2011 Styrene ND 25 ppbV 5 4/19/2011 Tetrachloroethylene 30 25 ppbV 5 4/19/2011 Tetrahydrofuran ND 25 ppbV 5 4/19/2011 Toluene 17000 25 E ppbV 5 4/19/2011 trans-1,2-Dlchloroethene ND 25 ppbV 5 4/19/2011 trans-1,3-Dlchloropropene ND 25 ppbV 5 4/19/2011 Trichloroethene 37 25 ppbV 5 4/19/2011 Vinyl acetate ND 25 ppbV 5 4/19/2011 Vinyl Bromide ND 25 ppbV 5 4/19/2011 Vinyl chloride ND 25 ppbV 5 4/19/2011 Surr: Bromofluorobenzene 101 70-130 %REC 5 4/1912011 NOTES: E - Estimated value. The amount exceeds the linear working range of the instrument,

Qunllficrs: •• Reporting Limit Results reported nre not blnnk corrected B Analytc detected in the ussociatcd Method Blank E Vnluc nbove qunntiLDtion rnnge H Holding times for prcpnrution or analysis exceeded J Annlyte detected nt or below qunntitntion limits Page 11JN ofNon-routine 23 onalytc. Qunntitotion estimated. ND Not Detected nt the Reporting Limit S Spike Recovery outside accepted recovery limits Page 3 of3 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 170 µg/m3 Average** Concentration Analysis [1[1bV Average Concentration Halogens 1 2 2 of Atoms No. Biagas Br 3 of No. FAtoms 3 2 2 2 2 4 2 2 2 2 2 2 2 3 3 3 3 3 1 1 1 1 1 1 1 4 2 2 4 6 .1 of Atoms No. Cl 99.0 96.9 99.0 94.9 50.5 99.0 76.5 B2.5 64.5 133.4 167.B 197.5 133.4 1B1.4 1B7.9 170.9 147.0 113.0 147.0 147.0 163.B 154.0 112.5 119.4 111.0 120.9 253.0 20B.3 260.B MW ,Jmole Formula .114) 113) (CFC (CFC Name 12) 151a) (CFC (CFC it1w!:s1f11c1¢c11:d¢1i$~~~~~IT:~~ Contaminant 1,2,2-trifluoroethane 1,2,2-tetrafluoroethane Corn_1J_ounds Tetrachloride Dichlorobenzene 1-Trichloroethane 0 °Dichloroethene 1,2-Trichloroethane 1,2,2,Tetrachloroethane 1,2-Trichloro' 1 Bromodic::hloromethane Bromofcirm Broniomethane Dibromochloromethane 1,2,4-Trichlorobenzene 1,2-Dibrornoethane 1,2-Dlchloro-1, 1, 1,1-Dk:hloroethane 1, 1~Chloro,1°fluoroethane 1, 1, 1, 1,2-Dichlorobenzene 1,2-Dichloroethane 1,2-Dichloropropane 1,3 1,4-Dlchlorobenzene 1, 1, T0,15 cis-1,2Dlchloroethene cls-1,3-0ichloropropene 3-Chloropropene Carbon Chlorobenzene Chloroethane Chloroform Chlorome!hane Dichlorodifluoron,ethane Hexachlorobutadiene ~Ei'irntl0ara1:irt~'Y:¢1 Page 12 of 23 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 199 203 402 spreadsheet This 109 1 2 3 1 1 4 2 1 3 2 1 1 TOTAL Cl temperature. 3 3 2 2 1 4 2 2 0 1 1 1 2 2 2 2 1 1 1 1 2 2 1 2 2 4 2 actual F degrees 84.9 97.0 66.1 62.5 96.9 86.5 99.0 50.5 68.5 50.5 65.1 165.8 131.4 137.5 102.0 173.0 109.0 106.6 126.6 165.1 153.0 147.0 104.5 126.6 101.0 111.0 147.0 165.8 102.9 186.0 109.0 77 or BTU/SCF C degrees 25 -at ~~\imtll!!._9~Jill~ = Value BTU ???) b) Gas 141 (CFC 134a) 11) 22) 21) (CFC 31) 13) (CFC 152a) (CFC (CFC (CFC (CFC (CFC (CFC Ether 1,2-trifluoroethane Vinyl Chlortde Fluortde Dibromide 1-bromo,3,3-dimethyl Chloride Dichloroethane Chloride ,3-Dichloropropene 1 Chlortde 0 1,2,2-Tetrafluoroethane 1-Dichloro-1-fluoroethane 1,-Difluoroethane Others Benzyl Methylene 1,2-Dichloro-1, 1, 1, 1,2-Dichlorobenzene 1,2-Dichloroethene 1, trans-1,2-Dichloroethene trans Chlorodifluoromethane Chlorofluoromethane Butane, Dichlorofluoromethane Vin;tl Tetrachloroethene Trtchloroethene Trtchlorofluorornethane 2-Chloroethyl a-Chlorotoluene c-1,2-Dichloroethene cis-1,2 Chloromethane Chlorotrtfluoroethene Methyl Perchloroethylene Dichlorobenzenes Ethylene cis-1,2-Dichloropropene trans-1,2-Dichloropropene Trimethyl

Page 13 of 23 by 1000 divide by then multiply F) Weight, IUPAC then C degrees Molecular 60 is degrees by 0 temperature), For ppmv applications standard multiply degrees gas 32 for is ppmv, temperature/ from 3 temperature µg/m temperature (actual x obtain Standard (Standard 22.414 To

Page 14 of 23 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 Cl 30.1 as ~v 0.01 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 µg/BTU 0 0 0 0 0 0 0 0 0 0 0 0 3 0 0 0 0 0 0 0 0 0 0 0 0 0 0.00 0.00 0.00 0.00 µg/SCF Concentration Cl 79.84% 84.60% 82.78% 79.83% 71.75% 73.24% 71.75% 66.06% 92.11% 58.69% 85.06% 86.00% 48.30% 48.30% 48.30% 70.31% 71.72% 62.84% 37.39% 92.21% 31.56% 93.77% 90.16% 55.04% 89.20% 46.39% 42.09% 63.98% 81.68% %Cl/mole

Page 15 of 23 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 25.7 30.0 85.8 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.01 0.00 0.01 0.02 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 4.56 4.93 0.00 0.00 0.00 12.94 temperature for correc TOTAL not 91.27% 57.53% 48.30% 48.40% 74.49% 73.24% 71.72% 79.54% 70.31% 70.30% 70.31% 73.20% 33.32% 65.14% 56.80% 52.02% 83.66% 84.97% 88.52% 87.44% 85.91% 85.63% 81.06% 85.63% 83.60% 48.30% 28.05% 28.04% 29.19% 63.98% 65.14% Cl does Page 16 of 23 Page 17 of 23 o o o o o o o o o o o o o o o o o o o o o o o o 338 1,273 Organosilicon 19.21% 18.95% 18.44% 17.87% 17.53% 14.76% 14.60% 13.48% 26.95% 21.77% 31.84% 31.14% 37.85% 41.82% 29.21% 20.93% 23.75% 21.23% 21.23% 21.23% 20.62% 30.47% 37.87% 35.62% 34.59% 40.42% 47.60% %Si/mole 88.2 90.2 96.2 92.2 104.2 118.3 129.0 132.3 132.3 132.3 134.3 136.2 146.2 148.2 148.4 152.3 157.2 160.2 162.4 190.3 192.3 208.3 208.5 222.5 236.0 236.5 268.4 MW g/mole 1 :~lm::~ 1 3 Si 0 3 0 OOSi Formula 18 130Si 10osi2 H csH c0H2402si3 CB C3H1 C6H C7H1302Si C8H20Si0 C5H160Si2 C9H16Si C8H20Si03 CBH20Si04 C6H2002Si3 C13H2402Si2 C3H6F2Si C6H160Si C4H1402Si2 C7H18Si0 C4H1204Si4 C4H12Si C8H18Si03 (CH3)3Si03C2H3 (CH3)3SiF (CH3)4Si0 (CH3)3SiOC2H5 (CH3)3SiOC3HB (CH3)3SiOC3HB (CH3)3SiOCH3 :m:m,,t 1 Ester Name # • # # Silane # Silane tiQ:i~JJg![~!))i\Ui/e~)j;[U:i:imm:m:i!iiij[i 2,4-bis(trimethylsilyl)- Silane Silane Fluoride• Trimethylsilyl Contaminant Acid, Project: Date: lsopropoxytrimethylsilane 1-Methylbutoxytrimethylsilane t'l!iX1liili\!tiY!9YSI Benzaldehyde, Methoxytrimethylsilane Butoxytrimethylsilane Pentamethyldisiloxane Difluorodimethylsilane Propoxytrimethylsilane Hexamethyltrisiloxane Ethoxytrimethylsilane 2,2-Dimethyl-1-oxa-2-silacyclo,3-5- 2,4,6,8-Tetramethylcyclotetrasiloxane 8~~anitl!RyJaisOiiicaniiHMMFill21l:mG:rnmm~m §11,:,~~n~'(MRTl/lrPs)'m2:mn=mi,::TTin11i1:m::Eillii'il'Di',rn Triallylsilane Tetrolic Tetraethylsilicate Trimethylsilyl Tert-butyldimethylsilanol Tetramethyldisiloxane Trimethoxymethyl Trimethoxyvinyl Trimethylsilanol Triethoxyethyl Tetramethylsilane Triethoxyvinyl ~Enter::o~ta~in$v~11&"w:rstfa'c1.e~1rce11s:r,~i~,,:1~:m,'l~t1w]::c.~~

Page 18 of 23 0 0 0 0 0 419 by 5,456 3,486 divide 1000 by then F) Weight, multiply C then degrees Molecular 60 is by degrees O temperature. 6.80% temperature), ppmv 20.18% 39.75% 37.88% 36.16% 37.88% 36.49% 37.88% For TOTALS Factual applications multiply standard degrees gas 32 degrees for 412.9 278.3 282.6 296.6 310.7 370.8 384.9 444.9 is ppmv, 77 or from C 3 temperature/ temperature µg/m temperature degrees (actual x 25 obtain C12H36O6Si6 C14H22O2Si2 22.4 Standard C8H26O3Si4 C20H38Cl3Si C12H36O4Si5 (Standard To **at L5) (D6) (MD3M, ~::~:~a~~~:~l~~;~;;;~;;~:~:~:r~~;~~~::IBTU/SCF 1,3,3,5,5,7,7-Octamethyltetrasiloxane Dodecamethylcyclohexasiloxane Dodecamethylpentasiloxane 1, &i~ii!it~~~~~t;i1~~~~~~~~ililj,"'''(g!~~~~~i~:: p-Trimethylsilyloxyphenyl-bis(trimethyl)- Trichlorodocosylsilane

Page 19 of 23 a.a a.a a.a a.a a.a a.a a.a a.a a.a a.a a.a a.a a.a a.a a.a a.a a.a a.a a.a a.a a.a a.a a.a a.a a.a 18.1 76.9 l~{~; Basis 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.007 0.000 0.029 ~~iil!it!f Content 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 4.95 19.82 (Si) ~tl(iyil Silicon 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.175 0.000 0.700 a a a a a a a a a a a a a a a a a a a a a a a 121 482 Biogas

Page 20 of 23 0.0 0.0 a.a a.a a.a 17.3 126.4 247.4 entirely 0.000 0.000 q~4f7-S~@Z!U·ss-:?~~:-,:. 0.079 0.009 0.123 0.000 0.000 0.000 ... two --~ are interchangeably. used Silicon" be "As 0.00 0.00 0.00 6.23 0.00 0.00 54.26 84.93 cannot and and Basis i·,:·:::z~:::~~~-~!.~1:::ii2i'.:'.lil .. Content 0.000 0.000 1.916 0.220 0.000 2.999 0.000 0.000 Silicon Note: different representations 0 0 0 a a 152 1,320 2,066 L..:~~!;r~£~,:;.··:,-~=s·::E~::iJ;·P1([~t>"::

Page 21 of 23 Vol. % D1946: psig 1.00 1.00 1.00 Limit, 1.00 1.00 balance) HHV) 100% LHV)- or ASTM 14.73 or for mass tolal por Reporting to (By (Gross (Net tested 3C D3588@ not corrected 694 625 1.11% 0.34% 30.1% 68.4% ND - = ASTM 0.851 Corrected Method and - -per '*Values (EPA 089 620 0.845 ID: Date: foot foot Constituents (Est.) Sample Sample Gravity Gas Dioxide Monoxide Vapor BTU/cubic BTU/cubic Sp. butane Isa Butane lsopentane Hydrogen Neopentane Major Total Ethane Propane Carbon Oxygen C6+ Pentane Methane Nitrogen Ethene Acetylene Water Total Carbon Total mmg~i~rciR11.ta~iH1v~116:WMs~~'a€t1':e~11~~~,~~%'i

Page 22 of 23 Page 23 of 23 Page 1 of 10 ---- ~EKTEKJ,ABORATORTF,8; TJT,C ___------~ ~.... 143 Mitller Park Drive• Syracuse, NY 13206 ' Phone (315) 431-9730 • Emergency 24/7 (315) 416-2752 ~ NYSDOI-1 ELAP Certificate No. 11830 !Analytical Reportl

Timothy Shadi, P .E. Friday, May 20, 2011 Savin Engineers, P.C. Order No.: Cl 105020 3 Campus Drive Pleasantville, NY I 0570

TEL: (914) 769 - 3200 FAX: RE: North River

Dear Timothy Shadi, P.E.:

Centek Laboratories, LLC received 2 sample( s) on 5/13/2011 for the analyses presented in the following report.

I certify that this data package is in compliance with the terms and conditions of the Contract, both technically and for completeness. Release of the data contained in this hardcopy data package and/or in the computer readable data submitted has been authorized by the Laboratory Manager or his designee, as verified by the following signature.

We do our best to make our reporting format clear and understandable and hope you are thoroughly satisfied with our services. Please contact your client service representative at (315) 4 31-973 0 or myself, if you would like any additional information regarding this report.

Thank you for using Centek Laboratories. This report can not be reproduced except in its entirety, without prior written authorization.

Sincerely, /4/~ Russell J. Pellegrino Technical Director

Disclaimer: The test results and procedures utilized, and laboratory interpretations of the data obtained by Centek as contained in this report are believed by Centek to be accurate and reliable for sample(s) tested. In accepting this report, the customer agrees that the full extent of any and all liability for actual and consequential damages of Centek for the services performed shall be equal Pageto the fee2 of charged 10 to the customer for the services as liquidated damages.

Centek Laboratories, LLC Terms and Conditions

Blanks Every sample is run with a surrogate or tracer compound at a pre-established concentration. The surrogate compound run with each sample is used as a standard to measure the performance of each rllll of the instrument. If required, a Mini can can be provided containing nitrogen to be run as a trip blank with your samples.

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Date: 24-May-I I

CLIENT: Savin Engineers, P.C. Project: North River CASE NARRATIVE Lab Order: C1105020

Compendium of Methods for the Determination of Toxic Organic Compounds, Compendium Method TO-15, January 1999.

Client needs BTU, sulfur, siloxanes, CO2 and methane content. Does not require TO 15 w/ TICs like previous analyses for this site.

Page I of I Page 5 of 10 G '; ?'a 431-9731 /UPS .2'J UJ /o.5 x r.r iJ (315) f: ~<> - 0c,-r:, J{)Z S A.;,:;, O Z)rlv~ f r '7- _e,--;:-., Cf , 76' ,I;,_ r~l:;c;>rlo:==ia Print ...... l,:,., -~-, Le>~ F=='======.ba=====+=====d======~1====s======,l=,.,,...,=====il====I C:c:,,r,l:;~I<. /:_Jc,, ,,..--- -Der - Noon 5pm ( Days Days Days Days iiitiiJ-·._:___- by by 7 5 .E 7 Day 'r Day Day Business Business Business Business 3 5 Same Next Next 4 2 Page 6 of 10

Sample Receipt Checklist

Client Name SAVIN ENGINEERS, P.C. Date and Time Receive 5/13/2011

Work Order Numbe C1105020 Received by DL

'I' /J-;-? - L I Checklist completed by fri · -f:i___ o"-.0-Jq'--'-'1f,..:1/Z=Jl"-I- Reviewed by , 7e.,;- -4; ,/4, "M,,,,- .5- _)if.;/ .JL lnlUals j Data

Matrix: Carrier name FedEx

Shipping container/cooler in good condition? Yes 0 NoD Not Presen D

Custody seals Intact on shippplng container/cooler? Yes D NoD Not Presen 0

Custody seals intact on sample bottles? Yes D NoD Not Presen 0

Chain of custody present? Yes 0 NoD

Chain of custody signed when relinquished and received? Yes 0 NoD

Chain of custody agrees with sample labels? Yes 0 NoD

Samples in proper container/bottle? Yes 0 NoD

Sample containers intact? Yes 0 NoD

Sufficient sample volume for Indicated test? Yes 0 NoD

All samples received within holding time? Yes 0 NoD

Container/Temp Blank temperature in compliance? Yes 0 NoD

Water- VOA vials have zero headspace? No VOA vlals submitted 0 Yes D NoD Water- pH ac!:f!ptable upon receipt? Yes D No@

Adjusted? Checked b

Any No and/or l'J.A (not appllcable) response must be detailed In the comments section be

Client contacted Date contacted: Person contacted

Contacted by: Regarding:

Comments:

Corrective Action Page 7 of 10

CLIENT: Savin Engineers, P .C. Project: North River Work Order Sample Summary Lab Order: Cl 105020

Lab Sample ID Client Sample ID Tag Number Collection Date Date Received Cl 105020-00JA Dig 5 5/12/2011 5/13/2011

C 1105020-002A Dig 7 5/12/2011 5/13/2011

Page I of 1 I I

Page 8 Dntc of 10 5/131201 511812011 5/13/201 5/13/2011 5/1312011 5113/2011 5/13/2011 j ~ I . !i , " 15/13/2011 15/13/2011 15/17/2011 , 1 1 l i I I Arlnlysis I Page Date REPORT Prep Date 24-May-ll DATES TCLP TO-15 TO-15 T0-15 T0-15 3588 by by by by Series Series Series Series ASTM3588 ASTM Series Series Series Series Gos Gas by by Nnmc BTU BTU Fixed Fixed Sulrur:s Siloxnne Sulfurs Siloxnne Sulfurs Sulfurs Test Air Matrix Dute 5/12/2011 Collection P.C. LLC ID River Engineers, Semple 5 7 Savin Cll05020 North Dig Client Dig Laboratories, ID Order: Project: Lab Cl105020-002A Cl105020-001A Client: Sample Centek ------'--- Page 9 of 10

.,...... ,.,,-.,-.. -- ~= - "" - =-=-="' Centek Laboratories, LLC Date: 24-May-1 J

CLIENT: Savin Engineers, P.C. Client Sample ID: Dig 5 Lab Order: Cl 105020 Tag Number: Project: North River Collection Date: 5/12/201 I Lab ID: CJ 105020-00JA Matrix: AIR

Analyses Result **Limit Qual Units DF Date Analyzed

BTU BY ASTM 3588 STM [email protected] Analyst: LL BTU Gross or HHV 710 0 BTU/cubic ft 5/13/2011 BTU Net or LHV 640 0 BTU/cubic ft 5/13/2011

FIXED GAS SERIES EPA METHOD 3C Analyst: LL Carbon dioxide 28.1 1.90 % 5/13/2011 Carbon Monoxide ND 0.880 % 5/13/2011 Methane 69.6 0.580 % 5/13/2011 Nitrogen 0.936 8.30 J % 5/13/2011 Oxygen 0.213 0.880 J % 5/13/2011

SILOXANE SERIES TO-15 Analyst: LL Decamethylcyc[opentaslloxane-D5 470 20 ppbV 4 5/13/2011 Decamethyltetraslloxane-L4 42 20 ppbV 4 5/13/2011 Hexamethylcyclotrlslloxane-D3 17 20 J ppbV 4 5/13/2011 Hexamethyldlslloxane-L2 ND 20 ppbV 4 5/13/2011 Octamethylcyclotetraslloxane-D4 280 20 ppbV 4 5/13/2011 Octamethyltrislloxane-L3 16 20 J ppbV 4 5/13/2011 Surr. Bromofluorobenzene 126 70-130 %REC 4 5/13/2011

SULFURS SERIES BY TO-15 TO-15 Analyst: LL 1-Propanethlol 1300 40 ppbV 4 5/13/2011 Carbon disulfide ND 40 ppbV 4 5/13/2011 Carbonyl sulfide 78 40 ppbV 4 5/13/2011 Dimethyl sulfide ND 40 ppbV 4 5/13/2011 Ethyl mercaptan 410 40 ppbV 4 5/13/2011 Hydrogen Sulfide 370000 100000 ppbV 10240 5/18/2011 11 :33:00 AM lsopropyl mercaptan 200 40 ppbV 4 5/1312011 Methyl mercaptan 90 40 ppbV 4 5/13/2011 Surr. Bromofluorobenzene 126 70-130 %REC 4 5/13/2011

Qualifiers: •• Reporting Limit Results reported nre not blnnk corrected 8 Annlyte detected in the a.ssociated MeUmd Blnnk E Vnlue nbove qunntitation range H Holding times for prepnration or nnalysis exceeded J Annlyte detected at or below qunntitation limits JN Non-routine nnalyte. Quantitntion estimated. ND Not Detected at the Reporting Limit Page I of2 S Spike Recovery outside accepted recovery limits Page 10 of 10

Centek Laboratories, LLC Date:

CLIENT: Savin Engineers, P.C. Client Sample ID: Dig 7 Lab Order: Cl105020 Tag Number: Project: North River Collection Date: 5/12/2011 Lab ID: Cl 105020-00ZA Matrix: AIR

Analyses Result ••Limit Qua! Units DF Date Analyzed

BTU BY ASTM 3588 STM [email protected] Analyst: LL BTU Gross or HHV 720 0 BTU/cubic ft 5/13/2011 BTU Net or LHV 640 0 BTU/cubic ft 5/13/2011

FIXED GAS SERIES EPA METHOD JC Analyst: LL Carbon dioxide 26.4 1.90 % 5/13/2011 Carbon Monoxide ND 0.880 % 5/13/2011 Methane 70.5 0.580 % 5/13/2011 Nitrogen 0.867 8.30 J % 5/13/2011 Oxygen 0.208 0.880 J % 5/13/2011

SILOXANE SERIES T0-15 Analyst: LL Decamethylcyclopentaslloxane-D5 230 20 ppbV 4 5/13/2011 Decamethyltetrasiloxane-L4 19 20 J ppbV 4 5/13/2011 Hexamethylcyclotrlsiloxane-D3 7.8 20 J ppbV 4 5/13/2011 Hexamethyldislloxane-L2 ND 20 ppbV 4 5/13/2011 OctamethyJcyclotetraslloxane-D4 200 20 ppbV 4 5/13/2011 Octamethyltrlslloxane-L3 12 20 J ppbV 4 5/13/2011 Surr: Bromofluorobenzene 128 70-130 %REC 4 5/13/2011

SULFURS SERIES BY T0-15 T0-15 Analyst: LL 1-Propanethlol 810 40 ppbV 4 511312011 Carbon disulfide ND 40 ppbV 4 5/1312011 Carbonyl sulfide 31 40 J ppbV 4 511312011 Dimethyl sulfide 26 40 J ppbV 4 5/13/2011 Ethyl mercaptan 300 40 ppbV 4 5/13/2011 Hydrogen Sulfide 310000 51000 ppbV 5120 5/17/2011 7:28:00 PM lsopropyl mercaptan 140 40 ppbV 4 5/1312011 Methyl mercaptan 240 40 ppbV 4 5/13/2011 Surr: Bromofluorobenzene 128 70-130 %REC 4 5/13/2011

Qualifiers: .. Reporting Limit Results reported arc not blnnk corrected B Annlytc detected in the a.ssocintedMethod Blank E Volue nbovc qunntiUltion rnnge H Holding times for prepnrotion or nnnlysis exceeded Anulytc detected nt or below qunntitntion limits JN Non-routine unulytc. Qunntitntion estimated. ND Not Detected nl the Reporting Limit S Spike Recovery outside occepted recovery limits Page 2 of2 <0:EN~!!;~,!.,:~~~J'2~s, LLC ~ Phone (315) 431-9730 • Emergency 24/7 (315) 416-2752 , NYSDOH ELAP Certificate No. 11830 _l______Analytical Reportl

Timothy Shadi, P.E. Friday, June 17, 2011 Savin Engineers, P.C. Order No.: Cl 106017 3 Campus Drive Pleasantville, NY I 0570

TEL: (914) 769 - 3200 FAX: RE: North River

Dear Timothy Shadi, P.E.:

Centek Laboratories, LLC received 3 sample(s) on 6/9/2011 for the analyses presented in the following report.

Thank you for using Centek Laboratories. This report can not be reproduced except in its entirety, without prior written authorization.

Sincerely, ~ /)1 L /J/ 7~ Russell J. Pellegrino Technical Director

Page 1 of 11 all liability for actual and consequential damages of Centek for the services performed shall be equal to the fee charged to the customer for the services as liquidated damages.

Centek Laboratories, LLC Terms and Conditions

Page 2 of 11 Rush Turnaround Samples Expedited tum around times is available. Please con.firm rush turnaround times with Client Services before submitting samples.

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Limitation on Liability Centek Laboratories, LLC warrants tl1e test results to be accurate to the methodology and sample type for each sample submitted to Centek Laboratories, LLC. In no event shall Centek Laboratories, LLC be liable for direct, indirect, special, punitive, incidental, exemplary or consequential damages, or any damages whatsoever, even if Centek Laboratories, LLC has been previously advised of tl1e possibility of such damages whether in an action under contract, negligence, or any other theory, arising out of or in connection with the use, inability to use or performance of the information, services, products and materials available from the laboratory or this site. These limitations shall apply notwithstanding any failure of essential purpose of any limited remedy. Because some jurisdictions do not allow limitations on how long an implied warranty lasts, or the exclusion or limitation of liability for consequential or incidental damages, the above limitations may not apply to you. This is a comprehensive limitation of liability that applies to all damages of any kind, including (without limitation) compensatory, direct, indirect or consequential damages, loss of data, income or profit and or loss of or damage to property and claims of third parties.

Page 3 of 11 ~~NTEK LABORATORIES, LLC Date: 18-Jun-11 . ~ .•,

CLIENT: Savin Engineers, P.C, Project: North River CASE NARRATIVE Lab Order: CJ106017

All method blanks, laboratory spikes, and/or matrix spikes met quality assurance objective except as indicated in the corrective action report(s). All samples were received and analyzed within the EPA reconunended holding times. Test results are not Method Blank (MB) corrected for contamination. Samples were analyzed using the methods outlined in the following references:

Compendium of Methods for the Determination of Toxic Organic Compounds, Compendium Method T0-15, January 1999.

Page I of I

Page 4 of 11 431-9731 (315) f: 431-9730 C1;t1c;o17 (315) p: Invoice: Phone: Company: 'o,570. x;}.31_ Project: PO#: Right Drive Custody Lower Parle NY13212 of #'s Mid/er Chain 143 Syracuse, Contact Repmt: Company: www.CentekLabs.com Phone: 'c."":~.'."7.c" .. SA'~ Name ~:~ T,.,., Print ':c::":'..~,:c' k ~ ~ 3 Noon 5pm -:;::.---· Days Days Days Days by by r. Day Day Day ,I,~~-~~"'= ,n;!f> Business Business Business Business l'\;~esyi'.er 5 Next Next 4 2 Saine 3

Page 5 of 11 Centek Laboratories, LLC

Sample Receipt Checklist

Client Name: SAVIN ENGINEERS, P.C. Date and Time Received 6/9/2011

Work Order Number C1106017 Received by: JDS

Reviewed by k ..J! ,Lu~~- b (CJ); f fnlUals ' Oata

Matrix: Carrier name: FedEx

Shipping container/co er In good condltion? Yes ~ NoD Not Present D

Custody seals intact on shlppplng container/cooler? Yes D NoD Not Present ~

Custody seals Intact on sample bottles? Yes D NoO Not Present ~

Chain of custody present? Yes ~ NoD Chain of custody signed when rellnqulshed and received? Yes ~ NoO

Chain of custody agrees with sample labels? Yes ~ NoD

Samples In proper container/bottle? Yes ~ NoO

Sample container.; Intact? Yes ~ NoD

Sufficient sample volume for Indicated test? Yes ~ NoO

All samples received within holdlng time? Yes ~ NoO Contalnerffemp Blank temperature In compliance? Yes ~ NoO

Water- VOA vials have zero headspace? No VOA vials submitted ~ Yes D NoO Water- pH acceptable upon receipt? Yes D No~

Adjusted? Checked by

Any No and/or NA {not applicable) response must be detalled In the comments section bel ------

Client contacted: ------Date contacted: Person contacted

Contacted by: Regarding:

Comments:

Corrective Action

Page 6 of 11 Date: 18-Jun-11 ~NI'EK LABORATORIES, LLC

CLIENT: Savin Engineers, P.C. Project: North River Work Order Sample Summary Lab Order: Cll06017

Lab Sample ID Client Sample ID Tag Number Collection Date Date Received C!I06017-00lA Digester 5 6/8/2011 6/9/2011

CI 1060 I 7-002A Digester 6 6/8/201 I 6/9/2011

C!I06017-003A Digester 3 6/8/2011 6/9/2011

Page 1 of 1

Page 7 of 11 l Date 6/10/2011 6/10/2011 6/14/2011 6/1612011 6115/2011 6/14/2011 6/10/201 6/10/2011 6/14/2011 6/16/2011 6/14/2011 6110/2011 6/10/2011 6/14/2011 6/14/2011 I of Analysis I Page Datt!: REPORT Prep l Dntc 18-Jun-l DATES TCLP T0-15 T0-15 T0-15 T0-15 T0-15 T0-15 3588 3588 3588 by by by by by by Series Series Series Series Series ASTM ASTM ASTM Series Seric:s Series Series Series Series Gus Gus Gus by by by Name BTU BTU BTU Fixed Fixed Fixed Test Sulfurs Sulfurs Sulfurs Siloxanc Sulfurs Sulfurs SiloxancScrics Siloxanc Sulfurs Air Mntrix Date 6/8/2011 Collection P.C. LLC ID River Engineers, 5 6 3 Sample Savin Cll06017 North Digester Digester Digester Client Laboratories, ID Order: Client: Centek Project: Lab Cl106017-001A Cl106017-002A Cl106017-003A Sample

Page 8 of 11 Centek Laboratories, LLC Date: 18-Jun-11

CLIENT: Savin Engineers, P.C. Client Sam pie ID: Digester 5 Lab Order: CJJ06017 Tag Number: Project: North River Collection Date: 6/8/2011 Lab ID: Cl 106017-00lA Matrix: AIR

Analyses Result ••Limit Qual Units DF Date Analyzed

BTU BY ASTM 3588 STM [email protected] Analyst: LL BTU Gross or HHV 710 0 BTU/cubic ft 6/10/2011 BTU Net or LHV 640 0 BTU/cubic ft 6/10/2011

FIXED GAS SERIES EPA METHOD 3C Analyst: LL Carbon dioxide 27.0 1.90 % 6/10/2011 Carbon Monoxide ND 0.880 % 6/10/2011 Methane 70.1 0.580 % 6/10/2011 Nitrogen 0.750 8.30 J % 6/10/2011 Oxygen 0.264 0.880 J % 6/10/2011

SILOXANE SERIES T0-15 Analyst: LL Decamethylcyclopentaslloxane-D5 210 25 ppbV 5 6/14/2011 Decamethyltetraslloxane-L4 14 25 J ppbV 5 6/14/2011 Hexamethylcyclotrlsiloxane-D3 100 25 ppbV 5 6/14/2011 Hexamethyidlslioxane-L2 ND 25 ppbV 5 6/14/2011 Octamethylcyclotetraslloxane-04 260 25 ppbV 5 6/14/2011 Octamethyltr1siioxane-L3 9.5 25 J ppbV 5 6/14/2011 Surr: Bromofluorobenzene 116 70-130 %REC 5 6/14/2011

SULFURS SERIES BY T0-15 T0-15 Analyst: LL 1-Propanethlol 640 200 ppbV 20 6/15/2011 7:54:00 AM Carbon d!sulfide ND 50 ppbV 5 6/14/2011 Carbonyl sulfide 140 50 ppbV 5 6/14/2011 Dimethyl sulfide ND 50 ppbV 5 6/14/2011 Ethyl mercaptan 250 50 ppbV 5 6/14/2011 Hydrogen Sulfide 190000 26000 ppbV 2560 6/16/2011 6:02:00 PM lsopropyl mercaptan 97 50 ppbV 5 6/14/2011 Methyl mercaptan 140 50 ppbV 5 6/14/2011 Surr: Bromofluorobenzene 116 70-130 %REC 5 6/14/2011

Qualifiers: .. Reporting Limit Results reported nre not blank corrected B Annlyte detected in the nssocinted Method Bhmk E Value above quantitntion range H Holding times for preparation or analysis exceeded J Annlytc detected at or below qunntitntion limits JN Non-routine 11111ilyte. Qunntitntion estimated. ND Not Detected at the Reporting Limit S Spike Recovery outside accepted recovery limits Page 1 of3

Page 9 of 11 Centek Laboratories, LLC Date: 18-Jun-JJ

CLIENT: Savin Engineers, P.C. Client Sample ID: Digester 6 Lab Order: Cl106017 Tag Number: Project: North River Collection Date: 6/8/2011 Lab ID: C II 060 I 7-002A Matrix: AIR

Analyses Result **Limit Qual Units DF Date Analyzed

BTU BY ASTM 3588 STM [email protected] Analyst: LL BTU Gross or HHV 720 0 BTU/cubic fl 6/10/2011 BTU Net or LHV 650 0 BTU/cubic fl 6/10/2011

FIXED GAS SERIES EPA METHOD 3C Analyst: LL Carbon dioxide 27.4 1.90 % 6/10/2011 Carbon Monoxide ND 0.BB0 % 6/10/2011 Methane 70.7 0,5B0 % 6/10/2011 Nitrogen 0.72B B.30 J % 6/10/2011 Oxygen 0.22B 0.BB0 J % 6/10/2011

SILOXANE SERIES T0-15 Analyst: LL Decamethylcyclopentaslloxane-D5 150 25 ppbV 5 6/14/2011 Decamethyltetraslloxane-L4 7.4 25 J ppbV 5 6/14/2011 Hexamethylcyclotnslloxane-D3 16 25 J ppbV 5 6/14/2011 Hexamethyldlslloxane-L2 ND 25 ppbV 5 6/14/2011 0 eta methyl cyclotetra sllaxane-D4 B4 25 ppbV 5 6/14/2011 Dctamethyltrlslloxane-L3 ND 25 ppbV 5 6/14/2011 Surr. Bromofluorobenzene 110 70-130 %REC 5 6/14/2011

SULFURS SERIES BY T0-15 T0-15 Analyst: LL 1-Propanethlol 320 50 ppbV 5 6/14/2011 Carbon disulfide ND 50 ppbV 5 6/14/2011 Carbonyl sulfide 56 50 ppbV 5 6/14/2011 Dimethyl sulfide ND 50 ppbV 5 6/14/2011 Ethyl mercaptan 140 50 ppbV 5 6/14/2011 Hydrogen Sulfide 130000 26000 ppbV 2560 6/16/2011 6:37:00 PM [sopropyl mercaptan 60 50 ppbV 5 6/14/2011 Methyl mercaptan 39 50 J ppbV 5 6/14/2011 Surr. Bromofluorobenzene 110 70-130 %REC 5 6/14/2011

Qu11lificrs: ,... Reporting Limit Results reported nre not blank corrected 8 Anulyte detected in the n.ssocinted Melhod Blank E Vuluc ubove quuntitntion rungc H Holding times for prepnrntion or nnnlysis exceeded J Annlyte detected ut or below qunntitation limits JN Non-routine unnlyte, Qunntitntion estimated. ND Not Detected ut the Reporting Limit S Spike Recovery outside accepted recovery limits Page 2 of3

Page 10 of 11 Centek Laboratories, LLC Dote: 18-Jun-ll

CLIENT: Savin Engineers, P.C. Client Som pie ID: Digester 3 Lob Order: Cl 106017 Tog Number: Project: North River Collection Dote: 6/8/201 I Lob ID: Cl 106017-003A Motrix: AIR

Anolyses Result **Limit Quol Units DF Date Anolyzed

BTU BY ASTM 3588 STM [email protected] Analyst: LL BTU Gross or HHV 750 0 BTU/cubic ft 611012011 BTU Net or LHV 680 0 BTU/cubic ft 6/10/2011

FIXED GAS SERIES EPA METHOD 3C Analyst: LL Carbon dioxide 26.0 1.90 % 6/10/2011 Carbon Monoxide ND 0.880 % 6110/2011 Methane 74.4 0.580 % 611012011 Nitrogen 1.46 8.30 J % 6110/2011 Oxygen 0.402 0.880 J % 6/10/2011

SILOXANE SERIES T0-15 Analyst: LL Decamethylcyclopentaslloxane-D5 330 25 ppbV 5 6/14/2011 Decamethyltetraslloxane-L4 18 25 J ppbV 5 6114/2011 Hexamethylcyclotrls!loxane-D3 85 25 ppbV 5 6114/2011 Hexamethyldlslloxane-L2 ND 25 ppbV 5 6/14/2011 Octamethy[cyctotetraslloxane-D4 350 25 ppbV 5 6114/2011 Octamethyltrisltoxane-L3 9.6 25 J ppbV 5 6/14/2011 Surr. Bromofluorobenzene 125 70-130 %REC 5 6/14/2011

SULFURS SERIES BY TO-15 T0-15 Analyst: LL 1-Propanethlol ND 50 ppbV 5 6/14/2011 Carbon disulfide 150 50 ppbV 5 6/1412011 Carbonyl sulfide 21 50 J ppbV 5 611412011 Dimethyl sulfide ND 50 ppbV 5 6114/2011 Ethyl mercaptan ND 50 ppbV 5 6/14/2011 Hydrogen Sulfide 1600 50 ppbV 5 6/14/2011 lsopropyl mercaptan ND 50 ppbV 5 6/14/2011 Methyl mercaptan ND 50 ppbV 5 6/14/2011 Surr: Bromofluorobenzene 125 70-130 %REC 5 6/14/2011

Qunlificrs: •• Reporting Limit Results reported nrc not blank corrected B Analytc detected in the ussociuted Method Blank E Value above quantitation runge H Holding times for preparation or analysis exceeded J Analyte detected at or below quantitntion limits JN Non~routine nnnlytc. Quantitntion estimated. ND Not Detected at the Reporting Limit S Spike Recovery outside accepted recovery limits Page 3 of3

Page 11 of 11 ATTACHMENT B-3

Catalyst Monitor System Information SHOP DRAWING: 11399-001 - 003

SPECIFICATION: 11399 TITLE: Oxidation Catalyst MANUFACTURER: General Electric PROJECT: NORTH RIVER COGENERATION & ELECTRIFICATION CONTRACTOR: NES

BLACK & VEATCH / SAVIN

NORTH RIVER COGENERATION & ELECTRIFICATION CONTRACT NR-38PS-1 FURNISH AS SUBMITTED Corrections or comments made on the shop drawings during this review do not relieve contractor from compliance with requirements of the contract documents and applicable laws, codes and regulations. This check is only for review of general conformance with the design concept of the project and general compliance with the information given in the contract documents. The contractor is responsible for confirming and correlating all quantities and dimensions; selecting fabrication processes and techniques of construction; coordinating his work with that of all other trades; and performing his work in a safe and satisfactory manner. DATE: 09/20/17 BY: KS

REVIEW COMMENTS

REF. SPEC. REVIEWER NO. COMMENTS PARA./ DWG. INITIALS 1 No Comments.. KS

END OF COMMENTS

Page 1 of 1 Northeast Energy Systems LETTER OF TRANSMITTAL Penn Power Group 8330 State Road Philadelphia, PA 19136 TEL: (215) 335-5015

DATE: September 18, 2017 JOB NO.: 2103.09

TO: Frank Giardina

NYC DEP RE: North River, WWTP : Contract NR-38PS-1

59-17 Junction Boulevard Shop Drawing Review Letter

Flushing, New York 11373 Submittal: # NR-38PS-1-11399-001 003

WE ARE SENDING YOU X ATTACHED UNDER SEPARATE COVER

QUANTITY IDENTIFYING NUMBER TITLE/DESCRIPTION

1 NR-38PS-1-11399-001 Oxi-Catalyst System

Furnish As Submitted Furnish As Corrected Revise & Resubmit

Rejected Received for Information

REMARKS: Oxidation-Catalyst System Submittal NR-38PS-1-11399-001 003

 NES Response to Savin Review  Catalyst Pressure Drop Calculation – Digester Gas  Catalyst Pressure Drop Calculation – Natural Gas  Monitor Panel Layout Diagram  Pressure Transducer Data Sheet  Catalyst Housing Diagram  Catalyst Monitor Data Sheet  Catalyst Monitor Installation & Operation manual  MSDS  Insulating Blanket Data Sheet  Thermocouple Data Sheet  Monitor Wiring Schematic

Project Name: CO-Generation Engine Generators & Gas Exhaust System Treatment Contract No.: NR38PS-1 Designated Supplier’s Name: Northeast Energy Systems Date: 18 September 2017 Items: 001 Specifications: 11399 Page No.: Para. No.: Contract Drawing Number: Location: North River WPCP Submittal No.: NR38PS-1-11399-001 Review Cycle No.: 003 Shop Drawing Reference No.: 11399-001 Component Manufacturer’s Name: HARCO Manufacturing Company Approved By: David Horowitz, Northeast Energy Systems NR-38PS-1 NES Responses to 11399-001 001 Comments 08 DEC 2015

NO. COMMENTS NES RESPONSE The Spec sheet is for Natural Gas only. Please provide the 1 specification sheet for a specification sheet for Digester Gas Amended to include Specification Sheet for Digester Gas. provided for Natural Gas 1) Exhaust temperatures are not linear with load. Unit design includes sufficient margin for temperature variations across the design exhaust temperature load spectrum. Page 43, Pressure Drop calculation inputs the "Max Bed 2) Catalyst is rated for operating temperatures through 1247 °F. (See Temperature" as 711 F however, the exhaust temperature on Catalyst Data Sheet.) DG at full load is 727. What is the exhaust temperature at part 3) Operating beyond the system design temperature (727°F) will have 2 load? Can the Catalyst survive at temperature beyond 711? minimal effect below the maximum unit rating of 1247°F temperature. What is the effect at temperature beyond the max design (See Catalyst Data Sheet.) temperature. Will the Pressure drop be the same at high 4) Design as provided is with consideration of high temperature temperature? operation. There is only a minimal pressure drop change across the operating range, unless the coatings have been shed or damaged, such as due to over-temperature (> 1247°F) operations.

3 Wire size and type not called out and who provides them. Revised wiring diagram to show wire supply and sizing.

12/18/2015 1 Customer: Boulden Energy Date Engine/Model: Jenbacher, J620F28 12/18/15

Monolithic Catalyst Pressure Drop Calculation Hegedus Hawthorn Correlation Note: THIS COLOR TEXT = INPUT DATA THIS COLOR TEXT = CACULATED DATA General Conditions Flow Rate 8,311 scfm No. of Panels/Layer 1 Max Bed Temp 727 F No. of Layers 1 Pressure 0 psig Space Velocity 145,948 hr-1

Panel Specifications Monolith Specifications

Diameter 47.3 inches Cell Density 300 cells/in2 Flow Depth 3.5 inches Cell wall thickness 0.006 inches Factor (% Area Available) 96 %

Calculated Results Disclaimer Superficial Velocity 709 ft/min @STP This sizing calculator is based on theoretical 2.46 in. H2O values; actual pressure drop can vary with 0.18 in. Hg engine and flow characteristics. It is Bed Pressure Drop 0.61 kPa designed as a guideline, but not intended to 6.14 mbar be an indicator of actual performance. 0.09 psi Customer: Boulden Energy Date Engine/Model: Jenbacher, J620F02 12/18/15

Monolithic Catalyst Pressure Drop Calculation Hegedus Hawthorn Correlation Note: THIS COLOR TEXT = INPUT DATA THIS COLOR TEXT = CACULATED DATA General Conditions Flow Rate 8,259 scfm No. of Panels/Layer 1 Max Bed Temp 714 F No. of Layers 1 Pressure 0 psig Space Velocity 145,034 hr-1

Panel Specifications Monolith Specifications

Diameter 47.3 inches Cell Density 300 cells/in2 Flow Depth 3.5 inches Cell wall thickness 0.006 inches Factor (% Area Available) 96 %

Calculated Results Disclaimer Superficial Velocity 705 ft/min @STP This sizing calculator is based on theoretical 2.40 in. H2O values; actual pressure drop can vary with 0.18 in. Hg engine and flow characteristics. It is Bed Pressure Drop 0.60 kPa designed as a guideline, but not intended to 5.99 mbar be an indicator of actual performance. 0.09 psi 4 3 2 1

4 .281 X .5 SLOT 6.75 TYP

9.375 B 8.694 B

8.375 8

1 1 4 6.438

6.375 A A NOTE: ENCLOSURE IS NEMA 4X STAINLESS STEEL. (COVER REMOVED)

1.5 1.5

TITLE 6 CATALYST MONITOR SYSTEM

DRAWN BY DATE SHEET NAM 6/3/2013 1 OF 2 4 3 2 1 Model CXLdp Differential Pressure Transmitter

APPLICATION PERFORMANCE SPECIFICATIONS Low-pressure measurement for Ref. Temperature: 70°F ±2°F (21°C ±1°C) building energy management Accuracy Class (Span): ±0.8% ±0.4% and comfort control Includes non-linearity, hysteresis, non-repeatability, zero offset and span setting errors. FEATURES Stability – Max. Change (Span/year): ≤0.25% ≤0.25% • Rugged ABS package capable of DIN Standard Ranges (Inches W.C.) rail or standard panel mounting Unidirectional Ranges: Differential • LED power status indicator to assist 0/0.10 0/0.75 0/2.50 0/10.00 in trouble shooting or quickly locating 0/0.25 0/1.00 0/3.00 0/15.00 the instrument on a duct 0/0.50 0/2.00 0/5.00 0/25.00 Bidirectional Ranges: • Detachable Euro style terminal block Compound reduces wiring errors and field wiring ±0.10 ±0.50 ±2.00 ±10.00 ±0.25 ±1.00 ±5.00 ±15.00 time Response Time: 250 msec • 19 standard pressure ranges all ENVIRONMENTAL SPECIFICATIONS Temperature Limits: capable of withstanding 15 psi with- Storage –40 to 180°F out damage or calibration change Operating +0 to 160°F 3 Compensated Range +35 to 130°F WARRANTY • Digitally compensated, 0.4% Span (10-95% R.H. non-condensing) and 0.8% Span accuracy models YEAR LOOK FOR THIS Temperature Coefficients: AGENCY MARK ON Zero & Span ±0.03% Span/°F OUR PRODUCTS • NIST traceable EMC: CE Compliant to EN61326: 1997+A1: 1998+A2: 2001 Annex A (Heavy Industrial) The Ashcroft® CXLdp transmitter uses FUNCTIONAL SPECIFICATIONS the patented Ashcroft Si-Glas™ variable Overpressure Limits: Proof Pressure 15 psid capacitance sensor. This MEMS sensor Burst Pressure 25 psid provides extraordinary sensitivity and long Max. static line pressure 25 psi term stability. New digital compensation is Mounting Position Effect: ±1%/g (lowest range) accomplished using a highly reliable Note: Calibration in vertical position is standard application specific integrated circuit (ASIC). ELECTRICAL SPECIFICATIONS Voltage Output: Supply Voltage: Supply Current: Featuring a highly reliable variable capac- 4-20mA (2 wire) 12-36 Vdc 21.5mA 0-5 Vdc (3 wire) 11.5-36 Vdc 4.5mA itance sensor using the patented 0-10 Vdc (3 wire) 14-36 Vdc or 24 Vac 6mA ® ™ Ashcroft SiGlas sensor. This ultra-thin Output signal is independent of power supply changes single crystal diaphragm provides inher- Reverse Wiring Protected ent sensor repeatability and stability. Zero and Span Adjustment: SENSOR CROSS SECTION Externally accessible Zero: ±5% F.S. Span: ±5% F.S. PHYSICAL SPECIFICATIONS Pressure Connections: 1 ⁄4˝ brass barbed fittings 1 The silicon diaphragm sensor has no glues or ⁄8 NPT Female brass other organics to contribute to drift or mechanical degradation over time. Electrical Connection: Euro style pluggable terminal block accepts 12-26 gauge wire Enclosure: NEMA Type 1 Fire-retardant ABS (meets UL 94-5VA) LED visual indicator standard Weight: Approx. 2.5 oz Media: Clean, dry and non-corrosive gas Mounting: Threaded fastener and 35mm DIN rail mount standard. 1 Option: ⁄2˝ plenum/conduit mounting bracket and cover kit (order part #101A213-01) XRH: (9 point NIST Calibration Certification)

All specifications are subject to change without notice. Ashcroft Inc., 250 East Main Street, Stratford, CT 06614 USA All sales subject to standard terms and conditions. Tel: 203-378-8281 • Fax: 203-385-0408 BULLETIN CT-6 © Ashcroft Inc. 2007 10/09 email: [email protected] • www.ashcroft.com Model CXLdp Low Pressure Differential Transmitter

DIMENSIONS (in inches) Load Limitations 4-20mA Output 1.45 Loop Resistance (Ω) .36 Ø.20 1.32 1250

1045 POWERPOWER 1000 HI LO

750 ZERO SPANSPAN 2.90 3.33 500

250 OPERATING Ø.16 REGION 1.89

LOOP RESISTANCE (OHMS) RESISTANCE LOOP 0 “MB2” 1/4 BARBED FITTINGS 0 10 12 20 30 36 40 LOOP SUPPLY VOLTAGE (VDC)

Vmin = 12V+ [.022A*(RL)] POWER *includes a 10% safety factor .56 HI LO RL =RS +RW RL = Loop Resistance (ohms) 2.90 ZERO SPAN RS = Sense Resistance (ohms) 3.33

RW = Wire Resistance (ohms)

1.89

"01" 1/8 FEMALE NPT FITTINGS

“F01” 1/8 FEMALE NPT FITTINGS

POWER

HI LO

ZERO SPAN

4.85 Standard DIN rail mount Optional 1/2˝ plenum/conduit kit

2.06

Ø.88

.78

1 ASSEMBLED WITH 101A213-01 ⁄2˝ PLENUM/CONDUIT KIT

How To Order

C X X

Pressure Range XAH** Accuracy/TC Output Conduit Kit Packaged (8) 0.8%, ±0.03%/°F Signal Diff. or Gauge: Compound: with the CXLdp (4) 0.4%, ±0.03%/°F (42) 4-20mA (P1IW) 0.10˝W.C. (P1IWL) ±0.10˝W.C. XRH (10) 0-10Vdc* (P25IW) 0.25˝W.C. (P25IWL) ±0.25˝W.C. Connection Traceable 9 Point 1 (P5IW) 0.50˝W.C. (P5IWL) ±0.50˝W.C. (MB2) ⁄4 Barbed Male Calibration Report 1 (P75IW) 0.75˝W.C. (1IWL) ±1.00˝W.C. Type (F01) ⁄8 NPT Female (CX) CXLdp (1IW) 1.00˝W.C. (2IWL) ±2.00˝W.C. (2IW) 2.00˝W.C. (5IWL) ±5.00˝W.C. (2P5IW) 2.50˝W.C. (10IWL) ±10.00˝W.C. (3IW) 3.00˝W.C. (15IWL) ±15.00˝W.C. (5IW) 5.00˝W.C. Notes: *Includes user selectable option 0-5Vdc output. (10IW) 10.00˝W.C. **Note: XAH option is for the conduit kit assembled with the CXLdp. (15IW) 15.00˝W.C. To get the conduit kit separately request Part No. 101A213-01 (25IW) 25.00˝W.C.

Figure 1 Load Limitations 4-20mA Output Follow the terminal block label markings on the ƽƽWARNING! READ CXLdp to identify the terminals; Loop Resistance (Ω) BEFORE INSTALLATION • 4-20mA Ouput: The left, negative (-), and right, positive (+) terminals are used, ignore 1. GENERAL: the center terminal which is not used. Con- A failure resulting in injury or damage may be nect the power supply positive lead to the caused by excessive overpressure, excessive vibration or pressure pulsation, excessive

instrument temperature, corrosion of the pres- TING ZERO SPAN sure containing parts, or other misuse. Con- – + sult Ashcroft Inc., Stratford, Connecticut, USA before installing if there are any questions or V = 12V+ [.022A*(R )] concerns. min L Zero adjust *includes a 10% safety factor Span adjust potentiometer potentiometer 2. OVERPRESSURE: RL =RS + RW RL = Loop Resistance (ohms) Pressure spikes in excess of the rated overpres- RS = Sense Resistance (ohms) + RW= Wire Resistance (ohms) POWER sure capability of the transducer may cause irre- + BCS –– SUPPLY versible electrical and/or mechanical damage to Loop Supply Voltage (Vdc) * F.S. pressure is equivalnt to the span of the transmitter (16mA). the pressure measuring and containing ele- CXLdp positive terminal, connect the negative ments. Reverse Wiring Protected power supply lead to the negative terminal of 3. STATIC ELECTRICAL CHARGES: Electrical Connection: unpluggable terminal block the BCS 4-20mA input. Last, connect the (-) Any electrical device may be susceptible to dam- accepts 12-26 AWG negative terminal on the CXLdp to the (+) age when exposed to static electrical charges. positive BCS input. To avoid damage to the transducer the Operating Temperature: 0-160°F operator/installer should follow proper ESD Enclosure: (electrostatic discharge) protection procedures NEMA 1 Fire-retardant ABS Meets UL 94-5VA before handling the pressure transducer. ZERO SPAN Weight: Approx. 2.5 oz. DESCRIPTION Pressure Connection Options: ® 1 The Ashcroft Model CXLdp is a low differential ⁄4˝ Brass Barbs or Zero adjust Span adjust pressure transmitter to be used on clean, dry, 1 Figure 2 ⁄8 NPT Female Brass potentiometer potentiometer non-corrosive gases. It is available in two accuracy 1 classes and its performance is traceable to the Optional: ⁄2˝ conduit or plenum mount- V U. S. National Institute of Standards and Technol- Common (V–) – Out + Vin (V+, Supply) ogy (NIST). The 8 or 4 located in the third position ing bracket and of the product code distinguishes a 0.8% from a cover available as POWER SUPPLY 0.4% accuracy transmitter. Both unidirectional separately ordered (e.g. 0 to +1.0 IW) or bi-directional (e.g. ±2.0 IW) kit – part number • 0-10Vdc; 0-5Vdc Output: Follow label mark- models are available. A green LED located on the 101A213-01. ings for terminal assignments; COM is for front of the transmitter indicates power and opera- (see Figure 2) Common (supply and output negative), VIN tional status. The LED light intensity increases as INSTALLATION is for supply positive and VOUT is for output pressure increases. signal. The CXLdp Voltage Output unit is sup- Mounting: plied as standard with 0-10 V output, to con- SPECIFICATIONS The transmitter vert to 0-5 V output see following Accuracy: (2) options,specified at time of order. Figure 3 instructions. can be mounted Use #8 • ±0.8% span on a 35 mm DIN Use or screw #10 - 0-10 Vdc Output: Product is supplied as - (±0.128mA for 4-20mA output units) rail or with #8 or screw standard with 0-10 V output, see instruction - (±0.08V for 0-10Vdc output units) #10 screws using below to access the Voltage Output jumper. or the 4 mounting • ±0.4% Span holes provided. - 0-5 Vdc Output: See below for proper - (±0.064mA for 4-20mA units) Torque limits on jumper selection. To convert the unit from a - (±0.04V for 0-10Vdc output units) the mounting 0-10 V output to a 0-5 V output unit note the holes provided is Green LED following. Access the jumper by simultane- Output Signal: Specified at time of order. ously pushing both housing tabs away from • 4-20ma (For symmetric bidirectional ranges 6 inch-pounds. Zero Pot (see Figure 3) the housing, see drawings under “General 0IW= 12mA Dimensions” for or Electrical Wiring: details. Change Figure 4 Jumper • 0-10Vdc; 0-5Vdc User selectable option (For (orange) 1. The use of sheilded cable is recommended for jumper (orange) symmetric bidirectional ranges 0IW= 5 or optimum performance. Connect the shield to the into position as 2.5Vdc respectively). 0-10 Vdc guard terminal on the reading instrument (meter, shown below, Supply Voltage: etc.) if available or to ground. carefully reattach • 4-20mA: 12-36 Vdc (no regulation required) housing cover. 2. Remove the terminal block on the front of the (see Figure 1) When finished transmitter. or mark check box • 0-10Vdc (0-5Vdc User selectable option): 3. Available electrical versions are: on front label in- 0-5 Vdc 14-36 Vdc or 24 Vac (+/- 20%) a.) CURRENT 4-20mA; black terminal block. dicating that the b.) VOLTAGE 0-5Vdc/0-10Vdc; green terminal unit now provides Label Part No. 238A713-01 • Supply Current: 6mA (4.5mA for 5Vdc block. a 0 – 5Vdc output. output option)

© 2011 Ashcroft Inc. 250 East Main Street 06614, Tel: 203-378-8281 • Fax: 203-378-0499, All specifications are subject to change without notice. All sales subject to standard terms and conditions. www.ashcroft.com All rights reserved. I&M011-10130 Rev. A 10/12 MODEL CXLdp DIFFERENTIAL PRESSURE TRANSDUCER INSTALLATION & MAINTENANCE SHEET

4. Firmly reinstall the terminal block plug to its Zero and Span Potentiometers GENERAL DIMENSIONS FOR mating connector. MODEL CXLdp (in inches) Set Up: Figure 7 ZERO SPAN 1 Note: For best immunity from EMI the pressure MB2 ⁄4˝ BARB FITTINGS "B2" 1/4 BARB FITTINGS connection fittings on the CXLdp should not be 1.45 grounded. .37 1.32 ÿ .20 The transmitters are calibrated at the factory in the Zero adjust Span adjust vertical position. Mounting in the horizontal posi- potentiometer potentiometer tion can cause a zero shift of as much as ±1% F.S. POWER in ranges below 1 W dp. Any minor zero offset can I Routine Maintenance: HI LO be minimized using the zero adjust potentiometer located on the front, left side of the instrument. The CXLdp is a very stable and reliable transmitter ZERO SPAN incorporating a proven, micro-machined silicon ca- 2.90 3.33 To find true zero differential pressure, pneumati- pacitive sensor and a new, state-of-the-art applica- cally connect the high and low pressure connection specific integrated circuit (ASIC). tions together using the tubing provided with the All calibration and temperature compensation func- ÿ .16 transmitter. The HOUSING TABS (2) tions are done with a microprocessor and 1.89 barbed connection Figure 5 digital routines. 1 1 accept ⁄4˝ O.D. ⁄8˝ I.D. tubing. To troubleshoot or verify performance, it is recom- 1 mended to pneumatically connect the pressure F01 ⁄8 NPT FEMALE FITTINGS (see Figure 5) "01" 1/8 FEMALE NPT FITTINGS ports to each other and establish a zero offset 1 1.45 When ⁄8 NPT fe- reading in the as-installed position. Adjusting zero .37 1.32 male brass fittings will not affect span calibration. are used, do not exceed 60 inch- Adjusting span should only be attempted when a POWER pound torque force high accuracy pressure standard and high quality .56 on female NPT fit- electrical meter are able to be used. HI LO ting. Figure 6 DIN Rail Transmitter Removal:

ZERO SPAN When connecting to In order to remove the transmitter when it is installed 2.90 3.33 the NPT fittings, do on a DIN rail, it is necessary to first unplug the wiring not apply torque to terminal block from the transmitter. the CXLdp fitting. 9 Insert a small slot- Use a ⁄16˝ wrench to 1.89 Figure 8 hold the CXLdp. ted screwdriver into (see Figure 6) the black plastic clip extending 3 ASSEMBLED WITH 101A213-01 Zero potentiometer adjustment requires using a ⁄32˝ slightly below the or 2.5 mm slotted or phillips screwdriver. The tub- transmitter case. CONDUIT KIT ASSEMBLED WITH 101A213-01 CONDUIT KIT ing should remain in place until the transmitter is (see Figure 8) to be connected to the BCS tubing system. (see Figure 7) Next, raise the screwdriver handle up thereby forcing the spring clip down. If questions or concerns need to be addressed, our Low Pressure Product Manager or Engineering Personnel can be contacted at (203) 378-8281 or 4.85 visit our website at www.ashcroft.com.

2.06

R .88

..7878

3.5 17.5 25.25 17.5 3.5 BODY 28.6~ C LENGTH LG 9.98 ----,---0 0 0 0 I A A ¢24

A A .05 54.568 ------~

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Catalyst Monitor

6 Channel Monitor / Data Logger

Designed for catalyst monitoring and data logging on Spark Ignited and Diesel engines.

• NSCR (3-way) & Oxidation (2-way) type catalysts

The following parameters are monitored:

• Catalyst Inlet / Outlet Temperatures plus Differential

• Catalyst Inlet / Outlet Pressures plus Differential

• Left Bank / Right Bank O2 Sensor Outputs for ensuring proper AFRC operation

• Engine Hours (5-digit non-resettable)

• Engine Speed

• Can be configured to alarm if inlet temperature out of compliance

• On-Board Data Logging of thousands of values with time / date stamp

Monitors catalyst inlet temperature based on 4 hour rolling average per RICE NESHAP requirements – data is saved to non-volatile flash memory

• Modbus RS-485 Communications Protocol for communications w/ SCADA or DCS

• CSA Class I, Division 2 Groups A, B, C & D approved • Fully programmable from front keypad

• High capacity on board flash memory

• Power loss will not erase memory

• Log Reader software allows data download to PC with USB cable p/n 270A-13020

Date EventID Value 1/13/20128:25 0 1075 1/13/20128:10 0 1072 1/13/20127:55 0 1070 1/13/20127:40 0 1078 1/13/20127:25 0 1078 1/13/20127:10 0 1080 1/13/20126:55 0 1078 1/13/20126:40 0 1085 1/13/20126:25 0 1082 1/13/20126:10 0 1078 1/13/20125:55 0 1079 SPECIFICATIONS 1/13/20125:40 0 1080 1/13/20125:25 0 1070 Electrical: 1/13/20125:10 0 1076 1/13/20124:55 0 1082 1/13/20124:40 0 1081 Supply Voltage: 10 – 36 VDC 1/13/20124:25 0 1079 1/13/20124:10 0 1075 Input Types: J, K type thermocouple 1/13/20123:55 0 1078 4 – 20 mA 1/13/20123:40 0 1080 0 – 1 VDC 0 – 5 VDC 0 – 10 VDC

Plus (1) pulsed input for RPM display

Output Type: (2) digital outputs rated 0.15 A @ 48 VDC

Scan Rate: All channels scanned in 100 milli-seconds

Accuracy: 0.2%

Mechanical:

¼ DIN package (3 ½” width X 3 ½” height) for panel mount

Splash-proof front panel

Removable connectors on back of enclosure

5450 NW 33rd Ave, Suite 104, Fort Lauderdale, FL 33309 Phone: 954-739-4300 Fax: 954-486-4968 www.dynalco.com 5450 NW 33rd Ave, Suite 104 Fort Lauderdale, FL 33309

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Published: December 4, 2013 IMPORTANT - PLEASE READ BEFORE PROCEEDING!

This manual applies to all Version2 Catalyst Monitors.

The Dynalco Catalyst Monitor is designed for reliable and rugged operation on engines with NSCR and oxidation catalysts. This product has been designed and tested to meet the demands required in many industrial and hazardous locations meeting critical CSA standards. The performance is directly related to the quality of the installation and knowledge of the user in operating and maintaining the instrument. To ensure continued operation to the design specifications, personnel should read this manual thoroughly before proceeding with installation, operation and maintenance of this instrument. If this product is used in a manner not specified by Dynalco, the protection provided by it against hazards may be impaired.

WARNING

• Failure to follow proper instructions may cause any one of the following situations to occur: Loss of life; personal injury; property damage; damage to this instrument; and warranty invalidation.

• For clarification of instructions in this manual or assistance with your application, contact Dynalco at (800) 368-6666 or (954) 739-4300 or send email to [email protected]

• Additional manuals and CSA certificates are available at www.dynalco.com

• Follow all warnings, cautions, and instructions marked on and supplied with the product.

• Use only qualified personnel to install, operate, program and maintain the product.

• Educate your personnel in the proper installation, operation, and maintenance of the product.

• Install equipment as specified in the installation section of this manual. Follow appropriate local and national codes. Only connect the product to power sources and end devices specified in this manual.

• Any repair is only to be performed by Dynalco using factory documented components. Tampering or unauthorized substitution of parts and procedures can affect the performance and cause unsafe operation of your process.

• All equipment doors must be closed and protective covers must be in place unless qualified personnel are performing maintenance.

• Shutdown / alarms should be tested monthly for proper operation (see page 14)

• Please see page 22 for CSA specific installation instructions.

System Overview

The Dynalco Catalyst Monitor is designed to address the RICE NESHAP mandate regarding continuous monitoring of catalyst inlet temperature and differential pressure on both spark- ignited and diesel engines. It is capable of reading up to 6 input channels, calculating differential values, providing alarm / shutdown outputs as well as allowing all parameters to be logged to an internal flash memory. An RS-485 Modbus link for communications to a DCS or PLC is also provided.

Additionally, the Catalyst Monitor is capable of calculating the engine catalyst inlet temperature based on a 4 hour rolling average per RICE NESHAP requirements.

Basic operation:

The Catalyst Monitor will be in “stopped” mode until a run indication is sensed. This is selectable as either a contact closure or magnetic pickup input. Once “running” mode is sensed, the Catalyst Monitor will read all inputs at a rate of 100 msec per channel. If any input crosses either an over or under threshold, the unit will invoke a flashing red LED on the front panel as well as an output trip (solid-state relay) that can be used for alarm or shutdown. Any trips will also cause the Catalyst Monitor to date / time stamp whenever a trip threshold is crossed. The monitor will log the last (10) events for each channel input.

Data Logging:

The Catalyst Monitor also allows data logging of any monitored values where they will be saved to an internal flash memory. Memory is sufficient to hold up to 500,000 data values with date / time stamp. These values can be downloaded at any time to a PC using Dynalco’s download cable and Log Reader software.

Additional Features

• 5 - Digit Hourmeter Function (non-resettable)

• Engine RPM Display

• Fully programmable from front keypad

• ¼ DIN package (3 ½” width X 3 ½” height) for panel mount

2 Specifications

Input Types J or K type thermocouple (ungrounded) accurate to +/- 0.2 % 4 - 20 mA 0 – 1 VDC 0 - 5 VDC 0 – 10 VDC Digital Input Closure to ground indicates run condition (or use pulsed input) Pulsed Input Magnetic pickup input for RPM display & to indicate run condition Relay Outputs 2 Digital Outputs rated @ 0.15 A / 48 VDC Input Power 10 – 36 VDC Display Backlit Graphic Display Data Logging Internal Flash Memory to retain data logged values w/ date & time stamp Communications Modbus Connections Two-Part Terminal Blocks Operating Temperature Range - 40 to + 70 Deg C Certification CSA Class I, Division 2, Groups A, B, C, D

User Interface

The Catalyst Monitor is configured via the keypad on the front panel which includes a graphical backlit LCD display capable of displaying alpha numeric values and custom engineering units of measure. The keypad implements a menu system, which is navigated using the up, down, left, right, enter and escape buttons.

Installation:

The Catalyst Monitor is a standard ¼ DIN package, designed to be panel mounted. The cutout dimensions are shown below.

3 The Catalyst Monitor has integral mounting clips for securing into the panel. The following drawings illustrate the mounting procedure.

4 Terminal Connections

All connections are made via the removable connectors on the back of the unit.

PIN Description PIN Description 1 GND (Power Gnd) 13 Channel 1 (-) 2 VIN (10 - 36 VDC input) 14 Channel 1 (+) 3 GND (mag pickup input) 15 Channel 2 (-) 4 RPM + (mag pickup input) 16 Channel 2 (+) 5 Receive Data (-) 17 Channel 3 (-) 6 Receive Data (+) 18 Channel 3 (+) 7 Transmit Data (-) 19 Channel 4 (-) 8 Transmit Data (+) 20 Channel 4 (+) 9 Alarm 1 21 Channel 5 (-) 10 Alarm 1 22 Channel 5 (+) 11 Alarm 2 23 Channel 6 (-) 12 Alarm 2 24 Channel 6 (+)

Also used for USB download cable assembly p/n 270A-13020 (see page 15)

Terminal screws to be tightened to 4 inch-pounds torque.

See page 21 for complete wiring information.

5 Outline Dimensions

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6 Programming Overview

All programming is accomplished through the front keypad. Below is a brief description of each key.

Press to enter or exit the configuration screens

Press to enter or accept values

Select up

Select down

Go back one screen

Select and advance to next screen

Initial configuration consists of the following steps:

1) Setting current date / time

2) Enabling each input

3) Defining each input type

4) Defining min. & max. display values for any current or voltage inputs

5) Defining measurement display units (PSI, mV, F, C, H20, etc)

6) Setting over / under setpoint trips

7) Selecting either output 1 or output 2 (or both) for alarm trips

8) Setting either latching or non-latching for output trips

9) Defining data logging events

7 Programming Instructions

Important: The Catalyst Monitor must first be programmed prior to operation.

When initially powering up the unit, the display will first indicate the firmware version and then go to the operational mode. It may also display a screen warning that the time & date need to be entered. This will be explained below.

To configure the Catalyst Monitor, first go to the main programming screen by pressing the Menu / Escape key:

The following menu icons will appear from left to right:

Run Signal - defines run status input type (if any)

Channel - enables each channel type and alarm thresholds

Calibration - defines zero & span values for DCV & mA inputs

Alarm Settings - for setting high /low alarm thresholds

Alarm Logs - allows the user to view alarm status

Communication - Log Reader / Modbus setup

Data Logging - allows configuration of up to (10) different logging events

System - allows display customization & current date / time input

8 A description of each menu item follows:

“Run Signal”

There are (3) run types available. The definitions are as follows:

None: No run indication required. Monitoring is always active. RPM: Monitoring is active when signal received from magnetic pickup. Digital: Monitoring is active when contact closure (connection to ground) is sensed.

To select run signal type, use the up / down arrows to select, then press the right arrow to accept and advance to the next screen.

If “None” is selected, there is no other action required other than to select “escape.” After selecting escape, you will be asked to select “yes” to save.

If “RPM” is selected, you will need to set the # gear teeth, RPM threshold and startup delay. The RPM threshold is the speed above which monitoring will be active. The startup delay can be configured to delay monitoring if desired, allowing time for all inputs to be at normal levels. If no delay is required, set to 0 seconds. The magnetic pickup input terminals are indicated on page 5.

If “Digital” is selected, you will only need to set the startup delay (if applicable). In this mode, a run signal will be sensed with a contact closure (or short) between the magnetic pickup input terminals indicated on page 5.

Pressing at any time during configuration will prompt you to save the changes. Select “Yes” to save any changes made. Selecting “No” will not save changes.

“Channel”

Select the channel number to configure by pressing the up / down arrows, then pressing the right arrow to navigate and select the following:

Enable Channel Yes / No Channel Type 0-1 V, 0-5 V, 0-10 V, 4-20 mA, J Type, K Type Description name input with up to 20 characters Engineering Units up to 3 characters, for example: PSI, mV, F, C etc… Note: For thermocouple inputs, you must enter either “F” or “C”

Differential calculations between channels 1&2, 3&4, 5&6 are also enabled by selecting the “Channel” icon. Enable “Differential 1” for channels 1&2, “Differential 2” for channels 3&4 and “Differential 3” for channels 5&6.

9 ”Calibration”

Select the channel number to configure by pressing the up / down arrows and pressing the right arrow to select and continue.

The screens allow you to define the “Cal Zero” and “Cal Span” values for any channels that are configured for 0-1 V, 0-5 V, 0-10 V or 4-20 mA inputs.

Example

A pressure transmitter is connected to channel # 1. The transmitter has a 4-20 mA output representing a pressure input of 0 - 500 PSI. The “Cal Zero” and “Cal Span” values would be defined as:

Cal Zero = 0 Cal Span = 500

Note that the “Engineering Units” would be input as PSI in “Channel” configuration above.

“Alarm Settings”

Select the channel number to configure by pressing the up / down arrows, then pressing the right arrow to navigate and select the following:

Enable alarms Yes / No Alarm Type Latching / Non-Latching Alarm Output None / Output 1 / Output 2 / Output 1 and 2 Alarm Low threshold for under-trip Alarm High threshold for over-trip Alarm Reset Points Set Defaults / Set Manually If “Set Manually” is selected, 2 more screens follow: Alarm Reset Low manually set reset hysteresis for low trip Alarm Reset High manually set reset hysteresis for high trip

“Alarm Logs”

Selecting the “Alarm Logs” icon will allow you to view any active alarms as well as the history log for each channel. Select any channel number by pressing the up / down arrows. Then press the right arrow to view any active or logged alarms. Once an active alarm is acknowledged, it will be placed into the history log. The history log will continuously store the last 10 alarms for each channel as well as the time & date of each alarm occurrence.

“Communication”

This allows configuration for downloading data and Modbus communications.

10 ”Data Logging”

The Catalyst Monitor can be configured to log any of the parameters being monitored, at user defined time intervals. The values are saved to an internal flash memory with sufficient memory to hold up to 500,000 data values with date / time stamps. These values can be downloaded at any time to a PC using Dynalco’s “Log Reader” software.

The logging of any parameter is configured as an event. The Catalyst Monitor will allow up to (10) individual events to be defined.

For the RICE NESHAP requirement, the catalyst inlet temperature (based on the 4 hour rolling average) is to be logged at 15 minute intervals while the engine is running. An event can be configured to comply with this mandate.

It’s also possible to configure another event that will log the catalyst differential pressure at defined intervals. Note that some users may decide to manually record differential pressure once per month since this value needs to be recorded with engine fully loaded per RICE NESHAP.

Example # 1:

To configure data logging of catalyst inlet temperature every 15 minutes:

Using the arrows on the keypad, select the “Data Logging” icon.

Next, select “Setup Log Events” and press the arrow.

The next screen will display a list of (10) events that can be configured. If this is the first event to be programmed, select “Event 1” and press the arrow.

Next select “Enable” and press the arrow.

The next screen allows you to define an “On” condition. The configuration for logging the inlet temperature does not require this since the “On” condition is normally defined by an “engine run” signal. See above (page 9) for the procedure for configuring the “run” signal. In this case, select “No” and press the arrow.

The next screen named “Input To Log” allows the user to select which parameter to log. Using the up / down arrows, select the input channel that is set up to monitor the catalyst inlet temperature. Press arrow.

The next screen named “Log Frequency” allows the configuration of how often (in minutes) the value is to be logged. Press enter and edit for 15 minutes. Selecting escape will return to the “Log Frequency” screen. Press the arrow and then select “Yes” to save the changes. Pressing the escape key two times will escape to the normal monitoring mode.

11 Example # 2:

To configure data logging of catalyst differential pressure after engine warm up:

(Note that this configuration will require an input signal from a magnetic pickup to sense engine running.)

Using the arrows on the keypad, select the “Data Logging” icon.

Next, select “Setup Log Events” and press the arrow.

The next screen will display a list of (10) events that can be configured. If this is the second event to be programmed, select “Event 2” and press the arrow.

Next select “Enable” and press the arrow.

The next screen allows you to define an “On” condition. The configuration for logging the differential pressure will require an “On” condition defined by an “engine run” signal. See above (page 9) for the procedure for configuring the “run” signal. In this case, select “Yes” and press the arrow.

Select “Edit Compare” on the next screen and press the arrow.

Select “Compare 1” on the next screen and press the arrow.

Select “RPM” on the next screen and press the arrow.

Select “Greater Than” on the next screen and press the arrow.

Select “A Value” on the next screen and press the arrow.

On the following screen, select an RPM value that will indicate engine running. This value should be lower than the normal engine running speed and higher than the RPM defined as the “run” signal in page 9.

The next screen will ask if you want to “Edit Another?” Select “no” and press the arrow.

Press the arrow (3) more times until the screen appears as “Enter ON Delay.” Enter this number as the time delay (in seconds) following engine start when you would like to log the catalyst differential pressure. The maximum value configurable is 3600 seconds (60 minutes.) After entering the time delay, press arrow.

The next screen allows you to define an “Off” condition. In this case, select “No” and press the arrow.

The next screen named “Input To Log” allows the user to select which parameter to log. Using the up / down arrows, select the input that is defined as the catalyst differential pressure. Press arrow.

12 The next screen named “Log Frequency” allows the configuration of how often (in minutes) the value is to be logged. Entering 0 minutes will allow only (1) data log event following the start delay. If you wanted to continuously log the differential pressure, you would select the frequency in minutes between data logs. Selecting escape will return to the “Log Frequency” screen.

Press the arrow and then select “Yes” to save the changes.

Pressing the escape key two times will escape to the normal monitoring mode.

“System”

“Display defaults” allows the selection of either single channel (absolute) or differential value display. Note that regardless of this setting, pressing the right or left arrow during normal operation will display the alternate display type.

“Digital output” allows the configuration of the solid state relay alarm outputs as either “Normally Open” or “Normally Closed”

“EPA enable” is used to enable a 4-hour rolling average calculation (a RICE NESHAP requirement) of the catalyst inlet temperature. Select whichever channel is configured to monitor the catalyst inlet temperature. On Catalyst Monitors with optional dual-bank monitoring, you will be able to select (2) channels with this function.

“Set date and time” is self-explanatory but is important for proper date / time stamps for both alarm logs and data logging.

IMPORTANT NOTICE REGARDING CORRECT DATE / TIME SETTING:

The correct date / time is imperative for proper data logging.

Please note that the date and time may need to be re-programmed if the Catalyst Monitor loses input power for over 1 week. This will be indicated by a warning upon powering up the unit.

Note that only the date / time may be affected by extended loss of power. Any data logged to the internal flash memory will be held indefinitely.

13 Alarm Outputs

The Catalyst Monitor will alarm when channel values or differential values are above or below limits as specified. Alarms can be configured as either latching or non-latching. If an alarm condition is met, the red LED on the front panel will blink and the digital output(s) will trip. The alarm point name (ch1, ch2, df1, df2) that caused the alarm will be stored in memory with date/time stamp info. Non-latching alarms will reset the alarm if its value returns to normal. Latching alarms require manual resetting via the front keypad.

WARNING:

The alarm / shutdown output should be tested monthly for proper operation, especially if being used for engine overspeed shutdown or other critical function.

Catalyst Inlet Temperature Monitoring (per RICE NESHAP requirements)

The Catalyst Monitor will allow you to configure any one channel to monitor the catalyst inlet temperature based on a 4 hour rolling average per the RICE NESHAP mandate. To set this up, first go to the main menu, then select “System.” Select “EPA enable” and then select which channel is monitoring the catalyst inlet temperature. Please note that once this is configured, the channel representing the catalyst inlet temperature will always display the 4 hour average, not instantaneous exhaust temperature. This temperature is only updated every 15 minutes per NESHAP requirements. See also “System” section on page 13.

Following this, selecting the “Alarm Settings” icon in the main menu screen will allow over and under temperature alarms to be set according to the mandate. (see page 10)

IMPORTANT NOTICE REGARDING POWER INTERRUPTION:

If input power to the Catalyst Monitor is disconnected or lost during a data log operation, there is a possibility of losing the last few values stored.

To prevent this, it is important to turn off the data logging prior to power disconnect. This is accomplished through the “Data Logging” icon on the main menu. When this is selected, the first screen will allow you to select “Stop Logging.” Pressing the arrow will provide instructions for a safe power down.

The data logging will be enabled automatically when power is re-applied.

14 Downloading logged values to PC:

The hardware connection from the Catalyst Monitor to a PC is via a USB cable assembly, Dynalco p/n 270A-13020. The 6 ft cable length allows easy connection via a 4 pin Phoenix plug to the lower connector (terminals 5, 6, 7, 8) on the back of the Catalyst Monitor. When initially plugging the download cable into the PC’s USB port, the new device should be recognized and the driver installed automatically.

Please call (954) 739-4300 if the driver is not installed properly or assistance is required.

The Dynalco host software is available as a free download from our website: www.dynalco.com/downloads

There are (2) versions available:

LogReader Ver. 1 Use for Version 1 Catalyst Monitors

LogReader ver. 2 Use for Version 2 Catalyst Monitors

Following installation, you may click on the icon to open the application. This software will allow date selectable log values to be downloaded to an excel spread sheet on the PC.

15 Modbus Communication

The unit also provides access to the internal registered values using the Modbus Protocol. The diagram below shows the recommended connections to the removable connectors on the back of the unit for either half-duplex or full-duplex (RS485).

Wiring is as follows:

PIN Description 5 TD(A) ** 6 TD(B) ** 7 Jumper to PIN 5 8 Jumper to PIN 6

** A 120 ohm termination resistor may need to be installed across pins 5 & 6.

16 Modbus Address Registers:

The Modbus address registers are defined in the tables below.

Input Register Table (table 1)

DŽĚŝĐŽŶ DŽĚďƵƐ ĞƐĐƌŝƉƚŝŽŶ DŝŶsĂůƵĞ DĂǆ ĂƚĂƚǇƉĞ ĚĚƌĞƐƐ KĨĨƐĞƚ sĂůƵĞ ϯϬϬϬϬϭ Ϭ ^ƚĂƚƵƐZĞŐŝƐƚĞƌ͕ϬсŶŽƚƌƵŶŶŝŶŐ͕ Ϭ ϭ ϭϲďŝƚƐŝŐŶĞĚŝŶƚĞŐĞƌ ϭсƌƵŶŶŝŶŐ͘ ϯϬϬϬϬϮ ϭ ZĞƐĞƌǀĞĚ ͲϯϮϳϲϴ ϯϮϳϲϴ ϭϲďŝƚƐŝŐŶĞĚŝŶƚĞŐĞƌ ϯϬϬϬϬϯ Ϯ ůĂƌŵƐ ŝƚŵĂƐŬ ŝƚϬͲŚĂŶŶĞůϭůĂƌŵ Ϭ ϭ ϬϬϬϭŚ ŝƚϭͲŚĂŶŶĞůϮůĂƌŵ Ϭ ϭ ϬϬϬϮŚ ŝƚϮͲŚĂŶŶĞůϯůĂƌŵ Ϭ ϭ ϬϬϬϰŚ ŝƚϯͲŚĂŶŶĞůϰůĂƌŵ Ϭ ϭ ϬϬϬϴŚ ŝƚϰͲŚĂŶŶĞůϱůĂƌŵ Ϭ ϭ ϬϬϭϬŚ ŝƚϱͲŚĂŶŶĞůϲůĂƌŵ Ϭ ϭ ϬϬϮϬŚ ŝƚϲͲŚĂŶŶĞůϭͲϮŝĨĨĞƌĞŶƚŝĂů Ϭ ϭ ϬϬϰϬŚ ůĂƌŵ ŝƚϳͲŚĂŶŶĞůϯͲϰŝĨĨĞƌĞŶƚŝĂů Ϭ ϭ ϬϬϴϬŚ ůĂƌŵ ŝƚϴͲŚĂŶŶĞůϱͲϲŝĨĨĞƌĞŶƚŝĂů Ϭ ϭ ϬϭϬϬŚ ůĂƌŵ ŝƚϵͲƌĞƐĞƌǀĞĚ Ϭ ϭ ϬϮϬϬŚ ŝƚϭϬͲƌĞƐĞƌǀĞĚ Ϭ ϭ ϬϰϬϬŚ ŝƚϭϭͲƌĞƐĞƌǀĞĚ Ϭ ϭ ϬϴϬϬŚ ŝƚϭϮͲƌĞƐĞƌǀĞĚ Ϭ ϭ ϭϬϬϬŚ ŝƚϭϯʹƌĞƐĞƌǀĞĚ Ϭ ϭ ϮϬϬϬŚ ŝƚϭϰʹƌĞƐĞƌǀĞĚ Ϭ ϭ ϰϬϬϬŚ ŝƚϭϰʹƌĞƐĞƌǀĞĚ Ϭ ϭ ϴϬϬϬŚ ϯϬϬϬϬϰ ϯ ŚĂŶŶĞůϭsĂůƵĞ ͲϯϮϳϲϴ ϯϮϳϲϳ ϭϲďŝƚƐŝŐŶĞĚŝŶƚĞŐĞƌ ϯϬϬϬϬϱ ϰ ŚĂŶŶĞůϮsĂůƵĞ ͲϯϮϳϲϴ ϯϮϳϲϳ ϭϲďŝƚƐŝŐŶĞĚŝŶƚĞŐĞƌ ϯϬϬϬϬϲ ϱ ŚĂŶŶĞůϯsĂůƵĞ ͲϯϮϳϲϴ ϯϮϳϲϳ ϭϲďŝƚƐŝŐŶĞĚŝŶƚĞŐĞƌ ϯϬϬϬϬϳ ϲ ŚĂŶŶĞůϰsĂůƵĞ ͲϯϮϳϲϴ ϯϮϳϲϳ ϭϲďŝƚƐŝŐŶĞĚŝŶƚĞŐĞƌ ϯϬϬϬϬϴ ϳ ŚĂŶŶĞůϱsĂůƵĞ ͲϯϮϳϲϴ ϯϮϳϲϳ ϭϲďŝƚƐŝŐŶĞĚŝŶƚĞŐĞƌ ϯϬϬϬϬϵ ϴ ŚĂŶŶĞůϲsĂůƵĞ ͲϯϮϳϲϴ ϯϮϳϲϳ ϭϲďŝƚƐŝŐŶĞĚŝŶƚĞŐĞƌ ϯϬϬϬϭϬ ϵ ŚĂŶŶĞůϭĂŶĚϮŝĨĨĞƌĞŶƚŝĂůsĂůƵĞ ͲϯϮϳϲϴ ϯϮϳϲϳ ϭϲďŝƚƐŝŐŶĞĚŝŶƚĞŐĞƌ ϯϬϬϬϭϭ ϭϬ ŚĂŶŶĞůϯĂŶĚϰŝĨĨĞƌĞŶƚŝĂůsĂůƵĞ ͲϯϮϳϲϴ ϯϮϳϲϳ ϭϲďŝƚƐŝŐŶĞĚŝŶƚĞŐĞƌ ϯϬϬϬϭϮ ϭϭ ŚĂŶŶĞůϱĂŶĚϲŝĨĨĞƌĞŶƚŝĂůsĂůƵĞ ͲϯϮϳϲϴ ϯϮϳϲϳ ϭϲďŝƚƐŝŐŶĞĚŝŶƚĞŐĞƌ ϯϬϬϬϭϯ ϭϮ ŚĂŶŶĞůϭ,ŝŐŚůĂƌŵ>ŝŵŝƚ ͲϯϮϳϲϴ ϯϮϳϲϳ ϭϲďŝƚƐŝŐŶĞĚŝŶƚĞŐĞƌ ϯϬϬϬϭϰ ϭϯ ŚĂŶŶĞůϮ,ŝŐŚůĂƌŵ>ŝŵŝƚ ͲϯϮϳϲϴ ϯϮϳϲϳ ϭϲďŝƚƐŝŐŶĞĚŝŶƚĞŐĞƌ ϯϬϬϬϭϱ ϭϰ ŚĂŶŶĞůϯ,ŝŐŚůĂƌŵ>ŝŵŝƚ ͲϯϮϳϲϴ ϯϮϳϲϳ ϭϲďŝƚƐŝŐŶĞĚŝŶƚĞŐĞƌ ϯϯϬϬϭϲ ϭϱ ŚĂŶŶĞůϰ,ŝŐŚůĂƌŵ>ŝŵŝƚ ͲϯϮϳϲϴ ϯϮϳϲϳ ϭϲďŝƚƐŝŐŶĞĚŝŶƚĞŐĞƌ

17 ϯϬϬϬϭϳ ϭϲ ŚĂŶŶĞůϱ,ŝŐŚůĂƌŵ>ŝŵŝƚ ͲϯϮϳϲϴ ϯϮϳϲϳ ϭϲďŝƚƐŝŐŶĞĚŝŶƚĞŐĞƌ ϯϬϬϬϭϴ ϭϳ ŚĂŶŶĞůϲ,ŝŐŚůĂƌŵ>ŝŵŝƚ ͲϯϮϳϲϴ ϯϮϳϲϳ ϭϲďŝƚƐŝŐŶĞĚŝŶƚĞŐĞƌ ϯϯϬϬϭϵ ϭϴ ŚĂŶŶĞůϭĂŶĚϮŝĨĨĞƌĞŶƚŝĂů,ŝŐŚ ͲϯϮϳϲϴ ϯϮϳϲϳ ϭϲďŝƚƐŝŐŶĞĚŝŶƚĞŐĞƌ ůĂƌŵ>ŝŵŝƚ ϯϬϬϬϮϬ ϭϵ ŚĂŶŶĞůϯĂŶĚϰŝĨĨĞƌĞŶƚŝĂů,ŝŐŚ ͲϯϮϳϲϴ ϯϮϳϲϳ ϭϲďŝƚƐŝŐŶĞĚŝŶƚĞŐĞƌ ůĂƌŵ>ŝŵŝƚ ϯϬϬϬϮϭ ϮϬ ŚĂŶŶĞůϱĂŶĚϲŝĨĨĞƌĞŶƚŝĂů,ŝŐŚ ͲϯϮϳϲϴ ϯϮϳϲϳ ϭϲďŝƚƐŝŐŶĞĚŝŶƚĞŐĞƌ ůĂƌŵ>ŝŵŝƚ ϯϬϬϬϮϮ Ϯϭ ŚĂŶŶĞůϭ>ŽǁůĂƌŵ>ŝŵŝƚ ͲϯϮϳϲϴ ϯϮϳϲϳ ϭϲďŝƚƐŝŐŶĞĚŝŶƚĞŐĞƌ ϯϬϬϬϮϯ ϮϮ ŚĂŶŶĞůϮ>ŽǁůĂƌŵ>ŝŵŝƚ ͲϯϮϳϲϴ ϯϮϳϲϳ ϭϲďŝƚƐŝŐŶĞĚŝŶƚĞŐĞƌ ϯϬϬϬϮϰ Ϯϯ ŚĂŶŶĞůϯ>ŽǁůĂƌŵ>ŝŵŝƚ ͲϯϮϳϲϴ ϯϮϳϲϳ ϭϲďŝƚƐŝŐŶĞĚŝŶƚĞŐĞƌ ϯϬϬϬϮϱ Ϯϰ ŚĂŶŶĞůϰ>ŽǁůĂƌŵ>ŝŵŝƚ ͲϯϮϳϲϴ ϯϮϳϲϳ ϭϲďŝƚƐŝŐŶĞĚŝŶƚĞŐĞƌ ϯϬϬϬϮϲ Ϯϱ ŚĂŶŶĞůϱ>ŽǁůĂƌŵ>ŝŵŝƚ ͲϯϮϳϲϴ ϯϮϳϲϳ ϭϲďŝƚƐŝŐŶĞĚŝŶƚĞŐĞƌ ϯϬϬϬϮϳ Ϯϲ ŚĂŶŶĞůϲ>ŽǁůĂƌŵ>ŝŵŝƚ ͲϯϮϳϲϴ ϯϮϳϲϳ ϭϲďŝƚƐŝŐŶĞĚŝŶƚĞŐĞƌ ϯϬϬϬϮϴ Ϯϳ ŚĂŶŶĞůϭĂŶĚϮŝĨĨĞƌĞŶƚŝĂů>Žǁ ͲϯϮϳϲϴ ϯϮϳϲϳ ϭϲďŝƚƐŝŐŶĞĚŝŶƚĞŐĞƌ ůĂƌŵ>ŝŵŝƚ ϯϬϬϬϮϵ Ϯϴ ŚĂŶŶĞůϯĂŶĚϰŝĨĨĞƌĞŶƚŝĂů>Žǁ ͲϯϮϳϲϴ ϯϮϳϲϳ ϭϲďŝƚƐŝŐŶĞĚŝŶƚĞŐĞƌ ůĂƌŵ>ŝŵŝƚ ϯϬϬϬϯϬ Ϯϵ ŚĂŶŶĞůϱĂŶĚϲŝĨĨĞƌĞŶƚŝĂů>Žǁ ͲϯϮϳϲϴ ϯϮϳϲϳ ϭϲďŝƚƐŝŐŶĞĚŝŶƚĞŐĞƌ ůĂƌŵ>ŝŵŝƚ ϯϬϬϬϯϭ ϯϬ ZWD Ϭ ϲϱϱϯϱ ϭϲďŝƚƵŶƐŝŐŶĞĚŝŶƚĞŐĞƌ ϯϬϬϬϯϮ ϯϭ ZĞŐŝƐƚĞƌdĂďůĞsĞƌƐŝŽŶ Ϭ ϲϱϱϯϱ ϭϲďŝƚƵŶƐŝŐŶĞĚŝŶƚĞŐĞƌ ϯϬϭϬϬϮͲ ϭϬϬϭͲ >ŽŐƵĨĨĞƌŶƚƌǇηϭ ƵƐƚŽŵ;^ĞĞƚĂďůĞϰͿ ϯϬϭϬϬϱ ϭϬϬϰ ϯϬϭϬϬϲͲ ϭϬϬϱͲ >ŽŐƵĨĨĞƌŶƚƌǇηϮ ƵƐƚŽŵ;^ĞĞƚĂďůĞϰͿ ϯϬϭϬϬϵ ϭϬϬϴ ϯϬϭϬϭϬͲ ϭϬϬϵͲ >ŽŐƵĨĨĞƌŶƚƌǇηϯ ƵƐƚŽŵ;^ĞĞƚĂďůĞϰͿ ϯϬϭϬϭϯ ϭϬϭϮ ϯϬϭϬϭϰͲ ϭϬϭϯͲ >ŽŐƵĨĨĞƌŶƚƌǇηϰ ƵƐƚŽŵ;^ĞĞƚĂďůĞϰͿ ϯϬϭϬϭϳ ϭϬϭϲ ϯϬϭϬϭϴͲ ϭϬϭϳͲ >ŽŐƵĨĨĞƌŶƚƌǇηϱ ƵƐƚŽŵ;^ĞĞƚĂďůĞϰͿ ϯϬϭϬϮϭ ϭϬϮϬ ϯϬϭϬϮϮͲ ϭϬϮϭͲ >ŽŐƵĨĨĞƌŶƚƌǇηϲ ƵƐƚŽŵ;^ĞĞƚĂďůĞϰͿ ϯϬϭϬϮϱ ϭϬϮϰ ϯϬϭϬϮϲͲ ϭϬϮϱͲ >ŽŐƵĨĨĞƌŶƚƌǇηϳ ƵƐƚŽŵ;^ĞĞƚĂďůĞϰͿ ϯϬϭϬϮϵ ϭϬϮϴ ϯϬϭϬϯϬͲ ϭϬϮϵͲ >ŽŐƵĨĨĞƌŶƚƌǇηϴ ƵƐƚŽŵ;^ĞĞƚĂďůĞϰͿ ϯϬϭϬϯϯ ϭϬϯϮ ϯϬϭϬϯϰͲ ϭϬϯϯͲ >ŽŐƵĨĨĞƌŶƚƌǇηϵ ƵƐƚŽŵ;^ĞĞƚĂďůĞϰͿ ϯϬϭϬϯϳ ϭϬϯϲ ϯϬϭϬϯϴͲ ϭϬϯϳͲ >ŽŐƵĨĨĞƌŶƚƌǇηϭϬ ƵƐƚŽŵ;^ĞĞƚĂďůĞϰͿ ϯϬϭϬϰϭ ϭϬϰϬ ϯϬϭϬϰϮͲ ϭϬϰϭͲ >ŽŐƵĨĨĞƌŶƚƌǇηϭϭ ƵƐƚŽŵ;^ĞĞƚĂďůĞϰͿ ϯϬϭϬϰϱ ϭϬϰϰ

18 ϯϬϭϬϰϲͲ ϭϬϰϱͲ >ŽŐƵĨĨĞƌŶƚƌǇηϭϮ ƵƐƚŽŵ;^ĞĞƚĂďůĞϰͿ ϯϬϭϬϰϵ ϭϬϰϴ ϯϬϭϬϱϬͲ ϭϬϰϵͲ >ŽŐƵĨĨĞƌŶƚƌǇηϭϯ ƵƐƚŽŵ;^ĞĞƚĂďůĞϰͿ ϯϬϭϬϱϯ ϭϬϱϮ ϯϬϭϬϱϰͲ ϭϬϱϯͲ >ŽŐƵĨĨĞƌŶƚƌǇηϭϰ ƵƐƚŽŵ;^ĞĞƚĂďůĞϰͿ ϯϬϭϬϱϳ ϭϬϱϲ ϯϬϭϬϱϴͲ ϭϬϱϳͲ >ŽŐƵĨĨĞƌŶƚƌǇηϭϱ ƵƐƚŽŵ;^ĞĞƚĂďůĞϰͿ ϯϬϭϬϲϭ ϭϬϲϬ ϯϬϭϬϲϮͲ ϭϬϲϭͲ >ŽŐƵĨĨĞƌŶƚƌǇηϭϲ ƵƐƚŽŵ;^ĞĞƚĂďůĞϰͿ ϯϬϭϬϲϱ ϭϬϲϰ ϯϬϭϬϲϲͲ ϭϬϲϱͲ >ŽŐƵĨĨĞƌŶƚƌǇηϭϳ ƵƐƚŽŵ;^ĞĞƚĂďůĞϰͿ ϯϬϭϬϲϵ ϭϬϲϴ ϯϬϭϬϳϬͲ ϭϬϲϵͲ >ŽŐƵĨĨĞƌŶƚƌǇηϭϴ ƵƐƚŽŵ;^ĞĞƚĂďůĞϰͿ ϯϬϭϬϳϯ ϭϬϳϮ ϯϬϭϬϳϰͲ ϭϬϳϯͲ >ŽŐƵĨĨĞƌŶƚƌǇηϭϵ ƵƐƚŽŵ;^ĞĞƚĂďůĞϰͿ ϯϬϭϬϳϳ ϭϬϳϲ ϯϬϭϬϳϴͲ ϭϬϳϳͲ >ŽŐƵĨĨĞƌŶƚƌǇηϮϬ ƵƐƚŽŵ;^ĞĞƚĂďůĞϰͿ ϯϬϭϬϴϭ ϭϬϴϬ ϯϬϭϬϴϮͲ ϭϬϴϭͲ >ŽŐƵĨĨĞƌŶƚƌǇηϮϭ ƵƐƚŽŵ;^ĞĞƚĂďůĞϰͿ ϯϬϭϬϴϱ ϭϬϴϰ ϯϬϭϬϴϲͲ ϭϬϴϱͲ >ŽŐƵĨĨĞƌŶƚƌǇηϮϮ ƵƐƚŽŵ;^ĞĞƚĂďůĞϰͿ ϯϬϭϬϴϵ ϭϬϴϴ ϯϬϭϬϵϬͲ ϭϬϴϵͲ >ŽŐƵĨĨĞƌŶƚƌǇηϮϯ ƵƐƚŽŵ;^ĞĞƚĂďůĞϰͿ ϯϬϭϬϵϯ ϭϬϵϮ ϯϬϭϬϵϰͲ ϭϬϵϯͲ >ŽŐƵĨĨĞƌŶƚƌǇηϮϰ ƵƐƚŽŵ;^ĞĞƚĂďůĞϰͿ ϯϬϭϬϵϳ ϭϬϵϲ ϯϬϭϬϵϴͲ ϭϬϵϳͲ >ŽŐƵĨĨĞƌŶƚƌǇηϮϱ ƵƐƚŽŵ;^ĞĞƚĂďůĞϰͿ ϯϬϭϭϬϭ ϭϭϬϬ ϯϬϭϭϬϮͲ ϭϭϬϭͲ >ŽŐƵĨĨĞƌŶƚƌǇηϮϲ ƵƐƚŽŵ;^ĞĞƚĂďůĞϰͿ ϯϬϭϭϬϱ ϭϭϬϰ ϯϬϭϭϬϲͲ ϭϭϬϱͲ >ŽŐƵĨĨĞƌŶƚƌǇηϮϳ ƵƐƚŽŵ;^ĞĞƚĂďůĞϰͿ ϯϬϭϭϬϵ ϭϭϬϴ ϯϬϭϭϭϬͲ ϭϭϬϵͲ >ŽŐƵĨĨĞƌŶƚƌǇηϮϴ ƵƐƚŽŵ;^ĞĞƚĂďůĞϰͿ ϯϬϭϭϭϯ ϭϭϭϮ ϯϬϭϭϭϰͲ ϭϭϭϯͲ >ŽŐƵĨĨĞƌŶƚƌǇηϮϵ ƵƐƚŽŵ;^ĞĞƚĂďůĞϰͿ ϯϬϭϭϭϳ ϭϭϭϲ ϯϬϭϭϭϴͲ ϭϭϭϳͲ >ŽŐƵĨĨĞƌŶƚƌǇηϯϬ ƵƐƚŽŵ;^ĞĞƚĂďůĞϰͿ ϯϬϭϭϮϭ ϭϭϮϬ ϯϬϮϬϬϮͲ ϮϬϬϭͲ ŚĂŶŶĞůϭ&ůŽĂƚsĂůƵĞ Ͳϵϵϵϵ͘Ϭ ϵϵϵϵϵ͘Ϭ ϯϮďŝƚ&ůŽĂƚ;/ϳϱϰͿ ϯϬϮϬϬϯ ϮϬϬϮ ϯϬϮϬϬϰͲ ϮϬϬϯͲ ŚĂŶŶĞůϮ&ůŽĂƚsĂůƵĞ Ͳϵϵϵϵ͘Ϭ ϵϵϵϵϵ͘Ϭ ϯϮďŝƚ&ůŽĂƚ;/ϳϱϰͿ ϯϬϮϬϬϱ ϮϬϬϰ

19 ϯϬϮϬϬϲͲ ϮϬϬϱͲ ŚĂŶŶĞůϯ&ůŽĂƚsĂůƵĞ Ͳϵϵϵϵ͘Ϭ ϵϵϵϵϵ͘Ϭ ϯϮďŝƚ&ůŽĂƚ;/ϳϱϰͿ ϯϬϮϬϬϳ ϮϬϬϲ ϯϬϮϬϬϴͲ ϮϬϬϳͲ ŚĂŶŶĞůϰ&ůŽĂƚsĂůƵĞ Ͳϵϵϵϵ͘Ϭ ϵϵϵϵϵ͘Ϭ ϯϮďŝƚ&ůŽĂƚ;/ϳϱϰͿ ϯϬϮϬϬϵ ϮϬϬϴ ϯϬϮϬϭϬͲ ϮϬϬϵͲ ŚĂŶŶĞůϱ&ůŽĂƚsĂůƵĞ Ͳϵϵϵϵ͘Ϭ ϵϵϵϵϵ͘Ϭ ϯϮďŝƚ&ůŽĂƚ;/ϳϱϰͿ ϯϬϮϬϭϭ ϮϬϭϬ ϯϬϮϬϭϮͲ ϮϬϭϭͲ ŚĂŶŶĞůϲ&ůŽĂƚsĂůƵĞ Ͳϵϵϵϵ͘Ϭ ϵϵϵϵϵ͘Ϭ ϯϮďŝƚ&ůŽĂƚ;/ϳϱϰͿ ϯϬϮϬϭϯ ϮϬϭϮ ϯϬϮϬϭϰͲ ϮϬϭϯͲ ŚĂŶŶĞůϭĂŶĚϮŝĨĨĞƌĞŶƚŝĂůsĂůƵĞ Ͳϵϵϵϵ͘Ϭ ϵϵϵϵϵ͘Ϭ ϯϮďŝƚ&ůŽĂƚ;/ϳϱϰͿ ϯϬϮϬϭϱ ϮϬϭϰ ϯϬϮϬϭϲͲ ϮϬϭϱͲ ŚĂŶŶĞůϯĂŶĚϰŝĨĨĞƌĞŶƚŝĂůsĂůƵĞ Ͳϵϵϵϵ͘Ϭ ϵϵϵϵϵ͘Ϭ ϯϮďŝƚ&ůŽĂƚ;/ϳϱϰͿ ϯϬϮϬϭϳ ϮϬϭϲ ϯϬϮϬϭϴͲ ϮϬϭϳͲ ŚĂŶŶĞůϱĂŶĚϲŝĨĨĞƌĞŶƚŝĂůsĂůƵĞ Ͳϵϵϵϵ͘Ϭ ϵϵϵϵϵ͘Ϭ ϯϮďŝƚ&ůŽĂƚ;/ϳϱϰͿ ϯϬϮϬϭϵ ϮϬϭϴ ϯϬϮϬϮϬͲ ϮϬϭϵͲ ŚĂŶŶĞůϭ,ŝŐŚůĂƌŵ>ŝŵŝƚ Ͳϵϵϵϵ͘Ϭ ϵϵϵϵϵ͘Ϭ ϯϮďŝƚ&ůŽĂƚ;/ϳϱϰͿ ϯϬϮϬϮϭ ϮϬϮϬ ϯϬϮϬϮϮͲ ϮϬϮϭͲ ŚĂŶŶĞůϮ,ŝŐŚůĂƌŵ>ŝŵŝƚ Ͳϵϵϵϵ͘Ϭ ϵϵϵϵϵ͘Ϭ ϯϮďŝƚ&ůŽĂƚ;/ϳϱϰͿ ϯϬϮϬϮϯ ϮϬϮϮ ϯϬϮϬϮϰͲ ϮϬϮϯͲ ŚĂŶŶĞůϯ,ŝŐŚůĂƌŵ>ŝŵŝƚ Ͳϵϵϵϵ͘Ϭ ϵϵϵϵϵ͘Ϭ ϯϮďŝƚ&ůŽĂƚ;/ϳϱϰͿ ϯϬϮϬϮϱ ϮϬϮϰ ϯϬϮϬϮϲͲ ϮϬϮϱͲ ŚĂŶŶĞůϰ,ŝŐŚůĂƌŵ>ŝŵŝƚ Ͳϵϵϵϵ͘Ϭ ϵϵϵϵϵ͘Ϭ ϯϮďŝƚ&ůŽĂƚ;/ϳϱϰͿ ϯϬϮϬϮϳ ϮϬϮϲ ϯϬϮϬϮϴͲ ϮϬϮϳͲ ŚĂŶŶĞůϱ,ŝŐŚůĂƌŵ>ŝŵŝƚ Ͳϵϵϵϵ͘Ϭ ϵϵϵϵϵ͘Ϭ ϯϮďŝƚ&ůŽĂƚ;/ϳϱϰͿ ϯϬϮϬϮϵ ϮϬϮϴ ϯϬϮϬϯϬͲ ϮϬϮϵͲ ŚĂŶŶĞůϲ,ŝŐŚůĂƌŵ>ŝŵŝƚ Ͳϵϵϵϵ͘Ϭ ϵϵϵϵϵ͘Ϭ ϯϮďŝƚ&ůŽĂƚ;/ϳϱϰͿ ϯϬϮϬϯϭ ϮϬϯϬ ϯϬϮϬϯϮͲ ϮϬϯϭͲ ŚĂŶŶĞůϭĂŶĚϮŝĨĨĞƌĞŶƚŝĂů,ŝŐŚ Ͳϵϵϵϵ͘Ϭ ϵϵϵϵϵ͘Ϭ ϯϮďŝƚ&ůŽĂƚ;/ϳϱϰͿ ϯϬϮϬϯϯ ϮϬϯϮ ůĂƌŵ>ŝŵŝƚ ϯϬϮϬϯϰͲ ϮϬϯϯͲ ŚĂŶŶĞůϯĂŶĚϰŝĨĨĞƌĞŶƚŝĂů,ŝŐŚ Ͳϵϵϵϵ͘Ϭ ϵϵϵϵϵ͘Ϭ ϯϮďŝƚ&ůŽĂƚ;/ϳϱϰͿ ϯϬϮϬϯϱ ϮϬϯϰ ůĂƌŵ>ŝŵŝƚ ϯϬϮϬϯϲͲ ϮϬϯϱͲ ŚĂŶŶĞůϱĂŶĚϲŝĨĨĞƌĞŶƚŝĂů,ŝŐŚ Ͳϵϵϵϵ͘Ϭ ϵϵϵϵϵ͘Ϭ ϯϮďŝƚ&ůŽĂƚ;/ϳϱϰͿ ϯϬϮϬϯϳ ϮϬϯϲ ůĂƌŵ>ŝŵŝƚ ϯϬϮϬϯϴͲ ϮϬϯϳͲ ŚĂŶŶĞůϭ,ŝŐŚ>Žǁ>ŝŵŝƚ Ͳϵϵϵϵ͘Ϭ ϵϵϵϵϵ͘Ϭ ϯϮďŝƚ&ůŽĂƚ;/ϳϱϰͿ ϯϬϮϬϯϵ ϮϬϯϴ ϯϬϮϬϰϬͲ ϮϬϯϵͲ ŚĂŶŶĞůϮ,ŝŐŚ>Žǁ>ŝŵŝƚ Ͳϵϵϵϵ͘Ϭ ϵϵϵϵϵ͘Ϭ ϯϮďŝƚ&ůŽĂƚ;/ϳϱϰͿ ϯϬϮϬϰϭ ϮϬϰϬ ϯϬϮϬϰϮͲ ϮϬϰϭͲ ŚĂŶŶĞůϯ,ŝŐŚ>Žǁ>ŝŵŝƚ Ͳϵϵϵϵ͘Ϭ ϵϵϵϵϵ͘Ϭ ϯϮďŝƚ&ůŽĂƚ;/ϳϱϰͿ ϯϬϮϬϰϯ ϮϬϰϮ ϯϬϮϬϰϰͲ ϮϬϰϯͲ ŚĂŶŶĞůϰ,ŝŐŚ>Žǁ>ŝŵŝƚ Ͳϵϵϵϵ͘Ϭ ϵϵϵϵϵ͘Ϭ ϯϮďŝƚ&ůŽĂƚ;/ϳϱϰͿ ϯϬϮϬϰϱ ϮϬϰϰ ϯϬϮϬϰϲͲ ϮϬϰϱͲ ŚĂŶŶĞůϱ,ŝŐŚ>Žǁ>ŝŵŝƚ Ͳϵϵϵϵ͘Ϭ ϵϵϵϵϵ͘Ϭ ϯϮďŝƚ&ůŽĂƚ;/ϳϱϰͿ ϯϬϮϬϰϳ ϮϬϰϲ

20 ϯϬϮϬϰϴͲ ϮϬϰϳͲ ŚĂŶŶĞůϲ,ŝŐŚ>Žǁ>ŝŵŝƚ Ͳϵϵϵϵ͘Ϭ ϵϵϵϵϵ͘Ϭ ϯϮďŝƚ&ůŽĂƚ;/ϳϱϰͿ ϯϬϮϬϰϵ ϮϬϰϴ ϯϬϮϬϱϬͲ ϮϬϰϵͲ ŚĂŶŶĞůϭĂŶĚϮŝĨĨĞƌĞŶƚŝĂů>Žǁ Ͳϵϵϵϵ͘Ϭ ϵϵϵϵϵ͘Ϭ ϯϮďŝƚ&ůŽĂƚ;/ϳϱϰͿ ϯϬϮϬϱϭ ϮϬϱϬ ůĂƌŵ>ŝŵŝƚ ϯϬϮϬϱϮͲ ϮϬϱϭͲ ŚĂŶŶĞůϯĂŶĚϰŝĨĨĞƌĞŶƚŝĂů>Žǁ Ͳϵϵϵϵ͘Ϭ ϵϵϵϵϵ͘Ϭ ϯϮďŝƚ&ůŽĂƚ;/ϳϱϰͿ ϯϬϮϬϱϯ ϮϬϱϮ ůĂƌŵ>ŝŵŝƚ ϯϬϮϬϱϰͲ ϮϬϱϯͲ ŚĂŶŶĞůϱĂŶĚϲŝĨĨĞƌĞŶƚŝĂů>Žǁ Ͳϵϵϵϵ͘Ϭ ϵϵϵϵϵ͘Ϭ ϯϮďŝƚ&ůŽĂƚ;/ϳϱϰͿ ϯϬϮϬϱϱ ϮϬϱϰ ůĂƌŵ>ŝŵŝƚ ϯϬϮϬϱϲͲ ϮϬϱϱͲ ZWD Ϭ ϵϵϵϵϵ͘Ϭ ϯϮďŝƚƵŶƐŝŐŶĞĚŝŶƚĞŐĞƌ ϯϬϮϬϱϳ ϮϬϱϲ ϯϬϮϬϱϴͲ ϮϬϱϳͲ ,ŽƵƌŵĞƚĞƌ Ϭ ϵϵϵϵϵ͘Ϭ ϯϮďŝƚƵŶƐŝŐŶĞĚŝŶƚĞŐĞƌ ϯϬϮϬϱϵ ϮϬϱϴ

Holding Register Table (table 2)

DŽĚŝĐŽŶ DŽĚďƵƐ ĞƐĐƌŝƉƚŝŽŶ DŝŶ DĂǆ ĂƚĂƚǇƉĞ ĚĚƌĞƐƐ KĨĨƐĞƚ sĂůƵĞ sĂůƵĞ ϰϬϭϬϬϭͲ ϭϬϬϬͲϭϬϬϭ >ŽŐƐƚĂƌƚĚĂƚĞ;ƵƉƉĞƌϭϲďŝƚƐ ƵƐƚŽŵ;^ĞĞƚĂďůĞϯͿ ϰϬϭϬϬϮ ĂŶĚůŽǁĞƌϭϲďŝƚƐ ƌĞƐƉĞĐƚŝǀĞůǇͿ

Date Format Table (table 3)

Second(MSB) Minute Hour Day Month Year(LSB) Bits 6 6 5 5 4 6 Value 0-59 0-59 0-23 1-31 1-12 0-63(relative to year range 2000)

Log Buffer Entry (table 4)

Datetime Event ID Value Length 32 bit unsigned 16 bit unsigned ϯϮďŝƚ&ůŽĂƚ;/ϳϱϰͿ integer integer Value See table 3 1-10 -9999.0 – 99999.0 range

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22 SUD-CHEMIE Creating Performance Technology

AIR PURIF ICATION CATALYSTS SUD CHEMIE INC. 32 Fremont Street Needham, MA 02494 USA Phone: (781)444-5188 Fax: (781)444-0130

www.sud-chemie.com

EnviCat® 2320 Oxidation Catalyst

A high performance catalyst for the oxidation of carbon monoxide (CO), hydrocarbons (HC) and Soluble Organic Fractions (SOF) including condensable particulate matter.

The EnviCat® Sulfer tolerant oxidation catalyst comprises a special precious metal formulation on patented Süd-Chemie washcoat

Catalyst Name ...... EnviCat® 2320

Applications ...... Diesel or Biogas Fueled Engines.

Substrate ...... Metal Honeycomb Monolith

Standard Sizes …………………………… 2 - 48” dia. x 3.5 & 5.91” cylindrical

Operating Temperature Range...... 572 Deg F to 1247 Deg F.

Cell Density, ………………………………. 100 to 400 cpsi

Washcoat Surface ………………………… Designed for high sulfur fuel

Typical Bulk Density ….…………………… 0.6-0.8 kg/L (37-50 lb/ ft3)

The information contained in this leaflet is the result of our research and experience. It is given in good faith, but under no circumstances does it constitute any guarantee, representation or warranty. Any responsibility and/or liability of Süd-Chemie Group Companies is subject to written contractual terms and conditions as agreed by Süd-Chemie Group Companies.

MATERIAL SAFETY DATA SHEET

EnviCat® 2320 Page 1

Substance key: SCIEC2320 Revision Date: 00/00/0000 Version : 0 - 0 / 0 Date of printing :06/10/2014

Section 01 - Product and company identification

Identification of the Clariant Corporation company: 4000 Monroe Road Charlotte, NC, 28205 Telephone No.: +1 704-331-7000

Information of the substance/preparation: Product Stewardship 1-704-331-7710

Emergency tel. number: +1 800-424-9300(CHEMTREC)

Trade name: EnviCat® 2320

Primary product use: Environmental Catalyst

Chemical family: Environmental catalyst

Section 02 - Hazards identification

Emergency overview: Brown or black metal monolith (shape varies). There are little or no health hazards associated with intact catalyst monolith. However, health hazards do exist as a result of the dusts generated if this product is ground, sliced or broken. Breathing dust may irritate nose, throat and lungs. Prolonged inhalation of dust may cause lung damage. May produce an allergic reaction.

Expected Route of entry: Inhalation: Route of exposure unlikely. There are little or no health hazards associated with intact catalyst monolith. However, health hazards do exist as a result of the dusts generated if this product is ground, sliced or broken. Breathing dust may irritate nose, throat and lungs. Skin contact: May cause skin irritation. May produce an allergic reaction. Eye contact: Route of exposure unlikely. MAY CAUSE SEVERE EYE IRRITATION. Use of proper chemical hygiene should prevent exposure. Ingestion: Route of exposure unlikely. Harmful if swallowed. Skin absorption: Route of exposure unlikely.

Health effects of exposure:

Silica ( 7631-86-9 )

MATERIAL SAFETY DATA SHEET

EnviCat® 2320 Page 2

Substance key: SCIEC2320 Revision Date: 00/00/0000 Version : 0 - 0 / 0 Date of printing :06/10/2014

Silica: considered to be a respirable particulate and may cause irritation to the lungs. Has also been known to cause eye irritation in certain individuals. Prolonged inhalation of dusts containing free silica may result in the development of a disabling pulmonary fibrosis known as silicosis.

Zirconium oxide ( 1314-23-4 ) Zirconium Oxide: Causes serious eye irritation. Causes skin irritation. May be absorbed through skin. May cause respiratory irritation. May cause dry cough. Repeated skin exposure may cause formation of benign tumor due to absorption of compound. May cause skin disease. Repeated exposures may cause lung disease, including fibrosis or pneumoconiosis. May cause allergic reactions which may be delayed.

Platinum ( 7440-06-4 ) Platinum: May cause eye irritation and may cause a burning sensation and excess lacrimation (tearing). May cause skin irritation. May be harmful if absorbed through skin. Material may be irritating to mucous membranes and upper respiratory tract. May be harmful if inhaled. May be harmful if swallowed. Flammable in a powder state. Prolonged or repeated skin exposure may cause allergic reactions in certain sensitive individuals. Prolonged or repeated inhalation exposure may cause allergic reactions in certain sensitive individuals.

Quartz ( 14808-60-7 ) Quartz: Confirmed carcinogen with experimental carcinogenic, tumorogenic,and neoplastogenic data.Experimental poison by intratracheal and intravenous routes.Human systemic effects by inhalation:cough,dyspnea, liver effects.IARC group 1 (carcinogenic to humans).

Zeolite ( 68989-23-1 ) Health hazards may arise from inhalation, ingestion, and/or contact with the skin and/or eyes. Ingestion may result in damage to throat, esophagus, and/or gastrointestinal tract. Inhalation may cause burning of the upper respiratory tract and/or temporary or permanent lung damage. Prolonged or repeated contact with the skin, in the absence of proper hygiene, may cause dryness, irritation, and/or dermatitis. Contact with the eye tissue may result in irritation, burns or conjunctivitis.

Known effects on other illnesses: Persons with pre-existing respiratory or skin diseases may be at an increased risk from exposure to this material. Listed carcinogen: IARC: Yes NTP: Yes OSHA: No Other: No

HMIS: Health: 2* Flammability: 0 Reactivity: 0

Section 03 - Composition/information on ingredients

Hazardous ingredients:

MATERIAL SAFETY DATA SHEET

EnviCat® 2320 Page 3

Substance key: SCIEC2320 Revision Date: 00/00/0000 Version : 0 - 0 / 0 Date of printing :06/10/2014

Component CAS-no. (Trade secret Concentration no.) Amorphous Silica 7631-86-9 < 5 % Zirconium Oxide 1314-23-4 < 5 % Platinum 7440-06-4 < 1 % Quartz (Silica-Crystalline) 14808-60-7 < 1 % Non-Hazardous Binder < 5 %

Section 04 - First aid measures

After inhalation: INHALATION: If exposed to excessive levels of dust or fumes, remove to fresh air and get medical attention. Get medical attention if cough and other symptoms develop.

After contact with skin: Wash area with mild soap and copious amounts of water. Call a physician if irritation develops or persists.

After contact with eyes: Hold eyelids apart and flush eyes with plenty of water for at least 15 minutes. Get medical attention.

After ingestion: Call your local Poison Control Center (In the U.S. call 1-800-222-1222). Never give anything by mouth to an unconscious person.

Advice to doctor / Treatment: Treat symptomatically.

Section 05 - Fire fighting measures

Flashpoint: not applicable

Hazardous combustion products: None known.

Extinguishing media: Use extinguishing measures that are appropriate to local circumstances and the surrounding environment.

Special fire fighting procedure: Wear full protective clothing and NIOSH/MSHA-approved positive pressure, self-contained breathing apparatus.

Unusual fire and explosion None known. hazards:

Section 06 - Accidental release measures

MATERIAL SAFETY DATA SHEET

EnviCat® 2320 Page 4

Substance key: SCIEC2320 Revision Date: 00/00/0000 Version : 0 - 0 / 0 Date of printing :06/10/2014

Steps to be taken in case of spill or leak: Wearing appropriate personal protective equipment, contain spill and collect into a suitable container. Material should be swept up or vacuumed, using ventilation to control the level of airborne dust. Avoid using compressed air or any method that creates airborne dust. If cleanup may create airborne dust, personnel should wear eye, skin, and respiratory protection. Refer to Section 8 for more information.

Section 07 - Handling and storage

Advice on safe handling: Avoid contact with skin. Avoid contact with eyes. Do not breathe dust/ fume/ gas/ mist/ vapours/ spray. Minimize dust generation and accumulation. Do NOT grind, slice, sand, scrape or otherwise break this product. Avoid dust formation. Avoid contact with/or the inhalation of dusts from this product.

Further info on storage conditions: Store in a cool, dry, well-ventilated area away from incompatible substances. Keep container tightly closed and dry.

Section 08 - Exposure controls / personal protection

Occupational exposure limits:

Component CAS Regulatory list Type of value Values / Remarks number: zirconium compounds 7440-67-7 US. Permissible 8-hour time 5 mg/m3 Exposure Limits weighted (PEL) Table Z-1 average Limits for Air Contaminants Zirconium compounds 7440-67-7 US. Table Z-1-A 8-hour time 5 mg/m3 Limits for Air weighted Contaminants average (1989 vacated values) Zirconium compounds 7440-67-7 US. Table Z-1-A Short-term 10 mg/m3 Limits for Air exposure limit Contaminants (1989 vacated values) Zirconium and 7440-67-7 US. Threshold 8-hour, time- 5 mg/m3 compounds Limit Values (TLV) weighted for Chemical average Substances in the Work Environment Adopted Values Zirconium and 7440-67-7 US. Threshold Short-term 10 mg/m3

MATERIAL SAFETY DATA SHEET

EnviCat® 2320 Page 5

Substance key: SCIEC2320 Revision Date: 00/00/0000 Version : 0 - 0 / 0 Date of printing :06/10/2014

compounds Limit Values (TLV) exposure limit for Chemical Substances in the Work Environment Adopted Values Platinum metal 7440-06-4 US. Threshold 8-hour, time- 1 mg/m3 Limit Values (TLV) weighted for Chemical average Substances in the Work Environment Adopted Values Platinum Metal 7440-06-4 US. Table Z-1-A 8-hour time 1 mg/m3 Limits for Air weighted Contaminants average (1989 vacated values) Silica, Crystalline - α- 14808-60-7 US. Threshold 8-hour, time- 0.025 mg/m3 Quartz Limit Values (TLV) weighted for Chemical average Substances in the Work Environment Adopted Values Silica, crystalline, 14808-60-7 US. Table Z-1-A 8-hour time 0.1 mg/m3 quartz ( Crystalline and Limits for Air weighted Dust) Contaminants average (1989 vacated values)

All inert or nuisance dusts, whether mineral, inorganic, or organic, not listed specifically by substance name are covered by the Particulates Not Otherwise Regulated (PNOR) limit which is 5 mg/m3 for respirable fraction and 15 mg/m3 for total dust. ACGIH exposure guidelines of less than 3 mg/m3 (respirable) and 10 mg/m3 (inhalable) have been established for particles (insoluble/poorly soluble) not otherwise specified (PNOS).

Respiratory protection: Wear NIOSH approved particulate filtering respirator rated N, R, or P95 or 100 or equivalent in the absence of proper environmental control. Type of respirator depends on level of exposure.

Hand protection: Impervious rubber such as neoprene, nitrile, natural rubber, butyl rubber, PVC, or teflon.

Eye protection: Follow facility guidelines in the absence of dusts. Tightly fitting safety goggles

Other protective equipment: Wear protective clothing, including long sleeves and gloves, to prevent skin contact. Thoroughly wash clothing before reuse.

Advice on system design: Use ventilation adequate to keep exposures below recommended exposure limits. See the safety datasheet.

MATERIAL SAFETY DATA SHEET

EnviCat® 2320 Page 6

Substance key: SCIEC2320 Revision Date: 00/00/0000 Version : 0 - 0 / 0 Date of printing :06/10/2014

Section 09 - Physical and chemical properties

Form: Solid form

Color: dark brown

Odor: none

Odor limit: not available

pH: not determined

Solubility in water: insoluble

Density: 0.7 g/cm3

Melting point : not determined

Boiling point : not determined

Evaporation number: not available

Vapor pressure: not determined

Bulk density: 43.68 lb/ft3

Relative vapor density: not determined

Partitioning coef. no data available octanol/water:

Loss on drying: Not Volatile

Section 10 - Stability and reactivity

Chemical stability: Stable

Hazardous Polymerization: Hazardous polymerisation does not occur. Conditions to avoid: None known.

Conditions to avoid: None known.

Section 11 - Toxicological information

Product information:

Eye irritation: Mild eye irritation (rabbit) Method: Draize Test

Component information:

Silica ( 7631-86-9 )

Acute oral toxicity: LD50 3,160 mg/kg (rat)

Zirconium oxide ( 1314-23-4 )

Acute oral toxicity: Test data for the substance are not available.

MATERIAL SAFETY DATA SHEET

EnviCat® 2320 Page 7

Substance key: SCIEC2320 Revision Date: 00/00/0000 Version : 0 - 0 / 0 Date of printing :06/10/2014

Platinum ( 7440-06-4 )

Acute oral toxicity: Test data for the substance are not available.

Section 12 - Ecological information

Component information:

Silica ( 7631-86-9 )

Fish toxicity: No adverse effect has been observed in acute toxicity tests.

Zirconium oxide ( 1314-23-4 )

Fish toxicity: Test data for the substance are not available.

Platinum ( 7440-06-4 )

Fish toxicity: Test data for the substance are not available.

Remarks: May cause long lasting harmful effects to aquatic life. Do not allow to enter ground water, waterways or waste water.

Section 13 - Disposal considerations

Waste disposal information: This product, if discarded as sold, is not a Federal RCRA hazardous waste. Processing, use or contamination of this product may change the waste management options. State and local disposal regulations may differ from federal disposal regulations.

RCRA hazardous waste: This material may exhibit one or more characteristics of a hazardous waste and require appropriate analysis to determine specific disposal requirements. Processing, use or contamination of this product may change the waste management options. State and local disposal regulations RCRA number: NONE

Section 14 - Transport information

DOT not restricted

IATA not restricted

IMDG not restricted

Section 15 - Regulatory information

TSCA Status: All components of this product are listed or excluded from listing on the United States Environmental Protection Agency Toxic Substances Control Act (TSCA) Inventory.

MATERIAL SAFETY DATA SHEET

EnviCat® 2320 Page 8

Substance key: SCIEC2320 Revision Date: 00/00/0000 Version : 0 - 0 / 0 Date of printing :06/10/2014

SARA (section 311/312): Reactive hazard: no Pressure hazard: no Fire hazard: no Immediate/acute: yes Delayed/chronic: yes

SARA 313 information: This product is not subject to SARA Title III Section 313 reporting requirements under 40 CFR 372.

Clean Water Act: Contains no known priority pollutants at concentrations greater than 0.1%.

CERCLA information: This material does not contain any components with a CERCLA RQ.

Section 16 - Other information

State regulatory information: California Proposition 65: This product is or contains chemical(s) known to the state of California to cause cancer.

Label information:

WARNING!

There are little or no health hazards associated with intact catalyst monolith. Hazards stated are related to the chemical on/in the support. Health hazards do exist as a result of the dusts generated if this product is ground, sliced, sanded, scraped, or broken. May cause eye, skin, and respiratory tract irritation. Prolonged or repeated inhalation may cause lung damage. May produce an allergic reaction.

Avoid breathing dust. Avoid contact with skin, eyes and clothing. Do not ingest. Keep container closed. Prior to handling this product, please refer to the current MSDS for recommended protective equipment and detailed hazard and precautionary information.

INHALATION: If exposed to excessive levels of dust or fumes, remove to fresh air and get medical attention. Get medical attention if cough and other symptoms develop. INGESTION: If swallowed, call your local Poison Control Center (1-800-222-1222 in the U.S.) In case of contact, immediately flush eyes with plenty of water for at least 15 minutes. IF ON SKIN: Wash with plenty of soap and water. Get medical attention if symptoms occur.

NFPA:

Health: 2 Flammability: 0 Reactivity: 0

MATERIAL SAFETY DATA SHEET

EnviCat® 2320 Page 9

Substance key: SCIEC2320 Revision Date: 00/00/0000 Version : 0 - 0 / 0 Date of printing :06/10/2014

This information is supplied under the OSHA Hazard Communication Standard, 29 CFR 1910.1200, and is offered in good faith based on data available to us that we believe to be true and accurate. The recommended industrial hygiene and safe handling procedures are believed to be generally applicable to the material. However, each user should review these recommendations in the specific context of the intended use and determine whether they are appropriate for that use. No warranty, express or implied, is made regarding the accuracy of this data, the hazards connected with the use of the material, or the results to be obtained from the use thereof. We assume no responsibility for damage or injury from the use of the product described herein. Data provided here are typical and not intended for use as product specifications.

- Specification Sheet - Oxidation Catalyst - For CO and VOC Reduction

Customer: NES Notes: Sulfur Tolerant Attention: David Horowitz Ref. No: B51125-1A Job Ref: North River WTP Date: 12/18/15

Engine Mfg: Jenbacher Model No: JGS620F28 Output eKW: 3030 EKW Cycle: 4 RPM: 1500 Fuel Type : Clean Digesster Gas Load: 100% Hours/Year 8,300

Model: EnviCat-2320-47.3x3.5x1 Nbr Units: 5

Item Description English Units Metric Units

Engine Output 4,183 BHP 3,121 BKW

Exhaust Gas Mass Flow 39,908 Lbs/Hour 18,102 Kg/Hour Exhaust Gas Temperature 727.0 °F 386.1 °C Exhaust Flow - Standard Units 498,661 SCFH 14,120 SCMH

Pre-Catalyst CO Emissions 2.50 G/BHP/Hr 1.86 G/BKW/Hr Pre-Catalyst CO Emissions 300 PPMV@15% O2 300 PPMV@15% O2 Pre-Catalyst CO Emissions 7.39 Lbs/MW/Hour 3.35 Kg/MW/Hour

Post-Catalyst CO Emissions 0.500 G/BHP/Hr 0.373 G/BKW/Hr Post-Catalyst CO Emissions 60 PPMV@15% O2 60 PPMV@15% O2 Post-Catalyst CO Emissions 1.477 Lbs/MW/Hour 0.670 Kg/MW/Hour

Percentage CO Reduction 80.0 % 80.0 %

Pre-Catalyst VOC Emissions 0.35 G/BHP/Hr 0.26 G/BKW/Hr Pre-Catalyst VOC Emissions 75 PPMV@15% O2 75 PPMV@15% O2 Pre-Catalyst VOC Emissions 1.03 Lbs/MW/Hour 0.47 Kg/MW/Hour

Post-Catalyst VOC Emissions 0.150 G/BHP/Hr 0.112 G/BKW/Hr Post-Catalyst VOC Emissions 32 PPMV@15% O2 32 PPMV@15% O2 Post-Catalyst VOC Emissions 0.443 Lbs/MW/Hour 0.201 Kg/MW/Hour

Percentage VOC Reduction 57.1 % 57.1 %

Pre-Catalyst H2CO Emissions 0.45 G/BHP/Hr 0.34 G/BKW/Hr Pre-Catalyst H2CO Emissions 68 PPMV@15% O2 68 PPMV@15% O2 Pre-Catalyst H2CO Emissions 4.15 Lbs/Hour 1.88 Kg/Hour

Post-Catalyst H2CO Emissions 0.020 G/BHP/Hr 0.015 G/BKW/Hr Post-Catalyst H2CO Emissions 3.0 PPMV@15% O2 3.0 PPMV@15% O2 Post-Catalyst H2CO Emissions 0.184 Lbs/Hour 0.084 Kg/Hour

Percentage H2CO Reduction 95.6 % 95.6 %

Back Pressure Thru Catalyst 3.5 In WC 8.8 mbar

Oxidation Catalyst Volume 3.417 Cu/Ft 0.0967 Cu/Meter Catalyst Element Diameter 47.30 Inches 1200 Millimeters Number of Elements 1 1 Oxidation Catalyst Space Velocity 145,949 SCFH/FT3 145,949 SCMH/M3

- Specification Sheet - Oxidation Catalyst - For CO and VOC Reduction

Customer: NES Notes: Sulfur Tolerant Attention: David Horowitz Ref. No: B51125-1B Job Ref: North River WTP Date: 12/18/15

Engine Mfg: Jenbacher Model No: JGS620F02 Output eKW: 3029 EKW Cycle: 4 RPM: 1500 Fuel Type : Natural Gas Load: 100% Hours/Year 8,300

Model: EnviCat-2320-47.3x3.5x1 Nbr Units: 5

Item Description English Units Metric Units

Engine Output 4,183 BHP 3,121 BKW

Exhaust Gas Mass Flow 39,113 Lbs/Hour 17,742 Kg/Hour Exhaust Gas Temperature 714.0 °F 378.9 °C Exhaust Flow - Standard Units 495,540 SCFH 14,032 SCMH

Pre-Catalyst CO Emissions 2.50 G/BHP/Hr 1.86 G/BKW/Hr Pre-Catalyst CO Emissions 300 PPMV@15% O2 300 PPMV@15% O2 Pre-Catalyst CO Emissions 7.39 Lbs/MW/Hour 3.35 Kg/MW/Hour

Post-Catalyst CO Emissions 0.500 G/BHP/Hr 0.373 G/BKW/Hr Post-Catalyst CO Emissions 60 PPMV@15% O2 60 PPMV@15% O2 Post-Catalyst CO Emissions 1.477 Lbs/MW/Hour 0.670 Kg/MW/Hour

Percentage CO Reduction 80.0 % 80.0 %

Pre-Catalyst VOC Emissions 0.35 G/BHP/Hr 0.26 G/BKW/Hr Pre-Catalyst VOC Emissions 75 PPMV@15% O2 75 PPMV@15% O2 Pre-Catalyst VOC Emissions 1.03 Lbs/MW/Hour 0.47 Kg/MW/Hour

Post-Catalyst VOC Emissions 0.150 G/BHP/Hr 0.112 G/BKW/Hr Post-Catalyst VOC Emissions 32 PPMV@15% O2 32 PPMV@15% O2 Post-Catalyst VOC Emissions 0.443 Lbs/MW/Hour 0.201 Kg/MW/Hour

Percentage VOC Reduction 57.1 % 57.1 %

Pre-Catalyst H2CO Emissions 0.45 G/BHP/Hr 0.34 G/BKW/Hr Pre-Catalyst H2CO Emissions 68 PPMV@15% O2 68 PPMV@15% O2 Pre-Catalyst H2CO Emissions 4.15 Lbs/Hour 1.88 Kg/Hour

Post-Catalyst H2CO Emissions 0.020 G/BHP/Hr 0.015 G/BKW/Hr Post-Catalyst H2CO Emissions 3.0 PPMV@15% O2 3.0 PPMV@15% O2 Post-Catalyst H2CO Emissions 0.184 Lbs/Hour 0.084 Kg/Hour

Percentage H2CO Reduction 95.6 % 95.6 %

Back Pressure Thru Catalyst 3.5 In WC 8.8 mbar

Oxidation Catalyst Volume 3.417 Cu/Ft 0.0967 Cu/Meter Catalyst Element Diameter 47.30 Inches 1200 Millimeters Number of Elements 1 1 Oxidation Catalyst Space Velocity 145,036 SCFH/FT3 145,036 SCMH/M3

.111.!:ii 'Jfl

firwin We've Got Yov Covered Firwin Plus Description Firwin Plus uses a patented technology that manufactures high temperature insulation wool with low bio- persistence. Firwin Plus is an Alkaline Earth Silicate (CAS number: 329211-92-9) offering the same benefits as our standard FWN 1800 but with improved handling strength and enhanced thermal properties.

Firwin Plus x Is manufactured from pure raw materials using a new manufacturing technology. x Has enhanced thermal properties; large nuisance dust particles have been effectively eliminated making the product soft to the touch and less irritating during use. x Is made of long AES fibers x Has the same chemical formulation as Firwin 1800 x Have outstanding insulating properties at elevated temperatures x Offers excellent thermal stability x Retains its original soft fibrous structure up to its maximum continuous use temperature x Is needled from both sides and possesses high strength, before and after heating x Contains neither binder nor lubricant and does not emit any fumes or smell during the first firing x Is flexible, easy to cut and shape and easy to install x Offers low heat storage x Has good resistance to tearing x Is immune to thermal shock x Has good sound absorption x Is exonerated from any carcinogenic classification under note Q of directive 97/69EC 6

Classification Temperature x Rated Temperature 1200°C / 2192°F EN 1094 [Continuous use] x Proven to withstand Continuous use in an oxidizing atmosphere at 1000°C.

Properties Color: White Density: 64, 96, 128, 160 kg/m3 (4, 6, 8, 10) lbs/ft3 Tensile strength: 128 kg/m3 75 kPa Thickness: ¼” – 2” [6.25 – 50mm] Linear Shrinkage; @1000°F [538°C] 2 @1800°F [982°C] 3 @ 2282°F [1250°C] -

High Temperature Performance Permanent linear shrinkage after 24 hours isotherm heating at 1200°C <1%

Chemical Composition SiO2: 62-68% CaO: 26-32% MgO: 3-7% Other: <1%

Firwin Corp., 1685 Flint Road, North York, ON M3J 2W8 Canada Tel: 416.745.9389 • Fax: 416.745.0782 • www.firwin.com

Firwin Plus Thermal Conductivity (ASTM C-201)

W/m.K (BTU in/hr/ft2 /°F)

Mean Temperature 64kg/m3 96kg/m3 128kg/m3 160kg/m3 4lbs/ft2 6lbs/ft2 8lbs/ft2 10lbs/ft2

200°C 392°F 0.06 [0.42] 0.05 (0.35) 0.05 (0.33) 0.05 (0.32)

400°C 752°F 0.26 (1.80) 0.09 (0.62) 0.08 (0.55) 0.08 (0.54)

600°C 1112°F 0.10 (0.69) 0.14 (0.97) 0.12 (0.83) 0.11 (0.79)

800°C 1472°F 0.17 (1.18) 0.21 (1.46) 0.18 (1.25) 0.16 (1.11)

1000°C 1832°F 0.38 (2.63) 0.29 (2.01) 0.25 (1.73) 0.22(1.49)

Firwin Corp., 1685 Flint Road, North York, ON M3J 2W8 Canada Tel: 416.745.9389 • Fax: 416.745.0782 • www.firwin.com

Page 1 of 1

ENGi E-CO PRESSOR THE MOCOUPLES

Thermocouple Ordering Information

11 102" Style

11',obe -j_ ____ .---- TJ,_( ___, A' --

EC~-102-~:~~--_ _,

Junction Calibration Diameter ' ' Len 1 MounUng Ftg. {Table 11 (Table 2) (Tabla 3) lncho:i (T_ab_l_o 4_,_ ____-J

NOTE· For any additional modifications to this assembly, add ·'-MOD" to the end of tho part number ond provide a physical description of the modificat,on.

Table 1 Table 2 Table 3 Table4 Junction Calibration Diameter Mounting Flttl!!_g_ 001:!!P,Uon P/N Doscrl.e_Uon PIN Doscllptlon P/N OoacriptlQl'I Ungrounded l J Type J 118 118 0 D A I 1/8" NPT Ad ustable Cr01.111dod K 1fPO K" 3116 0 0 B i '"'" NP·r Adjualablo f'f j ~ E TJPB 'E 114 1/4 0 D C 1/2" NPT AdJUSl:.lb!G I N ...3/8 l D 1/ 2· NPT Flxod Luu ~'°'-U""" T~N 31s·o o t GG Dual Grounded X Spa !al X s al E ~- NPT AclJuslable LEE Dual ~ I 314" NP I AdJUStable X Special X So ·~1 t Only Avo1lable 111 3i8' d1amele

Example: ECT·102-U-J-1/4-4.5-48-C 102 Style, Type 'J', ¼" diameter sheath, 4.S- acbve lengtti, ½" NPT adiustable mounting fitting

http://www.duro-sense.com/images/duro2011/template/Model-102-ordering.jpg 3/25/2014 DURO-SENSE CORPORATION THERMOCOUPLE WIRE FEP INSULATJON 400"F(204"CJ

Ordering Information:

Wire Gauge "S" Calibrat.i.otl .. '?~,"; .....·. ··.· . ·· Metallic Overbraid (Table 1) Denotes (Tabl~ 2-) . J.)~pptes . >.. (Table 3) c!~~~.~f!rs ·•" .i.D.:ilI)s.x~t~t~;1.:.) Table 1 Table 2 Table 3 Calibration Metallic Overbraid NOTES: ~uge Standard S eoial ss Stainless Steel The choices of gauge and calibration 0 J JJ 1B lnconel represent the most popular constructions 4 K KK CB Copper of this product. However, additional wire 0 T TT gauges and alternate calibrations can be E EE manufactured to meet specific applications. N NN Consult factory for additional information. R n/a s n/a B nla C n/a

Construction + Parallel Conductors with Flame Retardant Extruded FEP Insulation Product Characteristics + Excellent Abrasion Resistance + Excellent Chemical and Solvent Resistance + Excellent Moisture Resistance Applications + Aerospace + Industrial Equipment Testing + Petrochemical Plants Wire Specifications Nominal Conductor Nominal Insulation Thickness Nominal Overall Diameter Approximate Shipping Gauge Size Conductor Overall Weight in. (mm) in. (mm) in. (mm) in. (mm) lbs/mft kg/km 16 0.051 11.290 0.009 0.230 0.012 (0.305) 0.095 X 0.166 (2.410 X 4.220 28 (42) 16$* 0.060 1.520 0.009 0.230) 0.012 (0.305) 0.104 X 0.190 (2,640 X 4.830 30 (45) 20 0.032 0.813 0.009 0.230) 0.010 (0.254) 0.072 X 0.124 (2.337 X 3.912) 12 (18) 20S* 0.038 0.965 0.009 0.230 0.010 (0.254) 0.Q78 X 0.136 (2.464 X 4.166 14 (21) 24 0.020 0.508 0.008 0.200 0.010 (0.254) 0.060 X 0.100 (2.032 X 3.302 8 (12) 24S* 0.024 0.610 0.008 0.200 0.010 (0.254) 0.064 X 0.108 (2.134 X 3.505 9 (13) 30 0.010 <0.254) 0.005 0.130 0.005 (0.130) 0.046 X 0.072 (1.200 X 1.800 3 (5)

* "S" denotes stranded (7-strand) wire.

Tolerances Due to allowances in manufacturing processes, Duro-Sense Corporation reserves the right to ship a variation of± 10% from the quantity of goods ordered. Physical specifications shown are nominal. Shipping weights are an average of all types of conductors and are listed for estimating purposes only. These weights can vary significantly due to different types of spools, reels and/or conductors. The material contained in this document is presented in good faith and believed to be accurate and reliable. However, because testing conditions may vary and material quality or information provided, in whole or in part, by others may be beyond our control, no warranty, expressed or Implied, is given and Dure-Sense Corporation assumes no liability for results obtained or damages incurred through the application of the data presented. REVISIONS BY

NOTES: All wiring to be minimum1 BAWG, per Specification 17320G 2.03.C.3., unless otherwise indicated. Pressure Transducer to be wired with 18AWG Shielded TSP cable. 12/12/15 Added notes DH Thermocouple wiring to be rated for specified T/C use, and included shielded cabling. , e> Ql C w E l l ! 1 1 0 >, -·---1- ~ e> --1- Ql C w MONITOR iii Ql EXTERNAL CONNECTIONS .c"' t: DDDDDDDDDDDD 0 13 14 15 16 17 18 19 20 21 22 23 24 (Wire & Terminations by Contractor) z 1 2 3 4 5 6 7 8 9 10 11 12 ! [J_ DDDDDDDDDDDD C C Ql ~------·- [J_ > SSL 51.21 0 C 0 > SSL 51.21 'iii -~"' > Ql SSL 51.20 a. C > SSL 51.20 ,gi 'i > SSL 51.23 "O Ql > SSL 51.23 "'~ a.Ql (0 ~ M Ql £ C,- s 0 £ <( -~ - a. +24 "O 1 I 1 I SSL 51.19 ,gi • > .E 0 2 1 0 2 1 SSL 51.19 > "'C ~ 0 3 1 0 3 1 OVDC "§ • 0 4 1 0 4 Ashcroft 0 0 "O • o 5 I o 5 Differential ·a.Ql ,s;; a) 8 . a. o 6 I o 6 I _i_ Pressure "O ~ 010 - Transducer :, ea. 0 _l_ ~ 0:: Ql - Post Catalyst K-Type Thermocouple .D 0 0 C C rl "O C 0 "' M :=> ~ M ~ 00 Pre Catalyst K-Type Thermocouple "§. ea. .!!1 Ol ·ic Dote 06 November 2016 _i_ :=> "O Drown DH :c"' I- NR38PS-1-11399-001

Job North River WWTP

Sheet Of 1 Sheets