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Creative Optimization with Additive Manufacturing Webinar - Additive Manufacturing with Particle Size and Shape Analysis Many Additive Manufacturing (also called 3D printing) techniques such as selective laser sintering (SLS), selective laser melting (SLM) and electro-beam melting (EBM) use metal particle powders as a raw material (Aluminum, Titanium, Steel, Nickel, Tungsten and many Alloys). The particle size, size distribution and shape have a strong effect on the manufacturing result. Therefore it is important for manufacturers and suppliers to control the particle size and shape of their powders used in this process. In order to control particle size and shape these parameters must be measured. We discuss how to use the CAMSIZER technology to improve additive manufacturing results by monitoring the incoming particles. Value of Dynamic Image Analysis in 3D additive manufacturing How does Dynamic Image Analysis work? Why two cameras can control and monitor dust and oversize? Check the manufacturing and production of Additive Manufacturing powders Check the incoming raw material and the recycled powder for reuse 1 CAMSIZER XT & CAMSIZER X2 Additive Manufacturing December 5th of 2017 Julie Chen HORIBA Scientific Gert Beckmann Retsch Technology GmbH Processes Classification Technology Description Materials Binder Jetting 3D Printing Creates objects by depositing a Metal, Polymer, Ink-Jetting binding agent to join powdered Ceramic S-Print material. M-Print Direct Energy Direct Metal Deposition Builds parts by using focused Metal powder, Deposition Laser Deposition thermal energy to fuse materials as Metal wire Laser Consolidation they are deposited on a substrate. Electron Beam Direct Melting Material Fused Deposition Modelling Creates objects by dispensing Polymer Extrusion material through a nozzle to build layers. Material Jetting Polyjet Builds parts by depositing small Photo-polymer, Ink-Jetting droplets of build material, which Wax Thermojet are then cured by exposure to light. Powder Bed Direct Metal Laser Sintering Creates objects by using thermal Metal, Polymer, Fusion Selective Laser Melting energy to fuse regions of a powder Ceramic Electron Beam Melting bed. Selective Laser Sintering Sheet Ultrasonic Consolidation Builds parts by trimming sheets of Hybrids, Lamination Laminated Object Manufacture material and binding them together Metallic, in layers. Ceramic VAT Photopoly- Stereolithography Builds parts by using light to Photo-polymer, merisation Digital Light Processing selectively cure layers of material in Ceramic a vat of photopolymer. 3 Processes Classification Technology Description Materials Binder Jetting 3D Printing Creates objects by depositing a Metal, Polymer, Ink-Jetting binding agent to join powdered Ceramic S-Print material. M-Print Direct Energy Direct Metal Deposition Builds parts by using focused Metal powder, Deposition Laser Deposition thermal energy to fuse materials as Metal wire Laser Consolidation they are deposited on a substrate. Electron Beam Direct Melting Material Fused Deposition Modelling Creates objects by dispensing Polymer Extrusion material through a nozzle to build Filament layers. Material Jetting Polyjet Builds parts by depositing small Photo-polymer, Ink-Jetting droplets of build material, which Wax Thermojet are then cured by exposure to light. Powder Bed Direct Metal Laser Sintering Creates objects by using thermal Metal, Selective Laser Melting energy to fuse regions of a powder Fusion Electron Beam Melting bed. Polymer, Selective Laser Sintering Ceramic Sheet Ultrasonic Consolidation Builds parts by trimming sheets of Hybrids, Lamination Laminated Object Manufacture material and binding them together Metallic, in layers. Ceramic VAT Photopoly- Stereolithography Builds parts by using light to Photo-polymer, merisation Digital Light Processing selectively cure layers of material in Ceramic a vat of photopolymer. 4 Processes Type Technologies Materials Fused deposition modeling Thermoplastics, Eutectic metals, Edible materials, Extrusion (FDM) or Fused Filament Rubbers, Modeling clay, Plasticine, Metal clay Fabrication (FFF) (including Precious Metal Clay) Robocasting or Direct Ink Writing Ceramic materials, Metal alloy, Cermet, Metal matrix (DIW) composite, Ceramic matrix composite Light polymerized Stereolithography (SLA) Photopolymer Digital Light Processing (DLP) Photopolymer Powder bed and inkjet head 3D Powder Bed Almost any metal alloy, Powdered polymers, Plaster Printing (3DP) Electron-Beam Melting (EBM) Almost any metal alloy including Titanium alloys Titanium alloys, Cobalt Chrome alloys, Selective Laser Melting (SLM) Stainless Steel, Aluminium Selective Heat Sintering (SHS) Thermoplastic powder Selective Laser Sintering (SLS) Thermoplastics, Metal powders, Ceramic powders Direct metal laser sintering Almost any metal alloy (DMLS) Laminated Object Manufacturing Laminated Paper, Metal foil, Plastic film (LOM) Powder Fed Directed Energy Deposition Almost any metal alloy Electron Beam Freeform Wire Almost any metal alloy Fabrication (EBF3) 5 Processes Type Technologies Materials Fused deposition modeling Thermoplastics, Eutectic metals, Edible materials, Extrusion (FDM) or Fused Filament Rubbers, Modeling clay, Plasticine, Metal clay Fabrication (FFF) (including Precious Metal Clay) Robocasting or Direct Ink Writing Ceramic materials, Metal alloy, Cermet, Metal matrix (DIW) composite, Ceramic matrix composite Light polymerized Stereolithography (SLA) Photopolymer Digital Light Processing (DLP) Photopolymer Powder bed and inkjet head 3D Powder Bed Almost any metal alloy, Powdered polymers, Plaster Printing (3DP) Electron-Beam Melting (EBM) Almost any metal alloy including Titanium alloys Titanium alloys, Cobalt Chrome alloys, Selective Laser Melting (SLM) Stainless Steel, Aluminium Selective Heat Sintering (SHS) Thermoplastic powder Selective Laser Sintering (SLS) Thermoplastics, Metal powders, Ceramic powders Direct metal laser sintering Almost any metal alloy (DMLS) Laminated Object Manufacturing Laminated Paper, Metal foil, Plastic film (LOM) Powder Fed Directed Energy Deposition Almost any metal alloy Electron Beam Freeform Wire Almost any metal alloy Fabrication (EBF3) 6 Manufacturing of Metal Powders Direct iron ore reduction (into iron powder) (+) Fast (-) but irregular particle shape Atomization (iron and other metals) Gas atomization (+) Smoother rounder shape and narrow size distribution (-) but slower and cost intensive Liquid atomization (+) Fast (-) but irregular particle shape and wider size distribution © Retsch Technology GmbH 7 Classification of Metal Powders Separating Particle Sizes and Shapes (for manufacturing and/or testing) Size Classification: - Sieving or Air Classification Shape Classification: - Sieving with special shaped meshes - Sieving (fast and slow) - Air Classification © Retsch Technology GmbH 8 Recycling of Metal Powders Separating Particle sizes by Sieving or Air Classification After Atomization (Sieving or Air Classification ) For Recycling (Sieving off defects, dust, twins, agglomerates) © Retsch Technology GmbH 9 Example of Additive Manufacturing with Laser Sintering 10 Example for 3D printing © Retsch Technology GmbH 11 AM (Metal, Polymer and Ceramic Powder) Applications Plastic, Ceramic & Metal Powder Automotive, Airospace Industry, Fast Prototyping => small numbers => individual modifications Paper => Plastics => Metal Laser Melting (3D Metal Printing) Vacuum or Nylon Casting © Retsch Technology GmbH 12 3D Printing of Metal Construstions 3D printing with metal: The final frontier of additive manufacturing © Retsch Technology GmbH 13 CAMSIZER XT 3D Printing & Rapid Prototyping © Retsch Technology GmbH 14 3D Printing © Retsch Technology GmbH 15 3D Printing © Retsch Technology GmbH 16 Measuring Principle Digital Image Analysis STATIC DYNAMIC (ISO 13322-1) (ISO 13322-2) • Particles do not move during measurement • Particles in motion relative to camera • High resolution > 0,5 μm • Few 100 particles are analyzed • Resolution > 1 μm (low statistic) • Few million particles are analyzed • Limited measurement range (representative measurement) • Time consuming • Wide measurement range • Particles detected in stable orientation • Fast (2 Dimensions) • Particles measured in random orientations (3 Dimensions) © Retsch Technology GmbH 17 Content Instrument 1. Measurement principle 2. Results Applications 3. Markets and applications 4. Alternative analysis methods © Retsch Technology GmbH 18 CAMSIZER P4 (What‘s new) CAMSIZER P4 © Retsch Technology GmbH 20 Measurement Range Accurate measurement of big particles is not possible, even if they fit into the field of view: Upper measurement Big particles are limit defined by the touching the edge too field of view often reliable quantification not possible. Particle size ~ 1/3 of field of view © Retsch Technology GmbH 21 Two Camera-System (CAMSIZER P4, XT and X2) Large amount Small particles in of big particles high resolution Basic Camera Zoom Camera © Retsch Technology GmbH 22 Resolution ISO 13322-2: Smallest detectable CCD Basic CCD Zoom particle: 1 pixel One pixel is element of a projection when at least half of the pixel is covered. © Retsch Technology GmbH 23 Measurement principle (CAMSIZER XT) Advanced, patented optics design Sample flow Basic Camera Light source 2 Zoom Camera Light source 1 © Retsch Technology GmbH 24 New Optical Design of CAMSIZER X2 Advanced, patented optical design © Retsch Technology GmbH 25 Comparison CAMSIZER XT CAMSIZER X2 Why is perpendicular orientation*