Organic Data Validation Report Soil Samples Collected June 4,1997 Brodhead Creek, Stroudsburg, Pa

ENVIRONMENTAL RESEARCH AND CONSULTING, INC. 112 COMMONS COURT CHADDS FORD, PA 19317

ORGANIC DATA VALIDATION REPORT SOIL SAMPLES COLLECTED JUNE 4,1997 BRODHEAD CREEK, STROUDSBURG, PA

JULY 1997

ACRES INTERNATIONAL CORPORATION 140 John James Audubon Parkway Amherst, New York 14228-1 1 80

AR302871* TABLE OF CONTENTS

1 NARRATIVE ...... 1 2 OVERVIEW ...... 1 3 SUMMARY ...... 1 4 MAJORPROBLEMS ...... 1 5 MINOR PROBLEMS ...... 2 8 NOTES ...... "...... 2 7 REPORT CONTENT ...... 2 8 ATTACHMENTS ...... "...... '...... 3

APPENDICES APPENDIX A - GLOSSARY OF DATA QUALIFIER CODES APPENDIX B - DATA SUMMARY FORMS^ APPENDIX C- RESULTS AS REPORTED BY THE LABORATORY FOR ALL TARGET COMPOUNDS APPENDIX D - REVIEWED AND ACCEPTED TENTATIVELY IDENTIFIED COMPOUNDS APPENDIX E - SUPPORT DOCUMENTATION

AR302875 1 NARRATIVE

Date: July 28,1997

Subject Organic Data Validation for Sample Delivery Group (SDG) #BRH01 Brodhead Creek • Stroudsburg, Pennsylvania From: James R. Stachowski. Environmental Specialist Acres International Corporation

To: Harold M. Brundage III Environmental Research and Consulting, Inc.

2 OVERVIEW

This report pertains to data validation of fifteen (15) soil samples from the Brodhead Creek site, Stroudsburg, Pennsylvania. Laboratory analyses were performed by Lancaster Laboratories, Inc. for semivolatile organics in accordance with EPA Statement of Work (SOW) No. OLM 03.2. 'v .•• • Analyses were performed as Delivered Analytical Services (DAS) to Environmental Research and Consulting, Inc. 3 SUMMARY

All samples were successfully analyzed.

•— * 4 MAJORPROBLEMS ,

During the validation, no problems were'identified that seriously affect data usability.

AR302876 MINOR PROBLEMS

During the validation, no biases were identified that required placement of data qualifiers M*. "UJ". -K', V.or-UL". -

6 NOTES

• Continuing calibration percent difference values (%D) were outside the ± 25% criterion for N-Nitroso-dt^vpropyiamine for continuing calibrations performed on June 13,1997 at 1526 (30.3%) and June 19,1997 at 03:54 (29.4%). The relative response factors (RRF) of this compound for each continuing calibration were) 0.05. N-Nitroso-di-n-propylamine was not identified in the samples tested and no action was taken. • • Continuing calibration percent difference values*(%D) were outside the ± 25% criterion for compounds (listed below) which have historical performance data indicating poor response and/or erratic behavior. These compounds have no contractual %D limits. All continuing calibration RRFs were) 0.05.

Calibration Date/Time Compound %D 8/13-15:23 2,2'-oxybis (1- Chloropropana) 31.4 2-Nitroanilin9 37.2 8/19-03:54 2,2'-oxybis (1- Chloropropane) 32.3 2-Nitroaniline 32.0 Di-n-octylphthalate 29.3

D-n-octylphthalate was detected in sample BRH31 (95J vg/9) which is associated with the 8/19 calibration. 2,2'-oxybis (1-Chloropropana) and 2-Nitroaniline were not detected in associated samples. No action was taken.

An unknown compound (RT=11.42 min) was reported in method blank sample SBLKLA181J at 80J ug/f. This unknown was not identified in the corresponding samples.

Several non-target compounds were tentatively identified in an samples analyzed.

AR302877 7 REPORT CONTENT

Data were reviewed-in accordance with National Functional Guidelines for Organic Data Review, as modified for use in EPA Region III. The text of this report addresses only those problems which affect data usability.

8 ATTACHMENTS

The following appendices and their contents are included:

• Appendix A -Glossary of Data Qualifier Codes

This appendix contains a listing of all organic data qualifiers used in Region III and their definitions.

• Appendix B - Data Summary Forms Included are Data Summary Forms for all fractions analyzed. Information on the Data Summary Forms includes: organic fraction identified, sample matrix, concentration units, site, sampling date(s), sample numbers, dilution factors used, sample locations, sample identification, contract required quantitation Emit for each anafyte, all target analytes, all positive results and quantitation limits with qualifier codes, where applicable. • Appendix C - Results as Reported by the Laboratory for all Target Compounds

Appendix C contains photocopies of all of the Form Is.

• Appendix D • Reviewed and Accepted Tentatively Identified Compounds

Appendix D contains photocopies of the Tentatively Identified Compounds forms (Form I SV - TIC) for each sample.

• Appendix E • Support Documentation

Appendix E includes all support documentation to substantiate the findings described in the narrative.

-3-

AR302878 GLOSSARY O? DATA QUALIFIER COOES (ORGANIC)

CODES RELATED TO IDENTIFICATION (confidence concerning presence or absence of compounds) U =* Hot detected. The associated number indicates approximate sample concentration necessary to be detected. NO CODE « Confirmed identification. B = Not detected substantially above the level reported in laboratory or field blanks. R = Unusable result. Analyte may or may not be present in the sample. N « Tentative identification. Consider present. Special methods Bay be needed to conform its presence or absence in future sampling efforts.

• CODES RELATED TO OaANTITATION ' (can be used for both positive results and sample guantitation limits): • J «* Analyte present. Reported value may . not be accurate or precise. K = Analyte present. Reported value may be biased high. Actual value is expected to be lower. • * . L = Analyte present. Reported value may be biased low. Actual value is expected -to be higher. UJ =» Not detected. Quantitation limit may be inaccurate or imprecise. UL =» Not detected. Quantitation limit is probably higher. OTHER CODES NJ = Qualitative identification questionable due to poor resolution. Presumptively present at approximate quantity. . Q = No analytical result.

AR302879 ! - • ' • . •• -•.-.:-•••• .,--.-•. -: .--'>., - •5-/^.•».-•',----•> -•••.•-.-;:•>• •••:• ^.i--..--..-...... '-...>;-^-:>.^ ^.j'.-v.--:..-.. .• •'•;-:r::.::> The "x* flag added on the Form ISV-TIC indicates that the Tentatively Identified Compound could be an isomer of the given compound.

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11______AR302888 • *"• -. t • *, " -'*-' . ."--" AR302889 , s IB •:, EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET BRHS1 Name: LANCASTER LABS , Contract: Ssab Code: LANCAS Case No.: ____. SAS No.: ____. SDG No.: __ Matrix: (soil/water) SOIL . Lab Sample ID: 2723076 Sample wt/vol: 30 (g/mL) G Lab File ID: >JF245 Level: (low/med) LOW Date Received: 06/06/97 % Moisture: 4 decanted: (Y/N) N Date Extracted: 06/10/97 Concentrated Extract Volume: 500(uL) Date Analyzed: 06/18/97 Injection Volume: 2.0 (uL) Dilution Factor: 1.0 GPC Cleanup: (Y/N) Y pH: ____. CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q

108-95-2————— Phenol;______; 340 U 111-44-4-———— bis (2-cnioroetnyi) etner 340 U 95-57-8—————— 2-Chlorophenol______" 340 U 541-73-1————— 1,3-Dichlorobenzene___ 340 U 106-46-7——-—— 1,4-Dichlorobenzene___ 340 U 95-50-1————— l,2-Dichlorobenzene 340 U 95-48-7—————— 2-Methylphenol ——— 340 U 108-60-1-—-—— 2 , 2' -oxybis (1-cnxoropropane) 340 U 106-44-5————— 4-Methylphenol_____ 340 U 621-64-7————- N-Nitroso-di-n-propyiamine 340 U 67-72-1————— Hexachloroethane____ • 340 U 98-95-3————•— Nitrobenzene__ _ _ ^, _ ___ 340 U 78-59-1——-—— Isophorone 340 U 88-75-5-———•— 2-Nitrophenoj. 340 U 105-67-9————— 2,4-Diroethylpnenoi ~ 340 U 111-91-1————— bis(2-Chloroethoxy)metnane 340 U 120-83-2————— 2,4-Dichlorophenol — 340 U 120-82-1-———— 1,2,4-Trichlorobenzene 340 U 91-20-3—————— Naphthalene 340 U 106-47-8————— 4-chloroaniiine 340 U 87-68-3—————— Hexachlorobutadiene 340 U 59-50-7—————— 4-Chloro-3-methylphen6T 340 U 91-57-6- 2 -Methylnaphthalene 340 U 77-47-4- Hexachlorocyclopentaaiene 340 U 88-06-2-————— 2,4,6-Trichlprophenol 340 U 95-95-4————— 2,4,5-Trichlbrophenol" 860 U 91-58-7--——— 2-Chloronaphthalene 340 U 88-74-4————— 2-Nitroaniline 860 U 131-11-3————— DimethylphthalaTEe-" 340 U 606-20-2————— 2,6-Dinitrotoluene" 340 U 208-96-8————- Acenaphthylene 340 U 99-09-2—————— 3-Nitroanilihe" 860 U 83-32-9———•— Acenaphthene_ 340 U

FORM I SV-1 OLM03.2

AR302890 1C EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET BRHS1 Lab Name: LANCASTER LABS Contract: ____ .______Lab Code: LANCAS Case No.: ____. SAS No.: ____. SDG No.: ___ . Matrix: (soil/water) SOIL Lab Sample ID: 2723076 t . • Sample wt/vol: 30 (g/mL) G Lab File ID: >JF245 Level: (low/mad) LOW Date Received: 06/06/97 % Moisture: 4 decanted: (Y/N) N Date Extracted: 06/10/97 Concentrated Extract Volume: 500(uL) Date Analyzed: 06/13/97 Injection Volume: 2.0 (uL) Dilution Factor: 1.0 GPC Cleanup: (Y/N) Y pH: ____. CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q

51-23-5 —————— 2 . 4-Dinitrophenol 360 U 100-02-7 ————— 4-Nitroohenol 360 U 132-64-9-- — — — oicenzoturan 340 U 121-14-2 ————— 2 . 4-Dinitrotoluene 340 U 84-66-2 —————— DiethvlPhthalate 340 U 7005-72-3 ———— • 4-cnioropnenyl-phenyTeth"er 340 U 86-73-7 —————— Fluorene ' 340 U 100-01-6- —— — 4-Nitroaniiine '360 U 534-52-1- —— • — — 4 . 6-Dinitro-2vmetuiyipnenoi .360 U 86-30-6 —————— N-Nitrosodiphenylamine (1) 340 U 101-55-3 ————— 4-Broraophenyl-phenylether 340 U iia-74-1 ————— nexachlorobenzene 340 U 87-a e-5 ————— pentachlorophenol 360 U 35-01-8- ———— — pnenantnrena 340 U 120-12-7 —— — — Antnracene 340 U 85-74-8 —————— carbazole 340 U 84-J-74-2- —— •• — Di-n-mrcyJLphttialat'e 340 U 205-44-0 ————— riuoranrhene 340 U 129-oo-Q ——— —— pyrene 340 U 340 U 91-94-1 —————— 3.3'-Dichiorobenzidine 340 U 55-55-3— ——— — senzo(a) anthracene 340 U 117-81-7 ————— bis (2-Ethylhexyl) ph'£n"a"lat'e 340 U 218-01-9 ————— Chrysene • 340 U 340 U 205-99-2 ————— Benzofb! rluoranthene 340 U 207-08-9 ————— senzofK, tluoranthene 340 U bO-32-8 —————— Benzofa pyrene 340 U 193-39-5 ————— indeno(I,2.3-cd)pyrerie 340 U 53-70-3- ———— • DiDenzi a, h) anthracene 340 U 191-24-2 ————— Benzo(g,h,i)pervlene 340 U •*. . i) - cannot: o& separacea trorti uipnenyiamine FORM I SV-2 OLM03.2

AR30289I 3S IB EFA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET BRHS2 Tab Name: LANCASTER LABS Contract: Code: LANCAS Case No.: ____ . SAS No.: ____ . SDG No.: __ _ Matrix: (soil/water) SOIL Lab Sample ID: 2723077 Sample wt/vol: 30 (g/mL) G Lab File ID: >JF246 Level: (low/med) LOW Date Received: 06/06/97 % Moisture: 10 decanted: (Y/N) N Date Extracted: 06/10/97 Concentrated Extract Volume: 500 (uL) Date Analyzed: 06/18/97 Injection Volume: 2.0 (uL) Dilution Factor: 1.0 GPC Cleanup: (Y/N) Y pH: ___ . CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q

108-95-2————— Phenol______370 U 111-44-4————- bis(2-Cftioroetnyi)ether 370 U 95-57-8————— 2-Chlorophenol______" 370 U 541-73-1———— 1,3-Dichlorobenzene___ 370 U 106-46-7-——•— 1,4-Dichlorobenzene 370 U 95-50-1—-———— 1,2-Dichlorobenzene___ 370 U 95-48-7—————— 2-Methvlphenol ——— •370 U 108-60-1———— 2,2' -oxyfcis (1-cnioropropane) 370 U 106-44-5————— 4-Methylphenol______370 U 621-64-7————— N-Nitroso-di-n-propyiamine 370 U 67-72-1————— Hexachloroethane______370 U 98-95-3-—•——- Nitrobenzene 370 U 78-59-1———•—— Isophorone 370 U 88-75-5—————— 2-Nitrophenol 370 U 105-67-9————— 2,4-Dimethylpnenoi 370 U 111-91-1-———— bis(2-Chloroethoxy)metnane 370 U 12*0-83-2————— 2,4-Dichlorophenol — 370 U 120-82-1 -1,2,4-Trichlorobenzen _ ._..-«-. . e 370 U 91-20-3- Naphthalen...... _„.._...___e _ 370 U 106-47-8————— 4-Chloroaniiine 370. U 87-68-3—————— Hexachlorobutadiene 370 U 59-50-7—————— 4 -Chloro-3 -methylpheiio i 370 U 91-57-6—————— 2-Methylnaphthalene 370 U 77-47-4—;———-- Hexachlorocyclopentadiene 370 U 88-06-2—————— 2,4,6-Trichlorophenoi 370 U 95-95-4—————— 2,4,5-Trichlorophenol 920 U 91-58-7—————— 2-Chloronaphthalene 370 U 88-74-4————— 2-Nitroaniline___ 920 U 131-11-3————— DimethylphthalaEe"" 370 U 606-20-2————— 2,6-Dinitrotoluene~ 370 U 208-96-8————— Acenaphthylene__J 370 U 99-09-2-——•—• 3-Nitroanlline___ 920 U 83-32-9———— Acenaphthene____ 370 U

FORM I SV-1 OLM03.2

AR302892 54 1C EPA SAMPLE NO SEMTVOLATILE ORGANICS ANALYSIS DATA SHEET BRHS2 Lab Name: LANCASTER LABS Contract: Lab Code: LANCAS Case No.: ______. SAS No.: ____ . SDG No. : . Matrix: (soil/water) SOIL Lab Sample ID: 2723077 Sample' wt/vol: 30 (g/mL) G Lab File ID: >JF246 Level: (low/med) LOW Date Received: 06/06/97 % Moisture: 10 decanted: (Y/N) N Date Extracted: 06/10/97 Concentrated Extract Volume: 500 (uL) Date Analyzed: 06/13/97 Injection Volume: 2.0 (uL) Dilution Factor: 1.0 GPC Cleanup: (Y/N) Y pH: ___ . CONCENTRATION UNITS: CAS NO. COMPOUND ' (ug/L or ug/Kg) UG/KG Q

51-28-5—————— 2,4-Dinitrophenol 920 U 100-02-7————— 4-Nitrophenol____ 920 U 132-64-9————• Dibenzofuran 370 U 121-14-2————— 2,4-Dinitrotoluene 370 U 34-66-2—————— Diethylphthalate ' 370 U 7005-72-3———— 4-chlorophenyl-pnenyietner 370 U 36-73-7————— Fluorene ______~ 370 U 100-01-6————— 4 -Ni troanii me 920 U 534-52-1———— 4,6-Dinitro-2:-methyiphenoi 920 U 86-30-6—————— N-Nitrosodiphenylamine (!)____ 370 U 101-55-3—————• 4-Broraophenyl-phenylether_____ 370 U 118-74-1————— Hexachlorobenzene 370 U 37-86-5—•————• Pentachlorophenol" 920 U 85-01-8————— Phenanthrene___~ 43 J 120-12-7———— Anthracene 370 U 86-74-3—————— Carbazole 370 U 84-74-2———— Di-n-butyipntnaiate 370 U 2O6-44-0————— Fluoranthene____; 130 J 129-00-0———— Pyrene 120 J 85-68-7—————• Butylbenzyipntnaiate 370 U 91-94-1—————— 3,31 -Dichlorobenzidinir 370 U 56-55-3————• Benzo(a) anthracene 61 J 117-81-7————— bis(2-Ethylhexyl)ppntnaiati e 370 U 213-01-9————— Chrvsene 36 J 117-84-0—•——— Di-n-octylpjitnaiate 370 U 205-99-2————— Benzo b)fluoranthenX?!0flub": e 110 J 207-08-9————'- Benzo k) f luoranthene" 39 J 50-32-8—————— Benzo i[aipvtene. 74 J 193-39-5————— Indeno (1,2.3 -ca) py r ene 60 J 53-70-3————— Dibenz( a, h \ anthracene 370 U 191-24-2————— Benzo(g,h,i)perylene "~ 370 U lj - Cannot oa separated trom Dipnenylamine FORM I SV-2 OLM03.'2

AR302893 5S IB EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET BRHS8 Lab Name: LANCASTER LABS n Contract;'-' Code: LANCAS Case No.: ____. SAS No.: ____. SDG No.: Matrix: (soil/water) SOIL Lab Sample ID: 2723078 Sample'wt/vol: 30 (g/mL) G Lab File ID: >JF247 Level: (low/med) LOW Date Received: 06/06/97 % Moisture: 36 decanted: (Y/N) N Date Extracted: 06/10/97 Concentrated Extract Volume: 500(uL) Date Analyzed: 06/18/97 Injection Volume: 2.0 (uL) Dilution Factor: 1.0 GPC Cleanup: (Y/N) Y pH: ___. CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q

108-95-2————— Phenol •______520 U 111-44-4————— bis (2-ChioroetnyjL) ether 520 U 95-57-8————— 2-Chlorophenol____' 520 U 541-73-1————— 1,3-Dichlorobenzene___ 520 U 106-46-7————• l, 4-Dichlorobenzene___ 520 U 95-50-1————— 1,2-Dichlorobenzene 520 U 95-48-7————— 2-Methylphenol ' 520 U 108-60-1————_-_ ,. _ — _,2,2'-oxybis(l-_ _„.__,_ ChloropropaneC y '520 U 106-44-5————— 4-Methylphenol______520 U 621-64-7————— N-Nitroso-di-n-propyiamxne— 520 U 67-72-1—————— Hexachloroethane______"_ 520 U 98-95-3—————— Nitrobenzene ~"—"—— _ 520 U 78-59-1—————— Isophorone 520 U 88-75-5—————— 2-Nitrophenoi 520 U 105-67-9————— 2,4-Dimethylpnenoi —— 520 U lil-91-1———— bis (2-Chloroethoxy) metnane 520 U 120-83-2————— 2,4-Dichlorophenol — 520 U 120-82-1———— 1,2,4-Trichlorobenzene____ 520 U 91-20-3—————— Naphthalene______; 520 U 106-47-8————— 4-Chloroaniiine 520 U 87-68-3—————— Hexachlorobutadiene______520 U 59-50-7—————— 4-Chloro-3 -methylphenoi 520 U 91-57-6————— 2-Methylnaphthalene 520 U 77-47-4—•—•—— Hexachlorocyclopentactiene 520 U 88-06-2—————— 2,4,6-Trichlorophenol '—— 520 U 95-95-4————9 ^ & *f f —————————— 2,4,5-TrichIoropheno<• , 1 , —' — ±JL _>V>*i_.W_ WMitCiilV 1300 U 91-58-7——•—•— 2-Chloronaphthalene 520 U 88-74-4————— 2-Nitroaniline 1300 U 131-11-3————— Dimethylphthal_TEe~~ 520 U 606-20-2————— 2,6-Dinitrotoluene" 520 U 208-96-8——,—— Acenaphthylene 520 U 99-09-2————— 3-Nitroaniline" 1300 U 83-32-9—!—•——— Acenaphthene_" 520 U

FORM I SV-1 OLM03.2

AR30289t» 1C EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET BRHS3 Lab Name: LANCASTER LABS Contract: Lab Code: LANCAS Case No.: ____. SAS No.: ____. SDG No.: ____*. Matrix: (soil/water) SOIL Lab Sample ID: 2723073 Sample wt/vol: 30 .(g/mL) G Lab File ID: >JF247 Level: * (low/med) LOW Date Received: 06/06/97 % Moisture: 36 decanted: (Y/N) N Date Extracted: 06/10/97 Concentrated Extract Volume: 500(uL) Date Analyzed: 06/13/97 Injection Volume: 2.0 (uL) Dilution Factor: 1.0 GPC Cleanup: (Y/N) Y pH: ____. CONCENTRATION UNITS: CAS NO. COMPOUND . (ug/L or ug/Kg) UG/KG " Q

51-28-5————— 2,4-Dinitrophenol 1300 U 100-02-7————— 4-Nitrophenol__' 1300 U 132-64-9-——— Dibenzoruran 520 U 121-14-2————_l» A _L •_>** -to — 2,4-DinitrotoluenA * *w W-bAi^ W>J» W WW«J» V4Q e 520 U 84-66-2—————— DietHylphthalate 520 U 7005-72-3-—•——• 4-Chlorophenyl-pnenyietner 520 U 36-73-7—————— Fluorene______520 U 100-01-6————— 4-NitroaniJiine "~ •1300 U 534-52-1———— 4,6-Dinitro-2-methyiphenox 1300 U 86-30-6————— N-Nitrosodiphenylamine (1) — 520 U 101-55-3————— 4-Bromophenyl*phenylether__ 520 U 118-74-1——•—- Hexachlorobenzene 520 U 87-36-5—————— Pentachlorophenol" 1300 U 85-01-8—————• Phenanthrene___~ 78 J 120-12-7———— Anthracene^_____ 520 U 86-74-8———— Carbazole 520 U S4.-74-2——•——• Di-n-butyipntnaiatty^ e 520 U 206-44-0———— Fluorantnenthe e 150 J 129-00-0————— Pyrene______130 J 85-68-7———•—— Butylbenzyipntnaiata 520 U 91-94-1————— 3,31 -Dichlorobenzidine 520 U 56-55-3————— Benzo (a) anthracene 91. J 117-81-7————— bis(2-Ethylhexyl)pntnaiate 520 UJ 218-01-9———— Chrysene 110 J 117-84-0—••——— Di-n-octyiphtnaiate 520 U 205-99-2————"• " ' — Benz~ o (b"'' f luoranthene" 130 J 207-03-9————— Benzo (k fluoranthene" 520 U 50-32-3—————— Benzo(a] pyrena_..__.______93 J 193-39-5————— Indeno (: L, 2.3-ca; pyrene 520 U 53-70--3—————— Dibenz(a,hjanthracene ' 520 U 191-24-2————• Benzo (g, h, i) perylene___ 520 U i) - cannot oe separated from uipnenyiamane FORM I SV-2 OLM03.2,

AR302895 IB EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET BRH14 Lab Name: LANCASTER LABS • : Contract: tb Code: LANCAS Case No.: ____. SAS No.: . . SDG No.: __ Matrix: (soil/water) SOIL Lab Sample ID: 2723079 Sample * wt/vol: 30 '(g/mL) G Lab File ID: >JF248 Level: (low/med) LOW Date Received: 06/06/97 % Moisture: 14 decanted: (Y/N) N Date Extracted: 06/10/97 Concentrated Extract Volume: 500(uL) Date Analyzed: 06/18/97 Injection Volume: 2.0 (uL) Dilution Factor: 1.0 GPC Cleanup: (Y/N) Y pH: ___. CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q

108-95-2————— Phenol______380 U 111-44-4————— bis(2-cnioroetnyi)etner 380 U 95-57-8————— 2-Chlorophenol____. 380 U 541-73-1————— 1,3-Dichlorobenzene______380 U 106-46-7————— 1,4-Dichlorobenzene______380 U 95-50-1———•— 1,2-Dichlorobenzene______380 U 95-48-7—————— 2-Methyl Phenol 380 U 108-60-1———— 2,2'-oxybis(l-cnioropropane) 380 U 106-44-5————— 4-Methylphenol______380 U 621-64-7————— N-Nitroso-di-n-propyianune "~ 380 U 67-72-1————— Hexachloroethane______380 U 98-95-3—————— Nitrobenzene______. 380 U 78-59-1————— Isophorone______380 U 88-75-5—————— 2-Nltrophenoi 380 U 105-67-9——•—— 2.4 -Dimethyl pnenoi "~ 380 U 111-91-1————— bis(2-Chloroethoxy)metnane 380 U 120-83-2———— 2,4-Dichlorophenol — 380 U 120-82-1————— 1,2,4-Trichlorobenzene 380 U 91-20-3————— Naphthalene____ _ ' 380 U 106-47-8-————— 4 -Chloroaniiine 380 U 87-68-3————— Hexachlorobutadiene 380 U 59-50-7—————— 4 -Chloro-3 -methylphenoi 380 U 91-57-6-————— 2-Methylnaphthalene —' 380 U 77-47-4-————— Hexachlorocyclopentaaiene 380 U 88-06-2————— 2,4,6-Trichlorophenol___' 380 U 95-95-4—————— 2,4,5-Trichlorophenol 960 U 91-58-7-——-—— 2-Chloronaphthalene 380 U 88-74-4————— 2-Nitroaniline 960 U 131-11-3————— Dimethylphthala^F" 380 U 606-20-2————— 2,6-Dinitrotoluene~ 380 U 208-96-8————— Acenaphthylene___" 380 U 99-09-2————— 3-Nitroaniline——— 960 U 83-32-9—————— Acenaphthene_ 380 U

FORM I SV-1 OLM03.2

AR302896 154 1C EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET BRH14 Lab Name: LANCASTER LABS Contract: Lab Code: LANCAS Case No.: ____. SAS No.: ____. SDG No.: Matrix: (soil/water) SOIL Lab Sample ID: 2723079 Sample wt/vol: 30 (g/mL) G Lab File ID: >JF243 Level: (low/med) LOW Date Received: 06/06/97 % Moisture: 14 decanted: (Y/N) N Date Extracted: 06/10/97 Concentrated Extract Volume: 500(uL) Date Analyzed: 06/13/97 Injection Volume: 2.0 (uL) Dilution Factor: 1.0 GPC Cleanup: (Y/N) Y pH: ____. CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Xg) UG/KG Q

51-28-5————— 2,4-Dinitrophenol 960 U 100-02-7————— 4-Nitrophenol___" 960 U 132-64-9————— Dibenzoluran 330 U 121-14-2————— 2,4-Dinitrotoiuene • —— 330 U 84-66-2————— Diathylphthalate 330 U 7005-72-3———— 4-Chlorophenyl-pnenyietner 330 U 86-73-7————— Fluorene______~_ 330 U 100-01-6————— 4-Nitroanj.j.ine 960 U 534-52-1————— 4,6-Dinitro-2-metnyipnenoi 960 U 36-30-6————— N-Nitrosodiphenylamine (1)" 330 U 101-55-3-———— 4-Bromophenyr-pnenylether_J 330 U 113-74-1———•— Hexachlorobenzene 330 U 87-86-5—————— Pentachlorophenol 960 U 85-01-3——•—— Phenanthrene___ 330 U 120-12-7————— Anthracene_j____ 330 U 86-74-8——•——•— Carbazole 330 U 84-74-2-————— Di-n-butyipntnaiate 330 U 2 Q 6-4 4-0————— Fluoranthene______51 J 129-00-0——•—— Pyrene______61 J 85-68-7—————• Butylbenzyipntnaiate 330 U 91-94-1————— 3,31 -Dichlorobenzidine" 330 U 56-55-3-—•———• Benzo (a) anthracene 330 U 117-81-7————— bis (2-Etnylhexyl) pntnaiate 330 U 218-01-9————— Chrysene 47 J 117-84-0————— Di-n-octyipntnaiate 330 U 205-99-2—————— " - — -Benzo(b —_-«_»jluoranthene. " 330 U 207-08-9————— Benzofk flubranthena" 330 U 50-32-8————— Benzo (a,pyren _..__.._____e _ 51 J 193-39-5————— Indeno (.1,2/* X >•3* -ca ___ •:> pyrene 330 U 53-70-3—————— Dibenzf a, h) anthracene 330 U 191-24-2————— Benzo(g,h,i)perylene 330 U l) - cannot &e separated zirom Dipnenyiamine FORM I SV-2 OLM03.,2

flR302897 15S IB EFA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET BRH16 Tab Name: LANCASTER LABS Contract: Code: LANCAS Case No.: ____. SAS No.: ____. SDG No.: ____ Matrix: (soil/water) SOIL Lab Sample ID: 2723080 Sample wt/vol: 30 (g/mL) G Lab File ID: >JF249 Level: (low/med) LOW Date Received: 06/06/97 % Moisture: 8 decanted: (Y/N) N Date Extracted: 06/10/97 Concentrated Extract Volume: 500(uL) Date Analyzed: 06/18/97 Injection Volume: 2.0 (uL) Dilution Factor: 1.0 GPC Cleanup: (Y/N) Y pH: ____. CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q

108-95-2————— Phenol,:______360 U 111-44-4-———— bis(2-cnioroetnyi> ether 360 U 95-57-8————— 2-Chlorophenol____'. " 360 U 541-73-1————— 1,3-Dichlorobenzene______360 U 106-46-7———— 1,4-Dichlorobenzene___ 360 U 95-50-1————— 1,2-Dichlorobenzene______360 U 95-48-7—————— 2-Methylphenol ——— 360 U 108-60-1———— 2,2' -oxybis (1-Chioropropane) '360 U 106-44-5————— 4-Methylphenol____ 360 U 621-64-7———— N-Nitroso-di-n^propyiamine 360 U 67-72-1———»— Hexachloroethane______360 U 98-95-3-———— Nitrobenzene_ _ 360 U 78-59-1————- Isophorone 360 U 88-75-5————— 2-Nltrophenol 360 U 105-67-9—«——— 2,4 -Dimethylphenol ~" 360 U 111-91-1————— bis (2-Chloroethoxy> metnane 360 U 12-0-83-2————— 2,4-Dichlorophenol — 360 U 120-82-1———— l, 2,4-Trichlorobenzene 360 U 91-20-3—————— Naphthalene______~ 360 U 106-47-8——•— 4 -Chloroanii me 360 U 87-68-3————— Hexachlorobutadiene 360 U 59-50-7———~ 4-Chloro-3-methylphenoi 360 U 91-57-6————— 2-Methylnaphthalene ——— 360 U 77-47-4—————— Hexachlorocyclopentadiene 360 U 88-06-2————— 2,4,6-Trichlorophenol 360 U 95-95-4—————— 2,4,5-Trichlorophenol" 900 U 91-58-7—————— 2-Chloronaphthalene_" 360 U 88-74-4————— 2-Nitroaniline 900 U 131-11-3————— Dimethylphthalate"" 360 U 606-20-2————— 2,6-Dinitrotoluene" 360 U 208-96-8———•— Acenaphthylene___" 360 U 99-09-2—.--—— 3-Nitroana.line___ 900 U 83-32-9—————— Acenaphthene 360 U

FORM I SV-1 OLM03.2

AR302898 192 1C EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET BRH16 Lab Name: LANCASTER LABS Contract: Lab Code: LANCAS Case No.: ____. SAS No.: ____. SDG No.: ^N_-_»VB_-_^--» ^_«M_-_-M«_-_ai Matrix: (soil/water) SOIL Lab Sample ID: 2723030 Sample wt/vol: 30 (g/mL) G Lab File ID: >JF249 Level: (low/mad) LOW Date Received: 06/06/97 % Moisture: 3 decanted: (Y/N) N Date Extracted: 06/10/97 Concentrated Extract Volume: 500(uL) . Date Analyzed: 06/13/97 Injection Volume: 2.0 (uL) Dilution Factor: 1.0 GPC Cleanup: (Y/N) Y pH: ____. CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q

51-28-5—————— 2,4-Dinitrophenol 900 U 100-02-7————— 4-Nitrophenol___: 900 U 132-64-9———— Dibenzoturan 360 U 121-14-2————JL A -_< ^^ -M — 2,4-Dinitrotoiuen4_>«*V J-/*k*l__» W* W WV^«b UG. e 360 U 84-66-2—————— Diethylphthalate 360 U 7005-72-3———— 4-Chlorophenyl-pnenyj.etner "" 360 U 86-73-7————— Fluorene______360 U 100-01-6————— 4-Nitroanmne "" •900 U 534-52-1————— 4,6-Dinitro-2-metnyipnenoi 900 U 86-30-6————— N-Nitrosodiphenylamine (1)Z_ 360 U 101-55-3—•——- 4-Bromophenyl-phenylether__ 360 U 118-74-1———— Hexachlorobenzene______360 U 87-86-5-————- Pentachlorophenol______900 U 85-01-3————— Phenanthrana______.______360 U 120-12-7-———— Anthracene . _ ____ 360 U 86-74-8————— Carbazole 360 U 84-74-2————— Di-n-butyipntnaiate 360 U 2Q'6-44-o——— Fluoranthene______*ythej _ 45 J 129-00-0———— Pyrene____IZZ_III____Z 47 J 85-68-7———•— Butylbenzyipntnaiate 360 U 91-94-1————— 3,31 -Dichlorobenzidine" 360. U 56-55-3———— Benzo (a) anthracen 360 U 117-81-7————— bis(2-Ethylhexyl)pntnaiata 360 U 218-01-9————— Chrysene______360 U 117-84-0—•——— Di-n-octyiphthaiate 360 U -"•-nn--205-99-2————- — — Benz«——o '*-(b» fluoranthena" 360 U 207-08-9————— Berizo(k.fluoranthana" 360 U 50-32-8————- Benzo (a pyren_._..______e _ 360 U 193-39-5————— Indeno (1,2.3-cd) pyrene 360 U 53-70-3——•——— Dibenz( a, hj anthracene 360 U 191-24-2-———— Benzo(g,n,i)perylene_ 360 U 1) - cannot be separatedrrom uipnenyiamine FORM I SV-2 OLM03.2

AR302899 193 IB EFA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET BRH20 Lab Name: LANCASTER LABS - • Contract: Code: LANCAS Case No.: _____. SAS No..: ____. SDG No.: Matrix: (soil/water) SOIL Lab Sample ID: 2723083 Sample Vt/vol: 30 (g/mL) G Lab File ID: XTF252 Level: (low/med) LOW Date Received: 06/06/97 % Moisture: 26 decanted: (Y/N) N Date Extracted: 06/10/97 Concentrated Extract Volume: 500(uL) Date Analyzed: 06/19/97 Injection Volume: 2.0 (uL) Dilution Factor: 1.0 GPC Cleanup: (Y/N) Y pH: ___. CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q

108-95-2————— Phenol ______440 U 111-44-4-——•—- bis(2-Chioroetnyi)ether 440 U 95-57-8————— 2-Chlorophenol____• 440 U 541-73-1————— 1,3-Dichlorobenzene______440 U 106-4 6-7————— l, 4 -Dichl or obenz ene——— 440 U 95-50-1-————— 1,2-Dichlorobenzene 440 U 95-48-7————— 2-Methylphenol . 440 U 108-60-1————__ ._ _ — 2,2'-Oxybis(l-_,______,_ CnloropropaneC r .440 U 106-44-5————— 4-Methylphenol______440 U 621-64-7————— N-Nitroso-di-n-propyiaiaine— 440 U 67-72-1—————— Hexachloroethane______'— 440 U 98-95-3—————— Nitrobenzene ~ 440 U 78-59-1————— Isophorone 440 U 88-75-5—————— 2-Nltrophenoi 440 U 105-67-9————— 2,4-Dimethylphenoi 440 U 111-91-1————— bis(2-Chloroethoxy)metnane 440 U 120-83-2————— 2,4-Dichlorophenol — 440 U 120-82-1————— 1,2,4-Trichlorobenzene______440 U 91-20-3————— Naphthalene ____~~^ 440 U 10-6-47-8————— 4-ChloroaniJLine 440 U 87-68-3—————— Hexachlorobutadiene 44Q U 59-50-7————— 4-Chloro-3-methylphen6T 440 U 91-57-6-————— 2-Methylnaphthalene 440 U 77-47-4-——•—— Hexachlorocycyclopentl 'adiene 440 U 88-06-2—————— 2,4,6-Tri

FORM I SV-1 OI-.-03.2

AR302900 216 EPA SAMPLE NO.

BRH20 Lab Name: LANCASTER LABS . '. Contract: Lab Code: LANCAS Case No.: .___. SAS No.: ___. SDG No.: *.''..* .• % Matrix: (soil/water) SOIL lab Sample ID: 2723083 Sample-wt/vol: 30 JF252 Level: (low/mad) LOW Date Received: 06/06/97 % Moisture: 26 decanted: (Y/N) N Date Extracted: 06/10/97 Concentrated Extract Volume: 500(uL) Date Analyzed: 06/19/97 Injection Volume: 2.0 (uL) ' Dilution Factor: 1.0 GPC Cleanup: (Y/N) Y pH: ___. CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q

51-28-5—————— 2,4-Dinitrophenol 1100 U 100-02-7————— 4-Nitro$henol___: 1100 U 132-64-9————— Dibenzoruran 440 U 121-14-2————±£,J. — Jfct—_>——————— —————— 2,4-DinitrA I •« -/—.41J,—*.*—'WWi—USo toluen. e 440 U 34-66-2————— Diethylphthalate 440 U 7005-72-3———•- 4-Chlorophenyl-pnenyietner 440 U 86-73-7—————— Fluorene______— 440 U 100-01-6————— 4-Nitroaniiine ~* 1100 U 534-52-1———•—• 4,6-Dinitro-2-metnyipnenoi 1100 U 86-30-6————— N-Nitrosodiphenylamine (1) — 440 U 101-55-3-———— 4-Bromophenyl-phenylether____ 440 U 118-74-1————— Hexachlorobenzene______440 U 87-86-5————- Pentachlorophenol______1100 U 85-01-3————— Phenanthrene______440 U 120-12-7———— Anthracene______440 U 86-74-3————— Carbazole 440 U 84-74-2———— Di-n-butyipntnaiate 440 U 206-44-0———— Fluoranthene_____" 120 J 129-00-0————— Pyrene 130 J 85-68-7-—-———• Butylbenzyipntnaiate 440. U 91-94-1—————. 3,31 -Dichlorobenzidine 440 U 56-55-3———— Benzo (a) anthracene______71 J 117-31-7————• bis (2-Ethylhexyl) pntnaiata 440 U 218-01-9—•——— Chrysene 77 J 117-84-0———— Di-n-octyiphtnaiate 440 U 205-99-2————--. _,„ . — Benz«——'^-%_luorantheneo (b ~ 100 J 207-03-9———— Benzo (k.f luoranthene!! 440 U 50-32-3—————— Benzo (a pyren__„______e _ 78 J 193-39-5————> Indeno(..,2.3-cd)pyrene 57 J 53-70-3————— Dibenz( a, hj anthracene 440 U 191-24-2————• Benzo(g,h,i)perylene 440 U 1) - Cannot £>a separated £rom Dipnenyiamine FORM I SV-2 OLMOS.S IB EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET BRH24 Lab Name: LANCASTER LABS ^ Contract: Code: LANCAS Case No.: . SAS No.: ____ . SDG No.: Matrix: (soil/water) SOIL Lab Sample ID: 2723084 Sample Vt/vol : 30 (g/mL) G Lab File ID: >JF257 Level: (low/med) LOW Date Received: 06/06/97 % Moisture: 39 decanted: (Y/N) N Date Extracted: 06/10/97 Concentrated Extract Volume: 500 (uL) Date Analyzed: 06/19/97 Injection Volume: 2.0 (uL) Dilution Factor: 1.0 GPC Cleanup: (Y/N) Y pH: ____ . CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q

108-95-2————— Phenol . 540 U 111-44-4-——— bis (2-cnioroetnyi) etner 540 U 95-57-8————— 2-Chlorophenol____• 540 U 541-73-1———:— 1,3-Dichlorobenzene___ 540 U 106-46-7———— 1,4-Dichlorobenzene___ 540 U 95-50-1—«——— 1,2-Dichlorobenzene___ 540 U 95-48-7————— 2-Methylphenol ——— . 540 U 108-60-1———— 2,2' -oxybis (1-Chioropropane) •540 U. 106-44-5————— 4-Methylphenol 540 U 621-64-7 —— • —— N-Nitroso-di-h-propyiamine 540 U 67-72-1-—— •— — Hexachloroethane ______540 U 98-95-3 ————— Nitrobenzene 540 U 78-59-1 ————— Isophorone^ ______540 U 88-75-5 —————— 2-Nitrophenbi 540 U 105-67-9 ————— 2.4-Dimethylphenoi "" 540 U 111-91-1 — — —— bis (2-Chloroethoxy) metnane 540 U 120-83-2 ————— 2,4-Dichlorophenol — 540 U 120-82-1————— 1,2,4-Trichlorobenzene 540 U 91-20-3————— Naphthalene___ 540 U 106-47-8————— 4-ChloroaniITne 540 U 87-68-3—————— Hexachlorobutadiene___ 540 U 59-50-7————•— 4 -Chloro-3 -methylphenoi 540 U 91-57-6————— 2-Methylnaphthalene ——— 540 U 77-47-4————— Hexachlorocyclopentadiene 540 U 88-06-2-———— 2,4,6-Trichlorophenol 540 U' 95-95-4————— 2,4,5-Trichlorophenol' 1400 U 91-58-7———•—— 2-Chloronaphthalene 540 U 88-74-4————— 2-Nitroaniline 1400 U 131-11-3———— DimethylphthalaEe"" 540 U 606-20-2———— 2,6-Dinitro toluene" 540 U 208-96-8————— Acenaphthylene 480 J 99-09-2————— 3-Nitroaniline' 1400 U 83-32-9—————— Acenaphthene._~ 540 U

FORM I SV-1 OLM03.2

AR302902 263 1C EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET BRH24 Lab Name: LANCASTER LABS Contract: Lab Code: LANCAS Case No.: ____. SAS No.: ____. SDG No.: ____.,, Matrix: (soil/water) SOIL Lab Sample ID: 2723034 Sample wt/vol: 30 (g/mL) G Lab File ID: >JF257 Level: (low/med) LOW Date Received: 06/06/97 % Moisture: 39 decanted: (Y/N) N Date Extracted: 06/10/97 Concentrated Extract Volume: 500(uL) Date Analyzed: 06/19/97 Injection Volume: 2.0 (uL) Dilution Factor: 1.0 GPC Cleanup: (Y/N) Y pH: ___. CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG " Q

51-23-5————— 2,4-Dinitrophenol 1400 U 100-02-7————— 4-Nitrophenol__: 1400 U 132-64-9———— DibenzofUran 540 U 121-14-2 ————— 2,4-Dinitrotoluene - 540 U 84-66-2 —————— Diathvlphthalate 540 U 7005-72-3 ——— — 4-Chlorophenyl-pnenyietner 540 U 86-73-7 ————— Fluorene ______63 J 100-01-6 ————— 4-Nitroanxiine .1400 U 534-52-1 — — — — 4 , 6-Dinitro->2-metnyipnenoi 1400 U 86--30-6 —————— N-Nitrosodiphenylamine (1) 540 U 1011-55-3 ————— 4-Bromophenyl--phenylether 540 U 118-74-1— ——— Hexachlorobenzene 540 U 87-86-5 — • ———— • Pentachlorophenol 1400 U 85-01-8 —————— Phenanthrene__ _ 120 J 120-12-7- ———— • Anthracene 99 J 86-74-8 —————— Carbazole 540 U 84-74-2—•——— Di-n-butyiphtnaiate 540 U 206-44-0————— Fluorantheny-m1 e 230 J 12'9-00-0————— Pyrene______410 J 85-68-7————— Butylbenzyipftthaiate 540 U 91-94-1—————— 3,31 -Dichlorobenzidina" 540 U 56-55-3—————— Benzo (a) anthracene 340. J 117-81-7————— bis(2-Ethylhexyl)pntnaiate 160 J 213-01-9————— Chrysene 410 J 117--84-0— — • — - Di-n-octyipntnaiate 540 U . 205-99-2-! ———— Benzo (b)f luoranthene 630 207-08-9 ————— Benzo (k) f luoranthene 130 50-32-8———50-32-8— —— —— BenzBenzoo (a(a) pyrene______pyrene _ 740 193-39-5-——•—— Indeno(1,2.3-cd)pyrene 550 53-70-3——•——- Dibenz(a,h>anthracen, e 160 191-24-2 ————— Benzo(g,h, i)perylena 570 l) - cannotoe separated rrom Dipnanylamine FORM I SV-2 OLM03.?

AR302903 264 IB . EFA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET BRH27 Lab Name: LANCASTER LABS Contract: \_>ab Code: LANCAS Case No.: ____. SAS No.: ____. SDG No.: Matrix: (soil/water) SOIL Lab Sample ID: 2723085 Sample*wt/vol: 30 (g/mL) G Lab File ID: >JF258 Level: (low/med) LOW Date Received: 06/06/97 % Moisture: 30 decanted: (Y/N) N Date Extracted: 06/10/97 Concentrated Extract Volume: 500(uL) Date Analyzed: 06/19/97 Injection Volume: 2.0 (uL) Dilution Factor: 1.0 GPC Cleanup: (Y/N) Y pH: ____. CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q

108-95-2————— Phenol » _____47O U 111-44-4—•—— bis (2-cnioroetny-.) ether 470 U 95-57-8——————'. 2-Chlorophenol______^__ 470 U 541-73-1-—-——- 1,3-Dichlorobenzene______470 U 106-46-7————— 1,4-Dichlorobenzene______470 U 95-50-1—————— 1,2-Dichlorobenzene______470 U 95-48-7————— 2-Methylphenol 470 U 108-60-1——-—— 2,2'-oxybis(1-Chioropropane) 470 U 106-44-5————— 4-Methylphenol______470 U 621-64-7————— N-Nitroso-di-n-propyiaraine 470 U 67-72-1—————— Hexachloroethane______— 470 U 98-95-3——-—— Nitrobenzene______470 U 78-59-1————— Isophorone 470 U 88-75-5—————— 2-Nltrophenol 470 U 105-67-9————— 2f 4-Dimethylpnenoi_ ~ 470 U 111-91-1————— bis (2-Chloroethoxy)metnane 470 U 120-83-2————— 2,4-Dichlorophenol — 470 U 120-82-1————— 1,2,4-Trichlorobenzene 470 U 91-20-3—————— Naphthalene 58 J 106-47-8-———•— 4-chloroaniiine 470 U 87-68-3—————— Hexachlorobutadiene_____ 470 U 59-50-7—————— 4-Chloro-3-methylphenoi 470 U 91-57-6————— 2-Hethylnaphthalene — 470 U 77-47-4—————— Hexachlorocyclopentadiene 470 U 88-06-2————— 2,4,6-Trichloropnenol 470 U 95-95-4 2,4,5-Trichlorophenol" 1200 U 2-Chloronaphthalene * 470 U 88-74-4—————— 2-Nitroaniline 1200 U 131-11-3————— Dimethylphthalale" 470 U 606-20-2————— 2,6-Dinitrotoluene 470 U 208-96-8————— Accenaphthy1ene - - - e 470 U 99-09-2—————— 3--NitroanilineN ' 1200 U 83-32-9————— Acenaphthene 470 U

FORM I SV-1 OLM03.2

AR302901* 33° 1C EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET BRH27 Lab Name: LANCASTER LABS Contract: Lab Code: LANCAS Case No.: ____ . SAS No.: ____ . SDG No.: Matrix: (soil/water) SOIL Lab Sample ID: 2723035 Sample «wt/vol : 30 '(g/mL) G Lab File ID: >JF258 Level: (low/med) LOW Date Received: 06/06/97 % Moisture: 30 decanted: (Y/N) N Date Extracted: 06/10/97 Concentrated Extract Volume: 500 (uL) Date Analyzed: 06/19/97 Injection Volume: 2.0 (uL) Dilution Factor: 1.0 GPC Cleanup: (Y/N) Y pH: ____ . CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q

51-23-5————— 2,4-Dinitrophenol 1200 U 100-02-7————— 4-Nitroehenol___: 1200 U 132-64-9————— Dibenzoruran 470 U 121-14-2————^_ j.—_,t—_> — ———————— A2,4-Dinitrotoluen * ~r w_>*i_> wj. wt.w _,<—.*= e 470 U 84-66-2—————— Diethylphthalate______470 U 7005-72-3———— 4-chlorophenyl-pnenyietner— 470 U 86-73-7——•——— Fluorene______470 U 100-01-6————— 4-NitroaniJ.j.ne "" '1200 U 534-52-1————— 4,6-Dinitro-2-metnyipnenoi— 1200 U 86-30-6————— N-Nitrosodiphenylamine (1) — 470 U 101-55-3————— 4-Bromophenyl-phenylether____~ 470 U 118-74-1————— Hexachlorobenzene______470 U 87-86-5—————— Pentachlorophenol______1200 U 85-01-8————— Phenanthrena______200 J 120-12-7————— Anthracene______470 U 86-74-8-————— Carbazole 470 U 84-74-2————— Di-n-butyipntnaiate 470 U 206-44-0—————• Fluoranthene______•. 370 J 129-00-0————— Pyrene ______370 J 85-68-7—————— Butvlbenzyiphtnaiate 470 U 91-94-1————— 3,31 -Dichlorobenzidine 470 U 56-55-3—————— Benzo (a) anthracene _____ 160 J 117-81-7————— bis (2-Ethylhexyl) pntnaiate 230 J 213-01-9————— Chrysene______'_ 210 J 117-84-0————• Di-n-octyiphthaJ-ate 470 U 205-99-2————— Benzoi'b. fluoranthene 260 J 207-08-9————— Benzo i k f luoranthene" 99 J 50-32-8-——•—- Benzo a pyren__„______e _ 130 J 193-39-5————— Indeno (..,2.3 -cd) pyrene 160 J 53-70-3————— Dibenz( a, hj anthracene 470 U 191-24-2————— Benzo (g,h,i)perylene 150 J l) - Cannot be separated irom Dipnenyiamine FORM I SV-2 OLM03.2

AR302905 IB EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET BRH29 Lab Name: LANCASTER LABS Contract: Code: LANCAS Case No.: ____. SAS No.: _____. SDG No.: Matrix: (soil/water) SOIL Lab Sample ID: 2723086 Sample wt/vol: 30 (g/mL) G Lab File ID: >JF259 Level: (low/med) LOW Date Received: 06/06/97 % Moisture: 31 decanted: (Y/N) N Date Extracted: 06/10/97 Concentrated Extract Volume: 500(uL) Date Analyzed: 06/19/97 Injection Volume: 2.0 (uL) Dilution Factor: 1.0 GPC Cleanup: (Y/N) Y pH: ___. CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q

108-95-2————— Phenol -______. 480 U 111-44-4——-—• bis(2-cnioroetnyi)etner 480 U 95-57-8—————— 2-Chlorophenol______H~ 480 U 541-73-1————— 1.3-Dichlorobenzene 480 U 106-46-7————— 1,4-Dichlorobenzene 480 U 95-50-1—————— 1,2-Dichlorobenzene______480 U 95-48-7—————— 2-Methylphenol • 480 U 108-60-1————— 2,2' -oxybis (l-cftioropropane) ' 480 U 106-44-5————— 4-Methylphenol______.480 U 621-64-7————— N-Nitroso-di-n-propyiamine 480 U 67-72-1—————— Hexachloroethane _____"_"_ 480 U 98-95-3—————— Nitrobenzene ————————— 480 U 78-59-1—————• Isophorone 480 U 88-75-5————— 2-Nltrophenoi 480 U 105-67-9————— 2,4 -Dimethy Ipnenoi " 480 U 111-91-1————— bis(2-Chloroethoxyj metnane 480 U 12.0-83-2————— 2,4-Dichlorophenol — 480 U 120-82-1————— 1,2,4-Trichlorobenzene 480 U 91-20-3—————— Naphthalene_____ ' 480 U 106-47-8————— 4-ChloroaniTTne 480 U 87-68-3————— Hexachlorobutadiene 480 U 59-50-7—————— 4-Chloro-3-methylphenoT 480 U 91-57-6—————:- 2-Methylnaphthalen2-Methylnaphth« e 480 U 77-47-4-—————— HexachlorocyclopentadienHexachlorocyclc e 480 U 88-06-2—-———— 2,4,6-Trichlorophenol 480 U 95-95-4—————— 2,4,5-Trichlorophenol——— 1200 U 91-58-7————— 2-Chloronaphthalene 480 U 88-74-4————— 2-Nitroaniline 1200 U 131-11-3————— Dimethylphthalate — 480 U 606-20-2———— 2,6-Dinitrotoluene — 480 U 208-96-8———— Acenaphthylene______140 J 99-09-2————— 3-Nitroanlline — 1200 U 83-32-9—————— Acenaphthene ______480 U

FORM I SV-1 OLM03.2

AR302906 C93 1C EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET BRH29 Lab Name: LANCASTER LABS Contract: Lab Code: LANCAS Case No.: ____ . SAS No.: ____ . SDG No.: Matrix: (soil/water) SOIL Lab Sample ID: 2723036 Sample * wt/vol: 30 '(g/mL) G Lab File ID: >JF259 Level: (low/med) LOW Date Received: 06/06/97 % Moisture: 31 decanted: (Y/N) N Date Extracted: 06/10/97 Concentrated Extract Volume: 500 (uL) Date Analyzed: 06/19/97 Injection Volume: 2.0 (uL) Dilution Factor: 1.0 GPC Cleanup: (Y/N) Y pH: ____ . CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q

51-28-5————— 2,4-Dinitrophenol 1200 U 100-02-7-———— 4-Nitrophenol_,_~_ 1200 U 132-64-9————— Dibenzofuran 430 U 121-14-2————_,_<_,—j.i—*———————— _2 *(4-Dinitrotoluan •» —-/A-I—, •-. www_,v_a a 430 U 84-66-2—————— Diathylphthalate______430 U 7005-72-3———— 4-Chlorophenyl-pnenyietner 430 U 86-73-7—————— Fluorene_____ — . 430 U 100-01-6————— 4 -Nitroanii me 1200 U 534-52-1——•—— 4,6-Dlnitro-2-metnyipnenoi 1200 U 86-30-6————— N-Nitrosodiphenylamine (1)_ 480 U 101-55-3————— 4-Bromophenyl-pnenylether 430 U 118-74-1————— Hexachlorobenzene 430 U 8 7-86-5 ————— Pentachlorophenol" 1200 U 85-01-8————— Phenanthrene___" 150 J 120-12-7————— Anthracene_____ 61 J 36-74-3————— Carbazole 430 U 84-74-2—————— Di-n-butyipntnaiate 430 U 206-44-0————— Fluoranthene______•• 420 J 129-00-0————— Pyrene ______450 J 85-68-7-————— Butylbenzyiphtnaiate 430 U 91-94-1—————— 3,31 -Dichlorobenzidine "" 430 U 56-55-3————— Benzo (a) anthracene______230 J 117-31-7————— bis(2-Ethylhexyl)phthaiate_ 300 J 218-01-9—•——— .Chrysene 330 J 117-84-0——— Di-n-octyiphtnajkata 430 U 205-99-2————— Benzo(b) f lubranthana 400 J 207-08-9————— Benzo (k) f luoranthene_ 160 J 50-32-3————— Benzo (a) pyrene______340 J 193-39-5————— Indeno(1,2.3-Cd) pyrene 260 J 53-70-3—•———J J I « — -I——————————————•— DibenzWJ.M—Vll_>f \ a <_>,, l-h){ CZ* anthraceni «-*_-. ClWCli e 63 J 191-24-2—— —— Benzo(g,h,i)perylene 260 J -^trannotoe separated trom oipnenyiamina FORM I SV-2 OLM03.'2

AR302907 IB EPA SAMPLE NO, SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET BRH31 Lab Name: LANCASTER LABS • Contract: '? Code: LANCAS Case No.: _____. SAS No.: ____. SDG No.: Matrix: (soil/water) SOIL Lab Sample ID: 2723087 Sample* wt/vol: 30 '(g/mL) G ' Lab File ID: >JF260 Level: (low/ined) LOW Date Received: 06/06/97 % Moisture: 33 decanted: (Y/N) N Date Extracted: 06/10/97 Concentrated Extract Volume: 500(uL) Date Analyzed: 06/19/97 Injection Volume: 2.0 (uL) Dilution Factor: 1.0 GPC Cleanup: (Y/N) Y pH: ___. CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q

108-95-2————— Phenol , ______490 U 111-44-4-——— bis(2-cnioroetnyi)ether 490 U 95-57-8—————— 2-Chlorophenol 490 U 541-73-1-————— l,3-D:.chlorobenzene___ 490 U 106-46-7————— 1,4-D: .chlorobenzene___ 490 U 95-50-1—————— 1,2-D:.chlorobenzene_____ 490 U 95-48-7—————— 2-Methylphenol ——— • 490 U 108-60-1———— 2,2'-oxybis(1-cnioropropane) ' 490 U 106-44-5————— 4-Methylphenol______.160 J 621-64-7————— N-Nitroso-di-n-propyia-nine 490 U 67-72-1-————— Hexachloroethane______490 U 98-95-3—————— Nitrobenzene ————————— 490 U 78-59-1————— Isophorone 490 U 88-75-5—————— 2-Nitrophenoi 490 U 105-67-9————— 2,4-Dimethylpnenoi 490 U 111-91-1————— bis(2-Chloroethoxy)metnane 490 U 120-83-2————— 2,4-Dichlorophenol — 490 U 12'0-82-l————— 1,2,4-Trichlorobenzene 490 U 91-20-3—————— Naphthalene 490 U 106-47-8————— 4-Chloroaniline 490 u . 87-68-3—————— Hexachlorobutadiene 490 U 59-50-7—————— 4 -Chloro-3 -methylphenol 490 u 91-57-6—————— 2-Methylnaphthalene 490 u 77-47-4-————— Hexachlorocyclopentadiene 490 u 88-06-2—————— 2,4,6-Trichlprophenol 490 u 95-95-4————3'—•—'—'**——————————————— 2,4,5-TrichZ'orophenol

FORM I SV-1 OLM03.2

HR302908 459 1C EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET BRH31 Lab Name: LANCASTER LABS Contract: Lab Code: LANCAS Case No.: ____. SAS No.: ____. SDG No.: ______>->' Matrix: (soil/water) SOIL Lab Sample ID: 2723087 Sample wt/vol: 30-(g/mL) G Lab File ID: >JF260 Level: (low/med) LOW Date Received: 06/06/97 % Moisture: 33 decanted: (Y/N) N Date Extracted: 06/10/97 Concentrated Extract Volume: 500(uL) Date Analyzed: 06/19/97 Injection Volume: 2.0 (uL) Dilution Factor: 1.0 GPC Cleanup: (Y/N) Y pH: ____. CONCENTRATION UNITS: - CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q

51-23-5—————— 2,4-Dinitrophenol 1200 u 100-02-7————— 4-Nitrophenol___~ 1200 u 132-64-9————— Dibenzoturan 490 u 121-14-2————J» A -k _b *t A — 2,4-Dinitr-6 » Tf 4_r^J4Jk Wd-io WWW«I toluen_ U0, e 490 u 34-66-2————— Diethylphthalate______490 u 7005-72-3———— 4-Chlorophenyl-pnenyietner 490 u 86-73-7————— Fluorene 55 J 100-01-6————— 4-Nitroanmne .1200 u 534-52-1————— 4,6-Dinitro-2-metnyipnenoi 1200 u 86-30-6—————— N-Nitrosodipl\enylamine (1) — 490 u 101-55-3————— 4-Bromophenyl-phenylether___ 490 u 118-74-1————— Hexachlorobenzene 490 u 87-36-5—————• Pentachlorophenol" 1200 u 85-01-8————— Phenanthrene___" 660 120-12-7———— Anthracene 120 J 36-74-8—•———— Carbazole 93 J 84-74-2————— Di-n-butyipntnaiate 490 u 206-44-0————— Fluorantnene_____~_ 1000 129-00-0————— Pyrene 1200 85-68-7————- Butylbenzyipntnaiat---—-•-• e 93 J 91-94-1————— 3,31-Dichlorobenzidine, 490 u 56-55-3—————— Benzo (a) anthracene______610 117-31-7—————• bis(2-Ethylhexyl)pntnaiate 1400 213-01-9————— Chrysene______810 117-34-0-————— Di-n-octyiphthaiate 95 J 205-99-2————— Benzo (b)rlupranthene_____ 1000 207-08-9—————• Benzo (k) f luoranthene_____ 360 J 50-32-8——-——• Benzo (aa)) pyr.en pyrene______c _ 700 193-39-5————— Indeno (1,2,3-cd(1,2,3-< ) pyrene 670 53-70-3—————• Dibenz (a.h)an(a, hj anthracenl e 160 191-24-2———— Benzo (g,h,i)parylena_ 670 - cannot oe separated trora- Dipnenyiamine FORM I SV-2 OLM03.2

460 AR302909 IB , EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET BRH33 Name: LANCASTER LABS ' Contract: Code: LANCAS Case No.: ____. SAS No.: ____. SDG No.: __ Matrix: (soil/water) SOIL Lab Sample ID: 2723088 Sample wt/vol: 30 (g/mL) G Lab File ID: >JF261 Level: (low/med) LOW Date Received: 06/06/97 % Moisture: 40 decanted: (Y/N) N Date Extracted: 06/10/97 Concentrated Extract Volume: 500(uL) Date Analyzed: 06/19/97 Injection Volume: 2.0 (uL) Dilution Factor: 1.0 GPC Cleanup: (Y/N) Y pH: ___. CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q

108-95-2————— Phenol / 550 U 111-44-4————— bis (2-Chioroethyi)ether 550 U 95-57-8—————— 2-Chlorophenol______" 550 U 541-73-1————— 1.3-Dichlorobenzene "" 550 U 106-46-7————— 1,4-Dichlorobenzene______550 U 95-50-1—————— 1,2-Dichlorobenzene______. 550 U 95-48-7—————— 2-Hethylphenol .550 U 108-60-1———— 2,2'-oxybis(1-cnioropropane) 550 U 106-44-5————— 4-Methyiphenol 550 U 621-64-7————— N-Nitroso-di-n-propyiamine "" 550 U 67-72-1————— Hexachloroethane______' 550 U 98-95-3-————— Nitrobenzene______550 U 78-59-1—-—-—— Isophorone 550 U 88-75-5—————— 2-Nitrophenoi "" 550 U 105-67-9————— 2,4-Dimethylpnenoi "" 550 U 111-91-1——-— bis(2-Chloroethoxyjmetnane 550 U 120-83-2————— 2,4-Dichlorophenol______' 550 U 120-8 2-1————— 1,2,4 -Trichlorobenz ene 550 U 91-20-3—————— Naphthalene______——— 550 u 106-47-8-———— 4-Chloroaniiine——————— 550 u 87-68-3-————— Hexachlorobutadiene___ 550 u 59-50-7 —————.- 4-Chloro-3-methylphenoi 550 u 91-57-6—————— 2-Methvlnaphthalene 550 u 77-47-4-————— Hexachlorocyclopentadiene ~ 550 u 88-06-2—>——— 2,4,6-Trichlorophenol_____ 550 .u 95-95-4————— 2,4.5-Trichlorophenol' 1400 u 91-58-7-———- 2-Chloronaphthalene 550 u 88-74-4—————— 2-Nitroaniline____ 1400 u 131-11-3————— DimethylphthalaTe— 550 u 606-20-2————— 2,6-Dinitrptoluene 550 u 208-96-8——-—— Acenaphthylene 1800 99-09-2————— 3-Nitroan.iline 1400 u 83-32-9—————— Acenaphthene_ 550 u

FORM I SV-1 OLM03.2

AR3029IO 530 1C EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET BRH33 Lab Name: LANCASTER LABS Contract Lab Code: LANCAS Case No.: ____ . SAS No.: ____ . SDG No.: Matrix: (soil/water) SOIL Lab Sample ID: 2723033 Sample' wt/vol: 30 JF261 Level: (low/med) LOW • Date Received: 06/06/97 % Moisture: 40 decanted: (Y/N) N Date Extracted: 06/10/97 Concentrated Extract Volume: 500 (uL) Date Analyzed: 06/19/97 Injection Volume: 2.0 (uL) Dilution Factor: 1.0 GPC Cleanup: (Y/N) Y pH: ____ . CONCENTRATION UNITS: GAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q

51-28-5————— 2,4-Dinitrophenol 1400 U 100-02-7———— 4-Nitrophenol__' 1400 U 132-64-9————— Dibenzofuran 550 U 121-14-2————— 2.4-Dinitrotoluene 550 U 34-66-2—————— Diethylphthalate * 550 U 7005-72-3———— 4-Chlorophenyl-pnenyietner 550 U 36-73-7————— Fluorene . 220 J 100-01-6————— 4-Nitroaniiine 1400 u 534-52-1————— 4,6-Dinitro-2-met..yip__enoi 1400 u _ ^ 30-6————._. _ — — N-Nitrosodiphenylamin_.«*&«•_ . *«_«_ __« —*»*e (1)->___< — 550 u 101-55-3——- -. - — 4-Bromophenyl-pheny... l ether_____ 550 u 118-74-1————— Hexachlorobenzene_ 550 u 87-86-5————•— Pentachlorophenol_ 1400 u 85-01-8-————— Phenanthrene_____ 200 J 120-12-7————— Anthracene______460 J 86-74-3———•—— Carbazole______550 u 84-74-2————— Di-n-butyipntnaiatty. a 550 u 2.06-44-0———— Fluoranthene______the _ 720 129-00-0—•——— Pyrene______1600 85-68-7————— Butvlbenzyipntnaiate 550 u 91-94-1————— 3,31 -Dichlorobenz idine 550 u 56-55-3————— Benzo (a) anthracene______930 117-81-7————— bis (2 -Ethylhexyl) phtha JLat e 550 u 218-01-9————— Chrysene______1400 117-84-0—-—— Di-n-octyipnthaJrate 550 u 205-99-2————— Benzoib,fluoranthene 1400 207-08-9————— Benzo i k,flupranthene" 500 J 50-32-8—————— Benzoi a pyren_..__„______e _ 1900 193-39-5————— Indeno (:., 2.3 -cd) pyrene 1500 53-70-3—————— Dibenz( a, hj anthracene 420 191-24-2————— Benzo (g,h,i)perylene__ 1600 i) - cannot be separated rrom tupnenyiamine FORM I SV-2 OLM03.'2

AR3029II 53i IB EFA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET BRH34 Lab Name: LANCASTER LABS' •' Contract: Code: LANCAS Case No.: ____. SAS No.: ____. SDG No.: __ Matrix: (soil/water) SOIL Lab Sample ID: 2723089 Sample'wt/vol: 30 (g/mL) G Lab File ID: >JF262 Level: (low/med) LOW Date Received: 06/06/97 % Moisture: 31 decanted: (Y/N) N Date Extracted: 06/10/97 Concentrated Extract Volume: 500(uL) Date Analyzed: 06/19/97 Injection Volume: 2.0 (uL) Dilution Factor: 1.0 GPC Cleanup: (Y/N) Y pH: ____. CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q

108-95-2————— Phenol ,______480 U 111-44-4———•— bis(2-cnioroethyi)ether 480 U 95-57-8—————— 2-Chlorophenol 480 U 541-73-1————— 1,3 -Dichlorobenz ene 480 U 106-4 6-7————— 1,4-Dichlorobenzene 480 U 95-50-1—————— 1,2-Dichlorobenzene______480 u 95-48-7————— 2-Methylphenol ——— 480 u 108-60-1————— 2,2'-oxybis(l-cnioropropane) • 480 u 106-44-5————— 4-Methylphenol 480 u 621-64-7————— N-Nitroso-di-'n-propyiamine 480 u 67-72-1—————— Hexachl or oe thane______— 480 u 98-95-3————— Nitrobenzene______480 u 78-59-1-————— Isophorone 480 u 88-75-5—————— 2-Nltrophenoi 480 u 105-67-9————— 2,4 -Dimethylpnenoi ~ 480 u 111-91-1————— bis (2-Chloroethoxy) metnane 480 u 120-83-2————— 2,4-Dichlorophenol ____— 460 u 120-82-1————— 1.2,4-Trichlorobenzene 480 u 91-20-3—————— Naphthalene___ ——"~~~ 480 u 106-47-8————— 4-Chloroaniiine 480 u 87-68-3 ————— Hexachlorobutadiene 480 u 59-50-7—————— 4 -Chloro-3 -methylphenoi 480 u 91-57-6—————— 2-Methylnaphthalene____ 480 u 77-47-4—————— •. .Hexachlorocyclopentaaien cyclopentac e 480 u. 88-06-2—————— 2,4,6-Trichlorophenol 480 u 95-95-4————— 2,4,5-Trichflorophenor 1200 u 91-58-7—————— 2-Chloronaphthalene " 480 u 88-74-4————— 2-Nitroaniline 1200 u 131-11-3————— DimethylphthalaTEe^ 480 u 606-20-2———— 2,6-Dinitrotoluene 480 u 208-96-8————— Acenaphthylene 49 J 99-09-2————— 3-Nitroaniline" 1200 u 83-32-9-—•——— Acenaphthene 480 u

FORM I SV-1 OLM03.2

AR3029I2 59° 1C EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET BRH34 Lab Name: LANCASTER LABS Contract: Lab Code: LANCAS Case No.: ____. SAS No.: ____. SDG No.: Matrix: (soil/water) SOIL Lab Sample ID: 2723039 Sample, wt/vol: 30 JF262 Level: (low/med) LOW Date Received: 06/06/97 % Moisture: 31 decanted: (Y/N) N Date Extracted: 06/10/97 Concentrated Extract Volume: 500(uL) Date Analyzed: 06/19/97 Injection Volume: 2.0 (uL) Dilution Factor: 1.0 GPC Cleanup: (Y/N) Y pH: ____. CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Xg) UG/KG Q

51-23-5————— 2,4-Dinitrophenol 1200 U 100-02-7————— 4-Nitrophenol___: 1200 U 132-64-9———— Dibenzofuran 430 U 121-14-2———-._>_. — _,•»—_—————————————— 2.4-Dinitrotoiueni | I fcf -»**_> W_i WWWJ. UeC 430 U 84-66-2—————— Diethylphthalate______430 U 7005-72-3———— 4-Chlorophenyl-pnenyietner 430 U 86-73-7———— Fluorene____ 430 U 100-01-6————— 4-Nitroaniiine •1200 U 534-52-1————— 4,6-Dinitro-2-metnyipnenoi 1200 U 86-30-6————— N-Nitrosodiphenylamine (!)___. . 430 U 101-55-3-———— 4-Bromophenyl-phenylether_____ 430 U 118-74-1———— Hexachlorobenzene____• 430 U 87-36-5————— Pentachlorophenol______1200 U 85-01-3————— Phenanthrene______340 J 120-12-7———— Anthracene______74 J 86-74-3—————— Carbazole 430 U 84-74-2—————• Di-n-butyipntnaiate 430 U 205-44-0———— Fluoranthenthty-1. e 520 1-9-00-0———— Pyrene______610 85-68-7—————— Butylbenzyiphtnaiate 430 U 91-94-1————— 3,31 -Dichlorobenzidine" 480 U 56-55-3—•—•—— Benzo (a) anthracene 290 J 117-81-7———— bis(2-Ethylhexyl)pphtnaiat; e 490 218-01-9———— Chrysene ______370 J 117-84-0———— Di-n-octyipntnaiate 430 U 205-99-2————— -- - — Benz-——'^-^fluorantheneo (b. " 390 J 207-08-9———— Benzo (k f luoranthene" 160 J 50-32-8————— Benzo (a pyren_.,__._____e _ 320 J 193-39-5————— Indeno (. L, 2.3-cd) pyrene 270 J 53-70-3—————— Dibanz(a,h) anthracene ' 69 J 191-24-2————— Benzo (g,h,i)perylene 260 J i) - cannot ce separated rrom Dipnenyiamine FORM I SV-2 OLM03.2

AR3029I3 591 IB ,, EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET BRH36 Lab Name: LANCASTER LABS Contract: Ib Code: LANCAS Case No.: ____. SAS No.: ____. SDG No.: ______Matrix: (soil/water) SOIL Lab Sample ID: 2723090 Sample-wt/vol: 30 '(g/mL) G Lab File ID: >JF263 Level: (low/med) LOW Date Received: 06/06/97 % Moisture: 30 decanted: (Y/N) N Date Extracted: 06/10/97 Concentrated Extract Volume: 500(uL) Date Analyzed: 06/19/97 Injection Volume: 2.0 (uL) Dilution Factor: 1.0 GPC Cleanup: (Y/N) Y pH: ___. CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q

108-95-2————— Phenol 470 U 111-44-4——.—— bis (2-cnioroethyi) ether 470 U 95-57-8—————— 2-Chlorophenol 470 U 541-73-1————— 1,3-Dichlorobenzene___ 470 U 106-46-7"—-—— 1,4-Dichlorobenzene___ 470 U 95-50-1—•—•—— 1,2-Dichlorobenzene______470 U 95-48-7————— 2-Methylphenol ——— . 470 u 108-60-1————— 2,2'-oxybis(1-cnioropropane) • 470 u 106-44-5————— 4-Methylphenol______470 u 621-64-7————— N-Nitroso-di-n-propyiamine 470 u 67-72-1—————— Hexachloroethane______470 u 98-95-3—————— Nitrobenzene^ ————————— 470 u 78-59-1-——•——• Isophorone 470 u 88-75-5——————• 2-Nitrophenoi • 470 u 105-67-9————— 214-Dimethylpnenoi 470 u 111-91-1————— bis{2-Chloroethoxy)methane 470 u 12 0-8 3-2 ————— 2,4-Dichlorophenol — 470 u 120-82-1-————— 1,2,4-Trichlorobenzene 470 u 91-20-3—————— Naphthalene______ZZZH 470 u 106-47-8————— 4-ChloroaniJ.ine 470 u 87-68-3——•——— Hexachlorobutadiene___ 470. u 59-50-7—————— 4 -Chloro-3 -methylphenoi 470 u 91-57-6—————.- 2-1Methylnaphthalene 470 u 77-47-4—————- HexachlorocyclopentadTenxachlorocyclopent. e 470 u 88-06-2—————— 2,4,6-Trichlorophenol_____ 470 u 95-95-4————— 2,4,5-Trichlorophenol——— 1200 u 91-58-7————— 2-Chloronaphthalene 470 u 88-74-4————— 2-Nitroaniline 1200 u 131-11-3————— Dimethylphthalate — 470 u 606-20-2————— 2,6 -Dinitrotoluene — 470 u 208-96-8———— Acenaphthylene 470 u 99-09-2————— 3-Nitroaniline 1200 u 83-32-9————— Acenaphth£ne______470 u

FORM I SV-1 OLM03.2

651 AR3029U 1C EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET BRH36 Lab Name: LANCASTER LABS Contract: Lab Code: LANCAS Case No.: ____. SAS No.: ____. SDG No.: Matrix: (soil/water) SOIL Lab Sample ID: 2723090 Sample wt/vol: 30 .(g/mL) G Lab File ID: >JF263 ». Level: (low/mad) LOW Date Received: 06/06/97 % Moisture: 30 decanted: (Y/N) N Date Extracted: 06/10/97 Concentrated Extract Volume: 500(uL) Date Analyzed: 06/19/97 Injection Volume: 2.0 (uL) Dilution Factor: 1.0 GPC Cleanup: (Y/N) Y pH: ___. CONCENTRATION UNITS: CAS NO. COMPOUND . (ug/L or ug/Kg) UG/KG Q

51-28-5—————— 2,4-Dinitrophenol 1200 U 100-02-7————— 4-Nitrophenol_ ' 1200 U 132-64-9———• Dibanzoruran 470 U 121-14-2————— 2,4-Dinitrotoiuene • 470 U 84-66-2—————— Diethylphthalate 470 U 7005-72-3———— 4-Chlorophenyl-pnenyietnar 470 U 36-73-7-—————• Fluorene____ 470 U 100-01-6————— 4-Nitroaninna -1200 U 534-52-1————— 4,6-Dinitro-2-matnyipnenoi 1200 U 36-30-6————— N-Nitrosodiphenylaraine (1) — 470 U 101-55-3——•— 4-Bromophenyl-*phenylether___ 470 U 113-74-1-—•—— Hexachlorobenzene 470 U 37-86-5-————• Pentachlorophanol 1200 U 35-01-3————•— Phenanthrene_____ 430 J 120-12-7———'•— Anthracene 39 J 86-74-8—•—•— Carbazole______53 J 84-74-2————— Di-n-butyipntnaiate 470 u 206-44-0——•—— Fluoranthene 630 129-00-0————— Pyrene 660 35-68-7—————— Butylbenzyiphthaiate 470 u 91-94-1—————— 3,3"1 -Dichlorobenzidine . 470 u 56-55-3——•—— Benzo (a) anthracene______370- J 117-81-7———— bis (2-Ethylhexyl) pnthaiate 520 218-01-9———— Chrysene______• .______470 J 117-84-0————— Di-n-octyiphtnaiate 470 u 205-99-2————— Benzo (b,tluoranthene 540 207-08-9————— Benzo (k fluoranthene" 200 J 50-32-8———•——• Banzo(a pyren__ _,.______e _ 420 J 193-39-5———— Indeno {:., 2.3-cd) pyrene 390 J 53-70-3-—•——— Dibenz(a,hi anthracene ' 39 J 191-24-2————— Benzo (g,h,i)peryl ene 370 J - cannot oe separated rrom Dipnenylamina FORM I SV-2 OLM03.2

Aft302915 6S2 IB . .... -, EPA SAMPLE NO, SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET BRH38 Lab Name: LANCASTER LABS Contract; Code: LANCAS Case No.: ____. SAS No.: ______SDG No.: _____ Matrix: (soil/water) SOIL Lab Sample ID: 2723091 Sample'wt/vol: 30 (g/mL) G Lab File ID: >JF264 Level: (low/med) LOW Date Received: 06/06/97 % Moisture: 32 decanted: (Y/N) N Date Extracted: 06/10/97 Concentrated Extract Volume: 500(uL) Date Analyzed: 06/19/97 Injection Volume: 2.0 (uL) Dilution Factor: 1.0 GPC Cleanup: (Y/N) Y pH: ___. CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q

108-95-2————— Phenol .______480 U 111-44-4————— bis (2-cnioroetnyi) etner 480 U 95-57-8————— 2-Chlorophenol 480 U 541-73-1————— 1,3-Dichlorobenzene___ 480 U 106-4 6-7————— I/ 4-Dichlorobenzene_____ 69 J 95-50-1—————— 1,2-Dichlorobenzene______480 U 95-48-7—————— 2-Methylphenol ——— • 480 U 108-60-1————— 2,2' -oxyfais (1-cnioropropane) • 480 U 106-44-5————— 4-Methylphenol______480 U 621-64-7-————— N-Nitroso-di-h-propyiamine 480 u 67-72-1—————— Hexachloroethane______480 u 98-95-3————— Nitrobenzene_ ———————— 480 u 78-59-1—————— Isophorone 480 u 88-75-5—————— 2-Nitrophenoi 480 u 105-67-9————— 2.4 -Dimethylpnenoi 480 u 111-91-1————— bis (2-Chloroethoxy) methane 480 u 120-83-2————— 2,4-Dichlorophenol — 480 u 120-82-1————— 1,2,4-Trichlorobenzene 480 u 91-20-3—————— Naphthalene 78 J 106-47-8————— 4 -Chloroaniiine 480 u 87-68-3—————— Hexachlorobutadiene___ 480 u 59-50-7—————— 4 -Chloro-3 -me thy Iphenoi 480 u 91-57-6————— 2-Methylnaphthalene ——— 480 u 77-47-4—————— Hexachlorocyclopentadiene 480 u 88-06-2————— 2,4,6-Trichlorotfhenol 480 u 95-95-4————— 2,4, 5-Trichlorophenol' 1200 u 91-58-7—————— 2-Chloronaphthalene_" 480 u 88-74-4————— 2-Nitroaniline 1200 u 131-11-11-3————- — Dimethylphthalate 480 u 606-20-2————— 2,6-Dinitrotoluene 480 u 208-96-8————— Acenaphthylene 78 J 99-09-2—————— 3-Nitroanlline 1200 u 83-32-9-————— Acenaphthene_ 160 J

FORM I SV-1 OLM03.2

AR3029I6 1C EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET BRH38 Lab Name: LANCASTER LABS Contract: Lab Code: LANCAS Case No.: ____. SAS No.: ____. SDG No.: Matrix: (soil/water) SOIL Lab Sample ID: 2723091 Sample.wt/vol: 30 '(g/mL) G Lab File ID: >JF264 Level: (low/med) LOW Date Received: 06/06/97 % Moisture: 32 decanted: (Y/N) N Date Extracted: 06/10/97 Concentrated Extract Volume: 500(uL) Date Analyzed: 06/19/97 Injection Volume: 2.0 (uL) Dilution Factor: 1.0 GPC Cleanup: -(Y/N) Y pH: ____. CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG . Q

51-28-5—————— 2,4-Dinitrophenol 1200 U 100-02-7————— 4-Nitrophenol__" 1200 U 132-64-9—————• Dibenzozuran 100 J 121-14-2————— 2,4-Dinitrotoiuene ' 430 U 84-66-2————— Diethvlphthalate 430 U 7005-72-3———— 4-Chlorophenyl-pnenyietner 430 U 86-73-7————— Fluorene______260 J 100-01-6-———— 4-Nitroanj.nna "— •1200 U 534-52-1————— 4,6-Dinitro-2-matnyipnenoi 1200 U 36-30-6—————— N-Nitrosodiphenylamine (1) — 430 U 101-55-3————— 4-Bromophenyl-phenylether__ 430 U 118-74-1————— Hexachlorobenzene 430 U 87-86-5————•— Pentachlorophenol" 1200 U 85-01-8—————— Phenanthrene___" 1900 120-12-7———— Anthracene 430 J 86-74-3———•— Carbazole 200 J 84-74-2—————— Di-n-butyipntnaiate 480 U 2Q6-44-0———•— Fluoranthene______~_ 2200 129-00-0————— Pyrene 2300 85-68-7—————— Buutylbenzyiphthaiatt •" e 79 J 91-94-1——————— 3,31-Dichlorobenzidine 430 u 56-55-3—————• Benzo (a) anthracene______1200 117-31-7———.— bis(2-Ethylhexyl)pntnaiate 650 213-01-9———— Chrysene______1200 117-84-0————— Di-n-octyxpntnaiate 480 u 205-99-2————— Benzo(b rlupranthene 1300 207-08-9————— Benzo fluoranthana" 470 J 50-32-3- 1100 193-39-5- cd) pyrene_ 330 53-70-3—•——j->~ / w~j ——————————— Dibenzi_'_.J-'9i«_if \ aa. f hm) O4iw.i_.ciwdanthraceni e 220 191-24-2————— Benzo (g,h,i)perylene 730 17 - Cannot be separated r-rom Dipnenylamina FORM I SV-2 OU.03..2

AR3029I7 71S IB EPA SAMPLE NO, SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET BRK39 Lab Name: LANCASTER LABS Contract: ______ab Code: LANCAS Case No.: ___. SAS No!/: ____. SDG No.: Matrix: (soil/water) SOIL Lab Sample ID: 2723092 Sample'wt/vol: 30 (g/mL) G Lab File ID: >JF265 Level: (low/med) LOW Date Received: 06/06/97 % Moisture: 28 decanted: (Y/N) N Date Extracted: 06/10/97 Concentrated Extract Volume: 500(uL) Date Analyzed: 06/19/97 Injection Volume: 2.0 (uL) Dilution Factor: 1.0 GPC Cleanup: (Y/N) Y pH: ____. CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q

108-95-2————— Phenol______460 U 111-44-4-———- bis (2-cnioroetnyi) etner 460 U 95-57-8—————— 2-Chlorophenol____. 460 U 541-73-1————— 1,3-Dichlorobenzene 460 U 106-46-7-———— 1,4-Dichlorobenzene" 460 U 95-50-1————— l, 2-Dichlorobenzene" 460 U 95-48-7—————— 2-Methylphenol 460 U 108-60-1————— 2,2' -oxybis(1-cnioropropane) . 460 U 106-44-5————— 4-Methylphenol______460 u 621-64-7————— N-Nitroso-di-n-propyiamine 460 u 67-72-1————— Hexachloroethane______460 u 98-95-3—————— Nitrobenzene______460 u 78-59-1—————— Isophorone 460 u 88-75-5—————— 2-Nitrophenoi . 460 u 105-67-9————— 2,4-Dimethylpnenoi "" 460 u 111-91-1——-— bis (2-Chloroethoxy) metnane 460 u 120-83-2————— 2,4-Dichlorophenol — 460 u 120-82-1———•— 1,2,4-Trichlorobenzene 460 u 91-20-3—————— Naphthalene 250 J 106-47-8————— 4-ChloroaniTTruT______460 u 87-68-3—————— Hexachlorobutadiene______460 u 59-50-7————— 4-Chloro-3-methylphenoi 460 u 91-57-6—-——-- 2-Methylnaphthalene — 460 u 77-47-4————— Hexachlorocyclopentadiene 460 u 88-06-2————— 2,4,6-Trichlorophenol 460 u 95-95-4-————•— 2,4,5-Trichlorophenol" 1200 u 91-58-7-————•— 2-Chloronaphthalene " 460 u 88-74-4—————— 2-Nitroaniline 1200 u 131-11-3————— Dimethylphthal!vEe~~ 460 u 606-20-2————— 2,6-Dinitrotoluene" 460 u 208-96-8———— Acenaphthylene 240 J 99-09-2—————— 3 -Nitroanil ine——— 1200 u 83-32-9—————— Acenaphthene "——— 3400

FORM I SV-1 OLM03.2

AR3029I8 7SS 1C EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET BRH39 Lab Name: LANCASTER LABS Contract: Lab Code: LANCAS Case No.: ____. SAS No.: ____. SDG No.: Matrix: (soil/water) SOIL Lab Sample ID: 2723092 Sample twt/vol: 30 '(g/mL) G Lab File ID: >JF265 Level: (low/med) LOW Date Received: 06/06/97 % Moisture: 28 decanted: (Y/N) N Date Extracted: 06/10/97 Concentrated Extract Volume: 500(uL) Date Analyzed: 06/19/97 Injection Volume: 2.0 (uL) Dilution Factor: 1.0 GPC Cleanup: (Y/N) Y pH: ____. CONCENTRATION UNITS: GAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q

51-23-5 — — —— • 2 , 4-Dinitrophenol 1200 U 100-02-7 ————— 4-Nitrophenol 1200 U 132-64-9-——— — oibenzofuran 500 121-14-2 ————— 2 . 4-Dinitrotoliierie 460 U 84-66-2 —————— Diethvlphthalate " '" 460 U 70O5-72-3 ———— 4-cnioropnenyi-pneriyJLetner 460 U 86-73-7 ————— Fluorene 2200 100-01-6- —— — 4-Nitroaninne •1200 U 534-52-1- — • —— 4 , 6-Dinitro-2-metnyipnenoi 1200 U 86-30-6 ————— N-Nitrosodiphenylamine (1) 460 U 101-55-3- ———— 4-Bromophenyl-phenylether 460 U 118-74-1 ————— Hexachlorobenzene 460 U 87-86-5 ————— Pentachlorophenol 1200 U 85-01-8 — • ———— • Phenanthrene 4900 E 120-12-7 ————— Anthracene 1100 86-74-8 —————— Carbazole 160 J 84-74-2 ————— Di-n-butyipntnaiate 460 U 206-44-0 ————— Fluorantnene 1400 129-00-0 ————— Pyrene 1400 85-63-7 ————— • Butylbenzyipntnaiate 460 U 91-94-1 —————— 3 , 31 -Dichlorobenzidine 460 U 56-55-3 —————— Benzo (a) anthracene - 630 117-81-7 ————— bis(2-Ethylhexyl)pntnaiate 410 J 218-01-9 ————— Chrysene 670 117-34-0 ————— Di-n-octviphtnaiate 460 u 205-99-2 ————— Benzo i b) tluoranthene 760 207-08-9——— — • senzoi jc) riuorantnana 260 J 50-32-s ————— senzoi a) pyrene 590 193-39-5 —— • —— indenoii,2.3-cdTPYfene 470 53-70-3 —————— oibenz ( a , h } anthracene 130 J 191-24-2 — — — • senzo(g,n,i)peryiene 430 J i) - cannot oe separated r-rom. uipnenyiamine FORM I SV-2 OLM03.2

flR3029!9 IB EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET BRH39DL Lab Name: LANCASTER LABS ' Contract; rab Code: LANCAS Case No.: _____. SAS No.: ____. SDG No.: (soil/water) SOIL Lab Sample ID: 2723092DL Sample, wt/vol: 30 '(g/mL) G Lab File ID: >JF266 Level: (low/med) LOW Date Received: 06/06/97 % Moisture: 28 decanted: (Y/N) N Date Extracted: 06/10/97 Concentrated Extract Volume: 500(uL) Date Analyzed: 06/19/97 Injection Volume: 2.0 (uL) Dilution Factor: 2.0 GPC Cleanup: (Y/N) Y pH: ____. CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q

108-95-2————— Phenol______920 U 111-44-4————— bis(2-cnioroetnyijether 920 U 95-57-8—————— 2-Chlorophenol 920 U 541-73-1————— 1,3-Dichlorobenzene.____- 920 U 106-46-7————— 1,4-Dichlorobenzene______920 U 95-50-1—————— 1,2-Dichlorobenzene______920 U 95-48-7—————— 2-Methylphenol 920 U 108-60-1-———- 2,2'-oxybis(1-cnioropropane) ". 920 U 106-44-5————— 4-Methylphenol______920 U 621-64-7————— N-Nitroso-di-n-propyiamine 920 U 67-72-1—————— Hexachloroethane______— 920 U 98-95-3————— Nitrobenzene ————————— 920 U 78-59-1—————— Isophorone 920 U 88-75-5————— 2-Nitrophenol "" 920 u 105-67-9————— 2,4 -Dime thylphenoi "" 920 u 111-91-1————— bis (2-Chloroethoxy; metnane 920 u 120-83-2————— 2,4-Dichlorophenol — 920 u 120-82-1————— 1,2,4-Trichlorobenzene 920 u 91-20-3————— Naphthalene 290 J D 106-47-8————— 4-Chloroaniiine 920 U 87-6 8-3 —————— Hexachlorobutadiene___ 920 U 59-50-7—————— 4 -Chloro-3 -methylphenol 920 U 91-57-6—————— 2-Methylnaphthalene 920 U 77-47-4————— Hexachlorbcvclopentadiene "" 920 U 88-06-2————— 2,4,6-Trichloropbenol —— 920 u 95-95-4—————— 2,4,5-Trichlorophenol 2300 u 91-58-7————— 2-ChloronapHthalene ————— 920 u 88-74-4————— 2-Nitroaniline 2300 u 131-11-3————— DimethylphthalaTEe— 920 u 606-20-2————— 2,6-DinitrotoluenF 920 u 208-96-8————— Acenaphthylene___" 290 J D 99-09-2————— 3 -Nitroanil ine——— 2300 U 83-32-9—————— Acenaphthene 4000 D

FORM I SV-1 OLM03.2

AR302920 85S 1C EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET BRH39DL Lab Name: LANCASTER LABS Contract: Lab Code: LANCAS Case No.: ____. SAS No.: ____. SDG No, (soil/water) SOIL Lab Sample ID: 2723092DL Sample wt/vol: 30-(g/mL) G Lab File ID: >JF266 Level: (low/med) LOW Date Received: 06/06/97 % Moisture: 28 decanted: (Y/N) N Date Extracted: 06/10/97 Concentrated Extract Volume: 500(uL) Date Analyzed: 06/19/97 Injection Volume: 2.0 (uL) Dilution Factor: 2.0 GPC Cleanup: (Y/N) Y pH: ___. ' CONCENTRATION UNITS: - CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q

51-28-5—————— 2,4-Dinitrophenol 2300 U 100-02-7————— 4-Nitrophenol__: 2300 U 132-64-9————— Dibenzofuran 570 J D

121-14-2————J-tfi <«b -fe*t 4b — 2,4-Dinitr*6 * ~i J-/J.»4A<_b W-l»o W toluenWW A V^< e 920 U 84-66-2—————— Diethylphthalate______920 U 7005-72-3-———— 4-Chlorophenyl-pnenyietner_ 920 U 86-73-7————— Fluorene______2600 D 100-01-6-———— 4-Nitroaniiine ',2300 U 534-52-1————— 4,6-Dinitro-2-metiiyiphenoi 2300 U 86-30-6————— N-Nitrosodiphfinylamine (i)~ 920 U 101-55-3————— 4-Bromophenyl-phenylether " 920 U 118-74-1-—-—— Hexachlorobenzene 920 U 87-86-5—————— Pentachlorophenol" 2300 U 85-01-8-————— Phenanthrene___" 5300 D 120-12-7————— Anthracene______1200 D 86-74-8—————— Carbazole 160 J D 84-74-2-————— Di-n-butyipntnaiate 920 U 206-44-0———— Fluoranthene_____~ 1600 D 129-00-0————— Pyrene 1700 D 85-68-7—————— B*utylbenzyiphthaiate ——... " 920 U 91-94-1—————— 3,3n-Dichlorobenzidine 920 U 56-55-3—•———— Benzo (a) anthracene 700 J D 117-81-7————— bis(2-Ethylhexyl)pntnaiatep _ 450 J D 218-01-9————— Chrysene 780 J D 117-84-0—•—•— Di-n-octyipntnaiate 920 U 205-99-2————"** "" ~ — Benz"——"-'fluorantheneo (b, " 810 J D 207-08-9————— Benzo(k' flupranthene" 310 J D 50-32-8—————— Benzo (a' pyrene______640 J D 193-39-5—•——— Indeno(..,2,3-cd;pyrene 430 J D 53-70-3————•»«» / v j ————— ————— Dibenz(a,h./-.-Jdi-. i a, i) i- anthraceni aiib.__.owciet ' 110 J D 191-24-2————— Benzo (g,h,i)perylene 410 J D i> - cannot be separated rrom.uipnenyiamine .•' FORM I SV-2 OLM03.2

AR30292I S59 -•• v.'- ... ,.,. IF ^v-1 EPA SAMPLE NO, SEMIVOLATILE ORGANICS ANALYSIS DATA SI BRHS1 Tab Name: LANCASTER LABS Contract: Code: LANCAS Case No.: ____ . SAS No.: ____ . SDG No.: Matrix: (soil/water) SOIL Lab Sample ID: 2723076 * * Sample wt/vol: s 30 (g/mL) G Lab File ID: >JF245 Level: (low/med) LOW Date Received: 06/06/97 * Moisture: 4 decanted: (Y/N) N Date Extracted: 06/10/97 Concentrated Extract Volume: 500 (uL) Date Analyzed: 06/18/97 Injection Volume: 2.0 (uL) Dilution Factor: 1.0 GPC Cleanup: (Y/N) Y pH: ___. CONCENTRATION UNITS: Number TICs found: 2 (ug/L or ug/Kg) UG/KG

CAS NUMBER COMPOUND NAME RT EST. CONC. Q 1. Unknown 36.98 74. J 2. Unknown 49.60 100. J 3. 4. f b. . 6. 7. k 8. 9. . s^O.

^1. . • 12. 13. 14. 15. •- 16. 17. IB. 19. 20. 21. 22. r 23. / 24. 2b. • 26. 27. 26. 29. 30. .

FORM I SV-TIC OLM03.2

AR302923 ' 40 IF EPA SAMPLE NO. ALKANE SUMMARY

Lab Name: LANCASTER LABS Contract: £3£Vtlk3 O. Lab Code: LANCAS Case No.: ____. SAS No.: ____. SDG No.: Matrix:, (soil/water) SOIL Lab Sample ID: 2723076 Sample wt/vol: 30 (g/mL) G Lab File ID: >JF245 Level: (low/med) LOW Date Received: 06/06/97 % Moisture: 4 decanted: (Y/N) N Date Extracted: 06/10/97 Concentrated Extract Volume: 500 (uL) Date Analyzed: 06/13/97 Injection Volume: 2.0 (uL) Dilution Factor: 1.0 GPC Cleanup: (Y/N) Y pH: ____. CONCENTRATION UNITS: Number TICs found: 2 (ug/L or ug/Kg) UG/KG CAS NUMBER COMPOUND NAME RT EST. CONC. —-___-, 1. Unknown alkane "-tsTsi" 72. J= 2. Unknown alkane 33.21 93. J 3. 4. 5. 6. A 7. - 8. 9. — sJ 10. 11. 12. 13. 14 . 15. 16. 17. 18. • 19. 20. 21. - 22. 23. / 24. ,* 2b.

FORM 1 SV-TIC OLM03.2

AR302921* , 41 IF ,,,,,-.-. EPA SAMPLE NO, SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET BRHS2 Lab Name: LANCASTER LABS Contract: Code: LANCAS Case No.: ____. SAS No.: ____. SDG No.: Matrix: (soil/water) SOIL Lab Sample ID: 2723077 Sample'wt/vol: 30 (g/mL) G Lab File ID: >JF246 Level: (low/med) LOW Date Received: 06/06/97 % Moisture: 10 decanted: (Y/N) N Date Extracted: 06/10/97 Concentrated Extract Volume: 500 (uL) Date Analyzed: 06/18/97 Injection Volume: 2.0 (uL) Dilution Factor: 1.0 GPC Cleanup: (Y/N) Y pH: ____. CONCENTRATION UNITS: Number TICs found: 15 (ug/L or ug/Kg) UG/KG

CAS NUMBER COMPOUND NAME RT EST. CONC. Q 1. Unknown 12.16 120. J 2. 57103 Hexadecanoic acid 28.46 130. J 3. 9-Eicosene, (E)- 33.18 380. JX 4. Unknown 34.61 80. J 5. Unknown 36.98 *. 110. J 6. 636664 Octadecanal 37.30 340. J 7. Unknown v 38.33 360. J a. Benzo f j 1 f luoranthene 39.10 100. JX 9. 16-Octaaecenal 41.09 450. JX .°" Unknown 41.45 100. J Unknown 42.54 150. J 12. Unknown 43.93 92. J 1-3. Unknown 45.05 180. J 14. Unknown 46.46 150. J Ib. Unknown 4.9.63 630. J 16. 17. 16. 19. 20. 21. 22. . 23. • . 24. 25. i 26. 27. 28. 29. 30. -

FORM I SV-TIC OLM03.2

AR302925 56 IF EPA SAMPLE NO. ALKANE SUMMARY BRHS2 Lab Name: LANCASTER LABS Contract Lab Code: LANCAS Case No.: ____ . SAS No.: ____ . SDG No.: Matrix: (soil/water) SOIL Lab Sample ID: 2723077 Sample wt/vol: 30 (g/mL) G Lab File ID: >JF246 Level: (low/med) LOW Date Received: 06/06/97 % Moisture: 10 decanted: (Y/N) N Date Extracted: 06/10/97 Concentrated Extract Volume: 500 (uL) Date Analyzed: 06/13/97 Injection Volume: 2.0 (uL) Dilution Factor: 1.0 GPC Cleanup: (Y/N) Y pH: ____ . CONCENTRATION UNITS: Number TICs found: 6 (ug/L or ug/Kg) UG/KG

CAS NUMBER COMPOUND NAME RT EST. CONC. JQ^ 1. Unknown alkane 31.53 150. J 2. Unknown alkane 34.17 34. J 3. Unknown alkane 35.31 570. J 4. Unknown alkane 33.21 670. J 5. Unknown alkane 42.33 410. J 6. Unknown alkane 43.14 230. J 7. 8. 9. 10. —————— Vs- 11. 12. 13. 14. Ib. 16. 17. 13. 19. » 20. _— — 21. 22. 23. 24. / 2b. • 26. 27. 28. 29. 30. .'

FORM I SV-TIC OLM03.2

AR302926 57 IF EPA SAMPLE NO. SEMIVOLATILE ORGAN ICS ANALYSIS DATA SHEET BRHSS Lab Name: LANCASTER LABS Contract: Code: LANCAS Case No.: _. SAS No.: ____ . SDG No.: Matrix: (soil/water) SOIL Lab Sample ID: 2723078 Sample "wt/vol : 30 (g/mL) G Lab File ID: >JF247 Level: (low/med) LOW Date Received: 06/06/97 % Moisture: 36 decanted: (Y/N) N Date Extracted: 06/10/97 Concentrated Extract Volume: 500 (uL) Date Analyzed: 06/18/97 Injection Volume: 2.0 (uL) Dilution Factor: 1.0 GPC Cleanup: (Y/N) Y pH: ___ . CONCENTRATION UNITS: " Number TICs found: 29 (ug/L or ug/Kg) UG/KG

CAS NUMBER COMPOUND NAME RT EST. CONC. «=-S-r-_ 1. Unknown 14.36 210. J 2. Unknown 20.00 870. J 3. Unknown 23.22 520. J 4. Unknown 26.11 540. J 5. Unknown 26.92 180. J 6. Unknown 28.29 630. J 7. Unknown 28.47 1800. J 6. Unknown v 30.37 350. J 9. 16-Octadecenal 34.61 210. JX 10. Unknown 36.98 310. J 1-^11. 636664 Octadecanal 37.29 610. J 12. Unknown 37.70 520. J 13. Unknown 38.32 920. J 14. Unknown 38.58 180. J 15. Unknown 40.03 390. J 16 . Unknown 41.08 660. J 17. Unknown 42.53 460. J 18. Unknown 42.91 360. J 19. Unknown 43.92 2900. J 20. Unknown 45.04 540. .J 21. Unknown 46.44 340. J 22. Unknown 46.85 390. . J 23. Unknown 47.62 400. J 24. Unknown / 48.15 360. J 2b. Unknown 48.49 160. J 26. Unknown 49.03 150. J 27. Unknown 49.65 3100. J 26. Unknown 50.14 190. J 29. Unknown 51.47 220. J 30. ;

FORM I SV-TIC OLM03.2

AR302927 IF EPA SAMPLE NO. ALKANE SUMMARY BRHS3 Lab Name: LANCASTER LABS Contract Lab Code: LANCAS Case No.: ____. SAS No.: ____. SDG No.: Matrix: (soil/water) SOIL Lab Sample ID: 2723073 *_ * Sample wt/vol: 30 (g/mL) G Lab File ID: >JF247 Level: (low/med) LOW Date Received: 06/06/97 % Moisture: 36 decanted: (Y/N) N Date Extracted: 06/10/97 Concentrated Extract Volume: 500 (uL) Date Analyzed: 06/13/97 Injection Volume: 2.0 (uL) Dilution Factor: 1.0 GPC Cleanup: (Y/N) Y pH: ____. CONCENTRATION UNITS: Number TICs found: 9 (ug/L or ug/Kg) UG/KG

CAS NUMBER COMPOUND NAME RT EST. CONC. Q ====_=» Unknown alkane 29.34 140. J 2. Unknown alkane 31.52 290. J 3. Unknown alkane 32.31 190. J 4. Unknown alkane 33.17 - 1000. J 5. Unknown alkane 34.16 220. J 6. Unknown alkane 35.30 2100. J 7. Unknown alkane 36.64 290. J 8. Unknown alkane 33.22 2300. J 9. Unknown alkane 42.32 960. J v 10. 11. 12. 13. 14. 15. 16. I/. 16. • 19. 20. 21. 22. r 23. 1 24. . , 25. 26. 26. 29. 30.

FORM I SV-TIC OLM03.2

AR302928 99 IF EPA SAMPLE NO. SEMIVOLATILE ORGAN ICS ANALYSIS DATA SHEET BRH14 Lab Name: LANCASTER LABS Contract: ib Code: LANCAS Case No.: ____. SAS No.: . SDG No.: Matrix: (soil/water) SOIL Lab Sample ID: 2723079 Sample'wt/vol: 30.' (g/mL) G Lab File ID: >JF248 Level: (low/med) LOW Date Received: 06/06/97 % Moisture: 14 decanted: (Y/N) N Date Extracted: 06/10/97 Concentrated Extract Volume: 500 (uL) Date Analyzed: 06/18/97 Injection Volume: 2.0 (uL) Dilution Factor: 1.0 GPC Cleanup: (Y/N) Y pH: ___. CONCENTRATION UNITS: Number TICs found: 15 (ug/L or ug/Kg) UG/KG

CAS NUMBER COMPOUND NAME RT EST. CONC. =_Q__ ~l" === Unknown i27ieT 1207 J 2. Unknown 19.73 88. J 3. 57103 Hexadecanoic acid 28.45 91. J 4. Unknown 32.30 190. J 5. Unknown 34.61 81. J 6. Unknown 36.99 . • 200. J 7. Unknown 37.10 130. J 6. Unknown x 37.29 220. J 9. Unknown 38.10 250. J 10. Unknown 38.31 330. J 1-A1. Unknown 41.08 180. J 12. Unknown 42.52 95. J 13. Unknown 43.91 220. J 14. Unknown 45.03 190. J 15. Unknown 49.62 580; J 16. 17. 18. 19. 20. 21. 22...... 23. ... f 24. i 25. ______26. * 27. 26. 29. ——— 30. •; .

FORM I SV-TIC OLM03.2

AR302929 _„ 156 IF EPA SAMPLE NO. ALKANE SUMMARY BRH14 Lab Name: LANCASTER LABS Contract: Lab Code: LANCAS Case No.: ____. SAS No.: ____. SDG No.: Matrix: (soil/water) SOIL Lab Sample ID: 2723079 Sample wt/vol: 30 (g/mL) G Lab File ID: >JF248 Level: (low/med) LOW Date Received: 06/06/97 % Moisture: 14 decanted: (Y/N) N Date Extracted: 06/10/97 Concentrated Extract Volume: 500 (uL) Date Analyzed: 06/18/97 Injection Volume: 2.0 (uL) Dilution Factor: 1.0 GPC Cleanup: (Y/N) Y pH: ____. CONCENTRATION UNITS: Number TICs found: 7 (ug/L or ug/Kg) UG/KG CAS NUMBER COMPOUND NAME RT EST. CONC. -=2-= 1. Unknown alkane 31.53 92." j 2. Unknown alkane 33.17 140. j 3. Unknown alkane 35.32 300. j 4. Unknown alkane 33.20 210. j 5. Unknown alkane 40.03 91. j 6. Unknown alkane 42.32 • 250. j 7. Unknown alkane 43.14 140. j 6. 9. 10. ———— v 11. 12. • 13. 14. lb. 16. 17. 13. 19. . 20. 21. 22. 23. 24. 2b. • 26. 27. 23. 29. 30. <'

FORM I SV-TIC OLM03.2

AR302930 157 IF EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET BRH16 Lab Name: LANCASTER LABS Contract: Code: LANCAS Case No.: . SAS No.: ____ . SDG No.: Matrix: (soil/water) SOIL Lab Sample ID: 2723080 Sample 'wt/vol: 30 (g/mL) G Lab File ID: >JF249 Level: (low/med) LOW Date Received: 06/06/97 % Moisture: 8 decanted: (Y/N) N Date Extracted: 06/10/97 Concentrated Extract Volume: 500 (uL) Date Analyzed: 06/18/97 Injection Volume: 2.0 (uL) Dilution Factor: 1.0 GPC Cleanup: (Y/N) Y pH: ___ . CONCENTRATION UNITS: Number TICs found: 6 (ug/L or ug/Kg) UG/KG

CAS NUMBER COMPOUND NAME RT EST. CONC. Q 1. Unknown 12.16 81. J 2. Unknown 36.97 130. J 3. Unknown 37.30 93. J 4. Unknown 38.09 79. J 5. Unknown 38.33 130. J 6. Unknown 41.08 84. J 7. 8. " 9. t-ai10.. 12. 13. 14. 15. 16. 17. 16. 19. t 20. 21. 22. 23. r 24. t 25. 26. * 27. 26. 29. 30. ~~ ' f

FORM I SV-TIC OLM03.2

AR30293I 194 IF EPA SAMPLE NO. ALKANE SUMMARY BRH16 lab Name: LANCASTER LABS Contract: Lab Code: LANCAS Case No.: . SAS No.: . SDG No.: Matrix: (soil/water) SO.IL Lab Sample ID: 2723030 Sample 'wt/vol: 30 (g/mL) G Lab File ID: >JF249 Level: (low/med) LOW Date Received: 06/06/97 % Moisture: 3 decanted: (Y/N) N Date Extracted: 06/10/97 Concentrated Extract Volume: 500 (uL) Date Analyzed: 06/13/97 Injection Volume: 2.0 (uL) Dilution Factor: 1.0 GPC Cleanup: (Y/N) Y pH: ____ . CONCENTRATION UNITS: Number TICs found: 4 (ug/L or ug/Kg) UG/KG

CAS NUMBER COMPOUND NAME RT EST. CONC. Q 1. Unknown alkane ==337l7=* 120. J 2. Unknown alkane 35.30 110. J 3. Unknown alkane 33.20 120. J 4. Unknown alkane 42.31 140. J 5. 6. 7. 3. 9. 1110. ——— ^ 12. 13. 14. Ib. 16. 17. 18. 19. •- • 20. 21. 22. 23. 24. 25. •• 26. 2V. ——— - 28. 29. 30. .

FORM I SV-TIC OLM03.2

AR302932 IF ' EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET BRH20 Lab Name: LANCASTER LABS Contract: Code: LANCAS Case No.: ____. SAS No.: ____. SDG No.: Matrix: (soil/water) SOIL Lab Sample ID: 2723083 Sample'wt/vol: 30 (g/mL) G Lab File ID: >JF252 Level: (low/med) LOW Date Received: 06/06/97 % Moisture: 26 decanted: (Y/N) N . Date Extracted: 06/10/97 Concentrated Extract Volume: 500 (uL) Date Analyzed: 06/19/97 Injection Volume: 2.0 (uL) Dilution Factor: 1.0 GPC Cleanup: (Y/N) Y pH: ___. CONCENTRATION UNITS: Number TICs found: 21 (ug/L or ug/Kg) UG/KG

CAS NUMBER COMPOUND NAME RT EST. CONC. =_==_=__=_.. ___?— 1. Unknown 12.16 J~ 2. 100516 Benzenemethanol 13.89 100. J 3. Unknown 14.34 110. J 4. 2091294 9-Hexadecenoic acid 28.28 190. J 5. 57103 Hexadecanoic acid 28.45 220. J 6. Unknown 29.53 250. J 7. Unknown 29.87 220. J 6. Unknown 36.97 130. J 9. Unknown 37.29 380. J Unknown 38.32 450. J yil. Unknown 41.08 360. J 12. Unknown 42*. 54 340. J 13. Unknown 42.94 120. J 14. Unknown 43.93 2100. ' J 15. Unknown 45.04 280. J 16. Unknown 46.42 250. J IV. Unknown 46.86 170. J 16. Unknown 47.66 130. J 19. Unknown 49.60 1100. J 20. Unknown 50.11 110. J 21. Unknown 51.48 95. J 22. 23. , 24. 25. (* 26. 27. 28. 29. 30. .

FORM I SV-TIC OLM03.2

AR302933 IF EPA SAMPLE NO. ALKANE SUMMARY BRH20 Lab Name: LANCASTER LABS Contract: Lab Code: LANCAS Case No.: ____. SAS No.: ____. SDG No.: Matrix: (soil/water) SOIL Lab Sample ID: 2723083 Sample»wt/vol: 30 ' (g/mL) G Lab File ID: >JF252 Level: (low/med) LOW Date Received: 06/06/97 % Moisture: 26 decanted: (Y/N) N Date Extracted: 06/10/97 Concentrated Extract Volume: 500 (uL) Date Analyzed: 06/19/97 Injection Volume: 2.0 (uL) Dilution Factor: 1.0 GPC Cleanup: (Y/N) Y pH: ____. CONCENTRATION UNITS: Number TICs found: 7 (ug/L or ug/Kg) UG/KG

CAS NUMBER COMPOUND NAME RT EST. CONC. Q 1. Unknown alkane 31.53 130. J 2. Unknown alkane 32.31 140. J 3. Unknown alkane 33.17 260. J 4. Unknown alkane 35.30 510. J 5. Unknown alkane 33.21 360. J 6. Unknown alkane 42.32 630. J 7. Unknown alkane 48.11 200. J 6. V 9. 10. V 11. 12. 13. 14. 15. 15. • . 17. 16. 19. 20. 21. 22. 23. , 24. / 25. 26. 27. 23. 29. 30. ..

FORM I SV-TIC OLM03.2

UR30293U IF EFA SAMPLE NO, SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET BRH24 Lab Name: LANCASTER LABS Contract: Code: LANCAS Case No.: . SAS No.: ____ . SDG No.: Siatrix: (soil/water) SOIL Lab Sample ID: 2723084 Sample ( wt/vol: 30. (g/mL) G Lab File ID: >JF257 Level: (low/med) LOW Date Received: 06/06/97 % Moisture: 39 decanted: (Y/N) N Date Extracted: 06/10/97 Concentrated Extract Volume: 500 (uL) Date Analyzed: 06/19/97 Injection Volume: 2.0 (uL) Dilution Factor: 1.0 GPC Cleanup: (Y/N) Y pH: ____ . CONCENTRATION UNITS: Number TICs found: 30 (ug/L or ug/Kg) UG/KG

CAS NUMBER COMPOUND NAME RT EST. CONC. Q E!3£^£SSS5 1. Unknown 12.15 190. J 2. Naphthalene, 2-ethenyl- ' 21.78 260. JX 3. 2091294 9-Hexadecenoic acid 28.29 530. J .4. 57103 Hexadecanoic acid 28.46 710. J 5. Unknown 29.57 200. J 6. Unknown 29.99 370. J 7. Unknown 30.63 210. J 8. Unknown 30.82 870. J 9. Unknown 31.52 560. J 10. 5-Eicosene, (E)- 33.17 2100. JX 11. Unknown 34.61 240. J ,-12. Naphthalene, 1- (phenylmethyl 35.68 220. JX 13. Unknown 36.72 380. J 14. Unknown 37.30 1500. J Ib. Unknown 38.33 1700. J 16. Unknown 38.60 380. J 17 . Benz [e] acephenanthrylene 39.12 1100. JX 18. Unknown 41.08 1200. J 19. Unknown 42.55 1000. J 20. Unknown 42.93 800. J 21. Unknown 43.95 360. J 22. Unknown 44.27 290. J 23. Unknown 45.07 480. J 24. Unknown ' 46.87 390. J 25. Unknown ' 47.27 210. J 26. Unknown 48.52 210. J 2/. Unknown ' 49.05 280. J 26. Unknown 49.67 3900. J 29. Unknown 50.16 420. J 30. Unknown 51.52 560. J

FORM I SV-TIC OLM03.2

AR302935 IF EPA SAMPLE NO. ALKANE SUMMARY BRH24 Lab Name: LANCASTER LABS Contract: ______Lab Code: LANCAS Case No.: ____. SAS No.: ____. SDG No.: ____. Matrix: (soil/water) SOIL Lab Sample ID: 2723084 Sample'wt/vol: 30 (g/mL) G Lab File ID: >JF257 Level: (low/med) LOW Date Received: 06/06/97 % Moisture: 39 decanted: (Y/N) N Date Extracted: 06/10/97 Concentrated Extract Volume: 500 (uL) Date Analyzed: 06/19/97 Injection Volume: 2.0 (uL) Dilution Factor: 1.0 GPC Cleanup: (Y/N) Y pH: ___. CONCENTRATION UNITS: Number TICs found: 9 (ug/L or ug/Kg) UG/KG

CAS NUMBER COMPOUND NAME RT EST. CONC. Q 1. Unknown alkane 29.34 190. J 2. Unknown alkane 32.30 200. J 3. Unknown alkane 34.16 290. J 4. Unknown alkane 35.31 2000. J b. Unknown alkane 36.64 270. J 6. Unknown alkane 33.23 ' 2700. J 7. Unknown alkane 40.03 330. J 6. Unknown alkane 42.33 1400. J 9. Unknown alkane 43.13 230. 10. J y-/*' 11. 12. 13. 14. 15. 16. I/. 18. 19. • 20. 21. 22. 23. 24. / 25. . 26. 2;. 26. 29. 30. '•

FORM I SV-TIC OLM03.2

flR302936 266 IF EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET BRH27 Lab Name: LANCASTER LABS Contract: Lab Code: LANCAS Case No.: ____. SAS No.: ____. SDG No.: (soil/water) SOIL Lab Sample ID: 2723085 Sample wt/vol: 30 .(g/mL) G Lab File ID: >JF258 Level: (low/med) LOW Date Received: 06/06/97 % Moisture: 30 decanted: (Y/N) N 'Date Extracted: 06/10/97 Concentrated Extract Volume: 500 (uL) Date Analyzed: 06/19/97 Injection Volume: 2.0 (uL) Dilution Factor: 1.0 GPC Cleanup: (Y/N) Y pH: ____. CONCENTRATION UNITS: Number TICs found: 30 ' (ug/L or ug/Kg) UG/KG '

CAS NUMBER COMPOUND NAME . RT EST. CONC. Q 1. Unknown carboxylic acid 26.10 320. J 2. Unknown carboxylic acid - 26.91 290. J 3. Unknown 27.66 320. J 4. Unknown carboxylic acid 28.29 1600. J 5. Unknown carboxylic acid 28.48 2800. J 6. Unknown 29.88 630. J 7. Unknown 29.99 300. J 8. Unknown carboxylic acid 30.37 580. J 9. Unknown carboxylic1 acid 32.02 450. J 10. Unknown 32.28 860. J 1. Unknown 33.18 1100. J V J2. Unknown 36.98 470. J 13. Unknown 37.30 1600. J 14. Unknown 38.32 3200. J 15. Unknown 41.09 1500. J 16. Unknown alcohol 42.55 - 1500. J 17 . Unknown 42.72 550. J 16. Unknown 42.96 700. J 19. Unknown 43.94 2000. J 20. Unknown 44.28 3.80. J 21. Unknown 45.01 1300. J 22. Unknown 46.46 890. J 23. Unknown 46.87 830. J 24. Unknown 47.63 1000. J 2b. Unknown / 48.52 360. J 26. Unknown 49.69 7900. J 2/. Unknown 50.13 540. J 26. Unknown 50.43 740. J 29. Unknown 51.50 640. J 30. Unknown 51.55 640. J

FORM I SV-TIC OLM03.2

AR302937 IF EPA SAMPLE NO. ALKANE SUMMARY BRH27 Lab Name: LANCASTER LABS Contract: Lab Code: LANCAS Case No.: ____. SAS No.: ____. SDG No.: Matrix: (soil/water) SOIL Lab Sample ID: 2723035 Sample wt/vol: 30 (g/mL) G Lab File ID: >JF253 Level: (low/med) LOW Date Received: 06/06/97 % Moisture: 30 decanted: (Y/N) N Date Extracted: 06/10/97 Concentrated Extract Volume: 500 (uL) Date Analyzed: 06/19/97 Injection Volume: 2.0 (uL) Dilution Factor: 1.0 GPC Cleanup: (Y/N) Y pH: ____. CONCENTRATION UNITS: Number TICs found: 3 (ug/L or ug/Kg) UG/KG

CAS NUMBER COMPOUND NAME RT EST. CONC. Q 1. Unknown alkane 31.52 420. J 2. Unknown alkane 34.16 340. J 3. Unknown alkane 35.31 2400. J 4. Unknown alkane 36.62 340. J 5. Unknown alkane 33.22 '. 5400. J 6. Unknown alkane 40.10 420. J 7. Unknown alkane 42.34 2700. J 6. Unknown alkane 43.16 930. J 9. yV 10. 11. 12. 13. 14. 15. 16. 17. 18. 19. 20. 21. 22. , 23. / 24. 2b. . 26. 27 . 29. 30.

FORM I SV-TIC OLM03.2

AR302938 IF EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET BRH29 Lab Name: LANCASTER LABS Contract: Lab Code: LANCAS Case No.: ____. SAS No.: ____. SDG No.: (soil/water) SOIL Lab Sample ID: 2723086 Sample wt/vol: 30 (g/mL) G Lab File ID: >JF259 Level: * (low/med) LOW Date Received: 06/06/97 % Moisture: 31 decanted: (Y/N) N Date Extracted: 06/10/97 Concentrated Extract Volume: 500 (uL) Date Analyzed: 06/19/97 Injection Volume: 2.0 (uL) Dilution Factor: 1.0 GPC Cleanup: (Y/N) Y pH: ____. CONCENTRATION UNITS: Number TICs found: 30 (ug/L or ug/Kg) UG/KG -

CAS NUMBER COMPOUND NAME . RT EST. CONC. ====:r: ==s_ _.=_===_= s==r ____-L_- 1. Unknown ~~127l6 140. J.~ 2. Unknown 27.68 140. J 3. Unknown carboxylic acid 28.28 340. J 4. Unknown carboxylic acid 28.46 590. J 5. Unknown 29.09 190. J 6. Unknown 29.84 140. J 7. Unknown 29.99 140. J 6. Unknown carboxylic acid 30.37 ' 800. J 9. Unknown x 30.59 150. J 10. HH-Benzo[a]fluorene 31.29 210. J X 11. Unknown 31.53 440. J >2. HH-Benzo[b]fluorene 31.78 140. J X -43. Unknown 32.40 280. J 14. Unknown 32.72 280. J lb. Unknown 33.07 140. J 16. Unknown 36.99 600. J 17. Unknown 37.12 180. J 18. Unknown 37.29 800. J 19. Unknown 38.32 1000. J 20. Unknown 38.61 -170. J 21. 192972 Benzo [e] pyrene 39.10 5-20. J N 22. Unknown 40.43 230. J 23. Unknown 41.08 730. J 24. Unknown 43.06 4200. J 2b. Unknown , 43.94 610. J 26. Unknown •' 45.05 670. J 2Y. Unknown 46.46 440. J 26. Unknown 48.10 180. J 29. Unknown 49.03 150. J 30. Unknown 49.62 1200. J

FORM I SV-TIC OLM03.2

AR302939 395 IF EPA SAMPLE NO ALKANE SUMMARY BRH29 Lab Name: LANCASTER LABS Contract: Lab Code: LANCAS Case No.: ____. SAS No.: ____. SDG No.: Matrix: (soil/water) SOIL Lab Sample ID: 2723036 Sample* wt/vol: 30 ' (g/mL) G Lab File ID: XTF259 Level: (low/med) LOW Date Received: 06/06/97 % Moisture: 31 decanted: (Y/N) N Date Extracted: 06/10/97 Concentrated Extract Volume: 500 (uL) Date Analyzed: 06/19/97 Injection Volume: 2.0 (uL) Dilution Factor: 1.0 GPC Cleanup: (Y/N) Y pH: ____. CONCENTRATION UNITS: Number TICs found: 9 (ug/L or ug/Kg) UG/KG

CAS 'NUMBER COMPOUND NAME RT EST. CONC. Q 1. Unknown alkane 32.31 250. J 2. Unknown alkane 33.18 620. J 3. Unknown alkane 34.16 220. J 4. Unknown alkane 35.31 310. J 5. Unknown alkane 36.63 180. J 6. Unknown alkane 33.21 ' 2200. J Unknown alkane 40.09 . 300. J 6. Unknown alkane 42.32 970. J 9. Unknown cycloalkane 42.55 530. J V 10. 11. 12. • 13. 14. 16. 17. 18. 19. . 20. 21. 22. • 23. 24. 25. 26. 27. 26. 29. • 30. .

FORM I SV-TIC OLM03.2

396 AR3029l*0 IF EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET BRH31 0 Name: LANCASTER LABS Contract Lab Code: LANCAS Case No.: ____. SAS No.: . SDG No.: Matrix:1 (soil/water) SOIL •. - __^ ^ Lab Sample ID: 2723087 Sample wt/vol: 30 (g/mL)\G \ Lab File ID: >JF260 Level: (low/med) LOW * Date Received: 06/06/97 % Moisture: 33 decanted: (Y/N) N Date Extracted: 06/10/97 Concentrated Extract Volume: 500 (uL) Date Analyzed: 06/19/97 Injection Volume: 2.0 (uL) Dilution Factor: 1.0 GPC Cleanup: (Y/N) Y pH: ___. CONCENTRATION UNITS: Number TICs found: 30 (ug/L or ug/Kg) UG/KG

CAS NUMBER COMPOUND NAME . RT EST. CONC. Q 1. Unknown carboxylic acid 26.11 690. J 2. Unknown 27.68 700. J 3. Unknown 28.30 2100. J 4. Unknown carboxylic acid 28.49 '. 3500. J 5. Unknown 29.58 310. J 6. Unknown 29.87 530. J 7. Unknown 29.99 420. J 8. Unknown carboxylic acid 30.38 1000. J s _ /9 . Unknown 31.53 670. J 10. Pyrene, 2 -methyl- 31.79 450. J X 11. Unknown 33.18 1200. J 12. Unknown 37.32 1000. J 13. Unknown phthalate 38.90 370. J 14. .1929 /2 Benzo [e] pyrene 39.14 1100. J N 15. Unknown 40.43 460. J 16. Unknown 41.11 1400. J 17. Unknown 42.14 500. J 16. Unknown 42.59 1200. J 19. Unknown 43.08 1800. J 20. Unknown 43.97 2500. J 21. Unknown ' ^ 44.30 490. J 22. Unknown / 45.06 2300. J 23. Unknown 46.90 880. J 24. Unknown 47.69 890. J 2b. Unknown 47.91 360. J 26. Unknown 48.56 460. J 27. Unknown 49.73 4400. J 26. Unknown 50.15 310. J 29. Unknown 50.47 1100. J 30. Unknown 51.57 860. J t

FORM I SV-TIC OLM03.2

AR3029M 461 IF EPA SAMPLE NO. ALKANE SUMMARY BRH31 Lab Name: LANCASTER LABS Contract: Lab Code: LANCAS Case No.: ____ . SAS No.: ____ . SDG No.:. Matrix: (soil/water) SOIL Lab Sample ID: 2723037 Sample' wt/vol: 30 (g/mL) G Lab File ID: >JF260 Level: (low/med) LOW Date Received: 06/06/97 % Moisture: 33 decanted: (Y/N) N Date Extracted: 06/10/97 Concentrated Extract Volume: 500 (uL) Date Analyzed: 06/19/97 Injection Volume: 2.0 (uL) Dilution Factor: 1.0 GPC Cleanup: (Y/N) Y pH: ____ . CONCENTRATION UNITS: Number TICs found: 9 (ug/L or ug/Kg) UG/KG

CAS NUMBER COMPOUND NAME RT EST. CONC. Q S-3_-SSC 1. Unknown alkane 25.36 570. J 2. Unknown alkane 34.17 530. J 3. Unknown alkane 35.33 1700. J 4. Unknown alkane 36.65 440. J 5. Unknown alkane 33.24 • 3400. J 6. Unknown cycloalkane 33.33 • 1200. J 7. Unknown alkane 40.12 620. J 8. Unknown alkane 42.36 2600. J 9. Unknown alkane 43.20 1300. J 10. N 11. 12. 13. 14. 15. 16. 17. 18. 19. - 20. 21. 22. 23. 24. / 25. 26. 2/. 28. 29. ,• 30. •

FORM I SV-TIC OLM03.2

AR3029l*2 IF EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET BRH33 Lab Name: LANCASTER LABS Contract: Lab Code: LANCAS Case No.: ___ . SAS No.: ____. SDG No.: trix: (soil/water) SOIL Lab Sample ID: 2723088 Sample wt/vol: 30 (g/mL) G Lab File ID: >JF261 Level:* (low/med) LOW Date Received: 06/06/97 % Moisture: 40 decanted: (Y/N) N Date Extracted: 06/10/97 Concentrated Extract Volume: 500 (uL) Date Analyzed: 06/19/97 Injection Volume: 2.0 (uL) Dilution Factor: 1.0 GPC Cleanup: (Y/N) Y pH: ___. CONCENTRATION UNITS: Number TICs found: 30 (ug/L or ug/Kg) UG/KG

CAS NUMBER COMPOUND NAME RT EST. CONC. ______«__=_ == Benzocycloheptatriene 19.21 720. J X 2. Naphthalene, '2-ethenyl- 21.78 910. J X 3. Unknown 25.41 820. J 4. Unknown carboxylic acid 28.29 460. J 5. Unknown carboxylic acid 28.46 780. J 6. Anthracene, 1 -methyl - 28.75 590. J X 7. Anthracene , 9 , 10-dimethyl- 29.83 690. J X 8. Benzene, 1, !'-(!, 3 -butaaiyne 30.64 . • 790. J X 9. HH-Benzo [fa] f luorene 31.31 680. J X 10. llH-Benzorbi f luorene 31.52 1300. J X 11. HH-Benzo [b] f luorene 31.69 590. J X ^2. Pyrene, 2-methyl- 32.02 580. J X llH-Benzo [ a ] f luorene 32.09 460. J X ^.4w2-. Unknown 33; 18 670. J 15. Unknown 34.17 650. J 16. 82O53 7H-Benz [del anthracen-7-one 34.28 490. •J"N 17. Chrysene, 5 -me thy 1- 35.13 850. J X 18 . Unknown 35.32 2200. J 19. Unknown 35.69 600. J 20. Unknown 36.99 510. J 21. Unknown 37.30 500. J 22. Benzo fkl f luoranthene 38.31 2000. J X 23. 192972 Benzo rejpyrene 39.16 1400. J N 24. Benzo [ejpyr ene 39.83 630. J X 2b. Unknown 41.11 870. J 26. Unknown / 42.54 620. J 27. Unknown 43.95 1400. J 26. Unknown 45.05 470. J 29. Benzo [b] chrysene 45.63 540. J X 30. Unknown 49.64 1100. J

FORM I SV-TIC OLM03'.2

AR3029i)3 532 IF EPA SAMPLE NO. ALKANE SUMMARY BRH33 Lab Name: LANCASTER LABS Contract: Lab Code: LANCAS Case No.: ____. SAS No.: ____. SDG No.: Matrix:, (soil/water) SOIL Lab Sample ID: 2723083 Sample wt/vol: 30 (g/mL) G Lab File ID: >JF261 Level: (low/med) LOW Date Received: 06/06/97 % Moisture: 40 decanted: (Y/N) N Date Extracted: 06/10/97 Concentrated Extract Volume: 500 (uL) Date Analyzed: 06/19/97 Injection Volume: 2.0 (uL) Dilution Factor: 1.0 GPC Cleanup: (Y/N) Y pH: ____. CONCENTRATION UNITS: Number TICs found: 2 (ug/L or ug/Kg) UG/KG

CAS NUMBER COMPOUND NAME RT EST. CONC. Unknown alkane 38.23 1500. J 2. Unknown alkane 42.33 970. J 3. 4. - 5. 6. 7. 8. 9. V 10. 11. 12. 13. 14. 15. • 15. 17. 16. % 19. 20. 21. 22. ' 23. i 24. 25. 25. 27. 28. 29. 30.

FORM I SV-TIC OLM03.2

AR3029H IF EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET BRH34 Lab Name: LANCASTER LABS Contract: Lab Code: LANCAS Case No..: ____. SAS No.: _____. SDG No.: irix: (soil/water) SOIL Lab Sample ID: 2723089 Sample wt/vol: 30 (g/mL) G Lab File ID: >JF262 Level: '• (low/med) LOW ' Date Received: 06/06/97 % Moisture: 31 decanted: (Y/N) N Date Extracted: 06/10/97 Concentrated Extract Volume: 500 (uL) Date Analyzed: 06/19/97 Injection Volume: 2.0 (uL) Dilution Factor: 1.0 GPC Cleanup: (Y/N) Y pH: ___. CONCENTRATION UNITS: Number TICs found: 30 (ug/L or ug/Kg) UG/KG .

CAS NUMBER COMPOUND NAME RT EST. CONC. Q 1. Unknown 27.22 940. . J 2. Unknown 28.31 1700. J 3. Unknown carboxylic acid ' 28.49 2800. J 4. Unknown 29.46 1100. J 5. Unknown 29.56 9200. J 6. Unknown 29.87 1100. J 7. Unknown 29.99 - 1000. J 6. Unknown 30.31 • 1800. J 9. Unknown carboxylic acid 30.38 810. J 10. Unknown 4 31.53 510. J 11. Unknown 31.79 580. J 2. Unknown 32.02 720. J Unknown 32.62 770. J 14. Unknown 33.18 1700. J 15 . Unknown 35.33 2000. J 16. Unknown 37.00 790. J 17. Unknown 37.31 2700. J 18 . Unknown 38.33 2600. J 19. Unknown 41.09 2500. J 20. Unknown 42.55 1000. J 21. Unknown 42.76 500. J 22. Unknown 43.52 760. J 23. Unknown 43.95 1300. J 24. Unknown 45.06 1000. J 2b. Unknown 46.92 890. J 26. Unknown • • / 47:67 790. J 27. Unknown 49.75 8400. J . 26. Unknown 50.16 500. J 29. Unknown 50.49 740. J 30. Unknown 51.57 2000. J

FORM I SV-TIC OLM03.2

AR3029l»5 592 IF EPA SAMPLE NO. ALKANE SUMMARY BRH34 Lab Name: LANCASTER LABS Contract: Lab Code: LANCAS Case No.: ____ . SAS No.: ____ . SDG No.: Matrix: (.soil/water) SOIL Lab Sample ID: 2723089 Sample- wt/vol: 30 (g/mL) G lab File ID: >JF262 Level: (low/med) LOW Date Received: 06/06/97 % Moisture: 31 decanted: (Y/N) N Date Extracted: 06/10/97 Concentrated Extract Volume:' 500 (uL) "'-"Date Analyzed: 06/19/97 Injection Volume: 2.0 (uL) Dilution Factor: 1.0 GPC Cleanup: (Y/N) Y pH: ____ . CONCENTRATION UNITS: Number TICs found: 3 (ug/L or ug/Kg) UG/KG

CAS NUMBER COMPOUND NAME RT EST. CONC. Q 1. Unknown alkane 33.23 3700. J 2. Unknown alkane 42.35 3300. J 3. Unknown alkane 43.16 1600. J 4. 5. - 6. 7. 3. 9. 10. v,J 11. 12. • 13. 14. lb. 16. 17. 16. 19. , 20. 21. 22. 23. ' 24. / 25. 26. 27. 26. 29. 30. .

FORM I SV-TIC OLM03.2

593 IT EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET BRH36 Lab Name: LANCASTER LABS Contract: T_b Code: LANCAS Case No.: ____. SAS No.: ____. SDG No.: ____, Siatrix: (soil/water) SOIL Lab Sample ID: 2723090 Sample wt/vol: 30 (g/mL) G Lab File ID: >JF263 Level: (low/med) LOW Date Received: 06/06/97 % Moisture: 30 decanted: (Y/N) N Date Extracted: 06/10/97 Concentrated Extract Volume: 500 (uL) Date Analyzed: 06/19/97 Injection Volume: 2.0 (uL) Dilution Factor: 1.0 GPC Cleanup: (Y/N) Y pH: ___. CONCENTRATION UNITS: Number TICs found: 30 (ug/L or ug/Kg) UG/KG -

RT EST. CONC. CAS NUMBER _COMPOUND_NAME --__.- Unknown carboxylic acid 26.13 ~8507 J Unknown 27.67 270. J Unknown 28.30 1400. J Unknown carboxylic acid 28.53 8400. J Unknown 30.30 26000. J Unknown 30.36 1300. J Unknown carboxylic acid 30.43 ". 2400. J Unknown 30.95 540. J Unknown <• 31.54 1100. J Unknown 31.79 630. J Unknown 32.08 1100. J Benzo £ b]naphtho[2,1-d]thioph 33.10 250. J X Unknown 34.17 340. J Unknown 35.70 320. J Unknown 36.99 300. J Unknown 37.30 490. J .-192972 Benzo[e]pyrene 39.15 770. J N Unknown 40.42 400. J Unknown 41.10 840. J Unknown 43.02 2400. J Unknown 43.94 14-00. J Unknown 45.07 800. J Unknown 46.46 780. J Unknown 46.90 440. J Unknown / 47.63 260. J Unknown 47.89 300. J Unknown 48.15 380. J Unknown 49.67 2100. J Unknown 50.44 590. J Unknown 51.53 760. J

FORM I SV-TIC OLM03.2

AR30291*? 653 IF EPA SAMPLE NO. ALKANE SUMMARY BRH36 Lab Name: LANCASTER LABS Contract: Lab Code: LANCAS Case No.: ____ . SAS No.: ____ . SDG No.: Matrix: (soil/water) SOIL Lab Sample ID: 2723090 Sample 'wt/vol: 30 (g/mL) G Lab File ID: >JF263 Level: (low/med) LOW Date Received: 06/06/97 % Moisture: 30 decanted: (Y/N) N Date Extracted: 06/10/97 Concentrated Extract Volume: 500 (uL) Date Analyzed: 06/19/97 Injection Volume: 2.0 (uL) Dilution Factor: 1.0 GPC Cleanup: (Y/N) Y pH: ____ . CONCENTRATION UNITS: Number TICs found: 6 (ug/L or ug/Kg) UG/KG

CAS NUMBER COMPOUND NAME RT EST. CONC. Q 1. Unknown alkane 33.13 440. J 2. Unknown alkane 35.30 830. J 3. Unknown alkane 33.23 4000. J 4. Unknown alkane 40.10 350. J 5. Unknown alkane 42.34 • 1600. J 6. Unknown cycloalkane 42.56 • 310. J 7. ^ 6. 9. 10. > 11. 12. 13. 14. Ib. 16. 17. 18. 19. - 20. 21. 22. 23. , 24. 2b. • 26. 21. 28. 29. 30. ••

FORM I SV-TIC OLM03.2

AR.30291.8 654 IF EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET BRH38 Lab Name: LANCASTER LABS Contract: Lab Code: LANCAS Case No.: ____. SAS No.: ____. SDG No.: Watrix: (soil/water) SOIL Lab Sample ID: 2723091 Sample wt/vol: 30 . (g/mL) G Lab File. ID: >JF264 *. Level: (low/med) LOW Date Received: 06/06/97 % Moisture: 32 decanted: (Y/N) N Date Extracted: 06/10/97 Concentrated Extract Volume: 500 (uL) Date Analyzed: 06/19/97 Injection Volume: 2.0 (uL) Dilution Factor: 1.0 GPC Cleanup: (Y/N) Y pH: ____. CONCENTRATION UNITS: Number TICs found: 30 (ug/L or ug/Kg) UG/KG -

CAS NUMBER COMPOUND NAME RT EST. CONC. = ____=: _____ 1. 1.3, 6-i_eptatriene .2,5, 5-tri 12.11 J X 2. Bicyclo[2.2.1]heptan-2-ol, 1 18 . 99 450. J X 3. Unknown 25.38 270. J 4.. Unknown 28.29 670. J 5. Unknown carboxylic acid 28.48 1500. J 6. 4H-Cyclopenta [ oef ] phenanthre 28.75 400. J X 7. Unknown 29.57 310. J 8. Unknown 29.87 390. J 9. Unknown carboxylio acid 30.37 430. J 10. HH-Benzo [ a ] f luorene 31.53 580. J X 11. Unknown 34.16 1100. J J 12. Unknown 35.71 550. J 13. Unknown 37.32 500. J 14. 192972 Benzo [e] pyrene 39.16 1500. J N 15. Benzo [ j j f luoranthene 39.83 360. J X 16. Unknown 40.41 650; J 17. Unknown .41.08 1000. J 18. Unknown 41.36 270. J 19. Unknown 42.57 700. J 20. Unknown 43.07 400. J 21. Unknown 43.26 270. J 22. Unknown 43.95 630. J 23. Unknown 44.29 300. J 24. Unknown • , ' 45.10 1200. J 2b. BENZO [ A] NAPHTHAQENE 47.52 350. J X 26. Unknown 47.91 310. J 27. Unknown 49.69 2600. J 28. Unknown 50.18 390. J 29. Unknown 50.46 340. J' 30. Unknown 51.52 390. J

FORM I SV-TIC OLM03.2

AR3029i*9 716 IF EPA SAMPLE NO. ALKANE SUMMARY BRH38 Lab Name: LANCASTER LABS Contract: Lab Code: LANCAS Case No.: ____. SAS No.: ____. SDG No.: Matrix: (soil/water) SOIL Lab Sample ID: 2723091 Sample wt/vol: 30 (g/mL) G Lab File ID: >JF264 Level: (low/med) LOW Date Received: 06/06/97 % Moisture: 32 decanted: (Y/N) N Date Extracted: 06/10/97 Concentrated Extract Volume: 500 (uL) Date Analyzed: 06/19/97 Injection Volume: 2.0 (uL) Dilution Factor: 1.0 GPC Cleanup: (Y/N) Y pH: ____. CONCENTRATION UNITS: Number TICs found: 7 (ug/L or ug/Kg) UG/KG

CAS NUMBER COMPOUND NAME RT EST. CONC. _=Q__ 1. Unknown alkane "33.18 330. J 2. Unknown alkana 35.31 2000. J 3. Unknown alkane 36.64 360. J 4. Unknown alkane 33.24 3300. J 5. Unknown alkane 40.11 570. J 6. Unknown alkane 42.36 2200. J 7. Unknown alkane 43.20 1000. J 3. 9. 10. 11. • 12. 13. 14. Ib . 16. 17. 13. 19. • 20. 21. 22. f 23. i . 24. 25. 26. 27. 26. 29. 30.

FORM I SV-TIC OLM03.2

AR302950 '17 IF ., EPA SAMPLE NO, SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET BRH39 Lab Name: LANCASTER LABS Contract: Code: LANCAS Case No.: _____. SAS No.: ____. SDG No.: Matrix: (soil/water) SOIL Lab Sample ID: 2723092 Sample'wt/vol: 30 (g/mL) G Lab File ID: >JF265 Level: (low/med) LOW Date Received: 06/06/97 % Moisture: 28 decanted: (Y/N) N Date Extracted: 06/10/97 Concentrated Extract Volume: 500 (uL) Date Analyzed: 06/19/97 Injection Volume: 2.0 (uL) Dilution Factor: . 1.0 GPC Cleanup: (Y/N) Y pH: ____. CONCENTRATION UNITS: Number TICs found: 30 (ug/L or ug/Kg) UG/KG

CAS NUMBER COMPOUND NAME RT EST. CONC. _=__— 1. Unknown 16.50 400. J 2. IH-Indene, 1,1-dimethyl- 18.80 370. J X 3. 90120 Naphthalene, 1-methyl- 19.77 3200. J N 4. Naphthalene, 2-ethenyl- 20.85 490. J X 5. Naphthalene, 1-ethyl- 21.19 520. J X 6. Naphthalene , 1,3 -dimethyl- 21.36 • 3200. J X 7. Naphthalene , 1 . 4 -dimethyl- 21.60 3400. J X 8. Naphthalene, 2 -ethyl- 21.96 2000. J X 9. Naphthalene, 2-(l-methylethy 22.94 750. J X ,10. Naphthalene , 1,4, 6-trimethyl 23.37 500. J X ^r 11. Naphthalene , 1,4, 6-trimethyl 23.60 650. J X 12. Naphthalene , 1,4, 6-trimethyl 23.88 560. J X 13. IH-Phenalene 24.24 360. J X 14. Benzene, [l-(2,4-cyclopentad 24.47 440. J X 15. •- 9H-Fluorene, 1 -methyl - 25.96 540. J X 16. 9H-Fluorene, 9-methyl- 26.07 350. J X 17. 9H-Fluorene, 1 -methyl - 26.56 380. J X 16. 132650 Dibenzothiophene 26.82 730. J N 19. Anthracene, 1-methyl- 28.46 850. J X 20. Anthracene, 1 -methyl - 28.53 370. J X 21. 6H-CYCLOBUTAf JK] PHENANTHRENE 28.76 1100. J X 22. llH-Benzo [b] tluorene 31.53 440. J X 23. Unknown 37.31 1200. J 24. 192972 Benzo [e] pyrene I 39.14 880. J N 25. Unknown 40.46 370. J 26. Unknown 41.10 1500. J 27. Unknown 43.03 420. J 26. Unknown 45.06 590. J 29. Unknown 49.67 1600. J 30. Unknown 51.53 560. J

FORM I SV-TIC OLM03.2

AR30295I 7S7 IF EPA SAMPLE NO. ALKANE SUMMARY BRH39 Lab Name: LANCASTER LABS Contract: Lab Code: LANCAS Case No.: . SAS No.: . SDG No.: Matrix: (soil/water) SOIL Lab Sample ID: 2723092 Sample* wt/vol: 30 (g/mL) G Lab File ID: >JF265 Level: (low/med) LOW Date Received: 06/06/97 % Moisture: 23 decanted: (Y/N) N Date Extracted: 06/10/97 Concentrated Extract Volume: 500 (uL) Date Analyzed: 06/19/97 Injection Volume: 2.0 (uL) Dilution Factor: -1.0 GPC Cleanup: (Y/N) Y pH: ____ . CONCENTRATION UNITS: - Number TICs found: 7 (ug/L or ug/Kg) UG/KG

CAS NUMBER COMPOUND NAME RT EST. CONC. __Q__ 1. Unknown alkane 35.31 740. J 2. Unknown alkane 33.23 3200. J 3. Unknown cycloalkane 33.33 1000. J 4. Unknown alkane 40.09 370. J 5. Unknown alkane 42.34 1900. J 6. Unknown cycloalkane 42.56 550. J 7. Unknown alkane 43.16 710. J 8. \ 9. 1110. ——— ^ 12. 13. 14. 15. 16. 17. 18. 19. 20. • 21. 22. 23. ' 24. 2b. t 26. ' 27. 28. 29. 30. •*

FORM I SV-TIC OLM03.2

AR302952 7Ss . . :.-••••,. ;: -. ••:-1:V"V->-^-:;,-:V^^- ,/.-;•-.,,/.'-. , • - • - •- , -..- - ••• • - ••- . -~% * • •*' • • -..-•-.. -. . . ;-,'."="- • •.•••..•••••-'•'•-- • ;" . ; - '.'-•.'••.•••.-••-.'•>•*»*J090^,: ^ ^£l*OU__yD1 j •--,-;••••-•:.-_-,- --..-. -". •'- -"•;.• •' - •••-/'••:• - -.-••.-. "' -...'.'•:'- -.-.-..•••.• ;-:v--- '.-.-• • •vv-'^'^-n'- --,, r.- :-^> -.•-••-:•'..:. -,;,•. .:..?.•„.'.^-;.-;^-^: •.--.:'.-:.;•- ;:••.-.• .< -•.- - -.;• - -.'•'"•-''••"'• .... . :--- 7B SEMIVOLATILE CONTINUING CALIBRATION CHECK

'•> Name: LANCASTER LABS Contract: Lab Code: LANCAS Case No.: ____ . SAS No.: ____ . SDG No.: Instrument ID: HP05525- Calibration Date: 06/18/97 Time: 15:26 Lab File ID: >JF241 Init. Calib. Date(s): 06/11/97 06/11/97 Init. Calib. Times: 10:24 18:55 M1N MAX COMPOUND REF RRF50 RRF %D %D I"1 - g~*gr*^1"™' -C_i' smmas BBSS: N-Nitrosodimethvlamine 1.087 1.300 19.6 pyriaine 1.746 2 . 152 23.3 2-Picoline 1.745 2.025 16.0 pnenoi 1.647 1.974 .800 19.8 25. 0 Aniline '1.894 2.145 13.3 cis (2-cnioroetnyi) etner 1.382 1.600 .700 15.8 25.0 2 -cnioropnenoi 1.285 1.437 .800 11.8 25.0 i, 3-oicnioroDenzene 1.388 1.453 .600 4.6 25.0 i , 4 -oicniorooenzene 1.400 1.477 .500 5.6 25.0 Benzyl aiconoi .859 .984 14.5 i, 2-Dicniorooenzene 1.252 1.329 .400 6.2 25.0 2 -Mechy ipnenoi 1.139 1.312 .700 15.2 25.0 2.21 -oxybis ( i-chioropropane) 1.708 2.244 31.4 bis (2-Chloroisopropyl) ether 1.708 2.244 31.4 4 -Methylphenol 1.207 1.384 .600 14.7 25.0 Acetopnenone 1.905 2.247 18.0 N-Nirroso-ai-n-propyiamxne 1.003 1.309 .500 30.6 25.0 o-Toluidine 1.846 2.019 9.4 Hexacnioroethane .717 .803 .300 12.0 25.0 Nirrooenzene .498 .601 .200 20.7 25.0 isophorone .908 1.078 .400 18.7 25.0 2-Nitropnenoi • .237 .257 .100 8.6 25.0 2 , 4-Dimetnyipnenoi .458 .521 .200 13.9 25.0 benzoic acia .393 .383 2.6 bis ( 2.--cnioroetn6xy ) metnane .490 .556 ..300 13.4 25.0 2 , 4-Dichlorophenol .324 .330 .200 1.9 25.0 1,2,4 -Tricnlorocenzene .342 .343 .200 .3 25.0 wapntnaiene .984 1.048 .700 6.4 25.0 4-cnioroaniiine .448 .469 4.~8 * Hexacniorotmtactiene .215 .213 .6 4-cnioro-3-mernyipneriol .388 .461 .200 18.6 25.0 2-Methylnaphthalene • .633, .675 .400 6.7 25.0 i-Mecnyinapntnaiene /.582 .630 8.3 -.exacnlorocyciopentacirehe • .448 .407 9.1 2,4, 6-Trichlorophenol /.417 .431 .200 3.4 25.0 2,4, 5 -Tri cnioropnenoi .425 .460 .200 8.1 25.0 ij-Q-hloronaphthalene ' 1.208 1.241 .800 2.8 25.0 2-Nirroaniline .505 .693 37.2 oimetnyipnrnaiate 1.495 1.656 10.7 2 , 6-oinitrotoiuene .367 .404 .200 10.2 25.0 Acenaphthylene 1.853 1.965 .900 6.1 25.0 3-wi_roannine .403 .458 13.8 Acenapntnene 1.054 1.127 .900 6.9 25.0 2 , 4-Dinitropnenoi .223 .203 9.2 4-wirropnenoi .335 .412 22.8 Dibenzoruran 1.584 1.665 .800 5.2 25.0 i , 4-uinicro_oiuene .506 .572 .200 13.0 25.0 , Ail otner compounds must meet a minimum Kir ot c.010.

FORM VII SV-1 OLM03.2 AR30295U 914 7C SEMIVOLATILE CONTINUING CALIBRATION CHECK l Lab Name: LANCASTER LABS Contract: ____. Lab Code: LANCAS Case No.: ____. SAS No.: ____. SDG No.: Instrument ID: HP05525 Calibration Date: 06/13/97 Time: 15:26 Lab File ID: >JF241 ' Init. Calib. Date(s): 06/11/97 06/11/97 Init. Calib. Times: 10:24 13:55 M1N MAX COMPOUND RRF RRF50 RRF %D %D l-Naphthvlamine 1.061 1.025 3.4 2 -Napncny lamine 1.151 .992 13.3 Diechyipntnaiace 1.544 1.756 13.7 4-cnioropnenyi-pnenyietner .547 .531 .400 6.2 25.0 Fluorene 1.091 1.179 .900 3.0 25. -0 4-Nitroaniiina .363 .444 22.1 4 , 6-oinitro-2-mei:hyipnenoi .173 .175 1.7 N-Nitrosodiphenylamine (1) .523 .547 4.6 1 , 2-Diphenylhydrazine 1.040 1.232 13.4 4-sromopnenyi-pnenyieth'er . .224 .224 .100 .2 25.0 Hexachlorobenzene .252 .260 .100 3.3 25.0 penracnioropnenoi .136 :i49 .050 19.3 25.0 pnenantnrene 1.027 1.069 .700 4.1 25.0 Antnracene 1.002 1.041 .700 3.3 25.0 carcazoie .963 1.041 7.6 Di-n-Duryipntnaiaca 1.554 1.659 6.7 Fluorantnene 1.033 1.131 .600 9.0' 25.0 senzidine C2) .820 .662 19.3 _*yrene 1.506 1.522 .600 1.0 25.0 BUcyiBenzyiphtnaiate .931 1.075 9.5 3,3* -oicnlorooenz iaina .477 .449 5.9 senzo(a) anrnracene 1.165 1.237 .30.0 6.2 25.0 bis(2-fithyihexyi)pnthalat"e " 1.133 1.331 12.0 Chrysene — 1.030 1.097 .700 1.6 25.0 Di-n-octyipntnaiate 2.532 3.123 23.3 7 , 12-Dimechyifienz [a j antnface .572 .547 4.3 Benzo (b) f luoranthene 1.327 1.434 .700 3.0 25.0 Benzo (k)f luoranthene " " 1.220 1.283 .700 5.6 25.0 aenzoc a) pyrene 1.111 1.149 .700 3.5 25.0 inaeno (1,2. 3-cd) pyrene .943 .835 .500 12,0 25. -0 uibenz ( a , h) anrnracene .867 .300 .400 7.3 25.0 aenzo(cf,h,i)parvlene .874 .733 .500 16.2 25.0 S3SSB3SE 2 -Fluorophenol 1.410' 1.534 .600 12.3 25.0 phenoi-as 1.723 2.010 .300 16.3 25.0 2 -cm oropnenoi -d4 1.233 1.436 .300 11.9 25.0 i, 2-uicnlorooenzene-a4 ' .912 .953 .400 4.5 25.0 Nitrobenzene-dS .543 .652 .200 19.0 25.0 z-i-luoroDipnenyi 1.367 1.407 .700 2.9 25.0 2 , 4 , 6-Trioromopnenoi (O__MOI. .233 .255 7.1 2,4, 6-Tribromophenol (OLM03 . .154 .157 2.2 Terphenyl-dl4 1.116 1.103 .500 1.2 25.0 [11 Cannot be separated from Diphenylamine ;2) Benzidine level in the 50 standard is 200 ng/2uL. All other compounds must meet a minimum RRF of 0.010. FORM VII SV-2 OLM03.2

AR302955 91S SEMIVOLATILE CONTINUING CALIBRATION CHECK

Tab Name: LANCASTER LABS Contract: Code: LANCAS Case No.: . SAS No.: -. SDG No.: Instrument ID: HP05525. " 'Calibration Date: 06/19/97 Time: 03:54 Lab File ID: XTF256 Init. Calib. Date(s): 06/11/97 06/11/97 Init. Calib. Times: 10:24 18:55 M1N MAX COMPOUND Rra' RRF50 RRF %D %D N-N: .trosodimethylamine 1.087 1.274 17?! Pyr:.dine — .. 1.746 2.034 16.5 2-ficoline 1.745 1.933 10.8 Fnenoi 1.647 1.931 .800 17.2 25.JO Aniline 1.894 2.130 12.5 cis (2-cnioroetnyi) etner 1.382 1.602 .700 16.0 25.0 2-cnioropnenoi 1.285 1.438 .800 11.9 25.0 i , 3-DicnioroJoenzene 1.388 1.505 .600 8.4 25.0 i , 4 -DicnioroDenzene 1.400 1.507 .500 7.7 25.0 eenzyl alconol ~ ' .859 .980 14.1 i, 2-Dicmorobehzene 1.252 1:376 .400 9.9 25.0 2-Metnyipnenoi 1.139 1.306 .700 14.6 25.0 2 1 2 • -oxybis ( i-cftibropropane)1.708 2.260 32.3 bis (2-Chloroisopropyl) ether 1.708 2.260 32.3 4 -Methylphenol 1.207 1.367 .600 13.2 25.0 Acetopnenone 1.905 2.197 15.3- N-witroso-di-n-propyiamine 1.003 1.298 .500 29.4 25.0 o-Toluidine 1.846 2.063 11.7 tiexacm oroe thane .717 .804 .300 12.2 25.0 Nitrobenzene .498 .589 .200 18.4 25.0 isopnorone .908 1.052 .400 15.8 25.0 2-mrrophenoi -.237 .249 .100 5.3 25.0 2 , 4 -Dime tnyipnenoi .458 .506 .200 10.6 25.0 Benzoic acid .393 .387 1.7 ois (_j-cnJLoroetnoxy) metnane .490 .543 .300 10.9 25.0 2 , 4-Dichlorophenol .324 .322 .200 .6 25.0 i,2,4-Tricnioro&enzene .342 .342 .200 .0 25.0 wapntnalene .984 1.051 .700 6.7 25.0 4-cnioroaniiine .448 .473 5.7 • HexacnioroDUtadiene .215 .218 1.5 4-cnioro-3 -metnyipnenoi .388 .431 .200 11.0 25.0 2-Methylnaphthalene — '""" .633 .649 .400 2.5 25.0 i-nernyinapncnaiene ' .582'.606 4.2 Hexachlorocyciopentadiene '.448 .394 12.2 2,4,6-Trichlorophenol — " . .417 .421 .200 .8 25.0 2,4, 5-Trichloropnenol 1 .425 .469 .200 10.3 25.0 2-chloronapnrnaiene 1.208 1.245 .800 3.1 25.0 2-Nitroaniline .505 .666 32.0 uimernyipncnaiace 1.495 1.599 7.0 2 , 6-Dinitrotoluene .367 .393 .200 7.2 25.0 Acenaphthy 1 ene 1.853 1.937 .900 4.5 25.0 3-Nicroaniiine .403 .438 8.9 Acenapnrnene 1.054 1.110 .900 5.2 25.0 2 , 4-Dinitropnenoi .223 .186 16.5 4-Nicropnenoi .335 .383 14.2 uibenzoruran 1.584 1.626 .800 2.7 25.0 2 , 4-Dinicrotbiuene .506 .549 .200 8.6 25.0 AH other compounds must meet a nunimum REF or o.oio.

FORM VII SV-1 OLM03.2 AR302956 92± 7C SEMIVOLATILE CONTINUING CALIBRATION CHECK

Lab Name: LANCASTER LABS Contract: Lab Code: LANCAS Case No.: ____ . SAS No.: ___ _ . SDG No.: Instrument ID: HP05525 Calibration Date: 06/19/97 Time: 03:54 Lab File ID: >JF256 Init. Calib. Date(s) : 06/11/97 06/11/97 Init. Calib. Times: 10:24 13:55 M1W MAX COMPOUND KRT RRF50 RRF *D %D 1-Naphthvlamine =1.061 ~l7o73 1.6 2-Napntnviamine 1.151 1.106 3.9 Diethvlphthalate 1.544 1.715 11.0 4 -cnioropnenyi -pne'hyXe tner .547 .567 .400 3.5 25.0 Fluorene 1.091 1.143 .900 5.2 25 .-0 4-witroanmne .363 .405 11.4 4 , 6-Dinitro-2 -metnyipnenoi .173 .172 3.4 N-Nitrosodiphenylamine (1) .523 .539 3.0 1, 2-Diphenylhvdrazine 1.040 1.231 13.3 4-Bromophenyl-phenylefn"ef - .224 .219 .100 2.2 25.0 Hexachlorobenzene .252 ,250 .100 .6 25.0 pentacnloropnenoi .136 .144 .050 22.7 25.0 pnenantnrene 1.027 1.055 .700 2.7 25.0 Antnracene 1.002 1.047 .700 4.4 25.0 carcazoia .963 1.013 5.2 oi-n-DUtyipntnaiate 1.554 1.754 12.3 Fiuorantnene 1.038 1.095 .600 5.6' 25.0 Benzidine (2) .320 .746 9.0 pyrene 1.506 1.616 .600 7.3 25.0 Butyi&enzyipntnaiate .931 1.157 17.9 3,3' -Dichlorobenzidihe .477 .451 5.6 senzo (a ) antnracene 1.165 1.224 .800 5.1 25.0 bis i 2-£thylnexyl ) phthaiat'e 1.133 1.390 17.0 Chrysene 1.030 1.111 .700 2.9 25.0 oi-n-octyipntnaiate 2.532 3.287 29.3 7 , i2-*>DimethyiJDenz [a j anthrace .572 .577 .3 Benzo (b) f luoranthene 1.327 1.423 .700 7.6 25.0 Benzo (K iluorantnena 1.220 1.316 .700 7.9 25.0 Benzo (a pyrene 1.111 1.143 .700 3.4 25.0 indeno (1*2. 3-cd) pyrene .943 .342 .500 11-. 3 25:0 Dioenzc a, n\ antnracene .867 .330 .400 4.3 25.0 Benzo (g, n, i) peryiene .374 .791 .500 9.6 25.0 2 -Fluorophenol 1.4ld 1.573 .600 11.9 25.0 pnenoi-d5 1.723 1.950 .300 12.9 25.0 2-cnioropnenoi-d4 .1.233 1.417 .300 10.4 25.0 1 f 2-Dichlorobenzene-d4 .912 .966 .400 5.9 25.0 Nitrooenzene-d5 .548 .634 .200 15.3 25.0 2 -Fluorobiphenyl 1.367 1.402 .700 2.6 25.0 2,4, 6-TriDromopnenol ( OLMOI ... .238 .241 1.3 2,4, 6-Tribromophenol (OLM03 .- .154 .152 1.2 Terphenyl-dl4 1.116 1.142 .500 2.3 25.0 1) Cannot be separated from Diphanylamina 2) Benzidine level in the 50 standard is 200 ng/2uL. All other compounds must meet a minimum RRF or 0.010. FORM VII SV-2 OLM03.2

AR302957 922 IF EPA SAMPLE NO. SEMTVOLATILE ORGANICS ANALYSIS DATA SHEET SBLKLA161J ab Name: LANCASTER LABS Contract: Code: LANCAS Case No.: ___. SAS No.: ___. SDG No.: Matrix: (soil/water) SOIL Lab Sample ID: SBLKLA161 *. ' • Sample wt/vol: 30 (g/mL) G Lab File ID: >JF244 Level: (low/med) LOW Date Received: % Moisture: ___. decanted: (Y/N)__. Date Extracted: 06/10/97 Concentrated Extract Volume: 500 (uL) Date Analyzed: 06/18/97 Injection Volume: 2.0 (uL) Dilution Factor: 1.0 GPC Cleanup: (Y/N) Y pH: ___. CONCENTRATION UNITS: Number TICs found: 1 (ug/L or ug/Kg) UG/KG

CAS NUMBER COMPOUND NAME RT EST. CONC. ___?__ 1. Unknown 11.42 80. J N 2. 3. 4. f 5. . 6. 7. v e. 3. ^0. 11. . • 12. 13. , 14. Ib. 16. 17. 16. 19. 20. 21. 22. f 23. i 24. 25. • 26. 27. 28. 29. •• 30.

FORM I SV-TIC OLM03.2

944 AR302958