United States Patent (10) Patent No.: US 9,700,070 B2 Peet Et Al
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US0097.0007OB2 (12) United States Patent (10) Patent No.: US 9,700,070 B2 Peet et al. (45) Date of Patent: Jul. 11, 2017 (54) LOW BITTER CHICORY PRODUCTS 5,939,127 A 8, 1999 Abboud 7,214,507 B2 5/2007 Bouwmeester et al. (71) Applicant: REE PRAIRIE RANDs. INC., 2004/0224.0732004/0001898 A1 11/20041/2004 JanssensMalnoe et al. ilmington, DE (US) 2004/0241304 A1 12/2004 Bossard et al. (72) Inventors: Richard C. Peet, Wilmington, DE FOREIGN PATENT DOCUMENTS (US); Brad Justice, Wilmington, DE (US) FR 2834862 A1 * 7, 2003 ............. A21D 2,366 WO WO-02/13625 A2 2, 2002 (73) Assignee: BLUE PRAIRIE BRANDS, INC., W. w853.3 A. 1858. Wilmington, DE (US) WO WO-2016.057382 A1 4, 2016 (*) Notice: Subject to any disclaimer, the term of this patent is extended or adjusted under 35 OTHER PUBLICATIONS U.S.C. 154(b) by 0 days. Peters etal “A pilot Study on the effects of cultivation conditions of (21) Appl. No.: 14/875,093 chicory roots on the levels of Sesquiterpene lactones'. Food Research International vol. 29, Nos. 5-6, pp. 439-444, 1996.* (22) Filed: Oct. 5, 2015 Ravishankar et al "Chiciritum IntybusL-cultivation, Processing, utility, value addition and biotechnology, with an emphasis on (65) Prior Publication Data current status and future prospects”. Published in Journal of Science of Food and Agriculture, 81:467-484-2001.* US 2016/0095337 A1 Apr. 7, 2016 Nutrition facts and Analysis for chicory Roots, Self Nutrition data, O O Jun. 9, 2016, 4 pages.* Related U.S. Application Data PCT International Search Report and Written Opinion on applica (60) Provisional application No. 62/060,399, filed on Oct. tion PCT/US2015.053971 mailed Dec. 22, 2015, 10 pages. 6, 2014, provisional application No. 62/128,432, filed Hance et al., Quantification of chicory root bitterness by an ELISA on Mar. 4, 2015, provisional application No. 2007)for 11B, 13-dihydrolactucin': Food Chemistry, 105: 742-748 (Jan. 62/188,349, filed on Jul. 2, 2015. Mona et al.; "Chemical and Technological Studies on Chicory (Cichorium Initybus L) and Its Applications in Some Functional (51) Int. Cl. Food”; J. Adv. Agric. Res., 14(3): 735-756 (2009). A2.3L. I./22 (2006.01) PCT International Search Report and Written Opinion issued in A2ID 2/36 (2006.01) Application No. PCT/US16/55581 dated Dec. 16, 2016. A2ID I3/06 (2017.01) A2.3L 7/109 (2016.01) * cited by examiner A2.3L 9/00 (2016.01) (52) CPCU.S. Cl............. A23L 1/2121 (2013.01); A2ID 2/366 Primary Examiner Jyoti Chawla (2013.01); A2ID 13/06 (2013.01); A23L 7/109 (74) Attorney, Agent, or Firm — Foley & Lardner LLP (2016.08); A23L 19/01 (2016.08); A23L 19/03 (2016.08) (58) Field of Classification Search (57) ABSTRACT CPC ...... A23L 1/0528: A23L 1/308: A23L 1/2128; The present invention provides a food product comprising at A23L 1/164: A23L 1/2121: A23L 1/2123; least 1.5%. 5%, 10%, 20%, 30%, or more, by weight total A23K 10/30; A23K 1/14: A21D 2/36; ingredients of a low bitter chicory plant material or flour. A21D 13/08: A21D 2/366; A23D 7/0053; The present invention also provides a method for obtaining A23D 7/O15 a chicory product with reduced bitterness, comprising USPC ....... 426/243,518, 549, 557, 590, 594, 615, blanching chicory roots or root chips, drying the blanched 426/648, 661 chicory root chips, and optionally grinding the dried chicory See application file for complete search history. root chips and incorporating it into flour, dough, or other food products. Also provided is a method for obtaining a (56) References Cited chicory taproot with reduced bitterness, comprising culti U.S. PATENT DOCUMENTS Vating a chicory plant at a soil nitrogen level of 150 lbs per acre or less in the upper 3 feet of the soil. 2,161,511 A * 6/1939 Freud1 ....................... A23F 5/44 426,461 4,613,377 A 9, 1986 Yamazaki et al. 10 Claims, 12 Drawing Sheets U.S. Patent Jul. 11, 2017 Sheet 1 of 12 US 9,700,070 B2 FIGURE U.S. Patent Jul. 11, 2017 Sheet 2 of 12 US 9,700,070 B2 FIGURE 2 U.S. Patent Jul. 11, 2017 Sheet 3 of 12 US 9,700,070 B2 FIGURE 3 U.S. Patent Jul. 11, 2017 Sheet 4 of 12 US 9,700,070 B2 FGURE 4 U.S. Patent Jul. 11, 2017 Sheet S of 12 US 9,700,070 B2 Figure 5 TABLE 8 - Sesquiterperse actose Profile U.S. Patent Jul. 11, 2017 Sheet 6 of 12 US 9,700,070 B2 Gr. 6 ------------------------------s SewisNutrition Six: ; cox:k:se 2:Facts &xis: 8 sits Sociis (ing at: 3rbatiyirate 3: U.S. Patent Jul. 11, 2017 Sheet 7 of 12 US 9,700,070 B2 FIGURE 7A Nutrition Facts S8iving S28 -0g: Servigs & Corsaire FIGURE 7B ServingNutrition Size #2 sup {Sig Facts &; wings -er containe: 88out 8 &xister Saswig es for Fats: stay visis : otes at 3.5g % Saturata F3; 3g 6% U.S. Patent Jul. 11, 2017 Sheet 8 of 12 US 9,700,070 B2 FGURE 7 Nutrition Facts $8w:38;x& 83 g; S&wigs & container U.S. Patent Jul. 11, 2017 Sheet 9 of 12 US 9,700,070 B2 FGRE8 Nutritic Facts $38:a::: *a:S fists fates {choicesteroi 38g sodian sing otsi Crioscirate 33g stay is is U.S. Patent Jul. 11, 2017 Sheet 10 of 12 US 9,700,070 B2 GRE 9 Nutrition Facts Ss:ying Size: {3}} &saxx: 8 Sery Caicrisis {: (a?osies from F3t is : iota Fat &g Satsats: as: {g is as $3t {g iota Carichykirate 28s: 8:3882s roteit's 2g y:::::::: & 83% 3i: Caician 2% ... rer 2% U.S. Patent Jul. 11, 2017 Sheet 11 of 12 US 9,700,070 B2 FGURE O Nutrition Facts Sewing Size: text:3: $8g: 83 c : S 3: catories train at 23 : xxis six : s s :38: $88.88: 3.8x883: U.S. Patent Jul. 11, 2017 Sheet 12 of 12 US 9,700,070 B2 FGURE *::::::: *&g taxsters; 38 $xis isos isia essayirate2. 38tay $8; 38 US 9,700,070 B2 1. 2 LOW BITTER CHCORY PRODUCTS significantly more expensive than cellulose fibers. Hence, there is a need in the art for an economic process for CROSS REFERENCE TO RELATED producing low bitter chicory products (e.g., inulin-contain APPLICATIONS ing flour or dough) that avoids the costly steps of inulin extraction from the taproot and the separation thereof from This application claims priority to U.S. Provisional Appli bitter compounds. cation No. 62/060,399, filed on Oct. 6, 2014, U.S. Provi sional Application No. 62/128,432, filed on Mar. 4, 2015, SUMMARY OF THE INVENTION and U.S. Provisional Application No. 62/188,349, filed on Jul. 2, 2015, the contents of which are all incorporated 10 The present application answers the aforementioned need herein by reference in their entirety. by providing low bitter chicory flour and low bitter chicory products that are enriched in inulin and tasty to consumers. FIELD OF INVENTION Thus, one aspect of the invention relates to a low bitter chicory flour, food products comprising the low bitter The present disclosure relates to low bitter chicory chips, 15 chicory flour, and animal feed comprising the low bitter flour and products made from low bitter chicory chips and chicory flour. Examples of food products comprising the low flour, including but not limited to, food products such as bitter chicory flour include, but are not limited to, dairy dough, health bars, cereals, yogurt, pastries, and the like, as products, yoghurts, ice creams, milk-based drinks, milk well as pet food and animal feed. The present disclosure also based garnishes, puddings, milkshakes, egg custard, relates to methods for processing chicory plant taproots to cheeses, nutrition bars, energy bars, breakfast bars, confec produce low bitter chicory chips and flour, as well as tionery, bakery products, crackers, cookies, biscuits, cereal methods for producing chicory taproots with low bitterness. chips, Snack products, ice tea, fruit juice, diet drinks, Sodas, sports drinks, powdered drink mixtures for dietary Supple BACKGROUND mentation, infant and baby food, calcium-Supplemented 25 orange juice, bread, croissants, breakfast cereals, pasta, Fructan is a polydisperse fructose polymer. Biosynthesis noodles, spreads, Sugar-free biscuits and chocolates, calcium of fructan uses Sucrose as the starter molecule to which chews, meat products, mayonnaise, Salad dressings, nut fructosyl units, obtained from Sucrose, are added during the butter, sauces and Soups. Animal feed comprises, but is not elongation process. Bacterial fructan typically has a very limited to, dog food, cat food, bird feed, cow feed, reptile high degree of polymerization (DP) which can reach as 30 food, rodent food and the like. many as 100,000 fructose units. In plants, the DP generally In one aspect of the invention, the chicory plants are does not exceed 100. cultivated at a soil nitrogen level of 150 libs per acre or less Fructan with B(2-1) glycosidic linkages is called inulin. in the upper three feet of the soil. In another aspect of the Inulin can result from the elongation of the fructan chain invention, the chicory plants are cultivated at a soil nitrogen starting from the C1 of the fructose moiety of the initial 35 level of 100 libs per acre. In yet another aspect of the Sucrose. Alternatively, inulin can result from the elongation invention, the chicory plants are cultivated at a soil nitrogen form the C1 of the fructose moiety as well as from the C6 level of 50 libs per acre.