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Pt. 185 40 CFR Ch. I (7–1–98 Edition)

peaches, pears, strawberries, and toma- 185.3550 Hexakis. toes. This temporary exemption from 185.3575 Hexazinone. the requirement for a tolerance will 185.3600 Hydrogen cyanide. 185.3650 Imazalil. permit the marketing of the food com- 185.3700 Inorganic bromide. modities in this paragraph when treat- 185.3750 Iprodione. ed in accordance with the provisions of 185.3775 d-. experimental use permit 70515-EUP-1, 185.3800 Magnesium phosphide. which is being issued under the Federal 185.4000 Metalaxyl. , Fungicide, and Rodenticide 185.4035 Metarhizium anisopliae strain Act (FIFRA), as amended (7 U.S.C. 136). ESF1. 185.4100 . This temporary exemption from the re- 185.4150 . quirement of a tolerance expires and is 185.4250 Methyl chloride. revoked on June 1, 2001. This tem- 185.4300 Methyl formate. porary exemption from the require- 185.4400 Nitrogen. ment of a tolerance may be revoked at 185.4500 N-Octylbicycloheptene any time if the experimental use per- dicarboximide. 185.4650 Paraformaldehyde. mit is revoked or if any experience 185.4800 Phosalone. with or scientific data on this pesticide 185.4850 Picloram. indicate that the tolerance is not safe. 185.4900 Piperonyl butoxide. 185.4950 Pirimiphos-methyl. [63 FR 32134, June 12, 1998] 185.5000 Propargite. 185.5100 Propetamphos. PART 185—TOLERANCES FOR 185.5150 Propylene oxide. PESTICIDES IN FOOD 185.5200 . 185.5375 Sulfonium, trimethyl-salt with N- (phosphonomethyl)glycine (1:1). Subpart A [Reserved] 185.5950 Triforine. 185.6300 Zinc ion and maneb coordination Subpart B—Food Additives Permitted in product. Food for Human Consumption Sec. Subpart C—Food Additives Resulting From 185.150 . Contact With Containers or Equipment 185.200 Aluminum phosphide. and Food Additives Otherwise Affect- 185.250 4-Amino-6-(1,1-dimethylethyl)-3- ing Food (methylthio)-1,2,4-triazin-5(4H)-one. 185.650 Carbon dioxide. 185.7000 . 185.1000 . AUTHORITY: 21 U.S.C. 346a and 348. 185.1050 Chlorpyrifos-methyl. 185.1150 Combustion product gas. SOURCE: 40 FR 14156, Mar. 28, 1975, unless 185.1200 Copper. otherwise noted. Redesignated at 41 FR 26568, 185.1350 Cyhexatin. June 28, 1976, and 53 FR 24667, June 29, 1988. 185.1500 Dalapon. EDITORIAL NOTE: The text of part 185 set 185.1650 . forth below was transferred and recodified at 185.1700 Diatomaceous earth. 53 FR 24666, June 29, 1988. New part 185 for- 185.1800 Dicamba. merly appeared in 21 CFR part 193. A Redes- 185.1900 2,2-Dichlorovinyl dimethyl phos- ignation Table appears in the Finding Aids phate. section of this volume. 185.2200 O,O-Dimethyl O-(4-nitro-m-tolyl) phosphorothioate. 185.2250 Dimethyl phosphate of 3-hydroxy- Subpart A [Reserved] N-methyl-cis-crotonamide. 185.2500 Diquat. Subpart B—Food Additives Per- 185.2600 . 185.2700 Ethephon. mitted in Food for Human 185.2850 Ethylene oxide. Consumption 185.2950 Ethyl 3-methyl-4- (methylthio)phenyl (1-methylethyl)- § 185.150 Aldicarb. phosphoramidate. (a) A regulation is established per- 185.3000 O-Ethyl O-[4-(methylthio)phenyl] S- mitting the combined residues of the propyl phosphorodithioate. 185.3250 Fluazifop-butyl. insecticide/nematocide aldicarb 2- 185.3385 Flutolanil (N-(3-(1- methyl-2-(methylthio)propionaldehyde methylethoxy)phenyl)-2- O-(methylcarbamoyl)oxime and its (trifluoromethyl)benzamide). cholinesterase-inhibiting metabolites

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2-methyl-2-(methylsulfonyl) propion- Food Parts per aldehyde O-(methylcarbamoyl)oxime million and 2-methyl-2-(methyl- Wheat milled fractions (except flour) ...... 3 sulfonyl)propionaldehyde O-(methyl- carbamoyl)oxime in or on the commod- [44 FR 40283, July 10, 1979. Redesignated at 53 ity sorghum bran at 0.5 part per mil- FR 24667, June 29, 1988] lion. (b) [Reserved] § 185.650 Carbon dioxide. [47 FR 14894, Apr. 7, 1982, as amended at 53 The food additive carbon dioxide may FR 8874, Mar. 18, 1988. Redesignated at 53 FR be safely used after harvest in modified 24667, June 29, 1988] atmospheres for stored product insect control on all processed agricultural § 185.200 Aluminum phosphide. commodities. The food additive aluminum phosphide may be safely used in ac- [46 FR 32866, June 25, 1981. Redesignated at 53 FR 24667, June 29, 1988] cordance with the following prescribed conditions: § 185.1000 Chlorpyrifos. (a) It is used to generate phosphine in the fumigation of processed foods. (a) Tolerances are established for the (b) To assure safe use of the additive, combined residues of the insecticide it is used in compliance with label and chlorpyrifos [O,O- diethyl O-(3,5,6- labeling conforming to that registered trichloro-2-pyridyl) phosphorothioate] with the U.S. Environmental Protec- and its metabolite 3,5,6-trichloro-2- tion Agency. Labeling shall bear a pyridinol resulting from application of warning to aerate the finished food for the insecticide to growing crops as fol- 48 hours before it is offered to the con- lows: sumer. A further warning shall state Parts per that under no condition should the for- Foods million mulation containing aluminum Citrus oil ...... 25.0 phosphide be used so that it or its Corn oil ...... 3.0 unreacted residues will come in con- tact with any processed food, except (b) The additive chlorpyrifos [O,O- processed brewer’s rice, malt, and corn diethyl O-(3,5,6-trichloro-2-pyridyl) grits stored in breweries for use in the phosphorothioate] may be safely used manufacture of beer. in accordance with the following pre- (c) Residues of phosphine in or on scribed conditions. processed foods do not exceed 0.01 part (1) Application shall be limited solely per million. to spot and/or crack and crevice treat- [40 FR 14156, Mar. 28, 1975. Redesignated at 41 ment in food handling establishments FR 26568, June 28, 1976, and amended at 44 FR where food and food products are held, 35210, June 19, 1979. Redesignated at 53 FR processed, prepared or served. Contami- 24667, June 29, 1988] nation of food or food contact surfaces shall be avoided. Food must be re- § 185.250 4-Amino-6-(1,1- moved or covered during treatment. dimethylethyl)-3-(methylthio)-1,2,4- (2) Spray concentration for spot triazin-5(4H)-one. treatment shall be limited to a maxi- Tolerances are established for com- mum of 0.5 percent of the active ingre- bined residues of the herbicide 4- dient by weight. A course, low-pressure amino-6-(1,1-dimethylethyl)-3-(methyl- spray shall be used to avoid atomiza- thio)-1,2,4-triazin-5(4H)-one and its tri- tion or splashing of the spray. azinone metabolites in or on the fol- (3) Paint-on application for spot lowing processed foods when present treatment shall be limited to a maxi- therein as a result of application of mum of 2 percent of the active ingredi- this herbicide to growing crops: ent by weight. (4) Crack and crevice treatment shall Parts per Food million be limited to a maximum of 2 percent of the active ingredient by weight. Barley, milled fractions (except flour) ...... 3 Potatoes, processed (inc. potato chips) ...... 3 Equipment capable of delivering a pin- Sugarcane molasses ...... 2 stream of insecticide shall be used.

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(5) Application via adhesive strips application of the insecticide to grow- shall contain a maximum of 10% by ing crops as follows: weight of the controlled-release prod- Parts per uct in food-handling establishments Foods million where food and food products are held, processed, prepared, or served. A maxi- Milling fractions (except flour) of wheat ...... 1.5 Mint oil ...... 8 mum of 36 strips (or 5.15 grams of Peanut oil ...... 0.4 chlorpyrifos) is to be used per 100 square feet of floor space. The strips [47 FR 30478, July 14, 1982, as amended at 53 are not to be placed in exposed areas FR 9434, Mar. 23, 1988. Redesignated at 53 FR where direct contact with food, uten- 24667, June 29, 1988; 57 FR 10293, Mar. 25, 1992; sils, and food-contact surfaces would be 58 FR 19356, Apr. 14, 1993] likely to occur. (6) To assure safe use of the insecti- § 185.1050 Chlorpyrifos-methyl. cide, its label and labeling shall con- Tolerances are established for the form to that registered by the U.S. En- combined residues of the insecticide vironmental Protection Agency, and it chlorpyrifos-methyl (O,-O- dimethyl-O- shall be used in accordance with such (3,5,6-trichloro-2-pyridyl) phos- label and labeling. phorothioate and its metabolite (3,5,6- (c) A tolerance of 0.1 part per million trichloro-2-pyridinol) in or on the fol- is established for residues of lowing processed feeds when present chlorpyrifos, per se, in or on all food therein as a result of application to items (other than those already cov- stored grains: ered by a higher tolerance as a result of use on growing crops) in food service Parts per Food million establishments where food and food products are prepared and served, as a Barley milling fractions (except flour) ...... 90 Oats milling fractions (except flour) ...... 130 result of the application of chlorpyrifos Sorghum milling fractions (except flour) ...... 90 in microencapsulated form. Rice milling fractions (except flour) ...... 30 (1) Application of a microencap- Wheat milling fractions (except flour) ...... 30 sulated product shall be limited solely to spot and/or crack and crevice treat- [50 FR 26682, June 27, 1985. Redesignated at 53 ment in food handling establishments FR 24667, June 29, 1988] where food and food products are pre- pared and served. All treatments shall § 185.1150 Combustion product gas. be applied in such a manner as to avoid The food additive combustion prod- contamination of food or food contact uct gas may be safely used after har- surfaces. vest in modified atmospheres for stored (2) Spray concentrations shall be lim- product insect control on all processed ited to a maximum of 0.5 percent of the agricultural commodities (except fresh active ingredient by weight. meat) with the following prescribed (3) For crack and crevice treatment, conditions: equipment capable of delivering a pin (a) The combustion product gas is stream of spray directly into cracks produced by the controlled combustion and crevices or capable of applying in air of butane, propane, or natural small amounts of insecticide into gas. The combustion equipment shall cracks and crevices shall be used. be provided with an absorption type fil- (4) For spot treatment, an individual ter capable of removing possible toxic spot shall not exceed 2 square feet. impurities through which all gas used (5) To assure safe use of the insecti- in the treatment of food shall pass and cide, its label and labeling shall con- with suitable controls to insure that form to that registered by the U.S. En- any combustion products failing to vironmental Protection Agency, and it meet the specifications provided will shall be used in accordance with such be prevented from reaching the food label and labeling. being treated. (d) Tolerances are established for res- (b) The insecticide meets the follow- idues of the insecticide chlorpyrifos ing specifications: [O,O-diethyl O-(3,5,6-trichloro-2-pyri- (1) Carbon monoxide content not to dyl) phosphorothioate] resulting from exceed 4.5 percent by volume.

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(2) It is used or intended for use to diethyl phosphorothioate) in or on rai- displace or remove oxygen in the stor- sins from application of the insecticide age of food, except fresh meat. to the growing raw agricultural com- [46 FR 32866, June 25, 1981. Redesignated at 53 modity grapes. FR 24667, June 29, 1988] § 185.1700 Diatomaceous earth. § 185.1200 Copper. The food additive diatomaceous A tolerance of 1 part per million is earth may be safely used in accordance established in potable water for resi- with the following conditions. Applica- dues of copper resulting from the use of tion shall be limited solely to spot and/ the algicides or herbicides basic copper or crack and crevice treatments in food carbonate (malachite), copper sulfate, processing and food storage areas in ac- copper monoethanolamine, and copper cordance with the prescribed condi- triethanolamine to control aquatic tions: plants in reservoirs, lakes, ponds, irri- (a) It is used or intended for use for gation ditches, and other potential control of insects in food processing sources of potable water. and food storage areas: Provided, That [45 FR 53459, Aug. 12, 1980. Redesignated at 53 the food is removed or covered prior to FR 24667, June 29, 1988] such use. (b) To assure safe use of the insecti- § 185.1350 Cyhexatin. cide, its label and labeling shall con- Tolerances are established for com- form to that registered by the U.S. En- bined residues of the insecticide vironmental Protection Agency, and it cyhexatin (tricyclohexyl- shall be used in accordance with such hydroxystannane; CAS Reg. No. 13121– label and labeling. 70–5) and its organotin metabolites [46 FR 55511, Nov. 10, 1981. Redesignated at 53 (calculated as cyhexatin) in or on the FR 24667, June 29, 1988] following processed foods when present therein as a result of application of § 185.1800 Dicamba. this insecticide to the growing crops: Tolerances are established for the Food Parts per combined residues of the herbicide million dicamba (3,6-dichloro-o-anisic acid) and Hops, dried ...... 90 its metabolite 3,6-dichloro-5-hydroxy-o- Prunes, dried ...... 4 anisic acid in or on the following proc- essed foods when present therein as a [53 FR 23389, June 22, 1988. Redesignated at 53 result of application of this herbicide FR 24667, June 29, 1988] to growing crops.

§ 185.1500 Dalapon. Parts per Food million A tolerance of 0.2 part per million is established for residues of the herbi- Sugarcane molasses ...... 2.0 cide dalapon (2,2-dichloropropionic acid) in potable water when present [48 FR 11114, Mar. 16, 1983. Redesignated at 53 therein as a result of the application of FR 24667, June 29, 1988] dalapon sodium-magnesium salt mix- tures to irrigation ditch banks in the § 185.1900 2,2-Dichlorovinyl dimethyl western United States. phosphate. [43 FR 22345, May 25, 1978. Redesignated at 53 The food additive 2,2-dichlorovinyl FR 24667, June 29, 1988] dimethyl phosphate may be present as a residue from application as an insec- § 185.1650 Dialifor. ticide on packaged or bagged non- A tolerance of 2 parts per million is perishable processed food (see: 21 CFR established for combined residues of 170.3(j)) in an amount in such food not the insecticide dialifor (S-(2-chloro-1- in excess of 0.5 part per million (ppm). phthalimidoethyl) O,O-diethyl phos- To assure safe use of the insecticide, phorodithioate) and its oxygen analog its label and labeling shall conform to S-(2-chloro-1-phthalimidoethyl O,O- the label and labeling registered by the

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U.S. Environmental Protection Agen- under their direct control will make cy, and the usage employed shall con- certain that the treated water will not form with such label or labeling. be used for animal consumption, swim- ming, spraying, domestic purposes, or [56 FR 29183, June 26, 1991] for irrigation for 14 days post-treat- § 185.2200 O,O-Dimethyl O-(4-nitro-m- ment or until approved analysis shows tolyl) phosphorothioate. that the water does not contain more than 0.01 ppm of diquat (calculated as (a) A tolerance of 30 parts per mil- the cation) and that no treatment will lion, of which no more than 15 parts be made where commercial processing per million is O,O-dimethyl O-(4-nitro- of fish resulting in the production of m-tolyl) phosphorothioate or O,O-di- fish protein concentrate or fish meal is methyl O-(4-nitro-m-tolyl) phosphate, practiced. is established for combined residues of (b) A tolerance of 0.01 ppm is estab- the insecticide O,O-dimethyl O-(4- lished for residues of the herbicide nitro-m-tolyl) phosphorothioate and its diquat (6,7-dihydrodipyrido (1,2-a:2′,1′-c) metabolites O,O-dimethyl O-(4-nitro-m- pyrazinediium) (calculated as the tolyl) phosphate and 3-methyl-4- cation) derived from application of the nitrophenol in wheat gluten resulting dibromide salt in potable water result- from postharvest application of the in- ing from the application of the pes- secticide to stored wheat in Australia. ticide in ponds, lakes, and drainage (b) [Reserved] ditches where there is little or no out- [44 FR 40282, July 10, 1979, as amended at 53 flow of water and which are totally FR 8874, Mar. 18, 1988. Redesignated at 53 FR under control of the user. The applica- 24667, June 29, 1988] tor will make certain that treated water will not be used for animal con- § 185.2250 Dimethyl phosphate of 3-hy- sumption, swimming, spraying, irriga- droxy-N-methyl-cis-crotonamide. tion, or domestic purposes for 14 days A tolerance of 2 parts per million is post-treatment. For the purposes of established for residues of the insecti- this paragraph only (§ 185.2500(b)) these cide dimethyl phosphate of 3-hydroxy- applications of diquat are not to be N-methyl-cis-crotonamide in con- used in aquatic sites in Florida. centrated tomato products when (c) A food additive regulation of 0.5 present therein as a result of applica- part per million is established for resi- tion of the insecticide to growing to- dues of diquat in processed potatoes matoes. (includes potato chips). (Sec. 409(c) (1) & (4), Federal Food, Drug, and [46 FR 30339, June 8, 1981, and 47 FR 8007, Feb. Cosmetic Act (21 U.S.C. 348(c) (1) & (4)), 24, 1982. Redesignated and amended at 53 FR transferred to the Administrator EPA in Re- 24666, 24668, June 29, 1988; 55 FR 26440, June organization Plan No. 3 of 1970 (35 FR 15623)) 28, 1990] [40 FR 18168, Apr. 25, 1975. Redesignated at 41 FR 26568, June 28, 1976. Redesignated at 53 § 185.2600 Endosulfan. FR 24667, June 29, 1988] A tolerance of 24 parts per million is established for combined residues of § 185.2500 Diquat. the insecticide endosulfan (6,7,8,9,10,10- (a) A tolerance of 0.01 ppm is estab- hexachloro-1,5,5a,6,9,9a-hexahydro-6,9- lished for residues of the herbicide methano-2,4,3-benzodioxathiepin-3- diquat (6,7-dihydrodipyrido (1,2-a:2′,1′-c) oxide) and its metabolite endosulfan pyrazidiinium) derived from applica- sulfate (6,7,8,9,10,10-hexachloro- tion of the dibromide salt in potable 1,5,5a,6,9,9a-hexahydro-6,9-methano- water resulting from the application of 2,4,3-benzodioxathiepin-3,3-dioxide) in the pesticide for control of aquatic or on dried tea (reflecting less than 0.1 weeds in ponds, lakes, reservoirs, part per million residues in beverage marshes, bayous, drainage ditches, ca- tea) resulting from application of the nals, streams, and rivers which are insecticide to growing tea. slow-moving or quiescent in programs of the Corps of Engineers or other Fed- § 185.2700 Ethephon. eral or State public agencies. These A food additive regulation is estab- agencies or contractors or licensees lished permitting residues of the plant

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growth regulator ethephon [(2- (1-methylethyl)-phosphoramidate and chloroethyl) phosphonic acid] in or on its cholinesterase-inhibiting metabo- the following food commodities: lites ethyl 3-methyl-4-(methyl- sulfinyl)phenyl (1-methylethyl)-phos- Parts per Food million phoramidate and ethyl 3-methyl-4- (methylsulfonyl)-phenyl (1-methyl- Barley, milling fractions, except flour ...... 5.0 ethyl) phosphoramidate in or on the Sugarcane, molasses ...... 1.5 Wheat, milling fractions, except flour ...... 5.0 following food commodities:

Food Parts per [47 FR 20763, June 23, 1982, as amended at 50 million FR 14097, Apr. 10, 1985; 51 FR 31325, Sept. 3, 1986; 53 FR 5367, Feb. 24, 1988. Redesignated Citrus oil ...... 25.0 Raisins ...... 0.3 at 53 FR 24667, June 29, 1988; 60 FR 32097, June 19, 1995] [48 FR 29839, June 29, 1983. Redesignated at 53 § 185.2850 Ethylene oxide. FR 24667, June 29, 1988] Ethylene oxide may be safely used as a fumigant for the control of micro- § 185.3000 O-Ethyl O-[4-(methylthio) phenyl] S-propyl phosphorodithio- organisms and insect infestation in ate. ground spices and other processed nat- ural seasoning materials, except mix- A tolerance of 1 part per million is tures to which salt has been added, in established for residues of the insecti- accordance with the following pre- cide O-ethyl O-[4-(methylthio)- phenyl] scribed conditions: S-propyl phosphorodithioate and its (a) Ethylene oxide, either alone or cholinesterase-inhibiting metabolites admixed with carbon dioxide or dichlo- in cottonseed oil resulting from appli- rodifluoromethane, shall be used in cation of the pesticide to growing cot- amounts not to exceed that required to ton. accomplish the intended technical ef- [43 FR 32130, July 25, 1978. Redesignated at 53 fects. If used with dichlorodifluoro- FR 24667, June 29, 1988] methane, the dichlorodifluoromethane shall conform with the requirements § 185.3250 Fluazifop-butyl. prescribed by 21 CFR 173.355 of this Tolerances are established for resi- chapter. dues of (±)-2-[4-[[5-(trifluoromethyl)-2- (b) To assure safe use of the additive, pyridinyl]oxy]phenoxy]propanoic acid its label and labeling shall conform to (fluazifop), both free and conjugated, that registered with the U.S. Environ- and of (±)-butyl 2[4-[[5-(trifluoro- mental Protection Agency and it shall methyl)-2-pyr- be used in accordance with such label idinyl]oxy]phenoxy]propanoate or labeling. (fluazifop-butyl), all expressed as (c) Residues of ethylene oxide in fluazifop, in or on the following foods: ground spices from both postharvest application to the raw agricultural Food Parts per commodity whole spices and applica- million tion to the ground spices shall not ex- Cottonseed, oil ...... 0.2 ceed the established tolerance of 50 Soybean, oil ...... 2.0 parts per million for residues in whole spices in 40 CFR 180.151. [48 FR 19023, Apr. 27, 1983. Redesignated at 53 FR 24667, June 29, 1988] [40 FR 14156, Mar. 28, 1975. Redesignated at 41 FR 26568, June 28, 1976, and amended at 50 FR 2958, Jan. 23, 1985. Redesignated and amended § 185.3385 Flutolanil (N-(3-(1- at 53 FR 24666, 24668, June 29, 1988] methylethoxy)phenyl)-2- (trifluoromethyl)benzamide). § 185.2950 Ethyl 3-methyl-4- (a) A food additive regulation is es- (methylthio)phenyl (1-methylethyl)- tablished permitting the combined res- phosphoramidate. idues of the insecticide flutolanil, N-(3- Tolerances are established for the (1-methylethoxy)phenyl)-2- combined residues of the nematocide (trifluoromethyl)benzamide, and its ethyl 3-methyl-4-(methylthio)phenyl metabolites converted to 2-

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(trifluoromethyl) benzoic acid and cal- § 185.3600 Hydrogen cyanide. culated as flutolanil in or on the fol- The food additive hydrogen cyanide lowing processed food commodity: may be present as a residue in certain Parts per processed foods in accordance with the Commodity million following prescribed conditions: (a) The food additive is present as a Peanut meal ...... 1.0 result of its use as a fumigant. (b) The residues of hydrogen cyanide (b) A time-limited food additive regu- shall not exceed the following levels: lation is established permitting the (1) 125 parts per million in cereal combined residues of the fungicide flours. flutolanil N-(3-(1- (2) 90 parts per million in cereals that methylethoxy)phenyl)-2- are cooked before being eaten. (trifluoromethyl)benzamide and its me- (3) 50 parts per million in uncooked tabolites converted to 2- ham, bacon, and sausage. (trifluoromethyl) benzoic acid and cal- (4) 200 parts per million in cocoa. culated as flutolanil in or on the fol- (c) Where tolerances are established lowing raw processed food commodity: under both sections 408 and 409 of the Act on the raw agricultural commodity Commodities Parts per Expiration date and on the processed food, respectively, million the total residues of hydrogen cyanide Rice, hull ...... 7.0 April 30, 1998 in or on the processed food shall not be Rice, bran ...... 3.0 Do. greater than that designated in para- graph (b) of this section. [60 FR 42458, Aug. 16, 1995, as amended at 61 (d) To assure safe use of the additive, FR 33044, June 26, 1996] the label and labeling of the pesticide formulation containing the food addi- § 185.3550 Hexakis. tive shall conform to the label and la- beling registered by the U.S. Environ- A regulation is established permit- mental Protection Agency. ting the combined residues of the in- secticide hexakis (2-methyl-2-phenyl- § 185.3650 Imazalil. propyl) distannoxane and its organotin Tolerances are established for the metabolites calculated as hexakis (2- combined residues of the fungicide methyl-2-phenylpropyl) distannoxane imazalil 1-[2-(2,4-dichlorophenyl)-2-(2- in or on the following food items: propenyloxy)ethyl]-1H-imidazole and [47 FR 21532, May 19, 1982, as amended at 48 its metabolite 1-(2,4-dichlorophenyl)-2- FR 37204, Aug. 17, 1983; 48 FR 39058, Aug. 29, (1H- imidazole-1-yl)-1-ethanol in or on 1983. Redesignated at 53 FR 24667, June 29, the following food commodity: 1988; 59 FR 5109, Feb. 3, 1994] Parts per Food million § 185.3575 Hexazinone. Citrus oil ...... 25.0 A food additive tolerance with re- gional registration, as defined in § 180.1(n) and which excludes use of [48 FR 28433, June 22, 1983. Redesignated at 53 FR 24667, June 29, 1988] hexazinone on sugarcane in Florida, is established for combined residues of § 185.3700 Inorganic bromide. the herbicide hexazinone (3-cyclohexyl- The food additive inorganic bromide 6-(dimethylamino)-1-methyl-1,3,5-tri- may be present as a residue in certain azine-2,4(1H,3H)-dione) and its metabo- processed foods in accordance with the lites (calculated as hexazinone) in or following conditions: on the following food commodity: (a) When the food additive is present as a result of fumigation of the proc- Parts per Commodity million essed food with methyl bromide or from such fumigation in addition to Sugarcane, molasses ...... 5.0 the authorized use of methyl bromide on the source raw agricultural com- [60 FR 42462, Aug. 16, 1995] modity, as provided for in 40 CFR part

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180, the total residues of inorganic bro- § 185.3775 d-Limonene. mides (calculated as Br) shall not ex- The food additive d-limonene may be ceed the following levels: safely used in accordance with the fol- 400 parts per million in or on dried eggs and lowing conditions: processed herbs and spices. (a) It is used with the active ingredi- 325 parts per million in or on parmesan ents dihydro-5-pentyl-2(3H)-furanone cheese and roquefort cheese. and dihydro-5-heptyl-2(3H)-furanone in 250 parts per million in or on concentrated insect-repellent tablecloths and in in- tomato products and dried figs. sect-repellent strips used in food-han- 125 parts per million in or on processed foods other than those listed above. dling establishments. (b) To assure safe use of the insecti- (b) [Reserved] cide, its label and labeling shall con- (c) When the food additive is present form to that registered by the U.S. En- in fermented malt beverages in accord- vironmental Protection Agency, and it ance with §§ 185.3480 and/or 21 CFR shall be used in accordance with such 172.730(a)(2) of this chapter, the amount label and labeling. shall not exceed 25 parts per million (calculated as Br). [60 FR 16053, Mar. 29, 1995] (d)–(v) [Reserved] § 185.3800 Magnesium phosphide. (w) Where tolerances are established under sections 408 and 409 of the The food additive magnesium FFDCA on both the raw agricultural phosphide may be safely used in ac- commodities and processed foods made cordance with the following prescribed therefrom, the total residues of inor- conditions: ganic bromides in or on the processed (a) It is used to generate phosphine in food shall not be greater than those the fumigation of processed foods. designated in paragraphs (a) of this (b) To assure safe use of the additive, section, unless a higher level is estab- it is used in compliance with the label lished elsewhere in this part or in part and labeling conforming to that reg- 180. istered with the U.S. Environmental Protection Agency. The labeling shall [40 FR 14156, Mar. 28, 1975. Redesignated at 41 FR 26568, June 28, 1976, and amended at 49 FR bear a warning to aerate the finished 17149, Apr. 23, 1984; 50 FR 2958, Jan. 23, 1985; food for 48 hours before it is offered to 50 FR 3755, Jan. 28, 1985. Redesignated and the consumer. A further warning shall amended at 53 FR 24666, 24668, June 29, 1988; state that under no condition should 53 FR 52709, Dec. 29, 1988] the formulation containing magnesium phosphide be used so that it or its § 185.3750 Iprodione. unreacted residues will come in con- Tolerances are established for the tact with any processed food. combined residues of the fungicide (c) Residues of phosphine in or on iprodione [3-(3,5-dichlorophenyl)-N-(1- processed foods do not exceed 0.01 part methylethyl)-2,4-dioxo-1-imidazolidine- per million. carboxamide], its isomer [3-(1-methyl- ethyl)-N-(3,5-dichlorophenyl)-2,4-dioxo- [43 FR 56040, Nov. 30, 1978. Redesignated at 53 FR 24667, June 29, 1988] 1-imidazolidinecarboxamide], and its metabolite [3-(3,5-dichlorophenyl)-2,4- § 185.4000 Metalaxyl. dioxo-1-imidazolidinecarboxamide in or on the following food commodity: (a) A regulation is established per- mitting the combined residues of the Food Parts per fungicide metalaxyl [N-(2,6-dimethyl- million phenyl)-N-(methoxyacetyl) alanine Ginseng, dried ...... 4.0 methyl ester] and its metabolites con- Raisins ...... 300 taining the 2,6-dimethylaniline moiety, and N-(2-hydroxy methyl-6-methyl)-N- [50 FR 4208, Jan. 30, 1985, as amended at 52 methoxyacetyl)-alanine methylester, FR 10562, Apr. 2, 1987. Redesignated at 53 FR each expressed as metalaxyl, in or on 24667, June 29, 1988] the following food commodities:

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food-handling establishments, includ- Food Parts per million ing food service, manufacturing, and Apricots (dried) ...... 4.0 processing establishments such as res- Citrus, oil ...... 7.0 taurants, cafeterias, supermarkets, Potatoes, processed (including potato chips) ..... 4.0 bakeries, breweries, dairies, meat- Prunes (dried) ...... 4.0 Raisins ...... 6.0 slaughtering and packing plants, and Tomatoes, processed ...... 3.0 canneries where food and food products are held, processed, and served. (b) Indirect or inadvertent tolerances. (b) Application shall be limited sole- Tolerances are established for indirect ly to placement of attractant stations or inadvertent residues of metalaxyl in containing Metarhizium anisopliae the food commodities when present strain ESF1 in food-handling establish- therein as a result of the application of ments. metalaxyl to growing crops listed in 40 (c) To ensure safe use of the micro- CFR 180.408(a) and other non-food crops bial agent, its label and la- as listed below: beling shall conform to that registered Parts per by the U.S. Environmental Protection Food million Agency, and it shall be used in accord- ance with such label and labeling. Barley, milling fractions ...... 1.0 Oat milling fractions ...... 1.0 [58 FR 29121, May 19, 1993] Wheat, milling fractions ...... 1.0 § 185.4100 Methomyl. (c) [Reserved] (d) A food additive regulation is es- A food additive tolerance of 12 parts tablished for residues of the fungicide per million is established for residues metalaxyl, [N-(2,6-dimethylphenyl)-N- of the insecticide methomyl (S-methyl- (methoxyacetyl)alanine methyl ester], N-[(methylcarbomyl) and its metabolites containing the 2,6- oxy]thioacetimidate) in or on the proc- dimethylaniline moiety, and N-(2- essed commodity dried hops as a result hydroxymethyl-6-methylphenyl)-N- of application to the growing hops. (methoxyacetyl) alanine methyl ester, There are no United States registra- each expressed as metalaxyl, in or on tions for use of methomyl on hops, as the following processed foods when of February 14, 1990. present therein as a result of applica- [55 FR 5220, Feb. 14, 1990] tion to growing hops: § 185.4150 Methoprene. Parts per Food million A tolerance of 10 parts per million is Hops, dried ...... 20 established for residues of isopropyl (E,E)-11-methoxy-3,7,11-trimethyl-2,4- dodecadienoate) in or on the food addi- [48 FR 3587, Jan. 26, 1983, as amended at 50 FR 49688, Dec. 4, 1985; 52 FR 41418, Oct. 28, tive commodity cereal grain milled 1987; 52 FR 42760, Nov. 6, 1987; 53 FR 8874, fractions (except flour and rice hulls). Mar. 18, 1988. Redesignated at 53 FR 24667, [60 FR 42460, Aug. 16, 1995] June 29, 1988, and amended at 54 FR 12445, Mar. 27, 1989; 55 FR 14833, Apr. 19, 1990; 55 FR § 185.4250 Methyl chloride. 26440, June 28, 1990; 56 FR 2442, Jan. 23, 1991; 56 FR 65003, Dec. 13, 1991; 58 FR 30123, May 26, The food additive methyl chloride 1993] may be safely used in accordance with the following prescribed conditions: § 185.4035 Metarhizium anisopliae (a) It is used or intended for use as a strain ESF1. propellant in pesticide formulations in A food additive regulation is estab- an amount not to exceed 30 percent of lished allowing the use of the microbial the finished formulation. pest-control agent Metarhizium (b) It is used or intended for use in anisopliae strain ESF1 as follows: food storage and processing areas (a) Metarhizium anisopliae strain whereby spray applications do not con- ESF1 may be present as a residue in tact fatty foods. food items as a result of application of (c) To assure safe use of the additive, Metarhizium anisopliae strain ESF1 in the label and labeling of the pesticide

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formulation containing the food addi- § 185.4650 Paraformaldehyde. tive shall conform to the label and la- The food additive paraformaldehyde beling registered by the U.S. Environ- may be safely used in accordance with mental Protection Agency. the following prescribed conditions. § 185.4300 Methyl formate. (a) It is used to control microbial or fungal growth in maple tree tapholes The food additive methyl formate (b) It is so used that the maple sirup may be safely used in or on specified produced from the sap of treated maple dried fruits in accordance with the fol- trees does not contain in excess of 2 lowing prescribed conditions: parts per million of formaldehyde. (a) It is used or intended for use in or on raisins and dried Zante currants as § 185.4800 Phosalone. a bulk and package fumigant. Tolerances are established for resi- (b) It is used in accordance with di- dues of the insecticide phosalone (S-(6- rections registered with the U.S. Envi- chloro-3-(mercaptomethyl)-2-benzoxa- ronmental Protection Agency, and so zolinone) O,O- diethyl phosphorodithio- used that the total formic acid present, free and combined in the finished prod- ate) in or on the following processed uct shall not exceed 250 parts per mil- foods when present therein as a result lion. of application of the insecticide to the (c) To assure safe use of the additive, growing crops: its label and labeling shall conform to 40 parts per million in or on dried prunes. that registered with the U.S. Environ- 20 parts per million in or on raisins. mental Protection Agency. 8 parts per million in or on dried tea.

§ 185.4400 Nitrogen. § 185.4850 Picloram. The food additive nitrogen may be Tolerances are established for resi- safely used after harvest in modified dues of picloram [4-amino-3,5,6- atmospheres for stored product insect trichloropicolinic acid] resulting from control on all processed agricultural the application of the pesticide to commodities. growing crops in the following:

[46 FR 32866, June 25, 1981. Redesignated at 53 Food Parts per FR 24667, June 29, 1988] million Barley, milled fractions (exc flour) ...... 3 § 185.4500 N-Octylbicycloheptene Oats, milled fractions (exc flour) ...... 3 dicarboximide. Wheat, milled fractions (exc flour) ...... 3 The food additive N- octylbicycloheptene dicarboximide [41 FR 19211, May 11, 1976. Redesignated at 41 may be safely used in accordance with FR 26568, June 28, 1976, and at 53 FR 24667, the following prescribed conditions: June 29, 1988] (a) It is used in combination with piperonyl butoxide and pyrethrins for § 185.4900 Piperonyl butoxide. insect control in food-processing and The food additive piperonyl butoxide food-storage areas, provided that the may be safely used in accordance with food is removed or covered prior to the following prescribed conditions: such use. (a) It is used or intended for use in (b) Residues in food resulting from combination with pyrethrins for con- the use described in paragraph (a) of trol of insects: this section shall not exceed 10 parts (1) In cereal grain mills and in stor- per million of N- octylbicycloheptene age areas for milled cereal grain prod- dicarboximide, 10 parts per million of ucts, whereby the amount of piperonyl piperonyl butoxide, and 1 part per mil- butoxide is at least equal to but not lion of pyrethrins. more than 10 times the amount of (c) To assure safe use of the additive, pyrethrins in the formulation. its label and labeling shall conform to (2) On the outer ply of multiwall that registered with the U.S. Environ- paper bags of 50 pounds or more capac- mental Protection Agency and it shall ity in amounts not exceeding 60 milli- be used in accordance with such label grams per square foot, whereby the and labeling. amount of piperonyl butoxide is equal

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to 10 times the amount of pyrethrins in (d) To assure safe use of the additive, the formulation. Such treated bags are its label and labeling shall conform to to be used only for dried foods. that registered with the U.S. Environ- (3) On cotton bags of 50 pounds or mental Protection Agency, and it shall more capacity in amounts not exceed- be used in accordance with such label ing 55 milligrams per square foot of and labeling. cloth, whereby the amount of piperonyl (e) Where tolerances are established butoxide is equal to 10 times the under sections 408 and 409 of the Act on amount of pyrethrins in the formula- both raw agricultural commodities and tion. Such treated bags are constructed processed foods made therefrom, the with waxed paper liners and are to be total residues of piperonyl butoxide in used only for dried foods that contain 4 or on the processed food shall not be percent fat or less. greater than that permitted by the (4) In two-ply bags consisting of cel- larger of the two tolerances. lophane/polyolefin sheets bound to- gether by an adhesive layer when it is [40 FR 14156, Mar. 28, 1975. Redesignated at 41 incorporated in the adhesive. The FR 26568, June 28, 1976, and amended at 50 FR treated sheets shall contain not more 2958, Jan. 23, 1985. Redesignated at 53 FR than 50 milligrams of piperonyl 24667, June 29, 1988] butoxide per square foot (538 milli- grams per square meter). Such treated § 185.4950 Pirimiphos-methyl. bags are to be used only for packaging (a) Tolerances are established for the prunes, raisins, and other dried fruits combined residues of the insecticide and are to have a maximum ratio of pirimiphos-methyl (O-[2-diethylamino- 3.12 milligrams of piperonyl butoxide 6-methyl-4-pyrimidinyl] O,O-dimethyl per ounce of fruit (0.10 milligram of phosphorothioate) and its metabolite piperonyl butoxide per gram of prod- O-(2-ethylamino-6-methyl-pyrimidin-4- uct). yl) O,O-dimethyl phosphorothioate (5) In food processing and food stor- and, in free and conjugated forms, the age areas: Provided, That the food is re- metabolites 2-diethylamino-6-methyl- moved or covered prior to such use. pyrimidin-4-ol, 2-ethylamino-6-methyl- (b) It is used or intended for use in pyrimidin-4-ol, and 2-amino-6-methyl- combination with pyrethrins and N- pyrimidin-4-ol in or on the following octylbicycloheptene dicarboximide for processed foods when present therein insect control in accordance with as a result of application to stored § 178.3730. grains: (c) A tolerance of 10 parts per million is established for residues of piperonyl Food Parts per butoxide in or on: million (1) Milled fractions derived from ce- Corn milling fractions (except flour) ...... 40 real grains when present therein as a Corn oil ...... 88 result of its use in cereal grain mills Sorghum milling fractions (except flour) ...... 40 and in storage areas for milled cereal grain products. (b) A food additive tolerance of 8.0 (2) Dried foods when present as a re- parts per million is established for resi- sult of migration from its use on the dues of the insecticide pirimiphos- outer ply of multiwall paper bags of 50 methyl (0-[2-diethylamino-6-methyl-4- pounds or more capacity. pyrimidinyl]0,0-dimethyl phos- (3) Foods treated in accordance with phorothioate) and its metabolite 0-(2- § 178.3730. ethylamino-6-methyl-pyrimidine-4- (4) Dried foods that contain 4 percent yl)0,0-dimethylphosphorothioate and, fat, or less, when present as a result of in free and conjugated forms, the me- migration from its use on the cloth of tabolites 2-diethylamino-6-methyl-py- cotton bags of 50 pounds or more capac- rimidin-4-ol,2-ethylamino-6-methyl-py- ity constructed with waxed paper lin- rimidin-4-ol, and 2-amino-6-methylpy- ers. rimidin-4-ol in or on the processed (5) Foods treated in accordance with commodity wheat flour as a result of paragraph (a)(4) and (5) of this section. application to stored wheat grain.

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There are no United States registra- § 185.5150 Propylene oxide. tions for use of pirimiphos-methyl on The food additive propylene oxide wheat, as of June 12, 1990. may be safely used in or on foods in ac- [53 FR 8874, Mar. 18, 1988. Redesignated at 53 cordance with the following prescribed FR 24667, June 29, 1988, and amended at 55 FR conditions: 23737, June 12, 1990] (a) It is intended as a fumigant in or on bulk quantities of cocoa, gums, § 185.5000 Propargite. processed spices, and processed Tolerances are established for resi- nutmeats (except peanuts) when such dues of the insecticide propargite (2-(p- bulk foods are to be further processed tert-butylphenoxy)cyclohexyl 2- into a final food form. propynyl sulfite) in or on the following (b) It is applied in fumigation cham- processed foods when present therein bers not more than one time at a tem- as a result of the application of this in- perature not in excess of 125 °F. The secticide to growing crops: maximum period of fumigation shall not exceed 4 hours for cocoa, processed Food Parts per nutmeats (except peanuts), and proc- million essed spices. For edible gums, the max- Hops, dried ...... 30 imum duration shall be 24 hours. (c) When used as described in para- [44 FR 38841, July 3, 1979. Redesignated at 53 graphs (a) and (b) of this section, resi- FR 24667, June 29, 1988, as amended at 61 FR dues shall not exceed the following 12009, Mar. 22, 1996] limitations:

Food Limita- § 185.5100 Propetamphos. tions1 A tolerance of 0.1 part per million is Cocoa ...... 300 established for residues of the insecti- Gums ...... 300 cide propetamphos ([(e)-]-methylethyl Processed nutmeats (except peanuts) ...... 300 3-[[(ethylamino) Spices, processed ...... 300 methoxyphosphinothioyl]oxy]-2- 1 Expressed as parts per million of propylene oxide. butenoate]) in food commodities ex- posed to the insecticide during treat- (d) When used as a mixture with car- ment of food-handling establishments. bon dioxide (92 parts of carbon dioxide (a) Direct application shall be lim- to 8 parts of propylene oxide on a ited solely to spot and/or crack and weight/weight basis), all commodities crevice treatment in food-handling es- listed in paragraph (c) of this section may be processed not more than one tablishments where food and food prod- time for a period not to exceed 48 hours ucts are held, processed, prepared, or and at a temperature not to exceed 125 served. Spray and dust concentrations °F. shall be limited to a maximum of 1 per- (e) To assure safe use of the additive, cent active ingredient. For crack and the label and labeling of the pesticide crevice treatment, equipment capable formulation containing the food addi- of delivering a dust or a pin-stream of tive shall conform to the label an la- spray directly into cracks and crevices beling registered by the U. S. Environ- shall be used. For spot treatment, a mental Protection Agency. coarse, low-pressure spray shall be used to avoid contamination of food or food- [40 FR 14156, Mar. 28, 1975, as amended at 41 contact surfaces. FR 1589, Jan. 9, 1976. Redesignated at 41 FR (b) To ensure safe use of the insecti- 26568, June 28, 1976, and amended at 42 FR 59852, Nov. 22, 1977. Redesignated at 53 FR cide, its label and labeling shall con- 24667, June 29, 1988, as amended at 61 FR form to that registered by the U.S. En- 12009, Mar. 22, 1996; 61 FR 25154, May 20, 1996] vironmental Protection Agency, and it shall be used in accordance with such § 185.5200 Pyrethrins. label and labeling. The food additive pyrethrins may be [48 FR 52902, Nov. 23, 1983. Redesignated at 53 safely used in accordance with the fol- FR 24667, June 29, 1988] lowing prescribed conditions:

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(a) It is used or intended for use in (2) Dried foods when present as the combination with piperonyl butoxide result of migration from its use on the for control of insects: outer ply of multiwall paper bags of 50 (1) In cereal grain mills and in stor- pounds or more capacity. age areas for milled cereal grain prod- (3) Foods treated in accordance with ucts, whereby the amount of § 185.4500. pyrethrins is from 10 percent to 100 per- (4) Dried foods that contain 4 percent cent of the amount of piperonyl fat, or less, when present as a result of butoxide in the formulation. migration from its use on the cloth of (2) On the outer ply of multiwall cotton bags of 50 pounds or more capac- paper bags of 50 pounds or more capac- ity constructed with waxed paper lin- ity in amounts not exceeding 6 milli- grams per square foot, whereby the ers. amount of pyrethrins is equal to 10 per- (5) Foods treated in accordance with cent of the amount of piperonyl paragraphs (a)(4) and (a)(5) of this sec- butoxide in the formulation. Such tion. treated bags are to be used only for (d) To assure safe use of the additive, dried foods. its label and labeling shall conform to (3) On cotton bags of 50 pounds or that registered with the U.S. Environ- more capacity in amounts not exceed- mental Protection Agency, and it shall ing 5.5 milligrams per square foot of be used in accordance with such label cloth, whereby the amount of and labeling. pyrethrins is equal to 10 percent of the (e) Where tolerances are established amount of piperonyl butoxide in the under sections 408 and 409 of the Act on formulation. Such treated bags are both raw agricultural commodities and constructed with waxed paper liners processed foods made therefrom, the and are to be used only for dried foods total residues of pyrethrins in or on that contain 4 percent fat or less. the processed food shall not be greater (4) In two-ply bags consisting of cel- than that permitted by the larger of lophane/polyolefin sheets bound to- the two tolerances. gether by an adhesive layer when it is incorporated in the adhesive. The [40 FR 14156, Mar. 28, 1975. Redesignated at 41 treated sheets shall contain not more FR 26568, June 28, 1976, and further redesig- than 10 milligrams of pyrethrins per nated and amended at 53 FR 24666, 24668, square foot (107.6 milligrams per square June 29, 1988] meter). Such treated bags are to be used only for packaging prunes, rai- § 185.5375 Sulfonium, trimethyl-salt sins, and other dried fruits and are to with N-(phosphonomethyl)glycine have a maximum ratio of 0.31 milli- (1:1). gram of pyrethrins per ounce of fruit (a) Food additive regulation is estab- (0.01 milligram of pyrethrins per gram lished for residues of the herbicide sul- of product). fonium, trimethyl-salt with N- (5) In food processing areas and food (phosphonomethyl)glycine (1:1) (for- storage areas: Provided, That the food merly glyphosate-trimesium/sulfosate) is removed or covered prior to such in or on the following processed com- use. modities: (b) It is used or intended for use in combination with piperonyl butoxide Commodities Parts per and N-octylbicycloheptene dicarbox- million imide for insect control in accordance Prunes (of which no more than 0.05 ppm is with § 185.4500. trimethylsulfonium) ...... 0.2 (c) A tolerance of one part per mil- Raisins (of which no more than 0.05 ppm is lion is established for residues of trimethylsulfonium) ...... 0.20 Soybean, hulls (of which no more than 2 ppm is pyrethrins in or on: trimethylsulfonium) ...... 7.0 (1) Milled fractions derived from ce- real grains when present as a result of (b) [Reserved] its use in cereal grain mills and in stor- age areas for milled cereal grain prod- [61 FR 9359, Mar. 8, 1996, as amended at 61 FR ucts. 15900, Apr. 10, 1996]

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§ 185.5950 Triforine. PART 186—PESTICIDES IN ANIMAL A food additive regulation is estab- FEED lished to permit residues of the fun- gicide triforine (N,N-[1,4-pipera- Subpart A [Reserved] zinediylbis(2,2,2-trichloroethylidene)] bis[formamide]) in or on the following Subpart B—Feed Additives Permitted in processed foods when present therein Animal Feed as a result of application to growing Sec. hops: 186.150 Aldicarb. 186.200 Aluminum phosphide. Food Parts per 186.450 sec-Butylamine. million 186.550 . Hops, dried ...... 60 186.850 2-(m-Chlorophenoxy)propionic acid. 186.950 2-Chloro-1-(2,4,5- trichlorophenyl)vinyl dimethyl phos- [52 FR 39222, Oct. 21, 1987. Redesignated at 53 phate. FR 24667, June 29, 1988] 186.1000 Chlorpyrifos. 186.1050 Chlorpyrifos-methyl. § 185.6300 Zinc ion and maneb coordi- 186.1350 Cyhexatin. nation product. 186.1500 Dalapon. 186.1650 Dialifor. Tolerances are established for resi- 186.1700 Diatomaceous earth. dues of a fungicide which is a coordina- 186.1800 Dicamba. tion product of zinc ion and maneb 186.1860 3,7-Dichloro-8-quinoline carboxylic (manganous acid. ethylenebisdithiocarbamate) contain- 186.2000 . ing 20 percent manganese, 2.5 percent 186.2050 Dimethipin. zinc, and 77.5 percent 186.2100 including its oxygen ethylenebisdithiocarbamate (the whole analog. 186.2275 N,N-Dimethylpiperidinium chloride. product calculated as zinc 186.2325 O,O-Dimethyl 2,2,2-trichloro-1- ethylenebisdithiocarbamate) in or on hydroxyethyl phosphonate. the following processed foods, when 186.2450 . present therein as a result of the appli- 186.2500 Diquat. cation of this fungicide to growing 186.2700 Ethephon. crops: 186.2950 Ethyl 3-methyl-4-(methyl- thio)phenyl (1-methylethyl)-phos- 20 parts per million in the bran of oats. phoramidate. 186.3000 O-Ethyl O-[4-(methylthio)phenyl] S- [40 FR 14156, Mar. 28, 1975. Redesignated at 41 propyl phosphorodithioate. FR 26568, June 28, 1976 and 53 FR 24667, June 186.3250 Fluazifop-butyl. 29, 1988, and amended at 59 FR 33694, 33696, 186.3325 Flumiclorac pentyl; tolerances for June 30, 1994; 61 FR 12009, Mar. 22, 1996; 61 FR residues. 25154, May 20, 1996] 186.3400 (Alpha RS,2R)-fluvalinate [(RS)- alpha-cyano-3-phenoxbenzyl(R)-2-[2- Subpart C—Food Additives Result- chloro-4-(trifluoromethyl) anilino]-3- ing From Contact With Con- methylbutanoate]. 186.3550 Hexakis (2-methyl-2-phenyl- tainers or Equipment and propyl)distannoxane. Food Additives Otherwise Af- 186.3575 Hexazinone. fecting Food 186.3650 Imazalil. 186.3700 Inorganic bromides. § 185.7000 Malathion. 186.3750 Iprodione. 186.3775 d-Limonene. Malathion may be safely used for the 186.3800 Magnesium phosphide. control of insects during the drying of 186.3850 Malathion. grapes (raisins) in compliance with 186.4035 Metarhizium anisopliae strain § 185.3850 by incorporation into paper ESF1. trays in amounts not exceeding 100 186.4150 Methoprene. milligrams per square foot. 186.4575 . 186.4850 Picloram. [40 FR 14156, Mar. 28, 1975. Redesignated at 41 186.4900 Piperonyl butoxide. FR 26568, June 28, 1976, and amended at 50 FR 186.4950 Pirimiphos-methyl. 2958, Jan. 23, 1985. Redesignated and amended 186.4975 . at 53 FR 24666, 24668, June 29, 1988] 186.5000 Propargite.

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