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Polycyclic Aromatic Hydrocarbon (PAH) Distributions Within Urban Estuarine Sediments

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Polycyclic Aromatic Hydrocarbon (PAH) Distributions Within Urban Estuarine Sediments W&M ScholarWorks Dissertations, Theses, and Masters Projects Theses, Dissertations, & Master Projects 1997 Polycyclic aromatic hydrocarbon (PAH) distributions within urban estuarine sediments Siddhartha Mitra College of William and Mary - Virginia Institute of Marine Science Follow this and additional works at: https://scholarworks.wm.edu/etd Part of the Biogeochemistry Commons, Environmental Sciences Commons, and the Geochemistry Commons Recommended Citation Mitra, Siddhartha, "Polycyclic aromatic hydrocarbon (PAH) distributions within urban estuarine sediments" (1997). Dissertations, Theses, and Masters Projects. Paper 1539616779. https://dx.doi.org/doi:10.25773/v5-74km-4h38 This Dissertation is brought to you for free and open access by the Theses, Dissertations, & Master Projects at W&M ScholarWorks. It has been accepted for inclusion in Dissertations, Theses, and Masters Projects by an authorized administrator of W&M ScholarWorks. For more information, please contact [email protected]. INFORMATION TO USERS This manuscript has been reproduced from the microfilm master. UMI films the text directly from the original or copy submitted. Thus, some thesis and dissertation copies are in typewriter face, while others may be from any type o f computer printer. The quality of this reproduction is dependent upon the quality of the copy submitted. Broken or indistinct print, colored or poor quality illustrations and photographs, print bleedthrough, substandard margins, and improper alignment can adversely afreet reproduction. In the unlikely event that the author did not send UMI a complete manuscript and there are missing pages, these will be noted. Also, if unauthorized copyright material had to be removed, a note will indicate the deletion. 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Reproduced with with permission permission of the of copyright the copyright owner. owner.Further reproductionFurther reproduction prohibited without prohibited permission. without permission. Polycyclic Aromatic Hydrocarbon (PAH) Distributions Within Urban Estuarine Sediments A Dissertation Presented to the Faculty of the School of Marine Science The Virginia Institute of Marine Science The College of William and Mary In Partial Fulfillment of the Requirements for the Degree o f Doctor of Philosophy by Siddhartha Mitra 1997 Reproduced with permission of the copyright owner. Further reproduction prohibited without permission. UMI Number: 9815246 UMI Microform 9815246 Copyright 1998, by UMI Company. All rights reserved. This microform edition is protected against unauthorized copying under Title 17, United States Code. UMI 300 North Zeeb Road Ann Arbor, MI 48103 Reproduced with permission of the copyright owner. Further reproduction prohibited without permission. APPROVAL SHEET This dissertation is submitted in partial fulfillment of the requirements for the degree o f Doctor of Philosophy i ! i i Siddhartha Mitra Approved December 1997 Rebecca Dickhut, Ph. D. Committee Chairperson/Major Professor ames Bauer, Ph. D William MacIntyre, Ph. D: 7 n d ± ( M ^ , k Patterson, Ph. D. Linda Schaflner/frh. D. Brownawell Ph. D. SUNY Stonybrook Reproduced with permission of the copyright owner. Further reproduction prohibited without permission. TABLE OF CONTENTS Page Acknowledgements............................................................................... i Dedication.............................................................................................. k List of Tables......................................................................................... iti List of Figures........................................................................................ rv Abstract.................................................................................................. vi Chapter 1. Introduction...................................................................... 1 1.1 Introduction ..................................................................... 1 1.2 Sorption theory. ................................................................ 3 1.3 Hypotheses ...................................................................... 10 1.4 Objectives ........................................................................ 12 1.5 References ....................................................................... 13 Chapter 2. Polycyclic aromatic hydrocarbon distribution coefficients in estuarine sediments: The role of PAH source and sediment geochemistry................................................................................ 17 2.1 Introduction ......................................................................... 19 2.2 Factors hypothetically affecting PAH K’qcS.......................... 21 2.3 Sediment heterogeneity. ...................................................... 23 2.4 Site background .................................................................. 24 2.5 Methods .............................................................................. 26 2.6 Results and Discussion ........................................................ 31 2.7 Conclusions ........................................................................ 51 2.8 References .......................................................................... 52 Chapter 3. Three phase modeling of polycyclic aromatic hydrocarbon association with pore water dissolved organic carbon.................. 57 3.1 Introduction .......................................................................... 59 3.2 Methods ............................................................................... 63 3.3 Results and Discussion ......................................................... 66 3.4 Conclusions ......................................................................... 72 3.5 References .......................................................................... 76 Reproduced with permission of the copyright owner. Further reproduction prohibited without permission. I Page Chapter 4. Polycyclic aromatic hydrocarbon deposition and geochemistry in Hudson River sediments .......................................................... 79 4.1 Introduction ......................................................................... 81 4.2 Methods ............................................................................... 82 4.3 Results................................................................................. 88 4.4 Discussion ............................................................................ 102 4.5 Conclusions .......................................................................... 107 4.6 References ............................................................................ 108 Chapter 5. Summary. .............................................................................. 113 Appendices ............................................................................................... 116 Reproduced with permission of the copyright owner. Further reproduction prohibited without permission. ACKNOWLEDGMENTS First and foremost, I must acknowledge my advisor Dr. Rebecca Dickhut for her outstanding mentorship, confidence in my abilities, financial support, and the often deserved “kick.” I would also like to thank the rest of my committee members Dr. Jim Bauer, Dr. Bruce Brownawell, Dr. Bill MacIntyre, Dr. Mark Patterson, and Dr. Linda Schafifher. A special thanks to Dr. Linda Schafifher for her constant reminder to consider the “forest” while staring at the “tree” and to Dr. Bruce Brownawell for facilitating sampling the East River and Newark Bay. Many thanks to Dr. Catherine Chisholm-Brause and Dr. Elizabeth Canuel, not only for their advice over the years but also for use of their laboratory facilities. Certainly second to none as the person who can do it all and keep smiling, my unfailing gratitude goes out to Libby MacDonald. Also, special thanks to Ginger Edgecombe for the hours and hours of dedication to processing my samples. Shannon Burcham and Linda Meneghini: I appreciate all of your answers to my endless questions. Special thanks to Linda Meneghini for all the snacks she has provided—you have no idea how much energy a Tootsie Roll can infuse at 2 am when there is just one more sample to process. To the students on the third floor of Chesapeake Bay Hall, North Wing: I want to thank you for all of your help over the last few years and for your assistance in keeping us in organic geochemistry a "fine-tuned-silicone-lubricated- machine". There are some additional people who deserve special recognition - friends who helped sample at least once: Pat Calautti, Tim Dellapena, Kimani Kimbrough, Krisa Murray, Michelle Thompson, Andy Zimmerman - 1 thank you and hope you enjoyed your stint in urban oceanography, my roommate
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