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EPA Surveyneuse River WQ Report

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EPA Surveyneuse River WQ Report CITY OF RALEIGH PUBLIC UTILITIES DEPARTMENT Neuse River Water Quality Sampling Final Report June 2014 Table of Contents Executive Summary Neuse River Water Quality Sampling ES.1 Study Summary........................................................................................................................................ ES-1 ES.2 Study Overview ........................................................................................................................................ ES-1 ES.3 Key Results ................................................................................................................................................ ES-1 ES.4 Recommendations for Future Work ............................................................................................... ES-3 Section 1 Introduction 1.1 Project Background.................................................................................................................................. 1-1 1.2 Study Objectives and Report Format ............................................................................................... 1-2 1.3 Constituents of Interest in the Neuse River ................................................................................... 1-3 Section 2 Water Quality of the Neuse River 2.1 NCDENR Data ............................................................................................................................................. 2-2 2.1.1 DO and Chlorophyll Exceedances ...................................................................................... 2-2 2.1.2 Fecal Coliform Exceedances ................................................................................................ 2-2 2.1.3 Metals and Industrial Pollutants........................................................................................ 2-4 2.2 LNBA Historical Data ............................................................................................................................... 2-5 2.3 Trace Chemical Constituents in the Neuse River and Region ................................................ 2-8 2.3.1 Trace Chemical Constituents in the Neuse River ........................................................ 2-9 2.3.2 Drinking Water ........................................................................................................................2-10 2.4 Summary.....................................................................................................................................................2-11 Section 3 Water Quality of the Neuse River WWTP Effluent 3.1 Historical Compliance Data for Neuse River WWTP ................................................................. 3-1 3.2 Trace Chemical Constituents in WWTPs ........................................................................................ 3-1 3.2.1 Neuse River WWTP Effluent Trace Chemical Constituent Characterization (EPA Data) ............................................................................................. 3-1 3.2.2 Literature Survey of Trace Chemical Constituents in WWTPs in the Region ............................................................................................................................ 3-6 Section 4 Study Design 4.1 Selection of Constituents for Analysis.............................................................................................. 4-1 4.1.1 Conventional Parameters ..................................................................................................... 4-1 4.1.2 Microbial Indicators ................................................................................................................ 4-2 4.1.2.1 Viruses ..................................................................................................................................... 4-2 4.1.2.1 Bacteria ................................................................................................................................... 4-2 4.1.2.3 Protozoa .................................................................................................................................. 4-2 4.1.3 Chemical Constituents............................................................................................................ 4-3 4.1.4 Genotoxicity ................................................................................................................................ 4-5 4.1.5 Emission- Excitation Matrix (EEM) .................................................................................. 4-6 4.2 Selection of Sampling Locations ......................................................................................................... 4-7 4.3 Sampling Frequency, Duration, and Targeted River Flow ...................................................... 4-7 4.4 Sample Type ................................................................................................................................................ 4-9 i Table of Contents • City of Raleigh – Neuse River Water Quality Sampling Report Section 5 Neuse River Study Methods 5.1 Sample Collection ...................................................................................................................................... 5-1 5.2 Methods by Analyte .................................................................................................................................. 5-2 5.3 Method Descriptions ................................................................................................................................ 5-6 5.3.1 Ames Test ..................................................................................................................................... 5-6 5.3.2 Clostridium Perfringens ........................................................................................................ 5-6 5.3.3 E. Coli, Coliforms, and Enterococci .................................................................................... 5-7 5.3.4 Emission Excitation Matrix (EEM) .................................................................................... 5-7 5.3.5 HBCD .............................................................................................................................................. 5-7 5.3.6 N-Nitrosodimethylamine ...................................................................................................... 5-8 5.3.7 Nonylphenols ............................................................................................................................. 5-8 5.3.8 Perfluorinated Compounds .................................................................................................. 5-9 5.3.9 Pharmaceuticals & Personal Care Products .................................................................. 5-9 5.3.10 Sterols & Hormones ................................................................................................................. 5-9 5.4 Statistical Methods Used ..................................................................................................................... 5-10 5.5 Considerations for Data Interpretation ........................................................................................ 5-10 Section 6 Neuse River Study Results and Discussion 6.1 Presentation of Results and Discussion ........................................................................................... 6-1 6.1.1 Organization of Results and Discussion .......................................................................... 6-1 6.1.2 Statistical Tests .......................................................................................................................... 6-1 6.1.3 Data Quality................................................................................................................................. 6-1 6.1.4 Wastewater Tracer .................................................................................................................. 6-1 6.2 River Flow, Precipitation and Time of Travel ............................................................................... 6-3 6.2.1 Results ........................................................................................................................................... 6-3 6.2.2 Interpretation ............................................................................................................................ 6-5 6.3 Water Quality of the Neuse River WWTP Effluent During Sampling .................................. 6-6 6.3.1 Results ........................................................................................................................................... 6-6 6.3.2 Interpretation ............................................................................................................................ 6-6 6.4 Wastewater Tracer Sucralose ............................................................................................................. 6-6 6.4.1 Results ........................................................................................................................................... 6-6 6.4.2 Interpretation ............................................................................................................................ 6-7 6.5 Conventional Parameters (Neuse River Samples) ...................................................................... 6-7 6.5.1 Results ..........................................................................................................................................
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