Viewing My Thesis and Contributing to Its Improvement

Total Page:16

File Type:pdf, Size:1020Kb

Viewing My Thesis and Contributing to Its Improvement UNIVERSITY OF CINCINNATI Date:___________________ I, _________________________________________________________, hereby submit this work as part of the requirements for the degree of: in: It is entitled: This work and its defense approved by: Chair: _______________________________ _______________________________ _______________________________ _______________________________ _______________________________ Heat Transfer Studies of a Pyrotechnic Event and its Effect on Fuel Pool Ignition A thesis submitted to the Division of Research and Advanced Studies of the University of Cincinnati in partial fulfillment of the requirements for the degree of MASTER OF SCIENCE in the Department of Mechanical, Industrial and Nuclear Engineering of the College of Engineering 2005 by Ravi Prasad B.E., Marine Engineering and Research Institute, Kolkata, India Committee Chair: Dr. Peter J. Disimile ABSTRACT The local temperature field associated with a pyrotechnic event has numerous implications, particularly in the area of aircraft survivability. This study determined the temperature distribution within the vicinity of the fireball of a pyrotechnic event. A low cost simulation methodology has been developed to provide further understanding of this type of event from data involving both the geometric and thermal state of a generated incendiary cloud. The study discusses the temperature measurement methodology, the temperature distribution within and outside a fireball volume. The study also provides empirical evidence that the measured temperature, over the short duration of the pyrotechnic event, cannot accurately be determined from the size and radiant emission of the light emitted. The second phase of the study examines the ignition of a fuel pool by the pyrotechnic event. Ignition height for various fuel pool temperatures has been determined. These studies showed that the size and radiation emitted by the incendiary cloud, above the fuel pool, does not correlate with the height at which the fuel pool ignites. ACKNOWLEDGEMENTS I would like to thank the funding support from the Department of Defense, The Joint Aircraft Survivability (JAS) program office. I would like to thank Dr. Peter J. Disimile, Associate Professor at the Dept. of ASE & EM and my thesis advisor, for his excellent guidance, support and patience during the course of this dissertation. I would like to thank Dr. Norman Toy, Professor at the University of Surrey UK, for his valuable insights and suggestions during critical junctures of the research. I would also like to thank Dr. Michael Kazmierczak, Associate Professor at the Dept. of MINE, and Dr. Milind Jog, Associate Professor at the Dept. of MINE, for agreeing to be on the defense committee and reviewing my thesis and contributing to its improvement. I would also like to thank Mr. Curtis Fox, Research Associate at the Dept. of ASE & EM, for having helped in the various stages of the research. I appreciate the guidance of Mr. Doug Hurd, Junior Research Associate at the Dept. of MINE, at the Mechanical Engineering workshop. I would like to thank Mr. Bo Westheider, Instrumentation Specialist at the Dept. of MINE, for providing the electric supply equipment. Special thanks to Mr. Jeremy Dusina, Graduate Student at the Dept. of ASE & EM, for having provided an unending supply of thermocouples. I would like to thank all my friends for their moral support and having made my stay at the University of Cincinnati enjoyable. I would like to appreciate the support shown to me by the members of UC- FEST lab. Thank you. TABLE OF CONTENTS 1 INTRODUCTION ..................................................................................................................9 1.1 Problem Description ....................................................................................................... 9 1.2 Objective....................................................................................................................... 11 1.3 History and Background............................................................................................... 12 2 EXPERIMENTAL METHODS............................................................................................14 2.1 Development stage of the Experimental Rig ................................................................ 14 2.2 Manufacture of the Experimental Rig........................................................................... 19 2.3 Development stage of the Test Piece............................................................................ 24 2.4 Manufacture of the Test Charge ................................................................................... 28 2.4.1 Mold for cylindrical test charge............................................................................ 28 2.4.2 Support Rod with Heating Element ...................................................................... 28 2.4.3 Composition of test charge ................................................................................... 29 2.4.4 CPM ...................................................................................................................... 30 2.4.5 Labmix .................................................................................................................. 31 2.4.6 Electric match composition................................................................................... 32 2.4.7 Mixing Method..................................................................................................... 33 2.4.8 Casting Process..................................................................................................... 34 2.5 Experimental Procedure................................................................................................ 34 2.5.1 Fixing the test charge............................................................................................ 34 2.5.2 Alignment of thermocouple .................................................................................. 35 2.5.3 Setting up the data acquisition system.................................................................. 36 1 3 TEMPERATURE MEASUREMENTS................................................................................ 38 3.1 Theory of Thermocouples............................................................................................. 38 3.1.1 Seebeck effect....................................................................................................... 38 3.1.2 Thermocouple definition....................................................................................... 38 3.2 Thermocouples.............................................................................................................. 38 3.2.1 Types of thermocouples........................................................................................ 38 3.2.2 Thermocouple selection criteria............................................................................ 38 3.2.3 Thermocouple selected......................................................................................... 40 3.3 Calibration and Data acquisition................................................................................... 43 3.3.1 Effect of Additional Junctions .............................................................................. 43 3.3.2 Software compensation......................................................................................... 44 3.3.3 Data acquisition system ........................................................................................ 45 3.3.4 LabVIEW software ............................................................................................... 45 4 TEMPERATURE FIELD ANALYSIS ................................................................................ 48 4.1 Pyrotechnic theory........................................................................................................ 48 4.1.1 Definition .............................................................................................................. 48 4.1.2 Composition.......................................................................................................... 48 4.1.3 Reaction Process................................................................................................... 48 4.2 Heat Release calculations ............................................................................................. 50 4.2.1 Heat Release from test charge made of CPM ....................................................... 50 4.2.2 Heat Release from test charge made of Labmix ................................................... 52 4.2.3 Heat Release from Heating element ..................................................................... 54 4.3 Sparkler temperature profile analysis ........................................................................... 55 2 4.4 CPM profile analysis..................................................................................................... 60 4.5 Labmix profile analysis................................................................................................. 61 4.6 Comparison of profiles ................................................................................................. 63 5 IMAGING............................................................................................................................. 65 5.1 Development of the procedure...................................................................................... 65 5.2 Equipment
Recommended publications
  • The Study of Hems Based on the Mechanically Activated Intermetallic Al12mg17 Powder
    molecules Article The Study of HEMs Based on the Mechanically Activated Intermetallic Al12Mg17 Powder Sergei Sokolov * , Alexander Vorozhtsov, Vladimir Arkhipov and Ilya Zhukov Laboratory of Metallurgy Nanotechnologies, National Research Tomsk State University, Lenin Avenue, 36, 634050 Tomsk, Russia; [email protected] (A.V.); [email protected] (V.A.); [email protected] (I.Z.) * Correspondence: [email protected]; Tel.: +7-923-406-77-01 Academic Editor: Svatopluk Zeman Received: 30 May 2020; Accepted: 19 July 2020; Published: 5 August 2020 Abstract: In this work, Al–Mg intermetallic powders were characterized and obtained by melting, casting into a steel chill and subsequent mechanical activation in a planetary mill. The method for producing Al12Mg17 intermetallic powder is presented. The dispersity, morphology, chemical composition, and phase composition of the obtained powder materials were investigated. Certain thermodynamic properties of high-energy materials containing the Al-Mg powder after mechanical activation of various durations were investigated. The addition of the Al-Mg powders to the high-energy composition (synthetic rubber SKDM-80 + ammonium perchlorate AP + boron B) can significantly increase the burning rate by approximately 47% and the combustion heat by approximately 23% compared with the high-energy compositions without the Al-Mg powder. The addition of the Al12Mg17 powder obtained after 6 h of mechanical activation provides an increase in the burning rate by 8% (2.5 0.1 mm/s for the mechanically activated Al Mg powder and ± 12 17 2.3 0.1 mm/s for the commercially available powder) and an increase in the combustion heat by 3% ± (7.4 0.2 MJ/kg for the mechanically activated Al-Mg powder and 7.1 0.2 MJ/kg for the commercially ± ± available powder).
    [Show full text]
  • Development of Filler Metals and Procedures for Vacuum Brazing Of
    Development of Filler Metals and Procedures for Vacuum Brazing of Aluminum Several brazing filler metal compositions have been developed which offer significant improvements over existing compositions. They braze in vacuum at temperatures lower than normal flow temperatures and have equal or better flowability BY W. J. WERNER, G. M. SLAUGHTER AND F. B. GURTNER Introduction ry cleanliness levels under production vantages. As a single entity, it was This report documents work per­ conditions. The maximum allowable immediately more desirable from a formed toward the development of lag between cleaning and brazing was cleaning, assembling and material found to be 12 hours. handling standpoint. Metallurgically, new brazing filler metals for vacuum- 2 fluxless brazing (1 X 10~6 torr) C. S. Beuyukian developed tech­ the 4045 brazing filler metal with its certain aluminum alloys of interest to niques for vacuum or inert gas fluxless lower silicon content allowed greater the Army. The base metals under brazing of aluminum cold plates for latitude in processing parameters than consideration were alloys 6061, 2219, use in Apollo command modules. In did alloy No. 718. 7075 and 2024. Brazing filler metal this work, brazing filler metal No. 718 Finally, the workers at Aeronca, and No. 23 brazing sheet were evalu­ Inc. completed a study on inert gas flow temperatures needed for these 3 alloys encompass the temperature ated. Alloy No. 718 is nominally 88% brazing of aluminum in early 1967. range 900 to 1200F. Specifically, the aluminum, 12% silicon; No. 23 braz­ Their work was concerned with de­ contract called for the development of ing sheet is comprised of 6951 base velopment of high strength brazed alloys with flow temperatures of 950, alloy clad on one side with 4045 aluminum honeycomb structures 1000, and 1050F.
    [Show full text]
  • Maec.19 70 (University of London) London
    COMPLEX & INCREMENTAL STRESS CREEP OF A HIGH STRENGTH ALUMINIUM ALLOY AT ELEVATED TEMPERATURES (ALLOY: HIDUMINIUM RR58 SPECIFICATION DTD 731) by SURINDAR BAHADUR MATHUR Thesis presented in the Department of Mechanical Engineering for the Award of the Doctor of Philosphy in Mechanical Engineering of the University of London. Mechanical Engineering Department Imperial College of Science and Technology mAec.19 70 (University of London) London. ABSTRACT A theory for creep rates under complex and incremental stresses is deduced from experimental data concerning complex creep at elevated temperatures for the test material HIDUMINIUM RR 58 - Specification DID 731. The most important results are for tubular specimens tested at 150°C and 250°C under incremental loads. The analysis of results relates to steady state creep only. Modified relationships in stress equivalence and strain equivalence are proposed to account for thermal softening, polygonization, recrystallization and the resulting exaggerated flow in the direction of the applied shear. (The original equations are based on the hypothesis of Von Mises). A further relationship is suggested between the immediate total energy of distortion and the subsequent creep work rate. Results of the static tests and the results of the tests for creep behaviour under complex loading are presented and compared with the results of static torsion and simple incremental torsion creep tests on the basis of the proposed equations. An appendix describes the complex creep testing machine, furnace, extensometers
    [Show full text]
  • Pyrotechnic Serpents
    Edited by Jack & Dorothy Drewes American Fireworks News THE BEST OF AFN III Edited by Jack & Dorothy Drewes Copyright ©1995 by Rex E. & S. P., Inc. Published by American Fireworks News HC67 - Box 30 Dingmans Ferry, PA 18328 All rights reserved. ISBN 0-929931-11-4 Printed in The United States of America 1st printing, April, 1995. 2nd printing, March, 1996 3rd printing, March, 1998 Warning: This publication contains descriptions and pictures of fireworks. The information contained herein is based on the authors' experiences using specific tools and ingredients under specific conditions not necessarily described in the articles. No warranties are made, given or implied. Readers are cautioned that they must form their own opinion as to the application of any information contained herein. 2 CONTENTS BASICS, SMALL DEVICES DISPLAY GOODS & OPERATIONS Getting a Pyro Education 7 The Basic Technician, #1, 2, 3 62 Fireworks and Me 8 Unexplained Explosion & Probability Lightning & Thunder Fountain 9 Theory 66 Construction Techniques of %" Roman Pyro Emitting Device 67 Candle Using Round Stars 10 Fireworks on a Budget 68 Bigger & Better Breaks with Small Ball Vis-A-Vis Fountains 70 Shells 11 Neon Blue & Recumbent Lances 71 Designing Portfires 12 Molecular Sieves as Cores 72 Fun with Jumping Jacks 14 Lance Development 73 Tischfeuerwerk 15 Illumination Breaks & Shimmering Bike Wheel Pyro 16 Curtains 73 Ground Bloom Flower Wheel 16 Pyro Surprises 74 Easy Sun 18 Push Sticks Aid Low Breaks 75 Class C Repeaters 19 Eight Experiments in Non-Commercial Exploding
    [Show full text]
  • Washington State Patrol Crime Laboratory Division Materials
    Washington State Patrol Crime Laboratory Division Materials Analysis EXPLOSIVES TRAINING MANUAL May 2018 Washington State Patrol Crime Laboratory Division Explosives Laboratory Training Manual Contents 1 INTRODUCTION ..................................................................................................................................... 7 1.1 PURPOSE AND SCOPE ................................................................................................................... 7 1.2 ORGANIZATION OF THE TRAINING MANUAL ................................................................................ 7 2 EXPLOSIVES ANALYSIS OVERVIEW ........................................................................................................ 9 2.1 OBJECTIVES ................................................................................................................................... 9 2.2 OVERVIEW ..................................................................................................................................... 9 2.2.1 Definitions ............................................................................................................................. 9 2.3 SUGGESTED READINGS ............................................................................................................... 11 2.3.1 Introduction ........................................................................................................................ 11 2.3.2 Scene ..................................................................................................................................
    [Show full text]
  • Aluminium Alloys Chemical Composition Pdf
    Aluminium alloys chemical composition pdf Continue Alloy in which aluminum is the predominant lye frame of aluminum welded aluminium alloy, manufactured in 1990. Aluminum alloys (or aluminium alloys; see spelling differences) are alloys in which aluminium (Al) is the predominant metal. Typical alloy elements are copper, magnesium, manganese, silicon, tin and zinc. There are two main classifications, namely casting alloys and forged alloys, both further subdivided into heat-treatable and heat-free categories. Approximately 85% of aluminium is used for forged products, e.g. laminated plates, foils and extrusions. Aluminum cast alloys produce cost-effective products due to their low melting point, although they generally have lower tensile strength than forged alloys. The most important cast aluminium alloy system is Al–Si, where high silicon levels (4.0–13%) contributes to giving good casting features. Aluminum alloys are widely used in engineering structures and components where a low weight or corrosion resistance is required. [1] Alloys composed mostly of aluminium have been very important in aerospace production since the introduction of metal leather aircraft. Aluminum-magnesium alloys are both lighter than other aluminium alloys and much less flammable than other alloys containing a very high percentage of magnesium. [2] Aluminum alloy surfaces will develop a white layer, protective of aluminum oxide, if not protected by proper anodization and/or dyeing procedures. In a wet environment, galvanic corrosion can occur when an aluminum alloy is placed in electrical contact with other metals with a more positive corrosion potential than aluminum, and an electrolyte is present that allows the exchange of ions.
    [Show full text]
  • Microstructual and Thermal Analysis of Aluminum-Silicon and Magnesium-Aluminum Alloys Subjected to High Cooling Rates
    University of Windsor Scholarship at UWindsor Electronic Theses and Dissertations Theses, Dissertations, and Major Papers 2012 Microstructual and Thermal Analysis of Aluminum-Silicon and Magnesium-Aluminum Alloys Subjected to High Cooling Rates Paul Marchwica University of Windsor Follow this and additional works at: https://scholar.uwindsor.ca/etd Recommended Citation Marchwica, Paul, "Microstructual and Thermal Analysis of Aluminum-Silicon and Magnesium-Aluminum Alloys Subjected to High Cooling Rates" (2012). Electronic Theses and Dissertations. 5572. https://scholar.uwindsor.ca/etd/5572 This online database contains the full-text of PhD dissertations and Masters’ theses of University of Windsor students from 1954 forward. These documents are made available for personal study and research purposes only, in accordance with the Canadian Copyright Act and the Creative Commons license—CC BY-NC-ND (Attribution, Non-Commercial, No Derivative Works). Under this license, works must always be attributed to the copyright holder (original author), cannot be used for any commercial purposes, and may not be altered. Any other use would require the permission of the copyright holder. Students may inquire about withdrawing their dissertation and/or thesis from this database. For additional inquiries, please contact the repository administrator via email ([email protected]) or by telephone at 519-253-3000ext. 3208. Microstructual and Thermal Analysis of AlSi and MgAl Alloys Subjected to High Cooling Rates By Paul C. Marchwica A Thesis Submitted to the Faculty of Graduate Studies through the Department of Mechanical, Automotive and Materials Engineering in Partial Fulfillment of the Requirements for the Degree of Master of Applied Science at the University of Windsor Windsor, Ontario, Canada 2012 © 2012 P.
    [Show full text]
  • Aluminum Alloy Weldability: Identification of Weld Solidification Cracking Mechanisms Through Novel Experimental Technique and Model Development
    Dipl.-Ing. Nicolas Coniglio Aluminum Alloy Weldability: Identifi cation of Weld Solidifi cation Cracking Mechanisms through Novel Experimental Technique and Model Development BAM-Dissertationsreihe • Band 40 Berlin 2008 Die vorliegende Arbeit entstand an der BAM Bundesanstalt für Materialforschung und -prüfung. Impressum Aluminum Alloy Weldability: Identifi cation of Weld Solidifi cation Cracking Mechanisms through Novel Experimental Technique and Model Development 2008 Herausgeber: BAM Bundesanstalt für Materialforschung und -prüfung Unter den Eichen 87 12205 Berlin Telefon: +49 30 8104-0 Telefax: +49 30 8112029 E-Mail: [email protected] Internet: www.bam.de Copyright © 2008 by BAM Bundesanstalt für Materialforschung und -prüfung Layout: BAM-Arbeitsgruppe Z.64 ISSN 1613-4249 ISBN 978-3-9812354-3-2 Aluminum Alloy Weldability: Identification of Weld Solidification Cracking Mechanisms through Novel Experimental Technique and Model Development Dissertation zur Erlangung des akademischen Grades Doktor-Ingenieur (Dr.-Ing.) genehmigt durch die Fakultät für Maschinenbau der Otto-von-Guericke-Universität Madgeburg am 02.06.08 vorgelegte Dissertation von Dipl.-Ing. Nicolas Coniglio Thesis Committee: Prof. Dr.-Ing. A. Bertram Prof. Dr.-Ing. T. Böllinghaus Prof. C.E. Cross Prof. S. Marya Date of Examination: 23 October 2008 Abstract Abstract The objective of the present thesis is to make advancements in understanding solidification crack formation in aluminum welds, by investigating in particular the aluminum 6060/4043 system. Alloy 6060 is typical of a family of Al-Mg-Si extrusion alloys, which are considered weldable only when using an appropriate filler alloy such as 4043 (Al-5Si). The effect of 4043 filler dilution (i.e. weld metal silicon content) on cracking sensitivity and solidification path of Alloy 6060 welds are investigated.
    [Show full text]
  • DEFINITIONS and TYPES of CONSUMER FIREWORKS Summary of Survey Responses C.O.B., October 19, 2007
    FLORIDA DEPARTMENT OF AGRICULTURE AND CONSUMER SERVICES FLORIDA CONSUMER FIREWORKS TASK FORCE DEFINITIONS AND TYPES OF CONSUMER FIREWORKS Summary of Survey Responses C.O.B., October 19, 2007 Members Responding: Michelle Berger, Rickey Farrell, Tommy Glasgow, Les Hallman, Mike Long, Ira Schwartz Ken Welch Members Not Responding: Trey McCarley, Definition for “Consumer Fireworks” Respondents provided a definition that each would like the Task Force to evaluate at the October 25, 2007 meeting. o Consumer fireworks are those approved on a list maintained by the Florida State Fire Marshals office and which are sold for individual use. o Any small firework device designed to produce visible effects by combustion and which must comply with the construction, chemical composition, and cautionary labeling regulations of the CPSC, as set forth in title 16, Code of Federal Regulations, parts 1500 and 1507. Some small devices designed to produce audible effects are included, such as whistling devices, ground devices containing 50mg or less of explosive materials, and aerial devices containing 130mg or less of explosive materials. The U.S. Dept of Transportation (DOT) at 49 CFR 172.01 classifies consumer fireworks as fireworks UN0336 and UN0337. (Not all fireworks covered by this definition are allowed for consumer use in the State, however may be allowable for wholesale under certain conditions defined within this law.) o Retail purchase of product that does not explode or launch. o The term "consumer fireworks" shall mean and include: Any combustible
    [Show full text]
  • APA STANDARD 87-1 Contents 1
    APA STANDARD 87-1 Contents 1. INTRODUCTION..............................................................................................1 2. DEFINITIONS.....................................................................................................1 3. REQUIREMENTS FOR CONSUMER FIREWORKS, NOVELTIES AND THEATRICAL PYROTECHNICS .....................................................................4 3.1 Types of Consumer Fireworks.......................................................................5 3.2 Types of Novelties .........................................................................................8 3.4 Other Devices ................................................................................................9 3.6 Specific Requirements for Consumer Fireworks...........................................10 3.7 Prohibited Chemicals and Components.........................................................12 3.8 Requirements for Theatrical Pyrotechnics ....................................................13 3.9 Approval ........................................................................................................13 3.10 Marking and Labeling..................................................................................14 4. REQUIREMENTS FOR DISPLAY FIREWORKS DEVICES ..........................14 4.1 Types of Display Fireworks Devices.............................................................14 4.2 Construction of Aerial Shells.........................................................................15 4.3 Approval
    [Show full text]
  • Circular of the Bureau of Standards No. 76: Aluminum and Its Light Alloys
    DEPARTMENT OF COMMERCE Circular • i op the Bureau of Standards S. W. STRATTON. Director No. 76 ALUMINUM AND ITS LIGHT ALLOYS WASHINGTON GOVERNMENT PRINTING OFFICE DEPARTMENT OF COMMERCE Circular OF THE Bureau of Standards S. W. STRATTON, Director No. 76 ALUMINUM AND ITS LIGHT ALLOYS ISSUED APRIL 21, 1919 4 PRICE, 20 CENTS Sold only by the Superintendent of Documents, Government Printing Office Washington, D. C. WASHINGTON GOVERNMENT PRINTING OFFICE 1919 PREFACE The Bureau is continually in receipt of requests for information concerning the properties, statistics, and manufacture of metals and of alloys, coming from other departments of the Government, technical or purchasing agents of manufacturing firms, or from persons engaged in special investigative work in universities and private technical institutes. Such information is rarely to be form usually the sources of found in systematic ; such information are difficult of access, and their accuracy not always certain. Often quoted information of this sort is valueless, either for the reason that the data upon which it is based are actually incorrect or that they have not been properly interpreted. There are therefore being issued from time to time in response to these demands circulars on individual metals or alloys, with the idea of grouping in these circulars all of the best information which the Bureau has as a result of its tests and investigations, together with that available in all records of published tests and investiga- tions of such material. The circulars deal primarily with the physical properties of the metal or alloy. All other features, except a few statistics of pro- duction and such as methods of manufacture, presence of impurities, etc., are discussed only in their relation to these physical proper- ties.
    [Show full text]
  • Fireworks - Wikipedia, the Free Encyclopedia Page 1 of 17
    Fireworks - Wikipedia, the free encyclopedia Page 1 of 17 Fireworks Learn more about using Wikipedia for research. From Wikipedia, the free encyclopedia A firework is classified as a low explosive pyrotechnic device used primarily for aesthetic and entertainment purposes. The most common use of a firework is as part of a fireworks display. A fireworks event (also called a fireworks show or pyrotechnics) is a display of the effects produced by firework devices on various occasions. Fireworks competitions are also regularly held at a number of places. The biggest fireworks event in the world is held in Madeira, Portugal at the New Years' Eve celebrations, as referred in the Guinness World Records. Fireworks (devices) take many forms to produce the four primary effects: noise, light, smoke, and floating materials (confetti for example). They may be designed to burn with colored flames and sparks. Displays are common throughout the world and Fireworks over Miami, Florida, USA on are the focal point of many different cultural and religious celebrations. American Independence Day Fireworks were originally invented by the Chinese, for entertainment purposes, as a natural extension of the Chinese invention of gunpowder. In China, they were first made by firework masters who were well respected for their knowledge of the many complex techniques used to create truly dazzling firework displays. Such important events and festivities as New Year's and the Mid-Autumn Moon Festival were and still are times when fireworks are guaranteed sights. China is the largest manufacturer and exporter of fireworks in the world. China is estimated to have exported over 6 million cases or 120,000 tons of fireworks to the US in 2005.* Fireworks are generally classified as to where they perform, either as a ground or aerial firework.
    [Show full text]