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Standard X-Ray Diffraction Powder Patterns NATIONAL BUREAU of STANDARDS

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MDC UNIV. of ARIZONA MONOGRAPH 25-SECTION 18 Standard x-ray diffraction powder pattern C 13.44: 25/sec.18 \ VAU o? * 3 9001 90045 6248 U.S. DEPARTMENT OF COMMERCE/ National Bureau of Standards Standard X-ray Diffraction Powder Patterns NATIONAL BUREAU OF STANDARDS The National Bureau of Standards© was established by an act of Congress on March 3, 1901. The Bureau©s overall goal is to strengthen and advance the Nation©s science and technology and facilitate their effective application for public benefit. To this end, the Bureau conducts research and provides: (1) a basis for the Nation©s physical measurement system, (2) scientific and technological services for industry and government, (3) a technical basis for equity in trade, and (4) technical services to promote public safety. The Bureau©s technical work is per formed by the National Measurement Laboratory, the National Engineering Laboratory, and the Institute for Computer Sciences and Technology. THE NATIONAL MEASUREMENT LABORATORY provides the national system of physical and chemical and materials measurement; coordinates the system with measurement systems of other nations and furnishes essential services leading to accurate and uniform physical and chemical measurement throughout the Nation©s scientific community, industry, and commerce; conducts materials research leading to improved methods of measurement, standards, and data on the properties of materials needed by industry, commerce, educational institutions, and Government; provides advisory and research services to other Government agencies; develops, produces, and distributes Standard Reference Materials; and provides calibration services. The Laboratory consists of the following centers: Absolute Physical Quantities2 Radiation Research Thermodynamics and Molecular Science Analytical Chemistry Materials Science. THE NATIONAL ENGINEERING LABORATORY provides technology and technical ser vices to the public and private sectors to address national needs and to solve national problems; conducts research in engineering and applied science in support of these efforts; builds and maintains competence in the necessary disciplines required to carry out this research and technical service; develops engineering data and measurement capabilities; provides engineering measurement traceability services; develops test methods and proposes engineering standards and code changes; develops and proposes new engineering practices; and develops and improves mechanisms to transfer results of its research to the ultimate user. The Laboratory consists of the following centers. Applied Mathematics Electronics and Electrical Engineering* Mechanical Engineering and Process Technology-© Building Technology Fire Research Consumer Product Technology Field Methods. THE INSTITUTE FOR COMPUTER SCIENCES AND TECHNOLOGY conducts research and provides scientific and technical services to aid Federal agencies in the selection, acquisition, application, and use of computer technology to improve effectiveness and economy in Government operations in accordance with Public Law 89-306 (40 U.S.C. 759), relevant Executive Orders, and other directives; carries out this mission by managing the Federal Information Processing Standards Program, developing Federal ADP standards guidelines, and managing Federal participation in ADP voluntary standardization activities; provides scientific and technological advisory services and assistance to Federal agencies; and provides the technical foundation for computer-related policies of the Federal Government. The Institute consists of the following centers; Programming Science and Technology Computer Systems Engineering. Headquarters and Laboratories at Gaithersburg, MD, unless otherwise noted; mailing address Washington, DC 20234. ©Some divisions within the center are located at Boulder, CO 80303. Standard X-ray Diffraction Powder Patterns Section 18 Data for 58 Substances Marlene C. Morris, Howard F. McMurdie, Eloise H. Evans, Boris Paretzkin, Harry S. Parker, and Nicolas C. Panagiotopoulos International Centre for Diffraction Data Camden R. Hubbard National Measurement Laboratory National Bureau of Standards Washington, DC 20234 /,»«« • op c0 jCPDs ^ International Centre for Of "* Diffraction Data U.S. DEPARTMENT OF COMMERCE, Malcolm Baldrige, Secretary NATIONAL BUREAU OF STANDARDS, Ernest Ambler, Director Issued October 1981 Library of Congress Catalog Card Number: 53-61386 National Bureau of Standards Monograph 25 Section 18—Data for 58 Substances Nat. Bur. Stand. (U.S.), Monogr. 25—Sec. 18, 110 pages (Oct. 1981) CODEN: NBSMA6 CONTENTS Page Page Introduction 1 Nickel titanium oxide, NiTi03 .... 54 Potassium fluoride hydrate, KF*2H20 . 55 Experimental patterns: Potassium iron cyanide, K4Fe(CN) 6 . 56 Potassium vanadium oxide, KV03 . 57 Aluminum iron, AIFe .......... Silicon nitride, £-Si 3N4 ...... 59 Ammonium cerium nitrate, Silicon oxide (quartz, low), a-Si02 . 61 (NH4 ) 2Ce(N03 ) 6 .......... 6 Sodium aluminum oxide, p-NaA102 . 62 Ammonium tin fluoride, NH4SnF3 .... 8 Sodium borate, NaB02 ........ 63 Arsenic bromide, AsBr3 ........ 9 Sodium niobium oxide (lueshite), Barium aluminum titanium oxide, NaNb03 .............. 64 Ba 1 .23A1 2.46Ti 5.54°16 ....... 10 Sodium nitrosyl iron cyanide hydrate, Barium manganese oxide, BaMn04 .... 11 Na2 (NO)Fe(CN) 5 -2H20 ....... 66 Barium neodymium titanium oxide, Sodium vanadium oxide, a-NaV03 . 67 BaNd2Ti 30 10 ............ 12 Sodium vanadium oxide, p-NaV03 . 68 Benzidine hydrochloride, Strontium iron oxide, SrFe 1201 9 . 69 C12" 1.2" 2 *2HC1 ........... 14 Thorium carbide, ThC ........ 71 Beryllium nitride, Be3N2 ....... 15 Thorium nitrate hydrate, Bismuth selenide (paraguanajuatite), Th(N03 ) 4 -5H20 .......... 72 Bi 2Se3 ............... 16 Titanium carbide, TiC ........ 73 Calcium borate, CaB204 ........ 17 Tungsten oxide, W02 ......... 74 Calcium cyanamide, CaCN2 ....... 19 Uranium nitride, UN ......... 75 Calcium iron oxide, CaFe204 ...... 20 Uranyl acetate hydrate, C4H606U©2H20 76 Calcium sulfate hydrate (bassanite), Yttrium, Y ............. 77 CaS04 -0.5H20 ............ 22 Zinc acetate hydrate, C4H604Zn©2H20 . 78 Carbamazepine, P~C 15H 12N20 ....... 24 Zirconium fluoride, ZrF4 ...... 79 Cerium niobium oxide Zirconium oxide chloride hydrate, CeNb04 ............... 25 ZrOCl 2 -8H20 ........... 81 Cerium tantalum oxide, CeTa04 ..... 27 Cesium magnesium titanium oxide, Cs 1.45Mg0.724Ti 7,27°16 ...... 29 Cumulative indices Chromium boride, Cr5B3 ......... 30 Cobalt fluoride, CoF2 ......... 31 (Circular 539, Volumes 1-10 and Cobalt phosphide, Co2P ........ 32 Monograph 25, Sections 1-18 inclusive) Copper chloride hydrate (eriochalcite), CuCl2 -2H20 ............. 33 1. Inorganic . 82 lodoform, CHI 3 ............ 34 2. Organic formula 99 Iron boride, FeB ............ 35 3. Organic name 101 Iron fluoride, FeF3 .......... 36 4. Mineral .... 103 Iron oxide (hematite), a-Fe203 .... 37 Iron yttrium oxide, Fe 5Y30 12 ..... 38 Lithium iodide hydrate, LiI*3H20 .... 40 Magnesium phosphate, a-Mg2P20 7 .... 41 Manganese, p-Mn ............ 43 Molybdenum oxide, Mo02 ......... 44 Neodymium tantalum oxide, NdTa04 . 46 Neodymium titanium oxide, Nd2Ti05 . 48 Neodymium titanium oxide, Nd2Ti 2(>7 . 50 Neodymium titanium oxide, Nd4Ti 9024 . 52 iii STANDARD X-RAY DIFFRACTION POWDER PATTERNS Previous work has been published as a book entitled Powder Diffraction Data from the Joint Committee on Powder Diffraction Standards Associateship at the National Bureau of Standards (1976) (JCPDS Inter national Centre for Diffraction Data, 1601 Park Lane, Swarthmore, PA 19081). The volume is sold with an accompnaying search manual, and contains 949 card images of patterns of experimental data, published orig inally as Circular 539 (vols. 1-10) and Monograph 25, Sections 1-12, and most of Section 13. Individual copies of the Circular and Monograph are still available and may be obtained from the National Technical Information Service, 5285 Port Royal Road, Springfield, VA 22161. If a publication listed below is identified with a number, it must be used in ordering. All are available in hardcopy or microfiche; the price is not fixed and will be furnished on request. NBS Publication Number NBS Publication Number Circular 539, Volume 1.............PB 178 902 Monograph 25, Section 1..........PB 178 429 Volume 2.............PB 178 903 Section 2..........PB 178 430 Volume 3.............PB 178 904 Section 3..........PB 178 431 Volume 4.............PB 178 905 Section 4 Volume 5.............PB 178 906 Section 5 Volume 6.............PB 178 907 Section 6 Volume 7.............PB 178 908 Section 7 Volume 8.............PB 178 909 Section 8..........PB 194 872 Volume 9.............PB 178 910 Section 9.........COM 72-50002 Volume 10............PB 178 911 Section 10........COM 72-51079 Section 11........COM 74-50183 Section 12........COM 75-50162 Section 13.........PB 254 073 Section 14.........PB 272 372 Section 15.........PB 287 182 Also, until the present supply is exhausted, the following issues are for sale from the Superinten dent of Documents, U.S. Government Printing Office, Washington, DC 20402. Order by given catalog number, and add 25% to the price for other than U.S. mailing. Catalog Number Price Section 12..........................SN 003-003-01376-5 $1.50 Section 13..........................SN 003-003-01629-2 1.80 Section 14..........................SN 003-003-01842-2 2.75 Section 15..........................SN 003-003-01986-1 4 00 Section 16..........................SN 003-003-02128-8 5 00 Section 17..................
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