Development of Innovative Gas- Assisted Foam Injection Molding
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Polymers and Supercritical
Polymers and Supercritical CO2 - An invention to new polymer processing technologies - On-line Number 5017 Masahiro Ohshima Department of Chemical Engineering, Kyoto University, Nishikyo-ku, Kyoto, 615-8510, Japan E-mail: [email protected] ABSTRACT Supercritical CO2 (sc-CO2) is being utilized for various polymers processing such as polymer blending, additive impregnation and plastic foaming. When CO2 dissolves into polymers, the polymer chain mobility is enhanced and rheological and thermal properties of the polymer are changed. In this talk, the solubility and the diffusivity of CO2 in the polymer as well as the CO2-induced polymer property (i.e., plasticization effects), such as reduction of glass transition temperature and viscosity, are shown with experimental data. Then, CO2 microcellular polymeric foaming, a CO2 aided additive infusion and polymer surface modification schemes are introduced to illustrate the potential of CO2 creating new polymer processing techniques. KEYWORDS Super critical fluid, carbon dioxide, plasticization effect, polymer, foams, and surface modification INTRODUCTION Carbon dioxide (CO2) becomes supercritical at pressures and temperatures above 7.38 MPa and o 31.1 C. At the supercritical condition, the CO2 has a higher diffusion coefficient and a lower viscosity than liquids and the surface tension becomes absent, which allows a rapid penetration of molecule into the pores of heterogeneous matrices. Taking advantage of these characteristics together with its nontoxicity, nonflammability and inexpensiveness, CO2 has been used in a variety of industries, i.e., food, pharmaceutical, fiber, chemical and plastic industries (Berens et al, 1992; Schnitzler et al, 1999). At the beginning of the research on the supercritical fluids, the focus was mainly on extraction and separation of small molecules by the fluids. -
Processing and Characterization of Polycarbonate Foams with Supercritical
PROCESSING AND CHARACTERIZATION OF POLYCARBONATE FOAMS WITH SUPERCRITICAL CO2 AND 5-PHENYL-1H-TETRAZOLE Thomas Cloarec, B.S. Thesis Prepared for the Degree of MASTER OF SCIENCE UNIVERSITY OF NORTH TEXAS May 2015 APPROVED: Witold Brostow, Major Professor Samir Aouadi, Committee Member Nandika A. D’Souza, Committee Member Richard F. Reidy, Committee Member Cloarec, Thomas. Processing and Characterization of Polycarbonate Foams with Supercritical Co2 and 5-Phenyl-1h-Tetrazole. Master of Science (Materials Science and Engineering), May 2015, 100 pp., 11 tables, 59 figures, references, 5 titles. Since their discovery in the 1930s, polymeric foams have been widely used in the industry for a variety of applications such as acoustical and thermal insulation, filters, absorbents etc. The reason for this ascending trend can be attributed to factors such as cost, ease of processing and a high strength to weight ratio compared to non-foamed polymers. The purpose of this project was to develop an “indestructible” material made of polycarbonate (PC) for industrial applications. Due to the high price of polycarbonate, two foaming methods were investigated to reduce the amount of material used. Samples were foamed physically in supercritical CO2 or chemically with 5-phenyl-1H-tetrazole. After thermal characterization of the foams in differential scanning calorimetry (DSC), we saw that none of the foaming methods had an influence on the glass transition of polycarbonate. Micrographs taken in scanning electron microscopy (SEM) showed that foams obtained in physical and chemical foaming had different structures. Indeed, samples foamed in supercritical CO2 exhibited a microcellular opened-cell structure with a high cell density and a homogeneous cell distribution. -
Type of the Paper
polymers Review Tuning Power Ultrasound for Enhanced Performance of Thermoplastic Micro-Injection Molding: Principles, Methods, and Performances Baishun Zhao 1,2 , Yuanbao Qiang 1,2, Wangqing Wu 1,2,* and Bingyan Jiang 1,2 1 State Key Laboratory of High-Performance Complex Manufacturing, Central South University, Lushan South Road 932, Changsha 410083, China; [email protected] (B.Z.); [email protected] (Y.Q.); [email protected] (B.J.) 2 School of Mechanical and Electrical Engineering, Central South University, Lushan South Road 932, Changsha 410083, China * Correspondence: [email protected]; Tel.: +86-158-7429-5500 Abstract: With the wide application of Micro-Electro-Mechanical Systems (MEMSs), especially the rapid development of wearable flexible electronics technology, the efficient production of micro-parts with thermoplastic polymers will be the core technology of the harvesting market. However, it is significantly restrained by the limitations of the traditional micro-injection-molding (MIM) process, such as replication fidelity, material utilization, and energy consumption. Currently, the increas- ing investigation has been focused on the ultrasonic-assisted micro-injection molding (UAMIM) and ultrasonic plasticization micro-injection molding (UPMIM), which has the advantages of new Citation: Zhao, B.; Qiang, Y.; Wu, W.; plasticization principle, high replication fidelity, and cost-effectiveness. The aim of this review is Jiang, B. Tuning Power Ultrasound to present the latest research activities on the action mechanism of power ultrasound in various for Enhanced Performance of polymer micro-molding processes. At the beginning of this review, the physical changes, chemical Thermoplastic Micro-Injection changes, and morphological evolution mechanism of various thermoplastic polymers under different Molding: Principles, Methods, and application modes of ultrasonic energy field are introduced. -
FY 1992 Budget Summary Table for DOE Materials Activities
Is a.:. S A * A A 0 0 - 0@ E a a A - a 5 0O I.. - 0 - 0 S -. -. C S -. :. -. B S S --. - This report has been reproduced directly from the best available copy. Available to DOE and DOE contractors from the Office of Scientific and Technical Informa- tion, P.O. Box 62, Oak Ridge, TN 37831; prices available from (615) 576-8401, Available to the public from the National Technical Information Service, U.S. Department of Commerce, 5285 Port Royal Rd., Springfield, VA 22161. 0 Printed with soy ink on recycled paper DOE/ER-0589 ENERGY MATERIALS COORDINATING COMMITTEE (EMaCC) Fiscal Year 1992 May 1993 Annual Technical Report U.S. Department of Energy Office of Energy Research Office of Basic Energy Sciences Division of Materials Sciences Washington, D.C. 20585 Table of Contents TABLE OF CONTENTS Page Introduction ........................................................ 1 Membership List .................................................... 2 FY 1992 Budget Summary Table for DOE Materials Activities .................. 6 Program Descriptions OFFICE OF ENERGY EFFICIENCY AND RENEWABLE ENERGY ......... 9 Office of Building Technologies ................................... 13 Office of Building Energy Research .............................. 14 Buildings Systems and Materials Division ........................ 15 Office of Industrial Technologies .................................. 17 Office of Waste Reduction Technologies ........................... 21 Industrial Energy Efficiency Division ............................ 21 Waste Material Management Division -
Micro-Nanostructured Polymer Surfaces Using Injection Molding: a Review K
View metadata, citation and similar papers at core.ac.uk brought to you by CORE provided by Constellation Micro-Nanostructured Polymer Surfaces Using Injection Molding: A Review K. Maghsoudi*, R. Jafari, G. Momen, M. Farzaneh Department of Applied Sciences, University of Quebec in Chicoutimi (UQAC) 555, boul. de l'Université, Chicoutimi, Quebec, G7H 2B1, Canada * E-mail: [email protected] Abstract Micro injection molding is in great demand due to its efficiency and applicability for industry. Polymer surfaces having micro-nanostructures can be produced using injection molding. However, it is not as straightforward as scaling-up of conventional injection molding. The paper is organized based on three main technical areas: mold inserts, processing parameters, and demolding. An accurate set of processing parameters is required to achieve precise micro injection molding. This review provides a comparative description of the influence of processing parameters on the quality of final parts and the precision of final product dimensions in both thermoplastic polymers and rubber materials. It also highlights the key parameters to attain a high quality micro-nanostructured polymer and addresses the contradictory effects of these parameters on the final result. Moreover, since the produced part should be properly demolded to possess a high quality textured polymer, various demolding techniques are assessed in this review as well. Keywords: injection molding; micro-nanostructure; processing parameters; demolding; replication 1. Introduction Among the different polymer processing techniques used to produce materials having a specifically desired size and shape, injection molding is highly preferred for mass production systems, and has been used for many years in the polymer industry 1-2. -
(12) United States Patent (10) Patent No.: US 8,827,197 B2 Powers (45) Date of Patent: Sep
USOO8827 197B2 (12) United States Patent (10) Patent No.: US 8,827,197 B2 POWers (45) Date of Patent: Sep. 9, 2014 (54) APPARATUS AND METHOD FOR (56) References Cited INTERLEAVING POLYMERIC ROLL FOR GAS IMPREGNATION AND SOLD-STATE U.S. PATENT DOCUMENTS FOAMI PROCESSING 1948,568 A 2f1934 Faber 2,224,997 A * 12/1940 Weisse ....................... 242/.530.2 (75) Inventor: Steven Ray Powers, Everett, WA (US) (Continued) (73) Assignee: MicroGREEN Polymers Inc, Arlington, WA (US) FOREIGN PATENT DOCUMENTS (*) Notice: Subject to any disclaimer, the term of this E. 36 A1 8.8 patent is extended or adjusted under 35 U.S.C. 154(b) by 1305 days. (Continued) OTHER PUBLICATIONS (21) Appl. No.: 12/612,652 Wang, "Solvent-free Fabrication of Porous Polymer for Tissue Engi (22) Filed: Nov. 4, 2009 neering Applications.” University of Washington, Dept. of Mechani cal Engineering (dissertation), 2007. (65) Prior Publication Data US 2010/01 12301A1 May 6, 2010 (Continued) Related U.S. Application Data Primary Examiner — William A Rivera (60) Provisional application No. 61/111.298, filed on Nov. R Attorney, Agent, or Firm — John M Janeway; Janeway atent Law PLLC 4, 2008. (51) Int. Cl. (57) ABSTRACT B65H (8/08 (2006.01) The present invention relates to apparatuses and methods for B32B 37/00 (2006.01) making interleaved cylindrical rolls from a polymer roll and a B65H 39/6 (2006.01) porous roll. The interleaved rolls disclosed herein are useful B32B I/08 (2006.01) for Subsequent high pressure gas impregnation and solid-state B32B 27/2 (2006.01) foam processing. -
Development of High Strength Microcellular
DEVELOPMENT OF HIGH STRENGTH MICROCELLULAR FOAMS USING POLYETHER BLOCK AMIDE ………………….. KUN LIN ………………….. M.Eng. PROJECT REPORT DEPARTMENT OF MECHANICAL AND INDUSTRIAL ENGINEERING UNIVERSITY OF TORONTO 2010 DEVELOPMENT OF HIGH STRENGTH MICROCELLULAR FOAMS USING POLYETHER BLOCK AMIDE by KUN LIN A thesis submitted in conformity with the requirements for the degree of Masters of Engineering Graduate Department of Mechanical and Industrial Engineering University of Toronto © Copyright by Kun Lin (2010) Development of High Strength Microcellular Foams Using Polyether Block Amide M.Eng. 2010-09-15 Kun Lin Department of Mechanical & Industrial Engineering University of Toronto Abstract This report presents a successful development of batch foaming techniques of the engineering elastomer. The polyether block amide (PEBAX) was investigated as an engineering elastomer by using batch foaming techniques. The Pebax provide a unique combination of mechanical and chemical properties. Understanding the effect of the different parameter in batch foaming process allows obtaining the high quality foamed product of the engineering elastomer. Temperature has been considered as an important parameter in the batch foaming process. It was shown that the density of foamed product was decreasing by the temperature increasing under its melting temperature. Both temperature and pressure have to reach the minimum requirement to obtain the fine foamed product. As an experiment result, it indicates that there is an optimal portfolio of foaming parameter for the different Pebax resin. Acknowledgements I would like to thank my supervisor Professor Chul B. Park, who provided me this opportunity and resources to complete this research project. I would like to thank my co- supervisor Nan Chen for his guidance, supports and encouragements during my research. -
The Micro Injection Moulding Process for Polymeric Components Manufacturing
4 The Micro Injection Moulding Process for Polymeric Components Manufacturing R. Surace, G. Trotta, V. Bellantone and I. Fassi ITIA-CNR, Institute of Industrial Technology and Automation, National Research Council, Italy 1. Introduction In recent years, there is an increasing demand for small and even micro scale parts and this trend towards miniaturization makes the micro system technologies of growing importance. Microfabrication process capabilities should expand to encompass a wider range of materials and geometric forms, by defining processes and related process chains that can satisfy the specific functional and technical requirements of new emerging multi-material products, and ensure the compatibility of materials and processing technologies throughout these manufacturing chains. Example technologies to be investigated either individually or in combination are technologies for direct- or rapid manufacturing, energy assisted technologies, microreplication technologies, qualification and inspection methods, functional characterisation methods and integration of "easy and fast" on-line control systems. The processes should demonstrate significantly high production rates, accuracy and enhanced performance or quality, creating capabilities for mass manufacture of microcomponents and miniaturised parts incorporating micro- or nanofeatures in different materials. Processes should also provide high flexibility and seamless integration into new micro- and nanomanufacture scenario. Micro- and nano-manufacturing technologies can provide the basis of the next industrial revolution that could dramatically modify the way in which businesses are setup, run and marketed. Micro injection moulding can be defined as one of the key technologies for micro manufacturing because of its mass production capability and relatively low production cost. It is the process of transferring the micron or even submicron features of metallic moulds to a polymeric product. -
Injection and Micro Injection of Polymeric Plastics Materials: a Review
International Journal of Modern Manufacturing Technologies ISSN 2067–3604, Vol. V, No. 1 / 2013 INJECTION AND MICRO INJECTION OF POLYMERIC PLASTICS MATERIALS: A REVIEW Ciprian Ciofu, Daniel Teodor Mindru “Gheorghe Asachi” Technical University of Iasi-Romania, Department of Machine Manufacturing Technology Blvd. D. Mangeron No. 59A, 700050 Iasi, Romania Corresponding author: Ciprian Ciofu, [email protected] Abstract: The explosive development of plastics warpage and comparison of fibre orientation industry due, on one hand the emergence of many distribution. Specific properties of plastics products new polymers with very different characteristics, on allow a high quality and high reliability to use in the other hand improves their processing various industrial fields such as electronic technologies. Injection and micro-injection with engineering, aerospace and automotive industry, extruder, calendaring, are the main training electrical industry, food industry, industry objects techniques for plastics.Injection molding is the most household etc. popular method for producing plastic products Key words: injection, micro-injection, polymeric- because of its high productivity and the plastics materials, finite element analise manufacturability for making various complex shapes also is a widely used, complex but highly efficient 1. INTRODUCTION technique for producing a large variety of plastic products, particularly those with high production Plastics are made from polymers and are produced in requirement, tight tolerance and complex shapes. the temperature at which they become plastic in order The paper begins with an introduction on the to obtain the finished product. Polymer evolution of obtaining and processing of plastics by macromolecules are composed of groups of atoms injection and follow with injection and micro- that are repeated more or less ordered along the injection process presentation with issues such as: chain. -
Flame Retardants for ABS and ABS-Matrix Wood-Plastic Composites
Graduate Theses, Dissertations, and Problem Reports 2008 Flame Retardants for ABS and ABS-matrix Wood-Plastic Composites Tze-Wei Liu West Virginia University Follow this and additional works at: https://researchrepository.wvu.edu/etd Recommended Citation Liu, Tze-Wei, "Flame Retardants for ABS and ABS-matrix Wood-Plastic Composites" (2008). Graduate Theses, Dissertations, and Problem Reports. 4397. https://researchrepository.wvu.edu/etd/4397 This Dissertation is protected by copyright and/or related rights. It has been brought to you by the The Research Repository @ WVU with permission from the rights-holder(s). You are free to use this Dissertation in any way that is permitted by the copyright and related rights legislation that applies to your use. For other uses you must obtain permission from the rights-holder(s) directly, unless additional rights are indicated by a Creative Commons license in the record and/ or on the work itself. This Dissertation has been accepted for inclusion in WVU Graduate Theses, Dissertations, and Problem Reports collection by an authorized administrator of The Research Repository @ WVU. For more information, please contact [email protected]. Flame Retardants for ABS and ABS-matrix Wood-Plastic Composites Tze-Wei Liu Dissertation submitted to the College of Engineering and Mineral Resources At West Virginia University in partial fulfillment of the requirements for the degree of Doctor of Philosophy in Chemical Engineering Rakesh K. Gupta, Ph.D. Eung H. Cho, Ph.D. Caulton Irwin, Ph.D. Edwin L. Kugler, Ph.D. John Zondlo, Ph.D. Department of Chemical Engineering West Virginia University Morgantown, West Virginia 2008 Keywords: flame retardants, non-halogenated flame retardants, polymer recycling, acrylonitrile-butadiene-styrene, wood plastic composites, char formation, FTIR, flammability, thermal degradation. -
Effective Use of Filling Simulations to Balance Hot
Society of Plastics Engineers 6666tthh AAnnnnuuaall TTeecchhnniiccaall CCoonnffeerreennccee ooff tthhee SSoocciieettyy ooff PPllaassttiiccss EEnnggiinneeeerrss Plastics Encounter at ANTEC 2008 May 4 – 8, 2008 Milwaukee, Wisconsin, USA Volume 1 of 4 Printed from e-media with permission by: Curran Associates, Inc. 57 Morehouse Lane Red Hook, NY 12571 www.proceedings.com ISBN: 978-1-60560-320-9 Some format issues inherent in the e-media version may also appear in this print version. COPYRIGHTED © 2008 BY THE SOCIETY OF PLASTICS ENGINEERS. PO BOX 403, BROOKFIELD, CONNECTICUT 06804-0403 REPRODUCTION IN WHOLE OR IN PART WITH OUT WRITTEN PERMISSION IS PROHIBITED. Society of Plastics Engineers 66th Annual Technical Conference of the Society of Plastics Engineers 2008 TABLE OF CONTENTS VOLUME 1 AUTOMOTIVE – D31 AUTOMOTIVE DIVISION INTERACTIVE SESSION POLYMER FLOW ANALYSIS ON AN AUTOMOTIVE INSTRUMENT PANEL.................................. 1 Bhagat, Harsh COMPOSITES – D39 COMPOSITE PROCESSING AND APPLICATION SELF-REINFORCING THERMOPLASTIC COMPOSITES ................................................................. 6 Lesser, Alan; McCarthy, Thomas; Yoon, Joonsung HYDROXYAPATITE- POLYLACTIDE COMPOSITE FOR BONE REPAIR...................................... 11 Olson, James; Shaw, Montgomery; Sun, Shih-Po; Wei, Mei STRUCTURAL REINFORCED INJECTION MOLDING OF FIBERGLASS AND POLYDICYCLOPENTADIENE........................................................................................................... 14 Hoekstra, Nicole; Lao, Edward IMPROVING WATER RESISTANCE -
Microinjection Molding of Microsystem Components: New Aspects in Improving Performance
IOP PUBLISHING JOURNAL OF MICROMECHANICS AND MICROENGINEERING J. Micromech. Microeng. 23 (2013) 093001 (21pp) doi:10.1088/0960-1317/23/9/093001 TOPICAL REVIEW Microinjection molding of microsystem components: new aspects in improving performance Can Yang1, Xiao-Hong Yin and Guang-Ming Cheng Laboratory for Advanced Material Processing, Zhejiang Normal University, Jinhua, Zhejiang, 321004, People’s Republic of China E-mail: [email protected] Received 17 March 2013, in final form 17 May 2013 Published 1 August 2013 Online at stacks.iop.org/JMM/23/093001 Abstract Microinjection molding (μIM) is considered to be one of the most flexible, reliable and cost effective manufacturing routes to form plastic micro-components for microsystems. The molding machine, mold tool fabrication, material selection and process controlling in this specific field have been greatly developed over the past decades. This review aims to present the new trends towards improving micro-component performance by reviewing the latest developments in this area and by considering potential directions. The key concerns in product and mold designing, essential factors in simulation, and micro-morphology and resultant properties are evaluated and discussed. In addition, the applications, variant processes and outlook for μIM are presented. Throughout this review, decisive considerations in seeking improved performance for microsystem components are highlighted. (Some figures may appear in colour only in the online journal) 1. Introduction required in certain applications. Since the 1990s, polymer materials have been increasingly incorporated into MEMS Micro-electromechanical-systems (MEMS) or microsystem industries. An important reason is that they provide not only technology (MST) has already become a familiar part of controllable thermal, mechanical and electrical properties, but our daily life in that various micro-components can be also unique chemical, structural and biological functionalities found in a number of devices such as laptops, microphones, not available in any other material.