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EPSILON CARBON PRIVATE LIMITED ECPL CoalTar Distillation -300,000tpa Karnataka

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General TheEpsilon CarbonprivateLimited is aspiring to emergeasadynamiccompanyin India in the field of processing for manufacture ofvarious value added products.

The proposed green-field Coal tar distillation plant coupledwith solidpitchmeltingunitisproposedtosetupwith Coal tar processing capacity of 300,000tpaat Toranagallu in Bellary district of Karnataka.

Process Description: The coal tar are separated by distillation process. Coal tar containing several chemical compounds with major being Coal tar ,,Wash Oil, Light Oil, Oil & oil. Following are major manufacturing of process & Products: 1. Coal Tar pitch (Binder Grade Pitch) 2. Zero QI /Impregnated Pitch 3. Naphthalene &Naphthalene sulfonate formaldehyde (NSF) 4. Oils- Oil (CBO) ,Light oil, Phenol oil, Wash oil , Anthracene oil By Products: 5. Sodium Phenolate 6. Ammonical water

1. Binder Grade Pitch: Soft Pitch from the bottom of pitch column is sent to pitch column for further processing to modified pitch to increase QI content and blended with required high QI pitch to produce binder grade pitch for aluminum industry.

2. Impregnated Pitch : Blending of coal tar and wash oil in specific ratio, dehydration up to 180℃ to separate moisture content in coal tar. The dehydrated mixture is transferred to settling tank for reduction of QI. (Settling tank provide draw-off valve for QI sampling). QI value less material transfer to further distillation (Removal of Oils) to produce Impregnated Pitch.

Project Profile for 300,000 tpa Coal Tar Distillation plant EPSILON CARBON PRIVATE LIMITED ECPL CoalTar Distillation -300,000tpa Karnataka

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3. Carbon Black Oil(CBO): Blending of Soft Pitch from the bottom of pitch column and Anthracene oil in specific ratio with required specific gravity to produce carbon black oil for tyre industry.

4. Naphthalene &Naphthalene sulfonate formaldehyde (NSF) Three mixed oil fraction from distillation column is mixed with dilute alkali and treated in washing separating towers. The phenol fraction forms Sodium Phenolate which passes to aqueous layer as a byproduct. The washed fraction is further distilled in naphthalene columns to obtain wash oil & crude naphthalene. The crude naphthalene oil is further crystallizedto pure naphthalene. During Crystallization process residual naphthalene oil is generated which is treated with Sulphuric acid (Sulfonation Reaction), followed by formaldehyde (Condensation) and further neutralized by sodium hydroxide to produce naphthalene sulfonated formaldehyde. (NSF).

5. Oils- Light oil,Phenol oil & Anthracene oil Tar is pumped through pre heaters and fed to dehydration column in which azeotropic distillation takes to remove Light oil and moisture content in the tar from the top of column. Light oil & moisture is further separated in a separator to obtain pure light oil. Dehydrated tar from the bottom of dehydration column is pumped to pitch column. The overhead vapor from pitch column flow to the distillation column in which they are separated the top fraction contains phenol oil, the middle fraction contains naphthalene oil along with and wash oil & the bottom product contains Anthracene oil.

Project Profile for 300,000 tpa Coal Tar Distillation plant EPSILON CARBON PRIVATE LIMITED ECPL CoalTar Distillation -300,000tpa Karnataka

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PROCESS BLOCK DIAGRAM 3, 00,000 tpa COAL TAR DISTILLATION PLANT

A. Process Flow Diagram for coal Tar distillation

LIGHT OIL & NAPHTHALENE CRYSTALLIZERS KETTLE MOISTURE OIL

PHENOL OIL

COAL TAR DEHYDRATIO PITCH NAPHTHALENE COAL FLAKER N.S.F. TAR STORAGE N COLUMN COLUMN COLUMN TANK DISTILLATION COLUMN

HIGH QI PITCH PITCH PITCH PITCH MELTER REACTOR BLENDER ANTHRACENE WASH OIL NAPHTHALENE OIL

Liquid Binder Solid Binder CARBON Grade Pitch Grade Pitch BLACK OIL

B. Process Flow Diagram for Zero QI /Impregnated pitch

LIGHT OIL Crude & Naphthalen MOISTURE e COAL TAR

Solid Distillation Dehydratio Settling Impregnated n Pitch (Zero QI) Heavy Oil

Heavy Oil COAL TAR

Project Profile for 300,000 tpa Coal Tar Distillation plant