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Ldrd Project Summaries Idaho National Laboratory ANNUAL REPORT FY 2013 LDRD PROJECT SUMMARIES Acknowledgments This annual report provides an overview of the Laboratory Directed Research and Development (LDRD) Program at Idaho National Laboratory (INL). Summarized in this report are 89 technical research projects conducted in FY 2013. The LDRD Program at INL is managed for the Laboratory by John J. Grossenbacher, Laboratory Director; Todd Allen, Deputy Laboratory Director for Science and Technology; and Anita Gianotto, LDRD Program Manager. Many people contributed to this report; however, particular thanks go to the principal investigators who conduct the cutting-edge research so important to this laboratory. Managing Editor: Dena Tomchak Technical Writing and Quinn Grover Editing: Riley Goodwin Text Processing: Cheryl Priest Cover Design: Kris Burnham Prepared for the U.S. Department of Energy Director, Nuclear Energy, Science & Technology Under DOE Idaho Operations Office Contract Number: DE-AC07-05ID14517 Disclaimer This report was prepared as an account of work sponsored by an agency of the United States Government. Neither the United States Government nor any agency thereof, makes any warranty, express or implied, or assumes any legal liability or responsibility for the accuracy, completeness, or usefulness of any information, apparatus, product, or process disclosed, or represents that its use would not infringe privately owned rights. Reference herein to any specific commercial product, process, or service by trade name, trademark, manufacturer, or otherwise does not necessarily constitute or imply its endorsement, recommendation or favoring by the United States Government or any agency thereof. The views and opinions of authors expressed herein do not necessarily state or reflect those of the United States Government or any agency thereof. iii CONTENTS SECTION 1 NUCLEAR SCIENCE AND TECHNOLOGY 11-000 – Haptic Tele-Operated End Effector for Hazardous Environments ............................................................. 2 11-005 – Speciation Behavior of Americium Oxidation States for the Separation of Americium from Curium in Nuclear Processing ................................................................................................................... 6 11-023 – Development of a Simplified Soft Donor Technique for Trivalent Actinide/Lanthanide Separations ......... 9 11-051 – Alternative Processing for Improved UO2 Based Fuels ........................................................................... 13 11-055 – Spatially Resolved Positron Analysis of Hydride Formation in LWR Fuels with GE-Global Nuclear Fuels ........................................................................................................................................... 18 11-061 – Advanced Modeling and Simulation Concepts for ATR ........................................................................... 21 12-031 – 2-D and 3-D EBSD Technique Development and Microstructure Reconstruction for Phase Field Microstructure Evolution Models .............................................................................................................. 28 12-045 – Development of an Uncertainty Quantification Method for MIR Facility .................................................. 31 12-061 – Development of a High Burnup Zr-Based Fuel Cladding for LWRs ......................................................... 35 12-062 – Development of Diamond Based Sensors for User Facility Capabilities at INL Advanced Test Reactor ............................................................................................................................................ 37 12-070 – Separate Effects Fuels Development Capability ...................................................................................... 39 12-112 – Reactor Coolant Pump Alternate Can Material Development Program ................................................... 42 12-117 – Feasibility of a Broad Application Test Reactor Using LEU ..................................................................... 44 13-013 – Development of a Micromechanistic Phase-Field Modeling Approach for Life Estimation and Risk Assesment of Reactor Pressure Vessels ........................................................................................ 49 13-014 – Aluminium Electroplating from Low Temperature Molten Bromide Salts ................................................. 52 13-023 – Characterization and Modeling of High Burn-up Mixed Oxide Fuel ......................................................... 54 13-029 – In-Pile Detection of Crack Growth in the ATR .......................................................................................... 57 13-032 – Experimental and Computational Analysis of Hydride Microstructures in Zirconium in Dry Storage Conditions .................................................................................................................................. 61 13-039 – Induction Based Fluidics Mass Spectrometry for Characterizing Radioactive Extraction Solvents ......... 63 13-040 – Epistemic Uncertainty Quantification in Dynamic Probabilistic Risk Assessment ................................... 65 13-050 – Concurrent Atomistic to Macroscale Modeling of Materials Under Irradiation Using the Phase Field Crystal Model .................................................................................................................................. 67 13-071 – Advanced Fracture Modeling for Nuclear Fuel ......................................................................................... 69 13-097 – MOOSE Capability Extension In Support of Full Core Modeling ............................................................. 71 13-115 – Multi-scale Full Core Reactor Physics Simulation .................................................................................... 73 iv 13-121 – Advanced In-Situ Measurement Techniques in TREAT .......................................................................... 77 13-123 – Experimental Verification of Predicted Chemical Transmutation of Cesium-137 to Barium-137 via Beta Decay in CsCl Resulting in the Radioparagenetic Formation of Rocksalt BaCl ...................................... 80 SECTION 2 NATIONAL AND HOMELAND SECURITY 11-042 – Experimental Cyber Security: Vulnerability Prediction, Discovery, and Mitigation .................................. 83 11-059 – Unconventional Radiation Detection Methods for Nuclear Nonproliferation, Safeguards, and Treaty Verification ............................................................................................................................. 87 11-060 – SMC Advanced Armor Materials and Systems R&D ............................................................................... 90 12-001 – Long Term Evolution Wireless Cyber Security ......................................................................................... 92 12-017 – Polymer Components in Laminate Armor Systems for Ballistic Protection ............................................. 94 12-050 – Cross Section Representations for Nuclear Nonproliferation .................................................................. 96 12-054 – Treaty Verification with Photo-Induced Prompt Signatures ..................................................................... 98 12-066 – Electronic Energetic Initiation ................................................................................................................. 100 12-073 – A Nonproliferation Focused Study and Comparison of the GEANT4 Simulation Toolkit and MCNP Functionality, Accuracy, and Development Needs .................................................................... 102 13-060 – Metal Fluoride Preparation for AMS Analysis ........................................................................................ 105 13-092 – Fission Product Standard Production ..................................................................................................... 107 13-093 – Spectrum Allocation and Communications in Dynamic Spectrum Access Channels ............................ 109 13-118 – Geomagnetic Disturbance Field Coupling Measurements on INL Power Grid ...................................... 111 SECTION 3 ENERGY & ENVIRONMENT SCIENCE AND TECHNOLOGY 11-007 – Integration of Renewable Energy Resources through Energy Storage and SuperGrid......................... 115 12-093 – Development of Unique Nanomaterials for Selective Replacement of Strategic and Critical Materials .................................................................................................................................... 119 12-096 – Isolation and Purification of Critical Metals Using Ionic Liquid Based Solvent Extraction ..................... 123 12-099 – Designing Algal Biofuel Consortia for Increased Function and Reduced Nutrient Costs ...................... 125 12-108 – Bakken Hydraulic Fracturing Water Needs and Potential Impacts to the Fox Hills/ Hell Creek Aquifer .................................................................................................................................. 128 12-113 – Coupled-Smoothed Particle Hydrodynamics and Discrete Element Model (SPH-DEM) Simulation of Hydraulic Fracturing and Shale Gas Production ............................................................. 131 12-118 – A Leap Ahead in Energy Storage – An Integrated Approach to an Inorganic High Energy Lithium Battery ......................................................................................................................................
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