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RECE/Vfo JUN ~-; 1948 CAMPAIGN ANALYSIS REPORT GEN'L CH£M:ul ' I C Loveland Factory . o. The Great Western Sugar Company Campaign 1947-48

Copies to: • ., , IS .. General Chemist Colorado District Engineer, Superintendent Laboratory

May 26, 1948 Chief Chemist ------INDEX

Sheet No. 1 City WateJr 2 Ditch Water

3 Battery Supply Water 4 Press Wash Water 5 Water used to wash 'White sugar 6 Water used to wash cold saccharate

7 Water in Boiler Feed Tank 8 Condensed water pumped direct to boilers

9 Water in BoilerE Form 443-2M-7-41-Pads 100

WATER ANALYSIS

-·-···-·····-·l,QJ(EWD·-·····-······-·-··-·-·Factory ···-·-·-·Campaign ...... -... 19.47 .. ~-.1948__ ..

Kind of Water: Cit7 lfatett Description of Sample: Campaign average sample composed of three catch samples, per week.

Source of Water: Big Thompson River, about eight miles wes.t of factory.

ANALYSIS HYPOTHETICAL COMBINATIONS 4 PartsPer~• Parts Per~ Silica SiO, Silica SiO, 6~6 Iron Fe Chloride NaCl 3.6 Ca Na,SO, 6.7 Mg Sodium Na.CO, 7.6 Sodium Na Sodium Na,PO, 0 Chlorine CI MgCl2 0 Sulfuric so. MgSO. 0 Carbonic Acid CO, MgCO, 12.1 PO, Magnesium Phosphate Mg,(PO,). 0 Calcium Sulfate CaSO, 0 CaCO, 1.0 Calcium Phosphate Ca,(PO,). 0 Ferrous Carbonate FeCOa 1.7 Ferrous Phosphate Fe,(PO,), 0

pH - a.o

COPIES TO General Supt. General Chemist Asst. General Supt. District Engineer Superintendent Laboratory (1) d4ef~a,N(/ •...... L ..... J ._.,, ...... , ______,,.. _ ... , ...... _ Chief Chemlat. J<'orm 443-2M- 7-41-Pads 100

WATER ANALYSIS

______.LOiEEAND...... Factory ...... 9.~~gg...... 19.h?.~...... 194.~---

Kind of Water: Ditch Water· Description of Sample: Campaign average sample composed of three catch samples: per week.

Source of Water: Loveland and Cemetery Lakes.

ANALYSIS HYPOTHETICAL COMBINATIONS P.P.M. P.P.11 Parts llel,,,i.Qll,Aill Paris Per MMlpOIMI- Silica Si01 13.e Silica SiO, 13.8 Iron Fe 1.7 NaCl 1,.2: Calcium Ca 58.6 Sodium Sulfate Na.SO, 44.2. Magnesium Mg 22~ Na.CO, Sodium Na 20.3 Sodium Phosphate Na,PO, Chlorine Cl 9.2 Magnesium Chloride MgCI. Sulfuric Acid so. 184.5 Magnesium Sulfate MgSO, 109.9 Carbonic Acid co, 47.8 Magnesium Carbonate MgCO, Phosphoric Acid PO, Magnesium Phosphate Mg,(PO,), Calcium Sulfate CaSO, Calcium Carbonate CaCO, Calcium Phosphate Ca,(PO,), Ferrous Carbonate FeCO. Ferrous Phosphate Fe,(PO,).

358.l. Organic and Volatile (by difference) 60.B Organic and Volatile (by difference)

___ issolve ; SOLIDS AT 105° C 8 0 2__ ._ _ _...!issJll.'ei 'WIBIXSOLIDS AT 105° C pH 8.2

COPIES TO General Supt. General Chemist Asst. General Supt. District Engineer Superintendent Laboratory (2) ...... d~~~~·-··············-ChlefChnrlat. F'orm 443- 2M- 7-41-Pads 100 . . ..

WATER ANALYSIS

---·······-IDV.EUfilt ...... -...... -._···Factory ··------····-··C.ampaign.. ..l9.h7 ... ~ ... -...1948 _...

Kind Qf Water: Battery Supp~ Water' Description of Sample: Campaign average sample composed of three catch sample&. per week.

Source of Water: Overflow from press wash water tanks, city water, No. 1 and 2 white pan condensers .and make up water from seal tanks, drips from 1st effects of evaporators.

ANALYSIS HYPOTHETICAL COMBINATIONS Parts Per!~·m Parts p..,.P~• Silica SiO, Silica SiO, Iron Fe Sodium Chloride NaCl Calcium Ca Sodium Sulfate Na,SO, Magnesium Mg Sodium Carbonate Na.CO, Sodium Na Sodium Phosphate Na,PO, Chlorine Cl Magnesium Chloride MgCl, Sulfuric Acid SO, Magnesium Sulfate MgSO, Carbonic Acid co. Magnesium Carbonate MgCOa Phosphoric Acid PO, Magnesium Phosphate Mg,(PO,), Calcium Sulfate CaSO, Calcium Carbonate CaCO, Calcium Phosphate Ca,(PO,). Ferrous Carbonate FeCO. Ferrous Phosphate Fe,(PO,).

Organic and Volatile (by difference) Organic and Volatile (by difference) ___.w :.i.SSW.Ye_, , DX'U, SOLIDS AT 105° C Dissolved ~ SOLIDS AT 105° C

COPIES TO General Supt. General Chemist Asst. General Supt. District Engineer Superintendent Laboratory ...... &4/# ~ ...... Chief Chemist. (3) .l!'orm 443-2M- 7-41- Pads 100

• If' I ,

WATER ANALYSIS

______.LCNEI.AND ...... _ ____ .Factory -- ---·-·······Campaign ... .. -.. 19.47 .. ~ .... 194.8 ...

Kind of Water: Press Wash ·water Description of Sample: Campaign average sample composed of three catch samples per week

Source of Water: Drips from all heaters,, blow up coils:., Nos. 4 & 5 pan calandrias and overflow from boiler feed tanks.

ANALYSIS p.p.m HYPOTHETICAL COMBINATIONS p.p.m. Parts Per ISJIPT Parts Per DB Silica SiO. Silica SiO, Iron Fe Sodium Chloride NaCl Calcium Ca Sodium Sulfate Na.SO, Magnesium Mg Sodium Carbonate Na.CO, Sodium Na Sodium Phosphate Na,PO, Chlorine CI Magnesium Chloride MgCI. Sulfuric Acid so. Magnesium Sulfate MgSO, Carbonic Acid co, Magnesium Carbonate MgGO, Phosphoric Acid PO, Magnesium Phosphate Mg,(PO,). Calcium Sulfate CaSO, Calcium Carbonate CaCO, Calcium Phosphate Ca,(PO,). Ferrous Carbonate FeGO, Ferrous Phosphate Fe,(PO,).

Organic and Volatile (by difference) Organic and Volatile (by difference) __.,! D~i:::s~s~o~l;:!-:v!:e:!!d~:X~1~il~t~X~X.~.:!:S~O:!::L:!;ID~S~ A~T..;1!;:::0::::,5_0 ~c~ ___,sa:_. =o__ , __ D_ issolved! 'llDll SOLIDS AT 105° C

COPIES TO General Supt. General Chemist Asst. General Supt. District Engineer Superintendent Laboratory (4) ...... ~4!£ ~~------·- Chief Chemist. 1,'orm 443-2M-7-41-Pads 100 . ' . '

WATER ANALYSIS

______ID.VELAND._····-·········-·········Factory ·· ------Campaign ...... 1947. ....fl!l ... 194 .. &.

Kind of Water: Water used to wash white · sugar. Description of Sample: Campaign average sample composed or three catch samples, per week

Source of Water: Drips fran 3rd effects or evaporators

ANALYSIS HYPOTHETICAL COMBINATIONS p.p.m. Parts Pei:x,e;np Silica SiO, Silica SiO, Iron Fe Sodium Chloride NaCl Calcium Ca Sodium Sulfate Na,SO, Magnesium Mg Sodium Carbonate Na,CO. Sodium Na Sodium Phosphate Na,PO, Chlorine CI Magnesium Chloride MgCI, Sulfuric Acid so. Magnesium Sulfate MgSO, Carbonic Acid co. Magnesium Carbonate MgCOs Phosphoric Acid PO, Magnesium Phosphate Mg,(PO,), Calcium Sulfate CaSO, Calcium Carbonate CaCO, Calcium Phosphate Ca,(PO,). Ferrous Carbonate FeCOa Ferrous Phosphate Fe,(PO,),

Organic and Volatile (by difference) Organic and Volatile (by difference) Dissolved ,amm:, SOLIDS AT 105° C a

COPIES TO General Supt. General Chemist Asst. General Supt, District Engineer Superintendent Laboratory

(5) ················ -ittV/~a.-c.JChief Chemist...... F orm 443-2M-7-41-Pads 100 ' . .

WATER ANALYSIS

______L()VELAJm ______Factory ______C~aj,gn_____ l247~.194.~- -

Kind of Water: Water· used to wash Cold Saecharate Description of Sample:

Source of Water: Same as City Water·

ANALYSIS P•P•• HYPOTHETICAL COMBINATIONS P•P•• Parts Per l!IIID Parts Per~ Silica SiO, Silica SiO. Iron Fe Sodium Chloride NaCl Calcium Ca Sodium Sulfate Na2SO, Magnesium Mg Sodium Carbonate Na.CO, Sodium Na Sodium Phosphate Na,PO, Chlorine CI Magnesium Chloride MgCl, Sulfuric Acid SO, Magnesium Sulfate MgSO, Carbonic Acid co, Magnesium Carbonate MgCO, Phosphoric Acid PO, Magnesium Phosphate Mg,(PO,). Calcium Sulfate CaSO, .. Calcium Carbonate CaCO, Calcium Phosphate Ca,(P0,)2 Ferrous Carbonate FeCO, Ferrous Phosphate Fe,(P0,)2

Organic and Volatile (by difference) Organic and Volatile (by difference) _ -A/.,.r.Qint,1L1J;1edl ~ SOLIDS AT 105° C 4-7_.8__ D saolv ~4 SOLIDS AT 105° C .e

COPIES TO General Supt. General Chemist Asst. General Supt. District Engineer Superintendent Laboratory

(6) ...... &£..?.':~---······ Chief Chemist. .l<'orm 443- 2M-7-41- Pads 100 ' . I \ II f ~

WATER ANALYSIS

______.LOiEL&ND ______····-····-----·---Factory ------·----Campa.i.gn ...... 19.47..~----194.8 .. .

Kind of Water: Wate;r-, in Boiler· Feed Tank Description of Sample: Campaign average sample composed of three catch samples; per week

Source of Water: Drips from st.eam chests of 2nd, )rd, 4th, and 5th effects of evaporators:, granul&tor coil drips, coil drips from No o 3 and 4 pans, cit;y water, drips from all live steam traps throughout the factory, via flash tanlt..

ANALYSIS HYPOTHETICAL COMBINATIONS p.p.m. Parts PerOE:E· Parts Per IIDXIIJC Silica SiO. Silica SiO, Iron Fe Sodium Chloride NaCl Calcium Ca Sodium Sulfate Na.SO, Magnesium Mg Sodium Carbonate Na.CO, Sodium Na Sodium Phosphate Na,PO, Chlorine CI Magnesium Chloride MgCI2 Sulfuric Acid SO, Magnesium Sulfate MgSO, Carbonic Acid co, Magnesium Carbonate MgCO, Phosphoric Acid PO, Magnesium Phosphate Mg,(PO,), Calcium Sulfate CaSO, Calcium Carbonate CaCO, Calcium Phosphate Ca,(PO,). Ferrous Carbonate FeCO, Ferrous Phosphate Fe,(PO,).

Organic and Volatile (by difference) Organic and Volatile (by difference) Dissolved ~SOLIDS AT 105° C .6____ D- 1-· ssolved SOLIDS AT 105° C

COPIES TO General Supt. General Chemist Asst. General Supt. District Engineer Superintendent Laboratory ...... /41'.-z/d ~ a AAJ ...... (7) Chief Chemist. 'r Form 443-2M-7-41-Pads 100

~ " I ( • "• ' •• t ' ' .

WATER ANALYSIS

...... LOVEUJD ...... Factory ...... Q~~itm..... l9.47. .... ~... 194~ ....

Kind of Water: Condensed Water- pllDlped direct to Boilers, Description of Sample: Campaign average sample composed of three catch samples; pe:tr week.

Source of Water: Condensation from white pan coils;

ANALYSIS P•Polll HYPOTHETICAL COMBINATIONS P•P•lh Parts Per ¥tfl: PartsPerDlliX Silica SiO, Silica SiO, Iron Fe Sodium Chloride NaCl Calcium Ca Sodium Sulfate Na.SO, Magnesium Mg Sodium Carbonate Na,COa Sodium Na Sodium Phosphate Na,PO, Chlorine CI Magnesium Chloride MgCI, Sulfuric Acid so. Magnesium Sulfate MgSO, Carbonic Acid co, Magnesium Carbonate MgGO, Phosphoric Acid PO, Magnesium Phosphate Mg,(PO,). Calcium Sulfate Caso, Calcium Carbonate CaCO, Calcium Phosphate Ca,(PO,), Ferrous Carbonate FeCO, Ferrous Phosphate Fe,(PO,),

Organic and Volatile (by difference) Organic and Volatile (by difference) Disaolvedl.1l11Ltl. SOLIDS AT 105° C 6..o _ _.~_..,,isaolve ~SOLIDS AT 105° C

COPIES TO General Supt. General Chemist Asst. General Supt. District Engineer Superintendent Laboratory

(8) ---·--··-·----~41£~-~-----··----·-·Chief Chemist. · Form 443-2M-7-41-Pads 100 '•-. ,,., ·, I ' ' " I ( ' ,\ ' '

WATER ANALYSIS

...... LOVELAND · ...... Factory ...... C.ampaign ...... 1947..... !'!'. .••• 1948. .. .

Kind of Water: W.ateJr· iri Boilers · Description of Sample: Campaign canposite sample composed of one catch sample per day from al1 boilera: in operation. Softeners used in boilers during Campaign Total Pounds Pounda; per day Source of Water: Actual water· in boiler$ Soda ash 0 0 Caustic soda. 3340 37.7 196S 22.:.2 Sodium Sulphite 0 0

ANALYSIS P•P•• HYPOTHETICAL COMBINATIONS pop.m Parts Per 18fif!M' Parts Per1W3t Silica SiO, 1s.1 Silica SiO, 15~1 Iron Fe ,3~. Sodi.um Chloride NaCl 2,3\~6 Calcium Ca 1~4 Sodium Sulfate Na.SO, 133~2 Magnesium Mg ~6 Sodium Carbonate Na2CO, 821~ Sodium Na Sodium Phosphate Na,PO, l({\.r r:!6 434S -.l ' ;J • 6 Chlorine Cl 14~3 Magnesium Chloride MgCl, Sulfuric Acid so. 90~1 Magnesium Sulfate MgSO, Carbonic Acid CO, 464;9 Magnesium Carbonate MgCO, Phosphoric Acid PO, 40.2 Magnesium Phosphate Mg,(P0,)2 2.2. Calcium Sulfate CaSO, Calcium Carbonate CaCO, Calcium Phosphate Ca,(PO,), Ferrous Carbonate FeCO. Ferrous Phosphate Fe,(PO,).

1062~3 Organic and Volatile (by difference) 1062~3 Organic and Volatile (by difference) JDh7e7 J:Ok7~7- __J D[i~s~a~o!J:J;!~!;eci~'.c.l'Jm~· ~SOQ1L~l!!D~S.J.A~T~1!_20~5°:_QC ___2llO.Q _ 1_ -lJ..wH~ Ldl._ fil!J~.§SQOL!:;ILl,;D!..§S~A~TLl,!10~5.:,0 .QC___ "21l8 oO _ Campaign Laboratoey Sheet Averages. Campaign Composite Waten- Sample p&.ni P•P•• Alkaliiiity Dissolved Solids 194li Hardness 8 Hardness 6i pH 10.4 Sodium .. Sulphite 231 3S· 10.6 COPIES TO ~ General Supt. General Chemist Asst. General Supt. District Engineer Superintendent Laboratory ...... d/4/&u~au/ ...... (9) Chief Chemist.