Contractor Reports on CPSC Carpet and Chemical Irritation Studies, And

01890 Final Report January 31,1996 Appendix C Page17of43

COMPOUND IDENTIFIED 1.0 6.0 24.0 48.0 72.0 96.0 Nonane, 4-methyl 1.9 Octane, 3,6-dimethyl 2.3 . Pentane, 2,2,4-trimethyl (Isooctane) 1.6 0.7 Pinene, a 3.4 (2,6,6-Trimethyl-bicyclo[3.1.1 Jhept-2-ene 1 Styrene 7.0 3.1 5.5 5.5 4.2 6.5 Toluene (Methylbenzene) 9.2 0.7 Unidentified 1.5 Xylene (para and/or meta) 4.8 Xylene, ortho 2.0 cis-I-Ethyl-3-methykyciohexane* 4.0

%dicates best NISTIEPANH library match only. Individual compounds and TVOC (total volatile organic compounds) are calibrated relative to toluene. TVOC detection limit: 0.9 yg/m’. Individual detection limits may vary, depending on instrument response.

. 01890 Final Report January 31,1996 Appendix C Page18of43 Cushion C

Environmental Chamber, SA3 Product Loading: 0.42 m2/m3 Test Conditions: 1.00 ACH 50.0% RH f 5.0% RH 23.0 degs C f 2.0 degs C Test Period: 06/22/95 - 06126195

CHAMBER 7VOC CONCENTRATIONS FROM 0.000 TO 96.000 HOURS

ELAPSED Tvoc EXPOSURE CONCENTRATION HOUR ug/m3

0.000 0.0 1 .ooo 915.0 6.000 826.6

24.000 265.3 . 48.000 366.9 72.000 253.1 96.000 38.8

IVOC CONCENTtiTIONS (pg/m’) FROM 0.000 TO 96.000 HOURS

COMPOUND IDENTIFIED 1.0 6.0 24.0 48.0 72.0 96.0

1,3-Dioxolan-2-one, cl-methyl’ 5.9 4.8 11.0 9.1 l-Octanol, 3,7-dimethyl* 2.0 2.4 I-Pentanol, 2-methyl-’ 1.5 I-Pentanol, 4-methyl-2-propyl- (9CI)* 3.0 2,2,7,7-Tetmmethyloctane” 15.6 5.5 2,6-Diitert-butyWmethylphenol (BHT) 66.9 106.1 31.3 82.5 72.1 38.8 2-Hexanol, 5-methyl-* 4.5 2-Propanol (Isopropanol) 2.2

-I_.-__IL- . . . ..--- - -^__-_l”^ 01890 Final Report January 31,1996 Appendix C Page19of43

COMPOUND IDENTIFIED 1.0 6.0 24.0 48.0 7i.o 96.0 2-Propanol, 1 ,3-dichloro- 74.8 106.3 41.6 65.2 86.3 2.Propanone, I-(dimethylamino)-* 5.6 2i-k2,4a-Methanonaphthalene, 1.6 1.3 1.0 1.7 0.8 1,3,4,5,6,7-hexahydro-l , I ,5,5-tetramethyl -, (2s).’ 4-Octanol, 4,7-dimethyl-* 1.2 A&amide, N,N-dimethyl- (8Cl9CI) 82.0 65.0 61.8 Acetone (2.Propanone) 11.2 Benzene, I-ethyl-4-methyl 2.6 (IdEthyltofuene) Benzene, I-methyl+(1-methylethyl) 2.2 (p-Cymene; 4-lsopropyltoluene)* Benzene,(l ,I-Dimethylethyl)- . 6.8 2.0 (t-Butylbenzene)* Butane, 1.5 2,2’-[methylenebis(oxy)]bis[2-methyl-* Cyclohexane, propyl 1.7 Cyclohexanone, 4-methyl-* 1.4 Cyclohexasiloxane, dodecamethyl* 8.9 9.4 3.1 1.6 Cyclopentasiloxane, decamethyl* 145.4 123.7 7.3 0.8 Cyclotetrasiloxane, octamethyl 132.3 32.1 Decane, 2,5,9-trimethyl- (9CI) 5.0 4.6 0.7 Decane, 2-methyl’ 5.1 3.4 Decane, 3-methyl 16.8 5.1 Decane, 4-methyl 10.3 6.1 Dodecane 3.4 1.2 Ethane, III, I-trkhloro 2.8 Ethane, 1,2-dichloro 1.9 . Ethane,l ,l’oxybis[2-chloro- 1.2 (s-Dichloroethyl ether) Ethanol 10.9 01890 Final Report January 31,1996 Appendii C Page 20 of 43

COMPOUND IDENTIFIED 1.0 6.0 24.0 48.0 72.0 96.0 Ethene, 1,1,2,2-tetrachloro 2.7 (Tetrachloroethylene) Fomramide, N,N-dimethyl 2.8 78.9 13.5 6.1 Hepiane, 2,2,4,6,6-pentamethyl (8Cl9CI)” 6.8 1.9 Heptane, 2.2,6,6-tetramethyl* 11.2 1.3 Heptane, 4-ethyl-2,2,6,6-tetramethyl- 18.9 7.3 (9Cl) Hexanal (Hexaldehyde) 1.4 Hexane, 1 ,Y-Oxybis (Hexyl ether* 1.5 Hexane, 2,2,4-trimethyl 2.3 Isooctane, (ethenyloxy)- (9CI)* 1.3 Methanol 28.7 5.4 Methylene chloride (Dichloromethane) 5.1 N,N-Dimethyl-2-propenamide 5.0 100.9 70.9 126.8 82.6 Nonane 2.9 Nonane, 2,5-dimethyl-* 13.1 5.9 Nonane, 3,7-dimethyl’ 3.4 Nonane, 3-ethyl 1.9 Nonane, 3-methyl 1.5 Nonane, 4,5-dimethyl* 2.1 - Octane, 2,2-dimethyl* 4.7 Octane, 2,3,6-trimethyl-* 2.7 Octane, 2,3-dimethyl* 2.3 Octane, 2,6-dimethyl 3.0 Oxetane, 2+dimethyl-, trans-* 5.9 1.2 Oxirane, (chloromethyl)-• 1.4 Pentane* 1.3 Pentane, 2,2,4-trimethyl (Isooctane) 9.2 1.4 Pentane, 2,3,4-trimethyl 3.4 01890 Final Report January 31,1996 Appendix C Page 21 of 43

COMPOUND IDENTIFIED 1.0 6.0 24.0 48.0 72.0 96.0 Pentane, 3-ethyl-2,2-dimethyl- (8Cl9CI)” 2.8 Phenol 2.7 . 1.5 2.0 Propane,? ,2,3-trichloro 129.0 111.5 20.6 6.5 Toluene (Methylbenzene) 59.9 2.5 . Undecane 9.4 4.1 Undecane, 6-methyl-’ 3.2 1.3 Unidentified 5.7 2.3 Xylene (para and/or meta) 7.1 Xytene, ortho 2.8 a-Methylstyrene (iso-Propenylbenzene; 3.7 2.3 (I-Methylethenyl)benzene)

%dkates best NISTIEPAMH library match only. hdiidual compounds and TVOC (total volatile organic compounds) are calibrated relative to toluene. NDC detection limit: 0.9 pg/m’. Jndividual detection limits may vary, depending on instrument response. 01890 Final Report January 31,1996 Appendix C Page 22 of 43 Cushion D

Environmental Chamber. SA4 Product Loading: 0 40 m2/m3 T& Conditions: I:00 ACH 50.0% RH f 5.0% RH 23.0 degs C f 2.0 degs C TestPeriod: 06/26/95 - 06/30/95

CHAMBERTVOCCONCENTRATIONS FROM0.000TO96.000HOURS

ELAPSED Tvoc EXPOSURE CONCENTRATION HOUR (pglm3)

0.000 0.0 1 .ooo 349.0 6.000 634.9 24.000 421.6 48.000 345.8 72.000 NA*

96.000 212.0 4

‘NA: data not available due to laboratory error.

lVOCCONCENTRAT10NS(pglm3)FROM0.000T096.000HOURS

COMPOUND IDENTIFIED 1.0 6.0 24.0 48.0 96.0 l&Dimethylpiperazine 58.5 319.1 71.4 55.3 I H-Cyclopropa[a]naphthaIene, 1.3 1.7 1.3 la,2,3,5,6,7,7a,7b-octahydro-1,1,7,7a -te!ramethyl-,[laR-(laa,7a,7aa,7ba)J *

2,2,7,7-Tetramethyloctane* 0.8 2,6-Di-terkbutyl4methylphenol 23.5 108.1 149.9 122.1 100.9 (WIT) 2-Butenal’ 2.1 01890 Final Report January 31,1996 Appendii C Page 23 of 43

COMPOUND IDENTIFIED 1.0 6.0 24.0 48.0 96.0 2-Propanol (isopropanol) 2.5 44sobutylmorpholine* 1.1 Acetamide, N,N-dimethyl- (8Cl9CI) 13.0 19.4 15.7 11.0 7.4 Acetate, butyl 1.1 Acetic acid, hydroxy-• 1.0 Acetone (2,Propanone) 5.9 3enzene, l,2,4-trimethyl 0.7 Benzene, 1,2-dichloro 7.7 8.0 5.3 3.8 1.9 Benzene, ethyl 1.0 Benzene, propyl 1.0 Butane, 2-methyl (Isopentane) Cyclohexasiloxane, dodecamethyl*

Ethane, 1, 1, I-trichloro

Ethanol, 2-butoxy 01890 Final Report January 31,1996 Appendix C Page 24 of 43

COMPOUND IDENTIFIED 1.0 6.0 24.0 48.0 96.0 I Octane, 2,3-dimethyl 1.2 Pentane, 2,2,4-trimethyl (Isooctane) 2.1 1 Pentane, 2,3,4-trimethyl’ 0.6 Phenol 1.0 Pinene, a 1.1 (2,6,6-Trimethyl-bicyclo[3.1.l]hept-2-e ne) Styfene 40.6 40.3 23.1 12.2 4.2 Toluene (Methylbenzene) 16.9 4.0 Undecane 1.6 1.0 Unidentified 100.8 101.2 138.2 130.4 90.7 I Xyiene, ortho I 1.5 I I I I

Wtkates best NISTEPAINIH library match only. Individual compounds and TVOC (total volatile organic compounds) are calibrated relative to toluene. TVOC detection limit: 0.9 pg/m’. Individual detection limits may vary, depending on instrument response. 01890 Final Report January 31,1996 Appendii C Page 25 of 43 Cushion E

Environmental Chamber: SA5 Product Loading: 0.42 m2/m3 Test Conditions: I .OO ACH 50.0% RH k 5.0% RH 23.0 degs C f 2.0 degs C Test Period: 06/26/95 - 06/30/95

CHAMBER TVOC CONCENTRATIONS FROM 0.000 TO 96.000 HOURS

ELH’+P;;D;;) / EXPOSURE CONCENTF$ATION

0.000 0.0 1 .ooo 1447.1 6.000 1631.1 24.000 1260.0 48.000 856.1 72.900 572.9 96.000 177.7

IVOC CONCENTRATIONS &g/m’) FROM 0.000 TO 96.000 HOURS

COMPOUND IDENTIFIED 1.0 6.0 24.0 48.0 72.0 96.0

1,2-Propanediol (Propylene 3.1 27.1 - 28.1 26.8 20.2 glycol) I ,3-Butanediol’ 4.2 44.9 40.4 41.5 30.6 1,3-Cyclohexadiene, 2.5 2.2 I-methyl4(+methylethyl)-• I 1 $I-Cyclohexadiene, 0.8 I-methyl+(‘l-methylethyl)- (9CI) I ,4-Dimethylpiperazine 2.1 1 +Dioxane, 3.1 2-methyl-3-methylene-* 1-Heptanol, 6-methyl* 1.7 01890 Final Report January 31,1996 Appendix C Page 26 of 43

COMPOUND IDENTIFIED ‘1.0 6.0 24.0 48.0 72.0 96.0 IiUndecene, 8-methyl-* 6.5 5.3 2(3H)-Furanone,dihydro 3.3 3.5' 2.9 1.9 (Butyrolactone)* 2,3-Butanediol 2.9 28.2 24.5 26.2 19.8 2,6-Octadien-I-01, 3,7-dimethyl-, 1.7 (Z)-* 2-Butanone, 3-hydroxy-• 2.1 2-Decene, 4-methyl-, (Z)* 6.2 2-Decene, %methyl-, (Z)-” 5.7 2.7 2-Decene, 8-methyl-, (Z)-* 3.0 1.6 3-Cyclohexene-‘l-methanol, 43.7 69.1 49.8 54.7 35.7 20.2 a,a,4-trimethyl-, acetate* 4-Dodecene” 8.0 6.9 4-Phenylcyclohexene 2.3 9.8 8.4 5.5 3.0 1.6 4-Undecene, (Z)-• 7.0 6.3 NJndecene, (E) 8.3 6.4 6-Dodecene, (E)- (8Cl9CI)” 3.1 Acetamide, N,N-dimethyl- 2.7 2.5 3.4 1.7 (8Cl9CI) Acetate, methyl (Acetic acid, 11.4 1.7 Methyl ester) Acetic acid 1170.4 1271.3 1004.@ 641.7 426.1 137.5 Acetic acid, phenylmethyl ester 8.4 3.9 2.1 1.2 lBenzyl acetate) Acetone (2.Propanone) 16.8 3.7 Benzaldehyde 8.1 4.1 2.8 1.7 2.2 Benzyl alcohol 7.1 4.4 6.0 3.8 1.6 (Benzenemethanol) Bicyclo[3.1 .l]heptane-2-methano 0.3 I, 6,6-dimethyl-, acetate*

-“-- ..- --I-. -“. ”

-_ - I . . I. --.-_l_---_l_.__ . . . ______. 01890 Final Report January 31,1996 Appendix C Page 27 of 43

COMPOUND IDENTIFIED 1.0 6.0 24.0 48.0 72.0 96.0 Biqrclo~.2.0]undec-4-ene, 1.2 1.4 1.3 4J I,1 Wimethyl-8-methylene-,[I R-(1 R@,42,9S@)]-* Cedrene, a* 5.0 5.3 5.7 2.5 4.8 1.7 Cyclohexane, 1, I’-oxybis* 2.5 2.1 1.2 Cyclohexanol 1.8 Cyclohexanol, 1.2 1.3 0.9 I-methyl4(1-methylethenyl)-, acetate* Cyclohexene, 22.3 20.1 9.0 2.7 1.0 0.9 l-methyl-4-(I-methylethylidene)-• Cyclopentasiloxane, decamethyl* 21.4 2.4 Cyclopropane, l-ethyl-2-heptyl- 7.3 4.7 (9Cl)’ Cyclotetrasiioxane, octamethyl 1.3 Decane 1.4 1.9 Ethanol 3.1 1.8 Limonene (Dipentene; 25.9 35.0 31.0 13.9 6.0 6.6 j-Methyl4( 1 -methylethyl)cycioh exene) Methanol 24.6 Nonane, 2,6-dimethyl’ 2.0 Propanoic acid 19.6 - 16.8 12.3 9.5 1.5 Toluene (Methylbenzene) 4.8

WI --._- . -- _- -_ --- *, 01890 Final Report January 31,1996 Appendix C Page 28 of 43 , 1 COMPOUND IDENTIFIED 1.0 6.0 24.0 48.0 72.0 96.0 Tricyclo[5.4.0.02,8]undec-9-ene, 7.7 8.3 7.7 4.8 4.8 3.1 2,6,6,9-tetramethyl-• Unidentified 14.7 4.4 5.0 1.1 1.3 0.9 4

Wckates best NISTIEPAINIH library match only. tndiiual compounds and TVOC (total volatile organic compounds) are calibrated relative to toluene. TVOC detection limit: 0.9 vg/m’. Individual detection limits may vary, depending on instrument response. 01890 Final Report January 31,1996 Appendix C Page 29 of 43

Carpet B at Elevated Conditions (70 “C, 8% RH, high loading)

Environmentalchamber: SC4 Product Loading: 1.64 m2/m3 Test Conditions: l.OOACH 8.0% RH f 2.0% RH 70.0 degsCk5.0degsC TestPeriod: 06121/95 - 06/21/95

CHAMBERTVOCCONCENTRATlONSFROM0.000TO99.000HOURS t ELAPSED Tvoc EXPOSURE CONCENTRATION HOUR @g/m3

-J

lVOCCONCENTRAT10NS(~g/m3)FROM 0.000T06.000 HOURS

COMPOUND IDENTIFIED 0.0 1.0 6.0

1,2-Ethanediol (Ethylene glycol) 98.3 466.0 1,3-Butanediol, (S)-' 4.3 l+Pentadien-3-01' 36.3 7.9

I-Butanol (N-Butylalcohol) 165.1 12.3 A-Decanol (N-Decyl alcohol) 60.6 21.6 I-Decene, 8-methyl 292.6 92.5 I-Dodecanol 766.5 63.4 I-Dodecene* i 51.8 17.5 'I-Heptanol,6-methyl* 1163.7 288.2 1-Hexene 4.5 I-Octanol, 2-butyl-(8Cl9CI)* 7.1 178.7 I-Octene, 2.6-dimethyl-* 74.6 22.5 01890 Final Report January 31,1996 Appendix C Page 30 of 43

COMPOUND IDENTIFIED 0.0 1.0 6.0 I-Propanol (Propyl alcohol) 57.7 13.3 I-Propanol, 2-(2-hydroxypropoxy)* 405.1 371.5 1-Propene, 3-chloro-2-methyl-* 9.1 2.9 I-Tetradecanol’ 468.6 13.8 2(1 i-i)-Naphthalenone, 142.4 9.1 octahydro4a,7,74rimethyl-, trans-• 2,2/LTrimethyl-1,3-pentanediol 267.2 33.7 monoisobutyrate (Texanol)

2,2-Dimethyl-I-isopropyl-1,3-prop 137.3 29.0 anediol monoisobutyrate (Texanol) 2,6-Diitert-butyl+methyIphenol 2351.0 328.3 NJ-l 2,6-Octadien-l-01, 3,7-dimethyl-, 78.8 6.3 acetate, (2).• 2,6-Octadien-1-ol,3,7-dimethyl, (E) * 10.4 6.4 - (Geraniol)’ 2-Butanone (Methyl ethyl ketone, 5.0 MEK) 2-Butenal, 2-ethenyf-• 2.4 2-Cyclohexen-l-one, 14.3 6.9 2-methyl-5-( 1 -methylethenyl)-* 2-Decene, g-methyl-, (2).• 217.8 44.4 2-Decene, (Z)-• 2-Decene, 3-methyl-, (Z)-• 327.7 79.0 2-Decene, 5-methyt-, (Z)-* 387.6 173.0 2-Decene, 7-methyl-, (2)’ 220.0 35.8 2-Dodecen-l-yl(-)succinic 1090.4 anhydride*

2-Dodecene, (E)’ 322.3 2-Naphthalenemethanol, ’ 6.3 a-meth+, (.+I-J-• 01890 Final Report January 31,1996 Appendix C Page 31 of 43

COMPOUND IDENTIFIED 0.0 1.0 6.0 2-Octene, (E)-* 12.6 2-Octene, (z)-• 8.7 2-Octene, 4-ethyL* 96.7 2-Pentanone, 4hydroxy4methyl- 64.6 4.9 (m9cI)* 2-Pentanone, 4-methyl (Methyl 5.2 isobutyl ketone, MIBK)* 2-Propanol (lsopropanol) 21.1 4.1 2-Propen-l-01, 2-methyl 6.0 0.8 2-Propenal’ 3.9 2-Propenoic acid, methyl ester* 37.6 13.6 2-Undecene, 2,5-dimethyl-” 500.0 172.2 2l-LBenzocyclohepten-2-one, 1214.1 decahydro-4a-methyl-, trans-• 3,5-Cyclohexadiene-I ,2-dione, 11.5 3,5-bis(1, I-dimethyfethyl)-• 3-Buten-2-ol* 3.9 3-Cyclohexene-l-methanol, 82.8 29.5 a,a,4-trimethyl-* 3Cyclohexene+methanol, 61.5 9.4 a,a,lltrimethyl-, acetate* 3-Decene* 273.3 106.1 SDecene, 2-methyl-, (Z)-• 985.6 281.6 3-Dodecene, (E)* 527.3 158.6 SDodecene, (Z)- (8Cl9Cl)* 63.6 3-Ethyl-2-methyl-I-heptene’ 3.1 3-Octene, 2,6-dimethyl-• 99.1 18.2 3-Undecene, 2-methyl-, (E)-• 1660.4 469.6 IdDecene, 3-methyl-, (E)-• 697.0 4-Dodecene* 521.5 152.5 01890 Final Report January 31,1996 Appendix C Page 32 of 43

COMPOUND IDENTIFIED . 0.0 1.0 6.0 4-Isobutylmorpholine > 1317.7** 547.3 4-Nonene, 3-methyl, (2) .551.7 126.6 4-Nonene, 5-methyl-* 56.0 34.0 4-Octene, (E)’ 35.0 4-Octene, 2,3&trimethyl-• 130.5 4-Phenylcyclohexene 58.7 10.2 4-Piperidinecarboxylic acid, 633.1 26.2 4-phenyl-, ethyl ester* 4-tert-Butylcyclohexyl acetate* 3.3 5-Dodecene, (E)* 191.6 49.5 5-Undecene, (E)” 1045.9 331 .I 5-Undecene, (z)- (8C19CI)’ 1789.0 403.0 6-Dodecene, (E)- (BCl9Cl) 816.4 348.0 A&amide, N,N-dimethyl- 404.3 60.5 (BCl9Cl) Acetamide, 264.1 28.2 N-methyl-N-[4-[4-methoxy-I-hexa hydropyridyll-2-butynyi]-• Acetate, ethyl 4.0 Acetic acid 0.9 153.3 Acetone (2.Propanone) 78.0 23.1 Azulene, 7-ethyl-1,4-dimethyl-* 8.1 Benzene, I-ethyM-methyl 43.1 (4-Ethyltoluene) . Benzene, ethyl 23.4 Benzene.1 ,I’-Oxybis- (Diphenyl 126.4 10.3 ether)’ Benzoic acid, 2-hydroxy-, I - 399.7 53.6 3-methylbutyl ester” Benzoic acid, 2-hydroxy-, pentyl 333.3 * 10.1 ester* 01890 Final Report January 31,1996 Appendix C Page 33 of 43

COMPOUND IDENTIFIED 0.0 1.0 6.0 Benzoic acid, 138.0 4.7 3-(5-hydroxy-I-pentenyl)-, methyl ester, (E)-* Benzothiatole 8.8 Butane 6.7 Butanoic acid 10.3 Caryophyllene oxide* 464.7 Cyclohexane, (I-methylpropyl)-* 44.1 4.2 Cyclohexane, 1,1,2-trimethyl* 11.6 1.2 Cyclohexane, 278.0 163.0 1 ,I-dimethyl-Z-propyl-” Cyclohexane, 2.0 I-ethenyM-methylene-5-(l-prope nylidene)-* Cyclohexane, I-ethyl-2-methyl-, 17.5 3.9 cis- (8Cl9CI)” Cyclohexane, methyl 5.2 Cyclohexane, octyl’ 33.6 Cyclohexane, propyl 61.0 Cyclohexane, t-I-ethyM-methyl* 32.8 Cyclohexanol, 52.6 ’ 15.1 Z-methylene-3-(I-methylethyl)-, - acetate, cis-• Cyclopentane, 1,2,4-trimethyl, 11.0 1.7 (1 a,2&4a)* Cyclopentasiloxane, decamethyl’ 99.5 25.9 Decane 910.6 . 46.7 Decane, 6-ethyl-2-methyl- (9CI)* 12.1 Dipropylene glycol 229.4 23.7 Disiloxane, pentamethyl-• 4.1 ‘ Dodecane 122.8 11.2 01890 Final Report January 31,1998 Appendix C Page 34 of 43

COMPOUND IDENTIFIED 0.0 1.0 6.0 Ethane, 1 , 1,l -trichloro 4.7 Ethanol 210.4 4.7 Ethanol, 2-(2-butoxyethoxy) 224.8 105.2 Ethanol, 2-butoxy 35.6 3.7 Ethanol, 2-phenoxy- 84.4 36.6 Furantetrahydro; THF 2.0 Heptadecane* 2.4 Heptanal (Heptaldehyde)* 2.8 Heptane 15.6 Heptane, 2,4-dimethyl 25.0 Heptane, 2,5-dimethyl* 13.6 Heptane, 3-methyl 10.9 Heptane, 3-methylene- (9Cl)” 16.6 Heptane, 4-methyl 12.4 Hexadecane (Cetane) 235.7 10.5 Hexadecane, 2,6,10-trimethyl-* 10.0 Hexane, 2,2,5-trimethyl- (8Cl9CI)* 126.6 5.2 Hexane, 2,2-dimethyl 67.5 Hexane, 3-methyl 15.8 Hexanoic acid 77.6 66.4 lsobomyl acetate* 363.5 Methanesulfonyl chloride* 1.9 Morpholine, LGmethyl 6.6 3.4 Naphthalene 69.7 22.3 Naphthalene, 1,2-dimethyl-* 79.8 3.4 Naphthalene, t ,4,6-trimethyl* 120.2 8.2 Naphthalene, 1 +dimethyl’ 193.8 5.2 Naphthalene, 1,6-dimethyl* 199.9 10.7 01890 Final Report January 31,1998 Appendix C Page 35 of 43

COMPOUND IDENTIFIED 0.0 1.0 6.0 Naphthalene, 436.3 1,6-dimethyl(l-methylethyl)-’ Naphthalene, l-methyl 23.5 5.3 Naphthalene, 2,3,6-trimethyl- 18.5 (8Cl9CI)* Naphthalene, 2,7-dimethyl* 96.0 3.8 Naphthalene, 2-methyl 28.3 10.8 Naphthalene, 123.9 9.3 6(3-ethylpropyl)-1,2,3,4-tetrahydro l

Naphthalene, 298.7 12.4 decahydro-4a-methyl-l -methylene -7+methylethylidene)- (4aR- bans)-* Nonane 84.8 2.0 Nonane, 3-methyl 73.1 Nonane, 4-methyl 31.7 3.3 Octane 23.1 Octane, 2,6-dimethyl 121.1 15.6 Octane, 2-methyl 17.7 Octane, 3-methyl 43.6 14.4 Octane, Idethyl* 75.8 Pentadecane, 469.9 2,6,10,14-tetramethyl-• a Pentane, 2,2,4&imethyl 560.7 (Isooctane) Pentane, 2,3,4-trimethyl 61.6 Pentane, 2,3-dimethyl (8C19CI)* 11.8 Pentane, 2+dimethyl* 8.4 Pentanoic acid (Valeric acid) 30.1 20.2 Phenol 183.4 68.7 01890 Final Report January 31,1996 Appendix C Page 36 of 43

COMPOUND IDENTIFIED 0.0 1.0 6.0 Phenol, 79.6 2.0 4,6-di(l ,I-dimethylethyt)-2-methyl- l

Phenol, bis(1 ,l-dimethylethyI)- 8.0 (9Cl)’ Propanedioic acid, diproyl-, diethyl 747.7 59.4 ester* Pyridine, 52.5 l,2,3,6-tetrahydro-4~[4,5-dihydrox ypheny!]-1 -methyl-* TXIB - 324.8 19.2 (2,2,4-TrimethyI-1,3-pentanediol diisobutyrate) Terbutol* 66.5 Tetradecane 110.0 3.4 Toluene (Methylbenzene) 289.2 Tridecane 22.8 Trimethylamine 0.6 (methanamine,N,N-dimethyl)* Unidentified 1840.9 30.8 Xylene (para and/or meta) 52.9

‘Mites best NISTIEPAINIH library match only. “Values marked with l >. symbol were outside linear range of detector. Concentration value is a lower bound only. Individual compounds and TVOC (total volatile organic compounds) are calibrated relative to toluene. TVOC detection limit: 0.9 vg/rn’. Individual detection limits may vary, depending on insbument response.

I I.--“-^“.“l^ -e-P.-- _- -

- . . ..----. 01890 Final Report January 31,1998 Appendix C Page 37 of 43 Cushion B at Elevated Conditions (70 “C, 8% RH, high loading)

Environmental Chamber: SC5 Product Loading: 1.65 m2/m3 Test Conditions: 1.00 ACH 8.0% RH f 2.0% RH 70.0 degs C f 2.0 degs C Test Period: 06/21/95 - 06/21/95

CHAMBER IVOC CONCENTRATIONS FROM 0.000 TO 6.000 HOURS

ELAPSED Tvoc EXPOSURE CONCENTl$ATION HOtJR

p?jEzyj

IVOC CONCENTRATICNS (pg/m3) FROM 0.000 TO 6.000 HOURS

COMPOUND IDENTIFIED 1.0 6.0

(tert-Butoxymethyl)oxirane* 37.2 1,2-Ethanediol (Ethylene glycol) 30.9 39.4 1,2-Propanediol (Propylene glycol) 37.2 42.6 1 +Dimethylpiperatine 9.5 I-Acetoxy-2-propanol* 23.9 I-Butanol (N-Butyl alcohol) 471 .o 134.8 I-Dodecene 29.3 I-Hexanol, 2-ethyl 71.4 80.7 l-Nonene, 4,6&trimethyl- (9CI)* 8.8 8.0 I-Octanot 11.0 I-Octanol, 2-butyl- (8Cl9Cl) 14.7 I-Octene, 3-ethyl-* 26.5 4.9

- _ ^I--~ P - .-... 01890 Final Report January 31,1996 Appendix C Page 38 of 43

COMPOUND IDENTIFIED 1.0 6.0 I-Pentanol, 3-methyl 8.3 4.9 l-Phenyl-l-propyne 13.5 ?-Propane! (PropyI alcohol) 118.9 19.2 l-Tetradecene 7.6 A-Undecene 35.3 I H-lndene, 7.9 2,3-dihydro-I,? ,3-trimethyl-* 1 H-lndene, 28.1 48.9 2,3-dihydro-l,2-dimethyl-” 1 H-lndene, 46.8 41.0 2,3-dihydro-1,3-dimethyl* 1 H-lndene, 29.5 25.0 2,3-dihydro-4,7-dimethyl-* I H-lndene, 2,3-dihydro+methyl* 69.4 59.5 1 H-Phenanthro[9,10-dlimidazol-2-a 81.1 119.1 mine+ 2,2,4&Tetramethyioctane* 2.2,~Trimethyl- ,3-pentanediol 58.0 95.9 monoisobutyrate (Texanol) 2,2-Dimethyl-l-isopropyl-1,3-propan 34.2 41.9 ediol monoisobutyrate (Texanol) 2,5-Cyclohexadiene-1 +dione, 90.7 - 134.4 2,6-bis(1 ,I-dimethylethyl)- (9’ 2,6-Di-tert-butyI4methylphenol 1823.6 2585.8 (BHT) 2-Ethylhexanoic acid 664.5 1210.1 2-Pentanone, 4-hydroxy4methyk 447.3 303.9 (8C[9Cl)* 2-Pentanone, LGmethyI (Methyl 13.7 isobutyl ketone, MIBK)

2-Propanol (Isopropanol) 7.7 2-Propanol, 1,3=dichloro- 53.9 41.3 01890 Final Report January 31,1996 Appendix C Page 39 of 43

COMPOUND IDENTIFIED 1.0 6.0 2-Propanol, * 29.0 I-II-methyl-2-(2-propenyloxy)ethoxy

2-Propenal’ 12.3 2-Propenal, 2-methyl* 4.5 2-Pyrrolidinone, l-methyl 14.4 2H-2,4a-Methanonaphthalene, 40.1 37.9 I ,3,4,5,6,7-hexahydro-I, 1,5,5-tetra methyl-, (2S)-• 3-Carene” 63.4 3-Pentanol* 6.8 3-Penten-2-one, 4-methyl- (8Cl9CI)* 18.0 13.9 4kobutylmorpholine > 1135.3** > 1534.1”’ Acetamide, N,N-dimethyl- (8Cl9CI) 337.8 362.7 Acetate, butyl 10.2 Acetic acid 69.7 Acetic acid, 2-ethylbutyl ester’ 14.8 11.7 Acetic acid, phenylmethyl ester 39.8 Acetone (2-Propanone) 226.4 94.5 Benzaldehyde 20.0 10.6 Benzene, 1,2,4,5-tetramethyl* 37.3 Benzene, 1,2&trimethyl 90.9 35.4 Benzene, 1,4-dichloro 37.2 24.5 Benzene, I-ethyl-2,4-dimethyl-* 48.9 34.5 Benzene, I-ethyl-2-methyl 38.9 9.5 (2.Ethyltoluene) Benzene, 48.6 22.0 l-methyl4(l-methylethyl) (p-Cymene; 4lsopropyltoluene) Benzene, 4-ethyl-l &dimethyl* 21.6 Benzene, ethyl 9.8 01890 Final Report January 31,1996 Appendix C Page 40 of 43

COMPOUND IDENTIFIED 1.0 6.0 Butanal (Butyraldehyde) 5.2 Butanoic acid 8.5 Camphene 81.4 23.9 Cedrene, a* 16.0 12.8 Cyclohexane, hexyl’ 42.4 35.5 Cyclohexanone 8.9 7.2 Cyclohexene, 91.6 91.0 3-methyl-6-(I-methylethylidene)-• Cyclohexene, 4-(1 ,I-dimethylethyl)* 51.4 Cyclopentane, 15.6 1 -methyl-3-(29methylpropyl)-• Cyclopentanone’ 11.7 16.6 Cyclopentasiloxane, decamethyl* 77.2 34.4 Decane 114.1 18.0 Decane, 2,2,4-trimethyl-’ 37.7 Decane, 2,6,6-trimethyl-* 43.2 Decane, 2-methyl 40.8 Decane, 3,8-dimethyl 35.0 Decane, S-methyl* 73.2 Dodecane 80.0 - 57.4 Dodecane, 2,6, IO-trimethyl-* . 10.6 Dcdecane, 3-methyl- (8Cl9CI) 17.5 17.2 Ethane, 1 , 1, I-trichlom 3.1 Ethane, 1,2-dichloro 4.6 5.5 Ethanol 36.3 6.3 Ethanol, 2-(2.butoxyethoxy) 46.3 Ethanol, 2-butoxy 33.4 23.2 Ethanol, 2-chloro-• 2.8 * 01890 Final Report January 31,1996 Appendix C Page 41 of 43

COMPOUND IDENTIFIED 1.0 6.0 Ethene, 1 ,I ,2,2-tetrachloro 6.0 (Tetrachloroethylene) Ethyl 60.2 I-methylcyclopropanecarboxylate* Heptane, 2,2,6+tetramethyl 8.1 Heptane, 2,4,6-trimethyl 8.9 Hexane, 2,2,5-trimethyl- (8Cl9CI)’ 10.2 Hexanoic acid 27.5 lsobomyl acetate* 848.2 906.5 Limonene (Dipentene; 224.6 75.9 I-Methyl+ 1 -methylethyl)cyclohexe ne) LinalooP 71.2 Morpholine, 4-ethyl-’ 18.0 N,N-Dimethyl-2-propenamide 12.3 14.4 Naphthalene 115.0 95.3 Naphthalene, 13.8 -l,2,3,5,6,8a-hexahydro-4,7-dimethyl -I-(I-methylethyl)-, (IS-cis)-* Naphthalene, 1,4,6-trimethyl* 52.4 Naphthalene, ‘l,4-dimethyl 10.5 10.2 Naphthalene, 1 J-dimethyl- 6.6 - (8Cl9CI)’ Naphthalene, 11.6 I$-dimethyl4(?-methylethyl)-* Naphthalene, I-(2.propenyl)* 3.4 3.0 - Naphthalene, I-methi 21.8 24.9 Naphthalene, 2,3,6-trimethyl- 50.5 (8Cl9CI)’ Naphthalene, 2,6-dimethyl-* 9.5 Naphthalene, 2-ethyl* 5.9

.- 1-. . 01890 Final Report January 31,1996 Appendix C Page 42 of 43 . COMPOUND IDENTIFIED 1.0 6.0 Naphthalene, 2-methyl 63.4 69.7 Naphthalene,G-(1 ,l-dimethylethyl)-1 36.4 . ,2,3+tetrahydro-* Nonane 14.4 Nonane, 3,7-dimethyl’ 96.5 24.1 Nonane, 3-methyl-5-propyl-• 33.0 Nonane, 4,5-dimethyl* 140.6 Nonane, 4-methyl 32.0 Octane, 2,2,6-trimethyl* 50.9 11.8 Octane, 3-ethyl-2,7-dimethyl- (9CI)” 118.8 Pentanal (Valeraldehyde) 4.1 Pentane, 2,2+trimethyl (Isooctane) 2.7 Phenol 165.1 168.3 Phenol, 34.6 2,6-bis(1 ,I-dimethylethyl)+ethyl* Phenol, 4-t-butyl 10.4 (4-(1 ,I-Dimethylethyl)phenol)* Pinene, a 21.7 (2,6,6-Trimethyl-bicycloI3.1 .A Jhept-2 -ene) Propane, 2-methyl-2-nitro* 7.3 Propanoic acid 12.4 Propanoic acid, 2,2-dimethyl-’ 8.1 Propanoic acid, 2-methyl- (9CI)* 6.1 Propanoic acid, 10.1 8.2 2-methyl-2-f(trimethylsilyl)oxy]-, trimethyp Styrene 19.4 5.5 Styrene, 2,5-dimethyl* 31.5 28.9 Tetradecane 15.3 5.8 01890 Final Report January 31,1996 Appendix C Page 43 of 43

COMPOUND IDENTIFIED 1.0 6.0 Thiophene, 17.1 2-buty&(2-methylpropg)- (9CI)’ 1 I ~;~?fJlethylbenzene) / XL; 1 7.8 14.3

Undecane I 186.1 I 96.4 I Undecane, 2,3-dimethyl-’ - 34.1 25.5 Undecane, 2-methyl 27.6 Undecane, 3,9-dimethyl- (8CI)* 42.8 I 42.0 Undecane, 5-methyl- (8dl9Cl)* 30.6 Unidentified 374.8 503.3 Xylene (para and/or meta) 40.8 Xylene, ortho 28.9 9.4

‘Indicates best NISTEPANIH library match only. “Values marked with “pa symbol were outside Gnear range of detector. Concentration value is a lower bound only. Individual compounds and TVOC (total volatile organic, compounds) are calibrated relative to toluene. IVOC detection liiit: 0.9 yg/m’. Individual detection limits may vary, depending on instrument response.

-.----__ _-- - . ---_ _ APPENDIX D

INDIVIDUAL VOC CONCENTRAIIONS DURING EXPOSURES TO SYNTHESIZED MIXTURES

----_ .” - ---~. 61890 Flnet Report January 31,1996 Appendix 0 Page 1 of 37 TABLE D-l

CONCENTRATION DATA FOR EXPOSURE TO PRIME URETHANE “A” TEST MIXTURE

Compound Concentration (mg/m3) Mean Precision Concentration (% RSD) Sample 1 Sample 2 Sample 3 h4Jm (first IO minutes jmliidle IO minutes (!ast 90 minutes of of exposure) of exposure) exposure) 2,6-Di-tert-butyl-4- 6.2 12.3 12.1 10.2 33.9 methylphenol 1,4=Dimethylpiperarine 11.1 16.2 17.2 14.8 21.9 1 , 1, I -Trichloroethane 6.8 7.0 7.2’ 7.0 2.4 Adiponitrile 0.3 0.5 5.8 2.2 143 Styrene 5.6 6.1 6.1 5.9 . 4.2 Octamethylcyclotetrasiloxane 3.0 3.2 3.3 3.2 3.5 Ether 0.8 1.3 Ethyl acetate* 0.5 0.8 Methanonaphthalene* 0.2 0.3 0.3 Isooctane* 0.2 0.2 Methanol* 0.1 0.2 Oi 890 FM RepotI January 31,1996 Appendix D Page 2 of 37

Compound Concentration (mg/m3) Mean Precision Concentration (% RSD) Sample 1 (first 10 minutes (mlddleSample 10 minutes 2 (last Sample10 minutes 3 of h4m3) of exposure) of exposure) exposure)

HexaM 0.1 < 0.1 1 ,I-Dichloroethene’ 0.1 Hexamethylcyclotetrasiloxane* 0.1 . Benzene*

Wuantftatfon felath to toluene response only. .

01890 Final Report January 31,1996 Appendix D Page 3 of 37 TABLE D-2

CONCENTRATION DATA FOR EXPOSURE TO I . PRIME URETHANE “A” TEST MIXTURE WITH BHT REMOVED

Compound Concentration (mg/m’) Mean Precision -- Concentration (% RSD) piz- Sample 2 Sample 3 Wm3) (first 10 minutes (middle IO minutes (last 10 minutes of I I of exposure) of exposure) exposure) I 2,6-Di-tert-butyl-4- nd nd nd nd -- methylphenol 1.4.Dimethylpiperazine 13.8 19.2 15.8 I- 16.3 16.8 I, I, I-Trichloroethane 10.0 10.5 8.6 I 9.7 10.0 Adiponitrile nd 0.2 0.4 132 ~~ 1.1 Styrene I 6.2 6.7 6.7 6.5 ' 4.4 Octamethylcyclotetrasiloxane 4.4 4.3 4.6 I 4.4 3.4 Methanol* 4.5 3.1 1.9 Pyrazine* 0.1 0.2 0.3 Ether* 3.5 I -- I ,I-Dkhloroethene” 1.7 I Isooctane* 0.6 I 01890 Final Report January 3 1,1998 Appendix D Page 4 of 37

Concentration

Ethyl acetate* Acetone* Hexane* Benzene*

Qmtitatfon telative to toluene response onty, 61890 FM Report January 31,1996 Appendix D Page 5 of 37 TABLE D-3

CONCENTRATION DATA FOR EXPOSURE TO PRIME URETHANE “A” TEST MIXTURE WITH BHT AND 1,4=DIMETHYLPIPERAZINE REMOVED

Compound T Concentration (mglm’) T Mean Precision I I Concentration (% RSD) Sample 1 Sampie 2 Sampie 3 Sample 4 hm3; (first 10 (IO-30 (30 - 50 (last 10 mlnutes of minutes of minutes of minutes of exposure) exposure) exposure) exposure) nd nd nd nd nd I I nd I nd I nd nd nd I, 1, I-Trichloroethane 2.9 I 2.7 I 2.5 2.5 2.7 8.0 Adiponitrile 6.4 3.3 89 Styrene 4.9 4.7 7.6 Octamethylcyclotetrasiloxane 1.4 0.9 51 l Aluo esuodsal euanloj 01 wq]ep~ uo!pq~uen~,

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