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International Scientific Journal VOL. 67_2016 ISSN 2545-4315 International Scientific Journal INTERNATIONAL SCIENTIFIC JOURNAL JOURNAL OF AGRICULTURAL, FOOD AND ENVIRONMENTAL SCIENCES http://www.fznh.ukim.edu.mk/jafes/ The JAFES is an International scientific peer­reviewed Open Access Journal published twice а yearly JAFES On line (e-ISSN 2545-4315) offers free access to all articles at http://www.fznh.ukim.edu.mk/jafes/ Published by: Издава: “Ss. Cyril and Methodius" University in Skopje, Универзитет „Св. Кирил и Методиј“ во Скопје, Faculty of Agricultural sciences and food-Skopje Факултет за земјоделски науки и храна ­ Скопје Advisory board Издавачки совет EDITORIAL BOARD УРЕДУВАЧКИ ОДБОР Еditor in Chief Главен уредник Vjekoslav Tanaskovikj, Skopje, Macedonia Вјекослав Танасковиќ, Скопје, Македонија Kocho Porchu, Skopje, Macedonia Кочо Порчу, Скопје, Македонија Associate Editor Уредници Snezana Jovanovic, Belgrade, Serbia Снежана Јованович, Белград, Србија Jovica Vasin, Novi Sad, Serbia Јовица Васин, Нови Сад, Србија Radmila Stikić, Belgrade, Serbia Радмила Стикич, Белград, Србија Biljana Škrbić, Novi Sad, Serbia Билјана Шкрбич, Нови Сад, Србија Ana Marjanovic Jeromel¸ Novi Sad, Serbia Ана Марјанович Јеромел, Нови Сад, Србија Bojan Srdljević, Novi Sad, Serbia Бојан Срдљевич, Нови Сад, Србија Zoran Rajić, Belgrade, Serbia Зоран Рајич, Белград, Србија Jasmina Havranek, Zagreb, Croatia Јасмина Хавранек, Загреб, Хрватска Mirjana Herak­ Ćustić, Zagreb, Croatia Мирјана Херак­Чустич, Загреб, Хрватска Vlasta Piližota, Osijek, Croatia Иво Туршич, Осијек, Хрватска Ivo Tursich, Zagreb, Croatia Власта Пилижота, Загреб, Хрватска Darko Vončina, Zagreb, Croatia Дарко Вончина, Загреб, Хрватска Zlatan Sarić, Sarajevo, B&H Златан Сарич, Сарајево, БиХ Josip Ćolo, Sarajevo, B&H Јосип Чоло, Сарајево, БиХ Muhamed Brka, Sarajevo, B&H Мухамед Брка, Сарајево, БиХ Velibor Spalević, Podgorica, Montenegro Велибор Спалевич, Подгорица, Црна Гора Bozidarka Marković, Podgorica, Montenegro Божидарка Маркович, Подгорица, Црна Гора Nazim Gruda, Bonn, Germany Назим Груда, Бон, Германија Venelin Roychev, Plovdiv, Bulgaria Венелин Ројчев, Пловдив, Бугарија Nasya Tomlekova, Plovdiv, Bulgaria Насиа Томлекова, Пловдив, Бугарија Irena Rogelj, Ljubljana, Slovenia Ирена Рогељ, Љубљана, Словенија Drago Kompan, Ljubljana, Slovenia Драго Компан, Љубљана, Словенија Michael Murković, Graz, Austria Михаел Муркович, Грац, Австрија Hristaq Kume, Tirana, Albania Христаќ Куме, Тирана, Албаниа Sonja Srbinovska, Skopje, Macedonia Соња Србиновска, Скопје, Македонија Marjan Kiprijanovski, Skopje, Macedonia Марјан Кипријановски, Скопје, Македонија Marina Stojanova, Skopje, Macedonia Марина Стојанова, Скопје, Македонија Biljana Kuzmanovska, Skopje, Macedonia Билјана Кузмановска, Скопје, Македонија Mirjana Jankulovska, Skopje, Macedonia Мирјана Јанкуловска, Скопје, Македонија Dragi Dimitrievski, Skopje, Macedonia Драги Димитриевски, Скопје, Македонија JOURNAL OF AGRICULTURAL, FOOD AND ENVIRONMENTAL SCIENCES Address Адреса (Editorial Board) (Редакција) “Ss. Cyril and Methodius" University in Skopje Универзитет „Св. Кирил и Методиј“ во Скопје Faculty of Agricultural sciences and food-Skopje Факултет за земјоделски науки и храна ­ Скопје P.O. Box 297, MK-1000 Skopje, п. фах. 297, МК­1000 Скопје, Republic of Macedonia Република Македонија E-mail: [email protected] *THE AUTHORS ARE RESPONSIBLE FOR THE CONTENT AND FOR THE LANGUAGE OF THEIR CONTRIBUTION Journal of Agricultural, Food and Environmental Sciences ____________________________________________________________________________________________________ TABLE OF CONTENTS – СОДРЖИНА T. Eftimova - Tashevska, B. Petanovska - Ilievska, E. Dimitrieska - Stojkovik, L. Velkoska - Markovska COMMON NONCONFORMITIES DURING PROCEDURE FOR ACCREDITATION OF THE FOOD TESTING LABORATORIES IN THE R.MACEDONIA 1-10 L. Velkoska-Markovska, B. Petanovska-Ilievska, I. Stojanovska, M. S. Jankulovska SPE-RRLC DETERMINATION OF SOME PESTICIDE RESIDUES IN APPLE JUICE 11-17 M. S. Jankulovska , L. Velkoska-Markovska, B. Petanovska-Ilievska, S. Trpkovska HIGH-PERFORMANCE LIQUID CHROMATOGRAPHY METHOD FOR DETERMINATION OF PRESERVATIVES IN BEVERAGES 18-25 B. Petanovska-Ilievska , L.Velkoska-Markovska , I. Stojanovska , M. S. Jankulovska DEVELOPMENT OF HIGH SPEED RRLC METHOD FOR QUANTITATIVE DETERMINATION OF SOME PESTICIDE RESIDUES IN APPLE JUICE 26-32 A.Najdenoska DEVELOPMENT OF HPLC METHOD FOR ANALYSIS OF NITRITE AND NITRATE IN VEGETABLE 33-39 A. I. M. Loredana, T. T. Ioan, S. Daniela, R. Bogdan NUTRITIONAL VALUES OF PSEUDOCEREALS FLOUR MIXTURES USED IN GLUTEN-FREE SWEET BAKERY PRODUCTS 40-45 40-45 M. H. Elgammal, M. S.M. Hasanin ESTIMATION OF FURAN LEVELS IN SOME CANNED FOODS IN EGYPT AND HOW TO REDUCE IT 46-52 S. Sikder, P. Biswas, A. Chattopadhyay, P. Hazra ISOLATION OF PROMISING MUTANT OF ENHANCED FRUIT QUALITY IN TOMATO 53-58 D. Sylejmani, A. Hamidi INCIDENCE OF STAPHYLOCOCCUS AUREUS AND COAGULASE POSITIVE STAPH. AUREUS IN RAW MILK IN KOSOVO 59-61 JAFES, Vol 67 (2016) Journal of Agricultural, Food and Environmental Sciences ____________________________________________________________________________________________________ L. Velkoska-Markovska , B. Petanovska-Ilievska QUANTITATIVE DETERMINATION OF 2,4-D IN PESTICIDES MONOSAN HERBI AND DMA-6 62-67 C. Gözüaçık, A. Yiğit THE ALTERNATİVE HOSTS OF TRİSSOLCUS SPECİES, EGG PARASİTOİDS OF SUNN PEST AND HOST-PARAZİTOİD İNTERACTİONS İN SOUTH EASTERN ANATOLİA REGİON, TURKEY 68-74 M. Güllü, C. Gözüaçik, A. Konuksal, H. Hekimhan, H. Fidan THE DISTRIBUTION AND POPULATION DENSITY OF THE CEREAL WEEVIL, PACHYTYCHIUSHORDEI (BRULLÉ) (COLEOPTERA: CURCULIONIDAE) IN CEREAL FIELDS IN NORTHERN CYPRUS 75-81 JAFES, Vol 67 (2016) Journal of Agricultural, Food and Environmental Sciences UDC 338.246.027:006.83/.87:542.2(047.31) Original scientific paper ____________________________________________________________________________________________________ COMMON NONCONFORMITIES DURING PROCEDURE FOR ACCREDITATION OF THE FOOD TESTING LABORATORIES IN THE R.MACEDONIA T. Eftimova - Tashevska1*, B. Petanovska - Ilievska2, E. Dimitrieska - Stojkovik3, L. Velkoska - Markovska2 1Institute for Accreditation of the Republic of Macedonia 2Faculty of Agricultural Sciences and food, “Ss. Cyril and Methodius” University, Skopje, Republic of Macedonia 3Faculty of Veterinary Medicine, “Ss. Cyril and Methodius” University, Skopje, Republic of Macedonia *corresponding author: [email protected] Abstract During laboratory assessment in the frame of the accreditation procedure, they faced with number of nonconformities which are challenge for receiving the Certificate for accreditation and appropriate corrective measures shall be undertaken. Requirements that should be met by the food testing laboratories in the Republic of Macedonia, in order to gain accreditation certificate, contained in the standard МКС ENISO/IEC 17025:2006, ILAC (International Laboratory Accreditation Cooperation) document, ЕА (European Cooperation for Accreditation) document, Regulations and Procedures of the Institute for Accreditation of the Republic of Macedonia. In this paper the analysis is made and different proposals are given for the different ways of fulfilling of those requirements. The aim of this study is to emphasis the common nonconformities which are observed during realization of the Procedure of Accreditation of food testing laboratories and corrective measures undertaken. This investigation is of huge meaning for food testing laboratories which are already accredited and those which are planning to be accredited in the Republic of Macedonia. Furthermore, it is a very important for the Institute for accreditation of the Republic of Macedonia to come to conclusions for the weakest sides of the food testing laboratories and the assessment thereof. Such conclusions should initiate undertaking appropriate measures for improvement the Institute’s lead and technical assessors work towards nonconformities interpretation, identification and acceptance of the most suitable corrective measures. Key words: accreditation of food testing laboratories, common nonconformities, ISO/IEC 17025 Introduction proposals are given for the difеrent ways of During laboratory assessment in the frame of fullfiling of those requirements. the accreditation procedure, they faced with If a country’s industry could enter on the number of nonconformities which are global market, that country shall establish challenge for receving the Certificate for standards, technical regulations, metrology, accreditation and appropriate corrective testing, conformity assessment, certification measures shall be undertaken. Requirements and accreditation. All of these elements that should be met by the food testing consists the national quality infrastructure. laboratories in the Republic of Macedonia, in National quality infrastructure should provide order to gain accreditation certificate, approach to the international standards and contained in the standard МКС EN ISO/IEC technical regulation, to guarantee reliable 17025:2006, ILAC measures and to establish system for (InternationalLaboratoryAccreditationCoopera accreditation of the testing bodies and tion) document, ЕА (Europeanco- certification on the way that they are operationforAccreditation) document, international recognize. Regulations and Procedures of the Institute for The national quality infrastructure in the Accreditation of the Republic of Macedonia. Republic of Macedonia is consisting of: In this paper the analysis is made and difеrent Institute for Accreditation of
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