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Book of Abstracts and Program ETRADCHEM All ETRADCHEM Workshop 2017 23rd-24th March 2017. Villeurbanne, France 2017 Workshop « Electron Transfer, Radical Ions and Radical Chemistry ». March 23 and 24, 2017. Université Lyon 1 Campus LyonTech – La Doua 1 ETRADCHEM Workshop 2017 23rd-24th March 2017. Villeurbanne, France On behalf of the organizing committee, I warmly welcome you to this first Workshop edition that will focus on electron-transfer reactions and reactivity of radical ions and radicals. The program spans a range of topics of radical and electron-transfer processes in organic chemistry, electrochemistry, radical and electron-transfer induced polymerization processes, photo-electrochemistry, photoredox catalysis, catalysis and theory. This event will honor Professor John A. Murphy (University of Strathclyde, Glasgow, Scotland) who is an invited Professor at the Université Claude Bernard Lyon 1 from March 22 to April 20, 2017. I would like to express my sincere thanks to all members of the organizing committee for their continuous and enthusiastic efforts. The cellule financière of the ICBMS is also acknowledged for their help. I am also grateful to our generous institutional and industrial sponsors, who have made this event possible. I wish you all a very fruitful workshop and a pleasant stay in Lyon. Maurice MEDEBIELLE Organizing committee: Maurice Médebielle, Lionel Perrin, Paolo Larini and Anis Tlili. Université Claude Bernard Lyon 1, ICBMS UMR 5246. 2 ETRADCHEM Workshop 2017 23rd-24th March 2017. Villeurbanne, France GENERAL INFORMATION Location The workshop will take place at the CPE Lyon – Ecole Supérieure de Chimie Physique Electronique de Lyon Locate CPE building and Tramway stations LA DOUA GASTON BERGER and UNIVERSITE LYON 1: 3 ETRADCHEM Workshop 2017 23rd-24th March 2017. Villeurbanne, France To access the Université Claude Bernard Lyon 1 campus (La Doua) and location of the Workshop, please use tramway lines T1 (bound to IUT Feyssine) or T4 (bound to La Doua-Gaston Berger, Terminus) and get off at La Doua – Gaston Berger’s station. Both lines are connected to Part Dieu Railway Station (20-22 minutes). From Lyon Saint-Exupéry Airport, you can reach Part Dieu Railway Station using the Rhône- Express Train: https://www.rhonexpress.fr/en Transport Local public transport: http://www.tcl.fr 4 ETRADCHEM Workshop 2017 23rd-24th March 2017. Villeurbanne, France Internet Wifi access will be provided during the Workshop Working language The working language of the workshop is English SPONSORS 5 ETRADCHEM Workshop 2017 23rd-24th March 2017. Villeurbanne, France SCIENTIFIC PROGRAMME DAY 1 Thursday March 23 DAY 2 Friday March 24 8:30-9:10 Registration 8:30-8:55 Registration 9:15-9:30 Welcome 9:00-9:25 T. NOEL 9:30-10:00 J. A. MURPHY 9:30-9:55 B. KONIG 10:00-10:15 10:00-10:25 M. BRASHOLZ 10:20-10:45 S. ZARD 10:30-10:45 Break 10:50-11:15 Y. LANDAIS 10:50-11:15 M. E. BUDEN 11:20-11:45 L. FERAY 11:20-11:45 A. TLILI 11:50-12:15 C. OLLIVIER 11:50-12:15 M. PUIATTI 12:30-14:00 Lunch 12:30-14:00 Lunch 14:15-14:40 J. BROGGI 14:15-14:40 F. MASERAS 14:45-15:10 D. GIGMES 14:45-15:10 V. ROBERT 15:15-15:40 E. LACOTE 15:15-15:40 L. PERRIN 15:45-16:10 Break 15:45-16:10 Break 16:15-16:40 J. BONIN 16:15-16:45 Feedback 16:45-17:10 N. LE POUL 16:45-17:00 Farewell 17:15-17:40 C. BUCHER 17:45-18:10 M.-N. COLLOMB 19:45 Dîner Speakers PLENARY LECTURE John A. MURPHY (Glasgow, Scotland): Evolution of Organic Super Electron Donors INVITED LECTURES Samir ZARD (Ecole Polytechnique, Palaiseau): Radical-Polar Crossover: Manifold Implications for Synthesis Yannick LANDAIS (Université de Bordeaux, Bordeaux): Free-Radical Additions to Olefins. Recent Developments and Applications Laurence FERAY (Université d'Aix-Marseille, Marseille): α-Bromoacrylate as radical acceptor in dialkylzincs-mediated radical-polar crossover processes, theoretical investigation and synthetic applications 6 ETRADCHEM Workshop 2017 23rd-24th March 2017. Villeurbanne, France Cyril OLLIVIER (Université Pierre et Marie Curie, Paris): Photoredox Catalysis for the Generation of Carbon Centered Radicals and Synthetic Applications Julie BROGGI (Université d’Aix-Marseille, Marseille): New horizons for Organic Electron Donors Didier GIGMES (Université d’Aix-Marseille, Marseille): Photopolymerization initiators: Synthesis and photochemical studies Emmanuel LACOTE (Université Lyon 1, Villeurbanne): Organic and Polymer Free-radical Synthesis using NHC–Boranes Julien BONIN (Université Paris Diderot, Paris): Molecular Catalysis of the Photochemical Reduction of CO2 into CO and beyond: on the Road to Solar Fuels Nicolas Le POUL (Université de Brest, Brest): Surface functionalization by model complexes of copper enzymes: the “self-induced electroclick” approach Christophe BUCHER (ENS Lyon, Lyon): Electron-triggered metamorphism in viologen-based (supra)molecular materials Marie-Noëlle COLLOMB (Université Grenoble Alpes, Grenoble): Photo-induced redox catalysis for hydrogen production with molecular compounds Timothy NOEL (TU Eindhoven, Pays-Bas): Engineering of photocatalytic reactions in microreactors Burkhard KONIG (Université de Regensburg, Allemagne): Visible light photoredox catalysis with radical anions Malte BRASHOLZ (Université d'Hambourg, Allemagne): New photoredox-induced cascade reactions Maria Eugenia BUDEN (Université Nationale de Cordoba, Argentine): Photoinduced Electron Transfer in base-promoted Homolytic Aromatic Substitution and Related Systems. Is t-butoxide anion a key ingredient? Anis TLILI (Université Lyon 1, Villeurbanne): KOtBu promoted intermolecular cross-coupling through electron transfer Marcelo PUIATTI (Université Nationale de Cordoba, Argentine): “The Palme d'Or goes to ...". A search for the best functional for dealing with anionic organic species 7 ETRADCHEM Workshop 2017 23rd-24th March 2017. Villeurbanne, France Feliu MASERAS (Tarragone, ICIQ, Catalogne): Characterization of single electron steps in water oxidation through DFT calculations Vincent ROBERT (Université de Strasbourg, Strasbourg): Charge Transfer Processes: Prime Role of Optimized Molecular Orbitals Lionel PERRIN (Université Lyon 1, Villeurbanne): Exploring the reactivity of the Kagan’s reagent from a theoretical perspective 8 ETRADCHEM Workshop 2017 23rd-24th March 2017. Villeurbanne, France Evolution of Organic Super Electron Donors J. A. Murphy Department of Pure and Applied Chemistry, University of Strathclyde, 295 Cathedral Street, Glasgow G1 1XL, United Kingdom * [email protected] My research group has been fortunate to develop a number of simple organic electron donors, structurally related to enols, enolates and enamines; in this way, we have built upon the excellent pioneering work of many people including Bunnett,1 Rossi2 and Narasaka.3 Our starting point was to ask whether a neutral organic ground state molecule could reduce an aryl halide. The search for such a molecule led us to understand some of the factors that control the power and selectivity of organic electron donors, and their scope as reducing agents. 1,00E-05 5,00E-06 0,00E+00 -2,5 -2 -1,5 -1 -0,5 0 -5,00E-06 -1,00E-05 Current/ A Potential/ V -1,50E-05 Being coloured reagents, they readily absorb visible and near-UV light; this adds to their power as donors, and allows them to tackle even more challenging synthetic tasks. This presentation will give an overview of developments relating to these electron donors from our current perspective. References 1. Scamehorn, R. G.; Bunnett, J. F. J. Org. Chem. 1977, 42, 14491457. 2. Guastavino, J. V.; Rossi, R. A. J. Org. Chem. 2012, 77, 460472. 3. Narasaka, K. Pure & Appl. Chem. 1997, 69, 601604. 9 ETRADCHEM Workshop 2017 23rd-24th March 2017. Villeurbanne, France Professor JOHN A. MURPHY B.A. (Mod.), Ph.D., C. Chem., F.R.S.C., F.R.S.E. CURRICULUM VITAE http://www.johnmurphygroup.com/ 1. Name: John Anthony Murphy Nationality: Irish 2. University Education: 1972-1976 University of Dublin. Awarded B.A. (Moderatorship) First Class. Awards Held: Department of Education Scholar (1972-1976). University of Dublin Foundation Scholar (1974-1979). Goulding Scholar (1975); Gold Medallist of the University (1976); Cocker Medallist for Experimental Chemistry (1976). 1976-1979 University of Cambridge. (Hutchinson Research Studentship.) Awarded Ph.D. in Organic Chemistry (with Prof. Jim Staunton) 3. Appointments Held: 2013-2016 Head of Department 2007-2012 Director, Glasgow Centre for Physical Organic Chemistry 2010- to date Head of Organic Chemistry 2007-2013 Deputy Head of Department 2006-2008 Director, WestCHEM 2004-2006 Deputy Director, WestCHEM 1995- to date Merck-Pauson Professor, University of Strathclyde. 1994-1995 Reader, University of Nottingham. 1983-1994 Lecturer, University of Nottingham. 1982-1983 College Lecturer, Jesus College, Oxford. 1980-1983 Departmental Demonstrator, University of Oxford. with Prof. J. E. Baldwin on bioorganic chemistry. 1979-1980 Izaak Walton Killam Fellowship, University of Alberta 4. International and National Recognition: 2017 Visiting Professor, Université Claude Bernard (Lyon- 1) 2016 The Charles Rees Award for Heterocyclic Chemistry (Royal Society of Chemistry) 2013 Visiting Lectureship, University of Kyoto 2012 The Bader Award in Organic Chemistry (Royal Society of Chemistry) 2007 Visiting Fellow at the Australian National University. 2004 Visiting Professor, Université Pierre et Marie Curie, Paris 10 ETRADCHEM Workshop 2017 23rd-24th March 2017. Villeurbanne, France 2002 D.Sc. (University of Strathclyde) 2001 Presidential Visiting Professor, N.A.I.S.T., Japan. 2001 Elected Fellow of the Royal Society of Edinburgh 2001 Royal Society Leverhulme Senior Research Fellow 1999 Invited “Troisième Cycle” Lecturer, Switzerland. 1998 Elected Fellow of the Royal Society of Chemistry. 1996 Visiting Professor at l’Université d’Aix Marseille. 1995 Visiting Fellow at the Australian National University. I am an organic chemist and my research group revels in exploring chemical reactivity in synthesis and in biology. My research group website is http://www.johnmurphygroup.com/ We have a particular interest in electron transfer reactions and in radical chemistry, but are generally interested in mechanisms of organic reactions. 11 ETRADCHEM Workshop 2017 23rd-24th March 2017.
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