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Journal of Nehru Gram Bharati University ISSN-2319-9997 Volume: IV, Issue: 1 & 2, Year: 2015 Journal of Nehru Gram Bharati University Published By Nehru Gram Bharati Deemed to be University Allahabad, U.P. India www.ngbu.edu.in ISSN-2319-9997 Volume: IV, Issue: 1 & 2, Year: 2015 Journal of Nehru Gram Bharati University (A Biannually Published Peer Reviwed Journal) Editor-In-Chief Dr. Pravin Kumar Mishra Nehru Gram Bharati Deemed to be University Allahabad, 221505 U.P. India www.ngbu.edu.in Editorial Board Prof. K.P. Mishra (India) Prof. S. P. Mishra (India) Prof. M. R. Raju (India) Prof. Mohi Rezvani (U.K.) Prof. Carmel E. Mothersill (Canada) Prof. J. K. Kim (Sauth Korea) Prof. H. Mastsumoto (Japan) Prof. S. G. Praksh (India) Prof. R. P. Mishra (India) Prof. Prabuddha Ram Mishra (U.S.) Prof. Kazuo Suzuki (Japan) Prof. C. Rudowicz (Poland) Prof. B. N. Pandey (India) Prof. U. V. Desai (India) Prof. S. Mitaku (Japan) Prof. G. Safrany (Hungry) Prof. Anna Giovanetti (Italy) Prof. R. P. Hill (Canada) ISSN-2319-9997 Journal of Nehru Gram Bharati University (A Biannually Published Peer Reviwed Journal) Volume: IV, Issue: 1 & 2, Year: 2015 Contents ¾ Synthesis and Spectral Studies of [(RR Se)2.L] complexes with bidentate Schiff base ligand Ghanshyam Mani Mishra & Shekhar Srivastava 5-7 ¾ Legality to Keep and Bear the Arms in India Anil kumar 8-21 ¾ Women’s Quest for Self-Identity in India R.C.Mishra 22-26 ¾ Study of learning style and attitude of the students towards social media uses Nidhi Mishra & Ajay Prakash Tiwari 27-31 ¾ Development of Science & Technology in Ancient India – With Special Reference to Harappan Civilization Devendra Pratap Mishra 32-35 ¾ R.K. Narayan as the best Indian writer Chhaya Malviya 36-40 ¾ Naxalite Movement: Problems and Solutions (A Study Based On Naxalite Literature) Abhishek Tripathi 41-58 ¾ Teacher’s stress and burnout of elementary schools Pranita Mishra & Abhishek Tripathi 59-68 ¾ A Review on Human Rights in Agriculture & Rural Sector Himansu Dwivedi 69-76 ¾ orZeku ifjçs{; esa ;ksx dh çklafxdrk yky pUn 'kqDy 77-82 ¾ fo}Uef.k çks0 ds'kopUænk”k dh dforkvksa esa vk/kqfud ;qxcks/k ¼muds dkO; laxzg bZ'kk ds fo'ks"k lUnHkZ easa½ cfcrk fueZy 83-87 ¾ vYcVZ vkbaLVhu jktsUnz izlkn xqIrk 88-91 ¾ Rkqylh ds dkO; esa leUo;okn Ekerk feJk 92-95 ¾ iapk;rh jkt O;oLFkk ,oa tulgHkkfxrk c`ts'k dqekj flag 96-102 ¾ vk/kqfud Hkkjr vkSj nfyr vkUnksyu fofiu dqekj flag ,oa larks"k dqekj flag 103-107 ¾ xaxk laj{k.k ,oa lekt dk;Z Kkus'k dqekj f=osnh 108-110 ¾ Hkkjr esa vkS|ksfxd fodkl t;sUnz flag 111-116 ¾ xk¡/kh ds f'k{kk&n'kZu dh izklafxrk e/kq frokjh 117-121 ¾ mPp f'k{kk Lrj ij foÙkiksf"kr ,oa LofoÙkiksf"kr egkfo|ky;ksa esa v/;kiujr f'k{kdksa ds lek;kstu {kerk dk rqyukRed v/;;u jk?kosUnz ekyoh; ,oa vfouk'k ik.Ms; 122-129 ¾ Hkkjr esa ekuokf/kdkj % bfrgkl ,oa fodkl vfuy dqekj ekS;Z 130-134 ¾ Jh yky 'kqDy % lkekftd ljksdkj vuwi dqekj 135-140 ¾ 'kS{kkf.kd fØ;kdykiksa esa lkfgfR;d pksjh vkyksd dqekj f=ikBh ,oa lqjsUnz flag ;kno 141-145 ¾ Jheöxon~xhrk esa fufgr ;ksx ds Lo:i dk fo'ys"k.k rq"kkj jatu 146-148 ¾ f'k{kk ds futhdj.k dk vkSfpR; Jo.k dqekj ,oa ehuw ik.Ms; 149-154 ¾ Protectional Measures for the Safety of Human Health from Narcotic Drugs and Psychotropic Swapnil Tripathi 155-178 All the visions, thoughts and opinions published in JNGBU are of contributors. The acceptance of the Editor is not mandatory. ISSN-2319-9997 / Volume: IV / Issue: 1 & 2 / Year: 2015 Synthesis and Spectral Studies of [(RR Se)2.L] complexes with bidentate Schiff base ligands - Ghanshyam Mani Mishra & Shekhar Srivastava Abstract : Complexes of the type [(RR'Se)2L] (Where R=R'=CH3, R=R'=n-C4H9; R=R'= n-C8H17; R=R'=i-C3H7; R=R'= C6H5, R= C6H5 R' = C2H5; R'= CH3 R = C6H5 R'= C2H5, R'= CH2Cl and L = bidentate Schiff base ligands) have been synthesised and characterised by elemental analysis, molar conductivity, IR and XPS data. A trigonal bipyramidal geometry has been assigned to all these metal complexes. Experimental- Eight RR'Se [Where R =R' = CH3, R =R'= n- C4H9; R=R' =n-C8H17; R =R' = i-C3H7; R=R' = C6H5R' = C2H5; R' = CH3 R = C6H5 R' = C2H5,R' = CH2Cl] have been prepared as given in chapter II. Preparation Of Bidentate Sehiff Base Ligands; 2 mmol of 2- acetylpyrrole or 2- pyrrole carboxyaldehyde or 2- pyridylcarboxyaldehyde or 2-naphthyladehyde in 2ml dry chloroform was refluxed withh 1 mmol of cyclohexanediamine for about 3-hrs. The resulting solids were filtered, washed and purified and air-dired. It was further analysed by elemental analysis. Thus following four Schiff base ligands are prepared. Jouranal of Nehru Gram Bharati University 5 ISSN-2319-9997 / Volume: IV / Issue: 1 & 2 / Year: 2015 Preparation Of [RR'Se.L] Complexes: 1 mmol of RR'Se in dry choloroform was refluxed with 1 mmol of any prepared ligand (L) for about 3 hrs. The resulting mixture was rotory evaporated and concentrated. Solution was kept in deep freeze overnight. The product was obtained, washed with pet ether and vacuum dried. Results and Discussion: These new molecular adducts have been synthesized by the interaction of RR'Se with various bidentate ligands (L) in chloroform. RR'Se + L [RR'Se.L] (i) Elemental Analysis - were found within ± 0.5% suffested [[RR'Se.L] molecular formula. (ii) Molar Conductivity -20-30 ohm-1 cm2 mol-1 in acetone suggested non - electrolyte nature. (iii) Ir: >C=N Ligand ~ 1610-1620 Cm-1 Suggested Coordination of>C=NgP in metal complex - N=230-206 cm-1 present υ -N=410-420 cm-1 present (iv) XPS-data Complex 1 Se3p 2 (CH3)2 Se 168.6 1 (CH3)2 Se.L 167.6 2 (CH3)2 Se.L 167.6 3 (CH3)2 Se.L 167.6 Decrease in BE Se3P1/2 in metal complexes suggested electron density is increasing on se metal ion. Sr. No. Ligand & compound N1S 1. Ligand L1 401.4 1 2. (CH3)2Se.L 402.6 3. (n-C4H9)2Se.L1 102.6 1 4. (n-C8H17)2Se.L 402.6 increase in N1BE in metal complexes than ligand and only one symmetrical suggested coordination of all two nitrogen atoms with se metal ion. On the basis of above geometry. Jouranal of Nehru Gram Bharati University 6 ISSN-2319-9997 / Volume: IV / Issue: 1 & 2 / Year: 2015 assigned distorted octahedral. References : 1. J.J. Berzelium, Fvs. Kemi Mineralogi, 1818, 6, 42. 2. C.J. Lowig, Pogg. Ann, 1836, 37, 552. 3. The Chemistry of Organic Selenium and tellurium compounds Eds. S. Patai and Z. Rappoport. Wiley, Chichester, 1986, vol. 1; 1987, vol. 2. 4. Selenium in Biology and Human Health, Ed. R.F. Buck. Sprinter-Verlag, New York, 1994 and references therein. 5. S. Yamashita, Y. Moro, and H. Sasaki, Jpn. Kokai Tolyo loho JP, 0545, 772[9345, 772] 9Cl. GO3Ci/09) (Chem. Abs. 194, 120, 231749p). 6. M. Boeluman, Chem. Vap. deposition. 1996, 2, 85 and references therein. 7. E.G. hope and wilevason, Coord. Chem. Rev. 1993, 122, 109. 8. F. Kacer, Ger. Put. 557, 249 (Chem. Abst. 1993, 27, 304). 9. T. Wirth, tetrahedron, 1999, 55; land reference therein. 10. J. Arnold, "The Chemistry of Metal complexes with Selenolate and Tellurolate ligands' in Progress in Inorganic Chemistry, Ed. K.C. Karlin, John, Wiley & Sons, Inc. 1995, vol. 453, p., 353. 11. M.K. Davies, M. Dalton Trans., 1999, 1077. 12. A. Bock, 'Selenium Proteins containing Selenocysteine' in Encyclope dia of Inorganic Chemistry, Ed. R.B. King, John Wiley & Sons, Chichester, England, 1994, vol. 8, p. 3700. 13. Shekhar Srivastava, Appl. Spectroscopy Rev., 22(4), 401, 1986. Dr. Ghanshyam Mani Mishra and Prof. Shekhar Srivastava Ph.D., Department of Chemistry University of Allahabad Allahabad – 211002, INDIA Jouranal of Nehru Gram Bharati University 7 ISSN-2319-9997 / Volume: IV / Issue: 1 & 2 / Year: 2015 Legality to Keep and Bear the Arms in India - Anil kumar "To avoid domestic tyranny, the people must be armed to stand upon [their] own Defense; which if [they] are enabled to do, [they] shall never be put upon it, but [their] Swords may grow rusty in [their] hands; for that Nation is surest to live in Peace, that is most capable of making War; and a Man that hath a Sword by his side, shall have least occasion to make use of it.""The right of self-defense is the first law of nature; in most governments it has been the study of rulers to confine this right within the narrowest possible limits...and [when] the right of the people to keep and bear arms is, under any color or pretext whatsoever, prohibited, liberty, if not already annihilated, is on the brink of destruction." – Sir George Tucker1 Introduction- A weapon, arm, or armament is any device used with intent to inflict damage or harm to living beings, structures, or systems. Weapons are used to increase the efficacy and efficiency of activities such as crime, law enforcement, self-defense, and warfare. In a broader context, weapons may be construed to included anything used to gain a strategic, material or mental advantage over on adversary. While just about any ordinary objects such as sticks, stones, cars, or pencils can be used as weapons many are expressly designed for the purpose ranking from simple implements such as clubs, swords and guns, and to complicated modern intercontinental ballistic missiles, biological and cyber weapons.
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