Formula of a Compound
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Separation of Fluoride Residue Arising from Fluoride Volatility Recovery of Uranium from Spent Nuclear Fuel
University of Tennessee, Knoxville TRACE: Tennessee Research and Creative Exchange Masters Theses Graduate School 5-2004 Separation of Fluoride Residue Arising from Fluoride Volatility Recovery of Uranium from Spent Nuclear Fuel Jennifer L. Ladd-Lively University of Tennessee - Knoxville Follow this and additional works at: https://trace.tennessee.edu/utk_gradthes Part of the Chemical Engineering Commons Recommended Citation Ladd-Lively, Jennifer L., "Separation of Fluoride Residue Arising from Fluoride Volatility Recovery of Uranium from Spent Nuclear Fuel. " Master's Thesis, University of Tennessee, 2004. https://trace.tennessee.edu/utk_gradthes/2557 This Thesis is brought to you for free and open access by the Graduate School at TRACE: Tennessee Research and Creative Exchange. It has been accepted for inclusion in Masters Theses by an authorized administrator of TRACE: Tennessee Research and Creative Exchange. For more information, please contact [email protected]. To the Graduate Council: I am submitting herewith a thesis written by Jennifer L. Ladd-Lively entitled "Separation of Fluoride Residue Arising from Fluoride Volatility Recovery of Uranium from Spent Nuclear Fuel." I have examined the final electronic copy of this thesis for form and content and recommend that it be accepted in partial fulfillment of the equirr ements for the degree of Master of Science, with a major in Chemical Engineering. Robert M. Counce, Major Professor We have read this thesis and recommend its acceptance: Barry B. Spencer, Paul Bienkowski, Fred Weber Accepted for the Council: Carolyn R. Hodges Vice Provost and Dean of the Graduate School (Original signatures are on file with official studentecor r ds.) To the Graduate Council: I am submitting herewith a thesis written by Jennifer L. -
Chemistry: the Molecular Nature of Matter and Change
REVISED CONFIRMING PAGES The Components of Matter 2.1 Elements, Compounds, and 2.5 The Atomic Theory Today 2.8 Formula, Name, and Mass of Mixtures: An Atomic Overview Structure of the Atom a Compound 2.2 The Observations That Led to Atomic Number, Mass Number, and Binary Ionic Compounds an Atomic View of Matter Atomic Symbol Compounds That Contain Polyatomic Mass Conservation Isotopes Ions Definite Composition Atomic Masses of the Elements Acid Names from Anion Names Multiple Proportions 2.6 Elements: A First Look at the Binary Covalent Compounds The Simplest Organic Compounds: Dalton’s Atomic Theory Periodic Table 2.3 Straight-Chain Alkanes Postulates of the Atomic Theory Organization of the Periodic Table Masses from a Chemical Formula How the Atomic Theory Explains Classifying the Elements Representing Molecules with a the Mass Laws Compounds: An Introduction 2.7 Formula and a Model to Bonding 2.4 The Observations That Led to Mixtures: Classification and the Nuclear Atom Model The Formation of Ionic Compounds 2.9 Separation Discovery of the Electron and The Formation of Covalent An Overview of the Components of Its Properties Compounds Matter Discovery of the Atomic Nucleus (a) (b) (right) ©Rudy Umans/Shutterstock IN THIS CHAPTER . We examine the properties and composition of matter on the macroscopic and atomic scales. By the end of this chapter, you should be able to • Relate the three types of matter—elements or elementary substances, compounds, and mixtures—to the simple chemical entities that they comprise—atoms, ions, and molecules; -
Ionic Conductivity of Calcium and Strontium Fluorides
https://ntrs.nasa.gov/search.jsp?R=19670008817 2020-03-24T02:21:12+00:00Z View metadata, citation and similar papers at core.ac.uk brought to you by CORE provided by NASA Technical Reports Server IONIC CONDUCTIVITY OF CALCIUM AND STRONTIUM FLUORIDES I \ by William L. Fielder i \ i Lewis Research Center Cleveland, Ohio NATIONAL AERONAUTICS AND SPACE ADMINISTRATION WASHINGTON, D. C. FEBRUARY 1967 TECH LIBRARY KAFB, NM 0130483 IONIC CONDUCTIVITY OF CALCIUM AND STRONTIUM FLUORIDES By William L. Fielder Lewis Research Center Cleveland, Ohio NATIONAL AERONAUTICS AND SPACE ADMINISTRATION For sale by the Cleoringhouse for Federal Scientific and Technical Information Springfield, Virginio 22151 - Price $1.00 I IONIC CONDUCTIVITY OF CALCIUM AND STRONTIUM FLUORIDES by William L. Fielder Lewis Research Center SUMMARY The conductivities of single crystals of calcium and strontium fluoride were deter mined. In the extrinsic region (impurity controlled), the specific conductivity of each crys tal may differ. The extrinsic conductivities KI for the normal process of point-defect migration for two calcium fluoride (CaF2) crystals (A and B) between 430' and 535' C were as follows (in ohm-' cm-l): for A, KI = 1.11*0. O1xlO-l exp - (16 50&100/RT) and for B, KI = 1.21*0. OIXIO-l exp - (16 500*100/RT) where R is the gas constant (cal/(deg)(mole)) and T is the absolute temperature (deg). The extrinsic conductivity of strontium fluoride (SrF2) between 360' and 410' C was KI = 1.22&0.05X10-2 exp - (17 40&900/RT). Only one intrinsic region was observed for two calcium fluoride crystals between 645' and 830' C or for strontium fluoride between 580' and 760' C. -
Chemical Chemical Hazard and Compatibility Information
Chemical Chemical Hazard and Compatibility Information Acetic Acid HAZARDS & STORAGE: Corrosive and combustible liquid. Serious health hazard. Reacts with oxidizing and alkali materials. Keep above freezing point (62 degrees F) to avoid rupture of carboys and glass containers.. INCOMPATIBILITIES: 2-amino-ethanol, Acetaldehyde, Acetic anhydride, Acids, Alcohol, Amines, 2-Amino-ethanol, Ammonia, Ammonium nitrate, 5-Azidotetrazole, Bases, Bromine pentafluoride, Caustics (strong), Chlorosulfonic acid, Chromic Acid, Chromium trioxide, Chlorine trifluoride, Ethylene imine, Ethylene glycol, Ethylene diamine, Hydrogen cyanide, Hydrogen peroxide, Hydrogen sulfide, Hydroxyl compounds, Ketones, Nitric Acid, Oleum, Oxidizers (strong), P(OCN)3, Perchloric acid, Permanganates, Peroxides, Phenols, Phosphorus isocyanate, Phosphorus trichloride, Potassium hydroxide, Potassium permanganate, Potassium-tert-butoxide, Sodium hydroxide, Sodium peroxide, Sulfuric acid, n-Xylene. Acetone HAZARDS & STORAGE: Store in a cool, dry, well ventilated place. INCOMPATIBILITIES: Acids, Bromine trifluoride, Bromine, Bromoform, Carbon, Chloroform, Chromium oxide, Chromium trioxide, Chromyl chloride, Dioxygen difluoride, Fluorine oxide, Hydrogen peroxide, 2-Methyl-1,2-butadiene, NaOBr, Nitric acid, Nitrosyl chloride, Nitrosyl perchlorate, Nitryl perchlorate, NOCl, Oxidizing materials, Permonosulfuric acid, Peroxomonosulfuric acid, Potassium-tert-butoxide, Sulfur dichloride, Sulfuric acid, thio-Diglycol, Thiotrithiazyl perchlorate, Trichloromelamine, 2,4,6-Trichloro-1,3,5-triazine -
While There Are Many Thousands of Different Chemical Compounds There
NAMING CHEMICAL COMPOUNDS & WRITING CHEMICAL FORMULAS While there are many thousands of different chemical compounds there is a very definite system of nomenclature whereby we can name or write chemical formulas for most compounds. We divide the compounds into two main types – binary compounds and ternary compounds. I. Binary Compounds All true binary compounds contain only two elements. The name of every binary compound ends with “ide.” Binary compounds come in three types. They are: Type I ………. the metal forms only one type of cation Type II ……… the metal forms two or more types of cations Type III …….. contains only nonmetals We will look at each type, one at a time. Type I Binary Compounds For Type I binary compounds the metal present can be found in either Group 1 or Group 2 on the periodic table. The naming system for this type of compound is quite simple and is found below. Rules for naming Type I binary compounds 1. The cation is always name first and the anion second. 2. A simple cation (obtained from a single atom) takes its name from the name of the element. 3. A simple anion (obtained from a single atom) is named by taking the first part of the element name (the root) and adding the letters “IDE.” 4. Write the name for the compound by combining the names of the ions. When naming Type I binary compounds: name of first element root + ide The root is merely an abbreviation for the name of the second element. The roots of the most commonly used elements are listed in the following table. -
United States Patent Office Patented Dec
3,481,871 United States Patent Office Patented Dec. 2, 1969 1. 3,481,871 DTHOETHANE, DERVATIVES AND ORGANIC COMPOSTIONS CONTAINING THE SAME Herbert Myers, Barrington, and Alfred P. Kozacik, Woodbury, N.J., assignors to Mobil Oil Corpo ration, a corporation of New York No Drawing. Filed Apr. 24, 1967, Ser. No. 632,907 Int. CI. C10m 1/38, 3/32; C07c. 149/12 U.S. C. 252-45 2 Claims O and ABSTRACT OF THE DISCLOSURE Novel organo-sulfur derivatives are produced by re acting a mercaptain with a sulfur chloride compound, reacting the resulting organic sulfenyl or thiosulfenyl 5 chloride with an olefin, and finally reacting the resulting SSR, product with a metal sulfur-containing salt. The final product may be used in lubricating oils and other in wherein R, R2, and x have the above definitions, and X dustrial fluids as a load-carrying additive. is oxygen or sulfur, Y is oxygen, sulfur or nitrogen and 20 R is hydrogen, or alkyl, cycloalkyl, aralkyl, aryl or alkaryl having from 1 to 20 carbon atoms. Rb may also FIELD OF INVENTION contain nitrogen, oxygen- or sulfur-containing Substi This invention relates to organic compositions con tletS. taining novel organo-sulfur derivatives of dithioethanes, and to a method of producing these derivatives. 25 DESCRIPTION OF SPECIFIC EMBODIMENTS PRIOR ART The products of this invention are produced by react In U.S. Patents Nos. 2,708,199 and 2,886,593, specific ing (1) a mercaptan, RSH, with (2) a sulfur halide. The sulfur compounds have been disclosed. In the first-named resulting organosulfenyl halide is then reacted with (3) patent, there is disclosed a method of producing organic 3) an olefin, CRR2=CHP, to produce an organo thioethyl polysulfides by reacting an olefin having from 6 to 30 halide intermediate. -
Strontium Fluoride (Srf2)
Strontium Fluoride (SrF2) MICHAEL E, THOMAS Applied Physics Laboratory The Johns Hopkins University Laurel, Maryland Strontium fluoride offers a wide range of transparency, from the ultravio- let to the long-wave infrared (0.13 to 11 /zm), with low reflectance loss and low dispersion. This combination of broad transparency and low dispersion is rare in optical-window materials used in infrared systems. Like BaF 2, it allows experimenters to conveniently perform initial system alignment in the visible and then switch to the IR with only minor correction of the optical components. Furthermore, strontium fluoride has good surface hardness (Knoop scale 150 kg/mm 2) and is not hygroscopic. It has a flexure strength between those of CaF 2 (90 MPa) and BaF 2 (27 MPa). Strontium fluoride is a cubic crystal with the fluorite structure, space group Fm3m (Oh),5 with four formula units per unit cell. The lattice constant is 5.7996 A, giving a theoretical density of 4.277 g/cm 3. The atomic arrange- ment is strontium atoms occupy the 4(a) sites (m3m or Oh symmetry), and the fluorine atoms occupy the 8(c) sites (43m or Ta symmetry). Melting point is 1750 K. Ultraviolet reflectance of bulk SrF 2 was measured by Ganin et al. [ 1] up to 20 eV at room temperature and liquid-helium temperature. Rubloff [2] measured the room-temperature reflectance up to 36 eV. Unfortunately, these measurements are not reduced to optical constants. However, similar mea- surements from 10 to 36 eV by Nisar and Robin [3] have been reduced to optical constants using the Kramers-Kronig relation. -
Unit 10 Chemical Formulas and Valence
Unit 10 Chemical Formulas and Valence INTRODUCTION The formula of a compound describes the exact composition of a molecule of the compound. These formulas oftentimes were determined by tedious analysis of the compound itself. A simpler method of determining the chemical formula of a compound is to use the concept of valence. This method makes it much easier to predict the formulas for compounds even if we do not have a sample of the compound to physically work with. OBJECTIVES 1. The student will define or identify the terms associated with valence as described in this unit. 2. The student will assign valence to atoms and radicals using the rules given in this unit and a Periodic Chart. 3. The student will use valence to write the correct formula for a compound. DISCUSSION A. Valence The valence of an atom or group of atoms is a number that indicates the charge that an atom or group of atoms has when involved in a compound. The charge may be positive or negative and have values as low as a negative four (-4) to a positive seven (+7). Atoms or groups of atoms with a positive valence are called cations. Atoms or groups of atoms with a negative valence are called anions. The valence of an atom is related to the number of valence electrons and thus to the position of an atom on the Periodic Chart. The valence is written as a superscript to the atom. The number is preceded by a sign to indicate whether the valence is positive (+) or negative (-). -
Feasibility Study for the Processing of Hanford Site Cesium and Strontium Isotopic Sources in the Hanford Waste Vitrification Plant
WHC-EP-0460 Feasibility Study for the Processing of Hanford Site Cesium and Strontium Isotopic Sources in the Hanford Waste Vitrification Plant Prepared for the U.S. Department of Energy Office of Environmental Restoration and Waste Management Westinghouse ® HanfOIti Company Richland. Washington Hanford Operations and Engineering Contractor for the U.S. Department of Energy under Contract DE-AC06-87RL10930 Approved for Public Release DlfnmUTlON OF THIS OOCUBEMT IS UMLlWTEtt LEGAL DISCLAIMER This report was prepared as an account of work sponsored by an agency of the United States Government. Neither the United States Government nor any agency thereof, nor any of their employees, nor any of their contractors, subcontractors or their employees, makes any warranty, express or implied, or assumes any legal liability or responsibility for the accuracy, completeness, or any third party's use or the results of such use of any information, apparatus, product, or process disclosed, or represents that Its use would not infringe privately owned rights. Reference herein to any specific commercial product, process, or service by trade name, trademark, manufacturer, or otherwise, does not necessarily constitute or imply its endorsement, recommendation, or favoring by the United Stales Government or any agency thereof or its contractors or subcontractors. The views and opinions of authors expressed herein do not necessarily state or reflect those of the United States Government or any agency thereof. This report has been reproduced from the best available copy. Available in paper copy and microfiche. Available to the U.S. Department of Energy and its contractors from Office of Scientific and Technical Information P.O. -
(CDR) by CASRN Or Accession Number
List of Chemicals Reported for the 2012 Chemical Data Reporting (CDR) by CASRN or Accession Number For the 2012 CDR, 7,674 unique chemicals were reported by manufacturers (including importers). Chemicals are listed by CAS Registry Number (for non-confidential chemicals) or by TSCA Accession Number (for chemicals listed on the confidential portion of the TSCA Inventory). CASRN or CASRN or ACCESSION ACCESSION NUMBER CA INDEX NAME or GENERIC NAME NUMBER CA INDEX NAME or GENERIC NAME 100016 Benzenamine, 4-nitro- 10042769 Nitric acid, strontium salt (2:1) 10006287 Silicic acid (H2SiO3), potassium salt (1:2) 10043013 Sulfuric acid, aluminum salt (3:2) 1000824 Urea, N-(hydroxymethyl)- 10043115 Boron nitride (BN) 100107 Benzaldehyde, 4-(dimethylamino)- 10043353 Boric acid (H3BO3) 1001354728 4-Octanol, 3-amino- 10043524 Calcium chloride (CaCl2) 100174 Benzene, 1-methoxy-4-nitro- 100436 Pyridine, 4-ethenyl- 10017568 Ethanol, 2,2',2''-nitrilotris-, phosphate (1:?) 10043842 Phosphinic acid, manganese(2+) salt (2:1) 2,7-Anthracenedisulfonic acid, 9,10-dihydro- 100447 Benzene, (chloromethyl)- 10017591 9,10-dioxo-, sodium salt (1:?) 10045951 Nitric acid, neodymium(3+) salt (3:1) 100185 Benzene, 1,4-bis(1-methylethyl)- 100469 Benzenemethanamine 100209 1,4-Benzenedicarbonyl dichloride 100470 Benzonitrile 100210 1,4-Benzenedicarboxylic acid 100481 4-Pyridinecarbonitrile 10022318 Nitric acid, barium salt (2:1) 10048983 Phosphoric acid, barium salt (1:1) 9-Octadecenoic acid (9Z)-, 2-methylpropyl 10049044 Chlorine oxide (ClO2) 10024472 ester Phosphoric acid, -
Metal Fluorides Produced Using Chlorine Trifluoride Gas
Journal of Surface Engineered Materials and Advanced Technology, 2015, 5, 228-236 Published Online October 2015 in SciRes. http://www.scirp.org/journal/jsemat http://dx.doi.org/10.4236/jsemat.2015.54024 Metal Fluorides Produced Using Chlorine Trifluoride Gas Hitomi Matsuda1, Hitoshi Habuka1*, Yuuki Ishida2, Toshiyuki Ohno3 1Department of Chemical and Energy Engineering, Yokohama National University, Yokohama, Japan 2National Institute of Advanced Industrial Science and Technology, Tsukuba, Japan 3FUPET, Tsukuba, Japan Email: *[email protected] Received 12 September 2015; accepted 26 October 2015; published 29 October 2015 Copyright © 2015 by authors and Scientific Research Publishing Inc. This work is licensed under the Creative Commons Attribution International License (CC BY). http://creativecommons.org/licenses/by/4.0/ Abstract For developing coating materials, the fluorides of scandium, lanthanum, strontium, barium, mag- nesium and aluminum were produced from their oxides and chlorides by means of exposure to chlorine trifluoride gas at temperatures between room temperature and 700˚C. The metal chlo- rides could be easily fluorinated even at room temperature, while the metal oxides required tem- peratures higher than 300˚C. After the heating in ambient hydrogen at 1100˚C, the fluorides of lanthanum and barium showed very low weight losses at 1100˚C, although the weights of the other fluorides significantly decreased. These materials may work as protective films against corrosive and high temperature environments, particularly when using the chlorine trifluoride gas. Keywords Metal Fluoride, Metal Oxide, Chlorine Trifluoride, Synthesis, Coating Film Material 1. Introduction Chemical vapor deposition (CVD) can produce various high quality and functional material films [1]. In the CVD reactor, a film is formed not only on the substrate surface, but also on the surface of various reactor parts, such as the susceptor, gas distributor and exhaust. -
SDS (E-Mail): [email protected] Emergency Phone Number: Poison Emergency Call 1-800-222-1222 (Anywhere in the US) CHEMTREC Tel
Doxa Dental AB Ceramir ® Crown & Bridge QuikCap SAFETY DATA SHEET Section 1: Identification Day of issue: 2017-04-07 Product identifier: Ceramir ® Crown & Bridge QuikCap Recommended use of the chemical and restrictions on use: Dental cement intended for permanent cementation of restorations. Uses advised against: Applications other than the intended use. Details of the supplier of the safety data sheet: Manufacturer: US importer: Doxa Dental Doxa Dental Inc. Axel Johanssons gata 4-6 Tel.: +46 (0) 18 478 20 00 1(855)Doxa – USA (369-2872) SE-754 50 Uppsala www.ceramirUS.com SWEDEN Responsible for SDS (e-mail): [email protected] Emergency phone number: Poison Emergency call 1-800-222-1222 (anywhere in the US) CHEMTREC Tel. No.US: 1-800-424-9300 Section 2: Hazard(s) identification The product is not controlled under GHS or OSHA Hazard Communication Standard, 29 CFR 1910.1200, but under Federal Food, Drug, and Cosmetic Act as Medical Device. The labelling text is therefore shown below for safety purposes. Classification of the chemical: None Signal word None Pictogram(s)/Symbol(s) None Hazard statement(s) None. Precautionary statement(s) None Other hazards not otherwise classified: Do not use in patients who have an allergy to polyacrylic acid. In very rare cases, the product may cause hypersensitivity symptoms in some patients. Discontinue use of the product if such symptoms occur and consult a doctor. Ingredients with unknown acute toxicity: Not relevant. Section 3: Composition/Information on Ingredients Mixtures: The product consist of a powder base and a liquid base enclosed in a capsule (content 0.5 g).