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MAGNETICALLY IMPELLED ARC BUTT (MIAB) OF CHROMIUM- PLATED TUBULAR COMPONENTS UTILIZING ARC VOLTAGE MONITORING TECHNIQUES

DISSERTATION

Presented in Partial Fulfillment of the Requirements for the Degree Doctor of

Philosophy in the Graduate School of The Ohio State University

By

David H. Phillips, M.S.W.E

*****

The Ohio State University 2008

Dissertation Committee:

Professor Charley Albright, Advisor Approved by

Professor Dave Dickinson ______Professor John Lippold Advisor Welding Engineering Graduate Program

ABSTRACT

Magnetically Impelled Arc Butt (MIAB) welding is a technique which generates uniform heating at the joint through rapid rotation of an arc. This rotation results from forces imposed on the arc by an external magnetic field. MIAB welding is used extensively in Europe, but seldom utilized in the United States. The

MIAB equipment is robust and relatively simple in design, and requires low upset pressures compared to processes like .

In the automotive industry, tubular construction offers many advantages due to the rigidity, light weight, and materials savings that tubes provide. In the case of automotive suspension components, tubes may be chromium-plated on the ID to reduce the erosive effects of a special damping fluid. Welding these tubes using the

MIAB welding process offers unique technical challenges, but with potential for significant cost reduction vs. other welding options such as Friction welding. Based on published literature, this research project represented the first attempt to MIAB weld chromium-plated steel tubes, and to utilize voltage monitoring techniques to assess weld quality.

ii Optical and SEM microscopy, tensile testing, and an ID bend test technique were all used to assess the integrity of the MIAB weldments. This analysis revealed the potential for chromium-enriched regions, most likely chromium , to become trapped at the weld interface resulting in severe degradation of mechanical properties. Voltage plots generated during the arc monitoring were analyzed and correlated with Design of Experiment (DOE) statistical results and high speed video images.

The DOE results revealed the individual and interactive importance of arc heating (referred to as level II) time, expulsion (referred to as level III) current, and arc gap on weld quality. Correlations were established between specific features of the arc voltage plots and weld quality. Based on arc physics theory, it was proposed that these three variables affected arc pressure, which contributed to improved expulsion and a reduction in chromium entrapment in the joint. As a result, feasibility for MIAB welding chrome-plated suspension components was established, and voltage monitoring methodology was identified as a potential quality control technique for producing this joint.

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Dedicated to my parents, whose guidance and unwavering support has always propelled me through the difficult times in my life, and my sister Barbara, who has been my “guiding light” throughout adulthood

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ACKNOWLEDGMENTS

I would like to thank my advisor, Professor Charley Albright, for first providing me with the opportunity to pursue a PhD, and then supporting and encouraging me throughout the process, while always allowing me some measure of independence.

I am grateful to my good friend, Dr. Anthony Ananthanarayanan, for all of his moral, technical, and financial support throughout most of my PhD studies, and for allowing me the flexibility to pursue this degree while simultaneously working at

Delphi.

I am thankful to Delphi for providing most of the financial support during my

PhD. A special thank you goes out to Tom McCray and Jule Hegwood, who spent countless hours helping me with the DOE and statistical analysis aspect of this research.

I would also like to thank Dr. Vladimir Kachinskiy who provided valuable technical insight.

v

VITA

March 6, 1961 ……………...... Born – Chillicothe, Ohio

1984 ……………………………………. B.S. Welding Engineering, The Ohio State University

1986 ……………………………………. M.S. Welding Engineering, The Ohio State University

1986 - 1987 …………………………….. Corporate Welding Engineer Motor Wheel Corporation Lansing, Michigan

1987 - 1992 ……………………………... Welding Engineer GE Aircraft Engines Cincinnati, Ohio

1992 - 2004 …………………………….. Market Leader, Aerospace Edison Welding Institute Columbus, Ohio

2004 – present …………………………... Senior Weld Research Engineer Delphi Kettering, Ohio

PUBLICATIONS

1. D.H. Phillips, W.A. Baeslack III, “Selection and of Advanced -Base Alloys”, ASM Handbook Volume 6, Welding, , and , 524-528, (1993)

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2. W.A. Baeslack III, D.H. Phillips, G.K. Scarr, “Characterization of the Weld Heat Affected Zone in an Alpha-Two Titanium Aluminide”, Materials Characterization, Vol. 28, no. 1, 61-73 (1992)

3. W.A. Baeslack III, D.H. Phillips, C. English, A.P. Woodfield, “Inertia-Friction Welding of an Advanced Rapidly Solidified Titanium ”, Journal of Materials Science Letters 10, 1401-1408 (1991)

4. L.C. Mallory, W.A. Baeslack III, D.H. Phillips, “Evolution of the Weld Heat- Affected Zone Microstructure in a Ti-48Al-2Cr-2Nb Gamma Titanium Aluminide”, Journal of Materials Science Letters 13, 1061-1065 (1994)

5. L.C. Mallory, W.A. Baeslack III, D.H. Phillips, T.J. Kelly, “Gas Tungsten of a Ti-48Al-2Cr-2Nb Gamma Titanium Aluminide”, Titanium ’92 Science and Technology, Proceedings, Symposium at 7th World Titanium Conference, San Diego, Vol.2; 29 June-2 July 1992, 1115-1122, (1993)

6. S.A. David, J.A. Horton, G.M. Goodwin, D.H. Phillips, R.W. Reed, “Weldability and Microstructure of a Titanium Aluminide”, Welding Journal, Vol. 69, no. 4, 133s- 140s, (April, 1990)

7. M.C. Juhas et. al., “Interface Characteristics of Solid Phase Welds Between Ti- 6Al-2Sn-4Zr-2Mo-0.1Si and 14Al-21Nb Titanium Aluminide” Titanium ’92 Science and Technology, Proceedings, Symposium at 7th World Titanium Conference, San Diego, Vol.2; 29 June-2 July 1992, 1453-1460, (1993)

8. K.N. Hou, et. al., “An Electron Microscopy Study of Inertia-Friction Welds in Ti- 48Al-2Cr-2Nb Gamma Titanium Aluminide”, International Trends in Welding Science and Technology, Gatlinburg, Tennessee, 1-5 June 1992, 1135-1137, (1993)

FIELDS OF STUDY

Major Field: Welding Engineering

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TABLE OF CONTENTS

ABSTRACT...... ii ACKNOWLEDGMENTS...... v VITA...... vi LIST OF FIGURES ...... x LIST OF TABLES ...... xvi

CHAPTERS:

1. INTRODUCTION...... 1 1.1 MIAB WELD PROCESS DESCRIPTION ...... 1 1.1.1 MIAB Welding Principles ...... 3 1.1.2 Comparison to other Welding Processes...... 6 1.2 ARC MONITORING SYSTEMS...... 7 1.3 MOTIVATION FOR WELDING CHROMIUM-PLATED STEEL TUBES ...... 7 1.4 OBJECTIVES OF THE RESEARCH ...... 9 2. TECHNICAL REVIEW ...... 10 2.1 MAGNETIC AT THE MIAB WELD JOINT...... 10 2.2 ARC BEHAVIOR AT THE MIAB WELD JOINT...... 12 2.3 ARC ROTATION VELOCITY ...... 19 2.4 MIAB WELDING OF NON-FERROUS MATERIALS...... 23 2.5 EFFECTS...... 25 2.6 HEAT FLOW IN THE MIAB WELDING PROCESSES...... 28 2.7 MIAB APPLICATIONS ...... 30 2.8 GENERAL WELDABILITY OF CHROMIUM-PLATED STEEL...... 32 3. EXPERIMENTAL PROCEDURE ...... 36 3.1 MIAB EQUIPMENT ...... 37 3.2 DESCRIPTION OF COMPONENTS AND WELD SET-UP ...... 41 3.3 MECHANICAL TEST METHODS...... 42 3.4 METALLURGICAL EVALUATION METHODS...... 45 3.5 HIGH SPEED VIDEO MONITORING ...... 47 3.6 DOE METHODOLOGY ...... 49 3.7 ARC MONITORING...... 54

viii 4. RESULTS...... 55 4.1 METALLURGICAL ANALYSIS...... 56 4.2 MECHANICAL ANALYSIS ...... 63 4.3 ANODE/CATHODE EXPERIMENTS...... 65 4.4 L12 DOE BASED ON ID BEND TEST CRACK LENGTH ...... 66 4.5 ARC MONITORING PLOTS ...... 70 4.6 HIGH SPEED VIDEO IMAGES ...... 72 5. DISCUSSION ...... 74 5.1 METALLURGICAL ANALYSIS...... 74 5.1.1 Optical Microscopy of Tubes without Chromium-plating...... 74 5.1.2 Optical Microscopy of Tubes with Chromium-plating...... 75 5.1.3 SEM Fractography of MIAB Welds with Chromium-plating...... 76 5.1.4 Microhardness Testing ...... 77 5.2 MECHANICAL ANALYSIS ...... 78 5.3 ANODE/CATHODE (JOINT POSITION WITHIN THE MAGNETIC FIELD) EXPERIMENTS...... 79 5.4 L12 DOE...... 82 5.4.1 Individual Effect of Variables on ID Bend Test Crack Length...... 83 5.4.2 Interactive Effect of Variables on ID Bend Test Crack Length...... 84 5.4.3 Effect of Variables and the Concept of Arc Force and Arc Pressure ...... 87 5.4.4 Effect of Arc Gap Setting ...... 95 5.5 HIGH SPEED VIDEO IMAGE INTERPRETATION ...... 98 5.6 ANALYSIS OF ARC MONITORING VOLTAGE PLOTS - CORRELATION WITH DOE RESULTS ...... 100 5.6.1 Analysis of Voltage Plots – Interpretation of Characteristic Features...... 100 5.6.2 Analysis of Voltage Plots – Effect of Level II Time...... 102 5.6.3 Analysis of Voltage Plots - Effect of Level III Current ...... 106 5.6.4 Analysis of Voltage Plots - Effect of Gap Setting...... 109 5.6.5 Summary of Arc Monitoring Voltage Plot Analysis...... 112 5.7 CONCLUSIONS...... 113 5.8 FUTURE WORK ...... 115 5.8.1 Further Characterization of Fracture Surfaces...... 115 5.8.2 Shielding Gas Effects...... 115 5.8.3 Anode/Cathode Experiments ...... 116 5.8.4 Effect of Initial Gap Setting...... 116 5.8.5 Ratio of Solid-State Weld Interface Length to Overall Weld Interface Length...... 117 5.8.6 Further Analysis of Weld Voltage “Signatures” ...... 117 5.8.7 Continuation of High Speed Video and Arc Pressure Analysis...... 118 REFERENCES...... 119 APPENDIX A ...... 122 A.1 22 MM COMPONENT - RESULTS...... 122 A.1.1 Metallurgical Analysis...... 122 A.1.2 Mechanical Analysis...... 126 A.1.3 L16 DOE Based on Weld Interface Length Measurement...... 129 A.2 22 MM COMPONENT – DISCUSSION ...... 133 A.2.1 Metallurgical Analysis ...... 133 A.2.2 Mechanical Analysis...... 134 A.2.3 L16 DOE ...... 135 A.3 ARC MONITORING VOLTAGE PLOTS ...... 138 A.4 40 MM CHROME-PLATED COMPONENT PRELIMINARY DEVELOPMENT RAW DATA...... 145

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LIST OF FIGURES

Figure Page

1 Basic Schematic of the MIAB Welding Process……………………………...2

2 Interaction Between Current and an Applied Magnetic Field ………...... 3

3 Aligned Magnetic Flux Lines Create Force on Conductor……………………4

4 Radial Component of Arc Current Affects Arc Movement………………...... 5

5 Arc Monitoring System Detects GMAW Defect…………………………...... 8

6 Method for Measuring Magnetic Flux Density……………………………...11

7 Maximum Flux Density Occurs at 5 mm from Pipe Surface………………...11

8 Melting Patterns of Thick-Walled Tube Reveal Melting on ID……………..14

9 Magnetic Flux in Tube-to-Plate Joint Pushes Arc Outward…………………16

10 Arc Trace on Tube End Shows Movement from OD to ID………………….17

11 Magnetic Arc Blow due to Tube Geometry Effects…………………………18

12 Spontaneous Magnetization of as a Function of Temperature………….18

13 Movement of the Arc Toward Tube OD…………………………………...... 19

14 Speed of Arc Affected by Heating (1) and Arc Gap (2)……………………..20

15 Arc Velocity vs. Time Plot Reveals Three Distinct Regions………………...22

16 Variations in Flux Density at the Joint………………………………………24

x Figure Page

17 Magnetic Flux Lines Between Two Aluminum Tubes………………………25

18 Ar-H2 Shielding Gas Increases Process Window for Al-Cu Joints……….....27

19 Good Fit Between Predicted (Dashed Line) and Actual (Solid Line) Heat Flow in a MIAB Weld……………………………………………………….30

20 MIAB (Magnetarc) Weld Joint of -to-Steel………………………..32

21 Cr-Fe Phase Diagram Shows High Temperature Solid Solubility Between the Two …………………………………………………………………..33

22 Extensive Cracking in Laser-Welded Chromium-plated Steel………………34

23 MD-101 Pneumatic MIAB Welding Machine……………………………….37

24 Overall Set-up: MD-101, Miller Power Supply, and Control Unit…………..38

25 Close-Up View of Control Unit……………………………………………...38

26 40 mm Components Loaded in Machine Prior to Clamping………………...39

27 Voltage Monitoring Connections for ARCAgent System…………………...40

28 Torroid for Monitoring Current on ARCAgent System……………………..40

29 22 mm Hollow Rod, Tenon, and Holding Fixture…………………………...41

30 40 mm Tenon-Tube Joint Details……………………………………………42

31 ID Bend or "Tulip Test" Technique………………………………………….43

32 ID Bend Test Showing an Acceptable Weld on a 40 mm part………………44

33 Acceptable Tensile Test of 40 mm Component as Indicated by Failure in Tenon……………………………………………………………………...45

34 Measurement of MIAB Weld Interface Length……………………………...46

35 Concept of Altering Joint Position within Applied Magnetic Field…………48

36 Typical High Speed Video Image……………………………………………49

xi Figure Page

37 40 mm MIAB Tube-to-Tube Weldment Reveals Plastic Flow……………...57

38 40 mm Tube-to-Tenon Weld Interface………………………………………58

39 40 mm Chromium-plated Tube-to-Tenon Joint Reveals Evidence of Poor Bonding………………………………………………………………………59

40 SEM Fractograph of Tensile Test Weld Interface Fracture Surface…………60

41 SEM EDS Analysis of Region of Decohesive Rupture on Fracture Surface..61

42 Microhardness of Typical 40 mm Tube-to-Tenon MIAB Weld Joint……….62

43 Failed ID Bend Test of MIAB Weldment Utilizing Chromium-plated Tube……………………………………………………………………….....63

44 Evidence of Joint Position within Magnetic Field Affecting Arc Location…66

45 Individual Variable Effect of Joint Position, Level III Current, and Level II Time on Crack Length on 40 mm MIAB Weldments……………………….68

46 Interactive Variable Effects of Joint Position, Level III Current, and Level II Time on 40 mm MIAB Weldments………………………………………….69

47 Two Typical Arc Monitoring Plots of 40 mm Tube-to-Tenon MIAB Welds………………………………………………………………………...71

48 High Speed Video Image - Joint Centered in Magnetic Field…………….72

49 Joint Shifted Toward Anode Side of Arc…………………………………….73

50 Joint Shifted Toward Cathode Side of Arc…………………………………..73

51 Typical GTAW Arc Results in Much More Heating on Anode Side [22]...... 80

52 Thermionic Emission of Fe Greatly Exceeds Melting Temperature at Typical Arc Currents…………………………………………………………80

53 Interactive Variable Effect of Level II Time and Level III Current…………85

54 Magnetic Pinching Effect on GTAW Arc…………………………………...88

xii Figure Page

55 Pinching Effect Creates Downward Flow Which Exerts Pressure on Weld Puddle Depressing It………………………………………………….88

56 Plot of Arc Pressure vs. Radial Distance in a GTAW Arc Reveals Significant Arc Pressures………………………………………………….....89

57 Plot of Arc Pressure vs. Weld Current in the GTAW Process Shows a Linear Relationship between Pressure and Current……………………….....90

58 Arc Gap can have Significant Effect on Pressure Depending on Shielding Gas………………………………………………………………...91

59 Flared Arc Shape in MIAB Welding Creates Outward Pressure Induced Flow………………………………………………………………...93

60 Individual Variable Effects Including Effect of Gap on Crack Length……...97

61 Interactive Variable Gap Effects on Crack Length – Level III Current……..98

62 Common Features Observed in the Voltage Plots………………………….102

63 Increase in Level II (Arc Heating) Time at a Constant Low Level III Current Results in Voltage Plateau Prior to Upset………………………………….103

64 Level II Time Effect at Higher Level III Current………………………….104

65 Arc Pressure Variations at Various Arc Lengths for a GTAW Arc……….105

66 Level III Current Has Significant Effect on Expulsion at Short Times……107

67 Expulsion at Long Level II Times is Increased at High Level III Currents…………………………………………………………………….107

68 Arc Force vs. Current……………………………………………………….108

69 Gap Setting Affects Level of Voltage Plateau and Time of Arc Stabilization………………………………………………………………...110

70 Paschen’s Law……………………………………………………………...111

71 Microhardness Traverse from Tube (left) to Tenon (right)………………...123

xiii Figure Page

72 Optical Micrograph of a Typical MIAB Weld……………………………..124

73 Macrosection of 22 mm Tenon-to-Tube MIAB Weld……………………...124

74 MIAB Weld Joint Reveals Insufficient Upset……………………………...125

75 Voids Along Weld Interface Can Result from Insufficient Upset…………125

76 Portion of Acceptable 22 mm ID Bend (“Tulip”) Test Coupon……………126

77 Acceptable 22 mm Tensile Test Results in Base (Tenon) Failure…..127

78 22 mm Failed Tensile Test Due to Improper Parameters from Electrical Short in Controller………………………………………………………………...128

79 Weld Interface Length Measurement Technique Using Pax-It Software….129

80 MIAB Weld Variables Weld Current, Weld Time, and Upset Pressure Increase Length of MIAB Weld Interface…………………………………131

81 Interactive Variable Effects of MIAB Weld Parameters on Weld Interface Length………………………………………………………………………132

82 Linear Relationship of Melt Rate vs. Current for GMAW Process………...137

83 L12 Condition #1…………………………………………………………...138

84 L12 Condition #2…………………………………………………………...139

85 L12 Condition #3…………………………………………………………...139

86 L12 Condition #4…………………………………………………………...140

87 L12 Condition #5…………………………………………………………...140

88 L12 Condition #6…………………………………………………………...141

89 L12 Condition #7…………………………………………………………...141

90 L12 Condition #8…………………………………………………………...142

xiv Figure Page

91 L12 Condition #9…………………………………………………………...142

92 L12 Condition #10………………………………………………………….143

93 L12 Condition #11………………………………………………………….143

94 L12 Condition #12………………………………………………………….144

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LIST OF TABLES

Table Page

1 L16 Experimental Layout……………………………………………………51

2 Typical Data From Initial 40 mm Component Development Work…………64

3 L12 Experiment with ID Bend Test Crack Length (mm) Results…………. .67

4 Table 4 – Portion of the 40 mm Preliminary Development Raw Data……..149

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CHAPTER 1

INTRODUCTION

Magnetically Impelled Arc Butt (MIAB) welding is a unique process in that it utilizes relatively simple equipment, but relies on very complex interactions between an arc and both an applied and induced magnetic field. This interaction is made even more complex by the changes that occur during the heating of the parts being welded.

In this chapter the MIAB weld process is described and compared to other welding processes which might be considered for the same application. Arc monitoring methodology is introduced and the motivation for this research program is discussed.

1.1 MIAB Weld Process Description

The MIAB welding process was initially investigated by the E.O. Paton

Electric Welding Institute during the 1950's and 1960's. It was later developed for commercial applications by Kuka Welding systems, who named it the Magnetarc process. Today, MIAB welding is used for a variety of applications throughout

Europe and the Ukraine, and Paton continues its MIAB research and development efforts.

1 MIAB welding is a forge welding process that relies on an electric arc to generate the necessary heating to melt the faying surfaces being welded. The arc heating also lowers the yield strength of adjacent solid material to allow for sufficient forging action, a critical aspect of the process. A basic schematic of MIAB welding is shown in Figure 1, which depicts the welding of two tubes.

Figure 1 - Basic Schematic of the MIAB Welding Process [4]

As the figure indicates, an arc is made to spin around the tubes due to the presence of a magnetic field generated with either permanent or electromagnets. The velocity of the arc is considerable, reaching speeds as high as 200 m/s. The rapidly spinning arc, in combination with the thermal conductivity of the metal being welded, effectively creates very uniform heating at the joint. Upon completion of the heating phase, the parts are rapidly brought together under pressure. This upset step squeezes the molten material out of the joint, and creates a forging action on the remaining plasticized metal. The forging action produces the final solid-state joint. The process does not use . Shielding gas, although sometimes used, is usually not

2 required. When shielding gas is not used, as in the case of this research, a short pulse of high current is added which expels contaminated molten metal prior to upset.

1.1.1 MIAB Welding Principles

As shown in Figure 2, the MIAB welding process relies on the interaction

between electrical current flowing through the arc and a magnetic field. Upon

Figure 2 - Interaction Between Current and an Applied Magnetic Field [29]

initiation of a drawn arc, an electromagnetic force, FL, is generated on the arc. The

force is due to the axial component of current flow in the arc, IL, crossing the radial

component of the applied magnetic field, BL. This electromagnetic force on the

flowing current is referred to as a Lorentz force, and given by: f = J x B,

where f = electromagnetic force density, J = current density, and B = magnetic flux

density. The magnitude of the force, F, is proportional to the magnetic flux density,

B, the arc current I, and the arc length L and given by: F ~ B·I·L

3 The force exerted on the flowing current affects the acceleration of the

rotating arc. Therefore, it is clear that by adjusting the strength of the magnetic field, the magnitude of the arc current, or the width of the arc gap, the speed of the arc can be altered. The ability to alter the speed of the arc by changing arc current can play an important role in the process. In particular, by sharply increasing the current for a very short time just prior to upset, a rapid expulsion of molten metal occurs which provides cleaning action. This eliminates the need for shielding gas.

The direction of the force is determined by applying Fleming's left hand rule, which states that the rotating direction of the arc is always perpendicular to the applied magnetic field and the arc current, as shown previously in Figure 2. The force occurs due to the magnetic flux lines generated by the flowing current interacting with the magnetic flux lines of the applied magnetic field. This phenomenon is shown graphically on Figure 3 [29], which depicts a current carrying

Figure 3 - Aligned Magnetic Flux Lines Create Force on Conductor [29]

4 conductor under the influence of an applied magnetic field. The force is generated on

the side of the conductor where the magnetic flux lines are aligned. Ironically, in arc

welding processes, a similar interaction creates a phenomenon called "arc blow", often a detriment to the process.

In addition to the primary force on the arc that causes the arc to spin rapidly around the part, there is an additional important force on the arc [4]. This force is generated when the radial component of the arc, Ir, crosses the axial component of the magnetic field, Ba, as shown in Figure 4. Initially, when MIAB welding a

ferromagnetic material, the arc is pushed to the ID of the joint due to arc blow

Figure 4 - Radial Component of Arc Current Affects Arc Movement [4]

5 effects. Upon heating, the curie temperature is first reached on the ID of the tube,

altering the distribution of magnetic flux in the joint and pushing the arc outward.

The outward movement of the arc can play an important role in generating uniform heating at the joint.

1.1.2 Comparison to other Welding Processes

The MIAB welding process can be compared to both Friction welding and

Flash welding. Much like Friction welding, MIAB welding is ideal for round parts

(especially tubes and pipes). It produces a solid-state bond at the joint which is conducive to excellent mechanical properties. Processes which produce solid-state bonds also provide for the possibility of welding dissimilar metal joints. Unlike

Friction welding, MIAB welding equipment is much simpler and less expensive, since no part rotation is required and upset pressures are much lower. Other potential benefits of MIAB welding vs. Friction welding include less internal flash, shorter weld times, less metal loss, and reduced machine maintenance.

Flash welding does not actually generate a true arc, but relies on the creation of shorts between the parts being welded, and subsequent rapid expulsion of the metal at the localized shorting points. This results in considerable loss of material during the flashing process. Flash welding also does not utilize a magnetic field to control the movement of the arc, which promotes very uniform heating in the MIAB welding process. For these reasons, Flash welding is not an ideal process for welding tubular automotive components.

6 1.2 Arc Monitoring Systems

Arc weld monitoring techniques are effectively used for real-time quality

control in high production (GMAW) applications [30]. They

are easily automated and require minimal maintenance. They can be used to monitor

individual in-process weld faults, as well as overall part and weld tracking. IMPACT

Engineering manufactures and sells such a monitoring system called the ARCAgent.

An example of how the ARCAgent system and associated software can be used to

monitor GMAW quality is shown in Figure 5. This example shows a lap joint

weldment that exhibits lack of fusion toward the left side of the weld, and the

associated current/voltage signature recorded by the ARCAgent monitoring system that clearly detects this defect. There is no known documentation that indicates such a system has been used for monitoring MIAB welding prior to this research.

1.3 Motivation for Welding Chromium-Plated Steel Tubes

Tubes continue to become more and more important in the construction of an

automobile. Tubes provide light weight, excellent rigidity, and low cost. In particular, tubular suspension components are becoming more sophisticated in their design, and often require a weld joint in their construction. Tubular joints represent an ideal application for MIAB since the tube geometry plays a significant role in controlling the arc path, which promotes uniform heating of the joint.

A current important Delphi suspension component, called an MR

(Magnetorheological) Damper, provides for a continuously variable suspension

7 Highlighted region indicative of lack of fusion observed in weld below

Region of poor fusion

Figure 5 - Arc Monitoring System Detects GMAW Defect

mechanism. This is achieved through the ability to vary the viscosity of an MR fluid by altering the magnetic field surrounding the fluid. By changing the viscosity of the fluid, the yield force of the damper can be controlled. The MR fluid contains

8 particles that are erosive, leading to the requirement for the interior of the damper tube receiving a chromium-plating treatment to resist the erosive effects of the fluid.

The construction of this damper requires that a threaded fitting called a tenon be welded to the chromium-plated tube. Friction welding is one alternative for producing this joint, but as stated previously, has several potential disadvantages vs.

MIAB welding.

1.4 Objectives of the Research

The primary objectives of this research project are as follows:

1) To establish feasibility for MIAB welding chromium-plated tube-to-tenon joints

utilizing DOE methodology.

2) To understand the effects of critical MIAB weld variables for producing this joint.

3) To develop an approach for monitoring the MIAB welding process, and therefore the quality of the chromium-plated tube-to-tenon weldment, utilizing arc monitoring techniques.

4) To develop correlations between arc physics and arc welding theories, the arc monitoring methodology, and the effect of important MIAB weld variables on the quality of the chromium-plated tube-to-tenon MIAB weldments.

9

CHAPTER 2

TECHNICAL REVIEW

Relative to other welding processes, the amount of published research on

MIAB welding is very limited. Also, many of the papers are translated from Russian.

In some cases the translations are not clear, adding to the difficulty of understanding

what is already a very complex process. This chapter summarizes the papers which

were considered most relevant to this research. This summary also illustrates the considerable disagreement among the authors on a variety of MIAB welding concepts. Particular discrepancies pertain to the interaction between the arc and the applied and induced magnetic field.

2.1 Magnetic Flux at the MIAB Weld Joint

Kim and Choi [1] developed a two-dimensional finite element model for the

analysis of magnetic flux density distributions produced by electromagnets at the

MIAB weld joint. The primary objective was to establish a relationship between the

strength of the radial magnetic field at the joint and the quality of the weld joint

10 between two steel pipes. This concept was based on the knowledge that a stronger magnetic field produces a higher force on the arc, resulting in faster arc speeds and more uniform heating. Their experimental approach, shown in Figure 6, utilized a

Gauss-meter at the center of the joint, and flux density was plotted vs. distance from the outer surface of the pipes at various distances from the exciting coil. Figure 7 reveals the resulting plot developed when the exciting coils were located 10 mm from

Figure 6 - Method for Measuring Magnetic Flux Density

Figure 7 - Maximum Flux Density Occurs at 5 mm from Pipe Surface

11 the probe. This plot shows a maximum flux density approximately 5 mm from the pipe surfaces, and also reveals the accuracy of the finite element model developed.

The authors concluded that it was important to maintain maximum flux density at the joint for best weld quality. Therefore, the design of the electromagnet system for each application is very important, as is the exciting current applied to the electromagnets.

Gap size between the two pipes and relative permeability both had an effect on the magnetic flux at the joint. In summary, they showed that magnetic flux density increases with increasing permeability, decreasing distance from the magnets, and decreasing gap size. They also proposed that their numerical analysis model could be used in the design of electromagnet systems.

2.2 Arc Behavior at the MIAB Weld Joint

Steffen and Welz [2] investigated a variety of conditions and their effect on arc behavior, including the use of internal and external magnets and different power sources. Steel tubes of various dimensions were utilized. A high speed video camera and an electronic image converter were used to study the arc. Images from this set-up revealed the major differences between the action of the arc at the anode vs. the cathode side of the joint. The arc was seen to move freely on the anode side of the joint, but was constricted on the cathode side. As a result, when the arc is forced to move in the presence of a magnetic field, the anode spot is blown ahead while the cathode spot trails.

12 The arc was also seen to always initiate along the ID of the tube edges. They proposed this was due to the fact that the arc prefers regions that heat up the most quickly, and where the induced magnetic field surrounding the arc encounters the least magnetic resistance from the applied field. They postulated that as the steel melts on the ID edges, the arc length increases. The longer arc, combined with centrifugal forces pushing the arc outward, results in the arc moving toward the OD as the weld progresses. Internal magnets resulted in faster starting of the weld, but external magnets provided for a more controlled rotation of the magnet.

Several DC rectified power sources were evaluated and compared to power generated from a bank of batteries. This study revealed a marked improvement in arc characteristics when using the batteries. The batteries provided much more consistent power due to the small amount of inductance in the system vs. the power supply inductance. Although batteries are of course impractical for this application, the authors noted the importance of this information regarding the future development of low inductance power supplies. It was also shown that arc voltage was mostly independent of the power source used, but highly dependent on the arc gap.

Nentwig and Ludwig [3] also studied and contrasted the effect of an internal vs. an external magnetic coil on arc behavior during MIAB welding of tubes. It was determined that the maximum radial flux density in the weld gap is always along the edge of the tube closest to the coil. When welding ferromagnetic materials, the magnetic flux density drops sharply across the wall thickness of the tube. This mainly affects the arc starting characteristics immediately following arc initiation.

13 Interestingly, the arc was always observed to initiate on the ID of the tube, regardless of whether or not an external or internal coil was used. But arc stabilization occurred much more quickly with an internal coil, leading the authors to conclude that, when possible, it is always more desirable to utilize an internal vs. an external magnetic coil.

At the E.O. Paton Electric Welding Institute, Kachinskiy et. al. [4] investigated arc behavior during the welding of hollow parts with very thick (> 6 mm) wall thicknesses. In general, it becomes very difficult to MIAB weld thick walled components due to the tendency of the arc to concentrate on the ID of the component, resulting in uneven heating. Kachinskiy also postulated that the anode and cathode spot sizes of an arc should be relatively large relative to the wall thickness to achieve even heating. As shown in Figure 8, arc column traces consume the ID of the thick- walled tubes during the initial stages of welding. Upon further heating, the arc

Melting patterns evident along tube ID

Figure 8 - Melting Patterns of Thick-Walled Tube Reveal Melting on ID [4]

14

column moves to the OD, but the large wall thicknesses prevent stable movement of

the arc to the region of higher magnetic field induction leading to non-uniform heating.

In order to improve this situation, the authors adjusted the position of the

magnetic field in such a way to emphasize the axial component vs. the radial

component of the applied magnetic field. With this new approach, a larger axial

magnetic flux component crosses the radial current component of the arc. This, in turn, produces a greater force on the arc pushing, it toward the OD of the tube. This

force was shown previously on Figure 4.

Additional research at Paton by Kuchuk-Yatsenko et. al. [5] focused on arc

behavior during MIAB welding of a tube to a plate. In this type of joint, the

displacement of the arc from the ID to the OD discussed previously is much more

pronounced due to the magnetic blow resulting from the interaction of the arc and the

induced magnetic field. This creates a greater concentration of magnetic lines of

force on the ID of the tube, which pushes the arc outward as shown in Figure 9.

This situation can again lead to uneven heating and a poor quality weld. As

with Kachinskiy's work, the importance of controlling the axial component of the

magnetic field was emphasized. The ability to alter the axial component of the

magnetic field allowed for more precise control of the radial position of the arc in the joint. This produces more uniform heating, and thus, better quality welds. Such adjustments can be made by changing the magnetic field strength on one side of the

15

Figure 9 - Magnetic Flux in Tube-to-Plate Joint Pushes Arc Outward [5]

joint relative to the other side. A rotating electromagnet with an elliptical shape on the plate side of the joint was also shown to be beneficial in controlling the radial displacement of the arc.

Sato, Katayama, Ioka, and Otani [6] studied the phenomenon of the arc initiating on the ID of steel pipes and then moving to the OD, especially when welding thick cross-sections. Photo-transistors were used to assess the movement of the arc. Arc traces of the pipe ends were conducted when the arc was initiated on the

OD in the presence of an applied magnetic field, and also, in the absence of an applied magnetic field. In both cases, the arc moved to the ID of the pipe. One example of this movement is shown in Figure 10. Thus, the authors showed that the initial movement of the arc along the ID during the initial arcing phase was not due to the arc initiating there, nor was it due to the applied magnetic field pushing it toward

16 the ID. Instead, the authors postulated and later verified, that a magnetic arc blow

event is created due to the tube geometry interacting with the magnetic field of the

Arc trace

Figure 10 - Arc Trace on Tube End Shows Movement from OD to ID [6]

arc. This creates stronger lines of force on the OD of the tube which pushes the arc toward the ID. This concept is shown on Figure 11.

Upon further heating, the authors theorized that the movement of the arc from

the ID to the OD of the tube was due to the magnetic variations of the tube ends as the temperature rises. Specifically, as Figure 12 indicates, spontaneous magnetism of iron drops with temperature, and at the Curie temperature (770ºC), iron is no longer considered magnetic. This creates a condition in which the magnetic arc blow pushes the arc toward the OD. The authors further verified this by plotting arc movement from the ID to the OD as a function of heating time and arc current. These results are

shown on Figure 13 which clearly indicates a strong relationship between movement

of the arc toward the OD and arc time and current.

17

Figure 11 - Magnetic Arc Blow due to Tube Geometry Effects [6]

Figure 12 - Spontaneous Magnetization of Iron as a Function of Temperature [6]

18

Higher voltages indicate movement of arc toward OD of joint

Figure 13 - Movement of the Arc Toward Tube OD [6]

2.3 Arc Rotation Velocity

Yatsenko, Syrovatka, and Kuznetsov [7] studied the velocity of the arc moving in the gap between a tube and a plate. Specifically, they evaluated the affect of weld parameters and arc gap variations. Photoelectric cells and galvanometers were utilized to study the arc movement. It was determined that the speed of the arc depends on welding current, the magnetic field intensity, the arc gap, and the temperature of the metals being welded. Figure 14 summarizes their results, showing the effect of arc gap and heating (arcing time) on the speed of the arc. Scale and oxides on the faying surfaces at the joint played a role in arc velocity and mobility.

The arc was also observed to become highly mobile if scale was removed from the plate and tube ends. Distinctions between the anode (tube side) and cathode (plate

19

Arc rotation velocity

Arc gap length

Figure 14 - Speed of Arc Affected by Heating (1) and Arc Gap (2) [7]

side) spots were discussed. In particular, the anode spot was seen to be interrupted, with evidence of jump-like movement, especially in the presence of metal vapors.

As Figure 14 indicates, speed of the arc increased as the work piece temperatures increased. It was suggested that this was due to the fact that the area of the anode spot increases with increasing temperature. This reduces the current density and rigidity of the arc plasma, allowing greater distortion of the arc column from the applied magnetic field. The increased distortion promotes the increase of new anode spots, allowing faster movement of the arc. A layer of molten metal soon

20 forms on the tube end which reduces the gap and consequently, the arc length. The

reduced arc length causes a stiffer arc plasma, which is more difficult to move by the

applied magnetic field. This explains the drop in arc velocity after the first peak of

the figure.

The effect of the gap increase then causes another jump in arc velocity. This

is due again to the decrease in arc stiffness described above. Upon further heating of

the work pieces, the arc speed increases again due in part to electromagnetic forces

expelling more molten material. Again, the plasma rigidity is reduced resulting in the

velocity increase. The highest arc speeds resulted in large amounts of molten metal

which formed bridges and an unstable arc, resulting in the final drop in arc velocity

shown on the figure.

Taneko, Arakida, and Takagi [8] used a voltage detector at various locations

inside a pipe, an oscilloscope, and a high speed video camera to measure

arc velocities and arc angles. In particular, they studied the relationship between arc

velocity and angle, and position at which power was supplied to the tubes. They were

able to conclude that due to the arc blow effect and electrical resistance of the tube, current increases in the arc closer to the power supply connection on the tube. This increases the magnetic blow effect and decelerates the arc. As the arc moves away from the power supply point it then accelerates. The authors concluded that as a result, in order to support a stable moving arc, it is important to have numerous uniform contact points on the tube.

21 Plots of arc velocity vs. time showed three distinct regions: 1) the low velocity

region I, 2) the high velocity region II, and 3) the rotation velocity fluctuation region

III. A typical plot is shown in Figure 15. From these plots, the authors theorized that the transition from region I to region II occurs due to the ends of the pipe reaching the

Low velocity High Velocity fluctuation region velocity region region Velocity (m/s)

Time (seconds)

Figure 15 - Arc Velocity vs. Time Plot Reveals Three Distinct Regions [8]

Curie temperature (760°). Once this temperature is reached, the applied magnetic

field begins to dominate control of the arc vs. as opposed to the induced magnetic

field of the arc. This, in turn, causes the arc velocity to increase. The formation of

excessive molten material later in the process causes the arc velocity to fluctuate

(region III).

The three regions were shown to be separated by two distinct and important

times: 1) th - time for the area 1 mm from the pipe ends to reach the Curie

temperature, and 2) tf - time for the entire surface of the pipe ends to reach the

22 melting temperature. Time th separated region I from region II and time tf separated region II from region III. In summary, it was suggested that optimum welding conditions could be achieved when applying upset pressure immediately after reaching time tf.

2.4 MIAB Welding of Non-Ferrous Materials

Mori and Yasuda [9] evaluated the feasibility of the MIAB welding process with aluminum and aluminum- joints. It is a lot more difficult to achieve the required flux density at the joint with non-ferrous materials vs. ferrous materials. As a result, an iron core is often inserted inside the pipe. Variations in flux density with steel, aluminum, and aluminum with an iron core are graphically shown in Figure 16.

The importance of weld upset distance was emphasized in the welding of the aluminum joints. The use of shielding gas was important in producing the aluminum- copper joints, as was placing the aluminum on the cathode side of the joint to achieve cleaning action.

Nentwig and Schmidt [10] used iron filings to study and contrast the radial and axial magnetic field lines in the joint of ferrous and non-ferrous materials. These experiments showed that the location of the joint relative to the applied magnetic field can have a large impact on whether the axial or radial portion of the magnetic field dominates at the joint. They also observed irregularities in the distribution of the magnetic field in the presence of ferrous materials. They concluded that with non-

23 ferrous materials, it is possible to arrange the magnetic coils in such away to create the proper magnetic flux at the joint, although the magnetic flux density will be

Figure 16 - Variations in Flux Density at the Joint [9]

less than with ferrous materials. Figure 17 shows the results of one of their

experiments in which the magnetic flux lines generated at an aluminum tube joint are

clearly visible.

24 In previously discussed research conducted by Sato et. al. [6], arc blow had a

significant effect on MIAB welding of non-ferrous (aluminum) materials. Due to the

fact that the flux density was higher at the inner edges of the pipe, the arc is pushed to

the OD. This condition is just the opposite when compared with welding ferrous

materials, during which the arc blow tends to push the arc toward the ID.

Outline of tube walls in black Magnet Magnet

Figure 17 - Magnetic Flux Lines Between Two Aluminum Tubes [10]

2.5 Shielding Gas Effects

Welz and Nentwig [11] studied the significance of using shielding gas for a

variety of materials. At the time of their research, it was believed that shielding gas

was not necessary when welding low carbon steel, even though it did typically result

in more consistent arc initiation and a smoother flash after upset. However, with aluminum and high alloy , shielding gas was thought to be much more important

25 due to the formation and low mobility of oxides that can form if gas is not used. In

this research program, the authors evaluated a wide range of shielding gases including

argon and argon blends, , nitrogen and nitrogen blends, and helium.

There were no specific conclusions as to which shielding gases were the best.

However, the authors did observe the importance of the effect on surface tension of the molten metal and arc voltage depending on the shielding gas chosen. Gases which produced high surface tensions tended to restrict arc mobility, causing lack of fusion problems. They also discussed the difficulty of obtaining good shielding due

to the turbulence of the rotating arc, and the importance of using shielding gas (argon)

when welding aluminum.

Johnson et. al. [12] evaluated the MIAB welding process for joining steel

tubes, and included in their research the effect of carbon dioxide as a shielding gas.

They concluded that fewer bend test defects resulted from weldments produced with

this shielding gas. They postulated that carbon dioxide offered some protection

against oxidation during the welding cycle. Metallography revealed less pro-

eutectoid ferrite, probably due to the reduction in small oxide inclusions. The

shielding gas also provided for a 10% larger current range operating window.

Research on MIAB welding of non-magnetic, austenitic

conducted by Welz, Nentwig, and Schwarzkopf [13] showed the importance of using

shielding gas for these materials. They compared various gases and concluded that

argon with 20% helium, argon with 5-6% , and argon with 2.5% carbon

dioxide all produced acceptable bend and tensile test results. Pure argon and argon

26 with less than 15% helium shielding gases performed poorly due to excessively slow arc rotation speeds and uneven melting. The research showed that without proper shielding, oxides can remain at the joint interface resulting in poor mechanical properties.

Previously discussed research by Mori and Yasuda [9] evaluated the effects of different shielding gases when MIAB welding aluminum to copper joints. As indicated in Figure 18, an argon-hydrogen (5%) blend produced a much larger process window for welding than a pure argon shielding gas. With the hydrogen

Figure 18 - Ar-H2 Shielding Gas Increases Process Window for Al-Cu Joints [9]

27 blend, shorter arcing times and upset lengths still resulted in satisfactory welds compared to pure argon. This result was attributed to the fact that the addition of hydrogen raises the arc temperature resulting in more efficient heating at the copper side of the joint.

2.6 Heat Flow in the MIAB Welding Processes

There is a relatively small amount of published research on the subject of heat flow during MIAB welding. This is surprising considering the importance of heat flow in this process. A successful weld typically requires a good balance between the localized heating from the arc at the joint, and conduction of heat into the part to minimize the thickness of the liquid layer formed. In addition to the liquid layer formation, proper heating reduces the yield strength of the adjacent solid metal to facilitate proper upsetting. A study by Xiancong et. al. [14] addressed the subject of heat flow in the MIAB weld joint. They considered the rotating arc to be a constant heat source, and applied the following heat flow equation for predicting the temperature at time t and distance y from the arc:

28 qy ⎪⎧⎡ 4at y2 ⎡ y ⎤⎤⎪⎫ T(y,t) = ⎨⎢ exp(− ) − π ⎢1− Φ( ⎥⎥⎬ 2λπ ⎩⎪⎣ y 4at ⎣ 4at ⎦⎦⎭⎪

Where:

T = temperature (ºC)

t = arc rotation time (s)

q = heat input of the arc (cal/cm ºC)

y = distance from arc along the tube (cm)

λ = coefficient of (cal/cms ºC)

a = coefficient of temperature conduction (cm2/s)

y Φ( ) = function of Gauss probability 4at

It was determined that acceptable welds could be achieved at T = 1200 ºC at y = 0.1 cm or at T = 900 ºC at y = 0.4 cm. Therefore, the optimum relationship between heat input (q) and arc rotation time (t) could be calculated from this formula for a given temperature (T) and distance (y). The formula can also be used to calculate the width of the heat-affected zone.

Kalev et. al. [15] suggested that a MIAB welding arc is not a constant, uniform heat source since a typical weld cycle involves different levels of current from the beginning to the end. They were able to develop mathematical equations based on heat flow theory that incorporated the concept of current, or power, varying with time. They then compared the analytical results with thermal cycles of actual

29 weldments, which were determined through the use of thermocouples. The resulting plot, shown in Figure 19, reveals a good fit between the predicted and measured temperatures taken at various distances from the end of the tube.

Dashed lines represent analytical result

Thermal cycles at three different distances from tube ends T (°C) T (°C)

Figure 19 - Good Fit Between Predicted (Dashed Line) and Actual (Solid Line) Heat Flow in a MIAB Weld [15]

2.7 MIAB Applications

P.N. Hone [16] of The Welding Institute in Abington, England summarized

MIAB activity there and the numerous potential applications for this process.

Research on extremely thick (up to 12 mm) steel tubes is discussed. These thicknesses required orbiting one tube axis relative to the other in order to sufficiently heat the complete wall thickness of the tubes. Success welding a variety of aluminum

30 alloys as well as non-circular tubes was reported. In some cases, the non-circular

tubes required specially shaped magnets, but this was not always necessary.

A variety of production applications were sited, including propeller shafts,

automobile axles, fuel tank vent pipes, drive shafts, shock absorbers, and gas-filled

struts. The Ford Transit van axle utilized a large rectangular MIAB weld to join the

axle tube to the center housing. The rear axle on the Vauxhall Astramax is MIAB

welded. The process is also used in the construction of suburban gas distribution

systems.

Hagan and Riley [17] of the Ford Motor Company summarized their use of

MIAB welding in the manufacturing of the Fiesta rear axle cross tube assembly. In

selecting MIAB welding, they first considered other more common welding methods:

Friction, Flash, and GMAW. Friction was not acceptable because of the difficulty maintaining the radial relationship between the shaped flange spindles and the axle tube. Flash welding was known to leave clamping marks on parts, and presented problems regarding maintaining part alignment. GMAW was considered a more expensive process to operate and created more alignment problems due to distortion.

As a result, they decided to pursue MIAB welding for this application. After optimizing the welding variables, conducting all the necessary testing, and developing the weld quality monitoring procedures, the process was successfully implemented in mass production.

The use of MIAB (in this case, Magnetarc) welding in the production of truck cab suspension components was described by Hiller, Schmidt, and Breiksch [18] of

31 ThyssenKrupp Automotive Systems. This application involved MIAB welding a cast iron lever to an extruded steel torsion tube to produce the welded assembly shown in

Figure 20. The authors commented on the many advantages of this process, including short welding times and the excellent mechanical properties of the solid- state joint produced between cast iron and steel.

Figure 20 - MIAB (Magnetarc) Weld Joint of Cast Iron-to-Steel [18]

2.8 General Weldability of Chromium-Plated Steel

It is important to emphasize that there is an extremely limited amount of published research in the area of welding of chromium-plated steels. The obvious reason for this is that in most cases, chromium-plating is applied for decorative purposes, which in turn would mandate that any welding operation be conducted prior to the plating operation to avoid the degradation to the appearance of the chromed surface from the welding process. The Cr-Fe phase diagram [19] of Figure 21 shows complete solid solubility between iron and chromium at high temperatures, in

32 addition to two low temperature constituents known as Sigma Phase and Alpha

Prime. This diagram is used quite extensively in the development and analysis of

stainless steels. The diagram also reveals a fairly significant difference in the melting

temperatures of the two metals, with chromium melting at 325ºC higher than iron.

Figure 21 - Cr-Fe Phase Diagram Shows High Temperature Solid Solubility Between the Two Metals [19]

Although research on this subject is limited, Vedani et. al. [20] did attempt to use a laser to repair weld chromium-plated steel. As indicated in Figure 22, extensive cracking was discovered in the laser welded deposits of this material. Further

33 analysis revealed the presence of chromium and oxygen which resulted in the severe hot-cracking. The authors concluded that repair welding of chromium-plated steel using a laser process is not feasible.

Cracking in Laser weld fusion zone

Figure 22 - Extensive Cracking in Laser-Welded Chromium-plated Steel [20]

It should also be pointed out that certain chromium-rich stainless steels such as austenitic stainless steels can be very susceptible to solidification cracking [31].

Fusion zones with these alloys often solidify as . Austenitic solidification promotes greater partitioning of solute and the formation of less torturous solidification grain boundaries vs. ferrite. These factors contribute to the solidification cracking problem.

When welding chromium-plated steel however, the amount of chromium in the fusion zone would likely be very small. As a result, the issue of solidification

34 cracking known to be a problem when welding austenitic stainless steels probably does not apply. Vedani et. al. did not comment on whether or not the cracking they observed was related to the formation of a susceptible solidification structure.

35

CHAPTER 3

EXPERIMENTAL PROCEDURE

The experimental procedure involved several levels of experiments designed to first develop a knowledge base for MIAB welding steel tubes-to-tenons prior to conducting the main component of the research. Since there is very little information in the textbooks on MIAB welding, this knowledge base was deemed critical to the success of the research project. Once a solid understanding of MIAB welding of the tubes to tenons was established, the primary research of MIAB welding chromium- plated tubes-to-tenons utilizing arc monitoring equipment was conducted.

The initial development work was conducted on 22 mm steel tube-to-tenon joints. This was followed by 40 mm tube-to-tube joints, then 40 mm tubes-to-tenons, and finally, 40 mm chromium-plated tubes-to-tenons. Wall thicknesses for all components were approximately 2 mm. Design of Experiments (DOE) methodologies were deployed during two phases of the development work, first with the 22 mm components, and then with the 40 mm chromium-plated tubes. Several evaluation methods were utilized, including optical and SEM microscopy, tensile

36 testing, and a bend test called and ID bend or Tulip test. This chapter provides details on the MIAB welding equipment, the components that were welded, and the evaluation and monitoring techniques used throughout this research.

3.1 MIAB Equipment

The research conducted in this project utilized an MD-101 pneumatic MIAB welding machine supplied by KSET, and manufactured by the Paton Institute in the

Ukraine. A picture of the machine is shown in Figure 23, the overall set-up including controller and weld power supply in Figure 24, and closer views of the controller and the MIAB machine with parts loaded for welding in Figures 25 and 26 respectively.

Clamps are open to reveal top half of the Parts loaded in MD- dies 101 MIAB welding machine

Figure 23 - MD-101 Pneumatic MIAB Welding Machine

37 MD-101 MIAB welding machine Miller constant current with clamps closed power supply

Controller for MD-101 machine

Figure 24 - Overall Set-up: MD-101, Miller Power Supply, and Control Unit

MD-101 Control Unit

Time controls

Current controls

Figure 25 - Close-Up View of Control Unit

38 Permanent magnets Tenon holding fixture

Weld joint

40 mm tube 40 mm tenon

Figure 26 – 40 mm Components Loaded in Machine Prior to Clamping

The MIAB weld machine also utilizes custom-built clevis pin load cells that

provide accurate, real-time feed back of the load being applied during upset, and an

LVDT which can be used for monitoring weld upset distance. The ARCAgent [33] monitoring system is connected to the MIAB welding machine via the alligator clips shown on Figure 27 for monitoring voltage, and the torroid shown on Figure 28 for

monitoring current. The monitoring system is then connected to a laptop computer

containing ARCAgent [33] software that provides a user friendly monitoring interface

and produces the voltage plots that were used extensively during this research.

39 Voltage leads connected to MD-101 machine

Figure 27 - Voltage Monitoring Connections for ARCAgent System

Torroid

Figure 28 - Torroid for Monitoring Current on ARCAgent System

40 3.2 Description of Components and Weld Set-Up

The research was comprised of two separate DOE experiments involving two

component sizes. In both cases, the MIAB weld joint being produced joined a hollow

rod made of 1035 mild steel to a 1018 mild steel threaded tenon. Initial development work and the first DOE was conducted with 22 mm diameter parts which were not chromium-plated. The intent of this initial research was to assess the feasibility for producing the tube-to-tenon joint, to study the effect of MIAB weld process parameters, and to establish methods for determining integrity of the joint. The 22

mm hollow rod and tenon, with a tool to hold the tenon during welding are shown on

Figure 29. 22 mm diameter tenon, 2 mm Threaded wall thickness fixture holds 22 mm diameter the tenon tube, 2 mm wall during thickness

Figure 29 - 22 mm Hollow Rod, Tenon, and Holding Fixture

In the second DOE, 40 mm tubes and tenons which are used in the construction of the MR damper discussed previously, were utilized. A schematic of

41 these parts is shown in Figure 30. Since current production of these components

utilizes Friction welding, this drawing depicts a Friction welded part. Initially, welding trials on tubes with no chromium-plating were conducted to establish

Current production tube tenon part is Friction welded

Tubes are chromium-plated ID l

Figure 30 - 40 mm Tenon-Tube Joint Details

weld parameters for the larger sized parts. Tubes for the main experiment (second

DOE) were chromium-plated on the ID utilizing an electrodeposition process. This produced a hard wear-resistant surface approximately 10 mils thick. The arc monitoring system was also introduced in the second DOE.

3.3 Mechanical Test Methods

Two destructive mechanical test methods were deployed for this research.

One test, called an ID bend or "Tulip Test", involves cutting a series of longitudinal slots through the weld joint, and bending the individual "petals" backward to

42 approximately 90º relative to the axis of the tube. This places severe tensile stresses along the ID portion of the joint, which is then visually examined for any cracking.

Figure 31 represents a schematic of a typical ID bend test procedure and Figure 32 is a picture of an actual ID bend test coupon of a MIAB weldment after testing.

WELD

Figure 31 – ID Bend or "Tulip Test" Technique

43 ID of MIAB weld is crack-free following ID Tenon bend test

Tube cut into “petals” parallel to tube axis prior to bending

Figure 32 – ID Bend Test Showing an Acceptable Weld on a 40 mm part

Uniaxial tensile testing was the other mechanical test method used to assess the integrity of the welds. Ultimate loads at failure were monitored, but the primary indicator of an acceptable weld was whether or not failure occurred along the weld interface. Figure 33 is a picture of a typical acceptable tensile test which failed in the tenon and not in the weld joint. These tensile failures typically exceeded 30,000 pounds of load, which means the stress on the welds was usually between 50 and 55 ksi at the time of the tenon failure.

44 MIAB Weld Tenon failure location

Figure 33 – Acceptable Tensile Test of 40 mm Component as Indicated by Failure in Tenon

3.4 Metallurgical Evaluation Methods

Optical and SEM metallography techniques, including EDS, were utilized

during this research project. The results were correlated with mechanical test results

in order to establish what could be considered an acceptable microstructure. The

primary objective of the optical microscopy was to determine the quality and length of the weld interface. SEM/EDS analysis was utilized to analyze weld interface fracture surfaces of failed tensile and ID bend test samples to determine the mode of

failure.

Weld interface (or bond line) length measurement was chosen as a simple method to assess the weld quality and effect of weld variables during the initial 22 mm development work, and in the first L16 DOE. A simple schematic depicting this measurement method is shown in Figure 34. This method was chosen because proper

45

MIAB weld Tube wall

Weld interface length measurement

Figure 34 – Measurement of MIAB Weld Interface Length

heating and forging action is critical to the MIAB process, and a properly forged joint will result in sufficiently long weld interface lengths. Lengths less than the thickness of the tube were considered unacceptable since the strength of the joint is compromised. The measurements were made microscopically utilizing standard microscopy software.

Although weld interface length provides a good measure of the amount of upset, it should be pointed out that excessively long weld interface lengths are not desirable. While this condition doesn't reduce weld quality, it wastes material and drives up the cost of the component. So although the limitations of this method were noted, weld interface length was chosen as the best, and easiest to quantify method for assessing the effects of MIAB weld variables on the 22 mm component.

Attempts were made to determine whether or not there were remnants of molten metal along the weld interface, and also measure how far the previously

46 molten metal had been pushed outward into the flash. However, although there is

some macrostructural evidence of previously molten material, it is typically very

difficult to microstructurally distinguish these regions in a steel weldment. This is

because the molten metal in low carbon steels initially solidifies as BCC delta ferrite.

The BCC structure has high diffusion rates which minimize segregation during

solidification. Without segregation, it is difficult to see dendritic structure which is

indicative of material that melted.

In addition, upon further cooling, the delta ferrite transforms to austenite, and

later to other phases/constituents, further masking any evidence of previously melted

material. As a result, this type of analysis was not practical, and therefore, not

included in this research. However, this information could be useful in future work,

especially considering MIAB weldments produced without shielding gas. Since

molten material in these welds is exposed to an oxidizing environment, it is likely that

if it is not sufficiently squeezed out of the weld interface, mechanical properties will

be degraded.

3.5 High Speed Video Monitoring

An Image Lake high speed video system was used to study the shape of the

arc, as well as the effects of altering the joint position within the applied magnetic

field. The picture in Figure 35 illustrates the concept of moving the joint position.

The high speed video equipment is required to view the arc since it is moving so

47

For some experiments, the parts were moved closer to the anode side Joint Location or cathode side prior to welding to change the joint location within the applied magnetic field

Cathode Side Anode Side

Figure 35 – Concept of Altering Joint Position within Applied Magnetic Field

rapidly. Video clips were typically taken at 2000 frames per second. This frame rate turned out to be insufficient to study the arc in any detail, but did provide information regarding the shape and action of the arc during the welding process. It also revealed

differences in the arc shape as a result of different joint locations. A typical frame

taken from the high speed video camera is shown in Figure 36.

48

Approximate location of top of tube wall Arc movement along top of tube- to-tenon joint

Joint gap

Figure 36 - Typical High Speed Video Image

3.6 DOE Methodology

The research conducted in this project relied heavily on a Six Sigma Design of

Experiments (DOE) methodology [34]. Compared to trial and error and one-factor- at-a-time experimental approaches, DOE is a tool for assessing the effect and impact of variables and other factors in any process. Trial and error approaches can provide a quick fix to a problem, but do not always determine the root cause or result in a significant increase in knowledge. One-factor-at-a-time experimentation relies on the

49 often mistaken belief that one factor can be held constant without affecting others.

This approach also does not provide information regarding interactive effects of two or more variables.

Full factorial designs test every possible combination of factors (variables) over a given range and provide an extensive amount of information about the process or problem being investigated. For a given process, the number of levels of factors raised to the power of the number of factors to be studied determines the size of the

DOE experiment. A response variable is chosen to assess the effect of the factors.

To determine the impact of a factor or variable, the difference between the average of

the results at each level is calculated. To determine the effect of the interaction

between factors, the factors are first coded (high or low, + or -), and then the difference between the two coded levels is calculated. Analysis of variance calculations can then be made to determine whether or not a particular factor is statistically significant in affecting a response.

Two DOE trials were conducted during this research. The first trial utilized the 22 mm components with no chromium-plating. The purpose of this DOE was to develop a good understanding of the effect of the MIAB weld variables on the quality of the tube-to-tenon weld joint. The response variable in this case was weld interface

length measurement. The design for this trial was an L16: four variables at two levels

each produces 16 possible combinations. The four variables studied were weld

current, weld time, current before upset, and upset pressure. The experimental layout

of the L16 is shown in Table 1.

50 The second DOE trial, the most important part of this research, utilized chromium-plated 40 mm components, and incorporated the arc monitoring system.

In this case, a smaller, L12 (12 combinations of variables) experiment was designed

26 Run 4 factor Central Composite Design

A BC D Upset Weld Current Weld Time Upset Current tc Pressure 1 1=175 amps 1=1.5 sec 1= 400 amps 1=12 psi 2 1=175 amps 1=1.5 sec 1= 400 amps 2=24 psi 3 1=175 amps 1=1.5 sec 2=600 amps 1=12 psi 4 1=175 amps 1=1.5 sec 2=600 amps 2=24 psi 5 1=175 amps 2= 3.0 sec 1= 400 amps 1=12 psi Full 6 1=175 amps 2= 3.0 sec 1= 400 amps 2=24 psi factorial 7 1=175 amps 2= 3.0 sec 2=600 amps 1=12 psi experiment 8 1=175 amps 2= 3.0 sec 2=600 amps 2=24 psi (Four factor, 9 2=225 amps 1=1.5 sec 1= 400 amps 1=12 psi two 10 2=225 amps 1=1.5 sec 1= 400 amps 2=24 psi level) 11 2=225 amps 1=1.5 sec 2=600 amps 1=12 psi 12 2=225 amps 1=1.5 sec 2=600 amps 2=24 psi 13 2=225 amps 2= 3.0 sec 1= 400 amps 1=12 psi 14 2=225 amps 2= 3.0 sec 1= 400 amps 2=24 psi 15 2=225 amps 2= 3.0 sec 2=600 amps 1=12 psi 16 2=225 amps 2= 3.0 sec 2=600 amps 2=24 psi

Center 17 1.5=200 amps 1.5=2.25 sec 1.5=500 amps 1.5=18 psi 18 1.5=200 amps 1.5=2.25 sec 1.5=500 amps 1.5=18 psi

19 1=175 amps 1.5=2.25 sec 1.5=500 amps 1.5=18 psi Axials 20 2=225 amps 1.5=2.25 sec 1.5=500 amps 1.5=18 psi (Run and measure only 21 1.5=200 amps 1=1.5 sec 1.5=500 amps 1.5=18 psi if 22 1.5=200 amps 2= 3.0 sec 1.5=500 amps 1.5=18 psi center points show 23 1.5=200 amps 1.5=2.25 sec 1= 400 amps 1.5=18 psi evidence 24 1.5=200 amps 1.5=2.25 sec 2=600 amps 1.5=18 psi of non-linearity) 25 1.5=200 amps 1.5=2.25 sec 1.5=500 amps 1=12 psi 26 1.5=200 amps 1.5=2.25 sec 1.5=500 amps 2=24 psi

Table 1 - L16 Experimental Layout

51 to specifically focus on MIAB welding variables expected to play a significant role when welding chromium-plated tubes. Variables were selected which were expected to be at the very edge of the MIAB weld process window. The results were correlated with the arc monitoring results.

As discussed, in the L16 22 mm experiment, weld interface length was chosen as the response variable, or the measurable dependent variable used to assess the effect of the independent variables (parameters). For this experiment, weld interface length proved to be an effective choice as a response variable. However, there are two primary disadvantages in using this response variable. The first drawback is that longer weld interface lengths imply stronger welds, but extremely long lengths are indicative of excessive upset. As discussed previously, while excessive upset does not reduce weld quality, it wastes material which adds unnecessary cost to the part.

The second problem with weld interface length as a response variable is that it does not provide any evidence of chromium presence along the bond line, the primary issue with the 40 mm tube-to-tenon joint. Therefore, another mechanism for assessing the degrading effect of chromium presence along the weld interface had to be developed for the L12 experiment.

Tensile testing was considered as a potential response variable. However, tensile tests of these weldments typically did not provide a wide range of variable, quantifiable results, which are generally considered important to the success of a

DOE. As discussed previously, tensile testing tended to result in either base metal failures (“go”) or weld interface failures (“no-go”). This was primarily due to the fact

52 that component design resulted in base metal tensile failures in the tenon at loads that

were approximately 20% below the tensile strength of the tube. Therefore, in a

tensile test, the welds never experienced full loading. Tenon failures were considered

acceptable for production purposes, but did not provide for a full range of testing of

the weld joint.

In effect, tensile testing provided a response of good or bad without much

variation in between. Such variation is important to a successful DOE.

ID bend testing, however, can provide wide range of results including partial failure

of the petals. Lengths of the cracked weld interfaces along the petals can easily be

measured with a caliper, thus providing variable, quantifiable information. It is

important to note that in a production environment any cracking of an ID bend test

would be considered unacceptable. But for the purposes of the L12 experiment, this

response variable provided necessary quantifiable evidence of mechanical property

degradation due to the presence of chromium along the weld interface.

Once the response variable decision was made, the second DOE was devised for the investigation of the 40 mm chromium-plated tube-to-tenon joint. This DOE incorporated knowledge gained from the previous L16 DOE regarding basic effects of MIAB weld process parameters on the tube-to-tenon joint. In this case, however, the DOE was primarily designed to assess the effect of two variables expected to play

an important role in the cleaning action (and therefore, action affecting chromium

presence along the weld interface) of the process: level III (expulsion) current and

level II (arc heating) time.

53 Information gained from the anode/cathode experiments described above

resulted in the addition of a joint location variable as well. Three joint locations were

evaluated: 1) centered, 2) shifted toward the anode side, and 3) shifted toward the

cathode side. Combining all these factors, the DOE became an L12 arrangement with

three joint locations, two level III currents, and two level II times (3 x 2 x 2 = 12).

The L12 layout with the resulting ID bend test crack length (mm) measurements is

shown in on Table 3.

3.7 Arc Monitoring

The ARClient [33] arc monitoring system was utilized for the 40 mm MIAB

chromium-plated tube-to-tenon weld trials. This is most likely the first attempt to use such a system for monitoring MIAB weld quality. ARCAgent [33] software, used in conjunction with the monitoring system, provides a user friendly interface for interpreting, organizing, and displaying the results. Voltage and current vs. time plots were recorded for each weld. Since all welding was conducted in the constant current

mode, the current plots did not provide significant information about the process

other than to confirm the current output of the power supply. The voltage plots,

however, revealed a vast amount of information about the process. Analysis and interpretation of the voltage plots for each weld condition, and correlation of the plots to the L12 statistical results was a very important component of this research.

54

CHAPTER 4

RESULTS

This chapter describes the results of the research on the 40 mm chromium- plated component which represents the core of this investigation. Discussion and analysis of these results follows in the next chapter. Preliminary weld development work on smaller 22 mm components was conducted for the purpose of building a knowledge base for MIAB welding tubes-to-tenons in preparation for the research on the 40 mm components. Since the 22 mm work was considered preliminary and not part of the core research, the 22 mm results and discussion sections are included in the Appendices section. Following the 22 mm development work, preliminary 40 mm component weld trials had to be conducted in order to identify appropriate ranges of weld variables for the larger sized components

Once variable ranges were identified on 40 mm components without chromium-plating, chromium-plated (ID only) tube-to-tenon weldments were produced. Tensile and ID bend test cracking observed along the weld interface of these weldments provided the first evidence of the technical challenges associated

55 with welding chromium-plated material. Much of this raw data is also included in the Appendices section. Following the preliminary trials, the L12 experiment was developed and run utilizing the voltage monitoring methodology.

4.1 Metallurgical Analysis

Optical and SEM techniques revealed the presence of an unacceptable weld

interface following the initial weld trials with the chromium-plated tubes. This

information helped guide the decisions toward the development of the second DOE.

These results, as well as the metallurgical analysis from tubes without chromium-

plating are discussed.

4.1.1 Optical Microscopy of Tubes Without Chromium-plating

Initial 40 mm trials were restricted to welding two tubes, as shown in the

photomicrograph of Figure 37. Although this particular joint exhibits excessive upset, it provides strong evidence of the plastic flow that occurs during the upset phase of the MIAB welding process. Tube-to-tenon joints were then produced and analyzed optically. Figure 38 shows a typical joint with a closer view of the bond line. The tenon is oriented on the right side of this joint.

56 Weld “flash”

Tube wall Tube wall

Deformation lines reveal significant Weld “flash” plastic flow

Figure 37 - 40 mm MIAB Tube-to-Tube Weldment Reveals Plastic Flow

4.1.2 Optical Microscopy of Chromium-Plated Tubes

Initial metallurgical analysis of the chromium-plated tube-to-tenon joint

revealed significant changes to the joint morphology compared to previous

microstructures. In particular, the weld interface periodically revealed evidence of

poor bonding, as the continuous line along the weld interface of Figure 39 indicates.

Light microscopy was unable to delineate whether this line was some sort of phase,

continuous line of inclusions, or simply an indication of poor diffusion along the solid-state region of the weld interface. Further analysis was mandated and will be discussed later in this section.

57

Weld Interface

Tenon - 1018 Tube - 1035

Weld Interface

500X

Figure 38 - 40 mm Tube-to-Tenon Weld Interface

58 4.1.3 SEM Fractography of Chromium-Plated Tube-to-Tenon Weldments

Initial ID bend and tensile tests, which are discussed in more detail later in this section, resulted in severe cracking and fractures along the weld interface. In some ID bend tests, entire petals broke off. Such failures were not observed prior to welding the chromium-plated tubes. This cracking was believed to be related to the questionable weld interface features observed optically and shown on Figure 39.

The next step was to analyze the fracture surfaces from the failed ID bend and tensile tests in an effort to determine the cause of the poor bonding. A scanning electron microscope (SEM) was deployed for this analysis. The SEM fractography revealed regions of apparent ductile failure surrounding what appeared to be small

Distinct line along weld interface is indicative of poor bonding

100X

Figure 39 - 40 mm Chromium-Plated Tube-to-Tenon Joint Reveals Evidence of Poor Bonding

59 inclusions that were smooth in appearance. Figure 40 is a typical SEM fractograph showing the characteristic fracture surface from a failed tensile test. As the figure indicates, the fracture surfaces showed evidence of dimple rupture or microvoid coalescence, combined with numerous smooth, featureless regions indicative of a decohesive type rupture mode [32].

Further SEM analysis of these smooth regions on the fracture surface was conducted using EDS (Electron Dispersive Spectroscopy) techniques. Figure 41 reveals the results of this analysis, clearly indicating high chromium concentrations at these regions. Similar EDS analysis along the regions of dimple rupture showed no such evidence of chromium. Subsequent semi-quantitative analysis of these chromium-enriched regions revealed a chromium content of approximately

50 µm

Dimple Rupture Mode Fracture Features

Decohesive Rupture Mode Fracture Features

Figure 40 - SEM Fractograph of Tensile Test Weld Interface Fracture Surface

60

Figure 41 - SEM EDS Analysis of Region of Decohesive Rupture on Fracture Surface

70 % (atomic). Unfortunately, these methods were not capable of analyzing

interstitials such as oxygen and nitrogen, but clearly established a relationship

between the poor bond quality and the presence of chromium.

4.1.4 Microhardness Testing

A typical 40 mm component microhardness result is shown on Figure 42. It should be pointed out that while this particular microhardness testing was conducted on tube-to-tenon joints that utilized forged tenons, the majority of the research was conducted on machined tenons. The significance of utilizing forged tenons will be discussed in the next section.

61

Figure 42 - Microhardness of Typical 40 mm Tube-to-Tenon MIAB Weld Joint

62 4.2 Mechanical Analysis

As discussed above, both tensile and ID bend testing of MIAB weldments produced with the chromium-plated tubing resulted in severe cracking along the weld interface during the initial weld trials with this material. A typical failed ID bend test is shown in Figure 43. In many cases during these initial trials, entire “petals” of the

ID bend tests broke off.

Weld interface fractures

Figure 43 - Failed ID Bend Test of MIAB Weldment Utilizing Chromium-plated Tube

Closer examination of the fracture surfaces of figure 43 reveals dark gray shaded regions along the fracture surface. These regions were analyzed with SEM

EDS analysis and determined to consist of the high concentrations of chromium discussed previously. Tensile testing conducted on random samples resulted in similar fractures along the weld interface. Table 2 shows a small portion of the data collected during the initial trials. This development work provided the foundation of knowledge which guided the decision making in the subsequent L12 Design of

Experiments, in which the arc monitoring methodology was introduced.

63 Trial # Arc current Upset Level II Level III ID bend test (level II) time current current current result – (level III) cracking? time 1 3.3 0.21 190 630 Yes

2 3.3 0.26 190 630 Yes

3 3.3 0.21 190 630 Yes

4 3.5 0.21 190 630 Yes

5 3.5 0.21 190 630 Yes

6 3.5 0.21 190 630 Yes

7 3.5 0.21 190 630 Yes

8 3.5 0.21 190 630 Yes

9 3.5 0.21 190 630 Yes

10 3.85 0.21 200 640 Yes

11 3.85 0.21 220 630 Yes

12 3.85 0.21 240 630 Yes

13 3.85 0.21 240 630 Yes

14 3.85 0.21 240 630 Yes

15 3.85 0.21 240 630 Yes

16 3.85 0.21 240 630 Yes

17 3.85 0.21 240 630 Yes

18 3.85 0.21 240 630 Yes

Table 2 – Typical Data From Initial 40 mm Component Development Work

64

4.3 Anode/Cathode Experiments

Previous research [6] established that arc blow effects, and the interaction between the applied magnetic field and the magnetic field created by the arc, significantly affect arc location. In particular, position of the arc relative to the ID or

OD of the tubes is influenced by these factors as the arc rotates around the tubes. It was postulated for this research that since the chromium-plating on the 40 mm tubes was located on the ID only, arc location along the tube walls during rotation could play a role in the amount of chromium ending up along the weld interface.

In order to assess the feasibility of influencing arc location along the tube walls by altering joint position within the applied magnetic field, an experiment was devised with 40 mm tubes. The experiment involved shifting both parts (Figure 35), and therefore the joint location, to two extremes within the applied magnetic field. A shift to the right effectively moved the joint toward the anode side of the current path, and a shift to the left toward the cathode side.

The arc was then initiated for a short period of time (less than a second) in an attempt to allow only a few arc rotations, and power was shut off before significant heating or upset could occur. This procedure was repeated for both joint locations.

The surfaces of the tube ends were then examined under an optical stereoscope for evidence of the arcing location along the wall thickness. The results, shown in Figure

44, provide evidence that the location of the arc relative to the wall thickness of the

65

Edge of Edge of machining lines lines Melting shifted toward OD of tube wall

Extensive Melting on ID of tube wall

Inside wall (ID) of tube

Anode Side Cathode Side

Figure 44 - Evidence of Joint Position within Magnetic Field Affecting Arc Location

tube can be altered by moving the parts outside of the center position within the applied magnetic field. As a result, it was decided that joint position would become one of the variables investigated in the second DOE for the 40 mm chromium-plated tube-to-tenon joint.

4.4 L12 DOE Based on ID Bend Test Crack Length

As in the L16 experiment, the data was analyzed statistically and presented in

graphic form. Figure 45, the Y bar Marginal Means Plot, reveals the individual

variable effects of joint location, level III current, and level II time on ID bend test

crack length. As the figure shows, increases in level III current and level II time

66 significantly reduced ID bend crack lengths while joint position had a marginal effect.

Figure 46 provides evidence of the interactive effects among these three MIAB weld variables. These results and the significance of the interactive effects are discussed in the following section.

ID Bend Weld Interface Crack Length (mm)

Table 3 - L12 Experiment with ID Bend Test Crack Length (mm) Results

67

Y bar Marginal Means Plot

Anode Level II Time Centered

Cathode

Crack Length (mm) Joint Position

Level III Current

Effect Levels

Figure 45 – Individual Variable Effect of Joint Position, Level III Current, and Level II Time on Crack Length on 40 mm MIAB Weldments

68

Figure 46 – Interactive Variable Effects of Joint Position, Level III Current, and Level II Time on 40 mm MIAB Weldments

69

4.5 Arc Monitoring Plots

The voltage plots produced a characteristic weld “signature” for each weld.

Since current levels are controlled by the weld power source which is operating in the

constant current (drooping) mode, voltage is allowed to fluctuate during the MIAB

welding process. These fluctuations are due to changes in arc position and arc gap, heating of the part and subsequent thermal expansion, expulsion, and other factors which are discussed later. As a result, the voltage vs. time plots provided a significant amount of information uniquely for each weld. Two typical voltage

“signatures” are shown in Figure 47. The characteristic “signatures” contained specific features that could be correlated to weld variable effects from the L12 experiment, and therefore, weld quality. These correlations, as well as interpretation and analysis of all the plots is provided in the following Discussion section.

70 Voltage

Volts Current

Time (s)

Voltage Volts Current

Time (s)

Figure 47 - Two Typical Arc Monitoring Plots of 40 mm Tube-to-Tenon MIAB Welds

71 4.6 High Speed Video Images

Still images from high speed video clips taken for three joint positions are

shown in Figures 48, 49, and 50. These images show the general shape of the arc, or

an arc trace, as it moves along the top portion of the tube-to-tenon joint. The arc

movement shown on each images represents approximately 25% of the circumference of the joint. When the joint is centered in the magnetic field (Figure 48), the arc

shape is mostly uniform and centered in the joint. When it is shifted toward the anode (Figure 49), a slight flaring is seen toward the right or toward the anode. But

when it is shifted toward the cathode side as shown in Figure 50, significant flaring of

the arc is observed in the cathode direction. Interpretation and analysis of the images

follows in the Discussion section.

Top of tube

Arc trace shape is mostly uniform

Figure 48 - High Speed Video Image - Joint Centered in Magnetic Field

72 Slight flaring of arc Top of tube toward the right, or anode side

Figure 49 - Joint Shifted Toward Anode Side of Arc

Significant flaring Top of tube of arc toward the left, or cathode side

Figure 50 - Joint Shifted Toward Cathode Side of Arc

73

CHAPTER 5

DISCUSSION

The results of the 40 mm chromium-plated tube-to-tenon weld trials are discussed and analyzed in this chapter. In particular, arc voltage monitoring plots for the 40 mm chromium-plated tube-to-tenon weldments are interpreted, and correlated with the DOE results. Arc welding and arc physics principles are proposed as an explanation for some of the results, and also correlated with the voltage plots. Finally, the relationship between weld quality and certain features of the voltage plots is proposed. As before, the 22 mm component development work discussion is provided in the Appendices section.

5.1 Metallurgical Analysis

5.1.1 Optical Microscopy of Tubes without Chromium-plating

Figure 37 is a photomicrograph from the initial weld development trials of 40 mm tube-to-tube joints utilizing tubes that were not chromium-plated. The

74 photomicrograph provides strong evidence of the forging action of the MIAB weld

process. As discussed above, successful MIAB welds depend on the proper expelling

of the contaminated liquid metal from the joint followed by forging of the plasticized

region in order to create intimate metallurgical contact. This results in the diffusion required to achieve a sound solid-state weld joint. Figure 38 shows the result of good diffusion, namely, no evidence of a distinct bond line.

5.1.2 Optical Microscopy of Tubes with Chromium-plating

Initial weld trials on 40 mm chromium-plated tube-to-tenons immediately

showed a severe weld interface failure mechanism not seen on previous weldments

produced with non-chromium-plated tubes. Optical metallography was first deployed

to try to better understand the mechanism. The photomicrograph of Figure 39

represents a region along the weld interface adjacent to an ID bend test petal that

fractured along the weld interface. A distinct bond line can clearly be seen. In

comparison with Figure 38, the distinct bond line of Figure 39 provides strong

evidence of poor diffusion. This joint appears to be sufficiently upset, so the presence

of the bond line was indicative of another phenomenon which resulted in the poor ID

bend test results. However, light microscopy techniques were unable to provide

further information regarding the potential cause of the bond line failure so SEM

techniques were deployed.

75 5.1.3 SEM Fractography of MIAB Welds with Chromium-plating

The fracture surfaces from the failed ID bend tests contained contrasting

regions of darker gray and lighter silver which were easily detected with the naked

eye as shown in Figure 43. When analyzed with the SEM, the dark gray regions

turned out to be the portions of the fracture surface which failed via the decohesive

mode, while the light silver regions showed evidence of ductile tearing via a dimple

rupture mode (Figure 40). Decohesive ruptures involve little or no plastic deformation and usually occur as a result of impurities [32], while dimple ruptures occur due to overload and are usually associated with ductile failures.

EDS analysis (Figure 41) revealed the presence of significant amounts of chromium (approximately 70 atomic %) in the regions of decohesive rupture. It is important to mention that the EDS spot analyzes material at the surface, as well as slightly below the surface. Therefore, it is possible that the percentage of chromium along the decohesive rupture regions of the fracture surface was even greater than

70%, as there could have been a dilution effect from iron beneath the chromium.

Furthermore, this analysis is considered semi-quantitative, and not intended to be precise. Nonetheless, the chromium presence was very clear, and the origin

(chromium-plating) was obvious.

The SEM fractograph of Figure 40 seems to indicate that these regions of enriched chromium may be some form of an inclusion, but optical microscopy did not show any such evidence. The Chromium-Iron phase diagram of Figure 21 indicates there are no intermetallics formed between chromium and iron so intermetallic

76 formation is not a likely scenario. However, the phase diagram does reveal a

considerable variance between chromium and iron, with chromium

melting 325ºC higher than iron. It is possible that the melting temperature difference

plays a role in the resulting chromium contamination of the bond line. During the arc

heating and subsequent arc cleaning phase, it is possible to envision a scenario where

the slower-to-melt chromium-plating on the ID of the tube could be expelled into the

joint just prior to upset, and then become trapped there.

Chromium is also known to have a high affinity for interstitials oxygen and

nitrogen. In the presence of an unshielded arc, melted chromium would potentially easily absorb these interstitials and remain along the weld interface as a chromium oxide, severely affected the diffusion required to achieve a good solid state weld.

Unfortunately, the microscopy techniques deployed did not provide information regarding interstitial content. In summary, these are only theories worthy of further study which were beyond the scope of this research. The most important point from the SEM analysis was that chromium presence along the weld interface fracture surfaces was confirmed, and was clearly the reason for the poor ID bend and tensile test results.

5.1.4 Microhardness Testing

As was the case with the microhardness analysis of the 22 mm component, the

40 mm MIAB weldments revealed an increase in along the weld interface

(Figure 42). As discussed previously, this region of elevated hardness is most likely

77 due to a high concentration of dislocations as a consequence of the significant forging

action at the joint. In the case of the 40 mm joint, the peak hardness is slightly shifted

toward the tube side of the joint. This is probably due to the fact that the 40 mm

tenons were produced via a forging process, and therefore, experienced significant

softening via recrystallization in the HAZ. In summary, other than the HAZ

softening in the forged 40 mm tenon, the microhardness results for both the 22 mm

and 40 mm components did not reveal any information that would suggest any significant degradation in properties as a result of the MIAB welding process.

5.2 Mechanical Analysis

The ID bend and tensile test results from the initial weld trials provided

immediate evidence of the severe degradation in mechanical properties as a result of

the presence of chromium. In some cases, the degradation was so severe that all the

“petals” of the ID bend test broke off with minimal resistance to the person

conducting the test. Such severe failures obviously suggest a profound impact on the

mechanical properties as a result of welding chromium-plated tubes if the chromium

is not sufficiently expelled from the joint. These mechanical test results during the

initial 40 mm chromium-plated tube-to-tenon welding trials provided strong

justification for the need to develop a unique MIAB welding quality control

methodology through arc monitoring techniques.

78 5.3 Anode/Cathode (Joint Position within the Magnetic Field) Experiments

The purpose of the anode/cathode experiments was to establish the effect on

the arc position (closer to the ID or OD) as a result of shifting the joint toward the

anode or cathode side of the circuit. It was believed that if the rotating arc position

relative to the thickness of the pipe could be altered, it might have an effect on the

extent of chromium ending up in the joint.

Another possible factor that may play a role in arc position is the issue of

anode heating vs. cathode heating since the rate of heating will affect how quickly the

curie temperature is reached. This, will in turn, affect the deflection of the arc by

both the applied and induced magnetic fields. A significant amount of research has

been conducted over the years regarding the anode and cathode heating mechanisms

in typical welding arcs, such as GTAW. It is well established in the GTAW process

that the anode side of the joint, which receives the electrons emitted from the cathode,

experiences considerably more heating than the cathode side. This is illustrated in

Figure 51 [22].

However, in the GTAW arc, the cathode is a tungsten (or tungsten alloy)

which readily emits electrons at typical arc temperatures and currents via a

thermionic emission process. Therefore, it is “easy” for the cathode to emit the

electrons, resulting in the majority of the heating occurring on the anode side. In the

case of MIAB welding, however, both sides of the circuit are steel. As shown in

Figure 52 [22], in order for iron to emit electrons at typical welding currents, it must

79

Volts

Figure 51 - Typical GTAW Arc Results in Much More Heating on Anode Side [22]

Figure 52 - Thermionic Emission of Fe Greatly Exceeds Melting Temperature at Typical Arc Currents [22]

80 be heated well above its melting temperature. So iron vaporizes long before thermionic emission can occur. Therefore, the anode/cathode heating mechanisms, which are well understood with other arc welding processes such as GTAW and

GMAW, cannot be applied here.

In summary, although it was beyond the scope of this research to investigate anode vs. cathode heating effects during MIAB welding, it is likely there is a difference in the rate of heating between the two sides. As a result, one side of the joint would be expected to reach the curie temperature faster than the other side of the joint, and therefore, be affected differently by the applied magnetic field. Upon reaching the curie temperature, that portion of steel is no longer magnetic and will behave similar to air or non-ferrous materials regarding its ability to transfer magnetic flux. This being the case, the joint position within the magnetic field could be expected to play a role in how the applied magnetic field influences arc location, especially during the initial heating stage.

This effect was clearly evident in Figure 44, which provides evidence of the arc traces along the tube walls during the initial stages of arcing. The tube on the left was shifted toward the anode side of the joint, while the tube on the right was shifted toward the cathode side. It is clear that the forces acting on the arc cause it to concentrate more on the ID of the tube when it is shifted toward the anode. However, once the arc is stabilized and significant heating on both sides of the joint occurs, it is

81 likely that these differences will be reduced. In order to explore this effect in more depth, joint position within the applied magnetic field was included as a variable in the L12 DOE.

5.4 L12 DOE

The L12 DOE was designed to assess relationships among the variables of joint position, level II time (arc heating time), and level III current (current just prior to upset) with ID bend test crack length. ID bend test cracking was determined previously to be a direct result of the chromium presence along the weld interface.

Therefore, it was theorized that any influence these variables had on the amount of chromium along the weld interface would reveal itself in the form of ID bend test total crack length. In order to provide a wide range of crack length data, parameters were chosen that were expected to push the extreme edges of the MIAB welding process window for this component.

Table 3 shows the raw data for the L12 experiment. Three weldments were produced per condition. Upon initial evaluation of the data, it was clear that none of the conditions resulted in all three specimens experiencing a zero ID bend test crack length. Of particular interest, condition number 4 produced the extreme range of ID bend test results in which one specimen experienced no cracking while another specimen resulted in 100% “petal fractures” (crack length = 102.8 mm). Clearly,

82 statistical analysis was required to better interpret these results. These results will be

discussed first. Analysis of the results and correlations of the results with the arc

monitoring voltage plots will then be discussed.

5.4.1 Individual Effect of Variables on ID Bend Test Crack Length

Figure 45 graphically displays the effects of the individual parameters on ID

bend test crack length. Within the range of parameters chosen, higher level III

currents and level II times show a clear effect toward reduced crack lengths. Since

the level III current is the primary parameter affecting the expulsion (cleaning action)

of molten material just prior to upset, this result indicates that the lower level III

current chosen was not sufficient for expelling chromium from the joint. The positive

effect of higher level II time suggests that the lower level II time did not provide sufficient heating for proper upset. The joint position effect was less significant than the other two parameters evaluated, but there was a small negative effect as a result of

shifting the joint toward the anode side (position -1 on the plot).

The joint position result was interesting considering the previously discussed arc position experiment, which revealed a tendency for the arc to concentrate on the tube ID when the joint was shifted toward the anode side. Since the chromium-

plating is on the ID, it is possible that a joint shifted toward the anode side of the

circuit could produce more melting of the chrome which could eventually end up in

the joint. However, this theory also suggests a beneficial effect of shifting the joint

toward the cathode side (relative to the center position), a concept not supported by

83 the data in this experiment. As discussed previously, however, interpretation of individual parameter effects in any experiment can sometimes be risky, so it is important to consider the interactive effects among the variables.

5.4.2 Interactive Effect of Variables on ID Bend Test Crack Length

The interactive plots of Figure 46 reveal two significant interactive effects

between level II time and level III current. The first result is that at the longer level II

time, there is minimal effect of level III current, but at the shorter level II time the effect of the level III current is significant. The second interactive effect between these two variables is that higher level III currents are insensitive to level II times, whereas lower level III currents produce less cracking with longer level II times. The interactive plots also seem to indicate that there is no significant interaction between joint position and either of the other two variables.

The first interactive effect will be explained and discussed. The effect is shown in Figure 53 which is a diagram extracted from Figure 46. This figure shows two simple plots with each plot revealing the effect of level II time on average ID

bend test crack length. However, one plot shows this effect when the level III current

is high while the other plot reveals the effect when the level III current is low. In

summary, the level II time effect is significant and beneficial when the level III

current is low, but has no apparent effect when the level III current is high.

84

Level II Time vs Level III Current

98.67 Level III Current = 400 Level III 10.43 Current = 800 Average Crack Length (mm) 3.00 4.50 Level II Time (s)

Figure 53 - Interactive Variable Effect of Level II Time and Level III Current

There are several possible ways to interpret this result of longer level II times

being insensitive to level III currents. The first is that longer level II (weld heating)

times will produce a larger plasticized zone adjacent to the molten material. A larger

region of plasticized material will result in a greater amount of upset of solid-state

material during the forging stage of the process, which could in turn, more effectively

squeeze any contaminated or chrome-enriched material outward into the flash.

The second possible interpretation is that excessively long heating times will result in thermal expansion of the parts being welded, reducing the gap and subsequently, the voltage just prior to upset. It is possible that a smaller gap results in

85 more effective expulsion of molten material just prior to upset. A third possibility is

that a larger volume of molten material is produced by the longer times which is less

affected by surface tension and more easily expelled from the weld zone.

The second interactive effect revealed minimal effect of level II times at the

high level III current, but improvement at the lower level III current as a result of the

higher level II time. This result correlates with the results discussed above, but

presents a slightly different way to interpret the data, providing at least one more

argument for consideration. In this case, the data suggests that high level III currents

may provide enough expulsion before upset to overcome less than ideal weld conditions, such as a level II (weld heating) time that is either border line excessive or insufficient.

Previous research on this subject showed that higher level III currents result in higher Lorentz forces on the arc, producing a greater arc rotation speed [1]. Others have argued that a faster rotation speed of the arc creates a greater centrifugal force pushing the molten metal outward. When welding without shielding gas, this force is utilized to expel the molten material outward toward the OD of the parts being welded, providing the necessary cleaning action prior to upset.

The problem with this concept is that it implies that if centrifugal forces on the molten metal were the primary forces playing a role in the cleaning action, then there would little or no expulsion toward the ID which is not the case. During this research, it could therefore be argued that greater forces which expel molten material outward could reduce the quality of the weld. This is because there is potential for

86 more chromium, which is only present on the ID of the tube, to be expelled into the joint. This at least suggests that in addition to gravity and surface tension, there may other forces involved on the liquid metal just prior to upset.

5.4.3 Effect of Variables and the Concept of Arc Force and Arc Pressure

Another factor that is likely playing a significant role in the cleaning action of

MIAB welding of tubes which has not been discussed in the published literature is the force created by the pressure of the arc. Arc pressure is often described as an important phenomenon in the GTAW process. It occurs as a result of the magnetic pinching effect incurred on the current flowing within the surrounding magnetic field it creates.

In the case of GTAW, the arc flares from the sharp point of the tungsten electrode to the work piece. Since the same amount of current is flowing through the narrow portion of the arc as is flowing in the flared portion of the arc, the result is a higher current density and greater pinching effect or pressure on the arc near the electrode. The resulting pressure gradient from high to low creates a plasma flow from the constricted portion of the arc downward into the flared portion of arc. This plasma flow exerts pressure on the molten puddle. This phenomenon is shown in

Figures 54 [21] and 55 [22].

87

Figure 54 - Magnetic Pinching Effect on GTAW Arc [22]

Figure 55 - Pinching Effect Creates Downward Flow Which Exerts Pressure on Weld Puddle Depressing It [22]

88 Pressure measurements in GTAW arcs have confirmed that significant

pressures can be developed [21]. Figure 56 shows a typical plot of arc pressure vs.

Figure 56 - Plot of Arc Pressure vs. Radial Distance in a GTAW Arc Reveals Significant Arc Pressures [21]

radial distance from the center of the arc. The units of pressure, KN/m2, are

equivalent to about 1/100th of an atmosphere, or 4 inches of water. Since molten steel

is about 8 times as dense as water, 1 KN/m2 of pressure can be equated to 0.5 inches of molten steel. This implies that even small pressures can support a significant

amount of molten material, and therefore, provide a considerable depressing effect on the molten weld puddle.

89 Other important considerations regarding the arc pressure effect and correlation with the MIAB welding process include the effects of current and arc length on arc pressure. As indicated in Figure 57, arc pressure varies linearly with current, and Figure 58 provides evidence of the significance of arc gap on pressure, depending on the shielding gas used [21].

Figure 57 - Plot of Arc Pressure vs. Weld Current in the GTAW Process Shows a Linear Relationship between Pressure and Current [22]

90

Figure 58 - Arc Gap can have Significant Effect on Pressure Depending on Shielding Gas [21]

This research is based on the GTAW arc which typically has a pronounced bell shape as it flares from the tungsten electrode to the work piece. In the case of

MIAB welding, the arc is not constricted on one end by a pointed electrode.

However, the arc does naturally flare in the middle between the anode and cathode spots as evidenced by the high speed video results. While the flared shape of the arc is obviously not as pronounced as is the case with the GTAW process, there most certainly is a flaring of the arc as the electrons first leave the part from cathode spot and then are absorbed on the anode spot. Previous research [2] has indicated a tighter constriction of the arc at the cathode spot during initial arcing stages. This was due to the fact that the cathode surface must be heated extremely high to emit electrons, and is influenced by the presence of oxides on the surface which facilitate electron emission.

91 It was beyond the scope of this research to attempt to quantify the shape of the

MIAB arc. However, it is reasonable to assume that any flaring of an arc, which most

certainly occurs during the MIAB welding process, will create a pressure differential

from the constricted portion of the arc to the flared portion of the arc. If the arc is wider at the center than at either ends as the high speed video indicates, an outward flow would be created as a result of the pressure differential. The schematic of Figure

59 illustrates this concept.

If it were possible to accurately determine the shape and size of the MIAB arc, calculations could be made based on previous research [21] to determine the arc force pushing outward that is developed during this process. In particular, the following equation could be applied:

2 μo I ⎛ R2 ⎞ F = ⎜2ln +1⎟ 8π ⎝ R1 ⎠

Where:

F = arc force µo = permeability in free space I = current R2 = maximum arc radius R1 = minimum arc radius

92 This equation is the same equation developed for the GTAW arc force calculation

[21] except the radius of the arc at the cathode (R1) is replaced by the minimum arc

radius of the MIAB arc, and the radius of the arc at the anode (R2) is replaced by the

maximum arc radius of the MIAB arc.

As discussed previously in the analysis of the GTAW arc, current plays a

significant role in the amount of arc pressure created. Figure 57 shows that doubling

the current effectively doubles the arc pressure. Although this relationship is likely

different for the MIAB welding arc due to its different shape, it is clear that by

increasing current, arc pressure is increased, thereby increasing the outward flow of

the arc described in Figure 59.

Pressure Induced Arc Flow

Tube Wall Arc Tenon Wall

Pressure Induced Arc Flow Chrome Plating

Tube Center Line

Figure 59 - Flared Arc Shape in MIAB Welding Creates Outward Pressure Induced Flow

It is proposed, therefore, that the outward flow created by the pressure differential in the arc plays an important role in the cleaning (expulsion) action of

93 level III in the MIAB welding process, and therefore, affects the amount of chromium entrapment at the joint. This would also explain why there is molten material expelled toward both the ID and OD, as opposed to the centrifugal force concept which would tend to expel molten material toward the OD only. If expulsion occurred in the OD direction only, it could be argued that more chromium (from the plating on the tube ID) would end up at the weld interface with greater expulsion.

The arc pressure theory proposes that chromium from the plating on the ID would be pushed inward, away from the weld interface, as suggested in Figure 59. These arguments support one of the major results of the L12 experiment which showed a reduction in ID bend test cracking from chromium contamination as a result of a higher level III current.

Figure 58 reveals that in some cases, short arc gaps can significantly increase arc pressure in the GTAW process. This observation may relate to one of the other important interactive effects from the L12 experiment, namely that longer level II

(weld heating) times are insensitive to level III (expulsion) currents. As discussed previously, longer weld times result in greater thermal expansion of the components being welded which produces a shorter weld gap as the arc heating proceeds. If the smaller gap produces higher arc pressures as the previous research suggests, it follows that the need for increased level III currents to produce the required expulsion would be diminished.

94 5.4.4 Effect of Arc Gap Setting

As discussed previously, the MIAB process utilizes a constant current power supply to provide the arcing current. As a result, the arc voltage is highly dependent on the setting of the arc gap between the two components being welded. Since voltage plays such an important role in the MIAB welding process, it was decided to also statistically analyze the effect of the gap setting on the ID bend test cracking lengths. The gap setting refers to the gap that was set when the parts were loaded into the machine. This gap becomes the arc gap upon initiation of the arc. Whereas the gap distance was not considered an input variable and therefore not tightly controlled, it was measured and recorded for each weld produced. Previous welding experiments had indicated that for optimum arc stability, it was important to keep the gap at approximately 1.5 mm. For this L12 experiment, the gap was therefore maintained between 1.4 mm and 1.6 mm measurements since the configuration of the machine did not allow much more precision than this. But this range of gap variation provided

for the possibility to assess the gap effect, the results of which are shown in Figures

60 and 61.

The first interesting result is the individual effect of initial arc gap on crack

length (Figure 60). Within the 2 mm gap range utilized for the research, the smaller

gaps produced the least amount of cracking. The most important interactive variable

effect involving the initial arc gap setting is shown on Figure 61. This effect reveals

that smaller gaps (closest to 1.4 mm) were not as sensitive to the effects of longer

95 level III current. This result correlates well with the previous discussion suggesting

that smaller gaps produce higher arc pressures, which may assist in the cleaning action during the application of the level III current.

It should be mentioned however, that as Figure 60 indicates, there is a wide variation in the number of data points for the gap setting. This is due to the fact that gap was not chosen as an input variable for the L12, but analyzed later after the experiment was completed. As a result, whereas it does reveal a very interesting trend regarding the effect of the gap, the statistical relevance of the data would have to be considered marginal. Further studies are suggested, and are discussed in the

Future Work section later in this report. The L12 results and subsequent analysis of the results will now be correlated with the high speed video images, and finally, the arc monitoring plots later in this section.

96 Y bar Marginal Means Plot

120

100 Arc Gap 2 data pts 1 of these points is the outlier from TC 4

80 Level III Current Level II Time Joint Position Lev III Current 60 Level II Time Joint Position Gap 14 data pts

40 10 data pts ID Bend Test Crack LengthCrackID Bend(mm) Test

20 6 data pts

4 data pts

0 -1 0 1 400 800 3 4.5 1.4 1.45 1.5 1.55 1.6 Effect Levels

Figure 60 – Individual Variable Effects Including Effect of Gap on Crack Length

97 Lev III Current vs Gap

102.80 Gap = 1.4 Gap = 1.45 Gap = 1.5 Gap = 1.55 Gap = 1.6 4.10 Average ID Bend Crack Length (mm) (mm) Length Crack Bend ID Average 400.00 800.00 Level III Current

Figure 61 – Interactive Variable Gap Effects on Crack Length – Level III Current

5.5 High Speed Video Image Interpretation

The high speed video images of Figures 48, 49, and 50 reveal the general

shape of the arc as it moves along the top portion of the tube-to-tenon joint. The

resolution of this camera and relatively slow 2000 frames/second frame rate was not

sufficient for in-depth analysis of the arc motion and shape. However, the variation in the overall arc profile as a result of placing the joint in different positions within the applied magnetic field is evident. Figure 50 represents a MIAB weld shifted toward the cathode side. In this case, the arc can be seen to be flaring out of the joint.

This shows that the arc is rotating along the OD edge of the joint, and correlates well

98 with the arc tracing experiment (Figure 44) which revealed a tendency for the arc to move toward the OD of the tube wall when the joint was shifted toward the cathode side.

In Figure 48 the arc movement is obscured by the joint, indicating that arc rotation is oriented more toward the ID of the tube wall, also confirming the results of the arc tracing experiment. Compared to the arc tracing experiments which provided evidence of arc position at the very early stages of arcing, the video images were shot well after the arc stabilized. These images verified that the tendency for the arc position to be altered by joint position continues even after the parts are heated and the arcing is stable. Considering the obvious differences in arc position and shape for different joint locations within the magnetic field, it is surprising that the L12 data did not result in a stronger trend toward joint position affecting ID bend crack length.

Figure 50 also reveals a tendency for the arc to flare toward the left (cathode) when it is shifted toward the cathode. During the weld trials, the chromium-plated tubes were always placed on this side with the tenons on the right (anode) side. In the centered joint of Figure 49, the arc seems to show a very slight bias toward the cathode side, but it is difficult to say conclusively considering the resolution of these pictures. Again, further work is suggested in which the chromium-plated tubes be placed on the anode side.

99 5.6 Analysis of Arc Monitoring Voltage Plots - Correlation with DOE Results

The arc monitoring methodology produced voltage vs. time plots which

represented voltage “signatures” for each weldment producing during the L12 DOE.

Most of the plots contained similar generic characteristics, but also revealed unique

features which could be related to critical variable effects and subsequent weld

quality. In this section, the generic characteristics of the voltage vs. time plots are

discussed first. This is followed by a discussion and analysis of the voltage plots for each important weld condition produced during the L12 experiment, and correlation of these plots with the statistical results of the L12. In this way, relationships are proposed between chromium-plated tube-to-tenon MIAB weldment quality, and specific features of the voltage plots.

5.6.1 Analysis of Voltage Plots – Interpretation of Characteristic Features

Several characteristic features of features of the voltage plots were observed

in most welds. Figure 62 shows a typical plot that contains all of the most common features. The first observation to be made is the initial rise in voltage that occurs.

This is most likely due to the arc initiating along the ID of the tube-to-tenon joint due

to the arc blow effects shown previously on Figure 12, and then moving toward the

OD of the joint as localized heating results in the curie temperature being exceeded.

As the curie temperature is reached locally, that region along the tube wall no longer

easily conducts the magnetic flux lines surrounding the flow of current, and as a

100 result, the arc blow effect begins to push the rotating arc outward. This phenomenon

was observed by previous researchers [6] and was discussed in the Technical Review section. As the arc moves toward the OD, it flares out of the joint as evidenced by the

high speed video images. When the arc flares outward, its length is effectively increased, resulting in higher recorded voltages. The outward movement of the

rotating arc eventual results in a more uniform heat distribution across the wall

thickness of the tube and tenon. At this point, the arc can be considered stabilized as

evidenced by the peak voltage peak. Initial melting of the parts may also widen the

gap and contribute to the rise of voltage. This effect is evident to some degree on

every plot analyzed.

A second important and interesting observation from the plots is the overall

drop of the voltage that occurs with time following the initial rise. In some cases, the

drop results in a voltage “plateau” that may be an important feature in terms of

predicting weld quality and the effect of important variables. This feature is

discussed later in this section. The pronounced drop in voltage is occurring due to

heat flow into the parts. As heating progresses, thermal expansion in the axial

direction of both the tenon and the tube results in a narrowing of the arc gap. Just

before upset, a voltage spike is observed. This spike occurs due to the rapid increase

in the applied current which results in expulsion of molten metal and an increase in the arc gap just prior to upset. The voltage spike may be another important feature in terms of predicting weld quality and is also discussed later.

101 Thermal Expansion Arc Stabilization Reduces Arc Gap

Arc Initiates Volts Rotating Arc Moves Toward OD of Joint Expulsion Prior to Upset Voltage in Red Increases Arc Gap

Current in Black

Time (s)

Figure 62 - Common Features Observed in the Voltage Plots

5.6.2 Analysis of Voltage Plots – Effect of Level II Time

The statistical results of the individual variable effects from the L12 experiment revealed that longer level II (arc heating) times resulted in a reduction in

ID bend test crack length. Analysis of the interaction between variables revealed that the positive benefit of longer level II times only occurred when the level III current was low. These results will now be correlated with the appropriate voltage plots

102 shown in Figures 63 and 64. Figure 63 shows the effect of level II time when the level III current is low, and Figure 64 shows the same effect when the level III time is high.

The first observation that can be made is the effect of the longer level II time

in both plots. In each case, the longer times resulted in a lower voltage or voltage

“plateau” of 22-23 volts just prior to the expulsion stage. The “plateau” suggests that

a steady-state heat flow condition has been achieved in which there is no further

significant thermal expansion of the parts. It also suggests that a minimal arc gap has

Level II Time = 3.0s Level II Time = 4.5s Level III Current = 400a No Expulsion Level III Current = 400a Thermal Expulsion Expansion

Voltage Plateau

Figure 63 - Increase in Level II (Arc Heating) Time at a Constant Low Level III Current Results in Voltage Plateau Prior to Upset

103 Level II Time = 3.0s Minimal Level II Time = 4.5s Level III Current = 800a Expulsion Level III Current = 800a Significant Expulsion Volts Volts Voltage Plateau

Time (s) Time (s)

Figure 64 - Level II Time Effect at Higher Level III Current

been achieved since there is no further drop in voltage. Both of these conditions also

produced a larger voltage spike prior to upset, indicative of a greater amount of expulsion. This voltage spike occurs as the molten metal is expelled rapidly from the joint, creating an increase in the arc gap just prior to upset.

As discussed previously and shown on Figure 58, with the GTAW arc,

increases in arc pressure can result from decreases in arc gap distances [22]. This

phenomenon is also shown in Figure 65, which reveals how arc pressure in a helium-

shielded GTAW arc increases with smaller arc gaps and decreasing distances from

the center of the arc. Furthermore, arc pressure has been shown to be proportional to

I2/R2 [2], where I = arc current (amps), and R = radius of the arc. Smaller gaps would

likely have smaller diameter arcs, contributing to increases in pressure. These concepts suggest that the smallest gaps resulting from thermal expansion of the parts

104

Figure 65 – Arc Pressure Variations at Various Arc Lengths for a GTAW Arc

may allow for the greatest expulsion of chromium from the joint prior to upset. These results correlate well with the statistical results of the L12 experiment which revealed a beneficial individual variable effect due to longer level II times.

Of particular interest from the L12 statistical analysis was the interactive effect between level II time and level III current (Figure 46), which indicated that level III current had a minimal effect when the level II times were at the high levels.

But level III current had a strong effect when level II times were low. The voltage plots of Figures 63 and 64 display graphic evidence of this interaction. On the low

105 level III current plots of Figure 63, only the high level II time plot reveals evidence of

expulsion. In Figure 64, the high level III current plots, expulsion is evident with both level II times.

Therefore, it can be concluded that when the level II times were low, a higher level III current was required to achieve expulsion. When the level II times were high, expulsion was achieved in both cases. This implies that the smaller gaps created with the longer times resulted in greater arc pressure and subsequent expulsion regardless of the magnitude of the level III current. So if the arc gap is sufficiently small prior to the application of the level III current, the process potentially could be considered more robust and less sensitive to the level III current.

5.6.3 Analysis of Voltage Plots - Effect of Level III Current

In this case, level III current effects are compared and contrasted for given

level II times. Figure 66 shows the low level II time plots and Figure 67 the high

level II time plots. These results reveal the impact of level III current on arc pressure.

At the lower times (Figure 66), higher level III currents were required to achieve any

expulsion, whereas at the higher times (Figure 67), expulsion was evident in both

cases but significantly increased with the higher level III current. As discussed

previously, current also plays a significant role in arc pressure. Figure 68 is a plot of

arc force vs. current which summarizes the results from several research projects on

this subject [22]. This data was gathered from actual arc force measurements. It is

easy to see from this plot that for some researchers as much as a five-fold difference

106

Level III Current = 400a No Expulsion Level III Current = 800a Level II Time = 3.0s Level II Time = 3.0s Expulsion

Figure 66 - Level III Current Has Significant Effect on Expulsion at Short Times

Level III Current = 400a Level III Current = 800a Level II Time = 4.5s Level II Time = 4.5s Minimal Expulsion Significant Expulsion

Figure 67 - Expulsion at Long Level II Times is Increased at High Level III Currents

in arc force produced between 400 and 800 amps (the two level II currents utilized in

this research) was observed. Again, although this data is for a bell-shaped GTAW arc, it seems likely that similar trends would exist for the MIAB arc, but perhaps

107

Figure 68 – Arc Force vs. Current

would not be as pronounced. This analysis again supports the statistical evidence from the L12 experiment, which showed reduced cracking at higher level III currents.

It could also be surmised that higher level III currents make the process more robust to variations in level II times by creating sufficiently high pressures even if the gap is large. This again supports the theory of the importance of arc pressure, and the relationship between arc pressure and arc gap.

108 5.6.4 Analysis of Voltage Plots - Effect of Gap Setting

Finally, the effect of initial gap setting on the voltage plots is discussed. As

shown in Figures 60 and 61, smaller initial gap settings resulted in a trend toward

reduced cracking. Again, it is important to note that gap settings were not controlled

input variables in the L12 experiment, but represent measurements taken and

recorded during the welding trials. As a result, there was no attempt to generate

specific numbers of data points at different gap settings. Therefore, the L12 analysis,

which showed a beneficial effect from smaller gap settings, would require more data

points to be considered statistically relevant. Nonetheless, the trend was very interesting and the voltage plots were analyzed for the various gap settings and correlated with the L12 results.

Figure 69 shows the typical plot profiles of two gap setting extremes. These plots represent welds that were made using the same parameters, but the weld on the left utilized a 1.4 mm gap and the weld on the right utilized a 1.6 mm gap. This range represented the extremes of the gap settings used during the L12 experiment. The gap setting determines the arc gap distance at the beginning of the arc cycle. As the plots indicate, the smaller gaps resulted in lower voltages throughout the welding cycle. The most interesting difference, however, was that the voltages just prior to the application of level III current were consistently 1-2 volts lower with the 1.4 mm gap vs. the 1.6 mm gap. This occurred even though the voltage plateaus were usually reached in both cases. This suggests that even with a steady-state heat flow condition stabilizing the thermal expansion effect, the initial gap setting may play a role in the

109

Gap Setting = 1.4 mm Gap Setting = 1.6 mm

Voltage Plateau = 23 volts Voltage Plateau = 21 volts

Arc Stabilization Arc Stabilization

Figure 69 - Gap Setting Affects Level of Voltage Plateau and Time of Arc Stabilization

size of the gap just prior to the application of level III current. Per previous discussions, smaller gaps may result in higher pressures and more efficient cleaning action. This may explain one of the benefits from the smaller gap settings.

Further analysis of the plots of Figure 69 reveals another interesting difference between the two voltage plots. With the smaller 1.4 mm gap setting, arc stabilization is achieved earlier in the weld cycle. This is evidenced by the fact that the voltage peak on this plot occurs almost 1 second earlier than the voltage peak on the plot produced with the 1.6 mm gap. Earlier stabilization of the arc will result in significant heating of the parts to occur earlier in the cycle.

Arc physics can again be applied to explain this observation [22]. In order to achieve an arc, electrical breakdown must first occur in the atmosphere between the parts being welded. When breakdown occurs, the gas (air) in the joint becomes a

110 conductor. Breakdown results when an electron is sufficiently accelerated in the gap such that it has enough kinetic energy to ionize an atom in the gas. Ionization occurs

when the electron collides with the gas atom, resulting in a separation between the positively charged atom nucleus (ion) and the negatively charged electron. Paschen’s

Law states that the breakdown is related to voltage, arc gap, and gas pressure given by: Vs = kph, where Vs = voltage required for breakdown, k = Paschen constant

which depends on the gas, p = pressure of the gas, and h = gap distance. These

relationships are shown graphically on Figure 70 [22].

Figure 70 – Paschen’s Law [22]

Paschen’s Law also relates electrical breakdown of a gas to the electric field,

defined as: E = V/h. It is the electric field that accelerates the electron across the gap

creating the required kinetic energy for ionization. As this relationship shows, for a

111 given applied voltage, smaller gaps result in greater electric fields. As a result,

electrical breakdown and stabilization of the arc can occur more easily, explaining the

beneficial result of smaller gaps in the MIAB welding process shown on Figure 80.

5.6.5 Summary of Arc Monitoring Voltage Plot Analysis

The voltage plots clearly provided a significant amount of information regarding the effects of critical MIAB weld variables for this application. Correlation of specific features from these plots with the weld variable effects analyzed statistically in the L12 experiment was usually very good. It should be mentioned, however, that not all of the plots that contained features thought to be indicative of a

good weld produced crack-free welds. One of the possible reasons is that the MIAB

weld variables chosen for the L12 experiment were expected to be on the extreme

edges of the process window for the 40 mm chromium-plated tube-to-tenon joints.

This was required in order to produce a wide range of weld interface crack lengths to

enhance the subsequent statistical analysis of the results. In summary, this research

showed the feasibility for producing MIAB welded chromium-plated tube-to-tenon

joints, revealed the effect of critical variables, and proposed a method for monitoring

the quality of these weldments. Undoubtedly though, much more development work,

interpretation, and analysis of this methodology is required before applying it to a

production environment.

112 5.7 CONCLUSIONS

The MIAB welding process proved to be an effective welding technique for

the tubes-to-tenon joint. Feasibility for MIAB welding chromium-plated tubes-to-

tenons was established, although significant technical challenges to producing this

joint were discovered. The effect of critical MIAB weld variables was established for

this application. The use of arc monitoring equipment, in combination with high

speed video, metallurgical and mechanical analysis, and a Design of Experiment

statistical approach, provided significant insight into producing this joint. Specific

conclusions from this research program are as follows:

1) Feasibility for MIAB welding the chromium-plated tube-to-tenon joint was established.

2) The potential for MIAB weld interface failures as a result of the presence of chromium enriched regions at the weld interface was discovered. The chromium

enriched regions were most likely oxides that formed during arcing process and later

became trapped in the joint.

3) Beneficial effects of level II time, level III current, and arc gap toward reducing the chromium-induced weld interface cracking was established. Each of these effects played a role in improving the expulsion process, which more effectively removed chromium from the joint.

113 4) A methodology for monitoring MIAB weld quality of chromium-plated tube-to-tenon joints through the use of voltage monitoring, and the subsequent

interpretation of voltage “signatures” was proposed

114 5.8 FUTURE WORK

5.8.1 Further Characterization of Fracture Surfaces

While the presence of chromium along the MIAB weld interface was clearly

established during this research, the precise chemical composition and the morphology of the chromium-enriched regions was not. This is because the SEM

EDS analysis techniques utilized in this research are semi-quantitative, and do not

provide much precision. These techniques are also not capable of detecting interstitials such as oxygen. It is therefore proposed that more extensive chemical characterization techniques be deployed to more precisely analyze the chromium- enriched regions.

5.8.2 Shielding Gas Effects

If it is determined that the chromium-enriched regions along the weld

interface are actually chromium oxides, the use of shielding gas may provide some

benefit by not allowing oxygen to interact with the chromium. Future work should

include a variety of shielding gases, and there impact on chromium presence along the weld interface.

115 5.8.3 Anode/Cathode Experiments

During this research, the chromium-plated tube was always placed on the

anode side (left side facing the machine) and the tenon on the cathode side. Since the behavior of the arc at the anode spot has been shown to be different than at the cathode spot, a switch in joint orientation may provide further insight regarding chromium presence at the weld interface. A simple initial experiment would be to weld a group of parts with each orientation, and determine any differences with the metallographic and mechanical techniques used in this research.

5.8.4 Effect of Initial Gap Setting

The initial gap setting proved to be an important variable in this experiment.

This setting determines the arc length during the initiation of the arc. During this

research, only a small range of gap setting lengths were analyzed. The results for this

analysis provided insight regarding the importance of the initial gap, but were not

considered statistically relevant since gap variations were not part of the DOE, but

interpreted later. Future work on chromium-plated tube-to-tenon joints should focus

specifically on a wide range of gaps do determine whether or not gap length plays an

important role in chromium presence at the weld interface.

116 5.8.5 Ratio of Solid-State Weld Interface Length to Overall Weld Interface Length

The MIAB weld interface consists of a solid-state bond region which transitions to the previously molten material which is squeezed outward into the flash.

This transition is not easy to see microstructurally but can be seen when viewing the weld macrostructure. This molten material is most likely oxidized during MIAB weldments that are made without shielding gas. The molten material also most likely contains the chromium that produced the poor welds during this research. It is possible, therefore, that a higher ratio of previous molten material to solid state bond length along the entire weld interface might be degrading to mechanical properties, and is worthy of further study.

5.8.6 Further Analysis of Weld Voltage “Signatures”

This research program established the possibility for real-time MIAB weld quality monitoring through the use of arc monitoring to produce weld voltage

“signatures”. However, much more research on this approach is required before such a methodology can be utilized in production. In particular, the importance of the voltage “plateau” as it was suggested during this research program needs further exploration. It is also possible that pattern recognition techniques could be deployed for a more thorough analysis of the voltage plots toward the establishment of MIAB weld quality acceptance criteria.

117 5.8.7 Continuation of High Speed Video and Arc Pressure Analysis

The high speed video analysis of this research provided insight regarding the general shape of position of the arc as it rotated around the joint. However, the frame rate of this equipment was limited, and most of the video clips were shot at 2000 frames/per second. This frame rate was insufficient for detailed observation of the arc. Further research utilizing much higher frame rates and better resolution is suggested. This capability could provide for accurate measurements of the arc profile and determinations of arc pressures.

118

REFERENCES

[1] Kim, Choi, "A Study on the Numerical Analysis of Magnetic Flux Density by a Solenoid for Magnetically Impelled Arc Butt Welding", Proc. Instn. Mech. Engrs. Vol.217 Part B:J. Engineering Manufacture

[2] Steffen, Welz, "Pressure Welding of Tubes with a Magnetically Displaced Arc", Schweißen und Schneiden Translation, 4/1982, E70-E72

[3] Nentwid, Appel, "Coil Systems, Magnetic Field Distribution and Arc Behaviour in Pressure Welding with Magnetically Impelled Arc", Welding and Cutting, 1/1995, E9-E11

[4] Kachinskiy, Krivenko, Ignatenko, "Magnetically Impelled Arc Butt Welding of Hollow and Solid Parts", Welding in the World, Vol. 46, no. 7/8, 2002, 49-56

[5] Kuchuk-Yatsenko, et. al., "Control of the Arc Moving in a Narrow Gap Under the Effect of a Magnetic Field in Press Welding of Pipes", Welding International, 1988, no. 11, 965-968

[6] Sato, Katayama, Ioka, Otani, "An Experimental Study of Rotational Behaviour of the Arc During Magnetically Impelled Arc Butt Welding", Welding International, 1991, 5(1), 5-10

[7] Kuchuk-Yatsenko, Syrovatka, Kuznetsov, "Speed of Movement by an Arc in the Gap Between a Tube and a Plate Under the Action of a Magnetic Field", Automatic Welding, November, 1983, 23-26

[8] Taneko, Arakida, Takagi, "Analysis of Arc Rotation Velocity in Magnetically Impelled Arc Butt Welding", Welding International, 1987, Vol. 3, 247-253

[9] Mori, Yasuda, "Magnetically Impelled Arc Butt Welding of Aluminum Pipes", Transactions of the Japan Welding Society, Vol. 21, No. 1, April 1990, 3-10

119 [10] Nentwig, Schmidt, "Magnetic Field Distribution During Pressure Welding of Magnetic and Non-Magnetic Components with a Magnetically Controlled Arc", Welding and Cutting, 10/1986, E169-E171

[11] Welz, Nentwig, "Effects of Shielding Gas, of the Heating and Upsetting Process in Pressure Welding Using a Magnetically Moved Arc", Welding and Cutting, 4/1988, E65-E68

[12] Johnson, Carter, Dinsdale, Threadgill, Wright, "Magnetically Impelled Arc Butt Welding of Mild Steel Tubing", Welding Journal, November 1979, 17-27

[13] Welz, Nentwig, Schwarzkopf, "Magnetically Impelled Arc Pressure Welding of Non-Magnetic Steels", Welding and Cutting 2/1990, E24-E26

[14] Xiancong, Ruilin, et. al., "A Study of Magnetically Impelled Arc Butt Welding", The Welding Institution of The Chinese Mechanical Engineering Society, 6-8 September, 1984, 1-6

[15] Kalev, Mikhailov, V'lchev, "Calculation of Temperature Fields in Welding with a Magnetically Controlled Arc with the Power Changing with Time", Welding Production, October 1986, 28-29

[16] Hone, "Magnetically Impelled Arc Butt Welding", Production Engineer, February 1989, 38-40

[17] Hagan, Riley, "An Industrial Application of MIAB Welding of Tubes: A Rear Axle Cross Tube Assembly", Second International Conference on Pipe Welding, London, 20-22 November 1979, Volume 1 - Papers, Paper 17, 51-58

[18] Hiller, Schmidt, Breiksch, "Use of the Magnetarc Welding Process in the Production of Truck Cab Suspension Systems", ThyssenKrupp Techforum, December 2003, 40-43

[19] ASM Handbook, Volume 8, 8th Edition, "Metallography, Structures, and Phase Diagrams", 1973

[20] Vedani, Previtali, Vimercati, Sanvito, Somaschini, "Problems in Laser Repair- Welding a Surface-Treated Tool Steel", Surface and Coatings Technology 201 (2007), 4518-4525

[21] Lin, Eagar, "Pressures Produced by Gas Tungsten Arcs", Metallurgical Transactions B, Volume 17B, September 1986, 601-607

120 [22] Richardson, "Physics of Arc Welding", The Ohio State University, Welding Engineering 801 Class Notes, Copyright 2005

[23] "Precision Butt Welding of Axle Tubes at Vauxhall", no author listed, Sheet Metal Industries, October 1987, 520

[24] "Magnetarc Welding Technology", no author listed, Welding and , May/June 1987, 186

[25] Haman, "Welding Process Meets Modern Production Line Demands", Welding Journal, May 2001, 37-40

[26] Loebner, "Magnetarc Welding Theory and Practice", Second International Conference on Pipe Welding, London - 20-22 November 1979, Volume 1 - Papers, Paper 18, 29-37

[27] Black, "Magnetically Impelled Welds Join Tubular Sections", Advanced Materials & Processes, 12/99, 11

[28] Welz, Nentwig, Schwarzkopf, "Experiments in Selective Control of Arc Movement when Welding with a Magnetically Impelled Arc", Welding and Cutting 5, 1989, E82-E84

[29] Ganowski, "The Magnetarc Welding Process", Welding and Metal Fabrication, June 1974, 206-213

[30] Ivkovich, “Arc-Weld Monitoring with Coordinated Part Tracking”, 5th Robotics Conference, February 2001, presentation only

[31] Lippold, “Welding II”, The Ohio State University, Welding Engineering 612 Class Notes

[32] Lippold, “Special Topics in Welding Engineering”, The Ohio State University, Welding Engineering 715 Class Notes

[33] Arc monitoring equipment and software provided by IMPACT Engineering, Inc.

[34] Hegwood, McCray, “Six Sigma Green Belt training”, Delphi, November 2007

121

APPENDIX A

A.1 22 mm Component - Results

As discussed previously, the primary purpose of MIAB welding the 22 mm

tubes-to-tenons was to first establish feasibility for MIAB welding tubes-to-tenons,

and then to develop a MIAB welding knowledge base to help guide the 40 mm

chromium-plated tube-to-tenon research which followed. Feasibility for producing

the tube-to-tenon joint was established, as were metallurgical and mechanical techniques for assessing weld integrity. A critical variable was identified inadvertently as a result of an electrical malfunction in the MIAB weld controller.

Finally, significant knowledge was gained about the process and the effect of specific

variables through a Design of Experiments approach.

A.1.1 Metallurgical Analysis

Microhardness and optical metallography were the metallurgical analysis

techniques initially utilized in the 22 mm development work. Only a small amount of

microhardness testing was conducted since the materials being welded are not known

to have high hardenability.

122 A.1.1.1 Microhardness Testing

Microhardness traverses on randomly selected pats were also conducted and

correlated with the other methods for assessing the weld integrity. Figure 71 shows a typical traverse.

#11 Microhardness

500.0 50.0

450.0 45.0

400.0 40.0 Tube Side Tenon Side 350.0 35.0

300.0 30.0

HK Value 250.0 25.0 HRC Value HK Value HRC Value 200.0 20.0

150.0 15.0

100.0 10.0

Bond Line 50.0 5.0

0.0 0.0

0 8 6 4 2 0 8 6 4 2 0 8 6 4 2 0 6 4 2 0 8 6 5 3 2 1 9 7 6 5 4 3 1 0 9 7 4 3 2 1 8 .6 .6 .6 .6 .5 .5 .5 .5 .5 .5 .5 .4 .48 .4 .4 .4 .4 .39 .3 0 0 0 0 0.60 0 0 0 0 0 0 0.5 0 0 0 0 0.458 0 0.4 0 0 0 0 0.374 Coordinates in Inches

Figure 71 - Microhardness Traverse from Tube (left) to Tenon (right)

A.1.1.2 Optical Microscopy of Bond Region

In addition to the weld interface length measurements discussed previously,

the weld region was examined for any evidence of voids, lack of fusion, inclusions,

etc. Figure 72 is typical digital photo of a weld of high integrity. In Figure 73, the

entire 22 mm diameter tenon-to-tube MIAB weld region is shown. Figure 74 shows

123 an example of a weld in which sufficient upset was not achieved at the end of the weld cycle, and a closer view of such a weld in Figure 75 reveals voids that can be seen along the weld interface.

Evidence of previously molten material Tube

Weld interface

Tenon

Figure 72 - Optical Micrograph of a Typical MIAB Weld

Tube walls

Tenon

Figure 73 - Macrosection of 22 mm Tenon-to-Tube MIAB Weld

124

Evidence of previously molten material in joint

Figure 74 - MIAB Weld Joint Reveals Insufficient Upset

Voids along weld interface

Figure 75 - Voids Along Weld Interface Can Result from Insufficient Upset

125

A.1.2 Mechanical Analysis

ID bend and tensile test results are discussed. These methods were determined to be effective methods for assessing weld integrity, although tensile did not provide the range of results that ID bend testing did. As a result, tensile testing was not used in the DOE’s.

A.1.2.1 ID Bend Testing

Figure 76 is an example of an ID bend test coupon which was cut in half to

reveal its features. ID bend testing was not used in the L16 DOE analysis, but was

No visible cracking along weld ID

Cracking at tenon shoulder not close to weld

Figure 76 - Portion of Acceptable 22 mm ID Bend (“Tulip”) Test Coupon

126 conducted on random weldments with tensile testing to support the metallographic results. All ID bend tests conducted on MIAB weldments produced with the optimum L16 parameters were crack-free in the weld region.

A.1.2.2 Tensile Testing

As discussed above, tensile tests were conducted in conjunction with ID bend testing in order to support the bond length measurement analysis. The test results were not used in the L16 analysis. Although ultimate tensile loads at failure were monitored, the tensile test was basically considered to be “go” or “no-go”. An acceptable (“go”) tensile test was considered one in which the failure occurred in the base metal as shown in Figure 77. Any evidence of weld interface fractures as a

Tensile test failed in tenon away from the ld

Figure 77 - Acceptable 22 mm Tensile Test Results in Base Metal (Tenon) Failure

127 a result of the tensile test were considered to be unacceptable (“no-go”) tensile tests.

All tensile tests on MIAB weldments made with the optimum L16 conditions failed in

the base metal.

After the completion of the L16 experiment, more MIAB welded parts were

produced for validation testing. This type of testing, which includes tensile testing, is

designed to assess the parts worthiness as a potential production suspension

component. Optimal parameters from the L16 experiment were used to weld the parts. Early in the testing, it was discovered that some of the parts were failing catastrophically along the weld interface during tensile testing in a manner not seen before. Figure 78 shows a typical failure. Since no such failures occurred during any of the previous L16 analysis, these results were extremely puzzling. It was

Tensile Failure Along Weld Interface

Figure 78 - 22 mm Failed Tensile Test Due to Improper Parameters from Electrical Short in Controller

128 subsequently determined that a malfunction in the control unit due to an electrical short was resulting in an excessively low current delivered to the parts just prior to upset. This unintentional result provided insight regarding the importance of the

“pre-upset” current, later referred to as level III current.

A.1.3 L16 DOE Based on Weld Interface Length Measurement

As discussed previously, the initial development work on MIAB welding of the tube-to-tenon joint was based on an L16 DOE methodology. In this experiment, the length of the weld interface, as viewed on an optical microscope, was established as the primary criterion for assessing weld quality and the effect of MIAB weld variables. A commercially available metallographic software package called Pax-It provided the tool for conducting the weld interface length measurements. An example of this measurement technique is shown in Figure 79.

Metallographic software program provides accurate measurement of weld interface lengths

Figure 79 – Weld Interface Length Measurement Technique Using Pax-It Software

129 The results of the L16 revealed the effect of weld current, weld time, current

prior to upset, and upset pressure on weld interface length. These effects are shown in the Y bar marginal means plot of Figure 80. To summarize, the plot shows that higher levels of weld current, weld time, and upset pressure all have a positive effect on bond length, while upset current (later referred to as level III current) had a minimal effect. Further statistical analysis of the data, which considers all interactions, is shown on Figure 81. These plots provide information regarding the combined effects of parameters and will be discussed further in section 11, as will the

Y bar marginal means plot.

130 Y bar Marginal Means Plot Bond Length

4.5

4

3.5

3

2.5 Weld Current Weld Time Upset Current 2 Upset Pressure

1.5

1

0.5

0 -1 1 -1 1 -1 1 -1 1 Effect Levels

Figure 80 – MIAB Weld Variables Weld Current, Weld Time, and Upset Pressure Increase Length of MIAB Weld Interface

131 Weld Time vs Weld Current Weld Current vs Upset Weld Current vs Upset Current Pressure

4.62 Upset Wel d Pressure = - 4.62 Upset 4.62 Current = -1 1 Current = -1 Wel d Upset Upset Current = 0 Pressure = Current = 0 2.76 Wel d 2.76 2.76 0 Upset Current = 1 Upset Current = 1 -1.00 1.00 -1.00 1.00 -1.00 1.00 Pressure = 1

Upset Current vs Weld Upset Current vs Weld Time Weld Time vs Upset Current Current 4.62 4.62 Wel d Ti me = Upset 4.62 Wel d -1 Current = -1 Current = -1 Wel d Ti me = Upset Wel d 0 Current = 0 Current = 0 2.76 2.76 Wel d Ti me = 2.76 Upset Wel d 1 Current = 1 -1.00 1.00 Current = 1 -1.00 1.00 -1.00 1.00

Upset Pressure vs Weld Upset Pressure vs Weld Upset Pressure vs Upset Current Time Current

4.62 Wel d 4.62 Wel d Ti me = 4.62 Upset Current = -1 -1 Current = -1 Wel d Wel d Ti me = Upset Current = 0 0 Current = 0 2.76 2.76 2.76 Wel d Wel d Ti me = Upset -1.00 1.00 Current = 1 -1.00 1.00 1 -1.00 1.00 Current = 1

Figure 81 – Interactive Variable Effects of MIAB Weld Parameters on Weld Interface Length

132

A.2 22 mm Component – Discussion

A.2.1 Metallurgical Analysis

A.2.1.1 Microhardness Testing

The microhardness plot of Figure 71 shows that the highest hardness in this

particular MIAB weld joint occurs along the centerline of the weld. This is not

surprising considering the fact that there is significant plastic flow (see Figure 37)

occurring during the upset phase of this process, and the material along the weld

interface would be expected receive the most forging action. Since the remaining

forged material does not remain at high temperatures for very long, it is likely that

there is a high dislocation density in this region resulting in the higher hardness.

There was no microstructural evidence that this higher hardness was due to the

formation of martensite, which would not be expected due to the relatively low

cooling rates of this process, and the low hardenability of the material being welded.

A.2.1.2 Optical Microscopy

Figures 72 and 73 reveal the typical MIAB weld structure. Bonding between solid material without evidence of entrapped liquid phase material is observed across most of the weld interface. There is also evidence of previously molten material toward the outer regions (the flash) of the weld. Microscopy provided strong

133 evidence of the requirement for proper upset pressures. As shown in Figures 74 and

75, without proper upset, the molten material is not squeezed sufficiently out of the joint. This can result in voids and a weld interface which can no longer be considered solid-state.

Since the MIAB weldments produced during this research did not utilize shielding gas, any molten material remaining in the joint would likely be highly oxidized. Such a joint would most likely suffer from a severe degradation in mechanical properties. In summary, in a proper MIAB weld, optical microscopy should reveal a solid-state weld interface free of voids with evidence that the molten material was sufficiently squeezed out of the weld region into the flash.

A.2.2 Mechanical Analysis

The combination of ID bend and tensile testing proved to be a viable method

for establishing MIAB weldment integrity. As discussed in the previous section, a

particular group of welds resulted in tensile failures through the weld interface

(Figure 78). These welds were produced with parameters that previously resulted in

excellent quality welds. More welds were then produced after the initial tensile

failures with similar results. Arc monitoring equipment was deployed which revealed

a serious controller malfunction, resulting in the delivery of insufficient current prior

to upset, also referred to as step III current. It was determined that there was an

electrical short in the controller that was later repaired and the problem resolved.

134 However, the malfunction did reveal the significance of the step III current.

The step III current is a short pulse of elevated current delivered just prior to upset.

The surge of current has the effect of rapidly increasing arc rotation speed and arc pressure (discussed later) for the purpose of expelling oxidized molten material from the weld zone prior to the forging action. This step effectively eliminates the need for shielding gas, and is critical to the MIAB welding process when shielding gas is not being used. With chromium-plated tubes, this step potentially takes on further importance and complexity due to the requirement to remove chromium from the joint. Further analysis of the step III current, and correlation of this step with weld quality and the arc monitoring plots follows later in this section.

A.2.3 L16 DOE

The initial L16 DOE was developed and conducted for the primary purposes of establishing feasibility for producing tube-to-tenon weld joints with the MIAB welding process, and to develop an understanding of the individual as well as interactive parameter effects. As discussed previously, weld interface length (see

Figure 79) was chosen as the quantifiable measurement (response variable) for assessing these effects. Figures 80 and 81 graphically represent the statistical results from the DOE. The individual parameter effects on weld interface length of weld current, weld time, current prior to upset, and upset pressure are shown in Figure 80.

Not surprisingly, higher weld currents, longer weld times, and higher upset pressures all have a positive effect on weld interface length for the range of parameters chosen.

135 Higher weld currents and longer weld times produce more part heating, resulting in a

greater amount of molten and plasticized material. This in turn results in a greater

amount of material forged outward into the flash during the upset phase.

In addition, higher pressure creates greater forging forces and larger amounts

of upset material. The current prior to upset is applied for the purpose of creating the

cleaning action (rapid expulsion) of oxidized molten metal, and was shown to have

minimal effect on the weld interface length. However, as mentioned, the cleaning

action step is a critical part of the MIAB welding process when shielding gas is not

being used, and is discussed in more detail later in this section.

More interesting, and potentially more significant, is the information which

can be derived from the parameter interaction plots of Figure 81. These plots give an indication of how the various parameters studied interact with each other. For

example, the plot of Weld Time vs. Weld Current discloses that the positive effect of

weld time on bond length is more pronounced when the weld current is lower. This

relationship reveals important aspects of the MIAB welding process, namely heat

flow and heat balance. Higher currents for a given time produce more intense heating

(P = VI) at the surfaces, and therefore, more melting. Figure 82 [22], while not a true

representation of the heating and melting processes occurring during the MIAB

welding process, does reveal the linear relationship between GMAW electrode

136 Melting Rate

Figure 82 – Linear Relationship of Melt Rate vs. Current for GMAW Process [22]

melting rate and current, and provides some indication of the anticipated effect of current on MIAB weld melt rate. It should be pointed out that the linear part of this plot represents the arc heating effect of most importance to MIAB welding, while the curved portion comes from the resistive heating effect due to electrode extension in

GMAW, not relevant for the MIAB discussion. In summary, higher currents at a given time tend to produce more melting at the faying surfaces. Subsequent analysis of the arc monitoring voltage plots showed that larger amounts of molten material produce arc instability, and also result in molten material dropping out of the joint due to the effects of gravity.

Lower currents and longer times tend to result in a thinner layer of molten material at the tube and tenon ends, and more extensive heating into the parts. As discussed previously in the Technical Review section, proper heat flow in the MIAB

137 weld process provides for sufficient plasticizing (or yield strength reduction) of material adjacent to the melt layer without producing excessive melting. Upon upset, the plasticized material will form the solid-state region at the weld interface. This effect explains the relationship of longer bond lengths with longer weld times being more pronounced at lower relative currents, as indicated in the Weld Time vs. Weld

Current on the interactive L16 plot of Figure 81.

A.3 Arc Monitoring Voltage Plots

One plot is shown for each 12 of the conditions in the L12 DOE. Refer to

Table 3 for the details of each condition.

Figure 83 – L12 Condition #1

138

Figure 84 – L12 Condition #2

Figure 85 – L12 Condition #3

139

Figure 86 – L12 Condition #4

Figure 87 – L12 Condition #5

140

Figure 88 – L12 Condition #6

Figure 89 – L12 Condition #7

141

Figure 90 – L12 Condition #8

Figure 91 – L12 Condition #9

142

Figure 92 – L12 Condition #9

Figure 93 – L12 Condition #11

143

Figure 94 – L12 Condition #12

144 A.4 40 mm Chrome-Plated Component Preliminary Development Raw Data

Table 4 below represents a portion of the 40 mm chromium-plated component preliminary development raw data. The preliminary development work identified the technical challenges associated with MIAB welding chrome-plated components, and provided future guidance regarding the effects of various MIAB weld variables. This information was subsequently used to develop the L12 arc monitored DOE which was the primary component of this research. In the raw data spreadsheet of Table 4, t3 represents arc heating (level II) time and Step 3 represents level III (current).

The gap measurement is shown under the mm column, but the technique used to measure these gaps was slightly different than what was used during the L12 experiment, so the values cannot be compared directly. Under the tulip test column, a

NOK or nok means that the Tulip Test or ID bend test resulted in visible cracking and ok means no cracking was observed. If the column is blank it means cracking was observed. Also, t1 is a preset time on the controller, t2 is the arc initiation time, Step

1 is arc initiation current and Step 2 is arc heating current. Pressure is upset pressure measured in bars.

145 Welding parameters Step Step Step 2 Gap (mm) tulip 1 3 test t1 t2 t3 t4 pre colla curre curren curre result ssu pse recoiled mm nt t nt No re d 1 1.5 0.8 1.7 0.1 350 320 490 2

#3, 4,5 1.5 1.7 3.3 0.21 270 190 630 1.5 NOK #- 6- 10 1.7 3.3 0.26 1.5 NOK #1 1 1.5 1.7 3.5 0.21 1.5 NOK

#1 1.5 1.7 3.5 0.21 270 190 630 55.4 56.79 1.39 nok #2 55.8 56.8 1 nok 55.4 #3 5 56.73 1.28 nok 55.2 #4 5 56.72 1.47 nok 55.5 #5 5 56.87 1.32 nok 55.3 #6 3.9 5 56.85 1.5 nok 55.4 #1 1.5 1.7 3.9 0.21 270 200 640 3 56.96 1.53 54.3 #2 220 630 5 55.7 1.35 #3 250 240 55.6 56.8 1.2 #4 225 55 56.76 1.76 55.5 #5 250 5 56.85 1.3 #6 55.5 56.7 1.2 0 #1

#2 55.3 57 1.7 #3 3.3 55.3 57 1.7 ok #4 260 55.5 56.98 1.48 ok #5 3 55.5 57 1.5 ok #6 1.5 2.7 55.3 57.1 1.8

7 55.6 57 1.4 nok 8 54.9 57.2 2.3 nok 9 55.1 57 1.9 nok 10 0.31 240 55 57 2 11 55.4 57.02 1.62 nok

146 12 54.9 57.1 2.2 nok 13 nok 14 3 260 400 55.3 57.02 1.72 nok 55.4 15 660 5 56.95 1.5 nok 16 55.3 #1 3.3 0.21 260 630 5 56.87 1.52 ok 55.3 #2 7 56.88 1.51 ok #3 55.2 56.88 1.68 ok 55.4 #4 3.2 3 56.93 1.5 ok 55.4 #5 3 6 56.93 1.47 nok #6 3.3 0 0 55.5 #1 1.5 1.7 3.3 0.21 250 247 630 6 56.96 1.4 nok 55.5 #2 8 57.03 1.45 ok 55.4 #3 250 3 56.88 1.45 55.4 #4 250 6 56.93 1.47

Welding parameters Step Step tulip Step 2 1 3 test t1 t2 t3 t4 pre result curre curren curre ssu Start recoiled mm nt t nt No re #5 1.5 1.7 3.3 0.21 250 240 630 #6 #7 #8 0.15 0 55.5 1 0.21 5 56.77 1.22 nok 55.5 2 3 56.69 1.16 ok 55.5 3 235 3 56.7 1.17 nok 4 55.5 56.66 1.16 nok 3.3 55.5 5 230 235 580 bar 7 56.75 1.18 55.5 6 245 2 56.74 1.22 7 230 2.8 55.4 56.68 1.21

147 7 55.5 8 4 56.68 1.14

9 0 55.6 10 1.5 1.7 3.3 0.21 250 235 580 2.6 4 56.68 1.04

55.8 11 7 56.65 0.78 nok 55.7 12 3.5 250 215 1 56.63 0.92 ok 55.7 13 6 56.67 0.91 55.6 14 630 5 56.69 1.04 nok 55.6 15 650 6 56.55 0.89 nok 55.7 16 5 56.68 0.93 nok 17 2.8 0 55.6 18 6 56.63 0.97 nok 19 615 55.7 56.73 1.03 nok 55.5 20 3.3 0.21 260 630 2.6 2 56.75 1.23 ok 21 ok 55.8 22 2.5 300 2 56.78 0.96 ok 55.7 23 8 56.75 0.97 nok 55.7 24 4.1 233 7 56.71 0.94 ok 55.4 25 4.1 4 56.71 1.27 ok 55.5 26 1 56.73 1.22 55.4 27 4 56.65 1.21 55.7 1 3.3 0.21 260 630 3 5 56.76 1.01 ok 55.7 2 3.3 7 56.7 0.93 ok 55.7 3 3.3 4 56.72 0.98 ok 55.7 4 3.6 3 56.74 1.01 ok 55.8 5 3 1 56.88 1.07 6 3 55.8 56.67 0.82

148 5 55.9 7 250 3.3 1 56.6 0.69 nok 55.7 8 9 56.75 0.96 nok 55.7 9 750 9 56.84 1.05 ok 55.7 10 750 2 56.77 1.05 nok 55.8 11 0.18 250 825 3 56.91 1.08 ok 55.7 12 7 56.72 1.08 ok 55.9 13 240 1 56.92 0.81 ok 55.7 14 3 56.69 0.96 ok 55.8 15 230 4 55.9 0.06 ok 55.7 16 8 56.73 0.95 ok 1 1.5 1.5 3.3 0.18 350 320 825 0 ok 2 1.5 1.5 3.3 0.18 350 320 825 0 nok

55.5 1 1.5 1.7 3 0.12 250 260 900 1.8 5 56.25 0.7 nok

55.3 2 1.5 1.7 1.7 0.12 250 320 900 6 56.3 0.94

55.3 3 1.5 1.7 1.7 0.12 250 320 900 1.8 6 56.33 0.97

55.3 4 1.5 1.7 1.5 0.12 250 375 900 1.8 5 56.23 0.88

55.3 5 1.5 1.7 3.5 0.12 250 220 900 1.8 2 56.25 0.93 55.7 6 250 225 700 2 56.46 0.74 ok 7 2.5 275 55.9 56.65 0.75

Table 4 – Portion of the 40 mm Preliminary Development Raw Data

149