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CHEMISTRY ASSIGNMENT CLASS VII CHAP 3, Part – II Elements , Compounds and Mixture ( Separation Techniques of Mixtures )
CHEMISTRY ASSIGNMENT CLASS VII CHAP 3, Part – II Elements , compounds and Mixture ( Separation Techniques of Mixtures ) Mixture can be separated into its constituent by various method. Seperation technique totally depend upon the nature of the constituent. Q1. Describe a method to separate solid to solid mixture . Ans . We can separate solid to solid mixture by using Solvent Method , when one of the component is soluble. In this method we use a appropriate solvent to dissolve one of the component of the mixture .After that we filter the solute .The soluble solute get filtered from the insoluble solid. The filtered solution can be further separated from the solvent by heating or keeping in the sun.In this way we can separate out the two mixture. Q2. Differentiate between Solute and Solvent. Ans Solute Solvent The solid that is dissolved or spread evenly in the The liquid in which solute is dissolved is called solvent is called Solute . solvent. e.g. In sugar syrup sugar is the solute. e.g. In sugar syrup water is the solvent Q3. Name the various method used to separate solid to liquid mixture. Ans. The solid to liquid mixtures can be separated by various method – i. Evaporation ii. Filtration iii. Distillation Q4. What do you mean by filtration ? Draw a well labelled diagram to show filtration. Give one example too. Ans. Filtration is the simplest method to separate mixture when it contain one insoluble solid component and a liquid component by using a filter paper. The clear liquid that passes through the filterpaper is called Filtrate . -
Experiment 2 — Distillation and Gas Chromatography
Chem 21 Fall 2009 Experiment 2 — Distillation and Gas Chromatography _____________________________________________________________________________ Pre-lab preparation (1) Read the supplemental material on distillation theory and techniques from Zubrick, The Organic Chem Lab Survival Manual, and the section on Gas Chromatography from Fessenden, Fessenden, and Feist, Organic Laboratory Techniques, then read this handout carefully. (2) In your notebook, write a short paragraph summarizing what you will be doing in this experiment and what you hope to learn about the efficiencies of the distillation techniques. (3) Sketch the apparatus for the simple and fractional distillations. Your set-up will look much like that shown on p 198 of Zubrick, except that yours will have a simple drip tip in place of the more standard vacuum adaptor. (4) Look up the structures and relevant physical data for the two compounds you will be using. What data are relevant? Read the procedure, think about the data analysis, and decide what you need. (5) Since you have the necessary data, calculate the log of the volatility factor (log α) that you will need for the theoretical plate calculation. Distillation has been used since antiquity to separate the components of mixtures. In one form or another, distillation is used in the manufacture of perfumes, flavorings, liquors, and a variety of other organic chemicals. One of its most important modern applications is in refining crude oil to make fuels, lubricants, and other petrochemicals. The first step in the refining process is separation of crude petroleum into various hydrocarbon fractions by distillation through huge fractionating columns, called distillation towers, that are hundreds of feet high. -
The U.S. Wine Industry and Selected Trade Issues with the European Union
The U.S. Wine Industry and Selected Trade Issues with the European Union Renée Johnson Specialist in Agricultural Policy July 25, 2016 Congressional Research Service 7-5700 www.crs.gov R43658 The U.S. Wine Industry and Selected Trade Issues with the European Union Overview This report provides an overview of issues pertaining to the U.S. wine industry within ongoing U.S. trade negotiations in the proposed Trans-Pacific Partnership (TPP) and the proposed Transatlantic Trade and Investment Partnership (T-TIP). The report is organized in two parts. The first part provides an overview of global wine production and trade, focusing on the role of the United States within the industry. The second part provides an overview of reported barriers to trade for U.S. wine exporters, and describes some of the issues that are reportedly being discussed as part of the ongoing TPP and T-TIP negotiations that could influence market access, regulations, and rules related to wine trade. Given the magnitude of wine trade between the United States and the European Union (EU), much of the discussion in this report focuses on U.S. wine trade issues related to the EU. A few introductory comments are worth noting. There is some disagreement among countries over what constitutes “wine.” For example, the EU defines wine as only those beverages made by fermenting grapes. In the United States, wine is defined more broadly to include beverages produced by fermentation of any fruit (grapes, peaches, pears, etc.). European table wine generally contains between 9% and 15% alcohol. In contrast, U.S. -
Heterogeneous Azeotropic Distillation
PROSIMPLUS APPLICATION EXAMPLE HETEROGENEOUS AZEOTROPIC DISTILLATION EXAMPLE PURPOSE This example illustrates a high purity separation process of an azeotropic mixture (ethanol-water) through heterogeneous azeotropic distillation. This process includes distillation columns. Additionally these rigorous multi- stage separation modules are part of a recycling stream, demonstrating the efficiency of ProSimPlus convergence methods. Specifications are set on output streams in order to insure the required purity. This example illustrates the way to set "non-standard" specifications in the multi-stage separation modules. Three phase calculations (vapor-liquid- liquid) are done with the taken into account of possible liquid phase splitting. ACCESS Free-Internet Restricted to ProSim clients Restricted Confidential CORRESPONDING PROSIMPLUS FILE PSPS_EX_EN-Heterogeneous-Azeotropic-Distillation.pmp3 . Reader is reminded that this use case is only an example and should not be used for other purposes. Although this example is based on actual case it may not be considered as typical nor are the data used always the most accurate available. ProSim shall have no responsibility or liability for damages arising out of or related to the use of the results of calculations based on this example. Copyright © 2009 ProSim, Labège, France - All rights reserved www.prosim.net Heterogeneous azeotropic distillation Version: March, 2009 Page: 2 / 12 TABLE OF CONTENTS 1. PROCESS MODELING 3 1.1. Process description 3 1.2. Process flowsheet 5 1.3. Specifications 6 1.4. Components 6 1.5. Thermodynamic model 7 1.6. Operating conditions 7 1.7. "Hints and Tips" 9 2. RESULTS 9 2.1. Comments on results 9 2.2. Mass and energy balances 10 2.3. -
Drinking Water Treatment: Distillation Bruce I
® ® University of Nebraska–Lincoln Extension, Institute of Agriculture and Natural Resources Know how. Know now. G1493 (Revised December 2013) Drinking Water Treatment: Distillation Bruce I. Dvorak, Extension Environmental Engineering Specialist Sharon O. Skipton, Extension Water Quality Educator water as it is boiled in the distiller. Such compounds will not Homeowners are increasingly concerned about be completely removed unless another process is used prior contaminants in their water supply that may affect to condensation. See the section in this NebGuide on treat- health or cause taste, odor, or nuisance problems. Dis- ment principles for further discussion of ways distillers may tillation, one of the oldest methods of water treatment, remove VOCs. is an effective method for reducing many impurities The boiling process during distillation generally inacti- found in water. This NebGuide discusses the process vates microorganisms. However, if the distiller is idle for an and related equipment used for household drinking extended period, bacteria can be reintroduced from the outlet water treatment by distillation. spigot and may recontaminate the water. Water Testing Contaminants Removed from Water by Distillation Regardless of which water treatment system is con- Distillation can remove nearly all impurities from sidered, the water first should be tested to determine what water. Compounds removed include sodium, hardness substances are present. Public water systems routinely test compounds such as calcium and magnesium, other dis- for contaminants. Water utilities are required to publish solved solids (including iron and manganese), fluoride, Consumer Confidence Reports (CCRs), which inform con- and nitrate. Operated properly, it effectively inactivates sumers on the source of the water, contaminants present, microorganisms such as bacteria, viruses, and protozoan potential health effects of those contaminants, and methods cysts (though protozoan cysts are not likely to be found in of treatment used by the utility. -
It's Just a Phase!
Bay Area Scientists in School Presentation Plan Lesson Name It’s just a phase!______________ Presenter(s) Kevin Metcalf, David Ojala, Melanie Drake, Carly Anderson, Hilda Buss, Lin Louie, Chris Jakobson California Standards Connection(s): 3rd Grade – Physical Science 3-PS-Matter has three states which can change when energy is added or removed. Next Generation Science Standards: 2nd Grade – Physical Science 2-PS1-1. Plan and conduct an investigation to describe and classify different kinds of materials by their observable properties. 2-PS1-4. Construct an argument with evidence that some changes caused by heating or cooling can be reversed and some cannot. Science & Engineering Practices Disciplinary Core Ideas Crosscutting Concepts Planning and carrying out PS1.A: Structure and Properties Patterns investigations to answer of Matter ・Patterns in the natural and questions or test solutions to ・Different kinds of matter exist human designed world can be problems in K–2 builds on prior and many of them can be observed. (2-PS1-1) experiences and progresses to either solid or liquid, simple investigations, based on depending on temperature. Cause and Effect fair tests, which provide data to Matter can be described and ・Events have causes that support explanations or design classified by its observable generate observable patterns. solutions. properties. (2-PS1-1) (2-PS1-4) ・Plan and conduct an ・Different properties are suited ・Simple tests can be designed to investigation collaboratively to to different purposes. (2-PS1- gather evidence to support or produce data to serve as the 2), (2-PS1-3) refute student ideas about basis for evidence to answer a ・A great variety of objects can causes. -
Distillation1
Distillation1 Distillation is a commonly used method for purifying liquids and separating mixtures of liquids into their individual components. Familiar examples include the distillation of crude fermentation broths into alcoholic spirits such as gin and vodka, and the fractionation of crude oil into useful products such as gasoline and heating oil. In the organic lab, distillation is used for purifying solvents and liquid reaction products. In analyzing a distillation, how do we know the real composition of each collected component? In this lab, we will introduce gas chromatography (GC), which will tell us how pure each fraction we collected is. After the distillation of your unknown is complete, you will analyze both components via GC. See page 11 and 12 for a light discussion on GC. To understand distillation, first consider what happens upon heating a liquid. At any temperature, some molecules of a liquid possess enough kinetic energy to escape into the vapor phase (evaporation) and some of the molecules in the vapor phase return to the liquid (condensation). An equilibrium is set up, with molecules going back and forth between liquid and vapor. At higher temperatures, more molecules possess enough kinetic energy to escape, which results in a greater number of molecules being present in the vapor phase. If the liquid is placed into a closed container with a pressure gauge attached, one can obtain a quantitative measure of the degree of vaporization. This pressure is defined as the vapor pressure of the compound, which can be measured at different temperatures. Consider heating cyclohexane, a liquid hydrocarbon, and measuring its vapor pressure at different temperatures. -
Simulation of the Open Sky Seawater Distillation
Green and Sustainable Chemistry, 2013, 3, 68-88 http://dx.doi.org/10.4236/gsc.2013.32012 Published Online May 2013 (http://www.scirp.org/journal/gsc) The Best Available Technology of Water/Wastewater Treatment and Seawater Desalination: Simulation of the Open Sky Seawater Distillation Djamel Ghernaout Chemical Engineering Department, Saad Dahlab University of Blida, Blida, Algeria Email: [email protected] Received March 16, 2013; revised April 18, 2013; accepted April 26, 2013 Copyright © 2013 Djamel Ghernaout. This is an open access article distributed under the Creative Commons Attribution License, which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited. ABSTRACT This review suggests the concept of the best available technology of water/wastewater treatment and seawater desalina- tion which is in fact a simulation of the seawater distillation at the open sky: coagulation in salty water aerated basin/ coagulation using seawater as coagulant solution with distillation using stored solar energy followed by waterfall on a natural mountain. This natural, green, and technico-economical technology is composed of three steps: the first one is coagulation which may be achieved: 1) in salty water aerated basin (air stripping, AS; dissolved air flotation, DAF) where the raw water is “diluted” in seawater; or 2) in “conventional” coagulation using seawater as coagulant solution instead of alum/ferric salts. The first option seems to be more natural as it simulates river water dilution in seawater and the second one is more practical for “rapid” water consummation. For colloids and microorganisms’ removal, double- layer compression and charge neutralisation, as main coagulation and disinfection mechanisms, would be involved in the first and second options, respectively. -
877•279•2655 | [email protected] | 841 Latour Court, Suite A, Napa California 94558
TASTING NOTES Happy aromas of yellow apple, white peach and a lingering taste of meyer lemon. GUILT FREE! Perfect for those watching their calories, SERVING FACTS sugar or alcohol for any reason at all. VINEYARD SOURCES Artificial Color, Sweeteners, Gum Arabic or DMDC NO ADDED: VEGAN FRIENDLY 93% Chardonnay GLUTEN FREE Lodi AVA Only Natural The 70% of the fruit that comes from Lodi is No Artificial Ingredients! located at the northern edge of the San Joaquin Additions! Valley, east of San Francisco Bay. Lodi enjoys a similar climate and growing conditions to its WINEMAKING coastal neighbors Napa and Sonoma. The two ■ Champagne Press Cycle ■ 40% of volume dealcoholized via major rivers originating in the Sierra Nevada (Whole cluster) Spinning Cone Column Tech to 4% ABV, mountain range that feeds the Lodi appellation have brought soils rich in granitic-based minerals ■ Hyper OX blended back to create final 9.3% ABV that lend complex flavors to the wines of Lodi. ■ Clean Racking (under 50 NTU) ■ No residual sugar ■ Cold Fermentation at 59ºF 7% Sauvignon Blanc Clarksburg AVA, California We use a champagne press cycle to lower the phenolic content of our wine. The chardonnay goes through both primary and secondary fermentation to increase the richness and viscosity, An introduction of high quality Sauvignon Blanc while the Sauvignon Blanc fruit only goes through primary fermentation in order to maintain its acid and aromatic complexity. Both lots are combined 3 months before bottling and are fruit into the blend brings aromatic complexity cross-flow filtered. No chemical additives or adjustments are made except for the addition of and a re-balance of acidity. -
It's Only Natural: the 31 Wines You Need To
NATURAL WINE It’s only natural: And the winner is… La Stoppa, Ageno, Emilia, the 31 wines Emilia-Romagna, Italy 2011 94 Simon Woolf 95 Andrew Jefford 95 Sarah Jane Evans MW 92 £24.10-£28 Exel, Hay Wines, Les Caves de Pyrene, Ottolenghi, Vini Italiani Who would have thought that a defiantly tannic orange wine made you need to try with 30 days of maceration would triumph in this tasting? Yet triumph it did, proving that Malvasia di Candia Aromatica (the 94 In a comprehensive and landmark tasting, Decanter’s expert panel blind ❦POINTS tasted 122 natural wines from all corners of the globe. Here they name dominant variety here) takes to skin contact like bees to a their top wine as well as 10 personal favourites, after Simon Woolf honeypot. La Stoppa’s 50-hectare organic estate in Emilia-Romagna has explains how we define this niche but exciting wine category been established for more than a century, with the enigmatic Elena Pantaleoni its grande dame for the past 23 years. She prefers the term ‘artisanal’ to the more nebulous ‘natural’ for her wines. THE TIme FOR denial or protest is over it, partly in an attempt to limit the growing network of fairs, merchants, – we can safely retire that old adverse effects of their sometimes wine bars and sommeliers who on Simon Woolf A full-bodied, spicy and honeyed wine with camomile and thyme chestnut, ‘there’s no such thing as over-enthusiastic levels of consumption. occasion display a semi-religious zeal. notes leading to a thrilling palate with serious grip. -
CHEM 344 Distillation of Liquid Mixtures
CHEM 344 Distillation of liquid mixtures 1. Distillation basics The vaporization of a liquid and condensation of the resulting vapor is the basis of distillation. Organic liquids containing small amounts (<15%) of impurities or non-volatile substances are easily purified by simple distillation, as are liquid mixtures where the difference in boiling point of the components is >70 oC. Fractional distillation is more useful for separating mixtures of liquids where the boiling points of the components differ by <70 oC (see later). A typical simple distillation setup is shown in Figure 1. It consists of a flask containing the liquid to be distilled, an adapter to hold a thermometer and to connect the flask to a water-cooled condenser, and a flask to hold the condensed liquid (the distillate). Figure 1: Apparatus for a simple distillation. 1.1 The distillation flask The distillation flask is a round-bottom flask. The liquid to be distilled should fill the distillation flask to ~50-60% of its capacity. To promote even heating of the liquid, a boiling chip or a magnetic stir bar is added before heat is applied to the distillation flask. The irregular chips provide sites for bubbles of vapor to form, or alternatively the liquid is agitated with the magnetic stirrer as it is being heated. Never add a boiling chip or a stir bar to a hot liquid! Doing so can cause a seemingly calm liquid to boil suddenly and violently. 1 1.2 The distilling adapter The adapter connects the distillation flask, the condenser, and the thermometer. This type of adapter is often referred to as a distillation head. -
Enrichment of Natural Products Using an Integrated Solvent-Free Process: Molecular Distillation
BK1064-ch62_R2_250706 SYMPOSIUM SERIES NO. 152 # 2006 IChemE ENRICHMENT OF NATURAL PRODUCTS USING AN INTEGRATED SOLVENT-FREE PROCESS: MOLECULAR DISTILLATION Fregolente, L.V.; Moraes, E.B.; Martins, P.F.; Batistella, C.B.; Wolf Maciel, M.R.; Afonso, A.P.; Reis, M.H.M. Chemical Engineering School/Separation Process Development Laboratory (LDPS) State University of Campinas – CP 6066 – CEP 13081-970 – Campinas – SP – Brazil E-mail: [email protected] Molecular distillation is a potential process for separation, purification and/or concentration of natural products, usually constituted by complex and thermally sen- sitive molecules, such as vitamins. Furthermore, this process has advantages over other techniques that use solvents as the separating agent, avoiding problems of toxi- city. This process is characterized by short exposure of the distilled liquid to high temperatures, by high vacuum (around 1024 mmHg) in the distillation space and by a small distance between the evaporator and the condenser (around 2 cm). The pro- ductivity of the process is high, considering the concentration of high added value compounds. In this work, the molecular distillation process was applied to enrich borage oil in gamma-linolenic acid (GLA) and also to recover tocopherols from deo- dorizer distillate of soybean oil (DDSO), since these are components of interest for food and pharmaceutical industries. KEYWORDS: gamma-linolenic acid, vitamin E, molecular distillation, deodorizer distillate of soybean oil, borrage oil INTRODUCTION Molecular distillation shows potential in the separation, purification and/or concentration of natural products, usually constituted by complex and thermally sensitive molecules, such as vitamins and polyunsaturated fatty acids, because it can minimize losses by thermal decomposition.