S. Muthukumaran et al., International Journal of Advanced Engineering Technology E-ISSN 0976-3945

Research Paper INVESTIGATIONS ON MAGNETIC PULSE BASED OF TWO DISSIMILAR FERROUS AND NON FERROUS MATERIALS IN VARIOUS COMBINATIONS S. Muthukumaran1,*, A. Senthil Kumar1, S.Kudiyarasan2, S. Arungalai Vendan3

Address for Correspondence 1Department of Mechanical Engineering, University College of Engineering, Panruti campus, Panruti 2Technical Group, IGCAR, Kalpakkam. 3Industrial Automation and Instrumentation Division, School of Electrical Engineering, VIT University, Vellore, India. ABSTRACT In this paper the joining of dissimilar metal couple Al-Cu was studied. Commonly, MPW is considered as a non-melting process. Magnetic pulse (MPW) is a joining process in which lap joint surfaces of cylindrical shape metals, such as pipes and tubes, are welded by impact, using electromagnetic forces. MPW is classed in the group of solid-state bonding processes together with explosive welding (EXW). The technique has become an accepted welding process because it enables to join similar, as well as dissimilar metals, which is very difficult to weld by conventional techniques such as GTAW or EBW due differences in melting points. MPW process is very fast, produces no heat affected zone (HAZ) and may be performed without filler metals and protective gases. Nevertheless, it was detected a very thin film (10 to 40 µm) of two welded metals in the form of intermetallic phases, in which melting and solidification processes took place. These inter- metallic phases significantly affect the mechanical properties of the joint. The interface presents a typical wavy pattern and mutual diffusion of elements happens in the zone. The transition zone is composed of elements intermetallic, micro cracks and micro pores. The effect of the main process parameters on the morphology and structure of the interface has been investigated. The weld interface composition, structure and morphology were studied by optical and scanning electron microscopy (SEM). Energy-dispersive spectrometry (EDS) was used in order to evaluate the local distribution of alloying elements at the joint interface and its vicinity and also Nano-hardness tests were performed across the bonding zone at regular increments. The results of joints characterization allowed determining the optimal MPW process parameters. KEYWORDS: MPW, Al, Cu, Magnetic flux, welding. INTRODUCTION When a high magnetic field B is suddenly generated The Magnetic Pulse Welding (MPW) is solid-state and penetrated into metal, then the eddy currents joining process employed for similar and dissimilar (current density I pass through them and as a result, conductive metals viz., aluminum, brass, or copper to an electromagnetic force of F = I × B acts mainly on steel, titanium, stainless, aluminum, magnesium the base metal and it is accelerated away from the copper and most other metals. MPW system coil and collides rapidly with the target metal. The comprises a power supply, bank of capacitors, a high- eddy current I and the magnetic pressure p are given speed switching system and a coil (Fig.1). The parts as following: to be joined are inserted into the coil. The capacitor bank is charged and the high-speed switch is activated. A strong magnetic flux is created around the coil when the current is applied and as a result eddy currents are formed in the parts. The eddy currents oppose the magnetic field in the coil and an opposing force is generated1. This force drives the materials together at a tremendous high rate of speed and creates weld (see Fig 2). Where K, µ, τ, Bo and Bi are the electrical conductivity, magnetic permeability, thickness, the magnetic flux density at lower and upper surfaces of Al, respectively. The depth of skin effect (δ) can be obtained by calculation of angular frequency (ω) and it is governed by the complete MPW system’s inductivity L and its capacity C. The skin depth becomes important parameter especially for thin metal bonding process. When the thickness of the base metal is the same as the skin depth, then magnetic pressure equals 86% of its maximum value and it reaches 98% when the base metal thickness is

Fig. 1-Magnetic Pulse Set Up twice of the skin depth. The appropriate skin depth with capacitor bank. and higher magnetic pressure can be adjusted by the frequency of the discharge current2. At the moment of collision the colliding surfaces can be cleaned by a large kinetic energy getting before the collision. The velocities attained during this process range from 200 m/s to 500 m/s and the joining process completed within microsecond. Because of the short impact period, the extent of heating might be minimal along the joints3. Therefore, comparing to the traditional fusion

Fig. 2-MPW Principle welding process, no significant heat affected zones is

Int J Adv Engg Tech/Vol. VII/Issue II/April-June,2016/613-616 S. Muthukumaran et al., International Journal of Advanced Engineering Technology E-ISSN 0976-3945 produced in MPW joints and it can be noticed as a II. RESULTS AND DISCUSSION main advantage. The welded specimens are subjected to destructive The practical limitations of MPW relate to handling and non-destructive tests to evaluate its quality and very high electrical currents. The major limitation of strength. Metallurgical characterizations are MPW equipment concerns the electrical connections performed to analyze the bond integrity and between capacitors, switch, and coil. Very large examined for presences of inter-metallic phases8,9. metal components cannot be formed due to problems III. a. TENSILE TEST in design of very large coils4. It is expensive Welded samples are tested on a standard tensile equipment, just if able only by important mass testing machine. In all cases, failure occurred in the production5. region away from the weld area Fig.4(a) . The tensile The experimental results and welding characteristics results emphasizes that ductile failure of a welded Al- for several samples such as Al-Al and Al-Fe are Cu Rod/Pipe occurs at a distant from the weld. There reported in the available literatures. However, Al-Cu is no failure on the weld interface10 Fig.4(b). Table 1 tubular combination which has greater demand in presents the tensile test results. nuclear industries has been less reported with respect to MPW process. Moreover, the metallurgical characterization and non-destructive tests on MPW specimens in the available literatures are scanty. Hence, in this study, an attempt is being made to Al- Cu tubular components using MPW process. Further, Fig. 4 (a) -Specimens after Tensile test mechanical testing and metallurgical Table1-Tensile test results of MPW joining dissimilar materials characterizations are being carried out6. S.no Specimen Tensile Strength in I. EXPERIMENTAL PRIOR AND Description kN PROCEDURES 1 Al - Cu 11.050 The three trails are employed in this study. However a typical one specimen consist Cu (Driver) and Al (Flyer). The MPW equipment that is used in this study has a maximum charging energy of 10 kJ, Current of 12 kA and a Voltage of 10 kV. An outer Cu pipe was machined to be 2 mm thick, 80 mm long, and 40 mm in diameter. For the pipe joint, the gap between the Cu and Al was 1mm. The specimens are ground using emery paper to remove marks sustained during . First, the voltage had to be charged according to the welding conditions. Then welding is carried out by electromagnetic force from discharged current through a working coil which develops a repulsive force between the induced Fig. 4 (b) - Al-Cu Tensile test graph currents flowing parallel and in the opposite direction III. b. METALLOGRAPHY TEST in the tube7. Fig 3 shows few typical samples For all the three welded samples, the optical dimensional diagram, specimens after weld and cut microscopic examination was done and the results cross section and inner weld view respectively. observed were as expected in all the aspects of It may be observed that there is a reduction in perfections and integrity. First trail (Al-Cu), that was diameter in the area of the weld8. After welding, the examined under optical microscope after etching and work pieces are cross sectioned and prepared for polishing then the bonding of two materials were examination by standard metallographic procedures verified with magnification ranging from 10X to such as mechanical polishing down to 1-micrometer 100X and observed that there is no imperfections and grit and light chemical etching. The samples were defects noticed and integrity of both the materials is then examined by optical and scanning electron intact11. microscopy. Microanalysis by wavelength dispersive III. c. MICRO-STRUCTURAL ANALYSIS spectroscopy was utilized to evaluate the local Microstructures of cross sections of the different distribution of alloying elements at the joint and its configurations of dissimilar welds are presented in vicinity. Fig. 5. There is a prominent difference in the quality of welding particularly for these configurations, and in general there is no bonding or minimal bonding in the corners and start-end zones; however the center of the welds showed a exemplary bonding or bond integrity. This may be regarded as the important feature or even the very unique feature of this type of welding. The inadequacy in bonding at the corners of the weld zone is a typical feature of MPW cylindrical parts and according to literature is not critical for many applications12,13. The minimally bonded corners of the weld specimen however pose undesirability and less adaptive in corrosive environments and in Fig. 3-MPW Specimen dimensional diagram with Cut the case of recurrent cycled loads shown in fig. (5). Cross Section and inner weld view Int J Adv Engg Tech/Vol. VII/Issue II/April-June,2016/613-616 S. Muthukumaran et al., International Journal of Advanced Engineering Technology E-ISSN 0976-3945

Fig 6 (b) -Sum Spectra view of Proportionate quantity of metals in the welded portion Fig. 5 - Cu-Al specimen viewed under the optic microscope. IV. e. NANO INDENTATION The wave pattern by the side of the interface For MPW joint at the discharge voltage of 10kV, the significantly depends on sample geometry and to a nano indentation test was carried out to measure the negligible degree on the process parameters. micro hardness across the transition zone by using Substantial utility of dissimilar specimen cylinders Nano Indenters XP equipment. Five points near the and relatively low pulse energies inhibited the wave interfaces on both basic metals and one point on the formation. Contrary, applying hollow dissimilar transition zone were chosen for the test. combines’ cylinders and high pulse energies The magnitude and the distribution of the micro pronounced waves are visible, especially in the hardness are given in Fig. 7 (a) & (b). It is illustrated middle section of the welds (Fig. 7). This geometrical that the hardness value in the transition zone is the influence is in accordance with findings in12. It is highest and the values decrease with increasing the imperative to note that the wave formation process is distance away from the zone or the interface. It can not mandatory for a good bonding. It is furthermore be attributable to the sharp plastic deformation along worth mentioning that to some extent wave formation the interfaces that causes the gradient of work could also be observed in regions without bonding. hardening near the interface. Circumventing the formation of intermetallic phases Both the plastic deformation and the hardness reduce at the welding interface is impossible. The extent of with increasing the distance from the interfaces. In interface depends on the process parameters and is addition, the intermediate compounds might be produced in the transition zone that is fragile and has fairly connected with the structure of the interface. 15 It is pointed out that the phase film appears to be higher hardness than the basic metals , which will be interrupted by regions without any intermetallic. For analyzed deeply. a thickness below 5 microns the intermetallic contains rarely any cracks, voids or pores. III. d. SCANNING ELECTRON MICROSCOPY (SEM) with ENERGY DISPERSIVE SPECTROSCOPY (EDS) The SEM investigations present more information on bonding and phase formations. The SEM of the Al- Cu welded specimen is shown in Fig. 6(a). It may be noted that the dearth of any diffusion layers leads to the postulation that local melting is mainly involved in the phase formation and bonding process along the interface. Fig. 7 (a) -Indentation Hardness of Al/Cu As for low pulse energies the intermetallic phases consist primarily of aluminum, it is deduced that solely aluminum but not copper was molten during low energy MPW. Al-rich phases are formed under strong non equilibrium conditions. From the sharp and stepwise transition in chemical composition between the two parent metals and the formed intermetallic phases it is in accordance with Carpenter and Wittman14 who deduced that solid state diffusion is not involved as active bonding mechanism in the process of MPW aluminum to copper.

Fig. 7 (b) - Indentation Modulus of Al/Cu III. RELIABILITY ANALYSIS The magnetic pulse welding (MPW) is one of the reliable methods that can be used for the dissimilar metal joints. The magnetic pulse welding (MPW) provides an excellent tool for achieving of conductive metals such as aluminum, brass, or copper to steel, titanium, stainless, aluminum, 16 magnesium copper and most other metals joints . Fig. 6(a) - SEM of the Al-Cu welded specimen The structure of an interphase region was

Int J Adv Engg Tech/Vol. VII/Issue II/April-June,2016/613-616 S. Muthukumaran et al., International Journal of Advanced Engineering Technology E-ISSN 0976-3945 investigated using a microscope and scanning Engineering, University of Basrah, Basrah, Iraq, microscope, Chemical composition was determined November 30 - December 2, 2010 [12] Tsujino,J and Ueoka, T, “Ultrasonic butt welding by a spectroscope. The magnetic pulse welding of aluminum, anticorrosive aluminum and copper (MPW) is Reliable and well suited to high-volume plate specimens,” Ultrasonics Symposium, 1988. production (MTBF typically 1-5 million welds)17. Proceedings., IEEE 1988, A247(1955), 529-551. IV. CONCLUSION [13] Haiping Yu, ZhidanXu, ZhisongFan, ZhixueZhao, ChunfengLi, Materials Science & Engineering A Magnetic Pulse Welding of three dissimilar 561 (2013) 259–265. configurations of metals is performed and a detailed [14] Yuan Zhanga, Sudarsanam Suresh Babub, Curtis comparative study between the specimens is done. Prothec, Michael Blakelyd, John Kwasegroche, Specific Observations include the dissimilar metals Mike LaHae, Glenn S. Daehna Journal of Materials Processing Technology 211 (2011) 944– generates enough heat at the interface to enhance 952. plenty of mass transfer for the precipitation of [15] YU Hai-ping1, XU Zhi-dan, JIANG Hong-wei, intermetallic phases. However, the relative amounts ZHAO Zhi-xue, LI Chun-feng, Trans. Nonferrous of these phases remained small compared to fusion Met. Soc. China 22(2012) s548−s552. [16] Ivanas VIŠNIAKAS “Reliability Estimation of the welding processes because the observed transition Austenitic Steels Welded Joints” ISSN 1392–1320 region is narrow and discontinuous. The type and Materials Science (MEDŽIAGOTYRA) 13(2007). chemical composition of the created intermetallic Department of Welding and Material Science, depend on the pulse parameters chosen. This Vilnius Gediminas Technical University, Basanavičiaus 28, LT-03324, Vilnius, Lithuania. behavior is endorsed to different temperature-time http://www.bmax.com/technology/magnetic-pulse- system of the process leading to varying amounts of welding/ melting of the two base materials. To impound detrimental effects on the mechanical properties of the joints the thickness of the formed intermetallic should not exceed few microns. Hardness of the welded specimen at the joint region is observed to be the maximum in compared to the either side of transition zones having dissimilar metals. The magnetic pulse welding (MPW) is Reliable and well suited to high-volume production. The bonding of dissimilar metals at the interphase region is appreciably high. Above a critical thickness the intermetallic are prone to cracking and spallation. ACKNOWLEDGEMENTS The authors sincerely thank SERB, Dept. of Science and Technology, India for providing the financial assistance vide order # FTYSS: SR/FTP/ETA- 0134/2011 to carry out this research and IGCAR, India for testing & analysis. REFERENCES [1] Pulsar Ltd.: Magnetic Pulse Welding Solutions, Pulsar Ltd. Raanana, Israel, 2006. http://www.pulsar.co.il/systems/?did=30 5.9.2009. [2] Glouschenkov, V.A., Grechnikov, F.V., Mayshev, B.S. Journal de Physique IV. 7 (1997), Colloque C3, Suplement of Physic Journal 111. C3-45 to C3-48. [3] Weber, Austin. The Cold Welding Process is being used for more and more high-volume applications. Assembly Magazine, (2002). [4] Aizawa, T.,Lee, Kwang-Jin, Kumai, Shinji, Arai, Takashi.. Materials Science & Engineering A, 471 (2007), 95-101. [5] Ahmad K. Jassim,R&D, “Magnetic Pulse Welding Technology”, The State Company for Iron and Steel-Ministry of Industry, Iraq J. Electrical and Electronic Engineering, 7(2011) . [6] Ben-Artzy, A.; Stern, A.; Frage, N. ; Shribman, V.; Sadot, O.. International Journal of Impact Engineering 37(2010), 397-404. [7] Raoelisona R.N., Buirona N., Rachika M., Hayeb D., Franzc G. “Efficient welding conditions in magnetic pulse welding process”, Journal of Manufacturing Processes, Volume 14, Issue 3, August 2012, Pages 372-377 [8] Masumoto I., Tamaki K. and Kojima M: Journal of the Japan Welding Society, No. 1, 49 (1980), 29. [9] Aizawa T and yoshizawa M: Proc. 7th Symposium Of Japan Welding Society, Kobe, Japan (2001), 205. [10] Matthias Van Wonterghem, Pieter Vanhulsel “Magnetic pulse crimping of mechanical joints”, Ghent, June 2011. [11] 2010, 1st International Conference on Energy, Power and Control (EPC-IQ), College of

Int J Adv Engg Tech/Vol. VII/Issue II/April-June,2016/613-616