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CENTER FOR NUCLEAR WASTE REGULATORY ANALYSES TRIP REPORT

SUBJECT: Advanced Light Source Users' Association Annual Meeting (20-5704-073)

DATE/PLACE: October 20-21, 1994 Lawrence Berkeley Laboratory Berkeley, CA

AUTHOR(S): Roberto T. Pabalan

DISTRIBUTION:

CNWRA NRC-NMSS NRC-RES SwRI

W. Patrick J. Linehan B. Morris S. Rowe (SwRJ Contracts) Directors S. Fortuna F. Costanzi Element Managers B. Stiltenpole W. Ott B. Meehan J. Randall M. Federline G. Birchard M. Bell D. Brooks P. Justus

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SUBJECT: Advanced Light Source Users' Association Annual Meeting (20-5704-073)

DATE/PLACE: October 20-21, 1994 Lawrence Berkeley Laboratory Berkeley, CA

AUTHOR(S): Roberto T. Pabalan

PERSONS PRESENT: See attendance list (Attachment 1)

BACKGROUND AND PURPOSE OF TRIP:

The purpose of the trip was to attend the Annual Meeting of the Advanced Light Source (ALS) Users' Association and to visit the ALS facility at the Lawrence Berkeley Laboratory (LBL). The ALS facility opened in the spring of 1993 and provides the world's brightest beams of ultraviolet and soft x-ray synchrotron radiation for use in a variety of fields spanning materials science to biology. Because the ALS is a DOE national user facility, it is free to industrial and academic users conducting nonproprietary research. The objective of the trip was to investigate the possible use of the ALS facility for studies related to the CNWRA Sorption Research Project.

Meeting Summary:

Presentations on the morning of the first day focused on recent highlights on the ALS facility. William Oosterhuis of the Office of Basic Energy Sciences at the U.S. Department of Energy provided an overview of government funding climate for experimental facilities and for research at synchrotron-radiation facilities. He stated that the future holds continued tight funding for basic research and increased emphasis on applied research. He encouraged participants to be aggressive in submitting proposals that respond to national needs. Brian M. Kincaid, director of the ALS, gave an overview of the ALS facility. The ALS is currently operating at 60% of the maximum operating hours (9 eight-hour shifts per week); plans to achieve 100% operation is on hold because of budgetary constraints. Fiscal year 1995 total budget is $24.4 million and requested funding for 1996 is $37.7 million, which most likely will be reduced. He acknowledged the difficult budgetary outlook and stated that he believes the key to increased funding is for the various U.S. synchrotron facilities to demonstrate to the Office of Management and Budget that there is user demand for all of the facilities, not just for the most advanced ones, and that these facilities are being fully utilized (which is true for the ALS). He also talked about the ALS program to conform with the ISO 9000 quality assurance program, which he said is important for attracting ALS users from U.S. and European industry. A. Jackson, leader of the accelerator group, discussed in some detail the performance of the accelerator and how this is measured. He indicated that 7% of available beamtime was lost during the past year and provided a causal analysis of this loss. H. Padmore, leader of the experimental systems

2 group, discussed improvements in the ALS that occurred in the past year, such as new beam lines/workstations and their applications, and changes planned during the current fiscal year.

During the rest of the meeting several speakers presented results of their work using synchrotron radiation sources, either at the ALS or at another institution. B. Tonner (Univ. of Wisconsin, Milwaukee) presented results using the ALS beamline 7.0 as applied to spectroscopic study of small samples or small areas of samples. Beamline 7.0 was designed to take advantage of the high flux and small spot size (50 microns) of the ALS light source for studies of materials by ultra-ESCA (electron spectroscopy for chemical analysis) techniques. One study he showed was the characterization of minute radioactive curium oxide. The amount of curium oxide analyzed was less than 5 ng, which had a level of radioactivity considerably lower than that of a household smoke detector. The technique provided a safer alternative to other techniques which require working with larger amounts of material and could be useful for applications such as analyzing soil from contaminated waste sites.

Joseph Nordgren (Uppsala Univ.) discussed their research in the field of resonant inelastic x-ray scattering (RIXS) spectroscopy. The technique was applied by his research team to study benzene with respect to the symmetries of its molecular orbitals.

K. Jackson (LBL) discussed potential applications of the ALS for micromachining devices that can be used as microsensors for detecting pressure, acceleration, vapors, temperature and sound. Applications could be in medicine (microsensors to measure pressure gradients at heart valves or the velocity of blood vessels), automobiles (acceleration detectors for triggering air bags or adjusting engine performance), or as "chemical plants on a chip" - tiny reaction chambers only as big as a few grains of sand built into a silicon wafer, e.g., for DNA replication. The ALS facility can provide micromachining capability through deep-etch x-ray lithography. LBL research teams are planning a deep-etch x-ray lithography facility where users can fabricate micromachines on an industrial scale.

R. Stroud (Univ. of California, San Francisco) discussed the applications of the ALS to protein x-ray crystallography, which is currently the most successful way to get structural information about complex molecules in the human body. One example he showed was their study of the ras gene, the mutation of which can result in the formation of a cancer causing ras oncogene. Proteins created by the oncogene, known as oncoproteins, lose their ability to turn off the cell division signal, a disaster that can lead to the formation of deadly tumors. The research team derived highly accurate data on the position of the atoms in the normal and mutated forms of the ras proteins and discovered how the on-off switch works and what happens when it goes awry. This understanding will allow the pharmaceutical industry to focus on designing and synthesizing therapeutic molecules to counteract the disease-causing mechanism. The potential demand for the technique is so large that ALS management is putting substantial financial and human resources into building a protein crystallography facility at LBL that will offer analytical services to industry.

Several posters were also on exhibit at the ALS facility. Two posters showed the application of the x-ray fluorescence microprobe equipment on Beamline 10.3. At present the elemental sensitivity of the microprobe reaches the femitogram (1015 g) level for elements from potassium to zinc in the periodic table. Additional detection sensitivity is imparted by the ability to select the x-ray photon energy to avoid interfering fluorescence from other elements. A major advantage of the x-ray microprobe is that specimens do not have to be kept in vacuum or subjected to special contrast-enhancing preparation. One of the two posters showed results of a study designed to determine why a previously successful fabrication process for solar cells had begun turning out non functional photovoltaic cells. The fluorescence microprobe is able to detect trace elements in a bulk sample, whereas techniques involving electron photoemission are sensitive only to the elements on the surface. This capability, along with the high sensitivity and spatial resolution of the microprobe, revealed that extremely small

3 elements on the surface. This capability, along with the high sensitivity and spatial resolution of the microprobe, revealed that extremely small quantities of iron impurities present at and below the surface were probably introduced during fabrication and led to tlte cell's failure. The other poster presented the results of x-ray microprobe analysis of sediments from the San Francisco Bay and showed the distribution of toxic metals on the sediment surface. The study attempted to correlate toxic metal distribution with sorption sites on the sediments.

I had discussions with Eric Hudson (Lawrence Livermore National Laboratory) about uranium sorption studies. He is interested in using the synchrotron source at the Stanford Synchrotron Radiation Laboratory to study uranium sorption on mineral surfaces, particularly on clinoptilolite, and in a possible collaborative work in this area. We agreed that I should do some calculations to determine if it is experimentally feasible to load clinoptilolite or some other mineral with 5,000 ppm of U and investigate the availability of beam time at Stanford.

SUMMARY OF ACTIVITIES:

See attached meeting program.

IMPRESSIONS/CONCLUSIONS:

The meeting was well-organized and provided an opportunity for researchers from different scientific disciplines to present and discuss their work using synchrotron radiation. However, the potential application of the various techniques using the ALS to studies relevant to the CNWRA sorption research is not clear at this time. The technique that has been used for sorption studies (EXAFS, or extended x-ray fine-edge structure spectroscopy) is not available at the ALS facility, but is being utilized at the Stanford facility. Further contacts with ALS investigators are needed to pursue the potential use of the facility.

PROBLEMS ENCOUNTERED:

None.

PENDING ACTIONS:

R. Pabalan will investigate the possibility of collaborating technically and programmatically with E. Hudson of LLNL in using the Stanford Synchrotron Radiation Laboratory beam source for spectroscopic studies of uranium sorption on mineral surfaces. R. Pabalan will request information from ALS investigators about potential applications to sorption studies.

RECOMMENDATIONS:

None.

ATTACHMENTS:

1. Attendance List 2. Meeting program

4 SIGNATURES:

Roberto T. Pabalan Date Senior Research Scientist

CONCURRENCE SIGNATURES AND DATE:

M cKague, M anager Date SLawrence Geologic Setting

Biidhi Sagar Date Technical Director

/ar attachments

5 ADVANCED LIGHT SOURCE USERS' ASSOCIATION ANNUAL MEETING October 20-21, 1994

PARTICIPANT AND EXHIBITOR LIST ADVANCED LIGHT SOURCE USERS' ASSOCIATION ANNUAL MEETING October 20-21, 1994

Seppo Aksela Harald Ade Helena Aksela Department of Physics Department of Physics Department of Physics University of Oulu University of Oulu North Carolina State University Finland 90570 Oulu, Finland 90570 Box 8202 Oulu, 1319 358-81-553-1327 Raleigh, NO 27695-8202 358-81-553 358-81-553 1287 358-81-553-1287 (919) 515-4554 FYS-HA@ FNOU.OULU.F1 [email protected] (919) 515-3031 harald_ade ncsu.edu

Paul Alivisatos Patrick G. Allen Ilham Al Mahamid Lab. Department of Chemistry Lawrence Livermore National Lawrence Berkeley Laboratory of California, Berkeley P. 0. Box 808, L-396 1 Cyclotron Road, 70A-1 150 University Berkeley, CA 94720 Livermore, CA 94551 Berkeley, CA 94720 (510) 422-5837 (510) 422-7630

Jesper N. Andersen Uwe Arp Rosa Alvis Radiation Res. National Inst.Standards & Tech. Advanced Light Source Dept. of Synchrotron Lund University Gaithersburg, MD 20899 Lawrence Berkeley Laboratory Institute of Physics (301) 975-3233 1 Cyclotron Road, 80-101 S61vegatan 14 (301) 975-3038 Berkeley, CA 94720 Lund, Sweden S.22362 [email protected] (510) 486-4965 46-46-107265 (510) 486-4960 46-46-1 04321 jesper.anderson 0 maxlab.lu.se Attwood Antonella Balerna Maria Carmen Asensio David Center for X-ray Optics INFN-LNF-GRUPPO PULS Inside Ciencia de Materiales,Madrid Berkeley Laboratory C.P. 13 c/Serrano 144 Lawrence I Cyclotron Road, 2-400 Frascati Madrid, Spain 28008 Berkeley, CA 94720 Rome, Italy 00044 34-1-5633389 (510) 486-4463 06-9403542 34-1-411-7651 (510) 486-4955 06-9403304 asensio 0 lure.u-psud.fr attwood @ Ibl.gov bale ma @|nf.infn.it

1 Robert A. Bartynski -i. Raul Beguiristain jl B. Bell Optics University of Oklahoma Department of Physics -Center for X-ray 650 Parrington Oval #100 Rutgers University Lawrence Berkeley Laboratory Norman, CK 73019 P. 0. Box 849 1 Cyclotron Road, 2-400 (405) 325-3521 NJ 06855 Berkeley, CA 94720 .Piscataway, (405) 325-7383 (908) 445-4839 (510) 486-4079 pbell @gslan.offsys.uoknor.edu (908) 445-4343 (510) 486-4550 [email protected] [email protected]

Jeffrey Bokor John W. Bender Nora Berrah EECS Department Albuquerque Operations Physics Department Rocketdyne, University of California, Berkeley Broadbent Parkway, NE Western Michigan University 2511 Berkeley, CA 94720 Albuquerque, NM 87107 Kalamazoo, MI 49008 (505) 345-2660 (616) 387-4955 (505) 345-2589

Reid A. Brennen John D. Bozek Sean Brennan Jet Propulsion Laboratory/LBL Berkeley Laboratory Stanford Synchtron Radiation Lab. Lawrence 1 Cyclotron Road, 2-400 1 Road, 2-400 P. 0. Box 4349, MS 69 Cyclotron Berkeley, CA 94720 CA 94720 Stanford, CA 94309 Berkeley, (510) 486-7588 (510) 486-4967 (510) 486-4550 (510) 486-7696 jdbozek@IbLgov

Jerome Bucher Brion Richard Brundle Chris E. Lawrence Berkeley Laboratory of Chemistry IBM Almaden Research Department 1 Cyclotron Road, 70A-1150 of British Columbia K-32 University Berkeley, CA 94720 Main Mall San Jose, CA 95120-6099 2036 (510) 486-4486 BC Canada V6T IZI Vancouver, (510) 486-5596 (604) 822-3266 (604) 822-2847 brion@ chem.ubc.ca

Caldwell Thomas A. Callcott James M. Bustillo C. Denise of Physics University of Tennessee ERL: Berk. Sensor & Actuator Ctr. Department of Central Florida 401 Nielsen Physics Bldg. University of California, Berkeley University RF 32816 Knoxville, TN 37996 497 Cory Hall Orlando, (407) 823-5208 (615) 974-6765 Berkeley, CA 94720 (407) 823-5112 (615) 974-3949 (510) 643-6690 phys.physics.ucf.edu tcallcot@ utkvx.utk.edu (510) 643-6637 cdc@ bustillo @ argon.eecs.berkeley.adu

2 George Castro John A. Carlisto IBM Almaden Research Center Renyu Cao Livermore National Lab. Lawrence K31/802 SSRL/SLAC L-370 P. 0. Box 808, Road P. 0. Box 4349, Bin 69 650 Harry Livermore, CA 94550 95120 Stanford, CA 95014 San Jose, CA (408) 927-2400

Karen L. Chapman David W. Chandler Franco Cerrina Lawrence Berkeley Laboratory Sandia National Laboratories Electrical & Computer Eng. 1 Cyclotron Road, 2-400 Dept. Division 8353 of Wisconsin Berkeley, CA 94720 University Mail Stop 9055 Johnson Drive (510) 486-4399 1415 Livermore, CA 94550 WI 53706-1691 (510) 486-4550 Madison, (510) 294-3132 263-4955 [email protected] (608) (510) 294-2276 (608) 265-3811 chandler @ california.gov [email protected] Ron Chiarello Yu Chen Chean Geoscience Jie Lawrence Berkeley Laboratory of California, Davis Argonne National Laboratory University 1 Cyclotron Road, 2-300 Hall 9700 S. Cass Avenue 228 Walker Berkeley, CA 94720 Davis, CA 95616 Argonne, IL 60439 (510) 486-4067

Steve Cramer Tung J. Chuang Chou Jen-Chang Inst. of Atomic & Molecular Science in S.FJScience Div. CCNA./Office Academia Sinica America Pkway 5201 Great P. 0. Box 23-166 200 Suite Taipei, Taiwan Santa Clara, CA 95054 (408) 986-8686 (408) 986-8066

Paul Marie Cuyon D. Cubayna Jane Cross Laboratoire de Spectroscopic Light Source Advanced Atomique et lonique Laboratory Lawrence Berkeley Bat. 350 Road I Cyclotron Orsay, France 91440 Berkeley, CA 94720 [email protected] Glen Dahlbacka Jay C. Davis ",hard DeMarco "Cawrence Berkeley Laboratory Lawrence Berkeley Laboratory "-' Lawrence Livermore National Lab. -1 Cyclotron Road P. 0. Box 808 1 Cyclotron Road Berkeley, CA 94720 Berkeley, CA 94720 Livermore, CA 94550 (510) 486-6320 (510) - 486-5358

Debra Dixon Jonathan Denlinger Dick DiGennaro Lawrence Berkeley Laboratory Univ. of Wisconsin-Milwaukee/LBL Advanced Light Source 1 Cyclotron Road 1 Cyclotron Road Lawrence Berkeley Laboratory Berkeley, CA 94720 Berkeley, CA 94720 1 Cyclotron Road (510) 486-2971 Berkeley, CA 94720 jzhang @b17-20.als.Ibl.gov

Norman M. Edelstein Michael Domke Harvey E. Doner Lawrence Berkeley Laboratory FB Physik Earth Sciences Division, LBL 1 Cyclotron Road, 70A-1150 Freie University, Berlin University of California, Berkeley Berkeley, CA 94720 Arnimallee 14 108 Hilgard Hall (510) 486-5624 Berlin, Germany 0.14195 Berkeley, CA 94720 (510) 486-5596 (49) 30-838 6152 (510) 642-4148 (49) 30-838 6560 (510) 643-5098 [email protected]

Charles S. Fadley David Ederer Matt D. Evans of California Davis and LBL Physics Department Iowa State University Univ. 1 Cyclotron Road, 2-100 Tulane University 117 Wilhelm Hall Berkeley, CA 94720 6823 Charles Avenue Ames, IA 50011 (510) 486-5774 New Orleans, LA 84322 (515) 294-3965 (515) 294-5825 (510) 486-5530 mevans @ ias.edu [email protected]

Bengt-Arne H. Fredriksson Benedict Feinberg Rolf Follath Department of Pathology Advanced Light Source BESSY Link6ping University Lawrence Berkeley Laboratory Lentzeallee 100 E-M Lab 1 Cyclotron Road, 80-101 Berlin, Germany 14195 Link6ping, Sweden S-58185 Berkeley, CA 94720 49-30-82004-185 46-13-222-617 (510) 486-7725 49-30-82004-103 46-13-221-529 (510) 486-4960 follath @exp.bessy.de benfr @pat.liu.se Feinberg 0 Ibl.gov

4 Donald S. Gemmetl Cylon 1 .. I%,, Hubert Gasteiger LNLS Argonne National Laboratory Berkeley Laboratory Lawrence Phy 203 1 Cyclotron Road, 2-100 9700 S. Cass Avenue Berkeley, CA 94720 Argonne, IL 60439 (510) 486-4793 (708) 252-4053 (510) 486-5530 (708) 252-2864 [email protected] b 10327 @anlvm.ctd.anl.gov

Paul Marie Guyon Eric Gullikson Cylon Goncalves da Silva Lawrence Berkeley Laboratory LNLS 1 Cyclotron Road Cx.P. 6192 Berkeley, CA 94720 Campinas, Brazil 13081.970 55-192-542624 55-192-512458

Cecilia Hakansson Donna J. Hamamoto Coryn F. Hague Lawrence Berkeley Laboratory Dept. of Synchrotron Radiation Res. CNRS/University Paris 6 213 Donner Lab (Bldg. 1) Lund University Lab. Chimie Physique Berkeley, CA 94720 Institute of Physics Paris, Cedex 05, France 75231 (510) 486-5527 S61vegatan 14 33-1-4427-6625 (510) 486-6488 Lund, Sweden S-22362 33-1-4427-6226 46-46-107265 hague@ ccr.jussieu.fr 46-46-104321

Michael H. Hecht Phil Heimann Neal Hartman Lawrence Berkeley Laboratory Jet Propulsion Laboratory Lawrence Berkeley Laboratory 1 Cyclotron Road Mail Stop 302-231 1 Cyclotron Road, 2-300 Berkeley, CA 94720 4800 Oak Grove Dr. Berkeley, CA 94720 Pasadena, CA (510) 486-4067 (818) 354-2774 (818) 393-4540 michael_h_hecht@ ccmail.jpl.nasa.gov

John W. Hepburn Oliver A. Hammers Ulrich Heinzmamn Department of Chemistry Department of Chemistry Universitast Bielefeld University of Waterloo University of Nevada, Las Vegas Fakultaet fuer Physik Waterloo, Ont., Canada NI.3Gt 4505 Maryland Parkway Poutfach 10 01 31 (519) 888-4065 Las Vegas, NM 89122 Bielefeld, Germany 33501 (519) 746-0435 (702) 895-1687 49-521-106-5469 hepburn 0 watsci. uwaterloo.ca (702) 895-4072 49-521-106-6001 [email protected]

5 ,i R. Holton Roland F. Hirsch Adam P. Hitchcock 'VG Microtech U.S.. Department of Energy •- McMaster University Bellbrook Business Park ER-73, Mail Stop F240-GTN c/o Lawrence Berkeley Laboratory Bell Lane Washington, D.C. 20585 1 Cyclotron Road, 4-230 Uckfield,Susses, LK TN21OZ (301) 903-3982 Berkeley, CA 94720 44-825-761077 (301) 903-0567 (510) 486-6695 44-825-768343 roland.hirsch@ mailgw.er.doe.gov (510) 486-7696 aph @mcmaster.ca

Chia-Wei Hsu Malcolm Howells Egon Hoyer Lawrence Berkeley Laboratory Lawrence Berkeley Laoboratory Advanced Light Source 1 Cyclotron Road, 2-300 1 Cyclotron Road Lawrence Berkeley Laboratory Berkeley, CA 94720 Berkeley, CA 94720 1 Cyclotron Road, 46-161 Berkeley, CA 94720 (510) 486-5300 (510) 486-7235 (510) 486-6741 cwh @leea.cchem.berkeley.edu

Dave Humphries Eric Hudson Tony Huff Advanced Light Source Lawrence Livermore National Lab. Lawrence Berkeley Laboratory Lawrence Berkeley Laboratory MS L-396 1 Cyclotron Road, 2-300 1 Cyclotron Road, 46-161 Livermore, CA 94551 Berkeley, CA 94720 Berkeley, CA 94720 (510) 422-0989 (510) 486-4067 (510) 486-6797

Steven C. Irick Zahid Hussain Gene E Ice Laboratory Lawrence Berkeley Laboratory Lawrence Berkeley Laboratory Oak Ridge National 1 Cyclotron Road 1 Cyclotron Road P.O. Box 2008 Berkeley, CA 94720 Berkeley, CA 94720 Oak Ridge, TN 37831-6118 (510) 486-4077 (510) 486-4299 (615) 574-2744 (510) 486-7697 [email protected] (615) 574-7659 [email protected] [email protected]

Keith Jackson Toshio Ishikawa Alan Jackson Materials Sciences Department Fujita Corporation Lawrence Berkeley Laboratory Lawrence Berkeley Laboratory SR Project 1 Cyclotron Road, 80-101 Center for X-ray Optics 5-23-15, Sendagaya, Shibuya-ku Berkeley, CA 94720 1 Cyclotron Road, 2-400 Tokyo, Japan 151 (510) 486-6752 Berkeley, CA 94720 81-3-5269-5328 (510) 486-4960 (510) 486-6894 81-3-5269-5329 [email protected] (510) 486-4955 [email protected]

6 Jiajun Jia Lotti Jochum Duane H. Jaecks Laboratory Department of Physics Lawrence Berkeley Physics Department Road University of Tennessee 1 Cyclotron University of Nebraska Knoxville, TN 37996 Berkeley, CA 94720 Lincoln, NE 68588 (615) 974-6765 (510) 486-6631 (402) 472-3274 (402) 472-2879

Loic Journel Jiahong Z. Juda Glenn Jones Obs. LSAI, Universite Paris-Sud Smithsonian Astrophysical Advanced Light Source 81 Batiment 350 60 Garden Street, MS Lawrence Berkeley Laboratory 02138 Orsay Cedex, France 91405 Cambridge, MA 1 Cyclotron Road (617) 496-7722 Berkeley, CA 94720 (617) 495-7356 [email protected]

Scot Kellar Rod Keller Christian Jung Lawrence Berkeley Laboratory Advanced Ught Source BESSY 1 Cyclotron Road, 2-300 Lawrence Berkeley Laboratory Lentzeallee 100 Berkeley, CA 94720 1 Cyclotron Road, 80-101 Berlin, Germany 14195 (510) 486-4067 Berkeley, CA 94720 49-30-82004-101 49-30-82004-103 lung @exp.bessy.d400.de

Jun Kikuma Charles H. Kim Chantal Khan-Malek Lawrence Berkeley Laboratory Lawrence Berkeley Laboratory Cir. for X-Ray Optics 1 Cyclotron Road 1 Cyclotron Road, 80-101 Lawrence Berkeley Laboratory Berkeley, CA 94720 Berkeley, CA 94720 1 Cyclotron Road, 2-400 (510) 486-2971 (510) 486-7218 Berkeley, CA 94720 (510) 486-2930 (510) 486-4960 jkikuma@ csg.lbl.gov. CKIM@LBLGOV

Brian Kincaid Janos Kirz Kwang-Je Kim Lawrence Berkeley Laboratory Department of Physics Center for Beam Physics I Cyclotron Road, 80-101 SUNY at Stony Brook Lawrence Berkeley Laboratory 11794 Berkeley, CA 94720 Stony Brook, NY 1 Cyclotron Road, 716 (510) 486-4810 (516) 632-8106 Berkeley, CA 94720 (516) 632-8101 (510) 486-7224 kirz@ sbhep.physics.sunyab-odu (510) 486-7981

7 Masato Koike Frederick Koomanoff -..-eff Kortright Department of Energy Ctr. for X-Ray Optics Center for X-ray Optics U.S. Lawrence Berkeley Laboratory Berkeley Laboratory Lawrence 1 Cyclotron Road, 2-400 1 Cyclotron Road, 2-400 Berkeley, CA 94720 Berkeley, CA 94720 (510) 486-4131 (510) 486-4550 M_Koike@LBLGOV

Jim Krupnick Krebs Kannan M. Krishnan Gary Advanced Light Source Advanced Light Source Lawrence Berkeley Laboratory Cyclotron Road, 72-209 Lawrence Berkeley Laboratory Lawrence Berkeley Laboratory 1 94720 I Cyclotron Road 1 Cyclotron Road, 80-101 Berkeley, CA Berkeley, CA 94720 CA 94720 Berkeley, (510) 486-6480

Geraldine M. Lamble Henry Lancaster Christof Kunz Laboratory Advanced Light Source Institut fOr Experimental Physik Brookhaven National Lawrence Berkeley Laboratory Hamburg Upton, NY 11973 Universitat 1 Cyclotron Road, 46-125 149 (516) 282-7734 Luruper Chausee Berkeley, CA 94720 Germany 0-22761 (516) 282-5239 Hamburg, (510) 486-4261 4940-8998-3706 [email protected] 4940-8998-2787

Ted Lauritzen Thomas W. LeBrun Gerald Lapeyre Light Source Physics Division Physics Department Advanced Laboratory Argonne National Laboratory Montana State University Lawrence Berkeley 1 Cyclotron Road 9700 South Cass Avenue 106 AJM Johnson Hall Berkeley, CA 94720 Argonne, IL 60439 Bozeman, MT 59715 (510) 486-7233 (708) 252-3624 (406) 994-6155 (708) 252-2864 (406) 994-4452 [email protected]

Levin Steve A. Lindaas Kaidee Lee Jon C. of Tennessee Lawrence Berkeley Laboratory Synchrotron Radiation Research Ctr University 401 Nielsen Phys. Bldg. 1 Cyclotron Road, 2-400 No. I R&D Rd. VI Knoxville, TN 37996 Berkekely, CA 94720 Hsinchu Science-Based Industrial Pi irk (615) 974-8705 (510) 486-4060 Hsinchu, Taiwan, China 30077 (615) 574-1118 [email protected] 886-35-780281, Ext. 7215 886-35-783892 Lee @alpha2.srrc.gov.tw

a Kueih-Tzu Lu Michael S. Lubell Dennis W. Lindle Affairs Department of Chemistry Office of Public Lawrence Berkeley Laboratory Physical Society University of California, Berkeley The American 1 Cyclotron Road Building cdo Prof. Yuan T. Lee 1050 National Press Berkeley, CA 94720 Berkeley, CA 94720 Washington, D.C. 20045 (510) 486-6859 486-5741 (202) 662-8700 (510) 486-7696 (510) (510) 486-5311 (202) 662-8711 lindie @nevada.edu ktlu @leea.cchem.berkeley.edu [email protected]

Larry Madison Martin Magnuson Edvin Lundgren Berkeley Laboratory Lawrence Livermore National Lab. Lawrence Dept of Synchrotron Radiation Res. Road P.O. Box 808, L-43 1 Cyclotron Lund University 94720 Livermore, CA 94550-0622 Berkeley, CA Institute of Physics (510) 423-7156 (510) 486-2989 S61vegatan 14 (510) 423-5998 Lund, Sweden S-22362 46-46-107265 madison1 @llnl.gov 46-46-104321 edvin.lundgrenr@ swus.lv.se Vladimir Martynov Dexter Massoletti Steve Marks Advanced Light Source Lawrence Berkeley Laboratory Lawrence Berkeley Laboratory Berkeley Laboratory 1 Cyclotron Road 1 Cyclotron Road Lawrence 1 Cyclotron Road, 2-400 Berkeley, CA 94720 Berkeley, CA 94720 Berkeley, CA 94720 (510) 486-5828 486-6751 s_marks @Ibl.gov (510)

Kristen McCutheon Robert C. McDonald Paul J. Matthews Physics Department Materials Technology Department Argonne National Laboratory University of Oregon Intel Corporation Bldg. 371T Eugene, CR 97403 P.O. Box 58119, SC2-24 9700 South Cass Avenue (503) 346-5240 3065 Bowers Avenue Argonne, IL 60439 Santa Clara, CA 95052.8119 [email protected] (708) 252-9498 (408) 765-2056 (708) 252-5291 (408) 765-2393 pjm @oxygen.aps 1.anl.gov bmcdonald @mattec.intel.com Meyer-Ilse Denis B. McWhan Werner Wayne McKinney Laboratory NSLS, Brookhaven National Lab. Lawrence Berkeley Lawrence Berkeley Laboratory Bldg. 725D 1 Cyclotron Road 1 Cyclotron Road Upton, NY 11973 Berkeley, CA 94720 Berkeley, CA 94720 (516) 282-3927 (510) 486-6892 (510) 486-4395 (516) 282-5842 (510) 486-4550 [email protected] w_meyer-ilse @ Ibl.gov

9 "Tom Morgan P-aul Morin Eddie- Moler Physics Department LURE Lawrence Berkeley Laboratory 209 Centre Universitaire Wesleyan University Bt 1 Cyclotron Road, 2-300 Orsay, France 91405 Middletown, CT 06459 Berkeley, CA 94720 33-1-6666-8124 (510) 486-4067 33-1-6666-4148 [email protected]

Art J. Nelson Demitri Mossessian Mario M. Moronne Renewable Energy Laboratory Advanced Light Source Nati. Lawrence Berkeley Laboratory 1617 Cole, SERF Lawrence Berkeley Laboratory 1 Cyclotron Road, 1-213 (3 80401 1 Cyclotron Road, 2-400 Golden, Berkeley, CA 94720 384-6628 Berkeley, CA 94720 (303) (510) 486-4236 (303) 384-6490 (510) 486-5666 (510) 486-6488 [email protected] [email protected]

Ng Cheuk-Yiu Ng Waiman Irene Nenner Berkeley Laboratory Iowa State University Lawrence LLPE 1 Cyclotron Road, 2-300 Wilhelm Hall, Rm. 103 Centre Universitaire CA 94720 Ames, IA 50011 Berkeley, Orsay, France 486-4067 (515) 294-4225 (510) (515) 294-5825 S3.CYN @ISUMYS

Railf J. Nyholm Joseph Nordgren Anders R. Nilsson Max Lab. Lawrence Berkeley Laboratory Uppsala University Lund University 1 Cyclotron Road 2-400 r/o Lawrence Berkeley Laboratory P. 0. Box 118 Berkeley, CA 94720 1 Cyclotron Road, 7-222 Lund, Sweden S-22100 Berkeley, CA 94720 46-46-104452 (510) 486-2989 46-46-104710 (510) 486-2930 ralf.nyholm @maxlab.lu.se [email protected] Oosterhuis Marjorie Olmstead Bill Robert W. Odorn Science Division Department of Physics, FM-15 Materials Charles Evans & Associates U.S. Department of Energy University of Washington 301 Chesapeake Drive Office of Energy Research Seattle, WA 98195 Redwood City, CA 94063 ER-132, J-325/GTN (415) 369-4567 Washington, DC 20545 (415) 369-7921 (301) 903-3426 (301) 903-9513

10 Roberto T. Pabaian Howard Padmore William Orme-Johnson Lawrence Berkeley Laboratory Southwest Research Institute Road, 2-400 Department of Chemistry 1 Cyclotron 6220 Culebra Road 94720 Massachusetts Inst. of Technology Berkeley, CA San Antonio, TX 78250 (510) 486-5787 Bldg. 18-23 (210) 522-5304 Ave. (510) 486-7696 48 Massachusetts (210) 522-5184 Cambridge, MA 02139 (617) 253-1862 (617) 253-1998 whoj 0 mitvma.bitnet Rupert Perera Georgeanna Perdue Alan Paterson Advanced Light Source Advanced Light Source Advanced Light Source Lawrence Berkeley Laboratory Lawrence Berkeley Laboratory Berkeley Laboratory 1 Cyclotron Road, 2-400 Lawrence 1 Cyclotron Road, 80A 1 Cyclotron Road, 46-161 Berkeley, CA 94720 Berkeley, CA 94720 CA 94720 (510) 486-5680 Berkeley, (510) 486-7407 (510) 486-4198

Piero Pianetta Maria Novella Piancastelli Ctr. Eric J. Peterson Stanford Linear Accelerator Dept. of Chem. Sci & Technology Physical Electronics, Inc. P. 0. Box 4349, MS 69 University 'Tor Vergata Cloud Drive Stanford, CA 94309 6509 Flying Rome, Italy 00173 Prairie, MN 55344 Eden 39-6-72594337 928-6332 (612) 39-6-72594328 828-6322 (612) piancastelli @roma2.infn.it

Gerd Reichhardt Francos M. Quinn Powers BESSY Linda EPSRC-Daresbury Laboratory Ctr. for Biocatalysis Science Lentzeallee 100 Warrington, LK WA4UAD University Berlin, Germany 14195 Utah State 44-1925-6i03589 UT 84322 49-30-82004-185 Logan, 44-1925-860920 49-30-82004-103 (801) 750-3386 [email protected] reichardt @exp.bessy.d400.de

David Robin Marybeth Rice R. Renner Advanced Light Source Tim Cir. for X-Ray Optics Lawrence Berkeley Laboratory Lawrence Berkeley Laboratory Lawrence Berkeley Laboratory Cyclotron Road I Cyclotron Road, 80-101 1 1 Cyclotron Road, 2-400 CA 94720 Berkeley, CA 94720 Berkekely, Berkeley, CA 94720 (510) 486-7730 (510) 486-6028 (510) 486-7696 [email protected]

11 V-,nip N. Ross A r t Robinson -v1ark D. Roper Daresbury Laboratory Lawrence Berkeley Laboratory Lawrence Berkeley Laboratory 1 Cyclotron Road, 2-100 1 Cyclotron Road, 80-101 Warrington, Cheshire, LK WA4 4AD Berkeley, CA 94720 Berkeley, CA 94720 (510) 486-6226 (510) 486-6838 44-925-603314 44-925-603124 (510) 486-5530 (510) 486-4960 [email protected] artrob @Ibi

E. Rowe Volker Saile Eli Rotenberg Jack AT&T Bell Labs. CAMD Lawrence Berkeley Laboratory Room 3L-401 Louisiana State University 1 Cyclotron Road Drive Murray Hill, NJ 07974 3990 West Lakeshore Berkeley, CA 94720 Baton Rouge, LA 70803 (510) 486-2971 (908) 582-5878 582-3904 elime6l.lbl.gov (908) rowe @physics.att.com

Fred Schlachter Volker Schmidt Dale Sayers Light Source University of Freiburg North Carolina State University Advanced Laboratory Fakultit f. Physik Box 7518 Lawrence Berkeley Road, 2-400 Freiburg, Germany 79104 Raleigh, NO 27695-7518 1 Cyclotron Berkeley, CA 94720 761-203-5793 (510) 486-4892 761-203-5873 (510) 486-7696 FAX

V. Shank David Shirley Fred Sent Charles Berkeley Laboratory Pennsylvania State University BESSY Lawrence 1 Cyclotron Road 207 Old Main Lentzeallee 100 PA 16802 Berkeley, CA 94720 University Park, Berlin, Germany 14195 (814) 863-9580 49-30-82004-151 (814) 864-9459 49-30-82004-149 [email protected]

Neville Smith Gary Sommargren David K. Shuh Lab. Lawrence Berkeley Laboratory Lawrencr. Livermore National Lawrence Berkeley Laboratory Road, 80-101 7000 East Avenue 1 Cyclotron Road, 70A-1150 1 Cyclotron CA 94720 Livermore, CA 94550 Berkeley, CA 94720 Berkeley, 486-5423 (510) 423-8599 (510) 486-6937 (510) (510) 486-5596 [email protected]

12 Giovanni Stefani Robert Stroud Stephen H. Southworth Dept. of Biophysics & Biochemistry Dip. Fisica,Terza Universitya Roma Nati. Inst. Standards & Technology Univ. of California, San Francisco Pl. A. Moro 2 A141 San Francisco, CA 94143.0448 221, Rome, Italy 1.00185 MD 20899 (415) 476-4224 Gaithersburg, 39-6-49914527 975-4850 (415) 476-1902 (301) 39-6-4957697 (301) 975-3038 stefani@ romal .infn.it [email protected]

Louis J. Terminello Ron E. Tackaberry Craig A. Taatjes Lawrence Livermore National Lab. Center for X-ray Optics Sandia National Laboratories P. 0. Box 808 Lawrence Berkeley Laboratory Box 969 L-357 P.O. 1 Cyclotron Road Livermore, CA 94551.0969 Livermore, CA 94550 Berkeley, CA 94720 (510) 294-2764 (510) 294-2276 cataatj@ ca.sandia.gov

Roland J. Thissen Ray K. Thatcher Jeff Terry Universit6 de Lidge Lawrence Berkeley Laboratory Linear Accelerator Ctr. Lab. de Spec. de Photoelectrons Stanford 1 Cyclotron Road P. 0. Box 4349, MS 99 Sart Tilman 86 Berkeley, CA 94720 Stanford, CA 94309 Liege, Belgium 4000 [email protected] (415) 926-3008 32-41564328 (415) 926-3600 32-41562941 [email protected] thissen lure.upsud.fr

Will Thur John Thompson Al C. Thompson Advanced Light Source Advanced Light Source Lawrence Berkeley Laboratory Lawrence Berkeley Laboratory Lawrence Berkeley Laboratory Road 1 Cyclotron Road 1 Cyclotron I Cyclotron Road Berkeley, CA 94720 Berkeley, CA 94720 Berkeley, CA 94720 (510) 486-5590 (510) 486-7975 (510) 486-4550

William M. Tong Tetsu K. Tokunaga James G. Tobln Chemical Sciences Division Lawrence Berkeley Laboratory Lawrence Livermore National Lab. Lawrence Berkeley Laboratory 1 Cyclotron Road, 50E Box 808, L-357 1 Cyclotron Road P. 0. Berkeley, CA 94720 Livermore, CA 94550 Berkeley, CA 94720 (510) 486-7176 422-7247 (510) 486-5141 (510) (510) 486-5686 (510) 423-7040 (510) 486-5596 [email protected] wtong 0 actinide.lbl.gov

13 A. Van Hove Brian Tonner James Underwood :hel Laboratory Department of Physics Center for X-ray Optics Lawrence Berkeley Road University of Wisconsin-Milwaukee Lawrence Berkeley Laboratory 1 Cyclotron 94720 P. O. Box 413 1 Cyclotron Road, 2-400 Berkeley, CA (510) 486-6160 Milwaukee, W' 53201 Berkeley, CA 94720 (510) 486-4995 (414) 229-4626 (510) 486-4958 (510) 486-4955 [email protected] [email protected]

Wang Gordon A. Vrdoljak Chung Wang Jun Chinese Academy of Sciences University of California, Berkeley Lawrence Berkeley Laboratory HEP ESPM 108, Hilgard Hall 1 Cyclotron Road 0. Box 918(1) Berkeley, CA 94720 Berkeley, CA 94720 P. China 100039 (510) 643-9951 Beijing, (510) 643-5098 gvrdolia @nature.Berkeley.EDU

Tony Warwick Kuilong Wang Xiaodong Wang Lawrence Berkeley Laboratory Lawrence Berkeley Laboratory Dept. of Energy & Environment 1 Cyclotron Road, 2-400 1 Cyclotron Road, 2-100 Lawrence Berkeley Laobratory CA 94720 Berkeley, CA 94720 1 Cyclotron Road Berkeley, (510) 486-5819 (510) 486-4793 Berkeley, CA 94720 (510) 486-7696 (510) 486-5530 (916) 752-0219 [email protected] klwang @ux5.lbl.gov

P. Williams Michael White Christer Wigren Gwyn National Lab. Department of Chemistry Stanford Linear Accelerator Ctr. NSLS, Brookhaven Bldg. 725D Brookhaven National Laboratory P. 0. Box 4349, MS 99 Upton, NY 11973 Bldg. 55 Stanford, CA 94309 (516) 282-7529 Upton, NY 11973 (415) 926-3938 (516) 282-3238 (516) 282-4345 (415) 926-3600 gwyn @bnl.gov (516) 282-5815 wigren@ssrlol .slac.stanford.educ

Huasheng Wu Roy F. Willis Herman Winick Berkeley Laboratory Department of Physics Stanford Synchotron Radiation Lab. Lawrence 1 Cyclotron Road, 2-300 Penn State University P. 0. Box 4349 Berkeley, CA 94720 104 Davey Laboratory Stanford, CA 94309 (510) 486-4067 University Park, PA 16802 (814) 865-6101 (814) 865-3604 rfw4@ psuvm.bitnet

14 Francois Wuilleumier Vitall K. Yachandra Robert C.Y. WU Lawrence Berkeley Laboratory Universit6 de Paris-Sud University of Southern California 1 Cyclotron Road Lab. de Spectroscopie Atom Space Sciences Center Berkeley, CA 94720 et lonique, Batiment 350 Los Angeles, CA 90089-1341 (510) 486-4330 Orsay, Cedex, France F-91405 (213) 740-6332 (510) 486-6059 33-1-6941-6536 (213) 740-6342 [email protected] 33-1-6941-9460 [email protected]

Sheila Yeh Brian W. Yates Xueming Yang Chevron Research and Technology SRC, University of Wisconsin Lawrence Berkeley Laboratory 3731 Schneider Drive 1 Cyclotron Road, 2-300 Stoughton, W1 53589 Berkeley, CA 94720 (608) 877-2353 (510) 486-7639 (608) 877-2001 (510) 486-6741 [email protected]

Anthony T. Young Jian Zhang Lawrence Berkeley Laboratory Berkeley Laboratory Lawrence 1 Cyclotron Road I Cyclotron Road, 2-400 Berkeley, CA 94720 Berkeley, CA 94720 (510) 486-7746 (510) 486-7696 [email protected]

15 Program ALS Users' Association Annual Meeting Lawrence Berkeley Laboratory October 20-21, 1994

Thursday. October 20:. 7:30 - 9:00 a=mL Special Shuttle Bus Service Shattuck Hotel to LBL (Approximately every 20 minutes) Building 50 Auditorium Building 50, Auditorium Lobby 7.30 - 9:00 Registration and Coffee

Recent Highlights from the ALS (Chair:. Michael White, Brookhaven National Laboratory) 8:30 - 8:45 Welcome C. Shank, Director, LBL DOE/BES 8:45 - 9:00 Report from the DOE W. Oosterhuis, ALS 9.00 - 10.00 Overview of the ALS B. Kincaid, Director, 10.0•1 - 1l{.30 BREAK Leader of Accelerator Group, 10:30 - 11:00 Accelerator Performance A. Jackson, ALS Padmore, Leader of Experimental 11:00 - 11:30 Experimental Systems H. Systems Group, ALS N. Smith, Scientific Program Head, ALS 11"30 - 12.'00 Scientific Program Building 6 12.00 - 14:00 p.m. Box Lunch and Vendor Exhibit

Recent Results from User Beamlines at the ALS (Chair:. Nora Berrah, Western Michigan University) 14:00 - 14"30 Report on First Results from the B. Tonner, U. of Wisconsin, Milwaukee Beamline 7.0 Spectromicroscopy Facility 14"30 - 15.'00 Soft X-Ray Fluorescence (SXF) T. Callcott, U. of Tennessee Studies on the Tennessee/Tulane Endstation on Beamline 8.0

15.00 - 15:30 BREAK 15:30 - 16:00 SXF from C60 and Other Systems J. Nordgren, Uppsala U. 16:00 - 16:20 Micromachining K. Jackson, Center for X-Ray Optics, LBL 16:20 - 16:40 High-Resolution Photoemission D. Caldwell, U. of Central Florida from Simple Atoms and Molecules 16:40 - 17.00 Resonant Photoemission from Ni A. Nilsson, Uppsala U. 17:00 Adjourn Special Shuttle Bus Service ALS Users' Association Annual Meeting

Program (continued)

Friday. October 22: Special Shuttle Bus Service Shattuck Hotel to LBL Building 50 7:45 - 9:00 a.m. Auditorium (Approximately every 20 minutes) Auditorium Lobby Area Coffee 7:45 - 8:30 New Opportunities at the (Chair: Steve Cramer, U.C. Dý F. Wuilleumier, University of Paris 9:00 Atomic Physics 8-30 R. Stroud, U.C. San Francisco 9"30 Protein Crystallography 9.00 R. Brundle, Consultant Analysis 9.30 10.00 Surface 10:30 BREAK 10.00 -L Ade, North Carolina State U. 11:00 Polymer Microscopy 10-30-- G. Williams, NSLS 11:30 Infrared Microscopy 11.00 F. Schlachter, ALS User Liaison 11:50 How to Use the ALS 11"30 M. White, Chair UEC Association Meeting 11"50 12:00 Users' Vendor Exhibit. Building 6 12:00 - 3.00 Box Lunch, p.m. and Posters Special Shuttle Bus Service to Adjourn 3:00 Shattuck Hotel

Additional program (Building 2, Room I OOB) 2IM3 - 5-00 Workshop on Infrared Microscopy

1 QQA