Fluid Analysis Solutions 2018
Table of Contents
Introduction ...... 4-6
Engine Test Solutions ...... 7-14
Industrial Plant Solutions ...... 15-30
Fleet Maintenance Solutions ...... 31-42
Portable Oil Analysis Tools ...... 43-60 FieldLab 58 ...... 45 FluidScan 1000 ...... 49 FerroCheck 2000 ...... 53 MiniVisc 3000 ...... 55 FDM 6000 ...... 57 Soot Meter ...... 59
Oil Analysis Laboratory Instruments ...... 61-78 SpectroTrack ...... 63 SpectrOil M Series ...... 65 SpectrOil 100 ...... 69 LaserNet 200 ...... 73 T2FM 500 ...... 77
Application Specific Instruments ...... 79-92 BioDiesel/Ethanol ...... 81 Oil in Water ...... 83 SpectrOil M/N-W ...... 85 FluidScan 1210 BN Analyzer ...... 87 CoolCheck 2 ...... 89 SpectrOil M/F-W ...... 91
Service and Support ...... 93
Product Catalog | 3 Introduction
About Spectro Scientific Inc .
Spectro Scientific, an ISO 9001:2008 company, specializes in analytical tools and software for machine condition monitoring . Founded in 1983, the company is one of the largest suppliers of oil, fuel and fluid analysis instruments to industry and the military worldwide . The company headquarters is in Chelmsford, MA, United States, and a research & development and sales/ marketing branch is located in Beijing, China . With the support of over 50 global sales and service representative companies, Spectro Scientific products are used in over 100 countries . Industry clients include petrochemical, mining, transportation, oil & gas exploration and power generation companies as well as commercial testing laboratories .
Spectro Scientific company timeline
Spectro Inc. Spectro Scientific founded rebrand launch Acquired by SFW Acquired Acquired by Wilks Qinetiq NA Enterprise Completed industry oil analysis solution offering
1983 1994 2008 2011 2012 2013 2014 2015 2017
Acquired On-Site Acquired Analysis Inc. Spectroil M 5200 MiniLab was approved from Emerson by JOAP with first contract
Acquired LaserNet Fines from LMCO
4 | Product Catalog Oil & Grease Analysis Solutions Oil in Water/Soil Analyzers Fuel Analysis Instruments
Applications and technologies
Spectro Scientific’s focus in fluid analysis can be divided into three areas:
n Fluid nondestructive testing (NDT) and machine condition based maintenance (CBM) . This includes new and in-service fluid analysis for lubricants and greases, coolants and hydraulic fluids . We provide lab instruments, on-site oil analysis systems, and portable tools for a variety of customer needs . n Fuel and biofuel analysis for quality control and incoming inspection for blending plants (producers) and power plants (consumers) of fuels to ensure quality fuel is produced and delivered . n Oil in water or soil for environmental compliance testing of discharged water for EPA agencies, oil drilling sites and industrial plants . Spectro Scientific has focused on providing quick and high quality fluid analysis in labs, on-site, or in the field with easy to use, environmental friendly solutions . This mission is supported by our extensive and growing intellectual property portfolio . Spectro Scientific currently owns and exclusively licenses over 70 patents covering all product lines . They can be divided into several core measurement technologies including:
n Optical Emission Spectroscopy (OES) for elemental analysis of oil, fuel, coolant and water n FPQ-XRF for wear particle analysis in oil n LaserNet Fines® laser imaging particle analysis and ferrous particle analysis in oil n InfraRed absorption spectroscopy for fluid property analysis n Solvent free kinematic viscosity for temperature controlled viscosity measurement in the field n Headspace fuel vapor analysis using Surface Acoustic Wave sensor n UV-Vis and NIR dual absorption spectroscopy for coolant and diesel exhaust fluid analysis n Sample introduction technologies that enable high quality test data with small sample volume and no need for solvent use This unique set of IPs in hardware design and measurement technologies, combined with software and expert systems for diagnostics and recommendations, enables Spectro Scientific to provide comprehensive and easy to use systems, such as the MiniLab EL Series, MiniLab Series, MicroLab Series, and FieldLab Series, that are a fraction of the cost of setting up a full laboratory with comparable data quality for test reporting and analysis .
4 | Product Catalog Product Catalog | 5 Our commitment to quality and performance Over the years Spectro Scientific has contributed greatly to the advancement of oil analysis by initiating and publishing new ASTM standards . With recent publication of several new standards majority of the products now have designated ASTM standards .This gives our customers the peace of mind of instrument performance and data integrity when they use the products in various environments and applications . PRODUCT METHOD TITLE Below is a list of products and their designated ASTM standards . SpectrOil M or 100 Series D6595 Standard Test Method for Determination of Wear Metals and Contaminants in Used Lubricating Oils or Used Hydraulic Fluids by Rotating Disc Electrode Atomic Emission Spectrometry PRODUCT METHOD TITLE
SpectrOil M or 100 Series D6728 Standard Test Method for Determination of Contaminants in Gas Turbine and Diesel SpectrOil M or 100 Series D6595 Standard Test Method for Determination of Wear Metals and Contaminants in Engine Fuel by Rotating Disc Electrode Atomic Emission Spectrometry Used Lubricating Oils or Used Hydraulic Fluids by Rotating Disc Electrode Atomic Emission Spectrometry LaserNet 200 Series D7596 Standard Test Method for Automatic Particle Counting and Particle Shape Classification of Oils Using a Direct Imaging Integrated Tester SpectrOil M or 100 Series D6728 Standard Test Method for Determination of Contaminants in Gas Turbine and Diesel Engine Fuel by Rotating Disc Electrode Atomic Emission Spectrometry SpectroVisc 300 Series D7279 Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids by Automated Houillon Viscometer LaserNet 200 Series D7596 Standard Test Method for Automatic Particle Counting and Particle Shape Classification of Oils Using a Direct Imaging Integrated Tester Fluidscan 1000 Series D7889 Standard Test Method for Field Determination of In-Service Fluid Properties Using IR SpectroVisc 300 Series D7279 Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids Spectroscopy by Automated Houillon Viscometer T2FM 500 D7690 Standard Practice for Microscopic Characterization of Particles from In-Service Fluidscan 1000 Series D7889 Standard Test Method for Field Determination of In-Service Fluid Properties Using Lubricants by Analytical Ferrography IR Spectroscopy
FDM 6000 series D8004 Standard Test Method for Fuel Dilution of In-Service Lubricants Using Surface T2FM 500 D7690 Standard Practice for Microscopic Characterization of Particles from In-Service Acoustic Wave Sensing Lubricants by Analytical Ferrography
MiniVisc 3000 Series D8092 Test Method for Coupled Particulate and Elemental Analysis using XRF for FDM 6000 Series D8004 Standard Test Method for Fuel Dilution of In-Service Lubricants Using Surface In-Service Lubricants Acoustic Wave Sensing
FerroCheck 2000 Series D8120 Standard Test Method for Ferrous Debris Quantification MiniVisc 3000 Series D8092 Test Method for Coupled Particulate and Elemental Analysis using XRF for In-Service Lubricants
FieldLab 58 FPQ-XRF D8127 Test Method for Coupled Particulate and Elemental Analysis using XRF for FerroCheck 2000 Series D8120 Standard Test Method for Ferrous Debris Quantification In-Service Lubricants
MicroLab Series D7647 Standard Test Method for Automatic Particle Counting of Lubricating and Hydraulic FieldLab 58 FPQ-XRF D8127 Test Method for Coupled Particulate and Elemental Analysis using XRF for In- Fluids Using Dilution Techniques to Eliminate the Contribution of Water and Service Lubricants Interfering Soft Particles by Light Extinction MicroLab Series D7417 Standard Test Method for Automatic Particle Counting of Lubricating and Spectro 5200 D7416 Standard Practice for Analysis of In-Service Lubricants Using a Particular Five- Hydraulic Fluids Using Dilution Techniques to Eliminate the Contribution of Water Part (Dielectric Permittivity, Time-Resolved Dielectric Permittivity with Switching and Interfering Soft Particles by Light Extinction Magnetic Fields, Laser Particle Counter, Microscopic Debris Analysis, and Orbital Viscometer) Integrated Tester Spectro 5200 D7416 Standard Practice for Analysis of In-Service Lubricants Using a Particular Five-Part (Dielectric Permittivity, Time-Resolved Dielectric Permittivity with Switching Soot Meter D7686 Standard Test Method for Field-Based Condition Monitoring of Soot in In-Service Magnetic Fields, Laser Particle Counter, Microscopic Debris Analysis, and Orbital Lubricants Using a Fixed-Filter Infrared (IR) Instrument Viscometer) Integrated Tester
Soot Meter D7686 Standard Test Method for Field-Based Condition Monitoring of Soot in In-Service InfraCal Trans-SP D7066 Standard Test Method for dimer/trimer of chlorotrifluoroethylene (S-316) Lubricants Using a Fixed-Filter Infrared (IR) Instrument Recoverable Oil and Grease and Nonpolar Material by Infrared Determination InfraCal Trans-SP D7066 Standard Test Method for dimer/trimer of chlorotrifluoroethylene (S-316) Recoverable Oil and Grease and Nonpolar Material by Infrared Determination
6 | Product Catalog High Performance Engine Test Solutions
Optimize performance
Detect problems early
Ensure safety in operation
6 | Product Catalog Engine Oil Analysis: A Reliable Technique for Engine Condition Monitoring
Engine oil analysis is a reliable and mature non-destructive testing (NDT) technique used to monitor the condition of the engine in development, on the production line and for in-service maintenance. High performance reciprocating engines and jet turbines are complicated mechanical systems with many high-speed moving parts. Comprehensive engine oil analysis provides a complete picture of engine wear and other mechanical failures in addition to lubricant condition and contamination, in almost real time with a small amount of oil. This information advances engine design and development, ensures quality in production and reduces maintenance and repair costs. The need for real time engine oil analysis for high performance engines
Achieving and maintaining optimal performance from high performance engines in airplanes, racing cars or locomotives requires much care in engineering, production, and maintenance CONTAMINATION due to size, high speed or high power output. They also need great sensitivity in oil analysis › Fuel dilution as only a few parts per million (ppm) of trace metals in the oil can indicate abnormal wear › Coolant leak of a critical part. Near real time, lab quality engine oil analysis can significantly improve › Water the productivity of research and development, production quality, and performance and ENGINE WEAR › Soot reliability of these engines. › › Elemental wear Sand and dirt analysis MiniLab EL Series: A new non-destructive tool › Total ferrous measurement for use throughout an engine’s lifecycle The new MiniLab EL Series oil analyzer is an ideal non-destructive testing (NDT) tool for engineers in research and development, production QC or in-service maintenance. The MiniLab EL system allows organizations to gain deep insights into engine and lubricant OIL CONDITION condition when and where it is needed. › Viscosity HIGH PERFORMANCE ENVIRONMENTALLY FRIENDLY › Total Base Number (TBN) n Comprehensive (up to 36 parameters) n Low waste (total 4ml of oil used) › Oxidation, Sulfation, n n Nitration Full ASTM compliance No solvent n Wear, contamination, oil condition n No hazardous chemicals › Antiwear additive depletion CONVENIENT EXPANDABLE › Total Acid Number n Fast (less than 5 minutes) n Extended metals (up to 31 elements) (TAN – natural gas engines only) n No sample preparation n Coolant analysis n No special facility requirements n Fuel analysis
| | 82 | ProductMiniLab Catalog EL Series MiniLab EL Series 3 Engine Oil Analysis: SOLUTIONS ENGINE TEST A Reliable Technique for Engine Condition Monitoring
Engine oil analysis is a reliable and mature non-destructive testing (NDT) technique used to monitor the condition of the engine in development, on the production line and for in-service maintenance. High performance reciprocating engines and jet turbines are complicated mechanical systems with many high-speed moving parts. Comprehensive engine oil analysis provides a complete picture of engine wear and other mechanical failures in addition to lubricant condition and contamination, in almost real time with a small amount of oil. This information advances engine design and development, ensures quality in production and reduces maintenance and repair costs. The need for real time engine oil analysis for high performance engines
Achieving and maintaining optimal performance from high performance engines in airplanes, racing cars or locomotives requires much care in engineering, production, and maintenance CONTAMINATION due to size, high speed or high power output. They also need great sensitivity in oil analysis › Fuel dilution as only a few parts per million (ppm) of trace metals in the oil can indicate abnormal wear › Coolant leak of a critical part. Near real time, lab quality engine oil analysis can significantly improve › Water the productivity of research and development, production quality, and performance and ENGINE WEAR › Soot reliability of these engines. › › Elemental wear Sand and dirt analysis MiniLab EL Series: A new non-destructive tool › Total ferrous measurement for use throughout an engine’s lifecycle The new MiniLab EL Series oil analyzer is an ideal non-destructive testing (NDT) tool for engineers in research and development, production QC or in-service maintenance. The MiniLab EL system allows organizations to gain deep insights into engine and lubricant OIL CONDITION condition when and where it is needed. › Viscosity HIGH PERFORMANCE ENVIRONMENTALLY FRIENDLY › Total Base Number (TBN) n Comprehensive (up to 36 parameters) n Low waste (total 4ml of oil used) › Oxidation, Sulfation, n n Nitration Full ASTM compliance No solvent n Wear, contamination, oil condition n No hazardous chemicals › Antiwear additive depletion CONVENIENT EXPANDABLE › Total Acid Number n Fast (less than 5 minutes) n Extended metals (up to 31 elements) (TAN – natural gas engines only) n No sample preparation n Coolant analysis n No special facility requirements n Fuel analysis
| | 82 | ProductMiniLab Catalog EL Series MiniLabProduct EL Catalog Series | 93 MiniLab EL Series 5 simple tests to comprehensive engine oil analysis
Location: P42 LE Ciara Unit ID: Stbd Main Engine E1061073 Model: Machine Type: Engine, Diesel: Liquid-Cooled
Viscosity at 40 is not consistent with the stated grade.
Edward O'Dwyer, 20 Jun 2017
Oil Maxol HD Marine 1240 Sample ID 671F23 671F67 6666BE 669410 656684 R6202 R6203 R5588 R5749 R4703 Sampled on 08 Jun 2017 01 Jun 2017 25 May 2017 18 May 2017 27 Apr 2017 Note: Received on 15 Jun 2017 15 Jun 2017 30 May 2017 31 May 2017 05 May 2017 Km Total 30608 30570 30536 30500 30456 Km Oil 636 598 564 528 484 Top up (l.) 700.0 600.0 600.0 500.0 50.0 Warning Limits Iron ppm 75 8 12 12 14 18 Chromium ppm 10 <1 <1 <1 <1 <1 Nickel ppm <1 <1 <1 <1 <1 Molybdenum ppm <1 1 <1 <1 <1 ASTM D6595-00 Aluminium ppm 2 2 1 2 2 WEAR METALS Lead ppm 10 <1 <1 <1 <1 <1 Copper ppm 10 <1 <1 <1 <1 <1 Tin ppm 5 <1 <1 <1 <1 <1 Silver ppm <1 <1 <1 <1 <1 Titanium ppm <1 <1 <1 <1 <1 Silicon ppm 10 5 6 6 6 8 ASTM D6595-00 CONTAMINANT Sodium ppm 20 2 4 2 2 2 S Vanadium ppm <1 <1 <1 <1 <1 Calcium ppm 2878 2898 3391 3303 3753 Magnesium ppm 9 10 10 10 10 ppm ASTM D6595-00 Phosphorus 354 489 444 408 319 ADDITIVES Zinc ppm 426 417 468 479 410 Barium ppm <1 <1 <1 <1 <1 Boron ppm <1 <1 <1 <1 <1 ASTM D445 Viscosity at 40°C cSt 138 - 168 122 126 120 117 134 Viscosity at 100°C cSt 13.6 - 16.6 13.9 14.5 13.1 14.2 16.0 TBN mg KOH/g <5.00 13.00 13.10 12.71 14.10 15.03 Water ppm 1000.0 79.0 12.0 <10.0 90.0 <10.0 ASTM E2412 Oxidation By-Products abs/mm2 5.3 4.5 5.3 6.1 5.4 Glycol (Antifreeze) % 2.6 1.2 0.1 2.2 0.6 Soot %wt 2.0 2.6 2.1 2.4 2.9 Oil Chemistry Viscosity Elements Fuel Dilution Total Ferrous Fuel Dilution % 2.0 1.8 1.2 2.0 0.0 0.0
Date 29 Aug 2017 ASTM D7889 ASTM D8092 ASTM D6595 ASTM D8004 ASTM D8120 60 microliters of oil with no 60 microliters of oil with no 2 ml of oil with no sample 0.5 ml of sample with no 2 ml sample with no sample Sample report sample preparation sample preparation preparation sample preparation preparation
Printed on: 29 Aug 2017 Page 1 of 3 1 minute test time 2 sec- 6 min, viscosity 30 seconds test time 1 minute test time 30 sec test time dependent No solvent or chemicals No solvent or chemicals No solvent or chemicals No solvent or chemicals Temperature controlled at 40C 24 elements by default No solvent or chemicals
| | 104 | MiniLab Product ELCatalog Series MiniLab EL Series 5 MiniLab EL Series SOLUTIONS ENGINE TEST 5 simple tests to comprehensive engine oil analysis
Location: P42 LE Ciara Unit ID: Stbd Main Engine E1061073 Model: Machine Type: Engine, Diesel: Liquid-Cooled
Viscosity at 40 is not consistent with the stated grade.
Edward O'Dwyer, 20 Jun 2017
Oil Maxol HD Marine 1240 Sample ID 671F23 671F67 6666BE 669410 656684 R6202 R6203 R5588 R5749 R4703 Sampled on 08 Jun 2017 01 Jun 2017 25 May 2017 18 May 2017 27 Apr 2017 Note: Received on 15 Jun 2017 15 Jun 2017 30 May 2017 31 May 2017 05 May 2017 Km Total 30608 30570 30536 30500 30456 Km Oil 636 598 564 528 484 Top up (l.) 700.0 600.0 600.0 500.0 50.0 Warning Limits Iron ppm 75 8 12 12 14 18 Chromium ppm 10 <1 <1 <1 <1 <1 Nickel ppm <1 <1 <1 <1 <1 Molybdenum ppm <1 1 <1 <1 <1 ppm ASTM D6595-00 Aluminium 2 2 1 2 2 WEAR METALS Lead ppm 10 <1 <1 <1 <1 <1 Copper ppm 10 <1 <1 <1 <1 <1 Tin ppm 5 <1 <1 <1 <1 <1 Silver ppm <1 <1 <1 <1 <1 Titanium ppm <1 <1 <1 <1 <1 Silicon ppm 10 5 6 6 6 8 ASTM D6595-00 CONTAMINANT Sodium ppm 20 2 4 2 2 2 S Vanadium ppm <1 <1 <1 <1 <1 Calcium ppm 2878 2898 3391 3303 3753 Magnesium ppm 9 10 10 10 10 ppm ASTM D6595-00 Phosphorus 354 489 444 408 319 ADDITIVES Zinc ppm 426 417 468 479 410 Barium ppm <1 <1 <1 <1 <1 Boron ppm <1 <1 <1 <1 <1 ASTM D445 Viscosity at 40°C cSt 138 - 168 122 126 120 117 134 Viscosity at 100°C cSt 13.6 - 16.6 13.9 14.5 13.1 14.2 16.0 TBN mg KOH/g <5.00 13.00 13.10 12.71 14.10 15.03 Water ppm 1000.0 79.0 12.0 <10.0 90.0 <10.0 ASTM E2412 Oxidation By-Products abs/mm2 5.3 4.5 5.3 6.1 5.4 Glycol (Antifreeze) % 2.6 1.2 0.1 2.2 0.6 Soot %wt 2.0 2.6 2.1 2.4 2.9 Oil Chemistry Viscosity Elements Fuel Dilution Total Ferrous Fuel Dilution % 2.0 1.8 1.2 2.0 0.0 0.0
Date 29 Aug 2017 ASTM D7889 ASTM D8092 ASTM D6595 ASTM D8004 ASTM D8120 60 microliters of oil with no 60 microliters of oil with no 2 ml of oil with no sample 0.5 ml of sample with no 2 ml sample with no sample Sample report sample preparation sample preparation preparation sample preparation preparation
Printed on: 29 Aug 2017 Page 1 of 3 1 minute test time 2 sec- 6 min, viscosity 30 seconds test time 1 minute test time 30 sec test time dependent No solvent or chemicals No solvent or chemicals No solvent or chemicals No solvent or chemicals Temperature controlled at 40C 24 elements by default No solvent or chemicals
| | 104 | MiniLab Product ELCatalog Series MiniLabProduct ELCatalog Series | 11 5 MiniLab 143EL
MiniLab Software Suite MiniLab 143EL or 123EL MiniLab 123EL The MiniLab Software Suite is powerful yet Two MiniLab EL Series models are available: easy to use and includes two components: MiniLab 143EL – Elements, Oil Chemistry, Viscosity, the MiniLab Device Console (MDC) and the Fuel Dilution, Total Ferrous MiniLab LIMS. MiniLab 123EL – Elements, Oil Chemistry, Viscosity The MiniLab Device Console is installed on a local PC and controls: PARAMETER Elements Oil Chemistry Viscosity Fuel Dilution Total Ferrous n Sample or asset ID entry ASTM D6595 ASTM D7889 ASTM D8092 ASTM D8004 ASTM D8120 n Instrument operation Contamination Boron, Sodium, and Potassium ✔ n Data acquisition n Automatic data transfer to Water ✔ LIMS system Soot ✔
Glycol ✔ Fuel dilution ✔ MiniLab device console Chemistry Total Base Number (TBN) ✔ Oxidation, Nitration, and Sulfation ✔ Analysis Trend Charts
Irish Naval Service Location: Additive depletion (ZDDP) ✔ P42 LE Ciara Total Acid Number (TAN) for NatGas engines and lube oils ✔ Magnesium, Calcium, Barium, Zinc, Molybdenum, and ✔ Phosphorus
Viscosity ✔ Wear Total Ferrous ✔ Copper, Silver, Chromium, Titanium, Aluminum, Nickel, ✔ Iron, Manganese, Lead, Tin, Cadmium, and Vanadium
Location: P42 LE Ciara Unit ID: Stbd Main Engine E1061073 Model: Machine Type: Engine, Diesel: Liquid-Cooled Optional Accessories Two other instruments complement the MiniLab EL Series: Viscosity at 40 is not consistent with the stated grade.
Edward O'Dwyer, 20 Jun 2017
Oil Maxol HD Marine 1240 Sample ID 671F23 671F67 6666BE 669410 656684 The SootMeter extends MiniLab EL soot in engine oil The CoolCheck 2 provides measurement and profiling of coolant R6202 R6203 R5588 R5749 R4703 Sampled on 08 Jun 2017 01 Jun 2017 25 May 2017 18 May 2017 27 Apr 2017 Note: Received on 15 Jun 2017 15 Jun 2017 30 May 2017 31 May 2017 05 May 2017 measurement up to 15% by measuring infrared absorption at condition with a near IR (NIR) and UV/Visible dual spectrometer Km Total 30608 30570 30536 30500 30456 Km Oil 636 598 564 528 484 Top up (l.) 700.0 600.0 600.0 500.0 50.0 The MiniLab LIMS is a browser-based tool; it can be installed Printed on: 29 Aug 2017 Page 2 of 3 a fixed wavelength. design that measures 8 different properties in less than 45 seconds. Warning Limits on local PCs, local networks, or hosted in the cloud server. Iron ppm 75 8 12 12 14 18 n n Chromium ppm 10 <1 <1 <1 <1 <1 ASTM Method D7686 15 ml sample volume with no sample preparation Nickel ppm <1 <1 <1 <1 <1 MiniLab LIMS includes: Molybdenum ppm <1 1 <1 <1 <1 ppm n n ASTM D6595-00 Aluminium 2 2 1 2 2 1 ml sample volume with no sample preparation 45 second test time WEAR METALS Lead ppm 10 <1 <1 <1 <1 <1 n Copper ppm 10 <1 <1 <1 <1 <1 n n Asset management Tin ppm 5 <1 <1 <1 <1 <1 30 seconds test time No solvents needed for cleaning Silver ppm <1 <1 <1 <1 <1 n Titanium ppm <1 <1 <1 <1 <1 n n Alarm limits and alarm management Silicon ppm 10 5 6 6 6 8 No solvent needed for cleaning Parameters reported are: ASTM D6595-00 CONTAMINANT Sodium ppm 20 2 4 2 2 2 n S Vanadium ppm <1 <1 <1 <1 <1 n Customizable reports, including multi-parameter trend Calcium ppm 2878 2898 3391 3303 3753 Battery powered – Type of coolant Magnesium ppm 9 10 10 10 10 ppm ASTM D6595-00 Phosphorus 354 489 444 408 319 n graphs ADDITIVES Zinc ppm 426 417 468 479 410 Measurement range: – Clarity Barium ppm <1 <1 <1 <1 <1 n Enhanced notification and email options Boron ppm <1 <1 <1 <1 <1 0-15% soot – Contamination ASTM D445 Viscosity at 40°C cSt 138 - 168 122 126 120 117 134 Viscosity at 100°C cSt 13.6 - 16.6 13.9 14.5 13.1 14.2 16.0 n Option to support multiple MiniLab EL Series analyzers TBN mg KOH/g <5.00 13.00 13.10 12.71 14.10 15.03 – Freeze point Water ppm 1000.0 79.0 12.0 <10.0 90.0 <10.0 ASTM E2412 Oxidation By-Products abs/mm2 5.3 4.5 5.3 6.1 5.4 in different locations across an enterprise Glycol (Antifreeze) % 2.6 1.2 0.1 2.2 0.6 – Glycol content Soot %wt 2.0 2.6 2.1 2.4 2.9 Fuel Dilution % 2.0 1.8 1.2 2.0 0.0 0.0 – Boiling point Date 29 Aug 2017 – Nitrites
| | 126 | MiniLab Product ELCatalog Series MiniLab EL Series 7 Printed on: 29 Aug 2017 Page 1 of 3 MiniLab 143EL SOLUTIONS ENGINE TEST
MiniLab Software Suite MiniLab 143EL or 123EL MiniLab 123EL The MiniLab Software Suite is powerful yet Two MiniLab EL Series models are available: easy to use and includes two components: MiniLab 143EL – Elements, Oil Chemistry, Viscosity, the MiniLab Device Console (MDC) and the Fuel Dilution, Total Ferrous MiniLab LIMS. MiniLab 123EL – Elements, Oil Chemistry, Viscosity The MiniLab Device Console is installed on a local PC and controls: PARAMETER Elements Oil Chemistry Viscosity Fuel Dilution Total Ferrous n Sample or asset ID entry ASTM D6595 ASTM D7889 ASTM D8092 ASTM D8004 ASTM D8120 n Instrument operation Contamination Boron, Sodium, and Potassium ✔ n Data acquisition n Automatic data transfer to Water ✔ LIMS system Soot ✔
Glycol ✔ Fuel dilution ✔ MiniLab device console Chemistry Total Base Number (TBN) ✔ Oxidation, Nitration, and Sulfation ✔ Analysis Trend Charts
Irish Naval Service Location: Additive depletion (ZDDP) ✔ P42 LE Ciara Total Acid Number (TAN) for NatGas engines and lube oils ✔ Magnesium, Calcium, Barium, Zinc, Molybdenum, and ✔ Phosphorus
Viscosity ✔ Wear Total Ferrous ✔ Copper, Silver, Chromium, Titanium, Aluminum, Nickel, ✔ Iron, Manganese, Lead, Tin, Cadmium, and Vanadium
Location: P42 LE Ciara Unit ID: Stbd Main Engine E1061073 Model: Machine Type: Engine, Diesel: Liquid-Cooled Optional Accessories Two other instruments complement the MiniLab EL Series: Viscosity at 40 is not consistent with the stated grade.
Edward O'Dwyer, 20 Jun 2017
Oil Maxol HD Marine 1240 Sample ID 671F23 671F67 6666BE 669410 656684 The SootMeter extends MiniLab EL soot in engine oil The CoolCheck 2 provides measurement and profiling of coolant R6202 R6203 R5588 R5749 R4703 Sampled on 08 Jun 2017 01 Jun 2017 25 May 2017 18 May 2017 27 Apr 2017 Note: Received on 15 Jun 2017 15 Jun 2017 30 May 2017 31 May 2017 05 May 2017 measurement up to 15% by measuring infrared absorption at condition with a near IR (NIR) and UV/Visible dual spectrometer Km Total 30608 30570 30536 30500 30456 Km Oil 636 598 564 528 484 Top up (l.) 700.0 600.0 600.0 500.0 50.0 The MiniLab LIMS is a browser-based tool; it can be installed Printed on: 29 Aug 2017 Page 2 of 3 a fixed wavelength. design that measures 8 different properties in less than 45 seconds. Warning Limits on local PCs, local networks, or hosted in the cloud server. Iron ppm 75 8 12 12 14 18 n n Chromium ppm 10 <1 <1 <1 <1 <1 ASTM Method D7686 15 ml sample volume with no sample preparation Nickel ppm <1 <1 <1 <1 <1 MiniLab LIMS includes: Molybdenum ppm <1 1 <1 <1 <1 n n ASTM D6595-00 Aluminium ppm 2 2 1 2 2 1 ml sample volume with no sample preparation 45 second test time WEAR METALS Lead ppm 10 <1 <1 <1 <1 <1 n Copper ppm 10 <1 <1 <1 <1 <1 n n Asset management Tin ppm 5 <1 <1 <1 <1 <1 30 seconds test time No solvents needed for cleaning Silver ppm <1 <1 <1 <1 <1 n Titanium ppm <1 <1 <1 <1 <1 n n Alarm limits and alarm management Silicon ppm 10 5 6 6 6 8 No solvent needed for cleaning Parameters reported are: ASTM D6595-00 CONTAMINANT Sodium ppm 20 2 4 2 2 2 n S Vanadium ppm <1 <1 <1 <1 <1 n Customizable reports, including multi-parameter trend Calcium ppm 2878 2898 3391 3303 3753 Battery powered – Type of coolant Magnesium ppm 9 10 10 10 10 ppm ASTM D6595-00 Phosphorus 354 489 444 408 319 n graphs ADDITIVES Zinc ppm 426 417 468 479 410 Measurement range: – Clarity Barium ppm <1 <1 <1 <1 <1 n Enhanced notification and email options Boron ppm <1 <1 <1 <1 <1 0-15% soot – Contamination ASTM D445 Viscosity at 40°C cSt 138 - 168 122 126 120 117 134 Viscosity at 100°C cSt 13.6 - 16.6 13.9 14.5 13.1 14.2 16.0 n Option to support multiple MiniLab EL Series analyzers TBN mg KOH/g <5.00 13.00 13.10 12.71 14.10 15.03 – Freeze point Water ppm 1000.0 79.0 12.0 <10.0 90.0 <10.0 ASTM E2412 Oxidation By-Products abs/mm2 5.3 4.5 5.3 6.1 5.4 in different locations across an enterprise Glycol (Antifreeze) % 2.6 1.2 0.1 2.2 0.6 – Glycol content Soot %wt 2.0 2.6 2.1 2.4 2.9 Fuel Dilution % 2.0 1.8 1.2 2.0 0.0 0.0 – Boiling point Date 29 Aug 2017 – Nitrites
| | 126 | MiniLab Product ELCatalog Series MiniLabProduct ELCatalog Series | 13 7 Printed on: 29 Aug 2017 Page 1 of 3 MiniLab EL Series Product Information
PART NUMBER POWER REQUIREMENTS 800-00084 MiniLab 123EL with SpectroTrack LIMS, 115VAC, 60Hz Power 1 phase power, 1200W maximum (123EL and 143EL)
800-00085 MiniLab 123EL with SpectroTrack LIMS, 230VAC, 50Hz MECHANICAL SPECIFICATIONS 800-00086 MiniLab 123EL with SpectroTrack LIMS, 115VAC, 50Hz Dimensions MiniLab 123EL: 71 cm x 183 cm x 66 cm (H x W x D) (28” x 72” x 26”) 800-00087 MiniLab 123EL with SpectroTrack LIMS, 230VAC, 60Hz MiniLab 143EL: 71 cm x 214 cm x 66 cm 800-00089 MiniLab 143EL with SpectroTrack LIMS, 115VAC, 60Hz (28” x 84” x 26”) Weight MiniLab 123EL: 76 kg (167 lbs) 800-00090 MiniLab 143EL with SpectroTrack LIMS, 230VAC, 50Hz MiniLab 143EL: 82 kg (180 lbs) 800-00091 MiniLab 143EL with SpectroTrack LIMS, 115VAC, 50Hz COMPLIANCE 800-00092 MiniLab 143EL with SpectroTrack LIMS, 230VAC, 60Hz CE Mark-EMC directive, RoHS. ACCESSORIES AND CONSUMABLES ANALYTICAL RANGE 800-00088 MiniLab 123EL standard accessories Output Analytical Range Repeatability 600-00034 MiniLab 123EL consumables kit for 500 samples Elemental concentration of 24 Range and repeatability varies with 800-00093 MiniLab 143EL standard accessories elements, ppm element
600-00035 MiniLab 143EL consumables kit for 500 samples Total ferrous, ppm 0-10,000 ppm ≤ 3% RSD
600-00126 MiniLab 123EL validation standards kit Fuel dilution 0.2-15% ≤ 5% RSD + 0.2% fuel 600-00127 MiniLab 143EL validation standards kit dilution
M99903 Coolant analysis capability program for SpectrOil 120C 40°C Kinematic viscosity, cSt 1-320 cSt at 40°C ≤ 3% RSD (factory install) 100°C kinematic viscosity calculated 320-700 cSt at 40°C ≤ 5% RSD from V40C and Viscosity Index 450-00030 MiniLab tray assembly for FluidScan and MiniVisc Total Acid Number (TAN), mg KOH/g 0-6 mg KOH/g ≤ 3% RSD 42000-00 Coolcheck 2, 115/220VAC, 50 Total Base Number (TBN), mg KOH/g 0-70 mg KOH/g ≤ 3% RSD 29701-00 Coolcheck 2 standard accessories Oxidation, abs/0.1 mm 5-32 ≤ 3% RSD 405-2048 InfraCal 2 Soot Meter Nitration, abs/cm 0.5-18 ≤ 3% RSD PRODUCT INFORMATION Sulfation, abs/0.1 mm 16-39 ≤ 3% RSD Applications Mineral and synthetic lubricants including gear, engine, hydraulic, turbine and distillate fuels Soot 0-2% ≤ 3% RSD
Methodology ASTM D6595, D8120, D8092, D7889 , D8004 Glycol 0.2-10% ≤ 3% RSD
Calibration Factory calibrated, field calibration not required. Additive depletion (ZDDP) 0-100% ≤ 3% RSD Validation and standardization fluids supplied. Water, dissolved ppm 100 ppm-saturation* ≤ 3% RSD OPERATIONAL SPECIFICATIONS *Oil specific. RSD = Relative Standard Deviation. Environmental 5-40°C ambient temperature, requirements: 10-80% RH non-condensing Sample volume < 5 ml
Solvents: None required
USER INTERFACE SPECIFICATIONS Software/operating Personal computer with Windows 7 Pro or Win 10, 32 system or 64 bit, US English version. Quad core microprocessor speed 2.6 GHz or higher and 8 GB RAM minimum.
Validation standards for MiniLab 143EL Consumables for MiniLab 143EL
To learn more about Spectro Scientific products please call 978-431-1120 or visit us online at www.spectrosci.com.
Spectro Scientific | One Executive Drive, Suite 101, Chelmsford, MA 01824-2563 978-431-1120 | www.spectrosci.com | [email protected] | An ISO 9001:2008 company Copyright © 2017 Spectro Scientific. All rights reserved. While every effort is made to assure the information in this document is accurate, Spectro Scientific does not accept liability for any errors or mistakes that may arise. Specifications are subject to change without notice. Engine_BRv1_2017-10-11 14 | Product Catalog MiniLab EL Series Product Information
PART NUMBER POWER REQUIREMENTS 800-00084 MiniLab 123EL with SpectroTrack LIMS, 115VAC, 60Hz Power 1 phase power, 1200W maximum (123EL and 143EL) 800-00085 MiniLab 123EL with SpectroTrack LIMS, 230VAC, 50Hz MECHANICAL SPECIFICATIONS Industrial Plant Solutions 800-00086 MiniLab 123EL with SpectroTrack LIMS, 115VAC, 50Hz Dimensions MiniLab 123EL: 71 cm x 183 cm x 66 cm (H x W x D) (28” x 72” x 26”) 800-00087 MiniLab 123EL with SpectroTrack LIMS, 230VAC, 60Hz MiniLab 143EL: 71 cm x 214 cm x 66 cm 800-00089 MiniLab 143EL with SpectroTrack LIMS, 115VAC, 60Hz (28” x 84” x 26”) Weight MiniLab 123EL: 76 kg (167 lbs) 800-00090 MiniLab 143EL with SpectroTrack LIMS, 230VAC, 50Hz MiniLab 143EL: 82 kg (180 lbs) 800-00091 MiniLab 143EL with SpectroTrack LIMS, 115VAC, 50Hz COMPLIANCE 800-00092 MiniLab 143EL with SpectroTrack LIMS, 230VAC, 60Hz CE Mark-EMC directive, RoHS. ACCESSORIES AND CONSUMABLES ANALYTICAL RANGE 800-00088 MiniLab 123EL standard accessories Output Analytical Range Repeatability 600-00034 MiniLab 123EL consumables kit for 500 samples Elemental concentration of 24 Range and repeatability varies with 800-00093 MiniLab 143EL standard accessories elements, ppm element Maximize
600-00035 MiniLab 143EL consumables kit for 500 samples Total ferrous, ppm 0-10,000 ppm ≤ 3% RSD machine
600-00126 MiniLab 123EL validation standards kit Fuel dilution 0.2-15% ≤ 5% RSD uptime + 0.2% fuel 600-00127 MiniLab 143EL validation standards kit dilution
M99903 Coolant analysis capability program for SpectrOil 120C 40°C Kinematic viscosity, cSt 1-320 cSt at 40°C ≤ 3% RSD (factory install) 100°C kinematic viscosity calculated 320-700 cSt at 40°C ≤ 5% RSD from V40C and Viscosity Index 450-00030 MiniLab tray assembly for FluidScan and MiniVisc Total Acid Number (TAN), mg KOH/g 0-6 mg KOH/g ≤ 3% RSD Extend 42000-00 Coolcheck 2, 115/220VAC, 50 Total Base Number (TBN), mg KOH/g 0-70 mg KOH/g ≤ 3% RSD oil drains 29701-00 Coolcheck 2 standard accessories Oxidation, abs/0.1 mm 5-32 ≤ 3% RSD 405-2048 InfraCal 2 Soot Meter Nitration, abs/cm 0.5-18 ≤ 3% RSD PRODUCT INFORMATION Sulfation, abs/0.1 mm 16-39 ≤ 3% RSD Applications Mineral and synthetic lubricants including gear, engine, hydraulic, turbine and distillate fuels Soot 0-2% ≤ 3% RSD
Methodology ASTM D6595, D8120, D8092, D7889 , D8004 Glycol 0.2-10% ≤ 3% RSD Prevent
Calibration Factory calibrated, field calibration not required. Additive depletion (ZDDP) 0-100% ≤ 3% RSD premature Validation and standardization fluids supplied. Water, dissolved ppm 100 ppm-saturation* ≤ 3% RSD failures OPERATIONAL SPECIFICATIONS *Oil specific. RSD = Relative Standard Deviation. Environmental 5-40°C ambient temperature, requirements: 10-80% RH non-condensing Sample volume < 5 ml
Solvents: None required
USER INTERFACE SPECIFICATIONS Software/operating Personal computer with Windows 7 Pro or Win 10, 32 system or 64 bit, US English version. Quad core microprocessor speed 2.6 GHz or higher and 8 GB RAM minimum.
Validation standards for MiniLab 143EL Consumables for MiniLab 143EL
To learn more about Spectro Scientific products please call 978-431-1120 or visit us online at www.spectrosci.com.
Spectro Scientific | One Executive Drive, Suite 101, Chelmsford, MA 01824-2563 978-431-1120 | www.spectrosci.com | [email protected] | An ISO 9001:2008 company Copyright © 2017 Spectro Scientific. All rights reserved. While every effort is made to assure the information in this document is accurate, Spectro Scientific does not accept liability for any errors or mistakes that may arise. Specifications are subject to change without notice. Engine_BRv1_2017-10-11 14 | Product Catalog In-service Oil Analysis for Machine Condition Monitoring
Since the reliable operation of high value, fixed assets is critical to all industrial plants, As part of a proactive maintenance program, on-site oil analysis predictive maintenance programs are implemented to manage machinery uptime. delivers rapid results with immediate decision making to:
In-service oil analysis is a key machine condition monitoring technique for Condition n Lower operating costs Based Maintenance (CBM) and Reliability programs. It complements vibration n Reduce unscheduled downtime analysis, thermography and other predictive maintenance technologies. In the time n Increase machine availability n it takes external laboratories to return oil sample results, machinery condition can Extend equipment life n Decrease total lifecycle equipment costs change significantly. On-site oil analysis eliminates this wait and enables immediate n Provide immediate retest capability decision making. Corrosion and wear cause surface degradation of the lubricated surfaces in machinery and are the root causes of most mechanically-induced equipment downtime. Corrosion Trivector™ – oil and machine health simplified is caused by water or other fluids reacting with metal surfaces, while wear is caused The TriVector™ is a simple representation of the integrity of the lubrication system and the by surface abrasion, adhesion and fatigue. health of the machine itself. The Trivector indicates the degree of health in each vector. Oil analysis provides early indications of equipment wear and identifies the root Each vector is a representation of Alarm Limits based on underlying parameters, such as viscosity, water contamination, acid number, oxidation, total ferrous, particle count and ISO causes of corrosion. code, large ferrous particle count, etc. The following questions can be answered: ONSET OF FAILURE
OPTIMAL Is the machine healthy? WORKING The P-F Curve (Potential- CONDITION Can I predict when the
Failure Curve) illustrates EQUIPMENT machinery will fail? how in-service oil analysis FAILS provides critical information on machine condition in both Proactive and Predictive PROACTIVE PREDICTIVE Maintenance periods. MAINTENANCE MAINTENANCE Monitor Oil Condition Monitor for & Contamination: In the Proactive period, oil Abnormal Wear: • Viscosity, oil chemistry, water • Total ferrous condition and contamination • Particle count with ISO codes • Wear particle analysis Is the oil dry? monitoring help prevent the • Elemental analysis of • Elemental analysis onset of the root causes normal wear particles
EQUIPMENT CONDITION Is the oil clean/ of machine failure. In the • Total ferrous free of dirt? Predictive period, monitoring FAILURE the increasing severity of wear particles allows Is it the right oil? maintenance work orders to be executed for component Is the oil fit for use? replacement or repair before COST TO TO COST REPAIR catastrophic failure. OPERATING HOURS
| | 162 | Industrial Product CatalogSolutions *Trivector is a trademark of Emerson Process Systems Industrial Solutions 3 In-service Oil Analysis for Machine Condition Monitoring
Since the reliable operation of high value, fixed assets is critical to all industrial plants, As part of a proactive maintenance program, on-site oil analysis predictive maintenance programs are implemented to manage machinery uptime. delivers rapid results with immediate decision making to:
In-service oil analysis is a key machine condition monitoring technique for Condition n Lower operating costs INDUSTRIAL PLANT SOLUTIONS Based Maintenance (CBM) and Reliability programs. It complements vibration n Reduce unscheduled downtime analysis, thermography and other predictive maintenance technologies. In the time n Increase machine availability n it takes external laboratories to return oil sample results, machinery condition can Extend equipment life n Decrease total lifecycle equipment costs change significantly. On-site oil analysis eliminates this wait and enables immediate n Provide immediate retest capability decision making. Corrosion and wear cause surface degradation of the lubricated surfaces in machinery and are the root causes of most mechanically-induced equipment downtime. Corrosion Trivector™ – oil and machine health simplified is caused by water or other fluids reacting with metal surfaces, while wear is caused The TriVector™ is a simple representation of the integrity of the lubrication system and the by surface abrasion, adhesion and fatigue. health of the machine itself. The Trivector indicates the degree of health in each vector. Oil analysis provides early indications of equipment wear and identifies the root Each vector is a representation of Alarm Limits based on underlying parameters, such as viscosity, water contamination, acid number, oxidation, total ferrous, particle count and ISO causes of corrosion. code, large ferrous particle count, etc. The following questions can be answered: ONSET OF FAILURE
OPTIMAL Is the machine healthy? WORKING The P-F Curve (Potential- CONDITION Can I predict when the
Failure Curve) illustrates EQUIPMENT machinery will fail? how in-service oil analysis FAILS provides critical information on machine condition in both Proactive and Predictive PROACTIVE PREDICTIVE Maintenance periods. MAINTENANCE MAINTENANCE Monitor Oil Condition Monitor for & Contamination: In the Proactive period, oil Abnormal Wear: • Viscosity, oil chemistry, water • Total ferrous condition and contamination • Particle count with ISO codes • Wear particle analysis Is the oil dry? monitoring help prevent the • Elemental analysis of • Elemental analysis onset of the root causes normal wear particles
EQUIPMENT CONDITION Is the oil clean/ of machine failure. In the • Total ferrous free of dirt? Predictive period, monitoring FAILURE the increasing severity of wear particles allows Is it the right oil? maintenance work orders to be executed for component Is the oil fit for use? replacement or repair before COST TO TO COST REPAIR catastrophic failure. OPERATING HOURS
| | 162 | Industrial Product CatalogSolutions *Trivector is a trademark of Emerson Process Systems InduProductstrial SolutionsCatalog | 17 3 MiniLab Series Trivector reports on 4 simple tests and less than 15 minutes machinery health to comprehensive oil analysis Easy to interpret results with Trivector sample and trend reports. Can be operated on-site by plant staff; no chemist required.
Sample Trend - Spectro Scientific
Database Plant Boston.rbm Equipment U1 Turbine - Unit 1 Turbine Area U1 - Unit One Point P1 - Before Filter
Reference Oil Chevron - GST - 32
Sample Date 11/29/2016 9/27/2016 7/28/2016 4/25/2016 1/3/2016
Sample ID 16270 16163 15987 15894 15389
ELEMENTAL ANALYSIS Machine Wear Total Fe, ppm 0 73 0 0 0
Fe >25, pml 0 0 0 0 0
Fe >38, pml 0 0 0 0 0 The elemental analyzer provides Fe >50, pml 0 0 0 0 0 Fe >100, pml 0 0 0 0 0 Machine Wear measurement of 24 elements to Wear Class MxD Ct >20, pml 0 4 3 0 0
MxD Ct >50, pml 0 0 0 0 0 identify individual contaminants, MxD Ct >100, pml MxD Sl >20, pml 0 12 5 20 0
MxD Sl >50, pml 0 0 0 0 0 wear metals and the elemental MxD Sl >100, pml MxD Ft >20, pml 0 16 8 50 0
MxD Ft >50, pml 0 0 0 10 0 composition of additives. MxD Ft >100, pml
Contamination
ISO >4 13 18 18 28 17
ISO >6 11 17 18 26 15
ISO >14 8 12 14 18 12 Contamination MxD Ox >20, pml 2 2 18 105 0
MxD Ox >50, pml 0 0 0 0 0
MxD Ox >100, pml
Cnts >4, pml 71 2102 1385 1514631 711
Cnts >6, pml 20 956 1353 570201 316
Cnts >10, pml 2 86 1033 26763 94
Cnts >14, pml 2 33 139 2395 36
Cnts >18, pml 2 15 25 308 16
Cnts >21, pml 2 5 14 135 8
Cnts >26, pml 2 2 12 76 4 Chemistry Cnts >32, pml 2 1 8 48 2
Cnts >38, pml 2 0 8 34 0
Cnts >56, pml 2.0 0.1 8.0 22.0 0.0
Cnts >70, pml 2.0 0.0 8.0 8.0 0.0
Water, ppm 0 0 39 33 0
Chemistry
Visc 40C, cSt 28.5 48.7 30.2 34.5 0.0
TAN, mg KOH/g 0.00 0.02 0.00 0.00 0.00
IR Oxid., Abs/mm2 1.98 2.11 2.03 2.01 0.00 PARTICLE COUNT AND FERROUS MONITOR The direct imaging particle counter and ferrous monitor provides particle counts and ISO codes, wear classification, ferrous particle counts & size distribution, and total ferrous measurement.
CHEMICAL ANALYSIS The infrared spectrometer measures Total Acid Number (TAN), oxidation and water for machinery oils and hydraulics.
VISCOSITY The portable viscometer provides high accuracy 40°C kinematic viscosity measurements.
| | 184 | Industrial Product CatalogSolutions Industrial Solutions 5 MiniLab Series Trivector reports on 4 simple tests and less than 15 minutes machinery health to comprehensive oil analysis Easy to interpret results with Trivector sample
and trend reports. INDUSTRIAL PLANT SOLUTIONS Can be operated on-site by plant staff; no chemist required.
Sample Trend - Spectro Scientific
Database Plant Boston.rbm Equipment U1 Turbine - Unit 1 Turbine Area U1 - Unit One Point P1 - Before Filter
Reference Oil Chevron - GST - 32
Sample Date 11/29/2016 9/27/2016 7/28/2016 4/25/2016 1/3/2016
Sample ID 16270 16163 15987 15894 15389
ELEMENTAL ANALYSIS Machine Wear Total Fe, ppm 0 73 0 0 0
Fe >25, pml 0 0 0 0 0
Fe >38, pml 0 0 0 0 0 The elemental analyzer provides Fe >50, pml 0 0 0 0 0 Fe >100, pml 0 0 0 0 0 Machine Wear measurement of 24 elements to Wear Class MxD Ct >20, pml 0 4 3 0 0
MxD Ct >50, pml 0 0 0 0 0 identify individual contaminants, MxD Ct >100, pml MxD Sl >20, pml 0 12 5 20 0
MxD Sl >50, pml 0 0 0 0 0 wear metals and the elemental MxD Sl >100, pml MxD Ft >20, pml 0 16 8 50 0
MxD Ft >50, pml 0 0 0 10 0 composition of additives. MxD Ft >100, pml
Contamination
ISO >4 13 18 18 28 17
ISO >6 11 17 18 26 15
ISO >14 8 12 14 18 12 Contamination MxD Ox >20, pml 2 2 18 105 0
MxD Ox >50, pml 0 0 0 0 0
MxD Ox >100, pml
Cnts >4, pml 71 2102 1385 1514631 711
Cnts >6, pml 20 956 1353 570201 316
Cnts >10, pml 2 86 1033 26763 94
Cnts >14, pml 2 33 139 2395 36
Cnts >18, pml 2 15 25 308 16
Cnts >21, pml 2 5 14 135 8
Cnts >26, pml 2 2 12 76 4 Chemistry Cnts >32, pml 2 1 8 48 2
Cnts >38, pml 2 0 8 34 0
Cnts >56, pml 2.0 0.1 8.0 22.0 0.0
Cnts >70, pml 2.0 0.0 8.0 8.0 0.0
Water, ppm 0 0 39 33 0
Chemistry
Visc 40C, cSt 28.5 48.7 30.2 34.5 0.0
TAN, mg KOH/g 0.00 0.02 0.00 0.00 0.00
IR Oxid., Abs/mm2 1.98 2.11 2.03 2.01 0.00 PARTICLE COUNT AND FERROUS MONITOR The direct imaging particle counter and ferrous monitor provides particle counts and ISO codes, wear classification, ferrous particle counts & size distribution, and total ferrous measurement.
CHEMICAL ANALYSIS The infrared spectrometer measures Total Acid Number (TAN), oxidation and water for machinery oils and hydraulics.
VISCOSITY The portable viscometer provides high accuracy 40°C kinematic viscosity measurements.
| | 184 | Industrial Product CatalogSolutions IndustrialProduct SolutionsCatalog | 19 5 MiniLab Series Software Reports Standard and user configurable reports can be automatically generated. The following The MiniLab Series software is based on a Laboratory Information Management System (LIMS) Spectro Scientific trend report provides a concise report with multiple parameter trend plots. designed for oil analysis. It includes an asset management database, a reference oil database and reports. The software supports multiple databases and is available with single user or optional network configurations. Sample Trend - Spectro Scientific Simple, easy to use GUI Database Plant Boston.rbm Equipment U1 Turbine - Unit 1 Turbine Area U1 - Unit One Point P1 - Before Filter
Reference Oil Chevron - GST - 32
Sample Date 11/29/2016 9/27/2016 7/28/2016 4/25/2016 1/3/2016
Sample ID 16270 16163 15987 15894 15389
Machine Wear Total Fe, ppm 0 73 0 0 0 Sample Trend - Spectro Scientific Fe >25, pml 0 0 0 0 0 Fe >38, pml 0 0 0 0 0 Database Plant Boston.rbm Equipment U1 Turbine - Unit 1 Turbine Fe >50, pml 0 0 0 0 0 Area U1 - Unit One Point P1 - Before Filter Fe >100, pml 0 0 0 0 0 Machine Wear Wear Class
MxD Ct >20, pml 0 4 3 0 0
MxD Ct >50, pml 0 0 0 0 0
MxD Ct >100, pml
MxD Sl >20, pml 0 12 5 20 0
MxD Sl >50, pml 0 0 0 0 0
MxD Sl >100, pml
MxD Ft >20, pml 0 16 8 50 0
MxD Ft >50, pml 0 0 0 10 0
MxD Ft >100, pml
Contamination
ISO >4 13 18 18 28 17
ISO >6 11 17 18 26 15
ISO >14 8 12 14 18 12 Contamination MxD Ox >20, pml 2 2 18 105 0
MxD Ox >50, pml 0 0 0 0 0
MxD Ox >100, pml
Cnts >4, pml 71 2102 1385 1514631 711
Cnts >6, pml 20 956 1353 570201 316
Cnts >10, pml 2 86 1033 26763 94
Cnts >14, pml 2 33 139 2395 36
Cnts >18, pml 2 15 25 308 16
Cnts >21, pml 2 5 14 135 8
Cnts >26, pml 2 2 12 76 4 Chemistry Cnts >32, pml 2 1 8 48 2
Cnts >38, pml 2 0 8 34 0
Cnts >56, pml 2.0 0.1 8.0 22.0 0.0
Cnts >70, pml 2.0 0.0 8.0 8.0 0.0
Water, ppm 0 0 39 33 0
Asset management Alarms Chemistry Visc 40C, cSt 28.5 48.7 30.2 34.5 0.0
TAN, mg KOH/g 0.00 0.02 0.00 0.00 0.00
• Each asset in a database Color-coded Trivector reports provide a clear snapshot IR Oxid., Abs/mm2 1.98 2.11 2.03 2.01 0.00 is structured as an Area/ of machinery health by identifying parameters that Equipment/Point/Sample. are outside normal limits. Several parameters in each A Sample has a time category of Wear-Chemistry-Contamination are assigned Trend Report – Provides data and multiple stamp and unique Sample limits. The measured values of these parameters parameter plots for a series of samples ID and is created at the compared to these limits are used to generateWear the from the same component. Point asset level. Trivector plot of machinery health. • Reference oil database. Alarm Limits are initially established for key parameters A reference oil is assigned from the templates provided in the software,
y ALARM t
to each asset to allow machinery component specifications, industry standard i s ALERT
C o
trending comparison to recommendations or from user-definedo criteria. c n s WITHIN LIMITS Thumbnail images of i t V new oil properties. a wear particles m & Industry best practice is to refine Alarm Limits based on i n y a tr The Trivector shown has chemistry & • Schedule oil samples for machine history. Once a series tof measurements is made,s io i viscosity within normal limits, wear in n em routine sampling intervals. the initial alarm limits can be analyzed and adjusted.C h an alert condition, and contamination in an alarm condition.
| | 206 | Industrial Product CatalogSolutions Industrial Solutions 7 MiniLab Series Software Reports Standard and user configurable reports can be automatically generated. The following The MiniLab Series software is based on a Laboratory Information Management System (LIMS) Spectro Scientific trend report provides a concise report with multiple parameter trend plots. designed for oil analysis. It includes an asset management database, a reference oil database and reports. The software supports multiple databases and is available with single user or optional network configurations.
Sample Trend - Spectro Scientific INDUSTRIAL PLANT SOLUTIONS Simple, easy to use GUI Database Plant Boston.rbm Equipment U1 Turbine - Unit 1 Turbine Area U1 - Unit One Point P1 - Before Filter
Reference Oil Chevron - GST - 32
Sample Date 11/29/2016 9/27/2016 7/28/2016 4/25/2016 1/3/2016
Sample ID 16270 16163 15987 15894 15389
Machine Wear Total Fe, ppm 0 73 0 0 0 Sample Trend - Spectro Scientific Fe >25, pml 0 0 0 0 0 Fe >38, pml 0 0 0 0 0 Database Plant Boston.rbm Equipment U1 Turbine - Unit 1 Turbine Fe >50, pml 0 0 0 0 0 Area U1 - Unit One Point P1 - Before Filter Fe >100, pml 0 0 0 0 0 Machine Wear Wear Class
MxD Ct >20, pml 0 4 3 0 0
MxD Ct >50, pml 0 0 0 0 0
MxD Ct >100, pml
MxD Sl >20, pml 0 12 5 20 0
MxD Sl >50, pml 0 0 0 0 0
MxD Sl >100, pml
MxD Ft >20, pml 0 16 8 50 0
MxD Ft >50, pml 0 0 0 10 0
MxD Ft >100, pml
Contamination
ISO >4 13 18 18 28 17
ISO >6 11 17 18 26 15
ISO >14 8 12 14 18 12 Contamination MxD Ox >20, pml 2 2 18 105 0
MxD Ox >50, pml 0 0 0 0 0
MxD Ox >100, pml
Cnts >4, pml 71 2102 1385 1514631 711
Cnts >6, pml 20 956 1353 570201 316
Cnts >10, pml 2 86 1033 26763 94
Cnts >14, pml 2 33 139 2395 36
Cnts >18, pml 2 15 25 308 16
Cnts >21, pml 2 5 14 135 8
Cnts >26, pml 2 2 12 76 4 Chemistry Cnts >32, pml 2 1 8 48 2
Cnts >38, pml 2 0 8 34 0
Cnts >56, pml 2.0 0.1 8.0 22.0 0.0
Cnts >70, pml 2.0 0.0 8.0 8.0 0.0
Water, ppm 0 0 39 33 0
Asset management Alarms Chemistry Visc 40C, cSt 28.5 48.7 30.2 34.5 0.0
TAN, mg KOH/g 0.00 0.02 0.00 0.00 0.00
• Each asset in a database Color-coded Trivector reports provide a clear snapshot IR Oxid., Abs/mm2 1.98 2.11 2.03 2.01 0.00 is structured as an Area/ of machinery health by identifying parameters that Equipment/Point/Sample. are outside normal limits. Several parameters in each A Sample has a time category of Wear-Chemistry-Contamination are assigned Trend Report – Provides data and multiple stamp and unique Sample limits. The measured values of these parameters parameter plots for a series of samples ID and is created at the compared to these limits are used to generateWear the from the same component. Point asset level. Trivector plot of machinery health. • Reference oil database. Alarm Limits are initially established for key parameters A reference oil is assigned from the templates provided in the software,
y ALARM t to each asset to allow machinery component specifications, industry standard i s ALERT
C o trending comparison to recommendations or from user-definedo criteria. c n s WITHIN LIMITS Thumbnail images of i t V new oil properties. a wear particles m & Industry best practice is to refine Alarm Limits based on i n y a tr The Trivector shown has chemistry & • Schedule oil samples for machine history. Once a series tof measurements is made,s io i viscosity within normal limits, wear in n em routine sampling intervals. the initial alarm limits can be analyzed and adjusted.C h an alert condition, and contamination in an alarm condition.
| | 206 | Industrial Product CatalogSolutions IndustrialProduct SolutionsCatalog | 21 7 Typical limits for machinery MiniLab Evolution The most common oil analysis tests and typical alarm limits for several component types are shown below. Component manufacturers establish alarm limits for their equipment for specified parameters. 5200 MiniLab vs MiniLab 153 The MiniLab Series is the next generation of Trivector on-site oil analyzers replacing the 5200 MiniLab.
5200 MINILAB MINILAB 153 Wear Large Ferrous content, trending only Total ferrous particle content (ppm) Wear Debris Analysis (WDA) (Optional) Wear Debris Analysis (WDA) (Optional) Automatic wear particle shape classification, count & distribution MEASUREMENT TURBINES GEAR BOXES HYDRAULICS ENGINES Ferrous particle count & distribution (> 25 µm) Particle Count / ISO Code < 18/14/12 < 19/16/13 < 15/13/11 Wear elements: Fe, Cu, Pb, Mg, Ag, Sn Water < 100 ppm < 1,000 ppm < 150 ppm < 2,500 ppm Contamination Particle count & distribution, ISO codes Particle count & distribution, ISO codes Glycol 0.1% max Emulsified water only Dissolved water (ppm) Fuel dilution 5% max Free water (ppm) Viscosity + 15% / - 10% of nominal ISO + 15% / - 10% of nominal ISO + 15% / - 10% of nominal ISO + 20% to - 10% of nominal SAE Glycol contamination for engine oils TAN Baseline + 0.1 mg KOH/g max Baseline + 1.0 mg KOH/g max Baseline + 1.0 mg KOH/g max Contaminate elements: Si, Na TBN 20% of Baseline mg KOH/g min Chemistry Dynamic viscosity @ room temperature Kinematic viscosity @ 40°C Sodium < 40 ppm Dielectric, trending only Oxidation Boron < 20 ppm Total Acid Number (TAN) Aluminum, Chromium, Tin < 15 ppm Nitration, Sulfation, Anti-wear additive, Total Base Number (TBN), and soot for engine oils Iron, Lead < 100 ppm Additive elements: Ca, P, Zn, Mg, Ba, Mo Silicon < 10 ppm Application Typical mineral and synthetic lubricant and hydraulics oils Mineral and synthetic lubricant and hydraulics for industrial rotating Copper < 30 ppm < 40 ppm for industrial rotating machinery. machinery, plus engine oil for backup generators and ground fleet, Zinc < 2 ppm Not suitable for backup generators. and special lubricants such as phosphate esters and PAG.
Particle analysis and wearing mechanism Oil library database With total ppm, ferrous particles, LaserNet total particles and the wear classifier results, users can make informative actionable decisions by The MiniLab Series includes an extensive industrial oil library database to analyze in-service oils as a variety of identifying oil drain points, corrosive wear and the onset of a serious abnormal machine wear mechanism. lubricants and fluids are used in industrial equipment. The following fluid categories can be tested:
PARTICLE COUNT FERROUS PARTICLES LASERNET LARGE FLUIDS ELEMENTAL CHEMISTRY & FERROUS VISCOSITY MONITORING TOTAL Fe PPM >20 µm PARTICLES >20 µm LASERNET CLASSIFIER Mineral oil based Hydraulic fluids and lubricants Y Y Y Y Establish constant wear rate Dynamic equilibrium levels Dynamic equilibrium levels Dynamic equilibrium levels Synthetic hydrocarbon based hydraulic fluids and lubricants Y Y Y Y Oil change interval Reaches limit level NA NA NA Ester-based Lubricant blends Y Y Y Y Onset of corrossive wear Increase in rate No change No change No change Oil Soluble Polyglycols (OSP) Y Y Y Y Transition into abnormal wear mode Increase in rate Increase Increase Increase – cutting/sliding/fatigue Organic Esters (OE) Y Y Y Y Ongoing severe wear mechanism Same or decrease in rate Increase Increase Increase – cutting /sliding/ fatigue (breakdown shear mixed layer) Phosphate Esters (Fyrquel/Skydrol) Y Y Y1 Y Temporary wear rate change due Increase in rate No change No change No change 1 Polyalkylene Glycols (PAG) Y Y Y Y to increased load and speed Poly Alpha Olefins (PAO) Y Y Y Y Onset of external contamination No change No change Increase Increase – non-metallic Polyinternal Olefins Y Y Y Y 3 Body abrasive mechanism iron No change Increase Increase Increase – cutting/sliding Polyol Esters (POE) Y Y Y Y 3 Body abrasive mechanism No change No change Increase Increase – cutting/sliding Grease Y Y2 N N non-ferrous (copper, aluminum) Mineral Transformer Oil Y N Y Y Onset of rolling contact failure No change Increase Increase Increase – fatigue
1: Require factory installed Skydrol tube and fitting kits and compatible solvent 2: Oxidation and water (absorbance units) for trending
| | 228 | Industrial Product CatalogSolutions Industrial Solutions 9 Typical limits for machinery MiniLab Evolution The most common oil analysis tests and typical alarm limits for several component types are shown below. Component manufacturers establish alarm limits for their equipment for specified parameters. 5200 MiniLab vs MiniLab 153 The MiniLab Series is the next generation of Trivector on-site oil analyzers replacing the 5200 MiniLab.
5200 MINILAB MINILAB 153
Wear Large Ferrous content, trending only Total ferrous particle content (ppm) INDUSTRIAL PLANT SOLUTIONS Wear Debris Analysis (WDA) (Optional) Wear Debris Analysis (WDA) (Optional) Automatic wear particle shape classification, count & distribution MEASUREMENT TURBINES GEAR BOXES HYDRAULICS ENGINES Ferrous particle count & distribution (> 25 µm) Particle Count / ISO Code < 18/14/12 < 19/16/13 < 15/13/11 Wear elements: Fe, Cu, Pb, Mg, Ag, Sn Water < 100 ppm < 1,000 ppm < 150 ppm < 2,500 ppm Contamination Particle count & distribution, ISO codes Particle count & distribution, ISO codes Glycol 0.1% max Emulsified water only Dissolved water (ppm) Fuel dilution 5% max Free water (ppm) Viscosity + 15% / - 10% of nominal ISO + 15% / - 10% of nominal ISO + 15% / - 10% of nominal ISO + 20% to - 10% of nominal SAE Glycol contamination for engine oils TAN Baseline + 0.1 mg KOH/g max Baseline + 1.0 mg KOH/g max Baseline + 1.0 mg KOH/g max Contaminate elements: Si, Na TBN 20% of Baseline mg KOH/g min Chemistry Dynamic viscosity @ room temperature Kinematic viscosity @ 40°C Sodium < 40 ppm Dielectric, trending only Oxidation Boron < 20 ppm Total Acid Number (TAN) Aluminum, Chromium, Tin < 15 ppm Nitration, Sulfation, Anti-wear additive, Total Base Number (TBN), and soot for engine oils Iron, Lead < 100 ppm Additive elements: Ca, P, Zn, Mg, Ba, Mo Silicon < 10 ppm Application Typical mineral and synthetic lubricant and hydraulics oils Mineral and synthetic lubricant and hydraulics for industrial rotating Copper < 30 ppm < 40 ppm for industrial rotating machinery. machinery, plus engine oil for backup generators and ground fleet, Zinc < 2 ppm Not suitable for backup generators. and special lubricants such as phosphate esters and PAG.
Particle analysis and wearing mechanism Oil library database With total ppm, ferrous particles, LaserNet total particles and the wear classifier results, users can make informative actionable decisions by The MiniLab Series includes an extensive industrial oil library database to analyze in-service oils as a variety of identifying oil drain points, corrosive wear and the onset of a serious abnormal machine wear mechanism. lubricants and fluids are used in industrial equipment. The following fluid categories can be tested:
PARTICLE COUNT FERROUS PARTICLES LASERNET LARGE FLUIDS ELEMENTAL CHEMISTRY & FERROUS VISCOSITY MONITORING TOTAL Fe PPM >20 µm PARTICLES >20 µm LASERNET CLASSIFIER Mineral oil based Hydraulic fluids and lubricants Y Y Y Y Establish constant wear rate Dynamic equilibrium levels Dynamic equilibrium levels Dynamic equilibrium levels Synthetic hydrocarbon based hydraulic fluids and lubricants Y Y Y Y Oil change interval Reaches limit level NA NA NA Ester-based Lubricant blends Y Y Y Y Onset of corrossive wear Increase in rate No change No change No change Oil Soluble Polyglycols (OSP) Y Y Y Y Transition into abnormal wear mode Increase in rate Increase Increase Increase – cutting/sliding/fatigue Organic Esters (OE) Y Y Y Y Ongoing severe wear mechanism Same or decrease in rate Increase Increase Increase – cutting /sliding/ fatigue (breakdown shear mixed layer) Phosphate Esters (Fyrquel/Skydrol) Y Y Y1 Y Temporary wear rate change due Increase in rate No change No change No change 1 Polyalkylene Glycols (PAG) Y Y Y Y to increased load and speed Poly Alpha Olefins (PAO) Y Y Y Y Onset of external contamination No change No change Increase Increase – non-metallic Polyinternal Olefins Y Y Y Y 3 Body abrasive mechanism iron No change Increase Increase Increase – cutting/sliding Polyol Esters (POE) Y Y Y Y 3 Body abrasive mechanism No change No change Increase Increase – cutting/sliding Grease Y Y2 N N non-ferrous (copper, aluminum) Mineral Transformer Oil Y N Y Y Onset of rolling contact failure No change Increase Increase Increase – fatigue
1: Require factory installed Skydrol tube and fitting kits and compatible solvent 2: Oxidation and water (absorbance units) for trending
| | 228 | Industrial Product CatalogSolutions IndustrialProduct SolutionsCatalog | 23 9 Elemental Analysis Particle Count and Ferrous Monitor › Wear particle by metal type › Ferrous content › Contamination The SpectrOil 100 Series analyzes small particulate wear, lubricant additives and The LaserNet 200 Series provides particle counts and codes, large wear particle › Wear particle shape ID by source contaminants for trace quantities of elements dissolved or suspended as fine particles. classification and ferrous wear monitoring. › Particle count Using the proven rotating disc electrode (RDE) technique, the SpectrOil 100 Series has and codes › Oil additive n Particle count, size distribution and codes (ISO 4406, NAS 1638, NAVAIR 01-1A-17, levels become the workhorse of industrial, commercial and military oil analysis laboratories SAE AS 4059, GOST, ASTM D6786, HAL, and user defined bins). requiring rapid analysis of wear metals, contaminants and additives in lubricants. n Differentiates contaminants (silica and fibers from machine wear metal) Coolant, wash-down water and JOAP calibrations are available in addition to in-service n Classifies wear particles, stores images, and reports particle count and size lubricating oil and hydraulic fluid analysis. distribution for each wear type of Cutting, Sliding, Fatigue, Fibers and Nonmetallics n Ferrous Monitor measures total ferrous content in the sample and provides Ferrous n Measures ppm levels of up to 32 elements in less than 30 seconds particle count and size distribution n Easy to operate – no sample preparation, gases, coolants or solvents needed n Widest range up to 5,000,000 particles/ml n Compliant with ASTM D6595 for used oil analysis n Test oil viscosity up to ISO320 without dilution n Images through dark fluids containing up to 2% soot n Error corrections for water and air bubbles Options include an autosampler for high throughput sample processing as well as Grating On-site oil analysis provides greater configurations without the ferrous monitor and wear classification. Exit Slits insight into contaminant sources by linking elemental parameters with the probable source: LaserNet 200 Series instrument ELEMENT Oil Chemistry – metallic CCDs can be purchased separately.
additives possible sources Fixed Electrode Ferrous Particle Sodium Corrosion inhibitor additive, Entrance also indicates coolant leak into Slit FILTER SCREEN Optics & diffraction Count & Size oil, can also be road salt, sea AC Arc grating produce SpectrOil 100 Series instrument water, ingested dirt a spectrum Fiber Optic can be purchased separately. Rotating Boron Corrosion inhibitor additive, Cable SMALL COIL SET Electrode CUTTING WEAR SLIDING WEAR antiwear/antioxidant additive; CCD CAMERA can indicate coolant leak, 640 x 480 resolution Sample 100 frames/s grease contamination Cup • Particle size distribution Magnesium Detergent/dispersive additive, • ISO 4406 cleanliness codes can also be alloying element FLOW • Particle shape classification in steels CELL SpectrOil 100 Series rotating disc electrode optical CUTTING Calcium Detergent/dispersant additive, emission spectrometer schematic FATIGUE WEAR NONMETALLIC SLIDING alkaline reserve additive for high sulfur fueled engines, can FATIGUE be grease contamination, x4 Lens Actual Pixel NON METALLIC Molybdenum Solid/liquid antiwear additive, Resoluion WATER alloy in bearing and piston rings Barium Corrosion inhibitors, detergents, rust inhibitors Emission spectrum of hydrogen Zinc Antiwear, corrosion inhibitors, anti-oxidants, alloying element for bearings, thrust washers, galvanized cases Emission spectrum of iron Sample consumed using RDE LARGE COIL SET Phosphorus Antiwear, corrosion inhibitors, technology is optically analyzed with WASTE anti-oxidants additives, EP PUMP AE spectroscopy to detect elements. Ferrous PPM additives LaserNet 230 flow diagram
| | 2410 | ProductIndustrial Catalog Solutions Industrial Solutions 11 Elemental Analysis Particle Count and Ferrous Monitor › Wear particle by metal type › Ferrous content › Contamination The SpectrOil 100 Series analyzes small particulate wear, lubricant additives and The LaserNet 200 Series provides particle counts and codes, large wear particle › Wear particle shape ID by source contaminants for trace quantities of elements dissolved or suspended as fine particles. classification and ferrous wear monitoring. › Particle count Using the proven rotating disc electrode (RDE) technique, the SpectrOil 100 Series has and codes › Oil additive n Particle count, size distribution and codes (ISO 4406, NAS 1638, NAVAIR 01-1A-17, levels become the workhorse of industrial, commercial and military oil analysis laboratories SAE AS 4059, GOST, ASTM D6786, HAL, and user defined bins). requiring rapid analysis of wear metals, contaminants and additives in lubricants. INDUSTRIAL PLANT SOLUTIONS n Differentiates contaminants (silica and fibers from machine wear metal) Coolant, wash-down water and JOAP calibrations are available in addition to in-service n Classifies wear particles, stores images, and reports particle count and size lubricating oil and hydraulic fluid analysis. distribution for each wear type of Cutting, Sliding, Fatigue, Fibers and Nonmetallics n Ferrous Monitor measures total ferrous content in the sample and provides Ferrous n Measures ppm levels of up to 32 elements in less than 30 seconds particle count and size distribution n Easy to operate – no sample preparation, gases, coolants or solvents needed n Widest range up to 5,000,000 particles/ml n Compliant with ASTM D6595 for used oil analysis n Test oil viscosity up to ISO320 without dilution n Images through dark fluids containing up to 2% soot n Error corrections for water and air bubbles Options include an autosampler for high throughput sample processing as well as Grating On-site oil analysis provides greater configurations without the ferrous monitor and wear classification. Exit Slits insight into contaminant sources by linking elemental parameters with the probable source: LaserNet 200 Series instrument ELEMENT Oil Chemistry – metallic CCDs can be purchased separately. additives possible sources Fixed Electrode Ferrous Particle Sodium Corrosion inhibitor additive, Entrance also indicates coolant leak into Slit FILTER SCREEN Optics & diffraction Count & Size oil, can also be road salt, sea AC Arc grating produce SpectrOil 100 Series instrument water, ingested dirt a spectrum Fiber Optic can be purchased separately. Rotating Boron Corrosion inhibitor additive, Cable SMALL COIL SET Electrode CUTTING WEAR SLIDING WEAR antiwear/antioxidant additive; CCD CAMERA can indicate coolant leak, 640 x 480 resolution Sample 100 frames/s grease contamination Cup • Particle size distribution Magnesium Detergent/dispersive additive, • ISO 4406 cleanliness codes can also be alloying element FLOW • Particle shape classification in steels CELL SpectrOil 100 Series rotating disc electrode optical CUTTING Calcium Detergent/dispersant additive, emission spectrometer schematic FATIGUE WEAR NONMETALLIC SLIDING alkaline reserve additive for high sulfur fueled engines, can FATIGUE be grease contamination, x4 Lens Actual Pixel NON METALLIC Molybdenum Solid/liquid antiwear additive, Resoluion WATER alloy in bearing and piston rings Barium Corrosion inhibitors, detergents, rust inhibitors Emission spectrum of hydrogen Zinc Antiwear, corrosion inhibitors, anti-oxidants, alloying element for bearings, thrust washers, galvanized cases Emission spectrum of iron Sample consumed using RDE LARGE COIL SET Phosphorus Antiwear, corrosion inhibitors, technology is optically analyzed with WASTE anti-oxidants additives, EP PUMP AE spectroscopy to detect elements. Ferrous PPM additives LaserNet 230 flow diagram
| | 2410 | ProductIndustrial Catalog Solutions IndustrialProduct Solutions Catalog | 2511 › Viscosity › Water Chemical Analysis Viscosity
› TAN ® › TBN The FluidScan 1000 Series oil chemistry analyzer determines when in-service oil is no The MiniVisc 3000 Series provides fast, accurate 40°C kinematic viscosity measurements for › Oxidation longer fit for use due to oil degradation or the ingress of water or glycol. It is fast and easy detection of viscosity variations caused by contamination, mix-up and oil degradation. › Nitration easy to use, with just one drop of oil needed for the sample and less than one minute for › Sulfation n Solvent free, portable, and easy to use test results. The analyzer includes an extensive oil library; additional oils can be added › Soot n Viscosity range 1-700 cSt @40°C › Additive depletion by the user. n Accuracy +/- 3% to NIST viscosity standards › Glycol n Compliant to ASTM D7889 “Standard Test Method for Field Determination of n Fast results: ISO 15 ~10 seconds, ISO 320 ~ 3 minutes In-service Fluid Properties Using IR Spectroscopy” n High correlation to TAN and TBN laboratory tests conducted with ASTM D664 and D4739 n Patented, Comprehensive Water Measurement option extends range to 6.5%. For machinery oils, the 40°C kinematic (Included with all MiniLab systems.) viscosity is used as the reference value. Engine oils operate at higher temperatures than rotating machinery, so they require V100°C kinematic viscosity. The Viscosity Index of an oil is a parameter that relates the V40°C measurement value to the V100°C value. A reference Viscosity Index value can be entered in the viscometer and both the FluidScan 1000 Series MiniVisc 3000 Series portable viscometer measured V40°C viscosity and the calculated handheld infrared spectrometer can be purchased separately. V100°C viscosity values are displayed. can be purchased separately. Positive displacement pipette
The oil library contains various categories of fluids. The industrial library provided with the MiniLab series includes the Comprehensive Water Solution and the Industrial Fluid Oil Library. Industrial CATEGORY Fluid Library Open the two parallel plates for easy cleaning. MiniVisc 3000 Series kinematic viscometer schematic ASTM EP Gear/Hydro ✔ ASTM Petroleum Crankcase ✔ ASTM Polyol Ester ✔ BIODIESEL FEEDSTOCK CHILLER ✔ ENGINE ✔ FluidScan operating principle ENGINE-HEAVY DUTY ENGINE-HFO Total Ferrous ENGINE-NAT GAS ETHANOL IN GASOLINE The MiniLab 33 includes the FerroCheck, a portable ferrous analyzer that measures the FAME total ferrous content of a sample. It is easy to operate; simply insert the sample vial FAME in DIESEL ✔ COMPREHENSIVE 6.5% with fluid sample to measure. GEAR-PRESSURE WATER SOLUTION GEAR-SPLASH ✔ Dissolved and n Small sample requirement with results in 30 seconds HEAT TRANSFER ✔ Free Water Measurement – Up to 6.5% water n No sample preparation and no solvents required to clean HYDRAULIC ✔ n Measurement range 0-10,000 ppm for oil, 10-150,000 ppm for grease HYDRAULIC-FIRE RESISTANT ✔ ✔ SLIDEWAY STANDARD RANGE 0.03% TRANSMISSION Saturation Dissolved Water TURBINE-AERO ✔ Limit Measurement – (Oil Specific) Up to saturation limit FerroCheck 2000 Series portable ferrous TURBINE-CCGT ✔ analyzer can be purchased separately. TURBINE-STEAM ✔ Water measurement range Grease boat and sample introduction vials
| | 2612 | ProductIndustrial Catalog Solutions Industrial Solutions 13 › Viscosity › Water Chemical Analysis Viscosity
› TAN ® › TBN The FluidScan 1000 Series oil chemistry analyzer determines when in-service oil is no The MiniVisc 3000 Series provides fast, accurate 40°C kinematic viscosity measurements for › Oxidation longer fit for use due to oil degradation or the ingress of water or glycol. It is fast and easy detection of viscosity variations caused by contamination, mix-up and oil degradation. › Nitration easy to use, with just one drop of oil needed for the sample and less than one minute for › Sulfation n Solvent free, portable, and easy to use test results. The analyzer includes an extensive oil library; additional oils can be added › Soot n Viscosity range 1-700 cSt @40°C
› Additive depletion by the user. INDUSTRIAL PLANT SOLUTIONS n Accuracy +/- 3% to NIST viscosity standards › Glycol n Compliant to ASTM D7889 “Standard Test Method for Field Determination of n Fast results: ISO 15 ~10 seconds, ISO 320 ~ 3 minutes In-service Fluid Properties Using IR Spectroscopy” n High correlation to TAN and TBN laboratory tests conducted with ASTM D664 and D4739 n Patented, Comprehensive Water Measurement option extends range to 6.5%. For machinery oils, the 40°C kinematic (Included with all MiniLab systems.) viscosity is used as the reference value. Engine oils operate at higher temperatures than rotating machinery, so they require V100°C kinematic viscosity. The Viscosity Index of an oil is a parameter that relates the V40°C measurement value to the V100°C value. A reference Viscosity Index value can be entered in the viscometer and both the FluidScan 1000 Series MiniVisc 3000 Series portable viscometer measured V40°C viscosity and the calculated handheld infrared spectrometer can be purchased separately. V100°C viscosity values are displayed. can be purchased separately. Positive displacement pipette
The oil library contains various categories of fluids. The industrial library provided with the MiniLab series includes the Comprehensive Water Solution and the Industrial Fluid Oil Library. Industrial CATEGORY Fluid Library Open the two parallel plates for easy cleaning. MiniVisc 3000 Series kinematic viscometer schematic ASTM EP Gear/Hydro ✔ ASTM Petroleum Crankcase ✔ ASTM Polyol Ester ✔ BIODIESEL FEEDSTOCK CHILLER ✔ ENGINE ✔ FluidScan operating principle ENGINE-HEAVY DUTY ENGINE-HFO Total Ferrous ENGINE-NAT GAS ETHANOL IN GASOLINE The MiniLab 33 includes the FerroCheck, a portable ferrous analyzer that measures the FAME total ferrous content of a sample. It is easy to operate; simply insert the sample vial FAME in DIESEL ✔ COMPREHENSIVE 6.5% with fluid sample to measure. GEAR-PRESSURE WATER SOLUTION GEAR-SPLASH ✔ Dissolved and n Small sample requirement with results in 30 seconds HEAT TRANSFER ✔ Free Water Measurement – Up to 6.5% water n No sample preparation and no solvents required to clean HYDRAULIC ✔ n Measurement range 0-10,000 ppm for oil, 10-150,000 ppm for grease HYDRAULIC-FIRE RESISTANT ✔ ✔ SLIDEWAY STANDARD RANGE 0.03% TRANSMISSION Saturation Dissolved Water TURBINE-AERO ✔ Limit Measurement – (Oil Specific) Up to saturation limit FerroCheck 2000 Series portable ferrous TURBINE-CCGT ✔ analyzer can be purchased separately. TURBINE-STEAM ✔ Water measurement range Grease boat and sample introduction vials
| | 2612 | ProductIndustrial Catalog Solutions IndustrialProduct Solutions Catalog | 2713 Four MiniLab Options. Which One is for You? Accessories & Consumables
MiniLab 153 – provides a complete oil analysis report Sample Preparation Equipment Consumables with elemental analysis, comprehensive wear particle Sample preparation equipment such as the Homogenizer, Ultrasonic Deaerator, Electrode Spectro Scientific consumables are analysis, solid and water contamination, fluid chemistry Sharpener and Consumables for 100 samples is included with each MiniLab 153 system. selected and carefully tested with all and viscosity. It is ideal for large power plants and Spectro Scientific instruments to ensure manufacturing plants with many assets. SAMPLE PREPARATION – 3 SIMPLE STEPS consistent, repeatable results. Always use MiniLab 153 – 4 tests MiniLab 53 – provides a Trivector report with 1. Sharpen electrode Spectro Scientific certified consumables comprehensive wear particle analysis, solid and water 2. Homogenize the sample for better water for best results. contamination, fluid chemistry and viscosity. measurement 3. Ultrasonically degas the sample for MiniLab 33 – provides a basic Trivector report with total particle analysis ferrous wear, fluid chemistry, water in oil and viscosity. MiniLab 53 – 3 tests MiniLab 23 – provides basic oil condition information including viscosity, chemistry and water in oil.
Validation Standards and ASTM Standards Accessories MiniLab 33 – 3 tests Validation standards are supplied for all A variety of accessories to support your MiniLab Series instrumentation. These NIST oil analysis program are available, from traceable standards support internal quality drawing a sample from an oil sump to programs and compare current instrument preparing it for analysis. performance against factory calibration. MiniLab 23 – 2 tests All instruments in the MiniLab Series have an associated ASTM Standard Test Method.
Solvent Filtration and • PARTICLE COUNTER STANDARD • FERROUS PARTICLE ANALYZER • FLUIDSCAN IR CHECK FLUID Dispenser (A5051SF) PARAMETER Elemental Particle Count Ferrous Viscosity Chemical LNF-509 calibration checkfluid LNF-545 Ferrous Validation FL310 FluidScan CheckFluid and Ferrous Standard for Magnetometer ASTM METHOD D6595 ASTM METHOD D7596 ASTM METHOD D8120 ASTM METHOD D8092 ASTM METHOD D7889 • SPECTROMETER STANDARDS – Total Ferrous Content, • VISCOSITY STANDARDS Contamination Particle count and ISO codes ✔ CS-24 100 ppm, 900ppm, baseoil nominal 100 ppm PV1025 Visc 30 standard Wear Debris Anlaysis Kits: – Large Ferrous particle count, PV1026 Visc120 standard 115V (400-00101) Sampling Pump Non-metallic particle count, distribution and images ✔ nominal 42 µm particles 220V (400-00102) (350-00030) Sodium and Silicon ✔ Total Water ✔ Chemistry Viscosity ✔ Total Acid Number (TAN) ✔ Oxidation ✔ Service Contracts and Repair Total Base Number (TBN), Oxidation, Nitration, and ✔ Sulfation for engine oils Spectro Scientific’s service offerings for the MiniLab Series include:
Magnesium, Calcium, Barium, Zinc, Molybdenum, and ✔ System Installation & Training for instrument operation and routine maintenance. Phosphorus Service Contracts for extended warranty and preventive maintenance. Wear Wear particle images, counts and distribution ✔ Field Repair by certified customer service engineers on site. Total Ferrous content, ppm ✔ ✔ In-house Instrument Calibration, Maintenance, Repair, and Upgrades Ferrous particle count and size distribution ✔ performed at our facility near Boston, MA. Copper, Silver, Chromium, Titanium, Aluminum, Nickel, ✔ Iron, Manganese, Lead, Tin, Cadmium, and Vanadium
| | 2814 | ProductIndustrial Catalog Solutions Industrial Solutions 15 Four MiniLab Options. Which One is for You? Accessories & Consumables
MiniLab 153 – provides a complete oil analysis report Sample Preparation Equipment Consumables with elemental analysis, comprehensive wear particle Sample preparation equipment such as the Homogenizer, Ultrasonic Deaerator, Electrode Spectro Scientific consumables are analysis, solid and water contamination, fluid chemistry Sharpener and Consumables for 100 samples is included with each MiniLab 153 system. selected and carefully tested with all and viscosity. It is ideal for large power plants and Spectro Scientific instruments to ensure manufacturing plants with many assets. SAMPLE PREPARATION – 3 SIMPLE STEPS consistent, repeatable results. Always use INDUSTRIAL PLANT SOLUTIONS MiniLab 153 – 4 tests MiniLab 53 – provides a Trivector report with 1. Sharpen electrode Spectro Scientific certified consumables comprehensive wear particle analysis, solid and water 2. Homogenize the sample for better water for best results. contamination, fluid chemistry and viscosity. measurement 3. Ultrasonically degas the sample for MiniLab 33 – provides a basic Trivector report with total particle analysis ferrous wear, fluid chemistry, water in oil and viscosity. MiniLab 53 – 3 tests MiniLab 23 – provides basic oil condition information including viscosity, chemistry and water in oil.
Validation Standards and ASTM Standards Accessories MiniLab 33 – 3 tests Validation standards are supplied for all A variety of accessories to support your MiniLab Series instrumentation. These NIST oil analysis program are available, from traceable standards support internal quality drawing a sample from an oil sump to programs and compare current instrument preparing it for analysis. performance against factory calibration. MiniLab 23 – 2 tests All instruments in the MiniLab Series have an associated ASTM Standard Test Method.
Solvent Filtration and • PARTICLE COUNTER STANDARD • FERROUS PARTICLE ANALYZER • FLUIDSCAN IR CHECK FLUID Dispenser (A5051SF) PARAMETER Elemental Particle Count Ferrous Viscosity Chemical LNF-509 calibration checkfluid LNF-545 Ferrous Validation FL310 FluidScan CheckFluid and Ferrous Standard for Magnetometer ASTM METHOD D6595 ASTM METHOD D7596 ASTM METHOD D8120 ASTM METHOD D8092 ASTM METHOD D7889 • SPECTROMETER STANDARDS – Total Ferrous Content, • VISCOSITY STANDARDS Contamination Particle count and ISO codes ✔ CS-24 100 ppm, 900ppm, baseoil nominal 100 ppm PV1025 Visc 30 standard Wear Debris Anlaysis Kits: – Large Ferrous particle count, PV1026 Visc120 standard 115V (400-00101) Sampling Pump Non-metallic particle count, distribution and images ✔ nominal 42 µm particles 220V (400-00102) (350-00030) Sodium and Silicon ✔ Total Water ✔ Chemistry Viscosity ✔ Total Acid Number (TAN) ✔ Oxidation ✔ Service Contracts and Repair Total Base Number (TBN), Oxidation, Nitration, and ✔ Sulfation for engine oils Spectro Scientific’s service offerings for the MiniLab Series include:
Magnesium, Calcium, Barium, Zinc, Molybdenum, and ✔ System Installation & Training for instrument operation and routine maintenance. Phosphorus Service Contracts for extended warranty and preventive maintenance. Wear Wear particle images, counts and distribution ✔ Field Repair by certified customer service engineers on site. Total Ferrous content, ppm ✔ ✔ In-house Instrument Calibration, Maintenance, Repair, and Upgrades Ferrous particle count and size distribution ✔ performed at our facility near Boston, MA. Copper, Silver, Chromium, Titanium, Aluminum, Nickel, ✔ Iron, Manganese, Lead, Tin, Cadmium, and Vanadium
| | 2814 | ProductIndustrial Catalog Solutions IndustrialProduct Solutions Catalog | 2915 MiniLab Series Product Information PART NUMBER USER INTERFACE SPECIFICATIONS 800-00029 MiniLab 153 with OilView LIMS and PC, 115 VAC, 60 Hz. Software/Operating Personal computer with Windows 10 Pro or Windows 7 Pro, 800-00027 MiniLab 153, 115 VAC, 60 Hz. Requires OilView LIMS. System 32 or 64 bit, US English version. Quad core microprocessor speed 2.6 GHz or higher and 8 GB RAM minimum. 800-00030 MiniLab 153 with OilView LIMS and PC, 220 VAC, 50 Hz. 800-00028 MiniLab 153, 220 VAC, 50 Hz. Requires OilView LIMS. POWER REQUIREMENTS 800-00076 MiniLab 153 with OilView LIMS and PC, 240 VAC, 60 Hz. Power MiniLab 153: 1 Phase power, 1200 W (max) 800-00079 Minilab 153, 240 VAC, 60 Hz. Requires Oilview LIMS. MiniLab 53/33/23: 1 Phase power, 110 W (max) 800-00077 MiniLab 153 with OilView LIMS and PC, 120 VAC, 50 Hz. MECHANICAL SPECIFICATIONS 800-00078 Minilab 153, 120 VAC, 50 Hz. Requires Oilview LIMS. Dimensions MiniLab 153: 71 cm x 214 cm x 66 cm (28” x 84” x 26”) 800-00017 MiniLab 53, 115 VAC, 50/ 60 Hz. Requires OilView LIMS. (H x W x D) MiniLab 53: 35 cm x 50 cm x 53 cm (13.8” x 19.7” x 21”) 800-00018 MiniLab 53, 220 VAC, 50/60 Hz. Requires OilView LIMS. Minilab 33: 14 cm x 69 cm x 48 cm (5.5 x 27” x 19”) 800-00025 MiniLab 53, 115 VAC, 50/60 Hz with OilView LIMS Minilab 23: 10 cm x 51 cm x 48 cm (4” x 20” x 19”) 800-00026 MiniLab 53, 220 VAC, 50/60 Hz with OilView LIMS. Weight MiniLab 153: 84 kg (185 lbs) 800-00059 MiniLab 33, 115 VAC, 50/60 Hz. Requires OilView LIMS. MiniLab 53: 14 kg (31 lbs) 800-00060 MiniLab 33, 220 VAC, 50/60 Hz. Requires OilView LIMS. MiniLab 33: 9 kg (22 lbs) 800-00061 MiniLab 33, 115 VAC, 50/60 Hz with OilView LIMS. MiniLab 23: 6 kg (14 lbs) 800-00062 MiniLab 33, 220 VAC, 50/60 Hz with OilView LIMS. COMPLIANCE 800-00037 MiniLab 23, 115 VAC, 50/60 Hz. Requires Oilview LIMS. CE Mark-EMC directive, RoHS 800-00038 MiniLab 23, 220 VAC, 50/60 Hz. Requires Oilview LIMS. ANALYTICAL RANGE AND REPEATABILITY 800-00041 MiniLab 23, 115 VAC, 50/60 Hz with Oilview LIMS. Output Analytical Range Repeatability 800-00042 MiniLab 23, 220 VAC, 50/60 Hz with Oilview LIMS. Particle count and size distribution Particle count ≤ 6% RSD *OilView LIMS v5.61 or v5.7 is required for MiniLab operation. ISO codes per 4402/4406, 4-100 µm ACCESSORIES AND CONSUMABLES other codes selectable 800-00031 MiniLab 153 Standard Accessories Kit Ferrous particle count and size 25-100 µm ≤ 5% RSD 800-00032 MiniLab 153 Consumables Kit for 500 samples distribution 800-00019 MiniLab 53 Standard Accessories Kit Total Ferrous, ppm 10-2,000 ppm ≤ 5% RSD 400-00088 MiniLab 53 Consumables Kit for 500 samples Wear particle counts and size 20-100 µm distribution by wear mode : fatique, 800-00063 MiniLab 33 Standard Accessories Kit sliding, cutting,non-metallic, fibers 800-00064 MiniLab 33 Consumables Kit for 500 samples 40°C Kinematic viscosity, cSt 1-320 cSt at 40°C ≤ 3% RSD SA1022 MiniLab 23 Standard Accessories Kit 320-700 cSt at 40°C ≤ 5% RSD 800-00040 MiniLab 23 Consumables Kit for 500 samples Total Acid Number (TAN), mg KOH/g 0-6 mg KOH/g ≤ 3% RSD 600-00123 Minilab 153 Validation standards kit Total Base Number (TBN), mg KOH/g 0-70 mg KOH/g ≤ 3% RSD 600-00122 Minilab 53 Validation standards kit Oxidation, abs/0.1 mm 5-32 ≤ 3% RSD 600-00120 Minilab 33 Validation standards kit Nitration, abs/cm 0.5-18 ≤ 3% RSD 600-00119 Minilab 23 Validation standards kit Sulfation, abs/0.1 mm 16-39 ≤ 3% RSD 800-00073 MiniLab 153 with Skydrol kit standard accessories Water, dissolved ppm 100 ppm-saturation* ≤ 3% RSD 800-00072 MiniLab 53 with Skydrol kit standard accessories Water, free, ppm 0.03-6.5% (300- ≤ 25% RSD LNF-905 Skydrol kit (phosphate ester fluids) for LaserNet 230 only; 65,000 ppm) factory installation Elemental concentration of 23 Elemental analysis range and FL360 All Libraries license for FluidScan elements, ppm repeatability vary with element PRODUCT INFORMATION *Oil specific. RSD = Relative Standard Deviation. Applications Mineral and synthetic lubricants including gear, engine, hydraulic, turbine and distillate fuels SUPPORT RESOURCES Methodology ASTM D7596, ASTM D7889, ASTM 40831 ASTM D6595 SVC019 Service Contract – MiniLab 33 Calibration Factory calibrated, field calibration not required. SVC015 Service Contract – MiniLab 53 Validation and standardization fluids supplied. SVC057 Service Contract – MiniLab 153 OPERATIONAL SPECIFICATIONS Spectro Scientific offers On- and Off-site Product Training, Field Repair, In-house Environmental 5-40°C ambient temperature, 10-80% RH Instrument Calibration, Maintenance, Repair, and Upgrades and Service Contracts. Requirements non-condensing, 2000 m maximum altitude See previous page for more information about service and customer support. Sample Volume 30-50 ml, varies with viscosity Solvents Lamp oil, odorless kerosene, or Electron 22
To learn more about Spectro Scientific products please call 978-431-1120 or visit us online at www.spectrosci.com.
Spectro Scientific | One Executive Drive, Suite 101, Chelmsford, MA 01824-2563 978-431-1120 | www.spectrosci.com | [email protected] | An ISO 9001:2008 company Copyright © 2017 Spectro Scientific. All rights reserved. While every effort is made to assure the information in this document is accurate, Spectro Scientific does not accept liability for any errors or mistakes that may arise. Specifications are subject to change without notice. Industrial_BRv3_2017-09-27 30 | Product Catalog MiniLab Series Product Information PART NUMBER USER INTERFACE SPECIFICATIONS 800-00029 MiniLab 153 with OilView LIMS and PC, 115 VAC, 60 Hz. Software/Operating Personal computer with Windows 10 Pro or Windows 7 Pro, 800-00027 MiniLab 153, 115 VAC, 60 Hz. Requires OilView LIMS. System 32 or 64 bit, US English version. Quad core microprocessor speed 2.6 GHz or higher and 8 GB RAM minimum. 800-00030 MiniLab 153 with OilView LIMS and PC, 220 VAC, 50 Hz. Fleet Maintenance Solutions 800-00028 MiniLab 153, 220 VAC, 50 Hz. Requires OilView LIMS. POWER REQUIREMENTS 800-00076 MiniLab 153 with OilView LIMS and PC, 240 VAC, 60 Hz. Power MiniLab 153: 1 Phase power, 1200 W (max) 800-00079 Minilab 153, 240 VAC, 60 Hz. Requires Oilview LIMS. MiniLab 53/33/23: 1 Phase power, 110 W (max) 800-00077 MiniLab 153 with OilView LIMS and PC, 120 VAC, 50 Hz. MECHANICAL SPECIFICATIONS 800-00078 Minilab 153, 120 VAC, 50 Hz. Requires Oilview LIMS. Dimensions MiniLab 153: 71 cm x 214 cm x 66 cm (28” x 84” x 26”) 800-00017 MiniLab 53, 115 VAC, 50/ 60 Hz. Requires OilView LIMS. (H x W x D) MiniLab 53: 35 cm x 50 cm x 53 cm (13.8” x 19.7” x 21”) 800-00018 MiniLab 53, 220 VAC, 50/60 Hz. Requires OilView LIMS. Minilab 33: 14 cm x 69 cm x 48 cm (5.5 x 27” x 19”) 800-00025 MiniLab 53, 115 VAC, 50/60 Hz with OilView LIMS Minilab 23: 10 cm x 51 cm x 48 cm (4” x 20” x 19”) 800-00026 MiniLab 53, 220 VAC, 50/60 Hz with OilView LIMS. Weight MiniLab 153: 84 kg (185 lbs) 800-00059 MiniLab 33, 115 VAC, 50/60 Hz. Requires OilView LIMS. MiniLab 53: 14 kg (31 lbs) 800-00060 MiniLab 33, 220 VAC, 50/60 Hz. Requires OilView LIMS. MiniLab 33: 9 kg (22 lbs) 800-00061 MiniLab 33, 115 VAC, 50/60 Hz with OilView LIMS. MiniLab 23: 6 kg (14 lbs) 800-00062 MiniLab 33, 220 VAC, 50/60 Hz with OilView LIMS. COMPLIANCE Maximize 800-00037 MiniLab 23, 115 VAC, 50/60 Hz. Requires Oilview LIMS. CE Mark-EMC directive, RoHS 800-00038 MiniLab 23, 220 VAC, 50/60 Hz. Requires Oilview LIMS. machine ANALYTICAL RANGE AND REPEATABILITY 800-00041 MiniLab 23, 115 VAC, 50/60 Hz with Oilview LIMS. Output Analytical Range Repeatability uptime 800-00042 MiniLab 23, 220 VAC, 50/60 Hz with Oilview LIMS. Particle count and size distribution Particle count ≤ 6% RSD *OilView LIMS v5.61 or v5.7 is required for MiniLab operation. ISO codes per 4402/4406, 4-100 µm ACCESSORIES AND CONSUMABLES other codes selectable 800-00031 MiniLab 153 Standard Accessories Kit Ferrous particle count and size 25-100 µm ≤ 5% RSD 800-00032 MiniLab 153 Consumables Kit for 500 samples distribution 800-00019 MiniLab 53 Standard Accessories Kit Total Ferrous, ppm 10-2,000 ppm ≤ 5% RSD Extend 400-00088 MiniLab 53 Consumables Kit for 500 samples Wear particle counts and size 20-100 µm oil drains distribution by wear mode : fatique, 800-00063 MiniLab 33 Standard Accessories Kit sliding, cutting,non-metallic, fibers 800-00064 MiniLab 33 Consumables Kit for 500 samples 40°C Kinematic viscosity, cSt 1-320 cSt at 40°C ≤ 3% RSD SA1022 MiniLab 23 Standard Accessories Kit 320-700 cSt at 40°C ≤ 5% RSD 800-00040 MiniLab 23 Consumables Kit for 500 samples Total Acid Number (TAN), mg KOH/g 0-6 mg KOH/g ≤ 3% RSD 600-00123 Minilab 153 Validation standards kit Total Base Number (TBN), mg KOH/g 0-70 mg KOH/g ≤ 3% RSD 600-00122 Minilab 53 Validation standards kit Oxidation, abs/0.1 mm 5-32 ≤ 3% RSD 600-00120 Minilab 33 Validation standards kit Nitration, abs/cm 0.5-18 ≤ 3% RSD Prevent 600-00119 Minilab 23 Validation standards kit Sulfation, abs/0.1 mm 16-39 ≤ 3% RSD premature 800-00073 MiniLab 153 with Skydrol kit standard accessories Water, dissolved ppm 100 ppm-saturation* ≤ 3% RSD 800-00072 MiniLab 53 with Skydrol kit standard accessories Water, free, ppm 0.03-6.5% (300- ≤ 25% RSD failures LNF-905 Skydrol kit (phosphate ester fluids) for LaserNet 230 only; 65,000 ppm) factory installation Elemental concentration of 23 Elemental analysis range and FL360 All Libraries license for FluidScan elements, ppm repeatability vary with element PRODUCT INFORMATION *Oil specific. RSD = Relative Standard Deviation. Applications Mineral and synthetic lubricants including gear, engine, hydraulic, turbine and distillate fuels SUPPORT RESOURCES Methodology ASTM D7596, ASTM D7889, ASTM 40831 ASTM D6595 SVC019 Service Contract – MiniLab 33 Calibration Factory calibrated, field calibration not required. SVC015 Service Contract – MiniLab 53 Validation and standardization fluids supplied. SVC057 Service Contract – MiniLab 153 OPERATIONAL SPECIFICATIONS Spectro Scientific offers On- and Off-site Product Training, Field Repair, In-house Environmental 5-40°C ambient temperature, 10-80% RH Instrument Calibration, Maintenance, Repair, and Upgrades and Service Contracts. Requirements non-condensing, 2000 m maximum altitude See previous page for more information about service and customer support. Sample Volume 30-50 ml, varies with viscosity Solvents Lamp oil, odorless kerosene, or Electron 22
To learn more about Spectro Scientific products please call 978-431-1120 or visit us online at www.spectrosci.com.
Spectro Scientific | One Executive Drive, Suite 101, Chelmsford, MA 01824-2563 978-431-1120 | www.spectrosci.com | [email protected] | An ISO 9001:2008 company Copyright © 2017 Spectro Scientific. All rights reserved. While every effort is made to assure the information in this document is accurate, Spectro Scientific does not accept liability for any errors or mistakes that may arise. Specifications are subject to change without notice. Industrial_BRv3_2017-09-27 30 | Product Catalog Oil Analysis for Vehicle Preventative Maintenance
The reliable operation of vehicles in a fleet is critical in virtually every industry that As part of a proactive maintenance program, on-site oil analysis depends on equipment powered by engines including: delivers rapid results with immediate decision making to:
n Automotive n Trucking n Energy n Lower operating costs n Mining n Construction n Government (military and municipal) n Reduce unscheduled downtime n Increase vehicle availability and extend vehicle life Maintenance programs are implemented to keep this equipment operating and performing its required work. Downtime not only costs money to repair the equipment Achieving green initiatives with oil analysis but also lost productivity and loss of customer confidence. 500 6 =x 3000 Reduction in new oil fill and used oil disposal by extending oil drains can greatly Oil analysis is a critical part of vehicle maintenance, providing valuable information on contribute to achieving eco-goals. On-site oil analysis provides information about
the condition of the oil and the health of the vehicle. To be most effective, oil analysis the oil health while the equipment is being serviced so the mechanic knows HEAVY DUTY LESS LESS USED & TRUCKS GALLONS OF OIL LESS DISPOSED must be used when the mechanic is working on the vehicle so the technician can take instantly if the oil can be safely extended. immediate action and, if necessary, retest the oil for confirmation. An oil analysis Extending just one oil drain per vehicle per year can have a significant impact on EXAMPLE: With an average oil drain of program lowers the risk of a vehicle roadside failure and eliminates the costs involved oil usage and disposal across an entire fleet. 6 gallons per vehicle, reduction of 1 oil drain per vehicle in a fleet of 500 heavy duty trucks with having equipment out of service. saves 3000 gallons of oil per year.
ONSET OF FAILURE Oil analysis can help answer the following questions
OPTIMAL WORKING CONDITION SERVICEABLE LIFE OF THE OIL MECHANICAL ISSUES WITH THE EQUIPMENT EQUIPMENT FAILS
PROACTIVE PREDICTIVE Is there mechanical failure MAINTENANCE MAINTENANCE allowing contamination to enter? The longer it takes to identify Is it the right oil? (Coolant or dirt) a problem along the failure (Right viscosity and additive package) curve, the more expensive it Are the vehicle components in becomes to fix the equipment. Is the oil clean? good condition?
EQUIPMENT CONDITION (No dirt or dust) (Free of abnormal wear debris) Oil analysis is used for proactive maintenance to help FAILURE Can the oil drain be extended? Can I predict when a component prevent the onset of failures. (Degradation of viscosity or oil chemistry) will fail? (Wear metals present) In the predictive maintenance stage, oil analysis can identify Is there a coolant or a fuel leak? problems before they become (Elemental contamination or catastrophic failures. TO COST REPAIR degradation of viscosity) OPERATING HOURS
| | 322 | Fleet Product Solutions Catalog Fleet Solutions 3 Oil Analysis for Vehicle Preventative Maintenance
The reliable operation of vehicles in a fleet is critical in virtually every industry that As part of a proactive maintenance program, on-site oil analysis depends on equipment powered by engines including: delivers rapid results with immediate decision making to:
n Automotive n Trucking n Energy n Lower operating costs n Mining n Construction n Government (military and municipal) n Reduce unscheduled downtime n Increase vehicle availability and extend vehicle life Maintenance programs are implemented to keep this equipment operating and performing its required work. Downtime not only costs money to repair the equipment Achieving green initiatives with oil analysis but also lost productivity and loss of customer confidence. 500 6 =x 3000 Reduction in new oil fill and used oil disposal by extending oil drains can greatly
Oil analysis is a critical part of vehicle maintenance, providing valuable information on contribute to achieving eco-goals. On-site oil analysis provides information about FLEET MAINTENANCE SOLUTIONS the condition of the oil and the health of the vehicle. To be most effective, oil analysis the oil health while the equipment is being serviced so the mechanic knows HEAVY DUTY LESS LESS USED & TRUCKS GALLONS OF OIL LESS DISPOSED must be used when the mechanic is working on the vehicle so the technician can take instantly if the oil can be safely extended. immediate action and, if necessary, retest the oil for confirmation. An oil analysis Extending just one oil drain per vehicle per year can have a significant impact on EXAMPLE: With an average oil drain of program lowers the risk of a vehicle roadside failure and eliminates the costs involved oil usage and disposal across an entire fleet. 6 gallons per vehicle, reduction of 1 oil drain per vehicle in a fleet of 500 heavy duty trucks with having equipment out of service. saves 3000 gallons of oil per year.
ONSET OF FAILURE Oil analysis can help answer the following questions
OPTIMAL WORKING CONDITION SERVICEABLE LIFE OF THE OIL MECHANICAL ISSUES WITH THE EQUIPMENT EQUIPMENT FAILS
PROACTIVE PREDICTIVE Is there mechanical failure MAINTENANCE MAINTENANCE allowing contamination to enter? The longer it takes to identify Is it the right oil? (Coolant or dirt) a problem along the failure (Right viscosity and additive package) curve, the more expensive it Are the vehicle components in becomes to fix the equipment. Is the oil clean? good condition?
EQUIPMENT CONDITION (No dirt or dust) (Free of abnormal wear debris) Oil analysis is used for proactive maintenance to help FAILURE Can the oil drain be extended? Can I predict when a component prevent the onset of failures. (Degradation of viscosity or oil chemistry) will fail? (Wear metals present) In the predictive maintenance stage, oil analysis can identify Is there a coolant or a fuel leak? problems before they become (Elemental contamination or catastrophic failures. TO COST REPAIR degradation of viscosity) OPERATING HOURS
| | 322 | Fleet Product Solutions Catalog ProductFleet SCatalogolutions | 33 3 ® MicroLab Series Four automated oil tests FULLY AUTOMATED OIL ANALYSIS CHEMISTRY ® The MicroLab combines automation and artificial intelligence in an all-in-one oil analysis tool. The MicroLab Infrared Spectrometer measures six key parameters which indicate 15 minutes to comprehensive oil analysis potential oil degradation and contamination. Both the MicroLab 30 and 40 provide: n Can be operated by maintenance staff, no chemist required Oil degradation: oxidation, nitration, total n Fully automated operation and cleaning base number n Easy to understand reports with color-coded alarm limits and diagnostic statements Oil contamination: soot, water, glycol Monitoring equipment and oil health with oil analysis VISCOSITY The four automated MicroLab tests provide a complete look at equipment The MicroLab Dual Temperature Viscometer and oil condition. provides kinematic viscosity analysis which can help identify potential oil degradation or Mechanical condition parameters indicate potential equipment failure: contamination. Wear metal analysis Contamination (glycol, dirt, water) Both the MicroLab 30 and 40 provide: Kinematic viscosity at 40°C and 100°C Oil condition parameters indicate potential degradation and contamination: Viscosity Index (VI) Viscosity Oil chemistry (Total Base Number, oxidation, nitration) Contamination (glycol, water, soot, particle count) ELEMENTAL ANALYSIS Oil additive levels The MicroLab Optical Emission Spectrometer quantifies wear metals cause from mechanical components, as well as other elements from oil additives or sources of MicroLab 40 MicroLab 30 contamination. For engines, For engines, MicroLab 30 analyzes 10 basic metals: transmissions, transmissions, power steering, power steering, aluminum, chromium, copper, iron, lead, generators, generators molybdenum, potassium, silicon, sodium, hydraulics, and tin. It is upgradable to include all 20 gear oils elements. Infrared ✔ ✔ MicroLab 40 analyzes 20 elements spectrometer including the basic metals listed above and the extended metals: barium, boron, Kinematic ✔ ✔ viscometer calcium, magnesium, manganese, nickel, phosphorous, titanium, vanadium, and zinc. OES elemental ✔ ✔ analyzer
PARTICLE COUNT Particle ✔ The MicroLab 40 model is equipped with counter a particle counter to measure particle contamination which is crucial for maintaining hydraulic systems, compressors and turbines. The MicroLab 40 measures: Gross particle count ISO particle size
| | 344 | Fleet Product Solutions Catalog Fleet Solutions 5 ® MicroLab Series Four automated oil tests FULLY AUTOMATED OIL ANALYSIS CHEMISTRY ® The MicroLab combines automation and artificial intelligence in an all-in-one oil analysis tool. The MicroLab Infrared Spectrometer measures six key parameters which indicate 15 minutes to comprehensive oil analysis potential oil degradation and contamination. Both the MicroLab 30 and 40 provide: n Can be operated by maintenance staff, no chemist required Oil degradation: oxidation, nitration, total n Fully automated operation and cleaning base number n Easy to understand reports with color-coded alarm limits and diagnostic statements Oil contamination: soot, water, glycol Monitoring equipment and oil health with oil analysis VISCOSITY
The four automated MicroLab tests provide a complete look at equipment FLEET MAINTENANCE SOLUTIONS The MicroLab Dual Temperature Viscometer and oil condition. provides kinematic viscosity analysis which can help identify potential oil degradation or Mechanical condition parameters indicate potential equipment failure: contamination. Wear metal analysis Contamination (glycol, dirt, water) Both the MicroLab 30 and 40 provide: Kinematic viscosity at 40°C and 100°C Oil condition parameters indicate potential degradation and contamination: Viscosity Index (VI) Viscosity Oil chemistry (Total Base Number, oxidation, nitration) Contamination (glycol, water, soot, particle count) ELEMENTAL ANALYSIS Oil additive levels The MicroLab Optical Emission Spectrometer quantifies wear metals cause from mechanical components, as well as other elements from oil additives or sources of MicroLab 40 MicroLab 30 contamination. For engines, For engines, MicroLab 30 analyzes 10 basic metals: transmissions, transmissions, power steering, power steering, aluminum, chromium, copper, iron, lead, generators, generators molybdenum, potassium, silicon, sodium, hydraulics, and tin. It is upgradable to include all 20 gear oils elements. Infrared ✔ ✔ MicroLab 40 analyzes 20 elements spectrometer including the basic metals listed above and the extended metals: barium, boron, Kinematic ✔ ✔ viscometer calcium, magnesium, manganese, nickel, phosphorous, titanium, vanadium, and zinc. OES elemental ✔ ✔ analyzer
PARTICLE COUNT Particle ✔ The MicroLab 40 model is equipped with counter a particle counter to measure particle contamination which is crucial for maintaining hydraulic systems, compressors and turbines. The MicroLab 40 measures: Gross particle count ISO particle size
| | 344 | Fleet Product Solutions Catalog ProductFleet SCatalogolutions | 35 5 Converting Test Data EXPERT SYSTEM Sample into Maintenance Actions Input
User Rules Knowledge MicroLab Reports Interface Engine Base Advice The MicroLab has an embedded expert system that translates chemistry results into diagnostic Non-expert Knowledge statements specific to the type of equipment and guides the technician on necessary User from an Expert maintenance actions. The diagnostic statements can indicate whether an oil change is required or if the oil drain interval can be extended. It can also direct the technician to potential The user inputs information about: the equpment, mechanical problems to investigate. the component and the oil being tested . . . The Expert System does the rest. The comprehensive reports: Save time – compiles and analyzes all test data Embedded Expert System Take the guess work out of interpreting results – provides suggested maintenance actions Comprehensive MicroLab report includes color-coded alarm limits, diagnostic statements and trending history. Save money – no need to hire an analytical resource The Expert System is the “brains” of the MicroLab, translating analytical data into maintenance actions so the technician or mechanic do not need to interpret the chemistry behind the report; they simply read the service recommendations on the report. Built from Sample history for trending analysis over 20 years of industry knowledge and more than 10,000 individual software scripts, the MicroLab’s Expert System generates diagnostics that are specific to the: Analysis Results: Units Current Sample Sample ID 6 5 4 3 Date Analyzed 9/19/2017 9/19/2017 9/19/2017 9/19/2017 equipment application (e.g., automotive, on-road trucking, off-road trucking, generators) Date Sample Taken 9/19/2017 9/19/2017 9/19/2017 9/19/2017 Top Up qt/gal/L component type (e.g., diesel engine, gasoline engine, hydraulic) Miles on Oil 7500 2500 7500 3850 and often the equipment manufacturer Account: MICROLAB SYSTEM TEST Miles on Component 15000 10000 7500 3850 Address: 1 EXECUTIVE DR Oil Changed Y/N No Yes No No CHELMSFORD MA 01824 Oil Condition: The Expert System utilizes Rule Sets which are specific to each component type. These Rule Phone: Nitration abs <2.0 <2.0 8.1 - Sets contain the threshold levels and diagnostic scripts that are applied to sample results Email: Oxidation abs <2.0 <2.0 8.1 - Vehicle ID: OVER-ROAD Total Base Number mg KOH/g 8.9 9.4 3.9 3.9 to generate diagnostic statements. The Expert System grades individual sample results as Viscosity @ 100°C (M) cSt 10.3 11.0 7.6 8.2 Vehicle Make: FORD Viscosity @ 40°C (M) cSt 64 65 46 48 Normal, Abnormal or Severe, using color-coding of the results on the report. Vehicle Model: EXPLORER LIMITED Viscosity Index 148 162 132 145 Color-coded Vehicle Year : 2017 Contamination: Before comparing the results to custom threshold levels stored in the system’s database, the Glycol % - - - - alarm limits Component ID: OVER-ROADGSGENERAL Potassium ppm <2 <2 <2 <2 system automatically factors in: Component Type : GASOLINE ENGINE Silicon ppm <2 <2 <2 3 Sodium ppm <2 <2 31 24 Soot % <0.1 <0.1 <0.1 <0.1 usage time on the component Water % 2.0 <0.1 3.0 >3 Oil Brand: MOBIL time on the oil Wear Metals: Oil Type: MOBIL 1 FORMULA Aluminium ppm <2 <2 <2 <2 break-in periods Oil Weight: 5W30 Chromium ppm <2 <2 <2 <2 Sump Capacity: 6 QUARTS Copper ppm <2 3 8 12 Viscosity Limit 40 Deg C 50 - 68 Iron ppm <2 <2 15 17 Manganese ppm 0 0 0 1 Viscosity Limit 100 Deg C 9.3 - 12.5 FOR EXAMPLE Molybdenum ppm <2 <2 52 59 Diagnosis for current sample Nickel ppm 0 1 6 0 Lead ppm <2 <2 <2 <2 HEAVY CONCENTRATION OF WATER PRESENT. CHECK FOR SOURCE OF WATER ENTRY. OIL DRAIN AND REFILL MAY BE NECESSARY. CONSULT Tin ppm <2 <2 <2 <2 SERVICE PROVIDER FOR FURTHER RECOMMENDATIONS. TO CONFIRM, Titanium ppm 0 0 0 0 Report Results: 25 ppm Lead, 20 ppm Tin RESAMPLE AT 5,000 MILES (8,000 KM) OR 100 HOURS. Vanadium ppm 1 0 0 0 Additives: Barium ppm 0 0 0 0 Time on Engine Time on Oil Alarm Diagnostic Statement Diagnostic statements Boron ppm 41 31 25 27 Calcium ppm 1524 1162 1508 1360 with maintenance Magnesium ppm 41 22 0 0 35,000 miles 15,000 miles NORMAL WEAR METALS DETECTED FOR BREAK-IN OR OVERHAUL PERIOD recommendations Phosphorus ppm 744 663 814 756 Zinc ppm 1004 779 1243 877 375,000 miles 15,000 miles ABNORMAL BEARING WEAR DETECTED Additional Tests: Fuel Dilution % 0.7 1.0 4.8 4.5 Total Acid Number mg KOH/g 5.0 3.0 6.0 6.2 375,000 miles 5,000 miles SEVERE BEARING WEAR DETECTED Legend Total Ferrous ppm 250.0 200.0 925.0 920.0 ABNORMAL SEVERE X = NOT TESTED / - = NOT DETECTED Water % 2.0 0.0 3.0 3.2 NOT APPLICABLE
NA = NOT C = CALCULATED M = MEASURED AVAILABLE Results from external devices Given the same results for wear metals but varying the time on the component and oil, the resulting diagnostic statements will be different.
| | 366 | Fleet Product Solutions Catalog Fleet Solutions 7 Converting Test Data EXPERT SYSTEM Sample into Maintenance Actions Input
User Rules Knowledge MicroLab Reports Interface Engine Base Advice The MicroLab has an embedded expert system that translates chemistry results into diagnostic Non-expert Knowledge statements specific to the type of equipment and guides the technician on necessary User from an Expert maintenance actions. The diagnostic statements can indicate whether an oil change is required or if the oil drain interval can be extended. It can also direct the technician to potential The user inputs information about: the equpment, mechanical problems to investigate. the component and the oil being tested . . . The Expert System does the rest. The comprehensive reports:
Save time – compiles and analyzes all test data FLEET MAINTENANCE SOLUTIONS Embedded Expert System Take the guess work out of interpreting results – provides suggested maintenance actions Comprehensive MicroLab report includes color-coded alarm limits, diagnostic statements and trending history. Save money – no need to hire an analytical resource The Expert System is the “brains” of the MicroLab, translating analytical data into maintenance actions so the technician or mechanic do not need to interpret the chemistry behind the report; they simply read the service recommendations on the report. Built from Sample history for trending analysis over 20 years of industry knowledge and more than 10,000 individual software scripts, the MicroLab’s Expert System generates diagnostics that are specific to the: Analysis Results: Units Current Sample Sample ID 6 5 4 3 Date Analyzed 9/19/2017 9/19/2017 9/19/2017 9/19/2017 equipment application (e.g., automotive, on-road trucking, off-road trucking, generators) Date Sample Taken 9/19/2017 9/19/2017 9/19/2017 9/19/2017 Top Up qt/gal/L component type (e.g., diesel engine, gasoline engine, hydraulic) Miles on Oil 7500 2500 7500 3850 and often the equipment manufacturer Account: MICROLAB SYSTEM TEST Miles on Component 15000 10000 7500 3850 Address: 1 EXECUTIVE DR Oil Changed Y/N No Yes No No CHELMSFORD MA 01824 Oil Condition: The Expert System utilizes Rule Sets which are specific to each component type. These Rule Phone: Nitration abs <2.0 <2.0 8.1 - Sets contain the threshold levels and diagnostic scripts that are applied to sample results Email: Oxidation abs <2.0 <2.0 8.1 - Vehicle ID: OVER-ROAD Total Base Number mg KOH/g 8.9 9.4 3.9 3.9 to generate diagnostic statements. The Expert System grades individual sample results as Viscosity @ 100°C (M) cSt 10.3 11.0 7.6 8.2 Vehicle Make: FORD Viscosity @ 40°C (M) cSt 64 65 46 48 Normal, Abnormal or Severe, using color-coding of the results on the report. Vehicle Model: EXPLORER LIMITED Viscosity Index 148 162 132 145 Color-coded Vehicle Year : 2017 Contamination: Before comparing the results to custom threshold levels stored in the system’s database, the Glycol % - - - - alarm limits Component ID: OVER-ROADGSGENERAL Potassium ppm <2 <2 <2 <2 system automatically factors in: Component Type : GASOLINE ENGINE Silicon ppm <2 <2 <2 3 Sodium ppm <2 <2 31 24 Soot % <0.1 <0.1 <0.1 <0.1 usage time on the component Water % 2.0 <0.1 3.0 >3 Oil Brand: MOBIL time on the oil Wear Metals: Oil Type: MOBIL 1 FORMULA Aluminium ppm <2 <2 <2 <2 break-in periods Oil Weight: 5W30 Chromium ppm <2 <2 <2 <2 Sump Capacity: 6 QUARTS Copper ppm <2 3 8 12 Viscosity Limit 40 Deg C 50 - 68 Iron ppm <2 <2 15 17 Manganese ppm 0 0 0 1 Viscosity Limit 100 Deg C 9.3 - 12.5 FOR EXAMPLE Molybdenum ppm <2 <2 52 59 Diagnosis for current sample Nickel ppm 0 1 6 0 Lead ppm <2 <2 <2 <2 HEAVY CONCENTRATION OF WATER PRESENT. CHECK FOR SOURCE OF WATER ENTRY. OIL DRAIN AND REFILL MAY BE NECESSARY. CONSULT Tin ppm <2 <2 <2 <2 SERVICE PROVIDER FOR FURTHER RECOMMENDATIONS. TO CONFIRM, Titanium ppm 0 0 0 0 Report Results: 25 ppm Lead, 20 ppm Tin RESAMPLE AT 5,000 MILES (8,000 KM) OR 100 HOURS. Vanadium ppm 1 0 0 0 Additives: Barium ppm 0 0 0 0 Time on Engine Time on Oil Alarm Diagnostic Statement Diagnostic statements Boron ppm 41 31 25 27 Calcium ppm 1524 1162 1508 1360 with maintenance Magnesium ppm 41 22 0 0 35,000 miles 15,000 miles NORMAL WEAR METALS DETECTED FOR BREAK-IN OR OVERHAUL PERIOD recommendations Phosphorus ppm 744 663 814 756 Zinc ppm 1004 779 1243 877 375,000 miles 15,000 miles ABNORMAL BEARING WEAR DETECTED Additional Tests: Fuel Dilution % 0.7 1.0 4.8 4.5 Total Acid Number mg KOH/g 5.0 3.0 6.0 6.2 375,000 miles 5,000 miles SEVERE BEARING WEAR DETECTED Legend Total Ferrous ppm 250.0 200.0 925.0 920.0 ABNORMAL SEVERE X = NOT TESTED / - = NOT DETECTED Water % 2.0 0.0 3.0 3.2 NOT APPLICABLE
NA = NOT C = CALCULATED M = MEASURED AVAILABLE Results from external devices Given the same results for wear metals but varying the time on the component and oil, the resulting diagnostic statements will be different.
| | 366 | Fleet Product Solutions Catalog ProductFleet SCatalogolutions | 37 7 Converting Oil Reports into Fleet Decisions
LubeTrak™ Data Management Software
LubeTrak compiles individual oil reports into a consolidated database of historical information. This allows fleet managers to view and manage the oil analysis results across the entire fleet. This fleet-level view can be used to assess the health of the entire fleet to optimize maintenance program and practices. LubeTrak’s web-based, subscription data management system provides pre-configured reports and the option to custom-design reports. LubeTrak offers companies an on-line reporting solution to view, track, trend and share oil analysis results throughout your organization. The dashboard graphics provide an equipment overview, consolidates the latest results, and shows ‘red-flag’ problems. Data from MicroLab and CoolCheck instruments can be uploaded to LubeTrak. COMPLETE SAMPLE HISTORY IN ONE PLACE CUSTOMIZABLE Dashboard summary data for quick assessments Email alerts Sort by date, equipment type, condition (severity) or site Customized reports Fleet and Enterprise Solutions Mobile access Oil analysis with the MicroLab can help fleets to achieve an effective maintenance program which plays a critical role in asset management goals to: Optimize the lifecycle of the vehicles Minimize equipment downtime Control the costs of replacement parts and service Ensure the safety of the equipment and operators MicroLab Network Solution
Network solutions for multi-site fleets
When a fleet is managing assets across multiple sites, it is important to have an overall view of the entire maintenance program. Some fleets also may have vehicles that access any of their service locations; in those cases it is important that the vehicle’s oil analysis history is accessible regardless of which site they visit. Our network solutions allow multiple MicroLabs to be connected via a central server and LubeTrak to provide fleets the ability to: CENTRAL SERVER Generate reports locally at each site Synchronize assets and oil history across all sites Upload data from all sites to compare maintenance activities and issues across locations These network solutions are customized to meet the needs and SITE 1 SITE 3 configurations of many types of fleets to ensure information on the entire fleet is available whenever and wherever it is needed. SITE 2
| | 388 | Fleet Product Solutions Catalog Fleet Solutions 9 Converting Oil Reports into Fleet Decisions
LubeTrak™ Data Management Software
LubeTrak compiles individual oil reports into a consolidated database of historical information. This allows fleet managers to view and manage the oil analysis results across the entire fleet. This fleet-level view can be used to assess the health of the entire fleet to optimize maintenance program and practices. LubeTrak’s web-based, subscription data management system provides pre-configured reports and the option to custom-design reports. LubeTrak offers companies an on-line reporting solution to view, track, trend and share oil analysis results throughout your organization. The dashboard graphics provide an equipment overview, consolidates the latest results, and shows FLEET MAINTENANCE SOLUTIONS ‘red-flag’ problems. Data from MicroLab and CoolCheck instruments can be uploaded to LubeTrak. COMPLETE SAMPLE HISTORY IN ONE PLACE CUSTOMIZABLE Dashboard summary data for quick assessments Email alerts Sort by date, equipment type, condition (severity) or site Customized reports Fleet and Enterprise Solutions Mobile access Oil analysis with the MicroLab can help fleets to achieve an effective maintenance program which plays a critical role in asset management goals to: Optimize the lifecycle of the vehicles Minimize equipment downtime Control the costs of replacement parts and service Ensure the safety of the equipment and operators MicroLab Network Solution
Network solutions for multi-site fleets
When a fleet is managing assets across multiple sites, it is important to have an overall view of the entire maintenance program. Some fleets also may have vehicles that access any of their service locations; in those cases it is important that the vehicle’s oil analysis history is accessible regardless of which site they visit. Our network solutions allow multiple MicroLabs to be connected via a central server and LubeTrak to provide fleets the ability to: CENTRAL SERVER Generate reports locally at each site Synchronize assets and oil history across all sites Upload data from all sites to compare maintenance activities and issues across locations These network solutions are customized to meet the needs and SITE 1 SITE 3 configurations of many types of fleets to ensure information on the entire fleet is available whenever and wherever it is needed. SITE 2
| | 388 | Fleet Product Solutions Catalog ProductFleet SCatalogolutions | 39 9 MICROLAB COMPANION TOOLS
The MicroLab is truly an all-in-one solution designed to provide a complete oil analysis with one sample, however, for some specific situations an additional instrument may provide more information as a step two analysis. There are three companion products that fleets might consider depending on their needs. The MicroLab can screen for fuel dilution through a drop in viscosity, however, if a specific fuel dilution amount is needed then the Fuel Dilution Meter can be added to the analysis. CoolCheck 2 The MicroLab detects iron wear particles below 10µm, however, when larger iron wear particles need to be detected such as AUTOMATED COOLANT AND DIESEL EXHAUST FLUIDS in transmissions and gearboxes the FerroCheck can be added. ANALYSIS SYSTEM The MicroLab can detect contamination from a coolant leak but it cannot be used to test coolants. The CoolCheck 2 provides analysis on coolant condition as well as DEF purity. Results from external devices for fuel dilution, TAN, water and total ferrous can be manually entered to consolidate data into Coolant Analyzer the MicroLab report. Cooling systems play a vital role in preserving the overall engine heat balance and in protecting engine components against corrosion and other problems. CoolCheck offers an easy and fast way to test a fleet’s coolant to ensure optimum performance of the cooling system by identifying the most common problems such as, mixed fluid types, depletion of key performance additives and system contamination. FDM 6000 Series Testing coolant and maintaining systems at optimum levels will help prevent corrosion, overheating, engine seize up, and engine damage from freezing. AUTOMATED FUEL DILUTION METER The automated analyzer performs 8 different tests in less than a minute with a simple user Fuel dilution in lubrication oil can cause serious engine damage. In diesel engine crankcases, interface designed to be run by non-laboratory personnel. for example, fuel contamination can be caused by excessive idling, defective injectors or loose The CoolCheck confirms: connections. Glycol% The Fuel Dilution Meter 6000 Series detects fuel contamination in minutes which allows for Boil point and freeze point rapid maintenance actions. The device requires just a small sample size in a disposable vial. In Nitrites addition, the touchscreen and audio prompts guide the operator through the testing process Coolant type making it simple for any operator to use. Color Result in % fuel (0.2 to 15%) Contamination and clarity Small sample required in disposable vial – no solvents needed for cleaning Test results within a minute for direct measurement of fuel dilution. Diesel Exhaust Fluid (DEF) Analyzer Normal Sample – As an added benefit, CoolCheck tests All readings within acceptable range FerroCheck 2000 Series for correct DEF levels. An incorrect AUTOMATED FERROUS WEAR ANALYZER DEF mixture can reduce engine efficiency and negate emission Magnetic wear metal measurement in lubricants can be useful in determining the condition reduction systems. of the gearbox itself. Oil analysis can be used to determine wear conditions in the gears or The CoolCheck DEF test confirms bearings so corrective actions can be taken to prevent premature failures. % urea and total % DEF. Quick and easy measurements with a lightweight, battery operated system make the CoolCheck reports can be uploaded to LubeTrak FerroCheck 2000 Series an essential tool for measurements in the field. Highly repeatable (3 ppm) Abnormal Sample – Reports 0-10,000 ppm iron concentrations Freeze Point, Glycol Content and Boil Point all Rapid response (30 seconds) below acceptable range – additives depleted Small sample requirement (2 ml) No sample prep or solvents required
| | 4010 | ProductFleet Solutions Catalog Fleet Solutions 11 MICROLAB COMPANION TOOLS
The MicroLab is truly an all-in-one solution designed to provide a complete oil analysis with one sample, however, for some specific situations an additional instrument may provide more information as a step two analysis. There are three companion products that fleets might consider depending on their needs. The MicroLab can screen for fuel dilution through a drop in viscosity, however, if a specific fuel dilution amount is needed then the Fuel Dilution Meter can be added to the analysis. CoolCheck 2 The MicroLab detects iron wear particles below 10µm, however, when larger iron wear particles need to be detected such as AUTOMATED COOLANT AND DIESEL EXHAUST FLUIDS in transmissions and gearboxes the FerroCheck can be added. ANALYSIS SYSTEM The MicroLab can detect contamination from a coolant leak but it cannot be used to test coolants. The CoolCheck 2 provides analysis on coolant condition as well as DEF purity. Results from external devices for fuel dilution, TAN, water and total ferrous can be manually entered to consolidate data into Coolant Analyzer FLEET MAINTENANCE SOLUTIONS the MicroLab report. Cooling systems play a vital role in preserving the overall engine heat balance and in protecting engine components against corrosion and other problems. CoolCheck offers an easy and fast way to test a fleet’s coolant to ensure optimum performance of the cooling system by identifying the most common problems such as, mixed fluid types, depletion of key performance additives and system contamination. FDM 6000 Series Testing coolant and maintaining systems at optimum levels will help prevent corrosion, overheating, engine seize up, and engine damage from freezing. AUTOMATED FUEL DILUTION METER The automated analyzer performs 8 different tests in less than a minute with a simple user Fuel dilution in lubrication oil can cause serious engine damage. In diesel engine crankcases, interface designed to be run by non-laboratory personnel. for example, fuel contamination can be caused by excessive idling, defective injectors or loose The CoolCheck confirms: connections. Glycol% The Fuel Dilution Meter 6000 Series detects fuel contamination in minutes which allows for Boil point and freeze point rapid maintenance actions. The device requires just a small sample size in a disposable vial. In Nitrites addition, the touchscreen and audio prompts guide the operator through the testing process Coolant type making it simple for any operator to use. Color Result in % fuel (0.2 to 15%) Contamination and clarity Small sample required in disposable vial – no solvents needed for cleaning Test results within a minute for direct measurement of fuel dilution. Diesel Exhaust Fluid (DEF) Analyzer Normal Sample – As an added benefit, CoolCheck tests All readings within acceptable range FerroCheck 2000 Series for correct DEF levels. An incorrect AUTOMATED FERROUS WEAR ANALYZER DEF mixture can reduce engine efficiency and negate emission Magnetic wear metal measurement in lubricants can be useful in determining the condition reduction systems. of the gearbox itself. Oil analysis can be used to determine wear conditions in the gears or The CoolCheck DEF test confirms bearings so corrective actions can be taken to prevent premature failures. % urea and total % DEF. Quick and easy measurements with a lightweight, battery operated system make the CoolCheck reports can be uploaded to LubeTrak FerroCheck 2000 Series an essential tool for measurements in the field. Highly repeatable (3 ppm) Abnormal Sample – Reports 0-10,000 ppm iron concentrations Freeze Point, Glycol Content and Boil Point all Rapid response (30 seconds) below acceptable range – additives depleted Small sample requirement (2 ml) No sample prep or solvents required
| | 4010 | ProductFleet Solutions Catalog ProductFleet S olutionsCatalog | 4111 MicroLab Series Product Information
PART NUMBER PRODUCT INFORMATION 800-00033 (115v) MicroLab 30 Methodology Per ASTM D7417 800-00034 (230v) Requires 29837-00 Standard Accessory Kit Repeatability Per ASTM D7417 800-00043 (115v) MicroLab 30, extended metals. 800-00044 (230v) Requires 29838-00 Standard Accessory Kit OPERATIONAL SPECIFICATIONS 800-00035 (115v) MicroLab 40 Sample Volume 1-5 oz. depending on analyses performed 800-00036 (230v) Requires 29708-00 (115v) or 29847-00 (230v) Standard Required Accessory Kit Sample 5-15 minutes, depending on analyses selected COMPANION KITS Time Required 800-00103 (115v) MicroLab 31 Oil range specs Up to 680 cSt at 40C particle counter limited to 320cSt 800-00104 (230v) Includes: MicroLab 30, CoolCheck, 5YR LubeTrak License at 40C 800-00105 (115v) MicroLab 42 Calibration Standardization (analyzer metals detection) dependent 800-00106 (230v) Includes: MicroLab 40, FerroCheck, FDM6001, on application – typically required every 50 samples 5YR LubeTrak License (software-changeable) 800-00107 (115v) MicroLab 43 Ambient Operating 0° to 25° C 800-00108 (230v) Includes: MicroLab 40, FerroCheck, FDM6001, CoolCheck, Temperature 5YR LubeTrak License Operational Humidity 0-85% non-condensing ACCESSORIES & CONSUMABLES Ambient Altitude up to 3000 meters 29002-05-ABS 5 oz sample bottle w/cap (box of 300) USER INTERFACE SPECFICATIONS 29823-00 Long sipper straw (350 pcs) Computer OS Win10 32-bit; SQL server database 29824-00 Cleaning wipe for IR Cell (280 wipes) Display 15” (diag.) touchscreen 29033-00 Clean swabs packages (100 pcs) Data Entry Touchscreen / keyboard / USB port for computer mouse 29034-00 Sample Extraction Tubing (100 foot roll) Data Storage 512 GB hard drive; 23042-00 Upper Electrode 32 GB MSATA drive for database backups 23076-00 Lower Electrode Data Transfer FTP (for online reporting) 22194-00 Filter Screen, 1/2 Dia, #60 x 60 MESH, 304S Security AVG 2015 29088-01 Check Flush (One Gallon) Communication Network port 25 (email of reports) ; Port 21 (online reporting); Remote access software (LogMeIn) for 29087-01 Basic Metal Test Standard Fluid High (32 oz) - Blue support/training 29530-00 Extended Metal Low Test Standard (32 oz) LCS - Yellow POWER REQUIREMENTS 29531-00 Extended Metal High Test Standard (32 oz) HCS - Brown Power 115/230V 50/60 Hz (single-phase) – Spec. by part number (top) 29089-01 Low Viscosity Test Standard (32 oz) - Red Power Consumption 1100 Watts continuous; 1700 Watts instantaneous max. 29090-01 High Viscosity Test Standard (32 oz) - Green MECHANICAL SPECIFICATIONS Accessories Power conditioner/surge protector, universal cable kit, (Included with sample bottles (300), sample straws (1 box), Kimwipes Dimensions 29” (L) x 30” (W) x 26” (H) (74cm x 76cm x 66cm) instrument and (1 box), cleaning swabs (15 bags), waste bottle, sample Weight 130 lbs (59 kg) accessory kit) extractor and tubing, best practices poster, metals test standards, high and low viscosity standards, check flush COMPLIANCE (8 gal), wire brush, filter screens (25), remote drain port, allen wrenches CE Mark / RoHS
To keep your MicroLab running in top condition, it is important to use the recommended consumables including cleaning and standardization fluids. Spectro Scientific certified consumables are selected and carefully tested with all our instruments to ensure consistent, repeatable results. Always use Spectro Scientific supplied consumables for best results. CheckFlush is specially designed to clean the lines in the MicroLab between samples. This prevents cross-over contamination and keeps your instrument running its best.
Spectro Scientific | One Executive Drive, Suite 101, Chelmsford, MA 01824-2563 978-431-1120 | www.spectrosci.com | [email protected] | An ISO 9001:2008 company Copyright © 2017 Spectro Scientific. All rights reserved. While every effort is made to assure the information in this document is accurate, Spectro Scientific does not accept liability for any errors or mistakes that may arise. Specifications are subject to change without notice. Fleet_BRv2_2017-09-26 42 | Product Catalog MicroLab Series Product Information
PART NUMBER PRODUCT INFORMATION 800-00033 (115v) MicroLab 30 Methodology Per ASTM D7417 800-00034 (230v) Requires 29837-00 Standard Accessory Kit Repeatability Per ASTM D7417 800-00043 (115v) MicroLab 30, extended metals. OPERATIONAL SPECIFICATIONS Portable Oil Analysis Tools 800-00044 (230v) Requires 29838-00 Standard Accessory Kit 800-00035 (115v) MicroLab 40 Sample Volume 1-5 oz. depending on analyses performed 800-00036 (230v) Requires 29708-00 (115v) or 29847-00 (230v) Standard Required Accessory Kit Sample 5-15 minutes, depending on analyses selected COMPANION KITS Time Required 800-00103 (115v) MicroLab 31 Oil range specs Up to 680 cSt at 40C particle counter limited to 320cSt 800-00104 (230v) Includes: MicroLab 30, CoolCheck, 5YR LubeTrak License at 40C 800-00105 (115v) MicroLab 42 Calibration Standardization (analyzer metals detection) dependent 800-00106 (230v) Includes: MicroLab 40, FerroCheck, FDM6001, on application – typically required every 50 samples 5YR LubeTrak License (software-changeable) 800-00107 (115v) MicroLab 43 Ambient Operating 0° to 25° C 800-00108 (230v) Includes: MicroLab 40, FerroCheck, FDM6001, CoolCheck, Temperature 5YR LubeTrak License Operational Humidity 0-85% non-condensing ACCESSORIES & CONSUMABLES Ambient Altitude up to 3000 meters 29002-05-ABS 5 oz sample bottle w/cap (box of 300) USER INTERFACE SPECFICATIONS 29823-00 Long sipper straw (350 pcs) Computer OS Win10 32-bit; SQL server database 29824-00 Cleaning wipe for IR Cell (280 wipes) Display 15” (diag.) touchscreen 29033-00 Clean swabs packages (100 pcs) Data Entry Touchscreen / keyboard / USB port for computer mouse 29034-00 Sample Extraction Tubing (100 foot roll) Data Storage 512 GB hard drive; 23042-00 Upper Electrode 32 GB MSATA drive for database backups 23076-00 Lower Electrode Data Transfer FTP (for online reporting) 22194-00 Filter Screen, 1/2 Dia, #60 x 60 MESH, 304S Security AVG 2015 29088-01 Check Flush (One Gallon) Communication Network port 25 (email of reports) ; Port 21 (online reporting); Remote access software (LogMeIn) for 29087-01 Basic Metal Test Standard Fluid High (32 oz) - Blue support/training 29530-00 Extended Metal Low Test Standard (32 oz) LCS - Yellow POWER REQUIREMENTS 29531-00 Extended Metal High Test Standard (32 oz) HCS - Brown Power 115/230V 50/60 Hz (single-phase) – Spec. by part number (top) 29089-01 Low Viscosity Test Standard (32 oz) - Red Power Consumption 1100 Watts continuous; 1700 Watts instantaneous max. 29090-01 High Viscosity Test Standard (32 oz) - Green MECHANICAL SPECIFICATIONS Accessories Power conditioner/surge protector, universal cable kit, (Included with sample bottles (300), sample straws (1 box), Kimwipes Dimensions 29” (L) x 30” (W) x 26” (H) (74cm x 76cm x 66cm) instrument and (1 box), cleaning swabs (15 bags), waste bottle, sample Weight 130 lbs (59 kg) accessory kit) extractor and tubing, best practices poster, metals test standards, high and low viscosity standards, check flush COMPLIANCE (8 gal), wire brush, filter screens (25), remote drain port, allen wrenches CE Mark / RoHS
To keep your MicroLab running in top condition, it is important to use the recommended consumables including cleaning and standardization fluids. Spectro Scientific certified consumables are selected and carefully tested with all our instruments to ensure consistent, repeatable results. Always use Spectro Scientific supplied consumables for best results. CheckFlush is specially designed to clean the lines in the MicroLab between samples. This prevents cross-over contamination and keeps your instrument running its best.
Spectro Scientific | One Executive Drive, Suite 101, Chelmsford, MA 01824-2563 978-431-1120 | www.spectrosci.com | [email protected] | An ISO 9001:2008 company Copyright © 2017 Spectro Scientific. All rights reserved. While every effort is made to assure the information in this document is accurate, Spectro Scientific does not accept liability for any errors or mistakes that may arise. Specifications are subject to change without notice. Fleet_BRv2_2017-09-26 42 | Product Catalog Tools for Service Professionals
Conducting oil analysis in the field right next to the high value assets provides unparalleled advantage to reliability professionals and military personals to assess the condition of the assets in real time . Spectro Scientific offers a wide range of portable devices with field simplicity and lab accuracy . The product combinations are powerful for different applications as together they provide more comprehensive analysis of oil condition, contamination and machine FieldLab 58 wear condition . All Spectro portable devices are battery powered, use small amounts of oil, and do not require solvents or chemicals to clean and fully in compliance to ASTM standards . They EXPEDITIONARY FLUID ANALYSIS SYSTEM are light weighted and ideal for field use . Different combinations are recommended based on the type of asset (engines vs rotating machines such as gear boxes, transmissions, or compressors), and users . Even though devices can be purchased, there are three essential combinations and applications .
FieldLab 58 is a battery-powered, integrated oil analysis system COMBINATION KIT DEVICES APPLICATIONS Owners of critical assets in the that provides quick and comprehensive oil analysis in the field. military, mining and marine industries Basic Oil Analysis Kit MiniVisc, FerroCheck Used by OEM and service professional for basic need immediate information about Military and commercial field service professionals managing fleets of high-value assets oil condition and machine wear condition check in oil and equipment condition. The require portable, lightweight devices that provide rapid oil analysis results with quality various industries . portable FieldLab 58 oil analyzer similar to oil analysis labs. Funded by the United States Department of Defense (DoD) eliminates the wait for lab results, in 2009, then developed and commercialized by Spectro Scientific, the FieldLab 58 so you won’t miss early signs of Expeditionary Fluid Analysis System (EFAS) was designed. contamination or abnormal wear. The FieldLab 58 integrated system requires only a few milliliters of oil to complete four Key applications include: comprehensive tests to help maintain readiness of critical assets while economically Oil Condition Kit MiniVisc, FluidScan Primary for engine oil condition checking . Great In-service oil analysis for engines, managing maintenance costs. for marine, aerospace, railway and transportation gearboxes, hydraulics and turbines industries – Comprehensive oil analysis Key Features report Grease analysis for bearings, Rugged design with battery power for couplings and motor operated on-site field use valves No solvents or chemicals required – Wear metals – Oxidation Complete oil analysis lab with 4 technologies MiniLab 33 MiniVisc, FluidScan, FerroCheck Basic Trivector MiniLab for small and mid-size integrated into a small case industrial plant or power plant to start an on-site oil – Water (trending only) – X-Ray Florescence (XRF) spectrometer analysis program for elemental analysis – Filter Particle Quantifier (FPQ) pore blockage particle counter – Infrared (IR) spectrometer – Kinematic viscometer (40°C) Portable Oil Analysis Lab FieldLab 58 A battery powered lab in a suitcase that provides 4 tests generate more than 20 oil analysis elemental analysis, particle count, viscosity and oil parameters in 5 to 7 minutes condition . It is fully in compliance to ASTM standards and designed for Military personals and reliability Built-in controller for measurement, data, professionals to conduct oil analysis next to the high and asset with touch screen interface value assets Uses only 3 ml of oil
ASTM compliant
44 | Product Catalog FieldLab 58 EXPEDITIONARY FLUID ANALYSIS SYSTEM
FieldLab 58 is a battery-powered, integrated oil analysis system Owners of critical assets in the that provides quick and comprehensive oil analysis in the field. military, mining and marine industries need immediate information about Military and commercial field service professionals managing fleets of high-value assets oil and equipment condition. The require portable, lightweight devices that provide rapid oil analysis results with quality portable FieldLab 58 oil analyzer similar to oil analysis labs. Funded by the United States Department of Defense (DoD) ANALYSIS OIL PORTABLE TOOLS eliminates the wait for lab results, in 2009, then developed and commercialized by Spectro Scientific, the FieldLab 58 so you won’t miss early signs of Expeditionary Fluid Analysis System (EFAS) was designed. contamination or abnormal wear. The FieldLab 58 integrated system requires only a few milliliters of oil to complete four Key applications include: comprehensive tests to help maintain readiness of critical assets while economically In-service oil analysis for engines, managing maintenance costs. gearboxes, hydraulics and turbines – Comprehensive oil analysis Key Features report Grease analysis for bearings, Rugged design with battery power for couplings and motor operated on-site field use valves No solvents or chemicals required – Wear metals – Oxidation Complete oil analysis lab with 4 technologies – Water (trending only) integrated into a small case – X-Ray Florescence (XRF) spectrometer for elemental analysis – Filter Particle Quantifier (FPQ) pore blockage particle counter – Infrared (IR) spectrometer – Kinematic viscometer (40°C) 4 tests generate more than 20 oil analysis parameters in 5 to 7 minutes Built-in controller for measurement, data, and asset with touch screen interface Uses only 3 ml of oil ASTM compliant
44 | Product Catalog Product Catalog | 45 FieldLab 58 PRINCIPLES OF OPERATION Complete in-service oil analysis lab in the field Particle count and elemental analysis — ASTM D8127 Particle counts are generated using our patented FPQ pore blockage particle counter (ISO 21018-3). It captures the particles KEY PARAMETERS of interest for severe wear detection onto a unique filtergram. This debris may now be measured on the companion XRF MACHINE WEAR spectrometer for immediate results in ppm for 13 elements. – 13 elements for particles > 5 µm (Si, Al, Cr, Ti, Fe, Ni, Pb, Cu Sn, Mo,Ag, Zn, V) Wear and contamination particles larger than 4 microns deposit on the filtergram, and are tested using an X-Ray Florescence CONTAMINATION (XRF) spectrometer. The concentration (in ppm) for thirteen – Particle count, ISO codes different elements is reported. – Water, glycol, soot The filtergram coupon can be stored for future analysis, such as OIL CONDITION microscopic wear debris analysis of particle colors and shapes. – Oxidation, nitration, sulfation, TAN, TBN – Viscosity @40°C, calculated viscosity @100°C Oil Insertion Particles Filtergram
Link with LIMS software Fluid chemistry and contamination — ASTM D7889 Connects directly to the cloud-based SpectroTrack LIMS The IR spectrometer measures the chemistry of the lubricant and contamination in one using the FluidManager software minute using only one drop of oil; no chemicals or solvents are required. It combines ease Data transfer with the push of button of use, ruggedness and laboratory precision in a small package, which is ideal for field use. Fleet level oil analysis tracked and reported in SpectroTrack The oil condition parameters measured by FluidScan include oxidation, nitration, sulfation, Email notifications, trending reports and asset management readily anti-wear additive, Total Base Number (TBN), glycol, soot, and water for engine oil; and oxidation, Total Acid Number, and water for rotating machine lubricants such as gear oil, available to reliability managers transmission oil and hydraulic oil. FieldLab 58 data can also be imported into AMS OilView™ software
Viscosity — ASTM D8092 Viscosity is measured using a temperature-controlled kinematic viscometer with a patented split-cell design. A funnel, with a 100 micron gap, is formed in the center of the cell. Optical sensors in the cell detect the flow of oil under the influence of gravity. The time it takes the oil to flow through the cell is proportional to the
viscosity of the oil. When open, the cells can be cleaned Kinematic Viscosity (40C) = A* (t1-t0) + B using a non-abrasive wipe. No solvents are required. *A and B are calibration coefficients
46 | ProductSpe tro Catalog Track INFORMATION MANAGEMENT S STEM FieldLab 58 PRINCIPLES OF OPERATION Complete in-service oil analysis lab in the field Particle count and elemental analysis — ASTM D8127 Particle counts are generated using our patented FPQ pore blockage particle counter (ISO 21018-3). It captures the particles KEY PARAMETERS of interest for severe wear detection onto a unique filtergram. This debris may now be measured on the companion XRF MACHINE WEAR spectrometer for immediate results in ppm for 13 elements. – 13 elements for particles > 5 µm (Si, Al, Cr, Ti, Fe, Ni, Pb, Cu Sn, Mo,Ag, Zn, V) Wear and contamination particles larger than 4 microns deposit on the filtergram, and are tested using an X-Ray Florescence CONTAMINATION (XRF) spectrometer. The concentration (in ppm) for thirteen – Particle count, ISO codes different elements is reported. – Water, glycol, soot The filtergram coupon can be stored for future analysis, such as OIL CONDITION microscopic wear debris analysis of particle colors and shapes. – Oxidation, nitration, sulfation, TAN, TBN – Viscosity @40°C, calculated viscosity @100°C Oil Insertion Particles Filtergram
Link with LIMS software ANALYSIS OIL PORTABLE TOOLS Fluid chemistry and contamination — ASTM D7889 Connects directly to the cloud-based SpectroTrack LIMS The IR spectrometer measures the chemistry of the lubricant and contamination in one using the FluidManager software minute using only one drop of oil; no chemicals or solvents are required. It combines ease Data transfer with the push of button of use, ruggedness and laboratory precision in a small package, which is ideal for field use. Fleet level oil analysis tracked and reported in SpectroTrack The oil condition parameters measured by FluidScan include oxidation, nitration, sulfation, Email notifications, trending reports and asset management readily anti-wear additive, Total Base Number (TBN), glycol, soot, and water for engine oil; and oxidation, Total Acid Number, and water for rotating machine lubricants such as gear oil, available to reliability managers transmission oil and hydraulic oil. FieldLab 58 data can also be imported into AMS OilView™ software
Viscosity — ASTM D8092 Viscosity is measured using a temperature-controlled kinematic viscometer with a patented split-cell design. A funnel, with a 100 micron gap, is formed in the center of the cell. Optical sensors in the cell detect the flow of oil under the influence of gravity. The time it takes the oil to flow through the cell is proportional to the
viscosity of the oil. When open, the cells can be cleaned Kinematic Viscosity (40C) = A* (t1-t0) + B using a non-abrasive wipe. No solvents are required. *A and B are calibration coefficients
46 | ProductSpe tro Catalog Track Product Catalog | 47 INFORMATION MANAGEMENT S STEM FieldLab 58 Product Information
PRODUCT INFORMATION OUTPUTS Part Number 800-00094 Elemental Silicon (Si); Aluminum (Al); Chromium (Cr); Titanium Concentration (ppm) (Ti); Iron (Fe); Nickel (Ni); Lead (Pb); Copper (Cu); Applications Mineral and synthetic lubricants including gear, Tin (Sn); Molybdenum (Mo); Silver (Ag); Zinc (Zn); engines, transmissions, hydraulics, turbine as well as Vanadium (V) military, marine and mining applications In-service grease for industrial plants Fluid Chemistry TAN & TBN (mg KOH/g); Oxidation, Nitration, Sulfation (Abs/.1mm); Water (parts per million); ELEMENTAL MODULE Glycol (% by weight); Soot (% by weight); ® Detector 25 mm2 SDD detector; Peltier cooled Incorrect fluid (% by weight); Antioxidant Depletion (% remaining); Antiwear Depletion (% by weight) Resolution 122 eV FWHM resolution at 5.9 keV FluidScan 1000 Series Viscosity Kinematic viscosity @ 40C Excitation Source X-ray tube with Rhodium target; max voltage 50 kV Calculated viscosity @ 100C PORTABLE FLUID CONDITION MONITOR OPERATIONAL SPECIFICATIONS Particle Count Particle count #/ml (> 4 µm) Handheld, Solvent-free, Immediate Results Sample Volume 3 ml ISO Codes 4/6/14 Required (all tests) ISO codes >6 and >14 are extrapolated Sample Time Required Viscosity: 20 secs to 10 mins, dependent on grade Methodology ASTM D7889 (IR), ASTM D8092 (viscosity), ASTM D8127 (FPQ-XRF) Fluid Chemistry: less than 60 secs Rugged Direct Infrared Spectrometer Particle Count: 20 secs to 3 minutes, sample Calibration Factory, verification standards: NIST traceable dependent verification standards provided The FluidScan 1000 Series provides No moving parts, designed for handheld and field use applications High signal to noise ratio (>7000:1) to ensure high accuracy and repeatability XRF: 3-4 minutes CONSUMABLES quantitative measurement of a Ambient Operating 0° to 40°C P-11160 3 ml syringe (100 pack) lubricant’s condition and plays Easy to use Temperature an important role in predictive Needs just one drop of oil and one minute to test PV1012 60 ml disposable pipettes & non-abrasive cleaning maintenance. Using the device, Operational Humidity RH< 80% non-condensing pad kit (100 pack) No solvents required to clean you can eliminate unnecessary oil Ambient Altitude Up to 5,000 meters (16,404 feet) Color-coded, user adjustable alarm limits 34683143 FPQ waste container (3 pack) changes or service by testing not USER INTERFACE SPECIFICATIONS 34682166 FieldLab 58 verification standards (6 bottles) just servicing the oil. Determine when in service oil is no longer fit for Instrument OS SQL database on Windows CE FL310 IR Check Fluid 5 ml use due to liquid contamination or degradation Applications include: Direct immediate measurement of water, TAN and Display Fixed-angle 7” color touch screen display 0090-00022 FPQ filtergrams (50 pack) • Mineral and synthetic oxidation for lubricants used in gearboxes, turbines Data Storage Internal flash memory (SD card expansion) 000-00036 FPQ filtergrams – Grease (50 pack) oils used in gear boxes, engines, and hydraulic systems Data Transfer Ethernet, mini USB OPTIONAL ACCESSORIES transmissions Also measures TBN, water, glycol, soot, additive • Hydraulic systems, turbines and Data Entry Touch screen, FluidManager desktop software 600-00116 XRF calibration standard set depletion and oxidation for engine oil (asset loading and synchronization) other machinery components POWER REQUIREMENTS • Biodiesel/Fuel Highly repeatable and reproducible results ASTM D7889 Compliant – “Standard Test Method Battery Power Source Lithium-ion battery pack • Quality assurance of new oils for Field Determination of In-service Fluid Properties Charge Power 120/240 Vac, 50/60 Hz, 10 watts Using IR Spectroscopy” Typical Runtime 4-6 hours High correlation to KF water, TAN and TBN Recharge Time 2.5 hours FluidScan FluidScan laboratory tests MECHANICAL SPECIFICATIONS 1000 1100 Reproducibility and repeatability comparable to Dimensions 48 cm (L) x 39 cm (W) x 23 cm (H); 19.2” x 15.2” x 9” Color Yellow Blue benchtop FTIR method ASTM E2412 Weight 16.5 kg (36.4 lbs); Default One free library Industrial Data analysis compliant to ASTM E1655 20 kg (44.4 lbs with backpack and power supply) library from FL364 to Comprehensive Fluid Library FL371 at time COMPLIANCE of purchase Over 700 fluids for immediate, out-of-the-box operation CENELEC EN 60610-1:2010 Upgradable Yes Yes Results for critical properties such as TAN and water EN 61010-2-030 to full library contamination for industrial lubricants or TBN, water, CENEIEC EN 61326-2-1 Total water Optional Optional glycol and soot for engine oils FieldLab 58 consumables and standards MIL-STD 461 EMI license Easy dissolved water & free water measurement MIL-PRF 28800F Class II Drop Test Route base No Yes For both dissolved and free water using analysis homogenization technique OilView No Yes Interface Solvent free alternative to Karl Fischer titration Patented total water algorithm for both dissolved and Intended Fleet, marine, Industrial Spectro Scientific | One Executive Drive, Suite 101, Chelmsford, MA 01824-2563 application military, manufacturing free water 978-431-1120 | www.spectrosci.com | [email protected] | An ISO 9001:2008 company aerospace, plants, power Ideal for turbine oil, hydraulic fluids, and rotating Copyright © 2017 Spectro Scientific. All rights reserved. While every effort is made to assure the information in this document is accurate, fuel QC plants Spectro Scientific does not accept liability for any errors or mistakes that may arise. Specifications are subject to change without notice. machinery oils such as gear oil and compressor oil FieldLab 58_DSv4_2017-10-19 48 | Product Catalog FieldLab 58 Product Information
PRODUCT INFORMATION OUTPUTS Part Number 800-00094 Elemental Silicon (Si); Aluminum (Al); Chromium (Cr); Titanium Concentration (ppm) (Ti); Iron (Fe); Nickel (Ni); Lead (Pb); Copper (Cu); Applications Mineral and synthetic lubricants including gear, Tin (Sn); Molybdenum (Mo); Silver (Ag); Zinc (Zn); engines, transmissions, hydraulics, turbine as well as Vanadium (V) military, marine and mining applications In-service grease for industrial plants Fluid Chemistry TAN & TBN (mg KOH/g); Oxidation, Nitration, Sulfation (Abs/.1mm); Water (parts per million); ELEMENTAL MODULE Glycol (% by weight); Soot (% by weight); ® Detector 25 mm2 SDD detector; Peltier cooled Incorrect fluid (% by weight); Antioxidant Depletion (% remaining); Antiwear Depletion (% by weight) Resolution 122 eV FWHM resolution at 5.9 keV FluidScan 1000 Series Viscosity Kinematic viscosity @ 40C Excitation Source X-ray tube with Rhodium target; max voltage 50 kV Calculated viscosity @ 100C PORTABLE FLUID CONDITION MONITOR OPERATIONAL SPECIFICATIONS Particle Count Particle count #/ml (> 4 µm) Handheld, Solvent-free, Immediate Results Sample Volume 3 ml ISO Codes 4/6/14 Required (all tests) ISO codes >6 and >14 are extrapolated Sample Time Required Viscosity: 20 secs to 10 mins, dependent on grade Methodology ASTM D7889 (IR), ASTM D8092 (viscosity), ASTM D8127 (FPQ-XRF) Fluid Chemistry: less than 60 secs Rugged Direct Infrared Spectrometer Particle Count: 20 secs to 3 minutes, sample Calibration Factory, verification standards: NIST traceable dependent verification standards provided The FluidScan 1000 Series provides No moving parts, designed for handheld and field use applications High signal to noise ratio (>7000:1) to ensure high accuracy and repeatability XRF: 3-4 minutes CONSUMABLES quantitative measurement of a Ambient Operating 0° to 40°C P-11160 3 ml syringe (100 pack) lubricant’s condition and plays Easy to use Temperature an important role in predictive Needs just one drop of oil and one minute to test PV1012 60 ml disposable pipettes & non-abrasive cleaning maintenance. Using the device, Operational Humidity RH< 80% non-condensing pad kit (100 pack) No solvents required to clean you can eliminate unnecessary oil
Ambient Altitude Up to 5,000 meters (16,404 feet) Color-coded, user adjustable alarm limits ANALYSIS OIL PORTABLE TOOLS 34683143 FPQ waste container (3 pack) changes or service by testing not USER INTERFACE SPECIFICATIONS 34682166 FieldLab 58 verification standards (6 bottles) just servicing the oil. Determine when in service oil is no longer fit for Instrument OS SQL database on Windows CE FL310 IR Check Fluid 5 ml use due to liquid contamination or degradation Applications include: Direct immediate measurement of water, TAN and Display Fixed-angle 7” color touch screen display 0090-00022 FPQ filtergrams (50 pack) • Mineral and synthetic oxidation for lubricants used in gearboxes, turbines Data Storage Internal flash memory (SD card expansion) 000-00036 FPQ filtergrams – Grease (50 pack) oils used in gear boxes, engines, and hydraulic systems Data Transfer Ethernet, mini USB OPTIONAL ACCESSORIES transmissions Also measures TBN, water, glycol, soot, additive • Hydraulic systems, turbines and Data Entry Touch screen, FluidManager desktop software 600-00116 XRF calibration standard set depletion and oxidation for engine oil (asset loading and synchronization) other machinery components POWER REQUIREMENTS • Biodiesel/Fuel Highly repeatable and reproducible results ASTM D7889 Compliant – “Standard Test Method Battery Power Source Lithium-ion battery pack • Quality assurance of new oils for Field Determination of In-service Fluid Properties Charge Power 120/240 Vac, 50/60 Hz, 10 watts Using IR Spectroscopy” Typical Runtime 4-6 hours High correlation to KF water, TAN and TBN Recharge Time 2.5 hours FluidScan FluidScan laboratory tests MECHANICAL SPECIFICATIONS 1000 1100 Reproducibility and repeatability comparable to Dimensions 48 cm (L) x 39 cm (W) x 23 cm (H); 19.2” x 15.2” x 9” Color Yellow Blue benchtop FTIR method ASTM E2412 Weight 16.5 kg (36.4 lbs); Default One free library Industrial Data analysis compliant to ASTM E1655 20 kg (44.4 lbs with backpack and power supply) library from FL364 to Comprehensive Fluid Library FL371 at time COMPLIANCE of purchase Over 700 fluids for immediate, out-of-the-box operation CENELEC EN 60610-1:2010 Upgradable Yes Yes Results for critical properties such as TAN and water EN 61010-2-030 to full library contamination for industrial lubricants or TBN, water, CENEIEC EN 61326-2-1 Total water Optional Optional glycol and soot for engine oils FieldLab 58 consumables and standards MIL-STD 461 EMI license Easy dissolved water & free water measurement MIL-PRF 28800F Class II Drop Test Route base No Yes For both dissolved and free water using analysis homogenization technique OilView No Yes Interface Solvent free alternative to Karl Fischer titration Patented total water algorithm for both dissolved and Intended Fleet, marine, Industrial Spectro Scientific | One Executive Drive, Suite 101, Chelmsford, MA 01824-2563 application military, manufacturing free water 978-431-1120 | www.spectrosci.com | [email protected] | An ISO 9001:2008 company aerospace, plants, power Ideal for turbine oil, hydraulic fluids, and rotating Copyright © 2017 Spectro Scientific. All rights reserved. While every effort is made to assure the information in this document is accurate, fuel QC plants Spectro Scientific does not accept liability for any errors or mistakes that may arise. Specifications are subject to change without notice. machinery oils such as gear oil and compressor oil FieldLab 58_DSv4_2017-10-19 48 | Product Catalog Product Catalog | 49 Comparison of FluidScan ASTM D7889 and corresponding IR ASTM methods
OIL PROPERTY FLUIDSCAN IR IR ASTM Examples of fluid chemistry types REPEATABILITY REPEATABILITY included in the library
Oxidation (abs/0.1 mm) 0.2 0.68 D7414 ■ Mineral oil-based hydraulic, Nitration (abs/cm) 0.53 0.078 D7624 compression, transmission, turbine Sulfation (abs/0.1 mm) 0.31 0.3 D7415 and gear blends Antiwear Additive (abs/0.1 mm) 0.38 0.53 D7412 ■ Polyol Esters Soot (abs/cm) 0.43 0.9 D7844 ■ Phosphate Esters ■ Organic Esters Oil category and properties ■ Synthetic hydrocarbon-based hydraulic, compression, APPLICATION CATEGORIES PROPERTIES MEASURED BY FLUIDSCAN transmission, turbine and gear Transmission Water (ppm), Oxidation (Abs/0.1mm) blends Hydraulic – Fire resistant Water (ppm), TAN (mg KOH/g) (Phosphate Ester) ■ Ester-based Blends Hydraulic – Aerospace Water (ppm), Oxidation (Abs/0.1mm), Alien Fluid mineral based ■ Biodiesel (Synthetic Hydraulic Fluid) (MIL-H-2304) (%), and Alien Fluid engine oil (MIL-H-23699) (%) ■ Diesel Fuel Heat Transfer (Quenching Oil) Water (ppm), Oxidation (Abs/0.1mm) ■ Polyglycols Industrial Water (ppm), Oxidation (Abs/0.1mm), TAN (mg KOH/g) (Steam and CCGT Turbine, Hydraulic, ■ Polyalkylene Glycols Multivariate Calibrations Innovation in hardware and calibration compressor, Chiller, Gear, etc.) ■ Polyalphaolefins The FluidScan® classifies fluids into At the core of the FluidScan is a patented, mid-infrared spectrometer with grating optics Turbine Aerospace Water (ppm), TAN (mg KOH/g), Antioxidant (% depletion) (Synthetic Gas Turbine Oil) ■ Polyinternal Olefins groups called families based on and a linear detector array. The spectrometer collects the infrared light transmitted their chemical makeup, usage and Engines Water (ppm), Oxidation (Abs/0.1mm), TBN (mg KOH/g), Note: Fluid chemistry in the library is not through the fluid in the flip top cell into a waveguide. The waveguide then carries the spectral signature. The spectrum of (Engine oil for different engine types, TAN (mg KOH/g) (Natural Gas only), Sulfation (Abs/0.1mm), inclusive. Call Spectro Scientific support all fluids in each family changes in light to a prism-like diffraction grating that reflects the light into a high-performance including Gasoline, Diesel, Heavy Duty Nitration (Abs/cm), Soot (%), Glycol (%), Anti Wear (%) for more details before ordering. Diesel, HFO, Natural Gas, etc) a similar way with a given amount array detector which registers the infrared spectrum of the fluid. It provides more than of degradation or contamination. adequate spectral range, resolution and signal-to-noise ratio for the rapid analysis of Ethanol in Gasoline Ethanol (%) Family-specific algorithms are in-service lubricants. FAME in Diesel FAME (%) assigned that accurately quantify Biodiesel Feedstock Water (ppm), FFA % these amounts. These algorithms The FluidScan Applications Library includes over 700 oils and growing. Parameters for Fluid properties and corresponding yield quantitative results for the most the oils differ based on oil type so engine oil parameters are different from gear oils. Biodiesel Water (ppm), TAN (mg KOH/g), Total Glycerin (%) (compliance or correlation) methods critical properties of the most common Parameters such as water, TAN or TBN are calibrated according to ASTM methods used oil types. Multivariate calibrations are in common oil analysis labs with excellent correlation using multivariate calibration PROPERTY Fluid libraries and application categories included 1 applied so that quantitative readings methods. Fresh oils not in the library can be matched and added as user fluids, and Oxidation D7889 can be obtained, even with complex, Nitration D78891 contaminated samples. existing calibration can be applied to the user fluid with custom slope and offset P/N LIBRARY OIL CATEGORIES INCLUDED adjustments, if needed. FL364 Automotive Engine, Engine-Natural Gas, Hydraulic, Transmission Sulfation D78891 FL365 Aviation Compressor, Engine, Hydraulic, Hydraulic – Fire resistant, Hydraulic-Aero, AW Additive D78891 Turbine-Aero Soot D78891 2 FL366 Fuel QC Biodiesel, Biodiesel Feedstock, Ethanol in Gasoline, FAME in Diesel Gravimetric TBN D47392 FL367 Industrial Chiller, Compressor, Engine, Engine-Heavy Duty, Engine-Natural Gas, Gear- Pressure, Gear-Splash, Heat Transfer, Hydraulic, Hydraulic-Fire Resistant, TAN D6642 Slideway, Transmission, Turbine-Aero, Turbine-CCGT, Turbine-Steam Water D63042 FL368 Lab Trend ASTM Petroleum Engine, ASTM Polyol Ester (Turbine) Glycol Gravimetric2 FL369 Marine Chiller, Compressor, Engine, Engine-Heavy Duty, Engine-HFO, Gear-Pressure, Gear-Splash, Hydraulic, Transmission, Turbine-CCGT, Turbine-Steam Antioxidant E24122 Correlation with ASTM D6304 Gravimetric2 Correlation with ASTM D664 FL370 Military Chiller, Compressor, Engine, Engine-Heavy Duty, Engine-HFO, Gear-Pressure, Gear-Splash, Hydraulic-Fire Resistant, Hydraulic-Aero, Turbine-Aero Notes: 1. FluidScan complies with ASTM D7889 FL371 Railroad Compressor, Engine, Engine-Natural Gas, Hydraulic, Transmission 2. FluidScan correlates to ASTM method for TBN, A typical IR spectrum from FluidScan TAN correlation to titration Dissolved water correlation to Karl Fischer FL360 All Libraries All Categories of oils included TAN, Water, and gravimetric method for Glycol, antioxidant
50 | Product Catalog Comparison of FluidScan ASTM D7889 and corresponding IR ASTM methods
OIL PROPERTY FLUIDSCAN IR IR ASTM Examples of fluid chemistry types REPEATABILITY REPEATABILITY included in the library
Oxidation (abs/0.1 mm) 0.2 0.68 D7414 ■ Mineral oil-based hydraulic, Nitration (abs/cm) 0.53 0.078 D7624 compression, transmission, turbine Sulfation (abs/0.1 mm) 0.31 0.3 D7415 and gear blends Antiwear Additive (abs/0.1 mm) 0.38 0.53 D7412 ■ Polyol Esters Soot (abs/cm) 0.43 0.9 D7844 ■ Phosphate Esters ■ Organic Esters Oil category and properties ■ Synthetic hydrocarbon-based hydraulic, compression, APPLICATION CATEGORIES PROPERTIES MEASURED BY FLUIDSCAN transmission, turbine and gear Transmission Water (ppm), Oxidation (Abs/0.1mm) blends Hydraulic – Fire resistant Water (ppm), TAN (mg KOH/g) (Phosphate Ester) ■ Ester-based Blends Hydraulic – Aerospace Water (ppm), Oxidation (Abs/0.1mm), Alien Fluid mineral based ■ Biodiesel (Synthetic Hydraulic Fluid) (MIL-H-2304) (%), and Alien Fluid engine oil (MIL-H-23699) (%) ■ Diesel Fuel Heat Transfer (Quenching Oil) Water (ppm), Oxidation (Abs/0.1mm) ■ Polyglycols Industrial Water (ppm), Oxidation (Abs/0.1mm), TAN (mg KOH/g) PORTABLE OIL ANALYSIS OIL PORTABLE TOOLS (Steam and CCGT Turbine, Hydraulic, ■ Polyalkylene Glycols Multivariate Calibrations Innovation in hardware and calibration compressor, Chiller, Gear, etc.) ■ Polyalphaolefins The FluidScan® classifies fluids into At the core of the FluidScan is a patented, mid-infrared spectrometer with grating optics Turbine Aerospace Water (ppm), TAN (mg KOH/g), Antioxidant (% depletion) (Synthetic Gas Turbine Oil) ■ Polyinternal Olefins groups called families based on and a linear detector array. The spectrometer collects the infrared light transmitted their chemical makeup, usage and Engines Water (ppm), Oxidation (Abs/0.1mm), TBN (mg KOH/g), Note: Fluid chemistry in the library is not through the fluid in the flip top cell into a waveguide. The waveguide then carries the spectral signature. The spectrum of (Engine oil for different engine types, TAN (mg KOH/g) (Natural Gas only), Sulfation (Abs/0.1mm), inclusive. Call Spectro Scientific support all fluids in each family changes in light to a prism-like diffraction grating that reflects the light into a high-performance including Gasoline, Diesel, Heavy Duty Nitration (Abs/cm), Soot (%), Glycol (%), Anti Wear (%) for more details before ordering. Diesel, HFO, Natural Gas, etc) a similar way with a given amount array detector which registers the infrared spectrum of the fluid. It provides more than of degradation or contamination. adequate spectral range, resolution and signal-to-noise ratio for the rapid analysis of Ethanol in Gasoline Ethanol (%) Family-specific algorithms are in-service lubricants. FAME in Diesel FAME (%) assigned that accurately quantify Biodiesel Feedstock Water (ppm), FFA % these amounts. These algorithms The FluidScan Applications Library includes over 700 oils and growing. Parameters for Fluid properties and corresponding yield quantitative results for the most the oils differ based on oil type so engine oil parameters are different from gear oils. Biodiesel Water (ppm), TAN (mg KOH/g), Total Glycerin (%) (compliance or correlation) methods critical properties of the most common Parameters such as water, TAN or TBN are calibrated according to ASTM methods used oil types. Multivariate calibrations are in common oil analysis labs with excellent correlation using multivariate calibration PROPERTY Fluid libraries and application categories included 1 applied so that quantitative readings methods. Fresh oils not in the library can be matched and added as user fluids, and Oxidation D7889 can be obtained, even with complex, Nitration D78891 contaminated samples. existing calibration can be applied to the user fluid with custom slope and offset P/N LIBRARY OIL CATEGORIES INCLUDED adjustments, if needed. FL364 Automotive Engine, Engine-Natural Gas, Hydraulic, Transmission Sulfation D78891 FL365 Aviation Compressor, Engine, Hydraulic, Hydraulic – Fire resistant, Hydraulic-Aero, AW Additive D78891 Turbine-Aero Soot D78891 2 FL366 Fuel QC Biodiesel, Biodiesel Feedstock, Ethanol in Gasoline, FAME in Diesel Gravimetric TBN D47392 FL367 Industrial Chiller, Compressor, Engine, Engine-Heavy Duty, Engine-Natural Gas, Gear- Pressure, Gear-Splash, Heat Transfer, Hydraulic, Hydraulic-Fire Resistant, TAN D6642 Slideway, Transmission, Turbine-Aero, Turbine-CCGT, Turbine-Steam Water D63042 FL368 Lab Trend ASTM Petroleum Engine, ASTM Polyol Ester (Turbine) Glycol Gravimetric2 FL369 Marine Chiller, Compressor, Engine, Engine-Heavy Duty, Engine-HFO, Gear-Pressure, Gear-Splash, Hydraulic, Transmission, Turbine-CCGT, Turbine-Steam Antioxidant E24122 Correlation with ASTM D6304 Gravimetric2 Correlation with ASTM D664 FL370 Military Chiller, Compressor, Engine, Engine-Heavy Duty, Engine-HFO, Gear-Pressure, Gear-Splash, Hydraulic-Fire Resistant, Hydraulic-Aero, Turbine-Aero Notes: 1. FluidScan complies with ASTM D7889 FL371 Railroad Compressor, Engine, Engine-Natural Gas, Hydraulic, Transmission 2. FluidScan correlates to ASTM method for TBN, A typical IR spectrum from FluidScan TAN correlation to titration Dissolved water correlation to Karl Fischer FL360 All Libraries All Categories of oils included TAN, Water, and gravimetric method for Glycol, antioxidant
50 | Product Catalog Product Catalog | 51 FluidScan 1000 FluidScan 1100 & MiniVisc 3050 & MiniVisc 3050 FluidScan Series Product Information Combination Kit Combination Kit FluidScan can also be ordered in a combination kit with the MiniVisc 3050 portable viscometer. The battery-operated MiniVisc 3050 is a 40°C kinematic viscometer. It uses a few drops of oil to measure viscosity and does not require solvents to clean between samples.
PART NUMBER Ambient Operating 10°C to 50°C (14°F to 122°F) Temperature FluidScan 1000 FluidScan 1000 (requires SA1001 and Library license to operate) Relative Humidity 0 to 100%, non-condensing FerroCheck 2000 Series SA1001 FluidScan standard accessories Ambient Altitude up to 5,000 meters (16,404 feet) FERROUS METAL ANALYZER Spectro 1000/3050 FluidScan 1000 & MiniVisc 3050 Combination Kit USER INTERFACE SPECFICATIONS (requires SA1004 and Library license to operate) Solvent-free, simple to use, fast and accurate results Software/Operating Microsoft Windows® CE SA1004 Spectro Combination Kit standard accessories System SA1018 FluidScan 1000/1100 & 3050 Combination Kit Display 320 x 320 transflective color screen Standard Accessories Data Storage Up to 5,000 analyses FluidScan 1100 1100 FluidScan. Requires SA1001 Accessory Kit. Data Transfer USB for data updates and synchronization Spectro 1100/3050 FluidScan 1100 & MiniVisc 3050 Combination Kit. Accurate total ferrous measurement for in-service lubricants Data Entry Directional pad and soft buttons Requires SA1022 Accessory Kit. The FerroCheck 2000 Series enables Measure total ferrous content in Portable, battery-powered design POWER REQUIREMENTS SA1022 Spectro Combination Kit standard accessories fast and simple measurement of parts per million (ppm) by weight Lightweight and fits easily into a toolbox Battery Power Source Built in Rechargeable Lithium Ion Battery 400-00051 Comprehensive Water Solution with Portable the total ferrous wear content in Measures all ferrous material – or carrying bag; capable of operation for Homogenizer and license, 115 V, 60 Hz charger Power AC 110/240 V, 50/60 Hz, 10 Watts oils and grease for condition based normal machine wear and large over 4 hours before recharge. Unit plugs 400-00053 Comprehensive Water Solution with Portable Typical Runtime 6-8 hours maintenance of machinery and abnormal wear particles. in for continuous use. Homogenizer and license, 220 V, 50 Hz charger Recharge Time 6.5 hours engines. Highly accurate and repeatable ASTM compliance 400-00092 Comprehensive Water Solution with table top Wide range of measurement Homogenizer and license, 115 V, 60 Hz MECHANICAL SPECIFICATIONS Typical components trended for ASTM method D8120 “Standard Validation standards included 400-00093 Comprehensive Water Solution with table top Dimensions 24 cm (H) x 14 cm (W) x 7 cm (D) wear as part of a condition based Test Method for Ferrous Debris (9.5 in x 5.5 in x 2.75 in) Homogenizer and license, 220 V, 50 Hz maintenance program include: Easy to use Quantification” PRODUCT INFORMATION Weight 1.4 kg (3 lbs) Solvent-free operation and no sample ■ Gear boxes Shipping package 45.7 cm (H) x 40.6 cm (W) x 35.6 cm (L) preparation Application Library Mineral and synthetic lubricants including gear, engine, ■ Turbines transmission, hydraulics, turbine and biodiesels dimensions (18 in x 16 in x 14 in) Requires less than 2 ml of sample to test ■ Hydraulics Output TAN (mgKOH/g), TBN (mgKOH/g); Oxidation Shipping pkg weight 8.1 kg, (18 lbs) Results in 30 seconds ■ Transmissions (varies by fluid type (abs/0.1 mm); Nitration (abs/cm); Sulfation COMPLIANCE FerroCheck 2000 FerroCheck 2100 and application) (abs/0.1 mm); Water, ppm (dissolved, dissolved + free ■ Engines Expanded I/O capability water with Comprehensive Water Solution option); CE Mark: EMC Directive (2004/108/EC); RoHS ■ Pumps and compressors Automated data storage, export files Oil 0-10,000 ppm 0-10,000 ppm Glycol (% by weight); Soot (% by weight); Incorrect ™ ACCESSORIES & CONSUMABLES in CSV format or use AMS OilView Fluid (% by weight); Antioxidant Depletion (% Grease NA 0-15% remaining); Antiwear Depletion (% by weight). A475101 OilView LIMS software software interface Methodology ASTM D7889, ASTM E1655, E2412 modified FL310 IR Check Fluid 5 mL Standard Analytical Mid infrared range 950-3850 cm-1 PV1011 Disposable Non-Abrasive Cleaning Pads; pkg of 500 Range P-11052 60 µL Disposable Pipettes, package of 500 Accuracy ≤ ± 3% of measured value, typical PV1012 60 µL Disposable Pipettes & Non-Abrasive Cleaning Repeatability ≤ ± 6% of measured value, typical Pad Kit; package of 100 each SAMPLE VIAL Calibration Factory calibrated to wet chemistry methods ASTM FL360 Reference Fluid Application Library – all categories D664 for TAN and ASTM D4739 for TBN. Use Check Fluid for instrument validation. P-11178 Pipette tips for positive displacement pipette (used with MiniVisc 3050), package of 192 OPERATIONAL SPECIFICATIONS 450-00003 Tray Assembly and Charging Station, MEASUREMENT REFERENCE Sample Volume 100 μL (1 drop) 100-240 VAC, 50/60 Hz COIL COIL Principle of Operation Solvents/Reagents None The core of the FerroCheck 2000 is a pair of precision-rounded coils that when powered generate magnetic fields. When a small amount of in-service oil is inserted into one of the coils, Schematic of Coil Around Sample ferrous particles such as iron, nickel and cobalt interact with the magnetic field and introduce current changes in the coils. The amount of current change is proportional to the amount of | Spectro Scientific One Executive Drive, Suite 101, Chelmsford, MA 01824-2563 ferrous particles in the oil, calibrated in weight by parts per million (ppm). 978-431-1120 | www.spectrosci.com | [email protected] | An ISO 9001:2008 company Copyright © 2017 Spectro Scientific. All rights reserved. While every effort is made to assure the information in this document is accurate, Spectro Scientific does not accept liability for any errors or mistakes that may arise. Specifications are subject to change without notice. FluidScan Series_DSv5_2017-10-19 52 | Product Catalog FluidScan 1000 FluidScan 1100 & MiniVisc 3050 & MiniVisc 3050 FluidScan Series Product Information Combination Kit Combination Kit FluidScan can also be ordered in a combination kit with the MiniVisc 3050 portable viscometer. The battery-operated MiniVisc 3050 is a 40°C kinematic viscometer. It uses a few drops of oil to measure viscosity and does not require solvents to clean between samples.
PART NUMBER Ambient Operating 10°C to 50°C (14°F to 122°F) Temperature FluidScan 1000 FluidScan 1000 (requires SA1001 and Library license to operate) Relative Humidity 0 to 100%, non-condensing FerroCheck 2000 Series SA1001 FluidScan standard accessories Ambient Altitude up to 5,000 meters (16,404 feet) FERROUS METAL ANALYZER Spectro 1000/3050 FluidScan 1000 & MiniVisc 3050 Combination Kit USER INTERFACE SPECFICATIONS (requires SA1004 and Library license to operate) Solvent-free, simple to use, fast and accurate results Software/Operating Microsoft Windows® CE SA1004 Spectro Combination Kit standard accessories System SA1018 FluidScan 1000/1100 & 3050 Combination Kit Display 320 x 320 transflective color screen Standard Accessories Data Storage Up to 5,000 analyses FluidScan 1100 1100 FluidScan. Requires SA1001 Accessory Kit. Data Transfer USB for data updates and synchronization Spectro 1100/3050 FluidScan 1100 & MiniVisc 3050 Combination Kit. Accurate total ferrous measurement for in-service lubricants Data Entry Directional pad and soft buttons Requires SA1022 Accessory Kit. The FerroCheck 2000 Series enables Measure total ferrous content in Portable, battery-powered design POWER REQUIREMENTS SA1022 Spectro Combination Kit standard accessories fast and simple measurement of parts per million (ppm) by weight Lightweight and fits easily into a toolbox Battery Power Source Built in Rechargeable Lithium Ion Battery 400-00051 Comprehensive Water Solution with Portable the total ferrous wear content in Measures all ferrous material – or carrying bag; capable of operation for Homogenizer and license, 115 V, 60 Hz charger Power AC 110/240 V, 50/60 Hz, 10 Watts oils and grease for condition based normal machine wear and large over 4 hours before recharge. Unit plugs
400-00053 Comprehensive Water Solution with Portable Typical Runtime 6-8 hours maintenance of machinery and abnormal wear particles. in for continuous use. ANALYSIS OIL PORTABLE TOOLS Homogenizer and license, 220 V, 50 Hz charger Recharge Time 6.5 hours engines. Highly accurate and repeatable ASTM compliance 400-00092 Comprehensive Water Solution with table top Wide range of measurement Homogenizer and license, 115 V, 60 Hz MECHANICAL SPECIFICATIONS Typical components trended for ASTM method D8120 “Standard Validation standards included 400-00093 Comprehensive Water Solution with table top Dimensions 24 cm (H) x 14 cm (W) x 7 cm (D) wear as part of a condition based Test Method for Ferrous Debris (9.5 in x 5.5 in x 2.75 in) Homogenizer and license, 220 V, 50 Hz maintenance program include: Easy to use Quantification” PRODUCT INFORMATION Weight 1.4 kg (3 lbs) Solvent-free operation and no sample ■ Gear boxes Shipping package 45.7 cm (H) x 40.6 cm (W) x 35.6 cm (L) preparation Application Library Mineral and synthetic lubricants including gear, engine, ■ Turbines transmission, hydraulics, turbine and biodiesels dimensions (18 in x 16 in x 14 in) Requires less than 2 ml of sample to test ■ Hydraulics Output TAN (mgKOH/g), TBN (mgKOH/g); Oxidation Shipping pkg weight 8.1 kg, (18 lbs) Results in 30 seconds ■ Transmissions (varies by fluid type (abs/0.1 mm); Nitration (abs/cm); Sulfation COMPLIANCE FerroCheck 2000 FerroCheck 2100 and application) (abs/0.1 mm); Water, ppm (dissolved, dissolved + free ■ Engines Expanded I/O capability water with Comprehensive Water Solution option); CE Mark: EMC Directive (2004/108/EC); RoHS ■ Pumps and compressors Automated data storage, export files Oil 0-10,000 ppm 0-10,000 ppm Glycol (% by weight); Soot (% by weight); Incorrect ™ ACCESSORIES & CONSUMABLES in CSV format or use AMS OilView Fluid (% by weight); Antioxidant Depletion (% Grease NA 0-15% remaining); Antiwear Depletion (% by weight). A475101 OilView LIMS software software interface Methodology ASTM D7889, ASTM E1655, E2412 modified FL310 IR Check Fluid 5 mL Standard Analytical Mid infrared range 950-3850 cm-1 PV1011 Disposable Non-Abrasive Cleaning Pads; pkg of 500 Range P-11052 60 µL Disposable Pipettes, package of 500 Accuracy ≤ ± 3% of measured value, typical PV1012 60 µL Disposable Pipettes & Non-Abrasive Cleaning Repeatability ≤ ± 6% of measured value, typical Pad Kit; package of 100 each SAMPLE VIAL Calibration Factory calibrated to wet chemistry methods ASTM FL360 Reference Fluid Application Library – all categories D664 for TAN and ASTM D4739 for TBN. Use Check Fluid for instrument validation. P-11178 Pipette tips for positive displacement pipette (used with MiniVisc 3050), package of 192 OPERATIONAL SPECIFICATIONS 450-00003 Tray Assembly and Charging Station, MEASUREMENT REFERENCE Sample Volume 100 μL (1 drop) 100-240 VAC, 50/60 Hz COIL COIL Principle of Operation Solvents/Reagents None The core of the FerroCheck 2000 is a pair of precision-rounded coils that when powered generate magnetic fields. When a small amount of in-service oil is inserted into one of the coils, Schematic of Coil Around Sample ferrous particles such as iron, nickel and cobalt interact with the magnetic field and introduce current changes in the coils. The amount of current change is proportional to the amount of | Spectro Scientific One Executive Drive, Suite 101, Chelmsford, MA 01824-2563 ferrous particles in the oil, calibrated in weight by parts per million (ppm). 978-431-1120 | www.spectrosci.com | [email protected] | An ISO 9001:2008 company Copyright © 2017 Spectro Scientific. All rights reserved. While every effort is made to assure the information in this document is accurate, Spectro Scientific does not accept liability for any errors or mistakes that may arise. Specifications are subject to change without notice. FluidScan Series_DSv5_2017-10-19 52 | Product Catalog Product Catalog | 53 FerroCheck 2000 Series Product Information
PART NUMBERS USER INTERFACE SPECIFICATIONS 800-00071 FerroCheck 2000 ferrous monitor for oil Display 6”, fixed-angle, color touchscreen display
800-00069 FerroCheck 2000 standard accessories kit. Includes Data Transfer USB flashdrive or to OilView LIMS software instrument carrying case, dust cover, 1000 sample vials, 200 vial stoppers, and oil validation standards. Data Entry Touchscreen 800-00081 FerroCheck 2100 ferrous monitor for oil and grease POWER REQUIREMENTS
800-00082 FerroCheck 2100 standard accessories kit. Includes Power Source Built in rechargeable NiCd battery instrument carrying case, dust cover, 1000 sample Power 100-240 VAC, 50/60 Hz, 3.5 watts for charger vials, 300 grease boats and blades, 200 vial MiniVisc 3000 Series stoppers, and oil and grease validation standards. Typical Runtime Battery life 4-6 h or plug in for continuous use PORTABLE KINEMATIC VISCOMETERS PRODUCT INFORMATION MECHANICAL SPECIFICATIONS Solvent-free, simple to use, fast and accurate results Applications FerroCheck 2000: Lubricant oil Dimensions (WxDxH) 17 cm x 20 cm x 13.5 cm (6.6 in x 7.8 in x 5.2 in) FerroCheck 2100: Lubricant oil and grease Weight 2.9 kg Output Total ferrous, parts per million by weight COMPLIANCE Methodology ASTM D8120 CE, FCC Class B, NEMA 2, IP31 Standard Calibrated FerroCheck 2000: 0-2000 ppm, 2000-10,000 ppm High accuracy 40C kinematic viscosity measurements Ranges FerroCheck 2100: 0-2000 ppm, CONSUMABLES Applications include: for new and in-service oils 2000-10,000 ppm for oil 800-00070 FerroCheck 2000 consumables kit (500 samples). ■ Machine Condition Monitoring – Lab-quality results when and where Test even dark and sooty samples 0-2000 ppm, Includes 500 sample vials, 100 vial stoppers, and Increase availability of critical you need them Innovative design allows testing of 2000 ppm-15% for grease validation standards. equipment by monitoring viscosity Test Time < 30 s Accuracy +/- 3% Relative Standard virtually any sample including dark and 800-00075 FerroCheck 2100 consumables kit (500 samples). changes due to oil degradation and Includes 500 sample vials, 100 vial stoppers, 150 Deviation to NIST viscosity standards. sooty or transparent samples without any Limit of detection 3 ppm contamination. Avoid inadequate grease boats and blades, and validation standards. Solvent-free operation pre-checks. lubrication which causes Repeatability 3% RSD 600-00033 FerroCheck sample vials, qty 100 Portable, battery-powered design adhesive wear in machinery and Fewer consumables, lower disposal costs Calibration Ferrous standards provided 600-00031 Grease sample boats and blades, qty 50 each is a principal cause of equipment and less environmental impact. Fits easily into a toolbox or carrying bag Easy cleaning with the patented split-cell and capable of operation for over six OPERATIONAL SPECIFICATIONS 600-00032 Grease boat, blade and vial kit, qty 50 each downtime. design – just wipe off the surfaces with hours before recharge. Sample Volume For oil with sampling vial: 1.5 ml ■ Quality Control for Fuel/Oil Production 600-00074 FerroCheck sample vial stoppers, qty 100 each a nonabrasive cleaning pad between With grease boat: 0.75 ml and Blending Expanded I/O capability 600-00113 100 ppm verification fluid for FerroCheck (oil) samples. Import sample lists and export Ambient Operating 10 to 40C ■ Incoming Inspection Quality Control Temperature 600-00114 5000 ppm verification fluid for FerroCheck (oil) Requires only a few drops of oil to test measurement results via ViscTrack or AMS Oilview software. Relative Humidity 10-90% RH, non-condensing 600-00124 Verification standard for grease, high range Obtain samples without impacting lubricant level; only a few drops (60 μL) ASTM compliance Internal Data Storage 2,000 samples 600-00125 Verification standard for grease, low range of oil required. A positive displacement ASTM D8092 “Standard Test Method for RSD: Relative Standard Deviation pipette is provided for the most precise, Field Determination of Kinematic Viscosity repeatable measurements. Using a Microchannel Viscometer.”
A recommended solution set includes the FluidScan 1000, Grease boat and MiniVisc 3000 and grease boat inserted FerroCheck 2000. into sample vial
Principle of Operation MiniVisc 3000 Series viscometers use a patented split cell design that enables measurement of kinematic viscosity using only a few drops (60 µl) of oil. When closed, the center pieces of the split cell form a funnel with a 100 micron gap allowing oil to flow down by gravity. Sensors along the funnel are triggered when oil flows by and flow time between two sensors is measured. The kinematic viscosity is then calculated. When opened, the split cell can be | V40 = A* (t -t ) + B Spectro Scientific One Executive Drive, Suite 101, Chelmsford, MA 01824-2563 1 0 easily cleaned with a non-abrasive cleaning pad and it is ready for the next sample. The split 978-431-1120 | www.spectrosci.com | [email protected] | An ISO 9001:2008 company *A and B are calibration coefficients cell is controlled at 40°C throughout the measurement. Copyright © 2017 Spectro Scientific. All rights reserved. While every effort is made to assure the information in this document is accurate, Spectro Scientific does not accept liability for any errors or mistakes that may arise. Specifications are subject to change without notice. FerroCheck_DSv1_2017-10-19 54 | Product Catalog FerroCheck 2000 Series Product Information
PART NUMBERS USER INTERFACE SPECIFICATIONS 800-00071 FerroCheck 2000 ferrous monitor for oil Display 6”, fixed-angle, color touchscreen display
800-00069 FerroCheck 2000 standard accessories kit. Includes Data Transfer USB flashdrive or to OilView LIMS software instrument carrying case, dust cover, 1000 sample vials, 200 vial stoppers, and oil validation standards. Data Entry Touchscreen 800-00081 FerroCheck 2100 ferrous monitor for oil and grease POWER REQUIREMENTS
800-00082 FerroCheck 2100 standard accessories kit. Includes Power Source Built in rechargeable NiCd battery instrument carrying case, dust cover, 1000 sample Power 100-240 VAC, 50/60 Hz, 3.5 watts for charger vials, 300 grease boats and blades, 200 vial MiniVisc 3000 Series stoppers, and oil and grease validation standards. Typical Runtime Battery life 4-6 h or plug in for continuous use PORTABLE KINEMATIC VISCOMETERS PRODUCT INFORMATION MECHANICAL SPECIFICATIONS Solvent-free, simple to use, fast and accurate results Applications FerroCheck 2000: Lubricant oil Dimensions (WxDxH) 17 cm x 20 cm x 13.5 cm (6.6 in x 7.8 in x 5.2 in) FerroCheck 2100: Lubricant oil and grease Weight 2.9 kg Output Total ferrous, parts per million by weight COMPLIANCE Methodology ASTM D8120 CE, FCC Class B, NEMA 2, IP31 Standard Calibrated FerroCheck 2000: 0-2000 ppm, 2000-10,000 ppm High accuracy 40C kinematic viscosity measurements Ranges FerroCheck 2100: 0-2000 ppm, CONSUMABLES Applications include: for new and in-service oils 2000-10,000 ppm for oil 800-00070 FerroCheck 2000 consumables kit (500 samples). ■ Machine Condition Monitoring – Lab-quality results when and where Test even dark and sooty samples 0-2000 ppm, Includes 500 sample vials, 100 vial stoppers, and Increase availability of critical you need them Innovative design allows testing of 2000 ppm-15% for grease validation standards. equipment by monitoring viscosity Accuracy +/- 3% Relative Standard virtually any sample including dark and Test Time < 30 s 800-00075 FerroCheck 2100 consumables kit (500 samples). changes due to oil degradation and Deviation to NIST viscosity standards. sooty or transparent samples without any
Includes 500 sample vials, 100 vial stoppers, 150 ANALYSIS OIL PORTABLE TOOLS Limit of detection 3 ppm contamination. Avoid inadequate grease boats and blades, and validation standards. Solvent-free operation pre-checks. lubrication which causes Repeatability 3% RSD 600-00033 FerroCheck sample vials, qty 100 Portable, battery-powered design adhesive wear in machinery and Fewer consumables, lower disposal costs Calibration Ferrous standards provided 600-00031 Grease sample boats and blades, qty 50 each is a principal cause of equipment and less environmental impact. Fits easily into a toolbox or carrying bag Easy cleaning with the patented split-cell and capable of operation for over six OPERATIONAL SPECIFICATIONS 600-00032 Grease boat, blade and vial kit, qty 50 each downtime. design – just wipe off the surfaces with hours before recharge. Sample Volume For oil with sampling vial: 1.5 ml ■ Quality Control for Fuel/Oil Production 600-00074 FerroCheck sample vial stoppers, qty 100 each a nonabrasive cleaning pad between With grease boat: 0.75 ml and Blending Expanded I/O capability 600-00113 100 ppm verification fluid for FerroCheck (oil) samples. Import sample lists and export Ambient Operating 10 to 40C ■ Incoming Inspection Quality Control Temperature 600-00114 5000 ppm verification fluid for FerroCheck (oil) Requires only a few drops of oil to test measurement results via ViscTrack or AMS Oilview software. Relative Humidity 10-90% RH, non-condensing 600-00124 Verification standard for grease, high range Obtain samples without impacting lubricant level; only a few drops (60 μL) ASTM compliance Internal Data Storage 2,000 samples 600-00125 Verification standard for grease, low range of oil required. A positive displacement ASTM D8092 “Standard Test Method for RSD: Relative Standard Deviation pipette is provided for the most precise, Field Determination of Kinematic Viscosity repeatable measurements. Using a Microchannel Viscometer.”
A recommended solution set includes the FluidScan 1000, Grease boat and MiniVisc 3000 and grease boat inserted FerroCheck 2000. into sample vial
Principle of Operation MiniVisc 3000 Series viscometers use a patented split cell design that enables measurement of kinematic viscosity using only a few drops (60 µl) of oil. When closed, the center pieces of the split cell form a funnel with a 100 micron gap allowing oil to flow down by gravity. Sensors along the funnel are triggered when oil flows by and flow time between two sensors is measured. The kinematic viscosity is then calculated. When opened, the split cell can be | V40 = A* (t -t ) + B Spectro Scientific One Executive Drive, Suite 101, Chelmsford, MA 01824-2563 1 0 easily cleaned with a non-abrasive cleaning pad and it is ready for the next sample. The split 978-431-1120 | www.spectrosci.com | [email protected] | An ISO 9001:2008 company *A and B are calibration coefficients cell is controlled at 40°C throughout the measurement. Copyright © 2017 Spectro Scientific. All rights reserved. While every effort is made to assure the information in this document is accurate, Spectro Scientific does not accept liability for any errors or mistakes that may arise. Specifications are subject to change without notice. FerroCheck_DSv1_2017-10-19 54 | Product Catalog Product Catalog | 55 MiniVisc 3000 Series Product Information MiniVisc 3000 MiniVisc 3050 The MiniVisc 3000 includes the base viscometer, battery charger, USB cable, user’s Range 10-350 cSt 1-700 cSt manual DVD and ViscTrack software. The recommended 3050 Standard Accessories Outputs V40 V40 Kit SA1021 includes a positive displacement pipette, disposable pipette tips and V100 (calculated) cleaning pads for 192 samples, and two viscosity standards kits. Pipette Disposable Positive The recommended 3000 Standard Accessories Kit SA1002 includes disposable pipette displacement 60 μl pipettes and cleaning pads for 100 samples, and two viscosity standards kits. pipette
PART NUMBER USER INTERFACE SPECIFICATIONS SpectroVisc-Q3050 MiniVisc 3050 Portable Viscometer, 1-700 cSt. Display Fixed angle color touchscreen display Requires SA1021 Standard Accessories Kit. FDM 6000 Series Data Transfer USB for software updates SpectroVisc-Q3000 MiniVisc 3000 Portable Viscometer, 10-350 cSt. Data Entry Touchscreen PORTABLE FUEL DILUTION METER Requires SA1002 Standard Accessories Kit. POWER REQUIREMENTS Spectro-Q1100/Q3050 FluidScan 1100 Lubricant Condition Monitor & Solvent-free, simple to use, fast and accurate results MiniVisc 3050 Combo Kit. Requires SA1022 Standard Battery Power Source Built in rechargeable lithium ion battery Accessories for Combo Kit. Power AC 110/240 V, 50/60 Hz, 10 Watts Spectro-Q1000/Q3050 FluidScan 1000 Lubricant Condition Monitor & MiniVisc 3050 Combo Kit. Requires SA1022 Standard Typical Runtime 6-8 hours with full charge Accessories for Combo Kit. Recharge Time 2.5 hrs PRODUCT INFORMATION MECHANICAL SPECIFICATIONS FDM 6000 Series is a portable fuel dilution meter that measures Applications Lubricant oils (mineral and synthetic), coolants, Dimensions 152 mm (H) x 127 mm (W) x 203 mm (D) The Need for Fuel Dilution direct fuel dilution in engine oil. glycol, and any Newtonian fluid within the measuring (6.0 in x 5.0 in x 8.0 in) Measurement range Lab quality results where and when you need them Weight 1.8 kg (4.0 lbs) Output Kinematic viscosity (cSt) @ 40°C If left unchecked, fuel dilution in lube 0.2 to 15% fuel dilution measurement range. V100 viscosity calculation from VI index input (3050 only) Shipping Package 50.8 cm (H) x 40.6 cm (W) x 35.6 cm (L) oil causes serious engine damage. Dimensions (20 in x 16 in x 14 in) Excellent repeatability (≤5% RSD). Methodology ASTM D 8092 In diesel engine crankcases, fuel Shipping Package 4.9 kg (11 lbs) dilution can be caused by: Disposable FDM vials eliminat e carryover contamination. Standard Analytical 3000: 10-350 cSt @ 40°C Weight Range 3050: 1-700 cSt @ 40°C ■ Excessive idling Onboard memory allows use of up to three stored calibration profiles. COMPLIANCE ■ Defective injectors Accuracy 3000: Sample ID entry and data file export via USB cable. ■ ≤ ± 3% of measured value over range 10-350 cSt CE Mark: EMC Directive (2004/108/EC); RoHS Loose connections Battery powered, lightweight, optional hard case for transit. ■ Intercooler leakage 3050: CONSUMABLES Complies to ASTM D8004. ≤ ± 3% of measured value over range 1-350 cSt (aircraft hydraulic systems) P-11177 Positive displacement pipette, 10-100 μL ≤ ± 5% of measured value for viscosity > 350 cSt Fast and easy to use P-11178 Pipette tips for P-11177, package of 192 Therefore fuel dilution is a common Accuracy specification is with use of user correction function. test item for both on site and off site Small volume – 0.5 ml of sample required. P-11201 Pipette tips for P-11177, package of 960 Repeatability 3000: in-service engine oil analysis. No solvent needed for cleaning. ≤ ± 3% RSD of measured value, typical PV1011 Disposable non-abrasive cleaning pads, Less than one minute test time. 3050: package of 500 ≤ ± 3% RSD of value, typical, over range 1-350 cSt P-11052 60 μL disposable pipettes, package of 500 Direct reading of fuel dilution percentage. ≤ ± 5% RSD of measured value for viscosity > 350 cSt PV1025 Visc 30 standard, 20 ml Easy touch screen interface with voice guidance. RSD is Relative Standard Deviation. PV1026 Visc 120 standard, 20 ml Test Temperature ± 0.1°C Control Calibration Not required A recommended solution set includes PATENTED FDM SAMPLING SYSTEM OPERATIONAL SPECIFICATIONS the FluidScan 1000, Sample Volume 60 µL (about 3-4 drops) MiniVisc 3000 and
FerroCheck 2000. PURGE Solvents/Reagents None INLET PUMP
Ambient Operating 0°C to 40°C (32°F to 104°F) AMBIENT Temperature AIR SAW Innovative design Relative Humidity 10% to 80% r.h. non-condensing SENSOR ARRA The FDM analyzer employ a Surface Acoustic Wave (SAW) vapor sensor to measure the Ambient Altitude Up to 5,000 meters (16,404 feet) concentration of fuel in used oil samples by sampling the “headspace” in the vial. The device SAMPLE assumes (based on Henry’s Law) that the fuel concentration in the headspace vapor is directly VENT PUMP related to the fuel present in the oil sample. The surface of the SAW sensor has a polymer
DISPOSABLE coating with specific solubility to fuel vapors. The sample pump draws the headspace vapor | OIL SAMPLE Spectro Scientific One Executive Drive, Suite 101, Chelmsford, MA 01824-2563 CONTAINER through the SAW sensor where it is absorbed onto the polymer coating and detected. The purge 978-431-1120 | www.spectrosci.com | [email protected] | An ISO 9001:2008 company pump then pushes air through the SAW to clean the system so it is ready for the next sample. Copyright © 2017 Spectro Scientific. All rights reserved. While every effort is made to assure the information in this document is accurate, Spectro Scientific does not accept liability for any errors or mistakes that may arise. Specifications are subject to change without notice. MiniVisc3000Series_DSv4_2017-10-19 56 | Product Catalog MiniVisc 3000 Series Product Information MiniVisc 3000 MiniVisc 3050 The MiniVisc 3000 includes the base viscometer, battery charger, USB cable, user’s Range 10-350 cSt 1-700 cSt manual DVD and ViscTrack software. The recommended 3050 Standard Accessories Outputs V40 V40 Kit SA1021 includes a positive displacement pipette, disposable pipette tips and V100 (calculated) cleaning pads for 192 samples, and two viscosity standards kits. Pipette Disposable Positive The recommended 3000 Standard Accessories Kit SA1002 includes disposable pipette displacement 60 μl pipettes and cleaning pads for 100 samples, and two viscosity standards kits. pipette
PART NUMBER USER INTERFACE SPECIFICATIONS SpectroVisc-Q3050 MiniVisc 3050 Portable Viscometer, 1-700 cSt. Display Fixed angle color touchscreen display Requires SA1021 Standard Accessories Kit. FDM 6000 Series Data Transfer USB for software updates SpectroVisc-Q3000 MiniVisc 3000 Portable Viscometer, 10-350 cSt. Data Entry Touchscreen PORTABLE FUEL DILUTION METER Requires SA1002 Standard Accessories Kit. POWER REQUIREMENTS Spectro-Q1100/Q3050 FluidScan 1100 Lubricant Condition Monitor & Solvent-free, simple to use, fast and accurate results MiniVisc 3050 Combo Kit. Requires SA1022 Standard Battery Power Source Built in rechargeable lithium ion battery Accessories for Combo Kit. Power AC 110/240 V, 50/60 Hz, 10 Watts Spectro-Q1000/Q3050 FluidScan 1000 Lubricant Condition Monitor & MiniVisc 3050 Combo Kit. Requires SA1022 Standard Typical Runtime 6-8 hours with full charge Accessories for Combo Kit. Recharge Time 2.5 hrs PRODUCT INFORMATION MECHANICAL SPECIFICATIONS FDM 6000 Series is a portable fuel dilution meter that measures Applications Lubricant oils (mineral and synthetic), coolants, Dimensions 152 mm (H) x 127 mm (W) x 203 mm (D) The Need for Fuel Dilution direct fuel dilution in engine oil. glycol, and any Newtonian fluid within the measuring (6.0 in x 5.0 in x 8.0 in) Measurement range Lab quality results where and when you need them Weight 1.8 kg (4.0 lbs) Output Kinematic viscosity (cSt) @ 40°C If left unchecked, fuel dilution in lube 0.2 to 15% fuel dilution measurement range. V100 viscosity calculation from VI index input (3050 only) Shipping Package 50.8 cm (H) x 40.6 cm (W) x 35.6 cm (L) oil causes serious engine damage. Dimensions (20 in x 16 in x 14 in) Excellent repeatability (≤5% RSD). ANALYSIS OIL PORTABLE TOOLS Methodology ASTM D 8092 In diesel engine crankcases, fuel Shipping Package 4.9 kg (11 lbs) dilution can be caused by: Disposable FDM vials eliminat e carryover contamination. Standard Analytical 3000: 10-350 cSt @ 40°C Weight Range 3050: 1-700 cSt @ 40°C ■ Excessive idling Onboard memory allows use of up to three stored calibration profiles. COMPLIANCE ■ Defective injectors Accuracy 3000: Sample ID entry and data file export via USB cable. ■ ≤ ± 3% of measured value over range 10-350 cSt CE Mark: EMC Directive (2004/108/EC); RoHS Loose connections Battery powered, lightweight, optional hard case for transit. ■ Intercooler leakage 3050: CONSUMABLES Complies to ASTM D8004. ≤ ± 3% of measured value over range 1-350 cSt (aircraft hydraulic systems) P-11177 Positive displacement pipette, 10-100 μL ≤ ± 5% of measured value for viscosity > 350 cSt Fast and easy to use P-11178 Pipette tips for P-11177, package of 192 Therefore fuel dilution is a common Accuracy specification is with use of user correction function. test item for both on site and off site Small volume – 0.5 ml of sample required. P-11201 Pipette tips for P-11177, package of 960 Repeatability 3000: in-service engine oil analysis. No solvent needed for cleaning. ≤ ± 3% RSD of measured value, typical PV1011 Disposable non-abrasive cleaning pads, Less than one minute test time. 3050: package of 500 ≤ ± 3% RSD of value, typical, over range 1-350 cSt P-11052 60 μL disposable pipettes, package of 500 Direct reading of fuel dilution percentage. ≤ ± 5% RSD of measured value for viscosity > 350 cSt PV1025 Visc 30 standard, 20 ml Easy touch screen interface with voice guidance. RSD is Relative Standard Deviation. PV1026 Visc 120 standard, 20 ml Test Temperature ± 0.1°C Control Calibration Not required A recommended solution set includes PATENTED FDM SAMPLING SYSTEM OPERATIONAL SPECIFICATIONS the FluidScan 1000, Sample Volume 60 µL (about 3-4 drops) MiniVisc 3000 and
FerroCheck 2000. PURGE Solvents/Reagents None INLET PUMP
Ambient Operating 0°C to 40°C (32°F to 104°F) AMBIENT Temperature AIR SAW Innovative design Relative Humidity 10% to 80% r.h. non-condensing SENSOR ARRA The FDM analyzer employ a Surface Acoustic Wave (SAW) vapor sensor to measure the Ambient Altitude Up to 5,000 meters (16,404 feet) concentration of fuel in used oil samples by sampling the “headspace” in the vial. The device SAMPLE assumes (based on Henry’s Law) that the fuel concentration in the headspace vapor is directly VENT PUMP related to the fuel present in the oil sample. The surface of the SAW sensor has a polymer
DISPOSABLE coating with specific solubility to fuel vapors. The sample pump draws the headspace vapor | OIL SAMPLE Spectro Scientific One Executive Drive, Suite 101, Chelmsford, MA 01824-2563 CONTAINER through the SAW sensor where it is absorbed onto the polymer coating and detected. The purge 978-431-1120 | www.spectrosci.com | [email protected] | An ISO 9001:2008 company pump then pushes air through the SAW to clean the system so it is ready for the next sample. Copyright © 2017 Spectro Scientific. All rights reserved. While every effort is made to assure the information in this document is accurate, Spectro Scientific does not accept liability for any errors or mistakes that may arise. Specifications are subject to change without notice. MiniVisc3000Series_DSv4_2017-10-19 56 | Product Catalog Product Catalog | 57 FDM 6000 Series Product Information FDM 6000 FDM 6001 Both the FDM 6000 and 6001 include the base fuel dilution meter, soft tip stylus, battery charger, USB cable, CD manual, FDM vials and disposable pipettes for 100 samples. Stored Calibration 1 3
PART NUMBER MECHANICAL SPECIFICATIONS SpectroFDM-Q6001 FDM 6001 Fuel Dilution Meter System – Multiple Dimensions 15 cm (W) x 19.75 cm (D) x 13.5 cm (H) Calibration. Requires SA1019 Standard Accessory Kit. (5.9 in x 7.77 in x 5.31 in) SpectroFDM-Q6000 FDM 6000 Fuel Dilution Meter System – Single Weight 1.4 kg (3 lbs) Calibration. Requires SA1019 Standard Accessory Kit. Shipping Package 45.7 cm (H) x 40.6 cm (W) x 35.6 cm (L) InfraCal 2 Soot Meter SA1019 Spectro-Q6000 Standard Accessories Dimensions (18 in x 16 in x 14 in) PRODUCT INFORMATION Shipping Package 8.1 kg, (18 lbs) PORTABLE, RUGGED INFRARED ANALYZER Weight Application Mineral and Synthetic Lubricants used in liquid fueled engines COMPLIANCE Output % (wt or vol) ) Fuel dilution CENELEC EN 61010-1 (2010/10/01 Ed:3 ); CENELEC EN 61326-2-1 (2006/05/01); FCC 47CFR 15B; RoHS Methodology ASTM D8004 CONSUMABLES AND STANDARDS Standard Analytical 0.2 -15% fuel in oil (fuel dilution) The InfraCal 2 Soot Meter measures the amount of Range 346162035 FDM Vials Kit (50 pk) suspended carbon (soot) in diesel engine lubricating Measurement range: Accuracy ≤± 0.2% fuel dilution in range 0.2-2% 346162037 FDM Vials Kit (500 pk) Soot, in diesel engines, is made oils by infrared absorption at a fixed wavelength. 0 - 15% soot ≤± 10% of measurement in range 2-15% up of nanometer size hard carbon 346162036 500 μL Disposable Pipettes (50 pk) The Soot Meter is based on proven IR technology. Instrument repeatability: Repeatability ≤± 5% RSD of measurement + 0.2% fuel dilution particles and is deposited in the P-11185 500 uL Disposable Pipettes (500 pk) Results correlate to the TGA (thermogravimetric +/- 0.2 Calibration Single point, User developed or Certified Check oil as combustion by-products. DSL5%DEV-100 5% Devolatized diesel in oil fuel dilution standard, analysis) reference method ASTM D7686 and Complies with Standard (optional) As soot globules coagulate into NIST traceable, 100ml FTIR methods. No solvents requiring special ASTM Method D7686 OPERATIONAL SPECIFICATIONS larger particles, engine wear will DSLBLK-15W40-100 Diesel blank standard for fuel dilution standard, 100 ml ventilation, expensive waste disposal or difficult to No dilution or sample Sample Volume 0.5 mL accelerate. At very high levels GASFD-2P-100 2% Devolatized gasoline in oil standard, clean cells are needed. preparation soot can cause an increase in the Solvents/Reagents None NIST traceable, 100 ml Rapid analysis – less than oil viscosity. Higher than normal Ambient Operating 5°C to 35°C (41°F to 95 °F) OPTIONAL ACCESSORIES Ideal for: 30 seconds per sample Temperature levels can indicate an improper air/ P-11186 Positive Displacement Pipette 100-1000 μl Oil testing labs – achieve comparable results to Multiple language interface fuel ratio, plugged or defective air Relative Humidity 0 to 90%, non-condensing TGA or FTIR in a fraction of the time with touch screen input P-11187 Pipette Tips 100-1000 μl (182 pk) intakes or leaking injectors. Ambient Altitude up to 2,000 meters (6561 feet) Engine test labs – obtain on-the-spot assessment of P-11189 Transport Case FDM 6000 Series Password protected USER INTERFACE SPECFICATIONS the engine test progress settings Fleet maintenance shops – check soot level to Display 4.3” TFT color screen (480 X 272 ) know exactly when to schedule oil changes Data Storage 4 GB Construction or mining sites – stay operational Data Transfer USB with oil condition checks Data Entry Touch-screen with stylus On-board-ship – no need to return to port to monitor POWER REQUIREMENTS oil condition Battery Power Built in Rechargeable Lithium Ion Battery Power generation stations – monitor the quality of Source the lubricating oil without waiting for off-site lab Power AC 110/240 V, 50/60 Hz, 9 Watts, 9 Volts results Typical Runtime 3-4 hours Recharge Time 4 hours
Standards and optional FDM consumable and preparation kit Principle of Operation positive displacement Samples are applied to a zinc selenide (ZnSe) pipette attenuated total reflectance (ATR) sample plate. Infrared light from a source bounces multiple times between the top and bottom surfaces of ZnSe crystal as it travels horizontally from one side to the other. It is then filtered and measured by the detector. The loss of the light at specific wavelengths is due to the absorption by the oil sample on the top plate and it is then Spectro Scientific | One Executive Drive, Suite 101, Chelmsford, MA 01824-2563 978-431-1120 | www.spectrosci.com | [email protected] | An ISO 9001:2008 company calculated to percentage of soot based on calibration to gravimetric methods. Copyright © 2017 Spectro Scientific. All rights reserved. While every effort is made to assure the information in this document is accurate, Spectro Scientific does not accept liability for any errors or mistakes that may arise. Specifications are subject to change without notice. FDM 6000_DSv3_2017-10-19 58 | Product Catalog FDM 6000 Series Product Information FDM 6000 FDM 6001 Both the FDM 6000 and 6001 include the base fuel dilution meter, soft tip stylus, battery charger, USB cable, CD manual, FDM vials and disposable pipettes for 100 samples. Stored Calibration 1 3
PART NUMBER MECHANICAL SPECIFICATIONS SpectroFDM-Q6001 FDM 6001 Fuel Dilution Meter System – Multiple Dimensions 15 cm (W) x 19.75 cm (D) x 13.5 cm (H) Calibration. Requires SA1019 Standard Accessory Kit. (5.9 in x 7.77 in x 5.31 in) SpectroFDM-Q6000 FDM 6000 Fuel Dilution Meter System – Single Weight 1.4 kg (3 lbs) Calibration. Requires SA1019 Standard Accessory Kit. Shipping Package 45.7 cm (H) x 40.6 cm (W) x 35.6 cm (L) InfraCal 2 Soot Meter SA1019 Spectro-Q6000 Standard Accessories Dimensions (18 in x 16 in x 14 in) PRODUCT INFORMATION Shipping Package 8.1 kg, (18 lbs) PORTABLE, RUGGED INFRARED ANALYZER Weight Application Mineral and Synthetic Lubricants used in liquid fueled engines COMPLIANCE Output % (wt or vol) ) Fuel dilution CENELEC EN 61010-1 (2010/10/01 Ed:3 ); CENELEC EN 61326-2-1 (2006/05/01); FCC 47CFR 15B; RoHS Methodology ASTM D8004 CONSUMABLES AND STANDARDS Standard Analytical 0.2 -15% fuel in oil (fuel dilution) The InfraCal 2 Soot Meter measures the amount of Range 346162035 FDM Vials Kit (50 pk) suspended carbon (soot) in diesel engine lubricating Measurement range: Accuracy ≤± 0.2% fuel dilution in range 0.2-2% 346162037 FDM Vials Kit (500 pk) Soot, in diesel engines, is made oils by infrared absorption at a fixed wavelength. 0 - 15% soot ≤± 10% of measurement in range 2-15% up of nanometer size hard carbon 346162036 500 μL Disposable Pipettes (50 pk) The Soot Meter is based on proven IR technology. Instrument repeatability: Repeatability ≤± 5% RSD of measurement + 0.2% fuel dilution particles and is deposited in the P-11185 500 uL Disposable Pipettes (500 pk) Results correlate to the TGA (thermogravimetric +/- 0.2 Calibration Single point, User developed or Certified Check oil as combustion by-products. DSL5%DEV-100 5% Devolatized diesel in oil fuel dilution standard, analysis) reference method ASTM D7686 and Complies with Standard (optional) As soot globules coagulate into NIST traceable, 100ml FTIR methods. No solvents requiring special ASTM Method D7686 ANALYSIS OIL PORTABLE TOOLS OPERATIONAL SPECIFICATIONS larger particles, engine wear will DSLBLK-15W40-100 Diesel blank standard for fuel dilution standard, 100 ml ventilation, expensive waste disposal or difficult to No dilution or sample Sample Volume 0.5 mL accelerate. At very high levels GASFD-2P-100 2% Devolatized gasoline in oil standard, clean cells are needed. preparation soot can cause an increase in the Solvents/Reagents None NIST traceable, 100 ml Rapid analysis – less than oil viscosity. Higher than normal Ambient Operating 5°C to 35°C (41°F to 95 °F) OPTIONAL ACCESSORIES Ideal for: 30 seconds per sample Temperature levels can indicate an improper air/ P-11186 Positive Displacement Pipette 100-1000 μl Oil testing labs – achieve comparable results to Multiple language interface fuel ratio, plugged or defective air Relative Humidity 0 to 90%, non-condensing TGA or FTIR in a fraction of the time with touch screen input P-11187 Pipette Tips 100-1000 μl (182 pk) intakes or leaking injectors. Ambient Altitude up to 2,000 meters (6561 feet) Engine test labs – obtain on-the-spot assessment of P-11189 Transport Case FDM 6000 Series Password protected USER INTERFACE SPECFICATIONS the engine test progress settings Fleet maintenance shops – check soot level to Display 4.3” TFT color screen (480 X 272 ) know exactly when to schedule oil changes Data Storage 4 GB Construction or mining sites – stay operational Data Transfer USB with oil condition checks Data Entry Touch-screen with stylus On-board-ship – no need to return to port to monitor POWER REQUIREMENTS oil condition Battery Power Built in Rechargeable Lithium Ion Battery Power generation stations – monitor the quality of Source the lubricating oil without waiting for off-site lab Power AC 110/240 V, 50/60 Hz, 9 Watts, 9 Volts results Typical Runtime 3-4 hours Recharge Time 4 hours
Standards and optional FDM consumable and preparation kit Principle of Operation positive displacement Samples are applied to a zinc selenide (ZnSe) pipette attenuated total reflectance (ATR) sample plate. Infrared light from a source bounces multiple times between the top and bottom surfaces of ZnSe crystal as it travels horizontally from one side to the other. It is then filtered and measured by the detector. The loss of the light at specific wavelengths is due to the absorption by the oil sample on the top plate and it is then Spectro Scientific | One Executive Drive, Suite 101, Chelmsford, MA 01824-2563 978-431-1120 | www.spectrosci.com | [email protected] | An ISO 9001:2008 company calculated to percentage of soot based on calibration to gravimetric methods. Copyright © 2017 Spectro Scientific. All rights reserved. While every effort is made to assure the information in this document is accurate, Spectro Scientific does not accept liability for any errors or mistakes that may arise. Specifications are subject to change without notice. FDM 6000_DSv3_2017-10-19 58 | Product Catalog Product Catalog | 59 Soot Meter Product Information
PART NUMBER OPERATING SPECIFICATIONS 406-2048 InfraCal 2 Soot Meter, complete with HATR sample Sample Volume < 1 ml stage for direct measurement of suspended carbon (soot) level in diesel engine oils (factory calibrated Solvent/Reagent None to 12% soot concentration) set of reference oils and Operating Temperature 5°C - 40°C power supply. PRODUCT INFORMATION Relative Humidity 0 - 90%, non-condensing Analytical 3.9 micrometers, 2464 cm-1 Altitude Up to 5000 meters Wavelength/ MECHANICAL SPECIFICATIONS Wave Number Outputs % (by weight) soot in engine oil Weight 7.0 lbs (3.2 kg)
ASTM Method ASTM 7686 Dimensions 6.7” x 7.8” x 5.2” (170 x 198 x 132 mm)
Analytical Range 0 - 15% Shipping Weight 8.0 lbs (3.6 kg)
Analysis Time Less than 30 seconds Shipping Dimensions 10 x 10 x 14” (254 x 254 x 355 mm)
Instrument ±0.2% COMPLIANCE Repeatability CE, FCC Class B, NEMA 2, IP31 USER INTERFACE SPECIFICATIONS CONSUMABLES AND STANDARDS User interface 6” color display 403-0025 Set of 6 reference oils in dropper bottles, appropriate Data input Touch screen for calibration and verification of reproducibility 0 - 12% soot range. This set of reference oils Communication port USB, RS 232 has been correlated with the results obtained via thermal gravimetric analysis (TGA) of fresh used POWER REQUIREMENTS diesel oil samples. Battery Power Source 18 volt NiCad battery OPTIONAL ACCESSORIES External Power 18 volts DC, 3.3 amps 403-0013 Carrying case for InfraCal Analyzers with pre-diced Requirements pluck foam. 18.5” x 14.6” x 8”; 10 lbs Power Adaptor Input Universal AC/DC 403-1086 Dust cover Battery Run Time 4 - 6 hours
The Soot Meter can be used as part of a solutions kit for engine oil condition.
Spectro Scientific | One Executive Drive, Suite 101, Chelmsford, MA 01824-2563 978-431-1120 | www.spectrosci.com | [email protected] | An ISO 9001:2008 company Copyright © 2017 Spectro Scientific. All rights reserved. While every effort is made to assure the information in this document is accurate, Spectro Scientific does not accept liability for any errors or mistakes that may arise. Specifications are subject to change without notice. InfraCal 2 Soot Meter_DSv1_2017-06-30 60 | Product Catalog Soot Meter Product Information
PART NUMBER OPERATING SPECIFICATIONS 406-2048 InfraCal 2 Soot Meter, complete with HATR sample Sample Volume < 1 ml stage for direct measurement of suspended carbon Oil Analysis Laboratory Instruments (soot) level in diesel engine oils (factory calibrated Solvent/Reagent None to 12% soot concentration) set of reference oils and Operating Temperature 5°C - 40°C power supply. PRODUCT INFORMATION Relative Humidity 0 - 90%, non-condensing Analytical 3.9 micrometers, 2464 cm-1 Altitude Up to 5000 meters Wavelength/ MECHANICAL SPECIFICATIONS Wave Number Outputs % (by weight) soot in engine oil Weight 7.0 lbs (3.2 kg) ASTM Method ASTM 7686 Dimensions 6.7” x 7.8” x 5.2” (170 x 198 x 132 mm)
Analytical Range 0 - 15% Shipping Weight 8.0 lbs (3.6 kg)
Analysis Time Less than 30 seconds Shipping Dimensions 10 x 10 x 14” (254 x 254 x 355 mm)
Instrument ±0.2% COMPLIANCE Repeatability CE, FCC Class B, NEMA 2, IP31 USER INTERFACE SPECIFICATIONS CONSUMABLES AND STANDARDS User interface 6” color display 403-0025 Set of 6 reference oils in dropper bottles, appropriate Data input Touch screen for calibration and verification of reproducibility 0 - 12% soot range. This set of reference oils Communication port USB, RS 232 has been correlated with the results obtained via thermal gravimetric analysis (TGA) of fresh used POWER REQUIREMENTS diesel oil samples. Battery Power Source 18 volt NiCad battery OPTIONAL ACCESSORIES External Power 18 volts DC, 3.3 amps 403-0013 Carrying case for InfraCal Analyzers with pre-diced Requirements pluck foam. 18.5” x 14.6” x 8”; 10 lbs Power Adaptor Input Universal AC/DC 403-1086 Dust cover Battery Run Time 4 - 6 hours
The Soot Meter can be used as part of a solutions kit for engine oil condition.
Spectro Scientific | One Executive Drive, Suite 101, Chelmsford, MA 01824-2563 978-431-1120 | www.spectrosci.com | [email protected] | An ISO 9001:2008 company Copyright © 2017 Spectro Scientific. All rights reserved. While every effort is made to assure the information in this document is accurate, Spectro Scientific does not accept liability for any errors or mistakes that may arise. Specifications are subject to change without notice. InfraCal 2 Soot Meter_DSv1_2017-06-30 60 | Product Catalog SpectroTrack INFORMATION MANAGEMENT SYSTEM
Industrial Tribology Lab (ITL) Benefits of SpectroTrack IMS SpectroTrack is an information Efficient Data Collection = Greater Expandability The Spectro Scientific Industrial Tribology Laboratory (ITL) is a turnkey system that provides management system (IMS) optimized SpectroTrack offers a streamlined process for accepting oil analysis data from a variety a complete lubricant analysis condition monitoring solution . The measurements made for machine condition monitoring. of analytical instruments. Users have the flexibility to add new classes of analysis and using the Industrial Tribology Laboratory determine lubricant and machine condition, the The browser-based system is the ideal additional parameters as needed, including trend analysis. core of any effective predictive maintenance system . The ITL system is expandable and tool for accessing historical and trend can incorporate testing and measurement solutions for other machinery fluids such as fuel, information about an organization’s Browser-based System = Easy Accessibility coolants, transformer oils and greases . The center piece of the ITL is the SpectrTrack LIMS high-value assets. The system The system can be viewed on any browser-based device eliminating the need for installation software that helps use manage assets, oil sample life cycle, analytical results, reports and provides a single end-to-end view on each workstation. Customers can access and view online interactive sample results maintenance actions in one place . of a sample lifecycle from sample anywhere and at any time to support them in making equipment maintenance decisions. submission and receipt to results entry. The software also provides Data Consolidation = Improved Accuracy and Consistency all trending, imaging, numerical and SpectroTrack brings information together with centralization of all oil analysis data as well IN STRIAL TRI L LA textual asset data in one secure as images from both Spectro Inc.’s and other vendor’s instrumentation. location. Clients and laboratory Simple System Deployment and Maintenance = Improved Productivity personnel can see a comprehensive, Once SpectroTrack is installed, operators only need browser access to begin using the historical view of fluid condition for an software. With a zero footprint on the client machine and remote access support, the engine, department or an entire fleet. SpectroTrack minimizes the need for costly IT support and maintenance while giving the operator the information necessary to maintain the health of high-value assets.
Multi-lab Module = Enterprise-level Support with a Single Point of Contact Maintenance Assets SpectroTrack’s multi-lab function integrates the workflow of Operations multiple testing labs and enables each lab to view samples and support each other. Clients with assets deployed globally have visibility to all assets and conditions. Critical oil analysis test information is easily shared by all.
Oil/Lubricant Sample Management and Workflow = Removal of Gap Samples Between Operator and Lab SpectroTrack facilitates the workflow between the equipment maintainer and the lab by managing the sample lifecycle. The system gives both customers and on-site labs the information critical to assess sample results, and ultimately, machine Maintenance condition. Spe troTrack Management INFORMATION MANAGEMENT S STEM Test Results ITL Workshop
62 | Product Catalog SpectroTrack INFORMATION MANAGEMENT SYSTEM
Benefits of SpectroTrack IMS SpectroTrack is an information Efficient Data Collection = Greater Expandability management system (IMS) optimized SpectroTrack offers a streamlined process for accepting oil analysis data from a variety for machine condition monitoring. of analytical instruments. Users have the flexibility to add new classes of analysis and The browser-based system is the ideal additional parameters as needed, including trend analysis. tool for accessing historical and trend information about an organization’s Browser-based System = Easy Accessibility high-value assets. The system The system can be viewed on any browser-based device eliminating the need for installation provides a single end-to-end view on each workstation. Customers can access and view online interactive sample results of a sample lifecycle from sample anywhere and at any time to support them in making equipment maintenance decisions. submission and receipt to results entry. The software also provides Data Consolidation = Improved Accuracy and Consistency
all trending, imaging, numerical and SpectroTrack brings information together with centralization of all oil analysis data as well OIL ANALYSIS LABORATORY INSTRUMENTS textual asset data in one secure as images from both Spectro Inc.’s and other vendor’s instrumentation. location. Clients and laboratory Simple System Deployment and Maintenance = Improved Productivity personnel can see a comprehensive, Once SpectroTrack is installed, operators only need browser access to begin using the historical view of fluid condition for an software. With a zero footprint on the client machine and remote access support, the engine, department or an entire fleet. SpectroTrack minimizes the need for costly IT support and maintenance while giving the operator the information necessary to maintain the health of high-value assets.
Multi-lab Module = Enterprise-level Support with a Single Point of Contact Maintenance Assets SpectroTrack’s multi-lab function integrates the workflow of Operations multiple testing labs and enables each lab to view samples and support each other. Clients with assets deployed globally have visibility to all assets and conditions. Critical oil analysis test information is easily shared by all.
Oil/Lubricant Sample Management and Workflow = Removal of Gap Samples Between Operator and Lab SpectroTrack facilitates the workflow between the equipment maintainer and the lab by managing the sample lifecycle. The system gives both customers and on-site labs the information critical to assess sample results, and ultimately, machine Maintenance Management condition.
Test Results ITL Workshop
62 | Product Catalog Product Catalog | 63 Feature Overview SpectroTrack Product Information ■ Self-contained installation on one server ■ Automatically retrieves data from all Spectro Inc. instruments PART NUMBERS AND ADDITIONAL CONFIGURATION OPTIONS ■ Designed specifically for oil analysis programs – dedicated or M90035 Base Product contract testing M90038 Additional Laboratory User License (each) ■ Supports customer (private label) branding M90036 SpectroTrack Custom Device Interface Remote Login Import driver interface for lab instruments (Spectro products ■ Laboratory customer (interactive report viewers) can access included in base product defined data ■ Remote portals can be connected to the Internet M90037 Client Portal Access Pack (101-500 Clients) Accounts M90042 Multi Lab Option – Resides on Main server SpectrOil M Series ■ Laboratory user accounts and client accounts password protected Allows multiple labs to share and access SpectroTrack on main server. All laboratory users with rights can access and ■ Multi user accounts for distributor sales or corporate reliability diagnose oil samples from all labs. Each lab must have P/N OIL ANALYSIS SPECTROMETER grouping M90035 Standard for rugged spectrometric oil analysis in the field Equipment ACCESSORIES ■ Assigned to accounts and can be searched, created, removed M90039 SpectroTrack Customer Reference Guide (Print ) and reactivated with ease ■ Detail includes manufacturer, application and components M90041 SpectroTrack Laboratory Reference Guide (Print) ■ Maintenance feedback and notes visible to all stakeholders P-10885 SpectroTrack Labelwriter Components P-10886 SpectroTrack Lab Barcode Labels (750/roll) Originally designed for military applications in the mid 1990s, the SpectrOil M is the only ■ Rich customer component detail, complete with assigned test P-10887 SpectroTrack Customer Labels (300/roll) The SpectrOil M Series RDE-OES in service oil analysis spectrometer approved by the US Department of Defense (DoD) Joint package Oil Analysis Program (JOAP). Since its development, the SpectrOil M has been the industry I&T Installation & Training Elemental Analyzer is a compact, ■ Can be easily transferred to other equipment (engine change) rugged, transportable spectrometer standard for reliable, deployable spectrometers that perform the rapid analysis of wear RECOMMENDED HARDWARE Scheduling designed for accurate elemental metals, contaminants and additives in lubricants, hydraulic fluids, fuels, coolants and water. ■ Schedule maintenance activities and analysis intervals Server x64 Processor: AMD Opteron, AMD Athlon 64, Intel Xeon with analysis of a variety of fluids tested Processor Intel EM64T support, Intel Pentium IV with EM64T support ■ Automatic reminders sent via email in the field or in a laboratory. Using SpectrOil M Series key features ■ Customer bottle labels printed prior to submittal x86 Processor: Pentium III-compatible processor or faster the proven, reliable rotating disc Rugged frame and optics system that meets military shock and vibration and RAM 4 GB Sample Login electrode (RDE) technique, the environmental test standards (JOAP CID-0191) ■ Auto-fill and drop-down selection Hard Drive 500 GB analyzer measures trace quantities of Designed for remote locations and frequent transportation elements dissolved or suspended as Data Entry Operating Windows XP, Windows Server 2008 R2 Standard, No sample preparation required systems Windows 7 Professional Edition or Higher, fine particles in natural or synthetic ■ Bar code tracking bottle labels Windows Vista Professional Edition or Higher 30 second analysis time ■ petroleum-based products. It includes Shows status of each batch as it moves through the laboratory Analyzes up to 31 elements simultaneously ■ new and in-service lubricants, Automatic data collection from Spectro instruments Self-sustained with built-in industrial touch panel PC –Expandable with other vendor-supplied instruments hydraulic fluids, light (gasoline or Simple to operate; does not require special training ■ Laboratory dashboard for easy workflow management diesel) or heavy fuels (HFO), coolants, industrial process water or wash- No special utilities or gases required, only AC power Diagnostic Analysis down water for gas turbines. Compliant to ASTM D6595 (In service Lubricant) and ASTM D6728 (Fuel) ■ User defined limits for each test ■ Data rated as Notable, Abnormal, and Severe for both The SpectrOil M Series is widely used “Hi” and “Lo” limits in commercial and military aviation, ■ Default and customizable diagnostic recommendations with ground transportation, mining, power SpectrOil M Series includes the following models: historical trending generation and commercial in service ■ Alarm Limits specific to Component Type, Manufacturer, oil analysis laboratories. Model, and Application MODEL APPLICATIONS DEFAULT CALIBRATION PROGRAM M/C-W In service oil analysis for military, mining, oil & gas and 24 elements for lubricant and hydraulics Evaluation commercial laboratories in remote locations ■ Results color-coded with severity level ■ Evaluator assigns overall sample severity and comments M/F-W Fuel quality control for power plant turbines and diesel/ 15 elements for light fuel and heavy fuel gas engines Reports ■ Mult-language support M/F-LD No.2 diesel quality control for gas turbines, ultra low 15 elements for No.2 Diesel, ultra low ■ Printed or emailed to assigned recipient or accessed by the web SpectroTrack oil analysis report of limits of detection for alkali metals and vanadium limits of detection ■ Test results, graphs, comments, and particle images multi-site, power generation turbines. ■ Interactive portal reports M/N-W Only approved oil analysis elemental spectrometer for 15 elements for JOAP aerospace, marine and ground support for US DoD Joint Oil Analysis Program (JOAP)
Spectro Scientific | One Executive Drive, Suite 101, Chelmsford, MA 01824-2563 978-431-1120 | www.spectrosci.com | [email protected] | An ISO 9001:2008 company Copyright © 2017 Spectro Scientific. All rights reserved. While every effort is made to assure the information in this document is accurate, Spectro Scientific does not accept liability for any errors or mistakes that may arise. Specifications are subject to change without notice. SPECTROTRACK_DSv3_2017-06-26 64 | Product Catalog Feature Overview SpectroTrack Product Information ■ Self-contained installation on one server ■ Automatically retrieves data from all Spectro Inc. instruments PART NUMBERS AND ADDITIONAL CONFIGURATION OPTIONS ■ Designed specifically for oil analysis programs – dedicated or M90035 Base Product contract testing M90038 Additional Laboratory User License (each) ■ Supports customer (private label) branding M90036 SpectroTrack Custom Device Interface Remote Login Import driver interface for lab instruments (Spectro products ■ Laboratory customer (interactive report viewers) can access included in base product defined data ■ Remote portals can be connected to the Internet M90037 Client Portal Access Pack (101-500 Clients) Accounts M90042 Multi Lab Option – Resides on Main server SpectrOil M Series ■ Laboratory user accounts and client accounts password protected Allows multiple labs to share and access SpectroTrack on main server. All laboratory users with rights can access and ■ Multi user accounts for distributor sales or corporate reliability diagnose oil samples from all labs. Each lab must have P/N OIL ANALYSIS SPECTROMETER grouping M90035 Standard for rugged spectrometric oil analysis in the field Equipment ACCESSORIES ■ Assigned to accounts and can be searched, created, removed M90039 SpectroTrack Customer Reference Guide (Print ) and reactivated with ease ■ Detail includes manufacturer, application and components M90041 SpectroTrack Laboratory Reference Guide (Print) ■ Maintenance feedback and notes visible to all stakeholders P-10885 SpectroTrack Labelwriter Components P-10886 SpectroTrack Lab Barcode Labels (750/roll) Originally designed for military applications in the mid 1990s, the SpectrOil M is the only ■ Rich customer component detail, complete with assigned test P-10887 SpectroTrack Customer Labels (300/roll) The SpectrOil M Series RDE-OES in service oil analysis spectrometer approved by the US Department of Defense (DoD) Joint package Oil Analysis Program (JOAP). Since its development, the SpectrOil M has been the industry I&T Installation & Training Elemental Analyzer is a compact, ■ Can be easily transferred to other equipment (engine change) rugged, transportable spectrometer standard for reliable, deployable spectrometers that perform the rapid analysis of wear RECOMMENDED HARDWARE Scheduling designed for accurate elemental metals, contaminants and additives in lubricants, hydraulic fluids, fuels, coolants and water. ■ Schedule maintenance activities and analysis intervals Server x64 Processor: AMD Opteron, AMD Athlon 64, Intel Xeon with analysis of a variety of fluids tested Processor Intel EM64T support, Intel Pentium IV with EM64T support ■ Automatic reminders sent via email in the field or in a laboratory. Using SpectrOil M Series key features ■ Customer bottle labels printed prior to submittal x86 Processor: Pentium III-compatible processor or faster the proven, reliable rotating disc Rugged frame and optics system that meets military shock and vibration and RAM 4 GB Sample Login electrode (RDE) technique, the environmental test standards (JOAP CID-0191) ■ Auto-fill and drop-down selection Hard Drive 500 GB analyzer measures trace quantities of Designed for remote locations and frequent transportation elements dissolved or suspended as Data Entry Operating Windows XP, Windows Server 2008 R2 Standard, No sample preparation required systems Windows 7 Professional Edition or Higher, fine particles in natural or synthetic ■ Bar code tracking bottle labels 30 second analysis time Windows Vista Professional Edition or Higher OIL ANALYSIS LABORATORY INSTRUMENTS ■ petroleum-based products. It includes Shows status of each batch as it moves through the laboratory Analyzes up to 31 elements simultaneously ■ new and in-service lubricants, Automatic data collection from Spectro instruments Self-sustained with built-in industrial touch panel PC –Expandable with other vendor-supplied instruments hydraulic fluids, light (gasoline or Simple to operate; does not require special training ■ Laboratory dashboard for easy workflow management diesel) or heavy fuels (HFO), coolants, industrial process water or wash- No special utilities or gases required, only AC power Diagnostic Analysis down water for gas turbines. Compliant to ASTM D6595 (In service Lubricant) and ASTM D6728 (Fuel) ■ User defined limits for each test ■ Data rated as Notable, Abnormal, and Severe for both The SpectrOil M Series is widely used “Hi” and “Lo” limits in commercial and military aviation, ■ Default and customizable diagnostic recommendations with ground transportation, mining, power SpectrOil M Series includes the following models: historical trending generation and commercial in service ■ Alarm Limits specific to Component Type, Manufacturer, oil analysis laboratories. Model, and Application MODEL APPLICATIONS DEFAULT CALIBRATION PROGRAM M/C-W In service oil analysis for military, mining, oil & gas and 24 elements for lubricant and hydraulics Evaluation commercial laboratories in remote locations ■ Results color-coded with severity level ■ Evaluator assigns overall sample severity and comments M/F-W Fuel quality control for power plant turbines and diesel/ 15 elements for light fuel and heavy fuel gas engines Reports ■ Mult-language support M/F-LD No.2 diesel quality control for gas turbines, ultra low 15 elements for No.2 Diesel, ultra low ■ Printed or emailed to assigned recipient or accessed by the web SpectroTrack oil analysis report of limits of detection for alkali metals and vanadium limits of detection ■ Test results, graphs, comments, and particle images multi-site, power generation turbines. ■ Interactive portal reports M/N-W Only approved oil analysis elemental spectrometer for 15 elements for JOAP aerospace, marine and ground support for US DoD Joint Oil Analysis Program (JOAP)
Spectro Scientific | One Executive Drive, Suite 101, Chelmsford, MA 01824-2563 978-431-1120 | www.spectrosci.com | [email protected] | An ISO 9001:2008 company Copyright © 2017 Spectro Scientific. All rights reserved. While every effort is made to assure the information in this document is accurate, Spectro Scientific does not accept liability for any errors or mistakes that may arise. Specifications are subject to change without notice. SPECTROTRACK_DSv3_2017-06-26 64 | Product Catalog Product Catalog | 65 Laboratory SpectrOil M Series consists of three main components Available calibration programs (can be added to every model) 1. Excitation Source – introduces energy to the sample. This includes a high voltage AC Precision source that applies voltage across a small gap formed by the highly purified graphite rod CALIBRATION DESCRIPTION STANDARDS and disc with the disc rotating and picking up oil from the sample holder under it. Lubricating oil Detects and quantifies elemental wear CS-75-500 Base oil SpectrOil M is a rugged and precise (Commercial) and additives in lubricants. Conforms 2. Optical System – At the core of the spectrometer is a Rowland circle grating optics to ASTM-D6595. Default 24 elements, CS-24-100-200G 24 elements, 100 ppm Rotating Disc Electrode Optical system with 400 mm focal length. The temperature of the optics is tightly controlled at up to 31 elements SMA-900-200G 5 elements, 900 ppm Emission Spectrometer (RDE-OES). 40°C for the most stable result. Fourteen CCD array chips are precisely aligned on the edge of the optics. Light emitted from the burning sample is transmitted by optical fiber Fuel Detects quality and contamination of CS-75-500 Base Oil Measures sub-ppm elemental (Light and petrochemicals from crude through the concentrations with high-purity carbon into the optics and diffracted by the grating into different wavelengths and picked up by heavy fuel) final blended light fuels. Conforms to CS-GT15-10 10 ppm for light fuel the CCD chips. ASTM D-6728. It includes both light electrodes CS-GT15-100 100 ppm for heavy fuel 3. Readout System – detects and measures the light that has been separated into its and heavy fuel calibration programs. Detects elements in solution or particles as large as 10μm with component wavelengths by the optical system and presents this information to the Low Special calibration for #2 Diesel with CS-HP-100 High purity base oil Detection (LD) low limits of detection for alkali metals RDE’s precise pulsed-power, operator in a usable fashion. Diesel and vanadium. Specifically, the LOD CS-GT15-10 10 ppm, 15 elements high-temperature plasma A specific calibration program is applied to raw spectrum which eliminates the matrix of V is down to 0.1ppm, critical to meet turbine OEM specifications for CS-GT15-100 100 ppm, 15 elements Accurately identifies elements in a effect, so results are compliant to ASTM standards. Then, the user only needs to select the diesel fuel quality control wide variety of substances without calibration profile for specific fluids. So, switching from oil to fuel to coolant or water only 300-00010 1 ppm for Li, Na, K, V sample preparation or dilution takes seconds, not hours like ICP and other instruments. 600-00111 0.2 ppm for V Transit Case Coolant/Glycol Analyzes in service coolants JDIW DI water (water glycol mix) for additives and A transit case was designed for contamination SIGLYCOLSTD-500 Diluted glycol standard military personnel to transport the Process water Measures contamination in a variety of STE006 KIT DI water and 5ppm SpectrOil M where it is needed. applications like power plant cooling standard A hydraulic lifting system is water and turbine wash-down water carefully balanced to the right of JOAP Airforce JOAP Airforce calibration with D19-0 Base Oil the SpectrOil so it is easily raised 15 elements. Results correlate to Grating SpectrOil M/N-W D12-100 12 elements, 100ppm without effort. Four lifting rods are supplied with the SpectrOil M; D3-100 Zn, Mo, B, 100ppm Exit Slits they can be mounted on the unit so JOAP Army JOAP Army calibration with 20 D19-0 Base Oil two people can quickly transfer the elements. Results correlate to SpectrOil M/N-W D12-100 12 elements, 100ppm SpectrOil M from the transit case to a table top, and vice versa. D3-100 Zn, Mo, B, 100ppm
CCDs CS-24-100-200G 24 elements, 10ppm Fixed Ele trode SMA-900-200G 5 elements, 900ppm Entran e Slit Opti s diffra tion AC Ar grating prod e a spe tr m Consumables used by calibration programs Fi er Opti Rotating Ca le To ensure accurate and stable measurement results, different consumables are used for Ele trode different calibration programs. Only Spectro Scientific certified consumables are qualified to meet performance specifications. Sample C p CALIBRATION PROGRAMS DISC ROD SAMPLE HOLDER (CUP) Lubricant, coolant, water M97008 M97009 P-10524 high temperature sample cup (black)
Light, heavy fuel, LD fuel M97008 M97009 P-10524 high temperature sample cup (black) Schematic of how a SpectrOil analyzes a fluid M90204 sample cover for low flash point fuels sample to determine sub-ppm elemental content JOAP Airforce and Army M97200 M97201 M90909 Aluminum boat sample holder
66 | Product Catalog Laboratory SpectrOil M Series consists of three main components Available calibration programs (can be added to every model) 1. Excitation Source – introduces energy to the sample. This includes a high voltage AC Precision source that applies voltage across a small gap formed by the highly purified graphite rod CALIBRATION DESCRIPTION STANDARDS and disc with the disc rotating and picking up oil from the sample holder under it. Lubricating oil Detects and quantifies elemental wear CS-75-500 Base oil SpectrOil M is a rugged and precise (Commercial) and additives in lubricants. Conforms 2. Optical System – At the core of the spectrometer is a Rowland circle grating optics to ASTM-D6595. Default 24 elements, CS-24-100-200G 24 elements, 100 ppm Rotating Disc Electrode Optical system with 400 mm focal length. The temperature of the optics is tightly controlled at up to 31 elements SMA-900-200G 5 elements, 900 ppm Emission Spectrometer (RDE-OES). 40°C for the most stable result. Fourteen CCD array chips are precisely aligned on the edge of the optics. Light emitted from the burning sample is transmitted by optical fiber Fuel Detects quality and contamination of CS-75-500 Base Oil Measures sub-ppm elemental (Light and petrochemicals from crude through the concentrations with high-purity carbon into the optics and diffracted by the grating into different wavelengths and picked up by heavy fuel) final blended light fuels. Conforms to CS-GT15-10 10 ppm for light fuel the CCD chips. ASTM D-6728. It includes both light electrodes CS-GT15-100 100 ppm for heavy fuel 3. Readout System – detects and measures the light that has been separated into its and heavy fuel calibration programs. Detects elements in solution or particles as large as 10μm with component wavelengths by the optical system and presents this information to the Low Special calibration for #2 Diesel with CS-HP-100 High purity base oil Detection (LD) low limits of detection for alkali metals RDE’s precise pulsed-power, operator in a usable fashion. Diesel and vanadium. Specifically, the LOD CS-GT15-10 10 ppm, 15 elements high-temperature plasma A specific calibration program is applied to raw spectrum which eliminates the matrix of V is down to 0.1ppm, critical to meet turbine OEM specifications for CS-GT15-100 100 ppm, 15 elements Accurately identifies elements in a effect, so results are compliant to ASTM standards. Then, the user only needs to select the diesel fuel quality control wide variety of substances without calibration profile for specific fluids. So, switching from oil to fuel to coolant or water only 300-00010 1 ppm for Li, Na, K, V sample preparation or dilution takes seconds, not hours like ICP and other instruments. 600-00111 0.2 ppm for V Transit Case Coolant/Glycol Analyzes in service coolants JDIW DI water (water glycol mix) for additives and A transit case was designed for contamination SIGLYCOLSTD-500 Diluted glycol standard military personnel to transport the Process water Measures contamination in a variety of STE006 KIT DI water and 5ppm SpectrOil M where it is needed. applications like power plant cooling standard A hydraulic lifting system is water and turbine wash-down water carefully balanced to the right of JOAP Airforce JOAP Airforce calibration with D19-0 Base Oil the SpectrOil so it is easily raised 15 elements. Results correlate to Grating SpectrOil M/N-W D12-100 12 elements, 100ppm without effort. Four lifting rods are supplied with the SpectrOil M; D3-100 Zn, Mo, B, 100ppm Exit Slits they can be mounted on the unit so OIL ANALYSIS LABORATORY INSTRUMENTS JOAP Army JOAP Army calibration with 20 D19-0 Base Oil two people can quickly transfer the elements. Results correlate to SpectrOil M/N-W D12-100 12 elements, 100ppm SpectrOil M from the transit case to a table top, and vice versa. D3-100 Zn, Mo, B, 100ppm
CCDs CS-24-100-200G 24 elements, 10ppm Fixed Ele trode SMA-900-200G 5 elements, 900ppm Entran e Slit Opti s diffra tion AC Ar grating prod e a spe tr m Consumables used by calibration programs Fi er Opti Rotating Ca le To ensure accurate and stable measurement results, different consumables are used for Ele trode different calibration programs. Only Spectro Scientific certified consumables are qualified to meet performance specifications. Sample C p CALIBRATION PROGRAMS DISC ROD SAMPLE HOLDER (CUP) Lubricant, coolant, water M97008 M97009 P-10524 high temperature sample cup (black)
Light, heavy fuel, LD fuel M97008 M97009 P-10524 high temperature sample cup (black) Schematic of how a SpectrOil analyzes a fluid M90204 sample cover for low flash point fuels sample to determine sub-ppm elemental content JOAP Airforce and Army M97200 M97201 M90909 Aluminum boat sample holder
66 | Product Catalog Product Catalog | 67 SpectrOil M Series Product Information
Lubricant Light Heavy Fuel Low Glycol/ PRODUCT INFORMATION Element Lubricant Extended Fuel Fuel Detection Coolant Part Numbers Spectro-M/C-W, Spectro-M/F-W Spectro-M/F-W, Spectro-M/C/R-W Ag 0 - 1000 Spectro-M/N/R-W Al 0 - 1000 0 - 50 0 - 500 0 - 100 0 - 50 Applications new and in service lubricant, hydraulic, light or heavy As 0 - 100 fuel, water/glycol mix, water B 0 - 1000 0 - 1,000 Output mg/kg (ppm) Ba 0 - 6,000 ASTM D6595 (Oil), D6728 (Fuel) Bi 0 - 100 Ca 0 - 6,000 0 - 50 0 - 500 0 - 100 0 - 50 Calibration Factory set, no re-calibration needed Cd 0 - 1000 SpectrOil 100 Series HARDWARE SPECIFICATIONS Ce 0 - 100 Excitation Source Oscillatory arc discharge Co 0 - 100 MARKET-LEADING RDE-OES SPECTROMETER Optical System Rowland Circle polychromator Optic. Cr 0 - 1000 0 - 50 0 - 500 0 - 100 FOR ELEMENTAL ANALYSIS Temperature controlled at 40°C +/- 1C Cu 0 - 1000 0 - 50 0 - 500 0 - 100 0 - 50 Spectral Range 203 nm to 810 nm Fe 0 - 1000 0 - 50 0 - 500 0 - 100 0 - 50 Detectors CCD array In 0 - 100 K 0 - 1000 0 - 50 0 - 500 0 - 100 0 - 10,000 OPERATIONAL SPECIFICATIONS Li 0 - 1000 0 - 50 0 - 500 0 - 100 Sample Volume 2 ml of fluid Mg 0 - 6,000 0 - 150 0 - 1,500 0 - 100 0 - 50 The precision of SpectrOil 100 makes it an essential fluids analysis Ambient Operating 0 to 40°C (32F to 104F) Mn 0 - 1000 0 - 50 0 - 500 0 - 100 Temperature SpectrOil Advantage tool in QC labs, and its simplicity and ease of use brings these Mo 0 - 1000 0 - 500 reliable measurements to on-site predictive maintenance teams. Relative Humidity 0 to 90%, non-condensing Na 0 - 6,000 0 - 50 0 - 500 0 - 100 0 - 10,000 SpectrOil RDE technology is a proven USER INTERFACE SPECIFICATIONS Ni 0 - 1000 0 - 50 0 - 500 0 - 100 means of precisely determining The SpectrOil 100 is a Rotating Disk Electrode, Optical Emission Spectrometer (RDE-OES) elemental composition in engine Operating System Windows 7 Pro; Software – SpectrOil V8 P 0 - 6,000 0 - 2,500 built upon decades of technology development in support of the U.S. Military’s Joint Oil oil, coolant, fuels, grease, process Pb 0 - 1000 0 - 50 0 - 500 0 - 100 0 - 50 Analysis Program (JOAP). This robust technology enables measurements to be made PC and Display Industrial touch panel PC, 12” diplay water, and a wide variety of critical Sb 0- 100 Data Storage Internal PC, USB, CD-RW operating fluids. For decades this quickly and accurately on a variety of fluid types for condition monitoring and QC. Si 0 - 1000 0 - 50 0 - 500 0 - 100 0 - 500 POWER REQUIREMENTS robust technology has been used Sn 0 - 1000 Provides precise and reliable results as both a quality control tool and Voltage Input AC 120/240V, 50/60Hz Ti 0 - 1000 machine health monitor. Simultaneous multi-element analysis SpectrOil 110 – Power Consumption 1000 Watts at test V 0 - 1000 0 - 50 0 - 500 0 - 100 Repeatable and sensitive fluid characterization Basic Engine Wear package MECHANICAL SPECIFICATIONS W 0 - 100 MACHINE HEALTH Conforms to ASTM-D6595 (oil), and ASTM-D6728 (fuel) (15 essential elements) Zn 0 - 6,000 0 - 50 0 - 500 0 - 100 0 - 50 Oil is the lifeblood of equipment and Dimensions 80 cm (L) x 63.5 cm (W) x 70 cm (H) Fast and easy to operate SpectrOil 120 – (31.5 in x 25 in x 27 in) M/C, M/N, M/F Zr 0 - 100 thus oil analysis provides unique No sample preparation required Standard (24 elements) & insights into machinery health. Weights 114 kg (250 lbs) M/C, M/N, M/F No solvents or gasses required Extended Range packages 132 kg (290 lbs) M/C/R, M/N/R As a result, wear metals analysis Quick 30 second analysis time (31+ elements); options with SpectrOil 100 is the backbone include Wear Metals, Shipping Dimensions 102 cm (L) x 91 cm (W) x 94 cm (H) Robotics Option Minimal training/background required to operate (40 in x 36 in x 37 in ) for M/C, M/N, M/F of used oil analysis programs and Coolants, Fuels and custom 152 cm (L) x 91 cm (W) x 94 cm (H) The Double Disc Rapid Robot (D2R2) enables effective condition based Immediate results on-site application packages (60 in x 36 in x 37 in ) for M/C/R, M/N/R autosampler is a factory configured maintenance programs. Analysis at your facility Shipping Weights 261 kg (575 lbs) M/C, M/N, M/F option for the SpectrOil M/C or SpectrOil FLUID QUALITY CONTROL Bench-top, transportable system 295 kg (650 lbs) M/C/R, M/N/R M/N spectrometers that provides The precision of RDE spectrometry Low cost per sample automatic operation of used oil sample enables reliable, low concentration analysis. The SpectrOil D2R2 does not measurement of additive packages or use the traditional rod electrode used in harmful contaminants in virgin fuels, MODEL 110E 120C 120F 120M manual systems. A specially designed blended oil, coolants and wash down rotrode disc is used, allowing for water. Number of Elements 15 24 15 15 unattended operation. Default Calibration Lubricating Oils Lubricating Oils Light/Heavy Fuel JOAP
Optional Calibrations No Yes Yes Yes
Spectro Scientific | One Executive Drive, Suite 101, Chelmsford, MA 01824-2563 978-431-1120 | www.spectrosci.com | [email protected] | An ISO 9001:2008 company Copyright © 2017 Spectro Scientific. All rights reserved. While every effort is made to assure the information in this document is accurate, Spectro Scientific does not accept liability for any errors or mistakes that may arise. Specifications are subject to change without notice. SpectrOil M Series_DSv3_2017-08-28 68 | Product Catalog SpectrOil M Series Product Information
Lubricant Light Heavy Fuel Low Glycol/ PRODUCT INFORMATION Element Lubricant Extended Fuel Fuel Detection Coolant Part Numbers Spectro-M/C-W, Spectro-M/F-W Spectro-M/F-W, Spectro-M/C/R-W Ag 0 - 1000 Spectro-M/N/R-W Al 0 - 1000 0 - 50 0 - 500 0 - 100 0 - 50 Applications new and in service lubricant, hydraulic, light or heavy As 0 - 100 fuel, water/glycol mix, water B 0 - 1000 0 - 1,000 Output mg/kg (ppm) Ba 0 - 6,000 ASTM D6595 (Oil), D6728 (Fuel) Bi 0 - 100 Ca 0 - 6,000 0 - 50 0 - 500 0 - 100 0 - 50 Calibration Factory set, no re-calibration needed Cd 0 - 1000 SpectrOil 100 Series HARDWARE SPECIFICATIONS Ce 0 - 100 Excitation Source Oscillatory arc discharge Co 0 - 100 MARKET-LEADING RDE-OES SPECTROMETER Optical System Rowland Circle polychromator Optic. Cr 0 - 1000 0 - 50 0 - 500 0 - 100 FOR ELEMENTAL ANALYSIS Temperature controlled at 40°C +/- 1C Cu 0 - 1000 0 - 50 0 - 500 0 - 100 0 - 50 Spectral Range 203 nm to 810 nm Fe 0 - 1000 0 - 50 0 - 500 0 - 100 0 - 50 Detectors CCD array In 0 - 100 K 0 - 1000 0 - 50 0 - 500 0 - 100 0 - 10,000 OPERATIONAL SPECIFICATIONS Li 0 - 1000 0 - 50 0 - 500 0 - 100 Sample Volume 2 ml of fluid Mg 0 - 6,000 0 - 150 0 - 1,500 0 - 100 0 - 50 The precision of SpectrOil 100 makes it an essential fluids analysis Ambient Operating 0 to 40°C (32F to 104F) Mn 0 - 1000 0 - 50 0 - 500 0 - 100 Temperature SpectrOil Advantage tool in QC labs, and its simplicity and ease of use brings these Mo 0 - 1000 0 - 500 reliable measurements to on-site predictive maintenance teams. Relative Humidity 0 to 90%, non-condensing Na 0 - 6,000 0 - 50 0 - 500 0 - 100 0 - 10,000 SpectrOil RDE technology is a proven USER INTERFACE SPECIFICATIONS Ni 0 - 1000 0 - 50 0 - 500 0 - 100 means of precisely determining The SpectrOil 100 is a Rotating Disk Electrode, Optical Emission Spectrometer (RDE-OES) elemental composition in engine Operating System Windows 7 Pro; Software – SpectrOil V8 P 0 - 6,000 0 - 2,500 built upon decades of technology development in support of the U.S. Military’s Joint Oil oil, coolant, fuels, grease, process Pb 0 - 1000 0 - 50 0 - 500 0 - 100 0 - 50 Analysis Program (JOAP). This robust technology enables measurements to be made PC and Display Industrial touch panel PC, 12” diplay water, and a wide variety of critical Sb 0- 100 Data Storage Internal PC, USB, CD-RW operating fluids. For decades this quickly and accurately on a variety of fluid types for condition monitoring and QC. Si 0 - 1000 0 - 50 0 - 500 0 - 100 0 - 500 POWER REQUIREMENTS robust technology has been used Sn 0 - 1000 Provides precise and reliable results as both a quality control tool and Voltage Input AC 120/240V, 50/60Hz Ti 0 - 1000 machine health monitor. Simultaneous multi-element analysis SpectrOil 110 –
Power Consumption 1000 Watts at test V 0 - 1000 0 - 50 0 - 500 0 - 100 Repeatable and sensitive fluid characterization Basic Engine Wear package OIL ANALYSIS LABORATORY INSTRUMENTS MECHANICAL SPECIFICATIONS W 0 - 100 MACHINE HEALTH Conforms to ASTM-D6595 (oil), and ASTM-D6728 (fuel) (15 essential elements) Zn 0 - 6,000 0 - 50 0 - 500 0 - 100 0 - 50 Oil is the lifeblood of equipment and Dimensions 80 cm (L) x 63.5 cm (W) x 70 cm (H) Fast and easy to operate SpectrOil 120 – (31.5 in x 25 in x 27 in) M/C, M/N, M/F Zr 0 - 100 thus oil analysis provides unique No sample preparation required Standard (24 elements) & insights into machinery health. Weights 114 kg (250 lbs) M/C, M/N, M/F No solvents or gasses required Extended Range packages 132 kg (290 lbs) M/C/R, M/N/R As a result, wear metals analysis Quick 30 second analysis time (31+ elements); options with SpectrOil 100 is the backbone include Wear Metals, Shipping Dimensions 102 cm (L) x 91 cm (W) x 94 cm (H) Robotics Option Minimal training/background required to operate (40 in x 36 in x 37 in ) for M/C, M/N, M/F of used oil analysis programs and Coolants, Fuels and custom 152 cm (L) x 91 cm (W) x 94 cm (H) The Double Disc Rapid Robot (D2R2) enables effective condition based Immediate results on-site application packages (60 in x 36 in x 37 in ) for M/C/R, M/N/R autosampler is a factory configured maintenance programs. Analysis at your facility Shipping Weights 261 kg (575 lbs) M/C, M/N, M/F option for the SpectrOil M/C or SpectrOil FLUID QUALITY CONTROL Bench-top, transportable system 295 kg (650 lbs) M/C/R, M/N/R M/N spectrometers that provides The precision of RDE spectrometry Low cost per sample automatic operation of used oil sample enables reliable, low concentration analysis. The SpectrOil D2R2 does not measurement of additive packages or use the traditional rod electrode used in harmful contaminants in virgin fuels, MODEL 110E 120C 120F 120M manual systems. A specially designed blended oil, coolants and wash down rotrode disc is used, allowing for water. Number of Elements 15 24 15 15 unattended operation. Default Calibration Lubricating Oils Lubricating Oils Light/Heavy Fuel JOAP
Optional Calibrations No Yes Yes Yes
Spectro Scientific | One Executive Drive, Suite 101, Chelmsford, MA 01824-2563 978-431-1120 | www.spectrosci.com | [email protected] | An ISO 9001:2008 company Copyright © 2017 Spectro Scientific. All rights reserved. While every effort is made to assure the information in this document is accurate, Spectro Scientific does not accept liability for any errors or mistakes that may arise. Specifications are subject to change without notice. SpectrOil M Series_DSv3_2017-08-28 68 | Product Catalog Product Catalog | 69 SpectrOil 100 Series Laboratory Precision On-site Simplicity At the core of the SpectrOil 100 is a precision Rotating Disk Electrode, The simplicity and ease of using the SpectrOil 100 enables RDE technology to Optical Emission Spectrometer (RDE-OES). be brought to on-site inspection and condition based maintenance sites.
■ Measure sub-ppm elemental concentrations with high-purity carbon ■ The disposable electrodes & sample cup facilitate rapid sample electrodes. changes and ensure contamination free measurements. ■ Detect elements in solution or particles as large as 10μm with RDE’s ■ Without the purge gas or sample dilution required by other precision pulsed-power, high-temperature plasma. technologies, the simple RDE-OES steps are: Pour your fluid, ■ Accurately identify elements in a wide variety of substances close the door, and press START. without sample preparation or dilution. ■ The sophisticated analytics are automated, so no highly skilled or trained users are required. Just follow the simple steps and read the elemental results.
HOW IT WORKS APPLICATIONS
The RDE-OES technology utilizes a high-purity carbon electrode to transmit Oil & Grease Condition Monitoring high-voltage electricity across a small gap to a nearby carbon disk. The rotating Detecting and quantifying elemental wear in lubricants enables a rapid, non-invasive disk is partially submerged in a miniature cup of fluid sample and continuously determination of machine condition, while monitoring for additive depletion ensures that carries the sample into the electrical discharge gap between electrodes. When lubricating fluids continue to protect critical assets according to ASTM-D6595. the electricity arcs across the gap containing the sample, it forms a high- WEAR: Quantify elemental composition of wear temperature plasma which emits a unique, sample-dependent spectrum of light debris to determine the location and severity of from the ultraviolet, through the visible, and into the infrared wavelengths. component wear. The emitted light is collected and fiber-optically coupled to the SpectrOil 100’s sensitive optics which includes a diffraction grating to sort the light by CONTAMINATION: Detect unexpected elements to wavelength and focus it onto indicate fouled air filters, coolant leaks, sea water an array of highly sensitive CCD ingress, or dirt ingestion. Grating cameras. Sophisticated spectral CHEMISTRY: Measure additive package depletion to Exit Slits analysis software processes ensure expected oil protection. the CCDs’ spectra to precisely determine concentration of Fuel & Lubricant Quality Control
CCDs dozens of elements with SpectrOil is used to ensure composition and quality of petrochemicals from crude through the final Fixed Ele trode sub-ppm precision. blended product to ensure that processing is acceptable and to protect finished fuel against trace Entran e Slit contamination through handling, storage, and to the user in accordance with ASTM D-6728. Opti s diffra tion AC Ar grating prod e a spe tr m Coolant Condition Measurements Fi er Opti Rotating Ca le Ele trode Analyzing in-service coolant is a quick and accurate means of ensuring that it continues to provide the required corrosion protection and heat transfer. Sample C p Process Water Condition Analysis
Schematic of how a SpectrOil analyzes a fluid Measuring contamination in a variety of applications like power plant cooling water and turbine sample to determine sub-ppm elemental content. wash water provides unique system condition insights and ensures compliant disposal or reuse.
70 | Product Catalog *Trivector is a trademark of Emerson Process Systems SpectrOil 100 Series Laboratory Precision On-site Simplicity At the core of the SpectrOil 100 is a precision Rotating Disk Electrode, The simplicity and ease of using the SpectrOil 100 enables RDE technology to Optical Emission Spectrometer (RDE-OES). be brought to on-site inspection and condition based maintenance sites.
■ Measure sub-ppm elemental concentrations with high-purity carbon ■ The disposable electrodes & sample cup facilitate rapid sample electrodes. changes and ensure contamination free measurements. ■ Detect elements in solution or particles as large as 10μm with RDE’s ■ Without the purge gas or sample dilution required by other precision pulsed-power, high-temperature plasma. technologies, the simple RDE-OES steps are: Pour your fluid, ■ Accurately identify elements in a wide variety of substances close the door, and press START. without sample preparation or dilution. ■ The sophisticated analytics are automated, so no highly skilled or trained users are required. Just follow the simple steps and read the elemental results.
HOW IT WORKS APPLICATIONS
The RDE-OES technology utilizes a high-purity carbon electrode to transmit Oil & Grease Condition Monitoring high-voltage electricity across a small gap to a nearby carbon disk. The rotating Detecting and quantifying elemental wear in lubricants enables a rapid, non-invasive disk is partially submerged in a miniature cup of fluid sample and continuously determination of machine condition, while monitoring for additive depletion ensures that carries the sample into the electrical discharge gap between electrodes. When lubricating fluids continue to protect critical assets according to ASTM-D6595. the electricity arcs across the gap containing the sample, it forms a high- WEAR: Quantify elemental composition of wear OIL ANALYSIS LABORATORY INSTRUMENTS temperature plasma which emits a unique, sample-dependent spectrum of light debris to determine the location and severity of from the ultraviolet, through the visible, and into the infrared wavelengths. component wear. The emitted light is collected and fiber-optically coupled to the SpectrOil 100’s sensitive optics which includes a diffraction grating to sort the light by CONTAMINATION: Detect unexpected elements to wavelength and focus it onto indicate fouled air filters, coolant leaks, sea water an array of highly sensitive CCD ingress, or dirt ingestion. Grating cameras. Sophisticated spectral CHEMISTRY: Measure additive package depletion to Exit Slits analysis software processes ensure expected oil protection. the CCDs’ spectra to precisely determine concentration of Fuel & Lubricant Quality Control
CCDs dozens of elements with SpectrOil is used to ensure composition and quality of petrochemicals from crude through the final Fixed Ele trode sub-ppm precision. blended product to ensure that processing is acceptable and to protect finished fuel against trace Entran e Slit contamination through handling, storage, and to the user in accordance with ASTM D-6728. Opti s diffra tion AC Ar grating prod e a spe tr m Coolant Condition Measurements Fi er Opti Rotating Ca le Ele trode Analyzing in-service coolant is a quick and accurate means of ensuring that it continues to provide the required corrosion protection and heat transfer. Sample C p Process Water Condition Analysis
Schematic of how a SpectrOil analyzes a fluid Measuring contamination in a variety of applications like power plant cooling water and turbine sample to determine sub-ppm elemental content. wash water provides unique system condition insights and ensures compliant disposal or reuse.
70 | Product Catalog *Trivector is a trademark of Emerson Process Systems *Trivector is a trademark of EmersonProduct CatalogProcess |Systems 71 SpectrOil 100 Product Information SpectrOil Models and Calibration Ranges in ppm › Ferrous content › PRODUCT INFORMATION 110E 120C 120F Wear particle shape BASIC STANDARD EXTENDED COOLANT › Part # Spectro-[Model]-[Hz]-[Volts] APPLICATION FUELS Particle count ENGINE LUBRICANTS OPTION and codes Applications Mineral and synthetic lubricants, distilled fuel, heavy fuel oil (HFO), crude, glycol coolants and turbine Ag 0 - 1000 0 - 1000 washdown water Al 0 - 1000 0 - 1000 0 - 50 0 - 500 Output Concentration mg/kg (ppm) As 0 - 100 B 0 - 1000 0 - 1000 0 - 1,000 Methodology ASTM D6595; D6728 Ba 0 - 6,000 Standard Analytical Up to 31 elements from Li to Pb Bi 0 - 100 Range Typically 0-1000ppm (varies by application) Ca 0 - 3,000 0 - 6,000 0 - 50 0 - 500 Calibration Factory set, no maintenance required Cd 0 - 1000 LaserNet 200 Series Excitation Source Oscillatory arc discharge, JOAP characteristic Ce 0 - 100 Co 0 - 100 PARTICLE COUNTER, WEAR CLASSIFIER, FERROUS MONITOR OPTICAL SYSTEM Cr 0 - 1000 0 - 1000 0 - 500 Optical System Pashen-Runge polychromatar optic Cu 0 - 1000 0 - 1000 0 - 50 0 - 500 (Rowland Circle Alignment) Fe 0 - 1000 0 - 1000 0 - 50 0 - 500 Spectral Range 203 nm to 810 nm In 0 - 100 Temperature Control Thermally Stabilized; 40°C ± 1°C K 0 - 1000 0 - 10,000 0 - 500 Detectors CCD proprietary design for frequency range of interest Li 0 - 1000 0 - 500 Mg 0 - 6,000 0 - 50 0 - 1,500 OPERATIONAL SPECIFICATIONS Mn 0 - 1000 0 - 500 The LaserNet 200 Series is much The LaserNet 200 Series is the world’s best particle analyzer Sample Volume 2 mL of fluid Mo 0 - 1000 0 - 1000 0 - 500 more than a particle analyzer. It also for lubrication and hydraulic oil testing. calculates free water in ppm, and Solvents/Reagents None Na 0 - 3,000 0 - 6,000 0 - 10,000 0 - 100 Ni 0 - 1000 0 - 1000 0 - 500 differentiates contaminants (silica) from In commercial laboratories, power generation plants and industrial facilities, the Ambient Operating 0° to 40°C (32°F to 104°F) Temperature P 0 - 3,000 0 - 6,000 0 - 2,500 machine wear (metal). In addition, this LaserNet 200 Series offers unrivaled functionality for contamination control and Relative Humidity 0 to 90%, non-condensing Pb 0 - 1000 0 - 1000 0 - 50 0 - 500 instrument provides particle counts and condition-based maintenance programs. S codes, abnormal wear classification USER INTERFACE SPECIFICATIONS Sb 0 - 100 and ferrous wear measurement. FEATURES INCLUDE: Software/Operating Windows 10 Pro or Windows 7 Pro, 32 or 64 bit, Si 0 - 1000 0 - 1000 0 - 500 0 - 300 ■ Widest range up to 10 million System US English version Sn 0 - 1000 0 - 1000 Particle count, size distribution and codes (ISO 4406, NAS 1638, particles/ml Display External Monitor Ti 0 - 1000 NAVAIR 01-1A-17, SAE AS 4059, GOST, ASTM D6786, HAL and user-defined bins). ■ Automatic wear particle shape Data Storage External PC V 0 - 1000 0 - 500 Differentiation of contaminants (silica and fibers from machine wear metal) W 0 - 100 classification and ferrous particle Data Transfer USB Zn 0 - 3,000 0 - 6,000 0 - 50 0 - 500 analysis Classification of wear particles, image storage and reporting of particle count and Data Entry External Keyboard and Mouse Zr 0 - 100 ■ Imaging of dark fluids containing size for Cutting, Sliding, Fatigue, Fibers and Non-metallics wear types up to 2% soot POWER REQUIREMENTS Total# 15 24 +7 13 15 Ferrous content measurement in the sample with ferrous particle count and size ■ Error correction for water and air distribution Voltage Input AC 120/240V, 50/60 Hz bubbles Power Consumption 500 Watts at test Differentiation of large ferrous particles >25 micron from total ferrous particles. Fusing 10 amps Consumables & Standards Reporting percentage of large ferrous particles and ferrous wear severity index for easy trending and interpretation of the ferrous measurements. MECHANICAL SPECIFICATIONS KITS Dimensions 70.6 cm (H) x 38.4 cm (W) x 66 cm (L) M97007 Consumables Kit for 500 measurements (rod & disk LaserNet Comparison 210 215 220 230 (27.8 in x 15.1 in x 26 in) electrodes, sample cups, pipettes, wipes, cleaning solution, swabs, gloves) Weight 70 kg (154 lbs) Total particle count & codes Multiple configurations and options cover the needs of commercial laboratories M97016 Oil Standards Shipping Package 121.9 cm (H) x 63.5 cm (W) x 109.2 cm (L); Non-metallic particles and industrial plants for contamination control and predictive maintenance. Dimensions (48 in x 25 in x 43 in) M97017 Fuel Standards (sand/dirt) Shipping Package 150 kg (330 lbs) M97018 Fuel Standards, Low Detection OPTIONS INCLUDE: Weight Free water measurement M97019 Water Standards Ferrous Monitor to measure ferrous content – enables measurement of both ferrous COMPLIANCE Air bubble/water droplet M97020 Coolant Standards correction content and total particle count on the same sample, eliminating the need to measure CE Mark: EMC Directive (2004/108/EC); RoHS M96380 Routine Maintenance Kit ferrous content on another instrument Wear particle classification Use Spectro Scientific certified consumables and standards to ensure the accuracy Classification of wear particle shape – directly images wear particle silhouettes and Total ferrous concentration and repeatability of your measurements. counts and classifies wear particles over 20 microns Ferrous particle count & size distribution Autosampler for high throughput sample processing – provides automated, unattended processing of up to 24 used oil or hydraulic fluid samples | Large ferrous concentration Spectro Scientific One Executive Drive, Suite 101, Chelmsford, MA 01824-2563 978-431-1120 | www.spectrosci.com | [email protected] | An ISO 9001:2008 company Autosampler option Copyright © 2017 Spectro Scientific. All rights reserved. While every effort is made to assure the information in this document is accurate, Spectro Scientific does not accept liability for any errors or mistakes that may arise. Specifications are subject to change without notice. SpectrOil100_DSv3_2017-08-30 72 | Product Catalog SpectrOil 100 Product Information SpectrOil Models and Calibration Ranges in ppm › Ferrous content › PRODUCT INFORMATION 110E 120C 120F Wear particle shape BASIC STANDARD EXTENDED COOLANT › Part # Spectro-[Model]-[Hz]-[Volts] APPLICATION FUELS Particle count ENGINE LUBRICANTS OPTION and codes Applications Mineral and synthetic lubricants, distilled fuel, heavy fuel oil (HFO), crude, glycol coolants and turbine Ag 0 - 1000 0 - 1000 washdown water Al 0 - 1000 0 - 1000 0 - 50 0 - 500 Output Concentration mg/kg (ppm) As 0 - 100 B 0 - 1000 0 - 1000 0 - 1,000 Methodology ASTM D6595; D6728 Ba 0 - 6,000 Standard Analytical Up to 31 elements from Li to Pb Bi 0 - 100 Range Typically 0-1000ppm (varies by application) Ca 0 - 3,000 0 - 6,000 0 - 50 0 - 500 Calibration Factory set, no maintenance required Cd 0 - 1000 LaserNet 200 Series Excitation Source Oscillatory arc discharge, JOAP characteristic Ce 0 - 100 Co 0 - 100 PARTICLE COUNTER, WEAR CLASSIFIER, FERROUS MONITOR OPTICAL SYSTEM Cr 0 - 1000 0 - 1000 0 - 500 Optical System Pashen-Runge polychromatar optic Cu 0 - 1000 0 - 1000 0 - 50 0 - 500 (Rowland Circle Alignment) Fe 0 - 1000 0 - 1000 0 - 50 0 - 500 Spectral Range 203 nm to 810 nm In 0 - 100 Temperature Control Thermally Stabilized; 40°C ± 1°C K 0 - 1000 0 - 10,000 0 - 500 Detectors CCD proprietary design for frequency range of interest Li 0 - 1000 0 - 500 Mg 0 - 6,000 0 - 50 0 - 1,500 OPERATIONAL SPECIFICATIONS Mn 0 - 1000 0 - 500 The LaserNet 200 Series is much The LaserNet 200 Series is the world’s best particle analyzer Sample Volume 2 mL of fluid Mo 0 - 1000 0 - 1000 0 - 500 more than a particle analyzer. It also for lubrication and hydraulic oil testing. calculates free water in ppm, and Solvents/Reagents None Na 0 - 3,000 0 - 6,000 0 - 10,000 0 - 100 Ni 0 - 1000 0 - 1000 0 - 500 differentiates contaminants (silica) from In commercial laboratories, power generation plants and industrial facilities, the Ambient Operating 0° to 40°C (32°F to 104°F) Temperature P 0 - 3,000 0 - 6,000 0 - 2,500 machine wear (metal). In addition, this LaserNet 200 Series offers unrivaled functionality for contamination control and Relative Humidity 0 to 90%, non-condensing Pb 0 - 1000 0 - 1000 0 - 50 0 - 500 instrument provides particle counts and condition-based maintenance programs. S codes, abnormal wear classification USER INTERFACE SPECIFICATIONS Sb 0 - 100 and ferrous wear measurement. FEATURES INCLUDE: Software/Operating Windows 10 Pro or Windows 7 Pro, 32 or 64 bit, Si 0 - 1000 0 - 1000 0 - 500 0 - 300 ■ Widest range up to 10 million System US English version Sn 0 - 1000 0 - 1000 Particle count, size distribution and codes (ISO 4406, NAS 1638, particles/ml Display External Monitor Ti 0 - 1000 NAVAIR 01-1A-17, SAE AS 4059, GOST, ASTM D6786, HAL and user-defined bins). ■ Automatic wear particle shape Data Storage External PC V 0 - 1000 0 - 500 Differentiation of contaminants (silica and fibers from machine wear metal) W 0 - 100 classification and ferrous particle OIL ANALYSIS LABORATORY INSTRUMENTS Data Transfer USB Zn 0 - 3,000 0 - 6,000 0 - 50 0 - 500 analysis Classification of wear particles, image storage and reporting of particle count and Data Entry External Keyboard and Mouse Zr 0 - 100 ■ Imaging of dark fluids containing size for Cutting, Sliding, Fatigue, Fibers and Non-metallics wear types up to 2% soot POWER REQUIREMENTS Total# 15 24 +7 13 15 Ferrous content measurement in the sample with ferrous particle count and size ■ Error correction for water and air distribution Voltage Input AC 120/240V, 50/60 Hz bubbles Power Consumption 500 Watts at test Differentiation of large ferrous particles >25 micron from total ferrous particles. Fusing 10 amps Consumables & Standards Reporting percentage of large ferrous particles and ferrous wear severity index for easy trending and interpretation of the ferrous measurements. MECHANICAL SPECIFICATIONS KITS Dimensions 70.6 cm (H) x 38.4 cm (W) x 66 cm (L) M97007 Consumables Kit for 500 measurements (rod & disk LaserNet Comparison 210 215 220 230 (27.8 in x 15.1 in x 26 in) electrodes, sample cups, pipettes, wipes, cleaning solution, swabs, gloves) Weight 70 kg (154 lbs) Total particle count & codes Multiple configurations and options cover the needs of commercial laboratories M97016 Oil Standards Shipping Package 121.9 cm (H) x 63.5 cm (W) x 109.2 cm (L); Non-metallic particles and industrial plants for contamination control and predictive maintenance. Dimensions (48 in x 25 in x 43 in) M97017 Fuel Standards (sand/dirt) Shipping Package 150 kg (330 lbs) M97018 Fuel Standards, Low Detection OPTIONS INCLUDE: Weight Free water measurement M97019 Water Standards Ferrous Monitor to measure ferrous content – enables measurement of both ferrous COMPLIANCE Air bubble/water droplet M97020 Coolant Standards correction content and total particle count on the same sample, eliminating the need to measure CE Mark: EMC Directive (2004/108/EC); RoHS M96380 Routine Maintenance Kit ferrous content on another instrument Wear particle classification Use Spectro Scientific certified consumables and standards to ensure the accuracy Classification of wear particle shape – directly images wear particle silhouettes and Total ferrous concentration and repeatability of your measurements. counts and classifies wear particles over 20 microns Ferrous particle count & size distribution Autosampler for high throughput sample processing – provides automated, unattended processing of up to 24 used oil or hydraulic fluid samples | Large ferrous concentration Spectro Scientific One Executive Drive, Suite 101, Chelmsford, MA 01824-2563 978-431-1120 | www.spectrosci.com | [email protected] | An ISO 9001:2008 company Autosampler option Copyright © 2017 Spectro Scientific. All rights reserved. While every effort is made to assure the information in this document is accurate, Spectro Scientific does not accept liability for any errors or mistakes that may arise. Specifications are subject to change without notice. SpectrOil100_DSv3_2017-08-30 72 | Product Catalog Product Catalog | 73 Particle Counter, Wear Classifier, and Ferrous Monitor
The LaserNet 200 Series provides particle counts and codes, large wear particle Sample preparation Data Management classification and ferrous wear monitoring. Options include an autosampler for high Establishing alarm limits and Sample preparation is efficient with the LaserNet 200 Series The LaserNet 200 Series has a data throughput sample processing as well as configurations without the ferrous monitor and condemnation levels for large machinery wear classification. wear particles is often challenging. – viscosities up to 320cSt can be processed without dilution export capability to laboratory LIMS Unlike parameters such as ISO code, due to the wide dynamic range. And, unlike conventional light systems as well as comma or tab water, elemental concentration and TAN, blockage particle counters, there are no flow control valve delimited text file formats. The wear there are no pre-defined limits set by adjustments needed when testing different sample viscosities. images can be exported as .jpeg or CUTTING WEAR SLIDING WEAR the equipment supplier. In each piece of .bmp files. equipment, machinery wear particles of With an intuitive, configurable graphical user interface and no different sizes reach their own dynamic calibration required, the LaserNet 200 Series is fast, accurate Spectro Scientific’s MiniLab Series equilibrium condition. The LaserNet 200 and easy to use. software, when integrated with the software calculates recommended wear OilView LIMS module, can transfer FATIGUE WEAR NONMETALLIC particle limits for categories of cutting data to the AMS Machinery Health wear, severe sliding wear and fatigue Manager LIMS module. wear by analyzing a series of six or more samples. SpectroTrack is a browser-based Laboratory Information Management System (LIMS). It provides a single view of a sample lifecycle from scheduling the sample to report generation and includes a customizable asset management database for trend analysis. Wear images are stored and analyzed directly on the LaserNet 200 software. They can be sorted by wear class. OilViewTM software also reports on particle count and size distribution by wear category.
Ferrous Particle Count & Size FILTER SCREEN SpectroTrack LIMS sample lifecycle report
SMALL COIL SET CCD CAMERA • Particle size distribution • ISO 4406 cleanliness codes FLOW • Particle shape classification CELL CUTTING
SLIDING
FATIGUE