Fluid Analysis Solutions 2018
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Oil Analysis Handbook Third Edition Copyright © 2017 Spectro Scientific
Predictive Equipment Maintenance Oil Analysis Handbook Third Edition Copyright © 2017 Spectro Scientific. All rights reserved. FluidScan® and LaserNet Fines® are registered trademarks of Spectro Scientific Inc. While every effort is made to assure the information in this document ois accurate, Spectro Scientific does not accept liability for any errors or mistakes that may arise. Specifications are subject to change without notice. | 3 Preface Welcome to the third edition of the In-service Oil Analysis Handbook. It has been a few years since the publication of the first edition of Spectro Scientific’s In-Service Oil Analysis Handbook. Our original goal was to compile a comprehensive reference book of common in-service oil analysis techniques to help readers understand and choose the right technique and instrumentation for their needs. We had to limit the scope in the first two editions because of the amount of effort needed to cover all the topics. In-service oil analysis for condition based maintenance covers a wide array of topics. I am pleased to say that in this third edition, we are much closer to our goal. We reorganized the structure of the content for better clarity and we added articles to cover more topics and instruments associated with oil analysis. Also, we rewrote several articles including the latest developments on the market. As we learned more from our customers about their successes using on site oil analysis, we developed case studies that you can find in this edition. This work is not possible without the time and effort from the contributing authors: Patrick Henning, Daniel Walsh, Robert Yurko, Ken Caldwell, Thomas Barraclough, Maria Bartus, Randi Price, John Morgan, Aifeng Shi and Yuegang Zhao from Spectro Scientific and Ray Garvey from Emerson Process Management. -
Gas Generator Bottle Introduction SCIENTIFIC This Gas Generator Setup Provides an Easy Way to Generate and Collect Gas
Gas Generator Bottle Introduction SCIENTIFIC This gas generator setup provides an easy way to generate and collect gas. Specific instructions are provided for the generation of hydrogen gas using zinc and acid. Concepts • Generation of gases • Water displacement Materials Hydrochloric acid solution, HCl, 3 M Glass plates or Sulfuric acid solution, H2SO4, 3 M Glass tubing Mossy zinc, Zn, 6 g Pneumatic trough Water, tap Rubber tubing Bent glass tubing* Silicone grease packet* Gas collecting bottles or tubes, 3 or 4 Thistle tube* Gas generator bottle* Two-hole rubber stopper* *Materials included. Safety Precautions Hydrochloric acid solution is toxic by ingestion and inhalation and is severely corrosive to skin, eyes and other tissues, as is sulfuric acid solu- tion. Hydrogen gas is a highly flammable gas and a severe fire hazard. Exercise extreme caution when testing the gas and keep the gas generator away from flames. Wear chemical splash goggles, chemical-resistant gloves, and a chemical-resistant apron. This activity requires the use of hazardous components and/or has the potential for hazardous reactions. Please review current Material Safety Data Sheets for additional safety, handling, and disposal information. Procedure 1. Set up the apparatus as shown in the figure to the right. Lubricate the glass tubing and thistle tube with silicone grease before inserting into the stopper. Make sure Thistle tube the water level is above the platform. Prepare bottles for collecting gas by water Two-hole rubber stopper displacement. To do this, fill each gas collecting bottle (or tube) over the brim with tap water, and then cover each with a flat glass plate. -
BROOKFIELD DIAL READING VISCOMETER with Electronic Drive
BROOKFIELD DIAL READING VISCOMETER with Electronic Drive Operating Instructions Manual No. M00-151-I0614 SPECIALISTS IN THE MEASUREMENT AND CONTROL OF VISCOSITY with offices in : Boston • Chicago • London • Stuttgart • Guangzhou BROOKFIELD ENGINEERING LABORATORIES, INC. 11 Commerce Boulevard, Middleboro, MA 02346 USA TEL 508-946-6200 or 800-628-8139 (USA excluding MA) FAX 508-946-6262 INTERNET http://www.brookfieldengineering.com TABLE OF CONTENTS I. INTRODUCTION .....................................................................................5 I.1 Components .......................................................................................................5 I.2 Utilities ................................................................................................................6 I.3 Specifications .....................................................................................................6 I.4 Set-Up ................................................................................................................7 I.5 IQ, OQ, PQ .........................................................................................................7 I.6 Safety Symbols and Precautions .......................................................................8 I.7 Cleaning .............................................................................................................8 II. GETTING STARTED ..............................................................................9 II.1 Operation ...........................................................................................................9 -
HAAKE Viscometer Standard Operating Procedure [Updated Sept 10, 2014]
HAAKE Viscometer Standard Operating Procedure [Updated Sept 10, 2014] HAAKE Viscometer 7 R+ Location of Machine: Composites Lab, RFM 1218 Location of SOP and Machine Operating & Safety Manual: Composites Lab website under resources; Composites Lab TRACS site; and Hardcopy near machine. Emergency Contact: Call 911 Call EHS & Risk Management at 512-245-3616 Call Head Lab Technician, Dr. Ray Cook (office 512-245-2050) Call Dr. Jitendra S Tate (office 512-245-4872) Before using this machine: You must have permission from Dr. Tate. You must have received formal training from technician or, trained research student (designated by Dr. Tate) related to machine safety and operation. You must read and understand SOP and Machine Cleaning Manual. You must use this machine under direct supervision of Dr. Tate or, Dr. Cook or, trained research student (designated by Dr. Tate). You must have signed “Lab Rules” document with Dr. Tate. This document must be signed every semester fall, spring, and summer (as applicable). If you do NOT follow above instructions you will be held responsible for your own safety and damages. Safety Precautions: Protective Equipment: Prior to performing this procedure, the following personal protective equipment must be obtained and ready for use: Gloves, Safety Goggles, Face Mask, Lab Coat. Important Safeguards: 1. Prior to performing this procedure, the following safety equipment must be accessible and ready for use: (e.g. chemical fume hood, biological safety cabinet, laminar flow hood, chemical spill kits) Fume hood 2. All liquids should be drained to containers for chemical disposal and properly marked. 3. In the event that a hazardous material spill during this procedure, be prepared to clean with cleaner according to MSDS of materials used. -
Building and Validating a Rotational Viscometer Brian Cherrington & Jack Rothstein Mechanical Engineering Faculty Mentors: Dr
Building and Validating a Rotational Viscometer Brian Cherrington & Jack Rothstein Mechanical Engineering Faculty Mentors: Dr. Maria-Isabel Carnasciali, Dr. Samuel Daniels Abstract This project was an effort to redesign an initial prototype rotational viscometer to experimentally test whether or not viscosity values vary significantly when the geometry of the viscometer is changed. The scope of the project involved designing and building a viscometer that could vary the gap between the inner and outer cylinders, variation of the testing fluid’s temperature, and control of the device’s RPM. After weeks of planning, designing, and fabrication the new viscometer was complete. In order to control the device, monitor the sensor readings, and calculate the testing fluid’s viscosity a LabVIEW program was created. Testing on medium to high viscous fluids was completed to determine if the viscosity values and the geometry of the viscometer are dependent or independent of each other. The results did show a correlation between measured viscosity and variations in the geometry of the viscometer. More testing is required to further verify the results and properly calibrate the device. Introduction For this project a new design was conceptualized, fabricated, and tested. This new design met several criteria including, Viscosity is often referred to as a fluid’s thickness or how much it resists deformation due to an applied force. Designed for future use in ME labs; Rotational viscometers measure the amount of torque needed Designed to be durable, sustainable, and easy to to rotate an object moving through fluid at a known RPM. dissemble and clean; Using the measured torque, RPM, and dimensions of the Multiple inner cylinders for varying gap sizes; device, the viscosity can be calculated using equation 1. -
K–12 Science Safety Manual
K–12 Science Safety Manual Developed by the Innovative Teaching and Learning Unit Instructional Design and Professional Learning Division K–12 Science Department TABLE OF CONTENTS Importance of Safety 2 General Information 7 Prohibited Practices 9 Emergency Information 10 Safety on Field Trips 15 General Laboratory Safety 20 Elementary Science Safety 22 Biological Science Safety 24 Earth and Space Science Safety 28 Chemistry Science Safety 31 Physics Science Safety 35 Appendix A: Technical Safety Assistance Numbers 49 Appendix B: Safety Survey 50 Appendix C: Lab Inspection Checklist 51 Appendix D: Chemical Storage 55 Appendix E: Waste Disposal 63 Appendix F: Prohibited Chemicals 68 Appendix G: Restricted Chemicals 75 Appendix H: Animals in the Classroom 79 Appendix I: Safety Contracts and Exams 85 Appendix J: Safety Resource Websites 86 Restricted Chemical Request Form 87 Secondary Science Teacher Safety Manual Acknowledgement Form 88 IDPL-SCI-M002, Rev. B September 2009, Rev. C April 2015 0 SPECIAL ACKNOWLEDGMENTS The Clark County School District K–12 Science Safety Manual is a coordinated effort by a team of teachers, administrators, with input from the Southern Nevada Health District. Andy Cheney Environmental Health Supervisor, Southern Nevada Health District Ellen Dunne K–5 Science Project Facilitator, CCSD Instructional Design and Professional Learning Division Eileen Gilligan Elementary Science Coordinator, CCSD Instructional Design and Professional Learning Division Kim Krumland Risk and Environmental Services Department Director, -
Miniav®-X Automatic Viscometer Instruction & Operation Manual
MiniAV®-X Automatic Viscometer Instruction & Operation Manual 81.2254 i CONTENTS 1 INTRODUCTION/INSTALLATION 1 The miniAV®-X Automatic Viscometer .................................................................................. 1 Measuring kinematic viscosity ............................................................................................... 2 Safety cautions ..................................................................................................................... 2 Specifications ....................................................................................................................... 4 Installation ............................................................................................................................ 4 Required installation components ............................................................................... 4 Vacuum Pump unit connections ................................................................................. 6 Bath unit connections ................................................................................................ 6 VISCPRO® for Windows® XP® ............................................................................................ 6 Installing VISCPRO® software .............................................................................................. 7 Computer requirements ............................................................................................. 7 Windows® XP® installation ....................................................................................... -
Chemistry 1009 Lab Manual University of Louisiana at Monroe
Chemistry 1009 Lab Manual University of Louisiana at Monroe Department of Chemistry 2010 Version 2.0 Contents Lab Session 1: Laboratory Safety Rules and Check In .................................................. 1 Fire, Injury, Spills and Cleanliness .............................................................................. 2 Desk Assignment Sheet (Chemistry 1009) .................................................................. 4 Commonly Used Equipment (not in the desk drawer)................................................. 5 Lab Session 2, Experiment 1: Introductory Exercises ................................................... 10 Report Form 1 .............................................................................................................. 17 Lab Session 3, Experiment 2: Oxygen ........................................................................... 18 Report Form 2 .............................................................................................................. 21 Lab Session 4, Experiment 3: Preparation of Sodium Chloride .................................... 22 Report Form 3 .............................................................................................................. 25 Lab Session 5, Experiment 4: Law of Definite Proportions .......................................... 26 Report Form 4 ........................................................................................................... 30 Lab Session 6, Experiment 5: Hydrogen and the Activity Series of Metals ................. -
List of Equipments in the Department (Chemical Engineering) Mechanical
List of Equipments in the Department (Chemical Engineering) Mechanical Operation lab Fluid Mechanics Lab Heat transfer Lab Mass Transfer lab • Cyclone Separator • Reynold’s Apparatus • Double Pipe Heat Exchanger • Tray Dryer • Plate & Frame Filter Press • Bernoulli’s Theorem Apparatus • Shell & Tube Heat Exchanger • Sieve Plate Distillation Column • Vibrating Screen • Pitot Tube Apparatus • Vertical Condenser • Liquid-Liquid Extraction • Jaw Crusher • Calibration of Orifice meter, • Computerized Control Shell & • Adsorption of CO 2 • Ball Mill Venturi meter and Rota meter Tube Heat Exchanger • Steam Distillation • Roll Crusher • Coefficient of Discharge of • Thermal Conductivity of Metal • Bubble Cap Distillation Column • Rotary Vacuum filter Orifice and Mouthpiece Bar • Cooling Tower • Fluidized Bed • Film & Drop Wise Condensation • Diffusivity Apparatus • Single Effect Evaporator • Fluidized Bed Dryer • Simple Steam Distillation • Simple Distillation • VLE Apparatus • Equilibrium Flash Distillation • Humidification & Dehumidification • Refractometer Process Control Lab Chemical Reaction Engg. Lab Fuel Combustion Energy Technology Lab Environmental Lab • Process Training Simulator with • Plug Flow Reactor • Flash & Fire Point Apparatus • BOD Incubator Modules (Software) • Isothermal Batch Reactor • Aniline Point Apparatus • pH Meter • Pressure Control System • Single Tube Packed Bed Reactor • Orsat Gas Analysis Apparatus • Sedimentation Apparatus • Flow Control System • RTD in CSTR / Mixed flow • Redwood Viscometer • UV-VIS Spectrophotometer • pH control System Reactor • Bomb Calorimeter • DO Meter • Real Time Simulator Trainer • RTD in Tubular Reactor • Smoke Point Apparatus • Digital Conductivity Meter • Level Control System • Adiabatic Batch Reactor • Temperature Control System • Distillation Column • Two Tank Interacting system • Two Tank Non-Interacting System • CSTR Control System Research Equipments • UV-Spectrophotometer • Gas Chomatography . -
Department of Chemical Engineering
DISTILLATION FLASK : Made of borosilicate glass is specified dimension. Capacity: 125 ml. GRADUATED RECEIVER: Capacity : 100 ml. sub-division 1 ml. the cylinder is made of heat resistance borosilicate glass. FLASK SUPPORT ASSEMBLY BOARD: Three asbestos board on each with centre hole 32 mm, 37.5 mm and 50 mm. are provided. TEMPERATURE CONTROLLER: By solid state variable heat controller. Complete Apparatus as described above but supplied with 3 Nos. flask support boards and glassware for operation on 220/230 V, 1ph, 50 c/s, A.C. mains. SPARES FOR ABOVE DISTILLATION APPARATUS: 1. Distillation Flask, borosilicate glass, Capacity : 125 ml. packet of 2(two) pieces. 2. Receiver, 100 ml. packet of 2(two) pieces . 3. Thermometer : Mercury-in-Glass, with NABL Certificate IP – 5C, packet of two pieces.; IP – 6C, packet of two pieces; ASTM – 7C, packet of two pieces. ASTM – 8C, packet of two pieces. 4. Heating Element, packet of two pieces. …………….. 5. Flask support plate, packet of one each (Total 3 nos.) 32 mm. Centre Hole; 37.5 mm. Centre Hole; 50 mm. Centre Hole 2. FLASH POINT PENSKY MARTENS (CLOSED) CONFORMS TO : IS: 1448 & 1209 – 58, IP: 34, ASTM: D-93 SPECIAL FEATURES: Cup & Cover with ebonite handle for operating at high Temperature. For determining the flash point of petroleum products having a flash point above 120º C (48.89º F). The instrument which will give trouble free service under continuous operating conditions. The cast iron air bath is fitted with heaters for uniform heating. An enclosed safety type heater made of nichrome heating element. Temperature is controlled by Digital Temperature Indicator cum controller which ensure smooth and easy control of the temperature. -
Physical Quantity Measured by a Vibration Viscometer (Re: JCSS Standardization of Viscosity)
Article for the 23rd Sensing Forum Theme: Physical Quantity Measured by a Vibration Viscometer (Re: JCSS Standardization of Viscosity) Presented by: Naoto Izumo R&D Division, A&D Company, Limited October 2 ~ 3, 2006 Tsukuba Center Inc. Tsukuba, JAPAN Physical Quantity Measured by a Vibration Viscometer Subtitle: The JCSS Standardization of Viscosity Naoto Izumo R&D Division, A&D Co., Ltd. Higashi-Ikebukuro, Toshima-ku, Tokyo 170-0013 Japan Abstract The objective of this article is to introduce a viscometer that utilizes a new viscosimetry measuring method. In addition, the article will recommend a new unit system, which is utilized in the vibration viscometer. Using examples, the article explains JCSS viscosity standardization and recent requirements for viscosity measurements. Keywords: Vibration Viscometer, Static Viscosity (Viscosity × Density), Viscosity JCSS, Cloud Point Introduction The following is an introduction of the vibration viscometer, a new method for measuring viscosity. In addition to providing a description of the physical quantity that is measured using the vibration viscometer, a new unit system for viscosity will be proposed. Furthermore, there is an explanation regarding the Japan Calibration Service System (JCSS) standardization of viscosity and viscosity measurements using actual examples. There is also discussion of recent requirements for measuring viscosity. History and Development of Viscosity Measurement The history of viscosity measurements is extensive and is believed to date back to when people began measuring the viscosities of engine oils with the advent of the automobile industry in the United States. In the U.S., it had become necessary to control the viscosities of engine oils as a method of maintaining the performance of engines. -
QCM Viscometer for Bioremediation and Microbial Activity Monitoring Wesley A
304 IEEE SENSORS JOURNAL, VOL. 3, NO. 3, JUNE 2003 QCM Viscometer for Bioremediation and Microbial Activity Monitoring Wesley A. Gee, Member, IEEE, Kirsti M. Ritalahti, William D. Hunt, and Frank E. Löffler Abstract—A quartz crystal microbalance has been used to parameter eliminates the necessity of complex data interpreta- monitor the polymer production of a bacterial population in tion of samples by trained technicians. liquid medium. The increasing amount of produced polymer The aim of this study was to show that the QCM is a unique corresponds to an increase in the viscosity of the liquid, which is directly measurable as the fluid contacts the surface of the quartz and effective method to monitor a biological growth process to crystal in the sensor system. This procedure is being developed as aid in characterizing unknown bacterial populations. As a vis- a novel method for measuring microbial polymer production and cometer, this high shear rate device could be used in conjunc- growth of an environmental isolate obtained from river sediment tion with low shear rate laboratory viscosity measurement tech- contaminated with petroleum hydrocarbons. This measurement niques that currently include mechanical (rotational), capillary, technique may be used to monitor growth characteristics of unknown anaerobic bacteria when used in conjunction with falling ball, and other gravity or positive displacement methods. other currently employed microbiological test methods, such as spectrophotometry, to measure turbidity. II. DESCRIPTION OF BACTERIAL STRAIN In the presence of glucose, a novel, strictly anaerobic bacterial isolate, designated strain JEL-1, produces a viscous, as yet uniden- An unusual bacterial population, designated strain JEL-1, tified, polymer.