WASTE REDUCTION ADVICE for Farm Equipment Manufacturers

Iowa Waste Reduction Center University of Northern Iowa

WASTE REDUCTION ADVICE for Farm Equipment Manufacturers

nble of Contents

Section Description Page

I Introduction ...... 1

I1 General Regulatory Review ...... 2 I11 Machining Wastes ...... 3

IV Cleaning Solvent Wastes ...... 5 v Prepaint Treatment Wastes ...... 7

VI Paint and Thinner Wastes ...... 11

VII Paint Booth Filters ...... 13

VIII Storm Water ...... 14

IX Nonhazardous Solid Wastes ...... 15 . . Air Em~ss~ons...... 16 Hazardous Waste Management and Storage ...... 17 Superfund Amendments and Reauthorization Act (SARA) Title I11 ...... 18

Copyright 1991. Iowa Waste Reduction Center

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Appendices

A Conditionally Exempt Small Quantity Generator Requirements

B Small Quantity Generator Requirements

C Hazardous Waste Definitions D Tramp Oil Removal Equipment Vendors

E Used Oil Management Companies

F Distillation Equipment Vendors

G Hazardous Waste Management Companies H NPDES Permit Application Summary - Process Waters

I Total Toxic Organics (TTO) Solvent Management Plan

J Analytical Laboratories

K SWA Test Parameters SWA Application

L Paint Application Methods

M NPDES Permit Application Summary - Storm Water

N Solid Waste Recyclers

0 Air Permit Application

P Counting Hazardous Waste When Using a Solvent Still Q SARA Title I11 Reporting Instructions

I. INTRODUCTION

There are over 300 farm equipment manufacturers throughout the state of Iowa. These manufacturers have been targeted for waste management and reduction by the Iowa Waste Reduction Center (IWRC), located at the University of Northern Iowa. The primary method of outreach was through a direct mailing according to SIC codes. The mailing consisted of an IWRC brochure and a notice discussing potential liabilities resulting from improper storage methods and hazardous waste determinations. As a result of this mailing, the IWRC has conducted 30 on-site reviews to assist farm equipment manufacturers in developing and implementing effective and compliant waste management programs through waste reduction and recycling. On-site reviews for farm equipment manufacturers involve a facility tour to determine current waste streams and management methods. A review of hazardous waste shipping manifests, material safety data sheets, and other related documentation is also performed. Following an on-site review, a report is prepared and sent to the farm equipment manufacturer; continued contact is common as a means to assist the manufacturer in implementing the recommendations contained in the report. Six to nine months after an on-site review, a formal follow-up call is made to assess waste management and reduction progress. This also provides clients with an opportunity to have questions answered concerning recent developments. Farm equipment manufacturers fabricate and market a variety of products. These products include livestock confinement equipment, buildings, gates, wagons, trailers, and loaders as well as wood and plastic housing units. Fabrication aspects include the traditional metal working and finishing operations, plastic and fiberglass molding, painting, and woodworking. This manual reviews the general categories of waste generation common to most farm equipment manufacturers. Each category is divided into three sections, where appropriate, addressing standard existing conditions, regulatory requirements, and general recommendations. The following categories are discussed: 1. Machining Wastes (Scrap Metal and Cutting Fluids) 2. Cleaning Solvent Waste 3. Prepaint Treatment Wastes 4. Paint and Thinner Wastes 5. Paint Booth Filters 6. Storm Water 7. Nonhazardous Solid Wastes 8. Air Emissions 9. Hazardous Waste Management and Storage 10. Superfund Amendments and Reauthorization Act (SARA) Title I11 11. GENERAL REGULATORY REVIEW

Federal Environmental Protection Agency (EPA) regulations require all facilities that generate waste to determine whether the waste is hazardous or nonhazardous. This may be accomplished through laboratory testing or a thorough knowledge of the waste or process generating the waste. Wastes are defined as hazardous either by specific EPA listing (i.e., toluene) or by demonstrating one or more of the following hazardous characteristics: Ignitability Toxicity Corrosivity Reactivity Once the facility has determined the hazardous/nonhazardous nature of all its wastes, the facility's monthly hazardous waste generation rate must be established. The generation rate per calendar month (and the total quantity of hazardous waste stored on-site at any given time) defines which one of the following categories is applicable to the facility: * Conditionally Exempt Small Quantity Generator (CESQG) * Small Quantity Generator (SQG) Large Quantity Generator (LQG) EPA hazardous waste regulations that apply to the facility are contingent upon that facility's hazardous waste generator status. Therefore, it is important to accurately define and quantify all hazardous waste to assure that the correct generator category and applicable regulations have been determined. In general, less stringent regulations apply for the smaller quantity generators. A summary of the CESQG requirements is included in Appendix A; SQG requirements are summarized in Appendix B. Nonhazardous industrial waste regulation falls under the jurisdiction of the Iowa Department of Natural Resources (DNR). Nonhazardous industrial solid waste may be disposed of in local solid waste landfills, provided a Special Waste Authorization (SWA) is issued to the receiving landfill. A SWA is obtained by testing the waste for various parameters to verify that it is not hazardous and will not have a detrimental effect on landfill operation. These data are then submitted, along with a SWA application form, for DNR review. If the DNR requirements are met, an approved SWA will be sent to the receiving landfill (a copy to the applicant) and disposal may begin. Other restrictions may be imposed by the DNR prior to approval of a SWA. Air emission regulations are enforced by the Iowa DNR, contingent upon federal standards. Facilities or operations installed or modified since 1970, that have the potential to emit air pollutants (i.e., dust, smoke or vapors), are required to obtain an air permit from the DNR. The air permitting process may require emission testing and/or control. Facilities and operations installed prior to 1970 do not require air permits (provided no major modifications have been completed since 1970) but must still comply with applicable emission limits. Requirements for toxic air emissions are handled on a case-by-case basis. Process water discharges to public waterways (i.e., rivers, drain tiles) are regulated under federal Clean Water Act guidelines. The regulations require dischargers to obtain a permit which limits the amount of pollutants allowed to be discharged at any given time. The 2 permit program is administered by the Iowa DNR. Permit parameters typically include regular monitoring of discharges for various specified pollutants and the submittal of monthly or quarterly reports to the control authority. Storm water runoff from industrial areas (i.e., materials handling and waste storage), which is not collected for treatment through a wastewater treatment facility, is subject to new federal guidelines and permitting. Facilities which perform any industrial activity that is exposed to storm water are required to obtain a discharge permit for the runoff. Permit parameters are determined on a case-by-case basis but will likely require a minimal amount of pollutant monitoring. Pretreatment standards for wastewaters generated by a number of manufacturing processes have been designated by the EPA. These pretreatment standards determine the level of contaminants which are acceptable in wastewaters being discharged from a facility to a publicly ownedsanitavy sewer. Pretreatment standards apply to specific industrial processes, such as electroplating. Pretreatment program administration is by the local wastewater authority, with oversight by the Iowa DNR.

111. MACHINING WASTES (SCRAP METAL AND CUTTING FLUIDS)

1. Existing Conditions: Most metal farm equipment products are made from varying grades of steel or aluminum. Heavy cutoff pieces and turnings are collected and recycled through local scrap metal dealers. In a small number of the shops visited, turnings were no longer accepted by the scrap metal dealers due to cutting fluid residue. In these cases, turnings were disposed of through the local sanitary landfill. Practically all machining operations utilize cutting fluids to facilitate metal parts manufacturing. These operations include drilling, tapping, lathing, cutting, and grinding. All of the shops visited had previously converted to water soluble cutting fluids for most of their machining operations. Oils continue to be used for drilling and tapping operations. Disposal of water soluble cutting fluids has been through local wastewater treatment facilities; in most cases, the wastewater treatment facility granted approval of this method of disposal. One manufacturer contracted disposal through a commercial wastewater treatment facility. Unfortunately, more than half of the manufacturers visited have never replaced their cutting fluids. This is due primarily to poor cutting fluid management which leads to the constant need to add make-up water and virgin solution to replace evaporative losses. In these shops, addition of biocides and pH buffers does not occur since the solution evaporates before it becomes soiled. Regulatory Review: Materials collected for recycling (scrap metal) are not considered waste and are therefore exempt from state and federal waste disposal regulations. Disposal of metal "fines" is acceptable in Iowa sanitary landfills provided the material is not contaminated with excess oil (free liquid); recycling is the preferred method, however. Disposal of water soluble cutting fluids through the local wastewater treatment facility depends largely on the wastewater treatment facility's ability to properly handle the cutting fluid constituents and the total volume of cutting fluid being disposed of by local machine shops. Industrial dischargers are required to obtain the wastewater treatment facility's approval for all discharges of cutting fluids. Additional pretreatment requirements may apply depending on other facility wastewater discharges (see Section V). Farm equipment manufacturers which either (1) are located in communities without a wastewater treatment facility, or (2) discharge to a drain tile, river, ditch or other body of water, are required to obtain a National Pollutant Discharge Elimination System (NPDES) permit. To obtain a NPDES permit, the facility must have composite samples of its wastewaters tested for heavy metal concentrations, pH, temperature at the time of discharge, and overall flowrate. Additional testing for cyanides, phenols, and oiVgrease may be required in some cases. The NPDES permits are granted by the Iowa DNR for individual facilities. The application process is two part; part one consists of general information regarding the facility and property while part two requests information concerning specific discharge sources and constituents. The DNR has authority when granting NPDES permits to determine permit parameters on a case-by-case basis. Recommendations: Scrap metal recycling activities are good waste management practices and should be implemented whenever possible. Where scrap metal dealers are unwilling to accept "fines", manufacturers should inquire whether it is possible to recycle the fines elsewhere before disposal in a sanitary landfill takes place. Turnings and fines which are still wet should be collected in a suitable container and drained. The fines may then be acceptable for recycling through a scrap dealer; the collected coolant can be recycled back into equipment for reuse. Many large manufacturers have found that some scrap metal dealers will accept turnings if they have been compacted and baled. Other potential recyclers of dried fines are mini-mills and foundries. If the cutting fluid MSDS indicates no hazardous materials are present (see Appendix C), disposal through the local wastewater treatment facility is acceptable, provided approval is granted by the local wastewater authority. In cases where manufacturers discharge to state owned bodies of water, a NPDES permit should be obtained. Further discussion of the NPDES requirement is included in Section V. Farm equipment manufacturers can extend cutting fluid life to reduce waste generation and the associated costs of disposal and raw material purchase. Proper fluid management alsa yields longer tool life and high quality machined parts. Removal of tramp oil through use of a belt skimmer, coalescer or other means can dramatically extend the useful life of the cutting fluid. A list of vendors of this type of equipment is enclosed in Appendix D. The recovered tramp oil may be recycled off-site for energy recovery through a used oil management company (see Appendix E for a list of these companies). The cleaned coolant may then be returned to the machining equipment for reuse. Continuous screening for chip removal and regular skimming to remove tramp oil can potentially extend coolant life more than six months. 4 Water evaporation also causes accelerated fluid deteriorationwhich can have a devastating effect on coolant life. Additives in the coolant such as biocides and rust inhibitors are easily affected by water evaporation. As the water evaporates, the overall concentration of these additives will increase. At increased concentrations, rust inhibitors may actually begin to promote corrosion rather than deter it since the pH is no longer constant. Daily pH monitoring is also extremely important in extending coolant life. Biocides are effective for bacteria removal at neutral pHs; once the pH has drastically changed, it indicates the biocide has become ineffective. Consequently, the amount of water present in the cutting fluid should be monitored at least weekly, if not daily, and can be done through chemical means or use of a refractometer. Monitoring logs should be kept for each machine. The monitor log should include daily recordings of pH, biocide concentration and amount of water present as well as remarks on the overall appearance of the coolant at the time of the inspection. A simple refractometer can be purchased for $200 while the cost of virgin cutting fluid may be as much as $650 per drum. If two drums are purchased each year then the present cutting fluid cost (undiluted fluid) is $3.56/day. If the cutting fluid life could be tripled this would amount to a yearly savings of $868. The refractometer would pay for itself in two or three months, after which general operating costs would be lowered by $868 each successive year. A manual which discusses different types of cutting fluids, maximizing fluid life, and disposal methods is now available through the IWRC.

IV. CLEANING SOLVENT WASTES

1. Existing Conditions: More than two-thirds of the farm equipment manufacturers visited use solvents to remove oil and grease from metals. The amount of solvent waste generated from degreasing operations varies from one gallon per month to 300 gallons per month. The average waste solvent generated is approximately ten gallons per month. The most common solvent used as a degreaser was mineral spirits, although there was one manufacturer using 1,1,1- trichloroethane. The mineral spirits were used in a typical parts wash solvent sink while the l,l,l-trichloroethane was used in large open tanks. Disposable paper towels and rags (wipers),and cloth rags are sometimes used to wipe down metal pieces after machining and/or before painting. Wipers are usually saturated with toluene, xylene, or acetone and disposed of in the local municipal landfill. Cloth rags are recycled through a commercial laundry facility. 2. Regulatory Review: Spent mineral spirits are considered a hazardous waste according to EPA's ignitability characteristic (flashpoint below 140°F). Waste solvent must be handled through a permitted Treatment, Storage and Disposal Facility (TSDF) in order to comply with federal environmental regulations. The appropriate EPA waste code for spent mineral spirits is DO01 and should appear on the hazardous waste shipping manifest which is required for hazardous waste transport. If the farm equipment manufacturer is recycling or reclaiming the spent solvent off-site, a hazardous waste manifest may not be needed. A hazardous waste shipping manifest would not be required if there is a contract in place which (1) specifies the type of waste and frequency of shipments, (2) the vehicle used to transport the waste is owned and operated by the reclaimer of the waste, and (3) the generator maintains a copy of the reclamation agreement on file for at least three years after termination or expiration of the agreement. Spent l,l,l-trichloroethane is considered an EPA hazardous waste by specific listing. l,l,l- trichloroethane used in degreasing operations has been assigned the EPA waste code F001, which should be included on all shipping manifests and related documents. Again, the one time where a manifest would not be required would be during off-site solvent reclamation under a contractual agreement. Paper towels and disposable rags which have been contaminated with xylene, toluene, or acetone are usually considered hazardous wastes by EPA and must be handled as such, The wipers must be collected as a hazardous waste and disposed of through a hazardous waste management company. The EPA waste codes for wipers contaminated with xylene or acetone are F003 and D001; the waste codes for toluene contaminated wipers are F005 and D001. These waste codes and the name of the waste should appear on all hazardous waste documentation records and the quantity of waste wipers generated must be included when determining the facility's monthly hazardous waste generation rate. Cloth rags which are laundered and reused, either on-site or through a commercial laundry facility, are not considered hazardous wastes and are therefore not covered by federal regulations. All of the above hazardous wastes must be included in the calendar month hazardous waste generation rate, which will determine the applicable generator category of the facility. 3. Recommendations: Spent solvents such as mineral spirits and l,l,l-trichloroethane can be recycled either on- or off-site. Off-site solvent recycling is recommended when the total solvent generation rate (including paint thinner) is less than 30 gallons per month. On-site solvent recycling is recommended for larger quantities (greater than 30 gallons per month). There are many small distillation units currently available which could easily handle these waste streams. Small distillation units which process five gallon batches may be purchased for as little as $2,000. Prices for larger units range from $3,000 to $8,000 per unit and each unit is capable of processing many different solvents. For extremely large batch processing or continuous solvent recycling, stills are available in the range of $10,000. These larger units are often computerized with sensors and pumps to completely control the distillation process with very little attention required. The use of an on-site distillation system has two main advantages: (1) disposal costs are almost eliminated since most of the solvent is recovered and reused, and (2) raw material purchase costs may be reduced by more than 80% since spent solvent can be recycled and reused. If $200 is spent each month for disposal of 30 gallons of solvent wastes, and $180 is spent on new solvent purchase, payback on a small distillation unit could be realized in six to seven months. A list of distillation equipment vendors is included in Appendix F. Wipers contaminated with hazardous wastes should be managed as such through a hazardous waste management company. A list of hazardous waste management companies can be found in Appendix G. Wherever possible, cloth rags should be used and recycled either on-site or off-site through a commercial laundry facility. The advantages of using recyclable rags are the reduction in hazardous waste generation, elimination of new wiper purchase costs, and elimination of potential liabilities from land disposal of hazardous wiper waste.

V. PREPAINT TREATMENT WASTES

Existing Conditions: One third of the farm equipment manufacturers visited utilize an aqueous cleaning system prior to painting. Almost all these cleaning systems involve use of a 1-3% phosphoric acid solution; a small percentage used an iron or zinc phosphate/phosphoric acid solution with the intent of providing a phosphate conversion coating on the surfaces to be painted. When these solutions have become spent, discharge to the local wastewater treatment facility is the most common means of disposal. The remaining two-thirds performed minimal prepaint surface treatment, such as wiping with solvent cloths to clean. Regulatory Review: All industrial discharges to a sanitary sewer are required to be approved by the DNR through a "Treatment Agreement" arranged with the local sewer authority. Manufacturers in large communities (population greater than 25,000) have the Treatment Agreement approved by the local sewer authority, rather than the DNR. Use of mild phosphoric acid solutions to clean surfaces prior to painting does not constitute "conversion coating" and is therefore not regulated by EPA's categorical pretreatment standards for industrial wastewaters. For manufacturers using solely phosphoric acid in the prepaint treatment process, approval from the accepting wastewater treatment facility is required prior to any discharges. Iowa has not imposed stricter standards than the currently existing federal regulations, therefore, any additional regulation would be designated by the receiving wastewater treatment facility. In situations where direct discharge to state bodies of water is the means of disposal, the manufacturer is required to obtain a NPDES permit before any discharges take place. A summary of the NPDES permit application process is in Appendix H. Pretreatment of surfaces with an iron phosphate or zinc phosphate complex is considered "conversion coating" and discharges are regulated by the federal categorical pretreatment standards. Discharges from phosphate coating operations are regulated according to Title 40 of Code of the Federal Regulations (CFR), Part 433. Section 433.15 specifically applies to phosphate coating. Table 1 shows the pretreatment standards for existing sources that discharge wastewaters to Publicly Owned Treatment Works (POTWs). I'dble 1 Federal Pretreatment Standards for Existing Sources (PSES)

Pollutant Daily Maximum Monthly Average

Cadmium, total Chromium, total Copper, total Lead, total Nickel, total Silver, total Zinc, total Cyanide, total Total Toxic Organics (TTO)

The standards listed in Table 1 must be met prior to discharge to the sanitary sewer either through a wastewater pretreatment system or other available methods. Dilution of wastewater is not an acceptable method for pretreatment. Dischargers have been required to be in compliance with these pretreatment standards since February 15, 1986. The first reporting requirement under the pretreatment regulations is termed the Baseline Monitoring Report. This report requires: Facility name and address List of environmental permits, if any Description of operations (i.e., description of the phosphate coating line including a schematic of the line and point of discharge) Flow measurements Measurement of pollutants Certification statement regarding compliance with pretreatment standards, and whether additional measures are needed to achieve compliance Schedule of activities needed to come into compliance, if any Measurement of pollutants requires sampling and analysis of three discharge samples collected during a two week period of time. These samples must be taken at a point where all waste streams covered by the standards are combined, but before mixing with dilute waste streams such as domestic sewage or cooling water. Composite samples must be collected for all pollutants, except cyanide and TTO which must be grab sampled. In lieu of TTO monitoring, the control authority (DNR or a wastewater system with an approved pretreatment program) may allow dischargers to make the following certification statement: "Based on my inquiry of the person or persons directly responsible for managing compliance with the pretreatment standard for total toxic organics (TTO), I certify that, to the best of my knowledge and belief, no dumping of concentrated toxic organics into the wastewater has occurred since filing of the last discharge monitoring report. I further certify that this facility is implementing the toxic organic management plan submitted to the control authority." 8 When requesting this alternative to TTO monitoring, the discharger must submit a solvent management plan that specifies: The toxic organics compounds used at the facility (e.g., benzene) The method of disposal used instead of dumping (e.g., reclamation, contract hauling, or incineration) Procedures for ensuring that toxic organics do not routinely spill or leak into the wastewater. A listing of the TTO chemicals and a sample solvent management plan are included in Appendix I. Any discharge from phosphate conversion coating operations which would drain into a state owned water requires a NPDES permit. Testing requirements under a NPDES permit may vary from those described above. Sludges and sediments generated during conversion coating operations may be hazardous due to toxicity andlor corrosivity. Prior to disposal of these waste materials, a hazardous waste determination must be made. The appropriate test for toxicity is the "Toxicity Characteristic Leaching Procedure" (TCLP); a listing of TCLP parameters is included in Appendix C. If the sludge or sediment does not exceed any of the TCLP parameters and does not demonstrate corrosivity (low pH), it need not be handled as a hazardous waste. If any of the TCLP parameters are exceeded or the sludge is corrosive, then the sludge must be handled through a permitted hazardous waste facility. Sludges and sediments which do not demonstrate any of the characteristics of a hazardous waste may be acceptable for landfill disposal upon approval of a SWA by the DNR. To obtain a SWA, the sludge or sediment must be dry (i.e. no free liquids) and have less than 1% hydrocarbon content. 3. Recommendations: All facilities discharging wastewaters to a POTW are required to submit a baseline monitoring report to the Iowa DNR. Following submission of this report, each facility should establish a treatment agreement for wastewater discharges with their local sanitary sewer authority. It is recommended that facilities contact their local sewer authority to determine whether each of these documents is in place. A baseline monitoring report and treatment agreement form are available upon request from the IWRC (8001422-3109) or the Iowa DNR, Water Permit Section (800/367-1025). Solutions used to clean metal surfaces which are not conversion coatings (i.e., dilute phosphoric acid) should be neutralized before sanitary sewer discharge. Spent solutions can be collected in appropriately sized containers and neutralized on-site using sodium bicarbonate (soda ash) or 50% sodium hydroxide (caustic soda) solutions until the pH is between six and nine. The neutralized solution can then be flushed to the sanitary sewer with an equal volume of water. Farm equipment manufacturers utilizing a metal phosphate conversion coating system prior to painting operations should have their phosphate coating wastewater tested for the inorganic parameters listed in Table 1 (i.e., all parameters except TT0 and cyanide). The test sample collected should be representative of the wastewater that enters the sewer but prior to dilution with domestic sewage and cooling waters (i.e., pH adjusted phosphate and rinse tank mixture). Laboratories listed in Appendix J can provide sample bottles and conduct the analysis. Comparison of results with the pretreatment standards will determine whether these wastewaters will need to be included in planning for wastewater pretreatment. If the test data show all parameters less than the above limits, manufacturers should contact the wastewater treatment facility and request guidance for further activities required by city/state regulations. If the testing shows any parameters in excess of the limits listed in Table 1, discharges should cease and alternative disposal procedures or wastewater pretreatment should be implemented. If continued testing is required, manufacturers should review raw product Material Safety Data Sheets (MSDS) to determine which TTO compounds (a list of TT0 compounds is included in Appendix I) are present on-site. Probable materials that may contain TTO are paints, thinners, degreasers, etc. In order to avoid costly TTO testing, manufacturers are encouraged to submit asolvent management plan to the Iowa DNR providing a listing of the TTO's present at the facility and the procedures used to safely store the 'IT0 products so that entry into floor drains or other sewer discharges is controlled. The plan should be submitted to the Water Permit Section, Surface and Groundwater Protection Bureau of the Iowa Department of Natural Resources, Environmental Protection Division, 900 E. Grand, Des Moines, IA 50319. After submission of the solvent management plan, manufacturers may request exemption from the TTO testing requirements by submitting the certification statement addressed in Section 2. The signed certification statement should be submitted monthly to the local wastewater treatment facility for inclusion with their wastewater monitoring report to the DNR. Should the DNR request sampling, analytical costs can be minimized by testing for only those TTOs identified at the facility. Any sludge or sediment which is generated from pretreatment should be tested for the characteristics of toxicity and corrosivity to determine whether the sludge is hazardous or nonhazardous (toxicity test parameters are included in Appendix C). Prior to sampling, the sludge should be dried in order to remove all free liquids. The sludge should also be tested for the Special Waste Authorization (SWA) parameters listed in Appendix K. The laboratories listed in Appendix J are capable of performing the necessary testing. If the sludge is not considered hazardous by EPA regulations and does not exceed any of the SWA parameters, it is eligible for disposal at the local sanitary landfill. To obtain a SWA, the application form included in Appendix K should be completed and sent to the Iowa DNR along with a copy of the test results. Upon approval of the SWA, the DNR will notify the designated landfill and send a copy of the SWA to the applicant. A SWA does obligate the receiving landfill to accept the waste; it merely allows disposal and informs the landfill operator that the waste will not cause any detrimental environmental effects. If the sludge exceeds the SWA parameters or demonstrates one or more characteristics of a hazardous waste, then it must be handled as a hazardous waste. A partial listing of hazardous waste management companies is enclosed as Appendix G. VI. PAINT AND THINNER WASTES

1. Existing Conditions: Almost 80% of the farm equipment manufacturers which were visited operate either a paint booth or a dip tank. Paints used in these processes are usually enamels, acrylics and lacquers. Since the paints are solvent based, thinners used to clean guns, gun lines and other miscellaneous equipment include methyl ethyl ketone, xylene, and toluene. The monthly waste generation rate from painting operations averages 15 gallons. Practically all farm equipment manufacturers that are involved in painting apply the paint through means of a spray system. Approximately 35% also utilize a dip tank, but less than 15% use dip tank methods only. Spray methods include airless, air-assisted airless, and some electrostatic. Dip tanks and water-wall paint booths tend to generate varying quantities of paint sludge which is then collected separately and handled as a hazardous or special waste. 2. Regulatory Review: Waste paint (solvent based) is only regulated as a hazardous waste if it demonstrates one of the characteristics of a hazardous waste. Some paints today still use heavy metal compounds as pigmenting agents and may demonstrate the characteristic of toxicity. The main concerns for paint disposal are solvent content, toxicity due to heavy metal pigment, and ignitability. In almost all cases, waste paints must be managed as a hazardous waste. If the paint wastes contain no heavy metals, less than 1% hydrocarbon content, and no free liquids then the paint may be sent to a sanitary landfill in Iowa. This would be applicable for dried latex and some enamel paint residues in containers. Before disposal in a landfill, the farm equipment manufacturer must be granted a SWA from the Iowa DNR. Solvents used as paint thinners are considered hazardous due to toxicity and ignitability characteristics. Most of these solvents have the EPA waste codes of F003, F005, and D001. Solvents that demonstrate any EPA hazardous waste characteristic are banned from Iowa sanitary landfill disposal or direct discharge to a public wastewater treatment facility. Paint sludges from water-wall booths and dip tanks must have their hazardous1 nonhazardous nature determined as well. These wastes should be tested for toxicity using the TCLP for the eight listed metals, benzene, and methyl ethyl ketone, and ignitability. Nonhazardous paint sludge may be disposed of in a municipal landfill provided a SWA has been obtained for the sludge. Testing for hazardous characteristics and SWA criteria can be accomplished concurrently. Wastewater generated from water-wall paint booths is subject to numerous regulations contingent upon other facility wastewater generation and receiving water constraints. 3. Recommendations: Thinners should be used until their cleaning capabilities have been exhausted. Thinner used as gun cleaner can be saved and then used later to thin the next batch of same color paint. Occasionally coloring can be a problem if many different colors are used, but this can be worked out by separating the different colored gun washes from the most common colors for subsequent use as thinner for that respective color. Mixing of paint and paint thinner is a reasonable method for elimination of small quantities of waste paint. For larger quantities of waste paint, it is recommended that the two wastes be kept separate. This allows the thinner to be less contaminated with paint sludge; thus the thinner waste can be reclaimed more readily. There are a number of solvent recyclers who will handle paint thinner with paint as a constituent provided that the paint sludge comprises only a small percentage of the total volume. The list of hazardous waste management companies Appendix G which are capable of handling paint wastes are denoted with an asterisk. On-site solvent reclamation is recommended when the total volume of solvent waste (including parts wash solvent) exceeds 30 gallons per month. Payback on a small distillation unit can be realized in six months where paint thinner constitutes more than 50% of all solvent waste. A list of distillation unit equipment vendors is included in Appendix E Still bottoms generated from distillation will need to be collected in a suitable container and marked as hazardous waste. Since still bottoms are considered hazardous waste, off-site disposal will be required. Frequency of still bottom disposal will depend on the facility's hazardous waste generator status (LQG, SQG, or CESQG). The appropriate EPA waste codes for still bottoms are F003, F005, and D001. Skimming of "killed" paint from water-wall paint booths is recommended. The collected skimmings should be accumulated with water-wall booth sludge and the hazardous1 nonhazardous nature determined. Latex and solvent based paint sludges should be tested for toxicity using the TCLP for the eight listed metals. Latex paint sludge which is not considered hazardous should be dried and tested for the SWA parameters (see Appendix K). Solvent based paint sludges should be TCLP tested for the eight listed metals, benzene and methyl ethyl ketone. Paint sludges which demonstrate toxicity should be collected in a suitable container and managed off-sitethrough a hazardous waste management company (see Appendix G). Water which has been removed from water-wall paint booths should be saved and reused in the process. This will eliminate the need to determine proper wastewater disposal methods. Booth wastewater which cannot be reused may be subject to numerous wastewater regulations. For more detailed information or site-specific information concerning wastewater disposal from water-wall paint booths, contact the IWRC (8001422-3109). To avoid potentially costly wastewater testing and disposal, it is recommended that water- wall paint booths be replaced by dry booths which use styrofoam filters (solvent based paints) or fiberglass filters (latex paints). Proper application of paint during spray processes is critical to reduce hazardous waste generation from overspray. To develop an effective paint application program, the IWRC recommends that facilities establish a training program for employees on paint spray techniques. An effective tool for training is a video camera. Employees can be trained in a classroom atmosphere showing how to apply paint with reduced overspray techniques. The employees are then videotaped during paint application to determine where poor techniques are being used. Once the employee can actually see the difference on tape of proper techniques, it is easier to develop improved methods. Appendix L contains information regarding proper paint spray application. There are several methods to reduce paint overspray waste. These include improved application techniques, equipment upgrades, electrostatic painting, powder coating, high solids heat-setting painting, and high volurnellow pressure painting. Electrostatic painting incorporates basic paint application and powder coating methods, has the least amount of associated overspray, and requires less frequent paint booth filter changes and other cleanup. In cases where electrostatic painting is not a feasible option, air-assisted airless is recommended. This type of application is less effective in reducing overspray than electrostatic methods but much more effectivethan airless systems. The air-assisted airless applies a "softer" finish since the paint is not being blasted onto the work piece under high pressure. Powder coating involves application of a plastic powder to the surface, followed by curing of the plastic in an oven. Overspray from powder coating can be collected in a small baghouse and then recycled for the next application. In many situations, a 99% waste reduction can be achieved by collecting and reusing powder overspray. Surfaces must be exceptionally clean in order to achieve desired finished surface results; however, phosphate coating is typically not required to accomplish necessary cleaning. Changing to powder coating can eliminate processes which generate regulated wastewaters. Dip tanks are not recommended since there is a lot of paint waste from dripping parts, and tank capacities require large volumes of paint to be available. Also, tank use always invites the possibility of leaks andlor tank contamination. Both of these possibilities can generate a large amount of hazardous waste in a few hours. With spray application, there is only a small chance that an entire batch of paint will become contaminated and be unusable. For these reasons, the IWRC strongly recommends replacing dip tanks with spray systems. Proper selection of equipment is important as well. Correct sizing of gun nozzles and settings of airlpaint ratios can have a major impact on minimizing waste generation and maximizing process efficiency. Aerosol cans, for quick paint application over small surface areas, should be replaced by use of an airbrush. Airbrushes are particularly effective for final touch-ups and minor reworks.

VII. PAINT BOOTH FILTERS

1. Existing Conditions: Farm equipment manufacturers which have a dry paint booth also generate paint booth exhaust filters. These filters are usually a paper-based or fiber material. Paint booth exhaust filters are changed every few weeks up to three months depending on the amount of painting being done. Waste filters are typically thrown in the trash for disposal at the local sanitary landfill. 2. Regulatory Review: Waste paint booth filters need to be tested for ignitability and toxicity characteristics. The TCLP is used to determine if the filters contain toxic materials. Eight listed heavy metals, benzene, and methyl ethyl ketone should be tested with the TCLP for their contamination levels. If any one parameter exceeds the regulatory levels listed in Appendix C, then the filters must be managed as a hazardous waste. If the filters are nonhazardous, and the SWA requirements are met, then the filters can be sent to a solid waste landfill after a SWA is obtained. 3. Recommendations: It is recommended that farm equipment manufacturers have their paint booth filters tested for ignitability and toxicity (using the TCLP test for the eight listed metals, methyl ethyl ketone and benzene). It is rare that a paint booth filter will test as a hazardous waste assuming that only typical paints have been used. Should the paint booth filters demonstrate one or more of the characteristics of a hazardous waste, they cannot be disposed of in an Iowa municipal landfill. The farm equipment manufacturer will need to have a hazardous waste management company handle the filters. Appendix G contains a list of these companies; those denoted by a pound sign (#) are capable of handling spent booth filters. It may be possible to determine which paint is causing the filters to be hazardous, and then eliminate or reduce its use. If the filters are not hazardous due to these characteristics, contain less than 1% hydrocarbon content, and contain no free liquids, then they may be disposed of in an Iowa sanitary landfill with a SWA. The waste must be tested for the SWA test parameters listed in Appendix K. If the test results demonstrate that the filters are nonhazardous and meet SWA criteria, then a SWA application (Appendix K) should be completed. An alternative to standard paper and fiberglass filters is to use styrofoam filters. This type of filter is relatively new and has baffles to collect paint overspray. The filters can be cleaned and reused a number of times. When these filters need to be changed, the spent filters can be dissolved in used thinner and then placed in the storage container. Disposal of polystyrene filters in spent thinner reduces the reclamation rate of the thinner, so care should be taken to avoid placing too many filters in any one container of waste thinner.

VIII.STORM WATER Recent amendments to the federal Clean Water Act require dischargers of storm waters to receive National Pollutant Discharge Elimination System (NPDES) permits for those discharges. Specifically, the new requirements apply to facilities which are (1) engaged in industrial activity, or (2) already regulated under the Clean Water Act (i.e., phosphate coating process wastewaters). Farm equipment manufacturing is designated by SIC # 3523. Facilities with SIC # 20,21, 22,23,2434,25,265,267,27,283,285,30,31(except 311), 323,34 (except 3441), 35 (including 3523), 36,37 (except 373), 38,39, and 4221 through 4225 must obtain a NPDES permit for storm water discharges from the following areas: materials handling equipment materials handling activities raw material storage and handling intermediate products storage and/or handling final product storage and/or handling by-product or waste material storage and/or handling industrial machinery storage, use, or handling Facilities with other SIC #'s may have additional areas that could require storm water NPDES permits. Application for a NPDES permit involves completion of Form 1, Form 2F and possibly Form 2C. Form 1is a general form for existing facilities which requests general information such as facility name and address, contact persons, nature of the business, water sources and uses, and wastewater handling arrangements. Form 2F is an application for a permit to discharge storm water discharges associated with industrial activity. This form requests specific information concerning storm water discharge outfalls, topographical maps which indicate present drainage systems, analytical data of storm water contaminants, and descriptions of wastewater discharges (storm water and process water). Form 2C requests further information concerning any process water discharges that are combined with storm water and the manner in which they are effectively treated prior to discharging to a public waterway. For new sources, Form 2D should be used in place of Form 2C. A summary of the requirements to obtain a NPDES individual permit for storm water discharges is included in Appendix M. If your facility would like an individual permit application, please contact the IWRC at 3191273-2079,

IX. NONHAZARDOUS SOLID WASTES

1. Existing Conditions: A small number of farm equipment manufacturers also fabricate wood, fiberglass, andlor plastic products or parts. Wood scraps and shavings are disposed of in a number of ways, for example: burned in a wood stove for energy recovery, sold as miscellaneous scrap to hobby and craft shops, and occasionally landfilled. Plastic scrap is usually generated as "flash" which is produced when a mold is overfilled or does not seal during part fabrication. Most scrap is collected and returned to vendors for regrinding although a small amount is landfilled. Fiberglass overspray and matting is typically placed in the trash for disposal. Recent recycling efforts have begun where the overspray is reground and used as a raw material for gypsum board and sheet rock. 2. Regulatory Review: Nonhazardous industrial waste regulation falls under the jurisdiction of the Iowa Department of Natural Resources (DNR). At this time, the DNR does not require a "Special Waste Authorization" (SWA) for wood, plastic, or fiberglass wastes. 3. Recommendations: The IWRC encourages and supports recycling of any material in order to reduce waste generation. Materials which can be easily recycled include paper, cardboard, scrap metal, pallets, and plastic. Recyclers of these materials are included in Appendix N. A by-product and waste exchange service within Iowa has been established where any Iowa business can offer or accept desired materials for reuse. Contact the IWRC at 800/422-3109 to discuss materials exchanges. Other sources of information regarding waste reduction and recycling are: WRAP (Waste Reduction Assistance Program) Iowa Department of Natural Resources Wallace State Office Building Des Moines, IA 50319-0034 1-800-367-1025 1-515-281-8951 Regional economic development centers can also provide assistance regarding by-product exchanges within their regions.

X. AIR EMISSIONS

1. Existing Conditions: All of the farm equipment manufacturers visited exhausted work area and paint booth air to the outside. This not only includes shop floor air but also the air exhausted from welding operations, paint booths and solvent usage areas. Paint booth air emission controls are usually limited to dry filters that collect paint particulates. No control of volatile solvents is practiced. 2. Regulatory Review: Air emission regulations are enforced by the DNR, contingent upon federal standards. Facilities or operations installed or modified since 1970, that have the potential to emit air pollutants (i.e., paint dust, solvent fumes, etc.), are required to obtain an air permit from the DNR. The air permitting process may require emission testing andlor control. Facilities and operations installed prior to 1970 do not require air permits (provided no major modifications have been completed since 1970) but still must comply with applicable emission limits. Spray paint booth emissions are primarily regulated for particulates. The emission limit is 0.01 grain per standard cubic foot of exhaust gas. Additional limits on toxic solvent emissions are applied on a case-by-case basis. 3. Recommendations: The requirements for air permits and emission control are currently under revision at both the state and federal levels. As a result, future regulatory requirements cannot be determined at this time. Stricter regulation and permitting for air toxics are likely as a result of the new Clean Air Act Amendments. Installation of new air emission sources such as paint booths should not be done until an air permit for construction is obtained from the DNR. The current air permit application form is enclosed as Appendix 0. Depending on the estimated air emissions, computer modeling of emissions may be required to veri& that no adverse health effects will result from the new source.

XI. HAZARDOUS WASTE MANAGEMENT AND STORAGE

1. Existing Conditions: Almost all of the farm equipment manufacturers visited collect spent solvents, thinners, paints, and oil. However, very few follow all of the storage and accumulation requirements. For example, no distinction is normally made between permanent storage and satellite storage; signs are sometimes inappropriately posted; manifests and other hazardous waste disposal documentation may be on file, but are not usually kept together in a well organized format. Most manufacturers rely on their hazardous waste disposal companies to provide completed manifests and other necessary documentation. 2. Regulatory Review: The EPA requires that gnerators of more than 220 lbslmonth and less than 2,200 lbs/ month (SQG's) of hazardous waste meet the requirements for the following areas: 1. EPA Identification Number 2. Waste Generation, Accumulation and Storage 3. Packaging, Marking and Placarding 4. Uniform Hazardous Waste Manifest 5. Satellite Storage 6. Use and Management of Containers 7. Container Marking 8. Preparedness and Prevention 9. Contingency Requirements 10. Recordkeeping An in-depth summary of these guidelines is included in Appendix B. The summary can be used as a checklist to implement appropriate activities. Generators of less than 220 lbslmonth of hazardous waste are considered Conditionally Exempt Small Quantity Generators (CESQG's). CESQG's are required to perform a hazardous waste determination for each waste generated at the facility and to manage them properly. Appropriate management includes treatment and disposal of hazardous wastes through an EPA permitted facility, no more than 2,200 pounds may be accumulated on-site at any given time, and waste containers must be properly labeled. A more detailed summary of the CESQG requirements is included in Appendix A. Use of a solvent still will affect the volume of hazardous waste generated from the facility and thus the generator category. There are two methods of counting the monthly generation rate when using a still; the easiest method is explained in detail in Appendix P. 3. Recommendations: The IWRC examines each of these areas during a free, confidential on-site review. All records concerning hazardous waste management are discussed with appropriate personnel. Specific recommendations are made on an individual basis as each facility differs. Some common areas that need improvements are: preparedness and prevention, employee training records, use of unique hazardous waste manifest number, accumulation start dates on drum labels, and posting of emergency phone numbers.

XII. SUPERFUND AMENDMENTS AND REAUTHORIZATION ACT (SARA) TITLE I11

SARA Title I11 reporting requirements that may apply to industrial facilities include the following sections: Section 304 - Emergency Notification Sections 311 and 312 - Community Right-to-Know Section 313 - Toxic Chemical Release Emergency Notification (Section 304) requires facilities to report and respond to releases of listed hazardous substances if the volume of material released could affect persons or resources outside the facility's boundary and is in excess of the reportable quantity (RQ) volume established for the particular substance. The listed hazardous substances that must be reported and their corresponding RQ values are listed in Attachments EHS and CERCLA of Appendix Q. Notification of the following agencies must be completed within six hours of identification of the release: State Emergency Response Commission (SERC) Local Emergency Planning Committee (LEPC) Department of Natural Resources (DNR) Additional information and step-by-step guidance to determine if release reporting is necessary is enclosed in Appendix Q. Community Right-to-Know (Sections 311 and 312) reporting is required to provide state and local officials and the public with specific information on hazardous chemicals present at a facility during the previous year. Materials which require MSDS by Occupational Safety and Health Administration (OSHA) must be reported if the quantity stored exceeds 10,000 pounds at any given time. Section 311 requires that facilities submit either copies of its MSDS or a list of MSDS chemicals to: State Emergency Response Commission (SERC) Local Emergency Planning Committee (LEPC) Local Fire Department Chemical lists must include the chemical name or common name of each substance and any hazardous component as provided on the MSDS and should be organized by categories of health and physical hazards. The initial (one time) submission of the MSDS's or list was required October 17,1987, or three months after the facility is required to have available an MSDS under OSHA regulations. A revised MSDS must be provided to update MSDS which were originally submitted if significant new information regarding a chemical is discovered. The reporting requirements of Section 312 involve annual submission of emergency and hazardous chemical inventory forms (Tier I1 forms) to agencies identified above for Section 311. The hazardous chemicals and reporting quantities covered by Section 312 are the same as those covered in Section 311. Tier I1 reporting is required by March 1 for the previous calendar year. Additional information and step-by-step guidance to determine if Community Right-to-Know reporting is necessary is enclosed in Appendix Q. Toxic Chemical Release Reporting (Section 313) is to inform government officials and the public about releases of toxic chemicals into the environment and also assists in research and development of regulations, guidelines, and standards. Reporting requirements apply to facilities that have ten or more full-time employees, that are in Standard Industrial Classification Codes (SIC) 20 through 39 and that manufacture, process, or otherwise use a listed toxic chemical in excess of specified threshold quantities. The listed chemicals may be found in Attachment TCL of Appendix Q. Facilities using listed toxic chemicals in quantities over 10,000 pounds in a calendar year are required to submit toxic chemical release forms by July 1 of the following year. Facilities manufacturing or processing any of these chemicals in excess of 25,000 pounds in a year are required to submit the form. Report data must be submitted on the Form R to the U.S. Environmental Protection Agency and the State Emergency Response Commission (SERC). Additional information and step- by-step guidance to determine if Toxic Chemical Release reporting is required is enclosed in Appendix Q.

Appendix A

Conditionally Exempt Small Quantity Generator Requirements

Conditionally Exempt Small Quantity Generator Requirements

Key: 1 kg = 2.2 lbs = 0.25-0.3 gal 100 kg = 220 1bs = 25-30 gal 1000 kg = 2200 lbs = 250-300 gal

A. Appb to facilities tkat:

-< 100 kg Generate less than 100 kucalendar month hazardous waste. -< 1kg Generate less than 1 kg of acute hazardous waste per calendar month. -< 1,000 kg Never accumulate more than 1,000 kg total of all (non-acute) hazardous waste on-site. -< 1 kg Never accumulate more than 1 kg of all acute hazardous waste on-site. Do not generate or accumulate more than 100 kg of residue, contaminated soil, waste, or other debris resulting from an acute hazardous waste spill.

B. Hazardous Waste Quantify Determination DOES NOT include:

Used oil, provided it has not been mixed with a hazardous waste.

Spent lead acid batteries that are being reclaimed.

C. Hazardous Waste Quantify Determination DOES include:

Recyclable materials stored before being recycled.

Hazardous waste burned for energy recovery (fuel blending for cement kilns).

Recyclable materials used for precious metal recovery (photographic developing solutions, especially fixer).

D. YiSmall Quantitg Generator Requirements:

Determine whether waste(s) are hazardous.

Stay below generation and storage cutoff limits, and document that the facility is under the limits.

Treatment/disposal must occur at a RCRA facility or a legitimate recycling facility.

Conditionally Exempt Small Quantity Generator waste cannot go to a solid waste landfill under state law. E. Concem/Complicating Factors:

Small amounts may need to be accumulated over long periods of time to make pickup by commercial hazardous waste firm feasible.

Large amount of waste with reduce regulation (e.g. silver containing waste) may mean a very small amount of other hazardous waste must be manage by strict regulation facility space. 200 kglmonth fixer 1 gallonlmonth solvent Fixer -+ only manifest requirements apply Solvent -+ all AQG requirements apply Appendix B

Small Quantity Generator Requirements

Requirements for Small Quantity Generators* of Hazardous Waste

A. EPA Identification Number 1. An Environmental Protection Agency (EPA) Identification Number must be obtained from U.S. EPA Region VII in Kansas City, Kansas using the "Notification of Hazardous Waste Activity" form (Attachment Sl). the facility has an EPA ID Number, it can continue to use that number. EPA ID Number is used in shipping waste off-site. B. Waste Generation Accumulation, and Storage 1. Waste is generated at a rate of 100-1,000 kglcalendar month on a regular or intermittent basis. 2. If waste is generated at a rate greater than 1000 kglcalendar month (2,200 lbs.), then the generator immediately becomes subject to large quantity-generator regulations. 3. Quantity of waste accumulated on-site may never exceed 6000 kilograms (13,200 lbs.). 4. Up to 6,000 kilograms may be stored on-site for 180 days (or 270 days if the waste must be transported more than 200 miles). 5. If waste is accumulated in quantities exceeding 6,000 kilograms or stored for more than 180 days (or 270 days, if applicable), then the generator is an operator of a storage facility subject to hazardous waste permit requirements. C. Packaging, Marking and Placarding 1. Before transporting waste off-site the waste must be packaged, labeled and marked according to Department of Transportation (DOT) hazardous materials transport regulations. 2. Each container for transport must be marked with the following: HAZARDOUS WASTE - Federal Law Prohibits Improper Disposal. If found, contact the nearest police or public safety authority or the U.S. Environmental Protection Agency. Generator's Name and Address Manifest Document Number Commercially available labels can be used. (Attachment S2). 3. Before transporting, the generator must offer the appropriate placards to the transporter according to DOT regulations (the transporter may supply appropriate placards).

D. UniformHazardous Waste Manifest 1. All shipments of hazardous waste must be accompanied by a Uniform Hazardous Waste Manifest (Attachment S3). 2. The manifest must consist of copies for the generator, transporter, and operator of the designated facility; and a copy to be returned to the generator by the designated facility. 3. The generator must receive a signed copy from the designated facility within 60 days-if not received, then the generator must submit a copy of the manifest to EPA and indicate that waste delivery was not confirmed. * 100-1,000 kg of hazardous waste per calendar month = 220-2,200 Ibslmonth 4. Manifest requirements do not apply to hazardous waste where Waste is reclaimed under a contractual agreement, 5pe of waste, frequency of shipments are specified in the agreement, Transport vehicle used to transport the waste to the recycling facility and to deliver regenerated material back to the generator is owned and operated by the reclaimer, and Generator maintains a copy of the agreement for three years after termination. 5. A "Treatment Standard Notification" (TSN) for wastes subject to Land Ban restrictions must accompany the manifest, and a copy of the TSN should be kept on file. An example TSN is included as Attachment S4. Wastes which commonly require a TSN include: Chlorinated solvents: methylene chloride, dichlorobenztne, etc.; designated as F001, F002. Non-chlorinated solvents: toluene, xylene, methanol, etc.; designated as F003, F004, or F005. Liquid waste with heavy metals such as cadmium, chromium, lead, or mercury. Liquid waste with pH c2. E. Satellife Storage 1. Up to 55 gallons may be accumulated at one or several individual generation points (satellite storage areas). 2. Containers must be kept closed and marked to identify contents. 3. When more than 55 gallons are accumulated at any one satellite site, the waste must be moved to the designated storage area within three (3) days.

F. Use crnd Management of Containers 1. Containers must be in good condition and nbt leaking. 2. Containers must be compatible with the waste. 3. Containers must be stored closed. 4. Container storage area must be inspected weekly and record of inspection kept on file. 5. Incompatible wastes must not be placed in same container or stored in close proximity. 6. If tanks are used to store hazardous waste, then management standards in 40 CFR 265 Subpart J must be followed.

G. Container Marking 1. The date when waste accumulation in the container begins must be clearly marked on the stored container. 2. The stored container must be marked with the words" HAZARDOUS WASTE."

H. Preparedness and Prevention 1. Storage facilities must be maintained and operated to minimize the possibility of fire, explosion or release of hazardous waste. 2. Facilities must be equipped with or provide immediate access to the following: Internal communications or alarm system, Device (e.g., telephone) to summon emergency assistance from local authorities, Fire extinguisher and control equipment, Spill control equipment, Water to supply hoses, or sprinkler systems. 3. All equipment must be tested and maintained to assure proper operation. 4. When hazardous waste is handled, all personnel involved must have immediate access to an internal alarm or emergency communication device. 5. If just one employee is present, he must have immediate access to a device capable of summoning external assistance (e.g. telephone). 6. Aisle space must be maintained to allow for fire protection and spill control in an emergency. 7. The generator must make the following arrangements with local authorities: Arrangements to familiarize police, fire departments, and emergency response teams with the layout of the facility, properties of hazardous waste handled at the facility and associated hazards, places where facility personnel would normally be working, entrances to roads inside the facility, and possible evacuation routes; Where more than one police and fire department might respond to an emergency, agreements designating primary emergency authority to a specific police and a specific fire department and agreements with any others to provide support to the primary emergency authority; Arrangements with state emergency response teams, emergency response contractors and equipment suppliers; and Arrangements to familiarize local hospitals with the properties of hazardous waste handled at the facility and the types of injuries or illnesses which could result from fires, explosions or releases at the facility. 8. Where authorities decline to enter into arrangements, documentation of the attempt to make arrangements (e.g., certified letter requesting arrangements) must be kept on file (see example letter on page B-4). I. Contingencg Requirements 1. At all times, there must be at least one employee available or on call with the responsibility for coordinating all emergency response measures (emergency coordinator). 2. The following information must be posted at the telephone closest to the storage area (see attachment S5): Name and telephone number of emergency coordinator(s); Location of fire extinguisher, spill control material and fire alarm; and Telephone number of the fire department. 3. All employees involved in waste handling and management must be thoroughly familiar with proper waste handling and emergency procedures (records of training should be kept on file). 4. The emergency coordinator must respond appropriately to emergencies as follows: Fire; call the fire department andlor attempt to extinguish it. Spill; contain the flow of waste and clean up waste and contaminated materials/soil to prevent or minimize release to the environment. Release threatening human health outside the facility or spill reaching surface water; notify the National Response Center. (1-8001424-8802) 5. A Contingency Plan can be written and kept on file to document compliance with these requirements.

J. Recordkeeping 1. Signed manifest copies must be kept on file for three years. 2. Records of waste test results or analyses must be kept for three years from the date that the waste was last sent to treatment, storage or disposal. 3. Records to document compliance with other sections (e.g. weekly inspection log) should be kept on file. Date

To (Specific Individual; ie. Fire Chief, Police Captain, Hospital Administrator by name.)

Re: Notification of Small Quantity Waste Generation Activity

~omvanuname generates small quantities (less than 1,000 kglmonth) of hazardous waste, which is accumulated for time veriod before being collected by an authorized transporter. The waste is fsrve of wasfeo. This waste is collected and stored in our location ofstoraoe area which is located at Ures(see drawing). The maximum amount stored at any one time is less than number gallons. . . A Material Safety Data Sheet for the ~ngznalmaterra[ is enclosed. Fie and health risks from the used material are expected to be similar to that of the original material.

This letter is sent in order to fulfill 40 CFR Part 262.34 (d)(4) of the Federal Hazardous Waste Regulations.

Sincerely,

Authorized Personnel

Enclosure

Note: Send letter by certified mail so a return receipt can document that the letter was received. EPA Form 8700-12 (07-90)Prevlous edition Is obsolete. -1 - Form Appmed. OMB No. 20YJ4Q28. Emres 10-31-81 Please print or type wrth ELITE type (12 characters per inch) in the unshaded areas on)y GSA NO. 024B-EPWT

EPA Form 8700-12 (07-90) Previous editlon Is obsolete. -2 - Attachment S2

HAZARDOUS

FEDERAL LAW PROHIBITS IMPROPER DISPOSAL IF FOUND, CONTACT THE NEAREST POLICE, OR PUBLIC SAFETY AUTHORITY, OR THE U.S. ENVIRONMENTAL PROTECTION AGENCY

PROPER D.O.T. SHIPPING NAME UN OR NA# GENERATOR INFORMATION: bd NAME H ADDRESS ,& 4 CITY STATE ZIP EPA E PA 10 NO WASTE NO ACCUMULATION MANIFEST 11 START DATE DOCUMENT NO $1 CONTAINSHANDLE HAZARDOUS WITH OR TOXIC CARE! WASTES \. 1 STYLE WM.6 >>-&a >>-&a L2L.A. LLLL-LA Prlnteo by LABELMASTER DIV of AMERICAN LABELMARK CO INC CHICAGO -IL 60646 Attachment 53

Please mnt or tvw (Form desancd fu use cr etm (12-MchlbWU 1 Form Ap~rovedOM6 No 2050.0030 Exoms 9-30. ID No Document UNIFORM HAZARDOUS 1 Generators us 2 Page 1 lnformat~onIn the shaded area' IS not requlred by Federal law WASTE MANIFEST I I of 3 Generators Name and Matllng Address A Stale Manlfest Document Number

6 State Generator's ID 4 Generatoh Phone ( 1 5 Transponer 1 Company Name 6. US EPA ID Number C State Transponers ID I D Transponets Phone 7. Transporter 2 Company Name 8 US EPA ID Number E State Transponers ID I F Transponer's Phone 9 Des~gnatedFac~llty Name an0 Stte Address 10. US EPA ID Number G. State Factl~ty'sID

#. Factllty's Phone I 12 Conta~ners 13 14 1. 11. US DOT Descriptton (Includ~ngProper Shrpptng Name. Hazard Class and ID Number) Total Unlt Waste No. WtNol G f~i~ No Type Ouanttry :a E I A, r b. 0 I

C

d

J Addlttonal Descrlptlons for Matertals Ltsted Above K Handl~ngCodes for Wastes Ltsted Above

15 Specral Handltng lnsirucr~onsan3 Aadttronal Informallon

' 16 GENERATOR s CERTIFICATION I nere3y oec1a.e tw: tne conrents ot tnls conslgqment ace fully an0 a:curate~y oescr~oeoa3ove ay proler rwpolnp name .no are c,ars~t~edpacneo marneu rno 1a3c1.0 .no are m a11 respects In pfoDer conoitlon lor trans~orr3y hlgnway accord~ngto appl~cab~e~nterna:~ona ano nrt~onangove*nment regulrt~ons If I am a large quan:lty ge?e.arot I crrtlly lhal I nave r program m Otace to reouce tne volume rno tarlcltv 01 waste generated to the oegree I have oe:erm~neoto bt econom~callypract~cr),e .no (na. Inave re e:tea t?e practlca3le metnoo of treatment storage or a~saosaCurrently ava1la5le to me when mlnlmlzes :1t 3resel' an( tuture tnreat 10 numan nealln anC tne enr~ronmenr OR I1 I am a small auantlty generator Ihave maoe a go00 taltn ett0rl lo mlntmlze my waste ge?eva:eon an0 rehec the best waste rnanar~e~ew?et?ay tna' IS ma ,role IC me an0 :?at Icaq a'lorc Pr~nted/lyped Name S1gnatu.e Mom Day Yec I I I T 17 Transponer 1 Acknowledgement of Recelptof Malerrals R A Pnntedflyped Name Stgnature Mon:n Day Ye; N S P I I I 0 18 Transporter 2 Acknowledgement of Receipt 01 Matertals R r Pnntedflyped Name Signature Month Day Yei E R I I I 19 Olscrepancy tndtcat~onSpace

F A C I L, I 20 Factlrty Owner or 0~erz:or Csrllflcat~onof recetpl of hazardous materials covered by thls manifest except as noted In Item I9 1 v Pnnted/lypea Name Signature Monrn Day Yet I I I c.",- C.C..P.. .. . > - - . .--., -1. r ---- rr r1- r -r. ., - - -A. --- Attachment ~4

Notification of Treatment Requirements for FOOl through F005 Wastes

Number of Attached Manifest: EPA Hazardous Waste Numbers:

This form serves to notify that the above listed waste codes shipped under the attached manifest may contain the FOOl through F005 spent solvents identified under column B below. As such, notification is also served to that these same wastes are required to be treated to meet the treatment standards of 40CFR Part 268 Support D; as identified by column C below.

(A) (B (C) 40CFR Part 268 Generator1Service Co. Support D F001-F005 Check if contained Treatment Standard Spent Solvents in waste rnalliter CCWE acetone N-butyl alcohol carbon disulfide carbon tetrachloride chlorobenzene cresols (and cresylic acid) cyclohexanone 1.2-dichlorobenzene ethyl acetate ethyl benzene ethyl ether isobutanol methanol methylene chloride methyl ethyl ketone methyl isobutyl ketone nitrobenzene pyridine tetrachloroethylene toluene 1, 1,l-trichloroethane 1,1,2-trichloro -1,2,2-trifluoroethane trichloroethylene trichlorofluoromethane xylene

Signature: Title : Print Name: Date Submitted: Company Name1 Location: EPA or State ID Number:

This notification must be attached to the mmifest for shipment. Please attach waste analysis data, if available- Attachment S5

POL ICE FIRE AMBULANCE NATIONAL RESPONSE CENTER 1-800-424-8802 EPA REGION VII 1-800-223-0425 IOWA DNR 1-800-532-1114 COMPANY NAME ADDRESS

MAJOR WASTE TVPES

EMERGENCY COORDINATORS AND PHONE NUMBERS

LOCATION OF FIRE EXTINGUISHER

SPILL CONTROL MaTERIAL

FIRE ALARM

FIRST AID STATION

Inra Wnct,a Kcductrinn Center

/!.,lc CU.LPfCPrinted by UBELMASTER. Dlv, oIAMERlCAN LABELMARK C0. CHICAGO. I1 60Wf Appendix C

Hazardous Waste Definitions

Toxicity Characteristic Leaching Procedure (TCLP)

Regulatory EPA Hazardous Parameter Ida& lvh&wmh * Arsenic 5.0 mgil * Barium 100.0 mgil Benzene 0.5 mg/l * Cadmium 1.0 mgA Carbon tetrachloride 0.5 mgil

Chlordane 0.03 mgA Chlorobenzene 100.0 mgil Chloroform 6.0 mgA * Chromium 5.0 mg/l m-Cresol 200.0 mgA

0-Cresol p-Cresol Cresols (total) 14-Dichlorobenzene 1,2-Dichloroethane

1,l-Dichloroethylene 0.7 mg/1 2,4-Dinitrotoluene 0.13 mgil * Endrin 0.02 mll Heptachlor 0.008 mgA . Hexachlorobenzene 0.13 mgil Hexachloro-1,3-butadiene Hexachloroethane * Lead * Lindane * Mercury

* Methoxychlor Methyl ethyl ketone Nitrobenzene Pentachlorophenol Pyridine

* Selenium * Silver Tetrachloroethylene * Toxaphene Trichloroethylene

Vinyl chloride * 2,4,-D * 2,4,5-TP 2,4,5-Trichlorophenol 2,4,6-Trichlorophenol

* Former EP Toxicity Parameters

VII. Reprint of Part 261 from Title 40 of Ihc Code of Federal Regulations

Protection of Environment

PART 261

Revised as of July 1,1989

CONTAINING A CODIFICATION OF DOCUMENTS OF GENERAL APPUCABIUTY AND FUTURE EFFECT AS OF JULY 1, 1989

With Ancillaries

Published by the Office of the Federal Register National Archives and Records Administration

as a Special Edition of the Federal Register Part 261 40 CFR Ch. 1 (7-1-89 Edition)

APPENDIX X-METHOD OF ANALYSIS FOR C~IORINATEDDIBENZO-P-DIOXINS AND -DI- PART 26 1-IDENTIFICATION AND BENZOFURANS LISTING OF HAZARDOUS WASTE AUTHORITY:42 U.S.C. 6905, 6912ta). 6921, 6922, and 6938.' Subpart A4eneral SOURCE:45 F'R 33119, May 19, 1980, unless Sec. otherwise noted. 261.1 Purpose and scope. 261.2 Definition of solid waste. 261.3 Definition of hazardous waste. Subpart A-General 261.4 Exclusions. 261.5 Special requirements for hazardous S 261.1 Purpose and scope. waste generated by conditionally exempt small quantity generators. (a) This part identifies those solid 261.6 Requirements for recyclable materi- wastes which are subject to regulation als. as hazardous wastes under Parts 262 261.7 Residues of hazardous waste in through 265, 268, and Parts 270, 271, empty containers. and 124 of this chapter and which are subject to the notification require- Subpart &-Criteria for Identifying the Charac- ments of section 3010 of RCRA. In teristics of Hazardous Waste and for List- this part: ing Hazardous Wastes (1) Subpart A defines the terms 261.10 Criteria for identifying the charac- "solid waste" and "hazardous waste", teristics of hazardous waste. identifies those wastes which are ex- 261.11 Criteria for listing hazardous waste. cluded from regulation under Parts 262 through 266, 268 and 270 and es- Subpart C-Charadarlrtics of Hazardous tablishes special management require- Waste ments for hazardous waste produced 261.20 General. by conditionally exempt small quanti- 261.21 Characteristic of ignitability. ty generators and hazardous waste 261.22 Characteristic of corrosivity. which is recycled. 261.23 Characteristic of reactivity. (2) Subpart B sets forth the criteria 261.24 Characteristic of EP toxicity. used by EPA to identify characteris- tics of hazardous waste and to list par- Subpart 0-Lists of Hazardous Wastes ticular hazardous wastes. 261.30 General. (3) Subpart C identifies characteris- 261.31 Hazardous wastes from non-specific tics of hazardous waste. sources. (4) Subpart D lists particular haz- 261.32 Hazardous wastes from specific sources. ardous wastes. 26 1.33 Discarded commercial chemical (b)(1) The definition of solid waste products, off-specification species, con- contained in this part applies only to tainer residues, and spill residues there- wastes that also are hazardous for pur- of. poses of the regulations implementing Subtitle C of RCRA. For example, it does not apply to materials (such as APPENDIX I-REPRESENTATIVE SAMPLINGnon-hazardous scrap, paper, textiles, METHODS or rubber) that are not otherwise haz- APPENDIX 11-EP TOXICITYTEST PROCE- ardous wastes and that are recycled. DURES APPENDIX 111-CHEMICAL ANALYSIS TEST (2) This part identifies only some of METHODS the materials which are solid wastes APPENDIX IV-[RESERVED FOR RADIOACTIVEand hazardous wastes under sections WASTETEST METHODS] 3007,3013, and 7003 of RCRA. A mate- APPENDIX V-[RESERVED FOR INFECTIOUSrial which is not defined as a solid WASTETREATMENT ~PECIPICATIONS~ waste in this part, or is not a hazard- APPENDIX VI-[RESERV~D FOR ETIOLOQIC waste identified or listed in this AGENTSI ous APPPSDIX VII-BASIS ?OR LISTINGHAZARD- part, is still a solid waste and a hazard- OUS WASTE ous waste for purposes of these sec- APPENDIX VIII-~OVSCONSTTTVIE#TS tions If: APPWDXX IX-WASTES EXCLUDEDUNDER (i) In the case of sections 3007 and (1 260.20 AKD 260.22 3013, EPA has reason to believe that Environmental Protection Agency the material may be a solid waste when worn or superfluous can be recy- within the meaning of section 1004(27) cled. of RCRA and a hazardous waste (7) A material is "recybled" if it is within the meaning of section 1004(5) used, reused, or reclaimed. of RCRA; or (8) A material is "accumulated spec- (ii) In the case of section 7003, the ulatively" if it is accumulated before statutory elements are established. being recycled. A material is not accu- (c) For the purposes of 55 261.2 and mulated speculatively, however, if the 261.6: perzon accumulating it can show that (1) A "spent material" is any materi- the material is potentially recyclable al that has been used and as a result and has a feasible means of being recy- of contamination can no longer serve cled; and that-during the calendar the purpose for which it was produced year t commencing on January 1)-the without processing; amount of material that is recycled, or (2) "Sludge" has the same meaning transferred to a different site for recy- used in g 260.10 of this chapter; cling, equals at least 75 percent by (3) A "by-product" is a material that weight or volume of the amount of is not one of the primary products of a that material accumulated at the be- production process and is not solely or ginning of the period. In calculating separately produced by the production the percentage of turnover, the 75 per- process. Examples are process residues cent requirement is to be applied to such as slags or distillation column each material of the same type (e.g., bottoms. The term does not include a slags from a single smelting process) co-product that is produced for the that is recycled tin the same way (i.e., general public's use and is ordinarily from which the same material is recov- used in the form it is produced by the ered or that is used in the same way). process. Materials accumulating in units that (4) A material is "reclaimed" if it is would be exempt from regulation processed to recover a usable product, under 5 261.4

Use Energy Speculatie mstitmn9 -ery/fuel matio ion accumulam "SPOSa' (# '2(c)(3)) (9 261.2(c)(l)) (5 261.2(~)(2)) (9 261.2(~)(4))

(1) (2) (3) (4)

Spent Materials...... (*I , (*I (7 (*I Sludges (listed in 40 CFR Part 261.31 w 261.32) ...... (-1 (*I to) (-1 Sludges exhibitrng a characteristic 01 hazardous waste ...... (*I ( ) ...... (-1 By-products (listed in 40 CFR Part 261.31 or 261.32) ...... (*I (*I (*) (7 By-products exhibiting a characteristic of hazardous mste ...... (*I ( *) ...... (*) Commercial chemical products listed in 40 CFR 261.33 ...... (*I (*) ...... Scrap metal ...... (*I (*I (7 . (-1 Note: The terms "spont materials". "st-', "by-poducts," and "scrap metal" are defined in 9 261 .l. (dl Inherently waste-like mate-. substitute tor are found in raw materi- The following materials are solid als or products in smaller concentra- wastes when they are recycled in any tions) and are not used or reused manner: during the recycling process; and (1 Hazardous Waste Nos. F020, F021 (ii) The material may pose a sub- (unless used as an ingredient to make stantial hazard to human health and a product at the site of generation), the environment when recycled. F022, F023, F026, and F028. (el Materials that are not solid waste (2) The Administrator will use the when recycled. (1) Materials are not following criteria to add wastes to that solid wastes when they can be shown list: to be recycled by being: (i)(A) The materials are ordinarily (i) Used or reused as ingredients in disposed of, burned, or incinerated; or an industrial process to make a prod- (B)The materials contain toxic con- uct, provided the materials are not stituents listed in Appendix VIII of being reclaimed: or Part 261 and these constituents ue not ordinarily found in raw materials (ii) Used or reused as effective sub- or produce for which the materials stitutes for commercial products; or Environmental Protection Agency (iii) Returned to the original process (i) It exhibits any of the characteris- from which they are generated, with- tics of hazardous waste identified in out first being reclaimed. The material Subpart C. must be returned as a substitute for (ii) It is listed in Subpart D and has raw material feedstock, and the proc- not been excluded from the lists in ess must use raw materials as principal Subpart D under 99 260.20 and 260.22 feedstocks. of this chapter. (2) The following materials are solid (iii) It is a mixture of a solid waste wastes, even if the recycling involves and a hazardous waste that is listed in use, reuse, or return to the original Subprcrt D solely because it exhibits process (described in paragraphs t e )( 1) one or more of the characteristics of (i) through (iii) of this section): hazardous waste identified in Subpart C, unless the resultant mixture no (i) Materials used in a manner con- longer exhibits any characteristic of stituting disposal, or used to produce hazardous waste identified in Subpart products that are applied to the land; C. or (iv) It is a mixture of solid waste and (ii) Materials burned for energy re- one or more hazardous wastes listed in covery, used to produce a fuel, or con- Subpart D and has not been excluded tained in fuels; or from this paragraph under 55 260.20 (iii) Materials accumulated specula- and 260.22 of this chapter; however, tively; or the following mixtures of solid wastes (iv) Materials listed in paragraph and hazardous wastes listed in Sub- (dl(1) of this section. part D are not hazardous wastes (f) Documentation of claims that t except by application of paragraph materials are not solid wastes or are (al(2) (i) or (ii) of this section) if the conditionally exempt from regulation. generator can demonstrate that the Respondents in actions to enforce reg- mixture consists of wastewater the dis- ulations implementing Subtitle C of charge of which is subject to regula- RCRA who raise a claim that a certain tion under either section 402 or sec- material is not a solid waste, or is con- tion 307(b) of the Clean Water Act (in- ditionally exempt from regulation, cluding wastewater at facilities which must demonstrate that there is a have eliminated the discharge of known market or disposition for the wastewater) and: material, and that they meet the (A) One or more of the following terms of the exclusion or exemption. spent solvents listed in 8 261.31- In doing so, they must provide appro- carbon tetrachloride, tetrachloroethy- priate documentation (such as con- lene, trichoroethylene-Provided, tracts showing that a second person That the maximum total weekly usage uses the material as an ingredient in a of these solvents (other than the production process) to demonstrate amounts that can be demonstrated not that the material is not a waste, or is to be discharged to wastewater) divid- exempt from regulation. In addition, ed by the average weekly flow of owners or operators of facilities claim- wastewater into the headworks of the ing that they actually are recycling facility's wastewater treatment or pre- materials must show that they have treatment system does not exceed 1 the necessary equipment to do so. part per million; or (B) One or more of the following 150 FR 664, Jan. 4, 1985, as amended at 50 spent solvents listed in 5 261.31-meth- FR 33542, Aug. 20, 19851 ylene chloride, l,l,l-trichloroethane, 9 261.3 Definition of hazardous waste. chlorobenzene, o-dichlorobenzene, cre- sols, cresylic acid, nitrobenzene, tolu- (a) A solid waste, as defined in ene, methyl ethyl ketone, carbon di- O 261.2, is a hazardous waste if: sulfide, isobutanol, pyridine, spent (1) It is not excluded from regula- chlorofluorocarbon solvents-provided tion as a hazardous waste under that the maximum total weekly usage 8 261.4(b); and of these solvents (other than the (2) It meets any of the following cri- amounts that can be demonstrated not teria: to be discharged to wastewater) divid- 40 CFR Ch. 1 (7-1-89 Edition)

ed by the average weekly flow of the listing description set forth in wastewater into the headworks of the Subpart D. facility's wastewater treatment or pre- (2) In the case of a mixture of solid treatment system does not exceed 25 waste and one or more listed hazard- parts per million; or ous wastes, when a hazardous waste (C) One of the following wastes listed in Subpart D is first added to listed in B 261.32-heat exchanger the solid waste. bundle cleaning sludge from the petro- (3) In the case of any other waste leum refining industry (EPA Hazard- (including a waste mixture), when the ous Waste No. K050); or waste exhibits any of the characteris- (D)A discarded commercial chemi- tics identified in Subpart C. cal product, or chemical intermediate (c) Unlw and until it meets the cri- listed in 4 261.33, arising from de mini- teria of paragraph (dl: mis losses of these materials from (1) A hazardous waste will remain a manufacturing operations in which hazardous waste. these materials are used as raw mate- ( 2)( 1) Except as otherwise provided rials or are produced in the manufac- in paragraph tc)(2)(ii) of this section, turing process. For purposes of this any solid waste generated from the subparagraph, "de minimis" losses in- treatment, storage, or disposal of a clude those from normal material han- hazardous waste, including any sludge, dling operations te.g. spills from the spill residue, ash, emission control unloading or transfer of materials dust, or leachate (but not including from bins or other contahers, leaks precipitation run-off) is a hazardous from pipes, valves or other devices waste. (However, materials that are re- used to transfer materials); minor claimed from solid wastes and that are leaks of process equipment, storage used -beneficially are not solid wastes tanks or containers; leaks from well- and hence are not hazardous wastes maintained pump packings and seals; under this provision unless the re- eample purgings; relief device dis- claimed material is burned for energy charges; discharges from safety show- recovery or used in a manner consti- ers and rinsing and cleaning of person- tuting disposal.) al safety equipment; and rinsate from (ii) The following solid wastes are empty containers or from containers not hazardous even though they are that are rendered empty by that rins- generated from the treatment, stor- ing; or age, or disposal of a hazardous waste, (El Wastewater resulting from labo- unless they exhibit one or more of the ratory operations containing toxic (TI characteristics of hazardow waste: (A) wastes listed in Subpart D, Provided, Waste pickle liquor sludge generated That the annualized average flow of by lime stabilhation of spent pickle laboratory wastewater does not exceed liquor from the iron and steel industry one percent of total wastewater flow (SIC Codes 331 and 332). into the headworks of the facility's (B)Waste from burning any of the wastewater treatment or pre-treat- materials exempted from regulation ment system, or provided the wastes, by 8 261.6ta)(3) tv) through (ix). combined annualized average concen- (dl Any solid waste described in tration does not exceed one part per paragraph (c) of this section is not a million in the headworks of the facili- hazardous waste if it meets the follow- ty's wastewater treatment or pre-treat- ing criteria: ment facility. Toxic (TI wastes used in (1) In the case of any solid waste, it laboratories that are demonstrated does not exhibit any of the character- not to be discharged to wastewater are istics of hazardous waste identified in not to be included in this calculation. Subpart C. (b) A solid waste which is not ex- (2) In the case of a waste which is a cluded from regulation under para- listed waste under Subpart D, contains mph ( s)(1 ) of this section becomes a a waste listed under Subpart D or is hazardous waste when auy of the fol- derived from a waste listed in Subpart lowing events occur: 2 D, it also has been excluded from (1) In the case of a waste listed in paragraph (c) under 4 4 260.20 and Subpart D, when the waste first meets 260.22 of this chapter. Environmental Protection Ageney 145 FR 33119, May 19, 1980, as amended at (ii) Reclamation does not involve 46 F'R 56588, Nov. 17, 1981; 50 FR 14219, controlled flame combustion (such as Apr. 11, 1985; 50 F'R 49202, Nov. 29, 1985; 52 occurs in boilers, industrial furnaces, FR 11821, Apr. 13,19871 or incinerators 1; g 261.4 Exclusions. (iii) The secondary materials are never accumulated in such tanks for (a) Materials which are not solid over twelve months without being re- wastes. The following materials are claimed; and not solid wastes for the purpose of this (iv) The reclaimed material is not part: used to produce a fuel, or used to ( 1)(i) Domestic sewage; and (ii) Any mixture of domestic sewage produce products that are used in a and other wastes that passes through manner constituting disposal. a sewer system to a publicly-owned (b) Solid wastes which are not haz- treatment works for treatment. "Do- ardous wastes. The following solid mestic sewage" means untreated sani- wastes are not hazardous wastes: tary wastes that pass through a sewer (1) Household waste, including system. household waste that has been collect- (2) Industrial wastewater discharges ed, transported, stored, treated, dis- that are point source discharges sub- posed, recovered te.g., refuse-derived ject to regulation under section 402 of fuel) or reused. "Household waste" means any material (including gar- the Clean Water Act, as amended. bage, trash and sanitary wastes in [Comment: This exclusion applies only to septic tanks) derived from households the actual point source discharge. It does (including single and multiple resi- not exclude industrial wastewaters while they are being collected, stored or treated dences, hotels and motels, bunk- before discharge, nor does it exclude sludges houses, ranger stations, crew quarters, that are generated by industrial wastewater campgrounds, picnic grounds and day- treatment.I use recreation areas). A resource re- covery facility managing municipal (3) Irrigation return flows. solid waste shall not be deemed to be (4) Source, special nuclear or by- treating, storing, disposing of, or oth- product material as defined by the erwise managing hazardous wastes for Atomic Energy Act of 1954, as amend- the purposes of regulation under this ed, 42 U.S.C.2011 et seq. subtitle, if such facility: (5) Materials subjected to in-situ mining techniques which are not re- (i)Receives and burns only moved from the ground as part of the (A) Household waste (from single extraction process. and multiple dwellings, hotels, motels, (6) Pulping liquors (i.e., black liquor) and other residential sources) and that are reclaimed in a pulping liquor (B)Solid waste from commercial or recovery furnace and then reused in industrial sources that does not con- the pulping process, unless it is accu- tain hazardous waste; and mulated speculatively as defined in (ii) Such facility does not accept haz- 8 261.ltc) of this chapter. ardous wastes and the owner or opera- (7) Spent sulfuric acid used to tor of such facility has established produce virgin sulfuric acid, unless it contractual requirements or other ap- is accumulated speculatively as de- propriate notification or inspection fined in 6 261.ltc) of this chapter. procedures to assure that hazardous (8) Secondary materials that are re- wastes are not received at or burned in claimed and returned to the original such facility. process or processes in which they (2) Solid wastes generated by any of were generated where they are reused the following and which are returned in the production process provided: to the soils as fertilizers: (i) Only tank storage is involved, and (i) The growing and harvesting of the entire process through completion agricultural crops. of reclamation is closed by being en- (ii) The raising of animals, including tirely connected with pipes or other animal manures. comparable enclosed means of convey- (3) Mining overburden returned to ance; the mine site. 40 CFR Ch. 1 (7-1-89 Edition)

(4) Fly ash waste, bottom ash waste, hair save/chrome tm/retan/wet slag waste, and flue gas emission con- finish; retan/wet finish; no beam- trol waste generated primarily from house; through-the-blue. the combustion of coal or other fossil (D)Sewer screenings generated by fuels. the following subcategories of the (5) Drilling fluids, produced waters, leather tanning and finishing indus- and other wastes associated with the try: Hair pulp/crome tan/retan/wet exploration, development, or produc- finish; hair save/chrome -/retan/ tion of crude oil, natural gas or geo- wet finish; retan/wet finish; no beam- thermal energy. house; through-the-blue; and shear- (6)(i) Wastes which fail the test for ling. the characteristic of EP toxicity be- (E) Wastewater treatment sludges cause chromium is present or are generated by the following subcategor- listed in Subpart D due to the pres- ies of the leather tanning and finish- ence of chromium, which do not fail ing industry: Hair pulp/chrome tan/ the test for the characteristic of EP retan/wet finish; hair save/chrome toxicity for any other constituent or tan/retan/wet finish; retan/wet are not listed due to the presence of finish; no beamhouse; through-the- any other constituent, and which do blue; and shearling. not fail the text for any other charac- (F) Wastewater treatment sludes teristic, if it is shown by a waste gener- generated by the following subcategor- ator or by waste generators that: ies of the leather tanning and finish- (A) The chromium in the waste is ing industry: Hair pulp/chrome tan/ exclusively tor nearly exclusively) tri- retan/wet finish; hair save/chrome- valent chromium; and tan/retan/wet finish; and through- (B)The waste is generated from an the-Wue. industrial process which uses trivalent (GI Waste scrap leather from the chromium exlcusively tor nearly exclu- leather tanning industry, the shoe sively) and the process does not gener- manufacturing industry, and other ate hexavalent chromium; and leather product manufacturing indus- (C) The waste is typically and fre- tries. quently managed in non-oxidizing en- (HI Wastewater treatment sludges vironments. from the production of TiO, pigment (ii) Specific wastes which meet the using chromium-bearing ores by the standard in paragraphs (b)(6)(i)(A), chloride process. (B)and (C)(so long as they do not fail (7) Solid waste from the extraction, the test for the charactristic of EP beneficiation and procesing of ores toxicity, and do not fail the test for and minerals (including coal), includ- any other characteristic) are: ing phosphate rock and overburden (A) Chrome (blue) trimmings gener- from the mining of uranium ore. For ated by the following subcategories of the purposes of this paragraph, solid the leather tanning and finishing in- waste from the processing of ores and dustry; hair pulp/chrome tanhetan/ minerals does not include: wet finish; hair save/chrome tan/ (i) Acid plant blowdown slurry/ retan/wet finish; retan/wet finish; no sludge resulting from the thickening beamhouse; through-the-blue; and of blowdown slurry from prirnsry shearling. copper production; (B)Chrome (blue) shavings generat- (ii) Surface impoundment solids con- ed by the following subcategories of tained in the dredged from surface im- the leather tanning and finishing in- poundments at primary lead smelting dustry: Hair pulp/chrome tan/retan/ facilities; wet finish; hair save/chrome tan/ (iii) Sludge from treatment of proc- retan/wet finish; retan/wet finish; no ess wastewater and/or acid plant blow- beamhouse; through-the-blue; and down from primary zinc production; shearling. (iv) Spent potliners from primary (C) Buffing dust generated by the aluminum reduction; following subcategories of the leather (v) Emission control dust or sludge taming and finishing industry; hair from ferrochromiumsilicon produc- pulp/chrome tan/retan/wet finish; tion; Environmental Protection Agency (vi) Emission control dust or sludge (vi) The sample is being stored tem- from ferrochromium production. porarily in the laboratory after testing (8) Cement kiln dust waste. for a specific purpose (for example, (9) Solid waste which consists of dis- until conclusion of a court case or en- carded wood or wood products which forcement action where further test- fails the test for the characteristic of ing of the sample may be necessary). EP toxicity and which is not a hazard- (2) In order to qualify for the ex- ous waste for any other reason if the emption in paragraphs (d)(l) (i) and waste is generated by persons who uti- (ii) of this section, a sample collector lize the arsenical-treated wood and shipping samples to a laboratory and a wood products for these materials' in- laboratory returning samples to a tended end use. sample collector must: (c) Hazardous wastes which are ex- (i) Comply with U.S. Department of empted from certain regulations. A Transportation (DOT), U.S. Postal hazardous waste which is generated in Service (USPS), or any other applica- a product or raw material storage ble shipping requirements; or tank, a product or raw material trans- (ii) Comply with the following re- port vehicle or vessel, a product or raw quirements if the sample collector de- material pipeline, or in a manufactur- termines that DOT, USPS, or other ing process unit or an associated non- shipping requirements do not apply to waste-treatment-manufacturing unit, the shipment of the sample: is not subject to regulation under (A) Assure that the following infor- Parts 262 through 265, 268, 270, 271 mation accompanies the sample: and 124 of this chapter or to the noti- (1) The sample collector's name, fication requirements of section 3010 mailing address, and telephone of RCRA until it exits the unit in number; which it was generated, unless the (2) The laboratory's name, mailing unit is a surface impoundment, or address, and telephone number; unless the hazardous waste remains in (3) The quantity of the sample; the unit more than 90 days after the (4)The date of shipment; and unit ceases to be operated for manu- (5) A description of the sample. facturing, or for storage or transporta- (B)Package the sample so that it tion of product or raw materials. does not leak, spill, or vaporize from (dl Samples. (1) Except as provided its packaging. in paragraph (d)(2) of this section, a (3) This exemption does not apply if sample of solid waste or a sample of the laboratory determines that the water, soil, or air, which is collected waste is hazardous but the laboratory for the sole purpose of testing to de- is no longer meeting any of the condi- termine its characteristics or composi- tions stated in paragraph (d)(l)of this tion, is not subject to any require- section. ments of this part or Parts 262 (el Treatability Study Samples. (1) through 268 or Part 270 or Part 124 of Except as provided in paragraph (e)(2) this chapter or to the notification re- of this section, persons who generate quirements of section 3010 of RCRA, or collect samples for the purpose of when: conducting treatability studies as de- (i) The sample is being transported fined in section 260.10, are not subject to a laboratory for the purpose of test- to any requirement of Parts 261 ing; or through 263 of this chapter or to the (ii) The sample is being transported notification requirements of Section back to the sample collector after test- 3010 of RCRA, nor are such samples ing; or included in the quantity determina- (iii) The sample is being stored by tions of 8 261.5 and 8 262.34(d) when: the sample collector before transport (i) The sample is being collected and to a laboratory for testing; or prepqed for transportation by the (iv) The sample is being stored in a generator or sample collector; or laboratory before testing; or (ti) The sample is being accumulated tv) The sample is being stored in a or stored by the generator or sample laboratory after testing but before it is collector prior to transportation to a returned to the sample collector; or laboratory or testing facility; or 40 CFR Ch. 1 (7-1-89 Edition) (iii) The sample is being transported a period ending 3 years after comple- to the laboratory or testing facility for tion of the treatability study: the purpose of conducting a treatabil- (A) Copies of the shipping docu- ity study. ments; (2) The exemption in paragraph (B)A copy of the contract with the te)(l) of this section is applicable to facility conducting the treatability samples of hazardous waste being col- study; lected and shipped for the purpose of (C) Documentation showing: conducting treatability studies provid- (1) The amount of waste shipped ed that: under this exemption; (i) The generator or sample collector (2) The name, address, and EPA uses (in "treatability studies") no more identification number of the laborato- than 1000 kg of any non-acute hazard- ry or testing facility that received the ous waste, 1 kg of acute hazardous waste; waste, or 250 kg of soils, water, or (3) The date the shipment was made; debris contaminated with acute haz- and ardous waste for each process being (4) Whether or not unused samples evaluated for each generated waste and residues were returned to the gen- stream; and erator. (ii) The mass of each sample ship- tvi) The generator reports the infor- ment does not exceed 1000 kg of non- mation required under paragraph acute hazardous waste, 1 kg of acute te)tv)(C) of this section in its biennial hazardous waste, or 250 kg of soils, report. water, or debris contaminated with (3) The Regional Administrator, or acute hazardous waste; and State Director (if located in an author- (iii) The sample must be packaged so ized State), may grant requests, on a that it will not leak, spill, or vaporize case-by-case basis, for quantity limits from its packaging during shipment in excess of those specified in para- and the requirements of paragraph A graph te)(Z)(i)of this section, for up to or B of this subparagraph are met. an additional 500 kg of non-acute ha- (A) The transportation of each ardous waste, 1 kg of acute hazardous sample shipment complies with U.S. waste, and 250 kg of soils, water, or Department of Transportation (DOT), debris contaminated with acute haz- U.S. Postal Service (USPSI, or any ardous waste, to conduct further treat- other applicable shipping require- ability study evaluation when: There ments; or has been an equipment or mechanical (B) If the DOT, USPS, or other failure during the conduct of a treat- shipping requirements do not apply to ability study; there b a need to verify the shipment of the sample, the fol- the results of a previously conducted lowing informatidn must accompany treatability study; there is a need to the sample: study and an8,lyze alternative tech- (1) The name, mailing address, and niques within a previously evaluated telephone number of the originator of treatment process; or there is a need the sample; to do further evaluation of an ongoing (2) The name, address, and tele- treatability study to determine find phone number of the facility that will specifications for treatment. The addi- perform the treatability study; tional quantities allowed are subject to (3) The quantity of the sample; all the provisions in paragraphs (e)(l) (4)The date of shipment; and and (e)(2)(ii)(vi) of this section. The (5) A description of the sample, in- generator or sample collector must cluding its EPA Hazardous Waste apply to the Regional Administrator Number. in the Region where the sample is col- (iv) The sample is shipped to a labo- lected and provide in writing the fol- ratory or testing facility which is lowing information: exempt under 5 261.4(f) or has an ap- (i) The reason why the generator or propriate RCRA permit or interim sample collector requires additional status. quantity of sample for the treatability (v) The generator or sample collec- study evaluation and the additional tor maintains the following records for quantity needed; Environmental Protection Agency (ii) Documentation accounting for (2) The laboratory or testing facility all samples of hazardous waste from conducting the treatability study has the waste stream which have been an EPA identification number. sent for or undergone treatability (3) No more than a total of 250 kg of studies including the data each previ- "as received" hazardous waste is sub- ous sample from the waste stream was jected to initiation of treatment in all shipped, the quantity of each previous treatability studies in any single day. shipment, the laboratory or testing fa- "As received" waste refers to the waste cility to which it was shipped, what as received in the shipment from the treatability study processes were con- generator or sample collector. ducted on each sample shipped, and (4) The quantity of "as received" the available results of each treatabil- hazardous waste stored at the facility ity study; for the purpose of evaluation in treat- (iii) A description of the technical ability studies does not exceed 1000 kg, modifications or change in specifica- the total of which can include 500 kg tions which will be evaluated and the of soils, water, or debris contaminated expected results; with acute hazardous waste or 1 kg of acute hazardous waste. This quantity (iv) If such further study is being re- limitation does not include: quired due to equipment or mechani- (i) Treatability study residues; and cal failure, the applicant must include (ii) Treatment materials t including inlormation regarding the reason for nonhazardous solid waste) added to the failure or breakdown and also in- "as received" hazardous waste. clude what procedures or equipment (5) No more than 90 days have improvements have been made to pro- elapsed since the treatability study for tect against further breakdowns; and thesample was completed, or no more tv) Such other information that the than one year has elapsed since the Regional Administrator considers nec- generator or sample collector shipped essary. the sample to the laboratory or testing (f) Samples Undergoing Treatability facility, whichever date first occurs. Studies at Laboratories and Testing (6) The treatability study does not Facilities. Samples undergoing treat- involve the placement of hazardous ability studies and the laboratory or waste on the land or open burning of testing facility conducting such treat- hazardous waste. ability studies (to the extent such fa- (7) The facility maintains records cilities are not otherwise subject to for 3 years following completion of RCRA requirements) are not subject each study that show compliance with to any requirement of this Part, Part the treatment rate limits and the stor- 124, Parts 262-266, 268, and 270, or to age time and quantity limits. The fol- the notification requirements of Sec- lowing specific information must be in- tion 3010 of RCRA provided that the cluded for each treatability study con- conditions of paragraphs (f) (1) ducted: through (11) of this section are met. A ti) The name, address, and EPA mobile treatment unit (MTU) may identification number of the generator qualify as a testing facility subject to or sample collector of each waste paragraphs (f) (1) through (11) of this sample; section. Where a group of MTUs are (ii) The date the shipment was re- located at the same site, the limita- ceived; tions specified in (f) (1) through (11) (iii) The quantity of waste accepted; of this section apply to the entire (iv) The quantity of "as received" group of MTUs collectively as if the waste in storage each day; group were one MTU. tv) The date the treatment study (1) No less than 45 days before con- was initiated and the amount of "as ducting treatability studies, the f acili- received" waste introduced to treat- ty notifies the Regional Administra- ment each day; tor, or State Director (if located in an tvi) The date the treatability study authorized State), in writing that it in- was concluded; tends to conduct treatability studies tvii) The date any .mused sample or under this paragraph. residues generated from the treatabil- 40 CFR Ch. 1 (7-1-89 Edition)

ity study were returned to the genera- [45 FR 33119. May 19.19801 tor or sample collector or, if sent to a EDITORIALNOTE: For FEDERALREGISTER ci- designated facility, the name of the fa- tations affecting 5 261.4, see the List of CFR cility and the EPA identification Sections Affected in the Finding Aids sec- number. tion of this volume. (8) The facility keeps, on-site, a copy of the treatability study contract and 9 261.5 Special requirements for hazard- all shipping papers associated with the ous waste generated by conditionally transport of treatability study samples exempt small quantity generators. to and from the facility for a period (a) A generator is a conditionally ending 3 years from the completion exempt small quantity generator in a date of each treatability study. calendar month if he generates no (9) The facility prepares and submits more than 100 kilograms of hazardous a report to the Regional Administra- waste in that month. tor, or State Director (if located in an (b) Except for those wastes identi- authorized State), by March 15 of fied in paragraphs (el, (f), (g), and (j) each year that estimates the number of this section, a conditionally exempt of studies and the amount of waste ex- small quantity generator's hazardous pected to be used in treatability stud- wastes are not subject to regulation ies during the current year, and in- under Parts 262 through 266, 268, and cludes the following information for Parts 270 and 124 of this chapter, and the previous calendar year: the notification requirements of sec- (i) The name, address, and EPA tion 3010 of RCRA, provided the gen- identification number of the facility erator complies with the requirements conducting the treatability studies; of pgagraphs (f), (g), and (j) of this (ii) The types (by process) of treat- section. ability studies conducted; tc) Hazardous waste that is not sub- (iii) The names and addresses of per- ject to regulation or that is subject sons for whom studies have been con- only to Q 262.11, $262.12, 5 262.4Otc1, ducted (including their EPA identifica- and Q 262.41 is not included in the tion numbers); quantity determinations of this part (iv) The total quantity of waste in and Parts 262 through 266, 268, and storage each day; 270 and is not subject to any of the re- tv) The quantity and types of waste quirements of those parts. Hazardous subjected to treatability studies; waste that is subject to the require- tvi) When each treatability study ments of # 261.6 (b) and (c) and Sub-' was conducted; parts C, D, and F of Part 266 is includ- t vii) The final disposition of residues ed in the quantity determination of and unused sample from each treat- this part and is subject to the require- hbility study. ments of Parts 262 through 266 and (10 The facility determines whether 270. any unused sample or residues gener- (dl In determining the quantity of ated by the treatability study are haz- hazardous waste generated, a genera- ardous waste under 8 261.3 and, if so, tor need not include: are subject to Parts 261 through 268, (1) Hazardous waste when it is re- and Part 270 of this Chapter, unless moved from on-site storage; or the residues and unused samples are (2) Hazardous waste produced by on- returned to the sample originator site treatment (including reclamation) under the 3 261.4te) exemption. of his hazardous waste, so long as the ( 11 The facility notifies the Region- hazardous waste that is treated was al Administrator, or State Director (if counted once; or located in an authorized State), by (3) Spent materials that are generat- letter when the facility is no longer ed, reclaimed, and subsequently reused planning to conduct any treatability on-site, so long as such spent materials studies at the site. have been counted once. (Approved by the Office of Management (el If a generator generates acute and Budget under control number 2050- hazardous waste in a calendar month 0088) in quantities greater than set forth Environmental Protection Agency below. all quantities of that acute haz- (iv) Permitted, licensed, or registered ardous waste are subject to full regula- by a State to manage municipal or in- tion under Parts 262 through 266, 268, dustrial solid waste; or and Parts 270 and 124 of this chapter, tv) A facility which: and the notification requirements of (A) Beneficially uses or reuses, or le- section 3010 of RCRA: gitimately recycles or reclaims its (1) A total of one kilogram of acute waste; or hazardous wastes listed in $8 261.31, (B)Treats its waste prior to benefi- 261.32, or 261.33te). cial use or reuse, or legitimate recy- (2) A total of 100 kilograms of any cling or reclamation. residue or contaminated soil, waste, or other debris resulting from the clean- (g) In order for hazardous waste gen- up of a spill, into or on any land or erated by a conditionally exempt small water, of any acute hazardous wastes quantity generator in quantities of less listed in $5 261.31, 261.32, or 261.33te). than 100 kilograms of hazardous waste [Comment: "Full regulation" means those during a calendar month to be ex- regulations applicable to generators of cluded from full regulation under this greater than 1,000 kg of non-acutely hazard- section, the generator must comply ous waste in a calendar month.] with the following requirements: (f) In order for acute hazardous (1)Section 262.11 of this chapter; wastes generated by a generator of (2 The conditionally exempt small acute hazardous wastes in quantities quantity generator may accumulate equal to or less than those set forth in hazardous waste on-site. If he accumu- paragraph (e)(l) or (2) of this section lates at any time more than a total of to be excluded from fu 1 regulation 1000 kilograms of his hazardous under this section, the generator must wastes, all of those accumulated comply with the fctllowing require- wastes are subject to regulation under ments: the special provisions of Part 262 ap- (1)Section 262.1 1 of this chapter; plicable to generators of between 100 (2) The generator may accumulate kg and 1000 kg of hazardous waste in a acute hazardous waste on-site. If he calendar month as well as the require- accumulates at any time acute hazard- ments of Parts 263 through 266, 268, ous wastes in quantities greater than and Parts 270 and 124 of this chapter, those set forth in paragraph (e)(l) or and the applicable notification re- (eI(2) of this section, all of those accu- quirements of section 3010 of RCRA. mulated wastes are subject to regula- The time period of 8 262.34(d) for ac- tion under Parts 262 through 266, 268, cumulation of wastes on-site begins for and Parts 270 and 124 of this chapter, a conditionally exempt small quantity and the applicable notification re- generator when the accumulated quirements of section 3010 of RCRA. wastes exceed 1000 kilograms; The time period of 5 262.34(a) of this chapter, for accumulation of wastes (3) A conditionally exempt small . on-site, begins when the accumulated quantity generator may either treat or wastes exceed the applicable exclusion dispose of his hazardous waste in an limit; on-site facility or ensure delivery to an (3) A conditionally exempt small off-site treatment, storage or disposal quantity generator may either treat or facility, either of which, if located in dispose of his acute hazardous wwte the U.S., is: in an on-site facility or ensure delivery (i) Permitted under Part 270 of this to an off-site treatment, storage or dis- chapter; posal facility, either of which, if locat- (ii) In interim status under Parts 270 ed in the U.S., is: and 265 of this chapter; (i) Permitted under Part 270 of this ( iii Authorized to manage hazard- chapter; ous waste by a State with a hazardous (ii) In interim status under Parts 270 waste management program approved and 265 of this chapter; under Part 271 of this chapter; (iii) Authorized to manage hazard- (iv) Permitted, licensed, or registered ous waste by a State with a hazardous by a State to manage municipal or in- waste management program approved dustrial solid waste; or under Part 271 of this chapter; tv) A facility which: 8 261.6 40 CFR Ch. 1 (7-1-89 Edition) (A) Beneficially uses or reuses, or le- under Subpart 0 of Part 264 or 265 of gitimately recycles or reclaims its this chapter (Subpart Dl; waste; or (iii) Used oil that exhibits one or (B)Treats its waste prior to benefi- more of the characteristics of hazard- cial use or reuse, or legitimate recy- ous waste and is burned for energy re- cling or reclamation. covery in boilers and industrial fur- (h) Hazardous waste subject to the naces that are not regulated under reduced requirements of this section Subpart 0 of Part 264 or 265 of this may be mixed with non-hazardous chapter (Subpart El; waste and remain subject to these re- (iv) Recyclable materials from which duced requirements even though the precious metals are reclaimed (Sub- resultant mixture exceeds the quanti- part F); ty limitations identified in this section, unless the mixture meets any of the tv) Spent lead-acid batteries that are characteristics of hazardous waste being reclaimed (Subpart GI, identified in Subpart C. (3) The following recyclable materi- (i) If any person mixes a solid waste als are not subject to regulation under with a hazardous waste that exceeds a Parts 262 through Parts 266 or Parts quantity exclusion level of this sec- 268, 270 or 124 of this chapter, and are tion, the mixture is subject to full reg- not subject to the notification require- ulation. ments of section 3010 of RCRA: (j) If a conditionally exempt small (i) Industrial ethyl alcohol that is re- quantity generator's wastes are mixed claimed except that, unless provided with used oil, the mixture is subject to otherwise in ap international agree- Subpart E of Part 266 of this chapter ment as specified in 4 262.58: if it is destined to be burned for (A) A person initiating a shipment energy recovery. Any material pro? for reclamation in a foreign country, duced from such a mixture by process- and any intermediary arranging for ing, blending, or other treatment is the shipment, must comply with the also so regulated if it is destined to be requirements applicable to a primary burned for energy recovery. exporter in 4 8 262.53, 262.56 ta)(l)-(41, (61, and (b), and 262.57, export such 151 Fa 10174, Mar. 24, 1986, as amended at 51 FR 28682. Aug. 8, 1986; 51 FR 40637, Nov. materials only upon consent of the re- 7, 1986; 53 FR 27163, July 19,19881 ceiving country and in conformance with the EPA Acknowledgment of 9 261.6 Requirements for recyclable mate- Consent as defined in Subpart E of rials. Part 262, and provide a copy of the (a)(1) Hazardous wastes that are re- EPA Acknowledgment of Consent to cycled are subject to the requirements the shipment to the transporter trans- for generators, transporters, and stor- porting the shipment for export; age facilities of paragraphs (b) and tc) (B) Transporters transporting a of this section, except for the materi- shipment for export may not accept a als listed in paragraphs ta)(2) and shipment if he knows the shipment ta)(3) of this section. Hazardous does not conform to the EPA Acknowl- wastes that are recycled will be known edgment of Consent, must ensure that as "recyclable materials." a copy of the EPA Acknowledgment of (2 The following recyclable materi- Consent accompanies the shipment als are not subject to the requirements and must ensure that it is delivered to of this section but are regulated under the facility designated by the person Subparts C through G of Part 266 of initiating the shipment. this chapter and all applicable provi- (ii) Used batteries tor used battery sions in Parts 270 and 124 of this chap- cells) returned to a battery manufac- ter: turer for regeneration; (i) Recyclable materials used in a (iii) Used oil that exhibits one or manner constituting disposal (Subpart more of the characteristics of hazard- C 1; ous waste but is recycled in some other (ii) Hazardous wastes burned for manner than being burned for energy energy recovery in boilers and indus- recovery; trial furnaces that are not regulated (iv) Scrap metal; Environmental protection Agency tv) Fuels produced from the refining tics of hazardous waste in Part 261, of oil-bearing hazardous wastes along Subpart C. with normal process streams at a pe- (b) Generators and transporters of troleum refining facility if such wastes recyclable materials are subject to the result from normal petroleum refin- applicable requirements of Parts 262 ing, production, and transportation and 263 of this chapter and the notifi- practices; cation requirements under section (vi) Oil reclaimed from hazardous 3010 of RCRA, except as provided in waste resulting from normal petrole- paragraph (a) of this section. um refining, production, and transpor- tc)(1) Owners or operators of facili- tation practices, which oil is to be re- ties that store recyclable materials fined along with normal process before they are recycled are regulated streams at a petroleum refining facili- under all applicable provisions of Sub- ty; parts A through L of Parts 264 and (yii) Coke and coal tar from the iron 265, and under Parts 124, 266, 268, and and steel industry that contains EPA 270 of this Chapter and the notifica- Hazardous Waste No. KO87 (Decanter tank tar sludge from coking oper- tion requirements under section 3010 ations) from the iron and steel produc- of RCRA, except as provided in para- tion process; graph (a) of this section. (The recy- tviii)(A) Hazardous waste fuel pro- cling process itself is exempt from reg- duced from oil-bearing hazardous ulation.) wastes from petroleum refining, pro- (2) Owners or operators of facilities duction, or transportation practices, or that recycle recyclable materials with- produced from oil reclaimed from such out storing them before they are rcy- hazardous wastes, where such hazard- cled are subject to the following re- ous wastes are reintroduced into a quirements, except as provided in process that does not use distillation paragraph (a) of this section: or does not produce products from (i) Notification requirements under crude oil so long as the resulting fuel section 3010 of RCRA; meets the used oil specification under (ii) Sections 265.71 and 265.72 (deal- 5 266.40te) of this chapter and so long ing with the use of the manifest and as no other hazardous wastes are used manifest discrepancies) of this chap- to produce the hazardous waste fuel; ter. (B)Hazardous waste fuel produced from oil-bearing hazardous waste from C50 FR 49203, Nov. 29, 1985, as amended at 51 FR 28682, Aug. 8. 1986; 51 FR 40637, Nov. petroleum refining production, and FR transportation practices, where such 7, 1986; 52 11821, Apr. 13, 19871 hazardous wastes are reintroduced 0 261.7 Residues of hazardous waste in into a refining process after a point at empty containers. which contaminants are removed, so long as the fuel meets the used oil fuel t a)(1) Any hazardous waste remain- specification under 5 266.40te) of this ing in either (i) an empty container or chapter; and (ii) an inner liner removed from an (C) Oil reclaimed from oil-bearing empty container, as defined in para- hazardous wastes from petroleum re- graph (b) of this section, is not subject fining, production, and transportation to regulation under Parts 261 through practices, which reclaimed oil is 265, or Part 268, 270 or 124 of this burned as a fuel without reintroduc- chapter or to the notification require- tion to a refining process, so long as ments of section 3010 of RCRA. the reclaimed oil meets the used oil (2) Any hazardous waste in either (i) fuel sp~cificationunder 5 266.40te) of a container that is not empty or (ii) an this chacier; and inner liner removed from a container (ix) Petroleum coke produced from that is not empty, as defined in para- petroleum refinery hazardous wastes graph (b) of this section, is subject to containing oil at the same facility at regulation under Parts 261 through which such wastes were generated, 265, and Parts 268, 270 and 124 of this unless the resulting coke product ex- chapter and to the notification re- ceeds one or more of the characteris- quirements of section 3010 of RCRA. 40 CFR CR. 1 (7-1-89 Edition)

(b)(l)A container or an inner liner Subpart B-Criteria for Identifying removed from a container that has the Characteristics of Hazardous held any hazardous waste, except a Waste and for Listing Hazardous waste that is a compressed gas or that Waste is identified as an acute hazardous waste listed in 99 261.31, 261.32, or ff 261.10 Criteria for identifying the char- 261.33te) of this chapter is empty if: acteristics of hazardous waste. (i) All wastes have been removed t a) The Administrator shall identify that can be removed using the prac- and define a characteristic of hazard- tices commonly employed to remove ous waste in Subpart C only upon de- materials from that type of container, termining that: e,g., pouring, pumping, and aspirating, (1) A solid waste that exhibits the and characteristic may: (ii) No more than 2.5 centimeters (i) Cause, or significantly contribute (one inch) of residue remain on the to, an increase in mortality or an in- bottom of the container or inner liner, crease in serious irreversible, or inca- or pacitating reversible, illness; or (iii)(A) No more than 3 percent by (ii) Pose a substantial present or po- weight of the total capacity of the tential hazard to human health or the container remains in the container or environment when it is improperly inner liner if the container is less than treated, stored, transported, disposed or equal to 110 gallons in size, or of or otherwise managed; and (B) No more than 0.3 percent by (2 The characteristic can be: weight of the total capacity of the (i) Measured by an available stand- ardized test method which is reason- container remains in the container or ably within the capability of genera- inner liner if the container is greater tors of solid waste or private sector than 110 gallons in size. laboratories that are available to serve (2) A container that has held a haz- generators of solid waste; or ardous waste that is a compressed gas ( ii Reasonably detected by genera- is empty when the pressure in the con- tors of solid waste through their tainer approaches atmospheric. knowledge of their waste. (3) A container or an inner liner re- moved from a container that has held ff 261.11 Criteria for listing hazardous an acute hazardous waste listed in waste. 261.31, 261.32, or 261.33te) is empty (a) The Administrator shall list a if: solid waste as a hazardous waste only (i) The container or inner liner has upon determining that the solid waste been triple rinsed using a solvent capa- meets one of the following criteria: ble of removing the commercial chemi- (1) It exhibits any of the character- cal product or manufacturing chemi- istics of hazardous waste identified in cal intermediate; Subpart C. (ii) The container or inner liner has (2) It has been found to be fatal to been cleaned by another method that humans in low doses or, in the absence has been shown in the scientific litera- of data on human toxicity, it has been ture, or by tests conducted by the gen- shown in studies to have an oral LD 50 erator, to achieve equivalent removal; toxicity (rat) of less than 50 milli- or grams per kilogram, an inhalation LC (iii) In the case of a container, the 50 toxicity (rat) of less than 2 milli- inner liner that prevented contact of grams per liter, or a dermal LD 50 tox- icity (rabbit) of less than 200 milli- the commercial chemical product or grams per kilogram or is otherwise ca- manufacturing chemical intermediate pable of causing or significantly con- with the container, has been removed. tributing to an increase in serious be- 145 FR 78529, Nov. 25, 1980, as amended at versible, or incapacitating reversible, 47 FR 36097, Aug. 18. 1982; 48 FR 14294, illness. (Waste listed in accordance Apr. 1, 1983; 50 FFt 1999, Jan. 14, 1985; 61 with these criteria will be designated FR 40637, Nov. 7.19861 Acute Hazardous Waste.) Enviranmentol Protection Agency (3) It contains any of the toxic con- tb) The Administrator may list class- stituents listed in Appendix VIII es or types of solid waste as hazardous unless, after considering any of the waste if he has reason to believe that following factors, the Administrator individual wastes, within the class or concludes that the waste is not capa- type of waste, typically or frequently ble of posing a substantial present or are hazardous under the definition of potential hazard to human health or hazardous waste found in section the environment when improperly 1004(5)of the Act. treated, stored, transported or dis- tc) The Administrator will use the posed of, or otherwise managed: criteria for listing specified in this sec- (i) The nature of the toxicity pre- tion to establish the exclusion limits sented by the constituent. referred to in 8 261.5tc). (ii) The concentration of the constit- uent in the waste. Subpart C-Characteristics of (iii) The potential of the constituent or any toxic degradation product of Hazardous Waste the constituent to migrate from the Q 261.20 General. waste into the environment under the types of improper management consid- (a) A solid waste, as defined in ered in paragraph (a)t3)tvii) of this 0 261.2, which is not excluded from section. regulation as a hazardous waste under tiv) The persistence of the constitu- 8 261.4tb). is a hazardous waste if it ex- ent or any toxic degradation product hibits any of the characteristics identi- of the constituent. fied in this subpart. tv) The potential for the constituent [Comment: 6 262.11 of this chapter sets or any toxic degradation product of forth the generator's responsibility to deter- the constituent to degrade into non- mine whether his waste exhibits one or harmful constituents and the rate of more of the characteristics identified in this degradation. subpart I tvi) The degree to which the constit- (b) A hazardous waste which is iden- uent or any degradation product of tified by a characteristic in this sub- the constituent bioaccumulates in eco- part, but is not listed as a hazardous systems. waste in Subpart D, is assigned the tvii) The plausible types of improper EPA Hazardous Waste Number set management to which the waste could forth in the respective characteristic be subjected. in this subpart. This number must be tviii) The quantities of the waste used in complying with the notifica- generated at individual generation tion requirements of section 3010 of sites or on a regional or national basis. the Act and certain recordkeeping and tix) The nature and severity of the reporting requirements under Parts human health and environmental 262 through 265, 268, and Part 270 of damage that has occurred as a result this chapter. of the improper management of tc) For purposes of this subpart, the wastes containing the constituent. Administrator will consider a sample tx) Action taken by other govern- obtained using any of the applicable mental agencies or regulatory pro- sampling methods specified in Appen- grams based on the health or environ- dix I to be a representative sample mental hazard posed by the waste or within the meaning of Part 260 of this waste constituent. chapter. (xi) Such other factors as may be ap- propriate. [Comment: Since the Appendix I sampling methods are not being formally adopted by Substances will be listed on Appendix the Administrator, a person who desires to VIII only if they have been shown in employ an alternative sampling method is scientific studies to have toxic, carci- not required to demonstrate the equivalency nogenic, mutagenic or tera qgenic ef- of his method under the procedures set fects on humans or other life forms. forth in 0%260.20 and 260.21.1 (Wastes listed in accordance with C45 FR 33119. May 19. 1980, as amended at these criteria will be designated Toxic 48 FR 14294, Apr. 1, 1983; 51 FR 40636, Nov. wastes. 7.10861 40 CFR Ch. 1 (7-1-89 Edition)

g 261.21 Characteristic of ignitability. Methods for the Evaluation of Solid (a) A solid waste exhibits the charac- Waste, Physical/Chemical Methods" teristic of ignitability if a representa- (incorporated by reference, see tive sample of the waste has any of 8 260.11). the following properties: (2) It is a liquid and corrodes steel (1) It is a liquid, other than an aque- (SAE 1020) at a rate greater than 6.35 ous solution containing less than 24 mm (0.250 inch) per year at a test tem- percent alcohol by volume and has perature of 55°C (130°F)as determined flash point less than 60°C (140°F), as by the test method specified in NACE determined by a Pensky-Martens (National Association of Corrosion En- Closed Cup Tester, using the test gineers) Standard TM-01-69 as stand- method specified in ASTM Standard ardized in "Test Methods for the Eval- D-93-79 or D-93-80 (incorporated by uation of Solid Waste, Physical/ reference, see 5 260.1 1). or a Setaflash Chemical Methods" (incorporated by Closed Cup Tester, using the test reference, see H 260.1 1) or an equiva- method specified in ASTM Standard lent test method approved by the Ad- D-3278-78 (incorporated by reference, ministrator under the procedures set see O 260.111, or as determined by an forth in SO 260.20 and 260.21. equivalent test method approved by (b) A solid waste that exhibits the the Administrator under procedures characteristic of corrosivity, but is not set forth in 5s 260.20 and 260.21. listed as a hazardous waste in Subpart (2) It is not a liquid and is capable, D, has the EPA Hazardous Waste under standard temperature and pres- Number of D002. sure, of causing fire through friction, 145 FR 33119, May 19, 1980, as amended at absorption of moisture or spontaneous 46 FR 35247. July 7, 19811 chemical changes and, when ignited, - burns so vigorously and persistently 5 261.23 Characteristic of reactivity. that it creates a hazard. (a) A solid waste exhibits the charac- (3) It is an ignitable compressed gas teristic of reactivity if a representative as defined in 49 CFR 173.300 and as sample of the waste has any of the fol- determined by the test methods de- lowing properties: scribed in that regulation or equiva- (1) It is normally unstable and read- lent test methods approved by the Ad- ily undergoes violent change without ministrator under BQ 260.20 and 260.21, detonating. (4) It is an oxidizer as defined in 49 (2) It reacts violently with water. CFR 173.151. (3) It forms potentially explosive (b) A solid waste that exhibits the mixtures with water. characteristic of ignitability, but is not (4) When mixed with water, it gener- listed as a hazardous waste in Subpart ates toxic gases, vapors or fumes in a D, has the EPA Hazardous Waste quantity sufficient to present a danger Number of D001. to human health or the environment. C45 FR 33119, May 19, 1980, as amended at (5) It is a cyanide or sulfide bearing 46 FR 35247, July 7, 19811 waste which, when exposed to pH con- ditions between 2 and 12.5, can gener- 9 261.22 Characteristic of corrosivity. ate toxic gases, vapors or fumes in a (a) A solid waste exhibits the charac- quantity sufficient to present a danger teristic of corrosivity if a representa- to human health or the environment. tive sample of the waste has either of (6) It is capable of detonation or ex- the following properties: plosive reaction if it is subjected to a (1) It is aqueous and has a pH less strong initiating source or if heated than or equal to 2 or greater than or under confinement. equal to 12.5, as determined by a pH (7) It is readily capable of detona- meter using either an EPA test tion or explosive decomposition or re- method or an equivalent test method action at standard temperature and approved by the Administrator under pressure. the procedures set forth in Qg 260.20 (8) It is a forbidden explosive as de- and 260.21. The EPA test method for fined in 49 CFR 173.51, or a Class A pH is specified as Method 5.2 in "Test explosive as defined in 49 CFR 173.53 Environmental Protection Agency f) 261.30

or a Class B explosive as defined in 49 TABLEI-MAXIMUM CONCENTRATIONOF CON- CF'R 173.88. TAMINANTS FOR CHARACTERISTICOF EP (b) A solid waste that exhibits the TOXI~~TY-Continued characteristic of reactivity, but is not listed as a hazardous waste in Subpart EPA Maximum D, has the EPA Hazardous Waste hazardous Concentra. waste Contaminant tion Number of D003. number (mill ams perCer) ff 261.24 Characteristic of EP toxicity. DO16 ...... 2,4-D, (2,4-D'ichl~ophem~ya~8- 10.0 (a)A solid waste exhibits the charac- tic acid). teristic of EP toxicity if, using the test DO1 7 ...... 2,4,5-TP Silvex (2,4,5-Trichlo- 1.O methods described in Appendix 11 or rophenowypropionic acid). equivalent methods approved by the Administrator under the procedures set forth in 56 260.20 and 260.21, the Subpart D-Lists of Hazardous extract from a representative sample Wastes of the waste contains any of the con- taminants listed in Table I at a con- 9 261.30 General. centration equal to or greater than the (a) A solid waste is a hazardous respective value given in that Table. waste if it is listed in this subpart, Where the waste contains less than 0.5 unless it has been excluded from this percent filterable solids, the waste list under 80 260.20 and 260.22. itself, after filtering, is considered to (b) The Adrriinistrator will indicate be the extract for the purposes of this his basis for listing the classes or types section. of wastes listed in this Subpart by em- (b) A solid waste that exhibits the ploying one or more of the following characteristic of EP toxicity, but is not Hazard Codes: listed as a hazardous waste in Subpart D, has the EPA Hazardous Waste lgnible Waste ...... (1) Number specified in Table I which cor- Conos.ive Waste ...... (C) Reactive Waste ...... (R) responds to the toxic contaminant EP Toxic Waste ...... (El causing it to be hazardous. WeHazardous Waste ...... (HI Toxic Waste...... 0 TABLEI-MAXIMUM CONCENTRATIONOF CON- TAMINANTS FOR CHARACTERISTICOF EP Appendix VII identifies the constitu- TOXICITY ent which caused the Administrator to list the waste as an EP Toxic Waste EPA Mucimum (El or Toxic Waste (TI in 00 261.31 hazardous COIIcIMtra- and 261.32. waste Contaminant number (miIFmePer tc) Each hazardous waste listed in this subpart L assigned an EPA Haz- ardous Waste Number which precedes 0004 ...... Arsenic ...... 5.0 0005 ...... Barium ...... 100.0 the name of the waste. This number 0006 ...... Cadmium ...... 1.O must be used in complying with the DO07 ...... Chromium ...... 5.0 notification requirements of Section 0008 ...... Lead ...... 5.0 MXlQ ...... Mercury ...... 0.2 3010 of the Act and certain record- 0010 ...... Selenium ...... 1.O keeping and reporting requirements 001 1 ...... Siber ...... 5.0 under Parts 262 through 265, 268, and 0012 ...... Endrin (1,2,3,4,10,10-hexach. 0.02 Part 270 of this chapter. bro- 1,7spoxy- 1.4,4r.5,6.7,8,8eoctrhydro. (dl The following hazardous wastes 1,4-endo, mdo-5,0-dimeth- listed in 8 261.31 or 8 261.32 are subject amnaphthalene. to the exclusion limits for acutely hae- DO13 ...... Lindnne (1,2,3,4,5,6hexa- chlor- 0.4 ocydohexone, gamma isomer. ardous wastes established in 0 261.5: 0014 ...... MethoxycMor (1,l,l-TlichkrO. 10.0 EPA H-dous Wastes Nos. FO20, 2.2-bh CpmSrt\ox~- F021, F022, F023, F026, and F027. phenyllethane). 0015 ...... Toxsphe~(Ca&ll.cL, TOC-1 0.6 t45 FR 33119, May 19, 1080, 86 amended at chkrkuted -. 6749 48 FFt 14294, Apr. 1, 1083; 50 PR 2000, Jan. pmml chkrine). 14,1985; 51 FR 40636, Nov. 7,10861 40 CFW Ch. 1 (7-1-89 Edition)

S 261.31 Hazardous wastes from non-specific sources. The following solid wastes are listed hazardous wastes from non-specific sources unless they are excluded under 85 260.20 snd 260.22 and listed in Appen- dix IX.

Industry and EPA hazardous Hazardous waste Hazard waste No. code

Generic: ~001...... I The following spent halogenated solvents us8d in degreasing: Tetrachloroethylene, I (T) 1 trichloroethylene, methylem chloride, 1.l ,I-trichlor&thane; carbon tetrachiwide, 1 and chlorinated fluorocarbons; all spent solvent mixtureslblends used in deareas- I ing containing, before use, a total of ten percent or more (by volume) of & or more of the above halogenated solvents or those sohrents listed in F002, F004, and F005; and still bottoms from the rBCWeiy of lhese spent solvents and spent solvent mixtures. F002...... The following spent halogenated solvents: Tetrachlorwthylene, methylene chloride. trichloroethylene. 1.1 .I-trichloroethane, chlorobenzene, 1.l,2-trichloro-l,22-trifluor- 1 oethane, ortho-dichlorobenrene. nchlomflwomenn*. and 1.1.2-t1ich~U1ane; all spent solvent mixtures/blends containing, before use, a total of ten percent or more (by volume) of one or more of the ebove halogsnated solvents or those ,listed in FOO1, F004, or F005; and still bottwns from the recovery of these spent solvents and spent sdvent mixtures. m FOO~...... The following spent non-haloeenated solvents: Xylene, acetone, ethyl acetate, ethyl (I)' benzene, ethyl ether, methyl isobutyl ketone, n-butyl alcohol, cyclohexenone, and methanol: all spent solvent m@xes/blendre containing, before use. only the above spent non-halogenated solvents; and all spent solvent mixtures/blends containing, before use, one or more of the above non-halogenated solvents, and, a total of ten percent or more (by volume) of one %more of VIOse solvents listed in F001. F002, F004, and FW5; and still bottoms from the rmwyof these spent solvents and spent solvent mixtures. F004 ...... The following spent non-halogenated sdvents: Clesols and cresyli acid, and (T) nitrobenzene; all spent mlvent mixtures/bhds containing, before use, a total of ten percent or more (by volume) of om or meof the above non-halogenated solvents or those solvents Lted in FOO1, FOO2, and F005; and still bottom from the recovery of these spent sdvents and spent sdvent mixtures. F005 ...... The following spent non-halogenated solvents: Toluene, methyl ethyl ketone. carban (I,T) disulfi, isobutanol, pyndine, benzene, 2sthoxyeVllmd, and 2-nitropropane; aH spent solvent mixtures/blends containing, before use, a total of ten percent or more (by volume) of one or more of the above nokhalogenated solvents or those solvents listed in FWl. F002, or F004; and still bottoms from the recovery d these spent solvents and spent &vent mixtures. F006 ...... Wastewater treatment sludges from ektrWting operations except from the (l) follomng processes: (1) Sulfwic acid Wingof aluminum; (2) tin plating on carbon steel; (3) zinc plating (sqrwted Us)on carbon steel; (4) aluminum or zinc-aluminum plating on carbon at&, (5) deening/stripping associated with tin, zinc and aluminum plating on carbon steel: and (6) chemical etching and mihg of aluminum. FOl9...... Wastewater treatment sludges from the chemhl cow- coating of aluminum...... (T) F007 ...... Spent cyanide plating bath solutions from @ktm@ating apecations ...... (R, T) F008 ...... Plating bath reaidues from the bQnom of plating bths from electroplating operations (R. T) where cyanides are used m the process. FOOB ...... Spent stripping and cleaning bath solutions from electroplating operations where (R, T) cyanides are used in the pmces. FO10 ...... Quenching bath residues from oil baths from metcrl heat treating operations where (R, T) cyanides are used in the pocea. F011...... Spent cyanide solutions hem ral bath pot ckming from metal heat treating (R, T) operations. F012...... Mng waste water treatment from metal heat treating operatiom where 0 cyanides are uesd in th@poems. F024 ...... Wastes, including but not limited to, dietillation r-s, heavy ends, tars, and (l) reactor clean-wt wastes from the producbion of chlorinated alikhydrocar- bons, having uubon amtent from one to h, utili free radical catatyzed processes. [This h8ting does not include #ght ends. spent filters and filter aids, went deMicants; wastewater, wortmuater treatment , apgnt cawy8t8, and waste8 listed in 4 261.32.1. F020...... Wrstes (except w~tewater.nd mtccubon from hydroOen cMorkle puihcation) (H) hthe production a fnmufamuse (a8 a faactant, chemical intermediate, or oomponent in a formulating pmeea) ol trC or tv,a of interm diatea used to pro$m thek psdidde deriverim. (This bthg does not include wastes from the prOductkn ol Hexach- from NOMy puified 2,4,5 ~lotophend.). Environmental Protection Agency

Industry and €PA hazardous Hazardous waste Hazard waste No. --- code F021 ...... Wastes (except wastewater and spent carbon from hydrogen chloride purification) (H) from the production or manulactur~nguse (as a reactant. chemical intermediate. or component in a formulallng process) of pentachlorophenol, or of intermediates used to produce its derivatwes. F022 ...... Wastes (except wastewater and spent carbon from hydrogen chloride purification) (H) from the manulacturing use (as a reactant, chemlcal intermediate, or component in a formulating process) of tetra-, Penta-, or hexachlorobenzenes under alkaline conditions. ~023...... Wastes (except wastewater and spent carbon from hydrogen chloride purificat~on) (H) from the production of materials on equipment previously used for the production or manufacturing use (as a reactant, chemical intermediate, or component in a formulating process) of tri- and tetrachlorophenols. (This listing does not include wastes from equipment used only for the production or use of Hexachlorophene from highly purified 2,4.5-trichlorophenol.). F026 ...... Wastes (except Wastewater and spent carbon from hydrogen chloride purification) (H) from the production of materials on equipment previously used for the manufactur- ing use (as a reactant, chemical intermediate, or component in a formulating process) of tetra-, penta-, or hexachlorobenzene under alkaline conditions. F027...... Discarded unused formulations containing tri-, tetra-, or pentachlorophenol or dis- (H) carded unused formulations containing compounds derived from these chlorophen- 01s. (This Ilsttng does not include formulations containing Hexachlorophene sythe- sized from prepurified 2,4.5-trichlorophenol as the sole component.). F028 ...... Residues resulting from the incineration or thermal treatment of soil contaminated (T) with €PA Hazardous Waste Nos. F020. F021. F022. F023. F026, and F027.

' '(1.T) should be used to speclty mixtures Containing ignitable and toxic constituents.

146 FR 4617. Jan. 16,19811 EDITORIALNOTE: For FEDERALREGISTER citations affecting 5 261.31, see the List of CFR Sections Affected in the Finding Aids section of this volume. @ 261.32 Hazardous wastes from specific sources. The following solid wastes are listed hazardous wastes from specific sogrces unless they are excluded under 00 260.20 and 260.22 and listed in Appendix IX.

Industry and EPA hazardous Hazardous waste Hazard waste No. code

Wood preservation: KO01 ...... Bottom sediment sludge from the treatment of wastewaters from wood preserving (T) processes that use creosote and/or pentachlorophenol. Inorganic pigments: KW2 ...... Wastewater treatment sludge from the production of chrome yellow and orange pigments. KW3 ...... Wastewater treatment sludge from the production of molybdate orange pcgments ...... (T) KW4 ...... Wastewater treatment sludge from the production of zinc yellow pigments...... m KW5 ...... Wastewater treatment sludge from the production of chrome green pigments ...... m KO06 ...... Wastewater treatment sludge from the production of chrome oxide green pigments (T) (anhydrous and hydrated). KW7 ...... Wastewater treatment sludge from the production of iron blue pigments ...... m KO08 ...... Oven residue from the production of chrome oxide green pigments...... m Organic chemicals: KW9 ...... Distillation bottoms from the production of acetaldehyde from ethylene ...... m KO10 ...... hstillation side cuts from the production of acetaldehyde from ethylene...... m KO1 1 ...... Bottom stream from the wastewater stripper in the production of acrylonitrile...... (R. f) KO13 ...... Bottom stream from the acetonitr~lecolumn in the production of acrylonitrile ...... (R, 1) KO14 ...... Bottoms from the acetonitrile purification column in the production of anylonitrile ...... KO15 ...... Still bottoms from the distillation of benzyl chloride ...... m KO16 ...... Heavy ends or distillation residues from the production of carbon tetrachloride...... m KO17 ...... Heavy ends (still bottoms) from the purification column in the production of epchlwohydrin. KO18 ...... Heavy ends from the fract~onationcolumn In ethyl chloride production...... (TI KO19 ...... Heavy ends from the distillalum of ethylene &chloride in ethylene dichloride production. KO20 ...... Heavy ends from the distillation of vinyl chloride in vinyl chloride monomer production. KO21 ...... Aqueous spent antimony catalyst waste from fluoromethanes production...... m KO22 ...... OIstillalion bottom tars from the production of phenollacetone from curnene ...... m KO23 ...... Ihstillation light ends from the production of phthalic anhydride from naphthalene ...... (l) 40 CFR Ch. 1 (7-1-89 Edition)

Industry and EPA hazardous klazud waste No. Hazardous waste coda ----I-- -- . KO24 ...... Disttllation bottoms from the productton of phthalic anhydride from naphthalene ...... m KO93 ...... Chstillatlon light ends from the productton of phthalic anhydride from oriho-xylene ...... (T) KO94 ...... Rstillation bottoms from the product~onof phthalic anhydride from ortho-xylem ...... m KO25 ...... Distillatton bonoms from the productton of nitrobenzene by the nitration of benzene ..... (T) KO26 ...... Stripping still tails from the production of methy ethyl pyridines ...... (T) KO27 ...... Centrifuge and distillation residues from toluene diisocyanate production...... (R, f) KO28 ...... Spent catalyst from the hydrochlonnator reactor in the production of l,l,l-Mchlor- (T) oethane. KO29 ...... Waste from the product steam stripper in the productin of 1.1,l-trichloroethane ...... (T) KO95 ...... Distillation bottoms from the production of 1,l ,I-trichloroethane...... (T) KO96 ...... Heavy ends from the heavy ends column from the production of l,l,l-trichloroeth- ane. KO30 ...... Column bottoms or heavy ends from the combined production of trichloroethylene (T) and perchloroethylene. KO83 ...... Chstillat~onbottoms from aniline production ...... m K103 ...... Process residues from aniline extraction from the production of aniline ...... (T) K104 ...... Combined wastewater streams generated from nitrobenzene/aniline production ...... m KO85 ...... Distillatton or fractionation column bottoms from the production of chlorobenzenes...... (T) K105 ...... Separated aqueous stream from the reactor product washing step in the production (T) of chlorobenzenes. K111 ...... Product washwaters from the production of dinitrotoluene via nitration of toluene ...... (C.n K112 ...... Reaction by-product water from the drying column in the production of toluenedie- (T) mlne via hydrogenation of dinitrotoluene. K113 ...... Condensed ltqutd light endc from the purification of toluenediamine in the production (T) of toluenediamtne via hydrogenatton of dinitrotoluene. K114 ...... Vicinals from the purification of toluenediamine in the proddtion of toluenediamine Cr) via hydrogenatton of dnitrotoluene. K115 ...... Heavy ends from the purificatton of toluenediamine in the production of tolwndia- (T) mine via hydrogenation of din~trotoluene. K116 ...... Organtc condensate from the solvent recovery column in the production of toluene (T) dilsocyanate via phosgenation of toluenediamine. K117 ...... Wastewater from the reactor vent gas scwbber in the production of ethylene dibromide vla bromination of ethene. K118 ...... Spent adsorbent sollds from purlf~cattonof ethylene dibromide in the production of ethylene dibromide via bromination of ethene. K136 ...... Still bottoms from the purification of ethylene dibromide in the producti of ethylene (T) dibromide via bromtnatlon of ethene. Inorganic chemicals: KO71 ...... Brine purificat~onmuds from the mercury cell process in chlorine production, where (T) separately prepur~fiedbrlne is not used. KO73 ...... Chlorinated hydrocarbon waste from the purification step of the diaphragm cell (T) process using graphlte anodes In chlonne product~on. K106 ...... Wastewater treatment sludge from the mercury cell process in chlorine production...... (T) Pesticides: KO31 ...... By-product salts generated ~nthe production of MSMA and cecodylic acid ...... 0 KO32 ...... Wastewater treatment sludge from the production of chlordane...... (T) KO33 ...... Wastewater and scrub water from the chlorination of cyclopenbdiene in the Cr) production of chlordane. KO34 ...... Filter solids from the filtration of hexachlorocyclopenbdiene in the production of (T) chlordane. KO97 ...... Vacuum str~pper discharge from the chlordane chlorinator in the production of chlordane. KO35 ...... Wastewater treatment sludges generated in the production of creosote ...... m KO36 ...... Still bottoms from toluene reclamat~ondistillation in the production of disulfoton ...... (T) KO37 ...... Wastewater treatment sludges from the production of disulfoton ...... m KO38 ...... Wastewater trom the washing and strlpplng of phorate production...... (T) KO39 ...... Filter cake from the filtrat~onof diethylphosphorodith'oic acid in the product~mof (T) phorate. KO40 ...... Wastewater treatment sludge from the production of phorate ...... m KO41 ...... Wastewater treatment sludge from the production of toxaphene ...... m KO98 ...... Untreated process wastewater from the production of toxaphene ...... m KO42 ...... Heavy ends or dtstillation residues from the distillation of tetrachlorobenzene in the m production of 2.4.5-T. KO43 ...... 2.6-Dichlorophenol waste from the production of 2,4-D ...... (l) KO09 ...... Untreated wastewater from the production of 2,4-D ...... m K123 ...... Process wastewater (including wpernates, filtrates, and mshwaters) from tho (T) production of ethyleneblsc. -11ocarbarnicacid and its mlt. K124 ...... Reactor vent scrubber water from the production of ethyteriebisdthioc~micrcid (C, f) and its salts. K125 ...... Flitration, evaporation, and centrifugation sdids from the production of ethyle- (T) dithiiarbemic acid and its salts. Enrvimnmental Protection Agency 5 261.33

ld~~vyand EPA hazardous Hazardous waste Hazard waste No...... - .- ...... - --.-

~126...... Baghouse dust and floor sweepings In milling and packaging operations from the (T) production or formulation of ethylenebisdithiocarbamic acid and its salts. Ewplosnres: ~044...... Wastewater treatment sludges from the manufacturing and processing of explosives ... (A) ~045...... Spent carbon from the treatment ot wastewater containing explosives...... (R) KO46 ...... Wastewater treatment sludges from the manufacturing. formulation. and loading of (T) lead-based tnitiating compounds. KO47 ...... Pink/red water from TNT operabons ...... (R) Paoleurn refining: 16048 ...... Dissolved air flotation (DAF) float from the petroleum refining industry ...... (7) KO49 ...... Slop oil emulsion solids from the Petroleum refining industry...... (T) ~050...... Heat exchanger bundle cleaning sludge from the petroleum refining industry...... 0 ~051...... API separator sludge from the petroleum ref~ningindustry ...... ;...... (TI KO52 ...... Tank bottoms (leaded) from the petroleum refln~ngindustry ...... 0 kon and steel: KO61 ...... Emission control dust/sludge from the primary production of steel in electric furnaces. KO62 ...... Spent pickle liquor generated by steel finishing operations of facilities within the iron (C.T) and steel industry (SIC Codes 331 and 332). Ftirrmry copper: KO64 ...... Acid plant Mowdown slurry/sludge resulting from the thickening of blowdown duq (T) from primary copper production. Rimary lead: KO65 ...... Surface impoundment solids contained in and dredged from surface impoundments (T) at primary lead smelting facil~tres. Rimary zinc: KO66 ...... Sludge from treatment of process wastewater and/or acid plant blowdown from primary zinc productton. Mmary aluminum: KO88 ...... Spent potlners from primary aluminum reauction...... (T) Fenoalloys: KOBO ...... Emission control dust or sludge from ferrochromiumsilicon production ...... (T) KO01 ...... Emission control dust or sludge from terrochromium production ...... (T) Secondary lead: KO69 ...... Emission control dust/sludge from secondary lead smelting ...... (T) KlOO ...... Waste leaching solution from actd leaching of emlssion control dustlsluc&e from (T) secondary lead smelting. Veterinary pharmaceuticals: KO84 ...... Wastewater treatment sludges generated during the production of veterinary pharma- (l) ceuticals from arsenic or organo-arsenic compounds. KIOI ...... Distillation tar residues trom the distillation of aniline-based compounds in the (T) production of veterinary pharmaceuticals from arsenic or organo-arsenic com- pounds. K102 ...... Residue from the use of activated carbon for decolorization in the production of (T) veterinary pharmaceuticals from arsenic or organo-arsenic compounds. Ink formulation: KO86 Solvent washes and sludges, caustlc washes and sludges, or water washes and (T) sludges from cleaning tubs and equipment used in the formulation of ink from pgments, driers, soaps, and stabilizers containing chromium and lead. Coking: KO60 ...... Ammonia still lime sludge from coklng operations...... m K087 ...... Decanter tank tar sludge from coking operatons...... (T)

146 FR 461.8, Jan. 16. 19811 E~ITORIALNOTE: For FEDERALREGISTER citations affecting 9 261.32, see the List of CFR Gections Affected in the Finding Aids section of this volume.

Q 261.33 Discarde d commercial chemical the land for dust suppression or road products, off-specification species, con- treatment, when they are otherwfse tainer residues, and spill residues applied to the land in lieu of their thereof. original intended use or when they are The following materials or items are contained in products that are applied haawdous wastes if and when they are to the land in lieu of their original in- discarded or intended to be discarded tended use, or when, in lieu of their as described in $261.2(a)(2)(i), when original intended use, they are pro- they are mixed with waste oil or used duced for use as tor as a component oil or other material and applied to 40 CFR Ch. 1 (7-9-89 Edition) of a fuel, distributed for use as a fuel, debris resulting from the cleanup of a or burned as a fuel. spill, into or on any land or water, of (a) Any commercial chemical prod- any off-specification chemical product uct, or manufacturing chemical inter- and manufacturing chemical intenne- mediate having the generic name diate which, if it met specifications, listed in paragraph (el or (f) of this would have the generic name listed in section. paragraph (el or (f) of this section. (b) Any off-specification commercial [Comment: The phrase "commercial chemi- chemical product or manufacturing cal product or manufacturing chemical in- chemical intermediate which, if it met termediate having the generic name listed specifications, would have the generic in . . ." refers to a chemical substance name listed in paragraph (el or (f) of which is manufactured or formulated for commercial or manufacturing use which this section. consists of the commercially pure grade of tc) Any residue remaining in a con- the chemical, any technical grades of the tainer or in an inner liner removed chemical that are produced or marketed. from a container that has held any and all formulations in which the chemical commercial chemical product or man- is the sole active ingredient. It does not ufacturing chemical intermediate refer to a material, such as a manufacturing process waste, that contains any of the sub- having the generic name listed in stances listed in paragraph (el or (f). Where paragraph (el of this section, unless a manufacturing process waste is deemed to the container is empty as defined in be a hazardous waste because it contains a (5 261.7(b)(3)of the chapter. substance listed in paragraph (el or (f), such .[Comment: Unless the residue is being bene- waste will be listed in either H 261.31 or ficially used or reused, or legitimately recy- 5 261.32 or will be identified as a hazardous cled or reclaimed; or being accumulated. waste by the characteristics set forth in stored, transported or treated prior to such Subpart C of this part.) use, re-use, recycling or reclamation, EPA (el The commercial chemical prod- considers the residue to be intended for dis- ucts, manufacturing chemical interme- card, and thus, a hazardous waste. An exam- ple of a legitimate re-use of the residue diates or of f-specif ication commercial would be where the residue remains in the chemical products or manufacturing container and the container is used to hold chemical intermediates referred to in the same commercial chemical product or paragraphs (a) through (dl of this sec- manufacturing chemical intermediate it pre- tion, are identified as acute hazardous viously held. An example of the discard of wastes (HI and are subject to be the the residue would be where the drum is sent small quantity exclusion defined in to a drum reconditioner who reconditions 8 261.5te). the drum but discards the residue.] [Comment: For the convenience of the regu- (dl Any residue or contaminated soil, lated community the primary hazardous water or other debris resulting from properties of these materials have been indi- the cleanup of a spill into or on any cated by the letters T (Toxicity). and R (Re- land or water of any commercial activity). Absence of a letter indicates that chemical product or manufacturing the compound only is listed for acute toxici- chemical intermediate having the ge- ty.] neric name listed in paragraph (el or These wastes and their correspond- (f) of this section, or any residue or ing EPA Hazardous Waste Numbers contaminated soil, water or other are:

Haz- ardous Chemical waste abstracts No Subsfance No.

PO23 107-20-0 Acetaldehyde, chloro- PO02 591-08-2 Acetarmde. N-(aminothioxomethy0- PO57 640- 10-7 Acetemlde, 2-tluoro- PO58 62-74-8 Acet~cacid, fluoro-, sodium salt Po02 591-08-2 1-Acetyl.2-thiourea PO03 107-02-8 Acrole~n PO70 116-06-3 Aldlcarb Po04 309-00-2 Aldr~n Enviwnmentel Protection Agency

Haz- Chemical I Substance No. I I I 107-18-6 Allyl alcohol 20859-73-8 Aluminum phosphide (R,T) 2763-96-4 S(Arninomethyl)-3-i5oxazolol 504-24-5 4-Amlnopyndine 131-74-8 Ammonium picrale (R) 7803-55-6 Ammonlum vanadate 506-61-6 Argentate(1-), bis(cyano-C)-, potassium 7778-39-4 Arsenic acid H,AsO, 1327-53-3 Arsenic oxide As& 1303-28-2 Arsenic oxide A%Os 1303-28-2 Arsenlc pentoxide 1327-53-3 Arsen~ctnoxlde 69242-2 Arsine. dimthyl- 696-28-6 Arsonous d~chloride,phenyl- 151-56-4 Azirid~ne 75-55-8 Azirid~ne.2-methyl- 542-62-1 Barlum cyanide 106-47-8 Benzenamtne. 4-chloro- 100-01 -6 Benzenamine. 4-nitro- 100-44-7 Benzene. (chloromethy1)- 51-43-4 1.2-Benzenediol, 4-C 1-hydroxy.2-(rnethylarnino)ethyll-, (R)- 122-09-8 Benzeneethanamine, alpha,alpha-dimethyl- 108-98-5 Benzeneth~ol 1 81-81-2 2H-1-Benzopyran-2-one. 4-hydroxy-3-(3-oxo-lghenylbutyl)-,6 salts, when prewnt at ooncentrations greater than 0.3% 100-44-7 Benzyl chloride 7440-4 1-7 Beryllium 598-31 -2 Bromoacetone 357-57-3 Bruc~ne 39196-18-4 2-Butanone. 3,3-d~methyl-1-(methy1thio)-. 0-[methylam~no)carbonylloxlrne 592-01-8 Calcium cyanide 592-01 -8 Calcium cyanide Ca(CN)? 75-1 5-0 Carbon disulfide 75-44-5 Carbonic dichloride 107-20-0 Chloroacetaldehyde 106-47-8 p-Chloroaniline 5344-82-1 1-(0-Chlorophenyl)lhiourea 542-76-7 3-Chloroprop~onitrile 544-92-3 Copper cyanide 544-92-3 Copper cyanide Cu(CN) ...... Cyanides (soluble cyanide salts), not othenvise specified 460-19-5 Cyanogen 506-77-4 Cyanogen chloride 506-77-4 Cyanogen chloride (CN)CI 131-89-5 2-Cyclohexyl-4.6-dlnitrophenol 542-88-1 Dchloromethyl e!her 69628-6 Dchlorophenylarsine 60-57-1 Oeldrin 692-42-2 Diethylarsine 3 11-45-5 Dethyl-p-n~trophenylphosphate 297-97-2 0.0-D~ethyl0-pyrazinyl phosphorothiiate 55-91 -4 Disopropyltluorophosphate(DFP) 309-00-2 1,4.5.8-Dimethanonaphthalene,1.2.3,4,10,10-hexa- chloro-1,4.4a,5,8,8a,-hacahydro-, (lalpha.4alpha.4abeta.5alpha,8alphehe8abeta)- 465-73-6 1.4,5.8-D~methanonaphthalene,1.2.3,4.10,1 O-hexa- chloro-l,4.4a,5,8,8a-hexahydro-. (1alpha.4alpha.4abeta,5betata8beta,8ebeta)- 60-57-1 2.7:3,6-D1methanonaphth12.3-bloxirene.3.4.5,6.B,BhexrcMoro-la.2.2a,3.6,8a,7,7a9~tahydro-. (laalpha.2beta,2aalphaB3beta,6beU,6aa1pha,7beta7aalpha)- 72-20-8 2.7:3.6-Dmethanonaphth 12.3-bloxirene. 3.4.5.6.8.9-hexa~hlo~o.la,2,2e,3,6a,7, (laalpha.2~ta.2abeta,3alpha,6alpha,6abetete7beta,7aalpha)-, 6 metabolites PO44 60-51-5 Dtmethoate PO46 122-09-8 alpha,alpha-Omethylphenethylarnine Po47 534-52-1 4.6-Dinitrw-cresol. 8 salts PO48 51-28-5 2.4-D~nitrophenol Po20 88-85-7 hno~b Po85 152-16-9 &phosphoramide, octamethyl- Plll 107-49-3 Diphosphonc acid, tetraethyl ester Po39 298-04-4 hsulfoton 40 CFR Ch. 1 (7-1-89 Edition)

Haz- ardous ( Chemical Substance waste abstracts No. 1 No.

541-53-7 Dithiobluret 115-29-7 Endosultan 145-73-3 Endothall 72-20-8 Endrln 72-20-8 Endrin. 8 metabol~tes 51-43-4 Epinephrine 460-19-5 Ethanedinltrile 16752-77-5 Ethanimidothioic acid. N-[[(methylam~no)carbonylloxyl-,methyl ester 107-12-0 Ethyl cyanide 151-56-4 Ethyleneimlne 52-85-7 Famphur 7782-4 1-4 Fluorme 640-19-7 Fluoroacetamide 62-74-8 Fluoroacet~cacid, sdum salt 628-86-4 Fulmlnic acid, mercuty(2+) salt (R.1) 76-44-8 Heptachlor 757-58-4 Hexaethyl tetraphosphate 79-19-6 Hydrazinecarbothioamide 60-34-4 Hydrazine. methyl- 74-90-8 Hydrocyanic acid 74-90-8 Hydrogen cyanide 7803-51-2 Hydrogen phosphide 465-73-6 lsodrin 2763-96-4 3(2H)-lsoxazolone. 5-(aminomethyl)- 62-38-4 Mercury, (acetato-0)phenyl- 628-864 Mercury fulminate (R.T) 62-75-9 Methanamlne, N-methyl-N-nitroso- 624-83-9 Methane. isocyanato- 542-88-1 Methane, oxybis[chloro- 509-14-8 Methane, tetranitro- (A) 75-70-7 Methanethiol, trichloro- 115-29-7 6.9-Methano-2.43-benzodioxathiepin,6,7,8,9.10,10- hexachloro-1.5.5a,6,9,9a-hexahydro-,3-oxide 76-44-8 4.7-Methano-1H-indene. 1.4.5.6,7.8.8-heptachlwo- 3a.4.7.7a-tetrahydro- 16752-77-5 Methomyl 60-34-4 Methyl hydrazine 624-83-9 Methyl isocyanate 75-86-5 2-Methyllactonitrile 298-00-0 Methyl parathion 86-88-4 alpha-Naphthylth~ourea 13463-39-3 Nickel carbonyl 13463-39-3 Nickel carbonyl Ni(CO),. (T-4)- 557-1 9-7 Ntckel cyanide 557-19-7 N~ckelcynaide Ni(CN), 54-1 1-5 Ncotlne. 8 salts 10102-43-9 Nitric oxide 100-01 -6 p-Nitroaniline 10102-44-0 Nitrogen dloxide 10102-43-9 Ndrogen ox~deNO 1010244-0 Nitrogen oxide NO2 55-.63-0 Nltroglycerme (R) 62-75-9 N-Nitrosodimethylamine 4549-40-0 N-Nitrosomethylvinylamine 152-16-9 Octamethylpyrophosphoramide 20816-12-0 Osmium oxide OsO,, (T-4)- 208 16-1 2-0 Osmium tetroxide 145-73-3 7-0xabiqclo[2.2.1 lheptane-2.3dicarboxylic acid 56-38-2 Parathion 131-89-5 Phenol. 2-qclohexyl-4,6-dinitro- 51-28-5 Phenol, 2,4-dinitro- 1 534-52-1 Phenol. 2-methyl-4,6-dinitro-, 8 salts 88-85-7 Phenol. 2-(1-me1hylpropyl)-4,Winitro- 131-74-8 Phenol, 2.4,6-trinilro-. ammonium salt (R) 62-38-4 Phenylmercuty acetate 103-85-5 Phenyllhiourea 298-02-2 Phorate 7544-5 Phosgene 7803-51 -2 Phosphine Environmental Protection Agency -- Haz- udous Substance waste abstracts No. No. chemcal

U04 1 106-89-8 Epichlorohydr~n Uool 75-07-0 Ethanal (I) U174 55-18-5 Ethanamine. N-ethyl-N-nitro- U155 91-80-5 1.2-Elhanediam~ne,N.Ndimethyl-N'-2-pyridinyl-N'-(2-thienylmelt1yl)- U067 106-93-4 Ethane. 1.2-dibromo- U076 75-34-3 Ethane, 1.l -dichloro- U077 107-06-2 Ethane. 1.2-dichloro- U131 67-72-1 Ethane, hexachloro- W24 111-91-1 Ethane. 1,l '-[methylenebis(oxy)lbisC2thloro- U117 60-29-7 Ethane. 1.1 '-oxybis-(I) U025 1 11-44-4 Ethane, 1.l '-oxybisf2-chloro- U184 7641-7 Ethane. pentachloro- Urn8 630-20-6 Ethane, 1.l .l.2-tetrachloro- U209 79-34-5 Elhane. 1.1,2,2-tetrachloro- U218 62-55-5 Ethanethioamide U226 71-55-6 Ethane, 1.I .1 -trichloro- U227 79-00-5 Ethane, 1,1.2-trichloro- U359 1 10-80-5 Ethanol, 2-ethoxy- U173 1116-54-7 Ethanol, 2.2'-(nitrosoimino)bis- U004 -2 Elhanone. lphenyl- U043 75-01-4 Ethene, chloro- U042 110-75-8 Ethene, (2thloroethoxy)- U078 75-35-4 Ethene. 1.1 -diihloro- U079 15640-5 Ethene. 1,2dichloro-. (E)- U210 127-18-4 Ethene, tetrachloro- U228 79-01 -6 Ethene. trichloro- U112 141-78-6 Ethyl acetate (I) U113 140-88-5 Ethyl acrylate (I) U238 51-79-6 Ethyl arbamate (urethane) U117 60-29-7 Ethyl ether (I) U114 1 111-54-6 Ethylenebisdithwarbamic acid, salts 6 esters u067 106-93-4 Ethylene dibromide U077 107-06-2 Ethylene dichloride U359 110-80-5 Ethylene glycol monoethyl ether U115 75-21-8 Ethylene oxide (I,T) U116 9645-7 Ethylenethwea W76 75-34-3 Ethyliiene dichloride U118 97-63-2 Ethyl methacrylate Ull9 62-50-0 Ethyl methanesulfonate U120 206-44-0 Fluoranthene U122 50-00-0 Formaldehyde U123 64-18-6 Formic acid (C,T) U124 110-00-9 Furan (I) U125 98-01-1 2-Furancarboxaldehyde (I) U147 108-31-6 2.5-Furandione U213 109-99-9 Furan, tetrahydro-(I) U125 96-01-1 Furfural (I) U124 1 10-00-9 Furfuran (I) U206 18883-66-4 Glucopyranose. 2-deoxy-2-(3-methyl-3-nitr0%0~eido)-,D U206 18883-66-4 D-Glucose. 2-deoxy-24[(methylnitrosoamino)- arbonyllam~nol- 765-34-4 Glycldylaldehyde 70-25-7 Guanidine. N-methyl-N'-nitro-N-nitroso- 1 18-74-1 Hexachlorobenzene 87-68-3 Hexachlorobutadiene 77-47-4 Hexachlorocyclopentadiene 67-72-1 Hexachloroethane 70-30-4 Hexachlorophene 1888-7 1-7 Hexachloropropene 302-01 -2 Hydrazine (R.T) 1615-80-1 Hydrazine. 1.2dimthyl- 57-14-7 Hydrazimr, l,ld~methyl- 540-73-8 Hydrazine. 1.2-dimethyl- 122-66-7 Hydrazine, 1,24phenyl- 7664-39-3 Hydrofluoric acid (C.T) 7664-39-3 Hydrogen Ruoride (C.1) 7783-06-4 ~ogensulfii 7783-06-4 Hydrogen aiffide HIS 60-1 5-9 Hydroperoxide. 1-methyl- 1 -phenyhthyl- (R) 96-45-7 2-lmidazdithione 40 CFR Ch. 1 (7-1-89 MMm) - Haz- ardous _MI Substance -tracts No. 1 waste No.

193-39-5 lndenoCl.2.3-cdlpyrene 85-44-9 1,3-lsobenzofurandione 7843-1 lsobutyl alcohol (I,T) izo-58-1 Isosafrole 143-50-0 Kepone 303-34-4 Lasiocarpine 301-04-2 Lead acetate 1335-32-6 Lead, bis(acetat~)tetrahydroxVtri- 7446-27-7 Lead phosphate 133532-6 Lead subacetate 58-89-9 Lindane 70-25-7 MNNG 108-31-6 Maleic anhydride 123-33-1 Maleic hydrazide 109-77-3 Malononitrile 148-82-3 Melphalan 7439-97-6 Mercury 126-98-7 Methacrylonitrile (I, T) 124-40-3 Methanamine, N-methyl- (I) 74-83-9 Methane, biomo- 74-87-3 Methane. chloro- (1, T) 107-30-2 Methane, chloromethoxy- 74-95-3 Methane. diiromo- 75-09-2 Methane. diihloro- 75-71 -8 Methane, diihlorodifluoro- 74-88-4 Methane. iodo- 62-50-0 Methanesullonic acid, ethyl ester 56-23-5 Methane, tetrachloro- 74-93-1 Methanethd (I. T) 75-25-2 Methane. tribromo- 67-66-3 Methane. trichloro- 75-69-4 Methane, tnchlorofluoro- 57-74-9 4,7-Methano-1 H-indene. 1,2,4,5,6,7,8,8-0cta~hlor0.2,3,3a4,7,7~ 67-56-1 Methanol (I) 91-80-5 Methapyrilene 143-50-0 1,3.4-Metheno-2H-cyclobutaCcdlpentalen-2ne,1 ,1a,3,3a,4.5,5.5a5b1~o. 72-43-5 Methoxychlor 67-56-1 Methyl alcohol (I) 74-83-9 Methyl brotmde 504-60-9 1-Methylbutadiene (I) 74-87-3 Methyl chloride (1.T) 79-22-1 Methyl chlorocahnate (1.T) 71-55-6 Methyl chloroform 56-49-5 3-Methylcholanthrene 101-14-4 4,4'-Melhyl~s(2.chlw011niIine) 74-95-3 Methylene bromide 75-09-2 Methylene chloride 78-93-3 Methyl ethyl ketone (MEK) (1.T) 1338-23-4 Methyl ethyl ketone peroxida (R,T) 74-80-4 Methyl Mck 108-10-1 Methyl iw ketone (I) 80-626 Methyl methacrylate (I,T) 108-10-1 4-Methyl-2-p%ntanone(I) 56-04-2 Methylth'iwrecil 50-07-7 Mitomycin C 20830-81 -3 5,12-Nsphthacen6dione. &a~tyl-10-C(3-rmir)0-2,3,8~y).~~~)oyl- 7,8,9.l@Ietrahydra-6,8.11-trihydroxy-l-methoxy-, (BScb)- 134-32-7 1-Naphthahadm 81-59-8 2-Naphthalenrmim 494-03-1 NaphtJmlenamine. N,N'-bis(2cMoroothyl)- 81-20-3 Naphthalene 81-58-7 N@hVurlene. 2~hb0. 130-1 5-4 1,4-Naphth.lenedione 72-57-1 2.7-N@lVulengdisUn0nic a,3.3'-[(3,3'- dimethylC1.1'~14,4'~)bir(~o)bi8~~1-.Wmmdbm 8dt 130-1 5-4 1.4-N@lthOqunOne 134-32-7 alpha-Naphwmine 81-59-8 beta-Naphthylur#le 10102-45-1 NiUic add. molliurn(l+) ult 98-85-3 NibObe~n~0.T) EnvDronmental Pmt.ction Agency

Substance No. I I 1 U017 I 98-87-3 Benzene. (d~chloromethyl)- U223 26471-62-5 I Benzene. 1.3-diisocyanatomethyl- (R.T) 1330-20-7 Benzene. &methyl- (I,T) 108-46-3 1-3-Benzd~ol 1 18-74-1 Benzene. hexachloro- 110-82-7 Benzene. hexahydro- (I) 108-88-3 Benzene, methyl- 121-14-2 Benzene. 1-methyl-2.4diniWo- 606-20-2 Benzene. 2-methyl-1.3dinitro- 98-82-8 Benzene. (I-methylethyl). (I) 98-95-3 Benzene, nitro- 608-93-5 Benzene, pentachloro- 82-68-8 1 Benzene. pentachloronitro- Benzenewlfonic acid chloride (C,R) Benzmtfonyl chloride (C,R) Benzene. 1.2.4,5-tetrachloro- Benzene. 1.1 '-(2,2.2-trichlOro~thfl~)bie[4chl Benzene, 1.1'-(2.2.2-trichlOro~th~)bis[4-methow ~enzene;(trichl&omethyl)- - Benzene, 1,3,5-trinilro- Mine 1,2-hruisothiazol-3(2H)one, 1,l dioxide. 6 salts

' 1,9Benzodoxole, 5-prod- Benzo[rstlpentaphene 2H-l-Benzopyran-29ne, 4-hydroxy.3-(3oxel-phenyl-butyl)-,& &. when pr#6nt .t mw of 0.3% or less Benzo[alpyrene p-Benzoqu~none Benzobichlonde (C,R.T) 2,2'-Bioxirane [I,l'-B1phenyll-4,4'diamine [ 1.1'-Bil-4,4'diamine, 3.3'-dichlor@ t 1,I '-Biinyll-4.4'-diamine. 3,3'-dimethory- t I,l'-Biphenyil-4,4'diamine. 33-dimethyl- Bromofm 4-Bromophenyl phenyl ether 1.3-Butadiene, 1,1.2,3,4.4-hexachloro- I-Butanamine, N-butyl-N-nitow 1-Butend (I) 2-Butam (1,T) 2-Butanone, peroxide (R,T) 2-Butenal 2-Butene, 1-4-dichloro- (1.T) 2-Butenoic acid, 2-methyl-, 7-[[2,3dbhydroxy- 241-methoxvethvl)-3-methyl-1 ~~okrt~x~lmothyll-

.. . n-~utyialcohoi (i) ' ' Cacodyi~:acid I Calaum chromate I Wbarnic acid, ethyl ester Csrbemi aad, methylnitro!ie, ethyl eater Carbam~:chloride, dimethyl- wiacid, 1.2-etha~bis-, salts 6 esters CehmoM'i acid. Us(1-methylethyl)-, S(2.3dclWo-2- ertm Cafbowc acid, dithallium(1 +) salt Carbonicdmuonde Cattmochloridic acid, methyl ester (1.T) Cahon oxVnuonde (R.V Carbon tetrachloride Chlaal CMorambudl Chlordane, aW6 gamma iwmm Chbmephean Chlorobenzene CMcrobendhte paJoro-~esol 40 CFR Ch. 1 (7-1-89 Edition)

Subslance -No. U042 110-75-8 2-Chloroethyl nnyl ether U044 67-66-3 Chloroform U046 107-30-2 Chloromethyl methyl ether U047 91-58-7 beta-Chloronaphthalene U048 95-57-8 o-Chlorophenol U049 3165-93-3 4-Chloro-o-toluid~ne.hydrochloride U032 13765-19-0 Chromic acid H2Cr04,calcium salt U050 218-01 -9 Chrysene U051 Creosote U052 1319-77-3 Cresol (Cresyltc acid) U053 , 4 170-30-3 Grotonaldehyde U055 98-82-8 Cumene (I) U246 506-68-3 Cyanogen bromlde (CN)Br U197 106-51 -4 2,5-Cyclohexadtene-1.4dione U056 110-82-7 Cyclohexane (I) U129 58-89-9 Cyclohexane. 1.2.3.4.5.8hexechloro-, (1alpha.2alpha.3belata4elpha,5alphe,6beta)- 108-94-1 Cyclohexanone (I) 77-47-4 1.3-Cyclopentad~ene1.2.3,4,5.5-hexechloro- 50-18-0 Cyclophospham~de 1 94-75-7 2.4-D. salts 8 esters 20830-81-3 Daunomycin 72-54-8 DDD 50-29-3 DDT 2303- 16-4 D~allate 53-70-3 Dibenz[a.hlanthracene 189-55-9 DIbenzo[a.ilpyrene 96-12-8 1,2-Dibromo-3-chloropropane 84-74-2 Dibutyl phihalate 95-50-1 o-Dichlorobenzene 541-73-1 m-Dichlorobenzene 106-46-7 p-D~chlorobenzene 91-94-1 3.3'-Dichlorobenz~dine 764-41 -0 1,4-Dchloro-2-butene (1.T) 75-71 -8 Dichlorod~lluoromethane 75-35-4 1.l-Dichloroethylene 156-60-5 , 1.2-D~chloroethylene 111-44-4 D~chloroelhylether 108-60-1 Dtchloro~sopropylether 11 1-91 -1 Dichloromethoxy ethane 120-83-2 2,4-Dtchlorophenol 87-65-0 2.6-bchlorophenol 542-75-6 1.3-Dlchloropropene 1464-53-5 1.2:3.4-Diepoxybutane (1.T) 123-91-1 1.4-Dmthyleneox~de 117-81-7 Dtethylhexyl phthalate 1615-80- 1 N.N'-Wethylhydraztne 3288-58-2 0.0-Dlethyl S-methyl dithiophgsphate 84-66-2 Dtethyl phthalate 56-53-1 Diethylstilbesterol 94-58-6 bhydroeafrole 119-90-4 3.3'-D~methoxybenzidine 124-40-3 1 Dtmethvlamine (1)

U095 1 19-93-7 3,3'-bmeth$benzld1& U096 80-1 5-9 [email protected]~~droperoxide(R) w97 79-44-7 Dimethylcsrbamoyl chloride U098 57-1 4-7 1.1 -bmethylhydrazine U099 540-73-8 1,2-Dtrnelhylhydraz~ne UlOl 105-67-9 2.4-bmelhylphenol Ul02 131-1 1-3 [)lmethyl phthalete U103 77-78-1 OHnethyl sulfate U105 121-14-2 2,4-DIn1trotoloene U106 -20-2 2,&hnRrgtoluene U107 117-84-0 &n-oclyl phthalate Uloe 123-91-1 1.4-Dtoxane UlOg 122-667 1.2-Dphenylhydrazine UllO 142-84-7 Dpropylamine (I) Ulll 621-64-7 Dcn-propyinitrosamine 5 261.33 40 CPR Ch. 1 (7-1-89 Edition) (f) The commercial chemical prod- [Comment: For the convenience of the regu- ucts, manfacturing chemical interme- lated communit~.the primary hazardous diates, or off-specification commercial properties of these materials have been indi- chemical products referred to in para- cated by the letters T (Toxicity), R (Reac- tivity). I (Ignitability) and C (Corrosivity). through Of this section' Absence of a letter indicates that the con- are identified as toxic wastes (TI, pound is only for toxicity.3 unless otherwise designated and are subject to the small quantity genera- These wastes and their correspond- tor exclusion defined in 5 261.5 t a) and ing EPA Hazardous Waste Numbers (g). are:

Hat- r ardous Chemical Substance waste abstracts No. No.

UWl I Acetaldehyde (I) U034 Acetaldehyde, tr~chloro- U187 1 Acetam~de.N-(4-ethoxypheny1)- uw5 Acetam~de.N-9H-fluoren-2-yl- U240 Acet~cac~d. (2.4-d~chlorophenoxy)-. salts & esters U112 Acettc ac~dethyl ester (I) U144 Acet~cac~d, lead(2 +) salt U214 Acet~cacd, thalltum(1+) salt see Acet~cac~d. (2.4.5-tr~chlorophenoxy)- F027 U002 67-64-1 Acetone (I) UW3 75-05-8 Acetonitrile (l,T) U004 98-86-2 Acetophenone UW5 53-96-3 2-Acetylaminofluorene UW6 75-36-5 Acelyl chloride (C.R.T) U007 79-06-1 Acrylamide U008 79-10-7 Acryltc ac~d(1) U009 107-1 3-1 Acrylon~trile UOl 1 61-82-5 Amitrole U012 62-53-3 Aniline (l,T) U136 75-60-5 Arsinlc acid, dimethyl- U014 492-80-8 Auram~ne U015 115-02-6 Azaserlne UOIO 50-07-7 Azinno~2'.3':3.4lpyrroloL1.2-alindole~4,7-dione,&~no6-[C(aminocarbonyl)oxylme~l- 1.la.2.8.8a.8b-hexahydr0-88-methoxy-5-~l-, [laS(lulphr. 8bet&BePlpha,8balpha)l- 56-49-5 Benz[ilaceanthrylene, 1.2-dihydro-3-methyl- 225-51-4 BenzLclacridine 98-87-3 Benzal chloride 23950-58-5 Benzam~de.3.5-dichloro-N-(1,ldimethyl-2-prOWny))- 56-55-3 Benztalanthracene 57-97-6 BenzLalanthracene, 7.12-d~rnethyl- 62-53-3 Benzenamlne (l,T) 492-80-8 Benzenam~ne.4.4'-carbonimidoylbisCN.N-dimethyl- 3165-93-3 Benzenamne, 4-chloro-2-methyl-, hydrochloride 60-1 1-7 Benzenemine. N,N-dimethyl-4-(phenylazo)- 95-53-4 Benzenam~ne,2-methyl- 106-49-0 Benzenam~ne,4-methyl- 101-14-4 Benzenamine, 4.4'-methylenebis[2-chloro- 636-21-5 Benzenamine. 2-methyl., hydrochloride 99-55-8 Benzenamine, 2-methyl-bnitro- 71-43-2 Benzene (l,T) 510-15-6 Benzeneacetic acid. 4-chloro-alpha-(&hlorophe~)-~-~oxy-ahyl ester 101-55-3 Benzene, 1-bromo-4-phenoxy- 305-03-3 Benzenebutanoic acid, 4-[bis(2-chloroethfl]aminol- 108-90-7 Benzene, chloro- 25376-45-8 Benzenediamine, ar-methyl- 117-81 -7 1,2-Benzenediirboxylic acid. bis(2-ethylhexyl) ester 64-74-2 1,2-Ben~en~carboxylic acid, dtbutyl ester 64-66-2 1,2-Benzened1carboxyIic acid, diethyl ester 131-1 1-3 1,2-Benzenediixyl'i acid, dhethyl ester 117-84-0 1,2-Benzenediixylk acid, ckctyl ester 95-50-1 Benzene, 1.2-dichloro- 541-73-1 Benzene, 1,3dkhloro- 106-46-7 Benzene. 1.4diil~ 72-54-8 Benzene. 1.1 '-(2,2-dichlwoe~~)bisC4cMoro- Environmental Protection Agency

/ snn, 1 "waste abstracts No. No.

PO41 31 1-45-5 Phosphoric acid. ckethyl 4-nitrophenyl ester PO39 298-04-4 Phosphorodithiw acid, 0,Wlethyl S-t2-(ethylthio~lester Po94 298-02-2 Phosphorodithi acid, 0,O-dimthyl S-[(ethylthlo)me~Iester Po44 60-51-5 Phosphorodithioic acid. 0.0-dimethyl S-12-(methylamino)-2~xoethyllester KM3 55-91 -4 Phosphorolluoridic add, bis(1-methylethyt) ester Po89 56-38-2 Phosphorothioic acid. 0.0-diethyl 0-(4-nilrophenyl) ester POSO 297-97-2 Phosphorothii acid, 0,Wiethyl O-Pymzinyl ester Po97 52-85-7 Phosphorothii acid. 0-[4-[(dimethylamir~))sulfonyllphenyll0.0dikthyl ester PO71 298-00-0 Phosphorothii acid. 0.0.-dimethyl O(4-nitrophenyl) ester PI10 76-00-2 Plumbane, IetraeIhyh PO98 151-50-8 Potassurn cyanide Po98 151-50-8 Potassium cyanide K(CN) PO99 506-61 -6 Potassium silver cyanide PO70 116-06-3 Propanal. 2-methyl-2-(methylthio)-. 0-[(methylamino)csrbon~30xime PI01 107-1 2-0 Propanenitrile PO27 542-767 Propanenitrile. 3chloro. Po69 75-865 Propanenitnle, 2-hydroxy-2-methyl- Po81 55-63-0 1.2.3-Propanekn~l,trinitrate (R) PO1 7 598-31 -2 2-Propanone. 1-bromcr- PI02 107-1 9-7 Propargyl alcohol PO03 107-02-8 2-Pr0pe~l PO05 107-18-6 2-Propen-14 Po67 75-55-8 1-2-Propylenimine PI02 107-19-7 2-Propyn-1-01 Po08 504-24-5 4-Pynd~namine PO75 1 54-1 1-5 Pyridine, 3-(l-methyl-2-~didinyl)-.(S)-. & mlts PI14 12039-52-0 Selenious acid, dithallium(1 +) salt P103 630-10-4 Selenourea PI04 50664-9 Sllver cyanide PI04 506-64-9 Sllver cyan~deAg(CN) PI05 26628-22-8 Sodium azde PI06 143-33-9 Sodium cyanide PI06 143-33-9 Sodium cyanlde Na(CN) PI07 1314-96-1 Strontium sulfide SrS PI06 57-24-9 Strychndn-lOone, 6 salts PO18 357-57-3 Strychnidin.lOone, 2,Wmethowy- PI06 8 57-24-9 Strychnine. 6 salts PI15 7446-18-6 Sulfuric ad, dithalli(l+) salt PI09 3689-24-5 Tetraethyhjiw'iqhosphate PI10 78-00-2 Tetraethyl lead PI11 107-49-3 Tetraethyl ~rophosphate PI12 509-14-8 Tetranitromethane (R) PO62 757-58-4 Tetraphosphonc acid, hexaethyl ester PI13 1314-32-5 Thallic oxide I PI13 1314-32-5 Thallium ox& TbOI PI14 12039-52-0 Thallium(1) selenite PI15 7446-18-6 Thallium(l) sulfate PI09 3689-24-5 Thiod~phosphoncacid. telraethyl ester PO45 39196-18-4 Thofanox PO49 54 1-53-7 Thiimldodicarbonic diamide t(KN)C(S)],NH W14 106-98-5 Tmhenol P116 79-19-6 Thi~wmtmbazide PO26 5344-82-1 Thiourea, (2-chbophenyo. PO72 8688-4 Thowee, l-naphthalenyl- PO83 103-85-5 Thiourea. phenyl- Pl23 8001-35-2 Toxaphene PI10 75-70-7 Tnchlwomethanethiol PI19 7803-55-6 Vgnarhc ad, ammonium sall PI20 1314-62-1 Vanadium oxide VA PI20 1314-62-1 Vanabum pentoxide #It)s 4548-40-0 Vimine. N-mthyl-Nnitro~o. Fall 81-81-2 Wufuin. 6 MI& when plermt 1cmmUmt#nr gmlw Uun 0.3% P121 557-21-1 Zinc cyanide P121 557-21-1 ZiwuMe Zn(CNh PI22 1314-84-7 Zinc ph#phide ZrbPs. p.mt at qwOr (hm 10% (R,T)

'CAS Nunkrgivenfap~ntcompwndonly. Environmental Protection Agency

No. I I I

~179 Ute0 U181 U103 U058

U115 75-21-8 Wane (1.T) U128 765-34-4 Oxuanecarboxyaldehyde U041 106-89-8 Oxwane. (chl0romethyl)- U182 123-63-7 Paraldehyde U183 606-93-5 Pentachlorobenzene U184 76-01 -7 Pentachloroethane U185 82-68-8 I Penlachloronitrobenzene IPCNB) see 87-86-5 Pentachlorophenol F027 I U161 Pentanol, 4-methyl- U186 1.3-Pentadiene (I) U187 Phenacetin U188 Phenol U048 Phenol. O-chloro- U038 Phenol, 4ehloro-3-methyl- U081 Phenol. 2,4diihloro- U082 Phenol. 2,64chloro- U089 Phenol, 4.4'-(1.2-dielhyl-1.28~)bis-,(E)- UIOI Phenol, 2,4dimelhyl- w2 M,methyl- U132 Phenol. 2,2'-methflenebi~[3,4,6tfkhbf0- U170 Phenol, 4-nitro- See Phenol, pentachlore F027 see 58-90-2 Phenol, 2.3.4.6tetrachloro- F027 I See 05-95-4 Phenol. 2.4,Stfichloro- F027 I see 8806-2 Phenol, 2,4,8tfichloro- F027 u150 L-Phenylalanine, 4-[bis(2~~1- U145 Phosphoric add. lead(2 + ) mll(23) U087 Phosphorodithi ad, 0,adiethyl Smethyl eater ui8e -s wlhde (R) Ulgo Phthalic anhydride U101 2-Wine U17Q Pine.1 -nitroso- U192 Pronamide UlQ4 1-Propanemine (I,T)

propane, 1,2dibr&3&1& Propane. 1,2-dichloro- Propanedinitrile Propane, 2-nitro- (1.T) Propane. 2.2'0xyksC2-chloro- 1.3-Propane wltone Propanoic acid, 2-(2.4,5-t1ichlorophmoxy)- 10 CFR Ch. 1 (7-1-89 Edition)

No. I I I 1 U152 126-98-7 2-Propenenitrile, 2-methyl- (1.T) U008 79-10-7 2-Propenoic acid (I) U113 140-08-5 2-Propenoic acid, ethyl ester (I) U118 97-63-2 2-Propeno~cacid. 2-methyl-. ethyl ester U162 80-62-6 2-Propenoic acid, 2-methyl-, methyl ester (1.T) U194 107-10-8 n-Propylamine (l,T) U083 78-87-5 Propylene dichloride U148 123-33-1 3.6Pyridazinedione. 1.2dihydro- U196 110-861 Pyndine U191 109-06-8 Pyridine. 2-methyl- U237 66-75-1 2,4-(1H,3H)-Pyrimid~nedione, 5-Cbis(2- chloroethyl)aminol- U164 56-04-2 4(lH)-Pyr~midinone.2.3dihydro-6-methyl-2-thioxo- U180 930-55-2 Pynolidine, 1-n~troso- U200 50-55-5 Reserp~ne U201 108-46-3 Resorcinol U202 1 81-07-2 Saccharin. 8 salts U203 04-59-7 Safrole U204 778340-8 Selenious acid U204 7783-00-8 Selenium dioxide U205 7488-564 Selenium sulfide u205 7488-56-4 Selenium sulfide SeS (R,T) U015 115-02-6 L-Senne, diazoacetate (ester) see 93-72-1 Silvex (2,4.5-TP) F027 U206 Streptozotocin U103 Sulfunc ac~d,dimethyl ester U189 Sulfur phosphide (R) See 2,4.5-T F027 U207 Urn8 U209 U210 127-1 8-4 Tetrachloroethylene See 58-90-2 2,3.4,6-Tetrachlorophenol F027 U213 , Tetrahydrofuran (I) U214 Thallium(l) acetate U215 Thallium(l) carbonate U216 TWlium(1) chloride U216 Thallium chlonde Tlcl U217 Thellium(1) nitrate U218 Thiicetamide U153 Thiomethanol (1,T) U244 Thmperoxydiirbonic diamide C(I.kN)C(S)lrSI,tetrameuryl- U219 Thiourea U244 Thiam U220 Toluene U221 Tduenediamine U223 Toluene diisccyanale (R,T) U328 o-Toluidine U353 pToluid~ne U222 o-Toluid~nehydrochloride UOll 1H-1.2.4-TriBzol-3-amine U227 1.1 ,2-Tnchloroethane U228 Trichloroethylene U121 Trichlorornonoflwxornethane See 2.4.5-Tnchlormnol F027 See F027 U234 U182 U235 U236 U237 U176 Ul77 U043 U24a Environmental Protection Agency Part 261, App. II

substance

~239 1330-20-7 Xylene (I) urn 50-55-5 Yoh~mban-16-carboxylicacid, 11,17-dimethoxy-l&C(3,4.5.~J-, mrlhyl m, (3bea1&eta, 17alpha, 18bota,20alpha)- U249 1314-84-7 Zinc phosphrde ZrbP,, when pmt at cmcentrations of 10% or ka

I CAS Number given for parent compound only. (Approved by the Office of Management and Budget under control number 2050-0047) I45 FR 78529.78541, Nov. 25,19801 EDITORIALNo% For FEDERALREGISTER citations affecting 8 261.33, see the List of CFR Sections Affected in the Finding Aids section of this volume.

The methods and equipment used for sampling waste materials will vary with the A. Extraction Ptocedure (EP) fonn and consistency of the waste materials 1. A representative sample of the waste to to be sampled. Samples collected using the be tested (minimum she 100 grams) shall be sampling protocols listed below, for sam- obtained using the methods specified in Ap- pling waste with properties similar to the in- pendix I or any other method capable of dicated materials, will be considered by the yielding a representative sample within the Agency to be representative of the waste. meaning of Part 260. [For detailed guidance on conducting the various aspects of the EP Extremely viscous liquid-ASTM Standard see ".Test Methods for the Evaluation of D140-70 Crushed or powdered material- Solid Waste, Physical/Chemical Methods" ASTM Standard 0346-75 Soil or rock-like (incorporated by reference, see 8 260.11 1.1 material-ASTM Standard D420-69 Soil- 2. The sample shall be separated into its like material-ASTM Standard D1452-65 component liquid and solid phases using the Fly Ash-like material-ASTM Standard method described in "Separation Roce- D2234-76 CASTM Standards are available dure" below. If the solid residue obtained from ASTM, 1916 Race St., Philadelphia, using this method totab less than 0.5% of PA 191031 the original weight of the waste, the residue Containerized liquid wastes-"COLIWASA" can be. discarded and the operator shall described in "Test Methods for the Eval- treat the liquid phase as the extract and uation of Solid Waste, Physical/Chemical proceed immediately to Step 8. Methods," * U.S. Environmental Protec- 3. The solid material obtained- from the tion Agency. Office of Solid Waste, Wash- Separation Rocedure shall be evalusted for ington, D.C. 20460. [Copies may be ob- its particle size. If the solid material has a tained from Solid Waste Information, U.S. surface area per gram of material equal to, Environmental Protection Agency, 26 W. or greater than, 3.1 cm2or passes through a 9.6 mm (0.375 inch) standard sieve, the oper- St. Clair St., Cincinnati, Ohio 452681 ator shall proceed to Step 4. If the surface Liquid waste in pits, ponds, lagoons, and area is smaller or the particle size larger #Mar reservoirs.-"Pond Sampler" de- than specified above, the solid material scribed in "Test Methods for the Evalua- shall be prepared for extraction by crush- tion of Solid Waste, Physical/Chemical ing, cutting or grinding the material so that Methods." * This manual also ~~ntahadditional in- The percent solids is determined by fonnation on application of these protocols. dryinp the futer paat 80-c ~tflit reaches co~tantweight and then calculating the percent nollds using the following equation: Percent =

mTheaernetho0.45 pm. If the sample will 60 minute intervals, moving to the next not filter, various other separation tech- longer interval if the pH does not have to be niques can be used to aid in the filtration. adjusted more than 0.5N pH units. As described above, pressure filtration is tc) The adjustment procedure shall be employed to speed up the filtration process. continued for at least 6 hours. This does not alter the nature of the separa- (dl If at the end of the 24-hour extraction tion. If liquid does not separate during fU- period. the pH of the solution is not below tration, the waste can be centrifuged. If sep- 5.2 and the maximum amount of acid (4 ml aration occurs during centrifugation, the per gram of solids) has not been added, the liquid portion tcentrifugate) is filtered pH shall be adjusted to 5.0 + 0.2 and the ex- through the 0.45 pm filter prior to becoming traction continued for an additional four mixed with the liquid portion of the waste hours. during which the pH shall be adjust- obtained from the initial ftltration. Any ma- ed at one hour intervals. terial that will not pass through the filter 6. At the end of the 24 hour extraction after centrifugation Is considered a solid period, deionized water shall be added to and is extracted. Appendix D

Tramp Oil Removal Equipment Vendors

Oil Skimmer Suppliers

Centri-Spray Corp. Monroe Environmental Corp. Butch Abdo P.O. Box 806 39001 Schoolcraft Rd. Monroe, MI 84161 Livonia, MI 48150 (800)992-7707 (313)464-0100 None in Iowa. Monroe Envi. Corp.- Iowa Rep. Jerry McGill Cincinnati Industrial Machinery Integrated Industries Inc. 2027 Hageman St. 7 North Union St. Cincinnati, OH 45241 Elgin, IL 60123 (513)769-0700 (708)471-0870 None in Iowa. Oil Skimmers, Inc. Hudson Industries P.O. Box 33092 P.O. Box 2212 Cleveland, OH 44133 Hudson, OH 41228 (216)237-4600 (216)487-0668 None in Iowa. Oil Skimmers - Iowa Rep. Lyle or Ken Morse Hyde Products Inc. Morse Equipment Co. Iowa Rep.- Jerry Sileoff P.O. Box 741 Pheonix Limited Des Moines, IA 50309 P.O. Box 66012 (515)223-1236 West Des Moines, IA 50265 (515)279-9228 Plasfab Inc. 33 Minnesota Ave. MacDermid Group, J.T. Warwick, RI 02888 (203)283-5858 (401)739-1810 None in Iowa. Plasfab 1nc.- Iowa Rep. Man-Gill Chemical Co. Chuck Erdman Kathy Spik - New accounts Rep. Chemrey Corp. 2300 St. Clair Ave. 9842 Roosevelt Rd. Cleveland, OH 44117 Westchester, IL (800)627-6422 (708)344-2400 None in Iowa. Quality Plating Service Met-Pro Corp., Systems Div. Mike Triplett P.O. Box 144 P.O. Box 142 Harleysville, PA 19438 Bristol, CT 06010 (215)723-6751 (203)582-7518 None in Iowa. None in Iowa.

Appendix E

Used Oil Management Companies

Oil Recyclers

1. Capital Oil 1128 N. 11th Street Omaha, NE 68102 (402) 346-7441

2. Industrial Service Corp. 1128 Dunkerton Road Cedar Falls, IA 50613 (319) 266-2369

3. Jebro Inc. 2302 Bridgeport Drive Sioux City, IA 51111 (800) 831-8037

4. Safety-Kleen Oil Service 3035 West 73rd St. Davenport, IA 52806 (319) 386-3024

5. WiMett Oil Company 10404 NW 46th Avenue Des Moines, IA (515) 276-2785

6. BresLube USA Inc. 7001 West 62nd St. Chicago, IL 60638 (608) 785- 1563

7. Cedar Falls Oil Service 424 N Ellen Cedar Falls, IA 50613 (319) 266-7283

8. Oil Service Inc. 6503 Cecelia Circle Bloomington, MN 55435 (612) 943-8198

Appendix F

Distillation Equipment Vendors

Solvent Distillation Equipment Acra Electric COW.* Finish Engineering Co. 3801 N 25th Avenue Peter B. Scantlebury Schiller Park, IL 60176-2187 921 Creenyard Rd. 3121678-8870 Erie, PA 16501-1591 8 144554478 Artech, Inc. Bob Skorpil Interel cow.** 1221 East Houston Paris R. Briscoe Broken Arrow, OK 74012 P.O. Box 4676 9181251-0880 Englewood, CO 80155 3OY773-0753 B/R Instrument Corp. Ann D. Cole Lenan Corporation P.O. Box 7 Arnie Nehls Pasadena, MD 21121 615 N. Parker 6 121452-5695 Janesville, WI 53545 8OOl922-9206 608l752-1601 800-356-9424 Baron-Blakeslee J.M. Bowman Lenape Sales & Sewice, Inc. 2001 North Janice Ave. James J. Mastrain, Jr. Melrose Park, IL 60160 P.O. Box 285 3121450-4015 Manasquan, NJ 08736 2011681-2442 ChernIServ, Inc. Steve Beauchaine PBR Industries, Inc. 207 NE 6th Street 400 Farmingdale Rd. Minneapolis, MN 55413 West Babylon, NY 11704 6121'379-4411 5161422-0057 Corning Process Systems Progressive Recovery, Inc. William T. Jackson Joe Miller Corning Class Works 1020 North Main St. Big Flats Plant Columbia, IL 62236 Corning, NY 14830 618l281-7196 607l974-0299 Recyclene Products, Inc. DCI International Refus Williams Robert M. Zopf 404 Eccles Ave. 1229 Country Club Rd. S. San Francisco, CA 94080 Indianopolis, IN 46234 4151589-9600 317I271-4001 Renzmann Incorporated Detrex Corporation A1 M. Moser P.O. Box 5111 310 Oser Ave Southfield, MI 48086-5111 Hauppauge, NY 11788 313L358-5800 5161231-3030 Distillation Environmental Seneca Corp. Systems, Inc. Marvin Cooley 525 Boulevard 5636 NE 17th Street Kenilworth, NJ 07033 Des Moines, IA 50313 201I272-7600 8001362-2910 Dove Equipment Co., Inc. Roy H. Winemiller 1110 North Main Street East Peoria, IL 61611 3091694-6228 * Manufacture drum dewatering equipment in addition to stills. ** Barrel Distiller - a 55 gallon drum can be placed inside the still.

Appendix G

Hazardous Waste Management Companies

Hazardous Waste Management Companies

Aptus #* 10. Mineral Springs Corp. 21750 Cedar Avenue P.O. Box 500 Lakeville, MN 55044 Port Washington, WI 53074 8001328-4061 414284-9101 Dave Dashow 8001932-62 16 Barb Allen Chemical Waste Management Co. 2000 South Batavia Ave. 11. NUKEM Treatment Services Geneva, IL 60134 17515 West 9 Mile Road 7081513-4525 Southfield, MI 48075 Jeff Nelson 31Y559-5900 Lori Read ENSCO, Inc. 3112 Valley Creek Dr., Suite C # 12. Peoria Disposal Co. Baton Rouge, LA 70808 4700 North Sterling Avenue 5041927-9600 Peoria, IL 61615 Tom Englert 3091688-0760 Michelle Hillman Enviri te Corporation Doug Beck 620 West Germantown Pike Suite 250 Plymouth Meeting, PA 19462 13. Rollins Environmental Services 2151828-8655 P.O. Box 74137 Neil Daeubler Baton Rouge, LA 70874-4137 504'778-3535 Environmental Associated Services & David LaCoste Engineering, Inc. 2100 Eighteenth Avenue, Suite 2N * 14. Safety-Kleen Rock Island, IL 61201 7582 Hickman Road 3091788-4048 Des Moines, IA 50322 Laura Johnson 519270-8027 Brad Knudson Hydrite Chemical, Co 2815 WCF & North Drive 15. Systech Environmental Corp. Waterloo, IA 50703 245 North Valley Road 3191232-9731 Xenia, OH 45385 Mike Anderson 5131372-8077 Pat Lang Laidlaw Environmental Services 6125 North Pecatonica Road # 16. U.S. Pollution Control, Inc. P.O. Box 479 515 West Green Road, Suite 500 Pecatonica, IL 61063-0479 Houston, TX 77067 8151239-2377 4021493-8386 Craig Dummer 8001877-2401 Sheree Miller LWD P.O. Box 327 #* 17. Van Waters & Rogers, Inc. Calvert City, KY 42029 P.O. Box 159 5021395-8313 1819 West Burlington Avenue Susan Limpman Burlington, IA 52601 3191753-2253 Michigan Disposal, Inc. 8001828-9870 49350 North I94 Service Drive Gary McPherson Belleville, MI 48111 3131697-7830 Bob Pelissier

Appendix H

NPDES Permit Application Summary - Process Waters

NPDES permits are required for all discharges of wastewater to any public waterway. Public waterways include rivers, lakes, wells, ditches, and drain tiles. Wastewater discharges include noncontact cooling water, process water, and storm water. To receive a NPDES permit for process water discharges, Form 1and Form 3 should be completed and submitted to the Water Permits Section, Iowa Department of Natural Resources. Form 1 and Form 3 are available upon request from the IWRC (8001422-3109) and the DNR (8001532-11 14).

Form 1 requests general information regarding the facility name and location, contact persons, any current operating permits and licenses, any analytical results from wastewater testing, a topographical map, and sources and uses of water at the facility. Form 1 must be completed regardless of the type of discharge requiring a permit.

Form 3 is completed when a NPDES permit is sought for process wastewater. Specific information regarding average and maximum flowrates, duration of discharge, frequency of the discharge, and all pollutants must be reported. In addition, analytical test data must be obtained and reported for various parameters requested by the DNR. Required tests typically include metals concentration, biological oxygen demand, suspended solids, temperature, total organic carbon, nitrates, and chlorides. Since NPDES permits for process wastewater discharges are granted on a case-by-case basis, additional testing may be required. Contributing factors to NPDES permit requirements include the volume of water being discharged, contamination levels, other industrial discharges within the same water zone, and existing conditions of the receiving water.

IWRC staff are available to assist facilities in completing the necessary forms. Please contact our office at 8001422-3109 if you have determined your facility needs a NPDES permit, or have questions regarding the NPDES permit application process.

Appendix I

Total Toxic Organics (TTO) Solvent Management Plan

Total Toxic Organics Acenaphthene N-nitrosodi-n-propylamine Acrolein Pentachlorophenol Acrylonitrile Phenol Benzene Bis (2-ethylhexyl) phthalate Benzidine Butyl benzyl phthalate Carbon tetrachloride (tetrachloromethane) Di-n-butyl phthalate Chlorobenzene Di-n-octyl phthalate 1,2,4-Trichlorobenzene Diethyl phthalate Hexachlorobenzene Dimethyl phthalate l,2-Dichloroethane ' 1,2-Benzanthracene l,l,l-Trichloroethane (benzo(a)anthracene) Hexachloroethane Benzo(a)pyrene (3,4-benzopyrene) 1,l-Dichloroethane 34-Benzofluoranthene 1,1,2-Trichloroethane (benzo(b)fluoranthene) 1,1,2,2-Tetrachloroethane 11,12-Benzofluoranthene Chloroethane (benzo(k)fluoranthene) Bis (2-chloroethyl) ether Chrysene 2-Chloroethyl vinyl ether (mixed) Acenaphthylene 2-Chloronaphthalene Anthracene 2,4,6-Trichlorophenol 1,12-Benzoperylene (benzo(ghi)perylene) Parachlorometa cresol Fluorene Chloroform (trichloromethane) Phenanthrene 2-Chlorophenol 1,2,5,6-Dibenzanthracene 1,2-Dichlorobenzene (dibenzo(a,h)anthracene) 1,3-Dichlorobenzene Indeno(l,2,3-cd) pyrene (23-o-phenlene pyrene) l,4-Dichlorobenzene Pyrene 3,3-Dichlorobenzidine Tetrachloroethylene 1,l-Dichloroethylene Toluene 1,2 Trans-dichloroethylene Trichloroethylene 2,4-Dichlorophenol Vinyl chloride (chloroethylene) 1,2-Dichloropropane Aldrin 1,3-Dichloropropylene (1,3-dichloropropene) Dieldrin 2,4-Dimethylphenol Chlordane (technical mixture and metabolites) 2,4-Dinitrotoluene 4,4-DDT 2,6-Dinitrotoluene 4,4-DDE (p,p-DDX) 1,2-Diphenylhydrazine 4,4-DDD (p,p-TDE) Ethylbenzene Alpha-endosulfan Fluoranthene Beta-endosulfan 4-Chlorophenyl phenyl ether Endosulfan sulfate 4Bromophenyl phenyl ether Endrin Bis (2-chloroisopropyl) ether Endrin aldehyde Bis (2-chloroethoxy) methane Heptachlor Methylene chloride (dichloromethane) Heptachlor epoxide Methyl chloride (chloromethane) (BHC-hexachlorocyclohexane) Methyl bromide (bromomethane) Alpha-BHC Bromoform (tribromomethane) Beta-BHC Dichlorobromomethane Gamma-BHC Chlorodibromomethane Delta-BHC Hexaclorobutadiene PCB-polychlorinated biphenyls Hexachlorocyclopentadiene PCB-1242 (Arochlor 1242) Isophorone PCB-12% (Arochlor 1254) Naphthalene PCB-1221 (Arochlor 1221) Nitrobenzene PCB-1232 (Arochlor 1232) 2-Nitrophenol PCB-1248 (Arochlor 1248) 4-Nitrophenol PCB-1260 (Arochlor 1260) 2,4-Dinitrophenol PCB-1016 (Arochlor 1016) 4,6-Dinitro-o-cresol Toxaphene N-nitrosodimethylamine 2,3,7,8-Tetrachlorodibenzo-p-dioxin(TCDD) N-nitrosodiphenylamine Total Toxic Organics Certification and Management Plan

Certification:

"Based on my inquiry of the person or persons directly responsible for Managing compliance with the pretreatment standard for total toxic organics ('ITO), I certify that, to the best of my knowledge and belief, no dumping of concentrated toxic organics into the wastewaters has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the toxic organics management plan submitted to the control authority."

Name, Title

Management Plan:

A. Toxic Organic Compounds Used. 1. No listed TTO's are used at the facility. Only an unlisted organic, is used as a paint thinner and cleanup solvent.

B. Method of Disposal 1. All waste organic solvents (no TTO's) are recycled under contract with

C. Spill Prevention

1. All solvents (no TTO's) are stored 2. Spill cleanup equipment is stored near each solvent storageluse area. Appendix J

Analytical Laboratories

Analytical Laboratories

1. A & L Mid West Laboratories, Inc. 13611 "B" Street Omaha, NE 68144 4021334-77'70 Donna LaMura

2. Groundwater Technology, Inc. 5 158 Park Avenue Des Moines, IA 50321 5151282-9132 Deanne Geile

3. National Environmental Testing Cedar Falls, IA 50613 3191277-2401 Mike McGee

4. QCML, Inc. Davenport, IA 52804 3191386-7827 Lori Korsen

5. State Hygienic Lab Iowa City, IA 52240 3 191335-4500

6. Behnken Laboratories, Inc. 410 Johnson Street, PO Box 26 Keokuk, IA 52632 3191524-6431 Scott C. Behnken

7. Keystone Laboratories 501 W. 3rd Street North Newton, IA 50208 5151792-8451 Jeff King

Appendix K

SWA Test Parameters SWA Application

Special Waste Authorization Test Parameters

The following lab analysis must be performed and a copy of the results submitted with the Special Waste Authorization (SWA) application to the Department of Natural Resources.

1. Toxicity Characteristics Leaching Procedure (TCLP) Only those constituents suspected to be present must be tested for. Documentation of the rationale for parameter selection may be required. The eight metals must be tested for regardless. If a virgin product is being disposed, a MSDS may be substituted for the TCLP test. Contact the DNR at (515) 281-3426 prior to deleting any constituents.

Arsenic Barium Cadmium Chromium Lead Mercury Selenium Silver

2. Initial pH of the waste pH must be between 2 and 12.5

3. Paint Filter Liquids Test This is a passlfail test to determine if there are any free liquids in the waste material. If there are no free liquids, the material passes the test.

4. Total Extractable Hydrocarbons This test is only required for paint, varnish, and stain wastes. The result must be less than 1%, or 10,000 mgkg for disposal in an Iowa landfill.

IOWA DEPARTMENT OF NATURAL RESOURCES REQUEST FOR SPECIAL WASTE AUTHORIZATION DISPOSAL INSTRUCTIONS - - - - NOTE: Completion of this form recpires reference to Chapter 40, Code of Federal Regulations (CFR), Part 261. I Please type or print in ink. Conplete each item in its entirety. 1

FOR IfWUlPUTXM. HtnE --> Special Waste Authorization Environmental Protection Division Department of Natural Resources Henry A. Wallace Building) 900 East Grand Des Hoines, IA 50319-0034

-- PART I - GDERAL INF~TIM IS THIS IS A REWEST FOR RENEWAL OF A CURRENT SPECIAL WASTE AUTHORIZATION (!MA)? Yes [I No 11 IF YES, SWA WER IS -

NAHE

)urn ADDRESS CITY STATE ZIP GRERA-roR

NAME OF CONTACT PERSON TITLE PHONE

DISWSAL - ADDRESS CITY STATE ZIP

PIRT I1 - )USTE CHARACTrRTURON

NAME OF WASTE SWRCE OF WASTE

WASTE ON HAND FOR ImEDIATE DISPOSAL

LBS .

DISPOSAL WEIGHT PER DISPOSAL TIME PERIOD BETWEEN DISPOSALS IcAlE

.A

BASIC PHYSICAL STATE AT 70 F PERCENT SOLIDS pH (if solid, use 10% FLASH POINT PAINT FILTER ( room temperature distilled water) FOR LIQUIDS LIQUIDS TEST (1 Solid t 1 Liquid [ISludge % CF [I Pass 11 Fail - - -- HYDROCARBON SOLVENT (for paint, varnish, and stain-related wastes)

HAS ANY PRETREATMENT BEEN UTILIZED? If yes, describe.

I I Yes [I No

List all organic chemical constituents and percentage of the waste stream (raw material sllppliers may be able to assist with this information).

)R form ( 10-90/sp 542-3216 [I Protective clothing/suit I I Raspirator C I Absorbent tECESSARY ' C 1 R-r glover 1 I Gas mask f I Portable eye wasWshawer SAFETY Earn 1 I Rdher boots I1 Self-contained breathing I I Prnp truck w/water FOR apparatus MUNG [I Face shieldlgoggles I I Lime =>

I I Type "B" fire axtiwisher/ f 1 Other speeify fire blanket I I [INa

Is this waste listed utder any of tho following (from 40 C.F.R.,)? YES EPA H.W. NO. NO I261.31 Hazardous Waste from Nonspecific Sources ...... t I 11 261.32 Hazardous Waste from Specific Swrces ...... t 1 11

261.33 Discarded Commercial Chemical Pr&tsr Off-Specificatim,Sp.cies, Containers and Spill Residues Thereof:

261.33(f) ToxicWaste ...... [ 1 f I

If ywr mote has been delisted. attach a copy of EPA approval for dolisting. laboratorb Does the waste exhibit any of the following ohrractm~istics? results tc complete YES EPA H.W. NO. NO this item]

Ignitability (see 261.21 1 ...... I I I I

Corrosivity (see 261.22) ...... f 1 f 1

Reactivity (see 261.23 1 ...... 1 1 1 1

Toxicity Characteristic (see 261.24) ...... I I f I

DO YOU CONSIDER THE WASTE AS HAZARDOUS?

[I Yes I I No

H form f 10-90/sp I Page 2 PLLRT XI1 - OTHER USES FOR HASTE INDICATE ALTERNATIVE USES FOR THE GENERATED (OTHER THAN DISPOSAL) AND REASONS NOT UTILIZED

PART IV - CEmFIunm "I certify uder penalty of law t§4558.417.1(c), Code of Iowa) that I have personally mxamined and am familiar with the information sdnitted in this docunent concerning hazardous waste, and all attachments, and that, based on my inquiry of those individuals imnediately responsible for obtaining the information. I believe that the information is tcure, accurate, and conplete. I am aware that there are sigrificant penalties for shitting false information concerning hazardous waste, including the possibility of fine and imprisoment." Further, I am aware that the Special Waste Authorization for this waste will be voided if false representation occurs.

TYPED NAME TITLE DATE

d SIGNANRE COMPANY

1-O)(S FOR UBmATORY AWILYUS

, I(ASIIE WLYSIS

1. Perform the Toxicity Characteristic Leaching Procedure test outlined in 40 C.F.R. 261, Appendix 111. Perform the specific cation and anion determinations as specified. Rsport all results in mg/1 of eluate, mg/kg of original sanple. 111 some cases, if there is reason to believe some of the TCLP constituents are not present, the TCLP metals need only be analyzed for. Contact the department prior to deleting the speaific constituents.

2. Provide final pH of TCLP.

5. If a virgin product is being disposed, an HSDS sheet may be sdstituted for the TCLP test. Contact the department for verification.

.. Conduct the paint filter liquids test according to EPA pthlicrtion SW-846, Third Edition, Test bthods for Evaluating Solid Waste.

. Paint, varnish, and stain wastes require a Total Extractable Hydrocarbar test.

?form (10-90/sp) Page 3 542-3216 FOLD

HERE

FOLD

HERE

I I

PLACE STAMP HERE

Environmental Protection Division Iowa Department of Natural Resources Henry A. Wallace Building, 900 East Grand I Des Moines, Iowa 50319-0034 SPECIAL WASTE AUTHORIZATION - Appendix L

Paint Application Methods

Proper Spray Techniques

By far the least expensive to reduce Volatile Organic Compounds (VOC) emissions and material consumption is to practice proper spray techniques. Proper spray techniques can substantially improve transfer efficiency without the purchase of new or special equipment. All that needs to be done is to adjust the present equipment to the proper settings, train the spray operators on proper spraying techniques, and outline a system for maintaining the equipment for maximum efficiency. Supervision is necessary to make sure that spray operators do not slip back into bad habits. Excessive air or fluid pressure, improper distance from the workpiece, improper triggering, and fanning or aiming the spray gun all result in material waste. An operator who uses proper spray technique saves the employer money by using less material, covering the piece in fewer strokes, and creating less overspray which dirties equipment. By using less strokes the operator is not as fatigued at the end of the day. Training inexperienced operators in the use of proper spray techniques is often much easier than retraining operators who have been using bad habits for a long time. Inefficient operators are set in their ways and often feel that new methods slow them down. At first this may be true, but with practice, speed can be increased by using proper techniques. Better quality and consistency is the result of proper spraying techniques.

Fundamentals of Good Spray Technique

The basic fundamentals of good spray technique are: A 50 percent overlap of the spray pattern A distance from gun to workpiece of 6-8 inches A gun speed of approximately 250 ft/min Holding the gun perpendicular to the surface Triggering the gun at the beginning and end of each pass A. 50 Percent Overlap To produce a 50 percent overlap the operator, on his first pass, aims the spray gun nozzle at the bottom edge of the workpiece. On his second pass, the operator aims the nozzle at the bottom edge of the previous pass. In this manner, the workpiece gets a consistent finish with uniform build. If less than a 50 percent overlap is used, the piece will become streaked. If more than a 50 percent overlap is used, then finishing material is wasted and the operator ends up making more passes than necessary to finish the piece.

Figure 1 50 Percent Overlap

B. Gun Distance Gun distance must remain constant. As the gun distance increases, the width of the spray pattern and the thickness of the applied film decreases. A gun distance of more than eight inches usually results in some of the finishing material drying before it reaches the surface. Consequently, the dry finish bounces back from the surface causing excessive material waste or a grainy finish. spray guns should be adjusted for the distance at which they will be used. Spray operators should then maintain that distance.

Figure 2 Gun Distance

C. Gun Speed In order to obtain a consistent finish, one must have a consistent gun speed. Changing the gun speed changes the amount of material being applied. A gun speed that is too high may result in poor aiming, improper gun control, and a distorted spray pattern, all of which add to material loss. High gun speeds may also result in an inadequate film build. In order to obtain the proper buiId, the operator tends to make more passes which add to fatigue. Low gun speeds may result in too much film build causing sags or runs. A generally accepted gun speed is approximately 250 ft/min.

D. Holding the Gun Perpendicular In most cases, the spray gun should be held perpendicular to the surface at all times. There are a couple of reasons for this. First of all, if the gun is arced or fanned, the gun distance is constantly changing, making it very difficult to obtain a uniform finish. In addition, as the gun is arced, the angle of incidence of the spray increases causing the finish material to rebound off the surface.

Figure 3 Results of Not Holding the Gun Perpendicular

LIGHT COVERAGEJ

E. Wggering the Gun The object of finishing is to apply finish to the surface of the piece to be finished. Although this is obvious, it is not at all uncommon to see an operator applying finish to the atmosphere because of poor triggering. If the trigger is not released between strokes, a pile up of finish material occurs at the point where the gun stops when changing directions. To avoid this pile up, the operator extends his stroke past the edge of the piece. In doing this, the operator sprays the atmosphere instead of the piece which results in considerable material loss. The operator that properly triggers the gun spends less time spraying the atmosphere and therefore saves the employer money in material costs. The employer also realizes savings in clean up costs because there is less of a mess from overspray to clean up. Proper triggering includes releasing the trigger at the end of each stroke, having the gun already in motion when the trigger is pulled, and pulling the trigger all the way when spraying. The amount of fluid should be adjusted via fluid pressure and not be triggering. For every piece of furniture there is a best way of finishing it. In order to maximize efficiency, a study of each piece should be made to determine the most efficient way to finish it. This study accomplishes two things. It insures that the least number of strokes are used to finish piece. It also insures that all the pieces are finished in the same manner which provides for consistency.

F. naining Operators 1. Benefits of Formal Training Anyone would agree that a new spray operator would need to undergo some type of training to be able to perform the job. Often this training is done on the shop floor by a co-worker who shows the new operator the proper techniques. ?Raining in this manner is often inefficient. First of all, the trainee may pick up any bad habits that the trainer has. Secondly, the trainer may neglect to convt certain important points. For example, the trainer may not mention something which seems obvious. It may seem obvious tothe trainer but not to the new operator. Finally, this type of training often fails to give the trainee understanding of why proper techniques are important. For these reasons, it is recommended that some type of formal training be implemented. A company can benefit from a formal training program for spray operators in four ways: 1. Reduced finishing material usage/cost. 2. Higher quality finish. 3. Reduced emissions into the atmosphere. 4. Less overspray which means less of a mess to clean. Formal training should include an explanation of the fundamentills of good technique, what good techniques can accomplish and how the operator can benefit by practicing them. Using proper techniques can benefit the operator in two ways. First, it makes the job easier. Through proper techniques the operator can spray the piece faster, using less strokes than if proper techniques were not used. To illustrate, suppose an operator, by using correct technique, can reduce by 5 the number of strokes it takes to finish an article of furniture. If the operator sprays 400 articles a day, 2,000 strokes per day are saved. The second way the operator can benefit is by producing a higher quality finish. In general, people do want to do a good job, and most operators will appreciate the opportunity to produce a better finish. 2. Using Video Equipment to Aid Training Ethan Allen Furniture of Old Fort, North Carolina uses video equipment in their three-week training program. The following case study describes Ethan Allen's training method for spray operators. Ethan Allen's training program consists of 3 stages. In the first week, video tapes are made of each of the operators doing their job. Each tape should be about 15 minutes long. Before . taping begins it is very important to inform the operators what is going on so there are no surprises. This should be done in a positive way so as to get them interested. Often, just knowing that they are going to be on TV gets them interested. During the second week, the operators are taken in groups of three for a one-hour session with the supervisor and technical personnel. Here the tapes are reviewed. Since spray operators are usually very knowledgeable, they can often pick out their mistakes by watching themselves work. Instruction on how to improve spray techniques are also included in this one-hour session. The sessions are followed by instruction in actual production conditions. During the third and final week, the operators are retaped and given a chance compare the two tapes so they can observe first hand what improvements have been made. This training program would be repeated twice per year to reinforce proper technique and to benefit the new employees. Ethan Allen representatives emphasized the importance of using the supplier's technical personnel. They can be very helpful in explaining the proper application of spray gun tips, needles, fluid and air pressure, etc., for all types of guns. Appendix M

NPDES Permit Application Summary - Storm Water

Individual Permits

To receive an individual permit for storm water discharges only, companies must complete Form 1 and Form 2F of the NPDES application process. Companies whose storm water discharges are mixed with other industrial discharges need to complete Form 1, Form 2C, and Form 2E Any new discharge sources of storm water and non-storm water mixtures will require Form 1, Form 2D, and Form 2F to be completed. The NPDES permit approval will depend on the information contained in these forms; the deadline to apply for a NPDES permit under the storm water regulations is May 18, 1992.

Information needed to complete these forms includes, but may not be limited to, the following:

outfall location and receiving waters site drainage maps description of pollutant sources non-storm water discharges significant leaks and spills discharge information biological toxicity test data certification of application accuracy schematic diagrams of processes discharging wastewaters analyses of storm water samples flow measurements or estimates for the amount of storm water discharge during the event used for sampling date and duration of storm event which generated the sample and the amount of time since the last rainfall event where more than 0.1" was generated.

Storm water quantitative data must be based on samples collected during storm events using composite sampling methods. In situations where it is not possible to use an automatic sampler, grab samples of the storm water runoff should be taken every twenty to thirty minutes during the storm event for a period of at least three hours. Specific test parameters include oillgrease, pH, BODS, COD, TSS, total phosphorus, Kjeldahl nitrogen, and nitrite and nitrate nitrogen. A single grab sample may be used for pH, temperature, cyanides, phenols, oiVgrease and fecal coliform analyses. Individual permit application forms can be obtained from the Iowa DNR (800/532-1114) and the IWRC (800/422-3109).

Appendix N

Solid Waste Recyclers

Wood Pallet RebuildersIMfgs.

Andrew Pallet Co., Inc. Hackert Wood Products 190 SE 34th Street RR Des Moines, IA 50317 Richland, IA 52585 5 151266-9604 5151456-2134 Paul and Brian Andrew Ralph Hackert (all of Iowa) Ottumwa Pallet Rebuilders A.M.E Pallet 154 S. Fellows 936 E. Main Ottumwa, IA 52501 Manchester, IA 52057 5151684-5086 3191927-322 1 Robert Wilson Blessing Industries Pal-tech Enterprises Hwy 18, Box 23 P.O. Box 329 West Union, IA 52175 Central City, IA 52214 3191422-6041 319-438- 1006 Denny Andrew Bob Lewis Pallets 424 N. 5th Philips Pallets Chariton, IA 50049 PO Box 65A 5 151774-2549 Keosauqua, IA 52565 Bob Lewis 3191293-2590 Michael M. Philips Chase Manufacturing Co. PO Box 82 Riverside Pallets Luana, IA 52 156 10 Railroad Street 3191539-2400 Riverside, IA 52327 Walt Wedo 3191648-5008 John Hahn Generic Resources DVC (50 mile radius from) PO Box 31 Cantril, IA 52542 319f397-9900 Cecil Hamberg

Genesis Development 115 S. Wilson Jefferson, IA 50129 5151386-3017 Carrie Wilde LDPE Plastics Recycling Companies

Bio-Mass Energy and Recycling 322 N Main Avenue Sioux Center, IA 51250 Virgil Houtkooper, buyer 7121722-0692 Norlyn Van Beek 7121722-3709 (no film)

The Blueberry Patch, Ltd. 453 Tonawnda Dr. Des Moines, IA 50312 PCL & Eastern New Brunswick, Canada Tom Millar

Plastic-Cyc 4623 S 28th Street Omaha, NE Richard Arms 402173 1-5580 (from DNR guide)

Upnorth Plastics PO Box 127 9480 Jamaica Ave. S. Cottage Grove, MN 55016 7151682-8326 8001544-7659, ext. 238 Don Lee HDPE Plastic Recycling Companies

Bancher Products Ltd. Iowa Plastics 1515 N. Harlem 322 N. Main Oak Park, IL 60302 Sioux Center, IA 51250 3121848-8020 7121722-0690 Virgil Houtkeeper Century Plastic (M) Box 51 Main Plastics (P)(B) Hayfield, MN 55940 2600 Commonwealth Ave 5071447-3232 Chicago, IL 3121473-3553 CC & C Recycling (MidAmerica Recycling & Container Recovery) Mason City Recycling (B) 2744 SE Market 1410 S. Monroe Des Moines, IA 50317 Box 1534 5151265-0889 Mason City, IA 50401 Mick Barry 5151423- 1200 Dean Hess Eaglebrook Plastics (P)(M) 2600 W. Roosevelt Rd. Midwest Plastics (P)(M) Chicago, IL 60608 811 Collins Rd. 3121638-0006 Stoughton, WI 53589 3121473-3553 FDA Plastics (P)(B) 2001 N. 22nd St. #966 NCS Plastics Decatur, IL 1210 9th St. SW 2 171429-3373 Cedar Rapids, IA 52404 3191363-2112 Generic Resources, DVC Route 1 N.E.W. Polymers (M) Cantril, IA 52542 Box 220,112 Fourth 3191397-9900 (all plastics) Luxemberg, WI 54217 4141845-2326 Genesis Development 115 S. Wilson North Central MO Plastics Recycling Jefferson, IA 50129 Box 196 5151386-3017 Spickard, MO 64679 8161485-6299 Graggs Plastics (broker) Bill Coon RR 3 Bolckow, MO 64427 NUCON Corp. (M) 8161428-2201 540 Frontage Road MarWRobert Gragg Northfield, IL 60093 3121446-6777 Polymer Products (M) Sherman Co. RR #3, Box 182 6101 W. Dickens Iowa Falls, IA 50126 Chicago, IL 60639 515/648-5073 312/637-6400

Rubbermaid (M) Upnorth Plastics RR 1, Industrial Park PO Box 127 Centerville, IA 52544 9480 Jamaica Ave. S. 5151437- 1000 Cottage Grove, MN 55016 Jim Wesch 7151682-8326 800/544-7659, ext 238 Samuels, H. Co., Inc. P.O. Box 8800 Madison, WI 53708 608/241-7191

Code: (M) = Manufacturer (P) = Processor (B) = Broker PET Plastic Recyclers

CC & C Recycling Home Metal Recyclers (MidAmerica Recycling & Container 200 32nd St SE Recovery) Cedar Rapids, IA 52403 2744 SE Market 3191365-1620 Des Moines, IA 50317 (515)265-0889 Industrial Recycling 6305 11th Street SW Cimino Recycling Co. Cedar Rapids, IA 52404 201 SE 6th St. 3191365-0741 Des Moines, IA 50265 (515)243-1696 Mason City Recycling (broker) 1410 S. Monroe Container Recovery Inc. Box 1534 1700 E. Aurora Ave. Mason City, IA 50401 Des Moines, IA 50313 515/423-1200 (515)265-4275 Dean Hess Approximately 1,000,000 Ibs. PETlyear MCR Polymers, Inc. Genesis Development 1716 W. Webster 115 S. Wilson Chicago, IA Jefferson, IA 50129 5151386-3017 National Container Services Carrie Wilde or Cindy Boyd 1210 9th St. SW Cedar Rapids, IA 52404 Goodwill Industries (319)363-2111 Blairs Ferry Rd. Cedar Rapids, IA 52404 (319)393-3434 Approximately 500,000 lbs. PETlyear

Graggs Plastics (broker) RR 3, Box 115 Bolckow, MO 64427 8161428-2201 Mark Gragg PVC Plastic RecyclerdProcessors

H. Heller Co. First Federal Plaza, Suite 904 701 Adams St. Toledo, Ohio 43624 419/423-8211

Ralco Industries 1112 River St., PO Box 509 Woonsocket, Rhode Island 02895 40 1/767-2700

Reprocessing Plastic Co., Inc. 2950 Arkin Ct. Denver, Colorado 80216 303/294-0364

Shurnan Plastics 35 Neoga St. Depew, New York 14043 716/685-2121 (Bruce Gilburne) Paper Recyclers/Collectors

Alter Trading Corporation Cass Co. Solid Waste Commission 180 Harrison Street Route 4, Box 183 Dubuque, IA 52001 Atlantic, IA 50022 3191583-1731 7121243-5024 Bob Blazejewski Bill Hogueison

Area Recyclers Cedar County Workshop, Inc. 1104 Agency 401 West 9th St., Box 364 Burlington, IA 52601 Tipton, IA 52772 3191753-8126 3191886-6044 Kathy Lewis Best Recycling 201 SE 6th St. Central Paper Stock Co. Des Moines, IA 50309 1430 Macklind Ave. 515/243-1696 St. Louis, MO 63110 Bill Best or Tom Mihalovich Bud Kushins High grade white & colored paper, cardboard, & 3141781-3369 paperboard; pick up in DM metro area (500# minimum); 8001451-6646 drop-off at facility from Mon-Sat. Fax: 314781-6357 Corrugated boxes, brochures, catalogs, poly-coated board, Blessing Industries white & colored paper, some old newspapers and phone Hwy 18, Box 23 books, paperboard & coated paper, baled & nonbaled paper; West Union, IA 52175 provide gaylords. 3191422-6041 Blaine Blessing Champion International Main Street CC & C Recycling Keokuk, IA 52632 (also MidAmerica Recycling and Container Recovery) 3191524-5622 2744 SE Market W.W. Land Des Moines, IA 50317 515l265-0889 Cimino Recycling Co. Mick Barry 201 SE 6th St. All types of paper, including coated - not phone books; pay Des Moines, IA 50265 & pick-up when economically feasible; any quantity 5151243-1696 delivered; also takes color-sorted glass and PET and HDPE Bill Best plastics. City Carton Company, Inc Capitol Oil Company 1415 Dunkerton 729 S. Capitol, #408 Cedar Falls, IA 50613 Iowa City, IA 52244 3191277-3464 3191338-8136 Ron Dornath Richard Strauss City Carton Company, Inc. Carnation Paper Prod. 402 Harvey P1. 1305 Thomas Beck Rd. Mt. Pleasant, IA 52641 Des Moines, IA 50315 3191385-7206 5151244-4458 Tim Ockenfels Charles Meade City Carton Company, Inc. Carroll Enterprise Systems 917 S. Clinton Street 314 East 5th Street Iowa City, IA 52240 Carroll, IA 51401 3191351-2848 7121792-6713 John Ockenfels Dave Sterns City Carton Carton, Inc. GeraldISandy RedemptionfRecycle 4250 6th St. SW Highway 18 Cedar Rapids, IA 52404 Clermont, IA 52135 319A65-8659 3191423-7109 Andy Ockenfels GeraldISandy

Consolidated Packaging Corp. Grainek-Dunitz Co. PO Box 250 P.O. Box 246 Fort Madison, IA 52627 Newton, IA 50208 319B72-3152 5151792-7218 John Huprich Max Grainek

Distinctive Packaging Handicap Village Work Center 520 S. 18th St. 1200 North 9th Street West West Des Moines, IA 50265 Clear Lake, IA 50428 515t223-5560 5151357-5277 Joe Lane, Jr. Alan Marken

Dodd's Trash Hauling & Recycling Humboldt Workshop Route 3, Box 456 21 North Taft Newton, IA 50208 Humboldt, IA 50548 5151791-9195 5151332-2841 Davehiz Dodd Curk Dufield

Durbin Paper Stock Inc. J & S Recycle Paper Co. 1539 Rockingham Rd. 840 Cleveland Avenue Davenport, IA 52802 Keokuk, IA 52632 319B23-4909 3191524-6443 Bill Ellis Joe Scott Lee Co. SW Commission Ecology Control Corp. RR #1, Box 16 1000 E 12th Street Fort Madison, IA 52627 PO Box 713 3191372-6140 Dubuque, IA 52004 Ron Mace 3191588-7171 Key Recycling Center Environmental Recycling Company 1711 West 2nd Street South Loomis Avernighway 34 West Webster City, IA 50595 Corning, IA 50841 5151832-5516 Dwight Oglesbee 515l322-3222 Mason City Recycling Corrugated cardboard; other 1410 S. Monroe Box 1534 Genesis Development Mason City, IA 50401 115 S. Wilson 5151423-1200 Jefferson, IA 50129 Dean Hess 515l386-3017 Newspapers, cardboard, & high grade papers; Manufactures Carrie Wilde or Cindy Boyd cellulose insulation from newspapers; pick-up throughout Paper and corrugated cardboard from anyone who will drop Iowa. Prefers 10 - 20 tonlpick-up. it off and will pick up within a 50 mile radius. Packaging Corp of America Georgia Pacific P.O. Box 117 823 N. Cedar Tama, IA 52339 Monticello, IA 52310 5151484-2884 3 191465-3543 Jerry Brink D. Bohliren Paper Stock of Iowa Inc. R-Business Recyclers, Inc. 2308 Sunset Rd, 1284 Box 2706 Des Moines, IA 50305 Waterloo, IA 50704 515l243-3156 3191236-1344 L. Pomerantz Jim O'Regan

Paper Recovery Corp. Recycle Iowa, Inc. 1191 Engleside Drive 700 West Griemes, box 2042 Cedar Rapids, IA 52404 Fairfield, IA 52556 319B64-5572 Jim Ledenbach Sanitary Wiping Cloth Co. 2308 Sunset Road PECO Enterprises PO Box 1284 320 LeClaire Des Moines, IA 50305 Davenport, IA 52801 5151243-3156 319B23-4774 Don McCregor Frank Grantas Scott County Landfill Polar Insulation P.O. Box 563 P.O. Box 81 Buffalo, IA 52728 Muscatine, IA 52761 3191381-1300 319l263-7105 Cindy Turkle James Reynold Skyline Center, Inc. Pollock Equipment 2600 North 4th Street RR 1 Clinton, IA 52732 Denison, IA 51442 3191243-4065 712l263-5346 Jack Robinson

Progress Industries Spread-All Mfg. Co. 1017 East 7th St. North, Box 366 P.O. Box 191 Newton, IA 50208 Marshalltown, IA 50158 5151792-6119 5151753-5601 John Bartello John Maddick

Quality Insulation Mfg. Waldorf Corp 1930 Easton Blvd. 2250 Wabash Ave. Des Moines, IA 50316 St. Paul, MN 55114 515l266-2677 6121641-4725 Betty South Dick Johnson Corrogated, news and ledger stock; pick-up east of 1-35, Randy Lilleholm including SE Iowa. 35,000# minimum required. Rt. #1, PO Box 321 Denison, IA 51442 712l263-3310 Newspaper, will pick up in the Denison area or accept drop off. Paper used for livestock bedding.

Appendix 0

Air Permit Application

-.- TERRY E. BRANSTAD. GOVERNOR DEPARTMENT OF NATURAL RESOURCES

:g.:.:. .=x.:I J AIR QUWSECTlON .:.:. \y APPLICATION TO INSTALL OR ALTER DNR USE EQUIPMENT OR CONTROL EQUIPMENT Permit Number Read Instructions on Reverse Plant Number

APPLICANT Telephone Number ( 1 8 g 1 2 y$ :::$ &::::$ Firm Name Person to Contact $$ ....,. >. 8... 3 Mailing Address City State Zip Code :.:.: .:.:.:.:.:

( )New ( ) Modification

5 TYPe 6a. 6b. (Ibslhr) (tonslyear) 7 Production Capacity Make and Model

POLLUTlON CONiROL EQUIPMENT 9 :.:.. 9 10 :;:> .....$8 Start Date Completion Date f:# Type Construction Schedule ..... i:) 11 12a 12b :+: $ Make and Enode! Efficiency % Air Flow Rate(scfm) ::::: ...... $j 13a 13b 13c :A: :A. ... Actual Before Control Actual After Control Requested Permit Limit

1 15 ( 1 if: Name Date Title Telephone Number ::::. :.:...... Signature :.:...... I am the owner or owner's employee responsible for this installation. MI *lop

WAUACE STATE OFFICE BUILDING I DES MOINES, IOWA 50319 / 515-281-5145 I TDD 515-242-5967 1 FAX 5152818895 . , APPLICATION INFORMATION

CONTACT FOR INFORMATION ,

Environmental Protection Division Department of Natural Resources Wallace State Office Building Des Moines, lowa 50319 Phone: 5152818924 or 281-3499

BASIC INFORMATION

The owner of the equipment is responsible for obtaining the permit.

A permit, from this Department, is required for equipment th& is capable of emitting air contaminants. Starting construction, before obtaining this permit, Is a violation of section 455B.134a.. Code of lowa

A separate application for a permit is required for each vent or discharge to the atmosphere. However, one application can cover an entire system consisting of a number of separate pieces of basic process equipment, so long as there is only one point of discharge to the atmosphere.

FILLING AN APPLICATION FOR A PERM2 -. . -. Incomplete or illegible applications will be returned to the applicant A complete application consists of the application form (form 6) with all items completed plus the required attachments listed below. Submit application in duplicate. to this Department at the address shown above. REQUIRED ATTACHMENTS

1. A written description and process flow diagram of the system for which application is being made. The flow diagram shall clearly identify process quantities and air exhaust rates.

2. Final engineering plans and specifications. (drawings of the proposed system)

3. Manufacturer's catalog data for the pollution control equipment. (identify equipment used in catalog)

4. Engineering design or selection calculations.

5. Location and plot plans showing the distances to and heights of nearby buildings, adjacent streets and properties, location and elevations of the emission point(s). The drawing shall also locate any fences, and identify type, along property boundaries.

6. The composition of the exhaust stream, both before and after any'control equipment, with stack exhaust rate (scfm) and temperature, stack diameter, height, emission rate (Iblhr) and in-stack concentrations of each contaminant.

7. The chemical and physical characteristics of the air contaminants.

8. Details for sampling port locations. access platforms, and other associated facilities.

9. Identification of any control equipment that is to be replaced.

10. Projected operating schedule: hourslday. dayslweek. weekstyear.

11. For a medical waste incinerator: A listing of all off-site waste generators to be served by the incinerator and the maximum quantity, on an hourty basis, of off-site waste to be incinerated.

12. Complete the information requested on permit application Form 6. (ltems.1 through 15)

13. Prevention of Significant Deterioration (PSD) applicability determination including, but not limited to, identificationand quantification of emissions from all sources, plant-wide, for the following: total suspended particulates, particulate matter sized up to 10 microns (PMlO), sulfur dioxide, carbon monoxide, nitrogen oxides, volatile organic carbons, ozone and lead. See 40 Code of Federal Regulations 52.21 (i). tf PSD applies:

13a. PSD Best Available Technology List of All Available Control Technology Technical Feasibility Evacuation Energy Impact Analysis Table of Available Control Technologies Environmental Impact Analysis Economic Impact Analysis

13b. PSD Air lmpact Analysis Impact Area Determination Emissio~sInventory Existing Air Quality Projected Air Quality Increment Consumption Screening Analysis

13c. PSCY Addition Impacts Analysis Visibility Vegetation and Soils Associated Growth

14. Prepare and submit a detailed computer-aideddispersion evaluation.of the air contaminants for the proposed new emission unit and all existing emission units. Groundlevel values will be compared to the national ambient air quality standards. m 11.a.91 To complete the application, the following checklist items should be completed:

Checklist Item 1 Description of the process being exhausted (i.e. spray painting, welding, etc.). Type of exhaust system used (i.e. down draft booth, ceiling fan, etc.) and a hand drawn flow diagram of the system to be permitted. Stack air exhaust rate (may be found in manufacturer's specifications). Estimates of the amount of material used in the process (i.e. gallons of paint per month).

Checklist Item 2 Composition of exhaust stream specifically looks for the six criteria pollutants which include NOx, SOx, CO, Pb, 03, PM-10, and other particulates, and Volatile Organic Compounds (VOC1s). Type of control equipment used and estimated effectiveness (e.g. dry paint booth filters are use. They are 95% effective in removing particulate). Stack exhaust temperature (about 70°P for unheated processes. Stack air exhaust rate (already done in Checklist Item 1). Stack diameter (may be found in manufacturers specifications). Estimates of emission rates (lbslhr). This can be estimated from Material Safety Data Sheets (MSDS) or knowledge of the material being discharged. The IWRC can assist in estimating emission rates.

Checklist Item 3 The chemical and physical characteristics of the air contaminants may be found on MSDS for materials being discharged if the material does not undergo a chemical change (i.e. painting). If the material does undergo a chemical change (i.e. welding fumes) the IWRC can be contacted for assistance.

Checklist Item 4 Explain basis for using chosen equipment design, and pollution control equipment (Example: "Spray booth was chosen based on recommendations of manufacturer after evaluating shop layout and type of painting to be done to achieve maximum suitable design standards. Spray booth filter media was chosen based on recommendations of supplier of paint to be sprayed, and an evaluation of the efficiency of particulate removal of the filter media").

Checklist Item 5 Complete engineering plans showing design, installation and specifications of system. If this does not exist provide written description showing equipment was designed to meet standard and accept operating characteristics for that type of equipment. (Example: "The paint booth was designed to be incorporated into the current facility structure while providing a booth, hood, and fan to allow an air flow of 100-150 fWmin velocity across the face of the spray application to within a 60 fWmin cross draft").

Checklist Item 6 If you use pollution control equipment and have a manufacturer's catalog, photocopy the page. If you don't have a catalog, contact the manufacturer and request one.

Checklist Item 7 Self explanatory Checklist Item 8 This applies only to companies that have reason to believe monitoring may be necessary.

Checklist Item 9 Indicate what, if any, existing control equipment will be replaced.

Checklist Item 10 Indicate, using best apprmimation, the operating schedule that is currently used or will be used.

Checklist Item 11 Applies only to medical waste incinerators.

Checklist Item 12 Complete enclosed application (Form 6).

Checklist Item 13 Indicate if process already exists or date when construction begins (Example: "Booth construction was completed in 1977").

Checklist Item 14-18 This applies to companies that emit more than 100 tons per year of air pollutants, so for most it may be disregarded. If in doubt, please contact the IWRC at 3191273-2079 Appendix P

Counting Hazardous Waste When Using a Solvent Still

Solvent Waste Generation from Recycle Activities

Even though still "bottoms" are generally considered hazardous wastes, the overall hazardous waste generation rate is drastically reduced by recycling in-house. In the following example we will see how the monthly hazardous waste generation rate has been reduced by 75% through use of a solvent recycling unit, and how to determine the calendar month generation rate.

Week 1: 10 gallons of new solvent are used to clean gun lines and other equipment. On Friday, the spent solvent is placed in the still and recycled. Nine gallons are recovered as clean solvent while one gallon of still bottoms is collected. The hazardous waste generated so far is ten gallons (the original ten gallons which was spent and needed to be recycled).

Week 2: Nine gallons of cleaned solvent is mixed with one gallon of new solvent so that again we have ten gallons of solvent for the week. On Friday, the spent solvent is placed in the still and recycled. Nine gallons are recovered as clean solvent while one gallon of still bottoms is collected. The TOTAL hazardous waste generated so far is eleven gallons (the original ten gallons plus the one new gallon which became spent during the week).

Week 3: Same as week 2; the TOTAL hazardous waste generated so far is now twelve gallons.

Week 4: Same as weeks 2 and 3; the TOTAL hazardous waste generated in four weeks (one month) is now thirteen gallons.

NEW MONTH

Week 5: Same as week 1; week 5 is part of another calendar month and the original amount of spent solvent generated (ten gallons) must be counted EACH month.

Week 6: Same as week 2 (total eleven gallons)

Week 7: Same as week 3 (total eleven gallons)

Week 8: Same as week 4 (total eleven gallons)

By recycling on-site, the hazardous waste generation rate per calendar month is reduced from 40 gallons to 13 gallons. Plus, only 4 gallons of still bottoms are collected for off-site disposal.

Appendix Q

SARA Title III Reporting Instructions

SARA Title 111 - Emersencv Notification, Section 304

Facilities must immediately notify the State Emergency Response Commission (SERC):

State Emergency Response Commission (SERC) Grimes State Office Building Des Moines, IA 50319 515/281-6175

Local Emergency Planning Committee (LEPC):

and the Department of Natural Resources (DNR):

within 6 hours if there is a release of a listed hazardous substance that exceeds the reportable quantity (RQ) for that substance. The applicable lists of substances and associated RQ's are:

Extremely Hazardous Substance List (Attachment EHS) CERCLA Hazardous Substance List (Attachment CERCLA)

Step by step guidance to determine if release reporting is necessary under the Emergency Notification requirements is enclosed as Attachment EN.

SARA Title I11 - Community Riqht-to-Know, Section 311 and 312 Reporting

a. Any business or industry, regardless of size or number of employees, that stores or uses hazardous chemicals (as defined by Occupational Safety and Health Administration-OSHA) at anyone time in excess of designated thresholds (see 2).

b. Hazardous chemicals are those materials for which a Material Safety Data Sheet (MSDS) is required in the workplace.

c. Five exemptions from reporting requirements are:

A food additive regulated by Food and Drug Administration (FDA).

A solid (such as steel) that does not present a hazard under normal conditions. The solid is included if it is used in a manner (e.g. cutting, welding, grinding) that creates exposure to hazards.

A substance used for personal, family, or household purposes. Also, a material used by business that is in the same form (i.e. packaged for home use) and concentration as a material sold to the general public is exempt. Substances used in research labs, hospitals, or medical facilities under the direct supervision of a technically qualified individual.

Any substance used in routine agricultural operations, or any fertilizer held for sale by a retailer.

2. Thresholds

a. Reporting thresholds have been established for 1987 and 1988.

b. A hazardous substance present (at any time) above the threshold amount must be reported.

10,000 pounds is the reporting threshold for 1987 and 1988.

Reporting thresholds for 1989 and after have been proposed as 10,000 pounds by the Environmental Protection Agency (EPA).

c. An extremely hazardous substance present at any time above 500 pounds or the threshold planning quantity (whichever is less) must be reported. See Attachment EHS for these substances and threshold amounts.

3. Deadlines

a. Reporting deadlines are summarized in Attachment 311-312. -. b. MSDS's must be submitted on October 17, 1987; October 17, 1989; or three months after an MSDS is needed for a hazardous substance present above the threshold amount.

c. Tier I1 forms are due annually on March 1 for the preceding year. 4. MSDS Reporting

a. MSDS reporting for hazardous substances present above threshold amounts can be satisfied by a onetime submission of a list of MSDS's, or copies of the MSDS's.

b. MSDS's, or the MSDS list, are sent to the State Emergency Response Commission (SERC), Local Emergency Planning Committee (LEPC), and local fire department.

c. Copies of MSDS on file at your facility can be sent to fulfill the MSDS reporting requirement or

d. A list of all hazardous substances present above threshold levels. The list must include, for each entry:

The chemical or common name as stated on the MSDS.

Any hazardous component(s) listed on the MSDS. - The hazardous substances must be grouped by hazard category. e. Step by step guidance is enclosed as Attachment CR.

5. Tier I1 Reporting

a. Tier I1 reporting must be done on the Tier I1 form (Attachment TII).

b. The completed form is sent to the SERC, LEPC, and local fire department.

c. Step by step guidance is enclosed as Attachment CR.

6. State Emergency Response Commission (SERC)

a. The SERC is located at:

State Emergency Response Commission Grimes State Office Building Des Moines, IA 50319 515/281-6175

7. Local Emergency Planninq Committees (LEPC)

a. The LEPC is located at:

a. Fines for non-compliance with reporting requirements can be up to $25,000 per day.

SARA Title I11 - Toxic Chemical Release Reporting, Section 313 1. Applicability

a. Facilities with ten (10) or more full time-time employees in Standard Identification Code (SIC) 20-39.

2. Threshold

a. Manufactured or processed substances on the Section 313 Toxic Chemical List (Attachment TCL) in excess of 25,000 pounds.

b. Otherwise used 10,000 pounds of Section 313 Toxic Chemical List substances.

3. Deadlines

a. Reporting is due July 1, 1989 for the proceeding calendar year. 4. Reportinq

a. Section 313 reporting must be done on the R form (Attachment R).

b. The completed form must be sent to the US EPA and SERC.

c. Step by step guidance is enclosed as Attachment TC.

5. United States Environmental Protection Agency (USEPA)

a. US Environmental Protection Agency Attn: Toxic Chemical Release Inventory P.O. Box 70266 Washington, DC 20024-0266

State Emerqency Response Commission (SERC)

a. State Emergency Response Commission Grimes State Office Building Des Moines, IA 50319 Attachment EN

Section 304 - Emergency Notification

1. Spill into the environment that could affect persons or resources outside facility boundary..

2. Initiate personnel evacuation, containment, and clean-up as appropriate.

3. Identification of spilled material and quantity (pounds).

4. Identification of hazardous ingredients in spilled material (i.e. from MSDS) and quantity (pounds) of each hazardous ingredient. Example - Material spilled - XYZ Paint

Quantity - 500 gallons x density (i.e. 10 pounds/gallon) = 5,000 pounds Concentration of Weight of ingredient in ingredient in spilled product spilled product Hazardous Ingredients - Formaldehyde 10% 500 pounds Benzene 50% 2,500 pounds Lead 20% 1,000 pounds

5. Compare list of ingredients with Extremely Hazardous Substance (EHS) (Attachment EHS) and CERCLA (Attachment CERCLA) lists

Example: Formaldehyde is on the EHS list Benzene is on the CERCLA list Lead is on the CERCLA list

6. Compare weights of spilled ingredients with the EHS and CERCLA lists Reportable Quantities (RQ)

Example: Formaldehyde RQ = 1,000 pounds Benzene RQ = 1,000 pounds Lead RQ = 1 pound

7. If weights spilled exceed the EHS and CERCLA lists' RQ Notification, the following is required: State Emergency Response Commission (SERC) - 515/281-6175 Local Emergency Planning Committee (LEPC) - usually the local fire department. Department of Natural Resources - 515/281-8694

Example: Formaldehyde spilled = 500 pounds which is less than RQ of 1,000 pounds - Notification not Required

Benzene spilled = 2,500 pounds which is greater than RQ of 1,000 pounds - Notification Required

, Lead spilled = 1,000 pounds which is greater than RQ of 1 pound - Notification Required 8. Written update required to the SERC and LEPC including:

a. Type of material spilled b. Quantity spilled c. Quantity estimated to have been released to the environment d. Time and duration of spill e. Whether the spill occurred into the air, water, and/or land f. Anticipated health affects and advice regarding medical attention for exposed individuals. g. Precautions and clean up actions taken h. Name and telephone number of contact person Attachment 311-312

Title 111 Reporting Deadlines

Manufacturing Non Manufacturing

-MSDS Tier I1 -MSDS Tier I1 1987 October 17*

March 1 September 24 * (for 1987)- 1989 October 17** March 1 - March 1 (for 1988)* (for 1988)*

1990 - March 1 September 24** March 1 (for 1989)** (for 1989)** March 1 - March 1 (for 1990)** (for 1990)**

Three months Three months after an MSDS after an MSDS is needed for a is needed for a hazardous substance hazardous substance present above the present above the threshold amount. threshold amount.

* Reporting threshold 10,000 #. ** Reporting threshold to be established (proposed to remain at 10,000 #).

Attachment CR

Section 311 - 312 Comnity Right to Know

1. Obtain Material Safety Data Sheets (MSDS) and inventory data for -all products stored at your facility during the previous calendar year.

2. Prepare a worksheet listing each product for which a MSDS was supplied, maximum volume stored on-site at any one time, the MSDS listed hazardous ingredients and concentration, and finally the weight in pounds for each hazardous waste ingredient.

Example: Worksheet 1

1 2 3 4 5 Product Maximum Volume MSDS listed Concentration Maximum and On-Site at any Hazardous o f On-Site Density Given Time Ingredients Ingredient Weiaht

XYZ Paint 10 pounds/gallon 2,000 gal. Formaldehyde 10% 2,000 Benzene 50% 10,000 Lead 20% 4,000 XYZ Thinner 7.5 pounds/gallon 50 gal. Benzene 90% 340

Column 5 calculation - Product density x Column 2 x Column 4 / 100

Example: 10 pounds/gallon x 2,000 gallons x 10 / 100 = 2,000 pounds for Formaldehyde

3. Prepare a worksheet listing each hazardous ingredient and the total (combined) weights for each.

Example: Worksheet 2

Hazardous Ingredient Total maximum on-site (pounds)* Formaldehyde Benzene Lead * Total of column 5 weights for each individual chemical on worksheet 1

4. Compare your worksheet 2 hazardous ingredient with those chemicals listed on the Extremely Hazardous Substances (EHS) list (Attac-bentEHS).

~xample:' Formaldehyde is on the EHS list

5. Compare weights of worksheet 2, EHS ingredients, with the EHS threshold planning quantity (TPQ) or with 500 pounds, which ever is less.

Example: Formaldehyde total = 2,000 pounds EHS TPQ is 500 pounds for Formaldehyde 6. If the EHS ingredient is greater than the TPQ or 500 pounds (whichever is less) reporting required.

7. If the EHS ingredients is less than the TPQ or 500 pounds (whichever is less) reporting is not required.

8. Compare weights of non-EHS ingredients on worksheet 2 with 10,000 pounds.

9. If non-EHS ingredients exceed 10,000 pounds reporting required.

10. If non-EHS ingredients do not exceed 10,000 pounds reporting is not required.

11. Section 311 Rewortinq Copies of MSDS which contain ingredients determined to be reportable in steps 6 and 9, or

A list of all hazardous substances determined to be reportable in steps 6 and 9. The list must group the substances by hazard class.

The MSDS or the list of hazardous substances must be submitted to:

State Emergency Response Commission (SERC) Grimes State Office Building Des Moines, IA 50319 515/281-6175

Local Emergency Planning Committee (LEPC) (Contact and address may be obtained from the SERC or through the Iowa Waste Reduction Center (IWRC) at 319/273-2079

Local Fire Department

12. Section 312 Re~ortinq

Reporting for Section 312 requirements comprise the same chemicals and threshold levels as Section 311. Unlike Section 311, reporting must be done annually (by March 1, for the previous calendar year). Section 312 requires reporting on a standard inventory form (Tier I1 form) enclosed as Attachment TII. Submittal of the annual form is as described in the Section 311 summary (i.e. SERC, LEPC, and local fire department.) Attachment TC

Section 313 - Toxic Chemical Release Reporting 1. Obtain Material Safety Data Sheets (MSDS) and inventory/procurement data for all products used at your facility for the previous calendar year.

2. Prepare a worksheet listing each product for which a MSDS was supplied, maximum volume used during the year, the MSDS listed hazardous ingredients, and concentration, and finally the weight in pounds for each hazardous waste ingredient.

Example: Worksheet 3

Product Annual MSDS listed Concentration Annual and Volume Hazardous of use Density Used Inqredients Ingredient (pounds)

XYZ Paint 10 pounds/gallon 9,000 gal Formaldehyde 10% 9,000 Benzene 50% 45,000 Lead 20% 18,000

XYZ Thinner 7.5 pounds/gallon 500 gal Benzene 90% 3,375

3. Prepare a worksheet listing each hazardous ingredient and the total (combined) weights for each.

Example: Worksheet 4

Hazardous Ingredient Total Annual Use (pounds)

Formaldehyde Benzene Lead

4. Compare your worksheet 4 hazardous ingredients with those chemicals listed on the Section 313 Toxic Chemical list (Attachment TCL).

Exgmple: Formaldehyde is on the toxic chemical list Benzene is on the toxic chemical list Lead is on the toxic chemical list

5. Compare weights of your listed hazardous chemicals from worksheet 4 with 10,000 pounds (otherwise used threshold).

6. If your listed chemical exceeds 10,000 pounds, reporting required.

7. If you listed chemical does not exceed 10,000 pounds, reporting is not required.

Example: Formaldehyde total = 9,000 pounds Benzene = 48,375 pounds Lead = 20,000 pounds

Benzene and lead exceed 10,000 pounds and therefore must be reported, formaldehyde reporting is not required. 8. Section 313 Reporting

Report data must be submitted on US EPA form R, a copy of which is enclosed as Attachment R. Submittal is due July 1 for the previous year. Completed forms shall be forwarded to: U.S. Environmental Protection Agency I Attn: Toxic Chemical Release Inventory P.O. Box 70266 Washington, DC 20024-0266

State Emergency Response Commission (SERC) Grimes State Office Building Des Moines, IA 50319 515/281-6175

If the above steps indicate that you must submit Form R under the SARA Section 313 requirements, the IWRC will assist you in completing the form, based on worksheet 3 and 4 data. THE LIST OF EXTREMELY HAZARDOUS SUBSTANCES AND THEIR THRESHOLD PLANNING QUANTITIES Threshold Reportable CAS No. Chemical name [Trade Name] planning quantity quantity (pounds) (pounds)

Acetone Cyanohydrin Acetone Thiosemicarbazide Acrolein Acrylamide Acrylonitrile

Acrylyl Chloride Adiponitrile Aldicarb [Temik] Aldrin Ally1 Alcohol

Allylamine Aluminum Phosphide Aminopterin Arniton Arniton Oxalate

Ammonia Amphetamine Aniline Aniline, 2,4,6-Trimethyl Antimony Pentafluoride

197-94-0 Anitmycin A 86-88-4 ANTU )03-28-2 Arsenic Pentoxide 127-53-3 Arsenous Oxide '84-34-1 Arsenous Trichloride

184-42-1 Arsine ,42-71-9 Azinphos-Ethyl [Ethyl Guthion] 86-50-0 Azinphos-Methyl [Guthion] 98-87-3 Benzal Chloride 98-16-8 Benzenamine, 3-(Trifluoromethy1)-

.OO-14-1 Benzene, 1-(Chloromethy1)-4 Nitro- 500/10,000 1 98-05-5 Benzenearsonic Acid 10/ 10,000 1 115-21-2 Benzimidazole, 4,s-Dichloro-2-(Trifluoromethy1)- 500/10,000 1 98-07-7 Benzotrichloride 100 1 00-44-7 Benzyl Chloride 500 100

Note: When two TPQ's are given, the lower is for the powdered form of solid; higher quantity for non-powdered form. Threshold Reportah CAS No. Chemical name [Trade Name] planning quantity quantitl' (pounds) (pounds Benzyl Cyanide 500 1 Bicyclo[2.2.1]Heptane-2-Carbonitrile, 5-Chloro-6((((Methylamino)Carbonyl)Oxy)Iino)-, (Is-(1-alpha, 2-beta, 4-alpha, 5-alpha, 6E))- 500/10,000 l1 Bis(Chloromethy1) Ketone 10/10,000 1 litoscanate 500/10,000 1 boron Trichloride 500 1 Boron Trifluoride 500 Boron Trifluoride Compound w/ Methyl Ether(1:l) 1,000 Bromadiolone 100/10,000 Bromine 500 Cadmium Oxide 100/10,000 Cadmium Stearatc Calcium Arsenate Camphechlor Cantharidin Carbachol Chloride Carbamic Acid, Methyl-, 0-(((2,4-Dimethyl-1, 3-Dithiolan-2-y1)Methylene)Amino)- 100/10,000 1 Carbofuran [Furadan] 10/10,000 10 Carbon Disulfide 10,000 100 Carbophenothion 500 1 Chlordane 1,000 1 Chlorfenvinfos Chlorine Chlormephos Chlormequat Chloride Chloroacetic Acid Chloroethan01 Chloroethyl Chloroformate Chloroform Chloromethyl Ether Chloromethyl Methyl Ether Chlorophacinone 100/10,000 1 Chloroxuron 500/10,000 1 Chlorthiophos 500 1 Chromic Chloride 1/10,000 1 Cobalt, ((2,2'-1,2-Ethanediylbis (Nitrilomethylidyne))Bis(6-Fluorophenolato)) (2-)- N,N',0,O1)- 100/10,000 1 Threshold Reportable CAS No. Chemical name [Trade Name] planning quantity quantity (pounds) (pounds) 1210-68-1 Cobalt Carbonyl 10/10,000 1 64-86-8 Colchicine 10/10,000 1 56-72-4 Coumaphos 100/10,000 10 j836-29-3 Coumatetralyl 500/10,000 1 95-48-7 Cresol, o- 1,000/10,000 1,000

535-89-7 Crimidine 1170-30-3 Crotonaldehyde 123-73-9 Crotonaldehyde, (E)- 506-68-3 Cyanogen Bromide 506-78-5 Cyanogen Iodide

1636-26-2 Cyanophos 675-14-9 Cyanuric Fluoride 66-81-9 Cyc loheximide 108-91-8 Cyclohexylamine 702-41-9 Decaborane(l4)

1065-48-3 Demeton 919-86-8 Demeton-S-Methyl 1311-84-9 Dialifor 1287-45-7 Diborane 111-44-4 Dichloroethyl Ether

149-74-6 Dichloromethylphenylsilane 62-73-7 Dichlorvos 141-66-2 Dicrotophos 464-53-5 ~iepckybutane 814-49-3 Diethyl Chlorophospate

642-54-2 Diethylcarbamazine Citrate 71-63-6 Digitoxin 238-07-5 Diglycidyl Ether 830-75-5 Digoxin 115-26-4 Dimefox

60-51-5 Dimethoate 524-03-0 Dimethyl Phosphorochloridothioate 77-78-1 Dimethyl Sulfate 75-18-3 Dimethyl Sulfide 75-78-5 Dimethyldichlorosilane

57-14-7 Dimethylhydrazine 99-98-9 Dimethyl-p-Phenylenediamine 644-64-4 Dimet ilan 534-52-1 Dinitrocresol [DNOC] 88-85-7 Dinoseb [Premerge Dinitro] Threshold Reportat CAS No. Chemical name [Trade Name] planning quantity quantit: (pounds ) (pounds 1420-07-1 Dinoterb 500/10,000 1 78-34-2 Dioxathion 500 82-66-6 Diphacinone 10/10,000 1 \ 152-16-9 Diphosphoramide, Octamethyl- 100 100 298-04-4 Disulfoton 500 1

514-73-8 Dithiazanine Iodide 541-53-7 Dithiobiuret 316-42-7 Emetine, Dihydrochloride 115-29-7 Endosulfan [Di Syston] 2778-04-3 Endothion

72-20-8 Endrin 106-89-8 Epichlorohydrin 2104-64-5 EPN 50-14-6 Ergocalciferol 379-79-3 Ergotamine Tartrate

1622-32-8 Ethanesulfonyl Chloride, 2-Chloro- 10140-87-1 Ethanol, 1,2-Dichloro-, Acetate 563-12-2 Ethion 13194-48-4 Ethoprophos 538-07-8 Ethylbis(2-Ch1oroethyl)Amine

Ethylene Fluorohydrin Ethylene Oxide Ethylenediamine Ethyleneimine Ethylthiocyanate

Fenamiphos [Nomecur] Fenitrothion Fensulfothion Fluenetil Fluorine

Fluoroacetamide Fluoroacetic Acid Fluoroacetyl Chloride Fluorouracil Fonof os

Formaldehyde Formaldehyde Cyanohydrin Formetanate Hydrochloride [Carzol, Dicarzol] Formothion Formparanate Threshold Reportable CAS No. Chemical name [Trade Name] planning quantity quantity (pounds) (pounds)

1548-32-3 Fosthietan 500 , 1 )878-19-1 Fuberidazole 100/10,000 1 110-00-9 Furan 500 100 1450-90-3 Gallium Trichloride 500/10,000 1 77-47-4 Hexachlorocyclopentadiene 100 1

1835-11-4 Hexamethylenediamine, N,N'-Dibutyl- 302-01-2 Hydrazine 74-90-8 Hydrocyanic Acid '647-01-0 Hydrogen Chloride (Gas Only) '664-39-3 Hydrogen Fluoride '722-84-1 Hydrogen Peroxide (Conc > 52%) 1,000 1 '783-07-5 Hydrogen Selenide 10 1 '783-06-4 Hydrogen Sulfide 500 100 123-31-9 Hydroquinone I 500/10,000 1 1463-40-6 Iron, Pentacarbonyl- 100 1

297-78-9 Isobenzan 100/10,000 1 78-82-0 Isobutyronitrile 1,000 1 102-36-3 Isocyanic Acid, 3,4-Dichlorophenyl Ester 500/10,000 1 465-73-6 Isodrin 100/10,000 1 55-91-4 Isofluorphate 100 100

Isophorone Diisocyanate Isopropyl Chlorofomate Isopropyl Formate Isoproplymethylpyrazolyl Dimethylcarbamate Lactonitrile

Leptophos Lewisite Lindane Lithium Hydride Malononitrile

Manganese, Tricarbonyl Methylcyclopentadienyl Mechlore thamine Mephosfolan Mercuric Acetate Mercuric Chloride

Mercuric Oxide Methacrolein Diacetate Methacrylic Anhydride Methacrylonitrile Methacryloyl Chloride Threshold Repor tak CAS No. Chemical name [Trade Name] planning quantity quantit (pounds) (pounds

Methacryloyloxyethyl Isocyanate 100 1 Methamidophos [Monitor] 100/10,000 1 Methanesulfonyl Fluoride Methidathion [Supracide] Methiocarb [Mesurol]

Methomyl [Lannate, Nudrin] Methoxyethylmercuric Acetate Methyl 2-Chloroacrylate Methyl Bromide Methyl Chloroformate

Methyl Disulfide 100 Methyl Hydrazine 500 Methyl Isocyanate 500 Methyl Isothiocyanate [Meta-Sodium, Yapam, Yodex] 500 Methyl Mercaptan 500

Merhyl Phenkapton Methyl Phosphonic Dichloride Methyl Thiocyanate Methyl Vinyl Ketone Methylmercuric Dicyanamide

Methyltrichlorosilane Metolcarb Mevinphos [Phosdrin, Phosfene] Mexacarbate [Zectran] Mitomycin C

Monocrotophos [Azodrin] Muscimol Mustard Gas Nickel Carbonyl Nicotine

Nicotine Sulfate Nitric Acid Nitric Oxide Nitrobenzene Nitrocyclohexane

Nitrogen Dioxide Nitrosodimethylamine Norbormide Organorhodium Complex (PMN-82-147) Ouabain Threshold Reportable CAS No. Chemical name [Trade Name] planning quantity quantity (pounds) (pounds)

oxamyl [Ydate] 100/10,000 1 Oxetane, 3,3-Bix(Chloromethy1)- 500 e Oxydisulfoton 500 1. Ozone 100 1 Paraquat [Gramoxone] 10/10,000 1

Paraquat Methosulfate Parathion [Penncap-El Parathion-Methyl [Penncap-M] Paris Green Pentaborane

Pentadecylamine Peracetic Acid Perchloromethylmercaptan Phenol Phenol, 2,2'-Thiobis(4,6-Dichloro-

Phenol, 2,2'-Thiobis(4-chloro-6-Methyl-Phenol, 2,2'-Thiobis (4-Chloro-6-Methyl)- 100/10,000 1 Phenol, 3-(1-Methylethyl)-, Methylcarbamate 500/10,000 1 Phenoxarsine, 10,lO'-Oxydi- 500/10,000 1 Phenyl Dichloroarsine 500 1 Phenylhydrazine Hydrochloride 1,000/10,000 1

Phenylmercury Acetate Phenylsilatrane Phenylthiourea Phorate [Thimet, Rampart] Phosacetim

Phosfolan [Cyolane] Phosgene Phosmet [Imidan, Prolate] Phosphamidon [Dimecron, Apamidon] Phosphine

Phosphonothioic Acid, Methyl-, 0-Ethyl 0-4-(Methy1thio)Phenyl) Ester 500 Phosphonothioic Acid, Mehtyl-, S-(2-(Bis(1-Methylethy1)Amino)Ethyl 0-Ethyl Ester 100 Phosphonothioic Acid, Methyl-, (0-(4-Nitrophenyl) 0-Phenyl Ester 500 Phosphoric Acid, Dimethyl 4-(Methylthio) Phenyl Ester 500 Phosphorothioic Acid, 0,O-Dimethyl-S-(2-Methylthio) Ethyl Ester 500 Threshold Repor tak CAS No. Chemical name ITrade Name] planning quantity quantit: (pounds) ( pounJ s

Phosphorus 100 1 Phosphorus Oxychloride 500 1,000 Phosphorus Pentachloride 500 1 Phosphorus Pentoxide 10 1 Phosphorus Trichloride 1,000 1,000

Physostigmine Physostigrnine, Salicylate (1:l) Picrotoxin Piperidine Piprotal

Pirimifos-Ethyl [Primicid, Femex, Primotec] Potassium Arsenite Potassium Cyanide Potassium Silver Cyanide Promecarb [Carbamult]

Propargyl Bromide Propiolactone, Beta- Propionitrile Propionitrile, 3-Chloro- Propiophenone, 4-Amino-

Propyl Chloroformate Propylene Oxide Propyleneimine Prothoate Pyrene

Pyridine, 2-Methyl-5-Vinyl- Pyridine, 4-Amino- Pyridine, $-Nitro-, 1-Oxide Pyr iminil Salcomine

Sarin Selenious Acid Selenium Oxychloride Semicarbazide Hydrochloride Silane, (4-Aminobuty1)Diethoxymethyl-

Sodium Arsenate Sodium Arsenite Sodium Azide (Na(N3)) Sodium Cacodylate Sodium Cyanide (Na(CN)) Threshold Reportable CAS No. Chemical name [Trade Name] planning quantity quantity (pounds) (pounds)

62-74-8 Sodium Fluoroacetate 10/10,000 10 131-52-2 Sodium Pentachlorophenate 100/10,000 1 3410-01-0 Sodium Selenate 100/10,000 1 0102-18-8 Sodium Selenite 100/10,000 100 0102-20-2 Sodium Tellurite 500/10,000 1

Stannane, Acetoxytriphenyl- Strychnine Strychnine, Sulfate Sulf otep Sulfoxide, 3-Chloropropyl Octyl

Sulfur Dioxide Sulfur Tetraf luoride Sulfur Trioxide Sulfur Acid Tabun

Tellurium Tellurium Hexafluoride TEPP . Terbufos [Counter] Tetraethyllead

Tetraethyltin Tetramethyllead Tetranitromethane Thallium Sulfate Thallous Carbonate

Thallous Chloride Thallous Malonate Thallous Sulfate Thiocarbazide Thiofanox

Thionazin Thiophenol Thiosemicarbazide Thiourea, (2-Chloropheny1)- Thiourea, (2-Methylpheny1)-

Titanium Tetrachloride Toulene 2,4-Diisocyanate Toluene 2,6-Diisocyanate Trans-1,4-Dichlorobutene Triamiphos Threshold Reportal CAS No. Chemical name [Trade Name] planning quantity quant it (pounds) ( pound^

24017-47 -8 Triazof os 500 1 76-02-8 Trichloroacety Chloride 500 1 115-21-9 Trichloroethylsilane 500 1 327-98-0 Trichloronate 500 1 98-13-5 Trichlorophenylsilane 500 1

1558-25-4 Trichloro(Chloromethyl)Silane 100 1 27 137-85-5 Trichloro(Dichlorophenyl)Silane 500 1 998-30-1 Triethoxysilane 500 1 75-77-4 Trimethylchlorosilane 1,000 1 824-11-3 Trimethylolpropane Phosphite 100/10,000 1

1066-45-1 Trimethyltin Chloride 639-58-7 Triphenyltin Chloride 555-77-1 Tris(2-Chloroethy1)Amine 2001-95-8 Valinomycin 1314-62-1 Vanadium Pentoxide

108-05-4 Vinyl Acetate Monomer 1,000 5,000 81-81-2 Warfarin 500/10,000 100 129-06-6 Warfarin Sodium 100/10,000 1 28347-13-9 Xylylene Dichloride 100/10,000 1 58270-08-9 Zinc, Dichloro(4,4-Dimethyl-5((((Methylamino) Carbonyl)Oxy)Imino)Pentanenitrile)-AT-4)- 100/10,000 1

1314-84-7 Zinc Phosphide

EHS .LST Attachment CERCLA

TABLE 302.4-LIST OF HAZARDOUS SUBSTANCES AND REPORTABLE QUANTITIES [See lwlnoles a1 end of Table 302 41 Slatutoq - F~nalRO RCRA Hazardous Subslance CASRN Regulatory Synonyms Ca:90 RO Codet Waste Poundr(Kp) Number

Acenaplilherw ...... 83329 ...... 1 2 ...... B to0 (45 41 Acenaphlhyteno ...... 200968 ...... I* 2 ...... D SOOO(2270l Acetaldehyde ...... 75070 Ethanal...... 1OOO 1.4 UOOt C tOOO(454) Acetaldehyde, chloro- ...... I07200 Chtoroacetaldehyde...... 1' 4 PO23 C 1000 (4541 Acelaldehydc. Irichtoro-.... 75876 Chloral...... 1' 4 UOJ4 X IX(0 454) Acelamidc. N. 591082 l.Acclyl.2.thtcurea ...... I' 4 PO02 C 1000 (454) (aminolh10rome1hyl)-. Acetam~dc.N.14. 62442 Phcnacebn...... 1. 4 Ul87 X I# (0 454) elhoxyphenyl)-. Acetam~de.N.9H. 53963 2~Acelylam1nolluaene...... 1' 4 UOOS X 1X (0 454) Ituoren.2.yl.. Acetam1de,2.lluoro...... 640197 Fluoroacelamide...... 1' 4 PO57 . B to0145 41 Acetic ac~d...... 64 197 ...... I000 1 ...... D SOOO(2270I Acel~cacld. ethyl ester ..... 141786 Elhyl acclale ...... 1. 4 UIIZ D 5000 (22701 Acel~cacld. Iluoro.. 62748 Ftuoroaccl~cacld. 1. 4 PO58 A 10 (4 541 sod~umsalt. sod~umsalt. Acelc ac~d,lead sat1...... 301042 Lead acetate ...... 1.4 Ul44 0 SOooN (2270) Accttc acid. IhalLum(l) 563688 Thatl~um(l)acetate ...... SOW1 4 U214 B I00 (45 4) salt. Acetnanhydtide ...... 108247 ...... IOOO I ...... 0 5WO(Z270) AcoLm~dlcac1d.N. 16752775 Mcthomyl...... 1' 4 PO66 B 100 (45 4) I(mc1hylcarbamoyt) o#y)lhto., methyl eslcr. &otone ...... 67641 2.Propanone ...... 1' 4 UW2 0 5000(1270l -. / 9 302.4 40 CFR Ch. I (7-1-88 Edition) Environmental Protection Agency 9 302.4 TABLE 302.4-LIST OF HAZARDOUS SUBSTANCES AND REPORTABLE QUANTITIES- TABLE 302.4-LIST OF HAZARDOUS SUBSTANCES AND REPORTABLE QUANTITIES Continued Continued [See tootnotes at end 01 Table 302 41 [See tootnotes a1 end 01 TabIe 302 41 - Statutow -- ial RO -_tatutory- - -- I Hazardous Substance CASRN RCRA Catcgo- Hazardous Substance CASRN Regulatory Synonyms :atego- Pwnds(Kg) Code i WasIe Numbei -ry I Number ry Acetone cyanohydrin ...... 75865 2-Methyllactonitrile ...... A to (4.54) 'henol. 2.4.6-lrinilro-. 1' 4 Po09 A 10 (4 54) Propanenitrile. 2- Ammonium picrate...... 131748 ammonium salt. hydroxy.2-melhyl- 1'4 I Ammonium siticotluoride... 16919190 ...... 1000 1 ...... C 1000 1454) Acetonitrile...... 75058 Elhanerutrlle ...... 4 u003 D 5000 (2270) Ammonium sullamate ...... 7773060 ...... 5000 1 ...... D 5000 (2270) 3-(alpha- 81812 Warlarin ...... 4 Pool B 100 (45.4) Acetonylbenzy1)- 4- Ammonium sulfide ...... 12135761 ...... 5000 1 ...... B 100 (45 4) hydroxycoumarin and Ammonium sullile ...... 10196040 ...... 5000 1 ...... D 5000 (2270) salts. Ammonium tartrate ...... 14307438 ...... 5000 1 ...... 0 so00 12270) 3164292 Acetophenone...... 98862 Elhanone. 1-phen+ ...... 1' 4 uoo4 D 5000 (2270) 5000 1 ...... D 5000 (2270) 2-Acetylaminollwnene ...... 53963 Acetamide. N-9H- 1' 4 u005 X 11(0.454) : Ammonium thiocyanate .... 1762954 ...... Iluaen-2-yl-. Ammonium thiosullate ...... 7783188 ...... 5000 1 ...... D C 1000 (454) Acetyl bromide ...... 506967 5000 1 I...,.. D 5000 (2270) Ammonium vanadate ...... 7803556 iranadle acd. 1' 4 P119 Acetyl chloride ...... 75365 Emanoyl chloride...... 5ooo 1.4 0 so00 (2270) ammoniumsan. l-Ace(yt-2-vliouea ...... 591082 Acetamide. N- 1' 4 Po02 C 1000 (454) Amyl acetale ...... 628637 ...... too0 1 0 5000 (2270) (aminothioxome~yI)-. iso- 123922 Acrolein ...... 107028 2-Pmpenal ...... 1 1.2.4 PO03 X 1 (0.454) SeC- 626380 Acrytamide ...... 79061 2-Propenamide...... 1' 4 u007 D 5000 (2270) ten- 625161 Acrylic acid ...... 79107 2-Propendc acid...... 1' 4 UWB D 5000 (2270) Eenzenamine ...... 1000 1.4 UOl2 0 5000 12270) Acrylonitrile...... 107131 2-PropeneniWe ...... 1M 1.2.4 UOO9 B 1001 (45.4) ...... 1' 2 ...... D 5000 (2270) Adipic acid ...... 124049 ...... 5ooo 1 ...... D 5000 (2270) ...... 1' 2 ...... D MOO (2270) Alanine. 3-Cp-bis(2- 148823 Melphalan...... 1' 4 u150 X 11(0.454) 1' 2 ...... chloroethyt)aminol phenyl-.L-. 1000 1 ...... C 1m(454) Aldii ...... 116063 Propanal. 2-methyl-2- 1' 4 PO70 x 1 (0.454) 1000 1 ...... B 100 (45 4) (melhy1thio)-. 0 [(methylamino) 1000 1 ...... C 1000 (454) carbonylloxime...... 1000 1 ...... C 10001454) 1.2.3.4.10-10- 1 1.2.4 Po04 X l# (0.454) 1000 1 ...... C 1000 (454) Hexachlao- ...... so00 1 ...... C 1000 (454) 1.4.4a.5.8.Ba- 10 ...... A 101 (4 54) hexahydro- 1.45.8- Polychlorinated 1.2 endo. exo- Biphenyls (PCBS). A 101 (4 54) dimelhanonaphthalene. Polychlorinated 10 1.2 ...... Btphcnyls (PCBs). Allyl alcohol ...... 107186 2-Propen-1-01...... 100 1.4 B 100 145.4) Polychlorinalcd 10 1.2 ...... A 101 (4 54) Allyl chloride...... 107051 ...... 1000 1 C 1000 (454) Biphenyls (PCBS). Aluminum phosphae...... 20859738 ...... 1' 4 B 100 (45.4) 10 1.2 ...... A 101 (1 54) Aluminum sullale ...... 10043013 ...... 5000 1 0 5OOO (2270) Pdychlorinatcd 2-Amino-1-methyl 95534 0-Toluidine...... 1* 4 X 11(0.454) Biphcnyls (PCBs). benzene. Polychlorinaled 10 1.2 ...... A io1 (4 s41 4-Amino-1-methyl 106490 toluidine ...... 1* 4 X 11(0.454) Biphenyls (PCBs). benzene. Polychlorinalcd 10 1.2 A 101 (4 54) 5-(Aminomethyl)-b 2763964 3(2H)-lsoxazolone.5- 1' 4 C 1MX) (454) Biphenyls (PCBs). isoxazolol. (aminomethyl)-. Polychlorinalcd IO 1.2 ...... A 101 (4 54) 4-Aminopyridine ...... 504245 Wyridinamine...... 1' 4 C 1000 (454) Blphenyb (PCBs). Armtrole ...... 61825 lH-l.2.4-Triazol-3-amme ... 1' 4 X 11 (0.454) ...... 1- 2.3 ...... X 11(0 454) Ammonia ...... 766.1417 ...... 100 1 B 100 (45 4) ...... 1' 4 Pol0 X 11IO 454) Ammonium acetate ...... 63 1618 ...... 5000 1 D 5000 (2270) Ammonium benzoate...... 1863634 5000 1 D 5000 (2270) ...... 1- 2 ...... Ammonium bicarbonate.... 1066337 ...... 5000 1 D Moo (2270) Ammonium bichromale ..... 7789095 1000 1 C 10001 (454) ...... 5000 1 ...... D 50006 (2270) Ammonium billwride...... 134 1497 5000 1 B 100 (45 4) Arsentc trioxide ...... 5000 1.4 PO12 D 50001 (2270) Ammonium bisulfite...... 10192300 5000 1 D 5000 12270) Arsenic pentoxide ...... 5000 1.4 Wl1 D 5000112270) Ammonium carbamate ...... 11 11780 ...... 5000 1 D 5000 (2270) Arsenic[V) oxide...... 5000 1.4 PO1 1 0 50001 12270) Ammonium c .... 506876 5000 1 D 5000 (2270) ...... 5000 1 ...... D 50501 (2270) Ammonium c ... 12125029 5000 1 D 5000 (2270) Arsenic(ll1) oxide ...... 5000 t .4 PO12 D 50001 (22701 Ammonium c ... 7788989 ...... 1000 1 C 10001 (454) 5000 1 ...... D 50001 (2270) Ammonium citrate. 3012655 ...... 5000 1 D 5000 (2270) Diethylarsine...... I' 4 PO38 X t 1(0 454) dibasic...... 1' 2.3 ...... X 11(0454) ...... 5000 '1 D 5000 (2270) Benzenamine. 4.4'- 1' 4 U014 X 11 (0454) ...... 5000 1 B 100 (45.4) carbonimi&ytbis(N.N- Ammonium hydroxide 1336216 ...... 1000 1 C tW0 (454) dimethyl-. Ammonium oxalate...... 6009707 ...... 5000 1 D 5000 (2270) LSerine. diazoacetate 1. 4 U015 X I# (0 454) 5972736 (ester). 14258492 Ethylenimine ...... 1. 4 PO54 X I 1X (0.454) 116 117 9 302.4 40 CFR Ch. 1 (7-1-88 Edition) Environmental Protection Agency 9 302.4 TABLE 302.4-LIST OF HAZARDOUS SUBSTANCES AND REPORTABLE OUANTITIES- TABLE 302.4-LIST OF HAZARDOUS SUBSTANCES AND REPORTABLE OUANTITIES- Continued Continued [See loolnolos al end of Table 302.4) [See loolnolcs at and of Table 302.41 --Statutory hnal RQ Hazardous Subslance CASRN aegutatory SYMY~S I I I RQ 1 d 1 k% 1 I PouMU~ Number Number -- Benzene. 1-melhyl-2.4- 1 121142 1 2.4-~1nltrotoluene...... 1 1000

d~nllro-. Benzene. 1.2- 94597 Salrole...... 1' melhylened10xy-4-a11yl-. Benzene. 1.2- I 120581 1 Isosalrole ...... 1' Barium cyanide ...... 542621 ...... 1014541 propenyl-. Benz[ilaceanlhrylene. 56495 3-Melhylcholanlhrene I 1 1 1 : I ...... 11 (0.454) Benzene. 1.2- 1.2-dihvdra3meVnn-. 'I,-- I ...... melhvlenedmxv-4- 1 Benz[clacridine ...... 225514 3.4-Benzaaidine ...... 1' 4 U016 X 11 (0.454) 3.4-Benzacndine 98828 Cumene...... 5000 12270) ...... 225514 Benz[clacridine...... 1. 4 U016 X 11 (0.454) Benzene. l-melhylelhyl-... Benzal chloride 98953 N~lrobenzene lf 1WO (454) ...... 98873 Benzene. 1 4 U017 0 5000 (2270) Benzene. nilro-...... dichloromethyl-. Benzene. penlachloro- 608935 IPentachlorobenzene ...... 1 1 I / 1 10 (4 54) ...... Benz[alanlhracene 82688 Pentachloconitrobenzene.. U185 11(0454) ...... 56553 1.2-Benzanthracene... :...... 1' 2.4 U018 X 11(0.454) Benzene. Benzo[alanthracene penlachloronilro-. 1PEenzanlhracene...... 56553 Benz[alanthracene ...... 1' Benzene. 1.2.4.5 Benzo[alanlhracene tetrachloro-. 1.2-Benzanthracene. 57976 7.12-D~rnethylbenz[al Benzene. 7.12-d~melhyl-. anlhracene. lrichlorornelhyl-. 1 I Benzene. 1.3.5-trinitro- 99354 sym-Trin~lrobenzene...... Benzenamine ...... Aniline ...... 1000 ...... Benzenamine. 4.4'- Auramine ...... 1' Benzencacelic acid. 4- 510156 Elhyl 4.4'- carbon~m~doylbis(N.N- chloro-alpha-(4- diihlorobenzilate. I diilhyl-. chlorophcnyl)-alpha- I I Benzenamine. 4lhloro-.... p-Chboaniline...... 1' hydroxy-. ethyl ester. Benzenam~ne.4-chlWO- 4-Chloro-o-loluidii 1.2.Benzencdicarboxylic 85449 Phlhalic anhydre ...... 2-melhyl- hydrochloride. acid anhydride. .hydrochlwde. 1.2-Benzcnediiarboxylic 11781 7 Bis(2- e1hylhexyl)phlhalaIe. Benzenamne. N.N. Oimelhy(aminoazoben. I acid.Ibis(2-elhylhexyQ1 ester. dimelhyl-4-phcnylazo-. zene...... Benzenanune. 4.4'- 4A'.MethyInebis(2- 1.2-Benzened~carboxyl'i 84742 n-Bulyl phlhalate melhyleneb1s(2-chloro.. chloroaniline). ac~d.d~bulylesler. D~butvlohthalale Bcnzenammo. 2-melhyl.. o.Toluidmne I I I ~i-n.bui~lphlhalate hydrochloride. hydrochloride...... Benzenamine. 2-methyl. 5.N1tro-o-lohndine ...... acid.d~elhylesler. 5-n~tro-...... Bemenamme. 4.mlro- ...... p-Nitroaniline...... Benzene...... iod.dlmethyl ester: ...... 1.2-Benzened~carboxylic 117840 Di-n-oclylphlhalate ...... Benzene. l-bromo-4- 4-Bromophenyl phenyl acid.dl-n-oclyl ester. phenoxy-. ether. I I Benzene, chloro- ...... Chlorobenzene...... Benzene. chtoromelhyl-.... Benzyl chloride ...... Benzene. 1.2-dichloro-...... 1.2-D~chlorobenzene...... o.D~chlwobenzene Benzene. IJ-d~chloro- ...... 1.3-[hchlorobenzene ...... chlor~de. m-Bchlorobcnzene Benzenesullonyl chloride.. 98099 Benzenesulloruc acid Benzene. 1.4-dehlwo- ...... 1 1.4-Dshlorobenzene...... loo (45.4) chor~de...... p-Dichlorobenzene Benzenethiol...... 1 108985 Thlophenol I Benzene. Benzal chloride ...... 5000 (2270) Benzldlne ...... 92875 (1.1'-01phenyl)- dtchloromelhyl-. 4.Cdam1ne. Benzene. 2.4- Toluene dikocyanate ...... 100 (45.4) 1.2-Benzisolhiazoiin-3- 81072 Saccharin and salts ...... diisocyanalomelhyl-. one.1 .l -dlox~de.and I I Sa1t.5. Benzotalanlhracene...... Benzene. dimethyl...... I m- Benzo[bllluoranlhene...... o- Benzo(k)lluoranlhene...... P ~enzo[i.k]fluorene...... Benzene, hexachloro- ...... Hexachlwobenzene...... 1' Benmtc acid...... Ppnzene. hexahydro- ...... Cyclohexam...... 1000 Benzon~lrile...... Benzene, hydroxy-...... Phenol ...... 1000 Benzo[gh~lperylene...... Benzene, melhyl- ...... /IToluene lo00 ...... 1 Benzo[alpyrene ...... - 40 CFR Ch. 1 (7-I-$$Edition) Environmental Protection Agency

TABIF 302.4-LIST OF HAZARDOUS SUBSTANCES AND REPORTABLE QUANTITIES- TABLE 302.4-LIST OF HAZARDOUS SUBSTANCES AND REPORTABLE QUANTITIES-- Continued ! Continued [See lwlnoles a1 end of Table 302 4 1 I [See Iootnoles at end 01 Table 302.41 I Statutory F~nalRO Stalulory Ftnal RO Hazardous Substance CASRN Regulatwy Synonyms RCRA RO Codet Waste Catego- Pounds(Kg) RO Codet Waste Pounds(Kg) ry Number Cag~ Nzi 1 BenzoIalpyrene ...... 1' 2-Bulenal...... 123739 Crolonaldehyde...... 100 1.4 U053 B 100 (45 4) 1.4-Cyclohexad~ened~one.. 1' 4170303 Benzene. 1' 2-Butene. 1.4dehlorc- ..... 764410 1.4-Dichlorc-2-butene ...... 1' 4 U074 X 1 (0 454) trichloromelhyl-. Butyl acetale ...... 123864 ...... MOO 1 ...... D 5000(2270) zoyl chwde ...... 98884 ...... 1000 iso- 110190 3enzphenanlhrene...... 218019 Chrysene ...... 1' SeC- 105464 zvl chloride ...... 100447 Benzene. chlorornelhyl- .... 100 J. lerl- 540885 . ,Illurn t t ...... Beryllium dust...... 1' n-Butyl akohol ...... 71363 1-Butanol ...... 1 4 U031 ' D 5000 (2270) lYLLlUM AND ...... 1' Butylamine...... 109739 ...... 1000 1 ...... C 1000 (4%) 3MPOUNDS. iS0- 788 19 ,Ilium chloride ...... MOO SeC- 513495 nI11um dust...... Beryllium ...... 1 SeC- 13952846 llltum fluoride ...... 50M) terl- 75649 rlllum nitrate ...... so00 Butyl benzyl phlhalale...... 85687 ...... 1' 2 ...... B 100 (45.4) n-Butyl phlhalate...... 84742 1.2-BenzanodiarboxyI'e 100 1.2.4 U069 A 10 (4.54) la . BHC ...... 319846 ...... acid.dlbutyl esler. I. BHC ...... 319857 ...... Oibutyl phthalale Ima - BHC ...... 58899 Hexachlorocyclohexane Di-n-butyl phthalale (gamma isomer). Bulyric acid ...... 107926 ...... SOCO 1 ...... D 5000 (2270) Lindane iso- 79312 a . BHC ...... 319868 ...... Cacodylic acid ...... 75605 Hydroxydimethylarsine 1' 4 U136 X 1H (0.454) -Bioxrane ...... 1464535 1.2:3.4-Diepoxybulane...... oxide. X '-Btphenyl)- 92875 Benzidine...... Cadmium t t ...... 7440439 ...... 1. 2 ...... 1# (0.454) Cadmium acetate 543908 ...... 100 1 ...... B lOOH(45.4) .4'dlamine...... '-0iplrcnyl)-4.4' 9194 1 3.3'-Dichlwobenzidine...... CADMIUM AND ...... 1' 2 ...... :amina,3,3'dichloro.. COMPOUNDS. '.O#pt1rnyl).4,4' 119904 3.3'-D~melhoxybenzidme... Cadmium bomide ...... 7789426 ...... 100 1 ...... B 1001 (45 4) 1am1na.3.3'd1mcthoxy-. Cadmium chlortde...... 10108642 ...... 100 1 ...... B loon (454) 1000 1 ...... C lOOOa(454) '01phcnyl)-4.4'- 119937 3.3'-Ikmelhylbenzidino ...... Cakium arsenate...... 7778441 ...... 1 C 1000#(454) 1amine.3.3'-dtmethyi-. Cakiwn arsenite ...... 52740166 ...... 1000 ...... 1 A 10 (4 54) 2-chloroelhoxy) 111911 Ethane. 1.1'- Calcium carbide ...... 75207 ...... 50M) ...... C lWO# (454) ~ethane. Imethylenebis(oxy)l Calcium chromate...... 13765190 Chrome acid. cakii loo0 1.4 U032 bts(2-chloro-. salt. 592018 10 PO21 A 10 (4 54) (2-chloroelhyl)ether ... 111444 Dtchloroclhyl elher ...... Calcium cyanide...... 1.4 do6ecylbenzene 26264062 1000 1 ...... C 1000(454) Ethane, 1.1'-oxyb1sI2- Calcium ...... cllloro- sullonale. 7778543 100 1 ...... A 1014 54) EZ.chlcfoisopropyI) I08601 Propane. 2.2'-oxybos(2- Calc~umhypochlortle ...... X 1# (0 454) tllcr. chloro-. Camphene. Oclachloro- .... 8001352 Toxaphene ...... 1 1.2.4 PI23 10 1 ...... A 106 (4 54) Icllloromclhyl) ether ..... 547881 Mclhane. oxybis(chlwo. ... Captan...... 133062 ...... Carbam~cacid. ethyl 51796 Elhyl carbamale 1' 4 U238 X 11 (0454) 137268 Thiram ...... Lmcthyllh~ocarba- ester. (Urclhan). Carbamic acid. 615532 N-Ntlroso-N- 1' 4 U178 X 11 (0.454) mclhylnilroso-.ethyl methylurethane. 1.2.Bcnzencdicarboxyhc ester. acld. lbas(2- Carbam~de.N-ethyl-N- 759739 N-N~lroso-N-ethylurea...... 1' 4 U176 X 1# (0 454) elt1ylllexyl)l esler. n~troso-. mtne cyanide...... Cyanogcn bromlde ...... Carbam~de.N-methyl-N- 684935 N-Nitroso-N-methylurea.... 1' 4 U177 X 1a (0 454) moacelone ...... 2-Propanone. 1.bromo...... nitroso-. mo1orm ...... Methane. tr~bromo-...... Carbam~de.lhlo- ...... 62566 Thtourea ...... 1' 4 U219 X 11(0 454) tomophenyl phenyl Bcnzene, l-bromo-4- Carbamimidoselenoic 630104 Selenourea 1' 4 PI03 C 1000 (454) !ther...... phenoxy-. acid. ICtne ...... Slrychnldln-10-one,2.3- Carbamoyl chlwide. 79447 Dimethylcarbamoyl 1' 4 U097 X 1# (0.454) dimcthoxy-. d~melhyl-. chloride. nhtadiene. Hexachlorobutadiene...... Carbaryl...... 63252 ...... 100 1 ...... B 100 145 4) D.1.2.3.4.4-hexachlorc-. Carbofuran...... 1563662 ...... 10 1 ...... A 10 (4.54) lutanam~ne.N-butyl- Carbon bisullide...... 75150 Carbon disulbde ...... 5000 1.4 PO22 B 100 (45 4) 4-ntlroso-. Carbon diwlflde...... 75150 Carbon b~sullii...... 5000 1.4 PO22 B 100 (45.4) ranoic acid. 4-[brs(2- Chlwambucil...... Carbonic acid. 6533739 Thallium(1) carbonate ...... 1. 4 U215 B 100 (45.4) :hloroethyl)aminol dilhallium(l) salt. ~enzene-. Carbonochlonds acid. 79221 Methyl chlor~carbonale.... 1' 4 U156 C lo00 (454) jutan01 ...... n-Bulyl alcohol ...... methyl esler. %itanone ...... Methyl ethyl ketone...... Carbon oxylluoride ...... 353504 Carbonyl Ilwnde...... 1. 4 U033 C 1000 (454) 3ulanorie peroxide...... Methyl ethyl ketone Carbon tetrachloride...... 56235 Methane. telfachloro- ...... SO00 1.2.4 U211 D (2270) peroxide. Carbonvl chloride...... 75445 Phosoene...... 5000 1.4 PO95 A 10 (4.54) I 302.4 40 CFR Ch. 1 (7-1-88 Edition) Environmental Protection Agency 5 302.4 TABLE 302.4.LIST OF HAZARDOUS SUBSTANCES AND REPORTABLE QUANTITIES- TABLE 302.4.LlST OF HAZARDOUS SUBSTANCES AND REPORTABLE QUANTITIES- Continued Continued [See lootnotes at end of Table 302 41 1 [See lootnotes at end of Table 302 41 Statutory Final RO Stalulciy F~nalRO iazardous Substance CASRN Regulatory Synonyms RCRA Regulatory Synonyms RCR A CaEgO- Hazardous Substance CASRN Catego- RQ Coder waste Pounds(Kg) RO Codet Waste Pounds(Kg) Number Number 'Y . trbonyl fluoride...... 353504 Carbon oxylluoride ...... 1. 4 U033 C 1000 (454) 3-CMcfopro&n1lrtte...... 542767 Propamnilrile. 3-chbfo.... 1 4 PO27 C 1OoO (454) sloral ...... 75876 Acelaldchyde. trtchloro-.... 1' 4 U034 x In(0.454) Chlorosulfonic ac kl ...... 7790945 ...... 1 ...... C 1000 (454) .lorambuclI...... 305033 Bulano~cacid . 4-[b1s(2- 1' 4 U035 X I# (0.454) 4.Chloro.o.toluidine. 3165933 Benzcnam~ne. 4thloro- lo?1 4 U049 X 1H (0.454) chloroethyl)aminol hydrochlcfide. 2-melhyl- benzene. . .hydrochlortd e. ILORDANE ...... 1' 2 ...... a Chforpyr~los...... 2921882 ...... 1 1 ...... X 1 (0 454) TECHNICAL Chromic acetate ...... 1066304 ...... 1000 1 ...... C 1000 (454) dlXTURE AND Chromic ac~d...... 1 1115745 ...... t OM) 1 ...... C lOOO#l454) dETABOLITES). 7738945 lordane ...... 57749 Chlordane. technical ...... 1 1.2.4 U036 X 1# (0.454) Chromic acid. calcium 13765190 Calcium chromate...... 1000 1.4 U032 C 1MN)H (4541 4.7-Methanoindan. salt . 1.2.4.5.6.7.8.8- Chromic sullale ...... 10101538 ...... 1 ...... c 1000 (454) oclachloro- 3a.4.7.78- Chromium t t ...... 7440473 ...... 10y1 2 ...... X I# (0.454) tetrahydro- CHROMIUM AND ...... 1' 2 ...... lordane. technical ...... 57749 Chlordane ...... 1 1.2.4 U036 X 11 (0.454) COMPOUNDS. 4.7-Methanoindan. Chromous chloride...... 10049055 ...... 1000 1 ...... C 1000 (454) 1.2.4.5.6.7.8.8- ctuysene ...... 218019 12~~1hrene...... 1' 2.4 UO50 X 1I (0 4541 oclachloro- 3a.4.7.7a- Coballws bromide ...... 7789437 ...... 1000 1 ...... C tOOO(J54) tetrahydrt- Cobaltous lormate...... 544183 ...... lOCO 1 ...... C 1000 (454) 'LORINATED ...... 1' 2 ...... Cobaltous sulfamate ...... 14017415 ...... 1000 t ...... C 1000 (454) ENZENES. Coke Oven Emissions...... N.A...... 1' 3 ...... X 1# (0 454) LORINATED ...... 1' 2 .. 1 2 ...... D 5000(2270) ...... Copper t t ...... 7440508 ...... iTHANES. COPPER AND ...... 1. 2 ...... LORINATED ...... 1' 2 ...... COMPOUNDS. 4APHTHALENE . Coppercyanide...... 544923 ...... 1' 4 W29 A 10 (4 54) LORINATED ...... 1' 2 ...... Coumaphos ...... 56724 ...... 10 1 ...... A to (4 54) 'HENOLS . Creosote ...... 8001589 ...... 1' 4 U05I X :# (0 454) or~ne ...... 7782505 ...... 10 1 ...... A 10 (4.54) Cresol(s) ...... 1319773 Cresyhc acid ...... 1000 1.4 U052 C 1WOY (454) wine cyanide ...... 506774 Cyanogen chloride...... 1.4 PO33 A 10 (4.54) m- ...... 108394 ...... ornaphazine ...... 494031 2.Naphlhylamine. N. N. ;? 4 U026 X t# (0.454) 0- ...... 95487 ...... bis(2thloroethyl). . p...... 906445 ...... oroacetaldehyde 107200 ...... Acelaldehyde, chloro- ...... 1' 4 W23 C 100q!454) Cresyli acid ...... 1319773 Cresol(s) ...... 1000 1.4 U052 C 1M)OH (454) LOROALKYL ...... 1' 2 ...... m- 108394 ...... THERS . o- ...... 95487 ...... hloroaniline 106478 ...... Benzenamine. 4-chloro-.... 1' 4 PO24 C 1000 (454) p...... 106445 ...... orobenzene ...... 108907 Benzene. chloro- ...... 1.2.4 U037 B 100 (45.4) Crotonaldehyde...... 123739 2-Bulenal ...... 100 1.4 U053 too (45 4) hloro-maesol ...... 59507 p-Chloro-m-cresd...... '7 2.4 W39 D 5000 (2270) 4170303 Phenol. 4-chloro-3- Cumene...... 98828 Benzene l-melhylethyl- ... 1' 4 U055 D 5000 (2270) . 100 (45.4) methyl- Cuprlcacetale ...... 142712 ...... 100 1 ...... B hloro-mcresol...... 59507 4-Chloro-m-cresd...... 1' 2.4 U039 D MOO (2270) Cupric acetoarsenite ...... 12002038 ...... 100 1 ...... B l001(454) Phenol. 4thloro-3- Cupric chlcfide ...... 7447394 ...... 10 1 ...... A 10 I4 54) methyl- Cuprtc nttrale ...... 3251238 ...... 100 1 ...... B 100 (45 4) 3rodtbrommelhane.... 124481 ...... 1• 2 ...... B 100 (45.4) Cupric oxalate ...... 5893663 ...... 100 1 ...... B 100 (45 4) hloro.2.3. 106898 Epichlcfohydrin ...... 1000 1.4 U04t C lOOO# (454) Cupric sulfate ...... 7758987 ...... 10 1 ...... A 10 (4 54) ~xypropa~. Cupric sulfate 10380297 ...... 100 1 ...... B 100 (45 4) Oxlrane. 2- ammon~ated. (chloromethyl)- Cupr~clartrale ...... 8 15827 ...... t ...... B 100 .(45.4). 3roethane ...... 75003 ...... 1' 2 ...... 8 100 (45.4) CYANIDES...... 'Pp 2 ...... hloroethyl vinyl ether... 110758 Ethene. 2-chloroelhoxy-.... 1' 2.4 U042 C 1000 (454) Cyanides (soluble 57125 ...... 1' 4 W30 A 10 (4.54) noform ...... 67663 Melhane.lricWo ...... SWO 1.2.4 U044 D 5M)OC (2270) cyanide salts). not nomethyl methyl 107302 Methane. 1. 4 U046 X 11 (0.454) elsewhefe speciled . Iher 100 (45 4) . chloromelhoxy. Cyanogen...... 460195 ...... 1' 4 PO31 B 3-Chlaronaphlhalene ... 91587 2-Chloronaphthalene...... 1' 2.4 U047 D 5000 (2270) Cyanogen bromide ...... 506683 Bromine cyande ...... 1' 4 U246 c I000 (454) Naphlhalene. P-chloro- Cyanogen chlwide...... 506774 Chlorm cyanlde ...... 10 1.4 W33 A 10 (4 54) hloronaphthakne...... 91587 beta-Chloronaphlhalene... 1 2.4 U047 D 5000 (2270) 1.4.Cyc\ohexadienediom .. 106514 pBenzoqmnone...... 1' 4 U197 A 10 (4 54) Naphlhalene. 2-chloro- Cyclohexane...... 110827 Bewene. hexahydro- ...... 1000 1.4 U056 C lOOO(454) hbrophenol...... 95578 0-Chlorophenol ...... 1 2.4 U048 B loo (45.4) Cyclohexanone...... 108941 ...... 1' 4 U057 D 5000 (2270) 1# (0 454) Phenol. 2-chloro- l$.Cyclopentadene. 77474 Hexachlorocyclopenlb 1 1.2.4 U130 X lllorophend ...... 95578 2.Chlwophenol...... 1' 2.4 UM8 B 100 (45.4) 1.2.3.4.5.5.hexachlwo-. d~ene. X ir (0.454) Phenol. 2chloro- Cyclophosphanude ...... 50180 2H- 1.3.2. 1. 4 UOW I\lorophenyt phenyt 7005723 ...... 1• 2 ...... D SWO (2270) Oxazaphosphonne.2- !her . - [bis(2- 5344821 Thiourea. (2- 1 4 PO26 B 100 (45.4) chloroe1hyl)aminol hlorophenyl)thiwrea. chlorophenyl). . teuahydro-2sxde . , - s0;il.l 40 CFR Ch. I (7-1-88 Edition) Environmental Protection Agency 0 302.4 TABLE 302.4-LIST OF HAZARDOUS SUBSTANCES AND REPORTABLE OUANTITIES- TABLE 302.4-LIST OF HAZARDOUS SUBSTANCES AND REPORTABLE OUANTITIES- Continued Continued [See loolnoles a1 end 01 Tabla 302.41 [See footnotes at end 01 Table 302.4) - - - al A0 --Slatulory Final~- RO iazardws Substance CASRN Regulalg, Synonyms RCRA Hazardws Subslance CASRN RegulaIory Synonym RCRA Calcgo- Catcgo RO Waste Pounds(Kg) RO Code I waste Pwnds1Kgl dumber -ry - dumber -ry 1-0 Acid ...... 94757 2.4-0. salls and eslers ... 100 1.4 U240 B 100 (45.4) Dibenzla.hJanlhracene .... t- 2.4 UO63 X 1# (04541 ?,4. 1.25.6- Dichlorophenoxyacetic Dibenzanthraccne acid. salls and esters Dibenzla.ilpyrene...... 1' 4 u064 X 1w (0454) 1-0 Esters ...... 9411 I 100 -1 ...... B 100 (45.4) 1.2: 7.8-Dibenzopyrene ____.1' 4 u064 X 1410 454) 94791 Propane. 1.2-dibrOnh3-3- 1. 4 uo66 X 1I(0454) 94804 chloropropane. chloro-. 1320 189 Dibutyl phthalate... 1.2-Benzenedicarboxyli 100 1.2.4 u069 A to (4 54) 1928387 acid.&utyl ester. 19286 16 Di-n-butyl phthalate 1929733 n8utyl phthalate 2971382 1.2-BemenedcartmxyIii 100 1.2.4 UO69 A 10 (4 54) acid.dibuIy1 esler. 25168267 n-BuIyl phthalate 534671 11 Dibulyl phthalate '-0.salts and esters 94757 !.4-0 Acid 100 u240 __.._ ...... 1.4 B 100 (45.4) 1000 1 ...... 1000 (454) !,4- C Dichlobenil ...... 1000 1 B 100 (45 4) Dichlorophenoxyacetic ...... 1 1 ...... X 1 (0454) acid. salls and esters Diallate ...... 1' 4 u062 X 1w IO 454) unomycin...... 20830813 i.12-Naphthacenediine. 1' 4 U059 X I# (0.454) (8S-cis)-8-acetyl-10 C3-amm1-10- 2.3.6- Pronamide ...... 1' 4 U192 D (2270) trideoxy- alpha-l-lyxo- 5oM) dimelhyl-2- hexopyranosyl)oxy 1- propyny0benzamide. 7.8.9.1 O-lelrahydro- 100 1 B 100 I45 4) 6.8.11-tnhydroxy- 1- Benzene. 1.Pdichloro- .__.. 100 1.2.4 U070 B 100 I45 4) methoxy-. o-Dichlorobenzene 4.4' ODD 1 ...... 1.2.4 U060 X I# (0.454) Benzene. 1.3-dichlor 1' 2.4 U071 B 100 (45 4) Dichlorodipheqi e.... m-Dichlorobenzene dichloroelhane Benzene. 1.4-drhlwe.... 100 1.2.4 U072 B 100 (45 4) TOE p-Duhlorobenzene ODD 1 ...... 1.2.4 U060 X 1I (0.454) Benzene. 1.3-dichloro-.... 1. 2.4 U071 B 100 (45 4) Dichlorodiphenyl 1.3-Dichlorobenzene dichloroelhane Benzene. 1.2-dohloro-.... 100 1.2.4 U070 B 100 (45 4) TOE 1.2-Dehlorobenzcne 4.4' DOE ...... 1' 2 ...... X l# (0 454) Benzene. 1.4-dichbo-.... 100 1.2.4 U072 B 100 145 4) DDE ...... 1' 2 X I# (0.454) 1.4-Dtchlorobenzene T ...... 50291 4.4' WT ...... t 1.2.4 U061 X lb (0.454) 1' 2 .. Dichlorodiphcnyl (1.1'-8iphenyI)- 1. 2.4 U073 X 1X (0 454) lrichloroelhane 4.4'diamme.3.3'dichlor( 'DDT ...... 50292 OD1 ...... 1 1.2.4 U061 X I# (0.454) 1- 2 D 5000 (2270) Dichlorodiphenyl 2-Butene. lC-d~~hIoro-.__ 1' 4 U074 X 1 (04541 lrichloroelhane Methane. 1' 4 U075 D MOO (2270) T AND ...... t. 2 ...... dichlorodilluoro-. IETABOLITES. Dichlorodiphenyl ODD...... 1 1.2.4 UO60 X 1I (0 454) '.achloiooclahydro- 14350( Kepone...... 1 1.4 Ut42 I# (0.454) drhloroelhane. .3.4 melheno-2H- 4.4' ODD yclobulalc.dl- TOE enlalen-2-one. Dichlorodiphenyl DOT ...... 1 1.2.4 U06l X 1w (0 456) llale ...... 2303164 S-(P.3-Drhlnoallyl~ 1' 4 uo62 1I(0.454) lrichloroelhane. diisopropyllhiocarba- 4.4'DDT mate. Ethane. 1.1-dichloro- ...... 1' 2.4 U076 C 1000 (454) mine ...... Hydrazine ...... 1' 4 U133 I#(0.454) Elhyhdene dichloride Toluenedmmme ...... 1' 4 u221 1X (0.454) Ethane. 1.2-dichloro- ...... SO00 1.2.4 uo77 0 SDOod 12270) 2537645f Ethylene dichlorlde 4967.X Ethene. 1.l-dichtoro- ...... 5000 1.2.4 U078 D 50001 (2270) 82340: Vinyldcne chlorlde 2" ...... 53334 15 ...... 1 1 1 (0.454) 1.2-lrans- Ethene. trans-1.2- 1' 2.4 U079 C loo0 (454) cnzIa.hlanlhracene..... 53703 1.2:5.6- 1. 2.4 U063 I# (0.454) Drhloroethylene. dichloro-. Dibenzanlhraceno. 81s (2-chlorocthyl) ether. 1' 2.4 U025 X 1# (0454) 01benzola.hlanlhracens Ethane. l.l'-oxybis(2- 5.6- 53705 DtbenzIa.hlanlhracene.. 1. 2.4 UO63 I# (0.454) chlorc- hbenzanthracene. 2.4-Dihbrophenol . Phenol. 2.4-dichloro-...... 1- 2.4 U08l B 100 (454) Z.~~hlorophenof. Phenol. 2.6-&chloro...... I. 4 U082 B 100 (45 4) 124 125 302.4 40 CFR Ch. 1 (7-1-88 Edition) Environmental Protection Agency 9 302.4

TABLE 302.4-LIST OF HAZARDOUS SUBSTANCES AND REPORTABLE QUANTITIES- TABLE 302.4-LIST OF HAZARDOUS SUBSTANCES AND REPORTABLE OUAi'JTITIES- Continued Continued [See footnotes at end of Table 302.41 [See footnotes at end ol Table 302.41

Hazardous Substance CAW RWU~synonyms RO ( 1 1 ~~~~ Cay- [ PuldslKgl 1 Number I -- -- - .--- khlorophenoryacelii ~cd,salts and esters. alpha.alpha- I0159 Hydroperon~de.t-methyl- 1 1. I 4 I U096 I A I 10 14 541 D~melhyIbenzyIhydro- I I 1-phenylethyl-. perox~de. 3.3-Dlmelhyl-1. 39196184 Thiofanox ...... 1methvlthio)-2- I I -. , carbonyll oxik. Dimelhylcarbamoyl 79447 Carbarnoyl chloride. 1' chloride. d~methyl-. 1.I-Dimelhylhydrazmne ...... 57147 Hydrazmne, 1.1-d~methyl-. 1' 1.2-Dimethylhydrazine ...... 540738 Hydrazine. 1.2-dimethyl-. 1. 0.0-D~methylO-p 298000 Melhyl parathion ...... 100 n~trophenyl phosphorolh~oate. hmethylnitrosamine...... 62759 N-N~trosod~melhylam~ne.. 1' alpha.alpha- 122098 Ethanamine. 1.1- ' t [)rmethytphenelhyla- d~melhyl-2-phenyl-. nunc. Hexachloro-6.7-epoxy- 2.4 .hmelhylphenol ...... 105679 Phenol. 2.4-dimethyl- ...... 1' 1.4.4a.5.6.7.8.8a- D~methylphlhalale ...... 131113 1.2-Benzenedlcarboxylic 1. ac~d.d~methylester. Dimethyl sullale ...... 77781 Sulfuric acid. dimethyl 1' I ester. Dinitrobenzene (mixed) ..... 25154545 ...... tow m- 99650 0- I 528290 P- 100254 4.6-D~nilro-o-nesoland 534521 Phend. 2.4-dmltro-6- 1 salts. methyl-, and salts. Ht~ylthio)elhyll 4.6.Dlnllro-o- 131895 Phenol. 2-cycloheryl-4.6. I* hosphorod~lhmale. cyclohexylphenol. dm~tro-. D~n~trophenol...... 25550587 ...... 1ow 2.5- 3297 15 2.6- 573568 Ulyl-pnitrophenyl 2.4-Den~trophenol...... 51285 Phenol. 2.4-din~lro-...... 1000 Din~lrotoluene...... 25321 146 ...... tow 3.4-D~n~lrololuene 6 10399 2.4-Dm~trotoluene...... 121 142 Bcnzene. t-melhyl-2.4- dmtlro-. houJSphorothmte. D~noseb...... 88857 Phenol. 2.4-d~n1tro-6-(t- melhylpropyl)-. Dt-n.octyl phlhalale ...... 1I7840 1.2-Eenzened~carborylc ac~d.di-n-oclylcsler. l.4.D1oxanc ...... 123911 1 1.4-Dethylene d~ox~de...... 1 1' DIFI4ENYLHYDRAZINE ...... I.2-Dtphenylhydrazme ...... D~phosphoramide. octamethyl-. phoranude. Dpropylamme ...... 142847 I-Propanamme. N- 1' ~orophosphale. P~PY~-. 621647 N-N~lrosodi-n- 1' propylamine. acd.O.O.dlmethyI S- 85007 ...... 1000 2764729 298044 0.0-Diethyl S-12- 1 (ethylth~o)ethyll phosph~r~d~lh~oale. 541537 Thm~mtdodsarbons I' d~am~de. D~thiopyrophosphoric 3689245 Telraelhyld~th~opyrophos- 1' phale. I acid. teraethyl ester. I 40 CFR Ch. I (7-1-88 Edition) Environmental Protection Agency TABLE 302.4-LIST OF HAZARDOUS SUBSTANCES AND REPORTABLE QUANTITIES- TABLE 302.4-LIST OF HAZARDOUS SUBSTANCES AND REPORTABLE QUANTITIES- Continued Continued [See lootnotes at end 01 Table 302.41 [!he lootnotes at end ol Table 302.41

SlalucOry FdRO

Hazardous Substance CASRN Regulatwy Synonyms RCRA RO Codel- Waste ~ounds~~g) Number

Ethanelhioamide...... 62555 Thioacelamlde...... 1' 4 U218 X I# (0454) Ethanol. 2.2- 1116547 N-NilroSOdiethanolamine.. 1' 4 U173 X t 6 (0 454) (n~trosoimino)bis-. Elhanone. 1-phenyl...... 98862 Acetophenone...... 1' 4 U004 D 5000 (2270) d1methanol.l.4.5.6.7.7- Ethanoyl chloride ...... 75365 Acelyl chloride ...... 5000 1.4 U006 D 5000 (2270) hexachloro. cyclic Elhenammne. N-melhyC 4549400 N- 1' 4 PO84 X 1# (0.454) N-nilroso-. Nitrosomethylvinyla- . Endosullan...... mine. Ethene,chloro- ...... 75014 Vinylchloride ...... 1' 2.3.4 U043 X 11(0.454) JDOSULFAN AND Elhene. 2chloroelhow.... 110758 2-Chloroetbyl vinyl ether ... 1' 2.4 U042 C I000 (4541 Ethene. 1.ldiio-...... 75354 1.1-D~chloroelhylene...... 5000 1.2.4 U078 D 50M)I (2270) Vinylidene chlor~de Ethene. 1.1.2.2- 127184 Telrachloroelhylene...... 1' 2.4 U210 X l# (0.454) IelracMwo-. dtcarboxylic acid. Ethene, trans-l.2- 156605 1.2-lrans- 1' 2.4 U079 C 1000 (45.0 dichloro-. Dichloroethylene. Hexachloro-6.7-epoxy- Ethii...... 563122 ...... 10 1 ...... A 10 (4 54) 1.4.4a.5.6.7.8.8a- 2-EthoxyeVMnol ...... 110805 Ethyiene gly~d 1' 4 U359 X 1# (0.454) octahydro-endo.endo- monoethyl ether. 1.4:5.8- Elhyl acetate ...... 141786 Acetic aca, ethyl esler ..... 1. 4 U112 0 KXK)12270l dimelhanonaphlhalene. Elhyl acrylate ...... 140885 2-Propenoic acid, elhyl 1' 4 U113 C 1000 (454) ~dr~naldehyde ...... 7421934 ...... 1' 2 ...... X 1 (0.454) ester. JDRlN AND ...... z ...... 1' 2 ...... • . Elhylbenzene...... 100414 ...... 1.2 ...... C IWO (4%) METABOLITES. Elhyl carbamate 51796 Carbamic acid, ethyl 1 4 U238 X l# (0 454) ~~hlaohydrm...... 106898 l-CM010-2.3- loo0 1.4 U041 c 1000#(454) (Urethan). ester. epoxypropane. Ethyl cyanide...... 107120 Propanenilrib ...... 1' 4 PI01 A 10 (4 54) Oxrane. 2- Elhyl4.4'- 510156 Benzeneacetic acid. 4- 1' 4 U038 X 11(0.454) (chl0rornethyl)- diihlorobenzilate. chloro-alpha-(4- sinephrine ...... 51434 1.2-Benzenodd. 4-[l. 1. 4 Po42 C 1000 (454) ch1orophsnyl)- alpha- hydroxy.2- hydroxy-. elhyl esler. (m~hylamino)elhyll.. Ethylene dibromide...... 106934 Ethane. 1.2-d~brorno-...... 1000 1.4 U067 C I0006 (4%) wnal ...... 75070 Acetaldehyde ...... 1000 1.4 U001 C 1000 (454) Ethylene dichloride ...... 107062 1.2-Drhloroelhane ...... 5000 1.2.4 U077 D SOW# (2270) ianamine. 1.1 - I22098 atpha.alpha- 1' 4 W46 D 5000 (2270) Ethane. 1.2-dichloro- jirnethyl-2-phenyl-. bmethylphencthyla- Ethylene oxide ...... 75218 Oxirane...... 1' 4 Ul15 X 1# (0 454) rmne. Ethylenebs 111546 1.2- 1' 4 U114 0 "(2270) ianamine. N-ethyl-N- 55185 N-Nitrosodiethylamine ...... 1' 4 U174 X 16 (0.454) (dithiocarbamic acid). Ethanedtylbiscarbamo- ?tlroso-. dilhii acid. lane. 1.2-dibromo-...... 106934 Ethylene d~bromide...... 1000 1.4 U067 C I0006 (454) Elhylencdiamine...... 107153 ...... 1000 1 ...... D 5000(2270) mne. 1,l-dichloro-...... 75343 1.l-D~chloroclhane ...... 1' 2.4 U076 C lo00 (454) Ethytencd~am~ne 60004 ...... 5000 1 ...... D 5000(2270) Elhylldene dichloride tetraacetii acid lane. 1.2-dichloro- ...... 107062 1,2-I)1chloroelhano ...... 5000 1.2.4 U077 D 50006 (2270) (EDTA). Ethyleno dchlorlde Elhylenc glycol 110805 2-Ethoxycthanol...... 1. 4 U359 X 16 (0 454) me. 1.1.12.2.2- 67721 Hcxachlorocthane ...... 1 2.4 Ut31 X I# (0.454) monoethyl ether. rxachloro-. Elhyleneth~wrea...... 96457 2-lm1dazot1d1nelh1one...... 1' 4 Ut16 X l# (0454) lane. 1.1'- 11191 1 Bls(2-chloroethoxy) 1' 2.4 U024 C 1000 (454) Elhylen~mine...... 151564 Azir~dtne...... 1' 4 W54 X 1# (0 454) Imethylenebs(oxy)J methane. Elhylelher ...... 60297 Ethane.l.l'-oxyb~s- ...... 1' 4 U1t7 B lo0 (45.4) *e-chloro-. Ethylidene dichlod...... 75343 1.1-D~chloroethane...... 1. 2.4 U076 c loo0 (454) )am. 1.1'-oxybn- ...... 60297 Ethyl ether ...... 1' 4 U117 B 100 (45.4) Ethane, 1.1-dchloro- lane, 1-1'-oxybls(2- 111444 6is (2-chlwoeihyl) eVrw ... 1 ' 2.4 U025 X 11(0.454) Ethyl methacrylale...... 97632 2-Propenoic acid. 2- 1 4 Ull8 C 1000 (454) :lllore. methyl-. ethyl ester. DlcMoroeIhyl ether Ethyl melhanesutlonate.... 62500 Melhanesullonic ac~d. 1' 4 U119 X 16 (0.454) lane. pentachloro-...... 7601 7 Pentachlorwthane ...... 1 4 U184 X 16 (0.454) elhyl ester. lane, 1.1.1.2- 630206 1.1.1.2- 1' 4 UXU) X 11(0.454) Famphu...... 52857 Phosphotolhioic ac~d. 1 4 W97 c loo0 (454) elrachloro-. Tetrachloroethana. 0.0-dimethyl-0-Cp lane. 1.1.2.2- 79345 1.1.2.2- 1' 2.4 U209 X 16 (0.454) [(d~melhylamino)- etrachloro-. Telrachloroethane. wllonyllphenyll ester. lane. 1.1.2-VichlMO- ..... 79005 1.l.2-Trichloroethane ...... 1' 2.4 U227 X 11(0.454) Fetric ammonium citrete... 1185575 ...... I000 1 ...... C 1000 (4541 lane. 1.1.1-Oichloro- 72435 Methoxychlor...... 1 1.4 u247 x 1 (0.450) Ferric ammonium 2944674 ...... lo00 1 ...... c loo0 (454) ?.2-bis(p- oxatate. nelhoxyphenyi)-. 55488874 11 1546 Elhylencbis 1 4 U114 D 5000 (2270) Ferric chloride 7705080 ...... 1 ...... C tooo (454) Ithanediylbscarbemo- ...... (dithiocarbamic acid). Feriit daban 9004664 Iron dexlran "'...... 4 U139 0 5000 (2270) Lth~oicacid...... l'y Ferric fluoride ...... 7783508 ...... 100 1 ...... B 100 (45.4) banenitrile ...... 75058 Acetonilrii...... 1. 4 5004 U003 ti (2270) Fwrii nilrate ...... A 10421484 ...... 1000 1 ...... C lOOO(454) )2.4 40 CFR Ch. 1 (7-1-88 Edition) Environmental Protection Agency 5 302.4

ABLE 382.4-LIST OF HAZARDOUS SUBSTANCES AND REPORTABLE QUANTITIES- TABLE 302.4-LIST OF HAZARQOUS SUBSTANCES AND REPORTABLE QUANTITIES- Continued Continued [Sea lmlnoles a1 end ol Table 302.41 [See foolnotes at end 01 Table 382.41

Stalclory Flnal RO Slatulery Irdous Subslance CASRN Regulatory Synonyms RCRA CaFgo. Hazardous Subslance CAN Regulalwy Synonym RCRA RQ Codet Waste Pounds(Kg) 1 /a0 Code; Waste Number Number

sullale ...... 10028225 ...... 1008 1 ...... C lo00 (454) Herachloroherahydro- 1.2.3.4.10.10- 4 Po60 IS ammeniw 10045893 ...... 1000 1 ...... C lOOO(454) endo.endo- Hexachlore- 318. dmlhanonaphlhalene. 1.4.4a.5.8.Ba- IS chbride...... 7759943 ...... 100 1 ...... B 100 (45.4) hexahydro- 1.4.5.8. ~tsultate...... 772Q787 ...... 1MIB 1 ...... C lm(454) endo.endo- 778263'3 d~melhanonaphlhakne 9acelic acid. 62748 Acelic ac~d.Iluoro-. 1' 4 PO58 A 10 (4.54) 1.2.3.4.10.10- Hexachlwohexahydro- 4 W60 ~wsalt. setlium salt. Hexachloro- endo.ends- .nlhene...... 206448 Benze[j.kllluwene ...... 1' 2.4 U120 I 100 (45.4) 1.4.4a.5.8.kla- Lmelha-ne me ...... 86737 ...... 1' 2 ...... D SOOO(2270) hexahydro- 1.4.5.8- ...... 7782414 ...... 1. 4 PO56 A 10 (4.54) endo.endo- dlmelharonophthrkme. ,acebmde ...... 640197 Acelamide. 2-lluaro-...... 1' 4 PO57 6) 100 (45.4) ~Uehyde...... 5W Mdhyleneoxide ...... 1008 1.4 U122 C 1oo0X (454) 1.2.3.4.10-10- 1.2.4 PBM Hexachlorct :acid ...... 64186 Methan& ad...... Sew 1.4 U123 D SBOB (2270) nc acid, mercury(1lj 628864 Mercury fulminaM ...... 1. 4 PO65 A 10 (4.54) 1.4.4a.5.8.8a- hexahydrel.4:5.8- en&. exo- n:aW ...... 110178 ...... 1 ...... D 50W(2270) dwnelhanonaphlhalene...... 11- Furfuran ...... 1 4 U124 I 1BO (45.4) Haxachbophena...... 783W 2.2.-MelhykmebiY3.4.6 4 U132 . tetrahydro...... 109999 Telrahydrelwan...... 1' 4 U213 C lBBB(454) lrichkephmey. markaldehyde .... 9801 1 Fwiual...... lm 1.4 U125 B 5m(2278) 1888717 l-Repene. 1.1.2.3.3.3 4 U243 1800 1454) nandhe 198316 Maieicanhydriie U147 ...... 5m 1.4 D 5080(2270) hcuchlars. at ...... 9-1 1 2-FuranchxaMcW .... 1- 1.4 U125 D Xm (2278) an Hexaelhyl 757584 Tebaphespheric a- 4 Po62 lea (45 4) ...... 11Bm Furan...... 1' 4 U124 6) 10D (45.4) telraghesphale. hexaelhyl ester. :oi-yransse. 2- lB089C64 Sbeptozolocin ...... 1. 4 U206 X 11(0.454) Hydrazmne ...... 302@12 Dimin...... 4 U133 1X 10 454) xy-2-(3-melhyl-3- Hytuine. 1.2-dklhyl-...... 7615Wl N.W-Dielhylhydrazine ...... 4 U086 1 I0 454) nnreids).. n Hydrazine. 1.1-dimethyl- ... 57 147 1.1-Dimelhylhydrazme ...... 4 U098 I# (0454) #aldehyde...... 765344 1-Prepanal. 2.3-epoxy- 1 4 ...... ' U126 X 11 (0.454) Hydrazine. 1.24melhyl- ... 540738 1.2-Dimethy(hy*uine ...... 4 U099 la (0 454) 3m@. N-mtr.s~-N- 78257 N-Melhyl-N'-nitro-N- 1 4 ' U163 X 11(0.454) Hydrazine. l.2-ckphenyl- ... 122667 1.2-Oiphenvlhyhazim...... 2.4 UIW 1 (0 454) hyl-N'-nitro-. niboreguanidine. * Hydrazine. methyl- ...... 68344 Mewhydrazw ...... 4 PO68 10 I4 54) m ...... 06511 ...... 1 I ...... X 1 (0.454) Hydrazinecarbathisamide. 79196 ThiesernicarM...... 4 PI16 1K (45 4) ETHERS ...... I' 2 ...... Hydrochloric acid ...... 7647010 ...... 1 ...... 5000 12270) HETHANES ...... 1 2 ...... Hydrocyanic acid ...... 74908 Hydrogen cyanide ...... 1.4 PO63 10 14 54) *11w ...... 76448 4.7-Mclhano-1H- 1 1.2.4 PO59 X 1U(0.454) Hydrolluoric acid ...... 7664393 Hydrogen fluoride ...... 1.4 U134 100 (45 4) 1ndeno.l.4.5.6.7.8.8- Hydrogen cyantde ...... 74W9 Hydrocyanlc acid ...... 1.4 PO63 10 14 54) hcplachloro-3a.4.7.7a- Hydrogen fluoride ...... 7664393 Hydrelluor~cacid ...... 1.4 U134 100 (45 4) telrahydro-. Hydrogen phosphide ...... 7803512 Phosph~ne...... 4 PO96 loo (45 4) 4CHLOR AN0 ...... 1' 2 ...... Hydrogen sulbde ...... 7783064 Hydresulfwic ad...... 1.4 U135 1oo (45 4) rABOLITES. Sulfur hydr~dc :Illor cpoxlde ...... 1024573 ...... 1' 2 ...... X 11 (0 454) 00159 a1pha.alpha- 4 U096 10 14 54) IhgrOBenzene...... 118741 Benzcnc. hcxact~loro-...... 1. 2.4 U127 X 11(0.454) O~melhylbenzylhydr~- Illorebulachene...... 87603 1.3-Bulad~ene. 1' 2.4 U128 X 11(0.454) peroxide. 1.1.2.3.4.4-hexachloro-. Hydrosulfuricacid ...... I 7783064 Hydrogen suI11de ...... 1.4 U135 ZHLOROCYCLO 608731 ...... 1 2 ...... Wlur hydrde .ANE (all Isomers) Hydroxydimelhylarsine 75605 Cacodyllc aad...... 4 U136 hlorocycloherane 58899 gamma .BHC ...... 1 1.2.4 U129 X 11(0.454) oxide. nma Isomer). 2-lmdazolidinclh~one...... 96457 Elhylenethwea ...... 4 U116 Lindane Indeno(l.2.3sd)pyrene ..... 193395 1.10-(1.2-Ph8nylene)pyrene. 2.4 U137 hlorocyclopenta- 77474 1.3-Cyclopenladiene. 1 1.2.4 U130 X I# (0.454) 10. 1.2.3.4.5.Chexachloro-. Iron dexlran "'...... 9004664 Ferric dexlran "'...... 4 U139 1.l0.10- 72288 Endrin...... 1 1.2.4 PO51 X 1 (0.454) lsobutyl akW...... 78831 I-Propanot. 2-melhyl-...... 4 U140 achloro-6.7-epoxy- lsocyanic acid. melhyl 624839 Methyl isocyanate...... 4 Po64 ia.5.6.7.8.8a- ester. hydro-endo.endo- Isophorone...... 78591 2 5.8- ...... Isoprene ...... 78795 1 ...... 2lhanonaphlhalene. lsopropanolamine 42504161 1 ...... l.10.10- 60571 Dieldrin...... 1 1.2.4 PO37 X 11(0.454) dodecylbenzenesullon- achloro-6.7-epoxy- ate. 4a.5.6.7.8.Ba- Isosalrole...... 120581 Benzene. 1.2- 4 U141 hydro-endo.exo- * melhylenedioxy-4- 5.8- ?thancnaphthdene. propew-. J(2H)-lsoxambne, 5- 2753964 5-(Aminrnnelhyl)3- 1. 4 W07 hioroelhane 67721 ...... Ethane. 1.1.1.22.2- 1' 2.4 U131 X 11(0.454) (amnomethy!).. oorazolol. hexachloro-. Kellhane.- ...... I 115322 . 5000 1 ...... - 302.4 40 CFR Ch. 1(7-1-88 Edition) Environmental Protection Agency 5 302.4 TABLE 302.4-LIST OF HAZARDOUS SUBSTANCES AND REPORTABLE QUANTITIES- ! TABLE 302.4-LIST OF HAZARDOUS SUBSTANCES AND REPORTABLE QUANTITIES-- Continued Continued [See lwlnolcs at end of Table 302 41 [See lwtnolcs a1 end of Table 302.41 - ---. -- I---- I - - Statutory F~nalRO ACR A zdous Substance CAR Regulatory Synonyms RCR A Hazardous Substance CASRN Regulatory Synonyms Catego- 1 1 Code; Waste Pounds(Kg1 "I Numhn, k Number -- - . - --- -. ------

Mcthane. 4 U075 D 5000 (2270) dtchlorod~lluoro-. Methane. lodo-...... Methyl iod~de...... 4 Ut38 X IX (0 454) pentalen.2-one. Methane, oxyb~s(chloro-... Be(chloromcthyl)ether ..... 4 POI6 X 1W (0 454) .docarpme ...... 303344 ...... 1' 4 U143 X Methane, tetrachtoro-...... Carbon tctrachlor~de...... 1.2.4 U2t I D 500011 12270) ~d t 1 ...... 7439921 ...... 1' 2 ...... X Methane. tetranltro-...... Tetran~trornethane...... 4 PI12 A I0 (4 54) ~dacetate ...... 301042 Acettc ac~d.lead salt...... 5000 1.4 ~144 Methane. tr~bromo-...... Bromolorm...... 2.4 U225 8 100 (45 4) \D AN0 ...... 1' 2 ...... Mcthane. truhloro- ...... Chloroform...... 1.2.4 U044 0 500011 (2270) ;OMPOUNDS. Methane, trichlorotluoro-... i Trichl~omono~luoro- 4 U121 0 5000 (2270) ~d arsenale 7704409 ...... 5WU (2270) 7645252 Melhanesullonic acid. 1 Et~%~~nesullonate.... 4 U119 X IW (0 4%) 10102484 ethyl ester. ld chloride ...... 7758954 t00w (45.4) MeWanelhiol ...... 74931 Methylmercaptan...... 100 1.4 U153 B 100 (45 4) d lluoborale...... 130 14965 toow (45.4) Thiimethanol ld fluoride ...... 7783462 loow (45.4) Methanesulfenyl 594423 Trichloromethanesulleql 1' 4 PI18 B too (45 4) ld iod~de...... I0101630 loow (45.4) chloride. triihloro-. chlonde. ~d n~trate...... 10099748 toon (45.4) 4.7-Methano-1H- 76448 Heptachlw ...... 1 1.2.4 PO59 X I17 (0 4541 Id phosphate 7446277 ...... Ir (0.454) indene.1.4.5.6.7.8.8- hcptachloro- 50001 (2270) 3a.4.7.7a-letrahydro-. Methanor: acid...... Formic acid...... 5000 1.4 Ut23 D SO00 (2270) 4.7-Methanoindan. Chlordane ...... 1 1.2.4 U036 X 1X (0 454) 1.2.4.5.6.7.8.8- Chlordane. technical ~d subacelate...... I# (0.454) octachloro- 3a.4.7.7a- ~d sulfate...... 1008 (45.4) tetrahydro-. Methanol...... Methyl alcohol...... 4 Ut54 D 5000 (2270) ld sulfide...... 50008 (2270) Methapyrilene...... Pyriine. 2- [ (2- 4 Ut55 D 5000 (2270) ad thcyanale ...... toon (45.4) (dimethy1amino)ethyl)- dane ...... gamma . BHC ...... I# (0.454) 2-thenylaminol-. Hexachloroqclohexane Acetlmidic acid. N- 4 PO66 B 100 (45 4) (gamma isomer) [(methylcarbamoyl)oxyl ~lumchromate ...... 14307358 ...... 1000r (454) thio-. methyl esler. X 1 (0 4%) lalh~on...... 121755 ...... too (45.4) Ethane. t .I.I -trichloro- 1.4 U247 le~cacld ...... ttOl67 ...... 5000 (2270) 2.2-b~s(p- leic anhydrtde...... 108316 2.5.Furand1one...... 5000 (2270) methoxypheny1)-. D 5000 (2270) le~chydraade ...... I2333 I 1.2.Dlhydr0.3.6- 5000 (2270) Melhyl alcohol...... Mclhanol...... 4 Ut54 pyr~daz~ncdtone. 2-Methylaz~r~d~ne ...... t .2.Propylcn1mlne...... 4 PO67 X 111 (0 454) I000 (454) Propanrd~n~tr~lc...... loo0 (454) Methyl brom~rle...... Methane. bromo- ...... 2.4 U029 C I00 (45 4) Atanme. 3.lp.b1s(2. I# (0.454) 1-Mett~ylbutad~cne...... 1.3-Pentarlocnc ...... 4 U186 B cl~lorocthvl)am~nol Methyl chlorido...... Methane, chloro- ...... 2.4 U045 X I11 (0454) Metlyl chlorocarbo~te... Carbonochlondi acld. 4 U156 C two (454) rcaptod~melhur...... methyl esler. rcurlc cyan~de...... Mcthyl chlorolorm...... 1.1.1-Tr~chloroetl~ane..... 2.4 U226 C 1000 (454) ~CU~ICnosate ...... 4.4'.Melhylcneb1~(2- Benmnamlne. 4.4'- 4 U158 X IX (0 454) rcuri sul1atc ...... chloroarstmc). methylenebs(2-chloro-. rcur~cthicyanate ...... 2.2'-Mothylcncb1s(3.46 Hcxachlorophene...... 4 Ut32 B 100 (45 4) ~CU~OUSmlrato ...... trchlorophcnol). rcury ...... 3-Methylcholantl~rene...... Bcnzl~lacca~~ttirylene. 1' 4 Ut57 X 1X (0 454) RCURY AND 1.2-d~hydro.3-mcthyl-. ;OMPOUNDS. Mcthylcne brom~de...... Mcthane. d~bromo-...... 1' 4 U068 C 1000 (454) rcury. (acelato- 62384 Phenylmcrcurtc acetate .... Mctt~ylcr~cchlorldo ...... Mclhane. dchloro- ...... I. 2.4 U080 C I000 (554) ))phenyl-. I I Mcll~ylcneox~dc ...... Famaldeliyde ...... 1000 1.4 Ul22 c 1M)OI 1454) rcury tulmmate ...... Methyl ethyl ketone...... 2-Butanone...... I' 4 U159 D 5000 (2210) Methyl ethyl ketone 2-Butanone pcrox~de...... I' 4 U160 A 10 (4 54) .thacrylon~tr~le...... perox~dc. Methyl hydrazine...... 60344 Hydrazinc. methyl- ...... 1' 4 PO68 A I0 (4 54) ...... Methyl lod~de...... 74884 Methane.~odo-...... 1' 4 Ut38 X IX (0 454) .thane. bromo- ...... I Methyl isobulyl ketone...... tO8tOt 4-Methyl-2-pentanone ...... 1' 4 Ut61 0 5000 (2270) Methyl ~sccyanate...... 624839 lsocyan~cac~d. mclhyl 1' 4 PO64 X I1111 (0 454) ester. 75865 Acetone cyanohydrm ...... 10 1.4 PO69 A 10 (4 54) 1000 (454) Propanenttr~le.2- looo (454) hydroq-2-methyt- I 5 302.4 Environmental Protection Agency 5 302.4 40 CFR Ch. 1 (7-1-88 Edition) 1 TABLE 302.4-LIST OF HAZARDOUS SUBSTANCES AND REPORTABLE QUANTITIES- TABLE 302.4-LIST OF HAZARDOUS SUBSTANCES AND REPORTABLE QUANTITIES- Continued Conlinued ISoe footnotes end of Tablo 302 41 [See footnotes at end ol Table 302.41

Statutory F~nalRO Hazardous Substance CASRN Regulatory Synonyms RCRA Hazardous Substance CASRN Regulatory Synonyms RCRA Catego- Catego. A0 Codet Waste Pounds(Kg) Code. Waste Number 'Y Number I I I . .- .- - . -.. .- .-- .-- . - - - - Ucthylmercaptan...... 74931 Methanelniol...... 100 1.4 U153 B loo (45.4) Nickel cyan~de...... Nickel(ll) cyamdo ...... 4 PO74 X Thtomelhanol N~ckel(lt)cyanide ...... N~cketcyande ...... 4 PO74 x Methyl methacrylate...... 80626 2-Propencic acid. 2- 5000 1.4 U162 C 1000 (454) N~ckelhydroxode ...... 1 ...... C methyl-, methyl ester. Nickel nltrato ...... 1 ...... 0 "l.Mrthyt-N'-mto-N- 70257 Guan~dine.N-n~troso-N- 1' 4 Ut63 X 11(0.454) N~ckdsulfate ...... 1 ...... D nttrosoguanidtne. mett~yl.W-nitro-. Nrkel telracarbonyl ...... Nickel carbonyl ...... 4 PO73 X Methyl paralhon ...... 298000 O.O.D~methyl O-p- to0 1.4 PO71 B loo (45.4) Nrobne and salts...... Pynd~ne.(S)-3-(1.mcthyt- 4 Po75 B rutrophenyt 2.pyrroI1dmnyt)-. and pliosphorothioate. sat1s. 4-Methyl-2-pentanone...... 108101 Methyl is&utyl ketone...... 1' 4 U161 D 5000 (2270) Nitric acid...... 1 ...... C Welhyllhiouracil ...... 56042 4(1H)-Pyrimidinone. 2.3- 1 4 U164 X lU(0.454) Nitric oxide...... N~troyen(tl)oxide ...... 4 PO76 A diidrob-melhyl-2- p-Nitroaniline...... Benzenamme. 4-11111 o-.... 4 W77 D thioxo-. Nitrobenzene...... Benzene. nitro- ...... 1.2.4 Ut69 C Wev~nphos...... 7786347 1 1 ...... A ...... 10 (4.54) Nitrogen dioxide...... Nitrogen(tV) oxide ...... 1.4 PO78 A Wexacarbate...... 315184 ...... 1000 1 ...... C 1000(454) WttomycinC...... 50077 Azuino(2'.3':3.4)~~oto(l. 1' 4 U0lO X 11(0.454) Nttii oxide 4 PO76 A 2-a)1ndote-4.7-dtone.6 Nitrogen(tl) oxide ...... amino-& Nilrogen(lV) oxide...... Nilrogen d~oxide...... 1.4 PO78 A ~((amtnocarbonyt)oxy) I I methyll. 4 PU81 A 1.la.2.8.8a.Bb- hexahydro8a- Nitrophenol (mixed) ...... 1 ...... B methoxy- 5-methyl-. m- i4onoelhytamtne...... 75047 ...... 1000 1 ...... B 100 (45.4) 0. 2-N1trophmml Wonomethylam~ne...... 74895 ...... 1000 1 ...... 8 lo0 (45.4) P 4-Nttrophenot Valcd ...... 300765 ...... 1 ...... A to (4.54) Phenol. 4-n~tro- i.l2~Naphthacemdmne. 20830813 Dau~myan...... ;? 4 U059 X I# (0.454) pNitrophenol ...... 4-Ntsophenol ...... 1.2.4 Ut70 B (8S-c1s).8-acelyl-lO- Phend. 4.n1tro- 13-amino-2.3.6- 2.N1trophend ...... O-N~trophenot...... 1.2 ...... D tr~deoxy-alpha-L-lyxo- 4-Nitrophenol...... p-Nttrophcnol ...... 1.2.4 11170 B heaopyranosyl)oxyI- Phenol. 4-n~tro- 7.8.9.10-tetrahydro- NlTROPHENOLS...... 2 ...... 6.8.1 1-1iiydroxy 1- 2.N1tropopane ...... Propane. 2-nilro-...... 4 Utll X mcthoxy.. NITROSAMINES...... 2 ...... Vaphthalene ...... 91203 ...... 5000 1.2.4 U165 B 100 (45.4) N-Nttros&~-n-bulylam~ne.. 1-Bulanamme. N.butyl- 4 U172 X Vaphthalene. 2-chtoro-..... 91587 bcta.Chloronaphlhalene ... 1' 2.4 U047 0 5000 (2270) N-n~lroso-. 2-Chloronaphthalene Ethanol. 2.2'- 4 U173 X 1.4-Naphthatenedme 130154 ...... 1.4-Naphlhoquinone...... 1' 4 U166 D 5000 (2270) (n~troso~m~no)Lns-. ?.7- 72571 U236 X Trypan blue ...... 1' 4 11(0.454) Elhanammne. N-cthvl-N- 4 U174 X Naphthalenedisullonrc acid.3.3'.t(3.3'- d~methyl.(1.1'. bpheny1)-4.4'-d~yl). bts(azo)lbis(5-ammo- 4-hydroxy). letrasod~urnsalt. Yaphthcnic ec~d...... 1338245 ...... 100 1 ...... B 100 (45 4) natroso.. f.4.Naphthoquinone ...... 130154 1.4-Naphthalcnedmne...... 1' 4 U166 D 5000 (2270) Carbamlde. N-methyt-N- t-Naphthylamine...... 134327 alpha-Naphthytamhe...... 1' 4 U167 X 11(0454) nltroso-. Z.Naphthylam~ne...... 91598 bela-Naphlhylammne...... 1' 4 U168 X 11(0454) N-N~troso-N- Carbarmc acid. ilphaNaphthylam~ne...... 134327 1-Naphthytarmne...... 1' 4 U167 X 11(0 454) molhylurelhane. I methvtmlroso-.ethyl -ma-Naphthykmme ...... 91598 2-Naphthylamine...... 1' 4 U168 X 11(0.454) I Z Naphlhylarmm. N.N- 494031 Chtornaphazine...... 1. 4 U026 X 11(0.454) bo(2-chlorocthyl)-. ~IphaNaphlhylIhiiea..... 86884 Thiourea. 1- 1. 4 PO72 8 100 (45.4) Mphthaleny(-. Y~ckelIt ...... 7440020 ...... 1' 2 ...... X 1I (0.454) NICKEL AND ...... 1' 2 ...... COMPOUNDS. Nitrotoluene...... Vckel ammonium I5699180 ...... MOO 1 ...... D MOO# (2270) m- I sulfa?. Vrkct c%rhnyl ...... 13463393 Nrkel tetracarbonyl ...... 1 4 PO73 X 11(0.454) V~ckelchlwide...... 7718549 ...... SM)O 1 ...... D MOO1 (2270) 3721 1055 1 302.4 40 CFR Ch. 1 (7-1-88 Edition) Environmental Protection Agency 8 302.4 I TABLE 302.4-LIST OF HAZARDOUS SUBSTANCES AND REPORTABLE QUANTITIES- TABLE 302.4-LIST OF HAZARDOUS SUBSTANCES AND REPORTABLE QUANTITIES- Continued Continued [See loolnoles at end 01 Table 302.41 [See footnotes al end 01 Table 302 41

- - Statutory Fmal RO ' I .--- Hazardous Substance CARRN Rewtalow Synonyms RCRA Hazardous Subslance CASRN Regulalory Synonyms RCRA I I RO Codel Wasle Catego- Pounds(Kg) RO code: Waste ~arnds(~g) Number ry Number .. .. -- .-

Norbornene-2.3- 115297 Endosullan...... Phenylmercurc acetate ... 62384 Mercury. (acelalo- 1' 4 PO92 B loo (45 4) d1mcthand.l.4.5.6.7.7- Olphenyl-. hexachloro. cycle I I N-Phenylth~wrea...... I03855 Th~owca,phenyl- ...... 1' 4 PO93 B too (45.4) Phorate ...... 298022 Phosphorod~lh~o~cacid. 1. 4 PO94 A 10 (4.54) D~phosptmrarnide. 1. .4 PO85 loo (45.4) 0.0-delhyl S- octamethyl-. (elhyllhlo) methyl Osmlum letroxide ...... 1' 4 PO87 ester. Osmium oxide ...... 1' 4 PO87 Phosgene...... 75445 Carbonylchloride...... 5000 1.4 PO95 A 10 (4 54) Endorhall...... 1' 4 PO88 Ptmphnre...... 7803512 Hydrogen phosphiie...... I' 4 PO96 B I00 (45 4) Phosphoric acid ...... 7664382 ...... 5000 1 ...... D so00 (2270) Phosphoric acid.dielhyl 311455 Diethyl-p-nilrophenyl 1' 4 Po41 B too (45.4) p-ntlrophenyl ester. phosphate. Phosphoric acid. lead 7446277 Lead phosphate ...... 1 4 Ul45 X I# (0.454) dl. Phosphwodithioic acid. 3288582 0.0-Diethyl Smelhyl 1' 4 U087 D 5000 (2270) 0.0-dielhyl S- dilhtophwphate. methylesler. Phosphorod~thiicadd. 298022 Phaate ...... 1' 4 PO94 A 10 (4 54) 0.0-d~elhylS- (ethyllhio) mew ,, ester. €p&hlo;bh;drin Phosphorodilhioic 60515 Dimethoale...... 1' 4 PM4 A 10 (4.54) aralormaldehyde...... 30525894 ...... low (454) acid.O.0-dimethyl S- 'araldehyde...... 123637 1.3.5-Tr'mxane. 2.4.6 low (454) [2(melhylamim)-2- 1 himethyl-. oxoethyll esler. Phosphorothioic 11(0.454) Phosphoroltwidic 55914 Diisopmpyl 1' 4 PM3 B lo0 (45 4) acid.O.0-diethyl 0-(P acid.bis(1-melhylelhyl) NuaOphosphate. nttrophenyl) esler. ester. 'entachbobenzene ...... 608935 Benzene. penlachbo...... 10 (4.54) Phospholothii 56382 Parathion...... 1 1.4 Po89 X In (0.454) 'enlachloroelhane ...... 76017 Elhane. penlachloro-...... 11(0.4541 and.o.O-~hylo-(P entacMoronilrobmzene.. 82688 Bcnzcne. I# (0.454) nibophenyl) ester. pentacMoronilr0-. PhosplwolluMC acid. 297972 0.0-Diemylo-pyrazinyl 1' 4 PO40 B 100 (45 4) 'enlachtorophend...... 87865 Phenol, penlachloro-...... tow (4.54) 0.0-d~elhylO phosphorothioatt3. .3-Penlad~ene...... 504609 1-Methylbutad~ene...... loo (45.4) pyrazinyl ester. 'henacetln...... 62442 Acela&. N-(4- l# (0.454) Phosphorothimc acid. 52857 Famphur...... 1' 4 PO97 C lOoQ(454) elhoxyphenyl).. 0.0-dmethyl O.[p- 85018 ...... SOM, (2270) [(dtmclhylamno)- 108952 Benzene. hydroxy-...... 1000 (454) sullonyllphenyll ester. 95578 2.Chlorophe nol...... loo (45.4) Phosphorus ...... 7723140 ...... 1 1 ...... X 1 (0 454) o-Chlorophend Phosphorus oxychtonde.... 10025873 ...... !jOWj 1 ...... C 1000 (454) 'hend. 4-chlor0-3- 59507 4Ghloro.m-cresd ...... so00 (2270) Phosphorus pentasutlde.. 1314803 Phosphorus sulri...... iw 1.4 U189 B 1w(45.4) methyl-. pChloro-m-cresol Sullw phosphiie 'henol. 2-cyclohexyl.4.6. 131895 4.6-D1nllro-o- loo (45 4) Phosphorus sullide ...... 1314803 Phosphorus penlasulfide.. 100 1.4 U189 B loo (45.4) dm~lro-. Cyclohexylphenol. Sulfur phorplude 'hehenot. 2.4-dicMa0- ...... 120832 2.4-Dichlorophend ...... loo (454) Phosphorus lrichlwide...... 7719122 ...... MOO 1 ...... C 1000 (454) 'henol. 2.6-dichloro- ...... 87650 2.6-DrhlcfophenOl ...... loo (45.4) PHTHALATEESTERS...... 1' 2 ...... nenol. 2.4-dimethyl- ...... 105679 2.4-O~melhylphenol...... loo (45.4) Phlhattc anhydride ...... 85449 1.2-BenzenedearboxyI'c I' 4 U190 D MM) (2270) 'hend. 2.4-dinilro- ...... 51285 2.4-D~nitrophenol...... 10 (4.54) acid anhydride. 'hend. 2.4-d~nivo-6-(1- 88857 Dinoseb...... loo0 (454) 2-Peolii...... 109068 Pyrid~ne.Z-melhyl-...... 1' 4 U191 D W)OO (2270) melh~Iprwo-. Plumbane, letraelhyt- ...... 78002 Tetraethyl lead ...... 100 1.4 PI10 A lo# (4.54) 'henot. 2.4-d1niIro-& 534521 4.6-hnitro-o-aes0l and 10 (4.54) POLYCHLORINATED 1336363 Aroclws ...... 10 1.2 ...... A 106 (4.54) melhyl-. and salts. salts. BIPHENYLS (PCBs). 'henol. 4-niW ...... 100027 p-Nilfophenol ...... loo (45.4) 12674112 Ardor 1016 4-Nilfophenol 11 104282 ArOClw I221 'henol. pentahluo- 1 lox (4.54) 1...... I 11 141 I65 Aroilor 1232 Ylenol. 2.3.4.6- to (4.54) 53469219 Aroclw 1242 tetrachloro-. Telrachlofophenol. 12672296 Aroclor 1248 'henol. 2.4.5-hehloro- ...... 95954 2.4.5-Trichtofophenol ...... ion (4.54) 11097691 Aroclor 1254 %not. 2.4.6-trichloro- ...... 88062 2.4.6-TrichlorophenoI ...... lo# (4.54) I1096825 Aroclor 1260 henol. 2.4.6-lrinitro-. 131748 Ammonium picrate...... 10 (4.54) POLYNUCLEAR ...... 1' 2 ...... ammonium sall. AROMATIC 'henyl dichloroarsine I I 11(0.454) HYDROCARBONS...... lo-(1.2- 16 (0.454) Polassium arsenate ...... 7784410 ...... I ...... c iooon(4sr) Pheny1ene)pyrene. Potassium arsenite...... -... 10124502 ...... 1000 t ...... C IOOO#(~W) 40 CFR Ch. 1 (7-1-88 Edition) Environmental Protection Agency

TABLE 302.4-LIST OF HAZARDOUS SUBSTANCES AND REPORTABLE QUANTITIES- TABLE 302.4-LIST OF HAZARDOUS SUBSTANCES AND REPORTABLE QUANTITIES- Conlinued Continued [See footnotes at end of Tablo 302.41 [See lootnotes at end of Tablo 302 41 F~nalRO

I4azardous Subslance

otass~umbshromate ...... Pyrene ...... otnsslum chromate ...... Pyrelhrins...... otassoum cyanlde...... otass~umhydroxtde ...... otasslum pcrmanganate. otass~umsliver cyanlde PO99 X 1 (0 151) Pyrtdlne. 2.[(2. ronamide ...... (d~methylam~no)ethyl)- 2-thenylam~nol-. -Propanal. 2.3-epoxy- ..... ropanal. 2-methyl-2- (methylthi0)--0- I(methytamino) carbonylloxime. -Propanamine...... -Propanamine. N- propyl-. th~oxo-. ropane. 1.2-dlbromo-3- chloro-. Pyrophosphor~cacld. tetraethyl ester. 'ropane. 2-nitro-...... :...... 'ropane. 2.2'-oxybis(2- chtoro-. .3-Propane sultone ......

'ropaned~nitrile...... 'ropanenitrlle ...... 'ropanenltrde. 3-chloro-. PO27 C 1000 (454) 'ropanen~tr~le.2- hydroxy-2-methyl-. .2.3-Propanetnol, tr~n~trate-. -Propanol. 2.3-d~bromo- , phosphate (3.1) .Propanof. 2.methyl- ...... '.Propanone ...... '.Propanone. 1-bromo-. 'ropargtte ...... 'ropargyl alcohol...... ' .Propenal...... COMPOUNDS !.Propenarn~de...... 'ropene. 1.3-drhloro-..... -Propene. 1.1.2.3.3.3- hexachloro-. !-Propenen~tnle...... !-Propenenibde, 2- methyl-. ?-Propenoicactd ...... !-Propenoic acid, ethyl SILVER AND ester. COMPOUNDS. !-Propenoic acid. 2- methyl-, ethyl ester. ?-Propenoicac~d. 2- methyl-. methyl ester. 2-Propen-1-01...... ='ropionic acld ...... Dropionic acid. 2.(2.4.5- trichlorophenoxy)-. lroplonic anhydride...... n-Propylamine ...... Propylene dichlonde ...... Propyle?e oxlde ...... 1.2.Propylenimine ...... 2-Propyn-1-01...... '02.4 40 CFR Ch. 1 (7-1-88 Edition) Environmental Protection Agency $302.4 rABLE 302.4-LIST OF HAZARDOUS SUBSTANCES AND REPORTABLE QUANTITIES- TABLE 302.4-LIST OF HAZARDOUS SUBSTANCES AND REPORTABLE QUANTITIES- Continued Continued [See lootnoles at end ol Table 302.41

Slalutory Fmat RO Slalulory F~nalRO !ardous Substance WSRN Regulalory Synonyms RCR A Hazardous Substance CASRN Regulatory Synonyms RCAA RO Codet Wasle PoundqKg) RO Code; Waste POunds(Kg1 Number - Number Cay rm dadecylbenzene 25155300 ...... 1000 1 ...... C lOOO(454) TDE ...... 72548 DDD ...... t 1.2.4 uom x 1a (0 454) fenale. 4.4' DDD rm fluoride...... 768 1494 ...... SO00 1 ...... c lOOO(454) Dichlorodtphcnyl jrn hydrosdlide...... 16721805 ...... 1 ...... D 500012270) d~chloroelhane Im hydroxide...... 1310732 ...... 1060 1 ...... C loo0 (454) 1.2.4.5- 95943 Benzene. 1.2.4.5- 1 ' 4 U207 D 5000 (2270) rrn hypochlorile...... 7681529 ...... 100 1 ...... B 100 (45.4) Tetrachlorobenzene. lelrachloro-. 10022705 2.3.7.8- 1746016 ...... 1' 2 ...... X I# (0.4541 rm melhylale...... 124414 ...... 1000 1 ...... C 1000 (454) Tebachlorodibenzo-p- rm nilrile ...... 7632000 ...... 100 1 ...... B loo (45.4) dioxin(TCD0). ~rnpbsphate. 7558794 ...... 5080 1 ...... D 5000 (2270) 1.1.1.2- 630206 Ethane.1 .l.l.2- 1' 4 U208 X 11(0.454) 'ask. 10039324 Telrachloroethane. ~achloro-. 10140655 1.1.2.2- 79345 Elhane. 1.1.2.2- 1' 2.4 U209 X 1# (0.454) ~rnphosphate. 7601549 ...... 5800 1 ...... D 5000 (2270) Tetrachloroethane. telrachloro-. pasic. 7785844 TelrachloroeUlylene...... 127184 Ethene. 1.1.2.2- I* 2.4 U210 X 1U (0 4541 10101890 tetrachloro-. 10361894 2.3.4.6- 58902 Phenol. 2.3.4.6- 1' 4 U212 A 10 (4.54) 7758294 Telrachlorophenol. tetrachtoro-. 10124568 Tetraelhytdilhiopyophos- 3W9245 Githiopyrophospharic 1' 4 P109 B 100 (45 41 dm selen~te...... 10102188 ...... tom 1 ...... B 100 (45.4) phale. acid.lelrae1hyt ester. 7782823 Tetraelhyllead ...... 78002 Plumbane.tetraelhyl- ...... 100 1.4 PllO A lo# (4 541 X Stilbenediol. 56531 Dielhylstilbeslrol...... 1' 4 U089 l# (0.454) Tetraethyl 107493 Pyrophosphoric acid. 100 1.4 PI11 A 10 (4 54) 8ha.alpha'-dlelhyl-. pyrophosphate. tetraethyl ester. U206 X I# (8.454) ~lorotocin...... 18883664 D-Glucowranose. 2- 1- 4 Telrahydroluran...... 109999 Furan. lelrahydro-...... 1' 4 U213 C 1000 1454) deoxy-2-(3-methyl-3- Tetranilromelhane ...... 509148 Methane.lelranitro-...... 1' 4 PI12 A 10 (4 54) nilrosoureido)-. Tetraphosphoric acid. 757584 Hexaethyl 1 4 PO62 B 100 (45.4) 1 C 1000#(454) ,!wm chmate...... 7789062 ...... 1000 ...... hexaethyl ester. tetraphosphate. ltiurn sulfide 1314961 ...... 1' 4 P107 B 100 (45.4) ...... Thallic oxide ...... 1314325 TWlium(llt) oxide ...... 1' 4 PI13 B 1W (45 4) :hnidin-1O~ne.and 57249 Strychnine and salts...... 10 1.4 PI08 A 10 (4.54) Thallium t t ...... 7440280 ...... 1' 2 ...... C lOOO(454) '1s. THALLIUM AND I' .. 1' 4 PO18 B 100 (4.54) ...... 2 ...... :hnidin-IO-one. 2.3- 357573 Brucine ...... COMPOUNDS. wlhoxy-. Thallium(1) acetate ...... 563688 Acetic acid. thalliurn(1) 1' 4 U214 B 100 (45 4) hnine and salls 57249 Strychnidin-10-one. and 10 1.4 PI08 A 10 ~1.54) ...... salt. salts. Thall~um(l)carbonate ...... 6533739 Carbonic acid. 1' 4 U215 8 100 (45 4) ,ne ...... 100425 ...... 1OW 1 ...... C 1000 (454) d~lhall~um(l)salt. r hydride ...... 7783064 Hydrogen sullide...... 100 1.4 Ul35 B 100 (45.4) Thall~um~llchlor~de...... 7791120 1' 4 U216 1W 145 4) Hydrosulfur~cacid ...... B Thall~um(l)nilrale ...... 10102451 1' 4 U2t7 B lo0 (45 41 r rnonochlonde...... 12771083 ...... 1000 1 ...... c 1000 (454) ...... Thalhumllll) omdc ...... I314325 1' 4 P113 B cW (45.4) r phosphlde ...... 1314803 Pt~osphoruspcnlasulf~de .. 100 1.4 U189 B 100 1-45 41 Thall~coxde ...... 4 Phosphorus sull~de Thallum(l) sclcrude ...... I2039520 ...... 1' PI14 C I000 (4541 rsclenlde ...... 7188564 Selen~umd~sullide...... I' 4 U205 X 1# I04541 Thall~um(l)sullale ...... 7446186 Sullurlc acd. lhall~um(l) 1000 1.4 PI15 B 100 (45.4) ric acid ...... 7664939 .....: ...... 1000 1 ...... C lOOO(4541 10031591 salt. Thtoacetamide 8014957 ...... 62555 Elhanelhioamide...... 1' 4 U218 X 1U (0.454) ric acid, dlmerhyl 77781 Dimelhyl sullale ...... 1. 4 U103 X la (0.454) Thiolamx ...... 39196184 3.3-D~melhyl-1- 1' 4 Po45 B 100 (45.4) :er. (rnelhy1lh1o)l- rlc acid, Ulalltum(l) 7446186 ThaIlium(1) sullate ...... $000 1.4 P115 B 100 (45 4) bulanone.0- 1. 10031591 [(mclhylam~no) -T ...... 93765 2.4.5-7 acid ...... 100 1.4 U232 C lOOO(454) carbonyll oxune. 2.4.5-Trichtorophenoxy- Th~oim~dodicarbonic 54 1537 2.4-01th1ob1uret...... 1' 4 Po49 B 1W (45 4) dtarnlde. acetic acid -T ac~d...... 93765 2.4.5.T ...... 10Q 1.4 U232 C 1000 (454) Thimmelhad ...... 74931 Methanethd ...... 10Q 1.4 U153 B lo0 (45.4) 2.4.5-Tnchlorophenoxy- Melhylmercaplan acetlc acd Thiophenol...... 108985 Benzenelhiol...... 1' 4 PO14 8 100 (45 4) -T amines ...... 2008460 ...... 1W 1 ...... 0 so00 (2270) Thiosemicabzide...... 79196 Hydrazinecarbolhioamide. 1' 4 PI16 B 100 (45 4) 6369966 Thiourea ...... 62566 Carbarrude. lhio- ...... I' 4 UZ19 X 1U (0.454) 6369977 Thmurea. (2- 5344821 I-(+ 1' 4 PO26 8 lo0 (45.9 1319728 chlorophmyl)-. Chlorophenyl)lhmurea. 3813147 Thiourea. 1- 06884 alpha-Naphlhytthmursa..... 1' 4 PO72 B 100 (45 4) -T esters ...... 93798 ...... 100 1 ...... C 1000(454) naphthalenyl-. 2545597 Thiourea. phenyl-...... 103855 N-F'hmylthmurea...... 1' 4 Po93 B lo0 (45.4) 61792072 Thaam 137268 Bas 1- 4 U244 A 10 (4.54) 1928478 (dirnelhyllhtocarba. 25168154 ItIOylI disullde. -T salts...... 19560991 ...... 1W 1 C 1000 (454) Tdvene ...... 108883 Benzene. methyl-...... 1000 12.4 U220 C 1WO (454) 02.4 40 CFR Ch. 1 (7-1-88 Edition) Environmental Protection Agency 8 302.4 I rABLE 302.4-LIST OF HAZARDOUS SUBSTANCES AND REPORTABLE QUANTITIES- TABLE 302.4-LIST OF HAZARDOUS SUBSTANCES AND REPORTABLE QUANTITIES- Continued Continued [See loolnoles a1 em of Table 302.41 [See foolnotes at end ol Table 302.41

Staluloly Fmal RO zardous Substance CASRN Regulaloly Synonyms RCRA RO ~odet Waste ~ounds(~g) Number Cay-- mnediamine...... 95807 Diaminololuene...... 1' 4 U221 X 1# (0.454) 25376458 496720 823405 me drisocyanale ...... 584849 Benzene. 2.4- 1' 4 U223 B I00 (45.4) biphonyl)-4.4'-d1yl)- d~isocyanatomelhyl-. ba(azo)Ibls(5-amino- 91087 26471625 luid~ne...... 95534 2-Ammo-1-melhyl 1. 4 U328 X l# (0.454) Unltsled Hazardous benzene. Wastes Characlertslic Of EP Toxlclly. luidine ...... 106490 4-Amino-1-methyl 1. 4 U353 X 1# (0.454) benzene. luidine 636215 Benzenamine. 2-methyl-. 1' 4 U222 X 1# (0.454) drochloride. hydrochloride. ~phene...... 8001352 Campheno. oclachlor0- .... 1 1.2.4 PI23 X l# (0.454) 4 Do03 B (45.4) -7Pacid Propionicacid. 2-(2.4.5- 100 U233 B 100 (45.4) loo ...... 93721 1.4 ReacC~ily. 1richlorophenoxy)-. 4 . . Sihrex ...... >-TPacid eslers ...... 32534955 ...... 100 1 ...... B 100 (45.4) 4 DO04 X IX (0 454) .2.4-Tr1azd-3-amine... 61825 Amtlrole 1' 4 UOll X 11 (0.454) ...... 4 Do05 C 1000 (454) ~lorlon 52686 1000 1 ..,...... B 100 (45.4) ...... 4 W06 X 1# (0 454) I-Tr~chlorobenzene 120821 ...... 1' 2 ...... B 100 (45.4) ..... 4 0007 X la (04541 .Trichloroclhane 71556 Mclhyl chlorolorm 1' 2.4 U226 C 1000 (454) ...... 4 WO8 X 1##10454) !-Trachloroelhane 79005 Elhane. 1.1.2.lrrhlcfo- 1' 2.4 U227 X 1# (0 454) ...... 4 Do09 X 1 (0 454) ~loroelhene 79016 Trichloroelhykne 1000 U228 C lOOOU (454) ...... 1.2.4 4 0010 A 10 (4 54) lloroelhylene 79016 Trchloroelhene 1000 U228 C *OW# (454) ...... 1.2.4 4 W11 X 1 (0454) ~loromelhanesullenyl 594423 Melhanesullcnyl 1. 4 PI18 0 lo0 (45.4) 1.4 DO12 X 1 (0 454) lcf~de. chlordc. lrrhloro-. 1.4 1)013 X Id (0 4541 ~loromonolluoro- 75694 Methane. trichlorolluoro- 1' 4 U121 0 5000 (22701 ... 1.4 W14 X 1 (0 454) ?thane. 1.4 0015 X 1# (0.4541 tlor-d 25167822 10 1 A lo# (4.54) ...... 14 DO16 B lo0 (45 4) 2.3.4. 15950660 1r~chlorophonol 4 U237 X 11 (0 454) 2.3.5- 933788 chlotoclhyl)am~nol-. rchlorophenol 1 4 U237 X 1U (0 454) 2.3.6. 933755 Trchloroptwnol I ...... 0 loo (45 4) 2.4.5. 95954 Phcnol. 2.4.5.lrichloro- 1 ...... B lo0 (45 4) Tr~chlorophenol 4 PI19 c 1000 (454) 2.4.6- 88062 Phenol. 2.4.6-trichloro- Trchlofophenol 3.4.5- 609198 Tr~chlorophenot 1 ...... C looO(454) 5-Tr~chlorophend...... 95954 Phenol. 2.4.5-lrichloro- ...... 10 1.4 U230 A lo# (4.54) 5-Trichbrophenol ...... 88062 Phenol. 2.4.6-lrichlcfo- ...... I0 1.2.4 U231 A lo# (4.54) >- 93765 2.4.5-1 ...... 100 1.4 U232 C lM)O(454) ~chlnophenoxyace- : acid. 4 Po01 8 lo0 (45.4) 2.4.5-T acid lhanolamine 27323417 ...... loo0 1 ...... c (OM) (454) ~cylbenzeneullorr e. Ihylamine...... 121448 ...... 5000 1 ...... 5m(2270) ~elhylamine...... 75503 ...... 1000 1 B lo0 (45 4) 0- -Tr~nihobenzene...... 99354 Benzene. 1.3.5-lrinilr0- ...... 1. 4 U234 A 10 (4.54) 5-Trioxane. 2.4.6 123637 Paraldehyde 1' 4 U182 C 1000 (454) 1 ...... c IOW(454) melhyl-. 4 U2M) 0 5000 (2270) 2.3-dibcmopropyf) 126727 1-Propad. 2.3-dibromo- 1. 4 ~235 x I# (0.454) ~osphate. , phosphate (3:l). 18-t(3.4.5- 1rimelhcxybenzoyl)c~l- . melhylesler. Zm...... 7440666 2 ...... C lo00 (454) 40 CFR Ch. 1 (7-1-88 Edition) Environment01 Protection Agency I ABLE 302.4-LIST OF HAZARDOUS SUBSTANCES AND REPORTABLE QUANTITIES- TABLE 302.4-LIST OF HAZARDOUS SUBSTANCES AND REPORTABLE QUANTITIES-- Continued Continued [See loolnoteo st end 01 Table 302 4 1 ---- [See lootnotes at end of Table 302.41 Stalulcq F~nalRO Fsnal RO ardws Substance CASRN Regulalwy Synonyms Regulatory Synonyms RCRA Catego- RO codel waste ~ounds(~g) -- Number ry AND ...... 1' MPOUNDS. acetate ...... 557346 ...... 1000 tooo (454) ammonium chloride .. 52628258 ...... 5000 loo0 (454) F003 B loo (45 4) mrale ...... 1332076 ...... 1000 loo0 (454) The tollowtng spent sromtde ...... 7699458 ...... 5000 1000 (454) non.halogcnated :arbonate ...... 3486359 ...... 1M)O tooo (454) solvents and the :blonde...... :..... 7646857 ...... 5000 1000 (454) :yanide ...... 557211 ...... 10 to (4.54) fluoride ...... 7783495 ...... 1000 1000 (454) formate...... 5574 15 ...... 1000 1000 (454) hydrosullite ...... 7779864 ...... "-. 1000 1000 1454) nitrate ...... 7779886 ...... 5000 tooo (454) ohenolsulfonate...... 127822 ...... 5000 5WO (2270) Dhosphido ...... 1314847 ...... 1OW loo (45.4) sitofluoride ...... 16871719 ...... so00 5000 (2270) sullale...... 7733020 ...... 1000 1000 (454) nium nitrate...... 13746899 ...... 5000 5000 (2270) nium potassium 16923958 ...... SOW looo (454) wide. nium sulfate...... 14644612 ...... 5000 5000 (2270) nrum tetrachloride,.... 10026116 ...... Y)OO so00 (2270) ...... 1' 11(0.454) :lollowing spenl ~alogenated still bottoms from olvenls used in the recovery of legreasing and these solvents: ;ludges lrom the ecovely of these ;olvenls in (b) Nitrobenzene Icgreasing FMH B I00 (45.4) ~perations: a) Telrachlwo- 127184 ...... ethylene b) Trlchloroethylene . 79016 ...... C) Methylene 75002 ...... tho recovery ol chtortde. Ihesc solvents: d) 1.1.1- 7 1556 ...... (a) Tducne lrlchlorocthane. F) Carbon 56235 letractilorde. 1) Chlortnatcd (N.A.) fluorocarbons. 1 I ...... 4 F006 X ir (0.4541 e following spnt ialogenatcd ;olvents and the ;Itll bottoms lrom he recovery 01 hese solvents: processes: 'a) Tetrachloro- (1) Sullurtc acid ethylene. b) Methylene Chloride. :c) TrrMorwt~ :dl 1.1.1. Tnchloroelhane. !e) Chlorobemene... If) 1.1 -2-Tnchlore 1.2.2- (4) alunnnum or trttluoroethane Ztnc.alumnum 19) 0- loo (45.4) plaung on carbon D~chhobenzene. steel; I I 302.4 40 CFR Ch. 1 (7-1-88 Edition) Environmental Protection Agency 9 302.4

TABLE 302.4-LIST OF HAZARDOUS SUBSTANCES AND REPORTABLE QUANTITIES- TABLE 302.4-LIST OF HAZARDOUS SUBSTANCES AND REPORTABLE QUANTITIES- Continued Continued

[See Ioetnotes a1 end 01 Table 302 41 [See foolnotes at end of Table 302 41 ------Slatutory F~nalRO -1- statutory Hazardous Subslance I CASRN I Regulalwy Synonyms RCR A Hazardous Substance CASRN Regulatory Synonyms RCRA Catego- I RO 1 Cwde? 1 Waste 1 1 Pounds(Kg) RO Code.1. Waste Pounds(Kg) Number Number ry

(5) cleaning1 F007 ...... 1' 4 F007 A I0(4.54) strappin9 Spent cyanide plat~ng asseciatd with bath solut~onslrom tin. zinc and electroplatong aluminum plating operations (except en carbon steel: lor precious metals and eleclroplal~ngspent (6) chemical etching cyan~deplating bath and milling d solutions) aIwnii FW8 ...... 1. 4 FOOB A ir (4 54) Platong bath sludges from the Wtom 64 platin) baths from electroplaling operations where cyanides are used , in the process (except lor precieus metals electroplaling plallng bath sludges) FQ09...... I- 4 FW9 A 10 (4 54) Spcnl slr~ppingand clean~ngbath solut~onsfrom electroplalong operal~onswhore cyan~desare used in the process (except lor precious metals eleclroplating Spent stripping and cleanlng bath solul~ons) FOlO ...... 1' 4 FOIO A 10 (4.54) Oucnchong bath sludge from 011 baths from metal heat treallng operaloons where cyan~desare used in the process (except lor preclous metals heat-treating quenching bath slltdges) FO11 ...... 1' 4 FOII A to (4.54) Spcnl cyan~dc solutoons from salt bath pol cleanong lrom metal heat treating operations (except ler precious metals heal beating spent cyanide saIu110ns from salt bath pot cleaning) F012 ...... 1. 4 F012 A to (4.54)

40 CFR Ch. 1 (7-1-88 Edition) Environmental Protection Agency 5 302.4

TABLE 302.4-LIST OF HAZARDOUS SUBSTANCES AND REPORTABLE QUANTITIES-- TABLE 302.4-LIST OF HAZARDOUS SUBSTANCES AND REPORTABLE QUANTITIES- Continued Continued [See loolnetes at end of Table 302 41 [See footnotes at end ol Table 302.41

Statutory Final RO F~nalRO Hazardous Subslance CASRN - Regulatory Synonyms RCRA Catego- yrn Waste Catego- Pounds(Kg1 RO C0de.i. Waste Pounds(Kg) .... Number ry Number ry

Wastes, including but net limited to dntillation residues. containing tri-. tetra- heavy ends. tars. . or and reactor pentachlorophenol cleanout wastes. or discarded unused lrem the production lormulat~ons 91 chlorinated containing aliphatii cempounds derived hydrecahns.havig from these carbon content frem chlorophenols. (This em to rwe, utiliing listing does not free radical include formulalions catalyzed containing processes. (Thin hexachlerophene llsting does not synthesized from include light ends. prepurified 2.4.5- spent filters and trichlorophenel as filler aids, spent the sole ksicants(sic). component.) wastewater. F028 ...... wastewater Residues resulting treatment sludges. lrom the incineration spent catalysts.and or thermal treatment wastes listed in of soil contaminated 5 261.32.) with EPA Hazardous F026 ...... t ' 4 F026 X 1# (0.454) Waste Nos. F020. Wastes (except FD21. F022. F023. wastewater and F026. and F027. spent carbon from KW1 ...... hydrogen chloride Bottom sediment pwiliiatiin) lrom sludge from the the production of treatment of materials on wastewaters from equipment woad preserving previously used lor processes that use the manulacluring creosote andlor use (as a reactant. pentachlorophenol chemical K002...... intermediate. or Wastewater treatment component in a sludge from the formulating process) production of of tetra-, penta-, or chrome vellow and hexachlorobenzene orange piments under alkaline condilions. KO03 ...... Wastewater trcalment F027 4 ...... 1' ~027 x la (0.454) sludge lrom the productton of molybdato orange

KO04 ...... Wastewater treatment sludge from the DrOdiKllOll Of 21% ;ellow pigments KO05 ...... I 1. 1 4 1 KO05 I X 1 la(0.454) Wastewater treatment sludge lrom the product~on01 chromo green pigments KO06 ...... 1, ...... 1 ...... -- 40 CFR ch. 1 (7-1-88 ~di~i~~)Environmental Protection Agency TABLE 302.4-LIST OF HAZARDOUS SUBSTANCES AND REPORTABLE QUANTITIES-- TABLE 3024-LIST OF HAZARDOUS SUBSTANCES AND REPORTABLE QUANTITIES-- Continued Continued.- [See lootnoles at end ol Table 302.41 [See foe(rw1es at end ol Table 302 4)

Statutq Final RQ CASRN Regulatory Synonyms Hazardous Substance CASRN Regulatocy Synonyms RCRA Hazardous Substnnce yo -? ca:ge pl"(Kg) RO Codei. C1F90- sir Wasle Pouds(Kg) I 1 1 Numkr

Wastewaler treatment Heavy ends from tho sludge from the fractionallon column praduction of in ethyl chloride chrome oxide yreen 1. 4 KO19 X 118.454) pigments KO19 ...... ( 1 ( I 1 (anhydrous and Heaw ends from the I I hydrated) disiillation 01 K007 ethylene dichloride ...... 1. 4 KO07 X 11(0.454) Wastewater treatment in ethylene stud* lrom the dichloride ProfJucti 01 iron production bhm pigments KO26 ...... KOb8 Heavy ends hom the ...... 1 4 KOOI X 11(9.454) Own residue lrom the dislillal'm el vinyl produclion of chloride in vinyl chrome oxide green chloride nwn~nN pjments Km ...... 1. 4 KO09 X 11(9.454) Distillation bettoms Aqueous spent frem Ihe produclien antimony catalyst of acataldehyda waste lrom Irem ethylene ~luerernethanes I KOle ...... 1. 4 K91B X 11(9.454) KO22 1- Distillation side cuts .. Irom the poducli Oistittatron bettom tars 01 acelaldehyde frem the production 'rwn ethylene 01 ~henollacetone K@l1 trim cumene ...... :...... 1. 4 KO11 X 11 (0.454) KO23 ...... Bettam stream frem Cisl~llatlonIlghl ends the wastewalef stripper m the lrom the production 01 phthalic productin of anhydride from acrylonitrile naphthalono KO13 ...... 1' 4 KO13 X 11(0 454) KO24 ...... Bollem stream lrem Dtsldtalion bottoms the acetonitr~le lrom the production column in the of phthalic production of anhydride lrom 8uylon1trile naphthalene KO14 ...... 1. 4 KO14 D 5000 (2270) KO25 ...... Bettoms lrom the D~slillationbottoms acetonitrile from the production purification column d nilrebenzene by in the prelimo( the nitration of acfylonitriie benzene KO15 ...... 1. 4 KO15 X 11(0.454) KO26 ...... SliM WlMm lrm Stripping still tails lrOm thedstdlatton 01 the preduclion 01 benu chloride methvl ethvl net6...... 1. 4 KO16 X 11(0.454) Heavy ends or datlllat~onresidues Conbifvy and from lhe dist~llabenresidWS ~oduct~cahn lrom toluene letrachb~de dilsocyanate KO17 ...... 1. 4 KO17 X 11(8.454) production Heavy ends (still KO28 ...... I' bottoms) lrom the Spent catalyst from prifcatian column the hydrochlwinator in the preduction of reactor In Ihe epichlwohydrin produCli of 1.1 .I- KO18 ...... 1. 4 Kt318 X 11(0.454) tr'ikoett\ane KO29 ...... --.. Environmental Protection Agency 9 302.4

TABLE 302.4-LIST OF HAZARDOUS SUBSTANCES AND REPORTABLE OUANTITIES- Continued [See footnotes at end 01 Table 302.41

Statutory F~natRO

Hazardous Substance CASRN Regulatory Synonyms RCRA Cat")o- RO Codet Wasle Pounds(Kg) Number ry

Filter cake lrom the l~ltral~on01 d~cthytphosphoro- d~th~oicac~d in the production 01 phorate KO40 ...... 1' 4 KO40 X 1a (0.454) Wastewater treatment sludge from the production 01 phorate KO41 ...... 1. 4 KO41 X It (0.454) Wastewatcr treatment sludge from the production 01 toxaphene KO42 ...... 1' 4 KO42 X 1t (0.454) Heavy ends or distillation residues from the distillation Of tetrachlorobenzene in the producli 01 2.4.5-T KO43 ...... 1. 4 KO43 X ,I H (0454) 2.6-Lhchtorophenol waste lrom the production 01 2.4-D A 10 (4.54) KO44 ...... 1 4 KO44 Wastewater treatment sludges lrom the manufacturing and processing of explosives to (4.54) KO45 ...... 1' 4 KO45 A Spent carbon lrom the treatrncnt of wastewater contatntng explosives -KO46 ...... 1' 4 KO46 B IM) (45.4) Wastcwatcr treatment studgcs lrom the manulactunng . lormutat~onand loadlng 01 Icad- based lnitiatlng compounds KO47 ...... 1' 4 KO47 A 10 (4 54) Pinklred water from TNT operations It (0.454) KO48 ...... 1 4 KO48 X Dissolved air ttolation (DAF) float from the petroleum refining induslry KO49 ...... 1. 4 KO49 X 1H (0.454) Slop oil emulsion sottds lrom the pelroteum refining industry X l# (0.454) KO50 ...... I' 4 KO50 1302.4 40 CFR Ch. 1 (7-1-88 Edition) Environmental Protection Agency $302.4 TABLE 302.4-LIST OF HAZARDOUS SUBSTANCES AND REPORTABLE QUANTITIES- Continued [See loelnotes al end ol fable 302.41

Statutay F~nalRO Huardeus Subslance CASRN Regulatory Synonyms RCRA A0 Ceder Waste Ca'ega Pounds(Kp) Number ry

Heat exchanger hndle cleanm) sludge lrom the petroleum refin~ng industry K151 ...... 1 1b (0.454) API separalor sludge fr~the petroleum refming industry KO52 ...... ion (4.54) Tank bottoms (leaded) from the petroleum relining industry KOC8 ...... In (6.454) Ammenla sltlt Ii Sludge lrmcoking oseraliis I#(0.454) sludge from the MRW.U.tm I x, 1 ef steel in electric

11 (8.454) Spent pckle liua from steel fimshmg werations K069...... Emisstan control dust/ I I sludae lrom I I

smelting KO71 ...... Brtne purdcatiion muds from the mercwy cet! process in chlonm, poduc\m, where separalely pepwlf~edbr~ne is not used K873 ...... Chlwmnated hydrocarbon waste from Ihe purikatm slep ol the Qaphragm cell process using graph~leanodes in chlorine production KO83 ...... Distillation bottoms Com aruhne extraction ...... -...... L A L & a A L a L x d I U0x x x x ; P 8 8 0

X X X X m X X X X I

X X x

2 If x 3 xd 0 -. N m * L t in

X X X X X X X X

d 't t 0 0 -cnP -rP

Attachment TI1

TIER TWO INSTRUCTIONS

GENERAL INFORMATION WHAT CHEMICALS ARE EXCLUDED Submission of this Tier Two form (when requested) is required by Title Section 31 1(e) of Title Ill excludes the following substances: Ill of the Superfund Amendments and Reauthorization Act of 1986. (I) Any food, food additive, color additive, drug, or cosmetic regulated Section 312. Public Law 99-499. codified at 42 U.S.C. Section 11022., by the Food and Drug Administration; The purpose of this Tier Two form is to provide State and local officials (11) Any substance present as a solid in any manufactured item to the and the public with specific information on hazardous chemicals extent exposure to the substance does not occur under normal present at your facility during the past year. conditions of use; (Ill) Any substance to the extent it is used for personal, family, or CERTIFICATION household purposes, or is present in the same form and concentra The owner or operator or the officially designated representative of the tion as a product packaged for distribution and use by the general owner or operator must certify that all information included in the Tier public; Two submission is true, accurate, and complete. On the first page of (IV) Any substance tot he extent it is used in a research laboratory or a the Tier Two report, enter your full name and official title. Sign your hospital or other medical facility under the direct supervision of a name and enter the current date. Also, enter the total number of pages technically qualified individual; included in the Confidential and Non-Confidential information Sheets (V) Any substance to the extent it is used in routine agricultural as well as all attachments. An original signature is required on at least operations or is a fertilizer held for sale by a retailer to the ultimate the first page of the submission. Submissions to the SERC, LEPC, and customer. fire department must each contain an original signature on at least the first page. Subsequent pages must contain either an original signature, OSHA regulations, Section 1910.1 200(b), stipulate exemptions from a photocopy of the original signature, or a signature stamp. Each page the requirement to prepare or have available an MSDS. must contain the date on which the original signature was affixed to the first page of the submission and the total number of pages in the REPORTING THRESHOLDS submission. Minimum thresholds have been established for Tier Onerrier Two reporting under Title Ill, Section 312. These thresholds are as follows: YOU MUST PROVIDE ALL INFORMATION REQUESTED ON THlS FORM TO FULFILL TlER TWO REPORTING REQUIREMENTS. For Extremely Hazardous Substances (EHSs) designated under section 302 of Title Ill, the reporting threshold is 500 pounds (or 227 This form may also be used as a worksheet for completing the Tier kg.) or the threshold planning quantity (TPQ), whichever is lower: One form or may be submitted in place of the Tier One form. For all other hazardous chemicals for which facilities are required to WHO MUST SUBMIT THlS FORM have or prepare an MSDS, the minimum reporting threshold is 10,000 Section 312 of Title Ill requires that the owner or operator of a facility. pounds (or 4.540 kg.). submit this Tier Two form if so requested by a State emergency response commission, a local emergency planning committee. or a fire You need to report hazardous chemicals that were present at your department with jurisdiction over the facility. facility at any time during the previous calendar year at levels that equal or exceed these thresholds. For instructions on threshold This request may apply to the owner or operator of any facility that is determinations for components of mixtures, see "What About Mix- required, under regulations implementing the Occupational Safety and tures?" on page 2 of these instructions. Health Act of 1970, to prepare or have available a Material Safety Data Sheet (MSDS) for a hazardous chemical present at the facility. MSDS A requesting official may limit the responses required under Tier Two requirements are specified in the Occupational Safety and Health Ad- by specifying particular chemicals or groups of chemicals. Such ministration (OSHA) Hazard Communication Standard, found in Title 29 requests apply to hazardous chemicals regardless of established of the Code of Federal Regulations at 5 1910.1 200. thresholds. This form does not have to be submitted if all of the chemicals located at your facility are excluded under Section 31 1(e) of Title Ill.

WHAT CHEMICALS ARE INCLUDED If you are submitting Tier Two forms in lieu of Tier One, you must report the required information on this Tier Two form for each hazardous chemical present at your facility in quantities equal to or greater than established threshold amounts (discussed below), unless the chemi- cals are excluded under Section 31 1(e) of Title Ill. Hazardous chemi- cals are any substance for which your facility must maintain an MSDS under OSHA's tiazard Communication Standard. If you elect to submit Tier One rather than Tier Two, you may still be required to submit Tier Two information upon request. INSTRUCTIONS Please read these instructions carefully, Print or type all responses. need assistance in responding to a chemical accident at the facility.

WHEN TO SUBMIT THIS FORM Provide an emergency phone number where such emergency Owners or operators of facilities that have hazardous chemicals on information will be available 24 hours a day, every day. This require- hand in quantities equal to or greater than set threshold levels must ment is mandatory. The facility must make some arrangement to submit either Tier One or Tier Two forms by March 1. ensure that a 24 hour contact is available.

Ifyou choose to submit Tier One, rather than Tier Two, be aware that IDENTICAL INFORMATION you may have to s~lbmitTier Two information later, upon request of an Check the box indicating identical information, located below the authorized official. You must submit the Tier Two form within 30 days of emergency contacts on the Tier Two form, if the current chemical receipt of a written request. information being reported is identical to that submitted last year. Chemical descriptions, hazards, amounts, and locations must be WHERE TO SUBMIT THIS FORM provided in this year's form, even if the information is identical to that Send either a completed Tier One form or Tier Two forrn(s) to each of submitted last year. the following organizations: 1. Your State Emergency Response Commission. CHEMICAL INFORMATION: 2. Your Local Emergency Planning Committee. Description, Hazards, Amounts, and Locations 3. The fire department with jurisdiction over your facility. The main section of the Tier Two form requires specific information on amounts and locations of hazardous chemicals, as defined in the If a Tier Two form is submitted in response to a request, send the OSHA Hazard Communication Standard. completed form to the requesting agency. If you choose to indicate that all of the information on a specific PENALTIES hazardous chemical is identical to that submitted last year, check the Any owner or operator who violates any Tier Two reporting require- appropriate optional box provided at the right side of the storage codes ments shall be liable to the United States for a civil penalty of up to and locations on the Tier Two form. Chemical descriptions, hazards, $25,000 for each such violation. Each day a violation continues shall amounts, and locations must be provided even if the information is constitute a separate violation. identical to that submitted last year.

If your Tier Two responses require more than one page, use additional *What units should I use? forms and fill in the page number at the top of the form. Calculate all amounts as weight in pounds. To convert gas or liquid REPORTING PERIOD volume to weight in pounds, multiply by an appropriate density factor. Enter the appropriate calendar year, beginning January 1 and ending December 3 1. * What about mixtures?

FACILITY IDENTIFICATION If a chemical is part of a mixture, you have the option of reporting Enter the full name of your facility (and company identifier where either the weight of the entire mixture or only the portion of the mixture appropriate). that is a particular hazardous chemical (e.g., if a hazardous solution weighs 100 Ibs. but is composed of only 5% of a particular hazardous Enter the full street address or state road, if a street address is not chemical, you can indicate either 100 Ibs. of the mixture or 5 Ibs. of ' available, enter other appropriate identifiers that describe the physical the chemical). location of your facility (e.g., longitude and latitude). Include city, county, state, and zip code. The option used for each mixture must be consistent with the option used in your Section 31 1 reporting. Enter the primary Standard Industrial Classification (SIC) code and the Dun & Bradstreet number for your facility. The financial officer of your Because EHSs are important to Section 303 planning, EHSs have facility should be able to provide the Dun & Bradstreet number. If your lower thresholds. The amount of an EHS at a facility (both pure EHS firm does not have this information, contact the State or regional office substances and EHSs in mixtures) must be aggregated for purposes of Dun & Bradstreet to obtain your facility number or have one of threshold determination: It is suggested that the aggregation calcu assigned. lation be done as a first step in making the threshold determination. Once you determine whether a threshold for an EHS has been OWNERIOPERATOR reached, you should report either the total weight of the EHS at your Enter the owner's or operator's full name, mailing address, and phone facility, or the weight of each mixture containing the EHS. number.

EMERGENCY CONTACT Enter the name, title, and work phone number of at least one local person or office who can act as a referral if emergency responders CHEMICAL DESCRIPTION Hazard Category Comparison For Reporting 1. Enter the Chemical Abstract Service registry number (CAS). For Under Sections 31 1 and 31 2 mixtures, enter the CAS number of the mixture as a whole if it has EPA's OSH's been assigned a number distinct from its constituents. For a mixture Hazard Categories Hazard Categories that has no CAS number, leave this item blank or report the CAS numbers of as many constituent chemicals as possible. Fire Hazard Flammable Combustion Liquid If you are withholding the name of a chemical in accordance with Pyrophoric criteria specified in Title Ill, Section 322, enter the generic class or Oxidizer category that is structurally descriptive of the chemical (e.g., list Sudden Release Explosive toulene diisocyanate as organic isocyanate) and check the box of Pressure Compressed Gas marked Trade Secret. Trade secret information should be submitted to EPA and must include a substantiation. Please refer to EPA's final Reactive Unstable Reactive Organic Peroxide regulation on trade secrecy (53 FR 28772, July 29,1988) for Water Reactive detailed information on how to submit trade secrecy claims. Immediate (Acute)' Highly Toxic 2. Enter the chemical name or common name of each hazardous Health Hazards Toxic chemical. Irritant Sensitizer Corrosive 3. Check box for all applicable descriptors: pure or mixture: and solid, liquid, or gas; and whether the chemical is or contains an EHS. Other hazardous Chemicals with an 4. If the chemical is a mixture containing an EHS, enter the chemical adverse effect with name of each EHS in the mixture. short term exposure Delayed (Chronic) Carcinogens Health Hazard You have pure chlorine gas on hand, as well as two mixtures that Other hazardous contain liquid chlorine. You wite "chlorine" and enter the CAS number. chemicals with an adverse effect with Then you check pure" and 'mix" - as well as "liquid" and vas: long term exposure PHYSICAL AND HEALTH HAZARDS For each chemical you have listed, check all the physical and health hazard boxes that apply. These hazard categories are defined in 40 CFR 370.2. The two health hazard categories and three physical hazard categories are a consolidation of the 23 hazard categories defined in the OSHA Hazard Communication Standard, 29 CFR 1910.1200. MAXIMUM AMOUNT I 1. For each hazardous chemical, estimate the greatest EXAMPLE: amount present at your facility on any single day during the reporting period. The 25,000-gallon shipment of solvent you received last year was 2.Find the appropriate range value code in Table I. gradually used up and completely gone in 315 days. The sum of the daily volume levels in the tank is 4,536,000 gallons. By dividing 4, 3. Enter this range value as the Maximum Amonunt.. 536,000 gallons by 315 days on-site, you calculate an average daily amount of 14,400 gallons. TABLE IREPORTING RANGES Range Weight Range in Pounds You already know that the solvent contains 10% benzene, which is a hazardous chemical. Since 10% of 14,400 is 1,440, you figure that you Value From . . . . To.. . . ' 0 1 0 99 had an average of 1,440 gallons of benzene, You also know that the 02 100 999 density of benzene is 7.29 pounds per gallon, so you multiply 1,440 by 03 1,000 9,999 7.29 to get a weight of 10,500 pounds. 04 10,000 99,999 05 100,000 999,999 Then you look at Table Iand find that the range value 04 corresponds 06 1,000,000 9,999,999 to 10,500. You enter 04 as the Average Daily Amount. 07 10,000,000 49,999,999 08 50,000,000 99,999,999 (if you are using the form as a worksheet for completing a Tier One 09 100,000,000 499,999,999 form, you should write 10,500 in the shaded area.) 10 500,000,000 999,999,999 11 1 billion higher than 1 billion NUMBER OF DAYS ON-SITE Enter the number of days that the hazardous chemical was found on- If you are using this form as a worksheet for completing Tier One, enter site. the actual weight in pounds in the shaded space below the response blocks. Do this for both Maximum Amount and Average Daily Amount. EXAMPLE:

EXAMPLE: The solvent composed of 10% benzene was present for 315 days at your facility. Enter 31 5 in the space provided. You received one large shipment of a solvent mixture last year. The shipment filled five 5,000 gallon storage tanks. You know that the solvent contains 10% benzene, which is a hazardous chemical.

You figure that 10% of 25,000 gallons is 2,500 gallons. You also know that the density of benzene is 7.29 pounds per gallon, so you multiply 2,500 gallons by 7.29 pounds per gallon to get a weight of 18,225 pounds.

Then you look at Table I and find that the range value 04 corresponds to 18,225. You enter 04 as the Maximum Amount.

(If you are using the form as a worksheet for completing a Tier One form, you should write 18,255 in the shaded area.)

AVERAGE DAILY AMOUNT 1. For each hazardous chemical, estimate the average weight in pounds that was present at your facility during the year.

To do this, total all daily weights and divide by the number of days the chemical was present on the site.

2. Find the appropriate range value in Table I.

3. Enter this range value as the Average Daily Amount. --. STORAGE CODES AND STORAGE LOCATIONS EXAMPLE: List all non-confidential chemical locations in this column, along with The benzene in the main building is kept in a tank inside the building, storage typeslconditions associated with each location. Please note at ambient pressure and less than ambient temperature. that a particular chemical may be located in several places around the facility. Each row of boxes followed by a line represents a unique Table I1 shows you that the code for a tank inside a building is C. Table location for the same chemical. 111 shows you that the code for ambient pressures is 1, and the code for less than ambient temperature is 6.

Storage Codes: indicate the types and conditions of storage present: You enter: C 1 6 a. Look at Table II. For each location, find the appropriate storage type Storage Locations: and enter the corresponding code in the first box. Provide a brief description of the precise location of the chemical, so that emergency responders can locate the area easily. You may find it b. Look at Table Ill. For each location, find the appropriate storage advantageous to provide the optional site plan or site coordinates as types for pressure and temperature conditions. Enter the applicable explained below. pressure code in the second box. Enter the applicable temperature code in the third box. For each chemical, indicate at a minimum the building or lot. Addition- ally, where practical, the room or area may be indicated. You may respond in narrative form with appropriate site coordinates or abbrevia- Table II STORAGE TYPES tions. CODES Tvpes of Stor= If the chemical is present in more than one building, lot, or area Above ground tank location, continue your responses down the page as needed. If the Below ground tank chemical exists everywhere at the plant site simultaneously, you may Tank inside building report that the chemical is ubiquitous at the site. Steel drum Plastic or non-metallic drum Qplional attachments: If you choose to attach one of the following, Can check the appropriate Attachments box at the bottom of the Tier Two Carboy form. Silo a. A site plan with site coordinates indicated for buildings, lots, Fiber drum areas, etc., throughout your facility. b. A list of site coordinate abbreviations that correspond to build Bag ings, lots, areas, etc. throughout your facility. Box c. A description of dikes and other safeguard measures for storage Cylinder locations throughout your facility. Glass bottles or jugs Plastic bottles or jugs Tote bin EXAMPLE: Tank wagon You have benzene in the main room of the main building, and in tank 2 Rail car in tank field 10. You attach a site plan with coordinates as follows: main Other 'building = G-2. tank field 10 = 8-6. Fill in the Storage Location as follows:

8-6 ( Tank 2 ) G-2 ( Main Room )

Table Ill - TEMPERATURE CONFIDENTIAL INFORMATION AND PRESSURE CONDITIONS Under Title Ill. Section 324, you may elect to withhold location CODES Storaae Conditions information on a specific chemical from disclosure to the public, If you choose to do so: (PRESSURE) *Enter the word "confidential" in the Non-Confidential Location section 1 Ambient pressure of the Tier Two form on the first line of the storage locations. 2 Greater than ambient pressure Ona separate Tier Two Confidential Location lnformation Sheet, 3 Less than ambient pressure enter the name and CAS number of each chemical for which you are keeping the location confidential. (TEMPERATURE) * Enter the appropriate location and storage information, as described 4 Ambient temperature above for non-confidentiallocations. 5 Greater than ambient temperature * Attach the Tier Two Confidential Location lnformation Sheet to the 6 Less than ambient temperature Tier Two form. This separates confidential locations from other but not cryogenic information that will be disclosed to the public 7 Cryogenic conditions CERTIFICATION Instructions for this section are included on page one of these instructions.

Page of pages levised June 1990 68-0689 (11-90) Form Approved OM8 No. 2050-007 ( Facility Identification I OwnerlOperator Name TierTwo Name Name Phone (-1 - EMERGENCY AND _ Mall Address - HAZARDOUS cq Cwnty State ZQEmergency Contact CHEMICAL INVENTORY rrm 17~177 Nam Tale - - Phone (--) 24 HI. Phone ( \ FOR Specif~c OFFICtAL '" lniormation ~ame T~II. --- USE by Chemical Date Recemd ONLY Phone (- I 24 I+. Phane ( ) --

Check if information below is identical to the inlormadonsubmined Reporting Period From January l lo Ihcember31. 19- Important: Read all instructions before completing form lolast year. E - cs.5 Storage Codes and Locations fi Confidential Location Information Sheet a (Confidential) .- Ef, Storage Locations o'i

-* rrrn-ll ;::

themName -0 Imi'-l--l

Optional Attachments I certlty m& penally ot law tha Ihave persondly examned adam tamliar mlh the mfumtm&m((ed In pages me hrw@- . nd lhal Wed on my mqufy of hose ~ndwdudsresponvble tu oMirn~ng he mlctrna~on.Ibelleve hat he submned lntamabon IS be. aauae, ad complete I haw allached a sne plan I have anached a llst of Slte mordlnate abbrevtalwns ------. ------Nmr ard onaa 111. d o*nerlopsrala OR mriopwalPs wlhulz~reparnabw Spalute Oae xyd I have anached a descrptlon of dres and other saleguard measures Page ol pages Revised June 1990 ------68-0689 (1 1-90) Form Approved OMB Nc. 2050-0072

Phone ( )

24 Hr. Phone ( )

Storage Codes and '~ocations Chemical Description (Confidential) Storage Locations (Check all that apply)

Sudden Release

Pure Mar Sol~d L~quld Gas EHS

ICerbhcat~on (Read and sign alter mmpietvlg all sedions) ( Optional Attachments I I cemfy under penany ol law that I have persondly examlned and am faml~arwth the tnformahon submtned In pages one through _ and lhal based on my tnqutry of those tndwtduals responstble tor obtantng I have anached a sne plan the ~nlormatnn.I belleve !hat the submned ~nlormabonIS true, acanate and mrrplete i have anached a Its1 of site Coordtnate abbrevlattons - - I havn anrchad a descrlplnon ol d*es and Nsmc and ollorl dl@d unter opelalor OR ovmnlopar~los du(hon2ud ~l~pnw#tal~vaSq~elare Date sgnud olhrr saleguard mraulrss Attachment TCL 28 TABLE I11 SECTION 313 TOXIC CHEMICAL LIST (Including Chemical Categories) w: Chemicals may be added or deleted to the list. The Emergency Planning and Community Right-to-Know Hotline, (800) 635-0202 or (202) 479-2449 in Washington, D.C. or Almka, will provide up-to-date information on the status of there changes.] a. Al~habeticalList (Effective Date January 1,1987) CAS Number Chemical Name

Acetaldehyde C.I. Acid Green 3 Acetamide C.I. Basic Green 4 Acetone C.I. Basic Red 1 Acetonitrile C.I. Direct Black 38 2-Acetylaminofluorene C.I. Direct Blue 6 Acrolein C.I. Direct Brown 96 Acrylamide C.I. Disperse Yellow 3 Acrylic acid C.I. Food Red 6 Acrylonitrile C.I. Food Red 16 Aldrin [1,4:5,8-Dimethanonaphthalene, C.I. Solvent Orange 7 1,2,3,4,10,10-hexachloro-1,4,4a, C.I. Solvent Yellow 3 6,8,8a-hexahydro-(l.alpha., C.I. Solvent Yellow 14 4.alpha.,4a.beta.,5.alpha., C.I. Solvent Yellow 34 (Auramine) 8.alpha.,8a.beta.)-] C.I. Vat Yellow 4 Ally1 chloride Cadmium Aluminum (fume or dust) . Calcium cyanamide Aluminum oxide Captan [lH-Isoindole-1,3(2H)-dione, 2-Aminoanthraquinone Sal4,7,7a-tetrahydro-2- 4-Aminoacobencene [(trichloromethyl)thio]-] 4-Aminobiphenyl Carbaryl [I-Naphthalenol, 1-Amino-2-methylanthraquinone methylcarbamate] Ammonia Carbon disulfide Ammonium nitrate (solution) Carbon tetrachloride Ammonium sulfate (solution) Carbonyl sulfide Aniline Catechol -o-hisidine Chloramben [Beneoic acid, 3-amino- phisidine 2,6-dichloro-] 9-Anisidine hydrochloride Chlordane [4,7-Methanoindan, Anthracene 1,2,4,6,6,7,8,8- octachloro- Antimony 2,3,3a,4,7,7a-hexahydro-] Arsenic Chlorine Asbestos (friable) Chlorine dioxide Barium Chloroacetic acid Bencal chloride 2-Chloroacetophenone Beneamide Chlorobencene Benzene Chlorobensilate [Benzeneacetic acid, Beneidine 4-chloro-.alpha.-(4- Beneoic trichloride (Bencotrichloride) chloropheny1)- Ben~oylchloride .alpha.-hydroxy-, Beneoyl peroxide ethyl ester] Beneyl chloride Chloroethane (Ethyl chloride) Beryllium Chloroform Biphenyl Chloromethane (Methyl chloride) Bis(2-chloroethyl) ether Chloromethyl methyl ether Bis(chloromethy1) ether Chloroprene Bis(2-chloro-1-methylethyl)ether Chlorothalonil [1,3- Bis(2-ethylhexyl) adipate Beneenedicsrbonitrile, Bromoform (Tribromomethane) 2,4,6,6-tetrachloro-] Bromomethane (Methyl bromide) Chromium l,3-Butadiene Cobalt Butyl acrylate Copper -n-Butyl alcohol pcresidine -sec-Butyl alcohol Cresol (mixed isomers) s-Butyl alcohol m-Cresol Butyl benzyl phthalate -Z~resol 1,2-Butylene oxide pCresol Butyraldehyde Cumene C.I. Acid Blue 9, diammoniun~salt Cumene hydroperoxide C.I. Acid Blue 9, disodium salt Cupferron (Ben~eneamine,N-hydroxy N-nitroso, ammonium salt] Cyclohexane Heptachlor [X,4,5,6,7,8,8-Heptachloro- 2,4-D [Acetic acid, (2,4-dichloro- Sa,4,7,7a-tetrahydro-4,7- ppnox~)-I methano-lH-indenel Decabromod~phenyloxide Hexachlorobeneene Diallate [Carbarnothioic acid,bis Hexachloro-1,s-butadiene (I-methylethyl)-, 5-(2,s- Hexachlorocyclopentadiene dichloro-2-propcnyl) ester] Hexachloroethane 2,4-Diaminoaninole Hexachloronaphthalene 2,4-Diaminoanisole sulfate Hexamethylphosphoramidc 4,4'-Diaminodiphenyl ether Hydracine Diaminotoluene (mixed isomers) Hydracine sulfate 2,4-Diaminotoluene Hydrochloric acid Diasomethane Hydrogen cyanide Dibensofuran Hydrogen fluoride 1,2-Dibromo-3-chloropropane(DBCP) Hydroquinone 1,2-Dibromoethane (Ethylene dibromide) Isobutyraldehyde Dibutyl phthalate lsopropyl alcohol Dichlorobeneene (mixed isomers) (manufacturing-strong 1,2-~ichlorobeneene acid process, no rupplier 1,s-Dichlorobensene notification) 1,4-Dichlorobenrene 4,4'-Isopropylidenediphenol 3,s'-Dichlorobencidine Lead Dichlorobromomethane Lindane[Cyclohexane, 1,2,S,4,6,6-hex- 1,2-Dichloroethane (Ethylene achloro-,(l.alpha.,2.alpha.,S. dichloride) beta.,4.alpha.,5.alpha.,6.bets.)-] 1,2-Dichloroethylene Maleic anhydride Dichloromethane (Methylene chloride) Maneb [Carbamodithioic acid, 1,2- ' 2,4-Dichlorophenol ethanediylbir-, manganese 1,2-Dichloropropane complex] 1,s-Dichloropropylene Manganese Dichlorvos [Phosphoric acid, 2 Melamine dichloroethenyl dimethyl Mercury ester] Methanol Dicofol [Beneenemethanol, 4-chlom- Methoxychlor (Beneene, 1,l'-(2,2,2- .alpha.- 4-chloropheny1)- trichloroethylidene)bis .alpha.- (trichloromethyl)-] \4-methoxy-1 Diepoxybutane 2-Methoxyethanol Diethanolamine Methyi acrylate Di-(2-ethylhexyl) phthalate (DEHP) Methyl e-butyi ether Diethyl phthalate 4,l'-Methylenebis(2-chioro aniline) Diethyl sulfate (MBOCA) 3,3'-Dimethoxybeneidine (,la-Methylenebis(N,x-dimethyl) 4-Dimethylaminoazobensene beneenamine 3,3'-Dimethylbensidine (0-Tolidine) Methylenebis(phenylisocyanate) (MB!) Dimethylcarbamyl chloride Methylene bromide Ill-Dimethyl hydrarine 4,4'-Methylenedianiline 2,4-Dimethylphenol Methyl ethyl ketone Dimethyl phthalate Methyl hydracine Dimethyl sulfate Methyl iodide 4,6-Dinitro-2-ereso1 Methyl isobutyl ketone 2,4-Dinitrophenol Methyl isocyanate 2,4-Dinitrotoluene Methyl methacrylate 2,6-Dinitrotoluene Michler's ketone -n-Dioctyl phthalate Molybdenum trioxide l,4-Dioxane Mustard gas [Ethane, 1,l'-fahiobis 1,2-Diphenylhydraeine (2-chloro-] (Hydrasobenzene) Naphthalene Epichlorohydrin &-Naphthylamine 2-Ethoxyethanol -beta-Nophthylamine Ethyl acrylate Nickel Ethylben~ene Nitric acid Ethyl chloroformate Nitrilotriacetic acid Ethylene 5-Nitro-g-snisidine Ethylene glycol Nitrobeneene Ethyleneimine (hiridine) (-Nitrobiphenyl Ethylene oxide Nicrofen [Benzene, 2,4-dichloro- Ethylene thiourea 1-(4-nitrophenoxj)-1 Fluorneturon [Urea, N,N-dimethyl-N'- Nitrogen mustard (2-~hloro-N-(2- 13-(trifl~oromethyl)~henyl]-] chloroethyl) -N- Formaldehyde methylethanarnine) Freon 113 [Ethane, l,l,2-trichloro-l,2, Nitroglycerin 2-trifluoro-1 2-Nitrophenol 4-Nitrophenol 2-Nitropropane Triaciquone [2,5-Cyclohuadiene-1,4- pNitrosodiphenylarnine dione, 2,S,6-trir(1- &N-Dimethylaniline aciridiny1)-] x-Nitroaodi-n-butylarnine Trichlorfon [Phoaphonic acid, (2,2,2- E-Nitrosodiethylamine trichloro-1-hydroxyethy1)-, E-Nitroaodimethylamina dimethyl ester] N-Nitroaodiphenylamine 1,2,4-Trichlorobencene ~-~itroaodi-~-~ro~~lamine l,l,l-Trichloroethad (Methyl H-Nitrosomethylvinylamine chloroform) E-Nitroaomorpholine 1,1,2-Trichloroethano E-Nitroao-H-ethylurea Trichloroethylene -N-Nitroao-B-methylurea 2,4,6-Trichlorophend N-Nitroaonornicotine 2,4,6-Trichlorophenol E-~itroro~iperidine Trifluralin [Benceneamine, 2,6- Octachloronaphthalene dinitro-N,N-dipropyl-4- Osmium tetroxide (trifluoromethy1)-] Parathion [Phoaphorothioic acid, 0, 1,2,4-Trimethylbencene 0-diethyl-0-(4-nitrophenyl) Tria(2,S-dibromopropyl) phosphate eater] Urethane (Ethyl carbarnate) Pentachlorophenol (PCP) Vanadium (fume or duat) Peracetic acid Vinyl acetate Phenol Vinyl bromide pphenylenediamine Vinyl chloride 2-Phenylphenol Vinylidene chloride Phosgene Xylene (mixed isomem) Phosphoric acid m-Xylene Phosphorus (yellow or white) &xYlene Phthalic anhydride p-Xylene Picric acid 2,6-Xylidine Polychlorinated biphenyls (PCBs) Zinc (fume or duat) Propane sultone Zineb [Carbamodithioic acid, 1,2- &-Propiolactone ethanediylbis-, cinc complex] Propionaldehyde Propoxur [Phenol, 2-(1-methy1ethoxy)-, b. List Bv CAS Number (Effective Date methylcarbamate] January 1,1987) Propylene (Propene) Propyleneirnine CAS Number Chemical Name Propylene oxide Pyridine Formaldehyde Quinoline 2,4-Dinitrophenol Quinone Nitrogen mustard 12-Chloro-N-(2- Quintoeene [Pentachloronitrobencene] ehloroethy1)-N- Saccharin (manufacturing, no aupplier methylanaminel notification) [1,2- Urethane (Ethyl carbamate) Bencisothiacol -3(2H)-one, Trichlorfon [Phosphonic acid, (2,2,2- Ill-dioxide] trichloro-1-hydroxyethy1)- Safrole dimethyl ester] Selenium 2-Acetylaminofluorene Silver B-Nitrosodiethylamine Sodium hydroxide (solution) Bencamide Sodium sulfate (aolution) Nitroglycerin Styrene Carbon tetrachloride Styrene oxide Parathion [Phosphorothioic acid, 0,O- Sulfuric acid diethyl-0-(4- Terephthalic acid nitrophenyl)ester] 1,1,2,2-Tetrachlroethane Ill-Dimethyl hydraeine Tetrachloroethylene (Per~hloroeth~lene) -beta-Propiolactone Tetrachlorvinphos (Phoaphoric acid, 2- Chlordane [4,7-Methanoindan, chloro-1- (2,3,5- 1,2,4,5,6,7,8,8- octachloro- trich1orophenyl)ethenyl 2,3,3a,4,7,7a-hexahydro;] dimethyl eater] Lindane [Cyclohexane, 1,2,3,4,6,6- Thallium hexachloro-,(l.alpha., Thioacetamide t.alpha.,S.beta., 4,4'-Thiodianiline 4.alpha.,6.alpha.,6.beta.)-] Thiourea x-Nitroaomorpholine Thorium dioxide 4-Aminoacobeneene Titanium dioxide 4-Dimethylaminoaeobensenc Titanium tetrachloride Methyl hydracine Toluene Acetamide Toluene-2,4-diiaocy anate Aniline Toluene-2,6-diiaocyanr,te Thioacetamide 2-Toluidine Thiourea -o-Toluidine hydrochloride Dichlorvos [Phosphoric acid, 2,2- Toxaphene dichloroethenyl dimethyl ester] -N-Nitrosodimethylamina E-Nitrosodiphenylamine Carbaryl [1-Naphthalenol, 2,6-Xylidine rnethylcarbamate] Hutachloro-1,s-butadiene Diethyl sulfate Pentachlorophenol (PCP) Methanol 2,4,6-Trichlorophenol Isopropyl alcohol(manufacturing-strong 2-Nitrophenol acid process, no supplier Picric acid notification) -o-hisidine Acetone 2-Phenylphenol Chloroform Michler's ketone Hexachloroethane Toluene-2,6-diisocyanate Triaciquone [2,6-Cyclohexadiene-14- Naphthalene dione, 2,3,5-tris(1- Quinoline ariridiny1)-] -beta-Naphthylamine -n-Butyl alcohol 3,S1-Dichlorobenzidine Benrene Biphenyl l,l,l-Trichloroethane (Methyl 4-Arninobiphenyl chloroform) Benzidine Methoxychlor [Benzen*, 1,l'-(2,2,2- 4-Nitrobiphenyl trich1oroethylidene)bir Bencoyl peroxide [I-methoxy-] Safrole Bromomethane (Methyl bromide) 2,4-D [Acetic acid, (2,4- Ethylene dichlorophenoxy) -1 Chloromethane (Methyl chloride) -o-Xylene Methyl iodide -o-Cresol Hydrogen cyanide 1,2-Dichlorobenrene Methylene bromide -o-Toluidine Chloroethane (Ethyl chloride) 1,2,4-Trimethylbencene Vinyl chloride 2,4-Diaminotoluene Acetonitrile 2,4,6-Trichlorophenol Acetaldehyde I Styrene oxide Dichloromethane (Methylene chloride) 1,2-Dibromo-3-chloropropane(DBCP) Carbon disulfide Methyl acrylate Ethylene oxide Ethylene thiourea Bromoform (Tribromomethane) C.I. Solvent Yellow 3 Dichlorobromomethane Benaoic trichloride (Benrotrichloride) Vinylidene chloride Cumene Phosgene Beneal chloride Propyleneimine Beneoyl chloride Propylene oxide Nitrobenzene -tert-Butyl alcohol 6-Nitro-2-aniaidine Freon 113 [Ethane, I,l,2-trichloro- 4-Nitrophenol I,2,2-trifluoro-] Terephthalic acid Heptachlor [1,4,5,6,7,8,8-Heptachloro- Ethylbenzene 3a14,7,7a-tetrahydro- Styrene 4,7-methano-1H-indene] Benzyl chloride Hexachlorocyclopentadiene E-Nitrosopiperidine Dimethyl sulfate 4,4'-Methylenebis(2-chloroaniline) Isobutyraldehyde (MBoCA) 1,2-Dichloropropane 4,4'-Methylenebis(N,N-dimethyl) sec-Butyl alcohol benrenamine Kthyl ethyl ketone Methylenebis(pheny1isocyanate) (MBI) 1,1,2-Trichloroethane 4,4'-Methylenedianiline Trichloroethylene 4,4'-Diaminodiphenyl ether Acrylamide Bis(2-ethylhexyl) adipate Acrylic acid 2-Aniridine Chloroacetic acid 2,4-Dimethylphenol Peracetic acid pXylene 1,1,2,2-Tetrachloroethane pCresol Dimethylcarbamyl chloride l,4-Dichlorobencene 2-Nitropropane 2-Phenylenediamine 4,4'-Isopropylidenediphenol Quinone Cumene hydroperoxide I,2-Butylene oxide Methyl methacrylate Epichlorohydrin Saccharin (manufacturing, no supplier 1,2-Dibromoethane (Ethylene notification) [1,2- dibrornide) Benrisothiaeol- 1,3-Butadiene 3(2H)-one, l,l-dioxide] Acrolein C.I. Food Red 15 Ally1 chloride 1-Amino-2-methylanthraquinone 1,2-Dichloroethane (Ethylene Quintoeene [Pentachloronitrobencene] dichloride) Diethyl phthalate Acrylonitrile Dibutyl phthalate Ethylene glycol Phthalic anhydride Chloromethyl methyl ether Butyl benzyl phthalate Vinyl acetate Methyl isobutyl ketone Chlorobencilate [Benzeneacetic acid, Maleic anhydride 4-chloro-.alpha.-(4- Q-Xylene chlorophenyl)-.alpha.- ?1-Cresol hydroxy-,ehtyl ester] Bis(2-chloro-1-methylethyl) ether 2-Chlorciaceteghenme Melamine 4,O-Dinitre-2-crerol Toluene 1,2-Dichloroethylene Chtorobenrene Ethyl chlorofomate Phenol 1,s-Dichlorebensene 2-Methoxyethanol 1,s-Dichleropropylene 2-Ethoxyethanol Bir(ch1oromethyl) ether Cyclehexme C.I. Basic Green 4 Pyridine Toluene-2,4-diirocyanate Diethanolamine Vinyl bremide Bis(2-chloroethyl) ether 2,6-Dinitrotoluene Prepexur [Phenol, 2-(I-methy1ethoxy)-, 2,4-Diamineanisele methylcubamate] N-Nitrorodi-3-propylamine Propylene (Propene) Eethyl irocyanate Dicefol [Bensenemethmol, 4-chloro- o-Toluidine hydrochloride .alpha.-(4-chlorophenyl)- ~examethYlphorphoramidc .alpha.-(trichloromethyl)-] E-Nitroso-E-methylurco 2-Amincanthraquinone -N-Nitroso-PJ-ethylurea Di(2-ethylhexyl) phthalate (DEHP) C.I. Solvent Yellow 14 Q-Dioctyl phthalate -N-Nitronodi-n-butylarnine Hexachlorobenzene Tetrachlorvinphos [Phosphoric acid, 3,3'-Dimethoxybenzidine 2-chloro-1- (2,3,5- 3,3'-Dimethylbenridine (L?-Tolidine) trichloropheny1)ethenyl Anthracenr dimethyl ester] pcresidine C.I. Basic Red 1 Catechol Propane rultone 1,2,4-Trichlerobenzene Decabromodiphenyl oxide 2,4-Dichlorophenol Sodium hydroxide (~olution) 2,4-Dinitrotoluene Molybdenum trioxide --N,N-Dimethylaniline Thorium dioxide 1,2-Diphenylhydrarine Cresol (mixed isomem) (Hydrazobeneene) Xylene (mixed isomerr) Hydroquinone Asbestos (friable) Propionaldehyde Hexachloronaphthalene Butyraldehyde Polychlorinated biphenyls (PCBs) 1,4-Dioxane Aluminum oxide Tris(2,3-dibromopropyl) phosphate Diepoxybutane Chloroprene Trifluralin [Benzeneamine, 2,6- Tetrachloroethylene (Perchloroethylene) dinitro-N,N-dipropyl-4- C.I. Vat Yellow 4 (trifiuoromethyl)-] Dirnethyl phthalate Methyl &-butyl ether Dibencofuran Nitrofen [Bensene, 2,4-dichloro- Captan [lH-Isoindole-1,3(2H)-dionc, I-(4-nitr0phenoxy)-] 3a,4,7,7a-tetrahydro-2- Chlorothalonil [1,3-Bensenedicar- [(trichloromethyl) thiol-] bonitrile, 2,4,5,6-tetrachloro-] Chloramben [Benzoic acid, 3-amino- C,I. Direct Black 38 2,s-dichloro-] Fluometuron [Urea, N,N-dimethyl-N'- -o-Aniridine hydrochloride (3-(trifluoromethyl)phenyl]-] w-Naphthylamine Octachloronaphthalene Cupferron [Beneenearnine, N-hydroxy- Diallate [Carbamothioc acid, bis N-nitroso, ammonium salt] (I-methylethyl)-, S-(2,3- Nitrilotriacetic acid dichloro-2-propenyl) ester] 4,4'-Thiodianiline C.I. Direct Blue 6 Ethyl acrylate C.I. Acid Blue 9, diammonium salt Butyl acrylate C.I. Disperse Yellow 3 Ethyleneimine (Aziridine) C.I. Solvent Oranre 7 Q-Nitrosodiphenylamine C.I. Food Red 5 Calcium cyanamide C.I. Acid Blue 9, disodium nalt Hydrazinc E-Nitroromethylvinylamine Aldrin [l,4:5,8-Dimethanonaphthalcnc, C.I. Acid Green 3 1,2,3,4,10,10-hexachloro-l14,4a, Ammonium nitrate (nolution) 5,8,8a-hexahydro-(l.alpha., Aluminum (fume or dust) 4.alpha.,4a.beta.,5.alpha., Lead 8.alpha.,aa.beta.)-] Manganese Diasomethane Mercury Carbonyl sulfide Nickel C.I. Solvent Yellow 34 (Auramine) Silver Mustard gas [Ethane,l,ll-thiobis Thallium 12-chloro-1 Antimony Arsenic Buium Shromium Com~oundr- Includu any unique chemical Beryllium rubrtance that containr chromium as Dart of that Cadmium chemical'r infrartmcture. Chromium Cobalt Cobalt Commundr - Includer any unique chemical Copwr rubrtance that containr cobalt as part of that Vanadium (fume or dwt) chemical'r infrmtmcture. Zinc (fume or durt) Titanium tetrachloridr Co~~erCom~oundr - Includes any unique chemical Hydrochloric acid rubrtance that containr copper an part of that Phorphoric acid chemical'r i~tmcture. Hydrogen fluoride Ammonia Cvanide Com~oundr- X+ CN' where X = H+ or any Sulfuric acid other group where a formal dirrociation can be Nitric add made. For uarnpb KCN or Ca(CN)2. Phorphomr (yellow or white) Sodium sulfate (solution) Glycol Ethem - Includer mono- and di- ethem of Selenium ethylene glycol, diethylene glycol, and triethylene Chlorine glycol. Ammonium sulfate (solution) R-(OCH2CH2)n-OR' Toxaphene Where n = l.2.or 3 Hydrasine rulfate R = alkyl or-a&l groupr Chlorine dioxide R'= R, HI or groups which, when Zineb (Carbamodithioic acid, 1,2- removed, yield glycol ethem with the ethanediylbir-, rinc complex] rtructure: Maneb [Carbamodithioic acid, 1,2- R-(OCH2CH2),-OH ethanediylbis-, manganere complex] Polymem are excluded from this category. Titanium dioxide C.1 Direct Brown 96 Lead Com~ounds- Includer any unique chemical -N-Nitrosonornicotine rubrtance that containr lead aa part of that chemical'r Osmium tetroxide infrastructure. Dichlorobenrene (mixed isomem) Diaminotoluene (mixed iromem) Manranere Com~oundr- Includer any unique chemical 2,4-Diaminoanirole rulfate rubstance that containr manganere aa part of that chemical'r infraatmcture. c. Chemical Categories (Effective Date Mercury Com~ounds- Includes any unique chemical January 1,1987) substance that contaim mercury as part of that chemical'r infraatmcture. Antimony Com~oundr- Includer any unique chemical substance that containr antimony- aa -Dart of that Nickel Com~ounds- Includes any unique chemical chemical's infraatmcture. rubrtance that containr nickel as part of that chemical's infrastructure. Arsenic Com~ounds- Includer any unique chemicd substance that containr arsenic aa part of that chemical'r infrastructure. Barium Com~ounds- Includer any unique chemical substance that contains bariumaa part of that chemical'r infraatmcture. where x = 1 to 10 Bewilium Com~ounds- Includes any unique chemical rubatance that contains beryllium aa part of that Selenium Com~ounds- Includes any unique chemical chemical'r infrastructure. rubstance that containr aelenium aa part of that chemical'r infraatmcture. Cadmium Com~ounds- Includer any unique chemical substance that containr cadmium aa part of that Silver Com~ounds- Includes any unique chemical chemical'r infraatmcture. rubstance that contains silver aa part of that chemical'r infraatmcture. Thallium Com~ounds- Includes any unique chemical rubstance that contains thallium as part of that chemical'r infrastmcture. Zinc Com~oundr- Includes any unique chemical where x = 1 to 6 subntance that containa rinc aa part of that chemical'r infraatructure.