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Manual of Tests and Criteria Copyright © United Nations, 2019. All rights reserved ST/SG/AC.10/11/Rev.7 Manual of Tests and Criteria Seventh revised edition UNITED NATIONS New York and Geneva, 2019 Copyright © United Nations, 2019. All rights reserved NOTE The designations employed and the presentation of the material in this publication do not imply the expression of any opinion whatsoever on the part of the Secretariat of the United Nations concerning the legal status of any country, territory, city or area, or of its authorities, or concerning the delimitation of its frontiers or boundaries. ST/SG/AC.10/11/Rev.7 Copyright United Nations, 2019 All rights reserved. No part of this publication may, for sales purposes, be reproduced, stored in a retrieval system or transmitted in any form or by any means, electronic, electrostatic, magnetic tape, mechanical, photocopying or otherwise, without prior permission in writing from the United Nations. UNITED NATIONS PUBLICATION Sales No. E.20.VIII.1 ISBN 978-92-1-130394-0 eISBN 978-92-1-004503-2 ISSN 1014-7160 eISSN 2412-4664 Copyright © United Nations, 2019. All rights reserved INTRODUCTION The "Manual of Tests and Criteria" contains criteria, test methods and procedures to be used for the classification of dangerous goods according to the provisions of the "United Nations Recommendations on the Transport of Dangerous Goods, Model Regulations", as well as of chemicals presenting physical hazards according to the "Globally Harmonized System of Classification and Labelling of Chemicals (GHS)". It therefore also supplements national or international regulations which are derived from the Model Regulations or the GHS. Originally developed by the Economic and Social Council’s Committee of Experts on the Transport of Dangerous Goods, which adopted a first version in 1984, the Manual of Tests and Criteria has been regularly updated and amended. Currently, the updating is done under the auspices of the Committee of Experts on the Transport of Dangerous Goods and on the Globally Harmonized System of Classification and Labelling of Chemicals, which replaced the original committee in 2001. At its ninth session (7 December 2018), the Committee adopted a set of amendments to the sixth revised edition of the Manual as amended by Amendment 1. This seventh revised edition takes account of these amendments, which were circulated as document ST/SG/AC.10/46/Add.2. In addition, noting that the work to facilitate the use of the Manual in the context of the GHS had been completed, the Committee considered that the reference to the "Recommendations on the Transport of Dangerous Goods" in the title of the Manual was no longer appropriate, and decided that from now on, the Manual should be entitled "Manual of Tests and Criteria".1 The new amendments adopted in 2018 include: - A full review of the text of the Manual to facilitate its use in the context of the GHS; - A new test under test series 8, to determine the sensitiveness of a candidate ammonium nitrate emulsion or suspension or gel, intermediate for blasting explosive, to the effect of intense localised thermal ignition under high confinement (sub-section 18.8); - New provisions addressing classification of polymerizing substances for transport; - Stability tests for nitrocellulose mixtures (new Appendix 10); and - A compilation of classification results on industrial nitrocellulose in accordance with Chapter 2.17 of the GHS which can be used for the classification of industrial nitrocellulose based products (new Appendix 11). 1 See the report of the Committee of Experts on its ninth session, document ST/SG/AC.10/46, para.19. - iii - Copyright © United Nations, 2019. All rights reserved Copyright © United Nations, 2019. All rights reserved GENERAL TABLE OF CONTENTS Section Page 1. GENERAL INTRODUCTION (Introduction, Hazard classes in the Model Regulations and in the GHS, Precedence of hazard characteristics, Layout, Safety, General conditions for testing, Recommended tests and Reporting) ........................................ 1 PART I: CLASSIFICATION PROCEDURES, TEST METHODS AND CRITERIA RELATING TO EXPLOSIVES 10. INTRODUCTION TO PART I (Purpose, Scope, Acceptance procedure, Assignment procedure, Examples of test reports) ...................................................................... 15 11. TEST SERIES 1 (To determine if a substance has explosive properties) .................................... 39 12. TEST SERIES 2 (To determine if a substance is too insensitive for inclusion into the class of explosives) .................................................................................. 59 13. TEST SERIES 3 (To determine if a substance is an unstable explosive in the form in which it was tested) ............................................................................................. 79 14. TEST SERIES 4 (To determine if an article, packaged article or packaged substance is too dangerous for transport and classified as a GHS unstable explosive) .............................. 143 15. TEST SERIES 5 (To determine if a substance may be assigned to Division 1.5) ....................... 149 16. TEST SERIES 6 (To assign a substance or article to Division 1.1, 1.2, 1.3 or 1.4 or exclude it from the class of explosives) ................................................................................. 163 17. TEST SERIES 7 (To determine if an article may be assigned to Division 1.6) ........................... 177 18. TEST SERIES 8 (To determine if an ammonium nitrate emulsion, suspension or gel, intermediate for blasting explosives (ANE), is insensitive enough for classification as an oxidizing substance, and to evaluate the suitability for containment in tanks) ...................... 199 PART II: CLASSIFICATION PROCEDURES, TEST METHODS AND CRITERIA RELATING TO SELF-REACTIVE SUBSTANCES, ORGANIC PEROXIDES AND POLYMERIZING SUBSTANCES 20. INTRODUCTION TO PART II (Purpose, Scope, Preliminary procedure, Classification procedures, Example of test report) ..................................................................... 231 21. TEST SERIES A (To determine if there is propagation of detonation) ....................................... 243 22. TEST SERIES B (To determine if there is detonation in the package) ....................................... 255 23. TEST SERIES C (To determine if there is propagation of deflagration) ..................................... 259 24. TEST SERIES D (To determine if there is rapid deflagration in the package)............................ 269 25. TEST SERIES E (To determine the effect of heating under confinement) ................................. 271 26. TEST SERIES F (To determine the explosive power) ................................................................. 287 27. TEST SERIES G (To determine if there is thermal explosion in the package) ........................... 307 28. TEST SERIES H (To determine the self-accelerating decomposition temperature) ................... 311 - v - Copyright © United Nations, 2019. All rights reserved GENERAL TABLE OF CONTENTS (continued) Section Page PART III: CLASSIFICATION PROCEDURES, TEST METHODS AND CRITERIA RELATING TO VARIOUS HAZARD CLASSES 30. INTRODUCTION TO PART III (Purpose, Scope) ..................................................................... 339 31. CLASSIFICATION PROCEDURES, TEST METHODS AND CRITERIA RELATING TO THE FLAMMABILITY OF AEROSOLS ...................................................... 341 32. CLASSIFICATION PROCEDURES, TEST METHODS AND CRITERIA RELATING TO LIQUID DESENSITIZED EXPLOSIVES AND FLAMMABLE LIQUIDS .......................................................................................................... 355 33. CLASSIFICATION PROCEDURES, TEST METHODS AND CRITERIA RELATING TO FLAMMABLE SOLIDS, SOLID DESENSITIZED EXPLOSIVES, SUBSTANCES LIABLE TO SPONTANEOUS COMBUSTION AND SUBSTANCES WHICH, IN CONTACT WITH WATER, EMIT FLAMMABLE GASES............................... 365 34. CLASSIFICATION PROCEDURES, TEST METHODS AND CRITERIA RELATING TO OXIDIZING SOLIDS AND LIQUIDS .......................................................... 381 35. DETERMINATION OF CHEMICAL INSTABILITY OF GASES AND GAS MIXTURES ............................................................................................... 401 36. Reserved .................................................................................................................................. 409 37. CLASSIFICATION PROCEDURES, TEST METHODS AND CRITERIA RELATING TO SUBSTANCES CORROSIVE TO METALS ................................................ 411 38. CLASSIFICATION PROCEDURES, TEST METHODS AND CRITERIA RELATING TO SUBSTANCES AND ARTICLES OF TRANSPORT CLASS 9 ................... 415 39. CLASSIFICATION PROCEDURE AND CRITERIA RELATING TO SOLID AMMONIUM NITRATE BASED FERTILIZERS ........................................................................................... 435 PART IV: TEST METHODS CONCERNING TRANSPORT EQUIPMENT 40. INTRODUCTION TO PART IV (Purpose, Scope) ..................................................................... 443 41. DYNAMIC LONGITUDINAL IMPACT TEST FOR PORTABLE TANKS AND MULTIPLE-ELEMENT GAS CONTAINERS (MEGCs) ........................................................ 445 PART V: CLASSIFICATION PROCEDURES, TEST METHODS AND CRITERIA RELATING TO SECTORS OTHER THAN TRANSPORT 50. INTRODUCTION TO PART V (Purpose, Scope) ...................................................................... 457 51. CLASSIFICATION PROCEDURES, TEST METHODS AND CRITERIA RELATING TO THE HAZARD CLASS DESENSITIZED EXPLOSIVES ................................................
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