5-Methoxy-DALT the Drug Enforcement Administration's Special Testing and Research Laboratory Generated This Monograph Using Structurally Confirmed Reference Material

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5-Methoxy-DALT the Drug Enforcement Administration's Special Testing and Research Laboratory Generated This Monograph Using Structurally Confirmed Reference Material 5-Methoxy-DALT The Drug Enforcement Administration's Special Testing and Research Laboratory generated this monograph using structurally confirmed reference material. H2C N CH2 O H3C N H 1. GENERAL INFORMATION IUPAC Name: N-[2-(5-methoxy-1H-indol-3-yl)ethyl]-N-(prop-2-en-1-yl)prop-2-en-1-amine CAS#: 928822-98-4 (Base) Synonyms: 5-MeO-DALT, 5-Methoxy-N,N-Diallyltryptamine, N,N-Diallyl-5-methoxytryptamine Source: DEA Reference Material Collection Appearance: White powder (Base and HCl) UVmax(nm): 220 (Base) 2. CHEMICAL AND PHYSICAL DATA 2.1 CHEMICAL DATA Form Chemical Formula Molecular Weight Melting Point (oC) Base C17H22N2O 270 105.1 . HCl C17H22N2O HCl 306 160.3 Latest Revision: 07/30/15 SWGDRUG.org/monographs.htm Page 1 of 7 5-Methoxy-DALT The Drug Enforcement Administration's Special Testing and Research Laboratory generated this monograph using structurally confirmed reference material. 3. QUALITATIVE DATA 3.1 NUCLEAR MAGNETIC RESONANCE Sample Preparation: (Base) - Dilute analyte to ~10 mg/mL in CDCl3 containing TMS for 0 ppm reference and methenamine as quantitative internal standard. Instrument: 400 MHz NMR spectrometer Parameters: Spectral width: at least containing -3 ppm through 13 ppm Pulse angle: 90o Delay between pulses: 45 seconds 1 HNMR, 5-Methoxy-DALT Base, Lot K8H81105, CDCl3, 400MHz Methenamine 10 9 8 7 6 5 4 3 TMS 2 CHCl3 1 HDO 0 1 1 1 1 2 4 3 4 4 8 7 6 5 4 3 2 1 0 CHCl3 1 1 1 1 1 2 4 3 4 4 8.0 7.9 7.25 7.00 6.00 5.90 5.25 5.15 3.90 3.80 3.25 3.20 2.90 2.80 Latest Revision: 07/30/15 SWGDRUG.org/monographs.htm Page 2 of 7 5-Methoxy-DALT The Drug Enforcement Administration's Special Testing and Research Laboratory generated this monograph using structurally confirmed reference material. Sample Preparation: (HCl) Dilute analyte to ~30 mg/mL in D2O containing TSP for 0 ppm reference and maleic acid as quantitative internal standard. 1 HNMR, 5-Methoxy-DALT HCl, Lot RM-131001-04, D2O, 400MHz HDO 10 9 8 7 6 5 Maleic Acid (ISTD) 4 3 TSP 2 1 0 1 1 1 1 2 4 34 2 2 8 7 6 5 4 3 2 1 0 1 1 1 1 2 4 3 4 2 2 7.25 7.00 5.90 5.85 5.625 5.575 3.90 3.85 3.80 3.4 3.3 3.2 Latest Revision: 07/30/15 SWGDRUG.org/monographs.htm Page 3 of 7 Latest Retention Acquisition Tune Threshold: MS Injection 3) 2) 1) Oven MS MS MSD Temperatures: Carrier Column: Instrument: Sample 3.2 0.25 0.50 4 6 GAS Intens... [x 10 ] Intensity [x 10 ] Parameters: Revision: Preparation: Gas: EI+ EI+ CHROMATOGRAPHY/MASS DB-1 Parameters: 40 40 Time: 41 41 Agilent 41 41 The Helium 07/30/15 Drug generated 14.548 60 55 60 55 Dilute Enforcement Injector: 68 68 Split EI 80 80 Mass this 81 81 analyte monograph Spectrum, 100 100 Administration's ~4 SWGDRUG.org/monographs.htm Mass 110 110 mg/mL Quad: Source: 120 120 Ratio file: scan program: 117 117 transfer 117 117 MS using 5-Methoxy-DALT SPECTROMETRY 5-Methoxy-DALT min at gas 280 Hold Ramp 100 stune.u (or 1 into 150 130 130 range: 130 130 = 130 130 100 chromatograph mode: 140 140 structurally mL/min 230 20:1, equivalent); o line: o C C final chloroform o Special to C 145 145 initial o 30-550 C 1 scan 280 300 160 160 temperature m 160 160 L temperature o Testing o injected C confirmed C Base, amu at 30m (Base). operated 180 180 174 174 12 x Lot and o C/min 0.25 186 186 for reference K8H81105 for 200 200 Research in 9.0 199 199 mm split 1.0 min x min 220 220 mode 0.25 material. Laboratory m 229 229 with m 240 240 241 241 MS detector 260 260 Page 4 270 270 of 270 270 m/z m/z 7 407 407 7 426 528 426 426 of 442 5 638 488 760 791 499 Page 839 916 579 1007 1007 933 638 Wavenumber (cm-1) 1059 1105 Wavenumber (cm-1) 1173 1211 714 700 1219 714 Laboratory 1240 material. 760 K8H81105) 1414 791 1448 802 1448 802 800 1491 839 (Lot 1491 839 1500 Research 1585 852 reference 900 Base 916 and bounce) 933 (3 978 1007 1000 confirmed Testing 2000 1059 32 1105 1100 attachment Special scans: 1173 5-Methoxy-DALT 1211 structurally ATR 1219 1200 2500 32 -1 1240 1273 5-Methoxy-DALT using cm 8 Bounce), 1300 4 scans: background diamond 3 150 2839 1352 (FTIR) SWGDRUG.org/monographs.htm of of gain: 2877 Administration's 2877 with 1414 1414 1400 3000 1448 monograph 1448 FTIR Number Number Resolution: Sample Aperture: 1491 (Diamond, this 1500 Enforcement ATR 1585 1600 3500 generated SPECTROSCOPY Drug 07/30/15 FTIR, The 1700 Revision: Parameters: %Transmittance %Transmittance INFRARED 55 65 60 70 80 75 60 55 70 65 75 80 Latest Scan Insrument: 3.3 7 575 of 642 6 714 729 714 804 Page 831 903 575 933 991 642 Wavenumber (cm-1) 642 1076 656 Wavenumber (cm-1) 1107 1223 714 700 1240 729 Laboratory 729 material. 1423 760 1462 804 RM-131001-04 1493 800 1493 831 1587 1500 Lot Research reference 903 900 and 933 HCl, 991 1001 1000 confirmed 2000 Testing 1039 1066 1076 1107 1100 Special 2469 1186 structurally 5-Methoxy-DALT 2505 2505 1223 1200 2528 2500 1240 5-Methoxy-DALT using 1296 1300 Bounce), 3 SWGDRUG.org/monographs.htm Administration's 1423 1400 3000 1462 monograph 1462 3165 1493 this 1500 (Diamond, Enforcement 1587 ATR 1600 3500 generated Drug 07/30/15 FTIR, The 1700 Revision: %Transmittance %Transmittance 64 56 48 72 48 56 64 72 Latest 5-Methoxy-DALT The Drug Enforcement Administration's Special Testing and Research Laboratory generated this monograph using structurally confirmed reference material. 4. ADDITIONAL RESOURCES http://en.wikipedia.org/wiki/5-MeO-DALTWikipedia http://forendex.southernforensic.org/index.php/detail/index/1115Forendex Latest Revision: 07/30/15 SWGDRUG.org/monographs.htm Page 7 of 7.
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