Initial Calibration Data Semtvolatile HSL Compounds (Pagel) Case No: 3SQ>7~-______Instrument tD; Contractor: gMCOTT&C-______Calibration Date: 3./M-/&S" Contract No: 6&-g»3-"feWf______
Minimum RF for SPCC is 0*050 Maximum % RSD for CCC is 30%
Hesponw Factor (subcchpt is th« amount of nanogramt) SPCC -Syswm P«r*ormance Check Compound* (e.j RF -Avtrae« Retoonsa Factor , t -not d«tectataf« at 20 ng %RSD -Parcam Relative Standard Daviation CCC -Cal.brat.on Chack Compound. M
FormVI " - 4/84 Initial Calibration Data Semivolatile HSL Compounds (Page 2) Case No: -33O1—_____' Instrument ID: Contractor: ^COTEC,______. Calibration Date- 3-/2~:L/&S" Contract No:
Minimum RF for SPCC is 0.050 Maximum % RSD for CCC is 30%
Laboratory ID -B ita. i'2..3- CCC- Compound RF120 «F160 RF %RSD SPCC 2. 4-Dinitrotoiuent 2. 6-Pinitfototuene_____ &.'& 0.3ZV Diethylphthalate 4 - Chlor ophenyl -phanytether Fluorene »• 4-Nitroaniiine ^ ii>. :L-S| o/zet 4. 6-Dmttro-2-Methytphenol w. )°il N-Nitrosodiphenylamine (1 ) 4 - Bromophenyl -pheny let her Hexachlorobenzene o.l&l Pentachiorophanol O.tOf /3 Phenanthrene Anthracene 6 Dt-N-Butylphthalate Fluoranthene Benzidme 7® Pyrene Butylbenzylphthalate 2-3 3. S'-Dichlorobenzidme O.6ST Si Benzofa fcAnthrace ne .S6C. A bis<2-£thylhe*vl|Phthalaie 0.899 3? -- Chrysene LSI J Di-n-Octyl Phthalate Benzo(b)Fiuoranthene /.Z-30 /& Benzo( k |F luora nthene i.J-S* /a BenzoiajPyrene o.eeo IndenoO. 2. 3-cd}Pyrene . 5 S 5 Dioenz(a. hlAnthraeene h. t}Perylene O-foS"? /s
Response Factor {subscript is the amount of nanograms) SPCC -System Performance Check Compounds (••) RF .Average Response Factor t -not dttectable at 20 ng %RSD -Percent Relative Standard Deviation 0) 'Cannot be separated from dtphenylamine CCC -Calibration Check Compounds (•)
FormVt
ARIQ'0330 4/B4 uonunuing uaiioration Cheek Semivolatiie HSL Compound* (Pagel)
Case No: Contractor: &V^>7&C______Time: Contract No: && -&*-&-&¥ Laboratory ID: instrument ID: _____ &&L ______Initial Calibration Date:
Minimum RF for SPCC is 0.050 Maximum %D for CCC is 25%
Compound %D CCC SPCC N • Nit rosodimethyta mine A Phenol Aniline AO/O ryt*-* E but • 2 -ChloroeihyljE th«r 2-ChlofOpheno*
1. 4-Otchtorobenzene Benzyl Alcohol 0,3/2- Mo » os i *h i 2-Oichlorobanz«ne f 2 • Methylphenol bi&(2 -chloroi£Qprocyl}£lher 4-Merhylphenol N-Nrtroso-Di-n-Propyiamine 0.2.3C He xachlor oethane H Nitrooenzene Isophof one , 2-Nnrophenof £3-7,3? 2, 0,1V*]- m • 2 -CnlocoeihoxyJMethane 2. 4-Dichlorophenol O-T-BQ 1 2 4-TnchlofObenzene O-30/ Naphthalene 4.Chloroanilme Hexachtorobuiadiene 4 Cnloro-3-Methyiphenoi
Hexachlofocyclcpentadiene 0,3/2- 2-S 2. 4, B-TrtchJoropheno* 0-3&5" 2, 4, S'Tnchlorcpheno! 2 • Cnioronaptithalene 2 -Nirroarwlme Z2- Otmethyl Phthalate Acenaphthyfene 3-Mtiroanihne Acenaphthene A302. A/33 2 4-Diniuophenot Q.t+l 4>Nitropr>enoJ 2.3 Dibenzofuran A
RP50 H*«»"** ^acior *rom daily standard file at concentration %0 -Percent Difference indicated CCC -Calibration Check Compounds (.} RT Average Response Factor from initial calibration FermV) SPCC -System Performance Check Compounds {••)
Form VII 4/84 Continuing Calibration Check . Semivolatlle HSL Compounds (Page 2)
Case No: 3603______Calibration Date: Contractor: &JCz>T&C~______Time: ______Contract No: G& -Vlrdfo^ _____ Uboratory ID: Instrument ID: - ______; ____ initial Calibration Date:
Minimum RF for SPCC is 0.050 Maximum %D for CCC is 25%
Compound Iff RF80 SD CCC SPCC 2, 4-OinrtrotoiiMfW o.3"?-r O-330 /2- 2, C-Oinrtrotoiuane 0,32^2- 0,^*7"?" 6 Diethylphthjlate /.31& /./99 \ RFtn -Response Factor from daily standard tile ai concentration CCC -Calibration Check Compounds {•) indicated SPCC -System Performance Chech Compounds RT -Average Response Factor from initial calibration Form VI (1) -Cannot be separated from diphenylamme °»D Percent Difference ^. _ Form VII WI00332 4'84 Continuing Calibration Check Semivolatile HSL Compounds (Page!) Case No: 3&03______Calibration Data: Contractor: ^/CQ-TgC.______Time: ______ll:Zg> Contract No: ---- ______Laboratory ID: Instrument ID: (25GSL.______- Initial Calibration Date: Minimum RF for SPCC is 0.050 Maximum %D (or CCC is 25% Compound RF %D CCC SPCC N • Nitrosodimethylamine A 7/3 75" Phenol Aniline 14 t»t(-2-CMoro*thyl)Eth«r 2-. 2 •Chloropbenoi 1 , 3 Dtchiorobcnzene 1.ST& 7^33 Beruryl Alcohol f.cxfi 2-Methylphenol /.sen* bis(2-cftioroi*opfopYl)Elh*r 4. Methylphenol N-Nitroto-Cfc-n-PTOpytamine 23 * * Hexachioroethane Nitrobenzene isophorone 2-Nitrophenol 2, 4-Dimathylphenol 7-0 Benzoic Actd bis{ • 2 -ChloroeihoiyJMetriane 2. 4-Dichlorophenoi £>.*-«?? 1 2, 4 Tnchlorobemene Naphtnaiene 4-Cnlorosndinr &.2&C He xachlor obutadiene 4 - Chloro-3-Methyipheno! 2 • Methylnaphinalene Mexdchior ocyclopentadjene - 2 4, 6-Tr»chiorophenol /o 24 5-Tr»chIorophenol 2-Chloronaphihftlene 2'Nitroamtine Dimethyl Phthatate Acenaphthylene 3 Niuoanihne Acenapnthene 2, 4-Dmitrophenol 4-Nitrophenoi Drbenzofuran P*cio* from daily standard file at concentration %D -Percent Difference indicated CCC -Calibration Check Compounds (.) ST Average Response Factor from initial calibration Form VI SPCC -Sv*«*«W BertormancIff§33e Chec3 k Compounds (• 0 Form VII ^wv Continuing Calibration Ctwck ._, S«mivolatile HSL Compounds (Page 2) lr Case No: 3&03______Calibration Date: Contractor: &SC&7T£C~ ______Time: Contract No: —J^ ______Laboratory ID: Instrument ID: ____ - |nitiai Calibration Date: Minimum RF for SPCC i> 0.050 Maximum %D for CCC is 25% Compound RF %D CCC SPCC 2, 4-Diniiroto*i>ene Z-fc 2, o-Dmrtrotolueoe 2-3 Dtethyiphthalata 4-Chlwophenyf-phenytather 2.0 Ftuoren* 4-Nitroaniltne 4. 6-Dinitro-2-Methylph«nol O./ft? N'NitrosodiphcnyUrnin* (1 ) 4'Bromoph*nyt-pnftnyl0th*r H«xachk>rob«nrene O.i&l Z-2- Pentachlorophenol o. ft Phenanthrane Anthracene Di -N -Butyl Phthalate Fluoranthene /s Benzidin* Pyreon 2-0 Butylbenrylphthalata A// zo 3, S'-DtchJorobenzHJine "$£&' BenjotaiAnthracone it bi s(2 - Chrysene i. Di-n-Octyl Phthaiata A 6enzo(b)Fiuoranthen« AZJO Benzotk)F| uoranthene /3 Benxo(a)PyTtne Indanofl . 2. 3-cd)Pvene Dibenz(a, h)Anihric*n* i Benzo(g. h. i)Perytan« RFgQ -Response Factor from daily standard t*te at concentration CCC -Calibration Check Compounds (•) indicated SPCC -System Performance Chech Compounds {* •) HT -Average Response Factor from initial calibration Form Vt (1) -Cannot be separated Irom diphenylamine DoD Percent Difference • ••—T- Form Vt) 4/84 Case -o. __*p &• & ^ Laboratory fueej* Contract No. _._ £$-£/' 6 -re,-/ Column _g^--#"•/& Date of Analj,«i* 3/V--5/tr/ 4.4'-DDT JW7 {_**'* JSV&f* /&* 0 DIBUTYL CHLORENDATE ^^ 3**7 ^$r<&& s.y EVALUATION CHECK FOB 4.4'-DDT/ENDRIN BREAKDOWN PERCENT BREAKDOWN EXPRESSED AS TOTAL DEGRADATION EVAL. MIX B EVAL. MIX B EVAL. MIX B EVAL. MIX B ENDRW **l ^',3 tf & 4,4'-DDT ^-'/ ^/ ^ * LABORATORY 10 fgflt- &,£)£" £vs*t- C1*/** eitjtt. &,&/ £ t>'<*tr £J,0 / TIME OT ANALYSIS $.&$ /# . SB ^:z$ /.03T EVALUATION OF RETENTION TIME SHIFT FOR DIBUTYLCHLORENDAT6 SMO LAS TIME OF PERCENT SMO LAB TWEOF SAMPLE NO* ID ANALYSE DIFK* SAMPLE NO. to ANALYSIS A?. $3 C tt'tx & /¥ - /***, c 7y«v x? /-37 C 2% PACKED, *0.3% CAPILLARY * 5 u: s^ ^ ^ R V' i8o! •i tO c. \^ ^? m 1 • v ^j ^ \ ^, F f v\ V. y *^ O 1^ ig I o" r\^ »•• *• ^* ^^ o fv> f*f\ ^- rT\ •c 01 u ^ f\ ^ * 5t g ii r^- E V6 aI J N So ^ ^ "^ h* ' i o « « > *• 3E ^" 5 • «* S e « »- ) ^B fe fc < G U ,-S cc rf rs r^~ 5 ) H CO s * • S < V V «* ^4 t- « a »- 2 — — ^X c< c r< 1 * * • o ^ z t .V)T V ^ ^i 5 57 : *• 51 ^ o " • ^ i CJ ^ •^. ) ^^ ^ 2 P g I >» c w\ ) |E ^ 2 £ ^^ * ^^_ 1" ^ \ $SE *u; *C f \ ^ rv f ^ I S te « i g ^ ^ rv 5r \ ^ ; / - .? * i_! \ u. c . s> S ^ ^ f\ c^ ° v W A " * •^ — » Sh- ^ MM 7w .?^ ,- c ~L*! ^ 5 i•i ro ^ -c C e ^ S C3 ^ r^ § •' IT o 2) ^- € i > Xa u ^ ^ ^ - E 1'* O 4» *• 2 s • « ^^ * •e• 4 t^ ' 0 C & fc S* *- h (S c^ ^ ^ v" ^ C U (C tv rx •^ ^ ^H ^ ,m^ . , * * 1- 1k ^0 X » 5 ^ X. ^ « • _ mto ION ABUNDANCE CRITERIA %RELATIVE ABUNDANCE 61 30.0 ' OOM ol man 190 ¥-3.7- \ at Im then 2.0% of n»» 9 O Co. 00 m*M 00 rtiative tbundtnct V6.7 70 1m ttien 2 J* of mm 69 ® «zj; t27 40.0 • O0.» of me» 198 Vo-o 197 IMS tfwt 1 J% of miu 199 <2> 1M bM» pt«kr 100% rttHhrt ebundeACi /00 1» 6.0 - 9JQ* ol mm 191 6,76 275 10.0 -30.0% of m«» 198 /«,. SAMf LI ID LAtID DATE OF ANALYtlS TIME OF ANALYSIS 1.7. 13 ftR!D0338 DtcafJuorotrlphtnylphotphin* (OFTPP) Cm No. ,. 3603 f y*Sg> con^a, —&SCCT&C—————— Contract No. Inttrumtm ID - ^*~ D-f - .j-Pg/frST ID m/. |OM ABtmOANCC CRITERIA KRELATIVE ABUNDANCE SI 30J)-8fXO%af MHT98 ^S.S ** thin 2.0% of mutOO * <2> (^)f 89 im» 89 rtUttvt abcvidanc* 5Sf 70 ^.t^j.oxo/~-«r 0 (<2)' T27 40.0 * 804)% o* mo* f 98 ^i,7 197 IwthMlA^MalM <5 199 UM peek, 100% rtiitirt abundmci /00 198 M.fJUrfmMUW ^75 27S J00.3aO»of««i«8 /w*» ^^ 306 gr««tor ttiM 1J30% of mm 198 / jL-^% 441 prntftt. but tea thjn mw» 443 ••* /O 447 oruttr than 4QJJ% of mew 108 443 t7.0-23.0%ef n»«W //.V- fA<3J *V*H* in portnthtti* It % R»» 88. 2? 2V«lut In ptrtnthttfe Is % flmt 442. XI THIS PERFORMANCE TUNE APPLIES TO THE FOLLOWING CD SAMPLES, BLANKS AND STANDARDS. CD SAMPLE ID LAB 10 DATE OF ANALYSIS TIME OF ANALYSIS tRt CALIBRATION Dtcafluorotriphenylphosphine (DFTPP) No. contractor Instrument ID w~^ Date ~'"("=______Time Lab in **** r rl.5 J- Data Retgase Authorized By: _ m/t ION ABUNDANCE CRITERIA %RELATIVE ABUNDANCE 51 30.0- 60.0% of mass 198 0* J5 68 less than 2.0% of mass 69 C C^>' 69 man 69 relative abundance 11.7 70 less than 2.0% of man 69 c f ° J t27 40.0 - 60,0% of mass 198 y/,J~r 197 . ieu than 1.0% of mass 198 • o 198 bast peak, 100% relative abundance /£>& .C 199 5.0 -9.0% of mass 198 iv.'ic 275 10.0 -30.0% of mass 198 ,S.K 365 greater than 1.00% of mass 198 /,z1 441 present, but less than mass 443 • 9.*J 442 greater than 40.0% of mass 198 bV. 90 443 17.0 -23.0% of mass 442 U.*4 (/? )2 Value in parenthesis is % man 69. 'Value in parenthesis is % mass 442. CD THIS PERFORMANCE TUNE APPLIES TO THE FOLLOWING -3" SAMPLES. BLANKS AND STANDARDS. CD CD SAMPLE ID LAB ID DATE OF ANALYSIS TIME OF ANALYStS3^ *H WC/aVIS TUNING AND MASS CALIBRATION ,df Bromofluorobanzen* (BFB) C.«NQ. contractor OontfKfl*, tn Ub ID Data Rtlei$t Authorteed fly: m/e ION ABUNDANCE CRITERIA %RELATIVE ABUNDANCE 50 75.0 . 40.0% of Iht fca» peak za. s~ 75 3OO • 80^)% of tht bnt p«k ^zs.7 95 Saw p«*k, 100% relative abundanct / SAMPLE LAB ID DATE OF ANALYSIS TIME Of ANALYSIS C-7302. PR03ECT NAME; SouM/JljiU? Sajpflla- EPA SITE NO.: Vfl |2 1 TDD NOs F^ftO-Oftloft l « ' "T REGION; QUALITY ASSURANCE REVIEW OF INORGAFllC ANALYTICAL DATA PACKAGE Case No.: <3 Co O D ______Applicable Sample No's.: Contract No.; /o8-n/r-kft§2 ______. _ WY^tt3OfrnC4?3f; Wf 43-32, Contract Laboratory: .VEfiSAft. . WV^rvP^!) Vng4l1-l; Applicable IFB No.: ______„ Reviewer: ~ Review Date: S5 ______WTfa W^RZ. The inorganic analytical data for this case has been reviewed. The quality assurance evaluation is summarized in the following table: Reviewer's Evaluation* Fraction TASK 1 TASK 11 TASK II TASK III ICPor AA FURNACE AA COLD VAPOR A A CYANIDE METALS METALS MERCURY Acceptable v/ Acceptable with except onis. /£\^f*3 y ^ , *3 /43 juestionaWe Jnacceptabie * Definitions of the evaluation score categories are listed on next page. This evaluation was based upon an analysis of .the review items indicated below: • DATA COMPLETENESS • INITIAL CALIBRATION VERIFICATION • BLANK ANALYSIS RESULTS • CONTINUING CALIBRATION VERIFICATION • MATRIX SPIKE RESULTS • INTERFERENCE QC RESULTS • DUPLICATE ANALYSIS RESULTS • DETECTION LIMITS RESULTS • STANDARD ADDITIONS RESULTS • INSTRUMENT SENSITIVITY REPORTS ± • QUANTITATIVE CALCULATIONS Data review forms are attached for. each of the review items indicated above. ^No errors noted, no form attached. Q Spot C heck perf orm ed. Comments: ^H^lpOjv^ /Luu (vlxwK On^Jyp 1/1 rLkCMr*4^a&tr£> ARiOOSlf DATA EVALUATION SCORE- CATEGORIES ACCEPTABIE: Data, is within established control limits, or the data which is outside established control limits does not affect the validity of the analytical results. AOCEPgABJJE WISH EXCEPTIONCS ) .• Data is not completely within established control limits. The deficiences are identified and specific data is still valid, given certain qualifications which are listed below E: Data is not within established control limits. The deficiences bring the validity of the entire data set into question. However, the data validity is neither proved nor disproved by the available information« UKAOCEPTA3I£: Data is not within established control limits. The deficiences imply the results are not meaningful. en -IT 00 CD cr •~ DATA , COMPLETENESS CONC./ MATRIX I/A Co 1U ul^ ^*A Tk VH UU ^ A^ %»? %f "/^ ww Ife TRAFFIC jVMI 2>6 31' 33 55 3(p Vj REPORT #lHvlT 9\ ^ 3> T-\ ^3 M ^ %^? LAB I.D. *t <3- ^SrTi V3 •L 31 3^ 3-$ -s ^^ 31 ^(r. ^0 Mr- ^T^ft ^ FIELD QC BLANK " DUPLICATE y • S \f V y/ SPIKE s/ ^N/ \( y TASK 1 ; / — 1 RAW DATA 4— 1 WM ~ v n MM. V METALS TAB. RESULTS •J \_ TAB. D.L.'s /- ., ^ QA FORM V ^ ICAR INTER. QC V ' INSTR. SENS. \ V \ TASK II : RAW DATA J FURNACE \ AA: TAB- RESULTS v METALS v TAB. D.L.'« V V QA FORM iS x. INSTR. SENS. y/ \ TASK 11 : RAW DATA v COLD VAPOR N, AA:- . TAB. RESULTS ./ , MERCURY TAB. p.L.'s y- V / \ QA FORM v" INSTR. SENS. N. TASK Mi: RAW DATA > CYANIDE \ TAB. RESULTS f ' \^ TAB. D.L.'s v - QA FORM. y— V •^ INSTR. SENS. ' V """^^LJff Q ^^^ wT"W.^^ RAW DATA ^-^ ^^ T*ft^ESULTS **^ -^ TAB. D.L.'I^^^. ^••vn ^-" QA FORM •^-H **"" ^-^ i _ ->^^ INSTR. SENS. ^^-^^_ ^^v*^ -""'" ^-^ OTHER RAW DATA -^ -<-* (SPECIFY); -^^ TAB. RUSULTS ^^ "*^H ^ ^^. ^-^ TAB. D.L.'s^--'' -•^ - ^A-FORM "-^^^> "^^. INSTR. SENS. * ^ COMMENTS:, •ffhMfll •l^M^ DATA - COMPLETENESS CONC./ 1 uf i P MATRIX ^ % %P 2s.Jtd %f \ u/^ %\ %? REPORT * ^ '-ib WL> 63 Vfl w BC> ^Pfff «ef LAB |.D. # ^ L - f4 5> \S ' *- ^ u L. &1*5 &{* *f5 "1r FIELD QC SLANK \/ / ^/ / DUPLICATE SPIKE j TASK I ; RAW DATA w .\ (CAP OR AA ; v METALS TAS. RESULTS / TAB. D.L.'s V V QA FORM \/ v (CAR INTER,oc / \ WSTR. SENS. yt. \. TASK 11 : RAW DATA v FURNACE J- AA: TAB. RESULTS /• _ X. METALS TAg. D.L.'s \/ V ^ QA FORM / 4 INSTR. SENS. x/ TASK II : RAW DATA y s^ COLD VAPOR V AA: TAB. RESULTS v' A MERCURY i ^k TAS. D.L.*i v , ^ OA FORM V T/~ INSTR, SENS. V / TASK III : RAW DATA V KJe. ">fc *!*. v < CYANIDE \ i S TAB. RESULTS \/ v / X —— i. TAB.O.L.S /- " \_ QA FORM, V^ T\/ -_ i INSTR. SENS, y- ^ \/ N V-— X ^H^R RAW DATA ^^^ ^* T>B*4E3ULTS *r*^ TAS, D.L.T^-^ .^^ *~^ ^« ^" QA FORM ~\•^^ ^s^^^^ ^-^" -* INSTR. SENS. "^ ^~ OTHER RAW DATA ***^ •^-. (SPECIFY); .^-^ ^" TAS. RUSULTS -~~--^- ^-,-^. l^- TAB. D.L/s^--'" "-^^ "^ JWr^SflM •^^ - ^^^^ INSTR. SENS. - "^--| COMMENTS: ANALYSIS RESULTS TASK TYPE CONC MATRIX SAMPLE * SOURCEOF H20 COKTAMIM4NTJ ( CONCENT* ATIQH /DETECTION LlMr .6 . AVI ^ 54 A! ik4 Cc R\\ ^s^^^*r^^^^^^^+ c A-l LABORATORY REPORTED FIELD 9LAKK DATA IS COMPARED WITH THE SAMPLE DATA IN A TABULATION FORM WITHIN SAMPLE ANALYTICAL DATA SUMMARY. COMMENTS: (I) RESULT REPORTED BY LABORATORY AND CONFIRMED BY REVIEWER. (2) RESULT INFERRED FROM RAW DATA 10.8 3 BLANK ANALYSIS RESULTS FOR TARGET PRACTIOH TYPE CONC MATRIX SAMPLE * SOURCE OP H20 CONTAMINANTS ( CONCENTRATION / DETECTION LIMIT ) J=*=J%5 /xx/-/5^>o)&^. 47>S. W> (COAT) _CtL^.5^W 5 ^4=2 ' d A f to'ftef' _flta (<,Qju^J**fS«i*&)$.ls"- ?>&Df 15O • All •MH\»&»P KilB- AWV^T^i/fr/Sinto^Aa **5 '/ It 5 1 W ^ f4.'tfi*/tS*tc>_^y S^tl.KA&itf'j'* }&&- 2* L^*^2/^f^&^' o - • ~m LABORATORY REPORTED FIELD SLANK DATA IS COMPARED WITH THE SAMPLE DATA IN A TABULATION FORM WITHIN THE SAMPLE ANALYTICAL DATA SUMMARY. TENTATIVELY IDENTIFIED COMPOUNDS IN BLANKS ARE LISTED ON A SEPARATE FOP COMMENTS: (I) RESULT REPORTED BY LABORATORY AND CONFIRMED BY REVIEWER.______(2) RESULT INFERRED FROM QUANTITAT10N LIST, DIASNOST1CS, CHROMATQGRAM AND/OR SPECTRA. ..C.-:L"?C* I : I /v. ^ i\ a ;- 1 : V L -. S iVr -,i I ,\ C . C A > :. .. N 'J . : i c C j >~_ .. _ _ i /a* /J- -__ _ • "'" - -V7.T.T-LM1S: UC/L --.------.,_..,-. ^ -p?^- ---"V-T-Ji-;-;,.?———— ———— '- - :-. - IM ! I AL CCM 1M iNC u^Ll^ '• ''."MiM-r . 2oC.U _ 2_Cu,C ^L.'J £ Ji.3 I -V^ • i 7 , * * ' """ T i" C N Y .._ ^ . _ o C • L. : 6 C . L . .. c: C . U 2 *£ « U ^.L "' *"l '-. T-^L;' -2uC,u' — 2CC.L iCC.U l.CUi. • >j Ij ^^^"*^vt'rii* r~ 1 1 c * 1 1 ' /* 1 1 i ^ K i ' • ' _L_LVi -/»^U -**UU ^»^U . .1 • •J U i *0w -. "<-iL. • 2.CU 5.CL ,.CU a.Oli -3.-.;. 7. *"*».'* i L f - - -5 C \j C . U " ' 3000. L. 5CcC.U C 2a.3L -,,, o, rv->-ihii_r' iu.U . 1C.U 1C.U A.OU,.Cu 1. r*nn^ L- .-__.__.. 5C.L 50~. 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IOO. 100, IOO. S'9. 99^ INITIAL , CCMINUiNc C^Li,iftAlICf, bCL^Cc : hP^T Vf^iA.v* hLL LlMTi: ^tPCu«V ^NJ TIN -C-i^CJ ^LL Lti-;5 Cu"^"^Ti:f.L'5 vC-1 l 48J065 ";• V.. l*Y i' i /^ • . ^ ^ i - -V . rt IC C.C. .« L ? e. n T: i LINc CiLiet-AU^ V T * I F'l L A T I L M 3 ; f ..; ^j< v t ,\ c .. - " . . 1 _1 ... " C P :. 7 M" .: j t C _> L/li/tS .. . iC> NL.' 7c_4. ;..._. .._ U.sIIS: L./L IMMU. CtLiri.ll) LcMI.MIIW CAi_Ir.i£) 1 * *. ' . ' ' " i N L f1" t.s -<.- . • -: : - ~ c ^ 2 ." -"•- ~c "f i * i 0 i . r '. ^fTT,vCNY - I'-,*. .. ISt). l->2. ^S. P *' ^Nic ' " 54. 5-7. 1Q^. 54, ICDVF *. oi"Lr 437. ------,-j7, -^9. ,c. F s.^ = Tvi_LlLv 23=. 235." 2J5. '. 10C. P A4 r.^M iLw 24; . - =- - - - — - --2"4 3. . 23 C. 10 r. P ?. ^M. '"iLP -. ^iCoOC. . 4CtCC. 417CC. 1CJ. P '. r:u'>nr'IL.w 311. ^— 211* ...314. 1GI. P ^. r"i*LT 2*oi. • • • • .' -"2iil. 2c4. ICi. P 10. rn*>-» L^ .; 339 ...... :._; ..; .; .";"""•.:;_ ._..__.._ 335 . s^ 1- 101 . P 11. T -"IM 7Sc. ..._... j--- .__...._. 7S6. , 7c»J. ^7. " P ^. 1.*=^. __,.,._ - -J?6. BO- 107. 33 icd. F \ T , " ft c v i i u ?• .. d 4 o c . . ;~ ; 64CG. e t s c . l o 4 . f i/i.^MM'-'VM:^ T*Tc";~' ••••--;•• ; ... . ; . ..._:3;4c. - 3p7. 102. r iRM*7T*i_.i . u r yT ... L ^ . N T "v t L 207. -.,--..---.-. . 2C7 . 2ua. ^5* P ] 7 . ° ?T ^ ^ i I U jv S fi 0 C. ^ "•"" " S8CO.""~"c8iC. VC. P l " . ^i - M L r _ _ _,_ __ ^ 5D> 4^ 9 2> 5t>. /&t3'. F 10. ^,utK ^..^.144.. „.___..._„..,._. ..._.144V 14o. lOi. ? ""^ . Sn">TL.v . ^bf'OC*1 '* '"" "~ 465CC. 467CC. 1JC* p *rtoi . r^- ~/1 . trz '•», TT^' 2C.uU_. ; 2CCC. 20iC. 10 J. P •>**. 1M*MU^;^ d4.C* ~ :: -:" " ——— ___.-_.. £46. C5C... ICi. J? 7i. 7T»ir .. ._ ._..___. -^lt. 41S. *tJ3. 103. es t1'. "v*" iCb" ,_::.:: -~.:_- - :;- _ „. ------• CD F______^ _ , _ - ._ _ -. _ ——— _"— :-" --:^Z._ — - —— -- —— —— . (!',<•>> IMTI^Lt'CCxllNL*.NC C^UiifiATICr. iCt^Ct : £F/» » vt ^5irv ... . « r -> ^ f *•»•(- . •- 1 i T v T I ". : ^ i- P [*..«: Y a\r. T ! f, h^- . ? f. : AM fTh.- r f.i. ,w Ff!L \T S Form II Q. C. Uport Ho. XKZTZAL AND CONTINUING CALIBRATION VEEIrtCATtON3 LAB HAKE VgrsJW- Tv\c • CASE NO. SOW HO. "1 t n*TC \-S^-€^ nxits Initial C*llb.*______Continuing Ctlibneion2 H«alsk: Tru« Valu« Found IS. THM V&IUB found ro Found IS. Mschod^ 1. AluilSUX 2. Aacimonr 3. Ar*«n±c 54- sa. qur S2. ^, F 4. Xjirlia • 5. B«rrIIlum | r &. & B - S Form II c- " Q. C. Eeport No. I lu INITIAL AND CONTINUING CALIBRATION VERIFICATIOS3 LAB NAME Vl.^bft'T , Tn c , CASE NO. SOU NO. DATE __\ - 07- "&S UNITS , ' j ? Compound Initial Calib.1 Continuing Calibration14 H*tal«S True Value found I& True Value Found ZR Found a !JMathod- ' 1. Alumimia i 2. Antinonr 3 . Arsenic 5H- SI H sa. 'Itr. P 4. B*riuB S. Berjllina i t * C^QS^UA 7. Calcium 1 • 8. ChroaiuQ 9. Cobalt i 10. Cop?*r 11. Iron I : 12. Lead 23. 2S,.. |CO. 26. F • /^ 13 . Magnvaium . 1 4. M4n£«no*« 15. Mercury • 16. HidMl 17 . Potasiiua • • 18. S«l»niua ^. ^D. l^p 1 19, Silver | 20. Sodium ! 21. Thallium 50.4 5£. <*? 52. /cS> /=- i 22. Tin__ • 23. Vanadium , 24. Zinc ; Other: i . i Cyanide 1 i 1 Initial Calibration Sourea _ __ 2 Continuing Calibratioa Source € P,A 3 Control 'Limits: M«rcury and Tin 80-120; All Other Compounds 90-110 4 Indicat* Analytical" Sietfaod Us«d: ? - ICP/Flam* AA; F - rumace B - 3 fiR100366 Form II Q. C. Eeport No. INITIAL ANB CONTINUING CALISSAIION VERIFICATION3 LA3 HAKE j^.rsfl/- s T>>f . CASE NO. SOW NO. DATE ) -2-2-g^ ______' UNITS Compound, ____lai tlal_Calib._*______Continuing Calibration2 lietais: True Value Found a True Value Found ni found IR Method4' ' 1. Aluminum 2. Antimony 3. Arsenic S4. »=,S. % 52. ^t- F 4. Barius S. Beryllium 6. Cadmium 7. Calcium • S. Chromium 9. Cobalt ' i 10. Casper 11. Iroa_ _ 12. Lead -95. 4s. /CO. -1C. ^g. fo7, ^, !<*? F 13. HaxBecium . 14. Maairaaeee 15 . Mercury • 16. Hiefcel 17. Foeaszinm 18. Selenium If. Silver 20. Sodium i 21. Thallium 50.^ S"0, ^ *5&. 1^ F ( 22. Tin • 23. Vanadium , 2 4. Zinc i Other: j . 1 Cyanide i 1 1 Initial Calibration Source____ 2 Continuing Calibration Source 3 Control Limits: Xercury and Tin 80-120; All Other Compounds 90-110 4 Indicate Analytical fcethod Used: P - ICP/Flame AA; F - Furnace B - 8 form II G? Q. C. Report No. | "?S INITIAL AND CONTINUING CALIBRATION VERIFICATION3 us SAKE U?.r-sAr-. ^L»\s. CASE NO. SOW NO. ) l Compound Initija Calib,1 Cent.inuinjr C^11 bi'ation2 Hetalsk: True Value found ZR True Value Found ZR Found a Method" ' 1. Aluminum ! 2. Antimony 3. Arsenic ^4 su. lt>7. 54- S~7 lc^, S$. fu7 P 4. Barium f 1 3. Beryllium 1 i ' 6. Cadmium r 7. Calcium • 8. Chromium 9. Cobalt - j 1 10. Copper 11. Iron 12. Lead 4o. 4£r. io3. 46. - 4#. ttff 3ut /02. £ 13. Magnesium 1 4.. Manganese 15 . Mercury • 16. Nickel 17 . Potassium • 13. Selenium 19. Silver 20. Sodium i 21. Thallium *=>D-4 so. Ti 1 i 22. Tin • 23. Vanadium j 24. Zinc i i Other: l i Cyanide - i *• Initial Calibration Source 2 Continuing Calibration Source^ 3 Control Limits: Mercury and Tia 30-120; All Other Compounds 90-110 4 Indicate Analytical Method Used: P - ICP/Flame AA; F - Furnace B - 8 ;-& Fora II Q. C. Report No. INITIAL AND CONTINUING CALIBRATION VERIFICATION3 LAB SAME V|g_rt>Ar- ] XA* . CASE NO. SOW NO. vaz-e^_____ OSITS 'Camggund ____Initial ._e*jHb. *______Continuing Calibration2 HccalsS True Value Found a True Value Found ZR Found ZR Method" ' 1. Aluminum 2. Antimony 3. Arsenic 54. •51. 94 W % i 4. Barium 1 5. Beryllium i " t. Cadmium 7. Calcium i S. Chromium f. .Cobalt * • 10. Copper U. Iron ( 12. Lead 45. ?5>. fit 47. v^. P 12. Magnesium i 14, Kanyaneee 15. ^ercurj^ 16. Sickel 17. Potassium • • 18. Selenium If. Silver i 20. Sodium i i 21. Thallium i 22. Tin i 23. Vanadium , 24. Ziac j Other: ! i Cyanide 1 : 1 Initial Calibration Source 2 Continuing Calibration Source 3 Control uiaits: Mercury and Tin 80-120; All Other Compounds 90-110 4 Indicate Analytical Method Used: P - ICP/Flame AA; F - Furnace B - rC.:<.» .;.Z.V___ .. ._...... ___ .______--C_. *rrC-T: I7C \ it.!- if. Tri.Fp-'cNCfc.CKcl* ^ LL UMTjU) . UI7UL r.;.iL -^Z X -I j J C. * i-jr v'. I *. L11 .L t, J £ fi « c C /: •* L r J .- i- *.-.** t2J ^9iCCn.' ' •;?. A,. ulCJ. • __..lCCO. lot* iC-C* *. '«-H.K V39.- .-..-5.- 1CCC.' " "SoO*' Iu2. <«i. tt. "* • l~^t.riL-*p - l«i (j CC « 1S7 C • ' JCCOCC. 52t.CCC. 1J3-. 51.CC,. 1LC. . l*' 1 'J i 1 'i1 '".- * £. m• '-'- • - 5 C C - 533. - i it) - «li. >>C. if> . _A70. 3. 5cG. . 519. 110. T. T-SIM ^S^CCO. ^"-^TTC." "5"COCCC. ^t7iCOC* • ••*&- -Ht/iCCC. • 1'. L=*^------—-—— -—. .— - —— -. - - - _ j^.M.r.M-s j HP ^fc/.CQO .. _ _ tt_5_C,.: 5'OCCt.C* ^t iCCO. ^4. ^5*:CCC- c 7 *i . 4 .'' ' ' 1C L C • 4 ^ 7 „ 1 U o . -7^0. S C . ^' " t\ IL rt —— >^_ — . _ -». TTX1 ' " OC«, . - 17V ":-r- ; 10CC. .il^u. Ii9. 77-. -" g4 —----:—:--"--"——I"I"""—^7™—"^ 4t'5. 3.- - 1CCC. iC-'iG. 1.J7. -j^ 1. . r i l "T *M r;. S..L C...V.N. =;_.i. Li) T^UL VAi.Lt L r" I .vj/r p-^fuL^ L hi: Cft S-^.^PLt. APPENDIX G AJU 00372 V f r< r. grwronmtnMl Protection Agency. CLPSampJe Management Qtfict, Sample Number P, 0, Box 818. Afffunana. Virprnra 22313 703/557-2490 Organic* Analysis Data Sheet (Page 1) Laboratory Name: Gu££ South Research Institute Case No; . 3& 0^ Lab Sample /D No; r4 lp O /______QC Report No; Samnfa Mam* i.A^M-TC^ ^ .-^—r-J_____xi Contract No; 66-01- Data Re/ease Authorized By: ^^-^FX^^ ^^ Date Sample Received; VofatiJftjCompoundc Concentration: (Low J Medium (Circle One) Date An •l««rf."1/^/> /?*/ f ' C0nf?/pif Pftao*" „ ' ' ^ nH Iff ' f *^ Percent Unistura- ___A^^ Percent ^pjsture (Decanted) A/A •—•^ CAS < CAS ^ug/ljorug/Kg ""TCircte Ona) 74-87-3 CrUoromemane /O i»- 79-34-5 1. 1.2. 2-Tetraeriloreemane y u^ 74.S3-9 Bromomeman* /o y- 78-87-5 1, 2-DtcNoroprooane 5* iw 75-01-4 Vinyl Cnloride ;n it 10061-02-6 Trans-1. 3-0>cnioroorooene 5~ to 75-OO-3 Chlorofltnane /O *^ 79-01-6 Tnehforoethene 5"~ iu 7S-09-2 Manftvf»n« Cntoride -^.^B -^3-TT^SD 124-48-1 0)6romoen(oromerh»nc 5~ t-C 67-64-1 Acetone '£J FC 79-00-5 1. 1 2-TncrMoroeirtane 5* i*- 7S-1S-0 Carbon Otsulfide ^" /<_ 71 -43-2 Benzene Far importing ratuft* TO EPA. in* feJtownng wutty gu*lif Valu* a D» CC 'MS 'ul in tn* lin*i *RfjiCT U lM««M«mMuntfH..*«lVMArMMl«li ' K*eerr m* minrmum d«t*crte" unit far m« Mmiw rtv t«t wwir unwnt »i «*»" •» * umD'v ft U- BJ«n> contam Otfw 0»n*f Kweifie fiiflj and footnote* •«»» ft* rwuirwo te OSISfKAf. Environmental Protection Agency, CLP Sample Management OW'Ce. Sample Number P. O. Boxflia. Alexandria. Virginia 22313 703/557-2490 Organics Analysis Data Sheet (Page 2) SermveJatile Compounds Concentration: f.Low/ Medium (Circlhfe One) Date Analv 7frt- ft-nT- | £y Conc/Dil Fartnr" ^ 0 O ' ^ ^ ——* CAS (^ ug/jjarug/Kg CAS ( ug/Oorug/Kg Number *~^circl* On»j Number ^*TCireIe One» 62-75-9 N-Nitrosodirnetnvlarnine to io 83-32-9 Acenapnthene /O -^ 108-95-2 Phenol /O (^ 51-28-5 2. 4-Dmitropnenol -S"O **- 62-53-3 Aniline tn L<- 100-02-7 4-Nitroohenol £TO U_ 111-44-4 bis(-2-ChioroethvltEiher fO tu- 132-64-9 Oibenzofuran /O t^ 95-57-8 2-ChloroDhenol fO i*- 121-14-2 2. 4-Dinitrotoluene (0 !^ 541-73-1 1. 3-Dtchlorooenzene 1C W_ 606-20-2 2. 6-Dinitrotoluene /O U. 106-46-7 1 . 4-Dichlorobenzene /C iw 84-66-2 Diethyiohthatate /O V~ 100-51-6 Benzvl Alcohol /n LW 7005-72-3 4.CntoroDhenvl-oheny|ether /C i.w 95-50-1 1. 2-Dichlorobenzene ;o tc 86-73-7 Fluorene /O M_ 95-48-7 2-Methvlpnenol /C tc 100-01-6 4-Nitroanitme CD-61- 3963S-32-9 bis(2-chloroisopropyl)Eiher /O U- 534-52-1 4. 6-Dinnro-2-M«thylpnenol S*0 U. 106-44-5 4-Metnvionenol ;n i — 86-3O-6 N-Nitrosodtphenylamine (11 /r» t^ 621-64-7 N-Nitroso-Di-n-Propylamme ;0 M- 101-55-3 4-BromoDhenyl-phenytemer ^C /JL. 67-72-1 Hexachloroema ne /D tC 118-74-1 Hexachlorobenzene ;c LC. 98-95-3 Nitrobenzene 87-86-5 Pentachlorophenoi ,3-Dc C1 - fD lw "^Tj ty^- 78-59-1 Isophorone /O fcL 85-01-8 Phenanthrene /C £C 88-75-5 2-Nitroonenoi r n t^ 120-12-7 Anthracene ^O t(_ 105-67-9 2. 4-OimethylDnenol 84-74-2 Oi-n-Butylphthalate / D (L /i C,-. .LL 65-85-0 Benzoic Acid TO w- 206-44-0 F luoranrhene /^\ J^ * L,' t-C-^- 111-91-1 bis(- 2-Ch loroethoxyjMethane 10 ^ 92-87-5 Bcnzidme .Tr i^- 120-83-2 2. 4-Dicnloropnenol /O tw 129-00-0 Pvrene / O T ;.f i ^ 120-82-1 1 . 2, A-Tnchlorobenzene IO U 85-68-7 Butvlbenzyiphthaiate ^C cc 91-20-3 Naphthalene 10 K-, 91-94-1 3, 3'-Oichtoroaenziame oic tv. CO 106-47-8 4-Chforoaniitne /O iv 56-55-3 Benzoo (AnThracene /o t1- CD 87-68-3 Hexachloroouiaaiene /Ot.i 117-81-7 bis(2-Ethvihexvi)Phmaiate /o <-u S9-50-7 4-Chloro-3-Metrtyiphenoi !O (,- 218-01-9 Chrvsene /U tC- 91-57-6 2-Methytnaphthaiene ;o t\- 1 1 7-84-0 Di-n-Octyl Phthalate ;n tv. or 77-47-4 Hexacniorocvclopemaaiene tn tc 205-99-2 BenzcKDiFluoranthene ;r^ tc 88-06-2 2. 4. 6-Tnchloroonenot iO n. 207-08-9 Benzo<"i(tFiuoranthene /n u 95-95-4 2, 4. 5-Trichloroohenoi ~> O r L 50-32-8 Benzo Organrcs Analysis Data Sheet f (Page 3) L^Jt,- 0^ Pesticide/PCBs Concentration: (LOW /Medium, {Circle One) Date Extracted/Prepared: / Date Analyzed: _JJ Conc/Dil Factor: ^ & CAS ,—• Lug/lp/ug/Kg Number . . ——TCircl* One) 319-84-6 Aipna-SHC Q.C«? tX- 3T9-8S-7 Beta-BHC C CV" L*~- 319-85-8 Delta -BHC C.C^ t<_ 58-89-9 Gamma-BMC (Lmoane) D. C,*T t\^- " 76-44-8 Heotacnior C.tT ^-C 309-00-2 Aldnn r.c SO-29-3 4. 4%DOT C ftJ> * JL. 72«J3-5 Methoxvchlor r-5C U. 53494-7Q-5 Endrrn Ketone ,- •. r c tA. 57-74-9 Chlordane C.*5-o u 8001-35-2 Toxaonene }. Q t-v 12674.11-2 Arocior-1016 .o.ro £A. 11104-28-2 Arocfor-1221 r. Vj s Volume of extract injected (ul) V = Volume of water attracted (ml) W, - Weight of sample extracted (a) S V. = Volume of total extract (ul) V, A-J Environmental Protection Agency. CLPSamole Management Office. Sample Number P.Q.BoxSia. Alexandria. Virginia 22313 703/557-2490 , --- - - (\^ -^o? ^y Organics Anjalysis Data Sheet (Page 1} Laboratory N *m«- Gulf South Research Tnstitul.e Case No: 30 0^ . DMn- f-fDo-^ •:.- QC Report Nc f H**^' Sample Matr »• I A_-^CTc_ * Contract No: 68-01- (sfl^l Data Release Aufhofty»d Ry- <^<^ f^y^ f S i* :~$~te*ir • Rw»iu*rt- I^JH /ar Date Sample i > Volatilfl-i=om sounds Concentration: [LowJMtdium (Circ:le One) V— *• Date £xttacted/Prepared: * h m Date Ana v*"ri> '^A Conc/Dt Percent PJnictur*- /V W X/A Percent f^pjsu^e (Decanted) — ^ CAS ug/Lprug/Kg CAS . C ug^orug/Kg Numb* i1 :==:57Cfrc*« One I Numb*r ^^"^Circle One! 74-87-3 Chloromernane ;c tw 79-34-5 1. 1. 2. 2-TerracnioroeTnane _5~ ti^ 74-83-9 Bromometfiane ir-. 0_ 78-S7-5 1. 2-Dtcnioroprooane 5" i^- 75-01 -4 Vinyl Chloride roLt 10061-02-6 Trans-1. 3-Dicnioroorooene T »-O 75-00-3 Chloroernane /(_? i^ 79-01-6 Tricnioroetncne «5^T . — g~ hi»^ 75-09-2 MethylBne Chloride ;Q B -*=• ;r • 124-48-1 D ibrom ocn (orometha ne S~ fc<- 67-64-1 Acetone ro /u 79-00-S 1.1. 2-Trtchloroetnane 5" tx_ 75-15-0 Carbon Disufftde 5~ L^ 71-43-2 Benzene r «, 75-35-4 1. 1 -Drchlorofltnene V LC 10061-01-5 crs-1. 3-Dich(oroorooene >r *>- 75-34-3 1, l-Dichloroetnane S" tw 110-75-8 2-Chloro«invfvinvlether /c c<- 156-60-5 Trans-1, 2-Dichtoroerhene T Lv^ 75-25-2 Bromoform ^r *\ 67-66-3 Chloroform C i^<- 591-78-6 2-Hcxanone /o t*_ 107-06-2 1. 2-Dichloro«tnane c- u. 108-tO-l 4-Metnyl-2'Pentanone /c u. 78-93-3 2-Butanone '-^, ^/,c., c-. j^ 127-18-4 Tetrachioroetnene 5* u 71-55-6 1,1. 1-Trrchloroetnane S" iC 108-88-3 Toluene r ix... 56-23-5 Caroon Tetracntonde V U. 108-90-7 Chlorobenzcne JT ~Ax 103-05-4 Vmy[ Acetate /o **- 10O-41-4 Ethytbenzene S~ ^ 75-27-4 BromoOichlorometnane 5* tx^ 100-42-5 Styrene 5" ^ Total Xvt*n« -<~ 'A , Oau R«ooning Qualifiers For F*oorring mmti to £PA. m* following r»iuU« au*l ilwd oamaowno* ww» • 1 1 mootM ' gnvironmentslProteciion Agency, CLP Sample Management Office. Sample Number P 0 SoxSlS. Alexanaru. Virginia 22313 703/557-2490 Organics Analysis Data Sheet (Page 2) Sermv0Jajile Compounds Concentration:^^---/ Low^/ Mediu. - /m . (Circli ~e rOne) Date Extra rted /Prepared • ,'^/ -ST*" / s T Date Analv*«* i$- n^ Av ' Cone/Oil Factor- .. _^\r 1 \U ?*-}t ~—~"*>^ __ CAS (^ ug/torug/Kg CAS ^ug/Lorug/Kg Number 1 — TCircfe One) Number ^---fCirclfl One) 62-75-9 N-Nurosodtmetnvfamine fo i*~ 83-32-9 Acenaonthene /O **- 108-95-2 Phenol /O (^ 51-28-5 2. 4-Dimtroohenoi ..5*O.^ 62-53-3 Aniline in L<~ 100-02-7 4-Nitroonenoi S"o*iL 1 1 1 .44-4 bis<-2-ChIoroemvnEmer /n L^ 132-64-9 Dibcnzofuran /O L^ 95-57-8 2 -Chloroonenoi tc i>~ 121-14-2 2. 4-Oinr:rotoluene to t^ 541.73-1 1 3-Dicfilorooenzene 1C M_ 606-20-2 2. 6-OmitrotOluene /Q i^ M DietnylDhthalate » 106-46-7 1 '4-DicnioroDenzene /c i*~ 84-66-2 1C V*-J 100-51-6 Benjvl Alcohol ;p tu. 7005-72-3 4-ChtorODnenvi-onenvietner /C (.*- 93-50-1 1 2-Dicnlorobenzene in ti- S6-73-7 Fluorene /e uu 9S-4S-7 2-Merhvtohenol tc t-c 100-01-6 4-Nirroanrlme CD ^*- 3963S-32-9 b(s[2-chloroisooroDvii£ther 10 U- 534-52-1 4. 6-Omrtro-2-Metnyloheno( .^'O t-A- 106-44-5 i-Merhyfonenor in j ^. 86-30-6 N-NiirosooionenvJamine ( 1 J /n &~ 621-64-7 N-Nitroso-Di-n-ProfJviamme /O W_ 101-55-3 4-BromoDhenyf-ohenvietner IQ /*- 67-72-1 Hexachioroetnane /O tu 118-74-1 Hexacntorobenzene /C f.<- 98-95-3 Nitrobenzene /n fw 87-86-5 Pentachioroonenoi *3£)3~ •^G — *^- 78-59-1 Isoonorone /O M. 85-01 -8 Phenanthrene /C Environmental Protection Agencv. CLPSamo'e Management O^'CB. Sample Number P. O. Box 8ia. Alexandria, Virgmta 22313 703/557-2490 Organics Analysis Data Sheet (Page 3) Pesticide/PCBs ' Concentration: ( Low /Mediurn (Circle One) ' / -^ /. / p'// Date Extracted/Prepared: —/ ^ / u f AT"'____ Date Analyzed: / . i -. Conc/Dil Factor: ___ CAS j^ ug/Mpf ug / Kg Number TETircle One) 319-84-6 Aiona-BHC O.CS- lA- 319-85-7 8eta-8HC r cr LI- 319-86-8 Deita-BHC. c^j<; ix 58-89-9 =- = Gamma-BHC (lincanei c-.c^r 6\— 76-4A-8 Heotacnior C-cC /x_ 309-00-2 - Aldrm r.cft- Li 1024-57-3 Heatacnior Eooxtae C-CS" U. 959-98-8 Endosuifan 1 r.C..*T L-^ 60-57-1 Dieidrtn O, /o U- 72-55-9 4. 4--DDE r,. jo u^ 72-20-8 Endnn O.fO /;x_ 33213-65-9 Endosuifan ll c-tc; u. 72-54-8 . 4. 4--ODD C* tu /JU 7421-93-4 Endnn Aldehyde p. f u *^_, 1031-07-8 Endosuffan Sulfate" " r- (C /.A 50-29-3 4. 4'-DDT C fO f.A. 72-43-5 Methoxvchlor r . 5t- 6C 53494-70-5 Endnn Ketone ,". f C £x_ 57-74-9 Chiordane C.*s-o u 8001-35-2 Toxaonene i. O t<^ 12674-11-2 Aroclor'1016 ^ VD iA. 11104-28-2 Aroclor-1221 r.^O M" 11141-16-5 Aroctor-1232 O-^o IA_ 53469-21-9 Aroclor-1242 f . S O L^— 12672-29-6 Aroclor-1248 C-SO L^ 11097-69-1 Arocior-1254 ! • O j{ 11096-32-5 Aroclor-1250 - t-O *^ V- = Volume of extract injected {ul} V = Volume of water extracted (ml) W = Weight of sample extracted (g) V = Volume of total extract (uU V Se ... iw w ————————____—_ wor Ws /W / \______Vt / Uf—————————.^—— , U ^ ^ — V( ., (i^F^^'.f =——— ——— — _=——— — — — ^^ /!--.--l 1. ' Environment*! Protection Agency. CLPSjmpleManigement Office. Sampja Number P.O. Box SI I. AfexjnCna. Virginia 22313 703/557-2490 Q^~^~^(j.\ Organics Analysis Data She et 11 (Paget) 2 Laboratory N im«- £ulf South Research Institute Cas^ No- C 603 Lab Sample iON*- H CH D QC Report Nc f f^^t Sample Ma ir «- f AJ^.tc'1^ Contract No: 68-01- (jflS^il Data Release A,,fhnrr,«HfV ^^ g^/^.fr &,S'Date Sample R.^iu^. /t /«//§'/ ' VolatjlflJ?>m pound* Concentration: (Low Merdium (Ci;lre One) V— - Date Ext acted/Prepared:^. f. , ——————————— Date An; IZ/9- h*/ V- - / Q ' ' ^T &Q Conc/Di PflCTf»r' „«_,!. «^i pW -5,7 / Psrcent f^ftieti»r»- .A^^J Percent F^pjsture (Decanted) A/ A -— > CAS < ug/£pT tig/Kg CAS (ug/^orug/Kg Number :"-i-fwrel« On«) Numbwr Vi""^CifCle On«J 74-87-3 CTtloromerrianc ;o t*- 79-34-S 1 T. 2. 2-Tetrachloroethane ^- fcU 74-83-9 Bromomerhane /n (JL 78-87-5 1. 2'Dtchloroorooane 5* to 7S-O1-4 Vinyl Chloride Ar^ 0. 10061-02-6 Trans-1. 3-Dichioroorooene r «^o 75-00-3 Chloroetnane /'^ * w- 79-01-6 J Tnenioroerhene 71-S5-6 J. 1, 1-7ncnloro«trTine S~ tu 103-88-3 Toluene S^tT^ " J 4X_ 56-23-5 Caroon Terracnionfi* V u. 108-90-7 Chlorobenzene £" *u 103-05-4 Vinyl Acetate ;O u- 100-41-4 Ethvlbenzene $- tt^ 75-27-4 BromoCich/orometnane mwJ 0* GC 'MS Smgi* •nract U B«wrt m« mmtmtfm a«l»a>on nmn lot tft* wm»i* -«tn tft«U(*fl, tOU}MMd«nn«e««unreane*niriir0n' • Tn«< flag K uMM wn«n trw trwiyt* n fsund m in* cn* •***'( M • wmoi* tt maieaiMoeuiawerooaDi* w""« eonjam.nat.on ana w»rn* tn* Otfwr Orn*r uweihc flagi and focinoiw ma* 0* f*du"»d to 10 tn* Of it w*wr* * 1 I rMDentt n tuumad Environmental Protection Agency. CLP Sample Management Office. Sample Number P. 0. Box 818. Alexandria, Virginia 22313 703/557-2490 Organics Analysis Data Sheet (Page 2} Semiveia^ile Compounds Concentration: fx*——* Low.*/ Mediuim (Circli _ ef One) Date Anal>«,- 12, /(I l$f ' ' Conc/Dil Fartnr- *T 0 O v..- CAS C ug/tffrug/Kg CAS (^ug/^orug/Kg Number 1 TCirctaOna) Number ^--"rCircte One) 62-75-9 N-Nitroso p£Sticid e / P C B s Concentration: (LOW /Medium (Circje One} Date Extracted/Prepared: ; ^/^ / DatP. e Analyzed. , :. \ s.i -y*t t \ tf t Conc/Dil Factor: /OQ Aiona-BHC O.C^ F^— Seta-BHC c-cs il. 58-89-9 Gamma-BHC tLinaanet O-CS" ^-^ 76-44.-S Heotacnior Heotacnior Esoxioe C-C'S' U. 959-98-8 Enaosuifan l ^.GT L^ Dieiorm Qtf^> U. 72-55-9 4. 4--QDE i - Volume of extract injected (ul) s = Volume of water extracted (ml) s = Wetght of sample extracted (g) t = Volume of total extract (ul) vs ——^,\r ^_____ Orws Envtronmsntsl Proteciwn Ao«nev. CLPSample Management Office, Sample Number Alexandra. Viroimt 22313 703 /S 57 -2490 Organics Analysis Data She 8t (Page!) Laboratory N Ftm.fr Gulf South Research Institute Case NO- „ 603 Lab Sample 1nun- H ^'3 QC^ Report Nc [ £T^- ». f \Arcf~ Sample Matr ^ Cntraco t No: 68-01- (jflS^ Data Release Atithor'?f»fl By" £fc£ &?,., /^ ^"-^^•^^ Date Sample R*r*iw*H- /^'/'/j/Sr, Volatila-J^ompounds Concentration; (Low um fCirc:le One) V--^ Date Ext acted/Prepareri- f< r Date An* ly«rf- // " h l¥n Tetrachlonde S" U. 108-9O-7 Chlorobenzene £~ H^ 108-05-4 Vtnvt Acetate / O U. 100-41-4 Ethylbenrene €~ i^ 75-27-4 Bromodichforom etnane For nnoning rvtuti to E^A. fft* followtng ntults ou«l<''«r« *'• tiMO Addrt«nil ft»gs or ftetnotis •oUrninQ rt^ulis «r« *neouri9 dvtinnion of »§eti N«^ must tw •Kolwn t* nw '«uft •» » «'o» grwmr m«o w «auai to m« C Th.» fug anlifmM ov GC 'MS , ^ Showtd M conl tft« U (• 0 . 1 0Ut M»«tf on n*c««MFV eone*ntr»lip_n '. — * Th" fl-* '* UMia <*'»•« ">• •«•!«« « *ound •luttort aeiioni (Th« n not nvcMHriiy trw mnrument •• •**" *» • Mmgi* ft maejtM pocxi&w .1 Th* *o«rwt» ^ou« rwd U- **•»>* eenti «•• «n.tv»d for Out not *iected Tfw *«>coof «*r« n«fno«f >• m» mimmufn •nfiruew d«t»c:*oo limn (or riv Mfin« in» r«iutti H u**0 m*v must M 'u»v Mitmmd value Thw ft*e it tetcfibM «na auen aMcp0i«Mi lumm.* mrf, f| Q 3 & wn*r« • 1 T rwonM rt •Mum«d Mil 1 V *» ** Environmental Protection Agency. CLP Sample Management Office. Sample Number P. 0 8os SIS. Alexandria. Virgin* 22313 703/557-2490 Organics Analysis Data Sheet (Page 2) Sermve4o,tj)0 Compounds Concentration: [^—- low.^ / Mediu/m (Circlj .e. Oner ) Date Anal1,«H- 12/ISr/Sf' Conc/Dil Fartnrr ^ O C) """^ S— — ^ CAS (^ ug/I^Tug/Kg CAS (ug/J^rug/Kg Number ""^Circle On») Number "^"'fCircfe On«) 62-75-9 N-Nitrosodimeinvlamme /"o t*— 83-32-9 Acenaonthene /O *- 103-95-2 Phenol tO re 51-28-5 2, 4-Omitrophenol 50 **- 62-S3-3 Aniline /O l<- 100-02-7 4-Nitroohenol S"O tt- 1 1 1 .44-4 btsf-2-ChloroethvnEther iO 60 132-64-9 Dibenrofuran fo t^ 95-57-8 2-ChioroDhenot /C i^ 121-14-2 2. 4-Ointtroioluene fO L^ 541-73-1 1 . 3-Otch!orooenz8ne (C M— 606-20-2 2. 6-Dinitrotoluene /O t^M 106-46-7 1 4-Dictiforooenzene /C i^_ 84-66-2 Diethylphthatate 1C i^ 100-51-© 9*nn^ Alcohol /r> LW 7005-72-3 4-ChloroDhenyl-ohenviemer f£. L^ 95-50-1 1 , 2-Dichlorofaenzene in to- 86-73-7 Fluorene /© M_ 95-48-7 2-Methvlphenol fC M- 100-01-6 4-Nitroanihne CD t>~ 39638-32-9 btj£(2 -chloroisopropvUEiher /O U- 534-52 -1 4. 6-Dinitro-2-Methylphenol •SO (A. 106-44-5 4-MamvlDhenol ;o i •_ 86-30-6 N-Nitrosodiphenvlamine (1 ) ;r> b- €21-64-7 N-Nitroso-Di-n-Prooviamme ;0 W_ 101-55-3 4-8romophenyl-ohenyterher IO /*. 67-72-1 Hexachioroetnane /O W- 118-74-1 Hexachlorobenzene ;c /.*_ 9S-95-3 Nitrobenzene fO l^ 87-86-5 Pentachlorophenoi t^2C 78-59-1 JsQohorone /O «_ 85-01 -S Phenanthrene /C vL 88- 75 -5 2-Niiroonenol (0 M^ 120-12-7 Anthracene /O u_ 105-67-9 2. 4-Dimethyionenol > 0 (.L 84-74-2 Di-n-Butylphthalate /C 0. 65- 85-0 Senzoic Acid frO t-t- 206-44.-0 Fluoranthene /O w-^ 111.91-1 bisl- 2 -ChloroethoxvlM ethane )O IA_ 92-87-5 Senzidtne .•Tr ;>«- 120-83-2 2. 4-Oicn!orooheno( /o v- 129-00-0 Pyren* 'O /,^ 120-32-1 1, 2. 4-Tnchlorobenrene /G U 85-68-7 Butylbenzylpntnatate ^0 LC 91-20-3 Napninalene rO tc. 91-94-1 3. 3"-Dicnlorobenzidinc ' o^C rl_ 106-47-8 4-Chloroanilrne /O ik. 56-55-3 BenzotajAnihracene /O t>- 87-68-3 Hexacniorobutadiene /Cu 117-81-7 bis(2-6thvlnexvuPhtnaiate /O tv-. 59-50-7 4-Ch!oro-3-Metnytphenol ip {,- 218-O1-9 Chrvsene /u w^ 91-S7-6 2 -MethytnaDhtna lene JO EA_^ 117-84-0 Di-n-Octyl Phthalate /O 6t_ 77-47-4 Hexacniorocycfopentadtene (0 /,<_ 205-99-2 SenrotbjFluorantnene f r1 (,<_ 88-O6-2 2. 4. 6-TnchiOf oohenoi 207-O8-9 Benzo 12574-11-2 Aroclor-1016 /-y V*O (A- 11104-28-2 Aroclor.1221 r.<0 W 11141-16-5 Aroclor-1232 ti.^u t^ 53469-21-9 Aroclor-1242 r. Vj = Volume of extract injected (ul) Vs = Volume of water extracted (mf) W£ •= Weight of sample extracted {o) V. = Volume of total extract tut) v'5s I6D' ^ ~.______U _ or_orWws AJ'^H ' ^_____ vV /Q,dpU • X)-S A R i 0 0181*"" Environm»ftt4tProt«ciian Agency. fXPS*mple Management Office. Sample Number P.O.Box 818, Al«xinona. Virgimt 22313 703/557-2490 Organics Analysts Data Sheet (Pagel) Laboratory Name: Giilf South Research Inscicute Case No: ^5Cf 03 Lab Sample ID No; ffj 3.1 t______QC Report No: Sample Matrix: J^±kC£l______—-. . Contract No: 66-01- Data Release Authorized 3y: <£^g *** / .*&*/&w* Date Sample Received: Compounds Concentration: .(Low /Medium (Circle One) Date Ana ly»d.- /7-/?/$^ l v-- / fS / T Vv Conc/Di Parfni- / - V-» pH J ' TjJ „,. ,. Percent ^L^nieftir*- , A/ W Percent ^^ojsture (Decanted) /uA CAS (^ og/Jprug/Kg CAS (^ru9/K9 Numb*r ^ Numb«r x°l""^Circle On«| 74-S7-3 Chiorometnane ;o '.-- 79-34-5 1, 1.2, 2-Tetrachioroemine 74-83-9 Sromomernane /r> y- 78-87-5 1 . 2*Dichioroprooane —— f-j4^* i"^~ 75-01 -4 Vinyl Chloride 10061-02-6 Trans-1. 3-D'Chiorooropene —— F-ST1 / f.3 U- * \ 75-00-3 Chioroatnane /rj t^ 79-01-6 Tncfiioroerhene \~ , ^ 75-09-2 Memviene Chloride f ^ 13 -< — TT"^TS 124-48-1 Dibromocftioromethan* 67-64-1 Acetone ffj iC 79-00-5 1.1, 2-Trichiproethane s~ tf- 75-15-0 Carbon DisuUide ^T JL 71-43-2 Benzene r tc 75*35-4 1, 1-DichIoroetnene V i-L 10O6l-Ot-5 cis-1. 3-OiChforooropene /r **• 75-34-3 1. 1 -Dichloroetnsne S" c^ 110-75-8 2 -ChioroeihvJvinvietner fG "- 156-60-5 Tranj-1. 2-Dichioro«ihene *r tX' 75-25-2 Sromoform ^r f\ 67-66-3 Chloroform C L.C 591-78-6 2-Hexanene /O £<- 107-06-2 1, 2-Oichioroethana <~ n_ 108-10-1 4-Memvl*2'Pentanone /C U_ 78-93-3 2-BLrtanone ^ f ^ i LL. •SD 127-18-4 Tetrachioroethene r u 71-55-6 1,7. 1-Triehioroetnane 5~ i^. 108-88-3 Toluene r iX_ 56-23-5 Carbon Tetracnionot S~ U. 108-90-7 Chloro&enrene r* *o 108-05-4 Vmvi Acetate ;o w 1 00-41 -4 Ethvibenzene ^~ tCx 75-27-4 BromoaicftioromeTnjn* VaAiat If tftv f**uft is a WUM gr*iT*' tft*rt or •qua) to m« C Thia flag aooii*> to pctiiciiw Dar»"*«i»fi nm*'* ti« 4*I*ClfOn limit, [auon tn* v«iw* >e«niific«iion nat D*«n eon*irm«0 &v GC 'MS Stngi* mould M cantirmoa By GC 'MS «mfwmu«n oviacuon itmit lor in« Mine** wim IOU»o*t«d«nn*e««««fveonc«Mfaiion' • Thl» "•« n ui«d w««*i in* an»M» n found m tn» Biaru t nee r»e«»fiiv !«• tnnrum*m •• *•" •* * MAOI« n ino^at« pott-oi* 'tKW*Bi* U- ' Win* con«m.*,«,,on »ntt w»«w tf>« 9»t» u*«r 10 Uta Orn*f «o*e>fie flag* and faotnotv* "W M r^u r« a t 1 rtapona* •r tunvn m* mvu ipactnl Environmental Protection Agency. CLP Sample Management OHice. Sample Number P, 0. Box 818, Alexandria. Virginia 22313 703/557-2490 Organics Analysis Data Sheet (Page 2} Sermve*atile Compounds Concentration: ( Low/ Medium (Circle One) Date Analy~H- ^Ml Conc/Dil F*«nr.- ' '50 a V-.- -- — --•----£------)-- s*— — ^ CAS V^us^flTug/Kg CAS (, ug/lorug/Kg Number TCircle One) Number **^TCircte One 62-75-9 N-Nitrosodimetnylamine to £<~ 83-32-9 Acenaomnene - /O ^- 108-95-2 Phenol /O re. 51-28-5 2. 4-Dmitrophenot So t^- 62-53-3 Anrlme /n LC. 100-02-7 4-Nttrophenof £T(J iC 1 1 1 .44.4 b!S(-2-Chloroethvl)Ether /n to 132-64-9 Dibeniofuran ^O ^ 95-57-8 2-Chlorooheriol /D i^ 121-14-2 2. 4-Ointtroroluene ^0 ^ 541-73-1 1 , 3-Dichlorobenzene 1C M_ 606-20-2 2. 6-Dinttrotoluene /O uL 106-46-7 1 , 4-Dichlorobenzene /C U. 84-66-2 Diethvtphthaiate /O L^ 100-51-6 Benzvt Atcohol in u^ 7005-72-3 4.Chioropnenv(-phenvfether /C. {.w 95-50-1 1 . 2-Drchiorobenzene >r> u_ 86-73-7 Fluprene /e />(_ 95-48-7 2-Methvlphenoi /O u. 100-O1 -6 4-Nitroamhne ct> c«- 39638-32-9 bis(2 -chloroisopropvt (Ether >QLu 534-52-1 4. 6-Dinnro-2-Methvlphenol 5O (.A- 106-44-5 4-Methviohenol /n f_ 36-30-6 N-NitrosodiPhenvtaminedl /r\ t^ 621 -64-7 N-Nitroso-Di-n-ProDvlamme fO W_ 101-55-3 4-Brpmophenvt-phenvlether /C //- 67-72-1 Hexacnioroetnane /n t^- 118-74-1 HexachtoroPenzene /C /,*- S<3 98-95-3 Nitrobenzene FO Ux 87-86-5 Pentachloropheno! £^Q 3" -S© J«a-i 78-59-1 Isoohorone /O ^ 85-01 -8 Phenanthrene /C oC 88-75-5 2-Nitroorienoi in t<. 120-12-7 Anthracene /O cu 105-67-9 2. 4-Dimethviohenot / 0 (L 84-74-2 Oi-n-Butvlohthatate /C CL 65-85-0 Benzoic Acid TO w- 206-44-0 Fluorantnene fO 3 •11™ i' - JO 111-91-1 bis(-2-ChloroethOKv»Mcthane JO iA. 92-87-5 Benzidme cr i^_ 120-83-2 2. 4-Dichloropnenoi /O y- 129-00-0 Pvrene fc T ?s 120-82-1 1. 2. 4-Tnchlorobenzene iu u 85-68-7 Butvibenrvipmnaiate /c a. 91-20-3 Napntnaiene /O t^ 91-94-1 3. 3'-Oicnlorooenzioine -^C i^ 106-47-8 4-Chtoroaniline '( ; ;<. 56-55-3 " 8enzota)Anthracene /C t,1- 87-68-3 Hexacniorobutaoiene /c,.< 117-81-7 ois<2 -Einvthexyi iPhtnaiate rar -/-t—v w S^ 59-50-7 4-Chloro-3-Metnvtphenof tOL- 218-01-9 Chrvsene /u w^ 91-57-6 2-Methvtnaphtnalene /o i*~ 1 1 7-84-0 Di-n-Octvi Phthalate /O 6c OD 77-4.7-4 Hexacnlorocvciooentadiene fO_/.L 205-99-2 BenzcxoiFluorantnene f P (,C CO CO 88-06-2 * ' 2. 4. 6-Tnchloroonenol Oil. 207 -OS -9 BenzoiktFluorantnene /f» LC CD 95-95-4 2. 4. 5-Tnchloroonenol ^TG ?.L 50-32-8 BenzooiPvrene /P t^- CD 91-58-7 2 -Chloronapnthaiene IO M 193-39-5 lnaeno Concentration:i: (Lo( Loww /Medium/ , (Circle One) ^-^.—* Date Extracted/Prepared: Date Analyzed: ——! "J'Zi. I o Conc/Dil Factor: CAS , ^_ Numbvr x , ^"^"TCirctB One) 319-84-6 Alona-BHC O.CS" tA- 319-85-7 Beta-BHC r c.r L^- 319-86-8 Detta-BHC cx:^ i-C_ 58-89-9 Gamma-BHC (Lindane) O.C^T t\_ 76-44-8 Heotacnior C-cC LA- 309-00-2 Alarm r .c«r Lt 1024-57-3 Heotacntor Epoxiae C-C5 L\. 959-98-8 Enaosuitan I. r.G?" L^ SO-57-1 Dieldrin ^/o U- 72-55-9 4. 4--DDE r,. fo tc- 72-20-8 Endnn OJO /X_ 33213-65-9 Endosutfan il r-io- i<_ 72-54-8 4. 4 '-ODD O^ /-L, 7421-33-4 Endnn Aldenvde p. i u *^. 1031-07-8 Endosuifan Sutfate p (C /.4 50-29-3 4, 4-.DDT C tO IJL. 72-43-5 Merhoxvchlor e-.sc 6c 53494-70-5 Enarin Ketone (". f C M_ 57- 74-9 Chlordane C.*ro ^ 8O01-35-2 Toxaohene f, O tv, 12674-11-2 Aroclpr-1016 r-/.VO £^- 11104-28-2 ArocJor-1221 f.CO U 11141-16-5 Aroclpr-1232 C-^u U_ 53469-21-9 Aroctor-1242 r-Vo i«- 12672-29-6 Aroclpr-1248 C.s-c i^ 11 097-69- 1 Aroctor-1 254 i-^ /t. 11096-82-5 Aroclor-1260 1- O K^ Vj a Volume of extract tnfected (ul> Vs = Volume of water extracted (ml) W_ = Weight of sample extracted (g) V. * Volume o^ total extract (ul) I/A v )Q.(nro SompbNumb* Organic* Analysis Data 8ha«t Uboraton/Mwnr »Co*a ——————— CM. No: —— C-JQO > ^ ————— QCIUportMo: ______i ——— Contract** a^. O4W S*mpi ^ VoMtoCompoundf. Concontratlon: <:^^r Metfum Oatt Extraet*oyPrap«r»d ————pH Pvc*m Moteurr 57.7 P«rc«ni Mototurt (Dwtmtd): ttv*w »MMjTh*lMW»tfw^**w«U- •»t»M I II Mil IM m»«MKMHfc*i» tfftMfc 4HIMMM MMHM »IM» *** Of9>nfes Anafytla Data Shaat (P»0t2) SsmJvofsttts Compounds Concsntrstion: Low £fl6dhj0? *(CiitfcQn«) l^jl/?4 I OstsAnslyistf: /U -.-. ;U^L . AMn*i*. Virynia 22313 703/U7.2490 Organics Analysis Oats Shest (Fa0«3) Concentration: Low /^Madiurn^ (Circle One) Data Ertractad/Praparwfc Data Anatyt»d: ———««1 Conc/OH Factor: ———LJ.————— CAS Number (Circle One) 319-84-6 Aiphi-BHC /20* 319-85*7 Bete-BHC ZQd^ 319-86-S DatU-SHC /zo. 5S-8S-9 Oammft-SHClUftdm) ; 2(X. 74-44-8 Htptachlor /ZOu. 309-00-2 AUrin /?0u 1024.57.3 HepuchtorCpOMCle /2c% . ' W9-M-8 EndnuKanl ;^o 60-57-1 OwkJrm x'/tOt, 72-SS-9 4,4'.OOE ?yOu 72-20-9 Endrin ^VOt. 33213-65-9 Endosutfan t) Z y 72-54-8 4, 4--OOO *-' V(7r, . 7421-93-4 Endiin Akfehyae ."3on, 1031-07-8 Endo*uH*n *utf»» X"^u ' . 50-29-3 4. 4--DOT ^SC u 72*43-5 MelhoKvchlor /•^ cv*u 53494-70-5 Endrto Ketone -.00 t, 57*74-9 Chtontorw / 7 &G*, 8001 -35-2 Toxaphene T^ro (^ 12674.11-2 Arodor-1016 x-:^/f, 11104-28-2 AroclOf-1221 VOoCa 11 141- 16-6 Arodor.1232 111 oc« 53489-21 -9 Aroclor.1242 . • ooo^ 12672-29-8 A/oclOf-1249 ?&?"•* 11097-68-1 Aroctor.1254 "V.V^ff 11094-82-6 Aroctor.1280 *• rf>ett Vj • Volume o* •rtraa injected (ul) Vs * Voluma el water extracted (ml) Wf * Weight of sample attracted tg) V( * Volume aftoul extract M) 3 gnvironm«msl Protection Agency, CLP Samole Management Office. Sample Number P, O, BaxSli. Alexandria. Virginia 22313 703/557-249Q Organics Analysis Data Sheet (Page!) Laboratory Name: Qu-lf Souch Research Institute Case No: Ub Sample ID No: - n t>f f______QC Report No: Sample Matrix: lAAlTC1______~ Contract No; 6B-01- Data Release Authorized By: .£^'-£ < ^"L^f ^t^3i_ <•&*** Date Sample Volatile-Compound* Concentration: (Low ; Medium (Circle One) -*——-* Date Am lyMri-"" }~&l % ( 5 *i , , , Conc/Di Percent FLrlnivtitra- /V/W Percent P^pjsture (Decanted) AJA — >» CAS £ CAS (ug^orug/Kg Numb«r ^t*-(£irei« One-l Numb«r ^^"^circle Onal 74-87-3 Cn loror n etna ne /O 0- 79-34-5 1, 1.2. 2-Teiracnloroetnane «^- w^ 74-S3-9 §romometnan« /n UL 78-87-5 1. 2-Dichloroprooane S" to 75-01 -4 Vinv* ChJonde- ;« LL 10061-02-6 Tran*-1, 3-DicPilorooroo«ne __a_5^ i'^-^' 75-00-3 Chioroatnane FLl «^ 79-01-6 Tncnloroetnene 75-09-2 MetnvJ»n« Chlonae 5- g.-r^- fL- 124-48-1 Di&romocrHoromethane S" tt- . 67-64-1 Acetone ,D rll_ 79-00-5 1.1. 2-Tnchl0roetn8ne 5~ tk- 75-1S-O Carbon Disulfide far rvaofTing r«tut» to EPA tn* following raiuRi qualifiar* arc u»*d €Tl Addrtwnai Rcoorr m* minimum Mtaction limit far tf%« tamo** Mrttn CTM U (• S . 1OJ1 CMMd en n*c*s*trv ee«e»mration' • Th« flag >» U*M *vn«n tn« analvt* n 'eund in tnt &i»n» *fi/tMWt aenenc fTht« « not o*e»«»af'h'I»»* nu«iXM» n rv fflffwmum anainMW* a*t»ciw limn ( gr * * 1 I mecm* Environmental Protection Agency. CLP Sample Management OHice. Sample Number P. 0- Box 818. Alexandria. Virginia 22313 703/557-2490 Organics Analysis Data Sheet (Page 2) SermvoiAtrle Compounds Concentration: (x^—- Low.^ / Mediu/m . (Circlj -.e Oner ) Date Extra :ted/ Prepares / Z- / S-LI /IT Date Analy«*«•• /£/ ^4 Conc/Dil Fartnr- ^ C O "~"~"""S. _ CAS (]ug/tflT ug/Kg CAS Lug/Lor ug/Kg Number ""[Circle One) Numbar ^*"~rCircle One! 62-75-9 N-Nitrosoatmetnyiamme fo i<~ 83-32-9 Acenaomhene - yo -^ 108-95-2 Phenol to f±_ 51-28-5 2. 4-Dinitroohenol -S"O ttta 62-53-3 Aniline in i<- 100-02-7 4-Nnrooh«nol S"D l^- 1 1 1 .44-4 b!S(-2-ChloroetnvilEther (O to 132-64-9 Dibenzofuran (0 t^ 95-57-8 2-ChloroDhenol to i*- 121-14-2 2.4-Dimtrptoluene !0 t*~ 541-73-1 1. 3-Dichlorobenzene 1C £A__ 606-20-2 2. 6-Dinitrotoiuene /O i^ 106-46-7 1 . 4-Dichlorobenzene 1C i«_ 84-66-2 Diethvlpntnalate 10 V~ . 100-51-6 Benzvl Alcohol _..._. in u^ 7005-72-3 4-Chloroonenvl-ohenvietner /C c*- 95-50-1 1, 2-Dicfilorobenzene . in u. 86-73-7 Fluorene /O u_ 95-48-7 2-Methvlohenol /O W- 100-01-6 4-Nitroanilme CD LL- 39638-32-9 tHSl2-chloroisoproovl)Ether 10 U. 534-52-1 4. 6-Oinitro-2-Methvlpnenol .VO LC 106-44-5 4-Metnvionenbl /n i^- 86-30-6 N-Nitrosodtohenvlamme (1) ypi i^ 621-64.7 N-Nitroso-Di-n-ProDvlamme JO M_ 101-55-3 4-BromoDhenvl-Dhenviether tO ;•- 67-72-1 Hexachloroetnane /D £.t- 118-74-1 Hexacntorobenzene 1C (/- XJ 98-95-3 Nitrobenzene fD tw 87-86-5 Pentachiorooheno) ^'O c%*r*' *' 78-59-1 Isoohorone /O fcC 85-01 -8 Phenanthrene /C tC '1? 88-75-5 2-Nitroonenoi in M_ 120-12-7 Anthracene ^O LC O 105-67-9 2. 4-Oimethvlonenol /O (L 84-74-2 Di-n-Butytphinatate /O CL , 65-85-0 Benzoic Acid 5~0 w- 206-44-0 Ruoramnene tO IL^ IT" 111-91-1 bis(-2-Chloroethoxv)Methane fO u^ 92-87-5 Benzidme - T { L^^^ er 120-83-2 2. 4-Oichtoropnenol IO t,v_ 129-00-0 Pyrene 1C tV_ 120-82-1 1. 2. 4.-Trtchlorobenzene 10 U 85-68-7 Sutvibenzvipntnalate /C Lt_ 91-20-3 Napnthalene /O K_ 91-94-1 3. 3'-Dicr>iprooenzidme o*C iA_ 106-47-8 4-Chtoroanilme '("> iv. 56-55-3 BenzotajAntnracene /O W- 87-68-3 Hexacntorabutadiene 'OL( 117-81-7 bis<2-E:nvinexvitPtimaiate ;CT ^J f_' ' 1^^ 59-50-7 4-Chtoro-3-Methv(phenoi iOL- 218-01-9 Chrvsene ;u tu 91-57-6 2-Methvmaphthaiene jo td 117-84-0 Di-n-Octvi Phthalate /O tt. 77-47-4 HexacniorocvciODentadiene fO tU 205-99-2 SenzcxblFluoranthene f /"' L^ 88-06-2' 2. 4. 6-TnchloroDnenol 207-08-9 BenzoiniFluoranthene f f* LC 95-95-4 2. 4 5-Tnchloropfienbi -TO i.L 50-32-8 BenzotajPvrene /P *-\- 91-58-7 2-Chlorona0hthalene 'O ;', 193-39-5 indencxl. 2. 3-ca)Pvrene (U «- 88-74-4 2-Nitroantlme 'lO iL 53-70-3 Dibenna, njAntnracene ^n U 131-11-3 Dimethyl Phthatate to lu 191-24-2 Senzaq. h nPervlene fO f.o 208-96-8 Acenaonthvlene '0 IK. 99-09-2 3-Nitroantltne SO v^ fmcin&^3,flf£«fromdlononv,.m,n. Environmental Protection Agency. CLPSamoi* Management Office, Sample Number P.O. Box 818. AUuanana. Virginia 22313 703/557-2490 /•*/->-/ " ^ Organics Analysis Data Sheet {Page 3) icide/PCBs Concentration: ( Low /Medium, (Circle One) Dare Extracted/Prepared— : —/}- z? / / &i /I Date Analyzed; J. Conc/Dil Factor; CAS *•••" Lug/lpfug/Kg Number x . {Circle One) 319-84-6 Alpna-SHC O.C^ tx- 319-85-7 Beta-BHC r c-v t*~ 319-85-8 Delta -BHC "~^ " ^ •* i t 58-89-9 Gamma-BHC (Lmdanef LJ - 1_.^ *"Vta^' 76-44.-S Heotacnior \j 't. ^ f***^. 309-00-2 Aldrin r .u=? LI 1024-57-3 Heotacnior Eooxide c-c? u~. 959-98-S Endosuifan I r.GT L*~ 60-57-1 Dieldrm O, ;o U- 72-55-9 4.4--OOE r,- 10 L^ 72-20-8 Sndrin O./O tL, 33213-65-9 EndosuJfan ll r-ic^ £c 72-54-8 4. 4'-DDD r.tv /^ 7421-93-4 Endnn Aldehvde n.fu ^^_ 1031-07-S Endosuifan Sulfate r- ( c IA . 50-29-3 4. 4--DDT C tO LA. 72-43-5 Methoxvchfor \-.5t. U. 53494-70-5 Endnn Ketone ,' '. f C £X_ 57-74-9 Chlordane C-*ro i/ 8001-35-2 Toxaortene f. Q i-\_ 12674.11-2 Aroclor-1016 r-,.ro ^c 11104-28-2 Aroclor-1221 r. Vj = Volume of extract injected (ul) V = Volume of water extracted (ml) W 3 Weight of sample extracted (g) V. = Volume o' total extract (ul) VS Environmental Protection Agencv. CLP Sample Management Office, Sample Number P. O. BoxSIS, Alexandria. Virginia 22313 703/557-2490 Organics Analysis Data Sheet (Page!) Laboratory Name: Gulf South Research Institute Case No: Lab Sample ID No: J^H£______OC Report No: ( Sample Matrix: t=l______i______^ Contract No: 68-01- Data Release Authorized By: ^vg^ ^r s< •**•" *-t*s**{ Qate Sample Received: Vo latile-Compounds Concentration: (Low / Medium . (Circle One} -"' Date Ana ly*** f*-/* h'4 < Conc/Di Fartnr- / - O pH '£?,.,- ^,T ,. Percent fJ*itt"»- /VAi /uA Percent Pdgiswre (Decanted) /- ^ CAS C.jig/ipTu«/Ko; CAS {ug/Lt>r ug/Kg Number ^^^"(Circt* OneJ Number ^ fCircle One! 74-87-3 Chlorometnanc ^O L«- 79-34-5 1.1.2. 2-T«tracnioroethane _5* t(^ 74-83-9 Bromomethane /o t<- 78-87-5 1 . 2-Dichloroorooane t" 75-O1 -* Vinvl Chloride /O (JL 10061-02-6 Trans-1. 3-E>ichloroorooene <~ t-U 75-00-3 Chioroethane f / * u. 79-01-6 Tnchloro«then* . T fJU 75-09-2 •Methylene Chloride S" Jl 1 J ^^ J 1 • 124-48-1 Dibromochioromethane $~ W- 67-64-1 Acetone fO f(_ 79-00-5 1.1, 2-Trtchloroetnane T U_ 75-15-0 Carbon Oisulfide .5" L^ 71-43-2 Benzene c tc 75-35-4 1. 1 -Oichloroflthene V t'w 10061-01-5 cis-1. 3-Oichloroorof>ene . fT **• 75-34-3 1; l-Dtchloroernans S" cc 110-75-8 2 -Chloroflthvlvmviether tC "- 156-60-5 Trans-1. 2-Dtchloroethene T Lw 75-25-2 Bromoform ^ f\ 67-66-3 Chloroform S* 6*- 591-78-6 2-Hexanone (O b- 107-O6-2 1. 2-Dichloroetfian* c- u_ 108-10-1 4.Methvl-2.Pemanone /c u_ 78-93-3 2-8uianone /"Ci U- 127-18-4 Tetrachioroethene ^" u_ 71-55-6 1,1. 1-Trichloro«th8ne S~ «_ 108-88-3 Toluene r UL, 56-23-5 Carbon Tetrachionde S" U_ 108-90-7 Chlorobenzene S" ^ 108-05-4 Vinvl Acetate / o **- 100-41-4 Ethylbenrene 5" ^ 75-27-4 Bromoflicnioromethan* ^" 4>*^ 100-42-5 Stvene 6" *L/ -rr Total Xvlenes <~ ,'.\ , en Oat* Avoorting Qualifwrt CO for fmontng raiotti to E^A. in* followrmg rvtutti Qualifiers art uMd CD Addrlional flags or footnotat axciaming rawlis arc «ncourag«d Howwvwr, ir>* dvftnnton of vacn flag mu*f D* •«ol«c« CD ValiM ff n* mutt i» a ntu« gr.*,.r tn*n tv «aual to tn« C Th.« f tag aeoi>» to BMIIOM oaf«m*wr» «^r. tn« OC ort.rmac by GC 'MS _ final tnnct inouW b* conlinncd by GC 'MS U Inacatn compound *«t anaiynd for out nor o»i«ei« Raoort tn* minimum MIMCIKXI umii for ma iamoia ••"" m» u (• a 1 OUt 0*aao on rwcauarv eenc»ntr*iifln ' • Tn'« fl*fl •» "«*0 <*«*" "*• »*wMt if totmo m in# oiank fThw i* not r»cw«.f.iv tha .n«rum,i« •• «*» *• • w™oi» « ermve4*vtHe Compounds Concentration; (^" Low^/ Medium (Circ)e One) Date Analy «.. (z-y/r/s-/-' ' Conc/Dil Far,nr-. ^TO Q CAS (^^ug/ljoTug/K g CAS (^ug/Lorug/K^~-g Number ""TCircie One} Numb«r ^*— •rfSircle One) 62-75-9 N-Nitrosodimetnyiamme (O L<- 83-32-9 Acenaomnene /O «- 108-S5-2 Phenol /O /c 51-28-5 2. 4-DmrtroDhenoi SO ^ 62-S3-3 Aniline in u- 100-02-7 4-Nitroohenol S"O tu 111-44.4 bis^-2-ChloroethvilEther td to 132-64-9 Dibenzofuran ^O t^ 05-57-8 2-Chlorooh.enol >C l*~ 121-14-2 2. 4-Dinitrotoluene fO t*. 541-73-1 1. 3-Dicniorobenzene 1C IX_ 606-20-2 2. 6-DmitrotOluene /o ^A 1O6-46-7 1 4-Dichtorobenzene 1C l<~ 84-66-2 Diethvlohthalate tc i>m 100-51-6 Benrvl Alcohol )r- u^ 7005-72-3 4-Chloroohenvi-Dhenviether fC, L^ 95-SO-1 1 2-Dichlorobenzene in to- 86-73-7 Pluorene /e /x_ 95-48-7 2-Methviohenoi IC tc 100-O1 -6 4-Nitroanilme CT} L*- 39638-32-9 bts(2-chiorotsooroovl l£ther /O u. 534-52-1 4. 6-Dmitro-2-Methv'Dnenoi S'C L^ 106-44-5 4-Metrivlofieno! ;n fl_ 86-30-6 N-NitrosodtDhenvlamine ( 1 } /n &- 621*64-7 N-fJitroso-Di-n-ProDviamme ;0 w_ 1O1-55-3 4-BromoDhenvl-Dhenvletner /O /*- 67-72-1 Hexacnioroeinane /O fw 118-74-1 Hexacrtiorobenrene ;C i.<- 98-95-3 Nitrooenzene /n to 87-86-5 Pentacniorophenol -S'O L^ 78-59-1 Isoohorone fo u~ 85-01-8 Phenanthrene /C tC 88-75-5 2-NitroonenoJ in £.<. 120-12-7 Anthracene /C LL 105-67-9 2. 4-Oimetnvlonenol /O (L 84-74-2 Di-n-Buiv'ohthalate /C LL 65-85-0 Benzoic Acid yd i'-1- 206-44-0 Ffuorantnene /O LL^ 111-91-1 bia-2-Chloroethoxv)Methane io i>- 92-87-S Benzidine Pgsticid e / P C B s Concentration: (Low /'Medium (Circle One) Date Extracted/Prepared: f"2- f *-t I iv~ Date Analyzed: W^ b "______ CAS Cug/ip* ug / Kg Number TUircle One) 319-84-6 Aiona-BHC n.cs- &~ 319-85-7 . 8eta-8HC r,nr o- 319-86-8 Deita-BHC C^.'^ LL^ 58-89-9 Gamma-8HC ILmaane) o.r,s" <>\^ 76-44-8 Heotacnior C.r-C /x_ 309-00,2 ... Alarm r .L*T LI 1024-57-3 Heotacntor Eooxiae C-O5 U. 959-98-8 Enoosuifan 1 fn^/?~ L>- 60-57-1 Dieidrin ^ /CJ t^ 72-S5-.9 4, A'-DDE r.. to ct^ 72-20-8 . Endrrn O./O /,x_ 33213-65-9 Endosuifan II r-iu ic 72-54-8 4. 4'- ODD r./u /A, 74 21 -93-d Endrrn Aldenvde f).|0 *_ 1031-07-8 Endosuifan Sulfate r- (C 7.4 50-29-3 ,. 4. 4'-DOT C fO i.i. 72-43-5 Memoxvchlor r.^t- 0. 53494-70-5 Endnn Ketone (-. f C t^ 57-74-9 Chlordane C.*s-o ^ 8001-35-2 Toxaohene ]. O tv. 12674-11-2 Aroclor-1016 f, VG 6^ 11104-28-2 Aroclor-1221 r.CO W 11141-16-5 Aroclor-1232 tJ-^U ^ 53469-21-9 Aroclor-1242 r.-C(j t,^ 12672-29-6 ArocJor-1248 C-S'O /x_ 11097-69-1 Arocior-1254 i-o ;( 11096-82-5 Aroclor-I2SO j - O " i*-' j = Volume of extract injected (ul) = Volume of water extracted (ml) W = Weight of sample extracted (g) V. = Volume of total extract (ul) vs Number 2. Oryantes Analysis Oats Shaat CwNo: QCteportNo: Contract No: VoMla Compoundf . Conotntration: <^£pr Medium (Circte On*} Date Extract*d/Fr«pvKt: Moteurr _ — , Pcrcaitt Moistur* {Otcantvd}: CAS 79-34-5 1, 1, 2. 2-T«trachlofO«han* /Ov^- 78-87-5 1.2'DfChloroprooane /C (/- tooei-02-4 o 'tA^* 79-01*6 Trichteroetheoe . S LT- 124-48-1 oni ltu >*• wrviC Jt i- u w oma lhinanv 79-00-5 1.1. 2-Trtchloroethane /C \^B\ 71.43-2 Bcnnne 5v^» 10061 -O1-5 Ctt-1. 3-Oichloroprop9n« •Ttr— 1 10-75-8 2-ChIoro*thyMnylaihtff / ^ t/ — 75-25-2 Bromoform / v if- 691-78-6 2-Heianont 5\— 106-10-1 ^ i/ " 127-18-4 J \>""" " 106-88-3 Toluene ^ir- 106-90-7 Chtorotwnarne Ssmlvotsttta Compounds Conc*mrstion: low cJflfijijji? .(CirctoOna) / CAS Form I tr*«er*-n«nm*ii«»: inn Agency. SampU Numter P.O.SMS18. Atean*«.VW9ifHa223t3 703/U7.24SO C Organies Analysis Oats Shaat Concentration: Low adium? (Circle Onaj) DM Data Anatywt Cone/Oil Fsoor: ——/..,/ CAS ftfumaa* 319*84^ AJph»-BHC /20^ 319-85-7 Bata*BHC 2KCn 31&-M-8 Datta-SHC /2V,. SS-89-9 Gamrnj-BHC (Lindana) /zo* 76-44-8 /* 1 1 104.28-2 Aroclor-1221 &~J rtQU ni4i-ie-6 Arador-1232 7- ''&&i< 53469-21-9 Arador-1242 y«r»ff,, 12672.29-6 Aroc(or-124S *--rv. en 11097-69-1 Arodor-1254 y 9-"-^ CO 1 1096-62-5 Arador-1260 •^'f (7^, CD CD Vj * Volwma of axtraet irvactcd (ul} rr- Vf * Voluma of watar axiract*d (mt) «X Wt • Wa*eN of aampta aitraciad (9) V( * Voluma of total attract (uJ) F\ or Wt t f --— V, ABI003'99 Forml 4'84 Samp*aNumb*r W/MT-WW C- 7 G Organics Analysis Data Shaat <: • 7 s •• i V QCRtportNo: Simp* Mttrix Data ftataaaa Author iw3 By: ,..<'r^r-c^"^ 0»tt S»mpl« Racaiv^: M- j f / ? "——— — Votetiis Compound! . Concentration: <^t^ M**om (CirctoOnt) o Data _ DataAnaJyiacfc —— f ^c ^jjj' ———————— - O H Parcant Moistur* (Dtcantod): CAS (CtrdaOoa) Mumbat______ Ssmtvolsttts Compound* Coocamntion^Loi/ tUadiucn .(CirctaOna. CAS o9/l«»«gS CAS ' ug/lo Atoundna. Wn>ma 22313 703/557-3490 Organics Analysis Data Sheat (Page 3) Patticido/PCBi Concentration: CVl»ow^' Medium (Circle One) Data Enractad/Prapara^: Date Analyzed: —— Cone/Oil Factor: CAS Numtar CCircta On*) 319-84-6 Aipha-BHC *,0o 319-85-7 Bata-BHC ." '% 319-88-8 Dotta-BHC l-.C,, S8-B9-9 Gamma-BHC (Undarw) z.O. 76-44*6 *• . ('i. 309-00-2 AkJrm ' C" 1024-S7-3 HaptactUor Epoxioa 7..1 W9-98-B Endoautfan 1 i 80-57-1 Diatdrin V-A 72-55-9 4.4'-DD£ '•/.Or, 72-20-8 Endrin V.^ 33213-65-9 Enooauttan H V,(V 72-54-8 - 4, 4--DDD 7.^ 7421-93-4 Endrin Aldahyoa / . •* ' • j 1031^)7-8 Endoauttan Sutfata '<"*}» 50-29-3 4, 4'-OOT it i\» 72-43-5 Mathoxychtor 7 * "',. 53494-7O-5 Endrin Katona '/.::., 57-74-9 Diloroane ?C)tt 8001 -35-2 Toxaphana ^u . 12674-11-2 Aroclor-1016 zc^ 11104-28-2 Arochx-1221 <~ L is *? •-, 11141-16-5 Aroctor-1232 l 4 53469*21-9 Aroctor-t242 ', '\. 12572-29-6 Aroclor-1248 <»\ 11097-69-1 Aroclor-1254 ','Ou 11096-62 -5 Arocior-1260 '/o* V- B VoJum* of axtract injactad (ul) V. « Voluma of watat axtraetad (ml) Wf = WatQhi of sampta extractad (g) V( = Votuma of total artract (ul) Environmental Preliction Agency. CLP Sample Management Office Sample Number j P.O. Bo* 81 8. Alexandra. Virginia 22313 703/557-2490 Organics Antilysis Data Sheet (Page D Laboratory "N*m«- Gulf South Research Inscitu :e Case No; 3,6 03 . . Lab Sample IDNn* .MD-^1 QC Report Nc ( Qt^i* 1 <~C7 Sample Matr .. tLx /, Contract No: 68-01- (j.* j n SSS f £trr'"*''S \ -, i —if-itrt-^ Data Release Authoriz **"! HV" (S-i'~f(* ' ^" f ^f »**• 'L' •* ^ Date Sample Received- JI ./I//.?/ / i VolatilaJ5)mj sounds Concentr•ation: (Low Medturn (Cire;le One) \— -• Date Extiacted/Prepareds/: ^^ l Date Ana Iy7«rt- 12-^ Conc/Di Percent 1Joi<:rirr«- A/ .W Percent f^gisture (Decanted) A/A CAS t»g/lpf u0/Kg CAS C vg/lftr uy / Kg Number (===fcTrel» On«» Number '"*• "Tcirela On«t 74-87-3 ChlorometMsne /O t.- 79-34-5 1. 1.2. 2-Tetracnloroetnane C tu 74.83-0 Bfomomsmane 'O y- 78-87-5 1, 2-DicnJoroorooane •r™ 75-O1 -4 Vinv* Chiof ide ;« U- 10061-02-6 Trans-1, 3-Dicntorooroo«ne 5jr, ^•C, 'j 75-OO-3 Ctiloroetnane. ^CJ U- 79-01 -6 "TneMloroetriene 5^ ^ i 75-O9-2 Metnvfane Chtorifle *T"^,r -g- j^f^-? 1 24-48- 1 Oi bromocn f oromema ne «-«. 67-64-1 Ac«ion« rfj /C 79-00-5 1,1. 2-Tncfitoroemane 5" i>~ 7S-1S-O Carbon Oisuifide V iL 71-43-2 Benzene ^ LL 7S-35-4 7. 1-Dichforoatnene 9 U. 10061-01-5 Cis-l, 3-DiCrHorooroD«ne £? t*- 75-34-3 1. 1-Dtch!oro0ihane S" 1C 110-75-8 2-Chforo«thv(vfnvieiher /C "- 156-60-5 Tr»nj-l. 2-Dtehloroeth6ne S~ Lw 75-25-2 Sromoform ^" H- 67-66-3 Chloroform s" t^ 591-78-6 2-He*anone /O ^*- 107-06-2 1.2-Oicntoroethane *r tc 108-10-1 4-Metnvl-2-Pemanone /C U_ 78-93-3 2-Suianone ''D LL- 127-18-4 Tetra en loroetn s n e ^ a 71-55-6 1.1. 1 -Trieritoroetriane S~ tt_ 108-88-3 Toluene 5^ iX_ §6-23-5 Caroon Tatracnionde S" U- 108-90-7 Chlorobenzene 5~ *O 108-05-4 Vinvf Acetate / O l*- 100-41-4 Ethvlbenzene r* to 75-27-4 BromocJiCfilorometnane1 Vmttm t tft* mua i . o«i.m*e »v GC 'MS U. . (noenr,___c eemooun___ d^ w« s tnihrrad^ fo .r Out ntn a*i»ci*_d SftouKI (M contfrmea 6y GC 'MS ft»wn tn* minimum aewciwn imir lar ih« ume» nomoer i« tn* rrwwnum jnumaew eetecttoo nmn for , «*e um*.a Q**r Otrter soecifte flag* and footnotes mev 6e reamred to sroperiv define fne retuni ff ufteQ tftev muft oe »u»v Tin* fl«f it ume ertne* _ dvfenttM ana men aesefipttoA anaened to tne oau .ioi •r wmen in* mew caeetrai on* »na«ttee tne er Environmental Protection Agency, CLP Sample Management Office. Sample Number P. 0. Box 818. Alexandria. Virginia 22313 703/557-2490 Organics Analysis Data Sheet /-\ (Page 2) £&& Sernive4ajile Compounds Concentration: LLow/ Medium (Circle One) Date Ana!> ypd-. 112-* 1M YI V JAl *4T Conc/Dit Fartnr- ^ O O _ m_ CAS (^*""~"^ug/ifl!T ug/Kg CAS LugA-oS* ———^ r ug/Kg Number "^TCircle One) Number • ^""rcircle One) 62-75-9 N-Niirosodimetnylamme /o io 83-32-9 Acenapmnene /O *- 108-95-2 Pheno* to f^ 51-28-5 2. 4-Oinitropnenot 5D tv- G2-53-3 AmJine /r> t<- 100-02-7 4-Nitroonenol S"(J ic 1 1 1 .44.4 bisf-2-Chloroetnvi)Ether /O to 132-64-9 Dibenzofuran /O tv- 95-57-8 2-Chlorophenol /o*^- 121-14-2 2, 4-Dinitroto'uene ^O i^ 541-73-1 1. 3-Oictilorobenzene ;c w^ 606-20-2 2, 6-Dinitrotoluene /O LL^ 106-46-7 1, 4-Dichforobenzene /C 4^. 84-66-2 Diet hvJpntfia late 1C i*~ 100-51-6 Benzvl Alcohol »n tu- 7005-72-3 4-Chloropnenvl-phenytetner fC> u- 95-50-1 1. 2-Oichlorpbenzene /O tc 86-73-7 Fluorene /O M_ 95-48-7 2-Methvlphenoi /O tc 10O-01 -6 4-N»troani|ine CD y. 39638-32-9 brs(2-chIoroisopropvoEther JO (^ 534-52-1 4. 6-Oinitro-2-MethylDnenoJ SO U. 106-44-5 4-Metrwlpnenol ;o i^- 86-30-6 N-Nitrosodiohenyfamine (1 } /r» 6- 621-64-7 N-Nitroso-Oi-n-Proovlamine ;0 w. 101-55-3 4-Bromophenyt-phenyiether /O /^ 67-72-1 Mexacnloroemane /O £A_ 118-74-1 Hexachlorobenzene /C ,,-u 98-95-3 Nttrooenzene /n tw 87-86-5 PentachJoroohenol i'C tv- 78-59-1 Isoohorone /O vU 85-01 -8 Phenanthrene /C c<_ 88-75-5 2-NitroDhenoJ rn M^ 120-12-7 Anthracene /O d,c 105-67-9 2, 4-Dimethvlohenol /D (L 84-74-2 Oi-n-Butyiphthalate /O CL 65-85-0 Benzotc Acid 5"0 w- 206-44-0 Fiuoramnene 10 IL^ 111-91-1 bisf-2-ChloroethoxvtMethane 10 iA. 92-87-5 Senzidme Concentration: ( Low/Mediurrj {Circje One) Date Extracted/Prepared: Date Analyzed: _L. Conc/DH Factor: CAS Lug/Ipf ug/Kg Number ^"""TCireie Onej 319-34-6 Alpna-SHC O.CT CX- 319-85-7 Beta-BHC r cr L>*- 319-86-8 Defta-BHC CJLX LL- 58-89-9 Gamma-BMC (Lmdanei Cr.C*T t^- 76-44-8 Heotacntor C.cC /x_ 309-00-2 Aidrtn r .c«r u 1024-57-3 Heotacntor Epoxrde C-G? U, 959-98-8 Endosuifan 1 r,.C Vj = Volume of extract injected (ul) Vs s Volume of water extracted {mlj W? = Weight of sample extracted (g) V s Volume of tptal extract (ul) 7 . Onpnfcs Analyse* Date Shtwt . . ' No: • 730 ^ V ______OC (Upon No: s ______Contract No: I?-/ VoMei Compound!. Medium (Clre«*Onv) CAS vevfM««»*«eft*tMierM»»e*Mei»e* C IMefef •» M «e«-. 10UI X«^ e» ^ i in 111 i n i H i i' • »r,WJl Form , -ftRlOOUOS Of* Wf»*i 233U OiyanJc* Analyala Data Shoot (Paoo2) SantivolatUa Compounds Concentration: Low f CAS ug/teraig/IC^ CAO u0/lorurrK (ClwleTJR; fifi f Form iI *•*•"•S tl «I V^T w /. 4/f Office, ftwfipl* Number Sot US. Atoui*r*. Virginia 22313 703/iS7-24ta (T7JO/ Organics Analysis Data Shoot (Pago 3) Povtfeida/PCBs Concentration: Low (^ModiumJ {Circle One) Date Daw Anttyatf: - Conc/OU Factor CAS Numbof 319-85-7 Ben-BHC Delu-&HC S8-S9-9 Oammt 76^4-S AUrin 1024-57-3 HepceeMor Eooud* EndoeuHent 5O-57-1 Diet** 72-W-i 4,4'-ODE Z2-204 33213-65:9 72-W-* 4. 4 -ODD Z-/3 7*21-93-4 EndrtnAUehvoe 1031-07-8 Endo»uH»n SuH ate 50-29-3 4.4--ODT 72-43-5 Endrin Ketont 57.74-9 CMordane 8001*35-2 TeMphen* 12674.11-2 Aroctor-1016 11104.28-2 Aroelor-1221 11141.16-5 Arodor-1232 53469-21-9 Aractor-1242 12672-29-6 Arodor-1248 11097.69-1 Arodor-1254 11096-82-5 Areelor*1260 Vj * Volume of emreet injected (id) Vj « Volume ol water extracted (ml) W§ * Weight of tampfe exacted (g) V( * Volume of ttttt extract {ul. V. ,/° v /n.oo^ A form Swnpea Number r, 7jo5 Organic* Analysis Data Shoot . (Pt0ol) ££=______CaaeNo: -7fe 03 ^^^tpa^'t^r-V C- /-SUJV——— OC Report No: SWfeMnris:—*^0|U——.——————————— Contract Ma . By: ***? >c.*£+***^ Date Sample A«cehwl VolatPo Compoundf, Conetntrstion: C^r Ma»*um (CirciaOnaJ Daia Extracted/ Daw Ana»yJ»d; I..*/ .pH. CAS (CboteOne Number 74^7-J Ottoramarhane 1,1,2, 2*Terrachloroetrtan* 74^3-9 f d \r* 1. 2-Dtthtorooropane VfnytCMoride Trent-1.3-DtehloropfOpene 7I.-CO-3 Dnerotihen* / 0 V-' TrieMoroethene 124^8-1 Dejfomochloromtthene *7-S4~t Acetone 79-00-5 1.1.2-Trichlo»oomane 76-tS-O CMtoiOiaulfiOe 71^3-2 Becuene t, 1-OieMoroethene 10061-01-5 Ctt.1,3-E>«ch*or^^'^^" 75-34-3 1. f 1 10-75*6 Tn»oe-1, 2-OidMoreetttene 75-25-2 Ofomoteim €7-66*1 591-78-6 2-Mexanone 107-06-2 108-10-1 *44etn*/f-2-*vmenane 76-93.3 2 127-18-4 Tetrechtoroethene 71-66-4 . f. t-Tflehtooeihai»e 108-88-3 Toluene S4.23-6 Carbon Tetraehtende 100-90-7 Chtorobencene 106-06-4 WtyfAaetat* 100-41*4 Ethyfbemene 75-27-4 BromodjChleromethane 100-42-5 Styrene Total Xytene* V*v«eaHeei*«>we|f«e ,11 i*Mk ewMMMneMM f 0»«revKMr< *eiwche«wii«*»u ori Sample Number 0.6*618. A*«wr*«.Wf«it;U3l3Xa/U7.a4eO , Orpanfes Analysis Data Shoot Samlvotettta Compounds Conctntration: Low ^M^J^-'. (Drc*a Ona) ug/lor form I ImyiregyneyitalPTeteciJonAjancr. Sample Number P.O,6e«S19, AJMandrat.VWffina 22313 703/567-24*0 Organics Analysis Data Shoot (Pago 3) Ptttfcida/PCB^^__—--—^s< - * Concentration: Low ( Medium } (Circle One) Data Extracted/Prepared: Cone/W Factor: /..'/ CAS 119-84-6 Alpne-BHC teo» 319-85-7 Beta-SHC fkv *». 119-86-8 Delta -8HC y/J*i 58*89-9 6amma-BMC (Undane) . /-:/)*. 76-444 Heptachlor fZfi. 309-00-2 Atorm t 2t% 1024-57-3 HeocactitorEonide /2Ov M9.98-8 Endeautfan 1 /2tV 50-57-1 Dioidrm ZsfO* 72-S5-9 4. 4'-ODE Z/Pu 72-20-8 Endrin .c/o. 33213-66-9 EndoauHan U 2. iOu 72-54-8 4, 4*-DDO 2iO, 7421-93-4 Endrin Aldehyde ZI"L\ t 031-07.8 Endotulfan Sutfaie -;/ 3u 50-29-3 4, 4--ODT ZbOti 72-43-5 Methovychtor itOO^ 53494-70-5 EndrtnKetone *D C-fc 57-74-9 Chlorden* jj^_ & ^*T 800t.35-2 Toxaphena 3^ ^r c^o / 12674- IT -2 Aroctor-1016 £. .^t?5u 1110* -28 -2 Aroclor-1221 "•5 "7 C 3, M141.1C-5 VocJof-1232 S'*, 00^ '" 53469-21-9 Aroclor-1242 •270CS 12672-29-6 Aroclor-1248 / 9.-^i, 11 097-69- 1 Arockx-1254 V^HK 11096-82-5 Anxtor-1260 ^y,?^ V. * Volume of extract injected (ul) V( > Volume of water extracted (ml) Wft * Weight of Mmpie extracted (0) V, * Volume of total extract (uO V. ______orW. 4'B4 •ample Number 703/667.2480 iI C^,. -7 j- G Organic* Analysis Data Shoot Laboratory Kama: CaaaNo: 7.3Q b V—————— QCRaportNa Samp»,M«rte ot ,———.——————— Contact*: DataftolaaaaAuinorindBy: mf ^f'V^rV-^ Data Sampla ftacafcad: Votatfta Compounds. Concentration: <^\&2 Madiom (Clrda Ona) Data Extracted/Freparad; Data Anaryrad: __ ParcantMoiaturr Parcant Moittura (Dacamad): CAS uo>1o<1g^]Ca^ c** __ Number 79-34-5 1.1,2. 2>Tetraehlorpethane 78474 1 . 2-DfehtofOpf opine Trent-1,3-DieMoropropene 79-014 TrieMeroethene 124*48-1 DMromochtoroma thane 79-00-5 1. 1. 2*TrieMoroaitiane 7143-2 Boftnne 10061-01-6 en- T. 3-Dichlof oprupene 110-754 2-CntoroeihvMoyiethef 76-25-2 aromotom 691*784 2-Neunone 108-10-1 127-18-4 Tetraenloroathene 108-88-3 Toluene tfa 106-90-7 Chlorobeniena 100-414 Elhylbantene 10042-5 Styrena Total Xvtenet B>«e««*r erfww Vie « even eeewttMM MMC*W« w NW ecu J\RiOOUI2 r. 0*1 *.as»St8. AaMAn.V»fMa 12313 703^674480 Organic* Analysis Data Shoot ftamfootatila Compounds Concentration: Low Data Analynd; Cone/DU Factor CAS DibenKa. hVknthraeene CLP tempi* Me«*f.eflne*«Offie*, £*mp** ao-tlt, Atoiandna.Vire.Ma 22313 703/567-2490 Organics Analysis Data Shoot (Page 3) Poatiekto/PCBs Concentration: Low CMediuni/>*?~~~-~~?"yS (Circle One) Data Extracted/Prepared: Data Anah/zed: ————• Cone/Oil Factor: — CAS ug/lor/uo/Kfl Number 319-844 Afehe-BHC /^'«. 31945-7 Seta-BHC SOGu 31946-8 Dette-BHC /2Pv 58-89-9 Oamma-BHC (Undane) /•2C V( * Volume of extract injected (ul) Vft « Volume o* water eitrected (ml. W$ * Weight of sample ecu-acted (o) V, « Volume of total astract M) vt Fofml gnvironmenwl Protection Apencv, CLPSample Management Office. Sample Number 703/557-2490 C Organics Analysis Data Sheet (PageT) Laboratory Name: Gulf Souch Research Institute Case No: 36 Lab Sample fD No: ^± ______QC Report No: Sampte Matrix: v.T1 . _____ Contract No: -6 8-0 1- Data Release Authorized By: ^^>VOk-'3£^' Date Sample Received: Volatile-Compounds Concentration: (Low ) Medium (Circle One) N^—-^ . -. J _ i , / Date An;ty9mH. • ,-z,/^ /s C ia*w(ic«ion n*i DM" eomlirm«a erv CC'MS Strtyi COTioon*ni iMHicMMf >10nfl'ul tn m* fintl *jnr«et U 'MS Btpon m* mtnwnwm s*t*Ct(on *i"«t foe m* **fniw* wiin tfi*Uf*g. IOOJfl*»*ae«n»c««*Jn'efloe*ntr«non!' • Thu f(»g » u u§*f to Lit* Th* um «n*in*Iw* a*[*CTiO" iwnrf for rro«o *nfl jucn o*tcr*of «wi •n»en*o 19 in* a*'* F" D Environmental Protection Agency. CUP Sample Management Office. Sample Number P. O.BoxBlB. Alexandria. Virginia 22313 703/557-2490 . C Organics Analysis Data Sheet (Page 2) Sermve>4a|iie Compounds Concentration: s^—-( Low^ / Mediuim . (Circlf _.e r One) Date Extra ned/ Prepares - /z-/ S"-6 / IT Date Analyzed: |7J ——————————————— Cone/Oil Fartj-v- nO O X- - ' ——— > ^ —— \ CAS (^ ug/ljar ug/Kg CAS ( ug/Oor ug/Kg Number {Circle One) Number ^•^fCirele One) 62-75-9 N-Nitrosodimetrwlamine fO l^- 83-32-9 Acenaohthene /O ^~ 108-95-2 Phenol to (_^_ 51-28-5 2, 4-Dimtrophenol .S"O «"- 62-53-3 Aniline in i<_ 100-02-7 4-NftrotJhenol S"O U- 1 1 1 .44.4 bisf-2-Chlaroetrwl)Ether ID t\^ 132-64-9 Dibenzofuran 10 L^ 95-57-8 2-Chloroohenoi /c t*~ 121-14-2 2. 4-Dinitrotoluene tO L^ 541-73-1 1. 3-Dichlorobenzene )C t,L- 606-20-2 2. 6-Oinitrotoluene /O H__ 106-46-7 1 , 4-Dichlorobenzene tC i^_ 84-66-2 Diethylphthalate /C is- 100-51-6 Benzyl Alcohol IP tw 7005-72-3 d-ChlorODhenvt-phenvlether fC. Lw 95-50-1 1. 2-Dichtorobenzene JO iL. 86-73-7 Fluorene /© w_ 95-48-7 2-Methvlohenol 10 t-c 100-01-6 4-Nitroaniline CO t.1- 39638-32-9 bis(2-chlorotsaproDvn£ther 'Ou- 534-52-- 1 4. 6-Dinitro-2-Methylphenol •VO CA~ 106-44-5 4-Methvlohenol in t _ 86-30-6 N-Nitrosodiohenylamine (11 /(^ 6- 621-64-7 N-Nitroso-Oi-n-ProDvlamme ;0 U- 101-55-3 4-Sromophenvl-Drienvleiher /O /*- 67-72-1 Hexacnioroe thane /O (^ 118-74-1 Hexachtorobenzene ;C (*- 98-95-3 Nurooenzene in i\s S7-86-5 Pentachlorophenoi iaO T~ ^"Q"-u»_ 78-59-1 Isoohorone /D vu 85-01 -8 Phenanthrene /C t^L, 88-75-5 2-Nitroonenof in te 120-12-7 Anthracene /O LL 105-67-9 2, 4.-Dimethyipnen.ol / D (L 84- 74-2 Di-n-Suivluhthalate /C U. 65-85-0 Benzotc Acid TO M- 206-44-0 Ftuoranrhene t OT* / C Lf_ 111-91-1 bis(-2-Chloroethoxv)Methane '0 L.V- 92-87-5 Benzidine V/j s Volume of ertract mjeeied (ul) Vs s Volume of water extracted [ml) Ws = Weight of sample-extracrad (g) V = Volume of tPtal extract (ul) v$ - IQUU orw;_LLil___ v /o , Q 6 * ^^^^^^""^•^^^'••"'^ C ^^^^ - - ^^^^ ? ^^^"^MBBi^^^^^B^^Bi P.O. to. an Organic* Analysis Data Shaft Laboratory M«na: No: 3 o V QCIUporfNo: SolL ———————— ComrKtN* 0«te Swnpto Reeehwt VototHa Compound^. Medium (OrctoOna) CAS lee Mrfiimtfcy OC/Mt • HMMcftoMaMiMi aiir ^^W.-KLH Por^j * RQinQUlS O SampUNumaar C 7^0 f Offfsnles Anstysis Data Sha*t (Pi0t2) tamivotattta Compounda Madium *fOrclaOna) * / / j Form I tiujmuimiuirrgeac»onAj»rcT. CL**Samp**Me*t»ge««e*«Office Semple nf um6er ».0.»«81I. AJwmJria, Vk^ma 22313 WJ/W7-2410 Organic* Analysis Data Shaat /PCa* Concentration: U>w_ Medium (Circle One) DataEvtractad/Praparad; DataAnalyzad: Conc/Dil Factor: CAS lumber (Circlei 319-84-6 Alphe-BHC e.tv 319-85-7 Bet*-8HC a^.cv, 3 19*Ow*o DetU-ftHC ^ C,.. BB-89-9 Qemme-BHC {Lintfene) •j . 0- 76-444 HtpteCMOf p.fi* 309-00-2 Atdrin ?-&• - 1024-57.3 Heetechlor Eponde *.(?., .. M9-98-8 EndotuHenl t.Q,, 8057-1 Oieldrin VfV. 72-55-9 4. 4'.OOE V,0o 72-20-8 Endrin y,o<. 33213-65-9 Endc*urtanB V| * Volume ol extract injected tut) V, « Volume of water exirected (ml) Wf * Weight of temple attracted (9) Vt > Volume of tout extrect (u*) form 1 « «• i w w T«. w 4 ,a4 Environments! Protection Agency. CLP Sample Management Otf ice. Sample Number P.O. Box 81 9, Alexandria. Virginia 22313 703/S57-249O (L ^^o0/ Organics Analysis Data She et 4 (Pagel) 2 Laboratory N emer Gulf. South Research Institute Casp No- — UP Sample I™«- HD3PI QC Report Ncj> { $-mf- Sample Matr *. \Aj4.i&~ Contract No: 68-01- U-^^1 Data Release Authnrfysd By ^^^/Vi^S <^T Date Sample RArr*iw*H- f ^ / Y /* ' 1 < VolatjIe-JCom pounds Concent •ation: (LowJMIidium (Ci:lre One) V-^- Date Ext-acted/Prepared: "2, /T^/y^ Date Am £./ 9 ) y'H ' Conc/Di Percent 1Lflft»ct.tfi»- A/r*> Percent f^gtfttjre (Decanted) /uA CAS ug/Ipr ug/Kg CAS ^ Number <*— 'iCTrei* One) Number ^^•^TCirele On«l 74.07-3 Chforometftane /C t«- 79-34-S 1. 1. 2. 2-Tetracrtloroetnane ^- tt- 74-83-9 Srornometnane >n y- 78-87-5 1. 2-Dichiorooro0ane c* 7S-01-4 Vmv* Chfonde 10061-02-6 Trans-1, 3-DfCfHoroorooene ^" ^O 1 /n U. *, i 75-00-3 Chloroeirijne /•(J IX. 79-01-6 Triehloroetrtene 75-09-2 _] Metnylene Chlonde *f J3r jg. n_ i 124-48-1 DtbromocnioromBthane _>~ i>*- i 67-64-1 Acetone 'L> ilw 79-OO-S 1,1. 2-Tncntoroernane V tfc- 75-15-0 Carbon Dtsuifide 5" LL 71-43-2 Benzene 5" LL 75-35-4 1. 1-OicnJoroethene C LC 10061-01-5 CiS-1. 3-Otcnloroorooene ff* ^ 75-34-3 T. l-Oichforoerhane S" LU 110-75-8 2-Chioroethv(vinv(ether iC "- 156-60-5 Tran«-l, 2-Dictttoroemene V Lw 75-25-2 Bromoform T 4. 67.66-3 Chloroform C t*. 591-78-6 2-H.ntanone /O ^*- 107-06-2 1, 2-Dichioroemana c- u. L1 08- 10-1 4.Methvt-2-Pentanone /C U. 78 -§3-3 2-3uranone fb U- 127-18-4 Tetrachloroeihene r u_ 71-55-6 1, 7. 1 -Tncftloroetrume r iu 1OS-B8-3 Toluene r LC 56-23-5 Carbon Tetracfifonde s~ u_ 108-90-7 Chlorobenzene ^ *o 108 -OS-4 Vmvi Acetate /O u- 100-41^ gtnvlbenzene ?~ itx 75-27-4 Sromodicfiiorometnane ^- ix^ 100-42-5 Stvrene 5- ^ Total Xvlenes <~ ;t y Data nworTing Qu*t(fi«f» Far inserting rtiutts to E»*. in« flowing rviulis au«lrf«ri «r Mdnionil ftags or fomnmsi •KoUintng r*uitts ir» •ncaur«g«a Ho«ww«r. mt •vfinnion of «*cn fia^ mun M •wipctt m«a ov GC 'MS l •ifiy M( SemivoJ*tiIe Compounds Concentration: f Low/ Medium (Circle,0ne) Date Anat>«H. VlfrhH Conc/Dil Fartnr- *\C Q CAS (^'ug/l*rug/K ———> g CAS fX ug/Lorug/K ———* g Number 1 fCircleOnBl Number ^^--fCtrcfe One) 62-75-9 N-NiTrosodimemviamme to £<~ 83-32-9 Acenaontnene /O :^- 108-95-2 PhenoJ (0 ,c 51-28-5 2. 4-Dinttroohenot ^o t- 62-53-3 Aniline . /n y- 10O-02-7 4-Nitroonenol SD ix. 1 1 1 .44-4 bis(-2-ChloroethvHErher /O to 1 32-64-9 Dibenzofuran /O t^ 95-57-8 2-Chforonhenol /D i<~ 121-14-2 2. 4-Ointtrototuene to ^ 541-73-1 1. 3-Diehlorobenzene 1C t^- 606-20-2 2. 6-Oimtrotofuene ' /O u- 106-46-7 1. 4-Oicnlorobenzene . /C U_ 84-66-2 OierhvtoMthalate iQ V~ 100-51-6 Benzvl Alcohol fn LO 7005-72-3 4-Chloroohenvl-pr.envtetrter /C- c^ 95-50-1 1. 2-DiChlorobenzene >n U- 86-73-7 Fluorene /€> \JL. 95-48-7 2-Methvlpnenol /c w- 100-01-6 4-NJtroanifme CG y- 39638-32-9 bis(2-chloroisoproDVllEtrier '0 t^ 534-52-1 4, 6-Dinitro-2-Methvlphenol £0 (A- 106-44-5 4-MethvtohenoI m t — 86-30-6 N-NitrosoOipnenytamrne (1 ) /r» ^ 621-64-7 N-Nuroso-Di-n-Proovlamme ;o M- 101-55-3 4-8romophenvl-ohenyletrier /C t*. 67-72-1 Hexacntoroernane /D t^_ 118-74-1 Hexachlorobenzene JC //- 98-95-3 Nitrobenzene ;O Xw 87-85-5 Pentachiorophenol ^"C L^ 78-59-1 Isophorone /O 4C 85-01-8 Phenamhrene /C iX_ 88-75-5 2-Nttroonenol /n LL. 120-12-7 Anthracene /O 6U 105-67-9 2, 4-Dtmethviorienol t D (u 84-74-2 Di-n-8utvbhthalate /O CL 65-85-0 Benzoic Acid TO w- 206-44-0 Fluorantnene 10 v^ 111-91-1 bis(-2-ChloroethoxvtMethane JO u- 92-37-5 Benztdtne ^r i^- 120-83-2 2. 4-Dichloroohenoi /O tv- 129-OO-0 Pyrene /o ^.^ 120-82-1 1, 2. 4-Tnchlorobenzene IO U 85-68-7 Butvibenzviprtrnaiate /C t-C 91-20-3 Napnthalene rO L^ 91-94-1 3. 3'-DicnloroOenziarne oiC ijL 106-47-8 4-Chforoaniime /r.) iv 56-55-3 BenrcxafAntriracene to i^ 87-68-3 Hexacniorobutadiene /Qu 117-81-7 bisi2-EtnvihexvDPntnaiate IO tV- 59-50-7 4-Chloro-3-Metriviprienol 10 f- 218-01-9 Chrvsene fu u* 91-57-6 2-WetnvinaDnirialcne 'O t\- 117-84-0 Di-n-Octvt Phthatate IO LL 77-47-4 Mexacniorocvciopeniadiene fO tL 205-99-2 BenzwbtFluoraninene in IL_ 88-06-2 2, 4. 6-Tnchloropnenol rO I.L 207-08-9 BenzcKkiFluorantnene tn U 95-95-1 2, d. 5-Tncniorophenoi •TC fL 50-32-8 Benzo Pesticide/PC 8s Concentration: lLow /Medium (Circle One) i-^ /. I Date F*tfart»rf/Pr»pap»rl-. ',!-•!• Date Analyzed: J.^AtT/S T * 11^-, x" Conc/Dil Factor: CAS C"g/ip* ug/Kg Number ") Circle One) 319-84-6 Aiona-BHC O.C5" t*- 319-85-7 Beta-SHC c.c.r u^ 319-86-8 Deltl-BHC C.JJ<1 L^ 53-39-9 Gamma-BHC (Linoanei O.C*T M_. 76-44-8 Heptacntor C.C.C M_ 309-00-2 Alarm r .o«r LI 1024-57-3 Heotacnior Eooxioe C^J? iA. 959-93-8 Endosuifan I r.CT L^ 6O-57-1 Djeidnn n. /d 6c 72-55-9 4. 4--ODE iC.ro tc- 72-20-S Endnn O,(O /x» 33213-65-9 Endosuifan 11 c- 1 <-; ^C 72-54-8 4. 4'-ODD C ^u /ju 7421-93-4 Endnn Aldehvfle r\ ' w '^— 1031-07-8 Endosutfan Sutfate r- (C IA 50-29-3 4. 4--DDT C fO t^ 72-43-5 Methoxvcrtior r-5t- ix_ 53494-70-5 Endnn Ketone ,' '. r C £A_ 57-74-9 Chlordane C.*5-o tr 8001 -35-2 Toxaohene l. O tv- 1 2674-: .-2 Aroctor-1016 /-, vO t^ 11104-28-2 Aroclor-1221 r . ^o W 11141-16-5 Aroctor-1232 o.^u 6^- 53469-21-9 Aroclor-1242 T-Vo lw 12672-29-6 Arocior-1248 C.VO Lt, 11O97-69-1 Aroctor-1254 t. o • ;( 11096-82-5 Aroclor-1260 1-0 KX Vj = Volume of extract injected {ul) V = Volume of water extracted (ml) Wg = Weight of sample extracted (3. V = Volume of total extract (ul. r.w.eecet*. Mwm.Wfen*ZUU f - 7 •*/ Organic* Analyst* Data Short C«*eNo; O 13 I - V ' QC Report W* ,______. Contract No: . C*te S«mp*e Receive* VoMteCompoundf. Medium (Circle One) VeeeiB Aekel ""^^ •^BV •£10 ee/Hi« «w taei inneeeifi i niiiii i IIIIM HM r • fiyRIO 4/IL Eampie Number P.O. HP tit. !••• ••,W>*«i2313 XQ/UT-WD Organics Anatytli Data Sh*«t (P»9t 2) SamtvoUttet Compounds Concantiaiion: Lew ^_^Sjym _ • (Orel* One) L-3I tt CA« Sample Number 22313 70J/M7-14IO , Organics Analysis Data Shaat Concentration: Low /^Mediuny (CircleOne) Data EKtrectad/Praparad: DataAnatyad:——3'A/-5Vg 5" Cone/Oil factor ——LJ.—————— CAS Number (Ctfde 11944-6 Alpne-VHC /rov 31S-9&.7 Beta-BNC «51Pu }i»46-a Delu-BHC tic* SeVB»'9 Oemnw-BHC (Undene) )2C,L 76-444 /IO^ J09-00-2 AWrin no** 1024.57-3 Heptachlor Epoaioe j'^.a^ W9-9S-8 EneoewKenl /z<\, BO-57.1 DieUrin yiw,, 72-55-9 4. 4--DDE •/ id.. 72.204 Endrin * fOu 33213-65.9 Endoeuttenl •*. y 50-29-3 4. 4--DOT VOCV ( 72-43-5 / ? Vj * Volume of ettrect infected (ul) Vf B Volume of water ectrected (ml) W( « Weight of sample enrected (Q) V( » Volume of touf eviract (ul) v. ______ Form! WVI V w ^ *--- 4'B4, Organics Analysis Data D 27 Environmental Protection Agency. CLP Sample Management Office. Sample Number P.O. 3ox318. Alexandria, Virginia 22313 703/557-2490 Organics Analysis Data Sheet (Page 2) Sermvok,tile Compounds Concentration: ( Low/ Medium (Circle One) ^^-^-^ ; . I „.. T Date AnalymH-_• t£>-»"7 j/ i/ °n fr v X ^r ^* Conc/Di[ F»Mnr" "lO O ' ——— N. S~ ——— N ^^•4o fV ug/ljrr ug/Kg CAS ( ug/lor ug/Kg PlUFT1O0r """"TCircta One) Number ^^TUirclft One) 62-75-9 N-Nttrosodirnejnviamine fO L<~ 83-32-9 Acenapnthenc /O -*^ 108-95-2 Phenol (0 fc 51-28-5 2, 4-Dinttrophenoi ,5"O ttta 62-53-3 Aniline /n [,<- 100 -O2 -7 4-Nitroonenol S'O ix. 1 1 1 -44-4 bis(-2-Chloroethvl)Ether /n to 132-64-9 Dibenzofuran fo t^ 95-57-8 2-Chloroohenol /D ;*~ 121-14-2 2, 4-OinitrorolLt0ne /o ^ 541-73-1 1 . 3-DichloroOenzene 1C IX_ 606-20-2 2. 6-Dinitrotofuene /O M_ 106-46-7 1. 4-Dichlorobenzene /C £*_ 84-66-2 Diethylpnrhatate tc »- 100-51-6 Benzvl Alcohol ir> L.^ 7005-72-3 4-Chlorppnenyt-phenyietner fC, u- 95-50-1 1. 2-Dichlorobenzene )n u- 86-73-7 Fluorane /O ;^_ 95-48-7 2-Metnvlohenol 'C l<- 100-01-6 4-NitroanHme Ct) ^ 39638-32-9 bts(2-chloroisoproDvMEther '0 Lv- 534-52-1 4, 6-Dmitro-2-Methytphenol S'O tx. 106-44-5 4-Metnvipnenol /O f •— 86-30-6 N-Nitrosodtpnenytamine ( 1 . /r* £— 621-64-7 N-Nitroso-Di-n-Propvlamme JO W- 101-55-3 4-8romopnenyl-pheny)emer /O /*. 67-72-1 Hexacnloroetnane /D U- 118-74-1 Hexachlorobenzene ;C (,4. 98-95-3 Nitrooenzene ;O fv 87-86-5 Peniachlorophenot ^'O tw 78-59-1 Jsopnorone /O it 85-01 -8 Phenanthrene /C t<_ 88-75-5 2-Nitropnenof f n w.r 120-12-7 Anthracene /O £,(_ 105-67-9 2. 4-Oimetnvlonenot / 0 (L 84-74-2 Di-n-Butvlphthalate /C 6L 65-85-0 Benzoic Acifl *rO K- 206-44-0 Fluoranthene /O to- 111-91.1 brs(-2-Ch(oroethoxv)Methane 10 LV_ 92-87-5 Benzidme .Tn uX- 120-83-2 2. 4-Oichtorophenot 'O t*- 129-00-0 Pyrene /O L<- 120-82-1 1. 2. 4-Tricniorooenzene fO Lv. 85-68-7 ButylPenzvlphthaiate /C tx. 91-20-3 Napnthalene /O Lk_ 91-94-1 3. 3"-DichJorooenzidme fJJC /C 106-47-8 4-Chtoroanilme 'O i^ 56-55-3 Benzo Pesticide/PC Ss Concentration: (tow /Medium (Circle One) Date Extracted/Prepared: . ' ?/^* / °^ i-» /-» ^ /O,L{ L Date Analyzed: _L Conc/Dil Factor CAS -. • I ug/lj* ug/Kg Nombeir v . TCircle) On«J 319-84-6 Afona-BHC O.C'S' &- 319-85-7 Seta-SHC r r,r L*- 319-86-8 Delta-BHC C.C* iX- 58-89-9 Gamma-BHC (Unoanei D.f.T iu- 76-4A-S Heptacntor C.cC /x. 309-00-2 Alarm r .(J^- LI 1024-57-3 Heotacnior Eooxioe C-C5" u. 9S9-98-8 Endosuifan l r.CT (>- 60-57-1 Dieiflnn Oi /Cy i-^- 72-55-9 4. 4--DDE iC- IO £C- 72-20-8 Endnn O.fO AU 33213-65-9 Enocsutfan n c- 1 o' u. 72-54-8 4. 4--DDD ft- IV AC. 7421-93-4 Endnn AWehvae n. fo *^ 1031-07-8 Endosuifan Sulfate r to /A 50-29-3 4, 4--DDT C 'O r *. 72-43-5 Methorychlor c-5<- 6c 53494-70-5 Endnn Ketone ,- ;. r c u. 57-74-9 Chiordane C.*ro ^ 8001-35-2 Toxaphene i. O tv_ 12674.11-2 ArocIor-1016 /-, VD £A_ 11104-28-2 Aroclor-1221 r.-^C W 11141.16-5 Aroclor-1232 C-^u t^ 53469-21-9 Aroctor-1242 r.Co to 12672-2S-6 AroclOr- 1 248 C- *ro t\^ 11O97-69-1 Arocior-1254 (.0 tl 11096-82-5 Aroclor-1260 1 • O" v^ V; 2 Volume of extract injected (ul) V. = Volume of water extracted (mil W = Weight of sample extracted (g) V. = Volume of tPtai extract (ul) A/A \ C. 73 Organic* Anatysls Data Sh*trt No. UbS.-g.PH* C73/;^—————— OCfUportN* SolL~______—— Counsel Woe - Drti fltlMM ftumoriMdfir ^^^JL^^ 0*t« S»rrt?*« R#c^v«± VoMto Compoundf. CAS *. OC/US * *» U » *. tOU eeee* CM wMhcate*eMVMM ft p | rt.Men.MiM H fl I A/fi r, 0*1 Oiganles Analysis Data Shaat (P»g«2) SambolstUa Compounds Law CAS gency. Sampfe 0. ftwSlt, AtMMrtnt. VWgMft 22313 703/U7-24SO Organics Analysis Data Shoat Concentration: Uw /Ittodiurh (Circle On*) ^——•".« /x /^,j O.U Extrwt«l/rV«p.r«d: D«t* An*tY2*d: _——.ll Conc/DU Factor: CAS (Ctrcto 319-B4-6 Aipha-BHC 319-BS-7 D«U-BHC IWU-BMC 7l 58-89-9 HeyHCMor 309-00-2 AUrin 1 024*57-3 HvptacMor EpOMd* EndotuHint W-57-t 72-S&-9 4, 4'-DD€ 72-20-i Endrin Endotuftonl 72-S44 4.4*4)00 7421-93-4 Endrin AibehyO* Endosutfan Suf at* 50-23-3 4.4'-OOT 72-43-5 M*thonchler Endrin Kcton* 57-74-t 9001-35-2 12674-11-2 Arodor-IOIfl 2 700 H 11104-28-2 Aroclof-1221 Aroelor-1232 53469-21-9 Aractof-1242 12672-29-6 Aroctor-1248 1 1097-69-1 Arockw-1254 1 1096-12-5 Aredor-1260 V- • Vo(um« o* «0r»ci ini«cttxt (ul) Vg « Votum* ol water attracted (mil W, * Weight of umptt •uractod V, ______orW, ——LL———— V, ^.-"i'"-——— V4 Environmental Protection Agencv. CLPSampfe Management OWice. Sampia Number P. O, Bo* 813. Alexandria. Virginia 22313 703/557-2490 Organics Analysis Data Sheet (Page!) Laboratory Name: Gulf South Research Institute Case No; Ou tab Sample fawn- T^D 31- QC Report Nc r *^*- Sample Matr *• FAJ^.TC^" Csntract No: 68-01-' U^^f Data Release AMthnrf«rt By 7&&>.S&~'&&4 Date Sample H«.i«*H. /^/V/?/ Volatile^pmp(5und« Concentration: (lowjMedium *Cir«;ie One) Date Extiacted/Preparei Date Ana ^ )t*4/ =^r) Conc/Di pH U •1,PC-^ Percent ftffti«tiir»- ,, /y,W /J A Percent f^tsUire (Decanted) •—•^ CAS <^ug/lyrug/Kp CAS f ug^or ug/Kg Number Numb«r ^""Tcirel« One I 74-87-3 Chforometnane ^0 L*- 79-34-5 1 1,2. 2-Tetracnioroemane 75-01-* Vinvi Chloride ;ri 0_ 10061-02-6 Trans-1. 3-Dtchloroofooene 5^ *A—r — 75-00-3 Cftiorwrnane 79-01-6 Tnchloroernene /r_J i*- *• ^f> 75-09-2 Mernviend Chlonae . S". ^ ^.>^ R —— • ^^ 124-48-1 Dibromocnioromethane 67-64-1 Acetone; 'O f^ 79-00-5 1.1, 2-Trtcnforo«inan* 75-15-0 Car&an Otsulfide Value IT tt%* reiutt is * wlu* gr*aivr man or equal to tnt C Thit (lag >DOli*t to oatHCiO* Mrametar* wn«r* .n« <— -, SMectton ttmtt. reeon tn* va'u* iO*nnfic*tion nat ee*n eonfirm«a BV GC 'MS Smgi* comoon*ni o*«ttc«*«« *!0 ng 'ul m trie hnaJ extract ftmort rn* mifttmum detection limit for tna tamine *»>tn trw u (• 5. TOUl datatf on n»e»sa*rv esncaniration' a Thit flag it u&*d wnen in« analyi* >• found m tn* etana •iiution actions (Th* ta net n*c*«»aniy in* innrumaw at «*n ti a tamoia n md«ai*« pe««»t* acwemn bmic J Th* faoirxjt* cnouid r*afl U- 6'"n« contamination ana w*m* trw data u»*f Cema^mS «•• anaiwatf *or *ot net MtaetM Tr» a«xeonate action iom atumaoie aetenton wnrf »e* preo*Mv d*(.n« o.( r««uftt H uWO t«** mutt M Environmema I Protection Agency. CLP Sample Management Office, Sample Number P.O. Box 318. Alexandria. Virginia 22313 703/557-2490 Organics Analysis Data Sheet (Page 2) Sernive**vtile Compounds Concentration: r^Low/ Medium (Circle One) Date Extracted/Prepareci- _LZ-/S--£I /Y¥- _ 1 ~2, D^te Analyred- L L/iJH ' Conc/Dil Fartnr- ^O O S~— — * CAS (^ ug/tflT og/Kg CAS (. ug/^or ug/Kg Number ' {Circle One) Number "*"• '("Circle Onal 62-75-9 N-Nitrosodtmethyiamine fO io 83-32-9 Acenaonthene /O ^ 108-95-2 Phenol to f^ 51-28-5 2. 4-Dmitrophenol SO **- 62-53-3 Aniline in L<~ 100-02-7 4-Nitroohenol S"O iA- 1 1 1 -AA-A bisf-2-ChloroemvliEther /n LL, 132-64-9 Dibenzofuran ^o t.*~ 95-57-8 2-Ctilorophenol 10 ^^ 121-14-2 2. 4-Dmitrotofuene fO ,^ 541-73-1 1. 3-Dichtor_obenzene fC M_ 606-20-2 2. 6-Dintfrotoluene IO u 1O6-46-7 1. 4-Dichtorobenzehe /C U. 84-66-2 Diethytphthalaie 10 I*- 100-51-6 Benzvl Alcohol in u^ 7005-72-3 4-Chloroohenvl -ohenviether /O Lw 95-50-1 1. 2-Dichlorobenzene in u. 86-73-7 Fluorene /O f^c 95-48-7 2-Methvlohenol /C u.. 100-01-6 4-Nitroanriine C?^ 6*- 39638-32-9 •brsQ-chlororsooroDvMEther '0 L^ 534-52-1 4. 6*Dinitro-2-Methyiphenol sS'O f,C 106-44-5 4-MethylDhenot ir\ t ^_ 86-30-6 N-NitrosoOiphenvlamme (1 ) /r» b- 621-64-7 N-Nitroso-Di-n-Propylamine ^0 U. 101-55-3 4-Bromophenyl -phenylether /C /^- 67-72-1 Hexachtoroetnane /n L^ 118-74-1 Hexachtorobenzene ;C /.<_ 98-95-3 Nitrobenzene fO to 87-86-5 Pemachtorophenoi ^"O u^ 78-59-1 Isophorone /O *c 85-01-8 Phenanthrene /C tx_ 88-75-5 2-Nttroonenol in t^ 120-12-7 Anthracene /O t<_ 105-67-9 2, 4-Dimethvipnenol /O |.L 84-74-2 Di-n-Butylphthalate /C CL 65-85-0 Benzoic Acid 5~0 w- 206-44 -O Fluoranthene /O LL^ 111-91-1 brs{-2-Chloroethoxv)Methane iO u- 92-87-5 Benzidme , Pesticide/PCBs Concentration: (LOW /Medium JCircle One) Dare Extracted/Prepared: j/^/_ y ^ /j °' Date Analyzed: I7-/20 Conc/DN Factor ___ 319-S4-6 Aiona-BHC O.c^- ex. 319-85-7 Btra-BHC c.cr 6^ 313-86-8 Defta-BHC c-e^ t<_ 58-89-9 Gamma-BHC (Linda nei O.C.S" ix_. 76-44-8 Heotacnior c.cC ^x 309-00-2 Alarm r.ccr u 1024-57-3 Heotacntor Eooxide C-C5" /x 959-98-8 Endosuifan l r.G?" L-^ 60-57-1 Dieiann ^,^0 /X 72-55-9 4, 4--ODE r:- (O to 72-20-8 Endnn O.fO /X 33213-65-9 Endosutfan lj (^-IU iC 72-54-8 4. 4'- ODD r Vj = Volume of extract injected (ul) Vs = Volume of water extracted (ml) ws = Weight of sample extracted (3) Vt s Volume of total extract (u!) U Ghest _ ,*_,___*>*-•'. - /*•' f-: :.- *" •-""" •''_ r^.•—.^.:^>^^^--"n~^—^•v-"-~*"J !< -'''"' I L-'-' _^'-* , -"-' V'C-ft! Ptrcsnt &**-w5.lur5 ^-cr'A * sT^A t?'r^*-;"''-5"'s-!1^--""^ ,"*~~ -r _-C," ».--'".'.. ^ "-* ->''l • L••" _•3_ J! V-l' v-'. *. •' ?. A C ? .' I',^^^' ._....' "^"i I'f- 1-. " - _-- * -~-_~ ~ -. . -' : - -- '--- -—- -;_-- .- .-- - ^^-. ^--iV. t. - '• ^ ' '- v"-^l'" - L il ' .*>•••.-! n -t '••• — -• . -- -- .- ..__... •" »r. "f~A"A *I. 3 O b ^ -. Of 11 i*t*iiiisiHMfMM. femple Number Organic* AntfysJs Data Sh*«t Compounds Mtdlum • (Cfrcte One) / ~/V* ^/<* /Z CAS Fermi O^S»mpe» S*mpto Number A*e«ndr*. Vienna 22313 7Q3/W7-J4iO Organics Analysis Data ShMt (Page 3} Concentration: Lgfltx Medium (Circle One) D*ttExtract*d/Pr«p»r*d: DawAnah/wt ———— ;4 Conc/DU Factor: CAS Number 319-84-6 Alpha-SHC z r-u 319.85-7 Beta-aHC ^.f»n 319-66-8 Defta-BHC *'?n 5S-89-9 CUmma-aHClUndane) s *i r*-' 76-44-S y r. 309-00-2 AWrin 7. Oh 1024-57-3 Haptacntor Epexida i. .Ow 959-90-8 EndoauHan 1 X,CL BO-57-1 DiekJrin V (^ 72-55-9 4. 4--DOE V.A. 72-20-8 Endrin V. 0^ 33213-65-9 Endoautfah i v n*. 72-54-8 4, 4'-000 v.f\ 7421-93-4 Endrin Aldahydt- V.(7c. 1031-07-8 EndotuHan Surtate y a. 50-29-3 4. 4'-ODT y.f>« 72-43-5 Met noii ^rwor yp.^t 53494-70-5 Endrin Ketone v,J/, 57-74-9 Chlordana -CO. 0i 8001 -35-2 Tonphena y3 ^ 12674-11-2 Aroclor-1016 ^£?W 11104-28-2 Aroctor-1221 *.' 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PAGNESJ.UP I 3t^C.3 P. AM IPCf'Y 22. UK P 14. PANGANtSE 3.7. ' A«SEb 1C ^^ F5i 15. Pe*«CU^Y c^ILP £ 126.3 p ib. MCKEL t iS. J P cfcPYLL IL* i.C L p 17. PCTASSIUP "tl.iC. P CACPJLP S'.C U p 1«. SELtMUH ,.__..5:0.iL f 7. CALCILP 533CC. p !•?. SILVER M.C Ut< P ChnCMlP 38. R p 20. secies LCHALT 7.C L p 21. TH4LL1U** to.U. F CCPPEfr 37. p 22. TIK 2C. UP P I^CN 2oCCC. p 23. £• S.I] P ^AC M, F^**i ^fL &^* SCLICS At PA -—L ££(/JU> &«ff— - - — n n \ t- I - ^APHCRP" I""'""" " ••—-——---—---••• - • ...... _. .„._____ : SAPFLc LC-AAM,H i*« v,i.. ^23IJ _ . "" . " ;>C i/7« h.T j: 3-t57-2lSL . — _ .:::• ;,_ „ .: -•-;«,..... ANALYSIS .=, - —...... CC KEPuST NC 034.CCCC ~~ - ~. r =_.._... _,i._. AT ICN : LCU _> PEDiLP M^TEh . SCIL . X SLluCt PG/KC CRY I. ALLPINLP ulfc-C. P Ij. PAGNESIUf i' 'j 't c . 3 P '. ANTIPCNY _...._ 23. ,U« P 14. PANCANtSE 2C » P 1. ARSENIC :.. 15. PEi^CUKY o.x u. ^*- t 58."3 P 16. MLKEL i C » \j P LI Lft l.C U P 17. POTASSIUM 4 j. 5 . u P T. LALCiLP t 305C.3 P IS. SIi_VEW 1.2 u P -*. ur-PCMLP 37. P 20. SGClUr- t 127. j P •">. uCEA'Ll " ~" "~7.j U P 21. THALLluP JO L) F 1**. CCPPtK 52. P 22. TIN C <;4.j K P _-.—__„_————•—.—-.—,———-_— «_.„_.——..«—»——— — ————.*— \T. i^CN "" 7 tic. P 23* VANACIUP C j.3.3 P i-. L~tt - - —— -—58. f£ "- 2INC ^7^- p U PE«CLNT SCLICS i: Stt CCvEP PAGE. FCXr ! Ur. '•'M CClUrACT LALL-i-AltrY t^J^AM iil- - At.rxAM.fUt v«. <^313 " Tr C ANALYSIS CC KtPuKT NC C34.CCCC EATO -'lit ENTS UENTlFIfcu LLX , X PEDILP SLIL X P.G/Kt D^r ^t P 13. MNTIKMr 12. US P 14. r ANGANtiSF C i . 5 1 M 7. 4*5fcMC F ID. «KCUaY - - ... ____ .Jfc&. o.vu.^r cAML-P i. 4.c) p lo. MCKtL v.^i u P •:. saSYLULn C.53 U p 17. FCTASS1UP ill. 0 P CAtPlL> 2.G L p Id. SELEMurt £,(£ \) F uALCILP £ 37.3 P 1-3. SlLVEk ,.1 0 .P OPCr ILP 6.C p 2C. SCLIUP ite. u H V.L5ALT 3.7 U p 21. Tt-ALLlUh ^5.5 U F , uCPPES i 2.73 p 22. TIN 11. UK P . l^CN •*14C. p 23. V^ACl.P I C-lj P . ,EAE: ^4. 21NC [ D.1J P .__._ ___.Q^O_ F: LYAMCE u HLhCEM SCtlLS ^H.^ "LCTNCTES: SLt CCVcK r ,A'j - -. .. _...... f CHr* "I C C J. I f "2 C f LAcCf*rC?"Y ? 5 .j 0 S £-,»- • "" ...... NAGCPFM Crf-ICt ! _ ".Z- - - .1. - . : S_ArK = NC. FT:>: --557-249L AN U AN*LYTi5 -DATA C. Nu. So3 ; -" ------— :-: -cc R3PCRT NL. ELtMENTS lUENTIFIEb AUC X. PEU1LP " SCIL X SLCCGi: PG/KG C.KY ^ . . „ 1. ALLP1NLP . iSfcC. P 13. P/GNESIUP L 12c.]' P "». ANTIPChY 12. UR P ...... 14. f-A.NGANcSE il. P '*. sAKicp t T.I'I P 16.""NICKEL t.2 u f1 •* ^ •» ^ *» ^ ^ ^ ^ ^ ^^B^ ^ ^ ^^B-^^B ^^-^»^k-^ta^» r -- ^ ^-^-^^ ^*^» ^ ^ ^ ^»*^*» ^ ^ ^ ^ ^ ^ ^ ^^»«*4k»^M ^. cE«YLLILP- C.53. U P 17. PCTAiSiU?' 2*c. u P S. LALMLP 2,7 U P IB. SELENIoP ~f. CALC3L^ £10^.3 P lv. SILVER ^. 2 o P ^. Lh"CMLP 11. P 20, SCLlLP I i'^.3 P ">, CCPALl 3.G U P 21. ThALLlOP S ±0 F I'1. CCPPfcS i 7.c3 P 22. TIN 11. Ji* ? n. 1SGN j;75C. P 23. VANACIUP f t. e ] P 1 '. LEAL' i^ ffjg 24. ZINC C/.13 P CYANjCE " O-Z4" U " --—-PEnCENT SGLICS ^\^\ cLCTNLlf-i: SEi" CCtEk HAGE'.. :_=1.. - ...... _ ...... rCK" I LAhCfAfCKY HFOGfcAP ...... cF>ICfc . s-.SArFLt NC. AiNLRiH, VA. 22313 "" ";i^C <«77? t ANALYSIS L^TA bf-EtT —— LAO *|**c VtfSA* INC. CASE M/." JfrCj" '' Lc IL. NL« 9j*» S 5 4 CC kc?LRT NC '-TASK tf34.CCCC "' HATCH 17'j «**w ••^••B wt ^ •* ^ «b ^^B ^ vb M ^^ ^.^ < ELcPENTS ICENTIFItU :-^s LCh )( PEOILP WTER > SLIL SLLCGE • • LC/L »p ALLPINLP X i C U 4 ^ 13. _PAiiNESIUP- i. 3HOC.3 I ANTiPC^Y 22. Dft p 14. fANGANcSE 121F. ASStMC f. 15. PfcHCtHY o.*i ... __ .Jfi^.^ uAFHP i 53.3 p 16. NICKEL i5. C P cfcFYLLILP l.C U p 17. PC7ASS1UP £ 22CC.J P p CACPILP 5.C U Id..-.—_—.SELENIUP . — __^ StiLJ ^ .21 F LALC3LP 198CC. p 19. SILVER H_. CUH p LhfiCMLP i. c.c3 R p 20. SCCICfl 124CC. p CCEALT 7.C L' p 21, ThALLIuP 10,0f . CCPPfcK L 11.3 p 22. TIN tC» Ow * iSCN 357C. p 23. VANACILP 3.0 u H L&AL . __ ji^—F* 24. 2UC l£ . 22313 _ :PC 477.; " ANALYSIS C^TA ihb CC PbPCST i^C r^'-TASK o34.cccc -- - " - =- - I^TCH i?e ELcPENTS ICE'MlFJfcL AMJ PECILP SLIL X CRY 1. ALLPlhLP . 55C. P 13. PAGN8S1UP E ^5.3 P ">. ANTIPCNY 14.- UK P . 14 ." PANGANcSE I. o.l J P *. cASUf1. .".'. _. ' i 2.11 P 16. MChtL S.4 u P *j.~ &EKYLLRK C.63 U P 17. PCTASSIUP 2:>C. O P *«. C'ACPILP 3.i L1 P IS. Sbi-EMtM —-&L1L * ?. CALC3CP £ €5.3 P H. SILVER 2 . 5 u P •^. Cr-^CPlLP "." - "2.5 U - P 20. SCLIUP- i S . u P °. COBALT 4.4 U P 21. THALLlL'fl 6-2 d F "22. TIN i3. UH P 2 3 .V- A r. A D 1 0 -w i.S u P 24. t il.l F U " " PEKCtNT SGLKS he CLVcJi rAGr. " rCS" i A1C?Y PfiCOSAP CFUCG IA, VA. 22313 It ANALYSIS CA'TA 5r-nb. = 5- SAx INC, "" CA.iF Nu. D34.CCCC BATCH IVfi ELcPENFS iLtNTIFIEu ANU fEASL'PtD LLt~ X P.EOILP * SCIL SLLCGE UG/L 1. ALLMM>iLLP^LPP LLZ7. 27. 3 *PP 13. PAGNESIUP ANTIPCNY 52. LK P 1^. PANGANESE I 11.3 AiiSEMC u P* 15. PE*CUKY O.VU. oAPKP i 6.7 3 P 16. MCKEL 1.5. u P ctSYLLUr l.C U P 17. PCIASSIUP L 2±^t.) P **. CACPILCACPILPP 5.5.00 U U PP 13. SELENIUM c ^ jl f uALC IL^ cuSCC. p 19. SILVER " 4~.C Jrf P Lr-PCf UP 4.0 LK P 20. SCuIUP 173UC. t3 CCPALT 7.c L P 21. TMLLIuP \0, VJL f CLPPfc* L 11. 3 P 22. TIt> . *:C. c« ? Z-ECN 445. P ?3.--V4.\ACIuP j.C C P L£AC r-^M fC. 24. 2INC /5. P LYAMCE 5.OUH PEKCFNT SOL1CS Ss Stt""CCvEJ PAGE. CFt-ICt . .. .._.. --_•- ; ' -' : Sft.*fL3 IA. .Vi. _2231'3.v,.. ...,....,,.._ ...... _...... :WC 47 PC uATr Ci-it-ci ANALYSIS" OAT/ ihEET ———————• IN,. " :." . .~"~ ;-;-—-- CC acP.PT NC. 3J4.CCCC EATCh 17S ELcPENTS ICENTIFItu PECILP SLlL X SLLCGc C*Y HEIGHT 13.- PAONESIUP t 125.3 ? •>. ANTIPCNY 15. U'R P .. _.. _14. PANGANtSt S.4. P T. AkSEMC ^.^ U f 15' ^£*CUKf o.V UU*- '4. dAPTLT L 7.13 P lo. MCKfcL ^0. u P c;. LECYLLILil C.6S U P 17. POTASSIUP 277. 0 ? n. CACPILP' 3.5 U P IS. SELEMuP 350 7. C^LCiLP t fcC2.3 P 19. SILVER , *.fl u P **. ChKCMLP . {. 3.c3 P 20. SCLIUfl [ ^^.i P ^. LLHALT 4.S U P 21. ThaLLlUP foCf ^ f Li. cLFPtP 2.1.-U P 22. TIN C 21.] X P 1.1. iRCN 112CC. P _. _.23. VANAOIU.M [ c.^>3 P 1. "*. uFAC " ". V O fj? 24.7INC j3. P CYAMCE - FF^CENT SCLlCS LA-. P i N A11 ft F C A M I LAfcL&AfC'Y ?=Lu*AP LFt-ICl _,AT|: Cirli-c? INLkuAMt. ANALYSIS • CAT* ihEET . - — --——— ,_*n SR"«L_. It. NL. <541 9*6 CC KEP'CkT NC. i76 o!>n fc--.TA5K «34.CCCC EATCH 1?« ILENTirlEC ANC X PEDILP SLlL SLLCG£ LC-/L 1. ALLPINLP lo4CC. *P 13. PAGNeStUP. 731C. H *. ANTIPCNY , Z2. US P i4. PANGANcSE ' 2 *F 6 " 41 ** !!:!!.l.——.-._o._J- 15. PE^CURY 0.4 i. cARILP Z29. P It. MCKcL 15. o P ccSYLLILW L J.S J p 17. PCTtfSSiuP L 2 3 7 C . 1 P CACPILP 5.C U p Id. StLEMuP .-ja-ao. p CALCJCP 4o3GO. p 19. SlLVck 4.C u« P Lr-FGP ILf- 2C.. ^ p 2C. SCL'IUP, 3tlC. ? CC&AL1 7.L U p 21. ThALLIUP 40. U. f LCFPEP I 16.1 P 22. TUs 4C. u« P i*CN IbcCC. p 23. VANACICP . r 37.1 P LEAD 24. 2INC ijj. P . ___ _30^r.F LYANlCS ^.^ u[R PERCENT SCLIUS Set LiF: «^{.^^sY-f— -, I £ Lu FC~'P I CLMFACI LAfcOATCSY" P^JS-Aft . :...;..„...... "ANAGcPtNT Url-ICfc ' . . • SA^PLc M IM, W. 22313 . :VC 4..si iN-LYSIS b/TA ihEc! ---•--••— - . -vt f* r f ^^ A.^^^^^ ^^^ ^ ri.^' '-TASK 034.CCCC ' BATCh l/£ fL-PENTS IC£NTIFI£L AM- PbASUkcC CN: LtV *x PED1LP *ATtS SCIL X SLuLGE P.G/Kb CKY VEIGhT 1. ALLPINLP ^5<;0. P 13. PAC-NSSIUP I Ir3.) P ?. ANTIPCNY 21. Lrt P 14. PAhGANcSE - .£ 4.cl P '. AtScKIC QlU F 15* PchCUKY 0,X U.^ 4. cAk'lLC t 1C.3 P 16. NICKEL 1^- :-J H .^, cbHYLLKrt C.So L P 17. PGTASSIUP job. u P «.. CACPJL> .._ . .._j4.s)_.L_ P ._...... l.^..r StLfcNluP 4.^0 f 7. CALCILf* C ^1.70.3 P ' .19. SlLVga i.9 u P a. Cr-FGMLP 3.^ U P 20* SCLlL.1 £^« u F i. CCHALT fa.c i- P 21. Tt-ALLii;* 9 "7/; f Tn. CCPPtF 2.*» L P 22, TIN IS, uK P li, IKCN _..fc3C.;. .P. 23. VANADIur I J.ol P _ __ __<-_^^^_-—^—_-_ __^_-__—»——^ — — — ^— — ...— . . —._»_ __^.—^_—_—^ 1'. L£AC • •'• A\ f^ 24. ZIiNC L iC.l P CYAN3CE 0.4-3 U. PERCENT SQL ICS g\,^ -UGTNL7E5; Set CC»l;K "PAGI, -erfEMS: . ^AxrlfL- FCKM I CCMJ-ACT IJILJ-ATLFY PSCu&AP ...... CrJ-KE • " ; SA.-FL= NC. n, >A. 2^313 . • "i?C 47*3 ANALYSIS UAT* si-rcr CAifc S^M»Lt It. NL-. 942 957 CC ftEPL^T Nil. C34.CCCC EATCH l.c • «M»*4*^W-»«4»-» M-fr »-M* t cLcPENTS UtNTiFIcC X PEORP SC1L S UG/L 1. ALLPINLP i 43.3 »P 13. PAUNESIU^ I sl.l ''. ANT1PCNY 22. LiJ P 14. PANGANcSE " i.C u '*. dflsiip i.o L P 16. MLKEL is. o r> ^. cr^YLLTLrt I.C U P 17. PClASStUP 4CC. u H *-. cACPRP 5.C L P Ifc. SELEMUP 5 *> \J f LALC3LP L 49.3 P 19. SlLVr* "" H.C u-C P *. uhKCMLP 4.C UR P 20. SC.IbP 3C. u P ^. CCHAL1 7.0 L P 21. Tl-ALLIUM 4O, U. f l^. CCPPhP 3.0 L P ' 22. TIN tC. UK P ^. If^CN t 24.3 P "~ 23. ^ANAuiur " i.C u ? I'. utAC r-^M^fl " 24.2^C f!2.J P r>ACc •I.-. -*M CCMP/CT LAcOATCFY "PS'ilC^i"* s^«o«_r '^NatitPtM CrUCE ... """"" .°.">. "!nv tlo - ALrxa.NLHlAi VA. 223U 7i->/eiK--(:^SC rTj: c-it 7-2 4 ^'u " . " JATF ANALYSES UJT4 iHfctI CAbh No. r>on JC-T_ j-ASK 034.CCCC —— •- — -- --.-.,. ^j--— ELnPcNTS ILC'NTIFIEL ANu KJ=ASU«cC LLW X PEHICP SLIL X S HG/KC DRY I. ALLPiNLP S.p U P 13* PAGNE3IUP C <:.43 P '. ANTIPCNY 11. US P 14. PANGANcSE O.tC u P 15. PESCURY 0.1 1C* A. cAKILt C.5CU P 16. NICKEL f . 3 U r S, btRYLLJUtt C.5C U P 17. PUTASStU" 2 CC . 0 r" *». CACPJLP . .2.5 U P ia. SELENIUM AS a F f •>. LALC3LP L 12.3 P 19. SILVER 2 .C u P *. CKRCMLP " 2.C U P 20. SCLILP. 15. u ? n. CCEALT 3.2 U P 21. ThALLluP 4<2 t? F I"1. CCPPfcfr l.s U P 22."TIN 1C. u* P I1- 1-CN -~"~~"T"fc.c3 "P 23. VANACIuP. i.b - " P P . p I"*. LEAD \?"5" U 24. ZINC _.. — . CYAMCE 0.25'LL FE-KCENT SQLICS loo -LCTNL1ES: S.£h CC»cR HAGt. PAXrIKLu • r C *_* I •> CC:.I>*CI L AtCWrc* r P^U-TAP '«,«N*(HfEM ChMCr v -i,. - *LcX£NL*-IA, Vj. > INL b. 943 CC Stf'L.-iT I^L 034.CCCL EAICH l/l rvt WTEP / SCIL SLLCGt LG/i_ 1. ALLPiMP 914. *p 13. fACNESiOP i I7jC.3 P -, ANTIKNY 22. UK p 14. PANCANLSE . *4. P 15. P£KCL*Y 0.% £. ^AULP " " L 3 C . 3 p It. MCKfcL i5» " u P * . eEKYLl'JXr I.C U p 17. PC1ASSIUP £ licC.3 P <*. CACPKP 5.o p Id. SELfcMbP 3,0 i; F II •' ' ' . H •*. CALC1LP 2VCCC. p IS. SlLVfcK *1 . \J LhPCMLP i45C. K• p 20. SCLIUM Sc?C. H ^ CCEALT 7.C U p 2i. Th.LLIoP 10. UL F l^. CCPfcf I 3.cJ p .*. TIN JC . u* p I'. IPCN luOCC. p 23. VANACIuP .77. P 1"*. ucAH So U f R 24. ZINC .c. p * t PEKCfcKT "SGi. Ics - LCTNCTES: Sc£ CC^cK r LAG rCK^ I LAcLKATlKY PVCOfi^P CF.flCf- - - - ..... L-AT| 1C ANALYSIS UAT4 ^^£L^ INL- CA-L NC. CC KEPuKT NC* i?-j BATCH l?g LL. U X PECRP ] A TO TV. , , ,- ,. . ._...._ _. - r • **"*• > - S LG/L 1. ALLP1NLP I tO*3 *P 13. PAGKLSILP L l^tdj P ^. a^TI/'C^Y " 12. L'R P 14. PANGANtiE 153. P T. ^tS£f-3C JO.U ""f* l5' ^EKCURr O.X U. 4. tiAKlLP £ 2fc.3 .....P . 16. .MLKEL i5. u P trcf-'YiLUP — — x^c ^ -p 17. IASS1UP S5sC. P wACPKP 5.C t • P 13. SELENluP 5 O CJ CALCIO 225CO, P IS. SILVcR *t.C Uft H Ll-HC"PUP 4.u US P 20. SGCICH 7740. f CCHAL1 7,C L1 P 21. TfALLlUP 1O» U. F cCPPfcS" "~~~^J7C~ l P "~ 22. TIN t£. u^ P 1£CN ill. P 23. V^NAUIUf* j.C U P -LY*NJC-E- - MR "pfciCENT SCLICS' S: $±t ccvtR LAH Cf-l-ICt . : SifPLS NC. X£l*EhUt v_. 22313 ifC=47t!7 ' - JATt" C1-15--5 ANALYSIS DATA ihfcET ————————• M^«T vt?5A« IN*.. CASE Nc. ~2fcC MO. 7 a 4 SAM"ui- U. ^. Sn5 : • CC SEPCHT NC. 1-34.CCCC tATCH I7e ELnPENTS ICENTiFIEC ANL PEDILP TV. ^THR X SLl L 5LLCG = CG/L I. ALL^ULP 336¥p . 13. PAONESIUP 63«iC. P . "• !!I^!L______!f:_ Uft P 14. PANGANdSE 3j7. P 15. P£* *. rAfi ILP i 44, J P 16. MCKtL 15. C P *. ^YLLIL* l.c U P 17. PCIASSILP 72^C. F S. CACP1LP 5.C U P l^.JELcNIUP ______5j2.iL f 7. I.ALCUP lo2GC. p IS. SILS-E* 4.C UK P a. Li-XCMIP 6S. X P 20. SCLIUP. fc?2C. P •», CCPALT 7.C U P 21. TI-ALLIUi* \Qtu. F 11. LCPPcS 3.C U P 22. TIN iO. b« P CO ——————————————————————— U3 I1 . i^CN ^t9C. p 23. VANACIuP J.O U P ^J- ————————————————————————— CD m P PERCENT SCuILS ___,._,4R . ... ______•___ PS: Set tCvc* ^AGc. LAc ft Ft *y v. (V ^ '-*. PAXr IMLJS CORPORATION 332 OLD EAGLE'seHaai- R'bAOTSuiTe's'i B" WAYNE. PENNSYLVANIA 1 9OS7 " ' 215-BS7-S51O . . . '" -^ ----:; March 20, 1986 R-585-8-5,.30 68-01-6699 Mr. Harold Byer U.S. Environmental Protection Agency 841 Chestnut Building Ninth and Chestnut Streets Philadelphia, PA 19107 Subject: Peer Review Comments TDD No. F3-8408-08 Saunders Supply Chuckatuck, Virginia Dear Mr. Byer: Submitted herewith are the responses to the peer review comments for the subject project. The following changes and clarifications have been made within the report: " " '" ' ------—- - - - o Typographical errors have been corrected, and grammatical changes have been made where appropriate. o . proper technical reference to dioxin sampling was inserted in regard to section 1.2. o Hazard Ranking System (HRS) (reference no. 4) information has been added to section 2.4. o In regard to section 2.6, information concerning permit issue and testing were added to this section. o Pond and intake distances from the facility were included in section 3.1. Additionally, a statement clarifying that Godwins Mill pond is also known as Crumps Mill pond was added. o Section 3.7 has been rewritten to agree with the HRS. o HRS (reference no. 4) information dealing with waste quantity produced has been added to section 4.0. o Proper technical reference to dioxin sampling was inserted into section 5.1. A Halliburton c°m*w &B . G 0 U 6 U Mr. Harold Byer U.S. Environmental Protection Agency March 20, 1986 - Page 2 Saunders Supply Company Peer Review Comments Letter o The appropriate changes have been made to the Site Inspection Form. If you have any further questions, please contact me. Respectfully submitted, Reviewed by, Martin Howe Richard Cromer Garth Glenn Hydrogeologist Assistant Manager Jftanager, FIT III MH/kf NUS CORPORATION UNITED STATES ENVIRONMENTAL PROTECTION AGENCY - - REGION III 841 Chestnut Building W-jI Philadelphia, Pennsylvania 19107 SUBJECT:Request Assistance from FIT Office 7~ ~ DATE: 7. (/1 FROM: Darius Ostrauskas, Environmental Scientist Site Investigation & Support Section (3HW23) TO: Butch Byer, FIT Regional Project Officer Site Investigation and Support Section (3HW23) I. SITE NAME: II. LOCATION: HI. WORK ASSIGNMENT: Slt"!nKectlon - ————— Qualltl *"«•»« "-lew of Data Har«d£S%«, ————— Re-Sampling/Full Field Investigation ToxicologToxicoloyv Assessmen7 t ....__. other (See VI below) Enforcement Support ————— T7 , IV. PRIORITY V. Preferred Deadline High (*) ,: .. _. Medium EXPLANATION OF TASK (* To include justification for high priority): \y s* VII. To be completed by FIT RPO only:. Task complete date by FIT: Hours allocated:... t, 2 I G „ ^^ + ~V ^ ^ *^ ' >«r.s-t-c^fj~t -S",7" o - &&&*.--?. S^.oo p- d fr October 10, 1984 ™ To: FILE From: Darius Ostrauskas Subject: Saunders Supply Company Yesterday, I inspected the above site and spoke with Mr. F.D. Howell, Jr., Vice President of the facility. He stated the following at that tiae: - vood was f ••••••£ with pentachlorophenol (PCP) on-site between 1964 and 1974 - between 1964 and 1974, 1000 gallons of PCP sludge were generated per year and all of the sludge was disposed of on-site * disposal consisted of burning the sludge along with wood scraps in a pit on. site — in 1974, the facility began treating wood with chromated copper arsenate solution and started to slowly phase out the use of PCP - from 1974 to 1984, all PCP sludge was disposed of off-*ite by J & L Industries of Newport News, VA - frost 1964 to 1974, liquids separated from the PCP sludge were dis- charged into an on-site wastewater pond (during the inspection this pond was observed by D*0. to have a discharge pipe leading to an intermittent stream adjacent to the site) - sludge was separated from liquid on-site in at least 2 tanks - one tank had a capacity of 1000 gallons and was filled with what was identified as PCP sludge if the time of the inspection) NUS CORPORATION 332 OLD EAGLE SCHOOL ROAD. SU'lTE 31 B' WAYNE. PENNSYLVANIA 1 gd@7 " '" " '' 215-GB7-S51O -. -. '- -=:~ '.W^ .'":">-4-= March 20, 19S6 R-5S5-S-5-3Q 68-01-6699 Mr. Harold Byer U.S. Environmental Protection Agency 8*1 Chestnut Building Ninth and Chestnut Streets Philadelphia, PA 19107 Subject: Final Report TDD No. F3-8W8-08 Saunders. Supply Chuckatuck, Virginia Dear Mr. Byer: Submitted herewith is a final Site Inspection report for the subject project. Based on our review of available data, we have concluded that EPA should consider the following: • ... o A program of continued monitoring of Godwins Mill Pond Reservoir for organic and inorganic compounds should be implemented. o A program of continued monitoring of "the Keliey well and monitoring well system should also be implemented. . _ . . o Runoff from both the process area and the hardware store area should be controlled. o Air sampling for particulates (i.e., chromium and dioxins) should be conducted. •• - - o Remaining waste sludge and dioxin-contaminated soil should be removed and disposed and/or isolated. Saunders Supply Company is an active facility which began treating wood with pentachlorophenol (PQP) in 1964. :In 1970, they began also using chromated- copper-arsenate (CCA), and have been using CCA exclusively since 1984. Waste chemicals consisting of PCP, CCA, and no. 2 fuel oil were burned in a shallow surface pit as a means of disposal. In 1981, Ronald Keliey, of the neighboring Kelley's Nursery, complained to health officials that he was finding an oil liquid in post holes on his property. The Virginia State Health Department and Virginia State Water Control Board (VA SWCB) began an investigation which led them to conclude that the burn pit was the source of most of the contamination. Subsequently, Saunders had a monitoring well and recovery system installed, in addition to removing the noticeably contaminated soil from the burn pit. A Halliburton Company Mr. Harold Byer U.S. Environmental Protection Agency March 20, 19S6-Page2 Saunders Supply Final Site Inspection Report FIT III conducted a sampling of soil from auger holes adjacent to the burn pit. These samples were analyzed for all isomers of dioxin. The FIT also conducted a routine environmental sampling of the site, the surrounding area, Godwins Mill Pond Reservoir, and a monitoring well system for the burn pit. The results of these analyses can be found in appendix E and section 6.0, respectively. A release of contamination from the site to the groundwater has been established by the sample results. A release to the surface water is strongly suggested, although no substantiation for PCP found in the upstream sample has been determined. This, however, indicates that runoff from the Saunders Supply Hardware Store area may be carrying chemicals from the wood products to the tributary. Further investigation in this regard may be warranted. A toxicologicai evaluation of the site identifies numerous potential health threats to local residents and to those who consume water from Godwins Mill Pond. A complete review of .the toxicologicai impact of the site may be found in section 7.0. Presently, there are small quantities of waste sludges being held on the site in tanks and drums. It appears from the auger samples that additional soil, extent unknown, is contaminated with dioxin compounds outside the burn pit. Soil excavated from the pit by Saunders was taken to the John C. Holland Landfill (VA- 177) for disposal and should be screened for dioxin compounds. NUS has submitted a Hazard Ranking System (HRS) model to EPA for this site with a score-of 45*95. NUS is presently conducting a dioxin extent of contamination study* If you have any further questions, please contact me. Respectfully submitted, Reviewed by, Approved b Martin Howe Richard Cromer Garth Glenn Hydrogeologist Assistant Manager Wlanager, FIT III MH/kf NUS CORPORATJOIM