Synthesis of Morpholine and Derivatives Thereof Via the Reaction of Dialkylene Glycol and Ammonia
Europaisches Patentamt J» European Patent Office © Publication number: 0036 331 B2 Office europeen des brevets NEW EUROPEAN PATENT SPECIFICATION Date of publication of the new patent specification: mtci C07D 295/02 18.10.89 Application number: 81301126.9 Date of filing: 17.03.81 Synthesis of morpholine and derivatives thereof via the reaction of dialkylene glycol and ammonia. Priority: 17.03.80 US 130782 © Proprietor: AIR PRODUCTS AND CHEMICALS, INC., P.O. Box 538, Allentown, Pennsylvania 18105 (US) Date of publication of application : 23.09.81 Bulletin 81/38 Inventor: Daughenbaugh, Randall Jay, Box 334A, RD No. 1 Barton, PA 19505 (US) Inventor: Dixon, Dale David, Box 53D RD No. 2, @ Publication of the grant of the patent : Kutztown, PA 19530 (US) 01 .08.84 Bulletin 84/31 Inventor: Fowlkes, Robert Lee, 220 Cedar Street, Milton Florida 32570 (US) @ Mention of the opposition decision : 18.10.89 Bulletin 89/42 Representative: Burford, Anthony Frederick et al, W.H. Beck, Greener & Co. 7 Stone Buildings Lincoln's Inn, London WC2A3SZ(GB) Designated Contracting States: AT BE CH DE FR GB IT LI LU NL SE References cited - DE-A-2738115 DE-A-2 758 769 Cfi DE-C- 1 941 633 DE-C-2 040 507 SU-A-175 512 CO US-A-3151 112 US-A-3154 544 O CHEMICAL ABSTRACTS, vol. 75, no. 23, December 6. <0 1971, oage 327, abstract 140871h. COLUMBUS, OHIO O (US) o Q. Ill ACTORUM AG EP 0036 331 B2 Description carrying out the process the reactants are charged to an autoclave and reacted at 240°C and Technical field 25x105 Pa (25 atmospheres) in the presence of This invention relates to an improved process for hydrogen.
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