University of Central Florida STARS Retrospective Theses and Dissertations 1978 Synthesis and Flame Retardant Studies of Bromoester of 2,4-Pentadienoic Acid Hessam Ghane University of Central Florida Part of the Chemistry Commons Find similar works at: https://stars.library.ucf.edu/rtd University of Central Florida Libraries http://library.ucf.edu This Masters Thesis (Open Access) is brought to you for free and open access by STARS. It has been accepted for inclusion in Retrospective Theses and Dissertations by an authorized administrator of STARS. For more information, please contact
[email protected]. STARS Citation Ghane, Hessam, "Synthesis and Flame Retardant Studies of Bromoester of 2,4-Pentadienoic Acid" (1978). Retrospective Theses and Dissertations. 288. https://stars.library.ucf.edu/rtd/288 3YNTHESIS AND FLAME RETARDANT STUDIES OF BROIDESTER OF 2,4- ?ENTADIENOIC ACID BY HESS.4M GHANE B.S., National University of Iran, 1974 RESEARCH REPORT Submitted in partial fulfillment of the requirements for the degree of Master of SCience: Industrial Chemistr,y in the Graduate Studies Program of the College of Natural Sciences of Florida Technological University . Sunmer QUarter 1978 ABSTRACT The synthesis and fire retardancy of several bromoeste~ of 2,4-pentadienoic acid were investigated. The synthesis of 2,4 entadienoic acid was accomplished by liquid phase re- action of acrolein and malonic acid in the presence of pyridine. The conversion of the acid to bromoesters was performed by two different procedures. In the first procedure, the corres- ponding acid chloride was prepared from the acid via reaction 0 with 30Cl2 in the presence of powdered (3A ) molecular sieves.