An Early Medieval Lead-Smelting Bole from Banc Tynddol, Cwmystwyth, Ceredigion
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Some Problems and Potentials of the Study of Cupellation
Some problems and potentials of the study of cupellation remains: the case of post-medieval Montbéliard, France Marcos Martinon-Torres, Nicolas Thomas, Thilo Rehren, Aude Mongiatti To cite this version: Marcos Martinon-Torres, Nicolas Thomas, Thilo Rehren, Aude Mongiatti. Some problems and po- tentials of the study of cupellation remains: the case of post-medieval Montbéliard, France. Archeo- sciences, revue d’Archéométrie, G.M.P.C.A./Presses universitaires de Rennes, 2008, pp.59-70. halshs- 00599974 HAL Id: halshs-00599974 https://halshs.archives-ouvertes.fr/halshs-00599974 Submitted on 19 Jun 2011 HAL is a multi-disciplinary open access L’archive ouverte pluridisciplinaire HAL, est archive for the deposit and dissemination of sci- destinée au dépôt et à la diffusion de documents entific research documents, whether they are pub- scientifiques de niveau recherche, publiés ou non, lished or not. The documents may come from émanant des établissements d’enseignement et de teaching and research institutions in France or recherche français ou étrangers, des laboratoires abroad, or from public or private research centers. publics ou privés. Some problems and potentials of the study of cupellation remains: the case of early modern Montbéliard, France Problèmes et perspectives à partir de l’étude des vestiges archéologiques issus de la coupellation : l’exemple du site de Montbéliard (France) Marcos Martinón-Torres*, Nicolas Thomas**, Thilo Rehren*, and Aude Mongiatti* Abstract: Bone-ash cupels are increasingly identified in medieval and later archaeological contexts related to the refining of noble metals in alchemy, assaying, jewellery or coin minting. These small finds may provide information on metal refining activities, the technical knowledge of different craftspeople, and the versatility of laboratory practices, which often differed from the standard protocols recorded in metallurgical treatises. -
Effects of Varied Process Parameters on Froth Flotation Efficiency: a Case Study of Itakpe Iron Ore
Nigerian Journal of Technology (NIJOTECH) Vol. 39, No. 3, July 2020, pp. 807 – 815 Copyright© Faculty of Engineering, University of Nigeria, Nsukka, Print ISSN: 0331-8443, Electronic ISSN: 2467-8821 www.nijotech.com http://dx.doi.org/10.4314/njt.v39i3.21 EFFECTS OF VARIED PROCESS PARAMETERS ON FROTH FLOTATION EFFICIENCY: A CASE STUDY OF ITAKPE IRON ORE S. Akande1, E. O. Ajaka2, O. O. Alabi3 and T. A. Olatunji4,* 1, 2, DEPARTMENT OF MINING ENGINEERING, FEDERAL UNIV. OF TECHNOLOGY, AKURE, ONDO STATE, NIGERIA 3, 4, DEPT. OF MET. & MATERIALS ENGINEERING, FEDERAL UNIV. OF TECHNOLOGY, AKURE, ONDO STATE, NIGERIA Email addresses: 1 [email protected], 2 [email protected], 3 [email protected], 4 [email protected] ABSTRACT The dire need for Itakpe iron ore concentrates of appreciable iron content meets for smelting operation necessitated this study. Core samples of the iron ore sourced from Itakpe, Kogi State, Nigeria were prepared for petrological analysis followed by chemical and particle size analyses. Froth flotation was done using different collectors at varying particle sizes and pH values. Characterization studies carried out revealed that Itakpe iron ore is a lean ore assaying 36.18% Fe2O3 and contains predominantly quartz, sillimanite, and haematite. Its liberation size lies favourably at 75 µm. Processing the ore by froth flotation yielded appreciable enrichment. Optimal recovery (~92%) was achieved using potassium amyl xanthate (PAX) at pH 11 for fine feed sizes (<125 µm) yielding iron concentrate assaying 67.66% Fe2O3. Thus, processing at this set-of- conditions is recommended for the industrial production of more enriched Itakpe iron ore concentrates. -
Principles of Extractive Metallurgy Lectures Note
PRINCIPLES OF EXTRACTIVE METALLURGY B.TECH, 3RD SEMESTER LECTURES NOTE BY SAGAR NAYAK DR. KALI CHARAN SABAT DEPARTMENT OF METALLURGICAL AND MATERIALS ENGINEERING PARALA MAHARAJA ENGINEERING COLLEGE, BERHAMPUR DISCLAIMER This document does not claim any originality and cannot be used as a substitute for prescribed textbooks. The information presented here is merely a collection by the author for their respective teaching assignments as an additional tool for the teaching-learning process. Various sources as mentioned at the reference of the document as well as freely available material from internet were consulted for preparing this document. The ownership of the information lies with the respective author or institutions. Further, this document is not intended to be used for commercial purpose and the faculty is not accountable for any issues, legal or otherwise, arising out of use of this document. The committee faculty members make no representations or warranties with respect to the accuracy or completeness of the contents of this document and specifically disclaim any implied warranties of merchantability or fitness for a particular purpose. BPUT SYLLABUS PRINCIPLES OF EXTRACTIVE METALLURGY (3-1-0) MODULE I (14 HOURS) Unit processes in Pyro metallurgy: Calcination and roasting, sintering, smelting, converting, reduction, smelting-reduction, Metallothermic and hydrogen reduction; distillation and other physical and chemical refining methods: Fire refining, Zone refining, Liquation and Cupellation. Small problems related to pyro metallurgy. MODULE II (14 HOURS) Unit processes in Hydrometallurgy: Leaching practice: In situ leaching, Dump and heap leaching, Percolation leaching, Agitation leaching, Purification of leach liquor, Kinetics of Leaching; Bio- leaching: Recovery of metals from Leach liquor by Solvent Extraction, Ion exchange , Precipitation and Cementation process. -
Effects of Copper on the Cupellation of Silver
Scholars' Mine Bachelors Theses Student Theses and Dissertations 1908 Effects of copper on the cupellation of silver Charles A. Baker Miles Sedivy Follow this and additional works at: https://scholarsmine.mst.edu/bachelors_theses Part of the Mining Engineering Commons Department: Mining Engineering Recommended Citation Baker, Charles A. and Sedivy, Miles, "Effects of copper on the cupellation of silver" (1908). Bachelors Theses. 240. https://scholarsmine.mst.edu/bachelors_theses/240 This Thesis - Open Access is brought to you for free and open access by Scholars' Mine. It has been accepted for inclusion in Bachelors Theses by an authorized administrator of Scholars' Mine. This work is protected by U. S. Copyright Law. Unauthorized use including reproduction for redistribution requires the permission of the copyright holder. For more information, please contact [email protected]. bl.':~M J1IJ!(JWI.'.~1.. ""'~tlION T ,~~. ][VI'ECTS Ol~ COPP}1~H OU TIm CUPlilJJJAT Ion OF SI J~VER • Charles A. Baker Miles Sedivy. MSM til~ t~lCrlt. \lYj,M.cmloi\l (1) ::.:.. :.. : -~..-. : ...... "' .. " : .. ~ --- The ob~iect of this work is to rind--t-he effec't o~ coppa- in - .. = : : .... : - - .. tbe cupellation of silver. - .. Our Method of attack was: 1st. To find the effect of varying the amount of copper with constant lead and constant temperature. 2nd. Effect in cupel"' ation of varying the temperature and the lead in the presence of a constant amount of copper. 3rd. To detecnine the rate at which the copper is removed during cupellation. R.W.Lodge in his book on Assaying states,"If a lead button contains much copper,CuO will be formed with the PbO and this,when absorbed by the cupel,seems to take silver with it into the cupe1.· 2 ~ a.... -
Roberts & Evans, Aberystwyth
Llyfrgell Genedlaethol Cymru = The National Library of Wales Cymorth chwilio | Finding Aid - Roberts & Evans, Aberystwyth (Solicitors) Records, (GB 0210 ROBEVS) Cynhyrchir gan Access to Memory (AtoM) 2.3.0 Generated by Access to Memory (AtoM) 2.3.0 Argraffwyd: Mai 04, 2017 Printed: May 04, 2017 Wrth lunio'r disgrifiad hwn dilynwyd canllawiau ANW a seiliwyd ar ISAD(G) Ail Argraffiad; rheolau AACR2; ac LCSH Description follows ANW guidelines based on ISAD(G) 2nd ed.; AACR2; and LCSH https://archifau.llyfrgell.cymru/index.php/roberts-evans-aberystwyth-solicitors- records-2 archives.library .wales/index.php/roberts-evans-aberystwyth-solicitors-records-2 Llyfrgell Genedlaethol Cymru = The National Library of Wales Allt Penglais Aberystwyth Ceredigion United Kingdom SY23 3BU 01970 632 800 01970 615 709 [email protected] www.llgc.org.uk Roberts & Evans, Aberystwyth (Solicitors) Records, Tabl cynnwys | Table of contents Gwybodaeth grynodeb | Summary information .............................................................................................. 3 Hanes gweinyddol / Braslun bywgraffyddol | Administrative history | Biographical sketch ......................... 3 Natur a chynnwys | Scope and content .......................................................................................................... 5 Trefniant | Arrangement .................................................................................................................................. 5 Nodiadau | Notes ............................................................................................................................................ -
Pantglas Junior School
2 The Aberfan Disaster October 1966 I have been asked to inform that there has been a landslide ‘‘ at Pantglas. The tip has come down on the school Emergency call received by Merthyr Tydfil Police at 9.25am on 21st October 1966. ’’ The Tragedy At approximately 9.15am on Friday 21st October 1966, Merthyr Vale colliery tip situated The scene immediately following the disaster at Pantglas on the mountainside overlooking the village of Junior School Aberfan in South Wales, slipped and descended on Pantglas Junior School. Police supervised all of the victim identifications at Bethania Chapel, under the ministry of Reverend The tip slid like an avalanche. It destroyed the school, S. Lloyd, which was provided as a temporary mortuary 20 nearby houses in its path, and rendered other 250 yards from the scene of the devastation. houses in the vicinity unsafe for habitation. With its balcony, the chapel seated a congregation Half a million tonnes of coal waste in a tidal wave 40 of 500, and was approximately 30 yards by 20 yards feet high hit the village. The school was in session as it in size. was the last day before half term week. The vestry, 20 yards by 10 yards, housed voluntary 144 children and adults died; 116 were school workers for the Red Cross together with St John’s children. Half of all the pupils at Pantglas Junior School Ambulance stretcher-bearers. were killed together with five of their teachers. The chapel was in use as a mortuary and missing The tragedy was caused by two days of continual person’s bureau from 21st October until 4th heavy rain loosening the coal slag, which was situated November 1966. -
Pike Law Geology Report by Colin Fowler
Geology of the Pike Law area. The Pike law mine site lies astride the Newbiggin to Westgate road, bounded on the east by Flushiemere beck and on the west by Westerbeck, with Broadley Hill at the NE corner being the highest point at 530m. Dunham describes the area: “The outcrop of the beds between the base of the Great Limestone and the Firestone on Pike Law, between Wester Beck and Flushiemere Beck, is traversed by a remarkable complex of veins.” (PP 243) Details of the geology have been given by Dunham, (1948 &1990); Bridges and Young, (2007); Bevins et al, (2010). Geological Survey of England and Wales 1:63,360/1:50,000 geological map series, New Series, sheet 25, Alston. The area has been worked by shaft, adit and hush, with 3 named areas of hush to the East of the road, Leonard’s Hush; Pikelaw Hush and Flask Hushes. To the West of the road, West End Hushes. There are a complex of leats and old dams forming reservoirs on both sides of the road, though non of them seem to have been able to hold sufficient water to enable hydraulic flushing alone to have created the hushes that we see. It is most likely to have been quarried and the water used for washing the mineral. “The production of lead concentrates from 1852 to 1891, when all work ceased was only 1725 tons.” (Dunham) “Surface evidence suggests that the area had been heavily worked prior to 1852, and what is recorded is the last gleanings of an old mining field” (Fairburn, A 2009) The figure given in Dunham may be optimistic, J. -
Emission Estimation Technique Manual
1DWLRQDO3ROOXWDQW,QYHQWRU\ Emission Estimation Technique Manual for Lead Concentrating, Smelting and Refining First published in December 1999 EMISSION ESTIMATION TECHNIQUES FOR LEAD CONCENTRATING, SMELTING AND REFINING TABLE OF CONTENTS 1.0 INTRODUCTION 1 1.1 Context of this Manual 1 1.2 EETs Should be Considered as “Points of Reference” 2 1.3 Hierarchical Approach Recommended in Applying EETs 3 1.4 NPI Emissions in the Environmental Context 3 1.5 NPI Reporting Requirements 3 1.6 Use of this Manual 4 2.0 PROCESS DESCRIPTION 5 2.1 General 5 2.2 Lead Processing 6 2.2.1 Lead Concentrating 6 2.2.2 Smelting Process 8 2.3 Secondary Lead Processing 11 3.0 ANCILLARY ACTIVITIES AND ASSOCIATED FACILITIES 13 3.1 Ancillary Activities 13 3.1.1 Acid Plant 13 3.1.2 Selenium Removal Process 13 3.1.3 Zinc Recovery 15 3.1.4 Cadmium Plant 15 3.2 Associated Facilities 15 3.2.1 Fuel and Organic Liquid Storage 15 3.2.2 Fossil Fuel Electric Generation 16 3.2.3 Combustion Engines 16 3.3 Maintenance Activities 16 4.0 POSSIBLE EMISSIONS 17 4.1 Reporting Thresholds 19 4.2 Reporting Requirements 21 5.0 EMISSION ESTIMATION 22 5.1 Emission Estimation Techniques 22 5.1.1 Direct Measurement 32 5.1.2 Engineering Calculations 33 5.1.3 Mass Balance 33 5.1.4 Emission Factors 35 5.2 Acceptable Reliability and Uncertainty 36 5.2.1 Direct Measurement 36 5.2.2 Mass Balance 36 5.2.3 Engineering Calculations 37 5.2.4 Emission Factors 37 5.3 NPI Reporting Steps 38 Lead Concentrating, Smelting, and Refining i LEAD CONCENTRATING, SMELTING AND REFINING TABLE OF CONTENTS CONT’ 6.0 -
An Issue Dedicated to Solutions for the Modern Mining Industry
Metso’s customer magazine » ISSUE 1/2017 Mining minds An issue dedicated to solutions for the modern mining industry More efficiency Six-fold reduction Longer wear life and with less energy in moisture content fewer liner changes 06 and water 18 at Olenegorsky GOK 28 reduce costs “Metso has gone beyond combining and re-releasing technology based on prior designs. Its solution is more efficient, lasts longer and reduces operating costs.” mining Results mining is PUBLISHED BY EDITOR-IN-CHIEF © Copyright 2017 PRINTING Metso’s customer magazine Metso Corporation Inka Törmä, Metso Corporation. Hämeen Kirjapaino Oy, showcasing our work and [email protected] All rights reserved. February 2017 Töölönlahdenkatu 2, the success of our customers. P.O. Box 1220, DESIGN AND LAYOUT Reproduction permitted ISSN SUBSCRIPTIONS FI-00101 Helsinki, Brandkind, brandkind.fi quoting “Results mining” 2343-3590 To receive your personal Finland as source. ENGLISH LANGUAGE ADDRESSES 4041 0209 copy, please contact your Printed matter tel. +358 20 484 100 Kathleen Kuosmanen All product names used Metso customer data nearest Metso office or HÄMEEN KIRJAPAINO OY www.metso.com are trademarks of their the e-mail provided. respective owners. This magazine, including all claims regarding operational performance, is intended for sharing information on successful customer cases. Metso makes no warranty or representation whatsoever, either express or implied, that similar or any performance levels or improvements are achievable for all sites or for any particular site. Metso assumes no legal liability for any use of information contained in this presentation. If requested, Metso can execute a site specific survey to provide an estimate of performance or performance improvement for a specific site and operation. -
Georgius Agricola and Vannoccio Biringuccio, Long Deceased, Without Whose Work This Project Could Not Have Been Undertaken
TC0/61-- Project Number: 48-EMP-HGMW Mining and Metallurgy to the Renaissance An Interactive Qualifying Project Report submitted to the Faculty of the WORCESTER POLYTECHNIC INSTITUTE in partial fulfillment of the requirements for the Degree of Bachelor of Science by Matt Skinner Lenny Frank Michael Galvin r Advisor: Prof. E. Malc Parkinson E: Date: July 22, 1999 E Project Abstract The Higgins Armory staff are interested in the processing of metals before they reach the hands of the armor-maker. This project is a collection of some of the information available on mining, metal-working, and the early metal industry of Europe up to the Renaissance. It is intended to serve as an introduction for staff, and to provide information that they can incorporate into their guided tours of the museum. ii Acknowledgements The project team would like to thank the following people for their assistance and efforts. Professor E. Malcolm Parkinson, our project advisor, for his guidance, patience, and instruction on this project. Linda Honan, the former Director of Instruction, and Kent dur Russell, the Director of the Higgins Armory Museum, Worcester, for their support and interest in this project. Georgius Agricola and Vannoccio Biringuccio, long deceased, without whose work this project could not have been undertaken. iii Table of Contents List of Illustrations v Introduction 1 Ancient Times Ancient Sources 3 Ancient and Roman Mining Technique 4 Processing and Refining 14 Roman Mineral Sources 23 Medieval Times Medieval Mining 34 The Renaissance Introduction 36 Georgius Agricola 37 Vannoccio Biringuccio 41 De Re Metallica 43 Pirotechnia 77 Conclusion and Recommendations 92 Appendix I: Properties of Metals 94 Appendix II: Annotated Bibliography 98 iv List of Illustrations Ancient Fig. -
The Involvement of the Women of the South Wales Coalfield In
“Not Just Supporting But Leading”: The Involvement of the Women of the South Wales Coalfield in the 1984-85 Miners’ Strike By Rebecca Davies Enrolment: 00068411 Thesis submitted for Doctor of Philosophy degree at the University of Glamorgan February 2010. ABSTRACT The 1984-85 miners’ strike dramatically changed the face of the South Wales Valleys. This dissertation will show that the women’s groups that played such a crucial supportive role in it were not the homogenous entity that has often been portrayed. They shared some comparable features with similar groups in English pit villages but there were also qualitative differences between the South Wales groups and their English counterparts and between the different Welsh groups themselves. There is evidence of tensions between the Welsh groups and disputes with the communities they were trying to assist, as well as clashes with local miners’ lodges and the South Wales NUM. At the same time women’s support groups, various in structure and purpose but united in the aim of supporting the miners, challenged and shifted the balance of established gender roles The miners’ strike evokes warm memories of communities bonding together to fight for their survival. This thesis investigates in detail the women involved in support groups to discover what impact their involvement made on their lives afterwards. Their role is contextualised by the long-standing tradition of Welsh women’s involvement in popular politics and industrial disputes; however, not all women discovered a new confidence arising from their involvement. But others did and for them this self-belief survived the strike and, in some cases, permanently altered their own lives. -
The Relationship Between Iron Age Hill Forts, Roman Settlements and Metallurgy on the Atlantic Fringe
The Relationship between Iron Age Hill Forts, Roman Settlements and Metallurgy on the Atlantic Fringe Keith Haylock BSc Department of Geography and Earth Sciences Supervisors Professor John Grattan, Professor Henry Lamb and Dr Toby Driver Thesis submitted in fulfilment of the award of degree of Doctor of Philosophy at Aberystwyth University 2015 0 Abstract This thesis presents geochemical records of metalliferous enrichment of soils and isotope analysis of metal finds at Iron Age and Romano-British period settlements in North Ceredigion, Mid Wales, UK. The research sets out to explore whether North Ceredigion’s Iron Age sites had similar metal-production functions to other sites along the Atlantic fringe. Six sites were surveyed using portable x-ray fluorescence (pXRF), a previously unused method in the archaeology of Mid Wales. Also tested was the pXRF (Niton XLt700 pXRF) with regard to how environmentally driven matrix effects may alter its in situ analyses results. Portable x-ray fluorescence was further used to analyse testing a range of certified reference materials (CRM) and site samples to assess target elements (Pb, Cu, Zn and Fe) for comparative accuracy and precision against Atomic absorption spectroscopy (AAS) and Inductively coupled plasma mass spectrometry (ICP-MS) for both in situ and laboratory sampling. At Castell Grogwynion, one of the Iron Age sites surveyed recorded > 20 times Pb enrichment compared to back ground values of 110 ppm. Further geophysical surveys confirmed that high dipolar signals correlated to the pXRF Pb hotspots were similar to other known Iron Age and Roman period smelting sites, but the subsequent excavation only unearthed broken pottery and other waste midden development.