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Rheologie Und Noch Viel Mehr Rheology and a Whole Lot More

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Rheologie Und Noch Viel Mehr Rheology and a Whole Lot More Rheologie und noch viel mehr Rheology and a Whole Lot More Mark Husband, Nach 15 em Schnee und dem hartesten Winter seit Fairborn, OH, vielen Jahren im Mittelwesten war die Ankunft im USA schonen, sonnigen San Diego, Kalifornien, sicherlich ein vielversprechender Anfang eines bedeutenden Ereignisses: der 207. Tagung der Amenkan1schen Chemischen Gesellschaft (Amencan Chem1cal Soc1ety). Die ACS Tagungen, die zweimal jahrlich im Fri.ihjahr Leaving six inches of snow and the harshest Mid- und im Herbst stattfinden, gehoren zu den bestbesuch­ . western winter in recent memory to arnve 1n beautiful, ten naturwissenschaftlichen Konferenzen der Welt, und sunny San Diego, California was certainly an auspi­ die Tagung in San Diego w�r mit beinahe 15 000 Teil­ : cious beginning to a great event: the 207th Meetmg of nehmern keine Ausnahme. Uber 5. 700 Vortrage wur- the American Chemical Society. The ACS meet1ngs, den in 627 verschiedenen Sitzungen vorgestellt, wom1t. held biannually in the spring and fall, are among the ein umfangreicher Themenkomplex angeboten wurde, most highly attended scientific conferences 1n the um jedem denkbaren chemischen Verlangen nach­ world, and the San Diego Meeting was no exception, zukommen. Die diesjahrige Fri.ihjahrstagung fand vom with nearly 15,000 participants. Over 5,700 papers 13. bis 1 7. Marz 1994 statt. were presented in 627 different techn1cal_ sess1ons, Zahlreiche gesellschaftliche und Sonderprogramme offering a wide range of topics to satisfy every con­ begleiteten die Tagung, unter anderem eme groBe ceivable chemical yearning. This year's spnng meetmg Ausstellung mit 380 Standen von ca. 220 F1rmen. was held from March 13-1 7, 1994. Chemische Produkte, Laborausstattung und -gerate Numerous special and social events took place during sowie die neuesten naturwissenschaftlichen Software­ the meeting, including a large exposition featuring Pakete waren auf der Ausstellung zu sehen. 380 booths manned by approximately 220 compa­ Auch typisch fi.ireine ACS Tagung ist die groBe Anzahl nies. Chemical supplies, laboratory equipment and von Arbeitskreisen und Kursen, d1e 1n Verbmdung m1t instrumentation, as well as the latest in scientific soft­ der Konferenz angeboten werden. Das Rahmen­ ware was available for examination at the expos1t1on. programm umfaBte mehrere von den Fachgruppen der Also traditional for an ACS meeting is the large num­ ACS veranstaltete Begri.iBungsabendesow1e e1n Ehren­ ber of workshops and short courses offered in con­ bankert bei dem 43 Auszeichnungen verliehen junction with the conference. Social events included a wurden Die Posterprasentationen, die jeden Abend number of receptions hosted by diVISions_ w1th1n the stattfanden,: verliefen wie die gesellschaftlichen ACS as well as an award banquet honoring 43 recip­ Veranstaltungen - die Prasenz einer Bar belebte ient of ACS national awards. The poster sessions that typischerweise die bereits gehobene St1mmung. took� place each evening also took on the character of Von den 5. 700 vorgetragenen Beitragen waren ca. social events, with a cash bar typically ava1lable to 5% auf irgendeine Weise mit Rheologie verwandt help enliven the already charged atmosphere. Selbstverstandlich konnen von diesen nur e1ne kleme Of the 5, 700 papers presented, approximately 5% Anzahl zusammengefaBt werden und in vielen Fallen were in some way related to rheology. Of course only muBte man sich zwischen mehreren interessanten a small number of those can be summarized here, Vortragen entscheiden, die gleichzeitig in parallelen and, in many cases one had to choose among several Sitzungen prasentiert wurden. Veroffentliche Vers1onen interesting papers that were presented Simultaneously der hier erwahnten Vortrage enthalten d1e Tagungs­ in parallel sessions. Written versions of the papers bande der Fachgruppen Polymerchemie (Polymer reviewed here are provided in the Proceedmgs pub­ Chemistry Division) bzw. Polymerwerkstoffwissen­ lished by the Polymer Chemistry Division and the schaften und -technik (Polymer Matenals Sc1ence and Polymer Materials Science and Engmeenng DIVISion of Engineering Division) der ACS. the ACS, respectively. Die Fachgruppe Polymerchemie organisierte ein Drei­ The Division of Polymer Chemistry organized a three Tages Symposium zu Ehren von Prof. W. E. Stock­ day symposium in honor of Prof. W. E. Stockmayer of mayer von Dartmouth College. Das Thema des Sympo­ Dartmouth College. The subject of the sympos1um was siums war Polymer Dynamik und Thermodynam1k 1n Polymer Dynamics and Thermodynamics 1n Solut1on Losungen und umfaBte 46 Beitrage, die gr6Btente1ls and included 46 papers, many of wh1ch were present­ von ehemaligen Studenten und Kollegen von Prof. ed by former students and colleagues of Prof. Stockmayer vorgetragen wurden. Das Stockmayer Stockmayer. The Stockmayer symposium concluded Symposium wurde mit der Verleihung e1ner Auszelch­ with an award presented to Prof. Stockmay r for h1s nung an Prof. Stockmayer fi.ir se1ne v1elen w1cht1gen � many important contributions to polymer sc1ence over Beitrage zur Polymerwissenschaft uber_ e1ne lange und a long and distinguished career. renommierte Karriere beendet. Rheology 94 Juni/June 94 1994 KennzifferrrServ ce Reader-Serv1ce� �� L.{5:/' ., NEMO!Pumps. Ein paar hervorragende Beitrage vom Stockmayer Symposium sind hier erwahnt. Guy Berry und S. Yue von Carnegie Mellon berichteten uber ihre Untersu­ chungen an Ieicht konzentrierten Polystyrollosungen mit statischer und dynamischer Lichtstreuung. lm Vergleich zu verdunnten U:isungenis t die Charak­ terisierung von Ieicht konzentrierten Losungen schwie­ riger. Berry stellte eine Theorie vor, die ziemlich gute Vorhersagen fUr diese Losungen bei statischer Lichtstreuung ermoglicht und auch die dynamische The versatile Netzsch Tim Lodge Lichtstreuung im Griff zu scheinen hat. und pumping concept Our qualityassurance system Mitarbeiter der University of Minnesota prasentierten is certifiedaccording to for all branches DIN ISO 9001 under the Ergebnisse uber Diffusion von Polystyrolkugeln in DQS·No. 11405·01. Poly(vinylmethylether) Losungen. Prof. Lodge betonte, of industry. daB sich die Losung um die Kugel herum oft von der Netzsch·Mohnopumpen GmbH LiebigstraBe 28, P.O. Box 1120 Gesamtlosung unterscheidet, da oft die Kugel entwe­ 0·84464 Waldkraiburg, Germany der die Polymerketten anzieht oder abst6Bt. Somit Phone 08638163-0, Fax 67999 kann man nie eine Kugel als einen reprasentativen Teil Telex 56421 ® NEMO: Registered trade mark of einer Partikellosung betrachten, da sich die Gesamt­ NETZSCHMOH NOPUMPEN GMBH losung anders verhalt. NETZS[H A. Jones und Mitarbeiter von der Clark University und A few highlights of papers from the Stockmayer sym­ das GE R&D Zentrums berichteten von ihrer Arbeit, in posium are provided here. Guy Berry and S. Yue of der sie anhand von Festkbrper-NMR Sekundarrelaxa­ Carnegie Mellon reported on their investigations of tionen in Polymer-Blends feststellten. Sie fanden; daB static and dynamic light scattering of moderately con­ ein Umklappvorgang (Flipping Process) beobachtet centrated polystyrene solutions. In contrast to dilute werden kann infolge von Phenylgruppen, die von einer solutions, description of moderately concentrated Position zur anderen springen. Fur Polystyrol deckt solutions has been more difficult. Berry presented a sich der Umklappvorgang mit dem Glasubergangs­ theory that gives reasonable predictions for these vorgang, und ein Modell wurde entwickelt, daB zur solutions under static light scattering and also appears Vorhersage von NMR-Spektren dient. Gary Grest und to handle dynamic light scattering as well. Tim Lodge Mitarbeiter von Exxon berichteten uber die Kinematik and co-workers from the University of Minnesota pre­ und Relaxation von endvernetzten Polymer Netz­ sented results on diffusion of polystyrene spheres in werken. lnfolge der bei freier Vernetzung auftretender poly(vinylmethylether) solutions. Prof. Lodge empha­ UnregelmaBigkeiten (frei hangende Kettenenden und sized that the solution around a sphere is often differ­ starke Schwankungen im MW zwischen Vernetzungs­ ent from the bulk solution, because the sphere often punkten) haben sie ein rechnergesteuertes Modellieren either attracts or repulses the polymer chains. Thus, eingesetzt, um das Vernetzungssystem zu simulieren. you can never use a sphere as a probe of the particle Dadurch konnten sie ideales Vernetzen erreichen und solution, because the bulk solution will behave differ­ die daraus resultierenden Materialeigenschaften ently. berechnen. Sie verwendeten das Modell, um das Materialmodul zu berechnen, und die Ergebnisse zeig­ A. Jones and co-workers at Clark University and the ten, daB nicht frei bewegbare Verschlaufungen bei der GE R&D Center reported on their work detecting sec­ Bestimmung von Materialeigenschaften wichtig sind. ondary relaxations in polymer blends via solid-state NMR. They found that a flipping process can be I. Noda und Y. Takahashi von der Nagoya University, observed due to the phenyl group flipping from one Japan, prasentierten Daten der viskoelastischen Eigen­ position to another. For polystyrene, the flipping pro­ schaften von Polyelektrolytlbsungen. Sie bestimmten cess overlaps with the glass transition process and die Konzentrationsabhangigkeit der Viskositat, des they developed a model that could be used to predict Moduls und der Nachgiebigkeit und entwickelten eine the NMR spectra. Gary Grest and co-workers from Theorie fUr die Polymerdynamik aufbauend auf dem Exxon reported on the kinetics
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