Five Years of Separations Feature Paper 2018
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Five Years of SeparationsFive Years • Victoria Samanidou and Rafael Lucena Five Years of Separations Feature Paper 2018 Edited by Victoria Samanidou and Rafael Lucena Printed Edition of the Special Issue Published in Separations www.mdpi.com/journal/separations Five Years of Separations Five Years of Separations Feature Paper 2018 Editors Victoria Samanidou Rafael Lucena MDPI • Basel • Beijing • Wuhan • Barcelona • Belgrade • Manchester • Tokyo • Cluj • Tianjin Editors Victoria Samanidou Rafael Lucena Laboratory of Analytical Chemistry, Department of Analytical Chemistry, School of Chemistry, Universidad de Cordoba Aristotle University of Thessaloniki Spain Greece Editorial Office MDPI St. Alban-Anlage 66 4052 Basel, Switzerland This is a reprint of articles from the Special Issue published online in the open access journal Separations (ISSN 2297-8739) (available at: https://www.mdpi.com/journal/separations/special issues/five y ears separations). For citation purposes, cite each article independently as indicated on the article page online and as indicated below: LastName, A.A.; LastName, B.B.; LastName, C.C. Article Title. Journal Name Year, Article Number, Page Range. ISBN 978-3-03936-924-9 (Hbk) ISBN 978-3-03936-925-6 (PDF) Cover image courtesy of Victoria Samanidou. c 2020 by the authors. Articles in this book are Open Access and distributed under the Creative Commons Attribution (CC BY) license, which allows users to download, copy and build upon published articles, as long as the author and publisher are properly credited, which ensures maximum dissemination and a wider impact of our publications. The book as a whole is distributed by MDPI under the terms and conditions of the Creative Commons license CC BY-NC-ND. Contents About the Editors .............................................. vii Preface to ”Five Years of Separations” .................................. ix Natalia Manousi and Victoria F. Samanidou Applications of Gas Chromatography for the Analysis of Tricyclic Antidepressants in Biological Matrices Reprinted from: Separations 2019, 6, 24, doi:10.3390/separations6020024 ............... 1 Irene Panderi, Eugenia Taxiarchi, Constantinos Pistos, Eleni Kalogria and Ariadni Vonaparti Insights into the Mechanism of Separation of Bisphosphonates by Zwitterionic Hydrophilic Interaction Liquid Chromatography: Application to the Quantitation of Risedronate in Pharmaceuticals Reprinted from: Separations 2019, 6, 6, doi:10.3390/separations6010006 ............... 21 Maria Celeiro, Lua Vazquez, J. Pablo Lamas, Marlene Vila, Carmen Garcia-Jares and Maria Llompart Miniaturized Matrix Solid-Phase Dispersion for the Analysis of Ultraviolet Filters and Other Cosmetic Ingredients in Personal Care Products Reprinted from: Separations 2019, 6, 30, doi:10.3390/separations6020030 ............... 35 Anastasios I. Zouboulis, Efrosyni N. Peleka and Anastasia Ntolia Treatment of Tannery Wastewater with Vibratory Shear-Enhanced Processing Membrane Filtration Reprinted from: Separations 2019, 6, 20, doi:10.3390/separations6020020 ............... 49 Samantha L. Bowerbank, Michelle G. Carlin and John R. Dean Dissolution Testing of Single- and Dual-Component Thyroid Hormone Supplements Reprinted from: Separations 2019, 6, 18, doi:10.3390/separations6010018 ............... 67 Ana Isabel Argente-Garc´ıa, Lusine Hakobyan, Carmen Guillem and Pilar Camp´ıns-Falc´o Estimating Diphenylamine in Gunshot Residues from a New Tool for Identifying both Inorganic and Organic Residues in the Same Sample Reprinted from: Separations 2019, 6, 16, doi:10.3390/separations6010016 ............... 75 Ewa Skoczynska ´ and Jacob de Boer Retention Behaviour of Alkylated and Non-Alkylated Polycyclic Aromatic Hydrocarbons on Different Types of Stationary Phases in Gas Chromatography Reprinted from: Separations 2019, 6, 7, doi:10.3390/separations6010007 ............... 95 Cheryl Frankfater, Robert B. Abramovitch, Georgiana E. Purdy, John Turk, Laurent Legentil, Lo¨ıc Lemi`egre and Fong-Fu Hsu Multiple-stage Precursor Ion Separation and High Resolution Mass Spectrometry toward Structural Characterization of 2,3-Diacyltrehalose Family from Mycobacterium tuberculosis Reprinted from: Separations 2019, 6, 4, doi:10.3390/separations6010004 ...............107 Filip S. Ekholm, Suvi-Katriina Ruokonen, Marina Red´on, Virve Pitk¨anen, Anja Vilkman, Juhani Saarinen, Jari Helin, Tero Satomaa and Susanne K. Wiedmer Hydrophilic Monomethyl Auristatin E Derivatives as Novel Candidates for the Design of Antibody-Drug Conjugates Reprinted from: Separations 2019, 6, 1, doi:10.3390/separations6010001 ...............121 v Naysla Paulo Reinert, Camila M. S. Vieira, Cristian Berto da Silveira, Dilma Budziak and Eduardo Carasek A Low-Cost Approach Using Diatomaceous Earth Biosorbent as Alternative SPME Coating for the Determination of PAHs in Water Samples by GC-MS Reprinted from: Separations 2018, 5, 55, doi:10.3390/separations5040055 ...............133 vi About the Editors Victoria Samanidou was born on 11 January, 1963, in Thessaloniki, Greece. She obtained her Bachelor of Science degree in Chemistry in 1985 from the Chemistry Department of Aristotle University of Thessaloniki, Greece. In 1990, she obtained a doctorate (Ph.D.) in Chemistry from the Department of Chemistry of the Aristotle University of Thessaloniki. The topic of her thesis was “Distribution and mobilization of heavy metals in waters and sediments from rivers in Northern Greece”. In the same year, Dr. Samanidou joined the Laboratory of Analytical Chemistry, in the Department of Chemistry of Aristotle University of Thessaloniki, as a Technical Assistant. Nine years later, she was elected as Lecturer in the Laboratory of Analytical Chemistry in the Department of Chemistry of the Aristotle University of Thessaloniki. In 2007, she joined the Institute of Analytical Chemistry and Radiochemistry in Graz Technical University, for four months, developing methods by LC-MS/MS. Since 2015, Dr. Samanidou has been Full Professor in the Laboratory of Analytical Chemistry in the Department of Chemistry of Aristotle University of Thessaloniki, Greece, where she currently serves as Director of the Laboratory. Dr. Samanidou has authored and co-authored more than 170 original research articles in peer-reviewed journals and 45 reviews and 50 chapters in scientific books, with an H-index 36 (Scopus June 2020, http://orcid.org/0000-0002-8493-1106, Scopus Author ID 7003896015) and circa 3500 citations. She has supervised four PhD Theses, 24 postgraduate Diploma Theses, 2 postdoc researchers, and more than 15 undergraduate Diploma Theses. She has served as Member of 10 advisory PhD committees, 21 examination PhD committees, and 32 examination committees of postgraduate Diploma Theses. She is a member of the editorial board of more than 10 scientific journals, and she has reviewed circa 500 manuscripts in more than 100 scientific journals. She was also guest editor in more than 10 special issues in scientific journals. She has served as Academic Editor for Separations MDPI, as Regional editor in Current Analytical Chemistry, and as Editor in Chief of Pharmaceutica Analytica Acta. Her research interests include: 1. Development and validation of analytical methods for the determination of inorganic and organic substances using chromatographic techniques; 2. development and optimization of methodology for sample preparation of various samples, e.g., food, biological fluids; 3. study of new chromatographic materials used in separation and sample preparation (polymeric sorbents, monoliths, carbon nanotubes, fused core particles, etc.) compared to conventional materials. She has also been Member of the organizing and scientific committee in 20 scientific conferences. In December 2015, Dr. Samanidou was elected as President of the Steering Committee of the Division of Central and Western Macedonia of the Greek Chemists’ Association. In November 2018, she was reelected to serve at the same leading position for 3 more years. A milestone in her career was in 2016, when she was included in the top 50 power list of women in Analytical Science, as proposed by Texere Publishers. https://theanalyticalscientist.com/power-list/the-power-list-2016. vii Rafael Lucena has been a professor of Analytical Chemistry at the University of Cordoba´ since 2010 and the secretary of the Research Institute of Fine Chemistry and Nanochemistry at the same university. To date, Rafael has co-authored 109 scientific articles (h-index: 34, Scopus ID: 8517312100Scopus) dealing with different analytical chemistry facets, although sample preparation is the central core of his research. His research is mainly focused on the development of new extraction approaches and the design of novel materials for analytes isolation. Since 2017, he has worked on the design of a new paper-based sorptive phase with application in analytical chemistry and catalysis. He is also interested in the integration of microextraction techniques with sampling and instrumental analysis (spectroscopic and mass spectrometry techniques). Rafael has reviewed more than 500 articles in many scientific journals and has evaluated research projects for different agencies such as Fondecyt (Chile), Agencia Estatal de Investigacion´ (Espana)˜ and the Czech Science Foundation. He is a member of different societies, such as the American Chemical Society, American Society for Mass Spectrometry and Sociedad Espanola˜ de Qu´ımica Anal´ıtica. He is also a member of the Spanish Network for Sample Preparation and the EuChemS-DAC Sample Preparation