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Electronic Supplementary Material (ESI) for RSC Advances. This journal is © The Royal Society of Chemistry 2016 Supporting Information for Supercritical fluid assisted biotemplating synthesis of Si-O-C microspheres from microalgaes for advanced Li-ion batteries Yang Xia,a Ruyi Fang,a Zhen Xiao,b Luoyuan Ruan,a Rongjun Yan,c Hui Huang,a Chu Liang,a Yongping Gan,a Jun Zhang,a Xinyong Tao,a,* and Wenkui Zhanga,* a College of Materials Science and Engineering, Zhejiang University of Technology, Hangzhou, 310014, China. b College of Materials Science and Engineering, China Jiliang University, Hangzhou, 310018, China. c Ocean College, Zhejiang University of Technology, Hangzhou, 310014, China. * Corresponding authors: [email protected] (XY Tao); [email protected] (WK Zhang). Figure S1 The particle size distributions of microalgae carbon and Si-O-C microspheres. Figure S2 HRTEM and corresponding diffraction pattern images of microalgae carbon and Si-O- C microspheres. 1 / 2 Figure S3 The electrochemical properties comparison of various Si-O-C materials prepared different methods. References 1. Liu, X.; Zheng, M. C.; Xie, K. Mechanism of Lithium Storage in Si-O-C Composite Anodes. J. Power Sources, 2011, 196, 10667-10672. 2. Ji, F.; Li, Y. L.; Feng, J. M.; Su, D.; Wen, Y. Y.; Feng, Y.; Hou, F. Electrochemical Performance of Graphene Nanosheets and Ceramic Composites as Anodes for Lithium Batteries. J. Mater. Chem., 2009, 19, 9063-9067. 3. Dibandjo, P.; Graczyk-Zajac, M.; Riedel, R.; Pradeep, V. S.; Soraru, G. D. Structures and Lithium Storage Performance of Si-O-C Composite Materials Depending on Pyrolysis Temperatures. J. Eur. Ceram. Soc., 2012, 32, 2495-2503. 4. Kaspar, J.; Graczyk-Zajac, M.; Riedel, R. Lithium Insertion into Dense and Porous Carbon- Rich Polymer-Derived SiOC Ceramics. Solid State Ionics, 2012, 225, 527-531. 5. Fukui, H.; Eguchi, K.; Ohsuka, H.; Hino, T.; Kanamura, K. Carbon-Rich SiOC Anodes for Lithium-Ion Batteries: Part II. Role of Thermal Cross-Linking. J. Power Sources, 2013, 243, 152-158. 2 / 2.

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