Spring 1981 Gems & Gemology
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CUBIC ZIRCONIA: an UPDATE by Kurt Nassau
CUBIC ZIRCONIA: AN UPDATE By Kurt Nassau Soon after it was first marketed in 1976, ubic zirconia was discovered as a natural mineral in colorless cubic zirconia became the C 1937, when two German mineralogists, von Staclz- dominant diamond imitation, with elberg and Chudoba (1937), were examining a highly current production of approximately 60 metamict zircon given to them by B. W. Anderson. The million carats per year. Although cubic zircon contained some tiny crystals which they identified zirconia was discovered as a natural by X-ray diffraction as the cubic form of zirconium oxide mineral in 1937, crystals usable for (or zirconia), a compound lznown as baddeleyite when in faceting were first produced ill 1969 and it was not until a practical sltull-melting the monoclinic form. So little did von Staclzelberg and technique was developed in the USSR in Chudoba think of this discovery that they did not even 1972 that commercial production became assign a name to the new mineral. As a result, it is lznown feasible. This article reviews the sl<ull- to this day by its scientific name, cubic zirconia, and the melting technique used to produce cubic prefix synthetic, although proper, is not usually included. zirconio and examines the current status This same material had already been used for many of this diamond simulant with regard to years as a ceramic composition for high-temperature in- q~~ality,production, ond market. The dustrial and scientific purposes; because of an exception- patent situation is discussed, as well as ally high melting point, "stabilized zirconia" ceramics prospects lor new diamond imitations can be used at temperatures up to 2540°C (4604°F)and are and the recent surge of interest in colored cubic zirconia. -
Compilation of Reported Sapphire Occurrences in Montana
Report of Investigation 23 Compilation of Reported Sapphire Occurrences in Montana Richard B. Berg 2015 Cover photo by Richard Berg. Sapphires (very pale green and colorless) concentrated by panning. The small red grains are garnets, commonly found with sapphires in western Montana, and the black sand is mainly magnetite. Compilation of Reported Sapphire Occurrences, RI 23 Compilation of Reported Sapphire Occurrences in Montana Richard B. Berg Montana Bureau of Mines and Geology MBMG Report of Investigation 23 2015 i Compilation of Reported Sapphire Occurrences, RI 23 TABLE OF CONTENTS Introduction ............................................................................................................................1 Descriptions of Occurrences ..................................................................................................7 Selected Bibliography of Articles on Montana Sapphires ................................................... 75 General Montana ............................................................................................................75 Yogo ................................................................................................................................ 75 Southwestern Montana Alluvial Deposits........................................................................ 76 Specifi cally Rock Creek sapphire district ........................................................................ 76 Specifi cally Dry Cottonwood Creek deposit and the Butte area .................................... -
Preparation of Barium Strontium Titanate Powder from Citrate
APPLIED ORGANOMETALLIC CHEMISTRY Appl. Organometal. Chem. 13, 383–397 (1999) Preparation of Barium Strontium Titanate Powder from Citrate Precursor Chen-Feng Kao* and Wein-Duo Yang Department of Chemical Engineering, National Cheng Kung University, Tainan, 70101, Taiwan TiCl4 or titanium isopropoxide reacted with INTRODUCTION citric acid to form a titanyl citrate precipitate. Barium strontium citrate solutions were then BaTiO3 is ferroelectric and piezoelectric and has added to the titanyl citrate reaction to form gels. extensive applications as an electronic material. It These gels were dried and calcined to (Ba,Sr)- can be used as a capacitor, thermistor, transducer, TiO3 powders. The gels and powders were accelerometer or degausser of colour television. characterized by DSC/TGA, IR, SEM and BaTiO3 doped with strontium retains its original XRD analyses. These results showed that, at characteristics but has a lower Curie temperature 500 °C, the gels decomposed to Ba,Sr carbonate for positive temperature coefficient devices under and TiO2, followed by the formation of (Ba,Sr)- various conditions. TiO3. The onset of perovskite formation oc- Besides solid-state reactions, chemical reactions curred at 600 °C, and was nearly complete at have also been used to prepare BaTiO3 powder. 1 1000 °C. Traces of SrCO3 were still present. Among them the hydrolysis of metal alkoxide , The cation ratios of the titanate powder oxalate precipitation in ethanol2, and alcoholic prepared in the pH range 5–6 were closest to dehydration of citrate solution3 are among the more the original stoichiometry. Only 0.1 mol% of the attractive methods. In 1956 Clabaugh et al.4 free cations remained in solution. -
Simultaneous Diamond, White Sapphire & Moissanite
SIMULTANEOUS DIAMOND, WHITE SAPPHIRE & MOISSANITE TESTER NEW ADVANCED EXCLUSIVE TECHNOLOGY RECOMMENDED by CHARLES & COLVARD CREATED MOISSANITE READ BEFORE USING The new moissanite that was introduced in late 2015 has changed. It can no longer be easily visually identified. It is now D-E-F “colorless”, with few inclusions. More importantly, standard diamond/moissanite testers will identify it as diamond since it is now only very slightly electrically conductive. The UltraTester 3+ uses new technology and is calibrated to identify this faint property. Be aware that body oil is also electrically conductive. Due to the tester’s enhanced sensitivity, dirty diamonds may test as moissanite. To avoid false/positive readings on dirty diamonds, ALWAYS CLEAN THE STONE on a cloth prior to testing. Periodically, also clean any accumulated body oil off of the probe tip by gently rubbing it on uncoated paper - SEE MANUAL. NEED HELP? Call GemOro at 800.527.0719 for immediate assistance. The GemOro UltraTester 3+ is the ultimate tester for diamond fraud protection that’s exclusively RECOMMENDED BY CHARLES & COLVARD, the manufacturer of created moissanite! The UltraTester 3+ features NEW ADVANCED EXCLUSIVE TECHNOLOGY capable of identifying the widest range of the electrically conductive moissanite material available, including the new super-low electrically conductive moissanite. OPERATING PROCEDURE & OWNERS MANUAL Congratulations on your purchase of the UltraTester 3+ from GemOro Superior GEMORO ULTRATESTER 3+ 2 Instruments, the most trusted name in gemological instrumentation for the jewelry industry. You’ve made a great choice. Built upon the foundation of the second generation and most popular tester to date, the UltraTester 3+ offers even more. -
Sensitization of Titanium Dioxide and Strontium Titanate Electrodes By
Subscriber access provided by University of Texas Libraries Sensitization of titanium dioxide and strontium titanate electrodes by ruthenium(II) tris(2,2'-bipyridine-4,4'-dicarboxylic acid) and zinc tetrakis(4-carboxyphenyl)porphyrin: an evaluation of sensitization efficiency for component photoelectrodes in a multipanel device Reza Dabestani, Allen J. Bard, Alan Campion, Marye Anne Fox, Thomas E. Mallouk, Stephen E. Webber, and J. M. White J. Phys. Chem., 1988, 92 (7), 1872-1878 • DOI: 10.1021/j100318a035 Downloaded from http://pubs.acs.org on February 2, 2009 More About This Article The permalink http://dx.doi.org/10.1021/j100318a035 provides access to: • Links to articles and content related to this article • Copyright permission to reproduce figures and/or text from this article The Journal of Physical Chemistry is published by the American Chemical Society. 1155 Sixteenth Street N.W., Washington, DC 20036 1872 J. Phys Chem. 1988, 92, 1872-1878 Sensitization of Titanium Dioxide and Strontium Titanate Electrodes by Ruthenium( I I) Trls (2,2’- bipyridine-4,4’-dicar box y lic acid) and Zinc Tetrakis (4-carboxy phen yl) porphyrin: An Evaluation of Sensitization Efficiency for Component Photoelectrodes in a Muitipanei Device Reza Dabestani, Allen J. Bard, Alan Campion, Marye Anne Fox,* Thomas E. Mallouk, Stephen E. Webber, and J. M. White Department of Chemistry, University of Texas, Austin, Texas 78712 (Received: December 1. 1986; In Final Form: October 6, 1987) The utility of polycrystalline anatase Ti02 and SrTi03 semiconductor electrodes sensitized by ruthenium(I1) tris(2,2’-bi- pyridine-4,4’-dicarboxylicacid) (1) and by zinc tetrakis(4-carboxypheny1)porphyrin (2) as component photoelectrodes in a multipanel array has been evaluated. -
The Journal of Gemmology Editor: Dr R.R
he Journa TGemmolog Volume 25 No. 8 October 1997 The Gemmological Association and Gem Testing Laboratory of Great Britain Gemmological Association and Gem Testing Laboratory of Great Britain 27 Greville Street, London Eel N SSU Tel: 0171 404 1134 Fax: 0171 404 8843 e-mail: [email protected] Website: www.gagtl.ac.uklgagtl President: Professor R.A. Howie Vice-Presidents: LM. Bruton, Af'. ram, D.C. Kent, R.K. Mitchell Honorary Fellows: R.A. Howie, R.T. Liddicoat Inr, K. Nassau Honorary Life Members: D.). Callaghan, LA. lobbins, H. Tillander Council of Management: C.R. Cavey, T.]. Davidson, N.W. Decks, R.R. Harding, I. Thomson, V.P. Watson Members' Council: Aj. Allnutt, P. Dwyer-Hickey, R. fuller, l. Greatwood. B. jackson, J. Kessler, j. Monnickendam, L. Music, l.B. Nelson, P.G. Read, R. Shepherd, C.H. VVinter Branch Chairmen: Midlands - C.M. Green, North West - I. Knight, Scottish - B. jackson Examiners: A.j. Allnutt, M.Sc., Ph.D., leA, S.M. Anderson, B.Se. (Hons), I-CA, L. Bartlett, 13.Se, .'vI.phil., I-G/\' DCi\, E.M. Bruton, FGA, DC/\, c.~. Cavey, FGA, S. Coelho, B.Se, I-G,\' DGt\, Prof. A.T. Collins, B.Sc, Ph.D, A.G. Good, FGA, f1GA, Cj.E. Halt B.Sc. (Hons), FGr\, G.M. Howe, FG,'\, oo-, G.H. jones, B.Se, PhD., FCA, M. Newton, B.Se, D.PhiL, H.L. Plumb, B.Sc., ICA, DCA, R.D. Ross, B.5e, I-GA, DGA, P..A.. Sadler, 13.5c., IGA, DCA, E. Stern, I'GA, DC/\, Prof. I. -
Evaluation of Brilliance, Fire, and Scintillation in Round Brilliant
Optical Engineering 46͑9͒, 093604 ͑September 2007͒ Evaluation of brilliance, fire, and scintillation in round brilliant gemstones Jose Sasian, FELLOW SPIE Abstract. We discuss several illumination effects in gemstones and University of Arizona present maps to evaluate them. The matrices and tilt views of these College of Optical Sciences maps permit one to find the stones that perform best in terms of illumi- 1630 East University Boulevard nation properties. By using the concepts of the main cutter’s line, and the Tucson, Arizona 85721 anti-cutter’s line, the problem of finding the best stones is reduced by E-mail: [email protected] one dimension in the cutter’s space. For the first time it is clearly shown why the Tolkowsky cut, and other cuts adjacent to it along the main cutter’s line, is one of the best round brilliant cuts. The maps we intro- Jason Quick duce are a valuable educational tool, provide a basis for gemstone grad- Jacob Sheffield ing, and are useful in the jewelry industry to assess gemstone American Gem Society Laboratories performance. © 2007 Society of Photo-Optical Instrumentation Engineers. 8917 West Sahara Avenue ͓DOI: 10.1117/1.2769018͔ Las Vegas, Nevada 89117 Subject terms: gemstone evaluation; gemstone grading; gemstone brilliance; gemstone fire; gemstone scintillation; gemstone cuts; round brilliant; gemstones; diamond cuts; diamonds. James Caudill American Gem Society Advanced Instruments Paper 060668R received Aug. 28, 2006; revised manuscript received Feb. 16, 8881 West Sahara Avenue 2007; accepted for publication Apr. 10, 2007; published online Oct. 1, 2007. Las Vegas, Nevada 89117 Peter Yantzer American Gem Society Laboratories 8917 West Sahara Avenue Las Vegas, Nevada 89117 1 Introduction are refracted out of the stone. -
Download PRIM II Refractive Index Chart
What is Refractive Index (R.I.)? What do the numbers Light travels at different speeds through in the brackets on this chart mean? different types of gemstones due to The numbers in the brackets indicate the Important Note structure of the stone. This affects the tolerance level for readings derived from All testers have been calibrated during the manufacturing process and requires no amount of light refraction and causes the the product. These slight fluctuations further adjustment or user intervention. Self-calibration should not be attempted and is bending of light. The slower the light's indicating a tolerance level are necessary not advised. speed in the material; the greater the due to the optical sensor and electronic REFRACTIVE INDEX CHART FOR bending effect. The refractive index of the components in the product. To minimize any risks associated, users should contact Presidium at gemstone can be defined as the ratio [email protected] or its service center for assistance. PRESIDIUM REFRACTIVE INDEX METER II between the speed of light in vacuum versus the speed of light in gemstone. In the event that users require the manufacturer to re-calibrate the unit, users will have to bear the associated to and fro freight cost for shipping of the unit to the Presidium service center. Presidium Instruments Please note that the gemstone tested on this product must have a flat surface and should Unit 7, 207 Henderson Road Singapore 159550 not be an opaque gemstone. www.presidium.com.sg Family Name of Stones Refractive Index Reading Family -
Quartz: a Bull's Eye on Optical Activity
Quartz: a Bull’s Eye on Optical Activity Elise A. Skalwold The Mineralogical Society of America William A. Bassett Title: Quartz: a Bull’s Eye on Optical Activity Authors: Elise Ann Skalwold & William Akers Bassett Edition: First edition Publisher: Mineralogical Society of America, Chantilly, Virginia, USA Copyright: © 2015 by the authors, artists, and photographers. Reproduced with permission. All Rights Reserved. ISBN: 978-0-939950-00-3 Photographer & Designer: Elise A. Skalwold Front cover: Natural quartz crystal 60 x 65 x 40 mm; Hot Springs, Arkansas; ex. Dr. R.W.M. Woodside collection. Back cover: Lab-grown quartz cluster, 140 mm x 90 mm (hydrothermally grown by Mila and Vladimir A. Klipov, R&D XTALS, Inc.). Below: Natural quartz crystals and basal sections. On-going collaboration with Cornell’s Professor Emeritus William A. Bassett is truly priceless to me for this and other projects in the wings, as well as for those over the past eight years of work and research together. Bill shares my enthusi- asm for exploring the fascinating aspects of the classical science of mineralogy, and as my co-author he sets the highest bar for accuracy. All students should be so lucky to have such a mentor. Elise A. Skalwold, 2015 Ithaca, New York Mineralogical Society of America Quartz: a Bull’s Eye on Optical Activity Elise A. Skalwold [email protected] William A. Bassett [email protected] Both Authors: Department of Earth & Atmospheric Sciences Snee Hall, Cornell University Ithaca, NY 14853 All photographs: Elise A. Skalwold Figure 1. The “bull’s eye” uniaxial optic figure characteristic of quartz is indicative of its optical activity. -
General Information- Michigan's Gem Stones
CONTENTS: INDUSTRIES MAP —————— FACING I GENERAL INFORMATION- —————— I MICHIGAN'S GEM STONES- —————— 4 ASSAYS AND TESTS———— ————— I I ARTICLES, PERIODICALS, BOOKS- —————12 SOCIETIES—————————————————— ———— 23 MUSEUMS—————————————————— ———— 26 GEOLOGIC TIME SCALE ———— 30 GEOLOGIC MAP —————— ————— 3 I NMICHIGAN DEPARTMENT OF CONSERVATION ^GEOLOGICAL SURVEY DIVISION FREE DISTRIBUTION ONLY PREFACE TO THIRD EDITION The first edition, published in April, 1958 was needed in responding to queries following a mineral show on the Depart- ment T-V program "Michigan Conservation11. The second edition, July, 1959) was characterized by the addition of the section on gem stones* An abstracted version of the second edition titled "Pebbles to Pendants" was published in the July, 1958 issue of "Michigan Conservation". The present 'third edition is another major revision. Among the new materials added are: l) bedrock geologic map, 2) mineral industries map, 3) rock column and time scale, 4) mineral and fossil sketches, and 5) locality sketch maps* These, along with the cover, were prepared by Jim Campbell of our staff. The book list has been expanded and several titles were added to the articles list. Suggestions received from Arthur Johnstone, of the Michigan Mineralogical Society, were particularly helpful. Information regarding mineral and lapidary businesses may be found in the appropriate advertising media as well as from many of the clubs. Robert W. Kelley, Geologist Geological Survey Division Michigan Dept. Conservation March, I960 Lansing MICHIGAN'S MIN ERAL EXTRACTING INDUSTRIES D NON-METALLIC B BRINE H SALT 0 CLAY 0 SHALE 9 DOLOMITE H LIMESTONE 13 SAND& GRAVELCPRINCIPAL AREA) H GLASS SAND 0 GYPSUM B SANDSTONE D MARLCPRINCIPAL AREA) B PEAT • MISCELLANEOUS STONE A METALLIC L COPPER A IRON O FUELS <D GAS • OIL MAJOR FIELDS € OIL & GAS INDIANA O H I O GENERAL INFORMATION INTRODUCTION Interest in collecting minerals and gem stones and in doing lapidary work certainly is on the increase today. -
Colourless Gemstones
GEMS THE gem DeteCTIVE: COLOURLess gemstONes superseded in the 1970s by a man-made gemstone called cubic zirconia that is still the most popular and common diamond imitation in modern jewellery due to its low cost, high dispersion and good hardness (8.5 on Mohs scale). Another man-made gemstone called synthetic Moissanite was introduced as a diamond simulant in the late 1990s. Although TED A synthetic Moissanite tests positive on a FFILI A diamond tester, it is easily distinguished from diamond by a property called double refraction, detected using a 10x loupe. This property is also displayed by zircon, a natural CCREESH, O’NEILS O’NEILS CCREESH, gemstone with a sub-adamantine lustre. M N N A Complicating the process of identification are treatments that may affect the value of gemstones. For example, a laser may be used to drill down to a dark diamond inclusion and remove it using acid in a process called GE COURTESY OF BREND OF COURTESY GE laser drilling. Also common is fracture filling, ma I where a high refractive-index lead glass is used to fill surface-reaching fractures to make Sparkling, colourless gemstones may People love to assume that their great ALTHOUGH them less visible. Fortunately, both of these appear similar to the naked eye but they grandma’s solitaire engagement ring SYNTHETIC treatments are easily identified using a loupe can vary significantly in identity, rarity contained a natural diamond by virtue MOISSANITE or microscope. TESTS POSITIVE and value. Making such distinctions of its age but they should think again. Some off-coloured diamonds may be ON A DIamOND requires the detective skills of a qualified Synthetically-produced sapphire, spinel and TESTER, IT CAN BE whitened using High Pressure High gemmologist. -
Magnetic Properties and Defects in Iron Implanted Strontium Titanate Single Crystals and Thin Films
Western University Scholarship@Western Electronic Thesis and Dissertation Repository 4-4-2012 12:00 AM Magnetic Properties and Defects in Iron Implanted Strontium Titanate Single Crystals and Thin films Misha Chavarha The University of Western Ontario Supervisor Lyudmila Goncharova The University of Western Ontario Graduate Program in Physics A thesis submitted in partial fulfillment of the equirr ements for the degree in Master of Science © Misha Chavarha 2012 Follow this and additional works at: https://ir.lib.uwo.ca/etd Part of the Condensed Matter Physics Commons Recommended Citation Chavarha, Misha, "Magnetic Properties and Defects in Iron Implanted Strontium Titanate Single Crystals and Thin films" (2012). Electronic Thesis and Dissertation Repository. 435. https://ir.lib.uwo.ca/etd/435 This Dissertation/Thesis is brought to you for free and open access by Scholarship@Western. It has been accepted for inclusion in Electronic Thesis and Dissertation Repository by an authorized administrator of Scholarship@Western. For more information, please contact [email protected]. DEFECTS AND MAGNETIC PROPERTIES OF IRON-IMPLANTED STRONTIUM TITANATE AND THIN FIMS (Spine title: Defects and magnetic properties of iron-implanted strontium titanate and thin films) (Thesis format: Monograph) by Misha Chavarha Graduate Program in Physics A thesis submitted in partial fulfillment of the requirements for the degree of Master of Science The School of Graduate and Postdoctoral Studies The University of Western Ontario London, Ontario, Canada © Misha Chavarha 2012 THE UNIVERSITY OF WESTERN ONTARIO SCHOOL OF GRADUATE AND POSTDOCTORAL STUDIES CERTIFICATE OF EXAMINATION Supervisor Examiners ______________________________ ______________________________ Dr. Lyudmila Goncharova Dr. Giovanni Fanchini ______________________________ Supervisory Committee Dr. Jeffrey Hutter ______________________________ ______________________________ Dr.