Use of Friction Stir Processing and Friction Stir Welding for Nitinol

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Use of Friction Stir Processing and Friction Stir Welding for Nitinol 111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111 us 20060283918Al (19) United States (12) Patent Application Publication (10) Pub. No.: US 2006/0283918 Al London et al. (43) Pub. Date: Dec. 21, 2006 (54) USE OF FRICTION STIR PROCESSING AND Related U.S. Application Data FRICTION STIR WELDING FOR NITINOL MEDICAL DEVICES (60) Provisional application No. 60/652,104, filed on Feb. 11, 2005. (76) Inventors: Blair D. London, San Luis Obispo, CA (US); Murray Mahoney, Camarillo, Publication Classification CA (US); Alan Pelton, Fremont, CA (US) (51) Int. Cl. B23K 20/12 (2006.01) Correspondence Address: (52) U.S. Cl. 2281112.1 PHILIP S. JOHNSON JOHNSON & JOHNSON (57) ABSTRACT ONE JOHNSON & JOHNSON PLAZA NEW BRUNSWICK, NJ 08933-7003 (US) Metallic materials may be joined utilizing a friction stir processing teclmique. The friction stir processing technique (21) Appl. No.: 111341,828 utilizes a shaped, rotating tool to move material from one side of the joint to be welded to the other without liquefying (22) Filed: Jan. 27, 2006 the base material. Sufficient downward force to consolidate the weld Retreating side of weld Leading edge of the 1 Advancing rotating tool shoulder side of weld Trailing edge of the rotating tool shou Ider Patent Application Publication Dec. 21, 2006 Sheet 1 of 2 US 2006/0283918 Al FIG. 1 Sufficient downward force to consolidate the weld Retreati ng side of weld Leading edge of the 1 Advancing rotating tool shoulder side of weld Trailing edge of the rotating tool shoulder Patent Application Publication Dec. 21, 2006 Sheet 2 of 2 US 2006/0283918 Al FIG. 2 Processing direction It­ US 2006/0283918 Al Dec. 21, 2006 1 USE OF FRICTION STIR PROCESSING AND significantly different from the base material and conse­ FRICTION STIR WELDING FOR NITINOL quently the weld zone has inferior mechanical properties MEDICAL DEVICES relative to the remainder of the tubing that limit the useful­ ness of the end product. Furthermore, welding dissimilar CROSS REFERENCE TO RELATED materials such as nickel-titanium alloys and stainless steel APPLICATION by fusion methods leads to the formation of brittle interme­ tallic compounds in the weld zone. [0001] This application claims the benefit of U.S. Provi­ sional Patent Application Ser. No. 60/652,104 filed Feb. 11, [0007] Accordingly, there exists a need for welding tech­ 2005. nique that avoids the problems described herein. SUMMARY OF THE INVENTION BACKGROUND OF THE INVENTION [0008] The present invention overcomes the disadvan­ [0002] I. Field of the Invention tages associated with currently utilized welding techniques [0003] The present invention relates to the manufacture of as briefly described above. medical devices, and more particularly, to the use offriction [0009] In accordance with one embodiment, the present is stir welding and friction stir processing of nickel-titanium directed to a method of welding nickel-titanium alloys. The alloys for use in the fabrication of medical devices and method comprises positioning a rotating tool in the joint components. between a first material and a second material, rotating the [0004] II. Discussion of the Related Art tool at a predetermined velocity to move the material from one side ofthe joint to the other side ofthe joint, and moving [0005] Nickel-titanium alloys may be utilized in the fab­ the rotating tool from one end of the joint to the other end rication of any number of medical devices such as stents, of the joint. vena cava filters, distal protection devices, occluders and catheters. These medical devices are typically machined [0010] In accordance with another embodiment, the from seamless microtubing. The raw material that will present invention is directed to a method of modifYing the ultimately yield a desired small diameter, thin-walled tube surface of a nickel-titanium alloy. The method comprises appropriate for the fabrication of the above-described plunging a rotating tool into the surface of a metallic devices, is a modestly sized round bar (e.g. one inch in material to a predetermined depth, rotating the tool at a diameter round bar stock) of predetermined length. In order predetermined velocity to manipulate the microstructure of to facilitate the reduction of the initial bar stock into a much the metallic material, and moving the rotating tool along the smaller tubing configuration, an initial clearance hole must surface of the metallic material. be placed into the bar stock that runs the length of the bar [0011] The process of friction stir welding of the present stock. These tube hollows, i.e. heavy walled tubes, may be invention relies not on the melting of material, but rather on created by "gun-drilling," i.e. high depth to diameter ratio the transfer of material from one side of a joint to the other drilling, the bar stock. Typically, the tubing is manufactured side of the joint. The speed of rotation and the design of the from bars on the order of ten mm to thirty mm that are gun friction stir welding tool determines the speed and amount of drilled to create the longitudinal hole. These tube hollows material transferred. Without melting the base material, none are then drawn to the final size. The outside dimension, the of the negative effects associated with currently utilized wall thickness and the inside dimension are dictated by the welding techniques are manifested in the final work product. sequence of drawing steps and choice of mandrels. The tubing may also be subjected to a number of "hot" and/or BRIEF DESCRIPTION OF THE DRAWINGS "cold" working steps to achieve particular properties for the tubing. It is important to note that other industrially relevant [0012] The foregoing and other aspects of the present, methods ofcreating the tube hollows from bar stock may be invention will best be appreciated with reference to the utilized by those skilled in the art of tubing manufacture. detailed description of the invention in conjunction with the accompanying drawings, wherein: [0006] An alternate approach to the manufacture oftubing involves starting from sheet or other flat raw material [0013] FIG. 1 is a diagrammatic representation of the products. In starting with a sheet of material, the manufac­ friction stir welding process in accordance with the present turing process is greatly simplified. Typically, the raw mate­ invention. rial sheet is formed into cylindrical structures and joined by [0014] FIG. 2 illustrates the surface of a friction stir any number of known welding techniques. This method has processed nickel-titanium sheet in accordance with the been tried, and documented by Horikawa et al. (SMST-94, present invention. 347-352, 1994), on a 0.4 mm thick nickel-titanium sheet. The sheet was electron beam welded and subsequently hot DETAILED DESCRIPTION OF THE worked and cold worked to 1.0 mm and 0.5 mm outer PREFERRED EMBODIMENTS diameters. What was observed was that the welded tubes often broke during cold drawing and had non-uniform iuner [0015] Friction stir welding is a process wherein a rotating surfaces. Although not mentioned in the Horikawa et al. tool is positioned in the joint between two pieces of material paper, the breaks during manufacture were likely due to the that are to be joined together and moved along the joint properties of the weld zone common to welding techniques while rotating at a predetermined velocity. The design ofthe that melt the base material. Such fusion welding techniques tool and the rotation thereof causes the transfer of material or methods, for example, electron beam, inert gas and laser, from one side of the joint to the other side of the joint, are known for creating weld zone microstructures that are thereby effectively welding the two pieces of material US 2006/0283918 Al Dec. 21, 2006 2 together. As this is substantially a "cold" weld, there are no in the formation of the tubing or flat-stock forms (sheet, deleterious effects on the base material caused by heating strip) that are eventually used to manufacture medical associated with currently utilized welding techniques. devices. Alternatively, it is envisioned that these techniques may also be used on the finished or semi-finished devices to [0016] Although this process may be utilized in welding provide unique characteristics, such as joining a nickel­ any number of metallic materials together, it is particularly advantageous in the welding of nickel-titanium alloys. For titanium device to a dissimilar component. example, one product that may be manufactured by friction [0020] Friction stir welding allows for the continuous stir welding is nickel-titanium microtubing, which could joining of materials in the solid state, i.e., without melting then be further processed into final dimensions for any and re-solidification occurring in the weld zone. This solid­ number of medical devices as briefly described above. The state welding technique employs a non-consumable rotating friction stir welded tubing may be utilized as microcatheters tool with superior high-temperature properties as compared or as a starting material for any number of medical devices including stents, distal protection filters, vena cava filters, to those of the material or materials to be joined. Any occluders and anastomotic devices. Friction stir welding number of suitable materials may be utilized in the fabrica­ may also be utilized to weld nickel-titanium alloys with tion of the rotating tool, including polycrystalline cubic other medical grade engineering materials, such as stainless boron nitride (peBN) and tungsten-rhenium (W-Re). The steel, titanium alloys (alpha, beta and alpha+beta), cobalt­ selection of tool material depends on the materials to be based alloys (L605) and refractory metal alloys. This tech­ joined. The tool may comprise any suitable shape depending nique may also be utilized to join or otherwise secure more on the application. highly radiopaque materials to nickel-titanium alloys, [0021] The rotating tool is similar to the tool bit utilized including gold, platinum, palladium, silver, tantalum, tung­ with a router or shapero In the exemplary embodiment sten and molybdenum.
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